vxEPA
United States
Environmental Protection
Agency
Evaluation of Sediment
Agitation and Mixing into the
Surrounding Water
Column from Capping
- Boston Harbor
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EPA/540/R-05/014
July 2006
Evaluation of Sediment Agitation and Mixing
into the Surrounding Water Column from
Capping Activities - Boston Harbor
Final Report
by
Battelle
Columbus, Ohio 43201
Contract No. 68-C7-0008
Work Assignment No. 4-26
George T. Moore
Project Officer
Terrence Lyons
Work Assignment Manager
National Risk Management Research Laboratory
Office of Research and Development
U.S. Environmental Protection Agency
Cincinnati, Ohio 45268
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Notice
The information in this document has been funded wholly or in part by the U.S. Environmental Protection
Agency (EPA) in partial fulfillment of Contract No. 68-C-00-181 to Tetra Tech EM, Inc. It has been subject
to the Agency's peer and administrative review, and it has been approved for publication as an EPA
document. Mention of trade names of commercial products does not constitute an endorsement or
recommendation for use.
11
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This report is a work prepared for the United States Government by
Battelle. In no event shall either the United States Government or
Battelle have any responsibility or liability for any consequences of any
use, misuse, inability to use, or reliance on the information contained
herein, nor does either warrant or otherwise represent in any way the
accuracy, adequacy, efficacy, or applicability of the contents hereof.
in
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Foreword
The U.S. Environmental Protection Agency (EPA) is charged by Congress with protecting the
Nation's land, air, and water resources. Under a mandate of national environmental laws, the
Agency strives to formulate and implement actions leading to a compatible balance between
human activities and the ability of natural systems to support and nurture life. To meet this
mandate, EPA's research program is providing data and technical support for solving
environmental problems today and building a science knowledge base necessary to manage our
ecological resources wisely, understand how pollutants affect our health, and prevent or reduce
environmental risks in the future.
The National Risk Management Research Laboratory (NRMRL) is the Agency's center for
investigation of technological and management approaches for preventing and reducing risks
from pollution that threaten human health and the environment. The focus of the Laboratory's
research program is on methods and their cost-effectiveness for prevention and control of
pollution to air, land, water, and subsurface resources; protection of water quality in public water
systems; remediation of contaminated sites, sediments and ground water; prevention and control
of indoor air pollution; and restoration of ecosystems. NRMRL collaborates with both public and
private sector partners to foster technologies that reduce the cost of compliance and to anticipate
emerging problems. NRMRL's research provides solutions to environmental problems by:
developing and promoting technologies that protect and improve the environment;
advancing scientific and engineering information to support regulatory and policy decisions; and
providing the technical support and information transfer to ensure implementation of
environmental regulations and strategies at the national, state, and community levels.
This publication has been produced as part of the Laboratory's strategic long-term research plan.
It is published and made available by EPA's Office of Research and Development to assist the
user community and to link researchers with their clients.
Sally Gutierrez, Director
National Risk Management Research Laboratory
IV
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Abstract
Capping is a common remediation technology for the containment/stabilization of contaminated
sediments. During capping activities, capping material is commonly released from a barge at the
water surface and falls through the water column to the sediment surface, thus providing a clean
surface sediment layer. Little information exists on the potential release of contaminated
sediments during and after the capping operations. This report focuses on the measured release of
contaminants during individual capping events at two Confined Aquatic Disposal Cells (CADs)
located in the Mystic River, Boston, MA. The two CADs (M8 and Ml9) were previously filled
with dredged material contaminated with total petroleum hydrocarbons (TPH), polycyclic
aromatic hydrocarbons (PAHs), and polychlorinated biphenyls (PCBs). U.S. EPA/ORD sampled
the water column during each capping event to evaluate whether cap placement resulted in the
release of contaminated sediments. Results showed capping from the water surface resulted in
contaminant resuspension with the most significant releases occurring during the application of
the first layers of capping material. With each subsequent layering of the capping material, levels
of contaminant resuspension decrease with each successive application.
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CONTENTS
FIGURES iv
TABLES iv
ACRONYMS AND ABBREVIATIONS vi
1.0 INTRODUCTION 1
1.1 Background 1
1.2 Environmental System 2
1.3 Project Objectives 4
2.0 FIELD SAMPLING AND ANALYTICAL METHODS 5
2.1 Marine Water Sampling 5
2.1.1 Sampling and Navigation 5
2.1.2 Monitoring and Sampling Operations 7
2.1.3 Field Measurements and Collection of Water Samples 8
2.1.4 Decontamination of Sample Pumping System 8
2.1.5 Field Observations 9
2.2 Analyses of Organic Contaminants 9
2.2.1 TPH Analysis 10
2.2.2 PAH Analysis 11
2.2.3 PCB Analysis 11
2.3 TSS Analyses 11
2.4 RCRA 8 Metals Analyses 12
3.0 RESULTS AND DISCUSSION 13
3.1 Pre Survey Background 13
3.2 Total Suspended Solids 13
3.3 Total Petroleum Hydrocarbons 15
3.4 Fob/cyclic Aromatic Hydrocarbons 18
3.5 Fob/chlorinated Biphenyls 22
3.6 RCRA 8 Metals 22
3.7 Filtered Samples 27
3.8 Post Survey Sampling 28
3.9 Sand Capping Material 29
3.10 Data Comparisons 30
4.0 CONCLUSIONS 35
5.0 REFERENCES 37
APPENDIX A: BOSTON HARBOR PLUME TRACKING SURVEY REPORT A-l
APPENDIX B: CHAIN OF CUSTODY FORMS B-l
APPENDIX C: QUALITY CONTROL REPORTS C-l
APPENDIX D: TPH LABORATORY-REPORTED SAMPLE DATA WITH QC
QUALIFIERS D-l
APPENDIX E: PAH LABORATORY-REPORTED SAMPLE DATA WITH QC
QUALIFIERS E-l
APPENDIX F: PCB LABORATORY-REPORTED SAMPLE DATA WITH QC
QUALIFIERS F-l
vi
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APPENDIX G: RCRA 8 METALS LABORATORY-REPORTED SAMPLE DATA G-1
APPENDIX H: TSS AND CONTAMINANT OF CONCERN TWO-DIMENSIONAL PLOTS H-1
APPENDIX I: AVERAGE CURRENT VELOCITY PLOTS 1-1
FIGURES
Figure 1 -1. Location of Boston Harbor Navigation Improvement Proj ect and Cape Cod Canal 2
Figure 1-2. Boston Harbor Navigation Improvement Project, Mystic River and Inner
Confluence Disposal Cells 3
Figure 1 -3. Tug Boat Pushing Great Lakes Hopper Dredge, The Manhattan Island 3
Figure 2-1. BOSS In Situ Measurement and Onboard Components 6
Figure 2-2. BOSS Onboard Battelle's Vessel, Aquamonitor 7
Figure 2-3. Transect Line, Sampling Stations, and Station Types for BOSS Surveys and
Monitoring 8
Figure 2-4. Decontaminating the BOSS Between Sampling Events 9
Figure 3-1. Average TPH Concentrations - Cell M19 20
Figure 3-2. Average TPH Concentrations - Cell M8 20
Figure 3-3. Average Total PAH Concentrations - Cell M19 21
Figure 3-4. Average Total PAH Concentrations - Cell M8 21
Figure 3-5. Average Total PCB Concentrations- Cell M19 23
Figure 3-6. Average Total PCB Concentrations- Cell M8 23
Figure 3-7. 2-D Plot of PAH and TSS Concentrations for Run 1 CAD Cell M19 31
Figure 3-8. TPH Plotted Against TSS for Runs lThrough4 32
Figure 3-9. PAHs Plotted Against TSS for Runs 1 Through 4 32
Figure 3-10. PCBs Plotted Against TSS for Runs 1 Through 4 32
Figure 3-11. TPH Plotted Against TSS for Runs 5 through 8 33
Figure 3-12. PAHs Plotted Against TSS for Runs 5 Through 8 33
Figure 3-13. PCBs Plotted Against TSS for Runs 5 through 8 33
TABLES
Table 2-1. Critical and Noncritical Measurements 5
Table 2-2. Field Measurements and Instruments 6
Table 2-3. Number of Samples Collected During the Survey Events at Boston Harbor 7
Table 2-4. Compounds of Interest and Method Detection Limits 12
Table 3-1. Pre Survey Organics Analytical Results 14
Table 3-2. RCRA 8 Metals Analytical Results for Pre Survey 14
Table 3-3. Organics Analytical Results for Run 1 15
Table 3-4. Organics Analytical Results for Run 2 15
Table 3-5. Organics Analytical Results for Run 3 16
Table 3-6. Organics Analytical Results for Run 4 16
Table 3-7. Organics Analytical Results for Run 5 17
Table 3-8. Organics Analytical Results for Run 6 17
Table 3-9. Organics Analytical Results for Run 7 18
Table 3-10. Organics Analytical Results for Run 8 18
Table 3-11. RCRA 8 Metals Analytical Results for Run 1 19
Table 3-12. RCRA 8 Metals Analytical Results for Run 2 24
Table 3-13. RCRA 8 Metals Analytical Results for Run 3 24
Table 3-14. RCRA 8 Metals Analytical Results for Run 4 25
vn
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Table 3-15. RCRA 8 Metals Analytical Results for Run 5 25
Table 3-16. RCRA 8 Metals Analytical Results for Run 6 26
Table 3-17. RCRA 8 Metals Analytical Results for Run 7 26
Table 3-18. RCRA 8 Metals Analytical Results for Run 8 27
Table 3-19. Comparison of Filtered Samples 27
Table 3-20. Organics Analytical Results for Post Survey 28
Table 3-21. RCRA 8 Metals Analytical Results for Post Survey 29
Table 3-22. Organics Analytical Results for Sand Capping Material 29
Table 3 -23. Correlation Coefficients and Linear Regression Values for Runs 1 Through 8 34
Table 3-24. Average Current Velocity and Flow Direction Approximately 2 m Above the
River Bottom 34
Table 4-1. Comparison of Results from Boston Harbor and Eagle Harbor 35
Vlll
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ACRONYMS AND ABBREVIATIONS
2-D
two-dimensional
ADCP Acoustic Doppler Current Profiler
ALQ Analytical Limits of Quantitation
BHNIP Boston Harbor Navigation Improvement Project
BOSS Battelle Ocean Sampling System
CAD confined aquatic disposal
COC contaminant of concern
CTD conductivity, temperature, and depth
DCM dichloromethane
DUP duplicate
BCD electron capture detector
EPC electronic pressure controlled
GC gas chromatograph
GC/FID gas chromatography/flame ionization detection
GC/MS gas chromatography/mass spectrometry
GPS global positioning system
HC1 hydrochloric acid
HP Hewlett Packard
HPLC high-performance liquid chromatography
ICP-MS inductively coupled plasma - mass spectrometry
IUPAC International Union of Pure and Applied Chemistry
K-D Kunderna Danish
LCS laboratory control sample
MDL method detection limit
MLLW mean lower low water
MS matrix spike
MSD mass selective detector
NA not applicable
ND not detected
N-evap nitrogen evaporation
NRMRL National Risk Management Research Laboratory
PAH polycyclic aromatic hydrocarbon
PB procedural blank
PCB polychlorinated biphenyl
psi pounds per square inch
IX
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QAPP Quality Assurance Project Plan
RCRA Resource Conservation and Recovery Act
RF response factor
RIS Recovery Internal Standard
SIM select ion monitoring
SIS Surrogate Internal Standard
SOP Standard Operating Procedure
TPH total (extractable) petroleum hydrocarbons
TSS total suspended solids
USAGE United States Army Corps of Engineers
U.S. EPA United States Environmental Protection Agency
WA work assignment
WAL Work Assignment Leader
WAM Work Assignment Manager
x
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1.0 INTRODUCTION
This technical report was prepared in fulfillment of Contract No. 68-C7-0008, Work Assignment
(WA) No. 4-26 by Battelle under the sponsorship of the United States Environmental Protection
Agency's (U.S. EPA's) National Risk Management Research Laboratory (NRMRL). The work was
conducted at Battelle, Columbus, OH, from April 11, 2000 to September 30, 2001.
Mr. George T. Moore is the U.S. EPA Project Officer for this contract and Mr. Terrence Lyons is
the U.S. EPA Work Assignment Manager (WAM). Dr. Abraham Chen is the Battelle Program Manager
and Battelle Work Assignment Leader (WAL). The members of the Battelle project staff included
Ms. Jennifer Ickes, Mr. Wayne Trulli, Dr. Carl Albro, Ms. Carole Peven-McCarthy, Ms. Lydia Cumming,
and Dr. Victor Magar.
1.1 Background
The U.S. EPA's NRMRL is interested in evaluating if placement of marine caps would result in
the release of contaminants into the surrounding water column. The goal of this study was to achieve a
better understanding of the amount of contaminants released into the surrounding water column before,
during, and after capping. For this study, a state-of-the-art oceanographic technology was used to acquire
real time, high-resolution field data to determine the extent of the release of contaminants into the water
column caused by sediment agitation from capping activities for two confined aquatic disposal (CAD)
cells at the Mystic River/Boston Harbor, Boston, MA. A parallel study conducted under U.S. EPA
Contract No. 68-C7-0008, WA No. 4-30 focused on the resuspension of polycyclic aromatic hydrocarbon
(PAH) compounds during capping at the Wyckoff/Eagle Harbor Superfund site in Bainbridge Island, WA
(Battelle, 2001).
A common remediation technology for the containment/stabilization of contaminated sediments
is capping. Capping is the covering of contaminated sediments with sand, gravel, or fine-grain dredged or
excavated materials. During capping activities, tons of capping material are released from barges at the
water's surface to fall to the sediment layer below. Caged fish located downstream of the capping site
have been used to try to evaluate the extent of exposure from individual capping activities. Little
information exists on the amount of contaminants released into the surrounding water column during and
after capping.
CAD cells in Boston Harbor were used as disposal sites for silty, fine-grained sediments that were
determined to be unsuitable for ocean placement from the Boston Harbor Navigation Improvement
Project (BHNIP). Two of the CAD cells, located in the Mystic River portion of Boston Harbor (Fig-
ure 1-1), were filled with dredged material in January 2000. The two cells, M8 and M19 (Figure 1-2),
were left undisturbed for 8 months to allow the dredged material to consolidate prior to capping.
Consolidation was expected to reduce mixing between the sediments in the CAD cells and the cap
sediments.
CAD cell M8 was 700 ft by 200 ft, was excavated to 90 ft deep, and had an estimated capacity of
155,000 yd3 of dredged material. CAD cell M19 was the larger of the two cells at 800 ft by 300 ft, was
excavated to 80 ft deep, and had an estimated capacity of 179,000 yd3 of dredged material. Average
concentrations of total petroleum hydrocarbons (TPH), polychlorinated biphenyls (PCBs), and PAHs
measured in CAD cells from the Mystic River were 1,519 mg/kg, 220 ng/kg, and 64,478 ng/kg, respec-
tively (USAGE, 1999a). These concentrations were not measured in either CAD cells M19 or M8.
However, all CAD cells in the Mystic River were filled with dredged material from the same location, so
concentrations of the material placed in cells M8 and M19 should be consistent with these concentrations.
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Chelsea River
20000 0 20000 40000 Feet
Figure 1-1. Location of Boston Harbor Navigation Improvement Project and Cape Cod Canal
(Source: Fredette et al., 2000)
Sand dredged from Cape Cod Canal (Figure 1-1) was used to cap CAD cells M8 and Ml9
(Fredette et al., 2000). The sand cap was "sprinkled" on the cells using a partially opened hopper dredge,
which was maneuvered using a tug rather than utilizing the dredge's engines (Figure 1-3). This method
of capping was expected to minimize disturbance of the silt material in the CAD cells.
1.2 Environmental System
During a May 16, 2000 site visit, the U.S. EPA WAM, U.S. EPA Region 1 office, United States
Army Corps of Engineers' (USACE's) New England District, and Battelle identified Boston Harbor as a
suitable candidate site for monitoring sediment agitation and mixing during a capping event. Boston
Harbor was selected for this study for the following reasons:
The site has a well-documented history of contaminated sediments disposal, which made
identification of contaminants of concern (COCs) easier and eliminated the need for
sample collection and analysis for site characterization.
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400 BOO Feet
Figure 1-2. Boston Harbor Navigation Improvement Project,
Mystic River and Inner Confluence Disposal Cells (Source: Fredette et al., 2000)
Figure 1-3. Tug Boat Pushing Great Lakes Hopper Dredge, The Manhattan Island
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COC concentrations in the CAD were high enough to make detection possible during
monitoring.
The U.S. EPA Region 1 Office and the USACE's New England District expressed
interest in this study and agreed to provide technical support for the field efforts,
including data exchange.
The site was well characterized, thereby provided a large database of information to
select appropriate sample locations.
The capping of the CADs took place during fiscal year 2000, allowing field activities to
be completed during the time allotted for this work assignment.
1.3 Project Objectives
The primary objective of this work assignment was to evaluate if cap placement resulted in the
release of contaminants into the surrounding water column. This report focuses on results of water
quality analyses during capping events at the two Boston Harbor/Mystic River CAD cells.
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2.0 FIELD SAMPLING AND ANALYTICAL METHODS
This section describes field sampling methods used at Boston Harbor, and methods used to
analyze samples for TPH, PCBs, and PAHs, and Resource Conservation and Recovery Act (RCRA)
8 metals. Field and analytical methods were conducted in accordance with a U.S. EPA-approved Quality
Assurance Project Plan (QAPP) for the study (QAPP I.D. No. 206-Q2-0) (Battelle, 2000). The
experimental design is described in Section 2.0 of that QAPP.
Table 2-1 identifies both critical and noncritical measurements that were made during the course
of this study.
Table 2-1. Critical and Noncritical Measurements
Measurement
Method/Instrument
Critical Measurements
TPH (fingerprint) in water
PCBs in water
PAHs in water
RCRA metals in water
TSS
Transmissometry/ Turbidity
GPS Navigation
Battelle SOP 5-202
Battelle SOP 5-128
Battelle SOP 5-1 57
U.S. EPA Method 200.8
Battelle SOP 5-053
Seatech 20-cm (660 nm)
Battelle SOP
Noncritical Measurements
Conductivity
Temperature
Depth
Current velocity
OS200 CTD
OS200 CTD
Furuno FCV-52
RD Instruments ADCP WHM600-I-UG6
ADCP = Acoustic Doppler Current Profiler.
CTD = conductivity, temperature, and depth.
GPS = global positioning system.
SOP = Standard Operating Procedure.
TSS = total suspended solids.
2.1 Marine Water Sampling
2.1.1 Sampling and Navigation. Monitoring of the capping event was conducted using the Battelle
Ocean Sampling System (BOSS) deployed from a survey vessel. The BOSS in situ sensor package
included: conductivity, temperature, depth, and transmissometers, and a Teflon/titanium pumping
system for sample collection (Figure 2-1). A second transmissometer, calibrated to the in situ data, was
located at the water sampling manifold so that the appropriate parcel of water could be identified and
sampled at the appropriate time. Additionally, an Acoustic Doppler Current Profiler (ADCP) was
deployed to obtain vertical profiles of horizontal currents. Table 2-2 provides a summary of the field
measurements that were acquired from the survey vessel during each monitoring event. A more detailed
description of monitoring activities and sample collection can be found in the Boston Harbor Plume
Tracking Survey Report (Appendix A).
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Winch and Handling System
Navigation
Figure 2-1. BOSS In Situ Measurement and Onboard Components
Table 2-2. Field Measurements and Instruments
Measurements
Conductivity
Temperature
Pressure
Transmissometry /Turbidity
Bottom depth
Navigational position
Ocean current velocity
Units
|imhos/cm
°C
m
nT1
m
degrees
cm/sec
Instrument
OS200 CTD
OS200 CTD
OS200 CTD
Seatech 20-cm (660 nm) (2)
Furuno FCV-52
Northstar 942X
RD Instruments ADCP WHM600-
I-UG6
Several days prior to the field operations, all equipment was installed aboard the survey vessel
and tested. Two days prior to the initiation of capping, background sampling events were conducted at
CAD cells M8 and M19. Monitoring for both cells was a deviation of the approved QAPP (Battelle,
2000), which stated that either cell M8 or cell M19 would be monitored. Monitoring of both cells was
unavoidable because the hopper dredge was unable to cap one CAD cell continuously as the USAGE had
anticipated. Monitoring activities were conducted in approximately 14-hour intervals. Each 14-hour
interval included approximately 1 hour of capping for each barge drop plus 13 hours of barge reloading.
The hopper dredge was reloaded at Cape Cod, MA.
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2.1.2 Monitoring and Sampling Operations. Field survey operations consisted of 10 separate
sampling events conducted over a 22-day period (approximately two events per day plus background
samples before and after capping). All 10 events were conducted using the BOSS (Figure 2-2). During
the first event, sensor data and water samples were collected prior to initiation of capping activities at
CAD cells M8 and Ml9 for baseline/reference data. During the next eight events, sensor data and water
samples were collected while capping activities were conducted at either cells M8 or M19 (Table 2-3).
During the last (10th) event, sensor data and water samples were collected four days after completion of
all capping activities at cells M8 and M19. Figure 2-3 shows the target BOSS transects and target
sampling locations used for background surveys and active monitoring events (i.e., during capping).
Figure 2-2. BOSS Onboard Battelle's Vessel, Aquamonitor
Table 2-3. Number of Samples Collected During the Survey Events at Boston Harbor
Type of Event
Pre Survey
Pre Runs 1 - 4
Runs 1 - 4
Post Runs 1 - 4
Pre Runs 5-8
Runs 5-8
Post Runs 5-8
Post Survey
Total
Number of Events
per Survey
1
4
4
4
4
4
4
1
-
Number of Samples per Event
CAD Cell M19
5
3
9
553
0
0
0
5
-
CAD Cell M8
5
0
0
0
3
9
3
5
-
Total
10
12
36
10
12
36
12
10
138
(a) Sampler struck bottom immediately following sample collection for the first Post Run 3 sample,
and system components fouled with mud. As a result the second and third samples for Post
Run 3 could not be collected.
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Area of Study (-80 m x -240 m)
Start I
Current
> End
Trackline before capping
and 1 hour after capping
End
Start
Trackline during
capping operations
Sampling Station
Figure 2-3. Transect Line, Sampling Stations, and Station Types for BOSS Surveys and
Monitoring. The top transect represents the daily Pre Run and Post Run background monitoring events.
The bottom transect represents a typical monitoring event during capping.
A total of 138 water sample sets were collected during the study. Ten sample sets (for organics,
metals, and TSS) were collected during each of the first and last (10th) sampling events along the
Standard Transect Line (five at CAD cell M8 and five at CAD cell M19) (see Figure 2-3, Table 2-3, and
Appendix A Table 1). Fifteen sample sets (for organics, metals, and TSS) were collected during each of
the eight capping events (i.e., sampling events 2 through 9). Three samples were collected before and
after each of the two daily capping events (six samples total per event).
During these monitoring activities, real-time BOSS sensor data was collected continuously along
several transects within the designated CAD. The BOSS was towed at a distance of 2 m above the river bot-
tom for all transects (unless obstructed) in order to optimize the potential to detect resuspended sediments.
Three samples were collected along the Pre- and Post-Dump Transect Lines (Figure 2-3). Nine
samples were collected along the Standard Transect Line (Figure 2-3 and Appendix A Table 1) during
actual capping activities for each of the eight sampling events during capping.
Five sediment samples of the sand used as capping material for CAD cells M8 and M19 were
collected by the USAGE. These five samples were analyzed for organic contaminants.
2.1.3 Field Measurements and Collection of Water Samples. Monitoring equipment and sampling
techniques used for the monitoring survey are described in detail in Appendix A and in the approved
QAPP I.D. No. 206-Q2-0 (Battelle, 2000). Chain of custody documentation for all samples collected are
provided in Appendix B.
2.1.4 Decontamination of Sample Pumping System. Prior to each sampling event, the sample
pumping system was decontaminated by pumping the following solvents through the system (Figure 2-4):
Dichloromethane (DCM)
Acetone
5 % hydrochloric acid (HC1)
Deionized water (3 times the tubing volume).
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Figure 2-4. Decontaminating the BOSS Between Sampling Events
All solvents, acids, and aqueous waste residue resulting from the decontamination of field
sampling equipment were collected in separate, approved waste containers and returned to Battelle,
Duxbury, MA where they were disposed of in an appropriate hazardous waste stream.
2.1.5 Field Observations. A complete description of field observations can be found in the Boston
Harbor Plume Tracking Survey Report (Appendix A).
2.2 Analyses of Organic Contaminants
Given holding time constraints, samples were prepared and extracted within 7 days of the
respective collection dates. The extracts from each sample matrix were analyzed for TPH, PCBs, and
PAHs within 40 days of extraction. General physical observations of the samples (e.g., color, visible
sediments, and presence of plant/wood debris) were made and recorded in the laboratory preparation
records. Items such as sediments and debris were removed prior to processing by allowing the samples to
settle before decanting the supernatant for extraction and analysis.
Water samples obtained during field sampling were prepared for analysis of TPH, PCBs, and
PAHs according to Battelle SOP 5-200-02 (Water Extraction for Trace Level Semi-Volatile Organic
Contaminant Analysis) (Battelle, 2000). The method is summarized as follows:
If suspended sediment was visibly present in the water sample, it was filtered through a quartz
glass fiber filter (1.0 jam). Water samples of approximately 1,000 mL were spiked with Surrogate
Internal Standard (SIS) and serially extracted three times with 60 mL of DCM using a separatory funnel.
The SIS compounds added were o-terphenyl, naphthalene-ds, phenanthrene-dio, chrysene-di2, and the
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following PCB congeners1: C12 (PCB 14), C13 (PCB 34), C15 (PCB 104), and C15 (PCB 112). The three
extracts were combined and treated with anhydrous sodium sulfate to remove residual water from the
extract. The dried extract then was concentrated to approximately 0.5 mL using the Kunderna Danish
(K-D) and nitrogen evaporation (N-evap) techniques. The combined extracts were passed through a 2%
deactivated alumina column, and the eluate from the column concentrated to 900 L using K-D and/or
N-evap concentration techniques. This concentrated extract was fractionated by size-exclusion high-
performance liquid chromatography (HPLC) water. The HPLC extract was concentrated under nitrogen,
and the concentrated extract was spiked with Recovery Internal Standard (RIS) (containing 5ot-androstane,
acenaphthene-dio, fluorene-dio, benzo[a]pyrene-di2), and the following PCB congeners: C15 (PCB 96),
C15 (PCB 103), and C16 (PCB 166). The extract then was split for TPH and PAH/PCB analyses.
For selected filtered samples, the filters were placed into a 500-mL glass jar and spiked with SIS
and serially extracted three times with 100 mL of DCM using shaker table techniques. Sand capping
material collected by the USAGE was analyzed in a similar manner as the filters. The SIS compounds
added were o-terphenyl, naphthalene-ds, phenanthrene-dio, chrysene-di2, and the following PCB
congeners: C12 (PCB 14), C13 (PCB 34), C15 (PCB 104), and C15 (PCB 112). The three extracts were
combined and treated with anhydrous sodium sulfate to remove residual water from the extract. The
dried extract then was concentrated to approximately 0.5 mL using the K-D and N-evap techniques. The
combined extracts were passed through a 2% deactivated alumina column, and the eluate from the column
concentrated to 900 L using K-D and/or N-evap concentration techniques. This concentrated extract was
fractionated by size-exclusion HPLC water. The HPLC extract was concentrated under nitrogen, and the
concentrated extract was then spiked with RIS (containing 5a-androstane, acenaphthene-dio, fluorene-dio,
benzo[a]pyrene-d12), and the following PCB congeners: C15(PCB 96), C15(PCB 103), and C16(PCB 166).
The extract then was split for TPH and PAH/PCB analysis.
The following quality control samples were processed along with each batch of <20 water
samples:
1 laboratory control sample (LCS)
1 procedural blank (PB)
1 duplicate (DUP)
1 matrix spike (MS).
A quality control summary for all samples analyzed for organics is provided in Appendix C.
2.2.1 TPH Analysis. The high resolution "fingerprint" of the extractable TPH from each water sample
was conducted at Battelle's Duxbury laboratory using Battelle SOP 5-202-04, Determination of Low
Level Total Petroleum Hydrocarbons and Individual Hydrocarbon Concentrations in Environmental
Samples (Battelle, 2000). This method employed capillary gas chromatography with flame ionization
detection (GC/FID). The analytical system was comprised of a Hewlett Packard (HP) 5890 or equivalent
GC and FID. Prior to sample analysis, a five-point calibration was performed to demonstrate the linear
range of the analysis and to determine the individual compound response factors (RFs) at each calibration
solution concentration. The calibration solution was composed of selected C8 to C36 «-alkanes, pristane,
and phytane. Analyte concentrations in the standard solutions ranged from approximately 1.0 |o,g/mL to
100 jog/mL. The RF at each calibration concentration was determined and the TPH RF was based on the
average response factors of all the target analytes in the calibration solution. A mid-level calibration
check and solvent blank was analyzed for every 10 samples. Samples were quantified against the RIS
5ot-androstane. TPH laboratory-reported sample data is provided in Appendix D.
PCB numbers in parentheses refer to the International Union of Pure and Applied Chemistry (IUPAC) nomenclature.
10
-------
2.2.2 PAH Analysis. Water sample extracts were analyzed for the concentrations of 16 priority PAH
analytes (Table 2-3) by Battelle's Duxbury laboratory using high-resolution capillary gas chromatography
with mass spectrometry (GC/MS) as described in Battelle SOP 5-157, Identification and Quantitation of
Polynuclear Aromatic Hydrocarbons by Gas Chromatography/Mass Spectrometry (Battelle, 2000). The
analytical system was comprised of a HP 5890 or equivalent GC, equipped with an electronic pressure
controlled (EPC) inlet and an HP 5972 or equivalent mass selective detector (MSB) operating in the
selected ion monitoring (SIM) mode. A minimum of a five-point RF calibration was run with analyte
concentrations in the standard solutions ranging from approximately 0.02 ng/uL to approximately
10 ng/uL. The samples were bracketed by passing standard checks analyzed no less frequently than every
10 samples and at the completion of each sequence.
Quantification of individual compounds was obtained by the method of internal standards using
the RIS compound acenaphthene-dio as the quantification internal standard. Total PAH was determined
as the sum of the individual PAH analytes. Laboratory-reported sample data for PAHs is provided in
Appendix E.
2.2.3 PCB Analysis. Water extracts were analyzed for the concentration of 18 PCB congeners by
Battelle's Duxbury laboratory according to Battelle SOP 5-128, Identification and Quantitation of Poly-
chlorinated Biphenyls (by Congener andAroclor) and Chlorinated Pesticides by Gas Chromatog-
raphy/Electron Capture Detection (Battelle, 2000). This method employed high-resolution capillary GC
with an electron capture detector (BCD). The analytical system was comprised of a HP 5890 or equiva-
lent GC equipped with an EPC inlet and dual BCD detectors. A minimum of a five-point RF calibration
was run with analyte concentrations in the standard solutions ranging from 0.005 ng/uL to approximately
1.0 ng/uL. All 18 major PCB congeners (Table 2-3) were included in the calibration standards. The
samples were bracketed by passing standard checks analyzed no less frequently than every 10 samples
and at the completion of each sequence.
Quantification of individual compounds were obtained by the method of internal standards using
the RIS compounds as quantification internal standards using C15 (PCB 103) and C16 (PCB 166). Total
PCBs were determined as the sum of the individual PCB congeners. Laboratory-reported sample data for
PCBs is provided in Appendix F.
2.3 TSS Analyses
Water samples obtained during field sampling were prepared for analysis according to Battelle
SOP 5-053 (Total Suspended Solids) (Battelle, 2000). The method is summarized as follows:
Sample volumes of at least 500 mL were stored at 4°C±2°C in the dark for no more than 7 days.
These samples then were filtered using a polysulfone filter that was 47 mm in diameter and had a pore
size of 0.45 um. All samples were filtered in duplicate. A known amount of sample volume was
decanted into the filtering apparatus and filtered using a vacuum pump at 5 psi. Before the filter was
removed from the filter holder it was rinsed with Milli-Q water adjusted to pH 8. The filter then was air-
dried in a desiccator for at least 48 hours and reweighed.
TSS was calculated as follows:
particle mass (mg)
TSS (mg/L) =
volume of water filtered (L)
11
-------
where: particle mass (mg) = (filter with sample - filter tare weight)
volume of water filtered = (volume measured directly as initial
volume - final volume).
2.4 RCRA 8 Metals Analyses
Water samples obtained during field sampling for metals analysis were prepared according to
U.S. EPA Method 200.8 for total recoverable elements. Samples were acidified with (1+1) nitric acid to
pH < 2 in the field using reagent-grade acid. Samples were held for at least 16 hours at pH < 2 prior to
analysis. All quality control samples specified by U.S. EPA Method 200.8 were prepared with:
1 quality control sample (quarterly)
1 laboratory reagent blank (1 per < 20 samples)
1 laboratory fortified blank (1 per < 20 samples)
1 matrix spike sample (1 per 10 samples).
Water samples were analyzed, without additional laboratory processing, using inductively
coupled plasma-mass spectrometry (ICP-MS). Table 2-4 lists the target compounds and associated
method detection limits (MDLs) for this project. The method detection limits for RCRA 8 metals
reported for this project are higher than can generally be determined by ICP-MS because of matrix
interferences during analysis of the samples. Quality control summaries for samples analyzed for
RCRA 8 metals are provide in Appendix C. Laboratory-reported sample data for RCRA 8 metals is
provided in Appendix G.
Table 2-4. Compounds of Interest and Method Detection Limits
PAHs (ng/L)
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
Indeno( 1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
RCRA 8 Metals (mg/L)
Ag
As
Ba
Cd
Cr
Hg
Pb
Se
MDL
20.12
0.50
0.64
0.59
0.45
0.42
0.53
0.57
0.83
0.44
0.51
0.52
0.78
1.10
1.25
0.68
0.02
0.02
1.5
0.02
0.4
0.0005
0.02
0.2
PCBs (ng/L)(a)
C12(08)
C13(18)
C13(28)
C14(52)
C14(44)
C14(66)
C15(101)
C15(118)
C16(153)
C15(105)
C16(138)
C17(187)
C16(128)
C17(180)
C17(170)
C18(195)
C19(206)
C110(209)
TSS (mg/L)
TPH(ng/L)
MDL
9.60
0.83
1.04
0.86
0.87
0.89
0.69
0.52
0.64
0.35
0.80
0.52
0.84
0.58
0.61
0.65
0.73
0.76
0.1
78.4
(a) Numbers in parenthesis identify IUPAC numbers
12
-------
3.0 RESULTS AND DISCUSSION
This section describes the TPH, PAH, PCB, RCRA 8 metals, and TSS analytical results.
Tables 3-1 and 3-2 list the analytical results forthe Pre Survey. Tables 3-3 through 3-10 list the TSS,
TPH, total PAH, and total PCB analytical results, and Tables 3-11 through 3-18 list the analytical results
for the RCRA 8 metals. Table 3-19 lists TPH, total PAH, and total PCB results for the sand capping
material. Post Survey results are listed in Table 3-20 and 3-21. All samples are listed in the order in
which they were collected by the BOSS. Samples will be described in the following sections using the
terms described below:
Pre Survey: samples taken two days before capping began in Boston Harbor
Pre Run (1-8): samples taken approximately one hour before each capping event
Run (1-4): samples taken during capping at CAD cell Ml9
Run (5-8): samples taken during capping at CAD cell M8
Post Run (1-8): samples taken approximately one hour after each capping event for Runs 1-8
Post Survey: samples taken four days after capping was completed
Sand Capping Material: sand samples collected by USAGE and Great Lakes from the sand
used to cap both CAD cells M19 and cell M8.
Nine of the samples collected during capping were filtered before analysis to determine the
soluble fraction of TPH, PAHs, and PCBs and the amount of these organics sorbed to particulate matter.
Tables 3-3, 3-5, 3-7, 3-8, and 3-9 present the combined concentrations of the filtrate and particulate
matter, and Section 3.7 compares the two fractions of the filtered samples.
3.1 Pre Survey Background
Two days prior to capping, water samples were taken in Boston Harbor using the BOSS. Five
samples each were collected at both CAD cell M8 and cell M19 (Table 3-1). PCB results from all ten
samples showed that PCB levels were less than Analytical Limits of Quantitation (ALQ) prior to capping
in Boston Harbor. For several samples, all 18 PCB congeners were non-detected or were below the ALQ
(
-------
Table 3-1. Pre Survey Organics Analytical Results
Sample ID
Date Collected
Time Collected
TSS
(mg/L)
TPH
(Hg/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
Pre Survey CAD Cell MS
CAD01021
CAD01024
CAD01027
CAD0102A
CAD0102D
9/6/00
9/6/00
9/6/00
9/6/00
9/6/00
12:23
12:24
12:25
12:27
12:32
2.32
2.41
2.60
3.56
2.90
<156.80
8.72
12.74
24.47
14.76
72.26
36.06
40.72
62.14
42.87
-------
Table 3-3. Organics Analytical Results for Run 1
Sample ID
Date Collected
Time Collected
TSS
(mg/L)
TPH
(Hg/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
PreRun 1 CAD CellM19
CAD012AC
CAD012AF
CAD012B2
9/9/00
9/9/00
9/9/00
15:59
16:01
16:02
4.56
5.22
3.61
48.49
<156.80
47.99
61.83
51.80
66.34
-------
Table 3-5. Organics Analytical Results for Run 3
Sample
ID
Date
Collected
Time Collected
TSS
(mg/L)
TPH
(HS/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
PreRun3CADCettM19
CAD01371
CAD01376
CAD0137A
9/10/00
9/10/00
9/10/00
11:16
11:19
11:21
4.09
3.81
3.39
41.10
83.94
42.82
89.00
48.89
56.41
0.99
1.10
0.88
Run 3 CAD Cell M19
CAD01390
CAD01394
CAD01398
CAD0139F
CAD013A2
CAD013A6
CAD013AA
CAD013BO
CAD013B4
9/11/00
9/11/00
9/11/00
9/11/00
9/1 1/00
9/1 1/00
9/11/00
9/1 1/00
9/11/00
1:13
1:16
1:19
1:21
1:26
1:30
1:33
1:39
1:41
26.77
53.43
22.36
31.82
20.83
8.51
9.46
9.16
12.24
58.08W
201. 14W
60.85
62.07
55.54
255.76
213.74
238.85
208.06
186.41W
308.12(a)
168.55
188.14
164.15
72.87
92.43
95.57
69.51
1.67W
7.96(a)
2.91
3.75
3.06
2.16
3.36
2.71
1.83
Post Run 3 CAD CeUM19
-------
Table 3-7. Organics Analytical Results for Run 5
Sample
ID
Date
Collected
Time Collected
TSS
(mg/L)
TPH
(HS/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
Pre Run 5 CAD Cell MS
CAD01469
CAD0146C
CAD0146F
9/14/00
9/14/00
9/14/00
3:33
3:35
3:37
3.50
7.21
4.07
48.25
26.60
47.74
97.46
56.23
39.68
28.30
11.25
-------
Table 3-9. Organics Analytical Results for Run 7
Sample ID
Date Collected
Time Collected
TSS
(mg/L)
TPH
(Hg/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
Pre Run 7 CAD Cell MS
CAD01523
CAD01526
CAD01529
9/15/00
9/15/00
9/15/00
23:35
23:38
23:41
5.18
4.62
6.53
37.02
49.47
43.04
65.72
48.40
52.64
0.86
1.18
0.50
Run 7 CAD Cell MS
C ADO 15 34
CAD01538
CAD0153B
CAD0153E
CAD01541
CAD01544
CAD01547
CAD01547DUP
CAD0154C
CAD0154F
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
0:09
0:14
0:19
0:25
0:26
0:31
0:35
0:35
0:42
0:44
191.74
27.08
20.68
7.38
9.94
7.56
5.87
4.78
5.61
88.01(a)
72.30
52.53
50.27
66.65
71.17
75.24
40.08
32.85
7.27
111.97(a)
185.21
109.81
101.50
87.15
70.74
86.00
59.03
61.98
48.79
1.90(a)
2.02
2.18
1.29
1.60
1.59
1.26
5.08
1.57
Post Run 7 CAD Cell MS
CAD0155E
CAD01561
CAD01564
CAD01564DUP
9/16/00
9/16/00
9/16/00
9/16/00
1:33
1:35
1:39
1:39
4.30
3.41
4.05
21.57
50.42
10.96
133.53
67.35
66.28
108.99
157.55
0.50
1.46
0.80
(a) Value includes both water and sediment concentration for samples that were filtered before analysis. Water and
sediment concentrations are reported separately in Table 3-11.
Table 3-10. Organics Analytical Results for Run 8
Sample ID
Date Collected
Time Collected
TSS
(mg/L)
TPH
(Hg/L)
Total PAH
(ng/L)
Total PCB
(ng/L)
Pre Run SCAD Cell MS
CAD015AB
CAD015BO
CAD015B3
9/20/00
9/20/00
9/20/00
9:43
9:50
9:53
4.25
4.30
2.06
87.36
<156.80
10.97
72.38
57.30
32.14
-------
Table 3-11. RCRA 8 Metals Analytical Results for Run 1
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 1 CAD Cell M19
CAD012ACMM1
CAD012AFMM1
CAD012B2MM1
9/9/00
9/9/00
9/9/00
15:59
16:01
16:02
4.56
5.22
3.61
0.02
O.02
<0.02
0.5
O.5
0.5
0.02
O.02
0.02
O.04
O.04
0.04
0.02
O.02
0.02
0.02
O.02
0.02
0.0005
O.0005
0.0005
0.2
O.2
0.2
Run 1 CAD cell M19
CAD012BFMM1
CAD012C3MM1
CAD012C6MM1
CAD012CCMM1
CAD012CFMM1
CAD012D2MM1
CAD012D6MM1
CAD012DCMM1
CAD012EOMM1
9/9/00
9/9/00
9/9/00
9/9/00
9/9/00
9/9/00
9/9/00
9/9/00
9/9/00
16:59
17:03
17:05
17:07
17:10
17:12
17:17
17:23
17:25
122.40
95.18
122.61
71.56
39.97
114.06
14.28
21.46
46.57
O.02
<0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
O.5
0.5
0.5
O.5
0.5
O.5
0.5
0.5
O.5
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
O.04
0.04
0.047
O.04
0.04
O.04
0.041
0.04
O.04
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
O.0005
0.0005
0.0005
O.0005
0.0005
O.0005
0.0005
0.0005
O.0005
O.2
0.2
0.2
O.2
0.2
O.2
0.2
0.2
O.2
Post Run 1 CAD CettM19
CAD012ECMM1
CAD012FOMM1
CAD012F4MM1
9/9/00
9/9/00
9/9/00
18:33
18:37
18:42
9.10
9.46
9.01
O.02
0.02
0.02
O.5
0.5
0.5
O.02
0.02
0.02
O.04
0.04
O.04
O.02
0.02
0.02
O.02
0.02
0.02
O.0005
0.0005
0.0005
O.2
0.2
0.2
Note: Bold type indicates detected concentrations
Pre Run 1 samples for cell M19 had concentrations similar to background samples, with an
average Pre Run 1 concentration of 59.99 ng/L (Figure 3-3; Table 3-3). Total PAH concentrations
collected during capping were much greater than background and Pre Run 1 concentrations. Total PAH
concentrations in samples taken during Run 1 averaged 1,372 ng/L ± 1,569 ng/L, with a maximum of
5,242.30 ng/L. Post Run 1 samples collected one hour after capping stopped for Run 1 remained elevated
above the Pre Run 1 samples, but decreased significantly from samples collected during Run 1.
Pre Run 2 samples had higher total PAH concentrations compared to the samples collected during
Post Run 1 and Run 2. These samples also had elevated TSS, TPH, and PCB concentrations. The cause
of the higher concentrations in the Pre Run 2 samples is not known. Shortly before the Pre Run 2 samples
were collected, a container ship entered the harbor, passing over cell Ml9. It is possible the turbulence
from this ship's engines caused uncapped contaminants from cell M19 to be resuspended for a short
period of time. Further resuspension after Run 2 was not observed at cell M19.
Total PAH concentrations continued to decrease over the remaining capping events at cell Ml9.
By the end of sampling at cell Ml9, concentrations had returned to background levels measured during
the Pre Survey before capping began. For Runs 3 and 4, total PAH concentrations during each run were
slightly higher than Pre Run and Post Run concentrations.
Samples from Runs 5-8 at cell M8 followed a similar pattern to cell Ml9, but the PAH concentra-
tions for cell M8 were on average lower than those from cell Ml9. The highest PAH concentration for
cell M8 were detected during Run 5 (the first run), with an average concentration of 310 ng/L and a maxi-
mum concentration of 770.72 ng/L (Figure 3-4; Table 3-7). The Post Run 5 concentrations remained
elevated, but PAH levels returned to Pre Survey concentrations by the next morning, as seen by the Pre
Run 6 sampling. The remaining three runs had elevated PAH concentrations averaging around 100 ng/L.
The cause of the elevated total PAH concentrations during Runs 6, 7, and 8 is not known. The Post Run 8
concentrations dropped back to Pre Survey levels with an average concentration of 63.5 ng/L, and a
maximum concentration of 78.47 ng/L.
