United States
Environmental Protection
Agency
EPA-60Q/R-97-134b
November 1997
OF
THE
OF M
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FOREWORD
The U.S. Environmental Protection Agency is charged by Congress with protecting
the Nation's land, air, and water resources. Under a mandate of national
environmental laws, the Agency strives to formulate and implement actions leading
to a compatible balance between human activities and the ability of natural systems
to support and nurture life. To meet this mandate, EPA's research program is
providing data and technical support for solving environmental problems today and
building a science knowledge base necessary to manage our ecological resources
wisely, understand how pollutants affect our health, and prevent or reduce
environmental risks in the future.
The National Risk Management Research Laboratory is the Agency's center for
investigation of technological and management approaches for reducing risks from
threats to human health and the environment. The focus of the Laboratory's
research program is on methods for the prevention and control of pollution to air,
land, water, and subsurface resources; protection of water quality in public water
systems; remediation of contaminated sites and groundwater; and prevention and
control of indoor air pollution. The goal of this research effort is to catalyze
development and implementation of innovative, cost-effective environmental
technologies; develop scientific and engineering information needed by EPA to
support regulatory and policy decisions; and provide technical support and
information transfer to ensure effective implementation of environmental
regulations and strategies.
This publication has been produced as part of the Laboratory's strategic long-term
research plan. It is published and made available by EPA's Office of Research and
Development to assist the user community and to link researchers with their
clients.
E. Timothy Oppelt, Director
National Risk Management Research Laboratory
EPA REVIEW NOTICE
This report has been peer and administratively reviewed by the U.S. Environmental
Protection Agency, and approved for publication. Mention of trade names or
commercial products does not constitute endorsement or recommendation for use.
This document is available to the public through the National Technical
Information Service, Springfield, Virginia 22161.
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EVALUATION OF EMISSIONS FROM THE
OPEN BURNING OF HOUSEHOLD WASTE IN BARRELS
Volume 2. Appendices A-G
Prepared by:
Paul M. Lemieux
U.S. Environmental Protection Agency
National Risk Management Research Laboratory
Air Pollution Prevention and Control Division
Research Triangle Park, NC 27711
Prepared in Cooperation with:
New York State Department of Health
Bureau of Toxic Substances Assessment
and
New York State Department of Health
Wadsworth Center for Laboratories and Research
Albany, NY 12202
Prepared for:
U.S. Environmental Protection Agency
Office of Research and Development
Washington, D.C. 20460
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ABSTRACT
A detailed emissions characterization study was undertaken to examine, characterize, and quantify emissions from
the simulated burning of household waste materials in barrels. This study evaluated two separate waste streams: that
of an avid recycler, who removes most of the recyclable content from the waste stream prior to combustion; and that
of a non-recycler, who combusts the entire stream of household waste. Estimated emissions were developed in units
of mass emitted per mass of waste burned. Continuous gas samples were analyzed for oxygen, carbon dioxide,
carbon monoxide, nitric oxide, and total hydrocarbons. Gas-phase samples were collected using SUMMA®
canisters and analyzed by gas chromatography/mass spectrometry (GC/MS) for volatile organic compounds
(VOCs). Extractive samples from the combined paniculate- and gas-phase were analyzed for semivolatile organic
compounds (SVOCs), polycyclic aromatic hydrocarbons (PAHs), polychlorinated biphenyls (PCBs),
chlorobenzenes (CBs), polychlorinated dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs),
aldehydes and ketones, hydrogen chloride (HC1), hydrogen cyanide (HCN), and metals. Emissions of PMjo and
PM2.5 were also measured. Ash residue samples were analyzed for SVOCs, PCBs, PCDDs/PCDFs, and metals.
It was found that for most of the non-chlorinated compounds, including VOCs, SVOCs, PAHs, and aldehydes and
ketones, emissions from the non-recycler were higher, both on a per mass burned basis and on a per day basis (using
waste generation estimates from New York State). However, emissions of many of the chlorinated organics,
particularly CBs and PCDDs/PCDFs, were higher from the avid recycler, on a per mass burned basis. From
estimates of waste generated each day by New York households for the avid recycler and non-recycler scenarios,
emissions per day of PCDDs/PCDFs are significantly higher for the avid recycler. Emissions of PCBs were higher
from the non-recycler, although the cause of this phenomenon is not known. This phenomenon is likely due to
several factors, including the higher mass fraction of PVC in the avid recycler's waste. It is also possible that some
component of the non-recycler's waste may potentially serve to poison the metallic catalysts believed to be
responsible for enhancing formation rates of PCDDs/PCDFs. Results from HC1 sampling indicated much higher
HC1 emissions from the avid recycler, which is consistent with the higher emissions of chlorinated organics, and ash
residue analysis indicated that the avid recycler's residue had more copper, which could contribute to higher
emissions of PCDDs/PCDFs. It was noted that the temperature at the base of the burning bed was significantly
lower in the case of the avid recycler than it was for the non-recycler. Gas-phase emissions of metals were not a
strong function of the test conditions. PM emissions were much higher from the non-recycler. Almost all of the PM
emissions from both test conditions were < 2.5 |jm in diameter.
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TABLE OF CONTENTS
Technical Report Vol. 1
Abstract ii
Appendix A: Quality Control Evaluation Report A-l
Start and Stop Times for the Various Sampling Systems During the Experiments A-l
Data Quality Indicator Summary for Critical Measurements A-2
Weight Accuracy Check A-3
Volatiles Recoveries (Surrogates and Internal Standards) A-4
Post-Sampling Surrogate Recoveries A-5
PCDD/PCDF Sample Recoveries A-9
Appendix B: CEMData B-l
Appendix C: CEM Calibration Logs C-l
Appendix D: Fuel Preparation Notes D-l
Appendix E: Sample Custody Sheets E-l
Appendix F:
AcurexRaw VOC Analytical Data F-l
Acurex Raw SVOC Analytical Data F-3
Aldehydes andKetones F-27
HCL F-28
HCN F-28
PM F-29
Appendix G: WCL&R Raw Analytical Data
Chlorobenzene Analytical Data G-l
WCL&R SVOC Analytical Data G-3
WCL&R PAH Analytical Data G-6
WCL&R PCDD/PCDF Analytical Data G-8
WCL&R PCB Analytical Data G-10
WCL&R Metals Analytical Data G-13
WCL&R Hg Analytical G-17
WCL&R Ash Analytical Data G-19
in
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APPENDIX A
QUALITY CONTROL EVALUATION REPORT
This project was conducted under the guidance of an EPA-approved QA Test Plan (APPCD Category III) and an
approved Facility Manual for the test facility. These documents establish data quality objectives suitable for this
study. The quality control measures employed during this study were used to ensure that the data collected would
be suitable to measure air emissions resulting from open combustion of household waste.
Table A-l lists the sample start and stop times for all of the sampling devices.
Table A-l. Start and Stop Times
date
start background sampling
ignition time
Dioxin train
Aldehyde/Ketone train
Dichotomous Sampler
Semi-Vol train
Multi-Metals train
HCN train
HC1 train
SUMMA Can
Burn Ends/Door Opened
Test #1
Avid Recycler
8/30/95
14:26
14:39-14:41
14:43-15:55
14:43-15:43
14:43-15:32
14:43-15:55
14:43-15:53
14:43-15:55
14:43-15:55
14:42-15:55
15:58
for the Various Sampling Systems During the Experiments
Test #2
Avid Recycler
9/1/95
11:38
12:00-12:01
12:03-13:22
12:03-13:03
12:03-13:22
12:03-13:22
12:03-13:22
12:03-13:22
12:03-13:22
12:03-13:19
13:24
Test #3
Hut Blank
9/6/95
13:06
n/a
13:25-14:25
13:25-14:25
13:25-14:55
13:25-14:25
13:25-14:55
13:25-14:55
13:25-14:55
13:27-14:57
14.57
Test #4
Non Recycler
9/8/95
12:17
12:32-12:35
12:36-13:36
12:36-13:36
12:36-13:36
12:36-13:36
12:36-13:36
12:36-13:36
12:36-13:36
12:37-13:37
13:37
Test #5
Non Recycler
9/12/95
10:15
10:30-10:31
10:32-12:02
10:32-11:32
10:32-12:02
10:32-12:02
10:32-12:02
10:32-12:02
10:32-12:02
10:32-12:02
12:02
Table A-2 presents the data quality indicator (DQI) summaries for accuracy, precision, and completeness achieved
during testing along with the planned DQI goals for each measurement or analysis performed. In general, the
intended DQI goals were achieved. In several instances, however, targeted DQI goals were not achieved or could
not be assessed from the available data.
Case narratives for specific analytical activities are included in the following subsections.
A-1
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NO
TableA-2 Data Quality
Measurement Objective
Accuracy
(% Bias)
O2
CO2
CO
THC
NO
Temperature
Burn Hut Weight
Filter Weight
VOCs
SVOCs
PCDDs/PCDFs
Metals
HC1
Aldehydes & Ketones
HCN
Burn Hut Flow Rates
Dichotomous Flow Rates
±5
±5
±5
±5
±5
±2
±15
±15
NA
NA
NA
10
NA
NA
NA
25
25
Objective Objective
Accuracy Precision
(% QA/QC (% RPD)
Recovery)
NA
NA
NA
NA
NA
NA
NA
NA
40-120
40-120
40-120
75-125
80-120
70-130
80-120
NA
NA
5
5
5
5
5
±2
15
15
30
30
30
20
15
15
15
25
25
Indicator Summary for Critical Measurements
Objective Objective Achieved Achieved
Recovery Completeness Accuracy (% Accuracy (%
(%) (%) bias) QA/QC
Recovery)
NA
NA
NA
NA
NA
NA
NA
NA
50-150
18-120
40-120
NA
NA
NA
NA
NA
NA
70
70
70
70
70
100
100
100
75
70
75
80
75
75
75
100
90
0
3
3
0.1
4
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
-2.41 ->6.59
NA
NA
NA
NA
NA
NA
NA
NA
79-102
NA
*
75-125
NA
75-125
4.3
NA
NA
Achieved
Precision
5
5
5
5
5
±2
5.75
0.25
25
NA
*
20
NA
±25
3
2.4
1.2
Achieved Achieved
Recovery Completeness
NA
NA
NA
NA
NA
NA
NA
NA
79-102
15-135
*
NA
NA
NA
NA
NA
NA
100
100
100
100
100
100
100
100
100
100
42
100
100
100
100
100
100
* - see narrative text
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A.1 Air Continuous Measurement Results
The O2 analyzer was behaving erratically, and could not be feasibly replaced during the tests. For those reasons, an
Ecom suitcase-type 62 analyzer was used as a supplement, but computer problems marred the use of the Ecom
analyzer as well. For this reason, the 62 data shown in the CEM traces is of questionable accuracy, however,
qualitatively serves to show that 62 levels did not significantly deviate from ambient levels.
The CEM data also included temperature data. The data were recorded using two EXP-16 analog to digital
converter boards connected to a DASH-8 computer interface board. The computer was running LabTech Notebook
software which has the capability to convert voltages to temperatures for common thermocouple types. After the
tests were completed, the data were examined and it was found that the data was not intuitively correct, showing
much lower temperatures than would be reasonably expected. On further examination is was found that the gain
switch on the EXP-16 board used to acquire thermocouple data was in the wrong position. To derive a correction
factor for the data, a thermocouple temperature generator was used to replace one of the thermocouples. Signals
corresponding to temperatures ranging from 0-1200 °C were fed into the EXP-16 board using the same gain switch
setting as during the tests. The temperatures recorded by the data system were observed. These observations
yielded a calibration curve recorded during the burn. This calibration curve was used to correct thermocouple
readings during the experiments. An examination of the calibration curve and the transformed data set suggests that
this gain switch setting resulted in a loss of sensitivity to small temperature changes near ambient and a greater
potential for error in this temperature range.
The filter weight balance was calibrated on September 5, 1995. It registered 1.00247 g on a Ig weight and 0.50138
g on a 0.5 g weight. The balance in the burn hut was calibrated and Table A-3 lists results from the calibration.
Table A-3. Weight Accuracy Check
Test Weight (Ib)
1
o
J
6.1
6.6
7.4
11
17
30.5
Observed Weight (Ib)
0.8
2.8
5.6
6.6
7.2
11
16.8
30.2
Bias (%
25.00
7.14
8.93
0.00
2.78
0.00
1.19
0.99
of measured value)
A-3
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A.2 Air Volatile Organic Compound Analyses
Recoveries of the standards were acceptable for the volatile organic analyses. However, it should be noted that the
volatile organic analysis was done using the external standardization provisions of Method TO-14, and thus the
internal standards are really surrogates, and it would be expected that recoveries would be good for these types of
analytes since the spiking is performed into the purge vessel at the time of analysis. Table A-4 lists the recoveries of
the standards.
Table A-4. Volatiles Recoveries (Surrogates and Internal Standards)
Avid
Recycler
Test #2
Compound
bromochloromethane
d4-l,2-dichloroethane
1 ,4-diflurobenzene
d8-toluene
d5 -chlorobenzene
4-bromofluorobenzene
Target
Mass
ng
100
100
100
100
100
100
Meas.
Mass
ng
102.3
97.71
94.81
94.18
91.08
80.81
Rec.
102.3
97.71
94.81
94.18
91.08
80.81
Hut
Blank
Meas.
Mass
ng
92.97
99.27
98.35
99.65
100.4
91.02
Rec.
92.97
99.27
98.35
99.65
100.4
91.02
Non
Recycler
Test#l
Meas.
Mass
ng
102.01
100.22
96.38
95.79
94.11
83.29
Non
Recycler
Test #2
Rec.
102.01
100.22
96.38
95.79
94.11
83.29
Meas.
Mass
ng
101.44
95.66
90.18
90.79
90.34
79.05
Rec.
101.44
95.66
90.18
90.79
90.34
79.05
A.3 Air Semivolatile Organic Compound Analyses
A.3.1AEC Analyses
Table A-5 lists the post-sampling surrogate recovery limits. A pre-sampling surrogate, D 10-anthracene, was added
to these samples and recovery limits should parallel those listed for the post-sampling surrogates. These samples
were extracted in late summer of 1995 but were analyzed in late summer of 1996, (the delay was due to budgetary
constraints) therefore analytical hold times were exceeded. However, most samples demonstrated acceptable post-
sampling surrogate recoveries with the main exceptions being the Hut Blank and Non-Recycler #4. The Hut Blank
had post sampling surrogate recoveries between 7.5 and 14.3 % and Non-Recycler #4 had post sampling recoveries
between 1.1-17.0%. Pre-sampling surrogates had recovery values of 69.3 and 80.5 %, respectively. This indicates a
spiking problem for the post-sampling surrogates and does not invalidated the reported target analyte values for
these samples. All samples demonstrated an increasing trend with an increase in surrogate boiling point. This is
likely due to the extraction process and likely biased lighter target analytes slightly downward. The top 20 peaks
which were non-target analytes were also reported as tentatively identified compounds. Two different batches of
XAD may have been used during the sampling process. Both batches were analyzed (9608002 and 9608003) and
found to have slight phthalate contamination. A glassware blank (9608004) was also analyzed and this also had
slight phthalate contamination.
A-4
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Table A-5. Post-Sampling Surrogate Recoveries
Compound
2-fluorophenol
D5-phenol
D5-nitrobenzene
2-fluorobiphenyl
2,4,6-tribromophenol
D14-terphenyl
Lower Limit (%)
17.4
22.4
10.0
15.3
10.0
13.8
Upper Limit (%)
131.8
133.2
130.6
136.5
135.0
143.4
A.3.2 WCL&R Analyses
Daily QC performance checks met all EPA criteria.
