ENVIRONMENTAL PROTECTION AGENCY

             OFFICE OF ENFORCEMENT
                   EPA-330/2-77-012
                Emission  Testing

                       at

            Marathon Steel Company

                Tempe, Arizona
                  (APRIL 12-16, 1977)
NATIONAL ENFORCEMENT INVESTIGATIONS CENTER

              DENVER, COLORADO
                       AND                .
                                         $ £*
                   REGION IX
           SAN FRANCISCO. CALIFORNIA

                     JUNE 1977

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              Environmental  Protection Agency
                   Office of Enforcement
                    EPA - 220/2-77-012
                     EMISSION TESTING
                            AT
                      MARATHON STEEL
                      TEMPE, ARIZONA

                     April 12-16, 1977
                          June  1976
National Enforcement Investigations Center - Denver,  Colorado
                             and
            Region IX - San Francisco, California

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                          CONTENTS


  I  INTRODUCTION 	    1

 II  SUMMARY AND CONCLUSIONS  	    2

III  PROCESS DESCRIPTION  	    3

 IV  TEST PROCEDURES	    6

  V  TEST RESULTS	12
                           FIGURES

  1   Old Baghouse Station  1  (0401)   	    9

  2   New Baghouse - Stations 2  and  3
       (0402 - 0403)	11
                           TABLES

  1   Process Weight Summary 	    5

  2   Data Summary - Station 1	13
                                •
  3   Data Summary - Station 2	14

  4   Data Summary - Station 3	15

  5   Visible Emission  Summary  (Opacity)  	   16
                        APPENDICES

  A  Presurvey Inspection  of Marathon  Steel  Company
  B  Production Data  and Process Weight  Calculations
  C  Stack  Sampling Equipment
  D  Calibration Data
  E  Source Tests
  F  Chain  of Custody Record
  G  Particulate Field Data
                             ii

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                            I.   INTRODUCTION
     Marathon Steel Company, Tempe, Arizona manufactures  steel  reinforc-
 ing  rods  from scrap steel melted  in three electric-arc furnaces.  After
 melting,  the scrap steel  is refined and  then cast  into ingots.  The
 ingots are  heated and rolled into reinforcing rods of various diameters
 and  lengths.  Two baghouses (old and new)  control the emissions from
 the  furnaces, casting and other sources  [Appendix A].

     On November 15, 1976, National Enforcement Investigations  Center
 (NEIC) performed a presurvey inspection  requested by Environmental
 Protection  Agency (EPA), Region IX, to determine if the baghouse emis-
 sions could be sampled.  It was concluded that sampling was feasible
 provided  that minor modifications be made on the old baghouse stack
 testing platform.  No changes were needed at the new baghouse sampling
 location.

     During the period April 12 to 16, -1977 the baghouse emissions of
 Marathon Steel were tested by NEIC to determine the compliance  status of
 the  plant with the Arizona particulate regulation (R9-3-306).    The
 allowable baghouse particulate emission  rates were calculated with the
 equation in the Arizona regulation and the furnace process weight
 rates.  There are no limitations on particulate concentrations.  Visible
 emission observations were also made and compared to the Arizona opacity
 regulation  (R9-3-301), which limits the emission opacities to 20%,
 except for excursions to 40% for five minutes.
 *  Designation used by Marathon Steel.
**  The plant is located in the Phoenix-Tucson Air Quality Control Region.
      =       O.62
                                                                          .
***  E = 3.59 pO.62^ uhere E ±s the allowable particulate emissions (Ib/hr)
     and P is the furnace process weight (tons/hr).

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                     II.  SUMMARY AND CONCLUSIONS
     1.  The participate sampling results are summarized below.
Particulate Emissions
Baghouse
Old
New
Process
Weight
m. tons/hr
7.2
17.0
Al 1 owed
kg/hr
5.9
10.0
Ib/hr
12.9
22.1
Actual
kg/hr
6.0
2.9
Ib/hr
13.3
6.4
%
of allowable
emissions
102%
29%
     The plant met the requirements of the Arizona process weight regu-
lation.  On an individual basis, the old baghouse emissions (furnace
No. 1) exceeded the allowed emissions by 2%.  The new baghouse emissions
(furnaces 2 and 3), however, were only 29% of the allowable.

     2.  The baghouse visible emissions are in compliance with the
Arizona opacity regulation of 40%.  Visible emissions from the old and
new baghouses averaged 7 and 5%, respectively.

     3.  The average particulate concentration from the old baghouse is
more than eight times that of the new baghouse.  The possible causes of
the high particulate concentration include bleaking bags, the bag
cleaning cycle, suitability of bag material, etc.

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                       III.  PROCESS DESCRIPTION
     Marathon Steel manufactures steel reinforcing rod from reprocessed
scrap steel.  The Company operates three electric arc melting furnaces
(capacities-22.7, 22.7 and 27.2 m. tons) which are the major emission
sources.  Other emission sources include ladle cleaning (skulling),
casting, and fugitive.  The furnaces and skulling emissions are col-
lected by hoods and ducted to two baghouses.  The fugitive emissions
from the hoods and casting area collect under the building roof and are
also vented to the baghouses.

     The furnace No. 1 emissions are controlled by the old baghouse
(Station 1).  The baghouse uses Nomex  bags to clean 1,700 m /min
(60,000 acfm) of gas (air to cloth ratio of 2.3:1).

     Furnaces No. 2 and 3 and the skulling emissions are ducted together
and then split to the two sides (north, Station 3 and south, Station 2)
of the new baghouse.  Both sides have Dacron  bags and each clean 2,820
act. m3/min (100,000 acfm) of gas (air to cloth ratio of 2.7:1).

     The ducting to the baghouses is interconnected so that the gas
streams can be rerouted to one baghouse if necessary.  The fugitive
emissions can be vented to either baghouse.

     Plant log sheets lists the exact amounts of material  charged to a
furnace during a heat (melt)  along with any changes in operating pro-
cedure, e.g., changes of furnace electrodes, downtime, oxygen blow
*  Trade name.

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duration.  These log sheets were used to calculate the process weight
of each furnace during the sampling period [Appendix B].  The process
weight for furnaces Nos. 2 and 3 were combined when calculating the new
baghouse allowable particulate emission rate.  The furnace process
weights and the allowable emissions are summarized in Table 1.

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                       Table 1
               PROCESS WEIGHT SUMMARY
                   Marathon Steel
                   Tempe,  Arizona
                  April 12-16, 1977
Date
(April)
12
13
14
15
16
Average
Furnace
No.
1
2 and 3
1
2 and 3
1
2 and 3
2 and 3
1
2 and 3
1
2 and 3
Process
m.tons/
hr
8.0
16.2
6.4
14.2
7.4
18.1
0
19.7
6.9
16.5
7.2
17.0
Weight
tons/
hr
8.8
17.9
7.1
15.6
8.2
20.0
0
21.7
7.6
18.2
7.9
18.7
Allowable
Emissions
kg/
hr
6.3
9.8
5.5
9.0
6.0
10.5
0
11.0
5.7
9.9
5.9
10.0
hr
13.8
21.5
12.1
19.7
13.2
23.0
0
24.2
12.6
21.7
12.9
22.1
t  Furnace No.  1 down for reline.

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                         IV.  TEST PROCEDURES
     Testing was conducted at Marathon Steel from April 12 to 16, 1977
at the following locations:  Station 1, old baghouse; Station 2, new
baghouse (south side); Station 3, new baghouse (north side).  A pre-
liminary velocity, temperature and moisture traverse was made on Station
3, April 12.  Except for the number of points sampled in the old bag-
house stack (see section on sample locations), the tests were conducted
in accordance with the procedures specified in Method 5.

     The sampling train used was the Model AP 5000 manufactured by
Scientific Glass, Inc. [Appendix C] which was configured as follows:
     1.  Stainless steel (316) nozzle
     2.  Glass-lined probe
     3.  Glass fiber filter (11.4 cm diameter)
     4.  First impinger -- modified Greenburg-Smith with 100 ml
         distilled water
     5.  Second impinger -- Greenburg-Smith with 100 ml distilled water
     6.  Third impinger — modified Greenburg-Smith, empty
     7.  Fourth impinger -- modified Greenburg-Smith with approximately
         200 g of silica gel
Moisture content of the gas stream was determined from the increase in
volume in the first three impingers and the weight gain of the silica
gel (Method 4*).

     Stack gas molecular weight was based on the average analyses of
two to three gas  samples collected during each run.   Gas samples were
 *  40 CFR 603  Standards of Performance for New Stationary Sources^
    Appendix Test Methods,  June 83  1976.

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 obtained by the grab sample  technique   of Method  3  (40  CFR  60).   Analy-
 ses were performed with  Fyrite    type  combustion  gas  analyzers.
      A minimum of three  sampling  runs, within  the  isokinetic  range of  90
 to 110%,  were  performed  on  each stack.   Prior  to each  run,  the sampling
 train was leak-checked at 38 cm (15  in)  Hg.  At the completion of the
 run,  a second  leak check was conducted at the  highest  vacuum  recorded
 during the  test.  These  checks are acceptable  if the leakage  rate did
 not exceed  0.00057 m /min (0.02 cfm).  All sampling runs were structured
 to provide  a minimum sampling time of 60 minutes* and  a minimum sample
 volume of 849  dry std. liters (30 dscf).*  Probe and oven temperatures
 were  held within  14°C (25°F) of 120°C (248°F) during testing.

     All  pitobe assemblies, dry gas and orifice meters used in this test
 had been  calibrated prior to leaving Denver and were recalibrated upon
 return  [Appendix D].  The pitobe assemblies used during the compliance
 test were those identified as 5-5 (old baghouse stack) and 8-1 (new
 baghouse  ducts).

     An NEIC mobile laboratory,  located at the plant,  was used for all
 sampling  train preparation and  sample recovery.  Sample recovery pro-
ceeded as follows:
     1.  All filters were returned to their  storage container (Petri-
         dish)  and sealed with aluminum foil.
     2.  The nozzles,  probes, cyclones  and  front portion  of the  glass
         filter holder were  washed with  acetone and the washings  from
         each train  were  collected in a  glass  jar with  a  Teflon  -lined
         cap.
  *  The Arizona  SIP stack  sampling requirements specify  that  1)  an
     integrated gas  sample  be  taken,  2)   the sampling period be at  least
     2  hours,  and 3)  at  least 60 dscf be sampled.  These requirements,
     which  are more  stringent  than Method 5 requirements, were not
     strictly  followed.   It was determined during the pre-survey inspec-
     tion that the Method 5 procedures would obtain representative
     results.
**  Brand  name.

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                                                                  8
     3.  The volume of the contents of impingers 1-3 was measured as
         part of the moisture determination.  The contents were then
         discarded.
     4.  Impinger 4, which contained silica gel, was weighed to determine
         the moisture gain and the silica gel was discarded.

     All samples were returned to the NEIC laboratories for particulate
analyses [Appendix E].  Chain of custody was maintained at all times
[Appendix F].
Sample Locations

     The old baghouse stack (Station 1) is 1.5 m (5 ft) in diameter and
12 m (40 ft) tall [Figure 1].  The ports are located 3.0 stack diameters
(4.5 m or 15 ft) downstream of the inlet and 3.0 stack diameters upstream
of the stack exit.  Based on Method 1 criteria a total of 42 sampling
points were required.

     Two parallel bars (5 cm angle irons) cross the stack immediately (5
cm) upstream of the test ports and could cause flow disturbance.  Based
on a preliminary velocity traverse, a flow disturbance was found only
within 2.5 cm (1 in) of these bars.  The preliminary traverse also
determined that the gas velocity profile in the stack was flat, indi-
cating uniform flow.  Thus, the number of sample points could be reduced
to avoid sampling within 2.5 cm of the bars without affecting the sample
representativeness.  The number of sample points was therefore reduced
to 28 (from 42), which increased the distance from the bars to the
nearest sampling point to 7.6 cm (3 in).  Each point was sampled for 3
minutes (84 minutes per test).
 *  Brand name.

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       STACK
     E
    0
   EC
  to o
Fan
               EXISTING BAGHOUSE
                       I   I   I   111
                                                         SIDE VIEW
                                                       GROUND
1.6m (5.Oft)

   STACK
                         EXISTING BAGHOUSE
                   ;PORTS
                               CATWALK
                                                         TOP  VIEW
            Figure I. Marathon Stool,  Tempo, Arizona



                   Old  Baghouse  — Sfafion  040I

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                                                                  10
     The new baghouse emissions were sampled in the ducts  between the
baghouse and the fans (Stations 3, north side, and 2, south side).  Six
equally spaced 10 cm (4 in) sampling ports are located 2.1 equivalent
diameters (4.3 m or 14 ft) downstream of a flow disturbance and 0.5
equivalent diameters (1 m or 3.4 ft) upstream of a flow disturbance
         i **
[Figure 2],   therefore, Method 1 requires 48 sample points.  Each point
was sampled for 2 minutes (total test time of 96 minutes).
 *  The new baghouse has two identical ducts (north and south),  each
    of which handles approximately half of the waste gases.
**  The length to width ratio is 1.3.

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                                                                         11
                                        FROM
                                     BAQHOUSE
                         FLOW
FRONT VIEW
                    1 8m (6 Oft)
                                  ,PORTS
                   2.3m  (7 5ft)
                       FAN
      FAN  EXHAUST
 TOP VIEW
                                                                  SIDE VIEW
                                                                     "B"
                                                               FAN EXHAUST
       FAN EXHAUST
*^W//////S




STATION O4O3,
(NORTH)

i
1
PORTS
J 2.1m (7ft)

PLATFORM
PORTS
/


>

S


1
STATION O402 |
(SOUTH)


T—W/M
1
1
*
-.— 0
-I
IL




>
o
-*-_!
IL


BAGHOUSE



BAGHOUSE





i
                     Figure 2. Afarafhon Steel Tempo, Arizona
                      New Baghouse - Stations  0402, 0403

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                           V.  TEST RESULTS
     The old baghouse (Station 1) and the new baghouse, north side
(Station 3), were sampled three times, while the new baghouse, south
side (Station 2), was sampled five times.  The second run of the new
baghouse, south side, was unacceptable because the filter was not in
proper position after the final leak check.  Isokinetic sampling rates
for the eleven sample runs ranged from 94.6 to 108.9%, within the
specified range of 90 to 110%.  The test data [Appendix G] is summarized
in Tables 2, 3 and 4.
                                             /'
     The old baghouse (Station 1), particulate emissions [Table 2],
averaged 6.0 kg (13.3 lb)/hr, 2% over the allowed 5.9 kg (12.9 lb)/hr.
Since 2% is within the accuracy of the test method, a violation did not
occur.

