STATUS TABLES FOR SW-846, THIRD EDITION FINAL UPDATES I, II, IIA, IIB, III, AND MIA AND DRAFT UPDATES IVA AND IVB REVISED NOVEMBER 2000 ------- HOW TO USE THIS DOCUMENT This document provides historical status information on EPA-published draft, proposed, and final SW-846 methods and chapters. It contains two status tables, namely; the "SW-846 Method Status Table," which is a listing of SW-846 methods; and the "Status Table for SW-846 Chapter Text and Other Documents", which lists all other documents in SW-846. Use the "SW-846 Method Status Table" as a reference guide to identify the historical and current status of published SW-846 methods. It also identifies the current location of the method in the manual. Methods in this status table are listed sequentially by method number. This order is different from that in the hard copy manual, where the methods are grouped by purpose and included as part of one of the chapters. Use the "Status Table for SW-846 Chapter Text and Other Documents" as a reference guide to identify the historical and current status of published chapters and other SW-846 documents (e.g., the Disclaimer). ------- SW-846 METHOD STATUS TABLE November 2000 Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 0010 0020 0030 " "" " FINAL UP. I (7/92) " ~ " " RN. UP. II (9/94) IIA(8/93) IIB(1/95) mm ~~ * " FIN. UP. Ill (12/96) IIIA(4/98) 0011 m 0023A (Revision of Method 23. 40 CFR Part 60) ~~ 0031 0040 0050 0051 DRAFT UP. IVA (1/98) ~~ ~ DRAFT UP.IVB (11/00) ~~ 25D Referral 25E Referral ~ METHOD TITLE Modified Method 5 Sampling Train Sampling for Selected Aldehyde and Ketone Emissions from Stationary Sources Source Assessment Sampling System (SASS) Sampling Method for Polychlorinated Dibenzo-p- Dioxms and Polychlonnated Dibenzofuran Emissions from Stationary Sources Determination of the Volatile Organic Content of Waste Samples Determination of Vapor Phase Organic Concentration in Waste Samples Volatile Organic Sampling Train Sampling Method for Volatile Organic Compounds (SMVOC) Sampling of Principal Organic Hazardous Constituents from Combustion Sources Using Tedlarฎ Bags Isokinetic HCI/CI2 Emission Sampling Train Midget Impinger HCI/CI, Emission Sampling Train SW-846 VOU CHAP/ SEC Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 CURRENT PROMUL- GATED METHOD 0010 RevO (9/86) 0011 RevO (12/96) 0020 RevO (9/86) 0023A Rev1 (12/96) Not promul- gated as part of SW-846. See40CFR 60. Appendix A Not promul- gated as part of SW-846. See40CFR 60, Appendix A 0030 RevO (9/86) 0031 RevO (12/96) 0040 RevO (12/96) 0050 RevO (12/96) 0051 RevO (12/96) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) - 1010 1020 - 1110 1310 ~* RNAL UP.) (7/92) " mm - 1020 A - 1310A 1311 FIN. UP. II (9/94) IIA(8/93) IIB(1/95) " ~ - - ~~ ~~ RN. UP. Ill (12/96) IIIA(4/98) 0060 0061 0100 - ~ 1030 - 1120 ~~ DRAFT UP.IVA (1/98) ~ ~~ - ~ - " " DRAFT UP. IVB (11/00) 207-1 Referral 207-2 Referral "~ 1040 1050 ~ ~ ~~ METHOD TITLE Determination of Metals in Stack Emissions Determination of Hexavalent Chromium Emissions from Stationary Sources Sampling for Formaldehyde and Other Carbonyl Compounds in Indoor Air Sampling Method for Isocyanates Analysis for Isocyanates by High Performance Liquid Chromatography (HPLC) Pensky-Martens Closed-Cup Method for Determining Ignitability Setafiash Closed-Cup Method for Determining Ignitability Ignitability of Solids Test Method for Oxidizing Solids Test Methods to Determine Substances Likely to Spontaneously Combust Corrosivity Toward Steel Dermal Corrosion Extraction Procedure (EP) Toxicity Test Method and Structural Integrity Test Toxicity Characteristic Leaching Procedure SW-846 VOL/ CHAP/ SEC Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 Volll Chap 10 VollC Chap 8 Sec 81 VollC Chap 8 Sec 81 VollC Chap 6 VollC Chap 6 VollC Chap 6 VollC Chap 8 Sec 8.2 VollC Chap 6 VollC Chap 8 Sec 8.4 VollC ChapS Sec 8.4 CURRENT PROMUL- GATED METHOD 0060 RevO (12/96) 0061 RevO (12/96) 0100 RevO (12/96) Not Promul- gated Not Promul- gated 1010 RevO (9/86) 1020A Rev1 (7/92) 1030 RevO (12/96) Not Promul- gated Not Promul- gated 1110 RevO (9/86) 1120 RevO (12/96) 1310A Rev1 (7/92) 1311 RevO (7/92) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 1320 1330 3005 3010 ~ 3020 3040 3050 mm ~" FINAL UP.I (7/92) " " 1330A 3005A 3010A " 3020A " 3050A " "~ RN. UP. II (9/94) IIA(8/93) IIB(1/95) 1312 (Up. II) " 3015 (Up. II) " " 3051 (Up. II) ~ RN. UP. Ill (12/96) IIIA(4/98) " " ~~ 3031 3040A 3050B ~ 3052 DRAFT UP. IVA (1/98) " ~ 301 5A " " 3051A DRAFT UP.IVB (11/00) " " ~~ ~~ ~~ " METHOD TITLE Synthetic Precipitation Leaching Procedure Multiple Extraction Procedure Extraction Procedure for Oily Wastes Acid Digestion of Waters for Total Recoverable or Dissolved Metals for Analysis by FLAA or ICP Spectroscopy Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by FLAA or ICP Spectroscopy Microwave Assisted Acid Digestion of Aqueous Samples and Extracts Acid Digestion of Aqueous Samples and Extracts for Total Metals for Analysis by GFAA Spectroscopy Acid Digestion of Oils for Metals Analysis by Atomic Absorption