Instrument detection limits were obtained by replicate injection of 20 ng of each analyte. MDLs were also obtained
for our 8270 method but these were based on replicate extractions of aqueous samples, not entirely relevant to these
analyses. Standards were not available for several analytes at the time of injection but ions and retention times
obtained from the EPA method were used to scan for these.
The initial calibration performed prior to air sample analysis was slightly improved over the previous curve for ash
analysis. 1,4-Phenylenediamine, N-Nitrosodimethylamine, benzyl alcohol, hexachlorocyclopentadiene,
chlorobenzilate, famphur, benzo(b)fluoranthene and 7,12- dimethylbenz(a)anthracene exhibited %RSDs greater than
25%. Of these, only 1,4-phenylenediamine and famphur exhibited a %RSD greater than 32%. 1,4-
Phenylenediamine is not readily chromatographed and Famphur had not been evaluated for the earlier curve.
In addition to a subset of CLP surrogate spikes, anthracene-dlO had been added to extracts as a recovery standard.
Although an ampule of anthracene-dlO was provided by Acurex, this was not included in the mixture of surrogates
which we analyzed. Quantification of this analyte was performed by assuming a response of 1 relative to
phenanthrene-d 10.
The concentrations of anthracene-dlO and other surrogates were clearly much higher than expected from the
description we received and also beyond our calibration range, except where recoveries were low. Further, the
phenols exhibited concentration-dependent shifts in retention times at these high levels (an advantage of MS
detection is that we can still identify and quantify, even where such shifts occur; no ambiguities resulted from these
shifts). Since it is inappropriate to dilute samples for which only surrogates are beyond the calibration range, we
reported results only for the undiluted runs.
The XAD extracts from the air sampling procedure had plasticizers (di-C8 to di-CIO phthalates and di-C8-adipates)
as their most abundant non-target analytes (these were even more abundant in the hut and/or field blanks than in the
A-5
-------
samples). Some samples and blanks also exhibited abundant siloxanes, from hexamethylcyclotri-siloxane to
hexadecamethylcyclooctasiloxane. We also found di-lauryl thiopropionate in these samples and blanks, as we also
had for the ash samples [this is not a background substance which we normally encounter].
A.4 Air Chlorobenzene Analyses
A 100 |jL portion of the extracts was spiked with 26 (j^L of a 10 ng/|jL ^C-Cli-6 Chlorobenzene internal standard
mix. A 1 |j,L portion of the resulting 126 |jL was injected onto the GC/MS system operating in selected ion
monitoring (SIM) mode. Quantitation of the Chlorobenzene isomers was perfomed using the internal standard
method. Calculations for all these analyses were based on 1 mL original extract volume.
Analysis was performed on a Hewlett Packard 5890 Series II Gas Chromatograph (fitted with a Hewlett Packard
7673 automated injector), with programmable carrier gas pressure, the column of which was interfaced directly to
the source of a Hewlett Packard 5971 Mass Selective Detector. The column was a 60M x 0.25mm DB-5 column
(0.25|j, film). Injection volume was 1 |J,L using splitless injection. The helium pressure was programmed to start at
80 PSI for 1 minutes then ramped at 99 PSI/min to 30 PSI then ramped at 5 PSI/min to 45 PSI and maintained at that
pressure for the remainder of the run. The oven temperature was held at 70°C for 2 min, ramped at 8 deg/min to
300°C then held for 5 minutes.
Daily performance checks met all criteria for mass calibration and tuning. Multilevel standards were run to establish
linearity and response factors obtained were checked for continuing calibration.
Average recovery for the five labeled Chlorobenzene internal standards was 80% (average sample range 35% to
95%). Sample 9582045 had a low average recovery 35% the five other samples were all in excess of 80%.
Detection limits were generally less than 0.5 ng/mL of original extract.
A.5 Air PAH Analyses
A 10 |jL portion of the extracts was spiked with 1 |j,L of a 10 ng/|jL ^H-PAH internal standard mix containing 17
deuterated compounds. A 1 |jL portion of the resulting 11 |jL was injected onto the GC/MS system operating in
selected ion monitoring (SIM) mode. Quantitation of the PAHs was perfomed using the internal standard method.
Calculations for all these analyses were based on 1 mL original extract volume.
Analysis was performed on a Hewlett Packard 5890 Series II Gas Chromatograph (fitted with a Hewlett Packard
7673 automated injector), with programmable carrier gas pressure, the column of which was interfaced directly to
the source of a Hewlett Packard 5971 Mass Selective Detector. The column was a 60M x 0.25mm DB-5 column
(0.25 |j,m film). Injection volume was 1 |jL using splitless injection. The helium pressure was programmed to start
at 80 PSI for 1 minute then ramped at 99 PSI/min to 30 PSI then ramped at 5 PSI/min to 45 PSI and maintained at
that pressure for the remainder of the run. The oven temperature was held at 130°C for 2 min, ramped at 8 deg/min
A-6
-------
to 300°C then held for 30 minutes.
Daily performance checks met all criteria for mass calibration and tuning. Multilevel standards were run to establish
linearity and response factors obtained were checked for continuing calibration.
Average recovery for the labeled PAH internal standards was 82% (average sample ranged 63% to 90%). Detection
limits for PAHs were generally less than 50 pg/mL of original extract.
A.6 Air PCDD/PCDF Analyses
Air sampler XAD was spiked for PCDD/PCDF (13C-internal standard mix + M-23 13C-standard mix) and PCBs
(BZ-14, 65 and 166), extracted by Acurex and received at Wadsworth Labs on 10/5/95. Extracts were brought to 10
mL with toluene and spiked with 12.5 ng of 13C-1,2,3,4 TCDD as clean-up standard. A final cleaned-up extract of
75 |j,L in xylene which contained the PCDD/PCDF fraction was obtained which included 12.5 ng of an injection
standard of ^3C 1,2,3,7,8,9 HxCDD added during the final concentration step. The samples were cleaned up for
PCDD/PCDF analysis. Due to an oversight the PCB fraction from this clean-up was not retained and was lost to
waste. This required a request for an additional 250 |jL of the original extract held by Acurex for this type of
eventuality. The supplemental extract was cleaned-up in the same way but this time retaining the PCB fraction
which was analyzed by GC/EC using DEC method 91 -11 as specificed in the QATP. Calculations for all these
analyses were based on 1 mL original extract volume.
PCDD/PCDF analysis was performed on a Hewlett Packard 5890 Series II Gas Chromatograph (fitted with a
Hewlett Packard 7673 automated injector), with programmable carrier gas pressure, the column of which was
interfaced directly to the source of a Hewlett Packard 5971 Mass Selective Detector. The column was a 60M x
0.25mm DB-XLB column (0.25 |jm film). Injection volume was 2 |jL using splitless injection. The helium pressure
was programmed to start at 80 PSI for 1 minutes then ramped at 99 PSI/min to 30 PSI then ramped at 5 PSI/min to
45 PSI and maintained at that pressure for the remainder of the run. The oven temperature was held at 130°C for 1
min, ramped at 20 deg/min to 190°C then ramped at 5 deg/min to 240°C and held for 13.5 minutes, ramped at 10
deg/min to 290°C and held for 19.5 minutes.
Daily performance checks met all criteria for mass and retention time calibration and for the GC column
performance for 2,3,7,8- TCDD isomer resolution.
Table A-6 details the recoveries of the internal standards. It is expected that 40-60% recoveries would constitute
fully valid data, although trends may still be valid for lower recoveries. Most samples exhibited recoveries in the
40-120% range. However, for some of the avid recycler samples in particular, some congeners showed recoveries in
the 10-20% range. The numbers are still reported, though, with caveats.
A-7
-------
A.7 Air PCB Analyses
PCB analysis was performed on a Hewlett Packard 5890 Series II Gas Chromatograph (fitted with a Hewlett
Packard 7673 automated injector), with programmable carrier gas pressure, and electron capture detector. The
column was a 60M x 0.25mm DB-5 column (0. l|j, film). Injection volume was 2 |jL using splitless injection. The
helium carrier gas was programmed to a constant pressure of 19.5 PSI throughout the run. The oven temperature
was held at 90°C for 1 min, ramped at 25 deg/min to 150°C then held for 4 minutes before a final ramp at 1.5
deg/min to 290°C then held for 40 minutes. Total time before the next run was 140 minutes.
Calibration of the GC/EC was by means of a 3 point calibration. Response was checked using continuing calibration
which contains 120 PCB congeners each at lOng/ul concentration which was run during sample batches.
Recovery of the 3 PCB congeners through the extraction and clean-up was within QC limits of 40 140% (range 45-
115%). The 3,5-dichlorobiphenyl (BZ-14) showed a lower recovery in all the extracts which may be a result of the
higher vapor pressure and loss due to volatility during sample manipulations.
A.8 Air Acid Gas Analyses
Relatively little QA/QC was done for HC1 measurements. A five point calibration curve was run and found to be
linear and a laboratory blank was run and found to be clean. Data were not available to determine the value of this
DQO. For HCN measurements, a matrix spike of 10 |j,g/mL was analyzed in duplicate. The analyses resulted in a
measurement of 10.27351 and 10.58133, respectively.
A.9 Air Aldehyde and Ketone Analyses
For the determination of precision and accuracy of these analyses, the results from a EPA audit of Acurex ERO
laboratory prior to the time of the analyses of these samples. An additional blind audit was performed after these
samples were run. Both audits supported a +25 % accuracy and precision level.
A.10 Air Mercury Analyses Performed by Triangle Laboratories
Six 4% KMnO4/10% H2SO4 samples were analyzed for Hg; five of these samples were test samples and one was a
blank sample. For Hg analysis, the samples and associated QC samples were prepared and analyzed following the
guidelines of Method 101A (6/93). Hg concentrations were determined by cold vapor atomic absorption (CVAA).
All samples were non-detects. The samples were re-prepared using a larger aliquot and reanalyzed. The results of
the reanalyses were also non-detects. The original analysis was reported. The analytical data were considered valid
based on the guidelines of EPA Method 101 A.
A-8
-------
CO
Table A- 6. PCDD/PCDF Sample Recoveries (%)
Run
Avid Recy cler # 1
Avid Recycler #2
Hut Blank
Non-Recycler#l
Non-Recycler #2
2378
TCDD
8
12
33
80
59
12378
PCDD
7
11
32
72
53
123478
123678
123789
HXCDD HXCDD HXCDD
44
51
65
68
57
7
10
27
48
36
7
10
27
48
36
1234678
HPCDD
5
8
27
52
39
12346789
OCDD
5
8
27
52
39
2378
TCDF
5
10
29
75
53
12378
PCDF
9
12
36
79
58
23478
PCDF
44
52
59
66
55
123478
HXCDF
47
54
75
78
59
123678
HXCDF
7
10
28
48
37
234678
HXCDF
7
10
28
48
37
123789
HXCDF
7
10
28
48
37
1234678
HPCDF
6
9
27
54
4
1234789
HPCDF
37
46
58
51
42
12346789
OCDF
5
8
27
52
39
-------
A.11 Air Inorganic Analyses
Four filter samples, one hut blank filter and one filter blank were each cut into four quarters. One quarter from each
of the filters and the associated quality control (QC) were digested in a microwave oven using nitric acid. The
digestates were analyzed using ICP-MS for arsenic, barium, beryllium, cadmium, magnesium, copper, nickel, lead,
silver, and zinc. A portion of each digestate was analyzed for selenium using a graphite furnace. One quarter from
each filter was analyzed for mercury using cold vapor atomic absorption. One quarter from each filter was digested
in a microwave oven using nitric and hydrofluoric acids and analyzed for chromium and aluminum using an atomic
absorption spectrometer.
Three nitric acid wash samples, one hut blank and one reagent blank were concentrated and then digested in a
microwave oven. They were analyzed as above except for mercury which was not analyzed and hydrofluoric acid
was not used in the digestion procedure for chromium and aluminum.
Three hydrochloric acid rinse samples, one hut blank and one reagent blank were analyzed for mercury using cold
vapor atomic absorption.
All analytical procedures followed acceptable laboratory standards. A duplicate, spike and a Standard Reference
Material (SRM) (#1648 Urban Paniculate Matter) accompanied the samples from digestion through analysis with
the results within acceptable limits.
All samples, hut blanks, reagent and filter blanks were received on September 20, 1995 in good condition except for
one nitric acid wash which had no sample due to a broken cap.
A.12 Ash Semivolatile Organic Analyses
Separate initial calibrations were run for ash and air runs. Initial calibrations prior to ash analysis resulted in
%RSDs of less than 10% for most analytes, less than 25% for most others and greater than 25% for pyridine, N-
Nitrosodimethylamine, 3- or 4-methyl phenol, 2,4-dinitrophenol, 4-nitrophenol, pentachlorophenol, 4-
nitroquinoline-1-oxide and kepone.
EPA CLP surrogates were added to the ash samples and EPA CLP matrix spikes were added to sample 9582036
(Non Avid). Surrogate recoveries were within acceptance limits; matrix spike recoveries were good except for 25%
recovery of 2,4-dinitrotoluene in MS (low limit 28% for soil, 24% for water). Three RPDs were above acceptance
limits: 1,4-dichlorobenzene (39%, high limit 27%), 1,2,4-trichlorobenzene (34%, high limit 23%) and acenaphthene
(21%, high limit 19%).
Most of the non-target substances detected in the ash samples were either those also detected in the blank (Aldol
condensation products and di-lauryl-thio-di-propionate) or were hydrocarbons. An apparent modified form of the
A-10
-------
surrogate 2,4,6-tribromophenol was also detected in one sample; this was not in the corresponding blank but is
sometimes seen in blanks. The avid recycler sample 9582035 also contained substances tentatively identified as 6 -
9 carbon branched alkanes, alcohols, esters, aldehydes and ketones, 16 and 18 carbon possibly (l)-alkenes, benzoic
acid, hexdecanoic acid and a substance tentatively identified as 4,4'-butylidinebis[2-(l,l-dimethylethyl)-5-
methylphenol].
A.13 Ash PCDD/PCDF Analyses
Recovery of 10 ^C-internal standards through the cleanup averaged 50%. Injection standard recovery was 66-72%.
The matrix spike (MS 9582038) recovery for the 17 2,3,7,8 substituted PCDD/PCDF compounds (CU-8) was 92 to
143% and for the matrix spike duplicate (MSD 9582039) was 69 to 113% (except 1,2,3,4,6,7,8-HpCDF at 23%
probably due to large matrix concentration). The relative percent difference for the duplicates with the one
compound exception as noted above was less than 13% for the 16 remaining PCDD/PCDF compounds.
A.14 Ash PCB Analyses
Ash samples were spiked with a 200 |jL of a surrogate mix (tetrachloro-m-xylene [TCMX] and BZ 209)and with the
100 |jL of a 3 PCB congener mix which contained BZ-14, 65, and 166 prior to extraction and clean-up. Recoveries
ranged between 65 and 95%.
A.15 Ash Metal Analyses
A representative 2.0 g of ash samples were digested and refluxed in HNOs and/or HCI and H2O2. HCI was used as
the final reflux acid for Inductively Coupled Atomic Emission Spectrophotometry (ICP-AES) analyses of beryllium,
silver, barium, cadmium, chromium, copper, iron, manganese, nickel, strontium, titanium, vanadium, zinc, lead, tin,
aluminum, calcium, potassium, magnesium, and sodium using EPA method 200.7. HNOs was used as the complete
reflux acid for the Electrothermal Atomic Absorption Spectrophotometry (graphite furnace) analyses of arsenic,
selenium, antimony, and thallium using EPA method 206.2, 270.2, 204.2, and 279.2, respectively. Aqueous acid
digestates for mercury were analyzed using Cold Vapor Atomic Absorption and EPA method 101 A.
