UNITED STATES ENVIRONMENTAL PROTECTION AGENCY OFFICE OF ENFORCEMENT EPA-330/9-80-001 PESTICIDE FORMULATION METHODS INDEX July 1980 Dean F. Hill NATIONAL ENFORCEMENT INVESTIGATIONS CENTER Denver, Colorado ------- FOREWORD This Index is intended solely as a guide to the published and other- wise generally available methods for pesticide formulation and related analyses. Listing of the methods or their order of appearance does not imply any degree of EPA approval or lend to the methods any additional degree of status than they intrinsically possess. It should be kept in mind, however, that AOAC procedures are currently the only "Official" methods available. Many of the referenced procedures are obviously obsolete or will rarely find use due to the availability of newer and better methods, changing pesticide use patterns and regulatory restrictions. However, as many methods as posrible were listed, as there may be occasions, particu- larly for mixtures or other problem formulations, where some other than the normal approach may be necessary. Also, if possible, suspected chemical violations should be confirmed by several different methods. The analyst may find another convenient method listed here of which he or she was not originally aware. No attempt has been made in the Index to include more than a minimum number of chemical names in the main listing most of the pesticides are listed by their official, common, or in some cases, trade names. Chemical names may be located and/or verified via the cross-reference numbers given with each chemical by reference to: "Acceptable Common Names and Chemical Names for the Ingredient Statement on Pesticide Labels" Fourth Edition, Blaylock, C. R. et al, EPA 540/9-77-017, December 1979 (available from: NTIS, Springfield, VA 22161). Copies of the referenced methods (particularly those designated NEIC) may be obtained by request from the National Enforcement Investigation Center, Denver Federal Center, Building 53, Box 25227, Denver, Colorado 80225, (303/234-3751). The references cited in compiling this Index are abbreviated as follows: ------- 2 1. AOAC-13: Official Methods of Analysis of the Association of Official Analytical Chemists, 13th Edition, 1980. Published by the Association of Official Analytical Chemists. P.O. Box 540, Benjamin Franklin Station, Washington, O.C. Supplements issued annually. 2. EPA: Manual of Chemical Methods for Pesticides and Devices, Environmental Protection Agency, Office of Toxic Substances, Pesticide Programs, Benefits and Field Studies Branch, Beltsville, Maryland. First Issued 1974 and updated regularly. Available from the Association of Official Analytical Chemists. 3. Zweig I-X: Analytical Methods for Pesticides, Plant Growth Regulators and Food Additives, Ed. Gunter Zweig, Academic Press, New York. Vols. I-XI. Vols. VI-XI also edited by Joseph Sherma. 4. CIPAC-1 and IA: CIPAC Handbook, Volume I and IA , Analysis of Technical and Formulated Pesticides. Compiled by R. D. Ashworth, J. Henriet and J. F. Lovett, edited by G. R. Law. Collaborative International Pesticides Analytical Council Limited, 1970 and 1980. Published by W. H. Heffer and Sons Ltd., Cambridge, England. 5. AWPA: American Wood-Preserver's Association Standards. Published by the American Wood-Preservers Association, 1012 - 14th Street, N.W. , Washington, D.C. 20005. Revised periodically. ------- 3 6. NEIC: These methods are various analytical procedures on file at the National Enforcement Investigations Center that do not fit into any of the pre- vious categories. These methods are derived principally from industrial sources, but also include EPA and State developed methods. State methods are designated by the two-letter abbreviation after the reference. Journal methods other than the Journal of the Association of Official Analytical Chemists are also included in this category. If any laboratory using this Index has methods available that would be useful for inclusion, please send copies to Dean F. Hill at the National Enforcement Investigations Center and to Warren Bontoyan at the EPA Belts- vine Chemistry Laboratory. It would be particularly desirable to have methods listed for those compounds where none are given or where only elemental or other non-specific methods are listed. Dean F. Hill Pesticide Products Program Coordinator, NEIC ------- A-l Abate (See "Temephos" 1921) Acaralate (See "Chloropropylate" 492) Acarol (See "Bromopropylate" 259) Acephate (3) 1. GLC (TCD-IS) Zweig VII; p. 364 2. GLC (FID-IS) NEIC-3-1 (HI) 3. GLC (FID-IS) NEIC-3-2 Acetic Acid (4) 1. Titrimetric (in Acetates) NEIC-4-1 2. Titrimetric NEIC-4-2 Acetic Anhydride (5) 1. Titrimetric NEIC-5-1 Acetochlor (6) Acetone (7) 1. GC AOAC-13; 36.007 2. GC AOAC-13; 5.012 3. Qualitative Test NEIC-7-1 Acrolein (14) Acrylonitrile (15) Actidione (See "Cycloheximide" 601) Aerosol Containers 1. Non-volatiles (High-Pressure) NEIC-AER-1 2. Non-volatiles (Refillable High-Pressure) .... NEIC-AER-2 3. Non-volatiles (Low-Pressure) NEIC-AER-3 4. Flame Projection Test NEIC-AER-4 5. Drum Test (Flammabi1ity) NEIC-AER-5 6. Direct Sampling AOAC-13; 6.002 Agritox (See "Trichloronat" 1090) Akton (413) 1. GLC NEIC-413-1 2. IR NEIC-413-2 Alachlor (16) 1. GLC (TCD-IS) EPA-1-Tent. 2. GLC (FID-IS) EPA-2-Tent. 3. IR NEIC-16-1 4. GLC (FID-IS) Zweig X; p.257 Alanap-1 (See "Naptalam" 1470) ------- A-2 Alar (See "Daminozide" 619) Alcohols 1. GC NEIC-Alc-1 2. GC AOAC-13; 36.007 Aldicarb (18) 1. IR AOAC-13; 6.315 2. Colorimetric JAOAC 49,399 (1966) Aldrin (19) 1. Total Chlorine AOAC-13; 6.177 2. IR (HHDN) AOAC-13; 6.182 3. GLC Zweig VI; p. 268 4. IR NEIC-19-18 (VA) n-Alkyl Dimethyl benzyl ammonium Chloride (See "Quaternary Ammonium Chlorides") Allantoin (82) d-trans-Allethrin (84) 1. Titrimetric AOAC-13; 6.149 2. GLC (d-trans) AOAC-13; 6.155 3. GLC (FID-IS; with Resmethrin) NEIC-84-1 4. GLC (Mosquito Coils) NEIC-84-2 5. GLC (Mosquito Coils) NEIC-84-3 6. GLC (Pynamin-Forte, Mosquito Mats) NEIC-84-4 (HI) Allyl Alcohol (85) 1. IR CIPAC-1; p. 730 2. IR (with D-D Mixture) NEIC-85-1 Allyl Isothiocyanate (86) Alphachloralose (2015) 1. Total Chlorine NEIC-2015-1 2. Titrimetric NEIC-2015-2 3. Colorimetric NEIC-2015-3 Alpha-Naphthylthiourea (1472) 1. Titrimetric CIPAC-1; p. 16 Altosid (See "Methoprene" 1329) Aluminum Phosphide (92) 1. Titrimetric NEIC-92-1 2. GLC (FPD/PH3 Evol'n) (See "Zinc Phosphide/EPA-2") Ametryn (94) 1. Non-Aqueous Titration Zweig IV; p. 15 2 GLC AOAC-13; 6.431 3. GLC (FID-IS) NEIC-94-1 ------- A-3 Amiben (See "Chloramben" 374) Arnical 48 (See "Diiodomethyl-p-tolylsulfone" 853) Arnical 77 (See "p-Chlorophenyl diiodomethylsulfone" 463) Amidithion (95) Amiriobutane (See "sec-Butylamine: 281) Aminocarb (870) 1. IR NEIC-870-1 2. GLC (FID-IS) NEIC-870-2 4-Aminopyridine (104) 1. UV EPA-1 2. GLC (Sunflower Seeds) NEIO104-1 3. GLC/TLC (Corr.) NEIC-104-2 3-Amino-s-triazole (See "Amitrole" 106) Amitraz (105) 1. GLC/IR (Cattle Dips) JAOAC 61,1516(1978) Amitrole (106) 1. Titrimetric A0AC-13; 6.318 2. Colorimetric EPA-1 3. Colorimetric (with Simazine) NEIC-106-1 Amizine (See "Simazine" 1816) Ammate (See "Ammonium Sulfamate" 125) Ammoniacal Copper Arsenite 1. Ammonia AWPA; A2-71-1 2. Arsenic AWPA; A2-71-2 3. Copper AWPA; A2-71-6 Ammonium Sulfamate (125) 1. Titrimetric EPA-1 Ammonium Sulfate (126) 1. Titrimetric NEIC-126-1 p-tert-Amylphenol (131) and Potassium Salt (132) 1. GLC (See "Phenols and Chlorophenols/EPA-6-Tent. & EPA-8-Tent.") 2. HPLC NEIC-131-1 3. HPLC (RP) NEIC-131-2 4. HPLC (RP) NEIC-131-3 Anabasine (134) ------- A-4 Ancymidol (135) 1. GLC (FID-IS) Zweig VIII; p. 477 Anethole (136) Anfor (782) 1. GLC (TCD-IS) NEIC-782-1 Anilazine (685) 1. Labile Chlorine (See "Chloro-Triazine Herbicides/EPA-1") 2. IR EPA-l-Tent. 3. CLC (TCD-IS) EPA-2 Tent. 4. Hydrolyzable Chlorine Zweig III; p. 81 Animert (See "Tetrasul" 487) Anthio (See "Formothion" 884) Antimony Potassium Tartrate (141) 1. Titrimetric (See "Zinc Phosphide/EPA-1") Antimycin A (142) 1. UV EPA-l-Tent. ANTU (See "Alpha-Naphthylthiourea" 1472) Aramite (307) 1. Total Chlorine Zweig II; p. 36 2. Sulfite Generation/Titration NEIC-307-1 A-rest (See "Ancymidol" 135) Arochlors (See "Polychlorinated Biphenyls" 1666; 1667) Arsenic 1. Titrimetric (DSMA, etc.) EPA-1/3/4 2. Titrimetric (Inorganics) EPA-2 3. Distillation (Inorganics) AOAC-13; 6.005 4. Ion-exchange (Inorganics) AOAC-13; 6.010 Arsenic (Water Soluble) 1. Titrimetric (Inorganic Arsenicals) AOAC-13; 6.013 Aspon (1960) 1. IR NEIC-1960-1 2. GLC NEIC-1960-2 3. TLC/Total P NEIC-1960-3 4. IR NEIC-1960-4 (VA) Asulam (154) & Na Salt (155) 1. Non-Aqueous Titration Zweig VII; p. 499 2. UV EPA-l-Tent. ------- A-5 Atraton (1032) 1. Titrimetric Zweig IV; p. 28 Atrazine (156) 1. GLC AOAC-13; 6.431 2. Labile Chlorine (See "Chloro-Triazine Herbicides/EPA-1") 3. IR EPA-1 4. GLC (FID-IS) EPA-2 5. HPLC (RP-IS) NEIC-156-1 Avadex (See "Diallate" 682) Available Chlorine 1. Titrimetric (NaOCl) AOAC-13; 6.111 2. Titrimetric [(Ca(0Cl)2] AOAC-13; 6.117 3. Titrimetric (Chloramine T) AOAC-13; 6.118 4. Titrimetric (Cleansers) NEIC-AvCl-1 5. Titrimetric (Cyanurates) NEIC-AvCl-2 Avenge (See "Difenzoquat" 838) Azak (See "Terbutol" 670) Azinphos Ethyl (828) 1. GLC Zweig VI; p. 397 Azinphos Methyl (899) 1. IR EPA-1 2. Colorimetric Zweig II; p. 233 3. GLC Zweig VI; p. 397 4. IR AOAC-13; 6.A09 5. HPLC NEIC-899-2 Azobenzene (159) Azodrin (See "Monocrotophos" 901) Azothoate (461) ------- B-l Bacillus Thuringienisis (161) Balan (See "Benefin" 299) Banamite (188) 1. GLC (FID-IS) NEIC-188-1 Bandane (1669) Banol (See "Carbanolate" 507) Banvel