United States
Environmental Protection
Agency
Office of Water
Regulations and Standards
Washington nc 20460
Water
                 June, 1985
Environmental Profiles
and Hazard Indices
for Constituents
of Municipal Sludge:
Fluoride

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                                 PREFACE
     This document is one of^-a^series  of preliminary assessments dealing
with  chemicals  of potential  concern  in municipal  sewage sludge.   The
purpose of these  documents  is to:  (a)  summarize  the  available data for
the  constituents  of  potential  concern,  (b)  identify  the key environ-
mental pathways  for  each  constituent  related to  a reuse and disposal
option (based on  hazard  indices), and  (c) evaluate  the conditions under
which ~such a pollutant may pose a hazard.   Each document provides a sci-
entific baVvs  for making an  initial  determination  of whether  a pollu-
tant, at levels currently observed in sludges, poses a likely hazard to
human health  or  the  environment  when  sludge  is disposed  of by  any of
several methods.   These methods  include landspreading on  food  chain or
nonfood chain  crops,  distribution  and marketing  programs, landfilling,
incineration and ocean disposal.

     These documents  are intended to  serve as a rapid  screening tool to
narrow an initial list of pollutants to  those  of concern.   If a signifi-
cant  hazard is  indicated by  this preliminary analysis, a  more detailed
assessment will  be undertaken  to  better quantify  the  risk  from  this
chemical  and to derive  criteria  if warranted.   If a hazard  is  shown to
be unlikely, no further  assessment will be conducted at  this  time;  how-
ever, a  reassessment  will  be  conducted after  initial regulations  are
finalized.  In no case,  however,  will criteria be derived  solely on Che
basis of  information presented in this document.

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                            TABLE OP CONTENTS


                                                                     Page

PREFACE	   i

1.  INTRODUCTION	7..  1-1

2.  PRELIMINARY CONCLUSIONS FOR FLUORIDE IN MUNICIPAL SEWAGE
      SLUDGE	  2-1

    Landspreading and Distribution-and-Marketing 	  2-1

    Landfilling 	  2-2

    Incineration 	  2-2

    Ocean Disposal 	  2-2

3.  PRELIMINARY HAZARD INDICES FOR FLUORIDE IN MUNICIPAL SEWAGE
      SLUDGE	  3-1

    Landspreading and Distribution-and-Marketing 	  3-1

         Effect on soil concentration of fluoride (Index 1) 	  3-1
         Effect on soil biota and predators of soil biota
           (Indices 2-3) 	  3-3
         Effect on plants and plant tissue
           concentration (Indices 4-6) ..'.	'..'	  3-4
         Effect on herbivorous animals'(Indices 7-&) 	  3-9
         Effect on humans (Indices 9-13) 	  3-12

    Landf illing 	  3-21

    Incineration 	  3-21

    Ocean Disposal *.	  3-21

4.  PRELIMINARY DATA PROFILE FOR FLUORIDE IN MUNICIPAL SEWAGE
      SLUDGE	  4-1

    Occurrence 	  4-1

         Sludge 	  4-1
         Soil - Unpolluted 	.'..  4-1
         Water - Unpolluted 	'.	  4-2
         Air 	  4-2
         Food 	  4-3

    Human Effects 	   4-4

         Ingestion 	   4-4
         Inhalation 	   4-5

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                            TABLE OF CONTENTS
                               (Continued)

                                                                     Page

    Plant Effects 	  4-5

         Phytotoxicity 	  4-5
         Uptake 	  4-6

    Domestic Animal and Wildlife Effects 	  4-7

         Toxicity	  4-7
         Uptake 	  4-7

    Aquatic Life Effects	  4-7

    Soil Biota Effect	  4-7

    Physicochemical Data for Estimating Fate and Transport 	  4-7

5 .  REFERENCES	.'	  5-1

APPENDIX.  PRELIMINARY HAZARD INDEX CALCULATIONS FOR
    FLUORIDE IN MUNICIPAL SEWAGE SLUDGE 	  A-l
                                   ill

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                                SECTION 1

                               INTRODUCTION
     This preliminary  data profile is one of  a  series of profiles  deal-
ing with  chemical  pollutants potentially of  concern in municipal  sewage
sludges.   Fluoride was  initially  identified as being  of potential con-
cern when  sludge is landspread  (including  distribution and marketing).41
This  profile  is  a  compilation of  information  that  may  be  useful   in
determining  whether  fluoride poses an  actual hazard  to  human health  or
the environment when sludge is disposed of by this method.
     The  focus  of  this  document  is  the  calculation  of  "preliminary
hazard  indices"  for selected potential exposure  pathways,  as  shown  in
Section 3.   Each  index  illustrates  the hazard  that  could  result from
movement  of  a  pollutant  by  a  given pathway  to cause  a  given effect
(e.g., sludge •* soil •*• plant  uptake •* animal uptake  •*  human  toxicity).
The values and assumptions employed  in these calculations tend to repre-
sent a  reasonable  "worst case";  analysis  of  error or  uncertainty has
been conducted  to  a limited  degree.   The  resulting  value in  most  cases
is  indexed  to  unity;  i.e., values >1  may indicate  a  potential hazard,
depending upon the assumptions of the calculation.
     The data used for index  calculation have been selected  or estimated
based on  information presented  in  the "preliminary  data  profile", Sec-
tion 4.   Information  in the profile  is  based on a compilation  of the
recent  literature.   An  attempt has  been  made to  fill out  the profile
outline to the greatest  extent  possible.   However,  since  this is a pre-
liminary analysis,  the literature has not been exhaustively perused.
     The "preliminary  conclusions" drawn  from each  index in  Section  3
are summarized  in  Section 2.   The preliminary  hazard indices-  will  be
used: as a  screening  tool to determine'which  pollutants and  pathways may
pose a hazard.   Where  a potential hazard  is  indicated by interpretation
of  these  indices,,  further analysis will  include  a  more  detailed exami-
nation  of  potential risks as  well  as an  examination of  site-specific
factors.   These more  rigorous  evaluations  may  change  the  preliminary
conclusions  presented  in  Section  2,  which  are  based on a  reasonable
"worst case" analysis.
     The preliminary hazard indices  for selected  exposure routes perti-
nent  to  landspreading  and  distribution  and  marketing  practices  are
included in  this profile.   The calculation  formulae  for these  indices
are shown in the Appendix.   The indices  are rounded  to  two  significant
figures.
  Listings were  determined  by a  series  of expert  workshops  convened
  during  March-May,  1984  by  the  Office  of  Water   Regulations   and
  Standards (OWRS)  to  discuss landspreading, landfilling,  incineration,
  and ocean disposal,  respectively,  of  municipal  sewage  sludge.
                                   1-1

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                                SECTION 2

     PRELIMINARY CONCLUSIONS FOR FLUORIDE IN MUNICIPAL SEWAGE SLUDGE
     The  following  preliminary  conclusions  have  been derived  from the
calculation of  "preliminary hazard  indices",  which  represent conserva-
tive or  "worst  case" analyses  of  hazard.   The  indices and  their basis
and interpretation are explained in  Section  3.   Their calculation formu-
lae are shown in the Appendix.

  I. LANDSPREADING AND DISTRIBUTION-AND-MARKETING

     A«   Effect on Soil Concentration of Fluoride

          Soil  concentrations  of  fluoride  are  not  expected  to  change
          significantly due to landspreading of  sludge.   A high applica-
          tion of sludge  containing  a typical concentration  of fluoride
          may increase  the  soil  concentration  due  to  dilution, and  a
          high application of  sludge containing  a  high  concentration of
          fluoride may  increase  the soil  concentration  by   30  percent
          (see Index 1).

     B.   Effect on Soil Biota  and Predators of Soil Biota

          Conclusions were not  drawn because  index values could  not be
          calculated due to lack of data (see Indices 2 and 3).

     C.   Effect on Plants and  Plant Tissue Concentration

          Fluoride  in sludge-amended  soil  is  not  expected   to  pose  a
          hazard to plants (see  Index 4).  The  concentrations of fluor-
          ide in plants consumed by  animals  and humans are not expected
          to increase as  a result of landspreading sludge,  except  when
          sludge with a  high fluoride concentration  is  applied  at  high
          rates   (see  Index  5).     The  maximum  increase  in  fluoride
          concentration  predicted  for  plants  in  the human   and  animal
          diet will  not  be precluded  by  phytotoxicity (see  Index 6).

     D.   Effect on Herbivorous Animals

          Landspreading  of sludge is not expected to  pose  a toxic hazard
          from fluoride to grazing animals  that  feed on plants grown on
          sludge-amended  soil (see Index 7)., or  that  incidentally ingest
          sludge-amended  soil (see  Index  8).

     B.   Effect on Humans

          Landspreading  of  sludge  is  not  expected   to  pose  a  health
          hazard from  fluoride to  humans who  consume plants grown  on
          sludge-amended   soil  (see   Index  9);  ingest  animal products
          derived from animals  fed  crops  grown on sludge-amended  soil
          (see  Index  10);   or   consume   animal  products  derived   from
          animals  ingesting   sludge-amended  soil   (see   Index   11).
                                  2-1

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          Ingestion of  sludge-amended  soil  is  not expected  to  pose a
          human  health  hazard  due   to   fluoride,  except  possibly   for
          toddlers   who   ingest   pure   sludge   containing   a   high
          concentration of fluoride  (see Index 12).   An  aggregate human
          health hazard  due  to  fluoride is  not  expected  to occur  as a
          result of landspreading sludge (see Index 13).

 II. LANDPILLING

     Based on  the recommendations of the experts  at  the OWRS  meetings
     (April-May, 1984),  an  assessment of  this reuse/disposal option  is
     not being conducted at  this time.   The U.S. EPA  reserves  the right
     to conduct such an assessment for this option in the  future.

III. INCINERATION

     Based on  the recommendations of the experts  at  the OWRS  meetings
     (April-May, 1984),  an  assessment of  this reuse/disposal option  is
     not being conducted at  this time.   The U.S. EPA  reserves  the right
     to conduct such an assessment for this option in the  future.

 IV. OCEAN DISPOSAL

     Based on  the  recommendations of the experts  at  the OWRS  meetings
     (Aprilr-May, 1984),  an  assessment of  this reuse/disposal option  is
     not being conducted at  this time.   The U.S. EPA  reserves the right
     to conduct such an assessment for this option in the  future.
                                  2-2

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                                SECTION 3

                 PRELIMINARY HAZARD INDICES FOR FLUORIDE
                       IN MUNICIPAL SEWAGE SLUDGE
I. \ LANDSPREADING AND DISTRIBUTTON-AND-MARKETING

     A.   Effect on Soil Concentration of Fluoride

          1.   Index of Soil Concentration Increment (Index 1)

               a.   Explanation - Shows degree of  elevation of pollutant
                    concentration in  soil  to  which  sludge  is  applied.
                    Calculated  for  sludges  with   typical  (median  if
                    available) and  worst  (95th percentile  if available)
                    pollutant concentrations,  respectively, for each  of
                    four sludge loadings.   Applications (as  dry matter)
                    are chosen and explained as follows:

                      0 mt/ha  No  sludge applied.  Shown for  all indices
                               for  purposes of  comparison,  to  distin-
                               guish hazard posed  by  sludge from  pre-
                               existing   hazard   posed   by   background
                               levels  or other  sources of  the  pollutant.

