EPA-650/1-74-008




April   1974
Environmental  Health  Effects  Research  Series



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                                      EPA-650/1-74-008
            A  LITERATURE  SEARCH
     AND  ANALYSIS  OF  INFORMATION
REGARDING  SOURCES, USES,  PRODUCTION,
CONSUMPTION,  REPORTED  MEDICAL  CASES,
      AND  TOXICOLOGY OF  PLATINUM
               AND PALLADIUM
                        by
          R. A. Mayer, W. L. Prehn, Jr., and D. E. Johnson
                 Southwest Research Institute
                    8500 Culebra Road
                    P.O. Box 28510
                 San Antonio, Texas 78284
                  Contract No. 68-02-1274
                 Program Element No. 1AA002
                    ROAP No. 26AAE
            EPA Project Officer: Douglas L. Worf, Ph.D.
                     ^
                 Human Studies Laboratory
             National Environmental Research Center
            Research Triangle Park, North Carolina 27711
                     Prepared for

             OFFICE OF RESEARCH AND DEVELOPMENT
            U.S. ENVIRONMENTAL PROTECTION AGENCY
                 WASHINGTON, D.C. 20460

                      April 1974

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This report has been reviewed by the Environmental Protection Agency
and approved for publication.  Approval does not signify that the
contents necessarily reflect the views and policies of tho Agency,
nor does mention of trade names or commercial products constitute
endorsement or recommendation for use.
                                  11

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                    EXECUTIVE  SUMMARY
      An  intensive search  of the literature  provides the basis  For the
 following conclusions concerning platinum and palladium

      Supply and Demand.  An average of 3.7 million  troy ounces of
 platinum  and palladium were produced in  the world in the four-year
 1969-1972 period. The United States consumed about a third of this. The
 proved world reserves amount to some 394 million troy ounces, with con-
 siderable promise of increasing these reserves through new explorations
 Half of the proved reserves are in the Republic of South Africa and 45 per-
 cent in the Soviet Union. Projected 1980 and 1990 world demands are 6 2
 and  8.5 million troy ounces per year, respectively The introduction of a
 new demand for  automotive emission control catalyst purposes (18 per-
 cent of the total  in 1980 and IS percent in 1990) is not expected to upset
 the world supply/demand situation

      This  assumption  does not  consider  the possibility  that  other
 countries  may adopt the catalytic muffler for their use  If  this occurs,
 there will  be a  larger  demand  on  platinum and  palladium resources
 Although  it appears  that the projected demands on  platinum and palla-
 dium reserves can be met with known sources, it should be  pointed out
 that the  United  States  is almost completely  dependent upon  foreign
sources. The  United  States currently consumes nearly 40 percent of the
world production, but it produces less than 1 percent

      Health Hazards. No data exist by  which an estimate can be made of
transfer of platinum and palladium  to the  environment  Investigations
show that only the salts of platinum present human health hazards Indus-
trial  exposure to  these is limited to the mining and refining of platinum
ores  and the preparation  of catalysis  for the  chemical  and petroleum
refining industries
                                111

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                             TABLE OF CONTENTS

                                                                            Page

EXECUTIVE SUMMARY	       m

NARRATIVE SUMMARY    	      .         ...       1

     Present World Supply and Demand   	     .    ....    .     .  .     1
     Future World Demand	     2
     Environmental Considerations  .  .     .  .    .  .     ....       .    .   .       2

BIBLIOGRAPHY	       	      .          3

APPENDIX A	           	     A-l

APPENDIX B .  .       	       	     B-l
                                       IV

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          NARRATIVE SUMMARY

Present World Supply and Demand

     Based  on reasonably reliable  estimates from
foreign sources, world production  of platinum  and
palladium is estimated to  have increased from a total
of 3.12 million troy ounces  in l%9  to 3 90 million
troy ounces in 1972,  a four-year increase of 25 per-
cent World production by source is  summarized in
the table below
        WORLD PRODUCTION OF PLATINUM
                 & PALLADIUM

             Average Annual. 1969-1972
            (Thousands ol Troy Ounces)

Source
f.mada
Colombia
l.lhiopiu
Finland
Japan
Philippines
Republic of South Africa
USSR
United Stales
TOTAL
1969-1972 Average
Platinum
188
26
03
02
3
06
909
665
9
1801
Palladium
187

-
03
5
1
321
1339
13
1866
Total
375
26
03
05
8
1 6
1230
2004
22
3667
Sources: Minerals Yearbook and Engineering and
Mining Journal
      Half of world platinum and one-sixth of world
 palladium  production comes from  the  Union  of
 South Africa  One-third  of platinum and over  two-
 thirds of palladium production is from the U.S.S.R.
 Canada produces about ten percent of both platinum
 and palladium, while the United States  produces less
 than one percent of each  South Africa,  U.S S R., and
 Canada combined produce 98 percent of the world's
 platinum and palladium.

      Consumption of the  two  metals  in  1971  is
 estimated to have been 3.7 million troy ounces, with
 the United  States using 37 percent of the total,  as
 shown in the following table Japan used 20 percent,
 Russia 16 percent, and West Germany 12 percent All
 other  consumption totaled  15 percent  of the world
 total

      Sales  to United States users in  the five-year
 1967-1971 period averaged slightly less than 1 3 mil-
 lion troy ounces per year. Sales to specific industrial
 categories are shown in the following table
     WORLD CONSUMPTION OF PLATINUM
                & PALLADIUM

                     1971
           (Thousands of Troy Ounces)
Nation
United Stales
Japan
USSR
West Germany
France
Italy
Canada
United Kingdom
Netherlands
Sweden
Switzerland
TOTAL
Consumption
1376
758
589
451
313
74
68
49
33
17
12
3740
Source: Minerals Yearbook.
                                                            PLATINUM AND PALLADIUM SALES TO
                                                                      U.S. INDUSTRY

                                                                     1967-1971 Averages
                                                              (Thousands ol Troy Ounces per Year)

Industry Category

Electrical
Chemical
Petroleum Refining
Dental and Medical
Glass
Jewelry and Decorative
Miscellaneous
TOTAL
l-ive-Ycar Average
Annual Sales
Platinum
97
155
184
23
49
31
29
568
Palladium
389
208
9
56
5
19
35
721
Total
486
363
193
79
54
50
64
1289
Source: Minerals Yearbook.
     Some  38 percent of total  sales were to the
electrical industry, the palladium (over half) being
used chiefly in telephonic equipment  and the plati-
num being used chiefly for switch gear manufacture
The  chemical  industry purchased 28 percent of the
total during the  1967-1971  period, chiefly for sul-
furic and nitric  acid manufacture  The petroleum
refining industry  purchased 15 percent of the total
mostly  platinum, for use in  the  refining processes
These three  industry  groups purchased 81 percent of
the platinum and palladium sales during the five-year
period   World  reserves  of platinum and palladium
were estimated in the 1970 Mineral Facts and Prob-
lems to be about 394 million troy  ounces  These
reserves are  equivalent to 105 years of supply at the

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1971 rate of 3.7 million troy ounces per year  Proved
reserve figures are given in the table below. There are
extensive exploration  and  investigation of other
prospective  producing areas which are not included in
these totals.

    WORLD RESERVES PLATINUM & PALLADIUM

                  1970 Lstinutcs
            (Thousands of Troy Ounces)
      ESTIMATED FUTURE WORLD DEMAND
            PLATINUM & PALLADIUM

        (Thousands of Troy Ounces per Year)

Nation
Republic of South Africa
USSR
Canada
Colombia
United States
TOTAL
Reserves
Platinum
142,400
60,000
6,940
5,000
950
215,290
Palladium
50,200
120,000
6,860
-
1,960
179,020
Total
192,600
1 80 000
13,800
5,000
2,910
394,310
Source: Mineral Facts and Problems, 1970
     Nearly  half of total estimated reserves arc in
South  Africa, with another 45 percent in the Soviet
Union   Canada, Columbia,  and the  United States
account for only 5 5 percent

Future World Demand

     A series of estimates has been made for future
demand for  platinum and palladium on the part of
major consuming industries, both in the United States
and elsewhere. High, low, and median estimates were
made for consumption in 1980 and  1990 The follow-
ing table gives the median value of projected demands
and reflects the impact of new demands for automotive
exhaust emissions control catalysts. The 1971 sales to
industry figure is included for comparison This figure
is some 5 percent lower than the U S consumption fig-
ure shown earlier, reflecting transfers to small coun-
tries, chiefly for trading and speculation

     Catalyst use  for automotive emissions control,
40 percent of the United States demand in  1980 and
37 percent  in  1990,  is not  expected to impose a
supply hardship in the foreseeable future  The addi-
tional  needs amount to 18 percent of total world
demand in  1980 and 15 percent in  1990  Producer
indications are   that  production  can be increased as
the  demand  increases. The  1970 proved reserves of
394  million  troy ounces are equivalent to 46 years of
supply at the estimated 1990  annual consumption
rate  of 8.5 million troy ounces


United States base platinum
automotive catalysts
total platinum
base palladium
automotive catalysts
total palladium
total base
total automotive
Total
Rest of world platinum
palladium
Total
Grand total platinum
palladium
Total
Total Demand
1971
541
-
541
760
-
760
1301
-
1301
1283
1163
2446
1824
1923
3747
1980
734
774
1508
898
332
1230
1632
1106
2738
1826
1655
3481
3334
2885
6219
1990
1044
866
1910
1095
371
1466
2139
1237
3376
2703
2450
5153
4613
3916
8529
Source: Mineral Facts & Problems. 1970, A Look at
Business in 1990 (a Summary of the White Mouse Con-
ference on the Industrial World Ahead. February 7-9,
1972), and SwRI
Environmental Considerations

     Losses to the Environment Essentially, no data
were found  in  published souices covering industrial
rates of  transfer of  platinum  and  palladium to the
environment  If such transfer  is labeled  as  "unac-
countable losses" versus attrition (that known loss
from catalyst poisoning, handling and  the like), then
some speculation may be made as to (1) the probable
sources of unaccountable losses, and  (2) some feel for
the relative importance of these

     Most platinum  or  palladium is used by industry
in two forms  (l)as a metal, pure or  in alloy, fabri-
cated, melted  and  cast,  or used directly, or (2)as a
platinum or palladium compound either  in solution
or not and applied,  as for catalyst  preparation, to a
carrier or matrix

     While  process losses certainly  occur among the
industries using metallic  platinum and  palladium,
there should be little or no loss entering the environ-
ment in the  sense of a potential health hazard These
industries include  the electrical  industry  where
precious metals are used for switch contacts, dental

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work, the glass industry where  precious metal spin-
eietles arc used in the production of glass fibers, and
the jewelry and decorative industries

      In the chemical and petroleum refining indus-
tries,  there is probably some transfer of platinum or
palladium to the product. However,  the most prob-
able site of potential loss of platinum and palladium
to the environment, in one form or another in the
chemical  and petroleum refining industries, is at the
point  of  preparation of catalysis  rather than at the
chemical  plant itself As .in example, mineral carriers
arc impregnated  with a  platinum  compound such as
chloroplatmate in   manufacturing the  catalyst lor
producing nitric acid The catalyst  is  then further
processed  in order to rendei the platinum elemental
in foim  In  these processes there are opportunities
for spillage,  vapor eniraimnent.  or other mechanisms
for loss  Of the  354 thousand troy  ounces of plati-
num 
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Freedman,  S.O, Kruper, J ,  "Respiratory Allergy
Caused by Platinum Salts," J. Allerg. 42 233-7, 1968

Gerrard, M . "Toxicity and Biological Effects of Plati-
num,"  Report ORNL-TEP/TIRC-72-75,  Oak  Ridge
National Laboratory, Tenn , November 1972

Gertner. H B , "Toxicity of Palladium, Platinum, and
Their  Compounds-An  Annotated  Bibliography,"
Report  ORNL-TIRC-73-19,   Oak Ridge  National
Laboratory, Tenn , June 1973.

Hunter, D, "Toxicology of Some Metals and Their
Compounds  Used  in  Industry." Brit   Mcd   Bull.
7 5-15. I950.CA 45 8657i

Hunter, D.. Hilton,  R,  Perry,  K M.A,  "Asthma
Caused by the Complex Salts  of Platinum." Bnt J
Indust  Med 2 92, 1945.

International Directory of Mining and  Mineral Pro-
cessing Operations,  McGraw-Hill  Publications, New
York, 1972

Kusler, D J., "Demand for Platinum to Reduce Pollu-
tion  from Automobile Exhausts," U S   Department
of the Interior,  Bureau  of Mines Information Cir-
cular-8565. Washington, D.C , January 1973

Levene, G M . "Platinum Sensitivity," Br J Derma-
tol 85(6)  590-93, 1971

Marshall,  J ,  "Asthma  and  Dermatitis Caused  by
Chloroplalmic Acid," S.Afncan Med Joum  26(1)
8-9. 1952.

Merck  Index 7th  ed., Merck  & Co., Inc. Railway,
NJ ,1960

Milne,  J  E., "A  Case of Platmosis," Med. J.  Ami
1 1194-5,1970
Parrott, J L, Samdelle,  A., Ruff,  F., "Platinum and
Platmosis  Histamme Release by Some Platinum Salts
and  Platinum  Allergy,"  Presse  Med  (Pans)
75(2817) 20-30, 1967

Parrott,  J L., Saindelle, A.,  Tazi.  T ,  "Histamme
Liberation by Sodium  Chloroplatmate," J. Physiol,
(Pans) 55 314-5, 1963(Fr).

Pickering,  C.A ,  "Inhalation  Tests  with  Chemical
Allergens  Complex Salts of Platinum " Proc R Soc
Med., 65 2724,  1972

Platinum Metals  Review, Quarterly   Publication.
Johnson, Matthey & Co  , Ltd   London, England

Rosenberg, B . Vancamp, L, Trosko. J B , Mansour.
V .  "Platinum Compounds  A New Class of Potent
Antitumor Agents,"' Nature 222(5191) 385-6. 1969

Samdelle,  A .  Ruff.  F..  "Histamme  Release  by
Sodium  Chloroplalinate." Bnt   J  Pharmacol.
35 313-21. 1969, BA 51  56709

Sax, N I., (Ed). Dangerous Properties of Industrial
Metals, 3rd ed . pp 1031-2, Van  Nostrand Remhold
Co , New York, N Y., 1968

Schroeder, H H.  Mitchener, M,  "Scandium, Chro-
mium,  Gallium,  Yttrium,  Rhodium,  Palladium,
Indium  in Mice  Effects on Growth and Life Span,"
J Nutr ,181  1431-7, October  1971

Schwartz. L, Tulipan, L., Peck, S  M., (Eds ), Occupa-
tional Diseases of the Skin, 2nd ed , Lea & Febiger
Philadelphia, Pa  , 1947.

Spikes, J D,  Hodgson,  C.F , "Enzyme Inhibition by
Palladium Chloride," Bwchem Biophys  Res Com-
mun 35 420-2,  1969
National Materials Advisory Board (NAS-NAE), "Sub-
stitute Catalysts for Platinum in Automobile Emission
Control  Devices and Petroleum  Refining,"- Report
NMAB-297, Washington, D C , March 1973

Oil and Gas Journal, Petroleum Publishing Co . Tulsa

Parrott,  J L,  Herbert,  R . Saindelle. A , Ruff.  F ,
"Platinum and Platmosis  Allergy and Histamme Re-
lease  Due to Some  Platinum Salts," Arch.  Environ
Health (Chicago) \ 9 685-91,1969. BA 51  45039
 Standard & Poor's Register of Corporations, Directors
 and  Executives, Standard & Poor's Corporation, New
 York, 1974

 Suskmd, D.A , "Platinum Group-A Bonanza in the
 Automotive  Industry9" Engineering and Mining
 Journal, McGraw-Hill Publications, New York. March
 1973.

 The Watt Street Journal Dow Jones & Co , New York.
 NY

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 Thomas Register of American Manufacturers Thomas
 Publishing Company, New York, 1973

 U.S Department  of Commerce, Statistical Abstract
 of the United States, Bureau of the Census, Washing-
 ton, D.C., 1973.

 U.S. Department of Commerce, U.S. Industrial Out-
 look 1974 with Projections to 1980 Bureau of Com-
 petitive Assessment and Business Policy, Washington,
 D.C.,1974.

 U S. Department of the Interior, Mineral Facts and
Problems, Bureau of Mines Bulletin 650, Washington,
 D.C., 1970.
U.S. Department of the Interior, Minerals Yearbook,
Volumes I, II and III, 1970, Vol I., 1971, Bureau of
Mines, Washington, D.C.

U.S.  Department of  Transportation, Economic
Impact of Mass Production of Alternative Low Emis-
sions Automotive Power Systems, Office of the Secre-
tary, Washington, D.C., March 1973

Van Arsdell, P.M., "Toxicity of Chemicals in Electro-
plating," Metal Finishing 45(S)'55-60, 67, (9) 79-83,
(10)75-81, 1947.

Wood, J.M., "Biological Cycles for Toxic Elements in
the Environment,"Science. 183  1049-1052,1974

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                               APPENDIX A.  LITERATURE SEARCH

 1.      Introduction

        The platinum group metals are often referred to as platinoids and are comprised of platinum.
 palladium,  iridium,  osmium,  rhodium, and ruthenium.  Canada, the Republic of South Africa, and
 the U. S. S. R. are the main world suppliers.  Small quantities of platinoids are derived from
 Colombia, Ethiopia,  Finland,  Japan, the Philippines,  and the U.S.

        Platinoids are found in nature (a) associated with nickel-copper minerals that occur in ultra-
 basic rocks, dunite and norite, and (b) in placer deposits.  Nearly all of the Canadian production and
 most of the U. S. S. R. production  are a byproduct of nickel-copper refining. The South Africa produc-
 tion comes  from mines worked principally for the platinoids with nickel and copper recovered as
 coproducts  and gold and chromium as byproducts.  Ethiopia and Colombia derive their production
 from placer deposits, whereas Finland, Japan,  and the  Philippines produce small amounts of plati-
 noids as byproducts of copper refining.  Minute amounts are also produced in  Papua New Guinea.
 The U. S. output comes either from placer mining or is  derived in the refining of gold and copper.
 Fairly high platinum values were discovered during test drillings in western Australia and in north
 Aukland,  New Zealand,  but further sampling will determine the commercial potential of these finds.
 Prospecting in Southern Rhodesia has also uncovered significant occurrences.