D (See "Dicamba" 671) Banvel T (See "Tricamba" 2004) Barban (164) 1. UV Zweig IV; p. 40 2. HPLC NEIC-164-1 Barium Metaborate (167) Barthrin (168) Basalin (See "Fluchloralin" 1106) Baygon (See "Propoxur" 1238) Bayluscide (See "Clonitralid" 707) Baytex (See "Fenthion" 1098) Benazolin (451) Bendiocarb (172.5) 1. IR EPA-l-Tent. 2. UV EPA-2-Tent. 3. GLC (FID-IS; Pyrolysis) Zweig X; p. 6 4. IR (for Phenolic By-product) Zweig X; p. 8 5. Preparation of Analytical Standard Zweig X; p. 9 6. HPLC (Wool) JAOAC 63,47(1980) Benefin (299) 1. GLC AOAC-13; 6.209 2. UV AOAC-13; 6.203 3. IR EPA-1 4. GLC (FID-IS) EPA-2-Tent. 5. GLC (Separation from Trifluralin) NEIC-299 6. GLC (FID-IS) Zweig VIII; p. 342 Benfluralin (See "Benefin" 299) Benlate (See "Benomyl" 173) ------- B-2 Benomyl (173) 1. IR EPA-1 2. UV EPA-2-Tent. 3. Colorimetric JAOAC 58,971(1975) 4. IR Zweig X; p. 159 5. Non-Aqueous Titration Zweig X; p. 162 6. UV (also determines MBC) JAOAC 62,488(1979) 7. HPLC NEIC-173-1 (CA) Bensulide (862) 1. GLC Zweig VI; p. 672 2. IR EPA-1 3. IR NEIC-862-1/2 Bentazon (174) 1. UV (also Sodium Salt) EPA-l-Tent. 2. GLC NEIC-174-1 Benthiocarb (See "Thiobencarb" 1968) Benzadcx (175) Berizal dehyde (177) Benzene (178) 1- GC AOAC-13; 5.012 Benzene Hexachloride, Gamma Isomer (See "BHC, Gamma Isomer" 1282) Benzipram (180) « 1,2-Benzisothfazolirj-3-one (See "Proxel" 181) Benzocaine (1031) 1. Colorimetric AOAC-13; 38.138 2. Titrimetric AOAC-13; 38.143 3. UV AOAC-13; 38.144 Benzoic Acid (182) Benzothienyl Methyl carbamate (187) 1. Hydrolysis/Distillation NEIC-187-1 6-Benzyladenine (1629.5) 1. TLC Zweig X; p. 549 Benzyl Benzoate (191) 1. GLC NEIC-191-1 ------- B-3 Benzyl Bromacetate (192) 1. GLC NEIC-192-1 o-Benzyl-p-Chlorophenol (193), K Salt (194) & Na Salt (195) 1. GLC (See "Phenols and Chlorophenols/EPA-6-Tent. & EPA-8-Tent.") 2. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 3. HPLC NEIC-193-1 4. Non-Aqueous Titration NEIC-193-2 8etanal (See "Phenmedipham" 1588) Betasan (See "Bensulide" 862) BHC, Gamma Isomer (1282) 1. IR AOAC-13; 6.198 2. Column Chromatography AOAC-13; 6.192 3. IR EPA-1 4. Hydrolyzable Chlorine CIPAC-1; p. 986 5. Polarography CIPAC-1; p. 37 6. GLC NEIC-1282-1 7. IR NEIC-1282-2 (VA) BHC (179) 1. IR AOAC-13; 6.198 Bidisin (See "Chlorfenprop-methyl" 1345) Bidrin (See "Dicrotophos" 900) Bifenox (200) 1. GLC NEIC-200-2 Binapacryl (201) 1. IR EPA-1 2. Colorimetric Zweig V; p. 236 3. GLC (TCD) NEIC-201-1 Biobor (1548) 1. Titrimetric NEIC-1548-1 Bioquin (See "Copper 8-Quinolinolate" 560) Bforesrnethrin (See "Resmethrfn" 1773.5) ------- B-4 Biphenyl (202) 1. UV JAOAC 40,282(1957) 2. GLC (FID-IS) NEIC-202-1 3. UV (Fruit Wraps) NEIC-202-2 Birlane (See "Chlorfenvinphos" 412) Bis(tributyltin)oxide (229) 1. Titri metric EPA-1 Bithionol (1971) 1. UV NEIC-1971-1 Bladex (See "Cyanazine" 422) B-Nine (See "Daminozide" 619) Bolero (See "Benthiocarb" 1968) Bolstar (1078) 1. GLC (FID-IS) AOAC-13; 6.A32 2. GLC (TCD) NEIC-1078-1 Bomyl (886) Bone Oil (239) Borax (240) 1. Titrimetric (See "Boron Compounds/EPA-1") Bordeaux Mixture 1. Moisture AOAC-13; 6.067 2. Carbon Dioxide AOAC-13; 6.068 3. Copper (Electrolytic) AOAC-13; 6.070 4. Copper (Titrimetric) AOAC-13; 6.071 Boric Acid (241) 1. Titrimetric (Organic Matter Present) EPA-1 2. Titrimetric (Fluorine Present) EPA-2 Boron Compunds 1. Titrimetric (Inorganic) EPA-1 Botran (See "Dichloran" 704) Bravo (See "Chlorothalonil" 497) Brodifacoum (242.5) 1. HPLC NEIC-242.5-1 ------- B-5 Bromacil (243) 1. GLC (FID-IS) EPA-l-Tent. 2. GLC (Oil-Base, with Pentachlorophenol) NEIC-243-1 3. IR (Hyvar X) NEIC-243-2 4. IR and UV (with Diuron) NEIC-243-3 5. HPLC (Oil-Base, with Pentachlorophenol) NEIC-243-4 6. HPLC (Oil-Base with Pentachlorophenol) NEIC-243-5 7. Non-Aqueous Titration. . Zweig V; p. 62 8. HPLC (Pentachlorophenol & 2,4-D-IOE) NEIC-243-6 Bromeflor (See "Ethephon" 1018) Brominated Salicylanil ides (863) 1. UV EPA-1 Bromophos (254) 1. IR CIPAC-1; p. 730 2. GLC NEIC-254-1 3. Titrimetric Zweig X; p. 33 Bromophos Ethyl (253) 1. Titrimetric Zweig X; p. 43 Bromopropylate (259) 1. GLC NEIC-259-1 Bromoxynil (261) 1. GLC Zweig V; p. 354 2. Total Bromine Zweig V; p. 353 Bromoxynil Octanoate (262) 1. GLC (FID-IS) AOAC-13; 6.A01 Buctril (See "Bromoxynil" 261) Bufencarb (263) 1. GLC Zweig VII; p. 181 Bupirimate (264) 1. GLC NEIC-264-1 Busan 72 (1973) 1. Colorimetric JAOAC 59, 737(1977) 2. IR NEIC-1973-1 Busan 73 (440/1389) 1. Titrimetric NEIC-440/1389-1 Busan 74 (1210/1973) (See also "Busan 72") 1. Titrimetric & IR NEIC-1210/1973-1 ------- B-6 Busan 76 (586) 1. Hydrolyzable Bromine NEIC-586-1 2. GLC NEIC-586-2 Busan 77 (1684) 1. Titrimetric (27.3% Chloride) AOAC-13, 6.440 Busan 90 (255) 1. Hydrolyzable Bromine NEIC-255-1 Busan 881 (1715) (959) (1046) 1. Total Nitrogen NEIC-1715/959/1046-1 2. UV NEIC-1715/959/1046-2 Butachlor (265) Butam (266) Buthidazole (271) Butonate (914) Butoxypropylene Glycol (276) Butralin (278) 1. GLC (FID-IS) NEIC-278-1 Buturon (See "Chlorphoxin" 470) sec-Butyl amine (281) 1. Distillation/Titration Zweig VIII; p. 253 2. UV Zweig VIII; p. 255 3. Colorimetric JA0AC 61,1001(1978) Butylate (1039) 1. GLC AOAC-13; 6.426 2. GLC (TCD) EPA-l-Tent. 3. HPLC EPA-2-Tent. 4. GLC (FID-IS) EPA-3-Tent. 5. GLC (FID-IS) EPA-4 6. GLC (TCD-IS) EPA-5-Tent. 7. HPLC EPA-6-Tent. p-tert-Butylphenol (304), K salt (305) and Na salt (306) 1. GLC (See "Phenols and Chlorophenols/EPA-8") Bux (See "Bufencarb" 263) ------- c-l Cacodylic Acid (310) & Na Salt (311) 1. Polarography AOAC-13; 36.038 2. Titrimetric (See "Arsenic/EPA-4") 3. GLC NEIC-310-1 Cadium 1. AA EPA-1 Calcium Arsenate (323) 1. Arsenious Oxide (Titrimetric) AOAC-13; 6.052 2. Total Calcium (Titrmetric) AOAC-13; 6.055 3. Total Calcium (Gravimetric) AOAC-13; 6.056 Calcium Hypochlorite (333) 1. Titrimetric AOAC-13; 6.117 Calcium Polysulfide (340) 1. Gravimetric (Water Soluble Sulfur) AOAC-13; 6.103 2. Thiosulfate Sulfur (Titrimetric) AOAC-13; 6.105 3. Calcium (Gravimetric) AOAC-13; 6.110 Camphor (346) Capsaicin (350) Captafol (351) 1. IR EPA-l-Tent. 2. GLC Zweig V; p. 295 3. HPLC Zweig X; p. 173 4. GLC Zweig X; p. 175 5. IR CIPAC-1; p. 730 Captan (352) 1. GLC AOAC-13; 6.215 2. Hydrolyzable Chlorine EPA-1 3. IR EPA-2 4. GLC Zweig VI: p. 546 5. GLC (with Malathion and Methoxychlor) NEIC-352-1 6. IR CIPAC-1; p. 172/174 7. GLC (FID-IS) NEIC-352-2 8. HPLC (Flowables) NEIC-352-3 9. HPLC (Si 1 ica-IS) AOAC-13; 6.A09 Carbanolate (507) 1. UV . . Zweig V; p. 204 ------- C-2 Carbaryl (353) 1. IR AOAC-13; 6.320 2. UV EPA-1 3. HPLC EPA-2-Tent. 4. HPLC JAOAC 57,648(1974) 5. Colorimetric JAOAC 53,896(1970) 6. Near IR JAOAC 51,370(1968) 7. Colorimetric JAOAC 54,128(1971) 8. Methyl amine Distillation NEIC-353-1 9. HPLC (with Malathion, Folpet and Dicofol). . . . NEIC-353-2 10. HPLC (IS) NEIC-353-3 11. IR NEIC-353-4 (VA) 12. HPLC (Si) JAOAC 63, 650(1980) 13. HPLC (By-product Assay) CIPAC-1A; p. 1112 Carbetamide (354) 1. Hydrolysis/Distillation Zweig VII; p. 511 Carbofuran (355) 1. IR 2. GLC 3. Dimethylamine Distillation 4. HPLC 5. Colorimetric 6. GLC EPA-1 Zweig VII; p. 190 NEIC-355-1 NEIC-355-2 JAOAC 61,1513(1978) NEIC-355-3 Carbon Disulfide (359) 1. GLC A0AC-13; 6.143 Carbon Tetrachloride (360) 1. GLC AOAC-13; 6.143 2. IR AOAC-13; 36.013 3. GLC (FID) NEIC-FUM-1 Carbophenothion (361) 1. UV Zweig II; p. 548 2. GLC Zweig VI; p. 519 3. IR NEIC-361-1 (VA) Carboxin (362) 1. IR EPA-l-Tent. 2. UV EPA-2-Tent. 3. HPLC NEIC-362-1 4. IR Zweig VIII; p. 321 5. Titrimetric Zweig VIII; p. 322 6. TLC/UV JAOAC 61,971(1978) Carbyne (See "Barban" 164) Cartap (871) 1. Polarographic Zweig VII; p. 373 ------- C-3 Carzol (See "Formetanate" 1116) Casoron (See "Dichlobeni1" 678) CDAA (649) 1. Total Chlorine Zweig IV; p. 193 CDEC (396) 1. Total Chlorine Zweig IV; p. 249 Chlomethoxyni1 1. GLC Zweig X; p. 269 Chloramben (374) 1. UV AOAC-13; 6.188 2. Titrimetric Zweig V; p. 325 Chloramine T (381) 1. Titrimetric AOAC-13; 6.118 Chloranil (382) 1. Reduction/Titration Zweig III; p. 29 Chlorazine (383) 1. GLC JAOAC 61,161(1978) Chlorbenside (384) 1. IR CIPAC-1; p. 730 2. IR (as Mitox) NEIC-384-1 (VA) Chlorbromurori (385) 1. GLC EPA-l-Tent. 2. TLC/UV Zweig VII; p. 576 Chlordane, AG 1. IR AOAC-13; 6.232 2. GLC (Heptachlor Content) AOAC-13; 6.241 Chlordane, Technical (386) 1. Total Chlorine (Sodium Biphenyl) AOAC-13; 6.220 2. Colorimetric AOAC-13; 6.223 3. Total Chlorine (Sodium) Zweig II; p. 51 4. Composition JAOAC 59,696(1976) 5. Qualitative Test NEIC-386-1 6. IR Characterization CIPAC-IA; p. 1119 ------- C-4 Chlordecone (621) 1. IR NEIC-621-1 Chlordimeform (387) and Chlordimeform Hydrochloride (388) 1. Titrimetric Zweig VII; p. 214 2. GLC Zweig VII; p. 216 3. TLC NEIC-387-1 Clorofenac (See "Fenac" 2050) Chlorfenethol (702) Chlorfenprop-methyl (1345) 1. GLC NEIC-1345-1 Chlorfenson (See "Ovex" 1540) Chlorfenvinphos (412) 1. GLC NEIC-412-2 2. GLC (FID-IS) CIPAC-1A; p. 1132 Chlorflurazole (796) Chlorflurecol (428) Chlorflurecol-methyl 1. TLC/UV Zweig X; p. 527 2. GLC & HPLC JAOAC 60,728(1977) Chlorinated Camphene (See "Toxaphene" 1986) Chlorinated Hydrocarbon Contamination 1. TLC A0AC-13; 6.027 2. Qualitative Tests NEIC-C1HC-1 3. TLC Zweig VII; p. 6 Chlorinated Phenols (See "Phenols and Chlorinated Phenols") Chlorine Dioxide (392) 1. Titrimetric NEIC-392-1 Chlormephos (439) 1. GLC Zweig X; p. 51 Chlormequat Chloride (See "Cycocel" 425) Chlornidine (207) Chloroacetlc Acid (393) ------- C-5 Chlorobenzene (402) Chlorobenzilate (1038) 1. GLC (FID-IS) AOAC-13; 6.431 2. GLC (FID-IS) EPA-l-Tent. 3. GLC Zweig VI; p. 319 4. Total Chlorine Zweig II; p. 66 4-Chloro-2-cyclopentylphenol (408) and Potassium Salt (409) 1. GLC (See "Phenols and Chlorophenols/EPA-6 & EPA-8-Tent.") 2. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 3. GLC NEIC-408-1 4. HPLC NEIC-408-2 5-Chloro-2-(2,4-dichlorophenoxy)phenol (411) 1. UV NEIC-411-1 2. Total Chlorine NEIC-411-2 4-Chloro-3,5-dimethylphenol (See "4-Chloro-3,5-xylenol" 506) Chloroethylene bisthiocyanate (423) Chloroform (427) 1. GLC AOAC-13; 5.012 2. IR AOAC-13; 36.013 Chloroneb (446) 1. GLC Zweig VII; p. 658 l-Chloro-2-nitropropane (449) 1. GLC Zweig V; p. 306 Chlorophacinone (481) 1. UV EPA-l-Tent. 2. HPLC JAOAC 62,1001(1979) 3. UV JOAC 63, 996(1980) p-Chlorophenoxyacetic Acid (454) 1. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.") Chlorophenoxy Herbicides 1. Definition, Structure and Tech. Data EPA-1 2. UV (2,4-D and 2,4,5-T) EPA-2 3. HPLC (Acids and Esters) EPA-3-Tent. 4. GLC (Butoxyethyl Esters of 2,4-D and 2,4,5-T). . EPA-4-Tent. 5. GLC (2,4-D and 2,4,5-TP in Fertilizers) EPA-5-Tent. 6. GLC (as TMS Ester) Zweig VI; p. 630 7. Ester Volatility AOAC-13; 6.032 8. TLC NEIC-ClPh-1 9. TLC NEIC-ClPh-2 10. GLC (Methyl Ester) NEIC-ClPh-3 11. UV ft GLC (Use-dilutions) NEIC-ClPh-4 (WA) 12. HPLC (RP-IS) NEIC-ClPh-5 ------- C-6 p-Chlorophenyl Diiodomethyl Sulfone (463) 1. Titri metric NEIC-463-1 5-Chloro-4-phenyl-3H-l,2-dithiol-3-one (465) 1. UV NEIC-465-1 2-Chloro-4-phenylphenol (471) 1. GLC (See "Phenols and Chlorophenols/EPA-6 & EPA-8-Tent.") 2. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 4 & 6-Chloro-2-phenylphenol (472/473) 1. GLC (See "Phenols and Chlorophenols/EPA-6 & EPA-8-Tent.") 2. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") Chloropicrin (490) 1. GLC (with Methyl Bromide) NEIC-490-1 (CA) 2. GLC NEIC-490-2 Chloropropylate (492) 1. GLC (FID-IS) AOAC-13; 6.431 2. IR NEIC-492-1 (VA) 3. GLC (See "Bromopropylate/NEIC-259-1") Chlorothaloni1 (497) 1. IR (EC and Flowable) EPA-l-Tent. 2. GLC (FID-IS) EPA-2-Tent. 3. IR (Tech. and WP) NEIC-497-1 4. GLC (TCD or FID) Zweig VIII; p. 266 Chlorotriazine Herbicides 1. Labile Chlorine (Pot. Titr'n) EPA-1 Chloroxuron (505) 1. IR EPA-l-Tent. 2. GLC (TCD-IS) EPA-2-Tent. 3. Dimethyl amine Distillation AOAC-13; 6.245 4-Chloro-3,5-xylenol (506) 1. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 2. GLC (See "Phenols and Chlorophenols/EPA-7-Tent.") 3. UV NEIC-506-1 Chloroxynil (699) Chlorphoxim (465.5) Chlorpropham (1243) 1. IR NEIC-1243-1 (VA) 2. Hydrolysis/Titration CIPAC-1; p. 224 3. Total Chlorine (Sodium Reduction) Zweig VI; p. 53 4. GLC Zweig VI; p. 612 5. IR Zweig XI; p. 280 6. HPLC (see "Quintex") ------- C-7 Chlorpyrifos (509) 1. GLC JAOAC 56,1093(1973) 2. IR JAOAC 50,861(1967) 3. IR EPA-l-Tent. 4. UV EPA-2-Tent. 5. GLC (TCD-IS) EPA-3-Tent. 6. HPLC EPA-4-Tent. 7. IR NEIC-509-1 8. HPLC NEIC-509-2 9. GLC (FID-IS) NEIC-509-3 10. HPLC (RP-IS) AOAC-13; 6.B15 Chlorpyrifos Methyl (510) 1. GLC (FID-IS) NEIC-510-1 Chlorthianid 1. Qualitative CIPAC 1A; p. 1160 2. Titrimetric CIPAC IA; p. 1164 Chlortoluron (500) 1. Distillation/Titration AOAC-13; 6.245 2. GLC JAOAC 59,716(1976) Chromated Copper Arsenate 1. Total Chrominum AWPA; A2-71-5 2. Total Arsenic AWPA; A2-71-2 3. Total Copper AWPA; A2-71-6 Chromated Zinc Chloride 1. Total Zinc AWPA; A2-71-12 2. Total Chromium AWPA; A2-71-5 3. Total Chloride AWPA; A2-71-4 Chromi um 1. Colorimetric NEIC-Cr-1 Cidial (See "Phenthoate" 1040) Ciodrin (see "Crotoxyphos" 902) CIPC (See "Chlorpropham" 1243) Cisanalide (517) Clonitralid (707) 1. Colorimetric NEIC-707-1 Codlemone (977) 1. GLC NEIC-977-1 Copper (526) and Copper Compounds 1. Electrolytic AOAC-13; 6.015 2. Titrimetric AOAC-13; 6.016 3. EOTA Titration NEIC-526-1 4. Colorimetric & AA (Water Soluble from Fungicides) AOAC-13; 6.B01 ------- C-8 Copper Acetoarsenite (See "Paris Green" 529) Copper Carbonate (535) 1. Copper (Electrolytic) AOAC-13; 6.063 2. Copper (Titrimetric) AOAC-13; 6.064 Copperized Chromated Zinc Arsenate 1. Total Copper AWPA; A2-71-6 2. Total Chromium AWPA; A2-71-5 3. Total Zinc AWPA; A2-71-12 4. Total Arsenic AWPA; A2-71-2 Copper Naphthenate (550) 1. Electrolytic AOAC-13; 6.066 2. Titrimetric AOAC-13; 6.065 Copper-8-quinolinolate (560) Co-Ral (See "Coumaphos" 814) Cotoran (See "Fluometron" 1107) Coumachlor (8) 1. UV Zweig III, p. 188 Coumafuryl (9) 1. UV EPA-1 2. UV EPA-2 3. UV NEIC-9-1 (CA) Coumaphos (814) 1. IR EPA-l-Tent. 2. HPLC EPA-2-Tent. 3. GLC EPA-3 4. GLC Zweig VI; p. 332 5. UV (As Co-Ral) Zweig II; p. 86 Counter (See "Terbufos" 1924) Creosote (569) m-Cresol (571) Cresylic Acid (574) ------- C-9 Crotoxyphos (902) 1. GLC (FID-IS) EPA-l-Tent. 2. GLC Zweig VI; p. 325 3. IR Zweig V; p. 246 4. IR (with DDVP) NEIC-902-2 (VA) 5. GLC (FPD, with DDVP) NEIC-902-1 Crufomate (575) 1. IR EPA-l-Tent. 2. GLC (TCD-IS) EPA-2-Tent. Cryolite (576) Cupric Oxide (580) Cyanazine (422) 1. IR EPA-1 2. GLC NEIC-422-1 3. Labile Chlorine (See "Chlorotriazine Herbicides/EPA-1") 4. HPLC Zweig X; p. 277 5. IR (Water Dipersables) Zeig X; p. 283 Cyanides 1. Titrimetric AOAC-13; 6.100 Cyanuric Acid (593) (See "Available Chlorine") Cycloate (1037) 1. GLC AOAC-13; 6.426 2. GLC (TCD) EPA-l-Tent. 3. GLC (FID) EPA-2-Tent. 4. GLC (FID) EPA-3-Tent. 5. GLC Zweig V; p. 492 Cycloheximide (601) Cycloprate (1158) 1. GLC (GLC-FID) NEIC-1158-1 Cycocel (425) 1. Gravimetric Zweig VII; p. 524 2. Colorimetric Zweig VII; p. 525 Cygon (See "Dimethoate" 863) Cyhexatin (608) 1. Non-Aqueous Titration Zweig VII; p. 419 ------- C-10 Cyolane (See "Phosfolan" 594) Cypendazole (1370) Cyprazine (611) 1. Labile Chlorine (See "Chlorotriazine Herbicides/EPA-l") Cyprazole (612) Cyprex (See "Dodine" 1000) Cypromid (613) Cythioate (614) Cytrolane (See "Mephosfolan" 595) 1. UV JAOAC 53,971(1975) 2. GLC 3. Non-Aqueous Titration NEIC-611-1 NEIC-611-2 ------- D-l 2,4-D (708) 1. HPLC (Acids, Esters, & Amine Salts) AOAC-13; 6.275 2. HPLC (With Picloram) AOAC-13; 6.308 3. UV (With 2,4,5-T) (See "Chlorophenoxy Herbicides/EPA-2") 4. HPLC (See "Chlorohenoxy Herbicides/EPA-3-Tent.") 5. GLC (Butoxyethanol Ester) (See "Chlorophenoxy Herbicides/ EPA-4-Tent.") 6. GLC (In Fertilizers, with 2,4,5-T) (See "Chlorophenoxy Herbicides/ EPA-5-Tent.") 7. GLC (As TMS Ester) Zweig VI; p. 630 8. Ester Volatility AOAC-13; 6.032 9. TLC NEIC-C1Ph-1/2 10. GLC (As Methyl Ester) NEIC-ClPh-3 11. IR CIPAC-1; p. 730 Daconil 2787 (See "Chlorothalonil" 497) Dacthal (911) 1. IR AOAC-13; 6.262 2. GLC (Includes HCB Determination) AOAC-13; 6.259 Dalapon (615) and Sodium Salt (618) 1. Titrimetric (Na Salt) AOAC-13; 6.280 2. IR EPA-1 3. Colorimetric CIPAC-1; p. 274/276 4. GLC (As Methyl Ester) NEIC-615-1 (CA) Daminozide (619) 1. GLC Zweig VI; p. 697 2. Aqueous Base Titration Zweig V; p. 501 3. Non-Aqueous Base Titration NEIC-619-1 4. Redox Titration NEIC-619-2 Dasanit (See "Fensulfothion" 825) Dazomet (1952) 1. Hydrolysis/Titration Zweig III; p. 121 2. IR NEIC-1952-1 (VA) ------- D-2 2,4-DB (765) 1. Titrimetric Zweig V; p. 372 2. GLC (As TMS Ester) Zweig VI; p. 630 3. HPLC NEIC-765-1 (VA) DBCP (See "l,2-Dibromo-3-chloropropane" 656) DDD (See "TDE" 693) D~D Mixture (790) 1. IR (With Allyl Alcohol NEIC-790-1 2. GLC NEIC-790-2 DDT (694) 1. Total Chlorine AOAC-13; 6.254 2. IR (Dusts and Granules) AOAC-13; 6.257 3. IR (Emulsifiable Concentrates) EPA-1 4. Hydrolyzable Chlorine JAOAC 29, 188(1946) 5. IR NEIC~694-2 (VA) 6. GLC NEIC-694-1 DDVP (See "Dichlorvos" 797) Deet (837) 1. IR EPA-l-Tent. 2. GLC (TCD-IS) EPA-2-Tent. 3. GLC (FID-IS) EPA-3-Tent. 4. HPLC (RP) EPA-4-Tent. 5. GLC (With MGK's) NEIC-837-1 DEF (1991) 1. IR Zweig IV: p. 90 Dehydroabietylamine (624) 1. Colorimetric . NEIC-624-1 ------- D-3 Delachlor (531) 1. GLC NEIC-631-1 Delnav (See "Dioxathion" 941) Delphene (See "Deet" 837) Demeton (632) 1. GLC Zweig VI; p. 483 2. Hydrolysis/Titration Zweig II; p. 453 3. IR NEIC-632-1 (VA) Demeton-S-methyl (1087) Demosan (See "Chloroneb" 446) 2,4-DEP (2105) 1. Titrimetric Zweig IV: p. 127 Desmedipham (533) 1. HPLC Zweig X; p. 297 2. Total Nitrogen Zweig X; p. 295 3. TLC NEIC-633-1 4. Hydrolysis/Distillation NEIC-633-2 Dessin (See "Dinobuton" 293) Destun (See "Perfl uidone11 1575) Devrirtof (827) 1. GLC (FID-IS) Zweig VIII; p. 349 Dexon (See "Fenaminosulf" 865) Dialifor (636) 1. UV NEIC-636-1 2. HPLC NEI C~ 636-2 ------- D-4 Diallate (682) 1. GLC (TCD) NEIC-682-1 Diazinon (824) 1. GLC (FID-IS) AOAC-13; 6.431 2. GLC (TCD) EPA-1 3. HPLC EPA-2-Tent. 4. IR EPA-3 5. GLC (FID-IS) EPA-4 6. TLC JAOAC 53,514(1970) 7. Potentiometric Titration NEIC-824-1 8. GLC (FID-IS) NEIC-824-2 9. GLC (FID-IS, with P80) NEIC-824-3 10. GLC (Encapsulated) JAOAC 63,1003(1980) Dibam (See Sodium Dimethyldithiocarbamate (1846) Dibrom (See "Naled" 1457) l,2-Dibromo-3-chloropropane (656) 1. IR EPA-1 2. GLC (TCD) EPA-2-Tent. 2,2-Dibromo-3-nitri1opropionami de (659) 1. Titrimetric NEIC-659-1 Dibutalin (See "Butralin" 278) Dibutyl Phthalate (668) Dibutyl Succinate (669) 1. Hydrolysis/Titration EPA-1 Dicamba (671) 1. IR AOAC-13; 6.265 2. IR (With MCPA) AOAC-13; 6.270 3. GLC (As TMS Ester) Zweig VI: p. 630 4. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.) 5. GLC (As Methyl Ester) NEIC-CIPh-1 6. GLC (Use-dilutions, as Methyl Ester) NEIC-671-1 (WA) Dicapthon (677) ------- D-5 Dichlobenil (678) 1. IR EPA-1 2. 