19
-------
Pre Run 1 Run 2 Run 3 Run 4 Post
Survey Survey
Figure 3-1. Average TPH Concentrations - Cell M19
Pre Run 5 Run
Survey
Run 7 Run 8 Post
Survey
Figure 3-2. Average TPH Concentrations - Cell M8
20
-------
DPreRun
Run
Post Run
Pre Run 1 Run 2 Run 3 Run 4 Post
Survey Survey
Figure 3-3. Average Total PAH Concentrations - Cell M19
fin
13
+^
O
H
Pre Run 5 Run 6 Run 7 Run 8 Post
Survey Survey
Figure 3-4. Average Total PAH Concentrations - Cell M8
21
-------
3.5 Polychlorinated Biphenyls
PCB concentrations in background samples and Pre Run 1 samples were all
-------
J
"an
PQ
PH
-a
Pre Run 1 Run 2 Run 3
Survey
Run 4 Post
Survey
Figure 3-5. Average Total PCB Concentrations - Cell M19
12
lO-p
t ^
fin 6-t"
S 4-
H
0-
Pre Run 5 Run 6 Run 7 Run 8 Post
Survey Survey
Figure 3-6. Average Total PCB Concentrations - Cell M8
23
-------
Table 3-12. RCRA 8 Metals Analytical Results for Run 2
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 2 CAD Cell M19
CAD0130CMM1
CAD0130FMM1
CAD01312MM1
9/10/00
9/10/00
9/10/00
7:19
7:22
7:28
13.98
14.59
16.28
0.02
0.02
O.02
0.5
0.5
O.5
0.02
0.02
O.02
0.04
0.04
O.04
0.02
0.02
O.02
0.02
0.02
O.02
0.0005
0.0005
O.0005
0.2
0.2
O.2
Run 2 CAD Cell M19
CAD0131FMM1
CAD01322MM1
CAD01325MM1
CAD0132BMM1
CAD0132EMM1
CAD01331MM1
CAD01334MM1
CAD01337MM1
CAD0133AMM1
9/10/00
9/10/00
9/10/00
9/10/00
9/10/00
9/10/00
9/10/00
9/10/00
9/10/00
8:51
8:54
8:58
9:11
9:12
9:26
9:28
9:34
9:40
24.36
25.61
35.13
42.16
35.59
12.08
27.89
15.47
16.58
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.5
0.5
0.5
O.5
0.5
O.5
O.5
0.5
O.5
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.04
0.04
0.04
O.04
0.04
O.04
O.04
0.04
O.04
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.0005
0.0005
0.0005
O.0005
0.0005
O.0005
O.0005
0.0005
O.0005
O.2
0.2
0.2
O.2
0.2
O.2
O.2
0.2
O.2
Post Run 2 CAD Cell M19
CAD01348MM1
CAD0134BMM1
CAD0134EMM1
9/10/00
9/10/00
9/10/00
10:14
10:17
10:19
11.54
7.95
14.02
0.02
O.02
O.02
0.5
O.5
O.5
0.02
O.02
O.02
0.04
O.04
O.04
0.02
O.02
O.02
0.02
O.02
O.02
0.0005
O.0005
O.0005
0.2
O.2
O.2
Table 3-13. RCRA 8 Metals Analytical Results for Run 3
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 3 CAD Cell M19
CAD01371MM1
CAD01376MM1
CAD0137AMM1
9/10/00
9/10/00
9/10/00
11:16
11:19
11:21
4.09
3.81
3.39
O.02
O.02
0.02
O.5
O.5
0.5
O.02
O.02
0.02
O.04
O.04
0.04
O.02
O.02
0.02
O.02
O.02
0.02
O.0005
O.0005
0.0005
O.2
O.2
0.2
Run 3 CAD Cell M19
CAD01390MM1
CAD01394MM1
CAD01398MM1
CAD0139FMM1
CAD013A2MM1
CAD013A6MM1
CAD013AAMM1
CAD013BOMM1
CAD013B4MM1
9/11/00
9/11/00
9/11/00
9/11/00
9/11/00
9/11/00
9/11/00
9/11/00
9/11/00
1:13
1:16
1:19
1:21
1:26
1:30
1:33
1:39
1:41
26.77
53.43
22.36
31.82
20.83
8.51
9.46
9.16
12.24
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.5
0.5
O.5
0.5
O.5
0.5
0.5
O.5
0.5
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.04
0.04
O.04
0.04
O.04
0.04
0.04
O.04
0.04
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.0005
0.0005
O.0005
0.0005
O.0005
0.0005
0.0005
O.0005
0.0005
0.2
0.2
O.2
0.2
O.2
0.2
0.2
O.2
0.2
Post Run 3 CAD CettM19
CAD013C9MM1
9/11/00
2:25
5.86
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
24
-------
Table 3-14. RCRA 8 Metals Analytical Results for Run 4
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 4 CAD CellM19
CAD01405MM1
CAD01408MM1
CAD0140BMM1
9/12/00
9/12/00
9/12/00
21:35
21:36
21:38
5.29
5.42
4.33
<0.02
<0.02
0.027
0.5
0.5
O.5
0.02
0.02
O.02
0.06
0.058
0.057
0.02
0.02
O.02
0.025
0.024
0.024
0.0005
0.0005
O.0005
0.2
0.2
O.2
Run 4 CAD Cell M19
CAD01416MM1
CAD01419MM1
CAD0141CMM1
CAD0141FMM1
CAD01422MM1
CAD01425MM1
CAD01428MM1
CAD0142BMM1
CAD0142EMM1
9/12/00
9/12/00
9/12/00
9/12/00
9/12/00
9/12/00
9/12/00
9/12/00
9/12/00
22:14
22:17
22:20
22:24
22:29
22:36
22:37
22:45
22:46
38.72
19.00
16.48
25.03
21.92
17.60
11.75
8.62
7.54
0.024
<0.02
<0.02
O.02
0.029
0.031
0.028
<0.02
O.02
O.5
0.5
0.5
O.5
0.5
O.5
O.5
0.5
O.5
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
0.058
0.061
0.059
0.059
0.058
0.057
0.057
0.056
0.057
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
0.024
0.024
0.024
0.025
0.024
0.024
0.024
0.024
0.024
O.0005
0.0005
0.0005
O.0005
0.0005
O.0005
O.0005
0.0005
O.0005
O.2
0.2
0.2
O.2
0.2
O.2
O.2
0.2
O.2
Post Run 4 CAD Cell M19
CAD01436MM1
CAD01439MM1
CAD0143CMM1
9/12/00
9/12/00
9/12/00
23:32
23:34
23:36
3.49
4.64
3.84
0.028
0.026
<0.02
0.5
O.5
O.5
0.02
O.02
O.02
0.058
0.056
0.047
0.02
O.02
O.02
0.024
0.024
O.02
0.0005
O.0005
O.0005
0.2
O.2
O.2
Note: Bold type indicates detected concentrations
Table 3-15. RCRA 8 Metals Analytical Results for Run 5
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 5 CAD Cell MS
CAD01469MM1
CAD0146CMM1
CAD0146FMM1
9/14/00
9/14/00
9/14/00
3:33
3:35
3:37
3.50
7.21
4.07
O.02
0.02
O.02
O.5
0.5
O.5
O.02
0.02
O.02
0.048
0.047
0.048
O.02
0.02
O.02
O.02
0.02
O.02
O.0005
0.0005
O.0005
O.2
0.2
O.2
Run 5 CAD Cell MS
CAD0147DMM1
CAD01480MM1
CAD01483MM1
CAD01486MM1
CAD01489MM1
CAD0148CMM1
CAD0148FMM1
CAD01492MM1
CAD01495MM1
9/14/00
9/14/00
9/14/00
9/14/00
9/14/00
9/14/00
9/14/00
9/14/00
9/14/00
4:52
5:00
5:04
5:13
5:17
5:24
5:32
5:33
5:39
102.67
70.82
94.15
73.52
44.76
25.59
16.27
24.34
12.96
O.02
O.02
0.02
0.026
0.02
0.036
O.02
0.02
O.02
O.5
O.5
0.5
O.5
0.5
O.5
O.5
0.5
O.5
O.02
O.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
0.055
0.057
0.057
0.056
0.056
0.052
0.049
0.056
0.053
O.02
O.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.02
O.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.0005
O.0005
0.0005
O.0005
0.0005
O.0005
O.0005
0.0005
O.0005
O.2
O.2
0.2
O.2
0.2
O.2
O.2
0.2
O.2
Post Run 5 CAD Cell MS
CAD0149DMM1
CAD014AOMM1
CAD014A3MM1
9/14/00
9/14/00
9/14/00
6:11
6:13
6:16
9.23
8.75
7.93
0.022
O.02
O.02
0.5
O.5
O.5
0.02
O.02
O.02
0.052
0.052
0.049
0.02
O.02
O.02
0.02
O.02
O.02
0.0005
O.0005
O.0005
0.2
O.2
O.2
Note: Bold type indicates detected concentrations
25
-------
Table 3-16. RCRA 8 Metals Analytical Results for Run 6
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 6 CAD Cell MS
CAD014BFMM1
CAD014C2MM1
CAD014C5MM1
9/15/00
9/15/00
9/15/00
8:45
8:47
8:50
2.86
3.19
2.49
0.029
<0.02
O.02
0.5
0.5
O.5
0.02
0.02
O.02
0.051
0.052
0.056
0.02
0.02
O.02
0.02
0.02
O.02
0.0005
0.0005
O.0005
0.2
0.2
O.2
Run 6 CAD Cell MS
CAD014D4MM1
CAD014DBMM1
CAD014DEMM1
CAD014E4MM1
CAD014E7MM1
CAD014EAMM1
CAD014EDMM1
CAD014F3MM1
CAD014F6MM1
9/15/00
9/15/00
9/15/00
9/15/00
9/15/00
9/15/00
9/15/00
9/15/00
9/15/00
9:52
9:57
9:59
10:02
10:06
10:11
10:14
10:22
10:25
51.98
37.58
35.97
30.50
38.13
30.38
11.97
2.93
11.00
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
O.5
0.5
0.5
O.5
0.5
O.5
O.5
0.5
O.5
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
0.063
0.056
0.04
O.04
0.044
O.04
O.04
0.04
O.04
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.0005
0.0005
0.0005
O.0005
0.0005
O.0005
O.0005
0.0005
O.0005
O.2
0.2
0.2
O.2
0.2
O.2
O.2
0.2
O.2
Post Run 6 CAD Cell MS
CAD01511MM1
CAD01514MM1
CAD0151AMM1
9/15/00
9/15/00
9/15/00
11:36
11:48
11:50
5.03
4.80
4.86
0.02
<0.02
<0.02
0.5
O.5
O.5
0.02
O.02
O.02
0.04
O.04
O.04
0.02
O.02
O.02
0.02
O.02
O.02
0.0005
O.0005
O.0005
0.2
O.2
O.2
Note: Bold type indicates detected concentrations
Table 3-17. RCRA 8 Metals Analytical Results for Run 7
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 7 CAD Cell MS
CAD01523MM1
CAD01526MM1
CAD01529MM1
9/15/00
9/15/00
9/15/00
23:35
23:38
23:41
5.18
4.62
6.53
O.02
O.02
0.02
O.5
O.5
0.5
O.02
O.02
0.02
O.04
O.04
0.04
O.02
O.02
0.02
O.02
O.02
0.02
O.0005
O.0005
0.0005
O.2
O.2
0.2
Run 7 CAD Cell MS
CAD01534MM1
CAD01538MM1
CAD0153BMM1
CAD0153EMM1
CAD01541MM1
CAD01544MM1
CAD01547MM1
CAD0154CMM1
CAD0154FMM1
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
9/16/00
0:09
0:14
0:19
0:25
0:26
0:31
0:35
0:42
0:44
191.74
27.08
20.68
7.38
9.94
7.56
5.87
4.78
5.61
0.02
O.02
O.02
0.02
O.02
0.02
0.02
0.04
0.02
0.5
O.5
O.5
0.5
O.5
0.5
0.5
O.5
0.5
0.02
O.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.04
O.04
O.04
0.04
O.04
O.04
O.04
O.04
0.04
0.02
O.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.02
O.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.0005
O.0005
O.0005
0.0005
O.0005
0.0005
0.0005
O.0005
0.0005
0.2
O.2
O.2
0.2
O.2
0.2
0.2
O.2
0.2
Post Run 7 CAD Cell MS
CAD0155EMM1
CAD01561MM1
CAD01564MM1
9/16/00
9/16/00
9/16/00
1:33
1:35
1:39
4.30
3.41
4.05
0.02
0.02
0.02
0.5
0.5
0.5
0.02
0.02
0.02
O.04
O.04
O.04
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.0005
0.0005
0.2
0.2
0.2
Note: Bold type indicates detected concentrations
26
-------
Table 3-18. RCRA 8 Metals Analytical Results for Run 8
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Pre Run 8 CAD Cell MS
CAD015ABMM1
CAD015BOMM1
CAD015B3MM1
9/20/00
9/20/00
9/20/00
9:43
9:50
9:53
4.25
4.30
2.06
<0.02
<0.02
O.02
0.5
0.5
O.5
0.02
0.02
O.02
O.04
0.04
O.04
0.02
0.02
O.02
0.02
0.02
O.02
0.0005
0.0005
O.0005
0.2
0.2
O.2
Run 8 CAD Cell MS
CAD015C2MM1
CAD015C5MM1
CAD015CBMM1
CAD015CEMM1
CAD015D1MM1
CAD015D4MM1
CAD015D7MM1
CAD015DCMM1
CAD015DFMM1
9/20/00
9/20/00
9/20/00
9/20/00
9/20/00
9/20/00
9/20/00
9/20/00
9/20/00
10:34
10:38
10:45
10:49
10:54
11:01
11:05
11:10
11:12
48.69
9.09
25.25
36.26
13.38
15.57
11.96
9.98
10.73
<0.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.5
0.5
0.5
O.5
0.5
O.5
O.5
0.5
O.5
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.04
O.04
O.04
O.04
0.04
O.04
O.04
0.041
0.054
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.02
0.02
0.02
O.02
0.02
O.02
O.02
0.02
O.02
O.0005
0.0005
0.0005
0.0013
0.0005
O.0005
O.0005
0.0005
O.0005
O.2
0.2
0.2
O.2
0.2
O.2
O.2
0.2
O.2
Post Run 8 CAD Cell MS
CAD015EFMM1
CAD015F2MM1
CAD015F5MM1
9/20/00
9/20/00
9/20/00
11:52
11:56
12:00
4.48
4.28
2.86
0.03
O.02
0.027
0.5
O.5
O.5
0.02
O.02
O.02
0.056
0.057
0.057
0.02
O.02
O.02
0.02
O.02
O.02
0.0005
O.0005
O.0005
0.2
O.2
O.2
Note: Bold type indicates detected concentrations
Table 3-19. Comparison of Filtered Samples
Sample ID
CAD012BF
CAD012C3
CAD01390
CAD01394
CAD0147D
CAD01480
CAD014D4
CAD014DB
CAD01534
Date
Collected
9/9/00
9/9/00
9/11/00
9/11/00
9/14/00
9/14/00
9/15/00
9/15/00
9/16/00
Time
Collected
16:59
17:03
1:13
1:16
4:52
5:00
9:52
9:57
0:09
TSS
(mg/L)
122.40
95.18
26.77
53.43
102.67
70.82
51.98
37.58
191.74
TPH (ng/L)
Filtrate
25.10
41.95
43.15
58.82
44.39
30.17
54.07
338.97
53.31
Particulate
154.26
687.28
14.93
142.32
21.52
45.60
41.87
51.05
34.70
Total PAH (ng/L)
Filtrate
178.73
432.07
98.56
59.97
67.91
117.44
62.86
61.87
44.73
Particulate
629.64
4,810.23
87.85
248.15
68.49
194.91
79.35
126.76
67.24
Total PCB (ng/L)
Filtrate
-------
concentrations higher in water, with the largest difference in sample CAD014DB where the filtrate TPH
concentration was 338.97 |o,g/L and the participate concentration was 51.05 |o,g/L. All but one sample had
a higher PCB concentration in the participate and four of the nine samples had filtrate total PCB
concentrations
-------
Table 3-21. RCRA 8 Metals Analytical Results for Post Survey
Sample ID
Date
Collected
Time
Collected
TSS
(mg/L)
Analytes (mg/L)
Arsenic
Barium
Cadmium
Chromium
Silver
Lead
Mercury
Selenium
Post Survey CAD CellM19
CAD01610MM1
CAD01613MM1
CAD01616MM1
CAD01619MM1
CAD0161CMM1
9/28/00
9/28/00
9/28/00
9/28/00
9/28/00
9:22
9:26
9:29
9:32
9:35
4.14
3.61
3.48
3.28
2.39
<0.02
O.02
0.02
<0.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.0005
O.0005
0.0005
O.0005
0.0005
0.031
O.02
0.059
O.02
0.17
Post Survey CAD Cell MS
CAD01620MM1
CAD01623MM1
CAD01626MM1
CAD01629MM1
CAD0162CMM1
9/28/00
9/28/00
9/28/00
9/28/00
9/28/00
9:38
9:41
9:44
9:47
9:50
3.18
2.17
2.46
3.81
1.58
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
O.02
0.02
0.02
O.02
0.02
0.15
0.02
0.0005
O.0005
0.0005
O.0005
0.0005
0.023
0.072
0.036
O.02
0.02
Note: Bold type indicates detected concentrations
3.9 Sand Capping Material
Sand used for capping in Boston Harbor was analyzed for PCB, PAH, and TPH in order to deter-
mine if the levels of organics detected in the water samples taken during the survey could be caused by
the material used for capping. The capping sand was collected from the Cape Cod Canal, which has been
determined by the USAGE to be free from contaminants and contains sand suitable for use in capping.
The sand samples were obtained from the USAGE and Great Lakes Dredging Company. Samples were
taken from five different loads in order to provide a good representation of the sand used throughout the
capping process, and were collected during the last three days of capping at Boston Harbor in order to
meet the holding times for organics. A TPH analysis was run for Load #24, but no duplicate was run for
PCBs. These cap samples were not analyzed for the RCRA 8 metals because of the time and budget con-
straints on the project. However, the very low concentration of RCRA 8 metals detected during capping
indicate that the capping material would not have noticeably contributed to contamination of the water
column.
All of the Cape Cod sand samples had low levels of organic contaminants (Table 3-22). PCBs
were
-------
PAHs were detected at low levels in all five sand samples and the duplicate for Load #24. PAH
concentrations ranged from 2.81 ng/g in Load #21 to 14.46 ng/g in Load #24. The detections of TPH and
PAH were so low in the sand samples that they were probably related to natural background from the
Cape Cod area.
3.10 Data Comparisons
Analytical results of water samples collected before, during, and after capping activities were
compared to quantify changes in contaminant concentrations in the water column caused by the capping
activities. Contaminant concentrations were plotted against turbidity levels to determine whether areas of
high turbidity (caused by capping) corresponded to areas of relatively high contamination. Two dimen-
sional (2-D) turbidity maps were generated to show TSS levels and COCs in the area where the capping
took place. A 2-D diagram of PAH and TSS concentrations for Run 1 is shown in Figure 3-7 and 2-D
plots for the remaining runs can be found in Appendix H. Figures 3-8 through 3-10 show plots for TPH,
PAH, and PCB concentrations plotted against TSS, respectively, for Runs 1 through 4. Figures 3-11
through 3-13 show plots for TPH, PAH, and PCB concentration plotted against TSS, respectively, for
Runs 5 through 8. Linear regression values and correlation coefficients for each plot are shown in
Table 3-23. All r2 values were below 0.5 except PAH vs. TSS for Run 3 (r2 = 0.957), PCBs vs. TSS for
Run 7 (r2 = 0.7696) and PCBs for Run 3 (r2 = 0.6611). However, PCBs vs. TSS for Run 2 had a negative
slope, suggesting that the r2 value of 0.7696 was an artifact of the data and does not suggest a predictable
trend. In general, the low r2 values indicate that TSS values are not good predictors of suspended contam-
inant concentrations during capping. This is because the resuspended, contaminated TSS likely are over-
shadowed by the TSS from the capping material.
Information from the ADCP was used to determine flow velocity and direction for Boston Harbor
and the Mystic River during all sampling events. The data gathered using the ADCP and BOSS shows
that the current velocity during sampling was very slow and the flow direction was variable. Table 3-24
gives the average velocity and direction for each day of sampling; the standard deviation is also listed.
Average current velocities were plotted for each day (Appendix I). The velocities and flow direction in
Table 3-24 and the plots in Appendix I are calculated at approximately 2 m above the river bottom, which
was the same depth that samples were taken using the BOSS. The ADCP gathers profiles of horizontal
currents for the entire water column by depth, but the velocities and flow directions for the entire water
column were more variable than for 2 m above the river bottom. The current velocities observed in the
Mystic River probably were not great enough to transport sediments resuspended by capping "down-
stream" from the CAD cells.
Data from Boston Harbor indicate that resuspension was greater when capping was conducted
over uncapped sediments, and that resuspended contaminants probably did not travel downstream with
the current. Suspended sediments settled rapidly (within an hour) after the capping activities ceased and
resuspension decreased as more capping material was placed over the contaminated sediments.
In general, high TSS concentrations did not correlate to high organic concentrations at cell Ml9,
where the average correlation coefficient was 0.3560. At cell M19, four water samples taken during Run
1 had both high TSS concentrations and relatively high organic concentrations; however, several water
samples also had high TPH levels and very low TSS concentrations. Cell M19 also had one sample in
Run 4 with a high PCB concentration (23.79 ng/L), but low TSS (7.54 mg/L).
Samples taken at cell M8 showed even lower correlation between TSS and organic
concentrations, where the average correlation coefficient was 0.2195. TSS levels and organic
concentrations at cell M8 were generally lower than at cell Ml9.
30
-------
42.387
42.386
42.385
42.384
Boston Harbor - PAH
CAD M19-Pre Run 1
9/9/2001 15:59 to 16:02 PM
-71.058
-71.056
-71.054
-71.052
-71.05
42.386
42.385
42.384
-71.048
Boston Harbor - PAH
CAD M19 - Run 1
9/9/2001 16:59 to 17:25 PM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05
65
60
55
50
45
40
35
30
25
20
15
10
5
42.387
42.386 '
42.385
42.384
CADM19
Boston Harbor-PAH
CAD M19-Post Run 1
SY92001 18:33 to 18:37 PM
TSS Concentration
(mg/L)
PAH Concentration
(ng/L)
-71.058
-71.056
-71.054
-71.052
-71.05
71.048
Figure 3-7. 2-D Plot of PAH and TSS Concentrations for Run 1 CAD Cell M19
31
-------
700
600
cnn
oUU
400
300
200
100
n
*
* *
A
*A A ^
if - JB 1
'<5"*?«*_
»Run 1
Run 2
A Run 3
Run 4
0 20 40 60 80 100 120 140
TSS (mg/L)
Figure 3-8. TPH Plotted Against TSS for Runs 1 Through 4
ouuu -
5000
B, 4000
< 3000
Q.
5 2000
H
1000
n
*
^ ^
41 f '"" "^ V
Run 1
Run 2
ARun 3
Run 4
50 100
TSS (mg/L)
150
Figure 3-9. PAHs Plotted Against TSS for Runs 1 Through 4
80
70-
60
50
40
30
20
10
n -
*
^ . A »
Run 1
Run 2
ARun 3
Run 4
0 20 40 60 80 100 120 140
TSS (mg/L)
Figure 3-10. PCBs Plotted Against TSS for Runs 1 Through 4
32
-------
400
350
300
250
200
150
100
50
m
* J M A
jfe»*^B * *
J^~ *
Run 5
Run 6
A Run 7
Run 8
0 50 100 150 200
TSS (mg/L)
Figure 3-11. TPH Plotted Against TSS for Runs 5 through 8
800
700
600
500
400
300
200
100
n
^
+
* *
ft 1 * * A
^^v
*Run 5
Run 6
ARun7
Run 8
0 50 100 150 200
TSS (mg/L)
Figure 3-12. PAHs Plotted Against TSS for Runs 5 Through 8
o
a.
14
12
10
8
6
4
2
n -
*
*
"
*
V*
jf ** A
1*^ __ ^
»Run 5
Run 6
ARun 7
Run 8
0 50 100 150 200
TSS (mg/L)
Figure 3-13. PCBs Plotted Against TSS for Runs 5 through 8
33
-------
Table 3-23. Correlation Coefficients and Linear Regression Values
for Runs 1 Through 8
Run No.
r2
Slope
Y-intercept
TPH (Figures 3-8 and 3-11)
Runl
Run 2
Run 3
Run 4
Run 5
Run 6
Run 7
Run 8
0.2833
0.4014
0.1187
0.2935
0.0149
0.1453
0.2636
0.036
2.7939
-2.515
-2.0799
1.1141
0.0958
2.5489
0.2138
-0.7716
17.164
120.36
195.42
20.789
62.218
33.554
49.512
65.959
PAHs (Figures 3-9 and 3-1 2)
Runl
Run 2
Run 3
Run 4
Run 5
Run 6
Run 7
Run8
0.2027
0.0361
0.9566
0.2211
0.2822
0.3862
0.0327
0.0015
16.329
1.9267
5.0897
1.239
3.5999
2.2221
0.1212
-0.1668
196.11
108.01
38.02
72.676
124.07
53.941
87.357
116.13
PCBs (Figures 3-10 and 3-13)
Runl
Run 2
Run 3
Run 4
Run 5
Run 6
Run 7
Run 8
0.1431
0.7696
0.6611
0.1848
0.3809
0.4446
0.0033
0.643
0.2228
-0.1354
0.105
-0.342
0.075
0.1605
-0.0011
-0.0694
3.7986
5.3594
0.9945
10.897
2.3864
-1.8065
2.089
3.7327
Table 3-24. Average Current Velocity and Flow Direction Approximately 2 m Above
the River Bottom
Date
9/6/00
9/9/00
9/10/00
9/11/00
9/12/00
9/13/00
9/14/00
9/15/00
9/16/00
9/20/00
Velocity (East)
mm/s
12.5
3.2
-3.2
-16.5
15.2
-2.7
-5.2
32.5
49.5
0.2
Standard Deviation
(East) mm/s
213
222
221
224
254
223
221
231
239
216
Velocity (North)
mm/s
20.2
-5.5
3.0
23.2
5.6
-11.9
-22.0
10.3
27.0
-3.0
Standard Deviation
(North) mm/s
211
220
218
225
247
232
216
222
255
219
34
-------
4.0 CONCLUSIONS
Background levels of TPH, PCBs, and PAHs were below detection limits or very low levels were
detected. The highest resuspension of contaminant material was seen during the first event at each CAD
cell when previously uncapped sediments were being capped. In general, contaminant resuspension was
very low for all capping events during this survey. Rapid dissipation of TSS and contaminants was seen
for all capping events.
Table 4-1 compares sampling results at Boston Harbor to results from the parallel study at Eagle
Harbor. These two sites used very different methods for capping contaminated settlements, but both sites
showed similar results from the monitoring during the capping events. The capping material at Eagle
Harbor was washed off of a barge with a high-pressure hose, compared to the "sprinkling" method used at
Boston Harbor. A complete description of the capping method used at Eagle Harbor can be found in
Battelle (2001).
The BOSS proved to be an effective instrument for the collection of water samples before,
during, and after capping. Samples and data collected using the BOSS helped to achieve a better
understanding of the amount of contaminants released into the surrounding water column as a result of a
capping event.
Table 4-1. Comparison of Results from Boston Harbor and Eagle Harbor
Monitoring
Event
Before Capping
During
Capping
After Capping
Boston Harbor
PCBs (ng/L)
-------
36
-------
5.0 REFERENCES
Battelle. 2000. Final Quality Assurance Project Plan, Evaluation of Sediment Agitation and Mixing into
the Surrounding Water Column from Capping Activities. QAPP I.D. No. 206-02-0. August 30.
Battelle. 2001. Draft Final Report for Evaluation of Sediment Agitation and Mixing into the
Surrounding Water Column from Capping Activities at the Wyckoff/Eagle Harbor Superfund
Site. November.
Fredette, T.J., P.E. Jackson, C.J. Demos, D.A. Hadden, S.H. Wolf, T.A. Nowak Jr., and E. DeAngelo.
2000. The Boston Harbor Navigation Improvement Project CAD Cells: Recommendations for
Future Projects Based on Field Experience and Monitoring. Draft paper submitted to the June
2000 Western Dredging Association Conference, Warwick, RI.
United States Army Corps of Engineers (USAGE) 1999a. Chemistry Data Report - Boston Harbor
Navigation and Berth Dredging, Boston Harbor. August 5.
United States Army Corps of Engineers (USAGE). 1999b. Water Quality Certification - Compliance
with Condition E2, Boston Harbor Navigation and Berth Dredging Project - Phase 2 Letter
Report. December 28.
37
-------
v°/EPA
United States
PRESORTED STANDARD
POSTAGE & FEES PAID
EPA
PERMIT No. G-35
Environmental Protection
Agency
Office of Research and Development
National Risk Management
Research Laboratory
Cincinnati, OH 45268
Official Business
Penalty for Private Use
$300
EPA/540/R-05/014
July 2004
www.epa.gov
Recycled/Recyclable
Printed with vegetable-based ink on
paper that contains a minimum of
50% post-consumer fiber content
processed chlorine free
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX A
BOSTON HARBOR PLUME TRACKING SURVEY REPORT
-------
CAD 01 - BOSTON HARBOR, MA
BOSTON HARBOR PLUME TRACKING SURVEY REPORT
FOR
EVALUATION OF SEDIMENT AGITATION AND MIXING INTO THE
SURROUNDING WATER COLUMN FROM CAPPING ACTIVITIES
EPA Boston Harbor Resuspension Plume Monitoring Project
Contract No. 68-C7-0008
Work Assignment No. 26
Submitted to
U.S. ENVIRONMENTAL PROTECTION AGENCY
National Risk Management Research Laboratory
26 West Martin Luther King Drive
Cincinnati, OH 45268
Prepared by
Wayne Trulli
CarlAlbro
Submitted by
Battelle Duxbury Operations
397 Washington Street
Duxbury, MA 02332
(781) 934-0571
June 15,2001
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Boston Harbor Plume Tracking Survey Report June 15, 2001
TABLE OF CONTENTS
1. INTRODUCTION , 2
2. METHODS 5
2.1. DEVIATIONS 8
3. SURVEY CHRONOLOGY 9
4. SURVEY RESULTS 21
5. PROBLEMS EXPERIENCED, ACTIONS TAKEN, AND RECOMMENDATIONS 22
5.1. SCHEDULE 22
5.2. TECHNICAL 22
6. REFERENCES 23
LIST OF TABLES
TABLE 1. SURVEY PERSONNEL FOR EAGLE HARBOR PLUME TRACKING SURVEY, 2000 4
TABLE 2. SUMMARY OF FIELD MEASUREMENTS AND INSTRUMENTS 6
TABLE 3. ANALYTE, SAMPLE METHOD, VOLUME, PRESERVATION, AND HOLDING TIMES 8
TABLE 4. NUMBERS AND TYPES TRANSECTS TO BE OCCUPIED AND SAMPLES TO BE COLLECTED
DURING THE CAPPING RESUSPENSION SURVEY IN EAGLE HARBOR, WA 22
LIST OF FIGURES
FIGURE 1. EAGLE HARBOR MAP 3
APPENDICES
APPENDIX A 24
APPENDIX B 34
APPENDIX C 59
C:\Projects\Boston Harbor\Survey ReporftDraftl Survey Report CAD-01 .doc
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Boston Harbor Plume Tracking Survey Report June 15, 2001
1. Introduction
The U.S. Environmental Protection Agency's (U.S. EPA's) National Risk Management
Research Laboratory (NRMRL) wanted to determine whether the placement of a marine
sediment-cap results in the release of contaminants both into the surrounding water
column and onto surrounding sediments. The goal of this study was to achieve a better
understanding of the amount of contaminants released into the surrounding water column
before, during, and after capping. This study utilized state-of-the-art oceanographic
technology to acquire high-resolution field data for determining the extent of the release
of any contaminated sediment into the water column attributable to sediment agitation
during capping activities of a confined aquatic disposal (CAD) cell in Boston Harbor,
MA.
CAD cells in Boston Harbor have been used as disposal sites for silty, fine-grained
sediments from the Boston Harbor Navigation Improvement Project (BHNIP) that were
determined to be unsuitable for ocean disposal. Two of the CAD cells, located in the
Mystic River portion of Boston Harbor, were filled with dredged material in January 2000.
The dredged material in these two cells, M8 and M19 (Figure 1), has been allowed to
consolidate in order to reduce the amount of mixing between the dredged silt and cap sand
during capping of the cell. Sand dredged from the Cape Cod Canal was used to create
caps for cells M8 and M19 in Mystic River/Boston Harbor (Fredette et al, 2000). The
sand cap was "sprinkled" on the cells using a partially opened hopper dredge, which was
maneuvered using a tug down the length of the CAD cell. This "sprinkling" method of
cap creation minimizes the disturbance of the silt material in the disposal cells.
CAD cells M19 and M8 (Figure 1) were monitored during capping operations. The
objective of the study was to determine whether or not capping affects resuspension of
the contaminated sediments and adversely impacts the water column and surrounding
environment. To accomplish this objective Battelle conducted a plume tracking survey to
monitor the plumes at each of the two targeted Boston Harbor CAD sites.
This plume tracking survey at CAD Sites M19 and M8 was conducted from September 6
through 28, 2000. The survey involved tracking and sampling the plumes of sediment
generated by the capping activities. The Battelle-owned research vessel R/V
Aquamonitor served as the monitoring platform. Mobilization was conducted on
September 4 and 5, and final demobilization was conducted on September 28, while the
vessel was docked at Hewitts Cove Marina in Hingham, MA. The survey crew is listed
in Table 1. The planned numbers of events and samples to be collected are in Table 2.
This survey report describes the daily activities of survey CAD 01, and provides a
synopsis of some preliminary observations from the survey. A description of the survey
methods is provided in Section 2. A chronological summary of survey activities and
observations is provided in Section 3. Preliminary survey results are provided in Section
4. A description of survey problems and corrective actions, and recommendations for
future surveys can be found in Section 5.
C:\Projects\Boston HarboASurvey Report\Draftl Survey Report CAD-01 .doc
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
Figure 1. Boston Harbor Navigation Improvement Project
Mystic River and Inner Confluence Disposal Cells (Fredette et al., 2000)
Confluent e DJ*p«i4l Celt
Sources:
MdisGISiMIT Digtdl OrthopholOJ,
Produced by E NSR, 309100
400 0 400 800 Feet
C:\Projects\Boston Harbor\Survey ReportXDraftl Survey Report CAD-01.doc
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
Table -1. Survey Personnel for Boston Harbor,
2000. (Team 1: black,
MA, Plume Tracking Survey, September
Team 2: blue).
Activity:
Date:
Chief Scientist
NAVSAM Operator
Pi/Winch Operator
DPM/Sarapling
Technician
ADCP Operator
Captain (Subcontractor)
EPA Work Assignment
Manager
At-Sea Totals
Activity
Date
Chief Scientist
NAVSAM Operator
Pi/Winch Operator
DPM/Sampling
Technician
ADCP Operator
Captain (Subcontractor)
Work Assignment
Manager (EPA)
At-Sea Totals
Mobilization
9/4
B. Mandeville
T. Kaufman
L. Gildav
M. Mannis
S. Curtis
N/A
Pre-Capping
Background
Sampling
9/5
W. Trulli
C.Albro
B. Mandeville
S. Libbv
T. Kaufman
L. Gildav
L. Cumming
J. Ickes
L. Short
S. Curtis
B. Ryder
E. Chiasson
5
5
Daily Sampling at CAD M19
9/9
W. Trulli
B. Mandeville
T. Kaufman
L. Cumming
L. Short
B. Ryder
T. Lyons
6
N/A
9/10
C.Albro
S. Libbv
L. Gildav
J. Ickes
S. Curtis
E. Chiasson
T. Lyons
N/A
6
9/11*
W. Trulli
C.Albro
B. Mandeville
S. Libby
T. Kaufman
L. Gilday
L. Cumming
J. Ickes
L. Short
S. Curtis
B. Ryder
E. Chiasson
T. Lyons
T. Lyons
6
6
9/12**
W. Trulli
C.Albro
B. Mandeville
S. Libbv
T. Kaufman
L. Gildav
L. Cumming
J. Ickes
L. Short
S. Curtis
B. Ryder
E. Chiasson
T. Lyons
6
6
9/13
W. Trulli
B. Mandeville
T. Kaufman
L. Short
B. Ryder
T. Lyons
6
N/A
Daily Sampling at CAD M8
9/14
C.Albro
S. Libby
L. Gildav
J. Ickes
S. Curtis
E. Chiasson
T. Lyons
N/A
6
9/15
W. Trulli
B. Mandeville
T. Kaufman
J. Boyle
B. Ryder
6
N/A
9/16
W. Trulli
B. Mandeville
T. Kaufman
L. Short
B. Ryder
5
N/A
9/20
W. Trulli
B. Mandeville
T. Kaufman
L. Short
B. Ryder
5
N/A
9/28
S. Libbv
B. Mandeville
L. Gildav
S. Curtis
E. Chiasson
N/A
5
Table 1. Planned Numbers and Types Transects and Samples to be Collected
during the Capping Resuspension Survey in Boston Harbor MA.
Type of
Event
Precapping
Capping
Postcapping
Number of
Events in ,
Survey
1
8
1
Numbers and Types of
Transects per Event
1 standard transect
1 pre-dump background
transect
1 standard transect
1 post-dump background
transect
1 standard transect
Numbers and Types of
Samples per Event
Organics
5
3
9
3
5
Metals
5
3
9
3
5
TSS
5
3
9
3
5
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01.doc
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Boston Harbor Plume Tracking Survey Report June 15, 2001
2. Methods
The following subsections briefly summarize the methods used during this survey. The
Quality Assurance Project Plan (QAPP) (Battelle 2000) for the Evaluation of Sediment
Agitation and Mixing into the Surrounding Water Column from Capping Activities
contains additional details on survey sampling methods.
Method Descriptions:
Navigation. Vessel positioning during sampling operations was accomplished with the
BOSS navigation system. This system consists of a Northstar Differential Global
Positioning System (DGPS) interfaced to the NAVSAM computer and software. The
global positioning system (GPS) receiver has six dedicated channels and is capable of
locking onto six different satellites at one time. To correct the GPS calculations, the
Northstar DGPS received correction data from one of three United States Coast Guard
DGPS broadcast sites: Montauk Point, NY, Chatham, MA, or Portsmouth Harbor, NH.
This capability ensured strong signal reception, and accurate and reliable positioning with
2-second updates.
A calibration check of the GPS navigation system vs. known benchmarks was conducted
twice daily to verify that the system was working properly. The checks were conducted
prior to departing in the morning and following arrival at the dock in the evening.
Battelle Ocean Sampling System. Monitoring of the capping event was conducted using
the Battelle Ocean Sampling System (BOSS) deployed from the R/V Aquamonitor. The
BOSS in situ sensor package included a conductivity, temperature and, depth (CTD)
sensor (OS200 CTD), a turbidity sensor, and a Teflon/titanium pumping system for
sample collection. A second turbidity sensor, calibrated to the in situ data, was located at
the water-sampling manifold so that the appropriate parcel of water could be identified
and sampled at the appropriate time. Additionally, an Acoustic Doppler Current Profiler
(ADCP) was deployed for obtaining vertical profiles of horizontal currents. Table 2 lists
the field measurements acquired from the survey vessel during each monitoring event.
The entire pumping system, including suction strainers, pump, and Teflon tubing up to
but not including the on-deck transmissometer, was decontaminated with
dichloromethane (DCM) and acetone, followed by deionized water rinse. The
transmissometer could not be cleaned using this procedure because the solvents would
melt the plastic components of the unit. Decontamination was conducted during each
dumping event prior to initiating sampling operations.
Field measurements and instruments are listed in Table 3.
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01.doc
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
Table 3. Summary of Field Measurements and Instruments.
Parameter
Conductivity
Temperature
Pressure
Transmissometry/Turbidity
Bottom depth
Navigational position
Ocean current velocity
Lab
Battelle
Battelle
Battelle
Battelle
Battelle
Battelle
WHOI
Units
Mmhos/cm
°C
m
m-1
m
Degrees
Cm/sec
Instrument
OS200 CTD
OS200 CTD
OS200CTD
Seatech 20-cm (660nm) (2)
Furuno FCV-52
Northstar 942X
RD Instruments ADCP WHM600-I-UG6
Plume Tracking and Sampling. BOSS sensor data were collected continuously along
transects within each CAD cell (Figure 2). The configuration of the transect and the
sampling locations along each transect varied according to the capping activity (e.g., pre-
capping, capping, post-capping activities). During the transects, BOSS was towed at a
distance of ~2 m above the bottom along all transects (unless obstructed) to ensure that
sensors detected resuspended sediments (if detectable).
CAD (-80 m x -240 m)
Sta
rlA-
-±~>
End
Current
Daily Pre/ Post Dump
Background Transect
Trackline during pre-dump
and 1 hour after dump
End -^
Start
''^>*;CJ^;4 \>.?\
/i3fes
fr" C
.*i'« 4
^<«i! '*4
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Boston Harbor Plume Tracking Survey Report June 15, 2001
Three sample sets were collected immediately prior to each capping event, nine sample
sets were collected during each capping event, and, with one exception during Event 3 at
cell M19), three sets were collected immediately following each capping event. Each
sample set consisted of three water samples: one sample for organic-constituents analysis,
one sample for trace metals analysis, and one sample for total suspended solids (TSS)
analysis. Water sample sets were shipped to the analytical laboratories for analysis
immediately following the survey.
The station/sample location number, GPS coordinates, date and time, depth of the water
column, and any observations associated with the sampling at each sampling location
were made in the field survey logbook. Each sample was assigned a unique ID and label
by NAVSAM, which also electronically stores the field and sensor data. Exceptions are
noted in Section 5.
BOSS sensor data were collected continuously during transit through the site, pre- and
post-capping sampling activities, and along all transects between water-sampling
locations within the capping area during capping operations. [The plots are not included
in this survey report but will be reported in the final interpretive report.] The BOSS was
towed at a distance of approximately 2 m or less above the bottom along all transects
(unless obstructed) to ensure that sensors were deep enough to detect (if detectable) the
resuspended sediments, and the sampling intake was in the best place to sample for those
sediments.
Sample Shipping and Custody. Each day, samples were stored shipboard in coolers
containing ice, and returned to the Battelle Duxbury Laboratory following each sampling
event. Samples were stored in a walk-in chill room until analysis, or until shipment to
the analytical laboratories targeted to analyze TSS and trace metal samples. Before
shipping, the ice was replenished in each cooler, and the sample custody forms were
completed, placed in a sealed Ziploc bag which was taped to the inside of the cooler lid.
A cooler blank was included in the shipment. The laboratory sample custodian was
notified of the impending shipment on the day that the samples were shipped so that they
were alerted to expect the samples on the following day. Sample custodians were as
shown below.
Organlcs Analysis TSS Analysis Metals Analysis
Mr. Patrick Barrett Ms. Laura Reed Mr. Kevin Murray
Battelle Duxbury University of Rhode Island (URI) Alpha Analytical, Inc.
397 Washington Street Graduate School of Oceanography 255 Glendale Avenue, Suite 21
Duxbury, MA 02332 Narragansett, RI02882-1197 Sparks, Nevada 89431-5778
781-934-5400 (main) (401) 874-6657 (office) (775) 355-1044 (office)
781-952-5282 (direct) (401) 874-6651 (lab) (775) 355-0406 (FAX)
Sample Storage Conditions. Sample storage conditions are presented in Table 4.
C:\Projects\Boston Harbor\Survey ReportNDraftl Survey Report CAD-01 .doc 7
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
2.1. Deviations
Additional Work at CAD Cell M8. Under the original plan, only one of the two
uncapped CAD cells, the larger-area M19, was selected for monitoring during capping
activities. However, because Battelle was able to monitor only four dumping events at
M19, U.S. EPA and Battelle management jointly decided to monitor four consecutive
dumping events at cell M8. This activity provided additional valuable information on
resuspension of CAD sediments and contaminant concentrations at the site, and also
provided verification that sediments at cell M8 behaved similarly to those at cell M19
during capping. Sampling operations at cell M8 were conducted in pattern similar to the
pattern shown in Figure 2 and followed during the sampling at cell M19.
Table 4. Analyte, Sampling Method, Volume, Preservation, and Holding Times.
Analyte (Analytical
Laboratory)01'
Matrix
Method
Sample
Volume
Container Type
- . - -- ' . - '
Preservation
Holding
Time
Laboratory Analyses
TPH (EDO)
PCB (EDO)
PAH (EDO)
TSS (URI)
Metals (AAI)
Water
Water
Water
Water
Water
Battelle SOP
5-202-04
Battelle SOP
5-128
Battelle SOP
5-157
Battelle SOP
5-053
l.OOOmL
1,000 mL(b)
l,OOOmL(b)
500 mL
lOOOmL
Amber glass with
Teflon-lined cap
Amber glass with
Teflon-lined cap
Amber glass with
Teflon-lined cap
Poly ethylene plastic
Polyethylene plastic
Cool, 4°C±2°C
Cool, 4°C±2°C
Cool, 4°C±2°C
Cool, 4°C±2°C,
Dark
Cool, 4°C±2°C,
Dark
14 days
7 days/
40 days(c)
7 days/
40 days(c)
7 days
28 days
Field Analyses
Temperature (EDO)
Depth (EDO)
Transmissometry/
Turbidity (EDO)
Conductivity (EDO)
Water
Water
Water
Water
OS200 CTD
OS200 CTD
Seatech 20-cm
(660nm)
OS200 CTD
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
In situ
In situ
In situ
In situ
(a) EDO: Battelle Duxbury Operations; URI: University of Rhode Island; AAl:.Alpha Analytical, Inc.
(b) Sample for TPH also extracted for PAH analysis.
(c) Extractions must be complete within 7 days, and gas chromatography/mass spectrometry (GC/MS) analysis must be
complete within 40 days.
GC/MS = gas chromatography/mass spectrometry.
NA = Not applicable.
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
3. Survey Chronology
Note: All times are recorded as Eastern (Daylight Savings) Time.
Monday, September 4, 2000
0800 Loaded all equipment and supplies aboard the vessel R/V Aquamonitor.
Prepared water-column sampling-system for towing.
Tuesday, September 5,2000
0800 Continued mobilization activities. Ms. Jennifer Ickes and Ms.Lydia Gumming
arrive from Battelle Columbus.
Wednesday, September 6,2000
1100 Departed Hewitts Cove Marina (HCM) to CAD cell M8. Conducted training
exercises with staff from Sampling Team 2.
1223 Initiated collection of precapping reference samples at CAD cell M8.
Collected pre-capping reference sample at Station Bl.
1225 I Collected pre-capping reference sample at Station B2.
1226 Collected pre-capping reference sample at Station B3.
1227 Collected pre-capping reference sample at Station PI.
1232 Collected pre-capping reference sample at Station P2. Completed Collection
I of five pre-capping reference samples at CAD cell M8. Returned to HCM to
I pick up Sampling Team 1 for training.
1300 Switched sampling teams and returned to CAD cell Ml9 to conduct training
exercises and collect reference samples at CAD cell Ml9.
1413 Initiated collection of pre-capping reference samples at CAD cell M-19.
Collected pre-capping reference sample at Station B1.
1415 Collected pre-capping reference sample at Station B21.
1419 Collected pre-capping reference sample at Station B3.
"1422 I Collected pre-capping reference sample at Station PI.
I I
I 1424 Collected pre-capping reference sample at Station P2. Completed collection
| of pre-capping reference samples at CAD cell Ml9. Returned to HCM.
Saturday^_Sjeptember_9,__20pjD
1300 | Conducted navigation calibration. Meet with Sampling Team 1 to discuss the
| daily sampling strategy.
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
1320 I Departed HCM to Collected background samples at M19 before hopper
| dredge arrived at the site and began initial dump of capping material. In route,
| sampling team was notified that the dredge arrival on site will be
I approximately 1615. Aquamonitor proceeded to Pier 1 in East Boston.
1410 I Arrive Pier 1 dock; pick up Ms. Ickes and Ms. Gumming of Battelle-
| Columbus and Mr. Lyons of U.S. EPA.
1512 | Transited to cell M19 for sampling of Event 1.
1550 [ On site. Cleaned pumping system and calibrated pump.
1559 I Initiate monitoring/sampling activities along pre-dump transect. Collected
Event 1 pre-dump water samples for organics, metals, and TSS at Station Bl.
1601 Collected Event 1 pre-dump water samples for organics, metals, and TSS at
Station B2.
1603 | Collected Event 1 pre-dump water samples for organics, metals, and TSS at
| Station B3.
i
1650 | Hopper dredge Manhatten Island initiates capping operations (dumping). \
j.. _. __ .._ _ _ _ _ _ __ i
1700 | Collected Event I/Sample Set IF water samples for organics, metals, and TSS
| along Standard Transect at M19.
1704 Collected Event I/Sample Set 2H water samples for organics, metals, and TSS
along Standard Transect at M19.
1705 i Collected Event I/Sample Set 3F water samples for organics, metals, and TSS i
| along Standard Transect at M19. j
1708 j Collected Event I/Sample Set 4F water samples for organics, metals, and TSS
along Standard Transect at M19.
ni6 Collected Event I/Sample Set 5H water samples for organics, metals, and TSS
along Standard Transect at M19.
1713 | Collected Event I/Sample Set 6H water samples for organics, metals, and TSS |
| along Standard Transect at M19. I
1717 I Collected Event I/Sample Set 7F water samples for organics, metals, and TSS |
along Standard Transect at Ml9.
1723 Collected Event I/Sample Set 8H water samples for organics, metals, and TSS
along Standard Transect at M19. Pumping system hit bottom, and Chief
Scientist noted a reduction in the pumping rate.
1726" | Collected Event F/Sampie Set 9F water samples for organics, metals, and TSS
| along Standard Transect at M19. Dredge departs site.
1834 Collected Event 1 post-dump water samples for organics, metals, and TSS at
Station PI.
10
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
1837 | Collected Event 1 post-dump water samples for organics, metals, and TSS at
I Station P3.
1843 Collected Event 1 post-dump water samples for organics, metals, and TSS at
I Station P2.
1840
1910
Aquamonitor departed survey area.
Droped off Ms. Gumming, Ms. Ickes, and Mr. Lyons at Pier 1 in East Boston.
2010 ! Arrive HCM.
Sunday, SeptemberlO, 2000
0529 \ Performed navigation calibration.
0534 | Aquamonitor departed HCM.
0630 I Arrived Pier 1, East Boston, to pick up Battelle and U.S. EPA staff.
0700 | Arrive on site at cell Ml9. Clean pumping system. Check and record flow
| rate of pumping system. Container ship entering port delayed capping and
| sampling operations.
0720 Initiated monitoring/sampling activities along pre-dump reference transect.
Collected Event 2 pre-dump water samples for organics, metals, and TSS at
Station Bl.
0723 | Collected Event 2 pre-dump water samples for organics, metals, and TSS at
Station B3.
0729
0802
Collected Event 2 pre-dump water samples for organics, metals, and TSS at
Station B2.
Dredge Manhatten Island on site.
0835 | Dredge began dumping at cell M19.
0851 | Collected Event 2/Sample Set IF water samples for organics, metals, and TSS
1 along Standard Transect at M19.
0855 I Collected Event 2/Sample Set 2H water samples for organics, metals, and TSS
j along Standard Transect at Ml9.
0858 | Collected Event 2/Sample Set 3F water samples for organics, metals, and TSS
I along Standard Transect at M19.
0903
0917
Dredge completed dumping at Ml9.
Collected Event 2/Sample Set 4F water samples for organics, metals, and TSS
| along Standard Transect at M19.
0913 | Collected Event 2/Sample Set 5H water samples for organics, metals, and TSS
along Standard Transect at Ml9.
0926
Collected Event 2/Sample Set 6H water samples for organics, metals, and TSS
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
along Standard Transect at Ml9.
0928 | Collected Event 2/Sample Set 7F water samples for organics, metals, and TSS
| along Standard Transect at M19.
0934 | Collected Event 2/Sample Set 8H water samples for organics, metals, and TSS
I along Standard Transect at M19.
0941 | Collected Event 2/Sample Set 9F water samples for organics, metals, and TSS
| along Standard Transect at M19. Dredge departs site.
1015 I Collected Event 2 post-dump water samples for organics, metals, and TSS at
I Station PL
1017
1020
1025
Collected Event 2 post-dump water samples for organics, metals, and TSS at
Station P2.
Collected Event 2 post-dump water samples for organics, metals, and TSS at
Station P3.
Aquamonitor departs survey area for Pier 1 to drop off L. Gumming, J. Ickes,
and T. Lyons
1145 Arrived HCM. Repairs made to the pumping system. Sampling Team 1
| departed.
2030
_____
Sampling Team 2 arrived.
Aquamonitor departed HCM and transited to Pier 1 to pick up additional crew.
2230 Arrive on site at Ml9. Sampling system cleaned and calibrated.
2300 | System flow calibration completed.
2316 Collected Event 3 pre-dump water samples for organics, metals and TSS at
Station Bl.
2319
Collected Event 3 pre-dump water samples for organics, metals and TSS at
Station B2.
2322 I Collected Event 3 pre-dump water samples for organics, metals and TSS at
I Station B3.
2324 | Pumping system turned off.
Monday, September 11, 2000
0001 I Manhattan Island approached survey area. Personnel transferred from the tug
0052
0114
Pumping system turned
Collected Event 3/Samp
along Standard Transect
0115 | Dredge began dumping in other direction.
12
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
0116: Collected Event 3/Sample Set 2H water samples for organics, metals, and TSS
| along Standard Transect at M19.
0119 Collected" Event 3/Sampie Set 3F water samples for organics, metals, and TSS
along Standard Transect at M19.
0121 Collected Event 3/Sample Set 4F water samples for organics, metals, and TSS [
along Standard Transect at M19. |
0126 Collected Event 3/Sample Set 5H water samples for organics, metals, and TSS |
along Standard Transect at M19. I
0130 | Collected Event 3/Sample Set 6H water samples for organics, metals, and TSS |
I along Standard Transect at M19.
0133 | Collected Event 3/Sample Set 7F water samples for organics, metals, and TSS
| along Standard Transect at Ml9.
0135 | Barge completed dumping and departs.
0140 1 Collected Event 3/Sample Set 8H water samples for organics, metals, and TSS
I along Standard Transect at M19.
0141 | Collected Event 3/Sample Set 9F water samples for organics, metals, and TSS
| along Standard Transect at Ml9.
0145 | Began "Figure 8" towing.
0225 I Collected Event 3 post-dump water samples for organics, metals and TSS at
I Station PI, approximately 1 hour after dumping stopped. Sampler struck the |
| bottom immediately following PI sampling, and system components fouled j
I with mud. Extent of repairs/cleaning deemed too time consuming to remain
I on station. P2 and P3 samplings canceled. Repairs initiated. Transited to
t Pier 1
0252 I L. Cummings departed at Pier 1.
0430 I Arrived HCM. Sampling team departs.
1300 t Sampling Team arrived at jj^M.
1335 | Aquamonitor departs JJQM Pumping system flow rate was unacceptable
I i during transit to cell M19. Repairs initiated during transit to and at the
samping site while awaiting the dredge.
Manhattan Island arrived.
Dredge began dumping (Event 4).
Dumping completed and dredge departed site.
1647
Pumping system problems persisted. Event 4 Sampling suspended until the
problem is corrected. Aquamonitor returned to HCM.
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
Tuesday, September 12, 2000
I | Event 5 sampling was canceled.
I 2005 I Depart HCM for Event 6 sampling.
2135 I Collected Event 6 pre-dump water samples for organics, metals and TSS at
1 Station Bl.
2137 | Collected Event 6 pre-dump water samples for organics, metals and TSS at
I Station B2.
| 2139 | Collected Event 6 pre-dump water samples for organics, metals and TSS at
i Station B3.
2150
_____
________
2217
2220
2225
Manhattan Island arrives on site.
Dredge began dumping.
Collected Event 6/Sample Set IF water samples for organics, metals, and TSS
along Standard Transect at Ml 9.
Collected Event 6/Sample Set 2H water samples for organics, metals, and TSS
along Standard Transect at M19.
Collected Event 6/Sample Set 3F water samples for organics, metals, and TSS
along Standard Transect at Ml9. In sand.
2230
Collected Event 6/Sample Set 4F water samples for organics, metals, and TSS
along Standard Transect at M19.
Collected Event 6/Sample Set 5H water samples for organics, metals, and TSS
along Standard Transect at M19.
- 4
| 2231 | Dumping completed. Manhattan Island departs.
2236 | Collected Event 6/Sample Set 6H water samples for organics, metals, and TSS |
I along Standard Transect at M19. I
2237 | Collected Event 6/Sample Set 7F water samples for organics, metals, and TSS )
along Standard Transect at M19.
2245
2247
Collected Event 6/Sample Set 8H water samples for organics, metals, and TSS
along Standard Transect at Ml9.
2332
Collected Event 6/Sample Set 9F water samples for organics, metals, and TSS
along Standard Transect at M19.
Collected Event 6 post-dump water samples for organics, metals and TSS at
Station PI.
I 2334 I Collected Event 6 post-dump water samples for organics, metals and TSS at
! I Station P2.
2336 I Collected Event 6 post-dump water samples for organics, metals and TSS at
I Station P3.
14
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Boston Harbor Plume Tracking Survey Report
June 15,2001
Wednesday, September 13, 2000 _ _ _ _ _ _ _
1135 I Aquamonitor departs HCM. Sampling pump not working properly. Repairs
| initiated during transit to Pier 1.
1229 | Picked up Ms. Ickes at Peir 1 and departed for Ml9. Pump repairs ongoing
I during transit to Ml9 and while awaiting the dredge.
1400 \ Dumping began (Event 7). Pump repairs continued.
1430 | Pump repaired. Dumping completed. Initiated Figure 8-pattern sampling for
I turbidity measurements. Began Figure 8 at a point 200 m downcurrent and
| 2m above the bottom. Sampled in Figure 8 in the site at 2, 4, and 6 m above
| the bottom.
1500 | Figure 8 sampling completed. Tubidity mostly >3%. Depart for HCM
"""1615 1 ArriveHCMi
Thursday, September 14, 2000
| 0145 ! " " " " " " " " " '
6333 Arrived CAD cell M8. Collected Event 8 pre-dump water samples for
organics, metals and TSS at Station Bl.
0335 Collected Event 8 pre-dump water samples for organics, metals and TSS at
[ Station B2.
0338 | Collected Event 8 pre-dump water samples for organics, metals and TSS at
| Station B3.
0430 Manhattan Island arrived on site.
0448 Begin dumping.
| 0453 Collected Event 8/Sample Set IF water samples for organics, metals, and TSS
1 along Standard Transect at M8.
I _ _... _. _ _ _ _ _ ..._
0501 Collected Event 8/Sample Set 2H water samples for organics, metals, and TSS
along Standard Transect at M8.
0505 Collected Event 8/Sample Set 3F water samples for organics, metals, and TSS
along Standard Transect at M8.
0510 I Completed dumping. Manhattan Island remainedon site.
0513 I Collected Event 8/Sample Set 4F water samples for organics, metals, and TSS
along Standard Transect at M8.
0518 Collected Event 8/Sample Set 5H water samples for organics, metals, and TSS
along Standard Transect at M8.
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
0525 j Collected Event 8/Sample Set 6H water samples for organics, metals, and TSS |
along Standard Transect at M8. [
I
0530 \ Manhattan Island departs. I
0532 i Collected Event 8/Sample Set 7F water samples for organics, metals, and TSS |
I along Standard Transect at M8. Out of cell and downcurrent. j
0534 Collected Event 8/Sample Set 8H water samples for organics, metals, and TSS I
along Standard Transect at M8. I
0540 1 Collected Event 8/Sample Set 9F water samples for organics, metals, and TSS
I along Standard Transect at M8.
j. _ j _
I 0611 | Collected Event 8 post-dump water samples for organics, metals and TSS at
| | Station PI.
| 0613 I Collected Event 8 post-dump water samples for organics, metals and TSS at
| | Station P2.
I 0616 I Collected Event 8 post-dump water samples for organics, metals and TSS at
[ Station P3.
Friday, September 15, 2000
\ 0630 1 Crew arrived at HCM. """" "
0800 On site! " ~~ ~~ " " ~ ~ " ~ ~ " " " ~ [
0815 Cleaned system. I
0832 Pre-dump cross calibration with ADCP completed.
6840 Advised by B. Cuzzelli that the dump site is cell M8.
0846 Collected Event 9 pre-dump water samples for organics, metals and TSS at
Station Bl.
