ANALYTICAL REPORT
U. S. ENVIRONMENTAL PROTECTION AGENCY
ORDER NO. I1783NBSX
-------
ANALYTICAL REPORT
U. S. ENVIRONMENTAL PROTECTION AGENCY
ORDER NO. I1783NBSX
REPORT DATE: APRIL 30, 1980
PREPARED BY: ENVIRONMENTAL RESEARCH GROUP
ANN ARBOR, MICHIGAN
BRIDGEVIEW, ILLINOIS
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
NOTE TO THE READER: You will find included in the analytical results,
levels of phthalates below the reliable detection
limits as discussed in Mr. Epstein's letter to
Dr. Sturino, found in the correspondence section
of this report. These values are given to indi-
cate analytical detection, but do not represent
accuracy levels beyond those discussed in that
correspondence.
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
U. S. ENVIRONMENTAL PROTECTION AGENCY
ANALYTICAL REPORT
April 30. 1980
THE FOLLOWING IS A REPORT ON THE ANALYSIS OF WATER, FISH, FISH FOOD, AND
SEDIMENT SAMPLES, COLLECTED UNDER THE DIRECTION OF THE U.S.E.P.A., REGION V,
AND DELIVERED TO ENVIRONMENTAL RESEARCH GROUP'S LABORATORY IN ANN ARBOR,
MICHIGAN, FOR ANALYSIS. AUTHORIZATION FOR THIS WORK IS IN ACCORDANCE WITH
THE PROVISIONS OF THE GENERAL SERVICES ADMINISTRATION, CONTRACT NO. GS-04S-
22913 AND WAS REQUISITIONED BY THE GREAT LAKES NATIONAL PROGRAMS OFFICE
UNDER ORDER NO. I1783NBSX.
INCLUDED IN THIS REPORT ARE A TABULAR SUMMARY OF ANALYTICAL DATA AND
QUALITY CONTROL STATISTICS, COPIES OF RECONSTRUCTED ION CHROMATOGRAMS FOR
ALL GC/MS SCANS, A DESCRIPTION OF THE ANALYTICAL METHODOLOGY, AND A COM-
MENTARY ON ANALYTICAL QUALITY CONTROL AND GENERAL OBSERVATIONS.
ALL SAMPLE PREPARATION, ANALYSIS, CALCULATIONS, AND REPORTING WAS DONE BY
ENVIRONMENTAL RESEARCH GROUP PERSONNEL.
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
PC
I
E.P.A. SAMPLE 0 LB35C22
ERG SAMPLE if 40335
MATRIX FISH
SAMPLE RECEIVED 10/29/79
r-o
\o
INORGANIC RESULTS
PARAMJS;TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported ±n
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
£P-N.£ENTRATI.ON
260
1900
240
3200
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
DATA: B46335 #1
CALI: CAL2FEB 13
188.0
RIC
82/97/88 19:85:88
SAMPLE: B48335
RANGE: G L 1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
846
SCANS
1 TO 1488
888
26:48
1888
33:28
1288
40:08
I486 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 9 LB 35C23
ERG SAMPLE ff 40336
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
Z MOISTURE
CONCENTRATION
Results reported in — unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
640
1400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
186.8
DATA: B48336 ftl
CALI: CAL138 tl
RIC
82/87/80 28:86:88
SAMPLE: B48336
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
883
SCANS 1 TO 1488
4512
200
6:40
400
13:28
26:48
1088
33:20
1280
40:00
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 35C24
ERG SAMPLE ti 40337
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
£ A.R A M ]i T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C.P-.NCENTRATION (PPB)
11000
13000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
180.0n
DATA: B4033? #1
CALI; CAL138 #1
RIC
92/87/80 21:06:00
SAMPLE: B40337
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
882
SCANS 1 TO 1408
5000
200
6:40
400
13:20
600
20:00
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE # LB 35C25
ERG SAMPLE // 40338
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAMETI5R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
— unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
280
2000
3400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
02/97/30 22:87:00
SAMPLE: B40333
RANGE: G 1,1408
LABEL: N li 4.0 QUAN: A 0,
DATA: B40338 ttl
CALI: CAL31JAN2 II
1.0 BASE: U 20, 3
835
883
SCANS
1 TO 1400
RIC
7544
200
6:40
400
13:28
26:40
1000
33:20
1280
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 35C26
MATRIX FISH
ERG SAMPLE # 40339
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMET_E_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL CC/MS SCAN
RATON (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
360
850
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
DATA: B40339 #1
CALI: CAL31JAN2
160.0-1
RIC
02/07/88 23:10:80
SAMPLE: B40339
RANGE: G L 1480 LABEL: N 1, 4.0 QIJAN: A 0, 1.0 BASE: U 20, 3
887
SCANS 1 TO 1409
5384
200
6:40
408
13:20
880
26:40
1088
33:28
1288
48:08
1
1480 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE it LB 36C01
ERG SAMPLE // 40340
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
ON (PPB)
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
3100
13000
16000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC DATA: B40340 ttl
02/08/80 9:27:00 CALI: CAL28 11
SAMPLE: B40340 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAH: A 9, 1.0 BASE: U 20, 3
SCANS 1 TO 1400
190.0-1
1125
73344
RIC
635
•63,
484 574
200
6:40
400
13:20
26:40
1000
33:20
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB36C02
MATRIX FISH
, ERG SAMPLE // 40341
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAMJiTE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(JPPB)
540
1200
2400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
02/99/80 12:15:00
SAMPLE: B40341 EPA FISH
RANGE: G 1,1400 LABEL: N
DATA: B40341 #1
CALI: CAL28 »1
1, 4.0 QUAN: A Q, 1.0 BASE: U 20, 3
SCANS 1 TO 1408
100.0-1
1136
10336
RIC
852
641
430
681
786
51
,578
\
200
6:40
I
400
13:20
903
ft [ M35
1365
600
20:00
26:40
1000
33:20
1208
40:06
I
1400 SCAN
46:46 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C03
ERG .SAMPLE // 40342
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL. HEXYL PHTHALATE
BASE NEUTRAL CC/MS SCAN
£°_NC_J:NTRAT:[ON
320
810
3600
OTHER COMPOUNDS
NONE
ENVIRONMENTAL. RESEARCH GROUP. INC.
-------
RIC
02/89/88 13:17:00
SAMPLE: B40342 EPA FISH
RANGE: G 1,1400 LABEL:
DATA:
CALI:
B48342 II
CAL28 tl
SCANS
1 TO 1480
N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
100.0-1
1138
13384
RIC
851
641
785
200
6:40
T"
406
13:20
490
-A.
578
LJ
903
K *!
660
20:00
26:40
"7
1000
33:20
1237
1290
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NUSX
K.L'.A. SAMPLIi // LB 36C04
; SAMI'LK // 40343
MATRIX FISH
SAMIM.I-: KKCKIVKl)
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,2,4 TRICHLOROBENZENE
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
. BASE NEUTRAL GC/MS SCAN
C_ 0 N C E N T R A T! 1. 0 N
70
2200
360
2200
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100. 0-1
RIC
92/08/88 18:36:88
SAMPLE: 640343 EPA FISH
RANGE:'G 1,1409 LABEL: N 1, 4.0 QUAN: A 0. 1.0 BASE: U 20; 3
DATA: B40343 ftl
CALI: CAL28 #1
SCANS
1 TO 1468
1133
14496
288
6:40
488
13:20
688
28:08
26:48
1088
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 36C05
ERG SAMPLE // 40344
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAME^TER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OM_P()y_ND
HEXACHLOROBENZENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
0 N_ C E N T R A T _! 0 N (PPB)
1100
1100
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
DATA: B48344 tl
CALI: CAL28 #1
180.0-n
RIC
82/08/80 17:47:00
SAMPLE: B40344 EPA FISH
RANGE: G 1/1400 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
641
SCANS 1 TO 1400
4600
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB36C06
ERG SAMPLE // 40345A
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
£. A R A M E T_ E^ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
_unless otherwise noted.
BASE NEUTRAL GC/MS SCAN
220
2300
OTHER COMPOUNDS
NONE
SEE DUPLICATE ON NEXT PAGE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/98/88 16:41:88
SAMPLE: B46345A EF
RANGE: G 1,1488
* FISH
LABEL: N
4.8 QUAN: A
160.
DATA: MBA* fl
CALI: CAL28 tl
8, 1.8 BASE: U 29, 3
853
SCANS 1 TO 1488
RIC
5264
26:48
1888
33:28
1288
40:88
1468 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C06
MATRIX
ERG SAMPLE // 40345B
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAMETE_El
ARSENIC
CADMIUM
COBALT
COPPER .
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
NAPHTHALENE
HEXACHLOROBENZENE
ETHYL HEXYL PHTHALATE
410
110
3100
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
188.8-1
DATA: B48345B tl
CALI: CAL32898FEB *2
RIC
82/88/88 15:39:88
SAMPLE: B48345B EPA FISH
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
64?
SCANS 1 TO 1488
14968
1171
26:48
1888
33:28
1200
48:80
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 36C07
ERG SAMPLE # 40346
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMETER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
NAPHTHALENE
ETHYL HEXYL PHTHALATE
470
3300
OTHER COMPOUNDS
PCB's (PENTA)
<.01 (TRACE)
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/08/88 13:17:09
SAMPLE: B48346 EPA FISH
RANGE: G 1,1406 LABEL:
DATA: B49346 II
CALI: CAL32008FEB »2
N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
SCANS 1 TO 1400
100.0-1
181760
RIC
1156
603
'"•,69 ..,*„• 221
488
i
200
6:40
690
600
20:00
,858
1 L
JL fl
1
800
26:40
! i 962
1000 1200
33:20 40:00
1310
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C08
ERG SAMPLE # 40347
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
N C
N
200
2800
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/08/80 13:44:00
SAMPLE: B40347 EPA FISH
RANGE: G 1,1400 LABEL: N
1, 4.0 QUAN: A
100.0-1
DATA: B40347 #1
CALI: CAL28 #1
0, 1.0 BASE: U 20, 3
851
SCANS 1 TO 1400
8592
1141
RIC
400
13:20
600
20:00
26:48
1000
33:20
1200
40:00
1406 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C09
ERG SAMPLE // 40348
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ A R A M IS T .E R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£OMP_OUND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C_C1.!1C_E_N.TR_ATI_ONI (PPB)
9700
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
186.0
UHIH: tHWj48 *i
82/88/30 12:63:88 CALI: CAL32888FEB #2
SAMPLE: B40348 EPA FISH
RANGE: G 1/1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
631
8448
1148
26:48
1888
33:28
1288
48:86
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C1Q
ERG SAMPLE // 40349
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
:PARAM_ETE:R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
70
1700
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.0-1
RIC
RIC DATA: B40349 tl
02/88/80 11:44:00 CALI: CAL28 II
SAMPLE: B40349 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
637
SCANS 1 TO 1400
7072
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 36C11
ERG SAMPLE // 40350
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAM_ETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
260
1900
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
188.8n
RIC
DATA: B40350 #1
82/08/80 18:58:90 CALI: CAL28 #1
SAMPLE: 648350 EPA FISH
RANGE: G 1,1480 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
3oo
SCANS 1 TO 1400
5488
409
13:20
600
20:00
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C12
ERG SAMPLE // 40351A
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P A R A M E
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in — unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
580
18000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/08/30 12:43:98
SAMPLE: B40351 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.0
100.8-1
QUAN:
639
DATA: B40351 *1
CALI: CAL23 #1
A 0, 1.0 BASE: U 20, 3
SCANS 1 TO 1400
902
1143
5329
200
6:40
400
13:20
26:40
1000
33:20
1200
40:00
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 36C12
ERG SAMPLE ff 40351B
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C:()M_P()L[1ND
DIBUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
EHTYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
E ^J T R A T I 0 N (PPB)
1900
12000
1100
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
92/13/88 9:23:98
SAMPLE: B40351 EPA FISH
RANGE: C 1,1488 LABEL: N
\, 4.0 QUAN: A 8,
DATA: B48351 il
CALI: CAL213 13
U 28, 3
SCANS 1 TO 1488
180.8-1
RIC
795
.686
.44
35968
916
'1075
208
6:40
488
13:28
680
20:08
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIKE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C13
liRG SAMPLE //
40352
MATRIX FISH
' SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in — unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C 0 M P 0 U N D
NAPHTHALENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
IJ (PPB)
140
790
OTHER COMPOUNDS
PENTACHLOROBENZENE .
<.01 (TRACE)
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.0H
02/98/80 14:17:09
SAMPLE: 84*352 EPA FISH
RANGE: G 1,1409 LABEL: N
DATA: B49352 #1
CALI: CAL32008FEB #2
1, 4.9 QUAN: A 0, 1.0 BASE: U 20, 3
SCANS 1 TO 1400
1137
14496
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB36C14
ERG SAMPLE // 40353
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
^ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
NAPHTHALENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
°_ 0 N C K N T R A T J, 0 N (PPB)
1400
19300
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/68/86 16:53:66
SAMPLE: B46353 EPA FISH
RANGE: G 1,1466 LABEL: N
166.6-1
UHiA: B40353 wi
CALI: CAL32668FEB #2
4.6 QUAN: A 6, 1.6 BASE: U 26, 3
639
857
iuANS 1 'iu i486
661
RIC
3868
1176
26:48
1666
33:26
1266
46:68
1466
46:46
SCAN
TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB36C15
ERG SAMPLE // 40354
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
CIOMPOU^I)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
200
2700
(PPB)
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.0-
RIC
RIC DATA: B49354 #1
02/89/88 14:19:90 CALI: CAL28 #1
SAMPLE: B40354 EPA FISH
RANGE: G 1,1400 LABEL: N I, 4.0 QUAN: A 8. 1.0 BASE: U 20, 3
853
SCANS 1 TO 1400
4120
200
6:40
600
20:08
26:40
1008
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 36C16
ERG SAMPLE 9 40355A
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P A R A M EJ T
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_ 0 M P_ () £ N D
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
160
2700
(PPB)
OTHER COMPOUNDS
NONE
SEE DUPLICATE ON NEXT PAGE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/99/80 15:20:80
SAMPLE: B40355A EPft FISH
RANGE: G 1,1490 LABEL:
DATA:
CALI:
B40355A f 1
CAL2FEB §3
buANS 1 iu 1406
N I/ 4.6 QUAN: A 8, 1.0
186.6-1
BASE: U 20,
987
373G
1600
33:20
1280
48:00
1400 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 36C16
ERG SAMPLE // 40355B
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_AlRAMjiT_ER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
— unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
280
1300
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIG
82/88/88 19:51:88
SAMPLE: B48355B EF
RANGE: G 1,1488
* FISH
LABEL: N
1, 4.8
188.8n
QUAN: A
643
DATA: B483S5B #1
CALI: CAL28 «1
8, 1.8 BASE: U 28, 3
SCANS 1 TO 1489
3928
1348
288
6:46
26:48
1888
33:28
1288
46:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX -
E.P.A. SAMPLE // LB36C17
ERG SAMPLE # 40356
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.A.RAME.TE.RL
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
— unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
EHTYL HEXYL PHTHALATE
90
420
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
180.8-1
DrtTrt: 840356 #1
CALI: CAL28 #1
RIC
92/88/80 28:52:90
SAMPLE: B40356 EPA FISH
RANGE: G 1.1480 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
823
SCANS
1 TO 1400
6624
26:40
1000
33:20
1200
40:00
1400 5CAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE # LB36C18
ERG SAMPLE 9 40357
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAME_;TER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
-------
188.0-1
DATA: B40357 II
82/08/88 21:54:08 CALI: CAL28 ttl
SAMPLE: B40357 EPA FISH
RANGE: G 1,1498 LABEL: N 1, 4.9 QUAN: A 8, 1.8 BASE: U 28, 3
645 969
SCANS 1 TO 1486
PIC-
3552
280
6:40
408
13:20
26:40
1000
33:20
1280
46:08
1409 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 36C19
ERG SAMPLE // 40358
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P. A R. A M _E 1- Ji
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
7, MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
300
430
1200
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
18U.
