HEXAHY»R«-1,3,5-TRINITR»- 1,3,5-TRIAZINE (RDX) PROFILE OF DRINKING WATER CONTAMINANTS FOR EMERGENCY RESPONSE GENERAL INFORMATION Hexahydro-1,3,5-trinitro-1,3,5-triazine, commonly designated RDX (British code name for Research De- partment Explosive or Royal Demolition Explosive), is an extensively used high-impact explosive in munition formulations. It is also used as a rat poison. RDX is chemically stable and can be stored up to 10 months at 85°C without deteriorating. Production in the United States is mainly at one Army ammunition plant. RDX in wastewater is not expected to be appreciable because of the low solubility of RDX in water. However, the potential for aquatic pollution may exist from RDX manufacturing, loading, transportation, and storage. In soils, RDX persists, resists aerobic bacterial degradation, and slowly leaches into ground water. RDX is rapidly degraded by light. Volatilization is not a significant environmental fate. PHARMACOKINETICS RDX is completely absorbed when ingested, the rate being faster in rats than in humans, and rapidly dis- tributes to body tissues. Highest RDX levels are found in kidneys, liver, brain, and heart. RDX is metabolized by the liver, and its metabolites are excreted in urine. The metabolites have not been characterized. HEALTH EFFECTS Humans In some case studies of RDX ingestion by military personnel, symptoms of central nervous system (CNS) dysfunction including convulsions and coma were ob- served. Data gathered through an occupational health study at an Army ammunition plant indicated that inhalation of dust containing RDX at unknown levels causes nausea and CNS dysfunction including convulsions and unconscious- ness. In another study, medical tests of workers exposed to 1.57 mg RDX/m3 or less revealed no adverse health effects. HEALTH EFFECTS Experimental Animals Single oral doses of RDX in rats and mice produce convulsions, labored breathing, and other CNS effects. Oral doses of RDX for 10 days in monkeys induced vomiting and convulsions. Tests in rabbits indicate that RDX produces dermatitis. Slight erythema was observed in guinea pigs after the first but not subsequent applications. No con- clusive results were obtained in dogs given repeated topical applications of RDX. Toxic effects seen in 13-week feeding studies with rats and mice were increased liver weights and anemia. Lifetime feeding studies in rats and mice showed in- creased mortality, weight loss, anemia, liver and kidney toxicity, testicular degeneration, and prostate inflamma- tion. Decreased fertility was observed in a two-genera- tion reproductive study in rats. Decreased pup weights and embryo toxicity but no teratogenic effects were seen in the F, litter. RDX has not been found to be mutagenic. It in- duces hepatocellular carcinomas and adenomas in mice. OTHER CRITERIA, ANALYSES, AND TREATMENT TECHNOLOGIES The American Conference of Governmental Industrial Hygienists (ACGIH) 8-hour time-weighted average Threshold Limit Value (TLV) for exposure to RDX is 1.5 mg/m3. The U.S. Army Medical Bioengineering Research and Development Laboratory recommends an RDX limit of 0.03 mg/L in drinking water. Methods are available for the analysis of RDX in bulk material and in trace quantities. Volumetric meth- ods involving reduction, hydrolysis, or acid-base titra- tions are used for bulk analysis. For analyzing trace quantities (below 10 parts per million), high-perfor- mance liquid chromatography appears to be the method of choice. Other methods include thin-layer chroma- tography, gas-liquid chromatography, and single-sweep portography. Treatment technologies for the removal of RDX in wastewater include ultraviolet (UV) radiation in combi- nation with hydrogen peroxide, strongly alkaline ion ex- change resins, chemical oxidation, chemical coagula- tion with lime, activated carbon, and aerobic and anaerobic microbial degradation. ------- Empirical Formula Synonyms CAS Number Physical State Molecular Weight Melting Point Specific Gravity Solubility (at 25°C) Physical and Chemical Properties c,h6n6o6 RDX, Cyclonite, Hexogen, Cyclotrimethylenetrinitramine, Hexahydro-1,3,5- trinitro-1,3,5-triazine, sym-Trimethylenetrinitramine, 1,3,5-Trinitrohexahydro-s- triazine, T4 121-82-4 White crystalline solid 222.26 204'1°C 02N 1.816 at 20°C 2 2 In water. 7.6 mg/L. In acetone: 8.3% w/w. In nitrobenzene: 1.5% w/w. n(o2 rNvi NOc Health Effects Data and Advisory Values Genotoxicity RDX did not induce genetic effects in Salmonella typhimurium and Saccharo- myces cerevisiae assays, or in a rat dominant lethal assay. No unscheduled DNA synthesis was seen in in vitro studies with human fibroblasts. Reproductive and Developmental Effects Reduced rates of mating and fertility and decreased litter size and pup sur- vival, but no teratogenic effects, were reported in a two-generation study of Fischer 344 rats. No developmental effects were found in New Zealand rabbits below maternally toxic doses. Cancer Classification EPA Group C, possible human carcinogen, based on hepatocellular adenomas and carcinorrias in female B6C3F1 mice. Reference Dose (RfD) 0.003 mg/kg/day Drinking Water Equivalent Level (DWEL) 0.1 mg/L Health Advisory Values One-Day Ten-Day Longer-Term (child) Longer-Term (adult) Lifetime 0.1 mg/L 0.1 mg/L 0.1 mg/L 0.4 mg/L 0.002 mg/L This summary was developed using information from the Drinking Water Health Advisory. For further information contact EPA's Office of Science and Technology at (202) 260-7571. Office of Science and Technology Office of Water U.S. Environmental Protection Agency 401 M Street, SW Washington, DC 20460 june 17,1991 ------- |