STATUS TABLES FOR
SW-846, THIRD EDITION
FINAL UPDATES I, II, IIA, IIB, III, AND MIA
AND DRAFT UPDATES IVA AND IVB
REVISED NOVEMBER 2000
-------
HOW TO USE THIS DOCUMENT
This document provides historical status information on EPA-published draft, proposed, and
final SW-846 methods and chapters. It contains two status tables, namely; the "SW-846 Method
Status Table," which is a listing of SW-846 methods; and the "Status Table for SW-846 Chapter
Text and Other Documents", which lists all other documents in SW-846.
Use the "SW-846 Method Status Table" as a reference guide to identify the historical and
current status of published SW-846 methods. It also identifies the current location of the method
in the manual. Methods in this status table are listed sequentially by method number. This order
is different from that in the hard copy manual, where the methods are grouped by purpose and
included as part of one of the chapters.
Use the "Status Table for SW-846 Chapter Text and Other Documents" as a reference guide
to identify the historical and current status of published chapters and other SW-846 documents
(e.g., the Disclaimer).
-------
SW-846 METHOD STATUS TABLE
November 2000
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
0010
0020
0030
™"
•""
"
FINAL
UP. I
(7/92)
™
"
— —
~™
"™
"
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
mm
™ —
••
~~
*•
"
FIN. UP. Ill
(12/96)
IIIA(4/98)
—
0011
™ m
0023A
(Revision
of Method
23. 40 CFR
Part 60)
~~
0031
0040
0050
0051
DRAFT
UP. IVA
(1/98)
—
~~
—
—
—
~™
DRAFT
UP.IVB
(11/00)
—
~~
25D
Referral
25E
Referral
—
—
—
~™
METHOD TITLE
Modified Method 5
Sampling Train
Sampling for Selected
Aldehyde and Ketone
Emissions from Stationary
Sources
Source Assessment
Sampling System
(SASS)
Sampling Method for
Polychlorinated Dibenzo-p-
Dioxms and Polychlonnated
Dibenzofuran Emissions from
Stationary Sources
Determination of the Volatile
Organic Content of Waste
Samples
Determination of Vapor
Phase Organic Concentration
in Waste Samples
Volatile Organic
Sampling Train
Sampling Method for Volatile
Organic Compounds
(SMVOC)
Sampling of Principal Organic
Hazardous Constituents from
Combustion Sources Using
Tedlar® Bags
Isokinetic HCI/CI2 Emission
Sampling Train
Midget Impinger HCI/CI,
Emission Sampling Train
SW-846
VOU
CHAP/
SEC
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
CURRENT
PROMUL-
GATED
METHOD
0010
RevO
(9/86)
0011
RevO
(12/96)
0020
RevO
(9/86)
0023A
Rev1
(12/96)
Not promul-
gated as part
of SW-846.
See40CFR
60. Appendix
A
Not promul-
gated as part
of SW-846.
See40CFR
60, Appendix
A
0030
RevO
(9/86)
0031
RevO
(12/96)
0040
RevO
(12/96)
0050
RevO
(12/96)
0051
RevO
(12/96)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
—
—
—
-
1010
1020
—
-
—
1110
—
1310
~*
RNAL
UP.)
(7/92)
™"
mm
—
-
—
1020 A
—
-
—
—
—
1310A
1311
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
"™
™~
—
-
—
—
—
-
—
~~
—
~~
RN. UP. Ill
(12/96)
IIIA(4/98)
0060
0061
0100
-
™
~
1030
-
—
••
1120
~~
DRAFT
UP.IVA
(1/98)
~™
~~
—
-
••
—
~
-
—
"•
—
•"
DRAFT
UP. IVB
(11/00)
—
—
—
207-1
Referral
207-2
Referral
"~
—
—
1040
1050
•~
~
~~
METHOD TITLE
Determination of Metals in
Stack Emissions
Determination of Hexavalent
Chromium Emissions from
Stationary Sources
Sampling for Formaldehyde
and Other Carbonyl
Compounds in Indoor Air
Sampling Method for
Isocyanates
Analysis for Isocyanates by
High Performance Liquid
Chromatography (HPLC)
Pensky-Martens Closed-Cup
Method for Determining
Ignitability
Setafiash Closed-Cup
Method for Determining
Ignitability
Ignitability of Solids
Test Method for Oxidizing
Solids
Test Methods to Determine
Substances Likely to
Spontaneously Combust
Corrosivity Toward
Steel
Dermal Corrosion
Extraction Procedure (EP)
Toxicity Test Method and
Structural Integrity Test
Toxicity Characteristic
Leaching Procedure
SW-846
VOL/
CHAP/
SEC
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
Volll
Chap 10
VollC
Chap 8
Sec 81
VollC
Chap 8
Sec 81
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
VollC
Chap 8
Sec 8.2
VollC
Chap 6
VollC
Chap 8
Sec 8.4
VollC
ChapS
Sec 8.4
CURRENT
PROMUL-
GATED
METHOD
0060
RevO
(12/96)
0061
RevO
(12/96)
0100
RevO
(12/96)
Not Promul-
gated
Not Promul-
gated
1010
RevO
(9/86)
1020A
Rev1
(7/92)
1030
RevO
(12/96)
Not Promul-
gated
Not Promul-
gated
1110
RevO
(9/86)
1120
RevO
(12/96)
1310A
Rev1
(7/92)
1311
RevO
(7/92)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
1320
1330
3005
3010
~™
3020
3040
3050
mm
~"
FINAL
UP.I
(7/92)
"
"™
1330A
3005A
3010A
™"
3020A
"
3050A
"™
"~
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
1312
(Up. II)
"™
—
3015
(Up. II)
•
"
"
3051
(Up. II)
™~
RN. UP. Ill
(12/96)
IIIA(4/98)
"
™"
—
~~
3031
3040A
3050B
™~
3052
DRAFT
UP. IVA
(1/98)
"
— ~
—
301 5A
"
"
3051A
—
DRAFT
UP.IVB
(11/00)
™"
™"
—
~~
™—
~~
~~
•"
METHOD TITLE
Synthetic Precipitation
Leaching Procedure
Multiple Extraction
Procedure
Extraction Procedure for Oily
Wastes
Acid Digestion of Waters for
Total Recoverable or
Dissolved Metals for Analysis
by FLAA or ICP Spectroscopy
Acid Digestion of Aqueous
Samples and Extracts for
Total Metals for Analysis by
FLAA or ICP Spectroscopy
Microwave Assisted Acid
Digestion of Aqueous
Samples and Extracts
Acid Digestion of Aqueous
Samples and Extracts for
Total Metals for Analysis by
GFAA Spectroscopy
Acid Digestion of Oils for
Metals Analysis by Atomic
Absorption or ICP
Spectrometry
Dissolution Procedure for
Oils, Greases, or Waxes
Acid Digestion of Sediments,
Sludges, and Soils
Microwave Assisted Acid
Digestion of Sediments,
Sludges, Soils, and Oils
Microwave Assisted Acid
Digestion of Siliceous and
Organically Based Matrices
SW-846
VOU
CHAP/
SEC
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
VollA
Chap 3
Sec 3.2
CURRENT
PROMUL-
GATED
METHOD
1312
RevO
(9/94)
1320
RevO
(9/86)
1330A
Rev1
(7/92)
3005A
Rev1
(7/92)
3010A
Rev1
(7/92)
3015
RevO
(9/94)
3020A
Rev1
(7/92)
3031
RevO
(12/96)
3040A
Rev1
(12/96)
3050B
Rev 2
(12/96)
3051
RevO
(9/94)
3052
RevO
(12/96)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date m parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW
METHOD NUMBER
THIRD
ED.
