project NO.
CD
O
AIR POLLUTION
EMISSION TEST
INTERNATIONAL MINERALS AND
CHEMICAL COMPANY
SPRUCE PINE, N, C.
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
Office of Air and Waste Management
Office of Air Qualify Planning and Standards
Emission Measurement Branch
Research Triangle Park. North Carolina
-------
EMISSION STUDY
a t a
FELDSPAR CRUSHING AND GRINDING FACILITY
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Prepared for the
U.S. Environmental Protection Agency
by
Clayton Environmental Consultants., Inc.
25711 Southfield Road
Southfield, Michigan 48075
Project NMM-1
Task 25
Contract No. 68-02-1408
-------
P.a.g e
I. Introduction ...... ...,,,.,,.,....,...<....,, 1
II. Summary and Discussion of Results ..,..,ป,...,.. 2
III. Process Description and Operation ..... . T ....... 30
IV, Location of Sampling Ports ............. ....... ป 31
V. Sampling and Analytical Procedures .............. 36
FIGURES
FIGURE 1 Location of Visible Emissions Observers
Feldspar Mine, September 27, 1976 .... ...... 5
FIGURE 2 Location of Visible Emissions Observers
Final Hilling Plant, September 28-29, 1976 . 6
FIGURE 3 Particle Size Distribution, No. 2 Mill
laghouse North Inlet ................ ..... ,. 28
FIGURE 4 Particle Size Distribution, No. 2 Mill
Baghocse South Inlet ..... ........... , ...... 29
v
FIGURE 5 Sche atic Diagram of Baghouse Inlet and Out-
let Ducts, No, 2 Mill Baghouse ...... ....... 32
FIGURE 6 Schematic Diagram of Sampling Point Locations
No. 2 Hill Baghouse Outlet ................. 33
ซ
FIGURE 7 Schematic Diagram of Sampling Point Locations *
No. 2 Mill Baghouse Horth Inlet ..,,,.,ป... 34
FIGURE 8 Schematic Diagram of Sampling Point Locations
No. 2 Mill Baghouse South Inlet ............ 35
FIGURE 9 Schematic Diagram of Particulate Sampling
Train, No. 2 Mill Baghouse Outlet .......... 37
FIGURE 10 Schematic Diagram of Particulate Sampling
Train3 No. 2 Mill Baghouse North and South
Inlets ...... ........................ . ..... . 38
FIGURE 11 Schematic Diagram of Particle Size Sampling
Train, No. 2 Mill Baghouse ....... . ......... 39
-------
- 11 -
Page
TABLES
TABLE I Summary of Particulate Emissions (English
TABLE
TABLE
TABLE
II
III
IV
Summary of Particulate Emissions (Metric
Units), No. 2 Mill Baghouse
4
8
26
APPENDICES
APPENDIX A Project Participants
APPENDIX B EPA Draft Method 17
APPENDIX C Particulate Field Data Sheets
APPENDIX D Particle Sieing Field Data Sheets
APPENDIX E Visible Emissions Field Data Sheets
APPENDIX F Sanplir- Summary Sheets
APPENDIX G Particulate Weight: Data
APPENDIX H Calibration Data
APPENDIX I Example Calculations
-------
I. INTRODUCTION
The U.S. Environmental Protection Agency (IPA) retained Clay-
ton, Environmental Consultants, Inc. to conduct a series of emis-
sion tests at the International Minerals and Chemicals Corporation
facility located at Spruce Pine, North Carolina, The purpose of
this study was to provide the Environmental Protection Agency with
9
data for the establishment of source performance standards for the
non-metallic mineral-processing industry. This study was commis-
sioned as Project NHM-1 of Task 25; Contract No. 68-02-1408.
The International Minerals and Chemicals Corporation facility
is a feldspar crushing^ grinding, and milling operation. Fugitive
dust generated at each step in the crushing and grinding operation
is collected by reans of a system of dust recovery hoods and routed
through separate exhaust ventilation systems leading to two bagftouses
f
for capture and recovery of feldspar dust.
i
Source sampling was performed on the No. 2 Baghouse at the
final milling plant where feldspar powder is produced by a ba,^.! '*"
*^
mill. Particulate and particle sizing samples were taken at the
baghouse inlet ducts and the outlet stack by personnel from Clay-
ton Environmental Consultants, Inc. U.S. EPA personnel made opacity
readings of the baghouse outlet stack as well as the fugitive dust
generated at several locations within the plant at feldspar crushing
and grinding operations. In addition, EPA personnel observed the
source testing activities and monitored process operations.
This study was conducted during the week of September 26, 1976.
Appendix A lists the project participants.
-------
- 2 -
II. SUMMARY AND DISCUSSION OF RESULTS
Particulate Sampling Results
Tables I and II summarize the results of the particulate
sampling at the baghouse inlet and outlet in English and metric
units, respectively. Both filterable and total particulate emis-
sion rates measured at the outlet averaged 0.16 pound per hour
for the three tests and ranged from 0.14 to 0,18 pound per hour.
The north and south inlet loadings were 140 pounds per hour and
14,6 pounds per hour, respectively, for both filterable and total
particula te .
A comparison of the average total inlet and outlet volumetric
flowrates measured during particulate testing indicates that the
average outlet flovrate is significantly higher,, 3960 dry standard
cubic feet per minute (DSCFM), than the total inlet flowrate of
2930 DSCFM. Since the baghouse was under negative static pressure,
this difference izipi^es the possibility of air leakage into the
baghouse, possibly through the collection hopper beneath the bag-
house. The suspicion of air leakage into the baghouse is further
supported by the initial velocity traverse data which indicated a
total inlet airflow of 3260 DSCFM and an outlet flowrate of 4180
DSCFM.
Visible Emissions Observations
Opacity measurements were taken during the study by two
certified opacity readers provided by che U.S. EPA, Measurements
were taken at several locations at the feldspar mine on September
.27, as shown in Figure 1. Readings were taken at the final milling
r plant at the sites shown in Figure 2 "on September 28 and 29 In con-
Vi-junction with source testing activities.
--^ii ..
-------
TABLE I
SUMMARY OF PARTICULATE EMISSIONS (ENGLISH UNITS)
NO. 2 MILL BAGHOUSE
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
'' ,
f
i>
Ba ghouse
Outlet
', > i
<*
'^r "
t '
i i
Ba ghouse
, North
' Inlet
1 1 '
<
Bflghouse
South
Inlet
Test
No.
1
2
3
1976
Date
9/28
9/28
9/29
AVERAGE
1
2
9/28
9/28
Stack Gas
Conditions
Temp
(ฐF)
105
115
103
108
103
103
Fl owra te
ACFM
5070
4830
4470
4790
1520
2070
DSCFM
4210
3940
3720
3960
1260
1720
Pnrt-iculate Concentration
I'ilLerabif
gr/ACF
0.004
0.004
0.004
0 .004
10.7
0.823
gr/DSCF
0 .005
0 .005
0.004
0 ,005
12 .9
0.989
1 o t a 1
gr/ACT
0.004
0.004
0 .004
0,004
10.7
0.823
gr/DSCF
0.005
0.005
0,004
0 .005
12.9
0 .989
Pa r ticula te
Emission Rate
(Ibs/hr)
Filterable
0.17
0 .18
0.14
0.16
140
14.6
Total
0.17
0.18
0,14
0.14
140
14 .6
I
LO
I
Clayton Environmental Consultants, Inc.
-------
TABLE II
SUMMARY OF PARTICULATE EMISSIONS (METRIC UNI1S)
NO. 2 MILL BAGHOUSE
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
' 1 1* ,
Sampling
Location
'[, '
1 -;
i i
Baghouse
Outlet
r
t >
Baghouse
North
Mnlet
I t
Baghouse
South
Inlet
Test
No.
1
2
3
1976
Date
9/28
9/28
9/29
AVERAGE
1
2
9/28
9/28
Stack Gas
Cond i tions
T omn
41
46
39
42
39
39
Flowra te
Am3
mln
144
137
127
136
43
59
min
119
112
105
112
36
49
ParLiculate Concentration
Filterable
m g / A in
9
10
8
9
24,600
1880
tnn/DSm3
11
12
10
11
29,600
2260
Total
mg /Am
9
10
8
9
24,600
1880
mg/DSm
11
12
10
11
29,600
2260
Pa rticula te
Emission Rate
(kg/hr)
Filterable
0,08
O.OS
0 ,06
0.07
63.3
6.61
Total
0,08
0.08
0 .06
0.07
63 .3
6.61
Clayton Environmental Consultants, Inc.
-------
LOCATION OF VISIBLE EMISSIONS OBSERVERS
FELDSPAR MINE
SEPTEMBER 27, 1976
International Minerals arid Chemicals Corporation
Spruce Pine, North Carolina
TP-2
Se conda ry
Crus neif
Secondary Crus'rer
a .m.
'rirnary Crusher
a .in. .
KEY
~ Observer Location.
- Transfer Point
UGT -- Underground Transfer
r -] -^Conveyor
r(50
TF
TP-5 ,
-*-.
j j-
Clayton Environmental Consultants, Inc
- i >.& 7'a-*'s**ฃn. ***
*v^-^-Ji.'ii.*i";. '" -^ซ"-. ^
-------
ฎ South
Wall
9/29
a .m ซ
< ~v t * i'
ซ (i;.;a Im. '-/
,. <*"$*, . , f
L^ ' .East '*
TP-5
9/28
Ball
Mill
Feed
/
/
u
f
North
ฎ Wall
9/29
P. p.m.
"T
_.._T
TP-3
9/28
Elevator
TP-4
9/28
Ba ghouse
fP-2
9/28
[
Outlet
O Stack
i |TP-1
U/og
1 | "; -ฐ
LOCATIONIiOF VISIBIE EMISSIONS OBSERVERS
*
Loading
9/29
*ซ, FINAL MILLING PLANT
SEPTEMBER '28-29, 1976
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
- Observer Location
TP - Transfer Point
\| - Conveyor
Clayton Environmental Consultants, Inc
-------
- 7 -
Each observer took a reading once every 15 seconds during the
observation period. Readings were summed and averaged for each
six-minute period and plotted versus time. The series of six-
minute averages and the corresponding plots are presented for each
site in Tables III-l through 111-17.
Tables III-l through III-6 represent measurements taken
at various sites within the mining and crushing operation. These
sitesj depicted in Figure 1, included the primary crusher, the
secondary crusher, and conveyor transfer points TP-lj TP-2, and
TP-4.
No visible e-iissions were detected in this area except at
the primary crusher site, and these positive values comprised
only four to six percent of the trea suremen ts taken at the primary
crusher site. As presented in Tables III-l and III-2, these posi-
>
tive measurements contributed to the two positive s ix-minute* avera ge
values that, in both cases, were less than one percent. The max-
imum reading recorded by either observer at this site was five
,s- '
percent. **1
Tables III-7 through 111-17 apply to milling plant operations.
>,'
Opacity readings were taken at the following locations shown in , ''
Figure 2: baghouse outlet stack, roof and four plant vbuilding
walls (fugitive) , feldspar loading silos., and five product trans-
fer points within the milling plant,labeled TP-1 through TP-5.
No visible emissions were observed from the baghouse outlet
stack, the in-plant transfer points, or the plant building walls.
All visible emissions generated at the feldspar loading silos were
of five percent opacity or less. A white-grey fugitive plume of
-------
TABLE III-l
SJM11ARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
late; 9/27/76
'ype o f~ D i s"e h a r g e : Primary C rlis h e r
eight of Point of Discharge- 10-30'
ind Direction' NE
alar of Plume: "No visible plume
'bserver No.. ' 1 _
listance from Observer to Discharge
lirection of Observer from Discharge
leight of Observation Point-
lescription of Background;
IMC Feldspar
Sky ,
Partly Cloudy^
0-10 m i / h r
Type of Plant:
Location of Discharge: PrimaryCrusher
Description of
Uind Velocity,
Detached
Duration
P o in t:
Point;
Plume'
of Observation,
N/A
1 hr
a pprox. LOO
Ground leve1
Quarrywalland equipment structures
SUMMARY Or AVERAGE OPACITY
Set
Nunber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tine
Start
09 30
09:36
09 42
09-48
09- 54
10 00
10 06
10 12
10 18
10 24
End
09, 36
09. 42
09 48
09 54
10 00
10 06
10 12
10:18
10; 24
10. 30
Opฃ city
Sur.
V1
"*>
11
N
^
*
^
!>
Average
N
N
K
N
N
K
K
N
0.2
N
Set
Numb er
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Stare
End
Opac ity
Suin
^
9
Average
'
X
r-
Sketch Showing How Opacity Varied With Time:
Opacity
"if--*
&
. i
r * l
A i
-' 7
"V,~
'T
,- _ "
rt,T^
-;'-: -
-
*,
~ y ''*.ซ'
^
, - '
._.
~
aj._
-
_~"'f
T V ^
.- --
'_
--.*?"
-
"* ' '"' W " ,
l""-"1 ,'
- -"
J .
;;_-'
...
" ^
;- . ,"
^ -^
JlA^*
* .- "XT
:>- .y/i^r-^- ^.j't'-^r..^^! - 1,ซ Time," hours ' '"^ ^ J.^~/l.,'^ ^""l "y^-"*"- ^"~
-------
- y -
TABLE III-2
SU1IMA3.Y 0? VISIELE EMISSIONS
International Minerals
S pruce Pine
and Chemicals Corporation
North Carolina
Date: _
Type of
9/27/76
Primary Crusher
NE
No visible plume
2
IMC Feldspar
Discharge
-[eight of Point of Discharge; 10-30
/ind Direction:
Holor of Plume:
Dbserver No.:
Distance from Observer to Discharge
Direction of Observer from Discharge
{eight of Observation Point: _
Description of Background-
Type of Plant:
Location of Discharge: Prima'ry" Crusher'
Description of Sky: Partly Cloudy
Wind Velocity; 0-7 mi/hr
Detached P1 uir e: M / &
Duration of Observa txon; I Fir, '
Point:
Point:
approx_. 100
100' SSE
Ground level
Equipment strucCure
SUMMAR.Y OF AVERAGE OPACITY
Set
Kuraber
1
2
3
4
5
6
7
S
9
10
Time
Start
09-32
09 38
09 43
09 50
09 56
10- 02
10.08
10 14
10- 20
10. 26
11 i
12
13
14
15
16
17
18
19
20
End
09 37
09 C3
09- 49
09 55
10 01
10- 07
10-. 13
10: 19
10: 25
10, 30
Opa ci ty
S v~i
N
N
N
N
N
V1
\
N
15
N
Avera ge
N
N
N
N
N
N
N
N
0,6
N
Set
F umber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start
End
Opa ci cy
Sum
4
Average
s
f'
*?
.ketch Showing How Opacity Varied Uith Time:
Opacity
(7.) 8
-v . '" |
.,.- t^iiL.,.-* ~-
~.~'
:ป?'*
-
-
--
-"
, - -
-I-*"*-
0 Ji~_ - --,'-, ' '
-_
~_ ' -
1
J
-
4"^'
.^
.
: -
* "?
* ' ' *
'--
-ซ-_ ^_
i-
^
'^
-
-
^
t
-'- -, ~^-
, f'~
'.
'*.
" **- >
. --_-._ 2 - ' -- -
if
-tฃ.
-------
TABLE III-3
0V VISIBLE EMISSIONS
ate :
ype of
International Minerals
Spruce Pine
9/27/76
and Chemicals Corporation
, North Carolina
NW
No visible plume
Discharge. Secondary Crusher
eight of Point of Discharge:10-20'
ind Direction:
olor of Pltme:
bserver No,: __2
istance from Observer to Discharge
irection of Observer from Discharge
eight of Observation Point;
escrxotion of Background,
Type of Plant: IMC Feldspar
Location of Discharge Secondary Crusher
Description of Sky; Partly C1oady-CIoudy
Hind Velocity: 0-7 mi/hr
De tached
Duration
Point;
Point;
Plume; N/_A_
of Observation:
1 hr.
a p pr ox.
a pprox,
75'
TT"
SSB
Ground level
Equipment Structure
SUMMAE.Y OF AVERAGE OPACITY
Set
iuraber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
10 41
10' 47
10 53
11 45
11- 51
11: 57
12 03
12 09
12 15
12 21
12: 27
12 ;33
12; 39
12:45
End
10.46
10 52
10 53
11 50
11- 56
12 - 02
12, 03
12. 14
12" 20
12. 26
12 32
12: 38
12.44
12:50
Opacity
Su-
V
*,-
.ป
-1
\
1
%
v
*-
^
*
s
N
N
N
Av e r a g s
N
K
N
N
N
K
K
N
K
K
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start
End
Opa city
Sxizi
m,
ซ
Average
jf
*
*^*
,.' '
ketch Showing How Opacity Varied With Time;
Opacity
it i
. r
f.
"?
*#*&,ฃ
>. r|
*- jr "-
.- - '
z.
_1-.
,
j j
ป ** v
~_L
- - !
_ J
'A
^,^- -r
.'i
.
w*a *- ~
i
-
*
^ , ป
- i'*~ '"
I
e; i-
p
_
''"_
-v(J_
.
s~
> J'~1
'. ~
1 -
-v u^ -i,_ v,.*t~" - _^ - ^-_^ ^ ^ f_. ?!* Time 5 hours - , -v,f-"";v, . "--. U4 ^-^?-
-------
TABLE III-4
SUHHARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine3 North Carolina
ate: 9/27/76
ypa of Discharge- Convenor Transfer
[eight of Point of DischargeHP
If ^__~__
ind Direction: NE
olor of Plums. No visible plume
)b s erver No . : 1
IMC Feldspar
Type of Plant' _
Location of Discharge- TP-1
Description of Sky Overcast
Wind Velocity; 0-5 miThr"
Detached Plume:N/A
Distance from Observer to Discharge Point:
Direction of Observer from Discharge Point;
leight of Observation Point:
jlescription of Backgroand,^
Duration of Observation: approx. 1-1/4 hrs.
approx ,
50 '
SE
Ground 1 eve 1
Qua rry Wa11
SUMMARY OF AVERAGE OPACITY
Set
Eutnber
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Time
S tart
10:41
10,47
11 45
11- 51
11:57
12; 03
12 09
12 . 15
12, 21
12 27
12-33
12, 39
12-45
End
Opacity
Sun
10.47; N
10 53) N
11 51, *
11- 57
12 03
X
X
1 2 - 0 9 1
12 15
12 21
\
\
.
-------
TABLE III-5
3J?i!lARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
9/27/76
late: _
'yps of Discharge: Conveyor Transfer
[eight of Poxnt of Discharge:
'ind Direction: |
tolor of Plume:
IMC Feldspar
TP-2
40'
NMW
No v 1 3 1 b 1 e p 1 urn e
Ibserver No.: 1 _
listaBce front Observer Co Discharge
Hrection of Observer from Discharge
leigbt of Observation Point'
(escr ip t ion
Type of Plant;
Location of Discharge
Description of Sky: P a r 11 y C1 o od y - Qv e r c"a s t
Wind Velocity; 0-10 mi/hr
Detached
Dura tion
Point; a pprox . 50 '
Point;
N/A
Plume:
of Observa tion:appr ox . 1-1/2 hrs.
of Background:
SE
Ground level
Quarry wa11
S U M M A R Y
0
AVERAGE
0 P A C I T
Sat
Number
1
2
3
t,
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
13. 17
13 23
13. 29
13' 35
13,41
13 47
14-08
14- 14
14, 20
14: 26
14:32
14:38
14:44
14:50
14:56
End
13 23
13 29
13 35
13 41
13 47
13 52
14 14
In 20
14. 25
14: 32
14: 38
14:44
14:50
14:56
15:00
CDacity
Su-
K
*ซ
*;
_\
N
\-
..
V
_i
i
N
N
N
N
Avera ge
N
N
N
N
N
K
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tir>e
Start
End
Op a city
S uo
-
f
Average
if*
rV
Iketch Showing How Opacity Varied Vith Time-
Opacity
* "
, hours
-------
TABLE III-6
SUIKIARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine. North Carolina
9/27/76
>ate:
'ype of Discharge:ConveyorTransfer
leight of Point of Discharge; 1Q '
7ind Direction: N
'olor of Plume. No visible plume
Ibserver No.: 2.
)istance from Observer to Discharge
Jirection of Observer from Discharge
teight of Observation Point-
Description of Background-
IMC Feldspar
Cloudy
0-7 mi/nr
Type of Plant
Location of Discharge: IP-4
Description of Sky;
Wind Velocity:
Detached Plume:
Duration of Observation.- approx. 1 hr
Point: ' "
Point:
N/A
approx. 75
a pprox. 75' SE
Ground level
Cliffor Wall
S U M M A Pv Y OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
,6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tine
S tart
13 18
13 24
13 30
13 36
13,42
13:48
14 11
14- 17
1 4 ; 2 3
1^ 29
14, 35
14.41
14-47
14: 53
14-59
Ooa c i ty
End S u~i
i
13 23
13 29
13- 35
13 41
13-47
13 51
14 16
14; 22
14: 29
14. 34
14 40
14:46
14; 52
14: 58
15; 01
N
V
N
.N
\
il
,.
Oi
N
:s
N
N
K
N
N
N
N
Ave rage
K
K
N
N
N
N
N
N
N
N
K
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start
End
Opa city
Sun
1
Average
-F
(V
t}
ketch Showing HOT? Opacity Varied Uith Time:
Opacity
y 8
6
4 i
^r ~ *
_
~t- t!~
1 1;^-
,
-
- _
-- -
v^-
-
'
-_,
"'=-""
1 - J
,
'-
^-_
0 Jff^- jT'^- j^-w~ J^?7-^ '-rr"5.r_ 1 -^Xmi-- """^C ^-"wvr ->
^ ^J
-
^
V-
"--*
1.
> , .
e
"-*- ?
-"ฃ'- "ir~ ~-*^-,i^fe-^-1^.-?---- '->-
-------
TABLE 1II-7
5J711IARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
ate; 9/28/76
ype of Dis charg e. 0a tie t Stack
eighc of Point of 'Discharge: 100'
ind Direction: NW
olor of Plume; Ho visible plume
bserver No,' I
IMC Feldspar
Type of Plant:
Location of Discharge :NO . 2 Mil1 Baghouse
Description of Sky: Overcast
Uind Velocity:
Detached Plume;
Q-10 mx/hr
"ฅ71
Duration of Observation; 2-1/4 hr s7~
istance from Observer to Discharge Point:
irection of Observer from Discharge Point;
eight of Observation Poir>t
ascription of Background, ^^
a pprox,
appro*. 100'
trees on hillside
S U II M A R Y
0 ?
AVERAGE
OPACITY
Set
lumber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
09:48
09- 54
10, 00
10- 06
10; 12
10: 18
10. 24
10- 30
10 36
10:42
10:48
10: 54
11: 00
11 06
11:12
11, 18
11:24
11:30
11:36
11:42
End
09- 54
10:00
10 06
10 12
10, 18
10. 24
10 30
10 36
10.42
10:48
10, 54
11: 00
11, 06
11: 12
11- 18
11- 24
11:30
11-36
11,42
11-48
Opacity
S J-,
1"
\
,\
\
-;
^
I,
:,
-
_
^
>.
N
N
N
N
M
N
N
N
N
Ave rage
N
N
N
N
N
K
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38 ,
39
40
Ti.-^e
Start
11. 48
11 54
12; 00
End
11: 54
12. 00
12 06
Opacity
Sura
N
N
N
t
Average
N
N
N
,f~
fjs
ketch Showing How Opacity Varied With Time:
Opacity
8
6,
'
s
7
- _
fcai
-""' "if.*-
T- '.
~ T.;_'
. 'V -
*
-T..*.
i 1
~^,
" ,
- ~
,
,:'i:j'
1
^
' I
ป I t I
-
<. .
'-
,
-,
- -
_,
.
--= _
-;-
\ "1 vm - ""* , *J ซ*i ""'**. ซJ^.f,-(. (W- *t
-------
- J_ J -
TABLE III-8
SUUMARY OF VISIBLE EMISSIONS
i
International Minerals and Chemicals Corporation.
Spruce Pine, North Carolina
I
ate:
9/28/76
IMC Feldspar
Outlet Stack
ype of Discharge;
Height- of Point of Discharge,
lind Direction,
lolor of Plume.
Obs erver No, :
100 '
NW
No visible plume
Type of Plant-
Location of Discharge:No. 2 Mill Baghpuse
Description of Sky: Partly cloudy
Wind Velocity, 0-15 roi/hr
Detached Plume- H/A"
Duration of Ob serva tion; approx. 2-1/4 hra
Distance frcnn Observer to Discharge Point;
pirection of Observer from Discharge Point,
Height of Observation Point _ _.-_..
escription. of Background-
approx. 40 'SE~
SE
approx,
f
grassy hil1s ide
SUMMAR1 OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
IS
19
20
Time
Start
14-48
14 54
15 00
15,06
15- 12
15- 18
15:24
15: 30
15-36
15 42
15 48
15 54
16:00
16.06
16: 12
16, 18
16: 24
16- 30
16:36
16:42
End
14: 54
Opa ci ty
S ii-i
N
15,00 K
15 06
15. 12
15- 18
15: 2i
-<.T
_>
N
x-
,,!
