ECTION AGENCY
           OFFICE OF ENFORCEMENT
                 EPA-330/1-76-003
      Summary of Reference Methods
   tationary Source Emission Evaluations
            (40 CFR  Part 60)
FEDERAL ENFORCEMENT INVESTIGATIONS CENTER




             DENVER.COLORADO
              OCTOBER 1976

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      Environmental  Protection  Agency
           Office  of Enforcement
     SUMMARY  OF REFERENCE METHODS FOR
           EMISSION EVALUATIONS
             (40 CFR Part 60)
               October 1976
National  Enforcement Investigations Center
             Denver, Colorado

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Information in this report has
"been excerpted by NEIC from the
Code of Federal Regulations,
Title 403 Part 60, Appendix A.

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                               CONTENTS
METHOD 1  - Sample and Velocity Traverses
            for Stationary Sources  	   1

METHOD 2  - Determination of Stack Gas Velocity
            and Volumetric Flow Rate	2

METHOD 3  - Gas Analysis for Carbon Dioxide, Excess Air,
            and Dry Molecular Weight  	   3

METHOD 4  - Determination of Moisture in Stack Gases  	   4

METHOD 5  - Determination of Particulate Emissions
            from Stationary Sources   	   5

METHOD 6  - Determination of Sulfur Dioxide Emissions
            from Stationary Sources   	   6

METHOD 7  - Determination of Nitrogen Oxide Emissions
            from Stationary Sources   	   7
METHOD 8  - Determination of Sulfuric Acid Mist and
            Sulfur Dioxide Emissions from Stationary Sources  .  .   8

METHOD 9  - Visual Determination of the Opacity of Emissions
            from Stationary Sources   	   9

METHOD 10 - Determination of Carbon Monoxide Emissions
            from Stationary Sources   	  10

METHOD 11 - Determination of Hydrogen Sulfide Emissions
            from Stationary Sources   	  11

METHOD 12 - Determination of Sulfur Dioxide Emissions
            from Stationary Sources by Continuous Monitors  ...  12

METHOD 13A- Determination of Total Fluoride Emissions
            from Stationary Sources
            SPADNS Zirconium Lake Method  	  13

METHOD 13B- Determination of Total Fluoride Emissions
            from Stationary Sources
            Specific Ion Electrode Method   	  14

METHOD 14 - Determination of Fluoride Emissions
            from Pot Room Roof Monitors of Primary
            Aluminum Plants 	  15

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                39 FR 20790  June 14, 1974
                         METHOD 1
               SAMPLE AND VELOCITY TRAVERSES
                  FOR STATIONARY SOURCES
    1.1  Principle
1.2  Applicability
A sampling site and the number of
traverse points are selected to aid
in the extraction of a representative
sample.

This method should be applied only
when specified by the test procedures
for determining compliance with the
New Source Performance Standards.
Unless otherwise specified, this method
is not intended to apply to gas streams
other than those emitted directly to
the atmosphere without further
processing.

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                39 FR 20790  June 14,  1974
                         METHOD 2
            DETERMINATION OF STACK GAS VELOCITY
                 AND VOLUMETRIC FLOW RATE
                    (Type S Pi tot Tube)
    1.1   Principle      Stack gas velocity is determined
                        from the gas density and from
                        measurement of the velocity head
                        using a Type S (Stauscheibe or
                        reverse type) pi tot tube.

1.2  Applicability      This method should be applied only
                        when specified by the test procedures
                        for determining compliance with the
                        New Source Performance Standards.

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                39 FR 20790  June U3  1974
                         METHOD 3
       GAS ANALYSIS FOR CARBON DIOXIDE,  EXCESS AIR,
                 AND DRY MOLECULAR WEIGHT
    1.1   Principle      An integrated or grab gas  sample
                        is extracted from a  sampling point
                        and analyzed for its components
                        using an Orsat analyzer.

1.2  Applicability      This method should be applied only
                        when specified by the test procedures
                        for determining compliance with the
                        New Source Performance Standards.
                        The test procedure will  indicate
                        whether a grab sample or an integrated
                        sample is to be used.

