United States Office of Pesticides arid Toxic Substances Environmental Protection Office of Pesticide Programs (TS-766C) Agency Washington. DC 20460 EPA Pesticide Fact Sheet Name of Chemical: KARATE (PP321) Reason for Issuance: Conditional Registration Date Issued: May 16, 1988 Fact Sheet Number: 171 1. DESCRIPTION OF CHEMICAL *_ Generic Name: PP321; [ 1 alpha(S), 3 alpha(Z)]—(±) —cyano—(3—phenoxyphenyl) methyl 3(2—chioro— 3,3 ,3—trifluoro—l—propenyl )—2 ,2—dimethyl— cyc]opropanecarboxylate. Common Name: PP321 Trade Namer KARATE EPA Shaughnessy Code: 128867(a) Chemical Abstracts Service (CAS) Numbers: Year of Initial Registration: 1988 Pesticide Type: Insecticide Chemical Family: Synthetic pyrethroid U.S. Producers: ICI Americas, Inc. Wilmington, DE 19897 2. USE PATTERNS AND FORMULATIONS Application Sites: Agricultural use in/on Cotton Method of Application Foliar ground and aerial application Formulation Types: 13% liquid (EC) Application Rates: 0.01—0.03 lb.ai/Acre Usual Carriers: Organic solvents: Surfactants Limitations: RESTRICTED USE pesticide. Use limited to certified applicators or persons under their direct supervision. 3. SCIENCE FINDINGS Summary Science Statement : *pp321 comprises one of two diastereomers (enantiomeric pairs) of Cyhalothrin. Cyhalothrin consists of 4 cis isomers in the 2 configuration (enantiomeric pair A & B) of which PP321 consists of 2 cis isomers (enantiomeric pair B). ------- 2 Technical PP321 is a synthetic pyrethroid with moderate acute toxicity. The results of the acute toxicity on the end—use formulation indicates that product is of moderate to high acute toxicity. The end—use product is extremely irritating to the skin and is a mild sensitizer. Technical PP321 is not considered to be mutagenic or teratogenic in test animals. On the basis of structural considerations and metabolism and subchronic data on both PP321 and cyhalothrin, the Aqency has accepted the long term data on cyhalothrin in partial fulfillment of the chronic toxicity requirements for PP321. Sufficient data are available to characterize PP321 from an environmental fate and ecological effects standpoint. The results of acute toxicity studies indicate that PP321 is extremely toxic to fish and other aquatic organisms, but is practically non—toxic to waterfowl and upland game birds. However, reproduction data on mallards exposed to cyhalothrin domonstrated adverse effects on numbers of eggs laid at doses of 50 ppm, with a no-effect—level (NOEL) of 5 ppm cyhalothrin. Since technical PP321 is the more biologically active component of cyhalothrin, it may be more toxic; therefore, the Aqency has determined that the repro reproduction study be repeated using technical PP321. An acute contact LD5O study indicated that PP321 is highly toxic to bees with an LD5O of 0.909 ug/bee. Formulated PP321 is also highly toxic to honey bees with a reported LD5O of 0.098 ug/bee and an oral LD5O of 0.483 ug/bee. PP321 is readily degraded by soil and is virtually insoluble in water. There is little or no potential for leaching. The Agency has determined that the registration of PP321 may effect endangered aquatic and avian species. Pending a formal consultation with the Fish and Wildlife Service to determine use limitations with respect to these species, the product label contsists of language which will mitigate the risk to endangered species. A Tolerance Assessment has been conducted by the Residue Chemistry Branch to provide a dietary exposure analysis for the use on cotton. The refer- ence dose (Rfd) used to determine this dietary exposure is calculated to be 0.005 ppm based on a NOEL of 0.5 mgI kg/day from a 3—generation rat reproduction study and a safety factor of 100. The Theoretical Maximum Residue Contribution (TMRC) for the U. S. population is imately 2.6 % of the Average Daily Intake (ADI). ------- 3 A. Chemical/Physical Characteristics of the Technical Material Physical State: liquid Color: light yellow Odor: aromatic solvent odor at room temparature Melting Point: not applicable Vapor Pressure: 2.1 x 10—8 rnbars Density: 0.830 + .005 g/mi Solubility: 0.002 mg/mi at 20°C in water pH: 5.6 Octanol/Water Partition Coefficient: 4.2 x iü B. Toxicological Characteristics : (Technical PP321) Acute Oral (Mouse): males: 79 mg/kg Toxicity Category II (LD5O) females: 56 mg/kg Acute Dermal: males: 632 mg/kg (LD5O) females: 696 mg/kg Toxicity Category