fc>«K M It
United States 0">ce of Air Quality
Environmental Protection Planning and Standards
Agency Research Triangle Park NC 27711
E-MB- Report 78-GLS-3
February 197S
Air
Arsenic
3lass Manufacturing
f^~
-<*»•
Emission "lest heport
Corning Glass Works
Centra! Falls, Rhode Island
-------
EME Report 78-GLS-3
February 1979
ARSENIC GLASS MANUFACTURING
EMISSION TEST REPORT
FJLant Tested
Corning Glass Works
Central Falls, Rhode Island
October 9-12, 1978
Prepared for
Environmental Protection Agency
Office of Air Quality Planning and Standards
Emission Measurement Branch
Research Triangle Park
North Carolina 27711
by
M. T. Thalman, W. E. Meyer, and M. 0. White
Issued: April 12, 1979
MONSANTO RESEARCH CORPORATION
DAYTON LABORATORY
1515 Nicholas Road
Dayton, Ohio 45407
Report Reviewed by .D. Eivins
Contract 68-02-2818, Work Assignment No. 10
-------
TABLE OF CONTENTS
Section £££
I Introduction 3-
II Summary of Results 3
III Process Description H
IV Location of Sampling Points 13
V Sampling and Analytical Method - ^
Appendix
A Complete Arsenic Emission Results
B Field Data Sheets
C Analytical Data Sheets
D Field Visible Emission Data Sheets
E Analytical Methodology
F Project Participants
111
-------
LIST OF TABLES
Tacie
1 Summary of Arsenic Emissions
(metric units, inlet)
2 Surmarv of Arsenic Emissions
(English units, inlet)
3 Summary of Arsenic Emissions
(metric unirs, outlet)
4 .Summary of Arsenic Emissions
(English units, outlet)
5 Grab Sarr.ole Arsenic Concentrations
(for Central Falls, Rhode Island)
(for Central Falls, Rhode Island Plant!
(Ib'hr of Elemental Arsenic)
IV
-------
LIST OF FIGURES
Figure Page
1 Process Diagram 12
2 Diagram of inlet and outlet of baghouse 14
3 Inlet sampling train 16
4 Outlet samolinc train 17
-------
SECTION I
INTRODUCTION
The Corning Glass Works plant in Central Falls, Rhode Island,
was tested by Monsanto Research Corporation (MRC) for the Err.is-
sion .Measurement Branch, Field Testing Section of the Environ-
mental Protection Agency (EPA). The test was performed under
Contract Number 68-02-2818, Work Assignment Number 10. The pur-
pose of testing the Corning Glass plant was to gather data that
could possibly be used to support the setting of standards of
performance for the glass industry. The field test work was
directed by Dan Bivins, Field Testing Section, Emission Measure-
ment Branch, EPA. The sampling performed by MRC was directed
by Robert A. Wachter as team leader. Gaseous and particulate
arsenic emissions were determined at the inlet and cutlet of the
baghouse on Coming's Tank £86. Samples of batch and product
material, baghouse dust and slag material were collected so an
arsenic material balance could be performed.
The sampling at the Central Falls site was performed by MRC dur-
ing the week of October 9-12, 1978. The collection method em-
ployed was "Reference Method for the Determination of Particulate
and Gaseous Arsenic Emission from Non-Ferrous Smelters", Method
No. 108, with some approved modifications. The samples collected
were analyzed using atomic absorption spectre-photometry.
-------
SECTION II
SUMMARY OF RESULTS
For this project, a total of eight arsenic emission tests were
conducted at the baghouse inlet and the outlet stack. Tables 1
and 2 summarize the arsenic data at the inlet. Tables 3 and 4
summarize the arsenic data at the outlet.
Table 5 shows arsenic concentrations found in the grab samples
taken from the batch glass, product glass, ESP dust and slag.
Table 6 reviews the material balance that was completed on this
project.
All arsenic data are reported as elemental arsenic.
Summary sheets of emission opacity readings can be found in
Aocendix D.
-------
Table 1. .SUMMARY OF ARSKNTC EMISSIONS
(metric unit:;, .inlet)
Run Number
Da tie
Volume of gas sampled - DNCM'1
Percent moisture by volume
Average .stack temperature - °C
Stack volumetric flow rnte - DNCMI'M1'
Stack volumetric flow rate - ACMPM
Percent isokinetic
Duration of run - minutes
Arsenic loading
Front half - mg
- g/DNCM
- kg/hr
Back half - mg
- g/DNCM
- kg/hr
Total - mg
- g/DNCM
- kg/lu-
1-1
10/10/78
2.55
3.24
230
189
346
97.5
12 8
60.30
0.0267
0.303
4.70
O.J)OJL3
0.021
73.00
0.0286
0.324
1-2
10/11/78
2.58
3.50
235
1HO
327
103.9
120
59.00
0.0231
0.250
4.70
o.ooi8
0.019
64.50
0.0249
. 0.20?
1-3
10/11/78
2.68
3. 71
_21Q
189
350
102.5
128
62.50
0.0233
0.264
5.90
0.0022
0 . n ') ^
. fi_8 . 4 0
0.0255
0. 209
T-4
10/1 2/7H
2.47
235
173
324
103.0
128
62.40
0.0253
0 . 2 f, 3
7 . f> 0 ,
0,Q030
0.032
70.00
0.0283
0.295
Dry normal cubic meters at 20°C, 760 mm llg
Dry normal cubic meters per minute
-------
2. SUMMARY OP ARSFN7C
(Fnqlish units, in lot)
Run Number
Date
Volume of gas sampled - DSCFa
Percent moisture by volume
Average stack temperature - °F
Stack volumetric flow rate - DSCFM
Stack volumetric flow rate - ACFMb
Percent isokinetic
Duration of run - minutes
Arsenic loading
Front half - mg
- grains/DSCF
- lbs/hr
Back half - mg
- grains/DSCF
- lbs/hr
Total - mg
- grains/DSCF
- lbs/hr
1-1
10/10/78
90.07
3. 2 A
460
6685
12208
97.5
128
68. 30
0.0117
O.G69
4.70
0.0008
0.046
73.00
0.0125
0 . 7 1 5
1-2
10/11/78
9 1 . 1 4
3.50
455
6352
11538
103.9
128
59.80
0.0101
0.550
4 .70
0.0008
0.043
64 .50
0.0109
0.593
1-3
10/1.1/78
94.66
3.71
465
6686
12341
102.5
128
62. 50
0.0102
0.583
5.90
0.0009
0.055
68.40
0.0111
0.630
1-4
10/12/7R
87.10
3.53
455
6123
11441
103.0
128
62.40
0.0110
0.579
7.60
0.0014
0.070
70.00
0.0124
0.649
Dry standard cubic feet
Actual cubic feet per minute - stack conditions
-------
Table 3. SUMMARY 0?' ARSKNTC HMISSIONS
(metric unitr;. on I let)
Run Number
Da te
Volume of gas sampled - DNCMa
Percent moisture by volume
Average stack temperature - °C
Stack volumetric flow rate - DNCMPMl>
Stack volumetric flow rate - ACMPM
Percent isokinetic
Duration of run - minutes
Arsenic loading
Front half - mq
- g/DNCM
- kg/lir
Bade half - mg
- cj/DNCM
- kcj/hr
Total - mg
- cj/DNCM
- kg/hr
0-1
10/10/78
1.91
1 . 6 .3
14 '3
27.2
326
97.1
1.20
0.26
0.0001
0.002
2 . 4 .1
0.0013
0.017
2.67
0.00.1. 4
0.01')
0-2
10/11/78
1 .Oft
3.44
138
232
333
95.8
120
0.09
0.0000
0.001
2.51
0.00:i 3
0.0.17
2.60
0.00.1.3
0.0.18
n-i
10/11/78
1.91
3.70
135
222
317
96. G
.....120. .. .
0.05
0.0000
0.0000
3.13
0.0017
0.022
3.18
0.0017
0.022
n-.A. .
10/12/18..
1.93
4 . 4.J
137
215
.110
101.0
120
n.07
._ .O...OQOO
0.0000
4. 15
0.0022
0.028
4.22
0.0022
0.07.R
cr>
b
Dry normal cubic meters at 20°C, .760 mm llg
Dry normal cubic maters per minute
-------
Tnble 4. SUMMARY OP APSFNTC rMTSSTOMS
(Fnqlish units, outlet)
Run Number
Date
Volume of gas sampled - DSCFa
Percent moisture by volume
Average stack temperature - °F
Stack volumetric flow rate - DSCFM
Stack volumetric flow rate - ACFMl)
Percent isokinetic
Duration of run - minutes
Arsenic loading
Front half - mg
- grains/DSCF
- Ibs/hr
Back half - mg
- grains/DSCF
- Ibs/hr
Total - mg
- grains/DSCF
- Ibs/hr
0-1
10/10/78
67.^/1
3.63
292
7823
TIM')
97.1
120
0.26
0.0001
0.004
2.41
0.0005
0.037
2.G7
O.OOOf)
0.0*1
0-2
10/1.1/78
69.8 B
3. -14
280
8209
1 1774
9 5 . 8
120
0.09
0.0000
0.00.1
2.51
O.OOOG
0.039
2.60
0.0006
n nan
0-3
10/.1 1/78
67. 34
3.70
276
7841
11208
96 . 6
120
0.05
0.0000
0.001
3.13
0.0007
0.048
3.18
0.0007
0.049
0-4
10/11/78
68.01
4.43
278
7579
10945
101.0
120
0.07
0.0 000
0.001
4.15
n.noia
0.061
4.22 .
0.0010
0.062
Dry standard cubic feet
Actual cubic feet per minute - stack conditions
-------
Table 5. GRAB SAMPLE ARSENIC CONCENTRATIONS (FOR CENTRAL FALLS, RHODE ISLAND)
CD
Batch Feed
Description
Batch Gullet
Product
naghouse Capture
Slag
Cu.llet mixed w/raw materials
Run Number
1
2
3
4
Average
1
2
3
4
Average
1
2
3
4
Average
1
2
3
4
Average
All runs
All runs
m g As/g_material
7.fM
7.0G
6.58
_G_.HG_
7 .1)9
not col 1ected
7.0f>
6.94
7.09
7.03
6.89
7.48
7.40
7. 34*
7.34
73.0
65.4
65.4
5_2_._2__
64.0
1.9
7.30
*No sample taken for product for this run. Used the average concentration for the
four product samples taken.
-------
Table 6. ARSENIC MATERIAL BALANCE (FOR CENTRAL FALLS, RHODE ISLAND PLANT)
(lb/hr of Elemental Arsenic)
(1) Batch Feed (In)
(2) Feed Gullet (In)
(3) Return Cullet (In and Out)
(4) Molded Ware (Out)
(5) Stack Particulate (Out)
(6) Baqhouse - Collected Particulate (Out)
(7) Regenerator Condensed Particulate -
Estimated (Out)
TOTAL IN
TOTAL OUT
Run
1
8.
3.
4.
1.
-
.
H
98
95
18
08
04
97
03
Run
8.
3.
5.
10.
•
1.
?2
38
93
21
61
04
09
03
Run
7.
3.
5.
10.
•
1.
n
81
86
12
50
049
09
03
Run
7.
3.
6.
10.
•
•
a
#4
71
42
07
77
06
76
03
*
17.11
16.30
17.52
16.98
16.79
16.79
17.20
17.69
*No sample taken for molded ware for this run. Used the averaqe concentration for
the four product samples taken.
-------
SECTION III
PROCESS DESCRIPTION
The entire glass process revolves around the melt tank, which
attains a temperature of about 1400°C and is used for condition-
ing the glass before molding. The greatest level of pollution
from the plant comes from the melt tank emissions which are
directed through the plant's emission control equipment and
eventually out the stack.
Corning Glass Works mixes feed batch and feed cullet with hot
cullet return in the melt tank. Also mixed with these raw mate-
rials is a solution of arsenic acid. From the melting tank,
product is sent to molding and cutting machines. Excess glass
from molding forms and any glass produced during stoppages of
the molding production line is recycled as hot cullet return.
The gas stream leaves the melting tank and enters the regenerators
where slag is removed. Regenerator exhaust enters the baghouse
where particulate is collected. Gas from the baghouse is vented
to the atmosphere. A sketch of this process is shown in
Figure 1.
11
-------
to
ru.u I>MIV,II
FEED CULLET-j
X i '
MIXING & FILLING ARSENIC
MACHINE AC)D
;
1
MELTING
*" TANK 086
TO STACK
t
ta. n Tf TMI'IJ ATOD1" to* OAPIinilT
•^ KLbLNLKAlUK J UMulHJUjL
CONVEYOR
„ «^. f| ftT *—
1
HOT GULLET RETURN
,, PARTICULAT
rni I rrTED
MOLDING & CUTTING nnnmirT
MACHINES IKUUULI
Fiqurn 1. Procoss cliaqram
-------
SECTION IV
LOCATION OF SAT.PLING POINTS
The sampling plan required testing for arsenic emissions at the
inlet and outlet of the fabric filter baghouse on Coming's Tank
=86. Four arsenic runs were completed at both the inlet and
outlet of the control device. These simultaneous runs were used
to determine the efficiency of the baghouse.
The outlet stack is approximately 130 feet high with the sam-
pling port at approximately the 100 foot level of the stack.
Sampling was performed on a catwalk between the baghouse and the
main building. A 2" x 12" x 96" board was installed by MRC per-
sonnel across the handrails to support the sampling train while
traversing the stack. The outlet stack diameter is 36 inches
with two 3-inch diameter ports at 90° apart. The distances to
the nearest duct disturbance before and after the ports were
sufficient to use the minimum number of points for the traverse.
Total sampling time was 2 hours, which consisted of 24 points
sampled for 5 minutes each.
Steps provided access to the inlet ports. The inlet stack diame-
ter is 24 inches with two 3-inch diameter ports at 90° apart.
There are 54 inches before the ports (2.25 diameters) and 68 inches
after the ports (2.83 diameters) of duct work without any type of
disturbances, thus the maximum number of 32 traverse points was
used, sampling for 4 minutes per point.
A diagram of both sampling sites is shown in Figure 2.
13
-------
BAGHOUSE
N/1
r~>
O
o
01) I 111
STACK PORTS
ICL
I.D.
FAN
BUILDING I)
now
-J
J"
o-| -INLET PORTS
FROM
FURNACE
Figure 2. niaqrnm op inlet, ami oulilot of bnqhouse
-------
SECTION V
SAMPLING AND ANALYTICAL METHOD
The baghouse was sampled generally in accordance with the draft
Method 108. Method 108 is designed for use at nonferrous
smelters where high levels of S02 are expected. At Corning
Glass Works, only very small amounts of S02 were present, there-
fore, impinger solutions were changed from H202 to H2O to trap
the gaseous arsenic and moisture in the gas stream. Cleanup of
the impinger portion of the train was done using a solution of
NaOH in accordance with Method 108. A diagram of the cleanup
of the modified Method 108 sampling train used at the inlet is
illustrated in Figure 3. A diagram of the cleanup of the modi-
fied Method 108 used at the outlet is illustrated in Figure 4.
All other requirements of sampling using Method 108 were used
along with any Federal Register methods needed to perform
Method 108.
During the arsenic emission tests, an integrated gas sample was
taken at a single point according to Method 3 and analyzed by
Orsat to determine the stack gas molecular weight and excess
air. Also run simultaneously with the sampling runs for arsenic
was Method 9, an opacity determination by a single observer,
started 30 minutes before and ended 30 minutes after the runs.
Grab samples of baghouse dust, feed, material, slag and product
were collected during each run. These samples were analyzed for
arsenic content by the MRC lab.
15
-------
IM) ml
NaOII
2m gm
SILICA
GIL
WEIGH &
DISCARD
cr>
RINSE M-0. IN. Na()H
MEASURE «• COLLtCT
RINSU 2 -110.DISCARD
I. MEASURE*, COIIECrCONflNTS
2. KINSt;USE '1- I'OttllONS OF 0.1 N. N.iOII I 30mlsl
MLASIIIU: f- RFCOKI) VOl.UMl Of IMNSt I'OURtD
GUI Of IMI'INOIRS.ADO HINSF. 10 CONIAINIHS.
NOIE: RUN f - K HAD 2 ADDITIONAL
IMPINGERSOFH 02 ADOLD.
JUST BEFORE HICNaOII IMPIN-
CLR.
0
I'iciurc 3. Irilol: snmpl. i.nq I: rain
-------
200 gm
SILICA
GEL
WEIGH &
DISCARD
RINSE*! -0.1 N. NaOH
MEASURE fc COLLECT
RINSE*2-H2O.DISCARD
1. MEASURE & COLLECT CONTENTS
2. RINSE;USE 2 PORTIONS OF 0. IN. NaOH ( 30 mis)
MEASURE & RECORD VOLUME OF RINSE POURED
OUTOFIMPINGERS.ADD RINSE TO CONTAINERS.
f-
,A
©
NOTE: RUN 0-4 HAD 2 ADDITIONAL
IMPINGERS OF H.O ADDED
JUST BEFORE THE SILICA GEL.
Figure 4. Outlet sampling train
17
-------
All arsenic analysis was performed by Atomic Absorption Spec-
trophotometry (AA). Analysis was performed directly on the
liquid samples and on the solid samples after being digested. A
comclete description of the analytical procedures is presented
in Appendix E.