                      5 mt/ha  Sustainable yearly agronomic application;
                               i.e.,  loading  typical  of   agricultural
                               practice,  supplying   ^50   -kg   available
                               nitrogen per  hectare.

                     SO mt/ha  Higher   application   as  may   be  used  on
                               public   lands,   reclaimed areas  or   home
                               gardens.

                    500 mt/ha  Cumulative    loading   after    years    of
                               application.

               b.   Assumptions/Limitations  - Assumes  pollutant is  dis-
                    tributed and  retained within the upper  IS  cm of  soil
                    (i.e.,   the  plow  layer),  which  has  an  approximate
                    mass (dry matter)  of 2 x 103 mt/ha.

               c.   Data Used and  Rationale

                      i. Sludge concentration of pollutant (SC)

                         Typical     86.4  ug/g  DW
                         Worst       738.7  Ug/g  DW

                         The typical and worse  sludge concentrations are
                         the median and  95th  perentile values statis-
                         tically  derived from  sludge concentration data
                                  3-1

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          from  a  survey  of  40  publicly-owned  treatment
          works   (POTWs)   (U.S.   EPA,    1982).      (See
          Section 4, p. 4-1.)

      ii. Background concentration o£ pollutant in soil
          (BS) = 292 Ug/g DW

          The background soil  concentration for fluoride,
          292 Ug/g,  is  the  mean concentration for soils 0
          to  12  inches  in depth. (Robinson and Edgington,
          1946, as  cited  in National Academy of  Sciences
          (NAS),  1971).   The  mean  represents concentra-
          tions from 30 samples  throughout the U.S.  rang-
          ing  from 20  ug/g to  1620 Ug/g.    In  the  same
          study, concentrations  of fluoride  in soil  from
          0 to 3  inches  depth  ranged from  20  to  500  Ug/g
          with a  mean  of 190  Ug/g.  Since fluoride  con-
          centration generally increases with depth,  the
          concentrations for  12 inches   was  selected  con-
          servatively as  a representative concentration.
          This  selected value  falls  within  the  normal
          fluoride concentration range of  200  to  300  Ug/g
          for mineral soils  (U.S.  EPA,   1980).  (See  Sec-
          tion 4, p. 4-1.)

d.   Index 1 Values

                         Sludge Application Rate (mt/ha)
         Sludge
     Concentration        0        5        50       500
Typical
Worst
1
1
1.0
1.0
0.98
1.0
0.86
1.3
e.   Value Interpretation -  Value equals factor  by  which
     expected soil  concentration exceeds background  when
     sludge is applied.   (A value of 2  indicates concen-
     tration is doubled;  a  value of 0.5  indicates  reduc-
     tion by one-half.)

£.   Preliminary  Conclusion  -   Soil  concentrations   of
     fluoride are  not  expected  to  change  significantly
     due to landspreading of sludge.   A  high  application
     of  sludge   containing   a  typical   concentration   of
     fluoride may decrease  the  soil concentration due  to
     dilution,    and   a   high   application   of   sludge
     containing   a   high  concentration   of   fluoride   may
     increase the soil concentration by 30 percent.
                    3-2

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B.   Effect on Soil Biota and Predators of Soil Biota

     1.   Index of Soil Biota Toxicity (Index 2)

          a.   Explanation  - Compares  pollutant  concentrations  in
                sludge-amended soil with soil concentration shown to
               be toxic for some organism.

          b.   Assumptions/Limitations -  Assumes  pollutant  form in
               sludge-amended  soil   is   equally  bioavailable  and
               toxic as form used  in  study  where toxic effects were
               demonstrated.

          c.   Data Used and Rationale

                 i. Index of soil concentration increment (Index 1)

                    See Section 3,  p.  3-2.

                ii. Background concentration  of  pollutant in  soil
                    (BS) = 292 yg/g DW

                    See Section 3,  p.  3-2.

               iii. Soil concentration  toxic  to  soil  biota  (TB)  -
                    Data not immediately available.

          d.   Index 2  Values  -  Values were  not calculated  due .to
               lack of  data.

          e.   Value Interpretation - Value.equals factor by which
               expected soil concentration exceeds  toxic  concentra-
               tion.   Value >1  indicates a  toxic hazard  may exist
               for soil biota.

          f.   Preliminary  Conclusion  -  Conclusion was  not  drawn
               because  index values could  not  be calculated.

     2.   Index of Soil Biota Predator Toxicity (Index  3)

          a.   Explanation  -  Compares   pollutant  concentrations
               expected in  tissues  of organisms  inhabiting  sludge-
               amended   so'il  with  food  concentration  shown  to  be
               toxic to a'predator  on  soil organisms.

          b.   Assumptions/Limitations  -   Assumes  pollutant   form
               bioconcentrated  by soil biota  is equivalent in  tox-
               icity to form  used  to demonstrate toxic  effects  in
               predator.  Effect  level in predator may be  estimated
               from that in  a different species.
                             3-3

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          c.   Data Used and Rationale

                 i. Index of soil concentration increment (Index  1)

                    See Section 3, p. 3-2.

                ii. Background  concentration  of  pollutant  in soil
                    (BS) = 292 Ug/g DW

                    See Section 3, p. 3-2.

               iii. Uptake slope  of  pollutant in soil  biota (UB) -
                    Data not immediately'available.

                iv. Background  concentration  in  soil biota  (BB) -
                    Data not immediately available.

                 v. Peed  concentration  toxic  to  predator   (TR)  -
                    Data not immediately available.

          d.   Index  3  Values  - Values  were not calculated  due  to
               lack of 'data.

          e.   Value  Interpretation - Value equals  factor  by which
               expected  concentration in  soil  biota exceeds  that
               which  is  toxic  to predator.   Value >  1  indicates a
               toxic hazard may exist for predators of soil biota.

          f.   Preliminary  Conclusion -  Conclusion  was not  drawn
               because index values could not be calculated.

C.   Effect on Plants and Plant Tissue Concentration

     1.   Index of Phytotoxicity (Index 4)

          a.   Explanation -  Compares  pollutant concentrations  in
               sludge-amended soil with  the lowest  soil concentra-
               tion shown to be toxic for some plant.

          b.   Assumptions/Limitations -  Assumes pollutant  form  in
               sludge-amended  soil   is   equally  bioavailable  and
               toxic as form used in  study  where toxic effects were
               demonstrated.

          c.   Data Used and Rationale

                 i. Index of soil concentration increment (Index 1)

                    See Section 3, p.  3-2.

                ii. Background  concentration of  pollutant  in  soil
                    (BS) = 292  yg/g DW

                    See Section 3, p.  3-2.


                              3-4

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     ill. Soil  concentration   toxic  to  plants  (TP)  =
          454 ug/g DW

          The  soil  concentration   toxic  to  plants  was
          chosen   conservatively.      This  concentration
          represents  the  highest concentration  tested by
          Davis (1980)  in a study of  rye  grass  uptake of
          fluoride following  application of fluoride-rich
          sludge.   No  adverse  effects  were  observed at
          this concentration,  and,  in  fact,  the  yield was
          increased.    Cooke  et al.  (1976,  as   cited by
          Davis,  1980)  found  no symptoms  of  toxicity in
          rye grass  grown  on  fluorspar waste containing
          17.422  fluoride.   Although  Cooke  et al. (1976)
          reported a  higher  soil  concentration  where no
          effects  were  observed,    the  concentration  of
          454 Ug/g was  chosen as a  conservative estimate
          (304 Ug/g  plus  150  Ug/g  background in experi-
          mental  soil)  of  a  concentration  where effects
          might occur.  A study  by  Morse (1935), cited in
          Eagers  (1969),  reported that a concentration of
          100 Ug/g greatly diminished  seed germination of
          maize and 400 Ug/g  completely inhibited germi-
          nation.   However,  these   concentrations  repre-
          sent   soluble   fluoride   rather   than   total
          fluoride, which would normally  be  less  avail-
          able to plants.  Another  study- by  Thompson et
          al.  (1979)   reported  fluoride  damage  to  fir
          trees  where  soil  concentrations  of   fluoride
          were 36  Ug/g.  However,  the  soil  fluoride con-
          centrations  in  this  study'were  the  result  of
          deposit  of  airborne  fluoride from  a  factory.
          It  was   not  clear  to what   degree  the  damage
          observed  was  due to  atmospheric  exposure  to
          fluoride, since  plants are  known  to accumulate
          fluoride  and   suffer  injury  from  atmospheric
          exposure to  fluoride  (U.S.  EPA,  1980).   (See
          Section 4,  p.  4-9.)

d.   Index 4 Values

                        Sludge Application  Rate (mt/ha)
         Sludge
     Concentration        0         5       50        500
Typical
Worst
0.64
0.64
0.64
0.65
0.63
0.67
0.55
0.84
e.   Value Interpretation -  Value  equals factor by  which
     soil concentration exceeds phytotoxic  concentration.
     Value > 1 indicates a phytotoxic hazard may exist.

f.   Preliminary Conclusion  -  Fluoride  in  sludge-amended
     soil is not expected  to  pose a hazard  to  plants.
                    3-5

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2.   Index of  Plant Concentration  Increment Caused  by Uptake
     (Index 5)

     a.   Explanation -  Calculates  expected  tissue concentra-
          tion  increment  in  plants  grown  in  sludge-amended
          soil,  using   uptake  data  for  the  most  responsive
          plant  species  in the  following  categories:    (1)
          plants  included  in  the  U.S.  human   diet;  and  (2)
          plants  serving as animal  feed.    Plants used  vary
          according to  availability of  data.

     b.   Assumptions/Limitations -  Assumes  a  linear  uptake
          slope.   Neglects  the effect  of time;  i.e.,  cumula-
          tive  loading  over several years  is  treated  equiva-
          lently  to single  application  of  the same  amount.
          The  uptake factor  chosen  for  the   animal  diet  is
          assumed  to be  representative  of  all  crops  in  Che
          animal diet.    See  also  Index 6 for consideration of
          phytotoxicity.

     c.   Data Used and Rationale

            i.  Index of soil concentration increment (Index 1)

               See Section 3, p.  3-2.

           ii.  Background concentration  of   pollutant  in  soil
               (BS) = 292 ug/g  DW

               See Section 3, p.  3-2.

          iii.  Conversion  factor  between soil  concentration
               and application  rate  (CO) = 2  kg/ha
               Assumes  pollutant  is distributed  and  retained
               within upper  IS  cm  of  soil  (i.e.  plow  layer)
               which  has an  approximate mass  (dry matter)  of
               2  x  103.

           iv.  Uptake slope of pollutant  in plant tissue  (UP)

               Animal diet:
               Rye  grass  (tops)
                         0.0786 ug/g tissue  DW (kg/ha) -1

               Human  diet:
               Ground cover (cops)
                         0.0098 Wg/g tissue  DW (kg/ha) ~1

               Very limited  data  appropriate  for  calculation
               of   upcake  slopes  are  immediately  available.
               Rye  grass  was  chosen  as  the  representative
               plant  consumed by animals.  The uptake  slope  of
               0.0786  was  calculated from  data presented  by
               Davis  (1980) in a  study  which applied fluoride-