DATA: 64Q358 «1
CALI: CAL28 #1
RIC
02/08x'88 22:57:98
SAMPLE: B40358 EPA FISH
RANGE: G 1/1400 LABEL: N 1, 4.0 GRJAN: A 0, 1.0 BASE: U 20, 3
909
SCANS 1 TO 1488
3668
26:48
ieee
33:20
1208
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 9 LB36C20
ERG SAMPLE // 40359
MATRIX FISH
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAM_ET_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
1700
4400
(PPB)
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
92/89/89 16:26:90
SAMPLE: B48359 EPA FISH
RANGE: G 1,1468 LABEL:
DATA:
CALI:
B40353
CAL2FEB
SCANS 1 TO 1468
§3
N 1. 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
100.0-,
1148
RIC
644
498
II
I
288
6:48
488
13:28
680
20:88
26:48
1888
33:28
19360
1288
40:08
1408 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE
ERG SAMPLE ft
LB 37C02
40360
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAM_EJ:JSR
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
1.9 Ug/1
<.003
<.005
.006
<.005
<.010
<.0002
<1.0 vg/1
<.08
.007
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
.COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
<5
<5
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
81/21/88 18:27:86
SAMPLE: B48368, 3 UL + 1 UL IS
RANGE: G 1,1489 LABEL: N 1,
582
DAm: B4Bc!b0 il
CALI: CAL121B #1
4.8 QUAN: A 8, 1.8 BASE: U 28, 3
SCflNS 1 TO
18848
13,57
888
26:48
1088
33:28
1288
48:83
1488 SCAN
46:49 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE t LB37C03 MATRIX WATER
ERG SAMPLE if 40361 SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER CONCENTRATIOI^
ARSENIC <.5 yg/1
CADMIUM <.003
COBALT <*005
COPPER <.005
CHROMIUM <.005
LEAD <.010
MERCURY <.0002
SELENIUM <1 o pg/1
TIN <.08
ZINC <.005
% MOISTURE —
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
____H__Ji _______J^A^i5.^i (PPB)
ETHYL HEXYL.PHTHALATE <5.
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.8-1
RIC
01/21/88 19:34:08
SAMPLE: B40361, 3 UL + 1 UL IS
RANGE: G 1,1486 LABEL: N 1,
505
DATA: B40361 #1
CALI: CAL121B »1
4.0 QUAN: A 0, 1.8 BASE: U 20, 3
SCANS 1 TO 1490
RIC
16928
867
26:40
1008
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 37C04
ERG SAMPLE // 40362
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
j> A _R A M j£ T J£ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
1.3 yg/1
<.003
C.005
.005
<.005
<.010
<.0002
1.7 yg/1
<.08
.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
.C 0 M _P 0 IJ N D
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
22.
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100. 0-1
RIC
81/21/80 20:40:09
SAMPLE: B49362, 3 UL + 1 UL IS
RANGE: G 1,1489 LABEL: N 1, 4.0
504
DATA: B40362 f1
CALI: CAL121B «1
QUAN: A 0, 1.0 BASE: U 20, 3
SCANb
1 lU 1400
15088
13:20
686
20:00
26:48
1000
33:20
1208
40:00
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 37C05
ERG SAMPLE # 40363
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ A R A M E_ T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
1.3
<.003
<. 005
.005
<.005
<.010
.0005
<1.0 jig/1
<-.08
.005
Results reported in mS/l unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£P_MP_OU__ND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
0^ (ppB)
<5
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/21/80 21:45:00
SAMPLE: B40363, 3 UL + 1 UL
RANGE: G 1,1408 LABEL: N
IS
109.0
506
DATA: B40363 #1
CALI: CAL121B «1
4.0 QUAN: A 0, 1.0 BASE: U 20, 3
SCANS 1 TO I486
RIC
16992
200
6:40
400
13:20
26:40
1208
40:08
1469 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 37C06
ERG SAMPLE # 40364
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
£ARAMET_E_R
ARSENIC
CADMIUM
• COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 ug/1
<.003
<.005
<.005
< ,005
<.010
<.0002
1.1 Ug/1
<.08
.006
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
O^ (PPB)
<5
<5
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
81/21/89 22:48:88
SAMPLE: B48364, 3 UL + 1 UL IS
RANGE: G 1,1488 LABEL: N 1,
DATA: B40364 il
CALI: CAL121B il
4.0 QUAN: A 8, 1.8 BASE: U 28, 3
SCANS 1 TO 1408
100.0-
9136
RIC
26:40
1800
33:28
1286
46:88
1488 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE.# LB 37C07
ERG SAMPLE tf 40365
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<.5 ug/1
<.003
<.005
<.005
<.005
<.010
<.0002
<1.0 ug/1
<.08
.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
P.OMP.OU.ND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
11
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, tNC.
-------
RIC
81/22/80 8:45:88
SAMPLE: B40365: 3 UL SAMPLE,
RANGE: G 1,1488 LABEL: N
OAm:
CALI:
tl
CAL122
58 NG 018A
1, 4.8 QUAH:
A 8, 1.8 BASE: U 28, 3
188.
1314
RIC
559
I
782
1888
33:28
1208
48:08
1480 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE // LB37C08
ERG SAMPLE // A 03 66
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P. A R A M E: T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
c_0_NCJ£N.TRATJ.qN
.75 wg/1
<.003
<.005
.005
<.005
<.010
. 0005
<1.0 yg/1
<.08
<.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
10
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/22/89 9:48:09
SAMPLE: B48366: 3 UL SAMPLE,
RANGE: G ! 1400 LABEL: N
50 NG
1, 4.9
DATA:
CALI:
B48366 #1
CAL122 #1
SCANS 1 TO 1400
QUAN: A 8, 1.0 BASE: U 20, 3
100.8
RIC
2760
280
6:46
400
13:20
26:48
1000
33:20
1200
48:66
1400 SCAN
46:46 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX !
E.P.A. SAMPLE // LB37C09
ERG SAMPLE // 40367
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.56 yg/1
<.003
<.005
.005
<.005
<. 010
<.0002
<1.0 pg/1
<.08
.010
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£OMP_OL[_ND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
COlSC.ENTRATj.O^ (PPB)
<5
<5
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.0-
RIC
91/22/38 19:50:00
SAMPLE: B40367: 3 UL SAMPLE,
RANGE: G 1,1400 LABEL: N
56 NG D10A
1, 4.0 QLIAN:
DATA: B40367 #1
CALI: CAL122 *1
A 0, 1.0 BASE: U 20, 3
SCANS 1 TO 1400
3328
RIG
200
6:40
686
26:86
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE // LB 37C10
ERG SAMPLE 9 40368
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P. A R A M E T IE R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
C_ONCE_NTRATI_ON
.56 ug/1
<.003
<.005
.005
<.005
<.010
<.0002
1.7 ug/1
<.08
.008
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C.ONCE.N.TRATI.ON (PPB)
<5
<5
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/22/80 16:33:00
SAMPLE: B40368, 3 UL + 1 UL
RANGE: G 1,1400 LABEL: N
IS
4.0 QUAN: A 0,
100.0-1
DATA: B40368 #1
CALI: CAL122 #1
1.0 BASE: U 20, c
845
I
SCANS 1 TO 1400
5560
1357
400
13:20
600
20:00
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB37C11
ERG SAMPLE // 40369
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P A R A M E_ T_ E_
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
c_P__NC_j;_NTRATJ.O_N
1.1 Ug/1
<-003
<.005
.005
<.005
<.010
<.0002
<1.0 yg/1
<.08
<.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OM,POU_NI)
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
£°_NC__ENTRAT.ION
31
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
81/22/80 18:45:90
SAMPLE: B40369, 3 UL + 1 UL
RANGE: G 1,1400 LABEL: N
DATA:
CALI:
B40369 ft 1
CAL122 #1
SCANS 1 TU 1408
IS
1,
4.0 QUAH: A
100.0-1
0, 1.0
787
I
BASE: U 20, 3
9040
RIC
566
^^
200
6:40
420 505-
310- 5 -ft Ui
*1*^WyU-jv^vyn*
616
W^
835,
A JVIA
r
400
13:20
600
20:00
800
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE ff LB37C12
ERG SAMPLE It 403 7 OA
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
•56 ug/1
<.003
<.005
.005
<.005
<.010
<.0002
<.08
<.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
10
OTHER COMPOUNDS
NONE
SEE DUPLICATE ON FOLLOWING PAGE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/22/80 19:48:00
SAMPLE: B40370A, 3 UL + 1 UL IS
RANGE: G 1,1406 LABEL: N 1, 4.0
DATA: B40370A #1
CALI: CAL122 #1
QUAN: A 0, 1.8 BASE: U 20, 3
SCANS 1 TO 1400
190.8-1
RIC
3488
206
6:40
688
28:08
26:48
1088
33:28
1288
48:88
1408 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 37C12
ERG SAMPLE // 40370 B
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAMET_E;R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.56 jig/1
<.003
<.005
.005
<.005
<.010
<.0002
<1.0 ug/1
<.08
<.005
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
10
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/22/89 20:59:00
SAMPLE: B40370B, 3 UL + 1 UL IS
RANGE: G 1,1400 LABEL: N 1, 4.0
DATA:
CALI: CAL122 #1
QUAN: A 0, 1.0 BASE: U 20, 3
SCANb 1 IU
100.0
569
3980
200
6:40
600
20:00
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB37C13 MATRIX WATER
ERG SAMPLE // 40371 SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER CONCENTRATION*
ARSENIC 0002
SELENIUM <1 0 ue/1
™ <,08
ZINC .006
% MOISTURE
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
COM;POU_ND C.ON.C.JIN.IRALT^O^ CPPB)
DIBUTYL PHTHALATE <5
ETHYL HEXYL PHTHALATE ^
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.8-1
RIC
RIC
91/22/30 22:02:90
SAMPLE: B40371, 3 UL + 1 UL IS
RANGE: G 1,1409 LABEL: N 1,
4.0 QUAN: A
0, 1.0
787
DATA: B40371 #1
CALI: CAL122 #1
BASE: U 20, 3
566
585
421 I.-
720
615
A
834
tad
SCANS 1 TU 1408
5320
164$, ,.,„ 1206
608
28:08
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE # LB37C14 MATRIX WATER
ERG SAMPLE // 40372 SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
_PARAMETE_R . C_°_N.CE.N.T_RATJ:ON
ARSENIC <.5 yg/1
CADMIUM <.003
COBALT <.005
COPPER .005
CHROMIUM <.005
LEAD <.010
MERCURY <.0002
SELENIUM . <1.0 yg/1
TIN <.08
ZINC .006
% MOISTURE . —
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
C_£M£2_UbID c_21ic.E.liZRAlI.ON (PPB)
DIBUTYL PHTHALATE <5
ETHYL HEXYL PHTHALATE 15
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
108.0-1
DATA: B40372 #111
CALI: CAL122 #1
RIC
01/22/80 23:94:00
SAMPLE: B40372, 3 UL + 1 IJL IS
RANGE: G 1,1400 LABEL: N 1, 4.9 QUAN: A 0, 1.0 BASE: U 20, 3
786
SCANS 1 TO 1400
26:40
1006
33:28
4438
1288
40:08
1480 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 0 LB 37C15
ERG SAMPLE // 40373
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ A R. A M E_ T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.75 yg/1
<.003
<.005
.005
<.005
<-010
<.0002
<1.0 yg/1
<.08
.007
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C 0 M P 0 U N D
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
11
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
91/23/88 3:05:80
SAMPLE: B49373: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1406 LABEL: N 1, 4.8 QUAN:
UATA: B40373 *78?
CALI: CAL123 #1
A 0, 1.6 BASE: U 28, 3
SCRNb
l tu
100.0-1
1184
11200
488
13:28
688
28:88
26:48
33:28
1288
48:88
1408 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE // LB37C16
ERG SAMPLE //
MATRIX WATER
40374
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
1.7 ug/1
<.003
<.005
.005
<.005
<.0002
<1.0 yg/1
<.08
.009
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
4-BROMOPHENYL PHENYLETHER
ANTHRACENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
<5
<5
10
24
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.8-1
RIC
RIC OATfl:
81/23/88 11:49:80 CALI: CAL123 #1
SAMPLE: B40374: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1.1400 LABEL: N 1, 4.0 QUAN: A 3, 1.8 BASE: U 20, 3
187
i id
12112
288
6:40
488
13:20
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB37C17
ERG SAMPLE // 40375
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAME_TER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
C_°_N-CE_NT_RATI.ON
<.5 yg/1
<.003
<.005
.005
<.005
<.010
<.0002
<1.0 yg/1
<.08
.008
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C.°_N.C_E_NT_RATI_ON (PPB)
<5
16
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.01
uATA. u-r83iv, wl
91/23/80 12:51:09 CALI: CAL123 #1
SAMPLE: B40375: 3 UL SAMPLE, 58 NG D18A
RANGE: G 1,1408 LABEL: N 1, 4.0 QUAN: A 8, 1.8 BASE: U 28, 3
735
SCt—
., 14,_
4648
500
28:08
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB37C18
ERG SAMPLE # 40376
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
c.o.ncjililiiAJ-iO-N
<.50 ug/1.
<.
<
<
<
<
.003
.005
.005
.005
.010
<.0002
<1.0 yg/1
<.08
.007
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
10
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
KiL
01/23/80 13:57:00
SAMPLE: B40376: 3 UL SAMPLE, 50 MG D10A
RANGE: G 1,1400 LABEL: N 1, 4.0 CHAN: A
DAm; B4boro #1
CALI: CAL123 «1
9, 1.0 BASE: U 28, 3
,0
3896
488
13:20
686
26:08
26:48
1008
33:28
1288
48:06
1488 SCAN
46:46 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE § LB37C19
ERG SAMPLE // 40377
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 ug/1
003
005
005
005
010
<.0002
<.08
.008
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
<5
<5
17
OTHER COMPOUNDS
NONE
ENVIRONMENTAL. RESEARCH GROUP, INC.
-------
100.0H
01/24/80 17:19:08 CALI: CAL124 #1
SAMPLE: B40377, 3 UL * 1 UL IS
RANGE: G 1, 1400 LABEL: H \, 4.6 QUAN: A 0, 1.6 BASE: U 20, 3
86?:
800
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 37C20 MATRIX WATER
ERG SAMPLE // 40378 SAMPLE RECEIVED LO/2'J/79
INORGANIC RESULTS
ZAl^AMiijisji £?_N.c_^^Z5.AZl.0_]i
ARSENIC 29 ug/1
CADMIUM <.Q03
COBALT <.005
COPPER <.005
CHROMIUM <-005
LEAD <.010
MERCURY <.0002
SELENIUM <1-0 ug/1
TIN <-08
ZINC .007
% MOISTURE . —
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
ETHYL HEXYL PHTHALATE 14
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/23/80 17:13:00
SAMPLE: B40378, 3 UL + 1 UL IS
RANGE: G 1,1400 LABEL: N 1, 4.0
QUAN: A
100.0-1
DATA: B40378 #1
CALI: CAL123 #1
0, 1.0 BASE: U 20, 3
839
I
SCANS 1 TO 1490
5298
600
20:00
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 1? LB37C21
ERG SAMPLE // 40379
MATRIX WATER
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 yg/1
<.003
<.005
.005
<.005
<.010
<.0002
<1.0 yg/1
<.08
.007
Results reported in rag/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
<5
12
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
81/23/80 18:23:00
SAMPLE: 640379A, 3 UL + 1
RANGE: G 1,1400 LABEL:
DATA:
CALI:
B40379A #1
CAL123 #1
SCANS 1 TO 1408
UL
N
IS
1, 4.0
QUAN: A 0, 1.0 BASE: U 20, 3
108.0
5040
688
20:00
26:49
1008
33:28
1200
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE ff LB34CQ1
ERG SAMPLE // 40380
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAMETE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
8.7
27
13
130
25
98
<1
11
71
167.