(9/86)
[3060.
in the
2nd
Ed.]
3500
3510
3520
3540
—
~~
3550
™~
FINAL
UP. I
(7/92)
3500A
3510A
3520A
3540A
~
~~
""
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
—
3510B
(Up. II)
3520B
(Up. II)
3540B
(Up. II)
3541
(Up. II)
~~
3550A
(Up II)
™~
FIN. UP. Ill
(12/96)
IMA (4/98)
3060A
3500B
3510C
3520C
3535
3540C
™~
3542
3545
~~
3550B
3560
DRAFT
UP.IVA
(1/98)
—
•"
~~
3535A
—
—
3545A
~™
•"
DRAFT
UP.IVB
(11/00)
3500C
~~
—
3535A
(Replaces
IVA
version)
—
—
3545A
(Replaces
IVA
version)
3546
3550C
~~
METHOD TITLE
Alkaline Digestion for
Hexavalent Chromium
Organic Extraction and
Sample Preparation
Separatory Funnel Liquid-
Liquid Extraction
Continuous Liquid-Liquid
Extraction
Solid-Phase Extraction (SPE)
Soxhlet Extraction
Automated Soxhlet Extraction
Extraction of Semivolatile
Analytes Collected Using
Method 0010 (Modified
Method 5 Sampling Train)
Pressurized Fluid Extraction
(PFE)
Microwave Extraction
Ultrasonic Extraction
Supercritical Fluid Extraction
of Total Recoverable
Petroleum Hydrocarbons
SW-846
VOL/
CHAP/
SEC
VollA
Chap 3
Sec 3.2
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4 2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4 2.1
VollB
Chap 4
Sec
4.2.1
VollB
Chap 4
Sec 4 2.1
CURRENT
PROMUL-
GA7H>
METHOD
3060A
Rev1
(12/96)
3500B
Rev 2
(12/96)
3510C
Rev 3
(12/96)
3520C
Rev 3
(12/96)
3535
RevO
(12/96)
3540C
Rev 3
(12/96)
3541
RevO
(9/94)
3542
RevO
(12/96)
3545
RevO
(12/96)
Not Promul-
gated
3550B
Rev 2
(12/96)
3560
RevO
(12/96)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW
METHOD NUMBER
THIRD
ED.
(9/86)
3580
~~
3600
3610
3611
3620
3630
3640
3650
3660
FINAL
UP.)
(7/92)
3580A
~~
3600A
3610A
3611 A
3620A
3630A
"
3650A
3660A
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
"
—
3600B
(Up. II)
•"
—
3630B
(Up. II)
3640A
(Up. II)
"
"
3665
(Up. II)
RN. UP. Ill
(12/96)
IIIA(4/98)
3561
mm
3585
3600C
3610B
361 1B
3620B
3630C
"™
3650B
3660B
3665A
DRAFT
UP.IVA
(1/98)
3562
~~
—
—
—
—
~~
~~
~"
••
"
DRAFT
UP.IVB
(11/00)
~"
—
~
—
3620C
••
—
"•
"™
"
METHOD TITLE
Supercritical Fluid Extraction
of Polynuclear Aromatic
Hydrocarbons
Supercritical Fluid Extraction
of Polychlonnated Biphenyls
(PCBs) and Organochlorine
Pesticides
Waste Dilution
Waste Dilution for Volatile
Organics
Cleanup
Alumina Cleanup
Alumina Column Cleanup
and Separation of
Petroleum Wastes
Flonsil Cleanup
Silica Gel Cleanup
Gel-Permeation Cleanup
Acid-Base Partition Cleanup
Sulfur Cleanup
Sulfuric Acid/Permanganate
Cleanup
SW-846
VOU
CHAP/
SEC
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec
4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.2
VollB
Chap 4
Sec 4.2.2
VollB
Chap 4
Sec
4.2.2
VollB
Chap 4
Sec 4.2 2
VollB
Chap 4
Sec 4.2.2
VollB
Chap 4
Sec 4 2.2
VollB
Chap 4
Sec 4.2.2
VollB
Chap 4
Sec 4.2.2
VollB
Chap 4
Sec 4.2.2
CURRENT
PROMUL-
GATED
METHOD
3561
RevO
(12/96)
Not Promul-
gated
3580A
Rev1
(7/92)
3585
RevO
(12/96)
3600C
Rev 3
(12/96)
3610B
Rev 2
(12/96)
361 1B
Rev 2
(12/96)
3620B
Rev 2
(12/96)
3630C
Rev 3
(12/96)
3640A
Rev1
(9/94)
3650B
Rev 2
(12/96)
3660B
Rev 2
(12/96)
3665A
Rev1
(12/96)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
3810
™~
3820
—
~~
—
—
—
~~
~™
~ ~
—
~~
FINAL
UP. I
(7/92)
~~
"~
—
•"
—
—
—
~~
™~
~~
—
~~
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
— "
™
—
4010
(Up. MA)
—
-"
—
™"
"™
™~
—
~~
RN. UP. Ill
(12/96)
IDA (4/98)
~~
~~
4000
401 OA
4015
4020
4030
4035
4040
4041
4042
4050
DRAFT
UP.IVA
(1/98)
Noticed
for
removal
from
SW-846
~™
~~
—
~~
—
"
—
™"
™"
*™
—
™
DRAFT
UP.IVB
(11/00)
3815
"~
—
"~
—
—
™
~™
~~
~"
—
""
METHOD TITLE
Headspace
Screening Solid Samples for
Volatile Organics
Hexadecane Extraction and
Screening of Purgeable
Organics
Immunoassay
Screening for
Pentachlorophenol
by Immunoassay
Screening for 2,4-
Dichlorophenoxyacetic Acid by
Immunoassay
Screening for Polychlonnated
Biphenyls by Immunoassay
Soil Screening for Petroleum
Hydrocarbons by
Immunoassay
Soil Screening for Pol/nuclear
Aromatic Hydrocarbons by
Immunoassay
Soil Screening for Toxaphene
by Immunoassay
Soil Screening for Chlordane
by Immunoassay
Soil Screening for DDT by
Immunoassay
TNT Explosives in Soil by
Immunoassay
SW-846
VOL/
CHAP/
SEC
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
CURRENT
PROMUL-
GATED
METHOD
3810
RevO
(9/86)
Not Promul-
gated
3820
RevO
(9/86)
4000
RevO
(12/96)
401 OA
Rev1
(12/96)
4015
RevO
(12/96)
4020
RevO
(12/96)
4030
RevO
(12/96)
4035
RevO
(12/96)
4040
RevO
(12/96)
4041
RevO
(12/96)
4042
RevO
(12/96)
4050
RevO
(12/96)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note* The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
~~
~™
5030
™ "
5040
FINAL
UP.I
(7/92)
~~
~™
5030A
~™
RN.UP.