6848 Collected Event 9 pre-dump water samples for organics, metals and TSS at
Station B2.
| 0851 Collected Event 9'pre-dump water samples for organics, metals and TSS at
I Station B3.
0915 Manhattan Island arrived in the study area. Dredge advised W. Trulli
(Battelle Chief Scientist) to cease and desist further communication with the
| dredge (reasons unknown to Aquamonitor crew. Sampled area west to east.
0941 Dredge began dumping.
| 0949 Encountered sand approximately 50 m short of the site.
16
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
"V"
f.i
0952 I Collected Event 9/Sample Set IF water samples for organics, metals, and TSS
along Standard Transect at M8.
0956 | Dumping completed.
0957 | Collected Event 9/Sample Set 2H water samples for organics, metals, and TSS
along Standard Transect at M8.
1000
1003
Collected Event 9/Sample Set 3F water samples for organics, metals, and TSS
along Standard Transect at M8.
Collected Event 9/Sample Set 4F water samples for organics, metals, and TSS
along Standard Transect at M8. Manhattan Island departs survey area.
1006 | Collected Event 9/Sample Set 5H water samples for organics, metals, and TSS j
along Standard Transect at M8. |
1011 | Collected Event 9/Sample Set 6H water samples for organics, metals, and TSS \
| along Standard Transect at M8.
I6I4 | Collected Event 9/Sample Set 7F water samples for organics, metals, and TSS
I along Standard Transect at M8.
1023 I Collected Event 9/Sample Set 8H water samples for organics, metals, and TSS
along Standard Transect at M8.
1026
Collected Event 9/Sample Set 9F water samples for organics, metals, and TSS
along Standard Transect at M8.
1040 | Running Figure 8 tracks for turbidity measurements at 2, 4, and 6 m.
Turbidity between 3 and 15%.
1101
Sampler hit bottom. Scoop mud going into Station PI. System re-cleaned.
1136 | Collected Event 9 post-dump water samples for organics, metals and TSS at
| Station PL Muddy sediments in organics sample. Cleaned with DCM and
| Milli-Q water, recalibrated.
1149 | Collected Event 9 post-dump water samples for organics, metals and TSS at
I Station P2.
1151 | Collected Event 9 post-dump water samples for organics, metals and TSS at
I Station P3.
1154 I Depart site to return to HCM after pulling ADCP. Pumping system checked
1300
_____
Arrive HCM. Continued equipment maintenance.
Depart HCM for M8.
2335 Collected Event 10 pre-dump water samples for organics, metals and TSS at
Station Bl.
2338 Collected Event 10 pre-dump water samples for organics, metals and TSS at
Station B2.
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Boston Harbor Plume Tracking Survey Report
June 15,2001
2342 I Collected Event 10 pre-dump water samples for organics, metals and TSS at
I Station B3.
2355 I Manhattan Island arrives at M8.
0001 I Dumping began.
0009I
Collected Event 10/Sample Set IF water samples for organics, metals, and
TSS along Standard Transect at M8.
0015 | Collected Event 10/Sample Set 2H water samples for organics, metals, and
TSS along Standard Transect at M8.
0016
_____
0025
0027
0031 I
Dumping ended. Manhattan Island departed.
Collected Event 10/Sample Set 3F water samples for organics, metals, and
TSS along Standard Transect at M8.
Collected Event 10/Sample Set 4F water samples for organics, metals, and
TSS along Standard Transect at M8.
Collected Event 10/Sample Set 5H water samples for organics, metals, and
TSS along Standard Transect at M8.
0035
Collected Event 10/Sample Set 6H water samples for organics, metals, and
TSS along Standard Transect at M8.
Collected Event 10/Sample Set 7F water samples for organics, metals, and
TSS along Standard Transect at M8.
0042 i
"0045f
Collected Event 10/Sample Set 8H water samples for organics, metals, and
TSS along Standard Transect at M8.
Collected Event 10/Sample Set 9F water samples for organics, metals, and
TSS along Standard Transect at M8.
I 0120
""1)133" |
_l
0136 i
Pump not working, tripping breakers. Cleaned and deployed.
Collected Event 10 post-dump water samples for organics, metals and TSS at
Station PI.
Collected Event 10 post-dump water samples for organics, metals and TSS at
Station P2.
0140 Collected Event 10 post-dump water samples for organics, metals and TSS at
Station P3.
0305
Crew departed at HCM.
Departed HCM for cell M8.
Advised by the tugboat Little Joe that the Manhattan Island is not due in the
survey area until 1600-1630.
18
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
1435 \ Moored at Pier 1 to await the barge. Pumping system decontaminated.
1522 Departed Pierl for survey area.
1535 Arrived survey area.
1543 | Advised Manhattan Island estimated time of arrival at 1615.
1610 i System experienced weak flow. Corrective maintenance and calibration
performed.
1616 System deployed.
1641 System flow stopped. System retrieved and fixed. |
I650 I Manhattan Island set up on M19. Attempted to call dredge about setting up |
I on M8, with no response. Attempted to call Bob Cuzzelli but his cell phone j
was turned off. I
1705 Manhattan Island dumped1 at M19 insteadi of M8. Manhattan Island finished \
dumping at M8 and departs survey area. Manhattan Island did not respond to |
I radio hails. I
1712 Departed survey area for HCM. j
1720 Followed tugboat Little Joe to discuss with Bob Cuzzelli the just-completed |
dumping at M8. Mr. Cuzzelli indicated he did not realize that they were |
dumping at the wrong site. I
1824 I AJcrivedHCMT " ~ " " " " " ~~ " ~~
I. _ _ _ _ _
Wednesday, September 20,2000
0730 | Crew arrived. Equipment checks OK.
"0820TD^pMtedlKMfoTM8r" " ~ ~
0921 | Enter survey area and begin equipment decontamination.
0943 I Collected Event 12"pre-"idump water samples for organics, metals and TSS at
I | Station Bl.
I 0950 [ Collected Event 12 pre-dump water samples for organics, metals and TSS at
| [ Station B2.
| 0954 i Collected Event 12 pre-dump water samples for organics, metals and TSS at
Station B3.
1010 Manhattan island arrived at M8 to dump west to east.
1025 Manhattan Island began dumping.
1034 i Collected Event 12/Sample Set IF water samples for organics, metals, and
| TSS along Standard Transect at M8.
I037 | Little Joe moves to other side of Manhattan Island to help drop in reverse
I direction.
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
1039 | Collected Event 12/Sample Set 2H water samples for organics, metals, and
| TSS along Standard Transect at M8.
1045 | Collected Event 12/Sample Set 3F water samples for organics, metals, and
| TSS along Standard Transect at M8.
T049 1 Collected Event 12/Sample Set 4F water samples for organics, metals, and
| TSS along Standard Transect at M8.
1052 | Dumping completed.
1055 1 Collected Event 12/Sample Set 5H water samples for organics, metals, and
| TSS along Standard Transect at M8.
1101 I Collected Event 12/Sample Set 6H: water samples for organics, metals, and
| TSS along Standard Transect at M8.
1105 Collected Event 12/Sample Set 7F water samples for organics, metals, and
TSS along Standard Transect at M8.
1111 Collected Event 12/Sample Set 8H water samples for organics, metals, and
TSS along Standard Transect at M8.
1113 Collected Event 12/Sample Set 9F water samples for organics, metals, and
TSS along Standard Transect at M8.
1142 Complete Figure 8 runs.
1153 Collected Event 12 post-dump water samples for organics, metals and TSS at
I Station PI.
r i
1151 I Collected Event 12 post-dump water samples for organics, metals and TSS at [
i | Station P2.
| 1201 Collected Event 12 post-dump water samples for organics, metals and TSS at
t Station P3.
1205 Retrieved equipment and departed for HCM
1305 AniveidHCM Demobilized.
Thursday, September 28,2000
0756 DepartedlHCML
0900 O" station for Event 13 post-dumping activities. System cleaned.
0914 Equipment deployed.
| Collected Event 13 post-dumping water samples for organics, metals and TSS
| at Station IF.
0927 Collected'Event 13 post-dumping water samples for organics, metals and TSS |
at Station 2H. I
20
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Boston Harbor Plume Tracking Survey Report June 15, 2001
0930 | Collected Event 13 post-dumping water samples for organics, metals and TSS
I at Station 3F.
0933 [ Collected Event 13 post-dumping water samples for organics, metals and TSS
I at Station 4F.
0936 | Collected Event 13 post-dumping water samples for organics, metals and TSS
I at Station 5H.
i
0939 I Collected Event 13 post-dump water samples for organics, metals and TSS at
I Station 6H.
I 0942 | Collected Event 13 post-dump water samples for organics, metals and TSS at i
I I Station 7F. I
| 0944 | Collected Event 13 post-dump water samples for organics, metals and TSS at
I I Station 8H.
I 0947
Collected Event 13 post-dump water samples for organics, metals and TSS at
Station 9F.
0950 Collected Event 13 post-dump water samples for organics, metals and TSS at
I Station 10H.
1000 I Sampling completed.
4. Survey Results
Field sampling operations were successfully completed over a 23-day period during
which 10 separate events at CAD cells M8 and M19 were sampled and 138 sample sets
were collected (Table 5). One pre-capping event was sampled as a reference event to
characterize baseline conditions prior to capping operations. One post-capping event was
sampled to characterize post-dumping background conditions. Four capping events each
at CAD cells M19 and M8 were sampled to characterize the extent of any resuspension of
contaminate sediments caused by the capping operations. Equipment problems, primarily
with the BOSS pump, were responsible for missing 3 additional capping events at cell
M19. During the fourth cell M8 dumping event, sediments were actually dumped within
cell M19.
In situ hydrographic measurements of conductivity, temperature, depth, turbidity, and
transmissometry were collected during transit between stations (as much as possible) and
to follow the plume after daily capping operations were suspended. In most cases these
hydrographic measurements were taken at a depth of 2 m from the sea bottom, and in
some cases the measurements were made and one or more additional depths located at 2-
m increments above the bottom. During the survey, no apparent distinction in
turbidity/transmissometry could be made between the resuspension plume and the ever-
present visible capping material plume. Apparently, considerable concentrations of fine
particles in the capping sand were resuspended to produce a long-lasting and well-defined
plume that spanned the entire depth of the water column.
All field data (date, time, sampling coordinates, bathymetry, and sample depth) generated
during this survey are presented in Appendix A.
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01 .doc 21
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Boston Harbor Plume Tracking Survey Report
June 15,2001
Maps showing the actual sampling locations and transect lines between stations for each
set of events conducted on each sampling day are presented in Appendix B. The transect
lines are also color coded to indicate relative amount of turbidity.
Table 5. Actual Numbers and Types Transects Occupied and Samples Collected during
the Capping Resuspension Survey in Boston Harbor, MA.
Type of
Event
Pre-capping
Capping
Post-capping
Total
Number
of Events
2
9
1
12
Numbers and Types of Transects per
Event
- .- . ;
5 locations within uncapped area
3 pre-dump background transects per event
9 standard transects per event
3 post-dump background transects per
event
10 standard transects
Total Numbers of
Samples
Organics
10
24
72
22
10
138
Metals
10
24
72
22
10
138
TSS
10
24
72
22
10
138
5. Problems Experienced, Actions Taken, and
Recommendations
5.1. Schedule
Miscommunication between the captain and chief scientist resulted in a third missed
disposal event at cell Ml9. The captain did not receive the departure message and did
not report to the Aquamonitor at the appointed time.
Communications between the Aquamonitor and Manhatten Island (MI) were strained.
The MI was reluctant to respond to our questions regarding disposal initiation, pattern
of disposal, and time of arrival at the site. This made it very difficult to schedule
operations and conduct them efficiently.
A miscommunication between the U.S. Army Corps of Engineers observer allowed a
capping-material dump at M19 that should have occurred at M8. Because Battelle
completed monitoring operations at cell M19 and was monitoring at cell M8, the trip
was unproductive for the survey team aboard the Aquamonitor, and more importantly
was a needless expenditure of EPA funds.
5.2. Technical
All instruments worked well throughout the survey. However, the large coarse-
grained sand used as capping material severely wore the Teflon parts in the pump and
slip ring assembly of the water sampling system. As a result, two disposal events at
cell Ml9 were missed because repairs to the pumping system were necessary.
22
C:\Projects\Boston HarbonSurvey Report\Draftl Survey Report CAD-01 .doc
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Boston Harbor Plume Tracking Survey Report June 15, 2001
6. References
Battelle. 2000a. Quality Assurance Project Plan for Evaluation of Sediment Agitation
and Mixing into the Surrounding Water Column from Capping Activities: Boston Harbor
Site - Boston, Massachusetts. Report prepared for U.S. Environmental Protection
Agency; Cincinnati, OH.
Battelle. 2000b. Survey Plan for Evaluation of Sediment Agitation and Mixing into the
Surrounding Water Column from Capping Activities: Wyckoff/Eagle Harbor Site -
Bainbridge Island, Washington . Report prepared for U.S. Environmental Protection
Agency; Cincinnati, OH.
Fredette, T.J., P.E. Jackson, C.J. Demos, D.A. Hadden, S.H. Wolf, T.A. Nowak Jr., and
E. DeAngelo. 2000. The Boston Harbor Navigation Improvement Project CAD Cells:
Recommendations for Future Projects Based on Field Experience and Monitoring. Draft
paper submitted to the June 2000 Western Dredging Association Conference, Warwick,
RI.
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01.doc 23
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Boston Harbor Plume Tracking Survey Report June 15, 2001
Appendix A
Field Data for Samples
24 C:\Projects\Boston HarboASurvey Report\Draftl Survey Report CAD-01 .doc
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
Table A-l. Field Data for Samples
SamplelD SurveylD
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1 D:\CAD01\CAD01049.RAW |2AC B1
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ID Xposltidn I Yposition |zposition'|sampleDateTime|. Bathymetry
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! -71.06: 42.39: 9.70; 9/6/0012:23; 14.8:
I -71.06^ 42.39| 9.95: 9/6/0012:24! 14.5;
\ -71.06; 42.39; 12.69: 9/6/00 i2:24i 16.4;
-71.06; 42.39! 12.71! 9/6/0012:25! 16.1;
-71.061 42.39 12.69 9/6/0012:251 16.1
-71.06! 42.39 12.70 9/6/0012:251 15.8!
-71.06! 42.39! 9.84! 9/6/0012:26! 12.6
-71.06 42.39! 9.70 9/6/0012:261 12.7
-71.06; 42.39! 9.69! 9/6/00 12:27j 12.8
-71.06! 42.39! 9.66! 9/6/0012:271 12.9
i -71.06! 42.39! 9.60! 9/6/0012:28! 12.7t
! -71.06! 42.39! 12.041 9/6/0012:32! 15.7
! -71.06! 42.39! 13.28; 9/6/0012:32! 15.61
-71.06! 42.39! 13.30! 9/6/0012:33! 16.6'
-71.06! 42.39; 7.48! 9/6/00 J 4:1 3;^ 15.5
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-71.05 42.39 10.81 9/6/0014:14! 18.5
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-71.05! 42.39I 13.68 9/6/0014:18! 16.8
-71.05! 42.39I 14.40 9/6/0014:19! 16.1
-71.05! 42.39! 14.24! 9/6/0014:19! 16.2
-71.05 42.39 15.43 9/6/0014:22! 17.1
-71.05! 42.39! 14.10! 9/6/0014:22! 16.8
-71.05! 42.39! 9.87! 9/6/0014:23! 15.4
-7105 4238 1132 9/6/0014:24) 13.5
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-71.06 42.39! 12.84! 9/9/0015:59! 14.9
-71.05! 42.39! 13.08! 9/9/0015:59! 12.5
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' -71.05! 42.39! 13.92| 9/9/0016:01] 16.7
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i -71.05! 42.39! 8.74! 9/9/0017:071 16.6
C:\Projects\Boston Harbor\Survey ReportNDrattl Survey Report CAD-01 .doc
25
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
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1|D:\CAD01\CAD01069.RAW 1312
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7F -71 06
8H \ -71.06
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9F -71.05
9F ! -71 .05
9F -71.05
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P1 -71.05
P1 , -71 .05
P3 ! -71.06
P3 ! -71.06
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P2 ! -71 .05
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9/9/00 17:13
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9/9/00 17:24!
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Bathymetry
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13.6
17.1
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13.2
17.1
17.3
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12.9
15.1
13.2
15.5
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17.2
16.8
13.6
14.3
17.3
17.5
15.9
18.0
17.0
17.0
14.8
14.4
16.3
15.4
13.5
14.0
13.4
13.6
17.4
17.9
17.6
17.5
17.5
17.5
17.9
18.5
18.4
18.2
18.2
18.3
19.7j
19.8
19.8
19.8
19.8
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26
C:\Projects\Boston HarborXSurvey Report\Draftl Survey Report CAD-01 .doc
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Boston Harbor Plume Tracking Survey Report
June 15, 2001
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27
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
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C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01 .doc
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
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9/14/005:19
9/14/005:24
9/14/00 5:25
9/14/00 5:26
9/14/005:32
9/14/00 5:33
9/14/005:33
9/14/00 5:33
9/14/00 5:34
9/14/005:35
9/14/005:39
9/14/005:40
9/14/005:41
9/14/006:11
9/14/006:12
9/14/006:12
9/14/006:13
9/14/006:14
9/14/006:14
9/14/00 6:16
9/14/00 6:17
9/14/006:17
9/15/008:45
9/15/008:46
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9/15/008:48
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9/15/008:50
9/15/008:51
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13.9
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C:\Projects\Boston HarboASurvey Report\Draftl Survey Report CAD-01 .doc
29
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
SamplelD;
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C:\Projects\Boston Harbor\Survey ReportNDraftl Survey ReportCAD-01.doc
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
V-:-
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C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01 .doc
31
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
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P1 i -71.06
JP2 I -71 .06
iP2 i -71 .06
P2 i -71 .06
P3 i -71.06
!P3 I -71.06
P3 I -71 .06
;Vposition
42.39'
42.39;
42.39;
42.39:
42.39
42.39
42.39
42.39
: 42.39
4239
42.39
42.39:
42.39^
42.39
42.39
42.39
42.39;
42.39
42.39
42.39
42.39
42.39!
42.39!
4239
4239
4239
Zposition
14.09
6.96
13.00
13.12
8.73
13.77
13.85
13.88
14.47
14.46
14.45
9.34
9.38
11.56
14.33
14.30
7.88
11.06
11.05
11 05
1398
13.93
13.76
11 90
11 88
11 93
SarnpjeDateTirne '< ;
9/20/00 10:50:
9/20/00 10:50|
9/20/00 10:54:
9/20/00 10:55!
9/20/00 10:56!
9/20/00 11:01!
9/20/00 11:01!
9/20/00 11:02!
9/20/00 1 1 :05!
9/20/00 11:05
9/20/pp 11:06;
9/20/00 11:10!
9/20/00 11:1li
9/20/00 11:12i
9/20/0011:12!
9/20/0011:131
9/20/0011:13
9/20/00 11:52'
9/20/00 11:5J3|
9/20/00 1 1 :54!
9/20/00 11:56[
9/20/00 1 1 :57f
9/20/0011:58!
9/20/00 12:00,
9/20/00 12:01
9/20/00 12:02;
Bathymetry -
16.0
16.1
15.3
154
15.6
15.8
15.8
15,9
16.1
16.0
16.0
14.5
15.4
16.2
16.1
15.6
15.8
12.9
12.9
13.1
J6.2
16.2
16.4
15.2
15.3
...._ _ !5:5
32
C:\Projects\Boston HarboASurvey Report\Drafll Survey Report CAD-01 .doc
-------
Boston Harbor Plume Tracking Survey Report June 15, 2001
Appendix B-l
Survey Tracks CAD Cell M19, Boston Harbor, MA
C:\Projects\Boston HarboASurvey ReportXDraftl Survey Report CAD-01 .doc 33
-------
-------
042'23.342'N
«--
*
«
!
Figure B-l. Survey Track Pre Survey CAD Cell M19
-
3. 10.5 15.
Track Key - Seem Attenuation An
Figure B-2. Survey Track Pre Run 1 CAD Cell M19
-------
100m
042-23.02
071-03.478W
3. 105 18.
Track Key - Beam Attenuation A
Figure B-3L Survey Track Run 1 CAD Cell M19 with BOSS Four Meters from the
Sediment Surface
a % -.
^i.--p-1'
3, 10.S 18.
Track Key - ^sm Attenuation An
Figure B-4. Survey Track Run 1 CAD Cell M19 with BOSS Greater than 9.5 m Below
Water Surface
-------
1
%i ""»_
^m*m . *m
r.
042-22.969'N
071'03.7MW
^-r.^
3. 10.S 18.
Track Key - Beam AHenuatlon An
Figure B-5. Survey Track Post run 1 CAD Cell Ml9
042'22.969'N
071-03.744W
100 m * V
200m A
3. 10.5 18.
Trad: Key - Beam ABenualbn An
Figure B-6. Survey Track Pre ran 2 CAD Cell M19
-------
M19
100m
042'23.027'N
071tl3.47eW
3, 105 18.
Track Key - Beam Attenuation An
071-03.01BW
Figure B-7. Survey Track Run 2 CAD Cell M19 with BOSS Four Meters from the
Sediment Surface
/ /
200 m
100m
/IB
/ /Iff*"
-S
r.
042-22 seem
071'03J44W
3. 10.S IB.
Track Key - Beam Attenuation An
Figure B-8. Survey Track Run 2 CAD Cell M19 when BOSS is Greater than 9.5 Below
Water Surface
-------
"Hf
i*-
r mf
m
3. 10.5
Track Key - Beam Attenuation An
Figure B-9. Survey Track Post run 2 CAD Cell M19
042-
071-03.744W
3. 10.5 16
Track Key - Seam Attenuation An
Figure B-10. Survey Track Pre ran 3 CAD Cell M19
-------
I
im
042-23.01 SN
071-03.337W
M19
I I
i nn _ J
200m
3. 10.5 18.
Track Key - Beam Attenuation /m
Figure B-ll. Survey Track Run 3 CAD Cell M19 with BOSS Four Meters from the
Sediment Surface
200m '
100m
fy*
Ml 3
100m
042-22.969111
071'03.744W
3. 10.5 18.
Tract Key - Beam Attenuation *n
Figure B-12. Survey Track Run 3 CAD Cell M19 when BOSS is Greater than 9.5 Below
Water Surface
-------
I
042-22.969N
071-03.744W
3, 10.5 18.
Track Key - Beam Attenuation An
figure B-13. Survey Track Post run 3 CAD Cell M19
042-22.369^
071'03.744W
100 m
X
200m
Tr^kK
10.S 18.
Trade Key Beam Attenuation An
Figure B-14. Survey Track Pre run 4 CAD Cell M19
-------
M19
im
100m
200m
A
042-23.013N
071-03.337W
3. 105 18.
Trade Key - Beam Attenuation An
Figure B-15. Survey Track Run 4 CAD Cell M19 with BOSS Four Meters from the
Sediment Surface
10.5 18.
TracV Key - Beam Attenuation An
Figure B-16. Survey Track Run 4 CAD Cell M19 when BOSS is Greater than 9.5 Below
Water Surface
-------
' ', -v" <-
^_ ^v i «!
042-22-9S91M
071'03.744W
3. 10.5 1S.
Track Key - Beam Attenuslion An
Figure B-17. Survey Track Post run 4 CAD Cell M19
-------
-------
Boston Harbor Plume Tracking Survey Report June 15, 2001
Appendix B-2
Survey Tracks CAD Cell M8, Boston Harbor, MA
o A C:\Projects\Boston HarborVSurvey RepornDraftl Survey Report CAD-01.doc
-------
-------
042-23,342'N
. .»
»,&£« M1
,=" -1
.f I - y1
_ ^»_ « r
3. 10.S 18.
Track Key - Beam Attenuation An
Figure B-18. Survey Track Pre Survey CAD Cell M8
042-23 342'N
10.5 18.
Track Key - Beam Attenuation /m
Figure B-19. Survey Track Pre run 5 CAD Cell M8
-------
200m
100m
Q42'23.078'N
071°03.725W
M8
100 m
3. 10.5 tB.
Track Key - Seam Attenuation ftn
Figure B-20. Survey Track Run 5 CAD Cell M8 with BOSS Four Meters from the
Sediment Surface
3. 10,5 18,
Track Key - Beam Attenuation Jrn
Figure B-21. Survey Track Run 5 CAD Cell M8 with BOSS Greater than 9.5 m Below
Water Surface
-------
1
042-32.969W
07r03.7«W
. .
Track Key - Beam Attenuation An
Figure B-22. Survey Track Post run 5 CAD Cell
V -.
3. 10.5 18.
Track Key - Beam A
Figure B-23. Survey Track Pre ran 6 CAD Cell M8
-------
200m
M8
100m
3. 10.5 18.
Track Key - Beam Attenuation An
100m
Figure B-24. Survey Track Run 6 CAD Cell M8 with BOSS Four Meters from the
Sediment Surface
042'23 342'N
mm
042'22.969'N
071-03.744W
10.S 18.
Track Key - Beam Attenuation An
Figure B-25. Survey Track Run 6 CAD Cell M8 with BOSS Greater than 9.5 m Below
Water Surface
-------
200m
/ «««.-
to..-i*-
.. ///v
042'22.969'N
Q71'Q3.744W
3. 10.5 18.
Track Key - Beam Attenuation An
Figure B-26. Survey Track Post run 6 CAD Cell M8
2'23.342'N
,' r
042'22.969'N
071'03.744W
10.5 18.
Track Key - Beam Attenuation An
Figure B-27. Survey Track Pre run 7 CAD Cell M8
-------
1
200m
100m
10.5 18.
Track Key - Beam Attenuation An
100 m
Figure B-28, Survey Track Run 7 CAD Cell M8 with BOSS Four Meters from the
Sediment Surface
m-
200m
100m
042122.969'N
07r03.74
-------
3. 10.5 18
Track Key - Seam Attenuation An
Figure B-30. Survey Track Post run 7 CAD Cell M8
200m
M8
100m
3. 10.5 18.
Track Key - Beam Attenuation fm
100m
Figure B-31. Survey Track Pre run 8 CAD Cell M8
-------
200m
042'23.078'N
071-03.725W
100m
H8
3. 10,5 IB,
TracK Key - Beam, firtenwaloi im
100 m
Figure B-32. Survey Track Run 8 CAD Cell M8 with BOSS Four Meters from the
Sediment Surface
1
200m
M8
100m
3. 105 18.
facfc. Key - Seam Wlenuation An
100m
Figure B-33. Survey Track. Post, run 8 CAD Cell M8
-------
Boston Harbor Plume Tracking Survey Report
June 15,2001
Appendix C
TSS values based on Beam Attenuation
SurveylD CODE SamplelD STATION DEPTH
CADO 102D P2 12
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
1050
1053
1021
104D
102A
104A
1027
1056
1024
12B2
12EC
12AF
12D2
12F4
12CF
12C6
12FO
12BF
12EO
120C
12C3
12CC
B3
P1
B1
B2
P1
B1
B3
P2
B2
B3
P1
B2
6H
P2
5H
3F
P3
1F
9F
8H
2H
4F
13.7
15.4
8.8
14
9.7
7.5
12.7
11.3
12.7
10.5
10.8
15
14.7
13.6
14.2
15.7
13.6
16.6
13.5
7.6
11.9
8.7
TSS
2.73
3.07
3.65
4.475
2.585
2.93
2.165
2.47
2.46
3.175
3.25
3.86
2
2.19
2.575
2.62
3.545
4.175
2.45
2.37
3.435
3.79
9.01
9.185
5.315
5.13
114.44
113.675
9.085
8.93
39.11
40.82
119.975
125.24
9.74
9.175
118.105
126.695
45.3
47.845
21.415
21.5
96.275
94.08
68.555
74.555
C:\Projects\Boston HarborNSurvey Report\Draftl Survey Report CAD-01 .doc
35
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
SurveylD
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CODE
12AC
12D6
133A
134E
1331
137A
1371
1312
1334
130C
1325
1376
1337
134B
131F
132E
1348
130F
132B
1322
13A6
13C9
13AA
139F
SamplelD STATION
B1
7F
9F
P3
6H
B3
B1
B2
7F
B1
3F
B2
8H
P2
1F
5H
P1
B3
4F
2H
6H
P1
7F
4F
DEPTH
12.8
8.1
16.4
12.4
16.6
14.9
14.1
14.5
15.9
10.9
16.1
17
15.8
16.5
15.6
18.5
12
10.4
15.7
16.3
15.9
10.3
15.5
16.3
TSS
4.44
4.685
14.395
14.155
15.305
17.86
13.695
14.345
1 1 .835
12.32
3.055
3.73
4.09
4.085
16.13
16.43
27.255
28.525
13.86
14.09
35.115
35.145
3.93
3.695
15.29
15.64
7.785
8.12
22.9
25.815
34.665
36.52
11.29
1 1 .795
14.235
14.95
41.625
42.7
25.545
25.67
8.24
8.78
5.45
6.275
9.255
9.66
30.805
32.83
36
C:\Projects\Boston HarboiASurvey Report\Draftl Survey Report CAD-01 .doc
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
Ip-l
u
Survey ID
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CODE
13A2
1394
1390
13B4
13BO
1398
1410
1428
1422
142B
143C
1439
1425
142E
1436
140B
141F
141C
1416
1408
1405
14AO
1489
1486
SamplelD STATION
5H
2H
1F
9F
8H
3F
2H
7F
5H
8H
P3
P2
6H
9F
P1
B3
4F
3F
1F
B2
B1
P2
5H
4F
DEPTH
15.2
16.4
13.7
14.6
11.3
13.2
16
15.3
10.6
11.6
11.8
.16.4
17
16.6
12.4
9.9
16.4
15.1
16.8
15
10.3
14.1
12.6
14.3
TSS
19.98
21 .685
52.425
54.425
26.205
27.34
12.21
12.27
8.955
9.37
22.33
22.395
18.565
19.425
11.72
11.78
21.76
22.08
8.515
8.72
3.735
3.935
4.86
4.425
18.02
17.18
7.475
7.595
3.545
3.43
4.615
4.045
24.235
25.825
16.015
16.935
40.5
36.93
5.64
5.195
5.48
5.1
8.79
8.7
43.64
45.875
73.135
73.91
C:\Projects\Boston HarborXSurvey Report\Draftl Survey Report CAD-01.doc
37
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
Survey ID
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CODE
1480
147D
1483
149D
1495
14A3
146C
146F
1469
1492
148F
148C
154F
1538
153B
1514
1526
14ED
1544
153E
1534
1511
14EA
14E4
SamplelD STATION
2H
1F
3F
P1
9F
P3
B2
B3
B1
8H
7F
6H
9F
2H
3F
P2
B2
7F
6H
4F
1F
P1
6H
4F
DEPTH
14.2
14.9
14.5
12.2
13.7
9.5
15.4
10.6
11.4
14.4
9.8
12.5
15.9
16.3
16.5
16.3
16.6
15.3
15.7
17.3
17.2
13.2
15.3
15.6
TSS
68.96
72.675
102.96
102.37
91.41
96.895
9.145
9.315
12.865
13.055
7.76
8.09
8.05
6.36
4.2
3.93
3.32
3.68
24.945
23.725
16.11
16.425
24.82
26.365
5.58
5.635
26.95
27.2
19.82
21 .545
4.845
4.75
4.065
5.165
12.135
1 1 .795
6.47
8.65
7.075
7.675
189.225
194.245
4.615
5.44
30.12
30.64
29.115
31.885
38
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01.doc
-------
Boston Harbor Plume Tracking Survey Report
June 15,2001
SurveylD
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CODE
14E7
14DE
14DB
14F3
14D4
14C5
154C
14BF
14C2
1529
151A
14F6
1547
1523
1541
155E
1564
1561
15C2
15C5
15DF
15AB
15CB
15CE
SamplelD STATION
5H
3F
2H
8H
1F
B3
8H
B3
B2
B3
P3
9F
7F
B1
5H
P1
P3
P2
1F
2H
9F
B1
3F
4F
DEPTH
14.2
14.2
15.2
13
15.4
12.9
13.5
10.9
10.9
10.2
14.5
15.1
17.3
11.8
16.9
10.7
10.8
16.7
13.1
13.9
14.3
13.1
13.4
14.1
TSS
38.305
37.955
36.45
35.495
38.1
37.055
2.73
3.135
51.845
52.12
2.31
2.67
4.565
4.995
2.85
2.875
3.09
3.29
5.25
7.815
5.055
4.66
10.72
1 1 .285
5.765
5.965
5.185
5.165
9.515
10.36
4.155
4.44
3.805
4.295
3.225
3.585
50.515
46.855
8.945
9.235
10.205
11.26
3.89
4.6
24.34
26.15
35.355
37.17
C:\Projects\Boston Harbor\Survey Report\Draftl Survey Report CAD-01 .doc
39
-------
Boston Harbor Plume Tracking Survey Report
June 15, 2001
SurveylD
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CADO
CODE
15D1
15D4
15EF
15F2
15BO
15B3
15D7
15DC
15F5
1610
1613
1616
1619
161C
1620
1623
1626
1629
162C
SamplelD STATION
5H
6H
P1
P2
B2
B3
7F
8H
P3
1F
2H
3F
4F
5H
6H
7F
8H
9F
10H
DEPTH
13
13.8
11.1
14
14
10.3
14.5
9.3
11.9
12.4
14.5
13.5
16.7
10.7
10.7
15.5
15.1
15.8
10.2
TSS
12.635
14.115
15.435
15.695
4.45
4.51
4.31
4.255
4.04
4.565
1.975
2.135
11.575
12.345
9.575
10.385
2.79
2.935
4.25
4.035
3.525
3.695
3.29
3.66
3.175
3.39
2.255
2.525
2.97
3.38
2.24
2.105
2.43
2.495
3.865
3.76
1.59
1.56
40
C:\Projects\Boston HarborXSurvey Report\Draftl Survey Report CAD-01 .doc
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX B
CHAIN OF CUSTODY FORMS
-------
-------
Billing Information :
Battelie
505 King Avenue
Client:
Battelie Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
Page:
1 ofS
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
TEL: (775) 355-1044 FAX: (775) 355-0406
WorkOrder : BMI00092242
Company Phone/Fax
TEL: (614)424-7358
FAX: (614)424-3667
Job"
PO:
! Secondary Phone/Fax
'.TEL: (614)424-3723
[FAX: (614)424-3667
MWRA Harbor and Outfall Monitoring Program
Client's COC #: none
..' Report Due By : 5:00 PM On : 06-Oct-OO
I
! HDD Required : Yes
i
.-' Sampled by : Client
Cooler Temp: 12 °C 22-Sep-OO
QCLev*'!: S4
Alpha
Sample ID
: BMI00092242-01A
I BMI00092242-02A
i
; BM100092242-03A
: BMI00092242-04A
BMI00092242-05A
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Client Collection
Sample ID Matrix Date
CAD0133AMM
1
CAD01348MM
CAD0134BMM
A
CAD0134EMM
1
CAD01371MM
! 1
BMI00092242-06AJ CAD01376MM
I 1
BMI00092242-07A
Comments:'
Relinquished by:
Received by:
Relinquished by:
Received by:
CAD0137AMM
! 1
No. of Bottles
ORG SUB TAT
AQ~To.9/io/o6n o T 1
I 09:40 I I \
AQ
AQ
AQ
AQ
AQ
AQ
09/10/00
10:14
09/10/00
10:17
0
~
09/10/00 I 0
10:19 I
09/10/00
11:16
09/10/00
11:19
09/10/00
11:21
0
0
0
1
1
1
1
1
1
,. |
10
,0
,0
10
10
No security seals, real and blue ice melted. Contract No. S27^
[~~ Signature |
__£
, - -
<..(AAi
j/l/v^-tnAA
1
PWS#
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag,Sc
As. Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be. Cd,
Cr. Pb, Hg.
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As,Be,Cd,
Cr, Pb, Hg,
AS, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg.
Ag.Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag,Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr. Pb, Hg.
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Sc
As, Be. Cd,
Cr, Pb. Hg.
Ag, Se
Sample Remarks
RCRAWetals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
| RCRA Metals
&G&A S MifaU fvr c<.(l 5a-V^.t'-4-M.
| Print Name | f~ Company |
\(*>MA*
'^t
- -
-- - -
.
RCRA Metals
i Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Olher
-------
Billing Information :
Batielle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
i TEL: (775) 355-1044 FAX: (775) 355-0406
i Company Phone/Fax ; j Secondary Phone/Fax
I TEL: (614)424-7358 j ! TEL : (614)424-3723
[FAX: (614)424-3667 _ | JFAX: (614)_424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
Page:
2 of 5
WorkOrder : BMI00092242
Report Due By : 5:00 PM On : 06-Oct-OO
EDD Required : Yes
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QC Level: S4
Final Rpt, MBLK. LCS, MS/MSD With Surrogates
Alpha
Sample ID
: BMI00092242-08A
: BMI00092242-09A
Client Collection
Sample ID Matrix Date
CAD01390MM
1
CAD01394MM
1
: BMI00092242-10A I CAD01398MM
I 1
BMI00092242-11A
BMI00092242-12A
.BM100092242-13A
Comments:
CAD0139FMM
1
CAD013A2MM
1
AQ I 09/11/00
I 01:13
AQ
AQ
AQ
AQ
09/11/00
01:16
09/11/00
01:19
09/11/00
01:21
09/11/00
01:26
CAD013A6MM] AQ I 09/11/00
I 1 II 01:30
No. of
ORG
0
0
"
o
0
b
i
Bottles
SUB TAT PWS #
1 I 10
1
1
1
1
1
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg.
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be. Cd,
Cr.Pb.Hg,
Ag,Se
As, Be, Cd.
Cr, Pb, Hg.
Ag.Se
As, Be, Cd,
Cr, Pb. Hg,
Ag, Sc
As, Be. Cd.
Cr, Pb, Hg,
Ag,Se
MERCURY
As,Be.Cd,
Cr, Pb. Hg.
Ag.Se
As, Be. Cd,
Cr, Pb, Hg.
Ag.Se
As. Be, Cd.
Cr, Pb, Hg,
Ag, Se
As. Be. Cd,
Cr, Pb, Hg.
Ag,Se
As. Be, Cd.
Cr, Pb. Hg,
Ag,Se
As, Be. Cd,
Cr, Pb. Hg,
Ag.Se
r s
.....
Sample Remarks
RCRA Metals. Filler sample
prior to analysis, and
analyze for both aqueous
and solid phase.
RCRA Metals. Filter sample
prior to analysis, and
analyze for both aqueous
and solid phase.
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
No security seals, real and blue ice melted. Contract No. S274
, .. 1
Signature
Print Name
Company
Date/Time
Relinquished by:
Received by:
Relinquished by:
Received by:
.
i
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Batteile
505 K>ng Avenue
Client:
Batteile Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
3 of 5
Company Phone/Fax j j Secondary Phone/Fax
TEL: (614)424-7358 \ \ TEL: (614)424-3723
FAX: (614)424-3667 I j FAX: (614)424-3667
Job :~ MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
WorkOrder : BMI00092242
Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required : Yes
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QC Level: S4 = Final Rpt, MBLK. LCS, MS/MSD With Surrogates
Alpha Client Collection
Sample ID Sample ID Matrix Date
BMI00092242-14A
BMI00092242-15A
:BMI00092242-16A
BM1.00C92242-17A
BMI00092242-18A
CAD013AAMM
1
CAD013BOMM
1
CAD013B4MM
1
CAD013C9MM
1
CAD015ABMM
1
BMJ00092242-19A| CAD015BOMM
I 1
, BM100092242-20A
CAD015B3MM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/11/00
01:33
09/11/00
01:39
09/11/00
01:41
09/11/00
02:25
09/20/00
09:43
09/20/00
09:50
No. of Bottles
ORG SUB TAT PWS #
0 I 1
0
0
0
i
i 0
09/20/00 i 0
09:53 :
1
1
1
1
1
1
10
1U
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd.
Cr, Pb, Hg,
Ag,Se
MERCURY
As. Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr. Pb, Hg.
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As. Be. Cd,
Cr, Pb, Hg,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg.
Ag,Se
I
Sample Remarks
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals I
RCRA Metals I
RCRA Metals
RCRA Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
I Signature
Print Name 1
Company
Date/Time
Relinquished by:
Received by:
Relinquished by:
Received by:
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
CHAIN-OF-CUSTODY RECORD
Page:
4 of 5
suo Mng avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
QC Level: S4
Alpha
Sample iD
BMI00092242-21A
! BMI00092242-22A
3MI00092242-23A
] BMI00092242-24A
i BMI00092242-25A
BMI00092242-26A
; BMI00092242-27A
Comments:
I Relinquished by:
Received by:
Relinquished by:
Received by:
= Final Rpt, MBLK,
Alpha Analytical, Inc. Work!
255Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
TEL: (775) 355-1 044 FAX: (775) 355-0406 i
- -- ; : ;;:"..'.. ::z:::J Report Due
Company Phone/Fax [ Secondary Phone/Fax
iTEL: (614)424-7358 j TEL : (614)424-3723 ! EDI
iFAX: (614)424-3667 | | FAX : (614)424-3667
Job:
PO:
MWRA Harbor and Outfall Monitoring Program
Client's COC # : none
Drder : BMI00092242
By : 5:00 PM On : 06-Oct-OO
) Required : Yes
Sampled by : Client
Cooler Temp: 12 °C 22-Sep-OO
LCS, MS/MSD With Surrogates
Client Collection
Sample ID Matrix Date
CAD015C2MM A(
1
CAD015C5MM A(
1
CAD015CBMM A
1
CAD015CEMM A
1
CAD015D1MM A
1
CAD015D4MM A
1
CAD015D7MM A
1
3 09/20/00
10:34
a 09/20/00
10:38
3 09/20/00
10:45
Q 09/20/00
10:49
Q 09/20/00
10:54
Q 09/20/00
11:01
Q 09/20/00
11:05
No. of Bottles
ORG SUB
0
0
0
0
' 0
: 0
1
1
1
1
1
1
1
TAT PWS #
10
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr.Pb, Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb. Hg,
Ag,Se
As. Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be, Cd.
Cr. Pb. Hg,
Ag, Sc
No security seals, real and blue ice melted. Contract No. S274
| Signature |
^^K
MERCURY |
J _
As,Bc,Cd,
Cr. Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag, Se
As,Be,Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
I
As, Be.Cd,
Cr, Pb, Hg. ;
Ag.Se
| Print Name j
'&
>'2^-/
'
-
1
i
Sample Remarks
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
1 RCRA Metals
1 RCRA Metals
RCRA Metals
Company ; Dale/Time
-- --
W""
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Alr) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc. i
Page:
5 of 5
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
TEL: (775) 355-1044 FAX: (775) 355-0406
WorkOrder : BMI00092242
i
Company Phone/Fax
I TEL: (614)424-7358
Secondary Phone/Fax
TEL: (614)424-3723
[FAX: (614)424-3667 | | FAX: (614)424-3667
"job": """
PO:
MWRA Harbor and Outfall Monitoring Program
Client's COC # : none
:-_-' Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required : Yes
Sampled by : Client
Cooler Temp: 12 °C 22-Scp-OO
QC Level: S4
= Final Rpt. MBLK, LCS, MS/MSD With Surrogates
Alpha Client
Sample ID Sample ID
Collection No. of Bottles
Matrix Date ORG SUB TAT PWS #
; BM|60092242-28A I CAD015DCMMT AQ I 09/20/00
! I 1 II 11:10
! BMI00092242-29A
i
| BMI00092242-30A
i BMI00092242-31A1
i BMI00092242-32A
!
CAD015DFMM
1
AQ
CAD015EFMM) AQ
1 I
CAD015F2MM
1
AQ
CAD015F5MM I AQ
1 I
09/20/00
11:12
09/20/00
11:52
09/20/00
11:56
09/20/00
12:00
0
0
0
0
0
^
1
1
1
1
10 I
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb. Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be. Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb. Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg.
Ag.Se
MERCURY
~As,~ie7cd7
Cr, Pb, Hg,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg,
Ag, Se
As. Be, Cd.
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb. Hg.
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
Sample Remarks
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
Signature
Relinquished by:
Received by:
Relinquished by:
Received by:
f Print Name ~|
Company
Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order : BMI00092242
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BMI00092242-01A CAD0133AMM1
BMI00092242-02A CAD01348MM1
BMI00092242-03A CAD0134BMM1
BMI00092242-04A CAD0134EMM1
BMI00092242-05A CAD01371MM1
BMI00092242-06A CAD01376MM1
BMI00092242-07A CAD0137AMM1
BMI00092242-08A CAD01390MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/10/00
09:40
Aqueous 09/10/00
10:14
Aqueous 09/10/00
10:17
Aqueous 09/10/00
10:19
Aqueous 09/10/00
11:16
Aqueous 09/10/00
11:19
Aqueous 09/10/00
11:21
Aqueous 09/11/00
01:13
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
___ _ . . ruidi r\ui, IVIDI
EDO Required:
Yes
Requested Tests
SW7470
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Tolal
(MERCURY)
_r\, L^O, ma/mau wnn surrogates
22-Sep-OO
i
I Comments
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Melals. Filter sample prior
lo analysis, and analyze lor both
aqueous and solid phase.
Comments:
CA samples. Note comment for samples -08 and -09. A . A
dnf /§t
[ Date/Time ]
Date/Time
Relinquished by:
Relinquished by:
Received by:
Received by:
-------
Alpha Analytical, Inc.
255 (iloulalc Avenue
Suite :i
Sparks, Nevada 89431-5778
Phone: (775)355-1044
l;ax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092242
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BMI00092242-09A CAD01394MM1
BMI00092242-10A CAD01398MM1
BMI00092242-11A CAD0139FMM1
BMI00092242-12A CAD013A2MM1
BMI00092242-13A CAD013A6MM1
BMI00092242-14A CAD013AAMM1
BMI00092242-15A CAD013BOMM1
BMI00092242-1BA CAD013B4MM1
Co
mments: CA samples.
Relinquished by: /
Relinquished by:
TEL: (702)857-2400
FAX: (702) 857-2404
Acct#:
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/11/00 OTHER (1)
01:16
Aqueous 09/11/00 OTHER (1)
01:19
Aqueous 09/11/00 OTHER (1)
01:21
Aqueous 09/11/00 OTHER (1)
01:26
Aqueous. 09/11/00 OTHER (1)
01:30
Aqueous 09/11/00 OTHER (1)
01:33
Aqueous 09/11/00 OTHER (1)
01:39
Aqueous 09/11/00 OTHER (1)
01:41
rn0*rt/T!
uaie/ 1 1
' " ' - ~ '*-<.'-'.-'- f-t y_-__:..
p. p . . riuai i\fji, muurv, LV>O, iviomiou vvnii 01
Yes
Requested Tests
E200.8 SW7470
Com
mugaies
22-Sep-OO
merits
Inorganics by EPA MERCURY, Total RCRA Metals. Filter sample prior
Method 200.8 (MERCURY) to analysis, and analyze for both
(200.8) aqueous and solid phase.
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200,8)
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200.6)
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total RCRA Metals
Method 200.8 (MERCURY)
(200.8)
i
me J "" . Date/Tim
/.5yj "Received by: %%&& $3 <~*£~^*-~~" ^f'3.3. -&* /J^^
Received by:
e ' (-
,
-------
Alpha Analytical, Inc.
255 Glendalc Avenue
Suite 21
Sparks, Nevada 89431-5778
I'liiine:' (775)355-1044
1-ax: (775) 355-(MO(,
Subcontractor:
Sierra Environmental Monitoring
1135 Financial Blvd.
Reno, NV 89502
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092242
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
EDO Required:
Yes
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha's Sample ID Client's Sample ID
BMI00092242-17A CAD013C9MM1
BMI00092242-18A
BMI00092242-19A
BMI00092242-20A
BMI00092242-21A
CAD01SABMM1
CAD015BOMM1
CA0015B3MM1
CAD015C2MM1
BMI00092242-22A
CAD015C5MM1
BMI00092242-23A
BMI00092242-24A
Comments:
CAD015CBMM1
CAD015CEMM1
CA samples.
Requested Tests
Collection Type (j») or Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/11/00
02:25
OTHER (1)
Aqueous 09/20/00
09:43
Aqueous 09/20/00
09:50
Aqueous 09/20/00
09:53
Aqueous 09/20/00
10:34
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
Aqueous 09/20/00
10:38
Aqueous 09/20/00
10:45
Aqueous 09/20/00
10:49
OTHER (1)
OTHER (1)
OTHER (1)
E200.8
SW7470
Inorganics by EPA MERCURY. Tola)
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.8)
22-Sep-OO
Comments
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
I Relinquished by:
!
Relinquished by:
j Date/Time ~"| - - .
,JV t ., ...
'/£. rrVr/.';.-V. /^ ;A. Received by;
Received by:
Date/Time
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHA1N-OF-CUSTODY RECORD
Work Order : BMI00092242
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page , of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BMI00092242-25A CAD015D1MM1
BMI00092242-26A CAD015D4MM1
BMI00092242-27A CAD015D7MM1
BMI00092242-28A CAD015DCMM1
BMI00092242-29A CAD015DFMM1
BMI00092242-30A CAD015EFMM1
BMI00092242-31A CAD015F2MM1
BMI00092242-32A CAD015F5MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/20/00
10:54
Aqueous 09/20/00
11:01
Aqueous 09/20/00
11:05
Aqueous 09/20/00
11:10
Aqueous 09/20/00
11:12
Aqueous 09/20/00
11:52
Aqueous 09/20/00
11:56
Aqueous 09/20/00
12:00
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
EDO Required: Hl " ' °0' '"°
Yes
E200.8
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
»
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
[viou vvmi ounuyaius
22-Sep-OO
Comments
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
RCRA Metals
Comments:
CA samples.
Relinquished by:
Relinquished by:
[ Date/Time" J
''-''.--'--/-A'.> /<">>>! Received by:
" ~
Received by:
Date/Time
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus. OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Page:
1 of 14
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
TEL: (775) 355-1044 FAX: (775) 355-0406
I Company Phone/Fax
I TEL: (614)424-7358
[ FAX : (614) 424-36_67 _
| Secondary Phone/Fax
! TEL : (614) 424-3723
I FAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required : Yes
Sampled by : Client
Cooler Temp : 12 °C 22-Sep-OO
QC Level: S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS #
BMI00092241-01A
BMI00092241-02A
BMI00092241-03A
BMI00092241-04A
BMI00092241-05A
BMI00092241-06A
i BMI00092241-07A
1
CAD01021MM
1
CAD01024MM
1
CAD01027MM
1
CAD0102AMM
1
CAD0102DMM
1
CAD0104AMM
1
CAD0104DMM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/06/00
12:23
09/06/00
12:24
09/06/00
12:25
09/06/00
12:27
09/06/00
12:32
09/06/00
14:13
09/06/00
14:14
0
0
0
0
0
0
0
1
1
1
1
1
1
1
10
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As,Be.Cd,
Cr, Pb. Hg.
Ag.Se
As, Be, Cd,
Cr. Pb, Hg,
Ag.Se
As. Be. Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg.
Ag, Se
I As, Be. Cd,
Cr. Pb, Hg,
Ag, Se
As. Be. Cd,
Cr. Pb, Hg.
Ag.Se
MERCURY
As. Be. Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb. Hg,
Ag.Se
As. Be, Cd,
Cr.Pb,Hg,
Ag.Se
As, Be, Cd.
Cr, Pb, Hg,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg.
Ag.Se
As. Be, Cd,
Cr. Pb, Hg,
Ag,Se
__
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
1 RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No.!
f" Signature 1
Print Name
I Relinquished by:
| Received by:
i
| Relinquished by:
! Received by:
Company J |~ Date/Time
J/M/iK>IOJ$
frj££><
>«3
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-SoilJar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus. OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
i Alpha Analytical, Inc. j
; 255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778 |
I TEL: (775)355-1044 FAX: (775) 355-0406
Page:
2 of 14
WorkOrder : BMI00092241
i Company Phone/Fax
]TEL: (614)424-7358
i FAX: (614)424-3667
Secondary Phone/Fax
I j TEL: (614)424-3723
FAX: (614)424-3667
Report Due By : 5:00 PM On : 06-Oct-OO
Job : MWRA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
HDD Required: Yes
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QCLevel: S4
Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS#
BMI00092241-08A
BMI00092241-09A
BMI00092241-10A
BMI00092241-11A
IBMI00092241-12A
JBMI00092241-13A
\
BMI00092241-14A
CAD01050MM
1
CAD01053MM
1
CAD01056MM
1
CAD01405MM
1
CAD01408MM
1
CAD0140BMM
1
CAD01416MM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/06/00
14:18
09/06/00
14:22
09/06/00
14:24
09/12/00
21:35
09/12/00
21:36
09/12/00
21:38
09/12/00
22:14
0
0
0
0
0
0
0
1
1
1
1
1
1
1
10
10
10
10
10
10
10
Requested Tests
200_8
As. Be. Cd.