Samples showing high arsenic levels were quantitated using Flame
Atomic Absorption, while the low-level samples were quantitated
by Atomic Absorption using the hydride generation technique.
13
-------
5 DECEMBER 1976
CORNING GLASS. H I
ARSENIC SAMPLING
ABBR
DESCRIPTION (20 DtG C) UNITS
1-1
1-2
1-3
1-1
0-1
0-2
TT
PB
DCLH
VM
TM
VMSTO
vw
VWG
PCNTM
MD
CO?
02
N2
MWO
MW
DELP
CP
TS
PM
PS
VS
DS
AS
OS
OA
ON
PCTI
MF
MT
CAN
CAO
CAT
CAU
CAW
CAX
DURATION OF RUN
BAROMETRIC PRESSURE
AVG ORIFICE PRESS DROP
VOL DRY GAS(METER CONI
AVG GAS METER TEMP
VOL DRY GAS (STO COND)
TOTAL H20 COLLECTED
VOL H20 VAPOR{STD CON)
PERCNT MOISTURE BY VOL
MOLE FRACTION DRY GAS
PERCENT C02
PERCENT 02
PERCENT N2
MOl WT OF DRY GAS
riOL WT OF STACK GAS
AVG STACK VELOCITY HEAD
PlTOT COEFFICIENT
STACK TEMPERATURE
STACK PHESSURE(STATIC)
STACK PRESSURE (ABS)
AVG STACK GftS VELOCITY
STACK DIAMETER
STACK AREA
STACK FLOW RT(DHY STD)
STACK FLOW RTIACTUAL)
PROBE TIP OlAMEIEft
PERCENT ISqhINETIC
ARSEWC (FRONT)
'ARSENIC (TOTAL)
ARSENIC (FRONT)
ARSENIC (TOTAL)
ARSENIC (FRONT)
ARSENIC (TOTAL)
"ARSENIC (FRONT)
ARSENIC (TOTAL)
MINUTES
CM HG
CM H20
DCM
DEG C
DNCM
ML
NCH
CM H20
DEG Ci'
CM H20
CM HG
MPM
CM
SO CM
DNCMPM
ACMPM
CM
MG
MG
G/DNCM
G/DNCM
G/ACM
G/ACM
KG/HR
KG/HH
126.0
76.23
1.378
2.569
21.3
2.55
61.1
0.086
3.24
0.968
1.6
19. M
76.8
29.1
28.7
2.866
0.750
236.
-20.63
71.69
1262.
59.06
2739.2
169.
316.
0.615
97.5
66.30
73.00
0.0267
0.0286
0.0116
0.0156
0.303
0.32«4
128.0
76.15
1.051
2.589
23.8
2.56
70.1
0.091
3.50
0.965
2.1
17.0
80.6
29.1
28.7
2.531
0,750
235.
-21.59
71.87
1193.
59.06
2739,2
180.
327.
0.615
103.9
59.60
61.50
0.0231
0.0219
0.0127
0.0137
0.250
0.269
126.0
76.20
1.153
2.728
27.3
2.66
77.5
0.103
3.71
0.963
2.1
17.3
60.6
29.0
26.6
2.903
0,750
210.
-21,59
71.61
1276.
59.06
2739.2
189.
350.
0.615
102.5
62.50
68.140
0.0233
0.0255
0.0126
0.0137
0.261
0.289
126.0
71.10
3.732
2.535
22.9
2.17
67.6
0,090
3.53
0.965
2.1
17.3
80.3
29.1
26.7
2.127
0,750
235,
-21.59
72.61
1183.
59.06
2739.2
173,
321.
0.615
103.0
62.10
70.00
0.0253
0.0263
0.0135
0.0151
0.263
0.295
120.0
76.07
2.689
1.916
21.6
1.91
51.0
0.072
3.63
0.961
2.6
16.6
80.6
29.1
28.7
0.602
0.713
115.
-0.61
76.01
515.
69.85
6311.3
222,
326.
0.775
97.1
0.26
2.67
0.0001
0,0011
0.0001
0.0009
0.002
0.019
120.0
76.71
2.813
1.975
23.0
1.96
52.9
0.071
3.11
0.966
2.1
17.0
60.6
29.1
20.7
0.638
0.713
138,
-0.61
76.65
526.
69.85
6311.3
232.
333.
0.775
95.6
0.09
2.60
0.0000
0.0013
0.0000
0.0009
0.001
0.018
-------
APPENDIX A
V,-,T r-"-T ?r>s;r-yT£ E>'~CSION RESULTS
-------
ABBR
5 DECEMBER 1978
COHNJNG GLASS. R I
ARSENIC SAMPLING
bESCRIPTION (68 DEC F)
UNITS
1-1
1-2
1-3
1-4
0-1
0-2
TT DURATION OF RUN MINUTES
PB BAROMETRIC PRESSURE IN HG
DELH AVG ORIFICE PRESS DROP IN H20
VM VOL DRY GASIMETER CON) DCF
TM AVG GAS MEIER TEMP OEG F
VMSTO VOL DRY GAS
-------
5 OtCfMIM.H 1978
COKN1NG GLASS. K I
AHSINIC SAMPLING
AllllH
120 OEG Cl UNITS
0-3
0-H
TT
I'll
Of LM
VM
TM
VMS TO
vw
VWG
I'CNtM
Mil
CO?
02
N?
MWO
MU
01 LP
Cf>
fS
I'M
PS
vs
OS
AS
(JS
UA
l)N
PC T r
MF
MT
CAN
CAO
CAT,
CAO
CAW
CAX
uiMAHOfj OF now
|i/.MOMf.Ti:iC PIILSSUKE
rtVG OHir 1CI PKlSS OHOP
VOI. OHY GASIMLTEK CON)
nVG GAS MltLn TCMP
VCL Uttf GAS (STl) CONOI
TOTAL H?0 COLI.lCTtO
VOI ||?0 VAPOHISTO CONt
PIHCNT MOlSTUHf BY VOL
MOLE FRACTION OrtY GAS
PJKCLNT CO?
PlHCf.NT O?
I'l-MCINT N2
MOL WT OF OUT GAS
MJL WT OF SlACK GAS
AVG STACK VELOCITY1 HCAO
PI fOT COtFF ICIF-NT
STACK TIMPLKATOHE
STACK PUT SSUIU (STATIC 1
SlACK PHESSlllir. (AUSI
AVG STACK (-AS VELOCITY
STACK OtAMLltK
STACK AltEA
STACK FLOW HTlOHY STO)
STACK FLOW HT( ACTUAL)
PHOliE TIP OlAMFTER
PlHtl'MT ISOKINfTlC
AHSfNIC IFHONTI
AHStNIC (TOTALI
AKSTNir (FhONT)
AKSIHIC l^OTALt
AHSINIC (^''ONT*
AKSINIf I'OTAL)
AHSINIC (FRONT)
AHSINIC (TOTALI
MINUTES
CM HG
CM H20
OCM
(irr, c
DNCM
Ml.
NCM
CM H20
ore, c
CM 1120
CM MO
MI'M
CM
su CM
DNCMI'M
ATMPM
CM
MO
MO
G/ONCM
G/UNCM
G/ACM
G/ACM
KG/HK
KG/MM
1?0.0
76.71
2.95B
1 . V20
25. 7
1.91
5M .9
0.073
3.70
0.963
2. 1
17.2
00.7
29. n
26.6
0.5ns
0. 743
135.
-0.01
76.65
501 .
09.05
63M1.3
222.
317.
0.775
9<> .6
0.05
3. in
0.0000
0.0017
0.0000
0.0012
0.000
0.022
1?0.0
76.71
2.7»«
1 .915
21.9
1.93
fcfc.9
0.009
M.M3
0.956
2.M
17.3
00.3
29.1
20.6
0.551
0. 743
137.
-0.01
f Ci « t» D
It ii ty
W9.«5
63M1.3
215.
310.
0.775
101.0
0.07
M.22
0.0000
0.0022
0.0000
0.0015
0.000
0.020
-------
b OCCCMIJIH 1S78
COHNING GLASS. H I
.Att SAMI'LING
Ani)H
liLSCIHPTION (f.fl 01.0 Fl
UNITS
0-3
0-"4
TT
I'H
or.LM
VM
TM
VMSTO
vu
VUG
IT.NIM
Mn
CO?
02
N2
MWO
MW
OLLP
CP
TS
I'M
PS
vs
OS
AS
OS
on
ON
ITU
nr
MT
CAM
CAO
CAl'
CAO
CAW
C AX
dUHAiiON or RUN
HAHOMCinic I'nrssunr.
AVG OIUHCL I'KtSS OROP
VOL OUT GASIMCII.H CONI
AVG liAS MEIKR TCMC
VOU l)l«t GAS (S1U CONO)
101AI H20 COI.LfCTtO
VOL 1120 VAI'OHISJD CONI
PtRCNI MO 1 SIUHt BY VOL
MOlt FR ACT ION OHV GAS
I'lHCCNT CO?
PtMCCNT 02
• •IMCfNT N2
HOL Uf OF (IKY GAS
MOL Wf OF STACK CAS
AVG STACK Vtl.OCITY HEAD
PITOT corn ICIENT
STACK TIMPHMTUMC
STACK PHtSSURI (STATIC)
STACK PHfSSUUi: IAHSI
AVG STACK GAS VtLOCITY
STACK DlAWlTrH
STACK AHEA
STACK FLOW HTIOHY STO)
STACK f-LOU HTlACTUAH
PHOI1E HP UlAMLTtH
r-lUCtNl ISOKINPT1C
AUSlNIt; (fKONT
AUSlNlf. (TOTAL
AHSINH; IHIONT
AKS1NIC (TOTAL
AKSINIC (FRONT
AUSINIC (TOTAL
AIISINK; irKONT
AKSINIC (TOTALI
MINUTCS
IN MG
IN H20
OCF
ore, F
HSCF
ML
scr
IN H20
OF.G F
IN M?0
JN HG
H'M
JNC.HLS
SO IN
OSCFM
ACf M
INCIILS
M(.
MG
CR/OSCF
Gii/oscr
OH/ACF
GH/ACF
LII/MR
LO/KH
120. 0
30. ?0
1.165
bT.HOO
70.2
67. 5t
bM.9
2.bflf,
3. 70
o.9<»a
2.1
17.?
00. 7
2V.O
20. f,
0.230
0.7«43
?76.
-0.32
30. in
lfcM2.
3b.38
9«2.R
7«'ll.
n^on.
0.305
Vfc.fe
0.05
3. in
0.00(10
0.0007
0.0000
0 . (MMI 5
n . (MI i
0.0'»7
120.0
30.20
I .097
f>7.fclO
71.3
60.01
f>6.9
3.1^1
I.11* 3
0.95fe
2.M
17.3
00.3
29,1
?fl.6
0.217
0,7-»3
27fl.
-0.32
30.10
1G04.
35.30
9«2.0
7579.
109't5.
0.305
101.0
0.07
•1.2?
0.0000
0.0010
0 .0000
0.0007
n.oot
O.Oh?
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
DATE /g/f/rg
SAMPLING LOCATION J^ttr T-
INSIDE OF FAR WALL TO
OUTSIDE OF NIPPLE, (DISTANCE A) _
IKSiDE OF NEAR WALL TO
OUTSIDE OF NIPPLE, (DISTANCE B) _
STACK I.D., (DISTANCE A - DISTANCE B) 2 3 vy '
NEAREST UPSTREAM DISTURBANCE 5" -ft " Ok
XEAREST DOWNSTREAM, DISTURBANCE __i_/Lj__l£l
CALCULATOR /< . f^fcg +-r
c
SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
/ ,11
i it
2 (1
* ' tf
^ t./
t AJL
f j?3
* zy
/^ ;^
/f zV
U ,2-t
/3 ,^
/f ^
/I ,U
Vo
fEACW
OF STACK
MT'
1.0.
/. y
tf
^ 6
it.r
/i-l
/j^.C
;H-3
J7- r
u.
r
7
7^.0
fi-
$1.
r
°il,r
K.\
S4.t
STACK I.D.
^
OL ^
3 ^
5" 1A
4 r/4
^ Vy
/V Vt
it, \
/^ l/^
/9 ?/4
5D 3A
^ / y/
? ^^4
^^ T<
•
DISTANCE B
t VV ''
/
1
j
"
TRAVERSE POINT LOCATION
FROM OUTSIDE OF NIPPLE'.
(SUM 0 F COLUMNS 4 & 5)
k %
"7 J/i
$ V
-------
APPENDIX B
^- — — T r\ 7s; ^1 >"^ i ^V~»™S
-------
Plant
Run #
MOISTURE IN STACK GAS DETERMINATION
METHOD M
Date
J—
Location Sampled
Volume of gas at meter conditions (CF) = VM =
Average meter temperature (°P) = TM =
Barometric pressure absolute (in Hg) * PB = _
VMS = Volume of gas sampled at standard conditions (SCF)
(17.71)(VM)(PB) . 17.71
(TK + "'
"*
(
+ 460
Volume. of water final
Wt . of silica gel final
Volume of water initial
Volume collected Vj =
Vt . of silica gel initial
Wt . of water V2 =
Total volume of water collected (ml) = Vj + V2 = VL =
Volume of water vapor at standard conditions (CF) =
(~J_
Mole fraction of water vapor
M
Percent moisture = (100)(M)
0 .02-*
100 (fts
,-n0/
3 2 ^.
-------
PRELIMINARY VELOCITY TRAVERSE
1 I.HH 1 ' — ' — •j — " ^_________
O^TF I G / t '/7 *
IfifijinN 1^/tr *> 4'tt^'i_
rrACK i D c2 J '^ ''
BAROfr.ETRIC PRES
STACK GAUGE PRE
1IIBP in Hf ^ '- f'3-
_*»."*ifZl_- C
WIRF in H»0 •*C&^V-^ b.
TV t«. r f
TRAVERSE
POINT
NUMBER
;
z_
7
v/
VELOCITY
HEAD
Up,), in-HjO
C, GL
0,7o
0,7
7
7
/c
H
/7
/j
//
//
/IL
AVERAGE
0,^1
0.1S"
0.6^
0,7C
0,67
0.7 S"
0,7 ^
0.17
0,7 (p
STACK
TEJrtPERATURE
(T..-F
3B
43^
*f O
^f_S"fe
H-sT
^•6 6
i^Gl
q-ve
4^"^
4^9
^^ i
*4/3\
460
EPA (Dur» r"
-4/72
2—
V'"
SCHEMATIC OF TRAVERSE POlfT LAYOUT
TRAVERSE
POINT
MUWBER
1C
VELOCITY
HEAD
(ipj). in.HzO
O.V7
•2. I
2-05
AVERAGE
STACK
TEMPERATURE
(Ts), -F =
300
-------
NOMOGRAPH DATA (HP-65)
PLANT
DATE fO)l/j't
USED ON RUN NO
CALCULATOR: 7
SAMPLING LOCATION
STEP
INSTRUCTIONS
INPUT DATA/UNITS KEYS
OUTPUT
DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
14>
142
143
Run card
Initialize program
Enter average T (meter
temp. °F + 460) If meter
temp, unknown, use ambi-
ent + 20°F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacR) [P ± .073 x
stack gauge pressure in
In. H20]
Enter average T
(stack temperature + 460)
Enter Bms
(mole fraction of H20
vapor in gas stream)
Enter MD
(molecular weight of dry
gas)
Enter Cn
ftvne "5" nitnt tuhp rn-
efficient)
Enter average A
Highest AD ( y.^C )
Initialize " B "
Enter actual D
n
Enter AHo
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
pi
Enter actual A
Enter actual A
^0 -.
,£- f.f^ In. Hg
?«.^"-".
4 0 2 °R
A f-\ 7 Q, Fraction
(j.i*, --• of H2o
n * .» lbs/lb
(^ i ' '5 mo! e
r5 1*~
/.07 In- H2°
^pyST In.
/. <££>/ In. H20
f.»l
1.3 f
A
R/S
R/S
R/S
R/S
R/S
R/S
•D / C
K/ ;>
R/S
R/S
R/S
E
E
E
0.00
f" J O T
^^ ^^ *^^^ rr
J "} £. ( T / P
?;-fx %
,^' Ps/Ts
. . Fraction
f\ f ~7
°' '/ Dry
3 %• ? MW
molecular wt
of stack gas
Ibs/lb mole
f/r, *
Dn theo.
(nozzle dia.£
in inches)
e.' ** j.
K factor •
In. H?0
AH (^1
In. \\$^
AH
In. H20
-------
DRY MOLECULAR WEIGHT DETERMINATION
COMMENTS:
\ ['. 0 0
SAMPLING TIME (24Jif CLOCK)
SAMPLING LOCATION, fe.fr frH[OVli>*V
SAMPLE TYPE (BAG. INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD fl (U TL.
<*£-/* (3
AMBIENT TEMPERATURE
OPERATOR Vk) K
\. RUN
GAS ^\
C02
02
-------
FIELD DATA
DATE.
SAMPLING IOC
SAMPLE TYPE
RUN NUMBER.
OPERATOR
i^Xxohft
PROBE LENGTH AND TYPE.
NOZZLE 1.0 I
vofc:
a.
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, (P.)
FILTER NUMBER (*)
\F-
3°, 01
ASSUMED MOISTURE, t
SAMPLE BOX NUMBER
METER BOX NUMBER
METER AHp
C FACTOR
.1 •
'& o
(.0
/.