The solid Laboratory Control Sample (LCS 0287) was prepared by the UNLV Quality Assurance laboratory and
was distributed by ICF Technology, Inc. under contract to the EPA. The "True Value" concentrations were derived
from the results of an EPA multi-laboratory analysis of the solid material by Contract Laboratory Program
procedures. Calibration check standards were maintained at ±10% throughout the analysis. Spike recoveries were
good for all trace metals (within 75 - 125%) except for those metals where the spike amount was too low relative to
the endogenous concentration (aluminum, copper, iron, and zinc) or too low relative to the instrument's reporting
limit (silver). Reproducibility was acceptable for all trace metals except silver (23 vs. <8 mg/kg) and copper (3520
vs. 4520 or 26% RPD). Digestion QC sample (Soil Lot 214 from Environmental Resource Associates) was well
within the acceptable limits for all analytes.
A-11
-------
APPENDIX B. CONTINUOUS EMISSION MONITORING DATA
Barrel Burning Test No. 1 CEM Data
ET (MIN)
-20.08
-19.58
-19.08
-18.58
-18.08
-17.58
-17.08
-16.58
-16.08
-15.58
-15.08
-14.58
-14.08
-13.58
-13.08
-12.58
-12.08
-11.58
-11.08
-10.58
-10.08
-9.58
-9.08
-8.58
-8.08
-7.58
-7.08
-6.58
-6.08
-5.58
-5.08
-4.58
-4.08
-3.58
-3.08
-2.58
-2.08
-1.58
-1.08
-0.58
-0.08
0.42
0.92
1.42
1.92
2.42
2.92
3.42
3.92
4.42
4.92
5.42
5.92
6.42
6.92
7.42
7.92
8.42
8.92
9.42
9.92
10.42
10.92
11.42
11.92
12.42
12.92
13.42
13.92
14.42
CO(PPM) NOX(PPM) O2 (%)
1 0.3 21.5
2 0.2 23.5
2 0.4 24.2
0 0.3 23.1
1 0.3 20.1
0 : 0.2 ! 20.7
1 [ 0.3 j 21.1
2 i 0.3 i 21
-2 | 0.1 20.9
-1 | 0.4 20.9
2 : 0.4 21
2 i 0.3 20.8
2 i 0.2 19.9
2 \ 0.3 18.3
3 I 0.4 17.9
4 I 0.2 18.6
2 i 0.3 19.9
1 i 0.4 i 20.5
2 ; 0.2 i 20.9
2 i 0.3 i 21
1 i 0.2 i 20.9
2 0.2 21
2 0.3 21.1
1 i 0.3 i 21
1 i 0.3 I 21
1 [ 0.3 i 21
1 i 0.2 i 20.9
0 [ 0.4 ; 20.9
0 I 0.2 i 21
0 : 0.2 i 20.9
0 i 0.3 i 20.9
1 0.2 20.9
1 ! 0.3 I 20.9
-1 i 0.4 I 20.9
0 i 0.4 i 20.9
-1 ': 0.2 i 21
1 i 0.4 i 21
0 ; 0.4 i 21.1
0 ; 0.4 i 21
-1 \ 0.4 i 21
1 i 0.3 i 21.1
2 ! 0.2 I 21
2 ! 0.4 \ 20.9
1 i 0.4 I 21
2 [ 0.4 i 20.9
2 i 0.4 j 20.9
2 [ 0.4 20.9
2 I 0.5 i 21
4 I 0.6 i 21
5 i 0.7 i 21
4 0.4 21
8 0.8 I 20.9
11 i 0.8 I 20.9
11 i 0.8 i 21
8 _ 1 i 20.8
8 0.9 i 20.8
7 i 1.1 i 20.8
7 i 1.3 i 20.8
7 i 1 j 20.8
7 0.9 20.8
11 ! 0.8 i 20.9
12 ! 0.9 I 20.7
20 ': 0.7 i 20.9
32 I 0.4 i 20.8
39 • 0.6 i 20.9
39 ; 0.5 I 20.8
39 i 0.5 i 20.9
43 I 0.4 I 20.9
44 0.6 20.9
37 0.7 20.9
HC(PPM)
5
4
4
5
4
4
5
4
5
5
4
5
5
4
4
3
3
6
4
4
5
4
3
6
4
5
5
4
5
4
4
4
5
4
5
5
3
4
4
4
4
4
5
4
3
4
3
3
6
5
7
7
7
8
7
7
6
7
7
6
9
8
12
18
20
22
25
26
24
20
CO2 (%)
0.06
0.05
0.06
0.05
0.06
0.04
0.05
0.05
0.03
0.04
0.04
0.04
0.05
0.04
0.02
0.04
0.05
0.06
0.06
0.05
0.04
0.04
0.04
0.05
0.06
0.05
0.05
0.03
0.04
0.07
0.04
0.05
0.04
0.03
0.06
0.04
0.04
0.05
0.04
0.04
0.04
0.04
0.05
0.05
0.05
0.05
0.04
0.05
0.07
0.07
0.08
0.09
0.09
0.09
0.09
0.11
0.11
0.11
0.13
0.11
0.13
0.13
0.11
0.1
0.09
0.09
0.09
0.08
0.08
0.1
TEMPI (QTEMP2 (CJTEMP4 (C)TEMPS (CJTEMP6 (CJTEMP7 (C)TEMPS (C)
46 i 46 i 46 i 50.1
46 i 46 i 46 | 54.1
46 i 46 i 46 i 54.1
46 I 46 I 46 i 50.1
46 i 46 i 46 i 50.1
46 ! 46 i 46 54.1
46 i 46 i 46 54.1
46 i 46 j 46 50.1
46 46 46 50.1
46 50.1 46 54.1
46 46 46 54.1
46 46 46 50.1
50.1 46 50.1 50.1
46 46 46 50.1
46 46 50.1 50.1
50.1 50.1 46 50.1
50.1 50.1 50.1 54.1
50.1 i 46 i 50.1 ! 50.1
50.1 i 46 i 50.1 \ 50.1
50.1 I 50.1 i 50.1 I 54.1
50.1 i 46 i 50.1 | 54.1
50.1 i 50.1 i 50.1 | 54.1
50.1 I 46 I 50.1 i 54.1
50.1 I 46 I 50.1 I 54.1
50.1 I 50.1 I 50.1 i 54.1
50.1 ! 46 i 50.1 i 50.1
50.1 i 46 j 50.1 | 50.1
50.1 i 50.1 i 50.1 I 50.1
50.1 I 50.1 I 46 I 54.1
50.1 i 46 i 50.1 ! 54.1
50.1 i 50.1 i 50.1 I 50.1
50.1 i 50.1 i 50.1 i 50.1
50.1 I 46 I 50.1 I 50.1
50.1 I 50.1 I 50.1 : 50.1
50.1 ! 50.1 i 50.1 i 50.1
50.1 i 50.1 i 50.1 i 54.1
50.1 i 50.1 j 50.1 i 50.1
50.1 I 50.1 I 50.1 I 50.1
50.1 I 50.1 i 50.1 i 50.1
50.1 i 46 i 50.1 ! 50.1
50.1 i 50.1 i 50.1 | 50.1
50.1 I 50.1 I 50.1 i 50.1
50.1 \ 46 \ 50.1 i 50.1
54.1 I 50.1 I 50.1 i 54.1
54.1 ! 50.1 i 54.1 i 50.1
58.1 i 50.1 i 54.1 | 50.1
66.1 i 50.1 i 54.1 I 54.1
74.1 I 46 I 54.1 I 50.1
82.1 I 42 i 54.1 I 50.1
94.1 i 42 i 54.1 | 50.1
102.1 i 46 i 58.1 i 54.1
102.1 I 46 I 58.1 i 54.1
114.2 I 46 I 58.1 i 54.1
118.2 ! 46 i 58.1 i 54.1
130.2 ! 46 i 62.1 i 54.1
142.2 i 46 j 62.1 \ 54.1
150.2 I 46 I 62.1 I 54.1
154.2 I 46 I 62.1 i 54.1
154.2 i 46 i 62.1 i 54.1
154.2 i 46 i 66.1 i 54.1
150.2 i 46 i 66.1 i 54.1
138.2 I 46 I 66.1 I 54.1
126.2 I 50.1 I 66.1 I 54.1
118.2 ! 50.1 i 66.1 i 54.1
114.2 i 50.1 i 66.1 | 54.1
110.2 i 50.1 i 66.1 I 54.1
106.1 i 50.1 i 66.1 ! 54.1
106.1 I 50.1 i 66.1 I 54.1
110.2 50.1 66.1 54.1
126.2 54.1 66.1 54.1
46 i 50.1 i 46
46 i 50.1 i 46
46 i 50.1 i 46
46 I 50.1 I 46
46 I 50.1 I 46
46 ! 50.1 i 46
46 | 50.1 i 46
46 i 50.1 j 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 i 54.1 j 46
46 I 54.1 I 46
46 I 54.1 i 46
46 i 54.1 i 46
46 i 54.1 i 46
50.1 I 54.1 I 46
46 I 54.1 I 46
50.1 I 54.1 I 46
46 | 54.1 i 46
46 i 54.1 j 46
46 i 54.1 j 46
50.1 I 54.1 I 46
50.1 i 54.1 i 46
46 ': 54.1 ': 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 54.1 46
46 I 54.1 i 46
46 i 54.1 i 46
50.1 i 54.1 i 50.1
50.1 I 54.1 I 58.1
50.1 ! 54.1 ! 74.1
54.1 I 54.1 I 70.1
54.1 i 54.1 i 70.1
54.1 | 54.1 i 70.1
54.1 i 54.1 i 70.1
54.1 I 54.1 I 74.1
58.1 I 54.1 i 78.1
58.1 i 54.1 i 90.1
58.1 i 54.1 i 94.1
62.1 I 54.1 I 94.1
62.1 I 54.1 I 102.1
62.1 ! 54.1 i 106.1
62.1 | 54.1 i 114.2
661 i 54.1 j 126.2
66.1 I 54.1 I 130.2
661 I 54.1 I 130.2
66.1 i 54.1 i 130.2
70.1 i 54.1 i 130.2
70.1 i 54.1 i 126.2
70.1 I 54.1 I 118.2
70.1 I 54.1 I 110.2
70.1 ! 54.1 i 98.1
70.1 | 54.1 i 98.1
70.1 i 54.1 j 94.1
66.1 I 54.1 I 90.1
70.1 I 54.1 i 94.1
70.1 i 54.1 102.1
70.1 i 54.1 118.2
TEMP9 (C)*eight (LB
42 \ 27.6
42 ! 27.8
42 i 27.8
42 i 27.8
38 I 27.8
42 | 27.8
42 i 27.8
42 i 27.8
42 27.8
42 27.8
42 27.8
42 27.8
42 27.8
42 27.6
46 27.8
46 27.8
46 27.8
46 ! 27.6
46 \ 27.6
46 I 27.8
42 ! 27.6
42 i 27.6
50.1 i 27.8
46 I 27.8
42 i 27.8
46 i 27.6
46 | 27.8
42 I 27. &
46 I 27.8
46 ! 27.8
46 I 27.6
46 27.6
46 27.8
46 27.6
42 27.8
46 27.8
46 27.6
46 27.8
46 i 27.8
46 ! 27.6
46 i 27.4
46 i 27.4
46 i 27.6
46 i 27.4
46 i 27.4
46 | 27.4
42 I 27.2
42 I 26.8
42 I 26.8
42 ! 26.6
42 i 26.2
42 i 26.2
42 i 26
42 i 25.6
42 i 25.4
42 i 25.2
42 I 24. 8
42 i 24.6
42 ! 24.4
42 i 24
42 i 23.8
42 I 23.6
38 I 23.4
42 i 23.2
42 | 22.8
42 I 22.6
42 ! 22.6
46 I 22.2
46 22
42 21.6
B-1
-------
Barrel Burning Test No. 1 CEM Data
ET (MIN)
14.92
15.42
15.92
16.42
16.92
17.42
17.92
18.42
18.92
19.42
19.92
20.42
20.92
21.42
21.92
22.42
22.92
23.42
23.92
24.42
24.92
25.42
25.92
26.42
26.92
27.42
27.92
28.42
28.92
29.42
29.92
30.42
30.92
31.42
31.92
32.42
32.92
33.42
33.92
34.42
34.92
35.42
35.92
36.42
36.92
37.42
37.92
38.42
38.92
39.42
39.92
40.42
40.92
41.42
41.92
42.42
42.92
43.42
43.92
44.42
44.92
45.42
45.92
46.42
46.92
47.42
47.92
48.42
48.92
49.42
CO (PPM)
31
27
24
19
21
17
15
14
17
16
17
21
25
26
22
24
22
21
20
14
14
13
9
12
10
9
10
10
10
10
11
11
10
11
9
9
8
9
8
9
8
8
7
7
5
6
7
7
8
9
9
7
7
7
7
7
6
6
6
6
7
6
4
7
4
7
5
4
5
4
NOX (PPM)
0.8
0.7
1
0.8
0.7
0.8
0.9
0.9
0.9
0.9
0.9
1
0.9
0.7
0.9
0.8
1
0.9
0.7
0.6
0.8
0.7
0.6
0.4
0.8
0.6
0.7
0.6
0.6
0.6
0.6
0.6
0.7
0.4
0.5
0.4
0.6
0.4
0.6
0.4
0.4
0.7
0.3
0.4
0.6
0.5
0.5
0.4
0.6
0.4
0.4
0.4
0.6
0.5
0.4
0.2
0.5
0.3
0.5
0.3
0.5
0.4
0.3
0.4
0.3
0.4
0.4
0.4
0.4
0.4
02 (%)
21.1
20.9
20.8
20.8
20.7
20.7
20.7
20.8
20.9
20.8
20.7
20.7
20.9
20.8
20.8
20.8
20.7
20.8
20.8
20.8
20.7
20.8
20.9
21
20.8
20.8
20.8
20.9
20.9
21
21
21.1
21.1
21.1
21.1
21
21
21
21.1
21.2
21.2
21
21
21
21
20.9
20.8
20.7
20.8
20.8
20.8
20.8
20.9
21.1
21
21
21
21
20.9
21
21.1
21
20.9
21.1
20.9
21
20.9
21
21
20.9
HC (PPM)
17
16
13
13
14
10
10
10
9
8
11
12
13
11
10
11
13
11
10
10
9
8
8
9
8
8
8
10
8
7
8
8
8
9
7
9
7
10
8
10
8
7
7
9
7
8
8
7
7
9
9
9
6
7
7
7
7
6
7
8
6
7
7
5
8
7
9
7
7
7
C02 (%)
0.09
0.11
0.11
0.12
0.13
0.13
0.15
0.16
0.15
0.15
0.15
0.15
0.17
0.13
0.14
0.16
0.15
0.16
0.17
0.12
0.09
0.11
0.09
0.12
0.07
0.07
0.09
0.09
0.08
0.07
0.08
0.08
0.07
0.07
0.07
0.08
0.07
0.07
0.07
0.07
0.06
0.06
0.05
0.04
0.04
0.04
0.04
0.04
0.04
0.04
0.06
0.05
0.05
0.07
0.04
0.04
0.04
0.03
0.04
0.06
0.04
0.07
0.03
0.04
0.06
0.05
0.05
0.04
0.03
0.04
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (C)TEMP8 (C)
142.2 54.1 66.1 58.1 70.1 54.1 134.2
158.2 54.1 70.1 58.1 74.1 54.1 154.2
166.2 54.1 70.1 66.1 74.1 54.1 154.2
170.3 54.1 74.1 66.1 78.1 54.1 166.2
174.3 54.1 74.1 74.1 78.1 54.1 174.3
174.3 54.1 74.1 90.1 78.1 54.1 198.3
178.3 58.1 74.1 114.2 78.1 54.1 198.3
