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Plant Name:
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Run Number:
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Page .J-
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Test Date: -- 5'-' ~!L_._- u-.-..---- -.--.. --..
Operator: C G"4 -~
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Traverse 8'mpll"I/ Cod< Time Gas Meter Velocity OrifICe Pres. OiffercDliai Stack Pr. Impinger Dry Gu Meier Temp. Pump -
Point Time. (24-hour Readin, Ilead ~ PI) (cll) in. 1120 Temp. . F Temp.' Filler Temp. Inici vUuc, Vacuum
Number (min.) dock) ("- \ ftJ 1n.IIzO Desired Actual (1;) Temp.. P 8p ("18.. ). F fli....) .p In. III
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o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: ~P4 QoKe.- £.dhl.Ji~1Y1 <'r~ CIt.9~kl1. :r=tJ
Sampling Location: 0~ ~~I\I Jf.L""- :r 1'\ J e.., -+
Sample Recovery Person:_R\-<. /' 'RD
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Sampling Method Type: M '3 j 5
Run Number:~ - I- M:SJ5- I Impinger Train ID: ),j-lsJ.
Job ~rumber: ~.sQL:,. CXYJ
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Date: 'l!(I/qr
Field Team Leader:-1lS'
Front Half Data
Filter No.: 0'6 () -, ~ ~ - 05 Filter Media Type: 7 ~
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Tr- S8mpIng Cock Tme Gas Meter Velocity Orifice Pressure Difterential Stack Temperature Impinger Dry Gas Meter Temp. Pump ,
PoInt Tine (24-hour Reading Head (t.p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) II S in H2O Desired Actual (Ts) Probe Filler of (Tm in°F) (fm out oF) (in. Hg)
R ,. n '\}."). O).~ 1.o'\J- W//////////////////~ij'//,7 f /////~////////////////////~
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FIELD DATA SHEET
Plant: ~., ~ \"", ~\I:.c.. "-
Sampling location ).. ... \.. ... ~
Run Number: ~J.t"o';),s-t.. Date: ~ - \1 ~9 '6
PrelBst Leak Rate: ,00, elm @ ~ in. Hg.
Pretest Leak Check: Pitat: -d. O~: J
Sample Type: ft\ ~ \s Operator: ~ ~ N{-
Poor: 'd-Ot. '6 Ps: -"2. 3
C02: , S 02: d () I 5
Probe LengthfType: \ 0' (,1."'>') Pitot II: .tQ1o
Slack Diameter: \ \ +- As: 1 D . i ~
Avm-.J23 .57 ~ ~=
'Ji",
tJi..
Ir= ?-;;LS
Nozzle ID: . 1. \ 1; Thermocouple II: 12. p 1.. b
Assumed Bws: -J- Filter II: b'j () 7 q g - 64-
Meter Box:ll: , Y: 1. 0\ 1- llH@: 1. ~ ~ 4
Post-Test Leak Rate: ,0 IS cfm @ ~ in. Hg.
Post-Test Leak Check: Pitot: V Orsat: ==--
Tm=
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Run Number:
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Point Time, (24-hour Readine lie ad ~p.) (~I) In. 112° Tcmp. - F Temp. I Fillcr Temp. Inlet UUIIC:I Vacuum
Number (min.' dock) ""ft' In. I h 0 Desired Actual f1:) Temp.- F 8p (18... )8 F (li...,) 8p In. III
I I~~~ O~JS . QC4 \. C; I IS 3(n )J,S I 'l.~D 55 'oJ). IP J
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Plant Name:
Run Number:
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Test Date: __If - /?~ r -.-- __h_..._-. -.--.-.
()perator: C G~~
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Point Time, (24.l1oor RudinS lie ad ~ PI) (dl) hLlIJO Temp. . F Temp.' Filler Temp. Inlet u~~.)t. Vacuum
Number (min.' doclt) '''- \ ft] hLllJa Desired Actual ("t) Temp!' 17 .17 rr.... )8 F {"1i.F In. III
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Test Date: __LLu~--- --.--...--- -.--..-.
Opera tor: G c.",",
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ruinl Time. (24-hour Re8dinc lIead ~ P,) (611) IlL 1120 Temp. . F Tcmp. I Fillcr Tcmp. Inlet UUllcl Vactluln
Number (min.) dock) (" ) ft J IlL 1120 Desired Actual (1:) Temp.. f 8f (18.. ). F ("Ii.....) .f In. III
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o PACIfIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Plant: ~~L ~- Efff {gk,-
Sampling Location: B~ ~
Sample Recovery Person: 1../.. I ~ D
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Sampling Method Type: tI'1f 1, 15'
Run Number:_B~.7 - JIS" 2-
Job Number: SSt()("." 00
Sample Train Recovery Data
tZJerlw.r :::tJ.
Date: S' / /3/'19'
l {
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Field Team Leader:
Impinger Train 10: /f/ ". $
Comments:
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Filter No.:...J)JJ079~ oL/ Filter Media Type:
Filter Description: 15 (c..c- k. I J., ~o.....v /
Filter No.: 6 C( () 7 ~lY - 1'\ ' ;?rter Media Type: '1 liLt',P c:t
Filter Description: f?, /t?-t c. k- [,.,. ~ 10 f), C;- ~..J
Front Half Data
6/-' f'w /:-/.t",r -~/4/
c~ !e;.S '5 or; bp.-
....
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml): C. (9. ~ .,/
Description of Impinger catch:~~ (I"'r ~
Impinger Purge-
Start Time:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Back Half Data
Flow Rate:
I
I
\ Stop Time:
Purge Gas:
Impinger 1
1:1EJ-.c. Hz.D
tottt,.7
-..lID.?
3(.0
Impinger 4
Impinger 2
JJf{"'t:... h~D
o 3:;(. 3
~:~
Impinger 5
Impinger 3
/~P?-
~r{.O
' 7~5
10 ,~
SiIi~i Gel I
SI
-------
ji
,
FIELD DATA SHEET
K-= J.)'5
Nozzle ID: ,1,) Thermocouple II: [D20
Assumed Bws: ~ Filter II: 051 67 9 J- I~
MeterBoxll:L- Y: '.Oft l\H@: I.9S(
Post-Test Leak Rate: .0(\ 10 cfm @ .4::-in. Hg.
Post-Test Leak Check: Pitot: ~rsat: i/'
Plant: ~ t-, \\ \.. 1\ '" S ~ c ~ "-
Sampling location ':+ '\J l..t- "\ ~ t.. b J.). '0 '") :3 D S ~ 70 {. c; '1
~"';, \<().'6 ." ~ \,4- ,.~ ~1.1... - J.)~ ?-dcr rl fV bq d
~1\.5 \('\~'6 . Ob'" ,c>()t; II~ 1 ..,.~b 4-1( 10 be, ~
.OOC, I ~').5
1.055" , S 1.,. --z..., .,.5 \.1- ',4- 347 !'lJ.:> ').).. '1 .51 '70 &;0 4-
9S. \5<1. t.. 1
I OC) ~ , nl> "I ,00<"1 I noe: 0-0 'j j "L "1.- ').)-) "J.~o SJ- '80 76 '2....r
~ -"0 q"\ 0 \(., )_'V .OO~ . 00'; , 00") \ I 1...- 'J. ;)..) J-]t -5~ >f\ ,1 L-
fo\,)\ \L').~ \ ,e, 1 q. 1,4- "\1~ ') ~J ?- '), .TJ ~). -" ~
'" y,\ \10" "" ,bQ~ Qi) '\ , t'lQ" \ & 'JI "})( ,~ 1 .1"4 ~).. 7' '1..
~~r \ ". (" . It. \. n \. 4- "". )3)- '").}.t,. '):)~ ~" 'it', J~ 4-
G\"'.. \ (" (,., 4- '''o~ . 00'" .01.1<\ Lf~ ").~5 ).-)0 5" ~~ 7y '-
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'\5)- \~.}. \ or ~ ',1 \. '- ".>\-1 J~..s ?-~; ~~ ~.5 -,C; -u
1\.. 4- "\ 'Ol\~ \41 ") ). \ ')) ').. ').. ~,.5 '):;, 5~ g1 ~1 4-
\'" \0.. \1 \ \ ~ .tI~ ~ .00" .('70 ~ \ ~ a... ") ~C) "\ ." 0 Sf.. ~? ~\- 1.
t-:J' \f\'~ \..,(',4- ,bo .) '00' ,001 ').c.. 'p..") .'). :) I S' \( ~~ 1.
\1)}3 \ lfo 't\. .~()') . c.? O~ ,o\)~ , I 4- '). ). S #;() $1 ~
,9~
cP~
I
-------
Test Date:
Operator:
Page '-
g - I 3.. I. ) :; 1, 4- ").)~ I .}~o $1 ~~ ~" 4-
1 'O~~ \ 1 ", ~ ..00" ,00<1 .o~c, 17) ?)"'6 I ')..~'J,.. ..r~ ~, V~ "L
~," I 'O4.~ I i () ,f:- 0<;)1, .00 q .f') D"\ lIb ?>~ I '].:>() "S'1 >'9 ~G L
1 In41 'G" ,) ,C\L 1,4- 1.4- )9~ '} ~"I '}3 1 .5"1 ?'j 8'-' q,
I II) <1. '1 I ,p ,4-. ,06> .00"" ,on l 'd7 ')~5' ;))0 sa ~1 !>b ~
, \0,<; 1. \ 1 7.-
AI 1 IIi:) 6 \S?(;;.,'1- . nh... ,001 -001 D1 ).~o I ) :J..c, $'( qr ~)' "L
I II C& ,g~. 'f> . q'i? 1.4 \,4- ~ \.~ 'J11'~~~ S"7 "/ 8'~ 4-
I ,\ 10 l ~ 1 ,q \Ot:1~ .oo~ .oo~ \ 1 ~ ?1' 1)..30 S~ cr ( rty '-
'\111 \ 'R"I,,' .OoJ .nu~ . ()(~"I 11'1 d>-t-I ~:2~ -J'1 qL. p~ "L.
1 \\,<6 1~1/c.. . q ',1 I.L. leL l~J.. '»5' 'J),\ 5.5 C;L t61j 4-
I \\ ')c) l'\D,~ IOO~ '~D" .001 tS~ ''). 'l.5 I ')~., St:.. q)- 'b'¥ c-
I 1\ '}1 \<\1.~ '00) ,Ooe, (000, I~ 3 1..)3' )30 57 q/ 8''\ <-
f\~ 'n;o ' cn.~ '00) ,00"'1 10(.>~ 1~7 '}.).. ~ I ?'i ~7 "I ~c; 2-
I \\)~ \'\~..5 .~.s ,;+ \ I'" -~ +-1 d 70-~ , ) ~o $1 q, ~1 ..,..
1 \ \ ,",0 \..,5.~ ,()D~ OQ~ 0 DOl" I~"r 1)~ I '"} ~1 .rc. '(D ill .1-
I \\&,\ \C\1.~ ,'\5 \ . \- \. ~ ~> "').") " '')~'& $1 .10 CJ "" q.
I "~~ \q~\\-- .\)0' . n {)"\ ,OoC\ \ $J ~ } J&. I ?).~ SS 'it> ~"t 1
i\ ~ 1 \\S4- \I\~,\- .OCI' .OQ<:!f .00 ., \ )- t.o '1-" I '} ':>b 5b CfO ~c, 1-
'\\.51 100,?r , ~)'" \'1- '" ,").. ~f.~ ~ jJ-~ I ').",)'\ S.:s o.~ ~1 ~
I \).., ov ~o \," ..~O~ -00"'\ .0", \C\-~ 'n-It I 1)\ S~ "'-\J "S'b '''A-
-------
Page
~
of
5
Plant Name:
Run Number:
~e., \t L Q.,'-\~~
5:>\(f.\.
Test Date: __-1..:lil1.._,-- -----...--- ------.
Operator: ~ ~ t-\{
~~ \", ,\S -")
0.09;
Traverse So"pll"I/ Ood< TI..e Gas Meier Velocity OrifICe Pre.. DifferealiaJ Stack Probe Impinser Dry Ou Meier Temp. Pump
Point Time, (24-hour Re8dinc I lead ~ PI) (cll) In. 1110 Temp. . F Temp.' Filler Temp. Inlel UUIICI Vacuum
Number (min.) dock) ,"- UP in.IIzO Desired Actual ("t) Temp.. P .p (18.. ). F (li_l) .p In. III
~ " I ,~~c." J 0"'" "'71 ,ot)'" .~~ ~ 106':> '00<1 .00"'1 ~,D ..] ,.. Po..$ , ?;) \ fJ f7 ~">' Z
, 'L~c:;' 'LD'1, 6 ,'8 r \.'1 ,-" ':, \ \) ?}c\. 'i-'~ 5"3 8" tl7 t/.. ((
1 Ii- ~j a.. \0,1.. .00'" ,00"1 .00; T7.,,,, )).5 '7- 3n Sf ~<. $'5 <- ~
4...~... 1 1) 4--~ ?-\ 1 '~3l 00:> Cc>Of 'Ov"'1 , '&) ').~~ 1 )..,~ ,so ~~ ~S '- . Co I
1 ,
g-.1 I 1~>1o. ~\\4-:>\ 'boQ -l")!\~ r). J, ))5 I 1.~).. C, I 7~ )¥ ~ '00
"O\,,>~ ,"
, \'1 \D 1..,1..1 .q~ \, ~ \.") "-ell :J. ), I 'J~J ..1, 7x 7'6 il
1 \ ')., '") 1\ ),1> ,,(>0 '7 ,01:> "'1 1>0" t40 ');7) I ":J I $7 ~7 Y 7~ ~
1 '~41 ""). \ 4- . ~ ICO"'J ,()oq , (') co. ., 1).5 )..~ I ').'3)... S ("1 '?JI 7x- '-
I (~5v '"l.1.s ,v .'11.. \ ~ l"\ ~ 1--0 ').~ (' , ~?>o $'7 {'iJ , ~ 7.J
I \ 1.,57 ").\(0.'" , () \)'" ,n 0 '\ (00'" I C. 1 ")." '''l~' S7 'D f ~ '\..
p - 'Z.... , \ 1.. ~"\ '), \ ", ~ 'o\)~ ,0()"1 ,00'1 I ;). f:? l..W/'').~1,) S 'i. 80 I~ '-
1 \ &'0;' d- \ ~- ""' ,q 1... I, '\ 1.3 ~(. z... ,)~c:. I )"<1 5"6 QD ')v ~
1 , ~. ~s- '::119.1 ,ou~ ,01.1 'i .000, If' ').'),,1 'd'3v Sb 'if 0 lit L-
~-.3 1 \ frJ.' ""t..1.."t.~ 'OO~ DOq ~o(,/ ... IJ. () I~"'" ',~- ...r~ 9)... 7"i -J-.J.~
1 '''h \-~"). ~ \ ') 1... \.3 I.:; ~ \.5 ')-').~ ':J.~~ S1- "U' IJ ~:»
, 1 \ ~'X- "). '}'Jo. - Q, .~""> '0'-''\ ' () ()o, 1~3 ').).(,,). J{) ;fS ~.:3 80 -z.-
~-~ 1 \ \-4. ~ ')~1,~ ,00"':1 'oo~ .00'( \\\ '). ?..s '~)'1 s.,t "-,, ,~ L.
1 \~ '} ~o, \ ,Or)'J If"t.~ q \f) /) Cf 'to. <:. '1-""~')-~:' SI ~l ~\ 1-
1 \So:, 'J? , , ~ .0 I) ~ .n~\ ...,,'" \ t;) ," '). ') ~ ' d-'J'5 ~~ '8$ ~r 1...-
\\.,c.. I ~
-------
Page
'T-
of
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Plant Name:
Run Number:
~~, ~ L.~\}. ~ ov' ':),Cc l
~~ ~:,,~"':> .
Test Date: --~..::..\ y~.)-- --.--...--- -.--..-.
Operator: ~ ~IV
Traverse samrllnl/ Cock Time Gas Meter Velocity OrifICe Pres. Differeatial Stack Probe Impinger DIJ Gas Meter Temp. Pump
Point Time. (24.hour Readinc lIead ~ p.) . (~I) 1n.IIJO Temp. . F Temp.' Filler Temp. Imct VUIICI. Vacllum
Number (min.) dock} ("- ) ItJ in. 1 It 0 Desired Actual (1:) Temp.8", .... fr.... ). F (~"".).... In. III
~.c:; I '..q 1- '))),1.., '''3 . eor;;'\ .0,.,'\ \ 16 1 ").).c. I )."), 5"' ~J 3).- "'-
I , 5 \ '1 1-".15 I I;) , B 11 \ ,4- ,,4- ~I.J ).;J-~' ?-~o S1 ~~ q'l- 4-
I \S '}- \ ').~~, \ . oc") . ()() "I ,OoG1t 1(,.0 ? :).~. I :) 3 <> J7 flJ qL Z.
I \S~D ?"Yl, 5 \. L i..1 t,7 37"1/ ),l.d.' J~r. .s-~ "5 ~}- 4-
I 151')- d~1I, 1 .oo~ .001 .00; III ,. ~s I;:). >0 .51 ,s 8). <.
B~ I 1..5 "\ 1., '}::!>'IS,'1 (00) ooi 'Oo~ \J.G ,)-~ I ')::'0 ~o ca'~ ~) oz......
, \ .540 '"). ~ 0, 1..- \,L l, 1 1., 3 1-0 ")).4- '?~I So &,$ £)3 4-
, ~ S +L.- ."} \- (), ~ II!) ol.. .I/IA"! .00'\ (75 ")")-4- ' J2>,-> 4- "I <1.6 S/> "t..-
I \ ~ li'n ').4-) ,., IL \.'"L \.1 4-l0 ').)-oS ' ;)'3" .s~ 9~ 4-
I \oS .s r "}t 4- \ ,QI)~ ~ .00"1 \t'6 I)..~ I ")1:. +1 8~ S'~
,00'\ L
\) 1 I \ S-Sl '~1-S, J- ,0.:> ~ . 009 ,0,)'1 It"L ") ."..5 , ")~~ :J'7 ~(;, 9'3 '2-
I '-'00 '1- ~5 . '" L)' \.1 \.1 :'40 ?;)$ I ")3 I S'r g-, 9.!1 4-
I "t>"1 ') 61' 0 \OO~ ;01>", lOb"'i t-' )- ')}-oS I ?~ b s4- {(-' q~ ~
I \I.o\v ';} 4~ 1"'1 .'\,L \\4-- ,~ ,,->, ~ }H.' J/b ~I. ~b )') 4-
I \ b \'1.... ') \",,1 . tH>.~ . 0 t1.Oi .000\ \55 '),S I )~o .("::30 g, QJ. 2-
I \1.1'1\"\ d5\. + . q l... 'I (\.. \ ~ ~ \""L. 1-)t I '}~ b .s3 '1 .o\}~ 1~1 ;)~ I J -:>/) S'3 c;,."") 71~ ~
I \ I,,~:> ')..:.r 4 ...., ,0<.:>..... 1:1..:. "I tOO \ \I:J ')).4; ' ).},'.) s~ ~") ~4- ~
I \ ~ ~b ').5.s. ~ ,~9 \. " \ I 6.- )00 ')~.5 I.}~; S~ ~J is'~ ~
I \~ ")1 k 5<, , ~ ,O()~ ,00 " . () 0""\ ~n 1-H '').. '30 ~J.- 11 'it- 6
I lIo'~ ~s, \\ ,\') \) ~ I""In"'\ . DI,"- P-~ "")..")-:) , ").--:1<; .$~ 9( ~'J- ~
t>"\ I \10 4fp ?-$ ~.Io .c)\).... ,at' C\ .ObOt \ \S '"')Y.I, ' '}!to S"f.. ~" If\. 1..:....-
, Ib~\ Is. C(, . "\ . ~')- , I'?> \.) ~o.... ').)C) ,;}~, ss 8~ ~.s 'cl
-------
Page
s
of
5
Plant Name:
Run Number:
'61-' T ~lr: H<-t1
:>1~e \....-
Test Date:
Operator:
_J- , ;.~--,-- -.-.--.,.--- -'-_U-'
C. G"\'1
'R~ ~"1'~15-3
Travcnc SamPUoi; Cod< Tim. Gas Meter Velocity OriflCc Pres. DiffereDlili Slack Probe Impinp:r DIJ Ou Meier Temp. Pump
Poinl Time. (24-hour Readinc lie ad ~p.) (cll) lo.lIJO Temp. . F Temp. I Filler Temp. I nlct UUIIC' Vacuum
Number (min.) dock) '" ) It J io.llzO Desired Actual ("t) Temp.. P .p ("18... ). F ("Ii_..) .p In. III
11,q I \en 5"t- ";)"'I.D .Q()'" . 0'>" .00<1 I , Cf '}";}$ I '"). 1~ S"4- ~"I illS "L
I 'QD~ ?r.. ~J.' '\ ,~}- \.~ \.~ !:o) 0 ?;;I~ I ']]'1 $'~ C;~ ~r.s 4-
I \ ") 05 -)(Q~.~ 00) '001 ,1"109 \ 7 ~ ?dS I 1- 3D 5"3 %'1> 'i-S '-
{I,- 10 I 110' '1-~ ~ ~ '()o,.) 60 '1 00"1 ,~S 'l '#; I }~ I $'7 ~~ ~5 'z...
I ,'1 \1... J G, S. '1.,. ,~>- \-:, I. j 31 L '))-.$. I").!t() SO 41( ~s, 4-
I \"'\'4- ."). (,,, ,4- ,00:-, .OOc1 ,00" I S" I ?~. I ').)G SI '-r &-5 <-
I \1 1.0 '/bl,1 Oc)) . tJo c; ooC) , I '1 '). .,.5 I ') J 11 s~ 8Cf ~, L
I \'11~ ~~~. \ \,\ ,. C; L..:5 /k), 'J.).3""' I :1)0 .5"2 rc; ~~ f
I \I'J.S 'd re.q I "\- . bC'''' .OoCo .00") \44- ") >.) I ., ~o .s~ 8\ ~! '-
I \,:J ~ :l'l\.~~ . 00"> . r)(,q 06 ~ , 1. ')- )).fo I 'j -;1~ ~" ~~ ~~ L-
I I
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-------
~
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
..--
.SIB ..
r=:Jc:::::JCJ
C1 PACIFIC ENVIRONMENTAL SERVICES, INC
Sample Train Recovery Data
Plant: ~.~ SUeJ-ffA Cok,-~. ~.,.,t:-... Date:~
Sampling Location:~M, :£:./i}- .
Sample ReCOVeIY~: '?SJ r';: " Field Team Leader.~~U
Sampling Method Type: £:Pff 915
Run Number: 15 - E- ?;/5 -:3. Impinger Train ID: ~/-ft;
Job Number: S'S'otz. fJ&){)
;) (': {-h(~ vS" L
Comments:
Front Half Data
- ,/
Filter No.: tJ 0 :)t4K.=J"7 Filter Media Type:
Filter Description: ),Il?~ v 'i 0 b. Q ~
Fi!~er No.: Dcr O'? q t - I I Filter Mecj~ Type:
Filter Description: i-l.Pb. ( "7 bID. (: k
Back Half Data
Impinger Purge-
-
Start Time:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
~ ~ ~4-
-rC'~ C' d.: ~ 1c"c-~5 ,::.~' b c,.-
-
-
Purge Gas:
Flow Rate:
Stop Time:
Impinger 3
r£V3
~
-(] '7
Silica Gel
~L o;Jl
~::: f (f({
(g): :2 I , f'
Impinger 1
flPL c ~()
&57~3
L9?c' .\
()" ~
Impinger 2
Jlf'iC f!z tJ
'~D.o
-G~y
Impinger 5
Impinger 4
,---
",--
-
-
--
/'
5rJ'7
-------
FIELD DATA SHEET
Plant: ~~\,. \. "'-a...A S ~«- \
Sampling location ~""4 ~~~
Run Number: B-':C ~ :. I~~ ft.Date: D'"d - Ii( - ~ 8
Pretest Leak Rate: .('}o~ cfm @ I~ In. Hg.
Pretest Leak Check: POOt drt-O~: -
Sample Type: 31~ Operator: '.I>b ~-
Pbar: .;;:A. "7 Ps: -
C02: 0 02: ..)0 . <;
Probe L~nglhlType: ~'15~Pitotll: '" A
Slack Diameter: , I q :
Nozzle ID: . OJ loS Thermocouple II: ~ A.
Assumed Bws: ~ Filter II: 0 ~o.,) - ; 8- ((
Meter Box #: MB-I Y: I. oIl 6H@: 1.Cf.5f(
Post-Test Leak Rate: i!!>o.,). coo @ ~ in. Hg.
Post-Test Leak Check: Pitot: ~O~I:-=-
TreY"'" Samplng Cock rlm8 Gas Meter Velocity Orifice Pressure DiftBrential Stack Temperature Impinger Dry Gas Meter Temp. Pump
Point TIme (24-hour Reading Head (6p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) It S in H2O Desired Actual (Ts) Probe Filter of (Tm 1n0F) (T m out oF) (in. Hg)
o J '"J.I~ .J/~. Ol:f7 ~////////////////////////// f/////// .-07//////////// / / / / / / /Y.
I~ "DO ji~ ") =s '5 ~'p.. ~I~ ~ A * .,.;I~ ~SO gob ~'II ~I\I\
3c 1"7''5 .:)f~.~~< t.J , .0. " .;>~.:'\ I:; C> 8t:> , \ I
lIS ,.,;) "7 ~ fI '"Y5 I I I ,;)q~ ~D ,l.
17~ "'>1 A ,') X' I at./S ~
\J I
I
I
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I -
-
-
1$ "
C). oe..1
AVm-
~..
AH"
'fI..
-------
-..-
.Ii- -
c=Jc:::::::JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
6ett1le ke~
Sampling Location: r- '; r . U.A
Sample Recovery Person:_t vJ D ~
Sampling Method Type: jV1 "3 I ~
Run Number~50 G. <::) 0 CJ
Job Number: - -.. i ..." L S- - P: (3
~ vJt 1
,
Plant:
Comments:
----
Sample Train Recovery Data
e e t Date: <3/ It! /cn
..,- r. ((
1 0 .;...---,/[ e I-
Field Team Leader:~) S
N~~
Impinger Train ID:
Filter No.: oCt 6 7£1 g' ,- 2.
Filter Description: JI1 0
Filter No.:
Front Half Data
Filter Media Type:
Ik-rl.C-LA Ie. j.,
,
Filter Media Type:
Ire t'-- -Ire! ;? I q. '3 "
.--
Filter Description:
-
Impinger Purge-
-
Start Time:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Back Half Data
Flow Rate:
Stop Time:
-Purge Gas:
Impinger 1
I{fLr
~:;~
()-o
Impinger 4
---
Impinger 2
II J/L C-
o (7. V
~/7< ~
~
Impinger 3
£,A1r-?/v
~7 5-:~
~0S. L
O-L
Impinger 5
Silica Gel
5,- ( Gel
(g): 70C:,. 2
(g): '70 ro. ::2
(9): () - CJ
::>
--
--
-
D(
-------
FIELD DATA SHEET
Plant: ~cr +\..\..\.,.. ........ ~ +e... f
Sampling Location ~\.....b~~ '3:.....\.....*
Run Number: B-I-lf,,)1-1 Dale: 68 - ((- Cf;?
Pretest Leak Rate: ~~'. - elm @ .~ In. Hg.
~ oOl~
Pretest Leak Check: Pitot: V Orsat: -
- I
Noule ID: . .,;)11 Thermocouple #:
Assumed Bws: ~ .s Filter #: U,..""u_'- c..C'~/h f'
Meter Box II: ~(!)-(. Y: I.Oc:$ ~H@: ,." '7~ v
Post-Test Leak Rate: .0',;) efm @ .J.5. in. Hg.
Post-Test Leak Check: Pitot: ......-orsat: ~
Sample Type: I.J~C; Operator: ~tn'-
Poor: ~ '1.7 Ps: - Ot.. ;)
C02: c:::::> 02: ~(b .~
Probe lengthfType: II' /.$ Tie/' Pitot II: ---
Stack Diameter: 11'/ I, Ks: ID, .:JO '7
to 3,b" 1.(::: -' I -,
T rllVer88 Samping Ooclc rime Gas Meter Velocity Orifice Pressure Difterential Stack T emperalure Impinger Dry Gas Mehtr Temp. Pump
PoInt TiM (24-hour Reading Head (lip) (lIH) in H2O Temp. of Temp. Inlet Outlet Vacuum
- of (Tm in°F) (T m out«»t:)
Number (mln) dock) (Vm) II S In H2O Desired Actual (Ts) Probe Filter fIR. Hg)
&'.t> 0 I~JO 1.135. 11_< W/////////////~,,//,///////,/ f/ 'l'/''i////// / /,ij. ~/////U////~
~"~,, ~~ 5 1035 J./ 3'- . fj J D I .~. ~ I . ,,~ ~ ~ , L, ., OS ;,.
.--' .4.~ ~ .~ I,.,'R ""'50- ~~o
1"1~ 10 ~'J. L./~~.'" 10 . -i$~" fI'S f"J .... . C> -c, ,4 I . ~~o .;:> \ II d-I ~ c.l~\. ~~D .0. ~O~ I 1"\ I 4<; "",p -'8 ~
.0:::" I ~c.o ~C!.o
19~ I ~
110e. ~ If'lJ. ." ( .'ilO , . ~ '5 I. ~-5 --2.'30 I dS~ iJ'5C ~ 7'5 Ie,
- ."=--.
,,~~ J I 14'" ~/43. oz:.o .0' .oi( .~~ II G" ! ~SC. d$O "7'5' . 71. r~ ~
i"~ I' ,t.. ~ If q I( . ~ 'laD . '0 I.~ t7 ,.'50 "".55' ~'50 ?Ii>D ~ c:=( ~7 7C." ~
@ 8 ~J~ 112"'~ ~~-5.'i Ie) b.l .~~ .0"" I Ib ~~o a:S"~ ~~ ;Co ,c.. do
s'1l'.,) , I}.(,,~ 447. 'it;O c;e> ,."!.Q \.IS 0 ,;)"!o!) ~"Sc:> .:)",0 '51 "7$ ,~ "J-
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o PACIFIC ENVIRONMENTAL SERVICES. INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:~~Q.. ~Ai\ 51-u.\ CJ..1l ~Jvk,t1J IJJ
Sampling Location:~hov~ :X::nL-..~
Sample Recovery Person: A. K
Sampling Method Type: ~ A42~
Run Number.~'" I- th~2t1, - t
Job Number. .s 5D f..g. 000
Date:~
Field Team Leader.
f)S
Impinger Train ID:
N-5
Comments: :;:+:..,L.t.. -:';:'~ -1-4.,./ f'~
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Front Half Data
/}"'~ - '1261" / "'7
Filter No.: Filter Media Type:
Filter Description: fl4:..1 BJe. c-/( G rl.i ,'11 5 ..-4ofe,
riltei No.: 8-"J:.. Q.- 21',(fi...t) Filter Media Type:
Filter Description: t'-ev.v./ 12>1~c....-ll 'G~'\.A5-/..,.,~-"
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Initial Volume: (mi.) J ,I t.I. '1
. Net Volume: (mI) '1 ~
Total Moisture Collected (JIll): - 7<
Description of Impinger catch: (\~
Nv Cu." f
Contents:
Final Volume: (mt) )
Initial Volume: (mt) ~
Net Volume: (tAij 1
Contents:
Impinger 4
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103,3
Silica Gel
S,'I.-... ~/-
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FIELD DATA SHEET
Lof"3-
Nozzle ID: .;), S Thermocouple II: -
Assumed Bws: ~ Filter #: UM\\S ",,-'-..c- ~
Meter Box #: M~-G. Y: I .005 6H@: J. 7 ?~
Post-Test Leak Rate: . oos cfm @ ..to in. Hg.
Posl.Tesl Leak Check: Pllol: Orsat:-
F.
I LiZ:s .;).0'1) - -
-
~If ~ ~~"\. T,aY"" Samplng Oock rlmlt Gas Mete' Velocity Orifice Pressure Differential Stack Temperalure Impinger Dry Gas Meier Temp. Pump
yC> ~ """'~ PoInt TI118 (24-hour Reading Head (tip) (tlH) in H2O Temp. of Temp. Inlet Outlet Vacuum
.1fu~ ~L \,.~. - of (Tm In0F) (T m out0F)
Number (mln) dock) (Vm) ft S in H2O Desired Actual (Ts) Probe Filter (1f'I.Hg)
Q A /(~ 0 D1;J£/ S"> '8. ~ 1 8 ~///////////////////h'>~~/ ~.~:////////////////////////7/77777/, Y A. l"-
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Cj J..,J OCY33~ 5"30.'110 . '6"\ J 3';> \ 3.':) .;)9~ . ~5.;J J 53 ~ ::; 'i?C) ~C> I. 53
"..,41.11 C.~l 9::>0 I
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- .
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-:39 v,) Jl'") (') ::l):; 535.70.:) , C;;> ~ .nt/ . CY-I J Il- dS'I ...5~' -$( ~I P-.J ~ S'.3
.Lfo~~ .,~.")11~ 53t::.'1,}O .9~ 1.~9 \.~~ :3111 JSI5 ..:) '5< .' '5..2 "&"-' '8".=J 1- S"d.
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IS'" I 'J .c:,. <57.050 0\ .o.;! .0) J/# dl/7 dJ{o" ~"t 77 77 :J 50
I t:...(,. I)"~ 5 5~ . , 1 () q( 1.~4 1.)9 ,~\ ~S'S ~SO 5~ "7'7 77 ~ 50
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Plant ~-\\...\.02..he~ $\-e.e.\
Sampling location ~ "-oo~e r V\. \C!--\.
Run Number: 6 .::r-~ 0 :5
Probe Lenglh/Type: 11'/ .s.:r:JjIOI 11:-
Slack Diameler: II~ As: 70 .8~
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Page d. of~
Plant Name: ~e t h \e. \r-..e. "'!:'- S\: e..e.1 Test Date: __~/-1d-J-1.."R .------.u - ---_u -"
Run Number: ~- 7. - ~,;}'t - c;;1 Operator: ~(,? r"\ t'\. ~ ~ D. \~\~~c~~l-
T....... _Pllnl/ Ond< TIllIe Gas Meier Velocily Orifice Pre.. Differealial StICk Probe Impinger Dry Ou Meier Temp. Pump
Poinl Time. (24-hour Readinl lIead C-p.) (cll) ilL 1120 Temp. 'F Temp. I Filler Temp. Inlel UUIICI ~ Vacuum
Number (milL) dock) (" .. It J ilL I b 0 Desired Actual n;) Temp.' F IF ('So.. )' F ('lanu') IF In. III XA"
- -
I :J.lfCt 1 a.~, ~.:g 1-- ..1 ~9
I ,r.. 131~ !\("I. 7{~ I - ("""I , r,.;) .. b.:) I I ~ 7, 77
(\q~ J 1,<6 1 I~")O 5 b:J. g~ 3 .'1/ I.JI.J I 1./ ~ 30'1 ...J~"5/..:J~O see 7'8 77 6 Sfo
- J "Ct 1 p,q J 'Sr"l.{j{oo . c...:! ..;:>S ~ 1 .:J(,,~' :5"3 /8 \?I _1 -53
n\ .D,:) 110
.,)('} 1 1 131.f~ S '5. ., I:J .g~ '.30 '.30 ~Db .:)3c:::. 1 -> 36 5.) ,'if '80 to Sl./
.:>0 q I I ~Sl S,e,. 9 ;) \ .0\ 0;;> 1'>:> I/(P .::l3,,/..JLJD 51 7"l1 Ie:; d S~
~\\ I /35",,> s;8.3c::c::, ,Q;$ I.~'l? I.~~ <'/-<;1 .;J 3.1 1 .,;).38 5(0 '9,,) "iL3 t.. 5\
61()., ..J/~ 1 JJ./r,(') 5<0<7./7<; .D l. . 0 ~ .0..) J(J5 .;1 3'- 1 ,)'''I:l .5Lf 1?.;;>. 8q ~ S-'
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1.0'"
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"J it). , :!l/O 1 1)./ .oS:J S IJ.556 .0\ .0';>' .. 0,). 1/4 ;) :\ q 1 ..:J '31- S~ 7f.c, 7'g r::J.. S"I
.1'((, 1 ~ 574 on .,..., \ ,D:J ,c~ 1t5 d~~ 1 ')~(... 52 ,~ II ->~. 5,),
;)q'f{ I ~ ~ ,5.507 .q~ r. 3~ I,~)1 "3'~ ~33/~3f 51 "$'.J gD (" 5J
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~57~ 1 IS~~ $,7.505 . ~~ / ,q:J lL.{d 36~ :JJ1o 1 ,,-:;rg S5 g~ ~l Go- So
;;)(J.{ ,,~ ';J(.7 1 If~OD 57~.40~ 0\ O:l. .o.;l 1I(~ ;) 3(.. 1 -, ~b 54 ~~ ~\ ..:> 51
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.1q, 1 IL ~4 "'}i~_~'1 .Ctt I 4) 1.4 J 30"\ d3"8'rl~G:. .c;'':c; 7'i 70, I:. S~
300 1 \ <..33 s qq t.f'~ 0 .. 0\ oJ .0:> I I ~ :J 3(-' ':)-::r,q 'S~ '"7Cj 7Dt .J- $:J
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Page
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Plant Name:
Run Number:
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Test Date:
Opera tor:
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l::k...,~~...... ~. \~\.~~c..."'~ \... ------..~
~-I - fI~'7-~
Travcrse S...p1inc / Ooct 11... Gas Meier Velocity Ori6ce Pres. DiJrcrealiai Slick Probe Impincer Dry 0:11 Meier Temp. Pump
roinl Time. (24-hour Rudlnl lIeld (-p.) (cll) IlL IIJO Temp. . F Temp.' Filler Temp. Inld UUUCl Vacuum
Number (min.) dock) "')ftJ IlL IIzO Desired Actual (1;) Temp.. F .F (T.... ). F ("Ii_..) .F In. III
3Q- l.I ~H I J r.. 'Iii. !i;'F!7.~ .~q , . 'II 1 . 'II '?~ I ..l~'5' ~",,\q S, 78 7"7 t,.,
~~- - J:;' 33(... I ,i(")t; 5~q...) lie., . b \ .D..) - 0,) "~ .) 3(... I .J 3") scJ I~ ..,c, .-)
33.'>l. I J.., II Sqo. ~oc q,;) I. 3.~ \.3~ 3~:S .)~o '..J~~ S'd 79. ,e.., r...
"tuL " ""lIe, 5'10 ,&~ . ('"), . 0 'd- .("\...1 1 , 'S d 3'1' d~ 51 ,., 7)? ~
~4~ " 1~, ~'il. qJf7 . 'i~ 1.f.(0 \ ,l-(D ~.;lCo ;)~.c:.. '..::>-.r../"- "5..;t (~ { q Co
3 (,,(J-L \SC.. I I7J'1 5<1 ~ ./..fro c\. .0..) .o~ I \ A.. ..)~, J -1~" 'S\ 1'2 ce, ...1
~'S'. 51 I ~-z3\ J;.C\3.7e>5 c,"'\ .."-::::I. 1-':2.. ~ :::r.~~ d ,,..j ~ c:.,. C'~ ,i? -,~ ~
S'1'f.~ ~(,.L , I,~C; - - (\ I""'>..J I 14 cJ 3d ..) 'r- .c;-, ,'i? 75<' d-
~ ~.-.....- .0,1-
-::?r_"V , , 71( I 5'1'5. r~O .GJ ,.3) I. ~.:1 ~~.c:;, ') 7t 37 5J .9. ,S' #,
1.,~(p , 1'40, 5 't7. DOO r"\\ oJ.. . C"'W J ,.c::; d3")'';>~~ 51 ire; I~ c;;>
'3,'8 , lis::" <;..,~ ')l{ 1 ."'I~ ,,~o ,. ~b 3::11 ~3,1 ..;1~1 oC\'r...... 1<=1 ,8> G-,
3~ - -, 3~ I 1 ,'5'" '" Q,o,.All . ~I .O~ .o~ /15 ..,;) '3c} .d:' l <0 ''; I' .':I.
3~'% I 1-»01 lDoO. ~lj I 11~ 1 . LIe> 1.40 3,;)7 ') 2.r-. I .:> '30 50 7"-, 7J? l..o
~"'\, '..:t 10 (,,1"1\. 1,4,,) .0\ .0.;). . DJ I I I{ d 3rJ .:) ~D 5l (~ I~ ...,:)
39"\ I , ~ ,.:.\ (m');). /50:.. I. Ie> '.5~ \. "5 ':i? '3;>. 'f ~:3~' :)""io.;) 50 l?o 'gO t.o
qO~- B if I'ilJ..oOl. I 1831 ~ r...rll.o ~q I . (") \ .0;1 .O:::J 1/5 ~30' ';>3~ S::1 ~D ~o ~
l{.10 ~ I Iq33~'" ("li" 0 10 .lj~ lAc I.~b "'2. A.I" j 7.,' I ~,~ 5\ 7'1 ,'\ .4:.
tI~ ' ,~q3 ("H_. ~lnS .0\ .0J .oJ. 1'7 ,,:)"30' ;;"3~ C;,., ,t:! ," ;)
4~"" "4'3~ I ,gy..:; (..D"'1.o ogC; b . qt; 1.3'1. \. "3..g 3\~ ;1'3~/.:;\~~ ~:;:I. flo ,"'1 U
Lf3'1~ I 1~5.J3 l.n'8.575 .0\ . b") O~ IffD :J 34 1 P?..;I. 1 S\ 90 110 ~
'1 ~ , !..-J , 1 ~&:fi~ (- f)~.. ~oD . tfCo '40 1.40 ~1'1 d.~':3' ~ 30 5~ go :8D to
LJ '" n , I .ql)~ "f I). 6"11 f)\ . b;) .0;) I I d.. ;J. "3 D 1 ~ ~'5 "I '5?D ?~ :;)
l/~;) 'I.~ (" , .). ol10 ~~ 1,;:)( \.:;). ( 3d). J. '3 \ ' .:J 3(~ 5~ q\ Ie; to
111:,(..--,0 ~&;q Y,;I. I '.1,J Y.7 ~I-;. 000 . /':) \ .o.,}. .0.\ /11 ;)'35' ~ ~(- 55 1\ t"i .;)
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53
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-------
Page
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Plant Name:
Run Number:
Test Date:
Operator:
~ I Ie.~' fol~. 8 \0 .0\ .o~ o~ III d~~..1 --' -:>,\ 4 'i 'irO ~I ~
Lf~~ I IC",,- {,., 7.0SD qC, I.lIO /."iD Sl'1 ,,1 3 7' ~ '3 0, If''7 ~b ~I ~
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"'. ',~~1~~~i1~r:~~~I!~--'~',@1~'"(;;~;i~'~~,~i;~\;}~~t
II.
c::::::J r:::::::J c:::J
r:J PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: &lUi~ 5-/uP - ~/# c=o4....
Sampling Location: t3r"n, ~ ~r
Sample Recovery Person: 'J.t... J R P
,
Sampling Method Type: ~ ~b 12 r
Run Number: E - ;:;- - 0/2'7- 2-
Job Number: S.:rQ"'~ 00 0
c~) .fr-r J.w, / ::L...,/..
Date:~
Field Team Leader: j) S; 4rh..fJ
.
Comments: '3 P: \ }-~( tA.~ e J
Impinger Train ID:
/l.T~- ~
d v co
fe,
heb-vl
,
1f"\~d~"J
Front Half Data
Filter No.: ~.& /If '- r Filter Media Type:~ () Ui I¥I 6 er e rI
Filter Description: I I {r...( f ; C I.' I €.I.. ~
Filter No.: r I!' l Filter Media Type: -r;..( lo./J ,r'Z-. ~ 1-
Filter Description: t 1 f? CJ.- If ~ ?:. k c L fJ CA ( I - c:: 1,...( t::o. 1-1"
I
Contents:
Final Volume: (ml)
7-lnitial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Back Half Data
XAD-Trap
xJ4fO.:) h '"
~ 1-' ("--
') I.J
:.~. '-:\
......."- .
:2<1.. t:)
Impinger 1
~
t!f.2
'-f f;, f;
r~?f
Impinger 4
~&
~..2 7. ~
G 1-~. 1
.;;> . r
~~
(~'f7
Impinger 2
,A,{IIC~9,~1. C1
-!4t 19. 6
Silica Gel
(g):
-------
FIELD DATA SHEET
Plant: ~ T\.... "\,...a."....... ~ ~\
Sampling Location ~ \..o.::.~ :r.......~~
.;>
Run Number: ~ -:f -Lt.::»;- '!>Date: 11-. ~ -<;, ~
Pre",' Leak Rate: .oS ., efm @ . ..o.l in. Hg.
Pre",' Leak Check: Pilot: ,/ Orsal: -
Sample Type: Jf d '" Operator: ~h~
Poor: ~Dy.~ Ps: - d.~
C02: . 'S 02: ';>D .-S-
Probe lengthfType: ,~I/.6 T't: Pitot II: ~fLl t
Slack Diameter: I \4. II : In .07 '....)..
Nozzle ID: .;} '5 Thermocouple II: !::.Tf'-I'
Assumed Bws: b ,~~.J c.c.;';. .OID V//:'::////~~:////~/ij'~ r:~:/~:;//~t//~///~::/'//~ YA!:'::'I
f. ,3'38 ~CD5. ~oo "1'8
~ 1"3 'fO Uk ,. flO I.C>~ f.~ 1.~;;) 3,...,. d 3~ ";>"3,;) 4C, 77 7'5 Cc .l{tf
I ~ q8-'1 ; ~3-S 'Ie,
1(,)0, (.,G., I. Cr"7; .D:l .0'1 ,01.( /1 c.. I .;J:3' 7'7 7/ ., :So
Iql:) 1"':\ 50':1 (,c..C;. ~ I 0 . q 'i 1.t.lJ :3.;1.:> i ' S "7i1 Sc..>
I. 'f;> I oJ. 4 C> ';>37 71 ~
Jq 6 \ ~~ I
~'t':l c.. ""b. If f:)' "...,.2 .0'4 . c:> '1 II, I "JLIO .;> 3 '8 ~c 7(j """)'7 ~ sc.
,
11ft.) q ~I~ I\O'3j.,) (,,~ I.Cc;c, I. de, I. ~ (... I . 8'£' 3/8 ! Q)3'il .;\3-:> SO ?'il "78 ~ ~I
47 I I{ I "'I c..~..)3D ,0 (). . .01( .0'( I ,<; rf:3<- ";> ~.., ~, '0'11 ?~ .:J S\
Ii'" IU;\ t 111,1{. ,-roS . "'I \? I.I./?, /..,,-3 ~Dg d):.0 ~i./c> 51 'i? 78 it> S:).
~..I)"1il (17 I "'oc\ r...qD.750 .o~ .0'( .0" Ifl ..:J~I ...J"3":> S;) 7Y 77 ,;) SOd-
'if.\ 1 ~'I /511 c,,1,,).3"'V .9'5 1.37 I.~? 3/'7 ..,) 3.) ..)~) 5~ 7'i1 '77 to S~
/01 It:. 1<1
/0", .5J.\ G;.i~. I ~ I .c,g J. q). I.~ J ~I<; .;>3C-" ..,.)3/ '5'1 I~ 77 I~ SI
I ,(~ I<~V (...,\1< . .3 II .0).. . oJ.( .01( JILl ..;)3~ ~~~ S5 fer 77 ;) ~I
'Ig 530 rn~A. "'t g "r . i./ , Ie: d~~ ~ ~/" ~, ?v ,? :J OS \
" ,..,0;;> .<'<.In G,q'if. q15 . C\Q I ~~ I 11-1 3,:)\ q~? ~ "1. '51 til ''7 t. Sp
/ ~.) ) (, ."3fA 15"'~ CD g., .9 1'5 .0:\ ~.DtI .0'1 , IIJ ".... C, ::J"'(~ :S~ 7~ 7-' d 50
,3~ ,5~b tOe; I. 1"5 D ,qtl 1.3~ 1.3(, 3..:1$ ,;J '" / ~t./~ So 8\ 7'7 G, S-a.
.UL. I.c:~'i ,-ql.'iJC> I"'>;). '0'1 .0 t( 11< dl/~ .,;),3""? . LIS ~"3,'B' f-/'Z ~~ "79 ~ So
,~j... /l...lfo.~J (...'1"\ ~ 8, 9~ I.~c.., 1.3<.. ':I. ;J." ~~.,:) ,;)37 ~Cf 80 ..." t:. $'1
1 c..«\ ':a 11.\11:) (P'ti:.. '3co .o~ .o'i .04 I I '30 d~o, ~3(" 5'3 g\ "77 d 50..>
IL."7Y. 11.11\ \.-.1 (,..~ 7. '\ t;< ,.oS I ,0:;05 ,.~s 305 ~so j~1 S~ i\ '1 I~ St
,"'of) < ,~..... I (- 'J.LI ,,~~.,~\ "'':11 o~ .OLf II~ L9;;J5 d~C. S~ 'R\ l' .J S;;;)
I~~ \ 1".7,.(... ;f\ \ 0'" t; 1.00 I. £Ii 1.14' .3(:;(:;;> ,:)3~ ",,)'3, 5"l B\ '7~ ,- '"
~-
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80
-------
Page ---L- of
3
Plant Name:
Run Number:
Test Date:
Opera tor:
Be." \. \~ ~'"-
":>_\-4.e.\
08- ,:,- "tV
------.-- -_...._..._-~ -.--..--.
~\ v~(.,"'~'-
~-:L- I"'\ti.l'\- '3
u.
t>e.~~~S
Traverse SampUnc / Ood Time Gas Meier Vclocity OriflCc Prcs. Difrcrcalial Slack P,obe Impinger DfJ Gas Mclc' Temp. Pump
Poinl Time, (24-hour Readinl lIead ~p.) (lIIl) In. IIJO Temp. - F Temp.' Filler Temp. I nlel UUIICI Vacuum
Number Imln.) dodt) (" ) It J 1n.lbO Desircd Adual ft) Tcmp.-'" 8... (18.. )8 F ("Ii_.,) 8'" In. III
t q, I 1(~t.I<" ',..,:"1. ('")~o .O~ .n4 .01.( 1 I;J .,:) ":1\.", , ..0 ~c, 53 "6, HC 01
, q.c:. " £..LI 7 iQ'."3 ~\ 'i'\ lA
r~,.,'i'l 4 .)0'\ >-~ , .""1r::>l ~-"' 'DC: 13"'1 .~:> .0 t{ 01{ ,« '3 ~:,c..' ~3' <:") :5<'1 ~I d-
.;I ~ll.o~. , .iO:!>s;;.. lOb .q~5 qq I. qLf I, I{ q ~\5 ,.J 3G> ' .,.) 3'" 5\ ~I SOl ~.
..)I~v~ 'I"'O~ 107 (') I 7 .0,;) ot{ . 0-4 II ~ j'3?'...:3-""-' "',). Il 1 ~o ~
..),:y..,v) I 1'1 IJ. ~ ,caS .J o~ . 'i~ I. 3 ....., S \ ~n 8e:; <0
1(:::J."t>'\-~ ..)L/ 3 y~ I I'~S ~ .., l I. .;) \s ,f">:\ .0L/ .(")4 I I 'is oJ 3;)J ;;J ~ '8' '$0 ~I 8'0 d-
..Jlf5 y\ " i"; '7 ~ tlC).,&80 1.0"'.:, I.W; I -1.4 e, ":it..:! I ...)~:I' ~~(... 'S~ trl ~c Co
")S~ I I 7'1" ., \ ~.(,,{'£\ .0.:1 .01./ .oJl 1/7 ;)~~'...:> 35 ~I 'jJ l ~o .J.
,,~c , "Lf, , I.c;,.()~n I-DO '.45 1.45 3';):l ':>'31 ',)3:::J S'l ?rl go &::.
.:> (" "& I 1"1>00 '"\ \(". ro;) D ,0.;1 .oll .oq I 1 <.t. ,:)v_'.:J~':> 5~ 1r I 8'0 d-
.;)'/0 , 'QD~ ., 11.~Ob 0, /" 1.3'i \.'!I' 3~, ~~~'.:::t~( t;.:.\ .., ~I f.&,
(..)I(.~ .:J7"S1. I 1910 ., I~.!..OO .o~ .014 .~~ ,~() ,)3g' .;>3"1. ~~ ~I 8'1 ~
:::t.<1,..., I I "i'l ~ '7 ;:)0.010 "Y-I '.;J'),.7 <;;\ '01 fIe:. ~
'3\}.')-') , "I (A I l.qq, (- "S~ 'it ~l a
~I~ I ,CIC,n '7 :) 7. JG,.., '\1 1 '1/ I. 'II ':l :J,-, -' ').,t./ I oJ <: ~ J)/ R( )', (p
1~~ I l~o4 7Yt-~~O .0..3.. .04 01/ 1'"7 .a ~I:\ T.,:) 3 I "III '
S~ ~I ~
~'?I4 , .q\:)(P l.lG. 'ii l'i '.00 I 14~ PIS ".:>~ .:231l' .J3" 51 ~\ io fo
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-------
Page
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of
3
Plant Name:
Run Number:
(\ ~ \. \-.. \ e.\... '" ""'" -
~~e.e\
Test Date:
Operator:
-_--!/i!!..L..::.-1~~-- -----..---- ----'-'
&-1: -'/.;).'1. - ~
b4o/\."'~~ \).
\'0 \. ~"::> <.. '\.-. ~ \...