-'3.
PROBE HEATER SETTING
HEATER BOX SETTING
REFERENCE *r
-0
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA FVFRY tfw MINUTES LEAK RATE(%0~/7. 3
&o.
6.T.,
II- ft
12
c
JLL
_t
\^.io\
t?
^Ji
. oo
70
C 7
0-7
\
••/;
-------
NOMOGRAPH DATA (HP-65)
PLANT_
DATE
USED ON RUN NO.: /•"/
CALCULATOR: "f
SAMPLING LOCATION
STEP
INSTRUCTIONS
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
1*1
1*2
l«s
Run c a rd
Initialize program
Enter average * (meter
temp. °F * 460) If meter
temp, unknown, use ambi-
ent + 20 = F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacR) [P ± .073 x
stack gauge pressure in
In. H20]
Enter average T
(stack temperature + 460)
Enter Bms
(mole fraction of K 2 0
vasor in cas stream)
Enter MD
(molecular weight of dry
gas)
Enter Cn
(type "S" pitot tube co-
efficient j
Enter average A
P
Highest AQ ( )
Initialize "B"
Enter actual D
n
Enter AH*
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
Enter actual A
Enter actual A
P3
QO OR
T>().O\ I"- H9
tf.1l In' ^
^3 OR
^ /,->£. Fraction
0.0^ of H20
o a /? Ibs/lb
^ T- ^ mole
.?r —
/, 07 I"- H20
-PV^ In.
/. fctf / In. H20
L'l
-
A
R/S
R/S
R/S
R/S
R/S
R/S
R/S
R/S
B
R/S
R/S
E
E
E
0.00
/"^^ Tm
/2^VPr.
^lv/ ?s
S6n PS/TS
T\ o Fraction
6/1 ^7- Dry
-<' 4. b'2 KW
molecular wt
• of stack gas
Ibs/lb mole !
i
?* >: /
Dn theo. . I
(nczr'e d-;a.
in inches)
r>«
K factc r
AHl /- ^
In. H?0
AH
In. H20J
AH i
In. H 2 0 \
-------
CLEAN-UP DATA
Plant /<.xv
Date
svfc
Sampling Location,
Sample
Run Number **/
Sample Box Number_
Clean-up Man
IMFINGERS
Final Vol.
Initial Vol.
Net Vol.
#1
#2
ml
ml
Z-2_ml
<> ml
\ ST ml
Total Net Volume in Impingers
Comments:
tet
#3
ml
ml
ml
ml
ml
ml
ml
ml
_ml
ml
SILICA GEL
Final Weight
Initial Weight
Net Weight
g
, 1
Total Net Weight in Silica Gel
Total Moisture
g
g
g
Filter Number(s)
g
\
-------
PLANT
DATE
(0
H
RUN NO
TKAVEWC
POINT
HUMBCR
'~L
GA5 MCTER RtAOING
(V). II1
. ooo
^OLI
-&&r3*
VELOCITY
HEAD
(AP.I. i". Hj
l.
1,4
'r&3-
ORIf ICE PRESSURE
OlfFERtHHAL
OESIHF.D AC1UAL
^
JZJlXl
/;
t-
-U
ZML
\.
J.70
STACK
TEMPERATURE
Y«
>m
Uz
f
W-
^^d
DRY CM METER
UMPERATURE
IHIET OUTLET
77
22
LL
&L
32.
2Z
-zz.
21
%
-TZ
PUMP
VACUUM.
Ht. H|
76?
(*•
/t.o
1OO
30°
SAJWtfWX
TEMPERATURE,
•F
?J
TEWfATURt.
•f
2^.
2^L
71
(n?
dl.
2Z
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLAIfT
DATE ..
COMMENTS:
SAMPLING TIME (2Wtr CLOCK) /<"•
SAMPLING LOCATION +*(<,+-
SAMPLE TYPE (BAG, INTEGRATED, CONTINUOUS).
ANALYTICAL METHOD O^Jtff
AMBIENT TEMPERATURE^ frrV*^
OPERATOR
\^ RUN
GAS ^^\
C02
02
W.I
•' S t
MULTIPLIER
4VlM
32/100
a/ioo
a/ioo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
MJ, Ib/lb-mole
-/7Ajfc
s-.it
O .# &
21.lt 5~
TOTAL 2l-
-------
ISOKINETIC CALCULATION
r .
Plant
location d*1*"1 7' •s-;^-^"*- , Initials,
MOISTURE
Net volume of liquid collected
in impingers and silica gel = VL *
Net volume of gas through dry
gas meter at meter conditions = Vm = 0 J2 / ^ cu.f,
^ ^i f) i * LJ M
Barometric Pressure - absolute « BP « £__: "* n - 9
Average absolute meter tem-
perature (°F + 460) = Tm " —
Percent moisture = M
„ ._ ififi ——-
, ^ 373.63 ( V ) ( BP 1
| + it
m
100
373.63
a'
s *
MOLECULAR WEIGHT
Percent 02 by volume dry basis = 02
H CO " " " " s CO = ____*
C02 ' s C02S . %
N2 « 100 - (0, + C02 + CO) • 100 - ( + + )
* o-
Percent N2 by volume dry basis = N2 = _____ *
Dry molecular weight s KD
MD « 0.44 { C02 ) + 0.32 ( 02 ) + 0.28 ( N2 + CO )
HD • 0.44 ( ) + 0.32 ( ) + 0.28 ( + )
-------
ISOKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight = MS
MS * (MD )[1 - (M x 10"2)] * 18 (M x 10"2)
MS = ( S.fc )[1 - ( ,03 }] + 18 { .01 ) =
\
\\
VELOCITY
Pitot tube coefficient, type S = CP =
Average Absolute Stack Temp. (°F + 460) = T§ =
Average of the square root of Ap
Absolute pressure of stack (BP ± ?.f g) = P.
Stack gas velocity
*}.(/! in. Hg
V * (85.48) ( CP )
Vs = (85.48) ( |~Tp—
\l ( n° } / *"
(> ?, 3/ FPS
across orifice =AH= I-~?O in.H70
= T - /^ O mi n.
= d = O.IY^ in.
2 7 -y . y
7\ _ CA CA ^ in~u ( -ZrV^-) = '''/ ^(6 > sq. ft
1 ~ 3H.3H A IU
ti c i v
0 00?67 ^V ^ 4 » ^m ' I PR + ' ^ M
( T ) ( V,
A )
(1
.667)
(»o
0.
00267 ( *LA/
) + ( n-n )
( ^74 )
^£.0}+^-
^
13.6
>
)(
X
-------
NOMOGRAPH DATA (HP-65)
PLANT L Qr*;my
DATE /£>///
USED ON RUN NO.: 7>
CALCULATOR: /C . ^ c/c< T
+•
SAMPLING LOCATION_
STEP INSTRUCTIONS
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
Run card
Ini tial i ze program
Enter average T (meter
temp. °F + 450) If meter
temp, unknown, use ambi-
ent + 20°F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacR) [P ± .073 x
stack oauoe pressure in
In.- H-,01
Enter average TS
(stack temperature + 450)
Enter Bms
7 1 (mole fraction of H20
1 vaoor in ces stream)
8
S
10
11
12
13
l«i
1«2
1«3
Enter MD
(molecular weight of dry
gas)
Enter Cp
(type "S" pitot tube co-
ef f ic ient)
Enter average ~L
Highest Ap ( ^-SL )
Initialize "8"
Enter actual D
Enter AHg
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
Enter actual 4
P2
Enter actual L
P3
j
In. H20j
AH i
In. H20j
-------
FIEIODATA
DATE
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
OPERATOR
^ << r A
'/=.
rTo"
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE. (PJ ,
FILTER NUMBER It) <*Ofrfc ff-fJ-
' 4- ^ ''/'
PKOBE LENGTH AND TYPE.
NOZZLE ID 6, 7 Y2
e f*/J
ASSUMED MOISTURE, t-
SAMPLE BOX NUMBER _
METER BOX NUMBER __
METER AH.. /
J -O
5
A
PROBE HEATER SETTING,
"HEATER BOX SETTING
'*1o/l
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA FVERY / MINUTES
LEAK RATE
CFM
"Hg
TRAVERSE
POINT
NUMBER
SAMPLIIIC
TIME, mm
CLOCK TIME
(74 hf
CLOCK)
lO-ST
CAS METER READING
VELOCITY
HEAD
Ap,). in. HjO
ORIFICE PRESSURE
DIFFERENTIAL
(AH), in. H?0)
DESIRED ACTUAL
STACK
TEMPERATURE
JT,)."F
DRYGASHETER
TEMPERATURE
INLET OUTLET
PWP
VACUU*.
in. Nf
SAMPtCeOX
TEMPERATURE,
•F
NBPIItGER
TtMPERATimE,
•f
0*
IC.O}
.°'^7
-U°,
*M
ILL
6 0
T
(s>
« \
Jj
OUS"
H-7
17.5^7
.T t.
0
32-
ill
iJ3T.
7 (a
Ml
2,60
IL
7,7 >
2.0-9
77
y.i-
77
(08
2z
ji
'•7
s
I
on*-
77
a
ja.
-------
PIANT
Cfa/J
DATE
A////
RUN NO
TRAVEMt
POINT
NUMBER
n
u
•uo
2JL
SAMPLING
TIME, mid
•71-
JLl
AM.
IV
CLOCK TIME
(H hi
CLOCK)
V-oo
Ii£i.
I:!
.LI
CAS METER READING
-Z.
iV
VELOCITY
HEAD
/
72-
•77
-------
CLEAN-UP DATA
Plant
Date
£»--
Sampling Location
Sample Type
Run Number
Sample Box Number 1 1 - 3
Clean-up Man CA
Comments
IK?INGSRS
#1 #2 #3
Final Vol. 1 t>8 ml 133 ml 30 ml
Initial Vol. 1 SQ ml { H£ ml £ ml
Net Vol. "
ml g5~ml 30 ml -
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT L0rv\;nt k/ >°////7*
Txi/, f- /» /gttlh'UJ^ /'--^L
SAMPLE TYPE (OAG. INTEGRATED, CONTK
ANALYTICAL METHOD (l^ff)
IUOUS) r*»\T •
r
AMBIENT TEMPERATURE 6 f "^
OPERATOR -Tfckevr^'
f
\. RUN
GAS ^^\
C02
02-i
— yy
O .Ob
*"J **7 ™" "~ "7
J«t **^ ^^^ /
TOTAL ^ 7 $ ^
(?\ 1 •
-------
ISOKINETIC CALCULATION
Plant
Runl J^ Q^. , Date
Location J^ ff t- A ^t/^^^wyC- , Initials /C
373.63 ( V
1 •+• - m
100
) ( BP )
( VL )
, . 373.63 ( ?/-/.IO }
MOISTURE
Net volume of liquid collected
in impingers and silica gel = V, = ~~?U- I ml
Net volume of gas through dry
gas meter at meter conditions = V^
Barometric Pressure - absolute - BP - '££?• /Q in.Hg
Average absolute meter tem-
perature (°F + 460) = Tm
Percent moisture * M
^ rift
M
?
^
MOLECULAR WEIGHT
Percent 02 by volume dry basis = 02 =
11 CO " " " " = CO =
" C02 " " " " = C02=
N2 = 100 - (02 + C02 + CO) = 100 - ( + + )
Percent N2 by volume dry basis - N2 =
Dry molecular weight = MD
MD = 0.44 ( C02 ) + 0.32 ( 02 ) + 0.28 ( N2 + CO )
MD * 0.44 ( ) + 0.32 ( ) + 0.28 ( + )
MD =
-------
ISDKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT {Cont.d)
Stack gas molecular weight
MS - (KD )[1 - (M x 10
MS - (20 )H ' ( 'c^
= MS
2)3 + 18 (K
x 10'2)
VELOCITY
Pitot tube coefficient, type S
Average Absolute Stack Temp. (°F
Average of the square root of
Stack gas velocity
V$ = (85.48) ( CP
(85.48)
type S
emp. (°F
ot of Ap
ck (BP ±
Vs
+ 460)
D N
13.6/
= CP =
' Ts =
= \[ Ap =
= P =
s
1 ( T J
1 ( >,
1 ( f/r
) (
)
MS )
in.Hq
FPS
ISOKINETI
C PERCENT
Average pressure drop across orifice
Total sampling time
Dianeter of nozzle
Area of nozzle = A
A = 54.54 x 10"* (d2) = 54.54 x 10~*
I = percent Isokinetjc
I
(1.667)
0.00267 (V
- T
= d
( T ) (
jr.. H20
mi n.
in.
13.6
sq. ft
(1
.667
)
•/ ) + i_
(
/ / -o {
\
<"< x;
• i
60
3.6
>x
/
-------
NOMOGRAPH DATA (HP-65)
PLANT
DATE
USED ON RUN NO.:
CALCULATOR:
' '
SAMPLING LOCATION 7t{rf- /»
STEP INSTRUCTIONS
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
14l
142
143
Run card
Initialize program
Enter average T (meter
temp. °F + 460) If meter
temp, unknown, use ambi-
ent + 20°F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacR) [P ± .073 x
stack gauge pressure in
In. H20]
Enter average T$
(stack temperature + 460)
Enter Bms
(mole fraction of H20
vapor in qas stream)
Enter MD
(molecular weight of dry
gas)
Enter Cn ^
(type "S" pitot tube co-
efficient)
Enter average A
Richest A ( 1- 1 1 )
Initialize "B"
Enter actual Dp
Enter AH«
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
Enter actual A
Enter actual An
PS
P
, . o p
fj 1 t K
? Fraction
/^•>-> of H20
~ a m Ibs/lb
mole
^r~
' ' '
/,e?Q In. H20
,41 K In.
lr$0\ In. H20
1.**
i7 ^
/7,7 VPm
*w ^
^3^ps/Ts
4, .-^Fraction
rib' Dry
2 5-C7 MW
molecular wt
of stack gas
Ibs/lb mole
W
Dn theo. -2
(nozzle dia.
in inches)
K factor
AH! /'*
Tn. H?0
AH 7-
In. H20
AH
In. H20
f/
< v/
--)7
1 ' <_
*
-------
FIELD DATA
PIANT.
DATE.
*////'?$
SAMPLING LOCATION -l"1r<:
SAMPLE TYPE /^'r-'C
RUN NUMOER I-'*
OPERATOR A /W
-------
PIANT
DATE
A////7
RUN NO
J'l
TRAVERSE
POINT
NUMBER
SAMPLING
TIME. win
CLOCK TIME
(74 hi
CLOCK)
CM METER READING
IV-"3
VELOCITY
HEAD
(A>t). in. H^O
ORIFICE PRESSURE
DIFFERENTIAL
(AH), m. H.O)
DESIRED ACTUAL
JTACK
TEMPERATURE
DRY CM METER
TEWPERATURE
INLET OUTLET
VACUUM.
hi. H|
JA1PLE W*
TEMPERATURE,
•F
TtMPERATURt,
•r
££L
Vo
Olf.
I
u-.oj^
Mt-
m
uu
L
22.
-7-6
^
2 -f g I ^^ 2-
"Z.oS"
Z.o i
u
.1Z
U.o
MR
2,(o
J 0
JLL:
7fe-z->756
Jl
11,
60
L
13,
oo
t'-^-l
_768.71»
J5.
1>5L
i£l
(7.70
JLi
Ht
\.o7
Jl
0.7V
JA
273/177
78-5.^17
&
67
Jl
2,
t.
J
3,3-
77
7V
ZO. T-
H..--/.'
-------
CLEAN-U? DAT;
Plant £,
Date io/u/7?
Sampling Location fe^
Sample Type " "~
Run Number 3
Sample Box Nunber_
Clean-up Kan
IMFINGIRS
Final Vol.
Initial Vol.
Net Vcl.
#1
/ B 3 ml
#2
ml
ml
3S ml / ay ml
otal Net Volume in Impingers
Comments
#3
T*'
Final Weight
Initial Weight
Net Weight
Total Moisture f'> *?
g
ml
222,
20 0. <
21.5
S £
> e E
" E S
g
S
S
t in Silica Gel 7 ^-r g
ml
ml
mi
Filter Nur.ber(s) 7-
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATE
COMMENTS:
SAMPLING TIME (24-to CLOCK)
SAMPLING LOCATION
SAMPLE TYPE
ANALYTICAL METHOD
AMBIENT TEMPERATURE
OPERATOR _ /-.
gee. -put«u>4 /g> f &— -
~ V*
\^ RUN
GAS ^\^
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 WIN US
ACTUAL CO READING)
1
ACTUAL
READING
Z.I
i«.4
*A
NET
2A
113
b
«w
2
ACTUAL
READING
7-1
i<3 (L
\ *") *"I
NET
7.}
m
0
^
3
ACTUAL
READING
NET
AVERAGE
NET
VOLUME
ZJ
11.3
o
<*>.<,
MULTIPLIER
«/,»
32/100
a/ioo
-/»
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
MJ, Ib/lb-fltole
0.*^
5 , 53^
O
a^.s-ttr
TOTAL ^9,03
EPA(Duf)230
4/72
-------
Plant
.
