project NO.
  CD


O
      AIR  POLLUTION
      EMISSION  TEST
         INTERNATIONAL MINERALS AND

            CHEMICAL COMPANY

           SPRUCE PINE, N, C.


UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
      Office of Air and Waste Management
    Office of Air Qualify Planning and Standards
        Emission Measurement Branch
     Research Triangle Park. North Carolina

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                 EMISSION STUDY

                      a t a

     FELDSPAR CRUSHING AND GRINDING  FACILITY
International Minerals and Chemicals  Corporation
           Spruce  Pine, North Carolina
              September 27-29, 1976
                Prepared for  the

      U.S. Environmental Protection  Agency

                       by

     Clayton Environmental Consultants.,  Inc.
              25711 Southfield Road
          Southfield, Michigan    48075
                  Project NMM-1

                     Task 25

             Contract No. 68-02-1408

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                                                             P.a.g e


I.      Introduction  ...... .•..,,,.,,•.,...•.,...<....,,      1

II.     Summary and Discussion  of  Results  ..,..,ป,...,..      2

III.    Process Description  and  Operation  ..... . T .......     30

IV,     Location of Sampling Ports ............. ....... ป     31

V.      Sampling and  Analytical  Procedures ..............     36


FIGURES

FIGURE 1  Location of Visible Emissions  Observers
            Feldspar  Mine,  September  27,  1976 .... ......      5
FIGURE 2  Location of Visible  Emissions  Observers
            Final Hilling  Plant,  September 28-29, 1976 .       6

FIGURE 3  Particle Size Distribution,  No. 2 Mill
            laghouse North Inlet  ................ ..... ,.      28

FIGURE 4  Particle Size Distribution,  No. 2 Mill
            Baghocse South Inlet  ..... ........... , ......      29
                                                             v
FIGURE 5  Sche— atic Diagram  of Baghouse  Inlet and Out-
            let Ducts, No,  2 Mill Baghouse ...... .......      32

FIGURE 6  Schematic Diagram  of Sampling  Point Locations
            No. 2 Hill Baghouse Outlet  .................      33
                                                             ซ
FIGURE 7  Schematic Diagram  of Sampling  Point Locations      *
            No. 2 Mill Baghouse Horth  Inlet ..,„,,.,ป...      34

FIGURE 8  Schematic Diagram  of Sampling  Point Locations
            No. 2 Mill Baghouse South  Inlet ............      35

FIGURE 9  Schematic Diagram  of Particulate Sampling
            Train, No. 2 Mill  Baghouse  Outlet ..........      37

FIGURE 10 Schematic Diagram  of Particulate Sampling
            Train3 No. 2 Mill  Baghouse  North and South
            Inlets ...... ........................ . ..... .      38

FIGURE 11 Schematic Diagram  of Particle  Size Sampling
            Train, No. 2 Mill  Baghouse  ....... . .........      39


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                              - 11 -
                                                              Page
TABLES




TABLE I         Summary of Particulate Emissions  (English
TABLE
TABLE
TABLE
II
III
IV
Summary of Particulate Emissions (Metric
Units), No. 2 Mill Baghouse 	 	


4
8
26
APPENDICES




APPENDIX A   Project  Participants




APPENDIX B   EPA  Draft Method 17




APPENDIX C   Particulate  Field Data Sheets




APPENDIX D   Particle  Sieing Field Data Sheets




APPENDIX E   Visible  Emissions Field Data Sheets




APPENDIX F   Sanplir-  Summary Sheets




APPENDIX G   Particulate  Weight: Data




APPENDIX H   Calibration  Data




APPENDIX I   Example  Calculations

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                         I.   INTRODUCTION

     The U.S. Environmental  Protection Agency  (IPA)  retained Clay-

ton, Environmental Consultants,  Inc.  to conduct  a  series of emis-


sion tests at the International Minerals  and Chemicals  Corporation

facility located at Spruce Pine,  North Carolina,   The purpose of

this study was to provide the Environmental Protection  Agency with
                                   •9

data for the establishment of source  performance  standards for the


non-metallic mineral-processing industry.  This study was commis-

sioned as Project NHM-1  of Task 25;  Contract No.  68-02-1408.

     The International Minerals and  Chemicals  Corporation facility

is a feldspar crushing^  grinding,  and milling  operation.   Fugitive

dust generated at each step  in  the crushing and grinding  operation

is collected by reans of a system  of  dust  recovery hoods  and routed


through separate exhaust ventilation  systems leading to two bagftouses
                                                                f
for capture and recovery of  feldspar  dust.
                                                             i
     Source sampling was performed on the  No.  2 Baghouse  at the

final milling plant where feldspar powder  is produced by  a ba,^.! '*"
                                                             *^
mill.  Particulate and particle sizing samples were  taken at the

baghouse inlet ducts and the outlet  stack  by personnel  from Clay-

ton Environmental Consultants,  Inc.   U.S.  EPA  personnel made opacity

readings of the baghouse outlet stack as well  as  the fugitive dust

generated at several locations  within the  plant at feldspar crushing

and grinding operations.  In addition, EPA personnel observed the

source testing activities and monitored process operations.

     This study was conducted during  the week  of  September 26, 1976.


Appendix A lists the project participants.

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                                - 2 -






               II.  SUMMARY AND DISCUSSION OF RESULTS




  Particulate Sampling Results




       Tables I and II summarize the results  of the particulate




  sampling at the baghouse inlet and outlet in English and metric




  units,  respectively.  Both filterable  and total  particulate emis-




  sion  rates measured at the outlet averaged  0.16  pound per hour




  for  the three tests and ranged from  0.14 to 0,18 pound per hour.




  The  north and south inlet loadings were  140 pounds per hour and




  14,6  pounds per hour, respectively,  for  both filterable and total




  particula te .




       A  comparison of the average total  inlet and outlet volumetric




  flowrates measured during particulate  testing indicates that the




  average outlet flovrate is significantly higher,, 3960 dry standard




  cubic feet per minute (DSCFM), than  the  total inlet flowrate of




  2930  DSCFM.  Since the baghouse was  under negative static pressure,




  this  difference izipi^es the possibility  of  air leakage into the




  baghouse, possibly through the collection hopper beneath the bag-




  house.   The suspicion of air leakage  into the baghouse is further




  supported by the initial velocity traverse  data  which indicated a




  total inlet airflow of 3260 DSCFM and  an outlet  flowrate of 4180




  DSCFM.






  Visible Emissions Observations




       Opacity measurements were taken  during the  study by two




  certified opacity readers provided by  che U.S. EPA,  Measurements




  were  taken at several locations at the  feldspar  mine on September




 .27,  as  shown in Figure 1.  Readings  were taken at the final milling




r  plant at the sites shown in Figure 2 "on  September 28 and 29 In con-




•Vi-junction with source testing activities.
--^i—i   ..

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                     TABLE I

SUMMARY OF  PARTICULATE EMISSIONS  (ENGLISH UNITS)
               NO. 2 MILL  BAGHOUSE

International Minerals and Chemicals  Corporation
           Spruce Pine, North  Carolina
              September 27-29,  1976
'' ,
f
•i>
Ba ghouse
Outlet
', > i
<*
'^r "
t '
i i
Ba ghouse
, North
' Inlet
1 1 '
<
Bflghouse
South
Inlet
Test
No.
1
2
3
1976
Date
9/28
9/28
9/29
AVERAGE
1
2
9/28
9/28
Stack Gas
Conditions
Temp
(ฐF)
105
115
103
108
103
103
Fl owra te
ACFM
5070
4830
4470
4790
1520
2070
DSCFM
4210
3940
3720
3960
1260
1720
Pnrt-iculate Concentration
I'ilLerabif
gr/ACF
0.004
0.004
0.004
0 .004
10.7
0.823
gr/DSCF
0 .005
0 .005
0.004
0 ,005
12 .9
0.989
1 o t a 1
gr/ACT
0.004
0.004
0 .004
0,004
10.7
0.823
gr/DSCF
0.005
0.005
0,004
0 .005
12.9
0 .989
Pa r ticula te
Emission Rate
(Ibs/hr)
Filterable
0.17
0 .18
0.14
0.16
140
14.6
Total
0.17
0.18
0,14
0.14
140
14 .6
                                                                              I
                                                                              LO

                                                                              I
                             Clayton Environmental Consultants,  Inc.

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                    TABLE II

SUMMARY  OF  PARTICULATE EMISSIONS  (METRIC  UNI1S)
               NO.  2 MILL  BAGHOUSE

International Minerals and Chemicals Corporation
          Spruce  Pine,  North Carolina
              September  27-29, 1976
' 1 1* ,
Sampling
Location
'[, '
1 -;
i i
Baghouse
Outlet
r
t >
Baghouse
North
Mnlet
I t
Baghouse
South
Inlet
Test
No.

1

2

3
1976
Date

9/28

9/28

9/29
AVERAGE

1



2


9/28



9/28

Stack Gas
Cond i tions
T omn

41

46

39
42

39



39

Flowra te
Am3
mln
144

137

127
136

43



59

min
119

112

105
112

36



49

ParLiculate Concentration
Filterable

m g / A in
9

10

8
9

24,600



1880

tnn/DSm3
11

12

10
11

29,600



2260

Total

mg /Am
9

10

8
9

24,600



1880

mg/DSm
11

12

10
11

29,600



2260

Pa rticula te
Emission Rate
(kg/hr)
Filterable
0,08

O.OS

0 ,06
0.07

63.3



6.61

Total
0,08

0.08

0 .06
0.07

63 .3



6.61

                            Clayton Environmental Consultants, Inc.

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                 LOCATION OF VISIBLE  EMISSIONS  OBSERVERS
                               FELDSPAR MINE
                             SEPTEMBER  27,  1976

             International Minerals arid Chemicals Corporation
                        Spruce Pine,  North Carolina
                              TP-2
                                 Se conda ry
                                   Crus neif
     Secondary Crus'rer
                          a .m.
     'rirnary  Crusher
    a .in. .
         KEY

     ~  Observer Location.
     -  Transfer Point
UGT --  Underground Transfer

r  -] -^Conveyor
r(50
 TF
                                     TP-5  ,
       -*-.
       j j-
                                      Clayton  Environmental  Consultants, Inc
                                                           - i >.& •7'a-*'s**ฃn. ***
                                                     *v^-^-Ji.'ii.*i";. '" -^ซ"-. ^

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ฎ South
Wall
9/29
a .m ซ
<• ~v t * i'
ซ• (i;.;a Im. '-/


• ,. <*"$*, . , f
L^ ' .East '*•

TP-5
9/28
Ball
Mill
Feed



/
/














u

f

North
ฎ Wall
9/29
P. p.m.
"T
	 _.._T
TP-3
9/28
Elevator
TP-4
9/28
Ba ghouse
fP-2
9/28




[



Outlet
O Stack
i 	 |TP-1
U/og
1 | "; -ฐ







     LOCATIONIiOF VISIBIE EMISSIONS OBSERVERS
             *
Loading
 9/29
             *ซ, FINAL MILLING PLANT
              SEPTEMBER '28-29,  1976
International Minerals and Chemicals Corporation
           Spruce  Pine,  North Carolina
                 - Observer Location

              TP - Transfer Point

             \| - Conveyor

Clayton Environmental Consultants,  Inc

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                               - 7 -
     Each observer  took a reading once  every  15  seconds during  the

observation period.   Readings were  summed  and  averaged for each

six-minute period and plotted versus  time.   The  series of six-

minute averages  and  the corresponding  plots  are  presented for each

site in Tables  III-l  through 111-17.

     Tables III-l through III-6 represent  measurements taken

at various sites within the mining  and  crushing  operation.  These

sitesj depicted  in  Figure 1, included  the  primary crusher, the

secondary crusher,  and conveyor transfer  points  TP-lj TP-2, and

TP-4.

     No visible  e-iissions were detected  in this  area except at

the primary crusher  site, and these positive  values comprised

only four to  six percent of the trea suremen ts  taken at the primary

crusher site.   As presented in Tables  III-l  and  III-2, these posi-
                                                                 >
tive measurements contributed to  the  two  positive s ix-minute* avera ge

values that,  in both  cases, were  less  than  one percent.  The max-

imum reading  recorded by either observer  at  this site was five
                                                              ,s-  •'
percent.                                                     **1

     Tables III-7  through 111-17  apply  to  milling plant operations.
                                                                  >,'
Opacity readings were taken at the  following  locations shown in  , ''

Figure 2:  baghouse  outlet stack, roof  and  four  plant vbuilding

walls  (fugitive) , feldspar loading  silos.,  and  five product trans-

fer points within the milling plant,labeled  TP-1 through TP-5.

     No visible emissions were observed  from  the baghouse outlet

stack, the in-plant  transfer points,  or  the  plant building walls.

All visible emissions generated at  the  feldspar  loading silos were

of five percent opacity or less.  A white-grey fugitive plume of

-------
                                TABLE III-l

                        SJM11ARY OF VISIBLE EMISSIONS

              International Minerals and Chemicals  Corporation
                         Spruce Pine, North  Carolina
late; 	  9/27/76
'ype  o f~ D i s"e h a r g e :  Primary C rlis h e r
 eight  of  Point of Discharge- 10-30'
 ind  Direction'  	NE	
 alar of  Plume:      "No visible plume
'bserver  No..    '          1     	_
listance  from Observer  to  Discharge
lirection  of Observer from Discharge
leight  of  Observation Point-
lescription  of Background;
                                                              IMC Feldspar
                                                      Sky ,
Partly Cloudy^
0-10 m i / h r
 Type of Plant: 	
 Location of  Discharge:  PrimaryCrusher
 Description  of
 Uind Velocity,
 Detached
 Duration
P o in t:  	
 Point;
                                                Plume'  	
                                                of Observation,
N/A
    1 hr
                                                            a pprox.  LOO
                                                            Ground leve1
                                          Quarrywalland equipment structures
SUMMARY Or AVERAGE OPACITY
Set
Nunber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tine
Start
09 30
09:36
09 42
09-48
09- 54
10 00
10 06
10 12
10 18
10 24









End
09, 36
09. 42
09 48
09 54
10 00
10 06
10 12
10:18
10; 24
10. 30









Opฃ city
Sur.
V1
"*>
11



N
^
*
^
!•>









Average
N
N
K
N
N
K
K
N
0.2
N









Set
Numb er
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Stare



















End



















Opac ity
Suin






^





9






Average






'




X
• r-






Sketch Showing How  Opacity Varied With Time:
 Opacity
"if--*
&
. i
r * l
A i
-' 7 •
"V,~
'T

,- _ "
rt,T^
-;'-: -
-


*,
~ y ''*.ซ„'
^




, - '
._.



~
aj._




-
_~"'f
T V ^



—

.- --




'_
--.*•?"



-
"* ' '"' W " ,
l""-"1 ,'




- -•"
J .



;;_-'


—


...
" ^
;- . ,"
^ -^



JlA^*
*• .- "XT

:>- .y/i^r-^- ^.j't'-^r..^^! - 1,ซ Time," hours ' '"^ ^ J.^~/l.,'^ ^""l "y^-"*"- ^"~

-------
                                     -  y  -
                                 TABLE  III-2

                        SU1IMA3.Y  0? VISIELE EMISSIONS
             International Minerals
                         S pruce  Pine
                  and  Chemicals Corporation
                  North  Carolina
Date:  _
Type of
      9/27/76
Primary Crusher
                    	NE
                    No visible plume
                       2
                                                                IMC  Feldspar
        Discharge	
-[eight of Point  of  Discharge; 10-30
/ind Direction:
Holor of Plume:
Dbserver No.: 	
Distance from  Observer to Discharge
Direction of Observer  from Discharge
{eight of Observation  Point:         _
Description of Background-	
 Type of Plant:	
 Location  of  Discharge: Prima'ry" Crusher'
 Description  of  Sky:     Partly Cloudy
 Wind Velocity; 	   0-7 mi/hr
 Detached  P1 uir e:            M / &
 Duration  of  Observa txon;   I Fir,        '
Point: 	
 Point:
                                                           approx_.  100
                                                            100'  SSE
                                                            Ground  level
                                                      Equipment  strucCure
SUMMAR.Y OF AVERAGE OPACITY
Set
Kuraber
1
2
3
4
5
6
7
S
9
10
Time
Start
09-32
09 38
09 43
09 50
09 56
10- 02
10.08
10 14
10- 20
10. 26
11 i
12

13
14
15
16
17
18
19
20







End
09 37
09 C3
09- 49
09 55
10 01
10- 07
10-. 13
10: 19
10: 25
10, 30










Opa ci ty
S v~i
N
N
N
N
N
V1
\
N
15
N










Avera ge
N
N
N
N
N
N
N
N
0,6
N










Set
F umber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start




















End




















Opa ci cy
Sum












4







Average





s





f'
*?







.ketch Showing  How  Opacity Varied Uith  Time:
Opacity
(7.) 8
-v . '" |


.,.- t^iiL.,.-* ~-



~.~'
:ป•?'*



-
-„





--




-"
, - -
-I-*"*-

0 Ji~_— — - --,'-, ' '


-_
~_ ' -
1
J



-
4"^'
.^



.
: -
* "?



* ' •' *
'--
-ซ-_ ^_



i-
^
'^



—-
-
^



t
-'- -, ~^-
, f'~



'„.
'*.
" **- >

. --_-._ 2 - ' -- -
if
-tฃ.

-------
                               TABLE  III-3

                               0V VISIBLE EMISSIONS
ate :
ype of
            International Minerals
                       Spruce  Pine

                     9/27/76
                                    and  Chemicals Corporation
                                   ,  North  Carolina
                 		NW
                 No visible  plume
       Discharge. Secondary  Crusher
eight of Point  of  Discharge:10-20'
ind Direction:
olor of Pltme:  		        	
bserver No,: 	__2	
istance from  Observer  to Discharge
irection of Observer from Discharge
eight of Observation Point; 	
escrxotion of Background,
 Type of Plant:	IMC  Feldspar
 Location of  Discharge  Secondary Crusher
 Description  of Sky;  Partly  C1oady-CIoudy
 Hind Velocity:       0-7 mi/hr
 De tached
 Duration
Point; 	
 Point;
Plume; 	N/_A_
of Observation:
                                                                 1 hr.
                                                           a p pr ox.
                                                           a pprox,
                    75'
                    TT"
SSB
                                                           Ground level
                                                         Equipment Structure
SUMMAE.Y OF AVERAGE OPACITY
Set
iuraber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
10 41
10' 47
10 53
11 45
11- 51
11: 57
12 03
12 09
12 15
12 21
12: 27
12 ;33
12; 39
12:45






End
10.46
10 52
10 53
11 50
11- 56
12 - 02
12, 03
12. 14
12" 20
12. 26
12 32
12: 38
12.44
12:50






Opacity
Su-
V
•*,-

.ป
-1
\
1
%
•v
*-
^
„•*
s
N
N
N






Av e r a g s
N
K
N
N
N
K
K
N
K
K
N
N
N
N






Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start




















End




















Opa city
Sxizi






m,





ซ







Average






jf

*••


*^*
••,.' '







ketch Showing  How Opacity Varied With  Time;
Opacity
   it i

. r
f.
"?
*#*&,ฃ
>. r|



*- jr "-
.- „- '




z.
_1-.



,
j j
ป ** v

•


~_L—
- •- !




_ J —




'A
^,^- -r
.'i


.

w*a *- ~
i
-

*
^ , ป
- i'*~ '"




I
e; i-
p
_


''"_
-v(J_
.



s~
> J'~1




'. ~
1 - • —

-v u^ -i,_ v,.*t~" - _^ - ^-_^ ^ ^ f_. ?„!* Time 5 hours - , -v,f-"";v,— . "--.— U4 ^-^?-

-------
                                 TABLE III-4

                        SUHHARY  OF VISIBLE EMISSIONS

             International Minerals and Chemicals  Corporation
                         Spruce Pine3 North Carolina
 ate:	 9/27/76
 ypa of Discharge-  Convenor Transfer
[eight of Point of DischargeHP
   If                           ^__~__
 ind Direction:                 NE
 olor of Plums.    No  visible plume
)b s erver No . :            1
                         IMC Feldspar
Type of Plant'  _  	
Location  of  Discharge-  TP-1	
Description  of  Sky      Overcast
Wind Velocity;  	    0-5 miThr"
Detached  Plume:N/A
Distance  from  Observer to Discharge Point:
Direction of  Observer from  Discharge Point;
leight of Observation Point: 	
jlescription of Backgroand,^	
Duration  of  Observation: approx. 1-1/4 hrs.
                  approx ,
                          50 '
                  SE
                  Ground 1 eve 1
                  Qua rry Wa11
SUMMARY OF AVERAGE OPACITY
Set
Eutnber
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Time
S tart
10:41
10,47
11 45
11- 51
11:57
12; 03
12 09
12 . 15
12, 21
12 27
12-33
12, 39
12-45







End
Opacity
Sun
10.47; N
10 53) N
11 51, *
11- 57
12 03
X
X
•
1 2 - 0 9 1
12 15
12 21
\
\
.
-------
                                TABLE III-5

                       3J?i!lARY  OF VISIBLE  EMISSIONS

             International Minerals and Chemicals  Corporation
                        Spruce Pine, North  Carolina
                          9/27/76
late: _
'yps  of  Discharge: Conveyor Transfer
[eight  of Poxnt of Discharge:
'ind  Direction:    |
tolor of Plume:
                                                   IMC Feldspar
                                                               TP-2
                               40'
                               NMW
                    No v 1 3 1 b 1 e p 1 urn e
Ibserver  No.:             1 _
listaBce  front Observer  Co  Discharge
Hrection of Observer from Discharge
leigbt  of Observation Point'
(escr ip t ion
 Type of Plant; 	
 Location  of  Discharge  	
 Description  of Sky:  P a r 11 y C1 o od y - Qv e r c"a s t
 Wind Velocity;       0-10 mi/hr
 Detached
 Dura tion
Point;	a pprox .  50 '
 Point;
                                               N/A
Plume:
of Observa tion:appr ox . 1-1/2 hrs.
of Background:
                                                               SE	
                                                               Ground level
                                                               Quarry wa11
       S  U M M A R Y
                         0
                    AVERAGE
             0  P A C I T
Sat
Number
1
2
3
t,
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
13. 17
13 23
13. 29
13' 35
13,41
13 47
14-08
14- 14
14, 20
14: 26
14:32
14:38
14:44
14:50
14:56





End
13 23
13 29
13 35
13 41
13 47
13 52
14 14
In 20
14. 25
14: 32
14: 38
14:44
14:50
14:56
15:00





CDacity
Su-
K
*ซ
*;
_\
N
\-

..
V
_i
i
N
N
N
N





Avera ge
N
N
N
N
N
K
N
N
N
N
N
N
N
N
N





Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tir>e
Start




















End




















Op a city
S uo






-





f







Average






•




if*
rV







Iketch Showing How Opacity  Varied Vith Time-
Opacity

                                           ™  *    "
                                           ,  hours

-------
                                TABLE III-6

                       SUIKIARY  OF VISIBLE EMISSIONS

            International  Minerals and Chemicals  Corporation
                       Spruce Pine. North Carolina
                        9/27/76
>ate:	
'ype  of Discharge:ConveyorTransfer
leight of Point of  Discharge;  1Q '
7ind  Direction: 	N	
'olor of Plume. 	No visible  plume
Ibserver No.: 	2.	
)istance from  Observer  to Discharge
Jirection of Observer  from Discharge
teight of Observation  Point-
Description of Background-	
IMC Feldspar
                                                               Cloudy
                                                               0-7 mi/nr
 Type of Plant   	
 Location  of  Discharge:  IP-4
 Description  of  Sky;
 Wind Velocity:  	
 Detached  Plume:
 Duration  of  Observation.- approx. 1 hr
Point: 	       '        "
 Point:
                                                            N/A
                                                            approx. 75
                                                            a pprox.  75' SE
                                                            Ground level
                                                            Cliffor Wall
S U M M A Pv Y OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
,6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tine
S tart
13 18
13 24
13 30
13 36
13,42
13:48
14 11
14- 17
1 4 ; 2 3
1^ 29
14, 35
14.41
14-47
14: 53
14-59





Ooa c i ty
End S u~i
i
13 23
13 29
13- 35
13 41
13-47
13 51
14 16
14; 22
14: 29
14. 34
14 40
14:46
14; 52
14: 58
15; 01





N
V
N
.N
•\
il
,.
Oi
N
:s
N
N
K
N
N
N
N





Ave rage
K
K
N
N
N
N
N
N
N
N
K
N
N
N
N





Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start




















End




















Opa city
Sun












1







Average






-F




(V
t}







ketch Showing  HOT? Opacity  Varied Uith Time:
Opacity
y 8
6
4 i

^r ~ *


„_
~t- t!~
1 1;^-
,



-





	





- _





„-- -
v^-




-
'



-_,
"'=-""
1 - J


,
'„-
^-_

0 Jff^- •jT'™^- j^-w~ J^?7-^ 	 '-rr"5.r_ 1 — -^Xmi-- """^C 	 ^-"wvr— ->



^ ^J
-



^
V-
"--*




1.
> , .




e
"-*- ?