63
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OMP_OIJND
HEXACHLOROBUTADIENE
1,2,4 TRICHLOROBENZENE
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BENZO (a) PYRENE
BASE NEUTRAL GC/MS SCAN
150
830
12900
680
680
360
1380
1200
10900
1900
3800
1900
OTHER COMPOUNDS
PCB'S
PENTACHLOROBENZENE
3568
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
198.8-
RIC
81/38/88 21:58:88
SAMPLE: B48388, 3 UL + 1 UL
RANGE: G 1,1488 LABEL: N
DATA:
CALI:
B48388 #1
CAL138 tl
SCANS
1 TO 1480
A 8, 1.8 BASE: U 28, 3
124160
1880
33:20
1280
40:80
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE // LB34C03
ERG SAMPLE 9 40381
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
_PARAM_ET]iR
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
14
25
14
130
26
98
<1
14
87
175.2
48
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBUTADIENE .
1,2,4 TRICHLOROBENZENE
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BENZO (a) PYRENE
BASE NEUTRAL GC/MS SCAN
(PPB)
170
1400
20000
600
600
520
1200
1300
11600
1400
1400
2600
1200
OTHER COMPOUNDS
PCB's
3660
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
109.0-1
RIC
RIC
01/39/80 22:59:00
SAMPLE: 340381, 3 UL + 1 UL IS
RANGE: G 1,1409 LABEL: N 1, 4.0
535
DATA: B40381 tl
CALI: CAL130 tl
QUAN: A 0, 1.0 BASE: U 20, 3
SCANS 1 TO 1409
281
A.
I
200
6:40
174080
608
20:00
26:40
1000
33:20
1200
40:09
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB34C04
ERG SAMPLE //
40382
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAMETE;R.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
£°NC_ENT_RAT_ION
8.6
25
13
130
24
92
<1
12
95
170.0
64
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBUTADIENE
1,2,4 TRICHLOROBENZENE
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BENZO (a) PYRENE
BASE NEUTRAL GC/MS SCAN
O_N (PPB)
110
790
11800
670
670
420
1400
1200
11,100
1600
1600
300
1400
OTHER COMPOUNDS
PCB's
TETRACHLOROBENZENE
PENTACHLOROBENZENE
2420
200
310
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.9-1
DATA: 646382 «1
CALI: CAL138 il
RIC
01/31/80 9:57:00
SAMPLE: B49332: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1480 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
857
SCANS 1 TO 1406
280
6:40
129824
20:00
26:40
1000
33:20
1200
40:08
1
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 34C05
ERG SAMPLE // 40383
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
J?ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
13
26
14
130
24
96
<1
17
82
179.4
60
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,2,4 TRICHLOROBENZENE
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BENZO (a) PYRENE
BASE NEUTRAL GC/MS SCAN
CONCE_NTRA'TI_ON (PPB)
1200
13400
380
380
210
800
770
6600'
760
760
1300
470
OTHER COMPOUNDS
PCB's
PENTACHLOROBENZENE
1890
193
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
188.8-
Rii» JAT 40'
81/31/88 11:83:88 CAU: CAL138 tl
SAMPLE: B48383: 3 UL SAMPLE/ 58 NG 018A
RANGE: G 1/1488 LABEL: N I/ 4.8 QUAN: A 8, 1.8 BASE: U 29, 3
859
J 1.
133128
26:48
1088
33:28
1288
48:86
1
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 34C06
ERG SAMPLE // 40384
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMET1ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
13
1.6
10
27
33
37
<1
<4
50
96.3
33
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
PHENANTHRENE
ANTHRACENE
DIBUTYL.PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C_O^CEN_TRAT:ION (PPB)
50
50
380
100
100
3200
OTHER COMPOUNDS
HYDROCARBONS
UNRESOLVABLE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
91/31/89 12:85:90
SAMPLE: B48384: 3 UL SAMPLE,
RANGE: G 1,1499 LABEL: N
DATA:
CALI:
B49334 II
CALI38 il
SCANS 1 TO 1400
50 NG D19A
1, 4.9 QUAN: A 9,
199.0-,
1.9 BASE:
849
U 20, 3
30592
RIC
490
13:20
600
20:99
26:40
1990
33:20
1200
40:99
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB34C08
ERG SAMPLE // 40385A
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
12
1.6
11
28
31
53
<1
3.6
58
114.2
40
Results reported in rag/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
130
130
130
50
160
170
1400
30
30
OTHER COMPOUNDS
HYDROCARBONS
UNRESOLVABLE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/31/89 1:59:00
SAMPLE: B40335A: 3
RANGE: G 1,1400
DATA:
CALI:
B40385A «1
CAL130 II
SCANS 1 TO 1408
UL SAMPLE, 50 NG D10A
LABEL: N 1, 4.0 QUAN: A 0,
100.0n
1.0 BASE:
852
U 20, 3
105344
600
20:00
800
26:40
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB34C08
ERG SAMPLE // 40385B
MATRIX SEDIMENT
SAMPLE RECEIVED LO/29/79
INORGANIC RESULTS
P_ARAM_E;TE:R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
12
1.6
11
28
31
53
<1
3.6
58
114.2
40
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
PYRENE
ETHYL HEXYL PHTHALATE
20
20
70
20
740
OTHER COMPOUNDS
HYDROCARBONS
UNRESOLVABLE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
91/31/88 3:16:09
SAMPLE: B40385B: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAH:
DATA:
CALI:
B40335B II
CAL130 #1
SCANS
1 TO 1400
A 8,
100.0-1
1.0 BASE:
849
U 20, 3
26336
RIC
90S
290
6:40
400
13:20
600
20:80
1000
33:20
1200
40:00
1406 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE f LB 34C10
ERG SAMPLE t 40386
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PAjiAMETjSR
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
9.4
1.6
9.9
29
33
45
.48
4.6
36
96.8
41
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BEN20 (a) ANTHRACENE
60
550
550
130
680
620
3200
450
450
OTHER COMPOUNDS
HYDROCARBONS
LONG CHAIN ACIDS
UNRESOLVABLE
UNRESOLVABLE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
81/31/89 17:23:08
SAMPLE: 840386, 3 UL + 1 UL IS
RANGE: G 1,1490 LABEL: N I/
DATA: B48386 #1
CALI: CAL131 «1
SCANS 1 TO 1488
4.0 QUAN: A 0,
108.0-
1.8 BASE:
854
U 20, 3
58688
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 0 LB 34C11
ERG SAMPLE // 40387
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAMJST.ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
8
7.0
'12
34
49
37
<.7
1.5
51
126.8
49
Results reported in mS/kS unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,4 DICHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BASE NEUTRAL GC/MS SCAN
Cp_NC_E£TRAT1.0N
2200
500
500
260
1200
960
2700
700
700
420
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
RIC DATA: B48387 tl
81/31/88 18:21:06 CALI: CAL131 «1
SAMPLE: B48387, 3 UL * 1 UL IS
RANGE: G 1,1488 LABEL: N I/ 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
451
862
SCANS 1 TO 1408
288
6:48
488
13:28
26:48
1888
33:28
1288
48:88
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 9 LB34C12
ERG SAMPLE // 40388A
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
11
7.1
11
33
47
38
<1
<3
64
122.2
39
Results reported in rag/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,4 DICHLOROBENZENE
HEXACHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BASE NEUTRAL GC/MS SCAN
2900
20 *
530
530
220
780
780
1700
380
380
220 *
OTHER COMPOUNDS
METHYL PHENANTHRENE
METHYL ANTHRACENE
113.8 (TOTAL BOTH
COMPOUNDS)
*Please refer to correspondence PE/ES, 4/8/80
ENVIRONMENTAL RESEARCH OROUP. INC.
-------
186.6-1
RIC
RIC DATA: B48388A II
02/21/S8 4:43:86 CALI: CAL31JAN2 #1
SAMPLE: B48388A: 3 UL SAMPLE, 56 NG D18A
RANGE: G 1,1408 LABEL: N 1, 4.8 QUAN: A 6, 1.8 BASE: U 28, 3
448
J
854
SCANS
1 TO
15128
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 34C12
ERG SAMPLE // 40388B
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PARAMETER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
£P-N.c_j;NTRATI_ON
11
7.1
11
33
47
38
<1
<3
64
122.2
39
Results reported in rag/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,4 DICHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BASE NEUTRAL GC/MS SCAN
0 N C E N T R A T 10. N (PPB>
2700
230
230
60
440
490
1100
150
150
OTHER COMPOUNDS
METHYL PHENANTHRENE)
METHYL ANTHRACENE )
113.8 (TOTAL BOTH
COMPOUNDS)
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/31/80 21:13:00
SAMPLE: B40338B, 3 UL + 1 UL IS
RANGE: G 1,1400 LABEL: N 1, 4.0
QUAN: A
100.01
DATA: B48383B II
CALI: CAL131 »1
1.0 BASE: U 20, 3
856
SCANS 1 TO 1400
8768
449
RIC
217
JL
208
6:40
400
13:20
26:40
1000
33:20
1260
48:06
1400 SCAN
46:46 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 34C13
ERG SAMPLE // 40389
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAM_ET_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
70
7.3
11
33
49
37
<5
63
125.6
37
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
520
520
190
920
1100
1700
730
730
350
OTHER COMPOUNDS
METHYL PHENANTHRENE
METHYL ANTHRACENE
14 (TOTAL BOTH
COMPOUNDS)
IN6,
-------
RIC
81/31/80 23:19:80
SAMPLE: B48339, 3 UL + 1 UL IS
RANGE: G L 1488 LABEL: N 1,
4.8 QUAN: A 8, 1.8
100.8-1
DATA: B48389 #583
CALI: CAL2FEB #3
BASE: U 28, 3
358
SCANS
1 TO 1488
18368
RIC
288
6:48
26:48
1888
33:20
1286
40:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB34C14
ERG SAMPLE 9 40390
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
A M E T E R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
Results reported in
mg/kg
11
8.3
11
35
50
38
1.6
61
128.3
43
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
1,4 DICHLOROBENZENE
NAPHTHALENE
1,2,4 TRICHLOROBENZENE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
GHRYSENE
BENZO (a) ANTHRACENE
BENZO (k) FLUORANTHENE
BENZO (a) PYRENE
BASE NEUTRAL GC/MS SCAN
COrȣE_NTRATI_p_N
7000
10
100 . .
740
740
280
930
970
2600
590
590
370
70
(PPB)
OTHER COMPOUNDS
CHLORINATED STYRENE
139
RiMARCH OH3UP, I NO,
-------
108.8-1
RIC
RIC DATA: B48338 «1
82/81/88 3:36:88 CALI: CAL2FEB #3
SAMPLE: B48398: 3 UL SAMPLE, 58 NG 018A
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
442
SCANS 1 TO 1480
29664
488
13:20
680
20:08
26:48
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB34C17
ERG SAMPLE // 40391
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAM_ET_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
Results reported in
52
<.74
<.74
<2.5
<2
<5
29
<2.5
21
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OMJPO]J_ND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
100
790
OTHER COMPOUNDS
NONE
I NVIMONMf NTAL MIIAHCH OMOUP, ING,
-------
iic
82/91/86 5:44:06
SAMPLE: B40391, 3 UL + I UL IS
RANGE: G 1,1408 LABEL: N
DATA: B46391 «1
CALI: CAL31JAN2 #1
1.8 BASE: U 26, 3
SCANS 1 TO I486
106.0-1
RIC
1666
33:26
1286
48:66
I486 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 34C18
ERG SAMPLE // 40392
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
PA_RAME;TE:R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONC_fc:N_TR_ATJ.ON
2
<.70
<.70
<2.3
<1
<4
<2.5
15
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
30
520
• NVIRONMINTAL HBSIAMCH QHOUP, INC.
-------
180.8-1
RIC
82/81/88 6:44:88
SAMPLE: B48392, 3 UL + 1 UL IS
RANGE: G 1,1488 LABEL: N 1,
369
DATA: B48392 II
CALI: CAL31JMH2 il
4.0 QUAN: A 0, 1.8 BASE: U 28, 3
SCANS
1 TO I486
55368
282
RIC
586
1 1
^ b A
.
B
"A A «£:»..,
812
1
\ 639 „ ,766 fc. K^SX
• 98J • M49 » »'»1290
• ni • i •» i iir"^ i
208
6:48
408
13:28
688
28:88
26:48
1888
33:20
1288
40:88
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 34C19
ERG SAMPLE // 40393
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P.ARAME:T.ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<.74
<.74
<2.5
53
<2.5
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
20
no
OTHER COMPOUNDS
NONE
BNVIMONMINTAL NMIAMCH OHOUP, INC.
-------
100.0n
RIC
92/01/80 7:45:00
SAMPLE: B40333A, 3 UL + 1 UL IS
RANGE: G 1,1408 LABEL: N 1, 4.0
586
DATA: B48393A #1
CALI: CAL31JAN2 #1
QUAN: A 8, 1.0 BASE: U 26, 3
SCANS
1 TO 1400
RIC
6264
857
1000
33:20
1200
48:06
1430 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX .
E.P.A. SAMPLE it LB34C21
ERG SAMPLE 1} 40394
MATRIX SEDIMENT
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
lARAMET.ER,
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
120
380
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.8-
RIC
82/01/80 9:29:08
SAMPLE: B40394, 3 UL + 1 UL IS
RANGE: G L1400 LABEL: N 1,
374
DATA: B48394 »1
CALI: CAL31JAN2 #1
4.8 QUAN: A 8, 1.0 BASE: U 20, 3
SCANS
1 TO 1400
22408
33:29
1200
40:00
1480 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 39C501
ERG SAMPLE ff 40395
MATRIX FISH FOOD
SAMPLE RECEIVED 10/29/79
INORGANIC RESULTS
P_ARAME_T_:ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.24
<-72
<1.2
67
<7.2
2.8
<1
<3
38
44.76
Results reported in mg/kg unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
880
13000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
02/13/88 21:43:80
SAMPLE: B40395
RANGE: G 1,1409
LABEL: N 1, 4.0 QUAN: A 9, 1.0
100.8-1
DATA: B46395 #1
CALI: CAL213 #3
BASE: U 20, 3
921
SCANS
1 TO 1400
465920
200
6:40
400
13:20
600
20:08
1000
33:20
1200
40:00
I
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C01
ERG SAMPLE //
MATRIX WATER
41278
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.78 ug/1
<.003
.007
.012
<.005
.013
<.0002
2.4 ug/1
.088
.019
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
<5
86
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/24/89 3:09:00
SAMPLE: B41278:3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN:
UHiA:
CALI:
i4U0
CAL124 #1
BASE: U 20, 3
180.0-1
9744
200
6:40
400
13:20
800
26:40
1068
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE t LB 40C02
ERG SAMPLE //
MATRIX WATER
41279
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_A_RAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
.59 ug/1
.004
.007
.007
<.005
.015
<.0002
1.3 jjg/1
<.08
.018
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
(PP8)
<5
31
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/24/80 18:10:00
SAMPLE: B41279: 3 UL SAMPLE,
RANGE: G 1,1408 LABEL: N
DATA:
CALI:
B412f'S *1
CAL124 #1
SCHNi
1 iU
50 NG D10A
1, 4.0 QUAN:
160. 3-1
8^1.8
1 85
BASE: U 20, 3
719
585
RIC
5008
280
6:40
28:88
26:48
1888
33:28
1288
40:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C03 MATRIX WATER
ERG SAMPLE # 41280 SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PAR.AMETI5R
ARSENIC 1.6 ug/1
CADMIUM <.003
COBALT <.005
COPPER -OO^
CHROMIUM -0°6
LEAD -010
MERCURY <•°002
SELENIUM I-3 US/1
TIN <-08
ZINC -011
% MOISTURE .