Travc:rse S"''''I''I/ Clod< Time Gas Meter Velocity Orifice Pres. Differential 51 aclt Probe Impinger Dry Oas Meter Temp. Pump
roint Time. (24-hour Readina lie ad ~p.) (cll) In. 1110 Temp. - F Temp.' Filter Temp. Inlel VUIiCi . Vacuum
Number (min.) dock) ,"- ) ftJ In. I It 0 Desired Actual ft) Temp.- F .F n:.... ). F ("1'._..) .F In. III
":I.u:l I IC, 1£.1 -, '?o ,...loo .o~ .04 .oU 1 \ -S ...)~ (~ ' ~...." 4'; 5?1 "Jrl ..:l
<.~4 I ,-'1<0 l~\..c:;~D '.00 I. £.1$ /.4~ ~'3l~ :::r'\t(lrl~ $/ )?/ ""T'> le>
'3 (p (') '.",~:) -, .~Us -;t) 0.;). .oLI .0'1 /16> ';> 3'5' , ..:> 3 /0 s\. ,z\ gO ~
"' 1..:2 I Il:t~~ 734. l'l Cd .'1~ , .1111 , .'iLl 315 ,)':J.,q'.; 3'8 5\ 81 Trl Co
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S fj iiiI h..-
r=Jr::::::JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
1ILi/~(
Comments:
Sample Train Recovery Data
Plant: CJ-lt'/ \3e'~h\e kf'tV' 5.+ee\ -l2f A C~(?S~r"dt.r1,~)Date:
Sampling Location: '1"" \e -\- \3 fAl) h6C\ 5 e
Sample Recovery Person: i. \J ~) . I rz.L.- . Field ~eam Leader: D S
Sampling Method Type:-f\.~ C 0-' 10 ~, etl.. . J \:i '\ AI - :;
Run Number:J -.I- ~... :, Impinger Train ID:
Job Number: 5 c:; 0 ~. D D 0
M- :r -Mtf1..1-- 3
Filter No.: U "'~ l.tt/.."
Filter Description: //I Eo.. iJ V'
(
Fatei No.:
Front Half Data I
--rc.ffo"l ~ f
Filter Media Type: .~~ ~
&/0, C' L
Filtei Media Type: --
Filter Description:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Back Half Data
I
{
\
XAD- Trap- \
~O-?-
'~ 512
~(f)\?
( 1../
Impinger 3
~)
i:lO. r -
l r: \\ ' ':>
- !f'1~ 0
(' !f?f1.. r-
-
,Impinger 1
M
:-'q i I
~
Impinger 4
(J Mr*~b
~
~
7l~':>
..-/
Impinger 2
-l1J\CD3.1 JJ~f!:J
7(1.0
:} 1;3..~
Silica Gel
(g): c(l/ I. 7
(g): q \ d. a
(g):~
sg
-------
FIELD DATA SHEET
Nozzle 10: . ~ \~ Thermocouple II:
Assumed Bws: ~ Filter II: I JJ'\"'';.. I
C02: . .e,
Probe lengthlType:
Stack Diameter:
y.,}c, Operator: 'b~~
Ps: 0
02: ")b .~
:s '/05 -irPitot 11:-
Trev.... Sampling Cock Time Gas Meter Velocity Orifice Pressure Oilt8rentiaJ Stack Temperature Impinger Dry Gas Me.r Temp. Pump
PoInt Time (24-hour Reading Head (6pl (6H) in H2O Temp. of Temp. Inle' Outlet Vacuum
Number (mln) dock) (Vm) ft 3 in H2O Desired Actual (Ts) Probe Fdtsr of (Tm in°F) (Tmout°F) (n. Hg)
, (Qoo~ loP ,-.., 734.6'101 V///////////////////fi0//// f / ////////////////////// // / / / / fi
)L..'~ ,'" 7"34. "'CDS AJ/,a. 101 ~ ,..)J,.. ..v/~~ .}I(C> Jil b ~D iJ/A ~/r1
, ... 3D I~S .ooD ,. . I' .t. .
30 I " t JI 0 ,.J f'!- IJlfi
I b"~ '15 -7'3'5./00 ~I JI I I . \ I RD J~ ::t~
.... \!J ' v (
I
I
I
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I
'.
-
1'5"
(b.c~t.
~-
AVm-
AH-
T...
-------
~--
CJCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:
CI1?5ftr Ju VI
Field Team Leader:
Impinger Train ID:
Date: 8/N/pg
I
'~f2 OCJ
Comments:
fJ»~ ::LtJ. H4 ~/.-I;
3~:t~CfVl-/ P8
Filter No.: ~
Filter DescriPtio~: ~
Filter No.:
Front Half Data
Filter Media Type:
fp{/o y1
JI11al
Filter Media Type:
Filter Description:
Back Half Data
~DJ Trap
Yh I»
Final Volume: (ml) 32-16. "3
Initial Volume: (ml) "zra. 3
Net Volume: (ml) D. t)
Contents: J;:if!l/;kl~
Final Volume: (ml) Sf 2. f8
Initial Volume: (ml) 57:2 - ? .
Net Volume: (ml) 0, (p
Total Moisture Collected (ml): ----' I 0
Description of Impinger catch:
£1-1 d-/ Uu.t1c.aYl
Imprng.!'r 1
~t /t~lI~~
tf1~. 7
' 1~. 0-
- t'J . I
Impinger 4
EmjJf,/
.s i,.sf.l>
~:J<:[, 7)
0,0
Contents:
Impinger 2
;U/({t5/4~
~3?:.s
f) ~7~ r-
o. I
Silica Gel
5 " I G0' I
(g): ~ , y.o
(g): 8"~s. L
(g):~
I
sg
-------
a~ lo~
,..:,1 ~ ~
f/~ 't~
r.L"k
0/\ )/-
~
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS (-f.l-tf'
f
..~
:::: ==r- .===
---
Plant: gelh~#t./>-t s+cd
Oat.: '8 -llJ - r ,f
"
1;~O
Sampling L.CcatJOn: i'../I. ~v+le) ~.f
Insid. at Far Wall to Outside at Nippie: /-Z4- {su. foU,,,,:} (iJC') ':It,t-tV-
Inside at Near Wall to Outsida at Nipple (Nipple Lengtn): g/n., J
Stack I.C.: lOf{ II
Diatance Downstream from Flow Disturcance IDistance 61:
(,(,0 inche., Stack 1.0. = ~ dd
Distance ucstr.am from Flow Olsturbance IDlstance A':
5fi) inches , StacK 1.0. = ~ ad
Calculat.a By: VA/ITA
CC'~t - foCo~."
4
~ /0'6/0 ::rJ'-
- f) .
.
Sd1ot~
Sampling LccatICn
'(,e"
fJ
Traverse FraCtIon Lengtn Prccuct of Nipple Traverse Point
Point of (incnes) Columns 2 & 3 Lengtn location
Numcer Length (To nearest 1/8j (incheS) (Sum of Col. 4 & 5)
I tl. D3"" 108' '/ rJ< .~ lt2- I 1 /p,.) I\.~ ) 21.D
1 () .Iv) ~ ~ 1/.3lF ~ J \1.) I~.]h) 2'317i
) () 104 ;21. OJ f )/1.5 l1.i} 7 fX-Y'"
4 I 0 1.J:7, I 34. '1/8 I ~ JI}>' 4 2 1~ 7 5 Z s-5
I
-------
DuCt Diameters ucstream From Row Disturcance* (Distance A)
0.5 '.0 1.5 2.0 2.5
~ 501 I I
a. 40 I-
a)
en
-
CD
>
cu
.= 30
'0
AeM
.
AI
f
24
~ 20 [ I 20
S 16 I 16
~ -V-;I~Clty(NO-;;-pan;CUla~) -~ - 2..2- I
- 10
~ I .
~ 0 ' I I" I I I
2 3 4 5 6 7 e 9 10
DuCt Diameters Downstream From Row Disturbance* (Distance 8)
. tr",m ~lntot My T~ 0' Ol8turD8nC8 .a.na. C=8n8ICN'I. Conncaon. 8el
8
.~I
12
I
-,
I
I
:JIiIU'D8IlO.6
LOCATION OF TRAVERSE POINTS IN CIRCUlAR DUCTS
(Fracaon of StaCk Diameter trom Inside WaJl to Traverse Point)
Traverse \
Point Numcer of Traverse Points on a Diameter
Number
on a
Diameter 4 6 a 10 12
1 0.067 0.044 0.032 0.026 0.021
2 0.250 0.146 0.105 0.082 0.067
3 0.750 0.296 0.194 0.146 0.118
4 0.933 0.704 0.323 0.226 0.177
5 0.854 0.677 0.342 0.250
6 0.956 0.806 0.65B 0.356
7 0.895 0.774 0.644
8 . 0.968 0.854 0.750
9 0.81 B 0.823
10 0.974 0.S82
11 0.833
-------
811
II
t 1.,
---~--'
--- --~----------______n_-~_-- ------------_! ---__l!~__1'_____--
-------
---~
---.------------ ---. .
----, ------.-
----.------ -- -----------------~-
-- -_.'~~
--.--
--~~~-~._~~-~~ ~
----------- - ------~~~---
~ "":l\ 70f Ji _4 .. F~
- ---------_~~_~~rt ~- ------ ----------
--------.-
._- --- ------------. -----"----.--' --------
---.-.---.--,-- .-.,--~-_._._---------- -
.-- -"-------------.- ---"--------~---~ _._----~ -".-
---.-- ------
. '-'.- U_---"-
------"--------.-
'------ ----- ----
.- - -- - ---.--. -----
-----------
-- -- - .
------- '.J-- - -- --- -.
I
--.-., I
~-f/)!!:j- - -- ---- - - ------ --
----.-----.--------
------.--
---- --_._--------- .----..
I ...~T
.. -. - -~_... ..-....-.--. -
---- -,------------ --------------1/ ------ ----
--- ___n__- - 115 r
._-_._~----- '----.---.--"-- -
--- -- --
._-- . --- --_.~- - ._~
----~-----_._~--- -~- _h- ------.-
-- -- - -- - --------
------ ------- -- --..
- - --" --- ---"
- _._.~-- ---
- -..- - -_. ------~----.. --
.- - --~ ------------~-- --- ---
I J.H_"__- !~H -~-=---~-~---~----~~---~~.:b- -::".,~_II__y.;. ,,~!"~ -~~____d-
------ - Y''''- 24" ll'--C~
-------_u_----~,,~- ~t_o~._----- - -. u_--- ----- L____- w-- ---p_u- .-.--- .
---- - -- ----~- ~~ !-'i!.~--------_.
-.-"-----.-----.-------- -~---- .----- ---------_.-
~-----------_._- --- -_.--
--------- -~---------------,-~ -- _.__.----,._-~._- -~-~---~---_._----------'------
--..-. --
-----------------~---
------~-------------
------------.---
---- -
- -~._--------~~
-- ._"~_._---_.----~_. -. ---._---~-----'-_._--- .
. ~- -. -.-------.---.--.-----..-----------
- .-- ..-. ..---------'-- --- --~--- -----~_.._---..
-- -' -----.---- -. ---...
-------
4
-:;/5
I. ~7 z...
, ',£1
---
:J a c c::iI
~c=Jc=J
:::;
'f~ ~ ~
J f -7 CJ I
J . 0 c> -z.....
1(- 2.3)
GAS VELOCITY AND VOLUMETRIC FLOW RATE
.
Plant:~hJa...h"lM ~~e, ( - IIAd.~6..,,~
Sampling Location:_Rl1~~/I(~5<' Oufl2:.+
Run #:~\~M ;tA~,.t.
Barometric Pressure, in. Hg:
Moisture, %: Molecular wt., Dry:
Stack Dimension, in. Diameter or Side 1 :
Wet Bulb, of: Dry BUlb,o F:
Date: g--~- 95
Clock Time:
Operators: "714--/NAI/ SA
Static Pressure, in. ~O:
Pitot Tube, Cp:
Side 2:
Trave.... Velocity Me! .. (0.44 x ,,~) + (0.32 x %~) + (0.28 x %~)
Point Head
F:.~, Number In. H20 \. Me! - (0.44 x ) + (0.32 x ) + (0.28 x )
~'rt L .'.>......
I Md - * 1,11,
%H 0 %H 0
Ma - Me!x(1- -L) + 18(-L) ~ 80
100 100
M. - ( )X(1.-)+18(-K (51
100 100
:;
2. M. - ~ t'l
It 'I..- OR (oF + 460ft
i'i- OF - t;
P. - Pb + ~ .. ( ) + t1? () ?
13.15 13.8
Pe- In. Hg ,JO~ ,-;:J ~
3 IKP= ~ 1."
v. - 85.49 x Cp x 1& x ~ Ts fA)
PSXMB
VB so 85.49 x ( )),( )x~
~ '
VB - ftI.
2
3 A.- ft2
Ii Os - v. x A. x 60 B/m
Os- x xeo
Os- actm
Pe % HzO
Osetd" Os x 17.847 x - x (1. -)
T. 100
IAP- T. - Ctetd- X 17.047 X X(1'-)
100
-------
Pacific Environmental Services. Inc.
&flJ Cok. ~~ Dry Molecular Weight Determination
Cnent/Project: $5"0(,.,"" Orsat No. I
DateITime: & (iI., / fI Operator: JoJl..J,A.
.
Sample Type: 0 rSiA ~ Comments:
Ambient Temp. of 70.'" Site Locallon: ~~.k- ~~
Run No.(s) Run 1 Run 2 Run 3 Average Molecular Weight
Net Multiplier of
!3'C' Actual Net Actual Net Volume Stack Gas. Md
Actual Net % (lblMolel
?-It CO2 f.~ 0.5' ~;- ~.> ().5 0.«
O2' a.o.~ ~,o 2().{ 'UJ, f) .,20,0 0.32
CO~ 0.28
N2' 1P1J. rJ 79. 1"0, 1) ?f.G' 7't!r 0.28
Md=
Run No.(s) Run 1 Run 2 Run 3 Average Molecular Weight
Net Multiplier of
8'0'" Volume Slack Gas. Md
Actual Net "10 (lblMolel
:L:B 0.5 0.44
O2. 20,0 0.32
CO~ 0.28
N2' 100.0 1Q.45 0.28
Md=
Run No.(s) Run 1 Run 2 Run3 Average Molecular Weight
Net Multiplier of
6..()" Volume Stack Gas. Md
Net Actual Actual Net % (lblMolel
2G 0,5 0.44
O2. 10 .0 0.32
CO~ 0.28
N2' 7'1.5 0.28
Md-
. O2 Net Volume IS O2 acIU8I re8dlng minus CO2 actual reading.
II CO Net Volume IS CO actual re8d1ll9 minul O2 actual reading.
c N2 Net Volume 11100 mltlUl CO actual reading.
gg~
-------
Pacific Environmental Services. Inc.
£/1} ~b.,. -- /le.;t '-Wry Molecular Weight Determination
. ~ ---L-
Client/Project: S~".t100 Orsat No.
Datemme: '(IC jqP, 0 '11.1 7"- 0 0.28
Md=
Run No.(S) Run 1 Run 2 Run 3 Average Molecular Weight
Net Multiplier 01
13...0 ' Votume Stack Gal. Md
Actual Net % (lblMotel
18 P.t( 0.44
O2° ?o.S' 0.32
CO. 0.28
N2' '19.2" '1'/./ 0.28
Md=
Run No.IS) Run 1 Run2 Run 3 Average Motecular \/\/8Ignt
Net Multiplier 01
~O'" Actual Net Actual Net Votume Stack Gal. Md
Actual Net % (lblMoIel
I" CO2 0,'1 O,S 0,5 ~.If~ 0.44
O2" ;J, I. 0 ,0 ~5 .2.0. 0.32
COo 0.28
N2' PP. f1 1'f. ~ /'0. () 79. () 'If. f) 0.28
Md-
. O2 Net Votume II O2 actual rudIng minus CO2 acwaI reading.
II CO Net Votume IS CO actual re8C1lng minus O2 actual reading.
c N2 Net Votume 11100 minus CO actual reldlng.
g~
-------
Pacific Environmental Services, Inc.
Sample Type:
Ambient Temp. of
!h u., -~'- S,4:.e/
~/I ~/9f1
1)/',14.1
7o"'f
Dry Molecular Weight Determination
Operator.
I
"'72. I o,~ O.~ 0.44
O2' "Z-O.o 20.> 2-0. C1 0.32
CO" 0.28
N2' /6'0. 0 ~(i1{). 0 0.28
Md-
. O2 Net Volume IS O2 actual reading minus CO2 actual reading.
II CO Net Voluma IS CO actual re8dtng minus Oz actual reading.
. Nz Net Volume IS 100 mInUS CO actual reading.
!lg~
-------
METHOD 18 FIELD DATA SHEET
Plant:-5M Co/tv J?AJ.(J.UI ~'- Tested Analyte:--P f) H
Date: <1- if -q~ Orifice Tank #:
Location: "B4Shm,S1 0 v-r~+ Pump/Rotometer #:' Vos1" ~.-1-
Run #: B- 0 oJ h155Di~ - , pt: Pretest (mm Hg):
Stack 1.0.: tOg" P.ost-Test (mm Hg): ---
Pbar: .::z 'f. I C> Tt: Pretest ~F): ---
Sample Tube #: PJ .c-/J1~(,- / '7l.1j,~ ~ ~) C. Post- T est ~F): ---.
Operators:-=z:......t Time: Start:-=-Finish:~ Total: '330
Leak Check: Pre: /' Post: V' W/8:--==.D/8:-=-02:-3:LC92: ()
---
a a CJ :::::J
c::J c:::::; c:::=
CJ
Time
-
.-
-
---
-
: n L~-+
; r,-vr- 1 ~ "'"
. .""'\1 J
; o,cJ p...I
-
\r... j \I-..JL.
~~~:.
N~
iz.o,() ~~~ .15
1z...2US ~fl"1," \..5
~..; qtl~ ()
4Sfu1Z .0
(J) ~ Q~O.O
~ ~ 'ol'
qo q. ,&r>
JuS q I ~q
po q, SO
J:20e II. 1:
tfI; c '-'<1
j~..,& ,.s,S I < l2
difi nO 0\ I ( ..,
ti( ~:t 1-:1.
;1.06 12 ,,~
2-~ '" 2 ~
1-- it: ~ ',2 ~,. II
l.iI;S q t ,. ~
tkb &t ?_t.-I
<215 Q '2. 't ..
113Z$l~ i:.I."2../
.os (4 "\ ~
.~ . k-' ').,)) ~"",' &.\. s
,~ bli.J tP '"-)" u. '\.., 1::>1 16
,I( ...qJ
1oJ1'1
1 ~I' }{~
t.. f"J
;
~
~.
(.
,
,
o.
r
r
Gauge
Vacuum
(Ho)
'-
-
.--
-
"4,-,
~CItY
aa
in. '
,
5
::;.
'3
1
1
)
7
-,;-
:J
~
~
"l.
~
~
)
"'-
~
"1
.3
.J>
'1
'"
-
'\..I
Flow
Setting
-
--
-
~
-
Ant
~~
T~.
I
I
J
f
I
I
t
I
~
. /
,
t
I
/
J
I
I
I
I
,
I
I
Md .. 10.44 x %C02) + (0.32 x %02) ... (0.2B x %~)
Md .. 10.44 x
-
Md =
) + (0.32 x
) + (0.28 x
% H20 % H20
Ms = Mdxl1. -~. 18( -}
100 100
tt.
~3 &=
r9
U7 Vs - 85.49 x Cp x .[[;P x
~
F(. VS - 85.49 x (
~G.
r5 Vs .
!6
f;
~~ Aa-
gJ;
(\-L as. Vs II As x 60 S/m
It,
~ 08-
~(,
8t. 08 -
fS Ps" HzO
fj~ Oaatd" aU 17.B47x - x(1. --:-)
51. Ta 100
~'2.0
1.1. Oaatd-
't"t.
-
Ms - f
-
Ms -
-
Ts -
7 n. O'F- "'b S.P.
Ps-.. ._=~
13.8
Ps ,.
Oaad-
)X(1. _)+18(-1
100 100
OF -
OR (OF. 460)
) +
13.8
in. Hg
Ts fA)
Psx Ms
) x (
}x~
ftIs
112
x
xeo
adm
x 17.847 x
x(1.-.
100
-------
METHOD 18 FIELD DATA SHEET
Plant: .Ell!- tel<... &ti.~A_' ~I -::J:f\J Tested Analyte: PfJf.J
Date: >.r" {'A - '1'; Orifice Tank #:
Location:_B'rhl\i.~<1 O'..-t-L.+- Pump/Rotameter #:
Run #: 1?-o-M~')rl..-2. pt: Pretest (mm Hg):
Stack 1.0.: It)~? Post-Test (mm Hg):
Pbar: :z.q .7r Tt: Pretest fF):
Sample Tube #:lHJ-/>1SStX;-2u..h¥ Post-Test fF):
Operators: 7tfr- I Time: Start: -- Finish: - Total: 4 "'0
Leak Check: Pre: ,/ Post: ,/ W/B:-=.D/8: - 02:..2.L...C02: C
---
o C c::J =::J
c::::1 r== ==
C]
Time
- -
4k.~
A) /'7~
..
~
r 1 ""
~~v.rs.
int
Num r
~~ttJ{ 0 'f'2,';3,~
15 ~W ,0
~ l>~ e;J5.D
IO~
I.. 'l
I.
I . ~
/. i-
t...r
-
Vb~+- -P:~
-
. Md. (0.44 x %C02) + (0.32 x %02) + (0.28 x %Nz)
~
1X,.. IKP~
~"
fL Vs .. 65.49 x Co x .fiiP x
~
{, Va .. 65.49 x (
!\L.f
'(1 Vs .
~-"
17
&u A..
"
85 aa . Va Ie Aa x 60 aim
is'
7},.. aa.
1ft
~ aa-
~(g Ps '" ~o
G(g 08 d:a 08 x 17.1547 x - x (1 . - )
o ~ ~ 1~
~'1
9~
f& 08 atc:t"
8l;.
~5 088td-
f("
lS:5
Md :a (0.44 X
Md =
Ms = Md x ( I
Ma.. (
Ma ..
Ts ..
,.-:---
r hi. "'a. Pb + S.P. = (
13.e
Pa ..
) + (0.32 x
) + (0.28 x
. -
% H20 % H20
-,.18(-;
100 100
)x(I.-)+18(-)
100 100
OF.
OR (oF.. 460)
) +
13.8
in. Hg
Ts ("R)
p, x Ms
) x(
)x~
ItIs
112
x
xeo
ac:fm
It 17.1547 Ie
It (1--t
1~
-------
METHOD 18 FIELD DATA SHEEi
Plant: epll- Ct>k 2Q.~M SI-~I Tested Analyte: fJIIH
Date: fl-13-~~ Orifice Tank #: - .
Location ~'" I~ () tLd Pump/Rotameter #: »os+-+r'2,
Run ~:~B-()- 'M!550~ -3 Pt: Pretest (mm Hg): -
Stack 1.0.: .oe Post-Test (mm Hg): -
Pbar: ~ OJ . ~ Tt: Pretest fF): :::-
Sample Tube #: 8-{)~'" 1!!>~~ -~ 7vh# ~B, (. Post-Test fF):
Operators: Tfi Time: Start: -Finish: - Total:
Leak Check: Pre: V Post: W/B: -D/B: - 02: 2' C92: (:)
---
gg88
::J
Time
(Nt-
o 'j) /(/ Jlj
Po .\"t-
\/....
T-::t.rs8
nt
Nu r
D~J{t> Y }!::t..£ 301
1010 23;
/oil..5" ] -,
I off) .:g '1',"'-
/cf;!i" ~,~
11/1) ",!:i.
11~5 4.{ i ,2
/I~(J ~ / ~f"
"~~ f~)'
/2Ir7 ,<7;L
i ?J5 /., t'),2.
/"J«tJ c;30
,vr~ :<::... / .:l5'S i ,!sf)
c}(~'?-( J4(j).lL{I i,;f'{.
142,1. ~ 1"" J
'JID
fYJ'7-:;~ ~O~
,~ A "9tH
IfJ1I& I) q ~ 7
I('ll. () 1 ' u
't'l() ::3" K7
1,~5
,?IIJ JtJlL£
Gauge
Vacuum
(Hg)
-
'-
'.
"...
II.L
~IoClty
.0
in. 'I,C
4
'-/
'1
'"
"
'~
6(
J'f
4
II.
d
'J!
Ij
~
'-f
1./
i.I
~
~
4
''1
L
t1
.~
II
11
Flow
Setting
RoI-
~
T...~~
OF
J .51
'7..
a
K
~
I.q
,,[.0
J.
J,
I, (
/, "}
/.
I, '9
i q
I, '1
1.4
I. ,
/.<1
I. q
h~
,...,
'4
d). 0
iJ.v
19,0
..1..
~
~.A
-
'17
'1.7 h.
Md '" (0.44 X %C02) ... (0.32 x %02) ... (0.28 x %N.zI
Md '" (0.44 x
I + (0.32 x
) + (0.28 x
Md =
% H20 % H20
Ms-Mdx(1. -. -18(-;
100 100
Ms - I
)X(1.-).18(-)
100 100
Ms -
Ts -
OF ..
OR (oF. 460)
1M P Pb S.P.
s- +-=(
13.15
) +
13.15
Ps -
in. Hg
'1
,1
B.3
14
1D
q~
1.3
15
q7
~
I tJl
1"0
!s-
q(,
11.t
"'/
'.3-
8'(,
'3g
It
-------
FIELD DA'IA SHEET
Plant: Be~/L~G"" .5+ uJ
Sampling Location 13./1 0...4 (,,+
Run Number: I Date: 9" {I- 18
Pretest Leak':Rate: ().OD3 cfm @ {S in. Hg.
Pretest Leak Check: Pitot: iF Orsat: tJ J A
Sample Type: rfI3fS Operator: AI~
Poor: ~tf Ps: ~().05" 1i.10 (-O.~l)
C02: Ib- 02: 'lQ.1
Probe LengthfType: l.P: ,1c.J( POOt II: 5!.-
Stack Diamete~: I :)21 As: 03.~1...
Nozzle ID: /:).». Thermocouple II: rSi3
Assumed 8ws: L Filter II: 0307 r g - 6 Co
Meter Box II: 4- Y: O.cr:rf £\H@: /.9}"Z-
Post-Test Leak Rate:~.oo3 cfm @ L in. Hg.
Post-Test Leak Check: Pitot: ,/ Orsat: N/A
t<.~ z,.n, I l.'L,1.')
Tr- S8mpIing Qoc:k TIme Gas Meter Velocity Orilce Preaaure Difterential Stack T emperatur. Impinger Dry Gas Meter Temp. Pump
PoInt .'Jme (24-hour Reading Head (6p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) fl3 In H2O Desired Actual (Ts) Probe Filter of (Tm in°F) (T m out°F) fm. Hg)
I tJ'b- 15~. 45) ~/////////////////////////~'l"/////////////////////// //////~
I .f:r 1031 1Su.1S3 O~1 rJ~'l..-.(, rJ'~IZ,/ \1..4 ;Z&l 1. (,"1 {g'J 71 77 1-
1. loY, 1- Sf. ~ 0./ ().l.( o.?/ 131 1S-t{. "t(,'t 65 17 1-7 2-
8' (04.> "'4,c). ( 0.( 0.2( 0.2..( 11/ 2~ Z~) (,,0 -=19 79 2-
1"2- loW 7..(s) {. 'f () ,( 0- l..( c).v /7.8 Z.~1 2.uff- .Jf S''t. (?( 1-
/J lor-I 7-& I. 7- O.?~ 'Z.Vt. -z.o /uf 253 z~5 53 ~ fa tf
IS I()s~ . f.-(s,3. J oj tJ. 2.( i!J. 'L/ /J( 257 ZCH Stf 1& 77' '2-
,,0 I'" 58 +"'1.5 f).( O. l,.( 0.7...1 13( ZS'1 l.(.,-> .57 ?-:} 7& .;l
].5 1103 f(gc..o 0- ( C>;u 0.2./ /27 2.4J l.s( 57 ?-(p 1-CD ;;Z.
LI lIo~ t-CJ,:j. c 6.Cf--z.. l-~ c., 2..-0 /]:1 t..(g-z.. Zf.> Sf 1-1 7~ 4
)<> /to8 fCD f.( 0.( O"l...( Q.'7.' Ill, 25'"2.. "L.5"~ ~?- f-J- 7) '2
J.. 34 11/1 7-10. i 0 I O.U D.U /1/ 2~ l $"-( St, '1'" 7~ ~
.... 3'7 Ute.... f~.8" c.; ()l..( o. 'z.-( l,;,l'j 2;;,"- -z.so .sTo ?-5 ~ '"t...
4c '"1 71-1. ( ;'0 2-.( z.t /J'fo lSb Z~'2.. J1., 1-.5 1<4> ""
~'}.. /((1 11;,<:> 0.1 t/. l..( ().l./ Isl 21- "" 24P Sit> 71. 1<1 "Z.-
H /fvt 1~4.1 ().' o. Lf D.l.( 1]1. 2,!;5 I..,J( ~ lJ '11- '1..
S'O 'll:J -; U"-t. 1.1 2.4ft.... 2.'" IJ3 '2 'Sf "ZS'1 51, 1,. ?s .s-
~1- ((21 ~.o 0.( tJ. l.f O.ZI Ij; z54 z;$. s5 7'1 15' "2-
5:t- 1f}1 1~r.{ (). I 6.1./ 02-( 1)5" '"J:P '1.55 !1' 14 t5 '1
(00 ;lH 1- "'7-y..f 1 (~ t.". z.." 137 Z..f"L z.5J.. S;j- 11 19 S"
(gz... IIJ'1 1ft. v o.{ ()-l! ().v In "Z.:53 zfi S"f. }8 }9 -z...
3 (gg 11~5 181.. 5 0- 01 (:).;8' D.16 In 1~ 251 $tI 1'7 1f "l..
1/ /l'u "}iJ..5' o. &,} /. 8~ ,. '7 138 ZH l5( .5" 71 1J 1-
13 1150 '185,1 0.0-1 I).ff ~.U IJ! 7.53 -,.s5 .So 73 1
-------
;L
of
tf
Page
Plant Name:
Run Number:
B~4~~,. $f-<..L-'
/ J'1 31 S
Test Date: -L: 11- r~____- u.--...--- _.__00_.
fJ II 00+/,(,+
Opera tor:
NAJ
\"
Traverse S.IDpli"l / Coc:t TlID' Gas Meier Velocity OrifICe Pres. Differeolill Stick Probe Impinger Dry Gu Meier Temp. Pump
Poinl Time, (24.hour Re8dlns Held t> p.) (011) IlL 1110 Temp. . F Temp. 1 Filler Tcmp. Inlel UUllel Vacllum
Number (mlnj dock) ,,'}ftJ IlL 1110 Desired Actull ft) Temp.. F .F rr... }. F fli_.) .F . In. III
11 1 ~1 1 p..O" l-t~ - 'i 0.0+ O.IS- 6.1)- IJl. -Z S 1-J i'V -l.
18 I) ZIS 7 'rt. J" () - J-o i. ~J 1- ~ UJ z.n I z. S-( .s1c> }CD :fJ "
/00 1 1111 '~"'J.~ a.Of O. l? Ol?- IJ~ "lS-{ I 249 $"ro 7?- M 1!t-z-
,I 4 10 l- 1 illi 7-1<{,TI C.oJ 0- c <.D 0.0(. /31 "Z:J1 1 7.::P ~ 1-5 1-<.. 1
;)5
.~ 101 1 12.1+ 11<1. cr Q,C); 0-..;,<" G.O <..> i~o l$il.. I l. S'"/ S1g ~ 1-1 (
.cP
bl, ~l# IO~ 1 I Z. "2..-<" 1-1 S.J OcR'] 1.3v /.3 /1.1 ZST I z-S''"" s-' 17 N .' D..:.::) O.f6 tJ.t16- /30 l.~'f I "isl 5+ "H- N f
O"l1/LJ I,u I /,Z"33 1'i1.,- 0.65 O./J~ 0.1'0 /10 -z:SJ 1 z..sf S1- 7+ 1J- /
0. ,.sO Iz.( I I '7./1 1-11.1 0." S' C).I C O'(>J Ilo '2.051:.. I.z S'J SF- ~8 11 I
I-Z~ 1 iz," ~ 1'i 7, ~ O.u.o 1.1.- fJ> 1-) 11. (, 2. 5S- l"t $'"q SJ 7J 1'i' :r
1'\.) I 1 2.4 'J, fOo.t- 0.05 "./~ c)./a /"2'" lS4 1 z:;~ S"cf 1'1 ~7r ,
130 1 ,lAt iC(.:r D.cS' 0, I () 0.10 115 2.5) I "lS' 5~ n 7-'1 I
~ - / \ 1. ~ 1 i 1.SJ ~02. 711 - - - - _, - -
- - -
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\4} 1 i.h1 f6"~ O.p, O..I.S 0."') l3z.. 1- 5( 1 tOO SW 11 R- .....-
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15
-
-------
Page
5
of-L
Plant Name:
Run Number:
Be-l-Irkhal'-r ~ W
I /11115 I? II Ovf/~~
Test Da te:
Opera tor:
_J:.-11-1~__._- u..-.----- -'--'-
JJN
.
*
Travcrse 81m"';", / CIadr. TIme Gas Meier Velocity OrifICe Pres. DiUerealiai Stack Probe Impinger DI'J Oas Meier Temp. Pump
Point Time. (24-hour Re.din! I lead (> P,) (cll)ln.IIJO Temp. . F Temp.' Filler Temp. Inlel UUIICI Vacuum
Number (min.) dock) (" ) ItJ 111.1110 Desired Actual fU Temp.. F .F fCo... }. F (1;_..) -r- In. II,
3-=l /1-1 I /404 g(C6.Q () '/1 o.iS C.l. s- l.sf' 1S" I 25/ 1""1i4~! 7':/ 77' 1..
lB I 14-/" "y'j1.) ().{p lCPJ (.-:; (fa ZS1- I zS'f ~I tf- fo f
J86 I 11/1' 110.1 0./2. 0.2. S- Q.~5 Nt 15~ ' l5")... ~t FJ- tft> "1-
I'll I J~ 11 g' Jj . I 0.'0 I-h /.7 /4-0 lS'f I Z S1- ~~ '1f 19 ..
IQv I \4"1-'1 iZt-:f O.p... (). l. 'j <'. ~ ~ l'fo lsf; I l..Sl.? s-i H 1-'7 <)'.
20;- I 1+35 Klu.4,- O.(z o. t.) ".l. l' /41-- 2'f~ ' ZS-I S5 7-'} Ib 'l-
"1 1'* I 11-1+ ~'2=1.1 0./<. (J.t.~. Q.l.>" Iu'J 0-(7... O.l5 0 l-S" 1]1- lSu ' 2. S'1 S'1 'J-':? 7-J L
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1. 34 I r~( ¥JS-J (!) . d;J t.o lA) 11~ 'ZtfJ I z.s) .j1; 1~ 71 «.
1.31. I l}tJ'> KJv.~ (J./t. O.t.Y O.l~ /J~ '2.41 I zs1 J7... 1-" i~ l
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2- ~4- I ) 721 )I'll. Go (j .Il D.Z.S 0:2$ 13(" lS'f I 2.5z... :5'"7- 7J> 77 -z....
z.ss I rtJ." ~.1.( O'~ /.71 7" /]'.) 751' I zsc.. n 11 ff) 1-
lS'). I Ifz.
-------
Plant Name:
Run Number:
!?t: I/,!Ltc.#~ rbL-
/ f11 lis 11/-1
OuH"'t
Page
4-
of
o
Test Date: _E {d~.f___._- --..-...--. -'--"-
Opera tor: rJ tV
Travcrse -"lnl/ Code Time Gas Meter Velocity OriflCc Prcs. Diffcrcatial Slack Probe Impinger Dry Gu Meter Temp. Pump
Point Time. (24-hour Re8dins I lead t PI) (cll) IlL IlzO Temp. . F Temp.' Filler Temp. Inlct UUIICI YaellUln
Number (min.) dock) ""ft) ilL IIzO Desired Actual ("() Temp.. P .p rs.... ,8 F ('Ii.....) .p . In. III
'1- I J.J,. I Fl.s:J' gso .181 Oft 0.7.£' O.l j" /1"> 2~ ' Zs-.,. t?, ~ "7"'} t:.
1,1-5" I l rot frS/.o () .1D l.D L'O I3CP Z~.J I 25S (,( 1/ 7..1 f
111 I ,~():s JSl.' 0 .{~ O.2S ().zJ /1.:; 2 S1 '1~ 1.. S~ 1J ~7 ~
1, 'l.lf r J f/O P S.s . t O. /'2.- d.U' d.l Y' /35 2S; ' 2S g ~ 1? 4-
2M- I 1113 flQ-.o 0.12- c).l.S t/.1J /~o 'l.~-I ' Z ')'Q ~ ~ "/"1- l.
Zq:; I tJ'f J'n. ""L. ().97- ;'V I.r I? I' zs,' 7~/ s;p ,c. 71 4
1 217 , I 1"1-J it.&, a. Co ".17- .- cn..r (J.tS III zsz.. 1"L.rG. 1V ~
51 'l.
104 I I ¥'O F~?.. <.0 a.IL ().z.) o.z..s I3g ZS) ' 'Z't> I .5' 1-s :).~ '2.
4- 3tH I iJ'~ ~CQf'. o. I'" Q-Z-S (}.7. $ J Yf..' Z$9 I -zs, $1 ~ cfU ""1
~J'Z- '{1'}4 rC,q.7 0.5'0 {.f? l' IJtf 251 ' 2~;> S) ~ ~ +
11,. " ,...... 8~~J O'('L o.?"S (J.z.s. 13S" ZS I I Cf'f-c:::> Yfdri" l./ ~.3 t.~ ;10 1.$0( ' "l q.~ n, 11- =t1 s;
I zs" ' i' q1;' "i J'"l.f o.l~ o.a
-------
~,. f!III
1~>,,:;,!;.~JI01~;;.,p/F £''''1
D PAcu:1C ENVIRONMENTAL SERVICES. INC
4700 Duke Drive. Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Plant.-f.fA c.oI
-------
,
FIELD DAIA SHEET
'Plant Bcll-/<:h£# S +e.e-I
Sampling Location Ov~ Ie. \
Run Number: ~~o-~/.s. 1- Date: 8~ /2 .'1 J-
Pretest Leak Rate: (') -OO~ cfm @ ~ in. Hg.
Pretest Leak Check: Pitot: V Orsat: tJ tf\
Sample Type: ? /5 Operator: W
Poor: ~1'1 Ps: "'0 .C,! .
C02: -e- 02: 205"
Probe LengthfType: .f I f/4sr Pitot II: ~
Stack Diameter: /oK" , As: ~3.{,1.-
Nozzle ID: D.2JS Thermocouple II: SHJ
Assumed Bws: L- Filter II: og6lQg -0
Meter Box II: 4 Y: O.9-rJ llH@: /. 'j.:]-1..
Post-Test Leak Rate: D-Oo' efm @ 10 in. Hg.
, Post-Test Leak Check: Pitot: v Orsat ~
- k: 2.8 -
T,.,.,.. Sampling Qoc:k Tme Gas Mete' Velocity Oriice Pressure DiflBrenlieJ Stack Temperature Impinger Dry Gas Mete, Temp. Pump
PoInt TIme (24-hou, Reading Head (lip) (6H) in H2O Temp. of Temp. Inle' Ou1IeI Vacuum
Number (mln) dock) (Vm) ft 3 in H2O Desired Actual (Ts) Probe Falter of (Tm In°F) (Tm out°F) (in. Hg)
4- I 0 8'i~.51~ 'l'//////////7//////////' ~////' 'l////////7~////////////// ///
~ OCf-z 1 ~1~.S(i 0 . i z.. 1).33 0.$1 /4? 253 25 v (p(p 18 1'1 ;;l
~ Otf) 'f- 9;,1." Off 7.,S- 7.S /1<; 7.44 ?~&, (Ps 71 75 S
1 6'12 ~ <19l. ( O.j'\.- O. '?l on In ). '103. F 0.1"1.. 0.33 0.3J I~o 14~ LJ 6.J) 14.1 l,j'"V. !' 2. (,;,(.J (go ?-)1 9'1 t..
2 'Jo 0 '1 S'f 90 t 1- t;>.("1. D.31 O.::Y) /1f- 25' 1Sr (j,v M s( ~
4(P of () r- '11/, .J 0.1 '2..) 1.:J /Cf-5 'lS-2- 25=1- <.9'> 7-) ~I ~
3.sr 0<1(j} 71].+ 0, I '- 0.:17 o. J") 144 lSI l..st? ..5"G:;. 'f1 rf-d -z...
~) to I 7.. q/r. F O.('\.. O.':$J ().;J'l J(;? '2S) 2~1.- £"} if 8''- L-
4.> IOI'f- C-f/ (g. I C-15 Zf 2f I s
41 1°10 'j, 1-1 (1~ I ( 0.31) (1.3 }«J '21f1 z<'-" Sr fl ,Fb z..
5~ (oH 'i"2- r ' () O{?> 1..10 l.~ 4T 2~' 7fC&.. S0 '71 8) ::>
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~~ (oS,) Qt?t.1.- O. 't $ "l.. Co 7 ]..7 14(. 2 S ~ 'LJ 'f- "7 fo il S
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10 ~ Hn "/4 t.o (j ./0 V. tl D.ll . I]'; z61 zS1 ~f 74 f4 1-
liS l\1.'t 1 ii.;) 0.1.J [.1 l1~ \ L\ 0 'lS"1C Sn CI1~ 1
-------
Page :t
of
Plant Name:
Run Number:
(1(. ~~ I<-h~ M
R- 0- 5( S - 1.
~\~~
Test Date:
Operator:
_m'L! ?-1 A-
\4-'1 / )'2.>:> '154,.cr 0.3-0 2,14 1..,"" /:{::> "2S-z. ' ZS/ SJ ~ 7J .5
I ,\:c1 / i13'1 '151.0 d,Ou. D. n a,n... 1S1 "lSV / lS3 5] 7-c. .~ i
2. 1St> '/2.3? " 5 7. 3 O.u~ 6ft 0,17 I~! 1rl / L.5I $'> 7-~ t-J 'I.-
1:51' / i 2.'t-7 '1 ~9 . 'i v.iS '2./ '2. I J 3 f- l5& '2.0- 5J 1-<0 7-?-- S-
Ilil ' j''lNf '1'(,/ 1, o.(.)~ ().11 0.11 D~ z S~ , 2- J"<." SJ '1--" 1-1- L
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3 I f"I I 1101 '1fJ1 5" d. g.1. 2.) l.; Ito 2st ' Z4-} 5J ~ 1-3 S
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Iq~ / I1tv '-1 J.1. ~ r'H1..- ?'~ l ) 1« z~ / 2S-f 54 "f{o 1-J '-
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4 2.10 / 13?;.b c-l ?-;. z,- O.dj fJ. {. S ~,~5 'I) -z.H' 1 no ::J-tf }-" rtt "l-
11-<; / i54J 111. ~ D'1iY l.rD 2.-( I'ZJ 218 / 2 $1 55 1~ rt 5
1.11 / lJ C(8(.{ o.() O.L f O.2P I Z f 251 I 254 5"" t-G, f} ~.
')...\'\ I i"bJ-f 1 Q«5. \ ().l5 1.1 J.. ( '''"l 1l.J 7:J I 2J./1 SfJ 7(, 77 g
/ 140.3 0~.g 0/O ~.:l6 0,25 t2~ ,Jq 1/ ')'15 ..57 7l.r- ,7 '2-
'iHb5 ~ ~q, l. 0,1"2...- I. ~ I q"""" / 3D lit! ' ,)..4_<) 5(, 75 71i -S
1. - ( 3-Llo "40~ ~9 Do!'23 C,6 /~ Z-
1.41:1 '14/7 - ") cr 0 . 'J,~ 0.09 0 .l.<; O,'U I ~7 )S f '~,!~ ,r~ 7ro 77- 'J,.o-
~5Z I ftJ ~~~
-------
'1.~.J
'oJ
") JO>
; v'
..
Page
of
3
g~hfJ,~ StJ-
Test Date:
Opera tor:
_~/2- CfL__.-- -_u_."--' -.-_u-
IVtJ
Plant Name:
Run Number:
P->- 0 - 3 t s - 1-
Traverse Samplins / Oock Time Gas MeIer Velocity OriflCc Prcs. DiUcrcoliai Slack Probe Impin&er Dry Gas Meier Temp. Pump
Poinl Time. (24-hour Readins lie ad t p.) (011) In. 1120 Temp. . F Temp. I Filler Temp. (' Inlcl . UUIICI Vacuum
Number (min.) dock) ("- ) IIJ 1n.IIzO Desired Adual n) Temp.. r- 8r- T... ). F fli.....) 8r-8 In. III
I tn 'I s-4ct <191.3 o.t, 0.1..6 1). 'log '31 2JJ 'ZS1. S-(e, 74- 1-s 1.,.-
~ z~t' IL>~ 't'~1. J 0.6< ,4 1..tf 1]1. (~. ( (j11- 2.. (~ l.."'- /1 f 2S.r' n;J S'f 15 7+ ~-
.~ Jr.' I l~'l.~ 1\31<1.(., (). (c::. fJ.--V (). 2f~ }-;q 2'$1 I Z5'- j1 ., 'j 1') 2
Jil / 1(,3f" I~J 1'7, 7 .110 z:z. Z.? ,"$'1 251 I Z.$2 .5,.3" 7(, '77 6
~/.3 ' (c;. '311 1011."" I(J () , l1t o. l. r- /~" 2~1 I Z<~ .)5 {(, 77 Z-
-:?z.o ' l o.z$ /24 750 ' 2SJ .£1 1ff 18' z
3S'f ' ;1'~ I v )~~i .tI.Cj~ "L~1 ~.(., 115 7~{ /1S+ S?- t?- 1/ 5
~(,o / \11 1..~ ' i'S\> (p~ 7-H 7f z-
7.lq+ I 1ft\. II) "1\ I If.e; 1..) 1. -r 13 \Q ~~"t I 'lS-I Ss- 7-~ ~ s-
t.t, 'i 'nqq. \O~l. I 0.)] ".)~ l).}~ U<.> '} ffJ '750 S] -JJ ?t '\...
11 + ' n~1.. loq~. t 0.$0 1..~. ~o 13(, ~5; ' 15/ 5' +l "17 5'
31-' ' HS4 I o 2.0 LlI . ",- Z.13 "2~} 51- 1/ 19 S
~ 1~ ' llDS \()51.(, 0.1).. ~.~ (').t-" 13'" z'S( I 2 (,0 S1 t-J 7-7 '2
), .,
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4!'i
-------
Page
4-
of
1
Plant Name:
Run Number:
i5~Jhk/q~~ j-i-J
IJ- 0 - ]1.)- L
Test Date:
Operator:
_!i-I"l-'7tP ---.-- --.--...--- ---_u_'
NrJ
Traverse Sampllnl/ Cod TIrH Oas Meier Velocity OrifICe Pres. Differential Slick Probe Impinger DfJ Ou Meter Temp. Pump
roinl Time, (24.hour Readinl lIeld ~p.) (dl) 1n.IIJO Temp. . F Temp. / Filler Temp. ~mct UUllct Vacuum
Number (min.) dock) ("- \ ftJ In. I b 0 Desired Actull ft) Temp.. F .F .T.... \. F ("Ii-.,) eF In. III
J- ?7"f 11ft] 1052.( 0.11"'" 2.4 t.'" /35" z.q.~ / 21=(., ~o -:).1 7-1' S
400 I ItiS luS-3.B 0.(1 030 O.-g::> /35 2«:'1 '/ ZSC 57 7J 7cJ "L.
1/'1 I rJJ ~ /oS'7.~ 0.4-' 2.~ l.lf Iff 2~(:, I 2~" 5"J" f1 1-J S
4U I JrJI.. 10M., 0.11 o:~ 0 O. '} 0 ISf t. S"i / ZS3 5""1 1:( fJ 2-
J ~~ I I l14(' /<3C.S;b 0.1') 'l-.{) z.o 13"- zSl. / 2t.f~ $(. 1"f Sf 5
433 I I5tt 5 l0{gc..\.. (J./f 0)- ().).. 115" 25"1 I l'f'l 5t. 7--:r .Fe t.
~\) / I )-5~ / ol.P'i. 10 o,1~ 2.1z. 1.- ( ns 2.$3 / ~41 ~ 1'+ ;:0 s
.w-". / /851 Iota.:> 0.11 () 1~ 0.)" 1)"- ~ 5<" I 1. o.~ In ,$.} / 14.t ~8 1-1- ~ '2
l-tl.() / It'\ ,t;' !o,1,'-! .qQ 1.5 ?.5 1;'2. 2S' /1- 50 5~ 77 80 ~
4 c. t.. I \ &t 11 ,A .,~.Q .11 .30 ,:J/) 1)1 2$7 / 25' :Sf{ 77 ~o 2-
~ I I'fZr I 0 3'~. jldf - - ..... ,.... -/ - ... - -
,
/ /
I /
I /
I I
/ /
I /
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I t /
I .v /
/ /
-------
O PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Plant:
Sample Train Recovery Data
Cob*
f)*#
Sampling Location:_
a
Sample Recovery Person: £k/
Sampling Method Type: £ffi 3/5
Run Number: g-Q- 3/^-Z
Job Number:
, OoO
Date:
Field Team Leader
Impinger Train ID:_
Comments:
Filter No.:
Filter Description:
Filter No.:
Front Half Data
Filter Media Type: &&At fti*r f<\
//*-f- as^
u
Filter Media Type: ^
Filter Description:,
Back Half Data
Impinger Purge-
Start Time:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Flow Rate:
Impinger 1
l\?U ^0
£^^7.-S
5W2-
^T.S
Impinger 4
<=
fy
1 1 s'-tf ^T fai
~70(e,(t &Z7.1.
"I. 5- JJ- ^
Impinger 5 Silica Gel
(a): "7 /O. J
(a): 075-.V
(Q]. ^5"^ 5~
•^
-------
Plant Bel-h/Jw> Sic J
FIELD DA i A SHEET
Operator:
Q>4(«.J-
Sampling Location l>-
Run Number: fe-0-to-S Date: ff- J5-1 *
Pretest Leak Rate: 0 oo? cfrn @ IS in. Hg.
Pretest Leak Check: Ptot: i^ Great: ju/A
Sample Type:
Pbar q?.?
Ps:
O2: 20.?
Nozzle ID: 0 i"Z5 Thermocouple
Assumed Bvw: ^S_ Filter
Meter Box #: 4
Y: o
Probe LengthAType: 5
Stack Diameter: |o$"
Ptot
As:
Post-Test Leak Rate: a.c>o4 cfm @ /_ in. Hg.
Post-Test Leak Check: Ptot: i/ Orsat:
Point
NumbM
Inlet
Outlet
Swiping
Tim*
(mln)
dock Tim*
(244KMIT
dock)
GaalUtotw
Reading
Velocity
Head (Ap)
inH2O
Oil ca Pressure Drtterential
(AH) in H2O
Stack
Temp.
(Ts)
Temperature
°F
Impinger
Temp.
°F
Dry Gas Meter Temp.
Pump
Vacuum
(in.Hg)
0-13
2.C.
/20
75-
o. K
Jb
_o_il_
z?
ff-7
O
0
0-3f
2-
20
0-37
u?
z-S
ST
0^7
Ho I
III
OK
O-3-r
0.3?
/Jo
1*3
H4-7-
O-'Jo
-s
Z-jT
/34-
iff
s*
5?
o-Jt
6 If
n*
0 f 5
/w
230
-2s*
7?
fl
(OO'?
o.
so
Sf
Iff
1±
'3
2-75
IS'
5
St.
/UJ
-------
~
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(JJ> \
e'
-O,~1.\
Page
of
2
Plant Name:
Run Number:
~c~lk\1~,"", r~-
\?,~O- -;lS ,,3
Test Date:
Opera tor:
.).
8 -fJ-~1
------.-- --..-....--.. -.__."_0
;JAJ
Traverse -1'1101 / Clod Tim. Gas Meier Velocity OrifICe Pres. DiffereDtl~ Slick Probe Impinger Dry Ou Meier Temp. Pump
Poinl Time. (24-hour Reading llcad t> PI) (cll) IlL 1120 Temp. . F Temp.' Filler Temp. I nlel VUllcl Vacuum
Number tmln.) dock) ,"- ) ItJ ilL I b 0 Desired Actual ft) Temp.. F .F fr.... ). F (li_..) en In. III
~'~r:' -I I 'LV I 104" 2- ) S ?1f~ 1 Oov Q.lt () . (:) 1<3 ei'fJ' ':lSO &3 1l- 3;).. ;)--
12/0 I IO~ ,4(,"1.- O~6 ).{Q 1.-( Il.!; lSO I )Sb 57 8/ $I( S
\..8' / HDO \4 ;y,t- n.01- 0 lO CJ .'I-~ /3Ct> 2.51 ' l.S'f £8 JY PI ")...
131 I 1/01 /1 ~.3 ().3'0 ].l'f l...,1.. I 'to LSV ' 2.r"L SF ~( ~3 5
1~'1 I 1111 (4~. i D.D=1- 6.2~ o..z..o (tr LSJ ' t.J'p Sf ,!, 8') '}..
