Tower Chemical Company Superfund Site: Biological Assessment


TOWER CHEMICAL COMPANY
SUPERFUND SITE
BIOLOGICAL ASSESSMENT
APRIL 1994
REGION
U.S. EPA, REGION IV
ENVIRONMENTAL SERVICES DIVISION
ECOLOGICAL SUPPORT BRANCH
ATHENS, GEORGIA 30605

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REPORT:	BIOLOGICAL ASSESSMENT
TOWER CHEMICAL SUPERFUND SITE
CLERMONT, FLORIDA
March 28, 1994
INTRODUCTION
In October 1993, US EPA, Region IV, Environmental Services
Division personnel with the support of the Environmental Services
Assistance Team (ESAT), Biological Assistance Team, initiated a
study of the Tower Chemical Superfund Site near Clermont,
Florida. The purpose of this study was to conduct a biological
assessment of the surface waters associated with the Tower
Chemical Superfund Site.
The Tower Chemical Company produced pesticides at the Clermont
facility from 1957 to 1980. A variety of chemical compounds were
present at the site at some time during the company's operation
either as raw materials, registered products, or formulated
products. These compounds were introduced into the environment
primarily through effluent discharge to a holding pond (during
pesticide production) and subsequent overflow from the holding
pond during heavy rainfall events, chemical waste disposal at the
site, and abandonment of chemicals on-site after closing of the
facility. The primary chemicals of concern (COC) that have been
identified for this site are Dicofol (Kelthane), DDT and its
derivatives (DDT, DDD, DDE), and lieavy metals.
Objectives of this study were to:
•Determine the extent of environmental contamination to
the Unnamed Stream and Lake Apopka and its possible
connection to the Tower Chemical operation.
•Evaluate contaminants in Lake Apopka and identify their
potential source areas.
•Determine if site-related contaminants are accumulating
and/or concentrating in aquatic biota.
SITE DESCRIPTION
Surface waters associated with the Tower Chemical Site consist of
an unnamed stream extending from the study site to Lake Apopka,
and Lake Apopka itself (Figure 1 and Figure 2).

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2 of 21
The unnamed stream is a shallow, low-gradient, blackwater stream
about 3.2 km in length. It extends from its headwaters located
just upstream of the Tower Chemical Superfund site, along the
northern boundary of the site, and discharges into Lake Apopka
(Figures 1 and 2).
Typical stream widths range from 2-4 m, depths range from 0.25-
0.5 m, and streamflows range from 0.014-0.028 cubic meters/sec
(0.5-1 cfs). Stream sample station descriptions are presented in
Appendix A.
Lands adjacent to the unnamed stream are forested wetlands
interspersed with private rural dwellings. Near its confluence
with Lake Apopka, the stream channel becomes braided and shallow
with overbanking to a forested wetland prior to its convergence
with the lake.
Lake Apopka is a 12,500 ha surface area, hypereutrophic lake with
a mean depth of less than 2 m. Landuse surrounding the lake is
primarily muck and citrus farms and rural development. Citrus
groves are located intermittently around the lake, with the
exception of the muck farm area.
A reference stream and lake were selected from the same region as
the study stream and lake. The reference stream is tributary to
and merges with the unnamed stream just south of the Florida
turnpike. The reference lake (John's Lake) is located south of
and at a higher elevation than Lake Apopka (Figures 1 and 2).
Elevations of John's Lake and Lake Apopka are 94 and 66 feet
above sea level, respectively.
SAMPLING STRATEGY
In the field, biologists collected water and sediment samples,
measured in-situ water quality parameters, conducted Rapid
Bioassessments Protocol I, and collected plant, fish, and
alligators for tissue analyses.
The field work was conducted at six sampling stations along the
unnamed stream, at four locations within Lake Apopka, and at a
nearby stream and lake which served as a reference stream and
lake respectively (Figures 1 and 2). Sample station locations
and their numerical designations are shown in Table 1.

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3 Of 21
Beau Claire
Canal
Reference Stream
Figure 1. Sampling stations at Lake Apopka and Johns Lake, Clermont
Fl., 1993.

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Figure 2. Sampling locations along Unnamed Stream and Reference Stream, Clermont, FL.
it*
o
NJ

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Table 1. Stream and lake sample locations and their numerical designations, Tower Chemical, Clermont, Fl.
Stream Sampling Stations
Station Number
Station Location
TC-101 (background)
Background stream station, Unnamed stream, upstream of Tower discharge
TC-102
Unnamed stream downstream of Tower discharge
TC-103
Unnamed stream west of Highway 455
TC-104
Unnamed stream west of Old Highway 50
TC-105
Unnamed stream west of and adjacent to Old Highway 50
TC-106
Unnamed stream south of the Florida Turnpike
TC-108 (reference)
Reference" stream station, south of Old Highway 50 and tributary to the unnamed stream

Lake Sampling Stations
Station Number
Station Location
TC-109, 110, 111
Lake Apopka at 15, 30, and 45 meters, respectively, from mouth of unnamed stream
TC-112, 113, 114
Lake Apopka at 15, 30, and 45 meters, respectively, offshore of citrus farms
TC-115, 116, 117
Lake Apopka at 15, 30, and 45 meters, respectively, offshore of muck farms
TC-118, 119, 120 (background)
Background station, Lake Apopka at 15, 30, and 45 meters, respectively, offshore of Crown Point
TC-121 (reference)
Reference" lake station, St. John's Lake, southshore
* reference - station consisting of the best conditions attainable regionally.

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METHODS
Water Quality Measurements
Dissolved oxygen, pH, temperature, and conductivity were measured
in-situ using a calibrated Hydrolab® multi-parameter probe.
Alkalinity and hardness were determined later (within 72 hrs) in
the laboratory using EPA approved methods (APHA 1992). Water
quality data were taken at all sampling stations on the unnamed
stream, at the reference stream, at four lake sampling stations
(111, 114, 117 and 120), and at the reference lake (John's Lake).
Surface Water and Sediment Samples
Surface water and sediment samples were collected and preserved
in accordance with EPA Region IV Environmental Compliance Branch
Standard Operating Procedures (USEPA 1991). Surface water and
sediment samples were collected at all sampling stations along
the unnamed stream, at the reference stream, at four sampling
stations within Lake Apopka (111, 114, 117, and 120), and at the
reference lake (John's Lake). Additional sediment samples were
collected in Lake Apopka at stations 109, 110, 112, 113, 115,
116, 118, and 119.
Surface water and sediment samples were split in the following
manner to provide material for various chemical analyses as well
as for toxicity testing.
Water
3 - 40 ml glass bottles with teflon septum (for volatile organics)
1-1 liter polyethylene bottle (for metals)
1-4 liter amber glass jug (for pesticides and extractable organics)
1-4 liter cubitainer (for toxicity testing)
1 - 250 ml polyethylene bottle (for total organic carbon)
1 - 250 ml polyethylene bottle (for microtox)
Sediment
1-2 oz. glass jar with teflon septum (for volatile organics)
1-8 oz. glass jar (for metals)
1-8 oz. glass jar (for pesticides and extractable organics)
1 - 8 oz. glass jar (for total organic carbon)
1 - liter glass jar (for toxicity testing)
1 - whirl pack (for sediment sizing)
Chain-of-custody was maintained throughout sample collection and
testing.
Rapid Bioassessments
Rapid Bioassessments, used for detecting aquatic life impairments
and assessing their relative severity, were conducted according
to EPA Rapid Bioassessment Protocols for Use in Streams and

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Rivers (USEPA 1989). Rapid Bioassessments Protocol I (RBP I)
were performed at all sampling stations on the unnamed stream
(stations 101, 102, 103, 104, 105, and 106) and at the reference
stream (station 108). The general scope of RBP I consisted of a
Habitat Assessment and a Benthic Macroinvertebrates Survey.
Biological Sample Collection
Plant, fish, and alligators were collected for tissue analysis to
determine if site-related contaminants were accumulating and/or
concentrating in organisms on-site or downstream of the site.
Plant samples collected from each sample location were split in
two portions, one-half was wrapped in aluminum foil (for organic
analysis) and one-half wrapped in plastic (for metals analysis).
Samples were then frozen on dry ice. The emergent aquatic
macrophyte, Lizard's-tail (Saururus ceruus.), was selected as the
target species because it was the only aquatic macrophyte common
to the reference stream and almost all sampling stations on the
unnamed stream. Lizard's-tail was collected from five of the six
sampling stations on the unnamed stream (stations 101, 103, 104,
105, and 106) and from the reference stream (station 108). No
aquatic vegetation was collected from Lake Apopka or the
reference lake.
Fish were collected using a Smith-Root Type VII backpack
electroshocking unit. Stunned fish were dipped from the water
with a clean net. Fish samples for organic analysis were wrapped
in aluminum foil and fish samples for metals analysis were
wrapped in plastic. Samples were then frozen on dry ice.
Mosquitofish (Gambusia sp.) were selected as the target species
because it was common to both the unnamed stream and reference
stream as well as to Lake Apopka and the reference lake. Fish
were collected from one location on the unnamed stream (stations
104/105 combined), from the reference stream (station 108), and
from one location in Lake Apopka (near station 111). A mixed
fish sample consisting of mosquitofish and other fish species was
collected at the reference lake, John's Lake (station 121).
The University of Florida and the U.S. Fish and Wildlife Service,
Gainesville, Florida, collected one young alligator (<4 foot
total body length) from each of four sampling locations in Lake
Apopka (stations 111, 114, 117, and 120) and from a reference
lake (Orange Lake). Alligator samples were processed by the
University of Florida. Samples of liver and fat tissue from each
alligator were submitted for chemical analysis along with the
above plant and fish samples. Tissue samples were analyzed for
extractable organic compounds, pesticides/PCB compounds
(including dicofol and dichlorobenzilate), and metals.

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Toxicity Tests
Toxicity tests were conducted according the EPA Region IV
Ecological Support Branch Standard Operating Procedures (USEPA
1993). The following toxicity tests were performed on:
water samples
Ceriodaphnia 7-day Survival/Reproduction Test (SOP XV)
Lettuce Seed Root Elongation Test (SOP XIX)
Microtox® Basic Test
sediment samples
Ceriodaphnia 7-day Whole Sediment Test (SOP XV A)
Lettuce Seed Germination Test (SOP XVIII)
Microtox® Basic Test (performed on sediment pore water)
RESULTS
In-Situ Water Quality
The results of water quality measurements taken on the unnamed
stream, Lake Apopka, and corresponding reference stations are
summarized in Table 2. The pH of the water at the stream
background station 101 (4.4 pH units) is probably a naturally
occurring stream condition since low pH and low dissolved oxygen
levels are characteristic of low-gradient, blackwater streams.
Chemical Analyses of Surface Water and Sediment Samples
Results of chemical analyses of water and sediment samples are
provided in Appendix B. Surface water samples were devoid of
detectable levels of purgeable organics, extractable organics,
and pesticides. Levels of heavy metals exceeded Ambient Water
Quality Criteria (AWQC) at only one sampling station (103). Here
a zinc concentration of 210 ug/L exceeds the AWQC 24-hr average
(chronic value of 47 ug/L) but does not exceed the AWQC maximum
concentration of 320 ug/L (at a hardness of 100 mg/L as CaC03) .
At the same station a copper concentration of 30 ug/L exceeds
both the AWQC 24-hr value (5.6 ug/L) and maximum concentration
(22ug/L at a hardness of 100) for copper.
Sediment samples lacked detectable levels of purgeable and
extractable organics, however, detection levels in many instances
were not sensitive enough to meet sediment screening values. It
should be noted that sediment samples for virtually all stations
contained high levels of unidentified extractable compounds (from

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Table 2. Water quality measurements in stream and lake surface waters in the vicinity of Tower Chemical, Clermont Fl.
Sampling
Stations
In-situ stream water quality data
Temperature
(C°)
Dissolved 02
(mg/1)
PH
Conductivity
(/x mhos/cm2)
Alkalinity*
Hardness*
(mg/1 CaC03)
TC-101 (background)
23.6
1.0
4.4
410
26**
84
TC-102
22.2
4.3
6.2
242
7
33
TC-103
22.1
0.84
7.1
215
50
96
TC-104
24.3
1.78
7.22
182
26
59
TC-105
25.1
2.12
6.94
169
31
57
TC-106
26.5
2.42
6.46
470
64
220
TC-108 (reference)
24.58
3.4
7,53
262
53
108

- Sampling
Stations
In-situ lake water quality data
Temperature
(C°)
Dissolved Oz
(mg/1)
PH
Conductivity
(/x mhos/cm2)
Alkalinity*
(mg/1)
Hardness*
(mg/1 Ca C03)
TC-111
27.74
9.46
9.26
337
73
134
TC-114
28.22
7.18
9.03
365
75
136
TC-117
26.03
6.41
9.02
374
100
146
TC-120, (background)
29.58
14.25
9.51
369
100
146
TC-121 Johns Lake
(reference)
29.97
7.51
7.96
207
13
42
* Measurements performed in the laboratory.
** Alkalinity measured after pH adjusted for toxicity tests.
o
H)
to

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Table 3. Pesticide levels in stream and lake sediments in the vicinity of Tower Chemical,
Clermont Fl., October 19-21, 1993.
Sampling
Stations
Pesticides (/xg/kg)
DDT
DDE
DDD
Dicofol
Stream Stations
SD-101 (background)
5.5U
23
6.7
5.5U
SD-102
25U
1600
510
25U
SD-103
300U
1600
1100N
300U
SD-104
5.2U
20
5.2U
5.2U
SD-105
4.7U
12
4.7U
4.7U
SD-106
27U
27U
27U
27U
SD-108 (reference)
5.8U
5.8U
5.8U
5.8U
Lake Stations
Gourd Neck
SD-109
37U
37U
37U
37U
SD-110
41U
41U
41U
41U
SD-111
41U
41U
41U
41U
citrus
area
SD-112
55U
55U
55U
55U
SD-113
54U
54U
54U
54U
SD-114
65U
65U
65U
65U
muck farm
area
SD-115
47U
240n
180
47U
SD-116
23U
67
54
23U
SD-117
66U
66U
66U
66U
Crown Pt,
background
SD-118
46U
46U
46U
46U
SD-119
41U
41U
41U
41U
SD-120
37U
37U
37U
37U
SD-121 (reference)
4.3U
4.1J
4.3U
4.3U
J - analyzed for but not detected; the value shown is the US EPA Contract Laboratory Program
Practical Quantitation Limit.
J - estimated value. N - presumptive evidence of presence of material.

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11 of 21
20,000 - 200,000 ug/kg). Some samples did contain notable levels
of the pesticides DDE, DDD, and some heavy metals. The
concentration of DDE, DDD, DDT, and Dicofol in sediments is
summarized in Table 3. As seen in the table, only the more
persistent forms of DDT (ie. DDE and DDD) were present. A
gradient in DDE/DDD concentration exists on the unnamed stream
from the Tower site to Lake Apopka with the highest
concentrations being on-site (stations 102 and 103). Another
DDE/DDD gradient is evident in Lake Apopka near the muck farms
(stations 115, 116, and 117) with the highest levels of DDE/DDD
nearest the shore (station 115). No dicofol was detected in any
of the sediment samples.
Table 4 summarizes the concentrations of copper, lead, mercury,
and zinc in the sediments in the vicinity of Tower Chemical. As
with surface water samples, sediment at only one sampling
station, station 103, exceeded the effects levels set for metals
in sediments. In this case zinc was about double the ER-L
(Effects Range-Low value of 120 mg/kg) set by NOAA (Long & Morgan
1990) but still lower than the corresponding ER-M (Effects Range-
Medium value of 270 mg/kg). Copper and lead levels at 72 mg/kg
and 36 mg/kg just barely exceeded their respective ER-L's of 70
mg/kg and 35 mg/kg.
Tissue Analyses
Results of the chemical analyses of plant, fish and alligator
tissue are given in Appendix C. In addition, Table 5 lists the
concentrations of COC's in the plant, fish, and alligator tissue.
Plant tissue showed no detectable levels of pesticides.
Some heavy metals were detected in plant tissue, but they were
not substantially higher than stream background or reference
stations.
In fish samples, DDE was detected in fish tissue at the stream
station 104/105. Heavy metals (Cu, Hg, Zn) were also detected at
this station, but at levels lower than at the reference stream.
DDE was detected in the tissue of all four alligators collected
from Lake Apopka, but it was not detected in the alligator
collected from the reference lake. Heavy metals were also
detected in alligator liver and fat tissue, but detected levels
were not considerably different than samples collected from the
background or reference stations.
Rapid Bioassessments
The results of the Rapid Bioassessments (Protocol I) conducted
along the course of the unnamed stream and at the reference

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Table 4. Heavy metal concentrations in stream and lake sediments in the vicinity of Tower
Chemical, Clermont Fl., October 19-21, 1993.
Sampling
Stations
Heavy Metals (mg/kg)
Copper
Lead
Mercury
Zinc
Stream Stations
SD-101 (background)
5U
3
0.08U
9.5
SD-102
20U
2.7
0.07U
22
SD-103
72
36
0.05U
230
SD-104
3U
0,99
0.07U
12
SD-105
13
9.9
0.08U
31
SD-106
18
26
0.7U
33
SD-108 (reference)
8U
5.4
0.2U
17
Lake Stations
Gourd Neck
SD-109
9U
6.6U
0.56U
30U
SD-110
20U
6.7U
0.57U
100
SD-111
8U
6.9U
0.61U
30U
citrus
area
SD-112
16j
9.1U
0.83U
30U
SD-113
20U
20U
0.83U
40U
SD-114
18
7.9U
0.69U
30U
muck farm
area
SD-115
21
8.5
0.61U
40U
SD-116
20U
6.5
0.52U
30U
SD-117
10U
7.8U
0.67U
30U
Crown Pt.
background
SD-118
8U
7U
0.60U
30U
SD-119
14J
7.8U
20U
40U
SD-120
20U
6.8U
0.80U
40U
SD-121 (reference)
6U
2.7
0.07U
5U
J - analyzed but not detected; the value shown is the US EPA Contract Laboratory Program Practical
Quantitation Limit.
J - estimated value.

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Table 5. Pesticide and heavy metal content of plant and animal tissue collected in the vicinity
of Tower Chemical, Clermont Fl., October 19-21, 1993.
Sampling
Station
Tissue
Type
Pesticide (mg/kg)
Heavy Metals (mg/kg)
DDT
DDE
DDD
Dico-
fol
Cu
Pb
Hg
Zn
TC-101
(stream background)
Saururus
Lizard 's-tail
0.0093
U
0.0093
U
0.0093
U
2.4U
0.79
0.10U
0.02
4.7
TC-103
Saururus
0.011U
0.011U
0.011U
3.0U
1.2
0.18
0.02U
9.6
TC-104 and TC-105
Gambusia
Mosquito fish
0.022U
0.028
0.022U
5.6U
1.8
0.09U
0.07
51
Saururus
0.011U
0.011U
0.011U
2.8U
0.84
0.12
0.02U
5.1
TC-106
Saururus
0.014U
0.014U
0.014U
3.5U
0.82
0.32
0.02
5.2
TC-108
(stream reference)
Gambusia
0.013U
0.013U
0.013U
3.4U
2.5
0.09U
0.12
68
Saururus
0.014U
0.014U
0.014U
3.7U
0.36
0.26
0.2U
3.6
TC-111
(lake at mouth of
unnamed stream)
Gambusia
0.029U
0.029U
0.029U
7.6U
1.8
0.09U
0.07J
35
Liver
Alligator
Fat
0.017U
0.084
0.017U
4.5U
11
0.10U
0.07
26
0.012U
4.7
0.012U
32U
0.41
U
0.21U
0.02
2.8
TC-114
(lake, offshore
of citrus farms)
Liver
Alligator
Fat
0.018U
0.17
0.018U
4.7U
26
0.1 OU
0.15
23
0.11U
0.11U
0.11U
15U
0.5U
0.25U
0.02U
2.4
TC-117
(lake, offshore
of muck farms)
Liver
Alligator
Fat
0.022U
0.19
0.022U
2.8U
16
0.09U
0.23
22
2.2U
8.5
0.85U
27U
0.68
U
0.34U
0.03
5.0
TC-120
(lake, background
NE of Crown Pt)
Liver
Alligator
Fat
0.040U
0.013
0.040U
5.2U
30
0.09U
0.17
27
0.16U
1.6
0.16U
41U
0.71
U
0.35U
0.02U
4.6
TC-121
(Johns Lake,
reference)
Mixed Fish
Species
0.015U
0.015U
0.015U
4.0U
1.5
0.09U
0.07
55
Orange Lake
(reference)
Liver
Alligator
Fat
0.014U
0.014U
0.014U
3.6U
22
0.08U
0.95
24
0.054U
0.047U
0.054U
14U
0.38
U
0.20U
0.04
3.7
J - analyzed for but not detected; the value shown is the US EPA Contract Laboratory Program
Practical Qyantitation Limit.
J - estimated value.

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Table 6. Results of the Habitat Assessment Evaluation of streams in the vicinity of Tower
Chemical, Clermont Fl., October 19-21, 1993.
Sampling
Stations
Habitat Assessment Evaluation
Score
% comparability to
background
% comparability to
reference
Comparability Assessment
Background
Reference
TC-101
(background)
63
100%
89%
comparable
comparable
TC-102
68
92%
96%
comparable
comparable
TC-103
64
98%
90%
comparable
comparable
TC-104
63
100%
89%
comparable
comparable
TC-105
63
100%
89%
comparable
comparable
TC-106
51
81%
72%
supporting
partially
supporting
TC-108 (reference)
71
89%
100%
comparable
comparable

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Table 7. Macrobenthos qualitative sample list for seven stream sampling stations in the vicinity
of Tower Chemical, Clermont Fl., October 19-21, 1993.
Relative Abundance:	R = rare (< 3)	C = Common (3 -9)
A = Abundant (> 10) D = Dominant (> 50)
TAXON
TC-101
TC-102
TC-103
TC-104
TC-105
TC-106
TC-107
Porifera







Hydro zoa







Platyhelmenthes







Tubellaria







Hirundinia






R
Oligochaeta







Isopoda

C



C
R
Amphipoda

C

R
R


Decapoda
R
R
R
A
D


Gastropoda




R


Bivalvia
R


R
C

C
Anisoptera
A
C

C
C
R
C
Zygoptera


R


R
C
Hemiptera
R



c
R

Coleoptera
C
C
R
R
c
A
R
Lepidoptera




R


Sialidae







Corydalidae







Tipulidae







Empididae







Simuliidae







Tabanidae
R






Culicidae
R
R


R
A
R
Chironomidae
C
R

C
C
C

Plccoptera







Ephemeraoptera







Tricoptera







other
FROGS
FROGS

FROGS
SPIDER

Ptychop-
teridae
The shaded area represents pollution sensitive organisms typically found in good quality water.

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16 of 21
stream are summarized in Tables 6 and 7. Copies of the original
field data sheets are included in Appendix A of this report.
As seen in Table 6, the habitat at all but one station on the
unnamed stream was "comparable" -with the stream background
station (101) and reference station (108). In general all
stations scored relatively low due to the lack of true stream
structure such as gravel bottoms and riffle/run areas. Station
106 scored the lowest and was assigned a "supporting status" due
to the lack of water flow at the time of this study. By
comparison, water flow at all other stations on the unnamed
stream was slow but at least detectable. The low flow apparently
was the result of a lack of rain. The reference stream received
a slightly higher score because its flow was noticeably greater.
The reference stream appeared to be in part spring-fed.
Table 7 summarizes the results of Benthic Macroinvertebrate
Surveys conducted on the unnamed stream and reference stream.
The biotic assemblages displayed in the table are characteristic
of backwater or pond communities. Stream organisms such as
mayflies (Ephemeroptera), Stoneflies (Plecoptera), and
Caddisflies (Tricoptera) were absent from all stations. The
extremely low oxygen level (0.84 mg/L) at station 103 may account
for the scarcity of aquatic life observed at this station.
Toxicity Tests
The results of toxicity tests performed on surface water samples
and sediment samples are summarized in Tables 8 and 9
respectively. Copies of laboratory bench sheets for each test
are also included in this report as Appendix D. Test results for
each water and sediment sample were statistically compared to the
test results of their respective stream or lake background
station. Shaded boxes within Tables 8 & 9 indicate that the
value in the box is significantly different from its
corresponding background value.
As seen in Table 8, surface water at only one station (114)
produced a test value (for Ceriodaphnia reproduction)
significantly different from the background (station 120).
However, this slight depression in the number of young produced
at station 114 is probably not related the presence of toxic
materials. Chemical analyses failed to reveal any substances in
potentially toxic concentrations in the water from this station.
However, lower detection limits for water samples may have
revealed the presence of other toxins that were not revealed by
this study. Overall, water samples for the unnamed stream as
well as Lake Apopka appear to be non-toxic.
Table 9 summarizes the results for toxicity tests conducted on
sediment samples. As seen in the table several test values are

-------
17 of 21
Table 8. Summary of results of toxicity tests on surface water samples collected near Tower
Chemical, Clermont, Fl. September 1993.
Sample
ID H
Sampling
Location
Ceriodaphania
7 day Chronic
Lettuce Seed
Root Elongation
Average length in
cm
Microtox
LC501
Adult
Survival
Average
if Young
SW-101
Unamed Stream
(background)
1.0
24.4
40.1
>100
SW-102
on-site downstream of
previous Tower discharge
1.0
24.8
41.0
>100
SW-103
west of Hwy 455
1.0
20.9
30.6
>100
SW-104
west of Old Hwy 50
1.0
25.9
43.6
>100
SW-105
adjacent to Old Hwy 50
1.0
23.8
45.3
>100
SW-106
south of Florida Turnpike
1.0
26.1
43.1
>100
SW-108
reference stream
(south of Old Hwy 50)
1.0
26.2
33.1
>100
SW-111
Lake Apopka
(Gourd Neck)
1.0
16.5
35.1
>100
SW-114
Lake Apopka
(citrus area)
1.0
14.2
34.8
98.9
SW-117
Lake Apopka
(muck farm area)
1.0
18.7
22.4
>100
SW-120
Lake Apopka (Crown Pt.)
(background)
1.0
18.1
30.0
>100
SW-121
Johns Lake
(reference)
1.0
21.2
36.1
>100
A shaded box indicates a value significantly different from the value of its corresponding background.

-------
18 of 21
Table 9. Summary of results of toxicity tests on sediment samples collected near Tower
Chemical, Clermont, Fl. September 1993.
Sample
ID#
Sampling
Location
Ceriodaphania
7 day Chronic1
Lettuce Seed
Germination
(% germination)
Microtox
LC502
Adult
Survival
Average
# Young
SD-101
Unnamed Stream
(background)
1.00
20.8
77
>100
SD-102
on-site downstream of
previous Tower discharge
1.00
20.0
10
>100
SD-103
west of Hwy 455
0.30
12.7
0
>100
SD-104
west of Old Hwy 50
0.90
26.7
97
>100
SD-105
adjacent to Old Hwy 50
0.90
24.9
70
>100
SD-106
south of Florida Turnpike
1.00
15.5
30
>100
SD-108
reference stream
(south of Old Hwy 50)
0.90
18.1
NT
>100
SD-111
Lake Apopka
(Gourd Neck)
0.90
15.3
0
>100
SD-114
Lake Apopka
(citrus area)
1.00
18.7
7
>100
SD-117
Lake Apopka
(muck farm area)
1.00
20.0
90
>100
SD-120
Lake Apopka (Crown Pt.)
(background)
0.80
16.8
0
>100
SD-121
Johns Lake
(reference lake)
1.00
22.9
97
>100
- test completed in 6 days.
2 - LCSO values calculated from 5 minute readings.
NT - not tested.
A shaded box indicates a value significantly different from the value of its corresponding background.

-------
19 of 21
significantly different from their corresponding background
values. However, as with the above tests on surface water, a
significant difference may not always indicate toxicity. In this
case, the lack of seed germination may be attributed to physical
properties of the sediment. In the course of conducting numerous
seed germination tests, an inverse relationship has been observed
between organic content of the sediment and germination. In
"mucky" sediments of high organic content germination is poor.
This seems to be true for the sediments of lake stations 111,
114, and 120 and the sediment at stream stations 103 and 106.
Total organic carbon (TOC) content of these sediments range from
480,000 to 690,000 mg/kg (see data in Appendix B). Although
station 117 has a high organic content (540,000 mg/kg TOC), seed
germination was not inhibited. This is probably because organic
carbon at this station is primarily peat and not muck.
For stations 102 and 103 (on-site stations), elevated levels of
pesticides and/or heavy metals (Tables 3 and 4) may account for
the poor seed germination, especially in sediment from station
103 which contained elevated levels of copper and lead as well as
zinc.
Whole sediment toxicity tests with Ceriodaphnia show a decrease
in the number of young produced for stations 103 and 106 when
compared to the background station (Table 9). However, 80%
survival of adults and 15 or more young produced per adult
typically indicates a lack of toxicity. For station 106, the
number of young produced (15.5) and the lack of evidence of toxic
substances in the sediment (Table 3) suggest no potential toxic
effect. For station 103, the decrease in reproduction coupled
with a considerable decrease in adult survival and the existence
of toxic substances in the sediment clearly does indicate a toxic
effect. Heavy metals rather than pesticide seem to be the source
of toxicity. The DDE level of station 103 is matched by the
level at station 102. Yet, no toxic effects were observed in
Ceriodaphnia exposed to sediment from station 102. Sediment from
station 102 lacks the elevated levels of heavy metals found in
the sediment at station 103.
CONCLUSIONS
Based on this study, one portion of the aquatic ecosystem
associated with Tower Chemical and Lake Apopka appears to be
impacted by chemicals of concern derived from the Tower Chemical
site. The affected portion of the ecosystem is on-site in the
vicinity of station 103 on the unnamed stream. At this station
sediment was toxic to Ceriodaphnia dubia and inhibited lettuce
seed germination. The toxicity was restricted to the sediment.
Surface water at this station was not toxic to test organisms.
The scarcity of aquatic life (macrobenthos) observed at this

-------
20 Of 21
station (Table 7) may be the result of low dissolved oxygen
levels rather than toxic chemicals in the sediment.
Chemistry data shows a gradient for site-derived contaminants in
sediments extending from Tower Chemical to Lake Apopka with the
highest concentration of chemicals at station 103. At station
103 the DDE concentration, for example, was 1600 ppb.
Approximately 2500 ft. downstream the DDE level at station 105
dropped to 20 ppb. At station 106 the level was 12 ppb. This
information indicates that the wetlands through which the unnamed
stream flows is effectively sequestering both heavy metals and
pesticides. In addition, the three highways that cross the
unnamed stream appear to further impede the movement of site-
derived chemicals toward the lake. Field reconnaissance revealed
that the Florida Turnpike, in particular, serves as a barrier to
surface water flow during all but the wettest times of the year,
impounding water over many acres of wetlands before water levels
are high enough to spill through the culvert under the turnpike
and flow on to Lake Apopka.
The impact of site-derived contaminants on Lake Apopka is
difficult to ascertain. Detection limits for metals and
pesticides in water and for metals in sediment were adequate, but
detection limits for pesticides in sediments were not low enough
to detect toxic levels of some of these chemicals in the low ppb
range. For example, the published ER-L (Effects Range-Low) for
DDE in sediment (Long and Morgan 1990) is 2 ug/kg. At station
111, where the unnamed stream enters Lake Apopka, the lower
detection limit for DDE was 41 ug/kg.
Surficial sediment chemistry data (Table 3), used to identify
other potential source areas of contaminants to Lake Apopka,
reveals that DDE concentrations are as much as 4 to 5 times
higher offshore of the muck farms (stations 115, 116, and 117)
than at other areas of the lake. Tissue analysis of alligators
captured from the muck farm area also show the highest
concentration of DDE. These facts, coupled with the activities
of the intervening wetlands (between Tower Chemical and Lake
Apopka) and the existence of man made barriers (roadways) suggest
that the contribution Tower Chemical makes to the chemical load
(via surface water contributions) in Lake Apopka at this time is
limited. As long as the wetlands remain undisturbed and the
impact of remedial activities are restricted to the immediate
site, the idle Tower Chemical site probably poses less of an
ongoing threat to the ecology of Lake Apopka and the intervening
wetlands than do the continuing muck and citrus farming
activities.

-------
21 of 21
REFERENCES
APHA. 1992. Standard Methods for the Examination of Water and
Wastewater, 18th Edition. Greenberg, A.E., L.S. Clesceri,
and A. D, Eaton, eds. American Public Health Association,
American Water Works Association, and Water Pollution
Control Federation. 1015 Fifteenth Street, N.W.,
Washington, D.C. 20005.
Long, E.R. and L.G. Morgan. 1990. The potential for biological
effects of sediment-sorbed contaminants tested in the
National Status and Trends Program. NOAA Tech. Memo. NOS
OMA 52. U.S. National Oceanic and Atmospheric
Administration, Seattle, WA.
USEPA. 1993. Region IV Ecological Support Branch Standard
Operating Procedures for Hazardous Waste Site
Investigations. Prepared for U. S. Environmental Protection
Agency, Region IV Environmental Services Division, Athens,
GA, and prepared by ManTech Environmental Technology, Inc.,
Environmental Services Assistance Team, Athens, GA.
USEPA. 1991. Environmental Compliance Branch Standard Operating
Procedures and Quality Assurance Manual. U. S.
Environmental Protection Agency, Region IV, Environmental
Services Division, College Station Road, Athens, GA 30613.
USEPA. 1990. Laboratory Operations and Quality Control Manual,
U.S. Environmental Protection Agency, Analytical Support
Branch, Environmental Services Division, Region IV, Athens,
GA. 30605.
USEPA. 1989. Rapid Bioassessment Protocols for Use in Streams
and Rivers. U.S. Environmental Protection Agency,
Assessment and Watershed Protection Division. 401 M Street,
S.W., Washington, D.C. 20005.

-------
APPENDIX A
Field Data Sheets for Rapid Bioassessment (Protocol I)

-------
MTfllCAL CSAAACTSaZtATXOr
riXLO DATA i«l
QUALITY
n{?j
rtnzcu omatitunoi
iffMtJLi iQBi/firnuf fiAmti .
twdmmifmmt	Uld 9««l
ri*14/faat«r«	jricalt»r«l -
lu?7
Jxxz
itdr«ck
t •« 1 «!• r
C*b61•
Qltvtl
I«a4
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CUT
» n<-M (I • la.I
(3.S-K0 (ft.)
l-H-mm |«.1-2.1 l«. I
htutri
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I.MI-m <«Ucfct
ftCCIBl
C«ap«aHl**
I» l>»gll»^ W
<3 ay-
¦Loy.
Tt?•
tie
Rarl
lUckt, v««d,
C*«r«« 7 I •• t
Nit«rlali |Ch)il)
•lack, ftcf rli*
o r f•«1c C rion I
4 f mj, fl«11
fr«fa«a(i
r«ic*a(
a,oK
/O
~7 J ^ C
J'O
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		//-O	^
OSf ((VATIOM* * BO/OB HITCH

-------
HABITAT ABBBSSHIHT HILD DATA EHIIT
V>~a. K-ftUM.iL
Naae of Water Body
Data . Inveetigator
Coaaente	
Station l.
161

		L&JL
eLVrvr-*
v/v^ Lo " I d^A>-Z3i
KKol^.'^o V>—^ ! (A**
g-w- J JL i c^t 	
i 60* rubble,gravel,


10-30* rubble,gravel
<10* rubble,gra'
rel
8UBSTRATI/
1 aubaerged loga,
or other etabla

or other atable
or other atabla
AVAILABLE
undarout banka.or
habitat.

habitat. Habitat
habitat. Lack
of •
COVSR
other atabla habitat
Adequate habitat
,
availability <
habitat la ebvloue.&i




deelrable.
5~


18-20
11-
15
8-10
0-5
2. SHBIDDID-
Oravel.cobble, and
Oravel.cobble, a
nd
Oraval
75*

aurrounded br fine
aurrounded br fine
aurrounded by fine
aurrounded by
fine

aadlaant.
aedlaent.

aedlaent.
aedlaent.


16-20
11-
16
6-10
o
0-5
i '•»*»
3. 5 cr6
Coldi > 2 cfa
1-2 cfa
0.6-1 cfa
0.5 cfa


Marat >6 cfa
2-6 cfa
1-2 cfa
1 cfa


10-20
11-16
6-10

0-5
OR





>6 crs
Slow (<0.3 a/a),deep
3 of 4 habltata
2 of 4 habltata
Doalnated by
on«

(>0.5a);a low,ahalloa
preaent. (Hlealrvg
praaant. (Hlaalng
velocity/depth

I <0.5a))faati>0.3a/e)
rlfflaa or rune
riff lee/rune gat
category (uaually

deepi faat.ahallov
gat lover acore than
loaar acore.)
pool).


habltata all preaant
aleeing poola).

2-


18-20
11-16
8-10
0-5
4. CHAHHIL
ALTIRATIOH
Little / no enlarge- Boaa nea lnoraaaa in
• ant of lalande or bar ioraatlon.aoetly
point bar*¦ and/or
no channeliaatlon
12-15
froo eoaree iratili
and/or aoaa channal-
iaatlon preeent.
e-u
Moderate dapoaltlon
of nea gravel,coaree
aand on old and naw
bereipoole partially
filled a/a litiand/or
eabankaenta on both
banka.
4-T
Heavy dapoalta of
fine aaterlal, bar
developaent Increase
Host poola filled w/
allt;and/or eztenalve
channelization.

0-3
S. BOTTOM
8C0UF1H0
AHD
DIP0BITI0H
J* ofbottoa
•ffactad.
12-16
6-30* affeoted.Boour
at oonatrlctlona and
ateep gradte. Boaa
dapoaltlon In poola.
B* 11
30-60* affaotad.
Dapoalt and acour at
obatruotlone¦ benda,
and cooatrlotlona.
>50* bottoa chancing
naarlr Tear long.
Poola abaaot due to
dapoaltlon. Only
Boaa filling of poola large rocka aipoaed.
4-T
0-3
8. DUN/BIRD, 6-T. Tarlety of
POOt/RiriLI > hibltat.Deep rlfflaa
RATIO*"	and poola.
12-16
T-16. Adequate depth
In poola and rlfflaa
Banda provide habitat provide aoaa habitat
16-25. Occaaalonal >25. laaantlally a
riffle or band.Bottoa atralght atraaa. flat
8-11
4-T
water or ahallo*
Poor habitat.
-& 0-3
. BAH*
STABILITY
Stabla. Mo aroalon
or teat failure.Blda
alopaa <30*.

B-10
Moderately atabla
Infrequent aroalon
•oatly healed over.
Bide alopaa to 40*.
B-e
Hodaratalr unatable.	Vnatabla. Many eroded
Hodarata aroaloo and	araaa. Blda alopaa
alda alopaa to 60*.	>60*. "Haa* araaa
High aroalon during	frequent on atralght
blah tloa.	and bandf.
3-5	0r2
8. BAHK >80* of atraaabank	50-TB* covered br	25-4B* covered br <25* covarad br
VI08TATIYI covarad br vegetation	vegetation, gravel or	vegetation, gravel or vegetation. gravel or
STABILITY or bouldara and	larger aaterlal.	larger aaterlal. largar aaterlal.
cobbli. .
•-10	8-8	3-6 0-2
V-
T
9. STRIAMSIDK Doa
COVBB
Doa
la ahrub
la of tree for*.
e-e
Doalnant vagatatlon
la graae or forbee.
3-5
>50* no vegetation
Doalnant aaterlal la
aoll.rock, bridge
oeterlale.culverta.or
¦lna talllnga.
0-2
COLUHH TOTALS
SCORI
1
CI

-------
Rapid Bloassessment Protocol
Bloaurvey Field Data Sheet
(.4 C	I 0 (
RELATIVE ABUNDANCE OF AQUATIC BIOTA
Perlphyton	0 12 3	4
Filamentous Algte 0 12 3	4
Macrophytea	0 12 3	4
8llmes	0
Macrolnvertebrstes 0
Fl«h	0
3 4
3 4
3 4
0-Absent/Not Observed
1 - Rare
2 - Common
3 - Abundsnt
4 » Dominant
MACROBENTHOS QUALITATIVE SAMPLE LIST(lndlcali Rtlidr* Abundtnct R - Ran, C • Common, A • Abundant, 0 - Domlrunl)
Porifera
Anlsoptsra
Chlronomldae Q.
Hydrozoa
Zyjfoptera
Plecoptsra
Platyhelmlnthea
Hemlptera 1^
Ephemeroptera
lUrbellerla
Coleoptera C
THchoptere
Hlrudlnea
Lapldoplara
Other
Ollgochaeta
SleUdae
C
leopoda
Corydalldse
J
Amphlpoda
Tlpulldae

Oecapoda ft.
Empldldee

Gastropoda
Slmullldae

Blvalvla ^
Tsbanldae /C


Culkldae

Rare <3	Common 3-9	Abundant >10	Dominant >50 (Estimate)
Observetlona
Figure 6.VI. Bioiuivey Field Data Sheet lor uia with Rapid Bioamnment Protocol I.

-------
rintcii auaACTcassATlo*/
rxtu MM iiin

Tu
tec. 2_
ntiiui, cuucrtuunoi
»»mu nn/mnim mtwrn
fiiISI-u fit U.|
ll-ISI-M (l.S-lt U.I
)-44-m ll.t-l.S *¦. >_
|«(UtTl~
tt-mm '
«.*M-aa |alJ«k|
rafCMl
CaafttitlM
ta laatllaa lua

?*Z
toy<
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furl
RlMtUll ICrOH)
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£of-

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MOT 041

-------
HABITAT A6SIESHIHT P1ELD DATA SHUT

Naaa of Kttir Body_	Station * f P -		l C cJ2
Data , Invaatlgator	}"V\ k~ ^	v > *-$ ri-it
CATEGORIES
HABITAT
PARAMETER
IXCELLEKT
GOOD
PAIR
POOR
1. BOTTOM
>60* rubbla.(ravalt
30-50* rubble,gravel
10-30* rubbla,gravel
<10* rubbla .(ratal
SUBSTRATE/
aubaaraad lot*.
or othar *tabl*
or othar atabl*
or othar atabla
AVAILABLE
undarout banka,or
habitat.
habitat. Habitat
habitat. Lack of
COVER
othar atabla habitat
Adequate habitat.
availability <
habitat la obvloua.l


daalrabla.


10-20
11-15
6-10
O 0-5
2. EMBEDDED-
Qravel.oobble, and
Oravel.oobbla, and
Oraral.oobbla. and
Oraval.eobbla, and
NESS
bouldar ara <26*
bouldar ara 25-60*
bouldar ara 50-76*
bouldar ara >75*

aurroundad br fine
aurroundad br Una
aurroundad by flna
aurroundad by flna

•adlaant.
••dlaant.
aadlaant.
aadlaant.

16-20
11-16
6-10
o °-5
lOt
3. «* 6 crs
OR
>6 crs
Cold| > 2 cf*
Marei >6 of*
10-20
Slow (<0.3.a/a).daap
(>0.6a)j*lon,*h*lloa
(<0.6a)lf**t(>0.3a/a)
daapi faat,*halloa
kibltiti'ili pr***nt
IS-20
1-2	eta
2-6	cf*
11-16
3 of 4 habitat*
praaaot. (Mlaalna
rlfflaa or runa
¦at loaar aoora than
ilaalni pooli).
11-16
0.6-1 efa
1-2 efa
6-10
2 of 4 habltata
praaant. (Hlaalna
rlfflaa/runa vat
loaar aoora.)
0.5 efa
1 efa
0-5
Doalnatad by ona
valoclty/dapth
eatagorr (uaually
pool).
6-10	^ 0-5
4. CHANNEL
ALTERATION
Llttla/.no aniarga-
aant ot'liludi or
point bar*i and/or
no eha'nn*lliatlon
/	12-16
Ida* no* lcoraaaa'ln Hodarata dapoaltlon
bar.formation.aoctlyrof Baa araral.coara*
frea ooaraa aravalt aand on old and naa
and/or aoaa ehannal- baraipoola partlallr
laatlon praaant. flllad a/alltiand/or
•abankaanta on both
banka.
- 6-11	4-T
Haavy dapoalta of
tin* aatarlal, bar
dovalopaant lneraaaa
Hoat poola flllad ¦/
allt|and/or axtanalva
ehannalliatlon.
,€T
0-3
6?»BOTTOM
SCOOR1NO
ADD
DirOBITION
«6* of bottoa
)affaetad.
IC
12-16
6-30X affaotad.Boour
at eonatrletlona and
ataap aradaa.-Soaa
dapoaltlon In poola.
6-11
30-60X affaotad.
Dapoalt and acour-at
obstruction*, banda.
and eoattrletlona.
>50* bottoa ebanging
naarlr raar lone.
Fool* abaaat dua to
dapoaltlon. Only
Bom tilling of poola laraa rocka axpoaad.
4-T	0-3
6. RUN/BIND
POOL/RIPPLI
RATIO**
6-T. Variety of
hAbltat.D**p rlfflaa
and poola.
12-16
T-16. Adaquata dapth 16-25. Oeoa**lon*l >25. K**«atlallr *
In pool* and rltfl** rlffla or band.Bottoa atralaht atraaa. flat
Band* prorlda habitat provide aoaa habitat watar or (hallo*
Poor habitat.
6-11	4-T	3>" 0*3
T. BAKU
STABILITY
Stable. Ho arosloo
•r talk fallura.Blda
•lopa* OOX.
1
•-10
Hodaratalr atabl*
Infraquant aroalon
aoatly haalad ov*r.
Side alopa* to 40X.
6-6
Mod*ratalr unatabla.	Onatabla. Many arodad
Hod*rata aroalon and	araaa. Blda alopaa
alda alopaa to 60S.	>101. *Raa~ araaa
Hlah aroaloo during	frequent on atralaht
blah flo*.	and band*.
3-6	0-2
6. BANK
VE0ETATIVE
STABILITY
>10* of atraaabanh
eovarad by vagatatlon
or.boulder* and
eobblaa.
to
60-T9X eovarad br 25-46X covered br	<25* eov*r*d br
vegetation, gravel or vagetatloa, gravel or veaetatlon, aravel oi
larger aatarlal.	laraar aatarlal.	laraar.aatarlal.
6-6
9-6
0-2
>. STRIAH8I0I Doalnant vagatatlon
COVBR	la ahrub
Doali
tlon Doa
a
i
• -10
"2C
6-6
3-5
>60* no vegetation
Poaloant aatarlal la
eoll.rock, brldaa
¦aterlala.culverta.oi
alna tailing*.
0-2
COLUMN TOTALS
SCORE
/•2-

-------
Rapid Bloassessment Protocol I
Bloeurvey Field DaU Shoot

RELATIVE ABUNDANCE OF AQUATIC BIOTA
Parlphylon	0 12 3	4
Filamentous Algaa 0 12 9	4
Macrophytss	0 12 3	4
8llm*t	0 1 2 .3 4
MacrolnvarUbral** 0 12 3 4
Flah	0 12 3 4
6*Absant/Not Obaarved
1 ¦ Rara
2 ¦ Common
3 - Abundint
4 ¦ Dominant
MACROBENTHOS QUALITATIVE SAMPLE LIST(tndlc«U Rilibn Abun4tnc« R •Rar«l C> Common, A-Abundint, D 'Dominant)
Porlfara
AnlaopUra £
Chlronomldt* [Z
Hydro zoa
Zygoplcra
Plaeoptara
PlatyhalmlnlhM
Hamlptara
Ephamaroplara
lUitMiiarla
Ccltopltra £
IVIehoptara
Hinidlnaa*
Lapldoptara
Othar
3llgochasla

8lalldas

laopooa C.

Corydalldaa

Amphlpoda C
Tlpulldaa
-On	i.
Dacapoda ^. . v.
Empldldaa
rCK. <»<».¦, [10
Dominant >60 (Estlmala)
Obaarvatlons


Figure 6.1-1. Bioiurvay Fiald Dau Shaat for uia with Rapid Bioatiaumant Protocol I.
A-7

-------
nntcu ouiAaittuttoi
rnu tmni
OOAttTT
T"«	I 0J-

iiiuiu	ntmn
li«4tilnit *arraaa4Ia« UM B»«
Mat4/ra*tara	tiilnUim
Laatl nt((ik«il (raalaat	N«4(iii>
Lacal *it
Caa
•ratal
Otkat
iu«r
CiMtr Civti r Ofta
HDimw/winiMti
ItOlill MKIt
Ii4Ih«I 011*1
« IilUitU.IUaii.Mfllil ll((la
fa'laellt *"0
Baa
Daa Vfaaaatl Taa
" ^
-h--* 10 "L
Ckaalcat
Otkar
*•>4
-2U*
laliad
¦aa!4ar
Cakkta
aiatal
Ha<
ititr>t» Trf
tic
u
Vl»
>t)<-u III I	-fl	^
««-)»«-aa II.3-1* la.I	.
l-il-ia !•.I-l.S la.|
I.ll-I.ll'aa Ifdttrl
««-aa
«.«««-*• latlckl

rltUla, k««4(
(••ra« PUat
icrom
•!•€*~ ~•ry r
orftalc irrom
*"• cbl4	Opaque	lfal lac Caiar ~fcV_

*-vs.K«M< , . %t>° F

-------

C\^~
HAB1TAT.A6SEESHINT FIELD DATA SHUT
Maea ot Hater Body U*\ Ko ^	U
Station •.
ro3
Data JQ/rtm
Ca"«H«	» V/ >>l l»U	^UvJ .	• rt/1 »v-1 Lt^- lX\Q~-» <~j£.
_ Inveatlgator
*1"^^ WleU-rwl«»0	1.1 ouKy^ atffL
J-© W*.
70^
V>.»-

HABITAT
PARAMETER
CATBQ0RIE8

EXCELLENT
0000
iair
POOR
1. BOTTOM
SUBSTRATE/
AVAILABLE
COVER
>40* rubble,gravel,
aubaarged loga,
undercut banka.or
ethar atabla habitat
18-20
90-80K rubble.graval
or ethar atabla
' habitat.
Adequate habitat.
11-15
10-30* rubble,gravel
or ethar atabla
habitat. Habitat
availability <
daalrable.
6-10
<10* rubble.graval
or othar atabla
habitat. Lack of, j *
habitat la obTloue
S~ 0-5
2. EMBEDDED-
HISS
Oravel.cobbla, and
boulder ara <35*
aurroundad by Una
aadlaant.
18-20
Qraral,cobble. and
bouldar ara 26-50*
aurroundad by fin*
eediaent.
11-16
Oravel(oobble. and
bouldar ara 50-76*
aurroundad by fine
aadlaant.
8-10
Gravel.eobbla, and
bouldar ara >75*
aurroundad by fine
aadlaant.
	
3. ta & ere
OR
>6 CIS
Cold) > 2 eta
Hare) >6 cla
10-20
Sloe |<0.3 a/a)•deep
(>0.5a) ialoM|'ahallo»
t<0.5»)|feet(>0.3a/a)
•deepi taet.ehalloa
habltata all preaent
18-20
1-2	eta
2-6	ela
11-16
3 of 4 habltata
preaent. (Mleelng
t rlfflae or runa
¦at lover aeora thai
¦leelng pool*).
11-18
0.5-1 eta
1-2 ela
€-10
2 of 4 habltata
preaent.' (Mlaalng
rifflee/rune get
lo»ar aeora.)
• -10
0.5 efa
1 efa
0-5
Doelnated by ona
reloclty/depth
cataforr (uaually
Pool).
"2	 0-5
4."CHAHHEL
ALTERATION
Llttla / no enlarge-
ment el lelande or
point bara, and/or
-no ohennellaatlon

12-18
Bone no* lneraaaa In
bar formation.aoatly
froa ooaraa gravel)
•nd/'or aoaa ebannel-
itation prea*nt.
1-11.
Moderate depoaltion
of sa* trafel.coarae
aand on old and new
beraipoole partially
fillad «/alltiend/or
eabenkeente on both
banke.
4-7
Heavy dapoalta of
flna Material. bar
developaent lneraaaa
Heat poola fillad «/
allttand/or eateneiva
channaliiatlon.

0-3
(BOTTOM
8C00RIH0
AND
DEP0S1T10H
15* ofbottoe
affaatad.
IS"
8-30* 'effeot*d.8oour
at oonetrletlone and
ateep trade*. Boaa
deposition In pools
•-11
30-80* affaatad.
Dapoalt and aeour at
obstruotlons, bend*,
and eonatrlotlona.
>80* bottom changing
nearly year,long.
Poola abaant dua to
depoeltlo'n. Only
iBom filling of poola, large rocka aspeaad.
4-7
0-3
•. RUH/BERD
POOL/R1IILI
RATIO**
b-t• Variety of
hibltat.Deep rlfflae
•nd poola.
12-18
T-15. idequate depth 1 15-25. Oooaaalonal >25. Kaaantlally a
in pooie and rlfflae 1 riffle or band.Bottom atralght etreaa. Plat
Banda provide habitat'provide aoaa habitat
•-11 I
4-T
eater or eballoe
Poor habitat.
c> •-*
7.TBAHR
STABILITY
Stable. • Mo ores ion •<
or bask iallure.Blda
alop*a <30*.
t'o
•-10
Moderstely stable
.Infrequent eroalon
»oatly healed over.
Side slopes to 401.
e-i
'Moderately unstable.	Oneteble. Many eroded
.Moderate eroalon and areaa. 8Ida alopaa
side alopea to ®0*. >80*. "Ran" sreae
;Hlgh eroeles during	frequent on atralght
high floe. and benda.
3-5	0-2
•. BAKU	>>0* of etreaebank 50-79* covered by 25-49* covered by	<25* covered by
VE0ETATIYE covered by vegetation vegetation, gravel er vegetation, graval or vegetation, gravel or
STABILITY or bouldere and	larger Material.	larger eatarlal.	larger Material,
eobblee.
JQ »-10	0-8	3-5	0-2
9. STREAH6IDI Doa
C0VIB
la ehrub
la of traa for*.
to
• -10
6-8
Doalnant vagatatlon
la graaa or forbee.
3-5
>50* no vegetation
Doalnant eatarlal la
•oil,rock, bridge
aatarlala.culverta.or
¦in* tallinga.
0-2
COLUMK TOTALS
SCORE
iJL

-------
Rapid Bloassessment Protocol I
Bloaurvey Field Data Sheet
G/C-n^vV L
lt)Crv.k«*\ 103
|D//t/l3
RELATIVE ABUNDANCE OF AQUATIC BIOTA
Perlphyton	0 12 3	4
Fllamenloua Algae 0 12 3	4
Macrophytea	0 1 2 3	4
8llmaa	0 12 3 4
Macrolnverlabrataa 0 12 3 4
Flah	0 12 3 4
OvAbaant/Not Obaarvad
1 -Rare
2 - Common
3 - Abundant
4 * Dominant
MACROBENTHOS QUALITATIVE SAMPLE LISTpndlctU RtUtfv* Abundant* n • Ran, C - Common, A •Abundant, D « Dominant)
Porlfara
Anlaoptera
Chlronomldae
Hydrozoa
Zyeoptera (\ Sh><		
(PlicopUra
PlatyhelmtnthM
Hemlptera
Ephemeroptera
TUrballarla
Coteoptera (v'i^
Dlchoptera
Hlrudinaa
Lepldoplera
Olhtr i
Ollgochaata
Slalldae
6«* *—> ^aU»« a,
leopoda
Corydalldae

Ampnipooa
Tlpulldae

Decapoda (_ 1 )
Empldldae

Gaitropoda
Slmullldae

Blvalvla
Tabanldaa


Cullcldaa

Rare <3 Common 3-
9 Abundant >10
Dominant>80 (Eatlmata)
Obiarvatlona
S	O1^1 Lour--
c^rJWimwi	roK~it£>La \
ue&~ g^—^\	u-Zvjx^ts. )
Figure 6.1-1: Bioiurvey Field Data Sheet (or u*e with Rapid Bioaiienment Protocol I.
A-7

-------
miteu ciuictniuiMi/
ricLO tm ian
QUALITY
f 0<-f-
	Z
miteu auucmiunM
mum iom/wiwmii rutwii
N(im41t« bi< (i*
faraat	tfdnlluil	ItiUutitl	ctutniti	otkar
b«««« ¦¦«*(*•*« ¦(«¦»*¦ (r p««« wywiMlf , ¦•¦~7
Ueil IMtlilM m	aaMaacatrtc^taaa.Vataatlal (aarea^	Obvlawa *a«rcaa	,ot-^Ce. <-0. ^ / OO
«>»»»¦ iuu	HUM »«nm mm ' » _____ »	_0^j® .
¦ Ilk Vatat	O D«« Him») TM — *• y 0(U«
i«4t«k
•	•a War
Cakkta
Oladl
*•¦4
•	lit
clar
>lawwi
>is<-u iia'ia.i
««-»<-*¦ <1.3-1* la.I
K.l-l.S la.I
ffclttrl
M«-.(f-aa ,
><.**«-«• tallck)
farcaal
Ctafaaltiat


fTt»
jurl
Cttra* fltat
tcro«t
llael, T»fy flat
Orfiaic irroni
Qff0 Slall
rrafaMla
9o7«
Zp>"
«MII QUALITY
Taafaratar* T//.3 C Uimivm ny|u / ,13	fU *7 »2-2» Caatfuctlvlty T if	otkar
, C*14aataa MlUIHilfl
Vatar Matil Baraal laaafa fatralaaa	Ckaaleal laaa otkar	rf-a- f. Qto IV»j t±
Mataf Jorfaca ollai allck tkaaa Claka	rlaeka
T«rkl4ltyf ,(KI<(^ «ll«ktlr latkU Yarkl4	Opaqaa Watar Caiar 	„
«utm coaDiTlosi

T
moTMiAtB aoNtti

-------
Has* ot Nater Body
o.t.	93 IB,„t
HABITAT A88BSSH1HT I1ILD DATA SHEET
4c^vtt U-
jv
6tatlon '
i.
roH
Coaaentsi

—j l^V (fto
f-uL ~tMfllta.


\L U v, kL
t*»o
V
HABITAT
PARAHITIR
CATtOORIES
IXC1LLIHT
000D
PAIR
POOR
1. BOTTOM
SUB8TRATI/
AVAILABLE
COVER
>60* rubbls,gravel,
subaarged lei*.
undercut banks,or
other itibU habitat
18-20
30-60* rubble,gravel
er other etable
habitat.
Adequate habitat.
11-15
10-90* rubble,gravel
or othar stable
habitat. Habitat
availability <
daalrabla.
• -10
<10* rubble.gravel
or othar stable
habitat.- Lack oI
habitat la obvious,
lo
Ji
s
0-5
2. EHBIDDID-
Qravel,cobble, snd
Oravel.oobble, and
Oravel.cobble, and
Oravel.oobble. and
HISS
boulder srs <25*
boulder ere 25-50*
boulder are 60-75*
boulder are >75*

surroundsd by fins
aurrounded by fine
surroundsd by fine
aurrounded by fine

sedlaent.
aedlaent.
sedlaent.
aedlaent.

16-20
11-16
6-10
o °-*
9. <* 6 crs
OR
>6 CIS
Coldl > 2 cf«
Marat >5 of*
10-20
81o* (<0.3,a/e).d*ep
(>0.5a)talow,ahalloo
1«0.6b)tfaat(>0.9a/a)
dsepi fsst.shellos
habitats all prasant
16-20
1-2	c(i -
2-6	c(i
11-16
1 «{ 4 habitats
present. (Hlaaln«
rltllti or runs
gat lovar soors than
¦ lasing pools).
11-16
0.6-1 efs
1-2 efs
6-10
2 of 4 habitats
prsssnt. (Hissing
rlfflee/runs get
lover soors.)
6-10
0.5 efs
1 efs
0-5
Doalnatsd by one
velocity/depth
category (usually
pool).
0-5
4. 'CHAKHIb
ALTIRATIOH
Little / no enlarge-
aent of islands or
point bars, and/or
no chsnnellsstlon
12-16
Bobs nee locreaee In
bar formation,aoatly
froa coarse gravel]
and/or soss channel-
isation pressnt.
8-11
Moderate deposition
of naa grsvsl.eosrse
sand on old and nss
bar*(pools partially
filled •/slltiand/or
eabankaents on both
banks.
4-7
Heavy deposits of
tins aaterlal, bar
dsvelopaent lnersaee
Host pools filled v/
sllt;and/or axtenalv*
channelisation.
0-3
6. BOTTOM
8COOR1HO
AHD
DlFOSlTtOH
<6* of bottoa
affected.
1
r
12-16
6-30* affeoted.Boour
at oonstrletlons snd
ateep crsde*. Boa*
deposition In pools.
•-11
90-60* affsotsd.
Deposit snd scour at
obstructions^ bend*,
and constrictions,
>80* bottoa changing
nssrly ysar long.
Pools abssnt due to
deposition. Only
Boas filling of pools lsrgs rocks exposed
4-7	0-3
«. RUH/BIHD.
POOURllfLI
RATlOes
6-T. Variety of
hAbitat.Daep riffles
and pools.
12-16
T-16. Adequate depth 16-25. Oocasslonsl >26. Bsssatislly a
la pools and riffles riffle or band.Bottoa straight atreaa. ria"
Bands provide habitat provide aoae habitat water or ahallo*
Poor habitat.
B-ll	«-T	0-9
7. BAH*
STABILITY
Stabla.Ho jroslon
•r bank failure.Bide
alopaa <30*.
I 0
•-10
Moderately atable
Infrequent aroaion
mtlr bealed over.
•Ida slopes to 40*.
•-•
Moderately unstabla. Unstable. Hsny arodei
Modsrsta arosloo and arsss. 814a slope*
aids alopaa to SO*.
High arosloo during
high flea.
1-5
>80*. "Raw" areas
frequent on straight
and bands.
0-2
8. BAHR
VI0ETAT1YI
STABILITY
>•0* of atreaabank
covered by vegetation
»r boulders and
oobbj
•-10
sbblas.
60-78* oovarad by 26-49* eovated by	<25* covered by
vegetation, gravel or vegetation, gravel or. vegetation, gravel o
larger Material.	larger aaterlal.	larger aaterlal.
g-B
9-6
0-2
•. STRIAH8IDB Dos
COYER
la ahrub
COLUHH TOTALS
SCORB	-LL

P-10
Doalnant vegetation
la of tree fora.
• -8
Poalnant vegetation
ie graee or forbes.
9-5
>60* no vogstetlon
Doalnant aaterlal is
soil,rock, bridge
asterlale,culverts.o
alne tailing*. ~
0-2

-------
Rapid Bioassessment Protocol I r~~J~~Abaant/Not Observed
1 ¦Ran
2 » Common
3 ¦ Abundant
4 » Dominant
MACROBENTHOS QUALITATIVE SAMPLE LIST(lndlt>l* Rtlatlv* Aburvdinct fl • R»r», C • Common, A » Abundinf, D - Dominant)
PorMera
Anlsoptera
C,
Chlronomldaa
Hydroxoa
Zygoplara
Placoplara
Platyhalmlnthaa
Hamlptara f
Ephamaroptara
iTUibellarla
Coleoptsra
K
TVIchoptara
Hlnidlnaa.
Lapldoptara
Olhsr
OllgoetiaelaJ
lalldae
X^otL /4r\ A k
via
Corydalldaa
n n  10
Dominant > SO (Eatlmata)
Observations
figure 6.1-1- .Bioiurvey, Field Data Sheet for uie with Rapid Bioauaitment Protocol I.
A-7

-------
ctuticitl
rarsicAi. ciuutiiwiioi/
ruu tm ikr
Mutcii cuuantuRM
iiyuw loii/igitmn mtwii
(aitNi^laf Ui4 Vaat
raTaaV) ri«w>tiUf«	Miiwiiim
IMlt
Lacal Vtt«
la^lnkt Matai laital	,i*«afa -7 Nltatna	Ckuical
la^luit Oilat [Uatit^ Sllfll	Ralatala	kaatwaa
lallaaat	rapaf rUa>	la*4
OOAtlTt
I (roJt-v
/ o y
nyw/qz
Otkar



sb«4«4
Cfc*aa«lli*4t	V
Otktr

Othar
T»»
iiamau l»>a>»at» Ca«»aa»ata
JU!
l«4rMl
•<*Uai
Cabklt
•(•••I
Su4
¦ lit
ex.*
»lll-u ||« |a.|
«-!»••« ll.MI U.I
II.M.I la.I
• .Htlilfl
t<-aa
|all-
>\o7*
Qfylc |nbitf>U C»«f
Katai Odvrat ll»fail ) lava(• Patfalaaa	Ckaaleal	laaa Otkar _________________
fatar l«i(t«a Oflai Slick fkaaa Claka	Hacka	.
tarkiutyi (elaaf) «U«ktlr * 
-------
Maaa of MtUr Body_
Data ;,07-M>7"H
CnmmmnH	AVtXn
HABITAT A86ESSHEHT MILD DATA SHUT
j &OJ
Station *.
J0£
Inveatlgetor.	(xx\ k^»
y jA^Jj vr* tr U h
2£
UJ
»ijK t^>(

Ui
srU
Xc
o^m (wu?