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
<:OMP_OU^D c_0.N_
-------
RIC
01/24/80 11:12:00
SAMPLE: B41280: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1400 LABEL: H 1, 4.6 QUAN:
DATA: B41280 ttl
CALI: CAL123 #1
A 0, 1.0 BASE: U 20, 3
SCANS
1 IU
100.0-1
5584
RIC
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C04
ERG SAMPLE // 41281
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
£AR.AME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 yg/1
<.003
<.005
.012
.006
<.010
<.0002
<1.0 yg/1
<.08
.046
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
<:OM.PO]JND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
18
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
186.8
RIC
01/24/80 18:34:00
SAMPLE: B412S1, 3 UL + 1 UL IS
RANGE: G 1,1488 LABEL: N 1,
510
DATH:
CALI:
B412S1 #1
CAL124 #1
SCnro
i IU
4.8 QUAN: A 8, 1.8 BASE: U 20. 3
5688
488
13:28
688
28:88
26:48
1808
33:28
1208
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 40C05
ERG SAMPLE t 41282
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 yg/1
<.003
<.005
.009
<.005
<.010
<.0002
l.< ug/1
<.08
.024
ON
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OMPOUfJD
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
^ (PPB)
50
OTHER COMPOUNDS.
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/24/38 13:37:00
SAMPLE: B41232, 3 UL * 1 UL IS
RANGE; G 1,1400 LABEL: N 1,
4.0 QUAN: A
0, 1.0
738
DATA: 841282 #1
CALI: CAL124 Kl
BASE: U 20, 3
SCANS
1 TO 1408
9584
see
20:06
26:40
1000
33:20
1200
40:00
1480 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C06
ERG SAMPLE // 41283
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_AR_AME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<.5 yg/1
<.003
<.005
.007
.005
<.010
<.0002
1.3 ug/1
<.08
.021
Results reported in ™g/l unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_0_MP_()y_]IP-
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
C.ONC.E.NTIRATI.O.N (PPB)
31
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
81/24/88 29:39:80
SAMPLE: B41283, 3 UL + 1 UL IS
RANGE: G 1,1488 LABEL: N 1,
DATA: B41233 #1
CALI: CAL124 #1
4.0 QUAN: A 0, 1.8 BASE: U 20, 3
SCANS
1 TO
108.0-1
733
RIC
4672
1088
33:20
1208
48:88
1
1408 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE ff LB40CQ7
ERG SAMPLE // 41284
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 yg/1
<.003
<.005
.005
<.005
<.' 010
<.0002
<1.0 yg/1
<.08
.013
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
(?OM£OIJNI)
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
92
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.0-1
RIC
Rlf
81/24/30 21:50:80
SAMPLE: 841284, 3 UL + 1 UL IS
RANGE: G 1,1400 LABEL: N 1, 4.0
GUAM: A
OATn: o41Iot ffl
CALI: CAL124 #1
BASE: U 20, 3
SCnno
I I J 1 T
200
6:40
600
20:00
800
26:40
1000
33:20
11072
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C08
ERG SAMPLE // 41285A
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P.ARAM1ST.ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
7. MOISTURE
<.05 yg/1
<.003
<.005
.006
.007
.011
<.0002
1.2 yg/1
<-08
.007
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_0_M.POIJ_ND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
100
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.0-
RIC_
i
1
•1
RIC
01/24/88 22:55:89
SAMPLE: B41285A, 3 UL + 1 UL
RANGE: G 1,1468 LABEL: N
;5<
339 t£p
UrtV'-"*" .^.n^rY*^!,^^
288 408
6:48 13:28
IS
1, 4.8 QUAN: A 8, I
722
17
577
jA J-. .
CALI: CAL124 #1
..8 BASE: U 20, 3
11136
Tl&i11- 1862 1169 -1339ft
688 888 1888 1288 1488 SCAN
28:88 26:48 33:28 48:88 46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB40C08
ERG SAMPLE // 41285B
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
_PARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCJJN.TRATI.ON
<-5 yg/1
<.003
<. 005
.006
.007
.011
<.0002
1.2 yg/1
<.08
.007
Results reported in rag/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (ppe)
ETHYL HEXYL PHTHALATE
79
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIu
01/25/80 9:03:00
SAMPLE: B41285B: 3 UL SAMPLE.. 58 NG D10A
RANGE: G 1,1460 LABEL: N 1, 4.0 QUAH: A
100.0-1
565
RIC
259
451
576
L
6, 1.0
78b
JATl.. «
CALI: CAL125 #1
BASE: U 20, 3
H
720
hji
2538
280
6:40
460
13:20
660
20:00
1000
33:20
1200
40:00
1460 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB40C09
ERG SAMPLE // 41286
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
<.5 yg/1
<. 003
<.005
.005
<.005
<.010
<.0002
<1.0 yg/1
<.08
.009
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OM.P()y_ND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
43
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
108.0-1
RIC
81/25/89 12:10:68
SAMPLE: B41285: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN:
505
UATA:
CALI:
SCAns
I ill 14bu
CAL125 #1
H 0, 1.8 BASE: U 20, 3
RIC
230 304 .
,444
nr
200
6:40
789
723
876 '
jA^ugg^^u
1229 1347
i^^^Tv^^i^^A^tK*
480
13:20
600
20:06
888
26:40
1808
33:28
1280
40:80
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB 40C10 MATRIX WATER
ERG SAMPLE 9 41287 SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMETER £ 0_ N C _E N T R A T I 0 N
ARSENIC <-5 yg/1
CADMIUM <. 003
COBALT <.005
COPPER .005
CHROMIUM <.005
LEAD <.010
MERCURY <.0002
SELENIUM <1.0 Ug/1
TIN <-08
ZINC .010
% MOISTURE
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
£0_MP_0]J_NI) (LO.N^.EN.TIRATI.O.bl (PPB)
ETHYL HEXYL PHTHALATE 51
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/25/88 14:18:80
SAMPLE: B41287: 3 UL SAMPLE, 58 NG D18A
RANGE: G L 1488 LABEL: N 1, 4.8 QUAN:
UHTA: Dti28r «i
CALI: CAL125 #1
BASE: U 28, 3
iu
188.0
5446
488
13:28
608
28:08
808
26:40
1008
33:20
1200
40:80
1488 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 40G11
ERG SAMPLE // 41288A
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
I A R. A M E: T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
T '! 0 N
<.5 ug/1
<.003
<.005
.007
<.005
<.010
<.0002
<1.0 yg/1
<.08
.024
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_p_M£0_lJ_ND
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
0 N C
53
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
188.8-1
RIC
R^ DAI... _41L_... #1
01/25/80 15:16:09 CALI: CAL125 #1
SAMPLE: B41238A: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
503 734
579
719
I
400
13:20
600
20:00
800
26:40
1600
33:20
SC..
) 1.
323S
1234 •>*•
1200
40:00
-^
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB40C11
ERG SAMPLE // A1288B
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMET,E_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<.5 yg/1
<.003
<.005
.007
<.005
<.010
<.0002
<1.0 yg/1
<.08
.024
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£ £ M ,P ;p_ £ N, D
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
67
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
188.8-1
RIC
RlL
01/25/88 16:20:00
SAMPLE: B41288B: 3 UL SAMPLE. 50 NG D10A
RANGE: G I/ 1488 LABEL: N 1, 4.0 QUAN:
506
I' « 144 ' '
ddw
44 , , 310«. * I
*«»illh^^>»y^^>WW^
8, 1.0
787
-HTfi. ~.12Lw~ A
CALI: CAL125 #1
BASE: U 28, 3
SCh.._
722
200
6:40
460
13:20
608
20:88
880
26:40
1,; 987 ...» .1698 * 1183 > 1289.. 1316"
W^HU^*YW»**
1000
33:28
T
1288
40:88
862*
1400 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE 9 LB40C12 MATRIX WATER
ERG SAMPLE // 41289 SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC <.5 yg/1
CADMIUM <.003
COBALT <. 005
COPPER .007
CHROMIUM .005
LEAD <.010
MERCURY <.0002
SELENIUM <1.0 Mg/1
TIN <.08
ZINC .018
% MOISTURE
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
ETHYL HEXYL PHTHALATE . 84
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/25/88 19:40:00
SAMPLE: B41283, 3 UL + 1 UL
RANGE: G 1,1408 LABEL: N
14bu
IS
CALI: CAL125 #1
4.0 QUAN: A 0, 1.0 BASE: U 20, 3
180.0-1
785
719
RIC
504
1072U
1-274 1-364
200
6:40
400
13:20
688
28:88
808
26:48
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE I LB 40C13 MATRIX WATER
ERG SAMPLE // 41290 SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
I A R A M E_ T E_ R £ 0 N C E_ N T R A T 1^ 0 N^
ARSENIC <-5 Mg/1
CADMIUM < • 003
COBALT <•005
COPPER •°08
CHROMIUM <•005
LEAD <•010
MERCURY <.0002
SELENIUM
-------
01/25/80 20:44:80
SAMPLE: 641290, 3 UL + 1 UL IS
RANGE: G 1,1468 LABEL: N 1, 4.6
CALI: CAL125 #1
QUAN: A
160.8-1
0, 1.0
783
BASE: U 28,
3
3736
280
6:40
606
20:60
800
26:40
1090
33:20
1260
40:00
140y SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB 40C14
ERG SAMPLE // 41291
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMET:IER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 yg/1
<.003
<.005
.008
.008
<.010
<.0002
<1.0 ug/1
<.08
.024
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£P_M.Pp_U_JS[D
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
73
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100. 0-j
RIC ,
tm29i mi
CALI: CAL125 #1
rtIC
01/25/80 22:35:00
SAMPLE: 641291, 3 UL + 1 UL IS
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 20,
739
1 lu 140o
400
13:26
600
20:00
26:40
1000
33:20
3504
956. IK 1,068 H58
1301
T
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB40C15
ERG SAMPLE // 41292
MATRIX
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
<-5 ug/1
<.003
<.005
.009
.005
<.010
<.0002
<1.0 yg/1
<.08
.034
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
(:OMP_p_lJ_Np_
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
60
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/3W/80 12:48:88
SAMPLE: B41292: 3
RANGE: G 1,1498
UL SAMPLE,
LABEL: N
DATA:
CALI:
B41292 fl
CAL138 tl
SCflN5
1 TO 1400
58 NG D19A
I/ 4.8 QUAN:
A 8, 1.8 BASE: U 28, 3
188.8-1
8832
RIC
583
532
48
&
742
288
6:48
488
13:28
688
28:88
888
26:40
1880
33:28
1280
40:80
1480 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE # LB 40C16
ERG SAMPLE // 41291
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
E R
•76 yg/1
<.003
<.005
<.005
<.005
.012
<.0002
<1.0 ug/1
<.08
.009
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
(:OM,POU_ND
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
50
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
91/30/88 13:39:90
SAMPLE: B41233: 3 UL SAMPLE,
RANGE: G 1,1406 LABEL: N
50 NG D19A
1. 4.0 QUAN:
DATA:
CALI:
B41293 ttl
CAL138 tl
SCANS 1 TO 1400
A 8, 1.0 BASE: U 20, 3
100.01
10944
RIC
742
583
532
296
6:40
400
13:29
i
600
20:00
26:48
1000
33:28
1206
40:08
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB40C17 MATRIX WATER
ERG SAMPLE // 41294 SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME^TE_R C.0_N.C_E_NTRATI^O^
ARSENIC <-5 yg/1.
CADMIUM <•003
COBALT <.005
COPPER -005
CHROMIUM <•005
LEAD <•010
MERCURY <.0002
SELENIUM 1.3 yg/1
TIN <-08
ZINC -012
% MOISTURE
Results reported in mS/l unless otherwise noted.
ORGANIC RESULTS BASE NEUTRAL GC/MS SCAN
PRIORITY POLLUTANTS
CrtM"D'ATiMT\ fOMfP'NT'P.A'FTOMi PP R ^
UC'lirUUWU \* \j n \t & n i, R. i\ i ±. \J in \I?L Of
ETHYL HEXYL PHTHALATE 50
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
81/38/88 14:37:98
SAMPLE: B41294: 3 UL SAMPLE,
RANGE: G 1,1488 LABEL: N
DATA:
CALI:
B41294 II
CAL138 11
SCANS
1 TO 1488
58 NG D18A
I/ 4.8 QUAN:
A 8,
180.8-.
1.8
887
BASE: U 28, 3
PIC
583
532
415
_JL_
288
6:48
i
488
13:28
633
688
28:88
12568
855,
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U..S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 40C18
ERG SAMPLE // 41295
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
<-5 Mg/1
<.003
<.005
005
008
010
0002
<1.0 yg/1
<.08
.008
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
(]OMP_0]JND
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
50
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/30/80 15:45:00
SAMPLE: B41295: 3 UL SAMPLE, 50 NG D10A
RANGE: G 1,1480 LABEL: N 1, 4.0 QUAN: A 8,
DATA: B4123S fl
CALI: CAL130 11
i lu 1400
100.8-j
1.0
889
BASE: U 20, 3
RIC
584
743
416
I
200
6:40
13760
858 •• 940
486
13:20
,1664
800
26:40
1000
33:20
1200
40:00
1406 SCAN
46:40 TIHE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE # LB 40C19
ERG SAMPLE // 41296
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
_PAR_AME_T1EJR
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
3.3 yg/1
003
005
005
005
010
0002
<1.0 yg/1
<.08
.010
Results reported in rag/I unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£ 0 M _P 0 IJ tl D
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
40
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
01/38/88 16:54:09
SAMPLE: B41296, 3 UL «• 1 UL IS
RANGE: G 1/1406 LABEL: H 1,
DATA: B41296 il
CALI: CAL130 «1
bCANb
i4Qy
4.0 QUAH: A 0,
108.8-1
1.8 BASE:
817
U 28, 3
3680
RIC
589
38
751
537
200
6:40
nr
400
13:28
680
20:00
26:46
1000
33:20
1206
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE # LB40C20
ERG SAMPLE // 41297
MATRIX WATER
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
30 Mg/1.
<-003
<.005
<.005
<.005
<.010
<.0002
<1.0 yg/1
<.08
.018
Results reported in mg/1 unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIETHYL PHTHALATE
ANTHRACENE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C_°_.N-C_JL^TRATI.ON (PPB)
10
<5
130
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/38/88 17:54:88
SAMPLE: B41297, 3 UL + 1 UL IS
RANGE: G 1,1480 LABEL: N 1,
DATA: B412Ah£^W4feMi^^to^Aa^^taMiAM^
688
28:88
26:48
1000
33:20
f
1200
40:00
"1
1400 SCAN
46:40 TIHE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C01
ERG SAMPLE // 41299A
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAM_ET:ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C_ONJC_EbITRATI_ON
380
2700
6200
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/99/88 18:19:88
SAMPLE: B41299A EPA FISH
RANGE: G 1,1368 LABEL:
DATA:
CALI:
B41299A #1
CAL2FEB *3
SCANS 1 TO 1360
N 1, 4.8 QUAN: A 0, 1.0 BASE: U 20, 3
180.0-1
1153
14886
859
RIC
496
1
200
6:40
400
13:20
33:29
1200
40:00
SCAN
TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C01
ERG SAMPLE // 41299B
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME_T_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
BUTYL BENZYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
1900
8000
2600
6300
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/10/89 11:23:90
SAMPLE: 8412938 EPA FISH
RANGE: G 1,1400 LABEL-
DATA: 8412998 #1
CALI: CAL2FEB #3
N 1, 4.8 QUAN: A 8, 1.8 8ASE: U 20, 3
SCANS
1 TO 1409
188.8-1
1150
RIC
28352
1080
33:28
1208
48:08
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
EC P. A. SAMPLE // LB41C02
ERG SAMPLE // 41300
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
1500
2900
4000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
108.8-,
RIC
DATA: B41388 »1
CALI: CAL2FEB #3
RIC
82/11/88 13:19:88
SAMPLE: B41388 EPA FISH
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 0, 1.8 BASE: U 28,
85?
SCANS
1 TO I486
1156
2692
288
6:48
488
13:28
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB 41C03
ERG SAMPLE 9 41301
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME_T_ER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
2000
2700
OTHER COMPOUNDS
NONE
ENVIRONMENTAL. RESEARCH GROUP, INC.