II (9/94)
IIA(8/93)
IIB(1/95)
"
~~
™~
"
~~
™~
"
5040A
(Up. II)
FIN. UP. Ill
(12/96)
IIIA(4/98)
4051
~™
~~
5000
5021
5030B
5031
5032
5035
Deleted
from
SW-846
DRAFT
UP. IVA
(1/98)
"
4500
4670
~™
•~
—
" ' ™
DRAFT
UP.IVB
(11/00)
™"
4425
—
"•
~™
™
—
~~
METHOD TITLE
Hexahydro-1 ,3,5-trinitro-1 ,3,5-
triazine (RDX) in Soil by
Immunoassay
Screening Extracts of
Environmental Samples for
Planar Organic Compounds
(PAHs.PCBs.PCDDs/PCDFs)
by a Reporter Gene on a
Human Cell Line
Mercury in Soil by
Immunoassay
Triazine Herbicides as
Atrazine in Water by
Quantitative Immunoassay
Sample Preparation for
Volatile Organic Compounds
Volatile Organic Compounds
in Soils and Other Solid
Matrices Using Equilibrium
Headspace Analysis
Purge-and-Trap for Aqueous
Samples
Volatile, Nonpurgeable,
Water-Soluble Compounds
by Azeotropic Distillation
Volatile Organic Compounds
by Vacuum Distillation
Closed-System Purge-and-
Trap and Extraction for
Volatile Organics in Soil and
Waste Samples
Analysis of Sorbent
Cartridges from Volatile
Organic Sampling Train
(VOST):GasChro-
matography/Mass
Spectrometry Technique
SW-846
VOU
CHAP/
SEC
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.4
VollA
Chap 3
Sec 3.3
VollB
Chap 4
Sec 4.4
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
VollB
Chap 4
Sec 4.2.1
Deleted
from
SW-846
CURRENT
PROMUL-
GATED
METHOD
4051
RevO
(12/96)
Not Promul-
gated
Not Promul-
gated
Not Promul-
gated
5000
RevO
(12/96)
5021
RevO
(12/96)
5030B
Rev 2
(12/96)
5031
RevO
(12/96)
5032
RevO
(12/96)
5035
RevO
(12/96)
Deleted
from
SW-846
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note* The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
™
6010
"™
"
"
7000
«
7020
7040
RNAL
UP.I
(7/92)
~~
6010A
™~
"
"
7000A
•"
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
5041
(Up. II)
5050
(Up. II)
—
6020
(Up. II)
"
mm
™
FIN. UP. Ill
(12/96)
IIIA(4/98)
5041A
"~
601 OB
~~
"
mm
"~
DRAFT
UP.IVA
(1/98)
~
—
6020A
6200
6500
6800
7000B
7010
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
DRAFT
UP. IVB
(11/00)
•~
601 OC
™~
"™
«
—
METHOD TITLE
Analysis for Desorption of
Sorbent Cartridges from
Volatile Organic Sampling
Train (VOST)
Bomb Preparation Method for
Solid Waste
Inductively Coupled Plasma-
Atomic Emission
Spectrometry
Inductively Coupled Plasma -
Mass Spectrometry
Field Portable X-Ray
Fluorescence Spectrometry
for the Determination of
Elemental Concentrations in
Soil and Sediment
Dissolved Inorganic Anions in
Aqueous Matrices by Capillary
Ion Electrophoresis
Elemental and Speciated
Isotope Dilution Mass
Spectrometry
7000A (Promulgated):
Atomic Absorption Methods
7000B (Draft):
Flame Atomic Absorption
Spectrophotometry
Graphite Furnace Atomic
Absorption
Spectrophotometry
Aluminum (Atomic
Absorption, Direct Aspiration)
Antimony (Atomic Absorption.
Direct Aspiration)
SW-846
VOL/
CHAP/
SEC
VollB
Chap 4
Sec 4.2.1
VdlC
ChapS
VollA
ChapS
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
CURRENT
PROMUL-
GATED
METHOD
5041A
Rev1
(12/96)
5050
RevO
(9/94)
6010B
Rev 2
(12/96)
6020
RevO
(9/94)
Not Promul-
gated
Not Promul-
gated
Not Promul-
gated
7000A
Rev1
(7/92)
Not Promul-
gated
7020
RevO
(9/86)
7040
RevO
(9/86)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
7041
7060
7061
—
™
7080
7090
7091
7130
RNAL
UP.I
(7/92)
7061A
~
•~
7081
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
7060A
(Up. II)
"
7062
(Up. II)
"~
7080A
(Up II)
FIN. UP. Ill
(12/96)
MIA (4/98)
—
—
7063
DRAFT
UP.PVA
(1/98)
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
—
—
—
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
DRAFT
UP.IVB
(11/00)
mm
—
—
METHOD TITLE
Antimony (Atomic Absorption.
Furnace Technique)
Arsenic {Atomic Absorption.
Furnace Technique)
Arsenic (Atomic Absorption,
Gaseous Hydride)
Antimony and Arsenic (Atomic
Absorption, Borohydride
Reduction)
Arsenic in Aqueous Samples
and Extracts by Anodic
Stripping Voltammetry (ASV)
Barium (Atomic Absorption,
Direct Aspiration)
Barium (Atomic Absorption,
Furnace Technique)
Beryllium (Atomic Absorption,
Direct Aspiration)
Beryllium (Atomic Absorption,
Furnace Technique)
Cadmium (Atomic Absorption,
Direct Aspiration)
SW-846
VOL/
CHAP/
SEC
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
CURRENT
PROMUL-
GATED
METHOD
7041
RevO
(9/86)
7060A
Rev1
(9/94)
7061A
Rev1
(7/92)
7062
RevO
(9/94)
7063
RevO
(12/96)
7080A
Rev1
(9/94)
7081
RevO
(7/92)
7090
RevO
(9/86)
7091
RevO
(9/86)
7130
RevO
(9/86)
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW
METHOD NUMBER
THIRD
ED.
(9/86)
7131
7140
7190
7191
7195
7196
7197
7198
7200
FINAL
UP. I
(7/92)
—
7196A
—
—
HN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
7131A
(Up. II)
—
—
—
—
RN. UP. Ill
(12/96)
MIA (4/98)
•
—
—
—
—
7199
DRAFT
UP.IVA
(1/98)
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
—
—
—
—
Noticed
for
removal
from
SW-846
DRAFT
UP.IVB
(11/00)
—
—
—
~
METHOD TITLE
Cadmium (Atomic Absorption,
Furnace Technique)
Calcium (Atomic Absorption.
Direct Aspiration)
Chromium (Atomic
Absorption, Direct Aspiration)
Chromium (Atomic
Absorption, Furnace
Technique)
Chromium, Hexavalent
(Coprecipitation)
Chromium, Hexavalent
(Colonmetric)
Chromium, Hexavalent
(Chelation/Extraction)
Chromium, Hexavalent
(Differential Pulse
Polarography)
Determination of Hexavalent
Chromium in Drinking Water,
Groundwater and Industrial
Wastewater Effluents by Ion
Chromatography
Cobalt (Atomic Absorption,
Direct Aspiration)
SW-846
VOL/
CHAP/
SEC
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
CURRENT
PROMUL-
GATED
METHOD
7131A
Rev1
(9/94)
7140
RevO
(9/86)
7190
RevO
(9/86)
7191
RevO
(9/86)
7195
RevO
(9/86)
7196A
Rev1
(7/92)
7197
RevO
(9/86)
7198
RevO
(9/86)
7199
RevO
(12/96)
7200
RevO
(9/86)
10
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
7201
7210
7380
7420
7421
7450
FINAL
UP. I
(7/92)
7211
7381
7430
RN. UP.