or ICP Spectrometry Dissolution Procedure for Oils, Greases, or Waxes Acid Digestion of Sediments, Sludges, and Soils Microwave Assisted Acid Digestion of Sediments, Sludges, Soils, and Oils Microwave Assisted Acid Digestion of Siliceous and Organically Based Matrices SW-846 VOU CHAP/ SEC VollC Chap 6 VollC Chap 6 VollC Chap 6 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 VollA Chap 3 Sec 3.2 CURRENT PROMUL- GATED METHOD 1312 RevO (9/94) 1320 RevO (9/86) 1330A Rev1 (7/92) 3005A Rev1 (7/92) 3010A Rev1 (7/92) 3015 RevO (9/94) 3020A Rev1 (7/92) 3031 RevO (12/96) 3040A Rev1 (12/96) 3050B Rev 2 (12/96) 3051 RevO (9/94) 3052 RevO (12/96) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date m parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW METHOD NUMBER THIRD ED. (9/86) [3060. in the 2nd Ed.] 3500 3510 3520 3540 ~~ 3550 ~ FINAL UP. I (7/92) 3500A 3510A 3520A 3540A ~ ~~ "" FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 3510B (Up. II) 3520B (Up. II) 3540B (Up. II) 3541 (Up. II) ~~ 3550A (Up II) ~ FIN. UP. Ill (12/96) IMA (4/98) 3060A 3500B 3510C 3520C 3535 3540C ~ 3542 3545 ~~ 3550B 3560 DRAFT UP.IVA (1/98) " ~~ 3535A 3545A ~ " DRAFT UP.IVB (11/00) 3500C ~~ 3535A (Replaces IVA version) 3545A (Replaces IVA version) 3546 3550C ~~ METHOD TITLE Alkaline Digestion for Hexavalent Chromium Organic Extraction and Sample Preparation Separatory Funnel Liquid- Liquid Extraction Continuous Liquid-Liquid Extraction Solid-Phase Extraction (SPE) Soxhlet Extraction Automated Soxhlet Extraction Extraction of Semivolatile Analytes Collected Using Method 0010 (Modified Method 5 Sampling Train) Pressurized Fluid Extraction (PFE) Microwave Extraction Ultrasonic Extraction Supercritical Fluid Extraction of Total Recoverable Petroleum Hydrocarbons SW-846 VOL/ CHAP/ SEC VollA Chap 3 Sec 3.2 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4 2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4 2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4 2.1 CURRENT PROMUL- GA7H> METHOD 3060A Rev1 (12/96) 3500B Rev 2 (12/96) 3510C Rev 3 (12/96) 3520C Rev 3 (12/96) 3535 RevO (12/96) 3540C Rev 3 (12/96) 3541 RevO (9/94) 3542 RevO (12/96) 3545 RevO (12/96) Not Promul- gated 3550B Rev 2 (12/96) 3560 RevO (12/96) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW METHOD NUMBER THIRD ED. (9/86) 3580 ~~ 3600 3610 3611 3620 3630 3640 3650 3660 FINAL UP.) (7/92) 3580A ~~ 3600A 3610A 3611 A 3620A 3630A " 3650A 3660A RN. UP. II (9/94) IIA(8/93) IIB(1/95) " 3600B (Up. II) " 3630B (Up. II) 3640A (Up. II) " " 3665 (Up. II) RN. UP. Ill (12/96) IIIA(4/98) 3561 mm 3585 3600C 3610B 361 1B 3620B 3630C " 3650B 3660B 3665A DRAFT UP.IVA (1/98) 3562 ~~ ~~ ~~ ~" " DRAFT UP.IVB (11/00) ~" ~ 3620C " " " METHOD TITLE Supercritical Fluid Extraction of Polynuclear Aromatic Hydrocarbons Supercritical Fluid Extraction of Polychlonnated Biphenyls (PCBs) and Organochlorine Pesticides Waste Dilution Waste Dilution for Volatile Organics Cleanup Alumina Cleanup Alumina Column Cleanup and Separation of Petroleum Wastes Flonsil Cleanup Silica Gel Cleanup Gel-Permeation Cleanup Acid-Base Partition Cleanup Sulfur Cleanup Sulfuric Acid/Permanganate Cleanup SW-846 VOU CHAP/ SEC VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4.2 2 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4 2.2 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4.2.2 VollB Chap 4 Sec 4.2.2 CURRENT PROMUL- GATED METHOD 3561 RevO (12/96) Not Promul- gated 3580A Rev1 (7/92) 3585 RevO (12/96) 3600C Rev 3 (12/96) 3610B Rev 2 (12/96) 361 1B Rev 2 (12/96) 3620B Rev 2 (12/96) 3630C Rev 3 (12/96) 3640A Rev1 (9/94) 3650B Rev 2 (12/96) 3660B Rev 2 (12/96) 3665A Rev1 (12/96) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 3810 ~ 3820 ~~ ~~ ~ ~ ~ ~~ FINAL UP. I (7/92) ~~ "~ " ~~ ~ ~~ ~~ FIN. UP. II (9/94) IIA(8/93) IIB(1/95) " 4010 (Up. MA) -" " " ~ ~~ RN. UP. Ill (12/96) IDA (4/98) ~~ ~~ 4000 401 OA 4015 4020 4030 4035 4040 4041 4042 4050 DRAFT UP.IVA (1/98) Noticed for removal from SW-846 ~ ~~ ~~ " " " * DRAFT UP.IVB (11/00) 3815 "~ "~ ~ ~~ ~" "" METHOD TITLE Headspace Screening Solid Samples for Volatile Organics Hexadecane Extraction and Screening of Purgeable Organics Immunoassay Screening for Pentachlorophenol by Immunoassay Screening for 2,4- Dichlorophenoxyacetic Acid by Immunoassay Screening for Polychlonnated Biphenyls by Immunoassay Soil Screening for Petroleum Hydrocarbons by Immunoassay Soil Screening for Pol/nuclear Aromatic Hydrocarbons by Immunoassay Soil Screening for Toxaphene by Immunoassay Soil Screening for Chlordane by Immunoassay Soil Screening for DDT by Immunoassay TNT Explosives in Soil by Immunoassay SW-846 VOL/ CHAP/ SEC VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 CURRENT PROMUL- GATED METHOD 3810 RevO (9/86) Not Promul- gated 3820 RevO (9/86) 4000 RevO (12/96) 401 OA Rev1 (12/96) 4015 RevO (12/96) 4020 RevO (12/96) 4030 RevO (12/96) 4035 RevO (12/96) 4040 RevO (12/96) 4041 RevO (12/96) 4042 RevO (12/96) 4050 RevO (12/96) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note* The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) ~~ ~ 5030 " 5040 FINAL UP.I (7/92) ~~ ~ 5030A ~ RN.UP. II (9/94) IIA(8/93) IIB(1/95) " ~~ ~ " ~~ ~ " 5040A (Up. II) FIN. UP. Ill (12/96) IIIA(4/98) 4051 ~ ~~ 5000 5021 5030B 5031 5032 5035 Deleted from SW-846 DRAFT UP. IVA (1/98) " 4500 4670 ~ ~ " ' DRAFT UP.IVB (11/00) " 4425 " ~ ~~ METHOD TITLE Hexahydro-1 ,3,5-trinitro-1 ,3,5- triazine (RDX) in Soil by Immunoassay Screening Extracts of Environmental Samples for Planar Organic Compounds (PAHs.PCBs.PCDDs/PCDFs) by a Reporter Gene on a Human Cell Line Mercury in Soil by Immunoassay Triazine Herbicides as Atrazine in Water by Quantitative Immunoassay Sample Preparation for Volatile Organic Compounds Volatile Organic Compounds in Soils and Other Solid Matrices Using Equilibrium Headspace Analysis Purge-and-Trap for Aqueous Samples Volatile, Nonpurgeable, Water-Soluble Compounds by Azeotropic Distillation Volatile Organic Compounds by Vacuum Distillation Closed-System Purge-and- Trap and Extraction for Volatile Organics in Soil and Waste Samples Analysis of Sorbent Cartridges from Volatile Organic Sampling Train (VOST):GasChro- matography/Mass Spectrometry Technique SW-846 VOU CHAP/ SEC VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.4 VollA Chap 3 Sec 3.3 VollB Chap 4 Sec 4.4 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 VollB Chap 4 Sec 4.2.1 Deleted from SW-846 CURRENT PROMUL- GATED METHOD 4051 RevO (12/96) Not Promul- gated Not Promul- gated Not Promul- gated 5000 RevO (12/96) 5021 RevO (12/96) 5030B Rev 2 (12/96) 5031 RevO (12/96) 5032 RevO (12/96) 5035 RevO (12/96) Deleted from SW-846 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note* The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 6010 " " " 7000 ซ 7020 7040 RNAL UP.I (7/92) ~~ 6010A ~ " " 7000A " FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 5041 (Up. II) 5050 (Up. II) 6020 (Up. II) " mm FIN. UP. Ill (12/96) IIIA(4/98) 5041A "~ 601 OB ~~ " mm "~ DRAFT UP.IVA (1/98) ~ 6020A 6200 6500 6800 7000B 7010 Noticed for removal from SW-846 Noticed for removal from SW-846 DRAFT UP. IVB (11/00) ~ 601 OC ~ " ซ METHOD TITLE Analysis for Desorption of Sorbent Cartridges from Volatile Organic Sampling Train (VOST) Bomb Preparation Method for Solid Waste Inductively Coupled Plasma- Atomic Emission Spectrometry Inductively Coupled Plasma - Mass Spectrometry Field Portable X-Ray Fluorescence Spectrometry for the Determination of Elemental Concentrations in Soil and Sediment Dissolved Inorganic Anions in Aqueous Matrices by Capillary Ion Electrophoresis Elemental and Speciated Isotope Dilution Mass Spectrometry 7000A (Promulgated): Atomic Absorption Methods 7000B (Draft): Flame Atomic Absorption Spectrophotometry Graphite Furnace Atomic Absorption Spectrophotometry Aluminum (Atomic Absorption, Direct Aspiration) Antimony (Atomic Absorption. Direct Aspiration) SW-846 VOL/ CHAP/ SEC VollB Chap 4 Sec 4.2.1 VdlC ChapS VollA ChapS Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 CURRENT PROMUL- GATED METHOD 5041A Rev1 (12/96) 5050 RevO (9/94) 6010B Rev 2 (12/96) 6020 RevO (9/94) Not Promul- gated Not Promul- gated Not Promul- gated 7000A Rev1 (7/92) Not Promul- gated 7020 RevO (9/86) 7040 RevO (9/86) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 7041 7060 7061 7080 7090 7091 7130 RNAL UP.I (7/92) 7061A ~ ~ 7081 RN. UP. II (9/94) IIA(8/93) IIB(1/95) 7060A (Up. II) " 7062 (Up. II) "~ 7080A (Up II) FIN. UP. Ill (12/96) MIA (4/98) 7063 DRAFT UP.PVA (1/98) Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 DRAFT UP.IVB (11/00) mm METHOD TITLE Antimony (Atomic Absorption. Furnace Technique) Arsenic {Atomic Absorption. Furnace Technique) Arsenic (Atomic Absorption, Gaseous Hydride) Antimony and Arsenic (Atomic Absorption, Borohydride Reduction) Arsenic in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) Barium (Atomic Absorption, Direct Aspiration) Barium (Atomic Absorption, Furnace Technique) Beryllium (Atomic Absorption, Direct Aspiration) Beryllium (Atomic Absorption, Furnace Technique) Cadmium (Atomic Absorption, Direct Aspiration) SW-846 VOL/ CHAP/ SEC VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 CURRENT PROMUL- GATED METHOD 7041 RevO (9/86) 7060A Rev1 (9/94) 7061A Rev1 (7/92) 7062 RevO (9/94) 7063 RevO (12/96) 7080A Rev1 (9/94) 7081 RevO (7/92) 7090 RevO (9/86) 7091 RevO (9/86) 7130 RevO (9/86) ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW METHOD NUMBER THIRD ED. (9/86) 7131 7140 7190 7191 7195 7196 7197 7198 7200 FINAL UP. I (7/92) 7196A HN. UP. II (9/94) IIA(8/93) IIB(1/95) 7131A (Up. II) RN. UP. Ill (12/96) MIA (4/98) 7199 DRAFT UP.IVA (1/98) Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 DRAFT UP.IVB (11/00) ~ METHOD TITLE Cadmium (Atomic Absorption, Furnace Technique) Calcium (Atomic Absorption. Direct Aspiration) Chromium (Atomic Absorption, Direct Aspiration) Chromium (Atomic Absorption, Furnace Technique) Chromium, Hexavalent (Coprecipitation) Chromium, Hexavalent (Colonmetric) Chromium, Hexavalent (Chelation/Extraction) Chromium, Hexavalent (Differential Pulse Polarography) Determination of Hexavalent Chromium in Drinking