     The new baghouse particulate emissions are in compliance with state
regulations.  The emissions [Tables 3 and 4] averaged 2.9 kg (6.4 lb)/hr,
29% of the allowable emission (i.e. 10 kg/hr.  Combining the emission of
the two sides (north and south) was necessary because there are no
dampers to evenly control the gas flow rate to each side and the fur-
naces 2 and 3 process weights cannot be separated.  The design gas flow
rate of both sides (north and south) of the new baghouse is 2,830 act.
 o
m /min (100,000 acfm).  The flow rates observed during the survey were
3,020 act. m3/min (106,800 acfm) for the north side (Station 3), 35%
more volume than treated in the south side (Station 2) 2,230 act.
 2
m /min (78,700 acfm).  The emission particulate concentrations, however,
                              3
differed by less than 1.5 mg/m .

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                                                                 13




                               Table 2
DATA
Run Number
Sample Date (April)
Volume Sampled (STP)t
ft3
liters
Moisture %
Barometric Pressure
cm of Hg
in of Hg
Stack Gas Temperature
°F
°C
Molecular Weight (dry)
% Isokinetic
Stack Gas Velocity
ft/ sec
m/sec
Volumetric Flow Rate (STP)t
ft3/min
m3/min
Particulate Collected (mg)
Acetone Wash
Filter
Total
Particulate Concentration
gr/SCF
mg/m3
Particulate Emissions
Ib/hr
kg/h
SUMMARY - STATION .
Marathon Steel
Tempe, Arizona
April 197?
1
16
41.10
1,163
0.3
73.18
28.81
206
97
28.82
99.2
42.9
13.1
38,500
1,080
95.4
20.9
116.3
0.044
100
14.3
6.47
2
16
37.04
1,048
0.1
73.18
28.81
220
105
28.84
99.9
39.1
11.9
34,400
960
93.2
24.8
118.0
0.049
113
14.4
6.53
1
3
16
35.29
998
0.2
73.18
28.81
212
100
28.83
94.6
38.9
11.9
34,600
970
46.3
42.0
88.3
0.039
88.4
11.3
5.14

Average



101



35,800
1,000

0.044
13.3
6.05
t  STP - Standard Temperature (68°F)  and Pressure (29.92 in  of Hg)-Dry

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                                                                          14
                                    Table 3
DATA SUMMARY - STATION 2
Marathon Steel
Tempe, Arizona
April 1977
Run Number
Sample Date (April)
Volume Sampled (STP)t
ft3
liter
Moisture %
Barometric Pressure
cm of Hg
In of Hg
Stack Gas Temperature
°F
°C
Molecular Weight (dry)
% Isokinetic
Stack Gas Velocity
ft/sec
m/sec
Volumetric Flow Rate (STP)t
ftVmin
m3/min
Particulate Collected (mg)
Acetone Wash
Filter
Total
Particulate Concentration
gr/SCF
mg/m3
Particulate Emissions
Ib/hr
kg/hr
14
41.97
118
1.9
72.52
28.55
142
61
28.64
106.7
34.2
10.4

60.800
1,700
14.1
2.6
16.7
0.0061
14.1
3.17
1.44
T
14
40.80
1,134
0.0
72.52
28.55
154 .
68
28.84
108.9
32.6
9.94

58,500
1 ,640'
4.7
0.7
5.4
0.0021
4.76
1.04
0.47
3
14
44.40
1,256
0.4
72.52
28.55
180
82
28.84
107.4
29.2
8.91

50,300
1,400
15.1
0.9
16.0
0.0055
12.7
2.36
1.07

15
55.12
119
0.8
73.00
28.74
184
85
28.84
99.8
39.1
11.9

67,100
1,880
25.3
0.6
25.9
0.0072
16.6
4.12
1.87

5 " A'
15
52.40
148
0.2
73.00
28.74
197
92
28.84
98.2
38.3
11.7

64,800
1,800
6.9
2*
.1
9.0
0.0026-
6.07
1.46
0.66








78




60.300
1,690



0.0054
12.4
2.78
1.26
ft  Run No.  2,  station 0402 results  not  included in emission averages because
    filter was  not in proper position after final leak check.

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                                                                  15
                                Table 4
DATA
Run Number
Sample Date (April)
Volume Sampled (STP)t
ft3
liters
Moisture %
Barometric Pressure
cm of Hg
in of Hg
Stack Gas Temperature
°F
°C
Molecular Weight (dry)
% Isokinetic
Stack Gas Velocity
ft/sec
m/sec
Volumetric Flow Rate (STP)t
ft3/min
m3/min
Particulate Collected (mg)
Acetone Wash
Filter
Total
Particulate Concentration
gr/SCF 0.
mg/m3 8.
Particulate Emissions
Ib/hr 2.
kg/hr 1 .
SUMMARY - STATION
Marathon Steel
Tempe, Arizona
April 1977
1
13
57.39
1,624
0.9
72.90
28.70
127
53
28.84
100.0
47.9
14.6
90,000
2,520
12.5
0.5
13.0
0035
00
67
21
2
13
54.28
1,536
1.3
72.90
28.70
157
70
28.84
102.1
46.8
14.3
83,300
2,330
13.2
4.7
17.9
0.0051
11.7
3.62
1.64
3
3
13
53.93
1,526
0.4
72.64
28.60
149
65
28.84
100.1
46.6
14.2
84,500
2,370
17.5
3.7
21.2
0.0061
13.9
4.34
1.97

Average

9

63
\


85,900
2,410

0.0049
11.2
3.55
1.61
tSTP - Standard Temperature (68°F) and Pressure (29.92 in of Hg)-Dry.

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                                                                    16
                                                                    o
     The particulate concentration from the old baghouse is 100 mg/m ,
more than eight times the new baghouse particulate concentrations of
12.4 and 11.2 mg/m , south and north side, respectively.  The old bag-
                                    o
house gas flow rate was 1,340 act. m/min (47,500 acfm), only 80% of
the design flow rate of 1,700 act. (60,000 acfm).  No problems were
caused by the gas temperature (101°C)or moisture (<1%).   Possible
reasons for this difference include leaking bags, the bag cleaning
cycle or suitability of bag material.

     The visible emissions from all three emission points are in com-
pliance with the Arizona limitation of 40% opacity [Table 5].  Rarely
(2 of 14 observations) did the average opacities exceed  10% and these
observations occurred during one sample run (run 3 of the new baghouse,
north side).  As can be seen in the observation data sheets [Appendix G]
the emissions increased in opacity at regular intervals.  These inter-
vals occurred immediately after a baghouse section was cleaned.

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                                                  17
                Table 5

  VISIBLE EMISSION SUMMARY (Opacity)
            Marathon Steel
            Tempe3 Arizona
           April 12-16, 1977
Station
No.
0401


0402





0403




Run
No.
1
2
3
1
2
2
3
4
5
1
]T
2
3t
3
Avg. of 24
Readings
(%)
5.6
9.4
6.5
1.9
1.0
2.7
0.6
1.5
0.6
1.3
0.9
4.8
13.8
22,3
Readings
High Low
30
20
10
15
10
15
10
15
10
10
10
15
30
35
0
5
5
0
0
0
0
0
0
0
0
0
5
10
More than one set of 24 readings performed
during a single run.

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                  APPENDIX A

Presurvey Inspection of Marathon Steel Company
                Tempe, Arizona

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                                    APPENDIX A


                           ENVIRONMENTAL PROTECTION AGENCY
                                OFFICE OF ENFORCEMENT
                      NATIONAL ENFORCEMENT INVESTIGATIONS CENTER
                         BUILDING 53, BOX 25227. DENVER FEDERAL CENTER
                                DENVER, COLORADO  80225

      Chief, Field Operations Branch                      DATE.  December 20,  1976
:OM  :  Paul R. dePercin


IBJECT.  Presurvey Inspection of Marathon Steel  Company, Tempe, Arizona
           On November 15, 1976, Messrs.  Daniel  Yee,  EPA, Region IX,  and Gregory
      Witherspoon, Maricopa County Health Department, accompanied the writer on
      the subject inspection to determine the feasibility of performing source
      testing.  The inspection also included a review of the process  operations,
      the pollution control equipment and an evaluation of the control equipment
      operations.

           The plant manufactures structural reinforcement rods from  scrap steel.
      Approximately 205 m. tons (226 tons) of reinforcement rods are  produced
      each day.  The reinforcement rods vary in diameter and length according
      to customer orders [Figure 1].

           The plant representatives contacted were Messrs. Charles Brooks,
      Manager-Engineering, and George Collins, Plant Engineer.

      Process Description

           The scrap steel that enters the plant is used without any  prior
      conditioning (shredding or drying).  The scrap steel and alloying materials
      (silica, ferro manganese, feldspar, and carbon) are charged into one of
      three electric arc furnaces from a bottom drop charge bucket with only
      tv/o furnaces operating at a time.  The furnaces have rated capacities as
      follows:

                                               Process Rate
                                      Per Heat             Per Hour
           Furnace No.             m. tons (tons)       m. tons (tons)

               1                    22.7    (25)          9.1    (10)
               2                    22.7    (25)          9.1    (10)
               3                    27.2    (30)         11.3   (12.5)

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                                   -2-
furnace and the beginning and  end  times  of  each  heat.

     A hood is placed over the furnace after charging  and contains three
arc electrodes   The scrap acts as a conductor between the electrodes.
The hood and eiectrodes a're removed from the furnace after m
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                                   -3-
When furnaces No.  2 and 3 are melting  scrap  the  dampers  are open causing
60% of the gase flow to be drawn from  the furnace hoods  and 40% from the
roof monitor and skulling hood.   At all  other times  (i.e.,  pouring,  slagging
and charging) the No.  2 and 3 furnace  dampers are closed resulting in 1007,
of the gas flow to be  drawn from the roof monitor and the skulling hood.
While furnace No.  1 is melting (damper open) all  the emissions  controlled
by baghouse No. 1  are  from the furnace hood.  At present, the No. 1  furnace
is inoperable, the damper is closed and thus baghouse No. 1 controls just
the emissions collected in the roof monitor.

     All three baghouses have a  control  system to prevent the baghouse gas
temperature from exceeding the bag material  limitations.  During the furnace
melting cycle, if the  baghouse temperature reaches a predetermined value
(i.e., 250°F) the damper closes  further to allow greater dilution with
roof monitor gases.

     At the base of each baghouse are  the damper controls,  gas temperature
indicators and the cleaning cycle controls.   The Company reported that the
bags in each compartment are cleaned by shaking 30 seconds  out of every
two minutes.  The baghouss operate under a vacuum because the fans are
downstream.

     Baghouse No. 1 emissions vent from a steel  stack.  Baghouses No. 2
and 3 emissions are exhausted directly to the atmosphere from the fans.
The exhaust gas velocity from the three baghouses are expected to ranga
from 12-18 m  (40-60 ftj/sec with temperatures ranging from ambient to 300°F.
The moisture of the gases will be near ambient (0-5%).  The bulk of the
particulate present in the emissions gases will  be less than ten microns
in size.  No visible emissions were observed from the No. 1 baghouse, but
visible emissions of 5-10% occurred periodically from baghouses No. 2 and 3.

Source Sampling Feasibility

     The baghouse emissions can be sampled following the EPA, Method 5
procedures.  Modifications at baghouse No. 1 are required.

     Baghouse No. 1 stack is 1.5 m (5 ft) in diameter and 12 m (40 ft)  tall
[Figure 2] and has two sets of sample ports.  The first set of ports are
10 cm (4 inches) in diameter and are located 3.5 stack diameters  (5.2 m or
17.6 ft) downstream of the fan inlet and 2.5 stack diameters (3.8 m or  12.4
ft) upstream of the stack exit.   The ports are located 1.1  m (3.6 ft) above
a dualrail sampling platform and 2 m (6.5 ft) about the catwalk.  The second
set of ports are 9 cm  ( 3.5 inches) in diameter and are  located 3.0 stack
diameters (4.5 m or 15 ft) downstream of the fan inlet and 3.0 stack diameters
(4.5 m or 15 ft) upstream of the stack exit.  The second set of ports are
directly underneath the first set and about  .3 m (1 ft) above the dualrail
sampling platform mentioned previously.  The catwalk guardrail supports
the dualrail  sampling  platform  .9 m (3 ft) above the catwalk.  The dualrail
sampling platform  is 32 cm  (12.5 inches) wide and 2.7 m  (8.8 ft)  long and

-------

-------
                                    -4-
  is made of 5 cm  (2 inches) angle iron.  Guide wire brackets for supporting
•  a portable monorail are located approximately 1.8 m (6 ft) above the lower
  ports.  Access to the sampling platform is by ladder.

       Either sampling location on the No. 1 baghouse stack meet the EPA,
  Method 1 and 2 requirements.  The top set of ports are 2 m (6.5 ft) above
  the  catwalk.  Sampling at this location would require a platform to be
  built.  The ports are 1.2 m  (4 ft) above the catwalk, but only .3 m (1 ft)
  •above the dualrail sampling  platform.  A clearance of .4 m (13 ft) below
  the  ports is needed by the sample box, therefore, the dualrail samplinn
  platform and supporting section of guardrail would have to be removed.

       Baghouse No. 2 and 3 have identical geometries.  Neither baghouse
  fan  exhausts to  a stack, however, the baghouse emissions can be sampled
  in  the duft* between the baghouse and the exhaust fan [Figure 3J.  The
  duct is straight for half its  length and then tapers the other half.
  The  sample ports are located approximately halfway in this run of duct
  or  2 2 equivalent diameters  downstream of the 90° bend.  Downstream of
  the  ports  the duct geometry  converges in one place and diverges in another
  [Figure 3]   At  0.5 equivalent diameters downstream of the ports the  etrect
  of  the diverging and converging section should have  little impact because
  the cross  sectional area decreases  only slightly.  Forty-eight sampling
  points will  be  used at  the  baghouse  2 and 3  location.