>-
15 30 \T
15 36
A^
15-42 N
15:48
15- 5^
16: 00
16- 06
16.12
16: 18
16: 24
16 30
16.36
16:42
16 48
N
^
N
N
N
N
N
N
N
N
N
Average
N
K
3S
K
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Set
Ixuinbe r
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start
16.48
16 54
End
16- 54
17 : 00
Opacity
Sura.
N
N
f
A v e r a g e
N
N
V ^
. If
f
Sketch Showing How Opacity Varied Uith Time:
Opacity
8
1
!'
o
,. i_^-
~ - ^
-
0 ~ " - j -
0
*
- -^
---"
- -
-i^:--
-
-"--
,-
1 _
^ ,
-
^ฐ" Time. 'hours' """~~ , -^^ '_ ^~^-=- ^r'-^-- ^-^-s-/-'
" ,, -. . - J --" ' -^'- -- ' , ,, -ป ^ /"
-------
TABLE III-9
5'J7i:iARY OF VISIBLE EH IS S IONS
ate
ype
International Minerals
Spruce Pine
9/29/76
Outlet Stack
and Chemicals Corporation
, North Carolina
IMC Feldspar
ME
No visible plume
of Discharge,
eight of Point of Discharge; JLOJ)
ind Direction:
olor of Plume:
bserver No,; 2
istance from Observer to Discharge
irection of Observer from Discharge
eight of Observation Poirt
of
Type of Plant:
Location of D is charge'No . 2 Mill Bagh'ous~e
Description of Sky; Cloudy
Uind Veloc ity;
Detached Plune:'
Duration of Observation; 2 hrs 7
P o in t:
Point;"
0-5 mi/hr
N/A
a pprox. 50
same level as discharge
hillside with trees
escnpt ion
Background,
S U M M A R Y
0 F
AVERAGE
OPACITY
Set
lumber
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Tine
S tart
08,35
08 41
08 47
08 53
08: 59
09-05
09. 11
09: 17
09 23
09 29
09- 35
09:41
09.47
09: 53
0 9 ; 5 9
10:05
10; 11
10:17
10: 23
10:29
End
08 40
08- 46
08 52
08; 58
09 CK
09 10
09 16
09 22
09, 28
09- 34
09, 40
09: 46
09, 52
09: 58
10: 04
10 10
10. 16
10, 22
10; 28
10;34
Opacity
Sur
N
K
is
*:
\"
:
.*'
\
N
"\*
*>*
IS
N
N
N
N
N
N
N
N
Average
N
N
N
N
N
N
N
N
N
N
N
M
N
N
N
N
N
N
N
N
Set
t- umber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
33
39
40
Tine
Start
10: 35
End
10: 37
Qua c icy
S um
N
ซ
Average
N
X
*-*r
f.
ketch Showing How Opacity Varied With Time:
Opacity
8
rc
' :
" ' -,""
-
"
j**
- '
-
-. ~
-
A _
.^%
~
- "^
- "< -
""
'
,'
'
_
i _'
' ~, - ' ~ -, .. ~ " Time. hours ... * . .
-------
TABLE 111-10
St^lilARY OF VISIBLE EH IS S IONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
ate:
ype
9/28/76
H/A
If/A"
of Discharge- Feldspar loading
eight of Point of 'Discharge 15 '
ind Direction.
alar of PI urn e '. ^___
>b server No.: 2
istance from Observer to Discharge
irection of Observer from Discharge
eight of Observation Point:
of
IMC Feldspar
Iruck~&Trt. Car
N/A"~
N/A
P lun- e : N/A
Duration of Observation: aj>prox. 3/4n*r~
Point; ^
Point:
Type of Plant:
Location of Discharge'
Description of Sky:
Uind Velocity:
Detached
approx. 25~
Ground level
es crip tion
Background
Building Wall
SUMMARY OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
09- 03
09 09
12 09
12 15
12- 21
12 27
12- 33
End
09 09
09 15
12. 15
12 21
12 27
12: 33
12- 39
Opacity
Sun
K
0
0
5
30
30
10
Avera ge
H
0
0
0.21
1 .25
1 .25
1.67
Set
i-'uoiber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start
End
Opacity
S um
%
f
Average
^ S
iketch Showing How Opacity Varied With Time.
Opacity
8
6
ft
9.
-
'."
^
^-
'
1
-
-
-
-
-
o . , i r . _ '-
-------
TABLE III-11
OF VISIBLE EHISS IOrIS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
9/28/76
Type of Plant;
IMC Feldspar
la ta
'ype of Dischdrge, Indoor Trans fe r Pts , Location of D i s^~h a r g e : T P~-1, T P - 2 , T P - 3
teight of Point of Pischarge:VariableDescription of Sky; N/A
find Direction: ^___ N/A ^^ Uind Velocity;
!olor of Plume: No visible clume Detached Plui?e
)bserver No . :
>is
No visible plume
2
N/A
N/A
Duration of Observation. 3 hrs.
;e from Observer to Discharge Point:
lirsction of Observer fron Discharge Point:
[eight of Observation Point
lescription of Background;
6'-35
N/A
Building walls and equipment structures
SUMMARY OF AVERAGE OPACITY
Set
Suib er
1
2
3
4
-*TK3
6
1
8
9
10
11
12
13
15
^gTP-2
17
18
19
20
Time
S tart
13 45
13 51
13 57
14. 03
14; 09
14; 15
14- 21
14. 27
14; 33
-fl4 39
H-15- 00
15:06
15: 12
'
15- 18
15: 24
15-30
15:36
15:42
15:48
J.5. 54
_
E na
13 51
13: 57
14- 03
14 09
14: 15
14. 21
14- 27
14- 33
14 39
14:45
15- 06
15: 12
15: 18
15: 24
15-30
15: 36
15-42
15-48
15- 54
16: 00
Ops. city
Su-
>.
I*
;i
Ll
y
.-
ป
:ซ
\
\
N
S
N
N
N
N
N
N
N
Average
N
N
K
N
N
N
N
Is
N
N
N
N
N
K
N
K
N
N
N
N
Set
Numb er
21 -
22
23
24
25rp
26_4
27
28
29
30 L
31
32
33
34
35
36
37
38
39
40
Tine
Start
-16. 00
16: 06
16: 12
16 18
16.24
16. 30
16- 36
16. 42
16.48
-16: 54
End
16. 06
16- 12
16. 18
16- 24
16 30
16 36
16- 42
16. 48
16- 54
17. 00
Opacity
S un.
N
N
N
K
N
N
N
N
N
N
9
Average
N
N
N
N
N
N
N
N
N
N
y
t
M.
.ketch Showing How Opacity Varied Uith Time;
Opacity
8
'
, (
-i
-
.:
'-. "" \
r
- - *
__
~,
""
-
-
-
-
f ,
7'
i
.'-
-
f
'"" I1
""
-
",
_
- . -. Time, "hours ' ,
-------
TABLE 111-12
SUMMARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
ate; 9/28/76
ype of Discharge". Conveyor Transfer
eight of Point
ind Direction;
olor of Plume;
bserver lio . .
istance from
irection of
of Discharge:
20'
N/A
No visible plume
D ischarge
Observer to
Observer from Discharge
eight of Observation Poirt'
of
Type of Plant:
Location of Discharge.
Description of Sky;
If ind Velocity :
De tached
Dura tion
Point:
P o in t;
IMC Feldspar
N/A
N/A
Pluire: H/A
of Observation.
351"
2 hrs .
N/A
escription
Background.
Building and equipment structures
S U M M A P. Y OF AVERAGE OPACITY
Set
lumber
I
2
3
4
5_
^CP-5
7
8
9
10
11
12
13
^^XB4
16
17
18
19
20
Tine
S tart
09 30
09. 36
09-42
09 48
09; 54
10-00
10. 06
10- 12
10: 18
4 10: 24
_
"10.51
10:57
11- 03
11: 09
11: 15
11: 21
11: 27
11:33
11:39
11:45
End
09 36
09 42
09 ^8
09 5-r
10 00
10: 06
10: 12
10 IS
10: 2L
10. 30
10:57
11- 03
11:09
11: 15
11- 21
11; 27
11- 33
11:39
11:45
11: 50
Opa city
Su-
N
J,
IS
N
. <
X
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Ave rage
N
N
N
N
K
N
N
N
ft
N
N
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
26
29
30
31
32
33
34
35
36
37
38
39
40
Tine
S tart
End
Opacity
S um
1
Average
*
r
ketch Showing How Opacity Varied Uith Time:
Opacity
(7,) 8
6
j
4',
i
2 -
,c,-ll^^;\.p
~,,:
r -
i
- '
-
-
\
_
-
1
-
) - - - .1..- - ]_ - T-i mo *"' h n nr c "'i "" 2 -1 -* "" ~ """ "**" * ~L w
-------
TABLE 111-13
S'JTHARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
9/29/76
Discharge ;Fugit ive Emissions
ite: _
rpe of __
iight of Point of Discharge, 0-90
Lnd Direction; E
3lor of Plume
jserver No . -.
[.stance from
No visible plume
Observer to Discharge
Lrection of Observer from Discharge Point:
sight of Observation Point-
of Plant:
Location of Discharge;
Description of Sky;
Uind Velocity:
Detached
Duration
Point,
IMC Feldspar
W
Building Wall
Qverca st
0-5 mi/hr
Flure: H/A
of Observation:
1 hr .
a pprox. 7 5
Ground level
iscription of Background. Sky and building exterior^AITT wind ows
* Two windows at ground level. One door at upper level.
and door open
S U M M A R, Y
0 F
AVERAGE
OPACITY
Set
utnber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
08:45
08: 51
08- 57
09-03
09, 09
09: 15
09. 21
09: 27
09:33
09,39
End
OS' 51
08 57
09: 03
09 09
09, 15
09; 21
09 27
09 33
09. 39
09,45
Opacity
SL-
K
N
?<
^
}
-_
X
^,
*
"*.
Average
N
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start
End
Opacity
Sun
Average
./
ฃ-H
cetch Showing How Opacity Varied With Time:
ic)xty 8
4"
. . - .9.
s? r'fฃiป(r'Q
-
-
1
I
j
'
-
- '
1
' -
[} ^ ~~ A f-Swito Urt-i-t-p-c. ^ ~
-------
ill-
SUMMARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
ace; 9/29/76
ypa of Discharge- Fugitive Emis sio n s
eight of Point of 'Discharge:
ind Direction: E-KE
olor of Plume:
bserver No.;
istance from
Ho visible plume
Type of Plant:
Location of Discharge;
Description of Sky:
Uind Velocity ~
Detached Plume;
of Observation;
IMC Feldspar
Duration
E. Building Wan
pvercast
0-5 mi/hr '
N/A ~
1 hr.
Observer to Discharge Point;
irection of Observer from Discharge Point;
eight of Observation Point. ^^_ __
ascription of Background:
* Four windows, three upper, and one ground level-
Two doors at upper level
a pprox. 75'*
Ground level
Sky, trees on hillside
SUMMARY 0? AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tirae
S tar t
09 50
09 56
10, 02
10 08
10. 14
10: 20
10. 26
10: 32
10-38
10.44
End
09- 56
10 02
Opacity
S u~"
N
N
10 03 N
10 14
10 20
10 26
1J
r
N
10 32 i is
10-3S S
10-4-+J S
10. 50
N
Av er a gs
N
N
N
N
N
N
N
N
N
N
Set
I7 u m b e r
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start
End
Opacity
Suni
^
Avera ge
.ป
,f'
?*'
k.
,ketch
Showing
How Opacity Varied With Time
Opacity
( ฐl \
i
, -^ f __ ,_ ^.jj"
,
- ;.
* ' r
r -
_
-
) ir 'l^'i ^"^-' "^^ "*" *'*JJLJ-/-- :" ^r---'-^, *-^-
-
- "
-
.
_,
-^
. v- -
"~T -"Time, "vhours -v- 'r--'
-
*"
-
-
- ^
- "
-------
TABLE 111-15
oV VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North. Carolina
'ate: 9/29/76
'ype 0"f Discharge: fugitive Emissions
eight of Point of "D'I s c h a r g e : "^0-"9" 0 T
'ind Direction; ^ ME
olor of Plume: Ho v 1 s it) 1 e .pi urn e
>b server No-; 1
ixstance frotn Observer to Discharge
Direction of Observer from Discharge
[eight of Observation Point'
escription of Background-
'''Four windows on upper
at ground level.All
Type of Plant; ________
Location of Discharge:
Description of Sky:
Uind Velocity:
De tached
Duration
P o in t:
Point:
IMC Feldspar
S. Building Wall
Overcast
0-5mi/hr
Plume
of Observation:
N/A
1 hr .
approx. 75
approx. 4(P
"Blsyand tree's
level, One window, one large and one small door
windows a ud door s are open .
S U M M A R Y
0 F
AVERAGE
OPACITY
Set
Number
I
2
3
4
5
6
7
8
9
10
Time
S tart
10:55
11 01
1L.07
11- 13
11:19
11: 25
11:31
11-37
11-43
11-49
11 I
12
13
14
15
16
17
18
19
20
End
11,01
11- 07
11- 13
11: 19
11, 25
11-31
11 37
11 i3
11.49
11:55
Ooa city
Sur
Ii
i>
V
:.
V
:,
-i-
*,
"
Average
N
N
K
N
*-
IN
N
N
N
N
N
s.t
Numb sr
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start
End
Opacity
Sun
,,
ซ
Average
,*'
**
iketch Showing How Opacity Varied With Tine:
Opacity
~- 4
1*'* 0
Time "hours
-------
TABLE III-16
SU1LMARY OF VISIBLE EMISSIONS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
of Plant:
IMC Feldspar
ate: 9/29/76 Type ._
ype of Discharge: Fugitive E miss ion s Location of Discharge: N. Building Wall
' ' " of Point of 'Discharge: Q - 9 0v Description of Sky; Overcast
Uind Velocity, 0-10 mi/hr
Detached Plume:N/A
Duration of Observation;1 hr."
eight
ind Direction:
olor of Plume:
b s erver No . :
ME
No visible plume
istance from Qoserver to Discharge Point:
irection of Observer from Discharge Point;
eight of Observation Point,
escription of Background
a pprox 100'
w
a p'prox . 20 '
* Four open windows at upper level
Sky, traces, gray storage silo
SUMMARY 01 AVERAGE OPACITY
Set
^unber
1
2
3
4
S
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tirac
S tart
14: 00
14: 06
14; 12
14, 18
14: 24
14; 30
14, 36
14:42
14:48
14 54
End
Opa ci ty
Sun
14-06 J,
14. 12
14 18
14 24
14 30
14, 36
14- ^2
:!
;:
;\
*"
S
14,^8 ;:
14: 5^
15- 00
:;
N
Average
N
N
N
N
N
N
N
N
N
N
Set
JTunb er
21
22
23
24
25
26
27
28
29
30
31
32
33
3^
35
36
37
38
39
40
Tiwe
Start
End
Opacity
S urn
4
Average
X
*% V-
b '
A
iketch Showing How Opacity Varied With Time;
Opacity
8
6
J
?
ฃr
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r~'
\
^ .-
', --
i
. ~ -
'
...--
_.
, (
-
.-.
< ,,
-
_-
.
^ ':--
, ^
^
"V >"
i
.,-,
- - -
.--'.. - - - " -^ ".Time hours ~- " * ' ซ.<- ,- . . ^-^ -
-------
TABLE 111-17
SUMMARY'OF VISIBLE EMISSIONS
International Minerals
Spruce Pine
and Chemicals Corporation
, North Carolina
ate,
ype. of Discharge:
eight of Point
ind Direction:
olor
9/29/76
Type of Plant-
Location of Discharge:
of Discharge 100-125' Description of Sky;
Uind Velocity:
Detached Plume:
Duration
Point;
Point,
IMC Feldspar
Fug itive Dust
ME
White-grey
of Plume: ^
bserver No. : 2
istance from Observer to Discharge
irection of Observer from Discharge
eight of Observation Point.
ascription of
Entire Roof
Cloudy ~~
^^T^i/hT'~
K/A
of Observation: 58 mlns.'
appro*,300'
of discharge polnt
Background -
Eye-leve1 with a is charge pt
Hi 11sid ew11 h trees
SUMMARY 0? AVERAGE OPACITY
Set
rumber
1
2
3
4
5
6
7
B
9
10
11
12
13
14
15
16
17
18
19
20
Tine
Start
11: 00
11: 06
11 12
11, 18
11- 24
11,30
11: 36
11 42
11:48
11: 54
End
11 05
11 11
11, 17
11, 23
11- 29
11- 35
11 41
11 47
11: 53
11- 57
Opacity
Sv-
23 ^
205
200
2C5
i Q3
i-c
I~0
*. ~ ~
if 2
4- ซ*
Average
9,6
8. 5
8,3
8,5
7.7
7.1
7,1
7,7
6.3
8.1
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
3^-
35
36
37
38
39
40
Time
Start
End
Opacity
Sun
Average
X
g*
ketch Showing How Opacity Varied With Time;
Op=icit>
Time,
-------
- 25 -
from five to 15 percent opacity was observed emanating from the
building roof. The six-minute average opacities for the roof
ranged from 6.3 to 9.6 percent.
Opacity measurements taken for the baghouse outlet stack
were simultaneous with the three3 two-hour particulate tests
taken at the baghouse outlet. The absence of visible emissions
at this site correlates well with the low measured emission
rates.
Particle Size Sarapllrg Results
Tables IV-1 and. IV-2 present the results of the combination
of microsieve analysis and electronic particle counting for the
particle size samples taken at the North and South Baghouse In-
lets, respectively. Figures 3 and 4 present graphical represen-
tations of these zปj distributions. Figure 3 indicates that ap-
proximately 73 percent of the particulate weight was attributable
to particles greater than 10 microns in diameter at the North In-
let, while Figure 4 shows that at the South Inlet, approximately
*7
63 percent of the particles (by weight) was greater than 10
microns in diameter.
-------
PARTICLE
NO. 2 MILL
_ 26 -
TABLE IV-1
SIZE DISTRIBUTION
BAGHOUSE NORTH INLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Characteristic
Diameter
of
Partic les
(mic rons )
>45
30 - 45
20 - 30
10 - 20
8.0-10
6.3-8.0
5.0 - 6.3
4.0 - 5.0
3.2-i.O
2.5-3.2
2.0-2.5
1.6 - 2.0
1.3 - 1.6
1.0-1.3
0.5 -1.0
<0.5
TOTAL
Weight
(gm)
11.400
4.175
3.345
7.834
0.147
0.405
0.710
0.666
0.841
1, 028
0.902
0.621
0.349
0.401
0.396
0. 119
33.339
Size Distribution
by Weight
Percent
34.2
12.5
10.0
23.5
0.4
1.2
2. 1
2.0
2.5
3.1
2.7
1.9
1. 1
1. 2
1.2
0.4
100.0
Cumula tive
Percent
100.0
65.8
53.3
43.3
19.8
19,4
18. 2
16.1
14.1
11.6
8.5
5.8
3.9
2.8
1.6
0.4
Clayton Environmental Consultants, Inc.
-------
- 27 -
TABLE IV-2
PARTICL! SIZE DISTRIBUTION
NO. 2 MILL BAGHOUSE SOUTH INLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Characteristic
Diameter
n f
U J.
Particles
(microns )
>45
30 - L5
20 - 30
10 - 20
5.0 - 10
4.0-5,0
3.2 - i, 0
2.5-3.2
2.0 - 2.5
1.6 - 2.0
1.3-1.5
1.0 - 1.3
0.5 - 1.0
<0.5
TOTAL
Weight
(gm)
0,366
0.271
0. 233
0. 141
0.094
0.006
0.016
0. 030
0.040
0. 044
0.036
0.034
0.073
0.039
1.423
Size Distribution,
by Weight
Percent
25.7
19.1
16.4
9.9
6.6
0.4
1.1
2. 1
2.8
3.1
2.5
2.4
5.1
2.8
100.0
Cumulative
Percent
100.0
74.3
55,2
38.8
28. 9
22,3
21.9
20.8
18,7
15.9
12.8
10.3
7.9
2.8
Clayton Environmental Consultants, Inc.
-------
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1 FIGURE 3
PARTICLE SI2E DISTRIBUTION
NO. 2 MILL BAGHOUSE NORTH INLET
1 In te r national Mineral s and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
| fl
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T
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1
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NJ
co
001 0 05 0102 05 1 i
5 10 20 30 40 LiO 60 /O CO 90 95
Cumulative Percentage Less Than Indicated Diameter
98
99 8 99 9 99 30
-------
'* !
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,
Effective
Particle
Diameter
(microns )
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^-' 7 ' Q
N?'5''ฐ
<$ 4.0
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! F FIGURE 4
I/ PARTICLE SIZE DISTRIBUTION
/f j NO. 2 MILL BAGHOUSE SOUTH INLET
iVt International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
J
: ;. -\
-
I
r
i
1
l
t
"
1
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1
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s_ - ^
20 JO 10 -50 60 70 CO 90 95 93 W 99 G 99 9 99 99
K3
VO
Cumulative Percentage Less Than Indicated Diameter
-------
- 30 -
III. PROCESS DESCRIPTION AND OPERATION
(To be supplied by EPA)
-------
- 31 -
IV. LOCATION OF SAMPLING POINTS
Figure 5 depicts the positions of the ports used to sample
the baghouse vertical outlet stack and the two horizontal inlet
ducts. Each inlet and outlet duct is of cylindrical construction
and thus each was sampled from two ports separated by 90 degrees,
as required by EPA Method 1,
Figure 6 is a diagram of the sampling points used in sampling
the 19-inch diameter vertical baghouse outlet duct. The duct was
divided into equal annular areas and 24 points were sampled.
Figures 7 and 8 depict the sampling points on the north and
south inlets, respectively. Again, each duct was divided into
equal annular areas and a total of 24 points was sampled at each
location.
-------
SCHEMATIC DIAGRAM OF BAGHOUSE INLET AND OUTLET DUCTS
NO. 2 MILL BAGHOUSE
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
i Outlet
?
~l
5'0"
I
rL
Ba ghoas e
North
Inlet
7,0,r
South
Inlet
WEST SIDE VIEW
Outlet
Baghouse
TOP VIEW
North
Inlet
South
Inlet
Clayton Environmental Consultants, Inc.
-------
- 33 -
FIGURE 6
SCHEMATIC DIAGRAM OF SAMPLING POINT LOCATIONS
NO. 2 MILL BAGHOUSE OUTLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Pos ition
1
2
3
4
5
6
7
8
9
10
11
12
Distance
( Inches )
0
1
2
3
.38
.27
.24
i
- 3c
Ir. 15
6
12
U
15
16
17
18
, 73
. 27
.25
.6-
.76
.73
.62
Duct Diameter; 19"
7
7
8
10 i:
9 11
v
ton Environmental Consultants, Inc
-------
_ 34 -
FIGURE 7
SCHEMATIC DIAGRAM OF SAMPLING POINT LOCATIONS
NO, 2 MILL BAGHOUSE NORTH INLET
International Minerals arid Chemicals Corporation
Spruce Pine, North. Carolina
September 27-29, 1976
Pos ition
1
2
3
4
5
6
7
8
9
10
11
12
Distance
(Inches)
0,25
0.80
1,42
2 , I 2
3 ,00
4. 26
7 ,7-
9 . CC
9, S3
10,58
11,20
11.75
Duct Diameter: 12'
Clayton Environmental Consultants, Inc.
-------
- 35 -
FIGURE 8
-' 'SCHEMATIC DIAGRAM OF SAMPLING POINT LOCATIONS
NO. 2 MILL BAGHOUSE SOUTH INLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Position
1
2
3
4
5
6
7
8
9
10
11
12
Distance
(Incites)
0.32
1.00
1 .77
2 .66
3.75
5.32
9. 68
11-23
i "j
13.23
14.00
14.68
Duct Diameter: 15"
Clay ton -Envirortmenta 1 Consultants, Inc.
-------
- 36 -
V. SAMPLING AND ANALYTICAL PROCEDURES
All samples obtained at the baghouse outlet duct followed
the procedures outlined in EPA draft Method 17 (see Appendix B) .
In this instance j a 47-milliineter Gelman filter holder was employed
for in-stack filtration, as shown in Figure 9.
The inlet test procedure was a modification of EPA Method 17.
The in-stack filter holder was replaced by a section of teflon
probe leading from the sampling nozzle out of the stack to a
110-millimeter stainless steel filter holder, as shown in Figure
10. Field data sheets for all particulate sampling are presented
in Appendix C,
Particle size sampling at both inlet ducts employed an alundum
thimble connectec to the nozzle by a 12-inch section of stainless
steel probe followed by a 47-nill iiae ter type SGA filter contained
in a stainless steel Geltnan filter holder. This sampling train Is
shown in Figure 11. Only the contents of the thimble were retained
for laboratory analysis by microsieving at the Clayton Environmental
X
Consultants laboratory. The portion of the microsieve analyre found
to be less than five microns was sent to Battelle Columbus Laboratories
for further particle size determination by electronic particle coun-
ter methods. Field data sheets for all particle size sampling are
presented in Appendix D.