ISOKINETIC CALCULATION
C &'*'*]
Run* _ , Date
Location ^*^-f *» '?}
) ( BP
( v. )
L
• ) ( 10.S&
)
)
) (
MOLECULAR WEIGHT
Percent 02 by volume dry basis = 02 =
» CO " " " " = CO =
C02 " ' C02=
N2 • 100 - (02 + C02 + CO) » 100 - ( * + )
Percent N2 by volume dry basis = N2 = .
Dry molecular weight s MD
MD * 0.44 ( C02 ) + 0.32 ( 02 ) + 0.28 ( N2 + CO )
MD « 0.44 ( ) + 0.32 ( ) + 0.28 ( + )
MD * " a?,Q7
-------
ISOKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight = MS
MS «= (MD )[1 -(Mx 10'2)3 * 18 (M x
MS » ( O )H - ( °-°Y )3 + 18 ( d.
CP =
VELOCITY
Pitot tube coefficient, type S
Average Absolute Stack Temp. (°F + 460)
Average of the square root of Ap
Absolute pressure of stack (BP ±
Stack gas velocity = \le
V = (85.48) ( CP )
Vc = (85.48) ( .
\
I*.
J_
) (
= P.
z-
3 ?,
in.Hg
ISOKINETIC PERCENT
Average pressure drop across orifice
Total sampling time
Diameter of nozzle
Area of nozzle = A
A = 54.54 x 10"1* (d2) = 54.54 x 10~" ('
I = percent Isokinetic
I =
T
d
- /f
1 n . H , 0
m i n .
in.
( T ) (
(1.667)
0.00267
A )
13-6
sq. ft,
(1
.667)
(
Ts )
0.
00267
(V
L } + I
V ) /
— ^m — M P
Bo. A.
'
AH
13.
6
/
-------
NOMOGRAPH DATA (HP-65)
PLANT
USED ON RUN NO.
CALCULATOR:
SAMPLING LOCATION
STEP
INSTRUCTIONS
INPUT DATA/UNITS KEYS
OUTPUT
DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
14,
142
14,
Run card
Initial i ze program
Enter average T (meter
temp. °F + 460) If meter
temp, unknown, use ambi-
ent + 20°F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacR) [P ± .073 x
stack gauge pressure in
I n . H 2 0 1
Enter average T$
(stack temperature + 460)
Enter Bms
(mole fraction of H20
vapor in cas stream)
Enter KD
(molecular weight of dry
gas)
Enter Cn
(type "S" pitot tube co-
efficient)
Enter average A
Highest A ( )
Initialize "B"
Enter actual Dn
Enter AH*
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
Enter actual A
2
Enter actual A^
P3
°R
c2 ? 5/ in. Hg
In. Hg
92.JT °R
Fraction
tOy of H20
Ibs/lb
^2 9' G 3 mole
•7~—
In. H20
7 "' *n'
In. H20
/ /y
3,*c
A
R/S
R/S
R/S
R/S
R/S
R/S
R/S
R/S
B
R/S
R/S
E
E
E
0.00
^-*
^.js PS
5- 03 1
Fraction
molecular wt
of stack cas
. Ibs/lb mole
/'*
Dn thec.
(nozzle dia.
in inches)
,0 C 3
-------
FIELD DATA
PiAirr.
DATE.
SAMPLING LOCATION
SAMPLE TYPE
RUN NUMBER.
OPERATOR _
PROBE LENGTH AND TYPE &'
NOZZLE I.D. 0
t~V
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE, |P i
FILTER NUMBER Is)
ST'P-
a 3?
ASSUMED MOISTURE. % /
SAMPLE BOX NUMBER J
METER BOX NUMBER C
METER AHp /,V
-------
KANT
DATE
RUN NO.
-------
CLEAN-UP DATA
Plant
Date
Sampling Location_
Sample Type_
Run Number
Sample Box Number
Clean-up Kan \Otx
IKPINGERS
Final 'Vol.
Initial Vol.
Net Vol.
ml (l- ml
ml \ S^ ml
ml
17
Total Net Volume in Impingers
SILICA GEL
Final Weight Z&a.L? g
Initial Weight "lDt> g
Net Weight HS*ia g
Total Net Weight in Silica Gel
Total Moisture
Comments
3 mi ;
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT (_.pr *-*y _V(*l( c<
DATE (0 7/JL J/l4
SAMPLING TIME (24 ht CLOC
$AMP( ING 1 nr.ATION
K) n * *v f" JT Lf' *°- / "_/: W
r*(e+ /» /luohtni'f
SAMPLE TYPE (DAG. H^CTKrEU^frTiF
ANAIYTICAI METHOD ~~~~
liiHihv f rt't^'
,__^ fijffpr
AMfllFNT TEMPERATURE 7^^
OPERATOR •^tf./^^'f
\. RUN
GAS ^\
coz
02(«ET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
NZ (NET IS 100 MINUS
ACTUAL CO READING)
\
ACTUAL
READING
LY
IU
11.1
NET
2-/
/7T
d.o
2
ACTUAL
READING
AJ
llf-
• a r
NET
7-J
m
o.o
3
ACTUAL
READING
l-Y
111
—
JMMENTS:
NET
7- Y
m
AVERAGE
NET
VOLUME
7-Y
113
D.6
VI
MULTIPLIER
*Vioo
3Z/100
M/100
ffl/100
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Mj. Ib/lb-niole
f,&(y
C~ T^
I*
M.Y*
TOTAL n * Q "j
EPA (Our) 230
-------
ISOKINETIC CALCULATION
Plan t
s /-•*'>
Run*
T-V
Location
. Date
. Initials /C
MOISTURE
Net volume of liquid collected
in impingers and silica gel
Net volume of gas through dry
gas meter at meter conditions
Barometric Pressure - absolute
Average absolute meter tem-
perature (°F + 460)
Percent moisture = M
, V, * b 7- 6 ml
r V = ft?' ^^i CU.ft
m
= BP = Q 7.3 J in.Hg
. T . rjj
W ~ "
, , 373.63 ( Vm ) ( BP )
m
100
1 +
373.63
f.
5.5".
MOLECULAR WEIGHT
Percent 02 by volume dry basis
•« CO " " " "
C02 " " " "
N2 = 100 - (02 + C02 + CO) = 100 - (
Percent N2 by volume dry basis
Dry molecular weight = MD
MD > 0.44 ( C02 ) + 0.32 ( 02 )
MD = 0.44 ( ) + 0.32 ( )
02 =
CO *
c°2=
= N
+ 0.28 (
+ 0.28 (
CO )
-------
V$ = (£5.48) (
r
) (
ISOKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight - KS
MS = (HD )H - (M x 10'2)] + 18 (M x 10"2)
MS = ( £ f.*£ )[!•-( - °y r ) 3 + 18 ( .
VELOCITY
Pitot tube coefficient, type S
Average Absolute Stack Temp. (°F + 450)
Average of the square root of Ap
Absolute pressure of stack (BP ±
Stack gas velocity
V. = (85.48) ( CP
z-y
o .
Q, \
, 76 (i n . H,0)
in.Hg
ISOKINE7IC PERCENT
Average pressure drop across orifice
Total sampling time
Diameter of nozzle
Area of nozzle - A
A -_
I «
I =
( T ) ( V,
AH =
T =
d =
2
) s
f'J T in.H,
/? ^ mi
C, * Y2 i
_^
J./JX?'* ' sq.
0
n .
n .
f
t>4
pe
(1
. b4
rce
.66
n
1
x
t
)
IU " (Q*-
Isoki net
( Ts )
) = &S.S
ric
0.00267
)H
(V
X 1 U "
L ^
< Vn ) /PP 1 ( "
T ) I 13
(1.667) (
0.00267
;1
-------
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
/
I
r
«JWT(Loewi»og&\ASi- Gt-vsWfcl V^^ \},^- 2°
DATE 10\«MSR ' A
CAMPLING LDCA
JNSIDE OF FAR
OUTSIDE OF
INSIDE OF NEAR
OUTSIDE OF
STACK I.D., (DIS
NEAREST UPSTF
NEAREST DOWN'
CALCULATOR V
TION fiS^* ^\.i"\lr^r — ^ r\ r-\ r * -r ^ •>-, \
»ALL TO
NIPPLE, (DISTANCE A)
WALL TO
NIPPLE, (DISTANCE B)
TANCE A • DISTANCE B
?EA¥ DISTURBANCE
STREAM DISTURBANCE
/
> 3S. ^-is: "
30 '
1 D '
^p^e
TRAVERSE
POINT
NUKBER
* \
9,
^
q
s
•7
1 i
O*-
QL
i b
II
* ,1-
* ?" -U
f^cuJL
FRACTION
OF STACK 1.0.
.0X1
. DU1
. \ 12
. \"n
^T)
^sL
• 1^4-
. 1 S"D
• %13
, ^ ^-'-u
• ^3
Si ®i
«^Z<- L^'
, i i (i
.C^f^r,^ 1
STACK I.D.
•bs.^ns"
/\
1>S. VI ^
i, -vU^w
PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1/8 INCH)
.-\M
2.. "i"!
U , \~~1
L. U-
^, %4
\ 3L. S^
51 TL.IS
5.U ,S3
a^. \ I
S), 1-
3^. ^
ftto iM
-------
PRELIMINARY VELOCITY TRAVERSE
"*, S .
LOC.
STACK I.D.
BAROMETRIC PRESSURE, in. Hj.
STACK GAUGE PRESSURE, in. H.O — .37^
OPERATORS.
-
SCHEMATIC OF TRAVERSE POINT LAYOUT
-------
NOMOGRAPH DATA (HP-65)
. 10 5>, I Oir\
DATE
USED ON RUN NO.:
CALCULATOR:
MA
SAMPLING
STEP -
INSTRUCTIONS
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
H>
142
143
Run card
Initialize program
Enter average T (meter
temp. °F + 460)m If meter
temp, unknown, use ambi-
ent + 20°F
Enter P
(Barometric pressure at
meter)
Enter P (static pressure
in stacl) [P ± .073 x
stack gauge pressure in
In.- H20]
Enter average TS
(stack temperature + 460)
Enter Bms
(mole fraction of H20
vapor in gas stream)
Enter MD
(molecular weight of dry
gas)
Enter Cn
(type "S" pilot tube co-
efficient) . ~m 3
Enter average A
Hiohest A ( )
Initialize "B"
Enter actual Dn
Enter AH»
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
pi
Enter actual A
P2
Enter actual A
°R
^r^ o
s-ws1"- H9
In. Hg
7 c °R
• -/'•-/
Fraction
O^,J^ °f H2°
Ibs/lb
, mole
_7V3—
In. H20
Or'Z&S — In.
In. H20
o-tr
0-30 -
A
R/S
R/S
R/S
R/S
R/S
R/S
R/S
R/S
B
R/S
R/S
E
E
E
0.00
Tm
/7.7//,VPm
2?-^3 ps
P / T
D /^7 ^v_ S S
Fraction
^•x%'ST~ Dry
oi^-;r" MW
molecular wt
of stack gas
Ibs/lb mole
•^$9
Dn theo.
(nozzle dia.
in inches)
0 . ^
i- ' BO i37
K factor
Tn. H?0
AH /'^
In. H20
AH
In. H20
-------
SAMPLING LOCATION
SAMPLE TYPE £$<\
RUN NUMOER "
OPERATOR Kgr*, -A
AMOIENT TEMPERATURE
OAROMETRIC PRESSURE
WtIC PRESSURE.
-------
PIANT
T
DATE
r—r
RUN NO.
- 7
TlAVERtt
POIBT
NUMBER
AMPLING
TIMC.Min
CLOCK TIME
-------
CLEAN-U? DATA
r.t C O t- A->
Pla
., ., &, ~
D a u e /*s j / G / / o
s^ f
Sampling Location ^ OL^.^ -_^?
Sar.ple Type £ P A ~ /O
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
COMMENTS:
SAMPLING TIME (2«-hr CLOC
SAMPLING LOCATION
SAMPLE TYPE (BAG, INTEGRAND, CO^INUOUS)
ANALYTICAL METHOD
AMBIENT TEMPERATURE
OPERATOR
j
//- ^O 7D
^^^ RUN
GAS ^"\^
C02
02(NET IS ACTUAL 0?
READING MINUS ACTUAL
COZ READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
Oz READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
I
ACTUAL
READING
!.<*
m
ni
NET
*(o
/C,J
^.0
2
ACTUAL
READING
?>
/t.5
/is
NET
14
Hr-7
0>b
3
ACTUAL
READING
—
—
—
NET
—
—
—
AVERAGE
NET
VOLUME
;U
/^.»
/».*
8tf^
MULTIPLIER
44/ioo
32/100
a/ioo
a/ioo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
Md, Ib/lb-mole
^ /f ^
5~-376
O
J*.*W
TOTAL ^ ?. £) /
EPA (Dur) Z30
4/72
-------
ISOKINETIC CALCULATION
Plant V C*->\ , A-O (- (o S.
^
Run* =^ O' f
-> f
Location ^^ C?Wo ^ ^xo
S , v3T
, Date S<*/'*/r&-
, IniU.l,/>
MOISTURE
Net volume of liquid collected
in impingers and silica gel
Net volume of gas through dry
cas meter at meter conditions
Barometric Pressure - absolute
Average absolute meter tem-
perature (°F + 460)
Percent moisture s M
100
M
373.63 (
) (
(
BP
= V.
V
m
BP
m
5~"
ml
7.6^.2
J. 9 - ? S~~
cu.
in. He
S~ 3& * 9 > 7
'
100
373.63
3
MOLECULAR WEIGHT
Percent 02 by volume dry basis
CO "
C02 " " " "
N2 a TOO - (02 + C02 + CO) = 100
Percent N2 by volume dry basis
Dry molecular weight = MD
KD « 0.44 ( C02 ) 4 0.32
MD = 0.44 ( ) 4 0.32
- (
( 02 )
= 02 =
= CO *
= C02=
4
* N2 =
4 0.28
4 0.28
MD =
( N
4
4
CO )
r
1
-------
ISOKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight = MS
MS * (KD )[] - (M x 10"2)] + 18 (M x 10'2)
MS = ( aP )[1 - (O.osrt* 3)1+ 18 (0
X
VELOCITY
Pitot tube coefficient
Average Absolute Stack
Average of the square
Absolute pressure of s
Stack gas velocity =
V$ = (85.48) ( CP )
V's = (85.48) (0,7? 3 )
ISOKINETIC PERCENT
Average pressure drop
Total sampling time
Diameter of nozzle
Area of nozzle = A
A = 54.54 x 10"* (d
I = percent Isokine
I = (1.667) ( Ts )
( T )
I = (1.667) (,>*-•?'*&)
, type S = CP = O • 14 3
Temp. (°F + 460) = T, = 7 s~ 2 - a p <2 OR
root of Ap = u Ap = & , 4 T 3 (in.H?0)^
tack (BP ± Yf-j-j = P^ = 2? ?<2& in.Hq
_ Vs
I ( Tc )
^ ( Ps ) ( MS ) >{Tp —
I vs-y.iva. )
\| A Q'*l 7 *
"" *" *J L. jL
across orifice = AH = /./^^ in.H,0
« T * /A.O min.
« d « O - 3 OS- in.
. 2 _
-------
NOMOGRAPH DATA (HP-65)
- R.T |Ol.lQA~[
DATE
USED ON RUN NO. : Q ~
CALCULATOR:
SAMPLING
STEP
INSTRUCTIONS
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
7
8
10
11
12
13
14!
142
1«S
Run c a ** t4
Initialize program
Enter averaoe T (meter
temp. °F + 460) If meter
temp, unknown, use ambi-
ent + 20°F .
Enter P
(Barometric pressure at
meter )
Enter P (static pressure
in stacl) [P ± .073 x.
stack cauae pressure in
In. H26j
Enter average T
(stack tem?eratu-e + 460)
Enter Bms
(mole fraction of H20
vaccr in ca s s trearr )
Enter MD
(molecular weight of dry
gas )
Enter Cn
\iyps i p i k u k LUUC co-
efficient)
Enter average A
Highest &D ( )
Initialize "B"
Enter actual Dn
Enter ^H«
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
Enter actual A
Enter actual A
P3
-4*z&a^
^ cX~D CR
In. Ha
3 0, ;x.~D
In. Hg
3o, nn
o OR
-! ^^
Fraction
. A,r^0f H2°
lbs/lb
31. 01 Mle
• "7 V3
In. H20
.2? —
, 1 0& In'
In. H20
/.?3
A
R/S
R/S
R/S
R/S
R/S
R/S
p / c
K/ i
R/S
B
R/S
R/S
E
E
E
0.00
Tm
i-T-0
T /?
n.u-m m
^c.»-n s
.^^/T^
Fraction
.^r^" Dr*
P. r y r MW
molecular wt
. of stack gas
lbs/lb mcle
-7/6, -3
Dn theo.
(nozzle dia.
in inches;
_.J$S
v.eos^-L-
tJ.Vt.OB*}
K factor
AH,
In! H^O
AH
In. H20
AH
In. H20
-------
FIELD DATA
FlAHTvLot-m P
DATE I
-------
PLANT
I
S?.X
DATE
10 I* "IK
RUN NO
O ~
TRAVERSE
POINT
NUMOCR
SAMPLING
?
70
ff 0
CLOCK TWE
(74 h<
CLOCKI
/30D
CAS MCTER READING
2-
r^A.