Water, Groundwater and Industrial Wastewater Effluents by Ion Chromatography Cobalt (Atomic Absorption, Direct Aspiration) SW-846 VOL/ CHAP/ SEC VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 CURRENT PROMUL- GATED METHOD 7131A Rev1 (9/94) 7140 RevO (9/86) 7190 RevO (9/86) 7191 RevO (9/86) 7195 RevO (9/86) 7196A Rev1 (7/92) 7197 RevO (9/86) 7198 RevO (9/86) 7199 RevO (12/96) 7200 RevO (9/86) 10 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 7201 7210 7380 7420 7421 7450 FINAL UP. I (7/92) 7211 7381 7430 RN. UP. II (9/94) NA(8/93) IIB(1/95) RN. UP. Ill (12/96) IIIA(4/98) DRAFT UP. IVA (1/98) Noticed for removal fnom SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 DRAFT UP.IVB (11/00) METHOD TITLE Cobalt (Atomic Absorption. furnace Technique) Copper (Atomic Absorption, Direct Aspiration) Copper (Atomic Absorption, Furnace Technique) Iron (Atomic Absorption, Direct Aspiration) Iron (Atomic Absorption, Furnace Technique) Lead (Atomic Absorption, Direct Aspiration) Lead (Atomic Absorption, Furnace Technique) Lithium (Atomic Absorption, Direct Aspiration) ftfagnesium (Atomic Absorption, Direct Aspiration) SW-846 VOL/ CHAP/ SEC VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 CURRENT PROMUL- GATED METHOD 7201 RevO (9/86) 7210 RevO (9/86) 7211 RevO (7/92) 7380 RevO (9/86) 7381 RevO (7/92) 7420 RevO (9/86) 7421 RevO (9/86) 7430 RevO (7/92) 7450 RevO (9/86) 11 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW METHOD NUMBER THIRD ED. (9/86) 7460 7470 7471 7480 7481 7520 FINAL UP. I (7/92) 7461 ~~ " FIN. UP. II (9/94) IIA(8/93) IIBJ1/95) 7470A (Up. II) 7471A (Up. II) ~~ FIN. UP. Ill (12/96) MIA (4/98) 7472 ~ DRAFT UP. IVA (1/98) Noticed for removal from SW-846 Noticed for removal from SW-846 ~~ 7471 B 7473 7474 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 DRAFT UP. IVB (11/00) ~ ~ METHOD TITLE Manganese (Atomic Absorption, Direct Aspiration) Manganese (Atomic Absorption, Furnace Technique) Mercury in Liquid Waste (Manual Cold-Vapor Technique) Mercury in Solid or Semisolid Waste (Manual Cold-Vapor Technique) Mercury in Aqueous Samples and Extracts by Anodic Stripping Voltammetry (ASV) Mercury in Solids and Solutions by Thermal Decomposition, Amalgamation, and Atomic Absorption Spectrophotometry Mercury in Sediment and Tissue Samples by Atomic Fluorescence Spectrometry Molybdenum (Atomic Absorption, Direct Aspiration) Molybdenum (Atomic Absorption, Furnace Technique) Nickel (Atomic Absorption, Direct Aspiration) SW-846 VOL/ CHAP/ SEC VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 oGC O.O VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3 3 CURRENT PROMUL- GATED METHOD 7460 RevO (9/86) 7461 RevO (7/92) 7470A Rev1 (9/94) 7471A Rev1 (9/94) 7472 RevO (12/96) Not Promul- gated Not Promul- gated 7480 RevO (9/86) 7481 RevO (9/86) 7520 RevO (9/86) 12 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW METHOD NUMBER THIRD ED. (9/86) 7550 7610 7740 7741 mm 7760 7770 FINAL UP. I (7/92) ~ mm 7760A 7761 FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 7741 A (Up. II) 7742 (Up. II) RN. UP. Ill (12/96) IIIA(4/98) 7521 7580 * ~ ~~ DRAFT UP.IVA (1/98) Noticed for removal from SW- 846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 ~ ~~ Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 . DRAFT UP. IVB (11/00) " ~ METHOD TITLE Nickel (Atomic Absorption, Furnace Method) Osmium (Atomic Absorption. Direct Aspiration) White Phosphorus (Pซ) by Solvent Extraction and Gas Chromatography Potassium (Atomic Absorption, Direct Aspiration) Selenium (Atomic Absorption, Furnace Technique) Selenium (Atomic Absorption, Gaseous Hydride) Selenium (Atomic Absorption, Borohydride Reduction) Silver (Atomic Absorption, Direct Aspiration) Silver (Atomic Absorption, Furnace Technique) Sodium (Atomic Absorption, Direct Aspiration) SW-846 VOU CHAP/ SEC VollA Chap 3 Sec 3.3 VollA Chap 3 oGC ป5.O VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 CURRENT PROMUL- GATED METHOD 7521 RevO (12/96) 7550 RevO (9/86) 7580 RevO (12/96) 7610 RevO (9/86) 7740 RevO (9/86) 7741A Rev1 (9/94) 7742 RevO (9/94) 7760A Revl (7/92) 7761 RevO (7/92) 7770 RevO (9/86) 13 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand comer of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 7840 7841 7870 7910 7911 7950 8000 FINAL UP. I (7/92) 7780 7951 8000A FIN. UP. II (9/94) IIA(8/93) 118(1/95) " FIN. UP. Ill (12/96) IMA (4/98) 8000B DRAFT UP.IVA (1/98) Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 Noticed for removal from SW-846 ~~ DRAFT UP.IVB (11/00) METHOD TITLE Strontium (Atomic Absorption, Direct Aspiration) Thallium (Atomic Absorption, Direct Aspiration) Thallium (Atomic Absorption, Furnace Technique) Tin (Atomic Absorption, Direct Aspiration) Vanadium (Atomic Absorption, Direct Aspiration) Vanadium (Atomic Absorption, Furnace Technique) Zinc (Atomic Absorption, Direct Aspiration) Zinc (Atomic Absorption, Furnace Technique) Determinative Chromatographic Separations SW-846 VOU CHAP/ SEC VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollA Chap 3 oGC o O VollA Chap 3 Sec 3 3 VollA Chap 3 Sec 3 3 VollA Chap 