-------
RIC
82/11/38 11:21:88
SAMPLE: B41381 EPA FISH
RANGE: G 1,1488 LABEL:
DATA:
CALI:
B41381 #356
CAL2FEB *3
SCANS 1 TO 1488
N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
100.0-1
1147
6864
RIC
989
495
A
581
/L
288
6:48
408
13:28
688
28:88
1888
hii15
M^AWlMh-^
*
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB41C04
ERG SAMPLE // 41302
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMET_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
2700
550
1400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
180.0-
RIC DATA: B41302 »1
02/10/80 6:00:08 CALI: CAL2FEB #3
SAMPLE: B41302 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.8 QUAN: A 0, 1.8 BASE: U 20, 3
79b
SCANS
1 TO 1480
RIC
4664
13:20
600
20:00
26:40
1000
33:20
1200
40:00
1400 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A.. SAMPLE // LB41C05
ERG SAMPLE // 41303
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
_PARAME_TE_:R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported.In —
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
4000
1300
810
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.13-1
RIC
02/18/86 14:28:00
SAMPLE: B41303 EPA FISH
RANGE: G 1,1489 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
DATA: B41303 ttl
CALI: CAL2FEB #3
SCANS 1 TO 1480
1157
4776
490
13:20
600
20:96
26:40
1000
33:20
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // Lfi41C06
ERG SAMPLE // 41304
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMjiTE_R
ARSENIC.
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
D.IBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
660
680
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/18/88 17:81:80
SAMPLE: B41384 EPA FISH
RANGE: G 1,1408 LABEL:
DATA: B41304 ttl
CALI: CAL2FEB 13
N 1, 4.8 QUAN: A 0,
188.0-,
1.8 BASE:
823
U 20, 3
SCANS
1 TO I486
RIC
200
6:40
480
13:28
800
26:40
1000
33:20
1200
40:00
1480 SCAN
46:40 TINE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C07
ERG SAMPLE // 41305
MATRIX FISH
SAMPLE RECEIVED LI/14/79
INORGANIC RESULTS
_PARAME_TE__R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
EHTYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
810
360
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/11/88 3:11:98
SAMPLE: B41385 EPA FISH
RANGE: G 1,1488 LABEL: N
100.8-1
DATA: B41385 #1
CALIs CAL211 #3
4.8 QUAN: A 8, 1.8 BASE: U 28, 3
827
648
SCANS
1 TO 1488
1273
RIC
768
912
1165
200
6:48
486
13:28
688
28:86
26:48
1888
33:28
1288
48:68
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB41C08
ERG SAMPLE // 41306
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAMjiT_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
£OM_P£UNE>
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
460
570
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC DATA: B41386 #1
82/11/88 12:20:08 CALI: CAL2FEB #3
SAMPLE: B41386 EPA FISH
RANGE: G 1,1408 LABEL: N 1, 4.0 QUAN: A 8, 1.8 BASE: U 20, 3
SCANS
1 TO 1408
100.0-
1158
1182
488
13:28
680
28:00
26:48
1088
33:20
1288
48:88
1480 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C09
ERG SAMPLE // ., 41307
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C.OL.NCE.N.TRATI.ON (PPB)
920
860
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
DATA: B41307 fl
CALI: CAL2FEB 13
100.0-1
RIC
02/18/88 12:21:88
SAMPLE: B41387 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 6, 1.0 BASE: U 20, 3
968
SCANS
1 TO 1400
824
480
13:20
608
28:00
800
26:40
1000
33:20
1155
4192
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C10
ERG SAMPLE // 41308
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAM_ETE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
C_0_NC__E^TR A T_ I_ ON (PPB)
400
350
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
108.0-1
RIC
RIC DATA: 841388 #1
92/10/88 19:16:88 CALI: CAL2FEB #3
SAMPLE: 641388 EPA FISH
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
824
SCANS
1 TO 1488
1152
2724
208
6:48
488
13:28
888
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE //
ERG SAMPLE // 41309A
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
2100
1700
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/18x89 13:22:99
SAMPLE: B41303A E
RANGE:'c 1,1490
FISH
LABEL: N
DATA: B41399A #1
CALI: CAL2FEB #3
1, 4.9 QUAN: A 9, 1.9 BASE: U 20, 3
SCANS 1 TO 1490
188.
18784
1149
RIC
200
6:49
690
26:09
800
26:40
1090
33:20
1209
40:99
1480 SCAN
46:49 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB41C11
ERG SAMPLE // 41309B
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
^PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
O^ (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
5000
1200
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/10/SQ 16:03:90
SAMPLE: B41303B EPA FISH
RANGE: G 1,1400 LABEL:
DATA: B41309B #1
CALI: CAL2FEB 13
SCANS
1 TO 1400
N L 4.8 QUAN: A 0, 1.0
100.0-
BASE: U 20,
917
3
RIC
13920
1008
33:20
1200
48:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE // LB 41C12
ERG SAMPLE if
41310
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P.ARAMJETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
2600
740
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/11/88 15:23:88
SAMPLE: B41318 EPA FISH
RANGE: G 1,1486 LABEL:
DATA:
CALI:
B41318 #1
CAL2FEB #3
SCANS 1 TO 1409
N 1, 4.8 QUAN: A
100.0-1
0, 1.8
795
BASE: U 28, 3
10416
RIC
501
>_ A.
656 I
1183
1026 .4110
13U *•
280
6:40
400
13:28
609
28:06
26:40
1000
33:20
1208
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE
ERG SAMPLE //
LB41C13
41311
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMEITIER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
1500
1400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/11/88 14:25:06
SAMPLE: 841311 EPA FISH
RANGE: G 1,1400 LABEL:
DATA:
CALI:
B41311 #1
CAL2FEB *3
SCANS
1 TO 1408
N I/ 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
100.0-1
1159
RIC
652
200
6:40
498
729
400
13:20
I
600
28:00
973
11776
1316
26:48
1000
33:28
1208
40:88
1480 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41C14
liRG SAMPLE //
MATRIX FISH
41312
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
C_OM.POUN_D
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
oN (PPB)
5600
760
OTHER COMPOUNDS
NONE.
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
92/11/88 18:41:00
SAMPLE: B41312 EPA FISH
RANGE: G 1/1400 LABEL: N
100.0-1
1, 4.0 QUAN: A 0, 1.0
719
DATA: B41312 #1
CALI: CAL211 #3
BASE: U 20, 3
SCANS 1 TO 1480
1176
RIC
7256
6:40
688
28:88
26:48
1000
33:20
1200
40:08
1408 SCAN
46:48 TIHE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41C15
ERG SAMPLE // 41313
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C_Ot4C_jiNTRATI_()fJ
3300
27500
OTHER COMPOUNDS
NONANEDIOIC ACID, bis (2-ETHYL HEXYL) ESTER
245000
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/11/80 19:39:00
SAMPLE: B41313 EPA FISH
RANGE: G 1,1480 LABEL: N
1/4.0 QUAN: A
100.0-1
0, 1.8
775
DATA: 641313 #1
CALI: CAL211 t3
BASE: U 28, 3
SCANS
1 TO 1408
RIC
477 , , 631 , 708 • •
251904
1153
841
959
200
6:40
13:28
600
20:00
26:40
~T~
1000
33:20
'1099
L**1230 1323 •
T
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41C16
ERG SAMPLE // 41314A
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
.PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in —
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMP_0]JNr)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
E fl T; R A T I_ 0 _N (PPB)
670
600
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/11/89 21:46:90
SAMPLE: B41314A EPA FISH
RANGE: G 1,1400 LABEL: N
1, 4.0 QUAN: A
100.9-
0, 1.0
776
DATA: B41314A «1
CALI: CAL211 #3
BASE: U 20, 3
SCANS 1 TO 1400
1167
RJC
5480
1000
33:20
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX.
E.P.A. SAMPLE It LB 41C16
I<:RG SAMPLE // 41314B
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
.SELENIUM
TIN
ZINC
7, MOISTURE
CONCENTRATION
Results reported in —
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
610
270
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/11/80 23:00:08
SAMPLE: B41314B EPA FISH
RANGE: G 1,1400 LABEL:
DATA:
CALI:
B41314B *!
CAL2FEB #3
SCANS 1 TO 1400
N 1, 4.0 QUAN: A 0,
100.0-
1.0 BASE:
335
U 20, 3
RIC
1191
2466
600
20:00
26:40
1000
33:20
1200
46:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41C17
ERG SAMPLE // 41315
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in —
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
PHENANTHRENE
ANTHRACENE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
BUTYL BENZYL PHTHALATE
ETHYL HEXYL PHTHALATE
CHRYSENE
BASE NEUTRAL GC/MS SCAN
ON (PPB)
750
9900
840.
840
1100
520
520
1800
11000
250
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
P*2-/85-/S6 2 i: 52:68
SAMPLE:~B41315 FISH
ANGE: G 1,1480 LABEL
DATA: B41315 #1
CALI: CAL320e #1
H (?.. 4.6 C'UhN: k 0.. 1.3 BnSE: U 2C>
i !v
6:-40
13:20
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE # LB 41C18
ERG SAMPLE // 41316
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P.ARAME_T_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
FLUORANTHENE
PYRENE
ETHYL HEXYL PHTHALATE
CHRYSENE
BENZO (a) ANTHRACENE
BASE NEUTRAL GC/MS SCAN
N. (ppB)
570
7300
480
100
110
27000
290.
290
OTHER COMPOUNDS
PCB's
40
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/85/80 23:11:08
SAMPLE: B41316 FISH
RANGE: G 1,1408 LABEL: N
1, 4.8 QUAN: A 8,
100.8-1
DATA: B41316 #1
CALI: CAL3288 #1
1.8 BASE: U 20, 3
827
SCANS 1 TO 1488
RIC
fl ,. TO, 694 , *
vl j. r\— k •
288
6:48
T
408
13:20
r
608
20:00
85120
875
1861
994
1>26-- -1264".. 1363
800
26:40
I
1000
33:20
1200
40:00
1400
46:40
SCAN
TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41C19
I'RG SAMPLE // 41317
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIMETHYL PHTHALATE
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
800
14000
710
1800
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.0-1
RIC
RIC DATA: B41317 #1
82/86/88 10:28:88 CALI: CAL3200 #1
SAMPLE: B41317 FISH
RANGE: G 1,1480 LABEL: N 1, 4.0 QUAN: A 0, 1.8 BASE: U 20, 3
520
SCANS 1 TO 1400
400
13:20
600
20:00
878
.97* ,, 1967,,-1163
800
26:40
1000
33:20
1200
40:00
5640
,1360
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
•;.!>.A. SAMPLE * LB A1C2°
•KG SAMPLE // 41318
MATRIX FISH
SAMPLE RECEIVED 11/1.4/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TEN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
0 N C K N T R A T 1. 0 N (PPB)
1100
340
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
188.0-1
RIC
RIC DATA: B41318 #1
02/11/88 17:37:88 CALI: CAL211 13
SAMPLE: B41318 EPA FISH
RANGE: G 1,1408 LABEL: N 1, 4.0 QUAN: A 0. 1.0 BASE: U 20, 3
208
6:48
888
26:40
1808
33:28
SCANS
1 TO 1408
1168
13984
1288
48:00
1488 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
K.P.A. SAMPLE // LB 41D01
KRC SAMPLE // 41319
MATRIX FISH
SAMPLE RECEIVED 11/14/79
L NURGANIC RESULTS
11 A R A _M G T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LKAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unJess otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL CC/MS SCAN
CONCENTRATION (PPB)
1100
420
400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC DATA: B41319 #859
82/12/89 14:13:89 CALI: CAL212 #1
SAMPLE: B41319 EPA FISH
RANGE: G 1,1409 LABEL: N 1, 4.8 QUAN: A 0, 1.0 BASE: U 20, 3
789
SCANS 1 TO 1400
400
13:20
600
20:80
26:40
1000
33:20
4224
1160
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D02
ERG SAMPLE // 41320
MATRIX FISH
SAMPLE RECEIVED 11/14/79
I MORGAN1C RESULTS
!' A _R A M E T E
ARSENIC
CADMIUM
' COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
(PPB)
3900
710
260
OTHER COMPOUNDS
PCB's
780
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
100.0-1
DATA: B41328 #1
CALI: CAL28 #1
RIC
92/12/88 17:14:80
SAMPLE: B41320 EPA FISH
RANGE: G 1,1400 LABEL: N L 4.0 QUAN: A 0, 1.0 BASE: U 20, 3
913
SCANS
1 TO 1409
7488
400
13:20
600
29:00
800
26:40
1000
33:26
1206
40:06
1406 SCAN
46:46 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
K.P.A. SAMPLE // LB 41C03
KRG SAMPLE // 41321
MATRIX FISH
SAMPLK RECEIVED LI/.1.4/79
INORGANIC RESULTS
1' A R A M R T IE R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCK NTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(PPB)
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
3400
710
260
OTHER COMPOUNDS
PCB's
450
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.9-1
RIC
40
RIC DATA: B41321 #1
82/12/38 15:14:88 CALI: CAL28 #1
SAMPLE: B41321 EPA FISH
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
911
823
658
SCANS
1 TO 1488
4464
1157
280
6:48
688
28:88
26:48
1888
33:28
1288
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783N15SX
K.P.A. SAMPLE // LB 41DQ4
I'RG SAMPLE 0
41322
MATRIX FISH
SAMPLE RKGEIVED LI/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
GADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
CONG E.N.I RATION (ppu)
2000
3200
560
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
108.8-
RIC DATA: B41322 #1
82/12/88 8:56:89 CALI: CAL212 #1
SAMPLE: 641322 EPA FISH
RANGE: G 1,1488 LABEL: N 1, 4.8 QUAN: A 8, 1.8 BASE: U 28, 3
784
SCANS 1 TO 1490
RIC
1888
33:20
4838
1268
48:89
1408 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
K.I'.A. SAMPLE // LB 41D05
KRG SAMPLE // 41323
MATRIX FISH
SAMPLE Kl-CEIVED LI/.1.4/79
INURGANIC RESULTS
PARA M K T E_ R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
C P_ N C K N T R A T !_ 0 N (PPB)
2400
2100
740
OTHER COMPOUNDS
PCB's
60
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/12/88 11:12:88
SAMPLE: B41323 EPA FISH
RANGE: G 1,1488 LABEL:
DATA:
CALI:
B41323 #861
CAL212 #1
SCANS
1 TO 1400
N 1, 4.8 QUAN: A 8, 1.8
100.8-1
BASE: U 20,
917
7936
1178
RIC
26:40
1800
33:28
1208
40:80
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - L1783NBSX
K.I'.A. SAMPLE // LB 41DQ6
KRU SAMPLE // 41324
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARA M R T E R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL CC/MS SCAN
P. N C EI iN 1; R A T £ 0 N (PPB)
120
310
180
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/12/80 13:19:00
SAMPLE: B41324 EPA FISH
RANGE: G 1/1400 LABEL:
DATA:
CALI:
B41324 #1
CAL28 11
SCANS 1 TO 1408
N 1, 4.0 QUAN: A 8,
100.0-1
1.0 BASE: U 20,
829
3684
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
li.P.A. SAMPLE // LB 41D07
I'RG SAMPLE // 41325
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INURGANIC RESULTS
!!. A R A ?! E I
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
7. MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/.MS SCAN
CO^C E.NTRATJ.ON (pPB)
800
520
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
100.9-
RIC
RIC DATA: B41325 #1
82/12/80 19:20:99 CALI: CAL2FEB 13
SAMPLE: B41325 EPA FISH
RANGE: G 1,1400 LABEL: N 1, 4.8 QUAN: A 0, 1.9 BASE: U 20, 3
636
SCANS
1 TO 1400
2349
26:40
1900
33:20
1290
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - Q783NBSX
•;.P.A. SAMPLE // LB 41D08
•:RG SAMPLE // 41326
MATRIX FISH
SAMPLE RECEIVED ll/J/i/79
INORGANIC RESULTS
l> ARAM ]•. T E R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
T[N
ZINC
% MOISTURE
C O N C !•: N T R A T I () N
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
CONG E N T RATION (pp»)
490
1200
OTHER COMPOUNDS
HEXANEDIOIC ACID, bis (1-METHYL PROPYL) ESTER
14800
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/12/89 29:28:90
SAMPLE: B41326 EPA FISH
RANGE: G 1,1488 LABEL:
N 1* 4.8 QUAN: A
10W.8-]
0, 1.8
798
DATA: 841326 #1
CALI: CAL28 tl
BASE: U 20, 3
SCANS 1 TO 1408
28544
RIC
911
49
494
298
6:48
408
13:28
630
20:08
800
26:48
1880
33:28
1288
40:88
1400 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - LI783NBSX
K.I'.A. SAMPLE // LB 41D09
KRC SAMPLE // 41327
MATRIX __ FISH
SAMPLE RECEIVED 11/I/•//"-
1NURGANIC RESULTS
I' A R A M F, T E R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LKAD
MliRCURY
SELENIUM
TIN
ZINC
7, MOISTURE
CONCENTRATION
Results reported In
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL CC/MS SCAN
C 0 N C E N T R A T I 0 N
580
680
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
108.8n
RIC
RIC DATA: B4132? #1
82/12/88 21:27:88 CALI: CAL28 #1
SAMPLE: B41327 EPA FISH
RANGE: G 1.1488 LABEL: N 1, 4.8 QUAN: A 8; 1.8 BASE: II 28, 3
989
SCANS 1 TO 1408
2432
688
28:88
888
26:48
1888
33:28
1288
40:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - E1783NBSX
K.I'.A. SAMPLE // LB 41D10
ERG SAMPLE // 41328
MATRIX FISH
SAMPLE RECEIVED Ll/l/i//l>
INOKGANIC RESULTS
I' A R A M !•: T E R
ARSENIC
CADMIUM
COBALT
COI'PER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
0 N C ENTRATJ.ON (PPB)
790
360
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/12/88 22; 27: 00
SAMPLE: B41328 EPA FISH
RANGE: G 1,1400 LABEL: N
1, 4.0 QUAN: A
DATA: B41328 #1
CALI: CAL2FEB #3
0, 1.0 BASE: U 20, 3
827
SCANS
1 TO 1400
4664
RIC
600
20:00
800
26:40
33:20
1200
40:08
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
K.P.A. SAMPLE ffi LB 41D11
ERG SAMPLE 9 41329A
MATRIX FISH
SAMPLE RECEIVED II/.14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
EASE NEUTRAL GC/MS SCAN
CONG ENTRATJ_OJ* (ppfl)
560
2000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
02/13/30 16:41:90
SAMPLE: B41329A EPA FISH
RANGE: G 1,1460 LABEL: N 1, 4.0
DATA:
CALI:
B41329A #1
CAL213 13
U 20, 3
SCANS 1 TO 1409
5280
26:40
1000
33:20
1200
40:08
1400 SCAN
46:40 TINE
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
•.P.A. SAMPLE // LB 41D11
•:RG SAMPLE // 41329B
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAMETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
7. MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
HEXACHLOROBENZENE
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
BASE NEUTRAL GC/MS SCAN
]* (ppfi)
1500
950
17500
OTHER COMPOUNDS
NONANEDIOIC ACID, bis (2-ETHYL HEXYL) ESTER
212000
ENVIRONMENTAL RESEARCH OROUf, INC.