-•"ฃ'- "ir~ ~-*^-,i^fe-^-1^.-?---- '->-

-------
                                TABLE  1II-7

                       5J711IARY  OF VISIBLE EMISSIONS

             International Minerals  and  Chemicals Corporation
                        Spruce  Pine, North Carolina
ate; 	 9/28/76
ype of Dis charg e.  0a tie t  Stack
eighc of Point  of 'Discharge:   100'
ind Direction:	NW
olor of Plume; Ho visible  plume	
bserver No,'         I
                                   IMC Feldspar
      Type  of Plant: 	
      Location of Discharge :NO .  2 Mil1 Baghouse
      Description of Sky:      Overcast
      Uind  Velocity:
      Detached Plume;
                                       Q-10 mx/hr
                                       "ฅ71
             Duration of Observation;  2-1/4 hr s7~
istance  from  Observer to Discharge  Point:
irection  of Observer from Discharge  Point;
eight of  Observation Poir>t  	
ascription of  Background,	^^
                                     a pprox,
                                     appro*. 100'
                                     trees on hillside
      S U II M  A  R Y
0 ?
AVERAGE
OPACITY
Set
lumber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
09:48
09- 54
10, 00
10- 06
10; 12
10: 18
10. 24
10- 30
10 36
10:42
10:48
10: 54
11: 00
11 06
11:12
11, 18
11:24
11:30
11:36
11:42
End
09- 54
10:00
10 06
10 12
10, 18
10. 24
10 30
10 36
10.42
10:48
10, 54
11: 00
11, 06
11: 12
11- 18
11- 24
11:30
11-36
11,42
11-48
Opacity
S J-,
1"
\
,\
\
-;
^
I,
:,
-••
_
^
>.
N
N
N
N
M
N
N
N
N
Ave rage
N
N
N
N
N
K
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38 ,
39
40
Ti.-^e
Start
11. 48
11 54
12; 00

















End
11: 54
12. 00
12 06

















Opacity
Sura
N
N
N









t







Average
N
N
N








,f~
fjs







ketch Showing  How Opacity Varied With  Time:
Opacity
8
6,
'
s
7




- _
fcai
„-""' "if.*-



T- '.
~ T.;_'





. 'V -





— *
•-T..*.


•i 1
~^,
" , „




• - ~


,
,:'i:j'

1


^
' I
ป I t I

-
•
<. .
'-



,
-,
- -



_,
.
--= _



-;-

•
\ "1 vm -• ""* , *J ซ*i ""'**. ซJ^.f™,-(. (W-— *t

-------
                                    - J_ J -
                                  TABLE III-8
                        SUUMARY  OF  VISIBLE EMISSIONS
                                     i
              International  Minerals and Chemicals Corporation.
                          Spruce  Pine,  North Carolina
I
 ate:
                     9/28/76
IMC Feldspar
                     Outlet Stack
 ype of Discharge;
Height- of Point  of  Discharge,
lind Direction,
lolor of Plume.
Obs erver No, :
                                100 '
                                NW
                   No  visible plume
Type of Plant-	
Location  of  Discharge:No. 2 Mill Baghpuse
Description  of Sky:       Partly cloudy
Wind Velocity, 	     0-15 roi/hr
Detached  Plume-           H/A"
Duration  of  Ob serva tion;  approx. 2-1/4 hra
Distance frcnn  Observer to Discharge  Point;
pirection  of Observer from Discharge Point,
Height of  Observation Point         _  _.-_..
 escription. of  Background-	
                                                                 approx. 40 'SE~
                                                                 SE
                                                                 approx,
f
                                                                 grassy hil1s ide
SUMMAR1 OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
IS
19
20
Time
Start
14-48
14 54
15 00
15,06
15- 12
15- 18
15:24
15: 30
15-36
15 42
15 48
15 54
16:00
16.06
16: 12
16, 18
16: 24
16- 30
16:36
16:42
End
14: 54
Opa ci ty
S ii-i
N
15,00 K
15 06
15. 12
15- 18
15: 2i
-<.T
_>
N
x-
,,!
>-
15 30 \T
15 36
A^
15-42 N
15:48
15- 5^
16: 00
16- 06
16.12
16: 18
16: 24
16 30
16.36
16:42
16 48
N
^
N
N
N
N
N
N
N
N
N
Average
N
K
3S
K
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Set
Ixuinbe r
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Time
Start
16.48
16 54


















End
16- 54
17 : 00


















Opacity
Sura.
N
N











f






A v e r a g e
N
N










•V ^
. If
f






Sketch Showing  How Opacity Varied Uith  Time:
 Opacity
8
1
!'

o




,. i_^-
~ - ^





•





-







0 ~ " „ - j -


0
•*





- -^
---"




- -
-i^:--





-





-"--




,-
1 _





^ ,




-


^ฐ" Time. 'hours' """~~ , -^^ '_ ^~^-=- ^r'-^--— ^-^-s-/-'
" ,, -. . - J --" ' -^'- -- ' , ,, -ป ^ /"

-------
                                 TABLE  III-9
                       5'J7i:iARY  OF  VISIBLE EH IS S IONS
ate
ype
            International Minerals
                       Spruce  Pine

                  	9/29/76
                    Outlet  Stack
                     and Chemicals Corporation
                    , North Carolina
                                                 IMC Feldspar
                	ME
                No visible  plume
    of Discharge,  	
eight of  Point of  Discharge; JLOJ)
ind Direction:
olor of Plume:
bserver No,; 	2	
istance from  Observer to Discharge
irection  of  Observer from Discharge
eight of  Observation Poirt  	
           of
      Type  of  Plant:  		
      Location of D is charge'No .  2 Mill Bagh'ous~e
      Description of  Sky;    Cloudy
      Uind  Veloc ity;
      Detached Plune:'
      Duration of Observation;  2 hrs 7
     P o in t:
      Point;"
                                               0-5 mi/hr
                                               N/A
                                                             a pprox.  50
                                              same level as discharge
                                              hillside with trees
escnpt ion
Background,
      S U M  M A R Y
          0  F
AVERAGE
                                                 OPACITY
Set
lumber
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Tine
S tart
08,35
08 41
08 47
08 53
08: 59
09-05
09. 11
09: 17
09 23
09 29
09- 35
09:41
09.47
09: 53
0 9 ; 5 9
10:05
10; 11
10:17
10: 23
10:29
End
08 40
08- 46
08 52
08; 58
09 CK
09 10
09 16
09 22
09, 28
09- 34
09, 40
09: 46
09, 52
09: 58
10: 04
10 10
10. 16
10, 22
10; 28
10;34
Opacity
Sur
N
K
is
*:
\"
:
.*'

\
N
"\*
*>*
IS
N
N
N
N
N
N
N
N
Average
N
N
N
N
N
N
N
N
N
N
N
M
N
N
N
N
N
N
N
N
Set
t- umber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
33
39
40
Tine
Start
10: 35



















End
10: 37



















Qua c icy
S um
N











ซ







Average
N










X
*-*r
f.







ketch Showing  How Opacity Varied With Time:
Opacity
8


rc
' — :



" ' -,""
-




"—
j**










- '



-
-. ~
-
A _



.^%
~




- "^
™



- "< -
""
'




—




,'

'






_




i _—'

' ~, - ' ~ -, — .. ~ " Time. hours ... * — . .

-------
                                 TABLE 111-10
                        St^lilARY OF VISIBLE EH IS S IONS

              International Minerals  and  Chemicals Corporation
                         Spruce Pine,  North Carolina
 ate:
 ype
                       9/28/76
                                H/A
                                If/A"
     of  Discharge-  Feldspar loading
eight  of Point of 'Discharge•   15 '
ind  Direction.	
alar of PI urn e '.	^___	
>b server No.:	2
istance from  Observer  to  Discharge
irection of Observer from Discharge
eight  of Observation Point: 	
            of
                                                IMC Feldspar
                                                Iruck~&Trt. Car
                                                N/A"~
                                       	N/A
                                 P lun- e :          N/A	
                       Duration of Observation: aj>prox. 3/4n*r~
                      Point; ^	
                       Point:
Type of  Plant:  	
Location of  Discharge'
Description  of  Sky:
Uind Velocity:
Detached
                                                                 approx.  25~
                                                                 Ground level
 es crip tion
Background
                          Building Wall
SUMMARY OF AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
S
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
09- 03
09 • 09
12 09
12 15
12- 21
12 27
12- 33












End
09 09
09 15
12. 15
12 21
12 27
12: 33
12- 39












Opacity
Sun
K
0
0
5
30
30
10












Avera ge
H
0
0
0.21
1 .25
1 .25
1.67












Set
i-'uoiber
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start


















End


















Opacity
S um





%





f






Average










^ S







iketch Showing How  Opacity Varied With  Time.
Opacity
8
6
ft •
9.



-
'."
^











— ^-—









'


1



-
-




-




-

-

























o . • ,„ • i r . 	 • 	 _ '-

-------
                                 TABLE  III-11
                                OF VISIBLE EHISS IOrIS
               International Minerals and  Chemicals  Corporation
                          Spruce Pine, North  Carolina
                        9/28/76
                   Type  of  Plant;
                                                                 IMC Feldspar
la ta
'ype  of  Dischdrge, Indoor Trans fe r Pts , Location  of D i s^~h a r g e : T P~-1, T P - 2 , T P - 3
teight  of Point of Pischarge:VariableDescription of Sky;     N/A
find  Direction: ^___	  N/A ^^  Uind Velocity;
!olor of Plume:    No visible clume   Detached  Plui?e
)bserver No . :
>is
No visible plume
      2
                                                               N/A
                                                               N/A
                                      Duration  of Observation. 3 hrs.
      ;e from Observer  to  Discharge Point:
lirsction of Observer  fron Discharge Point:
[eight  of Observation  Point  	
lescription of Background;	
                                            6'-35
                                            N/A
                                        Building  walls  and equipment structures
SUMMARY OF AVERAGE OPACITY
Set
Suib er
1
2
3
4
-*TK3
6
1
8
9
10
11
12
13

15
^gTP-2
17
18
19
20









Time
S tart
13 45
13 51
13 57
14. 03
14; 09
14; 15
14- 21
14. 27
14; 33
-fl4 39
H-15- 00
15:06
•15: 12






'•
15- 18
15: 24
15-30
15:36
15:42
15:48
J.5. 54
_
E na
13 51
13: 57
14- 03
14 09
14: 15
14. 21
14- 27
14- 33
14 39
14:45
15- 06
15: 12
15: 18
15: 24
15-30
15: 36
15-42
15-48
15- 54
16: 00
Ops. city
Su-
>.
I*
;i
Ll
y
.-
•ป

:ซ
\
\
N
S
N
N
N
N
N
N
N
Average
N
N
K
N
N
N
N
Is
N
N
N
N
N
K
N
K
N
N
N
N
Set
Numb er
21 -
22
23
24
25rp
26_4
27
28
29
30 L
31
32
33
34
35
36
37
38
39
40
Tine
Start
-16. 00
16: 06
16: 12
16 18
16.24
16. 30
16- 36
16. 42
16.48
-16: 54










End
16. 06
16- 12
16. 18
16- 24
16 30
16 36
16- 42
16. 48
16- 54
17. 00










Opacity
S un.
N
N
N
K
N
N
N
N
N
N


9







Average
N
N
N
N
N
N
• N
N
N
N

y
t
M.







.ketch Showing How Opacity  Varied Uith Time;
Opacity
8
'
, (
-i




-
.: — „
'-. "" \



r

- - *
__



~,






""





-




-
-



-
f „ ,
7'

i

.'-

•



• -
f




'"" I1
""
-




",





_



                                 - . -„. Time, "hours '  ,

-------
                                TABLE 111-12

                       SUMMARY OF VISIBLE EMISSIONS

             International Minerals and Chemicals Corporation
                        Spruce Pine, North Carolina
ate; 	   9/28/76
ype of Discharge". Conveyor Transfer
eight of Point
ind Direction;
olor of Plume;
bserver lio . .
istance from
irection of
 of Discharge:
                               20'
                N/A
   No visible plume
            D ischarge
             Observer  to
            Observer  from Discharge
eight of Observation  Poirt'  	
           of
 Type of Plant: 	
 Location of Discharge.
 Description of Sky;
 If ind Velocity :
 De tached
 Dura tion
Point: 	
 P o in t;
                                               IMC Feldspar
              N/A
                                                             N/A
Pluire: 	H/A
of Observation.
              351"
                                                    2 hrs .
                                              N/A
escription
Background.
         Building and  equipment  structures
S U M M A P. Y OF AVERAGE OPACITY
Set
lumber
I
2
3
4
5_
^CP-5
7
8
9
10
11
12
13

^^XB4
16
17
18
19
20









Tine
S tart
•09 30
09. 36
09-42
09 48
09; 54
10-00
10. 06
10- 12
10: 18
4 10: 24
_









"10.51
10:57
11- 03
11: 09
11: 15
11: 21
11: 27
11:33
11:39
•11:45
End
09 36
09 42
09 ^8
09 5-r
10 00
10: 06
10: 12
10 IS
10: 2L
10. 30
10:57
11- 03
11:09
11: 15
11- 21
11; 27
11- 33
11:39
11:45
11: 50
Opa city
Su-
N
J,
IS
N
. <
X
N
N
N
N
N
N
N
N
N
N
N
N
N
N
Ave rage
N
N
N
N
K
N
N
N
ft
N
N
N
N
N
N
N
N
N
N
N
Set
Number
21
22
23
24
25
26
27
26
29
30
31
32
33
34
35
36
37
38
39
40
Tine
S tart




















End




















Opacity
S um












1







Average











*
r







ketch Showing How  Opacity Varied Uith Time:
Opacity
(7,) 8
6
j
4',
i
2 -
,c,-ll^^;\.p




~,,:
r -




i
- '•




-












-





\










_





-











1





-

) - - - .1..- - ]_ - T-i mo *"' h n nr c "'i "" 2 -1 -* "" ~ """— "**" 	 * ~L w

-------
                  TABLE 111-13

          S'JTHARY OF VISIBLE EMISSIONS

International Minerals and Chemicals Corporation
           Spruce Pine, North Carolina

           9/29/76
       Discharge ;Fugit ive Emissions
ite:  _
rpe  of            __	
iight of Point of Discharge, 0-90
Lnd  Direction; 	E
3lor of Plume
jserver No . -.
[.stance from
                  No visible plume
             Observer  to  Discharge
Lrection of Observer from Discharge Point:
sight of Observation Point-
                   of Plant:  	
             Location of Discharge;
             Description of Sky; 	
             Uind  Velocity:
             Detached
             Duration
            Point,
                                                               IMC Feldspar
                                                W
               Building Wall
                                                             Qverca st
                                                             0-5  mi/hr
                                 Flure:         H/A
                                 of  Observation:
                                                                1  hr .
                                              a pprox.  7 5
                                   Ground level
iscription of Background. Sky and building exterior^AITT wind ows
 * Two windows at ground level.  One door at upper  level.
                                          and door open
      S U M M A R, Y
0 F
                  AVERAGE
OPACITY
Set
utnber
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Time
Start
08:45
08: 51
08- 57
09-03
09, 09
09: 15
09. 21
09: 27
09:33
09,39










End
OS' 51
08 57
09: 03
09 09
09, 15
09; 21
09 27
09 33
09. 39
09,45










Opacity
SL-
K
N
?<
^
}
-_
X
^,
•*•
"*.










Average
N
N
N
N
N
N
N
N
N
N










Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start




















End




















Opacity
Sun




















Average











./
ฃ-H







cetch Showing How Opacity Varied With Time:
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-------
                                       ill-
                       SUMMARY  OF  VISIBLE EMISSIONS

              International Minerals and Chemicals Corporation
                         Spruce Pine, North Carolina
ace; 	9/29/76
ypa  of  Discharge-  Fugitive Emis sio n s
eight  of Point of 'Discharge:  	
ind  Direction:  	  E-KE	
olor of Plume:
bserver No.;
istance from
                   Ho visible  plume
                       Type of Plant: 	
                       Location of Discharge;
                       Description of Sky:
                       Uind Velocity 	~
                       Detached Plume;
                                of Observation;
                                                              IMC Feldspar
                                     Duration
E. Building Wan
pvercast
0-5 mi/hr      '
N/A           ~
    1 hr.
              Observer  to Discharge Point;
irection of Observer  from Discharge Point;
eight of Observation  Point.  ^^_	__
ascription of Background:	
*  Four windows, three upper,  and  one  ground level-
   Two doors at upper  level
                                           a pprox.  75'*
                                                          Ground level
                                                   Sky,  trees  on hillside
SUMMARY 0? AVERAGE OPACITY
Set
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tirae
S tar t
09 50
09 56
10, 02
10 08
10. 14
10: 20
10. 26
10: 32
10-38
10.44










End
09- 56
10 02
Opacity
S u~"
N
N
10 03 N
10 14
10 20
10 26
1J
r
N
10 32 i is
10-3S S
10-4-+J S
10. 50










N










Av er a gs
N
N
N
N
N
N
N
N
N
N










Set
I7 u m b e r
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start




















End




















Opacity
Suni












^







Avera ge






.ป





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,ketch
      Showing
How Opacity Varied  With Time
Opacity
( ฐl \
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-------
                                 TABLE  111-15

                                oV VISIBLE  EMISSIONS
              International Minerals  and  Chemicals Corporation
                         Spruce Pine,  North. Carolina
'ate:  	       9/29/76
'ype  0"f Discharge: fugitive Emissions
 eight of Point of "D'I s c h a r g e : "^0-"9" 0 T
'ind  Direction; ^    	     ME
 olor of Plume:   Ho v 1 s  it) 1 e .pi urn e
>b server No-;  	1
ixstance frotn  Observer to  Discharge
Direction of Observer  from  Discharge
[eight of Observation  Point' 	
 escription of Background-	
      '''Four windows on upper
       at ground level.All
              Type of Plant; ________
              Location of Discharge:
              Description of Sky: 	
              Uind Velocity: 	
              De tached
              Duration
             P o in t:  	
              Point:
                               IMC Feldspar
                               S. Building Wall
                               Overcast
                               0-5mi/hr
                Plume  	
                of Observation:
             N/A
               1 hr .
                            approx.  75
                                   approx.  4(P
                                   "Blsyand  tree's
     level,  One  window, one  large and one small door
     windows  a ud door s are open .	
       S U M M A R  Y
0 F
AVERAGE
OPACITY
Set
Number
I
2
3
4
5
6
7
8
9
10
Time
S tart
10:55
11 01
1L.07
11- 13
11:19
11: 25
11:31
11-37
11-43
11-49
11 I
12
13
14
15
16
17
18
19
20









End
11,01
11- 07
11- 13
11: 19
11, 25
11-31
11 37
11 i3
11.49
11:55










Ooa city
Sur
Ii
i>
V
:.
V
:,

-i-
•*,••
"










Average
N
N
K
N
•*-
IN
N
N
N
N
N










s.t
Numb sr
21
22
23
24
25
26
27
28
29
30
31
32
33
34
35
36
37
38
39
40
Tine
Start




















End




















Opacity
Sun






,,





ซ







Average











,*'
**







iketch Showing How  Opacity Varied With  Tine:
Opacity
      ~- 4
      1*'* 0
                                       Time  "hours

-------
                                 TABLE  III-16

                        SU1LMARY OF  VISIBLE EMISSIONS

               International Minerals and  Chemicals Corporation
                          Spruce Pine,  North  Carolina
                                           of Plant:
                                             IMC Feldspar
ate: 	      9/29/76      Type  ._	
ype of Discharge:  Fugitive E miss ion s Location of Discharge: N. Building Wall
 '  ' "  of Point  of  'Discharge:  Q - 9 0v  Description of Sky;    Overcast	
                                     Uind  Velocity, 	0-10 mi/hr	
                                     Detached Plume:N/A
                                     Duration of Observation;1 hr."
 eight
 ind  Direction:
 olor of Plume:
 b s erver No . :
	ME
 No  visible  plume
 istance from Qoserver  to  Discharge Point:
 irection of Observer  from Discharge Point;
 eight of Observation  Point, 	
 escription of Background
                                           a pprox	  100'
                                           w
                                           a p'prox .  20 '
        * Four open windows at upper  level
                            Sky, traces, gray  storage  silo
SUMMARY 01 AVERAGE OPACITY
Set
^unber
1
2
3
4
S
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
Tirac
S tart
14: 00
14: 06
14; 12
14, 18
14: 24
14; 30
14, 36
14:42
14:48
14 54










End
Opa ci ty
Sun
14-06 J,
14. 12
14 18
14 24
14 30
14, 36
14- ^2
:•!
„•
;:
;\
•*"
S
14,^8 ;:
14: 5^
15- 00










:;
N










Average
N
N
N
N
N
N
N
N
N
N










Set
JTunb er
21
22
23
24
25
26
27
28
29
30
31
32
33
3^
35
36
37
38
39
40
Tiwe
Start




















End




















Opacity
S urn












4







Average











X
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iketch Showing How Opacity  Varied With Time;
Opacity
8
6
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?
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-------
                               TABLE 111-17
                       SUMMARY'OF VISIBLE EMISSIONS
             International Minerals
                        Spruce Pine
                  and Chemicals Corporation
                 ,  North Carolina
ate,  	
ype. of Discharge:
eight of Point
ind Direction:
olor
      9/29/76
                      Type  of Plant-  	
   	   Location of Discharge:
of Discharge 100-125'  Description of Sky; 	
                      Uind  Velocity:
                      Detached Plume:
                      Duration
                    Point;  	
                      Point,
                                                               IMC  Feldspar
Fug itive Dust
    	ME
     White-grey
     of Plume: 	^	
bserver No. :             2	
istance from Observer  to  Discharge
irection of Observer  from Discharge
eight of Observation  Point.
ascription of
                Entire Roof
                Cloudy    ~~
                ^^T^i/hT'~
       	 K/A
of Observation: 58 mlns.'
                                                            appro*,300'
                                                         of discharge polnt
              Background -
                              Eye-leve1  with  a is charge pt
                              Hi 11sid ew11 h  trees
SUMMARY 0? AVERAGE OPACITY
Set
rumber
1
2
3
4
5
6
7
B
9
10
11
12
13
14
15
16
17
18
19
20
Tine
Start
11: 00
11: 06
11 12
11, 18
11- 24
11,30
11: 36
11 42
11:48
11: 54










End
11 05
11 11
11, 17
11, 23
11- 29
11- 35
11 41
11 47
11: 53
11- 57










Opacity
Sv-
23 ^
205
200
2C5
i Q3
i-c
I~0
*. ~ ~
if 2
4- ซ* —










Average
9,6
8. 5
8,3
8,5
7.7
7.1
7,1
7,7
6.3
8.1










Set
Number
21
22
23
24
25
26
27
28
29
30
31
32
33
3^-
35
36
37
38
39
40
Time
Start




















End




















Opacity
Sun




















Average











X
g*







ketch Showing How Opacity  Varied With Time;
Op=icit>
                                      Time,

-------
                              -  25 -


from five to 15 percent  opacity was  observed emanating from the

building roof.  The  six-minute  average opacities for the roof

ranged from 6.3 to 9.6  percent.

     Opacity measurements  taken for  the baghouse outlet stack

were simultaneous with  the three3 two-hour particulate tests

taken at the baghouse outlet.   The absence of visible emissions

at this site correlates  well  with the low measured emission

rates.


Particle Size  Sarapllrg  Results

     Tables IV-1 and.  IV-2  present the results of the combination

of microsieve  analysis  and electronic particle counting for the

particle size  samples taken at  the North and South Baghouse In-

lets, respectively.   Figures  3  and 4 present graphical represen-

tations of these zปj  distributions.   Figure 3 indicates that ap-

proximately 73 percent  of  the  particulate weight was attributable

to particles greater  than  10  microns in diameter at the North In-

let, while Figure 4  shows  that  at the South Inlet, approximately
                                                            *7
63 percent of  the particles (by weight) was greater than 10

microns in diameter.

-------
           PARTICLE
        NO.  2  MILL
                     _ 26 -
TABLE IV-1

 SIZE DISTRIBUTION
 BAGHOUSE  NORTH  INLET
International Minerals and Chemicals Corporation
           Spruce  Pine,  North Carolina
              September  27-29,  1976
Characteristic
Diameter
of
Partic les
(mic rons )
>45
30 - 45
20 - 30
10 - 20
8.0-10
6.3-8.0
5.0 - 6.3
4.0 - 5.0
3.2-i.O
2.5-3.2
2.0-2.5
1.6 - 2.0
1.3 - 1.6
1.0-1.3
0.5 -1.0
<0.5
TOTAL

Weight
(gm)
11.400
4.175
3.345
7.834
0.147
0.405
0.710
0.666
0.841
1, 028
0.902
0.621
0.349
0.401
0.396
0. 119
33.339
Size Distribution
by Weight
Percent
34.2
12.5
10.0
23.5
0.4
1.2
2. 1
2.0
2.5
3.1
2.7
1.9
1. 1
1. 2
1.2
0.4
100.0
Cumula tive
Percent
100.0
65.8
53.3
43.3
19.8
19,4
18. 2
16.1
14.1
11.6
8.5
5.8
3.9
2.8
1.6
0.4
	
                        Clayton Environmental  Consultants,  Inc.