Cr, Pb. Hg.
Ag, Se
As, Be. Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg.
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag. Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag. Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
MERCURY
As, Be, Cd,
Cr.Pb,Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Bc,Cd,
Cr, Pb, Hg,
Ag.Sc
As, Be, Cd.
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg.
Ag, Se
As,Be,Cd,
Cr, Pb, Hg,
Ag. St
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
Relinquished by:
Received by:
Relinquished by:
Received by:
No security seals, real and blue ice melted. Contract No. S274
Signature
Print Name
I Company ~j
Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus. OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Page:
3 of 14
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
WorkOrder : BMI00092241
: Company Phone/Fax
I TEL: (614)424-7358
FAX: (6^14)424-3667
Job":
PO:
Secondary Phone/Fax
TEL: (614)424-3723
FAX : (614) 424-3667
:; Report Due By : 5:00 PM On : 06-Oct-OO
I
! HDD Required : Yes
MWRA Harbor and Outfall Monitoring Program
Client's COC #: none
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QC Level: S4
Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha
Sample ID
BMIOOOS2241-15A
BMI00092241-16A
Client Collection No. of Bottles
Sample ID Matrix Date ORG SUB TAT PWS #
CAD01419MM
1
CAD0141CMM
1
IBMI00092241-17AI CAD0141FMM
I 1
BMl6o092241-18A| CAD01422MM
I 1
BMI00092241-19A
CAD01425MM
1
BMI00092241-20AI CAD01428MM
I 1
BMI00092241-21A
i
CAD0142BMM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/12/00
22:17
09/12/00
22:20
09/12/00
22:24
09/12/00
22:29
09/12/00
22:36
09/12/00
22:37
09/12/00
22:45
0
0
0
0
0
0
0
1
1
1
1
1
1
1
10
10
10
10
Requested Tests
200_8
As. Be, Cd,
Cr, Pb. Hg,
Ag,Se
As, Be, Cd.
Cr.Pb,Hg.
Ag.Se
I As,Be,Cd,
I Cr, Pb, Hg,
' Ag, Se
,0 |
10
10
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As. Be, Cd.
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb. Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
MERCURY
As, Be, Cd,
Cr.Pb.Hg.
Ag.Se
As, Be, Cd,
Cr, Pb. Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr. Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg.
Ag, Se
As, Be, Cd.
Cr. Pb, Hg,
Ag, Sc
r i
r I"
i
i
r
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
~ RCRA 8 Metals"
RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
f Signature \
Print Name
Company
I |
Date/Time
I
i Relinquished by:
| Received by:
i Relinquished by:
| Received by:
,<,
T
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC, The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Alr) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Page:
4 of 14
I Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Company Phone/Fax
TEL : (614) 424-7358
Secondary Phone/Fax
TEL: (614) 424-3723
FAX: (614)424-3667
I FAX : _(614)_424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required: Yes
Sampled by : Client
Cooler Temp: 12 °C 22-Sep-OO
QC Level: S4
Final Rpt, MBLK. LCS, MS/MSD With Surrogates
._ ....
Alpha Client Collection No. of Bottles
Sample ID Sample 10 Matrix Date ORG SUB TAT PWS #
BMI00092241-22AJ CAD0142EMM
BMI00092241-23A
CAD01436MM
1
BMJ00092241-24AI CAD01439MM
I 1
BMI00092241-25A
JBMI00092241-26A
JBMI00092241-27A
BMI00092241-28A
CAD0143CMM
1
CAD01469MM
1
CAD0146CMM
1
CAD0146FMM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/12/00
22:46
09/12/00
23:32
09/12/00
23:34
09/12/00
23:36
09/14/00
03:33
09/14/00
03:35
09/14/00
03:37
0
0
1
1
0 ,
0
0
0
0
1
1
1
1
10
10
15-
10
,0
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As, Be, Cd.
Cr, Pb, Hg.
Ag, Sc
As, Be, Cd,
Cr.Pb,H8,
Ag,Sc
As, Be, Cd,
Cr, Pb, Hg.
Ag.Se
As.Be.Cd,
Cr, Pb, Hg,
Ag.Se
As, Be. Cd,
Cr. Pb, Hg,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg.
Ag.Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr. Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be. Cd,
Cr, Pb, Hg.
Ag, Se
As, Be, Cd,
Cr, Pb, Hg.
Ag,Se
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
I I RCRA 8 Metals
r~ i i i
[ T
i r i i
RCRA 8 Metals
"" RCRA'B Metais
RCRA 8 Metals
RCRA 8 Metals
Comments: No security seals, real and blue ice melted. Contract No. S274
j^ Signature |
i Relinquished by:
i
i Received by:
: Relinquished by:
| Received by:
Print Name
Company
Date/Time
T
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
! Alpha Analytical, Inc.
! 255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778 !
TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
5 of 14
WorkOrder: BMI00092241
i Company Phone/Fax
! TEL: (614)424-7358 i
[FAX: J614) 424-3667 |
Secondary Phone/Fax
TEL : (614) 424-3723
FAX : (614) 424-3667
Report Due By : 5:00 PM On : 06-Oct-OO
HDD Required: Yes
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
Sampled by : Client
Cooler Temp: I2°C
22-Sep-OO
QC Level: S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS#
BMI00092241-29A
BMI00092241-30A
BM100092241-31A
BMI00092241-32A
BMI00092241-33A
j BMI00092241-34A
BMI00092241-35A
CAD0147DMM
1
CAD01480MM
1
AQ I 09/14/00
I 04:52
AQ
CAD01483MM I AQ
1 I
CAD01486MM
1
CAD01489MM
1
CAD0148CMM
1
CAD0148FMM
1
AQ
AQ
AQ
AQ
09/14/00
05:00
09/14/00
05:04
09/14/00
05:13
09/14/00
05:17
09/14/00
05:24
09/14/00
05:32
0
0
0
0
0
1 I'M
1
1
1
1
0 | ,
0
1
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
At, Be, Cd,
Cr, Pb, Hg.
Ag.Se
As.Be,Cd,
Cr, Pb. Hg,
Ag.Sc
As,Be,Cd,
Cr,Pb,Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb. Hg,
' Ag, Se
As. Be. Cd,
Cr, Pb, Hg,
Ag,Se
MERCURY
As.Be.Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr,Pb,Hg,
Ag.Sc
Aj.Be.Cd,
Cr. Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Sc
Sample Remarks
RCRA 8 Metals
5
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc. !
; 255G!endale Avenue, Suite 21 Sparks, Nevada 89431-5778 |
j TEL: (775) 355-1044 FAX: (775) 355-0406
Company Phone/Fax
! TEL : (614) 424-7358
I FAX : (614) 424-3667
! j Secondary Phone/Fax
! j TEL: (614)424-3723
j IFAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
_ ...J
Page:
6 of 14
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
HDD Required: Yes
Sampled by : Client
Cooler Temp: £2°C_ 22-Sep-OO
QC Level: S4 = Final Rpt, MBLK, LCS. MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS #
BMI00092241-36A
BMI00092241-37A
BMI00092241-38A
BMI00092241-39A
BMI00092241-40A
JBMI00092241-41A
| BMI00092241-42A
i
CAD01492MM
1
CAD01495MM
1
CAD0149DMM
1
CAD014AOMM
1
CAD014A3MM
1
CAD014BFMM
1
CAD014C2MM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/14/00
05:33
09/14/00
05:39
09/14/00
06:11
09/14/00
06:13
09/14/00
06:16
09/15/00
08:45
09/15/00
08:47
0
0
0
1
1
1
0 | 1
0
0
0
1
1
1
10
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr. Pb. Hg,
Ag,Se
I As. Be, Cd.
Cr, Pb, Hg,
Ag.Se
I As,Bc,C4
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr. Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg.
Ag,Se
MERCURY
As, Be, Cd,
Cr. Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As,Be,Cd,
Cr, Pb, Hg,
Ag.Se
As.Be.Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
I I I RCRA 8 Metals
I I RCRA 8 Metals
]~ F I RCRA 8 Metals
RCRA 8 Metals
Comments;
No security seals, real and blue ice melted. Contract No. S274
Signature
I Relinquished by:
i Received by:
Relinquished by:
' Received by:
Print Name
Company Date/Time
1/22/00
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505. King Avenue
Columbus, OH 43201
Report Attention : Jennifer I ekes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
7 of 14
; Company Phone/Fax \ \ Secondary Phone/Fax
;TEL: (614)424-7358 j j TEL: (614)424-3723
:FAX: (614)424-3667 _J | FAX : (614) 424-3667
Job : MWFtA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required: Yes
Sampled by : Client
Cooler Temp: K°C 22-Sep-OO
QC Level: S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS #
JBMI00092241-43AI CAD014C5MM
' I 1
I BMI00092241-44A
i
|BMI00092241-45A
i BMI00092241-46A
[BMI00092241-47A
j BMI00092241-48A
1BMI00092241-49A
i
CAD014D4MM
1
CAD014DBMM
1
CAD014DEMM
1
CAD014E4MM
1
CAD014E7MM
1
CAD014EAMM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/15/00
08:50
09/15/00
09:52
09/15/00
09:57
09/15/00
09:59
09/15/00
10:02
09/15/00
10:06
09/15/00
10:11
0
0
0
0
0
0
0
1
1
1
1
10
10
10
10
1 I 10
1
1
10
10
Requested Tests
200_8
As. Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb. Hg,
Ag,Se
|Ai,Be,Cd,
Cr. Pb, Hg,
Ag.Se
I As, Be, Cd,
Cr, Pb. Hg.
Ag, Se
As,Be,Cd,
Cr, Pb. Hg,
Ag,Se
As.Be.Cd,
Cr, Pb, Hg,
' Ag. Sc
MERCURY
As, Be. Cd,
Cr. Pb, Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg.
Ag, Sc
As,Be,Cd,
Cr, Pb. Hg,
Ag, Sc
At.Be.Cd,
Cr, Pb, Hg,
Ag.Se
As,Be.Cd.
Cr, Pb, Hg,
Ag, Se
As.Be.Cd.
Cr, Pb, Hg,
Ag,Se
As.Be.Cd,
Cr, Pb, Hg,
Ag.Se
r i
r i i
i
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
1 ! RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
Signature
Print Name
_L
j Company J Date/Time
| Relinquished by:
; Received by:
; Relinquished by:
! Received by:
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinklng Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Batte'le Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
i
| Company Phone/Fax :
i TEL : (614) 424-7358
|_FAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
. Secondary Phone/Fax
TEL: (614)424-3723
FAX: (614)424-3667
Page:
8 of 14
WorkOrder: BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
HDD Required: Yes
Sampled by : Client
Cooler Temp : 12 °C 22-Sep-OO
QC Level: S4
= Final Rpt, MBLK. LCS. MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS #
BMI00092241-50A
BMI00092241-51A
BMI00092241-52A
IBMI00092241-53A
I
BMI00092241-54A
CAD014EDMM
1
CAD014F3MM
1
CAD014F6MM
1
CAD01511MM
1
CAD01514MM
1
[BMI00092241-55AI CAD0151AMM
I ' I 1
IBMI00092241-56A
CAD01523MM
1
AQ I 09/15/00
I 10:14
AQ
AQ
AQ
AQ
AQ
AQ
09/15/00
10:22
09/15/00
10:25
09/15/00
11:36
09/15/00
11:48
09/15/00
11:50
09/15/00
23:35
0
0
0
0
0
0
0
1
1
1
1
1
1
1
"I
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr. Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As.Be,Cd,
Cr,Pb,Hg,
Ag, Se
As. Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As. Be. Cd.
Cr. Pb, Hg,
Ag.Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be. Cd.
Cr, Pb, Hg.
Ag.Se
Sample Remarks
RCRA 8 Metals I
RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
Comments:
Relinquished by:
Received by:
Relinquished by:
i Received by:
No security seals, real and blue ice melted. Contract No. S274
Signature
Print Name
Company
Date/Time
/
/ir^Cirf..-
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be relumed to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drink!ng Water) OT(Other) Bottle Type: L-Liter V-Voa S-SoilJar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client: :
Batte'.le Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention ; Jennifer I ekes
CHAIN-OF-CUSTODY RECORD
Page:
8 of 14
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
WorkOrder: BMI00092241
I
\ Company Phone/Fax
I TEL : (614) 424-7358
[FAX: (614)424-3667
TJob : MWRA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
J
Secondary Phone/Fax
TEL: (614)424-3723
FAX: (614)424-3667
Report Due By : 5:00 PM On : 06-Oct-OO
I HDD Required : Yes
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QC Level: S4 = Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection No. of Bottles
Sample ID Sample ID Matrix Date ORG SUB TAT PWS#
BMI00092241-50AI CAD014EDMM
I 1
BMI00092241-51A
BMI00092241-52A
BMI00092241-53A
i
JBMI00092241-54A
CAD014F3MM
1
CAD014F6MM
1
CAD01511MM
1
CAD01514MM
1
[BMI00092241-55A[ CAD0151AMM
i I 1
IBMI00092241-56A
i
CAD01523MM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/15/00
10:14
09/15/00
10:22
09/15/00
10:25
09/15/00
11:36
09/15/00
11:48
09/15/00
11:50
09/15/00
23:35
0
0
0
0
0
0
0
1
1
1
1
1
1
1
10 I I
10
10
10
10
10
10
Requested Tests
200_8
As.Be.Cd,
Cr,Pb.Hg.
Ag.Se
As,Be,Cd,
Cr,Pb,Hg,
Ag, Sc
As.Be.Cd,
Cr.Pb,Hg,
Ag.Sc
As.Be.Cd.
Cr. Pb. Hg.
Ag,Se
As, Be, Cd.
Cr. Pb, Hg,
Ag.Se
As, Be, Cd.
Cr. Pb, Hg.
' Ag. Sc
As, Be, Cd.
Cr, Pb, Hg.
Ag,Se
MERCURY
As.Be.Cd,
Cr, Pb. Hg.
Ag,Se
As, Be, Cd.
Cr, Pb, Hg,
Ag,Se
As.Be.Cd.
Cr,Pb,Hg,
Ag,Sc
As, Be, Cd,
Cr, Pb. Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg.
Ag, St
As, Be. Cd.
Cr, Pb. Hg,
Ag.Se
As.Be.Cd.
Cr, Pb, Hg,
Ag,Se
[ i
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
I RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
Signature
Relinquished by:
Received by: L^ ^/{/t-C^'t'^-^C'^t
Relinquished by:
Received by:
:
Print Name j Company |
l^syi is>&^ ^b&f
/
Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Batteile
505 King Avenue
Client:
BalteHe Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778 i
i TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
9 of 14
Company Phone/Fax
! TEL: (614)424-7358
FAX: (614)424-3667
7ob":
PO:
I Secondary Phone/Fax
I TEL: (614)424-3723
FAX: (614)424-3667
WorkOrder : BMI00092241
J Report Due By : 5:00 PM On : 06-Oct-OO
MWRA Harbor and Outfall Monitoring Program
Client's COG #: none
HDD Required: Yes
Sampled by : Client
Cooler Temp: 12°C
22-Sep-OO
QC Level: S4 = Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection
Sample ID Sample ID Matrix Date
; BMIOOOS2241 -57A i CAD01 526MM
[ I 1
I BMI00092241-58A
: BMI00092241-59A
BMI00092241-60A
BMI00092241-61A
CAD01529MM
1
CAD01534MM
1
CAD01538MM
1
CAD0153BMM
1
:BMI00092241-62A| CAD0153EMM
: I 1
BMI00092241-63A
CAD01541MM
1
AQ
AQ
AQ
AQ
AQ
AQ
AQ
09/15/00
23:38
09/15/00
23:41
09/15/00
12:09
09/15/00
00:14
09/15/00
00:19
09/15/00
00:25
09/15/00
00:26
No. of
ORG
~^~l
0
0
'
0
0
0
Bottles
SUB TAT PWS #
rpy -|
1
1
1
1
1
1
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag. Se
As,Be,Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr.Pb,Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr,Pb,Hg,
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg.
Ag, Sc
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA'SMetais 1
S Sltd/a Q phcrs & '
RCRA 8 Metals
| RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
f Signature |
Print Name
Company
Dale/Time
Relinquished by:
Received by:
Relinquished by:
Received by:
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
. 505 King Avenue
Client:
Battolle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
i Alpha Analytical, Inc.
I 255Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
! TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
10 of 14
i Company Phone/Fax
JTEL: (614)424-7358
[FAXj (614)424-3667
Secondary Phone/Fax
TEL: (614)424-3723
FAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO: Client's COC #: none
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
EDO Required: Yes
Sampled by : Client
Cooler Temp : 12 °C 22-Sep-OO
QC Level; S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha Client Collection
Sample ID Sample ID Matrix Date
BMI00092241-64A
BMI00092241-65A
BMI00092241-66A
BMI00092241-67A
BMI00092241-68A
BMI00092241-69A
BMI00092241-70A
CAD01544MM
1
CAD01547MM
1
CAD0154CMM
1
CAD0154FMM
1
CAD0155EMM
1
CAD01561MM
1
CAD01564MM
1
AQ 09/15/00
I 00:31
AQ
AQ
AQ
AQ
AQ
AU
09/15/00
00:35
09/15/00
00:42
No. of Bottles
ORG SUB TAT PWS #
0 | , | 10
0
0
09/15/00 0
00:44 I
09/16/00
01:33
09/16/00
01:35
09/16/00
01:39
0
0 ~^
0
1
1
1
1
1
1
10
10
10
10
10
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As.Be,Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Sc
As,Be,Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As,Be,Cd,
Cr. Pb, Hg,
Ag, Se
As, Be, Cd,
Cr. Pb, Hg,
Ag.Se
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
"RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
Signature
Print Name
Company
Date/Time
Relinquished by:
Received by:
Relinquished by:
Received by:
_ ~_ "' .,.--.. - ,.,,. ,. ., j
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431-5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Page:
11 of 14
Company Phone/Fax
;TEL: (614)424-7358
FAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC # : none
: Secondary Phone/Fax
! TEL: (614)424-3723
i FAX : (614) 424-3667
WorkOrder : BMI00092241
Report Due By : 5:00 PM On : 06-Oct-OO
HDD Required: Yes
Sampled by : Client
Cooler Temp: 12 °C 22-Sep-OO
QC Level: S4
= Final Rpt, MBLK. LCS. MS/MSD With Surrogates
Alpha
Sample !D
;BMI00092241-71A
BM100092241-72A
Client
Sample ID
CAD012ACMM
CAD012AFMM
1
Matri
70]
AQ
BMI00092241-73A I CAD012B2MM I AQ
11 'I
BMI00092241-74A
CAD012BFMM
1
AQ
Collection
x Date
09/09/00
15:59
09/09/00
16:01
09/09/00
16:02
09/09/00
16:59
No. of Bottles
ORG SUB TAT PWS #
0
0
0 "
0
1
1
10
10
1 10
I I
p"
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr,Pb,Hg.
Ag, Se
As,Be,Cd,
Cr, Pb, Hg,
Ag, Se
As, Be, Cd,
Cr, Pb. Hg,
Ag.Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd.
Cr. Pb, Hg,
Ag.Se
As,Be,Cd,
Cr, Pb, Hg.
Ag.Se
r i
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals. Filter prior
to analysis and analyze for
aqueous and solid phase.
BMI00092241-75A | CAD012C3MM
1
AQ
09/09/00
17:03
7
1
10
As, Be, Cd,
Cr, Pb. Hg,
Ag,Se
As. Be, Cd,
Cr, Pb, Hg,
Ag, Se
RCRA 8 Metals. Filter prior
to analysis and analyze for
aqueous and solid phase.
BMI00092241-76A
BMI00092241-77A
CAD012C6MM
1
CAD012CCMM
1
AQ
AQ
09/09/00
17:05
09/09/00
17:07
°
0
1
1
10
10
As, Be, Cd,
Cr, Pb. Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be. Cd,
Cr, Pb, Hg,
Ag. Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
RCRA 8 Metals
I RCRA 8 Metals
Comments:
No security seals, real and blue ice melted. Contract No. S274
Signature
Print Name
Company
Relinquished by:
Received by:
Relinquished by:
Received by:
Date/Time
r
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information :
Baltelle
505 King Avenue
Client:
Batteiie Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Page:
14 of 14
Alpha Analytical, Inc.
255 Glendale Avenue, Suile 21 Sparks, Nevada 89431-5778
TEL: (775)355-1044 FAX: (775)355-0406'
WorkOrder : BMI00092241
| Company Phone/Fax
| TEL: (614)424-7358
i FAX : (614) 424-3667
I : Secondary Phone/Fax
' !TEL: (614)424-3723
i i FAX: (614)424-3667
Report Due By : 5:00 PM On : 06-Oct-OO
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COC #: none
EDO Required : Yes
Sampled by : Client
Cooler Temp : 12°C
22-Sep-OO
QC Level: S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha
Sample ID
BMIOOOS2241-92A"
BMI00092241-93A
BMI00092241-94A
BMI00092241-95A
BMI00092241-96A
Client Collection
Sample ID Matrix Date
CAD0132BMM I AQ
1 I
CAD0132EMM
1
CAD01331MM
1
CAD01334MM
1
CAD01337MM
1
AQ
09/10/00
09:11
09/10/00
09:12
No. of Bottles
ORG SUB TAT
0
0
1 ^10
1
AQ I 09/10/00 I 0 I . 1
I 09:26 I i
AQ
AQ
09/10/00
09:28
0
09/10/00 I 0
09:34 I
'
1
10
10
10
10
PWS#
Requested Tests
200_8
As.Be.Cd,
Cr, Pb, HE,
Ag, Se
As,Be,Cd,
Cr. Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, HE,
Ag.Se
As, Be. Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, HE,
Ag.Se
MERCURY
As, Be. Cd.
Cr, Pb, HE,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg,
Ag.Se
As.Be.Cd,
Cr, Pb, Hg,
Ag.Se
As. Be, Cd,
Cr, Pb, Hg,
Ag,Se
As,Be.Cd,
Cr, Pb, HE,
Ag.Se
r '
r~ f
r i
r i
Sample Remarks
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
Relinquished by:
Received by:
Relinquished by:
Received by:
No security seals, real and blue ice melted. Contract No. S274
[ Signature 1
Print Name ~[
Company
Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type : AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
* Also please include the dates of analysis and detection limits.
Page of ,
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BMI00092241-01A CAD01021MM1
BMI00092241-02A CA001024MM1
BM100092241-03A CAD01027MM1
BMI00092241-04A CAD0102AMM1
BMI00092241-05A CAD0102DMM1
BMI00092241-06A CAD0104AMM1
BMI00092241-07A CAD0104DMM1
BMI00092241-08A CAD01050MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/06/00
12:23
Aqueous 09/06/00
12:24
Aqueous 09/06/00
12:25
Aqueous 09/06/00
12:27
Aqueous 09/06/00
12:32
Aqueous 09/06/00
14:13
Aqueous 09/06/00
14:14
Aqueous 09/06/00
14:18
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER ())
OTHER (1)
OTHER (1)
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.6
(200.8)
EDO Required: rmai Kpl' mBLK' LU>' MS
Yes
Requested Tests
SVY7470
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MSD With Surrogates
22-Sep-OO
Comments
RCRA 8 Metals
RCRA 8 Metals
RCRA 6 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
CA samples. Note comment on -74 and -75.
Relinquished by:
Relinquished by:
I Date/Time ~|
1 . .. I
Received by:
Received by:
-------
Alpha Analytical, Inc.
255 Glcmlale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample 10 Client's Sample 10 Matrix
BMI00092241-09A CAD01053MM1 Aqueous
BMI00092241-10A CAD01056MM1 Aqueous
BMI00092241-11A CAD01405MM1 Aqueous
BMI00092241-12A CAD0140BMM1 Aqueous
BMI00092241-13A CAD0140BMM1 Aqueous
BMI00092241-14A CAD01416MM1 Aqueous
BMI00092241-1SA CAD01419MM1 Aqueous
BMI00092241-16A CAD0141CMM1 Aqueous
Comments:
Relinquished by:
Relinquished by:
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.*) of Bottles
Date Sulfurlc Nitric Other
09/06/00
14:22
09/06/00
1424
09/12/00
21:35
09/12/00
21:36
09/12/00
21:38
09/12/00
22:14
09/12/00
22:17
09/12/00
2220
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
[. _ r
Uate/li
FDD Rpnnirptt wioi-rv, LOO, mo/mou wim surrogates
Yes
22-Sep-OO
Requested Tests
E2Q0.8 SW7470
Comments
Inorganics by EPA MERCURY. Total RCRA 8 Melals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA a Melals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA 8 Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total RCRA B Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA 8 Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA 8 Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total RCRA 8 Metals
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total RCRA 8 Melals
Method 200.8 (MERCURY)
(200.8)
f
me ~]~ - ' ..._.. ._. I" Date/Time ~|
/J>y,> Received by: yfi£/£. ^L^^tl- /~2'2,-ff^ // ' fy ' f
Received by:
_ ...
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*AIso please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample 10 Client's Sample ID Matrix
BMI0009224M7A
BMI00092241-18A
BMI00092241-19A
BMI00092241-20A
BMI00092241-21A
BMI00092241-22A
BMI00092241-23A
BMI00092241-24A
CAD0141FMM1 Aqueous
CAD01422MM1 Aqueous
CAD01425MM1 Aqueous
CAD01428MM1 Aqueous
CAD0142BMM1 Aqueous
CAD0142EMM1 Aqueous
CAD01436MM1 Aqueous
CA001439MM1 Aqueous
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type ( *) of Bottles
Dale Sulfurlc Nitric Other
09/12/00
22:24
09/12/00
22:29
09/12/00
22:36
09/12/00
22:37
09/12/00
22:45
09/12/00
22:46
09/12/00
23:32
09/12/00
23:34
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
pp. p. p i ' '"<" '»r"-i "lui-i^i i-v-o, mo/mou »mii ounuycues
Yes
22-Sep-OO
E200.B
Inorganics by EPA
Melhod 200.8
(200.8)
Inorganics by EPA
Melhod 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Melhod 200.8
(200.8)
Inorganics by EPA
Melhod 200.8
(200.8)
Inorganics by EPA
Melhod 200.8
(200.8)
Requested Tests
SW7470
Comments
MERCURY, Total RCRA 8 Metals
(MERCURY)
MERCURY. Total ' RCRA 8 Metals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Metals
(MERCURY)
MERCURY, Total RCRA 8 Melals
(MERCURY)
MERCURY, Total RCRA 8 Metals
(MERCURY)
MERCURY, Total RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Metals
(MERCURY)
Comments:
CA samples.
Relinquished by:
Relinquished by:
Date/Time J - -
Received by:
Received by:
Date/Time
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 894 31-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID
BMI00092241-25A
BMI00092241-26A
BMI00092241-27A
BMI00092241-28A
BMI00092241.-29A
BMI00092241-30A
BMI00092241-31A
BMI00092241-32A
Client's Sample ID
CADOH3CMM1
CAD01469MM1
CADOH6CMM1
CAD0146FMM1
CAD0147DMM1
CA0014BOMM1
CA001483MM1
CAD01486MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date SuKurlc Nitric Other
Aqueous 09/12/00
23:36
Aqueous 09/14/00
03:33
Aqueous 09/14/00
03:35
Aqueous 09/14/00
03:37
Aqueous 09/14/00
04:52
Aqueous 09/14/00
05:00
Aqueous 09/14/00
05:04
Aqueous 09/14/00
05:13
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
._,_.._. _. . . i iiiui I\UL, mui_r\, L.OO, moimou ««mi ouiiuudlUb
EDO Required: y
Yes
22-Sep-OO
E200.B
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
Comments
MERCURY. Total RCRA 8 Metals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY, Total RCRA B Melals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY, Total RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY, Total RCRA 8 Melals
(MERCURY)
Comments:
CA samples.
Relinquished by:
Relinquished by:
Date/Time [ -
'"^L'-^-L I ^Jt"~ Received by:
Received by:
Date/Time ]
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
1'lione; (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample 10 Client's Sample ID
BMI00092241-33A CAD01489MM1
BMI00092241-34A CAD0148CMM1
BM 100092241 -35 A CAD0148FMM1
BMI00092241-36A CAD01492MM1
BMI00092241-37A CAD01495MM1
BMI00092241-38A CAD01490MM1
BMI00092241-39A CAD014AOMM1
BMI00092241-40A CAD014A3MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.*) of Battles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/14/00
05:17
Aqueous 09/14/00
0524
Aqueous 09/14/00
05:32
Aqueous 09/14/00
05:33
Aqueous 09/14/00
05:39
Aqueous 09/14/00
06:1 1
Aqueous 09/14/00
08:13
Aqueous 09/14/00
06:16
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
rpip, p < j. rinai r\pi, uiourv, LI/O, motiviou vvuii ourrogaies
Yes
22-Sep-OO
E200.8
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
Comments
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY, Total . RCRA 8 Metals
(MERCURY)
MERCURY. Total RCRA 8 Metals
(MERCURY)
MERCURY. Total RCRA 8 Metals
(MERCURY)
MERCURY, Total RCRA 8 Melals
(MERCURY)
MERCURY. Tolal RCRA B Melals
(MERCURY)
MERCURY, Total RCRA 8 Metals
(MERCURY)
MERCURY, Tolal RCRA 8 Metals
(MERCURY)
Comments;
CA samples.
Relinquished by:
Relinquished by:
; /
Date/Time h
j(y Received by:
Received by:
Date/Time ~[
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
Sierra Environmental Monitoring
1135 Financial Blvd.
Reno, NV 89502
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
TEL: (702) 857-2400
FAX: (702) 857-2404
Acct#:
EDO Required:
Yes
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Final Rpt, MBLK, LCS, MS/MSD With Surrogates
22-Sep-OO
Alpha's Sample ID
BMI00092241-41A
Collection
Client's Sample ID Matrix Date
CAD014BFMM1 Aqueous 09/15/00
08:45
Type (.#) of Bottles
Sulfurlc Nitric Other
OTHER (1)
E200.8
Inorganics by EPA
Method 200.6
(200.8)
Requested Tests
SW7470
MERCURY. Total
(MERCURY)
Comments
RCRA 8 Melals
BMI00092241-42A
BMI00092241-43A
BMI00092241-44A
CAD014C2MM1
CAD014C5MM1
CA0014D4MM1
Aqueous 09/15/00
06:47
BMI00092241-4SA
CAD014DBMM1
Aqueous 09/15/00
08:50
Aqueous 09/15/00
09:52
Aqueous 09/15/00
09:57
BM 100092241 -46 A
CAD014DEMM1
Aqueous 09/15/00
09:59
BM 100092241 -47 A
BMI00092241-48A
Comments:
CAD014E4MM1
CAD014E7MM1
CA samples.
Aqueous 09/15/00
10:02
Aqueous 09/15/00
10:06
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.6
(200.6)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.6
(200.8)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
RCRA 8 Melals
RCRA 8 Melals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Melals
Relinquished by:
Relinquished by:
[ Date/Time ^J
~L~ Received by:
Received by:
Date/Time
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*AIso please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BM100092241-49A CAD014EAMM1
BMI00092241-50A CAD014EDMM1
BMI000922-I1-51A CAD014F3MM1
BMI00092241-52A CAD014F6MM1
BMI00092241-53A CAD01511MM1
BMI00092241-54A CAD01S14MM1
BM 10009224 1-5SA CAD0151AMM1
BMI00092241-56A CAD01523MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/15/00
10:11
Aqueous 09/15/00
10:14
Aqueous 09/15/00
10:22
Aqueous 09/15/00
10:25
Aqueous 09/15/00
11:36
Aqueous 09/15/00
11:48
Aqueous 09/15/00
11:50
Aqueous 09/15/00
23:35
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
EDO Required: H> "' "^ 1VI°
Yes
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.B)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
MERCURY. Tolal
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Tolal
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
iviou vviui surrogates
22-Sep-OO
Comments
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
CA samples.
Relinquished by:
Relinquished by:
Date/Time
Received by:
Received by:
Date/Time ]
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone:' (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID
BMI00092241-57A
BMI00092241-56A
BMI00092241-59A
BMI00092241-60A
BMI00092241-61A
BMI00092241-62A
BMI00092241-63A
BMI00092241-64A
Client's Sample ID
CAD01526MM1
CAD01529MM1
CAD01534MM1
CA001538MM1
CA00153BMM1
CAD0153EMM1
CAD01541MM1
CAD01544MM1
Matrix
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (Jf) of Bottles
Date Sulfurlc Nitric Other
09/15/00
23:38
09/15/00
23:41
09/15/00
12:09
09/15/00
00:14
09/15/00
00:19
09/15/00
00:25
09/15/00
00:26
09/15/00
00:31
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
EDO Required:
Yes
£200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.6
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
HIVJU torn ouiiuymes
22-Sep-OO
Comments
RCRA 8 Metals
RCRA 8 Melals
RCRA 8 Melals
RCRA 8 Melals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Melals
RCRA 8 Metals
Comments:
CA samples.
Relinquished by:
Relinquished by:
..... ---- [_ Date/Time j ---
^
Received by:
Date/Time "]-
-------
Alpha Analytical, Inc.
255 Gleiulalc Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*PIease reference the Work Order number on all reports and invoices.
* Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno. NV 89502
Alpha's Sample ID Client's Sample ID
BM I0009224 1-65 A CAD01547MM1
BMI00092241-66A CAD0154CMM1
BMI00092241-67A CA00154FMM1
BMI00092241-68A CA00155EMM1
BMI00092241-69A CAD01561MM1
BMI00092241-70A CAD01564MM1
BMI00092241-71A CA0012ACMM1
BMI00092241-72A CA0012AFMM1
Comments: CA samples.
! Relinquished by:
: Relinquished by:
TEL: (702)857-2400 EDO Required: Hl ' ' ' min aurr°9ates
FAX: (702)857-2404 Yes
Acct#: 22-Sep-OO
Requested Tests
Collection Type ( *) of Bottles
E200.8 SW7470
Matrix Data Sulfurlc Nitric Other . Comments
Aqueous 09/15/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Metals
00:35 Method 200.6 (MERCURY)
(200.8)
Aqueous 09/15/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Melals
00:42 Method 200.6 (MERCURY)
(200.8)
Aqueous 09/15/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Metals
00:44 Method 200.8 (MERCURY)
(200.8)
Aqueous 09/16/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA B Melals
01:33 Method 200.8 (MERCURY)
(200.6)
Aqueous 09/16/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Metals
01:35 Method 200.8 (MERCURY)
(200.8)
Aqueous 09/16/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Melals
01:39 Method 200.8 (MERCURY)
(200.8)
Aqueous 09/09/00 OTHER (1) Inorganics by EPA MERCURY, Total RCRA 8 Melals
15:59 Method 200.8 (MERCURY)
(200.8)
Aqueous 09/09/00 OTHER (1) Inorganics by EPA MERCURY. Total RCRA 8 Melals
16:01 Method 200.8 (MERCURY)
(200.8)
] uaie/iime j . -- ........ Date/Time
, : , ^7/f'/ ?7 ' / *f <,^ 1
..:.... >.,:-»^ "/'^/."i. /^y-> Received by: //£/£ /^i*^£^- /^32 -
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
Sierra Environmental Monitoring
1135 Financial Blvd.
Reno, NV 89502
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*AIso please include the dates of analysis and detection limits.
TEL: (702)857-2400
FAX: (702) 857-2404
Acct#:
EDO Required:
Yes
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Final Rpt, MBLK, LCS, MS/MSD With Surrogates
22-Sep-OO
Alpha's Sample ID
BMI00092241-73A
Collection
Client's Sample 10 Matrix Date
CAD012B2MM1 Aqueous 09/09/00
16:02
Type (.*) of Bottles
Sulfurlc Nitric Other
OTHER (1)
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Requested Tests
SW7470
MERCURY, Total
(MERCURY)
Comments
RCRA B Metals
BMI00092241-74A
BMI00092241-75A
BMI00092241-7SA
BMI00092241-77A
BMI00092241-78A
BMI00092241-79A
BMI00092241-80A
CAD012BFMM1
CAD012C3MM1
CAD012C6MM1
CAD012CCMM1
CA0012CFMM1
CAD01202MM1
CAD012D6MM1
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
Aqueous
09/09/00
16:59
09/09/00
17:03
09/09/00
17:05
09/09/00
17:07
09/09/00
17:10
09/09/00
17:12
09/09/00
17:17
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.6)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY, Total
(MERCURY)
RCRA 8 Metals. Filter prior to
analysis and analyze for aqueous
and solid phase.
RCRA 8 Metals. Filter prior lo
analysis and analyze for aqueous
and solid phase.
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
CA samples.
| Relinquished by:
i Relinquished by:
[ Date/Time J-- .
V'"li!i-*-l.._jL?_irl-:i Received by:
_ Received by:
[ Date/Time J-
-------
Alpha Analytical, Inc.
255 Gleiulale Avenue
Suile21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*PIease reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID
BMI00092241-81A
BMI00092241-82A
BMI00092241-B3A
BMI00092241-84A
BMI00092241-85A
BMI00092241-86A
BMI00092241-B7A
BMI00092241-8BA
Client's Sample 10
CAD012DCMM1
CA0012EOMM1
CAD012ECMM1
CAD012FOMM1
CAD012F4MM1
CAD0130CMM1
CAD0130FMM1
CAD01312MM1
TEL:
FAX:
Acctft
(702) 857-2400
(702) 857-2404
Collection Type (j») of Bottles
Matrix Date Sulturlc Nitric Other
Aqueous 09/09/00
17:23
Aqueous 09/09/00
1725
Aqueous 09/09/00
18;33
Aqueous 09/09/00
18:37
Aqueous 09/09/00
18:42
Aqueous 09/10/00
07:19
Aqueous 09/10/00
07:22
Aqueous 09/10/00
07:28
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
EDO Required: Hl ' ' '
Yes
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.B)
Requested Tests
SW7470
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Tolal
(MERCURY)
MERCURY. Total
(MERCURY)
MERCURY, Total
(MERCURY)
mou man ouiiuycntib
22-Sep-OO
Comments
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
RCRA 8 Metals
Comments:
CA samples.
Relinquished by:
Relinquished by:
- I Date/Time ] ;
//'"...-'.ViVt:- /.>'/- Received by:
Received by:
[ Date/Time _]-
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
I'lione:- (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page
of
Report Due By : 5:00 PM
On : 06-Oct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
BMI00092241-89A CAD0131FMM1
BMI00092241-90A CA001322MM1
BMI00092241-91A CAD01325MM1
BMI00092241-92A CAD0132BMM1
BM I0009224 1-93 A CAD0132EMM1
BMI00092241-94A CAD01331MM1
BMI00092241-95A CAD01334MM1
BMI00092241-96A CAD01337MM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type (.#) of Bottles
Matrix Date Sulfurlc Nitric Other
Aqueous 09/10/00
08:51
Aqueous 09/10/00
08:54
Aqueous 09/10/00
06:59
Aqueous 09/10/00
09:11
Aqueous 09/10/00
09:12
Aqueous 09/10/00
09:26
Aqueous 09/10/00
09:28
Aqueous 09/10/00
09:34
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
Fnn RP i H- v ' IVIDLIX| LUO' l"a"₯iau vvlin ourrogar.es
Yes
22-Sep-OO
E200.8
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200.8
(200.8)
Inorganics by EPA
Method 200:8
(200.8)
Inorganics by EPA
Method 200.8
(200.6)
Requested Testa
SW7470
Comments
MERCURY. Total RCRA B Mela,s
(MERCURY)
MERCURY. Total . RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Metals
(MERCURY)
MERCURY, Total RCRA 8 Metals
(MERCURY)
MERCURY, Tolal RCRA 8 Melals
(MERCURY)
MERCURY. Total RCRA 8 Melals
(MERCURY)
MERCURY, Tolal RCRA 8 Melals
(MERCURY)
MERCURY, Total RCRA 8 Metals
(MERCURY)
Comments:
CA samples.
Relinquished by:
Relinquished by:
_P_ate/Time |
"];.:-,;/ *:. * /'...'> / - Received by:
't
Received by:
[ Date/Time J-
-------
Alpha Analytical, Inc.
255 Glcndiilc Avenue
Suilc21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0-106
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00092241
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page of
Report Due By : 5:00 PM
Qn : 06-Qct-OO
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID Client's Sample ID
UMKJ0092241-29A CAD014/OMM1
BMI00092241-44A CA0014D-!MM1
OMI00092241-I5A CA0014DBMMI
BMIOB092241-59A CAU01S34MM1
TEL:
FAX:
Acct#:
(702)857-2400
(702)857-2404
Collection Typ«(*)o(Boti|ei
Matrix Date Sullurlc Nitric Other
Aqueous 09/14/00
04:52
Aqueous 09/15/00
09.52
Aqueous OS/15/00
09:57
AquJOuS 09/1 5/UO
12:09
OTHER (1)
OTHER (1)
OTHER (1)
OTHER (1)
E200.S
Inorganics; by EPA
Meihod 200.8
(200.6)
Inorganics" by EPA
Meihod 200 8
(200.B)
Inorganics by EPA
Method 200 8
(2008)
inorganics by EPA
Method 200.8
(200.6)
EDO Requirecj:
Yes
Requested Tests
SW7470
MERCURY, Tdal
(MbRCURY)
MERCURY. Total
(MERCURY)
MERCURY, Toial
(MERCURY)
MERCURY. Total
(MERCURY)
final Kpt, NIBLK, LUS, MSfMSp With Surrogates
26-Sep-OO
1 I
i
i
Comments
RCRA8Mcla!s f t(er prior to
analysis and analyze (or aqueous
tmd solid ph$sa.
RCRA6Mala!£ Filler prior to
analysis and analyze for aqueous
and SQbd phase.
RCRABMelalG Filler prior to
analysis and analyze lor aqueous
and solid phase.
RCRASMplals t-7lor prior lo
analysis and analyze (or aqueous
and solid phase.
Comments: Amended COG. These 4.«amfefttf samples need to be analysed for tlic aqueous and solid phis
I Relinquished by:
I Relinquished by:
§ Received by:
Received by:
[^ Date/Time J-
-------
Billing Information :
Ballelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus, OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Company Phone/Fax
TEL : (614) 424-7358
FAX : (614) 424-3667
Secondary Phone/Fax
TEL : (614) 424-3723
FAX: (614)424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO: Client's COG #: none
Page:
1 of 2
WorkOrder : BMI00101664
Report Due By : 5:00 PM On : 30-Oct-OO
EDD Required: Yes
Sampled by: Client
Cooler Temp: 4 °C 16-Oct-OO
QC Level: S4
= Final Rpt, MBLK, LCS, MS/MSD With Surrogates
Alpha
Sample ID
BMI00101664-01A
Client Collection
Sample ID Matrix Date
CAD01610MM A
1
3 09/28/00
09:22
No. of Bottles
ORG SUB TAT PWS #
1 I 0
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag,Sc
Sample Remarks
RCRA8
Metals.subcontracted to
SEM.
BMI00101664-02A
BMI00101664-03A
BMI00101664-04A
BMI00101664-05A
CAD01613MM
1
CAD01616MM
1
CAD1619MM1
I CAD0161CMM
I 1
AQ
AQ
AQ
AQ
09/28/00
09:26
09/28/00
09:29
09/28/00
09:32
09/28/00
09:35
1
1
1
1
0
0
0
0
10
10
10
10
As, Be, Cd,
Cr,Pb,Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As. Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
RCRA8
Metals.subcontracted to
SEM.
RCRA8
Metals, subcontracted to
SEM.
RCRA8
Melals.subcontracted to
SEM.
RCRA8
Metals.subcontracted to
SEM.
Comments:
No security seals preset. Blue and real ice frozen. Contract No.S274. RCRA 8 metals for all samples.subcontracted to SEM.
Signature
Print Name
Company
Date/Time
Relinquished by:
Received by:
Relinquished by:
Received by:
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Olher) Bottle Type: L-Liter V-Voa S-Soil Jar 0-Orbo T-Tedlar B-Brass P-Plastic OT-Other
-------
Billing Information:
Battelle
505 King Avenue
Client:
Battelle Memorial Institute
505 King Avenue
Columbus. OH 43201
Report Attention : Jennifer Ickes
CHAIN-OF-CUSTODY RECORD
Alpha Analytical, Inc.
255 Glendale Avenue, Suite 21 Sparks, Nevada 89431 -5778
TEL: (775) 355-1044 FAX: (775) 355-0406
Company Phone/Fax
TEL : (614) 424-7358
FAX: (614)424-3667
Secondary Phone/Fax
TEL : (614) 424-3723
FAX : (614) 424-3667
Job : MWRA Harbor and Outfall Monitoring Program
PO : Client's COG # : none
Page:
2 of 2
WorkOrder : BMI00101664
Report Due By : 5:00 PM On : 30-Oct-OO
EDD Required: Yes
Sampled by : Client
Cooler Temp: 4 °C 16-Oct-OO
QC Level: S4 = Final Rpt, MBLK, LCS. MS/MSD With Surrogates
Alpha
Sample ID
BMI00101664-06A
Client
Sample ID
CAD01620MM
1
Collection
Matrix Date
AQ
09/28/00
09:38
No. of Bottles
ORG SUB TAT PWS #
1
0
10
Requested Tests
200_8
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
MERCURY
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
Sample Remarks
RCRA8
Metals, subcontracted to
SEM.
BMI00101664-07A
BMI00101664-08A
BMI00101664-09A
BMI00101664-10A
CAD01623MM
1
CAD01626MM
1
CAD01629MM
CAD0162CMM
I 1
AQ
AQ
AQ
AQ
09/28/00
09:41
09/28/00
09:44
09/28/00
09:47
09/28/00
09:50
1
1
1
1
0
0
0
0
10
10
10
10
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr,Pb,Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr,Pb,Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag.Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
As, Be, Cd,
Cr, Pb, Hg,
Ag,Se
RCRA 8
Metals.subcontracted to
SEM.
RCRA 8
Metals.subcontracted to
SEM.
RCRA 8
Metals.subcontracted to
SEM.
RCRA 8
Metals, subcontracted to
SEM.
Comments:
Relinquished by:
Received by:
Relinquished by:
Received by:
No security seals preset. Blue arid real ice frozen. Contract No.S274. RCRA 8 metals for all samples.subcontracted to SEM.
Signature
Print Name
Company
U
Date/Time
NOTE: Samples are discarded 60 days after results are reported unless other arrangements are made. Hazardous samples will be returned to client or disposed of at client expense.
The report for the analysis of the above samples is applicable only to those samples received by the laboratory with this COC. The liability of the laboratory is limited to the amount paid for the report.
Matrix Type: AQ(Aqueous) AR(Air) SO(Soil) WS(Waste) DW(Drinking Water) OT(Other) Bottle Type: L-Liter V-Voa S-Soil Jar O-Orbo T-Tedlar B-Brass P-Plaslic OT-Other
-------
Alpha Analytical, Inc.
255 Glendale Avenue
Suite 21
Sparks, Nevada 89431-5778
Phone: (775)355-1044
Fax: (775) 355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00101664
*PIease reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
Page j of '~\J
Report Due By : 5:00 PM
On : 10/30/00
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample 10
BMI00101664-01A
BMI00101664-04A
BMI00101664-05A
Client's Sample 10
CAD01610MM1
CAD01613MM1
CA001616MM1
CAD1619MM1
CAD0161CMM1
CAD01620MM1
CAD01623MM1
TEL: (702) 857-2400
FAX: (702) 857-2404
Acct#:
Collection Type ( #) of Bottles
Matrix Date Sulfurlc Nitric Other
09:22
Aqueous 09/28/00
09:26
Aqueous 09/26/00
09:29
Aqueous 09/28/00
09:32
Aqueous 09/28/00
09:35
Aqueous OS/28/00
09:38
Aqueous 09/28/00
09:41
Aqueous 09/28/00
09:44
EDO Required" F'nal Rpt< MBLK> LCS' MS/MSD With Surrogates
Yes
16-Oct-OO
Requested Tests
E200.8 SW7470
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total ' ~
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY. Total
Method 200.B (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200,8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total "
Method 200.8 (MERCURY)
(200.8)
Inorganics by EPA MERCURY, Total
Method 200.8 (MERCURY)
(200.B)
Comments
RCRA B Metals.subconlracled to
SEM.
RCRA 8 Metals.subconlracted to
SEM.
RCRA 8 Metals.subconlracted to
SEM.
RCRA 8 Metals.subconlracled lo
SEM.
RCRA 8 Melals.subconlracted to
SEM.
RCRA 8 Metals.subcontracled to
SEM.
RCRA 8 Melals.subcontracted lo
SEM.
RCRA B Metals.subconlracled lo
SEM.
Comments:
200.8=RCRA 8 metalsfAs.Be.Cd.Cr.Pb.Hg.Ag.Se^
Relinquished by:
Date/Time
ReceivedV
Received by:
pate/Time
-------
Alpha Analytical, Inc.
255 Gluiulale Avenue
Suilc2l
Sparks, Nevada 8^-131-5778
Phone: (775) 355-1044
Fax: (775)355-0406
Subcontractor:
SUB CHAIN-OF-CUSTODY RECORD
Work Order: BMI00101664
*Please reference the Work Order number on all reports and invoices.
*Also please include the dates of analysis and detection limits.
of
Report Due By : 5:00 PM
On : 10/30/00
Required QC:
Sierra Environmental Monitoring
11 35 Financial Blvd.
Reno, NV 89502
Alpha's Sample ID
BMI00101664-09A
Client's Sample ID
CAD01629MM1
CAD0162CMM1
TEL:
FAX:
Acct#:
(702) 857-2400
(702) 857-2404
Collection Type ( ») of Bottles
Matrix Date Sulfurlc Nitric Other
09:47
Aqueous 09/26/00
EDO Required: Final Rpt< MBLKl LCS' MS/MSD With Su"°gates
Yes
16-Oct-OO
Requested Tests
E200.8 SW7470
Inorganics by EPA MERCURY, Tolal
Melhod 200.8 (MERCURY)
(200.8)
Inorganics bv EPA MERCURY Tmai
Comments
RCRA 8 Melals.subconlracted lo
SEM.
09:50
Melhod 200.8 (MERCURY)
(200.8)
RCRA 8 Metals,subcontracted to
SEM.
Comments: 200.8=RCRA 8 metals(As.Be,Cd,Cr.Pb.llx,Ag,Se)
, r, 1 i "' Date/Timp 1 ^ X
Relinquished byt . , ' \M.' .( Qji /> -v r? /T'X'r /f^>///s'/V) n j i.
1 J v-^:- v~ V .- V'-'-^-'f ^ ( ^- V- ^ t^'/tvZLfy Received by: - ^
Relinquished by: n . , , / /
1 J Received by: / /
'""^X o Date/Time
'^{)/n*Ji$ (A }(\1(fx /((/Vl^ /S"t/|
' '^/ : "
-------
MWRA Harbor and Outfall Monitoring Program
Contract No. S274
Chain-of-Custody Form
Today's Date : 9/28/00 10:08:51 AM
Chaln-of-Custody #: CAD01-MM-0500
Survey ID: CAD01
Analysis ID: MM
Analysis Description : Major metals
Laboratory : Alpha Analytical, Inc.
(Phone)
(Fax)
Bottle ID:
Bottle ID:
Sampling Date:
Station ID:
Ck1 Ck2 Ck3 Ck4
CAD01610MM1
9/28/00 9:22:57 AM
1F
-CO CAD01613MM1
-0 CAD01616MM1
9/28/00 9:26:31 AM 2H
9/28/00 9:29:35 AM 3F
~.<)y CAD01619MM1
-0£-CAD0161CMM1
9/28/00 9:32:41 AM 4F
9/28/00 9:35:47 AM 5H
Q
_£)/ CAD01620MM1
-A-, CAD01623MM1
9/28/00 9:38:53 AM 6H
9/28/00 9:41:42 AM 7F
CAD01626MM1
9/28/00 9:44:29 AM 8H
9/28/00 9:47:23 AM 9F
9/28/00 9:50:26 AM 10H
Q o CAD01629MM1
~/<5 CAD0162CMM1
2£±
Shipping Condition - Room Temperature:.
Received Condition - Room Temperature:.
Cold(ice):.
Cold(ice):.
-7
Frozen(dry ice):
Frozen(dry ice):
linquished By / Date / Time / Company J Transport-Airbill #
Received By / Date / Time / Company
v/
I/ tO- V:5/Ag^s,
Page 1 of 1
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX C
QUALITY CONTROL REPORTS
-------
-------
HBattelle
. . . Putting Technology To Work
Duxbury Operations
397 Washington Street
Duxbury, Massachusetts 02332
Telephone 781-934-0571
Fax:781-934-2124
August 27,2001
Jennifer Ickes
Battelle Memorial Institute
Columbus, OH
Subject: Delivery of QC Deliverable from Battelle Duxbury' s WA3-26: Boston Cap Project for
PAH/ECD/TPH Analyses
Dear Jennifer:
This letter provides a summary of the data quality for analyses Battelle's Duxbury Operations (EDO) has
performed in order to determine the concentrations of TPH, PCB, and PAH analytes from the analytical task:
WA3-26: Boston Cap Project.