/j^WOy	iP^y. j*. U £tfV—&-vg j u/ £Cc*. ^~l-*j Aa < * *"

HABITAT
PARAMETER
...L........
1. BOTTOH
SUBSTRATE/
AVAILABLE
COVER
CATEGORIES
EXCELLENT
000D
FAIR
POOR
»60* rubble.gravel,
aubaerged lege,
undareut bank*,or
other.atable habitat
16-20
30-60* rubble.gravel
•r othar atabla
habitat.
Adequate habitat.
11-15
10-30* robble.gravel
or othar atabla
habitat. Habitat
availability <
daalrabla.
6-10
*10* rubble.gravel
or othar atabla
habitat. Lack of
habitat la obvloue.
c£T~ 0-5
fL
2. EMBEDDED-
Oravalioobbla, and
Qravel.eobble. and
Oravalioobbla, and
Qravel.eobble, and
HI63
. boulder are <25*
boulder are 26-60*
boulder are 60-76*
bouldar are >75*

aurrounded by fine
aurrounded by fine
aurrounded by fine
aurrounded by flna

eedlaant.
eedlaant.
eedlaent.
eedlaant.

16-20
11-16
6-10
o °-5
3. <« 6 crs
OR
>6 crs
Coldl > 2 efe
Marat >6 eta
10-20
Blow (<0.3 a/a),deep
(>0.6a)|a low.(hallo*
(<0.5a)|teat(>0.3e/e)
•deapi faet.ahallow
habltate all preaent
16-20
1-2	cfa
2-6	cfa
11-16
3 of 4 habltata
preeent. (Hlialni
rlfflaa or rune
¦at lowar aeora than
aiealni poola).
11-15
0.6-1 cfa
1-2 cfa
6-10
2 of 4 habltata
praaant. (Hlaalng
.rlf (lee/rune gat
lower aeora.)
6-10
0.5 cfa
1 cfa
0-S
Doelnated by one
velocity/depth
category (uaually
pool).
2—
0-5
4.* CHAHHIL
ALTERATION
Little / no enlarge-
aent of lalanda or
point bara, and/or
.no ehannalliatlon
I 2-.-
12-15
Boae new lncraaaa in
bar formation.aoetly
froacoaraa gravel)
and/or aoaa cbannal-
laatlon praaant.
6-11
Moderate dapoaitlon
of new gravel,coaraa
aand on old and new
baraipoole partially
tilled w/alltjand/or
•abankaanta on both
banka.
4-7
Heavy dapoalta of
fine aaterlal, bar
developaent lncraaaa
Hoat poola flllad »/
alit;and/or extenalva
channelleation.
0-3
ft. B0H0H
SCOURIHO
AHD
DEPOSITION
<6* of bottoa
•ffaetad.
IS"
12-1#
5-90* affacted.8oour
•t oonatrlctlona and
ataap gredea. Soae
dapoaitlon in poola.
6-11
30-60* affaotad.
Oapoalt and aeour at
obatruotlone, banda,
and eooatrletlona.
>60* bottoa changing
nearly yaar loaf.
Poola abaent due to
dapoaitlon. Only
Soae filling of poola large rocka expoaed.
4-T	0-3
«. RUH/BIHD,
POOL/RIffLI
RATlOaa
6-7. Variety of
nibltat.Deep rlfflaa
And poola.
12-16
7-16. Adequate dapth 16-25. Oeeaaalonal >25. laeentlally a
In poola and rlfflaa riffle or band.Bottoa atralgbt atraaa. Flat
Bend* provide habitat provide aoae habitat water or aballow
Poor habitat.
•-U	4-T	O °*3
7. BAHK
STABILITY
Stable. Ho eroaloo
or bank (allure.Bide
alopea <30*.
to
8-10
Moderately atabla
Infrequent eroalon
aoetly healed over.
Side alopea to 40*.
8-6
Moderately unetable.	Onatabla. Many eroded
Moderate eroaloo and-	araaa. Side alopea
aide alopea to 60*.	>60*. "Raw" araaa
Nigh eroalon during	frequent on atraliht
blab flow. and benda.
3-8	0-2
8. BAHK >60* of atreaabank	60-76* covered by 26-49* covered by	<25* covered by
VS0ETAT1VE oovered by vegetation vegetation. gravel or vegetation^ gravel or. vegetation, gravel or
STABILITY or bouldera and	larger aaterlal. larger Material.	larger aaterlal.
oobblea.
£) »-l0	8-8 3-6	0-2
8. STIUHI1DI Dominant vegetatloe Dealt
COTSI
COLUMN TOTALS
la ahrub
Doalr
8-8
3-5
>50* no vegetation
Doalnant aaterlal la
aoil.rock. bridge
aatarlala.culvert*,or
alna taillnga.
0-2
SCORE
IX
-------
Raold Bloassessment Protocol I
Bloeurvey Field Data Sheet
TO ^ 10
RELATIVE ABUNDANCE OF AQUATIC BIOTA
Parlphyton	0 12 3 4
Filamenloua Algae 0 12 3 4
Macrophytea	0 12 3 4
Slim* i	0 12 3 4
Macrolnvartabretai 0 12 3 4
Flth	0 12 3 4
0«Abaant/Not Observed
1 ¦ R»re
2 » Common
3 » Abundant
4 - Dominant
MACROBENTHOS QUALITATIVE SAMPLE LIST(lndlc*lt RtUUv* Abundance R>ft*ie, C• Common, A»Abundtrrt, 0-Oomlntnt)
Porlfere
Anlaoptara £
Chlronomldaa
Hydroxoa
Zypoplera
Placoptara
Platyhelmlnthee
Hamlplara C,
Ephemaroptara
lUrbellarla
Colaoptara q
IVIehoptafa
tiiniainea
Lapldoptara
Othar
Oligocnaeu
SlaUdaa
10
Dominant > SO (Eitlmata)
Ooaervauona
Figure-6.1*1/.Bioiurvey.Field Date Sheet for um with Rapid Bioaiseument Protocol I.
A-7
-------
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g««U7I
| CS~Ia-b-"v / o
/«/v/
miicu atucmmnM
iiimim Mit/mmw mmt«
lUMiiut	tu4 iil
Jutit	Plal4/raatata	*f ilraltacal
ucti iit«iik«4 IimImi	Ma4arata ¦••~y
Ucii	Wta fallstlaat	'avldaaca	laaa MUitiai
IHt»«H< Hm« »!«> ' INP ¦	t«»lk| atffla
ll|l «tUf Mil
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la »aaplla< tn«
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laaiiiaaatli) Va«4	___—
yt* uw
Ittaaa fyf«i C«|4«atar ^ WifwitiFS
Halaf 04«f*i	iltua	Cbaalcil	oi»»r __________
Mataf JoKict 0llat Slick Ikaaa	CUM	flaeka	C'»"^ .
T«rkl4ttyi /fliif Sllfktly mikli	«utk!4	»»•<«•	Wat at Calar «»- Lt-	^
rNOTeoakta lumu
-------
J
HABITAT A66ESSHEHT FIELD DATA EHEET
Heee of Mater Bcrfv	»¦>.«-	k Cv_nx-^< Station a / ^ Ca
Data t	Inveetlgator fHcu*~ -C C»-| f
Coaaente	.S	ii ,0 cA^Q—~
r *Cl7?li~	ncCOsy-,	C/rv^ ^
CATEOORIES
Habitat
PARAMETER	EXCELLENT	000D	FAIR	POOR
1.	BOTTOM >60* rubbla,gravel. 30-60* rubble.gravel 10-30* rubble,grevel <10X rubble,gravel
SUBSTRATE/ aubaerged lot*.	or other atabla	or othar (table	or ethar (table
AVAILABLE undereut banka.or habitat. habitat. Habitat	habitat. Lack of
COVER othar atabla habitat Adequate habitat. availability <	habitat la obvious.
desirable.	_
16-20 11-15 9-10	( 0.5
2.	EMBEDDED- Oravel.Gobble, and Oraval.cobble, and (travel.oobbla, and (travel.cobble, and
HESS boulder are <23*	boulder are 26-60*	boulder are 60-75*	boulder are >75*
aurrounded by tine	aurrounded br fine	aurrounded by Una	aurroundad by fine
eedlaent.	aedlaent.	aedlaent. aedlaent.
16-20	11-16	6-10 Q 0-5
3.	<» 5 CfS	Cold| 2 cfa	1-2 cfa	0,6-1 efa	0.5 cfa
Harai >6 cfa	2-6 cfa	1-2 cfa l efa
10-20	11-16	6-10	0-5
OR
>6 crs Slow (<0.l a/a) ideep	9 of 4 habltata	2 of 4 habltata Doalnated by one
(>6.6a)sald*,ahallov	preeent. (Hlaalng	present. (Hlaalng velocity/depth
(<0.6>)ifeet(>0.3a/a)	rlfflee or rune	rlfflea/rune set category (uaually
deepi-fait.ahallo*	(at lower acoro than	lover aoore.) pool),
habltata .'all i praaent	alaalni poola).
16-20	11-16	6-10 0-5
4 CHANNEL Little-/ no'enlarge- Boae no* Increaae In	Moderate deposition	Heavy depoalta of
ALTERATI0H Bant ofilalanda or bar formation.aoatly	of nev gravel,coarae	floe aaterlal, bar
point bara, and/or froacoarse gravel)	aand on old and nee	developaent Increaae
no channelliatlon and/or aoae channel-	baraipoole partially	Moat poola filled u/
laatlon preaent.	filled a/allttand/or	elltiend/or extensive
eabankaenta on both	channelliatlon.
t *)	banka.
»¦ 12-16 6-11	4-7	0-3
6.*BOTTOM (6* of bottoa	6-30* affooted.Boour 90-60* affected. >60* bottoa changing
SCOORIHO affeeted.	at oonatrlctlona and	Depoalt and acour at nearly year long.
IHD	ateep gradee. Boae	obatruotlonat benda. Poola abaent due to
DEPOSITION	depoaltlon In poola.	and cooetrletlona. depoeltlon. Only
i("	Boae filling of poola large rocka. aspoaed.
| 0 12-16	6-11	4-T 0-3
4.	BVH/BEKP, 6-T. Variety of T-16. Adequate depth 16-26. Occassional >25. lasentlally a
POOL/RirrLE Mbltat.Deep rlfflea 1b poola and rlfflee riffle or bond.Bottoa atralght atreaa. riat
BATloaa	and poola.	Bonds provide habitat provide aoaa habitat aater or ahallo*
Poor habitat:
11-16	6-11	4-T	jp 0-3
T. BANK	Btabla. Ho oroalon Moderately atabla	Hoderately unstable.	9oatable."Hear'aroded
STABILITY or buk failure.Bide Infrequent oroalon	Moderate oroalon aod	areaa. Blde'alopes
alopea <901. Boatlr healed ovar.	aide alopet to 60*.	>60*. "Raalrareso
Bide alopea to 40X.	High eroalon during	frequent onTatrainht
. i\ blgb floe. and benda.
I (J |-10 6-8 9-6 0-2
6. BAHK	>60* of atreaabank 80-T6I covered by 26-411 covered by	<26* covered by
VB0ETAT1V! covered br vegetation vegetation, gravel or vegetation^ gravel or vegetation, gravel or
'STABILITY or bouldera and	larger aaterlal.	larger Baterlal.	larger aaterlal.
eobblaa.
^	6-10	6-6	3-6	0-2
B, 6TREAH61DI Dominant vegetation Doalnent vegetation Dominant vegetation >50* no vegetation
COVIB	ie shrub	le of tree form. la graae or forbaa. Dominant aaterlal la
eoll.rock. bridge
¦aterlele,culverts.or
A	nine tailings.
~7 »-10	6-6	3-5	0-2
COLUKH TOTALS	#6					_£	
SCORE	5 I
-------
Rapid Bloassessment Protocol I
Blosurvey Field Data Sheet
QoCu-hv*** loi
G ftf \
*"	Ua»<^u '
RELATIVE ABUNDANCE OF AQUATIC BIOTA
Parlphyton	0 12 3	4
Filamentous Algae 0 12 3	4
Macrophytaa	0 12 3	4
Slimes	0
Macrolnvarltbratei 0
Flth	0
2 3 4
2 3 4
2 3 4
0>AbaentfNot Observed
1 - Rare
2 - Common
3 - Abundant
4 - Dominant
MACROBENTHOS QUALITATIVE SAMPLE LISTflndlcal* Rditivt Abwndinet R«Aitt, C• Common, A»Abundirrt, 0» Domlntnl)
Porlfera
Anlaoptera
K
Chlronomldae C
Hydrozoa
Zyeoptara
K
Plecoptera
Platyhalmlnthea
Hem|plera
*
Ephamereptera
Ibrbellarla
Coleoplara
A
IMchoptera
Hirudins*
Lepldoptera
Other
Ongocnaeiaj
Slalldaa

laopoda <\
Coryaelldae

Amphlpoda]
Tlpulldae

Decaooda
Empldldae

(uatrepoda
Slmullldao

Blvaivia
Tabanldae


Culkldae
4

Rare <3 common J-
9
Abundant > 10
Dominant > SO (Eatlmate)
Obaervaiiona
FJaurt,6:iL1HBIoiur*eviFleld:Dai«:5neet!or.UM!>Mth:RiDia.BiftM»»miftVPlB\afta\\
-------
IITflCU OUUCTUZIATXOV
mu om mi
MALXtt
\fow«^ clr-3—vuJ
mucu ouunniuttM
iim>jui »on/»iT«mi r«*WM'
Fra4aaiaaat fiiim4U« Ui4 *•<
frt«b n«lI««Ui,	DHifMaMti.
mttrjoFM J iiitir
Caaaat clal
Boa
raal »ZS" a
¦a -
Ckaaaallaa4| faa
Ha
Caaafy- Cava*I Ifaat
Ja41aaat Marl laiul
IHUtat Altai Akaaat
•adlaaat"Oapaaltai
l««a|*
r•llfktl
Ckaalaal	*a«
Otkar
HU4atata	vrai
it	Nmi flkar
*aa4
ict>
Otkar
Uv- -*» /S3 K
»MH«»I«	Ca—a¦¦«!»
nt*
Mitel
KiUti
Cakkla
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«aa4.
Ml*.
ei«r
»lS(-«a |t* la.)
««-»«-aa ll.J-U la.I
!-«<-u	Ja.l
l.(M.H-«a |«rtttr>
l.«M-aa latlaki
fucaat
Caayaaltlaa
ta ln»ll»« tf»a
toy*
OH»alc	C»«M
¦ TTK
Hart
Ckaractaclatle
Stick*. Va«4,
Ctiia« lliii
n>t«ruii icrem
•lack, »«ry rlaa
Orfaale IfrOMI
«rar. Ik.11
fiaf»ati
Caafaaltlaa
la	»>•«
za A>
(•¦lifauia ______ C Dlaaal«a4 Oan>a _____	pi	Caa4«etl«ltf _____ Otkac
laatcaaaattal «aa4	~3*
-------
T75*
aurroundad br tin*	aurroundad br (lna	aurroundad by flna	aurroundad by flna
aadlaant.	aadlaant.	aadlaant.	aadlautt.
18-20	. 11-18	8-10	Q 0-5
9. <« 5 CfS Coldi > 2 efa	1-2 cfa	0.8-1 cfa	0.5 cfa
Karat >8 eta	2-8 cfa	1-2 cla	1 cfa
10-20	, li-15	6-10	0-5
OR	i It
»8 CI8 Slow <<0\3 a/a),daaj>	3 of 4 habltata	2 of 4 habltata	Doalnatod by ona
(>b.(a)ialoM,ahallo«	. praaant..(Mlaalng	praaant. (Mlaalng	valoclty/dapth
(<0.8a)tfaat(>0.3a/a)	Tarifflaa orruna	rlffloa/runa tat	catagorr (uaually
daapHfaat'.aballo*	«ot'lo«ar aooro than	loaar aoora.)	pool),
habltata-all'praaant	^alaalni poola).	'
18*20,	111-18	8-10	0-5
4.-CHANNEL L.lttla/-,noanlarga-	Bdae nai looraaaa In	Modarato dapoaltion	Hoary dopoalta of
.ALTERATION- aaotof ialanda or	bar foraatloBiOoatlr	of oaa grayal.coaraa	flna aatdrlal, bar
point bara( and/or	froaooaraa travail	aand on old and na*	dovolopaant lncraaaa
nochannaliiatlon	and/or aoaa channal-	baraipoola partially	Moat poola'fIliad ¦/
laatlon praaant.	flllad o/alltiand/or	alltjand/or oxtenalv
		oabankaanta on both	ohannalisatlon.
I C	banka.
I t-> 12-18	8-11	4-7	0-3
BOTTOM (8k of bottoa	8-30* affaotad.Soour	30-80* affaotad.	80* bottoa changing
SCOOR1HO affaotad.	at oonatrletlona and	Dapoalt and acour at	naarlyyaar lon«.
ABO	ataap gradaa.Boaa	obatruotlona. banda,	Poola abaaot due to
DEPOSITION	dopoaltlon In poola.	and oonatrletlona.	dapoaltlon. Onlr
, y-v	Bom filling of poola larsa roeka axpoaad.
IS 12-18	8-11	4tT.	0-3
_ RUN/BEND. 8-7. Tarlatr of	T-18. Adaquata daptb	18-28. Ooeaaalonal	>25. laaantlallr a
POOL/MIIU fcbitat.Doap rlfflaa	in poola and rlfflaa	rltfla or bond.Bottoa atralght atraaa. Fla
RATIO"* and poola.	Bonda provide habitat	provide aoaa habitat	oatar or ahallo*
Poor habitat;
12-18	B-ll	4-T	2_ °"3
7.'BANK	Stablo. Mo oroalon	tfoderately atablo	Moderately unatablo.	Ooetable. Many orode
8TABIL1TT or .bank fallura.Blda	Infrequent oroalon	Hodarato oroalon and	araaa. Blda alopaa
llopoa <30*.	Molly haalad over.	alda alopaa to 80*.	>80*. "Rao" araaa
Bida alopaa to 40*.	Hlch oroalon during	frequent on atraliht
I s~t	high flow.	and benda.
I CS 8-10	8-8	3-8	0-2
8.	BAN* >80* of atraaabank	B0-TB* covered br	25-49* covered by	<25* covered by
VEGETATIVE corarad br vegetation vegetation, gravel or	vegetation. gravel or vegetation. gravel c
STABILITY or bouldar* and	larger notorial.	larger aatarlal.	larcar aatarlal.
cobble*.
JQ 9-10	8-8	3-8	0-2
B. STREAHSIDE.Doalnant vegetation	Doalnant vegetation	Doalnant vegetation	>50* no vegetation
COVER la ahrub	la of traa for*.	la craaa or forbaa.	Doalnant aatarlal li
aoll.roek. bridge
aat«rlala.eulTarta,<
Cq	Bin* talllnga.
/ 8-10	8-8	3-5	0-2
COLUMN TOTALS					11"
SCORE	"7/
-------
Rapid Bloassessment Protocol I
Bloaurvey Field Data Sheet
Tb-i— • »
lof H f 13.
loerlphyton	0 12 3	4
filamentous Algae 0 12 3	4
Aacrophytea	0 12 3	4
Sllmaa	0 12 3 4
Mae'rolnvertabratas 0 12 3 4
Fish	0 12 3 4
)«Abaanl/Nol Observed
1 ¦ flare
2 - Common
3 » Abundant
4 » Dominant
MACROBENTHOS QUALITATIVE SAMPLE LIST(lndlc*U	Abundant* RaRir*, C» Common, A » AburuUM, Da Dominant)
tarlfera
Anlaoplara C
Chlronomldaa
ttydruoa
Zyooplara (_ i
Plecoptera
'latyhelmlnthee
Hamlplera
Ephemeroptera
Rubella ria
Coleoplara g
Itlchoplefa
taruainaa
Lapldoplera I
Olhar
Sllgocftaeti
Slalldae 1
rrAt
aopooa K
Corydalldaa 1
r ¦/ '
Imphlpoda
Tlpulldae

3ecapoda
Empldldaa

Saatropoda
Slmullldaa

Slvalvla C
Tabanldas


Culkldae £

Flare <3 Common 3-
0 Abundant >10
Dominant >50 (Estimate)
Dbaervatlona
Figure 6.1*1. Bioturvey Field Data Sheet for um with Rapid Bioastetiment Protocol I.
A-7
-------
APPENDIX B
Chemical Analyses of Surface Water and Sediment Samples
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
MEMORANDUM******
DATE: 12/14/93
SUBJECT:
FROM:
Results
94-0036
of Metals Analysis;
TOWER CHEMICAL
CLERMONT FL
CASE NO: 21073SAS
NO: 6175D

Charles H. HoopeL	/tpf\
Chief, Laboratory Evaluation/Qua!ity Assurance Section
TO: DELBERT HICKS
Attached are the results of analysis of samples collected as part
the subject project.
As a result of the Quality Assurance Review, certain data qualifie
may have been placed on the data. Attached is a DATA QUALIFIER
REPORT which explains the reasons that these qualifiers were requi
If you have any questions please contact me.
ATTACHMENT
-------
INORGANIC DATA QUALIFIERS REPORT
Case Number: 21073
Project Number: 94-0036
Site: Tower Chemical. Clermont. FL
Element
Flag
A. Water
Sb, Cd, Cu,	Hg, U
V
Al, Ca, Na,	Zn U
T1	J
Hg	J
Hg	J
All Metals	J
Ni	J
Cr	J
Al	J
B. Soil
Al, Sb, Cd, Hg, U
V, Zn
Samples Affected
Reason
Ca, Cu, Na
Sb
Hg
Al
Ca
Ba
Ni
K
Cr
U
J
J
J
J
J
All positives > IDL, but
<	CRDL
All positives > IDL, but
<	10X contaminant level
All
All positives
MDFQ06, 08, 10, 12, 14,
17, 19, 26, & 27
MDFQ08, 10, 12, 14, 17,
27, 32, 33, 38, & 39
MDFQ08, 14, & 19
MDFQ14
MDFQ38
All positives > IDL, but
<	CRDL
All positives > IDL, but
<	10X contaminant level
All
All positives
All
All
MDFQ20, 31, & 41
MDFQ15, & 41
MDFQ16 & 41
MDFQ13, 18, 21, 22, 23,
25, 30, 35, 36, 6 37
Baseline instability
Positives in blanks
Matrix spike recovery - 65.5%
Matrix spike recovery - 640%
Technical holding time exceeded
with 29 to 30 days elapsing
between sampling and analysis
Sample pH > 2.0 when received
by the laboratory
% RSD > 20% for 1CP multiple
exposures
% RSD > 20% for 1CP multiple
exposures
% RSD > 20% for ICP multiple
exposures
Baseline instability
Positives in blanks
Matrix spike recovery - 73.6%
Matrix spike recovery = 136.1%
Blind spike recovery - 640%
Serial dilution percent
difference - 51.2%
Serial dilution percent
difference - 14.6%
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
% RSD > .20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
-------
INORGANIC DATA QUALIFIERS REPORT (continued)
Case Number: 21073
Project Number: 94-0036
Site: Tower Chemical. Clermont. FL
Element
Cu
Mg
Mn
Se
Cd
As
As
Flap
Samples Affected
MDFQ23, 35, & 37
J	MDFQ13
J	MDFQ13
U	MDFQ41
U	MDFQ15 & 18
U	MDFQ20, 29, & 34
J	MDFQ28
Reason
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures
% RSD > 20% for ICP multiple
exposures and result >
< CRDL
:ipJ
IDL, out
% RSD > 20% for ICP
exposures and result >
<	CRDL
% RSD > 20% for ICP
exposures and result >
<	CRDL
multiple
IDL, but
multiple
IDL, but
Only 2X CRDL standard required
for ICP by SOW
-------
metal^dau report	SAMPLE and analyse
project no "94JUL* *•**«*.	epa~*Egion iv is
m !8We?ofHttICA<-SAMPLE N0" B0S°3 'sample type' SURF' ' * '
CASE NUMBER; 21YPE- s"RFACEWA
SAS NUMBER: 8175D
**
• *
* *
• •
**
iEMENT SYSTEM
fHENS. GA.
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST* FL
COLLECTION START. 10/19/93 1520 STOP: 00/00/00
MD NUMBER: FQ10
12/
UG/L
1100J
10UJ
3UJ
28J
1UJ
1UJ
25000J
5UJ
3UJ
3UJ
1300J
3UJ
7400J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
ANALYTICAL RESULTS
UG/L

56 J
MANGANESE
0 20UJ
MERCURY
7J
NICKEL
5800J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
30000J
SODIUM
3UJ
THALLIUM
NA
TIN
7UJ
VANADIUM
70UJ
ZINC
ANALYTICAL RESULTS
•"REMARKS***	t
SAMPLE RECEIVED WITH A PH GREATER THAN 2	wphakks
RECOMMENDED HOLDING TIME EXCEEDED-HG
•••FOOTNOTES***
?p nr Tun^rATcc tuaV£I9aF25..£ VI, ^°T^5.E.IECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS bATA report	SAMPLE AND ANALYSE
•• PROJECTV *o: ••••••. .	^-REGION ll11
S45 NWI6er, 817so
3EMENT system
¦THENS. GA.
12
/3
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
MD NUMBER: FQ08


550J
ALUMINUM
10UJ
ANTIMONY
3UJ
ARSENIC
12J
BARIUM
1UJ
BERYLLIUM
1UJ
CADMIUM
18000J
CALCIUM
5UJ
CHROMIUM
3UJ
COBALT
20UJ
COPPER
320J
IRON
4UJ
LEAD
4800J
MAGNESIUM
ANALYTICAL RESULTS
UG/L

78J
MANGANESE
0.20UJ
MERCURY
5J
NICKEL
9900J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
16000J
SODIUM
3UJ
THALLIUM
NA
TIN
5UJ
VANADIUM
6 OUJ
ZINC
ANALYTICAL RESULTS
•»»REMARKS»»»	...REMARKS.**
RECOMMENDED HOLDING TIME EXCEEDED-HG
SAMPLE RECEIVED WITH A PH GREATER THAN 2
* * * *A-AVERAGE *VALUE »NA-NOT ANALYZED «NA1-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPT1VE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	c™ »«.erratt«m
»R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
metals data report
SAMPLE AND ANALYSIS
EPA-REGION IV ES.
EMENT SYSTEM
.HENS. GA.
12/
*•
• *
• *
• *
• *
PROJECT NO. 94-0036 SAMPLE NO. 80499 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID: 103-SW
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED	BY: B CARTER
PITV- PI FPMHKJT	• Fl
COLLECTION START: 10/19/93	1055 STOP: 00/00/00
MD NUMBER: FQ06
UG/L

1700
ALUMINUM
10U
ANTIMONY
3U
ARSENIC
28
BARIUM
1U
BERYLL--u«l
1U
CADMIUM
34000
CALCIUM
5U
CHROMIUM
3U
COBALT
30
COPPER
1200
IRON
12
LEAD
5800
MAGNESIUM
ANALYTICAL RESULTS
UG/L

150
MANGANESE
0 20UJ
MERCURY
4U
NICKEL
6900
POTASSIUM
3U
SELENIUM
4U
SILVER
9800
SODIUM
3UJ
THALLIUM
NA
TIN
6U
VANADIUM
210
ZINC
ANALYTICAL RESULTS
»*»REMARKS»««
RECOMMENDED HOLDING TIME EXCEEDED-HG
•»'REMARKS'»»
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	„tDTrt,,Tinu
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS^DATA REPORT	SAMf>LE AND ANALYSIS
*« PitOJFrr an ****'»»»*.	EPA-REqion IV ESi
H	^ "saVle" t'vpV '
SAS NUMBER; 81750
EMENT SYSTEM
HENS. GA.
»**»*»»**»»»»*»«»»»»
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP:
MD NUMBER: FQ12
12/
00/00/00
800J
ALUMINUM
10 UJ
ANTIMONY
3UJ
ARSENIC
12J
BARIUM
1 UJ
BERYLLIUM
1UJ
CADMIUM
18000J
CALCIUM
5UJ
CHROMIUM
3UJ
COBALT
9UJ
COPPER
1200J
IRON
6J
LEAD
4300J
MAGNESIUM
ANALYTICAL RESULTS
UG/L
56 J
MANGANESE
0.20UJ
MERCURY
4UJ
NICKEL
1700J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
12000J
SODIUM
3UJ
THALLIUM
NA
TIN
30UJ
VANADIUM
80UJ
ZINC
ANALYTICAL RESULTS
** 'REMARKS* * *	• • *RFMARK<^t * *
SAMPLE RECEIVED WITH A PH GREATER THAN 2	KtMAKKb
RECOMMENDED HOLDING TIME EXCEEDED-HG
**'FOOTNOTES***
®H5 liWSSRK'WS'Saa gJvI5ESENCE 0F
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MA^NO^BE^RESENT^RESAMPLINg'and'"™ANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ESt .HENS, GA.
12/ J
PROJECT NO. 94-0036 SAMPLE NO. 80507
SOURCE: TOWER CHEMICAL
STATION ID: 105-SWM
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: 8 CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
MD NUMBER: FQ14
UG/L

48J
MANGANESE
0.2UJ
MERCURY
16J
NICKEL
1500J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
11000J
SODIUM
3UJ
THALLIUM
NA
TIN
3UJ
VANADIUM
30UJ
ZINC
UG/L
200J
ALUMINUM
10UJ
ANTIMONY
3UJ
ARSENIC
7J
BARIUM
1UJ
BERYLLIUM
1UJ
CADMIUM
14000J
CALCIUM
21J
CHROMIUM
3UJ
COBALT
9UJ
COPPER
330J
IRON
3UJ
LEAD
3 700J
MAGNESIUM
ANALYTICAL RESULTS
ANALYTICAL RESULTS
•••REMARKS***
SAMPLE RECEIVED WITH A PH GREATER THAN 2
RECOMMENDED HOLDING TIME EXCEEDED-HG
**'REMARKS***
••~FOOTNOTES***
•A-AVERAGE VALUE "NA-NOT ANALYZED »NAI—INTERFERENCES *J-ES11MATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
METALS DATA REPORT
*** ***********
SAMPLE AND ANALYSIS
EPA-REGION IV EL
3EMENT SYSTEM
JHENS. GA.
12,
j3
*******

* *
* * *
* *
* * *
»•	PROJECT NO. 94-0036 SAMPLE NO. 80512	SAMPLE TYPE: SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
**	SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: FL
~»	STATION ID: 106-SW	COLLECTION START: 10/20/93 1600 STOP:
••	CASE NUMBER: 21073	SAS NUMBER:	8175D	MD NUMBER: FQ19
» » • »
00/00/00
• •
* * *

* * *
310
ALUMINUM
10U
ANTIMONY
3U
ARSENIC
28
BARIUM
1U
BERYLLIUM
1U
CADMIUM
46000
CALCIUM
5U
CHROMIUM
3U
COBALT
7U
COPPER
580
IRON
3U
LEAD
21000
MAGNESIUM
***********
ANALYTICAL RESULTS
* * *
* *
* * »
UG/L
59
MANGANESE
0.20UJ
MERCURY
4J
NICKEL
700
POTASSIUM
3U
SELENIUM
4U
SILVER
16000
SODIUM
3UJ
THALLIUM
NA
TIN
3U
VANADIUM
30U
ZINC
**********
ANALYTICAL RESULTS
**'REMARKS***	* **RFMAPk^***
RECOMMENDED HOLDING TIME EXCEEDED-HG	kcmakks***
**'FOOTNOTES***
~A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES.
EMENT SYSTEM
.'HENS, GA.
12/
*»	PROJECT NO. 94-0036 SAMPLE NO. 80510
**	SOURCE: TOWER CHEMICAL
»»	STATION ID: 108-SW
••	CASE NUMBER: 21073	SAS NUMBER:
»»
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
MD NUMBER: FQ17
UG/L

93J
ALUMINUM
10UJ
ANTIMONY
3UJ
ARSENIC
28J
BARIUM
1UJ
BERYLLIUM
1UJ
CADMIUM
23000J
CALCIUM
5UJ
CHROMIUM
3UJ
COBALT
5UJ
COPPER
460J
IRON
3UJ
LEAD
12000J
MAGNESIUM
ANALYTICAL RESULTS
UG/L

53J
MANGANESE
0.20UJ
MERCURY
4UJ
NICKEL
2300J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
7200J
SODIUM
3UJ
THALLIUM
NA
TIN
3UJ
VANADIUM
20UJ
ZINC
ANALYTICAL RESULTS
•••REMARKS***
SAMPLE RECEIVED WITH A PH GREATER THAN 2
RECOMMENDED HOLDING TIME EXCEEDED-HG
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E.
METALS DATA REPORT
*** »*»«*»«•»»#»»«»*•«»~«*•*****»*»*
PROJECT NO. 94-0036 SAMPLE NO. 80520 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID: 111-SW	^
CASE NUMBER: 21073	SAS NUMBER: 8175D
ft
**
**
«*
**
GEMENT SYSTEM
«THENS. GA.
***»****~*»•»~•*«•*»**»**~
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1557 STOP: 00/00/00
MD NUMBER: FQ27
V*.
J3
UG/L

54J
ALUMINUM
10UJ
ANTIMONY
4UJ
ARSENIC
28J
BARIUM
1UJ
BERYLLIUM
1UJ
CADMIUM
28000J
CALCIUM
EUJ
CHROMIUM
3UJ
COBALT
5UJ
COPPER
13J
IRON
3UJ
LEAD
16000J
MAGNESIUM
ANALYTICAL RESULTS
UG/L

15J
MANGANESE
0.20UJ
MERCURY
4UJ
NICKEL
9700J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
15000J
SODIUM
3UJ
THALLIUM
NA
TIN
6UJ
VANADIUM
20UJ
ZINC
ANALYTICAL RESULTS
•«'REMARKS'*»
SAMPLE RECEIVED WITH A PH GREATER THAN 2
RECOMMENDED HOLDING TIME EXCEEDED-HG
*»'REMARKS***
"ISEkss -sans	saus ^pssBaTja'aas mese"ce of B1TE,",L
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES
EMENT SYSTEM
.HENS, GA.
12,
~* PROJECT NO. 94-0036 SAMPLE NO. 80519 SAMPLE TYPE: SURFACEWA
•* SOURCE: TOWER CHEMICAL
*~ STATION ID: 114-SW
»• CASE NUMBER: 21073	SAS NUMBER: 8175D
• •
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1803 STOP: 00/00/00
MD NUMBER: FQ26
UG/L

20
MANGANESE
0 20UJ
MERCURY
4U
NICKEL
11000
POTASSIUM
3U
SELENIUM
4U
SILVER
16000
SODIUM
3UJ
THALLIUM
NA
TIN
6U
VANADIUM
20U
ZINC
UG/L

89
ALUMINUM
10U
ANTIMONY
4U
ARSENIC
35
BARIUM
1U
BERYLLIUM
1U
CADMIUM
20000
CALCIUM
5U
CHROMIUM
3U
COBALT
4U
COPPER
24
IRON
3U
LEAD
18000
MAGNESIUM
ANALYTICAL RESULTS
ANALYTICAL RESULTS
»»'REMARKS*»»
RECOMMENDED HOLDING TIME EXCEEDED-HG
»*»REMARKS»»«
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
metals data report
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E- ATHENS, GA.
11. J3
PROJECT NO. 94-0036 SAMPLE NO. 80525 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID. 117-SW
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST- FL
COLLECTION START. 10/21/93 1140 STOP:
MD NUMBER: FQ32
00/00/00
UG/L
ANALYTICAL RESULTS
UG/L
MANGANESE
78J
ALUMINUM
23J
20UJ
ANTIMONY
0.20UJ
MERCURY
4UJ
ARSENIC
4UJ
NICKEL
35J
BARIUM
11000J
POTASSIUM
1UJ
BERYLLIUM
3UJ
SELENIUM
1UJ
CADMIUM
4UJ
SILVER
30000J
CALCIUM
16000J
SODIUM
5UJ
CHROMIUM
3UJ
THALLIUM
3UJ
COBALT
NA
TIN
5UJ
COPPER
4UJ
VANADIUM
11J
IRON
20UJ
2 INC
3UJ
LEAD