XIX. 13V
VELOCITY
HEAD
(APf). i«. Mj
J_Z
^ZJ_
// /— i
-..^fJ.al
®.4%8b
OniFICE PRESSURE
OirrERtNTIAL
IAH), iti. H^Ol
OESIIIED ACIUAL
{,3-D
A
, s
•/.It
STACK
TEMPERATURE
IT.I/F
^
DRY CAS METER
TEMPERATURE
INLET OUTLET
:z_Z
7?
L
rz
PUMP
VACUUM,
hi. H|
-?.P
2^
£*.&.
, 0
SMtTLEMX
TEHPERATURC.
•F
' 7
IttPWCER
RAT
*f
J>
To
22
-------
CLEAN-UP DATA
JQ3/g Comments
Date |0 ti
Sampling Local
Sample Type E1
Run Number O
Sample Box Nur
Clean-up Man V
IMFINGERS
Final'Vol. -3
Initial Vol.
-|« T^Sttl SWkDt
/ion Qg*rvj«_'\ * o fv^kooS'g- 6t,*T5oi t«/^Q
?P\ M^WoA,*" |o€
~X
nber M- >P<4
- y
WvLowx- -x f^A-<.<^<4^ 4- C,/0/ffc_ q
fo£n£ 3
#1 #2 #3 #^ #5
JB^geR.. ml \ JO- ml O ml ml ml \c
\ VCD ml \SD ml .0 ml ml ml *2\L
Net Vol. & ml 0 2- ml 0 ml ml ml ^
rppfpl N*f. Vnlume in Impineers O5 ml
SILICA GEL
Final Weight
Initial Weight
Net Weight
? g
. f g
/
-------
DRY MOLECULAR WEIGHT DETERMINATION
DATE lO/H/^l T - —
SAMPLING TIME (24 hf CLOC
SAMPLING LOCATION _B--{"
AMBIENT TEMPERATURE **•*•£ 5 *•£
OPERATOR >£/ffi
\. RUN
GAS ^\
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
C02 READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N 2 (NET IS 100 MINUS
ACTUAL CO READING)
*/ yf __ "^CO^JL^L -C\\ —
1
ACTUAL
READING
*-Y
(V(
0.0
NET
a-Y
tut
,*
i
ACTUAL
READING
y.f
/ % /
6.0
NET
M
n*
o.O
71"
3
ACTUAL
READING
—
~-
—
NET
M
ppo
^
AVERAGE
NF.T
VOLUME
a^-77
*&
°*
Wl
^
MULTIPLIER
4Vioo
3;!/100
^/lOO
^/lOO
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
MJ, Ib/lb mole
!.*<>
r.rr
O.o
t?.'7
TOTAL O
-------
ISOKINETIC CALCULATION
Plant
In
Run*
location
S «£L
MOISTURE
Net volume of liquid collected
in impingers and silica gel
Net volume of gas through dry
gas meter at meter conditions
Barometric Pressure - absolut
Average absolute meter tem-
perature (°F + 460)
Percent 'moisture
H 1C°
M
1 H
373.63 ( V _
« Tm } (
100
) ( BP )
\ '
373.63 (&?-7f<3) ( ?0'An)
.. Date
, Initials /n/?Y
= BP
= Tm
r* -
ml
MOLECULAR WEIGHT
Percent 02 by volume dry basis
CO "
C02
N2 • 100 - (02 + C02 + CO) » 100 - (
Percent N2 by volume dry basis
Dry molecular weight = MD
MD * 0.44 ( C02 ) + 0.32 ( 02
MD * 0.44 ( . ) + 0.32 (
02
CO
= N
+ 0.28 ( N2
+ 0.28 (
MD =
CO )
-------
ISOKIKETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight - MS
MS - (MD )tl - (M x TO"2)] + 18 (M x 10'*)
KS = (Zt-C 9 )[1 - (0, 0-3^6)3 + 18 (0-0
VELOCITY
Stack gas velocity
V - (85.48) ( CP
V, = (85.48) (Q.T4
, type S
Temp. (°F +
root of ip
tack (BP ± -
r Vs
1 ( Tr
[i < >>
= CP =
460) **$* Ts =
rfr)"^T:
)
) ( MS )
I ? -f O )
_\j (3&.fO )
0.00267
-------
NOMOGRAPH DATA (HP-65)
PLANT
DATE
SAMPLING LOCATION
STEP
cr-
INSTRUCTIONS
ft.A
USED ON RUN NO.:
CALCULATOR:
- 3>i-(~~4-
OUTPUT
INPUT DATA/UNITS KEYS DATA/UNITS
1
2
3
4
5
6
7
8
9
10
11
12
13
1<1
142
1*3
Run card
Initialize program
Enter average T (meter
temp. °F + 460) If meter
temp, unknown, use ambi-
ent + 20°F 7^/
Enter P 'r^
(Barometric pressirfe at
meterj
Enter P (static pressure
in stacR) [P ± .073 x
stack gauge pressure in
In. H20]
Enter average TS 9-^0
(stack temperature + 460)
Enter Bms
(mole fraction of H20
vaoor in gas stream)
Enter MD
(molecular weight of dry
gas)
Enter Cn
(type "S" pitot tube co-
efficient)
Enter average A
Highest AD ( )
Initialize "B"
Enter actual Dp
Enter AHn
(Calibrated pressure dif-
ferential across orifice)
Enter actual A
pi
Enter actual A
P2
Enter actual A,,
PS
sj 3 °R
3O. c2O In- H9
3O- / 77 In> Hg
7 + 0 °R
^ „ f- Fraction
^),03^ ^ H20
Ibs/lb
Z? . dP7 mole
0 - 7fi_3
O - ^ S5- In- H2°
O. 3o%- In-
/*3 In" H2°
d- ^%
$.1°
O-i*
A
R/S
R/S
R/S
R/S
R/S
R/S
R/S
R/S
B
R/S
R/S
E
E
E
0.00
$ 33 Tm
\7'*> VPm
3^./? ps
^.0- VTs
Fraction
0- f <^ jury
^.7^ MW
molecular wt
of stack gas
Ibs/lb mole
-?&3.%
Dn theo.
(nozzle dia.£
in inches)
^ -££f6 3
C, £n 7/<^
K factor
AH^-^
In. H?0
AH y-5-/
In. H20
AH^-^°
In. H20
-------
DATE ,
SAMPLING LOCATION /ftyS*'
SAMPLE TYPE
RUN NUMBER __=;
OPERATOR
.5
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE. (P,J ~Q.
FILTER NUMBER |i)
PROBE LENGTH AND TYPE;
HO/71 Fl.n <3". 50.
ASSUMED MOISTURE. %
SAMPLE BOX NUMBER
METER BOX NUMBER
METER AHfJ /. k>
C FACTOR
PROBE HEATER SETTING_
HEATER BOX SETTING
REFERENCE AP - / ^
ft Jo
5 r
$~
-i
T7
^/r1"
- r.o17
SCHEWATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY__5l_ MINUTES ^KA^ RATIi^^^PM g/J^'Hg
-------
PIANT
DATE
RUN NO.
THAYEWE
POINT
NUMBER
V
AMPLING
TIME, win
2£=
CLOCK TIME
(74 M
CLOCK)
M MtTER READING
eg. it3
ai
VELOCITY
HEAD
ORIFICE PRESSURE
DIFFERENTIAL
(AH), m. H?0)
DESIRED ACTUAL
STACK
TEMPERATURE
(T$)."F
^77
DRYGAS METER
TEMPERATURE
INLET OUTLET
PUMP
VACUUM.
m. H|
SAKPLC §OX
TEMPERATURE.
•F
TEWERATURt.
»f
3 o.
fi
.77
/,77
-7
133^
3^L.
i2
ZZ
,(,(*
JL°.
2.
-r\
LL.
3-
.2Z
6- 4
JLL
22^
-------
CLEAN-U? DATA
Dat e \ c \\
Run Number 0 —3
Sample Bex Number
Clean-up Kan NAc^gfc < VXfcl
IMFIN3ERS
Final. Vol.
Initial Vol
Net Vol.
r.
Comments:
Sampling Locatl on Do -yUA ~
Sample Type"£Vfi
#1 #2
1S4 nil | ri ml
1 STO r.l \ST> r.l
3- r.l
/X.1- t'1^
^>R.<:
Total Net Volume in I~.pir.gers
ml
SILICA GEL
Final Weight
Initial Weight
Net Weight
g
8
Total Net Weight in Silica Gel
Total Moisture
g
.g
g
13
g
_g
g
_g
Filter NuEber ( s ) 3»0 b feH ? H "
0.) vo-
MRC 7/73
-------
DRY MOLECULAR WEIGHT DETERMINATION
_ COMMENTS:
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION
SAMPLE TYPE (I
ANALYTICAL METHOl
AMBIENT TEMPERATURE
OPERATOR
II ', *Q iA> IV1SS~
'R
CONTINUOUS)
"\^^ RUN
GAS ^\^
C02
02(NET IS ACTUAL 02
READING MINUS ACTUAL
COZ READING)
CO (NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
z,/
11.*
1^.3
SO-
EPA (Dur) 230
4/72
-------
ISOKINETIC CALCULATION
Plant Co.-* 's-ef
Run! -& O - 3 _ , Date /V///7
Location Aa eL$^ S € /I t f . Initials
MOISTURE
Net volume of liquid collected
in impingers and silica gel = VL = 5""^- ' ml
Net volume of gas through dry
ges meter at rreter conditions = Vm = / -^ 6 / 3 cu.ft
Barometric Pressure - absolute = BP = "*>& ' £•£>.._. i n . Hg
Average absolute meter tem-
perature (°F 4 450) ->£. $ 0 = T - 5"
Percent moisture a M
M - - "
+ 373.63 ( V^ ) ( BP
< Tm ) ( VL
373.63 ( & .
MOLECULAR WEIGHT
Percent 02 by volumi
CO "
C02 '
N2 = 100 - (02 4 C02 4 CO)
Percent N2 by volume
Dry molecular weight
MD * 0.44 ( C02 )
MD = 0.44 ( )
ry basis
II M
„
CO) » TOO - (
Iry basis
= MD
4 0.32 ( 02 )
4 0.32 ( )
= 0, =
= CO =
= co,=
4 4 )
« N, -
4 0.28 ( N2 + CO
4 0.28 ( 4
)
)
MD = 2?.0
-------
ISOKINETIC CALCULATION (Cont.d)
HOLECULAR WEIGHT (Cont.d}
Stack gas molecular weight = MS
MS « (MD )[1 -(Mx ID'*)] * 18 (M x 10"2)
MS = (3?-^3)[i - (6.03707 )] + 18
5
->6
VELOCITY
Pitot tube coefficient, type S
Average Absolute Stack Temp. (°F + 460)
Average of the square root of Ap
Absolute pressure of stack (BP ± yf-g-J
Stack gas velocity •- " '
V$ = (85.48) ( CP )
Vc = (85.48) ( ( MS )
1 ( > J6 }
L\| (Jfc.,77) (^,/)J
across orifice = AH =
= T =
= d =
2
n = 54.54 x TO'* ^'^-r) "
r*~.
-°^7^-
/.tr?
72.0
0- 30 C
7 ^ FPS
in.H,0
min.
in .
„
-------
PLAN
DATE
SAMPLING LOCATION
SAMPLE
RUN NUMBER O'T
OPERATOR /L
AMBIENT TEMPERATURE
BAROMETRIC PRESSURE
STATIC PRESSURE. |P,I
FILTER NUMBER (i).
PROBE LENGTH AND TYPE.
NOZZLF ID • >g»J>
, ASSUMED MOISTURE. %
SAMPLE BOX NUMOER.
METER BOX NUMOER_
METER AH,
—7?
.s
AM.
CFACTOR
PROBE HEATER SETTING.
HEATER BOX SETTING
REFERENCEAO-^
rz
TZ-S"
SCHEMATIC OF TRAVERSE POINT LAYOUT
READ AND RECORD ALL DATA EVERY
MINUTES
J
CFM
"Hg
TRAVERSE
POINT
NUMBER
3
A L
.Z_
/o
SAMPLING
TIME, mm
/o
/r
AO
Jo
CLOCK TIME
(74 M
CLOCK)
3
O
$ r
CAS METER READING
3r j. / / 3
353 •
3£ ( • 3 8
is. r- "
JAl^.
^72- >(,
/. 06.
-/7~?/—
\ <
/r, u
HACK
TFMI'EKAIURE
J
-*0a
J7?
7 r
ORYUASHETEB
Tf«Pf.nATURE
INLET
A-L
> 3
•"16
77
OUTLET
60
^ -5"
67
<>?
_/
PUWP
VACUUM.
in. HI
/.
/. 5
SAMPLE BOX
TEMPERATURE
•F
J67
7 <3
7O
7
TEKPtRATURt
Of
3
9
60
S?
<0 <»-
.3 r
o
-------
EX.
RUN NO
TRAVERSE
POINT
NUMBER
AWLIHG
TIME, min
5"
CLOCK TIME
(» he
CLOCK)
1210
CAS METER READING
1V. It1
VELOCITY
HEAD
(AP,). in. H?0
ORIFICE PRESSURE
01FFEHEKTIAL
(AH), m. H,0)
DESIRED ACTUAL
-------
0.3, 1 3
38.8 5
DATA
s n M 5
Comments: ' ,
502- 0 fj
Date
\
Sampling Location
v* Da
'
Run NumberQ-M r-
Sample Box Number T _ 9
Clean-up Man
Final Weight £U 3-- ^ S S
Initial Weight gLOt)- O g g
Net Weight . °i g g
Total Net Weight in Silica Gel
Total Moisture _ • °l g
Filter Nunber(s)
IKFIN3SRS
#1 #2 #3 #4 #5
Final Vol. j QI 3, ml I SS ml "^H ml \ <^ g ml ^-7^ ml
Initial Vol. \S"O ml \ bTP ml f) ml g-CrO Kl g^C-^D ml
Net Vol. 42- ml g ml 3 4 ml - 2.0ml- £ ? ml
Total Net Volume in Impineers fT y ml
SILICA GEL
.^- ,i t\ A i _ - M..J IN.C- ^r~ i ^v _ v\ »..._\, ~ ^^*
^•kU
MRC 7/73
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATE
-
/Q/fr/7?
COMMENTS:
SAMPLING TIME (24-hr CLOCK) /*/' }&
SAMPLING LOCATION 0 "*4r *
/•'
O"Y
SAMPLE TYPE (BAG, INTEGRATED. CONTINUOUS
ANALYTICAL METHOD
AMBIENT TEMPERATURE
OPERATOR
\. RUN
GAS ^\^
C02
O^NET IS ACTUAL 02
READING MINUS ACTUAL
CO; READING)
CO(NET IS ACTUAL CO
READING MINUS ACTUAL
02 READING)
N2 (NET IS 100 MINUS
ACTUAL CO READING)
1
ACTUAL
READING
2.0
111
llf
NET
to
n\
0.0
2
ACTUAL
READING
2.1
M.7
(T.?
NET
3-Y
11}
0,0
3
ACTUAL
READING
z-y
ft- 7
—
NET
j-f
17.3
*-
AVERAGE
NET
VOLUME
?.?
11-3
O-O
P-l
MULTIPLIER
«/»
3Z/100
a/ioo
a/ioo
MOLECULAR WEIGHT OF
STACK GAS (DRY BASIS)
/,*<-
/:/-/
D *o
3.2. y^
TOTAL nftf^
EPA (Dm) 230
4/72
-------
ISOKINETIC CALCULATION
Plant
Run*
Location
jXQ_g>u
MOISTURE
Net volume of liquid collected
in impingers and silica gel
Net volume of gas through dry
gas meter at meter conditions
Barometric Pressure - absolute
Average absolute meter tern-
perature (°F + 460)
Percent moisture = M
373.63 (
) ( BP )
, Date
, Initial \
. - fa/* . '
ml
L ' "
V_ * If 7'b id
EP s ,3<2> -
-------
ISOKINETIC CALCULATION (Cont.d)
MOLECULAR WEIGHT (Cont.d)
Stack gas molecular weight = MS
MS « (MD )[!'- (M x 10"2)] + 18 (M x 10'2)
MS = (3.f<*>3 )[1 - (0.0H-3)] + 18
VELOCITY
Pitot tube coefficient, type S ^^
Average Absolute Stack Temp. (°F + 460)
Average of the square root of Ap
Absolute pressure of stack (BP ±
Stack gas velocity
V = (85.48) ( CP
V = (85.48) (0.74
)
f
I
L\
77
= CP
• TA
Ap
P.
MS
'
(in.H?0)H
• / 77 in.Hg
3. 7<
FPS
ISOKINETIC PERCENT
Average pressure drop across orifice
Total sampling time
Diameter of nozzle
Area of nozzle = A
A = 54.54 x 10'* (d2) - 54.54 x 10r*
I = percent Isokinetic
I = (1.667) ( Tc )|0.00267 (V ) -
m
L £fr7 in.H?0
min.
in.
. ft,
( AH
( T ) ( V,
) (
(1.667)
0.00267(^7) ^ LJZA&
13.6
-------
x«»_
DATE
SAMPLING LOCATION
-Of
10
SCHEJdATIC OF SAMPLING LOCATION
TRAVERSE
POINT
KUV.EER
FRACTION
OF STACK I.D.
fsr^
*- 1 r/.':«r)
/ViT.^3
/J f. 5"
/ ?5" -
/37, tf,
/ 3 9. -T
/ 3?-. ?-
/ J S'. /
STACK I.D.