II (9/94)
NA(8/93)
IIB(1/95)
RN. UP. Ill
(12/96)
IIIA(4/98)
DRAFT
UP. IVA
(1/98)
Noticed
for
removal
fnom
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
DRAFT
UP.IVB
(11/00)
METHOD TITLE
Cobalt (Atomic Absorption.
furnace Technique)
Copper (Atomic Absorption,
Direct Aspiration)
Copper (Atomic Absorption,
Furnace Technique)
Iron (Atomic Absorption,
Direct Aspiration)
Iron (Atomic Absorption,
Furnace Technique)
Lead (Atomic Absorption,
Direct Aspiration)
Lead (Atomic Absorption,
Furnace Technique)
Lithium (Atomic Absorption,
Direct Aspiration)
ftfagnesium (Atomic
Absorption, Direct Aspiration)
SW-846
VOL/
CHAP/
SEC
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
CURRENT
PROMUL-
GATED
METHOD
7201
RevO
(9/86)
7210
RevO
(9/86)
7211
RevO
(7/92)
7380
RevO
(9/86)
7381
RevO
(7/92)
7420
RevO
(9/86)
7421
RevO
(9/86)
7430
RevO
(7/92)
7450
RevO
(9/86)
11
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW
METHOD NUMBER
THIRD
ED.
(9/86)
7460
7470
7471
—
••
7480
7481
7520
FINAL
UP. I
(7/92)
7461
~~
—
—
"•
FIN. UP.
II (9/94)
IIA(8/93)
IIBJ1/95)
7470A
(Up. II)
7471A
(Up. II)
—
~~
FIN. UP. Ill
(12/96)
MIA (4/98)
—
—
7472
™~
DRAFT
UP. IVA
(1/98)
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
~~
7471 B
—
7473
7474
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
DRAFT
UP. IVB
(11/00)
~™
—
—
— ~
METHOD TITLE
Manganese (Atomic
Absorption, Direct Aspiration)
Manganese (Atomic
Absorption, Furnace
Technique)
Mercury in Liquid Waste
(Manual Cold-Vapor
Technique)
Mercury in Solid or Semisolid
Waste (Manual Cold-Vapor
Technique)
Mercury in Aqueous Samples
and Extracts by Anodic
Stripping Voltammetry (ASV)
Mercury in Solids and
Solutions by Thermal
Decomposition,
Amalgamation, and Atomic
Absorption
Spectrophotometry
Mercury in Sediment and
Tissue Samples by Atomic
Fluorescence Spectrometry
Molybdenum (Atomic
Absorption, Direct Aspiration)
Molybdenum (Atomic
Absorption, Furnace
Technique)
Nickel (Atomic Absorption,
Direct Aspiration)
SW-846
VOL/
CHAP/
SEC
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
oGC O.O
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3 3
CURRENT
PROMUL-
GATED
METHOD
7460
RevO
(9/86)
7461
RevO
(7/92)
7470A
Rev1
(9/94)
7471A
Rev1
(9/94)
7472
RevO
(12/96)
Not Promul-
gated
Not Promul-
gated
7480
RevO
(9/86)
7481
RevO
(9/86)
7520
RevO
(9/86)
12
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW
METHOD NUMBER
THIRD
ED.
(9/86)
7550
—
7610
7740
7741
mm
7760
7770
FINAL
UP. I
(7/92)
—
~™
mm
7760A
7761
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
—
7741 A
(Up. II)
7742
(Up. II)
RN. UP. Ill
(12/96)
IIIA(4/98)
7521
7580
* ~
~~
DRAFT
UP.IVA
(1/98)
Noticed
for
removal
from
SW-
846
Noticed
for
removal
from
SW-846
—
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
~—
~~
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
. DRAFT
UP. IVB
(11/00)
—
™"
™ ~
METHOD TITLE
Nickel (Atomic Absorption,
Furnace Method)
Osmium (Atomic Absorption.
Direct Aspiration)
White Phosphorus (P«) by
Solvent Extraction and Gas
Chromatography
Potassium (Atomic
Absorption, Direct Aspiration)
Selenium (Atomic Absorption,
Furnace Technique)
Selenium (Atomic Absorption,
Gaseous Hydride)
Selenium (Atomic Absorption,
Borohydride Reduction)
Silver (Atomic Absorption,
Direct Aspiration)
Silver (Atomic Absorption,
Furnace Technique)
Sodium (Atomic Absorption,
Direct Aspiration)
SW-846
VOU
CHAP/
SEC
VollA
Chap 3
Sec 3.3
VollA
Chap 3
oGC »5.O
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
CURRENT
PROMUL-
GATED
METHOD
7521
RevO
(12/96)
7550
RevO
(9/86)
7580
RevO
(12/96)
7610
RevO
(9/86)
7740
RevO
(9/86)
7741A
Rev1
(9/94)
7742
RevO
(9/94)
7760A
Revl
(7/92)
7761
RevO
(7/92)
7770
RevO
(9/86)
13
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand comer of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
7840
7841
7870
7910
7911
7950
8000
FINAL
UP. I
(7/92)
7780
7951
8000A
FIN. UP.