All opacity data were obtained according to EPA Method 9. Field
data sheets for all visible emissions observations are included in
Appendix E.
Appendix F contains the sampling summary sheets. Appendices
G and H present the particulate weight data and the calibration data,
"respectively. ~ "Appendix I presents example calculations.
-------
FIGURE 9
SCHEMATIC DIAGRAM OF PARTICULATE SAMPLING TRAIN
NO. 2 MILL BAGHOUSE OUTLET
International Minerals and Chemicals Corporation
Spruce Pine, North Garplina
September 27-29, 1976
4 7-mm Teflon
"8
f
I
I
4f i _
hertn
ocouple
i ni
Pi tot/
Tube'
Pyrometer Inclined
Manometer
Orifice
Meter
\
\ f
> /
r
<~~-
^ *
\
-i
Ice Bath
100 ml
Water
Dry Silica
Trap ^Gel
V
Valves,
Vacuum
Gauge
Leakless
Pump
Dry Clayton Environmental Consultants, Inc
Gas
Mot r r
-------
FIGURE 10
SCHEMATIC DIAGRAM OF PARTICIPATE SAMPLING TRAIN
NO. 2 MILL BAGHOUSE NORTH AND SOUTH INLETS
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976 ,
HO-mm
Filter
Teflon
Probe
/
.- Pyrometer Inclined
Manometer
Orifice
Meter
%
l~\
"3ST
/
J
"4.X-
&,
--T
', 1
1 v
t
1
-
y
> *
Ice
Ba th
u?
OT
Leaklesa
Pump
Dry Gas
Meter Clayton Environmental Consultants, I
-------
FIGURE 11
SCHEMATIC DIAGRAM OF PARTICLE SIZE SAMPLING TRAIN
NO. 2 MILL BAGHOUSE
i,
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Medium Porosity
Alundum Thimble
Glass-Fiber
Filter
Teflon
Probe
Teflon
Tubinu
,'Vt i
t'i S
i-ei &
ii:fc
i, S * ,
If'^.-1
& * 1 ฃ^
4
>
i '
i
r s
/
/
/
!
Pitot
Tube
lOO'ml
Water
Dry
Trap
1
\
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tl
r
i
1 1
"f ,
*
i 1
if
1
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Umbilical
Cord
Silica
Gel
Thermometers ^.Valves
Orifice
Meter
Pump
ry Ga s
Mete*
Clayton Environmental Consultants, I
-------
APPENDIX 4
PROJECT PARTICIPANTS
Clayton Environmental Consultants, Inc.
Victor W, Hanson
Harold P. Hood
Gerald E. Hawkins
Thomas R. Julien
Richard G. Keller
Helene ML Hysko
Janet L. Vecchio
David L, Holmberg
Mary L. Fegan
James M, McClain
Project Leader
Field Team Sampler, Data Processing
Field Team Sampler
Field Team Sampler
Field Team Sampler
Data Processing
Data Processing
Assistant "Laboratory Director
Laboratory Technician
Chemist
John E. Mutchler, P.E. Contract Manager
U.S. Environmental Protection Agency
Robert Martin Project Officer
Jim Eddinger Process Engineer
John Brown Visible Emissions Observer
Dennis Holzschuh Visible Emissions Observer
International Minerals and Chemicals Corporation
Jeff Van Jtike Environmental Engineer
-------
APPENDIX B
EPA DRAFT METHOD 17
-------
Ht-THOD 17. r'ET?Pt':..;-7IP[! fr P-fPTICLLpTE -,':><
FROIi STATIOTJAVf SOuVCLS (I."-STACiC FILTK^TICi! I.ETKC3)
Introduction
Particulate matter is not an absolute quantity, rather it
is a variable which is a function of tenperature and pressure.
For this reason, participate natter emission regulations and/or
associated test methods must define or take cognizance of the
temperature and pressure at which particulate natter is to be
measured. If temperature is not defined, and if the effect of
temperature upon the quantity of particulate in an effluent gas
is unknovm, then the participate emission regulation may be
variable. The range of pressures yhich exist from source to source
is of negligible importance.
In Method 5, 250ฐF is established as a nominal reference tem-
perature- Thus, where Fethcd 5 is specified in an applicable sub-
part of the standards, particulate natter is defined with respect
to temperature. In order to iraintain this indicated temperature,^?
Method 5 includes a heated alass sample probe and a heated filter
holder. This equipment is cumbersome and reouires care in its
operation. Therefore, vซ'here parti cul ate matter concentrations
(over the norrral range of tenperature associated v/ith a specified
source category) are known to be independent of teipperatura, it is
desirable to eliminate the olass probe and heating systems, and
sample at stack temperature.
-------
This fnECnOG describes an in-stack sarrpling system end samp-
ling procedures for use in such ceses. It 15 -intended to be used
only when specified by an applicable suhpart of the standards,
and only \iithin the applicable temperature limns (if specified),
or when otherwise approved by the Adnimsirator.
t
1. Principle and applicability.
1.1 Principle. Participate natter is withdrawn isolnnetically-
from the source and collected on glass_ fjber.,fliter maintained.at
stack temperature. The particulate mass is determined graviiretri-
cally after removal of unccmbined water.
1,2 />pplicability. This method applies to the d&ternination
of participate emissions froTi stationary sources for determining
compliance with new source performance standards, only v;hsn spe-
cifically provided for in an applicable subpart of the standards.
This method is not applicable to stacks which are saturated with'
v.'ater vapor. In addition, this method_sha11 not. be used as written,
if the projected cross sectional area_pf the orob^ rtension-filter
" ~ ,. ^
holder asseirbly (v.-hsn inserted halfway intc lh^ Swack) covers mdre than
3% of the stack cross-sectional area (see Section 4.1.2).
2. Apparatus.
2.1 Sampling train. A schematic of the sarrpling train used
in this method is shown in Figure 17-1. Construction details for
many, but not all, of the train components are given in APTD-0581;
for changes from the APTD-0531 document and for allowable modifica-
tions to Figure 17-1, consult with the Administrator.
-------
The operating and pM^titenar-e procedures fo>" r?any of the
sarpling train components are described in APTD-0576. Since
correct usaae is important in obtaining valid results, all
users should read the ฃPTQ-0576 docursnt and adopt the opGret-
ing and maintenance procedures outlined in it, unless otherwise
s
specified herein.
2.1.1 Probe nozzleStainless steel (316) with sharp,
tapered leading edge. The angle of taper shall be _ 30ฐ and
the taper shall be on the outside to preserve a constant internal
diameter. The probe nozzle shall be of the button-hook or elbov/
design, unless otherwise approved by the Administrator. The
nozzle shall be constructed from seamless stainless steel tubing.
Other configurations and construction material nay be used subject
to approval from the Administrator.
h.
A range of sizes suitable for isokinetic sampling should be
available, e.g., 0.32 cm (1/8 in.) up to 1.27 cm (1/2 in.) (or
' larger if higher volume sampling trains are used} inside diameter
4
(ID) nozzles in increments of 0.16 cm (1/16 in.}. Each nozzle
shall be calibrated according to the orocedures outlined in the
calibration section.
2.1.2 Filter Holder. The in-stack filter holder shall be
constructed of borosilicate or ouartz glass or stainless steel;
if a gasket is used, it shall be made of silicone rubber, teflon,
or stainless steel, Other holder and gasket materials nay be used
with approval from the /Mministrator. The filter holder shall be
-------
"""' j-M f
(irLlvCP
IMPINCEfl TRAIN OPTIONAL, MAY BE REPLACED
BY AM EQUIVALENT CONDENSER
CHECK
VALVE
VACUUM
LINE
PITOT MANOMETER'
ORIFICE
IMPINGERS ICE OATH
BY-PASS VALVE
THERMOMETERS
VACUUM
GAUGE
MAIN VALVE
DRYGASMETCn
Ain-TlGHT
PUMP
. ParticulatG-sampIing train.,
>
-------
designed to provide ฃ positive seal against IcaLaga from the out-
side or around the filter.
2.1,3 Probe Extension--ฃny suitable ricnd probe extension
may be used after the filter holder. Flexible tubing rray also
be used between the probe extension and the condenser.
x
2.1.4 Pi tot tubeType S, or other device approved by the
Administrator, attached to probe extension to alloy/ constant
monitoring of the stack gas velocity. The face openings of the
pitot tube and the probe nozzle shall be adjacent and parallel
to each other, not necessarily in the sarr.s plane, during ssrrpling,
The free space betveen the nozzle and pitot tube {see Figure 17-1}
shall be at least 1.9 cm (0.75 in.). The free space shall be set
based on a 1,3 cm (0,5 in.) ID nozzle. If the sampling train is
designed for sampling at higher flov rates than that described in
APTD-0581, thus necessitating the use of larger sized nozzles, the
largest sized nozzle shall be used to set the free space. In addi-
tion, to minimize aerodynamic interactions betvreen the pitot tubgy
and filter holder, there shall be a distance of at least 3 inches
between the center line of the pitot tube impact openings and the
leading edge of the filter holder (see Figure 17-1).
The pitot tuba must meet the criteria specified in Method 2,
and be calibrated separately (i.e., apart fron its asserrbly con-
figuration) according to the procedures outlined in that method
for the calibration of isolated Type S pitot tubes.
-------
E.I.5 Differential pressure qauce--Incliped nano.-ster
capable of Pleasuring velicity head to within 10% of the rruniPUin
measured value or ฑ 0.013 rrn (0-COQ5 in.)> whichever is greater,
Below a differential pressure of 1.3 ran (0.05 in.) water gauge,
j
nicromanpmeters with sensitivities of 0,013 ir."i (0.0005 in.)
JP
should be used, Hovrever, nricroin&noreters are not easily adaptable
to field conditions and are not easy to use with pulsating flow.
Thus, methods or other devices acceptable to the Administrator may
be used when conditions warrant.
2.1.6 CondenserAny system that cools the sample gas stream
(e.g., impingers connected in series, as in flethod 5) and allows
measurement of both the v/ater condensed and the moisture leaving
the condenser, each to v.'ithin 1 ml or 1 g. The moisture leaving the
condenser can be measured either by: (1) monitoring the tenperature
and pressure at the exit of the condenser and using Dalton's law; or
(2) passing the sample gas stream through a silica gel trap with
exit gases kept below 20ฐ C (68ฐ F) and determining the weight gain.
If means other than silica gel are used to determine the amount
of moisture leaving the condenser, it is recontended that silica gel
still be used between the condenser system and pump to prevent
moisture condensation in the pump and metering devices.
2.1,7 f'etering system--Vacuum qauge, leak-free pump, therrporpeters
capable of measuring temperature to within 3ฐ C (5.4ฐ F), dry gas r.eter
v/ith 2% accuracy, and related equipment, or equivalent, as required to
-------
paintein an isckinetic srrplira retc r.s', to d=taimpc sarple vclure.
Sanpling trains utilizinq peteiing systems desiqrod for hicjher flow
rates than that described in APTD-0501 or APTD-0576 pay be used
rovided that the specifications in section 2 of this rrsthod are
met. When the metering system is used in conjunction with a pitot
tube, the system shall enable checks of'isokinetic rates.
2 1.8 Baro-raterfercury, aneroid, or other barometers capa-
ble of measuring atmospheric pressure to v/ithin Z.S p.m Hg (0,1 in.
Hq) In wany cases, the barometric reading Kay be obtained from a
nearby v:eather bureau station, in which case the station value
(which is the absolute baroiretric pressure) shall be requested and
an adjustnent for elevation differences between the weather station
and sampling point shall be applied at a rate of minus 2.5 rm Hq
(0 1 in- Hg) per 30 m (100 "ft) elevation increase or vice versa- for
elevation decrease.
21,9 Gas density determination equipmentTemperature and
pressure gauges and gas analyzer as described in Tethods 2 and*&
2.1.10 Temperature end pressure gauqes--If Dal ton's lau is
used, to monitor tenperature and pressure at co-/-nser outlet. The
temperature gauge shall have an accuracy of 1ฐ C {2ฐ F). The
pressure gauge shall be capable of measuring pressure to vnthin
2,5 mm Hg (0.1 in* Hg). If silica qel is used in the condenser
system the tenperature and pressure nust be measured before the
silica gel component.
-------
2.2 Samnle recovery.
2,2.1 Probe nozzle brushKyi on bristles '-nth stainless steel
wire handle. The brush shall be prcoerly sized and shaped to brush
out the probe nozzle.
2.2.2 Glass wash bottlesTwo.
2.2.3 Glass sample storage containers-Chemically resistant,
borosilicate glass bottles, for acetone washes, 500 ml or 1,000 ml.
Screw cap closures shall be teflon rubber-backed liners or of such
Construction so as to be leak free and prevent chanical attack
from the acetone. (Marrow mouth glass bottles have been found to
be less prone to leakage.) Other types of containers nust be ap-
proved by the Administrator.
2,2.4 Petri dishesFor filter samples; glass or polyethylene,
unless otherwise specified by the Administrator.
2.2.5 Graduated cylinder and/or balanceTo measure condensed
>,
water to v/iihin 1 ml or 1 g. Graduated cylinders shall have sub-
divisions no greater than 2 nl. Post laboratory balances are capa-
ble of weighing to the nearest 0.5 g or less. Any of these balances
9>.
are suitable for use here and in section 2.3.4.
2.2.6 Plastic storage containersAir tight containers to
store silica gel.
2.2.7 Funnel and rubber policeiran--To aid in transfer of
silica gel to container; not necessary if silica gel is weighed in
the field.
2.3 Analysis.
-------
2.3.1 Glass ueiqhinci dishes.
2.3.2 Desiccator.
2,.3.3 Analytical balance--To neasure to within 0.1 r.ig.
2.3,4 BalanceTo neasure to within 0,5 g.
2.3,5 Beakers250 ml.
rs
2.3,6 HygrometerTo measure the relative humidity of the
laboratory environment,
2.3.7 Temperature gaugeTo neasure the temperature of the
laboratory environment.
3. Reagents
3.1 Sampling.
3.1.1 FiltersThe in-stack filters shall be glass rrats or
thimble fiber filters, vnthout organic binders, and shall exhibit
at least 99,95% efficiency (< D.05% penetration) on 0.3 micron
A
dioctyl phthalate smoke particles. The filter efficiency tests
shall be conducted in accordance vn'th ASTfl standard rvethod D 2926-71.
Test data from the supplier's Quality control prog ran is sufficient ,
4ฎ
"for i.} is purpose.
3.1.2 Silica gelIndicating type, 6-16 pesh. If previously
used, dry at 175ฐ C (350ฐ F) for 2 hours. New silica gel nay be
used as received,
3.1.3 Crushed ice.
3.1.4 Stopcock creaseAcetone insoluble, heat stable silicone
grease. This is not necessary if screw-on connectors with teflon
sleeves, or similar, are used.
-------
3,Z Sjrple recovery.
3.2.1 /1,cetcine--[7eegcnt grace, 5 0,001** residue, in glass
bottles. Acetone fron rretal containers generally has a high residue
i
blank and should not be used, Sonatinas, suppliers transfer acetone
to glass bottles from metal containers. Thus, acetone blanks shall
>
be run prior to field use and only acetone v/ith low blank values
(< 0,001%) shall be used,
3.3 Analysis.
3.3.1 AcetoneSaife as 3.2.1.
3.3.2 DesiccantAnhydrous calcium sulfate, indicating type.
4. Procedure
4.1 Sampling. The sampling shall be conducted by conpetent
personnel experienced with this test procedure,
4.1.1 Pretest preparation. All the components shall be main-
tained and calibrated according to tna procedure described in
APTD-Q57G, unless otherwise specified herein.
Weigh approximately 200-300 g of silica gel in air tiaJrc con-
-------
labol the slurping containers (glass or plastic potri dishes)
and l,o^p the filters in those contsinars at all tipcs except
during sampling and veicjhing.
Desiccate the filters ai 20 + 5.6ฐ C (68 ฑ 10ฐ F) and ambient
^
pressure for'at least 2^ hours and veiqh at 6 or more hour inter-
vals to a constant i,eight, i.e., 5 0,5 ng change from previous
weighing, and record results to the nearest 0.1 jug. During each
v/eighing the filter must not be exposed to the laboratory atrnos-
phere for a period greater than 2 minutes and a relative humidity
above 50%.
4.1,2 Preliminary deteminations. Select the sampling site
and the minimum number of sanpling points according to Hethod 1 or
as specified by the Administrator. Male a projected area model of
the probe extension-filler holder assembly, with the pi tot tube
impact openings positioned along the centerline of the stack, as"
shovn in Figure 17-2. If the estimated cross-section blockage,
calculated as shovn in Figure 17-2, exceeds 3 percent of the duct
,j
cross sectional area, then either one of the following shall be **"
done: (1) a suitable out-stack filtration method can be used
instead of in-stack filtration; or (2) a special in-stack assembly,
*designed to minimize blockage effects, can be used. For details
concerning the latter aporoach, consult uith the Administrator.
Determine the stack pressure, temperature, and the range of
velocity heads using Tethod 2', determine the moisture content using
Approximation I'ethod 4 or its alternatives for the purpose of making
-------
G.U
X /CC5
ป > or
*.ป ^^ ? e.f ~. ft- ~
or a.
.^- c^-^C
-------
iso!inetic stapling rate calculations. Estir'^tas ray be usrd.
However, final results nil be based on actual ncosurersnts radc
during the test.
Select a nozzle size based on tha range of velocity heads such
that it is not necessary to change the nozzle size in order to main-
tain isoKinetic sampling rates. During th'e run, do not change the
nozzle size. Ensure that the differential pressure gauge is capable
of measuring the minimum velocity head value to in thin 10^, or as
specified by the Administrator.
Select a probe extension length such that all traverse points
can be sanpled. Consider sampling from opposite sides for large
stacks to reduce the length of probas.
Select a total sampling tirre greater than or equal to the
m'ninurn total sampling tin>e specified in the test procedures for
the specific industry such that the sampling time per point is not
less than 2 min, (or some greater time interval if specified by the
Administrator) and the sariple volume taken will exceed the required
4ฃ
minimum total gas sample volume specified in the test procedures for
the specific industry. The latter is based on an approximate average
sampling rate. Note also that the minirum total sample volume is
corrected to standard conditions.
It is recoirnended that half-integral or integral numbers of
minutes be sampled at each point in order to avoid timekeepinq errors.
In some circumstances, e.g., batch cycles, it may be necessary
to sample for shorter times at the traverse points and to obtain
-------
smaller gas sample voltes. In tbosa cases, the Administrator's
approval must first be obtained,
4.1.3 Preparation of collection train. During preparation and
assembly of the sampling train, keep all openings where contanina-
tion can occur covered until just prior to assembly or until sampling
f
is about to begin.
If impingers are used to condense stack gas moisture, prepare
them as follov/s; place 100 ml of v:ater in each of the first two
impingers; leave the third iropinger erpty; and transfer approximately
200-300 g or more, if necessary, of prei.eighed silica gel from its
container to the fourth irpinger; alternatively, if a balance is
available in the field, the silica gel can bs weighed out in a tared
inpinger, and its weight gain deterninec! in the field. Place the
silica gel container in a clean place for later use in the sample
recovery. If soma weans other than ir.ping&rs is used to condense'
moisture, prepare the condenser (and, if appropriate, silica gel for
condenser outlet) for use.
rf*' '''
Using a tweezer or clean disposable surgical gloves, place ar1-
labeled (identified) and weighed filter in the filter holder. Be
sure that the filter is properly centered and the gasket properly
placed so as not to allow the sample gas stream to circumvent the
filter. Check filter for tears after assembly is conpleted. Mark
the probe extension with heat resistant tape or by some other method
to denote the proper distance into the stack or duct for each sampling
point.
-------
Unices otnr.-.-ire specifi_d b_> the Ad.i'.i'islrator, attach a
ler pei ฃ tur e sense1-' tc ihe prcLc z:- tension so ihcit the sensor
extends Ley one! tho leading ec'nc oT the prche extension and doss
not touch any metal, The sensor should be positioned at least
1.9 cm (0,75 in.) frou both the pi tot tube and probe nozzle to
j
avoid interference with the gas flow {see 'Figure 17-1).
Assemble ths train as in Figure "17-1, using (if applicable)
a very light coat of silicons grease on all ground glass joints and
greasing only the ou^er portion (see A?TD-C5?G) to avoid possibility
of contamination by the silicons grease. Place crushed ice around
the impingers (if applicable),
4,1,4 Leaf; check procedureAfter the sampling train has been
asserbledj a leak check of the filter holder shall be conducted as
follows: Plug the inlet to the probe nozzle with a material that
will be able to withstand the stack tenpsrature; alternatively, the
probe nozzle can be removed and ths inlet to the filter holder
plugged. Insert the holder into the stack and vait approximately
5 minutes (or longer, if necessary) to allow the systen to coine tfo-
equilibrium v/ith the temperature of the stack gas stream. Turn on
the pump and drau 2 vacuum of et least 380 ran Hg (15 in, Hg). De-
termine the leakage rate, if any, A leakage rate in excess of 4^
of the average sampling rate or 0,00057 m /min, (0.02 cfn), which-
ever is less, is unacceptable.
The follo'./ing leak check instructions for the sampling train
described in APTD-0576 and APTD-0531 may be helpful. Start the pump
-------
with by-pass valve fully op^n and coarse adjust valve completely
closed. Partially open the coarse adjust valve- and slowly close
the by~p?ss valve until 380 im Hg (15 In. Hg) vacuu-> is reached.
Do not reverse direction of by-pass valve- If 380 nn Hg (15 in,
Hg) is exceeded, either leak check,at this higher vacuum or end
the leak check as sho./n below and start over.
1,'hen the leak check is completed, first slowly remove the plug
from the inlet to the probe nozzle and immediately turn off the
vacuum pi/np. This prevents the water in the condenser from being
forced backward and keeps silica gel from being entrained backward.
Leak checks shall be conducted as described whenever the train
is disengaged, e.g., for silica gel or filter changes during the
test, prior to each test run, and at the completion of each test
run. If leaks are found to be in excess of the acceptable rate, the
test v/ill be considered invalid. To reduce lost tirra due to leakage
occurrences, it is reconmended that leak checks bs conducted between
port changes at the highest vacuum reading drawn during that sampling
at
traverse.
4,1.5 Particulate train operationDuring the sanpling run,
maintain the isokinetic sarpling rate to v/ithin 10ป (unless otherwise
specified by the Administrator) of true isokinetic.
For each run, record the data required on the example data
sheet shown in Figure 17-3. Ba sure to record the initial dry gas
meter reading. Record the dry gas meter readings at the beginning
and end of each sanpling time increnent, vhen changes in flow rates
-------
LOCATION.
OPERATOR.
\DATt
RUN NO
SAKV'LE DOXNO,.
PITOT TUBE COEFFICIENT, Cp,
SCHEMATIC OF STACK CHOSS SECTION
DAOOiVIETniC PRESSURE,
ASSUMED MOISTURE. %_
NOZZLE IDENTIFICATION NO
AVCHAGC CALIGHATED NOZZLE
LEAK RATE, m3/imn{cfm)_
', HATCIV1AL-L.
. cซ
-------
are rude, and when sampling is halted. Take other data point
readings at least once at each sanple point during each time
incrcrent and additional readings \'hen significant changes (207*
variation in velocity head readings) necessitate additional
adjustments in flov; rate. Level and zero the rianorreter.
Clean the portholes prior to the test run to minimize the
chance of sampling the deposited material. To begin sampling,
remove the nozzle cap and verify that the pi tot tube and probe
extension are properly positioned. Position the nozzle at the
first traverse point with the tip pointing directly into the gas
stream. Immediately start the purp and adjust the flew to isokinetic
conditions. Nomographs, which aid in the rapid adjustment of the
isokinetic sampling rate without excessive computations, are availa-
ble for use i.'henever the Type S pi tot tube coefficient is C.85 ฑ 0.02,
and the stack gas equivalent density (polecular v;eight) is 29 ฑ 4.
- APTD-0576 details the procedure for using these nomographs. If C
and Mj are outside the above stated ranges, do not Ge the nomograph r.
unless appropriate steps (see Reference 7.7] are taken to compensate
for the deviations.
V'hen the stack is under significant negative pressure (height
of impinger stem), take care to close the coarse adjust valve before
inserting the probe into the stack. If necessary, the pump may ba
turned on with the coarse adjust valve closed.
llhen the probe is in position, block off the openings around the
probe and porthole to prevent unrepresentative dilution of the gas
stream.
-------
Traverse the SLC-.C|. cress scci,ior,. as reoir'red by S'cthod 1 or
as specified by the AJmnistputor, being cateful not to btrtp the
probe nozzle into the stack v.'alls \ hen s?rpling near the vails or
when removing or inserting the probe extension through the port-
holes, to ninimze chance of extracting deposited natcrial,
*
During the test run, take appropriate steps (e.g., adding crushs
ice to the inpinger ice bath) to maintain a temperature of less than
20ฐ C (68ฐ F) at the condenser outlet; this will prevent excessive
moisture losses. Also, periodically check the level and zero of the
manometer.