3 o6C o.o VollB Chap 4 Sec 4 3.1 CURRENT PROMUL- GATH> METHOD 7780 RevO (7/92) 7840 RevO (9/86) 7841 RevO (9/86) 7870 RevO (9/86) 7910 RevO (9/86) 7911 RevO (9/86) 7950 RevO (9/86) 7951 RevO (7/92) 8000B Rev 2 (12/96) 14 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 8010 8015 8020 8030 ~ 8040 8060 FINAL UP.I (7/92) 8010A 8011 801 5A ~ 8021 8030A "~ 8040A ~~ ~ FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 8010B (Up. II) " 8020A (Up. II) 8021A (Up. II) 8031 (Up. II) 8032 (Up. II) ~~ ~~ ~ FIN. UP. Ill (12/96) IMA (4/98) Deleted from SW-846 8015B Deleted from SW-846 8021 B Deleted from SW-846 8032A 8033 Deleted from SW-846 8041 Deleted from SW-846 DRAFT UP.IVA (1/98) " ~" ~~ ~" DRAFT UP.IVB (11/00) ~ 801 5C ~~ 8041 A ~~ METHOD TITLE Halogenated Volatile Organics by Gas Chromatography 1 ,2-Dibromoethane and 1 ,2- Dibromo-3-chloropropane by Microextraction and Gas Chromatography Nonhalogenated Organics Using GC/FID Aromatic Volatile Organics by Gas Chromatography Aromatic and Halogenated Volatiles by Gas Chromatography Using Photoionization and/or Electrolytic Conductivity Detectors Acrolein and Acrylonitn'le by Gas Chromatography Acrylonitnle by Gas Chromatography Acrylamide by Gas Chromatography Acetonitnle by Gas Chromatography with Nitrogen-Phosphorus Detection Phenols by Gas Chromatography Phenols by Gas Chromatography Phthalate Esters SW-846 VOL/ CHAP/ SEC Deleted from SW-846 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 CURRENT PROMUL- GATED METHOD Deleted from SW-846 8011 RevO (7/92) 801 SB Rev 2 (12/96) Deleted from SW-846 8021 B Rev 2 (12/96) Deleted from SW-846 8031 RevO (9/94) 8032A Rev1 (12/96) 8033 RevO (12/96) Deleted from SW-846 8041 RevO (12/96) Deleted from SW-846 15 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) ~~ 8080 8090 "" 8100 FINAL UP. I (7/92) 8070 " 8110 FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 8061 (Up. II) ~~ 8080A (Up. II) 8081 (Up. II) ~~ ~~ " FIN. UP. Ill (12/96) IIIA(4/98) 8061A 8070A Deleted from SW-846 8081 A 8082 Deleted from SW-846 8091 ~~ " Deleted from SW-846 8111 DRAFT UP. IVA (1/98) 8081 B 8082A " " " DRAFT UP. IVB (11/00) " 8081 B (Replaces IVA version) 8082A (Replaces IVA version) 8085 8095 ~ " ~~ METHOD TITLE Phthalate Esters by Gas Chromatography with Electron Capture Detection (GC/ECD) Nitrosamines by Gas Chromatography Organochlorine Pesticides and Polychlorinated Biphenyls by Gas Chromatography Organochlorine Pesticides by Gas Chromatography Polychlorinated Biphenyls (PCBs) by Gas Chromatography Compound-independent Elemental Quantitation of Pesticides by Gas Chromatography with Atomic Emission Detection (GC/AED) Nitroaromatics and Cyclic Ketones Nitroaromatics and Cyclic Ketones by Gas Chromatography Explosives by Gas Chromatography Polynuclear Aromatic Hydrocarbons Haloethers by Gas Chromatography Haloethers by Gas Chromatography SW-846 VOU CHAP/ SEC VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.31 Deleted from SW-846 VollB Chap 4 Sec 4.31 VollB Chap 4 Sec431 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 CURRENT PROMUL- GATED METHOD 8061A Rev1 (12/96) 8070A Rev1 (12/96) Deleted from SW-846 8081 A Rev1 (12/96) 8082 RevO (12/96) Not Promul- gated Deleted from SW-846 8091 RevO (12/96) Not Promul- gated 8100 RevO (9/86) Deleted from SW-846 8111 RevO (12/96) 16 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note. The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 8120 ~~ 8140 8150 8240 8250 RNAL UP.I (7/92) ~ ~~ 8141 8150A 8240A 8260 FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 8120A (Up. II) 8121 (Up. II) "" 8141A (Up. II) 81 SOB (Up. II) 8151 (Up. II) 8240B (Up. II) 8250A (Up. II) 8260A (Up. II) RN. UP. Ill (12/96) IIIA (4/98) Deleted from SW-846 ~ 8131 Deleted from SW-846 Deleted from SW-846 8151A Deleted from SW-846 Deleted from SW-846 8260B DRAFT UP.IVA (1/98) " ~~ ~" 8141B mm DRAFT UP. IVB (11/00) ~ " 8141B (Replaces IVA version) " METHOD TITLE Chlorinated Hydrocarbons by Gas Chromatography Chlorinated Hydrocarbons by Gas Chromatography: Capi'flary Column Technique Aniline and Selected Derivatives by Gas Chromatography Organophosphorus Pesticides 8141 A (Promulgated): Organophosphorus Compounds by Gas Chromatography: Capillary Column Technique 8141 B (Draft): Organophosphorus Compounds by Gas Chromatography Chlorinated Herbicides by Gas Chromatography Chlorinated Herbicides by GC Using Methylation or Pentafluorobenzylation Denvatization Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Volatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) SW-846 VOU CHAP/ SEC Deleted from SW-846 VollB Chap 4 Sec 4.3.1 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 VollB Chap 4 Sec 4.3.1 Deleted from SW-846 Deleted from SW-846 VollB Chap 4 Sec 4.3.2 CURRENT PROMUL- GATED METHOD Deleted from SW-846 8121 RevO (9/94) 8131 RevO (12/96) Deleted from SW-846 8141A Rev1 (9/94) Deleted from SW-846 8151A Rev1 (12/96) Deleted from SW-846 Deleted from SW-846 8260B Rev 2 (12/96) 17 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand comer of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 8270 8280 _ 8310 FINAL UP.) (7/92) 8270A _ _ RN. UP. II (9/94) IIA(8/93) IIB(1/95) 8270B (Up II) 8275 (Up. II) .. 