II (9/94)
IIA(8/93)
118(1/95)
™"
FIN. UP. Ill
(12/96)
IMA (4/98)
8000B
DRAFT
UP.IVA
(1/98)
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
Noticed
for
removal
from
SW-846
~~
DRAFT
UP.IVB
(11/00)
—
METHOD TITLE
Strontium (Atomic Absorption,
Direct Aspiration)
Thallium (Atomic Absorption,
Direct Aspiration)
Thallium (Atomic Absorption,
Furnace Technique)
Tin (Atomic Absorption, Direct
Aspiration)
Vanadium (Atomic
Absorption, Direct Aspiration)
Vanadium (Atomic
Absorption, Furnace
Technique)
Zinc (Atomic Absorption,
Direct Aspiration)
Zinc (Atomic Absorption,
Furnace Technique)
Determinative
Chromatographic
Separations
SW-846
VOU
CHAP/
SEC
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollA
Chap 3
oGC o O
VollA
Chap 3
Sec 3 3
VollA
Chap 3
Sec 3 3
VollA
Chap 3
o6C o.o
VollB
Chap 4
Sec 4 3.1
CURRENT
PROMUL-
GATH>
METHOD
7780
RevO
(7/92)
7840
RevO
(9/86)
7841
RevO
(9/86)
7870
RevO
(9/86)
7910
RevO
(9/86)
7911
RevO
(9/86)
7950
RevO
(9/86)
7951
RevO
(7/92)
8000B
Rev 2
(12/96)
14
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
8010
8015
8020
8030
—
~™
8040
—
8060
FINAL
UP.I
(7/92)
8010A
8011
801 5A
™~
8021
8030A
—
"~
8040A
~~
™~
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
8010B
(Up. II)
"•
8020A
(Up. II)
8021A
(Up. II)
—
8031
(Up. II)
8032
(Up. II)
~~
~~
™~
FIN. UP. Ill
(12/96)
IMA (4/98)
Deleted
from
SW-846
8015B
Deleted
from
SW-846
8021 B
Deleted
from
SW-846
—
8032A
8033
Deleted
from
SW-846
8041
Deleted
from
SW-846
DRAFT
UP.IVA
(1/98)
"™
—
—
~"
—
™
~~
™
~"
DRAFT
UP.IVB
(11/00)
~™
801 5C
—
—
—
~~
—
8041 A
~~
METHOD TITLE
Halogenated Volatile
Organics by Gas
Chromatography
1 ,2-Dibromoethane and 1 ,2-
Dibromo-3-chloropropane by
Microextraction and Gas
Chromatography
Nonhalogenated Organics
Using GC/FID
Aromatic Volatile Organics by
Gas Chromatography
Aromatic and Halogenated
Volatiles by Gas
Chromatography Using
Photoionization and/or
Electrolytic Conductivity
Detectors
Acrolein and Acrylonitn'le by
Gas Chromatography
Acrylonitnle by Gas
Chromatography
Acrylamide by Gas
Chromatography
Acetonitnle by Gas
Chromatography with
Nitrogen-Phosphorus
Detection
Phenols by Gas
Chromatography
Phenols by Gas
Chromatography
Phthalate Esters
SW-846
VOL/
CHAP/
SEC
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
CURRENT
PROMUL-
GATED
METHOD
Deleted
from
SW-846
8011
RevO
(7/92)
801 SB
Rev 2
(12/96)
Deleted
from
SW-846
8021 B
Rev 2
(12/96)
Deleted
from
SW-846
8031
RevO
(9/94)
8032A
Rev1
(12/96)
8033
RevO
(12/96)
Deleted
from
SW-846
8041
RevO
(12/96)
Deleted
from
SW-846
15
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
~~
8080
8090
™ ™
""
8100
FINAL
UP. I
(7/92)
8070
—
™
™
"
8110
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
8061
(Up. II)
~~
8080A
(Up. II)
8081
(Up. II)
—
~~
~~
"
FIN. UP. Ill
(12/96)
IIIA(4/98)
8061A
8070A
Deleted
from
SW-846
8081 A
8082
Deleted
from
SW-846
8091
~~
"
Deleted
from
SW-846
8111
DRAFT
UP. IVA
(1/98)
™
8081 B
8082A
—
••
—
"
"
"
DRAFT
UP. IVB
(11/00)
•"
8081 B
(Replaces
IVA
version)
8082A
(Replaces
IVA
version)
8085
—
—
8095
™~
™"
~~
METHOD TITLE
Phthalate Esters by Gas
Chromatography with
Electron Capture Detection
(GC/ECD)
Nitrosamines by Gas
Chromatography
Organochlorine Pesticides
and Polychlorinated
Biphenyls by Gas
Chromatography
Organochlorine Pesticides by
Gas Chromatography
Polychlorinated Biphenyls
(PCBs) by Gas
Chromatography
Compound-independent
Elemental Quantitation of
Pesticides by Gas
Chromatography with Atomic
Emission Detection (GC/AED)
Nitroaromatics and Cyclic
Ketones
Nitroaromatics and Cyclic
Ketones by Gas
Chromatography
Explosives by Gas
Chromatography
Polynuclear Aromatic
Hydrocarbons
Haloethers by Gas
Chromatography
Haloethers by Gas
Chromatography
SW-846
VOU
CHAP/
SEC
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.31
Deleted
from
SW-846
VollB
Chap 4
Sec 4.31
VollB
Chap 4
Sec431
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
CURRENT
PROMUL-
GATED
METHOD
8061A
Rev1
(12/96)
8070A
Rev1
(12/96)
Deleted
from
SW-846
8081 A
Rev1
(12/96)
8082
RevO
(12/96)
Not Promul-
gated
Deleted
from
SW-846
8091
RevO
(12/96)
Not Promul-
gated
8100
RevO
(9/86)
Deleted
from
SW-846
8111
RevO
(12/96)
16
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note. The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
8120
~~
—
8140
8150
8240
8250
RNAL
UP.I
(7/92)
— ™
~™
—
~~
8141
8150A
8240A
8260
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
8120A
(Up. II)
8121
(Up. II)
—
•""
8141A
(Up. II)
81 SOB
(Up. II)
8151
(Up. II)
8240B
(Up. II)
8250A
(Up. II)
8260A
(Up. II)
RN. UP. Ill
(12/96)
IIIA (4/98)
Deleted
from
SW-846
~™
8131
Deleted
from
SW-846
Deleted
from
SW-846
8151A
Deleted
from
SW-846
Deleted
from
SW-846
8260B
DRAFT
UP.IVA
(1/98)
™"
~~
—
~"
8141B
mm
DRAFT
UP. IVB
(11/00)
~™
"•
—
—
8141B
(Replaces
IVA
version)
"™
METHOD TITLE
Chlorinated Hydrocarbons by
Gas Chromatography
Chlorinated Hydrocarbons by
Gas Chromatography:
Capi'flary Column Technique
Aniline and Selected
Derivatives by Gas
Chromatography
Organophosphorus
Pesticides
8141 A (Promulgated):
Organophosphorus
Compounds by Gas
Chromatography: Capillary
Column Technique
8141 B (Draft):
Organophosphorus
Compounds by Gas
Chromatography
Chlorinated Herbicides by
Gas Chromatography
Chlorinated Herbicides by GC
Using Methylation or
Pentafluorobenzylation
Denvatization
Volatile Organic Compounds
by Gas
Chromatography/Mass
Spectrometry (GC/MS)
Semivolatile Organic
Compounds by Gas
Chromatography/Mass
Spectrometry (GC/MS)
Volatile Organic Compounds
by Gas
Chromatography/Mass
Spectrometry (GC/MS)
SW-846
VOU
CHAP/
SEC
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.1
Deleted
from
SW-846
Deleted
from
SW-846
VollB
Chap 4
Sec 4.3.2
CURRENT
PROMUL-
GATED
METHOD
Deleted
from
SW-846
8121
RevO
(9/94)
8131
RevO
(12/96)
Deleted
from
SW-846
8141A
Rev1
(9/94)
Deleted
from
SW-846
8151A
Rev1
(12/96)
Deleted
from
SW-846
Deleted
from
SW-846
8260B
Rev 2
(12/96)
17
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand comer of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
—
8270
—
8280
_
8310
FINAL
UP.)
(7/92)
—
8270A
—
_
_
—
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
—
8270B
(Up II)
8275
(Up. II)
..
8290
(Up. II)
—
RN. UP. Ill
(12/96)
MIA (4/98)
—
8270C
8275A
8280A
..