                        3-6

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           rich  sludge at rates whictK equated to 0  to  672
           kg/ha.   An  uptake slope  for. fescue was  calcu-
           lated  to  be  0.0059  Ug/g tissue  DW  (kg/ha)'1
           based   on   data  presented  by  Wright  et   al.
           (1978).     However,  to   be  conservative,   the
           higher  uptake  slope  for  rye  grass was chosen.
           No  data were  immediately  available to  estimate
           the uptake slope for plants consumed by humans.
           An  uptake  slope  of  0.0098  was  available  for
           ground   cover  consisting  largely  of   clover
           (Trifoliam  repens).     Wright  et  al.   (1978)
           studied  the uptake of  fluoride  in ground  cover
           grown in soils contaminated with flouride.   The
           value for  ground cover  appeared  to be the most
           representative uptake  slope  available.   It  is
           assumed  that uptake of  fluoride  by leafy  vege-
           tables  is   similar  to  the  ground  cover uptake.
           (See Section 4,  p.  4-10.)

       v.  Background concentration in plant tissue (BP)

           Animal diet:
           Rye grass  (tops)       6.0 Ug/g DW

           Human diet:
           Ground cover (tops)    6.2 Ug/g DW

           Background  concentrations  of  fluoride in  rye
           grass and  ground cover  are those given by  Davis
           (1980)  and Wright  et al.  (1978),  respectively,
           in  the   studies  presenting data used  to  calcu-
           late the uptake slopes.   (See  Section 4,   p.  4-
           10.)

d.   Index S Values

                                   Sludge Application
                                      Rate (mt/ha)
                   Sludge
     Diet       Concentration  05      50        500
Animal
Typical
Worst
1.0
1.0
0.99
1.0
0.87
1.3
-0.077
3.3
     Human        Typical      1.0  1.0    0.98      0.87
                  Worst        1.0  1.0    1.0       1.3

e.   Value  Interpretation  - Value equals  factor  by which
     plant  tissue concentration  is  expected  to  increase
     above background when grown in sludge-amended soil.

.f.   Preliminary  Conclusion  -  The   concentrations   of
     fluoride  in  plants  consumed by  animals  and  humans
     are  not   expected   to  increase  as   a  result   of
                    3-7

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          Landspreading sludge, except when  sludge  with a high
          fluoride concentration is applied at high rates.

3.   Index  of  Plant   Concentration   Increment  Permitted  by
     Phytotoxicity (Index 6)

     a.   Explanation -  Compares  maximum plant  tissue concen-
          tration  associated  with  phytotoxicity  with  back-
          ground concentration in same plant  tissue.   The pur-
          pose is to determine whether the  plant concentration
          increments calculated  in Index 5  for high  applica-
          tions are truly realistic, or  whether such increases
          would be precluded by phytotoxicity.

     b.   Assumptions/Limitations -  Assumes  that  tissue  con-
          centration will be  a consistent indicator of phyto-
          toxicity.

     c.   Data Used and Rationale

            i. Maximum  plant  tissue  concentration  associated
               with phytotoxicity (PP)

               Animal  diet:
               Rye grass    2745  Ug/g DW

               Human diet:
               Spinach        857  Ug/g DW

               Available data indicate- that  rye grass  is'able
               to  tolerate  relatively high*  tissue  concentra-
               tions without exhibiting phytotoxicity.  A  con-
               centration of  2745  Ug/g DW caused  no  signs  of
               phytotoxicity  in  rye  grass grown on  fluorspar
               waste  (Cooke  et   al.,  1976   cited   in Davis,
               1980).     In  a  pot  study  using fluoride-rich
               sludge,  rye grass  yield increased at the high-
               est soil  fluoride  concentration; tissue fluor-
               ide was  60 Ug/g DW (Davis,  1980).  In  spite  of
               the fact  that  phytotoxicity  was not observed,
               the data  from  Cooke  et al.  (1976)  were chosen
               to    conservatively   maximize   the    value    of
               Index 6.   Spinach  was  chosen  as a representa-
               tive  leafy  vegetable  consumed  by  humans  for
               which  tissue  concentrations  associated   with
               toxicity  were  available.    The  spinach tissue
               concentrations  associated  with  toxicity ranged
               from  803  to  857  Ug/g DW  (U.S. EPA, 1980).
               Therefore,  the value of 857  Ug/g DW represents
               the  highest   concentration   associated   with
               phytotoxicity.   (See Section 4, p. 4-9.)
                        3-8

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                ii. Background concentration  in plant  tissue  (BP)

                    Animal diet:
                    Rye grass     127 ug/g  DW

                    Human diet:
                    Spinach        28.3 Ug/g  DW

                    The  background  tissue   concentration  for  rye
                    grass  was obtained   from Cooke  et  al.   (1976)
                    because  the  PP  value  for  rye grass  was taken
                    from this  study.   Background concentrations for
                    spinach were 35  Ug/g  DW reported by Benedict et
                    al., 1964  (as  cited in U.S.  EPA,  1980) and 1.3
                    to  28.3  llg/g  DW reported  by Garber,  1967  (as
                    cited  in  U.S.  EPA,   1980).    The  value  of
                    28.3 ]ig/g  was  chosen  since  it  is  between  the
                    highest and  lowest  values reported.   (See Sec-
                    tion 4, p. 4-6.)

          d.   Index 6 Values

                   Plant              Index Value

               Rye grass                 22
               Spinach                   30

          e.   Value  Interpretation  -   Value   gives   the  maximum
              • factor  of  .tissue .  concentration   increment   (above
               background)  which  is  permitted  by  phytotoxicity.
               Value is compared with  values for  the  same  or simi-
               lar plant tissues  given by  Index  5.    The  lowest  of
               the two indices indicates  the  maximal  increase which
               can occur at any given application rate.

          f.   Preliminary  Conclusion   -  The maximum  increase  in
               fluoride concentration  predicted  for  plants  in  the
               human  and   animal   diet  will  not  be  precluded  by
               phytotoxicity.

D.   Effect on Herbivorous Animals

     1.   Index of Animal Toxicity Resulting  from Plant Consumption
          (Index 7)

          a.   Explanation  -   Compares  pollutant   concentrations
               expected in  plant  tissues  grown   in  sludge-amended
               soil with  food concentration  shown to  be  toxic  to
               wild or domestic herbivorous animals.   Does  not con-
               sider  direct   contamination  of  forage  by  adhering
               sludge.

          b.   Assumptions/Limitations   -   Assumes  pollutant   form
               taken up by plants is equivalent in toxicity to form
                              3-9

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     used co demonstrate  toxic  effects in animal.  Uptake
     or  toxicity  in  specific  plants or  animals  may be
     estimated from other species.

c.   Data Used and Rationale

       i. Index  of plant  concentration  increment caused
          by uptake (Index 5)

          Index  S values  used  are  those  for  an animal
          diet (see Section 3, p. 3-7).

      ii. Background concentration  in plant tissue (BP) =
          6 Ug/g  DW

          The background  concentration value  used is for
          the plant chosen  for the animal  diet  (see Sec-
          tion 3, p. 3-7).

     iii. Peed concentration  toxic to herbivorous animal
          (TA) = 40 Ug/g DW

          The value for feed  concentration  represents the
          maximum  dietary  tolerance for dairy cattle and
          young  cattle  recommended  by NAS  (1980).   The
          maximum  dietary  tolerance for mature  beef  cat-
          tle is  50  Ug/g  (NAS,  1980).   Minor morpholog-
          ical lesions occur  in the  teeth'  of  cattle  when
          dietary  fluoride  exceeds 20  Ug/g during tooth
          development; however,  no  relationship  between
          these  lesions  and  animal performance  has  been
          determined (NAS,  1980).   Although Davis (1980)
          reported a  toxic  fluoride threshold  of  30  Ug/g
          for cattle,  Baxter  et  al.  (1983)   reported  no
          adverse  effects   for  cattle  at   this  feed
          concentration.   (See Section 4,  p. 4-11.)

d.   Index 7 Values

                        Sludge Application Rate (nut/ha)
         Sludge
     Concentration        0         5        SO        500
Typical
Worst
0.15
0.15
0.15
0.15
0.13
0.19
-0.012
0.50
e.   Value Interpretation -  Value equals factor  by  which
     expected  plant  tissue  concentration   exceeds   that
     which is  toxic  to  animals.   Value >1 indicates  a
     toxic hazard may exist  for herbivorous  animals.

f.   Preliminary Conclusion  -  Landspreading of sludge  is
     not expected to pose a  toxic hazard  from  fluoride  to
     herbivorous animals  that  feed  on  plants  grown  on
     sludge-amended soil.

                   3-10

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2.   Index of  Animal  Toxicity Resulting from  Sludge Ingestion
     (Index 8)

     a.   Explanation - Calculates  the amount of  pollutant in
          a grazing animal's  diet resulting from  sludge adhe-
          sion  to  forage  or  from  incidental   ingestion  of
          sludge-amended  soil  and  compares  this   with  the
          dietary toxic threshold concentration  for  a  grazing
          animal.

     b.   Assumptions/Limitations  -  Assumes  that  sludge  is
          applied over and  adheres  to  growing forage,  or that
          sludge constitutes  5 percent  of  dry  matter  in  the
          grazing animal's  diet, and  that  pollutant  form  in
          sludge  is  equally  bioavailable  and  toxic  as  form
          used to* demonstrate  toxic  effects.  Where  no sludge
          is  applied  (i.e.,  0 mt/ha), assumes diet  is  5  per-
          cent soil  as a basis for comparison.

     c.   Data Used  and Rationale

            i. Sludge  concentration  of  pollutant  (SC)

               Typical     86.4 (ig/g DW
               Worst       738.7 ug/g DW

               See Section 3,  p.  3-1.

           ii. Background  concentration  of  pollutant  in  soil
               (BS)  =  292  yg/g DW

               See Section 3,  p.  3-2.

          iii.  Fraction of animal diet assumed to be  soil  (GS)
               = 5Z

               Studies  of  sludge adhesion   to growing  forage
               following applications  of  liquid or filter-cake
               sludge  show  that  when 3  to  6  mt/ha  of  sludge
               solids   is   applied,  clipped  forage   initially
               consists  of up  to  30 percent sludge  on  a dry-
               weight  basis (Chaney and  Lloyd,  1979; Boswell,
               1975).   However,  this  contamination diminishes
               gradually with  time  and growth,  and  generally
               is  not  detected in the following year's  growth.
               For example, where pastures  amended at  16 and
               32  mt/ha were grazed throughout a growing sea-
               son (168 days), average sludge  content of for-
               age  was  only  2.14  and  4.75 percent,   respec-
               tively   (Bertrand   et  al.,  1981).    It  seems
               reasonable  to assume  that  animals  may receive
               long-term dietary  exposure to 5 percent  sludge
               if  maintained on  a forage  to which  sludge  is •
               regularly applied.   This estimate of  5 percent
                        3-11

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                    sludge  is  used regardless  of application  rate,
                    since  the  above  studies did  not show  a  clear
                    relationship  between application  rate  and  ini-
                    tial  contamination, and  since adhesion  is not
                    cumulative yearly because of die-back.