If the pressure drop across the filter becomes too high, rraking
isokinetic sampling difficult to maintain, the filter may be replaced
In the midst of a sample run. It is recoTrnonded that another com-
plete filter holder-nozzle assembly be used rather than attempting
to change the filter itself. After the new filter holder-nozzle
assembly is installed, conduct a leak check. The particulate weight
shall include the summation of all filter asser.bly catches.
iff
A single train shall be used for the entire sample run, except
for filter and silica gel changes. However, if approved by the
Administrator, two or pore trains nay be used for a single test run
when there are ti;o or pore ducts or sampling ports. The results shal
be the total of all sampling train catches.
At the end of the sample run, turn off the pump, remove the
probe extension-filter holder-nozzle assembly frorc the stack, and
record the final dry gas meter reading. Perfom a leak check at a
-------
"- equal to or greater t^en the nrxirur reached during s:rp-
ling. Calculate percent isckmetic (sc2 calculation section) to
determine vhether another test run should be rade. If there is
difficulty in n.eintaining isokinetic rates due to source conditions,
consult v/ith the Administrator for possible variance on the iso-
r
kinetic rates,
4.2 Sample recovery. Proper cleanup procedure begins as
soon as the probe extension-filter holder-nozzle assembly is
removed from the stack at the end of the sampling period. Allow
the assembly to cool,
Uhen the assembly can be safely handled, v/ipe off all external
participate matter near the tip of the probe nozzle and place a
cap over it to prevent losing or gaininq participate natter. Do
not cap off ths probs tip tightly v/nile the sairpling train is
cooling dov/n as this would create a vacuum in the filler holder, and
force condenser water backward.
Before moving the sample train to the cleanup site, disconnect
*r
tha filter holder-proba nozzle assembly from the probe extension;
cap the open inlet of the probe extension. Be careful not to lose
any condensate, if present, Remove the umbilical cord from the
condanser outlet and cap the outlet. If a flexible line is used
between the first impinger or condenser and the probe extension,
disconnect the line at the probe extension and let any condensed
water or liquid drain into the impingers or condenser. After
vnping off the silicons grease (if applicable) cap off the condenser
-------
inlet. Ocuncl class storr>c>*s, plestic cc"^,, cr sunn caps (v;icf-
ever are appropriate) may h? iiscd to close tr^se cpsninqs,
Transfer both the filler holder-p;obe nozzle ?rd condenser
assemblies to the cleanup area. This area should be clean and
protected frcpi the wind so that the chances of coritar'matina or
losing the sample t'ill be nininized.
Save a portion of the acetone used for cleanup as a blank.
Place about 200 ml of this acetone taken directly fro^ the v.-ash
bottle being used in a glass sanple container labeled "acetone blank."
Inspect the train prior to and during disassembly and note any
abnorrral conditions. Treat the samples as follows:
Cpntain_s_r__Kg_.. 1. Carefully remove the filter from the filter
holder and place in its identified petri dish container. Use a pair
of tv/eezers and/or clean disposable surgical gloves to handle the
filter. If it is necessary to fold the filter, do so such that the
participate cake is inside the fold, Cuantitatively remove any
participate matter and/or filter which adheres to the filter holder ''
gasket by carefully using a dry nylon bristle brush and/or a sharp-
edged blade and place into this container. Seal the container.
Container T'c. 2. Takina care to see that dust on the outside
of the probe nozzle or other exterior surfaces does not get into the
sanple, quantitatively recover ^articulate ratter or any cor.densate
fron the probe nozzle, fitting, and front half of the filter holder
by washing these components v/ith acetone and placing the wash into
a olass container in the follo'.nna manner; note that distilled water
ray be used instead of acetone wlipn approved by the ^dmnistrator
-------
or shall be used wj.en specified ty th" /cnmstrator, in these
cases, sa^e a water blank end follow Wnmstrator's circctiors
on analysis;
Carefully rercve the probe nozile ard clean the inside surface
by rinsing wfth acetone frcm a \,ash bottle and brushing with a nylon
f
bristle brush. Brush until acetone rinse sho-vs no visible particles,
after which make a final rinse of the insic'e surface v/ith acetone.
Brush and rinse with acetone the inside parts of the fitting
in a similar way until no visible particles renain. A funnel rcay
be used TO aid in transferring liauid washes to the container. Rinse
the brush with acetone and quantitatively collect these washings in
the sample container. Between sampling runs5 keep brushes clean
and protected from contamination.
After ensuring that all joints are wiped clean of silicons
grease (if app"Yice.ble), clean the inside of the front half of the
filter holder by rubbing the surfaces with a nylon bristle brush
and rinsing v/ith acetone. Pinse each surface three times or more ''
if needed to remove visible particulate. Fake a final rinse of the
brush and filter holder. After all acetone washings and particulate
matter are collected in the sarrple container, tighten the lid on
the sarrple container so that acetone will not leak out when it is
shipped to the laboratory, f'ark the height of the fluid level to
determine whether or not leakage occurred during transport, Label
container to clearly identify its contents.
Container F-'o. 3, Note color of indicating silica gel to deter-
nine if it has been completely spent and make a notation of its
-------
condition. Transfer trip silica ccl bac'-', to its crunr,-cl centalTT
and seal. / funnel r^ rake it rosier to POL"" the silica eel
without spilling, end a rubber policerran pay be used as an aid
in removing the silica qel. It is not necessary to remove the
small amount, of dust particles th~t may adhere to the walls ?nd
are difficult to remove. Since the gain in weight is to be used
for moisture calculations, do no:, use any \ictcr or other liquids
to transfer the silica gel. If a balance is available in the field,
follow the procedure under "Analysis."
Condenser water. Treat the condenser or inpinger water as
follows: make a notation of any color or ft In in tha liquid catch.
Measure the condensate to i.ithin t 1 ml by usina a graduated cylinder
or, if available, to within + 0,5 p by using a balance. Record the
conde^sete volume or weight. This information is required to cal-
culate the moisture content of the effluent gas. Discard the
liquid after rressuring and recording the volurs or weight,
4.3 Analysis. Record the daza required on the exarrple sheet
shown in Figure 17-4, Handle each sanple container as follows- -^
Container Kp. 1. Leave in shipping container or transfer the
filter and any loose particulate from the sarple container to a
tared glass weighing dish and desiccate for 24 hours in a desiccator
containing anhydrous calcium sulfate, Ueigh to a constant waight
and report the results to the nearest 0.1 rg. For purposes of this
section 4.3, the term "constant weight" means a difference of no
more than 0.5 pq or "IE of total veight less tare weight, whichever
is greater, between two consecutive weighings, with no less than 6
-------
Run f.'o
RD|Jlr,2 Uu 'ilJitV.
Amount ti7-.iu lc>t ilunrjj transport
Aeatone hb..k volume, ml
Acetone ir-'jiii volume, ml
Acetons bbnl, conceiitraticn, no/nig (equation 5-^)
Acctcnc ivzsh hl^nJ;, mg (cLju'dimn 5-5)
CONTAINER
N'JiY.BcR
1
2.
TOTAL
WEIGHT OF PARTICULATE COLLECTED,
mg
FIWAL \, EIGHT
^H^xdl
TARS V.'cIGHT
^I^xCC
Less acetone blank
Weight or p^rticu'aie matter
WEIGHT GAIN
1
FIWAL
INITIAL
LIQUID COLLECTED
TOTAL VOLUME COLLECTED
VOLUP'E OP LIQUID
WATER COLLECTED
<^' ' i- ,
i.'. ";;:c:fl
VO.U', ฃ.
ml
SILICA GEL
\iEIGHT.
g
g- ml
CONVERT ViEIGHT OF WATER TO VOLUVE BY DIVIDING TOTAL './EIGHT
INCREASE BY DENSITY1 OF WATER tig/ml),
INCREASฃ-9 - VOLU.VE WATER! mi
1 g/ml
/7-V-
Figure C^-r. Analytical dala.
-------
hours of desiccation lire LIT, con veighinrs tin;! no rorc then 2
rnrutes exposure to tre laboratory atrospherc (rust be less than
50% relative humdity) durirq \eichino.
Cent c^irer To, 2, note level of liquid In container and
confirm on analysis sheet whether or not leal age occurred during
transport. Measure the liquid in this container either volume-
trically to ฑ 1 ml or gravinetrically to ฑ 0,5 g, Transfer the
contents to a tared 250 ml beaker, and evaporate to dryness at airbient
temperature and pressure, Desiccate for 24 hours and veiah to a
constant weight. Report the results to the nearest 0,1 mo.
Container f'o. 3. Weigh the spent si lice ael to the nearest
0.5 g using a balance. This step IT ay be conducted in the field.
"Acetone Flank" fejvtainer. f'easurc acetone in this container
either volurnetrically or gravinetrically. Transfer the acetone to
a tared 250 nl beaker end evaporate to dryness at ambient temperature
and pressure. Desiccate for 24 hours and v/eiah to a constant weight.
.Report the results to tha nearest C.I ng.
<*" '
5. Calibration
flaintain a laboratory log of all calibrations.
5.1 Probe nozzle. Usinq a micrometer, measure the inside
diameter of the nozzle to the nearest 0.025 nm (0.001 in.), flake
3 separate measurements using different diameters each tire and
obtain the average of the neasurenents. The difference between the
high and low numbers shall not exceed 0,1 rrn (0,004 in.).
Uhen nozzles become nicked, dented, or corroded, thsy shall
be reshaped, sharpened, and recalibrated before use.
-------
Cach nozzle 11 fill tc pcrroi -'>tly ere! t.-npualy u'e-.tific-d.
5.2 Pi tot tube, "He pitox. tubs sK=.ll fce calibrated scpcrctcly
(i.e., apart from its assently configursficr) according to the pro-
cedures outlined in I'ethod 2 for calibration of isolated Type S pitot
tubes.
*
5,3 Dry gas meter end orifice reter. Both reters shall be
calibrated according to the procedure outlined in PPTD-C576, I/hen
a diaphragr, pmrp is used, assure that there is no leak.
5.4 Temperature cauqes. Calibrate dial and liouid filled tulb
thermonetsrs and thernocouple-rotentioneter systens aaainst mercury-
in-glass therir.orreters. Ice btth and boiling v-'ater (corrected for
barometric pressure) are acceptable reference points. For other
devices, check witn the /"'dn.imstrator.
6, Calculations
^
Carry out calculations, retaining at least one extra decimal
figure beyond that of the acquired date. Round off figures after
final calculation.
6.1 Nomenclature
2 2
t A = Cross sectional area of nozzle, m (ft )
n
B = Hater vapor in the aas stream, proportion by volurre
C = Acetone blank residue concentration, mg/q
a
c = Concentration of particulate natter in stack oas, dry basis,
corrected to standard conditions, q/dscm (p/dscf)
-------
v = Staci o?s velocv.y, calc^l->teu ty f'jt'roJ 2," Eouation 2-7
usino data obtsir^d frcn I'cti'cd 17, rr/src (ft/sec)
I,1 = l.'eipht of resides in acetone i ash, nq
3
&H - Average pressure chffc-rential across the criflcs rreter
(see Figure 17-3), rn H2C (in, H20)
p = Density of acetcne, rg/nl (see label on bottle)
'w
= Density of vater, 1 a/ml (0,00220 Ib/nl)
0 = Total sampling tire, nrin.
"13.6 = Specific gravity of mercury
60 = sec/min
100 = Conversion to percent
6.2 Average dry aas meter terrperature and average orifice
pressure drop. See data sheet (Figure 17-3),
6.3 Dry gas volume. Correct the sairole volure reasured by the
dry pas neter to standard conditions (20ฐ C, 760 nr. Ha or ฃ8ฐ F,"
29.92 in. Hg) by using Equation 17-1.
Xstd)
= V
m
std
= K V.
bar
Equation 17-1
where:
K
0.3855 ฐK/tnm Hg for metric units
17.65 ฐR/in. Hg for English units
-------
I = Percent of isc! v,:Uc
m = Total s'-'Q'jnt of pฃ.rriculcte ratter collected, rrg.
t-i = I'oleculsr veight of water, 18 q/q-trale (1G Ib/lb-trole)
m = Pass of residue of acetone efter evaporation, rg
s
P. '" = Barometric pressure et the serrplina site, rm Hg (in. Ha)
' "
p = Absolute stock ge.s pressure, mn Hq (in. Hq)
P td = Standard absolute pressure, 7CO rm Ha (29,92 in. Hg)
R = Ideal qas constant, O.C6236 irrn Hg-m3/ฐK-9-[r,ole (2KC3 in.
Hg-ft3/0P-lb-nole)
T = Absolute average dry oas treter trrrperature (see Fipure 17-3
T = Absolute average stack pas temperature (see Figure 77-3),
ฐK CฐR).
T td = Standard absolute temperature, 293ฐ K (528ฐ R)
V = Volune of acetone blank, ml
3
Va,, = Volume of acetone used in v/ash, nl
ow
V-, = Total volurre of liquid collected in condenser and ,
*,
silica gel (see Figure 17-4), nil,
V = Volume of aas sarple as nsasured by dry aas mater,
dcm (dcf)
V / t ,v = Volume of pas sarrple reasured by the dry qas meter
corrected to standard conditions, dscm (dscf).
V / t .> = Volune of \:ater vapor in the gas sample corrected to
standard conditions, sen (scf).
-------
Yolurc of \ atcr varn ,
fr(std) * Vlc flfi'1^4 = Kl'lc Cation 17-2
where
X
K = 0,00134 m3/nl for retric units
= 0.0472 ft3/ml for Fnqlish units
6,5 f'oisture content,
B ซ "l5|dL_ซ Equation 17-3
1/5 Vm(std) + V(std)
6.6 Acetone blank concentration,
3
Equation 17-4
6,7 Acetone v/ash blank.
Ha - Ca Vaii Pa Equation 17-5
3 3 <3V/ a
S.8 Total particulate veight. Determine the total participate
catch from the sum of the weights obtained from containers 1 and 2
less the acetone blank (see Figure 17-4),
6.S Particulate concentration.
c$ = (0.001 g/rncj} (mn/Vn(stdp Equation 17-6
-------
6,10 Conversion
From
scf
g/ft3
g/ft3
g/ft3
To
n3
gr/ft3
Ib/ft3
g/m3
fuU
0.
15.
2.
35.
.inV' bv
0283
4
205 x 10"3
31'
6.11 Isokinetic variation,
6.11.1 Calcul aliens from rev; data.
100 Ts [KV1c + (Vn/Tn)
=
Equation 17-7
vjhere:
K * 0.003^6 irn Hp-n3/rnl-ฐK for irstric units
= 0.00267 in. Hq-ft3/r,l-ฐP for English units
6.11.2 Calculations frcn internechate values.
P...J 100
Tstd vs 8 An Ps 60
Equation 17_8
v/here :
K = 4.323 for metric units
= 0.0944 for English units
-------
APPENDIX G
PARTICULATE SAMPLING FIELD DATA SHEETS
-------
PROJECT 'I
GEORGE D- CLAYTON & ASSOCIATES
EXHAUST GAS VELOCITY AND FLOW RATE
/ / j'f // -c " , CREW /"//'/
Sampling Station.
L. <- ~~ D ate
lime / C
Test No, P/cV^--> rr //'.
"" ~ '
Sampl ing
Paint
/. /^
(,- / f.
,/
JC
7
S
7
c-
^
^
3
^
I
Veloc i ty
Pressure
(In.H20)
ฃ-#r"
C*fr
& - ?ft
C-&/
0- ^
{<* >v
c:>
e (
o, /?
L''- ^"^
C - */ *-
C*9st
DB
Temp
(F)
C1 '
/'*>
*;
^*
f^
iT'"^ s
* *
<*<>'
C/ c
"?<>
c,
<->
c/^
Pitot Tub
Uncorrect ed
Vel ocity
(Ft/sec)
// c; f
4&5 ''
ฃ2'V
\
<^2 . S
^0, i
tfV.S -
*/6<3
ฃ/ ^ j
^j
(/
"7
c-
s
6
-*)
x-'-ป
/
/3*-)-J-x " ^'
Velocity
Pressur e
&*
***
9<
9>
9>
y
. ,/cx-v - 7
Uncorrected'
Velocity
(Ft/sec) ,1
i>2 9.
-- - ^
**~j C*^ ป^\
'o- >
^6 *2
. +*
'*$ '>
^^.S
^ ^
"5 ^
:^'^.2
^!j,%
if!tLf
r
Stack Wet Bulb Temperature, (ฐF)
A. Barometric Pressure, (In.Hg)
Stack Dimensions
Static Pressure of Stack Gases,
Pitot Tube Correction Factor
/.
Specific Gravity of Stack Gases Relative to Dry Air
Absolute Pressure of Stack Gases = A + (B/13.6), (In.Hg) ฃ3*0
Average Uncorrected Velocity, ( f t / a e c ) ^ , ^ฃ a r 60 * F, (ft/min)
.Corrected Velocity = F * C.
^
H
-I
Area of Stack, (ft2)
Gas Flow Rate
G * H, (ACFM)
;J,".'Average Stack Temperature, (T)
_- : '*^' -S"i _ , 4;'r &^' - "-<-_- - > - ' - -- - .-^7 '-/ -
i"K .!ฃr;Standard
-------
PROJECT
GEORGE D- CLAYTON & ASSOCIATES
EXHAUST GAS VELOCITY AND FLOW RATE
CREW /- &P
Sampling Station
Test No S,;<, VJi
Date
Time /,
Pitot Tube No. /
Manometer No.
Samp ling
Point
U' lฃ
//
/&
9
S1
/7
/
c
^
&
/
5
f>
1
Velocity
Pressure
(In.H20)
C.'S?
I)- I f/
o* & c
6.&?
C~ (r 7
0-L ^
C^ C C
$- *J.2
C- ซ?
f.(<
t - */3~
/-> , f
6 .. $ /
DB
Temp
(ฐF)
%
?Lr
?L
%
(/(
K
C?C-
CK
${-
ฃiC-
-------
PROJECT
GEORGE D- CLAYTON & ASSOCIATES
EXHAUST GAS VELOCITY AND FLOW RATE
I f CREW ฃ"-' A-
Sampling Station
Test No, Tf-^+'it
/" J* /^ d
_ --
Dat&
Time
,,
Pitot Tube No . 2 J
Manometer No.
Samp ling
Point
_ฃ '
Z.
3
N
T
ฃ.
7
y
-7
i 0
/ f
/ ฃ
Veloc i ty
Pres sure
(In.H20)
V tO
j-r
i Iff
,*o
i
,2*
,ro
. 21
,iฃ
i7
, ?>
^l-
. 20
- S"2/,:
, i i
, 1 ") I Z i
DB
Temp
CF)
t>"
E b
i )'
S i"
_ ^s"
c<-
_S bT
x ^
it"
f >'
,o-^ x>
^ / <- /
.- j "' -
^5 -
o r >
^l/ --"
-Dt :/
n. ซ. '
Sampl ing
Point
^ S ป
z
3
, ji^r
DB
Temp
(ฐF)
S^-""
?i-
3J~
fi~
?r
*y
^r
3J>
S b~
5 ^
^^'
sr
Uncorrected
Velocity
(Ft/sec) J
\
-^ ^
3a.5
H ^}
^ 1
-57 'i
^7 0
-/ I
Jt 5
^f
- ^r.3
^/ 5-
^ i
s
.V*
J*
Stack Wet Bulb Temperature, (ฐF)
A. Barometric Pressure, (In.Hg)
B -
Stack Dimensions
'
Static Pressure of Stack Gases, (In . H20)
Pitot Tube Correction Factor ฃ/ 3 >
~ ^ . 3
D
E
Specific Gravity of Stack Gases Relative to Dry Air /
Absolute Pressure of Stack Gases = A + (B/ 13 . 6^ (In. Hg) 3-? . a ^
Average Uncorrected Velocity, (ft/sec)^^ , y^^gr 60 * F>(ft/min)
.G 'Corrected Velocity = F * C
H- Area of Stack, (ft2) C.
(ft/min)
._, VI. ( Actual Gas Flow Rate * G * H, (ACFM)
"^ J , -* Aver age Stack Temperature, (ฐF)
-------
GEORGE D- CLAYTON & ASSOCIATES
EXHAUST GAS VELOCITY AND FLOW RATE
PROJECT
Satnpling Station
Test No. ?-,.,**
CREW /j k i^ / "7~J
_^y
I/ <."7 /7ฃ
Date
TimeJ/Vr -- /-Z.JO
.
Pitot Tube No, ;
Nanometer No.
Samp 1 ing
Point
13 ,
Z
3
V
r
4
7
S
=1
fy
l<
'ฃ
Velocity
Pr es sure
(In-H20)
4 ov
i J^
ซซฃ>
i ?C
, y~
, sr
. 33
. ?v
V Jlf
7, 1 ..
v2ซ=i.
. tr
-/ . eo//i
, 1 31
, ^ 7 V M
DB
Temp
(ฐF)
^V
vr
'* s~
^ \"
5^
C <
? r
sr
V "."
4 r
is
V V
< >
-> 'n'
7i-
Uncorrect ed
Velocity
(Ft/sec)
^/"/ 1 /
4- /
^j? '>
>fr <
Hf i
4r !
^ (,
^/r
y/ r
27, 'i
3t '^
31 'i
3V 6 f
9
Sampl ing
Point
S i
2
3
V
5
i'
v>"
?r
&r
T-V"
? r
5r
Uncorrect ed'
Velocity
(Ft/sec) ป
3^^
^S
^7 f
ซ& r
^3^
^/,S
^ '-y-
^ic i
^/ 7
4; 'j
^^
5S?
ฃ< *
*;
Stack Wet Bulb Temperature, ("F)
A. Barometric Pressure, (In,Hg)
B. Static Pressure of Stack Gases, (In,H20)
Pitot Tube Correction Factor ^f "2,
Stack Dimensions /
C.
D.
E.
F.
^
Specific Gravity of Stack Gases Relative to Dry Air /
Absolute Pressure of Stack Gases = A + (B/13. 61/., (In , Hg) ^
Average Uncorrected Velocity, (ft/see) t^rffi^ffi0^ 60 * F,(ft
. Q
Corrected Velocity =
Area of Stack, (ft2)
F * C
(ft/mitt).
f 2 Z7
H.
:i/\ Actual Gas Flow Rate = G * H, (ACFM)
J.i-Average Stack Temperature, (ฐF)
GDC-2
-------
SAMPLING TRAIN DATA
Source Designation;
Ceflt Number;
Field Person:
Filter Heater Setting:
Probe Heater $ettingr_
Nozzle Number;
A
Filter Nuiaber:_
Barometric Pressure ("Hg):_
Stack Static pressure ("I^C
Stack Dimensions: J^ '
Plume Appearance; ~~
6 7 -
. 27.3,3
-/ 6
\mbient Temperature(ฐP):
Record all Data Every
ฃ/*SQ T*/Ts x
Minutes
-(in.):ฃ
Pitot Tube No.A? ,Corr,Factor:
Meter Box No ./&^*v?> Corr. Fae
Meter Isokinetic Factor; /
Assumed Moisture (X) : /. y
Condensate Volume(ml):
Silica Gel Weight Gain(g);
Leak Rate &.0I CFM at
a*
V??# **/06 W/w
Trav-
erse
Point
No.
Tine
Samp-
ling
(rain)
Clock
Velocity
?r es sure
<"H20)
Stack
Temp
Dry Gas Meter
Vo lume
(ft3)
Teup (DP)
Inlet Outle c
Orifi.ce
Pressure
Differ-
ential
Filter
Box
Temp
Last
Imp
Gas
lemp Pre
CF
Sampling
Train
Static
ssure
("Hg)
o
BO
s
toy
ฃ77
A?
16
0
iZi.
/n
9$
7$
3% ??
//y
10Z
S-/3
/QUO
/3.I
103
3. 92.
3,3
/Qtt?
lo
*'3< 0
V ff
|7งrvf
$.ฅ
IOS
"tL
*/#
So
/a/
113
90
0,33
/.ft,
92.
2.0
0,30
2*1
10 -f
!.V
-- aW/0#fJ#i*LX00S -~~.r~. , _--_>.
I^/^PปMJ ' Clayton Environmental Consultants, Inc.
-------
ฃff>
SAMPLING TRAIN DATA
& M ฃL
Source Designation:
)ate: _ ฃ_
Teat Number; j/
Field Person:
filter Number:
Barometric Pressure
7-
("Hg):
Stack Static Pressure ("H^O)? /.
Stack Dimensions;
plume Appearancer
Vmbient Temperature("F):
Record all Data Every
Minutes
Filter Heater Setting: --^
probe Heater Setting;
Nozzle Number: ,Dia.(in.);
Pitot Tube No. /0,Corr.Factor:
Meter Box No^fxte-.!, Corr.Factor:
Meter Isokinetic Factor: ^
Assumed Moia ture (7.) :
Condensate Volume(ml):
Silica Gel Weight Gain(g):
Leak Rate &\QQ^ CFM at
J'2- Z
Hg
Tr av-
er se
Point
No.
Time
Samp-
ling
(rain)
Clock
Veloci ty
pr es sure
("H20)
Stack
Temp
Dry Gas Meter
Volume
(ft3)
Temp (ฐF)
InletOutle t
Orifice
Pressure
Differ-
ential
("H20)
Filter
Box
Temp
Last
Imp
Gas
lemp
Sampling
Train
Static
Pre ssur e
("Hg)
to
13
3.o
0.50
/at
//s
72
10
3**-
97.39
$
105
. 03.