—
DRAFT
UP.FVA
(1/98)
—
8270D
—
8280B
8290A
—
DRAFT
UP.IVB
(11/00)
8261
_
—
_
_
_
METHOD TITLE
Volatile Organic Compounds
by Vacuum Distillation in
Combination with Gas
Chromatography/Mass
Spectrometry (VD/GC/MS)
Semivolatile Organic
Compounds by Gas
Chromatography/Mass
Spectrometry (GC/MS)
Semivolatile Organic
Compounds (PAHs and
PCBs) in Soils/Sludges and
Solid Wastes Using Thermal
Extraction/Gas Chromatogra-
phy/Mass Spectrometry
(TE/GC/MS)
8280A (Promulgated):
The Analysis of
Polychlonnated Dibenzo-p-
Dioxms and Polychlorinated
Dibenzofurans by High
Resolution Gas
Chromatography/Low
Resolution Mass
Spectrometry (HRGC/LRMS)
8280B (Draft):
Polychlorinated Dibenzo-p-
Dioxins and Polychlorinated
Dibenzofurans by High
Resolution Gas
Chromatography/Low
Resolution Mass
Spectrometry (HRGC/LRMS)
Polychlorinated
Dibenzodioxins (PCDDs) and
Polychlonnated
Dibenzofurans (PCDFs) by
High-Resolution Gas
Chromatography/
High-Resolution Mass
Spectrometry (HRGC/HRMS)
Polynuclear Aromatic
Hydrocarbons
SW-846
VOL/
CHAP/
SEC
VollB
Chap 4
Sec 4 3.2
VollB
Chap 4
Sec 4.3.2
VollB
Chap 4
Sec 4.3 2
VollB
Chap 4
Sec 4.3 2
VollB
Chap 4
Sec 4.3.2
VollB
Chap 4
Sec 4.3.3
CURRENT
PROMUL-
GATED
METHOD
Not Promul-
gated
8270C
Rev 3
(12/96)
8275A
Rev1
(12/96)
8280A
Rev1
(12/96)
8290
RevO
(9/94)
8310
RevO
(9/86)
18
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
—
—
—
FINAL
UP.I
(7/92)
—
—
—
RN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
8315
(Up. II)
8316
(Up. II)
8318
(Up. II)
8321
(Up. II)
8330
(Up. II)
8331
(Up. II)
—
8410
(Up. II)
FIN. UP. W
(12/96)
MIA (4/98)
831 5A
~~
8321A
8325
—
8332
8430
DRAFT
UP.IVA
(1/98)
••
8321 B
8330A
—
—
DRAFT
UP.IVB
(11/00)
8318A
8321 B
(Replaces
IVA
version)
—
—
METHOD TITLE
Determination of Carbonyl
Compounds by High
Performance Liquid
Chromatography (HPLC)
Acrylamide, Acrylonitnle and
Acrolein by High Performance
Liquid Chromatography
(HPLC)
A/-Methylcarbamates by High
Performance Liquid
Chromatography (HPLC)
Solvent-Extractable
Nonvolatile Compounds by
High Performance Liquid
Chromatography/Thermo-
pray/Mass Spectrometry
(HPLC/TS/MS) or Ultraviolet
(UV) Detection
Solvent Extractable
Nonvolatile Compounds by
High Performance Liquid
Chromatography/Particle
Beam/Mass Spectrometry
(HPLC/PB/MS)
Nitroaromatics and
Nitramines by High
Performance Liquid
Chromatography (HPLC)
Tetrazene by Reverse Phase
High Performance Liquid
Chromatography (HPLC)
Nitroglycerine by High
Performance Liquid
Chromatography
Gas Chromatography/Fourier
Transform Infrared (GC/FT-IR)
Spectrometry for Semivolatile
Organics: Capillary Column
Analysis of Bis(2-chloroethyl)
Ether and Hydrolysis
Products by Direct Aqueous
Injection GC/FT-IR
SW-846
VOU
CHAP/
SEC
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.3
VollB
Chap 4
Sec 4.3.4
VollB
Chap 4
Sec 4.3.4
CURRENT
PROMUL-
GATED
METHOD
831 5A
Revl
(12/96)
8316
RevO
(9/94)
8318
RevO
(9/94)
8321A
Rev1
(12/96)
8325
RevO
(12/96)
8330
RevO
(9/94)
8331
RevO
(9/94)
8332
RevO
(12/96)
8410
RevO
(9/94)
8430
RevO
(12/96)
19
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom nght-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
"
mm
—
"•
™
mm
mm
9010
9012
"™
9020
HNAL
UP.)
(7/92)
™~
"™
—
™~
~~
~™
"™
9010A
~~
9013
9020A
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
™~
""
—
~™
~~
~~
"™
•"•
•"
~~
9020B
(Up. II)
RN. UP. Ill
(12/96)
IMA (4/98)
8440
~~
8515
8520
~~
"~
"™
901 OB
901 2A
"~
9014
"
DRAFT
UP.IVA
(1/98)
"™
••
—
—
—
~~
9000
9001
—
—
"•
™"
DRAFT
UP. IVB
(11/00)
~~
8510
— •
8535
8540
~~
—
—
—
~~
METHOD TITLE
Total Recoverable Petroleum
Hydrocarbons by Infrared
Spectrophotometry
Colorimetric Screening
Procedure for RDX and HMX
in Soil
Colorimetric Screening
Method for Trinitrotoluene
(TNT) in Soil
Continuous Measurement of
Formaldehyde in Ambient Air
Screening Procedure for Total
Volatile Organic Halides in
Water
Pentachlorophenol by UV-
induced Colorimetry
Determination of Water in
Waste Materials by Karl
Fischer Titration
Determination of Water in
Waste Materials by
Quantitative Calcium Hydride
Reaction
Total and Amenable Cyanide:
Distillation
Total and Amenable Cyanide
(Automated Colonmetric, with
Off-line Distillation)
Cyanide Extraction Procedure
for Solids and Oils
Titrimetric and Manual
Spectrophotometnc
Determinative Methods for
Cyanide
Total Organic Halides (TOX)
SW-846
VOL/
CHAP/
SEC
VollB
Chap 4
Sec 4.3.4
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.3.5
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.5
VollA
Chap 3
Sec 3.3
VollA
Chap 3
Sec 3.3
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
CURRENT
PROMUL-
GATED
METHOD
8440
RevO
(12/96)
Not Promul-
gated
8515
RevO
(12/96)
8520
RevO
(12/96)
Not Promul-
gated
Not Promul-
gated
Not Promul-
gated
Not Promul-
gated
9010B
Rev 2
(12/96)
901 2A
Rev1
(12/96)
9013
RevO
(7/92)
9014
Rev 0(12/96)
9020B
Rev 2
(9/94)
20
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
"
9022
~~
9030
™
•"
9035
9036
9038
9040
9041
9045
9050
FINAL
UP.I
(7/92)
9021
"™
—
9030A
9031
~~
™"
~™
"
9041A
9045A
"
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
~~
~~
—
mm
~~
~~
~~
~™
"
9040A
(Up. II)
9040B
(Up. IIB)
"
9045B
(Up. II)
9045C
(Up. IIB)
"
FIN. UP. Ill
(12/96)
IIIA(4/98)
~™
™~
9023
9030B
•"
9034
~~
™
~~
™~
9050A
DRAFT
UP.IVA
(1/98)
— ™
•"•
—
—
—
""
~~
—
™"
~™
mm
DRAFT
UP.IVB
(11/00)
™~
"~
—
—
—
~
••
—
~™
mm
~™
METHOD TITLE
Purgeable Organic Halides
(POX)
Total Organic Halides (TOX)
by Neutron Activation Analysis
Extractable Organic Halides
(EOX) in Solids
Acid-Soluble and Acid-
Insoluble Sulfides: Distillation
Extractable Sulfides
Titnmetric Procedure for Acid-
Soluble and Acid-Insoluble
Sulfides
Sulfate (Colorimetric,
Automated, Chloranilate)
Sulfate (Colorimetric.