)<+1 I IIl1 Iqq.o (J.1r {.1- z..."" }4:f 1..S1J ' '2.3"'L. 51 8'2. JJ S
J+7 / '1 z I jg,.' l.$(., ~ s~ rrJ L
I~ I~J.'f. o.fu O.1-} 0.", 131- "t.J'<- ' Z Jf., Gv-o 1-}- /-I l.-
1 )10 I 115). he1. ( o.f () O.LI b. z.~ i11 zJ5"']-S"1 (gC 1-:J fr 1-
If7 ' //>1 I u'f, cI ~ ~() ).;l. ~ ~ J!.'j 2 S'"~, 2~,-/ &0. 79 '30 ~
/'1 ' /201 i fR&, c;L ~tJ{; , i~ . I t:;' /lq 2.S f , .J.53 "0 77 ,#0 ;L
I ~ CD I t le~ {~k. 0 ().te 1.1- '1. 'V I J' -lS5" I 1.~ (.9:{) j: ~ yl "2.-
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-------
5
of
Page
Plant Name:
Run Number:
-15 L ~h k~&~
fS-o-1t5-'?
s~
Test Date:
Opera tor:
-$',3.-'1J' ---.-- __00__..__- ----..-.
rJ,J
'.0.211
Travcrse So"pll"I/ Oed Tkac Gas Mclcr Velnc:ity OriflCc Prcs. DiUcrcaliai Stack Probe Impinger DfJ Ou Melcr Temp. Pump
Point Time, (24-hour Readin. lIead ~p.) (cll) In. 1120 Temp- 8 F Temp-' Filler Temp. Inlet UUIICI Vacllum
Number IminJ dock) 1"- } It) 1n.IIJO Desired Actual (t) Temp_8 F 8F ("Co... )8 F ("Ii_I) 8F In. III
1--1 ~~~ I /138 1&4.01..3 0.0'1 01lJ O.l~ )/ sz... 17 ;:;/ I
~ 1~ I 14.;)/ ,'16,.4- o.I.)Cj o. 'l-r o.\...,..- (4"1- 1Jf ' 7 S"') $"1.. 19 f1 I
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] 333 I 1S""1I 214.] O.b) 1. -44 1. cf- II; 15l '1.451 Gto '}) .fb ?
'13~ ' ISI) lll.l.( t ~l o. 'q' ~. 2:5 II! 75] ' 1..C\-~ tOtJ fJ> It> I
3~1.. I is ~o 2.r~. I ,'6 s 2.~ 1-.LI {Z3 2-SI ' 150 ;./9 7~ (X.J 3
"':14Lf I /51- 1..- )2.0 0 .c..,t) 0.1-5 o,LS 16 P.52- , zC{ 7 17. -:If go 1
'Y;'1, I g'YJ 1'[''7.5 ,~iP 2.4 ~.7l I1,J :?'51.' ~ h1 77 fa :5
'J..~5 I /5;-1 22'1. 7 . v? OtiS 0.1-5 IYt '2 j'Z I 152 ~7 -rl 80 (
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Page 'f-
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"'?:l~ Plant Name:
'~ 4;'~
A~ Run Number:
Test Date:
Operator:
~-/3-c;8
~-
------.-- ...-..._..-._-~ -.--..-"
_R-o - J(~- J
)JAl
Traverse samPlinl/ aock Time Oas Metcr Velocity Orifice Prel. DiffercDli31 Stick Probe Impineer DI'J Ou Meier Temp. Pump
Poinl Time, (24-hour Rcadinl IIcad tp.) (~I) IlL 1120 Temp. - F Temp.' Filler Temp. Inlcl uUlle, . Vacuuan
Number Imln.) doclt) ,''- \ It J IlL 1120 Desired Adual ft) Tcmp.- F 8F (T... }8 F (Ii.....) 8F In. III
I-I 2&;O I 1545 11-6. I 41 007 ", Z 5 0 :Zj' I9-J '1 5+ I '24- ~ to'? t~ ~ (
~ {q?--- I I S&D 7UJ. S 0-16 2,( ;ltf /4't tSI I 211 (PI M >6 5
1(Pf I ) ~5"2- d.;.I J () 07 0.1-5 (). t-f 111. lSJ I ?s') (go 'ff ~ I
3ft. I i~oo lsD. f 6.+( I- C(f ~,o 1# 2S0 I Z:J, 5'0 JI S~ 5
?;\4 I IlIO-v 1.37...4 CJ. (0 Dl-} ().1J 143' 21-1 ' zso ..f~ -ffJ f..c I
331..0 I 1(, {Q l s't-j' O.f5 2.;J 1..1 11-5 2S'L. ' '21f' ~ro ¥( ~) (
'U-+ I lu I '1. Z 31.9. f O,{O (Y.U o.'1f ''\ 5' 15( I l. 4'1 57- b-I 75 ,
.,..... ~I I I b It( eJ.3 1. 4 " ~ S'" ).1 :2. I I iJ '2. ~0';;11'1 >( 1;L f:.f '3
t~.., I 1~a..1 2 "JA'tIJ _/2. ;30 3D H'- ;)~J- ':2'1 R 5''2 ( <6'() I
40& I l(g~ 2*,~ 0.;«; 21 z.( I J'j l.rl I 2~1 Sf ~ N g
d(o I llou '1fSJ 0.11.- 0,3::> (J.]b IJ1 /~ I 2$1 5', ;;, .F'I I
4/ i) I I C4 4-t- 2:51.0 0.51- '1.$1' 2.'- i]~ 1.'$"1 ' l.r"3 ,.-(p f" tf( .3
7 4£.-( I ILP'\'j ;)fl.} 0,/1- 0.7. O.~o IJ.r z..JO I 1.1'7 see. Jo ff I
43<0 I Jfo~ ". 5f. "V "",Cfl.- 2~ '2.~ /3') '~Sl I 2..,0 , 1~(p I l$J $Y ? P> I
~'tr I FH!' 1..(, (. '3 i. [) l.P Z./ 131 '}.55' I ~s-z. 5(P 'n 81 g
441- I \ 1-15 1v'~.1 c./? D -3<0 C.J(; 1-> 3 25'1,..' ~ ';.5 s-c", 17 J>( 1
4 Aw I l'trY ),(04. ().)] 03<. 0.3<' ("3, '!S( ' 75b ~ /-~ J'( I
4Sr 1\ lU',...1--~ 7.(,5".~ /0 'l.t z.f Il4- 2 5~ I 7..$"5 5f 17 h ?
451- I \1~r 'J.Ct 1.8 ~,/", () .J(p (). 3r., /?tf zn. ' 1.-5'7 57 S.31.> l3'\ 2 S < ' 25 } 5'- &fJ ~I I
41'''1 ' 1~1 'n.iQ,> h~< 1-.)j ")./f- 11,4 2S( I Zc;D .sG yo Sf .5
-------
.._~
c:::J c::::J r::::::::J
o PACIAC ENVIRONMENTAL SERVICES, !HC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Date: ?!I t{1} tj
I~ '5
Impinger Train ID:
"lj~:l
Comments:
Plant:£P# G,L~ C.ei~le~flA? 3-1ce/ ehe5,{,/~. 2AI
Sampling Location: ~t0 C!J",II.z-.t-
Sample Recovery Person: K l-Z. Field Team Leader:
Sampling Method Type: /V1 3 I 5"""
Run Number: 13- ()- '3 I J - .3
Job Number: S S- 0 (,., c; (j c
Front Half Data
Filter No.:-D~ t)'lCJ i - :(."2 Filter Media Type:-&'rec! 7-reo..fp,/
Filter Description: v P r v' /; /11 {'
Filter No.: ( Filter Media Type:
Filter Description:
.J k ~~ .p,. bet'""
~
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collect~d ~~ . r ~ f,/'
Description of Impinger catch: (' / ~ c.-....--
Impinger Purge-
Start Time:
Contents:
Final Volume~ <3
Initial Volume~ '3
Net Volume:--tT1'iTJ j
Back Half Data
I
I-
: Stop Time:
Purge Gas.
Impinger 3
~;l;/
-------
FIELD DATA SHEET
Plant: ~ \-\,.. ~~~ ~ ~~t
Sampling Location ~~u~ Ol ,-\-\.e.'\
Run Number: 6" . Dale: '8 -/J/- 'r¥
Pretest leak Rate: \ boC' cfm @ ~ in. Hg.
Pretest leak Check: Pitot JJl.d- O~: -
Sample Type: 3 IS Operator: Db\.o\.
Poor: ~~..; Ps: - (J-
C02: 0 02: .;10 ,q
Probe lengthfType: :5;/:1 '~~rzPitot /I: '1~
Stack Diameter: ---1)./.." As: t\}t'\
Nozzle ID: ,~IS Thermocouple II: "r::
Assumed Bws: .:5 Filter II: OgD7q~-cJ'9
Meter Bo)( /I:!!!B..:rL Y: 1.~..1 i\H@: / ~ '7'<{?
Post-Test leak Rate:..()o.;1. cfm @ 1"5 in. Hg.
Post-Test leak Check: Pitot:~ Orsat: ==-
T lev..... Sampling Cock rme Gas Mete, Velocity Orifice Pressure Diftelential Stack T emperalure Impinge, Dry Gas Met8, Temp. Pump
PoInt TIme (24-hou, Reading Head (6pl (6H1 in H2O Temp. of Temp. Inlet Outlet Vacuum
tbnber (mln) dock) (Ym) II 3 in H2O Desired Ac1uaJ (Ts) Probe Filler of (Tm 1n0F) (Tm out oF) (In. Hg)
,-, ~ 77. 7q~ ;:////////////////h;://///?'//-" -(.! ///////////~/////////P/ ~ h G0.d
/1;0 £) ""577. i 3""5' N I A ~Ji\ k '\11'\ "'lit c:)S"':) ,:)~~ ltt') N/A N Jra.. ,.~ -0,1
III.S ~,-g .005 "",',Q. ..~I.!\ ......,,'" ~J~' J'SJ .;1SS ~o .
,t"3 0 3 7~ . , &, S N I '" D'/04- ,.,.,1.*, ,.J)" I d5~ ':'$S 80 'V ... \ ,it
, T { I
I
I
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1
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~-
t.H..
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-------
lI.r
r=:J c:::::::J c::J
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
£ p;tC'(?le !3p!/t/P/:f/r1?5I-eel
Sampling Location: Er>-s 11 C' (.,( ')(? Q fA"; / f! -f
Sample Recovery Person: t: ~J If I~
Sampling Method Type: fi13 15'"
Run Number: S <;7)(,.. . r) ~t'..)
0-0- 3/5- r/?
He;/d ~/5Jar'L
Field Team Leader:
Date: rtl/ t( (! [
l:Js
Plant:
Impinger Train ID: .AI - 2
Job Number:
Comments:
Front Half Data
Filter No.: elll) 7 'lg' -'d.. i Filter Media Type: ~ rC J r re ~~t~ h (t;.~ S /'; L.. r
Filter Description: flu 17 C2 / i,' cu- ( Do Ie
v ---
Filter No.: -
Filter Media Type:-
~
Filter Description:
Back Half Data
Impinger Purge- ---
- -
Start Time: Flow Rate: Stop Time: Purge Gas:
Imp'jnger 2 Impinger 3
Contents: 1/70 £~/Iy'
Final Volume: (ml) ~/?~2 c(55rf
Initial Volume: (ml) 7/"1- Lj sS-: 3
Net Volume: (ml) 01 I
-0. -
Impinger 4 Impinger 5 Silica Gel I
Contents: -- - S"' ~ 1 Ge
Final Volume: (ml) - -......-. (g): 705.5
Initial Volume: (ml) - - (g): to 5.3
Net Volume: (ml) - --- (g): () " C ')
Total Moisture Collected (ml): -(). I
. Cr~rA~
-------
Plant CD/t~ tel!..! S/~ejJ (!:PIIJ Sample Type:(~4Z, Operator: ~ Nozzle ID: O.,2:J.. Thermocouple #: 6.E
Sampling Location B. fl. Out ,~ Poor: ~1. 7 Ps: .~ - . ~ ~ Assumed Bws: L Filter #: -l~f/~
Run Number: ~Date: B-//-?! C02: 6 02: Z, Meter Box #:2- Y:/OOL LlH@: i /11
Pretest Leak Rate: o.()O~ clm @ /5 in. Hg/ Probe LengthfType: £' POOt #: ..£II. Post-Test Leak Rate:,o r J.. clm @ ~ in. Hg.
Pretest leak Check: Pitot: V Orsat: ..,/' Stack Diameter: 10 e ,. As: <.t:5." Post-Test Leak Check: Pitot: --orsat: ..-'
- K~2,()S - -
Gas Meter Velocity Orilce Pressure Diflerential Stack Temperature Impinger Dry Gas Meter Temp. Pump ~ F
,.
Reading Head (6pl (6H) in H2O Temp. 0 F Temp, Inlet Outlet Vacuum
(Vml ft3 in H2O Desired I Actual (Tsl Probe Filler of (Tm in°F) (Tm out°F) (in. Hg) .XAI)
gj,o. -R l" b V/////////////////////////7 /7//////////////////////// / / / // / //
1t1fl. ( " 11/ .30 13D 130 ).'10 2O I~C 7.3 (,. -zS1 3'~ 7 tt ? 9 :s S"
~:2.,. '1 :JLj 1p ')J~V\.O~.1( J 7,.{) ':1.110\ ,2 r;.> r.. () -.' 1 q) (/' r; 1
, 11. ~ fo. \ l l--r t (i( 'J')~ ., ;"J., ~ t# I ''''L-' ..,q r.& 5,
f? :z..Q. {) , . '.1'\ ;t 1 1:.1 ~'t'1 J./nJ C"1 ') ""rc; ,-.)/
Q 7.11'). V . It .:;0 1:.0 '.:II ~n~ ;Z cl r8 "'c: .s'V '1 ~ 1
1;> t .:>. I . 4: 9 :J, I ':J, I I 9 .2.<':2 ..2 ~ & t;; e P 0 JJ. 0 , 5"
( J .3 I :1, i "~ fJ..~~ ~":J.. $"" '1( :I 0 1 ~8
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. It ...11 ..2~ I%.JJ .al{l ~~I 55 1~ 1~ ~1
,10 ,), I)). J1.4 ,;1&./1 .2101 ~f ~ gO >7
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~I ,),1.. .;z~ '1../. Jtl1 ~'lo ~o Bo PI I S'!
~ oq ,~ .1'\, i~~ ~4~ :J~'d tJO 1q 30 51'
, I. {) 2..0 :1. f\ (2, 1 )c;'""\ ., ClIO (~O ...,c. '"11 I ~ 0
, (\ ..,t~ ,,2.3 15S:; ~~)- '~'5'.1 flO I/o 80 r C;1
. tU 2~ , l..r t ~"1 ~t;8 ~r;u 1i0 tJO R () C;'
t {'L. ~,;J.~ . ;}-~ '1'2 { , J..~ ;Z ~ J (,O 1'1 Ie.) I Gr 0
i D J J 1. I 11"'/ ;J.C'i ;l~' ~., ~O 1° i ~'i
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. d /q a l't l2). ':1-L/'' 2~~ '0 .-,4 QI i fIIO
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"''''''-.-,-''''''P. -----.
- p
1~~'\~' .
Poc ~ I
Tr..... ~ Qoc:k Time
PoInt Time (24-hour
Number (mln) cIocIc)
( 0 ;0''1
} Ib~~
.3 If) 40
q I/f\Li {"
;~ Ineb
I" JAt:',
Ii i ~ c't.
~.. "1'\'
~ f1 OL,
2AJ 11
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t.b II l(,
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110M 'I'il
"I. DC /I L(S'
/1(,,01) 1I~:3
1.21 00 \l .:8
I :Jia rn I Z. bl
, ~ , ,"" , 2,.CJ"4
"J-cc , 'ld\
~14. , ; ~ ~ ':J.,I ~
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FIELD DAIASHEET
. ,
- .
tJ. ~l_.;3
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Plant Name:
Run Number:
~,J.
/3 - D... fYJ'IJ1 ~ I
Page
,;l.
of
'-I
Test Date: _8.::.1i!l.S---.-- --..-...--. -.--..-
Operator: 5B
Probe Impin&er
Temp. I Filter Temp.
Temp.- r: . r:
,2t./{ A i I ;lIt) I.f')
014l~ I ~~t;' ~ 0
Jqu I 02)1( S~
)"1 J I;" I ~tt
';'1)- I $ii..J (d'1
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I
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, .~u ;.31 I ~~ 60 .
13C'" ~ J' I ..1. <"": ,0
11.1. ~1C; 1...t:;1 r.D
/-~l, ;Jj, I PII< ~o
I; 8 ~~'1 I ~ t;L,' fPO
14 'L l~cI~ I ;t" uiS
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I~a, ~~ I pfJ» (,0
...,'0 J.~ '" I ..,,~ ,()
J,LJ 0 .;23"'1 I ~"I ftO
I'" ( 'J t9 I ;J..~r- ~~
Velocily OriflCc Pres. DiUercntiai Stack
IIcad ~p.) (011) hLlIJO Temp. . F
In. I It 0 Desired Actual ft )
~ I ~ . ')S' , X" 12 .2
I 00, . i q . I 't I~ :;1..
'. -1 b I (" I. r I 3"L-
. "0 ;1 I . ,. J ~>-
010 ,.,II ,}.. '13
, in D J '? 1 j 11 0
, I J .~ ~ ~ . .,1 j. \ ~ I
,0 - -' \ . J. I I);
Travcrse Samplins: leoct Time Gas Metcr
Point Timc. (24-hour RC8dinS
Number tmin.) dock) t" 1ftJ
.I J1 11/2 00 I I z. zo g,;}. .).
, t.llt,OO I t22.> ell'.. ~
I t41. Q'} I \ l.~ ,~& .1
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t ,cLoo I f.l3/o g 10. D
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ia", ()1) I flLit; 6ilJ.O
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.r I I ~2.n a 7"1. J{,(J
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(I) 1~"-c:rID I I ~~'lf. e 0D ..., . i' , :J-1. ~ .t t
I I I ilL4\ 8~;)...0\ "~i.. L-r I 1
ItA I ,1.MfJ ~BlL'"7 . /~ ,,~, eX"
~ 1 I, ~ ~ I ~ 9 (t) . $" . .~q I C.., t .,
:J fL~ I a 1. '(fJI. R R Q t- ,(J."'U"<" '~9*f c .1o..scr
- - _.& I 1'4 Otb gtto. j ~~9'" t. '1 " I. ~.
'Zt::ftO I Iud: 9.or~. /~ ,I~'~ I~
fl) J.O.oo I /u',f'\ <; ~ t. ... , I ~ .:n . ~4
" &./ C (j) I iti f~ ~G}". -'I . I't... .;1.1 ~ ,. -1
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C~m I Iii J..C: ?q({ I U .i' .}o..1. t ~~
fDO.OO I ic.4 ~O j 00 v "..,0 I. c; I. 5
/ ,¥I e,: .r)O I 14:3 c; 4:" 0:2 () . ( 0 . Jol .1. J
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Dry Gas Metcr Tcmp.
Inlet UUllcl
rr....'). F (1I_..).F
-,q eO
,q 'lq
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iet Ro
7 A "11
1~ 7tt
1lf go
-., tt 79.
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-------
Plant Name:
Run Number:
~-~--
J'-D- ml/:li-I
Page
Test Date: -~-U-1g
Opera tor: -51>
.5
of~
_._- -_.,,_"-0__. -..--...-.
Samplin.: jCock Time Oas Meier Vclocity Orirlce Prcs. Diffcrcalial Slack Probe Impin&cr
Time, (24-hour Readin, IIcad ~p.) (tJl) 'n.IIJO Tcmp. . F Tcmp.' Fillcr Tcmp.
(min.) dock) ,,, )ftJ ;"In.IIzO Desired Actual. ft) Temp.. F . F
HO.oo I (4 '(0 C:~f\1 n . tPI Ita I.IA ,..., () )2)' ;;..C:;, 'D
IISC!XI I 14c.1~ ~'o4 D ,0<0 ~ I ~ .I't.. I(p) q .2.;~ '.25"if ~O
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t ~~ 00 I it.{ S5 't 0 to. J- :bL- .. f)q ,nq irLI;J;t./ ' :Ill ~ ~~"
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/~ lID I l7 l:Z. ~ 2. I I /;. 01 A.~ ,~~ I~:; Q1l. ' ;2(II~ ~q
~D 1hD I '1'-' 1" 1./. () ., <1'1 1.3 I. c[ I '31 ~1~ ' ;l.~-' Co.
:J .. A"",' /7 ~ 4> '1 i.s: d- . t t/ ., ~ 1)", ll) I Jet - ,. ~i..:' , ,f4 U (p 0
:2. J'1IJO' 111,.7 .. 1"tt;..o ,1 ~ ..;).5' '~r I...., a.1J-' ~j (,()
.J.. ,..., IJO' I -, i./ I ", ..1 ~ . tt 0 . .. <. ., 6 I ';':.1~", ~ "". 11i~ rJ.J "t ' ~C;7 r;f
I It 'jq 1 Jf' 'l ~ 7. ~ . .QO .!I. q . --' '/1" I ~'" .) 'I C ' ;l~'" Co
~I I /~ 1'1 , J' j t 1,. l'i1 . .1" ,/~-~ ~)' .,y~J {,O
,,~ ", ~ q ~tt. r; ~ /7- ..;5 .2( 1< t; 2~{' ~(..~. (Ill"
Traverse
Poinl
Number
(3)
( .1'
,
Dry Ou Meier Temp.
Inlcl UUIICl
(18.. ). F ("Ii.....) . F
"1'1 ID
7J eO
1~ '0
11 I~
7' 16r
.
If
77
71
77
l'
I'
78-
1-
7(' '.
/,
75'
.,t'
7'
-,"
.,
.' 1J
'.7(
,... '-
..,...,
-,9
,4
7))
7 p
. 7C'l
~11
. .0
}Io
J'O
yo
jq
7'i
7"
7(
'lo
,2'
Pump
Vacuum
In. III :X..AD..
r;8
5')
~
, 58
~
, 4
~ S"'r
I GY
/ {;P
Ct ~3
I )',p
I fP
"1 II
L ~,
I S"J>
/ S"J
I $'11
I >'1 &
I ~ 5"~
1
, I 5}
-------
Pla'nt Name:
Run Number:
'J"
~I(. g,.~J 5I:t.J ~/A)
-B - O-'b1l/rJq. I
Test Date:
Opera tor:
Page -#-- of 1
-~ 11-96-____- u---.-.u. ----.. _.r
s~
Traverse S...plinc / Ood: Time Oas Meter Velocity OrifICc PICS. Diffclcatial Stack Probe Impinger DIJ Oas MClcr Temp. Pump
Point Time, (24-hour Re8dins Ilcad ~ PI) (611) 100IIzO Temp. 8 F - Temp. I Filler Temp. Inlel VUIIC' Vacuum
Number (min.) dock) ("- ) ftJ 10.1110 Desired Aclual (1;) Temp.. F .F rr... )8 F (1i_I) .F In. III
I'!,) '1, I /~~5 , 'I J. 1 '1' ~() 1.1 1.1 t3'J ).. '" I 2(; ~ fJO ?~ 7'/ 7
!>,:z. I 18 3 7) """. .11,. 71 "r-' I 'Z7 ; 31 I ~ Z (I 6 1'1 7g 1
0./) ~i ," ~, 'e{ ~- 8 .lL ~t; ,J.x f~ 1 ~t{o I~hl ~I"" ,8 7(} I
\. ~ I ICi 11" tf1I c. I ,I:L :1> 1)..'5 13) ~13 I ~ 5c./ (00 ,8 7f - l
I Jt~ I OJ4t't '.tIO '-'1 I. q IJI ~}I 1;7.(,'"1 tio 78 "7R
i~ I ('~ q sac It ()- f J..5 oJ., /1 " .;l5~ I ,.~~ ~o 73 7K
4ft"lb I 'ItJr. ~ 'r' $"'0. i~~ I(erg ~.l ~.I' tgo PI7 I -lS"G, f() ,., iP I
Pnr lit {) I l'ilo q$'O.Q ~-4 -+I rd I~, 7"7 ~
(d 5 I J't 15 ~~~,1 . I ';)- .MD .J.Jn I ?or ~7 I CJ51 ~ ,., ..,...,
'0 I ,Q20 q S"~. Q .f ,0 .IA .2./ ~./ /4:J :1(,1 I .2':0 f60 1t; 11 -
~ ~c.
(0.) tt; I Ii\~ c; c.1.~ ... J 1, ".1 ,.;)1 I ~~ ,.Jf.r,. I ~<.J IL () '.- ';' .,~
.;1.0 I Jtl:Jo 4 : ~'~i. .... J1. .J.7 1;1 1.5~ :J ~, I :2/,:'" (. O:i,f~ 7, 7fJ "
jl I I'I?} c~ y. J , , 2... ,~s ,#tS /13 ,;J fli I .1l.t;' ~ 0 -,t, -'It 1
(-;) .;t~ I /1 .~t'# (~f40." ~ ,90 1..1 I '1 I'JJ ;/~i I ~5' ~o 7,~ v 77 7
, 3a I I~I(() q (I,q (1"5 ;~, 1)./ /1-1. ;l('q, I J~:L G7 7(,
77 I
1~ I J'tq If f.,t./. J... . 1.0 ,J.I ~,I 110 dllfl I d~ ~ 7~ 7, -,
(~) 1~ I / 'II/I. q~(,.l) 1 15' , 3 J 31 133 ""'1 '.2SH ~~ 7u 1/ I
~L( I lti 54 .'_f J.. ." ~~ ;J...~ ,1.0 1.3 0 It.R I ~(;b 5"5 jfJ';:. 7(, ..,
"I! I 1'15'"8 '1", _1/'1 '3 .1'1 .36 . ~O I 3)... ')..c,i I 2rao r;1 ,e; '11 I
I ' I
I I
I I
I I ,
I I
I)tl
~1
r;1
t"I
~'l
'>3
s-P
~8
S'8
5"8 .
5!
~3
SJ
S-P
53
~
-------
--..
..--
~~1'''''>1
~~f-':-.-<'"
rg PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant~-Lo~ g~}~~m ~\ Cht=.~-krIo" I"rl.'" ""~
I
Sampling Location: BO,:}nl ,CQ O~ +-
Sample Recovery Person: R \!, R. D
,
Sampling Method Type: M AI':t q
RunNumber._B-O- M~- I
Job Number. g .5(){P. 000
Date: ~ - )} ... q 8
Field Team Leader.
DS
Impinger Train ID:
RTf ~2 J.j
Comments:
Front Half Data
Filter No.: 'T e..+)o v'\ Filter Media Type:
Filter Description: 1':"'1 v&A: J.t.Y - ,/'A-J , ), () 10 ~.~
Filter No.: Filter Media Type:
~
~.,
/:/k/
Filter Description:
Back Half Data
XAD- Trap Impinger 1 Impinger 2
Contents: ¥~D "t=M e-A / Nt. H~ I ~..- (03
Final Volume: (rT11J 1 3,4.5 t) ~t1 ~ d-- ~
No ~o...P} Initial Volume: (.fI11)? ~-:3. .5 4{~ ,'Z- -12(" t,
----- '1.\.~ ~.O ?(.~
Net Volume: (J:I1I)~
Impinger 3 Impinger 4 Silica Gel
Contents: ~t.-II(tl; 41 (6 ~PIIQ\; t:,\\ r,e\
Final Volume: ~ i <"lolL> . V ')10. l~ (g):~
Initial Volume: ~? ~ S ~7.I..J (g}:--9D 5. z..
Net Volume: (JR/f1 ~ ';,1-' (g): ~
-------
Plant (--'ok Ce-l:l. 5~~/ f; PII)
Sampling Location f) t.., J J d:.
Run Number: d - 0- t1Jtf.r(-1>ate: fJ. /2 A q B
Pretest Leak Rate:. ODCq efm @ L5- in. Hg.
Pretest Leak Check: Pitot: ./'Orsat: /"
Tr- ~ Cock TIme
PoInt Time (24-hour
tUnber (mln) doc:k)
I-I 0 CJ 1/1
c,. 'L1.s
IIJ q 3,f
14 t? t./ .).,-
Ilf ;t:Jt/ 7
~ lD 1.'15"'1
(:2.) ? I J ~~ J
~ t, 1f)1'a In
141 lOll
4~ '01 Lt.
S'1 10 2~
I~ ) ~ 0 10,). "
J-ttrlc 10~'
')~ II ~~ 101.41>
"J q ;&t; ~
Jln JD,q
(LJ) lo~ 1111-{
'- IO~ I/lu.
I~. /1 ,Z
II'j II).;'
lor, 1.20 II J.I
J-top ~r" .M () iI'ID
;'t1t .2-:i "If /J~
I"'/~ i~ /J,/D
7 1;Z/~
~7 ,..z '1.=t
.i1 ''-1''
Gas Met...
Reading
(Vm) 1t3
qlfl. q.o/
"dj 1),,' - D'
q 7~.1
~ 7~. LI
q71 ;L
.,~ 3, 0
~f8t:. I
q J1I ~f)
lI;lqf). ;).
qqd. '1
Cf'l7. 3
q"". .>
tJ 0 5.. 1
()f) 4 5
OOCb.'D
o If). D
01 (;, (Q
IJ /g. I
/').)0. c;
6~~. U
o a.J,/ J S-
f) ~ ~ J -~~ J ,
o Jt./ l/'lS'
o .:JL/. 1-,
fJ;)(P.~
() J.;J,d
011/ "{
AVm- 0200 .~r1~ ~-
FIELD DA'IA SHEET
Sample Type: 1/;,11 Operator:.5'p'
Poor: .2'1.~ Ps: - , '"'1
C02: tJ 02: .;2..1
Probe LengthlType: ~ i Pitot II: .£:A
Stack Diameter: i oB" As: ~ 3.'~
~:l,O
Nozzle ID: .:l ~~ Thermocouple II: f5"~
Assumed Bws:~Filte,tll: hf71".AJ
Meter Box II: tf'J~ ~~ Y: 1.1)(')/1... t:.H@: 1,'7 '17
Post-Test Leak Rate: ., COI clm @ B- in. Hg.
Post-Test Leak Check: Pitot: v'6rsat: ~
Velocity Oriloe Preaaure DiftBrential Stack Temperature Impinger Dry Gas Meter Temp. Pump
Head (6p) (6H) In H2O Temp. 0 F Temp. Inlet Ou1Iet Vacuum
In H2O Desired Actual (Ts) Probe f'1I88r of (Tm 1n0F) (Tm out°F) fm. Hg)
:////////////////////.o:///////////////////////////~'l'////////~ ~
./s rt/O .qO /i1J- ~J~ a~O IiO 77 17 I 5"11
,f~ 1.d _1. '1 ~1 ;1uB ~'i"1 t;] 71 ., 1 h 7'3'
, I~ . ?~ .1S)i.16 ,;}"r ~//JfI !to "19 jq I 5"'
,t}c: "il.1A .1. (. rR .:Jl4R .:J.t."'" /:"5 "1,8 In) r 5'~
" 2;J- ~ . !& ~ jg , ,i] ;2l4g Jl~-'i $' S- "7ef ~ A I 51
1 t> 2 i ;1./ /q/ .J~~ .)(bY ,I;'''' 56 ~:; '7 51
/,.3 'l,,1, ~ I~~ t:l~ 7. dJ"t.". .~ ~:- " :l.. 8 / 1 5';
. ~ ./.4 .) tA ~ 'If ~ /,~ ;,z ~ S'"l/# tiP ;J /q S1
4 11.. . l~ ,45 lite; -:uti .}{;; 3 fit) f:J ))/A I '51
. PIa .l.~ 2.'1 II{~I ~v~ ~~o~, B.1 ~ 1 t., 5}
, '1 iJ- d. S" ~.b /1(4 ,2 IV ~~ 3 J;7 J'~ fq (. g
~ I / ~]o ~.li, /'11 ,,'1 " ;4 . ;111 /4&' ~ (n ~ .'Jr.") uP 3 61 ~l> I S"1
/. U pl. -r d. J ,q 1 d)r,5'" a ~,;:J... ~C) 1"5" J' .J" ~ g>
.JI .J" ,jU 10// A(P~ ~~i II" ~'" 2'~ I ~S
Irj' D /J. 1 ~ 7 /t{D ;J~" IjlfLJ~ &I c) 1'1 rJ~ ~ >f
..1/ ",$'b ..gl> It/:L 2aL/ -,q-~ liD 9~'5 S'tt
, I ~
#. I;;A..,
,1\
, I-I
.t; 0
~ 1 (
I 12-
d...,S
.3D
~.t(
,JO
. j'J, 117 lU,~
). S' lift.! ,;1 '/l'
. 5U ('1" :J (,j
;J..J;{ 1_<"" .;{". t;"
, 1 ~ 1.1 r; ~ c, ~
:J (;4 ~()
.JSj ~ 6
~S:I ~o
27/ S.:l
.2~ I <'r"
9'
to
81
to
-,~
13
K:L
$0
7<:f
110
J ~r
/. S'1
"I ,010
., sry
J S1
AH..
fi.
rrn.
-------
Page
:J
of
1
Plant Name:
Run Number:
r t>/; ~ 'R",~j, I. <;/: ~ ILl (E I A J
B - CJ - h1~:I" - }...
Test Date: -ll: I:L .ft/
Operator: ~ t!
-.-- --....-...--. -.__"._0
~'\
.. 0
'ilY
Lq.
$\0
(1<': 3.0)
Traverse 81m"';", / (]oct TIm. Gas Meier Velocity OrifICe Pres. DiUerentiaJ Stack Probe Impinger "'" Dry Ou Meter Temp. Pump
Poinl Time. (24-hour Reading lIead (-PI) (011) IrLlIJO Temp. - F Temp.' Filter Temp. Inlet UiIllcl. Vacuum
Number {min.} dock) ." } ft) 10.1120 Desired Actual ("1:) Temp.- F 8F (T.... )8 F (18_.) 8F In. III J( ft '0
1/02) 20, ' ,2. :11. < 31) J 1. ;2 ~ "'"'> / ~ 7- ,J/6/' d Iii C" /() ryq ,' tst >'I
q, I , ').if IJ ;',q ~ ); , ~t; . ~~ I~~ ;JulJ.-';}.l," ~y 741 7/ V Set
5"'0 I I '2. c:;S"" Dt..{ ;1. Lj ,'1t; A.u. ;).& J1:.J ,7((J~' ~~ r;b 79 S D ~ ~5
5".)-. 112..51 of.( 1., .-13 ~ l'i ,-';5 J~u J.~fJ I %.:t ~7 71 31 S"t(
("'2.1 III , J't.. t>( D Ot/~. 't , 'l'7 c? ~- ~.t: , j7 aftJf ';J. cJ. S"$ , iVD~ '51 ji 90 t;'i 9'i
"'f~ I J J 1'1 (')~ I ., 9~ ~.< _? c:: 1<10 ;1(, ~ I ::Ji./, ~1 7q to l'o '59
:"'iJ I ,'11' 0("1. (:l ./~ .?r; . ~c::- ,q -r.. 1.1 ~" I ~,,(J <;", 74 ao & ~
(4) ~k I 11QO I'IInO..tt ,QD :J~ ;l< tgd.- :Hlt" I ~~() ~5 '7P 74 -, S"fp
, '17 ' I?".l..- "t;/l.B 5" I ~3 X1'J5 ? ~C; J 1., ''I~' JS2 ~<; 78 7( , ~
iO( 'J ':, 5-0 0 Ill. 0 tJ1- .J.e ),( 126 ~ t{ <'", 2fD4 ~o '71 7c) .,- S"'j
/01 , J.~ CJ... 0 Ur,') " J if .. ~17 J~ 111, gil,';)~ I ~6 It eO , S"IJ
) II::;- I /'11)0 111 (pq ... L '11/ :J..t/ 2.4 f 1. t;" J U4' .1..5'5 (""<" '7Ct 71 "7 5(P
I J-1 I I r.{()1. ~ ,'~~ .11.. :35 ~ ~ 11:, ;J. "S I ,l~5 ~t.{. 13' 7'1 I st,
f).O 'It{ 0 ( 07)... d'l /..3- '\....0 , ,
, S .,...c I A_- J ~ -- ~ ' ''''1
r4
()nrlc ~ n I 14,,10 tP7 ~ 1/9 ,.1 ~ i s~ I .1<;" Iii/"'} ~ '.;1<;":3- t..t:J 7-' ..,~ 1 ~
(I) . 10 I ,4 30 "''"7t"' J I..t; .-;iI .~I( .?'~ 1 3 2,.. ~:;)7>' 252 (,J" "(~ tf I ~
15 , 1"540/0 '7/. '0 ,'10 '2.~ "2-,'/ r~2 ZS""2S'"3 ~"2. 7, 7.5 (.. E;"~
.2...s I 1 $5~ t2\ .J~ ,3~ .3~ /3.LJ :zt-.il' 2S '2 (gO 77 7' I Go
~1 I I:5S f
-------
Page
~
of
4-
Plant Name:
Run Number:
~? J ~/
(1) I.CJ ' UL~( )l!Jl I . Bt)' ;J. ,1, 1_;~ ,2.CI ~~) I dC;;-~ I.b J7 7]( I~ '"
',I I 11131 /03 'f .f> I ~5 - ~t; /,~ ;J:J..1 I ~ t,:? II L,' 1'1 1.1> I ~
-J.). .;;1... ;J- I 'tt~ ..J;.-J I ;;l/,,£ (04 -Zg II L, ~I
~/') / 11..41 If) I IJ #Id , ~.4 -ii I~~ '2J, I &J-9J fql/ 7{~ '11 I ~o
(~) iO~ / i"f II ~. 'J -Q If, :lS"" ,,2, 1.1.\ J1.114 I ;}.~s t.6 '/'1 tY fi !:1
fe1 '111t /1 7.J lid . J~ . '1' ;~I 9-H ' ~~ Gb 7q iq 1 S'1
I , ~ I ",. '?-&."\ . t..! :z..~ :1' ;'2...9 '--ICf' :J.C;g C.J!;) 11' ...~ ,~ (,0
119 I 1'11.."\ ,:l.~ hC't 1'''J '1.1. 7~ (~I ~If' :u:1 ':'0 '19 1'1 -, ~d
A,t ~ fJ I j iJJ /,;l.;;, _/~' ,II) I ~~ ?'1 IIi ::J. \f, ' cJ. L/ C" ~o 7t 10, J (,6
[I) ., I /1'/ \ ( ') -t;;. J... I, ,1.1 ~.I /; ~ ?-io I ~~ tt'Z- 1R 1?J (, ,~
tIi I 174(' (.2 ~J1 .1'-1 . 3.~ ~" , 1-;' :J,q' ~r; Fa -'1 ,"1 I
i 1.0 I 1'7 (1 1).J'r./ ~q1 ~.) ~-,' (~LP J,f4V I ;lS';l. 1,,0 ..... ~ ..,y \...( ~~o
,~to , n~ 11.1. <' - ,<,- ;1{0 ,'In ;'1j ~c~ '.7/A? dO ~ '? 72 .... &£0
:J-I ,0' J'tol , J t{. <., qO .:J.A ~." 13~ :J.I,," ~t.{1 ~n 7' 7! d) ~.a
)q fJ I "or: I 'J~ J - {('" ...{o .dh J 1.~ ~,,~ /;.. 5"11 (00 "19 ,Cf I ~2-
(.) ) ~""7 0 / /(Llt. /31.'1 ~ :1." ,it ,7L1 ~7o' :J(o~ u~ 7ft 71 &- G:~
1.." 'I'I/~ IIfO. ", . 15" ~J 1 .,ll {J(, ).rA' t!J.('2. li3 73 10, t Q')...
~ J ~1
-------
Plant Name:
Run Number:
Traverse
Poinl
Number
Sampiinc /Cock Time
Time. (24-hour
(mln.) dock)
'( }.O I "/14
'10.0 I lIfe,-
f ;1..,0 I 1'1 S8
'! t!J. 0 I /q ()7J
qJ..oll~o'8
; 011.1) I 11/li
(0;',0 I }!J, Ii
f M. (J I ItU4
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
Page 4'
:r
Test Date: -~~.if__._- --..---.--- _.__..--
Operator: 5 g
C!o/f~ ~~e-~~JI:(:~ GJlA
t -D.-/I'1 ¥cl1 - ~
Gas Melcr
Readinc
,,, ) It J
I \1. I
15')'. t.J
/ n.
15 . "I "J 11~ ;:1tJ I d/:"S S-q
.,1' ~ L/ ,;J.t! (;&{ I ;170 I .11AC: ,. /)
,j 5 ,t.( 0 .4 () /J.JO :>"11 I ~ 5:J- ~ 0
I. J J.. q ----" -.1. q I?'Y c1'7o I .25"1 ~
. I)" I I./D tL/o I'll A.1'O I ).I.L'" q,
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
I
of
L/
DI'J Ou Mclcr Temp. Pump
Inlet UUIICI Vacuum
'18.. ). F ("Ii_.) 8F' In. III
1q ? 'i f
7Y 71 ~
71 7J' I
i1 7./ ~
"1'1 7! J
'lJ~ ~11 1
7~ 7';l f
~d
~
(pO
57
co
~u
-------
II.,
r:::::Jc:JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: ~~dt... 5~/
Sampling location: 8rv~ r:;r~
Sample Recovery Person: ~ 'S([)
Sampling Method Type: ~R8 1(2~
Run Number: 13- (1)- t(z'l- ~ ?..
Job Number: $~O(,.()OO
&"1',1 - ~.4~ ~.> Date: 'l>JI,-/78
:: ktl3/ ~ t
Field Team leader: J) >J:/1c.P
Impinger Train ID: ~ t'rP ~
Comments:
/i.t/ $/~I-
-~
~~~
...... /Z.,.,. M. -Z-
Front Half Data J
~w }
Filter No.: ~;:h.'I ~-r Filter Media Type:~ 1l1At¥.L,fJr..r)
Filter Description: " f e. ( \./ \ '. ~t \ e \f ' '; \ \.. \ p
Filter No.: C Filter Media Type:
,
Filter Description: ---
Contents:
Final Volume: (ml)
/ Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
r Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Back Half Data
XAD- Trap
'xItP -). r~J, 'r
...::;s.~'-:7
~~/5
~~.2
Impinger 3
;${1It'f;./A4. (OJ
.Jt'1~. \
rotA , ).
-/,lo
CIPr/"l r
;
,
I,
Impinger 1
""r~gDt Lv.!)
l.{ 1'1. 1/
If(rJ( d-
Impinger 4
E~~~
-19i .~
S~1..g
5:c,
Impinger 2
~ II CO~ /"'-, t2'~
&r}.O
~
-5:7/
Silica Gel
5", , ~ e I
(g): 5 ~q ,L.\
(g): B I 'J I fJ
(g):~
./"
S()
-------
P~nt .Co{r,~ ~/l1" } (FP1lJ-
Sampling Location f)/,L ~ f
Run Number: !l.-O.JtfI/iJ&/-l Date: g - Jj -'II)
.
Pr....t leak Rate: ,{XJ 'I efm @ IS in. Hg.
Pre...t leak Cheek: POOt: ........-t>rsaf: .......--
Sample Type: 111 '/,J/j Operator: .sA
Pbar' "Q D Ps' - co "",,<-
.~. .-;JI .'-."".Jil
C02: 0 02: d/
Probe lengthfType: Sl;/~ Pitot #:-.5A
Stack Diameter: / 0 ~ . As: ",3 , ~ fi
yJ2-
Nozzle ID: I ;/J £" Thermocouple if: 5'13
Assumed Bws:.£- Filter #: &.f Io.-J
Mete'r Box #:AIJ;L Y: /. COJ..llH@: I. 717
Post-Test leak Rate: ~ efm @ 1L in. Hg.
Post-Test leak Check: Pitot: """"""Orsat: ~
'oar
FIELD DATA SHEET
Traverw SIImpIng Cock Time Gas Meter Velocity Orifice Pressure DifI8renliaJ Stack T emperatur. Implnger Dry Gas Meter Temp. Pump
PoInt T1me (2' ~ ~ -7'2 7 <./ J S; :l
1'1 Ii';i I '1/ £' /. 0 :J..S ~,8 1~fJ- I U;/ ",~ p <:;() ~lt 7~ ...., ~iil-
(;)Oll I
:11. j) 1/ t:; J'1. , ~l. t.w I ~ ? ! :J~ei ;) ~o i(q 7d if, } !:'G:,
'l.f itOR J~ ~ L. 2 )4. -)LJ, I. 'D 'J ~ ~. R /;JC I ~U!/ :2 b 1/ iflJ 4"1'< 7' GJ 55
- .j >" ~~2. . Ho. .3 "'/!J - ~~\1 ,~~ I -zB :lI#J ).~ jjL C.2.. "0 ~I. Dl 91
I').) 4c 11" Ilf) - . q~- ---, ::J, J ::1,/ -/J# ;1.lIelJ ~' F ~;).. /'1 g? /lJ ~S
<"'~ ,}). Jq~'" /d I ~~ ~ 1G. I'ZO ;J{ ~t:, :J/~/J.. ..~J It;} ,t ~ S'S'
~'11 ~ ~~ /41 j .'70 J. t; ,;1 < (;q :;"70 ;:}~I «;;2. 6/ 10 ID if)
/'1\ ,,~ ~ '/{: ;}O(). ~ ~/W ~ 21 7' IJ.A :z 1,8 ,;z~o 5~ t'6 el/ ~ ~
\:" ~ al/'" ::J 0/ Jl ~M /'0 J7 tJ.7 ,zc: dhfn ~b3 t;'d e, flCl 10
-,' (~: J(y.J 1ft I I ~& lfo li5' 2.;0 ~? ~5 gj. (J~ . b!
.,; ,-~- a.. olP ,0 I ~jj )..1{ ~.L..f I 2.. fA '- :J. 70 X"( ~< .1'1 fJ~ (I) ~a
f" }htJ I ::JOJ ., . 11/ I J{.. 11? ,3a ~cA A.. 5" l 5~ 83 fit 59
(Qi Inl\1.. ;).IO ;L ~ 2.1.J 2.4 I;~ .1. (, A ~wl.t CII ~~ ~J " /4:>'-
"1'j~ t-o, 1.. ~,1..C; . it! « tlJ ,.311. /'(0 :JfI/t ,;J.5~ ~~' g$ ~l.t ::l '"
lOO@l q"j ItJlJ :1./ C ~ .14 ;,& ;t.lo 1{!1 J (,~ ;26, ~ CJ ell 91 10 ~
Ih-l,C6 . ~:21 9tt
II/~ ;) "i :J..O ,10 " ;1'1 1'10 J(,'t :21,0 C"d 89 I
1111. lo~q ..l~ ~, ., ,1'1 :J.e; ,1.\ 130 'ilS' ;\u3 c~ R ~ q ~7
1.10 iOIJ(J ;J. ~ "r;o . J::L, -~~ .3~ nL ~1 ?wt./ c(:z- .,~ 11 1 5!
o ~,91/. ~ J:iifil ~
~ti ~ 1//) 1....0 <'2... .l2(,~ q ./0 ,,;t
-------
Plant Name:
Run Number:
~oA~ l?t:7.f(J2~.-
B- 0 - rr1 L-} ~1- .s
of-L
Test Date: - t8 -----.li.-!l~--- .-..-...u- -'--'-'
Operator: ~B
Page ex..
J( = 7. :>
T....... S...plllII / Cod< 11m. Gas Meier Velocity Orirlce Pres. Differential Slick Probe Impinp:r Dry Gas Meter Temp. Pump
roin' Time. (24-hour Readinc lie ad to p.) (cll) ilL 112° Temp. . F Temp.' Filler Temp. Inlet UUIIC' Vacllum
Number (lOin.) doct) ,"- } It) in. I b 0 Desired Adull ft) Temp.. F .F (18... ). F (li_l) 8p In. III .....4..n
(I)' ~AJt Ii I IItD ~U51.t ~/() uZ"7 ,).1 1'1:1 ~(p~' ;/5"'0 ~' ~f ~8' , ~I
~(,.() 1////$ () 50,./ .J& ..;;t.3 ,;t. J.. 1114 t?r6' :~tO 4 ~!;,- g, j?7 q ~e
&1B,o 'II ;1.0 ,:JlII. f..rt.. 4f'D ~;J.7 :y7 /q{' ;;r,r,' ;} hD S'c:: 15' g~ 9i
(J,) b/S- 'II J.7 ".J 'f 5 I J... , 'ts :J.~ ;J.lf1 tZB ,).(117 I df44 ~7 Jt;, 3£g /0 ~7
j.f, I J I 31' ;11{ ~ b . I (J , ;.1 ,:J-7 11'1 ;). ~r, I do b'1 5"t-J q /tIn ;70 ':l~ 5"1 -'t (0 13 ' (,.3
(}) ~ I lit:;) :i 5.1.f. .$& :J.? B ~ /'11 :J~ ''l~ ~ 15 ,~ if "'Z.
~ lJg I I "ko ~ 5'5>/ ../0 .2/ .27 /4/ ~1o I ;;z~i ~z. Bt( e£,- I 6s
75' I 1101 ').~~. q ,'1>1 :J;~ ~A I ~'1 J. 70 I J5't tP3 ~t/ ~l.t GJ W
"71 I I ~ (YJ, ).~( '/1 I UO
Po( i-J r- ... I /1 ~~ ~13,qOI ' .t+ S3'
.,uO I ~"'t~", J D I t:J ~~ .:J. it.!. t.Q , /.A .:3 3 I 3.3 JJ.q 1)(,£/ I I- ~iR {pO f1J iff} } ~o
¥ 1~l!c . :J() I /,J..l{ C JJ f.#- A.. ,'2..- ::J. 5". ;J.~ j(t~ :J~C' I J-t;O ho $0 ego '7 ~t>
/J6t. /.f.e:> I I J.I/.~ 21~,1 ID . ~7 6- 1. 7- IwV ~~'" ;tf.l3 f46 f~ fo I
"J...", ~a
(1\ I 2,() I I 'Jcl ;z.,$/ J .q~ :1, J.\ /"1 :Jell' q.~q . .~~ II 80 Cf ~o
. {<).D 'I xl, -;a'tI, II / I ,Jo ~ ,0 ,,J1)1.( 1 'J$'C; <,tJ ~( 3'~
- I ~o
).u, D '1J1~ .:d' "'. q ,q'~ ,) t( ~. ~ /tf, .) 1-1 , A.t;J- ~'1./' fa z .., (,2,
d ~.o I 111o' t ' 61
-------
of --=I-
Test Date: -~ \ ~- .:LL_._- .-.--.-u-- -.--..-.
Operator: 2.B
Page 3
Plant Name:
Run Number:
~-~.-
-B-o- ~-3
Traverse S.mpli"l / Ooct T1me Gas Meier Velocity OrifICe Pres. Difrereolial StIck Probe Impinger Dry Gu Meter Temp. Pump
Point' Time, (24-hour Reading lIead ~r.) (cll) In. 1120 Temp. 8 F Temp.' Filler Temp. Imel UUIICI. Vacuum
Number tmln.) dock) . .. ,t"-) ItJ in. 1120 Desired Ac:Iual (1:) Temp.- F -F ("r.hi! )8 F (li....) 8F In. III )(A-St-
~ UuJ ~ lit; I 14 J.3 "" A'" .-- /() ..1.1 ..~1 i~~ JSI / :ZS8 ~1 60 6'0 It.o
~~ . «-l
~ ~ tt-&1) q~ I 15' II ~oq '9 -q~ J.I ;).l J/Y dSj '..2 5"1 115 30 f? q (,0
PJ~ / I 5,"1. :> \ '2~' ,rf) "JY . JJ IJDj I ?L((.. / J.5"LJ lAc) -30 ~L/ , ~o
ID~ I Ie; ~ t> .\\4. \ .4'~ -j-~ J.- (Z:z. ~~l.o / ;z.~~ ~ r( 12-. to; ~"Z..
lot. I ,c,~ '3\(,~q . II .. 1 \ .1. liJ..1 I (~rc.l / ~ t;'l Sc.s, ~..2 ,4 t "t~
, I ~ I 1531 '~I"." ,q'L J~ ').~ 11.. \ .9'-f" /,;,1 ~ S' s-~ cfI..( i-z... tn (,3
ILl) I 1("~"'2 ;J..o. 09 A ,,, ti~ .. ~., (~-; ;).5)..' d-~4 -~ <1:../ '8t.l , ~<.
PtIf-t ~ I IC;~ ~~ ,(;X I .