        In addition to  primary platinoid production, the metal group's high costs have stimulated a
 substantial  effort for secondary recovery from all forms of  scrap and used equipment, wherever
 economically feasible.

        The estimated world production of platinoids is shown in Table A-l.

                  Table A-l.   Estimated World  Production  of Platinum Group Metals
                                          (million troy oz)

                                                                                 1972
                                  1969            1970           1971            (Prelim.)

             Platinum            1.48            1.98           1.82              1.92
             Palladium           1.64            1.92           1.92              1.98
             Other               0.29            0.35           0.34              0. 35
               Total              3.41            4.25           4.08              4.25

             Source:  E/MJ, March 1973

        These data indicate that platinum and palladium are by far the most abundant and the most
 important elements of this  group.  Metals of the platinum  group are measured and traded in terms of
troy ounces in the British system of weights.  In the metric system, measurements are in kilograms
 (1 kg equals 32. 15 troy ounces).  Platinum group metals are commercially available in grades ranging
 from 99. 8 to 99. 999 percent purity.   Platinum and palladium are available in the form of sponge,
 single crystals, powder, wire, sheet, foil,  and rods.  Platinum above 99.7 percent is normally con-
 sidered as commercial grade.  According to Federal regulations, an article of trade may be marked
platinum if it contains 98. 5 percent platinum-group metals with a minimum of 93. 5 percent platinum.

        Most platinoids are recovered as byproducts of the milling,  smelting,  and refining of nickel
and copper materials.  In the Canadian Sudbury district, sulfide ore is processed by magnetic and
flotation techniques to yield concentrates of copper and nickel sulfates.   The nickel flotation concen-
trate is roasted with  a flux and melted into a matte which is cast into anodes for electrolytic refining
from which the precious metal  concentrate is  recovered.  The platinum, palladium, and gold in the
 concentrate are dissolved with  aqua  regia,  leaving a residue containing  the remaining four platinoids.
After the  gold has been removed from the solution with ferrous sulfate,  platinum is precipitated with
ammonium chloride.   Palladium may be precipitated as  a  chloride by the addition of excess  ammonia
and hydrogen chloride.  The chloride of platinum and palladium are separately reduced to sponge
metal which can be compacted and melted to massive metal.  Byproduct platinoids from gold or
copper ores are sometimes refined by electrolysis and by chemical means.
                                               A-l

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        Milling and beneficiation of the  platinum-bearing nickel ores from South Africa consist of
 gravity concentiall.in, flotation,  and smelting which produces a high-grade table concentrate called
 "metallics" for direct chemical refining and a nickel-copper matte for smelting and refining.  The
 process of extraction consists essentially of enriching the nickel-copper matte to about 65 percent
 platinum metals and then treating the enriched product with acids to separate the  individual plati-
 noids, followed by final refining.

        The mining of crude platinum in placer deposits furnishes a small pait of total production.
 The nrn.ning and processing techniques for recovering crude platinum from placers are similar to
 those used for  recovering gold.

        The industrial applications for platinum and palladium are diverse.  Platinum-group metals
 find application in the U.S.  in the chemical, petroleum,  glass, electrical, dental and medical, and
 jewelry and decorative industries.

        Platinum-group metal producers, in general,  experienced overproduction and idle capacity
 which lasted from 1970 to 1972.  Renewed growth is expected,  particularly for platinum and palla-
 dium to be used in automobile emission control systems scheduled to be installed from 1975 on.
 In addition to obtaining the required performance characteristics of these automotive catalytic con-
 verters,  lead content in gasoline must  be reduced and sulphur and phosphorus content must be limited
 to avoid rendering the platinum catalysts ineffective.  It has been estimated  that each car will  require
 an average of 0. 1 oz ol platinum-group metals, including 30-35 percent palladium,  with platinum
 comprising the balance.  The relatively high costs of platinum and palladium have initiated intensive
 research into the use of suitable  substitute catalysts.  Thus, while the growth of supply is resuming
 at a steady pace,  the  utilization of increased output is precariously dependent on the development
 and final  timing in the auto emission control area on a worldwide basis.

 2.     Platinum and Palladium Sources

       The platinoid industry in the free world is centered about two  major  mining companies and
 two affiliated refining and fabricating companies. The International Nickel Co. of Canada,  Ltd.
 (INCO) produces refined  platinum-group metals as byproducts of its nickel-copper ore mining and
 refining operations in Canada,  and accounts for about one-third of the free world output of these
 metals.

       Rustcnburg Platinum Mines, Ltd. , Republic of South Africa, produces platinum-group metals
 from ores mined chiefly  for platinum and contributes about two-thirds of the free world output of
 platinoids.

       The refining and fabricating  companu'S are Engclhardt Industries, Inc., Newark,  N. J.
 affiliated  with INCO and Johnson,  Matt hey & Co., Ltd. in Great Britain and their worldwide sub-
 sidiaries, affiliated with  Rustenburg.

       In addition to  these major companies in mining,  as well as refining and fabricating, a
 number of smaller organizations are engaged  in these same activities in various countries as will
 be shown  below; the level of their  activities depends to a great  extent on the  woild demand and supply.

       A  third major source of platinum and palladium in the total world market is the U. S. S. R.
 Little information is  available on her industry pattern.

       Canada.  The Sudbury region of Ont. and the Thompson-Wabowden area of Man. aic the
 major  sources of Canadian production,  derived in a residue at  nickel refineries.  A small amount
of platinum metals is  recovered from ores  at Shebandowan,  Ont. by INCO, in Quc.  by Rcnxy Mines
 Ltd. ,  and near  the Ont. -Man. boundary by  Consolidated  Canadian Faraday Ltd. and Dumbarton
Mines, Ltd.

       Canadian production  in  1972 was 399, 000 troy  ouncus compared with  475, 169 ounces in
 1971.   Cutting  back in nickel-copper production by INCO during this time period is the principal
factor  for the decline in Canadian  platinoid  production.

       In Ont. , INCO as  the  Largest pioduccr,  operated 13 nickel-copper mines, four concentrators,
and two nickel-copper smelters near Sudhury,  Ont. in 1972. A new nickel refinery was also being
                                                 A-2

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 tuned up,  where platinoid-bearing residues will be recovered.  The Comston Smelter and Totten and
 Crean Hill mines were temporarily closed,and production was reduced at several other operations
 in early 197Z.  Development work is continuing at INCO's Levack West mine scheduled  for produc-
 tion in 1975.  In Ont., INCO operated a nickel refinery at Port Colborne and started mining the
 Shebandowan deposits.

        Falconbridge Nickel Mines, Ltd. operated eight nickel-copper mines, four concentrators,
 and one smelter in the Sudbury region in 1972.  Their Longvack South mine  was temporarily closed.
 Consolidated Canadian Faraday,  Ltd. closed its Werner Lake  mine because ore reserves were
 exhausted.

        In  Que. ,  Renzy Mines,  Ltd. closed its nickel mine and  concentrator when the company's
 smelter contract expired.

        In  Man., INCO operated three mines,  one  concentrator, and a smelter-refinery complex at
 Thompson.  Falconbridge had a normal year of operations at its Manibridge mine and concentrator
 near Wabowden.  Dumbarton Mines, Ltd. which ships nickel-copper concentrate to the  Falconbridge
 smelter, increased ore production from 700 to 1100 tpd.

        INCO's crude platmum-metal-bcaring  residues arc initially concentrated in Canada and then
 shipped to INCO's Metals Refinery at Acton, London,  England  for extraction and refining of the
 platinum metals.   Much of the refined metals  are  returned to Canada and exported to the United
 States for  fabrication and distribution by Engelhard Industries, Inc. Newark, N.J.

        Falconbridge ships nickel-copper matte containing precious metals to its nickel  refinery in
 Kristiansand,  Norway from which platinoid-bearing  residue also goes to Engelhard for further
 refining.

        Republic of South Africa is the free world's largest producer of platinoids.   Rustenburg
 Platinum Mines, Ltd. (RPM) operates three mines,  one smelter and a refinery in the Transvaal
 district.  Rustenburg increased capacity to 1.  1 million ounces of platinoids a year,  but  reduced
 production in  1971 to about 500,000 ounces because of excessive inventory accumulations.  As
 prospects  for a new market are good, the opening  of a new mine and an increase of production to
 1. 3 million ounces a year are planned.

        Impala Platinum Ltd. operates a mine-concentrator-refinery complex near Rustenburg.
 Capacity at the operation is 350,000 ounces of platinum a year, and current  production is at an
 annual  rate of about 300,000 ounces.  Impala has also announced plans to expand its facilities.

        Atok Investments  (Pty. ) Ltd. , producing at Anglovaal and Middle Witwatersrand made its
 first shipment of a platiniferous concentrate and matte from the Middlepunt mine in 1970 and pro-
 duced an estimated 10,000 ounces of platinoids.

        The Lonrho Ltd. -Falconbndge Nickel Mines  Ltd. -South Africa Superior Oil Co.  consortium
 formed Western Platinum Ltd. , which commenced production at its Middlekraal mine near
 Rustenburg in  1971.  The operation has an  annual capacity of 150,000 ounces of plat no ids.   Annual
 capacity may be increased to 430,000 ounces of platinoids by 1974-75, and the company is con-
 sidering construction of a platinum refinery near the  mine.

        Platinum group metal production statistics  are not reported in  South  Africa.  In  1970,  RPM
 accounted for an estimated 83 percent of total  output, and Impala produced most of the remainder.
 An estimate of the platinoid growth potential is shown in Table  A-2.

        U. S. S. R. - The U. S. S. R.  is the second largest producer of platinum-group metals in the
world.

        Most of the production of platinum-group metals comes from nickel-copper ores of the
Norilsk region in northwestern Siberia.  Palladium accounts  for about 60 percent of this production  '
and platinum for 30 percent.  Nickel-copper ores in the Kola Peninsula also  contribute to the output
of these platinoids.  Placer platinum deposits  in the Ural mountains, which at one time  yielded most
of the platinum produced in the U. S. S. R., now contribute only  a small part of the overall output.
Presently,  the U. S. S. R.  is by far the largest producer of palladium, and ranks second after the
                                                A-3

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                Table A-2.  Growth Potential for South African Platinum and Palladium
                                           (1000 troy oz)

                                       197Z            19_73_           1974            1975

         Platinum
           Rustenburg                    550             900           1.300           1.500
           Impala                        345             400             500             650
           Western Platinum              93             125             160             200
           Atok                       	12          	15          	30             200
           Total Platinum              1.000           1.440           1.990           2,550
         Total Palladium                 355             550             700             890

         Source: E/MJ, March 1973

Republic of South Africa in production of platinum.  As official U. S. S. R. output figures are not
available,  it  is estimated that the U. S. S. R. is currently producing platinum group metals at an
annual rate of well over 2. 2  million oz of which over  half is palladium.  The U. S. S. R. is supplying
20 to 25 percent of international exports of platinum and 70 to 75 percent exports  of palladium.

       Colombia is the fourth largest producing country.   Crude platinum is  recovered largely as a
coproduct of  gold; it is marketed in the U. S.  through various dealers and refiners.  Although placer
deposits contain  substantial  reserves of platinum,  some areas are not easily accessible and the
contained platinum may not be  economically recoverable.  Colombia's platinum production has
declined for  several years and currently is about 25,000 oz annually.

       Ethiopia.  Explorations for platinum, copper and petroleum deposits by private industrial
firms and the Ethiopian Geological Society are continuing.   Placer platinum is  retrieved in  the
vicinity of Gambela, Ilubabor Province.

       Finland.  Platinum-group  metals are recovered as byproducts from the copper refinery at
Pori, owned  by  Outokumpu Oy.

       japan.  In 1970, Japan  has produced 47,000 oz of platinoids, mostly platinum and palladium,
as byproduct of  nickel-copper refining,  all of which were exported to Mainland China, the United
States and West Germany.

       The Philippines.  Platinum-group metals,  mostly platinum and palladium, come  from the
nickel-cobalt concentrates of Acoje Mining Co. at Santa Cruz, Zambales Province, Luzon.   The
concentrate,  which is  15 percent nickel-cobalt, assays 1.4 ounces of platinum  and 2.8 ounces of
palladium per ton of concentrate.

       United States of America.   The major part of the U. S.  output is recovered as a byproduct of
copper refining  in Maryland, New Jersey,  Texas, Utah, and Washington.   A small part of domestic
output is recovered from a placer platinum deposit at Goodnews Bay,  Alaska; this output  is pur-
chased by Johnson, Matthey &  Co. and refined by its affiliate, Matthey Bishop, Inc. Malvern, Pa.
U.S.  refiners also process imported materials such as crude platinum from Colombia and  platinum
bearing nickel-copper matte from the Republic of South Africa.  In addition,  the  refiners purchase
platinum- and palladium-bearing scrap, residues, catalysts,  and other platinum-bearing materials.
Secondary recovery  and toll refining are important segments of this industry.  In 1970, the  refinery
production of new metal in the  U.S. was 21, 395 oz, and of secondary metal 349,  126 oz;  the total
industry consumption was 1, 335,467 oz.

Summary of  Sources

Canada,  Qnt. :

       International Nickel Company of Canada, Ltd.
       Ontario Division
       Copper Cliff,  Ont. Canada (705/68
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            Coniston Smelter
            Copper Cliff,  Ont. , Canada
            Manager of Smelters:  J. N. Lilley

            Levack West Mine
            Copper Cliff,  Ont.  Canada
            Area Superintendent:  D. Lennie

            Port Colborne Refinery
            Copper Cliff,  Ont.  Canada
            Manager:  W.  V. Barker
            Employment:  2, 200

            Shebandowan Mine
            Copper Cliff,  Ont.  Canada
            Manager:  G. W. Johnston

            Copper Refinery
            Coppe r Cliff,  Ont., Canada
            Manager:  G. A. Dick

       Falconbridee Nickel Mines.  Ltd.
       Headquarters: P.O. Box 40, Commerce Court West
       Toronto 1, Ont.  Canada (416/863-7000)
       President and Managing Director:  Marsh A.  Cooper
       Employment: 4049  total

       Sudbury Operations  Headquarters;
       Falconbridge, Ont.  Canada (705/693-2761)
       Sudbury Operations  General Manager: G. A. Allen

Canada, Man.

       International Nickel Company of Canada,  Ltd.
       Manitoba Division
       Thompson, Man. Canada (204/677-5211)
       President and General Manager: D. E. Munn
       Employment: 3, 700

       Falconbridge Nickel Mines,  Ltd.
       Mainibridge, Man.  Canada  (204/689-2413)
       General Manager:  W.A.  Case
       Employment: 190

       Dumbarton Mines,   Ltd.
       Headquarters:  1600, 100 Adelaide St. West
       Toronto, Ont. Canada

            Mine
            Maskwa Lake, Man. Canada
            Concentrator  Superintendent:  K. Dixon
            Mine Superintendent:  C. P. Moore

Republic of South Africa

       Rustenburg Platinum Mines,  Ltd.
       Rustenburg and Union Sections
       Consolidated Bldg. , P.O. Box 590
       Johannesburg, Trvl. , S.  Africa
       General Manager:  J. S.  Ritchie
       Manager,  Rustenburg Section: J. C.J. Van Rensburg
       Manager,  Union Section: F. J. Brown
       Employment: 26, 000 total
                                               A-5

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        Impala Platinum Ltd.
        3rd floor, Unicorn House, 70 Marshall St.
        P.O. Box 61386,  Marshalltown
        Johannesburg, Trvl, S. Africa (834-4552)
        Managing Director:  K. A. B. Jackson
        Employment:  10, 000 total

             Batokeng Mine
             P. O. Box 363, Rustenburg, Trvl. , S. Africa
             Telephone:  Rustenburg 2616
             Mine Manager: R. C. Bovell
             Employment:  9, 500

             Refineries
             P.O. Box 222, Springs,  Trvl., S. Africa
             Telephone:  Springs 56-6777
             Chief Engineer: H. W. Read
             Manager Platinum Refinery:  P. A. Reynolds
             Employment:  500

        Western Platinum Ltd.
        Rustenburg, Trvl. ,  S. Africa
New Plants
       Atok Investments (Ptv) Ltd.
       c/o Anglovaal House, 56 Main St. ,  P. O.  Box 62379
       Marshalltown,
       Johannesburg,  Trvl. , S. Africa

New Plants

       Klockner Werke of West Germany
       c/o Rand Mines Limited
       The  Corner House 63,  P.O. Box 62370
       Marshalltown
       Johannesburg,  Trvl. , S. Africa

Exploration

U. S. S. R. All enterprises are owned and run by the communist government.

No detailed data are published outside Russia.

Colombia;

       Cia Miner a Choco  Pacifico. S. A.
       Andagoya, Istmina Choco,  Colombia
       Manager:  Jaime Zapata
       Employment: 438

       Cia Minera de Narino,  S. A.
       Barbacoas, Narino,  Colombia
       Manager:  Carlos AspilLera
       Employment:  192

       International  Mining  Corporation
       280 Park Avenue
       New York, N.Y.  10017(212/983-7500)
       President:  Patrick H.  O'Neill
       (Pato Consolidated Gold Dredging Ltd.
       Aparto Aereo 13-06,  Medellin,  Colombia
       General Manager:  Edward Moseley-Williams
       Employment: 455)
                                               A-6

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The Philippines

       Acoje Mining Co. Inc.

       2283 Pasong Tamo Extension
       Makati Rizal.  Philippines (89-35-61)

             Nickel Project
             Santa Cruz, Zambales, Philippines
             Mine Superintendent:  Elmer B. Gabaldow
             Employment:  130

Finland

       Oytokumpu
       Toolonkatu (Box 10280)
       Helsinki (10) Finland

             Pori Works
             Pori, Finland (Pori 11701)
             Works Manager: Aarne Kapanen
             Employment:  2000

Australia:  Possible future platinum operations.

       Matthey Garret Pty.  Ltd.
       P.O.  Box 165, Kogarah
       New South Wales 2217

New Zealand; Possible future platinum operations.