£^-0*-^
dr.i}^)
tvc . 3*
f? S~
/*£ 5
ft. 7
/yj, 3
PKJ'JL/U! Ur
rns jwwr, i MJ^I i
(Tff h'c/i0F?T 1 ? ih'IH)
«t"^ = 3
tb.ac Pf^ )
/ ?S". SL-
tV ff . 0 /
f. C S~
,'tr/. 9
/?£. CZL,
tr/, 7"
\
TRAVERSE POINT LOCATION i
FROtC. OUTSIDE OF NIPPLF.
(SUfi1. OF COLUMNS 4 & 5>
1
i
EPA (Dur) 232
-------
APPENDIX C
ANALYTICAL DATA SHEETS
-------
I
^
Ct-i
Cl\ X
69- i
a.3
a- 2
16-3
to?
1-z.,
A> B
AMI,
'III
<|7U
'17?-
'l?1
fr07.
Joi-
I
| .VI- 8
j VI-4
1 Joi-M
fl i
ti-j
n- (f
(oT-7
67-6
61 -'<
<.» - /o
j«"J
: \c*• to
(/•'IS
JO O»
O.O2.
711
1.0
o.o MM
O 064
0.
O.K.
I..L.U.U:
LUllJlLk
•. 17 ooi - "IMS"
•lot
MOj
MM)
'IK,
M 1.0
'151
MY1
t.V)
O'K.
I.'IO
781
6.of
10.1
t..}
iJ.C-
!(. 5"
100
loo
Jco
leo
lot)
J»0
Jeo
loo
.!<*>
Joo
lay
juo
100
Joo
1oo
Joo
1OO
Jco
As
f
•Ota
a .O
M-M
. »•*/-
J.I. *'<>
() OOOO
f) . Of» I >
O.'if-VJ
O. OOJi
O v,'a
o.c«.y5"
f.MMQ
0
O . a 7 S $
fi.'l(..S I
f>.
I.'IS
U.I
iUVto'*
5'i y I
' «'(y i
1. ot.
A.fV
6 vi y 10''
Afjv^1
(, flo X AV1
A" P<>^il
I Mlr'< I-1 /vi nr - ^) i 14Vyv i I/if M^
» vt i 1 • C t>»'iVfivi i-:'O Mt
i.
A
j MI in y
UMlcT
M-f)
I ; I 'i
Ai-v.
Culler
Ok^'ttnaf
A(>
>»
J(Hlt/iOL
Mi
Tl
-------
-------
=!«•»-*
"JOT • 1
'k>7- 3
Zol-C
3»1 - I
to7-J»
".jot • 'I
30J-7,
•m
MVI
'•M.
•131
S- »/»•<» J -
6.76
•51 OoM. J
ri ft'Ht 1
'II. U
411.1
VM
'6T ft
>»L/«*
Jno
JftJ
to;
ICTP
3»o
.foo
JCO
• ris"
//fl
3J10
o <* /* i
:, / v to*
*/ >•/» *
V* X"**,
'/« v /O *
vc v to »
SO V /*'
V
i 3 OV30 y 7-
13 - n»r C"-n r v
Vi -liffl Outkr-
t'l - IM (VIM
J-
A«iv t MI-HI o r«\ i >i.«) Hi It
A/I
6 *«
t
-------
APPENDIX D
FIELD VISIBLE EMISSION DATA SHEETS
-------
STATE. 0* U*CH»GAN
Tc^vT
fc! S -U»Cf « COUUlttlOH ^ Ujf,
-• - — t
WILLIAM G M'lltKEN. r,o»»tnO'
DEPARTMENT OF NATURAL RESOURCES 177
L
J Uo*c. >
O J
May 31, 1978
Mr. Lloyd A. Ccx
Monsanto Research Corporation
Station 8., P.O. Eox 8
Dayton. OH 45407
Dear Mr. Cox:
. Please be advised thct ycu have successfully completed the
requirements of the Michigan A1r Pollution Control Cc*w1ss1on'$
°.U'P 336.43(2) for visible er.1ss1on evaluation in Michigan As
of Kay 1, 1978, you met the following qualifications:
(1) Maintained ar averape deviation frwr the correct readlno
of less than 7.5? for a set of 25 white and 25 black
readings.
(2) Had no errors of 20" or more for the set of 25 white
-------
siv "••:,'. Y
r.::cr:n r-r V]b::i: EMISSIONS
Typ-> of Plr.nl
Plant Address (
Type of Diic-.argc?^
Discharge Lcj.Viicn
T
STACK ' OTHER
l:.-ir,ht of Po-int of Disc hire;?
0! i.r-rvor's Location:
f'istincc tc Dis:h2rr- Point
Height of Coscrv£ficr; Point
Direction fro:.' Disc:^rc2 Point
SH*e4-
Date \o/io/-7_if
Hours of Observation to^
Observer L.
Ci^r/'' Ovorcr.st Pertly Cloudy Other
Wind Direct-ion 4s-&^~ S. u!. Wind Velocity S--ID
Color
rv.i/hr
Dctcch-.-d:
Color: t.
No
Cth:r
LLt •;:::: tec' Di:tcncc Pl
L'::.i
x^ " A
or: Lor.ping (Coning
^ ----- .-'''
Lofting Fiiniqating
Visible y^
0
5
10
15
20
25
Other
i n.
sc-c.
Cecity
55
C.O
65
70
75
80
n
DO
100
-------
"R
u-n •& \
ricc~:n r? V;S::L: F::-;;s5io:;s
Typ? Of PU.-V.
Date
Plant Add-?ss
--^6
L'loc-rvcr's Lc-:-?.t icn:
1'istcr.cc- t: r-i£:;-.vr- Po-nt
r i C'
Hours of CbscrvafiCT, i ^ •.o
Obr.ervcr L
^*^
ypC1 Ci U.'r.r.crC? (i,.••.•„;. / C\!:~i:
Wl ! '
K 1
^3*5 Keu
^ .
\
se.
\
LV
11
-?J
~-<5
1 A
I/
/ i
/ \
»
^*o
i:-:r,c!
D?t
Cclc
P; u~.
Otror
0
£,
10
CO
6".
70
7 f:
100
-------
visim.r emissions SUMMARY
C
6 1ft SS . "t?. T .
Run No.
Interval of Observations
1
Start
End
Obs. 1
/I : CD
/*:+?
V*
/?3-
0
/0y
V
V
j>^
3V
/
D
D
0
O
0
M
X\
11.7
0.7
s:^
Obs. 2
/( ^(5
/3^
//A
^5^-
a
>os
^S
^u
/x
0
c,
C1
0
o
6
0
o
t>l.i
*.H
7.1
^.u
0
o
Iflb
1
Obs. 1
/r^
/t H1?
/o?
^A%
0
Sll^
ty
^fe
ii
1
O
0
c
&
o
0
o
\
I5-.1
1VI
! A.t
il. o. >-
o
«* IC>3.
Obs. 2
10 r i
Obs. 1
i
Obs. 2
^
Djration of Observation (min)
Tjtal No. of Readings
No. of Readings Unobservable
No. of Readings {? 0?; Opacity
5%
10%
15%
20%
25%
30%
35%
40?
45%
50%
Percent Readings Unobservable
Percent Readings @ 0» Opacity
5%
10°.'
15?;
20fi
Percent Readings Exceeding 20::
^A-hour clock start and end tirres
2Excluding the time that reodings were not recorded for period of observation.
•VuJ'ms i-.-.uidcd at IL-M.-Lor.d inlv.iv.jls »i,luSJ oLliorvrise noted.
-------
Plant Address
Stack Location
RECORD Of Y1S5BLE EMISSIONS
Date
Observer
Weather Conditions
Observer's
Location
TJMF
K
10
i-iiN' s'i:-.^ ,
CO 15 30 4b
00
01
c?
03
Oi
05
06
0?
r,P
C9
10
11
,,
13
14
IS
16
17
IS
19
20
21
22
23
2«
25
26
27
28
K
O
0
Ls
10
I*
p
c?
5
,c
/y
?~ r
o
0
o t>
0 C
o c
o
J
/v
!f
7t>
0
c
0
O
c
o 1 c o
0*^0
c \o
c o
c
0
0
D
0
0
0
0
0
o
•c
c
c
o
S'
2C
0
c
0
0
D
D
D
0
O
D
0
C
O
0
5
25"
C
0
O
o
7
0
0
0
0
0
o
o
c
c-
o
-------
Rl COH1) 0( VISlilLE [MISSIONS T£
I o/i Q/7 g
Plant M-?T« QQ,.
Stack Location /<
Hc.Uher Condition
1111
Hf.
'/P
) o
fill,
30
31
32
33
34
35
36
37
33
39
0
41
42
43
44
45
46
47
48
49
50
51
52
53
54
5S
56
57
03
59
0"
10
zo
7o
1 >
2?
-io
lo
,5
z°
1$
;f
rf
1$
•/$-
n
o
7?
J*Si
"~Si i
lb
?o
?<-
7"
,5-
/5
r&
2^
ID
75'
l>"
7?
/?'
f
/5
Zo
lo
c
,?
J^-S' -rJUt*. 'K'.T, Otiscrver L- C^
L+~iA- D^OJ- Ot>server's . „ /)
> ^Jf
Location XlM***-^./ f&s&X-
^ O <5 l^ u^-s. •<* |
COMMENTS
""3 '
/5-
?.0
ZC?
Z^
;5
/>'
2
;^
70
7^
70
lO
70
C9
O
yb'
4'-
/:>-
/ Ajj-^e,j? /^^ A.^Jb.
I / '
' ^ ! ' ° _/ J
»M>-C^VT C- ^e* ^
I I !' '' «' H «
/xJx^o, 5j!-t ^ 6-
-------
Company Hame
Plant Address C g-.4
RECORD Of VISIBLE EMISSIONS
' Date
. T .
Observer
Stack Location
O
Weather Conditions
Observer's
location
TIVE
colons
Ib
DO
01
0?
m
04
05
05
07
0?
09"
10
n
19
13
15
17
tUfi. C
IS
T^JL. £• — eJ a-H JL^i-
19
20
o !o
O
21
22
23
6
O
o_
0
! o
0
T
f?
24
c?
25
0
?6
o o
27 , 0 j O
28
0
sap.
-------
RfCORD Of VIS1ULE EMISSIONS
4
Company Name (* ^yv^^c— . t -^d CA^I^I — Date ID/'C'//^'
Plant Address Qi~lA'
/3
;^
/o
/o
s
10
10
5-
5
to
C
0
0
r -R Location /^yi^u^ J&v4j{_
v\ki*s C Jcfl~-o^v_ _. — ,
n x\ » < l— *V *
CO;;HENTS
n.;!'i
31
p
O
0
0
0
D
0
D
O
O
u
o
D
o
-
y ~
/O
'0
/o
/r
/>-
/o
10
0
5
5
5
to
0
0
4'j
D
O
<9
0
0
0
0
V
O
O
o
o
c>
D
0
r
/^
^T
'0
/o
/!r
/5-'
10
O
D '
5-
O
5-
o
0
r fr i > - ^, /a il -^.J^tA-^A-,
mrs-vL-*ffi- %. i ^J /^\rK ^, ^ ^ t^n— C" Ot- ^j*-^*^1 . j,^- L"^^- ^
(,• ^ ^
YTx^a^-j) \^2 /vu^V U^JEA^H^ftJ.
'/w dt c*^ "T *-&***<>-*- T^ ' \^-% • 'A^**^- f. £x. °^| "^ i&. (V ^ **
* 6 /
.**< (j^5
rxjL<,,^^
\
"•
-------
PC
Company flame
Plant Address
Stacfe Location
Weather Conations _£_
RECORD Or VISIBLE EMISSIONS
Dace
.TTAAfc5 HttJLLj^ 'K -1 •
Observer
Observer's
Location
K5
,1
74 IS
m
01
or
03
c-
05
ne
07
n«»
09
1r,
11
1'
t.
C J
0
o
o
o
D
p-
0
o
o
o
0
0
u
tC'.-S
j 5
C
o
o
D
D
0
/N
0
D
^
c
Q
T'.t
30
D
O
0
O
O
0
0
o
0
0
0
6>
0
r
it,
O
O
o
o
D
0
o
b
x—' •
O
O
0
0
coKutrrrs
o
K
is i c !
-------
Rrcono
Ctwipany Name Q, £4^-*^-^- _/\ £*
/^
Plant Address ^r^_4>^*J2 -fccl^a
Stack. Location TJ^CL< V. C^-ai. O
We.Uher Conditions /*_£i-a/v-»— <,
£>
Of" VISIBLE EH1SSIONS
axj-c^ Date ID/iO/TS1
"ic"."! . Observer L . Q t>
i^JjCx-i Observer's
Location S^s^+~-JL
1?
-v
i^P
a^-ri /
TUT
COI-.10TS
UK
' /2
HIN
30
3)
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
53
59
GO
O
O
O
0
0
o
,o
0
o
o
o
0
0
o
Q
c?
0
0
c
o
o
o
0
D
0
o
o
o
0
o
srcc;.'^
15
O
O
O
0
(9
0
O
0
o
0
o
0
D
C
O
t>
D
0
D
o
o
O
C
o
D
0
O
0
0
o
3D
0
o
o
0
o
c
0
o
c
0
t>
c
o
o
o
0
c
0
0
o
o
o
0
o
0
0
o
o
0
0
45
0
o
D
0
o
o
o
0
c?
0
o
o
0
Q
0
0
0
0
o
O
O
o'
o
o
0
o
0
0
o
D
OuJjE^I /OLffr-oU ^r-ojV* JL^LTW. •v-to'/o
1 • '
1 tS
0 Ju-f Ata^A. AP U^t ^
• I;
.
—
-------
R1CORO Of VISIBLE
7
Company tltmc
Plant Adircs
f (v^^^_v- ALio-^^- Date \v/\D/~7fr
0 '
s f c^\ *_J? -fc^JEJU. *R T Observer \.. C*->?.
Stact Location \"^,i.< W— ^ O^-**-<-T Observer's . r
6
Weathe- Conditions
Location -^i/v^T^ 3 -E-oJuJ^
* ir^t -_^ _'
r\ >-t*— ir i
TIM?
HK
n
IS
M;S ;
00
01
c?
03
0-3
05
06
o:
C3
09
10
n
,?
13
14
15
16
17
IP,
19
?n
21
22
22
?4
25
?6
27
28
CO i
O
O
o
c
o
o
o
1C
5
\ o
iO
-5^1 T
s~i s
!0
15
i
i
i
i
«i
1 O
o
C
o
^
o
O
b-
5"
^
5-
,«>'
Cr>«£fffs
-I
1C
'P.t.vcj^^ T^>A*— - -CU- Ufi^lc S^-.dL-
"• i .
t<^'^_
-------
Company Name g,
Plant Address d
RECORD OF VISIBLE EMISSIONS
Date to/to
Observer L.
Stack Location
Weather Conditions £
Observer's
Location
- _ -
/5
• i.
00
Cl
0?
03
04
05
06
0?
OR
05
10
11
12
13
14
15
16
17
IS
19
20
21
22
23
24
25
26
27
?8
79
00
o
0
o
o
o
o
0
0
0
o
0
o
s
$•
o
o
<
10
5
o
fT
O
O
Q
O
o
o
C
0
EuC.,0
; 15
C
o
0
o
o
0
o
0
0
o
0
5
C"
5"
o
5"
5"
5
0
c
5"
o
0
0
o
0
0
0
0
TI
•>
30
0
D
o
o
o
o
o
o
o
D
0
o
,0
0
0
3-
o
S'
0
sr
o
o
c?
o
c?
0
o
o
0
Hf
15
0
0
o
o
0
p
0
o
0
o
o
t-
^
6'
o
5
6"
tT
±>-
tr
o
o
0
0
0
c
0
0
O
•??w<~^ |
COMM[f>-'.:. /VC^^Ar-J
Jv^f S^-^v XA^oJe^
•
-
uu^l>W\;»Jl/eL?/iau)
-------
Co^ipOtiY N.ime
Plant AJdress
Stack location
RPCORD OK VIS1ULE HUSSIONS
Dote 10X1 &/"? ?
-f^LU, K.T.
Observer
Weather Conditions
TIP-:
Observer's
Location
CC"HCNTS
l!K
'/5"
Mlfi
30
31
32
33
34
35
36
37
38
30
^-*
'*/
o
to
i-S
^*
10
o
10
O
0
c
o
0
1C
5
sn
lb
O
0
c?
c
c
o
0
o
tv
r>
•^
0
C
D
r>
\.-
sO
5
0
•\
rf
6
^
/5
^7
0
$
0
1C
5
5
13
3D
O
0
-N
-^
P
0
0
p\
t. '
/-.
'—'
o
o
o
0
c
S"
5"
o
/ 0
Zo
*mS
O
o
/•^
b*
C1
* C
5"
0
.1
•Z
5
«s
2>
V
o
o
t>
o
^-s
V
O
. r,
^-
0
D
O
O
5"
i>
0
o
It
(0
~*
>
tT
/D
O
5
0
o
*
C?
0
tT
-------
Company Name (_,
Plznt Address
RECORD OF VISIBLE EMISSIONS
Date to/i
/o
Observer
Stack Location
c W£>VCA£.