-------
                     - 27 -
                   TABLE IV-2

           PARTICL! SIZE DISTRIBUTION
         NO.  2  MILL BAGHOUSE SOUTH INLET

International Minerals and  Chemicals  Corporation
           Spruce  Pine,  North Carolina
              September  27-29,  1976
Characteristic
Diameter
n f
U J.
Particles
(microns )
>45
30 - L5
20 - 30
10 - 20
5.0 - 10
4.0-5,0
3.2 - i, 0
2.5-3.2
2.0 - 2.5
1.6 - 2.0
1.3-1.5
1.0 - 1.3
0.5 - 1.0
<0.5
TOTAL

Weight
(gm)
0,366
0.271
0. 233
0. 141
0.094
0.006
0.016
0. 030
0.040
0. 044
0.036
0.034
0.073
0.039
1.423
Size Distribution,
by Weight
Percent
25.7
19.1
16.4
9.9
6.6
0.4
1.1
2. 1
2.8
3.1
2.5
2.4
5.1
2.8
100.0
Cumulative
Percent
100.0
74.3
55,2
38.8
28. 9
22,3
21.9
20.8
18,7
15.9
12.8
10.3
7.9
2.8
—
                        Clayton  Environmental  Consultants, Inc.

-------
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1 FIGURE 3
PARTICLE SI2E DISTRIBUTION
NO. 2 MILL BAGHOUSE NORTH INLET
1 In te r national Mineral s and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
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001   0 05 0102   05  1   i
     5     10     20   30  40   LiO  60  /O    CO     90    95

Cumulative  Percentage Less  Than Indicated  Diameter
98
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-------
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! F FIGURE 4
I/ PARTICLE SIZE DISTRIBUTION
/f j NO. 2 MILL BAGHOUSE SOUTH INLET
iVt International Minerals and Chemicals Corporation
Spruce Pine, North Carolina
September 27-29, 1976
J
: •;. -\



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20 JO 10 -50 60 70 CO 90 95 93 W 99 G 99 9 99 99
                                                                         K3
                                                                         VO
Cumulative Percentage Less Than  Indicated  Diameter

-------
                           - 30  -
           III.  PROCESS DESCRIPTION  AND  OPERATION
(To be supplied by EPA)

-------
                              - 31 -






                 IV.   LOCATION OF SAMPLING POINTS




     Figure 5 depicts  the  positions of the ports used  to  sample




the baghouse vertical  outlet stack and the two horizontal inlet




ducts.  Each inlet and  outlet duct is of cylindrical  construction




and thus each was  sampled  from two ports separated  by  90  degrees,




as required by EPA Method  1,




     Figure 6 is a diagram of the sampling points used in sampling




the 19-inch diameter  vertical baghouse outlet duct.   The  duct was




divided into equal annular areas and 24 points were sampled.




     Figures 7 and 8  depict the sampling points on  the north  and




south inlets, respectively.  Again, each duct was divided into




equal annular areas and a  total of 24 points was sampled  at each




location.

-------
      SCHEMATIC DIAGRAM OF BAGHOUSE INLET AND  OUTLET  DUCTS
                       NO.  2  MILL  BAGHOUSE

        International Minerals and Chemicals Corporation
                  Spruce  Pine,  North  Carolina
                      September  27-29, 1976
         i  Outlet
        ?
 ~l

5'0"
 I
rL
              Ba ghoas e
                              North
                              Inlet
                            7,0,r
                                               South
                                               Inlet
                         WEST SIDE VIEW
Outlet
              Baghouse
                  TOP VIEW
                              North
                              Inlet
                                               South
                                               Inlet
                               Clayton Environmental Consultants, Inc.

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                           - 33 -
                         FIGURE 6

      SCHEMATIC  DIAGRAM OF SAMPLING POINT LOCATIONS
                NO. 2 MILL BAGHOUSE  OUTLET

     International Minerals and Chemicals Corporation
               Spruce  Pine,  North Carolina
                   September  27-29, 1976
Pos ition
1
2
3
4
5
6
7
8
9
10
11
12
Distance
( Inches )
0
1
2
3
.38
.27
.24
i
- 3c
Ir. 15
6
12
U
15
16
17
18
, 73
. 27
.25
.6-
.76
.73
.62
Duct Diameter;  19"
7
7
8

10 i:
9 11

v
                                ton Environmental  Consultants, Inc

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                        _  34  -
                      FIGURE  7

   SCHEMATIC  DIAGRAM OF SAMPLING POINT  LOCATIONS
           NO,  2  MILL BAGHOUSE NORTH  INLET

  International Minerals  arid  Chemicals Corporation
             Spruce Pine, North. Carolina
                September 27-29, 1976
Pos ition
1
2
3
4
5
6
7
8
9
10
11
12
Distance
(Inches)
0,25
0.80
1,42
2 , I 2
3 ,00
4. 26
7 ,7-
9 . CC
9, S3
10,58
11,20
11.75
Duct Diameter:  12'
                         Clayton Environmental Consultants,  Inc.

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                        -  35  -
                      FIGURE  8

 -' 'SCHEMATIC  DIAGRAM OF SAMPLING POINT LOCATIONS
           NO.  2  MILL BAGHOUSE SOUTH INLET

  International Minerals  and  Chemicals Corporation
            Spruce  Pine, North Carolina
               September 27-29, 1976
Position
1
2
3
4
5
6
7
8
9
10
11
12
Distance
(Incites)
0.32
1.00
1 .77
2 .66
3.75
5.32
9. 68
11-23
i ••• "j
13.23
14.00
14.68
Duct Diameter:   15"
                         Clay ton -Envirortmenta 1 Consultants,  Inc.

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                              - 36 -


              V.   SAMPLING AND ANALYTICAL PROCEDURES

     All  samples  obtained at the baghouse outlet duct followed

 the  procedures  outlined in EPA draft Method 17 (see Appendix B) .

 In  this  instance j  a 47-milliineter Gelman filter holder was employed

 for  in-stack  filtration, as shown in Figure 9.

     The  inlet  test procedure was a modification of EPA Method  17.

 The  in-stack  filter holder was replaced by a section of teflon

 probe  leading from the sampling nozzle out of the stack to a

 110-millimeter  stainless steel filter holder, as shown in Figure

 10.  Field  data  sheets for all particulate sampling are presented

 in  Appendix C,

     Particle size sampling at both inlet ducts employed an alundum

 thimble  connectec  to the nozzle by a 12-inch section of stainless

 steel  probe followed by a 47-nill iiae ter type SGA filter contained

 in  a stainless  steel Geltnan filter holder.  This sampling train  Is

 shown  in  Figure  11.  Only the contents of the thimble were retained

 for  laboratory  analysis by microsieving at the Clayton Environmental
                                                                 X
 Consultants laboratory.  The portion of the microsieve analyre  found

 to  be  less  than  five microns was sent to Battelle Columbus Laboratories

 for  further particle size determination by electronic particle  coun-

 ter  methods.   Field data sheets for all particle size sampling  are

 presented in  Appendix D.

     All  opacity  data were obtained according to EPA Method 9.   Field

 data sheets for  all visible emissions observations are included  in

 Appendix  E.

     Appendix F  contains the sampling summary sheets.  Appendices

 G and  H  present  the particulate weight data and the calibration  data,

"respectively. ~ "Appendix I presents example calculations.

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                                          FIGURE 9

                      SCHEMATIC  DIAGRAM  OF  PARTICULATE  SAMPLING TRAIN
                                   NO. 2 MILL BAGHOUSE OUTLET

                      International Minerals and Chemicals Corporation
                                 Spruce  Pine,  North  Garplina
                                    September  27-29,  1976
       4 7-mm     Teflon
"8
f
I
I
4f i _
hertn
ocouple
i 	 ni
Pi tot/
Tube'

      Pyrometer    Inclined
                  Manometer
                Orifice
                Meter




—


\



\ f
	 > / 	

—


r














<~~-


^ *
\
-i



                                                           •Ice Bath
100 ml
Water
 Dry  Silica
Trap  ^Gel
      V •
Valves,
                                                  Vacuum
                                                  Gauge
                                                                     Leakless
                                                                       Pump
                                                       Dry   Clayton Environmental Consultants, Inc
                                                       Gas
                                                      Mot r r

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                                              FIGURE 10

                          SCHEMATIC  DIAGRAM  OF  PARTICIPATE SAMPLING TRAIN
                             NO. 2 MILL BAGHOUSE NORTH AND SOUTH  INLETS

                          International Minerals and Chemicals Corporation
                                     Spruce Pine,  North Carolina
                                        September  27-29,  1976  ,
              HO-mm
              Filter
Teflon
 Probe
  /
.- Pyrometer    Inclined
             Manometer
                Orifice
                 Meter

%













l~\
"3ST









/




J

"4.X-
















••&,





--T
', 1
1 v
t
1



-
y


•> *





                                                              Ice
                                                              Ba th
                                                                                                    u?
                                                                                                    OT
                                                                         Leaklesa
                                                                           Pump
                                                         Dry Gas
                                                          Meter  Clayton Environmental  Consultants,  I

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                                               FIGURE 11

                           SCHEMATIC  DIAGRAM OF PARTICLE SIZE SAMPLING TRAIN
                                          NO. 2 MILL BAGHOUSE
                                            i,
                           International Minerals and  Chemicals  Corporation
                                      Spruce Pine, North Carolina
                                         September 27-29, 1976
           Medium Porosity
           Alundum Thimble
                 Glass-Fiber
                   Filter
                               Teflon
                                Probe
Teflon
Tubinu
,'Vt  i
t'i  S
i-ei  &
ii:fc
i, S  * ,
If'^.-1
&— 	 * 	 1 	 ฃ^

4
>
i '
i
r s

/
/
/
!
Pitot
Tube


                                   lOO'ml
                                   Water
                                                Dry
                                                Trap
1

—
\
\

,
tl
r






i

1 1
"f ,
*
i 1
if
1
I




                                                                       Umbilical
                                                                         Cord
                                                              •Silica
                                                                Gel
                                                        •Thermometers  ^.Valves
                   Orifice
                   Meter
                                                                          Pump
                                                           ry Ga s
                                                           Mete*
                                                                  Clayton Environmental  Consultants,  I

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                           APPENDIX 4
                      PROJECT PARTICIPANTS

Clayton Environmental Consultants, Inc.
          Victor W, Hanson
          Harold P. Hood
          Gerald E. Hawkins
          Thomas R. Julien
          Richard G. Keller
          Helene ML Hysko
          Janet L. Vecchio
          David L, Holmberg
          Mary L. Fegan
          James M, McClain
Project Leader
Field Team Sampler, Data Processing
Field Team Sampler
Field Team Sampler
Field Team Sampler
Data Processing
Data Processing
Assistant "Laboratory Director
Laboratory Technician
Chemist
          John E. Mutchler, P.E.  Contract Manager
U.S. Environmental Protection Agency
          Robert Martin           Project Officer
          Jim Eddinger            Process Engineer
          John Brown              Visible Emissions Observer
          Dennis Holzschuh        Visible Emissions Observer
International Minerals and Chemicals  Corporation
          Jeff Van Jtike           Environmental Engineer

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     APPENDIX B
EPA DRAFT METHOD  17

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       Ht-THOD 17.  r'ET?Pt':..;-7IP[! fr P-fPTICLLpTE -,':><
      FROIi STATIOTJAVf SOuVCLS (I."-STACiC FILTK^TICi! I.ETKC3)
Introduction
     Particulate matter is not an absolute quantity, rather it
is a variable which is a function of tenperature and pressure.
For this reason, participate natter emission regulations and/or
associated test methods must define or take cognizance of the
temperature and pressure at which particulate natter is to be
measured.  If temperature is not defined, and if the effect of
temperature upon the quantity of particulate in an effluent gas
is unknovm, then the participate emission regulation may be
variable.  The range of pressures yhich exist from source to source
is of negligible importance.
     In Method 5, 250ฐF is established as a nominal  reference tem-
perature-  Thus, where Fethcd 5 is specified in an applicable sub-
part of the standards, particulate natter is defined with respect
to temperature.  In order to iraintain this indicated temperature,^?
Method 5 includes a heated alass sample probe and a  heated filter
holder.  This equipment is cumbersome and reouires care in its
operation.  Therefore, vซ'here parti cul ate matter concentrations
(over the norrral range of tenperature associated v/ith a specified
source category) are known to be independent of teipperatura, it is
desirable to eliminate the olass probe and heating systems, and
sample at stack temperature.

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     This fnECnOG describes an in-stack sarrpling system end samp-
ling procedures for use in such ceses.  It 15 -intended to be used
only when specified by an applicable suhpart of the standards,
and only \iithin the applicable temperature limns (if specified),
or when otherwise approved by the Adnimsirator.
            t
1.  Principle and applicability.
     1.1  Principle.  Participate natter is withdrawn isolnnetically-
from the source and collected on glass_ fjber.,fliter maintained.at
stack temperature.  The particulate mass is determined graviiretri-
cally after removal of unccmbined water.
     1,2  />pplicability.   This method applies to the d&ternination
of participate emissions froTi stationary sources for determining
compliance with new source performance standards, only v;hsn spe-
cifically provided for in an applicable subpart of the standards.
This method is not applicable to stacks which are saturated with'
v.'ater vapor.  In addition, this method_sha11  not. be used as written,
if the projected cross sectional  area_pf the  orob^ ••rtension-filter
                                  "                           ~ „,.  ^
holder asseirbly (v.-hsn inserted halfway intc lh^ Swack) covers mdre than
3% of the stack cross-sectional area (see Section 4.1.2).
2.  Apparatus.
     2.1  Sampling train.   A schematic of the sarrpling train used
in this method is shown in Figure 17-1.  Construction details for
many, but not all, of the train components are given in APTD-0581;
for changes from the APTD-0531 document and for allowable modifica-
tions to Figure 17-1, consult with the Administrator.

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       The operating and pM^titenar-e procedures fo>" r?any of the
  sarpling train components are described in APTD-0576.   Since
  correct usaae is important in obtaining valid results, all
  users should read the ฃPTQ-0576 docursnt and adopt the opGret-
  ing  and maintenance procedures outlined in it, unless  otherwise
                                         s
  specified herein.
       2.1.1  Probe nozzle—Stainless steel (316) with sharp,
  tapered leading edge.  The angle of taper shall be _ 30ฐ and
  the  taper shall be on the outside to preserve a constant internal
  diameter.  The probe nozzle shall be of the button-hook or elbov/
  design, unless otherwise approved by the Administrator.  The
  nozzle shall be constructed from seamless stainless steel tubing.
  Other configurations and construction material nay be  used subject
  to approval from the Administrator.
                                                                h.
       A range of sizes suitable for isokinetic sampling should be
  available, e.g., 0.32 cm (1/8 in.) up to 1.27 cm (1/2  in.) (or
'  larger if higher volume sampling trains are used}  inside diameter
                                                                4
  (ID) nozzles in increments of 0.16 cm (1/16 in.}.   Each nozzle
  shall be calibrated according to the orocedures outlined in  the
  calibration section.
       2.1.2  Filter Holder.  The in-stack filter holder shall be
  constructed of borosilicate or ouartz glass or stainless steel;
  if a gasket is used, it shall be made of silicone  rubber, teflon,
  or stainless steel,   Other holder and gasket materials nay be used
  with approval from the /Mministrator.  The filter holder shall be

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"""' j-M f
(•irLlvCP
                                                        IMPINCEfl TRAIN OPTIONAL, MAY BE REPLACED
                                                             BY AM EQUIVALENT CONDENSER
                                                                                         CHECK
                                                                                         VALVE
                                                                                         VACUUM
                                                                                           LINE
                           PITOT MANOMETER'

                                    ORIFICE
                         IMPINGERS               ICE OATH
                                  BY-PASS VALVE
                          THERMOMETERS
                                                                            VACUUM
                                                                            GAUGE
                                                                    MAIN VALVE
             DRYGASMETCn
                                                         Ain-TlGHT
                                                           PUMP
                                              . ParticulatG-sampIing train.,
                                                                   >

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designed to provide ฃ positive seal against IcaLaga from the out-
side or around the filter.
     2.1,3  Probe Extension--ฃny suitable ricnd probe extension
may be used after the filter holder.  Flexible tubing rray also
be used between the probe extension and the condenser.
                                         x
     2.1.4  Pi tot tube—Type S, or other device approved by the
Administrator, attached to probe extension to alloy/ constant
monitoring of the stack gas velocity.   The face openings of the
pitot tube and the probe nozzle shall  be adjacent and parallel
to each other, not necessarily in the  sarr.s plane, during ssrrpling,
The free space betveen the nozzle and  pitot tube {see Figure 17-1}
shall be at least 1.9 cm (0.75 in.).  The free space shall  be set
based on a 1,3 cm (0,5 in.) ID nozzle.  If the sampling  train is
designed for sampling at higher flov rates than that described in
APTD-0581, thus necessitating the use  of larger sized nozzles, the
largest sized nozzle shall be used to  set the free space.   In addi-
tion, to minimize aerodynamic interactions betvreen the pitot tubgy
and filter holder, there shall be a distance of at least 3  inches
between the center line of the pitot tube impact openings  and the
leading edge of the filter holder (see Figure 17-1).
     The pitot tuba must meet the criteria specified in  Method 2,
and be calibrated separately (i.e., apart fron its asserrbly con-
figuration) according to the procedures outlined in that method
for the calibration of isolated Type S pitot tubes.

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      E.I.5   Differential pressure qauce--Incliped nano.-ster
capable of Pleasuring velicity head to within 10% of the rruniPUin
measured  value or ฑ 0.013 rrn (0-COQ5 in.)> whichever is greater,
Below a differential pressure of 1.3 ran (0.05 in.) water gauge,
           j
nicromanpmeters with sensitivities of 0,013 ir."i (0.0005 in.)
                                        JP
should be used,  Hovrever, nricroin&noreters are not easily adaptable
to field  conditions and are not easy to use with pulsating flow.
Thus, methods or other devices acceptable to the Administrator may
be used when conditions warrant.
     2.1.6   Condenser—Any system that cools the sample gas stream
(e.g., impingers connected in series, as in flethod 5) and allows
measurement  of both the v/ater condensed and the moisture leaving
the condenser, each to v.'ithin 1  ml or 1 g.  The moisture leaving the
condenser can be measured either by:   (1)  monitoring the tenperature
and pressure at the exit of the  condenser and using Dalton's law; or
(2) passing  the sample gas stream through  a silica gel  trap with
exit gases kept below 20ฐ C (68ฐ F)  and determining the weight gain.
     If means other than silica  gel  are used to determine the amount
of moisture  leaving the condenser, it is recontended that silica gel
still be  used between the condenser system and pump to prevent
moisture  condensation in the pump and metering devices.
     2.1,7   f'etering system--Vacuum qauge, leak-free pump, therrporpeters
capable of measuring temperature to within 3ฐ C (5.4ฐ F), dry gas r.eter
v/ith 2% accuracy, and related equipment, or equivalent, as required to

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paintein an isckinetic srrplira retc r.s', to d=taimpc sarple vclure.
Sanpling trains utilizinq peteiing systems desiqrod for hicjher flow
rates than that described in APTD-0501 or APTD-0576 pay be  used
  rovided that  the specifications  in  section 2 of  this rrsthod are
met.  When the metering  system is used  in  conjunction with  a pitot
tube, the  system  shall enable  checks of'isokinetic rates.
      2  1.8  Baro-rater—fercury, aneroid,  or other barometers  capa-
 ble of measuring atmospheric pressure to v/ithin Z.S p.m Hg (0,1  in.
 Hq)   In wany cases, the barometric reading Kay be obtained from a
  nearby v:eather bureau station, in which case the station value
  (which is the absolute baroiretric pressure) shall be requested and
  an adjustnent for  elevation differences between  the weather station
  and sampling  point shall  be applied at a  rate  of minus 2.5 rm Hq
  (0 1 in-  Hg)  per 30 m (100 "ft) elevation  increase  or vice  versa- for
  elevation decrease.
       21,9  Gas density determination equipment—Temperature and
  pressure gauges and gas analyzer as described in Tethods 2 and*&
       2.1.10  Temperature  end pressure gauqes--If Dal ton's  lau  is
   used, to monitor  tenperature  and pressure at co-/-nser outlet.   The
   temperature  gauge shall  have an accuracy of 1ฐ  C {2ฐ F).  The
   pressure gauge  shall be  capable of measuring  pressure to vnthin
   2,5 mm Hg (0.1  in* Hg).   If  silica qel  is used  in the condenser
    system the  tenperature and pressure nust be  measured before the
    silica gel  component.

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     2.2  Samnle recovery.
     2,2.1  Probe nozzle brush—Kyi on bristles  '-nth  stainless  steel
wire handle.  The brush shall  be prcoerly sized and  shaped  to  brush
out the probe nozzle.
     2.2.2  Glass wash bottles—Two.
     2.2.3  Glass sample storage containers—-Chemically  resistant,
borosilicate glass bottles,  for acetone washes, 500  ml or 1,000 ml.
Screw cap closures shall be  teflon rubber-backed liners  or  of  such
Construction so as to be leak  free and prevent  chanical  attack
from the acetone.  (Marrow mouth glass bottles  have  been found to
be less prone to leakage.)   Other types of containers nust  be  ap-
proved by the Administrator.
     2,2.4  Petri dishes—For  filter  samples; glass  or polyethylene,
unless otherwise specified by  the Administrator.
     2.2.5  Graduated cylinder and/or balance—To measure condensed
                                                               •>,
water to v/iihin 1 ml  or 1  g.   Graduated cylinders shall  have sub-
divisions no greater than 2 nl.   Post laboratory balances are  capa-
ble of weighing to the nearest 0.5 g  or less. Any of these  balances
                                                              9>.
are suitable for use here and  in section 2.3.4.
     2.2.6  Plastic storage containers—Air tight containers to
store silica gel.
     2.2.7  Funnel and rubber  policeiran--To aid in transfer of
silica gel to container; not necessary if silica gel is  weighed in
the field.
     2.3  Analysis.

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      2.3.1  Glass ueiqhinci dishes.


      2.3.2  Desiccator.


      2,.3.3  Analytical balance--To neasure to within 0.1 r.ig.


      2.3,4  Balance—To neasure to within 0,5 g.


      2.3,5  Beakers—250 ml.
                                          rs

      2.3,6  Hygrometer—To measure the relative humidity of the


 laboratory environment,


      2.3.7  Temperature gauge—To neasure the temperature of the


 laboratory environment.


 3.  Reagents


      3.1  Sampling.


      3.1.1  Filters—The in-stack filters shall  be glass rrats or


 thimble fiber filters, vnthout organic binders,  and shall exhibit


 at least 99,95% efficiency (< D.05% penetration) on 0.3 micron

                                                                 A
 dioctyl phthalate smoke particles.  The filter efficiency tests


 shall be conducted in accordance vn'th ASTfl standard rvethod D 2926-71.


 Test  data from the supplier's Quality control prog ran is sufficient  ,

                                                                4ฎ
"for i.} is purpose.


      3.1.2  Silica gel—Indicating type, 6-16 pesh.  If previously


 used, dry at 175ฐ C (350ฐ F) for 2 hours.  New silica gel nay be


 used  as received,


      3.1.3  Crushed ice.


      3.1.4  Stopcock crease—Acetone insoluble,  heat stable silicone


 grease.  This is not necessary if screw-on connectors with teflon


 sleeves, or similar, are used.