8290 (Up. II) RN. UP. Ill (12/96) MIA (4/98) 8270C 8275A 8280A .. DRAFT UP.FVA (1/98) 8270D 8280B 8290A DRAFT UP.IVB (11/00) 8261 _ _ _ _ METHOD TITLE Volatile Organic Compounds by Vacuum Distillation in Combination with Gas Chromatography/Mass Spectrometry (VD/GC/MS) Semivolatile Organic Compounds by Gas Chromatography/Mass Spectrometry (GC/MS) Semivolatile Organic Compounds (PAHs and PCBs) in Soils/Sludges and Solid Wastes Using Thermal Extraction/Gas Chromatogra- phy/Mass Spectrometry (TE/GC/MS) 8280A (Promulgated): The Analysis of Polychlonnated Dibenzo-p- Dioxms and Polychlorinated Dibenzofurans by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) 8280B (Draft): Polychlorinated Dibenzo-p- Dioxins and Polychlorinated Dibenzofurans by High Resolution Gas Chromatography/Low Resolution Mass Spectrometry (HRGC/LRMS) Polychlorinated Dibenzodioxins (PCDDs) and Polychlonnated Dibenzofurans (PCDFs) by High-Resolution Gas Chromatography/ High-Resolution Mass Spectrometry (HRGC/HRMS) Polynuclear Aromatic Hydrocarbons SW-846 VOL/ CHAP/ SEC VollB Chap 4 Sec 4 3.2 VollB Chap 4 Sec 4.3.2 VollB Chap 4 Sec 4.3 2 VollB Chap 4 Sec 4.3 2 VollB Chap 4 Sec 4.3.2 VollB Chap 4 Sec 4.3.3 CURRENT PROMUL- GATED METHOD Not Promul- gated 8270C Rev 3 (12/96) 8275A Rev1 (12/96) 8280A Rev1 (12/96) 8290 RevO (9/94) 8310 RevO (9/86) 18 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) FINAL UP.I (7/92) RN. UP. II (9/94) IIA(8/93) IIB(1/95) 8315 (Up. II) 8316 (Up. II) 8318 (Up. II) 8321 (Up. II) 8330 (Up. II) 8331 (Up. II) 8410 (Up. II) FIN. UP. W (12/96) MIA (4/98) 831 5A ~~ 8321A 8325 8332 8430 DRAFT UP.IVA (1/98) 8321 B 8330A DRAFT UP.IVB (11/00) 8318A 8321 B (Replaces IVA version) METHOD TITLE Determination of Carbonyl Compounds by High Performance Liquid Chromatography (HPLC) Acrylamide, Acrylonitnle and Acrolein by High Performance Liquid Chromatography (HPLC) A/-Methylcarbamates by High Performance Liquid Chromatography (HPLC) Solvent-Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Thermo- pray/Mass Spectrometry (HPLC/TS/MS) or Ultraviolet (UV) Detection Solvent Extractable Nonvolatile Compounds by High Performance Liquid Chromatography/Particle Beam/Mass Spectrometry (HPLC/PB/MS) Nitroaromatics and Nitramines by High Performance Liquid Chromatography (HPLC) Tetrazene by Reverse Phase High Performance Liquid Chromatography (HPLC) Nitroglycerine by High Performance Liquid Chromatography Gas Chromatography/Fourier Transform Infrared (GC/FT-IR) Spectrometry for Semivolatile Organics: Capillary Column Analysis of Bis(2-chloroethyl) Ether and Hydrolysis Products by Direct Aqueous Injection GC/FT-IR SW-846 VOU CHAP/ SEC VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.3 VollB Chap 4 Sec 4.3.4 VollB Chap 4 Sec 4.3.4 CURRENT PROMUL- GATED METHOD 831 5A Revl (12/96) 8316 RevO (9/94) 8318 RevO (9/94) 8321A Rev1 (12/96) 8325 RevO (12/96) 8330 RevO (9/94) 8331 RevO (9/94) 8332 RevO (12/96) 8410 RevO (9/94) 8430 RevO (12/96) 19 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) " mm " mm mm 9010 9012 " 9020 HNAL UP.) (7/92) ~ " ~ ~~ ~ " 9010A ~~ 9013 9020A FIN. UP. II (9/94) IIA(8/93) IIB(1/95) ~ "" ~ ~~ ~~ " " " ~~ 9020B (Up. II) RN. UP. Ill (12/96) IMA (4/98) 8440 ~~ 8515 8520 ~~ "~ " 901 OB 901 2A "~ 9014 " DRAFT UP.IVA (1/98) " ~~ 9000 9001 " " DRAFT UP. IVB (11/00) ~~ 8510 8535 8540 ~~ ~~ METHOD TITLE Total Recoverable Petroleum Hydrocarbons by Infrared Spectrophotometry Colorimetric Screening Procedure for RDX and HMX in Soil Colorimetric Screening Method for Trinitrotoluene (TNT) in Soil Continuous Measurement of Formaldehyde in Ambient Air Screening Procedure for Total Volatile Organic Halides in Water Pentachlorophenol by UV- induced Colorimetry Determination of Water in Waste Materials by Karl Fischer Titration Determination of Water in Waste Materials by Quantitative Calcium Hydride Reaction Total and Amenable Cyanide: Distillation Total and Amenable Cyanide (Automated Colonmetric, with Off-line Distillation) Cyanide Extraction Procedure for Solids and Oils Titrimetric and Manual Spectrophotometnc Determinative Methods for Cyanide Total Organic Halides (TOX) SW-846 VOL/ CHAP/ SEC VollB Chap 4 Sec 4.3.4 VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.3.5 VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.5 VollA Chap 3 Sec 3.3 VollA Chap 3 Sec 3.3 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 CURRENT PROMUL- GATED METHOD 8440 RevO (12/96) Not Promul- gated 8515 RevO (12/96) 8520 RevO (12/96) Not Promul- gated Not Promul- gated Not Promul- gated Not Promul- gated 9010B Rev 2 (12/96) 901 2A Rev1 (12/96) 9013 RevO (7/92) 9014 Rev 0(12/96) 9020B Rev 2 (9/94) 20 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) " 9022 ~~ 9030 " 9035 9036 9038 9040 9041 9045 9050 FINAL UP.I (7/92) 9021 " 9030A 9031 ~~ " ~ " 9041A 9045A " FIN. UP. II (9/94) IIA(8/93) IIB(1/95) ~~ ~~ mm ~~ ~~ ~~ ~ " 9040A (Up. II) 9040B (Up. IIB) " 9045B (Up. II) 9045C (Up. IIB) " FIN. UP. Ill (12/96) IIIA(4/98) ~ ~ 9023 9030B " 9034 ~~ ~~ ~ 9050A DRAFT UP.IVA (1/98) " "" ~~ " ~ mm DRAFT UP.IVB (11/00) ~ "~ ~ ~ mm ~ METHOD TITLE Purgeable Organic Halides (POX) Total Organic Halides (TOX) by Neutron Activation Analysis Extractable Organic Halides (EOX) in Solids Acid-Soluble and Acid- Insoluble Sulfides: Distillation Extractable Sulfides Titnmetric Procedure for Acid- Soluble and Acid-Insoluble Sulfides Sulfate (Colorimetric, Automated, Chloranilate) Sulfate (Colorimetric. Automated, Methylthymol Blue, AA II) Sulfate (Turbidimetnc) pH Electrometric Measurement pH Paper Method Soil and Waste pH Specific Conductance SW-846 VOU CHAP/ SEC VollC Chap 5 VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC ChapS VollC Chap 6 VollC Chap 6 VollC Chap 6 CURRENT PROMUL- GATED METHOD 9021 RevO (7/92) 9022 RevO (9/86) 9023 RevO (12/96) 9030B Rev 2 (12/96) 9031 RevO (7/92) 9034 RevO (12/96) 9035 RevO (9/86) 9036 RevO (9/86) 9038 RevO (9/86) 9040B Rev 2 1/95 9041A Rev1 (7/92) 9045C Rev 3 1/95 9050A Rev1 (12/96) 21 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) ~ 9060 9065 9066 9067 9070 (1664 refer- ral) FINAL UP. I (7/92) ~~ ~~ ~~ ~~ FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 9056 (Up. II) ~~ ~~ FIN. UP. Ill (12/96) IIIA(4/98) ~ 9057 -- ~~ ~~ ~~ Title and text replaced with referral to Method 1664- method no. "9070" remains at top of referral page and in table of contents (Up. MIA) DRAFT UP.IVA (1/98) ~~ " " DRAFT UP.IVB (11/00) 9056A 9058 - METHOD TITLE Determination of Inorganic Anions by Ion Chromatography Determination of Chloride from HCI/CI2 Emission Sampling Train (Methods 0050 and 0051 ) by Anion Chromatography Determination of Perchlorate Using Ion Chromatography with Chemical Suppression Conductivity Detection Total Organic Carbon Phenolics (Spectrophotometric, Manual 4-AAP with Distillation) Phenolics (Colonmetnc, Automated 4-AAP with Distillation) Phenolics (Spectrophotometric, MBTH with Distillation) 9070. title and text removed- Total Recoverable Oil and Grease (Gravimetric. Separatory Funnel Extraction) Method 9070 page and table of contents entry under Method 9070 refer reader to: Method 1664: n-Hexane Extractable Material (HEM; Oil and Grease) and Silica Gel Treated n-Hexane Extractable Material (SGT-HEM; Non- polar Material) by Extraction and Gravimetry SW-846 VOL/ CHAP/ SEC VdlC Chap 5 VollC Chap 5 VdlC ChapS VollC ChapS VdlC ChapS VdlC ChapS VdlC ChapS VollC Chap 5 CURRENT PROMUL- GATED METHOD 9056 RevO (9/94) 9057 RevO (12/96) Not Promul- gated 9060 RevO (9/86) 9065 RevO (9/86) 9066 RevO (9/86) 9067 RevO (9/86) The current promulgated version of Method 1664 is Revision A1 See 40 CFR 136. Appendix A 1 Method 1664 Revision A (EPAPublication No. EPA-821-R-98-0021 is available via the Internet athttpV/wwww.epa oov/OST. It is also available from the National Technical Information Service (NTIS), NTIS Publication No PB99-121949 (call 703-605-6000 or 800-553-6847). 22 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 9071 " " 9080 9081 9090 9095 FINAL UP. I (7/92) ~~ " ~ " 9090A FIN. UP. II (9/94) IIA(8/93) IIB(1/95) 9071A (Up. II) 9075 (Up. II) 9076 (Up. II) 9077 (Up. II) " " mm 9096 (Up. II) FIN. UP. Ill (12/96) IIIA(4/98) 9071 B (Up IDA) 9078 9079 ~~ ~~ " 9095A DRAFT UP.IVA (1/98) " 9074 ~~ " DRAFT UP.IVB (11/00) ~ ~~ " " METHOD TITLE n-Hexane Extractable Material (HEM) for Sludge, Sediment, and Solid Samples Turbidimetric Screening Method for Total Recoverable Petroleum Hydrocarbons in Soil Test Method for Total Chlorine in New and Used Petroleum Products by X-Ray Fluorescence Spectrometry (XRF) Test Method for Total Chlorine in New and Used Petroleum Products by Oxidative Combustion and Microcoulometry Test Methods for Total Chlorine in New and Used Petroleum Products (Field Test Kit Methods) Screening Test Method for Pol/chlorinated Biphenyls in Soil Screening Test Method for Polychlorinated Biphenyls in Transformer Oil Cation-Exchange Capacity of Soils (Ammonium Acetate) Cation-Exchange Capacity of Soils (Sodium Acetate) Compatibility Test for Wastes and Membrane Liners Paint Filter Liquids Test Liquid Release Test (LRT) Procedure SW-846 VOL/ CHAP/ SEC VollC Chap 5 VollB Chap 4 Sec 4.5 VollC ChapS VollC ChapS VollC ChapS VollB Chap 4 Sec 4.5 VollB Chap 4 Sec 4.5 VollC Chap 6 VollC Chap 6 VollC Chap 6 VollC Chap 6 VollC Chap 6 CURRENT PROMUL- GATED METHOD 9071 B Rev 2 (4/98) Not Promul- gated 9075 RevO (9/94) 9076 RevO (9/94) 9077 RevO (9/94) 9078 RevO (12/96) 9079 RevO (12/96) 9080 RevO (9/86) 9081 RevO (9/86) 9090A Rev1 (7/92) 9095A Rev1 (12/96) 9096 RevO (9/94) 23 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 9100 9131 9132 9200 "" 9250 FINAL UP. I (7/92) ~~ ~ ~~ FIN. UP. II (9/94) IIA(8/93) IIB(1/95) ~ " FIN. UP. in (12/96) MIA (4/98) Deleted from SW-846 9210 9211 9212 9213 9214 9215 "~ ~~ DRAFT UP.IVA (1/98) 9216 " DRAFT UP.IVB (11/00) 9210A METHOD TITLE Saturated Hydraulic Conductivity, Saturated Leachate Conductivity, and Intrinsic Permeability Total Coliform: Multiple Tube Fermentation Technique Total Coliform: Membrane- Filter Technique Nitrate Potentiometric