       There  are  six  10  cm  (4  inch)  ports equally  spaced across  the 1.8 m
  (6  ft) wide  duct.   The  ports are  1.2 m  (4 ft) above  the  sampling platform
  which is  2.1  m  (7 ft)  wide  and 4.6  m (15  ft)  long.   The  same  platform
  would be  used  to sample  both baghouse ducts.  No modifications are  needed
  to perform the  source  sampling.

  Summary  and Conclusions

       The emissions  from the Marathon Steel  Company  plant can  be  determined
  using EPA,  Method 5 procedures.   To sample  baghouse  No.  1  several modifi-
  cations  at existing locations will  be necessary;

       a.   If the lower ports are  used the  dualrail system presently
           in place will need to be moved.   In addition,  a 51  cm (20
           inch)  wide section of the guardrail  where  the dual rails
           are attached must be removed in  order that sufficient
           horizontal  and vertical  clearances are provided.

       b.   If the upper ports are used, a  work platform with proper
           guardrails would need to be provided.   This would require
           raising the present platform about .75 cm (2.5 ft) and

  * The gases at  the sample point have a negative static pressure (vacuum)
    of approximately 13 cm (5 inches) of mercury.

-------
               a09^<
  9 B  •
/
t  t *

-------


                                                           6          a
                                                         O       O
                                                                          7~c>-A
                                                                .©
Figure 1: Plant  Plot Plan

-------
                                   -5-
         providing the horizontal  and vertical  clearances  described
         under (a).

     No modifications are necessary to sample baghouses  2  and 3 emissions,
Source tests at the  three locations described will  provide an adequate
determination of the total  emission load.

     The process and control  equipment operations can be monitored from
the heat logs and the baghouse control panels.

-------
                  APPENDIX B
Production Data and Process Weight Calculations

-------
                            APPENDIX B
                           Marathon  Steel
                        Daily Production  Rates
              Furnace
                 1
                 2
                 3
              m. tons
                HR

               8.0
               6.5
               9.7
                 Production
                  tons/hr

                    8.8
                    7.2
                   10.7
              Hour
           0837-1155
           1222-1625
           0833-1923
4/13
1
2
3
 6.5
 4.7
 9.4
 7.14
 5.16
10.4
0832-1727
1118-1721
0731-1830
4/14
1
2
3
 7.4
 8.9
 9.3
 8.2
 9.8
10.2
0957-1321
0820-1936
0550-1714
4/15
1
2
3
 — Down*
10.2
 9.5
                                                  11.2
                                                  10.5
           0725-1755
           0618-1741
4/16
1
2
3
 6.9
 9.3
 7.3
 7.6
10.2
 8.0
0722-1806
0727-2000
0954-1752
*Furnace Daun for reline

-------
                          Marathon Steel

Furnace #1              Weight of
Date                 Material  Melted              Time Period
4/12                   58,989 Lbs                  8:37 to  11:55
                           4 mi n 02
                       57,331 Lbs                 12:00 to  14:37
                          12 min 02
                       59,994 Lbs                 14:55 to  18:29
                          29 min 02

4/13                   58,536 Lbs                  8:32 to  11:49
                          No Go
                       57,866 Lbs                 12:35 to   5:27
                          No 02

4/14                   54,339 Lbs                  9:57 to  13:21
                          No 02

4/15                   Furnace Down

4/16                   51,333 Lbs                  7:22 to  10:06
                          No 02
                       54,486 Lbs                 10:26 to  13:33
                          No 0
 no uo
,830 Lbs
                       54,830 Lbs                14:14 to 18:06
                          No 02

-------
                           Marathon Steel

 Furnace #2              Weight of
 Date                  Material  Melted              Time Period
4/12                    57,401  Lbs                 12:22  to   4:25
                           No 02

4/13                    56,049  Lbs                 11:30  to   2:14
                           6 nrin 0?
                        57,666  Lbs                  2:35  to   5:13
                           3 min 0?
                        61,911  Lbs                 11:18  to  15:30
                           No Op (down  time)
                        59,026  Lbs                 15:30  to  17:21
                           No 02 (down  time)

4/14                    55,301  Lbs                  8:20  to  10:45
                           5 min Oo
                        61,666  Lbs                 12:25  to  15:30
                          12 min 02 (maintanence)
                        58,771  Lbs                 15:55  to  19:36
                          No 02     (maintanence)

4/15                    59,676  Lbs                  7:25  to  10:01
                           7 min 02
                        59,186  Lbs                 10:11  to  12:37
                          3% min 0?
                        58,921  Lbs                 12:45  to  15:00
                           3 min 02
                        58,159  Lbs                 15:22  to  17:55
                           No 02

4/16                    54,006  Lbs                  7:27  to  10:15
                           No 02
                        51,761  Lbs                 11:24  to  14:35
                           3 min 02
                        56,659  Lbs                 17:40  to  20:00
                           22 min 02

-------
                           Marathon Steel

 Furnace #3              Weight of
 Date                 Material Melted              Time Period
4/12                    59,216 Lbs                 8:33 to  11:03
                           1  min 02
                        59,444 Lbs                11:12 to  13:44
                          15  min On
                        59,474 Lbs                13:51  to  16:58
                          lh  min 02
                        57,561 Lbs                17:09 to  19:23
                          10  min 02

4/13                    58,286 Lbs                 7:31  to  10:08
                           3  min Op
                        60,586 Lbs                10:16 to  12:49
                           No 02
                        55,036 Lbs                12:59 to  15:46
                           Mo Oo
                        54,665 Cbs                15:55 to  18:30
                           No 02

4/14                    59,306 Lbs                 5:50 to   8:46
                           No 02
                        51,586 Lbs                 8:53 to  11:35
                           No 02
                        53,436 Lbs                11:53 to  14:11
                           No 02
                        60,504 Lbs                14:34 to  17:14
                           5  min 02

4/15                    57,236 Lbs                 6:18 to   8:28
                           No Oo
                        58,624 Lbs                 8:34 to  11:08
                           No 02
                        53,424 Lbs                11:25 to  13:59
                           No 02
                        60,589 Lbs                14:34 to  17:41
                           No 02

4/16                    53,274 Lbs                 9:54 to  13:40
                           No Op (problems)
                        59,374 Lbs                15:03 to  17:52
                           3  min 02

-------
       APPENDIX C



STACK SAMPLING EQUIPMENT

-------
                              APPENDIX C

                        STACK SAMPLING EQUIPMENT


     The Scientific Glass  Model  AP-5000 modular STAC-O-LATUR1'"  sampling
train consists of a control  unit,  a  sampling  unit  and  a  vacuum  unit.   The
units are connected together with  quick disconnect electrical and  air  lines
and umbilical  cords.   A ground fault interrupter provided  personnel  safety
from electrical  shorts.

     The AP-5000 control unit contains the following:

     1.  Dual-inclined monometer (range 0-5"  H20)  for  indicating  the
         pitot tube velocity pressure and the orifice  pressure  drop.

     2.  Temperature control for the oven and probe.

     3.  A flow valve and a bypass valve  for  adjusting sampling rates.

     4.  Digital Temperature Indicator  (DTI)  which give  an instant
         readout from six (6) points; stack,  probe, oven,  impinger
         outlet, meter inlet, meter outlet by the  use  of a selector
         switch.

     5.  Umbilical cords of (50 and 100  ft lengths) which interconnect
         the control and sampling units.

     6.  Communications sets are wired  through control unit, umbilical
         cord to the sampling unit*.

     The sampling  unit  is made up of three distinct sections; impinger
case,  oven and probe.  All  three sections can be converted to form one
sampling unit or can be separated for unusual sampling conditions.  Below
are  the  individual component descriptions:

     1.  Probe Sheath - Made of 316 stainless steel.  The nozzle end
         is packed with asbestos string.   The ball joint  (sampling
         unit) end has  a woven teflon 0 Ring as packing material.

     2.  Probe liner -  5/8" O.D. medium wall glass (pyrex) or stainless
         steel  (316) tubing logarithmically wrapped with  nicrome heating
         element,  having a  resistance of  2 ohms/ft.  The  liner is in-
         sulated with  fiberglass and asbestos with a type K thermocouple
         imbedded  for  sensing the probe temperature.

     3.  Filter  Frit -  Porous glass  frit  (coarse)  banded  to silicone
         rubber.

     4.  Oven -  Fiberglass  insulated capable of maintaining 120°C
          (248°F)  in  cold weather  (0°C).
 *Separate  communication  system  used during  this test program.

-------
                                  -2-
     Thc vacuum unit (pump)  is  capable  of  drawing  a  high vacuum  (50  cm  Hg)
and a moderate volume (11 1pm)  of air.   The  pump  is  rotary  fiber vane  type
which does not require lubrication,  but oil  bath  filters are  used for  pump
protection.

-------
   APPENDIX D
Calibration Data

-------
                         APPENDIX D
                      CALIBRATION DATA
          Dry Gas Meter Calibration by outside source
Control Module #_zb _ Make  fip $<:<.<:
DGM Serial i
Calibrated by (\>HLK   WV/ce.     On  7 eft ?
DGM adjusted (yes/no)    ycz _
Calibration:       IN.            OUT
     Capacity
     Check (40%)  Runyff/     ??.?
Personnel v/ho obtained calibration
                                            <.
                           Date    fen  7,
Comments:
          Dry Gas Meter Calibration by outside source
Control Module #	Make	
DGM Serial 9	
Calibrated by	On_
                                 i
DGM adjusted (yes/no)	
Calibration:          JN          OUT
     Capacity Run	
     Check (40%) Run	
Personnel who obtained calibration
                           Date   ~
Comments:

-------
                       Orifice Meter Calibration
     Date
Box No.
     Barometric pressure, Pb=	in.  Hg   Dry  gas meter No.  7& 6
Ori f i ce
Manometer
setting,
AH
in. H,0
t.
0.5
1.0
2.0
3.0
4.0

Gas volume
wet test
meter
V
ft3
_5_
-*-
-40-
*h
Wr

Calculations
AH
0.5
1.0
2.0
3.0
4.0
AH

13.6
0.0368
0.0737
0.147
0.219
Gas volume
dry gas
meter
V
ft3
^/07
f /re
A* Wf

/e>>34/
Tern
Wet Test
Meter
V
°F





erature
Dry g^as meter
Inlet
°F
£3
£y
6 2

63
Outlet Average
W td'
op op
£f &
£1 63
(,*> £*>

6
-------
                       Orifice Meter Calibration
Date
                     7
Box No.
                            --
     Barometric pressure, Pb=	in. Hg  Dry gas meter Ho.
Ori f i ce
Manometer
setting,
AH
in. H90
0.5
1.0
2.0
3.0
1 4.0

Gas volume
wet test
meter
VM,
ft3
5
5
10
10
10
Gas volume
dry gas
meter
vd«
ft3
57 /

/O o~3>
/c,r^3
/o 2 )
Tern
Wet Test
Meter
V
°F
(*zT
(*g~
CZ.&
GCr,
66 rj-
erature
Dry qas meter
Inlet
V
°F
7V

S^
^
cfi
/.c
/c
/c
/£
/AH0
/
/
/
.c=


/. 4.
,'
. /
I.L
AH(3
0.0317AH
Ph (tri+ 460)
f
(tv, + 460)5
' vw _..

.ooo«3/t.^ /373//<^-/.^

. Of V -.€"••£? tf^x. 7.7^42^ 5 ^ • ^"' '•* / d;

. o< ->c^r>r> M 7 < "3 -S t;3 7c.7'7 - LL,/

. Of ~>c>f~>f ">"?-£ *) VoSy?) u. \ ~ I l

~ f

, £>O("'<'5o<7?,rXSv/ snt'/'^ "'!S'/-7t

Where: V = Volume, v;et test meter Calibration
Vd = Volume Dry gas meter
Tw = Temperature, Uet Test Meter ' Checkec
Tj = Temperature, Dry Gas Meter
?5 = Atmospheric Pressure, Inches Hg
0 = Time, minutes
i by: 5^(-r^j-^U-/^-
J by: ^'-'' -' - -r


-— — •

j
y
*-
7
o
c?
>7'
,>"
— - —
Remarks:


4/24/77

-------
U> I nvironrnsruai   rOi.cci.ion  if
NaL'onal  Enforcement  Investigations Center-Denver
Calibration Pitot Tube: ID Number
Typc-S Pitot Tube ID Number:
                                            /
Ap
Standard
Pitot
2.f


i r\
&* -Ls


i..f


10 .


.So


• fe/


.41
•
.
•3-1

•
AP S-Type Pitot
A leg
•tf.c
V.o
4.0^
3.&\
3o^
2 V
;?3*r
5.35"
/, (o
/.<*
LL>
"/. 2S"
1,^-5^
/ *75K
, 'J7X
*&Z
,74*
,735
•'7V*
,7V*
•/J"?
, Tti-\
>7Xl
<7?3
.777
, 7M
,7*£
. ?Q *>
,'77
-------
Ur Fnvironnnntal Protection Ayoncy
Nai:onal enforcement Investigations Center-Denver
Calibration Pilot Tube: ID Number
Type-S Pi tot Tube ID Number:
AP
Standard
Pi tot
.11 •


.o?.
i3V^'
Xtf^




•


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3
B
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-;7//fr

















Co^ioients
•


•
•

•
•
-
-
•

•


•






.

Leg Average Cp
During Pitot Calibration:
     probe sheath attached
     nozzle attached
     sampling iso!flJ( I
7-7

-------
US rnvironnrnlfli iTCKecuon
    oiuil Diforccn!«rit
                                    Ccntcr-Dc:nvc:r
Calibration Pitot TubcrlH Number   /{/
^).SD

O.SD
6. (So)

*> !&<•










,
.


•
>Ap S-Type Pitot
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n-~\i •
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0 .-71
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B loq
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1-1"
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Vvv^,. *- ?>

_
•

^vvu.lt 'kiAtuM^wtfcL. "^ 6
l,,t,l f ^v,-. rj/r '
•
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.

Leg Average Cp
During Pitot  Calibration:
     probe  sheath attached
     nozzle attached
     sampling'isokinetically j
PerFonr.ad By:
                                        Calibration Date:.^/ ^  77

-------
US Environmental Protection i\gcncy
National Enforcement Investigations Center-Denver
Lcll IUi CILIUII r
Typs-S Pi tot
Standard
Pi tot



^0


1,5"


77


.9?