6LC (TCD) NEIC-678-1 3. GLC (FID-IS) Zweig X; p. 313 4. GLC (FID-IS) AOAC-13; 6.250 Dichlofenthion (679) Dichlohe (680) 1. IR EPA-1 Dichloran (704) 1. IR EPA-1 2. IR NEIC-704-1/2 Dichlormate (681) o-Dichlorobenzene (684) p-Dichlorobenzene (684.5) 1. IR EPA-1 2. GLC (TCD-IS) EPA-2-Tent. Dichloroisocyanuric Acid (795) (See "Available Chlorine") Dichlorophene (1376) 1. GLC (TMS Der. ) (See "Phenols and Chlorophenols/EPA-6-Tent.") 2. UV AOAC-13; 39.130 3. IR NEIC-1376-1 4. GLC (As Methyl Ester) NEIC-1376-2 5. GLC (As Methyl Ester) NEIC-1376-3 (HI) Dichloroprop (774) 1. IR CIPAC-1; p. 730 2. Titration CIPAC-IA; p. 1211 3. GLC Characterization CIPAC-IA; p. 1211 Dichlorvos (797) 1. IR (Baits and EC) AOAC-13; 6.324 2. IR (Sprays) AOAC-13; 6.328 3. GLC (Incl. Hexane/CH3CN Partitioning) Zweig IV; p. 529 4. GLC (FID) NEIC-797-1 5. GLC (FID, with Crotoxyphos) NEIC-797-2 6. GLC (FPD) NEIC-797-3 7. Chloral Content (GLC) CIPAC-IA; p. 1216 8. Titrimetric CIPAC-IA; p. 1221 Oiclofop (797.3) Diclofop-methyl (797.5) ------- D-6 Dicofol (213) 1. Hydrolyzable Chlorine AOAC-13; 6.283 2. IR CIPAC-1; p. 730 3. GLC JAOAC 54, 1237(1971) 4. GLC JAOAC 56, 1335(1973) 5. HPLC (With Carbaryl and Malathion) NEIC-213-1 6. IR NEIC-213-2 (VA) 7. HPLC JAOAC 63, 1296(1980) Dicrotophos (900) 1. IR Zweig V; p. 215 2. GLC Zweig VI: p. 290 3. IR NEIC-900-1 (VA) Dicryl (798) ~ieldrin (806) 1. Total Chlorine AOAC-13; 6.177 2. IR (HEOD) AOAC-13-, 6.182 3. GLC Zweig VI; p. 271 Oiethatyl-ethyl (808.5) 1. HPLC NE1C-808.5-1 Difenzoquat Methyl Sulfate (838) 1. UV Zweig XI; p. 292 2. HPLC (RP) NEIC-838-2 (MT) 3. HPLC (RP) JAOAC 63, 647 (1980) Diflubenzuron (839) 1. HPLC Zweig X; p. 59 2. UV Zweig X; p. 62 3. HPLC NEIC-839-1 4. HPLC NEIC-839-2 Difolatan (See "Captafol" 351) Diiodomethyl-p-tolyl sulfone (853) 1. Titrimetric NEIC-853-1 2. UV NEIC-853-2 Dilan (212) Dimefox (1959) 1. Differential Hydrolysis CIPAC-1; p. 330 Dimetan 1. Hydrolysis/Distillation Zweig II; p. 166 ------- D-7 Dimethoate (863) 1. GLC (TCD-IS) 2. GLC (FID-IS) 3. Hydrolysis/Distillation 4. Gravimetric 5. GLC 6. Near IR 7. By-Products (TLC/GLC) Zweig II; p. 172 Zweig II; p. 174 Zweig VI; p. 357 NEIC-863-1 CIPAC-IA; p. 1232 EPA-l-Tent. EPA-2-Tent. Dimethrin (864) Dimethyl Phthalate (905) 1. GLC (Mosquito Clothwipes) NEIC-905-1 Dimetilan (1214) Dimilin (See "Diflubenzuron" 839) Dimite (See "Chlorfenethol" 702) Dinitramine (917) 1. GLC (FID or TCD-IS) Zweig VIII; p. 362 Dinitro-o-sec-Butyl Phenol (See "Dinoseb" 932) Dinobuton (293) 1. Titrimetric Zweig VII; p. 277 2. Colorimetric Zweig VIII; p. 278 3. Non-Aqueous Titration NEIC-293-1 Dinocap (927) 1. Total Nitrogen EPA-1 2. IR EPA-2-Tent. 3. GLC Zweig VI: p. 568 4. Colorimetric JAOAC 57, 653(1974) 5. HPLC NEIC-927-1 NEIC-927-2 6. Polarography ------- D-8 Dinoseb (932) 1. Stannous Chloride Reduction (See "Nitrophenols/EPA-1") 2. Total Nitrogen (See "Nitrophenols/EPA-2") 3. IR EPA-l-Tent. 4. GLC (TCD) EPA-2-Tent. 5. UV CIPAC-1; p. 338 6. HPLC NEIC-932-1 7. HPLC (With Naptalam) NEIC-932-2 8. UV (With Naptalam) NEIC-932-3 9. Redox Titration Zweig V; p. 387 Dioxacarb (940) Dioxathion (941) 1. GLC (TCD) NEIC-941-1 2. IR NEIC-942-2 3. GLC JAOAC 53, 566(1970) 4. HPLC NEIC-141-3 5. IR NEIC-941-4 (VA) 6. GLC (Dips) JAOAC 63, 33(1980) Diphacinone (942) 1. UV EPA-1 2. HPLC EPA-2-Tent. 3. UV NEIC-942-1 4. UV (0.1%) NEIC-942-2 5. HPLC NEIC-942-3 Diphenamid (944) 1. IR Zweig V; p. 376 2. GLC Zweig V; p. 376 Diphenyl (See "Biphenyl" 202) Diphenylacetonitrile (945) 1. IR NEIC-945-1 Diphenylamine (946) 1. GLC NEIC-946-1 2. GLC (TCD) EPA-l-Tent. Dipterex (See "Trichlorofon" 913) ------- 0-9 Diquat Dibromide (958) 1. UV AOAC-13; 6.332 2. HPLC (RP-IS) NEIC-958-1 (MT) Disodium N-(2-Hydroxyethyl)iminodiacetate (962) 1. Potentiometric Titration NEIC-962-1 Disulfoton (823) 1. IR EPA-l-Tent. 2. GLC (FID-IS) EPA-2-Tent. 3. Hydrolysis/Titration Zweig II; p. 189 4. IR Zweig II; p. 190 5. GLC (FID-IS) NEIC-823-1/2 6. IR JAOAC 47, 257(1974) 7. GLC (TCD) NEIC-823-3 8. GLC (FID-IS) AOAC-13; 6.A27 Di-Syston (See "Disulfoton" 823) Dithane M-45 (2134) 1. Titrimetric CIPAC-1A; p. 1289 Dithianon (843) 1. IR JAOAC 52, 659(1969) 2. Colorimetric Zweig X; p. 183 3. Colorimetric NEIC-843-1 Dithiocarbamates 1. Carbon Disulfide Evolution AOAC-13; 6.338 2. Qualitative Test JAOAC 55, 939(1972) 3. Degradation Products and Analyses Zweig, XI; p. 197 Diuron (975) 1. Hydrolysis/Distillation EPA-1 2. HPLC EPA-2-Tent. 3. UV EPA-3-Tent. 4. IR EPA-4-Tent. 5. IR CIPAC-1; p. 730 6. HPLC (Use-dilution) NEIC-975-1 (HI) DNBP (See "Dinoseb" 932) ------- D-10 Dodine (1000) 1. Non-Aqueous Titration A0AC-13; 6.346 Dowicil 100 (397) 1. Titrimetric NEIC-397-1 2. TLC JAOAC 63, 864 (1980) Dowicil S-13 (See "2,3,5,6-Tetrach1oro-4-(methylsulfonyl)pyridine" 1933) 2,4-DP (See "Dichloroprop" 774) Drazoxolon (466) 1. Colorimetric Zweig VII; p. 667 Drepamon (See "Tiocarbenil" 1629.3) DSMA (963) 1. Titrimetric (See "Arsenic Compunds/EPA-3-Tent. & EPA-4") Duraset (1985) 1. Titrimetric Zweig V; p. 407 Dursban (See "Chlorpyrifos" 509) Du-Ter (See "Triphenyltin Hydroxide" 2101) Dyfonate (1081) 1. GLC Zweig VII; p. 270 2. IR NEIC-1081-1 (VA) Dylox (See "Trichlorofon" 913) Dymid (See "Diphenamid" 944) Dyrene (See "Anilizine" 685) ------- E-l Edifenphos (1041) 1. GLC (FID-IS) NEIC-1041-1 2. GLC (TCD) NEIC-1401-2 EDTA (1048) 1. Titrimetric NEIC-1048-1 (CA) 2. Colorimetric NEIC-1048-2 3. Qualitative Test NEIC-1048-3 Endosulfan (1001) 1. Hydrolysis/Titration EPA-1 2. IR EPA-2-Tent. 3. GLC (TCD-IS) EPA-3-Tent. 4. GLC (FID-IS) EPA-4-Tent. 5. GLC (FID-IS) EPA-5-Tent. 6. GLC Zweig VI; p. 511 7. Chromatography/IR CIPAC-1; p. 361 8. Hydrolysis/Titration CIPAC-1; p. 374 Endothall (1002) 1. Oxidation/Titration EPA-1 2. GLC (FID) EPA-2-Tent. 3. GLC Zweig X; p. 330 4. GLC NEIC-1002-1 5. Titrimetric NEIC-1002-2 Endrin (1009) 1. IR A0AC-13; 6.182 2. Total Chlorine A0AC-13; 6.177 3. IR NE I C~ 1009-2 (VA) 4. IR (With Methyl Parathion) NEIC-1009-1 Enide (See "Diphenamid" 944) Entex (See "Fenthion" 1098) ------- E-2 Epichlorohydrin (1010) EPN (1080) 1. Potentiometric Titration NEIC-1080-1 2. GLC (FID-IS) NEIC-1080-2 Eptam (See "EPTC" 1042) EPTC (1042) 1. GLC AOAC-13; 6.426 2. GLC (TCD-IS) EPA-l-Tent. 3. HPLC EPA-2-Tent. 4. GLC (FID-IS) EPA-3 5. GLC (FID-IS) EPA-4-Tent. 6. GLC (TCD-IS) EPA-5-Tent. 7. HPLC (RP) EPA-6-Tent. 8. IR NEIC-1042-1 (VA) Erbon (1012) 1. GLC JAOAC 56, 1087(1973) 2. Hydrolysis/Titratiori NEIC-1012-1 Ethafluralin (1015) 1. UV . . . . 2. GLC. . . . Zweig X; p. 343 Zweig X; p. 345 Ethanol (17) 1. GLC A0AC-13; 36.007 Ethephon (1018) 1. Titrimetric NEIC-1018-1 2. GLC NEIC-1018-2 Ethiolate (1019) Ethion (1020) 1. IR EPA-1 2. GLC (TCD) EPA-2-Tent. 3. HPLC AOAC-13; 6.352 ------- E-3 Ethirimol (297) 1. GLC (FID-IS; as TMS Der.) Zweig VIII; p. 288 2. UV Zwieg VIII; p. 287 3. TLC Zweig VIII; p. 287 Ethofumesate (1020.5) 1. GLC Zweig X; p. 355 2. GLC (FID-IS) EPA-l-Tent. Ethoprop (1021) 1. IR EPA-l-Tent. 2. GLC (TCD-IS) EPA-2-Tent. 3. GLC (FID-IS) EPA-3-Tent. 4. GLC (FID-IS) NEIC-1021-1 Ethoxyquin (1024) 1. Non-Aqueous Titration NEIC-1024-1 2. Fluorescence NEIC-1024-2 Ethrel (See "Ethephon" 1018) Ethylene Dibromide (1056) 1. GLC A0AC-13; 6.143 Ethylene Dichloride (1057) 1. GLC A0AC-13; 6.143 2. GLC (FID) NEIC-FUM-1 Ethylene Glycol (1058) 1. GLC NEIC-1058-1 Ethylene Oxide (1061) Ethylene Thiourea (ETU) 1. GLC (FID & TCD) EPA-l-Tent. 2. GLC & TLC JAOAC 55, 923(1972) 3. UV NEIC-ETU-1 4. TLC NEIC-ETU-2 Ethyl Guthion (See "Azinphosethyl" 828) 2-Ethyl-l,3~hexanediol (1064) 1. Acetylation EPA-1 2. GLC (TCD-IS) EPA-2-Tent. Etrimfos (1091) 1. GLC (FID-IS) Xweig XI; p. 128 ------- F-l Falone (See "2,4-DEP" 2105) Famphur (1093) 1. Colorimetric NEIC-1093-1 2. IR (Encapsulated) JAOAC 61, 1526(1978) 3. HPLC NEIC-1093-2 4. GLC NEIC-1093-3 Fenac <2050) Fenaminosulf (866) 1. Colorimetric Zweig III; p. 51 Fenazaflor (1598) 1. UV NEIC-1598-1 Fenitrothion (897) 1. Hydrolysis/UV Zweig VII; p. 461 2. GLC (FID-IS) NEIC-897-1 3. Titrimetric CIPAC-1A; p. 1255 Fenson (462) 1. Hydrolysis/Titration CIPAC-1; p. 392 2. IR CIPAC-1; p. 730 Fensulfothion (825) 1. Titrimetric Zweig VII; p. 256 2. IR NEIC-825-1 (VA) Fenthion (1098) 1. GLC (FID) NEIC-1Q98-1 2. GLC (0.5% in Oil) NEIC-1098-2 3. IR Zweig II; p. 45 4. GLC (in Feeds) Zweig VI; p. 301 5. IR NEIC-1098-3 Fentin Hydroxide (See "Triphenyltin Hydroxide" 2101) Fenuron (1099) 1. Dimethyl amine Distillation NEIC-1099-1 2. HPLC (See ."Quintex") Fenvalarate (590) 1. HPLC NEIC-590-1 Ferbam (1100) 1. Carbon Disulfide Evol'n AOAC-13; 6.338 2. UV CIPAC-1; p. 398 Ferrous Ammonium Sulfate (1104) 1. Titrimetric NEIC-1104-1 Ferrous Sulfate (1105) ------- F-2 Ficam (See "Bendiocarb" 172.5) Flammability 1. Flame Projection EPA-1 2. Closed Drum EPA-2 Fluchoralin (1106) 1. GLC JAOAC 60, 1145(1977) Fluometuron (1107) 1. GLC (TFA Derivative) AOAC-13; 6.289 2. IR EPA-1 3. UV EPA-2-Tent. 4. Dimethylamine Distillation Zweig VII; p. 574 5. Potentiometric Titration NEIC-1107-1 Fluor Chrom Arsenate Phenol 1. Total Fluorine AWPA; A2-71-8 2. Total Chrominum AWPA; A2-71-5 3. Total Arsenic AWPA; A2-71-2 4. Dinitrophenol Content AWPA; A2-71-7 5. Pentachlorophenol Content AWPA; A2-71-6 Flurecol (302) 1. UV Zweig XI; p. 321 2. GLC (Butyl ester) Zweig XI; p. 322 Fluoridamid (1108) 1. GLC (FID-IS) Zweig X; p. 535 2. Titrimetric NEIC-1108-1 Fluorine 1. Titrimetric (Travers) AOAC-13; 6.019 2. Titrimetric (Mod. Travers) AOAC-13; 6.021 3. Distillation/Titration AOAC-13; 6.023 4. Spec, ion electrode (Paints) AOAC-13; 5.004 Fluoroacetamide (1109) Fluoroacetic Acid (1110) 1. GLC JAOAC 60, 1434(1977) Fluorodifen (1111) 1. GLC NEIC-1111-1 Fluoromidine (504) Folcidin (See "Cypendazole" 1370) Folex (1992) 1. GLC (TCD-IS) NEIC-1992-1 2. IR NEIC-1992-2 (VA) ------- F-3 Folpet (1114) 1. HPLC AOAC-13; 6.294 2. IR EPA-1 3. GLC Zweig VI; p. 546 4. HPLC (With Carbaryl, Malathion and Dicofol) . . NEIC-1114-1 Formaldehyde (1115) 1. Oxidation/Titration AOAC-13; 6.348 2. Cyanide Method (Dilute Sol'ns) AOAC-13; 6.350 3. Cyanide Method (Seed Disinfectants) AOAC-13; 6.351 Formetanate (1116) & Formetanate Hydrochloride (1117) 1. Titrimetric Zweig VII; p. 281 2. TLC NEIC-1117-1 Formothion (884) 1. GLC AOAC-13; 6.356 Fosamine Ammonium (1117.5) 1. HPLC (AX-IS) NEIC-1117.5-1 Fospirate (1118) 1. UV NEIC-1118-1 Fumaric Acid (1119) Fumarin (See "Coumafuryl" 9) Fumigants 1. GLC AOAC-13; 6.143 2. GLC (FID) NEIC-FUM-1 Fumite (See "Tecnazene" 1934) Fundal (See "Chlordimeform" 387) Funginex (See "Triforine" 2083) Furadan (See "Carbofuran" 355) Furamethrin 1. GLC (Mosquito Coils) NEIC-Furamothrin-1 Furethrin (1121) ------- G-l Galecron (See "Chlordimeform" 387) Gamma BHC (See "BHC, Gamma Isomer" 1282) Gardorta (See "Tetrachlorvinphos" 503) Genite 923 (780) 1. IR Gibberellic Acid (1123) 1. Fluorimetrlc 2. UV Gibberelliris A4A7 (1123) 1. TLC Glutaraldehyde (1125) 1. Titrimetric. 