                    Studies  of grazing  animals indicate  that  soil
                    ingestion, ordinarily  <10 percent of dry weight
                    of  diet,  may  reach as  high  as  20  percent for
                    cattle  and 30  percent  for sheep during winter
                    months  when  forage  is  reduced   (Thornton and
                    Abrams,  1983).     If   the  soil  were  sludge-
                    amended, it is  conceivable  that up to 5 percent
                    sludge may be ingested in  this  manner  as  well.
                    Therefore,  this value  accounts  for either of
                    these scenarios, whether  forage is harvested or
                    grazed in the field.

                iv. Peed  concentration  toxic to  herbivorous animal
                    (TA) = 40 ug/g DW

                    See Section 3, p.  3-10.

          d.   Index 8 Values

                                  Sludge Application Rate (me/ha)
                   Sludge
               Concentration        0          5       50        500
Typical
Worst
0.37
0.37
0.11
0.92
0.11
0.92
0.11
0.92
          e.   Value' Interpretation -  Value equals factor  by which
               expected dietary concentration exceeds  toxic concen-
               tration.   Value > 1  indicates  a  toxic hazard  may
               exist for grazing animals.

          f.   Preliminary Conclusion  -  Landspreading  of sludge  is
               not expected to pose a  toxic hazard  from fluoride  to
               grazing   animals   incidentally   ingesting   sludge-
               amended soil.

B.   Effect on Humans

     1.   Index of  Human  Toxicity Resulting from Plant  Consumption
          (Index 9)

          a.   Explanation - Calculates dietary intake expected  to
               result   from  consumption of  crops grown  on  sludge-
               amended soil.    Compares dietary  intake  with  accept-
               able daily intake  (ADI)  of  the pollutant.

          b.   Assumptions/Limitations  - Assumes that all crops are
               grown  on   sludge-amended  soil  and  that  all  those
                             3-12

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considered  to  be affected  take  up the  pollutant at
the  same  rate  as  the most responsive  plant(s)  (as
chosen in  Index 5).   Divides  possible  variations in
dietary intake  into .two categories:    toddlers  (18
months to 3 years) and individuals over 3 years old.

Data Used and Rationale

  i. Index  of   plant  concentration increment  caused
     by uptake  (Index 5)

     Index 5 values  used are those for  a  human diet
     (see Section 3,  p.  3-7).

 ii. Background concentration  in  plant  tissue  (BP) =
     28.3 Mg/g  OW

     The background  concentration value used  is  for
     spinach, which  was  chosen as the  plant  for  the
     human diet  in Index 6 (see  Section  3,  p. 3-9).
     This    value  was   chosen,    rather  than   the
     background  concentration   for  ground   cover/
     since it is  higher, and thus, a more conserva-
     tive  choice and  since  it   represents  a  plant
     actually consumed by humans.

iii. Daily  human dietary  intake  of  affected  plant
     tissue (DT)

     Toddler     7-4.5 g/day
     Adult      205    g/day

     The intake  value  for  adults  is  based on  daily
     intake of crop  foods (excluding fruit)  by vege-
     tarians (Ryan et  al.,  1982); vegetarians were
     chosen to  represent  the  worst case.  The  value
     for toddlers is based  on the FDA  Revised  Total
     Diet   (Pennington,   1983)  and  food  groupings
     listed by the U.S. EPA (1984).  Dry weights  for
     individual  food  groups were  estimated from com-
     position data given by  the  U.S.  Department  of
     Agriculture (USDA)  (1975).    These values were
     composited  to estimated dry-weight  consumption
     of all non-fruit crops.

 iv. Average daily human dietary  intake  of pollutant
     (DI)

     Toddler     825  yg/day
     Adult       2500  Ug/day

     The  estimated daily intake of fluoride for tod-
     dlers, age  1  to 3,  was  reported  to range from
     417  to  825  pg/day  when  intake  from  food  and
              3-13

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     water  are totalled (U.S. EPA 1980, adapted  from
     Maier,  1971).   The higher value, 825 ug/day was
     selected  to  represent the average daily  intake.
     U.S. EPA  (1980) also reported that daily fluor-
     ide  intake  from  food  for  1-  to   2-year   old
     children  was  250  to  550 ug/day  (adapted  from
     Jones,  Harries,   and  Martin,   1971);  however,
     this value did not include intake from drinking
     water.    The  dietary intake  in  the  U.S.   for
     adults  from  food and fluoridated drinking water
     is  2500  tig/day  (U.S.   EPA,  1980 adapted  from
     Jones,  Harries, and Martin,  1971).   This value
     is   considered  a   conservative  choice  since
     fluoridated  drinking water  is   included  in   the
     value.   Other  values  reported  are  1800  ug/day
     for men and  1300 Ug/day for housewives (Cholak,
     1960,   in   U.S.   EPA,   1980),   and   2100   to
     2400 ug/day  for  young  adult  U.S.   males   (San
     Filippo  and   Battistone,  1971,  in  U.S.   EPA,
     1980).

  v. Acceptable  daily  intake of  pollutant  (ADI) =
     4000 Ug/day

     Singh and  Jolly (1970,  in U.S.  EPA,  1980)  con-
     sidered that 4000  to  5000 ug is the  daily limit
     that  may  be  ingested  without  hazardous   body
     storage.   Areas  of endemic  fluorosis  commonly
     have levels  of  ingestion  of over 8000  ug/day.
     Since,  no  ADIs  for- fluoride have  been  recom-
     mended,   the   value  of  4000   was   chosen   to
     represent the ADI.
Index 9 Values
Group
   Sludge
Concentration
    Sludge Application
       Rate (mt/ha)

         5     50     500
Toddler
Typical
Worst
0.21
0.21
0.21
0.21
0.20
0.22
0.14
0.36
Adult
  Typical
  Worst
0.62
0.62
0.62
0.63
0.60
0.67
0.44
1.0
Value Interpretation'-  Value equals factor  by  which
expected intake exceeds  ADI.   Value >  1  indicates  a
possible human  health threat.   Comparison with  the
null index  value  at 0 mt/ha indicates  the degree  to
which any  hazard  is  due to  sludge application,  as
opposed to pre-existing dietary sources.
              3-14

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     f.   Preliminary  Conclusion  - Landspreading  of  sludge is
          not  expected to pose a health hazard  from fluoride
          to humans  who consume  crops  grown  on sludge-amended
          soil.

2.   Index  of  Human  Toxicity  Resulting  from Consumption of
     Animal  Products  Derived  from Animals  Feeding  on  Plants
     (Index 10)

     a*   Explanation   -  Calculates   human   dietary   intake
          expected to  result  from consumption  of  animal prod-
          ucts  derived from  domestic animals  given  feed grown
          on  sludge-amended  soil  (crop or  pasture  land)  but
          not  directly contaminated  by adhering sludge.   Com-
          pares expected intake with ADI.

     b.   Assumptions/Limitations  -   Assumes   that  all  animal
          products are from animals  receiving all  their  feed
          from  sludge-amended soil.   The uptake slope of  pol-
          lutant  in  animal  tissue (UA)  used  is assumed to be
          representative of all animal  tissue  comprised  by the
          daily human  dietary  intake (DA) used.   Divides  pos-
          sible variations in dietary  intake  into  two categor-
          ies:     toddlers  (18   months  to   3  years)   and
          individuals over 3 years old.

     c.   Data Used and Rationale

            i. Index of plant  concentration  increment  caused
               by uptake (Index 5)

               Index 5 values  used  are  those  for  an  animal
               diet (see Section 3, p. 3-7).

           ii. Background concentration in plant tissue  (BP)  =
               6 ug/g  DW

               The background concentration  value  used  is  for
               the plant chosen for  the animal diet  (see  Sec-
               tion 3,  p. 3-7).

          iii. Uptake  slope of pollutant in animal  tissue  (UA)
               = 0.03176 Ug/g tissue DW (ug/g  feed DW)'1

               The uptake  slope  for animal  tissue was  calcu-
               lated from  data  for   beef  liver  presented by
               Suttie  et al. (1958,  in U.S.  EPA, 1980).   Beef
               liver was  chosen   as  the representative  tissue
               of grazing  animals that  is  consumed by  humans
               and for which  an  uptake  slope  could be  calcu-
               lated.   Uptake  slopes were  available for  beef
               heart  and kidney  (0.04365  and  0.31838, respec-
               tively);  however,   these  tissues  generally do
               not constitute  a  substantial   fraction  of   the
                        3-15

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          human  diet.   Uptake slopes were also calculated
          for  various  turkey tissues,  based  on data  pre-
          sented  by Anderson et  al. (1955,  in U.S.  EPA,
          1980).   With the exception of  bone, the uptake
          slopes  were  lower  than  those  for  beef liver.
          Also,  turkeys are  less  representative  of graz-
          ing animals  than cattle.

      iv. Daily  human  dietary  intake  of  affected animal
          tissue  (DA)

          Toddler    0.97 g/day
          Adult      5.76 g/day

          The  FDA Revised  Total  Diet  (Pennington,  1983)
          lists  average daily intake of  beef liver fresh
          weight  for various age-sex  classes.   The 95th
          percentile   of   liver   consumption   (chosen  in
          order  to  be  conservative)   is  assumed  to  be
          approximately 3  times the mean  values.   Conver-
          sion to dry weight is  based  on data from U.S.
          Department-of Agriculture (1975).

       v. Average daily human dietary  intake  of pollutant
          (DI)

          Toddler     825 Ug/day
          Adult      2500 Ug/day

          See Section 3, p. 3-13.

      vi. Acceptable  daily intake  of  pollutant   (ADI)  =
          4000 Ug/day

          See Section 3, p. 3-14.

d.   Index 10 Values

                                  Sludge Application
                                     Rate (me/ha)
                  Sludge
     Group     Concentration    0       5     50     500
Toddler
Typical
Worst
0.21
0.21
0.21
0.21
0.21
0.21
0.21
0.21
     Adult       Typical      0.62   0.62   0.62   0.62
                 Worst        0.62   0.62   0.62   0.62

e.   Value Interpretation - Same as for Index 9.

f.   Preliminary Conclusion  -  Landspreading of sludge  is
     not expected  to  pose a  health hazard  from  fluoride
     to humans  who consume  animal  products derived  from
     livestock fed  crops grown on sludge-amended soil.

                   3-16

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3.   Index  of Human  Toxicity  Resulting  from Consumption  of
     Animal  Products  Derived   from  Animals  Ingesting  Soil
     (Index 11)

     a.   Explanation  -   Calculates   human  dietary   intake
          expected to result  from consumption of  animal prod-
          ucts  derived   from  grazing   animals   incidentally
          ingesting  sludge-amended  soil.    Compares  expected
          intake with ADI.

     b.   Assumptions/Limitations  -  Assumes   that  all  animal
          products  are   from  animals   grazing  sludge-amended
          soil, and that  ail  animal  products  consumed  take  up
          the  pollutant   at  the  highest  rate   observed  for
          muscle  of  any   commonly  consumed species  or  at  the
          rate  observed   for  beef  liver  or  dairy  products
          (whichever is higher).   Divides  possible  variations
          in  dietary  intake  into two categories:    toddlers
          (18 months to  3  years)  and  individuals over  three
          years old.

     c.   Data Used and Rationale

            i. Animal  tissue = Beef liver

               See Section 3,  p.  3-15.

           ii. Background  concentration  of pollutant  in  soil
               (BS) =  292  ug/g .DW

               See Section 3,  p.  3-2.

          iii. Sludge  concentration of  pollutant  (SC)

               Typical      86.4  Ug/g  DW
               Worst      738.7  Ug/g  DW

               See Section 3,  p.  3-1.

           iv. Fraction of animal diet assumed to  be soil  (GS)
               =  52

               See Section 3,  p.  3-11.