,5-?


.3?


.£/


1 W ^ 1 W W W * * *
Tube ID Numt
AP S-Tvpe
A leg

y 2^
*/2-
3.2-

3.2-.
Ziff
2,15
2.M5
l'l
\,(*5
]MS
A3
1.3
1,3 '

£7^7"
ffi
£7
.£7

,37
/?#
i3&
During Pitot Calibration
proba sheath attach
nozzle attached )
sampl i ng " i sojprf^t ip
Performed By^f^/^-^/o
>er: ^-/
Pitot
B leg
l/2_
t/2^
4'L^
3?>
3.*>
13
2,5-
^.«/5'
2£
\,n
1,1

/.35
A3
1,3

.9^
i9fr

i^7
,67
.57

iJ9
:
ed V^3"
^-5^\
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A
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»77/
i77/
,913

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^75"
,975'

,76"5
,7^7
,9^7
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,7^7
.7^7

.762-
,762L
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,93^
/7J^
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, 777
-77/
.97'

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,7^,7
9t$5"
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,9^-7
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,7^7
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,n&-
,H53
,953
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,74^
.9^
,7^

Comments



'
11
!''

•
B

•











.

Leg Average Cp
R-l 0 (o^" M«v
^ ^n J
nr
'ally)/z/(?
^^
Ax y y X^7 ^^^ X
'J*ri£*L/ Calibration Date-.J^V^X^^X7

-------
    .ivironmpntal  Protection Agency
  .uional Enforcement Investigations Center-Denver

Calibration Pi tot Tube: ID Number
Type-S Pitot Tube ID Number:  fr
Ap
Standard
Pitot
.// '


.OZZ










•




m



•
xAp S-Type Pitot
A leg
.21
i7l
i2\
ill
- - t-^-t — - -—
,//
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,2i
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A
.nil
-7/7
-•7/7
.900
,900
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B
..9/7
.9/7
/9/7
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,700
i7oo



















Comments
•



•



.





•
•








Leg Average Cp
 During Pitot Calibration:
      probe  sheath  attached y
-------
US r.nviromnenlal Protection Agency
      .io'L Enforcement Investigations CenLer-Denvo*'
Calibration Pi tot Tube: ID Numh2r_
Type-S Pi tot Tube ID Number:	
   Standard
    Pi tot
                  S-Type Pi tot
A leq
B leg
              A
D

    .
                                     6 • 1 '
                                     •^ • i -.
                                                -> •-'
              0
(9
      "I
                      •\.y\i
               1 .
                                      -v'7
                                      , ' /
                                      0 *:.
   i_io
                                                 P 6 6
During Pitot Calibration:
     probe sheath attached
     nozzle attached	
     samp!ing'isokinet;

">rfor;nsd By:
                                                        Leg Average Cp
             Calibration Date:

-------
 APPENDIX E



Source Tests

-------
V-/3-97
O4t>3
                                          APPENDIX E
                                   SOURCE TESTS AT MARATHON STEEL
                  01
        00003
                                     "
                           o.
                                                                0*1311
                                                                                      - 77
         0^03
02
                           0. 73
                                                                0.
                                                                                    -£- 77
                  03
                        0.
                                      0.7317
                                                                          0.0039
                                                                                    -/?- 77
 -<-
01
OOOO&
                                           0. 73S8
                                   0.
                                                                0.73*8
                                                                 0.00 £(&

-------
                       BS/fK^K.
               7/JJL Of
                                                     H/T?
                                                           7/1XS.
                 Of
                                96.
                 01
                                          98.
                                                                o.ooov
                 03
£2°-
                        . 0/38
                                                      ?'/.
                    O.OOO'/
7?
                 Of
                      V/.J&08
   ovo/
'/-
                                £33
                                9A/P/89
                                                                0. 073/2
03
                                  9Z39/0
97.370?
                 of
                                          98.326V
                                                                0.0/+/I
&L
                                                                    o.
                 03
        30
                 O*/
         /to
                                                      73.
                    O-
                                                96. 3 8/'/
                                                    O. O06?
                              -#- 7?
                 Cf
                                                    O. Oft?
-------
                        ($
    - 79
         O'/O/
01
ooo//
        COOS'?
                                                               it/?:
o.
a
                              0.
                                                                     F/JL
a
                        a 73 7?
                                                                                   IV7T

-------
      APPENDIX F
Chain of Custody Record

-------
               APPENDIX F

  ENVIRONMENTAL PROTECTION AGENCY
           Office Of Enforcement
 NATIONAL ENFORCEMENT INVESTIGATIONS CENTER
   Building 53, Box 25227, Denver Federal Center
           Denver, Colorado  80225


      CHAIN OF CUSTODY RECORD
^URVEY
.' /' ft >*— — -. ^
,-•:- • ....... TV'. .>.&«./ f
STATION
NUMBER
•i '/ -» "
•I',,-

f ' •;• - 1

'i *, ,>
Wo'
-"£'. , .'
.....



STATION LOCATION
^ f ^ ^ „ fj^r/
,-r-^v- * In
x; , ' .^'//-i.^ f /-,- ^ r ^
*:tr~c** U
•* ^ ' ^ /
^,-r,^ XL /5
x:,.^. , ^-r^
A:/-T^ ^ x,7
,-' ->....,- ,-,..-x^



—
DATE
•//,.'.'/? 1
^.A,
^ X
,/,./„
^.^
^/ ^
^A/,7
»• '
/>/,./• T
/
/
y .



elinquished by: /Signoiure;
.elinquished by: (Signoiurej
Relinquished by: /Signa»u-e;
Relinquished by: (Signature)
Uispatched by: (Signature)
.Method of Shipment:

Date/
TIME
/«//<
, v/
/.:/::,
7-r-T
v' <- '.-
/ /^/. ->
//yo
.
-



SAMPLERS: /Signer,;
SAMPLE TYPE
Water
Camp
I-'"
—
(^
F mm^
£«•*""
,^-
ls~
/^
•','



Grab












Air
i,.-'
(^
L-'
^-
.^—
^
^
ix-
-,—



SEO
NO
?
^/
^
l
/
-,
— <
3
-



NO OF
CONTAINERS
1
/
^
' /
/
!
(
r
i
•'"
•


ANALYSIS
RtOUIRED
^.'X.T.V..'.rr
/
/i
/.
.
'/
(V
'.
•'



Received by: /Signa/urej |V
Received by: ffrgnorure;
Received by: /Signature;
Received by Mobile Laboratory for field
analysis: /Signature;
'Time
Received for Laboratory by:

Date/Time
Date/Time
Date/Time
Date/Time
Date/Time ,
c;i5/7/

Distribution:  Orig.—Accompany Shipment

           1 Copy—Survey Coordinator Field Files
                                                            CPO B3I-48*

-------
  ENVIRONMENTAL PROTECTION AGENCY
          Office Of Enforcement
 NATIONAL ENFORCEMENT INVESTIGATIONS CENTER
   Building 53, Box 25227, Denver Federal Center
           Denver, Colorado  80225


     CHAIN OF CUSTODY RECORD
JRVEY
STATION
NUMBER
'/".•"

f
• '/ * v
...
.
- It



'-.II- *
/ -'•• ->
STATION LOCATION
//.-71:,. #/*..*.'
, • *,.*• q
^
^ x ,.., , >* //
.
"" / ~T 4« ' y""~



/ " ' ~f* f S* r
/' • '• V*- ^~" i*^'. -^ y'^i
,_ ,r , ,.-• r--

' t*
DATE
^//J/4:
/
''/;./^
fr

/•-A-,
,'->/^r

wU,
X X
f
/, /, x .
;/,,/ f
'»/»A>
elinqujshed by: (Signature;

lelinquished by: (Signature;
Relinquished by: (Signotu.-ej
Relinquished by: (Signature;
Dispatched by: (Signoiurej
Method of Shipment:

Dote;
TIME
/>*
, . ^/»
o»/9
,,,-,
/ /•-
/'.V,-.
/JX/'O
-.^v
• -'J*-
ff)f,,y
/-{•
,„,<
SAMPLERS: (s.gnoture;.
•"" SAMPLE TYPE
Water
Camp

.,.
*•
.-'
*
-'
IS
' !*-

f ^__
•^
-
Crab
^











Air
A--*
t
6.-
/ 	
/^
's-
^
•w
i "
f,'
f-
^
SEQ
NO
/;/
,
/
-:.
p.
7,
~y
1
1
-
3
-•}
NO OF
CONTAINERS
/
/
/
/
/
/
1
!
:
I
/
/
ANALYSIS
REQUIRED
— /_^!_»'.' ' 	
• • f 7- • .- ' •
^,r"

	 i — • — ^_ 	

& i * ~i~
* f ' * / r
.* • • r
' ' • *"
.-<,. /
^i.r'.
.-^>7r>
Received by: (Signature;
Received by: (Signature;
Received by: (Signature;
Received by Mobile Laboratory for field
analysis: (Signature;
^Time
Received for Laboratory by:

Date/Time
Date/Time
Date/Time
Date/Time
Date/Time

Distribution;  Orig. — Accompany Shipment
           1  Copy—Survey Coordinator Field Files
                                                            6PO 831 -464

-------
  ENVIRONMENTAL PROTECTION AGENCY
           Office Of Enforcement
 NATIONAL ENFORCEMENT INVESTIGATIONS CENTER
   Building 53, Box 25227, Denver Federal Center
           Denver. Colorado  80225


      CHAIN OF CUSTODY RECORD
SURVEY
STATION
NUMBER
^,,.7>.
1










STATION LOCATION
0.0 ^ <-tJ> *?
A.T. * i. J^










DATE
<•)/' ^.V
uf. r-V

'









Relinquished by: {s,gnoiurc)
Relinquished by: (Signoiure;
Relinquished by: (Signotu.-e)
Relinquished by: (Signoturej
Dispatched by: (Signature;
Method of Shipment:

Datey
TIME
' /-^ uCV
,-?r.










SAMPLERS: (Signature)
SAMPLE TYPE
Watei
Camp












Crab
;.-'
, .-'










Air












SEO
NO
<•-
I










NO OF
CONTAINERS
3
i










ANALYSIS
REQUIRED
. ''./'., '.<.- ( -t1'-'^"
../^. /v.;..^










Received by: (s,gnoiuie)
Received by: (
-------
      APPENDIX G
Participate Field Data

-------
             Plant,.
             Run No.
             Location

             Date
             Operator
         ?ri£. iK>
                                         ICU   _ IE1     A

                                VERY IMPORTANT - FILL IH ALL BLA.VKS

                                Read and record at the start of
                                each test point.
                                 Time:  Start Time

                                       End Time
                                                                                      Ambient Temp "F   C* <~
                                                            Bar. Press. "Hg ^^ .<
                                                            Assumed Moisture 7._

                                                            Probe Tip Dia. In._

                                                            Pitot Tube No.  
-------
                                                                    !.	f „,
 Point
R-/V
II
   JG
    Clock
       '/£"
        bo
        (-1
             Dry Gas
             Meter, CF
   .7
   C*
L

        VL
         7<
Pitot
in. H-O
  AP
                       m.
                       AZ
      Orifice AH
        in H20
                              Desired
                                ,76=
                                   Actual
                                '• i  r
                                       ,17.
±£L
                             /.O
                                             Dry Gas Temp.
                                                •F
                                            Outlet
                                          yv:
                            Inlet
                                                 f?
                                            sv;
                                    .96
Pump
Vacuum
In. Hg
Ir.pinger
  Temp.
   °F
                                                       U-
                                                                  131
                                                    9--'.
                                                    /— '
                                                                      Oven
                                                                      Ten? .
Probe
Temp .
 °F

                                                                              Pvy
Stack
Tec?.
 °F
                                                                                         St
                                                                                         Te
                                                                                  n
      7?
Cocunents:

3/16/77
                   iZ
                         .47
                                1,0
                       ?/   w
                                        -7

                                                               /--si?

-------
SAMPLE CLEANUP SHEET
Plant: >^<..s*£. ^fc^
Address: /^.^r? , ^2— •
Station No'.: O^QJ
Run No.: ?^/
Barometric Pressure: -3,^7
Date: bs% ml Of ^-rd'-^l
> ml
ml
ml of fas &•(*->
ml
ml
ml of -^ — \^£.
ml ' ?
ml
ml of
ml
ml
r~gmof 4.£:'*^. &J&'
s" gm ^
gm
ml
Weight .
Tare Weight Collected
gm gm
gm qm
^C -v- on f/2'4/'??

-------
                                                   KECOJfl OF VISUAL DETOMIWTION OF OPACITY
a
C7
COMPANY /v-d/2/^no/J *Q:&&-L
LOCAT ION "^fCn^p^ t £\(L '] 2o.o*V-
TEST NUMBER ' O -7_
nnSFIIVER ArFILIATIOII L^"> ^/^ .
POIHT OF missions ^C^evC
HEIGHT OF DISCIWRGE POINT LrO r£T _

o
P
v>
•o
0

1
CLOCK TIME
OBSERVER LOCATION '
  Distance to Discharge
  Direction from Discharge
  Height of Observation Point
BACKGROUND DESCRIPTION
LEATHER CONDITIONS
  Hind Direction
  VMnd Speed
  Ambient Temperature
SKY CONDITIONS (clear,
  overcast, % clouds, etc.)
PLUKE DESCRIPTION
  Color
  Distance Visible
 OTHER IHFOK'ATIOIl
Initial
&
^
-T
r"1//^"'! y^
<&>y
z£i?
of
???£
CM*.
vh.bz
\s *^ " **

























Final
So'
fat
£w^
^
tottf
o-£
?£- %£
CLSK
Uh:te
tip'

i
i
1

SUWftRY OF AVERAGE OPACITY
• Set
Number










leadings i
'he sourc1
:he tiir.c
Tl-n
Start-End










Csaclty
S-jn










•anqcd from to X opac
i was/was not in ccnpliance wit
ivdlualion v;as race,
I^SS5«









ii-y
h 	 .at

-------
                            03SERYATIOH RECORD

CO^AVY  I'kr&Jfo^SjTZiZL,   Q9SERVCR ^
LOCATIC'r"^-. -n,1-^   qp-.Tror-irt-   TYPE FAClUT
TEST .v,"';U   'si/r,/               POINT OF ""
PATE   cy///./'-, 7
D x-~-£AGE , OF x ,
L'lt
HI
i
^L
























Y-J --j-r'-.r;/1 r^ )._/_t_
5S IC'li b ^ '4 ~'\ c UL

CC'-lHEtlTS


























» ^ ' ' tr*
(Con
COMPANY
LOCATION
TCST
DATE

Mr.