       Matthey Garret (NZ) Ltd.
       22 Drake St..  P.O. Box 2073. Auckland

United States of America

       Goodnews Bay Mining Co.
       (422 White Bldg. , Seattle.  Wash.  98101)
       Platinum. Alaska 99651
       Vice President and General Manager:  Edward Olson
       Employment:  47

       American Smelting and Refining Company
       Baltimore Plant, Highland and Eastbourne Aves.
       Baltimore, Md.  21224 (301/675-0090)
       Manager: R. H.  Funke, Jr.
       Employment:  1,200

       United States Metals Refining Co.
       440 Middlesex Ave. , Carteret, N. J.  07008
       (201/541-4141)
       General Superintendent:  Robert N.  Brown
       Employment:  1,800

       Phelps Dodge  Refining Corporation
       El Paso Refinery,  P.O. Box 2001
       El Paso, Texas,  79998 (915/772-2701)
       Vice President and Works Manager: M.S. Bell
       Employment:  880
                                               A-7

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 3.
American Smelting and Refining Company
Tacoma Plant, P.O.  Box 1677
Tacoma, Washington, 98401 (Z06/759-3551)
Manager: R. E. Shinkoskey
Employment:  1,000
(Company does custom smelting; verification of platinoid smelting necessary)

Kennecott Copper Corp. Metal Mining Division
Utah Copper Div. ,  P.O. Box 11299
Salt Lake City, Utah  84111 (801/322-1533)
General Manager:  J. P. O'Keefe
Employment:  7, 200
(Verification of platinoid smelting necessary)

Platinum and Palladium Processors
        It was stated earlier that the platinum-group metals industry in the free world is essentially
 centered around two mining companies and two affiliated  refining and fabricating  companies.  The
 majoi refining and fabricating companies processing mainly new platinoid materials (Engelhard and
 Johnson Matthey) arc not mining companies and are,  therefore,  not vertically integrated.  Imports
 of platinum-group metals include refined metals (90%), unrefined metals, crude ores and conccn-
 tiates, grain,  nuggets and  residue.  U.S. exports of platinum group metals, principally as semi-
 processed metals and alloys and as manufactured products are small compared with imports.
 Secondary recovery and toll refining comprise the bulk of domestic refining operations.  In 1968
 (latest figure available) 2. 3 million troy ounces were produced by toll refining  operations, of which
 91 percent represented used material and 9 percent was metal recovered from virgin material.  As
 it is not possible to separate this intertwined industry clearly by functions like mining, refining,
 fabucating,  etc. , the following lists show first the key members of this  industry (Group I) followed
 by those emphasizing refining  (Group II) and finally those emphasizing fabricating (Group III).  In
 i cality,  some companies may  be active in all areas and some only in segments of this industry.
 Companies listed are those with over $500, 000 total assets.   Some may be brokers only.  This can-
 not be avoided  as many of the specialized companies are not listed in Standard  &  Poor's  Register.
                     U.S.
Group I;  Key members

Engelhard Industries Division
(Engelhard Minerals and Chemicals Corp. )
430 Mountain Ave.
Murray Hill, N. J.  07974 (201/464-7000)
Executive  Vice President:  Robert S.  Levcnthal
Employment total;  7,500

Matthey Bishop,  Inc.
Malvorn,  Pa. 19355 (Z15/644-3100)
Vice President Operations:  U.S. Roberts
Also:  Johnson Matthey & Co., Inc., 608 Fifth
  Avenue, New York, N. Y.   10020(212/245-6790),
  representative of parent company, Johnson
  Matthey & Co. , Ltd. ,  78 Hatton Garden,
  London, E.G.  1,  England (01-405-6989)

Group II;  Refiners

Handy and Harman
850 Third Avenue
New York, N. Y.   10022
(212/752-3400)

American Chemical and  Refining Co.
P.O.  Box 4067
Waterbury, Conn.
                                                              Canada
                                            Engelhard Industries of Canada,  Ltd.
                                            512 King St. E.
                                            Toronto 2,  Ont.  (416/362-3211)
                                            Johnson Matthey & Mallory,  Ltd.
                                            110 Industry St.
                                            Toronto 15, Ont.  (416/763-5111)
                                            Handy and Harman of Canada. Ltd.
                                            141 John
                                            Toronto 20 Ont.


                                            National Refining Co. . Ltd.
                                            136 St.  Patrick
                                            Toronto (w)
                                                A-8

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                     U.S.
                   Canada
 National Lead Co.
 Goldsmith Division
 1300 W. 59th St.
 Chicago,  111.

 United Refining & Smelting Co.
 3700-ZO N. Runge Ave.
 Franklin Park,  111.  60131(312/455-8800)
 Hyper refiners.  Inc.
 P.O. Box 80-T
 Clifton,  N. J.
 Engelhard Minerals & Chemicals Corp.
 429 Oelaney St.
 Newark, N. J.  07105

 Eastern Smelting and Refining Corp.
 35 Bubier Street
 Lynn,  Mass (617/599-4000)

 Selrex Corp
 Precision Metals Recovery Division
 73 River Road
 Nutley, N.J.

 Spiral Metal Co.
 South Broadway
 South Amboy,  N.J.

 Sabin Metal Corp
 310-334 Meserolf St.
 Brooklyn, N.Y.  11206 (212/381-5000)

 Samuel J. A.  k Co. , Inc.
Engelhard Industries of Canada.
5 12 King St. E
Toronto 2.  Ont.  (416/362-3211)
Ltd.
233 Broadway
New York, N.Y.   10007

Midland Processing,  Inc.
53 Lafayette  Ave.
White Plains, N.Y.   10603(914/949-9310)

Mercer Refining
2801-T W Lake
Melrose Park, 111.

Croup III;  Fabricators
Western Gold k Platinum Co.
555 Harbor Blvd.
Belmont,  Calif.
Whittaker Corp.
10880 Wilshire Blvd.
Los Angeles,  Calif.

Wildberg Bros.  Smelting & Refining Co.
349 Oyster Point Blvd.
South San Francisco,  Calif.
                                               A-9

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                      U.S.
                                                                       Canada
 Ney.  J.M. Co.
 Drawer 990
 Hartford, Conn.  06101
 duPont. E.I, de Nemours &  Co.,  Inc.
 Wilmington,  Del.
 National Lead Co.
 Goldsmith Div.
 1300 W.  59th St.
 Chicago,  111.  60636 (312/925-3800)

 United RpfimriE & Smelting Co.
 3700-20 N. Rungc Ave.
 Franklin Park, III.  60131 (312/455-8800)

 Mercer Refining
 2801-T W. Lake
 Mel rose Park,  III.

 Texas Instruments, Inc.
 30 Forest
 Attloboro,  Mab&.

 Eastern Smelting &  Refining Corp
 35 Bubiur St.
 Lynn, Mass.  01901  (617/599-9000)

 Engelhard Minerals & Chemicals Corp
 1 13 Astor St.
 Newark, N.J.  07114 (201/243-2700)
 President: Milton F.  Rosonthal
 Employment: 7, 500 total

 Spiral Mutal Co.
 So. Broadway
 So. Amboy, N. J.  08879
Engelhard Industries of Canada. Ltd.
512 King St. E.
Toronto 2.  Ont.  (416/362-3211)
babin Metal Corp.
310-334 Mcscrole
Brooklyn,  N.Y.
Williams Gold Refining Co. , Inc.
2960 Main
Buffalo,  N.Y.

Adorer,  J. Inc.
44th Ave. & 22nd
Long Island City, N.Y.

Consolidated Refining, Inc.
120 Hoyt Ave.
Mamaronech,  N.Y.

American Metal Climax, Inc.
1270 Ave. of the Americas
New York, N.Y.

Anaconda Co.
25 Broadway
Now York, N.  Y.
                                              A-10

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                   U.S.
                                                                      Canada
Copper Joseph B.  fa Sons. Inc.
178 Varick
New York, N.Y.
Handy & Harman
850 Third Ave.
New York, N.Y.

Phillip Brothers Div.
299 Park Ave.
New York, N.Y.

Samuel,  J.A.  & Co.
233 Broadway
New York, N.Y.

United Mineral & Chemical Corp
Hudson  & Bach St.
New York, N.Y.
                Handy and Harman of Canada. Ltd.
                141 John
                Toronto 20, Ont.
Midland Processing. Inc.
53 Lafayette Ave.
White Plains,  N. Y.
Secon Metals Corp
5-7 Intervale
White Plains,  N.Y.
Buckeye Molding Co.
Crysteco Div.
181 E. Main
Wilmington, Ohio

Technic. Inc.
P. O.  Box 965
Providence, R. I.
American Chemical fa Refining Co.
P. O.  Box 4067
Waterbury,  Conn.

Deringer Metallurgical  Corp.
1252 E. Town Line Rd.
Mundelen, 111.
Inc.
Kron J. Williams Co. Inc.
301-303 Veteran Blvd.
Carlstadt,  N. J.

Hamos Co.
242 W. 30th
New York,  N.Y.
4.
       Prominent Sources and Processors
       In the U.S., most platinoids are byproducts from copper and gold refining and, therefore,
these types of companies are shown as representative  sources.  Processors (refiners and fabri-
cators) are those that may include refineries specifically for platinoids and thus direct human
exposure to platinum and palladium is expected to be much stronger during processing than during
copper and gold refining.
                                              A-11

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Prominent Sources (for details see pages A-4 through A-7).  Most Canadian concentrates,  residues
and matte are sent to England and Norway for refining or processing.
                     U.S.
                                                                      Canada
                                                   International Nickel Comp. of Canada,  Ltd.

                                                   Falconbridge Nickel Mines, Ltd.

                                                   Dumbarton Mines,  Ltd.
American Smelting & Refining Co.

United States Metals Refining Co.

Phelps Dodge Refining Corp.

American Smelting and Refining Corp.

Kennccott Copper  Corp.

Good News Bay Mining Co.

Prominent Piocessors :

Engelhard and Matthey Bishop are the most prominent and established platinoid companies, with
Engelhard having several divisions dealing in various platinoid applications.  In other companies,
paiticularly the larger and diversified ones, the number of employees may be misleading, as only
n relatively small number of employees may deal with platinum and palladium.
                     U.S.
Engelhard Minerals k Chemicals Corp.
Baker Platinum Division
700 Blair Road, Carteret, N. J.  07008

Chemicals & Catalysts; Engelhard Industries
Division of Engelhard Minerals &
  Chemicals Corp
429 Delaney, Newark, N. J.

Engelhard Industries
Division of Engelhard Minerals &
  Chemical Corp.
430 Mountain Ave.
Murry Hill, N. J. 07974 (201/464-7000)
Executive Vice President: Robert S.
  Li-vcnthal
Employment:  7, 500

Mattlmy  Bishop, Inc.
Malvirn, Pa.  19355 (215/644-3100)
Vice President Operations : H. S. Roberts

Handy & Harman
850 Third Ave.
Now York, N. Y.  1022(212/752-3400)
Vice President R&D: C. D. Coxc
Employees: 2, 200

Eastern  Smelting &  Refining Coip.
37-39 Bubicr
Lynn.  Mass. 01903(617/599-9000)
President: Jordan L. Alperin
Employees: 50
                                                                      Canada
                                                   Engelhard Industries of Canada,  Ltd.
                                                   512 King St. E.
                                                   Toronto 2,  Ont.  (416/362-3211)
                                                   Johnson Matthey & Mallory,  Ltd.
                                                   110 Industry St.
                                                   Toronto, 15,  Ont.  (416/763-5111)

                                                   Handy & Harman of Canada,  Ltd.
                                                   141 John
                                                   Toronto 21, Ont.
                                                A-12

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 	U.S.	      	Canada	

 N. L. Industries, Inc.
 Goldsmith Division
 1300 W.  59th St.
 Chicago,  III. 60636 (312/925-3800)
 General Manager: Albert Dipiazza, Jr.
 Employees:  160

 Consolidated Refining Co. Inc.
 120 Hoyt Ave.
 Mamaronek, N.Y.  10543(914/698-2300)
 President:  Mortimer M.  Cass
 Employees:  130

 Segrex Corp, Subsidiary
 Hooker Chemical Corp.
 Precious Metals Recovery Division
 73 River Road
 Nutley, N.J. 07110  (201/667-5200)
 Vice President  Research: D.  Bruce Mernfield
 Employees:  10, 000 total

 Western Gold &  Platinum Co.
 (Subs. GTE Sylvania)
 555 Harbor Blvd.
 Belmont,  Calif.  9400Z (415/593-3121)
 Vice President  Manufacturing:  Harold O. Richter
 Employees: 280

 J.  M. Ney Co.
 Drawer 990
 Hartford.  Conn. 06101 (203/242-2281)
 Production Manager:  Ronald G. Robinson
 Employees: 300

 5.     Manufacturers of Automotive Emission Control Systems

       U.S.
             Engelhard Minerals fc Chemicals Corp.
             Matthey  Bishop, Inc.
             Universal Oil Products
             W.  R. Grace
             Airproducts Division of Linde Products Company (Fecor Industries, Ltd. )

       Japan
             American Cyanamid and Japan Catalytic International

       Europe
             Deguzza  (VW)
             French Company (name unknown)
             Engelhard Kali-Chemie Autocat G. M. B. H. (West Germany)

6.      Production Data

       World production of platinum and palladium by country are shown in Tables A-3 and A-4 below.
It should be noted that official data—where available — are  usually 2 years behind in publication.  All
South African figures  are estimates,  as no data are published on this industry.

       World production expanded greatly in 1970, but demand failed to live up to expectations,  partly
because of the influence of business recession  in the leading consumer countries.  In early  1971,
producers were  forced to halt expansion projects and to cut back production.  As a result, world
                                               A-13

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                            Table A-3.  Platinum Production by Country
                                             (troy oz)
           Country

         Canada
         Colombia
         Ethiopia
         Finland
         Japan
         Philippines
         South Africa
         U.S. S. R.
         United States
         World Total

        Source:  Minerals Yearbook  1971 and E/MJ, March 1973.

                            Table A-4.  Palladium Production by Country
                                             (troy oz)

                                                         Year
1969
134, 715
27.805
343

3. 140

676.400
630,000
8, 702
1.481. 105
1970
209,374
26,358
273
295
3.296
352
1,068,000
660,000
8,036
1,975,984
1971
203,112
25,610
217
275
3,451
900
890,000
690,000
10. 198
1,823,763
1972 (Est.)
(205,000)
(24,000)
(250)
(250)
(3.000)
(1,000)
(1.000.000)
(678,500)
(8.000)
(1.920,000)
            Country            1969             1970             1971          197Z(E.t.)

         Canada               133.163         206.962          200,772          (208,000)
         Colombia              	
         Ethiopia               	
                                                   350              325

                                	                878            1,800

                             1.26o!oOO       l,3Zo!oOO        1,380^000       (1.397.000)
         UnitVd States            8J 387           11.875           20,951           (%™\
         World Total         1,643,877       1.921.175        1.922.979       (1,980,000)

         Source:  Minerals Yearbook 1971 and E/MJ, March 1973.

output slipped in 1971.  That trend was again reversed with auto industry  developments. Expansion
plans resumed aBain early in  1972,  and it is estimated that the  1972 output reached the previous high
of 1970   The most active growth in the free world occurs in South Africa where platinum output
may be  boosted to upwards of 1. 4 million o» in 1973 and further in  1974 and after, if the confidence
m the auto demand outlook is  unshaken.  Some output recovery  may be seen in Canada, although the
long-term trend is relatively  static.

7.      Consumption Data

        It was noted earlier that official data are published usually with a two year delay.  Hence, the
U. S.  consumption data are  now available for the year 1971.

        United States.  During 1971, the total sales of platinoids to  the chemical, petroleum and
electrical industries accounted for 83 percent of all sales compared with  82 peicent in 1970. Plati-
num  sales decreased slightly despite the 25-percent increase in sales to the petroleum industry and
nains m sales for dental, medical and  miscellaneous uses.  The increase in sales to the petroleum
industry was for new reforming units to produce non-leaded gasoline.  The bulk of platinum sales  in
1971  was distributed among petroleum icfmers (46.5  percent),  manufacturers of organic and
inorganic chemicals (25.0 percent), and  electrical and electronic equipment manufacturers (9.6 per-
cent).  Palladium sales increased  3 percent in 1971 despite sizable declines in sales to the glass
industry.  Sales to manufacturers of chemicals increased  18 percent,  to manufacturers of electrical
equipment 1 percent and accounted  for 29 and 57 percent,  respectively, of all  palladium sales.
Table A-5 shows the sales  of platinum and palladium to consuming industries in totals,  and Table A-b
and Table A-7 show sales to  industry groups.
                                                A-14

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                             Table A-5.  Platinum and Palladium Sold in
                                     the United States (troy oz)

                        Year             Platinum              Palladium

                        1967               633,864                6Z1. 141
                        1968               580,155                721,479
                        1969               515,578                758,738
                        1970               566,369                739.343
                        1971               541,164                760,106

                        Source: Minerals Yearbooks.


                Table A-6.  Platinum Sold to Consuming Industries in the United States
                                             (troy oz)

           	Industry	      1967        1968       1969       1970     ^  1971

           Chemical                  159,384    157,677    175,436    148,289   135,112
           Petroleum                245,560    161,050    58.602    202,015   251,876
           Glass                     45,150     47,935    63.350    46,687    40,703
           Electrical                 99,686    117,256    112,589    103,318    51,940
           Dental and Medical        24,630     24.903    22.266    18,302    23,097
           Jewelry and Decorative     33,342     40,184    36,161    29,203    18,577
           Miscellaneous             26. 112     31. 150    47. 174    18.555    19.859
           Total U.S.                633,864    580,155   515.578    566.369   541,164
           (re-revised)

           Source:  Minerals Yearbooks.
               Table A-7.  Palladium Sold to Consuming Industries in the United States
                                             (troy oz)

                                    	Year	
          	Industry	      1967       1968       1969       1970       1971

          Chemical                 192,011    228,318   214.508   184,618    218,651
          Petroleum                  3.506     22,683      1.337     15.494      2,916
          Glass                        301         10      3,891     21,147        237
          Electrical                324,684    329.012   430,258   429,032    431,505
          Dental and Medical         56.085     61.636     52,326     47.583     61,594
          Jewelry and Decorative     18,676     17,797     21,837     17,329     18,752
          Miscellaneous             25.878     62.023     34.581     24. 140     26.451
          Total U.S.                621,141    721,479   758,738   739.343    760,106

          Source:  Minerals Yearbooks.

       Consumption data of countries outside the United States are difficult to assess,  as trade data
for each individual country would be needed.  These are not readily available.  The Rustenburg group
has provided some estimates for the distribution of demand among the total Western world  for newly
mined platinum.  These estimates.are based on data for the period of 1965-69. As secrecy shrouds
platinoid data in some producing countries, the following figures, developed for 1971, can be con-
sidered as only an overview of a complex and highly inter me shed demand-supply relationship for
platinoid using countries. The Rustenburg data estimated that 30 percent  is distributed to the
chemical industry,  25 percent to petroleum catalytic uses, 20 percent to electrical and  allied
industries, 10 percent to glass manufacture,  and the remaining 15 percent are distributed among
various uses  including jewelry and medical applications.