18000J
MAGNESIUM


ANALYTICAL RESULTS
~ •~REMARKS*"
SAMPLE RECEIVED WITH A PH GREATER THAN 2
~•~REMARKS**'
~~~FOOTNOTES"*
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES ~J-ESTIMATED VALUE ~N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
METALS DATA REPORT	EPA-REGION IV E
•* SOURC^ ^Erc^CAL5^^ N°' 80526 SAMPLE TYPE* St/RFACEWA
** STATION ID: 517-SW
H CASE NUMBER: 21073	SAS NUMBER: 8175D
UG/L	ANALYTICAL RESULTS* ************
3EMENT SYSTEM
thens, GA.
12
74J
10UJ
4UJ
34 J
1UJ
1UJ
31000J
5UJ
3UJ
5UJ
12J
3J
18000J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
'collected'by.YcarJer '•••••••
'md'nUMBER: Sf033' 10/21/93	STOP: 00/00/00
'3
* I
UG/L
22J
0.20UJ
4UJ
12000J
3UJ
4U J
16000J
3UJ
NA
4UJ
20UJ
» » * » *
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
**»*»*»***,
ANALYTICAL RESULTS
••'REMARKS*»•
SAMPLE RECEIVED WITH A PH GREATER THAN 2	**'REMARKS***
*•'FOOTNOTES**•
-------
METALS DATA REPORT
SAMPLE AND ANALYSE GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
11 93
** PROJECT NO. 94-0036 SAMPLE NO. 80531	SAMPLE TYPE: SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
•« SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: FL
»•	STATION ID: 120-SW	COLLECTION START. 10/21/93 1350 STOP. 00/00/00
•»	CASE NUMBER: 21073	SAS NUMBER:	8175D	MD NUMBER: F038
*•
UG/L	ANALYTICAL RESULTS	UG/L	ANALYTICAL RESULTS
72J
ALUMINUM
22J
MANGANESE
10UJ
ANTIMONY
0.20UJ
MERCURY
4UJ
ARSENIC
4UJ
NICKEL
33J
BARIUM
11000J
POTASSIUM
1UJ
BERYLLIUM
3UJ
SELENIUM
1UJ
CADMIUM
4UJ
SILVER
31000J
CALCIUM
16000J
SODIUM
5UJ
CHROMIUM
3UJ
THALLIUM
3UJ
COBALT
NA
TIN
4UJ
COPPER
4UJ
VANADIUM
10UJ
IRON
20UJ
ZINC
3UJ
LEAD


18000J
MAGNESIUM


»»'REMARKS***
SAMPLE RECEIVED WITH A PH GREATER THAN 2
**'REMARKS***
**'FOOTNOTES***
VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
«K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
*«*••***»*
SAMPLE AND ANALYSIS
EPA-REGION IV E.
•	t
•	*
* *
SURFACEWA
SOURCE^ fgiE^Sfct.54"" m' 80532 SAM,'LE TVPE
STATION ID: 520-SW
CASE NUMBER: 21073	SAS NUMBER: 8175D
GEMENT SYSTEM
(THENS, GA.
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1350 STOP: 00/00/00
MD NUMBER: FQ39
11
J3


76J
ALUMINUM
10UJ
ANTIMONY
3UJ
ARSENIC
35J
BARIUM
1UJ
BERYLLIUM
1UJ
CADMIUM
31000J
CALCIUM
23J
CHROMIUM
3UJ
COBALT
9UJ
COPPER
110J
IRON
3UJ
LEAD
18000J
MAGNESIUM
ANALYTICAL RESULTS
UG/L

24J
MANGANESE
0.20UJ
MERCURY
15J
NICKEL
11000J
POTASSIUM
3UJ
SELENIUM
4UJ
SILVER
16000J
SODIUM
3UJ
THALLIUM
NA
TIN
3UJ
VANADIUM
30UJ
ZINC
ANALYTICAL RESULTS
•••REMARKS***
SAMPLE RECEIVED WITH A PH GREATER THAN 2
••~REMARKS***
**~FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSI!
EPA-REGION IV t
¦GEMENT SYSTEM
ATHENS. GA.
1.
13
PROJECT NO. 94-0036 SAMPLE NO. 80533 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID: 121-SW
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1830 STOP:
MD NUMBER: FQ41
00/00/00
UG/L

140
ALUMINUM
10U
ANTIMONY
3U
ARSENIC
11
BARIUM
1U
BERYLLIUM
1U
CADMIUM
3100
CALCIUM
5U
CHROMIUM
3U
COBALT
8U
COPPER
36
IRON
3U
LEAD
8600
MAGNESIUM
ANALYTICAL RESULTS
UG/L

5
MANGANESE
0.20U
MERCURY
4U
NICKEL
12000
POTASSIUM
3U
SELENIUM
4U
SILVER
1 3000
SODIUM
3UJ
THALLIUM
MA
TIN
3U
VANADIUM
30U
ZINC
ANALYTICAL RESULTS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALY2ED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E-
5EMENT SYSTEM
.THENS, GA.
12.
PROJECT NO. 94-0036 SAMPLE NO. 80504 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 101-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D


• * * •
MG/KG
1000J
3. 1UJ
0.70U
3.8
0.07U
0.34U
880J
2
1U
5U
120
3
98
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
ANALYTICAL RESULTS
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
MD NUMBER: FQ11
MG/KG
4.4
0.08U
1 . 3U
42U
0.94U
1 2U
70U
0.54U
MA
3U
9.5
43
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
•••FOOTNOTES'"
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUNO MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV ES
METALS DATA REPORT	_ .......
PROJECT NO. 94-0036 SAMPLE NO. 80502	SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 102-SD	_	„
CASE NUMBER: 21073	SAS NUMBER:	8175D
iEMENT SYSTEM
CHENS, GA.
12,
,3
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
MD NUMBER: FQ09
MG/KG
ALUMINUM
1000J
2.7UJ
ANTIMONY
0.62U
ARSENIC
2.2
BARIUM
0.06U
BERYLLIUM
0.29U
CADMIUM
730J
CALCIUM
2
CHROMIUM
0.88U
COBALT
20U
COPPER
280
IRON
2.7
LEAD
100
MAGNESIUM
ANALYTICAL RESULTS
MG/KG	ANALYTICAL RESULTS
2.5	MANGANESE
0.07U	MERCURY
1.1U	NICKEL
40U	POTASSIUM
0.82U	SELENIUM
1.1U	SILVER
40U	SODIUM
0.47U	THALLIUM
NA	TIN
2U	VANADIUM
22	ZINC
33	PERCENT MOISTURE
M tSVEKKWI MESENCE of "*ter,4L
^""indicate! ®v^?AFS5JSLrcKaED«.rSRWESof%JHlRfSrR?SJ^'2Ilo,-&y5is IS necessary for verif,«t,on.
-------
METALS DATA REPORT
• •*•****•••*•*••***•
PROJECT NO. 94-0036 SAMPLE NO. 80500
SOURCE: TOWER CHEMICAL
STATION ID: 103-SD
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE AND ANALYSIS
EPA-REGION IV El
* ************
SAMPLE TYPE: SOIL
8175D
JEMENT SYSTEM
.THENS. GA.
*»*»**»»»»»*»*»»»»»»#**»*
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1055 STOP: 00/00/00
MD NUMBER: FQ07
12,
ANALYTICAL RESULTS
4000J
ALUMINUM
20UJ
ANTIMONY
4.3U
ARSENIC
16
BARIUM
0.41U
BERYLLIUM
2U
CADMIUM
12000J
CALCIUM
20
CHROMIUM
6.1U
COBALT
72
COPPER
940
IRON
36
LEAD
1100
MAGNESIUM
MG/KG	ANALYTICAL RESULTS
58	MANGANESE
0 50U	MERCURY
8U	NICKEL
260U	POTASSIUM
5 7U	SELENIUM
7.6U	SILVER
400	SODIUM
3.3U	THALLIUM
NA	TIN
20U	VANADIUM
230	ZINC
90	PERCENT MOISTURE
*":S^«Eis>S"?5sniI?W!!aGlNJ!5S"E^lcT5S:E5K!gTfiM ^^IhS'SSSI8^5C5ENCE 0F M'TER"L
^,g?*%!SLrc8L^0«}^r?EWS,E^r"i.gi^IK,2joLSiliLYsis is met*™ for vesication.
-------
METALS DATA REPORT
*** *****•**•«*«*****,**»**»,,
PROJECT NO. 94-0036 SAMPLE NO. 80506 SAMPLE TYPE
SOURCE: TOWER CHEMICAL
STATION ID: 104-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
SAMPLE AND ANALYSIS
EPA-REGION IV Ei>
*•
• •
~ ~
• •
* •
SOIL
iEMENT SYSTEM
.THENS. GA.	12, j3
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP: 00/00/00
MD NUMBER: FQ13
MG/KG
170J
2. 7UJ
0.61U
1 .1
0.060
0.29U
7 70J
1 . 7 J
0.88U
3U
35
0.99
49J
ALUMINUM
ANTIMONY
ARSENIC
BARIUM
BERYLLIUM
CADMIUM
CALCIUM
CHROMIUM
COBALT
COPPER
IRON
LEAD
MAGNESIUM
ANALYTICAL RESULTS
MG/KG
0. 73J
MANGANESE
0.07U
MERCURY
1 . 1U
NICKEL
40U
POTASSIUM
1 6
SELENIUM
1 . 1U
SILVER
30U
SODIUM
0.47U
THALLIUM
NA
TIN
15
VANADIUM
12
ZINC
34
PERCENT MOISTURE
••~FOOTNOTES***
I*~£rTnApEUA?ficETc <,uo£;N9J £cA!"^£DT... •NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
^"uatppta^ waI amaFv9?K ISd	GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
lo'nri5n?rA?£l	?«FRF.„^L £0T,.R.E.I£CT£D.. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
METALS DATA REPORT
SAMPLE AND ANALYST
EPA-REGION IV L
\GEMENT SYSTEM
ATHENS, GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80508 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 105-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP:
MD NUMBER: FQ15
00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL
1200J
ALUMINUM
12
MANGANESE
3. 1UJ
ANTIMONY
0.08U
MERCURY
0. 7U
ARSENIC
1 . 5J
NICKEL
2.5
BARIUM
50U
POTASSIUM
0.07U
BERYLLIUM
0 93U
SELENIUM
1U
CADMIUM
1 . 2U
SILVER
25000J
CALCIUM
50U
SODIUM
5.3
CHROMIUM
0.53U
THALLIUM
1U
COBALT
NA
TIN
13
COPPER
5U
VANADIUM
700
IRON
31
ZINC
9.9
LEAD
40
PERCENT MOISTURE
300
MAGNESIUM


* * * FOOTNOTES* » *
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
• U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E_
3EMENT SYSTEM
• THENS, GA.
12,
;3
PROJECT NO. 94-0036 SAMPLE NO. 80509 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 106-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1510 STOP:
MD NUMBER: FQ16
00/00/00
MG/KG
ANALYTICAL RESULTS
5800J
ALUMINUM
20UJ
ANTIMONY
3.5U
ARSENIC
40
BARIUM
0.33U
BERYLLIUM
1 .7U
CADMIUM
21000J
CALCIUM
16
CHROMIUM
5U
COBALT
18
COPPER
2400
IRON
26
LEAD
2700
MAGNESIUM
MG/KG
37
0. 7UJ
6.5U
290J
4.6U
6. 1U
340
2. 7U
NA
20U
33
88
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
**'FOOTNOTES***
SyALYZED,. 'NAI-INTERFERENCES *J-ESTIMATED VALUE .N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
.THENS, GA.
li.. J3
PROJECT NO. 94-0036 SAMPLE NO. 80511 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 108-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
MD NUMBER: FQ18
MG/KG	ANALYTICAL RESULTS
980J
ALUMINUM
3.8U
ANTIMONY
0.86U
ARSENIC
6.2
BARIUM
0.08U
BERYLLIUM
1U
CADMIUM
4600J
CALCIUM
4.1J
CHROMIUM
1.2U
COBALT
8U
COPPER
1300
IRON
5.4
LEAD
310
MAGNESIUM
MG/KG	ANALYTICAL RESULTS
30
MANGANESE
0.2UJ
MERCURY
1 . 6U
NICKEL
60U
POTASSIUM
1 6
SELENIUM
1 . 5U
SILVER
50U
SODIUM
0.66U
THALLIUM
NA
TIN
4U
VANADIUM
17
ZINC
53
PERCENT MOISTURE
»*»FOOTNOTES»««
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV t
GEMENT SYSTEM
ATHENS, GA.
J3
• •
• •
• *
*•
**
PROJECT NO. 94-0036 SAMPLE NO. 80513
SOURCE: TOWER CHEMICAL
STATION ID: 109-SD
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SOIL
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1700 STOP:
MD NUMBER: FQ20
00/00/00
ANALYTICAL RESULTS
MG/KG
1400J
ALUMINUM
26
30UJ
ANTIMONY
0.56U
6U
ARSENIC
8.8U
23J
BARIUM
290U
0.45U
BERYLLIUM
6 3U
2.3U
CADMIUM
8.4U
21000J
CALCIUM
390
15
CHROMIUM
3.6U
6.8U
COBALT
NA
9U
COPPER
20U
1900
IRON
30U
6.6U
LEAD
91
2200
MAGNESIUM

MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
•••FOOTNOTES•»*
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	w^rrr-ATT^.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYST.
EPA-REGION IV E.
.GEMENT SYSTEM
ATHENS, GA.
93
*«	PROJECT NO. 94-0036 SAMPLE NO. 80514 SAMPLE TYPE: SOIL
**	SOURCE: TOWER CHEMICAL
»*	STATION ID: 110-SD
»»	CASE NUMBER: 21073	SAS NUMBER: 8175D
• «
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP:
MD NUMBER: FQ21
00/00/00
ANALYTICAL RESULTS
1700J
ALUMINUM
30UJ
ANTIMONY
4.8U
ARSENIC
26
BARIUM
0.46U
BERYLLIUM
2.3U
CADMIUM
22000J
CALCIUM
:6J
CHROMIUM
6.9U
COBALT
20U
COPPER
1700
IRON
6.7U
LEAD
2300
MAGNESIUM
MG/KG
32
0 57U
9U
290U
6 4U
8.5U
370
3. 7U
NA
20U
100
92
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	^ „rD,r,r.TT™.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES.
iEMENT SYSTEM
fHENS. GA.
12/
.3
PROJECT NO. 94-0036 SAMPLE NO. 80515 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 111-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
riTv- n FRMnwT	ST* FL
COLLECTION START: 10/21/93 1718 STOP: 00/00/00
MD NUMBER: FQ22
MG/KG	ANALYTICAL RESULTS
2000J
ALUMINUM
22UJ
ANTIMONY
5U
ARSENIC
9
BARIUM
0.48U
BERYLLIUM
2.4U
CADMIUM
16000J
CALCIUM
13J
CHROMIUM
7.2U
COBALT
8U
COPPER
2000
IRON
6.9U
LEAD
1900
MAGNESIUM
MG/KG	ANALYTICAL RESULTS
31
MANGANESE
0.61U
MERCURY
9.3U
NICKEL
300U
POTASSIUM
6 7U
SELENIUM
8.8U
SILVER
420
SODIUM
3.8U
THALLIUM
NA
TIN
30U
VANADIUM
30U
ZINC
92
PERCENT MOISTURE
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE '^-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~ U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	___ WCDtlrTrATtrMJ
»R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
vlAGEMENT SYSTEM
ATHENS. GA.
j/93
PROJECT NO. 94-0036 SAMPLE NO. 80516
SOURCE: TOWER CHEMICAL
STATION ID: 112-SD
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SOIL
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1840 STOP:
MD NUMBER: FQ23
00/00/00
ANALYTICAL RESULTS
1000J
ALUMINUM
30UJ
ANTIMONY
6.6U
ARSENIC
12
BARIUM
0.63U
BERYLLIUM
3.1U
CADMIUM
12000J
CALCIUM
19J
CHROMIUM
9.4U
COBALT
16J
COPPER
720
IRON
9.1U
LEAD
1700
MAGNESIUM
MG/KG	ANALYTICAL RESULTS
19	MANGANESE
0.83U	MERCURY
20U	NICKEL
400U	POTASSIUM
8.8U	SELENIUM
20U	SILVER
690	SODIUM
5U	THALLIUM
NA	TIN
30U	VANADIUM
30U	ZINC
94	PERCENT MOISTURE
*A-AVFRAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN .L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
• U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MI NI MUM OUANTIT AT I ON LIMIT .	NFr(r<-cARY FOR VERIFICATION
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES.
iEMENT SYSTEM
CHENS, GA.
12,
*»	PROJECT NO. 94-0036 SAMPLE NO. 80517 SAMPLE TYPE: SOIL
«» SOURCE: TOWER CHEMICAL
#* STATION ID: 113-SD
•• CASE NUMBER: 21073	SAS NUMBER: 8175D
• *
PROG ELEM: SSF COLLECTED BY: B CARTER
riTv• n FRUnwT	Ft
COLLECTION START: 10/21/93 1827 STOP: 00/00/00
MD NUMBER: FQ24
MG/KG
ANALYTICAL RESULTS
1600J
ALUMINUM
40UJ
ANTIMONY
7.6U
ARSENIC
14
BARIUM
0.72U
BERYLLIUM
3.6U
CADMIUM
15000J
CALCIUM
20U
CHROMIUM
20U
COBALT
20U
COPPER
1200
IRON
20U
LEAD
1900
MAGNESIUM
MG/KG
31
0.83U
14U
460U
20U
20U
560
5.8U
NA
50U
40U
94
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
*»A-AVERAGE * VALUE »NA-N0T ANALYZED .NAT-INTERFERENCES .J-ESTIMATED VALUE *N~PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	U..CC<.|DU pnD UCDTrtrATTnu
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV ES>
METALS DATA REPORT
»«*«»»»»»•«•»•»•»••»«**»»«»»**«*'
PROJECT NO. 94-0036 SAMPLE NO. 80518 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
JEMENT SYSTEM
.THENS. GA.
*»»»»»»«»»***»»•#»»»»»»»»
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START. 10/21/93 1813 STOP: 00/00/00
MD NUMBER" FQ25
12,
/3
MG/KG
ALUMINUM
2300J
30UJ
ANTIMONY
5. 7U
ARSENIC
21
BARIUM
0.54U
BERYLLIUM
2.7U
CADMIUM
24000J
CALCIUM
14J
CHROMIUM
8.2U
COBALT
18
COPPER
1800
IRON
7.9U
LEAD
2300
MAGNESIUM
ANALYTICAL RESULTS
MG/KG	ANALYTICAL RESULTS
37	MANGANESE
0.69U	MERCURY
20U	NICKEL
350U	POTASSIUM
7 6U	SELENIUM
20U	SILVER
440	SODIUM
4.4U	THALLIUM
NA	TIN
40U	VANADIUM
30U	ZINC
93	PERCENT MOISTURE
"'SfcSK&pM «£?£	jggs |?S^fa,WSI®S MESENCE 0F mm"L
:raT5SMl ffirS?AFSSuISSLrcSS5^Dl«™WE^}SJH^1irMR?^ISfJISJ,2!loLS?itl«LYSIS IS NECESSARY FOR VERIFICATION
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
aTHENS. GA.
J3
PROJECT NO. 94-0036 SAMPLE NO. 80521
SOURCE: TOWER CHEMICAL
STATION ID: 115-SD
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SOIL
8175D
PROG ELEM: SSF
CITY: CLERMONT
COLLECTION START:
MD NUMBER: F028
COLLECTED BY: B CARTER
ST: FL
10/21/93 1230 STOP:
00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANAL
2500J
ALUMINUM
93
MANGANESE
30UJ
ANTIMONY
0.61U
MERCURY
23J
ARSENIC
10U
NICKEL
59
BARIUM
330U
POTASSIUM
0.51U
BERYLLIUM
7.2U
SELENIUM
2.6U
CADMIUM
9.5U
SILVER
51000J
CALCIUM
590
SODIUM
21
CHROMIUM
4. 1U
THALLIUM
7.7U
COBALT
NA
TIN
21
COPPER
40U
VANADIUM
1800
IRON
40U
ZINC
8.5
LEAD
93
PERCENT MOISTURE
4500
MAGNESIUM


ANALYTICAL RESULTS
*»'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E-
METALS DATA REPORT	^ 4
PROJECT NO. 94-0036 SAMPLE NO. 80522	SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 116-SD	_	^
CASE NUMBER: 21073	SAS NUMBER:	8175D
3EMENT SYSTEM
.THENS. GA.
12.
/3
**»»~~~»«»«»»»•»»»»»~••*»»»»**
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL	_
COLLECTION START: 10/21/93 1215 STOP: 00/00/00
MD NUMBER: FQ29
MG/KG
ALUMINUM
900J
20UJ
ANTIMONY
8U
ARSENIC
75
BARIUM
0.40U
BERYLLIUM
13
CADMIUM
140000J
CALCIUM
13
CHROMIUM
5.9U
COBALT
20U
COPPER
910
IRON
6.5
LEAD
3700
MAGNESIUM
ANALYTICAL RESULTS
MG/KG	ANALYTICAL RESULTS
120	MANGANESE
0.52U	MERCURY
7.7U	NICKEL
250U	POTASSIUM
5.6U	SELENIUM
7.3U	SILVER
760	SODIUM
3.2U	THALLIUM
NA	TIN
20U	VANADIUM
30U	ZINC
90	PERCENT MOISTURE
.WA-NOT ANALYZED »NAI-INTERFERENCES .J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWK) BE LESSTHAN VALUE GIVEN .L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
• U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM OUANTI TAT ION LIMIT	NECESSARY FOR VERIFICATION
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS 15 NECES5ARY rOK vtKiriu
-------
METALS DATA REPORT
SAMPLE AND ANALYST.
EPA-REGION IV t.
.GEMENT SYSTEM
ATHENS, GA.
li.
93
PROJECT NO. 94-0036 SAMPLE NO. 80523 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 117-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST' FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
MD NUMBER: FQ30
ANALYTICAL RESULTS
310J
ALUMINUM
30UJ
ANTIMONY
5.6U
ARSENIC
30
BARIUM
0.54U
BERYLLIUM
2.7U
CADMIUM
50000J
CALCIUM
18J
CHROMIUM
8U
COBALT
10U
COPPER
420
IRON
7.8U
LEAD
3100
MAGNESIUM
MG/KG
76
0.67U
20U
340U
7 5U
9.9U
770
4. 3U
NA
20U
30U
93
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
•»'FOOTNOTES*»»
»A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
3EMENT SYSTEM
•THENS, GA.
12.
>3
PROJECT NO. 94-0036 SAMPLE NO. 80524 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 517-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/21/93 1200 STOP: 00/00/00
MD NUMBER: FQ31
MG/KG

290J
ALUMINUM
30UJ
ANTIMONY
5.8U
ARSENIC
17J
BARIUM
0.55U
BERYLLIUM
2.8U
CADMIUM
17000J
CALCIUM
21
CHROMIUM
8.3U
COBALT
9U
COPPER
310
IRON
8U
LEAD
3000
MAGNESIUM
ANALYTICAL RESULTS
MG/KG	ANALYTICAL RESULTS
61	MANGANESE
0.70U	MERCURY
20U	NICKEL
350U	POTASSIUM
7.7U	SELENIUM
20U	SILVER
530	SODIUM
4.4U	THALLIUM
NA	TIN
9U	VANADIUM
30U	ZINC
93	PERCENT MOISTURE
* * *»A^AVFRAGE *VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN ^L^ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS^THE MINIMUM QUANTITATION LIMIT	uerF^ARV FOR VFRIFICATION
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E-
METALS DATA REPORT
•«•»•*»••*•******•***•**********'
*• PROJECT NO. 94-0036 SAMPLE NO. 80527 SAMPLE TYPE: SOIL
•• SOURCE: TOWER CHEMICAL
~ * STATION ID. 118-SD	. . ..
CASE NUMBER: 21073	SAS NUMBER: 8175D
»»
3EMENT SYSTEM
.THENS, GA.
**«»»««**»»»»~»»«»»»»»~*»»
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/21/93 1445 STOP: 00/00/00
MD NUMBER: FQ34
12
MG/KG

2800J
ALUMINUM
30UJ
ANTIMONY
7U
ARSENIC
37
BARIUM
0.48U
BERYLLIUM
2.4U
CADMIUM
12000J
CALCIUM
16
CHROMIUM
7.2U
COBALT
8U
COPPER
2600
IRON
7U
LEAD
2900
MAGNESIUM
ANALYTICAL RESULTS
MG/KG	ANALYTICAL RESULTS
21	MANGANESE
O 60U	MERCURY
9.4U	NICKEL
31OU	POTASSIUM
6 8U	SELENIUM
8.9U	SILVER
400	SODIUM
3.9U	THALLIUM
NA	TIN
30U	VANADIUM
30U	ZINC
92	PERCENT MOISTURE
"':SEi^E.s	sus ™^psBffl,ui,6aH mesence of mater,al
t!!JV,EI?AFS5uIJLrcSSEVvVKESo}S^^rV^n!lPaL&LVSI5 IS NECESSARY FOR VEKIF,CAT,0».
-------
METALS DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV .
HGEMENT SYSTEM
ATHENS. GA.
93
**	PROJECT NO. 94-0036 SAMPLE NO. 80528 SAMPLE TYPE: SOIL
~ »	SOURCE: TOWER CHEMICAL
»~	STATION ID: 119-SD
»*	CASE NUMBER: 21073	SAS NUMBER: 8175D
*•
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1430 STOP:
MD NUMBER: FQ35
00/00/00
ANALYTICAL RESULTS
3 TOO J
ALUMINUM
39
MANGANESE
30UJ
ANTIMONY
0.60U
MERCURY
5.6U
ARSENIC
20U
NICKEL
31
BARIUM
340
POTASSIUM
0.54U
BERYLLIUM
7.5U
SELENIUM
2.7U
CADMIUM
9.9U
SILVER
18000J
CALCIUM
520
SODIUM
20J
CHROMIUM
4.3U
THALLIUM
8.1U
COBALT
NA
TIN
14J
COPPER
30U
VANADIUM
3200
IRON
40U
ZINC
7.8U
LEAD
93
PERCENT MOISTURE
3100
MAGNESIUM


ANALYTICAL RESULTS
•••FOOTNOTES*»»
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
3EMENT SYSTEM
.THENS, GA.
12 j3
PROJECT NO. 94-0036 SAMPLE NO. 80529 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 120-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM. SSF COLLECTED BY: B CARTER
r TTV • ri PPIAOKIT	• Fl
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
MD NUMBER: FQ36
MG/KG	ANALYTICAL RESULTS
2700J
ALUMINUM
30UJ
ANTIMONY
4.9U
ARSENIC
41
BARIUM
0.47U
BERYLLIUM
2.3U
CADMIUM
20000J
CALCIUM
18J
CHROMIUM
7U
COBALT
20U
COPPER
3100
IRON
6.8U
LEAD
2600
MAGNESIUM
MG/KG	ANALYTICAL RESULTS
42
MANGANESE
0 8UJ
MERCURY
9. 1U
NICKEL
300U
POTASSIUM
6 5U
SELENIUM
8.6U
SILVER
440
SODIUM
3 . 7U
THALLIUM
NA
TIN
30U
VANADIUM
40U
ZINC
91
PERCENT MOISTURE
•••FOOTNOTES***
YALyE	 'NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
SAMPLE AND ANALYSIS
EPA-REGION IV Et
«E«°!JT» »••~~~~•~~**~**»~ */*?,**
PROJECT NO. 94-0036 SAMPLE NO. 80530	SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD	017t-n
CASE NUMBER: 21073	SAS NUMBER:	8175D
3EMENT SYSTEM
.THENS, GA,
12,
~ *~*•~#*~**~~»*~***~~**~********
MG/KG	ANALYTICAL RESULTS
2600J	ALUMINUM
30UJ	ANTIMONY
5.1U	ARSENIC
31	BARIUM
0.48U	BERYLLIUM
2.4U	CADMIUM
17000	CALCIUM
11J	CHROMIUM
7.2U	COBALT
18J	COPPER
2700	IRON
7U	LEAD
2400	MAGNESIUM
,**«~*»««~»•»»************•*****
PROG ELEM: SSF COLLECTED BYj B^CARTER
COLLECTION^TART: 10/21/93 1415 STOP: 00/00/00
MD NUMBER: FQ37
*~*««»«#~****««***•*************
MG/KG	ANALYTICAL RESULTS
36	MANGANESE
0 61U	MERCURY
9.4U	NICKEL
310U	POTASSIUM
6.8U	SELENIUM
8.9U	SILVER
480	SODIUM
3.9U	THALLIUM
NA	TIN
20U	VANADIUM
30U	ZINC
92	PERCENT MOISTURE
• ••FOOTNOTES***	.....	...AT TuTFDFFRFkirF<; « i-FSTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
• A-AVERAGE VALUE '"fa*®}. RF i~F^t THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
15 NECESSARY F0R VERIFICATI0N
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV L
GEMENT SYSTEM
ATHENS, GA.
J3
PROJECT NO. 94-0036 SAMPLE NO. 80534
SOURCE: TOWER CHEMICAL
STATION ID. 121-SD
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SOIL
8175D
C??S:ESRM§5f C0LLECTE0
'md^NUMBER:SFQ*12 r0/!L"S3 '«» SW; 00/00/00
MG/KG

1200J
ALUMINUM
2.9UJ
ANTIMONY
0.67U
ARSENIC
1 .6J
BARIUM
0.06U
BERYLLIUM
0.32U
CADMIUM
190U
CALCIUM
2.5
CHROMIUM
0.96U
COBALT
6U
COPPER
300
IRON
2. 7
LEAD
80
MAGNESIUM
ANALYTICAL RESULTS
MG/KG
3
0.07U
1 4J
47J
2U
1 . 2U
40U
0.51U
NA
3U
5U
38
MANGANESE
MERCURY
NICKEL
POTASSIUM
SELENIUM
SILVER
SODIUM
THALLIUM
TIN
VANADIUM
ZINC
PERCENT MOISTURE
ANALYTICAL RESULTS
»•'FOOTNOTES*»*
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-GC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST. .GEMENT SYSTEM
EPA-REGION IV fc- ATHENS, GA.	lit, ,93
EXTRACTABLE ORGANICS DATA REPORT
*» PROJECT
~* SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO. 80503
TOWER CHEMICAL
ID: 101-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER ••
ST: FL ••
1520 STOP: 00/00/00 •*
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ10
• *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1,3-DlCHLOROBENZENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2.2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1.2.4-TRICHL0R0BENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHL0R0-3-METHYLPHEN0L
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHLOROPHENOL
25UJ	2,4.5-TRICHL0R0PHEN0L
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITR0PHEN0L
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4.6-DINITR0PHEN0L
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHL0R0BENZIDINE
10UJ	BENZO(AJANTHRACENE
10UJ	CHRYSENE
20UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BEN20(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A.H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI W3EMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	K 93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80503 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 101-SW	COLLECTION START: 10/19/93 1520 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ10 MD NO: FQ10
ANALYTICAL RESULTS UG/L
5JN HEXADECANOIC ACID
2JN DICHLOROBENZOIC ACID
•••REMARKS***	**»REMARKS**«
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26,1984)
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS IAGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	/93
EXTRACTABLE ORGANICS DATA REPORT
•« PROJECT
»* SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO. 80501
TOWER CHEMICAL
ID: 102-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER *»
ST: FL ••
1230 STOP: 00/00/00 *•
*• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ08
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHVL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1,3-DICHLOROBENZENE
10UJ	1.4-DICHLOROBENZENE
10UJ	1.2-DICHLOROBENZENE
10UJ	2-METHYLPHEN0L
10UJ	2,2'-CHL0R0IS0PR0PYLETHER
10UJ	(3-AND/OR 4-JMETHYLPHENOL
10UJ	N-NIT ROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NIT ROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1.2.4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHLORO-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHL0R0PHEN0L
25UJ	2,4,5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ 3-NITROANILINE
10UJ ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHLOROPHEK1YL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
1OUJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHL0R0BENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
20UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
»•'REMARKS*»•	*»'REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES**'
•A-AVERAGE VALUE *NA-NOT ANALYZED 'NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS JAGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	_,/93
EXTRACTABLE ORGANICS DATA REPORT
** PROJECT
*• SOURCE:
** STATION
NO. 94-0036 SAMPLE NO. 80499
TOWER CHEMICAL
ID: 103-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM. SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER *»
ST: FL ••
1055 STOP: 00/00/00 «*
** CASE NO.
21073
SAS NO.: 8175D
D. NO. : FQ06
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1.3-DICHLOROBENZENE
10UJ	1,4-DICHLOROBENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-JMETHYLPHENOL
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2,4-DIMETHYLPHENOL
10UJ	BISC 2-CHLOROETHOXY) METHANE
10UJ	2,4-DICHLOROPHENOL
10UJ	1.2.4-TRICHL0R0BENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHL0R0-3-METHYLPHEN0L
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHL0R0PHEN0L
25UJ	2,4,5-TRICHL0R0PHEN0L
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NIT ROANILINE
10UJ	ACENAPHTHENE
25UJ	2,4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4.6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.S'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
20UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZOC B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A.H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
**'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST. vGEMENT SYSTEM
EPA-REGION IV t. ATHENS. GA.	93
EXTRACTABLE ORGANICS DATA REPORT
«• PROJECT
•* SOURCE:
*» STATION
NO. 94-0036 SAMPLE NO. 80505
TOWER CHEMICAL
ID: 104-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER *»
ST: FL ••
1735 STOP: 00/00/00 •*
»* CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ12
« *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1.3-DICHLOROBENZENE
10UJ	1,4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-JMETHYLPHENOL
10UJ	N-NITROSODI-N-PROPYLAM1NE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2,4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHE NOL
10UJ	1,2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHLOROANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHLORO-3-ME THYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4,6-TRICHLOROPHENOL
25UJ	2.4,5-TRICHL0R0PHEN0L
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ 3-NITROANILINE
10UJ ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINI TROT OLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
1OUJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3,3'-DICHL0R0BENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZOCB AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***	•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS1! .GEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.	1; J3
EXTRACTABLE ORGANICS DATA REPORT
*• PROJECT
•• SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO. 80507
TOWER CHEMICAL
ID: 105-SWM
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER **
ST: FL ••
1800 STOP: 00/00/00 «•
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: F014
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHL0R0PHEN0L
10UJ	1 .3-DICHLOROBENZENE
10UJ	1.4-DICHL0R0BEN2ENE
10UJ	1.2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHENOL
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2,4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1.2.4-TRICHL0R0BENZENE
10UJ	NAPHTHALENE
10UJ	4-CHLOROANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHLORO-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHL0R0PHEN0L
25UJ	2,4.5-TRICHL0R0PHEN0L
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2.4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITR0ANILINE
25UJ	2-METHYL-4.6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO M.2.3-CD) PYRENE
10UJ	DIBENZOlA,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS**'
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••REMARKS***
•••FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS .EMENT SYSTEM
EPA-REGION IV ES. .THENS. GA.	12, j3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80507 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 105-SWM	COLLECTION START: 10/19/93 1800 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D NO.: F014 MD NO: FQ14
ANALYTICAL RESULTS UG/L
3JN DICHLOROBEKIZOIC ACID
•••REMARKS***	«»*REMARKS*»*
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•*"FOOTNOTES*»»
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI 4GEMENT SYSTEM
EPA-REGION IV t. ATHENS. GA.	li. /93
EXTRACTABLE ORGANICS DATA REPORT
*• PROJECT
•• SOURCE:
•* STATION
NO. 94-0036 SAMPLE NO. 80512
TOWER CHEMICAL
ID: 106-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER **
ST: FL ••
1600 STOP: 00/00/00 **
•* CASE NO.
21073
SAS NO.: 8175D
D. NO.: F019
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1.3-DICHL0R0BENZENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHL0R0PHEN0L
10UJ	1,2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUT ADIENE
10UJ	4-CHLORO-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4,6-TRICHLOROPHENOL
25UJ	2.4,5-TRICHL0R0PHEN0L
10UJ	2-CHL0R0NAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ 3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITR0PHEN0L
25UJ	4-NIT ROPHE NOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITR0T0LUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTVLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A.H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI CEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1_ /93
EXTRACTABLE ORGANICS DATA REPORT
•• PROJECT
•• SOURCE:
** STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 108-SW
80510 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER »«
ST: FL »•
1715 STOP: 00/00/00 »*
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ17
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
1OUJ	1.3-DICHLOROBEN2ENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1.2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2.2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHE NOL
10UJ	1,2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HE XACHLOROBUTADIENE
10UJ	4-CHL0R0-3-ME THYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHLOROPHENOL
25UJ	2.4,5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BROMOPHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
20UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1,2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHIJPERYLENE
»•'REMARKS'**	**'REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••FOOTNOTES***
~A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI	VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1, 93
EXTRACTABLE ORGANICS DATA REPORT
•» PROJECT
•• SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO. 80520
TOWER CHEMICAL
ID: 111-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER •«
ST: FL ••
1557 STOP: 00/00/00 **
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: F028
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
1OUJ	1.3-DICHLOROBENZENE
10UJ	1,4-DICHLOROBENZENE
10UJ	t,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHENOL
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
1OUJ	2.4-DICHLOROPHENOL
10UJ	1.2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHLOROANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHL0R0-3-METHYLPHEN0L
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHLOROPHENOL
25UJ	2.4.5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITR0ANILINE
251) J	2-METHYL-4.6-DINI TROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZOl A)ANTHRACENE
10UJ	CHRYSENE
30UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
••'REMARKS*»•
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26,1984)
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV EL .THENS, GA.	12, (3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80520 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY. CLERMONT ST. FL
STATION ID: 111—SW	COLLECTION START: 10/20/93 1557 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D NO.: FQ28 MD NO: FQ27
ANALYTICAL RESULTS UG/L
3JN HEXADECANOIC ACID
'"REMARKS'"
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
'"REMARKS'"
«» 'FOOTNOTES'"
'A-AVERAGE VALUE 'NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
'K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
SAMPLE AND ANALYST AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	/93
EXTRACTABLE ORGANICS DATA REPORT
•» PROJECT
•• SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 114-SW
80519 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER ••
ST: FL *•
1803 STOP: 00/00/00 **
• • CASE NO.
21073
SAS NO.: 8175D
D. NO.: F026
* •
UG/L	ANALYTICAL RESULTS
20UJ	PHENOL
20UJ	BIS(2-CHLOROETHYL) ETHER
20UJ	2-CHLOROPHENOL
20UJ	1.3-DICHLOROBENZENE
20UJ	1.4-DICHLOROBENZENE
20UJ	1,2-DICHLOROBENZENE
20UJ	2-METHYLPHENOL
20UJ	2.2'-CHL0R0IS0PR0PYLETHER
200J	(3-AND/OR 4-)METHYLPHENOL
20UJ	N-NIT ROSODI-N-PROPYLAMINE
20UJ	HEXACHLOROETHANE
20UJ	NITROBENZENE
20UJ	ISOPHORONE
20UJ	2-NIT ROPHENOL
20UJ	2,4-DIMETHYLPHENOL
20UJ	BIS(2-CHLOROETHOXY) METHANE
20UJ	2.4-DICHLOROPHENOL
20UJ	1,2,4-TRICHLOROBENZENE
20UJ	NAPHTHALENE
20UJ	4-CHL0R0ANILINE
20UJ	hexachlorobutadiene
20UJ	4-CHL0R0-3-METHYLPHEN0L
20UJ	2-METHYLNAPHTHALENE
20UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
20UJ	2,4.6-TRICHLOROPHENOL
50UJ	2,4,5-TRICHLOROPHENOL
20UJ	2-CHLORONAPHTHALENE
50UJ	2-NITROANILINE
20UJ	DIMETHYL PHTHALATE
20UJ	ACENAPHTHYLENE
20UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
50UJ 3-NITROANILINE
20UJ	ACENAPHTHENE
50UJ	2.4-DINITROPHENOL
50UJ	4-NITROPHENOL
20UJ	DIBENZOFURAN
20UJ	2.4-DINITROTOLUENE
20UJ	DIETHYL PHTHALATE
20UJ	4-CHLOROPHENYL PHENYL ETHER
20UJ	FLUORENE
50UJ	4-NITROANILINE
50UJ	2-METHYL-4.6-DINITROPHENOL
20UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
20UJ	4-BROMOPHENYL PHENYL ETHER
20UJ	HEXACHLOROBENZENE (HCB)
50UJ	PENTACHLOROPHENOL
20UJ	PHENANTHRENE
20UJ	ANTHRACENE
20UJ	CARBAZOLE
20UJ	DI-N-BUTYLPHTHALATE
20UJ	FLUORANTHENE
20UJ	PYRENE
20UJ	BENZYL BUTYL PHTHALATE
20UJ	3.3'-DICHLOROBENZIDINE
20UJ	BENZO(A)ANTHRACENE
20UJ	CHRYSENE
50UJ	BIS(2-ETHYLHEXYL) PHTHALATE
20UJ	DI-N-OCTYLPHTHALATE
20UJ	BENZOIB AND/OR K)FLUORANTHENE
20UJ	BENZO-A-PYRENE
20UJ	INDENO (1.2,3-CD) PYRENE
20UJ	DIBENZO(A.H)ANTHRACENE
20UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••remarks***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ESL ..HENS, GA.	12/.
EXTRACTABLE ORGANICS DATA REPORT
•» PROJECT
•• SOURCE:
»» STATION
NO. 94-0036 SAMPLE NO. 80525
TOWER CHEMICAL
ID: 117-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL *•
1140 STOP: 00/00/00 **
•» CASE NO.
21073
SAS NO.: 8175D
D. NO.: F034
* *
UG/L	ANALYTICAL RESULTS
,10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1,3-DICHLOROBENZENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2.2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2,4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1,2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUT ADIENE
10UJ	4-CHL0R0-3-METHYLPHEN0L
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2.4.6-TRICHLOROPHENOL
25UJ	2.4.5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITR0T0LUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2.4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4.6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BROMOPHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZOlA)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZOt B AND/OR K) FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZOtA.H)ANTHRACENE
10UJ	BENZOtGHI)PERYLENE
•••REMARKS***	•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS JEMENT SYSTEM
_ „	EPA-REGION IV ESu. ATHENS, GA.	12/.-,93
EXTRACTABLE ORGANICS DATA REPORT
*• PROJECT
•• SOURCE:
»» STATION
NO. 94-0036 SAMPLE NO. 80526
TOWER CHEMICAL
ID: 517-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER *«
ST: FL *•
1140 STOP: 00/00/00 **
*• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ35
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
tOUJ	2-CHLOROPHENOL
10UJ	1,3-DICHLOROBENZENE
10UJ	1,4-DICHLOROBENZENE
10UJ	t.2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NIT ROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1,2.4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHL0R0-3-METHYLPHEN0L
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2,4.6-TRICHLOROPHENOL
25UJ	2,4.5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ 3-NITR0ANILINE
10UJ ACENAPHTHENE
25UJ 2,4-DINITR0PHEN0L
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
1OUJ	N-NITROSOOIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	Dl-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3,3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1,2.3-CD) PYRENE
10UJ	DIBENZO(A.H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV Ei. aTHENS , GA.	12, J3
EXTRACTABLE ORGANICS DATA REPORT
«* PROJECT
•• SOURCE:
** STATION
NO. 94-0036 SAMPLE NO. 80531
TOWER CHEMICAL
ID: 120-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL ••
1350 STOP: 00/00/00 *»
** CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ40
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
1OUJ	1.3-DICHLOROBENZENE
1OUJ	1,4-DICHLOROBENZENE
10UJ	1.2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-JMETHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1,2,4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHLOROANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHLORO-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2,4.6-TRICHLOROPHENOL
25UJ	2,4,5-TRICHL0R0PHEN0L
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ 3-NITROANILINE
10UJ ACENAPHTHENE
25UJ	2.4-DINITROPHENOL
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2,4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4.6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BROMOPHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
*»'REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI! iGEMENT SYSTEM
EPA-REGION IV t. ATHENS. GA.	1i. 93
EXTRACTABLE ORGANICS DATA REPORT
•• PROJECT
•~ SOURCE:
»» STATION
NO. 94-0036 SAMPLE NO. 80532
TOWER CHEMICAL
ID: 520-SW
SAMPLE TYPE. SURFACEWA
PROG ELEM. SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER ••
ST: FL »•
1350 STOP: 00/00/00 ••
•* CASE NO.
21073
SAS NO.: 8175D
D. NO.: F041
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10U J	1.3-DICHLOROBENZENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2,2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHENOL
10UJ	1,2.4-TRICHLOROBENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHL0R0-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2,4,6-TRICHL0R0PHEN0L
25UJ	2,4.5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2.6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITR0PHEN0L
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2.4-DINITR0T0LUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NIT ROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BR0M0PHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3.3'-DICHLOROBENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZO(B AND/OR K)FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2,3-CD) PYRENE
10UJ	DIBENZOlA,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
**'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ES. . THENS, GA.	12/
EXTRACTABLE ORGANICS DATA REPORT
** PROJECT
*• SOURCE:
** STATION
NO. 94-0036 SAMPLE NO. 80533
TOWER CHEMICAL
ID: 121-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER »•
ST: FL **
1830 STOP: 00/00/00 **
•• CASE NO.
21073
SAS NO.: 8175D
0. NO.: FQ42
* *
UG/L	ANALYTICAL RESULTS
10UJ	PHENOL
10UJ	BIS(2-CHLOROETHYL) ETHER
10UJ	2-CHLOROPHENOL
10UJ	1.3-DICHLOROBENZENE
10UJ	1.4-DICHL0R0BENZENE
10UJ	1,2-DICHLOROBENZENE
10UJ	2-METHYLPHENOL
10UJ	2.2'-CHLOROISOPROPYLETHER
10UJ	(3-AND/OR 4-)METHYLPHEN0L
10UJ	N-NITROSODI-N-PROPYLAMINE
10UJ	HEXACHLOROETHANE
10UJ	NITROBENZENE
10UJ	ISOPHORONE
10UJ	2-NITROPHENOL
10UJ	2.4-DIMETHYLPHENOL
10UJ	BIS(2-CHLOROETHOXY) METHANE
10UJ	2.4-DICHLOROPHE NOL
10UJ	1.2.4-TRICHL0R0BENZENE
10UJ	NAPHTHALENE
10UJ	4-CHL0R0ANILINE
10UJ	HEXACHLOROBUTADIENE
10UJ	4-CHLORO-3-METHYLPHENOL
10UJ	2-METHYLNAPHTHALENE
10UJ	HEXACHLOROCYCLOPENTADIENE (HCCP)
10UJ	2,4.6-TRICHLOROPHENOL
25UJ	2,4.5-TRICHLOROPHENOL
10UJ	2-CHLORONAPHTHALENE
25UJ	2-NITROANILINE
10UJ	DIMETHYL PHTHALATE
10UJ	ACENAPHTHYLENE
10UJ	2,6-DINITROTOLUENE
UG/L	ANALYTICAL RESULTS
25UJ	3-NITROANILINE
10UJ	ACENAPHTHENE
25UJ	2.4-DINITR0PHEN0L
25UJ	4-NITROPHENOL
10UJ	DIBENZOFURAN
10UJ	2.4-DINITROTOLUENE
10UJ	DIETHYL PHTHALATE
10UJ	4-CHL0R0PHENYL PHENYL ETHER
10UJ	FLUORENE
25UJ	4-NITROANILINE
25UJ	2-METHYL-4,6-DINITROPHENOL
10UJ	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
10UJ	4-BROMOPHENYL PHENYL ETHER
10UJ	HEXACHLOROBENZENE (HCB)
25UJ	PENTACHLOROPHENOL
10UJ	PHENANTHRENE
10UJ	ANTHRACENE
10UJ	CARBAZOLE
10UJ	DI-N-BUTYLPHTHALATE
10UJ	FLUORANTHENE
10UJ	PYRENE
10UJ	BENZYL BUTYL PHTHALATE
10UJ	3,3'-DICHL0R0BENZIDINE
10UJ	BENZO(A)ANTHRACENE
10UJ	CHRYSENE
10UJ	BIS(2-ETHYLHEXYL) PHTHALATE
10UJ	DI-N-OCTYLPHTHALATE
10UJ	BENZOCB AND/OR K) FLUORANTHENE
10UJ	BENZO-A-PYRENE
10UJ	INDENO (1.2.3-CD) PYRENE
10UJ	DIBENZO(A,H)ANTHRACENE
10UJ	BENZO(GHI)PERYLENE
«•'REMARKS***	***REMARKS»«*
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRCSUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS	/AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	/93
MISCELLANEOUS EXTRACtABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80533 SAMPLE TYPE	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 121-SW	COLLECTION START: 10/21/93 1830 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ42 MONO: FQ41
ANALYTICAL RESULTS UG/L
60J 3 UNIDENTIFIED COMPOUNDS
•»'REMARKS*•«	•••REMARKS"'
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES*••
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
JAGEMENT SYSTEM
ATHENS. GA.


j/93
** PROJECT NO. 94-0036 SAMPLE NO. 80504
** SOURCE: TOWER CHEMICAL
*» STATION ID: 101-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF
CITY: CLERMONT
COLLECTION START
COLLECTED
10/19/93
BY: B CARTER
ST: FL
1520 STOP: 00/00/00
* *
* *
* *
•• CASE NO.: 21073
SAS NO.: 8175D
D. NO.: FQ11


~ »
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
560UJ
PHENOL
1300U
3-NITROANILINE
560U
BIS(2-CHLOROETHYL) ETHER
560UR
ACENAPHTHENE
560U
2-CHLOROPHENOL
1300U
2.4-DINITROPHENOL
560U
1.3-DICHLOROBENZENE
1300U
4-NITROPHENOL
560U
1.4-DICHLOROBENZENE
560U
DIBENZOFURAN
560U
1,2-DICHLOROBENZENE
560U
2,4-DINITROTOLUENE
560U
2-METHYLPHENOL
560U
DIETHYL PHTHALATE
560U
2.2'-CHLOROISOPROPYLETHER
560U
4-CHL0R0PHENYL PHENYL ETHER
560U
(3-AND/OR 4-)METHYLPHEN0L
560U
FLUORENE
560U
N-NITROSODI-N-PROPYL AMINE
1300U
4-NITR0ANILINE
560U
HEXACHLOROETHANE
1300U
2-METHYL-4,6-DINITROPHENOL
560U
NITROBENZENE
560U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
560U
ISOPHORONE
560U
4-BROMOPHENYL PHENYL ETHER
560U
2-NITROPHENOL
560U
HEXACHLOROBENZENE (HCB)
560UR
2,4-DIMETHYLPHENOL
1300U
PENTACHLOROPHENOL
560U
BIS(2-CHLOROETHOXY) METHANE
560U
PHENANTHRENE
560U
2.4-DICHL0R0PHEN0L
560U
ANTHRACENE
560U
1.2.4-TRICHL0R0BENZENE
560U
CARBAZOLE
560U
NAPHTHALENE
560U
DI-N-BUTYLPHTHALATE
560U
4-CHL0R0ANILINE
560U
FLUORANTHENE
560U
HEXACHLOROBUTADIENE
560U
PYRENE
560U
4-CHL0R0-3-METHYL PHENOL
560U
BENZYL BUTYL PHTHALATE
560U
2-METHYLNAPHTHALENE
560U
3.3'-DICHL0R0BENZIDINE
560U
HEXACHLOROCYCLOPENTADIENE (HCCP)
560U
BENZO(A)ANTHRACENE
560U
2.4,6-TRICHLOROPHENOL
560U
CHRYSENE
1300U
2.4.5-T RICHLOROPHENOL
560U
BIS(2-ETHYLHEXYL) PHTHALATE
560U
2-CHLORONAPHTHALENE
560U
DI-N-OCTYLPHTHALATE
130OU
2-NITROANILINE
560U
BENZO(8 AND/OR K) FLUORANTHENE
560U
DIMETHYL PHTHALATE
560U
BENZO-A-PYRENE
560U
ACENAPHTHYLENE
560U
INDENO (1.2.3-CD) PYRENE
560U
2,6-DINITROTOLUENE
560U
DIBENZO(A.H)ANTHRACENE


560U
BENZO(GHI)PERYLENE


41
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	iEMENT SYSTEM
EPA-REGION IV ES (HENS, GA.	12, 3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80504 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 101-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
D. NO. : FQ1 1	MD NO: FQ11
ANALYTICAL RESULTS UG/KG
1000JN HEXADECANOIC ACID (2 ISOMERS)
40000J 15 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
VAGEMENT SYSTEM
ATHENS. GA.

j/93
»* PROJECT NO. 94-0036 SAMPLE NO. 80502
•• SOURCE: TOWER CHEMICAL
•* STATION ID: 102-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/19/93
BY: B CARTER
ST: FL
1230 STOP: 00/00/00
* *
* *
* *
•• CASE NO.: 21073
SAS NO.: 8175D
D. NO.: FQ09

* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
510UJ
PHENOL
1200U
3-NITR0ANILINE
510U
BIS(2-CHLOROETHYL) ETHER
510UR
ACENAPHTHENE
510U
2-CHLOROPHENOL
1200U
2.4-DINITROPHENOL
510U
1.3-DICHLOROBENZENE
1200U
4-NITROPHENOL
510U
1,4-DICHL0R0BENZENE
510U
DIBENZOFURAN
510U
1,2-DICHL0R0BENZENE
51 OU
2,4-DINITROTOLUENE
510U
2-METHYLPHENOL
510U
DIETHYL PHTHALATE
510U
2.2'-CHLOROISOPROPYLETHER
510U
4-CHLOROPHENYL PHENYL ETHER
510U
(3-AND/OR 4-JMETHYLPHENOL
510U
FLUORENE
510U
N-NITROSODI-N-PROPYLAMINE
1200U
4-NITROANILINE
510U
HEXACHLOROETHANE
1200U
2-METHYL-4.6-DINITROPHENOL
510U
NITROBENZENE
51 OU
N-NITROSODI PHENYLAMINE/DI PHENYLAMINE
51OU
ISOPHORONE
510U
4-BR0M0PHENYL PHENYL ETHER
51OU
2-NITROPHENOL
510U
HEXACHLOROBENZENE (HCBJ
510UR
2,4-DIMETHYLPHENOL
1200U
PENTACHLOROPHENOL
510U
BIS(2-CHL0R0ETH0XY) METHANE
51 OU
PHENANTHRENE
510U
2.4-DICHLOROPHENOL
510U
ANTHRACENE
51 OU
1,2.4-TRICHL0R0BENZENE
51 OU
CARBAZOLE
51 OU
NAPHTHALENE
51 OU
DI-N-BUTYLPHTHALATE
510U
4-CHL0R0ANILINE
510U
FLUORANTHENE
510U
HEXACHLOROBUTADIENE
51 OU
PYRENE
510U
4-CHL0R0-3-METHYLPHENOL
510U
BENZYL BUTYL PHTHALATE
510U
2-METHYLNAPHTHALENE
510U
3.3'-DICHLOROBENZIDINE
51 OU
HEXACHLOROCYCLOPENTADIENE (HCCPJ
510U
BENZO(A)ANTHRACENE
510U
2.4.6-TRICHLOROPHENOL
510U
CHRYSENE
1200U
2.4.5-TRICHLOROPHE NOL
510U
BIS(2-ETHYLHEXYL) PHTHALATE
51 OU
2-CHLORONAPHTHALENE
510U
DI-N-OCTVLPHTHALATE
1200U
2-NITROANILINE
510U
BENZO(B AND/OR K)FLUORANTHENE
510U
DIMETHYL PHTHALATE
510U
BENZO-A-PYRENE
510U
ACENAPHTHYLENE
51 OU
INDENO (1.2.3-CD) PYRENE
510U
2.6-DINITROTOLUENE
510U
DIBENZO(A.H)ANTHRACENE


510U
BENZO(GHI)PERYLENE


36
PERCENT MOISTURE
**'FOOTNOTES*»»
~A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	iEMENt SYSTEM
EPA-REGION IV ES (HENS. GA.	12, J
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80502 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 102-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
D. NO. : FQ09	MD NO: FQ09
ANALYTICAL RESULTS UG/KG
600JNN HEXADECANOIC ACID
40000J 20 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS1	VGEMENT SYSTEM
EPA-REGION IV . ATHENS, GA.	1 /93
EXTRACTABLE ORGANICS DATA REPORT
«* PROJECT
•« SOURCE:
»* STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 103-SD
80500 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER »*
ST: FL •*
1055 STOP: 00/00/00 **
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ07
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
3000UJ
PHENOL
7200U
3-NITROANILINE
3000U
BIS(2-CHLOROETHYL) ETHER
3000UR
ACENAPHTHENE
3000U
2-CHLOROPHENOL
7200U
2.4-DINITROPHENOL
3000U
1.3-DICHLOROBENZENE
7200U
4-N1TROPHENOL
3000U
1.4-DICHLOROBENZENE
3000U
DIBENZOFURAN
3000U
1,2-DICHLOROBENZENE
3000U
2.4-DINITROTOLUENE
3000U
2-METHYLPHENOL
3000U
DIETHYL PHTHALATE
3000U
2.2'-CHLOROISOPROPYLETHER
3000U
4-CHLOROPHENYL PHENYL ETHER
3000U
(3-AND/OR 4-)METHYLPHEN0L
3000U
FLUORENE
3000U
N-NITROSODI-N-PROPYLAMINE
7200U
4-NITROANILINE
3000U
HEXACHLOROETHANE
7200U
2-METHYL-4.6-DINITROPHENOL
3000U
NITROBENZENE
3000U
N-NITROSODI PHENYLAMINE/DI PHENYLAMINE
3000U
ISOPHORONE
3000U
4-BROMOPHENYL PHENYL ETHER
3000U
2-NITROPHENOL
3000U
HEXACHLOROBENZENE (HCB)
3000UR
2,4-DIMETHYLPHENOL
7200U
PENTACHLOROPHENOL
3000U
BIS(2-CHLOROETHOXY) METHANE
3000U
PHENANTHRENE
3000U
2.4-DICHL0R0PHEN0L
3000U
ANTHRACENE
3000U
1,2,4-TRICHL0R0BENZENE
3000U
CARBAZOLE
3000U
NAPHTHALENE
3000U
DI-N-BUTYLPHTHALATE
3000U
4-CHL0R0ANILINE
3000U
FLUORANTHENE
3000U
HEXACHLOROBUTADIENE
3000U
PYRENE
3000U
4-CHLORO-3-METHYLPHENOL
3000U
BENZYL BUTYL PHTHALATE
3000U
2-ME THYLNAPHTHALENE
3000U
3,3'-DICHL0R0BENZIDINE
3000U
HEXACHLOROCYCLOPENTADIENE (HCCP)
30O0U
BENZOlA)ANTHRACENE
3000U
2.4.6-TRICHL0R0PHEN0L
3000U
CHRYSENE
7200U
2,4,5-TRICHL0R0PHEN0L
3000U
BIS(2-ETHYLHEXYL) PHTHALATE
3000U
2-CHLORONAPHTHALENE
3000U
DI-N-OCTYLPHTHALATE
7200U
2-NITROANILINE
3000U
BENZOC B AND/OR K)FLUORANTHENE
3000U
DIMETHYL PHTHALATE
3000U
BENZO-A-PYRENE
3000U
ACENAPHTHYLENE
3000U
INDENO (1.2.3-CD) PYRENE
3000U
2.6-DINITROTOLUENE
3000U
DIBENZOCA,H)ANTHRACENE


3000U
BENZO(GHIJPERYLENE


89
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~ R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI5
EPA-REGION IV t
GEMENT SYSTEM
aTHENS. GA.
J3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80500 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID. 103-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1055 STOP:
D. NO.: F007	MD NO: FQ07
00/00/00
ANALYTICAL RESULTS UG/KG
5000JN HEXADECANOIC ACID
100000J 15 UNIDENTIFIED COMPOUNDS
» » « FOOTNOTES* *•
•A-AVERAGE VALUE »NA-NOT ANALYZED 'NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E-
GEMENT SYSTEM
ATHENS, GA.

12,
J3
~* PROJECT NO. 94-0036 SAMPLE NO. 80506
•• SOURCE: TOWER CHEMICAL
»* STATION ID: 104-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER
ST: FL
1735 STOP: 00/00/00

* *
* *
* *
»» CASE NO.: 21073
SAS NO.: 8175D
D. NO.: FQ13


* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
520UJ
PHENOL
1300U
3-NITR0ANILINE
520U
BIS(2-CHLOROETHYL) ETHER
520UR
ACENAPHTHENE
520U
2-CHLOROPHENOL
1300U
2.4-DINITR0PHEN0L
520U
1.3-DICHL0R0BENZENE
1300U
4-NITROPHENOL
520U
1.4-DICHLOROBENZENE
520U
DIBENZOFURAN
520U
1,2-DICHL0R0BENZENE
520U
2.4-DINITR0T0LUENE
520U
2-METHYLPHEN0L
520U
DIETHYL PHTHALATE
520U
2.2'-CHLOROISOPROPYLETHER
520U
4-CHLOROPHENYL PHENYL ETHER
520U
(3-AND/OR 4-JMETHYLPHENOL
520U
FLUORENE
520U
N-NITROSODI-N-PROPYLAMINE
1300U
4-NITROANILINE
520U
HEXACHLOROETHANE
1300U
2-ME THYL-4,6-DINITROPHENOL
520U
NITROBENZENE
520U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
520U
ISOPHORONE
520U
4-BROMOPHENYL PHENYL ETHER
520U
2-NITROPHENOL
520U
HEXACHLOROBENZENE (HCB)
520UR
2.4-DIMETHYLPHENOL
1300U
PENTACHLOROPHENOL
520U
BIS(2-CHL0R0ETH0XY) METHANE
520U
PHENANTHRENE
520U
2,4-DICHLOROPHENOL
520U
ANTHRACENE
520U
1,2.4-TRICHLOROBENZENE
520U
CARBAZOLE
520U
NAPHTHALENE
520U
DI-N-BUTYLPHTHALATE
520U
4-CHLOROANILINE
520U
FLUORANTHENE
520U
HEXACHLOROBUTADIENE
520U
PYRENE
520U
4-CHL0R0-3-METHYLPHEN0L
520U
BENZYL BUTYL PHTHALATE
520U
2-METHYLNAPHTHALENE
520U
3,3'-DICHLOROBENZIDINE
520U
HEXACHLOROCYCLOPENTADIENE (HCCP)
520U
BENZO(A)ANTHRACENE
520U
2.4.6-TRICHLOROPHENOL
520U
CHRYSENE
1300U
2.4.5-TRICHLOROPHENOL
520U
BIS(2-ETHYLHEXYL) PHTHALATE
520U
2-CHLORONAPHTHALENE
520U
DI-N-OCTVLPHTHALATE
1300U
2-NITROANILINE
520U
BENZO(B AND/OR K)FLUORANTHENE
520U
DIMETHYL PHTHALATE
520U
BENZO-A-PYRENE
520U
ACENAPHTHYLENE
520U
INDENO (1.2.3-CD) PYRENE
520U
2.6-DINITROTOLUENE
520U
DIBENZO(A.H)ANTHRACENE


520U
BENZO(GHI)PERYLENE


37
PERCENT MOISTURE
«*•FOOTNOTES*••
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV E. IHENS. GA.	12 3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80506 SAMPLE TYPE: SOIL
SOURCE. TOWER CHEMICAL
STATION ID: 104-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP: 00/00/00
D. NO.: FQ13	MD NO: FQ13
ANALYTICAL RESULTS UG/KG
1000JN HEXADECANOIC ACID (2 ISOMERS)
30000J 17 UNIDENTIFIED COMPOUNDS
»*'FOOTNOTES*»•
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
VTHENS. GA.

12,
J3
•« PROJECT NO. 94-0036 SAMPLE NO. 80508
•• SOURCE: TOWER CHEMICAL
•• STATION ID: 105-SD
SAMPLE TYPE. SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER
ST: FL
1800 STOP: 00/00/00

**
**
* *
•» CASE NO.: 21073
SAS NO.: 8175D
D. NO.: FQ15


*9
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
470UJ
PHENOL
1100U
3-NITR0ANILINE
470U
BIS(2-CHLOROETHYL) ETHER
470UR
ACENAPHTHENE
470U
2-CHLOROPHE NOL
1100U
2.4-DINITR0PHEN0L
470U
1.3-DICHLOROBENZENE
1100U
4-NITROPHENOL
470U
1,4-DICHLOROBENZENE
470U
DIBENZOFURAN
470U
1.2-DICHLOROBENZENE
470U
2.4-DINITROTOLUENE
470U
2-METHYLPHENOL
470U
DIETHYL PHTHALATE
470U
2.2'-CHLOROISOPROPYLETHER
470U
4-CHL0R0PHENYL PHENYL ETHER
470U
(3-AND/OR 4-)METHYLPHENOL
470U
FLUORENE
470U
N-NITROSODI-N-PROPYLAMINE
1 100U
4-NITR0ANILINE
470U
HEXACHLOROETHANE
1 100U
2-METHYL-4,6-DINITROPHENOL
470U
NITROBENZENE
470U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
470U
ISOPHORONE
470U
4-BR0M0PHENYL PHENYL ETHER
470U
2-NITROPHENOL
470U
HEXACHLOROBENZENE (HCB)
470UR
2.4-DIMETHYLPHENOL
1100U
PENTACHLOROPHENOL
470U
BIS(2-CHLOROETHOXY) METHANE
470U
PHENANTHRENE
470U
2.4-DICHLOROPHENOL
470U
ANTHRACENE
470U
1.2,4-TRICHLOROBENZENE
470U
CARBAZOLE
470U
NAPHTHALENE
4 70U
DI-N-BUTYLPHTHALATE
470U
4-CHL0R0ANILINE
60J
FLUORANTHENE
470U
HEXACHLOROBUTADIENE
64J
PYRENE
470U
4-CHL0R0-3-METHYLPHEN0L
470U
BENZYL BUTYL PHTHALATE
470U
2-METHYLNAPHTHALENE
470U
3.3'-DICHL0R0BENZIDINE
470U
HEXACHLOROCYCLOPENTADIENE (HCCP)
470U
BENZOlA)ANTHRACENE
470U
2,4.6-TRICHLOROPHENOL
470U
CHRYSENE
1100U
2.4,5-TRICHLOROPHENOL
470U
BIS(2-ETHYLHEXYL) PHTHALATE
470U
2-CHLORONAPHTHALENE
470U
DI-N-OCTYLPHTHALATE
1100U
2-NITROANILINE
470U
BENZO(B AND/OR K)FLUORANTHENE
47 OU
DIMETHYL PHTHALATE
4 70U
BENZO-A-PVRENE
470U
ACENAPHTHYLENE
470U
INDENO (1,2,3-CD) PYRENE
470U
2.6-DINITR0T0LUENE
470U
DIBENZO(A.H)ANTHRACENE


470U
BENZO(GHI)PERYLENE


31
PERCENT MOISTURE
•'•FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST. .GEMENT SYSTEM
EPA-REGION IV E_ ATHENS. GA.	12, ,93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80508 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 105-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
D. NO.: FQ15	MD NO: FQ15
ANALYTICAL RESULTS UG/KG
3000JN HEXADECANOIC ACID (2 ISOMERS)
30000J 18 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1. ,/93
EXTRACTABLE ORGAN1CS DATA REPORT
~• PROJECT
•• SOURCE:
»« STATION
NO. 94-0036 SAMPLE NO. 80509
TOWER CHEMICAL
ID: 106-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER «•
ST: FL ••
1510 STOP: 00/00/00 »*
•• CASE NO.
21073
SAS NO.: 8175D
D NO.: FQ16
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
2700UJ
PHENOL
6600U
3-NITROANILINE
2700U
BIS(2-CHLOROETHYL) ETHER
2700UR
ACENAPHTHENE
2700U
2-CHLOROPHENOL
6600U
2,4-DINITROPHENOL
2700U
1.3-DICHLOROBENZENE
6600U
4-NITROPHENOL
2700U
1 .4-DICHLOROBENZENE
2700U
DIBENZOFURAN
2700U
1,2-DICHLOROBENZENE
2700U
2,4-DINITROTOLUENE
27O0U
2-METHYLPHENOL
2700U
DIETHYL PHTHALATE
2700U
2.2'-CHLOROISOPROPYLE THE R
2700U
4-CHL0R0PHENYL PHENYL ETHER
2700U
(3-AND/OR 4-)METHYLPHEN0L
2700U
FLUORENE
2700U
N-NITROSODI-N-PROPYLAMINE
6600U
4-NITROANILINE
2700U
HEXACHLOROETHANE
6600U
2-METHYL-4.6-DINITR0PHEN0L
2700U
NITROBENZENE
2700U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2700U
ISOPHORONE
2700U
4-BR0M0PHENYL PHENYL ETHER
2700U
2-NITROPHENOL
2700U
HEXACHLOROBENZENE (HCB)
2700UR
2.4-DIMETHYLPHENOL
6600U
PENTACHLOROPHENOL
2700U
BIS(2-CHLOROETHOXY) METHANE
2700U
PHENANTHRENE
2700U
2.4-DICHLOROPHENOL
2700U
ANTHRACENE
2700U
1,2.4-TRICHLOROBENZENE
2700U
CARBAZOLE
2700U
NAPHTHALENE
2700U
DI-N-BUTYLPHTHALATE
2700U
4-CHL0R0ANILINE
2700U
FLUORANTHENE
2700U
HEXACHLOROBUTADIENE
2700U
PYRENE
2700U
4-CHL0R0-3-METHYLPHEN0L
2700U
BENZYL BUTYL PHTHALATE
2700U
2-METHYLNAPHTHALENE
2700U
3.3'-DICHL0R0BENZIDINE
2700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
2700U
BENZOlAJANTHRACENE
2700U
2.4,6-TRICHLOROPHENOL
2700U
CHRYSENE
6600U
2.4,5-TRICHLOROPHENOL
2700U
BIS(2-ETHYLHEXYL) PHTHALATE
2700U
2-CHLORONAPHTHALENE
2700U
DI-N-OCTYLPHTHALATE
6600U
2-NITROANILINE
2700V
BENZO(B AND/OR K)FLUORANTHENE
2700U
DIMETHYL PHTHALATE
2700U
BENZO-A-PYRENE
2700U
ACENAPHTHYLENE
2700U
INDENO (1.2.3-CD) PYRENE
2700U
2.6-DINITROTOLUENE
2700U
DIBENZO(A.H)ANTHRACENE


2700U
BENZO(GHI)PERYLENE


88
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV Ei
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
» * • *»»»•»»»•»**»»»,
SOURCE' T0WER4EHEMICALSAMPU ^ 80509 SAMPLE TVPE: S0IL
STATION ID: 106-SD
CASE.MO.: 21073	SAS NO.: 8t750
» » «
GEMENT SYSTEM
ATHENS. GA.
C rrv: ^CLE^MONT ^^TeYbV: VcIrXER *''<**
10/20/93 MO^NO: F0f6P: 00/00/00
12/
93
ANALYTICAL RESULTS UG/K.G
20000JN BICYCLOTRIMETHYLHEPTANONE uETuul CTUV1 .
»* OCTAHYDROMETHYLMETHYLENE (METHYLETHYL)
7000JN TETRAHYDRODIMETHYL(METHYLETHYL)NAPHTHALENE
10000JN HEXADECANOIC ACID
200000J 17 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANlCS DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV L
4GEMENT SYSTEM
ATHENS. GA.

1.
93
•• PROJECT NO. 94-0036 SAMPLE NO. 80511
•• SOURCE: TOWER CHEMICAL
«• STATION ID: 108-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER
ST: FL
1715 STOP. 00/00/00

» *
• •
* *
•• CASE NO.: 21073
SAS NO.: 8175D
D. NO.: F018


* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
590UJ
PHENOL
1400U
3-NITR0ANILINE
590U
BIS(2-CHLOROETHYL) ETHER
590UR
ACENAPHTHENE
590U
2-CHLOROPHENOL
1400U
2.4-DINITROPHENOL
590U
1.3-DICHLOROBENZENE
1400U
4-NITROPHENOL
590U
1.4-DICHLOROBENZENE
590U
DIBENZOFURAN
590U
1,2-DICHLOROBENZENE
590U
2.4-DINITROTOLUENE
590U
2-METHYLPHENOL
590U
DIETHYL PHTHALATE
590U
2.2'-CHLOROISOPROPYLETHER
590U
4-CHLOROPHENYL PHENYL ETHER
590U
(3-AND/OR 4-)METHYLPHEN0L
590U
FLUORENE
590U
N-NITROSODI-N-PROPYLAMINE
1400U
4-NITROANILINE
590U
HEXACHLOROETHANE
1400U
2-ME THYL-4.6-DINITROPHENOL
590U
NITROBENZENE
590U
N-NITROSODI PHENYLAMINE/DI PHENYLAMINE
590U
ISOPHORONE
590U
4-BR0M0PHENYL PHENYL ETHER
590U
2-NITROPHENOL
590U
HEXACHLOROBENZENE (HCB)
590UR
2,4-DIMETHYLPHENOL
1400U
PENTACHLOROPHENOL
590U
BIS(2-CHLOROETHOXY) METHANE
590U
PHENANTHRENE
590U
2.4-DICHL0R0PHEN0L
590U
ANTHRACENE
590U
1,2.4-TRICHL0R0BENZENE
590U
CARBAZOLE
590U
NAPHTHALENE
590U
DI-N-BUTYLPHTHALATE
590U
4-CHLOROANILINE
590U
FLUORANTHENE
590U
HEXACHLOROBUTADIENE
590U
PYRENE
590U
4-CHLORO-3-ME THYL PHENOL
590U
BENZYL BUTYL PHTHALATE
590U
2-METHYLNAPHTHALENE
590U
3.3'-DICHL0R0BENZIDINE
590U
HEXACHLOROCYCLOPENTADIENE (HCCP)
590U
BENZ0(A)ANTHRACENE
590U
2,4.6-TRICHLOROPHENOL
590U
CHRYSENE
1400U
2.4.5-TRICHLOROPHENOL
590U
BIS(2-ETHYLHEXYL) PHTHALATE
590U
2-CHLORONAPHTHALENE
590U
DI-N-OCTYLPHTHALATE
1400U
2-NITROANILINE
590U
BENZO(B AND/OR K)FLUORANTHENE
590U
DIMETHYL PHTHALATE
590U
BENZO-A-PYRENE
590U
ACENAPHTHYLENE
590U
INDENO (1.2.3-CD) PYRENE
590U
2.6-DINITROTOLUENE
590U
DIBENZO(A.H)ANTHRACENE


590U
BENZO(GHI)PERYLENE


44
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ESw ATHENS. GA.
12/ , 93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
*»**«»»»*»*»**»««»»*»»**»»»»*•
PROJECT NO. 94-0036 SAMPLE NO. 80511 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 108-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
D NO : FQ18	MD NO: FQ18
ANALYTICAL RESULTS UG/KG
4000JN HEXADECANOIC ACID (2 ISOMERS)
20000J 19 UNIDENTIFIED COMPOUNDS
• ••FOOTNOTES*"
•A-AVERAGE VALUE 'NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSE .GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.	1;. 93
EXTRACTABLE ORGANICS DATA REPORT
•• PROJECT
»~ SOURCE:
STATION
NO. 94-0036 SAMPLE NO. 80513
TOWER CHEMICAL
ID: 109-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER «*
ST: FL *•
1700 STOP: 00/00/00 •«
»» CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ20
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
3700UJ
PHENOL
8900U
3-NITR0AN1LINE
3700U
BIS(2-CHLOROETHYL) ETHER
3700UR
ACENAPHTHENE
3700U
2-CHLOROPHENOL
8900U
2.4-DINITROPHENOL
3700U
1.3-DICHLOROBENZENE
8900U
4-NIT ROPHE NOL
3700U
1,4-DICHLOROBENZENE
3700U
DIBENZOFURAN
3700U
1,2-DICHLOROBENZENE
3700U
2.4-DINITROTOLUENE
3700U
2-METHYLPHENOL
3700U
DIETHYL PHTHALATE
3700U
2.2'-CHLOROISOPROPYLETHER
3700U
4-CHL0R0PHENYL PHENYL ETHER
3700U
(3-AND/OR 4-)METHYLPHEN0L
3700U
FLUORENE
3700U
N-NITROSODI-N-PROPYLAMINE
8900U
4-NITR0ANILINE
3700U
HEXACHLOROETHANE
8900U
2-METHYL-4.6-DINITROPHENOL
3700U
NITROBENZENE
3700U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
3700U
ISOPHORONE
3700U
4-BROMOPHENYL PHENYL ETHER
3700U
2-NITROPHENOL
3700U
HEXACHLOROBENZENE (HCB)
3700UR
2,4-DIMETHYLPHENOL
8900U
PENTACHLOROPHENOL
3700U
BIS(2-CHLOROETHOXY) METHANE
3700U
PHENANTHRENE
3700U
2.4-DICHL0R0PHEN0L
3700U
ANTHRACENE
3700U
1,2.4-TRICHL0R0BENZENE
3700U
CARBAZOLE
3700U
NAPHTHALENE
3700U
DI-N-BUTYLPHTHALATE
3700U
4-CHL0R0ANILINE
3700U
FLUORANTHENE
3700U
HEXACHLOROBUTADIENE
3700U
PYRENE
3700U
4-CHL0R0-3-METHYL PHENOL
3700U
BENZYL BUTYL PHTHALATE
3700U
2-METHYLNAPHTHALENE
3700U
3.3'-DICHL0R0BENZIDINE
3700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
3700U
BENZO(A)ANTHRACENE
3700U
2.4,6-TRICHL0R0PHEN0L
3700U
CHRYSENE
8900U
2.4.5-T RICHLOROPHENOL
3700U
BIS(2-ETHYLHEXYL) PHTHALATE
3700U
2-CHLORONAPHTHALENE
3700U
DI-N-OCTYLPHTHALATE
8900U
2-NITROANILINE
3700U
BENZOC B AND/OR K)FLUORANTHENE
3700U
DIMETHYL PHTHALATE
3700U
BENZO-A-PYRENE
3700U
ACENAPHTHYLENE
3700U
INDENO (1.2.3-CD) PYRENE
3700U
2,6-DINITROTOLUENE
3700U
DIBENZO(A.H)ANTHRACENE


3700U
BENZO(GHI)PERYLENE


91
PERCENT MOISTURE
«•'FOOTNOTES*««
• A-AVERAliE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
E PA-REG I ON IV Ei. ATHENS, GA.
12, . =33
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
««**««««**«**•»*•»»**»*******»
PROJECT NO. 94-0036 SAMPLE NO. 80513 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 109-SD	_ ^
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/21/93 1700 STOP: 00/00/00
D. NO.: F020	MD NO: F020
3000J
60000J
ANALYTICAL RESULTS UG/KG
HEXADECANOIC ACID (2 ISOMERS)
8 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIt CEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.	Ik ,93
EXTRACTABLE ORGANICS DATA REPORT
** PROJECT
•• SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO. 80514
TOWER CHEMICAL
ID: 110-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL •»
1625 STOP: 00/00/00 «»
•» CASE NO.
21073
SAS KIO. : 8175D
D. NO.: F021
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4100UJ
PHENOL
10000U
3-NITROANILINE
4100U
BIS(2-CHL0R0ETHYL) ETHER
4100UR
ACENAPHTHENE
4100U
2-CHL0R0PHEN0L
10000U
2.4-DINITROPHENOL
4100U
1,3-DICHL0R0BENZENE
10000U
4-NITROPHENOL
410OU
1.4-DICHL0R0BENZENE
4100U
DIBENZOFURAN
4100U
1,2-DICHLOROBENZENE
4100U
2.4-DINITROTOLUENE
4100U
2-ME THYLPHENOL
4100U
DIETHYL PHTHALATE
4100U
2.2'-CHLOROISOPROPYLETHER
4100U
4-CHL0R0PHENYL PHENYL ETHER
4100U
(3-AND/OR 4-)METHYLPHENOL
4100U
FLUORENE
4100U
N-NIT ROSODI-N-PROPYLAMINE
10000U
4-NITROANILINE
4100U
HEXACHLOROETHANE
10000U
2-METHYL-4.6-DINITROPHENOL
4100U
NITROBENZENE
4100U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4100U
1S0PH0R0NE
4100U
4-BR0M0PHENYL PHENYL ETHER
4100U
2-NITROPHENOL
4100U
HEXACHLOROBENZENE (HCB)
4100UR
2.4-DIMETHYLPHENOL
10000U
PENTACHLOROPHENOL
4100U
BIS(2-CHLOROETHOXY) METHANE
4100U
PHENANTHRENE
4100U
2.4-DICHLOROPHE NOL
4100U
ANTHRACENE
4100U
1,2.4-TRICHLOROBENZENE
4100U
CARBAZOLE
4100U
NAPHTHALENE
4100U
DI-N-BUTYLPHTHALATE
4100U
4-CHLOROANILINE
4100U
FLUORANTHENE
4100U
HE XACHLOROBUTADIENE
4100U
PYRENE
4100U
4-CHL0R0-3-METHYLPHEN0L
4100U
BENZYL BUTYL PHTHALATE
4100U
2-METHYLNAPHTHALENE
4100U
3.3'-DICHLOROBENZIDINE
4100U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4100U
BENZO(A)ANTHRACENE
4100U
2.4,6-TRICHLOROPHENOL
4100U
CHRYSENE
10000U
2.4.5-T RICHLOROPHE NOL
4100U
BIS(2-ETHYLHEXYL) PHTHALATE
4100U
2-CHLORONAPHTHALENE
4100U
DI-N-OCTYLPHTHALATE
10000U
2-NITROANILINE
4100U
BENZO(B AND/OR K)FLUORANTHENE
4100U
DIMETHYL PHTHALATE
4100U
BENZO-A-PYRENE
4100U
ACENAPHTHYLENE
4100U
INDENO (1,2.3-CD) PYRENE
4100U
2,6-DINITROTOLUENE
4100U
DIBENZO(A,H)ANTHRACENE


4100U
BENZO(GHI)PERYLENE


92
PERCENT MOISTURE
»««FOOTNOTES**»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESIIMAUD VALUE *N-PRESUMPTIVE EVIDENCE Oh PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS jEMENT SYSTEM
EPA-REGION IV ES^ .-.THENS, GA.	12/ j3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80514 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 110-SD
CASE NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP: 00/00/00
D NO : FQ21	MD NO: FQ21
ANALYTICAL RESULTS UG/KG
20000J 3 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI HGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	1. 93
EXTRACTABLE ORGANICS DATA REPORT
•» PROJECT
•• SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID. 111-SD
80515 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER •*
ST: FL ••
1718 STOP. 00/00/00 *»
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ22
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4100UJ
PHENOL
9800U
3-NITROANILINE
4100U
BIS(2-CHLOROETHYL) ETHER
4100UR
ACENAPHTHENE
4100U
2-CHL0R0PHE NOL
9800U
2.4-DINITROPHENOL
4100U
1.3-DICHLOROBENZENE
9800U
4-NITROPHENOL
4100U
1,4-DICHL0R0BENZENE
4100U
DIBENZOFURAN
4100U
1.2-DICHL0R0BENZENE
4100U
2.4-DINITROTOLUENE
4100U
2-METHYLPHEN0L
4100U
DIETHYL PHTHALATE
4100U
2.2'-CHLOROISOPROPYLETHER
4100U
4-CHL0R0PHENYL PHENYL ETHER
4100U
(3-AND/OR 4-)METHYLPHEN0L
4100U
FLUORENE
4100U
N-NITROSODI-N-PROPYLAMINE
9800U
4-NITROANILINE
4100U
HEXACHLOROETHANE
9800U
2-METHYL-4,6-DINITROPHENOL
4100U
NITROBENZENE
4100U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
41001)
ISOPHORONE
4100U
4-BROMOPHENYL PHENYL ETHER
4100U
2-NITROPHENOL
4100U
HEXACHLOROBENZENE (HCB)
4100UR
2.4-DIMETHYLPHENOL
9800U
PENTACHLOROPHENOL
4100U
BIS(2-CHLOROETHOXY) METHANE
4100U
PHENANTHRENE
4100U
2.4-DICHLOROPHENOL
4100U
ANTHRACENE
4100U
1,2.4-TRICHLOROBENZENE
4100U
CARBAZOLE
4100U
naphthalene
4100U
DI-N-BUTYLPHTHALATE
4100U
4-CHL0R0ANILINE
4100U
FLUORANTHENE
4100U
HE XACHLOROBUTADIENE
4100U
PYRENE
4100U
4-CHL0R0-3-METHYLPHEN0L
4100U
BENZYL BUTYL PHTHALATE
4100U
2-METHYLNAPHTHALENE
4100U
3.3'-DICHL0R0BENZIDINE
4100U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4100U
BENZO(AJANTHRACENE
4100U
2.4,6-TRICHLOROPHENOL
4100U
CHRYSENE
9800U
2.4,5-TRICHLOROPHENOL
4100U
BIS(2-ETHYLHEXYL) PHTHALATE
4100U
2-CHLORONAPHTHALENE
4100U
DI-N-OCTYLPHTHALATE
9800U
2-NITROANILINE
4100U
BENZOCB AND/OR K)FLUORANTHENE
4100U
DIMETHYL PHTHALATE
4100U
BENZO-A-PYRENE
4100U
ACENAPHTHYLENE
4100U
INDENO (1.2.3-CD) PYRENE
4100U
2,6-DINITROTOLUENE
4100U
DIBENZO(A.H)ANTHRACENE


4100U
BENZO(GHI)PERYLENE


92
PERCENT MOISTURE
••'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES. (HENS, GA.	12/ 3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80515 SAMPLE TYPE: SOIL
SOURCE. TOWER CHEMICAL
STATION ID: 111-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1718 STOP: 00/00/00
D. NO.: FQ22	MD NO: F022
ANALYTICAL RESULTS UG/KG
100000J 18 UNIDENTIFIED COMPOUNDS
»«"FOOTNOTES*»«
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	1. /93
EXTRACTABLE ORGAN!CS DATA REPORT
•• PROJECT
»• SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO. 80516
TOWER CHEMICAL
ID: 112-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/21/93
BY: B CARTER »•
ST: FL ••
1840 STOP: 00/00/00 •»
•• CASE NO.
21073
SAS NO.: 8175D
D. NO.: F023
* •
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
5400UJ
PHENOL
13000U
3-NITROANILINE
5400U
BIS(2-CHL0R0ETHYL) ETHER
5400UR
ACENAPHTHENE
5400U
2-CHLOROPHENOL
13000U
2,4-DINITROPHENOL
5400U
1.3-DICHL0R0BENZENE
13000U
4-NITROPHENOL
5400U
1,4-DICHLOROBENZENE
5400U
DIBENZOFURAN
5400U
1 .2-DICHLOROBENZENE
5400U
2.4-DINITR0T0LUENE
5400U
2-METHYLPHENOL
5400U
DIETHYL PHTHALATE
5400U
2.2'-CHLOROISOPROPYLETHER
5400U
4-CHLOROPHENYL PHENYL ETHER
5400U
(3-AND/OR 4-)METHYLPHEN0L
5400U
FLUORENE
5400U
N-NIT ROSODI-N-PROPYLAMINE
13000U
4-NITROANILINE
5400U
HEXACHLOROETHANE
13000U
2-METHYL-4.6-DINITROPHENOL
5400U
NITROBENZENE
5400U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
5400U
ISOPHORONE
5400U
4-BROMOPHENYL PHENYL ETHER
5400U
2-NITROPHENOL
5400U
HEXACHLOROBENZENE (HCB)
5400UR
2.4-DIMETHYLPHENOL
13000U
PENTACHLOROPHENOL
5400U
BIS(2-CHLOROETHOXY) METHANE
5400U
PHENANTHRENE
5400U
2.4-DICHLOROPHENOL
5400U
ANTHRACENE
5400U
1,2.4-TRICHLOROBENZENE
54001)
CARBAZOLE
5400U
NAPHTHALENE
5400U
DI-N-BUTYLPHTHALATE
5400U
4-CHL0R0ANILINE
5400U
FLUORANTHENE
5400U
HEXACHLOROBUTADIENE
5400U
PYRENE
5400U
4-CHL0R0-3-ME THYLPHENOL
5400U
BENZYL BUTYL PHTHALATE
5400U
2-METHYLNAPHTHALENE
5400U
3.3'-DICHL0R0BENZIDINE
5400U
HEXACHLOROCYCLOPENTADIENE (HCCP)
5400U
BENZ0(A)ANTHRACENE
5400U
2.4,6-TRICHLOROPHENOL
5400U
CHRYSENE
13000U
2.4.5-TRICHLOROPHENOL
5400U
BISC2-ETHYLHEXYL) PHTHALATE
5400U
2-CHLORONAPHTHALENE
5400U
DI-N-OCTYL PHTHALATE
13000U
2-NITROANILINE
5400U
BENZOCB AND/OR K)FLUORANTHENE
5400U
DIMETHYL PHTHALATE
5400U
BENZO-A-PYRENE
5400U
ACENAPHTHYLENE
5400U
INDENO (1,2.3-CD) PYRENE
5400U
2.6-DINITR0T0LUENE
5400U
DIBENZOCA,H)ANTHRACENE


5400U
BENZO(GHI)PERYLENE


94
PERCENT MOISTURE
•••FOOTNOTES*«*
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS MGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	/93
EXTRACTABLE ORGANICS DATA REPORT
•* PROJECT
•• SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO. 80517
TOWER CHEMICAL
ID. 113-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/21/93
BY: B CARTER **
ST: FL *•
1827 STOP: 00/00/00 *»
•* CASE NO.
21073
SAS NO.: 8175D
D. NO.: F024
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
5500UJ
PHENOL
13000U
3-NITR0ANILINE
5500U
BIS(2-CHLOROETHYL) ETHER
5500UR
ACENAPHTHENE
5500U
2-CHLOROPHENOL
13000U
2.4-DINITROPHENOL
5500U
1,3-DICHLOROBENZENE
13000U
4-NIT ROPHE NOL
5500U
1.4-DICHL0R0BENZENE
5500U
DIBENZOFURAN
5500U
1.2-DICHL0R0BENZENE
5500U
2,4-DINITR0T0LUENE
5500U
2-METHYLPHEN0L
5500U
DIETHYL PHTHALATE
5500U
2.2'-CHLOROISOPROPYLETHER
5500U
4-CHL0R0PHENYL PHENYL ETHER
5500U
(3-AND/OR 4-JMETHYLPHENOL
5500U
FLUORENE
5500U
N-NITROSODI-N-PROPYLAMINE
13000U
4-NITROANILINE
5500U
HEXACHLOROETHANE
13000U
2-METHYL-4,6-DINITR0PHEN0L
5500U
NITROBENZENE
5500U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
5500U
ISOPHORONE
5500U
4-BR0M0PHENYL PHENYL ETHER
5500U
2-NITROPHENOL
5500U
HEXACHLOROBENZENE (HCB)
5500UR
2,4-DIME THYLPHENOL
13000U
PENTACHLOROPHENOL
5500U
BIS(2-CHL0R0ETH0XY) METHANE
5500U
PHENANTHRENE
5500U
2.4-DICHLOROPHENOL
5500U
ANTHRACENE
5500U
1,2.4-TRICHL0R0BENZENE
5500U
CARBAZOLE
5500U
NAPHTHALENE
5500U
DI-N-BUTYLPHTHALATE
5500U
4-CHL0R0ANILINE
5500U
FLUORANTHENE
5500U
HEXACHLOROBUTADIENE
5500U
PYRENE
5500U
4-CHLORO-3-ME THYL PHENOL
5500U
BENZYL BUTYL PHTHALATE
5500U
2-METHYLNAPHTHALENE
5500U
3.3'-DICHLOROBENZIDINE
5500U
HEXACHLOROCYCLOPENTADIENE (HCCP)
5500U
BENZO(A)ANTHRACENE
5500U
2.4.6-TRICHLOROPHENOL
5500U
CHRYSENE
13000U
2.4,5-TRICHLOROPHENOL
8300U
BIS(2-ETHYLHEXYL) PHTHALATE
5500U
2-CHLORONAPHTHALENE
5500U
DI-N-OCTYLPHTHALATE
13000U
2-NITROANILINE
5500U
BENZO(B AND/OR K)FLUORANTHENE
5500U
DIMETHYL PHTHALATE
5500U
BENZO-A-PYRENE
5500U
ACENAPHTHYLENE
5500U
INDENO (1.2.3-CD) PYRENE
5500U
2.6-DINITROTOLUENE
5500U
DIBENZO(A.H)ANTHRACENE


5500U
BENZO(GHI)PERYLENE


94
PERCENT MOISTURE
*•»FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV El .THENS. GA.	12 ,3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80517 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 113-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1827 STOP- 00/00/00
D. NO. : FQ24	MD NO: FQ24
ANALYTICAL RESULTS UG/KG
2000JN HEXADECANOIC ACID
30000J 2 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE •NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.	li. 93
EXTRACTABLE ORGANICS DATA REPORT
»» PROJECT
SOURCE:
«• STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 114-SD
80518 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/21/93
BY: B CARTER »•
ST: FL •*
1813 STOP: 00/00/00 *»
»* CASE NO.
21073
SAS NO.: 8175D
D. NO.: F025
• •
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
6500UJ
PHENOL
16000U
3-NITR0ANILINE
6500U
BIS(2-CHLOROETHYL) ETHER
6500UR
ACENAPHTHENE
6500U
2-CHLOROPHENOL
16000U
2.4-DINITROPHENOL
6500U
1,3-DICHLOROBENZENE
16000U
4-NITROPHENOL
6500U
1.4-DICHLOROBENZENE
6500U
DIBENZOFURAN
6500U
1,2-DICHLOROBENZENE
6500U
2,4-DINITROTOLUENE
6500U
2-METHYLPHENOL
6500U
DIETHYL PHTHALATE
6500U
2,2'-CHL0R0IS0PR0PYLETHER
6500U
4-CHL0R0PHENYL PHENYL ETHER
6500U
(3-AND/OR 4-)METHYLPHEN0L
6500U
FLUORENE
6500U
N-NITROSODI-N-PROPYLAMINE
16000U
4-NITROANILINE
6500U
HEXACHLOROETHANE
16000U
2-METHYL-4,6-DINITROPHENOL
6500U
NITROBENZENE
6500U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
6500U
ISOPHORONE
6500U
4-BR0M0PHENYL PHENYL ETHER
6500U
2-NITROPHENOL
6500U
HEXACHLOROBENZENE (HCB)
6500UR
2.4-DIMETHYLPHENOL
16000U
PENTACHLOROPHENOL
6500U
BIS(2-CHLOROETHOXY) METHANE
6500U
PHENANTHRENE
6500U
2.4-DICHLOROPHENOL
6500U
ANTHRACENE
6500U
1,2,4-TRICHLOROBENZENE
6500U
CARBAZOLE
6500U
NAPHTHALENE
6500U
DI-N-BUTYLPHTHALATE
6500U
4-CHL0R0ANILINE
6500U
FLUORANTHENE
6500U
HEXACHLOROBUTADIENE
6500U
PYRENE
6500U
4-CHL0R0-3-METHYLPHEN0L
6500U
BENZYL BUTYL PHTHALATE
6500U
2-METHYLNAPHTHALENE
6500U
3,3'-DICHL0R0BENZIDINE
6500U
HE XACHLOROCYCLOPENTADIENE (HCCP)
6500U
BENZO(A)ANTHRACENE
6500U
2.4,6-TRICHLOROPHENOL
6500U
CHRYSENE
16000U
2,4.5-TRICHLOROPHENOL
6500U
BIS(2-ETHYLHEXYL) PHTHALATE
6500U
2-CHLORONAPHTHALENE
6500U
DI-N-OCTYLPHTHALATE
16000U
2-NITROANILINE
6500U
BENZOC B AND/OR K)FLUORANTHENE
6500U
DIMETHYL PHTHALATE
6500U
BENZO-A-PYRENE
6500U
ACENAPHTHYLENE
6500U
INDENO (1.2.3-CD) PYRENE
6500U
2,6-DINITROTOLUENE
6500U
DIBENZO(A.H)ANTHRACENE


6500U
BENZO(GHI)PERYLENE


95
PERCENT MOISTURE
»«•FOOTNOTES*»*
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ESl HENS, GA.	12/
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80518 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/21/93 1813 STOP: 00/00/00