,








MMSER



K
3'j
3"UJ
37
3!t
'.0
•TV"
15
47
/•.ij

50
fil
5,,
ij
" l^j;
15
"Of,
57

59

Seconds
6























Ib






















3'J






















<".'j






















(c^
A(






















[FO Doi.T
                                                  CESERVATIOX RECORD
PACE _ Or ^  .
                                                          02SEJWM	
                                                          TYPE FACIllTV
                                                          POINT OF CMISSTftiT
                                           [FO Ooc.?4-20ISO FUMl 11-11-71:8:45 am]
WCJ^CZ, VOL 39, NO. 219-.TUZSDAY, NOV£;rtB:S 19, 1974

-------
           Jy-ut>Vv-.  ^
                                             ART             DAT

                                       VERY IMPORTANT  -  FILL  IN ALL BLANTCS
                                                                               Asblent  Temp  *F   /T7T
Run No.
Location
  • *

Date
              /
            = /~
       f
Operator_
                                       Read and record  at  the start of
                                       each test point.
                                       Time:   Start  Time_

                                              End Time
                                                    Bar. Press. "Hg   ."<,~

                                                    Assumed Moisture Z  jQ

                                                    Probe Tip Dia. In."	

                                                    Pi tot Tube No.  £.> a_-

                                                                               Filter No.  /.2   ,
            /,
                                                                                                                z >
  Point
         Clock
                Dry  Cas
                Meter, CF
Pitot
in. H-0
  AP
Orifice AH
  In H20
                                   Desired  Actual
                                                    Dry  Cas  Temp.
                                                        "F •
                                                    Outlet   Inlet
Pu-"?
Vacuun
In. Hg
Inpingcr
  Temp.
   •F
Oven
Temp.
"•F
I'robe
Tenp.
 •F
Stack
Tcp>p.
 •F
Stack-
Ten-p.
 •F
CF+460)
 F—/9
         .S
                                                                         / ^
               V v/   •--•
                                      'c
                                                                          /•r,
                                                            v

                                                    v/
   c/
                          c  .
         VI
                          c
                                           f) -'
                           "l.'/'J
                                                            '77
                                                                                               X -'-
                                                           /o/
                          •\
                                                    to*
                                                    12_
                                                                           /<$
          < a
Coraccnts:

-------
                                                                       5riv.t-i_ ~
 Point
  10
  7
Clock
        9
Dry Gas
Meter, CF
Pitot
In.  H-0
  AP
                         to
Orifice AH
  in H20
                                Desired
                                Actual
                                          67
                                               Dry Gas Temp.
                                                  °F
                                 Outlet
                                       /oo
                               Inlet
                                                      97
                                     • -
                                                      /&>
                                               /GO
                                                      /cf
                                              /oo
Puaip
Vacuum
In.  Hg
                                                     i.v
                                                            Icpinger
                                                              Temp.
                                                     /*?•-.
Oven
Ter.o .
 °F
                                                              372-
Probe
Ten?.
 6F
Stack
Teno.
 °F
                                                                                       23$
Sta'
Ter
 CR
CF
         1.1
          , 0 y
                   57
                 1.
                                        jut*
                                                      /o-O
                                               /• 7
                                                                                2,0
                                                                                   *2-
Comments:
3/16/77
                   / 7
                         ,56  •
                                  fCrO ,
                                                      /(rf
                                                      /&
-------
                          SAMPLE CLEANUP  SHEET
Plant: // iv« "*.» ,W,v-/
Address: v'J^ ,,- ,.#v,t,. — .
^' Date: /^'.-'•/Xr.//r7
Operators: -^.i'/^^-'
Station No. : .;' -//. ,- : '
Run No. : £1
Barometric Pressure: '^Lf.
Ambient Temperature: /to
Sample Box Number: /

Impinqer 1
Final Volume /be?
Initial Volume ,'&!_,
Volume collected c*
Impinqer 2
Final Volume 9^
Initial Volume 7 oo
Volume collected —(,
Impinqer 3
Final Volume &
Initial Volume <-',.... L,
Volume collected ' xr>
Impinqer
Final Volume \^
Initial Volume \^
ml of Oi^ 1. ^-"' /'\j 0
ml
ml
ml of Pi < 1 • 'l^ U 5 C
ml
ml
ml of
ml
ml
ml of
ml
Volume collected ^^^^ ml
Impinqer
Final weight 7 '.^^ °
Initial weight 1-5 J . t
Weight collected -7. ^
Total Volume Collected /
Fi 1 ters
No. Final Weight
1 <*• . qm
qm
gm of '^. '..-_.-.. G< I
gm
gm
ml
Weight
Tare Weight Collected
qm gm
qm qm
Cleanup performed
on

-------
                                                RECOW OF YISVAt, DETEPfllMTMK OF OPACITY
                                                                                          PAGS_
O
C.
             COMPANY
             LOCATION rtffl&ti  * I-
TEST NUMBER
DATE
                          /77
TYPE FACILITY v-^u/^
/~-^
raOC
                                                    "ft-^r
                                            -Tar5"
                                                                       HOURS OF OBSERVATION //. VsT- /V..57
                                                                       03SEHVER ^ X/
        OBSERVER CERTIFICATION DATE.
        OBSERVER AFFIUATICII/Al/S
                                                                                    POIfiT Or EMISSIONS  ST/J
                                                                                    HEIGHT OF DISCHARGE POINT
o
p
O
J5
o
et->


























Final











F
1
1
SUMMARY OF AVERAGE OPACITY
Set
Number










leadings i
'he source
the tir.c <
TVo
Start-End










OoacUy
S'JT










•anqed fro.Ti to % cpcc
; was/was not in ccnpliance, wit
: valuation was rade.
/'vcrcgc
-.,









iiy
h 	 it

-------
COV?A
LC:AT
TEST
PATE ,
OBSERVATION RECORD PAGE t OF 1
VY (Yi, \idfVi i^.-u :-rc,
n-/

IV.



1 —
	
^^mm^
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rt— 1
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— -i —

	







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2
3
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23
Seconds
0




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la , 3H | £3
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STEAM
(ch?C'' If
7i-:tocT?T






















TYPE FPCIL1T
POINT CF EX1
•LU.1 iE
iT^l Iciblc^
ilCUChoS























Y sr.-^d- ,^i/i i
5510|ib -.r/i •- '--

CCMHEHTS
























COUPA
L OCA i
TCST
DATE


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45
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50
51
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n oos.7
                                                           OBSERVATION RECORD
PAGE	OF_
                                                                   OBSERVER 	
                                                                   7T?c rAClLlTV s -i^-.
                                                                   POINT OF EMlSS10;i7"Tr>I2L
                                                       D05.7i-201}0 FUcd 11-11-74.U:«5 us]
KDt-lAl KCCtJTE^ VOL 39, NO. 219_7U:St»AY, NOVWfltR 12, 1974

-------

Run
Location

Date
Operator >
                                   RTIi        1     ATA

                            VERY IHPORTANT -  FILL IN ALL BLANKS

                            Read and record at  the start of
                            each test point.
                                     Time:  Start  Tiire_

                                            End Time	
                                                                            Ambient Temp *F
                                                                            Bar. Press. "Hg  C? f~. /"/'

                                                                            Assured Moisture  Z    (. "*
                                                                   Probe Tip Dia. In.  <• -2
                                                       /£,
                                                                   Picot  Tube No. ."5~~J
Sample Box No._

Meter Box No._

Meter A H	

C Factor   /. /5
                   /
                                                                   Probe Length/type
                                                                               ...
                                                                   Filter No. /- ^
             /. 6 S
                                                                                  -•*     /  •
                                                                                  /  / V J '
  Point
Clock
               Dry Cas
               Meter, CF
Pitot
in.  H,0
  AP
Orifice fiH
  in H20
                                  Desired   Actual
                                                  Dry Gas temp.
                                                      °F
                                         Outlet  Inlet
Punp ,
Vacuum
In.  Hg
TCP?.
 "F
Oven
Te~p.
 °F
Ten1?.
 •F
Stack
Tcro.
 "F
 tack
Ter-p.
 °F
                  /-
                ?;"' X "
                   '//
                                                                       /'/*
                                                                       //&
                          r - A-
                         f,/)
                                                                                       v'i'V
                                                                                x'

          Jl
                                                                                   J//

                                                         /V
                                                                                                         (,
                                                                                          670
                                                                                                   6,76
                                                      7
                                                        /'f
                                                                                            3 a*
 Coments:.

-------
                                                                        aheec
                                                              -' -r
 Point
10
     Clock
         (,-.&
Dry Gas
Meter, CF
               "03 .
                    -9
                  L±
Pitot
in.  H-0
  AP
                          , So
                Orifice AH
                  in H20
                                Desired
                                  9o
                                  ,9o
                                     Actual
                                       .1*?
                                               Dry Gas Teirp .
                                                   °F
                                 Outlet
                                              137
                               Inlet
                                  /3
                                                13$
              310. II
              •3/3,11
Pump
Vacuum
In. Hg
                                                                 lopinger
                                                                   Tenp.
                                                                   /if
                                                          A3—/I
                                                I.I   |   /H9
                                                               Oven
                                                               Ten? .
                                                              J&9
                                                                                  Probe
                                                           111-
                                                                           P-7/
                                                                 tack
Stac!
Terp,
                                                                       Lcr
                                                                                      2-10
                                                                                               6,-?
       7?
                                          ,70
3/?..»./
                                  .vi
                                     Ch
                                              131
Comcients!
                                                                                        in
                                                                   ffl*
                                                 /O"
                                              iff
3/16/77

-------
                         SAMPLE  CLEANUP SHEET
Plant:
                                           Date:
Address: " X^.-,i_e ^V
Operators:
Station No.: rv-- / :
Run No. : -^ V
Barometric Pressure: Z*.F. 7Y
Ambient Temperature: sr^'"
Sample Box Number: /

Impinger 1

     Final Volume
                          /(
     Initial Volume
     Volume collected_

Impinqer 2

     Final Volume
                                _ml of
                                jnl
                                ml
     Initial Volume
     Volume collected_

Impinqer 3

     Final Volume
                                ml of_
                                >1
                                ml
                           c?
     Initial  Volume	
     Volume collected

Impinger

     Final  Volu>
     Initial  Volu
     Volume coll

Impinqer

     Final  weight	
     Initial  v/eight	
     Weight collected_
_ml  of
_ml
 ml
                                ml of
                                   of
                       -7/7
                                gm
Total Volume Collected_

Fi1ters
                                          /
No.
               Final  V'eight
                           gm
                                     Tare Height

                                     	gm

                                     	gm
                      Weight
                      Collected
                                                              _gm
Cleanup performed by
                                                on
                                                    *//*/?> -

-------
                                                    RECORD Or YISU/V. DETCRHIWWK Of OPACITY
                                                                                                  PASS
o
c;
               COMPANY..
               LOCATION	
               TEST NUMBER
               DATE    •
TYPE FACIL1TY_
CONTROL DEVICE
                                       //£><->--.£
                                                                              HOURS 0? 03SERVATJOJK
                                                                              OBSERVER     )A/   ~7~r'
    OBSERVER CERTIFICATION GATE
    OBSERVER AFFILIATION
    POINT OF EMISSIONS '
    "HEIGHT OF DISCHARGE FOMT r* ^p '
o
u
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OBSERVER LOCATION
  Distance to Discharge
  Direction from Discharge
  Height of Observation Point
BACKGROUND DESCRIPTION
HEATHER COMITIOw'S
  Wind Direction
  Wind Speed
  A.m.b1cnt Temperature
SKY CONDITIONS (clear,
  overcast, X clouds, etc.)
PLUKS DESCRIPTIOft
  Color
  Distance Visible
 OTIIC^ 1KFOOT10II
                                             Intal
                                              LlfafL
                                                           Final
          SlWIttRY OF AVERAGE OPACITY
                                                                                           Sot
                                                                                         Number
                                                                                                       Start— End
                                                                                                            Osjcity
                                                                                                          S-j-n
Readings ranged from
                                                                                                   to
                                                                                                                            opacity
                                                                                        The source was/was not In ccnpllancc with ,
                                                                                        the time evdluaLion v;as rracie.