WA3-26: Boston Cap Project
Samples were safely received at our lab on September 2000. A total of 5 sediment samples, 148 water samples,
and 9 filter samples, along with the appropriate quality control (QC) samples, were processed and analyzed in
12 analytical batches for both 8270M (PAH), 8081M (PCB) and 8015M (TPH) analyses (as defined in the
Project's QAPP).
Sample extractions and handling went smoothly
All of these data have been thoroughly reviewed and validated by EDO's independent Quality Assurance Unit,
as well as by staff of the chemistry department, as per the Project QAPP.
Specific Quality Control Sample Information
The quality control (QC) sample data quality objectives (DQOs) were largely met for this project, thereby
supporting the overall reliability and quality of the reported data. The overall data set was excellent. There are
isolated exceedences with some of the analyses, however there is no impact on the overall quality of the data.
Below is a listing and discussion of the QC for the data set.
All samples:
Sample Holding Times. All sample holding times were met.
There were 63 QC criteria of 3438 QC data points outside of acceptance criteria.
-------
PCB data:
Procedural (Method) Blanks. A method or procedural blank (PB) was processed and analyzed with each
analytical batch of samples. The PB's data quality objectives (DQOs) were consistently met as defined in
the Project QAPP.
Laboratory Control Sample Recovery. A laboratory control sample (LCS) was processed and analyzed
with each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8081M analyses as defined in the Project QAPP.
Matrix Spike Recovery and Precision. One matrix spike (MS) sample was processed with the field samples
in each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8081M analyses as defined in the Project QAPP.
Internal Standard Recoveries. Surrogate internal standards (SIS) and recovery internal standard
compounds (RIS) were added to each field and QC sample to monitor the sample processing efficiency.
For samples analyzed by 8081M, surrogate recoveries were within criteria in all but 5 samples. Four of the
five samples had artificially high surrogate recoveries, which was due to an interfering, unidentified
compound(s) that co-eluted with the surrogates. The fifth sample had a low surrogate recovery and was
noted in the sample preparation records.
Sample Duplicates. A sample duplicate (DUP) was processed and analyzed with each analytical batch of
samples. The DUP's data quality objectives (DQOs) were consistently met as defined in the Project QAPP.
There were 9 QC criteria of 950 QC data points outside of acceptance criteria.
PAH data:
Procedural (Method) Blanks. A method or procedural blank (PB) was processed and analyzed with each
analytical batch of samples. The PB's data quality objectives (DQOs) were consistently met as defined in
the Project QAPP with one exception. The PB in Batch #00-407 was contaminated. There was no sample
left for re-extraction, however all other QC data was excellent including the LCS and MS, and the water
data was consistent with those found in other batches.
Laboratory Control Sample Recovery. A laboratory control sample (LCS) was processed and analyzed
with each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8270M analyses as defined in the Project QAPP with one exception. There was 127% recovery of
fiuoranthene in Batch #00408. This appears to be an isolated incident and should have no impact on the
data.
Matrix Spike Recovery and Precision. One matrix spike (MS) sample was processed with the field samples
in each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8270M analyses as defined in the Project QAPP.
Internal Standard Recoveries. Surrogate internal standards (SIS) and recovery internal standard
-------
compounds (RIS) were added to each field and QC sample to monitor the sample processing efficiency.
For samples analyzed by 8270M, surrogate recoveries were within criteria in all but 10 samples. X8602
had a low naphthalene-d8 recovery, which is usually indicative of rapid concentration. The other surrogates
were just outside of acceptance criteria. The data are not impacted by these exceedences.
Sample Duplicates. A sample duplicate (DUP) was processed and analyzed with each analytical batch of
samples. The DUP's data quality objectives (DQOs) were consistently met as defined in the Project QAPP
with a few isolated exceptions. The data are not impacted by these exceedences.
There were 45 QC criteria of 2261 QC data points outside of acceptance criteria.
TPHdata:
Procedural (Method) Blanks. A method or procedural blank (PB) was processed and analyzed with each
analytical batch of samples. The PB's data quality objectives (DQOs) were consistently met as defined in
the Project QAPP.
Laboratory Control Sample Recovery. A laboratory control sample (LCS) was processed and analyzed
with each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8015M analyses as defined in the Project QAPP with some exceptions. Two of the LCS samples had
some analytes outside of criteria. The data are not impacted by these exceedences.
Matrix Spike Recovery and Precision. One matrix spike (MS) sample was processed with the field samples
in each analytical batch of samples. The target compound recoveries consistently met the DQOs for both
the 8015M analyses as defined in the Project QAPP with two exceptions. Two of the MS samples had one
analyte outside of criteria each.
Internal Standard Recoveries. Surrogate internal standards (SIS) and recovery internal standard
compounds (RIS) were added to each field and QC sample to monitor the sample processing efficiency.
For samples analyzed by 8015M, surrogate recoveries were within criteria in all but 5 samples. Four of the
five samples had artificially high surrogate recoveries, which was due to an interfering, unidentified
compound(s) that co-eluted with the surrogates. The fifth sample had a low surrogate recovery and was
noted in the sample preparation records.
Sample Duplicates. A sample duplicate (DUP) was processed and analyzed with each analytical batch of
samples. The DUP's data quality objectives (DQOs) were consistently met as defined in the Project QAPP.
There were 9 QC criteria of 227 QC data points outside of acceptance criteria.
Please do not hesitate to give us a call if you would like to discuss these data or if I can provide any further
assistance.
Sincerely,
Robert Lizotte, Jr.
Research Scientist
-------
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Approved By: |
Sierra Environmental Monitoring, Inc
Date:
Client:
Taken by:
Report:
PO#:
Date:
10/16/2000
ALP-855
Client
36912
This report is applicable only to the sample received by the laboratory. The liability of the laboratory is limited to the amount paid
for this report. This report is for the exclusive use of the client to whom it is addressed and upon the condition that the client
assumes all liability for the further distribution of the report or its contents.
William F. Pillsbury
President
Page 18 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
quality Control Report
T 7z Addendum to SEM Report Number: 36912
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092242
Parameter
Arsenic - ICP-MS
| Arsenic - ICP-MS
Arsenic - ICP-MS
7 Arsenic - ICP-MS
* Arsenic - ICP-MS
Arsenic - ICP-MS
: Barium - ICP-MS
Barium - ICP-MS
Barium - ICP-MS
Barium - ICP-MS
; Barium - ICP-MS
Barium - ICP-MS
T Barium - ICP-MS
i Barium - ICP-MS
Barium - ICP-MS
;, Cadmium - ICP-MS
Cadmium - ICP-MS
; Cadmium - ICP-MS
3
Cadmium - ICP-MS
? Cadmium - ICP-MS
£ Cadmium - ICP-MS
J Chromium - ICP-MS
:i Chromium - ICP-MS
, Chromium - ICP-MS
Chromium - ICP-MS
LCS, %
Recovery
96.9
96.9
96.9
96.9
96.9
96.9
93.7
93.7
93.7
93.7
93.7
93.7
93.7
93.7
93.7
95.7
95.7
95.7
95.7
95.7
95.7
95.4
95.4
95.4
95.4
MS, %
Recovery
89.2
89.2
89.2
89.2
89.2
89.2
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
85.6
85.6
85.6
85.6
85.6
85.6
99.5
99.5
99.5
99.5
MSD, %
Recovery
93.0
93.0
93.0
93.0
93.0
93.0
90.9
90.9
90.9
90.9
90.9
90.9
90.9
90.9
90.9
89.1
89.1
89.1
89.1
89.1
89.1
96.1
96.1
96.1
96.1
RPD, %
2.67
4.21
9.20
2.67
4.21
9.20
5.30
4.62
8.65
5.30
4.62
8.65
5.30
4.62
'.. 8.65
1.55
2.99
9.99
1.55
2.99
9.99
0.00
4.08
10.64
0.00
Method Blank
<0.02
<0.02
<0.02
<0.02
O.02
<0.02
<0.02
<0.02
<0.02
O.02
O.02
O.02
<0.5
<0.5
<0.5
< 0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.05
<0.05
<0.05
<0.02
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
,egend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
"hursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
Page 1 of 3
John Kobza, Ph.D.
John C. Seher
Managers
-------
Quality Control Report
An Addendum to SEM Report Number: 36912
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092242
Parameter
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Silver - ICP-MS
LCS, %
Recovery
95.4
95.4
95.4
95.4
95.4
93.6
93.6
93.6
93,6
93.6
93.6
103.2
103.2
103.2
103.2
96.0
96.0
96.0
96.0
96.0
96.0
96.0
96.0
96.0
98.3
MS, %
Recovery
99.5
99.5
99.5
99.5
99.5
80.5
80.5
80.5
80.5
80.5
80.5
94.8
94.8
94.8
94.8
78.0
78.0
78.0
78.0
78.0
78.0
78.0
78.0
78.0
81.0
MSD, %
Recovery
96.1
96.1
96.1
96.1
96.1
88.1
88.1
88.1
88.1
88.1
88.1
97.2
97.2
97.2
97.2
74.4
74.4
74.4
74.4
74.4
74.4
74.4
74.4
74.4
86.5
RPD, %
4.08
10.64
0.00
4.08
10.64
4.42
3.91
9.02
4.42
3.91
9.02
5.54
3.52
0.21
'.. 1.89
7.62
4.72
13.11
7.62
4.72
13.11
7.62
4..72
13.11
1.63
Method Blank
<0.02 mg/L
O.02 mg/L
O.04 mg/L
<0.04 mg/L
<0.04 mg/L
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
O.02 mg/L
<0.02 mg/L
<0.02 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L ;
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
<0.02 mg/L
<0.02 mg/L
<0.02 mg/L
<0.2 mg/L
<0.2 mg/L
<0.2 mg/L .
< 0.02 mg/L
Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Thursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-anaiytical.com
Page 2 of?
John Kobza, Ph.D.
John C. Seher
Managers
-------
Quality Control Report
] n Addendum to SEM Report Number: 36912
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092242
.--f Parameter
Silver
Silver
Silver
Silver
; Silver
Silver
Silver
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
LCS, %
Recovery
98
3
98.3
98
98
98
98
98
3
3
3
3
3
MS, %
Recovery
81
0
81.0
81
81
81
81
81
.0
.0
.0
.0
.0
MSD, %
Recovery
86.5
86.5
86.5
86.5
86.5
86.5
86.5
RPD, %
5.07
11.08
2.70
1.63
5.07
11.08
2.70
Method Blank
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Uiursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page 3 of3
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Approved By:
Sierra-Environmental Monitoring, Inc
Date:
Client:
Taken by:
Report:
P0#:
10/16/2000
ALP-855
Client
36913
Date:
This report is applicable only to the sample received by the laboratory. The liability of the laboratory is limited to the amount paid
for this report. This report is for the exclusive use of the client to whom it is addressed and upon the condition that the client
assumes all liability for the further distribution of the report or its contents.
William F. Pillsbury
President
Page 52 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Quality Control Report
\ n Addendum to SEM Report Number: 36913
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092241
,p Parameter
h
Arsenic -
^:>
Arsenic -
Arsenic -
! \ Arsenic -
J Arsenic -
Arsenic -
Arsenic -
Arsenic -
Arsenic -
Arsenic -
Barium -
Barium -
Barium -
Barium -
Barium -
v Barium -
Barium -
; Barium -
Barium -
Barium -
'^
Barium -
4 Barium -
Barium -
Barium -
i Barium -
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
LCS, %
Recovery
94
.7
94.7
94
.7
94.7
94
94
94
94
94
94
93
93
93
93
93
93
93
93
93
.7
.7
.7
.7
.7
.7
.7
.7
.7
.7
.7
.7
.7
.7
7
93.7
93.7
93.7
93.7
93.7
93.7
MS, %
Recovery
89
89
89
89
89
89
.2
.2
.2
.2
.2
.2
89.2
89.2
89.2
89.2
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
89.6
MSD, %
Recovery
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
91
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
.1
RPD, %
9
1
.20
.59
10.63
3
7
9
1
.39
.81
.20
.59
10.63
3.39
7.81
8.65
1.78
2.96
1.43
'. 7.70
8.65
1.78
2.96
1.43
7.70
8.65
1.78
2.96
1.43
7.70
Method Blank
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
O.02
<0.02
O.02
<0.02
<0.5
<0.5
0.5
<0.5
0.5
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
[.egend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Thursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
Page 1 of 5
John Kobza, Ph.D.
John C. Seher
Managers
-------
Quality Control Report
An Addendum to SEM Report Number: 36913
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092241
Parameter
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Cadmium -
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
Chromium
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
- ICP-MS
Chromium - ICP-MS
Chromium
Chromium
- ICP-MS
- ICP-MS
LCS, %
Recovery
95
95
95
95
95
95
95
95
95
95
93
93
93
93
93
93
93
93
93
93
93
93
93
93
93
.6
.6
.6
.6
.6
.6
.6
.6
.6
.6
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
.8
MS, %
Recovery
85
.6
85.6
85
85
85
85
85
85
.6
.6
.6
.6
.6
.6
85.6
85.6
99
99
99
99
99
99
99
.5
.5
.5
.5
.5
.5
.5
99.5
99
99
99
99
.5
.5
.5
.5
99.5
99.5
99
.5
MSD, %
Recovery
90.5
90.5
90.5
90.5
90.5
90.5
90.5
90.5
90.5
90.5
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
98.4
RPD,%
9.
99
0.44
3.
1.
59
32
0.33
9.
99
0.44
3.
1.
0.
59
32
33
10.64
1.
5.
3.
< 0.
01
69
82
96
10.64
1.
5.
3.
0.
10
1.
5.
3.
0.
01
69
82
96
.64
01
69
82
96
Method Blank
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
<0.02
<0.02
<0.05
<0.05
<0.05
< 0.05
<0.05
<0.02
<0.02
O.02
<0.02
O.02
<0.04
<0.04
<0.04
<0.04
O.04
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Thursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page 2 of
John Kobza, Ph.D.
John C. Seher
Managers
-------
I
Quality Control Report
} n Addendum to SEM Report Number: 36913
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092241
Parameter
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Chromium - ICP-MS
Lead -ICP-MS
Lead - ICP-MS
Lead -ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
Lead - ICP-MS
' Lead - ICP-MS
Lead -ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
~
Mercury - AA Cold Vapor
"
Mercury - AA Cold Vapor
Mercury - AA Cold Vapor
1 Mercury - AA Cold Vapor
- Selenium - ICP-MS
, Selenium - ICP-MS
: Selenium - ICP-MS
LCS, %
Recovery
93.8
93.8
93.8
93.8
93.8
93.6
93.6
93.6
93.6
93.6
93.6
93.6
93.6
93.6
93.6
99.6
99.6
99.6
99.6
99.6
99.6
99.6
90.0
90.0
90.0
MS, %
Recovery
99.5
99.5
99.5
99.5
99.5
80.5
80.5
80.5
80.5
80.5
80.5
80.5
80.5
80.5
80.5
97.4
97.4
97.4
97.4
97.4
97.4
97.4
62.5
62.5
62.5
MSD, %
Recovery
98.4
98.4
98.4
98.4
98.4
85.2
85.2
85.2
85.2
85.2
85.2
85.2
85.2
85.2
85.2
97.2
97.2
97.2
97.2
97.2
97.2
97.2
88.8
88.8
88.8
RPD, %
10.64
1.01
5.69
3.82
0.96
9.02
1.86
2.93
5.33
1.00
9.02
1.86
2.93
5.33
*.. 1.00
2.55
0.21
1.71
1.97
1.24
1.22
1.89
13.11
3.39
13.84
Method Blank
O.05 mg/L
O.05 mg/L
<0.05 mg/L
O.05 mg/L
<0.05 mg/L
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
<0.02 mg/L
<0.02 mg/L
<0.02 mg/L
<0.02 mg/L
O.02 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.0005 mg/L
< 0.02 mg/L
< 0.02 mg/L
< 0.02 mg/L
.egend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
'hursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page 3 of 5
John Kobza, Ph.D.
John C. Seher
Managers
-------
Quality Control Report
An Addendum to SEM Report Number: 36913
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092241
Parameter
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Selenium - ICP-MS
Silver - ICP-MS
Silver - ICP-MS
Silver - ICP-MS
Silver - ICP-MS
Silver -ICP-MS
Silver -ICP-MS
Silver - ICP-MS
Silver - ICP-MS
LCS, %
Recovery
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
90.0
98.3
98.3
98.3
98.3
98.3
98.3
98.3
98.3
MS,%
Recovery
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
62.5
81.0
81.0
81.0
81.0
81.0
81.0
81.0
81.0
MSD, %
Recovery
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
88.8
87.0
87.0
87.0
87.0
87.0
87.0
87.0
87.0
RPD, %
27.83
35.20
13.11
3.39
13.84
27.83
35.20
13.11
3.39
13.84
27.83
35.20
13.11
3.39
', 13.84
27.83
35.20
11.08
1.71
1.53
2.67
0.52
2.70
11.08
1.71
Method Blank
<0.02
<0.02
<0.02
O.02
O.02
O.02
<0.02
O.05
<0.05
O.05
<0.05
<0.05
<0.2
<0.2
<0.2
<0.2
<0.2
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
O.02
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L .
mg/L
Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Thursday, October 19, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page 4 of 5'
John Kobza, Ph.D.
John C. Seher
Managers
-------
I
Duality Control Report
] n Addendum to SEM Report Number: 36913
Sierra
Environmental
Monitoring, Inc.
Project ID:
BMI00092241
Parameter
LCS, %
Recovery
MS, %
Recovery
MSD, %
Recovery
RPD, %
Method Blank
Silver - ICP-MS
Silver - ICP-MS
Silver - ICP-MS
Silver - ICP-MS
98.3
98.3
98.3
98.3
81.0
81.0
81.0
81.0
87.0
87.0
87.0
87.0
1.53
2.67
0.52
2.70
O.02 mg/L
O.02 mg/L
O.02 mg/L
<0.02 mg/L
1 Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
' 'RPD, Relative Percent Difference
Thursday, October 19, 2000
' William F. Pillsbury
| President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page 5 of 5
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Approved By:
Date:
Client:
Taken by:
Report:
P0#:
Date:
10/25/00
ALP-855
Client
37235
icrra Environmental Monitoring, Inc
This report is applicable only to the sample received by the laboratory. The liability of the laboratory is limited to the amount paid
for this report. This report is for the exclusive use of the client to whom it is addressed and upon the condition that the client
assumes all liability for the further distribution of the report or its contents.
William F. Pillsbury
President
Page 6 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
j Quality Control Report
TAn Addendum to SEM Report Number: 37235
Sierra
Environmental
Monitoring, Inc.
Parameter
MS, %
Recovery
MSD, %
Recovery
RPD, %
Method Blank
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Silver - ICP-MS
105.0
102.0
96.8
94.7
91.4
69.0
92.4
91.5
97.9
92.0
91.6
89.0
85.7
71.2
72.9
84.5
7.00
10.31
5.52
6.21
6.44
3.14
23.59
7.95
0.005
O.005
O.005
O.005
O.005
O.0005
O.005
O.005
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Legend: LCS, Laboratory Control Standard; MS, Matrix Spike; MSD, Matrix Spike Duplicate;
RPD, Relative Percent Difference
Wednesday, October 25, 2000
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
Page I of I
John Kobza, Ph.D.
John C. Seher
Managers
-------
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX D
TPH LABORATORY-REPORTEDSAMPLE DATA WITH QC QUALIFIERS
-------
-------
lleatreiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank:
LCS for FID
LOAD #20
LOAD #24
LOAD #24
CJ:
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Weight (g):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
DTP RF:
MDL ug
YH91PB
00-441
NA
2.00
31.00
mg/kg
15885.193
15336.625
115.903
272.133
160.532
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.761
YH92LCS
00-441
NA
2.00
NA
mg/kg
NA
15336.625
119.961
267.829
NA
20.200
20.218
3.005
3.636
2.000
0.989
1.076
NA
YH94MS
00-441
09/22/00
2.00
16.17
mg/kg
NA
15336.625
99.379
291.170
NA
20.200
20.218
3.005
3.636
2.000
0.989
1.076
9.128
X9001
00-441
09/24/00
2.00
29.40
mg/kg
18648.783
15336.625
117.869
281 .825
2912.464
20.200
20.218
3.005
3.636
2.000
0.989
1.076
5.020
X9001DUP
00-441
09/24/00
2.00
30.46
mg/kg
15317.051
15336.625
123.969
281.020
ND
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.846
OTP Surrogate Recovery:
Total Hydrocarbons:
ND - Not Dectected
NA - Not Applicable.
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy
data quality objective.
- - QC value outside the accuracy
or precision
data quality objective -but meets
contingency criteria
79 83
0.47 J NA
63
NA
78
14.03
82
4.85
-------
dBaffelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Surrogate Corrected
Standard Reference-Material-1944
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Weight (g):
Units:
Sample Area:
DCMArea:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
DTP RF:
MDL ug
X8997
00-441
09/22/00
2.00
33.37
mg/kg
14199.915
15336.625
118.464
275.438
ND
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.423
X8998
00-441
09/22/00
2.00
31.00
mg/kg
15614.044
15336.625
113.244
268.840
ND
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.761
X8999
00-441
09/23/00
2.00
29.99
mg/kg
16281.691
15336.625
117.875
279.490
547.701
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.922
X9000
00-441
09/23/00
2.00
30.14
mg/kg
16481.273
15336.625
119.181
291.056
734.411
20.200
20.218
3.005
3.636
2.000
0.989
1.076
4.897
BDO#991 222-02
YH96SRM
00-441
NA
2.00
2.02
mg/kg
65450.66
15336.63
113.44
247.64
49752.95
20.20
20.22
3.00
3.64
0.00
2.00
0.99
1.08
73.07
DTP Surrogate Recovery:
Total Hydrocarbons:
ND - Not Dectected
NA - Not Applicable.
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy
data quality objective.
- - QC value outside the accuracy
or precision
data quality objective -but meets
contingency criteria
80
4.42 U
78
4.76 U
78
2.35 J
76
3.10 J
85.07
4058.04
-------
. . . Puffing Technology To Work
Projecl Name: WA 3-26 BOSTON CAP PROJ
Project Number: G464426-EPA11DUXLAB
Client ID:
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
Filter from
CAD01394OR1
X8437-F
00-425
09/1 1/00
2.00
2.00
ug/l
17477.225
15182.440
115.386
265.651
Filter from
CAD01534OR1
X8567-F
00-425
09/15/00
2.00
2.00
ug/l
16233.306
15020.065
116.686
373.633
Filter from
CAD014D40R1
XB582-F
00-425
09/1 5/00
2.00
2.00
ug/l
16341.659
15020.065
163.780
352.333
Filter from
CAD014DBOR1
X8583-F
00-425
09/15/00
2.00
2.00
ug/l
16752.555
15020.065
178.340
416.047
Filter from
CAD0147DOR1
X8597-F
00-425
09/14/00
2.00
2.00
ug/l
15906.434
15020.065
108.979
339.513
Filter from
CAD01480OR1
X859B-F
00-425
09/14/00
2.00
2.00
ug/l
17097.975
15020.065
155.001
554.391
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
20.200
20.218
3.005
3.636
2.000
722.922
20.200
20.218
3.005
3.636
2.000
805.481
20.200
20.218
3.005
3.636
2.000
20.200
20.218
3.005
3.636
2.000
437.877
20.200
20.218
3.005
3.636
2.000
20.200
20.218
3.005
3.636
2.000
AVE RF:
DTP RF:
MDL VALUE ug/L
DTP Surrogate Recovery:
Total Hydrocarbons:
0.989
1.076
78.40
81
142.32
0.989
1.076
78.40
58
34.70 J
0.989
1.076
78.40
86
41.87 J
0.989
1.076
78.40
80
51.05 J
0.989
.1 .076
78.40
60
21.52 J
0.989
1.076
78.40
52
45.60 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte delected at a level greater than 3*
MDL in PB
ME - Significant matrix interference estimated
value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
ff-T
-------
. .. Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP PROJECT
Project Number. G464426-EPA1IDUXLAB
Client ID:
Batlelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/L
OTP Surrogate Recovery:
Total Hydrocarbons:
Procedural Blank
YH09PB
00-425
NA
2.00
2.00
ug/l
15944.140
15182.440
135.900
281.638
344.162
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
90
20.14 J
FID LCS
YH10LCS
00-425
NA
2.00
2.00
ug/l
NA
15182.440
126.386
279.651
NA
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
84
NA
Fitter from
CAD012BFOR1
X8406-F
00-425
09/09/00
2.00
2.00
ug/l
17756.658
15182.440
73.696
284.514
2216.008
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
48
154.26
Filter from
CAD012C3OR1
X8407-F
00-425
09/09/00
2.00
2.00
ug/l
24519.291
15182.440
1 1 1 .228
264.452
8961.171
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
78
687.28
Filter from
CAD01390OR1
X8436-F
00-425
09/1 1/00
2.00
2.00
ug/l
15762.235
15182.440
66.022
261.183
252.590
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
47
14.93 J
NA-Not Applicable.
ND-Not Dectecled
J- Analyte detected below the MDL
B - Analyte detected at a level greater than 3*
MDLinPB
ME - Significant matrix interference estimated
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
data quality objective -but meets
contingency criteria
-------
f> Battelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
Client ID:
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL ug/l
Procedural Blank:
YE17PB
00-352
NA
2.00
1.80
ug/l
16033.56
15541.62
151.33
267.43
73.18
20.20
20.28
3.00
3.60
2.00
0.99
1.08
87.11
Laboratory Control
Sample
YE18LCS
00-352
NA
2.00
2.00
ug/l
0.00
15541.62
156.68
280.44
ND
20.20
20.28
3.00
3.60
2.00
0.99
1.08
78.40
1C
SC0755,6,1
00-352
NA
1.00
NA
ug/l
0.00
15541.62
186.44
172.05
NA
19.94
20.20
3.00
3.60
1.00
0.99
1.08
NA
OTP Surrogate Recovery:
Total Hydrocarbons:
105
0.87 J
103
NA U
99
NA
NA - Not Applicable.
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
-------
llBaffelie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
Client ID:
CAD0104AOR1
CAD0104DOR1
CAD01050OR1
CAD01053OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL ug/l
X7967
00-352
09/06/00
2.00
2.00
ug/l
16400.97
15541.62
144.38
280.93
434.04
20.20
20.28
3.00
3.60
2.00
0.99
1.08
78.40
X7968
00-352
09/06/00
2.00
2.00
ug/l
16391.88
15541.62
154.89
281 .20
414.17
20.20
20.28
3.00
3.60
2.00
0.99
1.08
78.40
X7969
00-352
09/06/00
2.00
2.00
ug/l
16291.47
15541.62
133.45
285.07
331 .33
20.20
20.28
3.00
3.60
2.00
0.99
1.08
78.40
X7970
00-352
09/06/00
2.00
2.00
ug/l
16359.11
15541.62
138.65
292.20
386.64 .
20.20
20.28
3.00
3.60
2.00
0.99
1.08
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
95
26.75 J
102
25.28 J
87
18.93 J
88
22.22 J
NA - Not Applicable.
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U analyte not detected
& - QC value outside the accuracy or
data quality objective.
" - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
-------
llBaltelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
Procedural Blank LCS for FID: CAD012ACOR1 CAD01322OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDLVALUEug/l
OTP Surrogate Recovery:
Total Hydrocarbons:
YF10PB
00-371
Water
2.00
1.85
ug/l
15725.541
15155.258
118.570
256.743
194.970
20.200
20.284
3.005
3.603
2.000
0.989
1 .076
84.76
85
11.57 J
YF1 1 LCS
00-371
Water
2.00
2.00
ug/l
0.000
15155.258
123.010
247.319
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
92
NA
YF13MS
00-371
Water
2.00
1.00
ug/l
0.000
15155.258
127.064
261.460
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
90
NA
X8422
00-371
Water
2.00
1.00
ug/l
16224.857
15155.258
125.850
267.433
676.316
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
87
93.69 J
f-'-
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBattelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
CAD01322OR1 CAD012ACOR1 CAD012AFOR1 CAD012B2OR1
Battelte Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
OTP Surrogate Recovery:
Total Hydrocarbons:
X8422DUP
00-371
Water
2.00
1.00
ug/l
15648.875
15155.258
123.807
261.966
107.844
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
87
7.20 J
X8403
00-371
Water
2.00
1.00
ug/l
15904.875
15155.258
120.145
259.849
369.623
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
86
48.49 J
X8404
00-371
Water
2.00
1.00
ug/l
15510.237
15155.258
121.771
257.017
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
88
156.80 U
X8405
00-371
Water
2.00
2.00
ug/l
16247.303
15155.258
128.114
268.876
695.055
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
88
47.99 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBairelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
CAD012BFOR1 CAD012C3OR1 CAD012C6OR1 CAD012CCOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
OTP Surrogate Recovery:
Total Hydrocarbons:
X8406
00-371
Water
2.00
2.00
ug/l
15943.924
15155.258
126.057
268.911
393.698
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
87
25.10 J
X8407
00-371
Water
2.00
2.00
ug/l
16134.387
15155.258
127.741
258.839
592.549
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
91
41.95 J
X8408
00-371
Water
2.00
2.00
ug/l
19760.939
15155.258
132.481
261.145
4212.055
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
94
324.63
X8409
00-371
Water
2.00
2.00
ug/l
15576.685
15155.258
127.896
260.783
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
91
78.40 U
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBalteile
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
CAD012CFOR1 CAD012D2OR1 CAD012D6OR1 CAD012DCOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVERF:
OTP RF:
MDL VALUE ug/1
X8410
00-371
Water
2.00
2.00
ug/l
17320.881
15155.258
129.020
267.671
1768.932
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X841 1
00-371
Water
2.00
2.00
ug/l
19726.238
15155.258
132.892
278.265
4159.823
20.200
20.284
3.005
3.603
2.000
0.989
1 .076
78.40
X8412
00-371
Water
2.00
2.00
ug/l
15821.592
15155.258
131.999
269.142
265.193
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8413
00-371
Water
2.00
2.00
ug/l
16051.463
15155.258
128.441
264.381
503.383
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
89
130.17
88
300.53
91
15.32 J
90
34.08 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBanene
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
CAD012EOOR1
CAD012ECOR1 CAD012FOOR1 CAD012F4OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
OTP Surrogate Recovery:
Total Hydrocarbons:
X8414
00-371
Water
2.00
2.00
ug/l
18773.342
15155.258
124.239
257.609
3236.236
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
89
251 .78
X8415
00-371
Water
2.00
2.00
ug/l
15229.387
15155.258
127.021
261 .342
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
90
78.40 U
X8416
00-371
Water
2.00
2.00
ug/l
16206.071
15155.258
127.968
269.956
652.889
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
88
44.59 J
X8417
00-371
Water
2.00
2.00
ug/l
16030.012
15155.258
130.525
274.737
469.492
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
88
30.10 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
tlBalteiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
Client ID:
CAD0130COR1 CAD0130FOR1 CAD01312OR1 CAD0131FOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
OTP Surrogate Recovery:
Total Hydrocarbons:
X8418
00-371
Water
2.00
2.00
ug/l
15256.302
15155.258
131.625
276.830
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
88
78.40 U
X8419
00-371
Water
2.00
2.00
ug/l
16665.953
15155.258
127.441
260.238
1123.016
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
91
83.33
X8420
00-371
Water
2.00
2.00
ug/l
16417.883
15155.258
126.879
258.251
877.495
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
91
64.59 J
X8421
00-371
Water
2.00
2.00
ug/l
16325.866
15155.258
124.330
256.545
789.733
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
90
58.07 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBatteile
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP PROJECT
Project Number: G464426-EPA11DUXLAB
Client ID:
Procedural Blank:
LCS tor FID:
CAD01325OR1
CAD0132EOR1
x-
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL ug/l
YF15PB
00-372
NA
2.00
1.00
ug/l
15743.855
15147.564
118.859
268.575
208.857
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
YF16LCS
00-372
NA
2.00
2.00
ug/l
0.000
15147.564
85.907
287.184
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
YF18MS
00-372
09/10/00
2.00
1.00
ug/l
0.000
15147.564
123.768
280.480
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8425
00-372
09/10/00
2.00
1.00
ug/l
15787.140
15147.564
124.341
288.320
226.915
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
82 55
22.15 J NA
82
156.80 U
80
22.54
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater than
3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but meets
contingency criteria
-------
lleaffeiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP PR
Project Number: G464426-EPA11DUXLAB
Client ID:
CAD0132EOR1 CAD01325OR1
CAD0132BOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL ug/l
X8425DUP
00-372
09/10/00
2.00
1.00
ug/l
16101.591
15147.564
126.117
284.494
543.416
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8423
00-372
09/10/00
2.00
1.00
ug/l
14566.922
15147.564
124.852
283.686
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8424
00-372
09/10/00
2.00
1.00
ug/l
15564.311
15147.564
121.453
270.833
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
82
68.41 J
81
156.80 U
83
156.80 U
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater than
3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but meets
contingency criteria
-------
OBaneae
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank:
LCS for FID:
CAD01331OR1
CAD013C9OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
YF74PB
00-393
NA
2.00
1.85
ug/L
15705.254
14759.394
153.263
348.959
443.638
20.200
20.284
3.005
3.603
2.000
1.001
1.053
84.76
YF75LCS
00-393
NA
2.00
2.00
ug/L
NA
14759.394
156.942
329.940
NA
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
YF77MS
00-393
09/10/00
2.00
1.00
ug/L
NA
14759.394
156.140
326.156
NA
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8445
00-393
09/11/00
2.00
1.00
ug/L
15942.517
13247.422
117.828
261 .627
2315.640
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
83 90
22.54 J NA
91
NA
83
351.94
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBanene
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD013C9OR1 CAD01331OR1
CAD01334OR1
CAD01337OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8445DUP
00-393
09/11/00
2.00
1.00
ug/L
16209.212
1 3247.422
117.482
246.712
2597.596
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8426
00-393
09/10/00
2.00
1.00
ug/L
15901.982
14759.394
150.294
328.504
663.790
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8427
00-393
09/10/00
2.00
1.00
ug/L
16025.136
14759.394
153.031
327.228
785.483
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8428
00-393
09/10/00
2.00
2.00
ug/L
16459.805
14759.394
149.613
322.180
1228.618
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
88
420.48
87
71.94 J
88
87.27 J
88
72.15 J
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBaltelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0133AOR1 CAD01348OR1 CAD0134BOR1 CAD0134EOR1
f i
Sf.
SfX
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
DTP RF:
MDL VALUE ug/l
X8429
00-393
09/10/00
2.00
2.00
ug/L
16754.652
14759.394
144.378
303.622
1 547.258
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8430
00-393
09/10/00
2.00
2.00
ug/L
15860.855
14759.394
122.452
343.661
635.348
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8431
00-393
09/10/00
2.00
2.00
ug/L
16281.910
14759.394
159.389
328.246
1034.881
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8432
00-393
09/10/00
2.00
2.00
ug/L
16449.537
14759.394
156.580
315.073
1218.490
20.200
20.284
3.005
3.603
2.000
1.001
1 .053
78.40
DTP Surrogate Recovery:
Total Hydrocarbons:
90
98.03
67
32.50 J
92
58.82 J
94
73.24 J
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBaneae
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01371OR1 CAD01376OR1 CAD0137AOR1
CAD01390OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8433
00-393
09/10/00
2.00
2.00
ug/L
16043.073
14759.394
162.604
342.326
778.749
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8434
00-393
09/10/00
2.00
2.00
ug/L
16813.703
14759.394
158.235
351.263
1544.811
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8435
00-393
09/10/00
2.00
2.00
ug/L
1 6059.394
14759.394
156.729
340.232
803.039
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8436
00-393
09/11/00
2.00
2.00
ug/L
16043.911
14759.394
152.708
335.188
796.621
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
90
41.10 J
85
83.94
87 86
42.82 J 43.15 J
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
flBaffelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01394OR1 CAD01398OR1 CAD0139FOR1 CAD013A2OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8437
00-393
09/11/00
2.00
2.00
ug/L
16330.122
14759.394
160.185
339.659
1070.884
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8438
00-393
09/11/00
2.00
2.00
ug/L
16389.561
14759.394
152.603
347.389
1130.175
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8439
00-393
09/11/00
2.00
2.00
ug/L
16350.870
14759.394
157.581
332.377
1101.518
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8440
00-393
09/11/00
2.00
2.00
ug/L
1 6257.830
14759.394
1 60.666
335.259
1002.511
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
89
58.82 J
.83
60.85 J
90
62.07 J
91
55.54 J
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBattelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD013A6OR1 CAD013AAOR1 CAD013BOOR1 CAD013B4OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8441
00-393
09/11/00
2.00
2.00
ug/L
16976.891
13247.422
120.066
262.360
3347.043
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8442
00-393
09/11/00
2.00
2.00
ug/L
16297.170
13247.422
113.561
250.956
2685.231
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8443
00-393
09/11/00
2.00
2.00
ug/L
16609.557
13247.422
121.296
250.654
2990.185
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8444
00-393
09/11/00
2.00
2.00
ug/L
16360.765
13247.422
118.611
262.192
2732.540
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
85
255.76
84
213.74
90
238.85
84
208.06
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBafflene
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank: LCSforFID CAD01405OR1
CAD0143COR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
DTP RF:
MDL VALUE ug
YG28PB
00-405
NA
2.00
1.80
ug/l
16626.646
16030.312
107.223
276.366
212.745
20.200
20.284
3.005
3.603
2.000
0.989
1.076
87.11
YG29LCS
00-405
NA
2.00
2.00
ug/l
NA
16030.312
125.945
284.585
NA
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
YG31MS
00-405
09/12/00
2.00
1.00
ug/l
NA
16030.312
127.503
277.566
NA
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8623
00-405
09/12/00
2.00
1.00
ug/l
15314.521
15075.366
123.264
251.589
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
72 82
12.13 J NA
85
NA
91
156.80 U
-------
OBauene
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0143COR1 CAD01405OR1 CAD01408OR1.
CAD0140BOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug
OTP Surrogate Recovery:
Total Hydrocarbons:
X8623DUP
00-405
09/12/00
2.00
1.00
ug/l
16017.566
15075.366
121.182
304.171
516.847
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
74
59.80 J
X8609
00-405
09/12/00
2.00
1.00
ug/l
16603.219
16030.312
116.767
280.673
175.467
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
77
15.93 J
X8610
00-405
09/12/00
2.00
1.00
ug/l
16312.979
16030.312
117.227
289.865
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
75
156.80 U
X8611
00-405
09/12/00
2.00
2.00
ug/l
16822.996
16030.312
124.095
305.922
362.667
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
75
19.41 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
lleaireiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01416OR1 CAD01419OR1 CAD0141COR1 CAD0141FOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug
X8612
00-405
09/12/00
2.00
2.00
ug/l
16767.227
15075.366
186.875
439.586
1065.400
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8613
00-405
09/12/00
2.00
2.00
ug/l
16409.033
15075.366
159.903
369.966
803.798
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8614
00-405
09/12/00
2.00
2.00
ug/l
16498.639
15075.366
150.137
356.202
916.934
20.200
20.284
3.005
3.603
2.000
0.989
1 .076
78.40
X8615
00-405
09/12/00
2.00
2.00
ug/l
17112.378
15075.366
165.694
367.633
1503.685
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
79
44.70 J
80
39.57 J
78
47.77 J
83
78.73
-------
lleaneiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
GAD01422OR1 CAD01425OR1 CAD01428OR1
CAD0142BOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug
OTP Surrogate Recovery:
Total Hydrocarbons:
X8616
00-405
09/12/00
2.00
2.00
ug/l
16399.672
15075.366
134.528
317.867
871.911
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
78
51.22 J
X8617
00-405
09/12/00
2.00
2.00
ug/l
15938.676
15075.366
122.122
265.585
475.603
20.200
20.284
3.005
3.603
2.000
0.989
1 .076
78.40
85
31.77 J
X8618
00-405
09/12/00
2.00
2.00
ug/l
16154.371
1 5075.366
129.651
273.072
676.282
20.200
20.284
3.005
3.603
2.000
0.989
1 .076
78.40
88
45.78 J
X8619
00-405
09/12/00
2.00
2.00
ug/l
15669.509
15075.366
131.190
299.019
163.934
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
81
6.39 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBaiteiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0142EOR1
CAD01436OR1 CAD01439OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug
OTP Surrogate Recovery:
Total Hydrocarbons:
X8620
00-405
09/12/00
2.00
2.00
ug/l
15940.971
15075.366
125.723
290.247
449.635
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
80
26.83 J
X8621
00-405
09/12/00
2.00
2.00
ug/l
15825.529
15075.366
120.483
274.744
354.936
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
81
21.58 J
X8622
00-405
09/12/00
2.00
2.00
ug/l
15967.413
15075.366
118.325
281.199
492.523
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
78
30.97 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBafleiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank
LCS for FID
CAD01469OR1
CAD014DBOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
YG33PB
00-406
NA
2.00
1.85
ug/l
16178.952
15522.477
126.698
284.358
245.419
20.200
20.284
3.005
3.603
2.000
0.989
1.076
84.76
YG34LCS
00-406
NA
2.00
1.00
ug/l
0.000
15522.477
129.845
287.723
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
YG36MS
00-406
09/14/00
2.00
1.00
ug/l
0.000
15522.477
121.049
284.229
ND
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8583
00-406
09/15/00
2.00
1.00
ug/l
18711.111
15522.477
138.014
319.991
2730.629
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
82
13.86 J
84
NA
79
NA
80
338.97
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
C-Baireiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD014DBOR1
CAD01469OR1
CAD0146COR1
CAD0146FOR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(i):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTPRF:
MDLVALUEug/l
X8583DUP
00-406
09/15/00
2.00
1.00
ug/l
16855.150
15522.477
140.865
300.918
890.890
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8594
00-406
09/14/00
2.00
1.00
ug/l
16281.556
15522.477
113.668
267.082
378.329
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8595
00-406
09/14/00
2.00
1.00
ug/l
16173.608
15522.477
118.359
282.404
250.368
20.200
20.284
3.005
3.603
2.000
0.989
1.076
156.80
X8596
00-406
09/14/00
2.00
2.00
ug/l
16765.906
15522.477
133.448
310.705
799.276
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
87
111.33 J
79
48.25 J
78
26.60 J
80
47.74 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBanene
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0147DOR1 CAD01480OR1 CAD01483OR1 CAD01486OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8597
00-406
09/14/00
2.00
2.00
ug/l
16665.971
15522.477
148.700
291.846
702.948
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8598
00-406
09/14/00
2.00
2.00
ug/l
16471.738
15522.477
155.762
292.544
500.955
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8599
00-406
09/14/00
2.00
2.00
ug/l
17074.283
15522.477
130.929
281.074
1139.803
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8600
00-406
09/14/00
2.00
2.00
ug/l
17134.203
15522.477
128.788
280.854
1202.084
20.200
20.284
3.005
3.603
.2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
94
44.39 J
99
30.17 J
86
78.02 J
85
82.61
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
ft Battelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01489OR1
CAD0148COR1 CAD0148FOR1 CAD01492OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8601
00-406
09/14/00
2.00
2.00
ug/l
16356.890
15522.477
133.461
298.192
402.760
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8602
00-406
09/14/00
2.00
2.00
ug/l
17120.975
15522.477
133.983
291.593
1172.922
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8603
00-406
09/14/00
2.00
2.00
ug/l
17586.373
15522.477
131.192
284.644
1648.060
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8604
00-406
09/14/00
2.00
2.00
ug/l
16792.848
15522.477
129.429
298.330
842.612
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
83
22.78 J
85 85
77.35 J 113.45
80
52.88 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBaffelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01495OR1 CAD0149DOR1
CAD014AOOR1 CAD014A3OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8605
00-406
09/14/00
2.00
2.00
ug/l
16536.615
15522.477
131.400
295.601
587.137
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8606
00-406
09/14/00
2.00
2.00
ug/l
16504.012
15522.477
115.852
256.479
609.204
20.200
20.284
3.005
3.603
2.000
0-989
1.076
78.40
X8607
00-406
09/14/00
2.00
2.00
ug/l
16252.591
15522.477
124.072
284.792
321.250
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8608
00-406
09/14/00
2.00
2.00
ug/l
18444.746
15522.477
120.584
289.224
2512.461
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
82
35.76 J
84
43.71 J
81
18.23 J
77
172.62
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBaltelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD014BFOR1 CAD014C2OR1 CAD014C5OR1 CAD014D4OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8579
00-406
09/15/00
2.00
2.00
ug/l
16865.328
15522.477
131.539
292.522
918.790
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8580
00-406
09/15/00
2.00
2.00
ug/l
16680.660
15522.477
131.096
280.117
746.970
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8581
00-406
09/15/00
2.00
2.00
ug/l
16633.686
15522.477
134.211
290.201
686.797
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
X8582
00-406
09/15/00
2.00
2.00
ug/l
16821.000
15522.477
154.861
294.550
849.112
20.200
20.284
3.005
3.603
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
83
59.35 J
87
49.66 J
86
43.53 J
97
54.07 J
ND-Not Dectected
J - Analyte detected below the MDL
B - Analyte detected at a level
greater than 3* MDL in PB
ME - Significant matrix interference
estimated value
U - Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
llBalfeiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank: LCS for FID:
CAD014DEOR1
CAD01547OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
YG38PB
00-407
NA
2.00
1.85
ug/l
16751.826
14463.697
197.332
442.790
1648.007
20.200
20.284
3.005
3.603
2.000
1.001
1.053
84.76
YG39LCS
00-407
NA
2.00
2.00
ug/l
NA
14463.697
163.090
354.594
NA
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
YG41MS
00-407
NA
2.00
1.00
ug/l
NA
14463.697
168.464
357.500
NA
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8573
00-407
09/15/00
2.00
1.00
ug/l
15614.383
14463.697
157.705
320.064
672.917
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
84
76.00 J
87
NA
89
NA
93
75.24 J
-------
llBaireiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01547OR1 CAD014DEOR1 CAD014E4OR1 CAD014E7OR1
TT:
f f
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
DTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
DTP RF:
MDL VALUE ug/l
X8573DUP
00-407
09/15/00
2.00
1.00
ug/l
15465.141
14463.697
164.997
374.898
461 .549
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8584
00-407
09/15/00
2.00
1.00
ug/l
15865.512
14463.697
165.620
356.946
879.249
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8585
00-407
09/15/00
2.00
1.00
ug/l
15693.479
14463.697
157.720
345.408
726.654
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8586
00-407
09/15/00
2.00
2.00
ug/l
16907.676
14463.697
163.662
363.726
1916.591
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
83
40.08 J
88
89.80 J
86
75.29 J
85
101.53
-------
-Battelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD014EAOR1
CAD014EDOR1 CAD014F3OR1
CAD014F6OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
OTP Surrogate Recovery:
Total Hydrocarbons:
X8587
00-407
09/15/00
2.00
2.00
ug/l
15890.675
14463.697
158.248
344.170
924.560
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
87
49.40 J
X8588
00-407
09/15/00
2.00
2.00
ug/l
16214.619
14463.697
173.992
366.508
1210.422
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
90
61.84 J
X8589
00-407
09/15/00
2.00
2.00
ug/l
15776.024
14463.697
162.762
350.896
798.669
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
88
41.12 J
X8590
00-407
09/15/00
2.00
2.00
ug/l
15981.193,
14463.697
157.122
350.168
1010.206
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
85
53.41 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBaneoe
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01511OR1 CAD01514OR1 CAD0151AOR1 CAD01523OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8591
00-407
09/15/00
2.00
2.00
ug/l
15797.486
14463.697
155.702
351.281
826.806
20.200
20.284
3.005
3.603
2.000
1 .00,1
1.053
78.40
X8592
00-407
09/15/00
2.00
2.00
ug/l
16212.533
14463.697
165.886
358.486
1224.464
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8593
00-407
09/15/00
2.00
2.00
ug/l
16415.920
14463.697
164.575
342.263
1445.385
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8564
00-407
09/15/00
2.00
2.00
ug/l
15809.036
14463.697
176.920
380.259
788.160
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
84
42.69 J
88
64.12 J
91
80.41
88
37.02 J
-------
flBaffeiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01526OR1 CAD01529OR1
CAD01534OR1
CAD01538OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8565
00-407
09/15/00
2.00
2.00
ug/l
15893.704
14463.697
157.377
344.922
927.708
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8566
00-407
09/15/00
2.00
2.00
ug/l
15972.594
14463.697
178.801
394.566
935.530
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8567
00-407
09/15/00
2.00
2.00
ug/l
16018.827
14463.697
187.430
352.519
1015.181
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8568
00-407
09/15/00
2.00
2.00
ug/l
16428.100
14463.697
169.423
372.336
1422.644
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
86
49.47 J
86
43.04 J
101
53.31
86
72.30 J
-------
lleattelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0153BOR1
CAD0153EOR1 CAD01541OR1 CAD01544OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
OTP Surrogate Recovery:
Total Hydrocarbons:
X8569
00-407
09/15/00
2.00
2.00
ug/l
16094.649
14463.697
182.230
377.165
1071.557
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
91
52.53 J
X8570
00-407
09/15/00
2.00
2.00
ug/l
15830.227
14463.697
160.143
323.491
882.896
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
94
50.27 J
X8571
00-407
09/15/00
2.00
2.00
ug/l
16294.820
14463.697
161.993
367.577
1301.553
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
83
66.65 J
X8572
00-407
09/15/00
2.00
2.00
ug/l
16360.988
14463.697
165.292
363.475
1368.524
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
86
71.17 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
OBaftelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank: LCS for FID:
CAD0154COR1 CAD01564OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
YG43PB
00-408
NA
2.00
1.40
ug/l
16245.397
14953.904
156.949
335.170
799.374
20.200
20.284
3.005
3.603
2.000
1.001
1.053
112.00
YG44LCS
00-408
NA
2.00
2.00
ug/l
NA
NA
182.287
341 .762
NA
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
YG46MS
00-408
09/15/00
2.00
1.00
ug/l
NA
NA
141.202
328.091
NA
20.200
20.284
3.005
3.603
2.000
1.001
1 1.053
156.80
X8578
00-408
09/16/00
2.00
1.00
ug/l
15499.273
14775.867
168.321
367.646
187.439
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
89
61.89 J
101
NA
81
NA
87
10.96 J
-------
QBaireiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON
CAP PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01564OR1 CAD0154COR1 CAD0154FOR1 CAD0155EOR1 CAD01561OR1
Battelle Sample ID:
Battelle Batch ID:
Collection Date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8578DUP
00-408
09/16/00
2.00
1.00
ug/l
16736.141
14775.867
180.740
391.389
1388.145
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8574
00-408
09/15/00
2.00
1.00
ug/l
15845.896
14953.904
157.855
357.739
376.398
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8575
00-408
09/15/00
2.00
1.00
ug/l
15628.851
14953.904
160.220
362.945
151.782
20.200
20.284
3.005
3.603
2.000
1.001
1.053
156.80
X8576
00-408
09/16/00
2.00
2.00
ug/l
15906.083
14953.904
158.382
344.073
449.724
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
X8577
00-408
09/16/00
2.00
2.00
ug/l
16417.303
14775.867
184.160
390.010
1067.266
20.200
20.284
3.005
3.603
2.000
1.001
1.053
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B-Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
87
133.53 J
83
32.85 J
83
7.27 J
87
21.57 J
89
50.42 J
-------
llBatteiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
Procedural Blank LCS for FID:
CAD015ABOR1
CAD015F5OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
OTP Surrogate Recovery:
Total Hydrocarbons:
YH01PB
00-422
NA
2.00
1.80
ug/l
15794.636
15072.746
122.365
273.478
326.047
20.200
20.218
3.005
3.636
2.000
0.989
1.076
87.11
83
21.70 J
YH02LCS
00-422
NA
2.00
2.00
ug/l
NA
15072.746
132.605
287.219
NA
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
86
NA
YH04MS
00-422
09/20/00
2.00
1.00
ug/l
NA
15072.746
125.030
257.559
NA
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
90
NA
X8877
00-422
09/20/00
2.00
1.00
ug/l
16053.931
15072.746
113.449
260.068
607.668
20,200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
81
85.80 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
-------
OBaoeae
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD015F5OR1 CAD015ABOR1
CAD015BOOR1
CAD015B3OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8877DUP
00-422
09/20/00
2.00
1.00
ug/l
16680.422
15072.746
113.234
250.700
1243.742
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8863
00-422
09/20/00
2.00
1.00
ug/l
16057.196
15072.746
124.760
254.738
604.952
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8864
00-422
09/20/00
2.00
1.00
ug/l
1 5474.909
15072.746
117.945
269.628
14.590
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8865
00-422
09/20/00
2.00
2.00
ug/l
15687.028
15072.746
116.537
280.667
217.078
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
84
193.01
91
87.36 J
81
156.80 U
77
10.97 J
-------
fl Battelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD015C2OR1
CAD015C5OR1
CAD015CBOR1
CAD015CEOR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8866
00-422
09/20/00
2.00
2.00
ug/l
16134.201
15072.746
118.855
264.669
677.931
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
X8867
00-422
09/20/00
2.00
2.00
ug/l
15830.161
15072.746
120.449
284.096
352.870
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
X8868
00-422
09/20/00
2.00
2.00
ug/l
15981.814
15072.746
115.817
287.497
505.754
20.200
20.218
3.005
3.636
2.000
0.989
1 .076
78.40
X8869
00-422
09/20/00
2.00
2.00
ug/l
15814.108
15072.746
134.021
288.746
318.595
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
83
47.49 J
79
20.55 J
75
31.11 J
86
17.71 J
-------
llBaltelle
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD015D1OR1 CAD015D4OR1 CAD015D7OR1 CAD015DCOR1
Battelie Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
OTP Surrogate Recovery:
Total Hydrocarbons:
X8870
00-422
09/20/00
2.00
2.00
ug/l
15518.403
15072.746
123.070
283.947
38.640
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
80
78.40 U
X8871
00-422
09/20/00
2.00
2.00
ug/l
16177.673
15072.746
129.450
300.036
675.441
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
80
41.16 J
X8872
00-422
09/20/00
2.00
2.00
ug/l
18263.006
15072.746
120.167
287.586
2782.507
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
78
192.79
X8873
00-422
09/20/00
2.00
2.00
ug/l
16423.867
15072.746
120.530
276.549
954.042
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
81
65.64 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision
data quality objective -but meets
contingency criteria
-------
lleaiteiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD0162COR1 CAD01610OR1 CAD01613OR1
CAD01616OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
OTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/1
X8991DUP
00-436
09/28/00
2.00
1.00
ug/l
16372.017
15075.366
124.070
283.312
889.269
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8982
00-436
09/28/00
2.00
1.00
ug/l
17011.797
15075.366
129.385
273.861
1533.185
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8983
00-436
09/28/00
2.00
1.00
ug/l
16165.121
15075.366
138.987
308.801
641.967
20.200
20.218
3.005
3.636
2.000
0.989
1.076
156.80
X8984
00-436
09/28/00
2.00
2.00
ug/l
16499.098
15075.366
138.457
305.507
979.768
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
81
118.57 J
88
219.05
84
75.28 J
84
60.68 J
-------
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01619OR1 CAD0161COR1 CAD01620OR1 CAD01623OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
AVE RF:
OTP RF:
MDL VALUE ug/l
X8985
00-436
09/28/00
2.00
2.00
ug/l
16646.258
15075.366
129.286
291 .442
1150.164
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
X8986
00-436
09/28/00
2.00
2.00
ug/l
16495.145
15075.366
130.139
282.545
1007.095
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
X8987
00-436
09/28/00
2.00
2.00
ug/l
16629.533
15075.366
137.665
293.595
1122.907
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
X8988
00-436
09/28/00
2.00
2.00
ug/l
16831.939
15075.366
136.940
278.599
1341.034
20.200
20.218
3.005
3.636
2.000
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
- - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
82
75.78 J
86
67.98 J
87
73.30 J
91
93.49
-------
llBaireiie
. . . Putting Technology To Work
Project Name: WA 3-26 BOSTON CAP
PROJECT
Project Number: G464426-
EPA11DUXLAB
Client ID:
CAD01626OR1 CAD01629OR1
Battelle Sample ID:
Battelle Batch ID:
Collection date
Dilution Factor
Sample Volume(l):
Units:
Sample Area:
DCM Area:
DTP Area:
Androstane Area:
X8989
00-436
09/28/00
2.00
2.00
ug/l
16188.718
15075.366
129.658
328.034
X8990
00-436
09/28/00
2.00
2.00
ug/l
16179.137
15075.366
126.239
271.413
SCA Sample Corrected Area:
Androstane Amount (ug):
OTP Amount (ug):
PAH RIS Amount (ug):
PAH SIS Amount (ug):
Dilution Factor:
655.660
20.200
20.218
3.005
3.636
2.000
706.119
20.200
20.218
3.005
3.636
2.000
AVE RF:
OTP RF:
MDL VALUE ug/l
0.989
1.076
78.40
0.989
1.076
78.40
OTP Surrogate Recovery:
Total Hydrocarbons:
73
36.00 J
86
48.31 J
NA-Not Applicable.