2. GLC Glycerol (1126) 1. Titrimetric Glycolic Acid (1127) Glycophene (See "Anfor" 782) Glyodin (1130) 1. Titrimetric Glyphosate (1131) 1. UV 2. HPLC Glyphosine (1133) Goal (See "Oxyfluorfen" 1551) Gophacide (209) 1. HPLC Gossyplure HF (1156) Griseofulvin (1134) 1. UV Guthion (See "Azinphosmethyl" 899) NEIC-780-1 (VA) Zweig V; p. 415 JAOAC 60, 859(1977) Zweig X; p. 548 NEIC-1125-1 NEIC-1125-2 A0AC-13; 35.080 Zweig III; p. 100 NEIC-1131-1 NEIC-1131-2 NEIC-209-1 A0AC-13; 42.299 ------- 1-1 Igran (See "Terbutryn" 1926) Iraidan (See "Phosmet" 1312) Indalone (287) Indole-3-butyric Acid (1219) 1. UV EPA-1 Iodine (and Iodine Complexes) (1222) 1. Potentiometric Titration NEIC-1222-1 Iodofenphos (701) Ioxynil (852) 1. GLC Zweig V; p. 354/428 IPC (See "Propham" 1241) Iprodione 1. HPLC (Silica) Zweig XI; p. 250 2. GLC (FID-IS) Zweig XI; p. 250 Irgasan DP 300 (411) 1. UV NEIC-411-1 2. Total Chlorine NEIC-411-2 3. HPLC (RP-IS) NEC-411-3 Isobenzan (1508) 1. IR NEIC-1508-1 2. IR NEIC-1508-2 (VA) Isocil (1232) Isolan (1245) 1. Dimethylamine Distillation Zweig II; p. 258 Isophorone (1235) Isoprocarb (1250) Isopropalin (1236) 1. Colorimetric Zweig VIII; p. 371 2. GLC (FID-IS) Zweig VIII; p. 373 Isopropanol (1237) 1. GC A0AC-13; 36.006 2. GC A0AC-13; 5.012 3. GLC NEIC-1237-1 ------- H-l Halazone (792) 1. Titrimetric NEIC-792-1 HCB (See "Hexachlorobenzene" 1149) Heptachlor (1139) 1. Labile Chlorine AOAC-13; 6.298 2. GLC AOAC-13; 6.301 3. IR EPA-1 4. IR NEIC-1139-1 (VA) Herban (See "Norea" 1503) Hexachlorobenzene (1149) 1. GLC (in Dacthal) AOAC-13; 6.259 Hexachlorocyclopentadiene (1151) 1. UV (in Tech. Chlordane) AOAC-13; 6.228 Hexachlorophene (1383) 1. UV AOAC-13; 35.028 2. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 3. GLC (See "Phenols and Chlorophenols/EPA-8-Tent.") 4. IR NEIC-1383-1 5. GLC Zweig X; p. 194 Hexamethylene Tetramine (1169) 1. Distillation/Titration NEIC-1169-1 Hinosan (See "Edifenphos" 1041) Hormodin (See "Indole-3-butyric Acid" 1219) HPMTS (1210) 1. Titrimetric NEIC-1210-1 Hydrochloric Acid (1180) 1. Titrimetric NEIC-1180-1 2. Titrimetric NEIC-1180-2 Hydroprene (1182) 2~[(Hydroxymethyl)ami no]ethanol (1204) ------- H-2 3-Hydroxy-5-methyli soxazole 1. GLC Zweig X; p. 218 2-(Hydroxymethy1)-2-nitro-l,2~propanediol (1207) 1. Colorimetric NEIC-1207-1 Hymexazol (See "3-Hydroxy-5-methy1isoxazole") Hyvar (See "Isocil" 1232) ------- 1-1 Igran (See "Terbutryn" 1926) Imidan (See "Phosmet" 1312) Indalone (287) Iridole-3-butyn'c Acid (1219) 1. UV EPA-1 Iodine (and Iodine Complexes) (1222) 1. Potentiometric Titration NEIC-1222-1 Iodofenphos (701) Ioxynil (852) 1. GLC Zweig V; p. 354/428 IPC (See "Propham" 1241) Irgasan DP 300 (411) 1. UV NEIC-411-1 2. Total Chlorine NEIC-411-2 Isobenzan (1508) 1. IR NEIC-1508-1 2. IR NEIC-1506-2 (VA) Isocil (1232) Isolan (1245) 1. Dimethyl amine Distillation Zweig, II; p. 258 Isophorone (1235) Isoprocarb (1250) Isopropalin (1236) 1. Colorimetric Zweig VIII; p. 371 2. GLC (FID-IS) Zweig VIII; p. 373 Isopropanol (1237) 1- GC AOAC-13; 36.006 2. GC AOAC-13, 5.012 3. GLC NEI C-1237-1 ------- 1-2 Isopropyl Carbanilate (See "Propham" 1241) Isoprothiolane 1. GLC (FID-IS) Zweig X; p. 231 Isothioate 1. TLC/Total Phosphorus Zweig X; p. 76 2. GLC Zweig X; p. 76 Isoxathion 1. GLC Zweig X; p. 85 ------- K-l Karathane (See "Dinocap" 927) Karbutilate (1261) 1. IR EPA-1 Kathon (See "2-n-0ctyl-4-isothiozolinone" 1515) Kelthane (See "Dicofol" 213) Kepone (See "Chlordecone" 621) Kerb (See "Pronamide" 690) Korlan (See "Ronnel" 1117.5) Krenite (See "Fosamine Ammonium" 1117.5) ------- L-l Lamprecide (2081) Landrin (2093) Lannate (See "Methomyl" 1328) Lanstan (See "Chloro-2-nitropropane" 449) Lasso (See "Alachlor" 16) Lead and Lead Compounds 1. Gravimetric A0AC-13; 6.014 Lead Arsenate (1276/1277) 1. Total Arsenic AOAC-13; 6.043 2. Total Arsenious Oxide AOAC-13; 6.045 3. Total Arsenic Oxide AOAC-13; 6.046 4. Total Lead A0AC-13; 6.049 Lenacil (1279) 1. TLC NEIC-1279-1 Leptophos (1280) 1. GLC NEIC-1280-1 2. IR NEIC-1280-2 Lethane 60 (1972) 1. Total Nitrogen AOAC-13; 6.423 Lethane 384 (277) 1. Total Nitrogen AOAC-13; 6.423 2. IR NEIC-277-1 3. GLC Zweig VI; p. 417 4. GLC (with Malathion) NE1C-277-2 Lime Sulfur (See "Calcium Polysulfide" 340) Limonene (1281) Lindane (See "BHC, Gamma Isomer" 1282) Linuron (1284) 1. HPLC EPA-l-Tent. 2. IR EPA-2 3. UV EPA-3-Tent. 4. Hydrolysis/Distillation Zweig V; p. 434 5. IR CIPAC-1; p. 730 Lithium Hypochlorite (1285) 1. Titrimetric NEIC-1285-1 Lorsban (See "Chiorpyrifos" 509) Lovozal (See "Fenazaflor" 1598) ------- M-l Maintain CF 125 (See "Chlorf1urecol-Methyl" 1346) Malathion (1299) 1. Argentimetric Titration A 2. Colorimetric A 3. GLC (FID-IS) A 4. HPLC E 5. IR E 6. GLC Z 7. HPLC N 8. HPLC (With Carbaryl and Dicofol) N 9. Total Phosphorus (See "Phosphorus Compounds/EPA-1") 10. HPLC (RP-IS) N AOAC-13; 6.359 AOAC-13; 6.364 AOAC-13; 6.372 EPA-l-Tent. EPA-2 Zweig VI; p. 418 NEIC-1299-1 NEIC-1299-2 NEIC-1299-3 Maleic Hydrazide (See "MH" 847) Maloran (See "Chlorbromuron" 385) Maneb (1302) 1. Carbon Disulfide Evolution AOAC-13; 6.338 Matacil (See "Aminocarb" 870) MCPA (1347) 1. Titrimetric Zweig V; p. 412 2. GLC (TMS Ester) Zweig VI; p. 663/630 3. IR CIPAC-1; p. 482 4. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.) 5. HPLC AOAC-13; 6.A18 MCPA Esters 1. Hydrolysis/Titration CIPAC-1; p. 499 MCPB (1362) 1. GLC Zweig VIII; p. 403 2. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.") MCPP (See "Mecoprop" 1364) Mecarbam (821) 1. GLC (FID-IS) Zweig VIII; p. 136 Mecoprop (1364) 1. GLC Zweig VI; p. 630 2. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.") 3. IR CIPAC-1; p. 730 4. Characterization (IR/GLC) CIPAC-1A, p. 1298 5. Titration CIPAC-IA, p. 1298 ------- M-2 Mefluidide (3106) 1. GLC NEIC-1306-1 Menazon (652) 1. Colorimetric Zweig VII; p. 320 Mephosfolan (595) 1. UV Zweig VII; p.233 2. GLC (FID-IS) Zweig VII; p. 236 Merbac 35 (See "Benzyl Bromoacetate" 192) Mercaptobenzothiazole (1308) and Sodium Salt (1311) 1. UV EPA-l-Tent. 2. Potentiometric Titration EPA-2-Tent. 3. HPLC (with Sodium Dimethyldithiocarbamate . . . NEIC-1308-1 Mercaptophos (See "Fenthion" 632) Mercurial Seed Disinfectants 1. Gravimetric (as Mercuric Sulfide) AOAC-13; 6.131 2. Titrimetric AOAC-13; 6.132 3. Gravimetric (1,2-Propanediamine Prec'n) AOAC-13; 6.136 Mercury (1316) and Mercury Compounds 1. Titrimetric (Thiocyanate) NEIC-1316-1 2. Titrimetric (Dithizone) NEIC-1316-2 Merphos (See"Folex" 1992) Mesityl Oxide (1321) Mestranol (1322) 1. Colorimetric NEIC-1322-1 Mesurol (See "Methiocarb" 1436) Metaldehyde (1323) 1. Titrimetric EPA-1 2. GLC (TCD-IS) EPA-2 3. IR EPA-3 4. GLC (TCD) EPA-4 Meta-Systox (See "Demeton-methyl" 1087) Meta-Systox R (See "Oxydemeton-methyl" 1084) ------- M-3 Methabenzthiazuron (185) Methalpropalin (1324.5) Methamidophos (1325) 1. GLC Zweig VII; p. 341 2. IR NEIC-1325-1 Methanol (1338) 1. GLC NEIC-1338-1 Methazole (3326) 1. IR Zweig X; p. 370 2. IR NEIC-1326-1 Methidathion (1327) 1. GLC (FID-IS) EPA-l-Tent. 2. GLC (FID-IS) Zweig VIII; p. 147 3. GLC (FID-IS) NEIC-1327-1 Methiocarb (1436) 1. IR EPA-l-Tent. 2. HPLC JAOAC 62, 5 (1979) 3. GLC NEIC-1436-1 Methomyl (1328) 1. HPLC Zweig VII; p. 333 2. HPLC EPA-l-Tent. 3. HPLC (Reverse Phase) NEIC-1328-1 4. IR NEIC-1328-2 Methoprene (1329) 1- GLC Zweig X; p. 96 2. GLC (FID-IS) NEIC-1329-1 3. GLC (On Treated Grain) NEIC-1329-2 4. IR (Encapsulated) JAOAC 63, 879 (1980) Methoprotryne (1239) 1. Titrimetric CIPAC-1A, p. 1302 Methoxychlor (3133) 1. IR EPA-l-Tent. 2. GLC (FID-IS) EPA-2-Tent. 3. HPLC EPA-3-Tent. 4. GLC (With Captan & Malathion) NEIC-1333-1 5. IR CIPAC-1; p. 730 6. Characterization JAOAC 63, 1007(1980) Methyl Bromide (1341) 1. GLC (With Chloropicrin) NEIC-1341-1 (CA) ------- M-4 Methylenebis(thlocyanate) (1382) 1. GLC NEIC-1382-1 2. Hydrolysis/Titration NEIC-1382-2 3. IR NEIC-1382-3 Methylene Chloride (1387) Methyl Isothiocyanate (3198) 1. Potentiometric Titration Zweig X; p. 565 2. GLC Zweig X; p. 566 Methyl Nonyl Ketone (1418) 1. GLC NEIC-1418-1 2. Titrimetric NEIC-1418-2 Methyl Parathion (896) 1. GLC AOAC-13; 6.400 2. HPLC AOAC-13; 6.405 3. GLC (Microencapsulated) AOAC-13; 6.409 4. HPLC . * EPA-l-Tent. 5. IR EPA-2 6. Colorimetric EPA-3 7. GLC (FID-IS) EPA-5 8. Electrometric Titration NEIC-896-1 9. GLC NEIC-896-2 10. GLC (Microencapsulated) AOAC-13; 6.409 Methyl Salicylate (1430) 1. HPLC NEIC-1430-1 2. GC NEIC-1430-2 Methyl Trithion (484) 1. IR NEIC-484-1 (VA) 2. GLC Zweig II; p. 315 3. UV Zweig II; p. 315 Metobromuron (1439) 1. IR EPA-l-Tent. 2. GLC EPA-2-Tent. 3. GLC (FID-IS) EPA-3-Tent. 4. UV Zweig VII; p. 574 Metolachlor (4140) 1. GLC (FID-IS) NEIC-1440-1 Metoxuron (436) 1. Hydrolysis/Titration AOAC-13; 6.245 2. HPLC/TLC NEIC-436-1 3. By-Products (TLC) CIPAC-1A; p. 