-------
OBSERVATION RECORD        -PAGE	OF	
LC-ATJC'i _—i •- 'f-,, >i
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                  FEOIMl RIGIJTCZ, YOU 39, NO, 219—7U;SDAY, NOVEMBER 12, 1974

-------
Plant	x
                                               CULj     ELE

                                      VERY IMPORTANT - FILL IN ALL 3LAMCS
                                                                            Ambient Temp  "?_
Run No.
Location
Date /i".
                                      Read and record at  the start of
                                      each test point.
                                      Time:  Start Time
                                                                           Bar. Press. "Hg    >.? fr • ^

                                                                           Assumed Moisture 7.   C*	

                                                                           Probe Tip Dia. In.  C • 3-]$
Operator/*^,
                                            End Time    /Old)
Sarple Box No._

Meter Box Ho._

Meter A 11
                                                                            Pltot Tube Ho.    o "  i	

                                                                            Probe Lengtli/type   c  /(?/<-*<*

                                                                            Filter No. 6;   .
C Factor   /•
                                  7£'
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 Li£
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          If?
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In.  H,0
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Orifice  AH
  In It20
                                  Desired  Actual
                                  //*
                                  X/o
                                   /-
                          0
                                  0
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                                          /
                                                  Dry Gas Temp.
                                                      °F
                                                  Outlet  Inlet
                                                          2/
                                                           73
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-------
                                                         X7*"- /
                                                                      Sheet g2.  of
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Clock
Dry Gas
Pitot
in. H20
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Orifice AH
  in H20
Desired
                                       Actual
                                              Dry Gas Temp.
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                                        Inlet
Pump
Vacuum
In. Hg
Impinger
  Temp.
   oF
                                            Oven
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                                             Teap.
Stack
Ten?.
 op-
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Tenp.
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D-'s
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                                              a-5
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3/16/77

-------
                                                                         Sheet  "S of
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Clock
Dry Gas
Meter, CF
PItot
in.  H~0
  AP
Orifice AH
  in H20
                                 Desired
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Impinger
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Comments:

3/16/77

-------
                         SAMPLE CLEANUP SHEET
Plant:
                                            Date:
Address:
Station No
Run No.:
Barometric
7 	 -r-
m *
s?t
*£'£• ^
Operators:
•
•
/ ' •

>f / Ambient Temperature:
Pressure: 
Impinger 1

     Final Volume
     Initial Volume
                          / S"
Total Volume Collected

Filters
No.
               Final Weight
                           gm
                          _gm
Cleanup performed by
                                _ml of
                                jnl
                                 ml
                                 ml of
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                                 ml of
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                                 ml
                                 ml of
                                ~ml
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                                 ml
Tare Weight

	gm

	gm
            •


           on
                                                       Weight
                                                       Collected
                                                                gm
                                                                gm

-------
                                                    RECORD OF VISUAL DETCRHHttTIOK OF 0?AC!TV

                                                                                                 PAG"  / C?X'
               LOCATION,/Sv.^  -
               TEST MJKBER_2±/_
               DATE
               TYPE FACILITY
               COIJ1P.OL DEVICE
                                                                             HOURS or ossERVATiofr.
                                                                             OBSERVER
X:-  --S-v -•-
                                                                             OBSERVER CERTIFICATION DATE,
                                                                             OBSERVER AFFILIATION'   &/. /"
                                                                             POINT OF EMISSIONS /;^/
-------
                            OBSERVATION RECORD
                   PAGE
OF£_
LC1ATIC
TEST I;1."'.'I7T
PATE
7v?t fY-cinT7
POIHT CF EM!
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                                                            [Pit oo5.74-aeiio
                                                                                                                  Il-ll-74i8:4) wa]
          TEDI2AI UC1STE2, VOL 39, NO. 219~TU£tt>AY, N
                                                                                              !2, 1974

-------
Plant
Run No.
Location
Date   /f,3~. I  / /,

Operator £r /( fJ<^~>
                                            ICU"     IEI     A

                                   VERY IMPORTANT - FILL IN ALL BLANKS

                                   Read and  record at the start of
                                   each test point.


                                   Time:  Start Time    I O l) Q

                                          End Time     ( £.%
                                                         Ambient Temp *F
                                                          Bar. Press. "Hg
                                                Assumed Moisture 7.

                                                Probe Tip Dia. In.

                                                Pitot Tube No.
                                                                         V "  '
Sample Box No._
Meter Box No.	

Meter A H	/

C Factor	/
                                                                        Probe Length/type

                                                                        Filter No. ~7  .
                                                       /S"  l-k -
  Point
        Clock
Dry Gas
Meter, CF
Pitot
in.  H,0
  AP
Orifice AH
  in H20
                  Desired  Actual
                                               Dry Gas
                                                   °F
                                                      Temp.
                                               Outlet
                                                      Inlet
Pu
Vacuum
In.  Hg
Inplngcr
  Temp.
   °F
Oven
Tenp
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Teirp
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Temp.
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-------
                                                                                 of  ->
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-------
                                                                          Sheet 3  of 3
 Point
        Clock
Dry Gas
Meter, CF
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in.  H-0
Orifice AH
  in H20
                                 Desired
                                         Actual
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                                  Outlet
                                Inlet
Pump
Vacuum
In.  Kg
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  Temp.
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Oven
Tetnp .
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Tercp.
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3/16/77
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                                                                 P3C-
                                                                   35
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                                                                                                  4/7

-------
                          SAMPLE CLEANUP SHEET
Plant: A... ^~z€ -. -X^-,-
Address:' ^^-.x , ^
Station No'. : ' ^: -^ :?
Run No.: .«-~»
Barometric Pressure: ^r. j"1"'
Dote: £y^fx£';-
Opera to rs : ,^XX_ /^v
: "/^V/ /'i ^L^
Ambient Temperature: /*->«>-
Sample Box Number: /

 Implnger 1
      Final Volume
                                  nl  of
Initial Volume //? =. ml
Volume collected - *-/ ml
Impinger 2
Final Volume
Initial Volume
Volume collected
Impinqer 3
Final Volume
Initial Volume
Volume collected
Impinqer
Final VW-mpe
Initial VoluTna^
Volume collected^
Impinger
Final weight %
Initial weight ^

<.-^> ml
Z ml
0
(-> nil
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ml of
ml
ml
r T / c*1^ £ s s
'/£• o gm ''
Weight collected £ c qm
Total Volume Collected i
6- S ml
Filters
No.
               Final Weight
   /
                           gm
Tare l.reight
Weight
Collected
                                                               _gm
                                                gm
                                                               _gm
Cleanup performed
                                                 on

-------
              TEST K'JKEER
              DATE    9
TYPE FACILITY^.
CONTROL DEVICE
                                                   WCQRO OF yiSUAU DETCPJIIHATIOK OF OPACITY
                                                                                                 PASc / of
                                .  ,/
                                                                            HOURS OF OBSERVATION   ^/
                                                                            OBSERVER   X '' .rC- /^-c _'~
                                                                            OBSERVER CERTIFICATION LV,TE_
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CLOCK TIME
OBSERVER LOCATIOH
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  VHnd Speed
  Ambient Temperature
SKY CONDITIONS  (clear,
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PLUKE  DESCRIPTlOft
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-------
                           OBSERVATION RECORD
                         PAGE
       _ ' --•• Q. . -". -"_^-L..


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PATE
       essrRVCR  X-"9-: -^* ,.
       TYPE  FACILITY "  s'-.^--?,,,/:
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   OBSERVATION' RECORD
(Continued)
PAGE	OF
                                                                          C(W?A','Y
                                                                           TEST UMBER
                                                                           DATE _
          02SEWE3
          7Y?c FACILITY
          POINT or i
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-------
Plant
Run No. ^ .7
Location_

Date   (->
             •s   /^

            >/-=» -V
       /   '
Operator_
                                UL/'     ELD

                      VERY IMPORTANT  -  FILL IN ALL BLANKS

                      Read and record at the start of
                      each test point.


                      Tine:  Start Tire  /v/\S

                            End Time
                                                                          Ambient Tern? *F
                                                                          Bar. Press.  "Kg
                                                 Assumed Moisture 7,

                                                 Prebe Tip PJa. In._

                                                 Pitot Tube No.   >
Sample Box No._

Meter Box No.
                                                                          Probe Length/type
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                                                                          Filter No.  7*  .
Meter A H    / f'. ?T

C Factor
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    sv
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in.  H,0
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  in  H20
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    °F
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Pump
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In. H8
Impinger
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Oven
Temp.
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Temp.
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-------
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                 £./(*
                      7
                                                                                   .?'•'**
3/16/77

-------
                                                                        Sheet
                                                                        of
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Clock
Dry Gas
Meter, CF
                        Pitot
                        in. H«0
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Orifice AH
  in H20
                                Desired
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                                               Dry Gas Temp.
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                                                      Inlet
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In. Hg
Impinger
  Temu.
   °F
Oven
Ter.o .
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Probe
Teno.
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Ter.n .
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A   *
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Comments:

3/16/77

-------
                          SAMPLE  CLEANUP SHEET
 Plant:	
 Address:	
 Station No.:
 Run f!o.:
     jDperators:
Pate:.__fc/£^£z
nr<; •   .s/ '/. /{.'
 Barometric Pressure:
   __Ambicnt Temperature:
   _Samplc Box Number:	
 Impinqer 1

      Final  Volume
ml Of
Initial Volume /o_-
Volume collected - ~7
Impinqer 2
Final Volume
Initial Volume /„&
Volume collected /of
Impinqer 3
Final Volume
Initial Volume 0
Volume collected
Impinqer
Final vVlume
Initial VtsLyme
Volume collected
\
Impinqer
Final weight "J.Z*? -J
Initial weight -^.-3. r. /."
ml
ml
ml of £^TC£
ml
ml
ml of u'/^r-f-.^
ml
ml
ml of
ml
ml
gm of f'LSr,* A_. f
gm
Weight collected 9- -C gm
Total Volume Collected 5, . 5
Filters
No. Final Weight
P . qm
qm
ml
Weight
Tare Weight Collected
gm qm
qm qm
Cleanup performed by
                on
                       (/
                   j 
-------
                                                  rccoao OF yis'JAu DETERMHWXON or OPACITY                   pAss_Lpf_i
n
n
C>
COMPANY /ft?*'1 <*«-•" &&*(• Co
LOCATION C> M o "J, 	 ...
TEST KUKDER 1>
DATE //p" ) 1 LL /°l1'l
TYPE FACILITY ,S-io I \M • I/
i\ i
CONTROL DEVICE 1?* • UJw A
o ^j
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% ^^HTIJWTO c

HOURS 0? 03SERVATIOH r
~l i- / ^ C'
OBSERVE!* CEPJlFICi\T10.ir>D.\TE
03SEKVER AFFILIATICH T I3 /I
POIliT OF EMISSIONS £•/«.;'
riEIGIil Or DI5CI!/\Kui r'JI.u / O

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O
V)
I
1
CLOCK TIH£
OBSERVER LOCATIOK
  Distance to Discharge
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BACKGROUND DESCRIPTION
WATHER CONDITIONS
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  Anblcnt Temperature
               SKV CO«OITIONS
                 overcast, % clouds, etc.)
               PLL'Kt  DESCRIPTION
                 Color
                 Distance Visible
               OTHER UIFOKuUIOll
Initial
•ifl1

-------
             OBSERVATION' RECORD
,.wi. A \.
       •
                              PAGE  1  OF J

                              C?
                           .
                           f—   I
L--lT:c'    '"' ;' J
TEST i.-j1'::,'.   p.-.

PATE    »-i / .'i 1 i i 'i
TYPE FACILITY

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                                                                                                     OBSERVATION RECOilO

                                                                                                  (Continued)"
                                                  iccArioM""""

                                                  TEST II'JKSCK

                                                  DATE 	
                                                                                              TYPE: FACILITY
                                                                                              POINT OF EK
                                                                                           PASS	OF , _
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1
                                                                               [rn Dos.74-:eiso
                                                                                        i:-u-7-i.8:<} MS]
                           BIOSTE8, VOL 39, NO. 319—TUZS&AY, NOVLM3I2 12, 1974

-------
Plant //fart 7K£ '' o) 6vVx VERY IMPORTA'JT - FILL IN ALL BLANKS
Run No. •// ^/
Location {} '-/ & •'
/1 . I if- /<&-/•-?
Date y/^'/ • / / ^ . / / / , '
-///'/,}.<£
Operator — •/ /C. / A.' • -'s
Sample Bo
Meter Bos
Meter A 1
C Factor
x No. %""/
No. ,^


6^l«5y
^-ir'( 51
Pitot
in. H.O
AP
fl-Vi
C?.V
0- ^X
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^-V~o
O.^c
<9.M
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C'P '. -
<9 m
O Ml
o » L M

^,7.)
O '^-c
Read and record at the start of
each test point.
Time: SLafC Time C> ^ £ I
End Tiire O* 1 S VJ
Anbicnt Temp °F ft (.'
Bar. Press.
-Hg -?^ /'/
Assumed Moisture
2 &
Prcbc Tip Dia. In. /"^ /•/'/
Pitot Tube !!o.
.-• '
> •'
Probe Lengtli/cype •*" /


Filter No. 7 , ,
U,uc.U,l.
Orifice AH
in H20
1
Desired ' Actual
rf ?,? 0 r;"'
,"i ") '"• O."'/:-
<:r °l 1. 1 r> Id,
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Dry Gas Temp.
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11
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Consients:

-------
                                                                              Sheet  ^ of   •>
                                                                     0 H ° •>-
  Point
    1
Clock
Dry Gas
Meter, <
     Pitot
     in.  H90
       AP ~
Orifice /
  in H90
                                  Desired
                                  (j '• ''o
                           1-00
                                   Actual
                                  c"; -
                                          Dry Gas Temp.
                                   Outle
                                Inlet
Pump
Vacuum
In. Hg
                                                         Inpinger
                                                           Temp.
Oven
Temp.
 OF
Probe
Temp.
 °F
                                                                    Stack
                                                                    Temp .
                                                                                                     Stack
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    c
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Comments:

3/16/77
)QQ. l*|
0-ft
                 16 1. M
                  O . '-1
                                     vi
                                                                            136
                                                                                       IT]
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                                                                                        It
                           0
                                    1 - 10

-------
                                                              OC./09
                                                                               Sheet
                                                                                of S
  Point
Clock
Dry Gas
Meter, CF
Pitot
in. H00
  AP '
Orifice AH
  in H00
                                   Desired
                                   Actual
Dry Gas Temp.
    °F
                                     Outlet
                                  Inlet
Pxinp
Vacuum
In. Hg
Impinger
  Tenp .
Oven
Temp.
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Tenp
 °F
Stack
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 °F
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 °F
     1
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Comments :
                                                                                       5

-------
                         SAMPLE CLLAHUP SHEET
Plant:
             7<,*+ J/..-,
Address: X-->, //..v, //^
Operators: '
Stati on No . : o y c ^ :
Run No.: *-f
Barometric Pressure: 3$'*?fi

Impinger 1
Final Volume /c <^
Initial Volume /&<:>
Volume collected «
Impinqer 2
Final Volume f*5~
Initial Volume y o o
Ambient Temperature: f'Z"
Sample Box Number: /

ml of /)/$/• /I? J ^c
ml
ml
ml of £•£?•'&<* /6 O
ml
Volume collected — S' ml
Impinger 3
     Final Volume	c
      Initial Volume
     Volume collected_
Impinger
     Final Volume
                          c-
      Initial Volume
     Volume collected_
Impinger
     Final  v;eight
                 	
     Initial weight
     Weight collected   ji/ .
Total Volume Collected    9:
Fi1ters
No.
               Final  Weight
                           gm
                           gm
                                 ml  of
                                               '4-
                                _
                                 ml
                                    of
                                _
                                jnl
                                .ml
                                  m of
                                _gm
                                _gm
                                ml
                                     Tare Weight
Weight
Collected
                                                               _gm
                                               gm
                                                               gm
Cleanup performed by
                                                on

-------
n
n
0
                                                    RECORD OF VISUAL DETOMIKATIOK OF OPACITY
                                                                                                 PAG"  /  of/
	 •''•"' / LLL^-^
COMPANY ^-t*x=*?=, ^-^
LOCATION .-'^'<-C^ ; 6'\ 	 .
TEST KuflBcRV^"/ ' C'/C'>
DATE '• i-//;^/? '~7
TYPE FACILITY' 17^1 '*-*.*!(
CO.'llROL DEVICE tf/\c.hrrt-S










HOURS OF OBSERVATION 1A/
OBSERVER ^r^'^< *••*' 	 .
OBSERVER CERTIFICATION DATE
OBSERVER AFFILIAT1CII L'. S~ (=". rt <" •
POIIJT OF EMISSIONS 
•O
V
CLOCK TIME
OBSERVER LOCATION
  Distance to Discharge
  Direction from Discharge
  Height of Observation Po^nt
BACKGWUNO DESCRIPTIOf!
 ' 7,-ER CONDITION'S
  Kind Direction
  Wind Speed
  Ar.bicnt Tenpcrature
SKY CONDITIONS (clear,
  overcast, % clouds, etc.)
PLUM? DESCRIPTION
  Color
  Distance Visible
 OTIICK IHFOK1AT10II
                                             Initial
                                                          Final
OF AVERAGE OPACITY
                                                                                         Set
                                                                                       Number
                                                                                                     Start-End
                 OozcUy
                                                                                       Readings ranged fron
        to
2 cpaciiy
                                                                                      The  source VMS/was not in ccnpli:ncc with t-
                                                                                      the  tiir.c evaluation was race.