ND-Not Dectected
J- Analyte detected below the MDL
B - Analyte detected at a level greater
than 3* MDL in PB
ME - Significant matrix interference
estimated value
U Analyte not detected
& - QC value outside the accuracy or
data quality objective.
~ - QC value outside the accuracy or
precision data quality objective -but
meets contingency criteria
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX E
PAH LABORATORY-REPORTEDSAMPLE DATA WITH QC QUALIFIERS
-------
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston Cap
Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Dry Weight (g):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
Procedural Blank
YH91PB
00-441
NA
2.00
31.00
ng/g
0.20 J
0.05 U
0.03 U
0.05 U
0.03 J
0.05 U
0.02 J
0.03 J
0.03 U
0.03 U
0.04 U
0.03 U
0.04 U
0.02 U
0.04 U
0.04
75
68
78
LOAD #20
X8997
00-441
09/22/00
2.00
33.37
ng/g
1.26 J
0.05 U
0.03 U
0.12
0.53
0.04 J
0.32
0.22
0.11
0.22
0.09
0.08
0.05
0.04
0.04 U
0.08
73
75
84
SRM 1944
YH96SRM
00-441
NA
2.00
2.02
ng/g
1050.56
704.77
326.48
456.36
4812.64
1353.35
7864.70
7868.99
4028.55
5117.97
3703.69
3104.50
2963.20
2280.73
636.09
2130.81
61
76
82
LOAD #21
X8998
00-441
09/22/00
2.00
31.00
ng/g
1.34 J
0.02 J
0.07
0.16
0.47
0.07
0.14
0.13
0.05
0.11
0.06
0.05
0.03 J
0.02 U
0.04 U
0.11
63
72
87
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baiteiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston Cap
Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Dry Weight (g):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
LOAD #22
X8999
00-441
09/23/00
2.00
29.99
ng/g
0.98 J
0.04 J
0.04
0.09
0.67
0.08
1.32
0.85
0.42
0.66
0.44
0.36
0.19
0.21
0.07
0.24
68
73
84
LOAD #23
X9000
00-441
09/23/00
2.00
30.14
ng/g
0.95 J
0.23
0.04
0.16
0.71
0.26
0.87
0.89
0.69
1.12
0.44
0.54
0.47
0.34
0.14
0.39
64
69
79
LOAD #24
X9001
00-441
09/24/00
2.00
29.40
ng/g
1.87 J
0.05 U
0.11
0.14
1.54
0.12
4.54
2.09
1.09
1.43
0.50
0.44
0.23
0.14
0.06
0.16
65
72
79
LOAD #24
X9001 DUP
00-441
09/24/00
2.00
30.46
ng/g
2.45 J
0.05
0.07
0.14
1.38
0.15
3.43
1.81
0.83
1.11
0.57
0.54
0.32
0.27
0.08
0.32
73
77
83
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaltelie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
r
£
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
Procedural Blank
YH09PB
00-425
NA
2.00
2.00
ng/L
5.47 J
0.50 U
0.64 U
0.59 U
0.28 J
0.42 U
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
0.68 U
86
77
73
CAD012BFOR1 CAD012C30R1 CAD01390OR1 CAD01394OR1
X8406-F
00-425
09/09/00
2.00
2.00
ng/L
43.17
17.04
3.84
6.22
22.19
17.98
95.39
102.37
47.83
48.16
39.04
49.95
54.88
36.42
8.23
36.93
33 &
45 &
49 &
X8407-F
00-425
09/09/00
2.00
2.00
ng/L
286.01
131.35
34.08
47.98
171.65
155.17
690.77
687.16
415.79
394.01
319.34
381.08
436.74
294.56
73.06
291.48
56
74
77
X8436-F
00-425
09/11/00
2.00
2.00
ng/L
12.35 J
1.63
0.64 U
1.04
3.61
1.82
15.54
13.77
6.64
5.91
5.59
5.74
5.98
3.77
0.89 J
3.57
38
43 &
46 &
X8437-F
00-425
09/1 1/00
2.00
2.00
ng/L
30.26
5.73
1.01
2.79
10.22
7.27
33.35
35.99
17.08
19.99
17.63
18.60
18.74
13.15
3.27
13.07
50
75
81
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL
&= Value outside accuracy or
precision DQO.
-------
ClBatteile
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: 6464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01534OR1 CAD014D40R1 CAD014DBOR1 CAD0147DOR1 CAD01480OR1
X8567-F
00-425
09/15/00
2.00
2.00
ng/L
13.15 J
1.26
0.59 J
1.43
4.20
2.55
9.06
8.37
3.54
4.39
3.92
4.22
3.65
2.75
1.17 J
2.99
34 &
48 &
50 &
X8582-F
00-425
09/15/00
2.00
2.00
ng/L
16.23 J
1.21
0.60 J
1.15
3.55
2.41
13.12
10.50
4.18
5.68
4.64
4.70
4.36
2.92
0.81 J
3.29
63
76
79
X8583-F
00-425
09/15/00
2.00
2.00
ng/L
29.71
2.44
1.00
1.63
4.90
3.18
16.13
15.32
7.78
8.69
6.80
8.13
8.88
4.80
1.89
5.48
51
74
77
X8597-F
00-425
09/14/00
2.00
2.00
ng/L
16.62 J
1.57
0.56 J
1.01
2.77
1.75
8.60
8.70
3.56
4.97
3.84
4.83
3.05
2.96
0.70 J
3.00
43
52 &
53 &
X8598-F
00-425
09/14/00
2.00
2.00
ng/L
25.41
3.22
1.81
3.76
12.15
3.86
40.86
33.11
11.71
13.98
12.47
12.55
2.36
7.54
2.02
8.10
40
43 &
40 &
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBattelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01021OR1 CAD01024OR1 CAD01027OR1
YE17PB
00-352
NA
2.00
2.00
ng/L
4.04 J
1.00U
1.28 U
1.18 U
0.90 U
0.84 U
1.06 U
1.14 U
0.41 J
0.45 J
1.02U
1.04 U
1.56 U
2.20 U
2.50 U
1.36 U
84
92
102
X7962
00-352
09/06/00
2.00
1.00
ng/L
1 1 .39 J
1.90
1.54
2.20
2.47
2.76
17.76
14.61
3.29
5.12
2.61
1.55
2.06
1.17 J
2.50 U
1.83
67
87
99
X7963
00-352
09/06/00
2.00
1.00
ng/L
8.89 J
0.97 J
1.28U
1.18 U
1.64
1.27
8.85
9.23
2.16
3.05
1.02 U
1 .04 U
1.56 U
2.20 U
2.50 U
1.36U
64
80
91
X7964
00-352
09/06/00
2.11
2.00
ng/L
6.03 J
1.13
0.68 J
0.86 J
1.12
1.25
9.21
9.39
2.25
2.91
1.41
1.18
1.31 J
0.88 J
2.63 U
1.11 J
60
89
100
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C^Baftelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD0102AOR1 CAD0102DOR1 CAD0104AOR1 CAD0104DOR1
X7965
00-352
09/06/00
2.00
2.00
ng/L
5.97 J
1.29
1.07 J
1.09 J
1.51
1.81
17.62
19.04
2.46
3.42
1.87
1.53
1.56 J
0.84 J
2.50 U
1.06 J
72
94
105
X7966
00-352
09/06/00
2.00
2.00
ng/L
6.30 J
1.00
0.64 J
0.72 J
1.04
1.42
10.41
10.10
2.10
2.85
1.61
1.35
1.49 J
0.89 J
2.50 U
0.95 J
54
84
94
X7967
00-352
09/06/00
2.00
2.00
ng/L
6.81 J
1.72
2.15
1.95
1.73
3.38
20.20
15.68
2.83
4.07
2.32
1.73
1.63
1.06 J
2.50 U
1.13 J
57
89
100
X7968
00-352
09/06/00
2.00
2.00
ng/L
5.40 J
0.96 J
0.91 J
0.91 J
1.16
1.40 .
10.23
10.34
2.04
2.99
1.70
1.89
1.55 J
0.84 J
2.50 U
1.15 J
69
93
108
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C'Balfelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
CAD01050OR1 CAD01053OR1 CAD01056OR1 CAD01056OR1
X7969
00-352
09/06/00
2.00
2.00
ng/L
6.42 J
0.84 J
0.87 J
0.98 J
1.45
1.19
9.72
9.83
2.11
2.96
2.03
1.54
1.90
0.98 J
2.50 U
1.23 J
55
80
91
X7970
00-352
09/06/00
2.00
2.00
ng/L
4.98 J
0.76 J
0.77 J
0.74 J
1.02
0.94
8.35
8.19
1.32 J
2.12
0.97 J
0.94 J
1.07 J
2.20 U
2.50 U
1.36 U
61
82
88
X7971
00-352
09/06/00
2.00
1.00
ng/L
10.83 J
1.66
1.22 J
1.37
2.42
2.14
14.36
13.89
3.17
4.21
2.54
2.73
2.78
1.27 J
2.50 U
1.50
66
85
97
X7971DUP
00-352
09/06/00
2.00
1.00
ng/L
13.03 J
1.17
1.58
1.80
2.21
2.18
14.89
13.43
3.01
4.25
2.82
2.63
2.69
1.37 J
1.23 J
2.21
78
90
102
U= Analyte not detected.
J= Analyte detected below the
MDL
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD012ACOR1 CAD012AFOR1 CAD012B2OR1
YF10PB
00-371
NA
2.00
2.00
ng/L
4.40 J
0.50 U
0.64 U
0.59 U
0.20 J
0.42 U
0.53 U
0.57 U
0.83 U
0.09 J
0.51 U
0.52 U
0.78 U
1.1.0 U
1.25 U
0.40 J
72
76
85
X8403
00-371
09/09/00
2.00
1.00
ng/L
10.80 J
1.63
0.82 J
0.89 J
1.50
1.58
13.07
11.74
2.41
4.58
2.47
2.56
2.73
1.62 J
0.88 J
2.55
63
80
90
X8404
00-371
09/09/00
2.00
1.00
ng/L
12.54 J
1.23
0.52 J
0.64 J
1.17
1.43
10.46
9.61
2.15
3.11
2.09
2.07
1.91
1.03 J
2.50 U
1.84
63
82
89
X8405
00-371
09/09/00
2.00
2.00
ng/L
9.83 J
1.50
0.39 J
0.85
1.82
2.06
17.82
14.47
2.92
4.19
2.39
2.41
2.21
1.31
0.41 J
1.76
67
83
88
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Batreiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Pnenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD012BFOR1 CAD012C3OR1 CAD012C6OR1 CAD012CCOR1
X8406
00-371
09/09/00
2.00
2.00
ng/L
5.89 J
2.52
9.61
3.31
1.58
3.53
67.10
68.26
6.09
6.84
1.17
0.86
1.04
0.31 J
1.25 U
0.62 J
61
80
87
X8407
00-371
09/09/00
2.00
2.00
ng/L
5.08 J
3.33
20.46
10.76
2.76
12.07
155.43
186.19
15.50
14.96
1.77
1.31
1.53
0.30 J
1.25 U
0.62 J
65
85
92
X8408
00-371
09/09/00
2.00
2.00
ng/L
96.87
35.92
13.41
17.86
58.51
34.08
289.63
340.17
106.83
139.37
111.10
108.34
0.78 U
74.29
17.11
75.04
66
92
97
X8409
00-371
09/09/00
2.00
2.00
ng/L
36.23
12.90
3.60
5.49
19.64
8.89
104.72
118.17
31.27
42.70
35.58
34.71
1.64
23.30
5.15
24.32
68
89
93
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Banelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CAD012CFOR1 CAD012D2OR1 CAD012D6OR1 CAD012DCOR1
X8410
00-371
09/09/00
2.00
2.00
ng/L
43.43
18.56
4.95
7.46
25.20
21.15
117.51
126.29
57.10
63.88
56.50
58.21
55.63
40.72
9.30
40.23
59
84
90
X8411
00-371
09/09/00
2.00
2.00
ng/L
93.53
53.46
14.64
19.51
62.17
59.76
311.64
370.64
152.60
156.95
135.74
128.15
142.69
94.55
21.86
94.53
61
84
90
X8412
00-371
09/09/00
2.00
2.00
ng/L
15.00 J
6.59
1.50
2.43
5.84
6.54
49.87
58.15
16.38
16.68
12.25
12.32
13.35
7.89
1.88
8.81
63
85
89
X8413
00-371
09/09/00
2.00
2.00
ng/L
9.95 J
2.64
0.47 J
1.45
2.77
3.46
21.66
21.73
5.71
6.92
3.74
3.73
3.64
2.17
0.53 J
2.47
66
85
88
U= Analyte not detected.
J= Analyte detected below the
MDL
&= Value outside accuracy or
precision DQO.
-------
C-Batteiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
PI Dilution Factor:
Sample Volume (L):
Units:
---I
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
i. , Phenanthrene
Anthracene
Fluoranthene
Pyrene
^ Benzo(a)anthracene
Chrysene
" Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
t^ lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
, j Benzo(g,h,i)perylene
,-,.
Surrogate Recoveries (%):
fc" Naphthalene-d8
Phenanthrene-d10
"?-; Chrysene-d12
CAD012EOOR1 CAD012ECOR1 CAD012FOOR1 CAD012F4OR1
X8414
00-371
09/09/00
2.00
2.00
ng/L
61.04
32.06
15.85
14.91
37.03
39.04
253.53
310.29
94.27
93.08
70.98
77.23
71.81
48.95
11.36
51.21
66
85
90
X8415
00-371
09/09/00
2.00
2.00
ng/L
10.88 J
3.13
0.71
1.53
3.40
3.44
21.88
21.39
7.08
8.68
7.16
6.40
6.00
3.87
0.90 J
4.28
65
86
87
X8416
00-371
09/09/00
2.00
2.00
ng/L
13.42 J
3.71
1.30
2.08
4.79
4.92
34.21
39.01
10.95
11.82
9.37
9.32
9.80
5.78
1.40
6.29
63
83
83
X8417
00-371
09/09/00
2.00
2.00
ng/L
11.78 J
3.53
1.55
2.13
4.28
4.67
33.72
38.17
9.00
11.61
7.11
7.32
6.85
4.10
1.17 J
4.54
63
81
83
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CAD0130COR1 CAD0130FOR1 CAD01312OR1 CAD0131FOR1
X8418
00-371
09/10/00
2.00
2.00
ng/L
21.75
6.61
1.13
2.48
6.81
6.75
42.79
44.58
1 1 .66
15.10
11.24
12.25
10.65
6.66
1.70
7.37
72
84
85
X8419
00-371
09/10/00
2.00
2.00
ng/L
28.39
6.41
1.65
3.66
8.52
7.99
45.35
44.50
12.09
15.66
12.18
11.58
9.78
6.68
1.84
7.44
74
85
86
X8420
00-371
09/10/00
2.00
2.00
ng/L
23.12
7.60
1.76
3.33
9.29
8.30
49.72
49.43
13.69
17.85
14.17
14.07
10.36
8.17
1.84
8.89
68
83
85
X8421
00-371
09/10/00
2.00
2.00
ng/L
18.69 J
3.29
0.92
1.77
4.26
3.45
26.49
25.58
6.60
9.08
6.44
6.37
5.99
3.17
0.68 J
3.68
66
81
83
U= Analyte not detected.
J= Analyte detected below the
MDL
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01322OR1 CAD01322OR1
X8422
00-371
09/10/00
2.00
1.00
ng/L
18.25 J
3.07
1.54
2.19
3.93
3.18
23.60
22.29
5.75
7.13
5.40
5.40
5.34
2.45
1.07 J
3.34
63
80
79
X8422DUP
00-371
09/10/00
2.00
1.00
ng/L
17.83 J
3.27
1.18 J
1.65
4.01
3.40
23.84
22.37
5.94
8.62
5.66
6.51
5.55
2.33
2.50 U
3.26
64
76
77
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaftelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01325OR1 CAD0132BOR1 CAD0132EOR1 CAD0132EOR1
YF15PB
00-372
NA
2.00
2.00
ng/L
3.64 J
1.00 U
1.28 U
1.18U
0.90 U
0.84 U
0.35 J
0.49 J
1.52 J
1.79
0.77 J
0.69 J
1 .56 U
2.20 U
2.50 U
1 .36 U
66
71
81
X8423
00-372
09/10/00
2.00
1.00
ng/L
7.74 J
1.76
0.75 J
0.92 J
1.83
1.93
18.81
18.77
3.29
4.38
2.71
2.10
3.06
2.08 J
2.50 U
1.75
52
73
79
X8424
00-372
09/10/00
2.00
1.00
ng/L
25.69 J
8.14
1.89
9.60
33.35
26.64
47.93
49.23
36.74
95.07
13.83
18.65
16.41
9.21
2.19 J
10.11
56
74
86
X8425
00-372
09/10/00
2.00
1.00
ng/L
6.99 J
1.47
1.28 U
1.02 J
1.11
1.83
18.63
21.93
3.57
4.72
2.39
2.57
1.79
0.91 J
2.50 U
1.58
57
70
80
X8425DUP
00-372
09/10/00
2.00
1.00
ng/L
1 1 .34 J
3.52
0.96 J
1.65
3.73
3.96
28.81
32.14
7.35
8.50
6.36
6.78
6.68
3.64
2.50 U
4.04
54
72
83
U= Analyte not detected.
J= Analyte detected below the
MDL
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA1 1 DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01331OR1 CAD01334OR1 CAD01337OR1
YF74PB
00-393
NA
2.00
1.00
ng/L
10.93 J
0.34 J
1.28 U
0.89 J
1.00
0.84 U
1 .06 U
1.14U
1.66U
0.88 U
1.02 U
1.04U
1.56U
2.20 U
2.50 U
1 .36 U
64
69
77
X8426
00-393
09/10/00
2.00
1.00
ng/L
22.35 J
2.02
0.79 J
1.17 J
3.12
2.45
19.42
19.63
7.11
9.58
5.00
5.65
5.50
2.94
1.68 J
3.53
59
73
98
X8427
00-393
09/10/00
2.00
1.00
ng/L
34.09 J
3.66
0.89 J
1.62
5.70
4.13
34.04
35.08
9.73
13.04
9.21
10.53
9.91
5.27
2.12 J
6.45
58
75
88
X8428
00-393
09/10/00
2.00
2.00
ng/L
21.87
3.50
0.94
1.89
4.45
3.41
35.38
35.96
9.62
13.00
8.46
10.29
8.91
5.45
1.43
6.26
60
80
90
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h , i)pery lene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD0133AOR1 CAD01348OR1 CAD0134BOR1 CAD0134EOR1 CAD01371OR1
X8429
00-393
09/10/00
2.00
2.00
ng/L
13.30 J
1.72
0.75
1.38
13.71
3.05
45.72
137.21
6.11
8.28
4.16
5.40
5.19
3.42
1.08 J
7.48
61
81
89
X8430
00-393
09/10/00
2.00
2.00
ng/L
8.12 J
0.69
0.36 J
0.55 J
1.08
0.86
11.77
12.00
2.04
3.03
1.57
1.71
1.23
0.94 J
1.25 U
1.16
47
57 &
64
X8431
00-393
09/10/00
2.00
2.00
ng/L
1 1 .93 J
1.60
0.44 J
1.04
2.59
1.80
17.27
17.20
4.42
6.45
3.91
5.04
3.84
2.28
0.67 J
2.83
66
80
89
X8432
00-393
09/10/00
2.00
2.00
ng/L
11.68 J
2.09
0.68
1.44
2.62
3.14
25.52
25.46
5.22
7.20
4.24
5.12
4.60
2.65
0.78 J
3.28
65
81
88
X8433
00-393
09/10/00
2.00
2.00
ng/L
8.86 J
0.93
1.38
1.87
5.90
1.97
27.71
20.68
3.65
5.21
2.14
2.45
2.22
1.55
1.25 U
2.48
67
86
92
U= Analyte not detected.
J= Analyte detected below the
MDL
&= Value outside accuracy or
precision DQO.
-------
OBafteiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
CAD01376OR1 CAD0137AOR1 CAD01390OR1 CAD01394OR1 CAD01398OR1
X8434
' 00-393
09/10/00
2.00
2.00
ng/L
10.49 J
0.88
0.49 J
0.83
1.39
0.70
11.69
10.05
1.84
3.22
1.53
1.33
1.22
0.86 J
0.77 J
1.60
64
76
85
X8435
00-393
09/10/00
2.00
2.00
ng/L
11.61 J
1.09
0.61
0.87
1.41
1.00
13.49
11.63
2.05
4.03
1.84
2.30
1.00
1.34
1.25U
2.14
62
81
88
X8436
00-393
09/11/00
2.00
2.00
ng/L
9.58
0.89
0.99 J
1.25
1.94
1.07
43.97
30.92
2.66
3.18
0.47
0.53
0.78 U
1.10U
1.25 U
1.11
69
78
85
X8437
00-393
09/11/00
2.00
2.00
ng/L
8.68
0.70
0.64 U
0.95
0.64
0.91
22.46
19.94
1.92
2.74
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
1.03
62
81
89
X8438
00-393
09/11/00
2.00
2.00
ng/L
21.44
4.17
0.63
3.71
14.11
6.31
32.26
28.40
7.72
11.86
7.19
8.75
7.98
5.81
1.33
6.88
59
73
81
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD0139FOR1 CAD013A2OR1 CAD013A6OR1 CAD013AAOR1 CAD013BOOR1
X8439
00-393
09/11/00
2.00
2.00
ng/L
27.49 J
3.63
1.50 J
2.72
7.30
4.58
33.21
31.68
11.73
15.76
9.80
11.74
10.49
7.02
1.92 J
7.57
62
81
90
X8440
00-393
09/11/00
2.00
2.00
ng/L
24.49 J
3.20
1.56 J
2.21
6.58
4.32
30.89
29.08
9.30
12.81
7.40
9.52
8.41
6.18
1.66 J
6.54
64
81
90
X8441
00-393
09/11/00
2.00
2.00
ng/L
11.11 J
1.15
0.57
1.07
1.32
1.51
20.82
17.48
2.81
4.12
2.20
2.23
2.03
1.46
0.69 J
2.30
61
76
85
X8442
00-393
09/11/00
2.00
2.00
ng/L
12.02 J
1.90
0.62 J
1.20
2.57
2.01
21.49
19.34
4.70
6.77
3.90
5.00
3.89
2.70
0.75
3.57
61
77
85
X8443
00-393
09/11/00
2.00
2.00
ng/L
17.51 J
1.71
0.66
1.36
3.54
2.06
22.21
19.66
4.11
6.21
3.12
4.08
3.16
2.30
0.76
3.12
63
82
88
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
0Battelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD013B4OR1 CAD013C9OR1 CAD013C9OR1
X8444
00-393
09/11/00
2.00
2.00
ng/L
8.64 J
1.33
0.51
0.91
1.19
1.71
19.85
16.42
3.36
4.69
2.38
2.64
2.38
1.48
1.25 U
2.02
62
77
85
X8445
00-393
09/11/00
2.00
1.00
ng/L
14.80 J
1.64
1.28U
0.99 J
1.76
1.76
23.09
20.79
3.75
6.14
2.60
3.28
2.93
2.17 J
2.50 U
2.57
61
76
87
X8445DUP
00-393
09/11/00
2.00
1.00
ng/L
15.60 J
1.66
1 .28 U
1.18 U
2.14
2.15
26.06
22.16
3.72
6.10
2.71
3.31
2.82
1.88 J
2.50 U
3.44
66
81
91
U= Analyte not detected.
J= Analyte detected below the
MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaffeile
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01405OR1 CAD01408OR1 CAD0140BOR1
YG28PB
00-405
NA
2.00
2.00
ng/L
12.25 J
0.50 U
0.64 U
0.59 U
0.45 U
0.65
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10U
1.25 U
0.68 U
50
57 &
66
X8609
00-405
09/12/00
2.00
1.00
ng/L
17.38 J
1.00 U
1.28 U
1.18 U
1.07
2.93
13.31
12.40
2.14
3.07
1.91
1.74
1.54 J
2.20 U
2.50 U
1.52
56
61
76
X8610
00-405
09/12/00
2.00
1.00
ng/L
19.36 J
1.00 U
1.28 U
1.18 U
0.90 U
0.84 U
12.96
13.70
2.20
3.14
2.23
1.71
1.22 J
2.20 U
2.50 U
2.00
60
67
82
X8611
00-405
09/12/00
2.00
2.00
ng/L
10.85 J
0.81
1.28
0.80
1.01
2.41
25.76
20.92
2.69
3.50
2.01
1.57
1.27
0.73 J
1.25 U
1.18
59
69
83
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL
&= Value outside accuracy or
precision DQO.
-------
OBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01416OR1 CAD01419OR1 CAD0141COR1 CAD0141FOR1 CAD01422OR1
X8612
00-405
09/12/00
2.00
2.00
ng/L
15.56 J
1.41
0.64 U
0.59 U
1.98
3.21
24.48
21.11
4.28
6.85
4.08
3.23
2.54
1.90
1.25 U
2.19
63
73
88
X8613
00-405
09/12/00
2.00
2.00
ng/L
15.02 J
1.30
0.64 U
0.59 U
2.05
1.84
22.83
20.00
3.13
4.79
3.26
2.73
2.41
1.70
1.25 U
2.33
62
75
87
X8614
00-405
09/12/00
2.00
2.00
ng/L
14.50 J
1.29
0.64 U
0.59 U
1.75
2.05
25.13
20.64
3.38
4.85
3.44
2.80
2.71
1.61
1.25 U
2.13
61
72
85
X8615
00-405
09/12/00
2.00
2.00
ng/L
37.91
0.50 U
0.64 U
0.59 U
5.25
14.70
38.42
26.65
5.04
6.98
5.25
4.37
1.65
2.18
1.25 U
2.62
63
73
87
X8616
00-405
09/12/00
2.00
2.00
ng/L
17.91
1.86
1.35
1.45
3.43
3.59
29.88
26.82
5.01
8.66
5.54
4.80
3.31
2.53
1.25
3.93
62
72
87
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Batteiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)f I uoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-dB
Phenanthrene-d1 0
Chrysene-d12
CAD01425OR1 CAD01428OR1 CAD0142BOR1 CAD0142EOR1
X8617
00-405
09/12/00
2.00
2.00
ng/L
J 11.99 J
1.62
0.64 U
0.59 U
2.48
2.41
26.29
22.24
4.31
5.73
3.97
3.59
2.25
1.10U
U 1.25 U
2.52
70
80
93
X8618
00-405
09/12/00
2.00
2.00
ng/L
13.29 J
1.61
0.64 U
0.59 U
2.06
3.17
23.90
21.30
3.62
6.77
3.24
3.30
2.52
1.70
1.25 U
2.37
71
82
92
X8619
00-405
09/12/00
2.00
2.00
ng/L
9.20 J
1.16
0.64 U
0.59 U
1.44
2.22
27.60
23.16
3.15
6.16
2.72
2.07
2.00
1.29
1.25 U
1.72
66
76
87
X8620
00-405
09/12/00
2.00
2.00
ng/L
9.31 J
1.12
0.64 U
0.59 U
1.85
1.34
19.42
16.82
2.60
4.47
2.61
2.35
0.78 U
1.38
1.25 U
1.59
65
74
86
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaireiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenantnrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CADQ1436OR1 CAD01439OR1 CAD0143COR1 CAD0143COR1
X8621
00-405
09/12/00
2.00
2.00
ng/L
15.38 J
1.13
0.68
0.61
0.92
4.05
23.93
19.01
2.17
3.41
1.85
1.53
1.24
1.10 U
1.25 U
1.41
65
73
85
X8622
00-405
09/12/00
2.00
2.00
ng/L
9.00 J
0.94
0.64 U
0.59 U
1.36
1.76
14.11
14.49
2.48
3.64
2.20
1.78
1.60
1.15
1 .25 U
1.58
64
71
82
X8623
00-405
09/12/00
2.00
1.00
ng/L
23.35 J
1.00 U
1.28 U
1.18 U
0.90 U
0.84 U
15.14
13.79
1.62 J
3.35
2.40
2.17
1.56 U
2.20 U
2.50 U
1.36 U
80
82
92
X8623DUP
00-405
09/12/00
2.00
1.00
ng/L
16.10 J
1.00 U
1.28 U
1.18 U
0.90 U
0.84 U
12.85
11.33
1.82
3.44
1.61
1.19
2.58
2.20 U
2.50 U
1.36 U
66
67
75
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaifeile
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01469OR1 CAD0146COR1 CAD0146FOR1
YG33PB
00-406
NA
2.00
2.00
ng/L
11.11 J
0.50 U
0.64 U
0.59 U
0.45 U
0.42 U
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10U
1.25U
0.68 U
76
77
83
X8594
00-406
09/14/00
2.00
1.00
ng/L
35.39 J
2.24
2.55
2.36
2.81
2.44
11.66
10.75
5.00
5.22
2.84
3.21
3.57
2.56
1.67 J
3.19
64
72
88
X8595
00-406
09/14/00
2.00
1.00
ng/L
25.75 J
0.98 J
0.73 J
0.81 J
1.10
1.27
8.14
7.79
1.39 J
2.42
0.92 J
1.30
1 .38 J
0.71 J
2.50 U
1.54
58
70
80
X8596
00-406
09/14/00
2.00
2.00
ng/L
12.73 J
0.66
0.28 J
0.50 J
0.58
0.89
9.33
8.04
1.12
1.86
0.68
0.96
0.55 J
0.54 J
0.22 J
0.74
59
76
85
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
CftBaifelie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d1 2
CAD0147DOR1 CAD01480OR1 CAD01483OR1 CAD01486OR1 CAD01489OR1
X8597
00-406
09/14/00
2.00
2.00
ng/L
6.40 J
1.58
2.01
2.36
2.64
3.09
15.91
14.61
3.36
4.10
1.86
2.33
2.39
1.67
1.53
2.07
62
78
86
X8598
00-406
09/14/00
2.00
2.00
ng/L
9.72 J
1.11
3.15
1.45
0.50
2.74
53.18
36.44
3.21
3.95
0.48 J
0.46 J
0.49 J
1.10 U
1.25 U
0.56 J
65
80
89
X8599
00-406
09/14/00
2.00
2.00
ng/L
32.81
12.30
7.77
6.86
18.80
18.34
159.21
116.41
44.32
43.55
37.96
35.11
33.85
20.55
4.76
19.94
67
84
95
X8600
00-406
09/14/00
2.00
2.00
ng/L
46.14
11.53
13.36
14.20
37.04
29.20
200.21
138.15
56.71
81.45
26.70
37.34
32.16
21.45
4.91
20.17
69
81
89
X8601
00-406
09/14/00
2.00
2.00
ng/L
20.56
4.15
6.77
3.95
6.49
8.00
112.85
76.50
18.54
18.41
8.06
11.55
10.21
5.20
1.23 J
5.84
64
82
90
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CAD0148COR1 CAD0148FOR1 CAD01492OR1 CAD01495OR1 CAD0149DOR1
X8602
00-406
09/14/00
2.00
2.00
ng/L
9.99 J
3.12
2.61
2.15
5.24
4.85
93.18
65.34
13.03
21.27
5.38
8.09
5.08
3.20
0.72 J
3.53
11 &
98
111
X8603
00-406
09/14/00
2.00
2.00
ng/L
16.88 J
1.73
2.43
2.30
3.34
4.40
41.94
30.40
7.84
8.36
3.72
4.60
4.47
2.28
0.39 J
2.30
62
78
88
X8604
00-406
09/14/00
2.00
2.00
ng/L
25.62
2.02
2.19
1.90
2.83
3.84
44.28
32.90
8.21
8.76
3.90
5.57
5.11
2.82
0.63 J
3.13
57
76
86
X8605
00-406
09/14/00
2.00
2.00
ng/L
1 1 .86 J
1.29
1.19
1.38
2.05
2.69
34.98
26.05
4.92
5.96
2.10
2.58
2.53
1.45
0.26 J
1.34
52
76
87
X8606
00-406
09/14/00
2.00
2.00
ng/L
24.45
1.40
0.96
1.42
1.37
2.39
22.41
18.09
3.43
4.31
1.71
2.36
2.29
1.06 J
1.25 U
1.60
60
82
90
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CAD014AOOR1 CAD014A3OR1 CAD014BFOR1 CAD014C2OR1 CAD014C5OR1
X8607
00-406
09/14/00
2.00
2.00
ng/L
10.58 J
1.05
1.17
1.30
1.46
1.95
23.11
17.62
2.92
4.09
1.47
1.75
1.50
0.73 J
1.25 U
0.99
56
77
86
X8608
00-406
09/14/00
2.00
2.00
ng/L
13.72 J
4.44
16.53
9.18
14.94
9.79
101.34
104.59
13.55
12.34
5.80
7.75
9.77
4.19
0.94 J
5.62
62
78
85
X8579
00-406
09/15/00
2.00
2.00
ng/L
10.68 J
1.24
0.69
1.27
0.72
1.58
14.46
12.28
1.74
2.86
0.95
1.25
1.15
0.59 J
1.25 U
0.94
70
79
85
X8580
00-406
09/15/00
2.00
2.00
ng/L
8.40 J
1.07
1.40
1.29
0.70
1.56
14.12
11.73
1.39
2.08
0.62
0.63
0.75 J
1.10U
1.25 U
0.60 J
75
84
90
X8581
00-406
09/15/00
2.00
2.00
ng/L
8.77 J
0.89
1.35
1.08
0.78
1.23
12.53
10.73
1.33
2.33
0.71
0.77
0.74 J
0.37 J
1.25 U
0.70
72
82
87
U= Analyte not detected.
J= Analyte detected below the MDL.
&= Value outside accuracy or
precision DQO.
-------
Oeaireiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD014D4OR1 CAD014DBOR1 CAD014DBOR1
X8582
00-406
09/15/00
2.00
2.00
ng/L
8.41 J
0.99
2.21
1.64
0.44 J
1.60
25.61
18.10
1.57
2.29
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
0.68 U
67
80
85
X8583
00-406
09/15/00
2.00
1.00
ng/L
16.14 J
0.98 J
3.52
2.14
1.34
1.89
18.42
14.18
1.26 J
2.00
1.02 U
1.04 U
1.56 U
2.20 U
2.50 U
1.36 U
51
66
75
X8583DUP
00-406
09/15/00
2.00
1.00
ng/L
9.64 J
1.11
3.80
2.18
1.39
1.49
20.09
14.82
1.48 J
2.27
1.02 U
1.04 U
1.56 U
2.20 U
2.50 U
1.36U
58
74
82
U= Analyte not detected.
J= Analyte detected below the MDL
&= Value outside accuracy or
precision DQO.
-------
C'Batielle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
Procedural Blank CAD014DEOR1 CAD014E4OR1 CAD014E7OR1
YG38PB
00-407
NA
2.00
2.00
ng/L
21.45
0.50 U
0.64 U
2.36 B
7.05 B
0.42 U
8.19 B
35.93 B
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
3.19 B
72
77
88
X8584
00-407
09/15/00
2.00
1.00
ng/L
22.75 J
2.57
3.41
2.59
4.35
4.17
41.82
34.55
8.19
9.49
7.19
6.76
6.14
3.22
2.50 U
3.82
65
78
97
X8585
00-407
09/15/00
2.00
1.00
ng/L
15.19 J
1.51
2.09
2.01
2.14
2.26
29.94
24.67
4.20
6.24
3.59
2.77
3.07
1.67 J
2.50 U
1.77
60
79
93
X8586
00-407
09/15/00
2.00
2.00
ng/L
22.22
2.47
4.17
2.89
5.00
5.06
52.11
41.49
9.49
12.15
7.18
7.34
6.29
3.99
1.25 U
4.01
58
77
89
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneue
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD014EAOR1 CAD014EDOR1 CAD014F3OR1 CAD014F6OR1 CAD01511OR1
X8587
00-407
09/15/00
2.00
2.00
ng/L -
15.38 J
1.99
2.23
1.86
3.27
3.02
35.54
30.81
8.73
12.24
11.38
10.57
9.95
7.71
1.58
8.61
64
80
93
X8588
00-407
09/15/00
2.00
2.00
ng/L
12.98 J
1.38
0.64 U
0.59 U
1.65
1.56
18.75
16.94
3.44
4.73
3.18
2.80
2.49
1.71
1.25 U
1.43
66
79
90
X8589
00-407
09/15/00
2.00
2.00
ng/L
3.75 J
0.50 U
0.64 U
0.59 U
1.39
1.36
13.70
12.71
1.78
2.80
1.43
1.25
1.24
1.10U
1.25 U
0.68 U
16 &
87
101
X8590
00-407
09/15/00
2.00
2.00
ng/L
8.49 J
1.38
2.24
1.80
1.93
2.39
21.39
18.30
3.98
4.70
3.12
2.87
2.90
1.46
1.25U
1.71
66
76
90
X8591
00-407
09/15/00
2.00
2.00
ng/L
16.65 J
1.01
2.56
1.80
1.36
1.66
14.14
13.56
2.71
3.75
1.69
1.50
1.33
1.10 U
1.25 U
0.68 U
68
78
87
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL
&= Value outside accuracy or
precision DQO.
-------
Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-dB
Phenanthrene-d10
Chrysene-d12
CAD01514OR1 CAD0151AOR1 CAD01523OR1 CAD01526OR1 CAD01529OR1
X8592
00-407
09/15/00
2.00
2.00
ng/L
13.08 J
1.08
2.27
0.85
1.59
1.58
15.01
14.67
2.61
4.04
2.13
1.95
1.58
1.10U
1.25U
0.91
66
79
90
X8593
00-407
09/15/00
2.00
2.00
ng/L
15.30 J
1.23
1.75
1.04
2.83
1.68
13.20
13.45
2.41
4.02
2.67
2.42
2.21
1.10 U
1.25U
1.20
67
81
92
X8564
00-407
09/15/00
2.00
2.00
ng/L
13.08 J
0.99
1.17
0.84
3.25
2.01
16.51
14.49
2.50
4.57
2.35
2.14
1.82
1.10 U
1.25U
0.68 U
61
79
89
X8565
00-407
09/15/00
2.00
2.00
ng/L
9.63 J
0.83
1.17
0.82
1.42
1.59
11.94
11.61
1.98
2.90
1.88
1.32
1.31
1.10 U
1.25 U
0.68 U
57
78
90
X8566
00-407
09/15/00
2.00
2.00
ng/L
9.59 J
0.50 U
1.79
1.51
1.59
1.62
14.91
13.07
1.91
2.83
1.39
1.27
1.16
1.10 U
1.25 U
0.68 U
55
76
90
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBattelle
. - . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-cIS
Phenanthrene-d10
Chrysene-d12
CAD01534OR1 CAD01538OR1 CAD0153BOR1 CAD0153EOR1 CAD01541OR1
X8567
00-407
09/15/00
2.00
2.00
ng/L
9.97 J
0.50 U
1.23
1.12
0.45 U
0.42 U
16.15
13.48
1.00
1.78
0.51 U
0.52 U
0.78 U
1.10U
1.25 U
0.68 U
51
77
91
X8568
00-407
09/15/00
2.00
2.00
ng/L
18.31 J
2.79
7.02
4.94
8.96
7.22
43.64
34.32
11.57
17.84
7.47
7.91
6.48
3.18
1.25 U
3.56
53
79
95
X8569
00-407
09/15/00
2.00
2.00
ng/L
18.82 J
1.98
2.96
1.88
3.31
2.65
24.96
21 .60
5.45
6.51
5.08
5.00
4.42
2.36
1.25 U
2.83
67
85
97
X8570
00-407
09/15/00
2.00
2.00
ng/L
13.13 J
1.72
2.33
1.89
5.43
2.80
24.83
22.65
5.19
5.81
4.21
3.93
3.55
1.93
1.25U
2.10
71
86
99
X8571
00-407
09/15/00
2.00
2.00
ng/L
15.20J
1.96
3.36
1.91
2.45
2.17
18.94
16.53
4.00
5.27
3.18
3.54
3.46
2.42
1.25 U
2.76
61
76
82
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
ClBaireife
. . . Putting Technology To IVorfc
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01544OR1 CAD01547OR1 CAD01547OR1
X8572
00-407
09/15/00
2.00
2.00
ng/L
15.12 J
1.20
2.40
1.62
2.44
2.56
15.21
14.19
2.79
3.94
2.18
2.32
1.82
1.38
1.25U
1.57
67
77
84
X8573
00-407
09/15/00
2.00
1.00
ng/L
34.18 J
1.00U
1.28U
1.18 U
2.95
9.07
13.35
13.05
2.48
4.66
2.19
2.02
2.05
2.20 U
2.50 U
1.36 U
75
82
88
X8573DUP
00-407
09/15/00
2.00
1.00
ng/L
21 .42 J
1.00U
1.28U
1.18U
1.62
1.38
12.69
11.53
1.82
3.09
1.94
1.75
1.79
2.20 U
2.50 U
1.36U
66
73
72
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD0154COR1 CAD0154FOR1 CAD0155EOR1
YG43PB
00-408
NA
2.00
2.00
ng/L
13.45 J
0.50 U
0.64 U
0.59 U
0.45 U
0.42 U
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
0.68 U
74
75
82
X8574
00-408
09/15/00
2.00
1.00
ng/L
22.68 J
1.00 U
3.23
1.57
1.51
1.68
14.69
11.86
2.16
2.60
1.02 U
1.04 U
1.56 U
2.20 U
2.50 U
1.36 U
65
77
88
X8575
00-408
09/15/00
2.00
1.00
ng/L
11.99 J
1.00 U
2.44
1.47
1.71
1.69
12.83
11.38
2.01
3.27
1 .02 U
1 .04 U
1.56 U
2.20 U
2.50 U
1.36 U
61
73
82
X8576
00-408
09/16/00
2.00
2.00
ng/L
22.58
0.58
1.51
1.03
3.50
8.13
12.56
9.62
1.60
2.28
1.31
1.15
0.50 J
1.10 U
1.25 U
1.00
55
66
77
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaltelle
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recovery %:
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01561OR1 CAD01564OR1 CAD01564OR1
X8577
00-408
09/16/00
2.00
2.00
ng/L
23.63
0.70
1.06
0.89
1.69
3.93
11.91
9.96
2.14
3.12
1.96
1.50
1.09
1.11
1.25 U
1.59
61
74
90
X8578
00-408
09/16/00
2.00
1.00
ng/L
48.98
1.00 U
2.33
1.29
9.67
10.45
13.30
15.67
2.98
4.32
1 .02 U
1.04 U
1.56 U
2.20 U
2.50 U
1.36 U
49
67
90
X8578DUP
00-408
09/16/00
2.00
1.00
ng/L
105.10
1.00U
2.79
1.47
3.59
7.91
15.56
12.56
2.53
3.72
2:32
1.04U
1.56 U
2.20 U
2.50 U
1.36 U
53
70
91
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-dS
Phenanthrene-d1 0
Chrysene-d12
Procedural Blank CAD015ABOR1 CAD015BOOR1 CAD015B3OR1
YH01PB
00-422
NA
2.00
2.00
ng/L
7.05 J
0.50 U
0.64 U
0.09 J
0.21 J
0.42 U
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10U
1.25 U
0.68 U
74
69
70
X8863
00-422
09/20/00
2.00
1.00
ng/L
25.46 J
1.96
0.97 J
1.43
3.67
1.59
10.49
9.54
2.64
4.27
2.53
2.46
2.17
1.55 J
2.50 U
1.65
70
82
88
X8864
00-422
09/20/00
2.00
1.00
ng/L
15.52 J
1.34
0.75 J
0.88 J
1.67
2.93
9.61
8.57
2.15
3.43
2.10
2.98
2.96
1.11 J
2.50 U
1.30 J
74
69
67
X8865
00-422
09/20/00
2.00
2.00
ng/L
1 1 .09 J
0.58
0.37 J
0.49 J
0.53
2.06
6.70
6.10
0.90
1.32
0.59
0.45 J
0.56 J
1.10 U
1.25 U
0.40 J
53
65
73
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD015C2OR1 CAD015C5OR1 CAD015CBOR1 CAD015CEOR1
X8866
00-422
09/20/00
2.00
2.00
ng/L
22.41
2.07
0.87
1.36
3.44
5.04
22.35
21.37
5.12
7.46
6.16
6.05
2.25
3.17
0.86 J
3.59
56
72
78
X8867
00-422
09/20/00
2.00
2.00
ng/L
19.40 J
2.06
0.55 J
0.86
2.59
2.36
15.64
14.70
4.46
5.69
4.80
4.19
4.32
3.09
0.58 J
3.38
49
65
70
X8868
00-422
09/20/00
2.00
2.00
ng/L
24.21
2.52
0.93
1.98
4.59
7.44
22.30
21.41
6.46
9.03
6.23
6.36
5.19
3.70
0.79 J
4.02
49
63
64
X8869
00-422
09/20/00
2.00
2.00
ng/L
17.09 J
1.87
0.76
1.34
2.51
2.92
19.29
17.62
3.98
5.59
4.39
4.12
3.62
2.54
0.64 J
2.55
51
71
75
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C'Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d1 0
Chrysene-d12
CAD015D1OR1 CAD015D4OR1 CAD015D7OR1 CAD015DCOR1 CAD015DFOR1
X8870
00-422
09/20/00
2.00
2.00
ng/L
15.72 J
0.97
0.66
0.80
1.41
2.34
12.01
11.39
2.26
2.99
2.34
1.72
1.55
1.17
1.25 U
1.33
48
66
69
X8871
00-422
09/20/00
2.00
2.00
ng/L
21.72
1.84
0.98
1.35
3.84
3.29
19.41
17.62
4.68
7.20
5.21
4.67
3.73
2.32
0.64 J
2.80
48
64
72
X8872
00-422
09/20/00
2.00
2.00
ng/L
21.17
2.38
1.69
1.93
16.24
8.71
34.00
80.85
11.20
42.03
1 1 .22
8.46
9.04
5.04
1.22 J
7.52
58
69
84
X8873
00-422
09/20/00
2.00
2.00
ng/L
1 1 .05 J
1.42
0.59 J
0.91
2.30
1.60
12.86
12.17
3.27
4.86
3.41
3.13
1.69
1.80
0.46 J
1.85
50
70
74
X8874
00-422
09/20/00
2.00
2.00
ng/L
19.04 J
3.53
0.59 J
1.19
2.29
6.43
15.91
16.40
6.02
12.10
6.08
5.55
4.88
3.85
0.80 J
4.04
51
61
69
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
OBattelie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD015EFOR1 CAD015F2OR1 CAD015F5OR1 CAD015F5OR1
X8875
00-422
09/20/00
2.00
2.00
ng/L
1 1 .47 J
1.47
0.57 J
1.20
3.29
2.24
10.41
9.86
5.16
6.93
4.14
3.94
3.70
1.71
0.53 J
2.04
52
70
74
X8876
00-422
09/20/00
2.00
2.00
ng/L
12.57 J
1.23
0.63 J
0.82
1.66
2.85
11.40
9.56
2.86
4.01
2.86
2.52
2.13
1.13
1.25 U
1.34
46
64
71
X8877
00-422
09/20/00
2.00
1.00
ng/L
15.72 J
0.77 J
1.14 J
1.57
2.31
1.62
8.41
7.29
1.48 J
2.46
1.45
1.63
1.48 J
0.97 J
2.50 U
1.10J
60
71
75
X8877-DUP
00-422
09/20/00
2.00
1.00
ng/L
24.52 J
1.71
0.85 J
2.12
3.03
3.79
12.27
10.47
3.76
4.49
2.86
2.72
3.23
1.31 J
2.50 U
1.34 J
54
72
76
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
Procedural Blank CAD01610OR1 CAD01613OR1 CAD01616OR1
YH64PB
00-436
NA
2.00
2.00
ng/L
10.12 J
0.50 U
0.64 U
0.59 U
0.36 J
0.80
0.53 U
0.57 U
0.83 U
0.44 U
0.51 U
0.52 U
0.78 U
1.10 U
1.25 U
0.68 U
73
76
89
X8982
00-436
09/28/00
2.00
1.00
ng/L
18.88 J
2.03
3.96
2.20
3.34
2.84
13.95
13.50
3.58
4.78
3.55
2.76
3.78
1.84 J
2.50 U
1.94
64
76
94
X8983
00-436
09/28/00
2.00
1.00
ng/L
19.95 J
1.25
2.66
1.83
2.27
2.19
14.83
12.92
2.26
3.78
2.79
2.07
2.42
1 .29 J
2.50 U
1.44
63
74
87
X8984
00-436
09/28/00
2.00
2.00
ng/L
9.35 J
1.03
2.12
1.72
1.91
1.43
12.86
12.70
2.13
3.40
2.03
1.88
1.86
0.85 J
1.25 U
1.12
60
78
91
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL.
&= Value outside accuracy or
precision DQO.