D. NO.¦ FQ25	MD NO: FQ25
ANALYTICAL RESULTS UG/KG
3000JN HEXADECANOIC ACID
90000J 6 UNIDENTIFIED COMPOUNDS
»*'FOOTNOTES*»*
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI'
EPA-REGION IV I
VGEMENT SYSTEM
ATHENS. GA.
93
«»	PROJECT NO. 94-0036 SAMPLE NO. 80521
• *	SOURCE: TOWER CHEMICAL
»~	STATION ID: 115-SD
*•
**	CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/21/93 1230 STOP: 00/00/00
D. NO.: F030
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4700UJ
PHENOL
11000U
3-NITR0ANILINE
4700U
BISC 2-CHLOROETHYL) ETHER
4700UR
ACENAPHTHENE
4700U
2-CHLOROPHENOL
11000U
2.4-DINITR0PHEN0L
4700U
1.3-DICHLOROBENZENE
11000U
4-NIT ROPHE NOL
4700U
1,4-DICHLOROBENZENE
4700U
DIBENZOFURAN
4700U
1,2-DICHLOROBENZENE
4700U
2,4-DINITROTOLUENE
4700U
2-METHYLPHENOL
4700U
DIETHYL PHTHALATE
4700U
2.2'-CHLOROISOPROPYLETHER
4700U
4-CHL0R0PHENYL PHENYL ETHER
4700U
(3-AND/OR 4-)METHYLPHENOL
4700U
FLUORENE
4700U
N-NITROSODI-N-PROPYLAMINE
11000U
4-NITROANILINE
4700U
HEXACHLOROETHANE
11000U
2-ME THYL-4.6-DINITROPHENOL
4700U
NITROBENZENE
4700U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4700U
ISOPHORONE
4700U
4-BROMOPHENYL PHENYL ETHER
4700U
2-NITROPHENOL
4700U
HEXACHLOROBENZENE (HCB)
4700UR
2,4-DIMETHYLPHENOL
11OOOU
PENTACHLOROPHENOL
4700U
BIS(2-CHL0R0ETH0XY) METHANE
4700U
PHENANTHRENE
4700U
2.4-DICHLOROPHE NOL
4700U
ANTHRACENE
4700U
1.2.4-TRICHLOROBENZENE
4700U
CARBAZOLE
4700U
NAPHTHALENE
4700U
D1-N-8UTYLPHTHALATE
4700U
4-CHL0R0ANILINE
4700U
FLUORANTHENE
4700U
HEXACHLOROBUTADIENE
4700U
PYRENE
4700U
4-CHLORO-3-METHYLPHENOL
4700U
BENZYL BUTYL PHTHALATE
4700U
2-METHYLNAPHTHALENE
4700U
3,3'-DICHLOROBENZIDINE
4700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4700U
BENZO(A)ANTHRACENE
4700U
2.4.6-TRICHLOROPHENOL
4700U
CHRYSENE
11000U
2,4,5-TRICHLOROPHENOL
4700U
BIS(2-ETHYLHEXYL) PHTHALATE
4700U
2-CHLORONAPHTHALENE
4700U
DI-N-OCTYLPHTHALATE
11000U
2-NITROANILINE
4700U
BENZO(B AND/OR K)FLUORANTHENE
4700U
DIMETHYL PHTHALATE
4700U
BENZO-A-PYRENE
4700U
ACENAPHTHYLENE
4700U
INDENO (1.2.3-CD) PYRENE
4700U
2,6-DINITROTOLUENE
4700U
DIBENZO(A.H)ANTHRACENE


4700U
BENZO(GHI)PERYLENE


93
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV Ei. JHENS, GA.	12, >3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
»» PROJECT
NO. 94-0036 SAMPLE
NO.
80521 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
*• SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL
»• STATION
ID: 115-SD


COLLECTION START: 10/21/93
1230 STOP: 00/00/00 »*
«« CASE.NO
* *
: 21073 SAS
NO.
: 8175D
D NO.: FQ30
MD NO: F028 ««
* *
ANALYTICAL RESULTS UG/KG
3000JN HEXADECANOIC ACID
200000J 15 UNIDENTIFIED COMPOUNDS
•»'FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS	AGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	,/93
EXTRACTABLE ORGANICS DATA REPORT
»• PROJECT
•* SOURCE:
»• STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 116-SD
80522 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER »•
ST: FL •»
1215 STOP: 00/00/00 •»
*• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ31
» *
UG/KG	ANALYTICAL RESULTS
2300UJ	PHENOL
2300U	BIS(2-CHLOROETHYL) ETHER
2300U	2-CHLOROPHENOL
2300U	1.3-DICHLOROBENZENE
2300U	1,4-DICHL0R0BENZENE
2300U	1.2-DICHLOROBENZENE
2300U	2-METHYLPHENOL
2300U	2,2'-CHLOROISOPROPYLETHER
2300U	(3-AND/OR 4-JMETHYLPHENOL
2300U	N-NITROSODI-N-PROPYLAMINE
230011	HEXACHLOROETHANE
2300U	NITROBENZENE
2300U	ISOPHORONE
2300U	2-NITROPHENOL
2300UR	2.4-DIMETHYLPHENOL
2300U	BIS(2-CHLOROETHOXY) METHANE
2300U	2.4-DICHLOROPHENOL
2300U	1,2,4-TRICHLOROBENZENE
2300U	NAPHTHALENE
2300U	4-CHL0R0ANILINE
2300U	HEXACHLOROBUTADIENE
2300U	4-CHLORO-3-METHYLPHENOL
2300U	2-METHYLNAPHTHALENE
2300U	HEXACHLOROCYCLOPENTADIENE (HCCP)
2300U	2,4,6-TRICHLOROPHENOL
5600U	2,4,5-TRICHLOROPHENOL
2300U	2-CHLORONAPHTHALENE
5600U	2-NITROANILINE
2300U	DIMETHYL PHTHALATE
2300U	ACENAPHTHYLENE
2300U	2.6-DINITR0T0LUENE
UG/KG	ANALYTICAL RESULTS
5600U	3-NITROANILINE
2300UR	ACENAPHTHENE
5600U	2.4-DINITROPHENOL
5600U	4-NIT ROPHE NOL
2300U	DIBENZOFURAN
2300U	2,4-DINITROTOLUENE
2300U	DIETHYL PHTHALATE
2300U	4-CHL0R0PHENYL PHENYL ETHER
2300U	FLUORENE
5600U	4-NITROANILINE
5600U	2-METHYL-4,6-DINITROPHENOL
2300U	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2300U	4-BR0M0PHENYL PHENYL ETHER
2300U	HEXACHLOROBENZENE (HCB)
5600U	PENTACHLOROPHENOL
2300U	PHENANTHRENE
2300U	ANTHRACENE
2300U	CARBAZOLE
2300U	DI-N-BUTYLPHTHALATE
2300U	FLUORANTHENE
2300U	PYRENE
2300U	BENZYL BUTYL PHTHALATE
2300U	3.3'-DICHL0R0BENZIDINE
2300U	BENZO(A)ANTHRACENE
2300U	CHRYSENE
2300U	BIS(2-ETHYLHEXYL) PHTHALATE
2300U	DI-N-OCTYLPHTHALATE
2300U	BENZOt B AND/OR K) FLUORANTHENE
2300U	BENZO-A-PYRENE
2300U	INDENO (1.2.3-CD) PYRENE
2300U	DIBENZO(A.H)ANTHRACENE
2300U	BENZO(GHIJPERYLENE
PERCENT MOISTURE
•~•FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV EL ATHENS, GA.	12, J3
MISCELLANEOUS EXTRACTABLE COMPOUNOS - OATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80522 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 116-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1215 STOP: 00/00/00
D. NO.: FQ31	MD NO: FQ29
ANALYTICAL RESULTS UG/KG
10000JN HEXADECANOIC ACID (2 ISOMERS)
200000J 18 UNIDENTIFIED COMPOUNDS
~••FOOTNOTES**'
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV E. THENS. GA.	12.
EXTRACTABLE ORGANICS DATA REPORT
*~ PROJECT
*» SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO.
TOWER CHEMICAL
ID: 117-SD
80523 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER *»
ST: FL **
1200 STOP: 00/00/00 *«
«• CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ32
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
6500UJ
PHENOL
16000U
3-NITR0ANILINE
6500U
BIS(2-CHLOROETHYL) ETHER
6500UR
ACENAPHTHENE
6500U
2-CHLOROPHENOL
16000U
2,4-DINITROPHENOL
6500U
1.3-DICHLOROBENZENE
16000U
4-NITROPHENOL
6500U
1.4-DICHLOROBENZENE
6500U
DIBENZOFURAN
6500U
1,2-DICHLOROBENZENE
6500U
2,4-DINITR0T0LUENE
6500U
2-METHYLPHENOL
6500U
DIETHYL PHTHALATE
6500U
2,2'-CHLOROISOPROPYLETHER
6500U
4-CHL0R0PHENYL PHENYL ETHER
6500U
(3-AND/OR 4-JMETHYLPHENOL
6500U
FLUORENE
6500U
N-NITROSODI-N-PROPYLAMINE
16000U
4-NITROANILINE
6500U
HEXACHLOROETHANE
16000U
2-METHYL-4,6-DINITR0PHEN0L
6500U
NITROBENZENE
6500U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
6500U
ISOPHORONE
6500U
4-BROMOPHENYL PHENYL ETHER
6500U
2-NITROPHENOL
6500U
HEXACHLOROBENZENE (HCB)
6500UR
2.4-DIMETHYL PHENOL
16000U
PENTACHLOROPHENOL
6500U
BIS(2-CHLOROETHOXY) METHANE
6500U
PHENANTHRENE
6500U
2.4-DICHLOROPHENOL
6500U
ANTHRACENE
6500U
1,2.4-TRICHLOROBENZENE
6500U
CARBAZOLE
6500U
NAPHTHALENE
6500U
DI-N-BUTYLPHTHALATE
6500U
4-CHLOROANILINE
6500U
FLUORANTHENE
6500U
HEXACHLOROBUTADIENE
6500U
PYRENE
6500U
4-CHL0R0-3-METHYLPHEN0L
6500U
BENZYL BUTYL PHTHALATE
6500U
2-METHYLNAPHTHALENE
6500U
3.3'-DICHL0R0BENZIDINE
6500U
HEXACHLOROCYCLOPENTADIENE (HCCP)
6500U
BENZ0(A)ANTHRACENE
6500U
2,4,6-TRICHLOROPHENOL
6500U
CHRYSENE
16000U
2.4.5-TRICHLOROPHENOL
8600U
BIS(2-ETHYLHEXYL) PHTHALATE
6500U
2-CHLORONAPHTHALENE
6500U
DI-N-OCTYLPHTHALATE
16000U
2-NITROANILINE
6500U
BENZOtB AND/OR K)FLUORANTHENE
6500U
DIMETHYL PHTHALATE
6500U
BENZO-A-PYRENE
6500U
ACENAPHTHYLENE
6500U
INDENO (1,2,3-CD) PYRENE
6500U
2,6-DINITROTOLUENE
6500U
DIBENZO(A.H)ANTHRACENE


6500U
BENZO(GHI)PERYLENE


95
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. .THENS, GA.	12 ^3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80523 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 117-SD
CASE.NO.: 21073	SAS NO.: 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO. : FQ32	MD NO: F030
ANALYTICAL RESULTS UG/KG
2000JN HEXADECANOIC ACID
80000J A UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES..
,EMENT SYSTEM
•CHENS, GA.
12/ >3
«« PROJECT NO. 94-0036 SAMPLE NO. 80524
»• SOURCE: TOWER CHEMICAL
«~	STATION ID: 517-SD
• »
»»	CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO.: FQ33
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4700UJ
PHENOL
11000U
3-NITR0ANILINE
470OU
BIS(2-CHLOROETHYL) ETHER
4700UR
ACENAPHTHENE
4700U
2-CHLOROPHENOL
11000U
2,4-DINITR0PHEN0L
4700U
1,3-DICHLOROBENZENE
11000U
4-NITROPHENOL
4700U
1.4-DICHLOROBENZENE
4700U
DIBENZOFURAN
4700U
1,2-DICHLOROBENZENE
4700U
2,4-DINITR0T0LUENE
4700U
2-METHYLPHENOL
4700U
DIETHYL PHTHALATE
4700U
2.2'-CHLOROISOPROPYLE THE R
4700U
4-CHL0R0PHENYL PHENYL ETHER
4700U
(3-AND/OR 4-)METHYLPHEN0L
4700U
FLUORENE
4700U
N-NITROSODI-N-PROPYLAMINE
11000U
4-NITROANILINE
4700U
HEXACHLOROETHANE
11000U
2-METHYL-4.6-DINITROPHENOL
4700U
NITROBENZENE
4700U
N-NITROSODI PHENYLAMINE/DIPHENYLAMINE
4700U
ISOPHORONE
4700U
4-BR0M0PHENYL PHENYL ETHER
4700U
2-NITROPHENOL
4700U
HEXACHLOROBENZENE (HCB)
4700UR
2.4-DIMETHYLPHENOL
11OOOU
PENTACHLOROPHENOL
4700U
BIS(2-CHLOROETHOX Y) METHANE
4700U
PHENANTHRENE
4700U
2.4-DICHLOROPHENOL
4700U
ANTHRACENE
4700U
1,2,4-TRICHL0R0BENZENE
4700U
CARBAZOLE
4700U
NAPHTHALENE
4 700U
DI-N-BUTYLPHTHALATE
4700U
4-CHL0R0ANILINE
4700U
FLUORANTHENE
4700U
HEXACHLOROBUTADIENE
4700U
PYRENE
4700U
4-CHL0R0-3-ME THYLPHENOL
4700U
BENZYL BUTYL PHTHALATE
4700U
2-METHYLNAPHTHALENE
4700U
3.3'-DICHLOROBENZIDINE
4700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4700U
BENZO(A)ANTHRACENE
4700U
2.4.6-TRICHLOROPHENOL
4700U
CHRYSENE
11000U
2,4,5-TRICHLOROPHENOL
4700U
BIS(2-ETHYLHEXYL) PHTHALATE
47001)
2-CHLORONAPHTHALENE
4700U
DI-N-OCTYLPHTHALATE
11000U
2-NITROANILINE
4700U
BENZOCB AND/OR K)FLUORANTHENE
4700U
DIMETHYL PHTHALATE
4700U
BENZO-A-PYRENE
4700U
ACENAPHTHYLENE
4700U
INDENO (1,2.3-CD) PYRENE
4700U
2,6-DINITROTOLUENE
4700U
DIBENZO(A.H)ANTHRACENE


4700U
BENZO(GHI)PERYLENE


93
PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES. (HENS, GA.	12
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80524 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 517-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO.: F033	MD NO: F031
ANALYTICAL RESULTS UG/KG
100000J 6 UNIDENTIFIED COMPOUNDS
••~FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES ^-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST AGEMENT SYSTEM
EPA-REGION IV L- ATHENS, GA.	1«_ ,/93
EXTRACTABLE ORGANICS DATA REPORT
•» PROJECT
•» SOURCE:
•• STATION
NO. 94-0036 SAMPLE NO. 80527
TOWER CHEMICAL
ID: 118-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: tO/21/93
BY: B CARTER »»
ST: FL •«
T445 STOP: 00/00/00 •»
•« CASE NO.
21073
SAS NO.: 8175D
D. NO.: F036
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4700UJ
PHENOL
11000U
3-NITROANILINE
4700U
BIS(2-CHLOROETHYL) ETHER
4700UR
ACENAPHTHENE
4700U
2-CHLOROPHENOL
11OOOU
2.4-DINIT ROPHENOL
4700U
1,3-DICHLOROBENZENE
11000U
4-NITROPHENOL
4700U
1,4-DICHL0R0BENZENE
4700U
DIBENZOFURAN
4700U
1,2-DICHLOROBENZENE
4700U
2.4-DINITR0T0LUENE
4700U
2-METHYLPHENOL
4700U
DIETHYL PHTHALATE
4700U
2.2'-CHLOROISOPROPYLETHER
4700U
4-CHL0R0PHENYL PHENYL ETHER
4700U
(3-AND/OR 4-)METHYLPHEN0L
4700U
FLUORENE
4700U
N-NITROSODI-N-PROPYLAMINE
nooou
4-NITROANILINE
4700U
HEXACHLOROETHANE
11000U
2-METHYL-4.6-DINITROPHENOL
4700U
NITROBENZENE
4700U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4700U
ISOPHORONE
4700U
4-BR0M0PHENYL PHENYL ETHER
4700U
2-NITROPHENOL
4700U
HEXACHLOROBENZENE (HCB)
4700UR
2,4-DIMETHYLPHENOL
11000U
PENTACHLOROPHENOL
4700U
BIS(2-CHLOROETHOXY) METHANE
4700U
PHENANTHRENE
4700U
2,4-DICHLOROPHENOL
4700U
ANTHRACENE
4700U
1.2.4-TRICHL0R0BENZENE
4700U
CARBAZOLE
4700V
NAPHTHALENE
4700U
DI-N-BUTYLPHTHALATE
4700U
4-CHLOROANILINE
4700U
FLUORANTHENE
4700U
HEXACHLOROBUTADIENE
4700U
PYRENE
4700U
4-CHL0R0-3-METHYLPHEN0L
4700U
BENZYL BUTYL PHTHALATE
4700U
2-METHYLNAPHTHALENE
4700U
3.3'-DICHLOROBE NZIDINE
4700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4700U
BENZOlA)ANTHRACENE
4700U
2.4.6-TRICHLOROPHENOL
4700U
CHRYSENE
11000U
2.4.5-TRICHLOROPHENOL
4700U
BIS(2-ETHYLHEXYL) PHTHALATE
4700U
2-CHLORONAPHTHALENE
4700U
DI-N-OCTYLPHTHALATE
11000U
2-NITROANILINE
4700V
BENZOCB AND/OR K)FLUORANTHENE
4700U
DIMETHYL PHTHALATE
4700U
BENZO-A-PYRENE
4700U
ACENAPHTHYLENE
4700U
INDENO (1.2.3-CD) PYRENE
4 700U
2,6-DINITROTOLUENE
4700U
DIBENZO(A,H)ANTHRACENE


4700U
BENZO(GHI)PERYLENE


93
PERCENT MOISTURE
• ••FOOTNOTES'"
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. aTHENS. GA.	12, J3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80527 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 118-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/21/93 1445 STOP: 00/00/00
D. NO.: FQ36	MD NO: FQ34
ANALYTICAL RESULTS UG/KG
30000J 2 UNIDENTIFIED COMPOUNDS
~••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
.THENS, GA.
1£.
J3
»»	PROJECT NO. 94-0036 SAMPLE NO. 80528
••	SOURCE: TOWER CHEMICAL
*»	STATION ID: 119-SD
*•
«»	CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 81750
PROG ELEM: SSF COLLECTED	BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1430 STOP:
D. NO.: FQ37
00/00/00
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
4100UJ
PHENOL
lOOOOU
3-NITR0ANILINE
4100U
BIS(2-CHLOROETHYL) ETHER
4100UR
ACENAPHTHENE
4100U
2-CHLOROPHENOL
10000U
2.4-DINITR0PHEN0L
4100U
1.3-DICHLOROBENZENE
10000U
4-NITROPHENOL
4100U
1.4-DICHL0R0BENZENE
4100U
DIBENZOFURAN
4100U
1.2-DICHL0R0BENZENE
4100U
2.4-DINITROTOLUENE
4100U
2-METHYLPHENOL
4100U
DIETHYL PHTHALATE
4100U
2.2'-CHLOROISOPROPYLETHER
4100U
4-CHLOROPHENYL PHENYL ETHER
4100U
(3-AND/OR 4-)METHYLPHEN0L
4100U
FLUORENE
4100U
N-NITROSODI-N-PROPYLAMINE
10000U
4-NITROANILINE
4100U
HEXACHLOROETHANE
10000U
2-METHYL-4.6-DINITROPHENOL
4100U
NITROBENZENE
4100U
N-NITROSODIPHENYLAMINE/DI PHENYLAMINE
4100U
ISOPHORONE
4100U
4-BR0M0PHENYL PHENYL ETHER
4100U
2-NITROPHENOL
4100U
HEXACHLOROBENZENE (HCB)
4100UR
2.4-DIMETHYLPHENOL
10000U
PENTACHLOROPHENOL
4100U
BIS(2-CHLOROETHOXY) METHANE
4100U
PHENANTHRENE
4100U
2.4-DICHL0R0PHEN0L
4100U
ANTHRACENE
4100U
1.2.4-TRICHL0R0BENZENE
4100U
CARBAZOLE
410OU
NAPHTHALENE
4100U
DI-N-BUTYLPHTHALATE
4100U
4-CHL0R0ANILINE
4100U
FLUORANTHENE
4100U
HEXACHLOROBUT ADIENE
4100U
PYRENE
4100U
4-CHL0R0-3-METHYLPHEN0L
4100U
BENZYL BUTYL PHTHALATE
4100U
2-METHYLNAPHTHALENE
4100U
3.3'-DICHLOROBENZIDINE
4100U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4100U
BENZO(A)ANTHRACENE
4100U
2.4.6-TRICHL0R0PHEN0L
4100U
CHRYSENE
10000U
2.4.5-TRICHLOROPHENOL
4100U
BIS(2-ETHYLHEXYL) PHTHALATE
4100U
2-CHLORONAPHTHALENE
4100U
DI-N-OCTYLPHTHALATE
10000U
2-NITROANILINE
4100U
BENZO(B AND/OR K) FLUORANTHENE
4100U
DIMETHYL PHTHALATE
4100U
BENZO-A-PYRENE
4100U
ACENAPHTHYLENE
4100U
INDENO (1.2.3-CD) PYRENE
4100U
2,6-DINITROTOLUENE
4100U
DIBENZO(A.H)ANTHRACENE


4100U
BENZO(GHI)PERYLENE


92
PERCENT MOISTURE
• ••FOOTNOTES*"
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSH GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.	1i. J3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80528 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 119-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1430 STOP: 00/00/00
D. NO.: FQ37	MD NO: F035
ANALYTICAL RESULTS UG/KG
2000JN HEXADECANOIC ACID
60000J 10 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.	,/93
EXTRACTABLE ORGANICS DATA REPORT
«• PROJECT
•• SOURCE:
»• STATION
NO. 94-0036 SAMPLE NO. 80529
TOWER CHEMICAL
ID: 120-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER »»
ST: FL •»
1415 STOP: 00/00/00 •»
*• CASE NO.
21073
SAS NO.: 8175D
D. NO.: F038
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
3700UJ
PHENOL
8900U
3-NITR0ANILINE
3700U
BIS(2-CHLOROETHYL) ETHER
3700UR
ACENAPHTHENE
3700U
2-CHLOROPHENOL
8900U
2 ,4-DINITROPHENOL
3700U
1.3-DICHLOROBENZENE
8900U
4-NITROPHENOL
3700U
1.4-DICHLOROBENZENE
3700U
DIBENZOFURAN
3700U
1.2-DICHLOROBENZENE
3700U
2.4-DINITROTOLUENE
3700U
2-METHYLPHENOL
3700U
DIETHYL PHTHALATE
3700U
2.2'-CHLOROISOPROPYLETHER
3700U
4-CHL0R0PHENYL PHENYL ETHER
3700U
(3-AND/OR 4-)METHYLPHEN0L
3700U
FLUORENE
3700U
N-NITROSODI-N-PROPYLAMINE
8900U
4-NITROANILINE
3700U
HEXACHLOROETHANE
8900U
2-METHYL-4,6-DINITR0PHEN0L
3700U
NITROBENZENE
3700U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
3700U
ISOPHORONE
3700U
4-BROMOPHENYL PHENYL ETHER
3700U
2-NITROPHENOL
3700U
HEXACHLOROBENZENE (HCB)
3700UR
2.4-DIMETHYLPHENOL
8900U
PENTACHLOROPHENOL
3700U
BIS(2-CHL0R0ETH0XY) METHANE
3700U
PHENANTHRENE
3700U
2.4-DICHL0R0PHEN0L
3700U
ANTHRACENE
3700U
1,2,4-TRICHLOROBENZENE
3700U
CARBAZOLE
3700U
NAPHTHALENE
3700U
DI-N-BUTYLPHTHALATE
3700U
4-CHLOROANIL1NE
3700U
FLUORANTHENE
3700U
HEXACHLOROBUTADIENE
3700U
PYRENE
3700U
4-CHL0R0-3-ME THYLPHENOL
3700U
BENZYL BUTYL PHTHALATE
3700U
2-METHYLNAPHTHALENE
3700U
3,3'-DICHLOROBENZIDINE
3700U
HEXACHLOROCYCLOPENTADIENE (HCCP)
3700U
BENZO(A)ANTHRACENE
3700U
2,4.6-TRICHLOROPHENOL
3700U
CHRYSENE
8900U
2,4,5-TRICHLOROPHENOL
3700U
BIS(2-ETHYLHEXYL) PHTHALATE
3700U
2-CHLORONAPHTHALENE
3700U
DI-N-OC.TYL PHTHALATE
8900U
2-NITROANILINE
3700U
BENZO(B AND/OR K)FLUORANTHENE
3700U
DIMETHYL PHTHALATE
3700U
BENZO-A-PYRENE
3700U
ACENAPHTHYLENE
3700U
INDENO (1.2.3-CD) PYRENE
3700U
2,6-DINITR0T0LUENE
3700U
DIBENZO(A.H)ANTHRACENE


3700U
BENZO(GHI)PERYLENE


91
PERCENT MOISTURE
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AMD ANALYSIS
EPA-REGION IV ES.
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80529 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID. 120-SD
CASE.NO.: 21073	SAS NO.: 8175D
iEMENT SYSTEM
CHENS. GA.
*««««»*»«*«*«»«*»»«****»~
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL „ _
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D NO.: FQ38	MD NO: FQ36
12/
30000J
ANALYTICAL RESULTS UG/KG
6 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES*'*
•A-AVERAGE VALUE »NA-N0T ANALYZED •NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS .EMENT SYSTEM
„ _ ..	EPA-REGION IV ESL. .THENS. GA.	12/^3
EXTRACTABLE ORGANICS DATA REPORT
** PROJECT
•• SOURCE:
•» STATION
NO. 94-0036 SAMPLE NO. 80530
TOWER CHEMICAL
ID. 520-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL «»
1415 STOP: 00/00/00 *»
•» CASE NO.
21073
SAS NO.: 8175D
D. NO.: FQ39
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
3700UJ
PHENOL
8900U
3-NITR0ANILINE
3700U
BIS(2-CHLOROETHYL) ETHER
3700UR
ACENAPHTHENE
3700U
2-CHLOROPHENOL
8900U
2.4-DINITROPHENOL
3700U
1.3-DICHLOROBENZENE
8900U
4-NITROPHENOL
3700U
1,4-DICHLOROBENZENE
3700U
DIBENZOFURAN
3700U
1,2-DICHLOROBENZENE
3700U
2 ,4-DINITROTOLUENE
3700U
2-METHYLPHENOL
3700U
DIETHYL PHTHALATE
3700U
2.2'-CHLOROISOPROPYLETHER
3700U
4-CHLOROPHENYL PHENYL ETHER
3700U
(3-AND/OR 4-JMETHYLPHENOL
3700U
FLUORENE
3700U
N-NITROSODI-N-PROPYLAMINE
8900U
4-NITROANILINE
3700U
HEXACHLOROETHANE
8900U
2-METHYL-4,6-DINITR0PHEN0L
3700U
NITROBENZENE
3700U
N-NITROSODI PHENYLAMINE/DIPHENYLAMINE
3700U
ISOPHORONE
3700U
4-BR0M0PHENYL PHENYL ETHER
3700U
2-NITROPHENOL
3700U
HEXACHLOROBENZENE (HCB)
3700UR
2.4-DIMETHYLPHENOL
8900U
PENTACHLOROPHENOL
3700U
BIS(2-CHL0R0ETH0XY) METHANE
3700U
PHENIANTHRENE
3700U
2.4-DICHLOROPHENOL
3700U
ANTHRACENE
3700U
1.2.4-TRICHLOROBENZENE
3700U
CARBAZOLE
3700U
NAPHTHALENE
3700U
DI-N-BUTYLPHTHALATE
3700U
4-CHL0R0ANILINE
3 700U
FLUORANTHENE
3700U
HEXACHLOROBUTADIENE
3700U
PYRENE
3700U
4-CHL0R0-3-METHYLPHENOL
3700U
BENZYL BUTYL PHTHALATE
3700U
2-METHYLNAPHTHALENE
3700U
3.3'-DICHL0R0BENZIDINE
3700U
HE XACHLOROCYCLOPE NT ADIENE (HCCP)
3700U
BENZO(A)ANTHRACENE
3700U
2.4,6-TRICHLOROPHENOL
3700U
CHRYSENE
8900U
2.4.5-TRICHLOROPHENOL
6000U
BIS(2-ETHYLHEXYL) PHTHALATE
3700U
2-CHLORONAPHTHALENE
37001J
DI-N-OCTYLPHTHALATE
8900U
2-NITROANILINE
3700U
BENZOtB AND/OR K)FLUORANTHENE
3700U
DIMETHYL PHTHALATE
3700U
BENZO-A-PYRENE
3700U
ACENAPHTHYLENE
3700U
INDENO (1.2.3-CD) PYRENE
3700U
2.6-DINITROTOLUENE
3700U
DIBENZO(A.H)ANTHRACENE


3700U
BENZO(GHI)PERYLENE


91
PERCENT MOISTURE
*»'FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV Ei. .THENS. GA.	12, >3
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80530 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D NO.: FQ39	MD NO: FQ37
ANALYTICAL RESULTS UG/KG
30000J 4 UNIDENTIFIED COMPOUNDS
•»"FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST'. kGEMENT SYSTEM
EPA-REGION IV t ATHENS, GA.	1i. 93
EXTRACTABLE ORGANICS DATA REPORT
»• PROJECT
«• SOURCE:
»• STATION
NO. 94-0036 SAMPLE NO. 80534
TOWER CHEMICAL
ID: 121-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER »*
ST: FL •*
1830 STOP. 00/00/00 »*
*• CASE NO.
21073
SAS NO.: 8175D
D. NO.: F043
* *
UG/KG	ANALYTICAL RESULTS
430UJ	PHENOL
430U	BIS(2-CHLOROETHYL) ETHER
430U	2-CHLOROPHENOL
430U	1.3-DICHLOROBENZENE
430U	1,4-DICHLOROBENZENE
430U	1,2-DICHLOROBENZENE
430U	2-METHYLPHENOL
430U	2,2'-CHLOROISOPROPYLETHER
430U	(3-AND/OR 4-)METHYLPHEN0L
430U	N-NIT ROSODI-N-PROPYLAMINE
430U	HEXACHLOROETHANE
430U	NITROBENZENE
430U	ISOPHORONE
430U	2-NITROPHENOL
430UR	2,4-DIME THYLPHENOL
430U	BIS(2-CHLOROETHOXY) METHANE
430U	2.4-DICHLOROPHENOL
430U	1,2,4-TRICHLOROBENZENE
430U	NAPHTHALENE
430U	4-CHL0R0ANILINE
430U	HEXACHLOROBUT ADIENE
430U	4-CHL0R0-3-METHYLPHEN0L
4301)	2-METHYLNAPHTHALENE
430U	HEXACHLOROCYCLOPENTADIENE (HCCP)
430U	2.4,6-TRICHLOROPHENOL
1000U	2.4,5-TRICHLOROPHE NOL
430U	2-CHLORONAPHTHALENE
1000U	2-NITROANILINE
430U	DIMETHYL PHTHALATE
430U	ACENAPHTHYLENE
430U	2,6-DINITROTOLUENE
UG/KG	ANALYTICAL RESULTS
1000U	3-NITROANILINE
430UR	ACENAPHTHENE
1000U	2.4-D1N1TROPHENOL
1000U	4-NITROPHENOL
430U	DIBENZOFURAN
430U	2,4-DINITROTOLUENE
430U	DIETHYL PHTHALATE
430U	4-CHLOROPHENYL PHENYL ETHER
430U	FLUORENE
1000U	4-NITROANILINE
1000U	2-METHYL-4,6-DINITROPHENOL
430U	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
430U	4-BROMOPHENYL PHENYL ETHER
430U	HEXACHLOROBENZENE (HCB)
1000U	PENTACHLOROPHENOL
430U	PHENANTHRENE
4SOU	ANTHRACENE
430U	CARBAZOLE
430U	DI-N-BUTYLPHTHALATE
430U	FLUORANTHENE
430U	PYRENE
430U	BENZYL BUTYL PHTHALATE
430U	3.3'-DICHLOROBENZIDINE
430U	BENZO(A)ANTHRACENE
430U	CHRYSENE
430U	BIS(2-ETHYLHEXYL) PHTHALATE
430U	DI-N-OCTYLPHTHALATE
430U	BENZO(B AND/OR K)FLUORANTHENE
430U	BENZO-A-PYRENE
430U	INDENO (1.2.3-CD) PYRENE
430U	DIBENZO(A.H)ANTHRACENE
430U	BENZO(GHI)PERYLENE
24	PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS JAGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	,/93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80534 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 121-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM- SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1830 STOP: 00/00/00
D . NO : FQ43	MD NO: FQ42
ANALYTICAL RESULTS UG/KG
6000J 5 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
*****MEMORANDUM******
DATE: 12/14/93
SUBJECT: Results of Pesticide/PCB Analysis;
9A - 00 3 6 TOWER CHEMICAL
CLERMONT FL
CASE NO: 21073SAS NO: 6175D
FROM: Charles H. Hooper
Chief, Laboratory Evaluation/Quality Assurance Section
TO: DELBERT HICKS
Attached are the results of analysis of samples collected as part of
the subject project.
As a result of the Quality Assurance Review, certain data qualifiers
may have been placed on the data. Attached is a DATA QUALIFIER
REPORT which explains the reasons that these qualifiers were required.
If you have any questions please contact me.
ATTACHMENT
-------
ORGANIC DATA QUALIFIER REPORT
Case Number 21073	Project Number 94-0036
Site ID. Tower Chemical, Clermont, FL
SAS Number
Compound or Fraction
Flag
Used
Reason
Volatiles



all waters
carbon tetrachloride
R
unacceptable blind spike recovery
80500,80511,
80513,80527,
80528,80530
acetone
N
common lab contaminant
80503,80510,
80512,80514,
80515,80517,
80518,80529,
80530
carbon disulfide
J
< quantitation limit
Extractables



all waters
all compounds
J
exceeded extraction holding times
all soils
phenol
acenaphthene
2,4-dimethylphenol
J
R
R
low blind spike recovery
unacceptable blind spike recovery
unacceptable blind spike recovery
80508
fluoranthene
pyrene
J
J
<	quantitation limit
<	quantitation limit
Pesticides



all waters
all compounds
J
exceeded extraction holding times
80500
4,4'-DDD
N
difference in column
quantitations
80521
4,4'-DDE
N
difference in column
quantitations
80534
4,4'-DDE
J
< quantitation limit
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIf iGEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.
1. 93
PROJECT NO. 94-0036 SAMPLE NO. 80503	SAMPLE TYPE: SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL CITY: CLERMONT	ST: FL
STATION ID: 101-SW	COLLECTION START: 10/19/93 1520 STOP: 00/00/00
CASE NUMBER: 21073	SAS NUMBER:	8175D	D. NUMBER: FQ10
UG/L
ANALYTICAL RESULTS
0.050UJ	ALPHA-BHC
0.050UJ	BETA-BHC
0.050UJ	DELTA-BHC
0.050UJ	GAMMA-BHC (LINDANE)
0.050UJ	HEPTACHLOR
0.050UJ	ALDRIN
0.050UJ	HEPTACHLOR EPOXIDE
0.050UJ	ENDOSULFAN I (ALPHA)
0.10UJ	DIELDRIN
0.10UJ	4,4'-DDE (P.P'-DDE)
O.10UJ	ENDRIN
0.10UJ	ENDOSULFAN II (BETA)
0.10UJ	4.4'-DDD (P.P'-DDD)
0 10UJ	ENDOSULFAN SULFATE
0.10UJ	4.4'-DDT (P.P'-DDT)
UG/L
ANALYTICAL RESULTS
0.50UJ	METHOXYCHLOR
0.10UJ	ENDRIN KETONE
0.10UJ	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
0.050UJ	GAMMA-CHLORDANE /2
0 050UJ	ALPHA-CHLORDANE /2
5.0UJ	TOXAPHENE
1.0UJ	PCB-1016 (AROCLOR 1016)
2.0UJ	PCB-1221 (AROCLOR 1221)
1.0UJ	PCB-1232 (AROCLOR 1232)
1.0UJ	PCB-1242 (AROCLOR 1242)
1.0UJ	PCB-1248 (AROCLOR 1248)
1.0UJ	PCB-1254 (AROCLOR 1254)
1.0UJ	PCB-1260 (AROCLOR 1260)
/I
"••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
**'REMARKS*»*
»•* FOOTNOTES* * *
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-fcSTIMAIED VALUE »N-PRESUMPTIVC EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
~C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI! .GEMENT SYSTEM
EPA-REGION IV I ATHENS. GA.	1 J3
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80503 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 101-SW	COLLECTION START: 10/19/93 1520 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ10 MD NO: FQ10
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHL0R0BENZ1LATE
•••REMARKS***	**'REMARKS*»*
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV t
»GEMENT SYSTEM
ATHENS, GA.
93
»* PROJECT NO. 94-0036 SAMPLE NO. 80501
• • SOURCE: TOWER CHEMICAL
*»	STATION ID: 102-SW
»*	CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
D. NUMBER: FQ08
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0. 10UJ
0. 10UJ
0. 10UJ
0. 10UJ
0.10UJ
0.10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0. 10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1	.OUJ
2	. OUJ
1 .OUJ
1 .OUJ
1 OUJ
1 OUJ
1 .OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
GAMMA-CHLORDANE	/2
ALPHA-CHLORDANE	/2
TOXAPHENE
PCB-1016 (AROCLOR	1016)
PCB-1221 (AROCLOR	1221)
PCB-1232 (AROCLOR	1232)
PCB-1242 (AROCLOR	1242)
PCB-1248 (AROCLOR	1248)
PCB-1254 (AROCLOR	1254)
PCB-1260 (AROCLOR	1260)
/1
• ••REMARKS"*	**«RFMARK^**«
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
•••FOOTNOTES*••
«~ArfniPEi/!ffhpE.c	^AhcliDruM..*f{ifr.iNJ^ERENCES '^-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
I°~BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
BUT N0T ^TECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
DATA ""USABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
o	~ — ¦ WHEN N0 VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.	1; J3
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80501 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 102-SW	COLLECTION START: 10/19/93 1230 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D NO.: FQ08 MD NO- FQ08
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZILATE
•••REMARKS***	»*'REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYST.
EPA-REGION IV t.
iGEMENT SYSTEM
ATHENS. GA.
93
«»	PROJECT NO. 94-0036 SAMPLE NO. 80499
••	SOURCE: TOWER CHEMICAL
«»	STATION ID: 103-SW
»*	CASE NUMBER: 21073	SAS NUMBER:
* *
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/19/93 1055 STOP: 00/00/00
D. NUMBER: FQ06
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
D1ELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1 .OUJ
2. OUJ
1 .OUJ
1 OUJ
1 OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/I
»*»REMARKS»»»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•»»REMARKS«»»
• ••FOOTNOTES'"
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS	EMENT SVSTEM
EPA-REGION IV ES. ,HENS, GA.	12/
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80499 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY. CLERMONT ST. FL
STATION ID: 103-SW	COLLECTION START: 10/19/93 1055 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ06 MD NO: FQ06
ANALYTICAL RESULTS UG/L
.10UJ DICOFOL
.10UJ CHLOROBENZILATE
*»»REMARKS**»	*»'REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
»•"FOOTNOTES'••
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
_ . .	^	EPA-REGION IV ES. iTHENS, GA.	12, J3
PESTIClDES/PCB'S DATA REPORT	'
PROJECT NO. 94-0036 SAMPLE NO. 80505	SAMPLE TYPE: SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL CITY: CLERMONT	ST: EL
STATION ID: 104-SW	COLLECTION START. 10/19/93 1735 STOP: 00/00/00
CASE NUMBER: 21073	SAS NUMBER:	8175D	D. NUMBER: FQ12
UG/L
ANALYTICAL RESULTS
0.050UJ	ALPHA-BHC
0.050UJ	BETA-BHC
0.050UJ	DELTA-BHC
0.050UJ	GAMMA-BHC (LINDANE)
0.050UJ	HEPTACHLOR
0.050UJ	ALDRIN
0.050UJ	HEPTACHLOR EPOXIDE
0.050UJ	ENDOSULFAN I (ALPHA)
0.10UJ	DIELDRIN
0.10UJ	4.4'—DDE (P.P'-DDE)
0.10UJ	ENDRIN
0.10UJ	ENDOSULFAN II (BETA)
0.10UJ	4.4'-DDD (P.P'-DDD)
0.10UJ	ENDOSULFAN SULFATE
0.10UJ	4.4'-DDT (P.P'-DDT)
UG/L
O.50U J
0.10UJ
0.10UJ
O.050UJ
0.050UJ
5.0UJ
1	OUJ
2	. OUJ
1 OUJ
1 OUJ
1 OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH.
GAMMA-CHLORDANE
ALPHA-CHLORDANE
TOXAPHENE
PCB-1016 (AROCLOR
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
MIXTURE)
/2
/2
1016)
1221 )
1232)
1242)
1248)
1254)
1260)
/1
»«*remarks»*«
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•»*REMARKS»«»
••'FOOTNOTES*«»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSI! CEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.	K 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80505 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY. CLERMONT ST: FL
STATION ID: 104-SW	COLLECTION START: 10/19/93 1735 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ12 MD NO: FQ12
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZILATE
»»»REMARKS»*»	*»«REMARKS«*»
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES*»»
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI!
EPA-REGION IV E
GEMENT SYSTEM
ATHENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80507
SOURCE: TOWER CHEMICAL
STATION ID: 105-SWM
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM. SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
D. NUMBER: FQ14
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0. 10U
0. 10U
0. 10U
0. 10U
0. 10U
0. 10U
0. 10U
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0 50U
0. 10U
0. 10U
3.050U
0.050U
5.0U
1	.OU
2	OU
1 OU
1 OU
1 OU
1 .OU
1 .OU
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/I
«*'REMARKS*•»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••REMARKS'**
*»'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIJ GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80507 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 105-SWM	COLLECTION START: 10/19/93 1800 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ14 MD NO: F014
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZILATE
••~REMARKS***	***REMARKS**»
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
••	PROJECT NO. 94-0036 SAMPLE NO. 80512 SAMPLE TYPE: SURFACEWA
•*	SOURCE: TOWER CHEMICAL
•»	STATION ID: 106-SW
'«	CASE NUMBER: 21073	SAS NUMBER: 8175D
**
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1600 STOP: 00/00/00
D. NUMBER: FQ19
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0 10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1	.OUJ
2	. OUJ
1 .OUJ
1 OUJ
1 .OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/I
• "REMARKS'"	**'REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
••'FOOTNOTES'•'
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES 'J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
'R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV I ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO. 80512 SAMPLE TYPE: SURFACEWA
PROG ELEM- SSF COLLECTED
BY: B CARTER ••
** SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST. FL *•
** STATION
ID: 106-SW

COLLECTION START: 10/20/93
1600 STOP: 00/00/00 ••
•• CASE.NO
* *
: 21073 SAS
NO.: 8175D
D. NO : FQ19
MD NO: FQ19 «*
* *
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZI LATE
•••REMARKS***	•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26,1984)
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIOES/PCB'S DATA REPORT
SAMPLE AND ANALYST
EPA-REGION IV t
CEMENT SYSTEM
ATHENS, GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80510
SOURCE: TOWER CHEMICAL
STATION ID: 108-SW
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
81750
PROG ELEM: SSF COLLECTED BY: B CARTER
riTV' n FPtintJT	ct- pi
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
D. NUMBER: FQ17
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P,P'-DDT)
UG/L
0.50UJ
0 10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1 .OUJ
2. OUJ
1 OUJ
1 OUJ
1 OUJ
1 .OUJ
1 .OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/1
•»"REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
»»'REMARKS*»»
• ••FOOTNOTES*"
•A-AVERAGE VALUE «NA-NOT ANALY2ED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSIf CEMENT SYSTEM
EPA-REGION IV t ATHENS¦ GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80510 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
•• SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL »•
»• STATION
ID: 108-SW


COLLECTION START: 10/20/93
1715 STOP: 00/00/00 ••
*• CASE.NO
*•
: 21073 SAS
NO.
: 8175D
D. NO.: FQ17
MD NO: FQ17 ••
* *
ANALYTICAL RESULTS UG/L
O.IOUJ DICOFOL
0.10UJ CHLOROBENZILATE
•••REMARKS***	•••REMARKS*"
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•»'FOOTNOTES**»
•A-AVERAGE VALUE "NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PESTlCIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
-------
SAMPLE AND ANALYSI 4GEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80520 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 111-SW	COLLECTION START: 10/20/93 1557 STOP" 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ28 MD NO: FQ27
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
O.10UJ CHLOROBENZILATE
•••REMARKS***	**»REMARKS»**
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NCCC:-ri
-------
PESTlCIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ESI
IMENT SYSTEM
HENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80519
SOURCE: TOWER CHEMICAL
STATION ID: 114-SW
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1803 STOP: 00/00/00
D. NUMBER: FQ26
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4,4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5 . OUJ
1	OUJ
2	OUJ
1 .OUJ
1 .OUJ
1 .OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/1
•»'REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
»«»REMARKS«»»
«••FOOTNOTES*»«
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYST VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
•* PROJECT
NO. 94-0036 SAMPLE
NO.
80519 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
•* SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL •*
• • STATION
ID: 114-SW


COLLECTION START: 10/20/93
1803 STOP: 00/00/00 •*
•* CASE.NO
* *
: 21073 SAS
NO.
: 8175D
D. NO.. FQ26
MD NO: FQ26 »#
* *
ANALYTICAL RESULTS UG/L
O.IOUJ DICOFOL
0.10UJ CHLOROBENZILATE
»»'REMARKS***	»»«REMARKS«*»
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ES.
jEMENT SYSTEM
CHENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80525
SOURCE: TOWER CHEMICAL
STATION ID: 117-SW
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
TTTV* n FPUHKIT	• Fl
COLLECTION START: 10/21/93 1140 STOP: 00/00/00
D. NUMBER: FQ34
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P,P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1	.OUJ
2	. OUJ
1 OUJ
1 OUJ
1 OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH.
GAMMA-CHLORDANE
ALPHA-CHLORDANE
TOXAPHENE
PCB-1016 (AROCLOR
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
MIXTURE)
/2
/2
1016)
1221)
1232)
1242)
1248)
1254)
1260)
/1
• ••REMARKS*"
HOLDING TIMES EXCEEDEDC40 CFR 136,OCTOBER 26.1984)
•••REMARKS***
•*•FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. aTHENS, GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
** PROJECT
NO. 94-0036 SAMPLE
NO.
80525 SAMPLE TYPE: SURFACEWA
PROG ELEM- SSF COLLECTED
BY: B CARTER «•
** SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL **
*• STATION
ID: 117-SW


COLLECTION START: 10/21/93
1140 STOP: 00/00/00 *»
** CASE.NO
* *
: 21073 SAS
NO.
: 8175D
D. NO.: FQ34
MD NO: F032 **
* *
ANALYTICAL RESULTS UG/L
O.IOUJ DICOFOL
O.IOUJ CHLOROBENZILATE
»*'REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
«*'REMARKS***
••~FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E'..
jEMENT SYSTEM
.THENS. GA.
»• PROJECT NO. 94-0036 SAMPLE NO. 80526 SAMPLE TYPE: SURFACEWA
~• SOURCE: TOWER CHEMICAL
»• STATION ID. 517-SW
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/21/93 1140 STOP. 00/00/00
D. NUMBER: FQ35
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0. 10UJ
0. 10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-ODD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5. OUJ
1 .OUJ
2. OUJ
1 .OUJ
1 .OUJ
1 .OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/I
•••REMARKS'**
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
••»REMARKS*••
• ••FOOTNOTES*"
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYST CEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80526 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED	BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST. FL
STATION ID: 517-SW	COLLECTION START: 10/21/93 1140 STOP- 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: F035	MD NO: FQ33
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZILATE
»•'REMARKS*•»	»*'REMARKS*»»
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
• ••FOOTNOTES"*
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV ESl
EMENT SYSTEM
.HENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80531
SOURCE: TOWER CHEMICAL
STATION ID: 120-SW
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1350 STOP: 00/00/00
D. NUMBER: FQ40
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.10UJ
0.10UJ
0.10UJ
0.10UJ
0. 10UJ
0. 10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4,4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5. OUJ
1	.OUJ
2	OUJ
1 .OUJ
1 OUJ
1 OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH.
GAMMA-CHLORDANE
ALPHA-CHLORDANE
TOXAPHENE
PCB-1016 (AROCLOR
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
MIXTURE)
/2
/2
1016)
1221 )
1232)
1242)
1248)
1254)
1260)
/1
••'REMARKS'»•
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
»•'REMARKS*»•
"•FOOTNOTES'"
•A-AVERAGE VALUE 'NA-NOT ANALYZED 'NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSE GEMENT SYSTEM
EPA-REGION IV t VTHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80531 SAMPLE	TYPE: SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 120-SW	COLLECTION START: 10/21/93 1350 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	0. NO.: FQ40 MD NO: FQ38
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHL0R0BEN21LATE
»*»REMARKS»*»	»»»REMARKS«»«
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
* » » FOOTNOTES* » *
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
••(.-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
«R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS I
EPA-REGION IV ESL
:ment system
HENS, GA.
12/
PROJECT NO. 94-0036 SAMPLE NO. 80532
SOURCE: TOWER CHEMICAL
STATION ID: 520-SW
CASE NUMBER: 21073	SAS NUMBER:
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1350 STOP: 00/00/00
D. NUMBER: FQ41
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0. 10UJ
0.10UJ
0.10UJ
0. 10UJ
0.10UJ
0. 10UJ
0.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P,P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P.P'-DDT)
UG/L
0.50UJ
0. 10UJ
0.10UJ
0.050UJ
0.050UJ
5.0UJ
1 .OUJ
2. OUJ
1 .OUJ
1 OUJ
1 .OUJ
1 .OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH.
GAMMA-CHLORDANE
ALPHA-CHLORDANE
TOXAPHENE
PCB-1016 (AROCLOR
PCB-1221
PCB-1232
PCB-1242
PCB-1248
PCB-1254
PCB-1260
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
(AROCLOR
MIXTURE)
/2
/2
1016)
1221)
1232)
1242)
1248)
1254)
1260)
/I
•••REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136.OCTOBER 26.1984)
*•'REMARKS***
••"FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80532 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 520-SW	COLLECTION START: 10/21/93 1350 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: FQ41 MD NO: FQ39
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHL0R0BEN2ILATE
•••REMARKS***	**'REMARKS***
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PESTlCIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
aTHENS, GA.
12,
J3
»*	PROJECT NO. 94-0036 SAMPLE NO. 80533
•	•	SOURCE: TOWER CHEMICAL
«•	STATION ID: 121-SW
«•	CASE NUMBER: 21073	SAS NUMBER:
*	*
SAMPLE TYPE: SURFACEWA
8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1830 STOP: 00/00/00
D. NUMBER: FQ42
UG/L
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
0.050UJ
O.10UJ
0.10UJ
0.10UJ
0. 10UJ
0.10UJ
0.10UJ
O.10UJ
ANALYTICAL RESULTS
ALPHA-BHC
BETA-BHC
DELTA-BHC
GAMMA-BHC (LINDANE)
HEPTACHLOR
ALDRIN
HEPTACHLOR EPOXIDE
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDE (P.P'-DDE)
ENDRIN
ENDOSULFAN II (BETA)
4.4'-DDD (P.P'-DDD)
ENDOSULFAN SULFATE
4.4'-DDT (P,P'-DDT)
UG/L
0.50UJ
0.10UJ
0.10UJ
0.050UJ
0.050UJ
5.OUJ
1 .OUJ
2.0UJ
1 OUJ
1 OUJ
1 .OUJ
1 OUJ
1 OUJ
ANALYTICAL RESULTS
METHOXYCHLOR
ENDRIN KETONE
ENDRIN ALDEHYDE
CHLORDANE (TECH MIXTURE)
GAMMA-CHLORDANE /2
ALPHA-CHLORDANE /2
TOXAPHENE
PCB-1016 (AROCLOR 1016)
PCB-1221 (AROCLOR 1221)
PCB-1232 (AROCLOR 1232)
PCB-1242 (AROCLOR 1242)
PCB-1248 (AROCLOR 1248)
PCB-1254 (AROCLOR 1254)
PCB-1260 (AROCLOR 1260)
/I
•»"REMARKS*«»
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26,1984)
••~REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE	IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV t
.GEMENT SYSTEM
ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80533
SOURCE: TOWER CHEMICAL
STATION ID: 121-SW
CASE.NO.: 21073	SAS NO.: 8175D
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1830 STOP: 00/00/00
D. NO.: FQ42	MD NO: FQ41
ANALYTICAL RESULTS UG/L
0.10UJ DICOFOL
0.10UJ CHLOROBENZILATE
••'REMARKS'*«
HOLDING TIMES EXCEEDED(40 CFR 136,OCTOBER 26.1984)
**'REMARKS***
•••FOOTNOTES»*•
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTlClDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIE
EPA-REGION IV E.
GEMENT SYSTEM
ATHENS, GA.
12. J3
PROJECT NO. 94-0036 SAMPLE NO. 80504 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 101-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
D. NUMBER: FQ11
UG/KG	ANALYTICAL RESULTS
2.8U	ALPHA-BHC
2.8U	BETA-BHC
2.8U	DELTA-BHC
2.8U	GAMMA-BHC (LINDANE)
2.8U	HEPTACHLOR
2.8U	ALDRIN
2.8U	HEPTACHLOR EPOXIDE
2.8U	ENDOSULFAN I (ALPHA)
5.5U	DIELDRIN
23	4.4'-DDE (P.P'-DDE)
5.5U	ENDRIN
5.5U	ENDOSULFAN II (BETA)
6.7	4,4'-DDD (P,P'-DDD)
5.5U	ENDOSULFAN SULFATE
5.5U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
28U	METHOXYCHLOR
5.5U	ENDRIN KETONE
5.5U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /I
2.8U	GAMMA-CHLORDANE /2
2.8U	ALPHA-CHLORDANE /2
280U	TOXAPHENE
55U	PCB-1016 (AROCLOR 1016)
10U	PCB-1221 (AROCLOR 1221)
55U	PCB-1232 (AROCLOR 1232)
55U	PCB-1242 (AROCLOR 1242)
55U	PCB-1248 (AROCLOR 1248)
55U	PCB-1254 (AROCLOR 1254)
55U	PCB-1260 (AROCLOR 1260)
41	PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI! .GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80504 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 101-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: 0 CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
D. NO.: FQ11	MD NO: FQ11
ANALYTICAL RESULTS UG/KG
5.5U DICOFOL
5.5U CHLOROBENZILATE
»•* FOOTNOTES*•*
•A-AVERAGE VALUE -NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE "N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST. IGEMENT SYSTEM
EPA-REGION IV t. ATHENS. GA.
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80502 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 102-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
D. NUMBER: FQ09
UG/KG	ANALYTICAL RESULTS
13U	ALPHA-BHC
13U	BETA-BHC
13U	DELTA-BHC
13U	GAMMA-BHC (LINDANE)
13U	HEPTACHLOR
13U	ALDRIN
13U	HEPTACHLOR EPOXIDE
100U	ENDOSULFAN I (ALPHA)
25U	DIELDRIN
1600	4.4'-DDE (P.P'-DDE)
25U	ENDRIN
25U	ENDOSULFAN II (BETA)
510	4.4'-DDD (P.P'-DDD)
25U	ENDOSULFAN SULFATE
25U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
13U	METHOXYCHLOR
25U	ENDRIN KETONE
25U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
13U	GAMMA-CHLORDANE	/2
13U	ALPHA-CHLORDANE	/2
1300U	TOXAPHENE
250U	PCB-1016 (AROCLOR	1016)
520U	PCB-1221 (AROCLOR	1221)
250U	PCB-1232 (AROCLOR	1232)
250U	PCB-1242 (AROCLOR	1242)
250U	PCB-1248 (AROCLOR	1248)
250U	PCB-1254 (AROCLOR	1254)
250U	PCB-1260 (AROCLOR	1260)
36	PERCENT MOISTURE
•••FOOTNOTES'*'
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80502 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 102-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START- 10/19/93 1230 STOP- 00/00/00
D. NO.: FQ09	MD NO: FQ09
ANALYTICAL RESULTS UG/KG
25U DICOFOL
25U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYS1 AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80500 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 103-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1055 STOP: 00/00/00
D. NUMBER: FQ07
UG/KG	ANALYTICAL RESULTS
1501/	ALPHA-BHC
150U	BETA-BHC
150U	DELTA-BHC
150U	GAMMA-BHC (LINDANE)
150U	HEPTACHLOR
150U	ALDRIN
150U	HEPTACHLOR EPOXIDE
150U	ENDOSULFAN I (ALPHA)
300U	DIELDRIN
1600	4.4'-DDE (P.P'-DDE)
300U	ENDRIN
300U	ENDOSULFAN II (BETA)
1100N	4.4'-DDD (P,P'-DDD)
300U	ENDOSULFAN SULFATE
300U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
1500U	METHOXYCHLOR
300U	ENDRIN KETONE
300U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
150U	GAMMA-CHLORDANE /2
150U	ALPHA-CHLORDANE /2
15000U	TOXAPHENE
3000U	PCB-1016 (AROCLOR 1016)
6000U	PCB-1221 (AROCLOR 1221)
3000U	PCB-1232 (AROCLOR 1232)
3000U	PCB-1242 (AROCLOR 1242)
3000U	PCB-1248 (AROCLOR 1248)
3000U	PCB-1254 (AROCLOR 1254)
3000U	PCB-1260 (AROCLOR 1260)
89	PERCENT MOISTURE
•••FOOTNOTES
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI AGEMENT SVSTEM
EPA-REGION IV	ATHENS. GA.	93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80500 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 103-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1055 STOP: 00/00/00
D. NO.: FQ07	MD NO: FQ07
ANALYTICAL RESULTS UG/KG
300U DICOFOL
300U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSII .GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80506 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 104-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP: 00/00/00
D. NUMBER: FQ13
UG/KG	ANALYTICAL RESULTS
2.7U	ALPHA-BHC
2.7U	BETA-BHC
2.7U	DELTA-BHC
2.7U	GAMMA-BHC (LINDANE)
2.7U	HEPTACHLOR
2.7U	ALDRIN
2.7U	HEPTACHLOR EPOXIDE
2.7U	ENDOSULFAN I (ALPHA)
5.2U	DIELDRIN
20	A.4'-DDE (P.P'-DDE)
5.2U	ENDRIN
5.2U	ENDOSULFAN II (BETA)
5.2U	4.4'-DDD (P.P'-DDD)
5.2U	ENDOSULFAN SULFATE
5.2U	4,4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
27U	METHOXYCHLOR
5.2U	ENDRIN KETONE
5.2U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
2.7U	GAMMA-CHLORDANE	/2
2.7U	ALPHA-CHLORDANE	/2
270U	TOXAPHENE
52U	PCB-1016 (AROCLOR 1016)
100U	PCB-1221 (AROCLOR	1221)
52U	PCB-1232 (AROCLOR	1232)
52U	PCB-1242 (AROCLOR	1242)
52U	PCB-1248 (AROCLOR	1248)
52U	PCB-1254 (AROCLOR	1254)
52U	PCB-1260 (AROCLOR	1260)
37	PERCENT MOISTURE
«»•FOOTNOTES*•»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI 1GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80506 SAMPLE TYPE. SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 104-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP: 00/00/00
D. NO.: FQ13	MD NO: FQ13
ANALYTICAL RESULTS UG/KG
5.2U DICOFOL
5.2U CHLOROBENZI LATE
~••FOOTNOTES***
• A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES • J—ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYST. »GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80508 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 105-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
D. NUMBER: FQ15
UG/KG	ANALYTICAL RESULTS
2.4U	ALPHA-BHC
2.4U	BETA-BHC
2.4U	DELTA-BHC
2.4U	GAMMA-BHC (LINDANE)
2.4U	HEPTACHLOR
2.4U	ALDRIN
2.4U	HEPTACHLOR EPOXIDE
2.4U	ENDOSULFAN I (ALPHA)
4.7U	DIELDRIN
12	4.4'-DDE (P.P'-DDE)
4.7U	ENDRIN
4.7U	ENDOSULFAN II (BETA)
4.7U	4.4'-DDD (P.P'-DDD)
4.7U	ENDOSULFAN SULFATE
4.7U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
24U	METHOXYCHLOR
4.7U	ENDRIN KETONE
4.7U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
2.4U	GAMMA-CHLORDANE	/2
2.4U	ALPHA-CHLORDANE	/2
240U	TOXAPHENE
47U	PCB-1016 (AROCLOR	1016)
96U	PCB-1221 (AROCLOR	1221)
47U	PCB-1232 (AROCLOR	1232)
47U	PCB-1242 (AROCLOR	1242)
47U	PCB-1248 (AROCLOR	1248)
47U	PCB-1254 (AROCLOR	1254)
47U	PCB-1260 (AROCLOR	1260)
31	PERCENT MOISTURE
•••FOOTNOTES*'*
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOI BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYS11 .GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80508 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 105-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START- 10/19/93 1800 STOP: 00/00/00
D. NO.: FQ15	MD NO: FQ15
ANALYTICAL RESULTS UG/KG
4.7U DICOFOL
4.7U CHLOROBENZILATE
•••FOOTNOTES*•»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. 
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV I ATHENS, GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80509 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 106-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1510 STOP: 00/00/00
D. NO.: FO16	MD NO: F016
ANALYTICAL RESULTS UG/KG
27U DICOFOL
27U CHLOROBENZILATE
• ••FOOTNOTES*"
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES ^-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCS'S DATA REPORT
SAMPLE AND ANALYSI	USEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80511 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 108-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/20/93 1715 STOP: 00/00/00
D. NUMBER: FQ18
UG/KG	ANALYTICAL RESULTS
3.OU	ALPHA-BHC
3.0U	BETA-BHC
3.0U	DELTA-BHC
3.0U	GANWA-BHC (LINDANE)
3.0U	HEPTACHLOR
3.0U	ALDRIN
3.OU	HEPTACHLOR EPOXIDE
3.0U	ENDOSULFAN I (ALPHA)
5.8U	DIELDRIN
5.8U	4.4'-DDE (P.P'-DDE)
5.8U	ENDRIN
5.8U	ENDOSULFAN II (BETA)
5.8U	4.4'-DDD (P,P'-DDD)
5.8U	ENDOSULFAN SULFATE
5.8U	4,4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
30U	METHOXYCHLOR
5.8U	ENDRIN KETONE
5.8U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /I
3 OU	GAMMA-CHLORDANE	/2
3.0U	ALPHA-CHLORDANE	/2
300U	TOXAPHENE
58U	PCB-1016 (AROCLOR 1016)
120U	PCB-1221 (AROCLOR 1221)
58U	PCB-1232 (AROCLOR 1232)
58U	PCB-1242 (AROCLOR 1242)
58U	PCB-1248 (AROCLOR 1248)
58U	PCB-1254 (AROCLOR 1254)
58U	PCB-1260 (AROCLOR	1260)
44	PERCENT MOISTURE
»•'FOOTNOTES*«»
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYST VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80511 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 108-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
D. NO.: FQ18	MD NO: FQ18
ANALYTICAL RESULTS UG/KG
5.8U DICOFOL
5.8U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSE
EPA-REGION IV E.
GEMENT SYSTEM
ATHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80513 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 109-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/21/93 1700 STOP: 00/00/00
D. NUMBER: FQ20
UG/KG	ANALYTICAL RESULTS
19U	ALPHA-BHC
19U	BETA-BHC
19U	DELTA-BHC
19U	GAMMA-BHC (LINDANE)
19U	HEPTACHLOR
19U	ALDRIN
19U	HEPTACHLOR EPOXIDE
19U	ENDOSULFAN I (ALPHA)
37U	DIELDRIN
37U	4.4'-DDE (P,P'~DDE)
37U	ENDRIN
37U	ENDOSULFAN II (BETA)
37U	4,4'-DDD (P.P'-DDD)
37U	ENDOSULFAN SULFATE
37U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
190U	METHOXYCHLOR
37U	ENDRIN KETONE
37U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
19U	GAMMA-CHLORDANE	/2
19U	ALPHA-CHLORDANE	/2
1900U	TOXAPHENE
370U	PCB-1016 (AROCLOR	1016)
740U	PCB-1221 (AROCLOR	1221)
370U	PCB-1232 (AROCLOR	1232)
370U	PCB-1242 (AROCLOR	1242)
370U	PCB-1248 (AROCLOR	1248)
370U	PCB-1254 (AROCLOR	1254)
370U	PCB-1260 (AROCLOR	1260)
91	PERCENT MOISTURE
» « » FOOTNOTES* »•
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80513 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 109-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM- SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1700 STOP: 00/00/00
D. NO.: FQ20	MD NO: FQ20
ANALYTICAL RESULTS UG/KG
37U DICOFOL
37U CHLOROBENZILATE
••~FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
AGEMENT SYSTEM
ATHENS. GA.
/93
PROJECT NO. 94-0036 SAMPLE NO. 80514 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 110-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP: 00/00/00
D. NUMBER: FQ21
UG/KG	ANALYTICAL RESULTS
21U	ALPHA-BHC
21U	BETA-BHC
21U	DELTA-BHC
21U	GAMMA-BHC (LINDANE)
21U	HEPTACHLOR
21U	ALDRIN
21U	HEPTACHLOR EPOXIDE
21U	ENDOSULFAN I (ALPHA)
41U	DIELDRIN
41U	4.4'-DDE (P.P'-DDE)
41U	ENDRIN
41U	ENDOSULFAN II (BETA)
41U	4,4'-ODD (P.P'-DDD)
41U	ENDOSULFAN SULFATE
41U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
210U	METHOXYCHLOR
41U	ENDRIN KETONE
41U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
21U	GAMMA-CHLORDANE /2
21U	ALPHA-CHLORDANE /2
2100U	TOXAPHENE
410U	PCB-1016 (AROCLOR 1016)
830U	PCB-1221 (AROCLOR 1221)
410U	PCB-1232 (AROCLOR 1232)
410U	PCB-1242 (AROCLOR 1242)
410U	PCB-1248 (AROCLOR 1248)
410U	PCB-1254 (AROCLOR 1254)
410U	PCB-1260 (AROCLOR 1260)
92	PERCENT MOISTURE
•••FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV I ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80514 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 110-SD
CASE.NO.: 21073	SAS NO.: 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP: 00/00/00
D. NO.: F021	MO NO: F021
ANALYTICAL RESULTS UG/KG
41U DICOFOL
41U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYS IAGEMENT SYSTEM
_ „ .	EPA-REGION IV	ATHENS. GA.	/93
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80515 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 111-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
r f TV • ri FDUOMT	CT* Fl
COLLECTION START: 10/21/93 1718 STOP: 00/00/00
D. NUMBER: FQ22
UG/KG	ANALYTICAL RESULTS
21U	ALPHA-BHC
21U	BETA-BHC
21U	DELTA-BHC
21U	GAMMA-BHC (LINDANE)
21U	HEPTACHLOR
21U	ALDRIN
21U	HEPTACHLOR EPOXIDE
21U	ENDOSULFAN I (ALPHA)
41U	DIELDRIN
41U	4.4'-DDE (P.P'-DDE)
41U	ENDRIN
41U	ENDOSULFAN II (BETA)
41U	4.4'-DDD (P.P'-DDD)
41U	ENDOSULFAN SULFATE
41U	4,4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
210U	METHOXYCHLOR
41U	ENDRIN KETONE
41U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
21U	GAMMA-CHLORDANE	/2
21U	ALPHA-CHLORDANE	/2
2100U	TOXAPHENE
410U	PCB-1016 (AROCLOR	1016)
840U	PCB-1221 (AROCLOR	1221)
410U	PCB-1232 (AROCLOR	1232)
410U	PCB-1242 (AROCLOR	1242)
410U	PCB-1248 (AROCLOR	1248)
410U	PCB-1254 (AROCLOR	1254)
410U	PCB-1260 (AROCLOR	1260)
92	PERCENT MOISTURE
• ••FOOTNOTES'"
•A AVERAGE VALUE *NA NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSH GEMENT SYSTEM
EPA-REGION IV t aTHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80515 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 111 —SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START- 10/21/93 1718 STOP: 00/00/00
D. NO.: F022	MD NO: F022
ANALYTICAL RESULTS UG/KG
41U DICOFOL
41U CHLOROBENZILATE
•»'FOOTNOTES*••
»A-AVERAGE VALUE «NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV EL. -VTHENS. GA.
12, J3
PROJECT NO. 94-0036 SAMPLE NO. 80516 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 112-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1840 STOP: 00/00/00
D. NUMBER: FQ23
UG/KG	ANALYTICAL RESULTS
28U	ALPHA-BHC
28U	BETA-BHC
28U	DELTA-BHC
28U	GAMMA-BHC (LINDANE)
28U	HEPTACHLOR
28U	ALDRIN
28U	HEPTACHLOR EPOXIDE
28U	ENDOSULFAN I (ALPHA)
55U	DIELDRIN
55U	4.4'-DDE (P.P'-DDE)
55U	ENDRIN
55U	ENDOSULFAN II (BETA)
55U	4.4'-ODD (P.P'-DDD)
55U	ENDOSULFAN SULFATE
55U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
280U	METHOXYCHLOR
55U	ENDRIN KETONE
55U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
28U	GAMMA-CHLORDANE	/2
28U	ALPHA-CHLORDANE	/2
2800U	TOXAPHENE
550U	PCB-1016 (AROCLOR 1016)
1100U	PCB-1221 (AROCLOR	1221)
550U	PCB-1232 (AROCLOR	1232)
550U	PCB-1242 (AROCLOR	1242)
550U	PCB-1248 (AROCLOR	1248)
550U	PCB-1254 (AROCLOR	1254)
550U	PCB-1260 (AROCLOR	1260)
94	PERCENT MOISTURE
• ••FOOTNOTES'"
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSI IGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80516 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 112-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START- 10/21/93 1840 STOP: 00/00/00
D. NO . : F023	MD NO: F023
ANALYTICAL RESULTS UG/KG
55U DICOFOL
55U CHLOROBENZILATE
••~FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI	VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
1. 93
PROJECT NO. 94-0036 SAMPLE NO. 80517 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 113-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST* FL
COLLECTION START: 10/21/93 1827 STOP: 00/00/00
D. NUMBER: FQ24
UG/KG	ANALYTICAL RESULTS
28U ALPHA-BHC
28U BETA-BHC
28U	DELTA-BHC
28U	GAMMA-BHC (LINDANE)
28U	HEPTACHLOR
28U	ALDRIN
28U	HEPTACHLOR EPOXIDE
28U	ENDOSULFAN I (ALPHA)
54U	DIELDRIN
54U	4.4'-DDE (P.P'-DDE)
54U	ENDRIN
54U	ENDOSULFAN II (BETA)
54U	4,4'-DDD (P.P'-DDD)
54U	ENDOSULFAN SULFATE
54U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
280U	METHOXYCHLOR
54U	ENDRIN KETONE
54U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
28U	GAMMA-CHLORDANE	/2
28U	ALPHA-CHLORDANE	/2
2800U	TOXAPHENE
540U	PCB-1016 (AROCLOR 1016)
1100U	PCB-1221 (AROCLOR	1221)
540U	PCB-1232 (AROCLOR 1232)
540U	PCB-1242 (AROCLOR 1242)
540U	PCB-1248 (AROCLOR	1248)
540U	PCB-1254 (AROCLOR	1254)
540U	PCB-1260 (AROCLOR	1260)
94	PERCENT MOISTURE
•••FOOTNOTES'**
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI. *GEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-O036 SAMPLE NO. 80517 SAMPLE TYPE: SOIL
SOURCE. TOWER CHEMICAL
STATION ID: 113-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
TTTV- PIF DUD KIT	CT- Fl
COLLECTION START: 10/21/93 1827 STOP: 00/00/00
D. NO : FQ24	MD NO: F024
ANALYTICAL RESULTS UG/KG
54U DICOFOL
54U CHLOROBENZILATE
* ••FOOTNOTES'"
•A-AVERAGE VALUE «NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI \GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
1. 93
PROJECT NO. 94-0036 SAMPLE NO. 80518 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1813 STOP: 00/00/00
D. NUMBER: FQ25
UG/KG	ANALYTICAL RESULTS
34U	ALPHA-BHC
34U	BETA-BHC
34U	DELTA-BHC
34U	GAMMA-BHC (LINDANE)
34U	HEPTACHLOR
34U	ALDRIN
34U	HEPTACHLOR EPOXIDE
34U	ENDOSULFAN I (ALPHA)
65U	DIELDRIN
65U	4.4'-DDE (P.P'-DDE)
65U	ENDRIN
65U	ENDOSULFAN II (BETA)
65U	4.4'-DDD (P.P'-DDD)
65U	ENDOSULFAN SULFATE
65U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
340U	METHOXYCHLOR
65U	ENDRIN KETONE
65U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
34U	GAMMA-CHLORDANE /2
34U	ALPHA-CHLORDANE /2
3400U	TOXAPHENE
650U	PCB-1016 (AROCLOR 1016)
1300U	PCB-1221 (AROCLOR 1221)
650U	PCB-1232 (AROCLOR 1232)
650U	PCB-1242 (AROCLOR 1242)
650U	PCB-1248 (AROCLOR 1248)
650U	PCB-1254 (AROCLOR 1254)
650U	PCB-1260 (AROCLOR 1260)
95	PERCENT MOISTURE
««»FOOTNOTES*•*
•A-AVERAGE VALUE 'NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80518 SAMPLE TYPE SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1813 STOP: 00/00/00
D NO.: FQ25	MD NO: FQ25
ANALYTICAL RESULTS UG/KG
65U DICOFOL
65U CHLOROBENZILATE
•••FOOTNOTES*»•
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	.EMENT SYSTEM
EPA-REGION IV ES. CHENS. GA.	12,
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80521 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 115-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY' CLERMONT	ST* FL
COLLECTION START: 10/21/93 1230 STOP: 00/00/00
D. NUMBER: FQ30
UG/KG	ANALYTICAL RESULTS
24U	ALPHA-BHC
24U	BETA-BHC
24U	DELTA-BHC
24U	GAMMA-BHC (LINDANE)
24U	HEPTACHLOR
24U	ALDRIN
24U	HEPTACHLOR EPOXIDE
24U	ENDOSULFAN I (ALPHA)
47U	DIELDRIN
240N	4.4'-DDE (P.P'-DDE)
47U	ENDRIN
47U	ENDOSULFAN II (BETA)
180	4.4'-DDD (P,P'-DDD)
47U	ENDOSULFAN SULFATE
47U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
240U	METHOXYCHLOR
47U	ENDRIN KETONE
47U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
24U	GAMMA-CHLORDANE /2
24U	ALPHA-CHLORDANE /2
2400U	TOXAPHENE
470U	PCB-1016 (AROCLOR 1016)
960U	PCB-1221 (AROCLOR 1221)
470U	PCB-1232 (AROCLOR 1232)
470U	PCB-1242 (AROCLOR 1242)
470U	PCB-1248 (AROCLOR 1248)
470U	PCB-1254 (AROCLOR 1254)
470U	PCB-1260 (AROCLOR 1260)
93	PERCENT MOISTURE
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80521 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 115-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1230 STOP: 00/00/00
D. NO. : FQ30	MD NO: F028
ANALYTICAL RESULTS UG/KG
47U DICOFOL
47U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTlCtDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV Ev_ «THENS, GA.
12, J3
PROJECT NO. 94-0036 SAMPLE NO. 80522 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 116-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED	BY: B CARTER
riTV- n rpuriMT	cr- fi
COLLECTION START: 10/21/93 1215 STOP: 00/00/00
D. NUMBER: FQ31
UG/KG	ANALYTICAL RESULTS
12U	ALPHA-BHC
12U	BETA-BHC
12U	DELTA-BHC
12U	GAMMA-BHC (LINDANE)
12U	HEPTACHLOR
12U	ALDRIN
12U	HEPTACHLOR EPOXIDE
12U	ENDOSULFAN I (ALPHA)
23U	DIELDRIN
67	4,4'-DDE (P.P'-DDE)
23U	ENDRIN
23U	ENDOSULFAN II (BETA)
54	4,4'-ODD (P,P'-DDD)
23U	ENDOSULFAN SULFATE
23U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
120U	METHOXYCHLOR
23U	ENDRIN KETONE
23U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
12U	GAMMA-CHLORDANE	/2
12U	ALPHA-CHLORDANE	/2
1200U	TOXAPHENE
230U	PCB-1016 (AROCLOR	1016)
480U	PCB-1221 (AROCLOR	1221)
230U	PCB-1232 (AROCLOR	1232)
230U	PCB-1242 (AROCLOR	1242)
230U	PCB-1248 (AROCLOR	1248)
230U	PCB-1254 (AROCLOR	1254)
230U	PCB-1260 (AROCLOR	1260)
86	PERCENT MOISTURE
»«'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI! GEMENT SYSTEM
EPA-REGION IV E. ^THENS, GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80522 SAMPLE TYPE. SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 116-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1215 STOP: 00/00/00
D. NO.: FQ31	MD NO: FQ29
ANALYTICAL RESULTS UG/K.G
23U DICOFOL
23U CHLOROBENZILATE
•••FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PEST1CIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV Ei
¦EMENT SYSTEM
(HENS, GA.
12,
PROJECT NO. 94-0036 SAMPLE NO. 80523 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 117-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NUMBER: FQ32
UG/KG	ANALYTICAL RESULTS
34U	ALPHA-BHC
34U	BETA-BHC
34U	DELTA-BHC
34U	GAMMA-BHC (LINDANE)
34U	HEPTACHLOR
34U	ALDRIN
34U	HEPTACHLOR EPOXIDE
34U	ENDOSULFAN I (ALPHA)
66U	DIELDRIN
66U	4.4'-DDE (P.P'-DDE)
66U	ENDRIN
66U	ENDOSULFAN II (BETA)
66U	4,4'-ODD (P.P'-DDD)
66U	ENDOSULFAN SULFATE
66U	4,4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
340U	METHOXYCHLOR
66U	ENDRIN KETONE
66U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /I
34U	GAMMA-CHLORDANE	/2
34U	ALPHA-CHLORDANE	/2
3400U	TOXAPHENE
660U	PCB-1016 (AROCLOR 1016)
1300U	PCB-1221 (AROCLOR 1221)
660U	PCB-1232 (AROCLOR	1232)
660U	PCB-1242 (AROCLOR	1242)
660U	PCB-1248 (AROCLOR	1248)
660U	PCB-1254 (AROCLOR	1254)
660U	PCB-1260 (AROCLOR	1260)
95	PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. iTHENS. GA.
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80523 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 117-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO : FQ32	MD NO: FQ30
ANALYTICAL RESULTS UG/KG
66U DICOFOL
66U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ESL .HENS, GA.
12/
PROJECT NO. 94-0036 SAMPLE NO. 80524 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 517-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NUMBER: FQ33
UG/KG	ANALYTICAL RESULTS
24U ALPHA-BHC
24U BETA-BHC
24U	DELTA-BHC
24U	GAMMA-BHC (LINDANE)
24U	HEPTACHLOR
24U	ALDRIN
24U	HEPTACHLOR EPOXIDE
24U	ENDOSULFAN I (ALPHA)
47U	DIELDRIN
47U	4,4'-DDE (P.P'-DDE)
47U	ENDRIN
47U	ENDOSULFAN II (BETA)
47U	4.4'-DDD (P.P'-DDD)
47U	ENDOSULFAN SULFATE
47U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
240U	METHOXYCHLOR
47U	ENDRIN KETONE
47U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
24U	GAMMA-CHLORDANE	/2
24U	ALPHA-CHLORDANE	/2
2400U	TOXAPHENE
470U	PCB-1016 (AROCLOR 1016)
960U	PCB-1221 (AROCLOR 1221)
470U	PCB-1232 (AROCLOR	1232)
470U	PCB-1242 (AROCLOR	1242)
470U	PCB-1248 (AROCLOR	1248)
470U	PCB-1254 (AROCLOR	1254)
470U	PCB-1260 (AROCLOR	1260)
93	PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	'93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80524 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 517-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO.: FQ33	MD NO: F031
ANALYTICAL RESULTS UG/KG
47U DICOFOL
47U CHLOROBENZILATE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES .HENS. GA.
12/
PROJECT NO. 94-0036 SAMPLE NO. 80527 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 118-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1445 STOP: 00/00/00
D. NUMBER: FQ36
UG/KG	ANALYTICAL RESULTS
24U ALPHA-BHC
24U BETA-BHC
24U DELTA-BHC
24U	GAMMA-BHC (LINDANE)
24U	HEPTACHLOR
24U	ALDRIN
24U	HEPTACHLOR EPOXIDE
24U	ENDOSULFAN I (ALPHA)
46U	DIELDRIN
46U	4.4'-DDE (P.P'-DDE)
46U	ENDRIN
46U	ENDOSULFAN II (BETA)
46U	4.4'-DDD (P.P'-DDD)
46U	ENDOSULFAN SULFATE
46U	4.4'-DDT (P,P'-DDT)
UG/KG	ANALYTICAL RESULTS
240U	METHOXYCHLOR
46U	ENDRIN KETONE
46U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
24U	GAMMA-CHLORDANE	/2
24U	ALPHA-CHLORDANE	/2
2400U	TOXAPHENE
460U	PCB-1016 (AROCLOR	1016)
940U	PCB-1221 (AROCLOR	1221)
460U	PCB-1232 (AROCLOR	1232)
460U	PCB-1242 (AROCLOR	1242)
460U	PCB-1248 (AROCLOR	1248)
460U	PCB-1254 (AROCLOR	1254)
460U	PCB-1260 (AROCLOR	1260)
93	PERCENT MOISTURE
» « * FOOTNOTES* » »
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
sample and analysi *gement system
EPA-REGION IV	ATHENS, GA.	93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80527 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 118-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1445 STOP: 00/00/00
D. NO. : FQ36	MD NO: F034
ANALYTICAL RESULTS UG/KG
46U DICOFOL
46U CHLOROBENZILATE
•••FOOTNOTES*»*
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES «J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV E. ,THENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80528 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 119-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST* FL
COLLECTION START: 10/21/93 1430 STOP: 00/00/00
D. NUMBER: FQ37
UG/KG	ANALYTICAL RESULTS
21U	ALPHA-BHC
21U	BETA-BHC
21U	DELTA-BHC
21U	GAMMA-BHC (LINDANE?
21U	HEPTACHLOR
21U	ALDRIN
21U	HEPTACHLOR EPOXIDE
21U	ENDOSULFAN I (ALPHA)
41U	DIELDRIN
41U	4.4'-DDE (P.P'-DDE)
41U	ENDRIN
41U	ENDOSULFAN II (BETA)
41U	4,4'-DDD (P.P'-DDD)
41U	ENDOSULFAN SULFATE
41U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
210U	METHOXYCHLOR
41U	ENDRIN KETONE
41U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
21U	GAMMA-CHLORDANE	/2
21U	ALPHA-CHLORDANE	/2
2100U	TOXAPHENE
410U	PCB-1016 (AROCLOR	1016)
830U	PCB-1221 (AROCLOR	1221)
410U	PCB-1232 (AROCLOR	1232)
410U	PCB-1242 (AROCLOR	1242)
410U	PCB-1248 (AROCLOR	1248)
410U	PCB-1254 (AROCLOR	1254)
410U	PCB-1260 (AROCLOR	1260)
92	PERCENT MOISTURE
•»'FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALVS15 GEMENT SYSTEM
EPA-REGION IV E «THENS, GA.
SCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80528 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 119-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1430 STOP: 00/00/00
D. NO.: FQ37	MD NO: FQ35
ANALYTICAL RESULTS UG/KG
41U DICOFOL
41U CHLOROBENZI LATE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN "L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ESL HENS. GA.	12/
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80529 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 120-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
r ttv- ri FPIAOKlT	ct« PI
COLLECTION START. 10/21/93 1415 STOP: 00/00/00
D. NUMBER: FQ38
UG/KG	ANALYTICAL RESULTS
19U	ALPHA-BHC
19U	BETA-BHC
19U	DELTA-BHC
19U	GAMMA-BHC (LINDANE)
19U	HEPTACHLOR
19U	ALDRIN
19U	HEPTACHLOR EPOXIDE
19U	ENDOSULFAN I (ALPHA)
37U	DIELDRIN
37U	4.4'-DDE (P.P'-DDE)
37U	ENDRIN
37U	ENDOSULFAN II (BETA)
37U	4.4'-DDD (P.P'-DDD)
37U	ENDOSULFAN SULFATE
37U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
190U	METHOXYCHLOR
37U	ENDRIN KETONE
37U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /1
19U	GAMMA-CHLORDANE /2
19U	ALPHA-CHLORDANE /2
1900U	TOXAPHENE
370U	PCB-1016 (AROCLOR 1016)
740U	PCB-1221 (AROCLOR 1221)
370U	PCB-1232 (AROCLOR 1232)
370U	PCB-1242 (AROCLOR 1242)
370U	PCB-1248 (AROCLOR 1248)
370U	PCB-1254 (AROCLOR 1254)
370U	PCB-1260 (AROCLOR 1260)
91	PERCENT MOISTURE
•••FOOTNOTES*»*
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI \GEMENT SYSTEM
EPA-REGION IV l ATHENS. GA.	1. 93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80529 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 120-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D. NO. : F038	MD NO: F036
ANALYTICAL RESULTS UG/KG
37U DICOFOL
37U CHLOROBENZILATE
*•'FOOTNOTES*»«
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES. .HENS. GA.
12/
PROJECT NO. 94-0036 SAMPLE NO. 80530 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
TTTV* n FHU^UT	CT. PI
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D. NUMBER: FQ39
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
19U	ALPHA-BHC
19U	BETA-BHC
19U	DELTA-BHC
19U	GAMMA-BHC (LINDANE)
19U	HEPTACHLOR
19U	ALDRIN
19U	HEPTACHLOR EPOXIDE
19U	ENDOSULFAN I (ALPHA)
36U	DIELDRIN
36U	4.4'-DDE (P.P'-DDE)
36U	ENDRIN
36U	ENDOSULFAN II (BETA)
36U	4,4'-DDD (P.P'-DDD)
36U	ENDOSULFAN SULFATE
36U	4.4'-ODT (P.P'-DDT)
190U METHOXYCHLOR
190U ENDRIN KETONE
36U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE)
19U	GAMMA-CHLORDANE	/2
36U	ALPHA-CHLORDANE	/2
19U	TOXAPHENE
1900U	PCB-1016 (AROCLOR	1016)
360U	PCB-1221 (AROCLOR	1221)
740U	PCB-1232 (AROCLOR	1232)
360U	PCB-1242 (AROCLOR	1242)
360U	PCB-1248 (AROCLOR	1248)
360U	PCB-1254 (AROCLOR	1254)
360U	PCB-1260 (AROCLOR	1260)
PERCENT MOISTURE
/1
•»REMARKS*••
*«»»«THIS REMARK NOT USED
• "REMARKS***
»»FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE	IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES	THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
»C-CONFIRMED BY	GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI
EPA-REGION IV
VGEMENT SYSTEM
ATHENS, GA.
93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80530 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D. NO : FQ39	MD NO: F037
ANALYTICAL RESULTS UG/KG
36U DICOFOL
36U CHLOROBENZI LATE
»»'REMARKS*»»
• •••~•THIS REMARK. NOT USED
*»'REMARKS***
»*'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS JEMENT SYSTEM
EPA-REGION IV ES ,THENS, GA.	12/
PESTICIDES/PCB'S DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80534 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID. 121-SD
CASE NUMBER: 21073	SAS NUMBER: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1830 STOP: 00/00/00
D. NUMBER: FQ43
UG/KG	ANALYTICAL RESULTS
2.2U	ALPHA-BHC
2.2U	BETA-BHC
2.2U	DELTA-BHC
2.2U	GAMMA-BHC (LINDANE)
2.2U	HEPTACHLOR
2.2U	ALDRIN
2.2U	HEPTACHLOR EPOXIDE
2.2U	ENDOSULFAN I (ALPHA)
4.3U	DIELDRIN
4.1J	4.4'-DDE (P.P'-DDE)
4.3U	ENDRIN
4.3U	ENDOSULFAN II (BETA)
4.3U	4.4'-DDD (P.P'-DDD)
4.3U	ENDOSULFAN SULFATE
4.3U	4.4'-DDT (P.P'-DDT)
UG/KG	ANALYTICAL RESULTS
22U	METHOXYCHLOR
4.3U	ENDRIN KETONE
4.3U	ENDRIN ALDEHYDE
CHLORDANE (TECH. MIXTURE) /^
2.2U	GAMMA-CHLORDANE	/2
2.2U	ALPHA-CHLORDANE	/2
220U	TOXAPHENE
43U	PCB-1016 (AROCLOR	1016)
87U	PCB-1221 (AROCLOR	1221)
43U	PCB-1232 (AROCLOR	1232)
43U	PCB-1242 (AROCLOR	1242)
43U	PCB-1248 (AROCLOR	1248)
43U	PCB-1254 (AROCLOR	1254)
43U	PCB-1260 (AROCLOR	1260)
24	PERCENT MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCE5 •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
•C-CONFIRMED BY GCMS	1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS.
2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYS IAGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	/93
MISCELLANEOUS PEST/PCB COMPOUNDS - DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80534 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 121-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START¦ 10/21/93 1830 STOP: 00/00/00
D. NO.: FQ43	MD NO: FQ42
ANALYTICAL RESULTS UG/KG
4.3U DICOFOL
4.3U CHLOROBENZILATE
•••FOOTNOTES*'*
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
~~~~~memorandum******
DATE: 12/14/93
SUBJECT: Results of Purgeable Organic Analysis:
9A-0036 TOWER CHEMICAL
CLERMONT FL
CASE NO: 21073SAS NO: 6175D
FROM: Charles H. Hooper
Chief, Laboratory Evaluation/Quality Assurance Section
TO: DELBERT HICKS
Attached are the results of analysis of samples collected as part of
the subject project.
As a result of the Quality Assurance Review, certain data qualifiers
may have been placed on the data. Attached is a DATA QUALIFIER
REPORT which explains the reasons that these qualifiers were required.
If you have any questions please contact me.
ATTACHMENT
-------
ORGANIC DATA QUALIFIER REPORT
Case Number 21073	Project Number 94-0036
Site ID. Tower Chemical, Clermont, FL
SAS Number
Flag
Reason
Volatiles