           .v. Uptake  slope of pollutant in animal tissue  (UA)
               •  0.03176 yg/g tissue  DW (ug/g  feed DW)"1

               See Section 3,  p.  3-15.
                        3-17

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           vi. Daily  human dietary  intake of  affected animal
               tissue (DA)

               Toddler    0.97 g/day
               Adult      S.76 g/day

               See Section 3, p. 3-16.

          vii. Average daily  human dietary intake of pollutant
               (DI)

               Toddler     825 Ug/day
               Adult      2SOO Ug/day

               See Section 3, p. 3-13.

         viii. Acceptable  daily intake  of  pollutant  (ADI)  =
               4000 ug/day

               See Section 3, p. 3-14.

     d.   Index 11 Values

                                       Sludge Application
                                          Rate (mt/ha)
                       Sludge
          Group     Concentration    0      5     SO     500
Toddler
Adult
Typical
Worst
Typical
Worst
0.21
. 0.21
0.63
0.63
0.21
0.21
0.63
0.63
0.21
0.21
0.63
0.63
0.21
0.21
0.63
0.63
     e.   Value Interpretation - Same as for Index 9.

     f.   Preliminary Conclusion  - Landspreading of  sludge is
          not expected  to pose a  health hazard  from fluoride
          to humans  who  consume  animal products derived  from
          livestock  which  had  incidentally  ingested  sludge-
          amended soil.

4.   Index of Human Toxicity from Soil Ingestion (Index 12)

     a.   Explanation -  Calculates  the amount of pollutant in
          the diet  of a  child  who  ingests  soil (pica  child)
          amended with sludge.  Compares this amount with ADI.

     b.   Assumptions/Limitations   -  Assumes  that   the  pica
          child  consumes an  average  of  5  g/day  of  sludge-
          amended soil.    If an ADI  specific  for  a child  is not
          available, this index assumes that the ADI  for  a 10
          kg child is the same as  that for a 70 kg  adult.   It
          is thus  assumed  that   uncertainty factors  used  in
                        3-18

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deriving  the  ADI  provide  protection for  the child,
taking  into account  the smaller  body  size  and any
other differences  in sensitivity.

Data Used and Rationale

  i. Index of soil concentration increment (Index 1)

     See Section 3, p. 3-2.

 ii. Sludge concentration of pollutant (SC)

     Typical     86.4 pg/g DW
     Worst      738.7 yg/g DW

     See Section 3, p. 3-1.

iii. Background  concentration  of  pollutant   in  soil
     (BS) = 292 yg/g DW

     See Section 3, p. 3-2.

 iv. Assumed amount of soil in  human diet  (DS)

     Pica child    5    g/day
     Adult         0.02 g/day

     The value  of  5  g/day  for  a  pica child  is  a
     worst-case  estimate  employed  by  .U.S.   EPA's
     Exposure   Assessment  Group   (U.S.  EPA/  1983).
     The value  of  0.02  g/day  for* an  adult  is an
     estimate  from U.S.  EPA (1984).

  v. Average daily human dietary intake of pollutant
     (DI)

     Toddler     825  Ug/day
     Adult       2500  Ug/day

     See Section 3,  p.  3-13.

vi. Acceptable  daily  intake of  pollutant  (ADI)  =
     4000 ug/day

     See Section 3, p. 3-14.
              3-19

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          Index 12 Values
                                Sludge Application
                                   Rate (at/ha)
Group
Toddler
Adult
Sludge
Concentration
Typical
Worst
Typical
Worst
0
0.57
0.57
0.63
0.63
5
0.57
0.57
0.63
0.63
50
0.56
0.58
0.63
0.63
500
0.52
0.68
0.63
0.63
Pure
Sludge
0.31
1.1
0.63
0.63
     e.   Value Interpretation - Same as for Index 9.

     £»   Preliminary Conclusion -  Ingestion  of sludge-amended
          soil is  not expected to  pose a human  health hazard
          due  to  fluoride,  except  possibly  for  toddlers  who
          ingest pure sludge  containing  a high  concentration
          of fluoride.

5.   Index of Aggregate Human Toxicity (Index 13)

     a.   Explanation  -  Calculates  the  aggregate  amount  of
          pollutant in  the  human  diet  resulting  from pathways
          described in  Indices  9  to 12.  Compares  this amount
          with ADI.

     b.   Assumptions/Limitations  - As  described  for Indices 9
          to 12.

     c.   Data Used and Rationale - As  described  for Indices 9
          to 12.
     d.   Index 13 Values
                                       Sludge Application
                                          Rate (mt/ha)
Group
Toddler
Adult
Sludge
Concentration
Typical
Worst
Typical
Worst
0
0.57
0.57
0.63
0.63
5
0.57
0.57
0.62
0.63
50
0.56
0.60
0.60
0.68
500
0.45
0.83
0.44
1.0
     e.   Value Interpretation - Same  as  for  Index  9.

     f.   Preliminary Conclusion - An  aggregate  human   health
          hazard due to fluoride is not expected to occur  as  a
          result of  landspreading sludge.
                        3-20

-------
 II. LANDPILLING

     Based on  the recommendations of  the experts  at the  OWRS  meetings
     (April-May,  198'4-^an assessment of  this reuse/disposal option is
     not being conducteoNat  this  time.   The U.S. EPA reserves  the right
     to conduct such an assessment for this option in the future.

III. INCINERATION

     Based on  the recommendations of  the experts  at the  OWRS  meetings
     (April-May,  1984),  an assessment of  this reuse/disposal option is
     not being conducted at  this  time.   The U.S. EPA reserves the right
     to conduct such an assessment for this option in the future.

 IV. OCEAN DISPOSAL

     Based on  the recommendations of  the experts  at the  OWRS  meetings
     (April-May,  1984),  an assessment of  this reuse/disposal option is
     not being conducted at  this  time.   The U.S. EPA reserves the right
     to conduct such an assessment for this option in the future.
                                  3-21

-------
                              SECTION 4

  PRELIMINARY DATA PROFILE  FOR  FLUORIDE  IN MUNICIPAL SEWAGE SLUDGE
I. OCCURRENCE

   A.   Sludge
   B.
             Frequency of Detection

             Assumed 1002 because of its use as an
             additive in water, toothpaste, etc.,
             and because of its ubiquitous nature.

             Concentration

             Sludges of 16 U.S. cities
             Median
             Mean
             95th percentile
             Minimum
                        86.4 yg/g DW
                       167.3 yg/g DW
                       738.7 yg/g DW
                         2.2 Ug/g DW
     33,500 ppm in fluoride-contaminated
     sludge

Soil - Unpolluted

1.   Frequency of Detection

     13th element in abundance constituting
     0.06 to 0.09Z of earth's crust

2.   Concentration

     209+23 ppm (DW) in controlled soil
     (Great Britain)

     20 to 500 ppm in soils 0 to 3 in.
     in depth, mean 190 ppm
Furr et al.,
1976 (p. 684)

Derived from
sludge concen-
tration data
presented in
U.S. EPA, 1982

Davis, 1980
(p. 279)
                                                        U.S.  EPA,  1980
                                                        (p.  1)
                                                        Wright  et al.,
                                                        1978  (p. 305)

                                                        Robinson and
                                                        Edgington,
                                                        1946  in MAS,
                                                        1971  (p. 6)
                                4-1

-------
     20  Co  1620 ppm  in  soils 0  to  12  in.  in
     depth, mean 292 ppm  (30 soils  sampled
     throughout the  United States)

     Max levels:  Idaho Soil -  3870 ppm
                  Tenn. Soil - 8300 ppm
     200 to 300 ppm "normal" for mineral
     soils

     200 ppm common value
Water - Unpolluted

1.   Frequency of Detection

     Assumed 100Z

2.   Concentration

     a.   Freshwater

          <0.3 ppm


     b.   Seawater

          1.4 to l.S ppm


          1.3 mg/L


     c.   Drinking water

          0.02 to 0.1 ppm in northwest United
          States; >0.2 ppm in west, midwest
          and south U.S. water supplies

Air

1.   Frequency of Detection

     Only 3Z of samples from rural locations
     had detectable fluoride
 Robinson and
 Edgington,
 1946 in NAS,
 1971 (p. 6)
 Robinson and
 Edgington,
 1946 in NAS
 1971 (p. 6)
 MeIntire,  1949
 in  NAS, 1971
 (p.  6)

 U.S. EPA,  1980
 (p.  2)

 Bowen,  1966 in
 Davis,  1980
U.S. EPA,  1980
(p. 9)
U.S. EPA, 1980
(p. 9)

Hem, 1970
(p. 11)
NAS, 1971
(p. 6)
NAS, 1971
(p. 233)
                         4-2

-------
     2.   Concentration

          a.   Urban

               <0.05
               >3 Ug/m   in  industrial areas

               87Z of samples <0.05  Ug/m3
          b.   Rural

               
-------
         2.   Concentration

              Typical Concentrations in Fresh Food       Cholak, 1959,
                                                         in NAS, 1971
              Meats               0.01 -  7.70 ppm       (p. 8)
              Fish               <0.10 - 24.00 ppm
              Citrus fruits       0.04 -  0.36 ppm
              Noncitrus fruits    0.02 -  1.32 ppm
              Vegetables          0.10 -  3.00 ppm
              Cereals and
                cereal products  <0.10 - 20.00 ppm
              Milk                0.04 -  0.5S ppm
              Eggs                0.00 -  2.05 ppm
              Butter              0.40 -  1.50 ppm
              Cheese              0.13 -  1.62 ppm
              Sugar               0.10 -  0.32 ppm
              Coffee              0.20 -  1.60 ppm
              Beer                0.15 -  0.86 ppm
              Wine                0.00 -  6.34 ppm

II. HUMAN EFFECTS

    A.   Ingestion

         1.   Carcinogenic!ty

              a.   Qualitative Assessment

                   No evidence of carcinogenicity        U.S.  EPA,  1980
                   induced by ingestion of  fluorides     (p.  320)

         2.   Chronic Tozicity

              a.   ADI

                   4000 to 5000 Mg/day - daily limit     Singh  and
                   that may be ingested without           Jolly,  1970  in
                   hazardous  body storage                 U.S. EPA,  1980
                                                         (p. 292)

              b.   Effects

                   No effects observed  at drinking        California
                   water levels of 0.8  mg/L               State Water
                   Teeth mottled in  children  at           Resources
                   drinking water levels of               Control Board,
                   1.0  to 6.0 mg/L                        1978 (p. 190)
                   Sublethal  level in drinking water
                 •  at 115 mg/L
                   Toxic to man in drinking water
                   at 180 mg/L
                   Lethal  dose in drinking water
                   of 2000 mg/L
                                 4-4

-------
          3.   Absorption Factor

               1 to 10 percent

          4.   Existing Regulations

               Ambient Water Quality Criteria
               ^1.0 mg/L
     B.   Inhalation

          1.   Careinogenicity

               a.   Qualitative Assessment

                    Not found to be carcinogenic to
                    humans when inhaled.

          2.   Chronic Toxicity

               a.   Inhalation Threshold or MPIH

                    See below, "Existing Regulations"

               b.   Effects

                    Overexposure (sh.ort term):
                    Irritation of eyes and respiratory
                    tract.

                    Overexposure (long-term):  Calcifi-
                    cation of bones and ligaments,  mot-
                    tled teeth, or skin rash.