1306 ------- M-5 Metribuzin (100) 1. GLC, IR and HPLC JAOAC 59, 278 (1976) 2. GLC (FID-IS) NEIC-100-1 3. GLC (TCD-IS) NEIC-100-2 Mevinphos (356) 1. GLC Zweig VI; p. 450 2. IR Zweig II; p. 360 3. Hydrolysis/Titration Zweig II; p. 356 4. GLC (Separates Isomers) NEIC-356-1 Mexacarbate (1441) 1. GLC EPA-l-Tent. 2. GLC NEIC-1441-1 3. IR NEIC-1441-2 MGK R-ll (206) 1. Titrimetric NEIC-206-1 2. GLC NEIC-206-2 MGK-264 (1512) 1. GLC (See "Pyrethrins/EPA-2") 2. GLC (FID-IS) JAOAC 58, 845 (1975) 3. GLC (FID) NEIC-1512-1 4. GLC (FID-IS) A0AC-13; 6.A15 MGK-326 (954) 1. UV NEIC-954-1 2. GLC NEIC-954-2 MGK R-874 (1194) MH (847) 1. UV EPA-1 2. Titrimetric Zweig IV; p. 149 Mineral Oils (1443) 1. Unsulfonated Residue AOAC-13; 6.121 2. Gravimetric JAOAC 56, 14 (1973) 3. Gravimetric CIPAC-1A; P. 1320 Mineral Oil - Soap Emulsions 1. Water AOAC-13; 6.125 2. Total Oil AOAC-13; 6.126 3. Soap AOAC-13; 6.127 Mi rex (976) 1. GLC (EC) NEIC-976-1 (MS) ------- M-6 Mitox (See "Chlorbenside" 384) Mobam (See "Benzothienyl Methyl carbamate" 187) Mocap (See "Ethoprop" 1021) Modown (See "Bifenox" 200) Molinate (1063) 1. GLC AOAC-13; 6.426 Monitor (See "Methamidophos" 1325) Monocrotophos (901) 1. IR EPA-1 2. GLC (FID-IS) EPA-2 3. GLC (FID-IS) EPA-3-Tent. 4. GLC Zweig VI; p. 287 5. IR Zweig V; p. 194 Monolinuron (467) Monuron (1450) 1. Dimethylamine Distillation EPA-1 2. UV EPA-2 3. IR EPA-3 4. HPLC NEIC-1450-1 5. IR CIPAC-1; p. 730 Monuron Trichloroacetatvi (1451) Morestan (See "Oxythioquinox" 1428) MSMA (1448) 1. Titrimetric (See "Arsenic Compounds/EPA-3-Tent. & EPA-4") Murfotox (See "Mecarbam" 821) Muscalure (See "(z)-9-Tricosene" 2064) Mylone (See "Dazomet" 1952) ------- N-l Nabam (1456) 1. Carbon Disulfide Evolution AOAC-13; 6.338 Naled (1457) 1. GLC Zweig VI; p. 350 2. IR NEIC-1457-1(VA) 3. GLC JAQAC 58, 1162(1975) Naphthalene (1458) 1. Sublimation NEIC-1458-1 2. GLC (FID-IS) NEIC-1458-2(MN) 1-Naphthaleneacetamide (1459) 1. GLC NEIC-1459-1 1-Naphthaleneacetic Acid (1460) 1. Titrimetric Zweig V; p. 457 2. HPLC NEIC-1460-1 3. IR . . NEIC-1460-1(VA) 1,8-Naphthalic Anhydride (See "Protect") 2-Naphthol (1467) 1. Colorimetric AOAC-13; 34.069/.070 2-Naphthoxyacetic Acid (1468) 1. UV (Aqueous) NEIC-1468-1 2. UV (Alcohol Sol'ns) NEIC-1468-2 Napropamide (See "Devrinol" 827) Naptalam (1470) 1. Gravimetric (With DNSBP) NEIC-1470-1 2. Titrimetric NEIC-1470-2 3. HPLC (with DNSBP) NEIC-1470-3(VA) 4. HPLC (with DNSBP; RP-IS) NEIC-1470-4 Neburon (4173) 1. IR EPA-l-Tent. 2. Hydrolysis/Distillation Zweig IV; p. 159 Neguvon (See "Trichlorofon" 913) Nellite (650) Nemacur (1079) 1. GLC NEIC-1079-1 ------- N-2 Nemagon (See ul,2-Dibromo-3-chloropropane" 656) Neopynamin (See "Tetramethrin" 1957) Neotran (208) Niclosamide (See "Clonitralid" 707) Nicotine (1479) and Nicotine Sulfate (1480) 1. Gravimetric AOAC-13; 6.175 2. UV NEIC-1479-1 3. HPLC NEIC-1479-2(TX) 4. HPLC (RP) NEIC-1479-3 Nitralin (1433) 1. IR Zweig VII; p. 628 2. GLC Zweig VII; p. 631 3. IR NEIC-1433-KVA) Nitrapyrin (1482) 1. GLC (TCD-IS) NEIC-1482-1 Nitrofen (786) 1. GLC (FID-IS) Zweig X; p. 405 Nitrophenols 1. Stannous Chloride Reduction EPA-1 2. Total Nitrogen EPA-2 Nitroso Compounds 1. Description and analysis Zweig XI; p. 363 Norbormide (1502) 1. UV EPA-1 Norea (1503) 1. IR NEIC-1503-1 Norflurazon (1504) 1. GLC (FID-IS) Zweig X; p. 417 2. TLC/UV Zweig X; p. 419 Nortron (See "Ethofumesate" 1020.5) ------- OCS-21693 (1434) 1. IR Octhilinone (1510.5) 1. GLC Oil of Citronella (1526) 1. UV (Citral content). Oil of Lemongrass (1530) 1. GLC Omite (See "Propargite" 1737) Ordram (See "Molinate" 1063) Organotin Compounds 1. Titrimetric Ornitrol (655) 1. Total Chlorine . . . Orthene (See "Acephate" 3) Oryzalin (1539) 1. Colorimetric . . . . 2. Colorimetric . . . . Outfox (See "Cyprazine" 611) Ovex (1540) 1. IR 2. Hydrolysis/Titration 3. IR Oxadiazon (1541) 1. GLC. . . . Oxalic Acid (1542) 1. Titrimetric Oxamyl (1543) 1. HPLC . . . Oxycarboxin (1549) 1. IR . . . 2. HPLC . . 0-1 NEIC-1434-1 NEIC-1510. 5-1 AOAC-13; 19.129 EPA-l-Tent. EPA-1 NEIC-655-1 Zweig VIII; p. 435 EPA-l-Tent. EPA-1 CIPAC-1; p. 214 CIPAC-1; p. 730 Zweig VII; p. 597 NEIC-1542-1 Zweig X; p. 113 NEIC-1549-1 NEIC-1549-2 ------- 0-2 Oxydemetonmethyl (1084) 1. GLC JAOAC 61, 500 (1978) 2. Hydrolysis/Titration Zweig II; p. 300 3. Redox Titration Zweig II; p. 300 4. IR NEIC-1084-1 5. TLC NEIC-1084-2 Oxyfluorfen (1551) 1. GLC (FID-IS) Zweig XI; p. 332 Oxythioquinox (1428) 1. UV . . . . Zweig V; p. 279 ------- p-1 Paarlan (See "Isopropalin" 1236) Padan (See "Cartap" 871) Panogen (589) (See "Mercury") Paradichlorobenzene (See "p-Dichlorobenzene" 684.5) Paraformaldehyde (See "Formaldehyde" 1554) Paraquat Dichloride (1555) and bis(Methylsulfate) (1556) 1. Colorimetric AOAC-13; 6.334 2. HPLC (CX) NEIC-1555-1 3. HPLC (RP) NEIC-1555-2(MT) 4. HPLC (RP) NEIC-1555-3 Parathion (1558) 1. GLC (FIC-IS) AO AC-13; 6.379 2. HPLC (IS) AOAC-13; 6.384 3. Titrimetric AOAC-13; 6.388 4. Colorimetric AOAC-13; 6.395 5 HPLC EPA-l-Tent. 6. GLC (FID-IS) EPA-2-Tent. 7. GLC EPA-3-Tent. 8. HPLC EPA-4-Tent. 9. IR NEIC-1558-1(VA) 10. GLC (Use-dilutions) NEIC"1558"2(WA) 11. GLC (Encapsulated) AOAC-13; 6.409 Parinol (1559) 1. GLC (FID-IS) NEIC-1559-1 Paris Green (529) 1. Total Arsenic AOAC-13; 6.035 2. Total Arsenious Oxide AOAC-13; 6.036/6.038 3. Total Copper (Electrolytic) AOAC-13; 6.040 4. Total Copper (Titrimetric) AOAC-13; 6.041 Parnon (See "Parinol" 1559) Patoran (See "Metobromuron" 1439) PBO (See "Piperonyl Butoxide" 1657) PCNB (See "Pentachloronitrobenzene" 1563) PCP (See "Pentachlorophenol" 1564) ------- P-2 Pebulate (1746) 1. GLC (FID-IS) AOAC-13; 6.426 2. GLC (TCD) EPA-l-Tent. 3. GLC (FID-IS) EPA-2-Tent. 4. GLC (FID-IS) EPA-3-Tent. Pendimethalin (1559.5) 1. GLC (FID-IS) Zweig X; p. 463 Pentac (620) 1. GLC (TCD-IS) NEIC-620-1 Pentachloronitrobenzene (1563) 1. IR Zweig III; p. 129 2. GLC Zweig VI; p. 577 3. GLC (In Fertilizer Mixtures) JAOAC 55. 657 (1972) 4. GLC (FID-IS) JAOAC 59, 708 (1976) 5. Colorimetric NEIC-1563-1 Peritachlorophenol (1564) and Sodium Salt (1566) 1. HPLC (See "Phenols and Chlorophenols/EPA-5-Tent. ") 2. GLC (As Methyl Ester) NEIC-1564-2 3. HPLC (With Bromacil in Oil Sprays) NEIC-1564-3 4. HPLC NEIC-1564-4 5. UV Zweig V; p. 314 6. GLC Zweig VI; p. 582 7. IR CIPAC-1; p. 730 8. Total Chlorine (See "Phenols and Chlorophenols/EPA-3") 9. Total Acidity AWPA; A5-74-1 10. Colorimetric AWPA; A5-74-6 11. GLC and TLC (In Paints) JAOAC 58, 19 (1975) 12. HPLC JAOAC 62, 1004 (1979) 13. HPLC (RP-IS) NEIC-1564-5 14. HPLC (with Bromacil & 2,4-D IOE) NEIC-1564-6 Perfluidone (1575) 1. GLC (FID-IS) Zweig X; p. 437 Permethrin (1575.5) 1. GLC (Aqueous Formulations) JAOAC 60, 9 (1977) 2. GLC (FID-IS) NEIC-1575.5-1 3, GLC NEIC-1575.5-2 Perthane (220) 1. IR . NEIC-220-1 (VA) ------- P-3 Petroleum Oils (1583) 1. Gravimetric (Neutral Oil Content) CIPAC-1; p. 583 Phaltan (See "Folpet" 1114) Phenkapton (816) Phenmedipham (1588) 1. TLC Zweig VII; p. 615 2. Hydrolysis/Titration NEIC-1588-1 3. Redox Titration NEIC-1588-1 Phenol (1589) Phenols and Chlorophenols 1. Definition, Structure, and Tech. Data EPA-1 2. UV (o-Phenylphenol) EPA-2 3. Total Chlorine (Lime Fusion) EPA-3 4. Bromination/Titration (o-Phenylphenol) .... EPA-4 5. HPLC (Pentachlorophenol) EPA-5-Tent. 6. GLC (FID) EPA-6-Tent. 7. GLC (FID/TCD) (4-Chloro-3,5-xylenol) EPA-7-Tent. 8. GLC (TCD-IS/TMS Der.) EPA-8-Tent. 9. HPLC (RP) NEIC-Phenols-1 Phenothiazine (1591) 1. Colorimetric AOAC-13; 42.128 2. GLC AOAC-13; 38.815 3. IR F.^A-l-Tent. 4. HPLC JAOAC 59, 693 (1976) 5. GLC (FID-IS) NEIC-1591-1 6. GLC (FID-IS) (Feeds) NEIC-1591-2 7. GLC (FID-IS) NEIC-1591-3 Phenothrin (1595) 1. GLC NEIC-1595-1 Phenoxy Herbicides (See "Chlorophenoxy Herbicides") Phenthoate (1040) 1. GLC (TCD-IS) Zweig VIII; p. 161 2. TLC Zweig VIII; p. 164 3. GLC NEIC-1040-1 Phenyl mercuric Acetate (1606) ------- P-4 o-Phenylphenylphenol (1631) and Sodium Salt (1636) 1. UV (See "Phenols and Chlorophenols/EPA-2") 2. Bromination/Titration (See "Phenols and Chlorophenols/EPA-4") 3. GLC (See "Phenols and Chlorophenols/EPA-6 and EPA-8-Tent.") 4. HPLC NEIC-1631-1 Phorate (1639) 1. IR AOAC-13; 6.415 2. IR EPA-1 3. GLC Zweig VI; p. 493 4. GLC NEIC-1639-1 Phosalone (1640) 1- GLC Zweig VII; p. 387 Phosdrin (See "Mevinphos" 356) Phosfolan (594) 1. UV Zweig VII; p. 419 2. GLC (FID-IS) Zweig VII; p. 236 Phosmet (1312) 1- IR Zweig V; p. 261 2. GLC Zweig VI; p. 408 3. IR, GLC & Colorimetric -JA0AC 52, 1017 (1969) Phosnichlor (See "Dicapthon" 677) Phosphamidon (1641) 1. Titrimetric Zweig II; p. 377 2. GLC NEIC-1641-1 3. IR NEIC-1641-2(VA) Phosphoric Acid (1642) 1. Potentiometric Titration (also with HC1) . . . NEIC-1642-1 Phosphorus (Total) 1. Gravimetric EPA-1 Phosphorus Paste 1. Gravimetric (See "Phosphorus/EPA-l") Phostoxin (See "Aluminum Phosphide" 92) Phosvel (See "Leptophos" 1280) Phoxim (1603) ------- P-5 Phthalthrin (See "Tetramethrin" 1957) Phygon (See "Oichlone" 680) Picloram (1645) 1. HPLC (with 2,4-D) AOAC-13; 6.308 2. HPLC EPA-l-Tent. 3. IR Zweig V; p. 512 4. GLC (As Methyl Ester) NEIC-1645-1 (CA) 5. UV NEIC-1645-2 Pindone (1661) 1. UV (Ether Extraction) EPA-1 2. UV (Pyrophosphate Extraction) EPA-2 3. UV (Water Soluble Formulations) EPA-3 Pine Oil (1651) 1. Gravimetric NEIC-1651-1 2. Fatty or Rosin Acid Content NEIC-1651-2 3. Water/Alcohol Content NEIC-1651-3 Piperalin (1424) Piperonal (1656) 1. GLC NEIC-1656—1 Piperonyl Butoxide (1657) 1. Colorimetric AOAC-13; 6.166 2. Qualitative Test EPA-1 3. GLC (FID-IS) EPA-2 4. GLC (See "Pyrethrins/EPA-2") 5. IR NEIC-1657-3(VA) 6. IR CIPAC-1; p. 730 7. TLC (Semi-Quantitative) NEIC-1657-1 8. GLC (FID-IS; with diazinon) NEIC-1657-2 Pirimicarb (1658) 1. Titrimetric Zweig VII; p. 401 2. Colorimetric Zweig VII; p. 401 3. GLC Zweig VII; p. 401 4. UV EPA-l-Tent. Pirimiphos Ethyl (1659) 1. GLC Zweig VIII; p. 174 2. TLC/UV Zweig VIII; p. 177 3. Hydrolysis/UV Zweig VIII; p. 179 ------- P-6 Pirimiphos Methyl (1660) 1. GLC 2. TLC/UV . . . 