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     3,Z  Sjrple recovery.
     3.2.1  /1,cetcine--[7eegcnt grace,  5 0,001** residue,  in glass
bottles.  Acetone fron rretal containers generally  has  a high residue
               i
blank and should not be used,  Sonatinas,  suppliers  transfer acetone
to glass bottles from metal  containers.  Thus,  acetone blanks shall
                                         >
be run prior to field use and only acetone v/ith low  blank values
(< 0,001%) shall  be used,
     3.3  Analysis.
     3.3.1  Acetone—Saife as 3.2.1.
     3.3.2  Desiccant—Anhydrous calcium sulfate,  indicating type.
4.  Procedure
     4.1  Sampling.  The sampling shall be conducted by conpetent
personnel experienced with this test procedure,
     4.1.1  Pretest preparation.  All the  components shall  be main-
tained and calibrated according to tna procedure described  in
APTD-Q57G, unless otherwise  specified herein.
     Weigh approximately 200-300 g of silica gel in  air tiaJrc con-
                                                                
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 labol  the slurping containers  (glass  or plastic potri  dishes)
 and l,o^p the filters in those  contsinars at  all tipcs  except
 during sampling and veicjhing.
      Desiccate the filters  ai  20 +  5.6ฐ  C (68 ฑ 10ฐ  F)  and  ambient
             ^
 pressure for'at least 2^ hours and  veiqh at  6 or more  hour  inter-
 vals to a constant i,eight,  i.e., 5  0,5 ng change from  previous
 weighing, and record results to the nearest  0.1 jug.  During each
 v/eighing the filter must not be exposed  to the laboratory atrnos-
 phere for a  period greater  than 2 minutes and a relative humidity
 above 50%.
      4.1,2  Preliminary deteminations.   Select the  sampling site
 and the minimum number of sanpling  points according  to  Hethod 1 or
 as specified by the Administrator.  Male a projected area model of
 the probe extension-filler  holder assembly,  with the pi tot  tube
 impact openings positioned  along the  centerline of the  stack, as"
 shovn in Figure 17-2.   If the  estimated  cross-section blockage,
 calculated as  shovn in Figure  17-2, exceeds  3 percent of the duct
                                                                    ,j
 cross sectional area,  then  either one of the following  shall be  **"
 done:   (1) a suitable  out-stack filtration method can be used
 instead of in-stack filtration; or  (2) a special in-stack assembly,
*designed to  minimize blockage  effects, can be used.  For details
 concerning the latter aporoach, consult  uith the Administrator.
      Determine the stack pressure,  temperature, and  the range of
 velocity heads using Tethod 2', determine the moisture content using
 Approximation  I'ethod 4 or its  alternatives for the purpose  of making

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                          G.U
                                                     X    /CC5
ป >   or
— *.ป    ^^ ? e.f ~. ft- ~
                                      or    a.
                                       .^-  c^-^C

-------
iso!inetic stapling rate calculations.   Estir'^tas  ray be usrd.
However, final results nil be based on actual  ncosurersnts radc
during the test.
     Select a nozzle size based on tha  range of velocity heads such
that it is not necessary to change the  nozzle size in order to main-
tain isoKinetic sampling rates.  During th'e run, do not change the
nozzle size.   Ensure that the differential  pressure gauge is capable
of measuring  the minimum velocity head  value to in thin 10^, or as
specified by  the Administrator.
     Select a probe extension length such that all  traverse points
can be sanpled.  Consider sampling from opposite sides for large
stacks to reduce the length of probas.
     Select a total sampling tirre greater than or  equal  to the
m'ninurn total sampling tin>e specified in the test  procedures for
the specific  industry such that the sampling time  per point is not
less than 2 min,  (or some greater time  interval if specified by the
Administrator) and the sariple volume taken  will exceed the required
                                                                 4ฃ
minimum total gas sample volume specified in the test procedures for
the specific  industry.  The latter is based on  an  approximate average
sampling rate.  Note also that the minirum  total sample  volume is
corrected to  standard conditions.
     It is recoirnended that half-integral or integral  numbers of
minutes be sampled at each point in order to avoid timekeepinq errors.
     In some  circumstances, e.g.,  batch cycles, it  may be necessary
to sample for shorter times at the traverse points  and to obtain

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smaller gas sample voltes.   In tbosa cases,  the  Administrator's
approval must first be obtained,
     4.1.3  Preparation of collection train.   During  preparation  and
assembly of the sampling train, keep all  openings where  contanina-
tion can occur covered until  just prior to assembly or until  sampling
                                          f
is about to begin.
     If impingers are used to condense stack  gas  moisture,  prepare
them as follov/s;   place 100 ml  of v:ater in each of the first  two
impingers; leave the third iropinger erpty; and transfer  approximately
200-300 g or more, if necessary,  of prei.eighed silica gel from  its
container to the fourth irpinger; alternatively,  if a balance is
available in the field, the silica gel  can bs weighed out in  a  tared
inpinger, and its weight gain deterninec!  in the field.   Place the
silica gel container in a clean place for later use in the  sample
recovery.  If soma weans other than ir.ping&rs is  used to condense'
moisture, prepare the condenser (and, if  appropriate, silica  gel  for
condenser outlet) for use.
                                                                rf*' '''
     Using a tweezer or clean disposable  surgical gloves, place ar1-
labeled (identified) and weighed  filter in the filter holder.  Be
sure that the filter is properly  centered and the gasket properly
placed so as not to allow the sample gas  stream to circumvent the
filter.  Check filter for tears after assembly is conpleted.  Mark
the probe extension with heat resistant tape  or by some other method
to denote the proper distance into the stack  or duct for each sampling
point.

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     Unices otnr.-.-ire specifi_d b_> the Ad.i'.i'islrator, attach a
ler pei ฃ tur e sense1-' tc ihe prcLc z:- tension so ihcit the sensor
extends Ley one! tho leading ec'nc oT the prche extension and doss
not touch any metal,   The sensor should be positioned at least
1.9 cm (0,75 in.) frou both the pi tot tube and probe nozzle to
             j
avoid interference with the gas flow {see 'Figure 17-1).
     Assemble ths train as in Figure "17-1, using (if applicable)
a very light coat of silicons grease on all  ground glass joints and
greasing only the ou^er portion (see A?TD-C5?G) to avoid possibility
of contamination by the silicons grease.   Place crushed ice around
the impingers (if applicable),
     4,1,4  Leaf; check procedure—After the  sampling train has been
asserbledj  a leak check of the filter holder shall  be conducted as
follows:  Plug the inlet to the probe nozzle with a material  that
will be able to withstand the stack tenpsrature;  alternatively, the
probe nozzle can be removed and ths inlet to the filter holder
plugged.  Insert the holder into the stack and vait approximately
5 minutes (or longer, if necessary) to allow the systen to coine tfo-
equilibrium v/ith the temperature of the stack gas stream.   Turn on
the pump and drau 2 vacuum of et least 380 ran Hg (15 in, Hg).   De-
termine the leakage rate, if any,  A leakage rate in excess of 4^
of the average sampling rate or 0,00057 m /min, (0.02 cfn), which-
ever is less, is unacceptable.
     The follo'./ing leak check instructions for the sampling train
described in APTD-0576 and APTD-0531 may be helpful.  Start the pump

-------
with by-pass valve fully op^n and coarse adjust valve  completely
closed.  Partially open the coarse adjust valve- and  slowly close
the by~p?ss valve until 380 im Hg (15 In. Hg)  vacuu-> is  reached.
Do not reverse direction of by-pass valve-   If 380 nn  Hg  (15  in,
Hg) is exceeded,  either leak check,at this  higher vacuum or  end
the leak check as sho./n below and start over.
     1,'hen the leak check is completed, first slowly  remove the plug
from the inlet to the probe nozzle and immediately turn  off the
vacuum pi/np.  This prevents the water in the condenser from being
forced backward and keeps silica gel from being entrained backward.
     Leak checks shall  be conducted as described whenever the train
is disengaged, e.g., for silica gel or filter changes  during  the
test, prior to each test run, and at the completion  of each test
run.  If leaks are found to be in excess of  the acceptable rate, the
test v/ill be considered invalid.  To reduce  lost tirra  due to  leakage
occurrences, it is reconmended that leak checks bs conducted  between
port changes at the highest vacuum reading drawn during  that  sampling
                                                                at
traverse.
     4,1.5  Particulate train operation—During the  sanpling  run,
maintain the isokinetic sarpling rate to v/ithin 10ป  (unless otherwise
specified by the Administrator) of true isokinetic.
     For each run, record the data required  on the example data
sheet shown in Figure 17-3.  Ba sure to record the initial  dry gas
meter reading.  Record  the dry gas meter readings at the  beginning
and end of each sanpling time increnent, vhen changes  in  flow rates

-------
  LOCATION.
  OPERATOR.
\DATt	
  RUN NO	
  SAKV'LE DOXNO,.
  PITOT TUBE COEFFICIENT, Cp,
                                           SCHEMATIC OF STACK CHOSS SECTION
DAOOiVIETniC PRESSURE,
ASSUMED MOISTURE. %_
NOZZLE IDENTIFICATION NO
AVCHAGC CALIGHATED NOZZLE
                                                                                   LEAK RATE, m3/imn{cfm)_
                                                                                             ', HATCIV1AL-L.
                                  . cซ 
-------
  are rude, and when sampling is halted.  Take other data point
  readings at least once at each sanple point during each time
  incrcrent and additional  readings \'hen significant changes (207*
  variation in velocity head readings) necessitate additional
  adjustments in flov; rate.  Level  and zero the rianorreter.
       Clean the portholes  prior to the test run to minimize the
  chance of sampling the deposited  material.  To begin sampling,
  remove the nozzle cap and verify  that the pi tot tube and  probe
  extension are properly positioned.  Position the nozzle at the
  first traverse point with the tip pointing directly into  the gas
  stream.  Immediately start the purp and adjust the flew to isokinetic
  conditions.   Nomographs,  which aid in the rapid adjustment of the
  isokinetic sampling rate  without  excessive computations,  are availa-
  ble for use i.'henever the  Type S pi tot tube coefficient  is C.85 ฑ 0.02,
  and the stack gas equivalent density (polecular v;eight)  is 29 ฑ 4.
-  APTD-0576 details the procedure for using these nomographs.  If C
  and Mj are outside the above stated ranges, do not  Ge  the nomograph r.
  unless appropriate steps  (see Reference 7.7] are taken  to compensate
  for the deviations.
       V'hen the stack is under significant negative pressure (height
  of impinger stem), take care to close the coarse adjust valve before
  inserting the probe into  the stack.  If necessary,  the  pump may ba
  turned on with the coarse adjust  valve closed.
       llhen the probe is in position, block off the openings around the
  probe and porthole to prevent unrepresentative dilution of the gas
  stream.

-------
     Traverse the SLC-.C|. cress scci,ior,. as reoir'red by S'cthod 1 or
as specified by the AJmnistputor, being cateful not to btrtp the
probe nozzle into the stack v.'alls \ hen s?rpling near the vails or
when removing or inserting the probe extension through the port-
holes, to ninimze chance of extracting deposited natcrial,
                                          *
     During the test run, take appropriate steps (e.g., adding crushs
ice to the inpinger ice bath) to maintain a temperature of less than
20ฐ C (68ฐ F) at the condenser outlet; this will prevent excessive
moisture losses.  Also, periodically check the level  and zero of the
manometer.
     If the pressure drop across the filter becomes too high, rraking
isokinetic sampling difficult to maintain, the filter may be replaced
In the midst of a sample run.  It is recoTrnonded that another com-
plete filter holder-nozzle assembly be used rather than attempting
to change the filter itself.  After the new filter holder-nozzle
assembly is installed, conduct a leak check.  The particulate weight
shall include the summation of all filter asser.bly catches.
                                                                 iff
     A single train shall be used for the entire sample run,  except
for filter and silica gel changes.  However, if approved by the
Administrator,  two or pore trains nay be used for a single test run
when there are ti;o or pore ducts or sampling ports.  The results shal
be the total  of all sampling train catches.
     At the end of the sample run, turn off the pump, remove the
probe extension-filter holder-nozzle assembly frorc the stack, and
record the final dry gas meter reading.  Perfom a leak check at a

-------
     "- equal to or greater t^en the nrxirur reached during s:rp-
ling.  Calculate percent isckmetic (sc2 calculation section) to
determine vhether another test run should be rade.   If there is
difficulty in n.eintaining isokinetic rates due to source conditions,
consult v/ith the Administrator for possible variance on the iso-
                                         r
kinetic rates,
     4.2  Sample recovery.   Proper cleanup procedure begins as
soon as the probe extension-filter holder-nozzle  assembly is
removed from the stack at the end of the sampling period.   Allow
the assembly to cool,
     Uhen the assembly can be safely handled,  v/ipe  off all  external
participate matter near the tip of the probe nozzle and place a
cap over it to prevent losing or gaininq participate natter.  Do
not cap off ths probs tip tightly v/nile the sairpling train is
cooling dov/n as this would create a vacuum in  the filler holder, and
force condenser water backward.
     Before moving the sample train to the cleanup  site, disconnect
                                                                *r
tha filter holder-proba nozzle assembly from the  probe extension;
cap the open inlet of the probe extension.   Be careful  not to lose
any condensate, if present,   Remove the umbilical  cord from the
condanser outlet and cap the outlet.   If a flexible line is  used
between the first impinger or condenser and the probe extension,
disconnect the line at the probe extension and let  any condensed
water or liquid drain into the impingers or condenser.   After
vnping off the silicons grease (if applicable) cap  off the condenser

-------
inlet.  Ocuncl class storr>c>*s, plestic cc"^,, cr sunn caps (v;icf-
ever are appropriate) may h? iiscd to close tr^se cpsninqs,
     Transfer both the filler holder-p;obe nozzle ?rd condenser
assemblies to the cleanup area.   This area should be clean and
protected frcpi the wind so that the chances of coritar'matina or
losing the sample t'ill be nininized.
     Save a portion of the acetone used for cleanup as a blank.
Place about 200 ml of this acetone taken directly fro^ the v.-ash
bottle being used in a glass sanple container labeled "acetone blank."
     Inspect the train prior to and during disassembly and note any
abnorrral conditions.   Treat the samples as follows:
     Cpntain_s_r__Kg_.. 1.  Carefully remove the filter from the filter
holder and place in its identified petri dish container.   Use a pair
of tv/eezers and/or clean disposable surgical gloves to handle the  ••
filter.  If it is necessary to fold the filter, do so such that the
participate cake is inside the fold,  Cuantitatively remove any
participate matter and/or filter which adheres to the filter holder ''
gasket by carefully using a dry nylon bristle brush and/or a sharp-
edged blade and place into this container.  Seal  the container.
     Container T'c. 2.  Takina care to see that dust on the outside
of the probe nozzle or other exterior surfaces does not get into the
sanple, quantitatively recover ^articulate ratter or any cor.densate
                                                                •
fron the probe nozzle, fitting, and front half of the filter holder
by washing these components v/ith acetone and placing the wash into
a olass container in the follo'.nna manner; note that distilled water
ray be used instead of acetone wlipn approved by the ^dmnistrator

-------
or shall be used wj.en specified ty th" /cnmstrator, in these
cases, sa^e a water blank end follow Wnmstrator's circctiors
on analysis;
     Carefully rercve the probe nozile ard clean the inside surface
by rinsing wfth acetone frcm a \,ash bottle and brushing with a nylon
                                         f
bristle brush.  Brush until acetone rinse sho-vs no visible particles,
after which make a final rinse of the insic'e surface v/ith acetone.
     Brush and rinse with acetone the inside parts of the fitting
in a similar way until no visible particles renain.   A funnel rcay
be used TO aid in transferring liauid washes to the container.  Rinse
the brush with acetone and quantitatively collect these washings in
the sample container.   Between sampling runs5 keep brushes clean
and protected from contamination.
     After ensuring that all joints are wiped clean of silicons
grease (if app"Yice.ble), clean the inside of the front half of the
filter holder by rubbing the surfaces with a nylon bristle brush
and rinsing v/ith acetone.   Pinse each  surface  three times or more  ''
if needed to remove visible particulate.   Fake a final rinse of the
brush and filter holder.  After all acetone washings and particulate
matter are collected in the sarrple container, tighten the lid on
the sarrple container so that acetone  will not leak out when it is
shipped to the laboratory,   f'ark the  height of the fluid level to
determine whether or not leakage occurred during transport,  Label
container to clearly identify its  contents.
     Container F-'o.  3,   Note color of  indicating silica gel  to deter-
nine if it has been completely spent  and make a notation of its

-------
condition.  Transfer trip silica ccl bac'-', to its crunr,-cl  centalTT
and seal.  / funnel r^ rake it rosier to POL"" the silica eel
without spilling, end a rubber policerran pay be used as an aid
in removing the silica qel.   It is not necessary to remove the
small amount, of dust particles th~t may adhere to the walls ?nd
are difficult to remove.  Since the gain in weight is to  be used
for moisture calculations, do no:, use any \ictcr or other  liquids
to transfer the silica gel.   If a balance is available in the field,
follow the procedure under "Analysis."
     Condenser water.  Treat the condenser or inpinger water as
follows:  make a notation of any color or ft In in tha liquid catch.
Measure the condensate to i.ithin t 1  ml  by usina a graduated cylinder
or, if available, to within  + 0,5 p by using a balance.   Record the
conde^sete volume or weight.   This information is required to  cal-
culate the moisture content  of the effluent gas.   Discard the
liquid after rressuring and recording  the volurs or weight,
     4.3  Analysis.  Record  the daza  required on the exarrple sheet
shown in Figure 17-4,  Handle each sanple container as follows-  -^
     Container Kp.  1.  Leave in shipping container or transfer the
filter and any loose particulate from the sarple container to  a
tared glass weighing dish and desiccate for 24 hours in a desiccator
containing anhydrous calcium sulfate,   Ueigh to a constant waight
and report the results to the nearest 0.1 rg.   For purposes  of this
section 4.3, the term "constant weight"  means a difference of  no
more than 0.5 pq or "IE of total veight less tare weight,  whichever
is greater, between two consecutive weighings, with no less  than 6

-------
Run f.'o
RD|Jlr,2 Uu 'ilJitV.
Amount ti7-.iu lc>t ilunrjj transport


Aeatone hb..k volume, ml


Acetone ir-'jiii volume, ml	
Acetons bbnl, conceiitraticn, no/nig (equation 5-^)


Acctcnc ivzsh hl^nJ;, mg (cLju'dimn 5-5)	
CONTAINER
N'JiY.BcR
1
•2.
TOTAL
WEIGHT OF PARTICULATE COLLECTED,
mg
FIWAL \, EIGHT


^H^xdl
TARS V.'cIGHT


^I^xCC
Less acetone blank
Weight or p^rticu'aie matter
WEIGHT GAIN




1

FIWAL
INITIAL
LIQUID COLLECTED
TOTAL VOLUME COLLECTED
VOLUP'E OP LIQUID
WATER COLLECTED
<^' ' i- ,
i.'. ";;:c:fl
VO.U', ฃ.
ml




SILICA GEL
\iEIGHT.
g



g- ml
       CONVERT ViEIGHT OF WATER TO VOLUVE BY DIVIDING TOTAL './EIGHT
       INCREASE BY DENSITY1 OF WATER tig/ml),


                                    INCREASฃ-9   - VOLU.VE WATER! mi
                                       1 g/ml

                                /7-V-
                          Figure C^-r.  Analytical dala.

-------
 hours of desiccation lire LIT, con veighinrs tin;! no rorc then 2
 rnrutes exposure to tre laboratory atrospherc (rust be less than
 50% relative humdity) durirq \eichino.
      Cent c^irer To,  2,   note level of liquid In container and
 confirm on analysis sheet whether or not leal age occurred during
 transport.  Measure the liquid in this container either volume-
 trically to ฑ 1 ml or gravinetrically to ฑ 0,5 g,   Transfer the
 contents to a tared 250 ml beaker, and evaporate to dryness at airbient
 temperature and pressure,   Desiccate for 24 hours  and veiah to a
 constant weight.  Report the results to the nearest 0,1  mo.
      Container f'o. 3.  Weigh the spent si lice ael  to the nearest
 0.5 g using a balance.   This step IT ay be conducted in the field.
      "Acetone Flank" fejvtainer.   f'easurc acetone in this container
 either volurnetrically or gravinetrically.  Transfer the acetone to
 a tared 250 nl beaker end evaporate to dryness at  ambient temperature
 and pressure.  Desiccate for 24  hours and v/eiah to a constant weight.
.Report the results to tha nearest C.I ng.
                                                                   <*" '
 5.  Calibration
      flaintain a laboratory log of all calibrations.
      5.1  Probe nozzle.  Usinq a micrometer, measure the inside
 diameter of the nozzle to the nearest 0.025 nm (0.001 in.),  flake
 3 separate measurements using different diameters  each tire and
 obtain the average of the neasurenents.  The difference between the
 high and low numbers shall not exceed 0,1 rrn (0,004 in.).
      Uhen nozzles become nicked, dented, or corroded, thsy shall
 be reshaped, sharpened, and recalibrated before use.

-------
     Cach nozzle 11 fill tc pcrroi -'>tly ere! t.-npualy u'e-.tific-d.



     5.2  Pi tot tube,  "He pitox. tubs sK=.ll fce calibrated scpcrctcly



(i.e., apart from its assently configursficr) according to the pro-



cedures outlined in I'ethod 2 for calibration of isolated Type S pitot



tubes.

                                         *•

     5,3  Dry gas meter end orifice reter.  Both reters shall be



calibrated according to the procedure outlined in PPTD-C576,  I/hen



a diaphragr, pmrp is used, assure that there is no leak.



     5.4  Temperature cauqes.  Calibrate dial and liouid filled tulb



thermonetsrs and thernocouple-rotentioneter systens aaainst mercury-



in-glass therir.orreters.  Ice btth and boiling v-'ater (corrected for



barometric pressure) are acceptable reference points.  For other



devices, check witn the /"'dn.imstrator.



6,  Calculations

                                                               •^

     Carry out calculations, retaining at least one extra decimal



figure beyond that of the acquired date.  Round off figures after



final calculation.



     6.1  Nomenclature


                                            2    2
t    A   = Cross sectional area of nozzle, m  (ft )
      n


     B   = Hater vapor in the aas stream, proportion by volurre



     C   = Acetone blank residue concentration, mg/q
      a


     c   = Concentration of particulate natter in stack oas, dry basis,



           corrected to standard conditions, q/dscm (p/dscf)

-------
v    = Staci o?s velocv.y, calc^l->teu ty f'jt'roJ 2," Eouation 2-7
       usino data obtsir^d frcn I'cti'cd 17, rr/src (ft/sec)
I,1    = l.'eipht of resides in acetone i ash, nq
 3
&H   - Average pressure chffc-rential across the criflcs rreter
       (see Figure 17-3), rn H2C (in, H20)
p     = Density of acetcne, rg/nl (see label on bottle)
'w
           = Density of vater, 1 a/ml (0,00220 Ib/nl)
     0     = Total sampling tire, nrin.
     "13.6 = Specific gravity of mercury
     60   = sec/min
     100  = Conversion to percent
     6.2  Average dry aas meter terrperature and average orifice
pressure drop.   See data sheet (Figure 17-3),
     6.3  Dry gas volume.  Correct the sairole volure reasured by the
dry pas neter to standard conditions (20ฐ C, 760 nr. Ha or ฃ8ฐ F,"
29.92 in. Hg) by using Equation 17-1.
Xstd)
         =  V
                  m

                                std
                                              = K V.
                                                   bar
                                           Equation 17-1
where:
     K
               0.3855 ฐK/tnm Hg for metric units
               17.65 ฐR/in. Hg for English units

-------
I        = Percent  of  isc! v,:Uc
m        = Total s'-'Q'jnt of pฃ.rriculcte ratter  collected,  rrg.
t-i        = I'oleculsr veight of water, 18 q/q-trale  (1G Ib/lb-trole)
m        = Pass of  residue of acetone efter evaporation,  rg
 s
P.      '" = Barometric  pressure et the serrplina  site,  rm Hg (in.  Ha)
                                    '                     "
p        = Absolute stock ge.s pressure, mn Hq  (in.  Hq)
P td     = Standard absolute pressure, 7CO rm  Ha  (29,92 in.  Hg)
R        = Ideal qas constant, O.C6236 irrn Hg-m3/ฐK-9-[r,ole  (2KC3 in.
           Hg-ft3/0P-lb-nole)
T        = Absolute average dry oas treter trrrperature  (see Fipure 17-3
T        = Absolute average stack pas temperature  (see  Figure 77-3),
           ฐK  CฐR).
T td     = Standard absolute temperature, 293ฐ  K (528ฐ  R)
V        = Volune of acetone blank, ml
 3
Va,,      = Volume of acetone used in v/ash, nl
 ow
V-,       = Total volurre of liquid collected  in  condenser and   „,
                                                           *,
           silica gel  (see Figure 17-4), nil,
V        = Volume of aas sarple as nsasured  by  dry aas  mater,
           dcm  (dcf)
V / t ,v  = Volume of pas sarrple reasured by  the dry qas meter
           corrected to standard conditions, dscm  (dscf).
V / t .>  = Volune of \:ater vapor in the gas  sample corrected  to
           standard conditions, sen (scf).

-------
          Yolurc of \ atcr varn ,
     fr(std)  *  Vlc  flfi'1^4  =   Kl'lc    Cation 17-2
     where

                                         X


          K = 0,00134 m3/nl for retric units



            = 0.0472 ft3/ml for Fnqlish units



     6,5  f'oisture content,
     B    ซ    	"l5|dL_ซ	               Equation 17-3

      1/5      Vm(std)  +  V(std)
     6.6  Acetone blank concentration,
               3
                                                Equation 17-4
     6,7  Acetone v/ash blank.




     Ha  -  Ca  Vaii  Pa                         Equation  17-5
      3      3   <3V/   a




     S.8  Total particulate veight.  Determine the total  participate



catch from the sum of the weights obtained from containers  1  and 2



less the acetone blank (see Figure 17-4),



     6.S  Particulate concentration.






     c$  =  (0.001 g/rncj}  (mn/Vn(stdp           Equation  17-6

-------
6,10  Conversion
From
scf
g/ft3
g/ft3
g/ft3
To
n3
gr/ft3
Ib/ft3
g/m3
fuU
0.
15.
2.
35.
.inV' bv
0283
4
205 x 10"3
31'
6.11  Isokinetic variation,
6.11.1  Calcul aliens from rev; data.
      100  Ts   [KV1c  +   (Vn/Tn)
   =
                                           Equation 17-7
vjhere:
     K * 0.003^6 irn Hp-n3/rnl-ฐK for irstric units
       = 0.00267 in. Hq-ft3/r,l-ฐP for English  units
6.11.2  Calculations frcn  internechate values.