          3.   Absorption Factor.

               Data not immediately available.

          4.   Existing Regulations

               2.5 mg/m3 (TWA)

III. PLANT EFFECTS

     A.   Phytotoxicity

          Most plants absorb very little fluoride
          from the soil

          See Table 4-1.
 California
 State Water
 Resources
 Control  Board,
 1978  (p.  190)
U.S.. Dept. of
Labor,  1978
ACGIH, 1982
NAS, 1971
(p. 7)
                                   4-5

-------
     No cases of fluorosis have ever been
     ascribed to excessive "natural" accumula-
     tion of fluorides in plant tissues

     Threshold for injury for susceptible plants
     is <150 ppm in tissues
     Intermediate plants threshold is  >200  ppm
B.   Uptake
     "Normal" concentrations:  Festuca rubra
     5.01+1.1 ppm DW
     Composite ground cover 8.1+1.3 ppm DW

     "Natural" forage fluoride 5-10 ppm DW
     Uncontaminated alfalfa (107  samples)
     0.8-36.5 ppm (DW),  3.6, median 2 ppm

     Crops uncontaminated by aerial deposition
     of fluorides contain 2 to 20 ppm fluoride

     2 to 20 Ug/g (DW)
     Fluoride Concentration in  Selected  Plants
Plant
Alfalfa
Grass, Hay
Corn
Wheat
Rye
Oats
Rice
Potato
Lettuce
Spinach
Spinach
Celery
Carrot
Tomato
Part
Tops
Plant
Cob
Grain
Grain
Grain
Grain
Tuber
Leaf
Leaf
Leaf
Stalk
Root
Fruit
Fluoride
(ppm DW)
7-15
1-6
1.6
1
1.5
0.5
0.76
1.5-3.0
4.4-11.3
1.3-28.3
35
2
0.4-8.4
2
 Baxter  et  al.,
 1983
NAS,  1971
(p. 98)
Wright et al.f
1978 (p. 305)
NAS, 1971
(p. 136)
Baxter et al.,
1983 (p. 14)

U.S. EPA, 1980
(p. 5)

U.S. EPA, 1980
(p. 119-120)
                                                    Zimmerman and
                                                    Hitchcock, 1956
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Garber, 1967
                                                    Benedict et al,
                                                    1964
                                                    Zimmerman and
                                                    Hitchcock, 1956
                                                    Garber, 1967
                                                    Zimmerman and
                                                    Hitchcock, 1956
                             4-6

-------
               <30 ppm  in 902 of  168  samples of           Suttie et al.,
               dairy feed, "some  samples had over         1958 in U.S.
               200 ppm"                                   EPA, 1980
                                                          (p. 137)

               "There is little or no relation between    NAS, 1971
               total fluoride content of soil and the     (p. 136)
               fluoride content of plants grown on it.
               There is some indication that acid soil
               promotes fluoride  uptake..."

               "Because soil fluoride may be unavailable  U.S. EPA, 1980
               to plants, a direct relationship between
               soil fluoride content and plant fluoride
               content does not necessarily exist."

               See Table 4-2.

 IV. DOMESTIC ANIMAL AND WILDLIFE EFFECTS

     A.   Toxicity

          See Table 4-3.

     B.   Uptake

          See Table 4-4.

  V. AQUATIC LIFE EFFECTS

     Data not immediately available.

 VI. SOIL BIOTA EFFECTS

     Only data available are fluoride pesticides

VII. PHYSICOCHEMICAL DATA FOE ESTIMATING FATE AND TRANSPORT

     Low soil pH greatly increases fluoride               Doss et al.,
     solubility and,  therefore,  availability              1977 (p.  367)
     of fluoride to plants

     Fluorides are mostly insoluble and, therefore,        Baxter,  et  al.,
     not particularly available  to plants                 1983 (p.  14)

     CaF2 (fluorite)                                       Hodgman et  al.,
          Molecular wt.:  78.08                            1961
          Solubility in water (18°C):  0.0016 g/100 mL

     MgF2 (sellaite)                                       Hodgman et  al.,
          Molecular wt.:  62.32                            1961
          Solubility in water (18°C):  0.0076 g/100 mL
                                   4-7

-------
NaF (villiaumite)                                    Hodgman et al,
     Molecular wt.:  42.00                           1961
     Solubility in water (18°C):  4.22 g/100 raL
                             4-8

-------
                                                       TABLE 4-1.  PHYTOTOXICITY OP PLUORIDB
Plant/Tissue
Rye grass


Perennial rye grass
(Loliuo perenne)
Haize



Pir Tree




Apple/Leaf
Apricot/leaf


Bean/leaf
Carrot/leaf
Corn/leaf
Spinach/leaf
Tomato/leaf
Citrus/leaves
Control
Chemical Tissue
Porn Growth Concentration
Applied Medium (|ig/B DW)
P-rich liquid-
digested sludge
(pot study)

Fluorspar
waste
Soluble P



Airborne P




HP gas
HP gas or
industrial
emission
NaP
HP gas
HP gas
NaP
NaP
NR
soil pH 7.0 6


NB 174
NRa NR



NR 7




NAC NA
NA NA


NR NR
NR NR
NR NR
NR
NR NR
NR NR
experimental'
Soil
Concentration
(MK/g W)
188
246
302
454
200
100

400

10
16
36
205
90S
NA
NA


NR
NA
• NA
NR
NR
NR
experimental
Application
Rate
(kg/ha)
84
168
336
672
NR









NA
NA


NR
NA
NA
NR
NR
NR
Experimental
Tissue
Concentration
(Ug/g DU)
HR
NR
NR
60
274S
NR

NR

7
44
91
141
281
72-234
S8-640


O10
2SO-723
48-491
803-8S7
277-2179
100-200
Effect
Increased yield
Increased yield
Increased yield
Increased yield
Mo symptoms of
toxicity
Greatly diminishes
germination
Completely inhibits
germination
No damage
Slight damage0
20-30Z trees deadb
40-60Z trees deadb
80-95Z trees deadb
Toxic symptoms
Toxic symptoms


Toxic symptoms
Toxic symptoms
Toxic symptoms
Toxic symptoms
Toxic symptoms
Significant yield
References
Davis. 1980


Cooke et al., 1976
in Davis 1980
(p. 181)
Horse, 1935 in
Eagers. 1969
Horse. 1935 in
Eagers, 1969
Thompson et al.,
1979



U.S. EPA, 1980








HAS, 1971
and growth reduction
a NR - Not reported.
D Results of study unclear as to whether toxicity was due to atmospheric- P damage or soil concentration.
c NA = Not available.

-------
TABLE 4-2.  UPTAKB OP FLUORIDB BY PLANTS


Plant/Tissue
Bye grass/
tops
Ground covered/
tops'
Fescue/tops

•M - number of
Application
Medium
(Study Type)
F-rich liquid-digested
sludge (pot study)
contaminated soil

contaminated
soil
application rates, including control.

Bange (N)« of
Control Tissue
Application Bates Concentration
Soil pU ( kg/ha )•
7.0

NB

NB


bSlope - y/x: x • kg applied/ha; y = Mg/g plant tissue dry
concentrations reported in Wright (1978) converted by kg/ha
^High frequency
of Tri folium repens (clover).

0-672 (5)

0-348,000 (4)c

0-348,000 (4)c


weight.
by subtracting background

(Vig/g DW)
6

6.2

4.7
.

concentration and then


Uptake
Blopeb
0.0786

0.0098

0.0059


calculating mass



Beferences
Davis, 1980

Wright et al..
1978
Wright et al.,
1978

F in ha IS en deep.


-------
TABLE 4-3.  TOXICITY OP PLUOBIBB TO DOMESTIC ANIMALS AND WILDLIFE
Species
Sheep
Horaea
Cattle
Cattle
Cattle, horses,
sheep
Cattle, auine, sheep,
horse
Nature dairy cattle
and young cattle
Mature beef
Young cattle
Feeder lambs
Horses
Pigs
Chickens
Chemical
Pom
Ped
NB
NB
NR
NB
Sludge
NB
NaP
NaP
NaP
NaF
NaP
NaP
NaP
Peed
Concentration
(Ug/g)
60
30
30
30
<100
300
40
SO
20
ISO
40
ISO
200
Water
Concentration
(mg/L)
NB
NB
NR
NB
NB
NR
NB
NR
NB
NB
NB
NB
NR
Pally
Intake
,
NB
NB
NR
NB
NR
NR
NR
NR
NR
NR
NR
NR
NR
Duration
of Study
NB
NB
NB
NB
NB
NR
NB
NB
NR
NB
NB
NB
NB
Effects Beferences
Safe level U.S. EPA, 1980
Safe level
Toxic- threshold Davis, 19BO
No adverse effects Baxter et al., 1983
Preaents little hazard
to gracing animals
No acute signs of toxicosis U.S. EPA, 1980
observed
Maximum dietary tolerance NAS, 1980
Maximum dietary tolerance
Minor morphological lesions NAS, 1980
in teeth | however no
relationship between teeth
and animal performance
established
Maximum dietary tolerance
Maximum dietary tolerance
Maximum dietary tolerance
Maximum dietary tolerance

-------
                                                              TABLE 4-3.   (Continued)



-C-

G



Speciea
Turkeys

Cattle

Sheep
Sheep
Chemical
Fora
Fed
NR

NR

NaP
CaF2
Peed
Concentration
(M8/8>
ISO

>600

40
2400
Water
Concentration
(«g/L)
NR

NR

NR
NR
Daily
Intake
(mg/kg)
NR

NR

NR
NR
Duration
of Study
MB

NR

2 daya
NR

Effects
Maximum dietary tolerance

Highly toxic

Inappetence
No inappetence


References


Hobbs et al.,
HAS, 1971
Ammerman et al
Anmerman et al


19S4 in

.. 1980
. , 1980
• MR = Not reported.

-------
                                          TABLE 4-4.  UPTAKE OP PLUOBIDB BY DOMESTIC AMIHALS AND WILDLIFE
Chemical
Species (N)a Porm Ped
Pield mole (5) CaP2



Voles CaP2
Apodemua (14)
Sore* (3)
Turkey NaP




Cattle NBe


Bange (Number)*
of Peed
Concentrations0
(pg/g DU)
6.6-4215(3)



6.6-4215(3)


0-1600(7)




0-50(5)


Tissue
Analysed
femur
kidney
liver
muscle
femur


femur
breast flesh
thigh flesh
liver
kidney
heart
liver
kidney
Control Tissue
Concentration
(pg/g DW)C
117
6.7
S.4
4.2
189


NSd
1.2
1.5
1.9
2.6
2-?
2.3
3.5
Uptake
SlopeD»c Beferences
0.4771 Wright et •!., 1978
0.0163
0.00596
0.00041
0.9238 Wright et •!., 1978


7.7648 Anderson et at., 1955 in
0.0173 U.S. EPA, 1980
0.0065
o.ooas
0.0203
0.0436S Suttie et al., 1958 in
0.03176 U.S. EPA, 1980 '
0.31838
•N °  Number of animals/treatment  group.
bWhen tissue values were reported  as  wet  weight,  unless  otherwise  indicated  a moisture content  of  77Z was  assumed  for
 kidney, 70Z for liver and 12Z for muscle.
cSlope ° y/xt  y • MB/8 feed! * =  P8/S tissue.
^NS  = Tissue concentration not significantly increased.
eNR = Not reported.