130
3-2-
^'57
133.
\o<
133.
3,
I3Z
76
1*3,19
131
n
it*
131
/to
I30M
? X
;<
Id**"-
y
ซ"y
/
_ *
^
Clayton Environmental Consultant3,L Inc.
-------
SAMPLING TRAIN DATA
Compnny:
Source Designation:
Date :
frff t/_S &
Teet Number;
Field Person-
Filter Heater Setting:__
probe Heater Setting;
Nozzle Number;
~> ,2 6 7 - 3 3
Filter Number:_
Barometric pressure ("Hg) :
Stack Static pressure ("H?0) ; ~/,
Stack Dimensions: /? " 3Z Q
Plume Appearance: ~~
Ambient Temperature(ฐF);
Record ail Data Every jZ"
Minutes
,Dia. (In.) -j0. ?
Pitot Tube No, /ฃ>,Corr.Factor;
Meter Box No .^ฃ^2, Corr. Factor:
Meter Isokinetic Factor; /"?/O
Assumed Moisture (7.) ; ^/ g g,
Condensate Volume(ml):
Silica Gel Weight Gain(g):
Leak Rate (0- OJ CFM at /x*'
"Hg
Trav-
erse
Point
No.
Time
Samp-
ling
(rain)
Clock
Velocity
Pressure
C"H20)
Stack
Temp
CF)
Dry Gas Meter
Volume
(ft3)
Temp(ฐF)
Inlet Outlet
Orifice
Pressure
Differ-
ential
Filter
Box
Temp
Last
Imp
Gas
rempjPre
CF)
Sampling
Train
Static
ssure
0,55
/O
/J/.65?
3.2
H
MIL
70
10
10
0.53*
ฃ3
jit
3'**
O.S&
It*
131
133
13?
30
135
35
H*
3-0
767-77
131*
\.7l
0>3/
135
It*
13V
1-29
Q.lb
H*
, - ^ - ,
i^sB -VE B- ACE^CTOT A i) ^S
Clayton environmental Consultants t~
-------
SAMPLING TRAIN DATA
Company ;
Source Designation;
Test Number;
Field Peraon
- ,3 & 7 -ป
Filter Number ; ,*
Barometric pressure ("Hg) :
Stack Static pressure ("H?0> : ^- /j
Stack Dimensions i _ /
Plume Appearance: _
hmbient Temperature ("F );
Record all Data Every
Filter Heater Setting?
Probe Heater Setting:
Nozzle Number; )V , Dla , (In. ) ; _ct
Pltot Tube No. /&>CorrซFactor:O
Meter Box K o . jฃAteL~Ji9 Corr.Facto n(.
Meter Isokinetlc Factor; /
Assumed Holsfcure(%); /,
Condensate Votutae (ml) ;
Silica Gel Weight Gain(g);
Minutes Leak Rate
CFM at
"Hg
Trav-
erse
point
No.
Tine
Samp-
ling
(mln)
Clock
Velocity
Pres sure
C"H20)
Stack
Temp
Dry Gas Meter
Volume
(ft3)
Temp (BF)
In let Outlet
Orifice
Pressure
Differ-
ential
("H20)
ilter
Box
Temp
(F)
iLast
Imp,
Gas
remp[pre
(F)
Sampling
Train
Static
ssure
("Kg)
s//
3JJ.
10
13$
76
3.*
10
0. ฅ3
1 90. 23
.99
1
3,
/It. 1
13*
13*
90
ytf
&S3
It
13*
/oo
3,6
0.37
II <
3.
tie
131
3,0
It*
1,5?
3-2.
tea
/off-
\.*l 0-5"
RACE -(TOTAL)
(i 5 5
lov-tj* "-/^ ; ? - *-_-- - -- ^*-. . . .v
'-"^Clayton Environmental Consultants, Inc.
-------
SAMPLING TRAIN DATA
Company :
Source Designation:
P-3
Test Number:
Field Person:
Filter Number; ^><.~ s-_ - ' f /
Barometric Pressure ("Kg);
Stack Static Pressure ("H2
Stack Dimensions ; /*7 v
Plume Appearance: "
Vrabienfc Temperature("F):
Record all Data Every
/*
Minutes
Filter Heater Setting;
Probe Henter Setting:
Nozzle Mumber:
, Dla. (in. ) ; &.
Pltot Tube No. /_O_ , Corrป Factor ;
-------
SAMPLING TRAIN DATA
Conpany -
Designat I
Date:
Teat Number:
Field person;
Filter Number:
Barometric pressure ("Hg):
Stack Static Pressure
Stack Dimensions:
Plume Appearance;
Filter Heater Setting:
Probe Heater Setting:^
Nozzle Number:
* /
Ambient Temperature(ฐF) :
Record all Data Every
Minutes
Pitot Tube No.^/^?,Corr. Factor :_ฃ
Meter Box No ./g>ปg-%?, Corr.Fac ton\_ฑ
Meter Isokinetic Factor; / 7/0
Assumed Moisture(%); /r g'g.
Condensate Volume (ml): A?
Silica Gel Weight Gain(g); /ff
Leak Rate Q,0f CFH at f f "Hg
10
Trav-
erse
Point
Mo.
Time
Samp-
ling
rain
Clock
Velocity
pr essure
("H20)
Stack
Temp
Dry Gas Meter
Vo lutne
Temp (ฐF)
Inlet Outle t
Orifice
ressure
Differ-
ential
("H-70)
Filter
Box
Temp
Las t
Imp,
Gas
Tempfpre
CF)
Sampling
Train
Static
ssure
("H
9/37
S&o
037
/Co
07 130
too
1*3
1.91
z-y
too
I**
)DO
67
1*5
68
10
/?:
/>-/*
ut*
3.0
y
/(/O
17
/*
fa**
to*
b?
Ho
10: 27
0,2$
/of
3/9. V7
10
/<*
/M
V*
Bi&VK
r
\Gb-~~
J_S -v t ,
)
-
io'4
.
Clayton Environmental Consultants, Inc,
-------
SAMPLING TRAIN DATA
lompony ;
lource Deaignation:
eet Number;
Person:
Filter Heater Setting;
probe Heater Settlng:_
Nozzle Number:
,Dla. (In. ) ;
filter Number; s (* 4 - I
laroractric Pressure ("Hg) ; Z.-?. Z.*j"
Itack Static Pressure ("H^O) : - 3
Stack Dimensions:
?lume Appearance:
i ^
ro
unbient Temperature (ฐ F) :
lecord all Data Every
Minutes
Pltot Tube No. !-?_, Corr. Factor ;
Meter Box No.g/k-z, > Corr .Factor; -;
Meter Isokinetic Factor: H 9j
Assumed Mola ture (7.) : /. ^~
Condensate Volume (ml);
Silica Gel Weight Gain(g
Leak Rate ( oo 9 CFM at
Trav-
erse
Point
No.
$ 3
J
3
^
S"
^
7
*f ?
^
/^
^
f^
'*
Time
Saap-
llng
(TOin)
C7
^f
( c
i b"
t J
ri~
lo
sr
^o
vr
s^
?ซ L
fC J-7
To^T
- r"-^
^ ~- "x
Velocity
pr es sure
<"H20)
-1*?
, ^
.N ^
.?A
,~^?
, 3 l
^ L
.U
. il
.32
.3i~
,^
,37
i" ; -^t*.
y^>^.^^-^' vVs -I-:
23^ER?CieS(TdTAL>3t&
Stack
Temp
CF)
'3
. 05
103
103
to ^
(a 7
ป33
<^3
ro?
o-s
f^ 3
^
*
,-"
~i ,
"f-^fet^-
Dry Gas Meter
Vo lume
(ft^)
r9^ o?
^,^
-ft^.^
-^^73
^i o.V
"1/^1 . Z-
^o..-
?;ซ. it*
^?v v
^zy
^35, /
^3?.iv?
- "
" ' c ^'
1,- , J>,
' -" >ซ-' r"
(-aปJ.ป-^T^rซ ซA
.Jjr^Tt^'' ' J '
Temp (ฐF>
Inlet
^0
) IV
nft
M S-
1 iฐ1
/ J.O
1 10
en
1 Zo
IT- Z.
112
11?
VI *
r
- ,v
r* Jป
,'' ~f"
**iwr
V .*Jt'
Outle t
i
>.
-, ~
_-^^ซ.^ฃki,
~t^.__^-i-vp
Filter
Box
Temp
(ฐF)
-
- v v
ฃ&;&
- -7S-*J6
Last
Imp.
Gas
Temp
(ฐF)
fe.
^LJ
15"
^^
bซ/
C9
vo
7Ji
7i^
4?
tป1
6^5
-i-
s-,. p
Sampling
Train
Static
Pressure
("Hg)
<*<
^ l
i.zr
u s-
>*^>'
i.r
^'
^. 0
t, r
e.^
2,^
ซป,
-------
SAMPLING TRAIN DATA
Company (-. ,3 /\
Source Designation:
Date ^ I i
/~
e. J~-Ur
Teat Number; r* ~ i
Field Person: /?
Wf ~ 2. C. 7 - -7 /
Filter Number:
Barometric Pressure ("Kg):
Stack Static Pressure ("H2
Stack Dimensions:
plume Appearance:
Ambient Temperature(" F) :
Record aLl Data Every
Filter Heater Setting:
probe Heater Setting:
Nozzle Number: ,Pia.(in.):.2$
Picot Tube No. ,Corr.Factor :
Meter Box No, , Corr. Factor;
Meter Isokinetic Factor:
Assumed Mois Cure (7.) :
Condensate Volume (ml) : ffl-tL^
Silica Gel Weight Gain(g): 70^(T
Minutes Leak Rate
CFM at
Trav-
erse
Point
No.
,3 ซ
to
I 0
1
y
1
C
r
<,
?
2
3
-
Time
Samp-
ling
(rain)
LO
45-
7.0
T
30
S|-
Dry Gas Meter
Vo lume
-6 1
its.t
?&fo v
-K'^.z-
1-7, .-ป
rnVrr
e^.ll^
r^,-.V
ff; ^' ;
t?^"j"j'
C^tw
Temp (ฐF)
Inlet
(Z*
i ? ?
/??
it^l
1^
/ Jo
'^
^30
, 30
J 30
13*
)30
j
,^^
" ' in
ฃi
Outle t
//=%
/ ^
, ,^
i ' V
1 i i~
i f (,
! '1
I * 7
// -7
Z 0
f 7C3
(TJ
-
lf-2^
,<"-^
gQ
Orifice
Pres sure
Differ-
ential
<"H70)
' -Jf
', L
; j-
i. V
2 i
f, I
,T7
.V4
,*ฃ
,TT
/VI
, 1 ->
-
/. 3^i ^
/fXv^
Filter
Box
Temp
"i* i- *~
^c
Last
Imp .
Gas
Temp
CF)
<-
T T
-If
7C
-7U
lc
T?S,
A
1 V
3 O
S-;
^1
Vl
w
&
Sampling
Train
Static
Pressure
("Hg)
3to
c, ^
*,*-
-7
5,
C
'' s-.a-
r,r
G
C
c
C
-
4.v\
** v Jf - *"
^j "^ ^v i *
Clayton Environmental Coha'ultanCs,'' Inc.
-------
SAMPLING TRAIN DATA
Company: _i~f^A y 2. C
Source Deal gnat ion:
)ate: ?.<>;-;_
L'^c
/-r
Teat Number:
leld Person:
'liter Number; S( A - ~2-
Jaromctrlc Pressure ("Hg) ;
stack Static Pressure ("Hg
Stack Dimensions: _ t ~z *7
Plume Appearance:
Filter Heater Setting:
Probe Heater Setting:
Kozzle Number: ,Dia.(in.);
Pitot Tube No. , T, , Corr. Factor ;
Meter Box No. ;7-k -^Corr. Fae ton
iimbient Temper ature (ฐF) :
Record all Data Every
/ O T
Meter Isokinetic Factorr_
Assumed Moisture (7.) : 1,<
Condensate Volume(ml): f
Silica Gel Weight Gain(g)
3 y
Minutes Leak Rate
CFM at
TifWfcn
15* "itg
Trav-
erse
Point
No.
5 /ป
/ i
/"?
'1
S
7
t
s'
t/
3
t
2.
-
-!= .^
Tiiae
Samp-
ling
(rain)
0
o
p J
i S
7^
Z-j"
1J
^ t*
VJ
</'"
r^>
b'S'
C-'j
_J'-4l *
-__O
Clock
''J Si"
-
iw * ^
Velocity
pressure
("H20)
,a^
r'Z1')
,i-V
n
, ? r
, 1 9
./S
- */7
ซ/7
-/?
^rJ
t^ f
^-
.- - , *._
T *' - ^ j"- ~ "X ' i" v* SL - "' _ "
v r~?" ' , - 1*~ * T-,t % . .. ซ? - ' > ป >? "^
-TJJ-A lK)j'Jllfr-L-^"' ^jtj*-f"C3*^*~V'-T' ifc "' H -Jj-- i ^ -fi---^l_- M
ig^^VERAGE?-(TOTAL) V^Iu.
Stack
Temp
(ฐF)
|c*
/o ^
1 l-1-
1 a ^
/L-1 V
(OS
A^
/i)ft
10 0
v&
\v*ฎ
loo
-^^f-t, ~
' t-^ *-
^
^^.^^fihfc^-
,i^lv-aJฃ.;
- -^3t
Dry Gas Meter
Vo lutae
(ft3)
(^7 lyt
1 >- 1 > y
->st
^ c , *
M-' ? s-
c? o j s-
^^6, 4"'
ditb
o/ 4.?
0/3. f
021 I
0 il, ซv
0^1 ,9^7
. ^..
'"' "t '' ' ซ"
^"rC -^ C
f^^-^tH-^
\ iSS-^^ija'J.". /
Temp (ฐF)
Inlet
r /Z.
1 1 -i
t^
n<\
j ?/
" ^
/^5L.
ity
111
ft^
MT
Jl V
r-
X f
^si:
>5u_x
On tie t
/ฐ0
M J>
;/z
I/-/
/ 1 '^
1! V
fu
iiฃ
/^
/2 +
rzr
i?>~
i* T -^
W-f
j* -r
?,0
tl
? . s
?. /
^ /
/^9
/ff
Al
(S^ < ฃ^-J
z,j
-
T J ill.^
-^.^^""^C^
' '^ " r '* -r
Filter
Box
Temp
TF)
" -
r
-,r--'--
^ * -" - ,
r ^-L ;^ ^
'l^wSf1
a Si.
Last
Imp.
Gas
Temp
(BF)
^ro
Pr
$0
Ho
$6
-i o
S&'
fa
fo
rd
S-o
^0
-
-.
- ^- ,-T,
* "5 '
*.T^r^
- '^
Sampling
Train
Static
Pressure
("Hg)
\
1
t
z.
'
f ^1T Jlv*. n j- i_ .,
TSJ-jUSsitS^^i.
."2 f *AU.- =-i
Clayton Environmental Consultants, Inc.
-------
SAMPLING TRAIN DATA
Z
JT
Company ; ฃ
Source Designation:
JatS: 9 /7 J / 7 i,
yn ซ IN """pii-Ji i in mm
Test Number; P - ^
field Person; /g*/y/C
Filter Number;
aarometric Pressure ("Hg):
Stack Static Pressure ("l^O):
Stack Dimens ions:
Plume Appearance;
Ambient Temperature(8F):
Record all Data Every __
'^ L.T
Filter Heater Setting;
probe Heater Setting: _
Nozzle Number; ,Dia.(in.):
Pitot Tube No. ,Corr.Factor:
Meter Box No. , Corr. Factor:
Meter Isokinetic Factor;
Assumed Moisture(Z);
Condensate Volume (ml); /(% _
Silica Gel Weight Gain(g);
Minutes Leak Rate
CFM at
"HB
Trav-
erse
Point
No.
5 ป
I,
t '7
0,
y
T
6
f
^
S
Z
^
*
-'-'^.-r".
Time
Samp-
ling
(rain)
<= 0
t S~
7 0
"7f
5^
f <"
"t ^
i r~
/O 0
1 0 <,'
)t ?
i< r
< 2o>
-TV- **"*"
"f", "
Clock
/GOT
/ics-
_
-^i ^ ^
Velocity
Pr es sure
("H20)
, 75L
30
^7
.1*1
, 13
J *
. 1 ^
, < (,
r /I
ปtt
,?C
,^0
.,.^\-l
- J~ ^_~S_ _ 'i "1,1 ,'" ' " "
S^|ftRA%ff(T]SYL)%Tt-
Stack
Temp
<ฐF>
; O O
/ ซ0
/oc2 . 3
0?i 7
^/ ri
ฃ y L
-- x . *r
T7 4
76.1
fi.S-
0*8^, %ol
ifli.a-.^ v
/:,Cv"/vi ซ
--:^v^^
(70031)
Temp ("F)
Inlet
/30
/2T>
I3C
<3i
il?
/5s-
1 X
/K
fIC
/3 L
/ J-C
16
i*
^^\
(sS
Qutle t
> ?\
i t ^~
1 ? y
I 7"^
1 7 S"
l&$~
t ?v-
vZc
1 1\-
11 S
t 0"
f ^(,"
^
T^
^'sji..^.
Orifice
Pressure
Differ-
ential
C'HjO)
*'/
J 3
"J 0
Z T
<:. /
?. /
l,v
1, 5r
I ซV
2, ^
? J
2 ฃ
2^'
,
-------
APPENDIX
PARTICLE SIZE SAMPLING FIELD DATA SHEETS
-------
SAMPLING TRAIN DATA
7 A
orap any r (
ource Designation; ฃ MC.
ater /^T/7'_ __
eat Number;
'ield Person: ,?/,/<.
Filter Heater Setting:
Probe Heater Setting;
Nozzle Number:
, Dla. (in, ) ;, 2.yo
liter Number: s /-A i b 7 > /
1 .
aroractric Pressure ("Hg) : 27
tack Stattc Pressure ("H-gO) " - 1 u
tack Dtmenslons ; _ '$" TQ _
'lume Appearance?
mbtent Temperature(ฐF);
Lecord all Data Every
/er
Minutes
Pitot Tube No. 1 ~L-t Corr. Factor;. ? 3 y
Meter Box No. /Me "L , Corr . Fac ton
Mecer Isokinetic Factor; j _/>, q _g
Assumed Moisture (%) ; "2
Condensate Volume (ml) ; <9
Silica Gel Weight Gatn(E): 1 1. 2.
Leak Rate
o 9- CFM at c $~
"HE
"r av-
erse
>oint
No.
> if
,,
1 C
9
f
>
4
r
N
,i
z.
z.
-"--"'
Time
Samp-
ling
(rain)
O
r
i a
I <;
7 J
<>-
3*
3r
<^
Vs"
S*
rr
6 0
-..^jr
Clock
t&4d
'7Yy
ซ-
_> ^^
Velocity
Pressure
("H20)
^
,l!T
^
,Tป
/"i
?
,11
. 1-7
,n
,rV
, -^ ^__-.-
Stack
Temp
/05"
fc b"
/ i5 *ป"
l 0 ^
/ ^ C
/or
JCST
re>7
/o t
K 5T
r-hviio
e~ฃ 0-f
. 'J. T ~ฐ* -"
Temp (eF)
Inlet
tav
(j'i
\ 1 1
1 1 ^
r tz
l 2?
'?!
j-z-
/ lv
< 2S-
/25
/zr
7^5
, -^
S
Outle t
9^
/ e>w
1-7
1 [J1 \
\0ซ,
I > C
f'3
I / V
I/ 1"
i / '-
.ซ 7
l / 1
X.
"
^r
Orifice
Pressure
Differ-
ential
<"H20)
! e.
hZ
i, i
1 ^jf
**l (jf
,1 7-
- *:a
,7^
,1V-
t^
,V1
,*?
-
^ .
*$&&-
Filter
Box
Temp
-
:'-?
?^k
Last
Irnp .
Gas
Temp
4<:
* 3
^0
S 1
rfc
>7
^7-
r ,
>V
ff^
^
FJ
-' -
i4
Sampling
Train
Static
Pressure
("Hg)
3
5,0-
1, 7
3, 1
3 S
i,y
3 o
3 7
3 ฃ
1, 3
Q . &
<-, 0
., ~ '-.
,^4^^
-------
SAMPLING TRAIN DATA
Company- f p/i 7/ฐ $ /C" - / f^C.
Sourc
Date;
e Designation: i^/^ti'7 7f ZJ^c t-ฃtz/
X (/
Filter Heater Setting:
r: &? <$ - /
on; ^-/"^ ^,-">/
probe Heater Setting:
Nozzle Number: =y/
Filter Number ; ^er _ 3^ , '-. / ^Sฃ.-A - 2( A- 2 7 Pito t Tube No.j?3.
Barometric Pressure ("Hg): JJ^7 -_^/
Stack Static Pressure ("
Stack Dincnslons:
Plume Appearance
Meter Box No.^/t'
^_, Dia. (in.
):n .5/0
, Corr. Factor f>y'f
1 , Corr. Factor:' "z<
l^O): -rj2=:?'" j^^Meter Isofcinetic Factor; ,/ 7/^
/^J/r/7
: ~
Ambient Temperature (ฐ F) :
Record all Data Every
Tr av-
e r s e
Point
No.
V-/0
V
10
L
y
<
v
3
0
o
-
\.
Time
S amp-
ling
(rain)
ฃ>
^
M
K
T'S
c<
30
r-
yo
vS
tf
'^
(u
-
Clock
/ u '
/_y '
/6 //j
/^,^-j
>i- ^
fl-ifc
po?
#13
/;./?
/;,^?
/^s
/7^5
/7^^
-
- -
^"'
.0"
Ve 1 oci ty
pr essur e
(MH20)
^ ^ ^
A^'
^- ^ ?
0 23
t.l*
c>,^
O.io
0. J3
C-Zl
0,2!
0 ? c
0+tf
'
-'ป ' ' 'ru
->.ป/ ""W/, /--' :ฃ ^ -
'3SlA VERA CE^CTO TAL fszfS
Stack
Temp
/r<5
/ Ot>
ft*
/
joe:
y
/^
X
/^s"
X
fO^>
/e->
" 4 /_.
^^^
Minute s
/?//<
Assumed Hois t ur e (7.) ;
Condensate Volume
Silica Gel Weight
Leak Rate (9, <:' /
*i ce**~ rrff
Dry Gas Meter
Vo lume
^ ^ ^/ ^
t?7ฃ/*79
9 '^-^9
57'3 /, yv-?
9J/-r/>
^^ V / ?
797. / 1
M^ ^//
7^5 ฃ)r
lotz.rt
iQI&fS
t /~i-"* i f1 *}
}U^ [o s^j^
/otf
/2L-
/32
**"
y
13%
h/o
13V
ftf
/J'/
tฃ'7
r3i
* -
/^
Ovitle t
//6
If*
>2^
/PC
/^i>
/3^
/^
;^z
/cC.
A23
/^
/^/
-
/?^
Q'Ot
Orifice
Pres sure
Differ-
entia 1
w-^
P-7/
j?,*/ s"
2,^
.?'^i
^ S'5
-73 /
/? ^ /
tJT '^ *v- 1? '
5^t>
SMI C*' t
-
>"* ~ _ - ,
^iA
^3.
(ml): _ //
Gain (g) : -o -3
CFM a
Filter
Box
Temp
_
-
" -.
r, .
>^^T
t /^ "Hg
'^" / *>X " /^^
Last
Imp .
Gas
Temp
57
9t
?f
92-
rf^
97
^7
9/
c;<
^r
ซ
93
-
n
Sampling
Train
Static
Pr e ssure
ฃป,<>
^^5L
^,^
$-2.
n^'
/& i
~ 1,2-0
I3.b
&.V
It,.*
!!<:>
/*.&>
_
- -
&&
Clavton Environmental roniuTtnnrn. Inc.
-------
SAMPLING TRAIN DATA
Company; |
Source Designation:
Date; ^/z.^/t
S - ."7
feat Number;
Field Person; _
Filter Number-, S 6*
Filter Heater Setting:
probe Heater Setting:
Nozzle Number;
,Dia. (in.) :
- 3 6 "7 - J I"
Barometric pressure ("Kg):
gtack Static Pressure ("H^O); ~ 3
Stack Diaensions; I Z '' f >
plume Appearance: ____
Pltot Tube Ho, tJ ,Corr.Factor;
Meter Box Ne,J?^t-g. ปCorr. Factor;
Meter Isokinetic Factor; I C_? 3
Assumed Moisture(%); /. jg- ^
Condensace Volume(ml):
jy
Aait>ient Temperature (*F) :
Record all Data Every 5-
~
Minutes
Silica Gel Weight Gatn(g): /J, 9
Leak Rate . Qj 4. CFM at / T
Hg
TT av-
erse
Point
No.
i /O
, JO
>0
ฐ>
9
7
4
r
<*
j
3
3
Time
Samp-
ling
(min)
O
(t>0
\DO
/ฃ?O
'i?O
too
ii?D
ivJ>O
i^C?
J<5J
_ .,
1 V-
nr ซ?&*^ซ*i^oy
${*! 0
<\z.