I> C> I 15'..,~ ~-~).. 10 I ,30 ~o (~q ;:)10 I a l.t./ ''0 -I~ ,'~ ' ~t>
'1- I .to ",-u 3;;&. c:L Jf'j :>.1 d-') ;c..IO ~/" 1 I ,?S5 I~ r... 13 '1"\ S''f
L. I {5~ -:;~y. (; ,lI ,?:P ,'~ 'eI" ::J{" 7 / <'0 5"7 "JO' 1( ;. ~o
I... I 11,,1'{) 3"3.b J 10 J.l .:1.1 '~a- -:JUt I ;1/01./ .rl/ I~ S tJ)p ~S
I'" I 1/.02 ~?> ;.D ~ .:L ....:u ..'~~ ;41.' Idr.A ,.:)~, .'i i:; 91 11r.1 --., 57
~. I 111110 J~tt 1 .t '~ :JC; ~.~ I 'It a-flQ I~ '> ID ~J ~~. 8" q 58'
:Jli I liI(£.. :S3, 9 ~(?- 1..2. .~;;t IIIIA ~p, ./,1)., 1 110 ~; g it.. I ii~
(J.) J/JrV I ll.Dl'1 .~ ~q. '- I "l S' J.< ;JS JLI '\ l"At' I tP-lD fo6 "4 ~3 /f).,: «0
'" 'Z."l I l(P~1 ~4 'i. ~ It (!)"1 . '~.2.. ~2... IV" 1.;1(,$' ..,I.-~~ &,() " . 1/ . J " .~o.
ai6 , ,,, ~II ;" c; ~ 1.0 )< ~.< I~ :11.1 I ill..8 c;t:J A3 f?3 ~' ~~,
~o I I(O~~ 1,{jq 1# .(2. ~ 1.\ -;~ /7..Q :~t4 I ~~? ~~ 11/ 84 I ~8 "-
\
t;R I (t.9 LI(" -~....a ,~h J~ ~.L/ (1.i.. 1tn /::Jc.?. (sf) "j.L 't~ ( .. 140
(~) QO I l<1rJ ~ 1. Cc t'\ ./1 :J~ .~g / 1l.J l!.9t I "J. ,,1/ ~ 9.1 3""2.. I t)7
'- 7S'" I ''101.. .~~~ ~ ,Q1 J.5 J5 "It ii'" /,.set r;y 1,. ~3 ~ ~
,.., I r7rY: 55f1. " 'l,O ..1' 1~1. 110' :JII'" ftf) -I ).... r."i
9£ / /7/1. 1&f.:L 1.0 ':} 1 2.1 (71/ ~t.A / ;;J(,S 1,11 "1 e;)., ,,'tJ . t,{):
T
1
),
-------
Page
'I
of
'I
Plant Name:
Run Number:
-.GAe 'l?e/l! ,)he / ~PA)
& - D - /VI i./ ~ 9 - ~5
Test Date: _-8- /3::!lL_._- --..-...--. -'--'-'
Opera tor:
.sg
Traverse Sompli,. / Oadt. TIm< Gas Meier Velocity Oonee Pres. Differential Stacie Probe Impinger Dry Ou Meter Temp. Pump
Point Time, (24-hour Readin, lIead (-p.> (cll) IlL 1120 Temp. . F Temp.' Filler Temp. Inlel VUIICI Vacllum
Number Imin.) dod::) 1'1. } It J IlL IIzO Desired Aclull (1;) Temp.. P .p (18100 ). F (Ii...,).p In. III
(?ho.J1.: 17 I )7/)" ? ~t(. S t II . SO # ~o fs~ .)(01' ~ fAt!; 1'3 Jt.( sQj ~
(4) "5"' I I -r.11 1 ~l...f ,10/ c2.f :J.7 /37 ;JfrI I )(~ I lRo }I'"( g -~ /0 '
9, I 17 J- C; <70A'~ ./3 ,3'5 135 ND :U,1 I.J(.,)" 51 <13 g .~ , S
/rft I 171,7 ~7) 7 /.D ~7 ;).1 i3~ ~ & fJ ' ,7(,,7, >'1 23 ~~ II
III I /111 ~7S. 0 ,/0 . :)., / /r /3'}J )(/j I J-5{' 5{ g-;L :Y< I S')
//9 I 17'1« 17&.71/ ,Q7 J.G? ;J.e., (3~ ..2 ~ ~ I ;1v/') 55 ~3 C-;- /1) ~
I;}..D I / ('I'? '
, ,
I I
I I
I I
I I
, ,
I ,
, I
I I
I ,
, I
I I
I ,
I ,
I I
, ,
, ,
o
o
-,
5"8
"8
-------
---
II." liIi)
c:JCJCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: G.--~ ~~ iA. ~ el~ -:f".j!
Sampling Location: ~:~ ~.J,(J-
Sample Recovery Person: ~I ~.
Sampling Method Type: c..A:RJs If "Vt
Run Number:_"B - ~ - '( 2Jf - ~
. Job Number: S~{}/;;.. $().()
Field Team Leader:
Date:
])SdJ:tJ!
Impinger Train ID:
1<71' 2~
Comments:
Front Half Data
Filter No.:
B -~- rZ?- :3
-r:~tol4. ~
Filter Description:
Filter No.:
Filter Description:
vtry
Filter Media Type: ~
"5 ,'H a. II 0--...,.,......1'). A.f ",{'
Filter Media Type:
~
fA'-.l ;~~ (~I-(
Back Half Data
XAD-Trap
XIIi}-)
'"357.'1
c1it~
Imp,inger 3
tJ 1\ HCD;! Nr;..~J1J
Final Volume: (ml) 7~' .-
Initial Volume: (ml) "1 61. . \.
Net Volume: (ml) -. ~
Total Moisture Collected (ml): --.J ~ <{
Description of Impinger catch:Ll..,p 0..- r
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
f)J~
Impinger 1
;;~tl +{
~
4'7 (Q. (Q
Y::2 :3
Impinger 4
~
~31. cJ
'l':JO ,~
t{~
/'
Impinger 2
.1JJCAIJCO~/ 16.2 C~
~ (;3: C.
(;I..~ .2
- :;:-(1')
Silica Gel
5:i GQ/
(g): e;' 51:. ~
:::: ~~~.b-\$
v/ SB
-------
FIELD DATA SHEET
Plant: ~ ~-\\""l e\.-e:;v~ S\;-~e \
Sampling location B~~~"~ C>v\\e:t-
Run Number: B-D-.tIJ9--fB ate: ~(t"19~
Pretest leak Rate: . co5 cfm @ J2 in. Hg.
Pretest leak Check: Pitot"J-.J/;1 O~: -
Sample Type: Jo' J 4c Operator: -b b "'-
Poor: ~~. 70 Ps: c>
C02: 0 02: ~ 0 . l)
Probe lengthlTyp~: 5; /j :lyPitot II: ~
Slack Diameter: ~ 1\ As: Iv 1"\
Nozzle 10: . ~ t'5 Thermocouple #: S s-r
Assumed Bws: ~ Filter #: ()nnlJ'jlll ioen?J
Meter Box #:/YJRr "i Y: .
-------
---
.s- ..
c::JC1c:J
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: Co k E I'll lSet/?!e1t e/J? S ~e I
Sampling Location: 150') h"u~p C:>U fret
Sample Recovery Person: f(t J;1 j
Sampling Method Type: # 9'~ l' '
Run Number: g- cJ- if:2 ~- F /?
Job Number: 5 Sl}"p, 6Z>
Field Team Leader:
Date:
~;t,~/9 B
D5
Impinger Train ID:~-~
~.~~
Aif/ :k:.-k--
Comments:
Filter NO.:J fl
Filter Description:
Filte:- No.:
Filter Description:
Front Half Data
Filter Media Type: rer/(J/) /Yltf +-
~~
Filter Media Type:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description .of Impinger catch:
Back Half Data
XAD- Trap
KI1,)'2
~
~
G.lt
ImPin~3
#tt~ ~~c~S"
72'6/ If
.2:itLD-
-lL..i-
-Q.J
Imping~r 1
~
'-(71 ~
t/?? 7
-n . ~
Impinger 4
'tl~
~;?9. <6
-0.5-
t/
Imp}2..ger 2
tJ,;/r°IA"'k ~
&,Iu ,0
~ ~ 1, ':)
- o. a.
Silica Gel
5;/ Ge /
(g): B~J#£?
(g):51 j, y
, . }
(g): - 0..,
,0
-------
r
II
"lii
.~
~..-::::::
'iI
U TS II
77
:r: ,I:> "
()
TRAVERSE POINT LOCATION FOR CIRCULAR
Plant:
Oat.:
'7~
rr
Insid. of Far Wall to Outside of Nipple:
Inside of N.ar Wall to Outside of Nipple (Nipple L.angtn): L/7~
StackI.D.: /71/1
Distance Downstr.am 1rom Flow Disturoance (Distance 6):
/ Jz 0 inche., Stack 1.0. = ~ '-I ~ dd
Distance ucstr.am from Flow Disturbance cDlstanc. A':
/7(. Lj inch.., Sta~ 1.0. = ?: 91 dd
Calcuiated By: /) 4J 5d1C //il
~-
--
II
,,10
t
SchematIC of
Traverse Point
Nipple
Length
(incnes)
Proauet of
Columns 2 & 3
(To nearest 1/8j
, ~ I
V1
FraCtIon
of
Length
Traverse
Point
Number
Lengm
(inches)
-------
DuCt Diameters ucstream From Flow Disturcance * (Distance A)
0.5 1,0 .1.5' 2.0 2.5
I~[ I I
~~ -
Q)
tn
...
Q)
>
cu
~ ~o-
Flow
.
A I
f
, --
'0
24
...
~ 20' ~ I 20
~ 16 I 16
~ - -V-;I~Clty(NO;-panlcUla~' -~ - .!..2_1
E 10-
'2
~
-
B~I
12
8
-1
0' I I I I I
2 3 4 5 6 7 8 9 10
Duct Diameters Downstream From Flow Disturbance* (Distance 8)
. ~"'''' Pl:tlnt of M'f Type of Ol8luro8ftC8 ,Send. =8118I0I'l. Comrac:aan. 811:1
I
:J/1lUrD8M88
Traverse "
Point Numcer of Traverse Points on a Diameter
Number
on a
Diameter 4 6 a 10 12
1 0.067 0.044 0.032 0.026 0.021
2 0.250 0.146 0.105 0.082 0.067
3 0.750 0.296 0.194 0.146 0.118
4 0.933 0.704 0.323 0.226 0.117
5 0.854 0.671 0.342 0.250
6 0.956 0.806 0.1558 0.356
7 0.895 0.774 0.644
8 0.968 0.854 0. 750
9 0.918 0.823
10 0.974 0.-
11 0.833
12 0.878
LOCATION OF TRAVERSE FOINTS IN CIRCULAR DUCTS
-------
......
..--
-
-8
Project No.
Page
of
Client
Location
PACIFIC ENVIRONMENTAL SERVICES, INC.
Prepared By
Date
Checked By
Date
Sheet Title
8" II
~~
, ;
(~J ~tM1'} /~
-- .
II
d1-
"' --- ---.- "
. r1 '1/1
., -- . ...----_.
6)2-C~~
"B'31-
~~)J1
I
.::: ~ Jif.k. j)1p'.
"L ,~,N
~
-------
Pacific Environmental Services, Inc.
Dry Molecular Weight Cetermination
Client/Project: ~~~ Orsat No. ()-I
DateITime: Operator: S M£://ffl
Sample Type: O~fA~ Comments: 9/1rL
Ambient Temp. 'F t30 Site Location: t//1/H..Ln/'.£
Run No.IS) Run 1 Run 2 Run 3 Average
Net Multiplier
Volume
5-L[- Actual Net Actual Net AdUal Net %
'2/- /
O2" /~3
CO. 0.28
N2' 0.28
Md=
Run No.IS) Run 1 Run 2 Run 3 Average Molecular Weight
Net Multiplier 01
Net Actual Net Actual Volume Stack Gas. Md
J)-.f4-~.1'" ""L Net % (lblMoiel
5.5 0.44
O2" ,b rSS 0.3'.
CO. 0.28
N2' 0.28
~5/%f Md=
Run No.ls) Run 1 Run 2 Run 3 Average Molecular Weight
Net MUltiplier 01
Net Actual Net Actual Volume Slack Gas. Md
Net % lib/Mole I
0.44
Oz" 0.32
CO. 0.28
Nz' 0.28
Md-
" Oz Net Volume IS O2 adual reading mlllus COz actual reeding.
8 CO Net Volume IS CO actual reading minus Oz actual re8dmg.
. Nz Net Volume IS 100 minus CO actual reacIIng.
~ge
-------
---
CJ c:J CJ :::::::
c::::1 c::= c:::::;
CJ
Plant: f!{l/+ C614
Date: ~"I 3- 48
Location: v;,4l.r-A",.£ f'J AM
Run #:.J6 - U - ""5:5W- l
Stack 1.0.: 177';
Pbar: 2C,i 8"
Sample Tube #: B-1; - I"t tS'$,O(, -I 7J-1 If- ,~ c..
Operators:---I...1t'- I /1
Leak Check: Pre: -../ Post: ..y
METHOD 18 FIELD DATA SHEET
Bttfh&k", 5/-1 Tested Analyte:
Orifice Tank #:
Pump/Rotameter #:
pt: Pretest (mm Hg):
Post-Test (mm Hg):
Tt: Pretest ~F):
Post-Test ~F):
Time: Start: - Finish: - Total:
W 18:~ D/8:-=:::... 02:....1.2- C92: 5""
4
;) (71 ~ 1
Time Gauge Flow
Vacuum Setting
(Hq)
-
L.----
---
-
-
----- 1---
-.
if
I?
~sJ-
(:)
(015
., '" V&I'" \~
~'I ~ Stack
nt Tlmp.
Numblr n. H.,o of
r-, 0.0 ~ ~"
I'; /16 n 1 ),If 3;J
1./; SU ~ q('
~~ So fA ' l9
f: &0 {H~ I' t.'~
() j ~3 (~ t.I
) 'IT fg ~ "0
o //)( 12.'i ~ 10
~ I 2. 0 ,,)1- ~ IO~
20 125 I h,b ., e; /oj
,
/1
". ~L/ '1;: -~. ~ q ~, 'J-
liD)
'" ~
It- ;,33
111°
~ l tJ
tJ.iJ..
/L;
17.~
/jD
Ij)
PIH/
---
1/ - lo
-
----
Md .. 10.44 x %C02) ... (0.32 x %02) ... (0.28 x %Noz)
Md .. (0.44 x
) + (0.32 x
) + (0.28 x
Md =
% H20 % H20
MI" Mdx(1. -;.. 18( -,
'00 100
MI - I
)X(I.-)...18(-)
100 100
Ms-
Ts -
OF ..
OR (oF eo 460)
.1d1.. PI" Pb + S.P. = (
13.15
) +
13.15
gg P,:,,:
'iIri'l1KP =
qr -
, 0 I v, - 85.49 x Cp x .{jji x
16 :J
10'
)13 Vs - 85.49 x (
111
II~ V
1 ,-
If
in. Hg
Ts t'R)
Ps x Ms
)XV
) x (
ftIs
A. ..
112
as - lis x As x 60 s/m
a. -
X 150
x
08-
acfm
Ps " ~ 0
08 tel"" O8X17.847x - x(1. -I
. r. 100
Oaltd ..
x 17.847 x
x ( 1 . -t
100
dIcfm
'3I'r~iJ ~
1~~-
~
-------
METHOD 18 FIELD DATA SHEET
Plant: FPf1 f',.,1JJ.. I!. " d f s' j.p~ / Tested Analyte: f} AJ/
Date: ~-jll-9~ Orifice Tank #: ........
Location: it,,u,dpl' Art'- oJJ.,f.. Pump/Rotometer #: II-tq
Run #: ~ - vt - m S-S'"l> (, - a pt: Pretest (mm Hg):
Stack I.D.: (77" Post-Test (mm Hg):
Pbar: a 9. B . Tt: Pretest ~F):
Sample Tube #: A- ~-hK-.s-c~ Post-Test ~F):
Operators: $ B / Time: Start:--=-Finish:~ Total: -
Leak Check: Pre: .,/' Post: W/8:~D/8:~Q2:--LS:C02: i;'
---
o 00 ~
r:=J c::= =::::=
::1
!wli"a~ '7
Time Gauge Flow
Vacuum Setting
(Hg)
~
)
VN\ tJ A. (!.. tl o~ -~
~ E ~
nt T .
umber . H.,o F
( b tJ. ~ 3 q?,. if
15' /~ d '11 IlL
~o ~ -I (} i7 If
'H'S 7lJ f.J q '{ II~
'tnn 'Xt.f l.. 9'e; /I'
110;-- 10' q 7 i~'
/1)'5 I ~(Q 1 ~11 I
/1117 /7r (. ~~'1 II)
S ir( 1ft I q c ''7 Ii!)
o } 7'0 3tO~ q 0 10
Do C) rJt er {) /0
~n '~.AD lie; l1~. ? &ov.
~rf
o ~ 1~(lfl1
po~t
II
\) ~ i6 n9
/tt'f
It{(~
. ,fll
fo~~
C- I>''lS
/~(lJ
f ~ ! It't l)
f~~ . 1110
,y"12
~ iJ ,'life
v-q.t'15~
/.I
",,-
Md .. (0.44)( %C~) + (0.32 x %02) ... (0.28 x %Nz)
Md .. (0.44 x
) + (0.32 x
) + (0.28)(
Md ..
%HO %HO
Ms.. Md X 11 - ..2...) ... 1'8 ( ---1- )
100 100
Ms - (
»)(1'-).'8(-)
100 100
Ms -
Ts -
OF ..
OR (oF... 460)
P Pb S.P.
s- +-=1
13.8
) +
13.8
Ps ..
;J--
IKP..
<.t
in. Hg
Ts fA)
Ps)( Ms
Vs - 85.49 II Cp II .[fji X
tfJ Vs - 85.49 )( (
~
~-
7)
A. -
)x~
) x(
ItIs
ft2
01 - Vs x As x 60 11m
a. -
)(
xeo
08-
acfm
PI " ~ 0
08 td"" 08 X 17.847 x - x(1- -)
. T. 100
a..td ..
x (1.-t
100
x 17.847 It
~ 0Ittd-
dlCfm
-------
---
(J CJ D c::;::)
c=:J ~ c:::::1
(J
pf'L~
o [;J ,~('
o~J.j,
0.':1,
.,11.11
I'II.Jif
t)'f &.{ (
0'1 5" III
.,"'~
-,94.tJ It, id ~ D q~
v
"
./
-
.---
--.
Md ... (0.44 x %C02) + (0.32 x %02) + (0.28 x %~)
Md - (0.44 x
) + (0.28 x
) + (0.32 X
Md =
% H20 % H20
Ms-Mdx(l- -) .18(-)
100 100
Ms - (
)X(I--)+18(-)
100 100
Ms ...
Ts ...
OF ..
OR (oF + 4(0)
~
Ps - Pb + ~.. (
13.8
) +
13.8
Ps =
in. Hg
IKP=
~
Ts fA)
Ps xMs
Vs .. 85.49 x Cp x .[FJ x
Vs ... 85.49 x (
1
t)
Oi Vs-
S" A'...
q
) x (
)xV
ItJs
112
Os .. Vs x As x 60 S/m
0, ...
x 150
x
0, ...
actm
Ps % ~O
0, td= Osx17.1!147x - x(1- -)
S TI 100
08 std =0
1(1--)
100
I( 17.847 x
I~std-
dacfm
~ ;
-------
FIELD DATA SHEET
Plant: (.:01, E".jJ,lsL,,/(£fAJ
Sampling location IA.AJd"I'IJI'- <'k..i:...
RunNumber:'-~-m1K'-1 Date: 9-1'1-98
Pretest leak Rate: A ol> .)... cfm @ ~in. Hg.
Pretest leak Check: Pitot: ~rsa1: ~
Sample Type: II?:J~ Operator: 5,3
Poor: ;It:{. e Ps: - . fl D
C02: S' 02: /t)
Probe lengthfType:,' 3h~s Pitol #: ~
Stack Diameter: 177" As: r70. j
Nozzle ID: 1'1'1 ':J... Thermocouple II: J (~
Assumed Bws: L!/- Fiher II: 11 8 (J 7 'f;$ -/7
Meter Box #:JflA (" Y: o.£!L6H@: J. 770
Post-Test leak Rate: ~ efm @..!i in. Hg.
Post-Test leak Check: Pilot: .........t>rsat: ~
j ~f/A -
c~L
- , II'
A;> - £1- 21.-1... <..~ . - -
Tr- Samplng Cock Time Gas Meter Velocity Orifice Pressure Difterenlial Stack Temperature Impinger Dry Gas Met&r Temp. Pump
PoInt Tim8 (24-hour Reading Head (6p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
~ber (mln) dock) (Vm) II S In H2O Desired Actual (fs) Probe Filler of (fm 10°f) (fm out of) fin. Hg)
o j) 0'(.11 ~$j'~ 1{{q ~//////////////////////////' ;~/ / ////////// / / / / / / / / / / / / // / / / / ~
I II) Of31 J'/ 1. ~ , of? I. /1 I. 11 ~J:] 1;;}1 ;/(p"1 u < zo 7Cf ']
;L 10 oq~1 ?ot;. q . IJ~ I. I I. I i ~ /1J . ~ ~ D .} 0/ 7 Co ~ $1 Jfj- s
'1< llz. flU/311..l1> . I
'? J" at. ~oln /..:1.. l;l ~/AjIJ 1,;1'1 1.(,2 ~4 q/ :FlOg
J I. () //0/ ~.).:J: 7 DC. 'Ie; If'! I.;~ li If 08 ;1-' J /Oq () ~ ~ ~
. I
:L 7< II /~ jJ.A I I 6~ /, 1. -L.2=- ~Ld£- ! dfQ( - ~ _G"~ ~g r.e ..~
'J . (;1} lulw I. i - ~ J.N/,II () , (J S if I" .q/... -il4..l. l..2tP..I'. .:ltg, "1 (" 0 cr '1 ~ {g .~
Ii; Ibe: ,.:J.o/ :< S"" 0 '-:1,. ..,.,~ . f ? ~9 1.1 C : J91 1.(,J... (,1 ?t; . 'VI -....,
). .:; 1).0 I e}./~ ~C;'j..J rtP4 ,I 178 tlI7 J.(,(J Ol.,/O Sl lfc, 9~ Z
1 , -I, 'S' ,lilt> 3lAaL/
-------
.... .
c:::JCJCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:
Sampling Location:
Sample Recovery Person:
Sampling Method Type:
Run Number:J - - 3/ S- - (
Job Number: S hOtb. O~
Field Team Leader:
Impinger Train 10:
Date: q //L//9r
I
'S-
Comments:
Front Half Data
Filter No.:Jfi 1./7 ~ ~ - l ~ Filter Media Type: 1; u: t
Filter Description: -(,'/If:> J=./o.('L ~6',J f,'(v-lc...+<,
tI
Filtei No.: Filter Media Type:
r;t.c; 5
r;:: 1. e~ r-
Filter Description:
Back Half Data
Impinger Purge- --
Start Time:
~
Purge Gas:
-"
Stop Time:
Flow Rate:
Impinger 1 Impinger 2
Contents: -f;LC f/PLC
Final Volume: (ml) 7;7 ~3'r:?
Initial Volume: (ml) ~~.5 /O? S7
~'Y1~q
Net Volume: (ml) (';).7~
Impinger 4 Impinger 5
Contents:
Final Volume: (ml) ~;,)\, .--
~'
Initial Volume: (ml) -- ,:.:'1
'\-'
Net Volume: (ml) t((J;) <6 .,
Total Moisture Collected (ml): " ../
Description of Impinger catch: C /Pf'A ./
Impinger 3
E ~/ljI
'-I ~ /,
.~
' fr r
'I.c:c
Silica Gel
,5;1 6e (
(g): iS3- 0
(g): q or: 1
(g): ;) '7: ~
S~
-------
;'
--,'
FIELD DATA SHEET
~ ;;:;.. ;;9.8
- Plant: u,-fF/lA) ;J~-I;j,J. .5~~ /
Sampling Location tLAle:!,'-/}'L ,!:;j.d~i::.
Run Number:4-i{-~(JS'-~ale: fJ-/~:'98
Prelest Leak Rale: r OOS" efm @ ) '5 in. Hg.
Pretest Leak Check: Pilot: ........orsal: ----
- I
Sample Type: In% IS Operator: 2J1_-,-
Pbar: ~'?J' Ps:~-
C02: '5 02: 10
Probe Lengtti/Type: 7"g /455 Pitot II: JJL
Stack Diameter: ( '/' ( As: nD, g
Nozzle 10: , y J5' - Thermocouple II: 7 D
Assumed Bws: jjf: Filter 1I:t) $I 0199 ,. J-;J
Meter Box II:LL.L£.. V: o. /f6' ~H@: I~ i7D
Post.Test Leak Rate: ,OQ)cfm @ 1-ln. Hg.
Post-Test Leak Check: Pitot: v/'Orsat:"/
Tr..... ~lng Co<:k TIme Gas Mete' Velocity Orifice Pressure DiftllrentiaJ Stack Temperature Impinger Dry Gas Metler Temp. Pwnp
PoInt TIme (24-hour Reading Head (~p) (6H) in H2O Temp. ° F Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) ftS in H2O Desired Actual (Ta) Probe Alter of (Tm 10°f) I (Tm out°f) (In. Hg)
o 0 {'/¥J 3 ffS" o~C> j////////////////////j'i//7//'T/!///////////////////////~///'i/h:
/ IS' Il./((, 3t:t'/ fA ,0).. '~t ..1' 'it/I - t9j~ ~~('I ~S' 16" Jdi ,
).. .3 0 I, I J .!t:ti () , . I? :1.. :, ;1 " 'J," tt.:;(-I . d.5*'1 ~ c, / <;, ~ ( (>"7 £7 4> J
'-~~ 1, ~{', ;5.J~- r6"l"")ill $'I,OJ.. ~:J~ -~(.. '-IlIq ICJs-s ;)C,t" ~4 110 101 J
£tl ' - I?:1'/i,D JS'S"O ;";0'9.,[ .n-:L. ~1 ,J, ili/q IJ(,q J-f40 tril II.]. /1 I
,',c",;""..t..,7> li40 5 tL./ N. .3 ,I C»)- -L3/ ~l4it-! ,Jr,~ ..25'? (p ~ /D1 If.) f i
I-l!J1k.' ',.'~J",. 90 1(P :2b t.{ )/. Df..qhi .,.,f.71,t) ~ ><.... S"" it(/;/ I P/57 - clfD..l ~ t{ / ht./ /0' rl
. ckil. . < -.'1"- /6$' I u 1(> t/,21 .qY. 0.1 . n" .. ~ 1I.1'tJ: ;J..5'''T .l5'51 (" q J o~ /(;").. I
:~y -/;1.0 i(,"~ "t Zt/ '., 10.3 . >& I'~(" "3~ ;!..>s rJ'4 ~I 11J,,;2. '1'1 A
3,7;:,.1$'>' 17(/0 c,,,j ,iJ../1 ,oJ ,7T 1l ('<;1 ) JI)~- tfi;
LtQ~t. ..,..... . -:f,';: :1('0 17 J. <; 'If,1. r;ocr / , 01/ .~ , 7.3 I.tt/{~ dJ'51 ,((,0 {JJ 0 q ~ r-t'<;,
t "t(. .2;;.:'t~: iu r 1140 "'5'8.. 7 " 0- . 9 D .. qO I/(;p)t b ~ (7 'ktJ ~q c~<'"
.3, J~O /7~t; t/~7.,JJ5 o-r;- .qt) qO 'fSt/ ,.;}v~ ;Z51 4'Q q7 tJ~
IR()' '
~ 5- ",., h - 4
.
J
1
- -
AVm-~_. ~- ,/7t..B ~H= O.5fDg' 18= '151./
~.. -.1 CJ JJ /
~
1/:'1>
AC.Frt'
, '13 ;}
O~c. P
(, ~l.
1::=
-------
.,.,. ,
c:::Jc:::JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:
Sampling Location: r :h,
Sample Recovery person:_1
-------
Oori A
-0.\1..1
I..tAJ;
c;ht4, -
po~ ~ J1
iqt
;"t,~
-
D.} ,t,
~~:~"~.:.,;!
"~
FIELD DAIA SHEET
J:: S"t;.7\
Nozzle 10: - '19 i' Thermocouple #: ~
Assumed Bws: J4- Filter #: ~
Meter Box #:MJj S Y: O.'lJI 6H@: J, /70
Post-Test Leak Rate: ,00;). c'A t; in. Hg.
. Post-Test Leak Check: Pitot: Orsat: ~
PIont C,,~~ 1l..4.~ S1r,~Lttf:!J
Sampling Location I-.s Date: lI-J ~ -9t1'
Pretest Leak Rate: , t:1D3 clm @/ 5"" in. Hg.
Pretesl Leak Check: Pitot: _~rsal: ~
Sample Type: " oJ I~ Operator: 5 ~
Poor. a.tf. 1,5 Ps: '-,87
C02: S 02: I 5"
Probe LengthfType: ~ Pool #: ..i.k
Stack Diameter: ~ As: , 7().,'~ f~"l.
Tr8V81'88 S8mpIing Cock TIme Gas Meter Velocity Orilce Pressure DiflBrentiaJ Stack Temperature Impinger Dry Gas Meter Temp. Pump
PoInt . TIme (24-hour Reacfmg Head (6p) (11H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) clock) (Vm) ft:5 !nH20 Desired Actual (Ts) Probe Filter of (Tm In°F) (Tm out°F) ~3 ~
ID OS'y~ '-1 7f. ;t. d) t;' I.Li /.{~ "19 :J. ~g ~"y C:..., "JLl 9q ,
15 Of63 l.j f..1.l Dig r..!: /.' l.fisJ ;. ~'$ ;;t.i (.0 9S ~3 t.
(}.. iJ.O D CZ1 (~ tg(,,~ . nib I ~ r.'- ,,~~ ~c;7 =tc,1 I" 1, Cj(. i~ '
.tS O~OJ L 'hI. ~ .. 0<. ;.~ ,. ( /..lilt A'-J ~5'" (,) 99 'lJt.{ ..
';0 0 4f oK. Co. ~4 i; .01:; I f" LC. ~JLt AliO ''''"n ~tI qO ~( ~
".1 ~5 ,,'}IJ &.4'tl ~ _n<: ./ lJ I. fA ~ 33 ;(>"1 ~(",O 5'e- ~ ,;
o JiIr 0';'1 S'OI./ 4~2. ..JIiIrI! pj ~ ..»(; ;e' <;"2,. ;; SI> '5'4 ~.~ '10 i.J
~_c ~c.o - A. "r. .,tCi . ~ .o~ \.1 , ( '- ,q ~(.o il~5 '1 " f"if ere ~
~ ~~ fJ.:tS3 c;~ LJ lOll fA r",t1 L ~~ .;). f.J () ;.."5"~ 1.4' ~.(, crt 4-
J,aIIO 70 o~S'~ c: ~t/. <; .0'- :J.?- .:1.')... u .. ;Zt::l ,5'7 '" q '11 ~-
1, i l"> /') '1. c:: ~fl .(" .()~ I,~ I~ t.. ~{~ ~~g ~c:; $' co '(~ G Jt. Lf
~ <10 I(IH,g ~~:l.< .oCiJ 1.'1 ,01 ~ 17 -"'flo ~/ ey~ ~3 «1
-
CJt; lOlj 5~,,'7 . a. 1.'1 I D ~;l'1 ;1-S, J-~, 5" ~8 'Ie;" ~
~D IOI~ c;- L{.6. <; [0 . ,-.{ I (,'1 I. C, u51 )..S/f a-~r ~.fl 1t:t 1t( 1./
iD~
I ..., If, I''''
I--P" 6Vm- 'T'" . 1"T"7 ~- 22 AH- 1.1.5'2 -
./ 3.5:?
fiii-~
Ti 1.1'36
It"
p o.
-------
)( ~ - c
-o.t>\~
j... .ta,l I.
,,"i(.~
Pod:D-
-
Page ~ of
a..
Test Date:
Opera tor:
8 ~ 15 --Q8_._- u----..--. -.--..-
~g
Plant Name:
Run Number:
Travenc samPIIDlj00ct Time Gas Mctcr Velocity OriflCc Pres. DiffercDtiai Slack Probe Impinccr
Point Time, (24.hour Rudin. I lead ~ PI) Cd I) IlL 1120 Te-:,!: . F Temp. ~ Filter Temp.
Number 1m In. , dock) '" , It J ilL I b 0 Desired Aclua' ( ~ ) Temp. F . F
o 0 I IO~) ~~o't. S ,65" 1~fJ.D (dJ L15~ ;)..51.(1 ~Sq t;;1
) l.O 1 "07 S"~ .~& .2. .. 05 LCI I , ~ lIt.{n ~ >.1':.lS7 5'"8
/'Z-S' ' lIo~ 5i1fA g . o~. /{D I,lo "11,0 2"0' ~('g ;,
/30 I I \ II 5"-ro t;; , ec:; l.in Llf 4 z-i -1t. ) '~f#t:> ~
\1.5 1 114/0 If'il./ "J..'i7 ID~ u. , f. 'it} I ~ fno l;t~ IJ. t
J'It> I i1T J J ;./SO lS'f 1;15'/ E;'1
,1(') I 1/4 Y S'i to."" tOf. ,. 1. / ~ -:;j!J~ J.~,' ;2 5"'1 cLi
)1~ I 11t:1 UtJ010 ~t!>4 I~ I "t4s-'-l .:15"1I,}-SL 154
I~o 111(;-Q /"01. .2 ,Ot.( 1.1. " ~ 'IC<:;'~ I;+(p() 5'3
I" c: 1 \' ~1, In()fo A1J~ I () 4 1.3 I 1. '-1'-1 1. ~s1 1 ~(.6 S'L(
1 T ,
1 I
1 I
, ,
o
(
2
C.de. I?
jb- t{-rtJjI5-3
;t
g
~,:?
(; ~ ~ 7 B 3 ~ ( 6. 0 1 Y LtAlC ~f.2) ~ Co 5', 7 ~ 5
Dry Gas Mcler Tcmp. Pump
Inlet UuUcl Vacllum
rr... ,. F fIi-,,) 8p In. III
4f2~ ~~ J.J
t:tt( "(,1 ~
'11 'IS oIj
'17 1tJJ I.f
' g q< L"(
'1 '1t: '-'
;00 qlf '-f
/00 ~1 t
(0 I 9(" o..j
103 '(J l
L- .
,",' ..... W
I () 0 ) 00 4 y"':
t f) fL1 (0 Z- ~
161 1(.:) c..t f...
1t!1 a Jo3 ~
/0"1 lD~ ~
10'1 fOc., t.,
It>, lo~ ..J
;05 (D ~ Y
\oS (oS "
-------
---
1iI.- -
[=::Jr:=JCJ
o PACIfIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:
f/J~
Sampling Location:
Sample Recovery Person:
Sampling Method Type: /
Run Number: - LA - 0/~-,
Job Number. ~ ~~. f'/')()
Field Team Leader:
Impinger Train ID:
Date:
Comments:
Front Half Data
Filter No.: (r{l. 6 ~ (
(g): flJCb 7. 0
(g): t!~?'r
-------
...J
[:=J r::::::J C:J
o PACIAC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: ,6 e + h )£? 11 ?,,1-1 ,5/PfP f
Sampling Location: l)., '" 'Apr-Cl r ~
Sample Recovery ~on:---' ,..0 ('.,;>---
Sampling Meth-}od Type: fV1 '3 tf p
Run Number: -- tA.. - S I ~ r::-!)
Job Number: ) SlJ h Q /JD
Field Team Leader:
Date: ~! J s:f1'{
l)5
Impinger Train ID: ft./ ?-
Comments:
Front Half Data
Filter No.:.!1'f)D'ffi -? ( Filter Media Type: -r; d. J t U..JI/( J /4 ~ S Is,.{', /..-.1
Filter Description: f7 D 0 r f;cu..UfL
Filter No.: - Filter Media Type: .-
-----
-. ,
Filter Description:
_...J
Back Half Data
Impinger Purge-
Start Time: ---Flow Rate:
Stop Time:
Purge Gas:
Impinger 1 . Impinger 2 Impinger 3
Contents: I/PLC I!/;>LC ~
Final Volume: (ml) G { 5, ~ ~ ¥Sl
Initial Volume: (ml) ~ ~~,{,~. J,
Net Volume: (ml) -,~ -,1 ~
Impinger 4 Impinger 5 Silica Gel
Contents: - ~; \ G~I
(g):lJ..f>. ~ '
Final Volume: (ml) ---
Initial Volume: (ml) --- ....-- (g): ~>.) ~
Net Volume: (ml) ------- (g): I.v
-
Total Moisture Collected (ml): -;1 /
Description of Impinger catch: c- I{"~
~~
-------
FIELD DAIA SHEET
Plant ~k~L"" s+c.cJ
Sampling location ~cr~/'t..
Run Number: Jh~~'~-1 Date: 3-f4-'8
Pretest leak Rate: (!).oo" cfm @ LL- in. Hg.
Pretest. leak Check: Pitot: V" Orsat: /oJ/A-
Sample Type: -421 Operator: 1.1,.)
Pbar: 21., Ps: -".~3
C02: S- 02: I ~
Probe LengthfTvpe: ~' ?{",,{ Pitot II: ~
Stack Diameter: I,::t-. As: /1tJ . 7
Nozzle ID: O.4f.\.. Thermocouple II: {- JIr
Assumed Bws: .M:.- Filter II: "'k.f/o,J
Meter Box II: 1.111 Y: l,otJ,/l1H@: 1.781-
Post-Test Leak Rate: I oO(qcfm @ .LEin. Hg.
Post-Test Leak Check: Pitot: V' Orsat: --
#-
I< :. l!f-..( 1"1.J
Tr- ~ Qock 11me Gas Meter Velocity Oriice Presaure Ditlarential Stack Temperature Impinger Dry Gas Meter Temp. Pump
PoInt T1me (24-hour Reading Head (t,p) (t,H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (min). cIocIc) (Vm) ftS in H2O Desired AduaJ (Ta) Probe Filter of (Tm in°F) (Tm oUI°F) (in. Hg)
I~-"- v / / / / 'l"'/////////////// ff/7/h-:/'/////////////////////// ///~
~ ~- I 0 D'tl' Q4/.4 S1. 0.01- I. 'V 1."-' 4"¥1 'l.S~ z.:;1 u~ '1i 100 .S-
'2- /5 0 't 3C. q~." 0.01- l.z. (. t t{Co? '( 'f1:1 1,(,i) ~\., 10 fo I{)~ 1-
like. 3 'to. oqst t:tsr.' lH)(" \.c~ 1.0 -4>2> 14(, Z:c. f SF lo}- 103 1-
g. I 4.t loo7,/f. Y It - - - - - - - - - -
- J- v
OF
)CA(:>.
"
~7
~
0./103 ~
58 fo"
S,
"
~{"
,"c..
51
~"
~
~
v"AVm-..!1~. 703 ~-~
10"""
AH-
. ~t,
T." J-{ S3
'Frii- Ij~ /
" ':off/., ,..,
~'FLh\ 3-
/1d 10
OS'Y~c
f 1:2. 'L t
1=
~'-6
~
-------
SSM.
CJC:JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: Co Iv:. Bel A 1(; l,e j4~ E f II
Sampling Location: tA t1dp r -VI r Q.. I
Sample Recovery perso~~ f- ~
Sampling Method Type: e d (;1.1
Run Number:--.1i::....LA - L/ d 1 - I
Job Number: 5 J6b. Dof)
Field Team Leader:
Impinger Train ID:
8/l'(lfi
D~
Kt )'f
Date: .
Comments:
Front Half Data
Filter No.: AI/!
Filter Description: L ~ f"t,/.
Filter No.:
Filter Description:
Filter Media Type: Ie -r I 0 r7 ~? f
~;... ~J7" H- /.J,}J~
/
Filter Media Type:
Back Half Data
XAD-Trap
Impinger 1
f, I'
t;:. ,fY\ f?T f
~lf6>.1
t.(7.~ 0
~
;re~
5 ("
??s-:
/, (p
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
311- Y
~5b.. e,
J.O, '"
ImPin,;/ .\
#a.lfc~ ~t'1Ar
'2-Sv 7
/90l7,7
-z. ,()
~ t; Tl. 3~1o.2
rv~A'<-
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Impi~9.er 2
Jet /i~ jII t,Ctt)2
"IJ 'f
o <{If ->
-O.~
Silica Gel
(g):~
(9): <6' 'I ~~
(9): ;? 4,. 1 .
jZ
I 'j, '7Q L.
-- V
~
-------
FIELD DAIA SHEET
Pitot #: 7D
As: 170 .;
Nozzle 10: (),fJ
Sampling Location f..IIIJcrf,,-
Run Number: v- C>-1t1- 'Z.-' Date: ?.. /f~ f/
Pretest leak Rate: g. tn I cfm @ R in. Hg.
Pretest Leak Check: Pitot: ,./ Orsat: "",a-
Sample Type: q Z. 'i
Poor: 21.8 Ps:
C02: 5' 02:
,
Probe LengthfType: a-
Stack Diameter: 1"11 ..
Operator: JJ pJ
- V. K}
lC7
-
- K... Jr'$' -
Tr8V8f'18 SempIIng Coc:k Time Gas Meter Velocity Oriice Pressure Differential Stack Temperature Impinger Dry Gas Me"r Temp. Pump
PoInt Time (24-hour Reading Head (~p) (flH) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) ft S In H2O Desired Actual (T5) Probe Filter of (Tm in°F) (T m out°F) (in. Hg)
~/////////////////////ij/////////////////////////7/////~/////
, 0 \ 4A'" f"J.e11UI. I ~ 0- () 11 U~ 1.4 4S-1 2,\0 15'(" ~1- ''1 $' Il C. ~
1.-- 19 \ '\. c.i). 5"O,~ 0'0 i '.3& ).4 4-(, f 'Z.<'It.. ls') lIO 111 1).)- 3
leAl ~ ]0 \ S 1'\0 ~I.Q O.i)~ '.M 1./ 4(Ql- z.C!:.> l.s1 ~o j~1 1'/..,,1,- 8
I 45" I s~ AS)'" "'} 1.4 'Hf:1\.s14 c> .0 4- o.1"tJ 11.10 4fC4 14 <) t'l fuJ 11,,, 11,{ ~
z.. ~o 155' I :+6.'i c). c»). /.1.- t.v 4 lI( 14-"}. 1 (,0 CDo 111- 1/ J 1-
r -1:. 3 1-s 1(, t. "0 (01. 1\4- 1~ .8
,o;k I IJS I ~ '-It4 lll. J 0.63 1,3f \.1 41} HI 15(, (,,1 liD ?i tv
t IS" n.}f I)l'~ o.o? {. '- t. 'I.- 4~4- 1<\5 1..S5 (PI ti1.. rf /1
r Ic.f' /1'5"+ 14l.{ O...6r l."\.- ,. "l 4~1 1,Sc) ZSf 4( 10 fCc. 1.7
/l'd 1M ISO.+<-( - - ~ - - - ~- - - -
-I' AVm- 10/.'00 ~= 0.2572..
AH- 1.12S
'fi- &.jLj5
fiii-
-------
. 1iI-
c:::JCJc:J
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant:
~
Date: B~'/ge
" ,... "''Z- -r .
Field Team Leader: j) 5/~
Impinger Train ID:
A/~'f
Comments:
lAL.
Ac..:,j~L
rfu 1- 1Lv"",
,-Ji ..J.o klNOvfL.,.,I'
(-IJ~
Filter Description:
Filter No.:
Front Half Data
Filter Media Type: 7~ ;....T
~t' ~V~ ~r
Filter Media Type:
Filter No.: 13 -V - 'I Vi.... 7-
J..J~
Filter Description:
Back Half Data
It../uJ
XAD-Trap Impinger 1 Impinger 2
Contents: J9!-IJ-2 ~ #4II~./~"L ~
Final Volume: (ml) J >if. , '1~o. 5 ~1.1
Initial Volume: (ml) 3¥~ I.( '177, z..
Net Volume: (ml) ~ 51)3 , \ -2.0
Impinger 3 Impinger 4 Silica Gel
Contents: ~#~ / Ifi.~ Cp~ E~~ 5~
Final Volume: (ml) 7Ie,~ S~.( (g): 'tj 5"7. b
Initial Volume: (ml) 7/8,1 573.0 (g):; ~ l-
Net Volume: (ml) -tJ.J ~.I (g): 50, '-\
Total Moisture Collected (ml): 5IP6,5
Description of Impinger catch:
-------
k= 1t. r1
FIELD DA'IA SHEET
Plant: _(!.e.Hd<.h~,.. ShL/
Sampling Location U ttdc.r .Q ~
Aun Number: a-U-4tf-"f Date: 8 -/J -1$
Pretest leak Rate: o.OO'L. cfm @ ~ in. Hg.
Pretest leak Check: Pitot: /'Orsat: N/A
Sample Type: 41.1 Operator: AnJ
Pbar: l.'i. (,,5" Ps: -0.$5"
C02: f 02: IS
Probe lengthfType: 8' ~\'S r Pitot #:
Stack Diameter: 111M As: 11
-------
FIELD DAIASHEET
Planl:~f.1'o s~u./
Sampling loCadon U t\dt..t.G ~
RunNumbel: I1-U.4lf-J Date: 8 - If.qg
Pretest Leak Rate: o.Q 0"1- efm @ 1& in. Hg.
Pletes' leak Check: Pitot: ../ Orser: ~
Noule 10: rJ. ~ 15 Thermocoupte II. 71"
Assumed Bws: .!L Filler #: -re.~/o..
Meter Box 11::1 Y: 1..otJ9- l1H@: ,.7$4-
. Post-Tesl Leak Rale: 0.001, efm @ L in. Hg.
Posl-Tes' Leak Check: PiCot r/ Orsat V
Sample Type: 4'l!t Operalor: AJ~
Pbal:.H.'S Ps: -O.Sf
C02: f 02: IS
Probe LenglhfTvpe: 5' ~1..SI Pitat #:'24-
Slack Diametcr: 1 t 1" As: 1 fe"
- - 1 J.1-S - --
J.<..
T(1MtRe Somping Qoc::k TIITW Gee Mel.. Velocity Ori'ce "eNU,e Dit8a'lIntial S1ack T empe.alur. Impinge. Dry Gas Meier Temp. Pump
Point 11me (24-hour ReDding liecd (lip) 46H) in H20 Temp. of lemp. Inlet Ou1Iei Vacuum y...
-.- of (Tm ill0F) (1m oul0F) a
Number Imln) doclc~ (Vro) 113 In H2O DesiUKI Actullf (1st Probe Fills. (in. Hot
- --- .-- ~~//~//~//////h>~ / ~ ij/'l~ ~~//ij///////////////h//////~:
-
1\--1 0 091& 1 ~ O. S<11 ~ 0.06 I.f~ I. f 44,. lS~ 1.)4. (,~ f' SI, {' f.6
S ()I4J 154\.1.. 0 .D (.. \.51. (.5 41.1 lJ~ 1:j" (g'L- 101 101 , S
\0 (J14J 1< 1. ~ O.D(., I . Sl.. /.) 4H )4, 7.f~ (,0 10] 101 1 -;
1 ,5" 08.r] /t,1- ~ 0.0 ~ /.51- I.f 44..f 2.41.. lS"C, (00 ,,,(, 10" f s'
t.0 010 IlsJ4 .., 0.0 (. t..s 1- /.5 4Sl.. 140 15" (,c. lOll 1°) 7
1.5" 0'10 J . ({jS. t 0.0 c.. /.51.. I.j 4J) Z4J lSf (gQ JO' 109 ~ 5
1 to 0<101 17.(.1 0.(,)') '., ~ /., 4~Co t~I '1(,1... Coo /iJ1 I(),f 1- S
~f 011J Il SA O. () S I . I ... 1.1 a1f~ 1.1) 1.~1 ~I }lo 10'1 ? S
40 {fl,t /7- 9. I) o. OJ ) .2 <.. ,. ') 4~ 1.4/ 1fJ,O "" II' /fJ 6 :] .s
I). I 45" 011> AtJ1J IJ2. -,)if 7, It/.. J o.otf lot 1.6 445 ?fF '! SR (PJ II, 1/7 7-
s'<> ot'jJ& JIS. 'to 0.0 r H(" '.1 45"1. Z1e; l'Sf (Pj //J liD '} So
n 0 lJott IJ8" c).o4 /.0/ }.o 'HII 141 15/ (po IN. /(/ 7 5i
1. (go 0 'I,,' 1&17.0 O.o'f J. of J. 0 4~ 'IiI 1lf!J SJ Ilf I/z '1 ~
(,s 6ifJJ J 'i~.1 CiJO'{ I,o( I.' 4J7J l'fl. lS1 SJ' JI1- /J1 ::; <"'6
~ atf5~ \1\1-.' ().o~ I l." t." 4101 lq)' 2rG, So; 1/7 1/1 1 .5
J fi' 1001 1a/. I o.or ,.1. ~ If "1.~ 11' In 57 If} 111 ~ 'r
gtJ 1 "" ~ 104.4 ('). c) f 1.1 C. I." 1(0 Z (1') [I. . Sf 110 111 } J'
,.r 16)1 1.0:). , o.of ,. 1 f. /.1 41" 1(b l,1 6i 11/ IIJ~ ')- 5
c-I 1" "tAO}l "l.U. 'Uti /1.\1..0~1o O.i!J d' '}~ () .~ {, 4\f 1 ~I lit.) tie. 11)- In. !' G
,,,- , 6' '- 1r.~1 0.01 0 . '}(. 0.1'- c\\) 11"" 1"'" €o} Wj )1+ ' f
,)
100 Ia.o4l ozn.f, D.O) c.l lor 6.)1# ~I\ S HI 1$1 {,O \\~ "1 s, . (
,. ,of 11)-\"- 1.11). '\ o.()~ ~,o l.iI 41'1 ~~\ 1 S~ S~ 11.' lit ' S
"rl I~ 1~1." 0 .() 'f /.0 1.6 4Ju 110 1(,' 51 p... III !, S
IIf I~ u~., Q.. ~ '.0 '.0 d)" HI ')" I sa ('1.) ,f? (, S'
J l'l° 11,,1 211i . ~ 0'0'" I.!.. \.5' 4to l.q~ 15'1 58 h) 1\ i( ) ~:
J14 110'"' :121.1 6.~ J.jl. ,.J 4/1 HI ~:)~ f~ IH II 1 ':/ s'
AVm-
~..
AH-
Ti..
1m..
~
ftJ
F
o
tj
7
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(,
,
7
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}-
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J
Af
-------
FIELD DAIASHEET
Sample Type: 47f Operator: /f/."J
Pbar: ;'1. "$ PS: - o,ff'
C02: J 02: I )'
Probe LengthlType: r' i!"/t// Pitat II: 1ft
,/
Stack Diameter: /71 As: 1~.1
Nozzle 10: 0.415 Thermocouple II: ";fA
Assumed Bws: 11:- Filter II: 1; f./.,J
MeterBoxll:L- Y: I.oaf- 6H@: /.7"
Post-Test Leak Rate: - cfm@ -in. Hg.
Post-Test Leak Check: Pitot: ~ Orsat:-.--:::.-
Plant d dlrle-J1u., 5f-J
Sampling Location (jlf,f,; tlrf.. she./{
Run Number: JJ-U'lt'~.l Date: Y'IJ,rf
Pretest Leak Rate: cfm @ -=- in. Hg.
Pretest Leak Check: Pitat: - Orsat: -
Tr8V8n8 S8mpIing Cock 11me Gas Meter Velocity Orilce Preasure DiftBrential Stack Temperature Impinger Dry Gas Me.... Temp. Pump
PoInt 11me (24-hour Reading Head (6p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Number (mln) dock) (Vm) It:l In H2O Desired Actual (Ts) Probe I FJI.... of (Tm in°f) (Tm out°f) (in. Hg)
- - - - //////////////7ff#/~ V//// all/////////////////////// / / / /;/ //
13~ Ii /I ZZr- "} 0-. 0 " I.$?- /.iJ 4 z. S'" lfo If") ~. /2fD /to 7-
0-/ J.1S \\\%p t.w..Jt.~"'[ ,OIlL 0.0' /.5"'" l.s 4-z.\.. 1.41 l-{b (,/ JU (w ;}
140 Iltl Z <11," o.~i /.,)~ /.s ,(.1) 14£ 2,fS- ~6 /7.-l /u r
/~ I J '1. 1A! Y ./ 0-0 Go I.S"" /.S 4"~ 14/ Zf J.. {,t Il'- 11.3 :J
1..- L~ "" t5/.5" (). () f l.l ~ I.'> 41" 240 z Stf' 1M 11(, /'5 7-
La 114' . 7 (""S./ r1.I}.:5" 1.1.1. /.;1 4"4 Z 1r Z~ (g{ tz:{- ('Z fI, 1-
L(g4I 1/41 1.51.4 O.DS I. 7.. ~ t.3 44:), '24.1- 2 t,S' v-V /1.:j {lr 1-
'3 Iw' Un 1 (., I. (p <5,00- /. z V. /.3 4fo4 14'1 loG. 0 ~, IZJ 11."> 7-
n-o 101 ".4.~ o.o~ I. z '- I. J, 4(., 11lf "7", <..( IU IZO ].
n~ )2.0'> 2~ 9..1' 0.0) /.2" /.) 45' 11f(. z "0 w tn. IZt{ 7-
t~ /Z,8 1. n. 1~ 1- - - - - - - - - - -
(gf
Cd
~1
CsY(
fo.!
WI.
"'1.-
(,~
c,......
/j1'\.
AVm- I It:). 7-3/
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AH= t ~ J.. ()
Ta- a.j L1 0
irii- I I S
a..
.,' .
~~10
-------
....
r::=Jc:::JCJ
DpACIAC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: ~--!-<+M.k..... ,"\:/'11-£1')# ~L Q~r- d~~ ZJ Date:~
Sampling Location: UI.u.Ah. ~ 1J1I.ttr .
Sample Recovery Person: 12.K. / R /) Field Team Leader. J) s;~/h.f1
Sampling Method Type: ~) 9i 'I
Run Number.B- (J- tlZ,9 - ~
Job Number. S5:P~, 6()t>
Impinger Train ID:
/J-6
, J
Comments:
;, L- fv'>t- -1N~
1+,;;.);.( S~ .A- I-
3l/ g. <6
1,,1... ./
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
~.4J
Impinger 1
~~-
-~'!7";, 9
Lf9~/
~
Impinger 4
~rr
.sB '/, "7
~ ~
~.
Imping,r 2
;tI,.tI CD1,/)/~ (, O~
ft'}3. ~
~ZB. . /'
---=-.:lLy
Silica Gel
(g): ~ to. L-j
(g): ?~ ~I
.
(g): ~ ? ~
./
sg
-------
FIELD DA'IA SHEET
Plant ....B~tk k..~(J~ f!:t!,
Sampling Location~
Run Number: 8-1{ -42. 4J- ~tPate: ~ - J r;- -'18
Pretest Laak Rate: . tJtJ7- efm @ I...S.- in. Hg.
Pretest Laak Check: Pilot: - Orsat:
Sample Type: 'f ).." Operator: .5l!./ u.Al
Pbar: ,J'!. te r;- Ps: -
C02: t; 02: ( s-
Probe LengthlTvpe: 8 'Pi: 3 k~t; Pitat II: 1A-
Slack Diameter: 177" As: /7a 'I ~eZ.