186.3 58.1 74.1 130.2 78.1 54.1 218.3
186.3 58.1 74.1 138.2 82.1 54.1 230.4
190.3 58.1 78.1 146.2 82.1 54.1 246.4
194.3 58.1 78.1 158.2 82.1 54.1 246.4
194.3 62.1 78.1 154.2 82.1 54.1 262.4
198.3 62.1 78.1 162.2 86.1 54.1 266.4
198.3 62.1 82.1 162.2 86.1 54.1 258.4
206.3 62.1 82.1 166.2 86.1 54.1 254.4
214.3 62.1 82.1 170.3 90.1 54.1 250.4
218.3 62.1 86.1 174.3 90.1 54.1 258.4
214.3 62.1 86.1 174.3 90.1 54.1 270.4
198.3 62.1 86.1 178.3 90.1 50.1 274.4
194.3 66.1 90.1 182.3 90.1 54.1 274.4
190.3 66.1 90.1 182.3 94.1 54.1 262.4
182.3 66.1 90.1 186.3 94.1 54.1 238.4
182.3 66.1 90.1 190.3 94.1 54.1 234.4
174.3 66.1 90.1 190.3 98.1 54.1 230.4
174.3 66.1 90.1 194.3 94.1 54.1 242.4
170.3 66.1 90.1 198.3 94.1 54.1 230.4
166.2 66.1 90.1 202.3 98.1 54.1 230.4
162.2 70.1 90.1 206.3 98.1 54.1 226.3
162.2 66.1 90.1 210.3 98.1 54.1 226.3
154.2 70.1 90.1 214.3 98.1 54.1 214.3
150.2 70.1 90.1 214.3 94.1 54.1 206.3
146.2 70.1 86.1 222.3 98.1 54.1 202.3
146.2 70.1 90.1 226.3 98.1 54.1 194.3
138.2 70.1 86.1 230.4 82.1 54.1 182.3
134.2 70.1 86.1 234.4 62.1 54.1 178.3
130.2 70.1 86.1 242.4 62.1 54.1 162.2
126.2 70.1 86.1 242.4 62.1 54.1 162.2
122.2 70.1 86.1 250.4 62.1 54.1 162.2
118.2 70.1 86.1 254.4 62.1 54.1 150.2
114.2 70.1 86.1 258.4 62.1 54.1 142.2
110.2 70.1 82.1 262.4 62.1 54.1 142.2
106.1 70.1 82.1 266.4 62.1 54.1 138.2
102.1 70.1 82.1 274.4 58.1 54.1 126.2
98.1 66.1 82.1 278.4 58.1 54.1 122.2
94.1 70.1 82.1 286.4 58.1 54.1 118.2
94.1 70.1 82.1 290.4 58.1 54.1 114.2
90.1 66.1 78.1 298.5 58.1 54.1 114.2
90.1 66.1 78.1 302.5 58.1 54.1 110.2
86.1 66.1 78.1 310.5 58.1 54.1 110.2
86.1 66.1 78.1 318.5 58.1 54.1 114.2
86.1 66.1 78.1 322.5 58.1 54.1 110.2
86.1 66.1 78.1 330.5 58.1 54.1 114.2
82.1 66.1 74.1 334.5 58.1 54.1 110.2
82.1 66.1 74.1 342.5 58.1 54.1 110.2
82.1 66.1 74.1 350.5 58.1 54.1 114.2
82.1 62.1 74.1 354.6 58.1 54.1 118.2
78.1 66.1 74.1 362.6 58.1 54.1 114.2
78.1 62.1 74.1 366.6 58.1 54.1 114.2
82.1 62.1 74.1 374.6 58.1 54.1 114.2
78.1 66.1 74.1 382.6 58.1 54.1 114.2
78.1 62.1 74.1 386.6 58.1 54.1 114.2
78.1 62.1 74.1 394.6 58.1 54.1 110.2
78.1 62.1 74.1 398.6 58.1 54.1 110.2
78.1 62.1 74.1 402.6 58.1 54.1 110.2
78.1 62.1 74.1 410.6 58.1 54.1 106.1
78.1 62.1 74.1 414.7 58.1 54.1 106.1
74.1 62.1 70.1 418.7 58.1 54.1 102.1
74.1 62.1 70.1 422.7 58.1 54.1 98.1
74.1 62.1 70.1 426.7 58.1 54.1 90.1
70.1 62.1 70.1 426.7 58.1 54.1 90.1
TEMP9 (C)weiqht (LB)
42 21.2
42 20.8
42 20.2
42 19.8
46 19.4
42 19.2
42 19.4
46 19
42 18.6
42 18.2
42 18
42 17.6
46 17.2
42 16.6
42 16.4
42 16.2
46 16
46 15.6
46 15.4
46 15.2
46 14.8
46 14.6
46 14.4
46 14.2
46 14
42 13.6
46 13.4
46 13.4
46 13
46 12.8
46 12.8
46 12.4
46 12.4
46 12.2
46 12.2
46 12
46 12
46 11.8
46 11.6
46 11.6
46 11.4
46 11.4
46 11.2
42 11.2
42 11.2
46 11
42 11
46 10.8
46 10.6
46 10.6
46 10.4
42 10.2
42 10.2
46 10
46 9.8
46 9.8
42 9.6
42 9.6
42 9.6
46 9.4
42 9.4
42 9.4
42 9.4
42 9.4
46 9.4
46 9.4
42 9.4
46 9.4
46 9.4
42 9.4
B-2
-------
Barrel Burning Test No. 1 CEM Data
ET (MIN)
49.92
50.42
50.92
51.42
51.92
52.42
52.92
53.42
53.92
54.42
54.92
55.42
55.92
56.42
56.92
57.42
57.92
58.42
58.92
59.42
59.92
60.42
60.92
61.42
61.92
62.42
62.92
63.42
63.92
64.42
64.92
65.42
65.92
66.42
66.92
67.42
67.92
68.42
68.92
69.42
69.92
70.42
70.92
71.42
71.92
72.42
72.92
73.42
73.92
74.42
74.92
75.42
75.92
76.42
76.92
77.42
77.92
78.42
78.92
CO (PPM)
7
7
6
7
6
9
8
9
7
9
8
6
5
7
6
6
8
5
4
4
7
8
10
8
5
6
6
7
5
2
6
6
7
6
5
4
6
7
6
5
6
5
6
7
6
7
5
5
6
5
3
7
5
6
6
5
2
5
18
NOX (PPM)
0.3
0.5
0.5
0.5
0.4
0.4
0.4
0.3
0.3
0.5
0.5
0.3
0.3
0.2
0.4
0.4
0.3
0.3
0.4
0.3
0.3
0.4
0.4
0.4
0.4
0.3
0.5
0.2
0.4
0.4
0.4
0.5
0.3
0.3
0.2
0.5
0.4
0.4
0.3
0.4
0.4
0.5
0.4
0.5
0.4
0.4
0.2
0.4
0.4
0.4
0.2
0.2
0.4
0.4
0.3
0.4
0.3
0.2
0.4
02 (%)
21
21.1
20.9
21
21
21.1
21.1
21
20.9
20.9
21
21.1
20.9
21.1
21
21
21.1
21
20.9
21
21.1
21.1
21.1
21
21
20.9
21.1
21.1
21
20.9
21
21.1
21.1
21
20.9
21
21.1
21.2
21.1
21
20.9
20.9
20.9
21.1
21.1
21.1
21
20.9
21.1
21.1
21
21.2
21
21
21.1
21
21
21
19.2
HC (PPM)
8
9
6
7
7
9
8
7
8
9
9
8
7
8
7
8
7
7
8
8
5
7
6
7
7
7
6
8
6
6
6
5
5
6
6
5
7
6
5
4
4
4
6
5
6
5
6
6
6
5
4
7
4
4
4
4
4
5
5
C02 (%)
0.05
0.03
0.03
0.04
0.04
0.05
0.04
0.03
0.03
0.06
0.07
0.04
0.04
0.03
0.04
0.04
0.04
0.02
0.03
0.03
0.03
0.03
0.04
0.04
0.03
0.04
0.03
0.04
0.03
0.03
0.03
0.03
0.03
0.02
0.04
0.02
0.04
0.04
0.04
0.02
0.02
0.02
0.04
0.04
0.02
0.04
0.04
0.02
0.03
0.03
0.02
0.04
0.02
0.02
0.02
0.02
0.04
0.03
0.02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (C)TEMP8 (C)
70.1 62.1 70.1 430.7 58.1 54.1 90.1
70.1 62.1 70.1 430.7 58.1 54.1 90.1
66.1 62.1 70.1 434.7 58.1 54.1 90.1
66.1 62.1 70.1 434.7 54.1 54.1 86.1
66.1 62.1 66.1 434.7 54.1 54.1 82.1
66.1 58.1 70.1 434.7 58.1 54.1 82.1
66.1 58.1 66.1 438.7 58.1 54.1 82.1
66.1 58.1 66.1 438.7 58.1 54.1 82.1
66.1 58.1 66.1 438.7 58.1 54.1 82.1
66.1 58.1 66.1 438.7 54.1 54.1 78.1
66.1 58.1 66.1 434.7 54.1 54.1 78.1
66.1 58.1 66.1 438.7 54.1 54.1 78.1
62.1 58.1 66.1 438.7 54.1 54.1 74.1
66.1 58.1 66.1 438.7 54.1 54.1 74.1
62.1 58.1 66.1 438.7 54.1 54.1 70.1
62.1 58.1 66.1 438.7 54.1 54.1 70.1
62.1 58.1 66.1 434.7 54.1 54.1 66.1
62.1 58.1 62.1 434.7 54.1 54.1 66.1
62.1 58.1 62.1 434.7 54.1 54.1 66.1
62.1 58.1 62.1 430.7 54.1 54.1 62.1
62.1 58.1 62.1 430.7 54.1 50.1 66.1
58.1 54.1 62.1 430.7 54.1 54.1 62.1
58.1 54.1 62.1 430.7 54.1 50.1 58.1
58.1 54.1 62.1 426.7 54.1 54.1 58.1
58.1 54.1 62.1 426.7 54.1 54.1 58.1
58.1 54.1 62.1 426.7 54.1 54.1 58.1
58.1 54.1 58.1 422.7 54.1 50.1 58.1
58.1 54.1 62.1 422.7 54.1 54.1 58.1
58.1 54.1 62.1 418.7 54.1 54.1 58.1
58.1 54.1 62.1 418.7 54.1 54.1 62.1
58.1 54.1 58.1 418.7 54.1 54.1 58.1
58.1 54.1 58.1 414.7 54.1 50.1 58.1
58.1 54.1 58.1 414.7 54.1 50.1 58.1
58.1 54.1 58.1 410.6 54.1 54.1 58.1
58.1 54.1 58.1 410.6 54.1 54.1 58.1
58.1 54.1 62.1 410.6 54.1 54.1 58.1
58.1 54.1 58.1 410.6 54.1 54.1 58.1
58.1 54.1 58.1 410.6 54.1 54.1 58.1
54.1 54.1 58.1 406.6 54.1 54.1 58.1
58.1 50.1 58.1 406.6 58.1 54.1 58.1
58.1 54.1 58.1 402.6 54.1 54.1 58.1
58.1 54.1 58.1 402.6 54.1 54.1 58.1
58.1 54.1 58.1 402.6 54.1 54.1 58.1
58.1 54.1 58.1 398.6 54.1 54.1 58.1
54.1 54.1 58.1 402.6 54.1 54.1 54.1
54.1 54.1 58.1 402.6 54.1 54.1 54.1
54.1 54.1 58.1 398.6 58.1 54.1 54.1
54.1 54.1 58.1 394.6 54.1 54.1 54.1
54.1 46 58.1 394.6 54.1 54.1 54.1
54.1 54.1 58.1 394.6 54.1 54.1 54.1
54.1 50.1 58.1 394.6 54.1 54.1 58.1
58.1 54.1 58.1 390.6 54.1 54.1 58.1
58.1 54.1 58.1 394.6 54.1 54.1 54.1
54.1 54.1 58.1 390.6 54.1 54.1 54.1
54.1 54.1 58.1 390.6 54.1 54.1 58.1
54.1 54.1 58.1 390.6 58.1 54.1 54.1
54.1 54.1 58.1 390.6 54.1 54.1 54.1
58.1 54.1 58.1 390.6 54.1 54.1 54.1
54.1 54.1 58.1 386.6 54.1 54.1 54.1
TEMP9 (C)weiqht (LB)
42 9.4
42 9.4
42 9.6
42 9.6
42 9.6
42 9.6
42 9.8
42 9.6
42 9.8
42 9.8
46 9.8
42 9.8
42 9.8
42 9.8
42 9.8
42 9.8
42 9.8
42 9.8
42 9.8
46 9.8
42 10
42 9.8
42 9.8
42 9.8
42 9.8
46 9.6
46 9.8
42 9.8
42 9.6
42 9.8
42 9.6
42 9.4
50.1 9.8
42 9.8
46 9.6
46 9.6
46 9.6
42 9.4
42 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.6
46 9.4
46 9.4
46 9.4
46 9.6
46 9.6
46 9.4
46 9.6
46 9.2
B-3
-------
Barrel Burning Test No. 2 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM) | C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMPS (CJTEMP7 (C)|rEMP8 (C)h"emp9 (C)| weight (IB
-19.92
-19.42
-18.92
-18.42
-17.92
-17.42
-16.92
-16.42
-15.92
-15.42
-14.92
-14.42
-13.92
-13.42
-12.92
-12.42
-11.92
-11 .42
-10.92
-10.42
-9.92
-9.42
-8.92
-8.42
-7.92
-7.42
-6.92
-6.42
-5.92
-5.42
-4.92
-4.42
-3.92
-3.42
-2.92
-2.42
-1.92
-1.42
-0.92
-0.42
0.08
0.58
1.08
1.58
2.08
2.58
3.08
3.58
4.08
4.58
5.08
5.58
6.08
6.58
7.08
7.58
8.08
8.58
9.08
9.58
10.08
10.58
11.08
11.58
12.08
12.58
13.08
13.58
14.08
14.58
0
1
1
-1
-1
1
-1
1
0
0
2
-1
0
-2
0
1
-2
0
0
0
-1
0
-1
0
1
2
0
1
0
2
-1
0
2
0
1
1
0
0
1
1
0
-1
0
0
1
2
5
8
2
5
4
6
4
3
7
10
12
20
20
20
22
22
20
20
26
23
22
21
17
16
0.4
0.5
0.3
0.5
0.5
0.4
0.6
0.3
0
0.2
0
0.1
0
0
-0.1
-0.1
-0.1
0
0
0
0
-0.1
0
0.1
0
0.1
0
0
0.2
0.1
0.1
-0.1
-0.1
0
0.1
0
0
0
0.2
0
0.2
0
0.1
0.2
0.2
0.4
0.7
1.2
0.9
0.7
0.9
0.9
0.8
0.8
0.7
0.7
0.8
0.6
0.7
0.7
0.4
0.6
0.5
0.4
0.7
0.6
0.7
0.6
0.7
0.7
21.3
21.3
21.3
21
20.9
21
21
20.9
20.9
20.9
20.9
20.8
20.9
20.8
20.9
20.8
20.8
20.9
20.8
20.8
20.9
20.8
21
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.8
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.8
20.9
20.9
20.8
20.9
20.9
20.8
21
20.7
20.8
20.6
20.7
20.7
20.5
20.7
20.8
20.8
20.8
20.7
20.6
20.8
20.7
20.7
20.9
20.9
20.9
20.8
20.8
20.9
20.9
20.9
20.8
3
2
5
5
4
4
4
4
5
4
5
5
3
5
4
5
3
3
5
5
4
4
5
4
5
5
5
5
4
3
4
4
5
6
5
4
3
4
4
5
4
6
3
4
4
6
7
5
5
6
5
4
7
7
7
10
15
14
13
17.