Determination of Nitrate in Aqueous Samples with Ion-selective Electrode Potentiometric Determination of Bromide in Aqueous Samples with Ion-Selective Electrode Potentiometric Determination of Chlonde in Aqueous Samples with Ion-Selective Electrode Potentiometric Determination of Cyanide in Aqueous Samples and Distillates with Ion-Selective Electrode Potentiometric Determination of Fluoride in Aqueous Samples with Ion-Selective Electrode Potentiometric Determination of Sulfide in Aqueous Samples and Distillates with Ion-Selective Electrode Potentiometric Determination of Nitrite in Aqueous Samples with Ion-Selective Electrode Chloride (Colorimetric, Automated Ferricyanide AAI) SW-846 VOU CHAP/ SEC VollC Chap 6 VollC Chap 5 VollC Chap 5 Deleted from SW-846 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 VollC Chap 5 CURRENT PROMUL- GATED METHOD 9100 RevO (9/86) 9131 RevO (9/86) 9132 RevO (9/86) Deleted from SW-846 9210 RevO (12/96) 9211 RevO (12/96) 9212 RevO (12/96) 9213 RevO (12/96) 9214 RevO (12/96) 9215 RevO (12/96) Not Promul- gated 9250 RevO (9/86) 24 ------- SW-846 METHOD STATUS TABLE November 2000 (continued) Note1 The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods that were formally deleted from the manual and are no longer supported by OSW. METHOD NUMBER THIRD ED. (9/86) 9251 9252 9310 9315 9320 HCN Test Meth. H2S Test Meth. FINAL UP.) (7/92) HCN Test Meth. H2S Test Meth. FIN. UP. 11(9/94) IIA(8/93) IIB(1/95) "~ 9252A (Up. II) 9253 (Up. II) HCN Test Method (Up. II) H2S Test Method (Up. II) FIN. UP. II) (12/96) IIIA(4/98) " Deleted from SW-846 HCN Test Method H2S Test Method DRAFT UP.IVA (1/98) ~~ ซ DRAFT UP.IVB (11/00) " METHOD TITLE Chloride (Colorimetric. Automated Ferricyanide AAII) Chloride (Trtrimetric. Mercuric Nitrate) Chloride (Titrimetric, Silver Nitrate) Gross Alpha and Gross Beta Alpha-Emitting Radium Isotopes Radium-228 Test Method to Determine Hydrogen Cyanide Released from Wastes Test Method to Determine Hydrogen Sulfide Released from Wastes SW-846 VOL/ CHAP/ SEC VollC Chap 5 Deleted from SW-846 VollC Chap 5 VollC Chap 6 VollC Chap 6 VollC Chap 5 VollC Chap 7 Sec 7.3.3.2 VollC Chap 7 Sec 7.3.4.2 CURRENT PROMUL- GATED METHOD 9251 RevO (9/86) Deleted from SW-846 9253 RevO (9/94) 9310 RevO (9/86) 9315 RevO (9/86) 9320 RevO (9/86) Guidance Method Only Guidance Method Only 25 ------- STATUS TABLE FOR SW-846 CHAPTER TEXT AND OTHER DOCUMENTS November 2000 Note: The date in parentheses is the date found at the bottom right hand comer of the document. The check mark (/) indicates that the material was revised in that update TITLE Disclaimer Abstract Table of Contents Method Index and Conversion Table Preface and Overview Acknowledgements Chapter One Quality Control Chapter Two Choosing the Correct Procedure Chapter Three Inorganic Analytes Chapter Four Organic Analytes Chapter Five Miscellaneous Test Methods Chapter Six Properties Chapter Seven Characteristics Introduction and Regulatory Definitions THIRD ED. (9/86) - / S S / / / / / / / / / FINAL UP. 1 (7/92) / / / - - - / / / / FIN. UP. II (9/94) IIA (8/93) IIB (1/95) - S (Up. II) s (Up. II and IIB) - - - - / (Up. II) / (Up. II) / (Up. II) / (Up. II) s (Up. II and IIB) / (Up. II) FINAL UP. Ill (12/96) UP. IMA (4/98) / - / (Up. Ill and MIA) - / - - / (Up. Ill) / (Up. Ill) / (Up. Ill) / (Up. Ill and IIIA) / / (Up. Ill) DRAFT UP. IVA (1/98) - / - - - - V / / / DRAFT UP. IVB (11/00) - - / (Replaces IVA version) - - - - / (Replaces IVA version) / (Replaces IVA version) S (Replaces IVA version) / (Replaces IVA version) SW-846 VOLUME LOCATION All Vols All Vols All Vols All Vols All Vols VollA All Vols VollA VollA VollB VollC VollC VollC CURRENT FINAL VERSION Rev1 (12/96) Rev 2 (9/94) Rev 5 (4/98) RevO (9/86) Rev1 (12/96) RevO (9/86) Rev1 (7/92) Rev 3 (12/96) Rev 3 (12/96) Rev 3 (12/96) Rev 3 (4/98) Rev 3* (12/96) Rev 3 (12/96) 26 ------- STATUS TABLE FOR SW-846 CHAPTER TEXT AND OTHER DOCUMENTS November 2000 (continued) Note: The date in parentheses is the date found at the bottom right hand corner of the document. The check mark (/) indicates that the material was revised in that update. TITLE Chapter Eight Methods for Determining Characteristics Chapter Nine Sampling Plan Chapter Ten Sampling Methods Chapter Eleven Ground Water Monitoring Chapter Twelve Land Treatment Monitoring Chapter Thirteen Incineration Appendix Company References THIRD ED. (9/86) / / / / / / / FINAL UP. 1 (7/92) - - - - FIN. UP. II (9/94) HA (8/93) IIB (1/95) / (Up. II) - - - - FINAL UP. Ill (12/96) UP. IMA (4/98) / (Up. Ill) - / (Up. Ill) - - DRAFT UP. IVA (1/98) - - - - DRAFT UP. IVB (11/00) ^ - / - - - - SW-846 VOLUME LOCATION VollC Volll Volll Volll Volll Volll All Vols CURRENT FINAL VERSION Rev 2 (12/96) RevO (9/86) Rev1* (12/96) RevO (9/86) RevO (9/86) RevO (9/86) RevO (9/86) The published final versions of Chapter Six and Chapter Ten do not contain the correct revision number in the footer. The correct revision numbers are reported in this table. The revision numbers for these chapters will be corrected with the next final chapter revision. 27 ------- |