Nozzle 10: () r"f7Sfhermoeouple 1I:...:2.A-
Assumed Bws: -1!1-- Filter II: 8 'Q, l{z"t - pg-74f~
Meter Box II: ~ Y: I. ~yl\H@: L 7H 1iIvrJ-u/
Post-Test Leak Rate: .AS'O.z..cfm @~. Hg.
Post-Test Leak Check: Pitot: ~ Orsat: ~
Tr8V81'18 S8mpIing Cock Time Gas Meter Velocity Oriice Pressure Dift8,ential Stack T emperatu,e Impinger Dry Gas Mete, Temp, Pump
Pm. Time (24-Mur Reading Head (6p) (6H) in H2O Temp, of Temp, Inlet Outlet Vacuum
Number (mIn) dodc) (Vm) ft:l in H2O Desi,ed Actual (Ts) Probe Falte, of (Tm in°F) (T m out°F) (in. Hg)
- 0 1211:> ~'71 41'1 ~///////////////////~ ///////////////////////77/////// /7///~
... (~ /24(,, ;l. I ~ ~ cc: Al'A- AJ ~ 111/4 ,J " :2 L/ {" 2<;'ft, 7( AI/A. 1//A- -
- \D '-~oo 271.1 ;2;Y N. A- \ ,)4/ d-t;1o 12 \ r -
- (j~ \ ?"I~ i7t::. f")'2- III '.4 "I.... J/ ,"v :JtJt; ;u::~ "1 I "" it -
t. tA It. ItI k
:-O~2 of/~
. eJOZ (4 1--15
. eJo:J . I- /5
-.I6P=
AVm-
AH=
Ta=
Tm=
-------
11.-
c:Jc:JCJ
o PACIFIC ENVIRONMENTAL SERVICES, INC
4700 Duke Drive, Suite 150
Mason, Ohio 45040
513.398.2556 FAX: 513.398.3342
Sample Train Recovery Data
Plant: MA/~ '?J:1-f! c:
Sampling Location: . f,~ ~ \ (;;1:.
Sample Recovery Person: Pf-,/ /g)
Sampling Method Type:J-prp '!Z9
Run Number: B - t/ - i/2..'1- F /.3
Job Number: 'S~. OfJO
e/iIf/98
I
Date:
, Field Team Leader: ~ 5r- ~/#
Impinger Train ID:
Comments:
Front Half Data
r-;;~4.
Filter No.: /3-1/' fZ'1 - F f) Filter Media Type:
Filter Description: i/l G> / cD CC!(i -'1 )
~
---- Filter Media Type: -
Filter No.:
--
--
Filter Description:
-----
Back Half Data
f)....Iif.U
E!mfr
if? ' ,
'f17./
().Q
Impinger 2
/'~ II ~ ,/ ;tJ.."L W1
V 7..'r
~6 9/ L
eJ.Q
XAD~Trap
,{ JIll - 2
'~~~ r
-:; '1~ ~
D.::?
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Silica Gel
Impinger 4
~~
SYOe(p
-cru
Impinger 3
p~~ jA/. LC'4
1/(
7$/.. s:.-
-(). ,_/
(1 '::2- .
C- f f? 0-.... ./
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
(g): 9'U. ~
(9): gBbij
(g): CJ. .
t;g
-------
FIELD DA".A SHEET
Sample Type: $15" Operator: ~~ / t1/JIi
,
Pbar: ,;)9./. c: Ps:
C02: S 02: 10
Probe LengthfType: B/~/Qs.s Pitot II: B.L
Stack Diameter: 17 7" As: 171)~'R ~-t:-,.
Plant
Sampling location l( 41 J~r IJ 1'.£ .. k ~ 1:
Run Number:B-'1-1Ir- ,:::"~ate: g-/r-f'N
Pretest Leak Rate: ~ aq cfm @ !.£.. in. Hg.
PreIBst Leak Check: Pilot: - Orsat: -
Nozzle 10:",. 4 ~} Thermocouple II: 1(/j
Assumed Bws: 1!:L Filter II: 0'807'1'- 2t
Meter Box II:~ Y: {).98 f1H@: /. 770
Post-Test Leak Rate: . ()O I efm @ {£in. Hg.
Post-Test Leak Check: Pitot: ~ Orsat:-==-
Tr- ~ Qoc:k 11rne Gas Meter Velocity Orilce Pressure DiftBrenlial Stack Temperature Impinger Dry Gas Meter Temp. Pump
PoInt 11rne (24-bour Reading Heed (l1p) (l1H) in H2O Temp. of Temp. Inlet Outlet Vacuum
Namber (I1IIn) c:IocIc) (Vm) ft S In H2O Desired Actual (Ts) Probe Filter of (Tm in°F) (Tm out°F) (in. Hg)
- ~ /21~ t,()7 I 254 ~/////// /////////////////// /7/////////////////////////// / /"'/~:
- It;" IZq~ ~ 0$7. I 2.t:" /f//A- III lit II/A- ,vIA- 2 <: 2.. z.~o '70 AlIA ~/A .-
- 30 I J ~() I../J/;, 9 ~b; AI/A 1 ~ ? r:; t/ 2 (PJ 76 f ( -
- LIt: 13/~ 1";:)/)9 ~I 7 /II! A- Ii J, tV z~{) 'LID 1. ?() '" Y -
,
.'
I..lA-Lra-b.
:::;;---;-:
. ~t> 101- Js
(981 0 f 15"
.
". t9t'J I Q f- t-f:,
AVm-
.fAPm
AH=
'fi- -
-------
~Saiii
c:JCJ
[J PACIFIC ENVIRONMENTAL SERVICES, IHC
Sample Train Recovery Data
Plantb erfL )l? l1~Y$1 S-IPl? I
Sampling Location: l A'" ,1.(/(£, f ~
Sample Recovery person:--.f \,0 f!,/--
Sampling Meth0tlype: /YI'? 'f p
Run Number: :lc -- t-( - S I ----=:. ~t)
Job Number: J STJ t, G IJD
4700 Duke Drive, Suite 150
Mason. Ohio 45040
513.398.2556 FAX: 513.398.3342
Field Team Leader:
Date: ~/ I s:?r'{
i)5
Impinger Train 10: .ft! ./ ::2
Comments:
Filter NO.:-O'!;(,'/f3 -? I Filter Media Type:
Filter Description: t1 D ["=h.r J-;rLA ~+-~
Filter No.: Filter Media Type:
Filter Description:
Front Half Data
~rf.J~'~Q.]yA ,lei ~t; ~.r,/'r/
..J
----.
Impinger Purge-
Start Time: -
--Flow Rate:
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Contents:
Final Volume: (ml)
Initial Volume: (ml)
Net Volume: (ml)
Total Moisture Collected (ml):
Description of Impinger catch:
Back Half Data
Stop Time:-
Purge Gas:
Impinger 1
IIPLC
~ ( 3, ~
~
-,;L
Impinger 2
, 'lIj~Lr:
~
~~,I,~'
"',7
Impinger 5
Impinger 3
~
~
~
Impinger 4
Silica Gel
~;\ {;el
(g):m. 6 '
(g): t>:; ~
(g):----LL-
-
---
-
--
-
-
-.1 /
C /C"'-r
~~
-------
TECHNICAL REPORT DATA
Please read instructions on the reverse before completing
1. REPORT NO. 2. 3. RECIPIENT'S ACCESSION NO.
EP A-454/R.99.00 1 a
4. TITLE AND SUBTITLE 5. REPORT DATE
Final Report - Emissions Testing of Combustion Stack and Pushing Operations at Coke February 1999
Battery No.2 at Bethlehem Steel Corporation's Bums Harbor Division in Chesterton, Indiana
6. PERFORMING ORGANIZATION CODE
Volume I of III
7. AUTHOR(S) 8. PERFORMING ORGANIZATION REPORT NO.
Franklin Meadows
Daniel F. Scheffel
9. PERFORMING ORGANIZATION NAME AND ADDRESS 10. PROGRAM ELEMENT NO.
Pacific Environmental Services, Inc.
Post Office Box 12077 II. CONTRACT/GRANT NO.
Research Triangle Park, North Carolina 27709-2077 68-0-98-004
12. SPONSORING AGENCY NAME AND ADDRESS 13. TYPE OF REPORT AND PERIOD COVERED
U.S. Environmental Protection Agency Final
Office of Air Quality Planning and Standards
Emissions, Monitoring and Analysis Division 14. SPONSORING AGENCY CODE
Research Triangle Park, North Carolina 27711
15. SUPPLEMENTARY NOTES
16. ABSTRACT
The United States Environmental Protection Agency (EPA) is investigating the coke making industry to characterize hazardous air pollutants (HAPs)
emitted from coke pushing operations and combustion (underfire) stacks. This test report addresses pushing emissions from a coke oven, and emissions
from the combustion (underfire) stack that serves Coke Battery No.2 at Bethlehem Steel Corporation's Bums Harbor Division in Chesterton, Indiana.
The purpose of this test program was to quantify emissions from the inlet and outlet of the baghouse controlling emissions from the coke pushing
operation and to quantify emissions from the combustion outlet stack. The data may be used by the EPA in the future to support a residual risk
assessment for coke oven facilities.
The testing was perfonned to quantify uncontrolled and controlled air emissions of filterable particulate matter (PM), methylene chloride extractable
matter (MCEM) and 19 polycyclic aromatic hydrocarbons (P AHs) including acenaphthene, acenaphthylene, anthracene, benzo(a)anthracene,
benzo(a)pyrene, benzo(b)fluoranthene, benzo(e)pyrene, benzo(k)fluoranthene, benzo(ghi)perylene, chrysene, dibenzo(a,h)anthracene, fluoranthene.
fluorene, indeno(I,2,3-cd)pyrene, 2-methylnapthalene, napthalene, perylene, phenanthrene, and pyrene. In addition, following the PM and MCEM
analyses, the samples were analyzed to screen for the presence of 17 trace metals. Baghouse dust samples were also collected and analyzed for 16 trace
metals. Simultaneous testing was perfonned at the inlet and outlet of the baghouse controlling emissions from the coke pushing operation. Sampling
was also perfonned on the combustion outlet stack. In addition to pollutant testing, oxygen (OJ and carbon dioxide (COJ were measured at each
location. During the sampling program, Research Triangle Institute (RTI), another EPA contractor, monitored and recorded process and emission
control system operating parameters.
This volume (Volume I) is comprised of221 pages and consists of the report text, and Appendices: A (Process Data) and B (Raw field Data).
]7. KEY WORDS AND DOCUMENT ANAL YS]S
a. DESCRIPTIONS b.lDENTIFIERS/OPEN ENDED TERMS c. COASTI Field/Group
Baghouse
Coke Ovens
Emission Measurements
Hazardous Air Pollutants
Metals
Methylene Chloride Extractable
Matter
Particulate Matter
Polycyclic Aromatic Hydrocarbons
18. DISTRIBUTION STATEMENT ]9. SECURITY CLASS (I'his Report) 21. NO. OF PAGES
Unclassified 960
Unlimited 20. SECURITY CLASS (I'his page)
22. PRICE
Unclassified
EPA Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
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United States
Environmental Protection
Agency
Office of Air Quality
Planning art"! Standards
Research Triangle Park, NC 27711
EPA-454/R-99-001a
February 1999
AIR
SEPA
Final Report - Volume I of
Emissions Testing of Combustion
Stack and Pushing Operations at
Coke Battery No. 2 at Bethlehem
Steel Corporation's Burns Harbor
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FINAL REPORT
EMISSIONS TESTING OF COMBUSTION STACK AND
PUSHING OPERATIONS AT COKE BATTERY NO.2 AT
BETHLEHEM STEEL CORPORATION'S
BURNS HARBOR DIVISION
IN CHESTERTON, INDIANA
Volume I
Report Body and Appendices A and B
EP A Contract No. 68-D-98-004
Work Assignment No. 2-01
Prepared for:
John C. Bosch Jr. (MD-19)
Work Assignment Manager
SCGA, EMC, EMAD, OAQPS
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
February 1999
p:\sS 11.000\finallpt wpd
Submitted by:
PACIFIC ENVIRONMENTAL SERVICES, INC.
5001 S. Miami Blvd., Suite 300
Post Office Box 12077
Research Triangle Park, NC 27709-2077
(919) 941-0333 FAX (919) 941-0234
Pr("l""''':-~'' "f
EP/\ ~ c-" -,
RTP r",....." ,
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DISCLAIMER
This document was prepared by Pacific Environmental Services, Inc. (PES) under EP A
Contract No. 68D98004, Work Assignment No. 2-01. This document has been reviewed
following PES' internal quality assurance procedures and has been approved for distribution.
The contents of this document do not necessarily reflect the views and policies of the U.S. EPA.
Mention of trade names does not constitute endorsement by the EPA or PES.
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1.0
2.0
3.0
4.0
5.0
TABLE OF CONTENTS
~
INTRODUCTION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . ., 1-1
SUMMARY OF RESULTS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-1
2.1
2.2
2.3
EMISSIONS TEST LOG. . . . . . . . . .. . .. .. .. . . . . . . . . . . .. .. . . . .. . . .. . 2-1
FILTERABLE PARTICULATE MATTER, METHYLENE CHLORIDE
EXTRACTABLE MATTER (MCEM), AND METALS .................2-1
POLYCYCLIC AROMATIC HYDROCARBONS (pAHs) . . . . . . . . . . . . . . 2-22
PROCESS AND CONTROL EQUIPMENT OPERATION. . . . . . . . . . . . . . . . . . . . . 3-1
3.1
3.2
3.3
INTRODUCTION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
PROCESS DESCRIPTION. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 3-1
PROCESS AND CONTROL DEVICE MONITORING. . . . . . . . . . . . . . . . . 3-4
SAMPLING LOCATIONS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-1
4.1
COKE OVEN BATTERY NO.2. . . . . . . . . . . . . . .. . . . . . . . . . . . . . .. . . .. 4-1
SAMPLING AND ANALYTICAL PROCEDURES. . . . . . . . . . . . . . . . . . . . . . . . . . 5-1
5.1
5.2
5.3
5.4
5.5
5.6
LOCATION OF MEASUREMENT SITES AND
SAMPLENELOCITYTRAVERSEPOINTS .........................5-1
DETERMINATION OF STACK GAS VOLUMETRIC FLOW RATE. . . . . 5-3
DETERMINATION OF STACK GAS EMISSION RATE CORRECTION
FACTORS, DRY MOLECULAR WEIGHT, AND EXCESS AIR ........, 5-3
DETERMINATION OF STACK GAS MOISTURE CONTENT. . . . . . . . . . 5-3
DETERMINATION OF PARTICULATE MATTERIMETHYLENE
CHLORIDEEXTRACTABLEMATTER/METALS....................5-3
POLYCYCLIC AROMATIC HYDROCARBONS .....................5-4
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TABLE OF CONTENTS (Concluded)
6.0
.
QUALITY ASSURANCE/QUALITY CONTROL PROCEDURES
AND RESULTS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-1
6.1
6.2
6.3
APPENDIX A
APPENDIX B
APPENDIX C
APPENDIX D
APPENDIX E
APPENDIX F
APPENDIX G
CALIBRATION OF APPARATUS.. .. .. .. ... .. . . . . . . . . .. . .. . ... .. . 6-1
ON-SITE MEASUREMENTS. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-5
LABORATORY ANALYSES.. . .. . .. ... .. .. . .. .. . . . . . . . . . .. . .. .. . 6-9
PROCESS DATA
RAW FIELD DATA
ANAL YTICAL DATA
CALCULATIONS
QAlQC DATA
P ARTICIP ANTS
SAMPLING AND ANALYTICAL PROCEDURES
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Table 2.1
Table 2.2
Table 2.3
Table 2.4
Table 2.5
Table 2.6
Table 2.7
Table 2.8
Table 2.9
Table 2.1 0
Table 2.11
Table 2.12
Table 2.13
Table 2.14
Table 2.15
Table 2.16
Table 2.17
LIST OF TABLES
~
Emissions Test Log, Bethlehem Steel Corporation, Chesterton,
Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-2
Particulate Matter/MCEM/Metals Emissions Sampling and Flue Gas
Parameters - Baghouse Inlet, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . 2-4
Filterable Particulate Matter Concentrations and Emission Rates -
Baghouse Inlet, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . 2-5
Methylene Chloride Extractable Matter Concentrations and Emission
Rates - Baghouse Inlet, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . 2-6
Multiple Metals Concentrations and Emission Rates Baghouse Inlet,
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-7
Particulate Matter/MCEM/Metals Emission Sampling and Flue Gas
Parameters - Baghouse Outlet, Bethlehem Steel, Chesterton, Indiana. . . . . . 2-12
Filterable Particulate Matter Concentrations and Emission Rates -
Baghouse Outlet, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . 2-13
Methylene Chloride Extractable Matter Concentrations and Emission
Rates - Baghouse Outlet, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . 2-14
Multiple Metals Concentrations and Emission Rates - Baghouse Outlet,
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-15
Baghouse Dust Multiple Metals Concentrations, Bethlehem Steel,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-18
Filterable Particulate Matter and Methylene Chloride Extractable
Matter Removal Efficiencies, Coke Oven Battery No.2 Baghouse,
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-20
Particulate Matter/MCEM/Metals Emissions Sampling and Flue Gas
Parameters - Underfire Stack, Bethlehem Steel, Chesterton, Indiana. . . . . . . 2-21
Filterable Particulate Matter Concentrations and Emission Rates -
Underfire Stack, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . 2-23
Methylene Chloride Extractable Matter Concentrations and Emission
Rates - Underfire Stack, Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . 2-24
Multiple Metals Concentrations and Emission Rates - Underfire Stack
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-25
P AH Emissions Sampling and Flue Gas Parameters - Baghouse Inlet
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-29
P AH Concentrations and Emission Rates, Baghouse Inlet,
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-30
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Table 2.18
Table 2.19
Table 2.20
Table 2.21
Table 3.1
Table 3.2A
Table 3.2B
Table 3.2C
Table 4.1
Table 4.2
Table 4.3
Table 4.4
Table 5.1
Table 6.1
Table 6.2
Table 6.3
Table 6.4
Table 6.5
Table 6.6
Table 6.7
Table 6.8
Table 6.9
Table 6.10
LIST OF TABLES (Concluded)
~
P AH Emissions Sampling and Flue Gas Parameters - Baghouse Outlet
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-34
P AH Concentrations and Emission Rates, Baghouse Outlet,
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-35
P AH Emissions Sampling and Flue Gas Parameters - Underfire Stack
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-38
P AH Concentrations and Emission Rates UnderfIre Stack
Bethlehem Steel, Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 2-40
Summary of Pushing Process and Control Device Parameters. . . . . . . . . . . . . 3-4
Combustion Stack Parameters Test Run No.1, 8/14/98 . . . . . . . . . . . . . . . . . . 3-6
Combustion Stack Parameters: Test Run No.2, 8/14/98 . . . . . . . . . . . . . . . . . . 3-7
Combustion Stack Parameters: Test Run No.3, 8/15/98 . . . . . . . . . . . . . . . . . . 3-8
Summary of Sampling and Analytical Methods, Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Summary of Sampling Locations, Test Parameters, Sampling Methods, and
Number and Duration of Tests, Bethlehem Steel Corp., Chesterton, Indiana. . 4-3
P AH In-Stack Detection Limits. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Estimated Metals In-Stack Detection Limits. . . . . . . . . . . . . . . . . . . . . . . . . . . 4-9
Summary of Sampling Locations, Test Parameters, Sampling Methods,
and Number and Duration of Tests, Bethlehem Steel Corporation,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 5-2
Summary of Temperature Sensor Calibration Data. . . . . . . . . . . . . . . . . . . . . . 6-2
Summary of Pitot Tube Dimensional Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-4
Summary of Dry Gas Meter and Orifice Calibration Data. . . . . . . . . . . . . . . . 6-6
Summaryof EP A Method 315 and CARB Method 429 Field Sampling
QAlQC Data. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-8
Summary of EP A Method 315 Analytical QC Data Lab Blank Analysis. . . . 6-10
Summary of EP A Method 315 Analytical QC Data Field Blank Analysis. .. 6-11
Summaryof EP A Method 29 Analytical QC Data Lab Control Sample
(LCS) Recovery and Duplicate Analysis. . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-13
Summary of CARB Method 429 Analytical QC Data Field Blank
Results. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-14
Summary of CARB Method 429 Analytical QC Data Lab Control
Sample (LCS) . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 6-15
Summary of CARB Method 429 Analytical QC Data Surrogate
Standard Recoveries. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-17
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Figure 1.1
Figure 3.1
Figure 4.1
Figure 4.2
Figure 4.3
Figure 4.4
Figure 4.5
Figure 4.6
Figure 5.1
Figure 5.2
Figure 5.3
Figure 5.4
LIST OF FIGURES
Page
Key Personnel and Responsibility for Testing at Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 1-2
Schematic Of Pushing Emission Control For Battery No.2. . . . . . . . . . . . . .. 3-2
Baghouse Inlet Sample Location, Bethlehem Steel Corp., Chesterton,
Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-2
Baghouse Inlet Traverse Point Locations, Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 4-3
Baghouse Outlet Sample Location, Bethlehem Steel Corp., Chesterton,
Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-4
Baghouse Outlet Traverse Point Locations, Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 4-5
Combustion (Underfire) Sampling Location, Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .. 4-7
Method 1 Calculation Sheet, Combustion Stack, Bethlehem Steel Corp.,
Chesterton, Indiana. . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 4-8
Sampling Train Schematic for EP A Method 315 """"""""""'" 5-5
Sampling Train Schematic for CARB Method 429 . . . . . . . . . . . . . . . . . . . . .. 5-7
CARB Method 429 Sample Recovery Schematic. . . . . . . . . . . . . . . . . . . . . .. 5-8
CARB Method 429 Analytical Schematic. . . . . . . . . . . . . . . . . . . . . . . . . . . .. 5-9
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1.0 INTRODUCTION
The United States Environmental Protection Agency (EP A) is investigating the coke
, making industry to characterize hazardous air pollutants (HAPs) emitted from coke oven pushing
operations and combustion (underfire) stacks. This test report addresses pushing emissions from
a coke oven and emissions from the combustion (underfire) stack that serves coke Battery No.2
at Bethlehem Steel Corporation's Burns Harbor Division in Chesterton, Indiana.
The purpose of this test program was to quantify emissions from the inlet and outlet of
the baghouse that controls pushing emissions and to quantify emissions from the combustion
stack outlet. The data may be used by EP A in the future to support a residual risk assessment for
coke oven facilities.
The testing was perfonned to quantify uncontrolled and controlled air emissions of
filterable particulate matter (PM), methylene chloride extractable matter (MCEM) and 19
. polycyclic aromatic hydrocarbons (PAHs) [acenaphthene, acenapthylene, anthracene,
benzo( a )anthracene, benzo( a )pyrene, benzo(b )fluoranthene, benzo( e )pyrene,
benzo(k)fluoranthene, benzo(ghi)perylene, chrysene, dibenzo(a,h)anthracene, fluoranthene,
fluorene, indeno(1 ,2,3-cd)pyrene, 2-methylnapthalene, napthalene, perylene, phenanthrene, and
pyrene]. In addition, following the PM and MCEM analyses, the samples were analyzed to
screen for the presence of 17 trace metals. Baghouse dust samples were also collected and
analyzed for the same 16 trace metals. Simultaneous testing was perfonned at the inlet and
outlet of the baghouse controlling emissions from the coke oven pushing operation. Outlet
sampling was also perfonned on the combustion stack. In addition to pollutant testing, oxygen
(02) and carbon dioxide (C02) were measured at each location. During tl?e sampling program,
Research Triangle Institute (RTI), another EPA contractor, monitored and recorded process and
emission control system operating parameters.
PES used two subcontractors for this effort: DEECO provided technical assistance in
preparation of the Quality Assurance Project Plan (QAPP) and assisted in the field sampling, and
Eastern Research Group (ERG) prepared filter media and analyzed the EP A Method 315 samples
for PM and EOM. In addition, PES used three contract laboratories for analytical services:
Quanterra Environmental Services (Quanterra) provided P AH analyses using California Air
Resources Board (CARB) Method 429, First Analytical Laboratories (F AL) provided metals
analyses of the PMlMCEM sample residues and baghouse dust samples, and Laboratory
Corporation of America (LabCorp) provided P AH analyses using National Institute for
Occupational Safety and Health (NIOSH) Method 5506. The test program organization and
major lines of communication are presented in Figure 1.1.
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Belhlehem Steel EPAIEMC EPAIESD
Corporation Work Assi~ent ManaRer
Tom Easterly Lula Melton
(219) 787-2712 John C. Bosch, Jr. (919) 541-2910
(919) 541-5583
I
PES Contractor
ProRram ManaRef Research Triangle Institute
John T. Chehaske Marvin Branscome
(703) 471-8383 (919) 990-8643
I
I I
PES PES
QAlQC Coordinator Proiect ManaRer
Dennis P. Holzschuh Franklin Meadows
(919)941-0333 (919) 941-0333
I
I I I I 1
Pretest Site Repon
Survey SSTP QAPP Field Testing Analyses Preparation
PES PES PES PES PES PES
I I I
Subcontractor Subcontractor Subcontractor
DEECO DEECO ERG
Quanterra
First Analytical
LabCorp
Figure 1.1 Key Personnel and Responsibility for Testing at Bethlehem Steel Corp., Chesterton, Indiana
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2.0 SUMMARY OF RESULTS
This section provides test result summaries obtained from the Bethlehem Steel testing.
Included in this summary are results of the tests conducted for filterable particulate matter (PM),
methylene chloride extractable matter (MCEM), multiple metals and polycyclic aromatic
hydrocarbons (P AHs) at the baghouse inlet and outlet, and the outlet stack of the combustion
(underfire) stack. At each sampling location, stack gas temperatures and flow rates were
determined using both the CARB 429 and EP A Method 315 sample procedures. At each
location, each method produced slightly different results. These differences are attributed 0
placement of the sample probes during the course of each sample run. The sample probes were
not placed together in the same sample port or at the same sample traverse point. The measured
temperatures and flow rates varied between sample ports, as well.
Also, because a significant amount of the sampling at the baghouse inlet and outlet
occured during non-pushing periods, the measured emissions from the pushing include any target
pollutants that were present in the ambient air around the ovens and captured by the hood. On a
mass emission basis, this represents a marginal, positive bias that is not believed to be
significant.
2.1
EMISSIONS TEST LOG
Sampling at the coke oven pushing baghouse was conducted on August 11, 12, and 13,
1998. Sampling on the combustion stack was conducted on August 14 and 15, 1998. Table 2.1
summarizes the emissions test log. Presented are the run numbers, test dates, pollutants, run
times and downtime for filter and sampling port changes.
2.2
FILTERABLE PARTICULATE MATTER, METHYLENE CHLORIDE
EXTRACT ABLE MATTER (MCEM), AND METALS
EP A Method 315 procedures were used to determine PM, MCEM, and 17 metals at the
baghouse inlet and outlet and underfire stack. The target metals included: antimony (Sb), arsenic
(As), barium (Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead
(Pb), manganese (Mn), mercury (Hg), nickel (Ni), phosphorous (P), selenium (Se), silver (Ag),
thallium (TI), and zinc (Zn). PM and MCEM were withdrawn isokinetically from the source.
The PM mass includes any material removed in the probe acetone rinse and material on the filter.
The MCEM was determined by adding a methylene chloride rinse of the probe and filter holder,
extracting the condensible hydrocarbons collected in the impinger water, adding an acetone rinse
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TABLE 2.1
EMISSIONS TEST LOG, BETHLEHEM STEEL CORPORATION, CHESTERTON, INDIANA
Run No. bate Pollutant Run Time Downtime, minutes
Coke Oven Battery No.2 Baghouse Inlet
B-I-M3]5-] 08/] 1/98 EOMlMetals ] 035-2020 ]26
B-I-M429-] 08/] 1/98 PAHs ]030-20]6 132
B-I-M5506-1 08/11/98 PAHs ]206-2007 149
B-I-M315-2 08/12/98 EOM/Metals 0922-1941 133
B-I-M429-2 08/12/98 PAHs 0924-]935 78
B-I-M5506-2 08/12/98 PAHs 0944-1928 154
B-]-M315-3 08/13/98 EOM/Metals 0842-1736 51
B-I-M429-3 08/13/98 PAHs 1332-] 934 _a
B-I-M5506-3 08/13/98 PAHs 0842-]710 28
Coke Oven Battery No.2 Baghouse Outlet
B-O-M315-1 08/11/98 EOM/Metals 1037-1958 110
B-O-M429-1 08/11/98 PAHs 1037-1958 194
B-O-M5506-1 08/11/98 PAHs 1207-2000 143
B-O-M315-2 08/12/98 EOM/Metals 0929-1935 126
B-O-M429-2 08/12/98 PAHs 0928-1934 128
B-O-M5506-2 08/12/98 PAHs 0944-1901 107
B-O-M315-3 08/13/98 EOM/Metals 0840-1749 68
B-O-M429-3 08/13/98 PAHs 0840-1748 68
B-O-M5506-3 08/13/98 PAHs 0840-1715 40
Coke Oven Battery No.2 Combustion Stack
B-U-M315-1 08/14/98 EOM/Metals 0921-1325 64
B-U-M429-1 08/14/98 P AI-Js 0921-1325 64
B-U-M5506-1 08/14/98 PAHs 1 ]03-1320 2
B-U-M315-2 08/14/98 EOM/Metals 1441-1809 28
B-U-M429-2 08/14/98 PAHs 1442-1809 27
B-U-M5506-2 08/14/98 PAHs 1441-1755 14
B-U-M315-3 08/15/98 EOM/Metals 0838-1203 25
B-U-M429-3 08/15/98 PAHs 0838-1208 30
B-U-M5506-3 08/15/98 PAHs 0841-1205 24
aSampling was continuous in only one port, over a 6-hour time frame. The first 4-hour portIon
of this sample run was voided due to an unacceptable post-test leak check.
-------
followed by a methylene chloride rinse of the sampling train components after the filter and
before the silica gel impinger, and determining residue gravimetrically after separating the
solvent. The metals analyses consisted of a nitric acid digestion of the filters and impinger
residues described above. The metals analysis was by Direct Aspiration Flame Atomic
Absorption Spectrophotometry (FLAAS), Graphite Furnace Atomic Absorption
Spectrophotometry (GF AAS), and Inductively Coupled Plasma - Optical Emission (ICP).
Mercury analysis was by Cold Vapor Atomic Adsorption Spectrophotometry (CV AAS). The
baghouse inlet and outlet were sampled simultaneously to determine PM, MCEM, and metals.
Sampling on the underfire stack was performed after the baghouse sampling effort.
The pushing operation necessitated adjusting sampling rates for maximum air flow during
the actual pushing of coke. The pushing process occurred roughly once every 15 minutes, and
lasted approximately two minutes. This required a maximum sample rate during the two minute
push and a much lower sample rate during the idle time. This sample approach was used for all
the isokinetic sample systems. The isokinetics were based on time weighted averages of pressure
drops (delta p), stack temperatures, and meter temperatures. All concentrations and emission rate
data in the tables are flow-weighted averages of both pushing and non-pushing periods.
2.2.1
Coke Oven Battery No.2 Baghouse Inlet
Table 2.2 summarizes the EP A Method 315 baghouse inlet sample times and flue gas
parameters. The total sampling time varied for each test run with an average of 484 minutes.
The average sampling rate was 0.252 dry standard cubic feet per minute (dscfm). The average
sample volume was 121.613 dry standard cubic feet (dscf) or 3.444 dry standard cubic meters
(dscm). The average flue gas temperature was 160 degrees Fahrenheit (OF). The flue gas
contained 0.5 percent (%) carbon dioxide (C02), 20.0% oxygen (02) and 2.2% moisture. The
average flue gas volumetric flow rate was 77,242 actual cubic feet per minute (acfm) or 63,568
dscfm, or 1,800 dry standard cubic meters per minute (dscmm).
Table 2.3 summarizes the flue gas PM concentrations and emission rates at the baghouse
inlet. The average concentration was 0.390 grains per dry standard cubic foot (gr/dscf) or
5.56E-05 pounds per dry standard cubic foot (lb/dscf) or 8.91E+05 micrograms per dry standard
cubic meter (.ug/dscm). The average emission rate was 212.3 pounds per hour (lb/hr) or
9.63E+ 10 micrograms per hour (ug/hr) or 1.9 pounds per ton of coke pushed (lb/ton pushed).
Table 2.4 summarizes the flue gas MCEM concentrations and emission rates at the
baghouse inlet. The average MCEM concentration was I.00E-03 gr/dscf or 1.43E-07 lb/dscf or
2,290 t-lg/dscm. The average MCEM emission rate was 0.5461b/hr or 2.48E+08 J,lg/hr or
4.89E-03 lb/ton pushed.
Table 2.5 summarizes the flue gas metals concentrations and emission rates. The PM and
MCEM residues were analyzed for 17 metals. Measured inlet metals concentrations were blank
corrected based on the quartz filter blank results. Average concentrations ranged from 0.13
J,lg/dscm for silver to 59.7 J,lg/dscm for zinc.
-------
TABLE 2.2
PARTICULAT~ MATTER/MCEM/METALS EMISSIONS SAMPLING
AND FLUE GAS PARAMETERS - BAGHOUSE INLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-315-1 I 8-1-315-2 I 8-1-315-3 I Average J
Date 08/11/98 08/12/98 08/13/98 -
Total Sampling Time, minutes 459 510 483 484
Coke Oven Pushes Per Test Run 46 47 42 45
Tons of Coke Pushed Per Hour 114.4 109.3 112.1 11 \.9
Avg. Sampling Rate, dscfm" 0.270 0.239 0.247 0.252
Sample Volume:
dscf" 123.890 12\.824 119.125 121.613
dscmc 3.508 3.450 3.373 3.444
A vg. Flue Gas Temp, OF 153 158 170 160
O2 Conc., % by Volume 20.1 20.0 20.0 20.0
CO2 Conc., % by Volume 0.5 0.5 0.5 0.5
Moisture, % by Volume 2.5 2.3 2.0 2.2
Flue Gas Volumetric Flow Rate:
acfmd 77,509 77 ,263 76,952 77,242
dscfm" 64,257 63,845 62,60 I 63,568
dscmmC 1,820 1,808 1,773 1,800
Isokinetic Sampling Ratio, % 118.1 105.2 110.8 111.4
"Dry standard cubic feet per minute at 68°F (20°e) and 1 atm.
bDry standard cubic feet at 68°F (20°e) and 1 atm.
CDry standard cubic meters at 68°F (20°e) and 1 atm.
d Actual cubic feet per minute at flue gas conditions.
-------
TABLE 2.3
FILTERABLE PARTICULATE MATTER CONCENTRATIONS
AND EMISSION RATES - BAG HOUSE INLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-315-1 I 8-1-315-2 I B-I-315-3 I Average I
Date 08/11/98 08/12/98 08/13/98 -
ClOCk Time, 24 hr Clock 1035-2020 0922-1941 0842-1736 --
Concentration:
gr/dscf" 0.339 0.471 0.358 0.390
Ib/dscf1> 4.85E-05 6.73E-05 5.11E-05 5.56E-05
~g/dscm< 7.77E+05 10.78E+05 8. 19E+05 8.9IE+05
Emission Rate:
Ib/hrd 187.0 257.8 192.1 212.3
~g/hr 8.48E+1O 11.70E+I0 8.71E+ 10 9.63E+ 1 0
Ib/ton pushedf 1.63 2.36 1.71 1.90
"Grains per dry standard cubic foot at 68°F (20°C) and 1 atm.
bPounds per dry standard cubic foot at 68°F (20°C) and 1 atm.
-------
TABLE 2.4
METHYLENE CHLORIDE EXTRACTABLE MATTER CONCENTRATIONS
AND EMISSION RATES - BAG HOUSE INLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-315-1 I 8-1-315-2 I 8-1-315-3 I Average 1
Date 08/11/98 08/12/98 08113/98 --
ClOCk Time, 24 hr Clock 1035-2020 0922-1941 0842-1736 --
Concentration:
gr/dscf' 1.02E-03 1.14E-03 0.84E-03 1.00E-03
Ib/dscf' 1.63E-07 1.63E-07 1.20E-07 1.43E-07
J.lg/dscmc 2,340 2,610 1,930 2,290
Emission Rate:
I blhtl 0.563 0.624 0.452 0.546
J.lglhr 255E+08 2.83E+08 2.05E+08 2.48E+08
Ib/ton pushed' 4.92E-03 5.71E-03 4.03E-03 4.89E-03
"Grains per dry standard cubic foot at 68°F (20°C) and I atm.
bPounds per dry standard cubic foot at 68°F (20°C) and 1 atm.
cMicrograms per dry standard cubic meter at 68°F (200C) and I atm.
dPounds per hour.
CMicrograms per hour.
'Pounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.5
MULTIPLE METALS CONCENTRATIONS AND EMISSION RATES
BAG HOUSE INLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-315-1 I 8-1-315-2 I 8-1-315-3 I Average I
Date 08/1 1/98 08/12/98 08/13/98 --
ClOCk Time, 24 hr Clock 1035-2020 0922-1941 0842-1736 --
Antimony
J.lgldscm. 1.23 1.07 1.01 1.10
J.lglhr> 1.34E+05 1.16E+05 1.07E+05 1.l9E+05
Ib/hr" 2.94E-04 2.56E-04 2.36E-04 2.62E-04
1b/ton pushedd 2.57E-06 2.34E-06 2.10E-06 2.34E-06
Arsenic
J.lgldscm. 17.9 23.7 27.4 23.0
J.lglhr> 1.96E+06 2.57E+06 2.91E+06 2.48E+06
1b/hr" 4.31 E-03 5.66E-03 6.40E-03 5.46E-03
Ib/ton pushedd 3.77E-05 5.18E-05 5.71E-OS 4.88E-05
Barium
J.lgldscm. 7.58 10.12 8.18 8.63
J.lglhr" 8.28E+05 1O.97E+05 8.70E+05 9.31E+05
Ib/hr" 1.82E-03 2.4IE-03 1.9 1 E-03 2.05E-03
Ib/ton pushedd 1.59E-05 2021E-05 1.71E-05 1.84E-05
Beryllium
J.lgldscm. 0.27 0.31 0.30 0.30
J.lglhr> 2.99E+04 3.36E+04 3.22E+04 3.19E+04
Ib/hr" 6.57E-05 7.40E-05 7.08E-05 7.02E-05
Ib/ton pushedd 5.75E-07 6.77E-07 6.31 E-07 6.28E-07
Cadmium
J.lgldscm. 0.37 0.61 0.77 0.58
J.lglhr> 4.05E+04 6.60E+04 8.20E+04 6.28E+04
Ib/hr" 0.89E-04 1.45E-04 1.80E-04 1.38E-04
Ib/ton pushedd 0.78E-06 1.33E-06 1.61E-06 1.24E-06
Chromium
J.lgldscm" 1.71 2.81 2.02 2.18
J.lglhr" 1.87E+05 3.05E+05 2.14E+05 2.3SE+05
1b/hr" 4.IIE-04 6.7 1 E-04 4.72E-04 5.18E-04
1b/ton pushedd 3.59E-06 6.14E-06 4.21 E-06 4.65E-06
Cobalt
J.lgldscm. 0.86 1.45 0.89 1.07
J.lglhr" 9.34E+OS 15.72E+OS 9.46E+05 1 151E+05
Ib/hr" 2.05E-04 3.46E-04 2.08E-04 2.53E-04
Ib/ton pushedd 1.80E-06 3.16E-06 I. 86E-06 2.27E-06
Copper
J.lgldscm" 3.99 6.09 5.93 5.34
J.lglhr" 4.36E+05 6.60E+05 6.3IE+05 5.76E+05
Ib/hr" 0.95E-03 1.45E-03 1.39E-03 1.27E-03
Ib/ton pushedd 0.84E-05 1.33E-05 1.24E-05 1.13E-05
-------
TABLE 2.5 (continued)
Run No. 8-1-315-1 8-1-315-2 8-1-315-3 Average
Lead
J.lg/dscma 29.2 44.1 37.7 37.0
J.lglhr> 3.18E+06 4.79E+06 4.01E+06 4.00E+06
Iblhr" 7.00E-03 10.50E-03 8.83E-03 8.79E-03
lb/ton pushedd 6. 12E-05 9.64E-05 7. 87E-05 7.88E-05
Manganese
J.lg/dscma 11.1 12.5 12.2 11.9
J.lglhr> 1.21 E+06 1.35E+06 \.29E+06 1.29E+06
Ib/hr" 2.67E-03 2.97E-03 2.84E-03 2.83E-03
Ib/ton pushedd 2.33E-05 2.72E-05 2.54E-05 2.53E-05
Mercury
J.lg/dscma 0.14 0.17 0.15 0.15
J.lglhr> 1.56E+04 1.89E+04 1.58E+04 1.67E+04
Iblhr" 3.42E-05 4. 15E-05 3.47E-05 3.68E-05
Ib/ton pushedd 2.99E-07 3.80E-07 3.09E-07 3.29E-07
Nickel
J.lg/dscma 24.8 25.1 18.2 22.7
J.lglhr> 2.7IE+06 2. 72E +06 1.94E+06 2.45E+06
lblhr" 5.96E-03 5.98E-03 4.26E-03 5.40E-03
Ib/ton pushedd 5.21E-05 5.47E-05 3.80E-05 4.83E-05
Phosphorus
J.lg/dscma I\.4 13.0 12.7 12.4
J.lglhr> 1.24E+06 1.42E+06 1.36E+06 1.34E+06
Iblhr" 2.74E-03 3.11E-03 2.98E-03 2.94E-03
Ib/ton pushedd 2.39E-05 2.85E-05 2.66E-05 2.63E-05
Selenium
J.lg/dscma 4.10 6.12 5.66 5.29
J.lglhr> 4.48E+05 6.63E+05 6.02E+05 5.7IE+05
Iblhr" 0.99E-03 1.46E-03 1.32E-03 1.26E-03
Ib/ton pushedd 0.86E-05 1.34E-05 1.18E-05 1. 13E-05
Silver
J.lg/dscma 0.09 0.17 0.12 0.13
J.lg/hr> 0.93E+04 1.89E+04 1.26E+04 1.36E+04
Ib/hr" 2.05E-05 4.15E-05 2.77E-05 2.99E-05
Ib/ton pushedd 1.80E-07 3.80E-07 2.47E-07 2.69E-07
Thallium
J.lg/dscma 1.05 1.42 1.36 1.28
J.lglhr" 1.I5E+05 1.54E+05 1.45E+05 1.38E+05
Iblhr" 2.53E-04 3.39E-04 3.19E-04 3.04E-04
Ib/ton pushedd 2.22E-06 3.10E-06 2.85E-06 2.72E-06
-------
TABLE 2.5 (concluded)
Run No. 8-1-315-1 8-1-315-2 8-1-315-3 Average
Zinc
Jlgldscm' 47.6 67.0 64.4 59.7
Jlg/hr" 5.20E+06 7. 27E+06 6.85E+06 6.44E+06
Ib/hr 1.14E-02 1.60E-02 1.5 1 E-02 1.42E-02
Ib/ton pushedd 1.00E-04 1.46E-04 1.34E-04 1.27E-04
'Micrograms per dry standard cubic meter.
bMicrograms per hour.
-------
The pushing operation necessitated adjusting sampling rates for maximum air flow during
the actual pushing of coke. The pushing process occurred roughly once every 15 minutes, and
lasted approximately two minutes. This required a maximum sample rate during the two minute
push and a much lower sample rate during the idle time. This sample approach was used for all
the isokinetic sample systems. The isokinetics were based on time weighted averages of pressure
drops (delta p), stack temperatures, and meter temperatures. All concentrations and emission rate
data in the tables are flow-weighted averages of both pushing and non-pushing periods.
The following notes were recorded during the field sampling effort and analyses of
samples. Events were discussed with the W AM and ESD personnel when modifications to the
test plan were required.
.
The baghouse inlet site could not be sampled using all four sampling ports. Two
ports were used, necessitating the use of a 10' effective Teflon@ lined probe and
flexible Teflon@ connections to the impinger system.
.
Inlet filters had to be changed during each port change due to heavy particulate
loading.
.
On August 11, sample runs were shortened from the original 10 hour proposed
sample length to eight hours. The runs were initially shortened due to darkness.
At this point in the program it was agreed upon to shorten test runs to eight hours.
Even with shortened sample times we were able to sample during a minimum of
40 pushes, which was one of the project goals.
.
Sample times were adjusted to insure all traverse points were sampled.
.
Run No. B-I-M315-1 did not pass the post-test leak check. Based on the previous
acceptable leak checks (port change), heavy particulate loading and sample
vacuums, the sample was accepted as representative. It was determined the break
occurred when removing the probe from the duct at the end of the test run.
.
Discussed calculation of isokinetics. Calculations would be based on time
weighted averages of velocity pressures (delta p), stack temperatures, and meter
temperatures.
.
Run No. B-I-M429 sample had a small amount of particulate get past the filter.
Robert Weidenfeld of Quanterra was contacted to discuss possible sample effects.
The total sample fraction is extracted for P AHs, the particulate should have no
effect on the XADti-2 resin analyses or results.
.
The EP A W AM, John Bosch, requested a discussion on the benefit of a thorough
review of laboratory sample handling and analyses procedures. PES was
instructed to implement review procedures for the analytical laboratories.
-------
.
Run No. B-I-M429-3 did not pass leak check at port change (- four hours into
run). Sample was voided and a new M429 run was restarted. Sample ran for six
hours (four hours simultaneous with outlet sample).
.
On August 18, Quanterra reported that one filter on the B-I-429-3 run had a small
amount of water from the ice used to keep samples cool.
.
On August 18, Quanterra reported that on Run No. B-I-M429-1 the water
knockout container had lost a small amount of contents.
2.2.2 Coke Oven Battery No.2 Baghouse Outlet
Table 2.6 summarizes the EP A Method 315 baghouse outlet sample times and flue gas
parameters. The total test time varied for the three test runs, with an average time of
443 minutes. The average sampling rate was 0.366 dscfm. The average sampling volume was
163.069 dscf or 4.618 dscm. The average flue gas temperature was 135°F, with average stack
gas compositions of20.2% O2 and 0.5% CO2, Moisture content of the flue gas averaged 2.3%.
Flue gas volumetric flow rates averaged 95,427 acfm or 82,242 dscfm or 2,329 dscmm. The
isokinetic sampling rate averaged 98.2 percent.
The baghouse outlet sampling location indicated a higher volumetric flowrate in
comparison to the baghouse inlet sampling location. This was due to a dilution air damper
located on the mass cooler remaining open at 10% of full opening during periods of non-pushing
(roughly 13 minutes of a total of 15 minutes). The dilution air damper was fully open during
pushing operations, or 2 minutes out of 15 minutes. This resulted in measurable air flow for the
entire length of the test during non-pushing operations at the baghouse outlet that were greater
than flows measured at the baghouse inlet sampling location, which was located prior to the mass
cooler.
Table 2.7 summarizes the PM concentrations and emission rates for the baghouse outlet.
The average PM concentration was 4.66E-04 gr/dscf or 6.66E-08 lb/dscf or 1,070 ,ugldscm. The
average emission rate was 0.329 lb/hr or 1.49E+08 ,uglhr or 2.85E-03 lb/ton pushed.
Table 2.8 summarizes the MCEM concentrations and emission rates for the baghouse
outlet. Concentrations averaged 4.49E-04 gr/dscf or 6.41E-08 lb/dscf or 1,030 ,ug/dscm.
Emission rates averaged 0.317 lb/hr or 1.44E+08 ,ug/hr or 2.74E-03 lb/ton pushed.
Table 2.9 summarizes the multiple metals concentrations and emission rates for the
combined PM and MCEM fractions collected with the EP A Method 315 sampling trains. The
majority of the 17 target metals were found to be non-detectable.
Table 2.10 summarizes the multiple metals concentrations from the baghouse dust
samples collected during each baghouse sample run. Baghouse samples were collected from the
dust hoppers at the beginning, middle, and end of each run.
-------
TABLE 2.6
PARTICULATE MATTER/MCEMIMETALS EMISSIONS SAMPLING AND
FLUE GAS PARAMETERS - BAGHOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
nNo. 8-0-315-1 8-0-315-2 8-0-315-3 Average
Date 08/11/98 08112/98 08/13/98 -
Total Sampling Time, minutes 368 480 481 443
Coke Oven Pushes Per Test Run 46 47 42 45
Tons of Coke Pushed Per Hour 119.3 11l.7 114.4 115.1
Avg. Sampling Rate, dscfmD 0.343 0.378 0.377 0.366
Sample Volume:
dscf' 126.388 181.292 181.577 163.069
dscmC 3.577 5.134 5.142 4.618
Avg. Flue Gas Temp, of 134 135 135 135
O2 Conc., % by Volume 20.5 20.0 20.0 20.2
CO2 Cone., % by Volume 0.5 0.5 0.5 0.5
Moisture, % by Volume 2.5 2.2 2.1 2.3
Flue Gas Volumetric Flow Rate:
acfmd 96,755 94,024 95,502 95,427
dscfmD 83,087 81,147 82,493 82,242
dscmm" 2,353 2,298 2,336 2,329
Isokinetic Sampling Ratio, % 99.6 98.3 96.7 98.2
"Dry standard cubic feet per minute at 68°F (20°C) and I atm.
bDry standard cubic feet at 68°F (20°C) and I atm.
COry standard cubic meters at 68DF (20°C) and I atm.
dActual cubic feet per minute at flue gas conditions.
CDry standard cubic meters per minute at 68DF (20DC) and I atm.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.7
FILTERABLE PARTICULATE MATTER CONCENTRATIONS
AND EMISSION RATES - BAGHOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
- . B-0-315-1 8-0-315-2 8-0-315-3 Average
I ~UII ,,0.
Date 08/11/98 08/12/98 08/13/98 --
Clock Time, 24 hr Clock 1037-1958 0929-1935 0840-1749 -
Concentration:
gr/dscf' 5.74E-04 3.75E-04 4.50E-04 4.66E-04
Ib/dscf' 8.20E-08 5.35E-08 6.43E-08 6.66E-08
J.lg/dscmc 1,310 857 1,030 1,070
Emission Rate:
Iblhr" 0.409 0.261 0.319 0.329
J.lg/hr" 1.85E+08 1.18E+08 1.44E+08 1.49E+08
Ib/ton pushedf 3.43E-03 2.33E-03 2.78E-03 2.85E-03
3Grains per dry standard cubic foot at 68°F (20°C) and 1 atm.
bPounds per dry standard cubic foot at 68°F (20°C) and I atm.
CMicrograms per dry standard cubic meter at 68°F (20°C) and 1 atm.
dPounds per hour.
"Micrograms per hour.
dPounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.8
METHYLENE CHtORIDE EXTRACTABLE MATTER CONCENTRATIONS
AND EMISSION RATES - BAG HOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I B-0-315-1 I B-0-315-2 I B-0-315-3 I Average I
Date 08/1 1/98 08/12/98 08/13198 --
ClOCk Time, 24 hr Clock 1037-1958 0929-1935 0840-1729 -
Concentration:
gr/dscF 5.13E-04 3.92E-04 4.42E-04 4.49E-04
Ib/dscF 7.33E-08 5.59E-08 6.3IE-08 6.41 E-08
~g/dscmc 1,170 896 1,010 1,030
Emission Rate:
I blhrt 0.365 0.272 0.312 0.317
~gIhr" 1.66E+08 1.24E+08 1.42E+08 1.44E+08
Iblton pushedf 3.06E-03 2.44E-03 2.73E-03 2.74E-03
"Grains per dry standard cubic foot at 68°P (20°C) and I atm.
bPounds per dry standard cubic foot at 68°P (20°C) and 1 atm.
"Micrograms per dry standard cubic meter at 68°F (200C) and 1 atm.
dPounds per hour.