                           P...J  100
       Tstd vs 8 An Ps  60
                                            Equation 17_8
v/here :
     K = 4.323 for metric units
       = 0.0944 for English units

-------
               APPENDIX G
PARTICULATE  SAMPLING FIELD DATA  SHEETS

-------
 PROJECT  'I
               GEORGE  D-  CLAYTON & ASSOCIATES
             EXHAUST  GAS  VELOCITY AND FLOW RATE
              / / j'f   // -c   •"  ,       CREW  /"//'/
 Sampling Station.
                             L. <•- ~~  D ate
                                                            lime  / C
Test No, P/cV^--> rr /•/'•.
•"" 	 ~ • '
Sampl ing
Paint
/. — /^
(,- / f.
,/
JC
7
S
7
c-
^
^
3
^
I



Veloc i ty
Pressure
(In.H20)
ฃ-#r"
C*fr
& - ?ft
C-&/
0- ^
{<* >v
c:
e 
*•;
^*
f^
iT'"^ s
* *
<*<>'
C/ c
"?<>
c,
<->
c/^



Pitot Tub
Uncorrect ed
Vel ocity
(Ft/sec)
// c; f
4&5 ''
ฃ2'V
\
<^2 . S
^0, i
tfV.S -
*/6<3
ฃ/ ^ j
^j
(/
"7
c-
s
6
-*)
x-'-ป
/

/3*-)-J-x "• ^'

Velocity
Pressur e
&* 
***
9<
9>
9>
y
•


. ,/cx-v - 7

Uncorrected'
Velocity
(Ft/sec) ,1
i>2 9.
•-- - ^
**~j C*^ ป^\
'o- >
^6 *2
. +*
'*$ '>
•^^.S
^ ^
"5 ^
:^'^.2
^!j,%
if!tLf
r •


 Stack Wet Bulb  Temperature,  (ฐF)
 A.  Barometric  Pressure,  (In.Hg)
                                         Stack Dimensions
     Static Pressure  of Stack Gases,
     Pitot Tube  Correction Factor
                                                               /.
     Specific Gravity  of Stack Gases Relative to Dry Air
     Absolute Pressure of Stack Gases = A +  (B/13.6), (In.Hg)   ฃ3*0
     Average Uncorrected Velocity,  ( f t / a e c ) ^ , ^ฃ a r  60  *  F, (ft/min)

     .Corrected  Velocity = F * C.
                          ••^
 H
-I
Area of Stack,  (ft2)
       Gas Flow Rate
                            G *  H,  (ACFM)
;J,".'Average Stack Temperature,  (T)
_- : '*^' -S—"i _ , 4;'r &^' - "-<•-_- -   > - ' - --• •- .-^7 '-/„ -
i"K .!ฃr;Standard

-------
   PROJECT
                    GEORGE  D-  CLAYTON & ASSOCIATES
                  EXHAUST  GAS  VELOCITY AND FLOW RATE
                                        CREW   /- &P
   Sampling Station
   Test No S,;•<„,• VJi
                                       Date
                               Time	/,
Pitot Tube No.   /
                                                   Manometer No.
Samp ling
Point
U' lฃ
//
/&
9
S1
/7
/
c
^
&
/
5
•f>
1



Velocity
Pressure
(In.H20)
C.'S?
I)- I f/
o* & c
6.&?
C~ (r 7
0-L ^
C^ C C
$- *J.2
C- ซ?
f. , f
6 .. $ /



DB
Temp
(ฐF)
%
?Lr
?L
%
(/(
K
C?C-
CK
${-
ฃiC-

-------
     PROJECT
                    GEORGE  D-  CLAYTON & ASSOCIATES
                  EXHAUST  GAS  VELOCITY AND  FLOW RATE
                  I f                     CREW    ฃ"-'  A-
Sampling  Station
Test No, Tf-^+'it
                        /" J* /^ d
                          _   --
                                        Dat&
                                                                 Time
                                                                       ,,
                              Pitot Tube No .   2 J
                                                         Manometer No.
Samp ling
Point
_ฃ '
Z.
3
N
T
ฃ.
7
y
-7
i 0
/ f
/ ฃ•



Veloc i ty
Pres sure
(In.H20)
V tO
j-r
i Iff
,*o
i
,2*
,ro
. 21
,iฃ
i7
, ?>
^l-
. 20
- S"2/,:
, i i
, 1 ") I Z i
DB
Temp
CF)
t>"
E b
i •)'
S i"
_ ^s"
c<-
_S bT
•x ^
it"
f >'

,o-^ x>
^ / <- /
•.- j "' -—
^5 -
o r >
^l/ --"
-Dt :/


n. ซ. '
Sampl ing
Point
^ S ป
z
3

, ji^r

DB
Temp
(ฐF)
S^-""
?i-
3J~
fi~
?r
*y
^r
3J>
S b~
5 ^
^^'
sr



Uncorrected
Velocity
(Ft/sec) J
\
-^ ^
3a.5
H ^}
^ 1
-57 'i
^7 0
-/ I
Jt 5
^•f
- ^r.3
^/ 5-
•^ i
s
.V*
J*

     Stack Wet Bulb Temperature,  (ฐF)
     A.   Barometric Pressure,  (In.Hg)
     B -
                                               Stack Dimensions
                                                                         '
Static Pressure  of Stack Gases,  (In . H20)
Pitot Tube  Correction Factor    ฃ/ 3  >
                                                  ~  ^ . 3
     D
     E
     Specific Gravity  of  Stack Gases Relative  to  Dry Air	/	
     Absolute Pressure  of Stack Gases = A +  (B/ 13 . 6^ (In. Hg)  3-? . a ^  •
     Average Uncorrected  Velocity,  (ft/sec)^^ , y^^gr 60 * F>(ft/min)
.G •  'Corrected Velocity  =  F * C

H-   Area of Stack,  (ft2)      C.
                                                      (ft/min)
._, VI. (  Actual Gas Flow  Rate * G * H,  (ACFM)
   "^ J , -* Aver age Stack Temperature, (ฐF)

-------
                     GEORGE D- CLAYTON  &  ASSOCIATES
                  EXHAUST GAS VELOCITY AND FLOW RATE
PROJECT
 Satnpling Station
 Test No. •?-,.,**
CREW   /j k i^ / "7~J
     	_^y
      I/ <."7 /7ฃ	
                                        Date
                                                              TimeJ/Vr -- /-Z.JO
                                     .
                              Pitot Tube No,   ;
                                                     Nanometer No.
Samp 1 ing
Point
13 ,
Z
3
V
r
4
7
S
=1
fy
l<
'ฃ



Velocity
Pr es sure
(In-H20)
•4 ov
i J^
ซซฃ>
i ?C
, y~
, sr
. 33
. ?v
V Jlf
7, 1 ..
v2ซ=i.
. tr
-/ . eo//i
, 1 31
, ^ 7 V M
DB
Temp
(ฐF)
^V
vr
'* s~
^ \"
5^
C <•
? r
sr
V "."
4 r
•is
V V

< >
-> 'n'
7i-
Uncorrect ed
Velocity
(Ft/sec)
^/"/ 1 /
4- •/
^j? '•>
>fr <
Hf i
4r !
^ (,
^/r
y/ r
27, 'i
3t '^
31 'i

3V 6 f
•9
Sampl ing
Point
S i
2
3
V
5
i'
v>"
?r
&r
T-V"
? r
5r



Uncorrect ed'
Velocity
(Ft/sec) ป
3^^
^S
^7 f
ซ& r
^3^
^•/,S
^ '-y-
^ic i
^/ 7
4; 'j
^^
5S?
ฃ<• *
*;

Stack Wet  Bulb Temperature,  ("F)	
A.  Barometric Pressure,  (In,Hg)	
B.  Static Pressure of  Stack Gases,  (In,H20)
    Pitot  Tube Correction Factor	  ^f "2,
                                               Stack Dimensions	/
 C.
 D.
•E.
 F.
                                           ^
    Specific Gravity  of  Stack Gases  Relative to Dry Air 	/
    Absolute Pressure  of Stack Gases =  A + (B/13. 61/., (In , Hg)	^
    Average Uncorrected  Velocity,  (ft/see) t^rffi^ffi0^ 60 * F,(ft
                                                                    . Q
     Corrected Velocity  =
     Area  of Stack,  (ft2)
                           F * C
                                                   (ft/mitt).
                                      f 2 Z7
 H.
:i/\ Actual Gas  Flow Rate = G *  H,  (ACFM)
 J.i-Average  Stack Temperature,  (ฐF)
GDC-2

-------
                            SAMPLING TRAIN DATA
Source Designation;
Ceflt Number;
Field Person:
                                        Filter  Heater  Setting:
                                        Probe Heater  $ettingr_
                                        Nozzle  Number;
                   A •
Filter Nuiaber:_
Barometric Pressure  ("Hg):_
Stack Static pressure  ("I^C
Stack Dimensions:	    J^ '
Plume Appearance;	~~
                        6 7 -
                               . 27.3,3
                               -/ 6
\mbient Temperature(ฐP):
Record all Data Every 	
ฃ/*SQ T*/Ts x
                               Minutes
                               -(in.):ฃ
        Pitot Tube No.A? ,Corr,Factor:
        Meter Box No ./&^*v?> Corr. Fae
        Meter Isokinetic  Factor;	/
        Assumed Moisture (X) :	/. y
        Condensate Volume(ml):	
        Silica Gel Weight Gain(g);
        Leak Rate &.0I    CFM  at
                       a*
                                             V??#      **/06   W/w
Trav-
erse
Point
 No.
        Tine
     Samp-
      ling
     (rain)
          Clock
                Velocity
                ?r es sure
                 <"H20)
                        Stack
                        Temp
                                 Dry Gas  Meter
Vo lume
 (ft3)
                                        Teup (DP)
                                       Inlet Outle c
     Orifi.ce
     Pressure
     Differ-
     ential
Filter
 Box
 Temp
                               Last
                               Imp
                                Gas
      lemp Pre
                                                               CF
                                                 Sampling
                                                  Train
                                                  Static
                         ssure
                        ("Hg)
      o
                                                               BO
      s
                                       toy
                                                 ฃ•77
   A?
      16
                0
iZi.
        /n
9$
      7$
                               3% ??
                                       //y
                                            10Z
                  S-/3
          /QUO
                                       /3.I
                                            103
                  3. 92.
                       3,3
          /Qtt?
                         lo
                                                                   *'3< 0
V ff
         |7งrvf
                 $.ฅ
                         IOS
                                             "tL
                  *•/#
                   So
                                       /a/
                                            113
                                                               90
                 0,33
                                                  /.ft,
                                                               92.
                                    2.0
                 0,30
                                                                   2*1
                         10 -f
               !.V

                             --  aW/0#fJ#i*LX00S   -~~.r~.   ,  _--_>.
                         I^/^PปMJ '  Clayton  Environmental Consultants, Inc.

-------
         ฃff>
                            SAMPLING TRAIN DATA

                               & M ฃL
Source Designation:
)ate:  _	ฃ_
Teat  Number;	j/
Field  Person:
filter Number:
Barometric  Pressure
                       7-
                    ("Hg):	
Stack Static  Pressure  ("H^O)?  — /.
Stack Dimensions;	
plume Appearancer	
Vmbient  Temperature("F):
Record  all  Data  Every
                              Minutes
                        Filter  Heater  Setting:	--^
                        probe Heater  Setting;	—
                        Nozzle  Number:	,Dia.(in.);
                        Pitot Tube  No. /0,Corr.Factor:
                        Meter Box No^fxte-.!, Corr.Factor:
                        Meter Isokinetic  Factor:	^
                        Assumed Moia ture (7.) :	
                        Condensate  Volume(ml):	
                        Silica  Gel  Weight Gain(g):
                        Leak Rate  &\QQ^ CFM at
                                                                J'2- Z—
                                                                        Hg
Tr av-
er se
Point
 No.
        Time
     Samp-
     ling
     (rain)
          Clock
Veloci ty
pr es sure
 ("H20)
                        Stack
                        Temp
                                 Dry  Gas  Meter
Volume
 (ft3)
                                        Temp (ฐF)
                                       InletOutle t
Orifice
Pressure
Differ-
 ential
 ("H20)
Filter
 Box
 Temp
Last
Imp
Gas
lemp
Sampling
 Train
 Static
Pre ssur e
 ("Hg)
      to
                                                               13
                                                                    3.o
                 0.50
                                       /at
                                            //s
                                               72
  10
                                                                   3**-
                              97.39
   $
                        105
                                 . 03.
                       130
                                    3-2-
                                                 ^'57
                                       133.
                        \o<
                                       133.
                                                                   3,
                                       I3Z
                                                               76
                              1*3,19
                                       131
                                                               n
     it*
                                       131
     /to
                              I30M
                                ?   X

                                         ;<
                        Id**"-
                                                     y
                                                     ซ"y
                                                     /
                                                               _ *•
                                                                       ^
                                  Clayton Environmental Consultant3,L Inc.

-------
                             SAMPLING TRAIN DATA
Compnny:	
Source Designation:
Date :
                           frff t/_S &
Teet Number;
Field Person-
                                        Filter  Heater Setting:__
                                        probe Heater Setting;	
                                        Nozzle  Number;
                     ~> ,2 6 7 - 3 3
Filter Number:_
Barometric pressure ("Hg) :
Stack Static pressure ("H?0) ;  ~/,
Stack Dimensions:	/?  "  3Z Q
Plume Appearance:	      	~~
Ambient Temperature(ฐF);	
Record ail Data Every   jZ"
                               Minutes
                                     	,Dia. (In.) -j0. ?
                        Pitot  Tube  No, /ฃ>,Corr.Factor;
                        Meter  Box No .^ฃ^2, Corr. Factor:	
                        Meter  Isokinetic  Factor;   /"?/O
                        Assumed  Moisture (7.) ;    ^/ g g,
                        Condensate  Volume(ml):	
                        Silica Gel  Weight Gain(g):	
                        Leak Rate (0- OJ    CFM  at   /x*'
                                                                       "Hg
Trav-
 erse
Point
 No.
         Time
     Samp-
      ling
     (rain)
           Clock
Velocity
Pressure
 C"H20)
Stack
Temp
CF)
                                 Dry Gas  Meter
Volume
 (ft3)
                                        Temp(ฐF)
                                       Inlet Outlet
Orifice
Pressure
Differ-
 ential
Filter
 Box
 Temp
                               Last
                               Imp
                               Gas
      rempjPre
      CF)
Sampling
 Train
 Static
   ssure
                 0,55
                          /O
                              /J/.65?
                                                   3.2
  H
                                       MIL
                                                               70
  10
      10
                 0.53*
                   ฃ3
               jit
                                    3'**
                 O.S&
                        It*
                                       131
                                        133
                                        13?
      30
                                        135
     35
                        H*
                                                                   3-0
                              767-77
                                       131*
                                                 \.7l
                0>3/
                                       135
                        It*
                                       13V
                                                 1-29
                 Q.lb
                         H*
  ,   -    ^  -      ,
 i^sB -VE B- ACE^CTOT A i) ^S
                                  Clayton environmental Consultants t~

-------
                            SAMPLING TRAIN DATA
Company ;
Source Designation;
Test Number;
Field Peraon
                    - ,3 & 7 -ป
Filter Number ;     ,*
Barometric pressure  ("Hg) :
Stack Static pressure  ("H?0> :  ^- /j
Stack Dimensions i _ /
Plume Appearance: _
hmbient Temperature ("F );
Record all Data Every
                                   Filter  Heater  Setting?
                                   Probe Heater  Setting:
                                   Nozzle  Number; )V  , Dla , (In. ) ; _ct
                             Pltot Tube No. /&>CorrซFactor:O
                             Meter Box K o . jฃAteL~Ji9 Corr.Facto n(.
                             Meter Isokinetlc Factor; /
                             Assumed Holsfcure(%);	/,
                             Condensate Votutae (ml) ;	
                             Silica Gel Weight Gain(g);
               Minutes  Leak Rate
                                               CFM at
                                                                  "Hg
Trav-
 erse
point
 No.
   Tine
Samp-
 ling
(mln)
Clock
Velocity
Pres sure
 C"H20)
              Stack
              Temp
                 Dry Gas  Meter
Volume
 (ft3)
                             Temp (BF)
                                       In let Outlet
Orifice
Pressure
Differ-
 ential
 ("H20)
ilter
 Box
Temp
(•F)
iLast
Imp,
 Gas
remp[pre
(•F)
Sampling
 Train
 Static
   ssure
 ("Kg)
 s//
                                       3JJ.
                                                          10
                                       13$
                                                          76
                                                         3.*
   10
           0. ฅ3
                    1 90. 23
                                   .99
                              1
                                                               3,
                              /It. 1
                                  13*
                                       13*
     90
                                       ytf
                 &S3
                   It
                             13*
     /oo
                                                              3,6
                 0.37
                   II <
                                                         3.
     tie
                                  131
                                                         3,0
     It*
                                            1,5?
                                                         3-2.
     tea
                              /off-
                              \.*l 0-5"
       RACE -(TOTAL)
                         (i    5  5
                               lov-tj*  "•—-/^ ; •?  -  *-—_-- - --  ^*-. .•  . .v
                              '-"^Clayton Environmental Consultants, Inc.

-------
                            SAMPLING TRAIN DATA
Company :	
Source Designation:
                   P-3
Test  Number:	
Field Person:	
Filter Number; ^><.~ s-_  •- ' f /
Barometric  Pressure  ("Kg);
Stack Static Pressure  ("H2
Stack Dimensions ;    /*7 v
Plume Appearance:	•"
•Vrabienfc  Temperature("F):
Record  all  Data  Every
                             —/*
                         Minutes
                                  Filter Heater Setting;
                                  Probe Henter Setting:
                                  Nozzle Mumber:
                                                         , Dla. (in. ) ; &.
                             Pltot Tube No. /_O_ , Corrป Factor ; 
-------
                            SAMPLING TRAIN DATA
Conpany -
       Designat I
Date:
Teat  Number:	
Field person;	
Filter Number:	
Barometric  pressure  ("Hg):
Stack Static Pressure
Stack Dimensions:	
Plume Appearance;	
                          Filter Heater Setting:
                          Probe Heater Setting:^
                          Nozzle Number:
                              *— / •
Ambient  Temperature(ฐF) :
Record all  Data Every
                              Minutes
                          Pitot Tube No.^/^?,Corr. Factor :_ฃ
                          Meter Box No ./g>ปg-%?, Corr.Fac ton\_ฑ
                          Meter Isokinetic Factor;   / 7/0
                          Assumed Moisture(%);    /r g'g.	
                          Condensate Volume (ml):	A?	
                          Silica Gel Weight Gain(g);   /ff
                          Leak Rate  Q,0f  CFH at    f f   "Hg
                       10
Trav-
erse
Point
 Mo.
        Time
     Samp-
     ling
     rain
          Clock
   Velocity
   pr essure
    ("H20)
                        Stack
                        Temp
                    Dry Gas Meter
      Vo lutne
                                       Temp (ฐF)
                                      Inlet Outle t
Orifice
ressure
Differ-
ential
 ("H-70)
                          Filter
                           Box
                           Temp
Las t
Imp,
Gas
Tempfpre
CF)
   Sampling
     Train
    Static
      ssure
     ("H
          9/37
                        S&o
                037
                        /Co
                      07 130
                        too
                                      1*3
                                    1.91
                                          z-y
                        too
                                       I**
                        )DO
                                                              67
                        1*5
                                                             68
      10
          /?:
          />-/*
                                            ut*
                                                      3.0
   y
     /(/O
17
     /*

          fa**
            to*
                                     b?
      Ho
          10: 27
    0,2$
/of
3/9. V7
10
     /<*
                                      /M
                               V*
                             Bi&VK
                        r
                        \Gb-~~
                        J_S -v t ,
                                     )
                            -
                         io'4
                                            .
                                  Clayton Environmental Consultants,  Inc,

-------
                             SAMPLING TRAIN  DATA
lompony ;
lource Deaignation:
 eet  Number;
      Person:
                Filter Heater Setting;
                probe  Heater Settlng:_
                Nozzle Number:
                                       ,Dla. (In. ) ;
filter Number;   s (* 4 - I
laroractric Pressure  ("Hg) ;  Z.-?. •Z.*j"
Itack Static Pressure  ("H^O) : - 3
Stack Dimensions:
?lume Appearance:
i ^
ro
unbient Temperature (ฐ F) :
lecord all Data Every
           Minutes
Pltot Tube  No. !-?_, Corr. Factor ;
Meter Box No.g/k-z, > Corr .Factor; -;
Meter Isokinetic  Factor:   H 9j
Assumed Mola ture (7.) :   /. ^~	
Condensate  Volume (ml);
Silica Gel  Weight Gain(g
Leak Rate  ( oo 9   CFM at
Trav-
erse
Point
No.
$ 3
J
3
^
S"
^
7
*f ?
^
/^
^
f^




'—•*
Time
Saap-
llng
(TOin)
C7
^f
( c
i b"
t J
ri~
lo
sr
^o
vr
s^
?ซ L






fC J-7
To^T







- r"-^
^ ~- "x
Velocity
pr es sure
<"H20)
-1*?
, ^
.N ^
.?A
,~^?
, 3 l
^ L
.U
. il
.32
.3i~
,^
,37




i" ; -^t*.
y^>^.^^-^' vVs -I-:
23^ER?CieS(TdTAL>3t&
Stack
Temp
CF)
'
^35, /
^3?.iv?


- "„
"• ' c ^'
1,- , J>,
' -" >ซ-' r"
(-•aปJ.ป-^T^rซ ซA
.Jjr^Tt^'' ' J '
Temp (ฐF>
Inlet
^0
) IV
nft
M S-
1 iฐ1
/ J.O
1 10
en
1 Zo
IT- Z.
112
11?



VI •*
r
- ,v
r* Jป
,'' ~f"
•**iwr
V .*Jt'
Outle t
 i



•>.
-, ~
_-^^ซ.^ฃki,
~t^.__^-i-vp
Filter
Box
Temp
(ฐF)














-

- v v —
•ฃ&;&
- -7S-*J6
Last
Imp.
Gas
Temp
(ฐF)
fe.
^LJ
15"
^^
bซ/
C9
vo

7Ji
7i^
4?
tป1
6^5





-•i-
•s-,. p
Sampling
Train
Static
Pressure
("Hg)
<*<
•^ l
i.zr
u s-
>*^>'
i.r
^'
^. 0
t, r
e.^
2,^
ซป, 
-------
                              SAMPLING  TRAIN DATA
Company •	(-. ,3 /\
Source Designation:
Date•       ^ I i
                      /~
                         e.  J~-Ur
Teat Number;   r* ~ i
Field Person:   /?
                   Wf ~ 2. C. 7 - -7 /
Filter Number:
Barometric Pressure  ("Kg):
Stack Static Pressure  ("H2
Stack Dimensions:	
plume Appearance:  	
Ambient Temperature(" F) :
Record aLl Data  Every
Filter Heater  Setting:	
probe Heater  Setting:	
Nozzle Number:	,Pia.(in.):.2$
Picot Tube No.	,Corr.Factor :	
Meter Box No,	, Corr. Factor;	
Meter Isokinetic  Factor:	
Assumed Mois Cure (7.) :	
Condensate Volume (ml) : ffl-tL^ 	
Silica Gel Weight Gain(g): 70^(T
                                Minutes  Leak  Rate
                                                            CFM at
Trav-
erse
Point
No.
,3 ซ
to
I 0
1
y
1
C
r
<,
?
2
3


-


Time
Samp-
ling
(rain)
LO
45-
•7.0
T
30
S|-
Dry Gas Meter
Vo lume

-6 1
its.t
?&fo v
-K'^.z-
1-7, .-ป
rnVrr
e^.ll^

r^,-.V
ff; ^' ;
t?^"j"j'
C^tw
Temp (ฐF)
Inlet
(Z*
i ? ?
/??
it^l
1^
/ Jo
'^
^30
, 30
J 30
13*
)30


j
,^^
" ' in
ฃi

Outle t
//=%
/ ^
, ,^
i ' V
1 i i~
i f (,
! '1
I * 7
// -7
Z 0
f 7C3
(TJ


-
lf-2^
,<"-^
gQ

Orifice
Pres sure
Differ-
ential
<"H70)
' -Jf
', L
; j-
i. V
2 i
f, I
,T7
.V4
,*ฃ
,TT
/VI
, 1 ->

-


/. 3^i ^
/fXv^
Filter
Box
Temp
















"i* i- *~
^c
Last
Imp .
Gas
Temp
CF)
<-
T T
-If
7C
-7U
lc
T?S,
A
1 V
3 O
S-;
^1
Vl


•

w
&
Sampling
Train
Static
Pressure
("Hg)
3to
c, ^
*,*-
-7
5,
C
'' s-.a-
r,r
G
C
c
C


- •
4.v\
•** v Jf - *"
^•j "^ ^v i *
                                    Clayton Environmental  Coha'ultanCs,'' Inc.