Weather Conditions
Observer's
Location .
WTf
LL
TIML
MIS
00
01
02
03
04
05
06
07
OP
09
10
T
12
13
14
15
16
17
1ft
19
20
21
22
23
24
75
?6
?7
?R
?9
SiCT';D5
00
0
to
0
o
c?
0
D
0
O
0
0
D
O
O
0
0
o
0
0
0
o
o
o
o
er
o
*>
.T
5"
1 D
15
D
iT
0
O
O
O
D
O
'O
o
C
0
0
o
o
O
0
C
o
0
0
o
D
0
10
o
IC7
/O
10
K
JU
5"
O
O
0
O
0
0
o
•o
o
C
0
o
0
o
o
0
o
o
o
o
0
0
0
lo
0
t"
;o
10
13
4!>
5
o
0
o
0
o
C
0
0
0
0
0
o
o
o
o
o
C
0
0
Ji WtA-c^
0 tJ.-k-i- jG~-xvWL Ro~. -^ tx»— sJM *J •
.avo^-V -€O^XL y
•
-------
RfCOKO OK V1SIHLE HUSSIONS
Company K^mc
Plant Addrts
Suck Loeitf
Weather Cond
C (*t/vu^^
on '1^0.^ 'K?^— i-<- t/vjA-Cf\^ Observer's § _ A
it ions C_
Locotion ^;Vox~. g< -^is^^L
k jL>f-^^^ ^-«k
t\ tx^*^ ^i '
TI'T CO'"1[NTS
Hi-1
•/fc
;fc
V.I'.
30
31
32
33
34
35
36
27
33
3D
40
;1
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
on
59
^i
/r
/o
£"
/o
/«?
10
\o
10
1C
;$-
JO
0
-N
^
0
D
O
O
^
S: C>^.'r^
]s
;o
10
10
10
ID
10
-------
sr :•••;,'. Y
p.:co":n rr V:L-::L:. r.y.issi.ri
Type of Plr.nl
Cc.~;p2iy ''""- . C..fr^v^
Plant Address £j%
Typo of ui Lf.:.::rge
bis char cc Locstic:
Date
I D ; i *i -t-e>
Hours of Observation H;OO
Jxu
OTriER
. Q
h.-i(;'-,t oi Po-nl o
:rver s Lccctvon:
[;ist;::cc to Dis-h-irr^ Po'iit
Heiaht of Coscrvit'icr; Point
Direotio'i fro:' Di?.c;;nr-;: Point _t_
:;.r;:-o ::•:.:'.• [--script - on Eiur ±L
rJ-.c-r-: ft'lc-f:;
AI
£
OvoTcr.st Partly Cloudy Other
Hind Direction -f/v^^ A/. £a.^/- Wind Velbcitv
Color __C
3-s" mi/1
DetachLd: fYes ,Tfio
Color: Blcck
I'lur::? Dirpersi cr EiJsvior: Lcr/ping Coning F?.n:n'r.g
^Lofti nc>4(Fiai eating) Other
Lst.-ir.3toc'. Di-thnce: P1u::.3 Visible
~.?ry of 0"
rr. i n.
10
1C
?0
55
CO
65
70
75
PO
GO
TOO
-------
vis:r.i.r
.i! No.
interval cf Observations $t.
t
i
-_.,i »•_ rf p „.,„(.; no,J
.v i.^ i MJ. GI KC^U.HUS
Nc. cf Readings Unobservable
;,:. cf Readings ? C% Opacity
20%
25%
30%
35X
leadings Unobservable
er.t Headings !? Ov Opacity
5%
20;
:c-nt "codings Exceeding
or
6-lAss
Obs. 1 Obs. 2 Obs. 1
(0
7
6
c
o
a?
clock start ar.d end times
. i 0 ;>- i
Obs.
Obs
Excluding the tin;e that
:c-re not recorded for period of observati
-------
Company flame
Plant Address
Stack Location
RECORD Or VISIBLE EMISSIONS
Date
Observer
Weather Conditions Q
Observer's
Location
> ^ fc
UK
0
\v
"MjN1"
00
01
0?
03
04
05
06
07
OS
00
10
n
12
13
14
15
16
17
1R
19
?n
21
,?
?«
25
26
71
sr
CO
o
f)
O
0
o
Cr/.':lS
15
O
O
O
C
hvcf e^ 'Rj^^-vu
* . 0
•"
-------
Company Name (_ C
Plant Address
Stack Loc»t1on
Of VIS1HLE HUSSIONS
Dote
Hc.Uher Conditions
Observer
Observer's
Locafion
COUNTS
(IV
10
M i r;
30
31
3?
33
34
35
36
37
3S
30
* •>
- ^
il
42
<3
44
45
46
47
ig
49
50
51
52
53
54
55
56
S7
Go
5?
>_>
0
^
o
o
*-\
v-y
O
r>
-\
'•^^
0
0
o
r~\
T~S
0
O
D
o
(->
o
0
o
o
0
0
0
c
o
o
G
o
o
sl^J
lb
D
s'
O
O
0
/->
o
0
•C
-/
/p
/*^,
— ''
€>
^
0
D
0
0
D
0
$
O
O
0
0
f~
-X
•^"
^<
<9
:f
^>
0
o
0
/-N
;-/
o
o
r"
o
0
0
o
o
c
o
s-\
•s
o
o
o
4^
^
b"
o
0
c
o
o
0
0
~>
o
0
_
0
o
0
o
o
^
s
o
o
0
o
-------
Company Name C
RECORD OP VISIBLE EMISSIONS
Date
Plant Address C
Stack Location
Weathcr Conditions
Observer
Q
Observer's
Location
RR
Jl
I'.iS
00
01
02
03
04
05
06
07
08
09
10
U
12
13
U
15
1*
17
18
19
20
21
22
23
24
25
26
27
28
79
S
00
D
o
0
(0
0
Q
O
5
0
/o
0
0
C
0
0
O
O
c?
O
O
0
0
o
0
•o
0
o
0
0
0
15
O
O
o
o
o
0
0
s
o
to
O
0
o
0
0
0
o
o
0
o
o
C
0
0
o
0
0
0
0
0
TI
Ij
30
0
0
0
o
0
o
o
5
5
•>
' \
0
o
0
o
o
o
o
0
0
o
0
C
D
0
o
o
0
^
o
•IE
45
o
0
0
o
o
C
o
5
s
5
o
o
o
C
0
o
o
C?
o
o
o
o
0
D
o
0
0
0
0
0
o "R7^ tt X
COMMENTS
•
-
-------
RIXORU 01
Comoanv Name \. fo-.«^— • *^ ^.\ «J; -TaJX^
Stack Location G^< ILS-U^J!. Ow
_rf -r,-^
h'c.ithpr Conditions ^^^--^v C-
f" visiULE E!iissiOrl/'lf
^.3- CXjseryer L. C.^1/
C^Ja-^ Ot)servcr's f
tocot^ on ^,-^t s<&~~~ &*- jcL-^jJ^iL
r\ KU^ ^ i.
COMMENTS
fiK
n
Mir.
3?
31
32
33
3^
35
36
37
38
39
40
41
12
<3
it
45
•'.6
17
48
49
50
51
52
53
5*
55
56
G7
'.'- -
59
:.-•;
C
0
0
r>
D
O
0
C
r-.
o
«?
0
<^
wy
t>
V
1^-.
\_
•3
5
5
0
S'
>•$
V
s*
^s
C'
w'
C
o
0
0
H>n
15
0
0
0
r>
0
P
D
0
.*\
u
,-\
p
C
C
o
C
C
r>
\s
s*
^/
^
.j
i7>
10
G
5"
r*-,
r\
w
0
o
0
0
• ' ' * r ^
3:1
o
Q
0
C
o
o
0
o
,-,
0
0
o
o
3
O
o
•T
>
;o
! *
; -
s
5
O
->/
D
0
C
O
0
.0
45
o
0
o
0
o
o
T;
O
->
u
O
O
0
C
D
O
*-t
5
~j
13
! o
O
0
O
0 •
0
/-
^
0
C
0
>
I F Ju^v~t o
-------
Company Name C
RECORD OF VISIBLE EMISSIONS
Date
Plant Address
Stack Location
o
Weather Conditions
T •
Observer
Observer's .
Location .vdA»<. -t£
/£.
— -
TIMF
"MTH' s"Cf:DS
00
00
01
02
03
04
05
06
07
OP
00
10
n
1?
13
14
15
1C
17
18
19
20
21
22
23
24
25
26
27
28
?P
0
O
o
r\
L/
0
n
0
o
o
is
0
O
0
i)
0
d
o
o
o
0 0
,'N
0
O
n
o
0
c
o
o
o
o
0
O
o
o
^
«=-,
^
•5"
^
0
0
o
0
0
o
0
0
o
o
o
o
o
r
£
of
D
^
Q
s
-r
30
0
o
0
o
D
0
0
o
D
O
0
O
O
O
o
o
o
D
n
p
o
r>
o
^
o
Q
5
5"
0
45
0
0
o
0
D
O
o
0
0
0
O
o
O
T>
f?
0
o
0
n
0
n
c
-
rr
o
f
n
p
0
-r
COMMENTS
X^- £,-Wk /U^ At-^^^J> «]**^ (3
-------
Cc*»pony Name Q
Plant Mdr^ss
Of VISIBLE EMISSIONS
Dote ( '
-p> «.,
. *Y
C*)server J. .
Location rs?v.
We.Uher Conditions 0
Observer's
location
«* 3-
30
31
32
33
-LU
\'i
COUNTS
_i! L
Vb
O
\J
1C . ~T
35
o
36
S °/
38
$
35
4]
42
43
44
0
C'
0
45
0
46
47
48
49_
50
51
5?
S3
54
55
56
57
59
'O
r;
0
0
0
Q
_0_
2_
0_
c
0
Q
o'
-------
Company Name Q
Plant Address C.
RECORD OF VISIBLE EMISSIONS
Date
Stack Location 6<<~<».
Weather Conditions
to
/it /-i
Observer
Observer's
Location
R
/3
M:S'!
00
01
or
03
04
C5
06
07
OR
09
10
11
1?
n
14
IS
Ifi
17
1R
19
20
?1
22
23
24
25
26
27
28
79
sr
CO
0
o
0
S
5
.0
O
10
0
0
T
5
t>
O
r?
T
f
0
n
^
o
5
5T
0
o
0
o
0
6
o
CC'.'DS
15
O
0
o
o
5
13
5
lT
0
o
f
o
(7
5"
IO
fo
10
O
O
o
5
f
0
<
O
0
Q
0
£
0
TIf
30
0
o
o
o
0
5
^
If
o
0
(9
o
o
5
0
<
(9
o
c
o
«;
T
o
o
o
o
r>
5"
<
0
r
41
O
o
0
ID
5
5
ID
£
O
5
i O
O
o
t>~
IO
10
^
0
O
o
o
r
-------
( JH^^H*-
RCCORO or visinu EMISSIONS
Dote
J1/'11
Plant Address _£_£
Slack Locition J2
~1^^ -ftJU.a i^.T. Oliservcr I. /^.j^
^.^ W-^£- O^A-CiT Oservcr's . . „
O
He,it*ipr Conditions f* £|
Location ^-us — •£ -iU^-U;
ji^A- j ^ , - . ^
*-
o
o
D
0
0
o
o
0
c
3
•5
5*
-------
Ivp? of Plr.nl
-|
Date
Co"r'2ny MC>.~ - C e>i
Plant'Address £
Type of Di:cna<-cervS-ACK
[)isc!:-r.rce Lc:^ticn
!: ir.ht o' Point o"
("."•server1 s Location:
Distance to Dis:h~r>-2 Po^nt ^oo '
Height of C.~;cr\'Cticn Point o/\&±
Direction fro:.- Disci.?.r?2 Point
Hours of Observation i«?-. ov-
F - c; -; r o -,r. d [; :• s or i p t -; c-r. tL^_Sfc^ jr^_£.ci^2iik. Jt±^t_2^
Ovorcr.st Pertly Cloudy Other _
Hind Direction -T^»-~ V\. uJ.
Color
V.'inci Velocity 3-S £i/JZ-
1
Deti^ iv ?•' YeE
Color: Blc-.ck
Jlu-.e Dir;p-jrsicn Ei!;2vior: Lor-ping Coning Frying
••toftTnS^ -J^Fii-ii gat i ncn Othe r
v^ \L^
Isliratec; Di.thnco Plur:e Visible
^ry of Gbservatio-:
0
5
10
10
'<"'.•
n.
Srj
CO
•65
70
80
(.."
CO
100
-------
visi!1.! r rMISSIONS r.u^R
\~Y\
's. V
i
i
i
I
i
i
I
i
1
i
t
i
1
j
1
1
!
i
i
i
-jf —
r»o . i o
Obs. 2
i
f
!
i
i
i
i
i
i
i
i
!
i
i
i
'
3. 10-5-1
Cbs. I
1
-
'
1
i
Obs. 2
*
.
?r
Excluding thv ti'".c- tnat rejdinrjs were not recorded for period of observation.
-------
Company N.«me (_, {^•^t/»^-«~
Plant Address C C^O^/W-
Stack Location *3o-c W-A.
We .ithpr Condi t ions £_ JQz
RKOKU or visniLE HUSSIONS
-XL -oJuv^-i- Date
c -• - -
fi. ^pJLL^ R.I- Observer
i«-^£ DiA-iJU-i" Observer's
Location
-^u*! 1 ^*<-^^*^~Sr-
"
1 O/ll /7 f
L. Ccr
xU^-J,
•£
^
&~*&
u^.* 3
IIH
1 *v
r Mir;
3"!
31
3?
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
53
53
54
55
56
G7
SO
59
:M
C
o
0
•o
O
o
0
0
D
0
O
0
0
0
0
sn
ib
o
o
0
0
0
o
0
0
0
0
0
0
0
0
0
r:,'^
3~
O
o
o
D
0
D
0
0
O
0
0
0
O
0
0
45
O
0
0
o
0
o
D
O
D
O '
0
0
0
o
0
S-fovf H VvU-TU-e/ ^ ^u-~_
Q
_
-------
o.
RECORD Of VISIBLE EMISSIONS
Company Name _v
Plant Address ft L-
Stack Location f^
-fiJ^
-T .
Observer
I.
Weather Conditions Q JJ
Observer's
Location
w '
/c-
!^ " •, "
DT
C1
0?
03
04
05
Of
07 j
0?
C5
10
11
\?
13
1-1
15
.<
17
IS
19
?0
?1
?2
?1
?i
?5
?6
?7
?6
79
i-_
rO i
c
ol
0
0
0
0
01
0
0
0
0
c
0
o
•\
/
c
0
<~
\^
o
c
0
0
D
O
0
o
5
1C
5"
0
-r.^
is i
D
O
O
o
c
0
c
D
0
0
^
w
Vv
O
o
/"•
0
o
0
D
^*
\J
0
o
c
o
0
£.
c
5"
o
c
TI*
30
o
o
0
0
r"!
c?
Q
0
0
w;
0
_'.
c
o
o
o
c
\J
c
0
6'
o
r/
0
0
0
tl_ c~ - ^.4 c^c lc ,'w-^ t~\e^ a Lt^.4 ^JU4_
-
-------
"p,,
CoRtp^ny N.inir
RrCOKO OK VlSlULl EMISSIONS
f* «A t AA^ n 1 1 p ID / i / "i s<"
Plant Address _Q_fr~
Stack Location ^o
Wc.ither Conditions
AA~£ 4V£JL&- ^?.T. ^server L. dr>i
U1^ V^-.-Lj. (D^-^t-' Observer's ( t n r\
CXt
Location S^A*- — * -*XA*E<.
a^^ -~p r1 '
Tl»T CCMIENTS
UK
It.
Hfi
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
59
1 srcc:ins
H 15
o
,
O
O
^
5"
^
ID
tT
o
10
0
Q
0
0
D
$
^
O
O
0
0
0
0
o
•o
o
o
o
o
p
0
0
p
cO
/O
;o
r
o
/o
5-
•o
0
o
0
0
0
o
c
o
o
0
o
0
0
c
o
o
o
3T
o
o
o
0
^ ^L£^^4r U^UL r.Lu_c^.
fl "u. ^t^-VjL JA^- /J.f ^
^~- ^
' ' r _/ ' -i • /j*
«i ck^— ^^- <±^k^ JA*~~- AA*.-^ P^-
rl, , ^ v^x^>n ^ HJPeLj.cc O^c^.
T5II" 4 J> r^J^_ J^A^ ^JA-^^aU^ce,
** • M s "^ i>
_^. ^^.ajB^_ ,. UwjtJ. ^-^i-c^
f' C
O
__ — .,
-
.
-------
Company Manx; _
Plant Address
Stack Location
L.
Weather Conditions C •£*-<
RECORD Or VISIBLE EMISSIONS
Oate
? .T
Observer
Observer's
Location
Jlfi
n
~M:S
DO
Cl
C?
03
0-J
05
06
n?
r,p
C?
10
n
12
13
14
15
',6
17
IS
19
?0
?1
?2
?3
?4
35
?6
27
?8
?9
•!
00
J>
c
0
0
o
0
0
0
C
-V
0
5
b
C
5
<,
0
0
f
5
5
C
/o
/C
0
o
o
o
0
O
is
D
0
C
o
0
o
0
0
(.>
C
C
o
5
5"
r
>"
C
c?