all waters
carbon tetrachloride
R
unacceptable blind spike recovery
80500,80511,
80513,80527,
80528,80530
acetone
N
common lab contaminant
80503,80510,
80512,80514,
80515,80517,
80518,80529,
80530
carbon disulfide
J
< quantitation limit
Extractables



all waters
all compounds
J
exceeded extraction holding times
all soils
phenol
acenaphthene
2,4-dimethylphenol
J
R
R
low blind spike recovery
unacceptable blind spike recovery
unacceptable blind spike recovery
80508
fluoranthene
pyrene
J
J
<	quantitation limit
<	quantitation limit
Pesticides



all waters
all compounds
J
exceeded extraction holding times
80500
4,4'-DDD
N
difference in column
quantitations
80521
4,4'-DDE
N
difference in column
quantitations
80534
4,4'-DDE
J
< quantitation limit
-------
PUfiGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
ATHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80503 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID: 101-SW
CASE NO.: 21073
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/19/93 1520 STOP. 00/00/00
D. NO.: F010
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
3J	CARBON DISULFIDE
10U	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1,2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1.1,1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
10U	1.2-DICHLOROPROPANE
10U	CIS-1,3-DICHLOROPROPENE
1OU	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
»»'REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYST. tGEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80531
SOURCE: TOWER CHEMICAL
STATION ID: 120-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1350 STOP: 00/00/00
D. NO.: FQ40
UG/L	ANALYTICAL RESULTS
NA	CHLOROMETHANE
NA	BROMOME THANE
NA	VINYL CHLORIDE
NA	CHLOROETHANE
NA	METHYLENE CHLORIDE
NA	ACETONE
NA	CARBON DISULFIDE
NA	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
NA	1.1-DICHLOROE THANE
NA	1.2-DICHLOROETHENE (TOTAL)
NA	CHLOROFORM
NA	1.2-DICHLOROETHANE
NA	METHYL ETHYL KETONE
NA	1 .1.1-TRICHLOROE THANE
NA	CARBON TETRACHLORIDE
NA	BROMODICHLOROME THANE
UG/L	ANALYTICAL RESULTS
NA	1,2-DICHLOROPROPANE
NA	CIS-1.3-DICHL0R0PR0PENE
NA	TRICHLOROETHENE(TRICHLOROETHYLENE)
NA	DIBROMOCHLOROMETHANE
NA	1,1.2-TRICHLOROETHANE
NA	BENZENE
NA	TRANS-1.3-DICHLOROPROPENE
NA	BROMOFORM
NA	METHYL ISOBUTYL KETONE
NA	METHYL BUTYL KETONE
NA	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
NA	1.1.2.2-TETRACHLOROETHANE
NA	TOLUENE
NA	CHLOROBENZENE
NA	ETHYL BENZENE
NA	STYRENE
NA	TOTAL XYLENES
•••REMARKS***
NO SAMPLE CONTAINER RECEIVED
*•'REMARKS*••
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80532
SOURCE: TOWER CHEMICAL
STATION ID: 520-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST' FL
COLLECTION START. 10/21/93 1350 STOP: 00/00/00
D. NO.: FQ41
UG/L	ANALYTICAL RESULTS
NA	CHLOROMETHANE
NA	BROMOMETHANE
NA	VINYL CHLORIDE
NA	CHLOROETHANE
NA	METHYLENE CHLORIDE
NA	ACETONE
NA	CARBON DISULFIDE
NA	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
NA	1,1-DICHLOROE THANE
NA	1.2-DICHLOROETHENE (TOTAL)
NA	CHLOROFORM
NA	1,2-DICHLOROETHANE
NA	METHYL ETHYL KETONE
NA	1.1,1-TRICHLOROETHANE
NA	CARBON TETRACHLORIDE
NA	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
NA	1.2-DICHLOROPROPANE
NA	CIS-1.3-DICHLOROPROPENE
NA	TRICHLOROETHENE(TRICHLOROETHYLENE )
NA	DIBROMOCHLOROMETHANE
NA	1.1.2-TRICHLOROETHANE
NA	BENZENE
NA	TRANS-1.3-DICHLOROPROPENE
NA	BROMOFORM
NA	METHYL ISOBUTYL KETONE
NA	METHYL BUTYL KETONE
NA	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
NA	1.1.2.2-TETRACHLOROETHANE
NA	TOLUENE
NA	CHLOROBENZENE
NA	ETHYL BENZENE
NA	STYRENE
NA	TOTAL XYLENES
**'REMARKS***
NO SAMPLE CONTAINER RECEIVED
»»'REMARKS*«*
•~~FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSII GEMENT SYSTEM
EPA-REGION IV E ATHENS, GA.
PURGEABLE ORGANICS DATA REPORT
•* PROJECT
»• SOURCE:
»• STATION
NO. 94-0036 SAMPLE NO. 80533
TOWER CHEMICAL
ID: 121-SW
SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL **
1830 STOP: 00/00/00 »*
»* CASE NO
: 21073
SAS NO.: 8175D
D. NO.: FQ42
* *
UG/L
ANALYTICAL RESULTS
UG/L
ANALYTICAL RESULTS
10U
CHLOROMETHANE
10U
1,2-DICHLOROPROPANE
10U
BROMOMETHANE
10U
CIS-1.3-DICHL0R0PR0PENE
10U
VINYL CHLORIDE
10U
TRICHLOROETHENE(TRICHLOROETHYLENE)
10U
CHLOROETHANE
10U
DIBROMOCHLOROME THANE
10U
METHYLENE CHLORIDE
10U
1 ,1.2-TRICHLOROETHANE
10U
ACETONE
10U
BENZENE
10U
CARBON DISULFIDE
10U
TRANS-1.3-DICHLOROPROPENE
10U
1.1-DICHLOROETHENE(1.1-DICHLOROETHYLENE)
10U
BROMOFORM
10U
1.1-DICHLOROETHANE
10U
METHYL ISOBUTYL KETONE
10U
1,2-DICHLOROETHENE (TOTAL)
10U
METHYL BUTYL KETONE
10U
CHLOROFORM
10U
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U
1.2-DICHLOROETHANE
10U
1.1.2.2-TETRACHL0R0ETHANE
10U
METHYL ETHYL KETONE
10U
TOLUENE
10U
1.1.1-TRICHLOROE THANE
10U
CHLOROBENZENE
10UR
CARBON TETRACHLORIDE
10U
ETHYL BENZENE
10U
BROMODICHLOROME THANE
10U
STYRENE


10U
TOTAL XYLENES
» * * FOOTNOTES*•»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV t «THENS, GA.
PURGEABLE ORGANICS DATA REPORT
•• PROJECT
»~ SOURCE:
** STATION
NO. 94-0036 SAMPLE NO. 80537
TOWER CHEMICAL
ID: 002-QA
SAMPLE TYPE: WATER
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER •*
ST: FL ••
1135 STOP: 00/00/00 •*
»* CASE NO
: 21073
SAS NO.: 8175D
D. NO.: FQ27
* *
UG/L
ANALYTICAL RESULTS
UG/L
ANALYTICAL RESULTS
10U
CHLOROMETHANE
10U
1,2-DICHLOROPROPANE
10U
BROMOMETHANE
10U
CIS-1.3-DICHL0R0PR0PENE
10U
VINYL CHLORIDE
10U
TRICHLOROETHENE(TRICHLOROETHYLENE)
10U
CHLOROETHANE
10U
DIBROMOCHLOROME THANE
10U
METHYLENE CHLORIDE
10U
1 .1 .2-TRICHLOROETHANE
10U
ACETONE
10U
BENZENE
10U
CARBON DISULFIDE
10U
TRANS-1.3-DICHL0R0PR0PENE
10U
1.1-DICHL0R0ETHENE(1,1-DICHLOROETHYLENE)
10U
BROMOFORM
10U
1.1-DICHLOROETHANE
10U
METHYL ISOBUTYL KETONE
10U
1.2-DICHLOROETHENE (TOTAL)
10U
METHYL BUTYL KETONE
10U
CHLOROFORM
10U
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U
1.2-DICHLOROETHANE
10U
1.1.2. 2-TETRACHLOROETHANE
10U
METHYL ETHYL KETONE
10U
TOLUENE
10U
1.1.1-TRICHLOROETHANE
10U
CHLOROBENZENE
10UR
CARBON TETRACHLORIDE
10U
ETHYL BENZENE
10U
BROMODICHLOROME THANE
10U
STYRENE


10U
TOTAL XYLENES
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV i
\GEMENT SYSTEM
ATHENS. GA.
1 93
PROJECT NO. 94-0036 SAMPLE NO. 80504
SOURCE: TOWER CHEMICAL
STATION ID: 101-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
D. NO.: F011
UG/KG	ANALYTICAL RESULTS
91U	CHLOROMETHANE
91U	BROMOMETHANE
91U	VINYL CHLORIDE
91U	CHLOROETHANE
91U	METHYLENE CHLORIDE
91U	ACETONE
91U	CARBON DISULFIDE
91U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
91U	1 .1 -DI CHLOROE THANE
91U	1.2-DICHLOROETHENE (TOTAL)
91U	CHLOROFORM
91U	1.2-DICHLOROE THANE
91U	METHYL ETHYL KETONE
91U	1.1.1-TRICHLOROETHANE
91U	CARBON TETRACHLORIDE
91U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
91U	1,2-D1CHLOROPROPANE
91U	CIS-1,3-DICHLOROPROPENE
91U	TRICHLOROETHENE(TRICHLOROETHYLENE)
91U	DIBROMOCHLOROMETHANE
91U	1.1.2-TRICHLOROETHANE
91U	BENZENE
91U	TRANS-1,3-DICHLOROPROPENE
91U	BROMOFORM
91U	METHYL ISOBUTYL KETONE
91U	METHYL BUTYL KETONE
91U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
91U	1.1.2.2-TETRACHLOROETHANE
91U	TOLUENE
91U	CHLOROBENZENE
91U	ETHYL BENZENE
91U	STYRENE
91U	TOTAL XYLENES
89	PERCENT MOISTURE
•••REMARKS***
•••REMARKS***
•••FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI	.GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
1. J3
PROJECT NO. 94-0036 SAMPLE NO. 80502
SOURCE: TOWER CHEMICAL
STATION ID. 102-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP: 00/00/00
D. NO.: FQ09
UG/KG	ANALYTICAL RESULTS
13U CHLOROMETHANE
13U BROMOMETHANE
13U	VINYL CHLORIDE
13U	CHLOROETHANE
20U	METHYLENE CHLORIDE
13U	ACETONE
13U	CARBON DISULFIDE
13U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
13U	1,1-DICHLOROETHANE
13U	1,2-DICHLOROETHENE (TOTAL)
13U	CHLOROFORM
13U	1,2-DICHLOROETHANE
13U	METHYL ETHYL KETONE
13U	1,1,1-TRICHLOROETHANE
13U	CARBON TETRACHLORIDE
13U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
13U	1.2-DICHLOROPROPANE
13U	CIS-1.3-DICHL0R0PR0PENE
13U	TRICHLOROETHENE(TRICHLOROETHYLENE)
13U	DIBROMOCHLOROMETHANE
13U	1,1.2-TRICHL0R0ETHANE
13U	BENZENE
13U	TRANS-1.3-DICHL0R0PR0PENE
13U	BROMOFORM
13U	METHYL ISOBUTYL KETONE
13U	METHYL BUTYL KETONE
13U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
13U	1.1.2.2-TETRACHLOROETHANE
13U	TOLUENE
13U	CHLOROBENZENE
13U	ETHYL BENZENE
13U	STYRENE
13U	TOTAL XYLENES
21	PERCENT MOISTURE
• ••REMARKS"*
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIf .GEMENT SYSTEM
EPA-REGION IV t VTHENS. GA.
1. J3
PROJECT NO. 94-0036 SAMPLE NO. 80500 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID. 103-SD
CASE NO.: 21073
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/19/93 1055 STOP: 00/00/00
D. NO.: FQ07
UG/KG
ANALYTICAL RESULTS
56U CHLOROMETHANE
56U	BROMOMETHANE
56U	VINYL CHLORIDE
56U	CHLOROETHANE
98U	METHYLENE CHLORIDE
1 SON ACETONE
56U	CARBON DISULFIDE
56U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
56U	1,1-DICHLOROE THANE
56U	1.2-01CHLOROETHENE (TOTAL)
56U	CHLOROFORM
56U	1,2-DICHLOROETHANE
56U	METHYL ETHYL KETONE
56U	1.1.1-TRICHLOROETHANE
56U	CARBON TETRACHLORIDE
56U	BROMODICHLOROME THANE
UG/KG	ANALYTICAL RESULTS
56 U	1,2-DICHLOROPROPANE
56U	CIS-1,3-DICHLOROPROPENE
56U	TRICHLOROETHENE(TRICHLOROETHYLENE)
56U	DIBROMOCHLOROMETHANE
56U	1.1 .2-TRICHLOROETHANE
56U BENZENE
56U	TRANS-1.3-DICHLOROPROPENE
56U	BROMOFORM
56U	METHYL ISOBUTYL KETONE
561/	METHYL BUTYL KETONE
56U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
56U	1.1.2.2-TETRACHLOROETHANE
56U	TOLUENE
56U	CHLOROBENZENE
56U	ETHYL BENZENE
56U	STYRENE
56U	TOTAL XYLENES
82	PERCENT MOISTURE
•••REMARKS***
*•"REMARKS*••
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
PURGE ABLE OROAWCS DAT* REPORT	EPA-REGIO* IV E- .THENS, GA.	,2.
»• PROJECT
•• SOURCE:
~* STATION
NO. 94-0036 SAMPLE NO. 80506
TOWER CHEMICAL
ID: 104-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/19/93
BY: B CARTER •«
ST: FL ••
1735 STOP: 00/00/00 •*
•• CASE NO
: 21073
SAS NO.: 8175D
D. NO.: F013
* •
UG/KG
ANALYTICAL RESULTS
20U
CHLOROMETHANE
20U
BROMOME THANE
20U
VINYL CHLORIDE
20U
CHLOROETHANE
140U
METHYLENE CHLORIDE
20U
ACETONE
20U
CARBON DISULFIDE
20U
1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
20U
1.1-DICHLOROETHANE
20U
1.2-DICHLOROETHENE (TOTAL)
20U
CHLOROFORM
20U
1.2-DICHLOROETHANE
20U
METHYL ETHYL KETONE
20U
1.1.1-TRICHLOROETHANE
20U
CARBON TETRACHLORIDE
20U
BROMODICHLOROME THANE
UG/KG	ANALYTICAL RESULTS
20U	1.2-DICHLOROPROPANE
20U	CIS-t.3-0ICHLOROPROPENE
20U	TRICHLOROETHENE(TRICHLOROETHYLENE)
20U	DIBROMOCHLOROMETHANE
20U	1.1,2-TRICHLOROETHANE
20U	BENZENE
20U	TRANS-1.3-DICHL0R0PR0PENE
20U	BROMOFORM
20U	METHYL ISOBUTYL KETONE
20U	METHYL BUTYL KETONE
20U	TE TRACHLOROETHENE(TE TRACHLOROE THYLENE)
20U	1.1.2.2-TETRACHLOROETHANE
20U	TOLUENE
20U	CHLOROBENZENE
20U	ETHYL BENZENE
20U	STYRENE
20U	TOTAL XYLENES
51	PERCENT MOISTURE
•••REMARKS***	•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
«THENS, GA.