-------
RIC
62/11/86 20:45:06
SAMPLE: B41329B EF
RANGE: G 1,1408
* FISH
LABEL: N
1, 4.0 QUAN: A
100.0-1
0, 1.0
798
DATA: B41329B «1
CALI: CAL211 #3
BASE: U 20, 3
SCANS 1 1U 14UU
RIC
£57 . 733.
260192
863
•1128
1306
I
200
6:40
400
13:20
I
606
20:00
r
890
26:40
1060
33:20
I
1200
48:08
"1
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D12
ERG SAMPLE // 41330
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
£ARAM_ETER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
EASE NEUTRAL GC/MS SCAN
N (PPB)
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
FLUORANTHENE
ETHYL HEXYL PHTHALATE
20000
1700
190
5800
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
92/96/88 14:18:98
SAMPLE:
RANGE: G 1,1480
LABEL: N L 4.8 QUAN: A
108.8-1
DATA: B41339 #1
CALI: CAL3288 «1
0, 1.8 BASE: U 28, 3
324
SCANS 1 TO 1488
RIC
458
517
1598
• i"
^ .. KJ*
288
6:48
488
13:28
I
688
28:88
759
692JL
19368
872
916'
1868
1981 f\ 11W. •J249-'
1356-
26:48
1888
33:28
I
1286
48:88
1488 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D13
ERG SAMPLE // "41331
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P_ARAME_T_ER
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
PYRENE
ETHYL HEXYL PHTHALATE
BENZO (a) ANTHRACENE
CHRYSENE
BASE NEUTRAL GC/MS SCAN
CONCENTRATION (PPB)
1100
640
970
66000
640
640
OTHER COMPOUNDS
DIETHYL PHTHALATE
DIBUTYL PHTHALATE
PYRENE
ETHYL HEXYL PHTHALATE
BENZO (a) ANTHRACENE
CHRYSENE
1100
640
970
66000
640
640
OTHER COMPOUNDS
NONANEDIOIC ACID, bis (2-ETHYL HEXYL) ESTER
6000
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
92/98/89 11:98:99
SAMPLE: B41331
RANGE: G 1,1499
LABEL: N 1, 4.9 QUAN: A
100.9-1
DATA: B41331 #1
CALI: CAL32998FEB #2
9, 1.9 BASE: U 29, 3
837
SCANS 1 TO 1499
RIC
192768
1128
899
26:49
1996
33:29
1209
49:99
1499 SCAN
46:49 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D14
ERG SAMPLE // 41332
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P^ARAME^TiER.
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
EASE NEUTRAL GC/MS SCAN
(ppR)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
1600
23000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH CROUP, INC.
-------
RIC
02/13/88 11:20:90
SAMPLE: B41332 EPA FISH
RANGE: G 1,1400 LABEL:
N 1, 4.0 QUAN: A
100.0-1
0, 1.0
797
DATA: 841332 #1
CALI: CAL213 #3
BASE: U 20, 3
SCANS
1 TO 1480
62283
RIC
•530
657
Ju
863
1172
918
"U84
'••1234 •»• 1833
T
1280
40:88
280
6:48
400
13:20
608
20:88
26:40
1008
33:28
"1
1488
46:48
SCAN
TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB41D16
ERG SAMPLE // 41334
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
_PARAMIETE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND ,
BASE NEUTRAL GC/MS SCAN
Ni (PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
720
20000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/13/89 18:49:08
SAMPLE: B41334 EPA FISH
RANGE: G 1,1400 LABEL: N
1, 4.0 QUAN: A
100.0-1
0, 1.9
738
DATA: B41334 HI
CALI: CAL213 #3
BASE: U 20, 3
SCANS 1 TO 1400
RIC
45
462
205312
865
,922
;A. L 1833 . 1124
1272
I
200
6:40
400
13:20
600
20:00
800
26:40
F
1000
33:20
1200
40:00
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE
ERG SAMPLE //
LB 41D17
41335
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P.A_RAME:TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
EASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
770
9400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
02/13/80 13:23:88
SAMPLE: B41335 EPA FISH
RANGE: G 1/1480 LABEL: N
1, 4.8 QUAN: A 8,
180.0-1
1.0
863
DATA: B41335 #863
CALI: CAL213 *3
BASE: U 20, 3
SCANS
1 TO 1400
RIC
38720
48
200
6:40
T
400
13:20
1200
927
989
'1/V
1-664 -H43
". .1286
606
28:80
26:48
1880
33:20
1
1200
40:80
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D18
ERG SAMPLE // 41336
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
P.ARAME_TE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
7, MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
DI-n-OCTYL PHTHALATE
800
4200
4400
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIL
82/13/88 19:42:98
SAMPLE: B41336 EPA FISH
RANGE: G 1,1489 LABEL:
uATA:
CALI:
Wl
CAL213 *3
1 lu 14eo
N 1, 4.8 GUAN: A 8,
186.8-1
1.8
807
BASE: U 28, 3
RIC
666
472
• 741,-
n. ./V «_/S
70496
1487
"32
1362
208
6:40
13:28
688
28:08
26:48
1888
33:28
I
1288
40:08
I
1408 SCAN
46:48 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D19
ERG SAMPLE // 41337
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAME_T_ER_
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONCENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
BASE NEUTRAL GC/MS SCAN
(ppB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
DI-n-OCTYL PHTHALATE
410
5600
610
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
82/13/88 15:23:88
SAMPLE: B41337 EPA FISH
RANGE: G 1,1489 LABEL:
4.8 QUAN: A
100.8-1
0, 1.8
791
uriTA; ot133r wi
CALI: CAL213 t3
BASE: U 20, 3
^CAn
14U,
RIC
46
672
fl-.: :;
J!
10496Q
857
1498
1385
280
6:40
480
13:20
680
20:00
880
26:40
33:20
1200
40:88
1400 SCAN
46:40 TIME
-------
ANALYTICAL RESULTS
U.S.E.P.A. - I1783NBSX
E.P.A. SAMPLE // LB 41D20
ERG SAMPLE // 41338
MATRIX FISH
SAMPLE RECEIVED 11/14/79
INORGANIC RESULTS
PARAM.ETE_R
ARSENIC
CADMIUM
COBALT
COPPER
CHROMIUM
LEAD
MERCURY
SELENIUM
TIN
ZINC
% MOISTURE
CONG ENTRATION
Results reported in
unless otherwise noted.
ORGANIC RESULTS
PRIORITY POLLUTANTS
COMPOUND
EASE NEUTRAL GC/MS SCAN
(PPB)
DIBUTYL PHTHALATE
ETHYL HEXYL PHTHALATE
360
18000
OTHER COMPOUNDS
NONE
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
RIC
82/13/88 12:24:88
SAMPLE: B41338 EPA FISH
RANGE: G 1,1488 LABEL:
DATA:
CALI:
B41338 #1
CAL213 *3
SCANS
1 TO 1488
N 1.. 4.0 QUAN: A 8, 1.8
188.0-1
BASE: U 28,
863
RIC
656
46
588
268
6:48
408
13:28
688
28:88
31236
977
1182
1179
/\ 1243
1338
I
1000
33:28
I
1288
48:88
I
1488 SCAN
46:48 TIME
-------
QUALITY CONTROL RESULTS
PROJECT EPA - BIO ASSAY
PARAMETER % Moisture (% by weight)
DETECTION LIMIT (WATER)
(SEDIMENT)
ERG //
40391
SAMPLE I.D.
LB34C17
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Sediment
VALUE A
20.6
VALUE B
20.6
%
DEVIATION
0
AVG.
VALUE
20.6
SPIKE
INCREMENT
CONTROL STANDARDS
TYPE -
SAMPLE
SPIKE
%
RECOVERY
ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIDGE VIEW, ILLINOIS 604S5 • 312 430 1111
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER CADMIUM
DETECTION LIMIT (WATER) .003 rag/1
(SEDIMENT). 71 mg/kg
ERG »
41278
41279
40360
40362
40395
44103
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
-.001
.005
.001
.000
.235
8.28
VALUE B
-1002
.003
.000
.001
0
7.86
2
DEVIATION
67
50
200
200
200
5.2
AVG.
VALUE
-.0015
.004
.0005
.0005
.1175
8.07
SPIKE
INCREMENT
.0625
.0625
.050
.050
SAMPLE
SPIKE
.055
.063
.042
.039
i
2
RECOVERY
90
94
83
77
CONTROL STANDARDS
TYPE - NBS 1645
-.001 mg/1 .001 mg/kg
-.001 mg/1 .001 mg/kg (Actual Value 10.2 ug/g)
-.001 mg/1 .002 mg/kg
-.001 mg/1 6.35
.000 mg/1 6.58
-.001 mg/1
ENVIRONMENTAL RESEARCH GROUP, INC • 7303 W 90TH STREET • BRIDGE VIEW, ILLINOIS 60455 • 31 2 430 111!
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER CHROMIUM
DETECTION LIMIT (WATER) .005 mg/1
(SEDIMENT) 1.2 mg/kg
ERG i
41278
41279
40360
40362
40395
44103
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
.001
.001
.003
.001
.4761
121
VALUE B
.001
.001
.004
.001
.476
121
%
DEVIATION
0
0
28
0
0
0
•
AVG.
VALUE
.001
.001
.0035
.001
.476
121
SPIKE
INCREMENT
.125
.125
.100
.100
CONTROL STANDARDS
TYPE - NBS 1645
SAMPLE
SPIKZ
.093
.090
.066
.064
%
RECOVERY
74
71
62
63
.002 mg/1 .000 mg/kg
.003 mg/1 .001 mg/kg (Actual Value 2.96%)
.002 mg/1 -.002 rag/kg
.000 rag/1 ^.J/A
.001 mg/1 2-33Z
.001 rag /I
ENVIRONMENTAL RESEARCH CROUP. INC • 7303 W 90TH STREET • BRIDGE VIEW ILLINOIS 60455 • 312 430 1H1
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER COBALT
DETECTION LIMIT (WATER) .005 rag/1
(SEDIMENT) 1.2 mg/kg
ERG //
41278
41279
40360
40362
40395
43739
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
.008
.005
.000
.001
.238
10.2
VALUE B
.005
.008
.001
.000
.238
11.5
%
DEVIATION
.46
46
200
200
0
12
AVG.
VALUE
.0065
.0065
.0005
.0005
.238
10.85
SPIKE
INCREMENT
CONTROL STANDARDS
TYPE -
NBS 1645
SAMPLE
SPIKE
%
RECOVERY
.000 mg/1 .001 mg/kg
-.002 mg/1 -.002 mg/kg (Actual Value 8ug/g)
.000 mg/1 -.001 mg/kg
.001 mg/1 5.4
-.002 mg/1 5.5
-.001 mg/1
L_ ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIOGEVIEW. ILLINOIS 60455 «312 430-1111
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER COPPER
DETECTION LIMIT (WATER) .005 me/1
(SEDIMENT) 1.2 mg/kg
ERG //
41278
41279
40360
40362
40395
44103
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
.000 mg/1 .001 mg/kg
.000 rag/1 .002 mg/kg
.002 mg/1 .002 mg/kg
.000 mg/1
.000 mg/1
.001 mg/1
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
.010
.008
.006
.005
6.7
699
VALUE B
.013
.006
.006
.006
6.7
708
%
DEVIATION
26
28
0
18
0
1.3
AVG.
VALUE
.0115
.007
.006
.0055
6.7
703.5
SPIKE
INCREMENT
.125
.125
.100
.100
X
CONTROL STANDARDS
TYPE - NBS 1645
(Actual Value 109 ug/g)
99.3
91.1
SAMPLE
SPIKE
.m
.125
.086
.080
%
RECOVERY
81
94
80
74
ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIDGE VIEW ILLINOIS 60455 «312 430 1111
-------
QUALITY CONTROL RESULTS
PROJECT EPA - BIO ASSAY
PARAMETER LEAD
DETECTION LIMIT (WATER) .010 mg/1
(SEDIMENT) 2.5 mg/kg
ERG 9
41278
41279
40360
40361
40395
44103
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
.013
.015
.001
.002
2.86
475
VALUE B
.010
.015
.001
-.003
2.62
440
Z
DEVIATION
26
0
0
1000
8.8
8.2
AVG.
VALUE
.0115
.015
.001
-.0005
2.74
457.5
SPIKE
INCREMENT
.125
.125
.100
.100
CONTROL STANDARDS
TYPE - NBS 1645
SAMPLE
SPIKE
.120
.130
.078
.071
%
RECOVERY
87
92
77
71
.002 mg/1 .006 mg/kg
.002 mg/1 -.001 mg/kg (Actual Value 714 yg/g)
.003 mg/1 -.005 mg/kg
.000 mg/1 585
-.002 mg/1 556
-.001 mg/1
[ ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET . BRIDGE VIEW. ILLINOIS 60455 -312 4301111
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER MERCURY
DETECTION LIMIT (WATER) .0002 mg/1
(SEDIMENT) .1 me/kg
ERG tf
40365
40361
* DONE IN
ERG //
40380
40381
40382
40383
SAMPLE I.D.