       The total new world production during 1971 in platinoids was  4,076, 788 ounces troy of which
1, 823, 763 oz were platinum and  1, 922, 979 oz were palladium.  Free world demand distribution  for
                                              A-15

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new platinum and palladium metals is shown in Tables A-8 and A-9.  The industry distribution is
based on U.S. 1971 data as shown in Tables A-6 and A-7,  with Rustenburg estimates for platinum
given in parentheses. The Rustenburg data differ widely with the  U.S.  distribution in most industrial
categories.  It should be expected that the demand distribution in  most industrialized nations of the
Free World follow more closely the U.S. pattern.  As Rustenburg assumes an authoritative position
in this metals industry, the actual demand distribution may be between both limits.

                       Table A-8.  Free World Platinum Demand Distribution
                                              (troy oz)

              Total 1971 world production                                  1,823,763
              U.S.S.R. estimated total 1971 production                        690,000
              U.S. S. R. estimated 1971 export                                336,375
              U.S.  new 1971 production                                        10,198
              Free World available new production                          1,459,940
              Estimated demand distribution
                 Chemical industry (25 percent)                  364.985     (473,852)
                 Petroleum industry (46. 5 percent)               678,872     (394,876)
                 Glass industry (7. 5 percent)                    109,496     (157,951)
                 Electrical industry (9.6  percent)                140,154     (315,901)
                 Dental and medical industry (4. 3 percent)         62,777
                 Jewelry and decorative industry (3. 4 percent)     49,638     (236,926)
                 Miscellaneous (3. 7 percent)                        54,018

              Source:  Minerals Yearbook 1971,  Universal Facts and Problems 1970
                       and Southwest Research Institute.


                       Table A-9.  Free World Palladium Demand Distribution
                                              (troy oz)

              Total 1971 world production                                  1,922,979
              U.S.S.R. estimated 1971 production                          1,380,000
              U.S.S.R. estimated 1971 export                              1,009,125
              U.S.  new 1971 production                                        20,951
              Free World available new production                          1,531, 153
              Estimated demand distribution
                 Chemical industry (28.8 percent)                440,972
                 Petroleum industry (0.4 percent)                  6, 125
                 Glass industry (0.03  percent)                        459
                 Electrical industry (56.77 percent)              869,236
                 Dental and medical industry (8. 1 percent)       124,023
                 Jewelry  and decorative industry (2.5 percent)      38,279
                 Miscellaneous (3.4 percent)                      52,059

              Source:  Minerals Yearbook 1971, Universal Facts and Problems 1970
                       and Southwest Research Institute.

       The determination of consumption  figures for individual countries is difficult for several
reasons.  The high cost of platinoids has created great demand for secondary sources and recovery.
Recovery takes  place by processing scrap materials which include discarded jewelry, used elec-
tronic components and spark plugs, sludges and sweeps.  In  addition,  large quantities of worn out
or contaminated platinum-metal-bcaring materials  are refined on toll.   This metal, compromising
the bulk of domestic refining operations, was received for reworking or re-refining of depleted
catalysts,  wornout extension dies, spinners, laboratory ware and other used equipment.   Recovery
fiom scrap is very efficient, and only  a small quantity of these metals  is wasted or lost.  Secondary
recovery of platinum and palladium in  the United States is shown in Table A-10.

       While quantities of secondary recovery  platinoids  are well known for the U. S. ,  the same
information for  other countries could not be obtained.  Furthermore, the trade patterns worldwide
as well as within the free world vary considerably.  Platinoids are shipped in form of ores, con-
centrates, residues, waste, scrap and sweepings, partly worked rolled and partly  worked not rolled.
                                                A-16

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                       Table A-10.  Platinum and Palladium Secondary Recovery
                                     in the United States (troy oz)

                             Year           Platinum          Palladium

                             1967            126,377           21S,162
                             1968            115,587           195,620
                             1969            126,822           227,763
                             1970          r!18,298          r208,555
                             1971            103,429           161,099

                             (r:  revised)

                             Source: Minerals Yearbook 1971.

        For example, during 1971 the U. S. has exported 404, 610 troy oz of platinoids in various
 metal stages to 17 countries.  These shipments included  154, 775 oz platinum unworked or partly
 worked not rolled and 15, 894 oz platinum unworked or partly worked rolled.  During the same year,
 the U. S.  has imported for consumption 1, 302, 740 oz from 24 countries in various unwrought or
 semimanufactured conditions.  These inputs included 551, 127 oz of platinum and  657, 983 oz of
 palladium.  These data indicate that no clear  picture emerges from these trade patterns to determine
 actual consumptions in foreign countries.  In  addition, and as noted earlier,  the U. S. S. R. and the
 Republic of South Africa,  the major platinoid  producers in the world, do not publish data on plati-
 noids, and all their figures, found in publications,  are estimates by the trade.  International trade
 data for platinoids are available for the year  1969.   Some of these data are given for platinum and
 palladium, some are given as a combination of platinoid and silver  shipments and some are given
 only for non-ferrous metals.  In Table A-ll,  the 1969 percentages of individual countries to the
 total 1969 world production of platinum and palladium are applied to the 1971 consumption year.

                 Table A-ll.  Platinum and Palladium Consumption by Major Country
                                    (Order of Magnitude in troy oz)

                              	Country	             1971

                              Canada                          68.259
                              France                         312,947
                              Germany,  West                 451,330
                              Italy                             74,227
                              Japan                          758,309
                              Netherlands                     32.824
                              Sweden                          17,158
                              Switzerland                      11,563
                              U. K.                            48, 863
                              U.S. S. R.                       589.340
                              U.S.                           1.375.788
                              Total Approximately            3, 740, 608

                              Source:  Minerals Yearbooks.

The total  consumption (3. 74  million troy ounces) compares favorably with the 1971 production
figure of 3. 75 million ounces.  The data shown represent  an order of magnitude approximation for
major consuming countries.   With the exception of Japan and the U. S., variations  are expected.
The causes for these are  based on inadequate  data on foreign stockpiles, dealer stocks, and foreign
secondary recovery.  These data  also include  small shipments of platinoids from  major consumer
countries to a large number of less  industrialized and small countries, caused very likely by
Futures trading and speculation.

8.     End Use Applications

       Platinoids find many applications in industry  because of their catalytic activity, resistance to
corrosion, resistance to oxidation at elevated  temperatures,  high melting  point, high strength and
good ductility.  Platinum and palladium are the major platinum metals; indium, osmium, ruthenium
                                                A-17

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and rhodium are used mainly as alloying elements to modify properties of platinum and palladium.
Rhodium is also used in plating.

       Chemical industry.  One of the major uses for platinum,  alloyed with 10 percent rhodium, is
as a catalyst in producing nitric acid for use in nitrate fertilizers and explosives.  New uses for
platinum and palladium as an oxidation catalyst are evolving in the rapidly expanding pollution con-
trol field.  Platinum and palladium are widely used as a catalyst in hydrogenation.  dehalogenation
and other reactions  used by chemical,  dyestuff and pharmaceutical industries.

       Platinum and other platinum-group metals are used also as catalysts in a great variety of other
chemical processes as  shown in Table A-12.

               Table A-li.  Chemical Processes Using Platinum-Group Metal Catalysts

         	Process	       	Catalyst	.	

         Hydrogenation                Pt, Pd, Ir, Rh, Ru,  Os.
         Dehydrogenation             Pt, Pd, Ir, Ru, Pd-Ag.
         Fragmentation               Pt, Pd.
         Decomposition               Ir, Ru.
         Hydrocracking               Pt, Ir.
         Reforming                    Pt, Ir,  Rh, Pt-Ir.
         Synthesis                    Ir, Rh, Ru.
         Polymerization              Ir-Ni, RhCl3.
         Isomenzation                Pd,  IrCl3. Ir-Ni, Ir-V, RhCl3,  Pt-Ir,  Pt-Rh. Pt-Ru,
                                        Pt-Os.
         Oxidation                    Pt, Rh, Ru,  Pt-Ir,  Pt-Rh.
         Regenerable reagents         PdCl3.
         Homogeneous  reactions
           Carbonylation              Ir, Ru, PdCl3, Rhds, Rh(NO3>3-
           Oxidation                   Ir, Ru, PdCl$.
           Reductions                 Ru,  Pt-Ir, RhCls-

         Source:  Minerals Yearbook 1971

       Platinum spinnerets are used in the production of synthetic fibers.   New precious-metal catalyst
systems are being developed constantly to reduce utilization of platinum at no loss in catalyst effi-
ciency.  A precious-mctal-plated titanium anode may replace graphite anodes  in the chlorine manu-
facturing industry.

       Petroleum industry.  Generally,  platinum and palladium are used as catalysts in the produc-
tion of high-octane gasolines and for hydrocarbon synthesis to produce numerous petrochemicals.
Reforming units to produce nonleaded gasoline will lead to  a substantial  increase in platinum con-
sumption.   However, application of a new platinum-rhenium catalyst to refining, requiring much
less platinum, may offset the demand for this puipose.

       Glass industry.   A substantial quantity of platinum-rhodium alloy is used for bushings for
attenuating the glass fibers and for equipment used in manufacturing other glass products. Glass-
making refractory equipment is coated with a thin layer of platinum sheet to prevent contamination
of the molten glass.  More uses for platinum-indium alloys are found in crucibles for growing
crystals for lasers,  optical modulators and other scientific applications.

       Electrical and electronic industry.  Platinum, palladium and various alloys find major
use in such application as light duty contacts, electric furnace windings, thermocouples,  cobalt-
platinum permanent magnets for travelling wave tubes,  resistance thermometers and precision
thermometers, relays, meters, voltage regulators, and other electrical instruments.  Palladium
especially is used in low voltage-low energy electrical contacts  in telephone equipment.   Platinum
and palladium are also used in powder (paste) form or as electrodeposits in components of electrical
printed circuits.  Platinum is also used in fuel cell electrodes,  and new developments in this field
could lead to a substantial increase in platinum requirements.  Significant quantities of platinum
were also  used in impressed current corrosion protection  systems.  Some pacemakers to stimulate
the heart muscle  use platinum or platinum-indium electrodes.
                                                 A-18

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        Dental and medical industry.  Additions of platinum and palladium to gold-based alloys
 increase strength, hardness and wear resistance,  raise the melting temperature and enhance the
 age hardening of the alloys.  These alloys are used extensively in fabricating mechanical aids and
 devices for application in prosthodontics and orthodontics.   Palladium-rich alloys are used as sup-
 ports in the porcelain-overlay type of dental restoration because palladium does not stain or  discolor
 the porcelain after it is fired.  Testing of platinum compounds for their therapeutic value in cancer
 treatment of humans is well along in  many institutes in the U.S. and abroad.  The possibility is
 indicated that platinum compounds knock out or cause remissions in a very broad  range of cancers,
 with little or  no side effects.  It also appears that platinum may have possibilities as an antiviral
 agent,  and that it may inhibit leukemia.

        Jewelry and decorative industry.  Platinum, palladium and rhodium are used to fabricate
 various jewelry articles  such as watch cases,  rings, brochcs and other settings.  These metals
 provide lightweight,  white, tarnish-free alloys.  Palladium-ruthenium alloys arc used for large
 jewelry articles because of their density and thus their light weight.  Platinum settings do not
 mask the true color of diamonds, whereas gold lends a yellow tint.  In addition, and because of
 platinum's mechanical properties, platinum settings hold gemstones more securely than gold.

        Miscellaneous uses.  These uses of platinum-group metals  include laboratory ware such as
 electrodes and crucibles.  Platinum is used to control galvanic corrosion such as the cathodic pro-
 tection of  ship hulls, and as inert anodes in electrodeposition.  New uses for control of corrosion
 are  found in the metal, chemical,  petroleum,  sewage disposal and  water supply industries.   Brazing
 alloys which contain palladium have good wetting ability and are relatively free  from erosion at high
 temperatures.  These alloys are frequently used in gas turbines, jet engines, and air frames when
 a high level of reliability is required. Platinum and chromium are used to give razor blades a hard,
 corrosion-resistant edge.  The automotive industry has all but accepted the platinum/palladium/
 ruthenium based  catalytic mufflers for pollution control beginning  with 1975 model automobiles.
 In this  system, exhaust gases pass over a platinum catalyst in the muffler and the carbon monoxide
 (CO) and hydrocarbons (HC) are converted to carbon dioxide and water.  Oxides of nitrogen (NOx)>
 which also have ceilings  under Environmental Protection Agency (EPA) guidelines, are not reduced
 by the platinum catalyst, but can be reduced by lower engine temperatures,  engine modifications,
 or other catalysts in the  system.  The system must use nonleaded gasoline, because lead, even in
 small amounts, makes the catalyst inoperable.

        Research  and Alternates.  Extensive research and development programs are pursued with
 particular emphasis on applications of platinum-group metals in such industries as petroleum and
 petrochemicals,  pharmaceuticals, electrical energy and electrical and electronic products,  and
 powder metallurgy.   Considerable effort is being directed toward the development of high-activity
 platinum electro-catalysts for the direct conversion of chemical energy into electrical energy in
 fuel cells, and there is an increased  interest in research to develop a technically and economically
 feasible method of recovering palladium and rhodium from atomic wastes.

        However,  there is also  constant economic pressure to substitute less expensive materials
 for the  platinum-group metals in industrial applications.   The platinum metals are only  used where
 they are justified  technically and economically.  Platinum and palladium as well as the minor
 platinum-group metals are used interchangeably to some extent for certain uses.  In some uses,
 tungsten and nickel alloys, vanadium, silver and gold can  be substituted for platinum-group  metals.
 Cladding with platinum-group metals  enables the surface properties of the noble metals  to be com-
 bined with the mechanical strength of cheaper metals.  Cladding is common in glass melting  pots
 and in chemical ware.  Rhenium-platinum  reforming catalysts may replace platinum to some extent
 in petroleum refining.  Cobalt-copper-rare-earth alloys may be substituted for platinum-cobalt
 as a high-energy magnetic alloy in certain electronic applications.

        In the  automotive industry, there are three approaches competing with the platinum/palladium
 catalytic muffler.  (1) The nonplatinum catalyst system uses a cheaper catalyst that is resistant to
 lead poisoning and hence can use currently available gasoline.  Some catalysts for this type of sys-
tem are oxides of vanadium, chromium,  manganese, iron, cobalt,  nickel, copper, molybdenum,
tungsten and  rare-earth elements.  Although few details have been  released on the performance of
these systems, they apparently have not been tested as extensively as the platinum system, and
their long-term reliability  is uncertain.  (2) The thermal reactor represents an afterburner to con-
vert CO and HC to carbon dioxide and water, in coordination with engine modifications and exhaust
gas recirculation  to reduce NOx* While these  systems approach the emission standards for the  life
                                                A-19

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of the car (versus platinum systems 25,000 to 50,000 mile reliability),  they reportedly reduce gas
mileage and "driveabihty" considerably.  Nevertheless, this system is a strong contender.
(3) Experimental automobiles with radical engine designs are being tested.  Their engines are
inherently pollution-free.  Some of these are steam-driven cars, battery-run electric cars, turbine-
engine cars,  or they may use the Warren engine and other stratified-charge engines.  Although the
design changes and lack of proved reliability and other characteristics make these cars unlikely
candidates for  1975 production by major manufacturers, some of these  engines may be adopted as
long-range solutions to the pollution problems in the 1980's.

9.     Attrition and Transfer to the Environment

       In providing attrition and transfer rates, it is necessary to review the following breakdowns
according to published statistics.

       Chemical Industry.  In 1971, this industry purchased 135, 112 oz of platinum and 218, 651 oz of
palladium.  It is estimated that these purchases were divided as follows:

                                                    1971                    1972
                                                 Platinum               Palladium
                                                 (troy oz)               (troy oz)

               Chemical (inorganic)           83,229  (61.6%)         47,227  (21.6%)
               Chemical (organic)	51.883  (38.4%)	171.424  (78.4%)
               Total Chemical Industry        135,112(100.0%)        218,651(100.1
       The rough data estimates for consumption rates in the chemical industry provided by the
Buieau of Mines  are for nitric acid production only.  These consumption data are related to the
latest industry purchased data of platinum and palladium,  published for 1971 (Tables A-6 and A-7).
In inorganics, the two largest production items  using catalysts with platinum-group metals are
shown  below in billions of pounds (bp):

       Sulfuric  acid, 100%           58. 84 bp
       Nitric acid,  100%            13. 48 bp.

In organics,  the three major production groups,  utilizing  such catalysts are:

       Ethylene                     18. 30 bp
       Cyclohexane                  1. 75 bp
       Benzene                      1.08 bp.

The total chemical industry produced in 1971 about 203.00 bp inorganics and about 77.00 bp organics,
or a total of  280. 00 bp.

       Petroleum Refining.  The major data in this industry are published for crude-oil throughput
capacity, catalytic cracking,  catalytic  reforming and hydroprocessmg.  The rough data estimates of
consumption rates, available  at this time, are for catalytic  reforming.  The development of total
U.S. refinery, cracking and reforming capacities are  shown below in  1,000 barrel per calendar days

                                           Crude Oil     Cracking      Reforming
                                           Capacity     Capacity      Capacity
                    	Year	   [1000  b/cd)   (1000 b/cd)     (1000 b/cd)

                    December 31,  1971    13.284.9     4,512.5       2,885.2
                    December 31.  1972    13,087.0     4,852.0       3,169.1
                    December 31,  1973    13,383.0     4,512.5       3,278.1

The following Tables A-13 and A-14  provide  rough consumption estimates,  available at this time,
for use,  replacement, scrap, attrition and transfer rates for platinum/palladium catalysts in major
industrial use categories. Based on the data shown above, order of magnitude comparisons are
possible  for  amounts of platinum and palladium used in those consuming industries for which detail
data are  not  available at this time.
                                                A-20

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                 Table A-13.  Estimated Platinum Consumption Rates in the United States
                                             (troy oz/Year)

Replacement Use Scrap Attrition
Industry Rate Rate Rate Rate
Chemical1)
(inorganic) 397,000 --- --- 53.0002)
Chemical
(organic) --- 	 	 	
Chemical Total 	 	 	 	
Petroleum
(reforming) 270,000 over 8, 5003)
Petroleum total 	 	 	 	
Glass4)
Electrical --- 92,000 18.000 74,000
Dental & medical 	 30,000 900 29,100
Jewelry &
decoration 	 20.000 4,600 15,400
Miscellaneous 	 50, 000^) 	 	
Total known
at this time 667,000 192.000 23.500 180,000
1) nitric acid production only
Transfer
Rate to
Environment

49,000 est.