12.
•• PROJECT NO. 94-0036 SAMPLE NO. 80508
•• SOURCE: TOWER CHEMICAL
*• STATION ID: 105-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/19/93
BY: B CARTER
ST: FL
1800 STOP: 00/00/00
* *
* *
* *
•~ CASE NO.: 21073
SAS NO.: 8175D
D. NO.: FQ15

* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
23U
CHLOROMETHANE
23U
1.2-DICHLOROPROPANE
23U
BROMOMETHANE
23U
CIS-1 . 3-DICHLOROPROPENE
23U
VINYL CHLORIDE
23U
TRICHLOROETHENE(TRICHLOROETHYLENE )
23U
CHLOROETHANE
23U
DIBROMOCHLOROME THANE
70U
METHYLENE CHLORIDE
23U
1.1.2-TRICHLOROETHANE
23U
ACETONE
23U
BENZENE
23U
CARBON DISULFIDE
23U
TRANS-1.3-DICHLOROPROPENE
23U
1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
23U
BROMOFORM
23U
1.1-DICHLOROETHANE
23U
METHYL ISOBUTYL KETONE
23U
1.2-DICHLOROETHENE (TOTAL)
23U
METHYL BUTYL KETONE
23U
CHLOROFORM
23U
TE TRACHLOROETHENE(TETRACHLOROETHYLENE)
23U
1.2-DICHLOROETHANE
23U
1.1.2.2-TETRACHLOROETHANE
23U
METHYL ETHYL KETONE
23U
TOLUENE
23U
1.1.1-TRICHLOROETHANE
23U
CHLOROBENZENE
23U
CARBON TETRACHLORIDE
23U
ETHYL BENZENE
23U
BROMODICHLOROMETHANE
23U
STYRENE


23U
TOTAL XYLENES


57
PERCENT MOISTURE
•••REMARKS***	•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV Ei. 
-------
SAMPLE AND ANALYSl! IGEMENT SYSTEM
.. _	EPA-REGION IV L ATHENS. GA.
PURGEABLE ORGANICS DATA REPORT
•* PROJECT
*» SOURCE:
*« STATION
NO. 94-0036 SAMPLE NO. 80511
TOWER CHEMICAL
ID: 108-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/20/93
BY: B CARTER •*
ST: FL •*
1715 STOP: 00/00/00 •»
•* CASE NO
: 21073
SAS NO.: 8175D
D. NO.: F018
» *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
29U
CHLOROMETHANE
29U
1 , 2-DICHLOROPROPANE
29U
BROMOMETHANE
29U
CIS-1 .3-DICHLOROPROPENE
29U
VINYL CHLORIDE
29U
TRICHLOROETHENE(TRICHLOROETHYLENE)
29U
CHLOROETHANE
29U
DIBROMOCHLOROME THANE
29U
METHYLENE CHLORIDE
29U
1.1,2-TRICHLOROETHANE
32N
ACETONE
29U
BENZENE
29U
CARBON DISULFIDE
29U
TRANS-1.3-DICHLOROPROPENE
29U
1,1-DICHLOROETHENE(1,1-DICHL0R0ETHYLENE)
29U
BROMOFORM
29U
1 ,1-DICHLOROETHANE
29U
METHYL ISOBUTYL KETONE
29U
1,2-DICHLOROETHENE (TOTAL)
29U
METHYL BUTYL KETONE
29U
CHLOROFORM
29U
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
29U
1 .2-DICHLOROETHANE
29U
1.1.2.2-TETRACHLOROETHANE
29U
METHYL ETHYL KETONE
29U
TOLUENE
29U
1.1,1-TRICHLOROETHANE
29U
CHLOROBENZENE
29U
CARBON TETRACHLORIDE
29U
ETHYL BENZENE
29U
BROMODICHLOROME THANE
29U
STYRENE


29U
TOTAL XYLENES


65
PERCENT MOISTURE
• ••REMARKS***	•••REMARKS*»»
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SVSTEM
PURGEABLE ORGANIC* DATA REPORT	EPA-REGION IV E- «THENS. GA.	12.
»~ PROJECT
•• SOURCE:
** STATION
NO. 94-0036 SAMPLE NO. 80513
TOWER CHEMICAL
ID: 109-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER ••
ST: FL **
1700 STOP: 00/00/00 ••
CASE NO
: 21073
SAS NO.: 8175D
D. NO.: F020
* t
UG/KG	ANALYTICAL RESULTS
120U	CHLOROMETHANE
120U	BROMOMETHANE
120U	VINYL CHLORIDE
120U	CHLOROETHANE
120U	METHYLENE CHLORIDE
260N	ACETONE
120U	CARBON DISULFIDE
120U	1.1-DICHLOROETHENE(1.1-DICHLOROETHYLENE)
120U	1 .1-DICHLOROE THANE
120U	1.2-DICHLOROETHENE (TOTAL)
120U	CHLOROFORM
120U	1.2-DICHLOROE THANE
120U	METHYL ETHYL KETONE
120U	1.1.1-TRICHLOROETHANE
120U	CARBON TETRACHLORIDE
120U	BROMODICHLOROME THANE
UG/KG	ANALYTICAL RESULTS
120U	1.2-DICHLOROPROPANE
120U	CIS-1,3-DICHLOROPROPENE
120U	TRICHLOROETHENE(TRICHLOROETHYLENE)
120U	DIBROMOCHLOROMETHANE
120U	1.1.2-TRICHLOROETHANE
120U	BENZENE
120U	TRANS-1.3-DICHLOROPROPENE
120U	BROMOFORM
120U	METHYL ISOBUTYL KETONE
120U	METHYL BUTYL KETONE
120U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
120U	1,1.2.2-TETRACHLOROETHANE
120U	TOLUENE
120U	CHLOROBENZENE
120U	ETHYL BENZENE
120U	STYRENE
120U	TOTAL XYLENES
92	PERCENT MOISTURE
*»'REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE OkGANICS DATA REPORT
SAMPLE AND ANALYST' VGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.
1. 33
PROJECT NO. 94-0036 SAMPLE NO. 80514 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 110-SD
CASE NO.: 21073
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP: 00/00/00
D. NO.: FQ21
UG/KG	ANALYTICAL RESULTS
91U	CHLOROMETHANE
91U	BROMOMETHANE
91U	VINYL CHLORIDE
91U	CHLOROETHANE
91U	METHYLENE CHLORIDE
91U	ACETONE
13J	CARBON DISULFIDE
91U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
91U	1.1-DICHLOROETHANE
91U	1,2-DICHLOROETHENE (TOTAL)
91U	CHLOROFORM
91U	1.2-DICHLOROETHANE
91U	METHYL ETHYL KETONE
91U	1,1.1-TRICHLOROETHANE
91U	CARBON TETRACHLORIDE
91U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
91U	1,2-DICHLOROPROPANE
91U	CIS-1.3-DICHL0R0PR0PENE
91U	TRICHLOROETHENE(TRICHLOROETHYLENE)
91U	DIBROMOCHLOROMETHANE
91U	1.1.2-TRICHLOROETHANE
91U	BENZENE
91U	TRANS-1.3-DICHL0R0PR0PENE
91U	BROMOFORM
91U	METHYL ISOBUTYL KETONE
91U	METHYL BUTYL KETONE
91U	TETRACHLOROETHENE( TETRACHLOROETHYLENE)
91U	1.1.2.2-TETRACHLOROETHANE
91U	TOLUENE
91U	CHLOROBENZENE
91U	ETHYL BENZENE
91U	STYRENE
91U	TOTAL XYLENES
89	PERCENT MOISTURE
••~REMARKS***
*•"REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
3EMENT SYSTEM
.THENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80515
SOURCE: TOWER CHEMICAL
STATION ID: 111-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1718 STOP: 00/00/00
D. NO.: FQ22
UG/KG	ANALYTICAL RESULTS
100U	CHLOROMETHANE
100U	BROMOMETHANE
100U	VINYL CHLORIDE
100U	CHLOROETHANE
100U	METHYLENE CHLORIDE
670	ACETONE
78J	CARBON DISULFIDE
100U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
100U	1.1-DICHLOROETHANE
100U	1.2-DICHLOROETHENE (TOTAL)
100U	CHLOROFORM
1OOU	1.2-DICHLOROETHANE
160	METHYL ETHYL KETONE
100U	1.1,1-TRICHLOROETHANE
100U	CARBON TETRACHLORIDE
100U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
1OOU	1,2-DICHLOROPROPANE
1OOU	CIS-1.3-DICHLOROPROPENE
100U	TRICHLOROETHENE(TRICHLOROETHYLENE)
100U	DIBROMOCHLOROMETHANE
100U	1.1.2-TRICHLOROETHANE
100U	BENZENE
100U	TRANS-1.3-DICHL0R0PR0PENE
100U	BROMOFORM
100U	METHYL ISOBUTYL KETONE
100U	METHYL BUTYL KETONE
100U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
100U	1.1.2.2-TETRACHLOROETHANE
100U	TOLUENE
100U	CHLOROBENZENE
100U	ETHYL BENZENE
100U	STYRENE
100U	TOTAL XYLENES
90	PERCENT MOISTURE
•«'REMARKS*»*
••'REMARKS*»»
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSADLE COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE 0RGAN1CS DATA REPORT
SAMPLE AND ANALYSIJ GEMENT SYSTEM
EPA-REGION IV E aTHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80516
SOURCE: TOWER CHEMICAL
STATION ID: 112-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO. : 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1840 STOP: 00/00/00
D. NO.: FQ23
UG/KG	ANALYTICAL RESULTS
200U	CHLOROMETHANE
200U	BROMOMETHANE
200U	VINYL CHLORIDE
200U	CHLOROETHANE
200U	METHYLENE CHLORIDE
200U	ACETONE
200U	CARBON DISULFIDE
200U	1.1-DICHL0R0ETHENE(1,1-DICHLOROETHYLENE)
200U	1.1-DICHLOROETHANE
200U	1.2-DICHLOROETHENE (TOTAL)
200U	CHLOROFORM
200U	1.2-DICHLOROETHANE
200U	METHYL ETHYL KETONE
200U	1,1.1-TRICHLOROETHANE
200U	CARBON TETRACHLORIDE
200U	BR0M0D1CHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
200U	1,2-DICHLOROPROPANE
200U	CIS-1.3-DICHLOROPROPENE
200U	TRICHLOROETHENE(TRICHLOROETHYLENE)
200U	DIBROMOCHLOROMETHANE
200U	1.1.2-TRICHLOROETHANE
200U	BENZENE
20OU	TRANS-1.3-DICHLOROPROPENE
200U	BROMOFORM
200U	METHYL ISOBUTYL KETONE
200U	METHYL BUTYL KETONE
200U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
200U	1.1.2.2-TETRACHLOROETHANE
200U	TOLUENE
200U	CHLOROBENZENE
200U	ETHYL BENZENE
200U	STYRENE
200U	TOTAL XYLENES
95	PERCENT MOISTURE
•••REMARKS***
**'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSJ AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80517
SOURCE: TOWER CHEMICAL
STATION ID: 113-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 81750
PROG ELEM: SSF COLLECTED	BY: B CARTER
riTv- ri FpuntdT	^T* fi
COLLECTION START: 10/21/93 1827 STOP: 00/00/00
D. NO.: FQ24
UG/KG	ANALYTICAL RESULTS
170U	CHLOROMETHANE
170U	BROMOMETHANE
170U	VINYL CHLORIDE
170U	CHLOROETHANE
170U	METHYLENE CHLORIDE
170U	ACETONE
28J	CARBON DISULFIDE
170U	1,1-DICHL0R0ETHENE(1,1-DICHLOROETHYLENE)
170U	1,1-DICHLOROE THANE
170U	1.2-DICHLOROETHENE (TOTAL)
170U	CHLOROFORM
170U	1.2-DICHLOROETHANE
170U	METHYL ETHYL KETONE
170U	1.1.1-TRICHLOROE THANE
170U	CARBON TETRACHLORIDE
17OU	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
170U	1.2-DICHLOROPROPANE
170U	CIS-1,3-DICHLOROPROPENE
170U	TRICHLOROETHENE(TRICHLOROETHYLENE)
170U	DIBROMOCHLOROME THANE
170U	1,1.2-TRICHLOROETHANE
170U	BENZENE
170U	TRANS-J.3-DICHLOROPROPENE
170U	BROMOFORM
170U	METHYL ISOBUTYL KETONE
170U	METHYL BUTYL KETONE
170U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
170U	1.1,2. 2-TETRACHLOROETHANE
170U	TOLUENE
170U	CHLOROBENZENE
170U	ETHYL BENZENE
170U	STYRENE
170U	TOTAL XYLENES
94	PERCENT MOISTURE
•••REMARKS'**
••'REMARKS'••
•••FOOTNOTES'*•
•A-AVERAGE VALUE *NA-NOT ANALYZED 'NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE URGANICS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
IAGEMENT SYSTEM
ATHENS, GA.
/93
PROJECT NO. 94-0036 SAMPLE NO. 80518
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1813 STOP: 00/00/00
D. NO.: FQ25
UG/KG	ANALYTICAL RESULTS
110U	CHLOROMETHANE
11OU	BROMOMETHANE
110U	VINYL CHLORIDE
110U	CHLOROETHANE
110U	METHYLENE CHLORIDE
210	ACETONE
41J	CARBON DISULFIDE
110U	1.1-DICHL0R0ETHENE(1,1-DICHL0R0ETHYLENE)
110U	1.1-DICHLOROE THANE
110U	1.2-DICHL0R0ETHENE (TOTAL)
110U	CHLOROFORM
110U	1,2-DICHLOROE THANE
110U	METHYL ETHYL KETONE
110U	1.1.1-TRICHLOROETHANE
110U	CARBON TETRACHLORIDE
110U	BROMODICHLOROME THANE
UG/KG	ANALYTICAL RESULTS
11OU	1.2-DICHLOROPROPANE
110U	CIS-1.3-DICHLOROPROPENE
110U	TRICHLOROETHENE(TRICHLOROETHYLENE)
110U	DIBROMOCHLOROME THANE
110U	1.1.2-TRICHLOROETHANE
11OU	BENZENE
11OU	TRANS-1.3-DICHLOROPROPENE
11OU	BROMOFORM
110U	METHYL ISOBUTYL KETONE
110U	METHYL BUTYL KETONE
110U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
110U	1,1.2.2-TETRACHLOROETHANE
11OU	TOLUENE
110U	CHLOROBENZENE
110U	ETHYL BENZENE
110U	STYRENE
110U	TOTAL XYLENES
91	PERCENT MOISTURE
•••REMARKS***
•••remarks***
• "FOOTNOTES* *»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
3EMENT SYSTEM
.THENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80521
SOURCE: TOWER CHEMICAL
STATION ID. 115-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1230 STOP: 00/00/00
D. NO.: FQ30
UG/KG	ANALYTICAL RESULTS
140U	CHLOROMETHANE
140U	BROMOMETHANE
140U	VINYL CHLORIDE
140U	CHLOROETHANE
140U	METHYLENE CHLORIDE
140U	ACETONE
140U	CARBON DISULFIDE
140U	1.1-DICHLOROETHENE(1.1-DICHLOROETHYLENE)
140U	1.1-DICHLOROE THANE
140U	1.2-DICHLOROETHENE (TOTAL)
140U	CHLOROFORM
140U	1.2-DICHLOROE THANE
140U	METHYL ETHYL KETONE
140U	1,1,1-TRICHLOROETHANE
140U	CARBON TETRACHLORIDE
140U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
140U	1.2-DICHLOROPROPANE
140U	CIS-1.3-DICHLOROPROPENE
140U	TRICHLOROETHENE(TRICHLOROETHYLENE)
140U	DIBROMOCHLOROMETHANE
140U	1.1.2-TRICHLOROETHANE
140U	BENZENE
140U	TRANS-1,3-DICHLOROPROPENE
140U	BROMOFORM
140U	METHYL ISOBUTYL KETONE
140U	METHYL BUTYL KETONE
140U	T E T RACHLOROE THENE(T E TRACHLOROE THYLENE)
140U	1.1,2.2-TETRACHLOROETHANE
140U	TOLUENE
140U	CHLOROBENZENE
140U	ETHYL BENZENE
140U	STYRENE
140U	TOTAL XYLENES
93	PERCENT MOISTURE
•«»REMARKS»»»
**'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEA0LE 0RGAN1CS DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV t ,THENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80522
SOURCE: TOWER CHEMICAL
STATION ID: 116-SD
CASE NO.: 21073
SAMPLE TYPE: SOIL
SAS NO : 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1215 STOP: 00/00/00
D. NO.
F031
UG/KG	ANALYTICAL RESULTS
77U	CHLOROMETHANE
77U	BROMOMETHANE
77U	VINYL CHLORIDE
77U	CHLOROETHANE
90U	METHYLENE CHLORIDE
77U	ACETONE
77U	CARBON DISULFIDE
77U	1.1-DICHLOROETHENEM.1-DICHLOROE THYLENE)
771)	1 . 1 -DI CHLOROE THANE
77U	1.2-DICHLOROETHENE (TOTAL)
77U	CHLOROFORM
77U	1.2-DICHLOROE THANE
77U	METHYL ETHYL KETONE
77U	1.1.1-TRICHLOROETHANE
77U	CARBON TETRACHLORIDE
77U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
77U	1,2-DlCHLOROPROPANE
77U	CIS-1,3-DICHLOROPROPENE
77U	TRICHLOROETHENE(TRICHLOROETHYLENE)
77U	DIBROMOCHLOROMETHANE
77U	1.1.2-TRICHLOROETHANE
77U	BENZENE
77U	TRANS-1,3-DICHLOROPROPENE
77U	BROMOFORM
77U	METHYL ISOBUTYL KETONE
77U	METHYL BUTYL KETONE
77U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
77U	1.1,2.2-TETRACHLOROETHANE
77U	TOLUENE
77U	CHLOROBENZENE
77U	ETHYL BENZENE
77U	STYRENE
77U	TOTAL XYLENES
87	PERCENT MOISTURE
•••REMARKS***
•••REMARKS'**
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI? \GEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80523 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 117-SD
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
CASE NO.: 21073
SAS NO.: 8175D
D. NO.
FQ32
UG/KG	ANALYTICAL RESULTS
140U	CHLOROMETHANE
140U	BROMOMETHANE
140U	VINYL CHLORIDE
140U	CHLOROETHANE
140U	METHYLENE CHLORIDE
140U	ACETONE
140U	CARBON DISULFIDE
140U	1.1-DICHL0R0ETHENE(1,1-DICHL0R0ETHYLENE)
140U	1.1-DICHLOROE THANE
140U	1,2-DICHLOROETHENE (TOTAL)
140U	CHLOROFORM
140U	1.2-DICHLOROETHANE
140U	METHYL ETHYL KETONE
140U	1.1,1-TRICHL0R0ETHANE
140U	CARBON TETRACHLORIDE
140U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
140U	1.2-DICHLOROPROPANE
140U	CIS-1,3-DICHLOROPROPENE
140U	TRICHLOROETHENE(TRICHLOROETHYLENE)
140U	DIBROMOCHLOROMETHANE
140U	1.1 .2-TRICHLOROETHANE
140U	BENZENE
140U	TRANS-1.3-DICHLOROPROPENE
140U	BROMOFORM
140U	METHYL ISOBUTYL KETONE
140U	METHYL BUTYL KETONE
140U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
140U	1.1.2.2-TETRACHLOROETHANE
140U	TOLUENE
140U	CHLOROBENZENE
140U	ETHYL BENZENE
140U	STYRENE
140U	TOTAL XYLENES
93	PERCENT MOISTURE
•••REMARKS***
•••remarks***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYST. .GEMENT SYSTEM
EPA-REGION IV t ATHENS, GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80501
SOURCE: TOWER CHEMICAL
STATION ID: 102-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1230 STOP:
D. NO. : FQ08
00/00/00
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
10U	CARBON DISULFIDE
10U	1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1,2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1,2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1.1,1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
1OU 1.2-DICHLOROPROPANE
1OU CIS-1.3-DICHLOROPROPENE
10U	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
**'REMARKS***
• "REMARKS'"
••~FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYS IAGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
/93
PROJECT NO. 94-0036 SAMPLE NO. 80499
SOURCE: TOWER CHEMICAL
STATION ID: 103-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/19/93 1055 STOP: 00/00/00
D. NO. : FQ06
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
16	CARBON DISULFIDE
10U	1. 1-DICHLOROETHENEU.1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-01CHLOROE THANE
10U	METHYL ETHYL KETONE
10U	1,1.1-TRICHLOROE THANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
10U	1 .2-DICHLOROPROPANE
1OU	CIS-1.3-DICHLOROPROPENE
10U	TRICHLOROETHENE(TRICHLOROETHYLENE )
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHLOROETHANE
10U	BENZENE
1OU	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
••'REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND RCANALYSIS IS NECESSARY TOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI5 GEMENT SYSTEM
EPA-REGION IV E .THENS, GA.
PROJECT NO. 94-0036 SAMPLE NO.
SOURCE: TOWER CHEMICAL
STATION ID: 104-SW
CASE NO.: 21073
80505 SAMPLE TYPE: SURFACEWA
SAS NO. 8175D
PROG ELEM: SSF COLLECTED	BY: B CARTER
riTv- ri FPunkJT	qt« fi
COLLECTION START. 10/19/93	1735 STOP: 00/00/00
D. NO.: FQ12
UG/L
ANALYTICAL RESULTS
UG/L
ANALYTICAL RESULTS
10U
CHLOROMETHANE
10U
1.2-DICHLOROPROPANE
10U
BROMOMETHANE
10U
CIS-1.3-DICHLOROPROPENE
10U
VINYL CHLORIDE
10U
TRICHLOROETHENE(TRICHLOROETHYLENE)
10U
CHLOROETHANE
10U
DIBROMOCHLOROME THANE
10U
METHYLENE CHLORIDE
10U
1 . 1 . 2-TRICHLOROETHANE
10U
ACETONE
10U
BENZENE
10U
CARBON DISULFIDE
10U
TRANS-1.3-DICHLOROPROPENE
10U
1.1-DICHL0R0ETHENE(1,1-DICHLOROETHYLENE)
10U
BROMOFORM
10U
1.1-DICHLOROETHANE
10U
METHYL ISOBUTYL KETONE
10U
1.2-DICHL0R0ETHENE (TOTAL)
10U
METHYL BUTYL KETONE
10U
CHLOROFORM
10U
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U
1 .2-DICHLOROETHANE
10U
1.1.2. 2-TETRACHLOROETHANE
10U
METHYL ETHYL KETONE
10U
TOLUENE
10U
1.1.1-TRICHLOROETHANE
10U
CHLOROBENZENE
10UR
CARBON TETRACHLORIDE
10U
ETHYL BENZENE
10U
BROMODICHLOROME THANE
10U
STYRENE


10U
TOTAL XYLENES
»«'REMARKS*••
•••remarks***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~ R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI 4GEMENT SYSTEM
EPA-REGION IV L. ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80507
SOURCE: TOWER CHEMICAL
STATION ID: 105-SWM
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
D. NO.: F014
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
11	CARBON DISULFIDE
10U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1,2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1.1.1-TRICHLOROE THANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
1OU 1.2-DICHLOROPROPANE
10U CIS-1,3-DICHLOROPROPENE
10U TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1,2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1,3-DICHLOROPROPENE
1OU	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1,2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
»*'REMARKS*«»
»•'REMARKS*»«
•*»FOOTNOTES*•*
~A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
~R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE URGANICS DATA REPORT
SAMPLE AND ANALYS' 1AGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.
93
PROJECT NO. 94-0036 SAMPLE NO.
SOURCE: TOWER CHEMICAL
STATION ID. 106-SW
CASE NO.: 21073
80512 SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM. SSF COLLECTED BY: B CARTER
CITY* CLERMONT	ST* FL
COLLECTION START: 10/20/93 1600 STOP: 00/00/00
D. NO. FQ19
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
6J	CARBON DISULFIDE
10U	1.1-DICHLOROETHENE(1.1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHLOROE THANE
10U	METHYL ETHYL KETONE
10U	1,1.1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
10U 1 ,2-DICHLOROPROPANE
1OU CIS-1.3-DICHLOROPROPENE
10U TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHL0R0ETHANE
10U	BENZENE
10U	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1,1,2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHL0R0BEN2ENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
•••REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI! CEMENT SYSTEM
EPA-REGION IV I ATHENS. GA.
93
PROJECT NO. 94-0036 SAMPLE NO. 80510
SOURCE: TOWER CHEMICAL
STATION ID: 108-SW
CASE NO.
UG/L
21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1715 STOP: 00/00/00
D. NO.: F017
ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOME THANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
2J	CARBON DISULFIDE
10U	1,1-DICHL0R0ETHENE(1.1-DICHL0R0ETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1.1.1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
10U 1,2-DICHLOROPROPANE
1OU CIS-1.3-DICHLOROPROPENE
10U	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	01BROMOCHLOROMETHANE
10U	1,1.2-TRICHL0R0ETHANE
10U	BENZENE
1OU	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
•••REMARKS***
»•'REMARKS*••
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
'AGEMENT SYSTEM
ATHENS, GA.
93
PROJECT NO. 94-0036 SAMPLE NO.
SOURCE: TOWER CHEMICAL
STATION ID: 111-SW
CASE NO.: 21073
80520 SAMPLE TYPE: SURFACEWA
SAS NO.: 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1557 STOP: 00/00/00
D. NO.
F028
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
10U	CARBON DISULFIDE
10U	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1 ,1,1-TRICHLOROE THANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
1OU 1,2-DICHLOROPROPANE
1OU	CIS-1.3-DICHLOROPROPENE
10U	TRICHLOROE THENE(TRICHLOROE THYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHLOROETHANE
10U	BENZENE
1OU	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
1OU	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHL0R0BEN2ENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
»•'REMARKS*»«
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI >GEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
1 93
PROJECT NO. 94-0036 SAMPLE NO. 80519
SOURCE: TOWER CHEMICAL
STATION ID: 114-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1803 STOP:
D. NO.: FQ26
00/00/00
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
10U	CARBON DISULFIDE
10U	1.1-DICHLOROETHENEO.1-DICHLOROE THYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
1OU	1.2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1,1,1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
10U 1,2-DICHLOROPROPANE
1OU CIS-1.3-DICHLOROPROPENE
1OU	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1.2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1.3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1 .2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
••"REMARKS*••
•••REMARKS***
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV t THENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80525
SOURCE: TOWER CHEMICAL
STATION ID: 117-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/21/93 1140 STOP: 00/00/00
0. NO.: F034
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
10U	CARBON DISULFIDE
10U	1.1-DICHLOROETHENEC1.1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHL0R0ETHANE
10U	METHYL ETHYL KETONE
10U	1,1,1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
1OU	1,2-DICHLOROPROPANE
1OU	CIS-1.3-DICHLOROPROPENE
1OU	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1.1,2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1.3-DICHL0R0PR0PENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
10U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHL0R08ENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
«»'REMARKS*••
*«'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION
-------
PURGEABLE ORGAN!CS DATA REPORT
SAMPLE AND ANALYST VGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
1 93
PROJECT NO. 94-0036 SAMPLE NO. 80526
SOURCE: TOWER CHEMICAL
STATION ID: 517-SW
CASE NO.: 21073
SAMPLE TYPE: SURFACEWA
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1140 STOP: 00/00/00
0. NO.: FQ35
UG/L	ANALYTICAL RESULTS
10U	CHLOROMETHANE
10U	BROMOMETHANE
10U	VINYL CHLORIDE
10U	CHLOROETHANE
10U	METHYLENE CHLORIDE
10U	ACETONE
10U	CARBON DISULFIDE
10U	1,1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
10U	1.1-DICHLOROE THANE
10U	1.2-DICHLOROETHENE (TOTAL)
10U	CHLOROFORM
10U	1.2-DICHLOROETHANE
10U	METHYL ETHYL KETONE
10U	1,1,1-TRICHLOROETHANE
10UR	CARBON TETRACHLORIDE
10U	BROMODICHLOROMETHANE
UG/L	ANALYTICAL RESULTS
1OU	1.2-DICHLOROPROPANE
10U	CIS-1,3-DICHLOROPROPENE
1OU	TRICHLOROETHENE(TRICHLOROETHYLENE)
10U	DIBROMOCHLOROMETHANE
10U	1,1,2-TRICHLOROETHANE
10U	BENZENE
10U	TRANS-1,3-DICHLOROPROPENE
10U	BROMOFORM
10U	METHYL ISOBUTYL KETONE
10U	METHYL BUTYL KETONE
1OU	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
10U	1.1.2.2-TETRACHLOROETHANE
10U	TOLUENE
10U	CHLOROBENZENE
10U	ETHYL BENZENE
10U	STYRENE
10U	TOTAL XYLENES
*•'REMARKS**•
«»"REMARKS***
**'FOOTNOTES**•
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI 4GEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.
1 93
PROJECT NO. 94-0036 SAMPLE NO. 80524 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 517-SD
CASE NO.: 21073
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1200 STOP: 00/00/00
D. NO.: F033
UG/KG	ANALYTICAL RESULTS
91U	CHLOROMETHANE
91U	BROMOMETHANE
91U	VINYL CHLORIDE
91U	CHLOROETHANE
91U	METHYLENE CHLORIDE
91U	ACETONE
91U	CARBON DISULFIDE
91U	1 .1-DICHL0R0ETHENE(1,1-DICHLOROETHYLENE)
91U	1.1-DICHLOROE THANE
91U	1.2-DICHLOROETHENE (TOTAL)
91U	CHLOROFORM
91U	1,2-DICHLOROE THANE
91U	METHYL ETHYL KETONE
91U	1.1.1-TRICHLOROETHANE
91U	CARBON TETRACHLORIDE
91U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
91U	1,2-DICHLOROPROPANE
91U	CIS-1,3-DICHLOROPROPENE
91U	TRICHLOROETHENE(TRICHLOROETHYLENE)
91U	DIBROMOCHLOROMETHANE
91U	1.1,2-TRICHLOROETHANE
91U	BENZENE
91U	TRANS-1,3-DICHLOROPROPENE
91U	BROMOFORM
91U	METHYL ISOBUTYL KETONE
91U	METHYL BUTYL KETONE
91U	TE TRACHLOROETHENE(TETRACHLOROETHYLENE)
91U	1.1.2. 2-TETRACHLOROETHANE
91U	TOLUENE
91U	CHLOROBENZENE
91U	ETHYL BENZENE
91U	STYRENE
91U	TOTAL XYLENES
89	PERCENT MOISTURE
««'REMARKS*»*
•••REMARKS***
*•'FOOTNOTES**•
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E »THENS¦ GA.
1i. J3
PROJECT NO. 94-0036 SAMPLE NO.
SOURCE: TOWER CHEMICAL
STATION ID: 118-SD
CASE NO.: 21073
80527 SAMPLE TYPE: SOIL
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
PTTV* ri FPftJDkJT	ct • Fl
COLLECTION START: 10/21/93 1445 STOP: 00/00/00
D. NO.: FQ36
UG/KG	ANALYTICAL RESULTS
170U	CHLOROMETHANE
170U	BROMOMETHANE
170U	VINYL CHLORIDE
170U	CHLOROETHANE
170U	METHYLENE CHLORIDE
270N	ACETONE
170U	CARBON DISULFIDE
170U	1.1-DICHLOROETHENEC1.1-DICHLOROETHYLENE)
170U	1,1-DICHLOROE THANE
170U	1.2-DICHLOROETHENE (TOTAL)
170U	CHLOROFORM
170U	1.2-DICHLOROETHANE
170U	METHYL ETHYL KETONE
170U	1.1.1-TRICHLOROETHANE
170U	CARBON TETRACHLORIDE
170U	BROMODICHLOROME THANE
UG/KG	ANALYTICAL RESULTS
170U	1.2-DICHLOROPROPANE
170U	CIS-1.3-DICHL0R0PR0PENE
170U	TRICHLOROETHENE(TRICHLOROETHYLENE)
170U	DIBROMOCHLOROMETHANE
170U	1.1.2-TRICHLOROETHANE
170U	BENZENE
170U	TRANS-1.3-DICHL0R0PR0PENE
170U	BROMOFORM
170U	METHYL ISOBUTYL KETONE
17OU	METHYL BUTYL KETONE
170U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
170U	1.1.2.2-TETRACHLOROETHANE
170U	TOLUENE
170U	CHLOROBENZENE
170U	ETHYL BENZENE
170U	STYRENE
170U	TOTAL XYLENES
94	PERCENT MOISTURE
•••REMARKS***
• ••REMARKS"*
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE organics data report
SAMPLE AND ANALYSIS
EPA-REGION IV E
GEMENT SYSTEM
THENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80528 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 119-SD
CASE NO.: 21073
SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1430 STOP: 00/00/00
D. NO.: F037
UG/KG	ANALYTICAL RESULTS
100U	CHLOROMETHANE
100U	BROMOMETHANE
100U	VINYL CHLORIDE
100U	C.HLOROE THANE
100U	METHYLENE CHLORIDE
490N	ACETONE
100U	CARBON DISULFIDE
100U	1.1-DICHL0R0ETHENE(1.1-DICHLOROETHYLENE)
10OU	1.1-DICHLOROE THANE
100U	1,2-DICHLOROETHENE (TOTAL)
100U	CHLOROFORM
1OOU	1,2-DICHLOROETHANE
100U	METHYL ETHYL KETONE
100U	1,1.1-TRICHLOROETHANE
100U	CARBON TETRACHLORIDE
100U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
1OOU	1,2-DICHLOROPROPANE
100U	CIS-1,3-DICHLOROPROPENE
1OOU	TRICHLOROETHENE(TRICHLOROETHYLENE)
100U	DIBROMOCHLOROMETHANE
100U	1.1.2-TRICHL0R0ETHANE
100U	BENZENE
100U	TRANS-1,3-DICHL0R0PR0PENE
100U	BROMOFORM
100U	METHYL ISOBUTYL KETONE
100U	METHYL BUTYL KETONE
10OU	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
100U	1,1.2.2-TETRACHLOROETHANE
100U	TOLUENE
100U	CHLOROBENZENE
100U	ETHYL BENZENE
100U	STYRENE
100U	TOTAL XYLENES
90	PERCENT MOISTURE
»»"REMARKS*»»
*»'REMARKS'**
**'FOOTNOTES**»
»A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
...	^	EPA-REGION IV L ATHENS. GA.	1. 93
PURGEABLE ORGANtCS DATA REPORT
~* PROJECT
•* SOURCE:
~» STATION
NO. 94-0036 SAMPLE NO. 80529
TOWER CHEMICAL
ID. 120-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START. 10/21/93
BY: B CARTER »»
ST: FL **
1415 STOP. 00/00/00 »*
»* CASE NO
: 21073
SAS NO.: 8175D
D. NO.: F038
* *
UG/KG
ANALYTICAL RESULTS
UG/KG
ANALYTICAL RESULTS
120U
CHLOROMETHANE
120U
1.2-DICHL0R0PR0PANE
120U
BROMOMETHANE
120U
CIS-1.3-DICHL0R0PR0PENE
120U
VINYL CHLORIDE
120U
TRICHLOROETHENE(TRICHLOROETHYLENE)
120U
CHLOROETHANE
120U
DIBROMOCHLOROME THANE
120U
METHYLENE CHLORIDE
120U
1.1,2-TRICHLOROETHANE
120U
ACETONE
120U
BENZENE
51J
CARBON DISULFIDE
120U
TRANS-1.3-DICHLOROPROPENE
120U
1.1-DICHLOROETHENE(1.1-DICHLOROETHYLENE)
120U
BROMOFORM
120U
1.1-DICHLOROE THANE
120U
METHYL ISOBUTYL KETONE
120U
1.2-DICHLOROE THE NE (TOTAL)
120U
METHYL BUTYL KETONE
120U
CHLOROFORM
120U
TETRACHLOROETHENE(TETRACHLOROETHYLENE)
120U
1.2-DICHLOROETHANE
120U
1,1.2.2-TETRACHLOROETHANE
120U
METHYL ETHYL KETONE
120U
TOLUENE
120U
1.1.1-TRICHLOROETHANE
120U
CHLOROBENZENE
120U
CARBON TETRACHLORIDE
120U
ETHYL BENZENE
120U
BROMODICHLOROME THANE
120U
STYRENE


120U
TOTAL XYLENES


92
PERCENT MOISTURE
•••REMARKS***	•••REMARKS*"
•••FOOTNOTES***
~A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
PURGEABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
1 93
PROJECT NO. 94-0036 SAMPLE NO. 80530 SAMPLE TYPE. SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD
CASE NO.: 21073
SAS NO.: 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: EL
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D. NO.: F039
UG/KG	ANALYTICAL RESULTS
110U	CHLOROMETHANE
110U	BROMOMETHANE
110U	VINYL CHLORIDE
110U	CHLOROETHANE
110U	METHYLENE CHLORIDE
460N	ACETONE
36J	CARBON DISULFIDE
110U	1.1-DICHLOROETHENEC1,1-DICHLOROETHYLENE)
110U	1.1-DICHLOROE THANE
110U	1.2-DICHLOROETHENE (TOTAL)
110U	CHLOROFORM
110U	1 .2-DICHLOROETHANE
120	METHYL ETHYL KETONE
110U	1,1.1-TRICHLOROE THANE
110U	CARBON TETRACHLORIDE
110U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
11OU	1,2-DICHLOROPROPANE
110U	CIS-1.3-DICHLOROPROPENE
110U	TRICHLOROETHENE(TRICHLOROETHYLENE)
11OU	01BROMOCHLOROME THANE
110U	1,1.2-TRICHLOROETHANE
110U	BENZENE
110U	TRANS-1.3-DICHLOROPROPENE
11OU	BROMOFORM
110U	METHYL ISOBUTYL KETONE
110U	METHYL BUTYL KETONE
110U	TE TRACHLOROETHENE(TE TRACHLOROE THYLENE)
110U	1.1.2.2-TETRACHLOROETHANE
110U	TOLUENE
110U	CHL0R0BEN2ENE
110U	ETHYL BENZENE
110U	STYRENE
110U	TOTAL XYLENES
91	PERCENT MOISTURE
«»"REMARKS*«»
*»'REMARKS**•
•»'FOOTNOTES*»»
»A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. *THENS, GA.
PURGEABLE ORGAN1CS DATA REPORT
«* PROJECT
*~ SOURCE:
»* STATION
NO. 94-0036 SAMPLE NO. 80534
TOWER CHEMICAL
ID: 121-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER **
ST: FL ••
1830 STOP: 00/00/00 *•
»» CASE NO
: 21073
SAS NO.: 8175D
D. NO.: F043
9 *
UG/KG	ANALYTICAL RESULTS
14U	CHLOROMETHANE
14U	BROMOMETHANE
14U	VINYL CHLORIDE
14U	CHLOROETHANE
14U	METHYLENE CHLORIDE
14U	ACETONE
14U	CARBON DISULFIDE
14U	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
14U	1.1-DICHLOROE THANE
14U	1,2-DICHLOROETHENE (TOTAL)
14U	CHLOROFORM
14U	1.2-DICHLOROETHANE
14U	METHYL ETHYL KETONE
14U	1,1.1-TRICHLOROETHANE
14U	CARBON TETRACHLORIDE
14U	BROMODICHLOROMETHANE
UG/KG	ANALYTICAL RESULTS
14U	1,2-DICHLOROPROPANE
14U	CIS-1.3-DICHL0R0PR0PENE
14U	TRICHLOROETHENE(TRICHLOROETHYLENE)
14U	DIBROMOCHLOROMETHANE
14U	1,1,2-TRICHLOROETHANE
14U	BENZENE
14U	TRANS-1.3-DICHLOROPROPENE
14U	BROMOFORM
14U	METHYL ISOBUTYL KETONE
14U	METHYL BUTYL KETONE
14U	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
14U	1.1.2.2-TETRACHLOROETHANE
14U	TOLUENE
14U	CHLOROBENZENE
14U	ETHYL BENZENE
14U	STYRENE
14U	TOTAL XYLENES
30	PERCENT MOISTURE
•••FOOTNOTES*'*
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV E. .THENS. GA.
PURGEABLE ORGANICS DATA REPORT
»* PROJECT
•• SOORCE:
STATION
NO. 94-0036 SAMPLE NO. 80538
TOWER CHEMICAL
ID: 304-SD
SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER «»
ST: FL *«
1445 STOP: 00/00/00 »•
«• CASE NO.
: 21073
SAS NO.: 8175D
D. NO.: FQ29
* *
UG/KG	ANALYTICAL RESULTS
11U	CHLOROMETHANE
11U	BROMOMETHANE
11U	VINYL CHLORIDE
11U	CHLOROETHANE
110	METHYLENE CHLORIDE
11U	ACETONE
11U	CARBON DISULFIDE
11U	1.1-DICHLOROETHENE(1,1-DICHLOROETHYLENE)
11U	1.1-DICHLOROE THANE
11U	1.2-DICHLOROETHENE (TOTAL)
11U	CHLOROFORM
11U	1.2-DICHLOROETHANE
110	METHYL ETHYL KETONE
11U	1.1.1-TRICHLOROETHANE
11U	CARBON TETRACHLORIDE
11U	B ROMODICHLOROME T HANE
UG/KG	ANALYTICAL RESULTS
11U	1.2-DICHLOROPROPANE
11U	CIS-1,3-DICHLOROPROPENE
11U	TRICHLOROETHENE(TRICHLOROETHYLENE)
11U	DIBROMOCHLOROMETHANE
11U	1.1.2-TRICHLOROETHANE
11U	BENZENE
11U	TRANS-1.3-DICHLOROPROPENE
11U	BROMOFORM
110	METHYL 1S0BUTYL KETONE
11U	METHYL BUTYL KETONE
110	TETRACHLOROETHENE(TETRACHLOROETHYLENE)
11U	1.1,2,2-TETRACHLOROETHANE
11U	TOLUENE
11U	CHLOROBENZENE
11U	ETHYL BENZENE
11U	STYRENE
11U	TOTAL XYLENES
13	PERCENT MOISTURE
••~FOOTNOTES**•
•A-AVERAGE VALOE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTOAL VALUE IS KNOWN TO BE LESS THAN VALOE GIVEN »L-ACTUAL VALOE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•O-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMOM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNOSABLE. COMPOOND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Region IV
Environmental Services Division
College Station Road, Athens, Ga. 30613
~~~~~memorandum******
DATE: 12/10/93
SUBJECT: Results of Specified Analysis;
9A - 00 3 6 TOWER CHEMICAL
CLERMONT FL
CASE NO: 21073SAS NO: 6175D
FROM: Charles H. Hooper/^^^7/^,
Chief, Laboratory Evaluation/Quality Assurance Section
TO: DELBERT HICKS
Attached are the results of analysis of samples collected as part of
the subject project.
As a result of the Quality Assurance Review, certain data qualifiers
may have been placed on the data. Attached is a DATA QUALIFIER
REPORT which explains the reasons that these qualifiers were required.
If you have any questions please contact me.
ATTACHMENT
-------
INORGANIC DATA QUALIFIERS REPORT
Case Number: 8175D	
Project Number: 94-0036	
Site: Tower Chemical. Clermont. FL	
Element	Flap	Samples Affected	Regggn
No Data Qualifiers Applied
-------
SAMPLE AND ANALYSI
EPA-REGION IV L
\GEMENT SYSTEM
ATHENS, GA.
93
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80543 SAMPLE TYPE: SURFACEWA
SOURCE: TOWER CHEMICAL
STATION ID: 101SW
CASE.NO.: 21073	SAS NO.: 81750
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST: FL
COLLECTION START: 10/19/93 1520 STOP: 00/00/00
D. NO.:	MD NO: 1391
RESULTS UNITS PARAMETER
97 MG/L TOTAL ORGANIC CARBON
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *NrPR£SUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K.-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E fHENS. GA.
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO. 80541 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER »•
** SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL •»
*• STATION
ID: 102SW

COLLECTION START: 10/19/93
1230 STOP: 00/00/00 •»
»• CASE.NO
• •
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1389 »«
• »
RESULTS UNITS PARAMETER
65 MG/L TOTAL ORGANIC CARBON
»»'FOOTNOTES*»»
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV I ATHENS, GA.	1. J3
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80539 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER »»
*• SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL •*
»• STATION
ID: 103SW


COLLECTION START: 10/19/93
1055 STOP: 00/00/00 *«
»* CASE.NO
* •
: 21073 SAS
NO.
: 8175D
D. NO. :
MD NO: 1387
• *
RESULTS UNITS PARAMETER
44 MG/L TOTAL ORGANIC CARBON
~••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. «THENS, GA.
SPECIFIED ANALYSIS DATA REPORT
PROJECT
NO. 94-0036 SAMPLE
NO. 80545 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER "
»« SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL "
STATION
ID: 104SW

COLLECTION START: 10/19/93
1735 STOP: 00/00/00 •*
»» CASE.NO
t*
: 21073 SAS
NO.: 8175D
D. NO. :
MD NO: 1393 •«
• *
RESULTS UNITS PARAMETER
29 MG/L TOTAL ORGANIC CARBON
»•'FOOTNOTES'••
•A-AVERAGE VALUE 'NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. «THENS. GA.
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO. 80547 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
•* SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL *»
•* STATION
ID: 105SW

COLLECTION START: 10/19/93
1800 STOP: 00/00/00 **
•• CASE.NO
• *
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1395 «*
* *
RESULTS UNITS PARAMETER
27 MG/L TOTAL ORGANIC CARBON
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
E PA-REG I ON IV Ei, fHENS, GA.	12,
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80560 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 106-SW	COLLECTION START: 10/20/93 1600 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: MD NO: 1400
RESULTS UNITS PARAMETER
81 MG/L TOTAL ORGANIC CARBON
**"FOOTNOTES*»«
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ES 
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV Ei. iHENS. GA.	12,
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80568 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER »»
»» SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL »»
•• STATION
ID: 111-SW


COLLECTION START: 10/21/93
1557 STOP: 00/00/00 »*
•• CASE.NO
• •
: 21073 SAS
NO.
: 8175D
D . NO. :
MD NO: 1408 *»
« *
RESULTS UNITS PARAMETER
39 MG/L TOTAL ORGANIC CARBON
•*"FOOTNOTES**»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI \GEMENT SYSTEM
EPA-REGION IV I. ATHENS, GA.	93
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80567 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER •*
•• SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL ••
•• STATION
ID: 114-SW


COLLECTION START- 10/21/93
1803 STOP: 00/00/00 ••
•• CASE.NO
• •
: 21073 SAS
NO.
: 8175D
D. NO.:
MD NO: 1407 •*
• *
RESULTS UNITS PARAMETER
47 MG/L TOTAL ORGANIC CARBON
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV l ATHENS, GA.	1. 93
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO. 80575 SAMPLE TYPE. SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER «»
»» SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL * «
»» STATION
ID: 117-SW

COLLECTION START: 10/21/93
1140 STOP: 00/00/00 •*
•• CASE.NO
*»
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1413 »*
* •
RESULTS UNITS PARAMETER
61 MG/L TOTAL ORGANIC CARBON
**'FOOTNOTES*»•
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSIS	1EMENT SYSTEM
EPA-REGION IV ES CHENS, GA.
12,
PROJECT NO. 94-0036 SAMPLE NO. 80552 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 120-SW	COLLECTION START: 10/21/93 1350 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: MD NO: 1419
RESULTS UNITS PARAMETER
42 MG/L TOTAL ORGANIC CARBON
»»»FOOTNOTES»»»
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS	IMENT SYSTEM
EPA-REGrON IV ESl HENS, GA.	12/
SPECIFIED ANALYSIS DATA REPORT
** PROJECT
NO. 94-0036 SAMPLE
NO. 80553 SAMPLE TYPE: SURFACEWA
PROG ELEM: SSF COLLECTED
BY: B CARTER «•
•» SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL »»
•* STATION
ID: 520-SW

COLLECTION START: 10/21/93
1350 STOP: 00/00/00 ••
«» CASE.NO
* *
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1420 •»
* *
RESULTS UNITS PARAMETER
40 MG/L TOTAL ORGANIC CARBON
»»'FOOTNOTES*»»
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV t ATHENS, GA.
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80555 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: 121-SW	COLLECTION START: 10/22/93 1830 STOP: 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO.: MD NO: 1421
RESULTS UNITS PARAMETER
16 MG/L TOTAL ORGANIC CARBON
» * » FOOTNOTES* « »
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSH iGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
1. &
PROJECT NO. 94-0036 SAMPLE NO. 80569 SAMPLE TYPE:	SURFACEWA PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY. CLERMONT ST: FL
STATION ID: 303-SW	COLLECTION START: 10/21/93 1425 STOP- 00/00/00
CASE.NO.: 21073 SAS NO.: 8175D	D. NO. MD NO: 1385
RESULTS UNITS PARAMETER
1U MG/L TOTAL ORGANIC CARBON
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI5 .GEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
SPECIFIED ANALYSIS DATA REPORT
~~ PROJECT
NO. 94-0036 SAMPLE
NO. 80544 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL »«
•• STATION
ID: 101SD

COLLECTION START: 10/19/93
1520 STOP: 00/00/00 ••
~« CASE.NO
• *
: 21073 SAS
NO.: 8175D
D. NO. :
MD NO: 1392 «»
* *
RESULTS UNITS PARAMETER
28000 MG/KG TOTAL ORGANIC CARBON
0 % % MOISTURE
»•'FOOTNOTES'»»
•A-AVERAGE VALUE 'NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
3EMENT SYSTEM
•THENS, GA.
PROJECT NO. 94-O036 SAMPLE NO. 80542 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 102SD
CASE.NO.: 21073	SAS NO.: 8175D
COLLECTED BY: B CARTER
CITY: CLERMONT	ST PL
£°4inCTI0N START' 10/19/93 1230 STOP: 00/00/00
0 NO . :	MD NO: 1390
RESULTS UNITS PARAMETER
150000 MG/KG TOTAL ORGANIC CARBON
3 % X MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS SEMENT SYSTEM
EPA-REGION IV E- THENS. GA.	12.
SPECIFIED ANALYSIS DATA REPORT
•» PROJECT
NO. 94-0036 SAMPLE
NO.
80540 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER »»
•» SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL »«
*• STATION
ID: 103SD


COLLECTION START: 10/19/93
1055 STOP: 00/00/00 •*
»» CASE.NO
• *
: 21073 SAS
NO.
: 8175D
D. NO.:
MD NO: 1388 **
* *
RESULTS UNITS PARAMETER
580000 MG/KG TOTAL ORGANIC CARBON
14 % % MOISTURE
» "FOOTNOTES* »»
•A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. aTHENS. GA.
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80546 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 104SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1735 STOP: 00/00/00
D. NO.:	MD NO: 1394
RESULTS UNITS PARAMETER
250000 MG/KG TOTAL ORGANIC CARBON
0%\ % X MOISTURE
~A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------


SAMPLE AND ANALYSIS
EMENT SYSTEM




EPA-REGION IV ESl
.HENS. GA.

12/
SPECIFIED ANALYSIS DATA REPORT





~» PROJECT NO. 94-0036 SAMPLE
NO.
80548 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER
**
»• SOURCE: TOWER CHEMICAL


CITY. CLERMONT
ST: FL
* *
*• STATION ID: 105SD


COLLECTION START: 10/19/93
1800 STOP: 00/00/00
* «
** CASE.NO.: 21073 SAS
* *
NO.
: 8175D
D. NO.:
MD NO: 1396
* *
* *
RESULTS UNITS PARAMETER
170000 MG/KG TOTAL ORGANIC CARBON
1 % % MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV I ATHENS, GA.	1. 93
SPECIFIED ANALYSIS DATA REPORT
•» PROJECT
NO. 94-0036 SAMPLE
NO. 80557 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER »•
•» SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL »•
•* STATION
ID: 106-SD

COLLECTION START: 10/20/93
1510 STOP: 00/00/00 *•
»» CASE.NO
• *
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1397 «»
* *
RESULTS UNITS PARAMETER
590000 MG/KG TOTAL ORGANIC CARBON
41 % X MOISTURE
»»'FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYS MAGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	,/93
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80559 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER »»
*» SOURCE.
TOWER CHEMICAL


CITY: CLERMONT
ST: FL **
*« STATION
ID: 108-SD


COLLECTION START: 10/20/93
1715 STOP: 00/00/00 »•
»• CASE.NO
*•
: 21073 SAS
NO.
: 8175D
D. NO.:
MD NO: 1399 »»
* *
RESULTS UNITS PARAMETER
82000 MG/KG TOTAL ORGANIC CARBON
2 % % MOISTURE
««'FOOTNOTES*••
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
•THENS. GA.

PROJECT NO. 94-0036 SAMPLE NO. 80561 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 109-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1700 STOP: 00/00/00
D. NO. :	MD NO: 1401
RESULTS UNITS PARAMETER
480000 MG/KG TOTAL ORGANIC CARBON
36 % % MOISTURE
«•'FOOTNOTES*»»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	93
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80562 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 110-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1625 STOP: 00/00/00
D. NO.:	MD NO: 1402
RESULTS UNITS PARAMETER
570000 MG/KG TOTAL ORGANIC CARBON
49 % % MOISTURE
•»»FOOTNOTES»««
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI! iGEMENT SYSTEM
EPA-REGION IV t ATHENS. GA.
SPECIFIED ANALYSIS DATA REPORT
•* PROJECT
NO. 94-0036 SAMPLE
NO. 80563 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER •*
»~ SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL «*
»* STATION
ID: 111-SD

COLLECTION START: 10/21/93
1718 STOP: 00/00/00 •*
** CASE.NO
* •
: 21073 SAS
NO.: 8175D
D. NO. :
MD NO: 1403 •*
• *
RESULTS UNITS PARAMETER
690000 MG/KG TOTAL ORGANIC CARBON
49 % X MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYST. .GEMENT SYSTEM
EPA-REGION IV E. /ATHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80564 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 112-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1840 STOP: 00/00/00
D NO.:	MD NO: 1404
RESULTS UNITS PARAMETER
430000 MG/KG TOTAL ORGANIC CARBON
13 % % MOISTURE
•••FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV Ei CHENS, GA.
PROJECT NO. 94-0036 SAMPLE NO. 80565 SAMPLE TYPE: SOIL
SOURCE. TOWER CHEMICAL
STATION ID: 113-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	21/g3	STOP: 00/00/00
COLLECTION START: 10/2'/93 i»^	5
D. NO.:
RESULTS UNITS PARAMETER
530000 MG/KG TOTAL ORGANIC CARBON
11 % % MOISTURE
••'FOOTNOTES*••
~A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSI: tGEMENT SYSTEM
EPA-REGION IV t. ATHENS. GA.
PROJECT NO. 94-0036 SAMPLE NO. 80566 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 114-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1813 STOP: 00/00/00
D. NO.:	MD NO: 1406
RESULTS UNITS PARAMETER
590000 MG/KG TOTAL ORGANIC CARBON
37 % % MOISTURE
*•'FOOTNOTES*»»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS jEMENT SYSTEM
EPA-REGION IV El .THENS, GA.
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80571 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 115-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1230 STOP: 00/00/00
D. NO.:	MD NO: 1409
RESULTS UNITS PARAMETER
600000 MG/KG TOTAL ORGANIC CARBON
46 % % MOISTURE
*»'FOOTNOTES**»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E- ATHENS, GA.	Ik. J3
SPECIFIED ANALYSIS DATA REPORT
•* PROJECT
NO. 94-0036 SAMPLE
NO.
80572 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER •*
»* SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL ««
STATION
ID: 116-SD


COLLECTION START: 10/21/93
1215 STOP: 00/00/00 •»
•« CASE.NO
* •
: 21073 SAS
NO.
: 8175D
D NO . :
MD NO: 1410 »*
* *
RESULTS UNITS PARAMETER
310000 MG/KG TOTAL ORGANIC CARBON
20 % X MOISTURE
•»*F00TN0TES»»«
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES. /HENS. GA.
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80573 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER •»
•» SOURCE:
TOWER CHEMICAL


CITY: CLERMONT
ST: FL *»
•* STATION
ID: 117-SD


COLLECTION START: 10/21/93
1200 STOP: 00/00/00 *»
*« CASE.NO
• *
: 21073 SAS
NO.
: 8175D
D . NO. :
MD NO: 1411 «»
* *
RESULTS UNITS PARAMETER
540000 MG/KG TOTAL ORGANIC CARBON
14 % % MOISTURE
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------


SAMPLE AND ANALYSIS
\GEMENT SYSTEM




EPA-REGION IV L
ATHENS. GA.

1.
SPECIFIED ANALYSIS DATA REPORT





•• PROJECT NO. 94-0036 SAMPLE
NO.
80574 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER
* *
•• SOURCE: TOWER CHEMICAL


CITY: CLERMONT
ST: FL
» *
»• STATION ID: 517-SD


COLLECTION START• 10/21/93
1200 STOP: 00/00/00
* *
•• CASE.NO.: 21073 SAS
• *
NO.
: 8175D
D. NO. :
MD NO: 1412
* *
• »
RESULTS UNITS PARAMETER
480000 MG/KG TOTAL ORGANIC CARBON
12 X X MOISTURE
*»'FOOTNOTES*»•
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV ES
EMENT SYSTEM
HENS. GA.
12
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0036 SAMPLE NO. 80576 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 118-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1445 STOP:
D. NO.:	MD NO: 1415
00/00/00
RESULTS UNITS PARAMETER
420000 MG/KG TOTAL ORGANIC CARBON
12 X X MOISTURE
***«A^AVERAGE*VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN .L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.	1. 93
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO. 80549 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER ••
»• SOURCE:
TOWER CHEMICAL

CITY. CLERMONT
ST. FL **
•• STATION
ID: 119-SD

COLLECTION START: 10/21/93
1430 STOP: 00/00/00 •*
•• CASE.NO
*»
: 21073 SAS
NO.: 8175D
D. NO.:
MD NO: 1416 **
* *
RESULTS UNITS PARAMETER
250000 MG/KG TOTAL ORGANIC CARBON
16 % X MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSH .GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
SPECIFIED ANALYSIS DATA REPORT
•• PROJECT
NO. 94-0036 SAMPLE
NO.
80550 SAMPLE TYPE: SOIL
PROG ELEM: SSF COLLECTED
BY: B CARTER *«
•* SOURCE.
TOWER CHEMICAL


CITY: CLERMONT
ST: FL *•
•• STATION
ID: 120-SD


COLLECTION START: 10/21/93
1415 STOP: 00/00/00 **
•• CASE.NO
• *
: 21073 SAS
NO.
: 8175D
D. NO.:
MD NO: 1417 **
* *



RESULTS UNITS
PARAMETER




480000 MG/KG
TOTAL ORGANIC CARBON




30 X
X MOISTURE

•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYSIS \GEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
1. ^3
PROJECT NO. 94-0036 SAMPLE NO. 80551 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 520-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1415 STOP: 00/00/00
D. NO.:	MD NO: 1418
RESULTS UNITS PARAMETER
530000 MG/KG TOTAL ORGANIC CARBON
43 % % MOISTURE
•«'FOOTNOTES*••
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYST CEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.
1. 93
PROJECT NO. 94-0036 SAMPLE NO. 80556 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 121-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/22/93 1830 STOP: 00/00/00
D. NO.:	MD NO: 1422
RESULTS UNITS PARAMETER
23000 MG/KG TOTAL ORGANIC CARBON
0 % X MOISTURE
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SPECIFIED ANALYSIS DATA REPORT
SAMPLE AND ANALYS1 AGEMENT SYSTEM
EPA-REGION IV . ATHENS. GA.
/93
PROJECT NO. 94-0036 SAMPLE NO. 80554 SAMPLE TYPE: SOIL
SOURCE: TOWER CHEMICAL
STATION ID: 303-SD
CASE.NO.: 21073	SAS NO.: 8175D
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1425 STOP: 00/00/00
D. NO.:	MD NO: 1386
RESULTS UNITS PARAMETER
34 MG/KG TOTAL ORGANIC CARBON
OX % MOISTURE
»•'FOOTNOTES*••
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
APPENDIX C
Chemical Analyses of Plant, Fish, and Alligator Tissue
-------
Alligator Tissue
Cross Reference for Sample/Station Identification
Station ID
(on lab data report)
Station ID 6 Location
(from Table 5)
34853
Orange Lake
34876
TC 111 - Lake Apopka at mouth
of unnamed stream
34877
TC 120 - Lake Apopka NE of
Crown Point
34878
TC 117 - Lake Apopka offshore
of muck farms
34879
TC 114 - Lake Apopka offshore
of citrus farms
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION IV
COLLEGE STATION RD.
ATHENS, GA. 30613
~~~~~memorandum******
DATE: 12/07/93
SUBJECT: Results of Metals Analysis;
9A - 0050 TOWER CHEMICAL
CLERMONT FL
Chief, Inorganic Ch	Section
Attached are the results of analysis of samples collected as part of
the subject project.
If you have any questions please contact me.
FROM: Mike Wasko, Chemist
TO: DELBERT HICKS
THRU: William H. McDaniel
ATTACHMENT
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV ES. ATHENS, GA.
12/ J3
PROJECT NO. 94-0050 SAMPLE NO. 80620
SOURCE: TOWER CHEMICAL
STATION ID: 34853L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
0. 331)
0.41U
NA
4.1
0.082U
0.082U
0.16U
0. 16U
22
0.16U
0.33U
0.08U
0.49U
1 . 1
0.41U
0.16U
0.82U
0.16U
1 . 6U
0. 16U
0. 16U
24
NA
0.95
2.0
0.38
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
47	CALCIUM
120	MAGNESIUM
220	IRON
870	SODIUM
2900	POTASSIUM
ANALYTICAL RESULTS
••'REMARKS***
•••REMARKS'**
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E- ATHENS, GA.	12, J3
METALS DATA REPORT
*• PROJECT
NO. 94-0050 SAMPLE
NO. 80621 SAMPLE TYPE. LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER **
*» SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL **
** STATION
* •
ID: 34876L ALLIGATOR
LIVER
COLLECTION START: 10/21/93
STOP: 00/00/00 **
* *
MG/KG
0.40U
0.20U
NA
0.25
0. 10U
0. 10U
0.20U
0.20U
11
0.20U
0.40U
0. 10U
0.60U
0.80
0.50U
0.20U
1 .OU
0.20U
2.0U
0.20U
0 20U
26
NA
0.07
2.0U
0 76
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
63
140
110
940
3100
CALCIUM
MAGNESIUM
IRON
SODIUM
POTASSIUM
ANALYTICAL RESULTS
•~•REMARKS***
**'REMARKS***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS CEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
li.. 93
PROJECT NO. 94-0050 SAMPLE NO. 80622
SOURCE: TOWER CHEMICAL
STATION ID. 34877L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
0.37U
0.46U
NA
0.28
0.092U
0.092U
0.18U
0.18U
30
0.18U
0.37U
0.09U
0.56U
1.3
0.46U
0.18U
0.92U
0.18U
1.8U
0.18U
0.18U
27
NA
0. 17
5.5
0.47
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
48	CALCIUM
130	MAGNESIUM
120	IRON
910	SODIUM
2900	POTASSIUM
ANALYTICAL RESULTS
•»'REMARKS*»•
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.	1i. J3
METALS DATA REPORT
•• PROJECT
NO. 94-0050 SAMPLE
NO. 80623 SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER **
•• SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL *•
•• STATION
• •
ID: 34878L ALLIGATOR
LIVER
COLLECTION START: 10/21/93
STOP: 00/00/00 * *
* *
MG/KG

0.35U
SILVER
0.43U
ARSENIC
NA
BORON
0.45
BARIUM
0.086U
BERYLLIUM
0.086U
CADMIUM
0. 17U
COBALT
0. 17U
CHROMIUM
16
COPPER
0.17U
MOLYBDENUM
0.35U
NICKEL
0.09U
LEAD
0.52U
ANTIMONY
0.83
SELENIUM
0.43U
TIN
0. 17U
STRONTIUM
0.86U
TELLURIUM
0. 17U
TITANIUM
1 . 7U
THALLIUM
0. 17U
VANADIUM
0 17U
YTTRIUM
22
ZINC
NA
ZIRCONIUM
0.23
MERCURY
1 .7U
ALUMINUM
0.67
MANGANESE
ANALYTICAL RESULTS
MG/KG
54	CALCIUM
120	MAGNESIUM
40	IRON
930	SODIUM
3000	POTASSIUM
ANALYTICAL RESULTS
•••REMARKS***
•••REMARKS'**
**'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ES. JHENS, GA.
12, 3
PROJECT NO. 94-0050 SAMPLE NO. 80624
SOURCE: TOWER CHEMICAL
STATION ID: 34879L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
0.40U
0.50U
NA
0.65
0.10U
0.10U
0.20U
0.20U
26
0.20U
0.40U
0.10U
0.60U
0.34
0.50U
0.20U
1 .OU
0.20U
2.0U
0.20U
0 20U
23
NA
0. 15
2.0U
0.89
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
59	CALCIUM
130	MAGNESIUM
31	IRON
1000	SODIUM
2800	POTASSIUM
ANALYTICAL RESULTS
•*»REMARKS*»«
**'REMARKS***
••~FOOTNOTES***
~A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYST. 4GEMENT SYSTEM
EPA-REGION IV E. ATHENS, GA.
12/ _^/93
PROJECT NO. 94-0050 SAMPLE NO. 80625 SAMPLE TYPE: FAT
SOURCE: TOWER CHEMICAL
STATION ID: 34853F ALLIGATOR FAT
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
0. 76U
0.95U
NA
1 .5
0. 19U
0. 19U
0.38U
0.38U
0.38U
0.38U
0 . 76U
0.20U
1 . 1U
1 .5U
0.95U
0.38U
1.9U
0.38U
3.8U
0.38U
0 38U
3. 7
NA
0.04
3.8U
0.38U
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
50	CALCIUM
26	MAGNESIUM
6.3	I RON
1000	SODIUM
440	POTASSIUM
ANALYTICAL RESULTS
••"REMARKS*••
•••REMARKS***
•••FOOTNOTES*•»
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT

SAMPLE AND ANALYSIS
EPA-REGION IV Ei>
3EMENT SYSTEM
.THENS. GA.