"Micrograms per hour.
dPounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.9
MUL TIPLE METALS CONCENTRATIONS AND
EMISSION RATES - BAG HOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-0-315-1 I 8-0-315-2 I 8-0-315-3 I Average I
Oate 08/11/98 08/12/98 08/13/98 --
ClOCk Time, 24 hr Clock 1037-1958 0929-1935 0840-1749 -
Antimony
J.lg/dscma NO NO NO NO
J.lg/hr> NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton pushedd NO NO NO NO
Arsenic
J.lg/dscma NO NO NO NO
J.lg/hr> NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton pushedd NO NO NO NO
Barium
J.lg/dscm' 1.12E-O I 1.36E-OI NO 0.83E-OI
J.lg/hr> 1.58E+04 1.88E+04 NO 1.15E+04
lb/hr" 3.47E-05 4.14E-05 NO 2.54E-05
Ib/ton pushedd 2.91E-07 3. 70E-07 NO 2.21E-07
Beryllium
J.lg/dscma NO NO NO NO
J.lg/hr> NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton pushedd NO NO NO NO
Cadmium
J.lg/dscma 2.80E-02 NO NO 0.93E-02
J.lg/hr> 3,946 NO NO 1,315
Ib/hr" 8.68E-06 NO NO 2.89E-06
Ib/ton pushedd 7.28E-08 NO NO 2.43E-08
Chromium
J.lg/dscma NO NO NO ND
J.lg/hr> NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton pushedd NO NO NO NO
Cobalt
J.lg/dscm' NO NO NO NO
J.lg/hr> NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton pushedd NO NO NO NO
Copper
J.lg/dscma NO 3.90E-01 NO 1.30E-O I
J.lg/hr> NO 5.37E-04 NO 1.79E+04
Ib/hr" NO 1.18E-04 NO 0.39E-04
Ib/ton pushedd NO 1.06E-06 NO 3.53E-07
-------
TABLE 2.9 (continued)
Run No. 8-0-315-1 8-0-315-2 8-0-315-3 Average
Lead
J-lg/dscma ND ND ND ND
J-lg/hr> ND ND ND ND
Iblhr ND ND ND ND
Ib/ton pushedd ND ND ND ND
Manganese
J-lg/dscm8 ND 7.79E-Ol ND 2.60E-0 1
J-lg/hr> ND 1.07E+05 ND 0.36E+05
Ib/hr ND 2.36E-04 ND 0.79E-04
Ib/ton pushedd ND 2.12E-06 ND 0.71E-06
Mercury
J-lg/dscm8 ND ND ND ND
J-lg/hr> ND ND ND ND
I blhrd ND ND ND ND
Ib/ton pushedd ND ND ND ND
Nickel
J-lg/dscma ND 1.75E-Ol ND 0.58E-Ol
J-lg/hr> ND 2.42E+04 ND 0.81E+04
Iblhr ND 5.32E-05 ND 1.77E-05
Ib/ton pushedd ND 4.76E-07 ND 1.59E-07
Phosphorus
J-lg/dscma ND ND ND ND
J-lg/hr> ND ND ND ND
Iblhr" ND ND ND ND
Ib/ton pushedd ND ND ND ND
Selenium
J-lg/dscma ND 9.74E-02 ND 3.25E-02
J-lg/hr> ND 1.34E+04 ND 0.45E+04
Iblhr ND 2.95E-05 ND 0.99E-05
Ib/ton pushedd ND 2.65E-07 ND 0.88E-07
Silver
J-lg/dscma ND 4.09E-0 I ND 1.36E-Ol
J-lg/hr> ND 5.64E+04 ND 1.88E+04
Ib/hr" ND 1.24E-04 ND 0.4 I E-04
Ib/ton pushedd ND 1.11 E-06 ND 0.37E-06
Thallium
J-lg/dscma ND ND ND ND
J-lg/hr> ND ND ND ND
Iblhr" ND ND ND ND
Ib/ton pushedd ND ND ND ND
-------
TABLE 2.9 (concluded)
Run No. 8-0-315-1 8-0-315-2 8-0-315-3 Average
Zinc
Jlg/dscm" ND 1.S6E-Ol NO O.52E-OI
Jlg/hr" ND 2. 15E+04 NO O.72E+04
Iblhr" NO 4.73E-05 NO 1.5SE-05
Ib/ton pushedd NO 4.23E-07 NO 1.41E-07
"Micrograms per dry standard cubic meter.
bMicrograms per hour.
.Pounds per hour.
dPounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.10
BAG HOUSE DUST MUL TIPLE METALS CONCENTRA nONS
BETHLEHEM STEEL, CHESTERTON, INDIANA
Run No. BD-BS-l BD-BS-2 BD-BS-3 Ave -eo-
Date 08/1 1198 08/12/98 08/13/98 -
Antimony, J.J.g!ft 0.33 0.52 0.36 0.40
Arsenic, J.J.g!g 10.70 10.50 1 1.00 10.73
Barium, /-lg!g 9.21 9.32 8.62 9.05
Beryllium, J.J.g!g 0.42 0.33 0.29 0.35
Cadmium, /-lg!g 1.64 1.50 1.80 1.65
Chromium, J.J.g!g 7.42 8.33 6.39 7.38
Copper, /-lg!g 7.70 8.10 6.50 7.43
Lead, J.J.g/g 35.80 36.40 38.90 37.03
Manganese, /-lglg 67.50 70.20 66.20 67.97
Mercury, J.J.glg 0.20 0.15 0.18 0.18
Nickel, /-lg!g 7.00 7.80 6.70 7.17
Phosphorus, /-lg/g 44.70 50.40 43.50 46.20
Selenium, /-lg!g 3.80 3.50 3.20 3.50
Silver, /-lglg 0.05 ND 0.06 0.04
Thallium, /-lg!g 0.77 0.88 0.72 0.79
Zinc, J.J.glg 37.50 36.10 39.70 37.77
"/-lg!g - Microgram per gram of dust sample.
ND . non detected, counted as "zero".
-------
Table 2.11 -summarizes the PM and MCEM removal efficiencies for the Coke Oven
Battery No.2 baghouse. PM removal efficiencies averaged 99.85%. MCEM removal
efficiencies averaged 41.94%.
The pushing operation necessitated adjusting sampling rates for maximum air flow during
the actual pushing of coke. The pushing process occurred roughly once every 15 minutes, and
lasted approximately two minutes. This required a maximum sample rate during the two minute
push and a much lower sample rate during the idle time. This sample approach was used for all
the isokinetic sample systems. The isokinetics were based on time weighted averages of pressure
drops (delta p), stack temperatures, and meter temperatures. All concentrations and emission rate
data in the tables are flow-weighted averages of both pushing and non-pushing periods.
The filterable PM does not necessarily have to be more than the MCEM. The filterable
PM is based on PM collected in the probe and on the MCEM. The MCEM includes both the
filterable PM and condensible sample fractions.
The following notes were recorded during the field sampling effort and analysis of
samples. Events were discussed with the W AM and ESD personnel when modifications to the
test plan were required.
.
The shortened sample times as described previously, apply to the outlet location
also.
.
Calculation of isokinetics, as discussed previously, also applies to the outlet
location.
.
On August 12 plant personnel were requested to modify eyebolts on the outlet
stack. The eyebolts were used to support a monorail sample conveyor system,
and were placed three feet above the ports. This was necessary to insure a safe
support system for sampling. This caused a slight delay in our start time.
2.2.3 Underfire Stack
The combustion or underfire stack was sampled for PM and MCEM concentrations and
emission rates, as well as multiple metals analysis on the EOM filters and residue. A total of
three, 180 minute sample runs were conducted at this test location.
Table 2.12 summarizes the EP A Method 315 underfire stack sample times and flue gas
parameters measured. Three sample runs were conducted over the course of two days. The
average sampling time was 182 minutes, sample Run No. U-315-3 being 185 minutes in length,
compared to 180 minutes for the other two runs. The average sampling rate was 0.537 dscfm.
The average sample volume was 97.823 dscf or 2.770 dscm. Flue gas temperatures averaged
444°F, with an average stack gas composition of 5.0% CO2 and 10.4% O2, Flue gas moisture
content averaged 17.0%. The flue gas volumetric flow rate averaged 157,321 acfm or 75,684
dscfm or 2,143 dscmm. Isokinetic sampling rates for the sample runs averaged 105%.
-------
TABLE 2.11
FIL TERABLE PARTICULATE MATTER AND METHYLENE CHLORIDE
EXTRACTABLE MATTER REMOVAL EFFICIENCIES
COKE OVEN BATTERY NO.2 BAG HOUSE
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Test Set No. I M-315-1 I M-315-2 I M-315-3 I Average J
Date 08/11/98 08/1 2/98 08/13/98 -
Filterable Particulate Matter
Emission Rate, Ib/hr;a
Inlet 187.0 257.8 192.1 212.3
Outlet 0.409 0.261 0.319 0.329
Removal Efficiency, %b 99.78 99.90 99.83 99.85
Extractable Organic Matter
Emission Rate, Ib/hr:a
Inlet 0.563 0.624 0.452 0.546
Outlet 0.365 0.272 0.3 I 2 0.317
Removal Efficiency, %b 35.17 56.41 30.97 41. 94
'Pounds per hour.
bRemoval Efficiency, % = Inlet. Ib/hr - Outlet. Iblhr x 100
Inlet, Ib/hr
Note; All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.12
PARTICULATE MATTERlMCEMlMETALS EMISSIONS SAMPLING AND
FLUE GAS PARAMETERS - UNDERFIRE STACK
BETHLEHEM STEEL, CHESTERTON, INDIANA
~un No. B-U-315-1 B-U-315-2 B-U-315-3 Average
Date 08/14/98 08/]4/98 08/15/98 --
Total Sampling Time, minutes 180 ]80 ]85 182
Tons of Co a! Charged Per Hour ]59.0 ]41.5 ]60.8 ]53.8
A vg. Sampling Rate, dscfm" 0.512 0.417 0.682 0.537
Sample Volume:
dscf> 92.]98 75.109 126.161 97.823
dscmc 2.6]] 2.127 3.572 2.770
A vg. Flue Gas Temp, OF 444 45] 438 444
O2 Conc., % by Volume 11.3 9.6 ]0.5 10.4
CO2 Conc., % by Volume 4.4 5.5 5.0 5.0
Moisture, % by Volume ]7.1 17.3 16.6 17.0
Flue Gas Volumetric Flow Rate:
acfmd ]60,715 134,733 176,514 157,321
dscfm" 77,362 64,153 85,538 75,684
dscmmc 2,191 1,8] 7 2,442 2,]43
Isokinetic Sampling Ratio, % 106 ]08 10] 105
"Ory standard cubic feet per minute at 68°F (20°C) and I atm.
bDry standard cubic feet at 68°F (20°C) and 1 atm.
COry standard cubic meters at 68°F (20DC) and I atm.
dActual cubic feet per minute at flue gas conditions.
.Dry standard cubic meters per minute at 68°F (20°C) and 1 atm.
-------
Analysis of the data indicates that the flow rate determined for Run No. B-U-31 5-2 was
about 20% lower than the average flow rate (81,450 dscfin) for Run Nos. B-U-31 5-1 and
B-U-315-3. Also, the flow rate was about 30% lower than the flow rate determined concurrently
during Run No. B-U-429-2 using CARB Method 429. Although no reason can be found to
explain this discrepancy, it appears that the flow rate during Run No. B-U-31S-2 was too low,
thereby biasing the PM, MCEM, and metals emission rates by 20-30% for that test run.
Table 2.13 summarizes the PM concentrations and emission rates for the underfire stack.
Concentrations averaged 3.9SE-02 gr/dscf or 5.65E-06 lb/dscf or 9.0SE+04 t-Lg/dscm. Emission
rates averaged 25.5 lb/hr or 1. 16E+09 t-Lg/hr or 1.66E-Ol pounds per ton of coal charged
(lb/ton charged).
Table 2.14 summarizes the MCEM concentrations and emission rates for the three sample
runs. Concentrations averaged lO.lE-03 gr/dscf or 14.4E-07Ib/dscf or 2.31E+04 t-Lg/dscm.
Emission rates averaged 6.851b/hr or 3.1IE+1O t-Lg/hr or 4.37E-02Ib/ton charged. Sample Run
No.3 results were roughly three times higher than the first two runs. Sample Run No: 3 was
performed on Saturday, August 15, 1998.
Table 2.15 summarizes the multiple metal concentrations and emission rates from the PM
and MCEM residues of the EP A Method 315 samples. Measured underfire metals
concentrations were blank corrected based on the blank quartz filter results. The majority of the
target analytes were below detectable quantities for most of the test runs. Arsenic, barium, lead,
and selenium were found in detectable quantities in all the samples.
The following notes were recorded during the field sampling effort and analysis of
samples. Events were discussed with the W AM and ESD personnel when modifications to the
test plan were required.
.
On August 13 the underfire site was prepared for sampling. Port covers were
removed and ports cleaned prior to sampling. Bethlehem Steel provided
personnel to cut steel rails to allow PES sample hardware to be used.
.
During a port change on Run No. B-U-429-1, the probe was broken. The glass
liner was changed and the run was continued. This did not affect the sample
results.
2.3
POLYCYCLIC AROMATIC HYDROCARBONS (PAHs)
The polycyclic aromatic hydrocarbons (P AHs) were collected using CARB Method 429,
"Determination of Polycyclic Aromatic Hydrocarbons from Stationary Sources." This method
was used to determine 19 individual P AHs. Particulate and gaseous phase P AHs were extracted
isokinetically from each source and collected in the probe, TeflonCl> filter, XADCI>-2 resin and
impinger portions of the sampling train. The baghouse inlet and outlet were sampled
simultaneously for the measurement of P AHs. The underfire stack P AHs were sampled
-------
TABLE 2.13
FILTERABLE P ARTICULATE MA TIER CONCENTRATIONS
AND EMISSION RATES - UNDERFIRE STACK
BETHLEHEM STEEL, CHESTERTON, INDIANA
Run No. B-U-315-1 B-U-315-2 B-U-315-3 Average
Date 08/14/98 08/14/98 08/15/98 -.
Clock Time, 24 hr Clock 0921-1325 1441-1809 0838-1203 -
Concentration:
gr/dscf' 3.41E-02 4.47E-02 3.99E-02 3.95E-02
lb/dscf' 4.87E-06 6.39E-06 5.69E-06 5.65E-06
J.tg/dscm< 7.80E+04 IO.23E+04 9. 12E+04 9.05E+04
Emission Rate:
I b/hrt 22.6 24.6 29.2 25.5
J.tglhr 1.03E+IO 1.12E+l0 l.33E+1O 1.16E+IO
Ib/ton chargedf 1.42E-0 I 1. 74E-O1 1. 82E-01 1.66E-O 1
"Grains per dry standard cubic foot at 68°F (20°C) and 1 atm.
bPounds per dry standard cubic foot at 68°F (20°C) and 1 atm.
-------
TABLE 2.14
METHYLENE CHLORIDE EXTRACTABLE MATTER CONCENTRATIONS
AND EMISSION RATES - UNDERFIRE STACK
BETHLEHEM STEEL, CHESTERTON, INDIANA
Run No. B-U-315-1 B-U-315-2 B-U-315-3 Average
Date 08/14/98 08/14/98 08/15198 .-
Clock Time, 24 hr Clock 0921-1325 1441-1809 0838-1203 --
Concentration:
gr/dscf 6.83E-03 6.64E-03 16.9E-03 10.IE-03
Ib/dscf1' 9.76E-07 9.48E-07 24.1 E-07 14.4E-07
~gldscm< 1.56E+04 1.52E+04 3.86E+04 2.3IE+04
Emission Rate:
Iblhr" 4.53 3.65 12.37 6.85
~glhr 2.05E+09 1.66E+09 5.6IE+09 3.lIE+09
Ib/ton chargedf 2.85E-02 2.58E-02 7.69E-02 4.37E-02
"Grains per dry standard cubic foot at 68°F (20°C) and I atm.
bPounds per dry standard cubic foot at 68°F (20°C) and I atm.
-------
TABLE 2.15
MULTIPLE METALS CONCENTRATIONS AND
EMISSION RATES - UNDERFIRE STACK
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I B-U-315-1 I B-U-315-2 I B-U-315-3 I Average I
Date 08/14/98 08/14/98 08/15/98 -
ClOCk Time, 24 hr Clock 0921-1325 1441-1809 0838-1203 -
Antimony
J.lgldscma NO NO ND ND
J.lglhr" NO NO ND ND
Ib/hr" ND NO ND NO
Ib/ton chargedd NO NO NO NO
Arsenic
J.lgldscma 2.19E-03 2.20E-03 2.39E-03 2.26E-03
J.lglhr" 6.31 E+05 4.36E+05 8.43E+05 6.37E+05
Ib/hr" 6.34E-07 5.28E-07 7.66E-07 6.42E-07
Ib/ton chargedd 3.99E-09 3.73E-09 4.76E-09 4.l6E-09
Barium
J.lgldscma 1.83E-04 9.9 I E-04 2.06E-04 4.60E-04
J.lglhr" 5.26E+04 19.6E+04 7.27E+04 1O.71E+04
Ib/hr" 5.28E-08 23.8E-08 6.60E-08 11.9E-08
Ib/ton chargedd 3.32E-IO 16.8E-IO 4.IOE-10 8.07E-l 0
Beryllium
~gldscma NO NO NO NO
J.lglhr" NO NO ND NO
Ib/hr NO NO NO ND
Ib/ton chargedd NO NO NO NO
Cadmium
J.lgldscma 9.13E-05 NO ND 3.04E-05
J.lglhr" 2.63E+04 NO NO 0.88E+04
Ib/hr 2.63E-08 NO NO 0.88E-08
Ib/ton chargedd 1.66E-IO NO NO 0.55E-10
Chromium
J.lgldscma NO NO NO NO
J.lglhr" NO NO NO NO
Ib/hr NO NO NO NO
Ib/ton chargedd NO NO NO NO
Cobalt
J.lgldscma NO NO NO NO
J.lglhr" NO NO NO NO
Ib/hr" NO NO NO NO
Ib/ton chargedd NO NO NO NO
Copper
J.lgldscma NO 1.65E-03 0.83E-03 0.83E-03
J.lglhr" NO 3.27E+05 2.91E+05 2.06E+05
Ib/hr" NO 3.96E-07 2.64E-07 2.20E-07
Ib/ton chargedd NO 2.80E-09 1.64E-09 1.48E-09
-------
TABLE 2.15 (continued)
Run No. B-U-31S-1 B-U-31S-2 B-U-31S-3 Average
Lead
~gldscm' 1.55E-03 1.60E-03 0.83E-03 1.32E-03
~glhr" 4.47E+05 3.16E+05 2.9 1 E+05 3.51E+05
Ib/hr" 4.49E-07 3.83E-07 2.64E-07 3.65E-07
Ib/ton chargedd 2.82E-09 2.7IE-09 1.64E-09 2.39E-09
Manganese
~gldscm' NO NO NO ND
~glhr" ND ND ND ND
lb/hr" ND NO ND ND
lb/ton chargedd ND ND ND ND
Mercury
~gldscm' ND NO NO ND
JJglhr" ND ND NO ND
lb/hr< ND NO NO ND
Ib/ton chargedd ND NO NO ND
Nickel
JJgldscm" NO NO NO ND
~glhr" ND ND ND ND
lb/hr" ND NO ND ND
lb/ton chargedd ND NO ND ND
Phosphorus
~gldscm' ND NO NO ND
~glhr" NO NO ND ND
Ib/hr" ND ND ND ND
Ib/ton chargedd ND NO NO ND
Selenium
~gldscm' 1.05E-03 1.1 OE-03 0.41E-03 0.86E-03
~g/hr" 3.02E+05 2. 18E+05 1.45E+05 2.22E+05
lb/hr" 3.04E-07 2.64E-07 1.32E-07 2.33E-07
Ib/ton chargedd 1.91 E-09 1.87E-09 0.82E-09 1.53E-09
Silver
~gldscm' ND ND ND ND
~glhr" NO NO NO ND
Ib/hr" ND NO NO ND
Ib/ton chargedd ND ND NO NO
ThaIlium
~gldscm' 4.IIE-04 NO 4.I3E-04 2.75E-04
~glhr" 1.18E+05 ND 1.45E+05 0.88E+05
lb/hr" 1.19E-07 NO 1.32E-07 0.84E-07
lb/ton chargedd 7.47E-1O NO 8.2IE-10 5.23E-10
-------
TABLE 2.15 (concluded)
Run No. B-U-315-1 B-U-315-2 8-U-315-3 Average
Zinc
~gldscm" 8.22E-04 4.95E-04 ND 4.39E-04
~glhr" 2.37E+05 O.98E+05 ND l.12E+05
lblhr" 2.38E-07 1.19E-07 ND l.19E-07
lb/ton chargedd 14.9E-1O 8.40E-IO ND 7.78E-IO
"Micrograms per dry standard cubic meter.
bMicrograms per hour.
.Pounds per hour.
dPounds per ton of coal charged.
-------
concurrently with the EP A Method 315 sampling train, and was performed after the baghouse
sampling effort. The concentrations at all three sample locations were corrected for the method
blank.
A NIOSH Method 5506 sample system was used to scan for gaseous phase PAHs at the
baghouse inlet/outlet and underfire stack. The NIOSH approach was used as a backup approach
to the CARB Method 429 sampling system. The P AHs had never been sampled at these sample
locations and there was no previous records of P AH detectable limits or quantities. The NIOSH
analytical results are presented in Appendix C. The majority of the NIOSH Method 5506 PAH
results were at the method detection limits.
2.3.1 Coke Oven Battery No.2 Baghouse Inlet
Table 2.16 summarizes the CARB Method 429 sample times and flue gas parameters at
the baghouse inlet. One sample run was conducted per day. The average length of the sample
runs was 432 minutes. The average sampling rate was 0.186 dscfm. The average sample volume
was 80.189 dscf or 2.271 dscm.
The average flue gas temperature was 145°F, with a stack gas composition of 0.5% CO2
and 20.0% O2, Moisture content averaged 3.6%. Flue gas volumetric flow rates averaged 67,672
acfm or 56,361 dscfm or 1,596 dscmm. The isokinetic sampling rate averaged 92.2%.
The stack gas moisture content determined using the CARB 429 sample train was slightly
greater "than the moisture content determined using the EP A Method 315 sample train (3.6%
versus 2.2%). The small but consistent difference in moisture is attributed to the Method 429
XAD@resin module. The resin was protected from sunlight with an aluminum foil wrap. During
sampling, the wrap would get wet by being submerged in a ice water bath. The trap was weighed
with the aluminum foil wrap before and after each sample run. The wrap probably retained a
small amount of moisture to contribute to a small position moisture bias. It was not possible to
completely dry out the aluminum foil. Also an unheated flexible TeflonQl) sample line, 20 feet
long, was used between the filter and impinger portion of the sample train which may have
caused minor differences in moisture content.
Table 2.17 summarizes the P AH concentrations and emission rates for the baghouse inlet.
All compounds were found in detectable levels for the three test runs with the exception of
perylene (not detected in Run Nos. 2 and 3) and dibenz(a,h) anthrancene (not detected in Run
No.2). Naphthalene was found in the highest concentrations, at an average of 13.3 J.lg/dscm.
Phenanthrene and fluoranthene were the other two compounds occurring in high concentrations
(relative to the other compounds).
The pushing operation necessitated adjusting sampling rates for maximum air flow during
the actual pushing of coke. The pushing process occurred roughly once every 15 minutes, and
lasted approximately two minutes. This required a maximum sample rate during the two minute
push and a much lower s~ple rate during the idle time. This sample approach was used for all
the isokinetic sample systems. The isokinetics were based on time weighted averages of pressure
-------
TABLE 2.16
P AH EMISSIONS SAMPLING AND FLUE
GASPARAMETERS-BAGHOUSEINLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-429-1 I B-I-429-2 I 8-1-429-3 I Average I
Date 08/11/98 08/12/98 08/13/98 -
Total Sampling Time, minutes 453 482 362 432
Coke Oven Pushes Per Test Run 46 47 27. 40
Tons of Coke Pushed Per Hour 114.1 110.8 109.5 111.5
Avg. Sampling Rate, dscfm" 0.192 0.178 0.187 0.186
Sample Volume:
dscf' 87.151 85.686 67.729 80.189
dscmc 2.468 2.426 1.918 2.271
Avg. Flue Gas Temp, 0P 142 147 145 145
O2 Conc., % by Volume 20.1 20.0 20.0 20.0
CO2 Conc., % by Volume 0.5 0.5 0.5 0.5
Moisture, % by Volume 3.3 3.4 3.9 3.6
Plue Gas Volumetric Plow Rate:
acfmd 70,118 63,871 69,027 67,672
dscfm" 58,683 53,111 57,287 56,361
dscmmc 1,662 1,504 1,622 1,596
Isokinetic Sampling Ratio, % 90.5 94.1 91.8 92.2
"Dry standard cubic feet per minute at 68°P (200C) and I atm.
bDry standard cubic feet at 68°P (20°C) and I atm.
CDry standard cubic meters at 68°P (20°C) and 1 atm.
dActual cubic feet per minute at flue gas conditions.
"Dry standard cubic meters per minute at 68°P (200C) and I atm.
.Run No. B-I-429-3 consisted of a shorter sample run due to a sample train malfunction when sampling the first
port. Sampling consisted ofa straight six-hour test run utilizing other port.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.17
PAD (;ONCENTRATIONS AND EMISSION RATES
BAGHOUSE INLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-1-429-1 I 8-1-429-2 I 8-1-429-3 I Average I
Date 08/11/98 08/12/98 08/13/98 -
ClOCk Time, 24 hr Clock 1030-2016 0924-1935 1332-1934 -
Naphthalene
~g/dscm' 10.7 14.2 1.48 13.3
~glhr> 1.07E+06 1.28E+06 1.45E+06 1.27E+06
lblbf 2.36E-03 2.83E-03 3. 19E-03 2. 79E-03
lb/ton pushedd 2.07E-05 2.55E-05 2.91E-05 2.51E-05
2-Methylnaphthalene
~g/dscm' 3.20 2.80 1.60 2.52
~glhr> 3. 18E+05 2.52E+05 1.52E+05 2.41 E+05
Iblbf 7.02E-04 5.56E-04 3.34E-04 5.31E-04
lb/ton pushedd 6. 15E-06 5.02E-06 3.05E-06 4.74E-0.6
Acenaphthylene
~g/dscm' 2.23 2.43 1.36 2.01
~g/hr> 2.22E+05 2. 19E+05 1.32E+05 1.91E+05
Iblb< 4.90E-04 4.84E-04 2.91E-04 4.22E-04
Ib/ton pushedd 4.29E-06 4,37E-06 2.66E-06 3.77E-06
Acenaphthene
~g/dscm' 0.28 0.19 0.28 0.25
~glhr> 2.79E+04 l.75E+04 2.69E+04 2.41E+04
lblb!'" 6.15E-05 3.85E-05 5.93E-05 5.31E-05
lb/ton pushedd 5.39E-07 3.48E-07 5.42E-07 4.76E-07
Fluorene
~g/dscm' 0.89 0.74 0.68 0.77
~glhr> 8.89E+04 6.69E+04 6.59E+04 7.39E+04
lb/hf 1.96E-04 1.48E-04 1.45E-04 1.63E-04
lb/ton pushedd 1. 72E-06 1.33E-06 1.33E-06 1.46E-06
Phenanthrene
~g/dscm' 8.09 10.29 10.42 9.60
~glhr> 8.07E+05 9.29E+05 10.l4E+05 9. 17E+05
Iblbf 1. 78E-03 2.05E-03 2.24E-03 2.02E-03
lb/ton pushedd 1.56E-05 1.85E-05 2.04E-05 1.82E-05
Anthrancene
~g/dscm" 0.30 0.28 0.33 0.31
~glhr> 2.95E+04 2.57E+04 3.25E+04 2.92E+04
lblb!'" 6.50E-05 5.66E-05 7. 16E-05 6.44E-05
lb/ton pushedd 5.70E-07 5.IIE-07 6.54E-07 5.78E-07
FJuoranthene .
~g/dscm' 5.67 7.42 3.44 5.5]
~glhr> 5.66E+05 6.69E+05 3.35E+05 5.23E+05
lblbf 1.25E-03 1.48E-03 0.74E-03 1.15E-D3
Ib/ton pushedd 1.09E-05 1,33E-05 67.5E-05 1.03E-05
-------
TABLE 2.17 (continued)
Run No. 8-1-429-1 8-1-429-2 8-1-429-3 Average
Pyrene
J.tgldscma 0.89 1.03 0.20 0.71
J.tg/hr> 8.89E+04 9.30E+04 1.93E+04 6.70E+04
Ib/hf 1.96E-04 2.05E-04 0.43E-04 1.48E-04
Ib/ton pushedd 1. 72E-06 1.85E-06 0.39E-06 t.32E-06
Benzo(a) Anthrancene
J.tgldscm" 0.37 0.32 0.07 0.25
J.tg/hr> 3.68E+04 2.86E+04 0.66E+04 2.40E+04
Ib/hr" 8.IIE-05 6.31 E-05 1.45E-05 5.29E-05
Ib/ton pushedd 7.1OE-07 5.70E-07 1.33E-07 4.7lE-07
Chrysene
J.tgldscm" 2.23 2.47 0.99 1.90
J.tg/hr> 2.22E+05 2.23E+05 0.96E+05 1.81E+05
Ib/hr" 4.90E-04 4.92E-04 2. 13E-04 3.98E-04
Ib/ton pushedd 4.29E-06 4.44E-06 1. 94E-06 3.56E-06
Benzo(b) Fluoranthene
J.tgldscma 3.04 3.38 1.51 2.64
J.tg/hr> 3.03E+05 3.05E+05 1.47E+05 2.52E+05
Ib/hr" 6.68E-04 6.72E-04 3.24E-04 5.55E-04
Ib/ton pushedd 5.85E-06 6.07E-06 2.96E-06 4.96E-06
Benzo(k) Fluoranthene
J.tgldscm" 1.22 1.28 0.43 0.98
J.tg/hr> 1.2 I E+05 1.15E+05 0.42E+05 0.93E+05
Ib/hr" 2.67E-04 2.54E-04 0.93E-04 2.05E-04
Ib/ton pushedd 2.34E-06 2.29E-06 0.85E-06 1.83E-06
Benzo( e) Pyrene
J.tgldscma 0.81 0.78 0.20 0.60
J.tg/hr> 8.08E+04 7.07E+04 1.98E+04 5.7lE+04
Iblhr" 1. 78E-04 t.56E-04 0.44E-04 1.26E-04
Ib/ton pushedd 1.56E-06 1.41E-06 0.40E-06 1.12E-06
Benzo(a) Pyrpne
J.tgldscmD 0.25 0.18 0.07 0.17
J.tg/hr> 2.50E+04 1.60E+04 0.66E+04 1.59E+04
Ib/hr" 5.52E-05 3.53E-05 1.45E-05 3.50E-05
Ib/ton pushedd 4.84E-07 3.18E-07 1.33E-07 3.12E-07
Perylene
J.tgldscma 0.041 ND ND 0.014
J.tg/hr> 4,040 ND ND 1,347
Ib/hf 8.9IE-06 ND ND 2.97E-06
Ib/ton pushedd 7.80E-08 ND ND 2.60E-08
Indeno( I ,2,3-cd) Pyrene
J.tgldscm" 1.09 1.11 0.24 0.81
J.tg/hr> 1.09E+05 1.00E+05 0.23E+05 0.77E+05
Ib/hf 2.40E-04 2.2 I E-04 0.50E-04 1. 71 E-04
Ib/ton pushedd 2.11 E-06 2.00E-06 0.46E-06 t.52E-06
-------
TABLE 2.17 (concluded)
Run No. . B-1-429-1 8-1-429-2 B-1-429-3 Average
Dibenz(a,h) Anthracene
flgldscm" 0.45 0.45 0.13 0.34
flglhr> 4.44£+04 4.09£+04 1.22£+04 3.25E+04
Iblhr 9.80£-05 9.02E-05 2.69E-05 7.17E-05
Ib/ton pushedd 8.58£-07 8. 1 4E-07 2.45E-07 6.39E-07
Benzo(g,h,i) Perylene
flgldscm" 0.89 0.91 0.17 0.66
flglhr> 8.89£+04 8.18E+04 1.62E+04 6.23E+04
Iblhr 1.96£-04 1.80E-04 0.36E-04 1.3 7E-04
Ib/ton pushedd I. 72£-06 1.63E-06 0.33E-06 1.22E-06
"Micrograms per dry standard cubic meter.
bMicrograms per hour.
.Pounds per hour.
dPounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
drops (delta p), stack temperatures, and meter temperatures. All concentrations and emission rate
data in the tables are flow-weighted averages of both pushing and non-pushing periods.
2.3.2 Coke Oven Battery No.2 BaKhouse Outlet
The baghouse outlet was sampled simultaneously with the baghouse inlet. Table 2.18
summarizes the Method Method 429 sample times and flue gas parameters measured at the
baghouse outlet. The average sampling length of the three tests was 442 minutes. The average
sampling rate was 0.406 dscfm. Sampling volumes averaged 179.321 dscf or 5.078 dscm.
Flue gas temperatures averaged 135°F, with an average stack gas composition of 0.5%
CO2 and 20.2% 02' Moisture content averaged 2.6%. Flue gas volumetric flow rates averaged
101,785 acfm or 87,325 dscfm or 2,473 dscmm. The isokinetic sampling rate averaged 102.7%.
The baghouse outlet sampling location indicated a higher volume flowrate in comparison
to the baghouse inlet sampling location. This was due to a dilution air damper located on the
mass cooler remaining open at 10% of full opening during periods of non-pushing (roughly 13
minutes of a total of 15 minutes). The dilution air damper was fully open during pushing
operatons, or 2 minutes out of 15 minutes. This resulted in measureable air flow for the entire
length of the test during non-pushing operatons at the baghouse outlet that were greater than
flows measured at the baghouse inlet sampling location, which was located prior to the mass
cooler.
Table 2.19 summarizes the P AH concentrations and emission rates for the baghouse
outlet. Naphthalene and 2-methyl naphthalene were the compounds found in the highest
concentration of the 19 compounds analyzed for, at 1.67 ,ug/dscm and 0.38 ,ug/dscm,
respectively. All of the other compounds were detected in lower concentrations than naphthalene
and 2-methyl naphthalene.
The pushing operation necessitated adjusting sampling rates for maximum air flow during
the actual pushing of coke. The pushing process occurred roughly once every 15 minutes, and
lasted approximately two minutes. This required a maximum sample rate during the two minute
push and a much lower sample rate during the idle time. This sample approach was used for all
the isokinetic sample systems. The isokinetics were based on time weighted averages of pressure
drops (delta p), stack temperatures, and meter temperatures. All concentrations and emission rate
data in the tables are flow-weighted averages of both pushing and non-pushing periods.
2.3.3 Underfire Stack
The underfire or combustion stack was sampled over the course of the two days. Sample
runs were 180 minutes in length. Table 2.20 summarizes the CARB Method 429 sample times
and flue gas parameters measured at the underfire stack. The average sampling rate was 0.554
dscfm, with an average sampling volume of99.664 dscf or 2.822 dscm. Flue gas temperatures
averaged 447°F. Flue gas composition averaged 5.0% CO2 and 10.4% 02' with an average
-------
TABLE 2.18
PAH EMISSIONS SAMPLING AND FLUE
GAS PARAMETERS - BAGHOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I 8-0-429-1 I 8-0-429-2 I 8-0-429-3 I Average I
Date 08/11198 08/12198 08/13/98 -
TOtal Sampling Time, minutes 367 478 480 442
Coke Oven Pushes Per Test Run 46 47 42 45
Tons of Coke Pushed Per Hour 119.3 111.7 114.7 115.2
Avg. Sampling Rate, dscfm" 0.399 0.411 0.407 0.406
Sample Volume:
dscf> 146.291 196.291 195.382 179.321
dscm' 4.142 5.558 5.533 5.078
Avg. Flue Gas Temp, OF 132 137 136 135
O2 Con c., % by Volume 20.5 20.0 20.0 20.2
CO2 Conc., % by Volume 0.5 0.5 0.5 0.5
Moisture, % by Volume 2.9 2.8 2.3 2.6
Flue Gas Volumetric Flow Rate:
acfmd 99,693 105,790 99,873 101,785
dscfin" 85,504 90,478 85,994 87,325
dscmm' 2,421 2,562 2,435 2,473
Isokinetic Sampling Ratio, % 112.4 95.9 100.0 102.7
"Dry standard cubic feet per minute at 68°F (20°C) and I atm.
bDry standard cubic feet at 68°F (20°C) and 1 atm.
'Dry standard cubic meters at 68°F (20"C) and I atm.
dActual cubic feet per minute at flue gas conditions.
'Dry standard cubic meters per minute at 68°F (20°C) and 1 atm.
Note: AII data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.19
P AH CONCENTRATIONS AND EMISSION RATES
BAGHOUSE OUTLET
BETHLEHEM STEEL, CHESTERTON, INDIANA
Run No. B-0-429-1 B-0-429-2 B-0-429-3 Average
Date 08/11/98 08/12/98 08/13/98 -
Clock Time, 24 hr Clock 1037-1958 0928-1934 0840-1748 -
Naphthalene
~g/dscm. 1.76 1.58 1.66 1.67
~glhr> 2.55E+05 2.43E+05 2.42E+05 2.46E+05
Ib/hr" 5.63E-04 5.35E-04 5.34E-04 5A4E-04
Ib/ton pushedd 4.72E-06 4.79E-06 4.66E-06 4. 72E-06
2-Methyl naphthalene
~g/dscm' 0.38 0.45 0.31 0.38
~glhr> 5.565E+04 6.88E+04 4.45E+04 5.63E+04
Ib/hr" 1.23E-04 1.52E-04 0.98E-04 1.24E-04
Ib/ton pushedd 1.03E-06 1.36E-06 0.86E-06 1.08E-06
Acenaphthy lene
~g/dscm. 0.07 0.05 0.06 0.06
~glhr> 1.05E+04 0.77E+04 0.90E+04 0.91E+04
Ib/hr" 2.32E-05 1. 71E-05 1.98E-05 2.00E-05
Ib/ton pushedd 1.94E-07 1.53E-07 1.73E-07 1.73E-07
Acenaphthene
~g/dscm. 0.03 0.02 0.02 0.02
~glhr> 4,910 3,319 2,562 3,597
Ib/hr" 1.08E-05 0.73E-05 0.57E-05 0.79E-05
Ib/ton pushedd 9.08E-08 6.55E-08 4.92E-08 6.85E-08
Fluorene
~g/dscm. 0.07 0.05 0.04 0.05
~glhr> 1.05E+04 0.75E+04 0.53E+04 0.78E+04
Ib/hr" 2.32E-05 1.65E-05 1.l6E-05 1. 71E-05
Ib/ton pushedd 1.94E-07 1.47E-07 1.02E-07 1.48E-07
Phenanthrene
~g/dscm. 0.28 0.17 0.11 0.19
~glhr> 4. 12E+04 2.62E+04 1.60E+04 2.78E+04
Ib/hr" 9.09E-05 5.77E-05 3.53E-05 6.I3E-05
Ib/ton pushedd 7.62E-07 5.16E-07 3.08E-07 5.29E-07
Anthrancene
~g/dscm. 0.020 0.007 0.004 0.010
~glhr> 2,946 1,051 528 1,508
Ib/hr" 6.49E-06 2.32E-06 1.16E-06 3.33E-06
Ib/ton pushedd 5.45E-08 2.07E-08 1.02E-08 2.85E-08
Fluoranthene
~g/dscm. 0.12 0.04 0.03 0.06
~glhr> 1.68E+04 0.66E+04 OAOE+04 0.91E+04
Ib/hr" 3.71E-05 IA6E-05 0.87E-05 2.02E-05
Ib/ton pushedd 3.1IE-07 1.3IE-07 0.76E-07 1.73E-07
-------
TABLE 2.19 (continued)
.
Run No. B-0-429-1 B-0-429-2 8-0-429-3 Average
Pyrene
~g/dscm' 0.07 0.03 O.(J2 0.04
~g!hr> 9,819 4,978 2,535 5,778
Iblbr" 2.16E-05 1.1 OE-05 0.56E-05 1.27E-05
lb/ton pushedd I. 82E-07 0.98E-07 0.49E-07 1.1 OE-07
Benzo(a) Anthrancene 0.008
~g/dscm' 0.013 0.008 (Um
~g!hr> 1,929 1,189 607 1,242
Iblbr" 4.25E-06 2.62E-06 1.34E-06 2.74E-06
lb/ton pushedd 3.57E-08 2.35E-08 1.l7E-08 2.36E-08
Chrysene
~g/dscm' 0.027 0.025 0.011 0.021
~g!hr> 3,858 3,872 1,664 3,131
Iblbr" 8.50E-06 8.54E-06 3.67E-06 6.90E-06
Ib/ton pushedd 7. 13E-08 7.64E-08 3.20£-08 5.99E-08
Benzo(b) Fluoranthene
~g/dscm' 0.018 0.011 0.007 0.012
~g!hr> 2,560 1,742 1,004 1,769
lblbr" 5.64E-06 3.84E-06 2.2IE-06 3.90E-06
Ib/ton pushedd 4.73E-08 3.44E-08 1.93E-08 3.37E-08
Benzo(k) Fluoranthene "
~g/dscm' 0.016 0.006 0.005 0.009
~g!hr> 2,385 885 660 1,310
Iblbr" 5.26E-06 1.95E-06 1.46E-06 2.89E-06
Ib/lon pushedd 4.41E-08 1.75E-08 1.27E-08 2.47E-08
Benzo(e) Pyrene
~g/dscm' 0.012 0.006 0.004 0.007
~g!hr> 1,683 913 634 1,077
Iblhr" 3.7IE-06 2.0IE-06 1.40E-06 2.37E-06
Ib/lon pushedd 3.11 E-08 1.80E-08 1.22E-08 2.04E-08
Benzo(a) Pyrene
~g/dscm' 0.012 0.005 0.004 0.007
~g!hr> 1,683 747 528 986
Iblbr" 3.7IE-06 1.65E-06 1.J6E-06 2. 1 7E-06
Ib/lon pushedd 3.11E-08 1.47E-08 1.02E-08 1.87E-08
Perylene
~g/dscm' 0.003 0.002 ND 0.002
~g!hr> 386 360 ND 248
Iblbr" 8.50E-07 7.93E-07 ND 5.48E-07
Ib/lon pushedd 7. 13E-09 7.IOE-09 ND 4.74E-09
Indeno(I,2,3-cd) Pyrene
~g/dscm' 0.015 0.005 0.005 0.008
~g!hr> 2,209 830 660 1,233
Iblhr" 4.87E-06 1.83E-06 1.46E-06 2.72E-06
Ib/ton pushedd 4.08E-08 1.64E-08 1.27E-08 2.33E-08
-------
TABLE 2.19 (concluded)
Run No. B-0-429-1 B-0-429-2 B-0-429-3 Average
Dibenz(a,h) Anthracene
J.lg/dscm" 0.003 NO NO 0.001
J.lg/hr> 491 NO NO 163.3
Iblb... 1.08E-06 NO NO 0.36E-06
Ib/ton pushedd 9.08E-09 NO NO 3.03E-09
Benzo(g,h,i) Perylene
J.lg/dscm" 0.034 0.008 0.011 0.018
J.lg/hr> 4,910 1,245 1,690 2,615
Iblb... 1.08E-05 2.74E-06 3.73E-06 5.76E-06
Ib/ton pushedd 9.08E-08 2.46E-08 3.25E-08 4.93E-08
"Micrograms per dry standard cubic meter.
bMicrograms per hour.
'Pounds per hour.
dPounds per ton of coke pushed.
Note: All data presented are weighted averages based on both push and non-push periods.
-------
TABLE 2.20
P AH EMISSIONS SAMPLING AND FLUE GAS
PARAMETERS - UNDERFIRE STACK
BETHLEHEM STEEL,CHESTERTON, INDIANA
Run No. B-U-429-1 B-U-429-2 B-U-429-3 Average
Date 08/14/98 08/14/98 08/15/98 --
Total Sampling Time, minutes 180 180 180 180
Tons of Coal Charged Per Hour 159.0 ]42.3 ]57.1 ]52.8
Avg. Sampling Rate, dscfma 0.494 0.558 0.609 0.554
Sample Volume:
dscf' 88.949 100.360 109.683 99.664
dscm" 2.519 2.842 3.106 2.822
Avg. Flue Gas Temp, OF 453 448 440 447
O2 Conc., % by Volume 11.3 9.6 10.5 10.4
CO2 Conc., % by Volume 4.4 5.5 5.0 5.0
Moisture, % by Volume 17.3 21.1 14.1 17.5
Flue Gas Volumetric Flow Rate:
acfmd 173,886 201,774 ]71,478 ] 82,379
dscfma 82,595 92,035 85,4]2 86,681
dscmm" 2,339 2,606 2,419 2,455
Isokinetic Sampling Ratio, % 96.0 100.8 99.1 98.6
"Dry standard cubic feet per minute at 68°F (20°C) and I atm.
bDry standard cubic feet at 68°F (20°C) and I atm.
"Dry standard cubic meters at 68°F (20°C) and I atm.
dActual cubic feet per minute at flue gas conditions.
"Dry standard cubic meters per minute at 68°F (20°C) and I atm.
-------
moisture content of 17.5%. Flue gas volumetric flow rates averaged 182,379 acfm or 86,681
dscfm or 2,455 dscmm. Isokinetic sampling rate averaged 98.6%.
Table 2.21 summarizes the P AH concentrations and emission rates for the underfire
stack. All of the target P AH analytes were detected in the analyzed samples with the exception
ofperylene and dibenz(a,h) anthracene (for Run Nos. 2 and 3). Naphthalene,2-methyl
naphthalene and phenanthrene were present in the highest concentrations.
-------
TABLE 2.21
PAD CONCENTRATIONS AND EMISSION RATES
UNDERFIRE STACK
BETHLEHEM STEEL, CHESTERTON, INDIANA
I Run No. I B-U-429-1 I B-U-429-2 I B-U-429-3 I Average I
Date 08/14/98 08/14/98 08/15/98 -
ClOCk Time, 24 hr Clock 0921-1325 1441-1809 0838-1208 --
Naphthalene
Jig/dscma 4.16 10.73 57.79 24.22
Jiglhr" 5.83E+05 16.77E+05 83.86E+05 35.48E+05
Ib/hr" 1.29E-03 3.70E-03 18.5E-03 7.82E-03
Ib/ton chargedd 0.81E-05 2.60E-05 11.8E-05 5.06E-05
2-Methyl naphthalene
Jig/dscma 2.30 0.70 2.64 1.88
Jiglhr" 3.225E+05 1.09E+05 3.82E+05 2.71E+05
Ib/hr" 7.llE-04 2.41E-04 8.43E-04 5.98E-04
Ib/ton chargedd 4.47E-06 1.69E-06 5.37E-06 3.84E-06
Acenaphthylene
Jig/dscma 0.38 0.10 0.84 0.44
Jiglhr" 5.29E+04 1.60E+04 12.15E+04 6.35E+04
Ib/hr" 1. 17E-04 0.35E-04 2.68E-04 1.40E-04
Ib/ton chargedd 7.34E-07 2.47E-07 17.0E-07 8.95E-07
Acenaphthene
Jig/dscma 0.08 0.04 0.14 0.09
Jiglhr" 1.05E+04 0.61E+04 2.10E+04 1.26E+04
Ib/hr" 2.33E-05 1.33E-05 4.64E-05 2. 77E-05
Ib/ton chargedd 1.47E-07 0.94E-07 2.95E-07 1.79E-07
Fluorene
Jig/dscma 0.32 0.08 0.42 0.27
Jiglhr" 4.51E+04 1.27E+04 6.07E+04 3.95E+04
Ib/hr" 9.95E-05 2.79E-05 13.4E-05 8.7IE-05
Ib/ton chargedd 6.26E-07 1.96E-07 8.52E-07 5.58E-07
Phenanthrene
Jig/dscma 0.63 0.25 0.54 0.47
Jiglhr" 8.78E+04 3.88E+04 7. 83E+04 6.83E+04
Ib/hr" 1.94E-04 0.86E-04 1.73E-04 1.51 E-04
Ib/ton chargedd 1.22E-06 0.60E-06 I.I0E-06 0.97E-06
Anthrancene
Jig/dscma 0.02 0.01 0.03 0.02
Jiglhr" 2,841 1,100 4,018 2,653
Ib/hr" 6.26E-06 2.43E-06 8.86E-06 5.85E-06
Ib/ton chargedd 3.94E-08 1.70E-08 5.64E-08 3.76E-08
Fluoranthene
Jig/dscma 0.17 0.08 0.20 0.15
Jiglhr" 2.40E+04 1.21E+04 2.90E+04 2. 17E+04
Ib/hr" 5.28E-05 2.67E-05 6.39E-05 4.78E-05
Ib/ton chargedd 3.32E-07 I. 88E-07 4.06E-07 3.09E-07
-------
TABLE 2.21 (continued)
Run No. B-U-429-1 B-U-429-2 B-U-429-3 Average
Pyrene
~g/dscm. 0.07 0.03 0.07 0.06
~gIhr> 9,471 4,402 10,279 8,051
Iblhr" 2.09E-05 0.97E-05 2.27E-05 1. 78E-05
Ib/ton chargedd 1.31 E-07 0.68E-07 1.44E-07 1.15E-07
Benzo(a) Anthrancene
~g/dscm. 0.02 0.01 0.02 0.02
~gIhr> 2,507 1,376 3,364 2,416
Iblhr" 5.53E-06 3.03E-06 7,42E-06 5.33E-06
Ib/ton chargedd 3.48E08 2.l3E-08 4.72E-08 3,44E-08
Chrysene
~g/dscm. 0.05 0.02 0.05 0.04
~gIhr> 6,686 3,246 7,476 5,803
Iblhr" 1.47E-05 0.72E-05 1.65E-05 1.28E-05
Ib/ton chargedd 9.27E-08 5.03E-08 10.5E-08 8.26E-08
Benzo(b) Fluoranthene
~g/dscm' 0.03 0.02 0.02 0.02
~g/hr" 4,234 2,476 2,990 3,234
Iblhr" 9.33E-06 5,46E-06 6.59E-06 7. 13E-06
Ib/ton chargedd 5.87E-08 3.84E-08 4.20E-08 4.63E-08
Benzo(k) Fluoranthene
~g/dscm' 0.02 0.01 0.01 0.01
~gIhr" 2,786 1,706 1,822 2,105
Ib/hr" 6.14E-06 3.76E-06 4.02E-06 4.64E-06
Ib/ton chargedd 3.86E-08 2.64E-08 2.56E-08 3.02E-08
Benzo( e) Pyrene
~g/dscm' 0.02 0.01 0.01 0.01
~gIhr" 2,340 1,761 1,589 1,896
Iblhr" 5.16E-06 3.88E-06 3.50E-06 4. I 8E-06
Ib/ton chargedd 3.25E-08 2.73E-08 2.23E-08 2.73E-08
Benzo(a) Pyrene
~g/dscm' 0.02 0.01 0.01 0.01
~gIhr" 2,619 1,321 1,495 1,811
Iblhr" 5.77E-06 2.9 I E-06 3.30E-06 3.99E-06
Ib/ton chargedd 3.63E-08 2.05E-08 2.IOE-08 2.59E-08
Perylene
~gldscm' 0.01 NO NO 0.00
~gIhr" 669 NO NO 223
Ib/hr" 1.47E-06 NO NO 4.9IE-07
Ib/ton chargedd 9.27E-09 NO ND 3.09E-09
Indeno( I ,2,3-cd) Pyrene
~gldscm' 0.017 0.011 0.011 0.013
~gIhr" 2,451 1,761 1,635 1,949
Ib/hr' 5,40E-06 3.88E-06 3.62E-06 4.30E-06
Ib/ton chargedd 3.40E-08 2.73E-08 2.29E-08 2.8IE-08
-------
TABLE 2.21 (concluded)
Run No. B-U-429-i B-U-429-2 B-U-429-3 Average
Oibenz(a,h) Anthracene
J.tg/dscma 0.005 NO NO 0.002
J.tg/hr" 669 NO NO 223
Iblhr" 1.47E-06 NO NO 4.91E-07
Ib/ton chargedd 9.27E-09 NO NO 3.09E-09
Benzo(g,h,i) Perylene
J.tg/dscma 0.03 0.03 0.02 0.03
J.tg/hr" 4,513 4,292 2,944 3,916
Iblhr" 9.95E-06 9.46E-06 6.49E-06 8.63E-06
Ib/ton chargedd 6.26E-08 6.65E-08 4.13E-08 5.68E-08
"Micrograms per dry standard cubic meter.
bMicrograms per hour.
.Pounds per hour.
dPounds per ton of coal charged.
-------
3.0 PROCESS AND CONTROL EQUIPMENT OPERATION
3.1
INTRODUCTION
Bethlehem Steel Corporation produces coke from two 6-meter coke oven batteries at their
Bums Harbor facility. Both batteries have 82 ovens and a gross coking time of 18 hours. They
are positioned end-to-end and served by a common rail.
Battery No.1 is a McKee-Otto design which began operation in 1969 and was rebuilt
from the pad up in 1983. The battery uses a combination of50% (by volume) blast furnace gas
(BFG) and 50% (by volume) coke oven gas (COG) to fuel combustion in a twin flue underjet
system. Pushing emissions are captured by a Minister Stein hood and vented via a fixed duct to a
venturi scrubber.
Battery No.2 is a Still/Otto design which began operation in 1972 and was rebuilt from
the pad up in 1994. The battery uses 100% COG to fuel combustion in an underjet system.
Pushing emissions are captured by a Minister Stein hood and vented via a fixed duct to a
baghouse.
Both batteries operate state-of-the-art Minister Stein capture systems. Battery No.2 was
selected for testing due to several factors. Baghouses are more representative of the control
devices used at coke ovens than venturi scrubbers; 45 batteries currently in operation use
baghouses for pushing emission control, and only 10 batteries use wet scrubbers. Also, Battery
No.2 operates on 100% COG, which is more common than a blend of COG and BFG.
3.2
PROCESS DESCRIPTION
3.2.1 Pushing
The pushing sequence used at Bums Harbor is the "Koppers minus 10" system, in which
ovens 1, 11,21... are pushed, followed by ovens 3, 13,23.... The even-numbered ovens, 2, 22,
32...through 8, 18, 28...are pushed after the odd-numbered ovens. Since there are no zeros in any
of the oven numbers, the battery's 82 ovens number from 1 to 92. The number of each oven in
Battery No.2 is preceded by a "2" (i.e. ovens 1, 11,21 would be referred to as 21, 211, 221).
An average of 31.5 tons of coal is charged into each oven, and an average of 23.8 tons of
coke is produced per coking cycle. The battery is operated 24 hours a day, 7 days a week;
-------
however, charging and pushing are stopped for 1 to 1.5 hours once a week for battery
maintenance and repairs.
.
Pushing emissions are captured by a moveable hood attached to a fixed duct system. The
hood connects with the hooded coke guide and covers the quench car during pushing. When the
dampers are open, the duct is open to the baghouse where a fan evacuates emissions from the
hood. The hood in place at Battery No.2 is a modified Minister Stein design; a tripper car
moves under the belt which seals the top of the duct; the tripper car and fume hood are connected
by a telescoping duct (see Figure 3.1).