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01619OR1 CAD0161COR1 CAD01620OR1 CAD01623OR1
X8985
00-436
09/28/00
2.00
2.00
ng/L
8.35 J
0.91
1.77
1.26
1.96
1.51
11.80
11.67
2.31
3.22
2.04
1.90
1.94
0.96 J
0.35 J
1.19
57
75
89
X8986
00-436
09/28/00
2.00
2.00
ng/L
8.54 J
1.03
2.18
1.46
1.61
1.39
15.11
13.09
2.10
2.90
1.57
1.29
1.43
0.78 J
1.25 U
0.95
64
77
81
X8987
00-436
09/28/00
2.00
2.00
ng/L
9.41 J
0.78
2.11
1.32
1.02
1.07
11.65
11.04
1.32
2.20
1.09
0.89
1.15
0.64 J
1.25 U
0.69
66
80
92
X8988
00-436
09/28/00
2.00
2.00
ng/L
10.13 J
0.72
2.09
1.08
1.05
1.14
11.63
11.11
1.21
2.05
0.92
0.87
0.69 J
0.38 J
1.25 U
0.62 J
70
82
96
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL
&= Value outside accuracy or
precision DQO.
-------
Oeaiteiie
. . . Putting Technology To Work
Project Name: WA3-26 (Boston
Cap Project)
Project Number: G464426-
EPA11DUXLAB
Client ID:
Lab ID:
Batch ID:
Sample Collection Date:
Dilution Factor:
Sample Volume (L):
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anth racene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(1 ,2,3-c,d)pyrene
Dibenz(a,h)anthracene
Benzo(g,h,i)perylene
Surrogate Recoveries (%):
Naphthalene-d8
Phenanthrene-d10
Chrysene-d12
CAD01626OR1 CAD01629OR1 CAD0162COR1 CAD0162COR1
X8989
00-436
09/28/00
2.00
2.00
ng/L
7.53 J
0.72
1.56
1.26
1.14
1.37
9.84
10.00
1.30
2.05
0.99
1.07
1.02
0.56 J
1.25 U
0.60 J
51
66
74
X8990
00-436
09/28/00
2.00
2.00
ng/L
7.14 J
1.32
3.14
1.69
2.33
1.77
15.30
14.67
2.80
3.58
2.17
1.92
2.06
1.16
1.25 U
1.22
67
79
92
X8991
00-436
09/28/00
2.00
1.00
ng/L
1 1 .24 J
0.89 J
1.88
1.39
1.21
1.60
12.06
12.15
1 .28 J
2.23
1.02 U
1.04 U
0.84 J
2.20 U
2.50 U
0.72 J
67
69
80
X8991DUP
00-436
09/28/00
2.00
1.00
ng/L
13.53 J
1.04
2.62
1.45
1.47
1.73
13.78
13.86
1.87
2.95
1.60
1.29
1.41 J
2.20 U
2.50 U
0.82 J
68
75
85
U= Analyte not detected.
J= Analyte detected below the
Sample Specific MDL
&= Value outside accuracy or
precision DQO.
-------
EPA/540/R-05/014
Evaluatin of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX F
PCB LABORATORY-REPORTED SAMPLE DATA WITH QC QUALIFIERS
-------
-------
dBattelle
. . . Putting Technology To Work
Project Name WA3-26 Boston Cap Project
Project Number G464426-EPA11DUXLAB
Client ID
LOAD #20
LOAD #21
LOAD #22
Field Sample Data
LOAD #23
J - Analyte detected below the ssMDL.
U - Analyte not detected.
& - QC value outside the accuracy or precision DQO.
LOAD #24
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Dry Wt. (g)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8997-ECD
00-441
22-Sep-OO
2.000
33.37
ng/g - Dry Wt.
0.15 U
0.07 U
0.10 U
0.09 U
0.10 U
0.11 U
0.09 U
0.08 U
0.10 U
0.17 U
0.09 U
0.13 U
0.09 U
0.09 U
0.08 U
0.08 U
0.08 U
0.08 U
99
87
X8998-ECD .
00-441
22-Sep-OO
2.000
31.00
ng/g - Dry Wt.
0.16 U
0.07 U
0.11 U
0.10 U
0.10 U
0.11 U
0.10 U
0.09 U
0.11 U
0.18 U
0.09 U
0.14 U
0.09 U
0.10 U
0.09 U
0.09 U
0.08 U
0.09 U
96
91
X8999-ECD
00-441
23-Sep-OO
2.000
29.99
ng/g - Dry Wt.
0.16 U
0.08 U
0.11 U
0.10 U
0.11 U
0.12 U
0.10 U
0.09 U
0.12 U
0.19 U
0.10 U
0.14 U
0.10 U
0.10 U
0.09 U
0.09 U
0.09 U
0.09 U
97
92
X9000-ECD
00-441
23-Sep-OO
2.000
30.14
ng/g - Dry Wt.
0.16 U
0.08 U
0.11 U
0.10 U
0.11 U
0.12 U
0.10 U
0.09 U
0.12 U
0.19 U
0.10 U
0.14 U
0.10 U
0.10 U
0.09 U
0.09 U
0.09 U
0.09 U
104
97
X9001-ECD
00-441
24-Sep-OO
2.000
29.40
ng/g - Dry Wt.
0.17 U
0.08 U
0.11 U
0.10 U
0.11 U
0.12 U
0.10 U
0.09 U
0.12 U
0.19 U
0.10 U
0.15 U
0.10 U
0.10 U
0.10 U
0.09 U
0.09 U
0.10 U
102
94
Prepared by Thorn 7/26/01
S00441ECD
-------
Baneiie
Field Sample Data
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD012BFOR1
CAD012C3OR1
CAD01390OR1
CAD01394OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCS 105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Total PCB
Surrogate Recoveries:
PCB34
PCB112
X8406-F-ECD
00-425
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
0.37 J
0.40 J
0.86 U
0.46 J
0.69 U
0.60
1.43
0.44 J
0.80 U
1.83
2.11
0.97
0.46 J
0.65 U
0.73 U
0.76 U
58
56
X8407-F-ECD
00-425
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
2.53
3.27
6.41
4.15
8.64
3.99
9.56
1.91
12.98
12.21
10.51
3.81
2.97
0.59 J
0.32 J
0.39 J
89
79
X8436-F-ECD
00-425
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.13 J
0.89 U
0.11 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.26 J
0.25 J
0.65 U
0.73 U
0.76 U
36 &
34&
X8437-F-ECD
00-425
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.62 J
0.20 J
0.48 J
0.37
0.39 J
0.84 U
1.69
0.71
0.62
0.53 J
0.84
0.45 J
0.73 U
0.76 U
86
82
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the accuracy
or precision DQO.
Prepared by Desreuisseau 7/26/01
F00425ECD
-------
OBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01534OR1
CAD014D4OR1
CAD014DBOR1
CAD0147DOR1
CAD014800R1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Total PCB
Surrogate Recoveries:
PCB34
PCB112
X8567-F-ECD
00-425
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.25 J
0.09 J
0.21 J
0.35 U
0.20 J
0.84 U
0.80 U
0.64 U
0.61 U
0.39 J
0.52 U
0.65 U
0.73 U
0.76 U
59
57
X8582-F-ECD
00-425
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
0.09 J
0.13 J
0.30 J
0.09 J
0.21 J
0.17 J
0.35 J
0.84 U
0.38 J
0.37 J
0.86
6.15
0.20 J
0.11 J
0.73 U
0.76 U
9.39
94
89
X8583-F-ECD
00-425
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.53 J
0.20 J
0.58 J
0.40 J
0.82 J
1.68 U
0.78 J
0.87 J
1.43
1.43
0.61 J
0.11 J
1.46 U
1.52 U
7.74
86
84
X8597-F-ECD
00-425
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
0.12 J
0.87 U
0.21 J
0.89 U
0.22 J
0.16 J
0.30 J
0.84 U
0.60 J
0.33 J
0.94
0.53 J
0.21 J
0.05 J
0.73 U
0.76 U
3.65
67
63
X8598-F-ECD
00-425
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
0.20 J
0.20 J
0.45 J
0.15 J
0.60 J
0.27 J
0.58
0.12 J
1.34
0.65
0.92
0.73
0.26 J
0.12 J
0.73 U
0.76 U
6.58
62
60
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the accuracy
or precision DQO.
Prepared by Desreuisseau 7/26/01
F00425ECD
-------
OBauene
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID CAD01021OR1
Field Sample Data
CAD01024OR1
CAD01027OR1
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
CAD0102AOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X7962-ECD
00-352
06-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.79 U
1.37U
0.69 U
1.04 U
1.68 U
1 .59 U
1.28U
1.22 U
1.15U
1.03 U
1.30 U
1.46 U
1.52 U
95
109
X7963-ECD
00-352
06-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.79 U
1.37U
0.69 U
1.04 U
1.68 U
1.59 U
1.28 U
1.22 U
1.15 U
1.03 U
1 .30 U
1.46 U
1.52U
83
98
X7964-ECD
00-352
06-Sep-OO
2.106
2.00
ng/L
10.11 U
0.88 U
1.09 U
0.92 U
0.91 U
0.94 U
0.72 U
0.36 U
0.55 U
0.88 U
0.84 U
0.67 U
0.64 U
0.61 U
0.54 U
0.69 U
0.77 U
0.80 U
100
114
X7965-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60
0.83
1.04
0.87
0.86
0.89
0.69
0.35
0.52
0.84
0.80
0.64
0.61
0.58
0.52
0.65
0.73
0.76
93
105
Prepared by Thorn 7/26/01
W00352ECD
-------
T,
OBafeOe
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD0102DOR1
CAD0104AOR1
CAD0104DOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
U
X7966-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
99
106
X7967-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
94
106
X7968-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
95
110
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Thorn 7/26/01
W00352ECD
-------
OBaUefle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01050OR1
CAD01053OR1
CAD01056OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X7969-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
85
98
X7970-ECD
00-352
06-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
90
100
X7971-ECD
00-352
06-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66U
2.08 U
1.74 U
1.72 U
1.79 U
1.37U
0.69 U
1.04 U
1.68 U
1.59 U
1.28U
1.22 U
1.15 U
1.03 U
1.30 U
1.46U
1.52 U
94
104
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Thorn 7/26/01
W00352ECD
-------
OBaffefie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
3AD012ACOR1 CAD012AFOR1 CAD012B2OR1
CAD012BFOR1
CAD012C3OR1 CAD012C6OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8403-ECD
00-371
09-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
75
89
X8404-ECD
00-371
09-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
74
89
X8405-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
, 0.65 U
0.73 U
0.76 U
118
54
X8406-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
91
93
X8407-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
93
95
X8408-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
O'.m U
3.36
1.17
2.98
0.50 J
4.29
4.00
0.61 U
1.63
0.82
0.33 J
0.73 U
0.76 U
97
90
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00371ECD
-------
Barrel le
. Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD012CCOR1 CAD012CFOR1 CAD012D2OR1 CAD012D6OR1 CAD012DCOR1 CAD012EOOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8409-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
1.10
0.36
1.05
0.84 U
2.24
1.40
0.61 U
0.91
0.32 J
0.65 U
0.73 U
0.76 U
84
95
X8410-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.75 J
0.33 J
1.29
0.53
1.24
0.84 U
6.98
2.04
0.61 U
1.67
0.70
0.65 U
3.18
0.76 U
92
92
X8411-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
1.09
1.73
1.20
3.73
1.32
3.11
0.61 J
6.04
4.22
0.61 U
2.06
1.03
0.21 J
0.24 J
0.13 J
97
86
X8412-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.56 J
0.89 U
0.41 J
0.14 J
0.44 J
0.84 U
3.56
0.48 J
0.61 U
0.33 J
0.52 U
0.65 U
0.09 J
0.76 U
86
99
X8413-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.96
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
86
95
X8414-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.69 J
0.89 U
0.52 J
0.19 J
0.49 J
0.84 U
2.09
0.75
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
87
95
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00371ECD
-------
llBaffelfe
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD012ECOR1
CAD012FOOR1
CAD012F4OR1
CAD0130COR1 CAD0130FOR1
CAD01312OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8415-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.39 J
0.35 U
0.52 U
0.84 U
1.83
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
86
97
X8416-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.57 J
0.89 U
0.47 J
0.23 J
0.45 J
0.84 U
2.33
0.58 J
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
88
100
X8417-ECD
00-371
09-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.78 J
0.89 U
0.23 J
0.23 J
0.29 J
0.84 U
1.79
0.51 J
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
90
88
X8418-ECD
00-371
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
1.58
0.81 J
2.45
0.77
2.17
0.32 J
4.07
2.98
0.61 U
1.60
0.79
0.22 J
0.26 J
0.76 U
95
83
X8419-ECD
00-371
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.82 J
0.89 U
0.54 J
0.19 J
0.46 J
0.84 U
1.65
0.82
0.61 U
0.44 J
0.52 U
0.65 U
0.73 U
0.76 U
89
89
X8420-ECD
00-371
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.70 J
0.89 U
0.63 J
0.21 J
0.40 J
0.84 U
1.71
0.84
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
81
89
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00371ECD
-------
OBafleUe
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD0131FOR1
CAD01322OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8421-ECD
00-371
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.70 J
0.89 U
0.31 J
0.16 J
0.28 J
0.84 U
1.12
0.45 J
0.61 U
0.34 J
0.52 U
0.65 U
0.73 U
0.76 U
84
90
X8422-ECD
00-371
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.64
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
87
88
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00371ECD
-------
T":
C-Baneiie
. . . Putting Technology To Work
Project Name WA3-26 Boston Cap Project
Project Number G464426-EPA11DUXLAB
Field Sample Data
Client ID
CAD01325OR1
CAD0132BOR1
CAD0132EOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8423-ECD
00-372
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.79 U
1.37 U
0.69 U
1.04 U
1.68 U
1.59 U
1.28 U
1.22 U
1.15 U
1.03 U
1.30 U
1.46 U
1.52 U
85
94
X8424-ECD
00-372
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.79 U
1.37 U
0.69 U
1 .04 U
1 .68 U
1.59 U
1.28 U
1.22 U
1.15 U
1.03 U
1.30 U
1.46 U
1.52 U
82
99
X8425-ECD
00-372
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1 .72 U
1.79 U
1.37 U
0.69 U
1.04 U
1.68 U
1.59 U
1.28 U
1.22 U
1.15 U
1.03 U
1 .30 U
1.46 U
1.52 U
86
97
J - Analyte detected below the ssMDL.
U - Analyte not detected.
& - QC value outside the accuracy or precision DQO.
Prepared by Thorn 7/26/01
W00372ECD
-------
OBatteiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01331OR1 CAD01334OR1 CAD01337OR1 CAD0133AOR1 CAD01348OR1 CAD0134BOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCS 128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8426-ECD
00-393
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
0.35 J
0.86 J
1.78 U
0.58 J
0.70 U
0.41 J
1.68 U
1.60 U
1.28 U
1.22 U
0.40 J
1.04 U
0.19 J
1.46 U
1.52 U
89
87
X8427-ECD
00-393
10-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
0.61 J
0.70 U
0.52 J
1.68 U
1.60 U
1.28 U
1.22 U
0.35 J
1.04 U
0.25 J
1.46 U
1.52 U
83
86
X8428-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.24 J
0.62 J
0.17 J
0.57 J
0.16 J
0.46 J
0.07 J
0.79 J
0.55 J
0.61 U
0.52 J
0.10 J
0.65 U
0.73 U
0.76 U
86
85
X8429-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.58 J
1.04 U
0.20 J
0.55 J
0.15 J
0.28 J
0.35 U
0.28 J
0.84 U
0.29 J
0.64 U
0.61 U
0.33 J
0.52 U
0.65 U
0.73 U
0.76 U
79
81
X8430-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.16 J
0.39 J
0.89 U
0.24 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
73
73
X8431-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.15 J
0.41 J
0.89 U
0.33 J
0.35 U
0.26 J
0.84 U
0.80 U
0.64 U
0.61 U
0.22 J
0.52 U
0.65 U
0.73 U
0.76 U
90
87
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00393ECD
-------
Oeaflefle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD0134EOR1
CAD01371OR1
CAD01376OR1 CAD0137AOR1
CAD01390OR1
CAD01394OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8432-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.49 J
0.89 U
0.44 J
0.35 U
0.29 J
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
90
85
X8433-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.18 J
0.47 J
0.89 U
0.18 J
0.35 U
0.16 J
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
91
91
X8434-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.18 J
0.50 J
0.89 U
0.24 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.18 J
0.52 U
0.65 U
0.73 U
0.76 U
95
90
X8435-ECD
00-393
10-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.51 J
0.89 U
0.20 J
0.35 U
0.17 J
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
83
84
X8436-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.24 J
0.68 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
98
84
X8437-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.29 J
0.52 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.25 J
0.76 U
110
84
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00393ECD
-------
CIBatrelle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01398OR1 CAD0139FOR1 CAD013A2OR1 CAD013A6OR1 CAD013AAOR1 CAD013BOOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8438-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.25 J
0.59 J
0.17 J
0.52 J
0.13 J
0.36 J
0.84 U
0.80 U
0.44 J
0.61 U
0.37 J
0.52 U
0.08 J
0.73 U
0.76 U
90
88
X8439-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.26 J
0.61 J
0.19 J
0.57 J
0.22 J
0.43 J
0.84 U
0.39 J
0.60 J
0.61 U
0.36 J
0.12 J
0.65 U
0.73 U
0.76 U
95
89
X8440-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.22 J
0.64 J
0.23 J
0.56 J
0.35 U
0.41 J
0.84 U
0.55 J
0.64 U
0.61 U
0.34 J
0.11 J
0.65 U
0.73 U
0.76 U
99
90
X8441-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.33 J
1.04 U
0.20 J
0.50 J
0.13 J
0.33 J
0.35 U
0.20 J
0.84 U
0.80 U
0.64 U
0.61 U
0.24 J
0.52 U
0.23 J
0.73 U
0.76 U
89
88
X8442-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.62 J
0.27 J
0.20 J
0.59 J
0.16 J
0.32 J
0.35 U
0.31 J
0.84 U
0.47 J
0.64 U
0.61 U
0.36 J
0.52 U
0.06 J
0.73 U
0.76 U
97
89
X8443-ECD
00-393
11-Sep-OO
2.000
2.00
ng/L
9.60 U
0.68 J
1.04 U
0.16 J
0.46 J
0.89 U
0.34 J
0.35 U
0.23 J
0.84 U
0.40 J
0.64 U
0.61 U
0.25 J
0.52 U
0.19 J
0.73 U
0.76 U
87
84
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00393ECD
-------
OBaflene
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD013B4OR1 CAD013C9OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCS 153
PCB170
PCS 180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8444-ECD
00-393
11-Sep-OO
2.000 '
2.00
ng/L
9.60 U
0.41 J
1.04 U
0.17 J
0.45 J
0.89 U
0.21 J
0.35 U
0.16 J
0.84 U
0.25 J
0.64 U
0.61 U
0.18 J
0.52 U
0.65 U
0.73 U
0.76 U
91
84
X8445-ECD
00-393
11-Sep-OO
2.000
1.00
ng/L
19.20 U
0.63 J
2.08 U
0.21 J
0.68 J
1.78 U
0.38 J
0.70 U
0.23 J
1.68 U
0.32 J
1.28 U
1.22 U
0.61 J
0.19 J
1.30 U
1.46 U
1.52 U
90
84
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00393ECD
-------
OBaftelle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01405OR1 CAD01408OR1 CAD0140BOR1 CAD01416OR1 CAD01419OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCS 138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PQB112
X8609-ECD
00-405
1 2-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
86
89
X8610-ECD
00-405
12-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
80
87
X8611-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
77
82
X8612-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1 .04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
88
96
X8613-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.74 J
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
84
86
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00405ECD
-------
OBaflefle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD0141COR1 CAD0141FOR1 CAD01422OR1 CAD01425OR1 CAD01428OR1 CAD0142BOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8614-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04.U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
20 &
23 &
X8615-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
2.61
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
84
91
X8616-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.64 J
0.89 U
0.36 J
0.35 U
0.25 J
0.84 U
2.85
0.64 U
0.61 U
2.34
1.32
0.65 U
0.73 U
0.76 U
90
99
X8617-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
2.83
0.69 U
0.35 U
0.40 J
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
151 &
19 &
X8618-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.72 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.86
0.64 U
0.61 U
0.72
0.52 U
0.65 U
0.73 U
0.76 U
86
93
X8619-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.55 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.86
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
62
69
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00405ECD
-------
QBaflefle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD0142EOR1
CAD01436OR1
CAD01439OR1 CAD0143COR1 CAD0143COR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8620-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.49 J
0.89 U
0.34 J
0.35 U
0.39 J
0.84 U
3.45
0.64 U
1.19
1.34
0.52 U
1.67
8.52
6.40
100
86
X8621-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.45 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
1.11
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
87
91
X8622-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.49 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.99
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
86
88
X8623-ECD X8623DUP-ECD
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.47 J
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
89
93
00-405
12-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.43 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.47 J
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
79
83
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00405ECD
-------
CIBairelle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01469OR1 CAD0146COR1 CAD0146FOR1 CAD0147DOR1 CAD01480OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8594-ECD
00-406
14-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
28.30
1.04 U
1.30 U
1.46 U
1.52 U
73
80
X8595-ECD
00-406
14-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
11.25
1.04 U
1.30 U
1.46 U
1.52 U
84
90
X8596-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
90
96
X8597-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
55
63
X8598-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
96
102
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00406ECD
-------
llBaffelle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01483OR1
CAD01486OR1
CAD01489OR1 CAD0148COR1 CAD0148FOR1 CAD01492OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8599-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.67 J
0.74 J
0.42 J
1.21
0.45
1.24
0.84 U
3.51
1.77
0.61 U
4.48
0.52 U
0.65 U
0.73 U
0.76 U
86
99
X8600-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.75 J
1.09
0.65 J
1.49
0.58
1.21
0.84 U
2.98
1.82
0.61 U
1.04
0.39 J
0.65 U
0.73 U
0.76 U
93
94
X8601-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.91
0.89 U
0.76
0.20 J
0.47 J
0.84 U
2.06
0.76
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
96
103
X8602-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.59 J
0.89 U
0.42 J
0.09 J
0.36 J
0.84 U
2.31
0.39 J
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
94
100
X8603-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.55 J
0.89 U
0.36 J
0.35 U
0.43 J
0.84 U
1.59
0.64 U
0.61 U
0.26 J
0.52 U
0.65 U
0.73 U
0.76 U
84
96
X8604-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.70 J
0.89 U
0.40 J
0.10 J
0.39 J
0.84 U
1.75
0.42 J
0.61 U
0.49 J
0.47 J
0.65 U
0.73 U
0.76 U
84
97
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00406ECD
-------
OBaffelle
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01495OR1 CAD0149DOR1 CAD014AOOR1 CAD014A3OR1 CAD014BFOR1 CAD014C2OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8605-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.47 J
0.89 U
0.25 J
0.35 U
0.16 J
0.84 U
1.31
0.64 U
0.61 U
0.21 J
0.52 U
0.65 U
0.73 U
0.76 U
86
102
X8606-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.43 J
0.89 U
0.23 J
0.35 U
0.13 J
0.84 U
1.02
0.64 U
0.61 U
0.29 J
0.52 U
0.65 U
0.73 U
0.76 U
78
90
X8607-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.49 J
0.89 U
0.17 J
0.35 U
0.12 J
0.84 U
0.80 U
0.64 U
0.61 U
0.41 J
0.52 U
0.65 U
0.73 U
0.76 U
83
94
X8608-ECD
00-406
14-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
1.84
1.12
0.89 U
0.28 J
0.35 U
0.25 J
0.84 U
1.13
0.64 U
0.61 U
0.58 U
0.31 J
0.65 U
0.73 U
0.76 U
86
90
X8579-ECD
00-406
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.35 J
0.89 U
0.33 J
0.35 U
0.52 U
0.84 U
0.90
0.64 U
0.61 U
2.26
1.89
0.65 U
0.73 U
0.76 U
91
96
X8580-ECD
00-406
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.33 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
1.35
0.64 U
0.61 U
0.31 J
0.52 U
0.65 U
0.73 U
0.76 U
85
95
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00406ECD
-------
OBaflelfe
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD014C5OR1 CAD014D4OR1 CAD014DBOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8581-ECD
00-406
15-Sep-OO
2.000 '
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.53 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.77 J
0.64 U
0.61 U
0.21 J
0.52 U
0.65 U
0.73 U
0.76 U
84
89
X8582-ECD
00-406
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.47 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
94
96
X8583-ECD
00-406
1 5-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.88 J
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1 .04 U
1.30 U
1.46 U
1.52 U
94
97
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00406ECD
-------
0Baltelie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD014DEOR1 CAD014E4OR1 CAD014E7OR1 CAD014EAOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8584-ECD
00-407
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1 .30 U
1.46 U
1.52 U
86
97
X8585-ECD
00-407
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1 .04 U
1.30 U
1.46 U
1.52 U
86
97
X8586-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.51 J
0.89 U
0.49 J
0.35 U
0.36 J
0.84 U
0,38 J
0.64 U
0.48 J
0.28 J
0.52 U
0.65 U
0.73 U
0.76 U
91
100
X8587-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.49 J
0.89 U
0.56 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.41 J
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
95
103
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00407ECD
-------
llBaiteiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD014EDOR1
CAD014F3OR1
CAD014F6OR1
CAD01511OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8588-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.27 J
0.32 J
0.52 U
0.65 U
0.73 U
0.76 U
94
103
X8589-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.13 J
0.21 J
0.52 U
0.65 U
0.73 U
0.76 U
89
98
X8590-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.28 J
0.31 J
0.52 U
0.65 U
0.73 U
0.76 U
91
97
X8591-ECD
00-407
1 5-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.23 J
0.22 J
0.52 U
0.65 U
0.73 U
0.76 U
84
92
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00407ECD
-------
T?
i.
flBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01514OR1 CAD0151AOR1
CAD01523OR1
CAD01526OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8592-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.36 J
0.89 U
0.25 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.29 J
0.19 J
0.52 U
0.65 U
0.73 U
0.76 U
100
105
X8593-ECD
00-407
1 5-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.36 J
0.89 U
0.42 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.42 J
0.23 J
0.52 U
0.65 U
0.73 U
0.76 U
92
99
X8564-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.38 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.25 J
0.23 J
0.52 U
0.65 U
0.73 U
0.76 U
100
106
X8565-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.30 J
0.89 U
0.51 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.18 J
0.19 J
0.52 U
0.65 U
0.73 U
0.76 U
88
94
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00407ECD
-------
flBaifeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01529OR1 CAD01534OR1 CAD01538OR1 CAD0153BOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8566-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.34 J
0.16 J
0.52 U
0.65 U
0.73 U
0.76 U
89
99
X8567-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.43 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.33 J
0.52 U
0.65 U
0.73 U
0.76 U
83
97
X8568-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.30 J
0.42 J
0.89 U
0.54 J
0.35 U
0.49 J
0.84 U
0.80 U
0.64 U
0.61 U
0.27 J
0.52 U
0.65 U
0.73 U
0.76 U
85
99
X8569-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.22 J
0.43 J
0.89 U
0.57 J
0.35 U
0.36 J
0.84 U
0.10 J
0.18 J
0.61 U
0.32 J
0.52 U
0.65 U
0.73 U
0.76 U
97
102
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00407ECD
-------
llBatteiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD0153EOR1
CAD01541OR1
CAD01544OR1
CAD01547OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8570-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.31 J
0.30 J
0.89 U
0.35 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.33 J
0.52 U
0.65 U
0.73 U
0.76 U
85
88
X8571-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.15 J
0.46 J
0.89 U
0.37 J
0.35 U
0.52 U
0.84 U
0.31 J
0.64 U
0.61 U
0.31 J
0.52 U
0.65 U
0.73 U
0.76 U
94
98
X8572-ECD
00-407
15-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 L)
0.21 J
0.43 J
0.89 U
0.56 J
0.35 U
0.16 J
0.84 U
0.80 U
0.64 U
0.61 U
0.23 J
0.52 U
0.65 U
0.73 U
0.76 U
90
96
X8573-ECD
00-407
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.48 J
1.78 U
0.22 J
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
0.56 J
1.04 U
1.30 U
1.46 U
1.52 U
81
83
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00407ECD
-------
Baneiie
. . . Putting Technology To Work
Project Name WA3-26 Boston Cap Project
Project Number G464426-EPA11DUXLAB
Client ID
CAD0154COR1
Field Sample Data
CAD0154FOR1 CAD0155EOR1
CAD01561OR1
CAD01564OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8574-ECD
00-408
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
0.40 J
0.79 J
0.32 J
0.56 J
0.70 U
0.36 J
0.23 J
0.59 J
1.28 U
0.43 J
0.53 J
0.23 J
0.25 J
0.22 J
0.17 J
100
96
X8575-ECD
00-408
15-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
0.18 J
0.56 J
1.78 U
0.40 J
0.70 U
0.19 J
1.68 U
1.60 U
1.28 U
1.22 U
0.24 J
1.04 U
1.30 U
1 .46 U
1.52 U
92
93
X8576-ECD
00-408
16-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.29 J
0.89 U
0.21 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
75
72
X8577-ECD
00-408
16-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.20 J
0.38 J
0.89 U
0.24 J
0.35 U
0.14 J
0.84 U
0.80 U
0.64 U
0.61 U
0.37 J
0.52 U
0.13 J
0.73 U
0.76 U
90
90
X8578-ECD
00-408
16-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.49 J
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
0.31 J
1.04 U
1.30 U
1.46 U
1.52 U
83
88
J - Analyte detected below the ssMDL.
U - Analyte not detected.
& - QC value outside the accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00408ECD
-------
OBaneae
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD015ABOR1 CAD015BOOR1 CAD015B3OR1 CAD015C2OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCS 187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8863-ECD
00-422
20-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1 .28 U
1.22 U
1.16 U
1.04 U
1.30U
1.46 U
1.52 U
85
90
X8864-ECD
00-422
20-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.62 J
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
0.34 J
1.04 U
1.30 U
1.46 U
1.52 U
90
95
X8865-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U -
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
143 &
66
X8866-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
2 &
4 &
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00422ECD
-------
llBatteiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD015C5OR1 CAD015CBOR1 CAD015CEOR1 CAD015D1OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8867-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.82 J
0.27 J
0.59 J
0.35 U
0.67
0.84 U
0.80 U
0.64 U
1.00
0.59
0.52 U
0.65 U
0.73 U
0.76 U
161 &
177 &
X8868-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.53 J
0.89 U
0.39 J
0.35 U
0.32 J
0.84 U
0.80 U
0.64 U
0.63
0.36 J
0.11 J
0.65 U
0.73 U
0.76 U
82
95
X8869-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.48 J
0.89 U
0.31 J
0.35 U
0.26 J
0.84 U
0.80 U
0.64 U
0.61 U
0.31 J
0.52 U
0.15 J
0.73 U
0.76 U
96
104
X8870-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.12 J
0.47 J
0.89 U
0.29 J
0.35 U
0.20 J
0.84 U
0.80 U
0.64 U
0.61 U
0.50 J
0.27 J
0.33 J
0.25 J
0.76 U
87
98
J - Analyte detected below the
ssMDL
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00422ECD
-------
llBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD015D4OR1 CAD015D7OR1 CAD015DCOR1 CAD015DFOR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8871-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.14 J
0.43 J
0.11 J
0.38 J
0.13 J
0.26 J
0.84 U
0.32 J
0.32 J
0.36 J
0.31 J
0.10 J
0.03 J
0.73 U
0.76 U
88
100
X8872-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.84
1.04 U
1.66
1.38
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.58 U
0.52 U
0.65 U
0.73 U
0.76 U
115
90
X8873-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.56 J
1.04 U
0.09 J
0.43 J
0.89 U
0.28 J
0.35 U
0.20 J
0.84 U
0.80 U
0.64 U
0.61 U
0.27 J
0.52 U
0.07 J
0.73 U
0.76 U
91
93
X8874-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.50 J
1.04 U
0.87 U
0.40 J
0.10 J
0.33 J
0.08 J
0.22 J
0.84 U
0.80 U
0.28 J
0.61 U
0.25 J
0.52 U
0.65 U
0.73 U
0.76 U
88
95
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00422ECD
-------
llBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Field Sample Data
Client ID
CAD015EFOR1
CAD015F2OR1
CAD015F5OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8875-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.35 J
0.12 J
0.11 J
0.32 J
0.07 J
0.28 J
0.35 U
0.17 J
0.84 U
0.80 U
0.64 U
0.61 U
0.27 J
0.52 U
0.06 J
0.73 U
0.76 U
83
96
X8876-ECD
00-422
20-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.21 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.52 J
0.52 U
0.65 U
0.73 U
0.76 U
83
93
X8877-ECD
00-422
20-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1 .68 U
1.60 U
1.28 U
1 .22 U
0.39 J
1.04 U
1.30 U
1.46 U
1.52 U
89
93
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00422ECD
-------
C-Baneiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD01610OR1 CAD01613OR1 CAD01616OR1
Field Sample Data
CAD01619OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8982-ECD
00-436
28-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.37 J
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1 .04 U
1.30 U
1.46 U
1.52 U
91
93
X8983-ECD
00-436
28-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74.U
1.72 U
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
89
97
X8984-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.10 J
0.29 J
0.89 U
0.25 J
0.35 U
0.52 U
0.84 U
0.19 J
0.64 U
0.61 U
0.34 J
0.52 U
0.65 U
0.73 U
0.76 U
90
96
X8985-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.33 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.36 J
0.52 U
0.65 U
0.73 U
0.76 U
100
102
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00436ECD
-------
llBaiteile
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
CAD0161COR1
CAD01620OR1
CAD01623OR1
CAD01626OR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8986-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.32 J
0.89 U
0.17 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.34 J
0.52 U
0.65 U
0.73 U
0.76 U
92
95
X8987-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.86 U
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.45 J
0.52 U
0.65 U
0.73 U
0.76 U
91
95
X8988-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.30 J
0.89 U
0.69 U
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.32 J
0.52 U
0.65 U
0.73 U
0.76 U
87
90
X8989-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.87 U
0.29 J
0.89 U
0.23 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.33 J
0.52 U
0.65 U
0.73 U
0.76 U
87
90
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00436ECD
-------
llBaffeiie
. . . Putting Technology To Work
Project Name: WA3-26 Boston
Cap Project
Project Number: G464426-
EPA11DUXLAB
Client ID
Field Sample Data
CAD01629OR1 CAD0162COR1
Sample ID
Batch ID
Collection Date
Dilution Factor
Sample Volume (L)
Units
PCB8
PCB18
PCB28
PCB44
PCB52
PCB66
PCB101
PCB105
PCB118
PCB128
PCB138
PCB153
PCB170
PCB180
PCB187
PCB195
PCB206
PCB209
Surrogate Recoveries:
PCB34
PCB112
X8990-ECD
00-436
28-Sep-OO
2.000
2.00
ng/L
9.60 U
0.83 U
1.04 U
0.12 J
0.45 J
0.89 U
0.35 J
0.35 U
0.52 U
0.84 U
0.80 U
0.64 U
0.61 U
0.57 J
0.52 U
0.65 U
0.73 U
0.76 U
97
99
X8991-ECD
00-436
28-Sep-OO
2.000
1.00
ng/L
19.20 U
1.66 U
2.08 U
1.74 U
0.44 J
1.78 U
1.38 U
0.70 U
1.04 U
1.68 U
1.60 U
1.28 U
1.22 U
1.16 U
1.04 U
1.30 U
1.46 U
1.52 U
88
92
J - Analyte detected below the
ssMDL.
U - Analyte not detected.
& - QC value outside the
accuracy or precision DQO.
Prepared by Desreuisseau 7/26/01
W00436ECD
-------
APPENDIX G
RCRA 8 METALS LABORATORY-REPORTED SAMPLE DATA
-------
-------
Laboratory Environmental
Analysis Report Monitoring, Inc.
v-: Alpha Analytical
255 Glendale Avenue Suite 21
;-: Sparks, NV 89431
u
-ample ID:
Customer Sample ED
' ^00009-1 161 BMI00092242-08 - CAD01390MMl-Total
Parameter
I otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
| admium - ICP-MS
* ihromium - ICP-MS
Silver - ICP-MS
pead -ICP-MS
: lercury - AA Cold Vapor
Selenium - ICP-MS
j ;-
] :imple ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
200009-1 162 BMI00092242-08 - CAD01390MMl-Dissolved
r
,y. Parameter
Sample Filtration
Tirsenic - ICP-MS
j jarium - ICP-MS
Dadmium - ICP-MS
rJhromium - ICP-MS
J Silver - ICP-MS
^ead - ICP-MS
vlercury - AA Cold Vapor
j ?elenium - ICP-MS
t ' "
Method Result
SEM - SOP Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Faulstich
Faulstich
Faulstich
Faulstich
Tretten
Faulstich
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Faulstich
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
9/29/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/4/2000
10/2/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/11/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
1 William F. Pillsbury
I President
Page 16 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-1 163 BMI00092242-09 - CAD01394MMl-Total
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-1 164 BMI00092242-09 - CAD01394MMl-Dissolved
Parameter
Sample Filtration
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
SEM - SOP
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
O.04
0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection '
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Faulstich
Faulstich
Faulstich
Faulstich
Tretten
Faulstich
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Faulstich
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
9/29/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/4/2000
10/2/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/11/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
William F. Pillsbury
President
Page 17 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report Monitoring, Inc.
t, .,- Alpha Analytical
,
25 5 Glendale Avenue Suite 21
v Sparks, NV 89431
Sample ID:
Customer Sample ID
200009-0892 BMI00092242-01 - CAD0133AMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
r Cadmium - ICP-MS
t j:hromium - ICP-MS
Silver - ICP-MS
f \ead - ICP-MS
vlercury - AA Cold Vapor
"Selenium - ICP-MS
( ;ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customs Sample ED
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0893 BMI00092242-02 - CAD013^8MM1
H
y Parameter
Total Recoverable Metals - Acid
Pl\rsenic - ICP-MS
| 3arium - ICP-MS
"Cadmium - ICP-MS
rChromium - ICP-MS
\ Silver - ICP-MS
MLead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8
-------
Laboratory |ESinn»nM
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0894 BMI00092242-03 - CAD0134BMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
O.5
O.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0895 BMI00092242-04 - CAD0134EMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver -ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten-
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000 -
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received :
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000 |
9/26/2000
9/26/2000
9/26/2000 r
9/26/2000
9/27/2000
9/26/2000 ,
William F. Pillsbury
President
Page 2 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
\
Laboratory
; Analysis Report
T-*. Alpha Analytical
:
;
255 Glendale Avenue Suite 21
' Sparks, NV 89431
.
Sample ID:
^ f
Customer Sample ID
200009-0896 BMI00092242-05 - CAD01371MM1
Parameter
:otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
~,ead- ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0897 BMI00092242-06 - CAD01376MM1
Parameter
Total Recoverable Metals - Acid
; \rsenic - ICP-MS
Barium - ICP-MS
"Cadmium - ICP-MS
^Chromium - ICP-MS
Silver - ICP-MS
'iead- ICP-MS
Mercury - AA Cold Vapor
' Helenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
^^^^
Sierra
Environmental
Monitoring, Inc.
Date: 10/16/2000
Client: ALP-855
Taken by:
Report:
PO#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
ft
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 3 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0898 BMI00092242-07 - CADO 1 37 AMM 1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium -ICP-MS
Silver - ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
O.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0899 BMI00092242-10 - CAD01398MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection ',.
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 4 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
^ Alpha Analytical
i
255 Glendale Avenue Suite 21
^- Sparks, NV 89431
h
Sample ID:
Customer Sample ID
1^00009-0900 BMI00092242-1 1 - CAD0139FMM1
I-
Parameter
| .'otal Recoverable Metals - Acid
S-Arsenic - ICP-MS
Barium - ICP-MS
padmium - ICP-MS
I Chromium - ICP-MS
Silver - ICP-MS
rT-,ead - ICP-MS
1 /lercury - AA Cold Vapor
"aelenium - ICP-MS
T''
j ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0901 BMI00092242-12 - CAD013A2MM1
t:?
! Parameter
Total Recoverable Metals - Acid
^Arsenic - ICP-MS
( Jarium - ICP-MS
^Cadmium - ICP-MS
Chromium - ICP-MS
1 Silver -ICP-MS
tiead - ICP-MS
Mercury - AA Cold Vapor
Tlelenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 O.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection '
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 5 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
3200009-0902 BMI00092242-13 - CAD013A6MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0903 BMI00092242-14 - CAD013AAMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
O.04
O.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection '
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 6 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
25 5 Glendale Avenue Suite 21
T- Sparks, NV 89431
f
Sample ID: Customer Sample ID
1 200009-0904 BMI00092242-15 - CAD013BOMM1
I;
Parameter
1 Total Recoverable Metals - Acid
'- Arsenic - ICP-MS
Barium - ICP-MS
] Cadmium - ICP-MS
"i Chromium - ICP-MS
Silver - ICP-MS
* r.ead - ICP-MS
! vlercury - AA Cold Vapor
1 Selenium - ICP-MS
T ^
1 ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0905 BMI00092242-16 - CAD013B4MM1
r
i
1 Parameter
Total Recoverable Metals - Acid
|: Arsenic - ICP-MS
| 3arium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
! Silver - ICP-MS
KCead - ICP-MS
Mercury - AA Cold Vapor
| 'Selenium -ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 7 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-0906 BMI00092242-17 - CAD013C9MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0907 BMI00092242- 1 8 - CADO 1 5ABMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/11/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000 ,
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000 ;
9/26/2000
9/26/2000
9/26/2000 r
9/26/2000 '
9/27/2000
9/26/2000 ,
William F. Pillsbury
President
Page 8 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
^00009-0908 BMI00092242-19-CAD015BOMM1
Parameter
"\rtal Recoverable Metals - Acid
4 Arsenic - ICP-MS
Barium - ICP-MS
f Cadmium - ICP-MS
Chromium -ICP-MS
Silver - ICP-MS
| lead -ICP-MS
[ Mercury - AA Cold Vapor
Selenium - ICP-MS
tiample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
O.02
0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0909 BMI00092242-20 - CAD015B3MM1
T"?
K. Parameter
Total Recoverable Metals - Acid
T^rsenic - ICP-MS
yaarium - ICP-MS
Cadmium - ICP-MS
j Chromium - ICP-MS
| Silver - ICP-MS
H,ead- ICP-MS
Mercury - AA Cold Vapor
f Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 9 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0910 BMI00092242-21 - CAD015C2MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-091 1 BMI00092242-22 - CAD015C5MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium -ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
<0.02
O.04
O.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000 r
9/26/2000
9/26/2000 r
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000 ;
9/26/2000 ;
9/26/2000
9/26/2000 '
9/26/2000 :
9/27/2000
9/26/2000 -,
William F. Pillsbury
President
Page 10 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem © sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory l|Xnmentai
Analysis Report Monitoring, Inc.
Alpha Analytical
f;
255 Glendale Avenue Suite 21
T< Sparks, NV 89431
r :
U
Sample ID: Customer Sample ID
1100009-0912 BMI00092242-23 - CAD015CBMM1
I. ,:
Parameter
j otal Recoverable Metals - Acid
Ursenic - ICP-MS
Barium - ICP-MS
T Cadmium - ICP-MS
| Jiromium - ICP-MS
Silver - ICP-MS
|T ead - ICP-MS
1 lercury - AA Cold Vapor
Velenium - ICP-MS
1 mple ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
O.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0913 BMI00092242-24 - CAD015CEMM1
P
1^ Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
f iarium - ICP-MS
Cadmium - ICP-MS
Dhromium - ICP-MS
fjlver- ICP-MS
Mead -ICP-MS
vlercury - AA Cold Vapor
f lelenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
O.04
O.02
<0.02
0.0013
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection '-
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 11 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem © sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-09 14 BMI00092242-25 - CADO 1 5D 1MM 1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0915 BMI00092242-26 - CAD015D4MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver -ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection '..
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 12 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
r
Alpha Analytical
| ,
1 ' 255 Glendale Avenue Suite 21
^ Sparks, NV 89431
Sample ID: Customer Sample ID
f -'00009-0916 BMI00092242-27 - CAD015D7MM1
| .;
Parameter Method Result
j :'otai Recoverable Metals - Acid EPA 200.2 Completed
i . Arsenic - ICP-MS EPA 200.8 <0.02
Barium - ICP-MS EPA 200.8 <0.5
7 "admium - ICP-MS EPA 200.8 <0.02
I :hromium- ICP-MS EPA 200.8 <0.04
Silver -ICP-MS EPA 200.8 <0.02
t Lead - ICP-MS EPA 200.8 <0.02
j v!ercury-AA Cold Vapor EPA 245.1 < 0.0005
Selenium -ICP-MS EPA 200.8 <0.2
I ample ID- Customer Sample ID
fcS200009-0917 BMI00092242-28 - CAD015DCMM1
! Parameter Method Result
f Total Recoverable Metals - Acid EPA 200.2 Completed
r Arsenic -ICP-MS EPA 200.8 <0.02
I Barium - ICP-MS EPA 200.8 <0.5
^Cadmium -ICP-MS EPA 200.8 <0.02
Chromium -ICP-MS EPA 200.8 0.041
f 'Silver -ICP-MS EPA 200.8 <0.02
I .Lead -ICP-MS EPA 200.8 <0.02
Mercury - AA Cold Vapor EPA 245.1 < 0.0005
1" Selenium - ICP-MS EPA 200.8 O.2
[-.-_ . __- --.-- - -
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection*
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/25/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Page 13 of 18
I William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
3200009-09 1 8 BMI00092242-29 - CAD01 5DFMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.054
EPA 200.8 < 0.02
EPA 200. 8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0919 BMI00092242-30 - CAD015EFMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 0.03
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.056
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 14 of 18
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
'00009-0920 BMI00092242-3 1 - CAD015F2MM1
Parameter Method Result
"otal Recoverable Metals - Acid EPA 200.2 Completed
Arsenic -ICP-MS EPA 200.8 <0.02
Barium - ICP-MS EPA 200.8 <0.5
Cadmium - ICP-MS EPA 200.8 < 0.02
Chromium -ICP-MS EPA 200.8 0.057
Silver -ICP-MS EPA 200.8 <0.02
Lead - ICP-MS EPA 200.8 < 0.02
ivlercury - AA Cold Vapor EPA 245.1 < 0.0005
Selenium - ICP-MS EPA 200.8 <0.2
Cample ID: Customer Sample ID
S200009-0921 BMI00092242-32 - CAD015F5MM1
Parameter Method Result
~ Total Recoverable Metals - Acid EPA 200.2 Completed
.Arsenic -ICP-MS EPA 200.8 0.027
Barium- ICP-MS EPA 200.8 <0.5
"Cadmium -ICP-MS EPA 200.8 <0.02
Chromium - ICP-MS EPA 200.8 0.057
""Silver - ICP-MS EPA 200.8 < 0.02
u^Lead- ICP-MS EPA 200.8 <0.02
Mercury - AA Cold Vapor EPA 245. 1 < 0.0005
T Selenium -ICP-MS EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/20/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/20/2000
Detection*
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36912
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Page 15 of 18
^William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical .com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0922 BMI00092241-01 - CAD01021MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
0.056
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0923 BMI00092241-02 - CAD01024MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.024
<0.5
<0.02
0.06
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/6/2000
Detection ' .
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000 ,
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/27/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000 '
9/26/2000
9/26/2000 '
9/26/2000
9/26/2000
9/26/2000 ,
9/26/2000 ,
9/27/2000
9/26/2000
William F. Pillsbury
President
Page 1 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
r,. Alpha Analytical
255 Glendale Avenue Suite 21
p Sparks, NV 89431
f-;
Sample ID:
Customer Sample ID
I ^00009-0924 BMI00092241-03-CAD01027MM1
I.;
~ Parameter
| 'otal Recoverable Metals - Acid
1 Arsenic - ICP-MS
Barium - ICP-MS
1 iadmium - ICP-MS
I Chromium - ICP-MS
Silver - ICP-MS
}"' 'lead -ICP-MS
j Mercury - AA Cold Vapor
Selenium - ICP-MS
j[ ;ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.061
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0925 BMI00092241-04 - CAD0102AMM1
f '
K. Parameter
Total Recoverable Metals - Acid
t\rsenic - ICP-MS
[ Barium -ICP-MS
Cadmium - ICP-MS
« Chromium - ICP-MS
I Silver - ICP-MS
* Lead -ICP-MS
Mercury - AA Cold Vapor
| Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.059
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
I!
William F. Pillsbury
President
Page 2 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0926 BMI00092241-05 - CAD0102DMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
0.031
<0.5
<0.02
0.06
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0927 BMI00092241-06- CAD0104AMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.064
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/6/2000
Detection '
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
William F. Pillsbury
President
Page 3 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
i
255 Glendale Avenue Suite 21
Sparks, NV 89431
i -
Sample ID:
Customer Sample ID
1 >00009-0928 BMI00092241-07 - CAD0104DMM1
i.
Parameter
' 'otal Recoverable Metals - Acid
1 Arsenic - ICP-MS
Barium - ICP-MS
"admium - ICP-MS
I Chromium - ICP-MS
Silver - ICP-MS
',ead - ICP-MS
; ,/tercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.059
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0929 BMI00092241-08 - CAD01050MM1
T
i -
i Parameter
Total Recoverable Metals - Acid
T Arsenic - ICP-MS
I iJarium - ICP-MS
Cadmium - ICP-MS
v Chromium - ICP-MS
i Silver - ICP-MS
MLead - ICP-MS
Mercury - AA Cold Vapor
1 Selenium -ICP-MS
1 :
Method Result
EPA 200.2 Completed
EPA 200.8 0.035
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.059
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/6/2000
ft
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
T-";William F. Pillsbury
President
Page 4 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory Sierra
. , . T, , Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-0930 BMI00092241-09 - CAD01053MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.061
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0931 BMI00092241-10 - CAD01056MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 0.027
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.059
EPA 200.8 < 0.02
EPA 200.8 < 0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/6/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/6/2000
Detection «.'
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
. Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Page 5 of 52
William F. Pillsbury
President
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i_ A Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
200009-0992 BMI00092241-71 - CAD012ACMM1
..:
Parameter
"otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
"Cadmium -ICP-MS
£hromium - ICP-MS
Silver - ICP-MS
f-.,ead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
jample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0993 BMI00092241-72 - CAD012AFMM1
"
ii Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
, Barium - ICP-MS
Cadmium - ICP-MS
, Chromium - ICP-MS
1 Silver - ICP-MS
lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 36 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i_ , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample BO
S200009-0994 BMI00092241-73 - CAD012B2MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
<0.02
O.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0995 BMI00092241-76 - CAD012C6MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.047
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 37 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D:
John C. Seher
Managers
-------
T Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
t-i Alpha Analytical
\.-i
255 Glendale Avenue Suite 21
p Sparks, NV 89431
i -
h
jSample ID: Customer Sample ID
) ;200009-0996 BMI00092241 -77 - CAD012CCMM1
V-'-
y Parameter
j "otal Recoverable Metals - Acid
Arsenic - ICP-MS
,3arium - ICP-MS
1 Zadmium - ICP-MS
t Chromium - ICP-MS
Silver - ICP-MS
V*.,ead - ICP-MS
ylercury - AA Cold Vapor
Selenium - ICP-MS
I ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
3200009-0997 BMI00092241-78 - CAD012CFMM1
n
I- > Parameter
Total Recoverable Metals - Acid
-TXrsenic - ICP-MS
LjSarium - ICP-MS
Cadmium - ICP-MS
f Chromium - ICP-MS
[ Silver - ICP-MS
'"lead - ICP-MS
JMercury - AA Cold Vapor
! Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000 ,
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Piilsbury
President
Page 38 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory iSSronmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-0998 BMI00092241-79 - CAD012D2MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 O.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0999 BMI00092241-80 - CAD012D6MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium -ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.041
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 39 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T u A Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
PS Alpha Analytical
255 Glendale Avenue Suite 21
- Sparks, NV 89431
Sample ID:
Customer Sample ID
200009-1000 BMI00092241-81 - CAD012DCMM1
Parameter
"otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
- Chromium - ICP-MS
Silver - ICP-MS
lead -ICP-MS
/lercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-1001 BMI00092241-82 - CAD012EOMM1
:
;> Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
jjlarium - ICP-MS
Cadmium - ICP-MS
^Chromium - ICP-MS
Silver - ICP-MS
4,ead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
t ; :
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000 t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
'William F. Pillsbuiy
President
Page 40 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory Invironmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-1002 BMI00092241-83 - CAD012ECMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
S200009-1003 BMI00092241-84 - CAD012FOMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
O.02
O.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 41 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T u A Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
-p. Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
200009-1004 BMI00092241-85 - CAD012F4MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
' Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
.ead- ICP-MS
vlercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
S200009-1005 BMI00092241-86 - CAD013
a Parameter
Total Recoverable Metals - Acid
-\rsenic - ICP-MS
. Barium - ICP-MS
v_,-,v
Cadmium - ICP-MS
'. Chromium - ICP-MS
Silver - ICP-MS
HLead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
OMM1
Result
Completed
<0.02
0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000 t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 42 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-1006 BMI00092241-87 - CAD0130FMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009- 1 007 BMI0009224 1 -88 - CADO 1 3 1 2MM 1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000 ,
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 43 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i_ A. Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
r T Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
200009-1008 BMI00092241-89-CAD0131FMM1
Parameter
^otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
T"
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
" >ad - ICP-MS
/lercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200,8
Customer
Result
Completed
<0.02
<0.5
O.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-1009 BMI00092241-90 - CAD01322MM1
if- -.