	
. .. .

over 8, 500 est.
...
...
74, 000 est. 5)
29, 100 est.

15,400 est.
- - •

176,000 est.

1971
Purchase for
Consumption

83,229 est.

51,883 est.
135, 112

_ _ _
~_. o-jf.
40,703
51, 940
23,097

18,577
19.859

541, 164

2) includes 4000 oz. refining, rest transferred to environment or into products
3) includes losses in reprocessing, does not include entrainment in products
4) no data available
5) includes transfer to environment direct and through manufactured
6) scrap, attrition and transfer rates unknown at this time
Source: Bureau of Mines and Southwest Research Institute
Table A- 14. Estimated Palladium Consumption Rates
(troy oz/Year)

Replacement Use Scrap Attrition
Industry Rate Rate Rate Rate
Chemical')
(inorganic) 	 ... 	 	
Chemical1)
(organic) 	 	 	 	
Chemical Total1) 	 	 	 	
Petroleum')
(reforming) 	 	 	 	
Petroleum Total1) 	 	 	 	
Glass2)
Electrical3) 	 425,000 	 	
Dental & medical --- 94,000 3,000 91,000
Jewelry &
decorative --- 19,000 4,500 14,500
Miscellaneous4) 	 28,000 	 	
Total known ~ ~ '
at this time 	 566,000 7,500 105,500

goods






in the United States

Transfer
Rate to
Environment

	
_ _ _


_ _ _


P. - —
91,000 est.

14,500 est.

105. 500 est.

1971
Purchase for
Con sumption

47,227 est.
171, 424 est.
218, 651


2 Q16
t« I 7 1 U
431,505
61,594

18. 752
26,451

7hn inft
1) no data available at this time.
2) no data available yet, as glass industry is difficult to assess
3) telephone industry is dominant user; scrap,  attrition and transfer rates unknown.
4) scrap,  attrition  and transfer rates unknown at this time

Source:  Bureau of Mines and Southwest Research  Institute
                                                A-21

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 10.     Supply and Demand Trends

        Apparent Supply.   U.S.  reserves are almost entirely in copper ores with a very small quantity
 in placers at Goodnews Bay,  Alaska.   The copper ores are estimated to average about  1 oz of platinum-
 group metals  per 6000 tons of ore.  Production from placer deposits at Goodnews Bay,  with signifi-
 cant amounts  of indium, rhodium and ruthenium,has been slowly declining in recent years, and the
 remaining reserve is  believed to be relatively small.  The aggregate reserve of byproduct platinum-
 group metals  in gold ores also is relatively small.

        The recoverable reserve in the Republic of South Africa is  estimated at 200 million ounces,
 averaging on the basis of past production about 70 percent platinum,  25 percent  palladium and 5 per-
 cent minor platinoids.  Actually, the  occurrence of platinum-group metals in significant quantities
 in the Merensky  Reef Horizon of the Bush veld igneous complex indicates that the quantity of platinum-
 bearing ore may be considerably larger.  The reserve of byproduct osmium and indium in the gold
 ore of the Republic of South Africa is  significant.  In Southern  Rhodesia, prospecting and exploration
 of the Great Dyke ultrabasic formation has disclosed the existence of platinum-group metals which
 may potentially reach 100 million ounces.

        Ethiopia has provided small quantities of metals from platinum placer deposits  for years.
 Exploration for additional sources is  underway.

        In Canada,  the platinum-group metal content of the proven nickel-copper ore reserve  of the
 Sudbury Basin and  Thompson, Manitoba areas is estimated at  16 million ounces, comprising  7.4 mil-
 lion ounces of platinum, 7.0 million ounces of palladium, and  1.6 million ounces of minor platinoids,
 chiefly  rhodium.

        Colombian placer deposits contain substantial reserves of platinum.

        U.S. S. R. production of platinum-group metals has been rapidly expanding in recent years,
 and it is estimated that reserves of platinum-group metals  in the U. S. S. R. are  at least 200 million
 ounces.

        Finland is providing small amounts of platinum-group metals from copper refining.

       Japan  provides small  amounts of platinoids, mostly platinum  and palladium as byproducts of
 nickel-copper refining.

       The Philippines are furnishing mostly platinum and  palladium from nickel-cobalt concentrates.

       In Western Australia,  high platinum values were found on the Northwest  Oil and Mineral Co.
 property.

       In New Zealand,  high  platinum values were found on the Georgia-Kaolin Co. property  near
 Kerikeri, North Auckland.

       In Papua New Guinea,  an  independent nation since December 1973, and  formerly under
 Australian administration,  increasing platinoid production is expected at or near the island of Bougain-
ville as substantial copper ore deposits are opened up.

       Estimated proved reserves of  platinum  and palladium metals from known conventional sources
are shown in Table A-15.

       The estimated  proportions of six coproduct metals  in the platinum  group are shown on
Table A-16.

       Demand.  Of immediate  effect on the demand for platinum,  palladium and possibly ruthenium
metals is the development in the automobile emission control and petroleum refining areas.   But, the
market  outlook and hence the  market  price for these metals is still clouded.  In the U. S., the major
automobile manufacturers have  negotiated substantial supply contracts to  permit all-out production
of 1975  cars equipped  with platinum/palladium based  converters.  Volvo (Sweden) has contracted for
 100,000 antipollution units to  equip cars for U.S. delivery.  Nissan Motors (Japan) have signed a
letter of intent to purchase 400, 000 converter devices to equip that firm's cars for U. S. delivery.
                                              A- 22

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                   Table A-15.  Estimated World Reserves of Platinum and Palladium
                                           (million troy oz)

                       Country                        Platinum       Palladium

                       United States                      0.95            1.96
                       Canada                           6.94            6.86
                       Colombia                         5.00            	
                       South Africa,  Republic of        142.40          50.20
                       U.S. S. R.                        60.00         120.00
                       Total                           215.29         179.02

                       Source:  Mineral Facts and Problems,  1970

                    Table A-16.  Estimated Composition of Platinoids by Source
                                             (percent)

                                   Source         Country
                   Metal           Canada       U.S. S. R.        South Africa

                   Platinum         43.4           30.0              71.20
                   Palladium        42.9           60.0              25.10
                   Indium            2.2            2. 0                .78
                   Rhodium          3.0            2.0               2.41
                   Ruthenium         8.5            6.0                .50
                   Osmium           	            	                 _ 0]

                   Source:  Mineral Facts and Problems, 1970

 Toyota Motor Co.  (Japan) has also contracted for catalysts,  Leyland Motor Corp. (Great Britain) is
 reportedly negotiating with prospective suppliers of platinum-based converters.  Engelhard Kali-
 Chemie Autocat G. M. B. H. (West  Germany) will provide catalysts  forDnouer-Benz,  Peugeot and
 Renault cars.   Although the Environmental Protection Agency (EPA) has resisted requests for an
 extension  of the 1975 deadline, Detroit is still pressing for delay.  This delay is also supported by
 the Administration for reasons of  the current energy and gasoline crises. Despite the fact that  the
 major U.S. manufacturers have negotiated substantial supply contracts,  the industry's actual com-
 mitment is small,  because of the escape clauses in these arrangements.

        Perhaps a still more serious problem  concerns the availability of unleaded gasoline.   Since
 platinum/palladium catalysts are rendered ineffective by the presence of lead,  unleaded fuel must be
 made available  in time to supply 1975 cars, and autofirms have indicated that the maximum residual
 lead content permissible  in such fuels is 0.03 g per gal.  However,  sources  in the petroleum industry
 have continued to express doubt as to the possibility of producing sufficient quantities of unleaded
 gasoline in time to meet  1975 auto requirements.  It seems almost certain that great quantities  of
 platinum and palladium (and possibly  some ruthenium) will be required in manufacturing converters
 for 1975 automobiles and that the petroleum companies will utilize  additional quantities of platinum
 catalysts in petroleum refining,  to boost the octane rating of gasoline without lead additives.  It has
 been estimated  by Engelhard that each car will require an average  of 0. 1 oz of metals including  30-
 35% palladium and  65-70% platinum.   If upwards of 10 million 1975 model U.S.  cars were equipped
 with these converters, then first year requirements beginning in 1974  could  amount to 700,000 to
 800, 000 oz of platinum and  300, 000 to 400, 000 oz of palladium with still larger quantities demanded
 in ensuing years.

       Based on these factors  and  allowing for expanded use by auto manufacturers outside the U. S.  ,
 it has been estimated that world consumption of platinum could increase from an estimated 1.92 million
 oz in 1972  (Table A-l) to  about 3.0 million oz  in 1974 and considerably more theieafter. Over the
 same period, global use of palladium  might expand from  around 1.98 million oz in 1972 (Table A-l)
 to perhaps 2.4 million oz in 1974 and  2.6 million oz in subsequent years.  These data suggest a  pos-
 sible increment  in annual world use during 1972-74 of over 1 million oz of platinum and 500. 000 oz of
 palladium.  Present trends  of platinum and palladium production were  shown in Tables A-l, A-3,  and
A-4 and estimated reserves in Table A-IS.
                                              A-23

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       Among the established producing areas, South Africa may experience the most active growth.
As shown in Table A-Z,  platinum output in 1972 was estimated to be 1  million oz, and palladium out-
put 355, 000 oz.  The output could be boosted to about 2.5 million oz of platinum and 890, 000 oz of
palladium in 1975.  The U. S. S. R. was expected to produce close to 700,000 oz of platinum and about
1.4 million oz of palladium in 1972.  Although she is exporting a substantial amount of both  metals,
her output in these metals appears to increase. It is estimated that Canada produced about 399,000 oz
of platinum group metals in 1972, and that she could increase production to over 500,000 oz.

       In emergencies,  and if Congress approves the release of stockpile  material, platinum and
palladium reserves could be provided for eventual sale.  The U.S.  national stockpile on Dec. 31,
1971 consisted of 402,646 oz of platinum and 507,314 oz of palladium.   The supplemental stockpile
included 49,999 oz of platinum and 747,680 oz of  palladium.

       Recent Developments.  Supply and demand trends will be influenced, above all, by possible
changes  in the Clean Air Act with regard to auto emission standards and timing for conformance.
Earlier, in April  1973, the EPA had established modified interim standards for auto emissions
and granted automobile manufacturers  a one-year extension in implementing the federal  1975 exhaust
emission standards on all cars manufactured with the exception of those sold in California.  Later,
at the end of 1973, the Administration  requested Congress to amend the Clean  Air Act and proposed
that  1975 interim levels should be frozen for 2 years to "permit auto manufacturers to concentrate
greater attention on  improving fuel economy while retaining a fixed target  for  lower emissions. "

       On March 22, 1974, the Administration has made several proposals to Congress to sacrifice
some air quality for making the nation  self-sufficient m energy by  1980.  Again included are proposals
to freeze the auto-emission standards through 1977.

       According to current trade  sources.  General Motors has indicated  it may  install  platinum/
palladium catalytic converters on many of its 1975  U.S. models to  ensure  compliance with interim
standards, and Ford considers that about 25 percent of its 1975 production will be fitted with platinum
converters.  Other manufacturers  expect to use catalytic  converters on cars manufactured for the
California market.  Hence, the EPA extension will have a moderate effect on delaying the projected
platinum and palladium consumption  in catalytic converters and while  the near term requirements
have become less stringent, the medium term outlook for these metals appears encouraging.

       It also is of interest to note that in July 1973, the Canadian  Government announced new exhaust
emission control standards for 1975  model cars in Canada that are much less  stringent  than those
adopted by the United States.

I 1.    Medical and Toxicological Information

       The information  m this section  is in part based on two literature searches, conducted by the
MED LINE Data System of the University of Texas Health Science Center at San Antonio and by the
National Technical Information Service, U.S. Department of Commerce, Springfield, Va.

       Human Exposure Cases

Synopsis.    Contact with the platinum oxide has  been reported  to cause eczematous lesions,  and the
             development of sensitivity to platinum chloride was observed in a chemist,  who suffered
             a generalized  eruption from contact with a small amount of the substance.   The trioxide
             has also given rise to dermatitis in  the Jewelry and Allied Industries.  Photographers
             have been reported to contract dermatoses from platinum solutions used in their work.
             Asthmatic  symptoms  are not uncommon among workers  exposed  to the salts of platinum.
             Palladium  compounds show little or no irritation,  when applied locally to the skin.

       Platinum (Pt) is  a silver-white metal,  tenacious, very malleable,  ductile and softer than silver.
Exposure to platinum in industry occurs in the metallurgical and chemical processes used in the pre-
paration of the metal and its salts.

       Platinum was considered relatively harmless until 1945  when Hunter,  Milton & Perry published
the results of their investigation of four platinum refineries.  They found that, of 91 workers exposed
to the dust or spray  of complex salts of platinum, 52 suffered from running of the nose,  sneezing,
tightness of the  chest, shortness of breath, cyanosis,  wheezing, and cough.  Thirteen of the men
complained of dermatitis.   None of these symptoms were apparent in  the workers exposed to metallic


                                              A-24

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 platinum dust only,  or to the complex salts of the other precious metals, including palladium.  The
 platinum content of the air samples taken at various stations throughout the works was determined
 spectrographically and found to vary from 5jig to 70 (ig  per cubic meter (Fothergill,  Withers & Cle-
 ments, 1945).   One may safely conclude,  therefore, that the soluble platinum  salts,  whether carried
 as dust or mist, present an industrial hazard,  and  that they should be carefully controlled and not
 exceed a maximum allowable concentration of 2 jig per cubic meter.

        The following case histories are given as examples of the syndrome.

        Milne (1970) reports the following clinical record from Australia:  The patient, a tall, brown-
 haired, blue-eyed male, aged 37 years, was first examined in early May 1969, when he stated that
 he had been born in Germany and had migrated to Australia at the age of 20 years.  He had worked
 as a laborer, a hospital orderly and a laboratory assistant.  Tn  1967,  he came to his present position
 as a chemical assistant in a firm which intermittently processes platinum.   He said that he had had
 no skin affliction of any sort until two years before coming for examination,  when his hands broke
 out in a "weeping rash". He was not directly involved in the handling of platinum alloys or salts  at
 that time but in the course  of his daily tasks would  often enter the refinery.  He went to many
 practitioners,  registered and otherwise,  in an effort  to obtain a cure.  The condition which was
 mostly diagnosed as "nerves" or "eczema" had slowly regressed until it had become a dry, itchy
 rash on each hand and wrist.  He had,  for years, also suffered  from occasional acute attacks of
 asthma, and had consulted  many doctors for this.

       About a  year before being interviewed,  he had first worked on platinum refining, without
 incident.  About nine months later he noticed one day that his  face was red and itchy.  Next day it
 began to "weep" and took several days  to  heal.   A few weeks later,  the same sequence of  events
 occurred,  and a fellow workman suggested to him that exposure to platinum  salts might be a causa-
 tive  factor.

       Although he handled platinum alloys constantly in the interim,  the patient then avoided platinum
 refining for six weeks until the day of interview,  when, after only 10 minutes' exposure in the refinery,
 he noticed  facial itch and swelling  around  the eyes. He stopped work after about half an hour, but
 "little blisters" formed on  his forehead,  and they began to "weep".  He  put hot towels and  "Vaseline"
 on his face in an effort to gain relief, and after an hour he left work feeling "shaky".  Soon after  his
 arrival home he vomited, then went to  bed,  and having drunk a glass of  beer,  he slept fitfully.

       Six hours later,  when I saw him,  the swelling had largely subsided, but he had noticeable
 infraorbital oedema and some blotchmess of the face.  The itch had almost disappeared.   He had no
 further shakiness, and his hands were  unaffected.

       In late October  1969, he was  interviewed again, and said that he had worked in a different
 department in the meantime, almost completely detached from precious metals.   His general health
 had improved.   The hands and wrists had  completely  cleared, his face showed no swelling, and the
 asthma had been "mild"--that is,  one attack in four months.   There were no patches of eczema any-
 where on his body.

       For two  months after that  hu was free of skin troubles and in good health,  and then, about the
 beginning of December 1969, he went a.s usual into the refmeiy, which he was, in the habit  of entering
 once a week to  make a complex gold salt--potassium-gold-cyanide.  Unknown  to him on this occasion,
 the refining and filtration of platinum salts were in progress.  Soon after this, his face broke out
 again, with "little pimples" over the forehead and cheeks.  The  skin was itchy, red and swollen.
 The "pimples" dried up over the next three or four days.  His neck was  also affected, and the same
 thing occurred at his wrists.  At the time of the interview, a few small, dry patches  remained on
 his wrists.

       Since that time he has continued to work away  from the precious  metal refinery, and has been
 untroubled  by skin complaints except on one occasion,  when, according to the  firm's chief chemist,
 he was again exposed,  unknown to himself, and a similar series of events occurred.

       Parrot (1969) reports the following cases  from France:

       Case 1. --A 50-yr old man was assigned directly  to the platinum  refining workshop in January
 I960.  No personal nor hereditary history of allergy was present.  After two months, an erythemato-
vesicular,  prurigmous  dermatitis of the eczema type  appeared on the anterior face or wrists and


                                              A-25

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under the  action of intravenously administered adrenocorticotropic hormone.

       Back to work, he had asthmatic attacks treated with aminophylhne (theophyUmc ethylened.a-
mm.)   H" r£»,red another month of hospitalization for asthma.  The dermatosis finally vanished.


                                           ^

                                         ^^^

                                        ^^
attacks when he met people from that workshop.

        Case 2 -A 45-year old man was taken on ,n July 1964  for the manufacture of chloroplatinatcs.
He had no personal no/family history of allergy.  After eight months' latency  bouts of nocturna!
asthma occuired.  These were treated with mamcmoloncdiacetate and aminophyllme  Over one
mo  1   the  asthma gradually worsened.  Attacks occurred dur.ng work, more specially during the
"ydrolV ». o, croons.  Then the subject exhibited dyspnea mght and day.  Despite ^Ptornatic
treatment  the dyspnea increased with more or less violent paroxysms.  A one-month work stoppage
hrothcomplete recovery. Forty-eight hours after return to work this man had a very severe
attac"  of  a'thma  was transferred to another workshop, and has remained asymptomatic since then
Cutaneous tes7s were negative but nQ test with chloroplatinate or chloroplatinic acid was carried out.