-------
                                 SECTION 5

                                REFERENCES
American  Conference   of  Governmental  Industrial  Hygienists.     1982.
     Threshold\Limit  Values for Chemical  Substances  in Work Air  Adopted
     by ACGIH for 1982.  Cincinnati, OH.

Ammerman,  C. B.,  P.  R. Henry,  J.  H.  Conrad,  K.  R.  Pick,  and  E. C.
     Araujo.   1980.    Inappetence  in Ruminants as a  Measure of Fluoride
     Solubility in Various  Phosphates.  J. Dairy  Sci. 63:1167-1171.

Anderson, J. 0., J.  S. Hurst,  D.  C.  Strong,  H. Nielsen, D., A. Greenwood,
     W. Robinson, J.  L.  Shupe,  W.  Binns,  R.  A. Bagley, and C. I.  Draper.
     1955.   Effect   of  Feeding  Various   Levels  of  Sodium  Fluoride to
     Crowing Turkeys.   Poult.  Sci. 34:1147-1153.   (As cited in U.S.  EPA,
     1980.)

Baxter, J.  C.,  D.  Johnson, E.  Kienholz,  W.  D. Surge,  and  W.  N.  Cramer.
     1983.   EPA 600/2-83-012.   Effects on Cattle  from Exposure to Sewage
     Sludge.  Cincinnati, OH.

Benedict, H. M., J.  M. Ross,  and R.  W. Wade.   1964.   The Disposition of
     Atmospheric Fluorides  by  Vegetation.  Int.  J. Hater Pollut.  3:279-
     289.  (As cited  in U.S. EPA, 1980.)

Bertrand, J- E., H.   C. Lutrick,  G.  T.  Edds, and  R.  L.  West.   1981.
     Metal  Residues  in Tissues,  Animal Performance and  Carcass Quality
     with Beef Steers  Grazing  Pensacola Bahiagrass  Pastures Treated with
     Liquid Digested Sludge.  J. Ani. Sci.  53:1.

Boswell,  F.  C.   1975.   Municipal  Sewage Sludge  and  Selected  Element
     Applications  to  Soil:  Effect  on Soil  and  Fescue.   J.  Environ.
     Qual.  4(2):267-273.

Bowen, H. J. M.  1966.  Trace  Elements in Biochemistry.  London Academic
     Press.   .(As cited in Davis, 1980.)

California  State Water Resources  Control Board.    1978.    Water  Quality
     Criteria.   Pasadena, CA.

Chaney, R.  A.,  and   C.  A. Lloyd.    1979.    Adherence  of  Spray-Applied
     Liquid  Digested  Sewage Sludge  to Tall  Fescue.   J. Environ.  Qual.
     8(3):407-411.

Cholak, J.   1959.  Flourides:   A Critical  Review.  I.   The  Occurrence of
     Fluoride in Air, Food, and Water.   J. Occup.  Med.  1:501-511.

Cholak, J.   1960.   Current Information on Quantities of  Fluorides Found
     in Air, Food, and Water.   Arch. Ind. Health 21:312-315.   (As cited
     in U.S. EPA,  1980).
                                   5-1

-------
Cooke, J. A.,  H. S. Johnson,  A.  W.  Davison, and A.  D.  Bradshaw.   1976.
     Fluoride  in Planes  Colonizing Fluorspar Mine Waste in Peak  District
     and  Weardale.   Environ.  Pollut.  11:9-13.   (As  cited  in Davis,
     1980.)

Davis,  R.  D.    1980.    Uptake of Fluorides by  Ryegrass  Grown  in Soil
     Treated with Sewage Sludge.  Environ. Pollut. (Series B)  1:277-282.

Doss, G. J.,  L. E. St.  John,  Jr.,  and D. L.  Lisk.^   19.77.    Studies of
     Flouride  Absorption by  Plants  Grown  in  Perlite.  ^"Byll.   Environ.
     Contain. Toxicol. 18(3):366-369.

Eagers, R. Y.   1969.   Toxic Properties  of  Inorganic  Fluorine Compounds.
     Elsevier Publishing Co. Ltd., NY.

Furr,  A.  K.,   A.  W.  Lawrence,  S.  S.  Tong,  M.  C. Grandolfo, R.  A.
     Hofstader,  C.  A.  Bache,  W.  H.  Gutenmann, and  D.  J. Lisk.    1976.'
     Multielement  and  Chlorinated  Hydrocarbon  Analysis  of  Municipal
     Sewage Sludges of American Cities.   Env.  Sci. & Technol. 10(7)683-
     687.

Garber, K.   1967.   About  the Fluorine  Content of Plants.   Qual. Plant
     Mater.  Veg. 15(l):29-36.  (As cited in U.S. EPA,  1980.)

Hem,  J.  D.     1970.     Study  of   Interpretation   of   the  Chemical
     Characteristics of  Natural  Water.   Geological  Survey  Paper 1473,
     Washington, D.C.

Hobbs, C.  S.,  et al.   1954.   Fluorosis in Cattle and Sheep.   Tern. Agri.
     Ezp.- Station Bull. 235.  (As cited in NAS, 1971.)

Uodgman, C.  D., R. C. Weast, and  S. M. Selby (eds.).   1961.   Handbook of
     Chemistry  and  Physics, 42nd Edition.    Chemical Rubber Publishing
     Co.,  Cleveland, OH.

Jones, C.  M., J. M. Harries, and  A. E. Martin.   1971.  Fluoride in Leafy
     Vegetables.  J. Sci. Food Agric.  22:602-605.

Mclntire,  W. H. et al.   1949.   Effects  of  Fluorine   in Tennessee Soils
     and Crops.  Ind.  Eng.  Chem. 41:2466-2475.  (As cited in NAS,  1971.)

Maier,  F.   J.    1971.    Fluoridation.    Crit.  Rev.  Environ.  Control
     2(3):387-430.

National Academy of Sciences.   1971.   Fluorides.   NAS, National  Research
     Council Committee  on  Biologic  Effects  of Atmospheric  Pollutants,
     Washington, D.C.

National Academy  of Sciences.    1980.   Mineral  Tolerances   of  Domestic
     Animals.    NAS,  National  Review Council   Subcommittee  on  Mineral
     Toxicities in  Animals,  Washington, D.C.

Pennington,  J.  A. T.  1983.  Revision of the Total Diet  Study Food Lists
     and Diets.  J.  Am. Diet.  Assoc.   82:166-173.
                                   5-2

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 Robinson,  W. 0., and 6. Edgington.   1946.   Fluoride  in Soils.  Soil Sci.
      61:341-353.  (As cited in NAS, 1971.)

 Ryan, J. A., H. R.  Pahren,  and J. B. Lucas.   1982.   Controlling Cadmium
      in the Human  Food Chain:   A Review  and  Rationale Based  on Health
      Effects.   Environ. Res.  28:251-302.

 San Filippo, F., and G. Battistone.   1971.   The  Fluorine Content  of a
      Representative  Diet  of  the Young Adult  Male.    Clin.  Chem.  Acta
      31:453-457.  (As cited in U.S. EPA,  1980.)

 Singh,  A.,  and  S.  S.  Jolly.    1970.   Toxic Effects  of Larger  Doses  of
      Fluoride:   III.  Chronic Toxic  Effects on the Skeletal  System.   In!
      Fluorides   and  Human  Health.    World  Health  Organization,  Geneva.
      pp. 238-249.   (As cited in U.S.  EPA,  1980.)

 Suttie, J. W.,  P. H.  Phillips,  and R.  F.  Miller.  1958.   Studies of the
      Effects of Dietary Sodium Fluoride on Dairy Cows.   III.   Skeletal
      and Soft  Tissue  Fluorine  Deposition  and  Fluorine Toxicosis.    J.
      Nutr. 65:293-304.  (As  cited in U.S.  EPA,  1980.)

 Thompson,  L.  K.,   S. S.  Sidhu, and B.  A.  Roberts.    1979.    Fluoride
      Accumulations   in  Soil  and   Vegetation   in   the  Vicinity of   a
      Phosphorus  Plant.  Environ. Pollut. 18:221-234.

 Thornton,  I.,  and  P. Abrams.  1983.  Soil  Ingestion -  A Major Pathway  of
      Heavy Metals  into Livestock Grazing  Contaminated Land.  Sci. Total
      Environ.   28:287-294.

'U.S.  Department of Agriculture.   1975.  Composition  of  Fpods.   Agricul--
      tural Handbook No.  8.                                    •

 U.S.  Department of  Labor.   1978.   Occupational Health Guidelines for
      Fluordie Dust  (as Fluoride).   Washington,  D.C.

 U.S.  Environmental  Protection  Agency.   1980.    Review of  Environmental
      Effects  of  Pollutants:     IX.     Fluoride.      EPA-600/1-78-040.
      Cincinnati, OH.

 U.S.   Environmental  Protection  Agency.    1982.     Fate  of   Priority
      Pollutants   in  Publicly-Owned  Treatment   Works.    Final  Report
      Volume  I.      EPA-440/r82-303.     Effluent  Guidelines   Division,
      Washington, D.C.  September.

 U.S.  Environmental   Protection  Agency.    1983.    Assessment of Human
      Exposure  to  Arsenic:    Tacoma,  Washington.     Internal  Document.
      OHEA-E-075-U.     Office of Health  and  Environmental  Assessment,
      Washington, D.C.   July  19.

 U.S.  Environmental  Protection Agency.   1984.   Air Quality Criteria for
      Lead.    External Review  Draft.   EPA  600/8-83-028B,  Environmental
      Criteria   and   Assessment  Office,   Research  Triangle  Park,  NC.
      September.
                                   5-3

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Wright,  D.  A.,  A. W.  Davison,  and H.  S.  Johnson.    1978.    Fluoride
     Accumulation by Long-Tailed  Field Mice (Apodemus  sylvantuns L.) and
     Field  Voles  (Microtus   agrestis  L.)  from  Polluted  Environments.
     Environ. Pollut. 17:303-310.

Zimmerman, P. W.,  and  A.  E.  Hitchcock.   1956.   Susceptibility of Plants
     to  Hydrofluoric  Acid  and  Sulfur  Dioxide  Gases.   Contrib.  Boyce
     Thompson Inst. 18:263-279.
                                  5-4

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                                APPENDIX

           PRELIMINARY HAZARD INDEX CALCULATIONS  FOR FLUORIDE
                       IN MUNICIPAL SEWAGE SLUDGE
I.   LANDSPREADING AND DISTRIBUTE ON- AND-MARKETING

     A.   Effect on Soil Concentration of Fluoride

          1.   Index of Soil Concentration Increment (Index 1)

               a.   Formula

                    ...   .  _ (SC x AR) + (BS x MS)
                    Ind" 1 -- BS (AR + MS)

                    where:

                         SC = Sludge    concentration    of     pollutant
                              (Ug/g DW)
                         AR = Sludge application rate (mt DW/ha)
                         BS = Background  concentration  of  pollutant  in
                              soil  (ug/g DW)
                         MS = 2000  mt  DW/ha =  Assumed  mass  of soil  in
                              upper 15  cm

               b.   Sample  calculation

          0- qqa _ (86.4 ug/g DW x 5 rot/ha) + (292 Ug/g DW x 2000 mt'/ha)
                         292 ug/g DW (5 rat/ha1* 2000 mt/ha)
                            •

     B.   Effect on Soil Biota and  Predators of Soil Biota

          1.   Index of Soil Biota  Toxicity (Index 2)

               a.   Formula

                               i  x  BS
                    Index 2

                    where:
                         II - Index   1  =  Index  of  soil  concentration
                             increment (unit less)
                         BS = Background  concentration  of pollutant  in
                             soil (ug/g DW)
                         TB = Soil  concentration  toxic  to  soil  biota
                             (Ug/g DW)
                                  A-l

-------
          b.   Sample calculation  - Values were not  calculated due
               to lack of data.