12/
»* PROJECT NO. 94-0050 SAMPLE
•• SOURCE: TOWER CHEMICAL
** STATION ID: 34876F ALLIGATOR
• »
NO. 80626
FAT
SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER
ST: FL
STOP: 00/00/00
* *
* *
• *
* *
MG/KG	ANALYTICAL RESULTS
0.83U
SILVER
1 .OU
ARSENIC
NA
BORON
0.41U
BARIUM
0.21U
BERYLLIUM
0.21U
CADMIUM
0.41U
COBALT
0.41U
CHROMIUM
0.41U
COPPER
0.41U
MOLYBDENUM
0 83U
NICKEL
0.21U
LEAD
1 . 2U
ANTIMONY
1 ,6U
SELENIUM
1 .OU
TIN
0.41U
STRONTIUM
2. 1U
TELLURIUM
0.41U
TITANIUM
4. 1U
THALLIUM
0.41U
VANADIUM
0 41U
YTTRIUM
2.8
ZINC
NA
ZIRCONIUM
0.02
MERCURY
4. 1U
ALUMINUM
0.41U
MANGANESE
«*»REMARKS*•«
MG/KG	ANALYTICAL RESULTS
32
CALCIUM
26
MAGNESIUM
3.2
IRON
700
SODIUM
500
POTASSIUM
•••REMARKS***
•••FOOTNOTES***
~A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYSI \GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
93
PROJECT NO. 94-0050 SAMPLE NO. 80627 SAMPLE TYPE: FAT
SOURCE: TOWER CHEMICAL
STATION ID: 34877F ALLIGATOR FAT
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY. CLERMONT	ST. FL
COLLECTION START: 10/21/93	STOP:
00/00/00
MG/KG
SILVER
1 . 4U
1 .8U
ARSENIC
NA
BORON
0.71U
BARIUM
0.35U
BERYLLIUM
0.35U
CADMIUM
0.71U
COBALT
0.71U
CHROMIUM
0.71U
COPPER
0.71U
MOLYBDENUM
1 ,4U
NICKEL
0.35U
LEAD
2. 1U
ANTIMONY
2.8U
SELENIUM
1 .8U
TIN
0.71U
STRONTIUM
3.5U
TELLURIUM
0.71U
TITANIUM
7. 1U
THALLIUM
0.71U
VANADIUM
0. 71U
VTTRIUM
4.6
ZINC
NA
ZIRCONIUM
0.02U
MERCURY
7. 1U
ALUMINUM
0. 71U
MANGANESE
ANALYTICAL RESULTS
MG/KG
66	CALCIUM
22	MAGNESIUM
4.6	I RON
1200	SODIUM
340	POTASSIUM
ANALYTICAL RESULTS
•»'REMARKS*•*
•••REMARKS***
•••footnotes***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSi JAGEMENT SYSTEM
EPA-REGION IV l- . ATHENS, GA.	,/93
METALS DATA REPORT
•* PROJECT
NO. 94-0050 SAMPLE
NO. 80628 SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED
BY: B CARTER **
*• SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL **
** STATION
• •
ID: 34878F ALLIGATOR
FAT
COLLECTION START: 10/21/93
STOP: 00/00/00 **
* *
MG/KG

1 ,4U
SILVER
1 . 7U
ARSENIC
NA
BORON
0.68U
BARIUM
0.34U
BERYLLIUM
0.34U
CADMIUM
0.68U
COBALT
0.68U
CHROMIUM
0.68U
COPPER
0.68U
MOLYBDENUM
1 . 4U
NICKEL
0.34U
LEAD
2.0U
ANTIMONY
2. 7U
SELENIUM
1 -7U
TIN
0.68U
STRONTIUM
3.4U
TELLURIUM
0.68U
TITANIUM
6.8U
THALLIUM
0.68U
VANADIUM
0.68U
YTTRIUM
5.0
ZINC
NA
ZIRCONIUM
0.03
MERCURY
6.8U
ALUMINUM
0.68U
MANGANESE
ANALYTICAL RESULTS
MG/KG
56	CALCIUM
16	MAGNESIUM
9 4	I RON
1100	SODIUM
230	POTASSIUM
ANALYTICAL RESULTS
•••REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYST. .GEMENT SYSTEM
EPA-REGION IV E~ ATHENS. GA.
1 93
PROJECT NO. 94-0050 SAMPLE NO. 80629 SAMPLE TYPE: FAT
SOURCE: TOWER CHEMICAL
STATION ID: 349879F ALLIGATOR FAT
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG

1 OU
SILVER
36
CALCIUM
0.45U
ARSENIC
20
MAGNESIUM
NA
BORON
2.5U
IRON
0.50U
BARIUM
820
SODIUM
0.25U
BERYLLIUM
380
POTASSIUM
0.25U
CADMIUM

0.50U
COBALT


0.50U
CHROMIUM


0. 50 U
COPPER


0.50U
MOLYBDENUM


1 .OU
NICKEL


0.25U
LEAD


1.5U
ANTIMONY


2.0U
SELENIUM


1 ,2U
TIN


0.50U
STRONTIUM


2.5U
TELLURIUM


0.50U
TITANIUM


5. OU
THALLIUM


0.50U
VANADIUM


O 50U
YTTRIUM


2.4
ZINC


NA
ZIRCONIUM


0.02U
MERCURY


8.0U
ALUMINUM


0.50U
MANGANESE


ANALYTICAL RESULTS
«•'REMARKS**«
•••REMARKS'**
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYS
EPA-REGION IV
aIAGEMENT SYSTEM
ATHENS. GA.
o/93
PROJECT NO. 94-0050 SAMPLE NO. 80630
SOURCE: TOWER CHEMICAL
STATION ID: TC104/105 GAMBUSIA
SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1130 STOP: 00/00/00

MG/KG

0. 71U
SILVER
2. 1U
ARSENIC
NA
BORON
3. 1
BARIUM
0.36U
BERYLLIUM
0.36U
CADMIUM
0.71U
COBALT
0.71U
CHROMIUM
1 .8
COPPER
0.71U
MOLYBDENUM
1 ,4U
NICKEL
0.09U
LEAD
2. 1U
ANTIMONY
2.8U
SELENIUM
1,8U
TIN
6.3
STRONTIUM
3.6U
TELLURIUM
0. 71U
TITANIUM
7. 1U
THALLIUM
0. 71U
VANADIUM
0. 71U
YTTRIUM
51
ZINC
NA
ZIRCONIUM
0.07
MERCURY
15
ALUMINUM
8 0
MANGANESE
**«*•*•***•*
ANALYTICAL RESULTS

*********
MG/KG
9000	CALCIUM
330	MAGNESIUM
23	IRON
770	SODIUM
2400	POTASSIUM
***••••***
ANALYTICAL RESULTS
* * * *
»»'REMARKS**8
**'REMARKS***
•••FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYS1
EPA-REGION IV
AGEMENT SYSTEM
ATHENS. GA.
/93
PROJECT NO. 94-0050 SAMPLE NO. 80631 SAMPLE TYPE: FISH
SOURCE: TOWER CHEMICAL
STATION ID: TC108 GAMBUSIA
PROG ELEM: SSF COLLECTED BY: 8 CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1315 STOP:
00/00/00
MG/KG

0.95U
SILVER
2.8U
ARSENIC
NA
BORON
7.8
BARIUM
0.48U
BERYLLIUM
0.48U
CADMIUM
0.95U
COBALT
0.95U
CHROMIUM
2.5
COPPER
0.95U
MOLYBDENUM
1 . 9U
NICKEL
0.09U
LEAD
2.8U
ANTIMONY
3.8U
SELENIUM
2.4U
TIN
11
STRONTIUM
4.8U
TELLURIUM
0.95U
TITANIUM
9.5U
THALLIUM
0.95U
VANADIUM
0.95U
YTTRIUM
68
ZINC
NA
ZIRCONIUM
0. 12
MERCURY
25
ALUMINUM
18
MANGANESE
ANALYTICAL RESULTS
MG/KG
14000	CALCIUM
410	MAGNESIUM
78	IRON
1200	SODIUM
2600	POTASSIUM
ANALYTICAL RESULTS
••~REMARKS'**
•••REMARKS***
••'FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND AMALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.	1. 93
METALS DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80632 SAMPLE TYPE: FISH	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: FL
STATION ID: TC111 GAMBUSIA	COLLECTION START: 10/22/93 1730 STOP. 00/00/00
MG/KG

0. 74U
SILVER
2.2U
ARSENIC
NA
BORON
2.3
BARIUM
0.37U
BERYLLIUM
0.37U
CADMIUM
0.74U
COBALT
0. 74U
CHROMIUM
1.8
COPPER
0.74U
MOLYBDENUM
1.5U
NICKEL
0.09U
LEAD
2.2U
ANTIMONY
3.0U
SELENIUM
1 .9U
TIN
13
STRONTIUM
3. 7U
TELLURIUM
0.74U
TITANIUM
7.4U
THALLIUM
0. 74U
VANADIUM
0. 74U
YTTRIUM
35
ZINC
NA
ZIRCONIUM
0.07 J
MERCURY
46
ALUMINUM
6.9
MANGANESE
ANALYTICAL RESULTS
MG/KG
8500	CALCIUM
370	MAGNESIUM
16	IRON
840	SODIUM
2500	POTASSIUM
ANALYTICAL RESULTS
••~REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYSE GEMENT SYSTEM
EPA-REGION IV t «THENS. GA.
PROJECT NO. 94-0050 SAMPLE NO. 80633 SAMPLE TYPE: FISH
SOURCE: TOWER CHEMICAL
STATION 10: TC121 MIXED FISH
PROG ELEM: SSF COLLECTED BY: B CARTER
COLLECTlON^START: 10/23/93 ?000 STOP: 00/00/00
MG/KG
0.93U
2.8U
NA
11
0.47U
0.47U
0.93U
0.93U
1.5
0.93U
1 . 9U
0.09U
2.8
3.	7U
2.3U
35
4.	7U
0.93U
9.3U
0.93U
O 93U
55
NA
0.07
34
8. 1
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
12000	CALCIUM
460	MAGNESIUM
24	IRON
1100	SODIUM
2800	POTASSIUM
ANALYTICAL RESULTS
•»'REMARKS*••
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
net., e n*-r*	EPA-REGION IV E- .THENS. GA.
METALS DATA REPORT
•• PROJECT
NO. 94-0050 SAMPLE NO. 80634 SAMPLE TYPE:
VEGETATION PROG ELEM: SSF COLLECTED
BY: B CARTER *•
•• SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL ••
•• STATION
• •
ID: TC101 SAURURUS
COLLECTION START: 10/21/93
1205 STOP: 00/00/00 *«
* t
MG/KG
0 19U
0.57U
NA
1 . 1
0.095U
0.095U
0.19U
0.19U
0. 79
0.19U
0. 381)
0. 101/
0.57U
0.76U
0.47U
1 .9
0.95U
0. 19U
1 . 9U
0.19U
O. 19U
4.7
NA
0.02
9.2
2.6
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
•••REMARKS***
MG/KG
460	CALCIUM
160	MAGNESIUM
30	I RON
370	SODIUM
4400	POTASSIUM
ANALYTICAL RESULTS
••'REMARKS**•
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALVSI AGEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.
1 93
PROJECT NO. 94-0050 SAMPLE NO. 80635 SAMPLE TYPE: VEGETATION PROG ELEM^SSF COLLECTED BY: SMARTER
i?ATIWI ID?ETC103MSAURURUS	COLLECTION START: 10/22/93 1215 STOP: 00/00/00

0.
0.
MG/KG
0.40U
0. 10U
NA
0.74
0.098U
0.098U
0.20U
0.20U
1.2
. 20U
. 39U
0.18
0.59 U
0.78U
0.49U
2.1
0.98U
0.35U
2.0U
0.20U
0.20U
9.6
NA
0.02U
40
11

SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS

MG/KG
1200	CALCIUM
370	MAGNESIUM
34	IRON
260	SODIUM
4300	POTASSIUM
* * *
• * *
ANALYTICAL RESULTS
•••REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYS. IAGEMENT SYSTEM
EPA-REGION IV	ATHENS, GA.	/93
METALS DATA REPORT
•* PROJECT
NO. 94-0050 SAMPLE NO. 80636 SAMPLE TYPE:
VEGETATION PROG ELEM: SSF COLLECTED
BY: B CARTER *•
•• SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL *•
~• STATION
* *
ID. TC105 SAURURUS
COLLECTION START: 10/19/93
1800 STOP. 00/00/00 »»
* *
MG/KG
0.40U
0. 10U
NA
0.61
0. 10U
0. 10U
0.20U
0.20U
0.84
0.20U
0.40U
0.12
0.60U
0.80U
0.50U
1 .8
1 .OU
0.20U
2.0U
0.20U
0.20U
5. 1
NA
0.02U
21
8.3
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
••'REMARKS'««
MG/KG
1000	CALCIUM
300	MAGNESIUM
31	IRON
310	SODIUM
3900	POTASSIUM
ANALYTICAL RESULTS
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.
93
PROJECT NO. 94-0050 SAMPLE NO. 80637
SOURCE: TOWER CHEMICAL
STATION ID: TC106 SAURURUS
SAMPLE TYPE: VEGETATION
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1510 STOP:
00/00/00
MG/KG
0.38U
0. 19U
NA
1 .4
0.094U
0.094U
0.19U
0.19U
0.82
0. 19U
0.38U
0.32
0.57U
0.75U
0.47U
2.2
0.94U
0.25
1 ,9U
0.19U
O. 19U
5.2
NA
0.02
31
17
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBOENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
1300	CALCIUM
400	MAGNESIUM
75	IRON
340	SODIUM
4000	POTASSIUM
ANALYTICAL RESULTS
«•'REMARKS*«»
•«'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
METALS DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. ATHENS. GA.
PROJECT NO. 94-0050 SAMPLE NO. 80638 SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: FL
STATION ID: TC108 SAURURUS	COLLECTION START: 10/21/93 1315 STOP:
00/00/00
MG/KG
0.38U
0.49
NA
1 .9
0.095U
0.095U
0. 19U
0.19U
0.36
0. 19U
0.38U
0.26
0.57U
0. 76U
0.47U
1.3
0.95U
0.19
1 . 9U
0. 19U
0. 19U
3.6
NA
0.2U
29
18
SILVER
ARSENIC
BORON
BARIUM
BERYLLIUM
CADMIUM
COBALT
CHROMIUM
COPPER
MOLYBDENUM
NICKEL
LEAD
ANTIMONY
SELENIUM
TIN
STRONTIUM
TELLURIUM
TITANIUM
THALLIUM
VANADIUM
YTTRIUM
ZINC
ZIRCONIUM
MERCURY
ALUMINUM
MANGANESE
ANALYTICAL RESULTS
MG/KG
560	CALCIUM
240	MAGNESIUM
530	IRON
270	SODIUM
3700	POTASSIUM
ANALYTICAL RESULTS
**'REMARKS***
•«'REMARKS*«•
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN "L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
PESTIC1DES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS W
EPA-REGION IV ESD.
MENT SYSTEM
(ENS. GA.
01/G
PROJECT NO. 94-0050 SAMPLE NO. 80620 SAMPLE TYPE: LIVER
SOURCE: TOWER CHEMICAL
STATION ID: 34853L ALLIGATOR LIVER
MG/KG
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0 014U
0.014U
0.014U
0 014U
0.035U
0.070U
0.070U
0.070U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
0.070U
0.070U
0.070U
0.070U
0.56U
/1
0.028U
0.014U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
*•'REMARKS***
»«»REMARKS»*«
•••footnotes***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSl
EPA-REGION IV L
VGEMENT SYSTEM
ATHENS. GA.
94
PROJECT NO. 94-0050 SAMPLE NO. 80625
SOURCE: TOWER CHEMICAL
STATION ID: 34853F ALLIGATOR FAT
SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP:
00/00/00
MG/KG
0.054U
0.054U
0.054U
0.054U
0.054U
0.054U
0.054U
0.054U
0.0541/
0.054U
0.047J
0.054U
0.054U
0.054U
0.054U
0.14U
0.27U
0.27U
0.27U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.27U
0.27U
0.27U
0.27U
2.2U
ANALYTICAL RESULTS
/1
0. 11U
0.054U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS***
•••REMARKS*'*
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
ATHENS. GA.
PROJECT NO. 94-0050 SAMPLE NO. 80621
SOURCE: TOWER CHEMICAL
STATION ID: 34876L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START. 10/21/93	STOP: 00/00/00
MG/KG
0.017U
0.017U
0.017U
0.017U
0.017U
0.017U
0.017U
0.017U
0.017U
0.017U
0.084
0.017U
0.017U
0.017U
0.017U
0.087U
0.087U
0.087U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
J
A)
/1
MG/KG
0.087U
0.087U
0.087U
0.087U
0.69U
0.0035U
0.0035U
0 0035U
0.0035U
0 0035U
0.0043J
0.0035U
0.0035U
0.0035U
0.035U
0.017U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS***
•••remarks***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E
GEMENT SYSTEM
.THENS. GA.
PROJECT NO. 94-0050 SAMPLE NO. 80626
SOURCE: TOWER CHEMICAL
STATION ID: 34876F ALLIGATOR FAT
SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP:
00/00/00
MG/KG
0. 12U
0.12U
0. 12U
0. 12U
0. 12U
0.12U
0. 12U
0. 12U
0.12U
0. 12U
4.7
0.12U
0.12U
0.12U
0.12U
2.5U
2. 5U
2. 5U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
/I
MG/KG
2.5U
2.5U
2.7
2.5U
9.8U
0. 12U
0. 12U
0. 12U
0.12U
012V
0. 12J
0. 12U
0 12U
0.068N
0 24U
0. 12U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
••~REMARKS***
•••remarks***
•••FOOTNOTES'**
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSI CEMENT SYSTEM
.. .	_	EPA-REGION IV i ATHENS. GA.	94
PESTICIDES/PCB'S DATA REPORT
•• PROJECT
NO. 94-0050 SAMPLE
NO. 80622 SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER »•
~~ SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL ••
•• STATION
• * '
ID: 34877L ALLIGATOR
LIVER
COLLECTION START: 10/21/93
STOP: 00/00/00 ••
• *
MG/KG
0.040U
0.040U
0.040U
0.040U
0.040U
0.040U
0.040U
0.040U
0.040U
0.040U
0.013
0.040U
0.040U
0.040U
0.040U
0. 10U
0. 10U
0. 10U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4 .4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0. 10U
O. 10U
0. 10U
0. 10U
0.81U
0.020U
0.020U
0.020U
0.020U
0.020U
0.014
0.020U
0.0038N
0.0054N
0.040U
0.040U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR
PCB-1248 (AROCLOR
PCB-1260 (AROCLOR
PCB-1016 (AROCLOR
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE
BETA CHLORDENE
GAMMA-CHLORDENE
GAMMA-CHLORDANE
TRANS-NONACHLOR
ALPHA-CHLORDANE
CIS-NONACHLOR
1232)
1248)
1260)
1016)
/2
/2
/2
/2
/2
/2
/2
OXYCHLORDANE (OCTACHLOREPOXIDE) /2
METHOXYCHLOR
ENDRIN KETONE
•••REMARKS***
***remarks«»»
•••FOOTNOTES***
•a-average value »na-not ANALYZED «NAI-INTERFERENCES »J-ESTIMATED value »n-presumptive evidence of presence of material
•k-actual value is known to be less than value given *l-actual value is known to BE greater than value given
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
_	^ _	EPA-REGION IV E .THENS. GA.
PESTICIDES/PCB'S DATA REPORT
*• PROJECT
NO. 94-0050 SAMPLE
NO. 80627 SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED
BY: B CARTER »*
•* SOURCE:
TOWER CHEMICAL
FAT
CITY: CLERMONT
ST: FL »•
** STATION
* •
ID: 34877F ALLIGATOR
COLLECTION START: 10/21/93
STOP: 00/00/00 **
* *
ANALYTICAL RESULTS
MG/KG
0.16U	ALDRIN
0.16U	HEPTACHLOR
0.16U	HEPTACHLOR EPOXIDE
0.16U	ALPHA-BHC
0.16U	BETA-BHC
0.16U	GAMMA-BHC (LINDANE)
0.16U	DELTA-BHC
0.15U	ENDOSULFAN I (ALPHA)
0.16U	DIELDRIN
0.16U	4.4'-DDT (P.P'-DDT)
1.6	4,4'-DDE (P.P'-DDE)
0.16U	4.4'-DDD (P.P'-DDD)
0.26U	ENDRIN
0.16U	ENDOSULFAN II (BETA)
0.16U	ENDOSULFAN SULFATE
—	CHLORDANE (TECH. MIXTURE)
1.6U	PCB-1242 (AROCLOR 1242)
1.6U	PCB-1254 (AROCLOR 1254)
1.6U	PCB-1221 (AROCLOR 1221)
/1
MG/KG
1 . 6U
1 . 6U
1 6U
1 .6U
13U
0.080U
0.080U
0.080U
0.080U
0 080U
0.51
0.080U
0.17
0.23N
0.32U
0. 16U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDAKIE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
**"REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-N0T ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AMD ANALYSI \GEMENT SYSTEM
EPA-REGION IV	ATHENS. GA.	0 94
»>EST1C!DES/PCB'S DATA REPORT
*~ PROJECT
NO. 94-0050 SAMPLE
NO. 80623 SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER •*
~* SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST. FL **
** STATION
• *
ID: 34878L ALLIGATOR
LIVER
COLLECTION START- 10/21/93
STOP: 00/00/00 **
* *
ANALYTICAL RF' I.TS
MG/KG
0.022U	ALDRIN
0.022U	HEPTACHLOR
0.022U	HEPTACHLOR EPOXIDE
0.022U	ALPHA-BHC
0.022U	BETA-BHC
0.022U	GAMMA-BHC (LINDANE)
0.022U	DELTA-BHC
0.022U	ENDOSULFAN I (ALPHA)
0.022U	DIELDRIN
O 022U	4.4'-DDT (P.P'-DDT)
0.19	4.4'-DDE (P.P'-DDE)
0.022U	4,4'-DDD (P.P'-DDD)
0.022U	ENDRIN
0.022U	ENDOSULFAN II (BETA)
0.022U	ENDOSULFAN SULFATE
—	CHLORDANE (TECH. MIXTURE)
0.11U	PCB-1242 (AROCLOR 1242)
0.11U	PCB-1254 (AROCLOR 1254)
0.11U	PCB-1221 (AROCLOR 1221)
/I
MG/KG
0.11U
0. 11U
0. 11U
0. 11U
0.90U
0.022U
0.022U
0.022U
0.022U
0.0043JN
0.0084J
0.0221)
O 022U
0.0030JN
0 045U
0.022U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMfl-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE) /2
METHOXYCHLOR
ENDRIN KETONE
•••REMARKS***
•••REMARKS***
••'FOOTNOTES**•
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN ^
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2 CONSTITUENTS CR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSIS 5EMENT SYSTEM
EPA-REGION IV Ei. .THENS, GA.	01,
PESTICIDES/PCB'S DATA REPORT
** PROJECT
NO. 94-0050 SAMPLE
NO. 80628 SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED
BY: B CARTER »•
** SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL ••
** STATION
• •
ID: 34878F ALLIGATOR
FAT
COLLECTION START: 10/21/93
STOP: 00/00/00 *»
* »
MG/KG
0.085U
0.085U
0.08511
0.085U
0.085U
0.085U
0.085U
0.085U
0.085U
2.2U
8.5
0.085U
0.085U
0.085U
2.2U
0.53U
0.53U
0.53U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4,4'-DDE (P.P'-DDE)
4,4'-DDD (P,P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
/1
MG/KG
0.53U
0.53U
0.53U
0.53U
4.2U
0.11U
0.11U
0.11U
0.11 u
0. 16
0.25
0. 11U
0. 11J
0. ION
0 21U
0.085U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
**(REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	C-CONFIRMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSI	VGEMENT SYSTEM
EPA-REGION IV I ATHENS. GA.	0. 94
PESTICIDES/PCB'S DATA REPORT
»» PROJECT
NO. 94-0050 SAMPLE
NO. 80624 SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER »•
»» SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL »»
»• STATION
• •
ID: 34879L ALLIGATOR
LIVER
COLLECTION START: 10/21/93
STOP: 00/00/00 » »
• *
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
0.018U	ALDRIN
0.018U	HEPTACHLOR
0.018U	HEPTACHLOR EPOXIDE
0.018U	ALPHA-BHC
0.018U	BETA-BHC
0.018U	GAMMA-BHC (LINDANE)
0.018U	DELTA-BHC
0.018U	ENDOSULFAN I (ALPHA)
0.018U	DIELDRIN
0.018U	4.4'-DDT (P.P'-DDT)
0.17	4.4'-DDE (P.P'-DDE)
0.018U	4.4'-DDD (P.P'-DDD)
0.018U	ENDRIN
0.018U	ENDOSULFAN II (BETA)
0.018U	ENDOSULFAN SULFATE
--	CHLORDANE (TECH. MIXTURE)
0.090U	PCB-1242 (AROCLOR 1242)
0.090U	PCB-1254 (AROCLOR 1254)
0.090U	PCB-1221 (AROCLOR 1221)
/I
0.090U
0.090U
0.090U
10.090U
J 0 72U
0.0090U
0.0090U
0.0090U
0.0090U
0 0090U
0.0038J
0 0090U
0.0090U
0.0090U
0 036U
0.018U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE) /2
METHOXYCHLOR
ENDRIN KETONE
«•"REMARKS*•»
« »'REMARKS* » *
••'FOOTNOTES*•*
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYSI VGEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	0 94
PESTiCIOES/PCB'S DATA REPORT
" PROJECT
NO. 94-0050 SAMPLE NO. 80629 SAMPLE TYPE: FAT
PROG ELEM: SSF COLLECTED
BY: B CARTER "
" SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL "
" STATION
**
ID: 349879F ALLIGATOR FAT
COLLECTION START: 10/21/93
STOP: 00/00/00 •»
* *
MG/KG
0. 11U
0. 11U
0. 11U
0.110
0 11U
0.11U
0. 11U
0. 11U
0. 11U
0.11U
0.11 u
0.11 u
0.11 u
0.11U
0.11U
0.56 U
0.56U
0.56U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-ODT)
4.4'-ODE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
/I
MG/KG
0 56U
0.56U
0.56U
0.56U
4 5U
0.056U
0.056U
0 056U
0.056U
0.20
0.23
0.056U
0.084
0.069N
0 1 1U
0.11U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•«'REMARKS'"
•»'REMARKS'»»
"•FOOTNOTES'"
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
SAMPLE AND ANALYST.
EPA-REGION IV t
PESTICIDES/PCB'S DATA REPORT		
«»««»«»»•*•»•**»»»»******»*******
PROJECT NO. 94-0050 SAMPLE NO. 80630 SAMPLE TYPE. FISH
SOURCE: TOWER CHEMICAL
STATION ID: TC104/105 GAMBUSIA
iGEMENT SYSTEM
ATHENS. GA.
PROG ELEM: SSF COLLECTED BY: B CARTER
COLLECTI0NMSTART: 10/20/93 ?130 STOP: 00/00/00
94
MG/KG
0.022U
0.022U
0.022U
0.022U
0 022U
0.022U
0.022U
0.022U
0.022U
0.022U
0.028
0.022V
0.022U
0.022U
0.022U
0.054U
0. 11U
0.11U
0. 11U
ANALYTICAL RESULTS
ALORIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0. 11U
0. 11U
0. 11U
0. 11U
0.86U
ANALYTICAL RESULTS
/1
0 043U
0.022U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
*•(REMARKS***
•••REMARKS***
TwiS'Ki SS«^Yai^rinwc^^DcoB.¥l!S5.,s "	«e?molites Of TECHNIC. CHLORDANE
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV L
IGEMENT SYSTEM
ATHENS. GA.

0
94
»* PROJECT NO. 94-0050 SAMPLE NO. 80631
*« SOURCE: TOWER CHEMICAL
*« STATION ID: TC108 GAMBUSIA
• *
SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED
CITY: CLERMONT
COLLECTION START: 10/21/93
BY: B CARTER
ST: FL
1315 STOP: 00/00/00

t *
* *
*	t
•	*
MG/KG
0.013U
0.013U
0.013U
0.0T3U
0.013U
0.013U
0.013U
0.013U
0.013U
0.013U
0.013U
0.013U
0.013U
0.013U
0013U
0.033U
0.065U
0.065U
0.065U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-D0T (P.P'-DOT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.065U
0.065U
0.065U
0.065U
0 52U
ANALYTICAL RESULTS
/I
0.026U
0.013U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE) /2
METHOXYCHLOR
ENDRIN KETONE
•••REMARKS***
•»"REMARKS***
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-C0NF1RMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
PESTICIDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV El
-.EMENT SYSTEM
CHENS. GA.
01,
PROJECT NO. 94-0050 SAMPLE NO. 80632
SOURCE: TOWER CHEMICAL
STATION ID. TCI11 GAM8USIA
SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED BY: 0 CARTER
CITY CLERMONT	ST: FL
COLLECTION START: 10/22/93 1730 STOP:
00/00/00
MG/KG
0.029U
0.029U
0.029U
0.029U
0.029U
0.029U
0.029U
0.029U
0.029U
O 029U
0.029U
0.029U
0.029U
0.029U
0.029U
0.074U
0. 14U
0. 14U
0.14U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0. 14U
0. 14U
0 14U
0. 14U
1 2U
ANALYTICAL RESULTS
/I
0 058U
0.029U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS'**
»*'REMARKS***
•A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
• U-MATERIAL WAS ANALY2ED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	„.Cr£2!^J.!?MED B GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AMD ANALYSIS
EPA-REGION IV E.
PESTlCIOES/PCB'S DATA REPORT
»««»~•••••»»••*•~*******•*** ...
PROJECT NO. 94-0050 SAMPLE NO. 80633 SAMPLE TYPE: FISH
SOURCE: TOWER CHEMICAL
STATION ID: TC121 MIXED FISH
3EMENT SYSTEM
.THENS. GA.
««*«•»»«»»»»«•»»»»•**»»**
PROG ELEM: SSF COLLECTED BY: B CARTER
COLLECTION^START: 10/23/93 ?000 STOP. 00/00/00
01
• * * *
MG/KG
0.015U
0.015U
0.015U
0.015U
0.015U
0.015U
0 015U
0.015U
0.015U
0.015U
0.015U
0.015U
0.015U
0.015U
0.015U
0.039U
0.077U
0.077U
0.077U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4,4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
/1
MG/KG	ANALYTICAL RESULTS
0.077U	PCB-1232 (AROCLOR 1232)
0.077U	PCB-1248 (AROCLOR 1248)
0.077U	PCB-1260 (AROCLOR 1260)
0.077U	PCB-1016 (AROCLOR 1016)
0.62U	TOXAPHENE
—	CHLORDENE /2
—	ALPHA-CHLORDENE /2
—	BETA CHLORDENE /2
—	GAMMA-CHLORDENE /2
—	GAMMA-CHLORDANE /2
—	TRANS-NONACHLOR /2
—	ALPHA-CHLORDANE /2
~	CIS-NONACHLOR /2
—	OXYCHLORDANE (OCTACHLOREPOXIDE)
0 031U	METHOXYCHLOR
0.015U	ENDRIN KETONE
/2
»•'REMARKS***
•••REMARKS***
»*"FOOTNOTES*** „	1MT	.uai TkiTFeFFRFMrF<; . I-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
Tm" G,u?-co»nR»ED »y
vALUE^S^EPORTEof^SE^CHLORDANE CONSTITUENTS T SSmuiStSm METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E.
PESTJClDES/PCB'S DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80634 SAMPLE TYPE: VEGETATION
SOURCE: TOWER CHEMICAL
STATION ID: TC101 SAURURUS
3EMENT SYSTEM
.THENS, GA.
01.
j4
»»»»•~»«»•»»»•~»»»•»~~*•«»*»*»
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START 10/21/93 1205 STOP: 00/00/00
MG/KG
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
0.0093U
00093U
0.023U
0.047U
0.047U
0.047U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDR1N
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.047U
0.047U
0 047U
0.047U
0. 370
ANALYTICAL RESULTS
/1
0.019U
0.0093U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS***
•••REMARKS***
***F9°Iw?lArruAi MF .MA MflT 4NAI V7FD »NAI-INTERFERENCES .J-EST1MATED VALUE .N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
:UaTERIALAWAS aSaL?2ED FORBBUTENOTTDETECTEDE ?HEENUMSESAISUTHEWMINIMiM oKlTAT^^LlSl" ™AN	C-CONFIRMED BY GC/MS
*1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
SAMPLE AND ANALYSIS
EPA-REGION IV Ei.
PEST1ClDES/PCB'S DATA REPORT	............
#•»»«•»•»•»«•«»»»«»»*»»**********
PROJECT NO. 94-0050 SAMPLE NO. 80635 SAMPLE TYPE: VEGETATION
SOURCE: TOWER CHEMICAL
STATION ID: TCI03 SAURURUS
iEMENT SYSTEM
fHENS. GA.
01.
»»»****«*««»*»«•»*»»*******
PROG ELEM: SSF COLLECTED BY: B CARTER
COLLECTIONMSTART: 10/22/93 ^215 STOP: 00/00/00
MG/KG
0.0I1U
0.011U
0.011U
0.0111)
0.011U
0.011U
0.011U
0.011U
0.0111)
0.011U
0.011U
0.011U
0.011U
0.011U
0.01iu
0.0291)
0.057U
0.057U
0.057U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.057U
0.057U
0.057U
0.057U
0 46U
ANALYTICAL RESULTS
/"i
0.023U
0.011U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE / 2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
*•.REMARKS*••
•~•REMARKS***
TwE!'& ;SUreV«l?OR?EDBUSE?0;H^l0CoKf,¥SSETS " '5'	MiTABOLliES of TECH«C«L CHLORDAKE
-------
SAMPLE AND ANALYST \GEMENT SYSTEM
EPA-REGION IV L ATHENS. GA.	0 94
PESTICIDES/PCB'S DATA REPORT
»» PROJECT
NO. 94-0050 SAMPLE NO. 80636 SAMPLE TYPE:
VEGETATION PROG ELEM: SSF COLLECTED
BY: B CARTER *»
*• SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL *«
•* STATION
• •
ID: TCI05 SAURURUS
COLLECTION START 10/19/93
1800 STOP: 00/00/00 »«
* *
MG/KG
0.011U
O.OIIU
0.011U
0.011U
O.OIIU
0.011U
0.011U
0.011U
O.OIIU
0.011U
0.011U
O.OIIU
O.OIIU
0.011U
0 011U
0.027U
0.0S4U
0.054U
0.054U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.054U
0.054U
0.054U
0.054U
0.43U
ANALYTICAL RESULTS
/I
0.022U
0.011U
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE) /2
METHOXYCHLOR
ENDRIN KETONE
•••REMARKS***
**'REMARKS***
•••FOOTNOTES***
~A-AVERAGE VALUE »NA-NOT ANALYZED *NA1-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
• K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN	„w „r
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2. CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE.
-------
PESTICIDES/PCB'5 DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV El
iEMENT SYSTEM
rHENS. GA.
01.
PROJECT NO. 94-0050 SAMPLE NO. 80637
SOURCE: TOWER CHEMICAL
STATION ID: TCI06 SAURURUS
SAMPLE TYPE: VEGETATION
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST" FL
COLLECTION START: 10/20/93 1510 STOP: 00/00/00
MG/KG
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.034U
0.068U
0.068U
0.068U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4.4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-ODD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.068U
0.0681/
0.068U
0.068U
0 55U
/I
0.027U
0.014U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCS-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.	C-CONFIRMED BY GC/MS
1. WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
PESTlClDES/PCB'S DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV EL
iEMENT SYSTEM
THENS, GA.
01,
PROJECT NO. 94-0050 SAMPLE NO. 80638
SOURCE: TOWER CHEMICAL
STATION ID: TCI08 SAURURUS
SAMPLE TYPE: VEGETATION
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1315 STOP:
00/00/00
MG/KG
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.014U
0.036U
0.072U
0.072U
0.072U
ANALYTICAL RESULTS
ALDRIN
HEPTACHLOR
HEPTACHLOR EPOXIDE
ALPHA-BHC
BETA-BHC
GAMMA-BHC (LINDANE)
DELTA-BHC
ENDOSULFAN I (ALPHA)
DIELDRIN
4,4'-DDT (P.P'-DDT)
4.4'-DDE (P.P'-DDE)
4.4'-DDD (P.P'-DDD)
ENDRIN
ENDOSULFAN II (BETA)
ENDOSULFAN SULFATE
CHLORDANE (TECH. MIXTURE)
PCB-1242 (AROCLOR 1242)
PCB-1254 (AROCLOR 1254)
PCB-1221 (AROCLOR 1221)
MG/KG
0.072U
0.072U
0.072U
0.072U
0.57U
/I
0 029U
0.014U
ANALYTICAL RESULTS
PCB-1232 (AROCLOR 1232)
PCB-1248 (AROCLOR 1248)
PCB-1260 (AROCLOR 1260)
PCB-1016 (AROCLOR 1016)
TOXAPHENE
CHLORDENE /2
ALPHA-CHLORDENE /2
BETA CHLORDENE /2
GAMMA-CHLORDENE /2
GAMMA-CHLORDANE /2
TRANS-NONACHLOR /2
ALPHA-CHLORDANE /2
CIS-NONACHLOR /2
OXYCHLORDANE (OCTACHLOREPOXIDE)
METHOXYCHLOR
ENDRIN KETONE
/2
•••REMARKS***
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	C-CONFIRMED BY GC/MS
1 WHEN NO VALUE IS REPORTED. SEE CHLORDANE CONSTITUENTS. 2 CONSTITUENTS OR METABOLITES OF TECHNICAL CHLORDANE
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
KEGiON IV
COLLEGE STATION KD.
ATHENS, OA. 1-06J3
MEMORANDUM******
DATE: 12/30/93
SUBJECT: Results of Specified Analysis;
9A-0050 TOWER CHEMICAL
CLERMONT FL
TO: DELBERT HICKS
*.tached are the results of analysis of f.amples collected as part of
je subject project.
If you have any questions please contact we.
FROM: Wade Knight
ATTACHMENT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REG ION IV ESu , ATHENS. GA.	12/.. .,93
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO 80620 SAMPLE TYPE: LIVER	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY. CLERMONT	ST. FL
STATION ID: 34853L ALLIGATOR LIVER	COLLECTION START- 10/21/93	STOP: 00/00/00
*¥*****************************************«********************
RESULTS UNITS PARAMETER
0.15U MG/KG DICHLOROBENZILATE
3.6U MG/KG DICOFOL (KELTHANE)
»**FOOTNOTES**»
«A-AVERAGE VALUE «NA-NOT ANALV2ED *NAI-INTERFERENrES «J-ESTIMATED VALUE *N-PRESUMPT IVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ESi , ATHENS. GA. 12,	93
SPECIFIED ANALYSIS DATA REPORT
*** »***#***********»********************»***********»*****»***~**	***
** PROJECT NO. 94-0050 SAMPLE NO. 80621 SAMPLE TYPE' LIVER PROG ELEM SSF COLLECTED BY: B CARTER	*«
** SOURCE. TOWER CHEMICAL CITY CLERMONT ST. FL	**
*» STATION ID 34876L ALLIGATOR LIVER COLLECTION START: 10/21/93 STOP: 00/00/00	**
»*	**
*** ~ »*********#**************************#****************~****#*	*t*
RESULTS UNITS PARAMETER
0.073U MG/KG DICHLOROBENZILATE
4.5U MG/KG DICOFOL (KELTHANE)
* * * FOOTNOTES* r*
*A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED	VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS	KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM	QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ES„. ATHENS. GA.	12 93
SPECIFIED ANALYSIS DATA REPORT
**»*****************************************#»******************
PROJECT NO 94-0050 SAMPLE NO 80622 SAMPLE TYPE LIVER	PROG ELEM SSF COLLECTED BY: B CARTER
SOURCE TOWER CHEMICAL	CITY CLERMONT	ST: FL
STATION ID 34877L ALLIGATOR LIVER	COLLECTION START: 10/21/93	STOP' 00/00/00
******************************~**************«»~*****#***~******
RESULTS UNITS PARAMETER
0 14U MG/KG DICHLOROBENZILATE
5.2U MG/KG DICOFOL (KELTHANE)
* "FOOTNOTES'**
*A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES * J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
«U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV ESl. . ATHENS, GA. 12	93
SPECIFIED ANALYSIS DATA REPORT
*** **************************************************************	***
»* PROJECT NO. 94-0050 SAMPLE NO. 80623 SAMPLE TYPE: LIVER PROG ELEM: SSF COLLECTED BY: B CARTER	«»
»» SOURCE. TOWER CHEMICAL CITY. CLERMONT ST: FL	»»
»» STATION ID- 34878L ALLIGATOR LIVER COLLECTION START: 10/21/93 STOP• 00/00/00	*»
* *	* *
*** ***<**********************************************************	***
RESULTS UNITS PARAMETER
0.095U MG/KG DICHLOROBENZILATE
5 8U MG/KG DICOFOL (KELTHANE)
* » * FOOTNOTES* * *
«A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV ESi., ATHENS. GA.	12, ,93
SPECIFIED ANALYSIS DATA REPORT
»* PROJECT NO. 94-0050 SAMPLE NO. 80624 SAMPLE TYPE' LIVER PROG ELEM: SSF COLLECTED BY: B CARTER	«*
** SOURCE: TOWER CHEMICAL CITY. CLERMONT ST: FL	**
** STATION ID: 34879L ALLIGATOR LIVER COLLECTION START: 10/21/93 STOP: 00/00/00	»*
*'	>s
RESULTS UNITS PARAMETER
0.076U MG/KG DICHL0R0BEN21 LATE
4 7U MG/KG DICOFOL (KELTHANE)
* * «FOOTNOTES* * *
~ A-/WERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ESb. ^THENS. GA.	12/
SPECIFIED ANALYSIS DATA REPORT
*************************************************************
PROJECT NO. 94-0050 SAMPLE NO. 80625 SAMPLE TYPE: FAT	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: FL
STATION ID: 34853F ALLIGATOR FAT	COLLECTION START: 10/21/93	STOP: 00/00/00
**»********»***»»****»*»**»»*******»»****»***»*»»»»*»»*»**»»*
RESULTS UNITS PARAMETER
0.23U MG/KG DICHLOROBENZILATE
14U MG/KG DICOFOL (KELTHANE)
'"FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATER1AL WAS ANALY2ED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS oEMENT SYSTEM
EPA-REGION IV ESu. ATHENS, GA.	12,
SPECIFIED ANALYSIS DATA REPORT
*»* *******»****»*»»***»»*»»»»**»**»**»******»****»»**»»**»*****»»
** PROJECT NO. 94-0050 SAMPLE NO. 80626 SAMPLE TYPE- FAT	PROG ELEM: SSF COLLECTED BY: B CARTER
** SOURCE: TOWER CHEMICAL	CITY. CLERMONT	ST. FL
** STATION ID 34876F ALLIGATOR FAT	COLLECTION START: 10/21/93	STOP: 00/00/00
* *
*********************************** ******^*******»***»**»*********
RESULTS UNITS PARAMETER
0.67U MG/KG DICHLOROBENZILATE
32U MG/KG DICOFOL (KELTHANE)
* *'FOOTNOTES* * *
*A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-EST1MATED	VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERI
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS	KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM	QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS uEMENT SYSTEM
EPA-REGION IV ESi.. ATHENS. GA.	12/
SPECIFIED ANALYSIS DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80627 SAMPLE TYPE. FAT	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE. TOWER CHEMICAL	CITY. CLERMONT	ST. FL
STATION ID" 34877F ALLIGATOR FAT	COLLECTION START: 10/21/93	STOP: 00/00/00
****************************************************************
RESULTS UNITS	PARAMETER
1.2J MG/KG	DICHLOROBENZILATE
41U MG/KG	DICOFOL (KELTHANE)
* * * FOOTNOTES* * *
*A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ESu, ATHENS, GA.	12/
SPECIFIED ANALYSIS DATA REPORT
**« »»**»**»******»»**»******»**«**»:***»**»*****»»*«»»»********»»*
** PROJECT NO 94-0050 SAMPLE NO. 80628 SAMPLE TYPE: FAT	PROG ELEM' SSF COLLECTED BY' B CARTER
** SOURCE: TOWER CHEMICAL	CITY. CLERMONT	ST: FL
»» STATION ID: 34878F ALLIGATOR FAT	COLLECTION START: 10/21/93	STOP' 00/00/00
* *
RESULTS UNITS PARAMETER
0.45U MG/KG DICHLOROBENZILATE
27U MG/KG DICOFOL (KELTHANE)
*«'FOOTNOTES*»*
»A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERI
»K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV ES„. ATHENS. GA.	12, 93
SPECIFIED ANALYSIS DATA REPORT
** PROJECT NO. 94-0050 SAMPLE NO 80629 SAMPLE TYPE" FAT PROG ELEM: SSF	COLLECTED BY: B CARTER *»
** SOURCE. TOWER CHEMICAL CITY: CLERMONT	ST: FL **
»* STATION ID- 349879F ALLIGATOR FAT COLLECTION START: 10/21/93	STOP: 00/00/00 »»
* *	* *
********************************* * * * * * * * * * * *	* * * * t * * * * * * * * * * * * * * * * * * *
RESULTS UNITS PARAMETER
0.38U MG/KG DICHLOROBENZI LATE
15U MG/KG DICOFOL (KELTHANE)
"'FOOTNOTES**'
*A-AVERAGE value *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
*K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS .GEMENT SYSTEM
EPA-REGION IV ES. ATHENS. GA.	12, 93
SPECIFIED ANALYSIS DATA REPORT
***	***
»* PROJECT NO. 94-0050 SAMPLE NO 80630 SAMPLE TYPE- FISH PROG ELEM: SSF COLLECTED BY: B CARTER	«*
*» SOURCE. TOWER CHEMICAL CITY: CLERMONT ST. FL	»»
** STATION ID- TCI04/105 GAMBUSIA COLLECTION START: 10/20/93 1130 STOP:	00/00/00 **
* *	* *
*** ***********»»*************************************~*»#*~****** ***
RESULTS UNITS PARAMETER
0.091U MG/KG DICHL0R0BEN2ILATE
5.6U MG/KG DICOFOL (KELTHANE)
»**FOOTNOTES»*»
*A-AVERAGE VALUE «NA-KJOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AMD ANALVSIS .GEMENT SYSTEM
EPA-REGION IV ES„. ATHENS. GA.	12 93
SPECIFIED ANALYSIS DATA REPORT
*** ********»»*******»»*»*********»***»**»»»*»»«*»»»****»»****»»»* *»»
»* PROJECT NO 94-0050 SAMPLE NO. 80631 SAMPLE TYPE: FISH PROG ELEM: SSF COLLECTED BY: B CARTER	**
*» SOURCE: TOWER CHEMICAL CITY. CLERMONT ST FL	»«
** STATION ID: TC108 GAMBUSIA COLLECTION START: 10/21/93 1315 STOP'	00/00/00 **
* *	* *
RESULTS UNITS PARAMETER
0 055U MG/KG DICHLOROBENZILATE
3.4U MG/KG DICOFOL (KELTHANE)
**'FOOTNOTES***
*A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS oEMENT SYSTEM
EPA-REGION IV ES.u . ATHENS, GA.	12/. J3
SPECIFIED ANALYSIS DATA REPORT
****************************************************************
PROJECT NO. 94-0050 SAMPLE NO. 80632 SAMPLE TYPE: FISH	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST. FL
STATION ID- TC111 GAMBUSIA	COLLECTION START: 10/22/93 1730 STOP: 00/00/00
RESULTS UNITS PARAMETER
0 12U MG/KG DICHLOROBENZILATE
7.6U MG/KG DICOFOL (KELTHANE)
'••FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ESi. . ATHENS, GA.
12, 33
SPECIFIED ANALYSIS DATA REPORT
***	«**»*»********»*»*****»***»*******»*»***»»»*»**»»»*»****»»»**»»
**	PROJECT NO. 94-0050 SAMPLE NO. 80633 SAMPLE TYPE: FISH	PROG ELEM SSF COLLECTED BY" B CARTER
'*	SOURCE. TOWER CHEMICAL	CITY. CLERMONT	ST: FL
*»	STATION ID- TC121 MIXED FISH	COLLECTION START: 10/23/93 1000 STOP: 00/00/00
* *
***	*»*~***~******»*~**#***#*****»*~#»##~****~**~**#~*#~***~*~*~*~*
RESULTS UNITS PARAMETER
0.066U MG/KG DICHLOROBENZILATE
4.0U MG/KG DICOFOL (KELTHANE)
* *»FOOTNOTES' * *
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN » L-ACTUAL VALUE IS	KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS uEMENT SYSTEM
EPA-REGION IV ESu. ATHENS. GA	12, 33
SPECIFIED ANALYSIS DATA REPORT
N0- 94-0050 SAMPLE NO. 80634 SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY- B CARTER
SOURCE. TOWER CHEMICAL	CITY: CLERMONT	ST- FL
STATION ID TC101 SAURURUS	COLLECTION START: 10/21/93 1205 STOP: 00/00/00
********************~********~~#**»***«*~~**~*~****
RESULTS UNITS PARAMETER
0.040U MG/KG DICHLOROBENZILATE
2.4U MG/KG DICOFOL (KELTHANE)
************
* * *FOOTNOTES* » »
*A-AVERAGE value *NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN * L~ACTUAL VALUE IS	KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBEP IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV Eb-. ATHENS, GA.	12/ ,93
SPECIFIED ANALYSIS DATA REPORT
»»»	***
«* PROJECT NO. 94-0050 SAMPLE NO, 80635 SAMPLE TYPE' VEGETATION PROG ELEM SSF COLLECTED	BY: B CARTER »*
»* SOURCE: TOWER CHEMICAL CITY. CLERMONT	ST FL **
»* STATION ID' TC103 SAURURUS COLLECTION START' 10/22/93	1215 STOP: 00/00/00 **
**	»»
**» ******»*»*******»»»**»»**«»*»*»*»»»***«»*****»**»******»»»»**» *»»
RESULTS UNITS PARAMETER
0.049U MG/KG DICHLOROBENZILATE
3.0U MG/KG DICOFOL (K.ELTHANE)
* * » FOOTNOTES* * *
*A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENC.ES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV Eb. . ATHENS. GA.	12 93
SPECIFIED ANALYSIS DATA REPORT
*** ft************************************************************* ***
** PROJECT NO. 94-0050 SAMPLE NO. 80636 SAMPLE TYPE: VEGETATION PROG ELEM- SSF COLLECTED BY: B CARTER	««
** SOURCE. TOWER CHEMICAL	CITY: CLERMONT	ST. FL	»*
»» STATION ID: TC105 SAURURUS	COLLECTION START' 10/19/93 1800 STOP: 00/00/00	*»
»» »
********************************************************************
RESULTS UNITS PARAMETER
0 046U MG/KG DICHLOROBENZILATE
2.8U MG/KG DICOFOL (KELTHANE)
* * »FOOTNOTES* * *
*A-AVERAGE VALUE *NA-N0T ANALYZED *NAI-INTERFERENCES *J-ESTIMATED	VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS	KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS CEMENT SYSTEM
EPA-REGION IV . ATHENS. GA. 12	93
SPECIFIED ANALYSIS DATA REPORT
*** *******»**#*«**»****»»******»***¦***************»**»***********	***
«» PROJECT NO. 94-0050 SAMPLE NO. 80637 SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER	**
«* SOURCE. TOWER CHEMICAL CITY. CLERMONT ST. FL	*»
*» STATION ID: TC106 SAURURUS COLLECTION START: 10/20/93 1510 STOP' 00/00/00	**
«*	**
»*t *~**»*******#***********#*#********<*****#*************»******	***
RESULTS UNITS PARAMETER
0 .058U MG/KG DICHLOROBENZI LATE
3 5U MG/KG DICOFOL (KELTHANE)
**»FOOTNOTES**t
*A-AVERAGE value *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
• K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
»U-MATER1AL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
SAMPLE AND ANALYSIS jEMENT SYSTEM
EPA-REGION IV ESl. aTHENS. GA.	12 J3
SPECIFIED ANALYSIS DATA REPORT
*** ************************************************************** ***
** PROJECT NO. 94-0050 SAMPLE NO. 80636 SAMPLE TYPE- VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER	*«
** SOURCE: TOWER CHEMICAL CITY CLERMONT ST: FL	**
»* STATION ID- TCI08 SAURURUS COLLECTION START: 10/21/93 1315 STOP: 00/00/00	»*
* *	» *
RESULTS UNITS PARAMETER
0 061U MG/KG DICHLOROBENZILATE
3.7U MG/KG DICOFOL (KELTHANE)
***FOOTNOTES*»*
'A-flVERAGE VALUE »NA—NOT ANALYZED *NAI-INTERFERENCES »J-ESTIWATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT
-------
EXTRACTABLE 0RGAN1CS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
.THENS, GA.
PROJECT NO. 94-0050 SAMPLE NO. 80620 SAMPLE TYPE. LIVER
SOURCE: TOWER CHEMICAL
STATION ID: 34853L ALLIGATOR LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG	ANALYTICAL RESULTS
2.8U	(3-AND/OR 4-)METHYLPHEN0L
2.8U	1.2.4-TRICHLOROBENZENE
2.8U	2.2'-CHL0R0IS0PR0PYLETHER
2.8U	2.3.4.6-TETRACHL0R0PHEN0L
2.8U	2.4.5-TRICHL0R0PHEN0L
2.8U	2.4.6-TRICHLOROPHENOL
2.8U	2.4-DICHLOROPHENOL
2.8U	2.4-DIMETHYLPHENOL
5.6U	2.4-DINIT ROPHE NOL
2.8U	2.4-DINITR0T0LUENE
2.8U	2.6-DINITR0T0LUENE
2.8U	2-CHLORONAPHTHALENE
2.8U	2-CHLOROPHENOL
5.6U	2-METHYL-4.6-DINITR0PHEN0L
2.8U	2-METHYLNAPHTHALENE
2.8U	2-METHYLPHENOL
2.8U	2-NITROANILINE
2.8U	2-NITROPHENOL
2.8U	3.3'-DICHL0R0BENZIDINE
2.8U	3-NITROANILINE
2.8U	4-BROMOPHENYL PHENYL ETHER
2.8U	4-CHLORO-3-METHYLPHENOL
2.8U	4-CHLOROANILINE
2.8U	4-CHLOROPHENYL PHENYL ETHER
2.8U	4-N1TR0AN1LINE
5.6U	4-NITROPHENOL
2.8U	ACENAPHTHENE
2.8U	ACENAPHTHYLENE
2.8U	ANTHRACENE
2.8U	BENZO(A)ANTHRACENE
2.8U	BENZOIB AND/OR KJFLUORANTHENE
MG/KG
2.8U
2.8U
2.8U
2.8U
2.8U
2.8U
2.8U
2.8U
2.8U
2. 8U
2.8U
2 8U
2 8U
2.8U
2 8U
2.8U
2
2
2
2
2
2.8U
2.8U
2 8U
2 8U
2.8U
5.6U
2.8U
2.8U
2.8U
8U
8U
8U
8U
8U
ANALYTICAL RESULTS
BENZOfGHIJPERYLENE
BENZO-A-PYRENE
BENZYL BUTYL PHTHALATE
BIS(2-CHLOROETHOXY) METHANE
B15(2-CHLOROETHYL) ETHER
BIS(2-ETHYLHEXYL) PHTHALATE
CARBAZOLE
CHRYSENE
DI-N-BUTYLPHTHALATE
DI-N-OCTYLPHTHALATE
DIBENZO(A.H)ANTHRACENE
DIBENZOFURAN
DIETHYL PHTHALATE
DIMETHYL PHTHALATE
FLUORANTHENE
FLUORENE
HEXACHLOROBENZENE (HCB)
HEXACHLOROBUTADIENE
HEXACHLOROCYCLOPENTADIENE (HCCP)
HEXACHLOROETHANE
INDENO (1.2.3-CD) PYRENE
ISOPHORONE
N-NITROSODI-N-PROPYLAMINE
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
NAPHTHALENE
NITROBENZENE
PENTACHLOROPHENOL
PHENANTHRENE
PHENOL
PYRENE
••'REMARKS*»•
«»'REMARKS*«»
•••FOOTNOTES**•
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS	iMENT SYSTEM
EPA-REGION IV ESL HENS, GA.
12/
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
*** *»*»#»•»*»»«»•»»»»•»»»•»*«»»*~*
•« PROJECT NO. 94-0050 SAMPLE NO. 80620 SAMPLE TYPE: LIVER
»» SOURCE: TOWER CHEMICAL
STATION ID: 34853L ALLIGATOR LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
5JN	TETRADECANOIC ACID
7JN	PENTADECANOIC ACID (2 ISOMERS)
10JN	HEXADECENOIC ACID
60JN	HEXADECANOIC ACID
20JN	HEPTADECANOIC ACID (2 ISOMERS)
40JN	OCTADECANOIC ACID
100J	7 UNIDENTIFIED COMPOUNDS
wai lie *MA—MOT ANALYZED *NAI—INTERFERENCES *J—ESTIMATED VALUE *N— PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
^-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	NECESSARY FOR VERIFICATION
«R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VtKIl-ILAIiun.
-------
SAMPLE AND ANALYSIS
EXTRACTABLE ORGANICS DATA REPORT
3EMENT SYSTEM
.Ti-icrio, GA.
12.
PROJECT NO. 94-0050 SAMPLE NO. 80621
SOURCE: TOWER CHEMICAL
STATION ID: 34876L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP:
00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
3.5U
(3-AND/OR 4-)METHYLPHENOL
3.5U
BENZO(GHI)PERYLENE
3.5U
1.2.4-TRICHLOROBENZENE
3.5U
BENZO-A-PYRENE
3.5U
2.2'-CHLOROISOPROPYLETHER
3 5U
BENZYL BUTYL PHTHALATE
3.5U
2.3.4.6-TETRACHL0R0PHEN0L
3.5U
BIS(2-CHLOROETHOXY) METHANE
3.5U
2.4.5-TRICHL0R0PHEN0L
3.5U
B1S(2-CHLOROETHYL) ETHER
3.5U
2.4.6-TRICHLOROPHENOL
3.5U
BIS(2-ETHYLHEXYL) PHTHALATE
3.5U
2.4-DICHLOROPHENOL
3.5U
CARBAZOLE
3.5U
2.4-DIMETHYLPHENOL
3.5U
CHRYSENE
7.0U
2.4-DINITR0PHEN0L
3.5U
DI-N-BUTYLPHTHALATE
3.5U
2.4-DINITROTOLUENE
3 5U
DI-N-OCTYLPHTHALATE
3.5U
2,6-DINITROTOLUENE
3.5U
DIBENZO(A.H)ANTHRACENE
3.5U
2-CHLORONAPHTHALENE
3.5U
DIBENZOFURAN
3.5U
2-CHLOROPHENOL
3.5U
DIETHYL PHTHALATE
7.0U
2-ME THYL-4.6-DINITROPHENOL
3.5U
DIMETHYL PHTHALATE
3.5U
2-METHYLNAPHTHALENE
3 5U
FLUORANTHENE
3.5U
2-METHYLPHENOL
3.5U
FLUORENE
3.5U
2-NITR0AN1LINE
3.5U
HEXACHLOROBENZENE (HCB)
3.5U
2-NITROPHENOL
3.5U
HE XACHLOROBUT ADIENE
3.5U
3.3'-DICHL0R0BENZIDINE
3.5U
HEXACHLOROCYCLOPENTADIENE (HCCP)
3.5U
3-NITROANILINE
3 5U
HEXflCHLOROETHANE
3.5U
4-BROMOPHENYL PHENYL ETHER
3.5U
INDENO (1.2.3-CD) PYRENE
3.5U
4-CHLORO-3-METHYLPHENOL
3 5U
ISOPHORONE
3.5U
4-CHL0R0ANILINE
3.5U
N-NITROSODI-N-PROPYLAMINE
3.5U
4-CHL0R0PHENYL PHENYL ETHER
3.5U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
3.5U
4-NIT ROANIL1NE
3.5U
NAPHTHALENE
7.0U
4-NITROPHENOL
3.5U
NITROBENZENE
3.5U
ACENAPHTHENE
7 OU
PENTACHLOROPHENOL
3 5U
ACENAPHTHYLENE
3 5U
PHENANTHRENE
3.5U
ANTHRACENE
3.5U
PHENOL
3 5U
BENZO(A)ANTHRACENE
3 5U
PYRENE
3.5U
BENZO(B AND/OR K)FLUORANTHENE


•»'REMARKS**»
»*'REMARKS***
•••FOOTNOTES*•»
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
~K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
MISCEUMIEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
*• source! T0WER4CHEMICALSAMPLE N0- 8062' SAMPLE TYPE* LIVER *
STATION ID: 34876L ALLIGATOR LIVER
CITV:ECl"|*»o5t' 'c°l«CTO*BY: VcInreJ
COLLECTION START: 10/21/93 ' STOP: 00/00/00
ANALYTICAL RESULTS MG/K.G
9JN TETRAOECANOIC ACID
4JN	PENTADECANOIC ACID
30JN	HEXADECENOIC ACID
100JN	HEXADECANOIC ACID
10JN	HEPTADECAN01C ACID (2 ISOMERS)
70JN	OCTADECANOIC ACID
200J	9 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN «L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. «THENS. GA.	12,
EXTRACTABLE ORGANICS DATA REPORT
•• PROJECT
NO. 94-0050 SAMPLE
NO. 80622 SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED
BY: B CARTER **
•• SOURCE:
TOWER CHEMICAL

CITY: CLERMONT
ST: FL **
•• STATION
• •
ID: 34877L ALLIGATOR
LIVER
COLLECTION START: 10/21/93
STOP: 00/00/00 **
* *
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
4.0U
(3-AND/OR 4-JMETHYLPHENOL
4.0U
BENZO(GHI)PERYLENE
4.0U
1.2,4-TRICHLOROBENZENE
4.0U
BENZO-A-PYRENE
4.0U
2.2'-CHLOROISOPROPYLETHER
4.0U
BENZYL BUTYL PHTHALATE
4.0U
2.3.4.6-TETRACHLOROPHENOL
4.0U
BIS(2-CHLOROETHOXY) METHANE
4.0U
2.4.5-T RICHLOROPHE NOL
4.0U
BIS(2-CHLOROETHYL) ETHER
4.0U
2,4.6-TRICHLOROPHENOL
4.0U
BIS(2-ETHYLHEXYL) PHTHALATE
4.0U
2.4-DICHLOROPHENOL
4.0U
CARBAZOLE
4.0U
2,4-DIMETHYLPHENOL
4.0U
CHRYSENE
8.1U
2,4-DINITROPHENOL
4.0U
DI-N-BUTYLPHTHALATE
4.0U
2.4-DINITR0T0LUENE
4.0U
DI-N-OCTYLPHTHALATE
4.0U
2.6-DINITROTOLUENE
4.0U
DIBENZO(A.H)ANTHRACENE
4.0U
2-CHLORONAPHTHALENE
4.0U
DIBENZOFURAN
4.0U
2-CHLOROPHENOL
4 OU
DIETHYL PHTHALATE
8.1U
2-ME THYL-4.6-DINITROPHENOL
4.0U
DIMETHYL PHTHALATE
4.0U
2-METHYLNAPHTHALENE
4.0U
FLUORANTHENE
4.0U
2-ME THYLPHENOL
4.0U
FLUORENE
4.0U
2-NITROANILINE
4.0U
HEXACHLOROBENZENE (HCB)
4.0U
2-NITROPHENOL
4.0U
HEXACHLOROBUTADIENE
4.0U
3.3'-DICHLOROBENZIDINE
4.0U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4 OU
3-NITROANILINE
4 OU
HEXACHLOROETHANE
4.0U
4-BROMOPHENYL PHENYL ETHER
4.0U
INDENO (1.2,3-CD) PYRENE
4.0U
4-CHLORO-3-METHYLPHENOL
4.0U
ISOPHORONE
4.0U
4-CHLOROANILINE
4 OU
N-NITROSODI-N-PROPYLAMINE
4.0U
4-CHLOROPHENYL PHENYL ETHER
4 OU
N-NITROSODI PHENYLAMINE/DI PHENYLAMINE
4.0U
4-NITROANILINE
4 OU
NAPHTHALENE
8.1U
4-NITROPHENOL
4.0U
NITROBENZENE
4.0U
ACENAPHTHENE
8. 1U
PENTACHLOROPHENOL
4.0U
ACENAPHTHYLENE
4 OU
PHENANTHRENE
4.0 U
ANTHRACENE
4.0U
PHENOL
4.0U
BENZO(A)ANTHRACENE
4.0U
PYRENE
4.0U
BENZO(B AND/OR K)FLUORANTHENE