/o
>"
o
5"
/o
0
o
o
0
0
0
6
T!
5
3«'
c^
O
0
0
O
0
o
0
^
0
5
5
5"
<
;o
s"
0
5~
fT
/iT
0
5-
5
0
O
0
0
C
o
0
O
D
0
O
O
O
o
D
.• >
^v
;o
<~
±T
r
c?
5- 1
•^
-^
S"
/o
C?
/o
5"
C
0
0
D
0
o
o
cocr^s 7?"~-.u ^>
•
-------
RfCORlJ OK VlSlllLt EMISSIONS
Company Namr _Q gr
Plant Address £_C-
Stack Location f3
i^v^ —
^A*J
C -^.^>w^ Date l o/» >/-)•*
G „ ^
^ -f^LLt 'K'.T. Observer L. C.^
ec<. kpv^X {PuA&A" Observer's
O
We.ithrr Condi tions C-£v»
Tlf
UK
' 17
Mlti
30
31
32
33
34
35
36
37
38
3D
40
41
42
43
44
45
16
47
48
49
50
51
52
53
54
55
56
57
53
59
on
0
O
0
0
0
0
0
0
0
0
o
0
0
0
o
o
5-
5
^
s
<
-
,^
^
5
5
5"
£-.
5
r
lii
D
O
0
o
0
0
o
o
o
0
0
o
o
D
O
O
tT
5"
^
-
<7
^
^~
r-
fT
5
5
5" '
cr
5"
Location ^iA/>c«^ — ^. ^y^->A^
>N- , ^u~. JL&-*,~ *^- (ttk-\, i ~
« K^u^- »£ 5
CO;-.HENTS
iliirS
31
C
L>
0
^
C?
0
0
o
o
o
0
0
O
O
0
o
:>-•
b'
5"
tT
5"
s-
5-
<
^
^
5"
5~
^
IT
45
O
0
0
0
0
o
o
0
0
0
o
0
o
0
0
o
10
<
5"
5
<
"5"
5-
5-
s'
5"
5-
5-
5"
Ku^ VUt^J- jt^U^ U—,ldU^<, • P— >"
0 "
O
PJ. . ! *• _ * ' "4- r t J. C -1 si1
(TV-l C A. fX^^^ <:V^' s**' \.-$^*-** £—
-------
RtCORO Of VISIBLE EMISSIONS
Company Name (/ 9\s+^u~^.c^ ^it^^>4^
O
Plant ^d!J^ess Q i~*.\.f.*I -f •-££}, X.T.
Stacx Location ^L^v^-*3^**-1- O-~>-£*-~*
"^
Vsathe- Conditions fjioy^
Date 1 o/i i /7'S
Cfcserver l~ . C jf.
Observer's .
Location . *^/. C e« ^, ^x*-<-<
IME
*" 3
iOOi IS
TT
00
5 ?
r
01
C?
03
O
04
D
05
Oc
07
cr;
11
12
13
15
16
C
_U_
18
21
22
23
Ji.
25
J6
27
?8
-------
si:1 :•••,-Y
RECORD o? Y3$::LF. ?.:-;issio:is
Ty?? of PI i'.nt
J
Date CV1
I 0 ; > 0 4
Hours of Observation m:o
-------
vis: "i.r rrissi c.1;^
C Qr
-r\
i O/l
serv-Kioni Star: i
.r-3.fi or. cf Observation (nun)
T--t"i1 No. cf Readings
V;. o'" P.-:-acings Unobservable
',;.. of Readings @ 0" Opacity
5%
20^
252
30%
35%
;?r:€nt Readings Urot-servable
^erce'.t Rssdings i? 0 :. Opacity
5r;
1C-:
15",
20,
Obs. 1
,0fe
!
i ,,,
*y**5> o
£3 ij if
0
' :
Obs. 1
i
i
!
j
)
i
.
i
1
i
i
i
ii
i
(i 103.1
Obs. 2
r
1
il
i
•• t
P
i
i
!
i
DiTi
Obs. 1
I
j
|
|
i I
i
j
i
1
i
.
il
i
Ii
i
!
!
r»Kc ?
w ^ i . L
\
f — —
— -
2-l-ho::r cloci-. start or.d e"ri f>es
?£xcludinc tne tii::e that re.vdinqs w»re not recorded for period of cbst'-vt
-------
Company Name C OA^L
Plant Address C.
RECORD OF VISIBLE EMISSIONS
^J^nA Date to/tz./-??
"^ .T . Observer L-
Stack Location
Heather Conditions
Observer's
Location
Rs~
10
"I'TTTT
OT
Cl
0?
03
04
C5
06
07
08
09"
10
n
12
n
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
?9
SF
CO !
i
1
O
S
10
0
0
o
^
n
0
n
f!
0
0
0
o
o
o
O
O
O
CC'OS
111 T
o
o
6
s-
cp
0
9
r>
0
0
^
5-
o
o
0
0
o
0
o
0
TIM
30
o
.j-
<
s-
o
D
r
O
o
,0
0
fT
o
p
0
0
0
c>
0
0
E
4L
O
5"
f
^
c>
o
£•
0
o
(9
0
r
0
o
o
o
o
o
o
o
COMMENTS 'K>i^v- tt ^
^OA.-! ^ YT^Jkx/ ^ ^£^
-------
Plant Address
Stack. location fA,, W.»—u,
Of ViSIULC HUSSIONS
Dote \_C
Observer _
Observer's
Location
ilt'
• \o
•
v.i:;
30
31
3?
33
34
35
36
37
38
•JO
i:
4!
4?
43
44
45
45
47
48
4?
SO
51
52
53
54
SB
56
07
03
59
0
o
O
o
£
Q
-\
r,
0
c
0
h'
o
c
0
e
0
0
0
o
o
0
0
p
c
0
c
o
o
ib
0
o
o
0
-
0
D
2
o
•"
c
r-.
0
C
D
0
r,
O
O
0
D
o
o
0
0
0
0
C
o
o
t;-;^«,
3
D
C
O
0
o
o
O
9
&
0
O
c
o
o
o
c
0
o
o
o
LX
o
0
o
0
o
0
0
c
o
*• -
0
o
D
o
o
o
o
0
.->
c>
o
o
o
o
o
0
c
D
o
0
o
o'
o
f.
d
o
o
c
o
0
-Bortk _ «.Utk ,u*-v-a, /.jw^xv-j^c*
-
-------
Company Najne _J
Plant Address (
Stack Location
RECORD OF VISIBLE EMISSIONS
^-^^- Date /s/;7 /?F
-To-tLfc. K .1. Observer I, C >/
Weather Conditions
Observer's
Location
^-< _
HU
//
00
01
02
03
04
05
06
07
na
09
10
n
12
13
14
15
16
17
IS
19
20
21
22
23
24
25
26
27
26
n
s
00
O
,*>
0
0
c
O
0
O
0
c
0
0
O
O
0
O
l)
c
O
0
O
0
O
V
O
c
O
0
c
•0
15
O
O
V
0
0
0
0
D
0
O
0
0
0
O
D
O
0
O
0
0
O
0
0
O
O
O
0
c
0
0
TI
3'J
O
o
D
o
0
o
0
0
0
0
0
D
0
0
(•>
0
o
D
o
0
o
0
o
c
o
o
0
o
0
o
Mt
45
o
0
o
0
o
o
o
^
0
0
o
o
D
0
c^
D
o
0
0
0
o
0
o
o
o
o
c
o
0
0
COMMENTS 'TXU~- -ft '-i
A JfjU*r ^C^>!<^d? c-^t^^ w^^_ J^L
-ri^. WcA^ruE* <£
*
T3£tt, ^^, ^Ld- jL^^c^^L^^jJL, • ^
u<~-jaxrT_~-*^ ^ ^
.
-------
OK vising
CcK^p^ny h*Tnc \_ ^~-.^»x»— — *•" _/£-T*-TT' s, •&,
Plant AJdress C j£-^^*^£ -TiJlij. ^7.1.
Stack. Location T^a-^U,^- — <>_*_ G — l^tJ"
We.1.!*?'' Conditions (/ -i-£,^ ^.M-^** v
0
Dote VD/il/
Observer L . C
Observer's
Location _-i/tfi*i—
7S
» _--,/•
xii ji£*x^kL
rs t*^^ it ^y
T!'T
CO^IENTS
US'
!/
"- 1 •'•
30
31
32
33
34
35
«
,7
36
3D
,,-
11
• 2
43
t.
45
'.6
47
48
49
50
51
52
53
54
55
55
„
S3
55
.M
<^ i
o\
o
c>
r,
>
0
^
"
o
n
c
r
C
D
<^7
.-
O
D
o
c
o
C
o
o
o
O
C
o
C
-o
srl
is
>
O
0
0
0
0
0
o
c
o
C
V
0
C
o
o
o
C
.0
o
0
o
o
c
0
o
0
o
C
o
,':;'"<,
j •
O
C
o
o
0
C
C
o
C
C
o
0
0
o
o
0
0
0
o
o
0
0
o
o
-D
0
o
o
C
0
4:
0
C
0
r>
0
C
o
C
c
C
c
•
0
o
— '
0
0
o
o
0
0
0
o
o
o
o
o
o
-------
Company Hanc C.
Plant Address C
Stack Location
Weather Conditions C
RECORD OF VISIBLE EMISSIONS
Date ID/I :,/•?%
.1. Observer L.
Observer's
Location
HI!
\2.
H I N '
OT
01
0?
03
OJ
05
06
0?
OR
09
10
11
12
13
14
!<;
16
17
1R
19
?0
?1
??
?"!
?4
25
?6
?7
?R
79
S r
00
o
D
O
O
0
o
o
o
0
o
o
C
r~i
o
0
,•">
o
0
o
o
0
o
D
<3
'O
o
0
o
o
0
CC'OS
15
o
o
0
0
o
0
o
o
o
o
o
o
C
0
o
C
0
0
o
o
0
0
0
o
0
o
0
o
o
€
TIV
30 1
D
o
n
Q
0
o
o
0
•o
o
o
C
o
o
C?
D
o
0
o
C?
0
o
o
o
r?
o
\D
o
o
0
f
45
0
o
o
o
o
s~\
•o
0
o
0
o
D
o
o
~N
\^s
o
C
0
o
0
o
o
o
0
o
o
o
o
0
o
COMMEOTS
•P ''-'V C ^ * *• vt<- tv^. oJf^u/^ kJ^-C
L
•
'T3
-------
KfCOW Ui" VISI1U.E C'HSSiONS
___ L5y 1"Z
("'server's
Location
3O V. )
R^-.^ M
T!f[
•f.
1Z
" i II
-^ ^
) .
31
3'
33
31
35
36
17
38
33
o
il
12
i;
• r
•'.6
•"i?
* ^
49
50
51
52
53
5*
55
56
57
^.T
fO
7
0
0
o
C
0
0
o
o
C
O
o
a
/•>
o
r>
D
•>
•>^
r^
D
0
0
0
0
0
0
D
0
0
D
P
,, .
v •_
IS
o
0
(9
O
0
0
0
o
0
O
0
C
C
~\
u<
•:-
/-t
o
o
C
0
0
0
o
0
0
0
o
0
0
0
. . . v-
"7 "'
0
0
o
0
o
0
D
o
J>
o
0
o
C
Q
D
o
0
D
0
0
0
D
0
o
o
t>
D
0
o
0
4 '
o
o
D
Q
o
o
o
o
o
0
o
o
0
^\
_^
0
Q
0
^-s
w
o
o
o
0
0
o
0
0
o
0
0
0
--^ . • t • i
r-' f J^ 1 ! ' -X- "T~ * ' ^
r£*^-^f-tvy d-t *<>_SC^, ^>i<-I-i ^^^^^ ^X^I- l^^f,*^.
C J? j . >vj
4. -t^T tH £~i^~*~ .
jJ^Sjj~r p^u. — ^f> t\s-t^- fL^Ju^^ d-s-^u — w _. Q~~u*~
' (/
«^.£t^ ^ 0>dJter i±<^4, ^ZAs^Zvid
V
JX- ^.faa.,V .Ax«x--v^ /v-C. ^/i.L ._vs^^ic(.
*
-------
Company Name
Plant Address Q
Stack Location
Weather Condi tions
RCCOPO Of VISIBLE EMISSIONS
Date l&/i./-lg
Observer *- . GJ^£
Observer's
Location
u^v — •..
K
\l
TIM?
M ! N ' '
00
01
0?
03
04
05
06
0?
ns
09
10
n
12
13
M
15
16
17
18
19
?0
21
22
23
24
25
?6
27
?8
?9
V Ll'.Jb
00
O
o
o
0
o
0
0
D
t '
0
.•^
<_/
O
b
0
o
0
o
0
0
0
0
0
o
0
• o
o
0
0
(9
o
Ib
o
o
o
o
o
o
0
0
o
0
0
o
0
o
o
D
o
D
o
o
o
o
0
o
0
o
0
0
0
o
Jl'
0
o
o
o
o
o
o
0
0
o
o
D
0
0
0
o
0
0
0
o
0
o
o
0
0
0
o
0
o
o
45
o
0
T>
0
0
D
0
o
o
0
o
0
0
o
0
D
o
0
0
0
o
o
o
0
o
0
0
o
o
o
COMMEfttS "Re— * *N
f^ o_c,kl -r^*^~- j( '.^ jU~f, ^U- u^CtV.. <><.*^A
-------
RCCORO OK VISIBLE HUSSIONS
C o*^ P ii n y ^3 n*o
( i*.^_--v , g; .^iX^-'i-'U-' Date 'O/'^-/"7^
Plant Address £, o_Axw»J2 -taJ-La- "?.T. Observer L. doi"
Stack Location "^W* VvO-(-*-t C^-CjH Observer's
U
We.ither Conditions 5 -^
^ Location >C*^u^«-(^ ^"isSJt,
<.j_cixv ( "• ^5 o tv> ^
0 ' l-*
J-
V. I '.
30
31
32
33
34
35
36
37
33
30
t~
1]
62
43
44
iS
46
47
48
4?
50
51
S2
S3
54
55
56
57
„
59
•*^.
0
L/
0
0
-)
o
n
J^
^
•~
D
$! i_r-i.rS
is
o
c
0
D
0
^
D
o
O
.J*
o
C> 0
0 | C
"^ i
0
0
O
L-
O
c
0
Q
O
D
0
O
0
c
0
0
o
0
o
o
o
Q
O
o
o
o
o
o
0
:>
O'
0
3?.
O
0
«• *
0
0
O
O
O
r>
O
O
D
O
O
D
O
0
O
O
O
D
0
D
0
0
O
O
0
O
O
C?
-\
0
0
-
.D
0
0
0
o
o
0
o
t)'
Q
0
o
D
c
o
0
o
"5-CtX. 'uvv^-Wk. /Vu^^ ri*-£- C«~- ^^J^ .J- 13,
*
. 1 * . . f
_— t , * 1 1 - I - f> ' fi
\ \fi-X~ >t*-^-V\_ C-^ £j-X- T
-------
Company Name C
RECORD or VISIBLE EMISSIONS
Date
Plant Address C q-^Vw^ -4
C
It
4i>
O
0
o
o
o
o
COHMEhfTS
&^<£ *-\ N^dUcS^ ^ C^sec^r^ v6—
-------
APPENDIX E
ANALYTICAL METHODOLOGY
-------
A variety of sample types were analyzed to provide arsenic data
on the Corning Plant. Product samples, feed material, slag, and
air filters, as well as impinger solutions, were received for
analysis.
Solid sar.ples (product, feed, slag, and filter materials) were
dissolved by acid attack in a pressurized vessel.
Liquid samples (0.1 N NaOH impinger solutions) were acidified
using concentrated nitric acid, and subsequently digested by
gentle evaporation and continued additions of acid.
The digested samples were evaluated for arsenic content by
Atomic Absorption. Samples showing high arsenic levels were
quantitated using Flame Atomic Absorption, while the low-level
sar.ples were quantitated using the hydride generation technique.
Correction for background absorption was used for all samples.
Those sar.ples analyzed by Flame Atomic Absorption have a limit
of detection of one (1) part per million (ppm) or one (1) micro-
gram per r.illiliter (-jg/rnl). These samples analyzed by the
hydride generation technique have a limit of detection of one (1)
parr per billion (ppb) or 0.001 microgram per milliliter
(O.OC1 -.g/ml) .
-------
APPENDIX F
PROJECT PARTICIPANTS
-------
PROJECT PARTICIPANTS
Dar. Bivins
Killiar, Kerrinc
P^D^SCt C'~ ~ i C £""
Emission Measurement Branch
Production and Process Control
Emission Standards and Engineering
Division
Mcnssr.tc Research Corporation
George Bail
Darrell Harris
.Mark Thai nan
Robert Wachter
Keith Tackett
TA i 11 i arr. Me y e r
Michael White
Thcnas Malone
Charles Clark
Lloyd Cox
Jeff Workman
Car-en Church
Patrick Hughes
Connie Hayes
Dave Gloekler
Joan Kecathorn
Contract Manager
Contract Manacer
Research Cher.ist
Research Engineer
Research Engineer
Research Technic_an
Research Technic.an
Research Technician
Research Technic.an
Research Technician
Research Chemist
Senior Research Technician
Research Technician
Research Chenist
Research Chemist
Secretarv
------- |