^Kf 7
41 ซT
fflo , )
ItZ , C,
idi
f i^^.T
[0s? C
/ / Z O
1 Ki . 'i
l/A.f>J
- -a.
( fel^>>
Tetnp(aF)
Inleti
94
rrS
ปd^
ii>J
! t.
a-?
^9-
Ji>1
i>=r
iOG
i d^
*o T
I J 1
ซ*r-
Orifice
Pressure
Differ-
ential
("H20)
).
^-Sear
i^ r
i^O
^
Sampling
Train
Static
Pressure
("Hg)
^
1
?
L_
^
Z
'* 2.
Z
?
^
2
2^
-
ซ-<*!- ปnrป> .
Clayton Environmental Consultants,'Inc.
-------
SAMPLING TRAIN DATA
Company ,.
Source Designation;
Date; _ 1/tS/"t 4
ฃT/M C
-- <
teat Number; PS -J
Field Person: ,74 "<-
Filter Humbert
Barometric Pressure ("Hg):
Stack Static Pressure ("H20);
Stack Dimensions:
plume Appearance:
Ambient Temperature (ฐF):
Record all Data Every
Minutes
Filter Heater Setting*
probe Heater Setting;
Nozzle Number: ,Dia.(in,);
Pitot Tube No. ,Corr.Factor:
Meter Box No, , Corr. Factor;
Meter Isokinetic Factor;
Assumed Mo is ture (7.) :
Condensate Volume(ml);
Silica Gel Weight Gain(g):
Leak Rate CFM at
"Hg
Trav-
erse
Point
, No.
/? fc
to
to
1
*
/
(,
S"
tป
I
1
3
* T
Time
Samp-
ling
Cinln)
ta
tr
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sr
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Temp
(ฐF)
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Dry Gas Meter
Volume
(ft3)
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Inlet
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Clayton Environment a 1 ConsuLconts, Inc,
-------
APPENDIX E
VISIBLE EMISSIONS FIELD DATA SHEETS
-------
-------
of Visible EnissiO'is
-1
'
->
,
lv> - i:>
LMtc: " "
T>p: of Plane: i
Type of Discharge: fl'*--
Location of Discharge:
Height of Point of Discharge:
Description of Background: Q<
Description of Sky:
Hind Direction; )ฐ
Color Of Plume: V->
Duration of Observation: I l&v-vw.
OF AVERAGE OPACITY
Distance from Observer to Discharge Point; .
Height of Observation Point: p^-v^-J l2t-.~\
Direction of Observer from Discharge Point:
~*-
Hind Velocity: 3 - |-q
Detached Plume: &> /A-
SUtt'MRY OF AVERAGE OPACITY
Time
Set Hurrier Start hod
1 '' ป
2 escป .">)L. i^ซ\ .Of-i
3 eซ-, ,HTL 0^ x~ i o ti
6 iii vT. \ o If
9 |o (-y ,O L^
10 ,u ?-i ,0 ',3
11
12
13
14
15
16
17
18
19
20
Opacity
Surn_ /--verage
0 0
c? C.
C 6
: v> O
tv O
^* O
a O
ฐO Q
*5 C'^.'Lt c
i -3 O
nme
Set iluvber Scart End
' 21 '
22
23
24
2S
26
27
23
29
30
31
32
33
34
' 35
36
37,
38
39
40
Opacity
5ura Average
Sketch Sfiovring How Opacity Varied With Time;
ซซJ
o.
o.
O
V
L
N" ' 4
Time, hour1
-------
prcon OF viti'iE anssio-is
Coimany hii>e
Plant fddrcs
i- nC Date S -1.1-1^
f)ป >ปj -, \tl1s
s ^KKA^U, V>-ป-ป. 5 n \C Ohscrvor ^\-U.' , Ou* ,_
" un , ' f U
Stack Location l/w-v^e-v^ L^>**~^, Observer's t
I'eather Conditions ^cO
/ 6* ป Location -"^ f^O &
J^. CXev JJ-, W/v-J3 o - fc >42.
TlJ!r fJ-v-tw^arU "'~^**~^'COi'11',FHTS
HR
aai
U --
>-''-:.
-'!!*!
30
31
32
33
34
35
36
37
36
39
40
At
42
41
44
4S
46
47
48
49
so'
SI
52
S3
54
55
56
57
50
59
05
h1
/M
Aj
A/
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M
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M
N
N
N
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15
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N
IN
N'
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30
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\ /^J^*_^t\ซrf IvJ f**^wv^^^
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-
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f ^ts-tx-lk. Jj i^ .-,.... ^j
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' -f _-."- ' *- - - ,-.',-_
^ -*" -. J'-ii- - -,,-.-_! "_'-*".. ^ - % ^- ,' ,_ '
-------
RECORD OF VISICLE EilISSlO'.S
Covpany Name ^ftAC- Date _
.**. t ^\ i r
Plant Address "*Vs-v-vCk. (y^-Hi "^ , C* , Observer \' , \p . vH^i v
Stack Location (. u-vnv.wj-v C-v~ป-f-~. Observer's t
Weather Conditions ^j*
u . ^ Location J^ V 3 3 <.
it'v tti-jC^ ซWMป* c" j ^ ^
.^ <}
TIME
l)R
10 1
--
--
tf
HIT
00
01
0?
03
04
05
06
07
OB
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
79
jd;
SECC IDS
00
4
/vJ
A/
N!
N)
W
NJ
NJ
fj
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N
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,
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w 1,
r
i^* JU* v.^, Cw^-_ ju.tlL^t. - ->
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i
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i
I 'V>AJy*ป K^ixvi^y ~ ~* ^ "^
------ ---*. -i, __----..., _ . , - ^e
-v ซ*r^ir' -ป^ '^^ ^t-,-" - ^ - '"/-".T"~ ' - ^- '-'ป-" V-" ! ^^
-------
' Sunmary of Visible Ernssiois
uotc,
I
Tyfi of Pi ant: si.
Type of Discharge: >
Location of Discharge:
Height of Point of Discharge:
Description of Background;
Description of Sky:
Hind Direction:
Color of Plune:
Duration of Observation: / /ul
OF AVERAGE OPACITY
' ' 7.
i*-1 LJLc'-d-*-!
d J
Distance fro- Observer to Discharge Point:
Height of Observation Point: cj-i^^-^r
Direction of Observer fron Discharge Point:
7 t f
O O W *?yVt~C-fV J iSfzbb-i-A-J jT/'
Wind Velocity:
Detached Plume:
SWWARY OF AVERAGE OPACITY
Time
Set Nurser Start End
1 oci 31 &fi)
2 OV K oV^3
3 O'i < Cv v f
4 o? yo 0<7 >r
5 Of J^ / 13 0 (
6 /o , ซ i- ^ j ฐ7
7 / ฃ, r C fr f J , !$
8 / - . // /& />
"9 /
10 ' $ J L f c. 1 r
11 ^ J
12
13
14
15
16
17
18
19
ฃ0
Opacity
Sum J-verage Set ilupber
AJ 'VI - 21
,V y(J ' 22
* >0 M
' 74
,A/ ^Kt/ ***
A? 0 25
^ ^ 25
/u ,^ 27
*^ /t,' , 28
U ?,L * J 29
,L x^ 30
31
32
33
34
' 35
3S
37-
. ' - 38
39
40
Time Opacity
Start End Sun Averigs
^
Sketch Snowing How Opacity Varied With Time:
e
o
a
a.
_ _....-^- -- .. . . _
!lS11ป*J^^^%^"^^ '3- .=~n-
-------
TO 0? VISILE MISSIONS
Coflpany Har e
Plant AdcJiess
Stack Location
?, r^c
I / KJ fj , l\s '
Obsen er
fi^J P
-. \,
LI jl
V.'calher Conditions
""u
T^. E^ ,v Obsen'^r E
LocaLion
\
S
h <
Jl
TII'E
hR
30
21-
_3_2_
33
34
35
36
37
30
39
40
V;
42
43
44
46
47
IB
49
51
52
53
54
55
57
53
59
JO
SCCC ,
15 31
,0
/u
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JlJ
A
A/
AJ
/J
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A
A)
A)
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A?
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c-V--^^>AJ
A-
^) i r
-t
Ji.
-------
\isuu
Djtc
">c-
Plant Address S^r^ct- ซ, ^t-s, A* C- Observer 0 P |^a}s.^ .V, J*>
Stocl- Location CriijVuo, Oj*<.Tk\i^'O l^ซ*TU'bren'cr's / r r" ฃ~ f A'J
Heather Condition* t't
Wl
cO
--
.-J ' , ~~" Location Xoc JJ^ ^ i- VT
^*\K, C I e. ป4,i>.
v> - '
TIME
~rrr,;
00
01
02
03
04
05
OB
07
03
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
71
28
29
;icJ ^
St
03 {
Ai
AJ
A'
/"U
A/
A;
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A-1
AJ
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i
p-
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1
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" - ซ - ^ i V '. " "^' jx>r-/ 1-1 '""':-". '
-------
Sun.rnary of Visiole Em;ssions
uate: ^-T-t-^ ซ-
Typ; of Plane: I
Type of Discharge: C~-*Ai i
4 |\ ' = 1 i\ .s-\
5 u-.si tv.ซ,
6 ( ! I-*. (Zl ป*\
7 ^ t , i>*\ \i_ ', ป >
- 8 It '- ป^ ^'T-I .
'9 I I- 7-1 1 7. . Z.T
10 IT . LI U.'.Vb
11 \t. ^ M.,-4^
12 IT-'.-VH ^.q<
13 Iv'.^S l-L.-yw
14
15
16
17
18
19
20
Opacity
Sum Average Set ilurroer
c. - 21
o ฐ ' 22
o <=> 23
o ^ 24
c, & 25
0 ฐ 26
o o '27
* ซ=> 28
'- ^ 29
& ฐ . 30
e 0 31
&' 32
c> t> - 33
34
' 35 - -
36
37.
38
39
40
Time Opacity
Start End Sum Average
Sketch Showing How Opacity Varied With Time:
0.
o
Time, hours
-------
CL-
or vni?LE
Company Name
Plant Add res
\^e Date ^-I'l-T^
^ ' , x- nu \ M ^
r ^ -1 X^ ^-. , "At [in^f 1"Uf>> \ 1 .~! \ r L-*jV\jV-ป
S j- t1-1 f_ -^. T rVV> 7| t ^. | ปJ|J J - 1 V '- 1 ff \ \/~ r M - ~
' \J
Stack Location >>L^^_ Tf'~\ Obseivoi's ,. ' ,- -
Weather Conditions Of*
Location A- 3 1; _>ซ-
-t-t -^\ _ 1^0 -^-A e ' 5"
y
TII'F ^' ^ "W*M- ^^OTu'lFNTS
HR
'llfl
30
31
32
33
31
35
36
37
38
39
40
n
42
43
44
45
46
47
46
49
50
51
SZ
53
54
55
5G
57
58
5"
00
^
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N
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----- .,-- j
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-------
Cei'pany tore L
Plant Address _f
Stac^ Location
Or VISIBLE L. IS3IO'1S
Uate
Observer
T> -
1,'eather Conditions
Observer's
Location
TlfE
7- .iFflTS
HR
SECC7TS
03
15
3D
45
31
31
32
33
34
35
36
37
3B
39
40
42
43
44
45
,4
)
A/
46
-0
47
48
49
A/
N
50
51
Al
A
52
IN/
53
hi
54
N
55
M
56
jsl
/SJ
A/
S7
58
ll
i
59
N
-------
RECQPD Of VISIBLE
Company liwc
Plant Addros
Stack Locati
Weather Cond
i nC Date ^ -tT-~Hป
S ^VVJ^A-^-^ V *-irA rt ^" Cbscr/er \ , U3, 1(>i-ซri^>,
on fV^^ซ. fi0-! Observer's
ttions Dv
. Location -~ S- ^>iZ
's*c^J. LxJ.^J U"b
j
TIME
Ilk"
It
1 v
MIH
00
01
02
03
04
05
06
07
03
09
10
n
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
SECCOS
00
i
fj
M
A/
*
N
N
^
M
/J
N1
(J
AJ
A,1
NJ
fJ
N
fj
M
N
tf
fyi
^v
N
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4
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M
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15
jj
A/
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fv
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4
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30
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^
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1*: W: ป^^^ '^^-^^cff^SEHTS
r\, e_
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4^^,^., ^^^i-w^vV'Ji'^-i -i~ป-^^s." *1^_: iป,'-^,v ui ^-^ .L^ป .'-- ~.;2
-------
01* VIABLE
Company lo'vc
Plant Addras
Stack Locati
I'ealher Cone
\^\C Pate M'tl-T1-
s Soo^^.^- PXjL . ft C Observer ,_\-V QrMjx^-.
Q - l rj
on V^Xvc IP - * Observer's
itions Ou<>
j. . , r Locntion -* t>o ฃ, t
-u.-^ .UJ^v-L. O - S
i
TIl'E ^i - ws ,x*~ox itvkv"y>"co1',i;pMTs
IIR
\1*.
--
'U'l
30
31
32
33
34
35
X
37
38
39
40
n
12
43
14
45
46
47
48
49
50
51
52
53
54
55
56
,57
58
59
Jl
N
H
lj
N
Aj
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M
N
N'
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r -. j^ i~- ~7" ij - \ /i
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ซ Q
,
1
,
1
,
.-""'* - , "
~" ~" ~ .' ~- ~t ,.XT ;: --'---'"-.- s . . -',
-------
Sunmary of Visible Emissions
U
Tyfi of Piant; \ rn c n^-
Type of Discharge: C_-v-~ซ*'*-
location of Discharge; - \ <*
Height of Point of Discharge:
Description of Background; C
Description of Sky: \*~3X-^
i
Mind Direction: N- ^ w'
Color of Plume; ^ ^&-u*-~ซ-
Duration of Observation: -^ \ ^2, jJrn^-T-
OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
Height of Observation Point: W^ซ-V
Direction of Cbserver froi Dlscnarge Point
,
"\
Hind Velocity; D-ip
Detached PI umai Ki //V
SUflHARY OF AVERAGE OPACITY
Set Huraer
,
2
3
4
5
6
7
. 8
'9
10
11
12
13
14
IS
16
17
IB
19
20
Time Opacity
Start trd Su,ii^ J-verage Set Nuraer
H-ปn iv v> ^ ^ ' 21
t^,L3- \S 5.ซ\ -^ 22
ivtl \'i ^ c 23
li^f u'^ii t? o 24
U -H rป ซn ^ Q 25
11' ^T i-a-j^ " ฐ 26
j^ ,o> if it * ฐ "27
i^ if M- ^-^ , ฐ ^ 28
\^ ', t^ t*s| , i,i*- ^ ^^ 5s
tA- , ju. H-'.^-L * * ,30
rt'.lt- 11. W -* ฐ ' 31
\% -!,ซ i4 '4* o c>' ' 32
iij'44 )f;s* * ฐ '33
m p ijo j^f , 5 ij o ^ 34
, *n ฃ? * ^C
l^lCU 1^,0^ ^ ซ|Q
3S
37-
38
33
40
Time Opacity
Start End Sum Aversgs
Sketch Showing Ho* Opacity Varied With Time:
I
01
II
Q
cx
o
.
-------
RECORD OF VISIBLE OUSSlQ'iS
Company flame \ v\ C.
Plant Address ""Sf* <~^ UA6- Vl,>^
Stack Location IM/WC, "Tp-^
Weather Conditions y^\tX-ป Diju^ . W-i-^
Date ฐ\ -i,n ,-> <-
Observer X ,\,~. ,Jtv/V-'
02
tป
03
04
05
05
07
OB
09
10
11
12
13
14
15
16
17
0
IB
N
19
/S
A)
20
N
N
21
22
h
N
23
/v
N/
24
fJ
25
25
/v
27
A/
tJ
28
N
vn
29
fsl
TT
-------
Co-npany tome I
or VISIPLE EMSSIOJ.S
Date cl-Vl--?ปป
Plant Address *^i
IV
M
(SI
^
.^
jj
Nf
A/
A/
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AJ
AJ
N)
N
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-
33
fO
A/
W
^
M
N'
rJ
.A/
AJ
\J
hi
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N
rV
fvr
N
A/
M
N/
^
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N
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N
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x\ o ฃ^r
,
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RECom or VISIBLE oussio-.s
Compary Itame
Plant Addres
Stacl Locati
Weather Cond
LJV\ C Dale ^ -'v"-1 ^
n - ป \ ' \ r
s >~\VA>-eJ!^ ^ '-y^- A A Observer ,-VVJ-, !iT-'^i>vv>
- ' ^
on "^Vt.-iv^. "T ' -"k- Observer's J
itions C\i
i . ^ Location A-^jO^t;
<-vj_t _^y , U) xi^i Ct - \
-------
Company Hanie
Plant Address J>y
nrcoro 01 VISI.HL LUSSIOMS
Date
-1 <ป
Observer
k Location yt\~.t.
l.'eather Conditions
-
C - .$
Observer's
Location
5*0 '
IT
TH'E
CO'JOTS
HR
SECONDS
rv.
30
00
IS
45
IL
32
u
A)
r
Ai
IV.
33
N
31
35
Vi
N
36
&
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N
37
R
A/
N
38
Kl
39
40
N
M
K)
K) N
N)
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43
N'
Nf
47
48
M
-0-
49
*
50
N
51
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N
52
N
K)
53
N
M
54
N
M
AJ
55
M
56
M
57
53
Ni
N
N)
N
-------
Summary of Visible Emissions
uatc,
Typ of Plant: -fiJiP*1" C>oJ A ^
L 7 r
Distance frcr. Observer to Discharge Point: <*,.-"/-**/ /u '
Tjpc of Discharge, o^ ojซc ซt\^j
Location of Discharge;
Height of Point of Discharge: /e -
if
Height of Observation Point:
i di Ll / tj ire I
Direction of Observer from Discharge Point:
Description of Background:
Description of Sky ฃ'
Wind Direction:
Color of Plume: /o <- <- ->< ( d r L<~*~>-'
Duration of Observation: 7 /H ,
SUfiMARY OF AVERAGE OPACITY
"'
>; -?>3
Hind Velocity;
Detached Plume:
77
<> r
;i
,i
SUMMARY OF AVERAGE OPACITY
Time
"Opacity
Time
Opacity"
Set Hunber Start End Suru f.verage Set uu^ber Start End Sum Average
2
3
4
5
G
7
8
"9
10
11
1Z
13
14
15
16
17
18
19
20
if . ฐ ?
/ j 's""
/ a ' 3 (
^; n
/ r 33
/ J 3 /
/ f i" c ^<, '
/ j t V /V
/ ^ 1-^ AJ
/).') (J A-
/;?' 3 2- /t
, 2 3 f J^-
/ 3 ' v y
>L/
24
25
27
28
29
30
31
32
33
34
35
36
37-
39
40
Sketch Showing How Opacity Varied With Tiir.e:
01
ex
"> Time, hours
-------
OF VlSh'U L'.ISSIO'.S
CoTpany Iteiie ' "-
Plant Aadu'ss -J,MOC e J/,^ei
i - * ' rfi
Stack Location S. , , ^ <~M C.v-jsu~\
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leather Conditions ^.-U^JJu
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Date 7 f - 7 /:
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Observer's _ , c
Location "7 "S v
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rrrorb 01 vi JIปIE iiissifi..$
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Stack Location J) <> ^-^O) ^-M C v~,Wv- Observer's / c ซ ( < /- I
I'cnllicr Conditions
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THE
HR
-
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30
31
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31
34
3<5
35
37
38
39
40
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42
43
44
45
46
47
43
49
50
51
52
53
54
55
56
57
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59
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VISIILt
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Date
5" -^ -
MantAddres
S,^3,-,,e P,,o^ >ซJ C o-ซcrซr D iP Aj*/ZJ*LL
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00
01
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03
04
05
06
07
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09
10
11
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
?e
29
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AJ
^
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Or \lbiric. UHSSIQhS
Date
CoTpany lljn.c _ / / / V:
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Location _ฃ_
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Suirmary of Visible Emissions
C_ I- t,o ซ I MJ ซ"ป
!r pi. -*-y
uate; ff ~Ji "/ ' t ฃ
Typ: of Plant.: VtSip*'
Typo of Discharge; I \-^ ,
Location of Discharge:
Height of Point of Discharge:
Description of Background; ^
Description of Sky: S/c^d
Hind Direction: C> uT
Color of Plune: /Uc
Duration of Observation: / /i j'^
Slff'iHARY OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
_ *
Height of Observation Point; \arcv#*
" 'IV
Direction of Observer from Discharge Point:
ฐr
Wind Velocity:
Detached Plume:
SUMMARY OF AVERAGE OPACITY
Set Huirber
1
2
3
4
5
6
7
. 8
9
10
11
12
13
14
li
16
17
18
15
20
Time Opacity
Start End Sum^ Average
I 3 ป'i / J.^-3 A- /w
/ i ' * ^ / 3' J'i ^ <"
/ J f ^ / 5 5 j' /v -A^
/^ a u. i3'jl>i' 'V
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1 H * '1 J -i' 3 V >U '<-'
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nme
Set nurter Start End
' 21
22
23
24
25
26
27
ซซx-r 28
J 23
30
31
32
33
34
' 35 '
36
37-
38
39
\40
Opacity
Sum Average
Sketch Sfiov/ing Haw Opacity Varied With Time: w
CL
o
-------
REcor
iutc
PlEUt /.:J|35S _ b* -j,,. ^ I *J^. iV C
T" V" Pi "^ A/
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Location "? 0 3 ^ _c> V
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1 18
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01
02
03
04
03
OS
07
08
09
10
,1
12
13
14
15
16
17
18
19
20
Zl
22
23
21
25
26
27
28
29
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Oi v'Su'Lt L '.i
CoTpany Ibirc
Plant Addiess
Steel; Location
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30
31
32
33
34
35
36
37
38
39
40
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43
44
45
46
17
48
49
50
51
52
53
54
55
56
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Stoci Location
Weather Conditions
^ -Vc.-
P'jscrvcr's
Location
Hi;
1
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01
02
03
04
05
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07
08
09
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13
14
15
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19
20
21
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23
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Plant Addies
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30
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32
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45
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bsci, nr'5
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11 R
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01
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03
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05
06
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09
10
11
12
13
14
15
16
17
18
19
20
21
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23
24
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->.
Sun.niary of Vis
uate: 6, -L<8 7 ^
Tyfi of Plant: \f* C
Type of Discharge; '
Location of Discharge: Ti>->i<- "
Height of Point of Discharge:
Description of Background:
Description of Sky: N), '- -
*
Hind Direction: M//>
Color of PI une: <> /A
Duration of Observation: ^M ^''/A,
Detached Plume: N> ,'/\
SUUflARY OF AVERAGE OPACITY
Time Opacity lime Opacity
Set Nurrher
iT-a;-
2 I
3 (
4 Of 1
5 ^ J
6 C^- ]
' 7 (
8
9
10
n
12
13
14
15
16
17
18
19
20
Start End SU.TI average Set Nurroer Start End Sum Averts 5
*ป*
roc\.o-b li-'voq - ฐ * 21
_oc' **< f* i* o 0 ^Z
-i*'.oei ,t.^ c e 23
, it ^ '^ v 5 O.LC** 24
1 ' T_ Ml IL1 T.1 'to |.l,r 25
U- >* !V,^ AC1 llfr ' 27
28
29
30
31
32
33
34
' 35
36
37-
38
39
40
Sketch Showing How Opacity Varied With Time:
8
01
o
ex
o
Time, hours
-------
or visirir L assi
Co ,'x>y J-d'.c
Plant /.-Mres
St. PC! Locati
Weather Cone
/ i/'/ ^ o^tc r/c*>j/ /&
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///
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00
01
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RECOIL 0. \1SIOLE
Ccr.piny Kar.2 _
Mont Addicss
Date
vci
Stack Location _/1_Q__[ _ig.Jj
Vlsather Conditions (L [
Observer's
Location
THE
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Company ^no
Plant Add re. s
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//i] C- Date Cj/rjf}/?^
s Ohrt,', ~t~ /" I ' f ^' *- Observer j^, ji IwfWc-V..^-,
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of Visible Emissions
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Typ- of Func: ' ' ^
Type of Discharge "vC-cl.^
Location of Discharge: ^ -^
Height of Point of Discharge:
Description of Background: T
Description of Sky: Ouv^, c^ c> >x ^ ^
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Sketch Showing HO.V Opacity Varied With Time:
V
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Company t.J"2 , \
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p]ant Address *-* ^ ^ ^ < a j-v^- . Vi /^ ป
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31
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33
34
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Date
Observer
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PCCORO Of VISIBLE EMISSlO'iS
Date ฐ\ I -. ]
Plant Aadiess ^>-o.u^ซ.'- ( ~-<- K.C, Observer X . \-^i VJ^-tv^v
11 r * 0
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-------
Company I'ji'ie
Plant Address
Stack Location
iU) 01 VISloLL LMISGIOSiS
Date ^ - 1 '6
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\
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Observer's
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vtr
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30
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33
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35
36
37
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RECOPD OF USIGIE [MISSIONS
_ Date
U -1 tป
Plant Address "S ,-
Stacf. Location
Weather Conditions
Observer
Observer's **j \ _
Location f A 21 t
V$T
"\r
-
_*_
MM
00
01
02
03
04
05
nf
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07
08
09
10
11
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13
14
15
16
17
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19
20
21
22
23
24
25
26
27
28
29
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00
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-------
Sun nary of Visible
uato:
Typ i of pi ant-
Type of Discharge; J*.-*$*
-U. -X l'ซ-'~' t-1 ,
Distance fror, Observer to Discharge Point:
;.,. J-
Height of Observation Point:
Location of Discharge: ^,ซL^, .-i--
- ' i f I
Height of Point of Discharge: "lo *,)i*' '"^'''Direction of Observer from Discharge Point:
Description of Background: p.-U.-.^ ^ L^,~^Lf ,ฃL-ซ- t-
Description of Sky: Ay '' ' .