1
i
II
Stack sampling location
Emergency flap
Isolallon valve
f"" ....D~~i.".1 ...too.g.. ...-oo"
6-Module Baghouse
Stack
Air dilution damper
Fume
Hood
Coke
Enclosed 0
Coke yens
Guide
Baghouse Inlet
sampling location
\
Minister Stein
Fume Duct
"One-Spot" Quench Car
Dust
conveyor
Dust
boxes
Figure 3.1 Schematic of Pushing Emission Control for Battery No.2
Typically three ovens in advance of the next oven to be pushed are dampered off the
collection main. The standpipe cap and mini-standpipe cap are then opened. Ovens are
dampered off for approximately 30 minutes prior to being pushed. Just prior to pushing, the door
machine removes the coke side door and positions the coke guide; the pusher machine removes
the pusher side door and aligns the pushing ram. The quench car is moved into position beneath
the hood. The door machine operator then opens the hood isolation damper, and the baghouse
damper is opened. A push, from the time the pushing ram starts to move until the quench car
-------
reaches the quench tower, takes approximately 75 seconds. A push typically occurs every 10 to
15 minutes. After an oven is pushed, the door jambs are automatically cleaned on both the
pusher and coke sides, and the doors are replaced. The ovens are charged in the order in which
they were pushed. Typical coking time (from coal charge to coke push) is 18 hours.
Pushing emissions captured by the hood travel through the fixed duct to a 6-compartment
baghouse. The baghouse was installed in 1994 and has a volumetric flow rate of 205,000 to
216,000 acfm. Of the 6 baghouse compartments, at least 4 are always on-line; one is usually out
of service for cleaning, and one can be out of service for maintenance at any given time. Each
compartment houses 352 12-foot-Iong Nomex bags. The bags are precoated with 1.5 pounds of
lime per pulse jet cleaning cycle. A total of3,100 pounds oflime is injected into the baghouse
per day. Pressure drop (delta p) is measured across the baghouse rather than across individual
compartments, and ranges from 4.4 to 8.8 inches of water. Air temperature in the baghouse
ranges from 300°F at the inlet to 140 - 160°F at the outlet. The gross filtering area is 40,440 ft2,
the net filtering area (with one module offline for cleaning) is 33,700 ft2, and the net air-to-cloth
ratio is 5.94 acfm/ft2.
3.2.2 Underfiring
The combustion, or underfiring, system regulates COG, air, and waste gas. Prior to
being used for combustion, raw COG is processed in a by-product recovery plant where tar and
naphthalene are removed and ammonia is recovered as ammonium sulfate. Approximately 30%
of the "clean" gas is used for underfiring, and the balance is used in other parts of the Burns
Harbor facility. COG is not desulfurized prior to being used at the coke ovens.
Battery No.2 is equipped with an underjet combustion system with double pair flues that
uses multiple staged air and is fueled solely by COG. Combination air inlet/waste heat boxes are
located on the coke side of the battery. The average flue temperature is 2,400°F. Combustion of
COG and air takes place in every other pair of heating flues. Waste gas is formed as a product of
combustion and flows downward in every other pair of heating flues through the regenerators
and out the battery stack. The battery "reverses" every 20 minutes: waste heat flues become
combustion flues and combustion flues become waste heat flues. Two channels carry waste gas
from the battery to the combustion stack. They are referred to as the North tunnel stack and
South tunnel stack, and both discharge to the combustion stack.
Several factors can affect emissions from the combustion stack, including incomplete
combustion in the flues or cracks in the brickwork between an oven chamber and flue.
Incomplete combustion is typically the result of excess gas and/or insufficient air in the system.
Excess emissions from damaged brickwork or overly decarbonized ovens is most notable just
after an oven is charged because gases from combusted coal dust are forced through cracks
during charging.
The Bums Harbor facility uses state-of-the-art instrumentation and monitoring to
maintain efficient combustion. This includes an O2 monitor, a continuous opacity monitor
(COM), and a waste heat temperature monitor. The COM is equipped to alarm when opacity
-------
exceeds the state limit of20% for Battery No.2. Heating personnel then check the most recently
charged oven for wall leakage.
3.3
PROCESS AND CONTROL DEVICE MONITORING
3.3.1 Pushing
Several parameters were monitored during each test run. Process parameters monitored
included the identification of each oven being pushed, the total quantity of coal charged to each
oven that was pushed during each run, and the total quantity of coke pushed during each run.
Control parameters monitored included fan amps, pressure drop, and inlet pressure. The
baghouse is controlled by a programmable logic controller (PLC) which continuously sends
readings of these parameters to several computer terminals around the plant. A summary of the
parameter values recorded during testing is presented in Table 3.1. A more detailed summary
(one reading during each push) is presented in Appendix A.
Visual observations of pushes were made during all three test runs to assess capture
efficiency ofthe hood and to note any differences in uncontrolled emissions. Excellent capture
of pushing emissions by the hood system resulted in relatively low fugitive emissions during
most pushes, which includes travel to the quench tower. After a few pushes, thick, dark
emissions were observed from the door area of the oven; however, the quench car usually
remained under the hood for a longer period of time after these pushes, and fugitive emissions
from the quench car remained low.
TABLE 3.1
SUMMARY OF PUSHING PROCESS AND CONTROL DEVICE PARAMETERS
~eter: Run No.1 Run No.2 Run No.3
Average Coal/Charge (tons) 32.5 32.2 32.8
Average Coking Time (hours) 18.6 17.9 17.8
Average Fan Amps 47 47 46
Average Delta P (in. H20) 5.8 6 5.8
Average Inlet Pressure (in. H20) 1.4 1 1.4
Average Damper Opening (%) 518 528 528
Total Coal Charged (tons) 1,494 1,515 1,671
Total Coke Pushed (tons) 1,115 1,128 1,244
8 Damper openings are controlled to provide at least 200,000 acfm during the push.
-------
3.3.2 Underfiring
Control parameters monitored during combustion stack testing included: opacity, stack
draft, percent excess oxygen, fuel gas flow rate and waste heat temperature. All of these
parameters are continuously monitored, and the values are sent to computer terminals at several
sites around the plant. COM readings are sent to computer terminals as well as a traditional chart
recorder which logs 6-minute averages. Opacity from the stack is also read manually three times
per week by a certified opacity reader. Process parameters monitored during testing included the
number of each oven charged and the quantities of coal charged and coke produced during each
run.
The data presented is primarily from continuous readings logged by the plant computer
system. Opacity data is in the fonn of 6-minute averages from the plant's COM chart recorder.
Waste heat temperature, stack draft and excess oxygen are continuously monitored in both the
North tunnel stack and South tunnel stack, both of which empty into the battery's combustion
stack. Control parameter values during testing are summarized in Tables 3.2a through 3.2c.
For all three test runs, stack draft ranged from 17.1 to 23.5 millimeters of water, excess
oxygen ranged from 3.5 to 22%, and the waste heat temperature ranged from 438 to 472 of. The
amount of dry coal charged per oven ranged from 31.8 to 33.3 tons. The average amount of coke
produced per oven was 24.4 tons. A total of 481 tons of coke was produced from the ovens
charged during Run No.1, 365 tons during Run No.2, and 414 tons during Run No.3, for a total
of 1,260 tons of coke produced during all three test runs. COM data indicate that 6-minute
averages for opacity ranged from approximately 3 to 7% during testing (see Figures 3.2 and 3.3
in Appendix A, respectively).
-------
TABLE 3.2A
COMBUSTION STACK PARAMETERS TEST RUN NO.1, 8/14/98
Underfire Gas Stack Excess O2 (%) Stack Draft (mm H20) Stack Temperature eF)
Time Oven Dry Coal Flow Rate
Weight (Ibs) (kscth8) North South North South North South
9:25:00 221 64,446 679 5.4 6 23.2 23.2 440 432
9:35:00 231 63,605 671 5.4 6 23.2 23 448 445
9:47:00 241 64,072 625 9 6 23.1 23.1 449 433
9:58:00 251 64,446 762 18 --- --- 19.3 466 441
10:08:00 261 64,633 678 5.6 6.6 23.4 23 441 436
10: 18:00 271 64,539 764 18 --- --- 18.8 449 448
10:27:00 281 64,259 637 8.2 6.2 22.9 22.9 450 433
10:43:00 291 65,940 672 5.1 5.8 23.1 22.9 443 433
10:57:00 203 64,726 668 5 5.8 23.3 23.2 450 448
11:07:00 213 64,633 637 8.3 6.3 23.4 23.2 451 434
11:17:00 223 64,726 667 5.7 5.8 23 22.8 472 442
11:38:00 233 65,847 767 19 --- -- 19 447 448
11 :47:00 243 63,886 630 8 5.8 23.1 22.9 451 434
11 :57:00 253 64,446 673 5.5 6 23.2 23 471 443
12:07:00 263 64,633 643 8 5.7 23.2 22.8 440 436
12:30:00 273 64,726 670 4.8 5.4 23.2 23.3 457 436
12:39:00 283 64,446 687 3.6 4.8 22.3 22.1 460 439
12:50:00 205 64,820 670 5.3 5.9 23.1 23.1 443 440
13:01:00 215 65,193 667 5.3 5.8 22.5 22.8 444 439
13:11:00 225 65 567 671 5.2 5.5 23.5 23.1 458 437
a 1,000 standard cubic feet per hour
-------
TABLE 3.28
COMBUSTION STACK PARAMETERS: TEST RUN NO.2, 8/14/98
Underflre Gas Stack Excess O2 (%) Stack Draft (mm H20) Stack Temperature COF)
Time Oven Dry Coal Flow Rate
Weight (Ibs) (kscfh8) North South North South North South
15:19:00 207 65,660 684 4.4 5.3 22.3 22.1 463 439
15:31:00 217 65,193 681 6.1 6 23.3 23.1 445 440
15:40:00 227 66,127 659 6.2 6.1 22.5 22.7 444 440
15:50:00 237 64,633 678 5.6 5.8 23.3 23.2 456 436
16:02:00 247 65,660 667 5. I 5.5 23 23.1 448 433
16:13:00 257 63,886 668 5.3 5.9 23.2 23.2 448 442
16:22:00 267 65,940 661 5.5 5.9 23 23 446 437
16:32:00 277 65,380 666 5. I 5.1 23.3 23.3 464 436
16:44:00 287 64,820 655 5.2 5.7 23.5 23.4 445 433
17:03:00 209 66,407 664 5.2 5.6 23.4 23.2 447 437
17:11:00 219 65,380 674 5.2 5.6 23.3 23.1 462 437
17:20:00 239 66,594 669 5.4 5.7 22.7 22.7 458 436
17:35:00 239 64,353 665 4.7 5.4 23.4 23.3 453 447
17:44:00 249 65,940 667 5.6 5.9 22.9 22.9 451 435
18:00:00 259 65 287 671 4.7 5.4 22.6 22.5 462 435
a 1,000 standard cubic feet per hour
-------
TABLE 3.2C
COMBUSTION STACK PARAMETERS: TEST RUN NO.3, 8/15/98
UnderfIre Gas Stack Excess O2 (%) Stack Draft (mm H20) Stack Temperature eF)
Time Oven Dry Coal Flow Rate
Weight (Ibs) (kscfh") North South North South North South
8:39:00 275 65,261 679 3.5 4.9 22.1 22.2 458 436
8:50:00 285 64,705 648 5.9 6.3 23.2 23.2 438 436
9:02:00 207 64,334 649 6.1 6 23.1 23.2 441 433
9:13:00 217 65,817 635 5.8 5.9 23.3 23.1 460 436
9:23:00 227 64,334 627 6.2 6.5 23.2 23.1 440 430
9:33:00 237 65,632 629 5.8 6.1 23.4 23.2 441 440
9:43:00 247 63,963 637 6.7 6.4 22.9 23 442 433
10:04:00 257 65,354 639 6 6.4 23.1 23.3 439 430
10:14:00 267 65,354 645 5.8 6.2 23.2 23 441 441
10:24:00 277 63,963 633 5.9 6.5 23 23 443 432
10:34:00 287 65,632 644 6.3 7.4 23.2 23.3 462 438
10:58:00 209 64,519 714 22 --- --- 17.7 446 446
11 :08:00 219 63,500 629 6.3 7.8 23.3 23.2 450 432
11:18:00 229 65,817 767 22 --- --- 18.4 468 441
II :27:00 239 64,056 598 8.6 6.2 23.2 23.1 438 433
11:37:00 249 64,612 640 6.2 6.1 23.2 23.1 447 446
11 :57:00 259 63,500 646 5.6 5.8 22.8 22.6 469 441
a 1,000 standard cubic feet per hour
-------
4.0 SAMPLING LOCATIONS
Source sampling was conducted at Coke Oven Battery No.2 at the Bethlehem Steel
Corporation's Burns Harbor Division in Chesterton, Indiana. Prior to sampling all locations
were checked for the presence of non-parallel or cyclonic flow as outlined in Section 2.4 of EP A
Method 1. At all three sampling locations, the average rotation angle for a null reading was well
below the EP A Method 1 criteria of 200. Therefore, sampling at each location was conducted
without site modifications. Brief descriptions and schematic diagrams of the sampling locations
are presented below.
4.1
COKE OVEN BATTERY NO.2
4.1.1 Baghouse Inlet
The baghouse inlet test location was located in a 114-inch inside diameter (ID) round
horizontal duct which leads from the coke oven pushing operation to the inlet of the baghouse.
This location was upstream of the mass cooler and dilution air damper (see Figure 3.1 in Section
3.2.1). Four sampling ports were positioned as shown in Figure 4.1. The two upper sample ports
were used for EP A Method 315 and CARB Method 429 isokinetic sampling. One of the other
two sample ports was used for the NIOSH Method 5506 sampling. This location was 572 inches
(5.0 duct diameters) downstream of the nearest flow disturbance (450 elbow) and 181 inches (1.6
duct diameters) upstream of the nearest flow disturbance (450 elbow). According to EPA
Method 1 criteria, this location required 20 sample traverse points, 10 along each of two
perpendicular diameters. The results of the EPA Method 1 calculations and the locations of the
traverse points are presented in Figure 4.2.
4.1.2 Baghouse Outlet
The baghouse outlet sampling location was located in a 108-inch ID round vertical stack
which was downstream of the baghouse. Four sampling ports were positioned as shown in
Figure 4.3. On one of the four ports, a longer coupling was required to in order to clear an
obstacle. Therefore, two sets of sample traverse points were required. All four ports were used
for the EP A method 315 and CARB Method 429 isokinetic sampling. The NIOSH Method
5506 sampling was conducted in one of the four ports not being used for the isokinetic sampling.
This location was 660 inches (6.1 stack diameters) downstream of the nearest flow disturbance
(baghouse fans) and 330 inches (3.1 stack diameters) upstream of the atmosphere. According to
EP A Method 1 criteria, this location required 16 sample traverse points, four in each of the four
sample ports. The results of the EPA Method 1 calculations and the locations of the traverse
points are presented in Figure 4.4.
-------
572"
Section A
Figure 4.1 Baghouse Inlet Sample Location, Bethlehem Steel Corp., Chesterton, Indiana
-------
Circular Stack Method 1 Calculation Results
Date: 11/03/98 Time:14:03:30
Bethlehem Steel, Bums Harbor
BH Inlet
Coke Oven 2, Baghouse Inlet
11/02/98
F. Meadows
Facility:
Source 10:
Source Name:
Date:
Calculated By:
%t11;~lli~ii\ji;~1nm$.w~i%w;i~itTm~i~iM~~wJ¥i~!~1$~mWJmiwC"':'~.~~:. :.~it~~'t~~~~:.;;~- ~;"~~¥t~i':.' ... .
Traverse Point Type:
Inside of far wall to outside of nipple:
Nipple Length:
Distance from Upstream Disturbance:
Distance from Downstream Disturbance:
Number of ports:
Sample - M5
120 1/4 Onches)
6 1/4 (Inches)
572 even (Inches)
181 even (Inches)
2 ports at 90 degrees
Inside Diameter.
Upstream Duct Diameters:
Downstream Duct Diameters:
Mininum Traverse Points:
114.0000
5.01
1.58
20
(Inches)
215/16 6 1/4 9 3/16
9 3/8 6 1/4 15 5/8
16 5/8 6 1/4 22 7/8
25 3/4 6 1/4 32 even
39 even 6 1/4 45 1/4
75 even 6 1/4 81 1/4
88 1/4 6 1/4 94 1/2
97 3/8 6 1/4 103 5/8
1 04 5/8 6 1/4 11 0 7/8
111 1/16 6 1/4 117 5/16
Figure 4.2 Baghouse Inlet Traverse Point Locations, Bethlehem Steel Corp.,
Chesterton, Indiana
-------
108"
A
A
330"
Section A
660"
From
Baghouse
Figure 4.3 Baghouse Outlet Sample Location, Bethlehem Steel Corp., Chesterton,
Indiana
-------
Circular Stack Method 1 Calculation Results
Date: 11/09/98 Time: 12:45:09
Bethlehem Steel, Bums Harbor
BH Outlet
Coke Oven 2, Baghouse Outlet
11/09/98
F. Meadows
Facility:
Source 10:
Source Name:
Date:
Calculated By:
Traverse Point Type:
Inside of far wall to outside of nipple:
Nipple Length:
Distance from Upstream Disturbance:
Distance from Downstream Disturbance:
Number of ports:
Sample - M5
116 even (Inches)
8 even (Inches)
660 even (Inches)
330 even (Inches)
4 ports at 90 degrees
~~~~~~4~~~~~~~1~~W~~*~~~ .~.~ ..'~ :~~~.._..,.
Inside Diameter:
Upstream Duct Diameters:
Downstream Duct Diameters:
Mininum Traverse Points:
108
6.11
3.05
16
(Inches)
-"h
1 08 even
1 08 even
1 08 even
1 08 even
3 7/16
11 5/16
20 15/16
34 7/8
8 even
8 even
8 even
8 even
11 7/16
19 5/16
2815/16
42 7/8
Traverse Point Type:
Inside of far wall to outside of nipple:
Nipple Length:
Distance from Upstream Disturbance:
Distance from Downstream Disturbance:
Number of ports:
Sample - M5
125 1/2 (Inches)
17 1/2 (Inches)
660 even (Inches)
330 even (Inches)
4 ports at 90 degrees
0.032
0.105
0.194
0.323
3 7/16
11 5/16
2015/16
34 7/8
17 1/2
17 1/2
17 1/2
171/2
Figure 4.4 Baghouse Outlet. Traverse Point Locations, Bethlehem Steel Corp.,
Chesterton, Indiana
-------
4.1.3 Combustion (Underfire) Stack
The combustion (lffiderfire) stack test location was located in a 177-inch ID round
vertical stack. The stack is a double wall stack with a slight decreasing diameter with the
increase of vertical stack height. There were no elbows or bends in the stack to affect the
direction of air flow. Four sampling ports were positioned as shown in Figure 4.5. All four
sample ports were used for the EP A Method 315 and CARB Method 429 isokinetic sampling.
The NIOSH Method 5506 sampling was conducted in one of the four ports not being used for the
isokinetic sampling. According to EP A Method I criteria, this location required 12 sample
traverse points, three in each of the four ports. The results of the EP A Method 1 calculations and
the locations of the traverse points are presented in Figure 4.6.
-------
177"
1764"
Section A
A
A
1320"
Figure 4.5 Combustion (Underfire) Sampling Location, Bethlehem Steel Corp.,
Chesterton, Indiana
-------
Circular Stack Method 1 Calculation Results
Date: 11/02198 Time: 16:24:18
F aGility:
Source 10:
Source Name:
Date:
Calculated By:
Bethlehem Steel, Bums Harbor
U F Stack
Underfire Stack
11/02/98
F. Meadows
;!::;Ii;::::;::;i[;~:::~i;~jj::::;W;\::;;t:::;;::::tim~i;@i)mt:@\1;;*ji;Mii;;1~m@1i::;mm::;ifJo.pijt:Yim~;i;i(im;lli1;jii;~~!Mmffi.~1]f&f.*1@ffuw#l;i~i*ij;i;1fi
Traverse Point Type:
Inside of far wall to outside of nipple:
Nipple Length:
Distance from Upstream Disturbance:
Distance from Downstream Disturbance:
Number of ports:
Sample - M5
224 even (inches)
47 even (inches)
1320 even (inches)
1764 even (inches)
2 ports at 90 degrees
Inside Diameter:
Upstream Duct Diameters:
Downstream Duct Diameters:
Mininum Traverse Points:
@hni::::~~@;j;::;)!iin:~@Hn:I:jI:;::;;:::;Iji:::M~~ii::iiiii:~::t@mm~}miim;iE~,;in~t~~l:v~@iii@;iI@ii;;i;ji@ii;ilii[i::::Ii~:::;;imt:ii::ii;R:~~~W:;im;;::@I~~~)i0m@l~ji\~I;
177 (inches)
7.45
9.96
12
t1:III'IIl{...__a-
1 0 044 1 77 even 7 1 3/1 6 47 even 54 1 3/1 6
2 0 1 46 1 77 even 25 1 3/1 6 47 even 72 1 3/1 6
3 0 296 1 77 eve n 52 3/8 47 even 99 3/8
4 0 704 1 77 even 1 24 5/8 47 even 1 7 1 5/8
5 0 854 1 77 even 1 5 1 3/1 6 47 even 1 98 3/1 6
6 0 956 1 77 eve n 1 69 3/1 6 47 even 2 1 6 3/1 6
Figure 4.6 Method 1 Calculation Sheet, Combustion Stack, Bethlehem Steel Corp.,
Chesterton, Indiana
-------
5.0 SAMPLING AND ANALYTICAL PROCEDURES
Source sampling was performed at the locations described in the preceding section to
determine the concentrations and mass emission rates of filterable particulate matter (PM),
methylene chloride extractable matter (MCEM), and polycyclic aromatic hydrocarbons (PARs).
In addition, once the MCEM analyses were completed, the MCEM samples were also analyzed
to determine 17 trace metals. Three test runs were conducted at each of the locations (the
baghouse inlet and outlet testing was conducted simultaneously). The underfire stack test was
conducted separately from the baghouse test.
Each test run covered approximately a 10-hour period for the baghouse sampling, one test
run per day. Due to the frequency and duration of each coke oven pushing event, isokinetic
sampling was conducted as follows:
.
During each oven push, a maximum air flow to and from the baghouse is achieved
when dampers are opened for a period of approximately 90 seconds, resulting in
significantly higher stack gas differential pressures than at idle periods. Maximum air
volumes were metered through the sample trains during each oven push. During idle
periods, isokinetic sampling was maintained at a much lower sampling rate. The
dampers on the baghouse remain open at approximately 10% during idle periods.
Sampling on the underfire stack resulted in test runs of approximately three hours
duration. Testing was conducted over two days.
In Table 5.1, the parameters measured, the sampling methods, the number of tests
performed, and the duration of each test are summarized. Brief descriptions of the sampling and
analysis procedures used are presented below.
5.1
LOCATION OF MEASUREMENT SITES AND SAMPLENELOCITY
TRAVERSE POINTS
EP A Method 1, "Sample and Velocity Traverses for Stationary Sources," was used to
establish velocity and sample traverse point locations. The process ductwork, and the locations
of measurement sites and sample traverse points are discussed in Section 4.0 of this document.
,
-------
TABLE 5.1
SUMMARY. OF SAMPLING LOCATIONS, TEST PARAMETERS,
SAMPLING METHODS, AND NUMBER AND DURATION OF TESTS,
BETHLEHEM STEEL CORPORATION, CHESTERTON, INDIANA
Sampling Number Avg. Duration
Location Test Parameter Sampling Methods of Tests Per Test (min.)
Coke Oven Exhaust gas flow rate EP A Method 2 3 482
Battery No.2 CO2 and O2 content EPA Method 3B 3 484
Baghouse Moisture content EP A Method 4 3 484
Inlet ParticulateIMCEMlmetals EPA Method 315 3 484
PAHs. CARB Method 429 3 432
NIOSH Method 5506 3 424
Coke Oven Exhaust gas flow rate EP A Method 2 3 442
Battery No.2 CO2 and O2 content EP A Method 3B 3 442
Baghouse Moisture content EP A Method 4 3 442
Outlet Particulate/MCEMlmetals EPA Method 315 3 443
PAHs CARB Method 429 3 442
NIOSH Method 5506 3 414
Underfire Exhaust gas flow rate EP A Method 2 3 180
Stack CO2 and O2 content EPA Method 3B 3 180
Moisture content EP A Method 4 3 180
ParticulateIMCEMlmetals EPA Method 315 3 182
PAHs CARB Method 429 3 180
NIOSH Method 5506 3 165
-------
5.2
DETERMINATION OF STACK GAS VOLUMETRIC FLOW RATE
EP A Method 2, "Determination of Stack Gas Velocity and Volumetric Flow Rate (Type
S Pitot Tube)," was used to determine exhaust gas velocity. A Type S Pitot tube, constructed
according to Method 2 criteria and having an assigned coefficient of 0.84, is connected to an
inclined-vertical manometer. The pitot tube was inserted into the duct and the velocity pressure
(delta p) was recorded at each traverse point. The effluent gas temperature was also recorded at
each traverse point using a Type K thermocouple. The average exhaust gas velocity was
calculated from the average square roots of the velocity pressure, average exhaust gas
. temperature, exhaust gas molecular weight, and absolute stack pressure. The baghouse sampling
required using time weighted averages of velocity pressure, exhaust gas temperatures, and meter
temperatures to calculate volumetric flow rates. The volumetric flow rate is the product of
velocity and the stack cross-sectional area of the duct at the sampling location.
5.3
DETERMINATION OF STACK GAS EMISSION RATE CORRECTION
FACTORS, DRY MOLECULAR WEIGHT, AND EXCESS AIR
EPA Method 3B, "Gas Analysis for the Determination of Emission Rate Correction
Factor or Excess Air," was used to determine stack gas emission rate correction factors and
molecular weight. Bag samples were collected and analyzed for each measurement run using an
Orsat@ combustion gas analyzer which read :f: 0.1 % concentrations of carbon dioxide and
oxygen. One integrated bag sample was collected per each 60 minutes of sampling time at the
baghouse inlet and outlet, as well as the underfire stack.
5.4
DETERMINATION OF STACK GAS MOISTURE CONTENT
EPA Method 4, "Determination of Moisture Content in Stack Gases," was used to
determine the flue gas moisture content. EP A Method 4 was performed in conjunction with each
EP A Method 315 and CARB Method 429 test run. Integrated, multi-point, isokinetic sampling
was performed. Condensed moisture was determined by recording pre-test and post-test weights
of the impingers, reagents, and silica gel. XAD@.2 adsorbent traps were also pre- and post-test
weighed and included in the CARB Method 429 moisture determination.
5.5
DETERMINATION OF PARTICULATE MATTERIMETHYLENE CHLORIDE
EXTRACTABLE MATTERIMETALS
EP A Method 315, "Determination of Particulate and Methylene Chloride Extractable
Matter (MCEM) from Selected Sources at Primary Aluminum Production Facilities" was used to
determine PM, MCEM, and metals.
This method is applicable for the simultaneous determination of PM and MCEM. PM
and MCEM were withdrawn isokinetically from the source. PM was collected in the probe and
-------
on a tared glass fiber filter at 248 ::I: 25 of. A schematic of the MCEM sample train is shown in
Figure 5.1. The sampling train consisted of a glass nozzle, a heated glass lined probe, a heated
tared quartz fiber filter, two impingers each containing 100 milliliters of Type II distilled, de-
ionized water, an empty impinger, and an impinger containing approximately 250 grams of
indicating silica gel. The glass nozzle was joined to the probe using a TeflonGiJ-coated stainless
steel union and Teflonil)or graphite ferrules. A Teflonil) liner was used at the baghouse inlet due
to the overall length (greater than 10') of the probe assembly and poor port access. Due to
particulate loading, filters were replaced at the baghouse inlet at port changes. At the baghouse
inlet sampling location, an unheated flexible Teflonil) sample line was used between the filter exit
and impinger inlet. This modification was necessitated by poor access to the sample ports. ERG
submitted tared, quartz fiber filters to PES for sampling, which were returned after the test
program for PM and MCEM analysis. The PM mass was determined gravimetrically after
removal of combined water. MCEM was then determined by performing a methylene chloride
extraction of the sample train fractions and determining the residue gravimetrically after
evaporating the solvents.
Following completion of the MCEM analyses by ERG, the PM and MCEM samples were
submitted to F AL where they were digested and analyzed for the presence of 17 trace metals
using three different analytical techniques. This analysis provided an approximation of the trace
metals present in the stack gases. The target metals include antimony (Sb), arsenic (As), barium
(Ba), beryllium (Be), cadmium (Cd), chromium (Cr), cobalt (Co), copper (Cu), lead (Pb),
manganese (Mn), mercury (Hg), nickel (Ni), phosphorous (P), selenium (Se), silver (Ag),
thallium (TI), and zinc (Zn). Cadmium, manganese, lead (inlet), and zinc were determined by
Direct Aspiration Flame Atomic Absorption Spectrophotometry (FLAAS). Antimony, arsenic,
beryllium, lead (other sources and blanks), nickel, selenium, silver, and thallium were
determined by Graphite Furnace Atomic Absorption Spectrophotometry (GF AAS). Barium,
chromium, cobalt, copper and phosphorus were determined by Inductively Coupled Plasma -
Optical Emission (ICP). Mercury was determined by Cold Vapor Atomic Adsorption
Spectrophotometry (CV AAS).
Baghouse dust samples were collected and compo sited in sample containers for each test
run. Composites were collected at the beginning, middle, and end of the individual sample runs.
F AL analyzed the three samples for the same number and type of analytes as for the EP A
Method 315 samples with the exception of cobalt which was inadvertantly omitted from the
analyte list provided to the analytical laboratory . Samples were prepared by nitric acid digestion,
followed by analysis by Direct Aspiration Flame Atomic Absorption Spectrophotometry
(FLAAS), Graphite Furnace Atomic Absorption Spectrophotometry (GF AAS), Inductively
Coupled Plasma - Optical Emission (ICP) and Cold Vapor Atomic Absorption
Spectrophotometry (CV AAS).
5.6
POLYCYCLIC AROMATIC HYDROCARBONS
CARB Method 429, "Determination of Polycyclic Aromatic Hydrocarbon (PAH)
Emissions from Stationary Sources," was used to determine PAHs. This method is applicable for
-------
Tempera...e
1i Sensor
emperabl'l Stack
Sensor ~ WaD
~ I Heat Traced
'" Ol=ed
88rwar
l .....
~
J.
PIal TdI8
/
Type S PIlot Tube
~
Ortftce
Ternp81'11ur8
Sensor
-----------------
01888 Finer
Holder
Heated ANa
Vacwm
line
Teg1p8rIJur8
Senaors
vaaun
Gauge
Figure 5.1 Sampling Train Schematic for EPA Method 315
-------
the determination of 19 P AHs. Quanterra submitted solvent extracted XAD-2/B) resin sorbent
cartridges and untared Teflon/B) filters for sampling purposes. The sampling train consisted of a
glass nozzle, a heated gla~s lined or Teflon/B) probe, a heated precleaned, untared Teflon/B) mat
filter, a water-cooled coil condenser, and an adsorbent trap containing approximately 40 grams of
XAD-2/B) adsorbent resin. Due to particulate loading and the length of sampling time, filters were
replaced at the baghouse inlet at port changes. The first impinger was empty, the next two each
contained 100 milliliters of 3 mM sodium bicarbonate and 2.4 mM sodium carbonate. The next
impinger was empty, followed by the last impinger which contained approximately 250 grams of
indicating silica gel. At the baghouse inlet sampling location, an unheated flexible Teflon~
sample line was used between the filter exit and condenser inlet. This modification was
necessitated by poor access to the sample ports. Particulate and gaseous phase P AHs were
extracted isokinetically from the source and collected in the probe and filter; XAD~-2 resin; and
impinger portions of the sample train. A schematic ofCARB Method 429 is shown in
Figure 5.2. Figure 5.3 is a schematic of the CARB Method 429 sample recovery process.
Analysis was accomplished by isotope dilution mass spectrometry combined with high
resolution gas chromatography. Figure 5.4 is a schematic of the CARB Method 429 analytical
process.
NIOSH Method 5506 was also used to scan for gaseous phase P AHs at the baghouse inlet
and outlet, and underfire stack. The samples were collected at each location using an in-stack
filter followed by a series of three out-of-stack XAD-21) sorbent tubes. Sampling was performed
continuously throughout the pushing operations and during idle periods at a sample rate of
1.5-2 liters per minute. The samples were analyzed using high performance liquid
chromatography and fluorescence/UV detection. The NIOSH 5506 method was used to scan for
P AHs in the event CARB Method 42~ results were below analytical detection limits. The
NIOSH results were not intended to be compared to CARB 429 results.
-------
G..
Exit -
Orilice
Conden.er
t
~:~ t ~
TypeS
Pltot Tub.
Stack
Wa.
A Heated Ola..
- U Liner
Temperatura
8en80r
Bunon Hook
Nozzle
l
H..tad Are.
Temperatur.
a.n.ora
Empl1 100 ml HPLC Water
Vacuum
Pump
Figure 5.2 Sampling Train Schematic for CARD Method 429
-------
Rinse wilh known volume:
1. acelone
2. melhylene chloride
3. hexane
(
Conlalner
No.1
Mark liquid level,
Store at orc or lower
lway from light
Tre sfer
)
Store at 4'C
or lower Iway
from light
Mark liquid level,
Store It orc or lower
away from Ught
Cap
Siore al 4 C or lower
away from light
A. Tare weigh Conlainer 14
B. Decanl conlenls 01
Impinpers inlo tared
Container 14
C. Weigh Conlainer 14
D. Mark liquid level,
Siore al 4'C or lower
away from lighl
Rinse whh known volume:
1. acelone
2. melhylene chloride
3. hexane
Mark liquid level,
Siore at 4'C or lower
away from light
Figure 5.3 CARD Method 429 Sample Recovery Schematic
5-8
A. Tare weigh .
cartrtridge with
silica gel
8. Weigh alter
sampling
-------
Surrogate Standards
Added to XAD.2 Resin
1
Solvent
Rinses
Internal
Standards
MeCI2
Soxhlet Extraction
Archive
1
Containers No.1 and No. 3
Figure 5.4 CARB Method 429 Analytical Schematic
-------
6.0 QUALITY ASSURANCE/QUALITY CONTROL
PROCEDURES AND RESULTS
This section describes the specific QAlQC procedures employed by PES in performing
this series of tests. The procedures contained in the "Quality Assurance Handbook for Air
Pollution Measurement Systems, Volume III, Stationary Source Specific Methods," EP A/6001R-
94/038c, and in the reference test methods served as the basis for performance for all testing and
related work activities in this project.
6.1
CALIBRATION OF APPARATUS
The preparation and calibration of source sampling equipment is essential in maintaining
data quality. Brief descriptions ofthe calibration procedures used by PES follow.
6.1.1 Barometers
PES used aneroid barometers which are calibrated against a station pressure value
reported by a nearby National Weather Service Station corrected for elevation.
6.1.2 Temperature Sensors
Bimetallic dial thermometers and Type K thermocouples were calibrated using the
procedure described in Section 3.4.2 of the Quality Assurance Handbook, Volume III, 1994.
Each temperature sensor was calibrated over the expected range of use against an ASTM 3C or
3F thermometer. Table 6.1 summarizes the type of calibrations performed, the acceptable levels
of variance, and the results. Digital thermometers were calibrated using a thermocouple
simulator having a range ofO-2400°F.
6.1.3 Pitot Tubes
Type S pitot tubes constructed to EP A Method 2 specifications were used. Pitot tubes
meeting these specifications are assigned a baseline coefficient of 0.84 and need not be
calibrated. The dimensional criteria and results for each pitot tube used are summarized in Table
6.2.
-------
TABLE 6.1
SUMMARY OF TEMPERATURE SENSOR CALIBRATION DATA
Temp. Sensor Temperature, of Temperature Calibration
I.D. Usage Difference, % Tolerances
Reference Sensor
5B Stack Gas 72 72 0.0 <:H.5%
44 44 0.0 <%: 1.5%
204 204 0.0 <%: 1.5%
400 400 0.0 <%:1.5%
T5B Stack Gas 74 74 0.0 <%: 1.5%
46 46 0.0 <%: 1.5%
200 200 0.0 <%: 1.5%
318 318 0.0 <%: 1.5%
7A Stack Gas 74 74 0.0 <%: 1.5%
36 36 0.0 <%: 1.5%
198 199 0.2 <%: 1.5%
333 332 0.1 <%: 1.5%
7D Stack Gas 74 74 0.0 <%: 1.5%
40 41 0.2 <%: 1.5%
206 205 0.2 <%: 1.5%
340 341 0.1 <%: 1.5%
8C Stack Gas 74 74 0.0 <%: 1.5%
38 38 0.0 <%: 1.5%
199 199 0.0 <%: 1.5%
339 339 0.0 <%: 1.5%
RP20 Stack Gas 72 69 0.7 <%: 1.5%
32 32 0.0 <%: 1.5%
210 208 0.3 <%: 1.5%
-- - - -
RP21 Stack Gas 74 75 0.2 <%: 1.5%
32 32 0.0 <%:1.5%
208 209 0.2 <%: 1.5%
-- -- - -
MB-l Meter Box Inlet 75 75 0.0 <%: 1.5%
38 38 0.0 <%: 1.5%
190 190 0.0 <%: 1.5%
Meter Box Outlet 75 74 0.2 <%: 1.5%
37 37 0.0 <%:1.5%
190 190 0.0 <%:1.5%
MB-2 Meter Box Inlet 70 69 0.2 <%: 1.5%
34 34 0.0 <%: 1.5%
160 159 0.2 <%: 1.5%
Meter Box Outlet 70 70 0.0 <%: 1.5%
34 33 0.2 <%: 1.5%
160 160 0.0 <%: 1.5%
-------
TABLE 6.1 (concluded)
Temp. Sensor Temperature, of Temperature Calibration
I.D. Usage Difference, % Tolerances
Reference Sensor
MB-3 Meter Box Inlet 74 74 0.0 <:I: 1.5%
30 31 0.2 <:I: 1.5%
190 190 0.0 <:I: 1.5%
Meter Box Outlet 73 72 0.2 <:I: 1.5%
32 31 0.2 <:I: 1.5%
190 190 0.0 <:I: 1.5%
MB-4 Meter Box Inlet 74 74 0.0 <:I: 1.5%
30 30 0.0 <:I: 1.5%
190 191 0.2 <:I: 1.5%
Meter Box Outlet 73 72 0.2 <:I: 1.5%
32 30 0.4 <:I: 1.5%
190 191 0.2 <:I: 1.5%
MB-5 Meter Box Inlet 70 69 0.2 <:1:1.5%
34 34 0.0 <:I: 1.5%
160 159 0.2 <:I: 1.5%
Meter Box Outlet 70 71 0.2 <:I: 1.5%
34 33 0.2 <:I: 1.5%
160 161 0.2 <:I: 1.5%
MB-6 Meter Box Inlet 68 67 0.2 <:I: 1.5%
33 34 0.2 <:I: 1.5%
155 155 0.0 <:I: 1.5%
Meter Box Outlet 68 68 0.0 <:I: 1.5%
33 34 0.2 <:I: 1.5%
155 156 0.2 <:I: 1.5%
-------
TABLE 6.2
SUMMARY OF PITOT TUBE DIMENSIONAL DATA
Results
Measurement Criteria Pitot Tube Identification
SB SC SE 7A 7D 8C RP20 RP21
exl <10° 3 0 I 0 3 3 0 0
ex2 <10° 3 I 1 1 3 0 1 1
pi <5° 1 I 1 3 1 1 1 1
p2 <5° 3 I 3 2 I 1 0 0
y - 3 1 0 4 I I 1 I
a - I 1 1 1 0 0 0 0
A - 1.124 0.948 1.122 0.996 0.931 0.939 1.023 1.023
Z ~ 0.125 in. 0.059 0.017 0.00 0.069 0.016 0.016 0.018 0.018
W ~ 0.03125 in. 0.020 0.017 0.020 0.017 0 0 0 0
D, 0.1875" ~ D, ~ 0.375 0.375 0.375 0.375 0.375 0.375 0.375 0.375
0.375"
A/2/D, 1.05 D. ~ A~ 1.50 1.26 1.50 1.33 1.24 1.25 1.36 1.36
1.50 D,
Acceptable Yes Yes Yes Yes Yes Yes Yes Yes
Assigned Coefficient 0.84 0.84 0.84 0.84 0.84 0.84 0.84 0.84
-------
6.1.4 Differential Pressure Gauges
PES used Dwyer inclined/vertical manometers to measure differential pressures. The
differential pressures measurements included velocity pressure, static pressure, and meter orifice
pressure. Manometers are selected with sufficient sensitivity to accurately measure pressures
over the entire range of expected values. Manometers are primary standards and require no
calibration.
6.1.5 Dry Gas Meters and Orifices
The EP A Method 315 and CARB Method 429 dry gas meters and orifices were calibrated
in accordance with Sections 5.3.1 and 5.3.2 ofEPA Method 5. This procedure involves direct
comparison of the dry gas meter to a reference dry test meter. The reference dry test meter is
calibrated annually using a wet test meter. Before its initial use in the field, the metering system
was calibrated over the entire range of operation as specified in EP A Method 5. After field use,
the metering system was calibrated at a single intermediate setting based on the previous field
test. Acceptable tolerances for the initial and final dry gas meter factors and orifice calibration
factors are:]: 0.05 and:]: 0.20 from average, respectively. The calibration results for the gas
meters and orifices used in this test program are summarized in Table 6.3.
6.2
ON-SITE MEASUREMENTS
The on-site QA/QC activities include:
6.2.1
Measurement Sites
Prior to sampling, the stack and inlet duct were checked dimensionally to determine
measurement site locations, location of velocity and sample test ports, inside stack/duct
dimensions, and sample traverse point locations. Inside stack/duct dimensions were checked
through both traverse axis to ensure uniformity of the stack/duct inside diameter. The inside
stack/duct dimensions, wall thickness, and sample port depths were measured to the nearest 1/8
inch.
6.2.2 Velocity Measurements
All velocity measurement apparatus were assembled, leveled, zeroed, and leak-checked
prior to use and at the end of each determination. The static pressure was determined at a single
point near the center of the stack or duct cross-section.
-------
TABLE 6.3
SUMMARY OF DRY GAS METER AND ORIFICE CALIBRATION DATA
.
Meter Gamma Orifice Coefficient
No. Pre-test Post-test % Diff. EP A Criteria Avera2e Ranl!e EP A Criteria
MB-l 1.012 1.011 0.1 %5% 1.954 1.754-2.154 1.954 % 0.20
MB-2 1.002 0.999 0.3 %5% 1.797 1.597-1.997 1.797 :I: 0.20
MB-3 1.004 0.990 1.4 :t: 5% 1.784 1.584-1.984 1.784 :I: 0.20
MB-4 0.979 0.992 1.4 :t:5% 1.872 1.672-2.072 1.872 :I: 0.20
MB-5 0.981 0.994 1.3 :t: 5% 1.770 1.570-1.970 1.770 :I: 0.20
MB-6 1.005 1.005 0.0 :t: 5% 1.778 1.578-1.978 1.778 :I: 0.20
-------
6.2.3 Flue Gas Composition
Integrated, multi-point, flue gas samples were collected in Tedlar@ gas bags from the
baghouse inlet and outlet and underfire stack. Prior to use the bags were leak checked and
purged with nitrogen to ensure cleanliness. Prior to and after completion of each sampling run,
the entire sampling system was leak checked from the tip of the probe. The bag samples were
analyzed on-site using an Orsat@ analyzer within four hours after sample collection, in
accordance with EP A Method 3B. Prior to use the Orsat@ analyzer was assembled and
replenished with fresh reagents and leak checked using the manufacturer's procedures.
6.2.4 Moisture
The EP A Method 315 and CARB Method 429 sampling trains were used to determine the
flue gas moisture content. During sampling, the exit gas of the last impinger was maintained
below 68°F to ensure complete condensation of flue gas water vapor. The total moisture was
determined gravimetrically using an electronic platform balance with 0.1 gram sensitivity. The
XAD@-2 adsorbent modules from the CARB Method 429 sampling trains were also weighed and
their weights included in the moisture catch.
6.2.5 EP A Method 315 and CARB Method 429
The field sampling QA/QC for the EP A Method 315 and CARB Method 429 sampling
trains were similar. Table 6.4 summarizes the critical measurements made and EP A's critical
acceptability criteria. All pre- and post-test sample train leak checks met the acceptance criteria.
Most of the isokinetic sampling rates deviated by no more than :i:10 percent thereby meeting the
method criteria of 90-11 0%. There were three sample runs slightly outside of this range, two at
the baghouse inlet and one at the baghouse outlet. These are not believed to have had an impact
on sample results.
The EP A Method 315 and CARB Method 429 field blanks were collected near each of
the sampling locations to check for any sample contamination at the sites. Sample trains were
assembled and pre- and post-test leak checks were conducted. The sample trains were recovered
in the same manner as the actual sample runs. Each field blank train was subjected to a
minimum of one leak check in the laboratory (filter holder assembly) and a minimum of three at
the sampling site.
An acetone and methylene chloride blank and tared quartz fiber filter were taken as
control samples for the particulate/MCEM analysis and subsequent analysis for metals. Blanks
were taken of the impinger and recovery reagents. CARB 429 control samples consisted of
acetone, methylene chloride and hexane, as well as an untared Teflon@ filter and XAD@-2 resin
trap.
-------
TABLE 6.4
SUMMARY OF EPA METHOD 315 AND CARR METHOD 429 FIELD SAMPLING QA/QC DATA
Pre-Test Post-Test EPA Percent EPA
Date Site Run No. Leak Rate Leak Rate Criteria Isokinetic Criteria
acfm acfm acfm
Baghouse Inlet B-I-315-1 0.010 @ 15" Hg 0.001 @ 5" Hg sO.02 118.1 90-110%
B-I-429-1 0.011 @ 15" Hg 0.012 @ 15" Hg sO.02 90.5 90-11 0%
08/11/98
Baghouse Outlet B-0-315-1 0.003 @ 15" Hg 0.003 @ 8" Hg sO.02 99.6 90-110%
B-0-429-1 0.008 @ 15" Hg 0.012 @ 7" Hg sO.02 112.4 90-11 0%
Baghouse Inlet B-I-315-2 0.007 @ 15" Hg 0.015 @ 5" Hg sO.02 105.2 90-110%
B-I-429-2 0.008 @ 13" Hg 0.005 @ 10" Hg sO.02 94.1 90-110%
08/12/98
Baghouse Outlet B-0-315-2 0.007 @ 16" Hg 0.003 @ 10" Hg sO.02 98.3 90-110%
B-0-429-2 0.006 @ 15" Hg 0.001 @8" Hg sO.02 95.9 90-110%
Baghouse Inlet B-I-315-3 0.005 @ 15" Hg 0.006 @ 4" Hg sO.02 110.8 90-11 0%
B-I-429-3 0.002 @ 15" Hg 0.006 @ 6" Hg sO.02 91.8 90-11 0%
08/13/98
Baghouse Outlet B-0-315-3 0.003 @ 15" Hg 0.004 @ 8" Hg sO.02 96.7 90-110%
B-0-429-3 0.004 @ 15" Hg 0.004 @ 11" Hg sO.02 100.0 90-11 0%
Underfire Stack B-U-315-1 0.002 @ 15" Hg 0.001 @ 4" Hg sO.02 106.0 90-110%
08/14/98 B-U-315-2 0.005 @ 15" Hg 0.002 @ 3" Hg sO.02 107.5 90-110%
B-U-429-1 0.006 @ 15" Hg 0.006 @ 18" Hg sO.02 96.0 90-110%
B-U-429-2 0.001 @ 17" Hg 0.006 @ 14" Hg sO.02 100.8 90-11 0%
08/15/98 B-U-315-3 0.003 @ 15" Hg 0.002 @ 5" Hg sO.02 103.5 90-110%
B-U-429-3 0.002 @ 15" Hg 0.002 @ 7" Hg sO.02 99.1 90-110%
-------
6.3
LABORATORY ANALYSES
The EP A Method 315 and CARB Method 315 samples were hand delivered to PES'
contract laboratories for analyses. Upon delivery, the samples were transferred to the laboratory
sample custodian, where they were unpacked and inspected for damage, status, and chain-of-
custody documentation. All samples were received by the laboratories in good condition. The
PES Project Manager and Field Team Leader then contacted the laboratory analysts and
discussed the samples and the analyses required.
PES also conducted a follow-up visit to three of the four laboratories to review
procedures for sample handling and tracking, sample preparation and analyses, data reporting,
and quality control. Visits were made to ERG, F AL and Quanterra. A visit was not made to
LabCorp. The results of these visits are summarized in Appendix E. It is the opinion of PES that
the analytical laboratories selected to support this assignment were well staffed, used state-of-
the-art equipment, followed rigorous QAlQC procedures, and submitted accurate reports of the
anlaytical results.
6.3.1 EPA Method 315 Filterable Particulate and Methylene Chloride Extractable Matter
Filterable PM and MCEM analysis consisted of front half acetone and methylene cWoride
sample rinses and quartz fiber filters. Back half MCEM analysis consisted of acetone and
methylene chloride rinses of impingers containing distilled, deionized water. Prior to the field
testing program, the filters were tared in the ERG laboratory, stored in glass petri dishes and
sealed with Teflon@ tape. Upon receipt of the samples in the ERG laboratory, the acetone rinses
were placed in tared beakers and evaporated to dryness at room temperature. The filters and
beakers were dessicated and weighed to a constant weight. Table 6.5 summarizes the EP A
Method 315 lab blank QC data results. Table 6.6 summarizes the EP A Method 315 field blank
QC data results. At the baghouse inlet and outlet, the MCEM in the field blanks was about 22%
of the MCEM collected in the actual samples. At the underfire stack, the MCEM in the field
blank was less than 1 % of the MCEM collected in the actual samples. The field blank values
represent MCEM contained in the ambient air at the test sites. Field blanks are not required by
EP A Method 315 and, therefore, there is no provision in the method for corrections to the
MCEM in the actual samples.
The front half samples were re-dissolved in methylene chloride, filtered, and the filtered
liquid dessicated to dryness for MCEM determination. The backhalfimpinger fraction was
extracted with several portions of methylene chloride and placed in a beaker. The solvent is
evaporated and dessicated to dryness for weighing. Criteria of acceptance of gravimetric
analysis is:f: 0.5 milligrams between two weights, taken at least six hours apart.
6.3.2 EP A Method 29 - Multiple Metals
F AL analyzed the filterable particulate catch of the quartz filters and also the particulate
and extracted organic matter residue of the EP A Method 315 samples. A total of 17 metals were
analyzed for. Analysis followed EP A Method 29 analytical procedures. A total of 13 samples
were analyzed, nine were stack gas samples, three were field blanks and one reagent blank.
Cadmium, manganese, lead (inlet samples) and zinc were analyzed by Direct Aspiration Flame
Atomic Absorption Spectrophotometry (FLAA). Antimony, arsenic, beryllium, lead, nickel,
selenium, silver, and thallium were determined by Graphite Furnace Atomic Absorption
Spectrophotometry (GF AA). Barium, chromium, cobalt, copper, and phosphorus were
-------
TABLE 6.5
SUMMARY OF EPA METHOD 315 ANALYTICAL QC DATA
. LAB BLANK ANALYSIS
Sample Fraction Particulate, MCEM,
grams grams
Quartz Filter 0.0032 0.0000
Acetone 0.0002 --
Methylene Chloride 0.0000 --
Distilled Water 0.0001 --
-------
TABLE 6.6
SUMMARY OF EPA METHOD 315 ANALYTICAL QC DATA
FIELD BLANK ANALYSIS
Baghouse Inlet Baghouse Outlet Underfire Stack
Sample Fraction B-I-315-FB, B-O-315-FB, B-U-315-FB,
grams grams grams
Filter - PM 0.0017 0.0011 0.0058
MCEM 0.0003 0.0002 0.0000
Acetone FHR, 0.0022 0.0014 0.0022
PM
Methylene Chloride FHR, 0.0001 0.0009 0.0003
MCEM
Acetone BHR, 0.0000 0.0000 0.0000
MCEM
Methylene Chloride BHR, 0.0001 0.0000 0.0000
MCEM
H20 Impinger Rinses, 0.0016 0.0001 0.0000
MCEM
-------
detennined by Inductively Coupled Plasma - Optical Emission (ICP). Specific QA and QC
activities for the analyses consisted of a reagent blank (quartz filter and pan) and spike recoveries
of 16 of the analytes. R~coveries ranged from 83 percent to 106 percent. Duplicate analysis on
several metals were within the acceptable limit of20%. Table 6.7 summarizes the EPA Method
29 analytical recovery and duplicate analyses QC results.
6.3.3 CARB Method 429
PAHs were analyzed following the procedures ofCARB Method 429. All fractions of
the sampling train were combined for a single extract which was analyzed by high resolution gas
chromatography/high resolution mass spectrophotometry (HRGG/HRMS). Nine stack gas
samples were analyzed, along with three field blanks, a method blank and lab blank. The XAD4D
resin cartridges were spiked with surrogate standards prior to use for field sampling to
demonstrate overall sampling and analytical recovery efficiency. After samples were received in
the laboratory and prior to sample extraction, a laboratory control sample was prepared with two
levels of surrogate standards to monitor the precision and accuracy of the analytical process
independently of sample matrix effects. Table 6.8 summarizes the CARB Method 429 field
blank QC results. Table 6.9 summarizes the CARB Method 429 lab control sample QC results.
Table 6.10 summarizes the CARB Method 429 surrogate standards recoveries for 17 analytes for
all nine field sample runs.