3. Hydrolysis/UV 4. HPLC .... Zweig VIII; p. 189 Zweig VIII; p. 190 Zweig VIII; p. 190 JAOAC 60, 14 (1977) Pival (See "Pindone" 1661) Planavin (See "Nitralin" 1433) Plantvax (See "Oxycarboxin" 1549) Plictran (See "Cyhexatin" 608) PMP (1257) 1. UV (Ether Extraction) EPA-1 2. UV (Pyrophosphate Extraction) EPA-2 3 UV (Aqueous Formulations) EPA-3 Polaris (See "Glyphosine" 1133) Polychlorinated Biphenyls (1666) Polyram (108) 1. Carbon Disulfide Evolution NEIC-108-1 Potassium Azide (1695) 1. GLC NEIC-1695-1 Potassium Bisulfate (1692) Potassium Chromate (1700) 1. Titrimetric NEIC-1700-1 Potassium Cyanate (1701) 1. Gravimetric AOAC-13; 6.098 Potassium Cyanide (1702) 1. Titrimetric AOAC-13; 6.100 Potassium Dichloro-s-triazinetrione (1703) (See "Available Chlorine") Potassium-N-methyldithiocarbamate (1715) Potassium Permanganate (1719) 1. Titrimetric NEIC-1719-1 ------- P-7 Potassium Persulfate (1721) 1. Titrimetric NEIC-1721-1 Pramitol (See "Prometone" 1735) Prefar (See "Bensulide" 862) Preforan (See "Fluorodifen" 1111) Primidophos (12) Princep (See "Simazine" 1816) Probe (See "Methazole" 1326) Procyazine (1733) 1. GLC NEIC-1733-1 Profluralin (1734) 1. GLC (FID-IS) Zweig X; p. 453 Promacyl 1. GLC (FID-IS) Zweig VIII, p. 209 & Zweig XI; p. 141 2. GLC (Cattle Dips) Zweig VIII, p. 214 & Zweig XI; p. 144 Promecarb (609) Prometone (1735) 1. GLC AOAC-13; 6.433 2. GLC (TCD-IS) EPA-l-Tent. 3. GLC (FID-IS) EPA-2-Tent. 4. Non-aqueous Titration Zweig IV; p. 173 Prometryn (1736) 1. GLC AOAC-13; 6.433 2. Non-aqueous Titration Zweig IV; p. 181 Pronamide (690) 1. GLC NEIC-690- 2. GLC (FID-IS) Zweig VIII; p. 445 3. GLC NEIC-690-2 Propachlor (432) Propanil (791) 1. Total Chlorine Zweig IV; p. 326 2. GLC NEIC-791-1 ------- P-8 Propargite (1737) 1. IR 2. GLC (TCD-IS) Propazine (1740) 1. Labile Chlorine Propham (1241) 1. Hydrolysis/Titration . . 2. HPLC (See "Quintex") Prophos (See "Ethoprop" 1241) Propionic Acid (1742) Propoxur (1238) 1. IR 2. Colorimetric 3. IR (Bait Formulations) . 4. HPLC (Oil Sprays). . . . 5. GLC 6. IR 7. HPLC Propylene Glycol (1749) 1. GLC (TCD-IS) 2. GLC (FID-IS) 3. Titrimetric n-Propyl Isome (955) Prosulfalin (1754) Protect 1. IR 2. GLC Prothoate (832) 1. GLC (TCD-IS) 2. TLC/Total Phosphorus . . Prowl (See "Pendimethalin" 1559.5) Proxel (181) 1. HPLC EPA-l-Tent. EPA-2-Tent. Zweig IV; p. 188 CIPAC-1; p. 593 Zweig VII; p. 165 NEIC-1238-1 NEIC-1238-2 NEIC-1238-3 NEIC-1238-4 NEIC-1238-5 NEIC-1238-6 EPA-l-Tent. AOAC-13; 35.007 AOAC-13; 19.006 Zweig VIII; p. 484 NEIC-Protect-1 Zweig VIII; p. 215 Zweig VIII; p. 217 NEIC-181-1 Pydrin (See "Fenvalarate" 590) ------- P-9 Pyrazon (1756) 1. IR EPA-l-Tent. 2. UV EPA-2-Tent. 3. GLC JAQAC 61, 161 (1978) Pyrazophos (1070) 1. TLC/Total Sulfur Zweig X; p. 239 Pyrethrins (1757) 1. Titrimetric (Deniges) AOAC-13; 6.169 2. Description EPA-1 3. GLC (FID) EPA-2 4. Titrimetric (Seil) EPA-3 5. TLC (with PBO) NEIC-1757-1 6. GLC (with PBO and MGK-264) Zweig VIII; p. 232 7. HPLC (RP) NEIC-1757-2 8. HPLC (Silica) NEIC-1757-3 Pyridine (7159) 1. Distillation/Titration NEIC-1759-1 Pyrolan (1422) 1. Hydrolysis/Distillation Zweig II; p. 416 Pyroxychlor (1764) ------- Q-l Quaternary Ammonium Compounds 1. Chloride Titration (Potentiometric) AOAC-13; 6.440 2. Chloride Titration (Absorption Indicator). . . AOAC-13; 6.441 3. Conversion Factors EPA-1 4. Auerbach Qualitative Test EPA-2 5. Ferricyanide Method EPA-3 6. Epton Titration EPA-4 7. Chloride/Bromide (Potentiometric Titr'n) . . . EPA-5 8. Colorimetric NEIC-Quat-1 9. Titrimetric NEIC-Quat-2(CA) 10. Gravimetric NEIC-Quat-3(CA) Quinalphcs (835) 1. TLC/UV Zweig XI; p. 149 2. GLC (FID-IS) Zweig XI; p. 151 8-Quinolinol Sulfate (1768) 1. UV NEIC-1768-1 ® Quintex (Fenuron + Propham + Chlorpropham) 1. HPLC (RP) Zweig XI; p. 344 Quintiofos (1083) 1. GLC (Dip washes) NEIC-1083-1 ------- R-l Rabon (See "Tetrachlorvinphos" 503) Ramrod (See "Propachlor" 432) Randox (See "CDAA" 649) Raticate (See "Norbormide" 1502) Red Squill (1772) 1. Paper Chromatography/Fluorescence NEIC-1772-1 2. General Description NEIC-1772-1 Resmethrin (1773.5) 1. IR EPA-l-Tent. 2. GLC (TCD) EPA-2-Tent. 3. GLC (TCD-IS) EPA-3-Tent. 4. HPLC EPA-4-Tent. 5. GLC (FID-IS) EPA-5-Tent. 6. GLC Zweig VII; p. 445 7. GLC (Separates Isomers) Zweig VII; p. 447 8. Colorimetric Zweig VII; p. 448 Rogor (See "Dimethoate" 863) Rogue (See "Propanil" 791) Ro-Neet (See "Cycloate" 1037) Ronnel (1775) 1. GLC (Feeds) AOAC-13; 42.145 2. UV (Mineral Feeds) AOAC-13; 42.148 3. IR EPA-1 4. GLC (FID-IS) EPA-2 5. IR (Korlan, Smears, etc.) NEIC-1775-1 6. GLC (FID-IS) NEIC-1775-2 7. Colorimetric (Feeds and Dips) NEIC-1775-3 8. IR CIPAC-1; p. 730 Rotenone (1776) 1. Crystallization AOAC-13; 6.160 2. Total Ether Extract AOAC-13; 6.165 3. IR AOAC-13; 6.163 4. Qualitative Test EPA-1 5. TLC NEIC-1776-1 6. GLC (Reduction with NaBH4) NEIC-1776-2 7. Colorimetric CIPAC-1; p. 611 8. GLC J AO AC 56, 1342 (1973) 9. HPLC (Silica) JA0AC 58, 958 (1975) 10. HPLC (Reverse Phase) NEIC-1776-3(TX) 11. UV and IR (Effects of other Rotenoids) .... JAOAC 59, 703 (1976) 12. HPLC (RP) NEIC-1776-4 ------- R-2 Round-Up (See "Glyphosate" 1132) Rowmate (See "Dichlormate" 681) Rowtate (See "Cisanilide" 517) Rozol (See "Chlorophacinone" 481) Ruelene (See "Crufomate" 575) Ryanodine (1777) 1. UV NEIC-1777-1 (CA) ------- Sabadilla Alkaloid (1778) 1. Gravimetric Safrole (1779) 1. GC (Semi-quant.) . . . . Salicylanilide (1780) 1. UV Salithion (1330) 1. Colorimetric 2. GLC Saturn (See "Benthiocarb" 1968) SBP-1382 (See "Resmethrin" 1773.5) Schrader. (1509.5) 1. Differential Hydrolysis. 2. Hydrolysis/Titration . . Secbumaton (1783) 1. Potentiometric Titration Sector (See "Butralin" 278) Selenium (1784) 1. Gravimetric 2. Gravimetric Sencor (See "Metribuzin" 100) Sendran (See "Propoxur" 1238) Sesame Oil (1786) 1. Qual. test Sesone (772) 1. Hydrolysis/Titration . . Sevin (See "Carbaryl" 353) Siduron (1787) 1. UV 2. Hydrolysis/Distillation. S-l AOAC-13; 6.173 AOAC-13; 12.046 EPA-1 Zweig VII; p. 433 Zweig VII; p. 435 CIPAC-1; p. 621 NEIC-1509.5-1 NEIC-1783-1 NEIC-1784-1 NEIC-1784-2 AOAC-13; 28.118 Zweig IV; p. 201 EPA-l-Tent. NEIC-1787-1 ------- S-2 Silica Gel (1788) 1. Gravimetric NEIC-1788-1 Silver (1790) 1. Titrimetric AOAC-13; 36.092 Si 1 vex (1795) 1. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent 2. GLC (See "Chlorophenoxy Herbicides/EPA-5-Tent.") 3. GLC (As TMS Ester) Zweig VI; p. 688 Silvex, Propylene Glycol Butyl Ether Ester (1798) 1. Hydrolysis/Titration NEIC-1798-1 Simazine (1816) 1. GLC AOAC-13; 6.431 2. Labile Chlorine (See "Chloro-Triazine Herbicides/EPA-1") 3. UV (0.1% Aqueous Suspension) EPA-l-Tent. 4. Non-Aqueous Titration Zweig IV; p. 217 Soap (1817) 1. Moisture by Distillation AOAC-13; 6.123 2. Sodium and Potassium AOAC-13; 6.124 Sodium Arsenate (1822) 1. Titrimetric AOAC-13; 6.046 Sodium Arsenite (1823) 1. Titrimetric AOAC-13; 6.045 Sodium Benzoate (1825) 1. Titrimetric NEIC-1825-1 Sodium Bisulfate (1819) 1. Titrimetric NEIC-1819-1 Sodium Bisulfite (1829) 1. Titrimetric NEIC-1829-1 Sodium Carbonate (1832) 1. Titrimetric AOAC-13; 5.019 Sodium Chlorate (1833) 1. Titrimetric EPA-1 2. Titrimetric CIPAC-1; p. 626 ------- S-3 Sodium Cyanide (1843) 1. Titrimetric AOAC-13; 6.100 2. Titrimetric NEIC-1843-1 Sodium Dichloro-s-triazinetrione (1844.5) (See "Available Chlorine") Sodium Dimethyldithiocarbamate (1846) 1. HPLC (with 2-Mercaptobenzothiazole) NEIC-1846-1 Sodium Fluoride (1850) 1. Total Fluorine AOAC-13; 6.019 2. Titrimetric NEIC-1850-1 Sodium Fluoroacetate (1851) 1. GLC (derivitization) JAOAC 63, 49 (1980) Sodium Hydroxide (1854) 1. Titrimetric AOAC-13; 5.019 Sodium Hypochlorite (1856) 1. Titrimetric AOAC-13; 6.111 2. Chloride Content AOAC-13; 6.114 3. Sodium Hydroxide Content AOAC-13; 6.115 4. Titrimetric (Rel. Iodine) NEIC-1856-1 Sodium Metaborate (1863) Sodium Selenate (1880) Sodium Trichloroacetate (1888) 1. Titrimetric AOAC-13; 6.312 2. Decarboxylation/Titration CIPAC-1; p. 691 Solan (1892) 1. Total Chlorine NEIC-1892-1 Sorbic Acid (1893) and Potassium Salt (1894) Spectracide (See "Diazinon" 824) Spergon (See "Chloranil" 382) Spike (See "Tebuthiuron" 1920) Stabilene (See "Butoxypropylene Glycol" 276) Stam (See "Propanil" 791) Starlicide (499) 1. Colorimetric NEIC-499-1 ------- S-4 Streptomycin (1898) and Sulfate (1899) 1. UV EPA-1 Strobane (1927) Strychnine Alkaloid (1900) and Sulfate (1901) 1. Gravimetric EPA-1 2. UV EPA-2 3. HPLC EPA-3-Tent. 4. GLC JAOAC 58, 961 (1975) 5. HPLC JAOAC 58, 957 (1975) 6. UV NEIC-1900-1 7. HPLC (Reverse Phase) JAOAC 61, 612 (1978) 8. HPLC (Reverse Phase, I.S.) NEIC-1900-2 9. HPLC (Anion Exchange) NEIC-1900-3 Sulfallate (See "CDEC" 396) Sulfamic Acid (1904) 1. Titrimetric NEIC-1904-1 Sulfanilamide (1905) Sulfaquirioxaline (1771) 1. Colorimetric . AOAC-13; 42.179/.184 2. HPLC (With Warfarin) EPA-l-Tent. Sulfotepp (1948) 1. GLC Zweig VI; p. 483 Sulfoxide (1522) 1. UV AOAC-13; 6.419 Sulfur (1911) 1. Gravimetric (Sulfide Sulfur) AOAC-13; 6.107 2. Gravimetric (CS? Extraction) EPA-1 3. Gravimetric (Nitric Acid Oxidation) EPA-2 4. Gravimetric (Acetone Method) EPA-3 5. Titrimetric CIPAC-1; p. 632 Sulfur Dioxide (1912) 1. Titrimetric (Fumigants) EPA-1 Sulfuric Acid (1914) 1. Titrimetric NEIC-1914-1 Sulfuryl Fluoride (1916) ------- S-5 Sulphenone (482) Sulprofos (See"Bolstar" 1078) Sumithion (See "Fenitrothion" 897) Supona (See "Chlorfenvinphos" 412) Supracide (See "Methadathion" 1327) Surflan (See "Oryzalin" 1539) Sustar (See "Fluridamid" 1108) Sutan (See "Butylate" 1039) Swep (1917) Systox (See "Demeton" 632) ------- T-l 2,4,5-T (2024) 1. UV (With 2,4-D) (See "Chlorophenoxy Herbicides/EPA-2") 2. HPLC (See "Chlorophenoxy Herbicides/EPA-3-Tent.") 3. Extraction/Titration CIPAC-1; p. 642 4. GLC (As Methyl Ester) NEIC-2024-1 5. HPLC NEIC-2024-2 6. GLC (As TMS Ester) Zweig VI; p. 630 7. GLC (As TMS Ester, on-column) NEIC-2024-3 8. HPLC AOAC-13; 6.A23 2,4,5-T, Butoxyethanol Ester (2039) 1. GLC (See "Chlorophenoxy Herbicides/EPA-4-Tent.") 1. Hydrolysis/Titration CIPAC-1; p. 646 2,4,5-T, Isooctyl Ester (2043) Tabutrex (See "Dibutyl Succinate" 669) Talon (See "Brodifacoum" 242.5) Tandex (See "Karbutylate" 1261) 2,4,5-TB (2048) TBA (2008) TCA (See "Trichoroacetic Acid" 2005) TCC (2011) TCNB (See "Tecnazine" 1934) TOE (693) 1. IR NEIC-693-l(VA) Tebuthiuron (1920) 1- UV NEIC-1920-1 2. GLC (FID-IS) Zweig XI; p. 355 3. HPLC (Silica) Zweig XI; P. 353 Tecnazene (1934) 1. Polarography CIPAC-1; p. 663 Tedion (See "Tetradifon" 1946) Telodrin (See "Isobenzan" 1508) Telone (See "D-D Mixture" 790.5) Telvar (See "Monuron" 1450) ------- T-2 Temephos (1921) 1. UV Zweig VII; p. 121 2. GLC Zweig VII; p. 125 Temik (See "Aldicarb" 18) Tenoran (See "Chloroxuron" 505) TEPP (1949) 1. Titrimetric ADAC-13; 6.420 2. Hydrolysis/Titration CIPAC-1; p. 567 Terbacil (1922) 1. HPLC Zweig X; p. 485 2. IR Zweig X; p. 485 Terbufos (1924) 1. GLC (FID-IS) Zweig XI; p. 166 Terbut (See "Secbumeton" 1783) Terbuthylazine (1925) 1. GLC (FID-IS) A0AC-13;6.B20 Terbutol (670) 1- IR EPA-l-Tent. 2. GLC (FID-rS) EPA-2-Tent. 3. UV NEIC-670-1 Terbutryn (1926) 1. GLC A0AC-13; 6.431 2. IR NEJC-1926-1 Terperte Polychlorinates (See "Strobane" 1927) Terraclor (See "Pentachloronitrobenzene" 1563) Terramycin (1552) Terrazole (1029) 1. GLC NEIC-1029-1 2. IR (With PCNB) NEIC-1029-2 3. GLC (With PCNB) NEIC-1029-3 2,3,5,6-Tetrachloro-4-(methylsulfonyl)pyridine (1933) 1. GLC NEIC-1933-1 2. UV NEIC-1933-2 ------- T-3 Tetrachlorophenols (1935) and Sodium Salts (1938) 1. IR CIPAC-1; p. 730 2. Titrimetric NEIC-1935-1 3. IR NEIC-1935-2 4. GLC (See "Pentachlorophenol/NEIC-1564-2") 5. HPLC (See "Pentachlorophenol/NEIC-1564-4") Tetrachlorothiophene (1943) Tetrachlorvinphos (503) 1. GLC Zweig VII; p. 299 2. IR Zweig VII; p. 302 3. GLC (FID-IS) NEIC-503-1 Tetradifon (1946) 1. GLC Zweig X; p. 121 2. GLC Zweig II; p. 474 3. Total Chlorine (Na Reduction) Zweig II; p. 475 4. IR CIPAC-1; p. 730 5. GLC (FID-IS) A0AC-13;6.B09 Tetralin (1953.5) Tetraethylpyrophosphate (See "TEPP" 1949) Tetramethrin (1957) 1. GLC Zweig VII; p. 349 2. TLC/UV Zweig VII; p. 347 3. GLC (With Resmethrin) NEIC-1957-1 4. GLC (With Synergists) NEIC-1957-2 Tetrasul (487) TFM (See "Lamprecide" 2081) TH-6040 (See "Diflubenzuron" 839) Thallium Sulfate (1964) 1. Gravimetric AOAC-13; 6.140 2. AA NEIC-1964-1 Thanite (1227) 1. Total Nitrogen AOAC-13; 6.423 Thiabendazole (1965) 1. Colorimetric AOAC-13; 42.185 2. Titrimetric NEIC-1965-1 3. UV Zweig VIII; p. 301 4. Colorimetric JAOAC 58, 971 (1975) ------- T-4 Thimet (See "Phorate" 1639) Thiobencarb (1968) Thiocarbamates 1. GLC Thiocyanates 1. Total Nitrogen Thi ocyclam-Hydrogenoxalate 1. HPLC (RP-IS) Thiodan (See "Endosulfan" 1001) Thiofanox (1974) Thiometon (1086) 1. IR 2. GLC (FID-IS) 3. GLC Thiophanate (829) 1. UV 2. HPLC (with Thiram) Thiophanate-Methyl (1975) 1. Colorimetric 2. UV Thiourea (1977) 1. Qualitative Tests Thiram (1978) 1. CS2 Evolution 2. UV 3. IR 4. IR 5. HPLC (RP with Thiophanate) 6. HPLC (RP-IS) Thymol (1979) 1. Titrimetric TIBA (2084) Tiguvon (See "Fenthion" 1098) Til lam (See "Pebulate" 1746) Tin & Tin Compounds 1. Titrimetric (See "Bis(tributyltin)oxide/EPA-l") Tiocarbenil (1629.3) 1. GLC (FID-IS 2. TLC AOAC-13; 6.426 AOAC-13; 6.423 Zweig XI; p. 187 CIPAC-1; p. 730 Zweig VIII; p. 242 NEIC-1086-1 NEIC-829-1 NEIC-829-2 (VT) NEIC-1975-1 NEIC-1975-2 AOAC-13; 20.115/.116 AOAC-13; 6.342 EPA-1 EPA-2 CIPAC-1; p. 730 NEIC-1978-1 (VT) NEIC-1978-2 AOAC-13; 37.140/.142 Zweig XI; p. 309 Zweig XI; p. 311 ------- T-5 Tirpate (878) TOK (See "Nitrofen" 786) Tolban (See "Profluralin" 1734) Toluene (1982) 1. GC AOAC-13; 5.012 Topcide (See "Benzadox" 175) Topsin (See "Thiophanate" 829) Topsin M (See "Thiophanate-Methyl" 1975) Torak (See "Dialifor" 636) Tordon (See "picloratn" 1645) Toxaphene (1986) 1. IR Zweig II; p. 531 2. Total Chlorine Zweig II; p. 525 3. IR CIPAC-1; p, 730 4. IR NEIC-1986-1 2,4,5-TP (See "Si 1 vex" 1795) Treflan (See "Trifluralin" 2082) Triallate (2006) 1. GLC NEIC-2006-1 Triarimol (1987) 1. GLC JAOAC 56, 11 (1973) Triazine Herbicides 1. GLC AOAC-13; 6.431 2. Titrimetric JAOAC 54, 4 (1971) 3. GLC Zweig X; p. 513 s-Triazinetriol (593) (See "Available Chlorine") Triazophos (831) 1. TLC/Total Sulfur Zweig X; p. 129 3,4,5-Tribromosalicylani1ide (1989) 1. UV (See "Brominated Salicylani1ides/EPA-1") ------- T-6 Tributyl Tin Fluoride (1997) (See "Tin" and "Fluorine") Tributyltin oxide (See "Bis(tributyltin)oxide" 229) Tricamba (2004) Trichloroacetic Acid (2005) 1. Decarboxylation/Titration 1.2.4-Trichlorobenzene (2007) 2,3,6-Trichlorobenzoic Acid (2008) 3,4,4'-Trichlorocarbani1ide (2011) 1. UV 1,1,1-Trichloroethane (2013) Trichloroethylene (2014) 1. IR Trichlorofon (913) 1. IR 2. GLC (FID-IS) 3. Hydrolyzable Chlorine 4. Dehydrohalogenation 5. GLC 6. GLC (TMS Der.) Trichloromelamine (2016) (See "Available Chlorine") Trichloromethylfos (See "Chlorpyriphos Methyl" 510) Trichloronitromethane (See "Chloropicrin" 490) Trichloronat (1090) 2.4.5-Trichlorophenol (2020) and Sodium Salt (2023) Trichloro-s-triazinetrione (2060) (See "Available Chlorine") Triclopyr (2062) (Z)-9-Tricosene (2064) 1. GLC 2. GLC CIPAC-1; p. 691 EPA-1 AOAC-13; 36.013 EPA-l-Tent. EPA-2-Tent. Zweig II; p. 201 Zweig II; p. 202 Zweig VI; p. 387 JAOAC 57, 1128 (1974) NEIC-2064-1 NEIC-2064-2 ------- T-7 Tricresyl Phosphate (2065) Tricyclazole (2066) 1. GLC (FID-IS) Zweig XI; p. 265 2. HPLC (Silica) Zweig XI; p. 267 Tridemorph (915) Triethanolamine (2070) Triethylene Glycol (2078) 1. GLC EPA-l-Tent. Trifenofos (2080) Trifenson (See "Sulphenone" 482) Trifluralin (2082) 1. UV AOAC-13; 6.203 2. GLC A0AC-13; 6.209 3. GLC (FID-IS) EPA-1 4. IR EPA-2 5. GLC (Separation from Benefin) NEIC-2082-1 Triforine (2083) 1. TLC/Densitometry Zweig X; p. 245 2. Total Chlorine Zweig X; p. 247 3. Non-Aqueous Titration NEIC-2083-1 4. HPLC NEIC-2083-2 Triphenyltin Hydroxide (2101) 1. UV NEIC-2101-1 2. GLC JAOAC 61, 1507 (1978) 3. Potentiometric Titration AOAC-13; 6.436 4. GLC (with Dithiocarbamates) Zweig XI; p. 231 Triprene (2103) Tris-Nitro (See "2-Hydroxymethyl-2-nitro-l,3-propanediol" 1207) Trithion (See "Carbophenothion" 361) 4-Tritylmorpholine (2108) Tropital (See "Piperonal" 1656) Troysan 174 (See "2-((Hydroxymethyl)amino)ethanol" 1204) Trysben (See "TBA" 2008) ------- 1-8 Tunic (See "Methazole" 1326) Tupersan (See "Siduron" 1787) Turkey Red Oil (2109) Turpentine (2111) Tyrothricin (2112) ------- u-l Urea (2114) Ureas, Substituted 1. HPLC NEIC-SU-1 Urox (See "Monuron Trichloroacetate" 1451) ------- V-l Vacor (1763.5) 1. UV EPA-l-Tent. 2. HPLC EPA-2-Tent. 3. HPLC JAOAC 60, 1375 (1977) 4. HPLC NEIC-1763.5-1 5. Potentiometric Titration NEIC-1763.5-2 Valone (See "PMP" 1257) Vamidothion (904) 1. Titrimetric Zweig VII; p. 483 2. GLC Zweig VII; p. 481 Vapam (1865) 1. Carbon Disulfide Evolution Zweig III; p. 180 2. Colorimetric Zweig III; p. 180 Vapona (See "DDVP" 797) VBT (See "Vinylene Bisthiocyanate" 2116) Vegadex (See "CDEC" 396) Vendex (1165) 1. IR NEIC-1165-1 2. Non-Aqueous Titration NEIC-1165-2 Venzar (See "Lenacil" 1279) Vernolate (1747) 1. GLC AOAC-13; 6.426 2. IR EPA-1 3. GLC (FID-IS) EPA-2 4. GLC (TCD-IS) EPA-3-Tent. 5. HPLC (RP) EPA-4-Tent. Vikane (See "Sulfuryl Fluoride" 1916) Vinyl Chloride 1. GLC (Qual. Test) NEIC-VCM-1 2. IR (Qual. Test) NEIC-VCM-2 3. GLC/IR (Qual. Test, Also Other Propellants). . NEIC-VCM-3 Vinylene Bisthiocyanate (2116) 1. Polarographic NEIC-2116-1 Vitavax (See "Carboxin" 362) Vydate (See "Oxamyl" 1543) ------- w-l Warfarin (2117) 1. UV (Ether Extraction) AOAC-13; 6.141 2. HPLC EPA-l-Tent. 3. UV (Pyrophosphate Extraction) EPA-2 4. HPLC (Sodium Salt) EPA-3-Tent. 5. UV (Silicic Acid Clean-up) Zweig III; p. 203 6. UV (Ether/Hexane Extraction) Zweig VII; p. 678 7. HPLC JAOAC 59, 1104 (1976) 8. HPLC (RP, with Sulfaquinoxaline) NEIC-2117-1 Water 1. Oistillation (Soap) AOAC-13; 6.123 2. Oistillation (Pine Oils) NEIC-H20~1 3. Distillation (Phenolic or Coal-tar Creosote) . NEIC-H20"2 4. Distillation (Liquor Creosolis Saponatus). . . NEIC-H20~3 5. Isopropanol Conversion Table NEIC-H20-4 Wepsyn (103) ------- X-l Xylene (2121) ------- Zectran (See "Mexacarbate" 1441) Zinc and Zinc Compounds 1. Gravimetric AOAC-13; 6.017 2. Titrimetric NEIC-Zn-l(CA) Zinc Arsenite (2126) 1. Total Arsenic AOAC-13; 6.058 2. Total Arsenious Oxide AOAC-13; 6.059/.060 3. Water Soluble Arsenic A0AC-13; 6.061 4. Total Zinc AOAC-13; 6.062 Zinc Fluosilicate (2131) 1. Titrimetric AOAC-13; 6.021 Zinc Naphthenate (2137) 1. Gravimetric AOAC-13; 6.017 Zinc Phosphide (2141) 1. Phosphine Evolution (KMn04 Oxidation) EPA-1 2. Phosphine Evolution (GLC-FPD) EPA-2 3. Phosphine Evolution (Iodometric Titration) . . CIPAC-1; p. 703 Zineb (2151) 1. Carbon Disulfide Evolution A0AC-13; 6.338 Ziram (2153) Zoalene (2154 1. Qualitative Test AOAC-13; 42.001 2. Colorimetric AOAC-13; 42.190 Zolone (See "Phosalone" 1640) Zytron (783) 1. IR NEIC-783-1 (VA) ------- |