II Primary Dermal Irritation (rabbit): PIS= 0 Toxicity Category IV (none observed) Skin Sensitization (guinea pig): not a sensitizer Acute Inhalation: LD5O (4 hour) males: 0.315 mg/i Toxicity (end—use formulation) females: 0.175 mg/i Category II Teratology: (rat) Maternal NOEL = 10 mg/kg/day (Cyhaiothrin) Maternal LEL = 15 mg/kg/day Fetotoxic NOEL = 15 mg/kg/day Teratogenic NOEL = not teratogenic (rabbit) Maternal NOEL = 10mg/kg/day Maternal NOEL = 3Omg/ka/day Fetotoxic NOEL = 15 mg/kg/day Teratogenci NOEL = not teratogenic 2—Year Feedina/Oncogenicity: (rat) Oncogenic NOEL = 2.5 mg/kg/day (Cyhalothrin) Systemic NOEL = 0.5 mg/kg/day (mouse) Oncogenic NOEL = 15 mg/kg/day Gene Mutation (Ames): negative Structural Chromosome Aberration: negative In Vitro Cytogenetics Assay: negative ------- 4 PP321 formulation— 13.1% Acute Oral Toxicity in rats: Toxicity Category II LD5O = 64 mg/kg Acute Dermal Toxicity in rats: Toxicity Category III LD5O = >2000 mi/mg Acute Inhalation: Toxicity Category II LC5O = 0.315 rng/l(M); 0.175 mg/l(F) Primary Eye Irritation: Toxicity Category II Primary Dermal Irritation: Toxicity Category I PIS = 6.7 Dermal Sensitiztion: mild sensitizer C. Physiological and Rio1 ’icai Characteristics The mode of action in bioli,qicai systems is stomach and contact exhibiting neuropathological characteristics typical of pvrethroid insecticides. Slight repeilant effect. Foliar absorption: N/A Translocation: N/A D. Environmental Characteristics Adequate data are sufficient to define the fate of PP321 in the environment. PP321 is stable to photolysis at environmental pH and temperature. It photodegrades rapidly and is practically water insoluble. Tinder the conditions of the soil TLC test using various soils, (aged and unaged) PP321 residues are considered immobile in soils with a half—life of <14 days in silt and 28—56 days in clay loam, respectively. Anaerobic conditions did not alter either degradation rate or products. It has a bioaccumuiation factor in fish of 858X. Residues are depurated radidly in untreated water. Accumulated residues are found in non—edible tissue. PP321 and its degradates do not leach into the soil. There are no concerns at this time in regard to ground water. ------- 5 E. Ecological Characteristics Avian Acute Oral: Mallard duck — LD5O > 3950 mg/kg Avian Subacute Dietary: Mallard duck — LC5O 3948 ppm Bobwhite quail — LC5O > 5000 ppm Freshwater Fish: Bluegill — LC5O = 0.21 ug/L Rainbow Trout — LC5O = 0.24 ug/L Freshwater Invertebrate: Daphnia magna LC5O = 0.36 ug/L Marine/Estuarine Invertebrate: Mysid shrimp — LC5O = 4.9 ng/L Eastern Oyster ECSO = 0.59 ng/L Marine/Estuarine Fish: Sheepshead minnow — LC5O = 0.807 ng/L 4. Summary of Regulatory Position and Rationale The Agency has determined that it should allow the conditional registration of PP321 for agricultural use to control insects in/on cotton. Adequate data are available to assess the acute and chronic toxicological effects of PP321 to humans. However since certain long—term fish, aquatic and avian data are missing and required, the registration is being conditionally approved with an expiration date of August 30, 1990 which coincides with the dates for submission of the data recuired to satisfy the remaining data gaps listed he1o . In 7je’4 of the high toxicity of technical PP321 to aquatic organisms (invertebrates and fish) and the potential hazard associated with exposure to this product, the Agency is concerned about exposure which may result from improper application or use and so is restricting use of this pesticide. The Agency has determined that endangered species labeling restrictions are necessary to protect endangered species and is requiring specific limitations on use of this product to prevent or mitigate exposure. 5. Summary of Major Data Gaps 1. Avian Reproduction — Mallard (71—4) A final report is due in May, 1990. 2. Fish Life—Cycle (72—5) A final report is due in August, 1990. 3. Aquatic Invertebrate Lifecycle (72—4) A final report is due in August, 1989. ------- 6 6. Contact Person at EPA George T. LaRocca Product Manager (15) Insecticide—Rodenticide Branch Registration Division (TS—767C) Office of Pesticide Programs Environmental Protection Agency 401 M Street, S. W. Washington, D. C. 20460 Office location and telephone number: Room 211, Crystal Mall #2 1921 Jefferson Davis Highway Arlington, VA 22202 (703) 557—2400 ------- |