;.-. Parameter
Total Recoverable Metals - Acid
T Arsenic - ICP-MS
jtarium - ICP-MS
Cadmium - ICP-MS
f Chromium - ICP-MS
- >ilver - ICP-MS
LLead - ICP-MS
__ Mercury - AA Cold Vapor
] Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 44 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-1010 BMI00092241-91 - CAD01325MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
0.5
O.02
<0.04
<0.02
O.02
< 0.0005
O.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-101 1 BMI00092241-92 - CAD0132BMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
0.02
O.04
O.02
O.02
< 0.0005
O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 45 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i_ A. Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
\
Sample ID:
T- %
Customer Sample ID
200009-1012 BMI00092241-93-CAD0132EMM1
-'- -
r Parameter
i notal Recoverable Metals - Acid
fc Arsenic - ICP-MS
Barium - ICP-MS
f ;admium - ICP-MS
£j;hromium - ICP-MS
Silver - ICP-MS
f "lead - ICP-MS
| lercury - AA Cold Vapor
Selenium - ICP-MS
{"; ,
\ ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-1013 BMI00092241-94 - CAD01331MM1
| -;
(b, Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
1 Barium - ICP-MS
Cadmium - ICP-MS
f Chromium -ICP-MS
reiver - ICP-MS
>tead - ICP-MS
Mercury - AA Cold Vapor
I "Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 0.5
EPA 200.8 O.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
^
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
| William F. Pillsbury
I President
Page 46 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ED: Customer Sample ID
S200009-1014 BMI00092241-95 - CAD01334MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
<0.04
O.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
S200009-1015 BMI00092241-96 - CAD01337MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.02
<0.5
O.02
O.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/10/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Kleinworth
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/27/2000
William F. Pillsbury
President
Page 47 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
. Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
200009-1153 BMI00092241-74-CAD012BFMMl-Total
Parameter
"otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
~.ead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
ample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-1154 BMI00092241-74-CAD012BFMMl-Dissolved
.'
Parameter
Sample Filtration
:\rsenic - ICP-MS
Jarium - ICP-MS
Cadmium - ICP-MS
r- Chromium - ICP-MS
silver - ICP-MS
^ Lead -ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
SEM - SOP Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 O.04
EPA 200.8 0.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Faulstich
Faulstich
Faulstich
Faulstich
Tretten
Faulstich
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
9/29/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/4/2000
10/2/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/2/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
T "
["William F. Pillsbury
President
Page 48 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T u * Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009- 1155 BMI0009224 1 -75 - CADO 12C3MM1 -Total
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-1 156 BMI00092241-75 - CAD012C3MMl-Dissolved
Parameter
Sample Filtration
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
SEM - SOP Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 O.04
EPA 200.8 <0.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/9/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Faulstich
Faulstich
Faulstich
Faulstich
Tretten
Faulstich
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
9/29/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/2/2000
10/4/2000
10/2/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/2/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
William F. Pillsbury
President
Page 49 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
r* Alpha Analytical
i
255 Glendale Avenue Suite 21
I -': Sparks, NV 89431
^Sample ID: Customer Sample ID
' "200009-1 157 BMI00092241-29 - CAD0147DMM1 -Dissolved
Parameter
Sample Filtration
-Arsenic -ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
sample ID:
Method
SEM - SOP
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.02
O.5
<0.02
O.04
O.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
S200009-1 158 BMI00092241-44 - CAD014D4MM1 -Dissolved
Parameter
Sample Filtration
t -Arsenic - ICP-MS
, :Barium - ICP-MS
Cadmium - ICP-MS
r .Chromium - ICP-MS
Silver - ICP-MS
"-Lead - ICP-MS
Mercury - AA Cold Vapor
:- Selenium - ICP-MS
Method
SEM - SOP
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
i* f
9?//2QQO
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date. Sampled
9/02000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/2/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/2/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
]. William R Pillsbury
i President
Page 50 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analyticat.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-1 159 BMI00092241-45 - CAD014DBMMl-Dissolved
Parameter
Sample Filtration
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
SEM - SOP
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
O.02
<0.04
O.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-1 160 BMI00092241-59 - CAD01534MMl-Dissolved
Parameter
Sample Filtration
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
SEM - SOP
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.05
<0.5
O.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/^2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9J972000
Detection
Limit
0.05
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Time Sampled
Analyst
Tretten
Tretten
Faulstich
Tretten
Faulstich
Tretten
Tretten
Kobza
Faulstich
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/2/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000
Date Received
9/22/2000
Date
Analyzed
10/2/2000
10/5/2000
10/11/2000
10/2/2000
10/11/2000
10/2/2000
10/2/2000
10/4/2000
10/11/2000,
William F. Pillsbury
President
Page 51 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory InlTronmental
Analysis Report Monitoring, Inc.
^ Alpha Analytical
-
255 Glendale Avenue Suite 21
*?; Sparks, NV 89431
i ;
Sample ID:
Customer Sample ID
:!00009-0932 BMI00092241-1 1 - CAD01405MM1
Parameter
1 'otal Recoverable Metals -
'Arsenic - ICP-MS
Barium - ICP-MS
'"] Cadmium - ICP-MS
1 Chromium- ICP-MS
Silver - ICP-MS
r;,ead- ICP-MS
i Mercury - AA Cold Vapor
Selenium - ICP-MS
r -
.' ample ID:
Method Result
Acid EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.06
EPA 200.8 < 0.02
EPA 200.8 0.025
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0933 BMI00092241-12 - CAD01408MM1
T:
! Parameter
Total Recoverable Metals -
*"\rsenic - ICP-MS
i' Barium - ICP-MS
'Cadmium - ICP-MS
f ^Chromium - ICP-MS
5 Silver - ICP-MS
}iead - ICP-MS
Mercury - AA Cold Vapor
Tf elenium - ICP-MS
Method Result
Acid EPA 200.2 Completed
EPA 200.8 < 0.02
EPA 200.8 <0.5
EPA 200.8 < 0.02
EPA 200.8 0.058
EPA 200.8 < 0.02
EPA 200.8 0.024
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
L
William F. Pillsbury
President
Page 6 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0934 BMI00092241-13 - CAD0140BMM1
Parameter Method Result
Total Recoverable Metals - Acid EPA 200.2 Completed
Arsenic - ICP-MS EPA 200.8 0.027
Barium - ICP-MS EPA 200.8 <0.5
Cadmium -ICP-MS EPA 200.8 <0.02
Chromium - ICP-MS EPA 200.8 0.057
Silver - ICP-MS EPA 200.8 < 0.02
Lead - ICP-MS EPA 200.8 0.024
Mercury - AA Cold Vapor EPA 245. 1 < 0.0005
Selenium - ICP-MS EPA 200.8 <0.2
Sample ID: Customer Sample ID
3200009-0935 BMI00092241-14 - CAD01416MM1
Parameter Method Result
Total Recoverable Metals - Acid EPA 200.2 Completed
Arsenic - ICP-MS EPA 200.8 0.024
Barium -ICP-MS EPA 200.8 <0.5
Cadmium - ICP-MS EPA 200.8 < 0.02
Chromium -ICP-MS EPA 200.8 0.058
Silver - ICP-MS EPA 200.8 < 0.02
Lead - ICP-MS EPA 200.8 0.024
Mercury - AA Cold Vapor EPA 245 . 1 < 0.0005
Selenium - ICP-MS EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/12/2000
t-
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
William F. Pillsbury
President
Page 7 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory Environmental
Analysis Report Monitoring, Inc.
,, Alpha Analytical
| '.
255 Glendale Avenue Suite 21
T; Sparks, NV 89431
i ;
Sample ID: Customer Sample ID
f ^00009-0936 BMI00092241-15 - CAD01419MM1
L- :
T , Parameter
1 "otal Recoverable Metals - Acid
1 Arsenic - ICP-MS
Barium - ICP-MS
| badmium - ICP-MS
i Chromium - ICP-MS
Silver - ICP-MS
pead - ICP-MS
j Mercury - AA Cold Vapor
"Selenium - ICP-MS
t ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
0.061
<0.02
0.024
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0937 BMI00092241-16- CAD0141CMM1
T-
U Parameter
Total Recoverable Metals - Acid
T \rsenic - ICP-MS
i Jarium- ICP-MS
Cadmium - ICP-MS
TChromium - ICP-MS
,' Silver - ICP-MS
>iead - ICP-MS
Mercury - AA Cold Vapor
T Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.059
<0.02
0.024
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
'-- William F. Pillsbury
t President
Page 8 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory IJfvTronmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
3200009-0942 BMI00092241-21 - CAD0142BMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.056
EPA 200.8 O.02
EPA 200.8 0.024
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0943 BMI00092241-22 - CAD0142EMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.057
EPA 200.8 O.02
EPA 200.8 0.024
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/28/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 11 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ semranalytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
,f,. Alpha Analytical
V "
255 Glendale Avenue Suite 21
P Sparks, NV 89431
1;
sample ID: Customer Sample ID
( '.00009-0944 BMI00092241-23 - CAD01436MM1
-fox
,, , Parameter Method Result
| 'otal Recoverable Metals - Acid EPA 200.2 Completed
^Arsenic - ICP-MS EPA 200.8 0.028
Barium - ICP-MS EPA 200.8 <0.5
I :admium - ICP-MS EPA 200.8 O.02
\ :hromium - ICP-MS . EPA 200.8 0.058
Silver - ICP-MS EPA 200.8 <0.02
r,ead - ICP-MS EPA 200.8 0.024
I lercury - AA Cold Vapor EPA 245.1 < 0.0005
1 Selenium - ICP-MS EPA 200.8 <0.2
| imple ID: Customer Sample ID
5200009-0945 BMI00092241-24 - CAD01439MM1
T'
li Parameter Method Result
Total Recoverable Metals - Acid EPA 200.2 Completed
F arsenic - ICP-MS EPA 200.8 0.026
f ;!arium - ICP-MS EPA 200.8 <0.5
Cadmium - ICP-MS EPA 200.8 <0.02
« Chromium -ICP-MS EPA 200.8 0.056
| lilver - ICP-MS EPA 200.8 <0.02
»iead - ICP-MS EPA 200.8 0.024
Mercury - AA Cold Vapor EPA 245. 1 < 0.0005
f Selenium - ICP-MS EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 12 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory ||fvrSnmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0946 BMI00092241-25 - CAD0143CMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.047
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
S200009-0947 BMI00092241-26 - CAD01469MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
0.048
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/12/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
*
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 13 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ setn-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
T-I Alpha Analytical
255 Glendale Avenue Suite 21
:" Sparks, NV 89431
:
Sample ID:
Customer Sample ID
200009-0948 BMI0009224 1 -27 - CADO 146CMM 1
Parameter
?otal Recoverable Metals - Acid
Arsenic - ICP-MS
r Barium - ICP-MS
Oadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
lead - ICP-MS
ylercury - AA Cold Vapor
Selenium - ICP-MS
, Cample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.047
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0949 BMI00092241-28 - CAD0146FMM1
'- Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
^Barium - ICP-MS
Cadmium - ICP-MS
v Chromium - ICP-MS
[Silver -ICP-MS
Lead - ICP-MS
, .Mercury - AA Cold Vapor
1 (Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 0.048
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 14 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory iKRmmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0950 BMI00092241-29 - CAD0147DMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
0.055
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0951 BMI00092241-30 - CAD01480MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
<0.02
0.057
0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
' 0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 15 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory Environmental
Analysis Report Monitoring, Inc.
r- Alpha Analytical
255 Glendale Avenue Suite 21
- Sparks, NV 89431
Sample ID: Customer Sample ID
100009-0952 BMI00092241-31 - CAD01483MM1
Parameter
'otal Recoverable Metals - Acid
Arsenic - ICP-MS
f JBarium - ICP-MS
>admium - ICP-MS
Jhromium - ICP-MS
Silver - ICP-MS
,ead- ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
implelD:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
0.5
O.02
0.057
O.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0953 BMI00092241-32 -CAD01486MM1
r <
Parameter
Total Recoverable Metals - Acid
f \rsenic - ICP-MS
t Jarium - ICP-MS
Cadmium - ICP-MS
v 'Chromium - ICP-MS
1 Silver - ICP-MS
'"'Lead -ICP-MS
Mercury - AA Cold Vapor
; Selenium - ICP-MS
Method
EPA 200.2
EPA 200. 8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.026
<0.5
O.02
0.056
O.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
^
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
; President
Page 16 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory llfvironmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Date:
Client:
Taken by:
Report:
PO#:
10/16/2000
ALP-855
Client
36913
Sample ID: Customer Sample ID
3200009-0954 BMI00092241-33 - CAD01489MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
0.02
<0.5
<0.02
0.056
O.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0955 BMI00092241-34 - CAD0148CMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.036
<0.5
O.02
0.052
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
*
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000 f
William F. Pillsbury
President
Page 17 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analvtical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
; Alpha Analytical
i
255 Glendale Avenue Suite 21
Sparks, NV 89431
Cample ID: Customer Sample ID
200009-0956 BMI00092241-35 - CAD0148FMM1
Parameter
'otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
f :admium - ICP-MS
* chromium - ICP-MS
Silver - ICP-MS
f lead -ICP-MS
| alercury - AA Cold Vapor
Selenium - ICP-MS
I
temple ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
<0.02
0.049
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0957 BMI00092241-36 - CAD01492MM1
f '
%*< Parameter
Total Recoverable Metals - Acid
f \rsenic - ICP-MS
iLSarium - ICP-MS
Cadmium - ICP-MS
f'hromium - ICP-MS
f Silver - ICP-MS
HLead - ICP-MS
rMercury . AA Cold Vapor
|: ^elenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.056
0.02
O.02
< 0.0005
O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
|. William F. Pillsbury
President
Page 18 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i- A. Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
3200009-0958 BMI00092241-37 - CAD01495MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.053
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0959 BMI00092241-38 - CAD0149DMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver -ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 0.022
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.052
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000 ,
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 19 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
f T Alpha Analytical
!
255 Glendale Avenue Suite 21
p Sparks, NV 89431
I i:
Sample ID: Customer Sample ID
f ;'00009-0960 BMI00092241-39 - CAD014AOMM1
T Parameter
| otal Recoverable Metals - Acid
Xrsenic - ICP-MS
TBarium - ICP-MS
I admium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
T "ead - ICP-MS
! lercury - AA Cold Vapor
Selenium - ICP-MS
L ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
0.052
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0961 BMI00092241-40 - CAD014A3MM1
t «
:
l> Parameter
Total Recoverable Metals - Acid
Hrsenic - ICP-MS
Uarium - ICP-MS
Cadmium - ICP-MS
TTftromium - ICP-MS
f Silver - ICP-MS
^Lead - ICP-MS
Mercury - AA Cold Vapor
T Selenium - ICP-MS
H
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
O.02
0.049
O.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/14/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
- - -
j William F. Pillsbury
I President
Page 20 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0962 BMI00092241-41 - CAD014BFMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
0.029
<0.5
O.02
0.051
O.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0963 BMI00092241-42 - CAD014C2MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
0.052
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000 ,
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000 ,'
Date
Analyzed
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/26/2000
9/29/2000
9/26/2000
Date Received;
9/22/2000
Date
Analyzed
9/26/2000
9/26/2000 ;
9/26/2000 ,
9/26/2000
9/26/2000
9/26/2000 '
9/26/2000
9/29/2000
9/26/2000
William F. Pillsbury
President
Page 21 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
|-t Alpha Analytical
255 Glendale Avenue Suite 21
f Sparks, NV 89431
I.
Cample ID:
Customer Sample ID
I :00009-0964 BMI00092241-43 - CAD014C5MM1
I;
r Parameter
otal Recoverable Metals - Acid
Arsenic - ICP-MS
.Barium - ICP-MS
! ladmium - ICP-MS
Jhromium - ICP-MS
Silver - ICP-MS
ead- ICP-MS
lercury - AA Cold Vapor
Selenium - ICP-MS
imple ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 0.056
EPA 200.8 O.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 O.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0965 BMI00092241-44-CAD014D4MM1
f
» Parameter
Total Recoverable Metals - Acid
f Arsenic - ICP-MS
Lilarium - ICP-MS
Cadmium - ICP-MS
f Chromium - ICP-MS
hilver - ICP-MS
- Lead - ICP-MS
Mercury - AA Cold Vapor
f Helenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 O.5
EPA 200.8 O.02
EPA 200.8 0.063
EPA 200.8 O.02
EPA 200.8 O.02
EPA 245.1 < 0.0005
EPA 200.8 O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
William F. Pillsbury
President
Page 22 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Sicrrs
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0966 BMI0009224 1 -45 - CADO 14DBMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
<0.02
0.056
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0967 BMI00092241-46 - CAD014DEMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000 t.
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Kleinworth
Lambert
Lambert
Lambert
Lambert
Lambert
Lambert
Kobza
Lambert
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000 ;
9/27/2000 ,
9/27/2000
9/27/2000
9/27/2000 '.
9/27/2000
9/29/2000
9/27/2000 '
William F. Pillsbury
President
Page 23 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
200009-0968 BMI00092241-47 - CAD014E4MM1
Parameter
^otal Recoverable Metals -
' Arsenic - ICP-MS
, Barium - ICP-MS
:admium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
' ,ead- ICP-MS
, -/lercury - AA Cold Vapor
Selenium - ICP-MS
yample ID:
Method Result
Acid EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0969 BMI00092241-48 - CAD014E7MM1
n
.:
8 Parameter
Total Recoverable Metals -
Fkrsenic - ICP-MS
iJJarium - ICP-MS
Cadmium - ICP-MS
pChromium - ICP-MS
silver - ICP-MS
4,ead - ICP-MS
...Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
Acid EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 0.044
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
L
William F. Pillsbury
President
Page 24 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
3200009-0970 BMI00092241-49 - CAD014EAMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0971 BMI00092241-50 - CAD014EDMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
William F. Pillsbury
President
Page 25 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
r-> Alpha Analytical
255 Glendale Avenue Suite 21
'" Sparks, NV 89431
. ^
»g,mple ID:
Customer Sample ID
;00009-0972 BMI00092241-51 - CAD014F3MM1
Parameter
otal Recoverable Metals - Acid
Arsenic - ICP-MS
Blarium - ICP-MS
admium - ICP-MS
Jhromium - ICP-MS
Silver - ICP-MS
3ad - ICP-MS
lercury - AA Cold Vapor
Selenium - ICP-MS
mple ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
5200009-0973 BMI00092241-52 - CAD014F6MM1
--- Parameter
Total Recoverable Metals - Acid
:.rsenic - ICP-MS
^arium - ICP-MS
Cadmium - ICP-MS
t Chromium - ICP-MS
iilver - ICP-MS
Lead - ICP-MS
fMercury - AA Cold Vapor
'elenium - ICP-MS
*i - - - -
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/27/2000
; William F. Pillsbury
i President
Page 26 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem ©sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0974 BMI00092241-53 - CAD0151 1MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
<0.02
<0.04
O.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0975 BMI00092241-54 - CAD01514MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000 '
William F. Pillsbury
President
Page 27 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
TV. + Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
r-3 Alpha Analytical
,.i
255 Glendale Avenue Suite 21
"t Sparks, NV 89431
Sample ID: Customer Sample ID
;»00009-0976 BMI00092241-55 - CAD0151AMM1
Parameter
:'otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
.Cadmium - ICP-MS
Chromium - ICP-MS
Silver -ICP-MS
,ead- ICP-MS
lercury - AA Cold Vapor
Selenium - ICP-MS
.ample D):
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
O.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0977 BMI00092241-56 - CAD01523MM1
Parameter
Total Recoverable Metals - Acid
\rsenic - ICP-MS
Sarium - ICP-MS
Cadmium - ICP-MS
'Chromium - ICP-MS
silver - ICP-MS
'Lead - ICP-MS
^Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
0.02
< 0.0005
0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000 t
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
William F. Pillsbury
, President
Page 28 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T i, 4. Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
Customer Sample ID
S200009-0978 BMI00092241-57 - CAD01526MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method Result
EPA 200.2 Completed
EPA 200.8 <0.02
EPA 200.8 <0.5
EPA 200.8 <0.02
EPA 200.8 <0.04
EPA 200.8 O.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Customer Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0979 BMI00092241-58 - CAD01529MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method Result
EPA 200.2 Completed
EPA 200.8 O.02
EPA 200.8 <0.5
EPA 200.8 O.02
EPA 200.8 O.04
EPA 200.8 <0.02
EPA 200.8 <0.02
EPA 245.1 < 0.0005
EPA 200.8 <0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000 ,
9/27/2000
9/27/2000
9/27/2000
9/27/2000 '
9/27/2000 !
9/29/2000
9/29/2000 :
William F. Pillsbury
President
Page 29 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
j-.t Alpha Analytical
255 Glendale Avenue Suite 21
^ Sparks, NV 89431
Sample ID: Customer Sample ID
200009-0980 BMI00092241-59 - CAD01534MM1
I;
Parameter
Total Recoverable Metals - Acid
'Arsenic - ICP-MS
Barium - ICP-MS
Jadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
,ead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
.ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
O.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0981 BMI00092241-60 - CAD01538MM1
I Parameter
Total Recoverable Metals - Acid
V:\rsenic - ICP-MS
k Barium - ICP-MS
Cadmium - ICP-MS
^Chromium - ICP-MS
( -Silver - ICP-MS
H,ead - ICP-MS
Mercury - AA Cold Vapor
Selenium -ICP-MS
f >
rs
y
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
<0.5
<0.02
<0.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
William F. Pillsbury
President
Page 30 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0982 BMI00092241-61 - CAD0153BMM/1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
<0.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0983 BMI00092241-62 - CAD0153EMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000 :
9/27/2000
9/27/2000
9/27/2000
9/29/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000 ,
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000 ,
William F. Pillsbury
President
Page 31 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
r , Alpha Analytical
i;
255 Glendale Avenue Suite 21
| Sparks, NV 89431
Cample ID: Customer Sample ID
'00009-0984 BMI00092241-63-CAD01541MM1
Parameter
'otal Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
r ---
;admium - ICP-MS
i Chromium - ICP-MS
Silver - ICP-MS
Head- ICP-MS
, lercury - AA Cold Vapor
Selenium - ICP-MS
[Ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0985 BMI00092241-64 - CAD01544MM1
t-> Parameter
Total Recoverable Metals - Acid
: \rsenic - ICP-MS
; Barium - ICP-MS
Cadmium - ICP-MS
r; Chromium - ICP-MS
| Silver - ICP-MS
KLead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
O.02
O.04
<0.02
<0.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 32 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T , Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0986 BMI00092241-65 - CAD01547MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
<0.02
0.5
0.02
O.04
O.02
O.02
< 0.0005
O.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
3200009-0987 BMI00092241-66 - CAD0154CMM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
0.04
O.5
O.02
O.04
0.02
0.02
< 0.0005
O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/15/2000 ,.
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000 :
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000 '
William F. Pillsbury
President
Page 33 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
T u ^ Sierra
Laboratory Environmental
Analysis Report Monitoring, Inc.
r ,- Alpha Analytical
j.
255 Glendale Avenue Suite 21
T? Sparks, NV 89431
Sample ID: Customer Sample ID
I ?200009-0988 BMI00092241-67 - CAD0154FMM1
,- Parameter
f Total Recoverable Metals - Acid
1 Arsenic - ICP-MS
Barium - ICP-MS
j :admium - ICP-MS
L Jhromium - ICP-MS
Silver - ICP-MS
1 ~.ead - ICP-MS
j i/Iercury - AA Cold Vapor
Selenium - ICP-MS
i
1 .ample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
0.02
0.5
O.02
0.04
O.02
O.02
< 0.0005
O.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0989 BMI00092241-68 - CAD0155EMM1
] '
I--, Parameter
Total Recoverable Metals - Acid
| Arsenic - ICP-MS
[ Barium - ICP-MS
Cadmium - ICP-MS
r Chromium - ICP-MS
f Silver - ICP-MS
* Lead -ICP-MS
Mercury - AA Cold Vapor
I Selenium - ICP-MS
I, e
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
O.02
0.5
O.02
O.04
O.02
O.02
< 0.0005
O.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/15/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/16/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 34 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID: Customer Sample ID
S200009-0990 BMI00092241-69 - CAD01561MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Customer
Result
Completed
O.02
<0.5
O.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Sample ID
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
S200009-0991 BMI00092241-70 - CAD01564MM1
Parameter
Total Recoverable Metals - Acid
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Method
EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
Result
Completed
<0.02
<0.5
<0.02
<0.04
<0.02
O.02
< 0.0005
<0.2
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/16/2000
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
Date Sampled
9/16/2000 ,
Detection
Limit
0.02
0.5
0.02
0.04
0.02
0.02
0.0005
0.2
10/16/2000
ALP-855
Client
36913
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Time Sampled
Analyst
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Tretten
Kobza
Tretten
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
Date Received
9/22/2000
Date
Analyzed
9/26/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
9/27/2000
10/2/2000
9/29/2000
William F. Pillsbury
President
Page 35 of 52
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
. :
Sample ID:
200010-0663
Parameter
'otal Recoverable Metals -
arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
, rhromium- ICP-MS
Silver - ICP-MS
",ead- ICP-MS
lercury - AA Cold Vapor
Selenium - ICP-MS
^mple ID:
J2000 10-0664
"
, Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium- ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
§ilver- ICP-MS
HLead- ICP-MS
Vlercury - AA Cold Vapor
Selenium - ICP-MS
Customer Sample ID
BMI00101664-01
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
-CAD01610MM1
Result
Completed
O.02
<0.02
<0.02
O.02
O.02
O.02
<0.0005
0.031
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
BMI00101664-02
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
-CAD01613MM1
Result
Completed
O.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.0005
<0.02
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
Date Sampled
9/28/00
t
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
10/25/00
ALP-855
Client
37235
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
William F. Pillsbury
President
Page 1 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
S2000 10-0665
Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium -ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Sample ID:
3200010-0666
Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Customer Sample ID
BMI00101664-03
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
- CAD01616MM1
Result
Completed
O.02
<0.02
O.02
<0.02
O.02
<0.02
O.0005
0.059
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
BMI00101 664-04
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
-CAD01619MM1
Result
Completed
<0.02
<0.02
<0.02
<0.02
<0.02
<0.02
<0.0005
O.02
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
10/25/00
ALP-855
Client
37235 -
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
1.0/18/00
10/20/00
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
William F. Pillsbury
President
Page 2 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory Sierra
, . ^ Environmental
Analysis Report Monitoring, Inc.
Alpha Analytical
1 255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
;^0001 0-0667
Parameter
7otal Recoverable Metals -
Arsenic - ICP-MS
Barium - ICP-MS
tadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead -ICP-MS
/tercury - AA Cold Vapor
Jelenium - ICP-MS
ample ID:
S2000 10-0668
- ,
Parameter
Total Recoverable Metals -
, Arsenic - ICP-MS
Sarium - ICP-MS
"Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
j.ead - ICP-MS
Mercury - AA Cold Vapor
* Selenium - ICP-MS
1 -- --
Customer Sample ID
BMI00101664-05
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
-CAD0161CMM1
Result
Completed
<0.02
<0.02
O.02
<0.02
0.02
<0.02
O.0005
0.17
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
BMI00101664-06
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
- CAD01620MM1
Result
Completed
<0.02
<0.02
<0.02
<0.02
<0.02
0.02
<0.0005
0.023
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
Date Sampled
9/28/00
Detection *
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
10/25/00
ALP-855
Client
37235
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
William F. Pillsbury
President
Page 3 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem@sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory
Analysis Report
Sierra
Environmental
Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
S2000 10-0669
Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead -ICP-MS
Mercury - AA Cold Vapor
Selenium -ICP-MS
Sample ID:
S2000 10-0670
Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium - ICP-MS
Cadmium - ICP-MS
Chromium - ICP-MS
Silver - ICP-MS
Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Customer Sample ID
BMI00101664-07
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
- CAD01623MM1
Result
Completed
<0.02
<0.02
O.02
<0.02
O.02
O.02
O.0005
0.072
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
BMI00101664-08
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
- CAD01626MM1
Result
Completed
<0.02
<0.02
<0.02
O.02
<0.02
<0.02
O.0005
0.036
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
PO#:
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
10/25/00
ALP-855
Client
37235
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
William F. Pillsbury
President
Page 4 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
Laboratory ISnmental
Analysis Report Monitoring, Inc.
Alpha Analytical
255 Glendale Avenue Suite 21
Sparks, NV 89431
Sample ID:
700010-0671
,-.
Parameter
Total Recoverable Metals -
Arsenic - ICP-MS
Barium - ICP-MS
"admium - ICP-MS
"hromium - ICP-MS
Silver - ICP-MS
, JLead - ICP-MS
vlercury - AA Cold Vapor
- Selenium - ICP-MS
ample ID:
-'t
S2000 10-0672
Parameter
Total Recoverable Metals -
Arsenic--- ICP-MS
Barium - ICP-MS
"Cadmium - ICP-MS
Chromium - ICP-MS
Silver -ICP-MS
..Lead - ICP-MS
Mercury - AA Cold Vapor
Selenium - ICP-MS
Customer Sample ID
BMI00101664-09-
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
CAD01629MM1
Result
Completed
O.02
<0.02
<0.02
<0.02
<0.02
0.15
O.0005
0.02
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Customer Sample ID
BMI00101664-10-
Method
Acid EPA 200.2
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 200.8
EPA 245.1
EPA 200.8
CAD0162CMM1
Result
Completed
0.02
O.02
O.02
O.02
O.02
O.02
O.0005
O.02
Units
Of Measure
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
mg/L
Date:
Client:
Taken by:
Report:
P0#:
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
Date Sampled
9/28/00
Detection
Limit
0.02
0.02
0.02
0.02
0.02
0.02
0.0005
0.02
10/25/00
ALP-855
Client
37235
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Time Sampled
Analyst
Kleinworth
Rivera
Rivera
Rivera
Rivera
Rivera
Rivera
Kobza
Rivera
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
Date Received
10/16/00
Date
Analyzed
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/20/00
10/18/00
10/20/00
William F. Pillsbury
President
Page 5 of 6
1135 Financial Blvd.
Reno, NV 89502-2348
Phone (775) 857-2400
FAX (775) 857-2404
sem @ sem-analytical.com
John Kobza, Ph.D.
John C. Seher
Managers
-------
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping -
Boston Harbor
APPENDIX H
TSS AND CONTAMINANT OF CONCERN 2-DIMENSIONAL PLOTS
-------
-------
!
Pre Survey CAD Cell M19 All Contaminants
42.386-
42.385H
42.3844
Pre-survey Reference CAD M19
9/6/2001 14:13 to 14:24
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
42.386-
42.385-i
42.384-
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
42.386-
42.385-
42.384-I
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
42.386-
42.385-
42.384-
-71.06
-71.058
-71.056
-71.048
Pre-survey Reference CAD M19
9/6/2001 14:13 to 14:24
-71.048
Boston H
Pre-survey Reference CAD M19
9/6/2001 14:13 to 14:24
-71.048
Pre-survey Reference CAD M19
9/6/2001 14:13 to 14:24
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71.054
-71.052
-71.05
-71.048
PAH Concentration
(ng/L)
PCB Concentration
(ng/L)
TPH Concentration
(M9/L)
42.386
42.385-
42.384-
Boston
Pre-survey Reference CAD M19
9/6/2001 14:13 to 14:24
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
Arsenic Concentration
(mg/L)
Chromium Concentration
(mg/L)
-71.048
-------
Run 1 CAD Cell M19 - TPH
42.387
42 386 -
42.385 -
Bosbn Harbor-TPH
I CAD M19-Pre Run 1
42.384- 9,9/2001 1559 b 16.02PM
-71 .058
-71 .056
-71 .054
-71 .052
-71 .05
-71 .048
/ CAD M 8
42386
42 385 -
42 384 --
Bos ton Harbor-TPH
CAD M19 -Run 1
9/9/2001 1659 b 1725PM
-71 .059~ -71.058 -71~D57 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71 05
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
TPH Concentration
(pg/L)
42.387-1
42.386-f~-41
42.385-
42.384-
Boston Harbor-TPH
CAD M19-Post Run 1
9/9/2001 18:33 to 18:37 PM
CADM19
-71.058
-71.056
-71.054
-71.052
-71.05
71.048
-------
Run 1 CAD Cell M19 - PAH
42.387
42.386
42.385-
42.384-
Boston Harbor - PAH
CAD M19 -Pre Run 1
9/9/2001 15:59 to 16:02PM
-71.058
-71.056
-71.054
-71.052
-71.05
42.386-
42.385-
42.384-
Boston Harbor - PAH
CADM19-Run1
9/9/2001 16:59 to 17:25 PM
-71.048
65
60
55
50
45
40
35
30
25
20
15
10
5
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05 TSS Concentration
(mg/L)
42.387-I
42.386--
42.385-
42.384-
Boston Harbor - PAH
CAD M19-Post Run 1
9/9/2001 18:33 to 18:37 PM
PAH Concentration
(ng/L)
-71.058
-71.056
-71.054
-71.052
-71.05
-71.048
-------
Run 1 CAD Cell M19 - PCB
42.387 -
42,386 H
42.385^
| Boston Harbor-PCB
j CAD M19 -PieRun 1
42.384 -] 9/9/2001 15 59 to 16 02PM
|
-71.058
-71.056
-71 .054
-71.052
-71 .05
-71.048
42.386
42.385 -
42.384 -
Bos ton Harbor-PAH
CADM19-Run 1
9/9G001 1659 b 1725PM
-71 .059 -71 .058 -71 .057 -71.056 -71 .055 -71 .054 -71 .053 -71.052 -71 .051
-71 .05
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
PCB Concentration
(ng/L)
42.387 H
42.386 -
42385-
42.384 -
Bos ton Harbor-PCB
CAD M 19 -PostRun 1
9/9/2001 1833 b 1837PM
CAD M 19
-71.058
-71.056
-71.054
-71.052
-71.05
-71.048
-------
Run 1 CAD Cell M19 - Cr
42.385 -
42.384 -
Boston Harbor-Chrom urn
CADM19 -PteRun 1
9/9/2001 1559 b 1602PM
-71.058 -71 .056 -71.054 -71 .052
-71 .05
42386
42.385 -
42.384 -
Boston Harbor-Chum Lm
CAD M19 -Run 1
9/9/2001 1659 b 1725PM
-71 .048
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051
-71 .05
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
42.387-T
42.386-
42.385-
42.384-
Boston Hartrar - Chromium
CAD M19 - Post Run 1
9/9/2001 18:33 to 18:37 PM
CADM19
-71.058
-71.056
-71.054
-71052
-71.05
Chromium Concentration
(mg/L)
-71.048
-------
Run 2 CAD Cell Ml9 - TPH
9/9/2001 07:19 to 07:28 PM
42.385
-71.064 -71.062 -71.06 -71.058 -71.056 -71.054 -71.052
42.387-
42.386-
42.385-
42.384-
Boston Harbor - TPH
CADM19-Run2
9/10/2001 08:51 to 09:40 AM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05 -71.049 -71.048
j65
J60
55
50
45
40
135
30
25
20
15
10
5
TSS Concentration
(mg/L)
TPH Concentration
(M9/L)
42.38i
42.385-
42.384-
Boston Harbor - TPH
CAD M19-Post Run 2
9/10/2001 10:14 to 10:19 AM
-71.06 -71.058 -71.056 -71.054 -71.052
-71.05
-------
Run 2 CAD Cell
42.388-
-
42.387-
42.386-
42.385-
Boston Harbor - PAH
CADM19-Pre Run 2
9/9/2001 07:19 to 07:28 PM
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
42.387-
42.386
42.385-
42.384-
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
^^^^^^^^_ , (mg/L)
9/10/2001 08:51 to 09:40 AM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -7l'.05 -71.049 -71.048
PAH Concentration
(ng/L)
42.386-
42.385-
42.384-
Boston Harbor-PAH
CAD M19 -Post Run 2
9/10/2001 10:14 to 10:19 AM
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
,
-------
Run 2 CAB Cell M19 - PCB
42 .388
42.387 -
42.386 -
42 385 -
CAD M 19
Bosbn Harbor-PCB
CADM19-Pre Run 2
9/9/2001 0719 to 0728PM
-71 .064 -71 .062
-71 .06 -71 .058 -71 .056 -71 .054 -71 .052
42.387 -
42.386
42,385 -
42.384 -
Boston Harbor-PCB
CAD M 19-Run 2
9/10/2001 0851 to 09:40 AM
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71 .059 -71 .058 -71 .057 -71 .056 -71 .055 -71 .054 -71.053 -71 .052 -71 .051 -71 .05 -71 .049 -71 .048
42.386 -
42.385 -
42.384 -
CADM19
Bos ton Harbor-PCB
CAD M19 -PostRun2
9/10/2001 10:14 to10:19AM
-71 .06
-71 .058
-71.056
-71.054
-71.052
-71
-------
Run 3 CAD Ceil Ml 9 - TPH
'
42.386-
42.385-j
Boston Harbor - TPH
CAD M19 -Pre Run 3
42384- 9/10/2001 23:16 to 23;21 PM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -711)52 -71.051 -7105 -71.049
42.386-
42.385-
42.384-
CADM19-Run3
9/11/2001 01:13 to 01:41 AM
-71.058
-71.056
-71.054
-71.052
-71.05
-71.048
65
60
55
50
45
! 40
135
30
25
20
15
10
5
TSS Concentration
(mg/L)
42.387-
42.386-
42.385-
42.384-
Boston Harbor-TPH
CAD M19 - Post Run 3
9/11/2001 02:25 AM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05 -71.049
TPH Concentration
(jJEfI-5
-------
Run. 3 CAD Cell M19 - PAH
42.386-
42.385-
42.384-
Boston Harbor - PAH
CAD M19 - Pre Run 3
9/10/2001 23:16to23;21 PM
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05 -71.049
42.386-+
42.385-
42.384-
Boston Harbor - PAH
CAD M19-Run 3
9/11/2001 01:13 to 01:41 AM
-71.058
-71.056
-71.054
-71.052
-71.05
-71.048
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
42.387-
42.386
42.385-I
42.384
Boston Harbor - PAH
CADM19-PostRun3
9/11/2001 02:25 AM
PAH Concentration
(ng/L)
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71.05 -71.049
-------
Run 3 CAD Cell M19 - PCB
42.386-
42.385
Boston Harbor-PCB
CADM19 -PreRun 3
42384 ' 9flo/2001 23:16 to 2321PM
-71 .059 -71 .058 -71 .057 -71 .056 -71 .055 -71 .054 -71.053 -71 .052 -71 .051 -71 J05 -71 .049
42386
42385-
42 384 -
Boston Harbor-PCB
CAD M19-Run 3
9/11/2001 01 13 to 01 :41 AM
-71 .058
-71.056
-71 .054
-71 .052
-71 .05
-71 .048
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
42.387 -
42.386 -
42 385 -
42.384 -
Bos ton Harbor-PCB
CAD M19 -PostRunS
9/11/2001 0225AM
CAD M 19
-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052 -71.051 -71 !o5 -71.049
-------
Pre Survey CAD Ceil M8 All Contaminants
j
42.387-
42.386-1
42.385
Boston Harbor - Arsenic
Pre-survey Reference CADM8
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
42.385-
Boston Harbor - PAH
Pre-survey Reference CADM8
42.387-
42.386-
Boston Harbor - Chromium
Pre-survey Reference CADM8
42.385-j 9/6/2001 11:43
-71.064
42.387-
42.386-
-71.064
-71.062
65
60
J55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
PAH Concentration
(ng/L)
-71 058
-71.056
-71.054
-71.052
42.387-
42.386-
42.385-
Boston Harbor - PCB
Pre-survey Reference CADM8
9/6/2001 11:43
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
PCB Concentration
(ng/L)
TPH Concentration
(M9/L)
Arsenic Concentration
(mg/L)
42.387-
42.386-
42.385-
Boston Harbor - TPH
Pre-survey Reference CADM8
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
Chromium Concentration
(mg/L)
-------
Run 5 CAD Cell M8 - TPH
r
42.387-
42.386-
42.385-H
Boston Harbor TPH
CAD M8 - Pre Run 5
9/14/2001 03:33 to 03:37AM
-71.064 -71.062 -71.06 -71.058 -71.056 -71.054 -71.052
42.387-
42.386-
42.385-
42.387-
42.386-
42.385-
42.384-I
Boston Harbor - TPH
CAD M8 - Run 5
9/15/2001 04:52 to 05:39 AM
-71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
Boston Harbor-TPH
CAD M8 - Post Run 5
9/14/2001 06:11 to 06:16 AM
65
60
55
50
45
40
35
30
25
20
15
10
5
'-10
TSS Concentration
(mg/L)
TPH Concentration
(M9/U)
-71.064 -71.062 -71.06 -71.058 -71.056 -71.054 -71.052
-------
Run 5 CAD Cell
42,387-i
42.386-
42.385-1
Boston Harbor - PAH
GAD M8 - Pre Run 5
9/14/2001 03:33 to 03:37AM
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
42.387-
Boston Harbor - PAH
CAD M8 - Run 5
0/15/2001 04:52 to 05:39 AM
318 247
42.386-
% VS? 103
? A * 136
CAD MS 312
42.385-
CADM19
-71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.387-
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Post Run 5
9/14/2001 06:11 to 06:16 AM
42.384-t-
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
65
60
55
50
45
40
35
30
25
120
15
10
5
'-10
TSS Concentration
(mg/L)
PAH Concentration
(ng/L)
-------
Run 5 CAD Cell M8 - PCS
42.387-1
42,386-
42.385-
CADM8-Pre Run 5
9/14/2001 03:33 to 03:37AM
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
42.387-
42.386-
42.385-
42.387-
42.386-
42.385-
Boston Harbor - PCB
CAD M8 - Run 5
1/15/2001 04:52 to 05:39 AM
-71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.384-L
Boston Harbor - PCB
CAD M8 - Post Run 5
9/14/2001 06:11 to 06:16 AM
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
;65
60
55
50
45
40
35
30
25
20
15
10
IS
'-10
TSS Concentration
(mg/L)
PCB Concentration
(ng/L)
-------
Run 5 CAD Cell
42.387-
42.386-
42.385-
Boston Harbor - Arsenic
CAD M8 - Pre Run 5
9/14/2001 03:33 to 03:37AM
-71.064
-71.062
-71.06
-71.05.8
-71.056 -71.054 -71.052
42.387-
42.386-
42.385-
Boston Harbor - Arsenic
CAD M8 - Run 5
9/15/2001 04:52 to 05:39 AM
I I I 1 1 1 1 1 !
-71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
Arsenic Concentration
(mg/L)
42.387-
42.386-
42.385-
42.384-I
Boston Harbor - Arsenic
CAD M8- Post Run 5
9/14/2001 06:11 to 06:16 AM
-71.064
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
-------
Run S CAD Cell M8 - Cr
42.387-1
42.386^
42.385-
Boston Harbor - Chromium
CAD M8 - Pre Run 5
9/14/2001 03:33 to 03:37AM
-71.064 -71.062
-71.06
-71.058 -71.056 -71.054 -71.052
42.387-
42.386-
42.385-
Boston Harbor - Chromium
CAD M8 - Run 5
9/15/2001 04:52 to 05:39 AM
-71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
Chromium Concentration
(mg/L)
42.387-
42.386-
42.385-
42.384-1
CAD M8 - Post Run 5
9/14/2001 06:11 to 06:16 AM
-71.064 -71.062 -71,06 -71.058 -71.056 -71.054 -71.052
-
-------
Run 6 CAD Cell M8 - TPH
42.387-
42.386-n
Boston Harbor - TPH
CAD M8 - Pre Run 6
42.385-j g/15/2001 08:45 to 08:50 AM
-71.062 -71.061 -7i.06 -71,059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.387-
42.386-
42.385-
CADM8
Boston Harbor - TPH
CAD M8 - Run 6
9/15/2001 09:52 to 10:25 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
TPH Concentration
(W/L)
42,386-
42.385-
Boston Harbor - TPH
CAD M8 -Post Run 6
9/15/200 11:36 to 11:50 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
-------
Run 6 CAD Cell M8 - PAH
r
42.387-
42.386-1
42.385-
Boston Harbor - PAH
CAD M8 - Pre Run 6
9/15/2001 08:45 to 08:50 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.387-
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Run 6
9/14/2001 08:45 to 08:50 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
'
PAH Concentration
(ng/L)
42.386-
42.385-
Boston Harbor - PAH
CAD M8 -Post Run 6
9/15/200 11:36 to 11:50 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
-------
Run 6 CAD Cell M8 - PCB
42.387-
42.386-
42.385-
Boston Harbor - PCB
CAD M8 - Pre Run 6
9/15/2001 08:45 to 08:50 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.387-
42.386-
42.385-
CAD M8
Boston Harbor - PCB
CAD M8 - Run 6
9/15/2001 09:52 to 10:25 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
PCB Concentration
(ng/L)
42.386-
42.385-
Boston Harbor - PCB
CAD M8 -Post Run 6
9/15/200 11:36 to 11:50 AM
-71.062 -71.061 -71'.06 -71.059 -71.058 -71.057-71.056 -71.055 -71.054 -71.053 -71.052
-------
Run 7 CAD Cell M8 - TPH
r
42.386
Boston Harbor - TPH
j CAD MS - Pre Run 7
42384! 9/15/2001 11:35 to 11:41 PM
-71.062 -71.06 -71.058 -71.056 -71.054 -71.052 -71.05
-71.048
42.387-
42.386-
42.385-
Boston Harbor - TPH
CAD M8 - Run 7
9/16/2001 12:09 to 12:44 AM
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
TPH Concentration
42.387-
42.386-1
42.385-
Boston Harbor - TPH
CAD M8 - Post Run 7
9/16/2001 01:33 to 01:39 AM
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
-------
Run 7 CAD Cell
42.386
i
Boston Harbor - PAH
| CAD M8 - Pre Run 7
42384-i 9/15/2001 11:35 to 11:41 PM
-71.062
-71.06
-71.058
-71.056 -71.054
-71.052
-71.05
-71.048
42.387-
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Run 7
9/16/200 12:09 to 12:44 AM
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
PAH Concentration
(ng/L)
42.387-
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Post Run 7
9/16/2001 01:33 to 01:39 AM
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
-------
Run 7 CAD Cell M8 - PCB
.
42.386J
42.384-
Boston Harbor - PCB
CAD M8 - Pre Run 7
9/15/2001 11:35 to 11:41 PM
-71.062 -71.06 -71.058 -71.056 -71.054 -71.052 -71.05 -71.048
42.387-
42.386-
42.385-
Boston Harbor - PCB
CAD M8 - Run 7
9/16/2001 12:09 to 12:44 AM
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
'
42.387-
42.386-
42.385-
Boston Harbor - PCB
CAD M8 - Post Run 7
9/16/2001 01:33 to 01:39 AM
-71.062
-71.06
-71.058
-71.056
-71.054
-71.052
PCB Concentration
(ng/L)
-------
Run 8 CAD Cell M8 - TPH
42.388-
42.387
42.386-
42.385-
Boston Harbor - TPH
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
CAD M19
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388-1
42.387-
42.386-
42.385-
Boston Harbor -
CADM8 Run8
9/20/2001 1.0:34.to..1.1
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
TPH Concentration
42,387-
42.386-
42.385-
Boston Harbor - TPH
CAD MS - Post. Run 8
9/20/2001 11:52 AM to 12:00 PM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71,052
-------
Run 8 CAD Cell MS - PAH
42,388-
42.387-
42.386-1
42.385-
Boston Harbor - PAH
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388-f
42.387-1
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Run 8
9/20/2001 10:34 to 11:12 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
PAH Concentration
(ng/L)
42.387-
42.386-
42.385-
Boston Harbor - PAH
CAD M8 - Post Run 8
9/20/2001 11:52 AM to 12:00 PM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
-------
RUE 8 CAD Cell M8 - PCB
42.388-
42.387-
42.386
42.385-
Boston Harbor - PCB
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388-H
42.387-
42.386-
42.385-
Boston Harbor -
CAD M8 - Run 8
9/20/2001 10:34 to-11:12 AM
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.387
Boston Harbor - PCB
--CAD M8-Post Run-8
9/20/2001 11:52 AM to 12:00 PM
-71.061 -71.06 '-71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
PCB Concentration
(ng/L)
-------
-As
-
42.388-
42.387-
42.386-
42.385-
Boston Harbor - Arsenic
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388-f
42.387-
42.386-
42.385-
9/20/2001 10:34 to 11:12 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
Arsenic Concentration
(mg/L)
42.387
42.386-
42.385-
Boston Harbor - Arsenic
CAD M8 - Post Run 8
9/20/2001 11:52 AM to 12:00 PM
~i I I \ i 1 i i 1 .
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
-------
Run 8 CAD Ceil M8 - Cr
42.388-1
42.387-
42.386-
42.385-
Boston Harbor - Chromium
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388H
42.387-
42.386-
42.385-
Boston Harbor -
CAD M8 - Run 8
9/20/200 T 10:34 to 11:12 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
30
25
20
15
10
5
TSS Concentration
(mg/L)
Chromium Concentration
(mg/L)
42.387-
42.386-
42.385-
Boston Harbor - Chromium
CAD M8 - Post Run 8
9/20/2001 11:52 AM to 12:00 PM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
-------
-
Run 8 CAD Cell M8 - Hg
42.388-
42.387-
42.386-
42.385-
Boston Harbor - Mercury
CAD M8 - Pre Run 8
9/20/2001 09:43 to 09:53 AM
I i I I i ~i 1 1 i 1
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
42.388-I
42.387-
42.386-
42.385-
Boston Harbor - Mer
CAD MB - Run 8
9/20/2001 10:34 to 11.-12 AM
-71.062 -71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
65
60
55
50
45
40
35
J30
25
20
15
10
5
TSS Concentration
(mg/L)
o
Mercury Concentration
(mg/L)
L
42.387-
42.386-
42.385-
Boston Harbor - Mercury
CAD-M8- Post Run 8
9/20/2001 11:52 AM to 12:00 PM
-71.061 -71.06 -71.059 -71.058 -71.057 -71.056 -71.055 -71.054 -71.053 -71.052
'
-------
Post Survey CAD Cell M8 All Analytes
42,387-
42.386-^
42.385-
Post-survey Reference CAD MB
9/28/2001 09:37 to 09:51 AM
-71.06
-71.058
-71.056
-71.054
-71.052
42.386-
42.385-
Boston Harbor - Lead
Post-survey Reference CAD M8
9/28/2001 09:37 to 09:51 AM
-71.06
-71.058
-71,056
-71.054
-71.052
42.387-
42.386-
42.385-
-71.05
-71.05
Boston Harbor - PCB
Post-survey Reference CAD M8
9/28/2001 09:37 to 09:51 AM
65
60
55
50
45
40
3.5
30
25
20
15
10
5
TSS Concentration
(mg/L)
PAH Concentration
(ng/L)
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
42.387-
42.386-
42.385-
Boston Harbor - Selenium
Post-survey Reference CAD M8
9/28/2001 09:37 to 09:51 AM
-71.06
-71.058
-71.056
-71.054
-71.052
-7l'.05
-71.06
-71.058
-71.056
-71.054
-71.052
-71.05
PCB Concentration
(ng/L)
TPH Concentration
Selenium Concentration
(mg/L)
Boston Harbor - TPH
Post-survey Reference CAD M8
9/28/2001 09:37 to 09:51 AM
o
Lead Concentration
(mg/L)
-------
EPA/540/R-05/014
Evaluation of Sediment Agitation and
Mixing into the Surrounding Water
Column from Capping Activities -
Boston Harbor
APPENDIX I
AVERAGE CURRENT VELOCITY PLOTS
-------
-------
Slick Ship Tiiielt |Ref: Bum
Ship Track Average
.500'
621
East fin]
-------
Slick Slii|) Tliick (Reft Bun)
Distance E.ist [ml
-------
1
Stick Ship Ti.ick (Reft Btm)
Ship Trad* Average
-50Q1
-621
100
Distance East fmjj
-------
9/11
Slick Sliip Tiock'(Ref:Bnu)
Ship Track Average
-500'
-621
100
Distance East |m]
-------
'/12
Stick Ship Tiack (Ref: Btin)
600'
-821
100
Distance Eiist (ml
-------
9/13
Stick Ship Ti.ick (Ref: Bun)
-Ship Tiaek Aveiage
-5D01
-621
Distance Easi fm]
-------
'/14
Slick Ship Tiack (Ref: Bun)
Ship Track Avetage
-500'
-821
100
ce East fut]
-------
9/15
Slick SJit[> Tiock (Ref: Btml
Ship Track Average
193
Distance East [in]
-------
1
Stick Ship Tiiick (Ref: Btm)
Distance East fm]
-------
Stick Ship Tuick {Ref: Blm)
Ship Tuck Auetage
300
-3001
-677
100
Distance East (mj|
------- |