Wind Direction: /-'/^ Wind Velocity: f- /^'
Color of PI we: ^f >,,>-l'k< yV-^.- Detached Plume: /.//j1
Duration of Observation: / /-< ^-*v
SUfSHARY OF AVERAGE OPACITY , SUMMARY OF AVERAGE OPACITY
Time Opacity
Set ftuFier Scart tnd Sum r.verags
! /-e^^ cr'_S- f
2 ( e^*.\<ซ o'.'at- - ป
3 1 c^ Ml t-'O ซปS '- "^
4 1 -ซ, <,v aซ, s-( c O
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7
. 8
9
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11 rrc si ij -si ^ ^
12
13
14
15 .
1 U S^ 1 C A v
1 > O "j 1 1 O rl c ^
u o-i v 5 ฃ" c
V A<, " l-V c ฐ
15 H * \ ji n 'V <^T *-* k'
17 \ u.ti i.-:^s ^ ซ>
18 U 13 \> 31 ^ c^
19 | u 51 U 'ซ<*"$" c^ ^
20 V. v^S il.So ' ^ o
Time Opacity
Set rlmrter Start End Stfn Average
' 21
22
23
24
25
26
27
2S
29
30
31
32
33
34
" 35
36
37-
38
39
40
Sketch Sfiowing How Opacity Varied U'ith Time:
c
v
BJ
a.
s ^.
fi-
ll
Time, hours
-------
01
/ /#
Plant McSress -^ /j^, k >. *- //>vc-_r X
Stacl. location T'-'S.. f /-
-------
RECC'J
c
Plant Address _
Steel Locetio.i
l/sathor Co-icfif.
r ซ- P, ;^r^ Ay
1SICLC L.li G,i-,S
I)'to __^
f jsci or X. '' ^ /^
Ob1 cr.cr's
Location
n
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rr,;
01
m
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03
04
0>
06
07
08
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ID
n
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13
14
15
16
17
13
19
20
21
22
23
24
?5
26
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28
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Date
Plant AdJisss ซ5tJt
Stack Locjtion
/(J <
dosorvrr _jQ
if _A/ g
I t-a*. ^ U . I ^
Conditions
Obsci vor's
LocaLioi
Tit
CO .fiJT
30
31
32
33
34
35
36
37
M
SLCC-.QS
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fi - \ V S
fr // .A/, II
^
c' 77t-
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-------
ptconi f sisir^c
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-------
IIP
f-L
PI \i3iuu
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Date
Plant Addi ess ^ plru c
Stud- Location f f c- *.<- j
I'calhrr Conditions /
c P,^s A
. f^.^ (Pj-^*;
'J/4
*Cs Obseiver {J il hJ*
, j^j sef/lr
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Locali on o >-
$lt.' ~ Jt*.--L/
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on
30_
31
32
33
A/
A
5CCC,
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A/
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35
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38
39
A'
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13
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46
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48
A/
A,
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f)
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50
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1L
54
55
^6_
_57_
1L
51
-------
Summary of Visible Emissions
uate: '
Typ.: of Punt: (
Type of Discharge: GV^^M-V- I ^>-^K^ v. ^.M-V,
Location of Discharge; Tif5 , \ (-rp ^ yp-,5
Height of Point of Discharge: \)^^*<,
Description of Background;
Description of Sky; ff/A
*
Hind Direction; jO/A
s. V ซ* ,
Color of Plume: >U iP-^'-iM- ^
Duration of Observation: \ ^^-^ >^_^
SUMMARY OF AVERAGE OPACITY
Distance frorc Observer to Discharge Paint- <
Height of Observation Point:
Direction of Observer fron Discharge Point:
Wind Velocity;
Detached Plume:
SUMMARY OF AVERAGE OPACITY
Set Hur-oer
1
2
3
A- i
R " \
6 ^
' ?
-!
10 l
11 T
12
13
1 5"ft" """"
16 \
17
18
19
20
Time Opacity
Start End Sum fverage Set Nutrber
^[S-k* \3'->( 0 ฐ - 21 /
, p fm t I
| 3 S 1 f^'-i? 0 C) 22 V
v^ ST ^.i-5 0 C 23
^ 4^ ; o<^ | q. \ ) O O 25 "f " ^ A
^.,T i^ M ^ C- 25 J A
^at ^ ^ o o 27
,4,1-1 K,^ *- ฃj 2B
,<, ,)$ i4', -Ji <^ ^ 29
^jq ,1*1 .^.ir -^" ^ 30
"1-5 ,0L> i ^> ^ ^ (_, 31
1 C ' o ^- ' ป ^ ^ *30
-^ ^ ^ *""*
.s.ii. Wi% ฐ 33
Vxlir vV2f ฐ ฐ 34
(~V /""S * *% P*
1 "5 , 2"f 1-5 30 ^ CJ 35
K 3<3 iS.'SC C) " ' 36
is ,3t- i5." t^1 ^ 0 37-
*s "C1
Sketch Showing Ho*f Opacity Varied With Time:
*>
o
*
0ป
a.
^i
OL
O
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" '
* * *
mm
m
,
r '
. >
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Pr *l
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.
-
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"
Tltro, hours
-------
LI OF VISIEAF u;
3r,j,i i) 11 an'
Iniit Ac'di ess
-5 r ^ c c
Stacl Location
Heather Condi tiors
f
^ rr t
r C - C'jsci vcr _ ฃ) , (P
Observer's
Location
TI'iF
co : I[;:
W
SLLC :js
01 15 \ 30
00
01
^
02
A,
03
^
04
05
06
A.
07
r/7/
08
09
10
11
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24
25
26
27
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30
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fy
A/
r4
^' ^ " ri"**"v"a)j"'EHTs
,
,_ t
1
_^t 1
^E ' 1
-._._. '
1
"
]
' - . .. *.-..._- . ^ ป
* "S * 1
,, | .- . -,../ป.. ... v.-. ,^ A -- -
-------
APPENDIX I
EXAMPLE CALCULATIONS
-------
RFfORU Of VISH'U C.ISSICJiS
Coiuany llJiiiG \ V\ C_
-t ,^ '.<,-
f * ,Vv ป
Heather Conditions ^^<^t, ^>! , ;v wv f - o
Date M Z-i-~|fc
> ' ' "
Observer i, v^\j ;Vt- -'>->
Observer's ^ ^
Location ^ -^^ "] J S
Tl'T ' .-,.--- - co i!rNTS
K'R
C
" .
J ~" If
"{'(
30
31
32
33
34
35
36
37
38
39
40
T
42
43
44
45
16
17
48
49
50
51
52
53
54
55
56
57
58
59
i
J3
A
\i
!^
N
"v/
I
ri
NJ
f^
\'
N1
.J
^0
A!
\r
SECO..OS
15
Ai
A,'
rJ
w
N1
N'
AJ
^j
M
V
V
IN/
f;
(0
Nf
_-
33
Aj
^
M
.N1
A/
M
rJ
rJ
A,'
?sl
rO
N
N1
N1
f-J
45
n
rJ
Ni
N
M
N
rJ
rJ
M
/M
?J
fv
^
N'
^
-
-
,
J"
*'
-
i
,
''-.* - - ' v, . . r
-.--." ': -" ^ - - --,, , _^- -,- *
~.~ ซ5-j
""ป*. M. *~*q-ป M> ' ~ _, 1 ^..*
,**- -,-ta h-p, ปซ._ซ.._ .(-UT^, ซซ, JV"
-------
Summary of Visible Emissions
uatc' " -"" "* '^
"^ "ป *-j"i * rt.jt'*-
Typi of Punt: 1 ^ C -~ t^*y_^^ "'"'".^ ^-v-> ^ *~>V-^ i^i--C*-
Type of Discharge: ^- '>_v'-jt^-^^"T"
Wind Velocity:
Detached Plume:
Direction of Observer from Discharge Point: S
Kind Direction: ~ - n ฃ
Color of Plume:
Duration of Observation:
SUMMARY OF AVERAGE OPACITY
SUHttARY OF AVERAGE OPACITY
Time
Set Nunber Start tnd
, c-.'i^ ซ1^t=
2 C ""ป 5 b /C /O V
3 t",e c. 1C ' <-"*
4 | c c ^ > /('';ซ'
5 /u ' 1 4 /c ป ฃ~
B i c ป c.c jc' z i.
7 i c ' t-u ป o : 3 i
8 i c ', > i. < e " - x
-9 icr 4i /c: */ซ
10 )o lit 'J ซ > ^
11
12
13
14
15
16
17
IS
19
20
Opacity
Suซi Average
ฃ if
^ o
J> O
O t>
D .
c- ฐ
o
o o
c o
L-"1 l>
Set ilu^ber
" 21
22
23
24
25
26
27
28
29
30
31
32
- 33
34
35
36
37-
38
39
40
Time Opacity
Start End Sum Average
Skstch Showing How Opacity Varied With Tire:
ฃ 5-
o
IQ
CL
O
*ป"", "f> 'ff-^:"^ J^-1!"7'=-i"'-^-J gt'n^'-'-i-z^v-v""'*-!-0-? '** V-v^'^K^i* -;- ,
,lJny'^:. v.~^j?ปซ-1.-Jฑ-^r._ *' .-^ฃ:?- __tป-_L;?w4r4...-ป.is', .-A ,,:ซ
T hours
-------
Coi'pany Name \ \f C.
Plant Address Srf>_k^i
RKOI'J OF VI SI I'LL HilSSIOliS
Date
vcr
V;.
Stack Location
Observer's ^_
Location /
leather Conditions
HP
~^%
'
1
s ~\ *
'
-^
J.I i
30
31
32
33
34
35
36
.17
38
39
40
T
42
43
44
45
16
47
43
49
50
51
52
53
54
55
56
57
58
59
Tir
33
M
Nl
rJ
is!
M
fJ
N
^
N
Nl
SLC
IS
rJ
N'
N
hi
N1
N
N
N
N
N
c,:OS
33
Nf
N/
Nl
^
^
N
M
N
N
N
45
v/
r,1
Nl
Nj
|>i
NJ
hi
|S/
^
N"
CO ./IFfiTS
ซ
,
.K -
*" '.
.... , ;
.
\
,
1
,
.
.'---- - ; . - , . -- - , . -- *
"-. -,--7 ''- -- - ~~ -i "" . ". ;~--r,.- - V-5 - -
"TSW- "^ * "
-------
REcon or VISIBU
Company Ifaire
Plant Address
ฐ, 2-V7L
Observer
Stacl Location
c -
Observer's
Location
Weather Conditions \f ?->* r~
s ฃ
Hk
*s
e"
ฃ-*, -
.&,
riTi,1
od
01
oz
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
IB
19
20
21
22
23
24
25
26
27
28
?9
<
SE
CO
A
ri
N
IvJ
1!
r-/
fv!
K
is/
M
/J
F^
J\/
Nl
fj
A/
A/
h1
fO
N
N
N
^
N
-\J
N
M
N
N
rJ
1
.LC'.'OS
IS
F'J
r,1
\
^
r ,
AJ
fj
N'
Ay
r,'
^
M
N1
N
\'
N
^
^
re
N
A/
^
N
Nl
^
N
N
i4
N
N
| V-
Til
30
f-
r'
i j
>;
N'
U
M
N;
w
^4
li
N1
^
^
M
rJ
A/
A/
N
N
M
rJ
M
N
V
ซvj
rJ
ri
M
M
N
i.
IE
i5
r)
rJ
/^
fj
K
H
A/
'vl
M
N1
K:
^
IxJ
N
V
r/
^l
i\i
(\'
M
N
N)
M
N'
N
IN!
NJ
K
rJ
r*
-*
^ . ^J a >3-- t-~ "^rME;,TS
,
1
1
J
4
1
,ซ
*7 i
i
i
i
-
-
i
' i
-.- , - - .- - _.t
-. :-- ,-", -. --, .,-'--'-
-------
Company 1'jn's '
OittJ 01- VlSli'lt C 1
PU'lt Address Sr-ip-'K-.c^P -~. T^
f** +-.-A----. /t ' I
Strck Location V--> i .~~ซ-. *>-.,. N
' > ~ฃp
l'e?ther Conditions r. x..w. ? tU
SSIOJ.S
Date c ^'
Observer __>*-_
Observer's w
Location '
TIfE ' CO . lEfiTS
HP
\\t 0
rv!
rJ
M
N
N
N
r^J
N
N1
N
^
N
j3
A<
^i
tJ
M
N!
/J
rJ
\!
^
N
H
r4
N
fJ
jv;
Nl
N!
^
M
K
4S
'-]
fl
V!
\\
ti
ti
^
M
(I
N
i
^
I1
N
M
K!
N
K
fJ
rl
'-
t
-
*;
,
;
,
,
~ - ~ ^ "* , '*"^~ **
-.-,"""
-------
Sun.mary of Visible
uotc: T- '- ' ^
T>p- of Plane: ' f'1 C "T.
,\ -
Type of Discharge: ^ ./-ryu --<_ *
Location of Discharge: .'U*- x -ซ*/
Height of Point of Discharge: ^ - -~'"1CS
Description of Background: "i1^1*",) 7 ' u<: ^
~ i
Description of Sky; 'J^-c^t-^-
Hind Direction: \' ^
r
Color of Plune: ^ LvwiQ ^c*-ซ-*-
Duration of Observation: \ \i-ii,wi
OF AVERAGE OPACITY
Distance fro.1*; Cbservar to Discharge Point:
r
\Height of Observation Point: .^- ^c
Direction of Observer frora Discharge Point:
^;
Wind Velocity: f -ฃ f
Detached Plume: ,^//'-
SUfulARY OF AVERAGE OPACITY
Time Opacity Time Opacity
Set Huriier
1
2
3
4.
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Start tra Sum average Set uuirber Start End Sum Average
\o-._ _,-* \ ,;ci c ^ '21
\.. '.e\ u-.QT C 0 22
vv - c T v - , -%, .r- c 23
\ \ : \ v ' ', 1 1 ^ c c1 24
i.-.c. K', ^-L.^ t% o 25
H'. i1* c, *. i t o c-ซ 26
U'.-s, n'. M ^ ฐ " Z7
f. ^-7 i : *n ^ ฐ 28
1 - ', ? V , -. ซ ci '--1 D 29
U ',f\.r> M -, -si' r ^ 30
31
32
33
34
' 35
36
37-
38
39
40
Sketch Showing Ho// Opacity Varied With Time:
Hฐ.^
lime,
-------
OF VMi'lE L'HSSrO'.'S
JV. C
V
Plant We!1 oss -,I.-'-S.. ;
"it
Observer
\ ,'
Stack Location
Voathcr Conditions
*? . \,-^f **+. i ฃ " **
Obsc1 vcr's
Location
TItt
. J/i M/V^"""**-'V"-
CO,,,;F;,TS
w
"1C*
\e-
v - -
r.ifi
30
31
32
33
31
35
36
37
33
39
40
/,:
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
59
00
fO
r4
fJ
N
N
SLC
Ib
^
S
[4
rsl
N
C :15"
3J
.
N
{^
fsf
N
N
45
tf
r^
n
Kl
JT^I
-
,
-
/
*'
;
,
i
i
.
-
_ ,.",- * *"*' -
-------
Company Ihi.o
Plant Address
Stack Location
RECORD OF YISIEIC EMISSIONS
Date
i "vfj-u^o-v
, ,j
m jvu^v
lions '^T.
f A. 1 ' C -
,\ i r | (
u ป
~tt vV U --Wv '? b
Observer ) iC \v- ซ/"<>*-
\
Observer's ^ /
Local] OT '"J 5a */.
Hk
^
V-:
T.TTT
00
01
02
03
04
05
06
0?
OS
09
10
11
n
13
H
15
16
17
IB
19
20
21
22
23
24
25
26
27
28
n
u
Sc
00
fj
rJ
A,
^
K
)J
Nl
W
N'
r-;
/j
rj
v
N
M
N
H
^
h1
N
M
ti
N
Nf
N
M
N
iJ
.CC ,5?
15
M
H
pi
N
rJ
fj
.ri
N
^'
N
N
/%'
TV'
N
rs>
Nl
f/
^
fl
N
N'
M
ซ\'
\'
h!
(S/
Nl
N)
N
fxl
TI,'
;o
^
a'
fJ
*)
N1
fsj
M
N1
NJ
M
/v1
rj
M
M
ri
N'
N
N
N
N
Kj
!>/
,v
V
isl
^
N
N
W
K!
k
1E
45
N
ft/
^
A)
rj
*j
N!
Kj
ri
t\*
fj
K1
N
W
W
N/
N
tsl
M
\'
\'
A/
N
N
^/
N
ij
N
rJ
N1
t
UT^-SJ^ ^-v C0.|1)E;;TS
ป
rfs"
'
"
- - * ""* /1_ -1 -( -If^^^fc""*,
>f*-
-------
ITrOi'iJ 01 VISi.'Lt
Con. an/ Name 1 |A Cr
f -^ \ * f
Pl&i't Address V-OVA^X-, >-*- ' ^-
Stack Location ""%_\.IU^. tVb~>*,'-^v 'J4, "
(feather Conditions nv,-i -ปซ , ',- *vx> r
THE g*^w.^ -
,I3SI&,,S
Date
Observer
Observer's
Location
5-
*->ซr> .-ซ~- f
CO .iFilTS
- 7,4 -1 '
\ i K
> . L-^ r>u-ww
I _ ^ /
HR
' 1",
*
_ J
r'I'i
31
31
32
33
34
35
36
M
38
39
40
,-,
42
43
44
45
46
47
48
49
50
51
52
53
54
55
56
57
58
51
,""1
r1
tj
fJ
r.'
N
K
>!
[0
^
A,1
n
r!
N
^
H
f,1
rl
:J
fc
^;
N
/J
K)
/J
l\!
"
SECO.iDS
15
-I
tl
M
r/
rJ
;'.'
i !
K1
M
/J
w
ti
!
i
1 !
f '
M
'\'
A'
N
IJ
fO
rJ
M
fJ
3D
r^i
rV
M
>-l
>J
r1
u
K/
rJ
iO
. i
JV
f!
T:
fx
r]
/:
Ki
A'
'
. i
V
M
M
iJ
^
rf
45
? <
'j
f','
r>
j;
f;
r.
!'
[\j
\
^I
II
N',
f<
f>'
N!
N
^
1
< i
V
K]
NJ
N
H
N)
V
*/ ;
.
"i^^ij" S-tA-vtZ* ^^'-KC
'
-------
Summary of Visible Emissions
uatc: 'VvvT1"
Typ: of Hanc: 1 ^\C.
Type of Discharge: ^'
Location of Discharge: "' ^- ^ ^ -^
Height of Point of Discharge: &- '
Description of Background: "%'--> f
r- "?-
Description of Sky: '- v-fc-^-c ^ -
r
Hind Direction: fa c
Color of Plune;^-^ \.uw.\!
Duration of Observation:
SUW'ARY OF AVERAGE OPACITY
. n u
Distance fron: Observer to Discharge Point: o 'Co-
Height of Observation Point: <~ *iO
Direction of Observer from Discharge Point: V\J
(. 4
Wind Velocity: ^ -/&
Detached Plume: ^ A
SUHHARY OF AVERAGE OPACITY
Time
Opacity
lime
Opacity
Set Nuroer Starr Lrd
Su^i
Average Set .Jurroer Start
End
Sum Average
t ซ" i
21
4 \4',l* H ^^ ~ ฐ ^ . 24
5 4',H i^!^J Jo 25
6 |cj -,^o :^| ,^u o o 25
"7 i^'.-sc '^.^t o ^ '27
8 i^ ,a ^ i
-------
RECOKD Of VI5IBLC E.",I5S!C,S
CD
Company Hare H > ^ Date \ - LV"! *=-
n \ 'N "
Pl*nt MdiGSS S-o^c^. >>. -v V 'i- Observer / i . l _ป , V>*-fcv..~
ซ V
Stacl. Location >-"T*J._ ,f>^J./i . v 'v: >- Observer's -
Weather Conditions t i
U Location s~ ' O >> ^^M
t-w^i-s 5 O-,.~A l - 1 O
T - '
TIKE
HD>
%^
Ml'fl
00
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
2?
2fl
29
SฃCG ,JS
00
B
Aj
i\/
\
^
^
T;
n
u
*' Jr
i!
^
^
N
rs/
U
N'
tl
hi
IV]
fJ
N
fJ
A'
N
^
ti
N
hi
Aj
~ .J jj,4.
i5
^
rM
^
\'
^
fj
, * 3
M
U
M
hi
M
Iv
N
N'
N
A/
M
^
rJ
^
fJ
fvl
*/
f^1
N
^
N
h
fsl
30
M
. i
r )
N
ft/
N
i]
?!
Ki
;J
N
ป-4
V)
!^
N
fJ
h!
hJ
/o
,-j
fsl
AJ
M
^
fj
ISl
N'
H
i
fO
.A-
N3
A/
N,1
' ]
w
U
1 '
1
JM
M
N
/^ ,Wซ>
i
I
[^"--v1^- V n^,x-A
'" !| J ' "
j
-
'
i* -T ป^*^- j -^f-^i^-"" %- * ^z ^ "V***.^* "i^~r' * ! '% ฅ"****^ - * i **-; *-**- ?"*-*- v
-------
urcorj oi VISIBLE
Co.i'prnv lij 2 n 0-
Plant Arlclicss >~oi~-v_~ r j~
Stffd. Location") *-'^ V-->-
r,nher Condi tiuns ( -i-^ ^
^.V, C
*L.V ^ --
, <),
2. ^^l o-t
1
Date ,vj "Vl^u-
^
y<- \ 3 O IxJ
HR
-(4-
-
_ .
Ill .
30
31
32
33
31
35
35
37
38
39
f{Q
*t t
ซz
13
14
45
46
17
48
49
50
51
52
53
54
55
56
57
58
59
TIC
T]
ti
fJ
M
rJ
ri
fi
rJ
f^
>j
^
;]
^
N
M
*>)
N
r^
r'
ปj
\)
r\j
M
^4
N'
Aj
rJ
N
N
NJ
H
SLC
1=5
^
rJ
L
N
f!
tf
/-'
,V
rj
NJ
A/
KJ
/\'
fv'
l'j
fJ
r^J
r>l
IN!
rJ
tl
M
M
N!
N
N
^
isl
N
hi
C..1S
3D
^
A/
N1
-f'
rJ
rJ
,^
N
,'J
N
A;
ปv/
K!
K
ti
NI
NJ
N1
rJ
N
jx]
Nl
r4
N'
r4
N
M
N
N
l\i
45
^
fi
fJ
N
N
i
i
,\
N1
r-'
,M
rJ
i
M
f\!
N
N1
!\i
/J
rJ
^y
K/
rJ
N/
N
N
N
N
N
Ax!
. * ^ L ' CO .nr'iTS
-
ซ
,,-
*
... . :
-
-
i
J
I
;
1
'-/,-. _ , . _. -" 5-
-------
KLCORJ C!
Ccrrpany ikr:
Plant Mdiess
LIUSSIC.S
Date
^ J.
Observer
_.
/P P
Stack Location &tj{*cT or f J ./tปjpซ.U*^>J)bsen.e) 's n f / /
_ ,I flj I / /. Locatitn /a A el ..L/Q Lซ
Vcather Conditions C U^jU Un=M ./t_Ar Jty' 7/7
-. f
HP- '
-
r^f
jป
^
:;i'i
30
31
32
33
34
35
36
37
38
39
40
-^
42
43
44
45
46
17
48
49
50
51
52
53
54
55
50
57
58
59
TU-
CK)
fij
f.)
fj
ll/
IL'
K
A;
^
ฅ
pi
A/'
/
rl/
AJ
A/
ti
V
y
,t/
y
y
/t/y
,v
SLL
15
A;
/j
/J
*ซJ
^ป
/v
/v
V
V
A-
/I/
A/
V
/I/
y
v
/)/
y
v
A/
/I/
/!/
ca iii.vrs
-
-
,
,ป
*-' !
, *
-
i
i
'
i
t
i -'-'-'"
-------
Sumiary of Visible Emissions
Distance from Observer to Discharge Pennt:
of Observation Point: J"- ฃ-^l
c>-z^ -~l t
Tyf. i of Plant; /
Type of Discharge.