LB37C07
LB37C03
TRIPLICATE
SAMPLE I.D.
LB34C01
LB34C03
LB34C04
LB34C05
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
MATRIX
Sediment
Sediment
Sediment
Sediment
VALUE A
-.00019
-.00019
VALUE A
4.033
3.475
2.922
1.252
VALUE B
-.00019
- . 00006
VALUE B
3.422
2.825
2.322
1.451
%
DEVIATION
0
104
VALUE C
4.045
.718
2.033
1.660
AVG.
VALUE
-.00019
-.00012
% DEV.
9.2
62
19
14
SPIKE
INCREMENT
)
AVG. VALUE
3.833
2.339
2.425
1.454
CONTROL STANDARDS
TYPE - NBS 1645
SAMPLE
SPIKE
%
RECOVERY
.0004 mg/1 .01 wg Reading
.0004 mg/1 .03 yg Reading (Actual Value 1.1 Mg/g)
.0003 mg/1 .00 pg Reading
.0004 mg/1 .01 yg Reading 1.14
.0002 mg/1 .01 vig Reading 1.10
.0004 mg/1 .01 pg Reading 1.14
.0001 mg/1
.0001 mg/1
ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIDGEVIEW ILLINOIS 60455 »312 430 1112
-------
QUALITY CONTROL RESULTS
PROJECT trA - BJ.U A&&AI
PARAMETER TIN
DETECTION LIMIT (WATER) -08 mg/1
(SEDIMENT) 19 mg/ke
ERG //
41278
41279
40360
40362
40395
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
REAGENT BLANKS
WATER SEDIMENT
.00 mg/1 .04 mg/kg
-.03 mg/1 .01 mg/kg
-.02 mg/1 .02 mg/kg
-.02 mg/1
.00 mg/1
-.01 mg/1
MATRIX
Water
Water
Water
Water
Fish Food
VALUE A
.10
.00
.02
.01
32.6
VALUE B
.075
-.01
.01
.04
42.2
%
DEVIATION
28
200
67
120
26
AVG.
VALUE
.0875
-.005
.015
.025
37.4
SPIKE
INCREMENT
CONTROL STANDARDS
TYPE -
SAMPLE
SPIKE
%
RECOVERY
ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIOGEVIEW ILLINOIS 60455 »312 430 1111
-------
PROJECT EPA - BIO ASSAY
QUALITY CONTROL RESULTS
PARAMETER ZINC
DETECTION LIMIT (WATER) .005 mg/1
(SEDIMENT)
ERG 9
41278
41279
40360
40362
40395
44103
SAMPLE I.D.
LB40C01
LB40C02
LB37C02
LB37C04
LB39C501
Not EPA
REAGENT BLANKS
WATER SEDIMENT
MATRIX
Water
Water
Water
Water
Fish Food
Sediment
VALUE A
.009
.008
.007
.005
44.8
653
VALUE B
.006
.005
.006
.005
42.2
657
I
DEVIATION
40
46
15
0
6.0
.61
AVG.
VALUE
.0075
.0065
.0065
.005
43.5
655
SPIKE
INCREMENT
.125
.125
.100
.100
CONTROL STANDARDS
TYPE - NBS 1645
SAMPLE
SPIKE
.118
.130
.080
.082
%
RECOVERY
88
99
74
77
.000 mg/1 -.004 rag/kg
-.001 rag/1 -.007 mg/kg (Actual Value 1720 ug/g)
.002 mg/1 -.008 mg/kg
.000 mg/1 1009
.001 mg/1 1086
.001 mg/1
ENVIRONMENTAL RESEARCH GROUP. INC • 7303 W 90TH STREET • BRIDGEVIEW. ILLINOIS 60455 • 312 430 1 112
-------
QUALITY CONTROL RESULTS
PROJECT EPA - BIO ASSAY
PARAMETER ARSENIC
DETECTION LIMIT (WATER) .5 pg/1
(SEDIMENT)
ERG it
40365
40375
41278
41287
40385
SAMPLE I.D.
LB37C07
LB37C017
LB40C01
LB40C10
LB34C08
MATRIX
Water
Water
Water
Water
Sediment
VALUE A
.374
0
.781
0
12.0
VALUE B
.374
0
1.17
0
9.7
DEVIATION
0
0
40
0
21
AVG.
VALUE
.374
0
.975
0
10.8
SPIKE
INCREMENT
5.0
5.0
5.0
5.0
SAMPLE
SPIKE
7.66
4.86
6.63
5.73
RECOVERY
145
97
113
115
REAGENT BLANKS
WATER
SEDIMENT
CONTROL STANDARDS
TYPE -
0 Ug
0 Ug
0 Ug
ENVIRONMENTAL RESEARCH GROUP. INC • 7303W 90TH STREET .BRIOGEVIEW. ILLINOIS 60455 »312 430 1111
-------
QUALITY CONTROL RESULTS
PROJECT EPA - BIO ASSAY
PARAMETER SELENIUM
DETECTION LIMIT (WATER)
1.0 ug/1
(SEDIMENT)
ERG //
40365
40375
41278
41287
40385
SAMPLE I.D.
LB37C07
LB37C017
LB40C01
LB40C10
LB34C08
MATRIX
Water
Water
Water
Water
Sediment
VALUE A
.794
.635
2.29
.666
3.6
VALUE B
0
.953
1.31
.666
2.2
X
DEVIATION
200
40
54
0
43
AVG.
VALUE
.379
.794
1.80
.666
2.8
SPIKE
INCREMENT
5.0
5.0
5.0
5.0
SAMPLE
SPIKE
4.45
3.18
5.57
4.33
%
RECOVERY
81
48
75
73
REAGENT BLANKS
WATER
SEDIMENT
CONTROL STANDARDS
TYPE - ______
0 ug
ENVIRONMENTAL RESEARCH CROUP. INC • 7303 W 90TH STREET . BRlOGEVlEK ILLINOIS 60455 *312 430 1111 |
-------
QUALITY CONTROL COMMENTARY
BIO ASSAY
GENERAL
This project involved analysis of water, sediment, fish food and fish samples. A
limited quantity of all sample matrices were provided by the EPA for analysis. A
list of parameters indicating the priority of analysis to be completed, was pro-
vided by the EPA due to the lack of sufficient sample quantities to complete the
entire list of parameters originally requested.
Quality control was performed on all analyses that were reported, but due to the
lack of sample quantity, there was little or no sample left to reanalyze samples
with questionable results indicated by the quality control statistics.
% MOISTURE - (15 Sediments)
One (1) duplicate was run and was within acceptable % deviation range.
CADMIUM - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run, only One (1) sample was above the detection
limit and had a high % deviation but, was in a low analytical range. Four (4)
water spikes were run with an 86% recovery average. One (1) fish food duplicate
was run and was below the detection limit. One (1) sediment duplicate on a non-
EPA sample was run and was within acceptable % deviation range.
NBS SR 1645 - Actual Value - 10.2 ug/g - Average Value Found - 6.4 ug/g -
Average % Recovery - 63%
CHROMIUM - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run all were below the detection limit. Four (4)
water spikes were run with an average of 68% recovery. One (1) fish food dupli-
cate was run and was below the detection limit. One (1) sediment duplicate on
a non-EPA sample was run and was within acceptable % deviation range.
NBS SR 1645 - Actual Value 2.96% - Average Value Found 2.36% - Average %
Recovery - 80%
COBALT - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run all were below the detection limit. Mixed
spike solution did not contain cobalt, no spikes run. One (1) fish food dupli-
cate was run and was below the detection limit. One (1) sediment duplicate on
a non-EPA sample was run and was slightly above acceptable % deviation range, but
only at 12% in a low analytical range.
NBS SR 1645 - Actual Value 8ug/g - Average Value Found 5.45 ug/g - Average
% Recovery - 68%
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
QUALITY CONTROL COMMENTARY
BIO ASSAY
COPPER - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run, some high % deviation but, in a low analyti-
cal range. Four (4) water spikes were run with an average of 82% recovery. One
(1) fish food duplicate was run and was within acceptable % deviation range. One
(1) sediment duplicate on a non-EPA sample was run and was within acceptable %
deviation range.
NBS SR 1645 - Actual Value 109 ng/g - Average Value Found - 95.2 yg/g -
Average % Recovery -87%
LEAD - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run, two (2) are within acceptable 7, deviation
range and two (2) have high X deviations but, are either below or near the det-
ection limit. Four (4) water spikes were run with an average of 82% recovery.
One (1) fish food duplicate was run within acceptable % deviation range. One (1)
sediment duplicate on a non-EPA sample was run within acceptable % deviation
range.
NBS SR 1645 - Actual Value 714 ng/g - Average Value Found 570 ug/g - Average
% Recovery - 80S?
MERCURY - (41 Water Samples, 15 Sediment Samples)
Two (2) water duplicates were run both were below the detection limit. No spikes
were run on water. Four (4) sediments were chosen randomly, as all were done in
triplicate. High % relative s.d. were found, but I believe this deviation is to
be expected for the methodology used and is the reason for requiring triplicate
analysis.
NBS SR 1645 - Actual Value 1.1 ug/g - Average Value Found - 1.13 pg/g - Average
% Recovery - 102%
TIN - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run, all below the detection limit. Mixed spike
solution did not contain tin, no spikes run. One (1) fish food duplicate was run
with a high % deviation, but low analytical range for parameter and matrix envolved.
No NBS reference standard available.
ZINC - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run with high % deviations, but all were in a low
analytical range. Four (4) water spikes were run with an average of 84% recovery.
One (1) fish food duplicate was run within acceptable % deviation range. One (1)
sediment duplicate on a non-EPA sample was run within acceptable % deviation range.
NBS SR 1645 - Actual Value 1720 jjg/g - Average Value Found 1047 ug/g - Average
% Recovery - 61%
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
QUALITY CONTROL COMMENTARY
BIO ASSAY
* ARSENIC - (41 Water Samples, 15 Sediment Samples)
Four water duplicates were run, one (1) % deviation high, but in a low analytical
range. Four (4) water spikes were run with an average of 118% recovery. One (1)
sediment duplicate was run and had a high % deviation at 21%.
No NBS reference standard available.
* SELENIUM - (41 Water Samples, 15 Sediment Samples)
Four (4) water duplicates were run, high % deviations below or near detection
limit. Four (4) water spikes were run with an average of 69% recovery. One (1)
sediment duplicate was run with a high % deviation, but in a low analytical range.
No NBS reference standard available.
* The reproducibility and spike recovery of As and Se should
be looked at in light of recent EPA interlaboratory check
sample statistics for low level reference samples.
(WPOQ4) 4/27/79
As Se
(Real Value 18 ppb) (Real Value 3.5 ppb)
Warning limits - 5.4 - 30 Warning limits - 0 - 9.79
Acceptable limits - 1.3 - 34.2 Acceptable limits - 0 - 11.7
(WP005) 5/10/79
As
(Real Value 22 ppb)
Warning limits - 11.3 - 31.7
Acceptable limits - 7.89 - 35.2
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
U.S.E.P.A. 11783 NBSX
GC/MS QUALITY CONTROL
ALL SCANS - BASE NEUTRAL
DUPLICATE COMPARISONS
INJECTION A
INJECTION B
SAMPLE NUMBER
40345
(Fish)
40351
(Fish)
40355
(Fish)
40385
(Sediment)
40388
(Sediment)
COMPOUND
Dibutyl Phthalate
Ethyl Hexyl
Phthalate
Dibutyl Phthalate
Ethyl Hexyl
Phthalate
CONG. (PPB)
220
2300
580
18000
Dibutyl Phthalate 160
Ethyl Hexyl Phthalate 2700
Hexachlorobenzene 130*
Phenanthrene 130
Anthracene 130
Dibutyl Phthalate 50
Fluoranthene 160
Pyrene 170
Ethyl Hexyl Phthalate 1400
Chrysene 30
Benzo (a) Anthracene 30
1,4 Dichlorobenzene 2900
Hexachlorobenzene 20*
Phenanthrene 530
Anthracene 530
Dibutyl Phthalate 220
Fluoranthene 780
Pyrene 780
Ethyl Hexyl Phthalate 1700
Chrysene 380
Benzo (a) Anthracene 380
Benzo (k) Fluoranthene 220*
COMPOUND
Naphthalene
Hexachlorobenzene
Ethyl Hexyl
Phthalate
Dibutyl Phthalate
Butyl Benzyl
Phthalate
Ethyl Hexyl
Phthalate
Dibutyl Phthalate
Ethyl Hexyl
Phthalate
Phenanthrene
Anthracene
Dibutyl Phthalate
Pyrene
Ethyl Hexyl
Phthalate
CONG. (PPB)
410*
110*
3100
1900
12000
1100
280
1300
20
20
70
20
740
1,4 Dichlorobenzene 2700
Phenanthrene 230
Anthracene 230
Dibutyl Phthalate 60
Fluoranthene 440
Pyrene 490
Ethyl Hexyl
Phthalate 1100
Chrysene 150
Benzo (a) Anthracene 150
*Please refer to correspondence PE/ES, 4/8/80
ENVIRONMENTAL RESEARCH GROUP, INC.
-------
CG/MS QUALITY CONTROL
INJECTION A
SAMPLE NUMBER
41285
(Water)
41288
(Water
41299
(Fish)
INJECTION B
41309
(Fish)
41314
(Fish)
41329
(Fish)
COMPOUND
Ethyl Hexyl
Fhthalate
Ethyl Hexyl
Fhthalate
Hexachlorobenzene
Dibutyl Phthalate
Ethyl Hexyl
Phthalate
Dibutyl Phthalate
Ehtyl Hexyl
Phthalate
Dibutyl Phthalate
Ehtyl Hexyl
Phthalate
Dibutyl Phthalate
Ehtyl Hexyl
Phthalate
CONG. (PPB)
100
53
380
2700
6200
2100
1700
670
600
560
2000
COMPOUND
Ethyl Hexyl
Phthalate
Ethyl Hexyl
Phthalate
CONG. (PPB)
79
67
Hexachlorobenzene 1900
Dibutyl Phthalate 8000
Butyl Benzyl
Phthalate 2600
Ethyl Hexyl
Phthalate 6300
Dibutyl Phthalate 5000
Ethyl Hexyl
Phthalate 1200
Dibutyl Phthalate 610
Ethyl Hexyl
Phthalate 270
Dibutyl Phthalate 950
Ehtyl Hexyl
Phthalate 17500
Chromatograms are included with regular data set.
BLANKS
Procedure blanks typically showed only internal standards, with trace concentrations
of phthalates. Typical blank values are shown here; the chroraatograms are found
below.
B Blank // 5 - 2/13/80
Dibutyl Phthalate
Bis (Ethyl Hexyl) Phthalate
B Blank //I - 2/11/80
Dibutyl Phthalate
Bis (Ehtyl Hexyl) Phthalate
730 ppb
700 ppb
670 ppb
300 ppb
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
188.0-
RIC
RIC DATA: BBLK5 #1
82/13/88 17:43:00 CALI: CAL213 #3
SAMPLE: BBLK5 EPA FI5H
RANGE: G 1,1400 LABEL: N 1, 4.0 QUAN: A 0, 1.0 BASE: U 28, 3
653
SCANS 1 TO 1400
917
3016
1360
680
20:08
26:40
1008
33:20
1280
40:88
1400 SCAN
46:48 TIMt
-------
RIC
02/11/88 16:37:88
SAMPLE: BBLK1 EPA FISH
RANGE: G L1400 LABEL:
DATA:
CALI:
BBLK1 «1
CAL2FEB #3
SCANS 1 TO 1488
N 1, 4.9 QUAN: A
180.0-1
8, 1.8
732
BASE: U 28, 3
RIC
44
582
288
6:40
~r
400
13:20
164364
858
680
28:08
26:48
1088
33:20
1280
40:00
1488 SCAN
46:40 TIME
-------
E.P.A. 11783 NBSX
GC/MS QUALITY
ALL SCANS - BASE NEUTRAL
SPIKE STATISTICS
SPIKE
I.D. DATE COMPOUND
#2R Water 1/25/80 Hexachloroe thane
2,4 -Dinetrotoluene
Pyrene
Benzo (a) Anthracene
Composite 1/30/80 Hexachloroethane
Water 2,4 -Dinitrotoluene
(41295, 96, Pyrene
97) Benzo (a) Anthracene
//2 Fish 2/9/80 Hexachloroethane
2,4 -Dinitrotoluene
Pyrene
Benzo (a) Anthracene
#3 Fish 2/12/80 Hexachloroethane
2, 4-Dinitrotoluene
Pyrene
Benzo (a) Anthracene
#5R Fish 2/13/80 Hexachloroethane
2,4 -Dinitrotoluene
Pyrene
Benzo (a) Anthracene
Chromatograms are found below.