        Case 3 --A 52-year-old man waa employed in 1958 to manufacture chloroplatinic acid.  For
one year  there was no trouble. Then cutaneous prunginous ecjematoid lesions appeared on the  fore-
. rn   elbow  folds,  face,  and  neck.   Hydrocort.sone acetate ointment l^™*^™™^^
dcimatitis  over the weekend, relapse occurred on Monday when work was resumed.   Platinum salts
test" we  e  Lhly Po.,t,ve.  Hyposensitization to chloroplatinates and chloroplatmic  ac.d was per-
  "•med without appreciable result:   epidermal reaction wrth 1/1,000 platinum chloride  solution ,t.U
 y°eE  d : zcma  "This man could carry on with the same work unt,l 1962 when ho was transferred to
 another workshop v.herc pallad,um was extracted from .olution. containing various  precious  metals
 amo Kthem, lltinum.   Under those conditions slight eczema persisted.  In 1964, the actory was
 m™v"d o a new ve.y modern buildma.  The worker was assigned to chloroplatinate  calcination   A
 'Terahzed Bc.oma  immed.ately occurred,  with m.htly attacks of asthma.  The asthma pers.sted and
 attacks occurred several times a day, a violc-it attack  required hosp.tahzation.

        This worker  resumed  his woi k in May in anothoi workshop  where he no longer  had contact
 with platinum salts.  Eczema remained  cured,  but slight asthma persisted, triggered by irritating
 vapors or by the  presence of workers Ijom the platinum relimng shop.

        Case  4  --A Zi-year-old man was assic,ied to the platinum workshop.   Two months later,
 pruriRinoua erythema appeared on the forearms,  elbow folds,  armpit.,  and mterdigital spaces
 D."m.t"ti. -mproved on Saturdays and Sundays but  -ecurred Mondays.   For the two  "b.oquent
 monL.  I..l0n.  reached  the neck,  groin,  and chest.   The alternate application of h^oc^SOne
 ointment and acid paste,  as well as intiamu.cularly injected cortisone acetate, brought a complete
 cure  although the patient did not mterrupt hi, wo, k.  After e,Bht days, ^rmatit.s recurred.  Then.
  subsequent to slight choking following the  accidental inhaling of a few  puffs of  chlorine, diy cough
  and th4en attacks  of asthma started.  At the hospital, cutaneous tests with ^^f^^f ^
  ammonium and sodium chloroplatinate were h,Rhty pos.twe:  chloroplatinic ac.d tests in 1 / 1, 000
  dUuTon  .ore followed by an ep.dormal  reaction,  then a tremendous cutaneous reaction, so we had to
  rlmove  the patch right away.  Solutions of more dilute chloroplatmic  acid and chloroplatmates were
  also  positive.  Hyposensit.zat.on was not done.  Permanent dyspnea developed  exaggeiated by
  activity. This required many days away from woik.  T.anafcr to  another job brought  a complete
  cure.
         Case 5 --A  19-yeai-old man was  employed on March 16. 1964, at platinum lefimng. After
  six months on this job, some attacks of asthma occurred  at mght.   They did not occur  at work   but
  dyspnea was permanent and breathing  remained wheezy.  Weekly wo. k  stops for two days would
                                                A-26

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 cause complete recession of respiratory signs.  Sometimes  before the onset of asthma this worker
 exhibited eczematoid dermatitis on wrists, forearms, face,  and neck.  He was treated with topical
 applications of corticoids and ammophylline suppositories.   Despite epidermal reaction tests showing
 allergy to chloroplatinates,  chloroplatinic acid, and rubber, no hyposensitization was  started.  During
 military service this man was hospitalized, then discharged for  asthma and allergic eczema.  When
 back at work, he was assigned to another workshop; asthma  did not recur,  but eczema persisted.
 Finally, this man had to leave the factory.

        Case 6. --A 23-year-old  man was employed at the test laboratory where chloroplatinates were
 calcined.  After seven years, he found that skin contact with such products triggered a nettle-rash
 reaction after one  minute latency which lasted about two hours.  These phenomena became more
 severe: as soon as he walked into the laboratory, conjuntivitis, allergic rhinitis, asthma,  and edema
 of the eyelids appeared for half an hour. Transfer to another department produced complete cure.

        Case 7. --A 27-year-old  man was employed at the chloroplatinic acid workshop.  Three months
 after starting this  work, he exhibited eczema of wrists and forearms, then of the neck.  Fifteen days
 later, while dermatitis remained, bronchial asthma occurred nightly  and did not stop for four  or five
 days.  Bouts of asthma also occurred during work.  Transfer brought cure after one month.   Now
 this man can even  walk into the platinum workshop without trouble.

        Case 8. --A 30-yeai -old  employee in the chloroplatinate workshop for five months developed
 eczema on his upper limbs extending to the shoulders; he did not stop working.   Since  he did not
 touch chloroplatinates  any longer, he remained cured.

        Freedman et. al.  (1968)  report the following case from  Canada: Dr.  T. T. ,  a 34-year-old
 inorganic chemist  on the teaching staff of a large university  in the Montreal area,  consulted  one of us
 (S. O. F. } in April 1967, because of possible allergy to platinum salts.  His history was that he had
 worked with platinum compounds for about  10 years..  During the previous 3 years,  he  noted  that
 whenever he came in close contact with platinum salts he would develop acute rhinitis  and asthma.
 His symptoms became  progressively worse,  finally reaching a point where he could  no longer  enter
 his own laboratory without experiencing severe cough, wheezing, and shortness of breath.   On one
 occasion, a solution of ammonium chloroplatinate  was accidentally splashed in his face by  a  co-worker
 in the laboratory.  Almost immediately, he developed massive angioedema of the face  and  acute genera-
 lized urticaria which required epinephrine and steroids for control.

       The patient was admitted to the Montreal General  Hospital during an asymptomatic  period for
 detailed investigation.   In the allergy history, .t was  determined that the patient had suffered from
 mild ragweed hay fever for many years and that his daughter had infantile eczema.   Otherwise, he
 was  completely free of atopic symptoms, except when exposed to platinum salts.

       Complete physical examination was within normal limits.  The resting blood  pressure was
 recorded as  140/80 mm Hg.  A chest x-ray wa^ reported as  showing no evidence of pulmonary, cardiac,
 or pleural disease. Respiratory function studies showed  normal values for the vital capacity,  timed
 vital  capacity,  maximum breathing capacity, and >naximum  midexpiratory-flow  rate.  The electro-
 cardiogram was within normal limits.  Thus, theie was no evidence for underlying pulmonary or
 cardiac disease which may have  been aggravated in a nonspecific fashion by inert dust  particles.

       Routine intradermal  allergy tostb showed modeiate positive reactions to house  dust and rag-
weed.  There was no peripheral  blood eosmophilia.

       Marshall (1952) reports  from South Africa:  Mr. D.  B.  S. ,  a European male aged 25, was
first seen in July 1951  when he complained of a rash affecting his left  thigh, hands and face.   He gave
no history of any previous skin or allergic disease and there was no family history of allergy.

       He had worked  as a  laboratory assistant foi over a year and had been employed intermittently
during the previous eight months  in the preparation of a platinum catalyst.   Part of this process con-
sisted of the deposition of platinum  metal on a base; and this was accomplished by evaporating chloro-
platinic acid over  hot plates in an exhaust-ventilated fume cupooard.   The fluid had,  however,  to be
stirred by hand and the operator was bound to inhale a certain small amount of fumes and to  have his
hands contaminated by  the acid.
                                               A-27

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       In March 1951, about four months after he had first begun work on this process,  the patient
began to experience attacks of 'tightness of the chest1 while at work.  He felt 'as if no oxygen were
reaching the lungs'.  At  the same time his eyes and nose watered and he soaked his handkerchief
many times in a day.  The attacks worked up to an evening climax,  but had passed  off by the next
morning.  On one occasion he was off work for a week with 'bronchitis' which he considers to have
been a major attack.

       One day in June 1951 he wiped his work bench clean of chloroplatmic acid (concentration unknown)
with his handkerchief.  The next morning there was a patch of erythema on his left thigh, corresponding
to his trouser pocket where he kept his handkerchief. Two weeks later a rash appeared on the dorsa
of both hands; and about  ten days later still the face became affected.

       When first examined he presented a patch of erythematous,  oedematous,  scaling and  excoriated
acute dermatitis,  about  10 cm. in diameter, on the upper and anterior aspect of the left thigh.  The
dorsa of both hands  and wrists were similarly affected;  and there were similar lesions of both cheeks,
and oedema of the eyelids.

       Patch tests of the substances  used in his work were applied  to the anterior surfaces of the
forearms and the following  results were obtained:

             1% Hydrochloric acid:  Negative after 48 hours.
             1% Nitric acid: Negative after 48 hours.
             1% Chloroplatmic acid:   Positive 4-plus (bullous reaction) in less than 24 hours.

       Removed from work and treated only with bland applications, the patient rapidly recovered
from his dermatitis and  had no further asthmatic attacks.

       Hunter, et. al. (1945) report  the results of an investigation  of workers in four platinum
refineries in Great Britain:

       Case 1.--R.C. ,  act. 58,  research chemist,  worked a refinery A from  1907 to 1924 (18 years).
From the first year at this work he noticed a tightness of the chest  witha wheeze when certain pro-
cesses in the refinery which caused a spray were in operation.  He noticed a tightening also in the
muscles of the back and  marked  sneezing.  There was a watering of the eyes and a dislike of light.
He would  go home and go straight to bed, and would wake up in the morning quite fit,  only to repeat
the same  symptoms the next day. He was forced to leave the refinery in 1924 because the symptoms
became so bad he could no longer carry on.  Since then he has  been perfectly well.  On one occasion
he returned to the refinery on business and immediately noticed a tightness of his chest,  even though
the process to which he was sensitive was not going on in the room.  However,  it was discovered
that sodium chloroplatinate had been  weighed out in the room about  half an hour previously.  There
was no family history of asthma.  He  now showed no abnormal  physical signs.  His blood count was
4, 160,000 red cells per  c. c. , haemoglobin 111 percent,   (photoelectric estimation of alkaline
haematin  100 percent., equivalent to 13.8 gm. haemoglobin percent.), white cells  12,200, poly-
morphs 61 percent., small lymphocytes 6 percent,  large lymphocytes 27 percent,  large hyalines
6 percent.  Dr.  D. Jennings reported on an X-ray  of his chest--old  bilateral apical infection with
fibrosis and drawing upward of both hila, emphysema of both  bases.

       Case 2. --A. W.,  male, aet.  38, started work at the age of  15  in a chocolate manufacturing
factory.   He worked here for 6 months and then transferred to  platinum refinery A.  After six years
on this work he noticed that when certain processes were  in operation  his nose started to run and he
would start sneezing.  This lasted for half an hour.  The symptoms  gradually got worse and  after
ten years he began to get tightness of his chest, shortness of breath,  wheeze and cough,  but he
produced  no sputum. He never had an attack at home.  The attacks  gradually got more frequent
and more severe, and two months before he was  interviewed  he was moved to the "other precious
metals" department. Since this  move he has not had further  attacks.  He had had no previous
illness, and there was no family  history of asthma.  On examination no abnormal physical signs
were found, except that when he  painted a 3 percent solution of sodium chloroplatinate on his  fore-
arm a large wheal appeared.  His blood count showed 5, 120, 000 red cells,  100 percent, haemoglobin
(photo-electric estimation), 11,200 white cells, 50 percent polymorphs,  41 percent,  lymphocytes,
3-5 percent eosmophils, 5.5 percent monocytes.  X-rays of his chest  showed emphysema.

-------
        Case 3. --E.  V.  N. ,  chest,  assistant manager of wet process at refinery B, aet.  28,  had
 worked for five years in the laboratory and for 2-1 /2 years as assistant manager of the wet process.
 Immediately he started  on the process he became aware that if he entered the room where ammonium
 chloroplatinate was dried  his nose started to run, producing perfectly clear fluid.  He would  soak
 three handkerchiefs in an  hour.  He would develop severe sneezing attacks and some irritation of his
 eyes.  After he had been there three months these symptoms were followed by tightness of the chest
 which would last for half an  hour, and wheezing which lasted 5 hours.   He would be awakened in the
 early hours of the morning with a cough which might last an hour, but the  following day he would be
 quite fit.   He had had no previous illness, and there was no family history of asthma. He entered
 the drying-room on the  day he was  interviewed and  was observed in an attack.   He was cyanosed,
 dyspnoeic and had an audible wheeze.  His respiration rate  was 34.  He had no clubbing of his fingers.
 His chest moved evenly, was hyper-re sonant with normal air entry but many sibilant rhonchi through-
 out.  There were no other abnormal physical signs.   His blood count showed 6,350, 000 red cells,
 130 percent, haemoglobin (photo-electric estimation), 8200 white  cells, 60 per cent, polymorphs,
 30 per cent, lymphocytes, 5 per cent, eosmophils,  1 per cent, basophils and 4 per cent,  monocytes.
 X-ray of his chest revealed  no abnormality.  During the attack he was given 10 minims of 1/1000
 adrenalin intramuscularly, but it did  not produce any relief of the symptoms, though it raised the
 pulse rate from 80 to 120.

        Case 4. --L.  J. , aet. 36,  process hand, worked 7 years at a chemical  plant and then  for
 14 years at platinum refinery  B on the wet process  and in the 'other precious metals' department.
 During  the past 3 years  he had had attacks of running nose,  sneezing,  shortness of breath,  tightness
 of the chest, wheeze and cough.  He was frequently awakened by attacks of coughing at 2  a. m., and
 had had such an attack every night for the three months previous to his sick-leave which  had  lasted
 3 weeks at the time of interview.  He had never had any attacks while away from the works.  He was
 moved to  the time office, but still got some attacks, and was therefore transferred to another depart-
 ment where he would not be exposed to the salts of platinum.  He had had pleurisy at the  age  of 8,
 and had his tonsils removed  1  year  previously because of his asthma.   There was no family history
 of asthma.  When examined he had not been at the refinery for three weeks, so he appeared a healthy
 man, and showed no abnormal physical  signs.  His blood count showed 4, 760, 000 red cells, 104 per
 cent, haemoglobin (photo-electric estimation),  7450 white cells, 57 per cent,  polymorphs,  1.5 per
 cent., eosmophils 39.5  percent lymphocytes  and 2 percent, monocytes. Dr.  M. H. Jupe reported  on
 an X-ray  of his chest as follows:  "There are a few scattered calcified nodules over the lung  fields.
 The hilar shadows are well seen,  but not excessive. "

       Case 5. --M.  D.  , female,  aet. 20, had worked as  a  press operator before entering  platinum
 refinery C; 3 months before  her interview she was observed sieving spongy platinum without  exhaust
 ventilation or mask,  and was seen to be without any symptoms.  She said that when she handled the
 dry complex salt her eyes  and nose  would run,  and she sneezed continuously.   She experienced some
 tightness of the chest the same evening, but this never woke her at night.  She had never  been ill,  and
 had no family history of asthma.   On examination she had no abnormal  physical signs.  Her blood
 count showed 4,500,000  red  cells, 98 per cent, haemoglobin (photo-electric estimation),  12, 000 white
 cells, 58 per cent, polymorphs,  2 per cent,  eosinophils, 3. 1  per cent, lymphocytes, 6 per cent.
 monocytes.  X-ray of her  chest revealed no abnormality.

       Case 6. --A. A. , chemist, aet. 33, for past 4 years had been in charge of platinum refinery
 D.  For 12 years  before that he had been an analytical chemist. He had no symptoms except  when he
 treated  the filtrates with granulated zinc, tins caused effervescence and droplets containing complex
 salts to be thrown into the  atmosphere.  Then his nose ran and he  sneezed. This might last for half
an hour.  He had no tightness of his chest, shortness of breath, cough or wheeze.  He had had scarlet
fever as a child,  but there was no family history of asthma.  On examination, apart from a very mild
degree of  funnel chest, he  had no abnormal physical  signs.  His blood  count showed 5, 950, 000 red cells,
 118 per cent,  haemoglobin (photo-electric estimation), 7000 white cells, 60 per cent,  polymorphs,
 36 per cent,  lymphocytes.  1  per cent, eosmophils,  and 3 per cent, monocytes.

       lexicological Information

Synopsis:

             Platinum:

             Exposure to complex platinum salts has been shown to cause  allergic symptoms of
             asthma and dermatitis  such as wheezing, coughing,  running of the nose,  tightness in


                                              A-29

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             the chest, shortness of breath, cyanosis, and itching of the skin, whereas exposure to
             dust of pure metallic platinum causes no symptoms.  People working with complex
             platinum salts are often troubled with dermatitis.  This does not appear to include
             the complex salts of other precious metals.

             Palladium:

             Toxicity is low.  This  metal, in the form of palladium  chloride, has been administered
             orally in dosage of about 1  gram daily in the treatment of tuberculosis.  These amounts
             resulted in no toxic effects.  Applied locally to the skin,  palladium chloride shows little
             or no irritation.  In experimental animals,  palladium chloride has been given by
             intravenous injection,  producing damage to bone marrow, liver and  kidneys when the
             dosage was of the order of 0. 5 to 1. 0 mg per kg  of body weight.

       L,evene(1971) provides the following comments on platinum sensitivity:  Disease caused by
platinum worked into annular or trinket form  is not an everyday problem.  Dermatitis from metallic
platinum has apparently only been recorded in one patient (Sheard,  1955).  However, those concerned
in the refining or analysis of platinum are required to work with the complex salts of the metal and
it is these which give rise to a characteristic  syndrome.  The complex salts  are  sodium,  potassium
or ammonium tetrachloroplatmate or hexachloroplatmate. Apart from being essential intermediate
compounds in the refining and assaying of the  metal, they are used in the manufacture of platinum
sponge, a finely divided form of the metal which is  a most valuable  industrial catalyst.  Individuals
may work in an atmosphere containing these salts for periods of months or years without trouble,
but sooner or later the majority of workers will develop symptoms referable to the respiratory sys-
tem and/or the skin.