15
11
11
16
14
14
13.
10
10
10
0.03
0.02
0.04
0.03
0.03
0.03
0.04
0.01
0.03
0.02
0.03
0.02
0.03
0.02
0.03
0.03
0.01
0.02
0.02
0.04
0.02
0.02
0.03
0.01
0.02
0.02
0.02
0.02
0
0.03
0.02
0.01
0.02
0.03
0.02
0.04
0.02
0.02
0.02
0.02
0.02
0.02
0.01
0.03
0.02
0.04
0.04
0.04
0.05
0.07
0.08
0.08
0.08
0.07
0.09
0.09
0.08
0.08
0.09
0.08
0.09
0.08
0.08
0.09
0.08
0.07
0.09
0.09
0.1
0.09
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
50.1
50.1
58.1
74.1
102.1
134.2
154.2
166.2
170.3
162.2
158.2
162.2
158.2
150.2
146.2
146.2
146.2
146.2
150.2
150.2
150.2
146.2
158.2
162.2
170.3
174.3
178.3
178.3
178.3
50.1
50.1
46
50.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
50.1
50.1
46
46
46
46
46
46
46
50.1
46
46
46
46
46
50.1
46
50.1
46
46
46
50.1
46
46
46
46
46
46
50.1
42.
42
42.
42
46
42
42
46
46.
46
46
46
46.
50.1
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
B-4
22
26
22
6
6
18
18
10
2
6
6
6
18
18
6
18
18
10
18
2
2
6
6
2
2
14
14
22
22
22
22
22
2
14
14
26
26
22
22
18
2
2
22
10
10
10
10
14
14.
18
10
2
2
6
10
14.
6
18
46
14
46.
54.1
46
50.1
46
46.
54.1
54.1
54.1
62.1
46.
46.
46
46
50.1
50.1
46.
46.
50.1
50.1
50.1
46.
50.1
50.1
50.1
46
50.1
50.1
46.
46.
50.1
50.1
50.1
50.1
50.1
46.
50.1
50.1
46
46.
50.1
46.
50.1
50.1
50.1
50.1
46.
46
50.1
46
46
46.
50.1
50.1
46
50.1
46
50.1
50.1
50.1
46
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
54.1
50.1
54.1
50.1
54.1
50.1
54.1
50.1
54.1
50.1
54.1
50.1
50.1
50.1
54.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
50.1
54.1
50.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
46
46
46
46
46
42
46
42
46
42
42
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
46
50.1
54.1
62.1
102.1
190.3
222.3
214.3
226.3
206.3
202.3
206.3
198.3
194.3
206.3
198.3
230.4
250.4
234.4
226.3
214.3
206.3
230.4
226.3
238.4
250.4
246.4
246.4
242.4
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
30
30.2
29.8
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
29.8
30
30
30
30
30
29.8
30
29.8
30
30
30
30
29.8
30
30
30
30
29.8
29.8
30
30
29.6
29.4
29.2
29
28.6
28.2
28
27.8
27.2
27
26.6
26.4
26.2
25.8
25.6
25.2
25
24.6
24.2
24.2
23.6
23.4
22.8
22.6
22
21.8
21.2
-------
Barrel Burning Test No. 2 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM)
C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMPS (CJTEMP7 (C)|rEMP8 (C)h"emp9 (C)| weight (IB
15.08
15.58
16.08
16.58
17.08
17.58
18.08
18.58
19.08
19.58
20.08
20.58
21.08
21.58
22.08
22.58
23.08
23.58
24.08
24.58
25.08
25.58
26.08
26.58
27.08
27.58
28.08
28.58
29.08
29.58
30.08
30.58
31.08
31.58
32.08
32.58
33.08
33.58
34.08
34.58
35.08
35.58
36.08
36.58
37.08
37.58
38.08
38.58
39.08
39.58
40.08
40.58
41.08
41.58
42.08
42.58
43.08
43.58
44.08
44.58
45.08
45.58
46.08
46.58
47.08
47.58
48.08
48.58
49.08
49.58
18
16
16
13
11
10
7
10
11
11
9
7
9
10
9
10
10
8
9
9
10
13
10
9
9
9
12
9
10
10
9
10
9
8
7
9
9
8
7
7
7
7
6
5
6
6
5
5
6
8
6
9
9
9
4
7
6
9
8
6
7
4
4
3
5
5
4
0
3
2
0.7
0.6
0.8
0.7
0.7
0.8
0.8
0.9
0.8
0.8
0.7
0.7
0.8
0.6
0.8
0.7
0.9
0.7
0.6
0.6
0.4
0.6
0.4
0.5
0.5
0.4
0.3
0.3
0.3
0.5
0.4
0.5
0.4
0.4
0.4
0.4
0.4
0.4
0.5
0.4
0.5
0.5
0.5
0.3
0.3
0.3
0.2
0.3
0.2
0.3
0.4
0.2
0.2
0.1
0.4
0.3
0.1
0.3
0.1
0.2
0.2
0.4
0.2
0.3
0.3
0.1
0.2
0.2
0.4
0.2
20.7
20.7
20.7
20.7
20.8
20.7
20.6
20.6
20.7
20.8
20.7
20.6
20.8
20.8
20.7
20.7
20.8
20.7
20.8
20.8
20.7
20.8
20.9
20.8
20.7
20.7
20.8
20.8
20.8
20.8
20.8
20.9
20.8
20.9
20.9
20.9
20.9
20.8
20.8
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.9
21
20.9
21
20.8
21
20.9
21
21
21
20.9
20.9
21
20.9
21
21
21
21
21
20.9
21
21.1
10
0.09
0.08
0.08
0.08
0.09
0.11
0.08
0.1
0.09
0.11
0.1
0.11
0.09
0.11
0.07
0.09
0.1
0.08
0.08
0.07
0.09
0.09
0.08
0.08
0.07
0.06
0.07
0.05
0.06
0.04
0.05
0.06
0.05
0.06
0.05
0.04
0.04
0.04
0.04
0.04
0.04
0.04
0.04
0.04
0.03
0.02
0.02
0.04
0.05
0.04
0.02
0.02
0.04
0.04
0.02
0.04
0.04
0.04
0.01
0.02
0.03
0.02
0.02
0.02
0.04
0.02
0
0.02
0.02
0.03
174.3
178.3
186.3
190.3
194.3
194.3
198.3
202.3
206.3
198.3
190.3
190.3
194.3
198.3
202.3
202.3
202.3
198.3
194.3
190.3
186.3
182.3
182.3
178.3
174.3
174.3
170.3
170.3
166.2
166.2
166.2
162.2
162.2
158.2
154.2
154.2
150.2
150.2
146.2
146.2
142.2
142.2
138.2
138.2
134.2
130.2
130.2
126.2
126.2
122.2
118.2
114.2
114.2
110.2
106.1
106.1
102.1
98.1
94.1
94.1
90.1
86.1
86.1
82.1
82.1
78.1
78.1
78.1
74.1
74.1
54.1
54.1
54.1
58.1
58.1
54.1
58.1
58.1
58.1
62.1
58.1
58.1
62.1
62.1
62.1
62.1
62.1
62.1
66.1
62.1
62.1
66.1
70.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
70.1
70.1
70.1
66.1
70.1
66.1
70.1
66.1
70.1
66.1
-38.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
62.1
66.1
66.1
66.1
62.1
66.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
58.1
B-5
62.1
50.1
42
62.1
66.1
38
30
34
58.1
82.1
58.1
46
78.1
78.1
50.1
86.1
82.1
66.1
102.1
78.1
90.1
118.2
114.2
94.1
90.1
98.1
122.2
130.2
134.2
134.2
150.2
166.2
150.2
154.2
162.2
166.2
166.2
162.2
162.2
166.2
174.3
174.3
170.3
178.3
194.3
186.3
178.3
170.3
182.3
194.3
166.2
190.3
162.2
198.3
154.2
190.3
194.3
190.3
186.3
178.3
166.2
150.2
146.2
150.2
162.2
174.3
162.2
142.2
142.2
162.2
50.1
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
58.1
58.1
62.1
62.1
66.1
70.1
70.1
74.1
78.1
82.1
90.1
94.1
98.1
106.1
114.2
114.2
118.2
118.2
118.2
122.2
122.2
126.2
126.2
130.2
130.2
134.2
134.2
138.2
142.2
142.2
142.2
146.2
150.2
150.2
154.2
154.2
158.2
158.2
162.2
162.2
162.2
166.2
170.3
170.3
174.3
174.3
178.3
178.3
182.3
182.3
186.3
186.3
190.3
190.3
194.3
194.3
194.3
198.3
198.3
202.3
206.3
54.1
54.1
54.1
54.1
54.1
58.1
54.1
54.1
54.1
54.1
58.1
54.1
54.1
58.1
58.1
58.1
58.1
58.1
58.1
54.1
58.1
54.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
54.1
54.1
58.1
58.1
58.1
54.1
58.1
54.1
54.1
58.1
54.1
54.1
58.1
54.1
54.1
58.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
50.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
250.4
302.5
322.5
334.5
346.5
358.6
402.6
402.6
414.7
422.7
418.7
438.7
442.7
446.7
514.8
506.8
486.8
450.7
434.7
406.6
410.6
402.6
406.6
378.6
378.6
366.6
334.5
342.5
346.5
358.6
342.5
330.5
322.5
290.4
298.5
290.4
278.4
278.4
274.4
266.4
246.4
230.4
238.4
222.3
218.3
218.3
210.3
194.3
190.3
178.3
186.3
194.3
182.3
178.3
178.3
162.2
166.2
154.2
146.2
146.2
150.2
146.2
150.2
142.2
146.2
154.2
150.2
142.2
142.2
142.2
42
42
42
42
42
42
42
42
42
42
46
42
46
46
46
46
42
46
46
46
46
46
46
46
46
42
46
46
46
46
46
46
46
46
46
42
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
42
46
46
42
42
42
46
46
46
46
46
46
46
46
42
46
46
42
46
21
20.6
20.2
19.6
19.2
18.8
18.2
17.8
17.4
16.8
16.8
16.4
16.2
16
15.8
15.4
15
14.6
14.6
14.6
14.4
14
13.8
13.6
13.4
13.2
13
13
12.8
12.6
12.6
12.2
12.2
12.2
12
11.6
11.6
11.6
11.4
11.2
11.2
11.2
11
11
11
11
10.8
10.8
10.8
10.6
10.6
10.6
10.4
10.4
10.4
10.4
10.4
10.4
10.4
10.4
10.4
10.4
10.4
10.2
10
10.2
10.2
10.2
10.2
10.2
-------
Barrel Burning Test No. 2 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM)
C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMPS (CJTEMP7 (C)|rEMP8 (C)h"emp9 (C)| weight (IB
50.08
50.58
51.08
51.58
52.08
52.58
53.08
53.58
54.08
54.58
55.08
55.58
56.08
56.58
57.08
57.58
58.08
58.58
59.08
59.58
60.08
60.58
61.08
61.58
62.08
62.58
63.08
63.58
64.08
64.58
65.08
65.58
66.08
66.58
67.08
67.58
68.08
68.58
69.08
69.58
70.08
70.58
71.08
71.58
72.08
72.58
73.08
73.58
74.08
74.58
75.08
75.58
76.08
76.58
77.08
77.58
78.08
78.58
79.08
79.58
0.2
0.2
0.1
0.1
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0
0.2
0.1
0.3
0.2
0.2
0.1
0.2
0.2
0.2
0.3
0.1
0.2
0.2
0.2
0.2
0.2
0.3
0.2
0.2
0.2
0.2
0.1
0.1
0.3
0.1
0.2
0.2
0.2
0.2
0.3
0.2
0.3
0.4
0.3
0.3
0.3
0.2
0.1
0.1
0.2
0.2
0.2
0.3
0.2
0.2
0.3
0.2
0.2
21.1
21.1
20.9
21
21.1
21.1
21.1
21
21
21.1
21.1
21.2
21.1
21
21
20.9
20.9
20.9
20.9
20.9
20.9
20.9
20.9
21
21
21
21
21
21.1
21.1
21
21
20.9
21
21.1
21.1
21
21.1
21.2
21.1
21.1
21
21
21
21
21.1
21.1
21.1
21.2
21.2
21.2
21.1
21
21.1
21
21.1
21.1
21
21
21
0.02
0.02
0.01
0.02
0.02
0
0.03
0.04
0.03
0.02
0.03
0.02
0
0.01
0.02
0.01
0.02
0
0.01
0.02
0.01
0.02
0.01
0.02
0.01
0.02
0.02
0.03
0.03
0.03
0.02
0.03
0.03
0.01
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.02
0.03
0.03
0.02
0.02
0.02
0.03
0.02
0.02
0.03
0.03
0.02
0.03
0.02
0.01
0.01
0.02
0.03
0.02
74.1
70.1
70.1
70.1
70.1
70.1
70.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
62.1
66.1
62.1
58.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
42.