CONTROL
ORIGINAL
CONCENTRATION
430 ppb
490 ppb
460 ppb
410 ppb
710 ppb
810 ppb
760 ppb
690 ppb
122 mg/kg
138 mg/kg
130 rag/kg
118 mg/kg
145 rag/kg
164 rag/kg
155 mg/kg
140 mg/kg
130 mg/kg
146 mg/kg
138 mg/kg
125 mg/kg
DETECTED
CONCENTRATION
110 ppb
430 ppb
330 ppb
330 ppb
430 ppb
1000 ppb
770 ppb
750 ppb
52.7 mg/kg
123 mg/kg
118' mg/kg
101 mg/kg
39 mg/kg
75 mg/kg
105 mg/kg
97 mg/kg
47.3 mg/kg
80.4 mg/kg
78.5 mg/kg
62.5 mg/kg
%
RECOVERY
26
88
72
80
61
123
101
109
43
89
91
86
27
46
68
69
36
55
57
50
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
RIC
01/25/89 18:32:08
SAMPLE: BSPK2, 3 UL + 1 UL IS
RANGE: G 1,1486 LABEL: N 1,
4.8
109.9-1
QUAN: A 8,
707
DATA: BSPK2 #1
CALI: CAL125 #1
1.0 BASE: U 28, 3
SCANS 1 TO 1490
510Q3
RIC
283
314 388
583
1181
206
6:40
400
13:29
609
29:99
1989
33:29
1299
49:99
l
1499 SCAN
46:49 TIME
-------
RIC
81/38/88 19:55:88
SAMPLE: BCOMPSPK, 3 UL + 1 UL IS
RANGE: G 1,1488 LABEL: N 1, 4.8
QUAN:
108.8-1
A 8,
722
DATA: BCOMPSPK #1
CALI: CAL138 II
1.8 BASE: U 28; 3
SCANS
1 TO I486
RIC
495
417
I
288
6:48
637
112648
838
991-L 988
1184
1249 ••••<
488
13:28
688
28:88
26:48
1886
33:28
1288
48:88
1489 SCAN
46:48 TIME
-------
RIC
82/99/88 17:22:88
SAMPLE: BSPK2 EPA FISH
RANGE: G 1,1400 LABEL:
N li 4.0 QUAN: A
100.0-1
0, 1.0
785
DATA: BSPK2 #1
CALI: CAL31JAN2 fl
BASE: U 28, 3
SCANS
1 TO U00
51520
902
RIC
556
141
A
200
6:40
I
400
13:20
658
1
862
1157
969
i • 11 n it
1249 '"135*-
I
600
20:00
800
26:40
1000
33:20
1286
48:08
I
1400 SCAN
46:40 TIME
-------
RIC
92/12/80 16:13:09
SAMPLE: BSPK3 EPA FISH
RANGE: G 1/1499 LABEL: N
1, 4.9 QUAN: A
100.8-1
0, 1.9
735
DATA: BSPK3 #559
CALI: CAL28 »1
BASE: U 29, 3
SCANS 1 TO 1490
31136
RIC
559
200
6:40
652
i
369
490
13:29
609
20:99
26:49
1900
33:29
1208
40:00
1400 SCAN
46:40 TIME
-------
RIC
82/13/89 20:41:90
SAMPLE: BSPK5R EPA FISH
RANGE: G 1/1480 LABEL:
DATA: BSPK5R #1
CALI: CAL213 #3
SCANS
1 TO 1400
N 0; 4.0 QUAN: A 0, 1.0
190.0-1
BASE:
864
U 28, 3
793
RIC
264 348 429 504
38656
913
200
6:49
T"
400
13:20
T"
606
20:00
26:40
1000
33s 21
1200
40:00
1400 SCAN
46:40 TIME
-------
U. S. ENVIRONMENTAL PROTECTION AGENCY
METHODOLOGY
ANALYTE
METHODOLOGY
REFERENCE
Cadmium, Cobalt, Chromium,
Copper Lead, Tin, Zinc
A) Water Sample Digestion
B) Sediment Digestion
C) Analysis
Arsenic (Water)
Arsenic (Soil)
Selenium (Water)
Selenium (Soil)
Mercury (Water)
Mercury (Soil)
Nitric Acid Digestion
H.O., Aqua Regia Digestion
Flame Atomic Absorption
Flameless Atomic Absorption
Neutron Activation Analysis
Flameless Atomic Absorption
Neutron Activation Analysis
Cold Vapor, Manual
Cold Vapor, Sediments
Std. Methods p. 147
ERG Procedure 11-176
Attached
EPA Manual p. 213.1,
219.1, 218.1, 220.1,
239.1, 282.1, 289.1
EPA Manual p. 206.2
Advances in Activation
Analysis
EPA Manual p. 270.2
Advances in Activation
Analysis
EPA Manual p. 245.1
EPA Manual p. 245.5
REFERENCES
1. EPA Manual for Chemical Analysis of Water and Wastes, EPA 1979.
2. Standard Methods for the Examination of Water and Wastewater, APHA 1976.
3. Advances in Activation Analysis, Lehihan and Thomson, Vol. 1, Academic Press, 1969.
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
SEDIMENT AND SLUDGE TRACE METALS DIGESTION PROCEDURE
(BLOCK DIGESTOR METHOD)
PRINCIPLE
Organic matter in sediment and sludge is destroyed by oxidation with
hydrogen peroxide. Metallic complexes are further digested by a
reflux of aqua regia under controlled temperature.
REAGENTS
(1) 15% H.02 prepare by diluting 30% H.02 1:1 with deionezed water.
(2) Aqua regia - prepare by cautiously mixing 3 parts HC1 to 1
part cone. HNO_. Prepare just before use as this mixture is
unstable.
PROCEDURE
(1) Rinse Technicon constricted neck test tubes with deionized
water. Add 5 ml of 25% HN03 and heat at 150 - 160° for
30 minutes.
(2) Rinse tubes thoroughly with deionized water.
(3) Weigh approx. 200 mg of dried sediment into the test tube.
Record sample weight to the nearest 0.1 mg on metals data
sheet. Prepare 2 NBS River Sediment Standard (SRM 1645)
and 10% of the samples in duplicate.
(4) 3 reagent blanks should be prepared with each set of
samples.
(5) Add 4 ml of 15% H-0- to each test tube and heat carefully
as the sample may boil over. Heat until effervescence
ceases.
(6) Cool the samples and add 5 ml of aqua regia to each tube.
(7) Heat at 150 - 160° C. Do not let the samples go dry.
Rinse down sides of the tubes periodically with a min-
imum amount of H-0 if spattering occurs. When fully
digested, samples should be light colored. Normally
three to four hours of digestion is sufficient.
(8) Dilute each sample to 10 ml with distilled H.O. Transfer
sample into a labeled plastic vial.
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
U. S. ENVIRONMENTAL PROTECTION AGENCY
ORGANIC (GC/MS) METHODOLOGY
Samples were prepared according to the method outlined in the "Interim Methods
for the Sampling and Analysis of Priority Pollutants in Sediments and Fish
Tissue" prepared by the U. S. Environmental Protection Agency, EMSL Laboratory,
Cincinnati, Ohio.
The fish samples were prepared by the method "Analysis of Fish for General
Organics by Solvent Extraction, P. 15.
The water samples were prepared following the methods outlined in the December 3,
1979 issue of the Federal Register.
The sediments were prepared following the above mentioned "Interim Methods."
ENVIRONMENTAL RESEARCH GROUP. INC.
-------
ENVIRONMENTAL RESEARCH GROUP INC.
117 N (MM Arm Arbcu. Michigan 48104 (313)662-3104
April 8, 1980
Dr. Emilio Sturino
U.S. Environmental Protection
Agency
Central Region Laboratory
536 S. Clark Street
Tenth Floor
Chicago, Illinois 60605
Dear Dr. Sturino:
In accordance with your letter of March 12, 1980 to Jim Bolger and your
instructions at our meeting" of March 19, 1980, I have compiled the
following information:
(1) Copies of the mass spectral and chromatographic data indicating
• the presence of chloroalkyl ethers in ERG Samples 40563, 40564, and
40801. As you can see on the enclosed chromatograms, the data
clearly indicates the presence of chloroalkyl ethers. The correct
identification should be as follows:
ERG/H 40563
Ethane, 1, T - oxybis/2-chloro 1320 PPB
Propane, 1,1'- oxybis/3-chloro
(This could be any one of several isomers) 5410 PPB
ERG0 40564
Propane, 1, T - oxybis/3-chloro 2620 PPB
ERG# 40801
Propane, 2, 2' - oxybis/1-chloro 4550 PPB
(2) A reanalysis of 20% of the raw data of the two projects 1n question.
Enclosed you will find a list of the ERG samples that were reanalyzed
and a summary of the results of this reanalysis.
Files Reanalyzed from the BASF Project
These files were reviewed from the BASF Project:
B40561, A40561, B40568, 840799, B40805, 840808, B39034
All ion count data reviewed agreed with the original data to +/- 3%. The
principal differences were several compounds which were found in the review
had been deleted from the final report to comply with the .01 mg/kg detection
limit called for in the contract. As a result of our discussions, these
compounds will be included in the final version of the report.
Inn Jil>,n ( In, HMO t li-\iliind iu/i h'rum MI u Minntupulis-Sl Paul
-------
Dr. Emilio Sturino
April 8, 1980
Page Two
Files Reanalyzed from the Bioassay Project
The following files were reanalyzed from the Bioassay Project:
841288 840379 841285 B41299 B41309 B41329 B40368
B40370 B40351 B40385A B40385B B40390 B40362 B40367
B40371 840375 B40381 B40385 B41283 B41290 B41296
B40561 B40808 B40805 B40799
As with the review of the BASF Project, all ion count data agreed with the
reported values to +/- 3%. In one sample there was a mistaken identification
of isophorone. All samples in which isophorone was reported were rechecked
and the one positive report (ERG# B40395) was deleted. The sample in question
did have the major fragment of isophorone at the correct retention time.
However, on closer examination, it became obvious that the material in
question was not isophorone. In addition, all samples that had positive
results for any priority pollutants were checked for transcription errors.
Only one error was found. In that review it was found that sample # B41320
was reported to contain 3400 PPB hexachlorobenzene. That figure should have
been 3900 PPB, and is being incorporated in the final report.
As part of our review, a careful analysis was made of the blank, spike, and
duplicate data. The following is a summary of this review.
Analysis of Blanks
Based on the data from the blanks that were run, it became evident that we
were incorporating phthalates into our samples during the preparation for
analysis. Taking this fact into consideration, we will not report any
phthalates as positive unless they exceed the 10,000 PPB level in the fish
matrices, and 1,000 PPB in the waters and sediments. In addition, considering
the small sample sizes involved in the fish and the sediments, one should view
with skepticism any phthalate values that do not exceed 20,000 PPB. This is
four times a reasonable detection limit of 5,000 PPB for a 2-10 gram initial
sample. Very low levels of the heavier PNA's (<100 PPB) were also difficult
to detect reproducibly. The total ion counts were in the 50-500 ion range,
making replicate analysis difficult.
Spike Data
The spike recoveries were excellent in the water samples and fair to very good
in the fish. The recoveries of hexachloroethane were lower in all cases than
the other compounds that were spiked into the samples.
Ann •»//>!•» (liniivn (/in/ii/ii/ Sun hiuniiuu Minneapoli\-Sl Paul
-------
Dr. Emilio Sturino
April 8, 1980
Page Three
Considering the small sample sizes encountered in the fish and sediment
samples, a reasonable detection limit at which quantification 1s reliable
is 5,000 PPB. We have, however, included data below this level for the
qualitative purpose of identifying the materials present in the sample.
In any case, wherever we detected a measurable quantity of the characteristic
ions (within the expected retention time window) of any of the compounds
suspected in this study, we have now included that data in the reports.
PCB's were identified and quantified by using an extracted ion current
profile for the characteristic ions. During the rechecking of the data,
it was discovered that two samples containing PCB's were quantified using
an ion count for the wrong ion. All positive PCB's were then rechecked.
There were no other occurances of this error. Samples 40382 and 40383
should have been reported .as containing PCB's at the following levels:
ERG# B40382 2420 PPB
ERG# 840383 1890 PPB
This'change is being incorporated in the final report.
Duplicate Data
On reviewing the duplicate data previously submitted, it appears that much
of the confusion stems from our failure to edit the report as carefully as
we should have. For example, ERG Sample #8413298 was reported to contain
hexachlorobenzene. This was a transcription error. Several other questions
were resolved as a result of the reanalysis. Sample B40385A contained 500
ions of hexachlorobenzene. This was not detected in the B injection. We
also reported 30 PPB chrysene in the A injection that was not in the B
injection. This represented a total of 130 ions at M/E 228. The
non-reproducibility of this data at two orders of magnitude below a
reasonable detection limit is real but I do not feel it is indicative
of poor performance. An additional factor that affected the replicate
data was the use of separate fish as duplicate samples, rather than
preferred method of homogenizing the entire sample and then splitting
the honogenized material for extraction.
In reviewing all the correspondence on these projects, I discovered that
my last letter to you also had several typographical errors. I have
included corrected copies of the pages that were incorrect. Having now
spent more than one month reviewing the data on these two projects, I
believe the data in its present form is a reliable representation of
the samples involved in the two projects.
•tun til,,', c/m i;o' I l,-\ i ItiiiJ Sun Frummti Minneapolis-Si Paul
-------
Dr. Emilio Sturino
April 8, 1980
Page Four
We have undergone several changes of personnel and control systems, and
increased our capacity since the completion of these projects. As a
result of these changes, we do not anticipate any further recurrences
of the problems encountered during the fulfillment of these contracts.
We have recently completed the first part of EPA Order #53342 NBSX.
I believe our performance on this is a better indicator of the type
of results you can expect from us in the future.
G*U^t_
Paul Epstein
Manager GC/MS
PP.: pa
Ann A
(Im i
( 1111 In nil
Sun Fmni i\i n
Minneapi>li\-.Sl. Paul
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ENVIRONMENTAL RESEARCH GROUP, INC
117.N. First Ann Arbor, Michigan 48104 (313)662-3104
16 April 1980
Dr. Erallio Sturino
U.S. Environmental Protection Agency
Central Regional Laboratory
536 South Clark Street, Tenth Floor
Chicago, Illinois 60608
Or. Sturino:
The following information is submitted in answer to your letter concerning
samples which your records indicate were received at ERG but for which you
have not received any data.
1. BASF project, sample number 820232. This sample was received at ERG. The
inorganic analysis was completed and reported. Our records also indicate that
the organic extraction was completed, but that the sample was not analyzed.
We are unable to locate the extracted vial and I must assume it was lost when
we moved our GC/MS equipment, which occurred at about the same time.
2. Aahtabula project, sample numbers LB34C02, LB34C07, LB34C15. LB34D15. These
samples were not received at ERG. The records technician who signed for the
shipping container did not log in the samples until after the delivery person
had left. When the samples were logged in, the fact that samples were missing
was noted and your office was contacted by telephone.
Our log-in person should not have signed without first checking the samples,
but since the containers were not damaged it was felt that all of the samples
would be present as listed.
If you have any additional questions, please feel free to contact me.
Yours truly,
Richard R. Encelewski
Operations Manager
RRE:mgl
Ann Arbor Chicago Cleveland San Francisco Minneapolis-Si. Ptuil
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