-------
CCiV?A\f  "/•'
LCl^TIC1.1"^:
irsT .'"vv.2c.''.  "•<•/  -
PAfE    -/', - /->-,
OBSERVATION1 RECORD        PAGE I   OF/
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CKWIY
LOCAHOM
TEST NUMBER
DATE	'
                                                                                                    OBSERVATION RECORD
                                                                                                  (Continued)
OBSERVE*
TYPE
P011IT OF
                                                    PAG:	OF,   ,

Mr.






















.








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30
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                       DOJ.7-V-261JO
                                                                                                                11-11-74,8:4: US]
                                                           VOl. 37, KO. 219—.TUSSDAY, NOVmBtR 13, 1974

-------
                                                    2LD
Plant   I I  iC^g \
                                   VERY IJIPORTAMT - FILL IN ALL BLANKS      Ambient Temp "F   ££"
Run No
        •ii  C
     .  "  •=>
Location  CM

Date
Operator_
                     Read and record at  the start of
                     each test point.
                                   Time:  Start Time_

                                         End Time
                                                                       Bar. Press. "Hg  3 5
                                                         Assuncd Moisture 7._

                                                         Probe Tip Dia. In._

                                                         Pitot Tube No.   •!
                                                                                          -?«/.  |.50
                                                                                 Jli
         10
:Ui2i
-.  I-
hi  I |63>
                                                             H-o
                                                       I.3C1
                                                                           JS5
                                                                               06V
                                                I
      a.
 ja^Ji
                           /-.( >
                   Soi  I- ^o
 Consents:
          /£,
                         0--3>6
                                        o-H
                                 _Lil	\	1
                                               H  •>

-------
                                                                                  «£
                                                                w. b
Point
Clock
              Dry Gas
              Meter, CF
                    Pitot
                    in. H20
                     AP
                         Orifice AH
                           in H20
                                Desired
                                 Actual
                                               Dry Gas Temp.
                                                 Outlet
                                                   Inlet
Pump
Vacuum
In .  Kg
Impinger
  Tenp.
Oven
Tenp.
 °F
Probe
Temp .
                                                                                     O 11
Stack
Tenp.
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Stack
Te:rp.
                                                                                                 0 1-1
   1
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Conmients:

3/16/77
                                 o
                         6
                                    -de?
                                                       '?
                                                                         s
                                                        3-0
                         O -
                                  o
                                           I00

-------
                                                                                          of
Comments:




3/16/77

-------
SAMPLE CLEANUP SHEET
Plant: //"'"•'• -/,£/,< J^.- /
Address: >V-_,^. .. <^-
' c:- Hate: -/'^/' '
Operators: ?)^'_.,(i
Station No'.: X^--? ' ''
Run Mo. : >*• S"~"
Barometric Pressure: '2 f y"/
Ambient Temperature:
Sample Box. Number: /

Impinqor I
Final Volume *y 3
Initial Volume /^o
Volume collected - V
Impinqer 2
Final Volume 9?
Initial Volume /co
Volume collected ~~ /
Impinoer 3
Final Volume
Initial Volume ^Vt/'/'i c
Volume collected '
Impinqer .
Final VolumeX^
Initial Volume ^-v^
Volume collected "\.
Impincer
Final weight ~^'-^~^' *J
Initial v;eight ^^'^ 0
Weight collected , /
Total Volume Collected -S 3-
Filters
No. Final Weight
/£' gm
gm
Cleanup performed by // /c2^
/ * ' / '
ml of ^>-*/' 'fa"' /'; -'
ml
ml
ml of /?, '-/' '-^J /-£ -'
ml
ml
ml of
ml
ml
ml of
ml
ml
gm of S •' '' c-^ Co'< /
gm
gm
ml
Weight
Tare Weight Collected
gm gm
qm gm
// *
'-' J^r^ on ///'''•'/ A^ /9~S

-------
                                                   RECORD OF VISUAL DETOM1M7IOK OF OPACITY
                                                                                                 PAGZ
o
              COMPANY1	
              LOCATION	
              TEST NUXCER.
              DATE	
              TYPE  FACIL1TY_
              CONTROL  DEVICE
                                                                            HOURS Or OBSERVATION.
                                                                            03SERYER
                                                                                                 ii LVJE
                                                                            OBSERVER AFFILIATION
                                                                            POINT OF EMISSIONS
                                                                             HEIGHT OF DISCHARGE FOI.TT
o
M
o
o
m
01
      TIME
OBSERVER LOCATION
  Distance to Discharge '
  Direction from Discharge
  Height of Observation Point
BACKGROUND DESCRIPTION
VEATHER CONOITIOHS
  Kind Direction
  Vlind Speed
  Arsbicnt Temperature
•SKY CONDITIONS (dear,
  overcast, 2 clouds, etc.)
PLL'Kc DESCRIPTIOK
  Color
  Distance Visible
       1NFOOTIOII
Initial











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'










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•

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I
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SUWttRY OF AVERAGE OPACITY
Set
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'he source
the tir.c <
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•anged from to £ o?:c
» was/was not in ccnplicncs wit
:vd1uat1or. was rrac'c.
/•/erase









iiy
h tt


-------
OBSERVATION RECORD
                                                   PAGE
L*J.
PATE
       TYPE FACILITY
       POL'iT CF
         //-, /-v -7
,1-J
IV. l"(n.
/' . ' 0
	
_____







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  OBSERVATION RECORD
(Continued)
PAGE	OF
                                                                      COMPAVY
                                            7CST W.W3ER
                                            DATE _
          OBSERVES __
          TYPE rACILlTY
          POINT OF
llr.






























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                                                                  005.74-201:
                                                                                                          n-ii-7*;u:'.j
                                          KOESAt RSOISTC?, VOL 39, NO. 219-.TUESSAY, NOVH?A3EB 12, 1974

-------
                                                            :LD
Plant
                                        VERY IMPORTANT  -  FILL IN ALL BLANKS
Ambient Tc-np "F
                                                                                                    o
^ 1 ,
Run No. **•/ -i si' ." i&Z
*
(,ut\. <-/ r;
/Tc' Ij C, (i H
1
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1 1-
M..-.J k
/••
X" / vi, -^4
Location ^f*^-?
3ate__g?V
Operator
Sample Bo
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Meter A H
C Factor
^ ^ ,9_,^
L.A' (^'. (>;
x No. (
NO. :z
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Point
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7,
6
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Meter, CF
73 -f
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74T-770'
7«/«/^
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in. H20
- ^ 7^-
,•;/.<•
^,^i
	
^.6'-s
—
"0.62-
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Read and record at the start of
each test point.
Time: Stare Tine
End Time
Bar. Press.
"»g *j. y ^ri
Assumed Moisture
7. ¥
Probe Tip Dia. In. , .? / ^
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7- /
Probe Lencth/cype . '•' j

Orifice AH
in H20
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-------
                         SAMPLE CLEANUP SHEET
Plant: /V 	 //. „ ,< /» /
Address: 7 '•..-./..> // , , L.. 	
Station No.: o LLx^ -*<^ty
Run No.: xz^j1' ^HX"1'"
Barometric Pressure: 3.*. ~ih

Impinger 1
Final Volume \f>o
Initial Volume 1 1?,.
Volusne collected 6
Impinger 2
Final Volume c/ 1 • 5
Initial Volume 1 t> o
Volume collected —
-------
0
U
0  C
      0
      A
                Plant
                Run No.
                                                           •     :UL/<     ELD

                                                      VERY IMPORTANT - FILL IN ALL BLANKS

                                                      Read and record at the start of
                                                      each test point.
                                                                  Ambient Temp "F
                                                                  Bar. Press. "Hg_
                                                                                                               A' '7/0
                Location
                            a
                Date  St.**. S /J /I* ' '/*
                                                      Tire:   Start Time
                Operator_
                                                            End Time     O>  \
                                                                  Assu-ned Moisture Z_

                                                                  Probe Tip  DJa. In.	

                                                                  Pitot Tube No.   d  ~~ /
                                   I
                 Sanple Box No

                 Meter Box No.	^L.

                 Meter o H	/ & ^

                 C Factor
                                                                  Probe Lcngth/type_

                                                                  Filter No.
                   L
      C
                                    C t.
                                               O*
L^\C'
                   Point
                 /I
Clock
                          ^L
                         in
                         U
                                     Dry Gas
                                     Meter, CF

                                          U
                               T55/H
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in.  H-
  AP
                                         0
                                           0 •'Co
                                          6
                                           Q.^lg
                                          ^ . fto
                                          0
                                          o
                                                   Orifice AH
                                                     in H0
                                                 Desired  Actual
                                                           1-15
                                                     Lol
                                                                      a?*l
                                         Dry Gas^Tenp.
                                            •F
                                                                  Outlet I Inlet
                                                                 C- o
                                         6
                                                           1.35
                                                   /•go
                                                     Jo
                                                     >flO
                                                     I  oo    I -00
                                           JL
                                                                          Lcl
                                                   i  -oo
Pump
Vacuum
In.  Hg
                                                                                J'O
                                                       5-0
                                                       3-o
                                                                                S'O
                             Irpinger
                               Temp .
                                "F
                                                                                  l-o
                                                                                3  c
                                                                                5  -o
                                                                                         li
                                                                                        16
Oven
Tenp
 "F
Probe
Tonp.
 °F
                                                                                                  (,5
Stack
Tepp.
 eF
                                                                             All
                                                                              TIC
                                                                                                              /I
                                                                                                            135
                                                                                                                   7)!
Stack
Te--?.
 °F
("F+460)
                                                                                                                        -* ' A
                                                                                                                   4-7?
                 Consents:

-------
                                                                       Sheet JL   of
 Point
 -
Clock
Dry Gas
Me
Pitot

in.  H-0
  AT* ^
  Ui.
Orifice
  in H.,C
Desired
                                        Actual
Dry Gas Temp.
    °F
                                       Outlet
                                              Inlet
Punp
Vacuum
   Kg
                                                            i.o
Iinpinger
  Temp.
   op-
                                                                    Oven
                                                                    Tcnp
                                                                     Of

                                                            10
                                                  Probe
                                                  Te^.p .
                                                                                  OTT
                                             Stack
                                             Temp .
                                                                                        OT?
Stack
Tec?.
 °F
(°F+460)
0- 1
M.
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 C'- C,
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                                                                          */
-------
                                                                      bneet
                                                                               of
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C-7
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£-4
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        C
        /o
Dry Gas
Meter, CF
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in. H00
  AP "
                        0-6^
                        0
                        0 "IS
                        CD
Orifice AH
  in H00
                               Desired
                                1-
                                 ). lo
                                       Actual
                                        1-1,0
                           I  lo
                                              Dry Gas Temp.
                                              Outlet
                                              70
                                 "It
                                 11
                                 1!
                                        Inlet
                                                    "U
                                              11
                                                     16
Pump
Vacuum
In. Hg
                                              2-0
                                                            a o
                                                              -o
                                                            a-
                                                           a . o
Impinger
  Temp.
   CF
                                             lo
                                                                           Oven
                                                                           Tes?
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Temp.
 °F
                                                    341
                                                                                     Stack
                                                                                     Tenip .
                                                                                      °F
S tack
Teir.p.
 n «

(°F+450)
                                                             574
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                                 1  10
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                        6 -
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                                        -ac
                                               IS
                                                    I  -
                                                                    lo
                                                       -13L
                                                                    13
[-*/
f- i
Connients:

3/16/77
                        0-10
                                 . 10
                                  -35
                        c'-V
                                        l.lfl
                                 15
                                     2-0
                                                                           346
                                                      -51
                                               iM  :
                                                            2-c
                                                                           3 MM
                                           • J?
                                           *T
                                                            3 -o
                                                                                       17,6
                                                                                       /|C-

-------
                         SAMPLE  CLEANUP SHEET
Plant:	
Address:__ 'TT-'-^o/   ••
Station No.:   'G'Sc.
Run No.:   -^ /
              ,.,^^fe*
Barometric Pressure:
                                     Operators:
                     _Ambient Temperature:   --_.
                                                on

-------
1
 n
 O
TEST KUKEER
DAT E
                                 / X
               TYPE FAcllTY
               CO-'HROL DEVICE  <
                                     RECORD OF VISUAL DETOfllKATIOK Or  OPACITY
                                                                                                                PAGc /  o? /
                                                                                           HOURS OF OBSERVATION	^
                                                                                           OBSERVER S^s? Xvc ^-
                     lRVtP. CERTIFICATION LVJE
                  OBSERVER AFF IL IAT1C"   ^
                  POIIJT OF 'EMISSIONS  ^  xl
                                                                             HEIGHT OF DISCHARGE FOI.NT
"u
.-°
O
 r
 O
 .5
 O
    '^ TIMS
OBSERVER LOCATION
  Distance to Discharge
  Direction from Discharge
  Height of Observation Point
BACKGROUND DESCRIPTION
KATHER CONDITIONS
  Wind Direction
  Wind Speed
  Anbicnt Temperature
SKY CONDITION'S (dear,
  overcast, % clouds, etc.)
PLL'KE DESCRIPTION
  Color
  Distance Visible
 OTIIta IIJFOKIUIOII
                              Initial
Final
SUWWRY OF AVERAGE CPACIT/
                                                                                          Sot
                                                                                        Number
                                                                                                      Start-End
                                               OsscUy
                                              S-JT
                                                                                       Readings ranged from
                                       to
                          opacity
                                                                                       The source VMS/was not  in compliance, with mm
                                                                                       the time evaluation was race.