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
170.3
170.3
162.2
166.2
170.3
170.3
162.2
138.2
138.2
138.2
150.2
158.2
162.2
150.2
138.2
122.2
122.2
122.2
118.2
118.2
114.2
114.2
122.2
126.2
126.2
126.2
122.2
114.2
130.2
142.2
118.2
110.2
106.1
114.2
142.2
122.2
118.2
146.2
138.2
134.2
114.2
110.2
110.2
106.1
106.1
110.2
122.2
130.2
142.2
146.2
142.2
122.2
106.1
142.2
114.2
134.2
122.2
102.1
102.1
102.1
206.3
206.3
210.3
210.3
214.3
218.3
218.3
218.3
222.3
222.3
226.3
226.3
230.4
230.4
230.4
234.4
234.4
234.4
238.4
238.4
242.4
242.4
234.4
246.4
250.4
250.4
250.4
254.4
254.4
258.4
258.4
262.4
262.4
266.4
266.4
266.4
270.4
270.4
274.4
274.4
274.4
278.4
278.4
282.4
282.4
282.4
286.4
286.4
290.4
286.4
290.4
290.4
290.4
294.5
294.5
294.5
298.5
298.5
298.5
302.5
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
138.2
134.2
130.2
122.2
122.2
122.2
122.2
114.2
110.2
106.1
106.1
106.1
102.1
98.1
94.1
90.1
90.1
86.1
86.1
82.1
82.1
78.1
82.1
78.1
78.1
78.1
78.1
78.1
82.1
78.1
78.1
74.1
74.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
70.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
66.1
42
46
42
46
42
42
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
46
46
42
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
46
46
10.2
10
10
10
10
10
10
10
9.8
10
10
9.8
10
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
10
9.8
9.8
9.8
9.6
9.8
9.6
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.8
9.6
9.8
9.8
9.6
9.8
9.8
9.6
9.8
9.6
9.6
9.4
9.6
9.8
9.6
9.6
9.6
B-6
-------
Barrel Burning Test No. 4 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM)
C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (IB
-19.73
-19.23
-18.73
-18.23
-17.73
-17.23
-16.73
-16.23
-15.73
-15.23
-14.73
-14.23
-13.73
-13.23
-12.73
-12.23
-11.73
-11.23
-10.73
-10.23
-9.73
-9.23
-8.73
-8.23
-7.73
-7.23
-6.73
-6.23
-5.73
-5.23
-4.73
-4.23
-3.73
-3.23
-2.73
-2.23
-1.73
-1.23
-0.73
-0.23
0.27
0.77
1.27
1.77
2.27
2.77
3.27
3.77
4.27
4.77
5.27
5.77
6.27
6.77
7.27
7.77
8.27
8.77
9.27
9.77
10.27
10.77
11.27
11.77
12.27
12.77
13.27
13.77
14.27
14.77
5
2
2
3
4
4
4
6
4
2
5
6
3
4
4
4
4
3
5
7
3
2
2
3
3
4
4
4
5
4
3
3
3
6
4
3
4
6
3
3
14
24
20
13
13
13
15
20
22
25
22
24
22
21
21
20
18
22
20
18
18
17
16
14
17
18
22
20
21
23
0.1
0
0
0
0.1
0
-0.2
0
0
0
0
-0.1
0
0
0
0
-0.1
-0.1
0
0.1
0
0
0.2
0
0
0.2
0.1
-0.1
0.2
-0.1
0
0.1
0
0
0
-0.1
-0.2
0
0.1
0.4
0.5
0.7
0.7
0.9
0.9
1.1
1.1
1.5
1.1
1.3
1.1
1
0.8
0.6
1
0.8
0.7
0.8
0.6
0.7
0.8
0.7
0.6
0.4
0.4
0.4
0.4
0.5
0.4
0.4
21.7
21.6
21.6
21.7
21.7
21.7
21.7
21.6
21.6
21.6
21.7
21.6
21.6
21.7
21.6
21.6
21.7
21.6
21.7
21.7
21.6
21.5
21.6
21.6
21.6
21.7
21.6
21.7
21.6
21.6
21.5
21.5
21.5
21.6
21.6
21.6
21.6
21.6
21.5
21.6
21.5
21.4
21.4
21.4
21.4
21.3
21.3
21.3
21.3
21.3
21.4
21.4
21.3
21.5
21.5
21.3
21.4
21.4
21.6
21.5
21.4
21.4
21.4
21.4
21.4
21.6
21.5
21.4
21.6
21.7
6
6
7
7
8
5
5
7
7
7
7
6
7
7
7
7
8
7
7
8
12
13
10
9
8
10
9
12
13
13.
12
13
13
14
11
12
10
11
12
11
11
11
13
13
13
15
15
13
16
16
0.02
0.02
0.04
0.03
0.03
0.03
0.03
0.02
0.03
0.02
0.02
0
0.02
0.02
0.02
0.02
0.03
0.01
0.04
0.02
0.02
0.02
0.02
0.01
0.02
0.03
0.01
0.03
0.01
0.02
0.01
0.02
0.02
0.02
0.01
0.02
0.02
0.02
0.02
0.02
0.04
0.03
0.05
0.05
0.07
0.08
0.08
0.09
0.11
0.09
0.1
0.11
0.09
0.11
0.09
0.09
0.08
0.1
0.09
0.09
0.08
0.09
0.09
0.09
0.07
0.09
0.09
0.07
0.09
0.07
46
46
46
46
46
42
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
42.
42
42
42
42
42.
42.
42
46
42
42.
42.
42.
50.1
74.1
94.1
106.1
126.2
138.2
142.2
146.2
150.2
150.2
150.2
146.2
146.2
142.2
142.2
142.2
142.2
146.2
150.2
150.2
150.2
150.2
150.2
146.2
146.2
146.2
142.2
138.2
134.2
134.2
126.2
122.2
46.
46
46
46
46
46.
46
46.
46
46
46
46
46.
42.
46
46
46
46.
46
46.
46
46
46
46
46.
46
46
46
42
42.
42.
46.
42
42
42
42.
42.
42.
42
42
46
46.
42.
42.
42
46
46
46
46.
46
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
58.1
58.1
58.1
58.1
58.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
B-7
46.
46.
46
46
46
46.
50.1
50.1
50.1
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
58.1
70.1
78.1
82.1
114.2
186.3
246.4
306.5
378.6
478.8
570.9
639
683.1
703.1
723.2
727.2
727.2
731.2
735.2
731.2
731.2
727.2
747.2
755.2
763.2
767.2
775.2
787.3
791.3
42
42
42
42
42
42
42
42
42
42
46
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
46
50.1
50.1
50.1
54.1
58.1
62.1
66.1
66.1
70.1
74.1
74.1
74.1
74.1
78.1
78.1
78.1
78.1
78.1
82.1
82.1
82.1
82.1
82.1
82.1
82.1
82.1
86.1
86.1
86.1
90.1
90.1
90.1
50.1
50.1
46
50.1
46
46
46
50.1
46
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
46
50.1
50.1
46
46
50.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
46
46
46
46
46
46
46
50.1
46
50.1
50.1
50.1
50.1
46
50.1
50.1
46
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
46
42
42
42
46
50.1
70.1
90.1
102.1
170.3
302.5
318.5
310.5
290.4
274.4
262.4
258.4
250.4
242.4
238.4
234.4
222.3
234.4
270.4
254.4
246.4
254.4
258.4
238.4
222.3
214.3
226.3
222.3
222.3
226.3
218.3
202.3
182.3
38
42
38
42
38
38
38
42
42
42
42
42
42
42
38
38
38
38
38
38
38
38
42
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
14.2
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
15
14.8
14.8
14.8
15
14.4
14.2
13.8
13.2
12.6
12
11.6
11.6
11.4
11.2
11.2
11.4
11.4
11.4
10.6
10.2
9.8
9.2
8.8
8.8
8.2
8
7.8
7.6
7.4
7.4
7.2
7
7
6.8
6.8
6.8
-------
Barrel Burning Test No. 4 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM) | C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (IB
15.27
15.77
16.27
16.77
17.27
17.77
18.27
18.77
19.27
19.77
20.27
20.77
21.27
21.77
22.27
22.77
23.27
23.77
24.27
24.77
25.27
25.77
26.27
26.77
27.27
21.11
28.27
28.77
29.27
29.77
30.27
30.77
31.27
31.77
32.27
32.77
33.27
33.77
34.27
34.77
35.27
35.77
36.27
36.77
37.27
37.77
38.27
38.77
39.27
39.77
40.27
40.77
41.27
41.77
42.27
42.77
43.27
43.77
44.27
44.77
45.27
45.77
46.27
46.77
47.27
47.77
48.27
48.77
49.27
49.77
26
27
27
27
31
25
24
23
24
23
22
24
23
22
20
21
20
18
16
17
15
15
15
16
16
13
13
16
11
12
12
14
13
12
11
10
13
12
12
9
10
11
11
11
11
11
9
9
11
9
9
9
9
7
10
9
9
7
7
11
7
0.4
0.2
0.4
0.2
0.2
0.1
0
0.3
0.2
0.2
0.2
0
0
0
0
0
0
-0.1
0
0.2
0
0
0.2
-0.1
0.1
0.2
-0.1
0
0
0
0.1
0.1
0.1
0
0.1
0
-0.1
0
0
0.1
0.3
0
0
0
0.1
0.1
0
0.2
-0.1
0.1
0
0.1
0
0
0.1
0
0
0
0.1
0
0
0
0.2
0
0
0
0
0
0
0.1
21.7
21.6
21.5
21.5
21.7
21.6
21.6
21.7
21.6
21.5
21.5
21.4
21.5
21.5
21.5
21.6
21.6
21.5
21.5
21.6
21.4
21.4
21.6
21.6
21.6
21.5
21.6
21.6
21.5
21.5
21.6
21.6
21.6
21.5
21.6
21.5
21.6
21.7
21.6
21.5
21.6
21.6
21.7
21.6
21.6
21.7
21.6
21.6
21.4
21.5
21.5
21.5
21.5
21.5
21.6
21.5
21.5
21.4
21.6
21.5
21.5
21.5
21.5
21.5
21.5
21.5
21.4
21.5
21.4
21.5
16
21
18
18
17
17
15.
14
16
14
12
14.
12
12
13
13
11
11
11
12
11
10
10
10
9
9
11
11
10
10
9
9
10
8
7
7
9
10
7
9
9
0.08
0.08
0.07
0.08
0.07
0.07
0.07
0.06
0.07
0.06
0.05
0.06
0.05
0.05
0.07
0.07
0.04
0.05
0.05
0.05
0.04
0.03
0.04
0.03
0.03
0.04
0.04
0.05
0.04
0.04
0.04
0.02
0.02
0.04
0.04
0.02
0.04
0.04
0.04
0.03
0.02
0.03
0.04
0.04
0.02
0.04
0.05
0.03
0.02
0.02
0.04
0.04
0.04
0.02
0.02
0.01
0.02
0.02
0.03
0.04
0.03
0.03
0.03
0.04
0.04
0.04
0.03
0.05
0.03
0.02
118.2
114.2
106.1
102.1
98.1
98.1
94.1
90.1
90.1
86.1
86.1
82.1
78.1
78.1
78.1
74.1
70.1
70.1
70.1
66.1
66.1
62.1
66.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
66.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
62.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
46
46
50.1
46
46
46
46
46
46
46
46
46
46
42
46
46
46
46
46
46
46
B-8
787.3
783.3
771.2
767.2
759.2
751.2
739.2
723.2
711.1
679.1
643
611
586.9
558.9
530.8
498.8
458.7
434.7
402.6
378.6
354.6
338.5
326.5
310.5
290.4
282.4
270.4
262.4
250.4
242.4
230.4
222.3
218.3
210.3
202.3
198.3
190.3
186.3
182.3
174.3
174.3
170.3
166.2
162.2
158.2
154.2
150.2
142.2
138.2
138.2
134.2
130.2
126.2
126.2
122.2
122.2
122.2
118.2
114.2
114.2
114.2
114.2
110.2
110.2
110.2
106.1
106.1
106.1
106.1
106.1
90.1
90.1
86.1
86.1
86.1
78.1
74.1
74.1
70.1
70.1
70.1
70.1
66.1
66.1
66.1
66.1
62.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
58.1
58.1
54.1
58.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
46
50.1
50.1
50.1
50.1
50.1
46
46
50.1
46
50.1
46
46
46
46
50.1
50.1
46
46
46
46
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
46
50.1
50.1
50.1
50.1
46
46
46
50.1
50.1
46
46
46
46
46
46
50.1
50.1
50.1
50.1
46
50.1
50.1
46
162.2
150.2
150.2
142.2
134.2
126.2
122.2
118.2
114.2
114.2
110.2
106.1
102.1
98.1
94.1
94.1
90.1
82.1
78.1
78.1
78.1
74.1
70.1
70.1
70.1
70.1
66.1
66.1
66.1
62.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
58.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
42
38
38
38
42
38
38
38
38
42
42
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
6.8
6.6
6.6
6.6
6.6
6.4
6.4
6.6
6.4
6.4
6.4
6.4
6.6
6.6
6.6
6.8
6.6
6.8
6.8
6.6
6.8
7
6.6
7
7
6.8
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
7
6.8
6.8
7
7
6.8
6.8
6.8
7
7
6.8
7
6.8
7
6.8
7
7
7
-------
Barrel Burning Test No. 4 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM)
C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (IB
50.27
50.77
51.27
51.77
52.27
52.77
53.27
53.77
54.27
54.77
55.27
55.77
56.27
56.77
57.27
57.77
58.27
58.77
59.27
59.77
60.27
60.77
61.27
61.77
62.27
7
9
9
9
11
7
8
10
8
9
7
6
9
8
11
7
7
7
7
-0.1
0
0.1
0
0
0
0.2
0
0.1
-0.1
0
0
0
0.2
0
0.2
0.2
0.1
0
-0.2
0.1
-0.1
0.1
0.2
0.1
21.4
21.6
21.4
21.4
21.5
21.5
21.6
21.5
21.4
21.4
21.5
21.6
21.6
21.5
21.4
21.4
21.3
21.4
21.4
21.5
21.6
21.5
21.5
21.5
21.3
0.03
0.04
0.03
0.04
0.03
0.03
0.04
0.02
0.03
0.04
0.04
0.03
0.04
0.03
0.04
0.02
0.04
0.02
0.04
0.03
0.04
0.05
0.04
0.04
0.12
46
50.1
46
50.1
50.1
50.1
50.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
42
42.
46
46
46
42
42
42
42.
42.
42
46
46
46
46
102.1
102.1
102.1
98.1
98.1
98.1
98.1
98.1
98.1
94.1
94.1
94.1
94.1
94.1
90.1
94.1
94.1
94.1
94.1
94.1
94.1
90.1
90.1
94.1
94.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
50.1
50.1
50.1
46
46
46
46
50.1
50.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
50.1
50.1
50.1
50.1
50.1
50.1
46
50.1
50.1
46
50.1
50.1
46
50.1
46
50.1
46
46
46
46
46
46
46
46
46
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
7
7
6.8
6.8
7
7
6.8
7
6.8
6.8
6.8
6.8
7
7
6.8
6.8
6.8
6.8
6.8
6.8
6.8
7
6.8
6.8
6.8
B-9
-------
Barrel Burning Test No. 5 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM) | C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (IB
-19.847
-19.347
-18.847
-18.347
-17.847
-17.347
-16.847
-16.347
-15.847
-15.347
-14.847
-14.347
-13.847
-13.347
-12.847
-12.347
-11.847
-11.347
-10.847
-10.347
-9.8467
-9.3467
-8.8467
-8.3467
-7.8467
-7.3467
-6.8467
-6.3467
-5.8467
-5.3467
-4.8467
-4.3467
-3.8467
-3.3467
-2.8467
-2.3467
-1.8467
-1.3467
-0.8467
-0.3467
0.15333
0.65333
1.15333
1.65333
2.15333
2.65333
3.15333
3.65333
4.15333
4.65333
5.15333
5.65333
6.15333
6.65333
7.15333
7.65333
8.15333
8.65333
9.15333
9.65333
10.1533
10.6533
11.1533
11.6533
12.1533
12.6533
13.1533
13.6533
14.1533
14.6533
6
7
7
7
8
7
5
5
7
7
7
7
8
7
6
12
9
7
5
4
5
5
5
7
6
7
5
13
10
7
6
6
7
9
7
6
8
10
32
30
21
17
14
17
15
16
15
14
15
16
16
16
16
16
15
15
17
19
18
18
22
27
23
20
21
18
0.2
0.3
0.3
0.3
0.2
0.1
0.5
0.3
0.3
0.2
0.2
0.1
0.2
0.2
0.2
0.2
0.2
0.4
0.2
0.2
0.3
0.3
0.3
0.2
0.4
0.3
0.3
0.3
0.4
0.4
0.2
0.4
0.2
0.4
0.3
0.2
0.2
0.3
0.3
0.4
0.7
0.9
1.5
1.8
2.1
2.6
2.8
2.8
2.2
2.1
1.9
1.8
1.7
1.7
1.6
1.6
1.6
1.5
1.5
1.4
1.3
1.1
1.2
0.9
0.9
1.1
1.2
1.2
1
0.9
23.1
23.1
23.1
23.2
23.1
23.2
23.2
23.1
23.2
23.2
23.2
23.2
23.3
23.2
23.1
23
23.3
23.2
23.2
23.1
23.1
23.1
23.1
23.1
23
23.2
23.2
23
23.2
23.3
23.2
23.3
23.3
23.2
23.1
23.2
23.2
23.4
23.4
23.3
23.3
23.3
23.1
23.2
23.1
23.1
22.9
22.9
22.9
22.8
22.8
22.9
23
23
23
22.9
22.9
22.9
22.9
22.9
22.9
22.9
23
23
23.2
23.2
23.1
23.1
23.3
23.1
9
7
8
7
9
7
10
9
9
9
9
9
7
7
9
7
9
9
9
11
17
13.