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                39 FR 20790  June 14,  1974
                         METHOD 4
         DETERMINATION OF MOISTURE IN STACK GASES
    1.1   Principle
Moisture is removed from the gas
stream, condensed, and determined
volumetrically.
1.2  Applicability
This method is applicable for the
determination of moisture in stack
gas only when specified by test
procedures for determining compliance
with New Source Performance Standards.
This method does not apply when
liquid droplets are present in the
gas stream* and the moisture is
subsequently used in the determination
of stack gas molecular weight.
                        Other methods  such as  drying  tubes,
                        wet bulb-dry bulb techniques,  and
                        volumetric condensation  techniques
                        may be used.
    *  If liquid droplets are present in the  gas  stream,
       assume the stream to be saturated,  determine  the
       average stack gas temperature by  traversing according
       to Method 1,  and use a psychrometric chart to obtain
       an approximation of the moisture  percentage.

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                39 FR 20790  June 14,  1974
                         METHOD 5
          DETERMINATION OF PARTICULATE EMISSIONS
                  FROM STATIONARY SOURCES
    1.1  Principle      Particulate matter is withdrawn
                        isokinetically from the source
                        and its weight is determined
                        gravimetrically after removal  of
                        uncombined water.

1.2  Applicability      This method is applicable for
                        the determination of particulate
                        emissions from stationary
                        sources only when specified by
                        the test procedures for
                        determining compliance with
                        New Source Performance Standards.

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                39 FR 20790  June 14,  1974
                         METHOD 6
         DETERMINATION OF SULFUR DIOXIDE EMISSIONS
                  FROM STATIONARY SOURCES
    1.1   Principle
A gas sample is extracted from
the sampling point in the
stack.  The acid mist, including
sulfur trioxide, is separated
from the sulfur dioxide.  The
sulfur dioxide fraction is
measured by the barium-thorin
titration method.
1.2  Applicability
This method is applicable for
the determination of sulfur
dioxide emissions from
stationary sources only when
specified by the test procedures
for determining compliance with
New Source Performance Standards.

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                39 FR 20790  June 14,  1974
                         METHOD 7
         DETERMINATION OF NITROGEN OXIDE EMISSIONS
                  FROM STATIONARY SOURCES
    1.1   Principle
1.2  Applicability
A grab sample is collected
in an evacuated flask containing
a dilute sulfuric acid-hydrogen
peroxide absorbing solution,
and the nitrogen oxides, except
nitrous oxide, are measured
colorimetrically using the
phenoldisulfonic acid (PDS)
procedure.

This method is applicable
for the measurement of
nitrogen oxides from stationary
sources only when specified by
the test procedures for
determining compliance with
New Source Performance Standards.

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                                                            8
                39 FR 20790  June 14,  1974
                         METHOD 8
          DETERMINATION OF SULFURIC ACID MIST AND
     SULFUR DIOXIDE EMISSIONS FROM STATIONARY SOURCES
    1.1   Principle
A gas sample is extracted
from a sampling point in the
stack and the acid mist
including sulfur trioxide is
separated from sulfur dioxide.
Both fractions are measured
separately by the barium-thorin
titration method.
1.2  Applicability
This method is applicable to
determination of sulfuric
acid mist (including sulfur
trioxide) and sulfur dioxide
from stationary sources only
when specified by the test
procedures for determining
compliance with the
New Source Performance Standards.

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                39 FR 20790  June 24,  1974
                         METHOD 9
     VISUAL DETERMINATION OF THE OPACITY OF EMISSIONS
                  FROM STATIONARY SOURCES
    1.1   Principle      The relative opacity of an
                        emission from a stationary
                        source is determined visually
                        by a qualified observer.

1.2  Applicability      This method is applicable
                        for the determination of the
                        relative opacity of visible
                        emissions from stationary
                        sources only when specified
                        by test procedures for
                        determining compliance with the
                        New Source Performance Standards.

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                39 FR 20790  June 14,  1974
                         METHOD 10
        DETERMINATION OF CARBON MONOXIDE EMISSIONS
                  FROM STATIONARY SOURCES
                                                            10
    1.1   Principle
1.2  Applicability
An integrated or continuous
gas sample is extracted from
a sampling point and analyzed
for carbon monoxide (CO)
content using a Luft-type
non-dispersive infrared
analyzer (NDIR) or equivalent.