-------
OBSERVATION RECORD
                   PAGE 7^ OF/^
LCI'- ''ill   r:
TEST KVElTr
C/Jt   ^xf Jx
OBSERVES 	
TYPE F/'ClLitY  xT7>
POl.'lT CF £.'-!lSSTi^r
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       OBSERVATION RECORD
     (Continued) '
                                                                                                                                    PASS	OF	
                                                 COWA'JY
                                                 LOCATION
                                                 TEST Uir.S
                                                 DATE     .
               03SCRVE3 	
               TYPE FACILITY
               POltlT OF CKISSIG.'S"
Mr.






















,







Kin.
30
31
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0

-------
Plant
Run No.
Location

Date   ^
Operator
                                         p;     LA      :D i

                                     VERY IMPORTANT -  FILL IN ALL BLANKS

                                     Read and record at  the start of
                                     each test point.
                                     Time:  Start Time_

                                           End Tiu-e
                                                                         Aaibient Temp  *F_

                                                                         Bar. Press. "HB   3 ^ . ~1 0

                                                                         Assuned Moisture 7.  O
                                                                          Probe Tip Dla. In.  0 • 3  I
                                                                           Pltot Tube No.
Sample Box No.

Meter Box No._

Meter A H	

C Factor	
                                                                           Probe Lenp.ch/type

                                                                           Filter No. *-[
  Point
 L
        Clock
              Dry Gas
              Meter, CF
              ^0*4.0 1
Pitot
in.  H.O
  AP
Orifice AH
  in H20
                                  Desired  Actual
                                          1.15
                                          1
                                                 Dry Gas Temp.
                                                     "F
                                                 Outlet  Inlet
Punp
Vacuun
In.  Hg
                                                                 3
Inpingcr
  Ten?.
   "F
Tero
 "F
Probe
Tcrp.
 °F
Stack.
Terp.
 °F
                                                                                            H6
Stack
Te-1?.
 •F
("F-^60)
 r-s
          lo
                                                            3L
                                                                               751
        II
                                          I- IS
                                                                                           153
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                         o
                                    00
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                                                      l  :  'a a.
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                                                           55
                           0
                                                   so
                                                                                            157
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                                                                                              SM
                                     '00
                                                                                            (55
               ft^-fl
                                          )• IS
                                                                                      ^ a
                                   i.«<>
 Conr.cn ts :

-------
                                                                 bneet
                                                                                  of
  Point
Clock
Dry Gas
Meter, CF
Pitot
in.  H-O
Orifice AH
  in  H20
                                Desired
                                 Actual
Dry Gas Temp.
    °F
                                  Outlet
                               Inlet
Pump
Vacuum
In. HE
Icpinger
  Tenp.
   °F
Oven
Te.ro ,
   "
                                                                                   Probe
Stack
Tercp .
   '
Stack
Teirp.
 °F
                                 l-lo
                                 l-lo
                                                                           I7S
 b-i
                0 -10
                   I. lo
                    OO
                          \-60
                           \. -co
                                  1  00
                                 1 -00
                                                                                 Lrll
 D-M
             O
                   1 • O O
                   06
                                                         167
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                         1-oS
                                        0-%-S
                                                              is
         id
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                                                           l
 C  1
                          1  lei
                                                                                  top
 C-
                                  \-\0
                                                 3
                                                     31S
 C
                         1  \5
                            MS
  C-2
         li.
Comments:

3/16/77
                                 MS
                                  M5
                                                               3.V-
                                                                  1 6
                                   O O
                                                si
                                                        11
                                                                  \U
                          \. \  0
                            Mo
                                                                   65
                                                                               -( e-  ^ 6 ')   i s1 /
                                                                6,26,

-------
                                                                         Sheet ?x  of
 Point
Clock
Dry Gas
Meter, CF
                     5
                       Pitot
                       in. H00
                         AP fc
Orifice AH
  in H00
                                Desired
                                 Actual
                                 1  Do
Dry Gas Temp.
    °F
                                  Outlet
                                                       Inlet
Pump
Vacuum
In.  Hg
Iipinger
  Temp.
   °F
Oven
Tenp
                                                                             s
                                                                34H
Probe
Tenp .
                                                                                     SF
                                                                                         Stack
                                                                                         Tena.
Stack
Terp.
 fW.
 I
S'MI
                                ) .
                                   30
                                  1 Jo
                       <**
                      IS
                                                    0
                         o-lo
                          l-lo
                                                         IS
 IV
 fo
  U
-o
  A-  \
Consents:

3/16/77

-------
                          SAMPLE  CLCAf.'UP SI I LET
Plant: ^^^-^^ . -ifc>
Address: xr— ^^ "•»"'•<-.., 	 *•
Station NoT: CYC? ''
Run No.: ^-^
BaroneLric Pressure: 3. F,'*>r>





Date: '//s>J->'?
Operators: ^ '
*
Ambient Temperature: s' ','"
Sample Box Number: /

Impinger 1
Final Volume ^,
Initial Volume xo
Impinqer 2
Final Volume /a?
Initial Volume /oo
Volume collected _ /'
Impinger 3 \
Final Volume\
Initial VolumX
Volume collected
Impinqer
Final Volume - ^
Initial Volume d'^
Volume collected o
Impiniier
Final weight *?&? &
Initial v/eight ^/L-^CJ
Height collected ;~> <^>
Total Volume Collected / ->j "r?*"/r
of

/" «-^"
of r^--.- -r^^-
Weight
Tare Weight Collected
gm gm
gm gm
Cleanup performed  by
on

-------
Cl
                      ^
COMPAKY^^y-^-Z*-.
LOCATION	
TEST NUMBER
DATE
RECORD Or VISUAL DETOSUMTIOK  OF OPACITY                    FAG"  / cf /
                                       HOURS OF OBSERVATION   x£
                                      o   .-
              TYPE FACILITY x^/
               COHTROL  DEVICE  .,/-
                                       OBSERVER	
                                       OBSERVER CERTIFICATION DATE	
                                       OBSERVER AFFILIATIC.'I  L',~/*'r9.~1
                                       POINT OF EHISS
                                                                             HEIGHT OF DISCl'ARGi FOII1T
o
Z
O
r
>
s
CLOCK TIME
OBSERVER LOCATION
  Distance to Discharga
  Direction from Discharge
  Height of Observation Point
BACKGROUND DESCRIPTION
LEATHER CONDITIONS
  Kind Direction
  Vlind Speed
  Ambient Temperature
SKY  CONDITIONS (clear,
  overcast, % clouds, etc.)
PLL'Ks DESCRIPTION
  Color
  Distance Visible
 OTliCH
Initial
Y*.S>
^
t^fl
'•£.•.?"/
2
y-f /}
7?.-'
r£^
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Final











I
1
1
SlTCttRY OF AVERAGE OPACITY
Set
Mur.be r










leadings r
'he sourc!
the time (
Tlr-n
Start—End










Cssclty
_....^, . , .

' 1
I








•anged fro.n to % cp;c
j VMS/was not in ccr.pl io^cc wit
jvdlu'alion VMS race,



	



iiy
h ..&t

-------
Plant
                                                :uu     ELD

                                      VERY IMPORTANT - FILL IN ALL BLANKS
Run No.
                             Read and record at the start of
                             each test point.
                                                                             Anbient Temp  °

                                                                             Bar. Press. "H
Location ?lr~^/> F . /T?

Bate   V/V ~/~ ~'' //'
                                    C»-i~t-  T-f mn
                                             End Time
                                                  )6
                                                                             Assumed Moisture 7.   O
                                                                                               "i ~7 ' <~
                                                                             Prnhe Tip Dia.  In.«- * - " / -*

                                                                             Pitot Tube No.    f~ /
Sample Box No.

Keter Box No._

Keter A H	

C Factor
                  {_
                                                                     Probe Lenp.th/type

                                                                     Filter No.
             /./?
                                              */.  ^
  Point
 //  f
Clock
          12
               Dry Gas
                ieter, CF
                 .<»V 7 ^
Pitot
in.  H,0
  A?
                          o -
                 o. SS
Orifice fill
  in H20
                                   Desired  Actual
                          I-3S
                            106'
                                    1 .
                                    6 Ij
                                             -06.
                                   r.
                                                   Dry Gas  Te:rp.
                                                       °F
                                          Outlet   Inlet
Pum|/
Vacuun
In. Hg
                                                                     •«>
                                                                  i -o
Impinge r
  Tenp.
   "F
                                                                  "*>
                                                                    •
Oven
Teirp.
 "F
                                                        /; (,
Tcnp .
 °F
                                                                                        =?-;/.,
                                                                                P
Terp.
 "F
                                                                                               15S
                                                                     K-i
                                                                                       U
                                                                                                     Stack
                                                                                                 ,   L-^C-
 /_'
                                       IS   ;. K
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                                    135    -3S
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                                                                                             (.-/Iff
                                                                               c? <"
                                                                                                     LoL
                                                                                               /Vl
                                                                                                      GtT-
     -/
 (fonncnco ;

-------
                                                                  Sheet
                                                                                    of
  Point
Clock
Dry Gas
Meter, <
Pitot
in.  H.,0
  AP -
Orifice AH
  in H20
                                  Desired
                                 Actual
                                                 Dry Gas Temp.
                        Outlet
              Inlet
Pump
Vacuum
In.  Hg
                                             Inpinger
                                               Ten?.
                                      Oven
                                      Tenp
Probe
Temp.
 °F
Stack
Tenn =
 °F
 e- 1
                            6-7
                          1-0
 S
           lo
l-\o
                                    t  I
                                       l.c
                                                            2 SI
 c-d
                                                       "S-6
                                          ;.*
                                                       ? 0
                                                      .76 r
          IU
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           , )G
        0
  -9V
                                         c
                                    i o
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 N
                 /-/o
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                                       3
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                                                       -?.£•:?
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                                    60  |
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0
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                          < cS
               % 1.
/• lo
 O-V
           • h
                                                               J
         /-f
Comments:

3/16/77
                          0
                                                                J

-------
                                                                               Sheet S   of
  Point
Clock
Dry Gas
Meter, CF
Pitot
in.  H?0
  AP "
Orifice AH
  in H90
                                   Desired
                                   Actual
                                                    Dry Gas Temp.
                                    Outlet
                                  Inlet
Pump
Vacuum
In. Hg
Impinger
  Tenn .
     "
  .  r«

£••' '5
 Oven
 leap.
  °F
Probe
Tesp.
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3/16/77
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-------
                          SAMPLE  CLEANUP SHEET
Plant:
                                            Da Le :
Address: 7?...; ..> ^'L^-.^.-
Station No. : ' c'-^c • '
Run No. : *?3
Baromc-tric Pressure: jj-.'^c
Operators: '
i
Ambient Temperature: _j> *<•/--
Sample Box Number: /
i
 Impinqer  1
     Fi nal Volume	
     Initial Volume	
     Volume collected
Impincjer 2
     Final Volume	
     Initial Volume	
     Volume collected
Impinqer 3
     Final Volume	
     Initial Volume	
     Volume collected
Impincier
                          /so
                            r
                  _ml of
                  jnl
                  ml
                                 _ml of
                                 _ml
                                 ml
                                 jnl of_
                                 jnl
                                 ml
     Final Vtnume	
     Initial VoSoime
     Volume col levied

Impinqer

     Final weight_
     Weight collected
Total Volume Collected_

Filters
No.
Final I/eight
                 jnl of_
                 jnl
                  ml
                                    Of
     Initial weight     /: £ :. o  qm
                              c._gm
                                 ml
                                      Tare Height
                                                       Weight
                                                       Collected
            gm
                                                gm
                                                                gm
            gm
                                                gm
                                                                gm
Cleanup performed by
                      /LtL^z
                                                   /

-------
n
o
                                                    RECOR3 OF yiStW, DETERMINATION Of OPACITY
                                                                                            HOURS 0? OBSERVATION
               LOCATION
               TEST NUMBER
               DATE
TYPE FAC1LITY__
CO.'HROL DEVICE
                                                                             OBSERVER
                                                                             03SERVEP. CEB.TIFICATIO.X LVJE
                                                                             OBSERVER AFF ILIATIC!.' £S ^
                                                                             POINT OF EMISSIONS  X^-X'f
                                                                                            HEIGHT OF DISCIWRG; FO'l.'iT
O

I
\
CLOCK TIME
OBSERVER LOCATION
  Distance to Discharge
  Direction from Dfscfiarge
  Hclfjht of Observation Point
BACKGROUND DESCRIPTION
LEATHER CONDITIONS
  Wind Direction
  VMnd Speed
  Anblcnt Temperature
SKY COIJOITIONS (clear,
  overcast, % clouds, ctc.y
PLUME DESCRIPTION
  Color
  Distance Visible
 OTHER IKFOOTIOII
                                             Initial
                                                           Final
                                                                                          OF AVERAGE OPACITY
Set
Number










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Start— End










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Sun










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_
                                                                                       Readings ranged from
                                                                                                   to
                                                                                       The  source VMS/was rot In ccnpUs.ncs with
                                                                                       the  time  evaluation VMS race.

-------
AST  V'".:
                           OBSERVATION RECCttD        PAGE /  .OF/
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