-------
                             SAMPLING TRAIN DATA
Company:   _i~f^A  y 2. C
Source  Deal gnat ion:
)ate:     ;-;_
                      L'^c
                                        /-r
Teat Number:
 leld  Person:
'liter Number;  S( A - ~2-
Jaromctrlc Pressure ("Hg) ;
stack Static Pressure ("Hg
Stack Dimensions: _ t ~z *7
Plume Appearance:
                                         Filter  Heater Setting:
                                         Probe  Heater Setting:
                                         Kozzle  Number:	,Dia.(in.);
                                         Pitot  Tube No.  , T, , Corr. Factor ;
                                         Meter  Box No.  ;7-k -^Corr. Fae ton
iimbient Temper ature (ฐF) :
Record all Data Every
                           / O T
         Meter  Isokinetic  Factorr_
         Assumed Moisture (7.) :   1,<
         Condensate Volume(ml):	f
         Silica Gel Weight  Gain(g)
                                                                   3 y
Minutes  Leak Rate
                                                           CFM at
                                                                  TifWfcn
                                                                    15*   "itg
Trav-
erse
Point
No.
5 /ป
/ i
/"?
'1
S
7
t
s'
t/
3
t
2.



-
-!= .^
Tiiae
Samp-
ling
(rain)
0
o
p J
i S
7^
Z-j"
1J
^ t*
VJ
<•/'"
r^>
b'S'
C-'j


_J'-4l *•
-__O
Clock
''J Si"














-
iw * ^
Velocity
pressure
("H20)
,a^
r'Z1')
,i-V
n
, ? r
, 1 9
./S
- */7
ซ/7
-/?
^rJ
t^ f



^-
.- - , *._
T *' - ^ j"- ~ "X ' •i" v* SL - "' _ "„
•v r~?" ' , - 1*~ * T-,t % . .. ซ? - ' > ป >?• "^
-TJJ-A ••lK)j'Jllfr-L-^"' ^jtj*-f"C3*^*~V'-T' ifc "' H • -Jj-- i ^ -fi---^l_- M
ig^^VERAGE?-(TOTAL) V^Iu.
Stack
Temp
(ฐF)
|c*
/o ^
1 l-1-
1 a ^
/L-1 V
(OS
A^
/i)ft
10 0
v&
\v*ฎ
loo



-^^f-t, ~
' t-^ •*-•
•^
^^.^^fihfc^-
,i^lv-aJฃ.;
— •- -^3t
Dry Gas Meter
Vo lutae
(ft3)
(^7 lyt
1 >- 1 > y
->st
^ c , *
M-' ? s-
c? o j s-
^^6, 4"'
ditb
o/ 4.?
0/3. f
021 I
0 il, ซv
0^1 ,9^7


. ^..
'"•' "t '' ' — ซ"
^"rC -^ C
f^^-^tH-^
\ iSS-^^ija'J.". /
Temp (ฐF)
Inlet
r /Z.
1 1 -i
t^
n<\
j ?/
" ^
/^5L.
ity
111
ft^
MT
Jl V




r-
X f
^si:
>5u_x
On tie t
/ฐ0
M J>
;/z
I/-/
/ 1 '^
1! V
fu
iiฃ
/^
/2 +
rzr
i?>~




i* T -^
W-f
j* ™  -r
?,0
tl
? . s
?. /
^ /
/^9
/ff
Al
(S^ < ฃ^-J
z,j



-
T J ill.^
-^.^^""^C^
' '^ "• r '*• -r
Filter
Box
Temp
TF)















" -
r
-,r--'--
^ * -" - ,
r ^-L ;^ ^
'l^wSf1
a 	 Si.
Last
Imp.
Gas
Temp
(BF)
^ro
Pr
$0
Ho
$6
-i o
S&'
fa
fo
rd
S-o
^0


-
-.
- ^- ,-T,
* "5 '
*.T^r^
- • '^
Sampling
Train
Static
Pressure
("Hg)
\
1
t
•z.
'
f— ^1T Jlv*. n j- i_ .,
TSJ-jUSsitS^^i.
."2 f *AU.- =-i
                                   Clayton Environmental  Consultants,  Inc.

-------
                             SAMPLING TRAIN  DATA
                   Z
                     JT
Company ;      ฃ
Source Designation:
JatS:    9 /7 J / 7 i,
         •yn ซ IN ""•"•pii-Ji i in  mm
Test Number;  P - ^	
field  Person;   /g*/y/C	
Filter Number;	
aarometric Pressure ("Hg):	
Stack  Static Pressure  ("l^O):
Stack  Dimens ions:	
Plume  Appearance;	
Ambient Temperature(8F):
Record all Data Every __
'^ L.T
    Filter Heater Setting;	
    probe Heater  Setting:	 _
    Nozzle Number;	,Dia.(in.):	
    Pitot Tube No.	,Corr.Factor:
    Meter Box No.	 , Corr. Factor:
    Meter Isokinetic  Factor;	
    Assumed Moisture(Z);	
    Condensate Volume (ml);   /(%    _
    Silica Gel Weight Gain(g);
                                Minutes  Leak Rate
                       CFM at
"HB
Trav-
erse
Point
No.
5 ป
I,
t '7
0,
y
T
6
f
^
S
Z
^



•*
-'-'^.-r".
Time
Samp-
ling
(rain)
<= 0
t S~
7 0
"7f
5^
f <"
"t ^
i r~
/O 0
1 0 <,'
)t ?
i< r
< 2o>


-TV- **"*"
"f", "
Clock
/GOT











/ics-


_
-^i™ ^ ^
Velocity
Pr es sure
("H20)
, 75L
•30
^7
.1*1
, 13
J *
. 1 ^
, < (,
r /I
ปtt
,?C
,^0




.,.^\-l
- J~ ^_~S_ _ 'i "1,1 ,'" ' " •"
S^|ftRA%ff(T]SYL)%Tt-
Stack
Temp
<ฐF>
; O O
/ ซ0
/oc2 . 3
0?i 7
^/ ri
ฃ y L
-- x . *r
T7 4
76.1
fi.S-
0*8^, %ol


ifli.a-.^ v
/:,Cv"/vi ซ
--:^v^^
(70031)
Temp ("F)
Inlet
/30
/2T>
I3C
<3i
il?
/5s-
1 X
/K
fIC
/3 L
/ J-C
• 16



i*
^^\
(sS
Qutle t
> ?\
i t ^~
1 ? y
I 7"^
1 7 S"
l&$~
t ?v-
vZc
1 1\-
11 S
t 0"
f ^(,"




^
T^
^•'sji..^.
Orifice
Pressure
Differ-
ential
C'HjO)
*'/
J 3
"J 0
Z T
<:. /
?. /
l,v
1, 5r
I ซV
2, ^
? J
2 ฃ




2^'
,
-------
                APPENDIX
PARTICLE SIZE  SAMPLING FIELD DATA  SHEETS

-------
                             SAMPLING TRAIN DATA
                7 A
orap any r	(•
ource Designation;   ฃ MC.
ater      /
                                  1 .
aroractric  Pressure ("Hg) :  27
tack  Stattc  Pressure ("H-gO) "• - 1  u
tack  Dtmenslons ; _ '$"  TQ _
'lume  Appearance?
mbtent  Temperature(ฐF);
Lecord all  Data Every
                           /er
Minutes
Pitot Tube No. 1 ~L-t Corr. Factor;. ? 3 y
Meter Box No. /Me "L , Corr . Fac ton
Mecer Isokinetic  Factor; j _/>, q _g
Assumed Moisture (%) ;    "2
Condensate Volume (ml) ;    <9
Silica Gel Weight Gatn(E):  1 1. 2.
Leak Rate
o 9-   CFM  at  c $~
                                                                         "HE
"r av-
erse
>oint
No.
> if
,,
1 C
9
f
>
4
r
N
,i
z.
z.




-"--"'
Time
Samp-
ling
(rain)
O
r
i a
I <;
7 J
<>-
3*
3r
<^
Vs"
S*
rr
6 0



-..^jr
Clock
t&4d











'7Yy


ซ-
_> ^^
Velocity
Pressure
("H20)
^
,l!T
^
,Tป
•/"i
?
,11
. 1-7
,n


,rV




, -^ ^__-.-

Stack
Temp
/05"
fc b"
/ i5 *ป"
l 0 ^
/ ^ C
/or
JCST
re>7
/o t
K 5T
r-hviio

e~ฃ 0-f

. 'J. T ~ฐ* •-"

Temp (eF)
Inlet
tav
(j'i
\ 1 1
1 1 ^
r tz
l 2?
'?!
j-z-
/ lv
< 2S-
/25
/zr


7^5
, 	 -^

S
Outle t
9^
/ e>w
1-7
1 [J1 \
\0ซ,
I > C
f'3
I / V
I/ 1"
i / '-
.ซ 7
l / 1


X.

"
^r
Orifice
Pressure
Differ-
ential
<"H20)
!• e.
hZ
i, i
1 ^jf
**l (jf
,1 7-
- *:a
,7^
,1V-
t^
,V1
,*?



-
•^ • — „.
•*$&&-
Filter
Box
Temp














-

:'-?
?^k
Last
Irnp .
Gas
Temp
4<:
* 3
^0
S 1
rfc
>7
^7-
r ,
>V
ff^
^
FJ




-' -
i4
Sampling
Train
Static
Pressure
("Hg)
3
5,0-
1, 7
3, 1
3 S
i,y
3 o
3 7
3 ฃ
1, 3
Q . &
<-, 0




., ~ '-.
,^4^^

-------
SAMPLING TRAIN  DATA
Company- f p/i 7/ฐ $ /C" - / f^C.
Sourc
Date;
e Designation: i^/^ti'7 7f ZJ^c t-ฃtz/
X (/
Filter Heater Setting:
r: &? <$ - /
on; ^-/"^ ^,-">/


probe Heater Setting: — —
Nozzle Number: =y/
Filter Number ; ^er _ 3^ , '-. y'f
1 , Corr. Factor:' "z<
l^O): -rj2=:?'" j^^Meter Isofcinetic Factor; ,/ 7/^
/^J/r/7
: 	 ~
Ambient Temperature (ฐ F) :
Record all Data Every

Tr av-
e r s e
Point
No.
V-/0
V
10
L
y


<
v
3
0
o



-
\.
Time
S amp-
ling
(rain)
ฃ>
^
M
K
T'S
c<
30
r-
yo
vS
tf
'^
(u



-
Clock
/ u '
/_y '
/6 //j
/^,^-j
>i- ^
fl-ifc
po?
#•13
/;./?
/;,^?
/^s
/7^5
/7^^


-
- — -„•
,^
O.io
0. J3
C-Zl
0,2!
0 ? c
0+tf



'
-'ป ' ' 'ru
->.ป/ ""W/, /--' „:ฃ ^ 	 „-
'3SlA VERA CE^CTO TAL fszfS
Stack
Temp
/r<5
/ Ot>
ft*
/
joe:
y
/^
X
/^s"
X
fO^>
/e->




" 4— /_.
^^^
Minute s
/?//<
Assumed Hois t ur e (7.) ;
Condensate Volume
Silica Gel Weight
Leak Rate (9, <:' /
*i ce**~ rrff
Dry Gas Meter
Vo lume
^ ^ ^/ ^
t?7ฃ/*79
9 '^-^9
57'3 /, yv-?
9J/-r/>
^^ V / ?
797. / 1
M^ ^//
7^5 ฃ)r
lotz.rt
iQI&fS
t /~i-"* i f1 *}
}U^ [o s^j^
/otf
/2L-
/32
**"
y
13%
h/o
13V
ftf
/J'/
tฃ'7
r3i




* -
/^
Ovitle t
//6
If*
>2^
/PC
/^i>
/3^
/^
;^z
/cC.
A23
/^
/^/




-
/?^
Q'Ot
Orifice
Pres sure
Differ-
entia 1
•w-^
P-7/
j?,*/ s"
2,^
.?'^i


^ S'5
-73 /
/? ^ /
tJT '^ *v- 1? '
5^t>
SMI C*' t



-
>"*„ ~ _ - ,
^iA
^3.
(ml): _ //
Gain (g) : -o -3
CFM a
Filter
Box
Temp
—
—
—
—
—
	 •
—
—
	
—
_
- —



" -.
r, .
>^^T
t /^ "Hg
'^" / *>X " /^^
Last
Imp .
Gas
Temp
57
9t
?f
92-
rf^
97
^7
9/
c;<
^•r
ซ
93




-
n
Sampling
Train
Static
Pr e ssure
ฃป,<>
^^5L
^,^
$-2.
n^'
/& i
~ 1,2-0
I3.b
&.V
It,.*
!!•<:>
/*.&>



_
- -
•&&
      Clavton  Environmental roniuTtnnrn.  Inc.

-------
                             SAMPLING TRAIN  DATA
Company;	|	
Source Designation:
Date;        ^/z.^/t
                 S - ."7
feat Number;
Field Person;      _
Filter Number-,   S 6*
                                         Filter Heater Setting:
                                         probe Heater Setting:
                                         Nozzle Number;
                                                            ,Dia. (in.) :
                      - 3 6 "7 - J I"
Barometric pressure  ("Kg):	
gtack Static Pressure  ("H^O);  ~ 3
Stack Diaensions;    I Z '' f €>	
plume Appearance:  	____
Pltot Tube Ho, tJ ,Corr.Factor;
Meter Box Ne,J?^t-g. ปCorr. Factor;
Meter Isokinetic  Factor;	I C_? 3
Assumed Moisture(%);   /. jg-  ^
Condensace Volume(ml):	
                                                                           jy
Aait>ient Temperature (*F) :
Record all Data Every     5-
                                                                           ~
                                Minutes
Silica Gel Weight  Gatn(g):   /J, 9
Leak Rate  . Qj 4.   CFM at    / T
                                                                           Hg
TT av-
erse
Point
No.
i /O
, JO
>0
ฐ>
9
7
4
r
<*
j
3
3





Time
Samp-
ling
(min)
O

(t>0
\DO
/ฃ?O
'i?O
too
ii?D
ivJ>O
i^C?
J<5J




_ .,
1 V-
nr ซ?&*^ซ*i^oy
${*! 0
<\z.
^Kf 7
41 ซT
fflo , )
ItZ , C,
idi
f i^^.T
[0s? C
/ / Z O
1 Ki . 'i
l/A.f>J



- -a.
( fel^>>
Tetnp(aF)
Inleti
94
rrS
ปd^
ii>J
! t.
a-?
^9-
Ji>1
i>=r
iOG
i d^
*o T
I J 1





ซ*r-
Orifice
Pressure
Differ-
ential
("H20)
).•
Sampling
Train
Static
Pressure
("Hg)
•^
1
?
L_
^
Z
'* 2.
Z
?
^
2
2^




-
ซ-<*!-• ปnrป>— .
                                   Clayton Environmental Consultants,'Inc.

-------
                             SAMPLING TRAIN DATA
Company •	,.	
Source Designation;
Date;  _   1/tS/"t 4
ฃT/M C
                                 -- <•
teat Number;   PS -J
Field Person:   ,74 "<-
Filter Humbert	
Barometric Pressure  ("Hg):	
Stack Static Pressure  ("H20);
Stack Dimensions:	
plume Appearance:  	
Ambient Temperature (ฐF):
Record all Data Every 	
         Minutes
Filter Heater Setting*	
probe Heater Setting;	
Nozzle Number:	,Dia.(in,);
Pitot Tube No.	,Corr.Factor:
Meter Box No,	, Corr. Factor;
Meter Isokinetic  Factor;	
Assumed Mo is ture (7.) :
Condensate Volume(ml);	
Silica Gel Weight  Gain(g):	
Leak Rate          CFM at
                                                                         "Hg
Trav-
erse
Point
, No.
/? fc
to
to
1
*
/•
(,
S"
tป
I
1
3




* T
Time
Samp-
ling
Cinln)
ta
tr
Ot?
T
<9<3
sr
^f
_j i a
cr
!Z4iC2^^r^i^S,i™
sJa.^V E R AC ET(TO T A t )Tfe
Stack
Temp
(ฐF)
r P o
(03
/J J
/ oT
| J O
/<5t?
) OU
J O t3
^C??
^ O 0
?t?0
}OD



-, -
^ f
-•^7fcl^S.
iซซZi 0^^
Dry Gas Meter
Volume
(ft3)
Mt,jT73
N 1,7
' ^. 7
of, V
i 7S,<*
>32_
I 3V C
)3T ,?
iS^.t,
is/, r
/V3^
i ^fe l
i^.-io**



-
C "Slfe-fS:)
Temp (ฐF)
Inlet
J n
/ '1
iฃJ
'2t_
("Zl
/21
\tl
,T*>
a3
,^s
1 23

( 13
Mt*
ป /
?. /
,->7
^9
. i~s
,49
,s
^ o





w*"1* ' * — *
"^1-'*-^^'^^
                                   Clayton Environment a 1  ConsuLconts,  Inc,

-------
             APPENDIX E
VISIBLE EMISSIONS  FIELD DATA SHEETS

-------

-------
                                      of Visible EnissiO'is
            -1
              '
->
          ,
        lv> - i:>
LMtc: "  "
T>p: of Plane:    i
Type of Discharge:  fl'*--
Location of Discharge:
Height of Point of Discharge:
Description of Background: Q<
Description of Sky:
Hind Direction;    )ฐ
Color Of Plume:  V->
Duration of Observation:   I  l&v-vw.
                      OF AVERAGE OPACITY
                                             Distance from Observer to Discharge Point; .
                                             Height of Observation Point: p^-v^-J  l2t-.~\
                                             Direction of Observer from Discharge Point:
                                                                   •~*-
                                             Hind Velocity:  3 - |-q
                                             Detached Plume:    &•> /A-
                                                            SUtt'MRY OF AVERAGE OPACITY
Time
Set Hurrier Start hod
1 '' ป
2 escป .">)L. i^ซ\ .Of-i
3 eซ-, ,HTL 0^ x~ i o ti
6 iii vT. \ o If
9 |o (-y ,O L^
10 ,u ?-i ,0 ',3
11
12
13
14
15
16
17
18
19
20
Opacity
Surn_ /--verage
0 0
c? C.
C 6
: v> O
tv O
^* O
a O
ฐO Q
*5 C'^.'Lt c
i -3 O










nme
Set iluvber Scart End
' 21 '
22
23
24
2S
26
27
23
29
30
31
32
33
34
' 35 •
36
37,
38
39
40
Opacity
5ura Average




















Sketch Sfiovring How Opacity Varied With Time;
      ซซJ
       o.
       o.
      O
                                                      V
                                                      L
                                                                   N" •' 4
                                            Time, hour1

-------
prcon OF viti'iE anssio-is
Coimany hii>e
Plant fddrcs
i- nC Date S -1.1-1^
f)ป >ปj -, \tl1s
s ^KKA^U, V>-ป-ป. 5 n \C Ohscrvor ^\-U.' , Ou* — ,_
" un , ' f U
Stack Location l/w-v^e-v^ L^—>**~^, Observer's t
I'eather Conditions ^cO

/• 6* ป Location -"^ f^O &
J^. CXev JJ-, W/v-J3 o - fc >42.

TlJ!r fJ-v-tw^arU "'~^**~^'COi'11',FHTS
HR

aai


























U --
>-''-:.
-'!!*!

30
31
32
33
34
35
36
37
36
39
40
At
42
41
44
4S
46
47
48
49
so'
SI
52
S3
54
55
56
57
50
59

05
h1
/M
Aj
A/
d
M
ปs!
N/
M
N
N
N
N
H
'M
N1
/J
A>
A/
A/
ซ^
/J
yJ
^
rJ
^
A/
|J
iJ
r^
SECCtlOS
15
k/
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M
M
M
^
pj
M
t^
N
IN
N'
Al
A/
Mป*
iy/
^J
/xl
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fj
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N!
M
N
AJ
N
^J
?M
30
A;
rJ
/j
rJ
M
ro
^
*^j
"•*
N
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^J
Al
A/
N
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A/
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Al
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M
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r/
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ii
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ปi
45^
^
,^
w
rJ
KJ
rs]
^
rJ
NJ
N!
fsj
N
N
H
_ WtN^y^v-^J







\ /^J^*_^t\ซrf IvJ f**^wv^^^
r

1
\ /k^*c^^ fJ*ซ*rt*vป-\'O '
•

-

I "^4A-^fr^ AJ*^^**' — 1/ฃ*
r
1
*

,
f ^ts-tx-lk. Jj i^ .-,.... ^j
J -----
' • -f _-."- ' •*- - — - „,-.',-_
^ -*" -. J'-ii- - -,,-.-_! "_'-*".. ^ - % ^- ,' ,_ '

-------
                             RECORD OF VISICLE EilISSlO'.S



Covpany Name	^ftAC-	    Date _
.•**. t ^\ i r
Plant Address "*Vs-v-vCk. (y^-Hi "^ , C* , Observer \' , \p . vH^i— v
Stack Location (. u-vnv.wj-v C-v~ป-f-~.— Observer's t
Weather Conditions ^j*

u . ^ Location J^ V 3 3 <.
it'v tti-jC^ ซWMป* c" — j ^ ^
.^ <} •
TIME
l)R

10 1



























--
--
tf
HIT

00
01
0?
03
04
05
06
07
OB
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
79
jd;
SECC IDS
00
4
/vJ
A/
N!
N)
W
NJ
NJ
fj
h)
/sl
N
w
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Kb
A/
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hi
(^
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-

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w 1,
r
i^* JU* v.^, Cw^-_ ju.tlL^t. - ->
* j1


r ป JT'™ -jirf1^' 1
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r
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V rMA^vv.. )j t/ป->\^>

i
i
-


i
I 'V>AJy*ป K^ixvi^y ~ ~* ^ "^
------ ---*. -i, •__----..., _ . , - ^e
-v ซ*r^ir' -ป^ '^^ ^t-,-" •- ^ - '"/-".T"~ ' - • ^- '-'ป-" V-" !• ^—^

-------
              '                 Sunmary  of Visible Ernssiois
uotc,
                    I
Tyfi of Pi ant:      si.
Type of Discharge:    >
Location of Discharge:
Height of Point of Discharge:
Description of Background;
Description of Sky:
Hind Direction:
Color of Plune:
Duration of Observation:     / /ul
                      OF  AVERAGE OPACITY
                           •' '  7.
                          i*-1   LJLc'-d-*-!
                          d        J
                                             Distance  fro-  Observer  to  Discharge Point:
                                             Height of Observation Point:   cj-i^^-^r
                                             Direction of Observer fron Discharge Point:
                                                                                7    t   f
                                                       O O   W *?yVt~C-fV   J iSfzbb-i-A-J jT/'
                                             Wind Velocity:
                                             Detached  Plume:
                                                             SWWARY  OF AVERAGE OPACITY
Time
Set Nurser Start End
1 oci 31 &fi)
2 OV K oV^3
3 O'i <r
5 Of J^ / 13 0 (
6 /o , ซ i- ^ j ฐ7
7 / ฃ, r C fr f J , !$
8 / - . // /& />
"9 / 
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11 ^ J
12
13
14
15
16
17
18
19
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Opacity
Sum J-verage Set ilupber
AJ 'VI - 21
,V y(J ' 22
* >0 M
' 74
,A/ ^Kt/ ***™
A? 0 25
^ ^ 25
/u ,^ 27
*^ /t,' , 28
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• ,L x^ 30
31
32
• 33
34
' 35
3S
37-
. ' - 38
39
40
Time Opacity
Start End Sun Averigs


^

















Sketch Snowing How Opacity Varied With Time:
       e
       o
       •a
       a.
                _       _....-^- --       .. .  .  _
       !lS11ป*J^^^%^"^^                                          '3- .=~n-

-------
                                    TO 0?  VISILE  MISSIONS
Coflpany Har e 	
Plant AdcJiess
Stack Location
?,        r^c
I  / KJ fj  , l\s '—•
                                           Obsen er
                                                            fi^J  P
                                                                                       -. \,
                                        LI jl
       V.'calher Conditions

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-------
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11
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-------
                              Sun.rnary of Visiole Em;ssions
uate:  ^-T-t-^  ซ-
Typ; of Plane:    I
Type of Discharge: C~-*Ai i
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15
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o ^ 24
c, „ & 25
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e 0 31
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c> t> - 33
34
' 35 - -
36
37.
38
39
40
Time Opacity
Start End Sum Average




















 Sketch  Showing How Opacity Varied With Time:
       0.
       o
                                            Time, hours

-------
                                                  CL-
or vni?LE
Company Name
Plant Add res
\^e Date ^-I'l-T^
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-------
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Stac^ Location
                                         Or VISIBLE L. IS3IO'1S

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-------
RECQPD Of VISIBLE
Company liwc
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Stack Locati
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i nC Date ^ -tT-~Hป
S ^VVJ^A-^-^ V *-irA rt ^" Cbscr/er \ , U3, 1(>i-ซri^>,
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-------
01* VIABLE
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-------
                              Sunmary of Visible Emissions
                                    U
Tyfi of Piant;   \ rn c    n^-
Type of Discharge:   C_-v-~ซ*'*-
location of Discharge;   - \ <*
Height of Point of Discharge:
Description of Background;  C
Description of Sky:  \*~3X-^
                    i
Mind Direction:     N-  ^ w'
Color of Plume;   ^ ^&-u*-~ซ-
Duration of Observation: -^  \  ^2,  jJrn^-T-
                      OF AVERAGE OPACITY
Distance from Observer to Discharge Point:
Height of Observation Point:  W^ซ-V
Direction of Cbserver froi Dlscnarge Point
                                 —,
                                  "\
                                             Hind Velocity;   D-ip
                                             Detached PI umai   Ki //V
                                                            SUflHARY OF AVERAGE OPACITY

Set Huraer
,
2
3
4
5
6
• 7
. 8
'9
10
11
12
13
14
IS
16
17
IB
19
20
Time Opacity
Start trd Su,ii^ J-verage Set Nuraer
H-ปn iv v> ^ ^ ' 21
t^,L3- \S 5.ซ\ -^ 22
ivtl \'i ^ c 23
li^f u'^ii t? o 24
U -H rป ซn ^ Q 25
11' ^T i-a-j^ " ฐ 26
j^ ,o> if it * ฐ "27
i^ if M- ^-^ , ฐ ^ 28
\^ ', t^ t*s| , i,i*- ^ ^^ 5s
tA- , ju. H-'.^-L •* * ,30
rt'.lt- 11. W -* ฐ ' 31
\% -!,ซ i4 '4* o c>' ' 32
iij'44 )f;s* * ฐ '33
m p ijo j^f , 5 ij o ^ 34
, *n ฃ? * ^C
l^lCU 1^,0^ ^ ซ|Q
3S
37-
38
33
40
Time Opacity
Start End Sum Aversgs




















Sketch Showing Ho* Opacity Varied With Time:
       I
      •01
       II
       •Q
       cx
      o
           .