11
11
10
11
9
10
9
9
9
11
11
11
11
10
12
12
13.
15
13.
15
15
15
15
15.
13.
12
13
0.02
0.02
0.03
0.03
0.02
0.03
0.03
0.03
0.02
0.05
0.03
0.04
0.04
0.04
0.04
0.04
0.05
0.04
0.04
0.04
0.02
0.03
0.03
0.04
0.03
0.03
0.03
0.04
0.04
0.04
0.03
0.03
0.04
0.02
0.04
0.02
0.04
0.03
0.03
0.03
0.03
0.03
0.04
0.03
0.04
0.05
0.07
0.09
0.12
0.11
0.13
0.12
0.14
0.15
0.15
0.14
0.13
0.13
0.11
0.11
0.11
0.13
0.11
0.12
0.11
0.09
0.09
0.08
0.09
0.09
42
42.
42
42
42
42
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
46
54.1
102.1
138.2
162.2
174.3
190.3
202.3
202.3
194.3
194.3
190.3
186.3
182.3
178.3
174.3
170.3
170.3
166.2
158.2
154.2
150.2
146.2
142.2
138.2
134.2
130.2
130.2
126.2
122.2
118.2
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
42
42
42.
42.
42.
42
46
46
46
46.
42.
50.1
50.1
50.1
54.1
54.1
54.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
58.1
62.1
58.1
B-10
42.
42.
42
38
42
38.
38
38.
38
42
42
42.
42.
38
38
42
42
42.
42.
42.
42
42
42
42.
42.
42.
38
42
42
42.
42.
42.
42
38
42
42.
42.
42.
42
42
46
54.1
66.1
106.1
214.3
322.5
386.6
438.7
470.7
490.8
502.8
510.8
514.8
514.8
518.8
522.8
526.8
530.8
534.9
542.9
546.9
554.9
562.9
574.9
590.9
607
631
639
639
639
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
46
46
46
46
42
46
58.1
50.1
54.1
58.1
58.1
58.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
62.1
58.1
58.1
58.1
58.1
42
42
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
38
38
38
38
38
38
38
38
38
38
38
38
42
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
42
42
38
42
46
46
50.1
90.1
350.5
522.8
578.9
578.9
623
627
538.9
530.8
518.8
478.8
430.7
382.6
358.6
330.5
302.5
306.5
318.5
294.5
258.4
250.4
242.4
222.3
218.3
214.3
210.3
206.3
198.3
190.3
182.3
34
34
34
34
34
34
34
34
34
34
38
34
38
34
34
38
38
34
34
34
38
34
34
34
38
34
34
34
38
34
38
38
34
34
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
38
20.4
20.2
20.2
20.2
20.2
20.4
20.2
20.2
20
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20
20.2
20.2
20.2
20
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20.2
20
20
20
20
19.4
19
19
19
19
19.4
19
18.4
18.4
17.4
16.6
16.2
16
15.6
15
14.8
14.6
14.2
14.2
14
13.8
13.8
13.6
13.6
13.4
13.4
13.4
13.2
13.2
13
-------
Barrel Burning Test No. 5 CEM Data
ET (MIN) CO (
15.1533
15.6533
16.1533
16.6533
17.1533
17.6533
18.1533
18.6533
19.1533
19.6533
20.1533
20.6533
21.1533
21.6533
22.1533
22.6533
23.1533
23.6533
24.1533
24.6533
25.1533
25.6533
26.1533
26.6533
27.1533
27.6533
28.1533
28.6533
29.1533
29.6533
30.1533
30.6533
31.1533
31.6533
32.1533
32.6533
33.1533
33.6533
34.1533
34.6533
35.1533
35.6533
36.1533
36.6533
37.1533
37.6533
38.1533
38.6533
39.1533
39.6533
40.1533
40.6533
41.1533
41.6533
42.1533
42.6533
43.1533
43.6533
44.1533
44.6533
45.1533
45.6533
46.1533
46.6533
47.1533
47.6533
48.1533
48.6533
49.1533
49.6533
=PM) NOX (PPMJ02 (%) HC (PPM)
21 0.7 23.2 14
32 0.9 23.2 12
22 0.9 23 14
20 0.8 23.2 14
24 0.7 23.3 13
20 0.7 23.2 13
20 0.8 23.2 14
19 0.6 23.1 15
23 0.6 23.2 13
24 0.7 23.3 13
20 0.7 23.2 16
23 0.7 23.1 15
23 0.7 23.2 15
22 0.6 23.1 17
24 0.7 23.2 15
25 0.7 23.2 15
23 0.7 23.3 15
22 0.7 23.2 13
24 0.7 23.3 13
22 0.7 23.3 13
26 0.6 23.2 15
31 0.6 23.4 14
22 0.7 23.2 11
20 0.6 23.4 14
18 0.6 23.2 13
16 0.7 23.3 12
17 0.7 23.4 13
17 0.6 23.4 13
18 0.6 23.5 12
16 0.7 23.3 11
17 0.7 23.3 13
18 0.7 23.4 12
14 0.7 23.4 13
17 0.6 23.3 11
14 0.4 23.2 12
17 0.4 23.3 11
18 0.5 23.5 11
15 0.5 23.4 12
15 0.6 23.2 11
16 0.7 23.3 11
22 0.6 23.4 12
17 0.7 23.5 12
12 0.6 23.2 11
13 0.5 23.3 11
13 0.6 23.5 11
14 0.7 23.3 12
14 0.6 23.3 10
15 0.7 23.4 11
13 0.6 23.4 13
12 0.7 23.3 11
13 0.5 23.3 11
14 0.5 23.4 11
13 0.5 23.5 11
12 0.7 23.4 11
11 0.6 23.3 10
15 0.5 23.3 10
25 0.5 23.5 9
11 0.6 23.5 9
12 0.7 23.4 12
11 0.6 23.3 11
11 0.6 23.3 11
9 0.7 23.3 9
12 0.4 23.3 11
13 0.5 23.4 10
14 0.5 23.5 10
10 0.7 23.4 9
9 0.6 23.3 11
11 0.7 23.4 11
11 0.4 23.4 9
14 0.5 23.5 11
C02 (%) TEMPI (cllEMP2 (cllEMP4 (CJTEMPS (CJTEMP6 (cllEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (LB
0.1 114.2 62.1 0 647 58.1 46 170.3 38 13.2
0.09 110.2 58.1 0 643 58.1 46 154.2 38 13
0.09 106.1 58.1 0 643 58.1 46 146.2 38 13
0.08 102.1 58.1 0 643 58.1 46 134.2 38 13
0.08 98.1 58.1 0 647 58.1 46 134.2 38 13
0.08 98.1 58.1 0 651 54.1 46 130.2 38 13
0.06 94.1 58.1 0 655 54.1 46 126.2 38 12.8
0.08 94.1 58.1 0 659.1 54.1 46 126.2 38 12.8
0.06 90.1 58.1 0 655 54.1 46 122.2 38 12.8
0.07 90.1 58.1 0 651 54.1 46 122.2 38 12.6
0.07 86.1 58.1 0 643 54.1 46 122.2 38 12.4
0.05 86.1 58.1 0 643 54.1 46 114.2 38 12.6
0.04 82.1 58.1 0 643 54.1 46 110.2 38 12.6
0.05 82.1 58.1 0 639 54.1 46 110.2 38 12.4
0.06 82.1 54.1 0 643 54.1 46 106.1 38 12.4
0.06 78.1 54.1 0 643 54.1 46 102.1 38 12.4
0.07 78.1 54.1 0 647 54.1 46 98.1 38 12.2
0.04 78.1 54.1 0 647 50.1 46 94.1 38 12.2
0.04 74.1 54.1 0 647 50.1 46 90.1 38 12.2
0.05 74.1 54.1 0 647 50.1 46 90.1 38 12.2
0.07 74.1 54.1 0 651 50.1 50.1 90.1 38 12.2
0.07 74.1 54.1 0 647 50.1 46 90.1 38 12.2
0.05 70.1 54.1 0 647 50.1 46 82.1 38 12.2
0.04 70.1 54.1 0 643 50.1 46 78.1 38 12.2
0.06 70.1 54.1 0 643 50.1 46 78.1 38 12.2
0.04 70.1 54.1 0 643 50.1 50.1 78.1 38 12
0.05 70.1 54.1 0 639 50.1 50.1 78.1 38 12
0.06 66.1 54.1 0 643 50.1 50.1 74.1 38 12
0.07 66.1 54.1 0 639 50.1 50.1 74.1 38 12.2
0.06 66.1 54.1 0 639 50.1 50.1 74.1 38 12
0.05 66.1 54.1 0 643 50.1 50.1 70.1 38 12
0.06 66.1 54.1 0 643 50.1 50.1 70.1 38 12
0.06 66.1 54.1 0 643 50.1 50.1 70.1 38 12
0.04 62.1 54.1 0 643 50.1 50.1 66.1 38 12
0.05 62.1 54.1 0 647 50.1 50.1 66.1 38 12
0.05 62.1 50.1 0 647 50.1 50.1 62.1 38 12
0.07 62.1 50.1 0 651 50.1 50.1 62.1 38 12
0.05 62.1 54.1 0 651 50.1 50.1 62.1 42 12
0.06 62.1 54.1 0 651 50.1 50.1 66.1 42 12
0.04 58.1 54.1 0 655 50.1 50.1 62.1 42 12
0.05 58.1 54.1 0 655 50.1 50.1 62.1 42 12
0.05 58.1 50.1 0 659.1 50.1 50.1 62.1 42 12
0.03 58.1 50.1 0 659.1 50.1 50.1 62.1 42 12
0.03 58.1 50.1 0 663.1 50.1 50.1 62.1 42 12
0.04 58.1 54.1 0 663.1 50.1 50.1 62.1 42 12
0.04 58.1 50.1 0 667.1 50.1 50.1 58.1 42 11.8
0.03 58.1 50.1 0 667.1 50.1 50.1 58.1 42 12
0.02 58.1 50.1 0 671.1 50.1 50.1 58.1 38 12
0.03 58.1 50.1 0 671.1 50.1 50.1 58.1 42 12
0.02 54.1 50.1 0 675.1 50.1 50.1 58.1 38 12
0.04 54.1 50.1 0 675.1 50.1 50.1 58.1 38 12
0.03 54.1 50.1 0 679.1 50.1 50.1 58.1 38 11.8
0.03 54.1 50.1 0 679.1 50.1 50.1 58.1 42 12
0.04 54.1 50.1 0 679.1 50.1 50.1 58.1 42 11.8
0.02 54.1 50.1 0 679.1 50.1 50.1 58.1 42 11.8
0.04 54.1 50.1 0 679.1 50.1 50.1 58.1 38 11.8
0.03 54.1 50.1 0 683.1 50.1 50.1 58.1 42 11.8
0.03 54.1 50.1 0 679.1 50.1 50.1 58.1 38 11.8
0.04 54.1 50.1 0 683.1 54.1 50.1 54.1 38 11.8
0.03 54.1 50.1 0 683.1 50.1 50.1 58.1 42 11.8
0.04 54.1 50.1 0 683.1 50.1 50.1 54.1 42 11.8
0.03 54.1 50.1 0 687.1 50.1 50.1 54.1 42 11.8
0.03 54.1 50.1 0 691.1 50.1 50.1 54.1 42 11.6
0.03 54.1 50.1 0 691.1 50.1 50.1 54.1 42 11.6
0.02 54.1 50.1 0 695.1 50.1 50.1 54.1 42 11.8
0.03 54.1 50.1 0 695.1 50.1 50.1 54.1 42 11.6
0.03 54.1 50.1 0 695.1 50.1 50.1 54.1 42 11.6
0.03 54.1 50.1 0 699.1 50.1 50.1 54.1 42 11.6
0.04 54.1 50.1 0 699.1 50.1 50.1 54.1 42 11.6
0.04 54.1 50.1 0 695.1 50.1 50.1 54.1 42 11.6
B-11
-------
Barrel Burning Test No. 5 CEM Data
ET (MIN) | CO (PPM) | NOX (PPM)02 (%) HC (PPM) | C02
TEMPI (CJTEMP2 (CJTEMP4 (CJTEMP5 (CJTEMP6 (CJTEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (IB
50.1533
50.6533
51.1533
51.6533
52.1533
52.6533
53.1533
53.6533
54.1533
54.6533
55.1533
55.6533
56.1533
56.6533
57.1533
57.6533
58.1533
58.6533
59.1533
59.6533
60.1533
60.6533
61.1533
61.6533
62.1533
62.6533
63.1533
63.6533
64.1533
64.6533
65.1533
65.6533
66.1533
66.6533
67.1533
67.6533
68.1533
68.6533
69.1533
69.6533
70.1533
70.6533
71.1533
71.6533
72.1533
72.6533
73.1533
73.6533
74.1533
74.6533
75.1533
75.6533
76.1533
76.6533
77.1533
77.6533
78.1533
78.6533
79.1533
79.6533
80.1533
80.6533
81.1533
81.6533
82.1533
82.6533
83.1533
83.6533
84.1533
84.6533
11
11
10
14
11
12
13
13
23
15
15
15
14
13
13
9
12
16
26
19
12
10
13
12
10
10
11
11
10
13
11
11
11
13
12
9
11
11
21
22
20
15
12
13
11
11
11
11
10
12
13
10
17
15
13
13
14
13
9
11
13
10
11
13
17
21
23
21
11
9
0.6
0.7
0.7
0.6
0.5
0.7
0.6
0.7
0.7
0.7
0.8
0.6
0.4
0.9
0.7
0.7
0.6
0.6
0.6
0.5
0.7
0.6
0.8
0.7
0.8
0.6
0.7
0.7
0.7
0.8
0.8
0.6
0.7
0.6
0.7
0.9
0.7
0.9
0.7
0.6
0.7
0.7
0.7
0.8
0.8
0.9
0.8
0.8
0.7
0.7
0.6
0.9
0.9
0.9
0.8
0.7
0.6
0.8
0.8
0.7
0.7
0.9
0.9
0.7
0.7
0.9
0.8
0.8
0.9
0.9
23.5
23.4
23.4
23.4
23.4
23.5
23.5
23.3
23.4
23.5
23.3
23.4
23.5
23.5
23.4
23.3
23.4
23.4
23.5
23.5
23.6
23.5
23.4
23.4
23.3
23.3
23.3
23.4
23.4
23.5
23.3
23.5
23.4
23.4
23.4
23.3
23.5
23.4
23.4
23.5
23.4
23.4
23.5
23.5
23.4
23.3
23.3
23.3
23.4
23.4
23.3
23.4
23.5
23.5
23.4
23.4
23.4
23.6
23.4
23.4
23.5
23.5
23.4
23.5
23.5
23.4
23.4
23.6
23.5
23.4
9
10
9
11
10
11
12
9
11
10
11
10
11
11
11
10
10
10
9
11
11
10
12
11
10
10
10
11
10
11
9
11
10
11
11
9
11
10
10
11
9
10
9
9
11
10
10
9
9
9
9
9
11
10
11
10
10
9
9
10
10
7
10
10
10
9
9
11
10
9
0.04
0.03
0.04
0.04
0.02
0.03
0.05
0.04
0.02
0.04
0.02
0.03
0.04
0.06
0.04
0.06
0.04
0.03
0.03
0.03
0.03
0.03
0.04
0.05
0.04
0.03
0.03
0.02
0.03
0.05
0.03
0.04
0.04
0.02
0.04
0.03
0.03
0.04
0.02
0.02
0.04
0.04
0.03
0.05
0.04
0.03
0.03
0.03
0.02
0.03
0.03
0.03
0.06
0.04
0.04
0.02
0.03
0.03
0.04
0.02
0.03
0.04
0.03
0.04
0.04
0.03
0.04
0.04
0.05
0.03
54.1
54.1
54.1
50.1
54.1
50.1
54.1
54.1
54.1
50.1
50.1
54.1
54.1
54.1
50.1
54.1
54.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
54.1
54.1
50.1
50.1
50.1
54.1
50.1
50.1
54.1
54.1
54.1
50.1
50.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
46
46
46
46
50.1
46
50.1
46
46
50.1
46
46
46
46
46
46
46
46
46
50.1
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
46
50.1
46
46
46
46
46
46
46
46
46
46
46
50.1
46
46
46
46
46
46
50.1
46
B-12