       The respiratory symptoms were clearly described in a classic paper by Hunter, et. al.  (1945)
and consist of rhinorrhoea, sneezing, cough,  tightness in the chest, wheezing,  shortness of breath
and cyanosis.  In short, they resemble a mixture of hay fever and asthma.  Symptoms can arise
within minutes  of exposure.  In the  patients  reported by  Hunter, et. al. ,  52 of  91 employees who
worked  in platinum refineries in the London area had the asthma/hay  fever syndrome to a significant
degree.  Thirteen of the 91 had a skin eruption of scaly erythematous type but a few had urticanal
lesions.  Jordi (1951) in Zurich described 3 cases in which asthma followed inhalation of platinum
salts and immediate urticaria followed splashing of solutions  on the neck and forearms. One case
produced a cutaneous weal within 2  min.  of painting with  a 3% solution of sodium  chloroplatmate but
the responses were not clear-cut.   Roberts (1951) in Malvern, Pennsylvania investigated reactions
seen in  employees in a platinum laboratory and refinery over a period of 5 years.  He coined the
term "platmosis" for the syndromes he encountered.

       He noted that once disabling symptoms arose in any one case that person  never  again became
asymptomatic in a platinum-containing atmosphere.  His observations concurred exactly with the
other reports, and it was advised that sufferers from the  effects  of  platinum  salts should be trans-
ferred to other work.   Five cases with both asthma and eczematous dermatitis have been described
from Pans by  Parrot,  et. al. (1969), in. a study of 51  subjects 3b had symptoms  of platmosis.
Freedman  and Krupey (1968) report a man with the respiratory syndrome who developed massive
angio-oedema and acute generalized urticaria following accidental splashing of ammonium chloro-
platmate solution on  the face.

        Roberts carried out scratch tests with aqueous solutions of sodium chloroplatmate on 60 plati-
num workers.  He found that all subjects developed  a one plus ( + ) reaction with a 1:10 dilution of the
salt. Following the onset of symptoms,  either of the cutaneous or respiratory type, a reaction was
always  obtained with a 1:1000 dilution.  He decided that  initial scratch-testing was an unreliable
index of liability to develop future symptoms and he claimed that a person with a strong personal or
family history  of atopy or of contact dermatitis was more likely to  succumb to platmosis than others.
However, he believed that individuals with moles, acne  or sebaceous cysts were also particularly
prone to the condition.

        The elicitation of an immediate skin weal and symptoms resembling asthma and hay fever
after exposure to complex platinum salts suggest that either a pharmocological or an allergic hista-
mine liberating process is operating.  Parrot, et.  al. (1963) injected sodium chloroplatmate solution
intravenously into normal guinea pigs and found that when a sufficient dose was given,  the animal
                                               A-30

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 developed intense asthma and died witlnn a few minutes.   Smaller closes provoked non-fatal asthma,
 and if the dose was repeated several times the effect became successively less intense.   Complete
 protection against such asthmatic episodes was  afforded by prior injection with the antihistamine
 drug mepyrdmine.  From these observations and further experiment!, using isolated guinea pig ileum
 in vitro,  the authors concluded th,;t platinum salts .let as powei fill histamine  liberators in the guinea
 pig.  However, despite those findings it seems clear that  the clinical syndrome of platinosis in man
 is Largely the result of hyper sensitivity to platinum salts.  Evidence in favour of  this contention is as
 follows-  (1) workers do not have symptoms initially, the syndrome comes only after months or even
 years of exposure to the salts,  (i) symptoms increase  in severity with repeated exposure, (3) cutan-
 eous scratch tests to platinum salts at a. dilution of 1 1000 become positive with the onset of symptoms
 when they had been previously negative (Rulicil<>, 1951), (I) [missive transfer tests (Prausmtz-
 Knitner  reaction) using patient's icruni have been positive using both the platinum salt alone  and in
 conjunction with human sciuni albumin (F reocl.ii.in .incl  Kruucy,  !%H).

        It is  worth pointing out that scratch 01 ml i 'ide1 :nal testing can be hazardous to the point of
 being life-threatening  in these patients.  A single inti ade i mal teat using potassium hexachloroplati-
 nate at n concentration of 1 ng/ml produced an .iii.ipliylac tic leactiori in  the patient of Freedman
 and  Krupey (1968). It is WISP for these patients  to be pi otected by systemic antihistammc prior to
 skin testing.

        It h.is hitlieito  been  recommended th.it pat lent a  with platmosis should change their occupation.
 rhcie is no  doubt that this management is effective sine*,  symptoms resolve rapidly when the patient
 is i cmoved from exposure to platinum salts.  I lovc-vc. i, since the main components of the syndromes
 of sensitivity to platinum salts are those f>l an hype rsi.nsitivily rfspon.se.it uould  seem reasonable
 to attempt hyposensitixation by  pi ogressively increasing mtraderm.illy injector) doses  of  platinum
 s.ilt in ?i  way analogous to that employed using p(ill<_n in hay fever  (FranUland, I9(>5),  and strepto-
 mycin in cases of immediate liypc-rsensitivitv to  tins ding (Cohen, 1954; Levone and Withers,  1969).

        •Successful hyposcnbitization was rcci nliy .ichicvud in an analytical chemist who exhibited
 typical severe symptoms of li.iy fevei, asthm.i .mil contact urticaria when exposed to platinum com-
 plex salts in the course of his work (Lcvene and  Calnan,  1971).  Starting with a dose of 1 0 ng he was
 i;iven inci easing doses of ammonium he\cirhloi oplatmale intrade rmally several times  daily for a
 month.   Immediate symptoms wcie weal and ll.tr>.  at the site of injection, and wheezing and flushing,
 v hich usually passed off within  30 minutes. On the twelfth day  of the course of injections he began to
 develop crops of widespread symmetrical cM-ythcm.Ltous, papules and joint pains coming on 2 hours
 afte i  injection, i.e. he developed a seium sicKness-likc  reaction.  Histology of the papulcr showed
 in intense perivascular infiltrate of polymoip! ~i ..irluji luukocyte.s--mainly eosmophils.   The  injection
 sites at first produced veiy pjom-nent \A ea.lt, aid ll.uos but these tended to diminish with  increasing
 doses.  At fust the weals laded lapidly with  no sequelae but later in the couise,  with higher doses,
 the injection sites developed pinkish-brown ln.der papulea rfftei the initial weal had subsided.   With
 the highest injected dose (100 jig), the injection bilv. became very tendei  and  nccrotic after i days.
 The appearance resembled the Aithus pln-nom jnon as seen in experimental animals.  An  injection
 of this dose into A normal subject pioduced omy  . slight tiansienl reaction at 24 hrs.  By this time
 it  was  found  that the patient coulci carry oul his usual woj k and handle  ammonium bcxachloroplatmatc
 without the hay fcvei anil asthm.i symptoms and  uiticaria which had previously partially disabled
 him.  He remained well while uui-Kini> with he •w.ichloi oplalinntc although a chance exposure to tetra-
 chloroplatmatc produced symptoms, hiiygehling that his  reduced sensitivity was specific for the  hexa-
 chloroplatinale.   A furthei chaptei in Ins pathology occurred nftei he stopped working with platinum
 salts for  about 3 months.  When he w.is ai-.iin exposed he  found that he had partially relapsed,  and he
 j -v[uired  i e.idmission to hospital for a furthei conisi, of injections.  Since then, he has had continuous
 e\posuie and has remained well.

       It is of interest to ciinsidi.i  the nu-chaiiisiii of his liypersensitwity and its  amelioration by the
 technique of  hyposensitization.  It is postulated lhat the ofYgirial symptoms were  mediated by
 icaginic (IgK) antibody and that  injections of the platimnn salt stimulated production of IgC (blocking)
 •i ut i body which combined pn:leri:iilially with the  antigen to pi event anaphylactic symptoms.  The
development of a  scium sickne.ts-like and Ai thus-like reaction during hyposensiti&ation give  support
to this hypothesis smee then-  is evidence  that suih reactions me caused by immune complex foima-
tion involving precipitating .intibndy (Crc.un and Tuik,  I°7I).  Although specific  IgG antibody was not
directly dumonstrable  in this case by double diffusion in agar 01 by haemagglutmation  using either
the platinum  salt alone or in conjugation \\. ith human scium albumin , it was found that intraclermal
                                              A-JI

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injection of the platinum salt incubated with post-hyposensitization serum gave a much smaller weal
and flare than salt incubated with pre-hyposensitization serum.   This  indicated that post-hyposensiti-
zation serum had acquired the ability to block the immediate weal and flare response and it seems
very likely that newly formed IgG antibody was responsible for this blocking activity.  The platinum
salt presumably acts as a hapten which combines with an endogenous protein to form  an allergenic
hapten-protem complex.  A likely candidate for the protein concerned is serum albumin as  suggested
by Freedman and Krupey (1968).  Although it has been assumed that the anaphylactic  symptoms in
these cases are  the  result of IgE antibody, it has recently been shown (Parish,  1970) that IgG antibody
can have limited anaphylactic activity.  However.  Parish confers ,t unlikely that anaphylactic IgG
could participate in  the classical reagm-mediated reactions-asthma, hay fever, or urticaria--that
occur within minutes of exposure to antigen.

       The situation with . egard to the eczematous dermatitis in response to  complex platinum salts
as described by several authors ,s less clear.  It ,s qu.te  likely that allergic contact sensitiv.ty can
occur but this has not yet been convincingly proven by patch tests in appropriate cases.  Allergic
contact sensitivity is a  delayed hypersensitivity reaction, and the situation ,s complicated by the well-
documented ability of these salts to produce urticaria on contact.  It is not even clear what is an
appropriate concentration  to be used for patch testing.   For a patch test to be valid it must, of course.
be shown that the chosen concentration does not produce an irritant reaction in control subjects (Bet
and Calnan, 1957).  Complex salts of platinum are not readily soluble >n distilled water, but solubility
,. improved ,f physiological salmc ,. used.   They dissolve m dilute hydrochloric acid but such solu-
tion? are probablv not suitable for patch testing.  These problems remain to be resolved.

        Although platinosis is a rare disease outside platinum refineries, recent reports indicate that
platinum  salts may  be of value in cancer chemotherapy (Rosenberg, et al. . 1969. Harder and Rosen-
bere   1970)   Platinum  compounds have  not been widely used as therapeutic agents despite an earlv
report that they were "very effective" in syphilis and rheumatism (Hoefer. 1841).  If these com-
pounds do come into generalise, one can anticipate that allergic reactions to them may be seen.

        Schroeder  et  al.. (1971) report on studies of the innate effects of low dos.es of abnormal
trace elements  in drinking water on mice and rats  exposed for  life, conducted in an environment
built so as to exclude metallic contaminants:

        In order to evaluate  possible innate toxic effects of small doses of rhodium and palladium in
teims of growth and survival, mice divided as to sex were raised in  an environment limited in
metallic contamination  and given 5 PPm metal in drinking water from  weaning  until natural death.
Body weight was measured at monthly intervals up to 6  months, at 1  year and at 18 months of age.
The feeding of palladium was  associated with growth suppression  at 7 and of rhodium at 6 of 16 intei-
vals compared to mean weights of controls.  Survival of palladium-fed males was greater  than that
of controls.   Tumors were found at  necropsy in 16.3% of  one group of controls, 28. 8% of the rhodium
and 29 i% of  the palladium groups.  Malignant tumors were increased in rhodium and palladium
groups  at a minimally significant level of confidence (P < 0. 05),  all but one  tumor being malignant.
In a second series,  tumors  were present in 26. 8% of controls.   All tumors in these  latter  groups
wore mal.gnant.  Rhodium and palladium appear to exhibit slight carcinogenic activity in mice.

        Spikes,  et.  al.  , (1969) report on experiments of enzyme inhibition by palladium chloride-

        In the course of examining palladium  poiphynns as  possible sensitizers for the photodynamic
 mactivation of enzymes, it was observed that palladium ( + 2) inactivated tryps.n directly by a non-
 photochemical process. Although palladium  (KJ) has been shown to bind to proteins  such as carboxy-
 peptidase,  casein,  papam and silk  fibroin,  and to mterfe.c with plant growth, reports were not
 found in the literature  on it, action  as an enzyme inhibitor.  For this reason  a preliminary examina-
 tion of the effects of palladium (+2)  on several enzymes was carried  out.

        Of the enzymes listed above, only chymotrypsin and trypsm were inactivated by palladium (+2).
  The mactivation was time-  and pH-dependent.  Trypsm was very rapidly mactiviated at pH 4. 2,  but
 was not inactivated at  PH 8. 9.  Alphachymoti ypsm was also inactivated  very rapidly at PH 4. 2,   but,
 in contrast to trypsm,  was  inactivated fairly rapidly at pH 8. 9.

        The mechanism of the mactivation of chymotrypsin and  trypsm by palladium ( + 2) is not known.
 Other metals (copper,  zinc,  mercury) in the divalent form also inhibit these enzymes;  mercury
                                                A-32

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 presumably inhibits trypsin by reacting with sulfhydryl groups.  It has been suggested that mercury
 may inactivate chymotrypsin (which has no free sulfhydryl groups) by forming a stable chelate with
 the active-site histidme.  Palladium (+2) binds to papaln with the same stoichiometry as does mercury
 (+2),  which suggests that, for this enzyme,  its binding is due to interaction with sulfhydryl groups.
 Palladium (+2) forms complexes with L-cysteine, L-cystme and L-methionine in solution, but not
 with L-histidine.  Thus,  one could  envision that palladium (+2) inactivates trypsin by combining
 with free sulfhydryl groups and/or  with cystine groupings, while the inactivation of chymotrypsin
 might result from reactions with cystine groupings.

        Wood (1974) reported recently:

        Platinum and palladium will be methylated in the environment by microorganisms.  These
 metabolic products could be more toxic than other forms of the metals.   Platinum and palladium were
 listed as  very toxic and relatively accessible.

        Summary of Medical and Toxicological Information

        Metallic platinum is non-toxic  and never gives rise to occupational injury.  The oxide causes
 eczema of the hands  and forearms and some lesions of the nails. Dust and spray fxom the complex
 salts  of platinum have been found to cause asthma after continued exposure.  The initial symptoms
 of the reaction begin with repeated  sneezing followed by  a profuse running of the nose with a watery
 mucous discharge.  Later reactions which may develop are tightness of the chest, shortness of the
 breath, with wheezing and blue coloration of the face.  When the operator leaves the work, the
 symptoms clear with the exception  of the persistent bouts of coughing in the  night which may endure
 for about one-half hour.  When the  work is resumed, the symptoms recur.  Certain typical skin
 reactions may also develop in some individuals;  this is  characterized by a scaly red rash.  Blood
 checks, skin tests,  and X-rays do not reveal any abnormalities  leading to the lesions noted.  Pre-
 cautions lie in minimizing the exposure by adequate means not to exceed a maximum  allowable con-
 centration of 2 ng per cubic meter for the soluble platinum salts. Treatment consists in removal
 from  exposure and consultation with a physician with a full-history of the exposure.

        Palladium salts commonly used are the chloride  and the  amino-nitrite.  So far as is  known,
 the palladium salts do not constitute any threat of injury in industry, but laboratory tests show that
when  these substances are introduced mammals, damage occurs to the heart, kidneys,  liver and
 bone marrow.  From  these indications, it would seem that palladium  salts should be carefully watched
 for chronic and cumulative toxic effects.

       The Environmental  Protection Agency has  efforts underway at EPA-Cincmnati on the toxicity
of platinum and palladium.   The results of these studies should provide substantial additions to the
toxicity data  presently available.
                                              A-33

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                          APPENDIX B.  ANALYSIS AND PROJECTIONS

  1.     End Use and Production Projections

        The projected forecast base for total demand of platinum and palladium was established for
  each of the end use categories. The  forecast bases were derived by relating domestic end uses of
  each metal in 1971  to the anticipated  growth  of such indicators as the gross national product (CNP)
  or total population, adapted from the White House Conference on the Industrial World Ahead- A Look
  at Business in 1990.  Relevant contingency factors, which would have a positive or negative influence
  on the  projected demand in each end use category, were then considered to obtain a high and low range
  of demand.  The aggregation of these internal ranges for each end use  category constitutes the
  median,  low and high forecast ranges in the  years  1980 and  1990 for platinum and  palladium.

        In the rest of the world, the demand  for platinum catalysts in the petroleum industry is
  increasing more rapidly than  in the United States as the use of platinum in  reforming processes to
  produce higher octane  motor fuels  is  being adopted.  Rest-of-the-world growth in chemical uses  will
  probably increase fairly rapidly as the demand for fertilizer materials increases.   Within the electric
  industry,  where palladium is  used, the move to electronic and other means of switching may result
  in a relatively slow rate of future growth in the  rest of the world.  Demand in dental, medical, glass
 and jewelry applications in other countries will  probably grow at rates approximating those in the
  United  States.  Based upon these considerations, the rest-of-the-world demand for platinum is
 expected to range between 1.565 and 2.087 million ounces in 1980 (with a median of 1.826 million
 ounces),  and between 2.317 and 3.089 million ounces in 1990 (median,  2.703 million ounces).  The
 growth rate corresponds to 4.0 percent. The rest-of-the-world palladium demand  is expected to
 range between 1. 182 and 2. 128 million ounces in 1980 (median,  1.655 million ounces).  In 1990,  the
 range is projected from about 1. 750 to 3. 150 million ounces at a median of 2.450 million ounces.
 The median growth  rate corresponds  also to  4.0 percent.  The following Tables B-l and B-2 show
 the domestic and rest-of-the-world forecast  ranges of demand for platinum and palladium.  Tables
 B-3 and B-4 present forecast  bases for each category of end use.

                    Table B-l.  Forecast Range of World Demand for Platinum
                                        (thousand troy oz)

                                                      1971        1980        1990

United States


Rest-of-the-world

Total world demand
estimate

high
median
low
high
median
low
high
median
low

541
	
	
1283
---
1824
	
1900
1508
1141
2087
1826
1565
3987
3334
2706
2442
1910
1453
3089
2703
2317
5531
4613
3770
              Source:  Mineral Facts and Problems 1970 and Southwest Research
                       Institute

       The projections for platinum and palladium in  catalytic mufflers are based on an immediate
demand of 700, 000 oz  platinum and 300, 000 oz palladium, required at the original 1975 timetable.
The rest-of-the-world demands in 1971 are taken from Tables A-3,  A-4,  A-8, and A-9, where it was
shown that about 1.82  million oz of platinum and about 1.92 million oz of  palladium were produced in
1971. The projection of production figures to 1980 and 1990 are given in terms of requirements from
major producers on Table B-5.