     2.   Index of Soil Biota Predator Toxicity (Index 3)

          a.   Formula

                         (Ii - 1)(BS x UB) + BB
               Index 3 = —=	^	


               where:

                    II = Index  1  »  Index  of  soil   concentration
                         increment (unitless)
                    BS = Background  concentration  of  pollutant  in
                         soil (Ug/g DW)
                    UB = Uptake  slope  of  pollutant   in  soil  biota
                         (Ug/g tissue DW [ug/g soil DW]'1)
                    BB = Background  concentration  in   soil   biota
                         (Ug/g DW)
                    TR = Feed concentration toxic to  predator  (ug/g
                         DW)

          b.   Sample calculation  -  Values were not  calculated due
               to lack of data.

C.   Effect on Plants and Plant Tissue Concentration

     1. '  Index of Phytotoxicity (Index 4)

          a.   Formula

                            x BS
               Index 4 =


               where :

                    !]_ = Index  1  =  Index   of   soil   concentration
                         increment  (unitless)
                    BS = Background concentration  of  pollutant  in
                         soil  (ug/g DW)
                    TP = Soil  concentration  toxic  to  plants (ug/g
                         DW)

          b.   Sample calculation

                       0.998 x 292  ug/g DW
               n
               °'     "  454 Ug/g
                             A-2

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2.   Index  of Plant  Concentration Increment Caused  by Uptake
     (Index 5)

     a.   Formula

                     (Ii -  1) x  BS
          Index 5 = —=	•	  x CO x UP  + 1
                         BP

          where:

               II - Index  1  =  Index  of  soil  concentration
                    increment (unitless)
               BS = Background  concentration of  pollutant  in
                    soil (ug/g DW)
               CO » 2  kg/ha   (ug/g)'1  =   Conversion  factor
                    between soil concentration  and  application
                    rate
               UP - Uptake slope of  pollutant in plant  tissue
                    (Ug/g tissue DW [kg/ha]'1)
               BP = Background  concentration in  plant  tissue
                    (Ug/g DW)

     b.   Sample calculation

          0 qa7 _  (0.998-1)  x 292  ug/g DW     2 kg/ha
                          6 Ug/g DW         xug/g soil

               9 0.0786 ua/g tissue   .
               *       kg/ha          i

3.   Index  of  Plant  Concentration  Increment  Permitted  by
     Phytotoxicity (Index 6)

     a.   Formula


          Index 6 =
          where:
               PP = Maximum    plant     tissue     concentration
                    associated with phytotoxicity  (ug/g DW)
               BP = Background concentration  in  plant  tissue
                    (pg/g DW)
     b.   Sample calculation

          ,.  ,  _ 2745  Ug/g DW
          Z1'6  "  127  Ug/g DW
                        A-3

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C.   Effect on Herbivorous Animals

     1.   Index of Animal Toxicity Resulting  from Plant Consumption
          (Index 7)

          a.   Formula

                            x BF
               Index 7 =
               where:

                    15  = Index  5  =  Index  of  plant  concentration
                         increment caused  by uptake  (unit less)
                    BP  = Background  concentration  in  plant tissue
                         (Ug/g DW)
                    TA  = Feed   concentration  toxic   to  herbivorous
                         animal (ug/g  DW)

          b.    Sample calculation

               n  IAS -  0.987 x 6 Ug/g  DW
               °'1A8 "    40 ug/g DW

     2.    Index of Animal Toxicity Resulting from Sludge Ingest ion
          (Index  8)

          a.    Formula


               IfAR-O,   IS'55^5

               rf AR f  o,   ia  = 2£^-£§


               where:

                    AR  =  Sludge  application  race (mt DW/ha)
                    SC  =  Sludge    concentration     of     pollutant
                         (Ug/g  DW)
                    BS  =  Background  concentration of pollutant  in
                         soil (ug/g DW)
                    GS  =  Fraction of animal  diet  assumed Co  be  soil
                         (unicless)
                    TA  =  Feed  concentration  toxic  to   herbivorous
                        animal  (ug/g DW)

          b.    Sample calculation

                                   292       DW *°-°5
              If AR = 0,   0.365             7  nu
                                        40 Ug/g DW

              If AR * 0,   0.108  = 86.4 UR/R DW x 0.05
                                         40 Ug/g DW
                             A-4

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E.   Effect on Humans

     1.   Index of  Human Toxicity Resulting  from Plant Consumption
          (Index 9)

          a.   Formula

                         [(£5^- 1) BP x DT] + DI
               Index 9 =	
                                 ADI

               where:

                    15 = Index  5  = Index  of  plant  concentration
                         increment caused by uptake (unitless)
                    BP - Background   concentration in  plant  tissue
                         (Ug/g DW)
                    DT = Daily  human  dietary  intake  of  affected
                         plant tissue (g/day DW)
                    DI = Average  daily  human  dietary   intake   of
                         pollutant (ug/day)
                   ADI = Acceptable   daily   intake   of   pollutant
                         (llg/day)

          b.   Sample calculation  (toddler)

     0  2ns - f(0'987 - 1) x 28.3 Ug/g DW x 74.5  g/dayl * 825 Ug/dav
                                  4000  U8/day

     2.   Index of  Human  Toxicity   Resulting "from  Consumption  of
          Animal  Products  Derived  from  Animals  Feeding on  Plants.
          (Index  10)

          a.   Formula

                          [(Is - 1)  BP x UA z DA]  + DI
               Index 10 =	7^=	
                                       ADI

               where:

                    15  = Index  5  =  Index  of  plant  concentration
                         increment caused by uptake (unitless)
                    BP  = Background  concentration  in  plant  tissue
                         (Ug/g DW)
                    UA  = Uptake  slope of  pollutant in animal  tissue
                         (Ug/g tissue DW  [pg/g feed DW)~1)
                    DA  = Daily  human  dietary   intake  of   affected
                         animal  tissue (g/day DW)
                    DI  = Average   daily   human  dietary  intake  of
                         pollutant (ug/day)
                  ADI  = Acceptable   daily   intake   of   pollutant
                         (Ug/day)
                             A-5

-------
                         b.   Sample calculation (toddler)

»,   [(0.987-1) ac 6 ug/g  DW x 0.03176 ug/g tissueFue/g  feed!"1 x 0.97 g/davl  *  825  ug/dav
                                      4000 Ug/day

                    3.    Index of  Human  Toxicity  Resulting from  Consumption  of
                         Animal  Products  Derived  from  Animals   Ingesting   Soil
                         (Index 11)

                         a.   Formula

                              If  AR = 0,   Index 11 = (BS X  GS X "tp* DA) * DI

                              If  AR * 0,   Index 11 = CSC x GS x UA x DA) + DI
                                                                  ADI

                              where:

                                   AR =  Sludge application rate (mt  DW/ha)
                                   BS =  Background  concentration  of  pollutant   in
                                        soil  (ug/g  DW)
                                   SC =  Sludge     concentration     of    pollutant
                                        (Ug/g DW)
                                   GS =  Fraction of animal diet  assumed  to be soil
                                        (unitless)
                                   UA =  Uptake slope of  pollutant  in animal tissue
                                        (Ug/g tissue DW  [Ug/g feed  DW'1]
                                   DA =  Average  daily   human  dietary  intake   of
                                        affected animal  tissue (g/day DW)
                                   DI =  Average  daily   human ' dietary  intake   of
                                        pollutant (ug/day)
                                 ADI =  Acceptable   daily   intake   of   pollutant
                                        (Ug/day)

                   b.    Sample calculation (toddler)

                              0.206 =

     (86.4  lig/gDW  x  0.05  x  0.03176  ue/e  tissuefug/g feed]"1 x 0.97g/davDW)  + 825 ug/dav
                                         AOOO Ug/day

                   4.    Index of  Human Toxicity  Resulting  from   Soil  Ingestion
                         (Index 12)

                         a.    Formula

                                             x BS x DS)  +  DI
                             Index 12
                                                  ADI

                                                                 (SC x DS) + DI
                             Pure sludge ingestion:  Index  12          .__
                                                                       ADI
                                            A-6

-------
          where :

               II = Index  1  =  Index  of  soil  concentration
                    increment (unitless)
               SC = Sludge    concentration     of    pollutant
                    (Ug/g DW)
               BS = Background  concentration  of  pollutant  in
                    soil (Ug/g DW)
               DS = Assumed  amount  of   soil   in  human  diet
                    (g/day)
               DI = Average daily  dietary intake  of pollutant
                    (Ug/day)1
              ADI = Acceptable   daily   intake  of   pollutant
                    ( Ug/day)

     b.   Sample calculation (toddler)

     0 S71 = (0.998 x 292 ue/g DW x 5 g soil/day) +  825 ue/dav
          •                4000 ug/day

          Pure sludge:

                  (86.4 ug/g DW x 5 g soil/day) + 825 ue/dav
                          4000 Mg/day

5.   Index of Aggregate Human Toxicity (Index 13)

     a.   Formula
          Index 13 = I9 + I10 + IU *  I12  -  ()

          where :

                 Ig = Index  9  =   Index  of   human   toxicity
                      resulting'    from    plant    consumption
                      (unitless)
                    = Index  10  =  Index  of   human   toxicity
                      resulting  from  consumption  of   animal
                      products  derived from  animals feeding  on
                      plants (unitless)
                    ~ Index  11  =  Index  of   human   toxicity
                      resulting  from  consumption  of   animal
                      products  derived  from  animals  ingesting
                      soil (unitless)
                Il2 = Index  12  =  Index  of   human   toxicity
                      resulting from soil ingestion  (unitless)
                 DI = Average   daily    dietary   intake    of
                      pollutant (ug/day)
                ADI = Acceptable  daily  intake  of   pollutant
                      ()ig/day)
                         A-7

-------
          b.   Sample calculation (toddler)

          d.569 = (0.205 * 0.206 * 0.206 * 0.571) -
 II. LANDFILLING

     Based on  the recommendations  of  the experts  at the OWRS  meetings
     (April-May,  1984),  an assessment of  this reuse/disposal option  is
     not being conducted at  this  time.   The U.S. EPA reserves the right
     to conduct such an assessment for this option in the future.

III. INCINERATION

     Based on  the recommendations  of  the experts  at the OWRS  meetings
     (April-May,  1984),  an assessment of  this reuse/disposal option  is
     not being conducted at  this  time.   The U.S. EPA reserves the right
     to conduct such an assessment for this option in the future.

 IV. OCEAN DISPOSAL

     Based on  the recommendations  of  the experts  at the OWRS  meetings
     (April-May,  1984),  an assessment of  this reuse/disposal option  is
     not being conducted at  this  time.   The U.S. EPA reserves the right
     to conduct such an assessment for this option in the future.
                                  A-8

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