Automated, Methylthymol
Blue, AA II)
Sulfate (Turbidimetnc)
pH Electrometric
Measurement
pH Paper Method
Soil and Waste pH
Specific Conductance
SW-846
VOU
CHAP/
SEC
VollC
Chap 5
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
CURRENT
PROMUL-
GATED
METHOD
9021
RevO
(7/92)
9022
RevO
(9/86)
9023
RevO
(12/96)
9030B
Rev 2
(12/96)
9031
RevO
(7/92)
9034
RevO
(12/96)
9035
RevO
(9/86)
9036
RevO
(9/86)
9038
RevO
(9/86)
9040B
Rev 2
1/95
9041A
Rev1
(7/92)
9045C
Rev 3
1/95
9050A
Rev1
(12/96)
21
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
~™
9060
9065
9066
9067
9070
(1664
refer-
ral)
FINAL
UP. I
(7/92)
~~
—
~~
~~
~~
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
9056
(Up. II)
—
™
~~
~~
FIN. UP. Ill
(12/96)
IIIA(4/98)
•~
9057
--
~~
~~
~~
Title and
text
replaced
with
referral to
Method
1664-
method no.
"9070"
remains at
top of
referral
page and
in table of
contents
(Up. MIA)
DRAFT
UP.IVA
(1/98)
—
—
~~
•"
"•
DRAFT
UP.IVB
(11/00)
9056A
9058 -
—
—
—
—
METHOD TITLE
Determination of Inorganic
Anions by Ion
Chromatography
Determination of Chloride
from HCI/CI2 Emission
Sampling Train (Methods
0050 and 0051 ) by Anion
Chromatography
Determination of Perchlorate
Using Ion Chromatography
with Chemical Suppression
Conductivity Detection
Total Organic Carbon
Phenolics
(Spectrophotometric, Manual
4-AAP with Distillation)
Phenolics (Colonmetnc,
Automated 4-AAP with
Distillation)
Phenolics
(Spectrophotometric, MBTH
with Distillation)
9070. title and text removed-
Total Recoverable Oil and
Grease (Gravimetric.
Separatory Funnel Extraction)
Method 9070 page and table
of contents entry under
Method 9070 refer reader to:
Method 1664: n-Hexane
Extractable Material (HEM; Oil
and Grease) and Silica Gel
Treated n-Hexane Extractable
Material (SGT-HEM; Non-
polar Material) by Extraction
and Gravimetry
SW-846
VOL/
CHAP/
SEC
VdlC
Chap 5
VollC
Chap 5
VdlC
ChapS
VollC
ChapS
VdlC
ChapS
VdlC
ChapS
VdlC
ChapS
VollC
Chap 5
CURRENT
PROMUL-
GATED
METHOD
9056
RevO
(9/94)
9057
RevO
(12/96)
Not Promul-
gated
9060
RevO
(9/86)
9065
RevO
(9/86)
9066
RevO
(9/86)
9067
RevO
(9/86)
The current
promulgated
version of
Method 1664
is Revision
A1
See 40 CFR
136.
Appendix A
1 Method 1664 Revision A (EPAPublication No. EPA-821-R-98-0021 is available via the Internet athttpV/wwww.epa oov/OST. It is also available
from the National Technical Information Service (NTIS), NTIS Publication No PB99-121949 (call 703-605-6000 or 800-553-6847).
22
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
9071
™"
"
9080
9081
9090
9095
FINAL
UP. I
(7/92)
~~
"
~™
"
9090A
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
9071A
(Up. II)
9075
(Up. II)
9076
(Up. II)
9077
(Up. II)
••
"™
™"
mm
9096
(Up. II)
FIN. UP. Ill
(12/96)
IIIA(4/98)
9071 B
(Up IDA)
9078
9079
~~
~~
"
9095A
DRAFT
UP.IVA
(1/98)
"™
9074
—
~~
—
••
"
™ ™
DRAFT
UP.IVB
(11/00)
~™
—
••
—
—
~~
™"
"
METHOD TITLE
n-Hexane Extractable Material
(HEM) for Sludge, Sediment,
and Solid Samples
Turbidimetric Screening
Method for Total Recoverable
Petroleum Hydrocarbons in
Soil
Test Method for Total Chlorine
in New and Used Petroleum
Products by X-Ray
Fluorescence Spectrometry
(XRF)
Test Method for Total Chlorine
in New and Used Petroleum
Products by Oxidative
Combustion and
Microcoulometry
Test Methods for Total
Chlorine in New and Used
Petroleum Products (Field
Test Kit Methods)
Screening Test Method for
Pol/chlorinated Biphenyls in
Soil
Screening Test Method for
Polychlorinated Biphenyls in
Transformer Oil
Cation-Exchange Capacity of
Soils (Ammonium Acetate)
Cation-Exchange Capacity of
Soils (Sodium Acetate)
Compatibility Test for Wastes
and Membrane Liners
Paint Filter Liquids Test
Liquid Release Test (LRT)
Procedure
SW-846
VOL/
CHAP/
SEC
VollC
Chap 5
VollB
Chap 4
Sec 4.5
VollC
ChapS
VollC
ChapS
VollC
ChapS
VollB
Chap 4
Sec 4.5
VollB
Chap 4
Sec 4.5
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
VollC
Chap 6
CURRENT
PROMUL-
GATED
METHOD
9071 B
Rev 2
(4/98)
Not Promul-
gated
9075
RevO
(9/94)
9076
RevO
(9/94)
9077
RevO
(9/94)
9078
RevO
(12/96)
9079
RevO
(12/96)
9080
RevO
(9/86)
9081
RevO
(9/86)
9090A
Rev1
(7/92)
9095A
Rev1
(12/96)
9096
RevO
(9/94)
23
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right-hand corner of the method The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
9100
9131
9132
9200
""
9250
FINAL
UP. I
(7/92)
~~
—
—
~™
~~
FIN. UP.
II (9/94)
IIA(8/93)
IIB(1/95)
—
—
—
~™
™"
FIN. UP. in
(12/96)
MIA (4/98)
—
—
Deleted
from
SW-846
9210
9211
9212
9213
9214
9215
"~
~~
DRAFT
UP.IVA
(1/98)
™
—
—
9216
"•
DRAFT
UP.IVB
(11/00)
—
—
—
9210A
—
—
METHOD TITLE
Saturated Hydraulic
Conductivity, Saturated
Leachate Conductivity, and
Intrinsic Permeability
Total Coliform: Multiple Tube
Fermentation Technique
Total Coliform: Membrane-
Filter Technique
Nitrate
Potentiometric Determination
of Nitrate in Aqueous
Samples with Ion-selective
Electrode
Potentiometric Determination
of Bromide in Aqueous
Samples with Ion-Selective
Electrode
Potentiometric Determination
of Chlonde in Aqueous
Samples with Ion-Selective
Electrode
Potentiometric Determination
of Cyanide in Aqueous
Samples and Distillates with
Ion-Selective Electrode
Potentiometric Determination
of Fluoride in Aqueous
Samples with Ion-Selective
Electrode
Potentiometric Determination
of Sulfide in Aqueous
Samples and Distillates with
Ion-Selective Electrode
Potentiometric Determination
of Nitrite in Aqueous Samples
with Ion-Selective Electrode
Chloride (Colorimetric,
Automated Ferricyanide AAI)
SW-846
VOU
CHAP/
SEC
VollC
Chap 6
VollC
Chap 5
VollC
Chap 5
Deleted
from
SW-846
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
VollC
Chap 5
CURRENT
PROMUL-
GATED
METHOD
9100
RevO
(9/86)
9131
RevO
(9/86)
9132
RevO
(9/86)
Deleted
from
SW-846
9210
RevO
(12/96)
9211
RevO
(12/96)
9212
RevO
(12/96)
9213
RevO
(12/96)
9214
RevO
(12/96)
9215
RevO
(12/96)
Not Promul-
gated
9250
RevO
(9/86)
24
-------
SW-846 METHOD STATUS TABLE November 2000 (continued)
Note1 The date in parentheses is the date found at the bottom right-hand corner of the method. The shaded rows indicate those methods
that were formally deleted from the manual and are no longer supported by OSW.