       A  comparison of the 1975 production  objectives for major producing countries with the  pro-
jected world demand shows that a constant 1975 production rate for platinum  would meed the 1980
median demand, whereas the constant 1975 production rate for palladium  would not meet the 1980
median demand.  Based on the 1975 objective, it would appear that the world platinum production
needs to be increased by 2. 064 million  oz to meet the  1990 high demand projection, and by 1. U6mil-
lion oz to  meet the  1990 median projections.   World palladium production would need to be increased


                                               B-l

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                  Table B-Z.
Forecast Range of World Demand for Palladium
        (thousand troy oz)
                                                    1971
                                  1980
                                                                           1990

United States


Rest-of-the-world


Total world demand
estimate
high
median
low
high
median
low
high
median
low

760
	
	
1163
---
...
19Z3
...
1589
IZ30
78Z
Z1Z8
1655
1182
3717
Z885
1964
1919
1466
962
3150
Z450
1750
5069
3916
Z7IZ
             Source  Mineral Facts and Problems 1970 and Southwest Research
                     Institute

                Table B-3.  Contingency Forecasts of U.S.  Demand for Platinum
                                  by End Use,  1980  and 1990
                                      (thousand troy oz)
U.S.
End Us.: Demand
liyTnduatiy '.971
Chemical ,
(inorganic)
Chemical,
(organic)
I'eti oleum
Glass
riecti ical and
Electronic
Dental and
Medical
lew ell y and
Decorative
Miscellaneous
Automotive
Catalysts
Total (Rounded)
81

54
ill
41

52

23

18
20

541
U.S.
Forecast
Base 1980
1 17

60
365
59

58

Z5

i\
29
774
1508
U.S.
Low
1980
105

43
261
54

30

25

19
24
580
1 141
U.S.
High
1980
195

69
489
88

74

50

47
36
852
1900
U.S.
Forecast
Base 1990
177

67
551
90

64

28

23
44
866
1910
U.S.
Low
1990
159

48
394
83

33

28

21
37
650
1453
U.S.
High
1990
295

77
738
135

82

56

51
55
953
2442
     Souicu:  Minoial Facts and Problems 1970 and Southwest Research Institute

liy 2  106 mi Hi on 01 to meot the  1990 high demand projection, and by 1.343 million oz to meet the 1990
median projection.   Table A-l 5 showed that platinum reserves of major producing nations are estimated
as 215 29 million OB and palladium reserves as 179.02 million oz.  It would appear that the projected
demands for platinum and palladium can be met amply during the forecast period from  known reserves.

£.	Contingency  Assumptions

       Contingency  assumptions made to establish the U.S. forecast range of demand for each end use
in 1980 and  1990 arc presented below.

       Industr ,al Inorganic Chemicals. The forecast base in the years 1 980 and 1990 for this end use was
oUamed by  ielating the growth in demand for platinum and palladium to the growth in CNP which is
anticipated as 4. 2%  annually according to the White House Conference Board.  The forecast bases  of
demand for  platinum are  117,000(1980),  1 77, 600 (1 990) oz and for palladium 191, 000 (1980) and
289  000  (1990) oz   The chemical industry is a large consumer, especially for the production of nitric
aciri wh.ch ,s  used m tonnage quantities in the  production of fertilizers and exploswes.  With the steady
increase in populat.on as well  as demand for food products world wide,  there is a continuing demand
                                                B-Z

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                  Table B-4.  Contingency Forecasts of U. S.  Demand for Palladium
                                     by End Use.  1980 and 1990
                                         (thousand troy oz)
End use
by Industry
Chemical
(inorganic)
Chemical
(organic)
Petroleum
Glass
Electrical and
Electronic
Dental and
Medical
Jewelry and
Decorative
Miscellaneous
Automotive
Catalysts
Total (Rounded)
U.S.
Demand
1971

132

87
3
0.20

432

61

19
26

	
TbO
U.S.
Forecast
Base 1980

191

96
4.3
0.29

478

69

21
28

332
1230
U.S.
Low
1980

179

96
3.2
0.27

212

69

21
36

166
782
U.S.
High
1980

298

128
6.5
0.43

584

104

49
54

365
1589
U.S.
Forecast
Base 1990

289

108
7
0.44

534

77

23
57

371
1910
U.S.
Low
1990

271

108
5.3
0.40

237

77

23
54

186
962
U.S.
High
1900

452

144
10.5
0.66

653

1 16

54
81

408
1919
      Source:  Mineral Facts and Problems 1970 and Southwest Research Institute

              Table B-5.  World Production Requirement for Platinum  and Palladium
                           World Demand
                         (thousand troy oz)
                       1971    1980     1990
                                  Production Objective 1975
                                      (thousand troy oz)
                         Canada    U.S. S. R.     U.S.A.
        Platinum:
          high
          medium
          low
        Palladium:
          high
          medium
          low

1824
	
3987
3334
2706
5531
4613 217
3770

700 2550 3467
~~ "
1923
3717
2885
1964
5069
3916
2712
                           283
                                      1400
890
                                                              2573
        Source:  Southwest Research Institute

 for fertilizers.  The demand for explosives may increase due to increased activity in mining and
 quarrying operations and m  the construction of roads,  dams and reservoirs.  The present rate of
 growth for the chemical industry is about 10 percent per year. At this growth rate,  the high demand
 for platinum would be 195,000 (1980), 295, 000 (1990) oz and for palladium 298. 000 (1980) and 452  000
 (1990) oz.  More efficient use  of these metals or the use of alternate metals  in catalysts  for producing
 nitric  acid may  contribute to a low demand for platinum and palladium.  It is also possible that nitro-
 gen replenishment of the soil by direct application of ammonia will increase  substantially.  Addition-
 ally, the use of  mechanized  boring machines for mining and quarrying operations may reduce the
 demand for explosives.  These contingencies may  result in a low demand for platinum of 105 000
 (1980). 159,000  (1990) oz and for palladium of 179,000 (1980) and 271,000 (1990) oz.

       Industrial OrBanic Chemicals. The forecast bases in the years  1980 and  1990  were obtained by
 relating the  growth in demand for platinum and palladium to the anticipated growth rate of total popula-
tion at 1. 125 percent per annum, resulting in platinum  demand of 60, 000 (1980),  67,000 (1990) oz and
in palladium demand of 96. 000 (1980) and 108. 000 (1990) oz.  The use of medicmals proportional to
total population will probably rise due to  increase m longevity and an expansion  in Medicare  and other
health  programs. It  is also  anticipated that synthetic fibers will be used increasingly m lieu of
natural fibers.  Thus, the demand could reach highs for platinum of 69, 000 (1980),  77, 000 (1990) oz
                                               B-3

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and for palladium  128,000 (1980) and 144, 000 (1990) oz.  A low demand in this category may result
from the development of alternative processes for producing medicinals.  Moreover,  education may
result  in higher health standards achieved through preventive medicine.  New techniques in fabrica-
ting and producing synthetic fibers may reduce the demand for spinnerets made from platinum-group
metals.  Due to these contingencies, the low demand could be for platinum 43, 000 (1980), 48, 000
(1990)  oz and for palladium 96,000 (1980) and 108,000 (1990) oz.

       Petroleum  Refining. The forecast bases in this end use  are for platinum 365,000 (1980),
551, 000 (1990) oz  and for palladium 4. 300 (1980) and 7. 000 (1990) oz, obtained by relating the growth
in this  sectorto the projected growth of the GNP at 4. 2 percent  per annum.  Increased affluence could
result  in greater production of automobiles and other motorized recreation vehicles, and thus in
increased demand  for gasoline.  As lead is outlawed as a means of controlling antiknock characteris-
tics of gasoline and for rendering catalytic mufflers effective, platinum requirements may be sub-
stantially increased in the production of gasoline of higher octane ratings.  Based on the increased
mobility,  limitations on environmental pollution,  and other considerations,  the demand for platinum
could reach a high of 489. 000 (1980), 738,000(1990) oz and for palladium 6,500 (1980) and 10.500
(1990)  oz.  However, innovations in transportation such as the development of electric automobiles
or the  introduction of mass transit systems would severely limit the demand for gasoline.  In addition,
new techniques in  petroleum  refining or use of alternate  materials  for catalysts could reduce the
demand for platinum and palladium.  These contingencies could result in a low demand for platinum
of 261, 000 (1980),  394, 000 (1990) oz and for palladium of 3, 200 (1980) and 5. 300 (1990) oz.

       Class Industry.   The end use in this category was obtained by relating the growth to the CNP
at 4.2  percent per annum, resulting in forecast bases for platinum of 59,000 (1980), 90,000 (1990) oz
and for palladium  of 290 (1980) and 440 (1990) oz.  Concern over fire hazards could lead to increased
use of  fire-resistant glass fibers for carpeting and drapes by the domestic and industrial sectors.
Also,  tire manufacturers may adopt increasingly the use of fiberglass for belting in tires.  More-
over,  if there is a drastic change in transportation, fiberglass  belting may be used for conveyer-type
sidewalks.  Fiberglass will probably be utilized  increasingly in the production of boats,  snowmobiles
and car bodies. Based on these  assumptions, a high demand could result for platinum of 88,000
(1980). 135,000 (1990) oz and for palladium of 430 (1980) and 660 (1990) oz.  However, mass trans-
portation  systems  may  greatly reduce the  demand for automobiles.  Manufacturers may continue to
use aluminum in boats.  Moreover, natural fibers, chemically treated for fi reproofing, maybe
aesthetically preferred to  glass fibers.  These considerations could result in a low for platinum of
54, 000 (1980),  83, 000 (1990) oz and for palladium of 270 (1980) and 400 (1990) oz.

       Electrical  and Electronic Industry.  The forecast  bases  for  platinum of 58,000 (1980), 64,000
(1990)  oz and for palladium of 478, 000 (1980) and 534, 000 (1990) oz were obtained by relating the
growth in this end  use to the  projected growth rate of total population at 1. 125 percent annually.  Due
to affluence and the growth in population, communications equipment,  including telephone and tele-
vision, is expected to be in large demand.  It is  also likely that fuel cells which will utilize platinum
or palladium will be developed.  Moreover,  the reliability of platinum-group  metals as electrical
components will sustain their use in aerospace applications.  These contingencies could result  in  a
high demand for platinum of 74, 000 (1980), 82, 000 (1990) oz  and for palladium of 584, 000 (1980) and
653, 000 (1990) oz.  Conversely,  current applications,  utilizing these metals may decline.  For
instance,  the major use of thermocouples,  containing platinum, is currently in the  steel industry.
The production of  steel by the basic oxygen furnace requires fewer thermocouples than  production by
the open hearth and the electric furnace.   Demand for  spark  plugs with platinum contents in aircraft
engines is expected to decline due to increased use of jet propulsion.  Use of  other  metals in alloys
for magnet materials and increased use of solid  state devices for electronic switching will contribute
to a decline in demand for platinum-group metals.  These contingencies could result in a low demand
for platinum of 30.000 (1980),  33.000 (1990) oz and for palladium of 212,000 (1980) and 237,000
(1990)  oz.

       Dental and Medical Industry. The forecast bases  for  platinum of 25,000 (1980),  28,000 (1990)
oz and for palladium of 69, 000 (1980) and 77, 000  (1990) oz were obtained by relating the growth in
this end use to the anticipated  growth rate for total population of 1. 125 percent per  annum.  Affluence,
increased awareness of dental hygene and vanity considerations will probably result in increased
attention to orthodontic treatment and prosthetic dentistry.   Hence, the use of the platinum-group
metals in corrective devices for straightening teeth, dental plates, and supports may result in a high
demand for platinum of 50, 000 (1980), 56,000 (1990) oz and for  palladium of 104,000 (1980) and
116, 000 (1990) oz.  Conversely,  prophylaxis  either through teaching or through such means as  chemical
                                              B-4

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  treatment of drinking water with fluoride may decrease the need for dental plates or other  prosthetic
  devices.  These considerations could result in a low demand for platinum  of 25, 000 (1980), 28, 000
  (1990) oz and for palladium of 69, 000 (1980) and 77, 000 (1990) oz.

         Jewelry and Decorative Industry. The  forecast bases for platinum  of Zl, 000 (1980), 23,000
  (1990) oz and for palladium of 21,000 (1980) and 23.000 (1990) oz were obtained by relating the growth
  in this category to projected growth of total population at 1. 125  percent annually.  On the assumption
  of increased affluence and the desire for quality jewelry, the demand can be expected to reach a high  for
  platinum of 47,000 (1980), 51,000 (1990) oz and for palladium of 49,000 (1980) and 54,000 (1990) oz.
  However, changes  in style and taste may result in a low demand for platinum of 19,000 (1980), 21,000
  (1990) oz and for palladium of 21, 000 (1980) and 23, 000 (1990) oz.

        Miscellaneous Uses.  These uses include such applications as laboratory ware and brazing
  alloys containing the platinum-group metals.   The forecast bases for platinum of 29, 000 (1980),
  44, 000 (1990) oz and for palladium of 38, 000 (1980)  and 51, 000 (1990) oz were obtained by relating
  the growth in this end use to the growth in the  CNP of 4. 2 percent per annum.  The  forecast bases
  for automobile catalysts for platinum  of 774, 000 (1980), 866,000 (1990) oz and for palladium of
  332, 000 (1980) and 371, 000 (1990) oz were obtained by relating the growth  in this end use to the pro-
  jected growth rate  of total population of 1. 125  percent per annum.  The high  demand may be realized
  by the development of industrial anti-pollution devices  and  by fuels cells which may use platinum-
  group metals:  platinum 36,000 (I960), 55. 000 (1990) oz and palladium 54,  000 (I 980), and 81, 000
  (1990) oz.  The low demand in miscellaneous uses could be as the result of the substitution of alter-
  nate metals.  The low demand would be for platinum 24, 000 (1980), 37, 000 (1990) oz and  for palladium
  36, 000(1980)and 54, 000(1990)oz.

        The  low demand for catalytic mufflers in automobiles  may be due to alternate catalytic
 materials or due to different technical solutions to the emission  problems.  The low demand for
 platinum would be 580,000 (1980), 650,000 (1990) oz and for palladium 166,000 (1980) and 186, 000
 (1990) oz respectively.  The high demand could be  realized, if the alternate materials and technical
 solution would not be feasible.   These considerations could result in a high demand for platinum of
 852,000 (1980), 953,000 (1990) oz and for palladium of 365,000 (1980) and 408,000 (1990) oz.

 3.	U.S. Supply and Demand Statistics

        Table B-6 shows salient U.S.  platinum and palladium  statistics for the latest published year.

                  Table B-6.  Salient  Platinum and Palladium Statistics for 1971

                                                            Platinum        Palladium

          United States                                      (18,029)           	
            Mine production                                    	
            Refinery production                                	              	
              New Metal                                     10, 198            20,951
              Secondary Metal                               103,420          161,099
            Exports (except manufacturers)                 319,642            76,471
            Imports for consumption                        551t 127          657,983
            Stocks Dec.  31; refiner,  importer, dealer       445,821           316,126
            Consumption                                    541,164          76o]l06
          World Production                                1,823,763         1,922,979

         Source:  Minerals Yearbook 1971  and  Southwest Research Institute

       Data  on mine production include production from crude platinum placers and byproduct
platinum-group metals recovered larRely from  domestic gold and copper ores.  The product from
placer dredging operations at Goodncws Bay, Alaska assays about 64 to 76  percent platinum and
0.23 to 0.39 percent palladium.  Byproduct production from copper and gold refining is mostly palladium.

             U.S. exports of platinum-group metals include 79 percent platinum of a total of 404,610 oz
for all metals.  It was assumed that 18.9 percent represented palladium and 2. 1 percent  minor
platinum-group metals.
                                               B-5

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                                     TECHNICAL REPORT DATA
                             (/'lease read instructions on the reverse before completing)
    EPA-650/1-74-008
                                                            3 RECIPIENT'S ACCESSION NO
    TITLE AND SUBTITLE  A Literature bearch and Analysis of
    Information  Regarding Sources, Uses, Production, Con-
    sumption,  Reported  Medical  Cases, and Toxicology of
    Platinum and Palladium
                                                          REPORT DATE
                                                          April 1974
                                                        6 PERFORMING ORGANIZATION CODE
    Richard A. Mayer, W.  Lawrence Prehn, Jr., and
    Donald E. Johnson
                                                            8 PERFORMING ORGANIZATION REPORT NO
                                                          SWRI    013881
  9 PERFORMING OR~ANIZATION NAME AND ADDRESS
    Southwest Research  Institute
    8500 Culebra Road
    San Antonio, Texas  78284
                                                        10- KnoGRAiW Etti«6NT NO
                                                          1AA002
                                                        11. CONTRACT/GRANT NO
                                                          68-02-1274
              iGENCV NAME AND ADDRESS
Environmental Protection  Agency
National Environmental  Research Center
Research Triangle Park, North  Carolina  27711
                                                            13. TYPE OF REPORT AND PERIOD COVERED
                                                             Final 2/15/74-4/15/74
                                                            4. SPONSORING AGENCY CODE
                 IOTES
                                                        the basis  tor  the
    SI^tS,1Sl!SSTn5e??SiSlitSdlJI!RSfS.prwidas the basis
       Supply and Demand. An average of 3.7 million  troy ounces of platinum and
    S™^
    troy  ounces,  with considerable promise of  increasing these reserves through new ex-
                                            Introduction  of a n   dmd fout«ote

                                                                          lB 1990) 1


                                                 >ears that the
                                                       sources, it Should be pointed
                                                          : upon fpreign sources.  The
                                                          production, but it produces
                                                                         o
   cal  and petroleum
                             -,,  i      I     _  , *"****Bjj»*»»iwii.*  mJtt v/»« \*i i\A \t Willjr Ul 1C «) Q I LJ
                             itij hazards.   Industrial  exposure to these is limited ti
                             atinum ores and the preparation of catalysts for chemi-
                           industries.
 17
                                KEY WORDS AND DOCUMENT ANALYSIS
                  DESCRIPTOR
   Platinum catalysts
   Palladium catalysts
   Catalytic converters - automotive
   Trace  contaminants
   Heavy  metal  pollution
   Auto emissions
                                              b IDENTIFIERS/OPEN ENDED TERMS
                                                                        c  COSATI I icId/Croup
  Unlimited
                                             19 SECURITY CLASS (This Report)
                                                Unclassified
                                                                    21 NO OF PAGES

                                                                         46
EPA Form 2220-1 (9-73)
                                              10 SECURITY CLASS (Thispage)

                                                Unclassified
                                                                    22 PRICE
                                            B-6

-------