-------
                                   RECORD OF VISIBLE OUSSlQ'iS
Company flame \ v\ C.
Plant Address ""Sf* — <~^ UA—6- Vl,>^
Stack Location IM/WC, "Tp-^
Weather Conditions y^\tX-ป Diju^ . W-i-^
Date ฐ\ -i,n ,-> <-
Observer X ,\,~. ,Jtv/V-'
     02
                                          tป
     03
     04
     05
     05
     07
     OB
     09
     10
     11
     12
     13
     14
     15
     16
     17
0
     IB
          N
     19
          /S
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     20
                    N
               N
     21
      22
               h
          N
      23
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          N/
      24
                    fJ
      25
      25
          /v
      27
     A/
                    tJ
      28

               N
                               vn
      29
               fsl
                                                 TT

-------
Co-npany tome   I
or VISIPLE EMSSIOJ.S
             Date   cl-Vl--?ปป
Plant Address *^i
IV
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-------
RECom  or VISIBLE oussio-.s
Compary Itame
Plant Addres
Stacl Locati
Weather Cond
LJV\ C Dale ^ -'v"-1 ^
n - ป \ ' \ r
s >~\VA>-eJ!^ ^ '-y^- A A • Observer ,-VVJ-, !iT-'^i>vv>
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itions C\i

i . ^ Location A-^jO^t;
<-vj_t _^y , U) xi^i Ct - \ 

  • -------
           Company Hanie
    
    
           Plant Address J>y
                                    nrcoro 01 VISI.HL LUSSIOMS
    
                                                         Date
                                                                   -1 <ป
                                                    Observer
               k Location  yt\~.t.
      l.'eather Conditions
                                                       -
                                                   C - .$
                                                    Observer's
    
                                                     Location
                                                                       •5*0 '
                                                                                IT
               TH'E
                                                   CO'JOTS
    HR
               SECONDS
    rv.
    30
              00
               IS
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    IL
    
    32
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         31
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         37
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         38
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         40
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         47
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                                                         -0-
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          51
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          53
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          54
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          55
              M
          56
                  M
          57
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                             N
    

    -------
                                   Summary of Visible Emissions
    uatc,
    Typ of Plant:   -fiJiP*1"  C>oJ A ^    •
                                           L                                                          7 r
                                                  Distance frcr. Observer to Discharge Point: <*,.-"/-*•*/• /u  '
    Tjpc of Discharge,  o^ ojซc ซt\^j
    
    Location of Discharge;
    
    Height of Point of Discharge:   /e -
                               if
                                                  Height of Observation Point:
                                                                         i di Ll   / tj ire I
                                                  Direction of Observer from Discharge  Point:
    Description of Background:
    
    Description of Sky  ฃ'
    
    Wind Direction:
    
    Color of Plume:   /o <-  <- -•><• ( d  r L<~*~>-'
    
    Duration of Observation:    7  /H ,
    
                  SUfiMARY OF  AVERAGE OPACITY
                                                                "'
                                    >;          -?>3
    
    
    
                                     Hind Velocity;
    
                                     Detached Plume:
                                                                        77
                                                                                <> r
                                                         ;i
                                                                                                ,i
                                                                 SUMMARY OF AVERAGE OPACITY
                       Time
                                   "Opacity
                                                        Time
                                                            Opacity"
    Set Hunber    Start    End     Suru    f.verage   Set uu^ber    Start    End    Sum    Average
        2
        3
        4
        5
        G
        7
       • 8
        "9
       10
       11
       1Z
       13
       14
       15
       16
       17
       18
       19
       20
    if . ฐ ?
    / j  's""
    / a ' 3 (
    ^;  n
    
     / r  33
    / J  3 /
    / f i" c    ^<,    '
    
    
    
    
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      / ^  1-^  AJ
    
      /•).') (J   A-
    
       /;?' 3 2-  /t
    
        , 2  3 f   J^-
        / 3 ' v y
                                         >L/
    24
    25
    
    27
    28
    29
    30
    31
    32
    33
    34
    35
    36
    37-
    
    39
    40
    Sketch  Showing  How Opacity Varied With Tiir.e:
          •01
           ex
                                               "> Time, hours
    

    -------
                                                       OF  VlSh'U  L'.ISSIO'.S
    CoTpany Iteiie ' "-
    Plant Aadu'ss -J,MOC e J/,^ei
    — 	 i - 	 — 	 •* 	 ' 	 	 	 rfi 	
    Stack Location S. , , ^ <~M C.v-jsu~\
    o
    leather Conditions ^.-U^JJu
    $
    Date 7 f - 7 /:
    /\J C_> Obscncr ri P H
    Observer's _ , c
    Location "7 "S v
    
    
    ?<.,
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    -------
    rrrorb  01  vi JIปIE  iiissifi..$
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                                  Suirmary of Visible Emissions
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                                 REcor
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                                                                   D,te
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                Stoci  Location
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                                           ^ — -Vc.-
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    ->.
                                  Sun.niary  of Vis
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    Tyfi of Plant:   \f* C
    Type of Discharge; '
    Location of Discharge: Ti>->i<- "
    Height of Point of Discharge:
    Description of Background:
    Description of Sky:   N),  '-       -
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    Hind Direction:   M//>
    Color of PI une:  <> /A
    Duration of Observation:  ^M ^''/A,
                                                 Detached  Plume:   N> ,'/\
                                                                SUUflARY OF AVERAGE OPACITY
    Time Opacity lime Opacity
    Set Nurrher
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    28
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    30
    31
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    ' 35
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    37-
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    Sketch Showing How Opacity Varied With Time:
           8
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    -------
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                                          of Visible Emissions
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                 Coipanj  \\? .e    1
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                                    i) 01 visiiu r  t
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    -------
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                                 RECOPD OF USIGIE  [MISSIONS
    
                                   _    Date
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    Plant Address  "S ,-	
    Stacf. Location
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    -------
                                   Sun nary of Visible
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                  SUfSHARY OF AVERAGE OPACITY                ,    SUMMARY OF AVERAGE OPACITY
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    Time Opacity
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    ' 21
    22
    23
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    26
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    30
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    32
    33
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    Sketch Sfiowing  How Opacity Varied U'ith Time:
           c
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          fi-
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                                                Time, hours
    

    -------
                            01
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    -------
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    -------
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    -------
                                  Sunmary of  Visible Emissions
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    Type of Discharge:  ;?
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                   SUfiriARY OF AVERAGE OPACITY
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    -------
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                                          of Visible Ennssiois
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    -------
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    -------
         APPENDIX  I
    
    
    
    
    EXAMPLE CALCULATIONS
    

    -------
                      RFfORU Of VISH'U C.ISSICJiS
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    -------
                                    Summary of Visible Emissions
    
    
    
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                                                            "^                   "ป   *-j"i       * rt.jt'*-
    
    
    Typi of  Punt:  1 ^ C  -~ t^*y_^^          "'"'".^  ^-v->  ^  *~>V-^   i^i--C*-
    
    
    Type of  Discharge:   ^-  '>_v'-jt^-^^"T"
    
    
                                                    Wind Velocity:
    
    
                                                    Detached Plume:
                                                    Direction of  Observer from Discharge  Point:   S
    Kind  Direction:    ~  - n ฃ
    
    
    Color of Plume:
    
    
    Duration of Observation:
    
    
                   SUMMARY OF AVERAGE OPACITY
                                                                    SUHttARY OF AVERAGE  OPACITY
    Time
    Set Nunber Start tnd
    , c-.'i^ ซ1^t=
    2 C ""ป 5 b /C /O V
    3 t /(•'';ซ'•
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    10 )o lit 'J ซ > ^
    11
    12
    13
    14
    15
    16
    17
    IS
    19
    20
    Opacity
    Suซi Average
    ฃ if
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    D . ۥ
    c- ฐ
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    L-"1 l>
    
    
    
    
    
    
    
    
    
    
    
    Set ilu^ber
    " 21
    22
    23
    24
    25
    26
    27
    28
    29
    30
    31
    32
    - 33
    34
    35
    36
    37-
    38
    39
    40
    Time Opacity
    Start End Sum Average
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
     Skstch Showing How Opacity Varied With  Tire:
           ฃ  5-
           o
           IQ
           CL
           O
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                                                       T hours
    

    -------
    Coi'pany Name  	\  \f C.
    
    Plant Address  Srf>_k^i
                             RKOI'J OF VI SI I'LL HilSSIOliS
    
                                                  Date
                                                       vcr
    V;.
    Stack Location
                                                  Observer's  ^_
                                                   Location     /
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    31
    32
    33
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    35
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    39
    40
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    42
    43
    44
    45
    16
    47
    43
    49
    50
    51
    52
    53
    54
    55
    56
    57
    58
    59
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    -------
                                REcon or VISIBU
    Company Ifaire
    
    Plant Address
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    -------
    Company 1'jn's 	'
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    -------
                                  Sun.mary of Visible
    
    uotc:     T- '- ' ^
    
    T>p- of Plane:    ' f'1 C   "T.
                        ,\      -
    Type of Discharge:   ^ ./-ryu --<_  *
    
    Location of Discharge: .'U*- x •-ซ*/••
    
    Height of Point of Discharge:  ^ - -~'"1CS
    
    
    Description of Background: "i1^1*",) 7  ' u<: ^
                          ~         i
    Description of Sky;  'J^-c^t-^-
    
    
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                               r
    
    Color of Plune:  ^   LvwiQ   ^c*-ซ-*-
    
    
    Duration of Observation:   \   \i-ii,wi—
    
                          OF AVERAGE OPACITY
                                                 Distance fro.1*; Cbservar to  Discharge  Point: ••
                                                                                       r
                                                \Height of Observation Point:  .^- ^c
    
                                                 Direction of Observer frora Discharge Point:
    
                                                  ^;
                                                 Wind Velocity:  f -ฃ f
    
                                                 Detached Plume:   ,^//'-
                                                                SUfulARY OF AVERAGE OPACITY
    Time Opacity Time Opacity
    Set Huriier
    1
    2
    3
    4.
    5
    6
    7
    8
    9
    10
    11
    12
    13
    14
    15
    16
    17
    18
    19
    20
    Start tra Sum average Set uuirber Start End Sum Average
    \o-._ •_,-*• \ ,;ci c ^ '21
    \.. '.e\ u-.QT C 0 22
    vv •- c T v - , -%, .r- c 23
    \ \ : \ v ' ', 1 1 ^ c c1 24
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    1 - ', •? V , -. ซ ci '--1 D 29
    U ',f\.r> M -, -si' r ^ 30
    31
    32
    33
    34
    ' 35
    36
    37-
    38
    39
    40
    Sketch Showing Ho// Opacity Varied With  Time:
          Hฐ.^
                                                lime,
    

    -------
                                        OF  VMi'lE  L'HSSrO'.'S
                       JV. C
                                    V
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    45
    46
    47
    48
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    -------
    Company Ihi.o
    Plant Address
    Stack Location
                                          RECORD  OF  YISIEIC EMISSIONS
                                                               Date
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    -------
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    -------
                                  Summary of Visible Emissions
    
    uatc:   'VvvT1"
    
    Typ: of Hanc:   1 ^\C.
    
    Type of Discharge:  ^'
    
    Location of Discharge: "' ^- ^ ^ -^
    
    Height of Point of Discharge:  &-  '
    
    Description of Background:  "%'•--> f
                         r-        "?-
    Description of Sky:  '- v-fc-^-c ^  -
                         r
    Hind Direction:  fa c
    
    Color of Plune;^-^ \.uw.\!
    
    Duration of Observation:
    
                  SUW'ARY OF AVERAGE OPACITY
                                      .                     n u
    
    
                     Distance fron: Observer to  Discharge  Point:  o 'Co-
    
                     Height of Observation  Point:  <~  *iO
    
                     Direction of Observer  from Discharge  Point:  V\J
    
    
                      „   (.       4
    
    
    
                     Wind Velocity:   ^ -/&
    
                     Detached Plume:   ^ A
    
    
    
    
                                    SUHHARY OF  AVERAGE  OPACITY
                      Time
       Opacity
                                 lime
              Opacity
    Set Nuroer   Starr   Lrd
    Su^i
    Average   Set .Jurroer    Start
    End
    Sum    Average
                         t ซ•" i
                                                    21
        4        \4',l*   H ^^  ~ ฐ       ^     .    24
        5         4',H   i^!^J   Jo         25
        6        |cj -,^o   :^| ,^u  o      o        25
      "7        i^'.-sc   '^.^t  o      ^     '27
       • 8        i^  ,a ^   i
    -------
    RECOKD Of VI5IBLC E.",I5S!C,S
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    5"
    ^
    	 	 r
    /o
    /.o
    
    $•
    /^
    /O
    /r?
    r
    
    ^
    5
    /o
    /o
    /o
    r
    s^
    10
    .<
    <
    ^
    ^
    fo
    -to
    /o
    
    
    45
    '
    fT
    /^
    /^
    <
    ^
    fO
    
    5"
    /j
    /€>
    /ฃ>
    y
    /O
    ^r
    5^
    ^
    ^
    f-
    /o
    0
    /o
    
    
    
    
    
    
    ~
    
    
    
    
    
    
    
    
    
    
    ,
    
    , *
    *•
    1
    
    
    
    
    r
    1
    
    •ป 1
    •
    
    -
    ' '
    
    

    -------
           APPENDIX F
    SAMPLING SUMMARY  SHEETS
    

    -------
       I  i
      -'Plant  Internationa 1 Minera Is and  Chemica 1 s  Corpora txon  Location  Spruce  Pine,  North  Carolina
       t  ,r
       'Sampled  Source  No,  2 Mill   fiaghguse  Outlet	
    ,l Run
    t
    P-l
    P-2
    . e-3
    
    Date
    9/28/76
    9/28/76
    9/29/76
    
    NP
    20
    20
    20
    
    Pro
    2 ,32
    2,06
    1 ,82
    
    Pl>
    27 .23
    27 .23
    27 .22
    
    Vm
    105 ,631
    100,848
    93,551
    
    T
    Anv
    119
    129
    116
    
    v
    mstd
    SB .228
    82 .743
    78,^04
    
    vw
    32
    34
    37
    
    Vwgas
    1 ,507
    1,601
    1.743
    
    7M
    1 , 68
    1 .90
    2 .17
    
    Md
    0,98
    0,98
    0,98
    
       i,
    
    lun
    T
    . P-l
    P-2
    P-3
    
    
    MWd
    29
    29
    29
    
    
    MW
    28 ,78
    28.78
    28.78
    
    
    ?st
    -0,12
    -0,12
    -0.12
    
    
    P
    s
    27 . 11
    27.11
    27.11
    
    
    CP
    0. 839
    0,839
    0 .839
    
    
    VaPBX(Ts+460)c
    16,767
    15.948
    14 ,738
    
    
    vs
    2579
    2453
    2267
    
    
    TS
    105
    115
    103
    
    
    TC
    120
    120
    120
    
    
    Dn
    0,25
    0.25
    0.25
    
    
    %I
    100,1
    100 ,5
    100 ,8
    
                                   100 H
                              f H*
                                         _JlJi
                              H.ซ 100 'tM
                               *  *^B3
                0H (10,
    
    
    
                11(1 -H
    v, • f 120.1.1 tp i /  4>~x i^
    
    
        1.Q1I ป {T, ป *W1 i V.
                •
    N
    9
    m
    fb
    Vซ
    Trt
    ฅ_
    P.*
    V*
    
    
    Toll) Ho, of Sampling PoliU
    Drpfiป In- B,Q
    liwwtrlc Pressure, In, (|).
    Absolute
    VfiluKe of Dry Gal *t Hctar
    '•^illlloni, DCF
    AMrajo Hctaป" Teitpefilurj,
    Voluiro of Dry Gil It &TP,
    4 DStr
    Toiil llS^CollecUd In IiMln-
    gtrx'ind Sltlci Cel, il
    Dry tUnJiJi'd cubic fuot it 4
    * SUndJrJ condlCtoni il^'i7,
    t *
    m M ! .. i • . ii . • • . . , .
    Vw
    I H
    IC0|
    ซซl'
    1 CO
    wd
    |ar, zง,sz in.
    Z9.9J in. Ilj.
    Volwa of Witfg Ifipor ColJiel
    1 Kali lure by Ynluw
    Hull Friction si Dry til
    Volunซ X Dry
    Volume t Dry
    Votiwe X Dry
    Voluno 1 Cry
    Hoi ecul ir Vtlght of Slick Oil
    Dry Q*i Is
    HaltcuUrVelght of Stick
    Cu. Mil Dud
    Kg.
    
    P..   Suite Prmurt of Stick
     11     cซt, In. H.J
    
    I1    Slick Cii Prciiui't, (rt, !•
           Atl'-olult
    
    C '    Pilot Tube Ccปrfltlint
                                                                                                                           If    S?icl CM Vflucltj1 it Sli
                                                                                                                                  Condition!,  tfft
               Stltk
           "r
    
    
        Kit Ttim of Ititi mo.
    
    
               Koiclt
                                                                                                                           I I  Nrctnt
                                                                   TCO)  1ป tletarmlned by ซvorซf|lnj tha squsro Not if
                                                                        pnil'-ct of ihu vjlocliy tiซid (&t>i) tnd Ihi
                                                                             tatperilurn trn tuh ปtปpllnQ paint
    

    -------
    Plant International Minerals and Chemicals Corporation Location    Spruce  Pine,  North Caroling
    i
    f
    i
    •'•,,d
    ', >'*
    {•'
    fซป
    (-;
    > '{
    ' {
    ftป
    Sampled Source Mo. 2 Mill Baghouse
    1 ;
    1
    i
    ^
    Kor
    th Inlet
    
    pu V
    r D TO
    27
    ,25 S0.3C
    
    
    
    
    ! Run MWd MW Pst Pg
    P-l 29 28.78 -0.22 27.
    03
    
    i
    
    /"7- 65 ป ฅ Ch * 'i \ ^w * *ซ ^o ToU' Na<
    
    
    Cp V^
    0 .838
    
    
    
    of Stapling Podll
    '• (f * 46^5 L ^u t V
    * Jld M ,. f,. Averige-DHMei PreJiuri
    f flป • Drop. 1ft. H20
    t " * ' 100 b Wiiolute
    i
    V Voluปซ tt Orj Ctซ it BeUr
    ' 14 i i 3i i 78 '""dl llonii DCf
    I. Averse Helor Teปftrtlซrซ,
    J * tf * * V., Voluw Of Dr/ Cit ปt STP,
    j piti oscr*
    PtP - *. '
    * ~ ll IL Totil lf,0 CoJJccltd ffi Icjin-
    r i i V 5trj "^ ^"ca ^1< ''
    . — _ m.^ . ., I 	 * 	 i
    Ilia, 1,1 cซ • / ปP * [T( t 4ISJ |_Fง i WJ
    ff *
    t • *
    VT,. >,.•<*(•.}'
    Cry ilindjrd cubic fit) it ฃ
    lUndinl condltloni u^&'F.
    ^ป ซ
    
    
    TV V V %H MJ
    ^m mstd * wgas d
    1 US 67.065 ?.? 1,272 1.86 0,93
    
    
    
    
    
    SX(TS+460)C Vs T5 Tt Dn XI
    12.996 2000 103 120 0,250 98,1
    
    
    
    V Volusa of yปUr Vipor CoHftLad r Suilc P/TiiKr* ซf Jtitl
    511 it SIP, SCF •* c*s. In, 113
    I H S tatiturt by Valvn* P Sink tu Prcviui't, 1n.
    Ab'.olnl*
    Hj Mule Friction pf Bjy til
    C ' Pilot fybt Crtfflsltnl
    J C02 Volunซ $ Or/ P
    V. Stick Cn Vtleclli1 il SI
    1 0, Voluw X Dry lonilUont, fpi
    j CO Yoli/ne C Dry ^ง ^vijfl Slit* Tcmpfrltilf
    2 Hy Voluro I Dry
    T. KH Tim of Tell, MIrt,
    Wj Molecular ซซfปht cfllicl Olli l
    Dry Dasll
    P. liflpllAg Noizlt OlcuUl
    >H HiUculir Wilghl of Stick tf . e^,
    
    -------
    'Plant Internationa 1 Miner a Is and Chemicajjs Corpora t ion Location  Spruce  Pine, North Carolina
    r
    ^
    \
    f
    i
    Sampled Source No. 2 Mill Baghouse South Inlet
    -i
    i
    '.Run Dace Np Pm Pb Vm Tm Vmgtd ^
    P-2 9/28/76 20 2,4 27.25 106.937 127 88.198
    
    
    
    >
    
    Run MWd MW P t P C *y^p X(TS+460)C Vs
    , P-? 29 28.78 -0.18 27.07 O.C37 11,004 169
    
    
    
    
    
    'v vw %M Md
    37 1,743 1,<4 0,98
    
    
    
    
    Ts Tt D 7ปI
    3 103 120 0.313 97.2
    
    
    
    
    ' /7ฃ5ป V ' ln> "zฐ Hd Hole Friction cf Dry
    \.l "" ฐ^7/ ซ ป„ ^ • 1M • V K Pfc lirmtrlc Preiiura, In. Ig. , rn „„,. 	 	
    1
    y
    ซi •
    P( Jlitk Cn fititafw, 1n. Wj
    til
    C' Pllol Tu(iป CrtfneUnt
    * ^00 ftbiolule i I-IV.-B ป vi/
    t$ Stitk Cn Velocity il Stit
    i V Voluna of Diy Git ซt K*lปr X 0, Voluw I Dry Condition!, f[ซ
    fltO *' \t 110 " \ ( 1 Cfl + 1H \ " '"-'"(Jlltorl, OCF
    2 VDO i IflO • 2 103 j [5 VpJure I Drv ^ซ Awiofl StKi TcmfUriturf
    T. <ซr(gc He lor Tenperปture, ปwi""o ป i/r/ f ,f
    x "t • r
    HJ H ซ u n H \ * "z ^i"™ * Ory
    -' d " VMwSfis"ia'fi<' "Jd w.c-uru.itf.i.fn.aou. Tt "ll TlB< " T"tr "'"•
    ซ!• uj^r ซ p Juj^j
    PU ป F.. *a D. Jinpung Won If OljauUr.
    0 ~ ll V.. ToUl II,B CalUtttd In lป)ii\- a ,
    , r 1 1 1/1 s=r* ซnd Sllfc* Del. il fW Holeculซr UMjht flT Itlck . t ป. . i ,.• ,i
    ' ^••••—^^••tw IT 1 m ' .1 • 1 f\i Vet DAI^I ^ WfTlBl lutlMlIC
    • ,tff •, „
    *- i Drj lUnijrd cubic fซl i*v8'ป Z3>SZ Ini Us-
    • n^> _ |v * flฃA\ • b ^ f
    
     i Ktt• r  ซ ซ4ป(or
    iquare reot of
    

    -------
           APPENDIX
    PARTICULATE  WEIGHT DATA
    

    -------
         SUMMARY OF PARTICIPATE WEIGHT FRACTIONS
             NO, 2 MILL  BAGHOUSE  OUTLET
    International Minerals  and  Chemicals Corporation
               Spruce Pine, North Carolina
                  September 27-29, 1976
    Test
    NO.
    