METHOD NUMBER
THIRD
ED.
(9/86)
9251
9252
—
9310
9315
9320
HCN
Test
Meth.
H2S
Test
Meth.
FINAL
UP.)
(7/92)
—
—
—
—
—
—
HCN
Test
Meth.
H2S
Test
Meth.
FIN. UP.
11(9/94)
IIA(8/93)
IIB(1/95)
"~
9252A
(Up. II)
9253
(Up. II)
—
—
—
HCN Test
Method
(Up. II)
H2S Test
Method
(Up. II)
FIN. UP. II)
(12/96)
IIIA(4/98)
•"
Deleted
from
SW-846
—
—
—
—
HCN Test
Method
H2S Test
Method
DRAFT
UP.IVA
(1/98)
~~
—
—
—
—
«
DRAFT
UP.IVB
(11/00)
"™
—
—
—
—
—
METHOD TITLE
Chloride (Colorimetric.
Automated Ferricyanide AAII)
Chloride (Trtrimetric. Mercuric
Nitrate)
Chloride (Titrimetric, Silver
Nitrate)
Gross Alpha and Gross Beta
Alpha-Emitting Radium
Isotopes
Radium-228
Test Method to Determine
Hydrogen Cyanide Released
from Wastes
Test Method to Determine
Hydrogen Sulfide Released
from Wastes
SW-846
VOL/
CHAP/
SEC
VollC
Chap 5
Deleted
from
SW-846
VollC
Chap 5
VollC
Chap 6
VollC
Chap 6
VollC
Chap 5
VollC
Chap 7
Sec
7.3.3.2
VollC
Chap 7
Sec
7.3.4.2
CURRENT
PROMUL-
GATED
METHOD
9251
RevO
(9/86)
Deleted
from
SW-846
9253
RevO
(9/94)
9310
RevO
(9/86)
9315
RevO
(9/86)
9320
RevO
(9/86)
Guidance
Method Only
Guidance
Method Only
25
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STATUS TABLE FOR SW-846 CHAPTER TEXT AND OTHER DOCUMENTS
November 2000
Note: The date in parentheses is the date found at the bottom right hand comer of the document. The check mark (/) indicates that the
material was revised in that update
TITLE
Disclaimer
Abstract
Table of Contents
Method Index and
Conversion Table
Preface and Overview
Acknowledgements
Chapter One
Quality Control
Chapter Two
Choosing the Correct
Procedure
Chapter Three
Inorganic Analytes
Chapter Four
Organic Analytes
Chapter Five
Miscellaneous Test
Methods
Chapter Six
Properties
Chapter Seven
Characteristics
Introduction and
Regulatory Definitions
THIRD
ED.
(9/86)
-
/
S
S
/
/
/
/
/
/
/•
/
/
FINAL
UP. 1
(7/92)
/
/
/
-
-
-
/
/
/
—
—
—
/
FIN. UP.
II (9/94)
IIA (8/93)
IIB (1/95)
-
S
(Up. II)
s
(Up. II
and IIB)
-
-
-
-
/
(Up. II)
/
(Up. II)
/
(Up. II)
/
(Up. II)
s
(Up. II
and IIB)
/
(Up. II)
FINAL
UP. Ill
(12/96)
UP. IMA
(4/98)
/
-
/
(Up. Ill
and MIA)
-
/
-
-
/
(Up. Ill)
/
(Up. Ill)
/
(Up. Ill)
/
(Up. Ill
and IIIA)
/
/
(Up. Ill)
DRAFT
UP. IVA
(1/98)
-
—
/
-
-
-
-
V
/
/
/
—
DRAFT
UP. IVB
(11/00)
-
-
/
(Replaces
IVA version)
-
-
-
-
/
(Replaces
IVA version)
/
(Replaces
IVA version)
S
(Replaces
IVA version)
/
(Replaces
IVA version)
•
SW-846
VOLUME
LOCATION
All Vols
All Vols
All Vols
All Vols
All Vols
VollA
All Vols
VollA
VollA
VollB
VollC
VollC
VollC
CURRENT
FINAL
VERSION
Rev1
(12/96)
Rev 2
(9/94)
Rev 5
(4/98)
RevO
(9/86)
Rev1
(12/96)
RevO
(9/86)
Rev1
(7/92)
Rev 3
(12/96)
Rev 3
(12/96)
Rev 3
(12/96)
Rev 3
(4/98)
Rev 3*
(12/96)
Rev 3
(12/96)
26
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STATUS TABLE FOR SW-846 CHAPTER TEXT AND OTHER DOCUMENTS
November 2000 (continued)
Note: The date in parentheses is the date found at the bottom right hand corner of the document. The check mark (/) indicates that the
material was revised in that update.
TITLE
Chapter Eight
Methods for
Determining
Characteristics
Chapter Nine
Sampling Plan
Chapter Ten
Sampling Methods
Chapter Eleven
Ground Water
Monitoring
Chapter Twelve
Land Treatment
Monitoring
Chapter Thirteen
Incineration
Appendix
Company References
THIRD
ED.
(9/86)
/
/
/
/
/
/
/
FINAL
UP. 1
(7/92)
-
-
—
—
-
-
FIN. UP.
II (9/94)
HA (8/93)
IIB (1/95)
/
(Up. II)
-
-
—
—
-
-
FINAL
UP. Ill
(12/96)
UP. IMA
(4/98)
/
(Up. Ill)
-
/
(Up. Ill)
—
—
-
-
DRAFT
UP. IVA
(1/98)
-
-
—
—
-
-
DRAFT
UP. IVB
(11/00)
^
-
/
-
-
-
-
SW-846
VOLUME
LOCATION
VollC
Volll
Volll
Volll
Volll
Volll
All Vols
CURRENT
FINAL
VERSION
Rev 2
(12/96)
RevO
(9/86)
Rev1*
(12/96)
RevO
(9/86)
RevO
(9/86)
RevO
(9/86)
RevO
(9/86)
•The published final versions of Chapter Six and Chapter Ten do not contain the correct revision number in the footer. The correct
revision numbers are reported in this table. The revision numbers for these chapters will be corrected with the next final chapter revision.
27
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