-------
TABLE 6.7
SUMMARY OF EPA METHOD 29 ANALYTICAL QC DATA
LAB CONTROL SAMPLE (LCS) RECOVERY AND DUPLICATE ANALYSIS
Spike LCS Recovery Duplicate RPD Limit,
Analyte Amount, Recovery, Limit, RPD,
Jlg/l % % % 0.10
Antimony 100 94 70-130 -- --
Arsenic 100 85 70-130 -- --
Barium 1000 96 70-130 -- --
Beryllium 5.0 91 70-130 -- --
Cadmium 400 97 70-130 0.0 :!: 20%
Chromium 2000 85 70-130 -- --
Cobalt 1000 88 70-130 -- --
Copper 2000 89 70-130 -- --
Manganese 400 95 70-130 0.0 :!: 20%
Mercury 5.0 95 70-130 -- --
Lead 2000/100 98/98 70-130 2.6 :!: 20%
Nickel 100 86 70-130 -- --
Phosphorus 2000 83 70-130 -- --
Selenium 50 103 70-130 -- --
Silver 10 106 70-130 -- --
Thallium 50 88 70-130 -- --
Zinc 400 104 . 70-130 9.8 :!: 20%
-------
TABLE 6.8
SUMMAF-Y OF CARD METHOD 429 ANALYTICAL QC DATA
FIELD BLANK RESULTS
Baghouse Baghouse Underfire Stack
Analyte Inlet Outlet
.u!lsample .u!lsample .ug/sample
Naphthalene 1.1 00 0.620 2.900
2-Methylnaphthalene 0.089 0.076 0.840
Acenaphthylene 0.027 ND 0.280
Acenaphthene 0.014 0.041 0.097
Fluorene 0.022 0.022 0.140
Phenanthrene 0.160 0.130 0.370
Anthracene ND ND 0.025
Fluoranthene 0.078 0.044 0.097
Pyrene 0.029 0.054 0.058
Benzo(a) anthracene 0.013 0.011 0.018
Chrysene 0.023 0.017 0.030
Benzo(b) fluoranthene 0.018 0.015 0.021
Benzo(k) fluoranthene 0.015 0.012 0.015
Benzo( e) pyrene 0.013 0.011 0.012
Benzo(a) pyrene 0.014 0.012 0.013
Perylene ND ND ND
Indeno(1,2,3-cd) pyrene 0.015 0.012 0.013
Dibenz(a,h) anthracene ND ND ND
Benzo(g,h,i) perylene 0.041 0.037 0.032
-------
TABLE 6.9
SUMMARY OF CARD METHOD 429 ANALYTICAL QC DATA
LAB CONTROL SAMPLE (LCS)
Spike LCS Recovery, Recovery
Analyte Amounts, % Limits,
,ug/sample %
Naphthalene 100 107 50-150
2-Methylnapthalene 100 102 50-150
Acenaphthylene 100 114 50-150
Acenaphthene 100 112 50-150
Fluorene 100 117 50-150
Phenanthrene 100 110 50-150
Anthracene 100 113 50-150
Fluoranthene 100 115 50-150
Pyrene 100 113 50-150
Benzo( a )anthracene 100 103 50-150
Chrysene 100 102 50-150
Benzo(b )fluoranthene 100 108 50-150
Benzo(k)fluoranthene 100 111 50-150
Benzo( e )pyrene 100 124 50-150
Benzo( a )pyrene 100 104 50-150
Perylene 100 87 50-150
Indeno(1,2,3-cd)pyrene 100 99 50-150
Dibenz( a, h) anthracene 100 111 50-150
Benzo(g,h,i )pery lene 100 104 50-150
Naphthalene-d8 50 67 50-150
Acenaphthylene-d8 50 61 50-150
Acenaphthene-d 10 50 66 50-150
-------
TABLE 6.9 (Concluded)
Spike LCS Recovery, Recovery
Analyte Amounts, Limits,
j.lglsample % 0/0
Fluorene-dl0 50 62 50-150
Phenanthrene-dl0 50 65 50-150
Fluoranthene-d 10 50 76 50-150
Pyrene-d 1 0 50 79 50-150
Benzo( a )anthracene-d 12 50 92 50-150
Chrysene-d 12 50 102 50-150
Benzo(b )fluoranthene-d 12 50 95 50-150
Benzo(k) fluoranthene-d 12 50 91 50-150
Benzo( a )pyrene-d 12 50 83 50-150
Perylene-dl2 50 83 50-150
Indeno(123 -cd)pyrene-d 12 50 96 50-150
Dibenz( a,h) anthracene-d 14 50 91 50-150
Benzo(g,h,i) perylene-dl2 50 97 50-150
-------
TABLE 6.10
SUMMARY OF CARD METHOD 429 ANALYTICAL QC DATA
SURROGATE STANDARD RECOVERIES
B-I-429-I, B-I-429-2, B-I-429-3, B-0-429-I, B-0-429-2, B-0-429-3, B-U-429-I, B-U-429-2, B-U-429-3, Recovery
Analyte % % % % % % % % % Limits,
%
13C-Fluorene 87 90 82 83 81 80 105 96 93 50-150
Naphthalene-d8 90 69 82 67 65 58 64 94 121 50-150
Acenaphthylene-d8 69 57 63 73 73 76 68 57 60 50-150
Acenaphthene-d I 0 85 72 76 79 76 83 77 60 44 50-150
Fluorene-d I 0 84 67 76 70 79 78 70 75 74 50-ISO
Phenanthrene-d I 0 96 87 91 78 84 86 75 85 83 50-150
Fluoranthene-d 10 109 93 94 81 85 82 72 84 85 50-150
Pyrene-d I 0 107 90 93 81 86 83 68 75 78 50-150
Benzo( a)anthracene-d 12 105 98 105 87 93 99 78 75 82 50-150
Perylene-d 12 90 81 88 85 86 84 68 58 64 50-150
Indeno(123cd)pyrene-d12 93 82 94 99 103 104 77 81 79 50-150
Chrysene-d 12 101 92 110 74 79 89 71 78 76 50-150
Benzo(b )t1uoranthene-d 12 104 100 98 107 104 III 88 92 95 50-150
Benzo(k)t1uoranthene-d 12 99 87 96 84 91 93 86 94 91 50-150
Benzo( a)pyrene-d 12 90 82 87 93 97 96 73 67 75 50-150
Dibenz( a,h)anthracene-d 14 90 81 92 103 104 105 80 88 88 50-150
Benzo( g,h,i)perylene-d 12 91 83 96 91 93 95 70 76 74 50-150
-------
APPENDIX A
-------
PUSHING PROCESS AND CONTROL DEVICE PARAMETERS: TEST RUN NO. 1,8/11/98
Time Oven No. Dry Coal Charged Coking Time Amps Delta P (in. of Inlel Pressure (in. Damper (%
flh.\ Ihn~,"'\ WA'",,\ nf WA._.I n....n\
10:34:10 291 64,310 18.6 48 6.2 1.8 54
10:48:00 203 65,238 18.7 46 5.5 1.4 48
11 :03:20 213 64,032 18.7 47 4.9 1 49
11:13:20 223 65,053 18.7 49 6.2 1.5 58
11:23:30 233 63,939 18.7 47 5.3 1 53
11 :34:20 243 64,496 18.4 46 5.6 1.2 48
11:45:10 253 63,846 18.4 46 5.7 1.4 50
12:01:30 263 65,053 18.5 45 5.4 1.3 44
12:11:20 273 64,032 18.5 47 6.1 1.6 53
12:22:40 283 65,981 18.6 45 5.2 1.4 44
12:37:20 205 64,774 18.6 45 4.7 1 47
12:56:40 215 65,981 18.7 53 6.7 2 69
13:06:50 225 64,682 18.8 47 6 1.4 51
13:26:40 235 65,888 18.9 54 7.5 1.8 72
13:35:40 245 64,589 18.9 46 5.9 1.4 51
13:44:40 255 65,517 18.6 45 5.6 1.2 44
13:54:10 265 64,589 18.5 50 7.3 1.9 64
14:03:30 275 66,074 18.5 45 5.9 1.4 49
14:13:20 285 64,589 18.5 44 5.7 1.3 44
14:23:40 207 65,888 18.5 44 5.9 1.3 47
15:08:00 217 64,682 19.0 51 7 1.7 62
15:16:30 227 64,125 19.0 47 6.4 1.5 53
15:27:50 237 64,774 19.0 46 5.9 1.1 49
15:38:40 247 64,496 19.0 48 6.6 1.5 56
15:48:50 257 65,238 18.8 46 5.2 1.1 51
15:58:30 267 63,475 18.8 45 5.9 1.3 48
16:08:20 277 64,774 18.8 46 5.7 1.4 50
16:18:30 287 65,517 18.8 46 5.8 1.5 49
16:28:30 209 64,125 18.8 44 5.3 1.4 44
16:39:40 219 65,238 18.8 46 5.7 1.3 50
16:58:20 229 64,403 18.9 46 5.8 1.2 50
17:08:20 239 65,331 19.0 47 5.8 1.3 51
17:19:10 249 64,867 19.0 45 5.6 1.3 48
17:33:20 259 65,331 18.2 47 5.6 1.2 53
17:42:40 269 64 ,960 18.1 46 6 1.4 49
17:58:10 279 65,795 18.2 44 4.6 0.9 44
J 8:08:00 289 65,146 18.1 44 4.2 0.9 42
18:18:00 202 65,610 18.1 44 5.5 1.4 42
18:34:50 212 65,146 18.2 46 5.9 1.5 50
18:44:00 222 65,238 18.1 49 7 1.5 59
19:03:20 232 64,960 18.3 46 5.9 1.2 49
19:12:40 242 66,445 18.2 46 5.4 0.9 51
19:28:00 252 65,146 18.4 46 5.6 1.3 48
19:37:00 262 65,702 18.1 46 5.8 1.3 48
19:46:20 272 63,939 18.1 49 6.4 \.8 59
-------
PUSHING PROCESS AND CONTROL DEVICE PARAMETERS: TEST RUN NO. Z, 8IIZI98
Time Oven No. Dry Coal Charged Coking Time Amps Delta P (in. of Inlet Pressure (in. Damper (% open)
nh.\ Ihn.....\ =0'''''\ nf"",,_\
. 5.3 52
9:30:50 247 66,430 17.7 47 1.2
9:40:20 257 63,631 17.7 45 5.7 1.3 47
9:51:30 267 65,777 17.7 46 5.5 1.4 49
10:01:50 277 63,444 17.7 44 5.3 1.3 44
10:12:00 287 65,683 17.7 47 5.5 1.5 54
10:24:00 209 63,444 17.7 47 6.2 1.S 54
10:37:20 219 65,683 17.6 48 6.1 1.4 55
10:49:30 229 63,911 17.7 47 6.4 1.3 54
11:11:30 239 64,097 17.9 46 5.9 1.1 51
11:21:20 249 63,631 17.8 48 6.5 1.S 57
11 :32:50 259 65,123 17.8 46 5.4 1.1 50
11 :42:50 269 63,724 17.7 46 5.6 1.1 51
11 :53:00 279 65,310 17.8 45 6.1 1.4 48
12:09:20 289 64,284 17.9 47 6.5 1.6 55
12:31:30 202 63,537 18.0 47 5.7 1.2 51
12:44:30 212 64,004 18.0 46 6.1 1.4 48
12:55:30 222 64,657 17.9 46 5.7 1.1 51
13:06:10 232 64,190 17.9 45 5.7 1.2 45
13:16:50 242 64,284 17.8 46 6.5 1.3 52
13:40:10 252 63,351 18.1 46 4.8 0.9 48
13:50:10 262 65,030 18.1 47 6.2 1.6 52
14:00:00 272 62,978 17.9 48 5.8 1.6 56
14:09:20 282 64,470 17.9 46 5.9 1.S 50
14:28:30 204 63,724 17.9 46 5.5 1.S 49
15:08:30 214 64,750 18.4 48 6.1 1.7 52
15:18:00 224 63,257 18.3 50 6.4 1.7 58
15:28:30 234 64,190 18.3 52 6.9 1.8 64
15:38:50 244 63,724 18.3 47 5.8 1.4 51
15:48:30 254 63,817 18.3 49 6.6 1.7 59
15:59:40 264 64,937 J 8.4 46 5.6 1.S 51
16:11:40 274 65,497 18.4 45 5.6 1.4 48
16:21:00 284 64,004 18.4 45 5.2 1.4 46
16:32:30 206 64,564 18.4 46 5.9 1.5 51
16:41:40 216 63,817 18.4 46 5.5 1.4 50
17:09:00 226 64,937 17.6 48 5.9 1.S 53
17:19:10 236 64,004 17.6 47 5.7 1.2 51
17:28:50 246 65,403 18.5 47 6 1.4 52
17:38:50 256 63,631 17.6 47 6.2 1.4 54
17:48:40 266 65,217 17.6 46 5.2 I 49
17:59:20 276 64,377 18.5 46 6.1 1.4 49
18 :09:30 286 65,777 17.5 45 6 1.4 48
18:31:20 208 63,724 17.6 48 6.8 1.6 54
18:42:40 218 65,123 17.5 49 7.1 1.6 57
18:52:10 228 65,030 17.5 46 5.8 0.9 50
19:02:40 238 65,310 17.5 48 7.1 1.3 58
19:12:00 248 64,377 17.5 47 7 1.4 55
-------
PUSHING AND PROCESS CONTROL DEVICE PARAMETERS: TEST RUN NO.3, 8/13/98
Time Oven No. Dry Coal Charged Coking Time Amps Delta P (in. of Inlet Pressure (in. Damper (% open)
nh.' n.n..~' w"pr' nfw.._'
8:40:10 204 66,336 18.2 48 5.4 1.4 54
8:52:40 214 64,937 17.6 47 5.3 1.3 52
9:03:50 224 66,056 17.6 46 5.4 1.4 48
9:19:10 234 64,377 17.7 48 6.2 1.S 55
9:29:00 244 65,497 17.7 46 5.8 1.4 50
9:39:50 254 66,430 17.7 46 6 1.5 51
9:49:10 264 65,310 17.6 45 5.7 1.3 45
9:58:40 274 66,336 17.6 47 6.6 1.S 54
10:09:20 284 64,844 17.6 46 5.9 1.4 51
10:33 :30 206 65,497 17.9 46 6.1 1.4 49
10:44:50 216 65,310 17.5 47 6.1 1.S 52
10:55:20 226 65,497 17.6 49 6.9 1.5 59
II :05:40 236 65,777 17.6 46 6 1.1 51
11:15:50 246 64,377 17.6 47 6.3 1.4 54
11:35:00 256 64,657 17.8 46 5.6 1.2 48
11:44:50 266 65,963 17.8 45 5 I 48
II :55 :40 276 65,030 17.8 45 5.4 1.3 48
12:04:50 286 64,750 17.6 45 5.3 1.1 50
12:33:40 208 64,657 17.8 45 5.2 1.4 44
12:44:20 218 66,243 17.8 46 5.7 1.2 48
12:53:50 228 64,097 17.9 45 5.6 1.2 45
13:03:40 238 66,150 17.9 46 4.8 0.8 50
13:14:30 248 64 ,844 17.7 47 6.3 1.6 55
13:26:30 258 66,056 17.7 48 6.1 1.6 57
13:36:50 268 65,123 17.7 44 4.8 0.9 47
13:47:40 278 66,056 17.7 46 5.9 1.S 52
14:00:40 288 64,844 17.8 46 6 1.5 51
14:17:50 201 66,243 17.7 46 5.7 1.6 50
15:08:00 211 65,030 18.3 49 6.5 1.8 55
15:17:10 221 65,870 18.3 49 6.2 1.7 58
15:27:20 231 64,844 18.3 48 5.9 1.3 56
15:37:00 241 65,963 18.3 45 5.4 1.2 47
15:47:20 251 65,497 18.2 47 6.2 1.S 55
15:57:00 261 65,497 18.2 45 5.9 1.4 50
16:06:50 271 64,937 18.2 45 5.6 1.3 49
16:16:30 281 65,403 18.2 45 5.9 1.S 49
16:33:20 291 65,123 18.2 47 5.8 1.6 55
16:44:10 203 64,470 18.3 46 5.9 1.6 50
17:00:40 213 66,150 17.6 49 5.9 1.7 59
17:10:00 223 65,777 17.5 49 6 1.S 59
17:20:00 233 65,403 17.5 47 5.4 1.3 55
17:34:40 243 65,310 17.6 50 6.7 1.5 61
17:44:00 253 66,803 17.5 47 5.5 1.3 55
17:59:30 263 65,870 17.6 46 5.4 1.2 52
18:09:10 273 65,123 17.6 47 5.7 1.S 52
18:19:40 283 66,056 17.6 45 5.6 1.5 48
18:35:20 205 65,310 17.6 46 5.2 1.2 50
18:47:30 215 66,616 17.6 46 6.2 1.S 52
19:03:00 225 66,150 17.5 46 5.8 1.3 50
19:13:20 235 66,430 17.5 45 5.8 1.2 47
-------
Run No. Date Run Time Coal Charged Coke Pushed
- (tons) (tons)
B-I-M315-1 08/11/98 1035-2020 1,494 1,115
B-I-M429-1 08/11/98 1030-2016 1,494 1,115
B-I-M5506-1 08/11/98 1206-2007 1,236 922
B-I-M315-2 08/12/98 0922-1941 1,515 1,128
B-I-M429-2 08/12/98 0924-1935 1,515 . 1,128
B-I-M5506-2 08/12/98 0944-1928 1,481 1,103
B-I-M315-3 08/13/98 0842-1736 1,340 998
B-I-M429-3 08/13/98 1332-1934 943 660
B-I-M5506-3 08/13/98 0842-1710 1,275 974
B-O-M315-1 08/11198 1035-1958 1,494 1,115
B-O-M429-1 08/11198 1037-1958 1,494 1,115
B-O-M5506-1 08/11/98 1207-2000 1,204 898
B-O-M315-2 08/12/98 0929-1935 1,515 1,128
B-O-M429-2 08/12/98 0928-1934 1,515 1,128
B-O-M5506-2 08/12/98 0944-1901 1,352 1,031
B-O-M315-3 08/13/98 0840-1749 1,407 1,047
B-O-M429-3 08/13/98 0840-1748 1,407 1,047
B-O-M5506-3 08/13/98 0840-1715 1,275 974
B-U-M315-1 08/14/98 0921-1325 647 481
B-U-M429-1 08/14/98 0921-1325 647 481
B-U-M5506-1 08/14/98 1103-1320 356 267
B-U-M315-2 08/14/98 1441-1809 491 365
B-U-M429-2 08/14/98 1442-1809 491 365
B-U-M5506-2 08/14/98 1441-1755 458 341
B-U-M315-3 08/15/98 0838-1203 550 414
B-U-M429-3 08/15/98 0838-1208 550 414
-------
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
Time
OvenID
Pushing Emissions Observations
Travel Emissions Observations
dt.f
---1
1
;),11
;l
;20 '1
;;2./ ~
v,',1t-.C)/1
YT7> e#U ~ .
~
:23'J
;J. tj
;25~
. ...Jo h..t ~II
We~V1e5cJQ) '-I
Date~S
-------
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
Time
Oven ID
I)ushing Emissions Observations
Travel Emissions Observations
~
3'. J
3:
3'.3
3'.Y~
3:5
tJ: /l
t-f'~D
j tYZAJ
~
:1
:D~
5: /$
5 :2S
5:?
-------
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
Time
5: tfk
,.p-.
=fE-
+-
~
~
~
'* ~U.h a..bl>v~..} bel. I\~ bo.. +J--c: 0-t -
vis ;Io~ \; ~ ol,U. ClA-l+ ~
Date#'7Y
-------
,..
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
Time
0:7;3
IO',y.'f
0',56
1',03
j',,5
'"
Oven ID
Pushing Emissions Observations
;tA
23
J.Lf
;LS4
~
1&
~~4
~Dg
~
~~
J,fJlAJ
Ihu(!;)~'-f
Date~9g
Travel Emissions Observations
~
-------
r
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
Time
Oven ID
Pushing Emissions Observations
Travel Emissions Observations
):lfY-
7
.
/ J: 'i 3. ei1Ji D..f -to{! t7h /1.!)
~)
~
Vl- ~?)
?
;l ?J
o I
I
~
~
k-
Date~g
-------
PUSHING PARAMETERS - CAPTURE OBSERVATIONS: BETHLEHEM STEEL, BURNS HARBOR, IN
tJore: fAil V1'lLdir1Jj ~ on ~i~ p~~: ~ kJ-R~ tAhl>ve .J- 'tJehil'1L)/ !::a.+ff:V""f - t/,'s,~bi J ,'+-1 d;U,'~.
Time
:5: DO
5:0
5~ I ~
3
5: 5 'f
:Dg
1..,:1'1
u~ 35
CD: '-+7
1! D:(
1:J.3
1~ 31
Oven ID
213
J7..3
J33
~~3
:1.53 .
2Le3
.3
21
S
5'
2~5
?:>5
~f5
Date~f(
Pushing Emissions Observations
Travel Emissions Observations
~
lJl-0
~
~-
-------
COM on August
0ty Averages From
art of 6-Minute Opacl
Figure 3-2: Ch
13-14, 1998
11:00
11 :00 PM 8/14/98
PM 8/13/98 through
-------
Figure 3-3: Chart of6-Minute Opacity Averages From COM on August 14-15, 1998
11 :00 PM 8/14/98 through 11 :00 PM 8/15/98
-------
APPENDIX B
-------
----
==;;;;;;J....~
---
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
Plant: B~~h\e\1~m Stee \ - C~~il>dol'\ I TN
Dat.: e!1o/ ~8
Sampling L.ccation: 'Ba.J h D..\SQ TY\It-\ it 2 CoW:e O~ert 8QHe.(y
Inside of Far Wall to Outside of Nipple: 120. 2S ~
Inside of Near Wall to Outside of Nipple (Nipple Length): frJ.a'5H-"rf;:"
StackI.D.: \\4.0* f-w ~
Distance Downstream from Flow Disturbance IDistancell: 1/ g.,"'-r
S7A .0
~'Db inche., Stack 1.0. = . -' dd
Distance Upstream 1rom Flow Disturbance IDlstance AI:
~ inch.. , Stack I.D. = 1,'7 ad
Calculated By: RK/GbJ l'G
---- . I
'r
P
o
Hf'
o
--1
r/Y>
J:Y-
SchematIC of '\ D;) ..; .s-
Sampling Location +L.H r>"
f.r 3t'/<{31
$Ii-ry
Traverse FraCtIon Lengm ProcuCt of Nipple Traverse Point
Point of (inches) Columns 2 & 3 Length Location
Number Length (To nearest 1 ISj (ind1es) (Sum of Col. 4 & 5)
I 0 . Ol..t::. \ \ L{ I' "Z. ~ C( (p I ~ I' 8.0
1.. 0,687... Q.3 IS 3/B
:3 O,14~ lie,. ~ 22 5/8
'" I ()12~ 25.7 ~I V..
5 0 , 3t.12. .~". '\ I 33,0
~ o. h5if1 7~;o aLo
-, o. 71'-1 S 8.2. 9Li y~
B C,BSlf '17.3 10'3 1/'1
"I 0.(116 10'l.~ I \ 0 'sIB
-------
DuCt Diameters Ucstream From Flow Disturbance" (Distance A)
0.5 1,0 1.5 2.0 2.5
. 50 I I
en
.:e:
'0
a.. 40
CD
en
-
Q)
>
n:I
~ 30
"5
24
-
CD
~ 20
~
z
.E
. ~ 10
E
'2
~
~
,
16
-------------.....
Velocity (Non-Panlcutate)
12
8
o I I I I I I
2 3 4 5 6 7 8 9 10
Duct Diameters Downstream From Flow Disturbance" (Distance 8)
. Fl'Om Pl31nt of My Type of OI8lwD- lBend. C=8n8IOn. ConftCllOn. etc'
LOCATION OF TRAVERSE POINTS IN CIRCULAR DUCTS
(Fraction of Stack Diameter from Inside Wall to Traverse Point)
Flow
,
AI
f
i
i
BI
i
.1.
I
Ol8U118nC188
Traverse
Point Numcer of Traverse Points on a Diameter
Number
ana
Diameter 4 6 8 10 12
1 0.067 0.044 0.032 0.026 0.021
2 0.250 0.146 0.105 0.082 0.067
3 0.750 0.296 0.194 0.146 0.118
4 0.933 0.704 0.323 0.226 0.177
5 0.854 0.677 0.342 0.250
6 0.956 0.806 0.658 0.356
7 0.895 0.774 0.644
8 0.968 0.854 0.750
9 0.918 0.823
10 0.974 0.882
11 0.933
-------
---
~,.. -
c=Jc=J c=J
o
GAS VELOCITY AND VOLUMETRIC FLOW RATE
Plant: ~ H l H'I\'" ~ ,!"<-P \
Sampling Location: -+ "\It- ~ T
Run#:
Barometric Pressure, in. Hg:
Moisture, %: Molecular wt., Dry:
Stack Dimension, in. Diameter or Side 1:
Wet Bulb, 0 F: Dry Bulb,o F:
Date: tg-! D- t:iy
Clock Time:
Operators: G 6-
Static Pressure, in. ~O:
Pitot Tube, Cp:
Side2:
, () I o,t
Traverse Velocity Stack
Point Head Temp.
Number In. H20 of
( \ . \ I (P L
). .0\<. ?-O,->
?> q 1 ).. p-
~ ~S )..&5
.s I
io
'01 ~.f. yt6
\~ -----
d- /,, '/3.)0
) ~ .... 3?-~
.~ 9<1 ~"
S ,
(, (
IKP.. ~ ;)I~
Ta ..
"~1c.,1
I "IS SS
~ Z , 2....
. 8 tf..
Md .. (0.44 x %~) + (0.32 x %02) + (0.28 x %~)
Md = (0.44 x
) + (0.32 x
) + (0.28 x
Md= 'L8'f>tL
% H20 % H20
Ma=Mdx(1- -) + 18(-)
100 100
Ma .. (
)x(1- -)+18(-)
100 100
Ma =
;).~.) '7
T8 =
OF =
oR (oF + 460)
Pa = Pb + S,P. = (
13.8
) +
13.6
Pa = }. '7 .s) in. Hg
1KP=
Va .. 85.49 x Cp x JlJi x ~
Ts fiR)
PsxMs
Va = 85.49 x (
)x~
). (
Va = (, 1 . t ')
ft/a
A1J..
ft2
Os =VaxA1Jx60a!m
Os-
xeo
x
Os..
acfm
Pa % ~o
Osatd-OsX17.e47X-X(1- -)
Ta 100
Qa std-
x 17.847 X
Oaatd"
dacfm
X ( 1 - -)
-------
Pacific Environmental Services. Inc.
~'I} Cu~ - 8oltt,}fd Dry Molecular Weight Determination
Client/Project: 5506,000 . Orsat No. I
DatefTime: '?J1/l/ffJ Operator. J2/V..t. / p ~fe/V
Sample Type: Or~W+ Comments:
Ambtent Temp. of 70'~ Site Location: ~r.s.- ~
Run 1 Run 2 Run 3 Average Molecular Weight
Net Multiplier of
B,. Volume Stack Gas. Md
Net Actual Net Actual Net % (lblMoIe)
//1 0,,5 0,5 o.~~ 0.44
,& ;JiJ, I .2.0 ~ 0.32
CO~ 0.28
NzO '19, r 0.28
Md"
Run No.(s) Run 1 Run2 Run 3 Avef1lge Molecular Wetght
Net Multiplier of
g..1>' Actual Net Actual Volume Stack Gas. Md
Net % (fbIMoIe)
J~ tJ,5 I,)' 0.44
Oz' 'UJ,{ 1e-'.f) 0.32
CO~ 0.28
Nzo IQ-D.O 'I'/,5" 0.28
Md=
Run No.IS) Run 1 Run 2', Run 3 Average Molecular Weight
Net Multiplier of
(3.-1' Net Actual Net Actual Volume Stack Gas. Md
Net % (lblMole)
I.G O,~ P. ~ 0.44
Oz' 'k,o J.(). 0 0.32
CO~ 0.28
Nzo 1'!.'I /P1,D 7?' 'If,'IJ 0.28
Md-
. O2 Net Volume IS OZ actual reeding minus CO2 actual f1IlCIing.
. CO Net Volume IS CO actual f1Iadlng minus Oz actual readtng.
° Nz Net Volume IS 100 minus CO actual reading.
gge
ap_C IJMIIO_JALUIMCU,IIIC.
,,'
r"
-------
Pacific Environmental Services. Inc.
Dry Molecular Weight Determination
Client/Project: &4 k... ff. 0 2J:J,$ 2.0-0 1£;,tI) 0.32
CO" 0.28
N2" 7tt, i /-r>t). rJ 71.) 79. ff 0.28
Md=
Run 1 Run 2 Run 3 Average Molecular Welgnl
Net Multiplier 01
Volume Stack Gas. Md
Net Actual Net Actual Net % (lblMolel
t" p,5 ~ 0.44
O2' IJ 20,{ ~.c.. () W. t? 0.32
CO" 0.28
N2" /~; (J '71.5 /~,o 71.; 7/,J 0.28
Md-
. O2 Net Volume IS O2 actual reBdIl'lg minus CO2 aaual reading.
. CO Net Volume IS CO adual reac1lng minus O2 aaual readang.
"N2 Net Volume IS 100 minus CO actual reldlng.
~g~
-------
Pacific Environmental Services. Inc.
Sample Type:
Ambient Temp. of
t f IJ. c,t."
~~h5;;G.~:lrv
'6/0('6 I
~5A7'"
7o'p
Dry Molecular Weight Determination
Client/Project:
OateITime:
Orsat No.
----L-
J2I'-fJ-
Operator:
Comments:
Site LocatIOn:
~
Run 2 Run 3 Average Molecular Weight
Run NO.IS) Run 1 Net Multiplier of
~,:t-- Volume Stack Gas. Md
Net Actual Net Actual Net "10 (lblMolel
--;/1 ()., 0.44
Oz" 2/), f) 0.32
CO" 0.28
Nz' /1)0,0 7'1,; ,f/I' 0.28
Md=
Run No.(S) Run 1 Run 2 Run 3 Average Molecular Weight
Net Mulliplier 01
f3 - -:;: - Volume Stack Gas. Md
Net Adual Net Actual Net "10 (lblMolel
'?'B tJ,5 0.44
Oz" 2o.D 0.32
CO" 0.28
Nz' /90. D '7 1, ~ /0.0.0 71,) t1J~5' 0.28
Md=
Run No.ls) Run 1 Run2 Run 3 I Average Molecular W8Ight
Net Multiplier of
p;,.. 1 - Volume Slack Gas. Md
Actual Net Actual Net Actual Net % (ib/Molel
'?I';' COz eJ,L/ (f), p.{ as' 0, if>' 0.44
OZ" ;la~ 'lo, z...... :lc>,. 5 2.0.-'; 0,' 0.32
co" 0.28
Nz' ..>, '/?,Jf 0.28
Md-
" Oz Net Volume IS Oz actual relldlng minus CO2 actual reeding.
.. CO Net Volume IS CO adual rellClln9 minUI Oz adual reeding.
, Nz Net Volume IS 100 minUI CO adUBI reeding.
~ge
-------
---
CJ OD ==
c:::J c::::= ==
:J
.~
M"~
/1,.ofA
7~e ()
../"
"'!iA;~
. -d'f:~!: "10
.' \.... "f .0
, ~.r.,:,~i}" .: - '" .:::
.,1 "..,~ I'~ ~~ ~ j.~4. -J
.r'::j''X . 11.5
1\.10
15~.L\
o
\~
3D
qo
105
\'2.0
'3'1
IS,
11~
. ~. .u-v.~;.... :I. \.~-,.
..
--..
~~ ~. If/-:~..Ie.
~~
METHOD 18 FIELD DATA SHEET
Plant: t1u4~ ~ Tested Analyte: fY~,f;
~~~~~on: :i~_- f:i ~~~~~~;~~~;e:-:/ ~6Stgox .. 1-
Run #: -- . 5~()---2-L pt: Pretest (mm Hg): NI\
Stack 1.0.:_\ \~ " Post-Test (mm Hg): tJ(\
Pbar: "V? 7() Tt: Pretest ~F): N A
Sample Tube #: -z~ S-S-06-1 ". ~c.. Post-Test ~F): NA
Operators: ? Time: Start:~Finish:~ Total:~
Leak Check: Pre: . Post: V W/8:~D/8:--1U1.02:~C02: 0
1\11'\
~
Time Gauge Flow
Vacuum Setting
(Hg)
ItD~ - 20, '17 I / f/-~c.c
I/Z2i 1'=>9.Q \.'6 i,o
I/l~ 111. 1 l,g 1.0
1251 2Bh. '" I.~ I, D
I~D6 2~o7 IJ3 L<>
\321 '0\3,4 \.8 ).0
-r: .1. /~. ~/
1¥8\, .f.... ¥wtocIty St£Ir
~ HHa ~.
\ ~ NtIrrIeer ~
o 121. 5 \. ~ \. D
i'35\ ~I.\ \ 0 \. ~ 1.0
11-\\ ~"D.I i. 1.0
141{, "1.1!>,c 1.\ '.0
11~4l ~' 2 ,z. j,B I.D
I IIt?- 31:\ Z. 2 c:; \,8 I, Q
17~D 411.'1 I B 1.0
l-rlJ2. 4'Z./ "I loB 1,0
1~~1..- ~7q 0 \,8 lib
185'1 '-\'I2,(P \.8 \,0
I £1i '1 5bf>.1 19 1,0
1'\2~ 5'2. '2.5 '1.8 \.~
q\.tc. '3)7. 2 I. 8 1,0
11007 h'r.;A. p,q 19J 10
08Qtd-
dlCfm
1M Md.. (0.44 x %C02) ... (0.32 x %02) ... (0.28 x %Nz)
Md .. (0.44 x
) + (0.32 x
) + (0.28 x
7'-
1'1
Md =
"HO %HO
.. 2 2
-~-18(-.
100 100
7~
Ms = Md x ( 1
~~
170
7 S Ms.. (
,7
71
)X(1--)...18(-)
100 '00
Ms ..
75
OR (OF... 460)
. T"s..
OF ..
"/"1 Ps.. Pb ... ~ = (
13.8
) +
13.8
in. Hg
Ps ..
77 -
11 IKP =
is
7g Vs. 85.49 x Cp x .[f;P x
19
lLi
7(p Vs.. 85.49 x (
17
., 7 v...
.,~
IS Ae"
~
1 i.f as.. Vs x As x 60 11m
1-1
Ts fR)
Ps x Ms
)XV
) x(
ftls
112
0.-
x
x ISO
0..
ac:fm
Ps % Kzo
08 d",aax17.847X-X(1o-1
at T. 100
08 atd ..
x 17.847 X
x (1.-)
-------
---
CJ CJ 0 =:::;
c:::::::; c:::;; c:::::;
a
METHOD 18 FIELD DATA SHEET
Stt~ Tested Analyte: {)AIi~ - AhO'J# 6S,'D (,
Orifice Tank #: NA- "
Pump/Rotameter #: vast BQ~ L
pt: Pretest (mm Hg): NPr
Post-Test (mm Hg): tJA
Tt: Pretest fF): tJA-
Post- Test fF): tJ/Ir
Time: Start:~Finish:- Total:
W/8:.2:!!LD/8:.2!L02:~C02; 0,5
Plant: Be,\:h\t \.,!Y\
Date :_B / III G\ B
Location: !:n\et
Run #:Ju.f\ # 1-
Stack 1.0,: \\1.\"
Pbar: 29. BD
Sample Tube #: 6-1- 550(0 - 2 A. B.C
Operators: 'J'G / R "-
Leak Check: Pre: v Post:
Time Gauge Flow Md .. 10.44)( %C02) + (0.32 x %02) ~ (0.28 x %Nz)
Vacuum
(HQ) Setting TWo.
'II 0\. .- Md... (0.44 )( ) + (0.32 x ) + (0.28 x
o q~L.\ '5>'08. 37 \.is (.0 13
Md =
l!:i qsq 51'2.15 i. '3 1.0 11
% H20 % H20
30 lOlt.i 13/0(0. g I.B I.D e\ Ms = Mdxl1' -~. 18( - i
100 100
YS 10Zq CQQO.?. I.~ \,0 ~2 Ms... ( )x(I.-).18(-)
1\0 t+ i lD\~.() l.€ 100 100
(gO 1,0 B1.
7~ 10SCI (p2 B. "I MI"
LQ; \,0 60
0.0 \I III k?42.Z. \,8 \.0 1B Ts.. of '"' oR (oF. 4601
Tlihe (~a"'Q. ;:: low Ps .. Pb + ~ = (
Tla".u,. . \1.llel1l~ alee II 13.15 )+ 13.8
Fulnl ~ \ ~"III T.,llp.
~JI:I"'e.r 0 .in "',o~ --4-- Ps.. in, Hg
HO Ir~t.\ t 0.1 I,B 1.0 T7 -
120 \I "I L\ IJ)~ 0 I 1 L 9. ',C) 11 fF;p =
I ~ 1) \159 'nl 4 (, \.~ 1.0 77
!'t~ {~/; (,~r~/? /.,ftJ ~< ?7 Vs.. 65.49 x Cp x .[f;P x Ts fA)
~1{f)S 2.;B 12\.'\ :.\iD \.6 11 Ps x Ms
* ~"''" I 'aD 17J.~'?J 744 L{ 4 0 I., 11
~l',. rJ., 1''5 \1~Q 1'D/q,!I. "-t.C j,C; 17 Vs.. 85.49 x ( ) x( )X~
~. 1\0 1~1=3 7B~.lD . ~.o 1.5 .n
-If I,' J( 2.~O 1~~3 B~1. .10 "l,e> ',5 17 VI. ft/I
II:A. l~lIP.
1.;.; il.,()'2 a 1.\.0 Li 0 11; 73 A'. tt2
210 IltDlR R'IB.; Un L 7 71f
z..a~ ICI/?3 J.o \ t '5 7C;
QQ7.7 ----- --- as . VI x As x 60 11m
:Soo 1(,39. q2.0.~ 4.0 .5 1,
115 ,.,n'1 l\ 40,B u,O 1 5 7~ a.. )( xeo
;~ l\Q q '-2.0 ~,O I.S ..," '
',...
!>'t? 1'B '\~U. t; 4.0 ) S ,7 a.. 'acfm
'J,o 1ijQ IOOU',5 4.0 I,e 18 PI'" ~ 0
115 ;\Qol, '02" 0 ~.\? L., 77 Os td= 01 x 17.547 x - x (1. --:... )
~o I. fill I"\.t~ . () ':ih 1 T, 100
" 11
4ot; \~1 \() 1n 0 A: 0 It; 16
~:'2.0 It; ~ \0 I. a.t c 0 I . , Osetd:a x 17.847 x X(1.-t
11 100
~1S II1! 03 \ \"3. b I ,~ }.~ 1'7
qso II \8 II ~q.n ~ ,~ 1., ;7 Oattd- dlCfm
a.t&8 \'\1' /148,00 S.C) \.5 "
-------
---
Q Q c:::J ....-.,
r::=::; c:::; c
[1
'05
\'L0
,~o
ISO
Ib5
\g'3
200
2'0
215
~7~
PlantJ2s!h\lhtlY\ S-he.\
Date: '&/i3/9P,
Location: ' xt'\\~t
Run #: R\4\'\ -It 3>
Stack 1.0.: \ \4"
Pbar: lQ. BO
Sample Tube #: B-! - 5;0(.,- 3 lL1"~ A.".t
Operators: JC
Leak Check: Pre: V" Post: /
METHOD 18 FIELD DATA SHEET
Tested Analyte: Nlot:;t-\ Sc;o(o
Orifice Tank #: v -1-
Pump/Rotameter #: 'JQs"t '(,0)1. 1-
pt: Pretest (mm Hg): NI\.
Post-Test (mm Hg): NPr
Tt: Pretest fF): ~ t\ .
Post-TestfF}: tJ(\
Time: Start: eli'Z. Finish:J.11Q.. Total: U~.O
W/8:~D/8:~02: 20,5 C02: D,S
o
II;
Gauge Flow
Time Vacuum Setting
~o\ (HQ)
'd42 \\ 4'1 .'54 .~. () \.5
851 I '1 () . ~ ~,O LS
q16 \I~'5,6 3,0 t.'~
q~l \2.11.5 ,,\) 1.5
9~1. \ 2~(. .8 '3.0 1.5
QSl ,1~L.j. ~ 3.5" \.;
10\1 11.1&'. ~ 1.5 1.5
i'MIt \j,..,1 G1~ qQ. FIQu)
-fr8nnI8 ~ Slack
- "\lI..10 ~..8 Tltmp.
......Nw",b.J ..iA, H..e QF
\D 2.1 114Q.O 40 , .e;.
IhLJ1 '~1 1.5"
1 '3
I I{ I; l1 5.0 1.5
13... I') IoIJ () S.O \.5
'410 '~j ~.8 r;.o 1.$
l\tt'l5 I hO"7.c:\1 5,0 1.5
11j.~1J \~3C;,~ "',0 \0'5
'''58 ~1a5S.(o ..,.0 1.5
\5' 0 IlD13 II ~.o \.~
,~ O \"71 {J:/ ;'0 \,5'
'';\4 lD 11 't.\. 7 '.0 \05
\.., ") ' 8.1 t 0 1.5
IIPlo 11C; ; .n 1.5
~; 111 ,q 1,0 I.~
I'> Lt 0 \.,<:f\ .'1 ,,0 /.1)
fII~c; I s:l2' t.' 5,0 I..;"
;3
4;
fto
"5
qo
Z10
281;
~O
3\5
334
3~B
~O
~
~'11r1
~t)r;-
if''lO
"t35
tfg)
£.11,5
46t> \1 '0
,.0
UHS.41
IS
Md '" (0.44 x %C02) ... (0.32 x %02) ... (0.28 x %Nz)
~ Md '" (0.44 x ) + (0.32 x ) + (0.28 x
(,B
72
% H20 % H20
l' MI",Mdx(I,-~.'8(-;
V1 1 00 100
,'"' Mlc! )X(I- -) ...,8(-1
100 100
PA>
MI -
f,3
8'i TI -
Md =
OF.
OR (oF. 4601
111\
PI - Pb + ~.. (
13.15
13.15
) +
- PI=
in. Hg
ab -
~1 IF? =
&'-
~ VI - 85.49 x Cp x .flji x
BS
65
lOb VI - 85.49 x (
Bio
8 ~ VI-
as
11 AI-
11
'7 01. VI xAn so 11m
18
"'18 CI .
~
,'\ CI .
8() Ps" ~O
DO Oa td= 08 x 17.1147 x - x (1. -)
0, ra 100
Be
B\
81 Oa,tct'"
~t>
1'\ 081tc:t.
1"
Ts fA)
PI x Ms
) x (
)x~
/tI1
ft2
x
xeo
acfm
x(1.-)
'00
x 17.547 x
-------
-~--- ~--_.-
Plant $..., \\ \\\ oJ\ SiGt L
Sampling Location -':+IV(,. ~"\
Run Number:~~ '" ~\S.-" Dale: ~-I/.., 'I
Pretest leak Rate: . 0 \ cfm @ !S in. Hg.
Pretest leak Check: POOt: l O~: v
FIELD DATA SHEET
r~) 1 ~
. LIS"
Sample Type: \vi. ~\ 5 Operator: G c.,,"1 Nozzle ID: JlIf' Thermocouple II: R P l-<:J
Pbar: .;2.'1,1 Ps: - 1. .1... Assumed Bws: L Filter II: "0 731 ?- 6..$
C02: Q 02: ':1-\ '1""""-< MeterBox#:L- y:I.O/Ll\H@: ) (s~
Probe LengthlType: \0' 't",> Pitot II: t P 10 Post-Test Leak Rate: ,00' cfm @.s in. Hg. l~t..f~
- - {3f!L.'\
Stack Diameter: \ \ \- As: 1 () '1'6 Post-Test leak Check: Pitot: ~ Orsat: V
Trav... Sllmplng Oock TII118 Gas Meter Velocity Orifice Pressure Differential Stack Temperature Impinger Dry Gas Meter Temp. Pump
PoInt T1m8 (24-hour Reading Head (6p) (6H) in H2O Temp. of Temp. Inlet Outlet Vacuum
tbnber (mln) dock) (Vm) ft S In H2O Desired Actual (Ts) Probe Filter of (Tm in°F) (T m out oF) (in. Hg)
I 0 \0)5 f ~ s ,., S\a ;//////////// / / / / / / / / //, '///// r-Y/////////// / / / / / / / / / / / /7 / / / //
./1,. \ 'b) ') ~qlf.,) . ,1'1. - ~ . ot ,n4- I 0 I 1.51-- -:2<; (. 61 , 4- '7 t 2
\G)~ \O~ ..5I}-.-G\ I , ~ I ~.5 ~ ; - ~!»)- ?-5 l) 61'1 'I " :.--.
\ l"1 \0 '-b 9'1 'U ,:). . 0 1- -" 4- '04-- \q.~ i ~~ Z-- 1-( I J '1 11 15 ""L-
, ot, ~ .~ 4- ,q . ~ 1 }1.s I 'd51f-- ")..q..~ " ...." 75
- I -
\ rn:$ ~ .'1 bO,~ \ .(;t~ ~ .04-- I ?-t...r ,. })
.0'- I&L! 1.S). 0~ 'L
"1.. }, ,10 -'L C'fo1.., .oL , D ~ ~t. I" f I '1..S r 1<;,-, f>~ r ')s '7t:. "7
L Ilo(.. £'\0) .~ . ,,5. \.~ '.-5 ?-III ~ "1. .. "t "-$ 3 JL Ii 1f.. ~
lIo"8 qb~.b .oL .04- . Oct ) ~~ ".l-,r 0 1$5 .f"" 7C1 16 ..,
\ \ \ t... '" c<... .q-S \,.5 1.< ~Tb '1.5"- Xv f) ,q 7b cL
dli ()[ Q (., "\ .0 L .oL , () L \ 1-). ')..~4- "-$'}... J"~ I( 7'- 'L
\' ~lt:! '\ a, 1 . "\.5 11~. I. S' :!. 1...0 """l j~ ) s ~ 5)' ?A ), 4-
1\)" C\ 0\.1 'oL ',0 /:- .o~ i z... 1... ..;1.$1,. J. .s).. r-" .,'\ J(... It-
~ \\ ~o "\ oC\ ,4- .0 L .o~ .() {. I I J' :l.H )54. S'¥ '7&f 1i }
\\ ~ 1 ~IU,~ 1.1.- \. "'\ \.1 ~c.' ~)S .;lJ$ $4- 7' l' 3'
\ \ 'VI ~~\.,,\ ,01.- , () ~ .0(.. I \ e--5r )..-s ~ J't )~ lL <:
\\ (1"'1 ~\s. \; .ot.. '04- ,() ~ \ Y1 '')..5 '- ')...S~ 5') 7~ 71: "3
4- \ ''':00 ,\11. b . () '\.. 'Q'- (') j; \,Il 1.S S" }S~ S::> 7, 71. ?
\').\) ~ G\\',1 \,1- \. i 1,1 l»o'f ')...S")- J.S, J'S ~)- ,.., ~
\ 1..0<0 G\,,,,, L ' o}. ,oc... '06 \3 L ~) )..s"y .rs g'l 7, '-
I'). \~ ",'}.~.6r- \ , 1. \ . Ie. ,. -J J \~ 1-S L 'J.rJ .r~ $'~ 7'" _r
\').. \~ 0..').."1.0 - t)")... lOt.:. .....<0 \),,:t 1- 4- '\ 'J S)- -S1 a 1- IY 1-
\).,.., C\.1-'- ~ ,I;:) '- Q\o (:)<. \\) '}..!'o ""5~ "1J ~v 7~ I
S \')-')5 I\",";I."\., \.1.- \.i \." '}, '). '" '\.~ \ 1-5').- .:rfi ~"- ."t .s
\. ,. "\." t1'\ '\.- "".c.. , 1:> ';Ir- .h(n -OVJ \ 3~ ~c,.~ "'Y.s"). 51 ~).- 171 ~
\'\.. ~~ 0.. '}. So,~ . 1'11. -0(", . ()fo \ \ 4- ')5> )~1 J'Cj f}. 7
-------
~ ~ -~ ,S .- \
Page
l'est Dale: ___~~l~_\l__.._._---
Operator: ~~~~
<-
or
Lf
Plant Name:
Run Number:
~~..,.~,,\,."" ~\~'-
-"---.. _.
Traverse Somp11nc / Cod< Thac Gas Meter Velocity OurlCe P.es. nine.callal Slack Probe Impinger Dry 015 MCler TClllp. Pump
Pulnl Time, (24-hour Readinl lIead ~p.) (cll) IlL IIJO Temp. 8 F Tcmp. I Filler Tcmp. Inlel Uullel Vacuum
Number (min.) doc:t) ('" ) It J ilL 1120 Desired Aduat ft) Temp.. F of ("L.. ). F (li.....) of In. IIg
..s I \).\\:) ~}\. ~ \,L \..q \, -? ~1-h ').d.'i 1 ?oS, ~~ $?.,- 1'i S
\'}'it I b- 4. "\- '" )-u, - '0 .o~ ,Q'o ,0'0 tOt ?-.> 0 1,,:,s 6b ~J 7 'X ""2-
{" I I 'L~ o~ 'Ob II , ).s..r 1).51. S'1 9).- 7y ?...
I ,~(O '\ ~ ~.'\ . ""L \. \ \~ 3SS ~ 3 I ),(,5 S'1$ ~J--.. 1'1 .5
I \~(L '\'t.S.JI .0"-, .0(. ,0 C:, \\0 ""~1 I '}...SJ SI g) 7'1J "L
I. I \~ LO '\ M.. f... .0 <. 'Ob .o~ 'C>(I. ')ss 1'')-57 J'~ .9:S 7 r 1
I \ ~ ~<\ '\ ~1,' , :tt '-. \.i \ .~ ~"l.' l)] I -:1--\ 1, .or (. ~3 7~ 5-
I ,~~\ -1 - .o'\., .o\.. .0(" \ \ l) )S~ I).!; 5 s{. . ~ \1- \'i \."ir ~ ~4- '}() I ')S R j"J. ¥1- i Y b
I \~fr", a.~\,\. -.., '1", .ne.. . nl'..... , , \a :LS-S I )..s) $] fj)J.- 7~ L
I \ ~.s\.. <1 H.5 -0",\ .0(. '06 \13 1- 4-0 I 'J....}<. .S" "- ,';). ., , J...
I \ ~ 5h !\. ~5. i I ,') \ . -jl \-,~ ~.:c,~ 1-S \ I ')..~_S $")- 'in- 7'1 ,
I \ ~1~ "-\-1,\ .0 \ fiG-. .OQ . \...... ").~ ~ '?-f.) ..r."r- I).. ?CJ ~
I \W~ f.\. ,'( '" \~ "~ \ ~ ~ 'If '}S J I }oS 5" .3r B )., 1 C; .b
.1 \ "'Oil 0... a,~.~ .0"" .O\a .O\:) \}5 "'-5 \ I ~.\.. S't f~ 7 <; "2-
~ li;i \ 4-\S ,,( t, 0 .01., O~ b~ I \ 'r ').50 I ~2S- -1'" ~~ J~ 1
I \ \\h 'tSt. 4.. . '\s \, f\.- \.4- ~ ~y '}-Sf I 7--.J'b Iy 5l.J 7 cl ,
I ,~\~ t\.s). . ~ \o~ . n{o . ()("... ".., ')..\-~ I ')-J.., :f"'\ ~> 7<\ "L-
I \~ '\ s~.~ . "\ <., ',f)... \\ ~ "0 ')..!,~ I ').~ J- SOl t\-- ,'1 10
-------
l,("Ik. ,he(.
- 0.152.
«cf
,~
~o
Page
of -4:.-
.3
Plant Name:
Run Number:
~"" \\ \\.'---- ~ ""'\~ ~
Test Date: --~~-L_,-- --.--...--- -.--..-,
Operator: G G-Atf
'0 ~ \"'\ '?\ <) , \
Traverse S...pllnc / Cod< n.. Oas MeIer Velocity Orifice Pres. DifrereDliai Slack Probe Impinger Dry Oas MeIer Temp. Pump L ~"(( V
Poinl Time. (24-hour Readinl I lead ~ P,) (till) In. 1120 Temp. 8 F Temp.' Filler Temp. Inlet VUliel Vacuum '"
Number (min.) dock) (" ) It J In. 1 b 0 Desired Adual (1;) Temp.- F 8F rr....)8 F ('Ii.....) 8F In. III "
'"
"- ~ I \ 'r)~ <1~j.i\ .I;)? ,CIo {\ to , 1'1 '). ~ ' '"} 5") -~ ')'~ IQ 'L r;/'
I 144:>- C\&q<; ,n" () {, Ob lOG ? \~ ' )oS}- Sc; .. 81- 8'", '- f t)t/8
r< I ,\.S+- ,(f, n~ '2. 'l')~ ,dc:. '0 (, I"h :J-,sO' ~Sl ~C; Ir' 7l'j <-
If"'" I '-'~\.1Q4 I ~'I
, I l'1lV, - .f"'I "1., .0(" . O£., I \l") :2$':>Jl h':o 7'i/ 73 Z ' c:JD /
I \ 111) iC\r,,'). S . (') "::7 (')~ b"- lOG -:15 ~ I '-56 '0 7q 7(( 1.
, \1 " 'Ie, \,..5 \.i) ~~r U>';)5' CoD l' 7 if S
I ,1,'1, 4 (c 1.., .C\ -(I), -0(-, IO~ \ ?, --> ) S).- , ?oS.., .sc, '19 7}f L
I \')}y qc,c" Q .0\'\ \.5 \.5 ~;).S )..I\b'?-$ 1. S~ g;.- ~o 5'
I \1~A. "(ftc.. <\ ,0::> t)(..., r () c; \?:r. ':1.5ll I -:l5J S-c, ~L ~" 2...-
?- I \1')..\ --- .n~ ,Ok. In" '10 ~s' ).(0 s~ fS1- ~ , ?
I \1:\)- q In i. 1.. ,n~ Oe) f\c.... \05 ~ J. I '1-5- .f8 8 i ...- |
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