Location of Discharge; Kvtฃ <-e>*~y
Height of Point of Discharge: *.ฃ./ป*<** /pu'L*i Direction of Observer from Discharge Point:
- ix.. U i- - * I , , , ,, , r , x
Description of Background; Cu-4A*-lig t *
Description of Sky: dX<ซ_X-ซ
' ^O
Hind Direction;
Color of Plune: A-'U t)*.~_nL. PL~-~ซ_
Duration of Observation: 3 k-vi
SUWARY OF AVERAGE OPACITY
w_,
Hind Velocity;
Detached Plume:
j) t\
SUMI-UVRY OF AVERAGE OPACITY
Time Opacity Time Opacity
Set Nurroer Start End 5ira_ Average Set ilurrber Start End Sum Averaga
1
2
3
4
5
6
" 7
6
9
10
11
12
13
14
15
16
17
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19
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-------
RECOiY ur VISUAL
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RffOi't) 01 VJS.i'Lt L.USSIC S
COTpcMiy |'J(. C
Plant AdtJies
Stacl- Locntl
Weather Ccnd
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s ^ , _ V.1._' c: , 'u I Observer Q I1 /J^ii*-U^Uy
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33
34
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-------
RECOi D 0" VISIGLE t!IISS!OiS
,Data
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L-
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Stack Locclion
Weather Condit-ons
Observ
Location
.cr'v-r- f ( , f .,
lion Ltป & \- J ilo ( /hi'^-'H.
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00
01
02
03
04
05
06
07
08
09
10
11
12
13
11
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16
17
18
19
?0
21
22
23
24
?5
26
27
28
29
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-------
of visn i(
CoTpany ton 2
Plant Addles
Stack Locati
Keathcr Cond
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on > ^
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itions ^_VS
u Location //\i^fl- J//o ^Mjinu J.-<"
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30
31
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33
34
35
36
37
38
19
40
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42
43
44
45
46
47
48
49
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52
53
54
55
56
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Sun i.ia ry of Visible Emissions
-> '
Date; <
Typ? of Plane;
Type of Discharge: ^
Location of Discharge:
Height of Point of Discharge:
Description of Background:
Description of Sky:
Hind Direction:
Color of Pluma:
Duration of Observation: -i e^ '^
SUM-WRY OF AVERAGE OPACITY
Distance fro- Observer to Discharge Point:
L t U-vtk {
Height of Observation Point: -
/av-,jf Direction of Observer from Discharge Point:
Wind Velocity:
Detached Plume:
SUrU-WRY OF AVERAGE OPACITY
Time Opacity
Set MuToer Start End Sumr Average
T //,0-c* - !*ฃ 33 * 9^'
2 / / o o.- // M 3 ฃ j" , ssy *
3 // /i // / 7 ^ c u , ^3 i
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-------
Cgmp
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Plant /.dc'rsss O |">,-QI -e ( /
VT, J* /
Stacf Locct'ion K.c?*H V-^-i jV-ซ-r^
-------
UffOPQ Oh \} Si U \ L.HSSIOUS
Coppaivy tiau'a
Plant Aidics
/ r-t L. Date 7/^?y^ ^
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36
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43
44
45
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49
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-------
APPENDIX F
SAMPLING SUMMARY SHEETS
-------
I i
-'Plant Internationa 1 Minera Is and Chemica 1 s Corpora txon Location Spruce Pine, North Carolina
t ,r
'Sampled Source No, 2 Mill fiaghguse Outlet
,l Run
t
P-l
P-2
. e-3
Date
9/28/76
9/28/76
9/29/76
NP
20
20
20
Pro
2 ,32
2,06
1 ,82
Pl>
27 .23
27 .23
27 .22
Vm
105 ,631
100,848
93,551
T
Anv
119
129
116
v
mstd
SB .228
82 .743
78,^04
vw
32
34
37
Vwgas
1 ,507
1,601
1.743
7M
1 , 68
1 .90
2 .17
Md
0,98
0,98
0,98
i,
lun
T
. P-l
P-2
P-3
MWd
29
29
29
MW
28 ,78
28.78
28.78
?st
-0,12
-0,12
-0.12
P
s
27 . 11
27.11
27.11
CP
0. 839
0,839
0 .839
VaPBX(Ts+460)c
16,767
15.948
14 ,738
vs
2579
2453
2267
TS
105
115
103
TC
120
120
120
Dn
0,25
0.25
0.25
%I
100,1
100 ,5
100 ,8
100 H
f H*
_JlJi
H.ซ 100 'tM
* *^B3
0H (10,
11(1 -H
v, f 120.1.1 tp i / 4>~x i^
1.Q1I ป {T, ป *W1 i V.
N
9
m
fb
Vซ
Trt
ฅ_
P.*
V*
Toll) Ho, of Sampling PoliU
Drpfiป In- B,Q
liwwtrlc Pressure, In, (|).
Absolute
VfiluKe of Dry Gal *t Hctar
'^illlloni, DCF
AMrajo Hctaป" Teitpefilurj,
Voluiro of Dry Gil It &TP,
4 DStr
Toiil llS^CollecUd In IiMln-
gtrx'ind Sltlci Cel, il
Dry tUnJiJi'd cubic fuot it 4
* SUndJrJ condlCtoni il^'i7,
t *
m M ! .. i . ii . . . , .
Vw
I H
IC0|
ซซl'
1 CO
wd
|ar, zง,sz in.
Z9.9J in. Ilj.
Volwa of Witfg Ifipor ColJiel
1 Kali lure by Ynluw
Hull Friction si Dry til
Volunซ X Dry
Volume t Dry
Votiwe X Dry
Voluno 1 Cry
Hoi ecul ir Vtlght of Slick Oil
Dry Q*i Is
HaltcuUrVelght of Stick
Cu. Mil Dud
Kg.
P.. Suite Prmurt of Stick
11 cซt, In. H.J
I1 Slick Cii Prciiui't, (rt, !
Atl'-olult
C ' Pilot Tube Ccปrfltlint
If S?icl CM Vflucltj1 it Sli
Condition!, tfft
Stltk
"r
Kit Ttim of Ititi mo.
Koiclt
I I Nrctnt
TCO) 1ป tletarmlned by ซvorซf|lnj tha squsro Not if
pnil'-ct of ihu vjlocliy tiซid (&t>i) tnd Ihi
tatperilurn trn tuh ปtปpllnQ paint
-------
Plant International Minerals and Chemicals Corporation Location Spruce Pine, North Caroling
i
f
i
',,d
', >'*
{'
fซป
(-;
> '{
' {
ftป
Sampled Source Mo. 2 Mill Baghouse
1 ;
1
i
^
Kor
th Inlet
pu V
r D TO
27
,25 S0.3C
! Run MWd MW Pst Pg
P-l 29 28.78 -0.22 27.
03
i
/"7- 65 ป ฅ Ch * 'i \ ^w * *ซ ^o ToU' Na<
Cp V^
0 .838
of Stapling Podll
' (f * 46^5 L ^u t V
* Jld M ,. f,. Averige-DHMei PreJiuri
f flป Drop. 1ft. H20
t " * ' 100 b Wiiolute
i
V Voluปซ tt Orj Ctซ it BeUr
' 14 i i 3i i 78 '""dl llonii DCf
I. Averse Helor Teปftrtlซrซ,
J * tf * * V., Voluw Of Dr/ Cit ปt STP,
j piti oscr*
PtP - *. '
* ~ ll IL Totil lf,0 CoJJccltd ffi Icjin-
r i i V 5trj "^ ^"ca ^1< ''
. _ m.^ . ., I * i
Ilia, 1,1 cซ / ปP * [T( t 4ISJ |_Fง i WJ
ff *
t *
VT,. >,.<*(.}'
Cry ilindjrd cubic fit) it ฃ
lUndinl condltloni u^&'F.
^ป ซ
TV V V %H MJ
^m mstd * wgas d
1 US 67.065 ?.? 1,272 1.86 0,93
SX(TS+460)C Vs T5 Tt Dn XI
12.996 2000 103 120 0,250 98,1
V Volusa of yปUr Vipor CoHftLad r Suilc P/TiiKr* ซf Jtitl
511 it SIP, SCF * c*s. In, 113
I H S tatiturt by Valvn* P Sink tu Prcviui't, 1n.
Ab'.olnl*
Hj Mule Friction pf Bjy til
C ' Pilot fybt Crtfflsltnl
J C02 Volunซ $ Or/ P
V. Stick Cn Vtleclli1 il SI
1 0, Voluw X Dry lonilUont, fpi
j CO Yoli/ne C Dry ^ง ^vijfl Slit* Tcmpfrltilf
2 Hy Voluro I Dry
T. KH Tim of Tell, MIrt,
Wj Molecular ซซfปht cfllicl Olli l
Dry Dasll
P. liflpllAg Noizlt OlcuUl
>H HiUculir Wilghl of Stick tf . e^,
-------
'Plant Internationa 1 Miner a Is and Chemicajjs Corpora t ion Location Spruce Pine, North Carolina
r
^
\
f
i
Sampled Source No. 2 Mill Baghouse South Inlet
-i
i
'.Run Dace Np Pm Pb Vm Tm Vmgtd ^
P-2 9/28/76 20 2,4 27.25 106.937 127 88.198
>
Run MWd MW P t P C *y^p X(TS+460)C Vs
, P-? 29 28.78 -0.18 27.07 O.C37 11,004 169
'v vw %M Md
37 1,743 1,<4 0,98
Ts Tt D 7ปI
3 103 120 0.313 97.2
' /7ฃ5ป V ' ln> "zฐ Hd Hole Friction cf Dry
\.l "" ฐ^7/ ซ ป ^ 1M V K Pfc lirmtrlc Preiiura, In. Ig. , rn ,.
1
y
ซi
P( Jlitk Cn fititafw, 1n. Wj
til
C' Pllol Tu(iป CrtfneUnt
* ^00 ftbiolule i I-IV.-B ป vi/
t$ Stitk Cn Velocity il Stit
i V Voluna of Diy Git ซt K*lปr X 0, Voluw I Dry Condition!, f[ซ
fltO *' \t 110 " \ ( 1 Cfl + 1H \ " '"-'"(Jlltorl, OCF
2 VDO i IflO 2 103 j [5 VpJure I Drv ^ซ Awiofl StKi TcmfUriturf
T. <ซr(gc He lor Tenperปture, ปwi""o ป i/r/ f ,f
x "t r
HJ H ซ u n H \ * "z ^i" * Ory
-' d " VMwSfis"ia'fi<' "Jd w.c-uru.itf.i.fn.aou. Tt "ll TlB< " T"tr "'"
ซ! uj^r ซ p Juj^j
PU ป F.. *a D. Jinpung Won If OljauUr.
0 ~ ll V.. ToUl II,B CalUtttd In lป)ii\- a ,
, r 1 1 1/1 s=r* ซnd Sllfc* Del. il fW Holeculซr UMjht flT Itlck . t ป. . i ,. ,i
' ^^^tw IT 1 m ' .1 1 f\i Vet DAI^I ^ WfTlBl lutlMlIC
,tff ,
*- i Drj lUnijrd cubic fซl i*v8'ป Z3>SZ Ini Us-
n^> _ |v * flฃA\ b ^ f
i Ktt r ซ ซ4ป(or
iquare reot of
-------
APPENDIX
PARTICULATE WEIGHT DATA
-------
SUMMARY OF PARTICIPATE WEIGHT FRACTIONS
NO, 2 MILL BAGHOUSE OUTLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Test
NO.
1
, t
)
*>
3
Fra ct ion
Water Probe Rinse
Filter
Front-Half Total
Iinpinger Contents &
Back-Half Water Rinse
Total Particulate
Water Probe Rinse
Filter
*?._1irt'i s I1 n f*a 1
Impinger Contents &
Back-Half Water Rinse
Total Particulate
Mater Probe Rinse
Filter
1? i- s-h n 4- lljil f TrtHal
Impinger Contents &
Back-Half Water Rinse
Final
Weight
(gm)
98 -0907
0 .1482
87 .3930
93.2040
0,1628
91 .5397
95,7591
0.1434
88.t569
Tare
Weight
(gm)
98.0860
0 .1258
87 ,3885
93 . 2021
0 .1369
91.5367
95.7548
0.1261
88.8516
Weight
of
Particulate
(gm)
0 .0047
0 .0224
,
0 ,0045
0.0019
0.0259
0.0030
0.0043
0 ,0173
0.0053
Applicable
Blank
Value
(gm)
<0,0001
<0,0001
0 .0114
'
<0 .0001
<0 .0001
0 .0096
,
<0.0001
<0 ,0001
0.0072
Blank-
Corrected
Par t icula te
(gm)
0 .0047
0 ,0224
0.0271
<0 .0001
0.0271
0 ,0019
0.0259
A n 9 7 fl
i A
Clayton Environmental Consultants, Inc
-------
SUMMARY OF PARTICULATE WEIGHT FRACTIONS
NO, 2 MILL BAGHQUSE NORTH INLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Test
No.
>s
1
t
Fraction
Water Probe Rinse
Filter
Front-Half Total
Implnger Contents &
Back-Half Water Rinse
Total Particulate
Fina 1
Weight
(gm)
96.3448
1.1162
148.6669
101.7626
Tare
Weight
(gm)
94.8061
0.7889
94,3484
101,7594
Weight
of
Particula te
(gm)
1 .5387
0.3273
54,3185
0 ,0032
Applicable
Blank
Value
(gm)
<0.0001
0,0005
-
0.0073
Blank-
Corrected
Particulate
(eซ0
1.5387
0.3268
54.3185
56.1840
<0.0001
56 .1840
Clayton Environmental Consultants, Ine ,
-------
APPENDIX H
CALIBRATION DATA
-------
SUMMARY OF PARTICULATE WEIGHT FRACTIONS
NO. 2 MILL BAGHOUSE SOUTH INLET
International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
Test
No.
Frac tion
Mater Probe Rinse
Filter
iron.C"*MajLI JLOtax
Itnpinger Contents &
Back-Half Water Rinse
Totfll Particulate
Fina I
Weight
(gra)
92.1401
5.9924
94.7524
Tare
Weight
(sm)
91 .6736
0.8068
94,7497
Weight
of
Particula te
(sm)
0,4665
5.1856
0.0027
Appl iea ble
Blank
Value
(งm)
<0.0001
0 .0005
0,0076
Blank-
Correc lad
Particulate
Cgm)
0 ,4665
5.1851
S 6 S16
<0 ,0001
5 6516
Clayton Environmental Consultants, Ine
-------
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-------
GEORGE D, CLAYTON & ASSOCIATES
POTENTIOMETER CALIBRATION
Instrument No.-Pyrotest 73090015 Ifxniraite,
S cale-P>ro tes t .J 1-Iinimite
//?? / / a
<ฃ - 5"7 "73*J>
METER
STAHDARDIZ
TICK
ibratcd By
e
d June, Temp.
eut
o ces t
ding
100
200
300
400
500
600
700
800
f 900
1000
1100
1200
1300
1400
1500
1600.: \ "' .
. -^T j*k "* - *ป *~"*T"tJ*T"r'SJ*' **^L
isoo -:'
^.ZrV/
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77-*
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Minimi te
Reading
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OF
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.
-------
GKQRGF, D, CLAVfOn & ASSOCIMES
POTENTI011ETER CALIBRATION
Instrument llo.-Pyrotc.st 73090015 llininitc s??c x? ฃs.- 3/ / o /
S ca le-Pyro tcs t ^ t.iriuii ce ^'/g
METER
STANDARDIZATION
Lbratcd By
^
1 June. Temp.
int
ites t
ling
ฐF
100
200
300
400
500
600
700
800
900
1000
1100
1200
1300
1400
1500 -
1600 '"-^"
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-------
APPENDIX I
EXAMPLE CALCULATIONS
-------
Nomencla ture
o
AS = Stack area., inches
Cf = Front half (probe 6. filter) parfciculate concentration3
gr/DSCF
Cp = Pitot tube correction factor, dimensionless
Ct = Total particulate concentration, gr/DSCF
CMf = Front half (probe & filter) particulate concentration,
CM^ = Total particulate concentration, m
Dn = Sampling nozzle diameter, inches
ERf = Emission rate of front half particulate, Ib/hr
ERt = Emission rate of total particulate, Ib/hr
ERMf = Emission rate of front half particulate, kg/hr
ERMt = Emission rate of total particulate, kg/hr
Mjj = Mole fraction of dry gas, g/g-mole
MW = Molecular weight of wet stack gas
MW, = Molecular weight of dry stack gas
p, = Barometric pressure, inches mercury
P = Average orifice pressure drop, inches water
P = Absolute stack gas pressure, inches mercury
Pgt = Static pressure of stack gas, inches mercury
Q = Dry stack gas flowrate at standard conditions, DSCFM
SWf = Front half sample weight, mg
SW = Total sample weight, mg
Tm = Average meter temperature, ฐF
TS *= Stack temperature, ฐF
Tฃ = Net time of test, minutes
Vm ~ Vo^ume ฐf ^ry Sas at meter conditions, ft^
-------
V = Volume of dry gas at standard conditions, BSCF
s td
Vs = Stack gas velocity at stack conditions, fpm
Vw = Total condensate collected in sampling train, ml
V., = Volume of water vapor at standard conditions, SCF
"gas r *
AP - Velocity pressure, inches water
%I - Percent of isokinetic variation, dimensionless
%M = Percent moisture, dimensionless
Calculation of Particulate Emissions
The dry volume of sampled gas corrected to standard condi-
tions of 20ฐC and 760 mm Hg (29-92 in, Hg) is calculated as fol-
lows ;
V = 17.65 * Vm * Pb
T + 460
m
The sampled volume for the first particulate test taken on the No.
2 Mill Baghouse Outlet at the International Minerals and Chemicals
Corporation is:
2,32
v 17.65 (105.631) [27.23 '
mstd
/
[27.
(119 + 460)
= 88.230
The dry stack gas flowrate corrected to standard conditions is
calculated using the following set of equations sequentially;
Vw = 0.0471 * V
gas w
100 * Vw
7aM . _^ 8"
-f V
wgas
100 - TM
MW,
(7.C02 * 44/100) + (%02 * 32/100) + [(%CO + %N2)*28/10o]
-------
- 3 -
MW = (KW * M) + 18(1 -
d
Pb + Pst
*-J L
I 5
V = 5120.8 * C *1/AP * (T + 460) ..
s p V s s ' V p * MW
0.1225 * V * A * M * P
Q a s s d s
S -_ _ _ -| __ __^-__! ___ _ _ - - - - - - - _
T + 460
S
The calculations for determining the flowrate for the first
particulate test on the No. 2 Mill Baghouse Outlet follow. This
sampling location has a 19-inch interior diameter.
V - 0.0471 (32)
w
gas
= 1.507
100 * 1.507
88.230 + 1 ,507
1.68
100 - 1.68
= -
d 100
ซ 0.98
MWd ซ= 29 (Because this is not a combustion source, MW^ is
assumed to be the molecular weight of air.)
MW = (29 * 0.98) + 18(1 - 0.98)
= 28.78
P^ = 27.23 - 0.12
S
= 27.11
V = 5120.8 (0.839) (16.767) ,,
s I/ 27.11 (28.79)
r - = 2579 ' ' -
-------
= 0-1225 (2579) (283.5) (0.98) (27.11)
(105 4- 460)
= 4210
The equation employed to determine percent of isokinetic
variation is:
1032 * (T, + 460) * V
Vs * Tfc * Ps * Md * (Dn)2
For the first particulate test taken at the No, 2 Mill Baghouse
Outlet j
1032 (105 + 460) (88.228)
Ja J EJ II
(2579) (120) (27.11) (0.98) (0.25)2
= 100.1
To determine the concentration of particulate matter in
grains per dry standard cubic foot (gr/BSCF), one of the fol-
lowing equations is used;
SWf
Cf = 0.01543 * and
rastd
SWa.
C,. = 0.01543 *
Jte v W -** J ^' -^ _-_ f
mstd
When metric units are desired, the concentration is calcu-
lated in milligrams per dry normal cubic meter (mg/DSm3) as fol-
lows ;
SWf
CMฃ = (0.02832)(Vm .) and
CM
t (0.02832)(V )
mstd
-------
Front half particulate concentrations are obtained by summing the
weight of particulate matter collected on the filter and all por-
tions of the train preceding it. Total particulate concentration
includes, in addition, any particulate matter collected in the
impingers.
The first particulate test taken at the No. 2 Mill Baghouse
Outlet yielded the following concentrations of filterable and
total particulate;
27.1
Cf = 0.01543 *
r 88.2
= 0.0047
27 .1
C,. = 0.01543 *
88.2
= 0.0047
27.1
CMf * (0.02832)(S3,2)
ซ 10 .8
27.1
CMt ** (0.02832) (88 .2)
= 10.8
The emission rate of particulate matter can be calculated
from the filterable or total particulate concentration using one
of the following equations:
ERf = O.OOS57 * Cf * Qs and
ERt = 0,00857 * Ct * Qs
For metric units,
ERMf = (1.70 * 10~6) * CMf * Qs and
ERMfc ป (1.70 * 10~6) * CMt _* Qs .
-------
- 6 -
To avoid rounding errors it is preferable to carry out the calcu-
lation of concentration and emission rate in one operation.
The emission rates of front half and total particulate matter
for the first test taken at the No. 2 Mill Baghouse Outlet are
calculated as follows:
ER = 0.00857 (0.0047) (4210)
ป 0.17
ERt = 0.00857 (0.0047) (4210)
= 0.17
ERMf = (1,70 * 10~6) (10,8) (4210)
- 0.08
ERM = (1.70 * 10"6) (10,8) (4210)
" 0.08
-------
DRAFT/WP
d3006-4/971130
03/30/92 1
"RATES/
Emission Test Report
Review Checklist
Reviewer :
Review Date:
A. Background Information
l. Facility name:
Location:
7.
pi
int
Source category:
Test date:
Test sponsor:
Testing contractor:
6. Purpose of test: P
-------
DRAFT/WP
d3006-4/971130
03/30/92 2
B. Process Information
1. Provide a brief narrative description of the process.
With as much detail as possible, (e.g., if a furnace or
conveyor system is used, identify the type of unit)
describe the equipment used for those operations tested.
(Note: If process description provided in test report is
adequate, attach copy or reproduce herej
'"
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DRAFT/WP
33006-4/971130
03/30/92 3
2. For each process tested list feedstock materials and
products. Indicate if activity factors are for feed (F)
rate or product (P) rate.
Process ID
A
Feedstock materials
Products
Basis for activity
factor
F/P
Basis for data:
(Indicate page/table Nos. in test report)
3. For each process or operation tested and each test run
note process capacity and operating rate during test.
Process ID
Capacity
Units
Test run
I
2
3
4
1
2
3
4
1
2
3
4
1
2
3
4
Process rate
Urals
Basis for data;
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DRAFT/WP
d300-4/97H30
03/30/92 4
C. Air Pollution Control Systems Tested
1. For each air pollution control system pollution control
system identified in A.8, note the following
ID
Type of APCD
Manufacturer
Model No.
Note: Be as specific as possible in identifying APCD. For
example, indicate "pulse jet fabric filter" rather than simply
"fabric filter."
2. For each system identified above, provide a narrative
description. For fugitive systems describe capture
techniques as well as the removal techniques (use a
separate page if necessary)
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DRAPT/WP
33006-4/971130
03/30/92 5
3. Using the attached parameter list for guidance complete
the table below. (Use additional pages as needed.)
APCDID
Type of
APCD
Type of
APCD:
Type of
APCD:
Parameter
Unita
Readings
Run 1
Run 2
Run 3
Run 4
"
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DRAFT/WP
(33006-4/971130
03/30/92 6
D. Sampling and Analysis Methods
1. Complete the following table
Test location
Pollutant
SSt A method
Reference/
conditional
method
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Deviations
noted
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
Y/N
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DRAFT/WP
(13006-4/971130
03/30/92 7
2. If a method used was not a reference or conditional
method, provide a narrative discussion including any data
manipulation needed to make results correspond to
reference or conditional method results.
3. Describe any deviations identified above,
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DRAFT/WP
33006-4/971130
03/30/92 8
B. Emission Data Documentation
1. Tabulate the following stack gas data from the test
report^ (Use additional pagea as needed,)
TestID
Parameter
Stack temperature
Moisture
Oxygen
Volumetric flow, actual
Volumetric flow, standard
Percent isokinetic
Units
Values reported
Run 1
Run 2
Run 3
Run 4
Pollutant concentration;
Stack temperature
Moisture
Oxygen
Volumetric flow, actual
Volumetric flow, standard
Percent isokinetic
Pollutant concentration:
Stack temperature
Moisture
Oxygen
Volumetric flow, actual
Volumetric flow, standard
Percent uolcuifitic
Pollutant conccntrub on:
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DRAFT/WP
33006-4/971130
03/30/92 9
2. Tabulate pollutant mags flux ratea
Test ED
Pollutant
Units
Run L
Run 2
Mass flux rates
Run 3
Run 4
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DRAFT/WP
d3006-4/97H30
03/30/92 10
3. Present example emission factor calculations below.
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DRAFT/WP
d3Q06-4/971130
03/30/92 11
4. Tabulate emission factors
Procesi
Pollutant
Ualts
Avenge emission factor
Uncontrolled
Controlled
b3006-4/971130
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