    
    1
    
    
    
    , t
    •)
    *>
    
    
    
    
    •3
    
    
    
    
    Fra ct ion
    Water Probe Rinse
    Filter
    Front-Half Total
    Iinpinger Contents &
    Back-Half Water Rinse
    Total Particulate
    Water Probe Rinse
    Filter
    *?._1irt'i s I1 n f*a 1
    
    Impinger Contents &
    Back-Half Water Rinse
    Total Particulate
    • Mater Probe Rinse
    Filter
    1? i- s-h n 4- lljil f TrtHal
    
    Impinger Contents &
    Back-Half Water Rinse
    
    
    Final
    Weight
    (gm)
    98 -0907
    0 .1482
    	
    87 .3930
    	
    93.2040
    0,1628
    
    
    91 .5397
    	
    95,7591
    0.1434
    
    
    88.t569
    
    
    Tare
    Weight
    (gm)
    98.0860
    0 .1258
    	
    87 ,3885
    	
    93 . 2021
    0 .1369
    
    
    91.5367
    	
    95.7548
    0.1261
    
    
    88.8516
    
    
    Weight
    of
    Particulate
    (gm)
    0 .0047
    0 .0224
    	 ,
    0 ,0045
    	
    0.0019
    0.0259
    
    
    0.0030
    	
    0.0043
    0 ,0173
    
    
    0.0053
    
    
    Applicable
    Blank
    Value
    (gm)
    <0,0001
    <0,0001
    	
    0 .0114
    	 '
    <0 .0001
    <0 .0001
    
    
    0 .0096
    	 ,
    <0.0001
    <0 ,0001
    
    
    0.0072
    
    
    Blank-
    Corrected
    Par t icula te
    (gm)
    0 .0047
    0 ,0224
    0.0271
    <0 .0001
    0.0271
    0 ,0019
    0.0259
    A n 9 7 fl
    
     i A
    
                                       Clayton Environmental Consultants,  Inc
    

    -------
        SUMMARY  OF  PARTICULATE  WEIGHT  FRACTIONS
            NO, 2 MILL BAGHQUSE  NORTH INLET
    
    International Minerals and Chemicals Corporation
               Spruce  Pine,  North  Carolina
                  September  27-29,  1976
    Test
    No.
    >s
    1
    t
    Fraction
    Water Probe Rinse
    Filter
    Front-Half Total
    Implnger Contents &
    Back-Half Water Rinse
    Total Particulate
    Fina 1
    Weight
    (gm)
    96.3448
    1.1162
    148.6669
    	
    101.7626
    	
    Tare
    Weight
    (gm)
    94.8061
    0.7889
    94,3484
    	
    101,7594
    	
    Weight
    of
    Particula te
    (gm)
    1 .5387
    0.3273
    54,3185
    	 •
    0 ,0032
    	
    Applicable
    Blank
    Value
    (gm)
    <0.0001
    0,0005
    — -
    0.0073
    	
    Blank-
    Corrected
    Particulate
    (eซ0
    1.5387
    0.3268
    54.3185
    56.1840
    <0.0001
    56 .1840
                                      Clayton Environmental Consultants,  Ine ,
    

    -------
       APPENDIX H
    CALIBRATION DATA
    

    -------
        SUMMARY OF PARTICULATE WEIGHT  FRACTIONS
            NO.  2  MILL BAGHOUSE SOUTH INLET
    
    International  Minerals and Chemicals Corporation
              Spruce  Pine, North  Carolina
                  September 27-29,  1976
    Test
    No.
    
    
    
    
    
    
    
    Frac tion
    Mater Probe Rinse
    Filter
    
    iron.C"*MajLI JLOtax
    Itnpinger Contents &
    Back-Half Water Rinse
    
    Totfll Particulate
    Fina I
    Weight
    (gra)
    92.1401
    5.9924
    
    
    94.7524
    
    
    Tare
    Weight
    (sm)
    91 .6736
    0.8068
    
    
    94,7497
    
    
    Weight
    of
    Particula te
    (sm)
    0,4665
    5.1856
    
    
    0.0027
    
    
    Appl iea ble
    Blank
    Value
    (งm)
    <0.0001
    0 .0005
    
    
    0,0076
    
    
    Blank-
    Correc lad
    Particulate
    Cgm)
    0 ,4665
    5.1851
    S 6 S16
    
    <0 ,0001
    5 6516
    
                                      Clayton Environmental Consultants,  Ine
    

    -------
     ^ i ,
    ;•;*,'   i
    i!.  '  •
                                                Aftl) UK.J.J.1 -
    
                                Calibrator
    trie ,,Pressure Pb  ("Hg)
                                                        /o
                             Meter Box Number  /?/?
                             Gas  Meter Number
       .. i-
    1 -'",1 "'
    Stop, <
    bLrtrt
    Average
    Stop
    Start
    \vcrafje
    Slop,
    S t a r t
    A V C V P ft C
    Stop ,
    Start <
    Average
    Stop -
    Start
    Average
    
    Stop ,.
    Start ,
    Average
    
    4
    Orifice
    Manometer
    Sett ing , A m
    (in. H20)
    (0.5) O. <>
    C, f
    0,<
    (1,0) /•<>
    /.tf
    /. *>
    (2-,C) ' 3
    -. o
    .''.4
    (3.0) 3'-^
    3 • <>
    ' •* r j
    . > i v
    ("& . 0 ) '/ ^
    : - ^ t/, \)
    1 l/,(/
    
    (5.0) <,Q
    *;0
    > • <, (^
    
    Gas Volume
    Wet Test
    Meter
    ^ฃ70, on
    ^>~? 'SZ.oo
    (5) _r.^o
    jrt*?*rt>c.
    J't '/&-<> a
    (5) tr.5 / U 5 1 C O
    JTd ?f. o o
    (io)/o^7(;
    o-7/.r tf^
    ^yVlTrW
    _L\U}s0-0t>
    3'7ฃSs
    &?/&. €' C>
    (lb}/6 ,ev
    
    f? 4$',ซซ
    ^7 ฃ•,'*ฃ><>
    (10)|0.01C?
    
    Gas Volume
    Dry Gas
    Meter
    (ft-3)
    S'/J^.Wtf
    Vets' Vdv
    ^'9f/<
    V/X ^fi*
    ^.09. ?^
    /O - 3'fJL
    jslf.. /V'-J
    y J5". r^2
    / .13.6 1 3 ซ to
    Tempo r n tut e
    Test
    Meter
    
    <<<7
    
    
    ^ 7
    
    
    ^' 9
    
    
    7o
    
    
    70
    
    
    
    7c>
    
    
    V,
    _ \
    Dry Gas Meter
    Inlet
    $0
    ฅ0
    60
    *4
    $0
    !L
    72
    yt.
    ^?
    7^
    c/ ^
    9^
    7V
    7 V
    ^/y
    
    /^'^
    C7^-
    lct
    
    Outlet
    tcdo
    7^
    ^'y
    ^^?
    74
    70
    72.
    7V
    74
    7(,
    ^Z
    ?Y
    ^C>
    ฅ.3
    ฅ2,
    4*,*
    
    v4
    •33
    ฃ34
    
    
    r . / Pw
    ra 0 \| TT Am
    Average
    td
    74*
    74*
    74. ^ ^
    ^<0
    7~*
    77,0"
    Vฃ
    yo
    •X2,^y
    96
    r.<
    JZ.f'
    f/6.4
    f/o
    .&
    
    */ฃ
    */ฃ.*
    *}/, 2-4*
    
    Vacuum
    Wet Test
    Meter
    pw
    (in. I120)
    
    . 05
    
    
    . ^^
    
    
    *OS
    
    
    ,&.?
    
    
    / ><-><:
    
    
    
    / . nf
    
    
    Time
    6
    (nin)
    ^
    V.6S
    7^: 05
    jO^1
    ^
    
    9 ^^1
    
    AVERAGE
    Me tier
    CorrccLioi
    Factor
    (/)
    I. tio
    U'
    t
    t-'
    /?r ^v 'J
    
    ^?. ?'5.
    
    iX97/
    •*Tn
    i'
    ix
    i
    ^x,,-;
    ,,--->
    
    *^:
    
    ^/;"'^
    
      Vw Pw  (bd'+ 460)
         PrT  (tvr  + 460)~
    Isolcinatic  Factor  (ISO)  •"
                                                                       27.40
                                                                       ("Km)'''
     27,40
    (
    

    -------
                             Calibrator
                                                                   Meter Box Number
           Pressure  Pb  ("Hg)
                                                                   Gas Meter Number   /l/jc.
    \ • IU ,,
    " prJ •
    '• '* ^;"-f* *
    1 !„ .
    Stop!
    S t n'r t
    .Wcvase
    Stopp
    S t A r t
    \verage
    S t Q p x
    Stsrt:
    vverpSG
    Stop,
    Start
    Lvcrage
    Stop |,
    Stsrt
    vox-age
    
    Stop'ff •
    Stcrt,
    vcrage
    
    Orifice
    Manometer
    Setting^ Am
    (in. H20)
    (0.5)
    
    
    (1,0)
    
    
    (2.0)
    i ,
    
    (3.0)
    
    
    ("4', 0 )
    
    
    
    (5.0)
    ** * -i *
    
    
    Gas Volume
    Wet Test
    Meter
    (fS)
    jT$cฃ-o<)
    &&&&. oo
    ( 5 ) 3* GO
    ฃ % /O ,CC>
    ^
    (10)/d-00
    ,/ 9 J?O , c-' #
    ^^>fC?,C'0
    ao)/^. ^t>
    ฃฃ>0
    S3 30 foe>
    (10) / o
    (10)/j?,oป
    
    Gas Volume
    Dry Gas
    Meter
    7.5^,^J^
    ฃ•ฃ. 7, ^C? Cป
    .5". /^/2
    z a 7-. &/a
    ^. 3^ 43Z
    ,-T. / /T
    z47. ^
    7?
    79*';
    *^ฃ
    ฅ2.
    ^&$"
    C)Q. f
    rt O- ^
    [J jf 5
    ฃ?• ^
    •v-V.^
    ^0.5
    7/, */
    
    ^
    72--^
    75
    
    Vacuum
    Wet Test
    Meter
    PW
    (in, 1!20)
    
    .OS
    
    
    .& ฃ
    
    
    >&ฃ
    
    
    .Off
    
    
    .0^
    
    
    
    .oฃ
    
    
    Time
    8
    (min)
    %%
    \ W
    /A \ v
    1 ^
    ^,
    ^
    
    f A
    - \"j t'
    
    AVERAGE
    Meter
    Conrccticn
    Factor
    /O C7C'/')
    Cxa /otx
    /O ^7$
    tr*
    OW~
    *s
    
    J\ f\ f)f 1
    ft t, J f\ I
    
    \/
    ซ,
    Ir-
    C/,* / 2 o I
    <'*ป
    0,^
    0. V-l!
    
    O.I&
    
    *'
      •v  p   ru
    _; ' VW '*W  * d
    Vd
                                         Isokinetic Factor  (ISO)
    27.40
    (Km)1"
                                                                               27>40
    

    -------
           S , f~ %
                                Calibrator
    irbncfiric'Pressure  Pb  ("llg)
    Mater Box Number
    Gas Meter Number
    11 ll
    -' !j;i!
    top .! '
    cart ;j .
    1 c r a g c
    it OP | it
    .tart cr age
    top •• t ,
    tart*'
    •erage
    
    eopv -
    t ft r t ;y
    Ner af;e
    
    1, Orifice
    nanometer
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    Instrument No.-Pyrotest   73090015  Ifxniraite,
    
    
    
    
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    -------
                GKQRGF,  D,  CLAVfOn  & ASSOCIMES
    
    
    
    
                    POTENTI011ETER  CALIBRATION
    
    
    
    
    
    
    
    Instrument llo.-Pyrotc.st   73090015  llininitc  s??c x? ฃs.-  3/ / o /
    
    
    
    
               S ca le-Pyro tcs t  ^	 t.iriuii ce ^'/g
         METER
    STANDARDIZATION
    Lbratcd By
    ^
    1 June. Temp.
    int
    ites t
    ling
    ฐF
    100
    200
    300
    400
    500
    600
    700
    800
    900
    1000
    1100
    1200
    1300
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    1500 - •
    1600 '"-^"
    .1700 , /,.'_"
    "
    ฃ.s./s
    '*/*/?*
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    .
    

    -------
         APPENDIX I
    EXAMPLE CALCULATIONS
    

    -------
    Nomencla ture
    
                               o
    AS    =  Stack  area.,  inches
    
    
    Cf    =  Front  half  (probe 6. filter) parfciculate  concentration3
             gr/DSCF
    
    
    Cp    =  Pitot  tube  correction factor, dimensionless
    
    
    Ct    =  Total  particulate concentration,  gr/DSCF
    
    
    CMf   =  Front  half  (probe & filter) particulate  concentration,
    CM^   = Total  particulate concentration, m
    
    
    Dn    = Sampling  nozzle diameter, inches
    
    
    ERf   = Emission  rate of front half particulate,  Ib/hr
    
    
    ERt   = Emission  rate of total particulate,  Ib/hr
    
    
    ERMf  = Emission  rate of front half particulate,  kg/hr
    
    
    ERMt  = Emission  rate of total particulate,  kg/hr
    
    
    Mjj    = Mole fraction of dry gas, g/g-mole
    
    
    MW    = Molecular weight of wet stack gas
    
    
    MW,   = Molecular weight of dry stack gas
    
    
    p,     = Barometric pressure, inches mercury
    
    
    P     = Average orifice pressure drop, inches water
    
    
    P     = Absolute  stack gas pressure, inches  mercury
    
    
    Pgt   = Static pressure of stack gas, inches mercury
    
    
    Q     = Dry stack gas flowrate at standard conditions, DSCFM
    
    
    SWf   = Front half sample weight, mg
    
    
    SW    = Total  sample  weight, mg
    
    
    Tm    = Average meter temperature, ฐF
    
    
    TS    *= Stack  temperature, ฐF
    
    
    Tฃ    = Net time  of test, minutes
    
    
    Vm    ~ Vo^ume ฐf ^ry Sas at meter conditions, ft^
    

    -------
    V     = Volume  of dry gas at  standard  conditions, BSCF
      s td
    
    Vs    = Stack  gas velocity  at  stack conditions,  fpm
    
    
    Vw    = Total  condensate collected  in  sampling train, ml
    
    
    V.,    = Volume  of water vapor  at  standard conditions, SCF
     "gas                      r                           *
    
    AP    - Velocity pressure,  inches water
    
    
    %I    - Percent of isokinetic  variation, dimensionless
    
    
    %M    = Percent moisture, dimensionless
    
    
    
    
    Calculation  of  Particulate Emissions
    
    
         The  dry volume of sampled  gas  corrected to  standard condi-
    
    
    tions of  20ฐC  and 760 mm Hg  (29-92  in,  Hg) is calculated as fol-
    
    
    lows ;
    
         V     =  17.65 * Vm * Pb •
                             T  + 460
                              m
    
    
    The sampled  volume for the first  particulate test taken  on the No.
    
    
    2 Mill Baghouse  Outlet at the  International Minerals and  Chemicals
    
    
    Corporation  is:
                                       2,32
    v         17.65  (105.631) [27.23 '
    
     mstd
                                   /
                                   [27.
                              (119 + 460)
    
    
               =  88.230
    
    
    The dry  stack gas flowrate corrected  to standard conditions is
    
    
    calculated using the following set  of equations sequentially;
    
    
         Vw    =  0.0471 * V
           gas              w
    
                    100 * Vw
         7aM    .  _^	   8"
                         -f V
                            wgas
                   100 - TM
    MW,
                  (7.C02 * 44/100) +  (%02  * 32/100) +  [(%CO  + %N2)*28/10o]
    

    -------
                                   - 3 -
         MW     =  (KW   *  M)  + 18(1 -
                           d
                  Pb  + Pst
                                                    *-J	L
    
    
                                                     I    5
    V      =  5120.8  *  C  *1/AP  *  (T  +  460)   ..	
     s                  p   V   s     s       '   V  p  * MW
                   0.1225  * V  * A  * M  * P
    
         Q      a            s    s    d    s
          S       -_ •_ _ -| __ __^-__! ___ _ _ -    - - - - - - _
                            T  + 460
                             S
    
    
    
    
    
    
         The calculations  for determining  the  flowrate  for the first
    
    
    
    
    particulate  test  on  the No. 2 Mill Baghouse  Outlet  follow.  This
    
    
    
    
    sampling location has  a 19-inch interior diameter.
         V      -  0.0471  (32)
          w
           gas
    
                =  1.507
                     100  * 1.507
                    88.230 + 1 ,507
    
    
    
                   1.68
                   100  -  1.68
                = -
    
          d           100
    
    
    
                ซ  0.98
         MWd    ซ=  29  (Because this is not  a  combustion source, MW^  is
    
    
    
    
                       assumed to be the molecular weight of air.)
    
    
    
    
    
    
         MW     =  (29  * 0.98) + 18(1 - 0.98)
    
    
    
    
                =  28.78
    
    
    
    
    
    
         P^     •=  27.23 - 0.12
          S
    
    
    
                •=  27.11
         V      =  5120.8 (0.839) (16.767)  ,,
    
          s                                 I/  27.11  (28.79)
    
    
             r - =  2579            '    '•  -
    

    -------
               =  0-1225  (2579)  (283.5)  (0.98) (27.11)
                                (105 4- 460)
               = 4210
         The equation  employed  to determine percent of  isokinetic
    
    variation is:
                  1032  *  (T,  +  460)  * V
                  Vs  *  Tfc  * Ps * Md * (Dn)2
    
    For the first particulate  test taken at the No, 2 Mill  Baghouse
    
    Outlet j
    
                        1032 (105 + 460)  (88.228)
         Ja J    EJ                                 II
                    (2579)  (120) (27.11)  (0.98)  (0.25)2
               = 100.1
    
         To determine  the  concentration  of particulate matter  in
    
    grains per dry  standard cubic foot (gr/BSCF), one of the  fol-
    
    lowing equations  is used;
    
                              SWf
         Cf    = 0.01543 * —	—   and
                              rastd
                              SWa.
         C,.    = 0.01543 *
          Jte       v • W -** J ^' -^     _-_       f
                              mstd
    
         When metric units  are desired, the concentration  is  calcu-
    
    lated in milligrams  per dry normal cubic meter (mg/DSm3)  as  fol-
    
    lows ;
    
                         SWf
         CMฃ   =   (0.02832)(Vm  .)	   and
         CM
           t       (0.02832)(V    )
                              mstd
    

    -------
    Front half particulate concentrations  are  obtained by summing the
    
    
    weight of particulate matter  collected on  the filter and all por-
    
    
    tions of the train preceding  it.   Total  particulate concentration
    
    
    includes, in addition, any  particulate matter collected in the
    
    
    impingers.
    
    
         The first particulate  test  taken  at the No.  2 Mill Baghouse
    
    
    Outlet yielded the following  concentrations of filterable and
    
    
    total particulate;
    
    
    
                          27.1
         Cf  = 0.01543 * 	
          r               88.2
    
    
             = 0.0047
    
    
                          27 .1
         C,.  = 0.01543 *
                          88.2
    
    
             = 0.0047
    
    
                     27.1	
    
         CMf *  (0.02832)(S3,2)
    
    
             ซ 10 .8
    
    
               	27.1	
    
         CMt **  (0.02832) (88 .2)
    
    
             = 10.8
    
    
    
         The emission rate  of particulate  matter can be calculated
    
    
    from the filterable  or  total  particulate concentration using one
    
    
    of the following equations:
    
    
         ERf = O.OOS57 *  Cf  * Qs    and
    
    
         ERt = 0,00857 *  Ct  * Qs
    
    
    For metric units,
    
    
         ERMf = (1.70 *  10~6) * CMf * Qs    and
    
    
         ERMfc ป (1.70 *  10~6) * CMt _* Qs   .
    

    -------
                                   -  6  -
    
    
    
    
    
    
    To avoid rounding  errors  it  is preferable to carry out the calcu-
    
    
    
    
    lation of concentration and  emission rate in one operation.
    
    
    
    
         The emission  rates of  front half and total particulate matter
    
    
    
    
    for the first test  taken  at  the  No.  2 Mill Baghouse Outlet are
    
    
    
    
    calculated as follows:
         ER  = 0.00857  (0.0047)  (4210)
    
    
    
    
             ป 0.17
         ERt = 0.00857  (0.0047)  (4210)
    
    
    
    
             = 0.17
        ERMf =  (1,70  *  10~6)  (10,8)  (4210)
    
    
    
    
             -  0.08
        ERM  =  (1.70  *  10"6)  (10,8)  (4210)
    
    
    
    
             "  0.08
    

    -------
    DRAFT/WP
    d3006-4/971130
    03/30/92  1
                    "RATES/
                          Emission Test Report
                            Review Checklist
                                 Reviewer :
                                 Review Date:
    A.  Background Information
    
        l.   Facility name:
    
            Location:
        7.
    pi
                                  int
            Source category:
    
            Test date:
            Test sponsor:
            Testing contractor:
    
        6.   Purpose of test:   P
    -------
    DRAFT/WP
    d3006-4/971130
    03/30/92  2
    
    B.  Process Information
    
        1.  Provide a brief narrative description of the process.
            With as much detail as possible,  (e.g., if a furnace or
            conveyor system is used, identify the type of unit)
            describe the equipment used for those operations tested.
            (Note:  If process description provided in test report is
            adequate, attach copy or reproduce herej
                                             '"
    

    -------
    DRAFT/WP
    33006-4/971130
    03/30/92  3
    
        2.  For each process tested list feedstock materials and
            products.  Indicate if activity factors are for feed  (F)
            rate or product  (P) rate.
    Process ID
    A
    
    
    
    
    
    
    
    Feedstock materials
    
    
    
    
    
    
    
    
    Products
    
    
    
    
    
    
    
    
    Basis for activity
    factor
    
    
    
    
    
    
    
    
    F/P
    
    
    
    
    
    
    
    
    Basis for data:
                         (Indicate page/table Nos. in test report)
        3.   For each process or operation tested and each test run
            note process capacity and operating rate during test.
    Process ID
    
    Capacity
    
    Units
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Test run
    I
    2
    3
    4
    1
    2
    3
    4
    1
    2
    3
    4
    1
    2
    3
    4
    Process rate
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Urals
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Basis for data;
    

    -------
    DRAFT/WP
    d300€-4/97H30
    03/30/92  4
    
    C.  Air Pollution Control Systems Tested
    
        1.  For each air pollution control system pollution control
            system identified in A.8, note the following
    ID
    
    
    
    
    
    
    
    Type of APCD
    
    
    
    
    
    
    
    Manufacturer
    
    
    
    
    
    
    
    Model No.
    
    
    
    
    
    
    
    Note:  Be as specific as possible in identifying APCD.  For
    example, indicate "pulse jet fabric filter" rather than simply
    "fabric filter."
        2.  For each system identified above, provide a narrative
            description.  For fugitive systems describe capture
            techniques as well as the removal techniques (use a
            separate page if necessary)
    

    -------
    DRAPT/WP
    33006-4/971130
    03/30/92  5
    
        3.  Using the attached parameter list for guidance complete
            the table below. (Use additional pages as needed.)
    APCDID
    
    Type of
    APCD
    
    Type of
    APCD:
    
    Type of
    APCD:
    Parameter
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Unita
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Readings
    Run 1
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Run 2
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Run 3
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Run 4
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    "
    
    
    

    -------
    DRAFT/WP
    (33006-4/971130
    03/30/92  6
    
    D.  Sampling and Analysis Methods
    
        1.  Complete the following table
    Test location
    
    
    
    
    
    
    
    
    
    
    Pollutant
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    SSt A method
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Reference/
    conditional
    method
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Deviations
    noted
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    Y/N
    

    -------
    DRAFT/WP
    (13006-4/971130
    03/30/92  7
    
        2.  If a method used was not a reference or conditional
            method,  provide a narrative discussion including any data
            manipulation needed to make results correspond to
            reference or conditional method results.
        3.   Describe any deviations identified above,
    

    -------
    DRAFT/WP
    33006-4/971130
    03/30/92  8
    
    B.  Emission Data Documentation
    
        1.  Tabulate the following stack gas data from the test
            report^ (Use additional pagea as needed,)
    TestID
    
    
    
    
    
    
    Parameter
    Stack temperature
    Moisture
    Oxygen
    Volumetric flow, actual
    Volumetric flow, standard
    Percent isokinetic
    Units
    
    
    
    
    
    
    Values reported
    Run 1
    
    
    
    
    
    
    Run 2
    
    
    
    
    
    
    Run 3
    
    
    
    
    
    
    Run 4
    
    
    
    
    
    
    Pollutant concentration;
    
    
    
    
    
    
    
    Stack temperature
    Moisture
    Oxygen
    Volumetric flow, actual
    Volumetric flow, standard
    Percent isokinetic
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    Pollutant concentration:
    
    
    
    
    
    
    
    Stack temperature
    Moisture
    Oxygen
    Volumetric flow, actual
    Volumetric flow, standard
    Percent uolcuifitic
    Pollutant conccntrub on:
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    
    

    -------
    DRAFT/WP
    33006-4/971130
    03/30/92  9
    
        2.   Tabulate  pollutant  mags flux ratea
    Test ED
    Pollutant
    Units
                                   Run L
                                   Run 2
                             Mass flux rates
    
                                   Run 3
    Run 4
    

    -------
    DRAFT/WP
    d3006-4/97H30
    03/30/92  10
    
        3.  Present example emission factor calculations below.
    

    -------
    DRAFT/WP
    d3Q06-4/971130
    03/30/92   11
    
         4.  Tabulate emission factors
     Procesi
    Pollutant
    Ualts
                                                        Avenge emission factor
                                                    Uncontrolled
                                                    Controlled
    b3006-4/971130
    

    -------