This method is applicable
for the determination of
carbon monoxide emissions
from stationary sources only
when specified by the test
procedures for determining
compliance with New Source
Performance Standards.  The
test procedures will indicate
whether a continuous or an
integrated sample is to be used.

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                                                            11
                29 FR 20790  June 14, 1974
                         METHOD 11
        DETERMINATION OF HYDROGEN SULFIDE EMISSIONS
                  FROM STATIONARY SOURCES
    1.1  Principle
1.2  Applicability
Hydrogen sulfide (HgS) is
collected from the source
in a series of midget impingers
and reacted with alkaline
cadmium hydroxide [Cd(OH)2]
to form cadmium sulfide (CdS).
The precipitated CdS is then
dissolved in hydrochloric
acid and absorbed in a known
volume of iodine solution.
The iodine consumed is a
measure of the HpS content of
the gas.  An impinger containing
hydrogen peroxide is included to
remove SOp as an interfering species.

This method is applicable
for the determination of
hydrogen sulfide emissions from
stationary sources only when
specified by the test procedures
for determining compliance with the
New Source Performance Standards.

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                                                              12
               39 FR 37016  October 16,  1974
                         METHOD 12
         DETERMINATION OF SULFUR DIOXIDE EMISSIONS
      FROM STATIONARY SOURCES BY CONTINUOUS MONITORS
    1.1  Principle
1.2  Applicability
Gases are continuously sampled
in the stack emissions and
analyzed for sulfur dioxide
by a continuously operating
emission measurement system.
Sampling may include either the
extractive or non-extractive
(in situ) approach.

This method is applicable to the
instrument systems specified by
subparts for continuously monitoring
sulfur dioxide emissions.
Specifications for continuous
measurement of sulfur dioxide are
given in terms of performance
specifications.  Test procedures are
given to determine the capability of
the measurement systems to conform
to the performance specifications
prior to approving the systems
installed by an affected facility.

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               39 FR 37016  October 16,  1974
                         METHOD ISA
         DETERMINATION OF TOTAL FLUORIDE EMISSIONS
                  FROM STATIONARY SOURCES

               SPADNS Zirconium Lake Method
                                                             13
    1.1   Principle
Gaseous and particulate fluorides
are withdrawn isokinetically from
the source using a sampling train.
The fluorides are collected in the
impinger water and on the filter
of the sampling train.  The weight
of total fluorides in the train
is determined by the SPADNS Zirconium
Lake colorimetric method.
1.2  Applicability
This method is applicable for the
determination of fluoride emissions
from stationary sources only when
specified by the test procedures for
determining compliance with
New Source Performance Standards.
Fluorocarbons, such as Freons, are
not quantitatively collected or
measured by this procedure.

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                                                            14
               39 FP 37016  October 16,  1974
                         METHOD 13B
         DETERMINATION OF TOTAL FLUORIDE EMISSIONS
                  FROM STATIONARY SOURCES

               Specific Ion Electrode Method
    1.1   Principle
Gaseous and participate fluorides
are withdrawn isokinetically from
the source using a sampling train.
The fluorides are collected in the
impinger water and on the filter
of the sampling train.  The weight
of total fluorides in the train
is determined by the specific ion
electrode method.
1.2  Applicability
This method is applicable for the
determination of fluoride emissions
from stationary sources only when
specified by the test procedures for
determining compliance with
New Source Performance Standards.
Fluorocarbons, such as Freons, are
not quantitatively collected or
measured by this procedure.

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               39 FR 37016  October 16,  1974
                         METHOD 14
     DETERMINATION OF FLUORIDE EMISSIONS FROM POT ROOM
          ROOF MONITORS OF PRIMARY ALUMINUM PLANTS
    1.1   Principle
Gaseous and particulate fluoride
roof monitor emissions are drawn
into a permanent sampling
manifold through several large
nozzles.  The sample is transported
from the sampling manifold to
ground level through a duct.
The gas in the duct is sampled
using Method ISA or 13B —
Determination of Total Fluoride
Emissions from Stationary Sources.
Effluent velocity and volumetric
flow rate are determined with
anemometers permanently
located in the roof monitor.
1.2  Applicability
This method is applicable for
the determination of fluoride
emissions from stationary sources
only when specified by the test
procedures for determining
compliance with the
New Source Performance Standards.

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