•••REMARKS***	**'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E. .THENS. GA.
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80622 SAMPLE TYPE: LIVER
SOURCE: TOWER CHEMICAL
STATION ID: 34877L ALLIGATOR LIVER
PROG ELEM: SSF COLLECTED BY: 0 CARTER
COLLECT IO^StIrT- 10/21/93	STOP" 00/00/00
ANALYTICAL RESULTS MG/KG
10JN	HEXADECENOIC ACID
60JN	HEXADECANOIC ACID
7JN	HEPTADECANOIC ACID
50JN	OCTADECANOIC ACID
100J	5 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE URGANICS DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES HENS. GA.
12/
PROJECT NO. 94-0050 SAMPLE NO. 80623 SAMPLE TYPE: LIVER
SOURCE: TOWER CHEMICAL
STATION ID. 34878L ALLIGATOR LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
4.5U
(3-AND/OR 4-)METHYLPHENOL
4.5U
BENZO(GHI)PERYLENE
4. 5U
1.2.4-TRICHLOROBENZENE
4.5U
BENZO-A-PYRENE
4.5U
2.2'-CHLOROISOPROPYLETHER
4.5U
BENZYL BUTYL PHTHALATE
4.5U
2.3.4.6-TETRACHL0R0PHEN0L
4 5U
BIS(2-CHLOROETHOXY) METHANE
4.5U
2.4.5-TRICHL0R0PHEN0L
4.5U
BIS(2-CHLOROETHYL) ETHER
4.5U
2.4,6-TRICHLOROPHENOL
4.5U
BIS(2-ETHYLHEXYL) PHTHALATE
4.5U
2,4-DICHLOROPHE NOL
4.5U
CARBAZOLE
4.5U
2.4-DIMETHYLPHENOL
4.5U
CHRYSENE
9.0U
2.4-DINIT ROPHENOL
4. 5U
DI-N-BUTYLPHTHALATE
4.5U
2.4-DINITR0T0LUENE
4.5U
DI-N-OCTYLPHTHALATE
4.5U
2.6-DINITR0T0LUENE
4.5U
DIBENZO(A.H)ANTHRACENE
4.5U
2-CHLORONAPHTHALENE
4.5U
DIBENZOFURAN
4.5U
2-CHLOROPHENOL
4 5U
DIETHYL PHTHALATE
9.0U
2-METHYL-4.6-DINITROPHENOL
4.5U
DIMETHYL PHTHALATE
4.5U
2-METHYLNAPHTHALENE
4.5U
FLUORANTHENE
4.5U
2-METHYLPHENOL
4.5U
FLUORENE
4.5U
2-NITROANILINE
4.5U
HEXACHLOROBENZENE (HCB)
4.5U
2-NITROPHE NOL
4 5U
HEXACHLOROBUTADIENE
4.5U
3,3'-DICHL0R0BENZIDINE
4.5U
HEXACHLOROCYCLOPENTADIENE (HCCP)
4 SU
3-NITROANIL1NE
4 5U
HEXAGHLOROETHANE
4.5U
4-BR0M0PHENYL PHENYL ETHER
4.5U
INDENO (1.2,3-CD) PYRENE
4.5U
4-CHL0R0-3-ME THYLPHENOL
4.5U
ISOPHORONE
4.5U
4-CHL0R0ANILINE
4.5U
N-NITROSODI-N-PROPYLAMINE
4.5U
4-CHLOROPHENYL PHENYL ETHER
4 5U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
4.5U
4-NITROANILINE
4.5U
NAPHTHALENE
9.0U
4-NITR0PHEN0L
4.5U
NITROBENZENE
4.5U
ACENAPHTHENE
9.0U
PENTACHLOROPHENOL
4.5U
ACENAPHTHYLENE
4 5U
PHENANTHRENE
4.5U
ANTHRACENE
4 . 5U
PHENOL
4.5U
BENZO(A)ANTHRACENE
4 5U
PYRENE
4.5U
BENZO(B AND/OR K)FLUORANTHENE


•••REMARKS'**
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS JEMENT SYSTEM
EPA-REGION IV ES. rHENS, GA.
12
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
*•• *»»~»*»*»»*»*»»»»**»*»«•**»*»**
»• PROJECT NO. 94-0050 SAMPLE NO. 80623 SAMPLE TYPE: LIVER
«• SOURCE. TOWER CHEMICAL
•• STATION ID: 34878L ALLIGATOR LIVER
*******•***»***«»**•••••*(****•*
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
7JN	HEXADECENOIC ACID
30JN	HEXADECANOIC ACID
20JN	OCTADECANOIC ACID
90J	3 UNIDENTIFIED COMPOUND
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE uRGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV EL
\EMENT SYSTEM
.HEKIS, GA.
12,
PROJECT NO. 94-0050 SAMPLE NO. 80624
SOURCE: TOWER CHEMICAL
STATION ID. 34879L ALLIGATOR LIVER
SAMPLE TYPE: LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
MG/KG	ANALYTICAL RESULTS
3.6U	(3-AND/0R 4-JMETHYLPHENOL
3.6U	1,2,4-TRICHLOROBENZENE
3.6U	2.2'-CHLOROISOPROPYLETHER
3.6U	2,3,4.6-TETRACHL0R0PHEN0L
3.6U	2,4,5-T RICHLOROPHE NOL
3.6U	2.4,6-TRICHL0R0PHEN0L
3.6U	2.4-DICHL0R0PHEN0L
3.6U	2,4-DIMETHYLPHENOL
7.2U	2.4-DINITR0PHEN0L
3.6U	2.4-DINITROTOLUENE
3.6U	2.6-DINITR0T0LUENE
3.6U	2-CHLORONAPHTHALENE
3. 6U	2-CHLOROPHENOL
7.2U	2-METHYL-4,6-DINITR0PHEN0L
3.6U	2-METHYLNAPHTHALENE
3.6U	2-METHYLPHENOL
3.6U	2-N1TR0AN1LINE
3.6U	2-NITR0PHEN0L
3.6U	3.3'-DICHL0R0BENZIDINE
3 6U	3-NITR0ANIL1NE
3.6U	4-BR0M0PHENYL PHENYL ETHER
3.6U	4-CHL0R0-3-METHYLPHEN0L
3.6U	4-CHL0R0ANILINE
3.6U	4-CHL0R0PHENYL PHENYL ETHER
3.6U	4-NITROANILINE
7.2U	4-NITR0PHEN0L
3.6U	ACENAPHTHENE
3.6U	ACENAPHTHYLENE
3.6U	ANTHRACENE
3.6U	BEN20(A)ANTHRACENE
3.6U	BENZOtB AND/OR K)FLUORANTHENE
MG/KG	ANALYTICAL RESULTS
3.6U	BENZ0(GHI)PERYLENE
3.6U	BENZO-A-PYRENE
3.6U	BENZYL BUTYL PHTHALATE
3.6U	BIS(2-CHLOROETHOXY) METHANE
3 6U	BIS (2-CHLOROETHYL) ETHER
3 6U	BIS(2-ETHYLHEXYL) PHTHALATE
3 6U	CARBAZOLE
3.6U	CHRYSENE
3.6U	DI-N-BUTYLPHTHALATE
3.6U	DI-N-OCTYLPHTHALATE
3.6U	DIBENZ0(A.H)ANTHRACENE
3.6U	DIBENZOFURAN
3.6U	DIETHYL PHTHALATE
3.6U	DIMETHYL PHTHALATE
3 6U	FLUORANTHENE
3.6U	FLUORENE
3.6U	HEXACHLOROBENZENE (HCB)
3.6U	HEXACHLOROBUTADIENE
3.6U	HEXACHLOROCYCLOPENTADIENE (HCCP)
3 6U	HEXACHLOROETHANE
3.6U	INDENO (1,2.3-CD) PYRENE
3.6U	ISOPHORONE
3.6U	N-NITROSODI-N-PROPYLAMINE
3 6U	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
3.6U	NAPHTHALENE
3.6U	NITROBENZENE
7.2U	PENTACHLOROPHENOL
3.6U	PHENANTHRENE
3.6U	PHENOL
3 6U	PYRENE
• «'REMARKS* ••
••'REMARKS*»•
••~FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE »N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS jEMENT SYSTEM
EPA-REGION IV ES «THENS. GA.	12,
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80624 SAMPLE TYPE: LIVER
SOURCE: TOWER CHEMICAL
STATION ID- 34879L ALLIGATOR LIVER
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93	STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
4JN	TETRADECANOIC ACID
20JN	HEXADECENOIC ACID
60JN	HEXADECANOIC ACID
8JN	HEPTADECANOIC ACID
30JN	OCTADECANOIC ACID
100J	6 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI AGEMENT SYSTEM
EPA-REGION IV t- . ATHENS. GA.
/93
PROJECT NO. 94-0050 SAMPLE NO. 80630
SOURCE: TOWER CHEMICAL
STATION ID: TC104/105 GAMBUSIA
SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1130 STOP: 00/00/00
MG/KG	ANALYTICAL RESULTS
4.3U	(3-AND/OR 4-)METHYLPHEN0L
4.3U	1.2.4-TRICHLOROBENZENE
4.3U	2.2'-CHL0R0IS0PR0PYLETHER
4.3U	2,3.4.6-TETRACHL0R0PHEN0L
4.3U	2.4.5-TRICHL0R0PHEN0L
4.3U	2.4.6-TRICHLOROPHENOL
4.3U	2.4-DICHL0R0PHEN0L
4.3U	2.4-DIMETHYLPHEN0L
8.6U	2.4-DINITROPHENOL
4.3U	2.4-DINITROTOLUENE
4.3U	2.6-DINITROTOLUENE
4.3U	2-CHLORONAPHTHALENE
4.3U	2-CHLOROPHENOL
8.6U	2-METHYL-4,6-DINITROPHENOL
4.3U	2-METHYLNAPHTHALENE
4.3U	2-METHYLPHENOL
4.3U	2-NITROANILINE
4.3U	2-NITROPHENOL
4.3U	3.3'-DICHL0R0BENZIDINE
4 3U	3-NITROANILINE
4.3U	4-BR0M0PHENYL PHENYL ETHER
4.3U	4-CHL0R0-3-METHYLPHEN0L
4.3U	4-CHL0R0ANILINE
4.3U	4-CHL0R0PHENYL PHENYL ETHER
4.3U	4-NITROANILINE
8.6U	4-NITROPHENOL
4.3U	ACENAPHTHENE
4.3U	ACENAPHTHYLENE
4.3U	ANTHRACENE
4.3U	BENZO(A)ANTHRACENE
4.3U	BENZO(B AND/OR K)FLUORANTHENE
MG/KG	ANALYTICAL RESULTS
4.3U	BENZO(GHIJPERYLENE
4.3U	BENZO-A-PYRENE
4.3U	BENZYL BUTYL PHTHALATE
4 3U	BIS(2-CHLOROE THOXY) METHANE
4.3U	BIS(2-CHLOROETHYL) ETHER
4.3U	BIS(2-ETHYLHEXYL) PHTHALATE
4.3U	CARBAZOLE
4.3U	CHRYSENE
4.3U	DI-N-BUTYLPHTHALATE
4.3U	DI-N-OCTYLPHTHALATE
4.3U	DIBENZO(A.H(ANTHRACENE
4.3U	DIBENZOFURAN
4.3U	DIETHYL PHTHALATE
4.3U	DIMETHYL PHTHALATE
4.3U	FLUORANTHENE
4.3U	FLUORENE
4.3U	HEXACHLOROBENZENE (HCB)
4.3U	HE XACHLOROBUT ADIENE
4.3U	HEXACHLOROCYCLOPENTADIENE (HCCP)
4 3U	HEXAfHLOROETHANE
4.3U	INDENO (1.2,3-CD) PYRENE
4.3U	ISOPHORONE
4.3U	N-NITROSODI-N-PROPYLAMINE
4.3U	N-NITROSODI PHENYLAMINE/DI PHENYLAMINE
4 3U	NAPHTHALENE
4.3U	NITROBENZENE
8.6U	PENTACHLOROPHENOL
4 3U	PHENANTHRENF
4.3U	PHENOL
4 3U	PYRENE
»«'REMARKS'**
••~REMARKS***
**'FOOTNOTES***
*A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV ES. ATHENS, GA.	12 93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
•* PROJECT
NO. 94-0050 SAMPLE NO. 80630 SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED
BY: B CARTER **
*» SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL **
** STATION
* *
ID: TC104/105 GAMBUSIA
COLLECTION START: 10/20/93
1130 STOP" 00/00/00 *•
* *
ANALYTICAL RESULTS MG/KG
10JN	TETRADECANOIC ACID
10JN	PENTADECANOIC ACID (2 ISOMERS)
90JN	HEXADECENOIC ACID
100JN	HEXADECANOIC ACID
20JN	HEPTADECANOIC ACID (3 ISOMERS)
40JN	OCTADECANOIC ACID
6JN	NONADECANOIC ACID
10JN	BIS(HYDROXYETHYL)DODECANAMIDE
50J	3 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
• R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS	EMENT SYSTEM
EPA-REGION IV ES. .HENS, GA.
12
PROJECT NO. 94-0050 SAMPLE NO. 80631 SAMPLE TYPE: FISH
SOURCE: TOWER CHEMICAL
STATION ID. TCI08 GAMBUSIA
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1315 STOP: 00/00/00
MG/KG	ANALYTICAL RESULTS
13U	(3-AND/OR 4-)METHYLPHENOL
13U	1.2.4-TRICHLOROBENZENE
13U	2.2'-CHLOROISOPROPYLETHER
13U	2,3.4.6-TETRACHLOROPHENOL
13U	2.4,5-TRICHL0R0PHEN0L
13U	2.4,6-TRICHLOROPHENOL
13U	2.4-DICHLOROPHENOL
13U	2.4-DIME THYL PHE NOL
26U	2.4-DINITROPHE NOL
13U	2.4-0INITR0T0LUENE
13U	2,6-DINITROTOLUENE
13U	2-CHLORONAPHTHALENE
13U	2-CHLOROPHENOL
26U	2-METHYL-4,6-DINITROPHENOL
13U	2-METHYLNAPHTHALENE
13U	2-METHYLPHENOL
13U	2-NITROANILINE
13U	2-NITROPHENOL
13UJ	3.3'-DICHLOROBENZIDINE
13U	3-NITROANILINE
13U	4-BR0M0PHENYL PHENYL ETHER
13U	4-CHL0R0-3-METHYLPHEN0L
13U	4-CHL0R0ANILINE
13U	4-CHL0R0PHENYL PHENYL ETHER
13U	4-NITR0AN1LINE
26U	4-NITR0PHEN0L
13U	ACENAPHTHENE
13U	ACEWAPHTHYLENE
13U	ANTHRACENE
13UJ	BENZOtA)ANTHRACENE
13UJ	BENZOtB AND/OR MFLUORANTHENE
MG/KG	ANALYTICAL RESULTS
13UJ	BENZOtGHI)PERYLENE
13UJ	BENZO-A-PYRENE
13UJ	BENZYL BUTYL PHTHALATE
13U	BIS(2-CHLOROETHOXY) METHANE
1311	BIS(2-CHL0R0ETHYL) ETHER
13UJ	BIS(2-ETHYLHEXYL) PHTHALATE
13U	CARBAZOLE
13UJ	CHRYSENE
13U	DI-N-BUTYLPHTHALATE
13UJ	DI-N-OCTYLPHTHALATE
13UJ	DIBENZO(A.H)ANTHRACENE
13U	DIBENZOFURAN
13U	DIETHYL PHTHALATE
13U	DIMETHYL PHTHALATE
13UJ	FLUORANTHENE
13U	FLUORENE
13U	HEXACHLOROBENZENE (HCB)
13U	HEXACHLOROBUTADIENE
13U	HEXACHLOROCYCLOPENTADIENE (HCCP)
13U	HEXACHLOROE THANE
13UJ	INDENO (1.2.3-CD) PYRENE
13U	ISOPHORONE
13U	N-NITROSODI-N-PROPYLAMINE
13U	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
13U	NAPHTHALENE
13U	NITROBENZENE
26U	PENTACHLOROPHENOL
13U	PHENANTHRENE
13U	PHENOL
13UJ	PYRENE
*•'REMARKS***
••~REMARKS***
•~•FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALY2ED *NAI-INTERFERENCES •J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E.
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
*»»»»»»»»»»»»»»»»»»»•»»»
• * * *
PROJECT NO. 94-0050 SAMPLE NO.
SOURCE: TOWER CHEMICAL
STATION ID: TC108 GAMBUSIA
80631 SAMPLE TYPE: FISH
GEMENT SYSTEM
aTHENS, GA.
»»»»#»»»»»»»*»»»»»**»»»»»**»»
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1315 STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
70JN	HEXADECENOIC ACID
70JN	HEXADECANOIC ACID
20JN	OCTADECAN01C ACID
N	PETROLEUM PRODUCT
KSS&"?; Sri:?II0THAM-^^INS!5?5RESEElcT5}!:E5i;!ftT!i K	MESEMCE 0F M1TERI4L
:u=o£"5£tfeA^! fs;vvA?AFS5ui^rcSB6J!D»»rBRNa«em!srEPR?i"irli?^[iii;,s!Di-jEi;ALvsis is	™ verification-
-------
SAMPLE AND ANALYSIS GEMENT SYSTEM
_ .	EPA-REGION IV E. ,THENS, GA.	1k
EXTRACTABLE ORGANICS DATA REPORT
•• PROJECT
NO. 94-0050 SAMPLE NO. 80632 SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED
BY: B CARTER **
•~ SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL ••
»» STATION
* •
ID: TC111 GAMBUSIA
COLLECTION START: 10/22/93
1730 STOP: 00/00/00 **
* *
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
29U
(3-AND/OR 4-)METHYLPHENOL
29UJ
BENZO(GHI)PERYLENE
29U
1,2.4-TRICHLOROBENZENE
290J
8ENZ0-A-PYRENE
29U
2.2'-CHLOROISOPROPYLETHER
29UJ
BENZYL BUTYL PHTHALATE
29U
2.3.4.6-TETRACHL0R0PHEN0L
29U
BIS(2-CHLOROETHOXY) METHANE
29U
2.4.5—TRICHLOROPHE NOL
29U
BIS(2-CHLOROETHVL) ETHER
29U
2.4.6-TRICHLOROPHE NOL
29UJ
BIS(2-ETHYLHEXYL) PHTHALATE
29U
2,4-DICHLOROPHENOL
29U
CARBAZOLE
29U
2.4-OIMETHYLPHENOL
29UJ
CHRYSENE
58 U
2,4-DINITR0PHEN0L
29U
DI-N-BUTYLPHTHALATE
29U
2,4-DINITROTOLUENE
29UJ
DI-N-OCTYLPHTHALATE
29U
2.6-DINITR0T0LUENE
29UJ
DIBENZOC A.H)ANTHRACENE
29U
2-CHL0R0NAPHTHALENE
29U
DIBENZOFURAN
29U
2-CHLOROPHENOL
29U
DIETHYL PHTHALATE
58U
2-METHYL-4.6-DINITR0PHEN0L
29U
DIMETHYL PHTHALATE
29U
2-METHYLNAPHTHALENE
29UJ
FLUORANTHENE
29U
2-METHYLPHENOL
29U
FLUORENE
29U
2-NITROANILINE
29U
HEXACHLOROBENZENE (HCB)
29U
2-NITROPHENOL
29U
HEXACHLOROBUTADIENE
29UJ
3.3'-DICHLOROBENZIDINE
29U
HEXACHLOROCYCLOPENTADIENE (HCCP)
29U
3-NITROANILINE
29U
HEXACHLOROETHANE
29U
4-BR0M0PHENYL PHENYL ETHER
29UJ
INDENO (1.2.3-CD) PYRENE
29U
4-CHL0R0-3-METHYLPHEN0L
29U
1S0PH0R0NE
29U
4-CHL0R0ANILINE
29U
N-NITROSODI-N-PROPYL AMINE
29U
4-CHL0R0PHENYL PHENYL ETHER
29U
N-NITROSODI PHENYLAMINE/DIPHENYLAMINE
29U
4-NIT ROANILINE
29U
NAPHTHALENE
58U
4-NITR0PHEN0L
29U
NITROBENZENE
29U
ACENAPHTHENE
58U
PENTACHLOROPHENOL
29U
ACENAPHTHYLENE
29U
PHENANTHRENE
29U
ANTHRACENE
29U
PHENOL
29UJ
BENZO(A)ANTHRACENE
29UJ
PYRENE
29UJ
BENZOCB AND/OR K)FLUORANTHENE


~••REMARKS***	•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES •J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSI	VGEMENT SYSTEM
EPA-REGION IV L ATHENS, GA.	1 93
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
»• PROJECT
NO. 94-0050 SAMPLE NO. 80632 SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED
BY: B CARTER »*
•• SOURCE:
TOWER CHEMICAL
CITY: CLERMONT
ST: FL »»
*« STATION
• •
ID: TC111 GAMBUSIA
COLLECTION START* 10/22/93
1730 STOP: 00/00/00 *»
* *
ANALYTICAL RESULTS MG/KG
40JN HEXADECANOIC ACID
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED «NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
*R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
.THENS, GA.
12
PROJECT NO. 94-0050 SAMPLE NO. 80633
SOURCE: TOWER CHEMICAL
STATION ID: TC121 MIXED FISH
SAMPLE TYPE: FISH
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/23/93 1000 STOP. 00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
3.1U
(3-AND/OR 4-JMETHYLPHENOL
3. 1U
BENZO(GHI)PERYLENE
3.1U
1.2.4-TR1CHLOROBENZENE
3. 1U
BENZO-A-PYRENE
3.1U
2.2'-CHLOROISOPROPYLETHER
3. 1U
BENZYL BUTYL PHTHALATE
3.1UJ
2.3.4,6-TETRACHLOROPHENOL
3. 1U
BIS(2-CHLOROETHOXY) METHANE
3. 1UJ
2.4.5-TRICHLOROPHE NOL
3. 1U
BIS(2-CHLOROETHYL) ETHER
3.1UJ
2.4,6-TRICHL0R0PHEN0L
3. 1U
BIS(2-ETHYLHEXYL) PHTHALATE
3.1U
2.4-DICHL0R0PHEN0L
3. 1U
CARBAZOLE
3.1U
2.4-DIMETHYLPHENOL
3. 1U
CHRYSENE
6.211J
2.4-DINITROPHENOL
3. 1U
DI-N-BUTYLPHTHALATE
3. 1UJ
2.4-DINITR0T0LUENE
3. 1U
DI-N-OCTYLPHTHALATE
3. 1UJ
2.6-DINITR0T0LUENE
3. 1U
DIBENZOCA.H)ANTHRACENE
3.1UJ
2-CHL0R0NAPHTHALENE
3. 1UJ
DIBENZOFURAN
3.1U
2-CHL0R0PHEN0L
3. 1 UJ
DIETHYL PHTHALATE
6.2U
2-METHYL-4.6-DINITROPHENOL
3. 1UJ
DIMETHYL PHTHALATE
3.1U
2-METHYLNAPHTHALENE
3 1U
FLUORANTHENE
3.1U
2-METHYLPHEN0L
3. 1UJ
FLUORENE
3.1UJ
2-NITROANILINE
3. 1U
HEXACHLOROBENZENE (HCB)
3. 1U
2-NITROPHENOL
3. 1U
HEXACHLOROBUTADIENE
3.1U
3,3'-DICHLOROBENZIDINE
3. 1UJ
HEXACHLOROCYCLOPENTADIENE (HCCP)
3. 1UJ
3-NIT ROANILINE
3 1U
hexachloroethane
3. 1U
4-BR0M0PHENYL PHENYL ETHER
3. 1U
INDENO (1.2.3-CD) PYRENE
3. 1U
4-CHL0R0-3-METHYLPHENOL
3. 1U
ISOPHORONE
3. 1U
4-CHL0R0ANILINE
3. 1U
N-NITROSODI-N-PROPYLAMINE
3.1UJ
4-CHL0R0PHENYL PHENYL ETHER
3. 1U
N-NITROSODI PHENYLAMINE/DIPHENYLAMINE
3. 1UJ
4-NITROANILINE
3 IU
NAPHTHALENE
6.2UJ
4-NITROPHENOL
3. 1U
NITROBENZENE
3. 1UJ
ACENAPHTHENE
6.2U
PENTACHLOROPHENOL
3. 1 UJ
ACENAPHTHYLENE
3 1U
PHENANTHRENE
3. 1U
ANTHRACENE
3. 1U
PHENOL
3 1U
BENZO(A)ANTHRACENE
3. 1U
PYRENE
3. 1U
BENZOtB AND/OR K)FLUORANTHENE


•••REMARKS*•»
•••REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED «NAI-INTERFERENCES *J-ESTIMATED VALUE 'N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REG10N IV E- THENS. GA.	12
SCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT	^ ^
PROJECT*NO. 94-0050 SAMPLE NO. 80633 SAMPLE TYPE: FISH	PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT	ST: IFL 	
STATION ID: TC121 MIXED PISH	COLLECTION START: 10/23/93 1000 STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
10JN	HEXADECENOIC ACID
50JN	HEXADECANOIC ACID
30JN	OCTADECANOIC ACID
N	PETROLEUM PRODUCT
•••FOOTNOTES'**
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
'K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ES fHENS. GA.
12 3
PROJECT NO. 94-0050 SAMPLE NO. 80634
SOURCE: TOWER CHEMICAL
STATION ID: TC101 SAURURUS
SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1205 STOP: 00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
1,9U
(3-AND/OR 4-)METHYLPHEN0L
1 ,9U
BENZOCGHI)PERYLENE
1.9U
1,2.4-TRICHLOROBENZENE
1 . 9U
BENZO-A-PYRENE
1,9U
2.2'-CHLOROISOPROPYLETHER
1 . 9U
BENZYL BUTYL PHTHALATE
1.9U
2.3.4.6-TETRACHLOROPHENOL
1 . 9U
BIS(2-CHLOROETHOXY) METHANE
1 ,9U
2.4.5-TRICHL0R0PHEN0L
1 . 9U
BIS(2-CHLOROETHYL) ETHER
1,9U
2.4.6-TRICHL0R0PHEN0L
1 . 9U
BIS(2-ETHYLHEXYL) PHTHALATE
1 ,9U
2,4-DICHL0R0PHEN0L
1 . 9U
CARBAZOLE
1,9U
2.4-DIMETHYLPHENOL
1 . 9U
CHRYSENE
3.7U
2,4-DINITROPHENOL
1 . 9U
DI-N-BUTYLPHTHALATE
1 .9U
2.4-DINITROTOLUENE
1 . 9U
DI-N-OCTYLPHTHALATE
1.9U
2.6-DINITROTOLUENE
1 .9U
DIBENZO(A.HJANTHRACENE
1.9U
2-CHLORONAPHTHALENE
1 . 9U
DIBENZOFURAN
1 9U
2-CHLOROPHENOL
1 .9U
DIETHYL PHTHALATE
3. 7U
2-METHYL-4.6-DINITROPHENOL
1 ,9U
DIMETHYL PHTHALATE
1.9U
2-METHYLNAPHTHALENE
1 ,9U
FLUORANTHENE
1 . 9U
2-METHYLPHENOL
1 . 9U
FLUORENE
1 . 9U
2-NITROANILINE
1 . 9U
HEXACHLOROBENZENE (HCB)
1 . 9U
2-NITROPHENOL
1 ,9U
HEXACHLOROBUTADIENE
1 . 9U
3.3'-DICHL0R0BENZIDINE
1 . 9U
HEXACHLOROCYCLOPENTADIENE (HCCP)
1 9U
3-NITROANILINE
1 9U
HEXACHLOROETHANE
1 . 9U
4-BROMOPHENYL PHENYL ETHER
1 ,9U
INDENO (1.2.3-CD) PYRENE
1 . 9U
4-CHL0R0-3-METHYLPHEN0L
1 ,9U
ISOPHORONE
1 . 9U
4-CHL0R0ANILINE
1 ,9U
N-NITROSODI-N-PROPYLAMINE
1 . 9U
4-CHL0R0PHENYL PHENYL ETHER
1 ,9U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
1 9U
4-NITROANILINE
1 .90
NAPHTHALENE
3. 7U
4-NITROPHENOL
1 ,9U
NITROBENZENE
1 . 9U
ACENAPHTHENE
3. 7U
PENTACHLOROPHENOL
1 9U
ACENAPHTHYLENE
1 9U
PHENANTHRENE
1 9U
ANTHRACENE
1 . 9U
PHENOL
1 . 9U
BENZO(A)ANTHRACENE
1 . 9U
PYRENE
1 . 9U
BENZCKB AND/OR K)FLUORANTHENE


•*»REMARKS»*»
*•'REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE «NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIOENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS 3EMENT SYSTEM
EPA-REGION IV El .THENS¦ GA.
12
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80634 SAMPLE TYPE:	VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITV: CLERMONT ST:fL nn/OO/OO
STATION ID: TC101 SAURURUS	COLLECTION START. 10/21/93 1205 STOP. OO/OO/UU
ANALYTICAL RESULTS MG/KG
4JN	METHYL(METHYLETHYL )BICYCOLHEXENE
50JN	(PROPENYL)BENZODIOXOLE
6JN	CARYOPHYLLENE
9JN	DODECANOIC ACID
40J	4 UNIDENTIFIED COMPOUNDS
'"™IvER«ir;«LUE "NA-NOT ANAIY2E0 »MAI-INTERFERENCES • J-ESTIMATED VALUE .»-|RES^PTIVE EVIDENCE OF PRESENCE OF MATERIAL
»K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATER1AL WAS ANALY2ED FOR BUT NOT DETECTED THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	NFrF«;SARY FOR VERIFICATION
»R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR vtKiritAiiu
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS GEMENT SYSTEM
EPA-REGION IV E- UHENS, GA.
12, 33
PROJECT NO. 94-0050 SAMPLE NO. 80635
SOURCE: TOWER CHEMICAL
STATION ID: TC103 SAURURUS
SAMPLE TYPE: VEGETATIOM
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/22/93 1215 STOP:
00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
2.3U
(3-AND/OR 4-JMETHYLPHENOL
2.3U
BENZO(GHI)PERYLENE
2.3U
1.2.4-TRICHLOROBENZENE
2.3U
BENZO-A-PYRENE
2.3U
2.2'-CHLOROISOPROPYLETHER
2.3U
BENZYL BUTYL PHTHALATE
2.3U
2.3.4.6-TETRACHLOROPHENOL
2.3U
BIS(2-CHLOROETHOXY) METHANE
2.3U
2.4.5-TRICHL0R0PHEN0L
2.3U
BIS(2-CHLOROETHYLJ ETHER
2.3U
2.4 ,6-TRICHLOROPHENOL
2.3U
BIS(2-ETHYLHEXYL) PHTHALATE
2.3U
2,4-DICHLOROPHE NOL
2.3U
CARBAZOLE
2.3U
2.4-DIME THYL PHE NOL
2 . 3U
CHRYSENE
4.6U
2.4-DINITROPHENOL
2.3U
DI-N-BUTYLPHTHALATE
2.3U
2,4-DINITR0T0LUENE
2.3U
DI-N-OCTYLPHTHALATE
2.3U
2.6-DINITROTOLUENE
2.3U
DIBENZO(A.H)ANTHRACENE
2.3U
2-CHLORONAPHTHALENE
2.3U
DIBENZOFURAN
2.3U
2-CHLOROPHENOL
2.3U
DIETHYL PHTHALATE
4.6U
2-METHYL-4.6-DINITR0PHEN0L
2.3U
DIMETHYL PHTHALATE
2.3U
2-METHYLNAPHTHALENE
2 3U
FLUORANTHENE
2.3U
2-METHYLPHENOL
2.3U
FLUORENE
2.3U
2-NITR0ANIL1NE
2.3U
HEXACHLOROBENZENE (HCB)
2.3U
2-NITROPHENOL
2.3U
HEXACHLOROBUTADIENE
2.3U
3.3'-DICHL0R0BENZIDINE
2.3U
HEXACHLOROCYCLOPENTADIENE (HCCP)
2 3U
3-NITROANILINE
2.3U
HEXACHLOROETHANE
2.3U
4-BR0M0PHENYL PHENYL ETHER
2.3U
INDENO (1.2.3-CD) PYRENE
2.3U
4-CHLORO-3-METHYLPHENOL
2 3U
ISOPHORONE
2.3U
4-CHLOROANILINE
2.3U
N-NITROSODI-N-PROPYLAMINE
2.3U
4-CHL0R0PHENYL PHENYL ETHER
2.3U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2 3U
4-NITROANILINE
2 3U
NAPHTHALENE
4.6U
4-NITROPHENOL
2.3U
NITROBENZENE
2.3U
ACENAPHTHENE
4.6U
PENTACHLOROPHENOL
2.3U
ACENAPHTHYLENE
2 3U
PHENANTHRENE
2.3U
ANTHRACENE
2.3U
PHENOL
2. 3U
BENZ0(A)ANTHRACENE
2.3U
PYRENE
2.3U
BENZO(B AND/OR K)FLUORANTHENE


•••REMARKS'**
•»'REMARKS**•
•••FOOTNOTES*«*
•A-AVERAGE VALbF «NA-NOT ANALYZED »NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALY2ED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV E.
GEMENT SYSTEM
«THENS, GA.
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT	....
PROJECT NO. 94-0050 SAMPLE NO. 80635 SAMPLE	TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE TOWER CHEMICAL	CITY: CLERMONT ST: FL
STATION ID: TC103 SAURURUS	COLLECTION START: 10/22/93 1215 STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
30JN	DIMETHOXY(PROPENYL)BENZENE
3JN	CARYOPHYLLENE
20JN	(DIMETHYLBUTYL)METHOXYBENZENE
30J	3 UNIDENTIFIED COMPOUNDS
•A-AVERAGE VALUE «NA-NOT ANALYZED »NAI-INTERFERENCES «J-ESTIMATED VAUJE .N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN 'L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
• U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM OUANTITATIW LIMIT	pnp i/ppi r irAT TDkl
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGAN!CS DATA REPORT
SAMPLE AND ANALYSII
EPA-REGION IV E.
GEMENT SYSTEM
ATHENS, GA.
PROJECT NO. 94-0050 SAMPLE NO. 80636
SOURCE: TOWER CHEMICAL
STATION ID: TC105 SAURURUS
SAMPLE TYPE: VEGETATION
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/19/93 1800 STOP: 00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
2.2U
(3-AND/OR 4-JMETHYLPHENOL
2.2U
BENZOCGHI)PERYLENE
2.2U
1 .2.4-TRICHLOROBENZENE
2.2U
BENZO-A-PYRENE
2.2U
2.2'-CHLOROISOPROPYLETHER
2.2U
BENZYL BUTYL PHTHALATE
2.2U
2,3.4.6-TETRACHLOROPHENOL
2 2U
BIS(2-CHLOROETHOXY) METHANE
2.2U
2.4.5-TRICHLOROPHENOL
2 2U
BIS(2-CHLOROETHYL) ETHER
2.2U
2.4.6-TRICHLOROPHENOL
2.2U
BIS(2-ETHYLHEXYL) PHTHALATE
2.2U
2.4-DICHLOROPHENOL
2.2U
CARBAZOLE
2.2U
2.4-DIMETHYLPHENOL
2.2U
CHRYSENE
4.3U
2.4-DINITROPHENOL
2.2U
DI-N-BUTYLPHTHALATE
2.2U
2.4-OINITROTOLUENE
2.2U
DI-N-OCTYLPHTHALATE
2.2U
2.6-DINITROTOLUENE
2.2U
DIBENZO(A.H)ANTHRACENE
2 . 2U
2-CHLORONAPHTHALENE
2.2U
DIBENZOFURAN
2.2U
2-CHLOROPHENOL
2.2U
DIETHYL PHTHALATE
4.3U
2-METHYL-4.6-DINITROPHENOL
2.2U
DIMETHYL PHTHALATE
2.2U
2-METHYLNAPHTHALENE
2 2U
FLUORANTHENE
2.2U
2-METHYLPHENOL
2.2U
FLUORENE
2.2U
2-NITROANILINE
2.2U
HEXACHLOROBENZENE (HCB)
2.2U
2-NITROPHENOL
2.2U
HEXACHLOROBUTADIENE
2.2U
3.3'-DICHLOROBENZIDINE
2.2U
HEXACHLOROCYCLOPENTADIENE (HCCP)
2 2U
3-NITROANILINE
2 2U
HEXACHLOROETHANE
2.2U
4-BROMOPHENYL PHENYL ETHER
2.2U
INDENO (1.2.3-CD) PYRENE
2.2U
4-CHLORO-3-METHYLPHENOL
2.2U
ISOPHORONE
2.2U
4-CHLOROANILINE
2.2U
N-NITROSODI-N-PROPYLAMINE
2.2U
4-CHL0R0PHENYL PHENYL ETHER
2.2U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2.2U
4-NITR0ANILINE
2 2U
NAPHTHALENE
4.3U
4-NITR0PHEN0L
2.2U
NITROBENZENE
2.2U
ACENAPHTHENE
4.3U
PENTACHLOROPHENOL
2.2U
ACENAPHTHYLENE
2.2U
PHENANTHRENE
2.2U
ANTHRACENE
2.2U
PHENOL
2 2U
BENZ0(A)ANTHRACENE
2 2U
PYRENE
2.2U
BENZOtB AND/OR K)FLUORANTHENE


•»'REMARKS*»*
••~REMARKS***
•••FOOTNOTES***
•A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPT1VE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS iEMENT SYSTEM
EPA-REGION IV ES THENS. GA.
12,
MISCELLANEOUS EXTRACTABLE COMPOUNOS - DATA REPORT
PROJECT NO. 94-0050 SAMPLE NO. 80636 SAMPLE TYPE.	VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	CITY: CLERMONT ST: EL
STATION ID: TC105 SAURURUS	COLLECTION START* 10/19/93 1800 STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
70JN (PROPENYL JBENZODIOXOLE
20J 2 UNIDENTIFIED COMPOUNDS
•••FOOTNOTES***
•A-AVERAGE VALUE *NA-NOT ANALYZED »NAI-INTERFERENCES »J-ESTIMATED VALUE «N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
•R-OC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT. BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSIS
EPA-REGION IV EL
3EMENT SYSTEM
.THENS, GA.
12.
,3
PROJECT NO. 94-0050 SAMPLE NO. 80637
SOURCE: TOWER CHEMICAL
STATION ID: TC106 SAURURUS
SAMPLE TYPE: VEGETATION
PROG ELEM: SSF COLLECTED BY: B CARTER
CITY- CLERMONT	ST: FL
COLLECTION START: 10/20/93 1510 STOP:
00/00/00
MG/KG
ANALYTICAL RESULTS
MG/KG
ANALYTICAL RESULTS
2.7U
(3-AND/OR 4-)METHYLPHEN0L
2. 7U
BENZO(GHI)PERYLENE
2.7U
1, 2,4-TRICHL0R0BENZENE
2 7U
BENZO-A-PYRENE
2 . 7U
2.2'-CHLOROISOPROPYLE THER
2. 7U
BENZYL BUTYL PHTHALATE
2.7U
2.3,4.6-TETRACHL0R0PHEN0L
2. 7U
BIS(2-CHL0R0ETHOX Y) METHANE
2. 7U
2.4,5-TRICHLOROPHENOL
2 7U
BIS(2-CHL0R0ETHYL) ETHER
2.7U
2.4.6-TRICHLOROPHENOL
2. 7U
BIS(2-ETHYLHEXYL) PHTHALATE
2 . 7U
2.4-DICHLOROPHENOL
2. 7U
CARBAZOLE
2. 7U
2.4-DIMETHYLPHENOL
2. 7U
CHRYSENE
5.5U
2,4-DINITROPHENOL
2 . 7U
DI-N-BUTYLPHTHALATE
2.7U
2,4-DINITR0T0LUENE
2 7U
DI-N-OCTYLPHTHALATE
2.7U
2,6-DINITROTOLUENE
2. 7U
DIBENZO(A.H)ANTHRACENE
2 . 7U
2-CHLORONAPHTHALENE
2. 7U
DIBENZOFURAN
2. 7U
2-CHLOROPHENOL
2 . 7U
DIETHYL PHTHALATE
5.5U
2-METHYL-4.6-DINITROPHENOL
2. 7U
DIMETHYL PHTHALATE
2 . 7U
2-ME THYLNAPHTHALENE
2 7U
FLUORANTHENE
2.7U
2-METHYLPHENOL
2. 7U
FLUORENE
2.7U
2-NITROANILINE
2 7U
HEXACHLOROBENZENE (HCB)
2.7U
2-NITROPHENOL
2. 7U
HEXACHLOROBUTADIENE
2. 7U
3.3'-DICHL0R0BEN2IDINE
2 7U
HEXACHLOROCYCLOPENTADIENE (HCCP)
2 7U
3-NITR0ANIL1NE
2 7U
HEXACHLOROETHANE
2. 7U
4-BROMOPHENYL PHENYL ETHER
2.7U
INDENO (1.2.3-CD) PYRENE
2.7U
4-CHL0R0-3-METHYLPHEN0L
2. 7U
ISOPHORONE
2 . 7U
4-CHL0R0ANILINE
2. 7U
N-NITROSODI-N-PROPYLAMINE
2. 7U
4-CHL0R0PHENYL PHENYL ETHER
2. 7U
N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2. 7U
4-NITR0ANILINE
2. 7U
NAPHTHALENE
5. 5U
4-NITROPHENOL
2. 71)
NITROBENZENE
2 . 7U
ACENAPHTHENE
5 5U
PENTACHLOROPHENOL
2 . 7U
AC.ENAPHTHYLENE
2 7U
PHENANTHRENE
2.7U
ANTHRACENE
2. 7U
PHENOL
2 7U
BENZOlA)ANTHRACENE
2. 7U
PYRENE
2. 7U
BENZ0(B AND/OR K)FLUORANTHENE


»*'REMARKS*»»
*•'REMARKS*»»
* * * FOOTNOTES* » »
~A-AVERAGE VALUE »NA-NOT ANALYZED *NAI-INTERFERENCES »J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
*U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
SAMPLE AND ANALYSIS
EPA-REGION IV EL
3EMENT SYSTEM
.THENS, GA.
12,
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT
~ »~«»»•***•»**»»•**•»•»»»«•*»*****•******
PROJECT NO. 94-0050 SAMPLE NO. 80637 SAMPLE TYPE: VEGETATION PROG ELEM: SSF
SOURCE: TOWER CHEMICAL
STATION ID: TC106 SAURURUS
*•»**»•»»»•*»***
COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/20/93 1510 STOP: 00/00/00
ANALYTICAL RESULTS MG/KG
8JN (PROPENYL)BENZ0DI0X0LE
40JN DIMETHYL(PROPENYL)BENZENE
60J 4 UNIDENTIFIED COMPOUNDS
'":Si?vr»?Eis	gri:?II0THAM-^GlNJ?5[SRE^-lcTu^c5I^T!i K ,oNirEI^"iufhIK'SISSI givenesence of "1TERIAL
:S3STfS}tAul ?SirlS?Ar8Su!^rc8£JSW»NWEWSErH^¥%™KI5"2»DLjEi;«LV51S IS NECESSARY FOR VERIFICATION.
-------
EXTRACTABLE ORGANICS DATA REPORT
SAMPLE AND ANALYSI
EPA-REGION IV
CEMENT SYSTEM
ATHENS. GA.
93
PROJECT NO. 94-0050 SAMPLE MO. 80638
SOURCE: TOWER CHEMICAL
STATION ID: TC108 SAURURUS
SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
CITY: CLERMONT	ST: FL
COLLECTION START: 10/21/93 1315 STOP: 00/00/00
MG/KG	ANALYTICAL RESULTS
2.9U	(3-AND/0R 4-)METHYLPHEN0L
2.9U	1,2.4-TRICHLOROBENZENE
2.9U	2.2'-CHLOROISOPROPYLETHER
2.9U	2.3.4.6-TETRACHLOROPHENOL
2.9U	2.4,5-TRICHLOROPHENOL
2.9U	2.4,6-TRICHLOROPHENOL
2.9U	2.4-DICHLOROPHENOL
2.9U	2.4-DIMETHYLPHENOL
5.7U	2,4-DINITROPHENOL
2.9U	2,4-DINITROTOLUENE
2.9U	2.6-DINITROTOLUENE
2.9U	2-CHLORONAPHTHALENE
2.9U	2-CHLOROPHENOL
5.7U	2-METHYL-4,6-DINITROPHENOL
2.9U	2-METHYLNAPHTHALENE
2.9U	2-METHYLPHENOL
2.9U	2-NITROANILINE
2.9U	2-NITROPHENOL
2.9U	3.3'-DICHLOROBEN2IDINE
2.9U	3-NITR0ANIL1NE
2.9U	4-BROMOPHENYL PHENYL ETHER
2.9U	4-CHL0R0-3-METHYLPHEN0L
2.9U	4-CHL0R0ANILI NE
2.9U	4-CHL0R0PHENYL PHENYL ETHER
2.9U	4-NITROANILINE
5.7U	4-NITROPHENOL
2.9U	ACENAPHTHENE
2.9U	ACENAPHTHYLENE
2.9U	ANTHRACENE
2.9U	BENZO(A)ANTHRACENE
2.9U	BENZO(B AND/OR KJFLUORANTHENE
MG/KG	ANALYTICAL RESULTS
2.9U	BENZOCGHI)PERYLENE
2.9U	BENZO-A-PYREME
2.9U	BENZYL BUTYL PHTHALATE
2.9U	BIS(2-CHLOROETHOXY) METHANE
2.9U	BIS(2-CHLOROETHYL) ETHER
2.9U	BIS(2-ETHYLHEXYL) PHTHALATE
2 9U	CARBAZOLE
2.9U	CHRYSENE
2.9U	DI-N-BUTYLPHTHALATE
2 9U	DI-N-OCTYLPHTHALATE
2.9U	DIBENZO(A,H)ANTHRACENE
2.9U	DIBENZOFURAN
2.9U	DIETHYL PHTHALATE
2.9U	DIMETHYL PHTHALATE
2.9U	FLUORANTHENE
2.9U	FLUORENE
2.9U	HEXACHLOROBENZENE (HCB)
2.9U	HE XACHLOROBUT ADIENE
2.9U	HEXACHLOROCYCLOPENTADIENE (HCCP)
2 9U	HE XAC.HLOROE THANE
2.9U	INDENO (1,2.3-CD) PYRENE
2.9U	ISOPHORONE
2.9U	N-NITROSODI-N-PROPYLAMINE
2 9U	N-NITROSODIPHENYLAMINE/DIPHENYLAMINE
2 9U	NAPHTHALENE
2.9U	NITROBENZENE
5.7U	PENTACHLOROPHENOL
2 9U	PHENANTHRENE
2.9U	PHENOL
2 9U	PYRENE
«»»REMARKS»»*
»«'REMARKS'•»
~••FOOTNOTES***
~A-AVERAGE VALUE *NA-NOT ANALYZED *NAI-INTERFERENCES *J-ESTIMATED VALUE *N-PRESUMPTIVE EVIDENCE OF PRESENCE OF MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN *L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
~U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT.
-------
sample and analysh gement system
EPA-REGION IV E aTHENS, GA.
MISCELLANEOUS EXTRACTABLE COMPOUNDS - DATA REPORT		
PROJECT NO. 94-0050 SAMPLE NO.	80638 SAMPLE TYPE: VEGETATION PROG ELEM: SSF COLLECTED BY: B CARTER
SOURCE: TOWER CHEMICAL	&1T,Y,^SV£EM£tL>t ,n/oi zoo flU crnD- nrwrvwnn
STATION ID: TC108 SAURURUS	COLLECTION START: 10/21/93 1315 STOP. 00/00/00
ANALYTICAL RESULTS MG/KG
100JN (PROPENYL)BENZODIOXOLE
5JN CARYOPHYLLENE
40J 2 UNIDENTIFIED COMPOUNDS
•A-AVERAGE VALUE »NA-NOT ANALYZED »NAI-INTERFERENCES "J-ESTIMATED VAUJE TAN«RrlcA?cl tuIw Sa^mf rfuFM	MATERIAL
•K-ACTUAL VALUE IS KNOWN TO BE LESS THAN VALUE GIVEN »L-ACTUAL VALUE IS KNOWN TO BE GREATER THAN VALUE GIVEN
•U-MATERIAL WAS ANALYZED FOR BUT NOT DETECTED. THE NUMBER IS THE MINIMUM QUANTITATION LIMIT	UFr,,.„BV FnR urptrtrtTTnu
•R-QC INDICATES THAT DATA UNUSABLE. COMPOUND MAY OR MAY NOT BE PRESENT. RESAMPLING AND REANALYSIS IS NECESSARY FOR VERIFICATION.
-------
APPENDIX D
Laboratory Bench Sheets for Toxicity Tests Performed on Surface
Water and Sediment Samples
-------
SOP XV.4 Short-Term Chronic Toxicity Test — Cladoceran Summary Data
Industry/Study: *TI
Location: L»|cc Anapk*
Date Collected:
Analyst: /?Tl. , Aj  / w/rf
Staple $
tad/or
Cosecal ratios
Day
"/¦ /*•**¦«•/ V / /
Number
of Young
Number of
Surhi&g
Adulu
Young per
Adult
1
1
3
4
5
6
7
8
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7 c
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4
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&

5
-------
SOP XV.4 Short-Term Chronic Toxicity Test — Cladoceran Summary Data
Industry/Study: Tou^ty ^"AfmuW Analyst: ^ i J M
Location: L±kc Apjpkt Start (Date & Time): f '/i-v/'j7
Date Collected:			Stop (Date & Time):	
Sample 1
tnd/or
Cooceol ration

^ a y / ~ ~ ~ ~
Number
of Yoozif
Number of
SorriTifi^
AdulU
Young per
Adult
D»y
1 2
3 4
s
< 7
s
»
10

Off

U
W


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u
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in.
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t-
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<3
7

s
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jr
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'2-
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/ 3{f

tr.z
7*-
hi
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V
V

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ti-
16
?*l
to
?
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rtv
<7


Total
»?>
N
11
ll
xu
?-/
n
U
1 1

• It7
10
nn
rt
m


is
~V
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L
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7
-------
SOP XV.4 Short-Term Chronic Toxicity Test — Cladoceran Summary Data
Industry/Study; / °
Location:
Date Collected:
A"V/*	'
Analyst:
*31.
v/ /M
Start (Datc&TimcV.
Sample /
¦ad/or
Concentration
r*f
Kepiieate
Number
of Yo«n|
Number of
SurriTing
Adulla
Young per
Adult
1
2
3
4
5
<
7
s
9
10

i0



LS
i_—
i_^
i/-
¦ y
-------
ROOT ELONGATION
Industry/Study: ibyjjur	.	 Analyst: Mfr/MM
Locatipn: La.kg Aqq-> S-U*a^—	 Start (Date-Time): lO la i q 3 .
type of Seed: LgCtcUje >	Stop (Date-Time): (i\f 2.t»/V-». 7u ^
Sample
ID#
pH
Rep.
#
Root Lengths (mm)
Average
Length (mm)
Remarks
&JU

1
hi*

HO
47
OitnctfJS
H\.l~
--
")H
2
Uo
?o
M
ut*
V-k-

3
&
V5"
T>4

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2
m
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4






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r
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4








1







2






3






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3






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3






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2






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4






-------
\jO
ROOT ELONGATION
Industry/Study: ToCk e*v\.	 Analyst: ma / kuj	
Location: LoSsl Qy>0fkA		 Start (Date-Time):	Zp,^ .
Type of Seed:	Le-Uucg,	Stop (Date-Time): iolana*
•V •
Sample
ID#
PH
Rep.
#

Boot
lengths 0
mm)

Average
Length (mm)
Remarks
GucItpI
WU.'-Q

1
2
	
V7
	
fl
i>-?r
(/«
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(/ >*'
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53
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1







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3






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1







2






3






4






-------
ROOT ELONGATION
Industry/Study: Tou»*	J
Location: Ulc* Ay.
Type of Seed: llv*


Analyst: VAU^	
Start fDate-TimeV. )elZfjgi, l-'3gyt^ .
Stop (Date-Time):	2.'>*-o-imo
Sample
ID#
pll j
Rep.
#
Root Lengths (mm)
Average
Length (am)
Remarks
|ju


m.b
3
1
4






ft6elle«^
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31
2.4
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21 .T
3
2.b
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47
43
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1







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1







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3






4






)wW»j
-------
SOP XV
Revision No. 4
Date: September 10,1993
Page: 18 of 20
SUMMARY DATA
Industry/Study: f,ntpejr
Location: La.k&. /Wpiba., PL.	
Dale: loh-\ 193 f TO
Analyst: Am)	
N» <>
"a
»\«vl
?>
•»>D

V« s.
*\ ^
/ • T«l trfwlm «n««
X • T«l «rpMlim
Sanplt I
asd/er
CoaualrmlloB
D*r
RtpUcal*
Nubn
of Y*bb|
Number of
Surrlrlnf
Adolta
Younf par
Adult
* 3„
4 ^
3
"?
4 „ J. 6 7 1


CjokWo \
i r
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¦JH?
to-
H

IT


p->
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0-1
7.2-V

13> I
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If1
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f-T
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ifcfi

>h<1
ft'lOS"
lP
1/
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35
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7*/
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y
p
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-------
^	(s i>lrTO<*9
TbHoy
1










O

1
>










0


3










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5










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7
	

	

——





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Total
3=

2Z

W
E
s
IE
7-3
3=
5SI
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*??l
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i













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7




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Total
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2E
Lm.

tn-
3°
ic

&
-------

SOP XV
RtTliioa No. 4
Dale: September 10,1993
Page: 18 o(20
v
•o
<»
o\f VO
->i
Po^eji*. I
SUMMARY DATA
Industry/Study: Tou)eir CMmyucaSI
Location: lake Wyopk-*
Date: /o /x2.|Q ?> (frA 3:3or ^
Analyst: >Kti)	
Suoplt /
asd/or
Concentration
D»r
l*l M
RcpUcalo
Nunbtr
of Yona(
Number of
Siirrlfloi
AdaKj
Young p«r
Adult
% «h V

_!a Jjl
\

>/
V
~
~
J
yj
~
ix





is
i/

1/

~
V/

»>

J



3*1
*>
S"
L>


(0



7-



4r
~
V
y/

~
~
~
~
~
y
-r>


»w


9
9tl
(°
y
?+2-
?? '1
lo
b + 1



•r
wii

IH
1*2-
/r
/«/
/V
n
/,r
l{
mi



7f
/?+/

'v
13
/5-

/,?
H
//
/
1^6


Total
44


-b%
mn


HVf
41
Id
407

MO, 7
7t-\0*o
IS
/
V
V
t'

V
V
1/
»/
K



*3
V
~
V

~
S

~

/



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<>
4
mi
3f2-
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3
sT
V

S"
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4T
v/
V
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~
~
y
r\


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v>
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w

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v/
v/

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~
~
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V'/
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JUL
7
\n
tfi-l
X
so


4r

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i>
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~
V

IS
~
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SUJ
7^3

f°
?+/
;?


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7*2.
97'


«r
»?-
/<2-
r
6-/Z.
?
7
7
,r
3^-z.
in^t


«T
/+s~

h+l
b+t

/'7
7


f+t
Tj-


'P
Y
V
V
f
r
~
k
~
s
f
a«>


Total
,lt
Ite
I*


in!)
>4
»<
1-1

\c\ 0
1 )«1.0
-a'"*
13

V
V



~
~
V




»S
V
~
~
~
\/

u"

1/




3M
\/

4
Kl
w
3

H
?.
H




3

V
V
Y
V
1
V
V/
v/
1.0


5k>
~

S
5"
u>
S"+i.
fc

1
,r



•f
rT

HtH
1~t5~
4 + 7-
a+f
M
&¦/ /
V

 •Bw	X «T«loipatim 4*4	f • N««ikrr «f thr* r*vn| •# a tfenktc •( }*vii| M - Lmi m mlalni < > ktili
Figure XV.4 Short-Term Chronic Toxicity Test — Clndocerau Summary Data
O 1 o'r 3- (S«<
f a} '
-------
CtyyvtcM-**. fr1 IpcU+yi(3 ijy-txrtAs)
Fe^Y 2- •** 3-
SUMMARY DATA
Industry/Study: Touvt^fiA^ru-r^jP
Location: L«in Ayi^^i/d^.	
SOP XV
RcTistoo No. 4
Dale: September 10,1993
Page: 18 of 20
Date: (Fv. \ 3s
Analyst: i^vu)	
SuapU f
and/or
Conetnlralloa

JUpUult
Numbtr
•fYaut
Numbtr o(
Sarrltlnf
Adulu
I'ounf ptr
Adull
l»jr
1 2
3
4
s
<
7
•
9
10

1










0



2










O


OjwM
3










Xt


4










O


5













6
7










f*4 1



Total
Tto

v\




H2>
3c

JSHM
to
2s.<#
fC-10 k
1










O


2













3













4










O


5










q /


«
7










/as"



Total
3o
3.7
*1

/f?
1
27
ZQ 1
2? 1
w\
1
in ]


1










0


1










0


3










KD


4










0


5













5










t-3


«
7










7?*


Total
It
/ *•
Iff
12
ffi
"ZO

/8
/fe

^5-
* 0
/fewS1

1










0


2










0


3










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4










/ O


J










CS>-


«
7













Total
ft
11
20

/s-
»7
1
It
7
/r
K9-
/6
/a.x

1













2













3













4













S













<













7













Total |
1
1
1 1 1

1 1
~ * T«l trfMbai illv*
X " T«l •rpuiWre	i m Nvmfcrr •( II*t jwng	• Nvmfctr «f tfaJ j%*a| M • LmI «r «nU«lii|
Figure XV.4 Short-Term Chronic Toxicity Test — CIndoccrati Summary Data
- 0. 2.
• Malt
-------
1 tfx
SOP xv
Revision No. 4
Ditc: September 10,1993
Paget 18 of 20
SUMMARY DATA
Industry/Study: Toumat
Location: Lakt^Byo^lc^. PL
Date: lol^-M U a/Sum.?) l?3oP'^-
Analyst: M\>Q	
.A
-IV
SWDfl*
aad/sr
CoDttolrallaa
D»r
RtpUcal*
Nambtr
•rYomn*
Number •(
Sarrirlag
Adalu
Yni| for
Adalt
I 1 3 4 1 5 « | 7
• •
10


t/

V
~

U'
\S
~


0


n
\y


~
W

W

us
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o


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>
5W

r
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r
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3
s-+i
KVr


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V
V
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~
~
iS

~
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VI
Ur











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7*5
/I
Tv"4

n
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r

J 2-1-



7 8

~
-3

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%/
V
»/


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2-1
/



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y
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14
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figure XY.4
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Short-Term Chronic Toxicity Test — Cladoceran Summary Data
Q "Szjl Siwun^nj p 2, o?
-------
pSL o*r X.
CeYYtuA-^t S^r	(3 broods)	iUruion No. 4
5")
JL^CU/. O
SUMMARY DATA +
Industry/Study: Pule; to\3-M ha. H3of^ d^SAfl/ - 7.0f)
Location: uJa. Q^pk^ ; PL	Annljrsl: Maa)	
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tad/or
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3.0 1 l
-------
SOP XV
Rcrision No. 4
Date: September 10,1993
Pat" 18 of 20
SUMMARY DATA
Industry/Study:"*/^;#^QJ/[c^-V Dale: /0I^fQ ^[Xu»g ) to'* 3o&.
Location: Laid,	. PL-	 Analyst: M uJ	
SuspU #
and/or
Conctal ration

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Number of
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Figure XV.4 Short-Term Chronic Toxicity Test — CIndocci an Summary Dala
pi «fx
-------
CtrtY*-tAt*4 -firi
pJ2. .V- 2-
lOatM<
SOP XV
RtTisIoa No. 4
Datt: S«|i(cubcr 10,1993
P«|t: 18 of 20
SUMMARY DATA
Industry/Study: "Toustv
Location; Lfrla WpopJha P L	
Uutc: A? (afc/fl3 (Tiun^ fot3c? A .
Analyst: KcoJ	
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Short-Term Chronic Toxicity Test - Cladoccran Summary Data
-------
SEED GERMINATION DATA
Industry/study: iauioir	Analyst: Mto IJM 		
Location:	fyepk-*-		 Start (Date-Time): "/a-f I~
0
0

2
-------
SEED GERMINATION DATA
Industry/Study:	 Analyst's	
Location:	 Start (Date-Time):
Species:	 Stop (Date-Time):
Sample ID 8 or
Concentration
Rep.
#
# Seeds
Planted
. rt^Seeds
Germinated
Proportion
Germinated
Remarks
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Figure XVm.l
-------
SEED GERMINATION DATA
Industry/Study:	 Analyst:	
Location:		 Start (Date-Time):
Species:		 Slop (Date-Time):
Sample ID # or
Concentration
Rep.
I
# Seeds
Planted
Seeds
Germinated
Proportion
Germinated
Remarks
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Figure XVm.l
-------
SEED GERMINATION DATA
Industry/Study:	 Analyst:	
Location:	^ Start (Date-Time):
Species:	' ~ Stop (Date-Time):
Sample ID ti or
Concentration
Rep.
t
I Seeds
Planted
^wfiiSecds
Germinated
Proportion
Germinated
Remarks
TC'll|
1
5"
-------