695.1
691.1
691.1
687.1
683.1
675.1
667.1
659.1
655
647
643
639
635
631
627
623
623
619
619
615
611
611
607
603
603
603
603
599
599
599
594.9
594.9
590.9
590.9
590.9
590.9
590.9
586.9
586.9
586.9
582.9
582.9
582.9
578.9
578.9
578.9
578.9
574.9
574.9
574.9
574.9
570.9
570.9
566.9
566.9
566.9
562.9
562.9
562.9
558.9
558.9
554.9
558.9
554.9
554.9
550.9
550.9
546.9
546.9
546.9
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
50.1
50.1
50.1
54.1
50.1
54.1
54.1
50.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
50.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
54.1
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
42
46
42
42
42
42
42
42
42
42
11.6
11.6
11.6
11.6
11.4
11.4
11.4
11.4
11.6
11.4
11.4
11.4
11.4
11.4
11.4
11.4
11.4
11.2
11.2
11.2
11.2
11.2
11.2
11.2
11.4
11.2
11.2
11.2
11.2
11.2
11
11.2
11.2
11
11
11
11
11
10.8
11
10.8
10.6
11
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.8
10.6
10.8
10.6
10.6
10.6
10.6
10.6
10.6
10.6
-------
Barrel Burning Test No. 5 CEM Data
ET (MIN) CO (
85.1533
85.6533
86.1533
86.6533
87.1533
87.6533
88.1533
88.6533
89.1533
89.6533
90.1533
90.6533
91.1533
91.6533
92.1533
92.6533
93.1533
93.6533
94.1533
94.6533
95.1533
95.6533
=PM) NOX (PPMJ02 (%) HC (PPM)
14 0.8 23.5 9
14 0.8 23.5 9
12 0.9 23.4 9
11 0.9 23.4 8
13 0.7 23.5 9
13 0.9 23.5 10
11 1 23.4 9
10 1 23.3 12
10 1.1 23.3 9
12 0.9 23.3 10
10 0.8 23.4 9
12 0.9 23.6 10
14 0.9 23.6 10
13 0.8 23.5 11
13 0.7 23.5 10
13 0.9 23.4 8
13 0.9 23.5 11
13 0.7 23.5 10
15 0.9 23.6 12
11 0.9 23.5 11
14 1.4 23.4 11
11 1 22.3 7
C02 (%) TEMPI (cllEMP2 (cllEMP4 (CJTEMPS (CJTEMP6 (cllEMP7 (CJTEMP8 (CJTEMP9 (CJ weight (LB
0.04 54.1 46 0 542.9 54.1 54.1 54.1 42 10.6
0.05 54.1 46 0 542.9 54.1 54.1 54.1 42 10.4
0.05 54.1 46 0 542.9 50.1 54.1 54.1 42 10.6
0.04 54.1 46 0 542.9 50.1 54.1 54.1 42 10.6
0.04 50.1 46 0 542.9 54.1 54.1 54.1 42 10.6
0.04 54.1 46 0 538.9 54.1 54.1 54.1 42 10.6
0.04 50.1 50.1 0 538.9 54.1 54.1 54.1 42 10.4
0.03 54.1 46 0 538.9 54.1 54.1 54.1 42 10.4
0.04 54.1 46 0 538.9 54.1 54.1 54.1 46 10.4
0.03 54.1 50.1 0 534.9 54.1 54.1 54.1 42 10.4
0.02 54.1 46 0 530.8 54.1 54.1 54.1 42 10.4
0.05 54.1 46 0 530.8 54.1 54.1 54.1 42 10.2
0.03 54.1 50.1 0 530.8 54.1 54.1 54.1 42 10.4
0.03 54.1 46 0 530.8 54.1 54.1 54.1 42 10.2
0.04 54.1 50.1 0 526.8 54.1 54.1 54.1 42 10.4
0.04 54.1 50.1 0 526.8 54.1 54.1 54.1 42 10.2
0.04 54.1 50.1 0 526.8 54.1 54.1 54.1 42 10.2
0.02 54.1 50.1 0 526.8 54.1 54.1 54.1 42 10.2
0.06 54.1 50.1 0 526.8 54.1 54.1 54.1 42 10.2
0.03 54.1 50.1 0 522.8 54.1 54.1 54.1 42 10.2
0.04 54.1 50.1 0 522.8 54.1 54.1 54.1 42 10.2
0.01 50.1 50.1 0 518.8 54.1 54.1 50.1 46 10.2
B-13
-------
o
CEM CALIBRATION DATASHEET
Date %''£.'*' '*??
Analyzer Type/Model Q*-, > folS A /*? ~%?$L
Analyzer Working Range 2. 3 ^
Analyzer Zero Control Setting (Initial/Final) ? '^ / 9' ->
Analyzer Span Control Setting (InitiaVRnaD /
"
tn™-™ P™t*™ Po»*at%
Concentration P •&
1 f -7
V I1'3 5~~ i ^ 0 j 1 • /* ]} '/
2&'\ 2*0 ,\
*-- / id "\
Z /l-^ -^ ^^6 /^.o /f'C^
J I?- Y > ,vd/f.i
Reference Standards
1. Supplier Aiff. vfi£ 1/ *L* t~7~~J Tank#
Tank Presssure 1 1 QD /V / Concentration
Certified by Certification date
2. Supplier 4 i r< ffaPls^-Tf Tank*
Tank Presssure /A35 /^2_ Concentration
Certified by Certification date
3. Supplier Arffc /faj?^^/ Tank*
Tank Presssure /5"£> /5" / Concentration
Certified by Certification date
Figure 4-1. CEM caltoration data sheet.
CEM CALIBRATION DATASHEET
Anarppr Type/Model ^^2- 1 L5e &(*>X
Anaryzer Working Ranoe J£> '/*
Analyzer Zero Control Settim (Initial/Final) g', 1 / ^> "\
AnaiyzBr Span Control Settina (Initial/final) /
KnownCySnder Delwiy Analynr Maaiurad %Oe»umlon «„„„<( Deviation torn
Concenliation P(pai) HowRals Conoenralion ofFu««cale concgnMjon known Oonoenlrat
1 f> ft}.
I 2 fz-fio ^> o •'i 6 u -° ^ ^Uf*
/ -/
x fij^y. ^> 0 • " //3 t=. /,6o
^ /i 01% ^5~ 0- 'i. & / ' 66
1,4— ^ /^//
y O -jfi./' ^> o • t o O-^i !
Reference Standards
1. Supplier /^//-t ffZa I? £<{,-{ J Tank#
Tank Presssure //££> /*->£. Concentration
Certified by Certification date
^
2. Supplier _/| ^/f (f^l/fi^L // Tank #
Tank Presssure //}d& /xT" Concentration
Certified by Certification date
?, ,
3. Supplier /{>£. (/A^J/tf'tf / / Tank*
Tank Presssure 1 ^6b f(,£~ Concentration
Certified by Certification date
„
4. Suppter /jtrt 1 £j(?U-t3~ * Tank*
Tank Presssure -5&t> /*Xj Concentration
Certified by Certification date
Figure 4-1. CEM caltoration data sheet.
-------
OEM CAUBRATION DATASHEET
Date
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (Initial/Final)
GEM CALIBRATION DATASHEET
Date
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (Initial/Final)
0
ro
Known OfMat
Concentration
2&»
Slfa
29fa
Delvoy
J-
J,"
5^
Aivlyw
O.«o
0,<4«
6.^*
Maaund
(5
^^
A47
%Devi«ion
MMtumd
/d
5^
Z,«8
Dwialionttim
Reference Standards
1. Supplier A\R~ ffo&t^Tj Tank#
Tank Presssure / ' //2& /*£•£" Concentration
Certified by
Certification date
2. Suppiier_
Tank Presssure
Certified by
3. Supplier,
Tar* Presssure
Certifiedby
4. Supplier
Tank Presssure
Certified by
Tank #
Concentration
Certification date
Tank#
Concentration
Certification date
Tank*
Concentration _
Certification date
Known Cylinder
Concentration
2^5
/df^
j? /?/?/*\
DafcMfy
5
^
5~
Analyzer
Flow fata
.yr
,vr
,^/r-
Mewured
Conoenrafcn
6*6
/0,C
^^
%OwMon
olFulUcale
POSKB
Meaturad
Concentration
1,2-
m
i^
Deviation torn
known ConcenraL
^
Reference Standards
1. Supplier AlR ^/^fl^Tj Tank*
Tank Presssure / j dD ff/ Concentration
Certified by
Certification date
Z. Supplier_
Tank Presssure
Certified by
/
Tank #
Concentration _
Certification date
3. Supplier A /X
Tank Presssure
Certified by
Tank#
Concentration _
Certification date
4. Supplier,
Tank Presssure
Certified by
Tank #
Concentration
Certification date
Figure 4-1, CEM calibration data sheet
Figure 4-1. CEM calibration data sheet.
-------
GEM CAUBRATIQN DATASHEET
GEM CALBHATIC*! DATASHEET
Date
Date
o
CO
I
2
1
Analyzer Type/
Analyzer Worit
Analyzer Zero
Analyzer Span
Known Oftntet
2e^
*SOff«
fOfa
31^
Model /14C— I f)6CbJW/v '-
noRaree
Control Setting
Control Setting
IT
J
J
2
3
(InitiaLfinal)
'OZ^ _
1
(Inrtial/Rnal) /
Amlym
Row MM
0
9
/o
?
^x«
^
y^^
^ Itf-n,
^V-
olFulKais
MMWKJ
-37
^
^
//
Deference Standarts _
1, Steelier A/r< j^ft^£?UlTJ Tank#
Tank Presssure / 1 $D /'^ / Concentratksn
Certifiedby
2. Supplier
Certification date
A /SL fs?/)J9&<-CTf Tank*
Tank Presssure /9€?^ /%"/ Concentration
Certfcdby
3. Supplier
CertStcation date
/4/-/C f>A&0tojC~S Tank*
Tank Presssure Concentration
Certifiedby
4, Supplier
Certification date
A (/***. f&ftPfr-CT"/' Tank*
Tank Presssure /£&$ /*/"/ Concentration
Certifiedby
CertSkation date
Analyzer Type/
Analyzer Work!
Analyzer Zero
Analyzer Span
Known CrtWer
J^
2&A
t?.r
i^i. ^\
Model >n:>A (--^ / /rfgO'fr-.
rfl Rarae (b - 7-° *6>
Sontral Setting
Control Setting
Mwy
^^
&
O
Initial/Final)
/
(Mai/Final) /
£*£L
<^zft
Q.S-
o, *l
/?.«-
H,C
*™
PMHMt
2(-2-
I A 1Z.
I &I Q
DeviftBoo Hvn
Reference Standards
i. Supdier Tankf
Tank Presssure Concentration
Certified by
a. Supplier
Certification date
Tank #
Tank Presssure Concentration
Certifiedby
3, Supplier
Certification date
Tank*
Tank Presssure Concentration
Certifiedby
4. Supplier
Certification data
Tankt
Tank Presssure Concentration
Certifiedby
Certification date
Figure 4-1. GEM calibration data sheet.
Figure 4-1. GEM caltoratton data sheet.
-------
Date
9*- 5o
GEM CALBHAT10N DATASHEET
CEM CALBHATION DATASHEET
Date
O
Analyzer Type/
Analyzer Worki
Analyzer Zero
Analyzer Span
Known Cylnvlef
-2^
/ i^J */
/ * <__?£? /f
/.^
o.s*-
Modal C-°J? / PfeCfc. y&>i
rig Range O . •- ..{o "*^
Dontrol Setting
Control Setting
^
S
J5
^
Model C.6 1 /^f£/i W
ng Range O ~ /£>£?&
Qontrol Setting
Control Setting
EMwy
£•
s-
sr
(Initial/Final)
^
i
(Initial/Final) /
fUn Kale
o.f~
0,C
o.r
Conamration
0
L^ / ,X^
**7 £T* /
*SS
MtM(M
12_
5"J?
Zf](
ImmOmiiinni
Rafarence Standards
1. Suffer Tank#
Tank Presssure Concantration
Certified by
2. Supplier
Certification date
Tank #
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank*
Tank Presssure Concentration
Certified by
4, Supplier
Certification date
Tank*
Tank Presssure Concentration
Carttffedby
Certification date
Figure 4-1. CEM calibration data sheet.
Figure 4-1. CEM calibration data sheet
-------
GEM CALIBRATION DATASHEET
GEM CALBRATION DATASHEET
o
Date
Date
g
Analyzer Typa*
Analyzer Work;
Analyzer Zero
Analyzer Span
rrr
~L€X*
;*
0
^.c
l%££
PEW-MI
0^
13
s.<*
Analyzer Type/
Analyzer Worki
Analyzer Zero
Analyzer Span
srr
?.***
H^b
10
Model 7/^C— / TfSezo S~ {
no Ranoe O — /oc>a ,#9*5*1
Control Setting
Control Setting
DaSwKy
°(
1
*l
(Initial/Final)
1
(IrtitiaVRnaf) /
Anatyzw
FowBae
/.O
/.o
1^
^^m
z
LffTSJ
Cj O.
Otfl&KM>
MMWTM
A
i^i
^
Reference Standards Reference Standards
1. Supplier Tank* 1. Supplier Tank*
Tank Presssure Concentration
Certified by
2. Supplier
Certification date
Tank #
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank*
Tank Presssure Concentration
Certified by
4. Supplier
Certification date
Tank*
Tank Presssure Concentration
Certified by
Certification date
Tank Presssure Concentration
Certified by
I, Supplier
Certification date
Tank*
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank#
Tar* Presssure Concentration
Certified by
i Supplier
Certification date
Tank #
Tank Presssure Concentration
Certified by
Certitication date
Figure 4-1. CEM calibration data sheet.
Figure 4-1. CEM calibration data sheet.
-------
GEM CAUBRAT1ON DATASHEET
CEM CALIBRATION DATASHEET
Date
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (IniUalrRnal)
Analyzer Span Control Setting (MflaYRnal)
0
O)
rrr
/y,f
f^.n
^(, 0
PtMD
5"
^
5-
How Aw
0
Deviation from
Reference Standards
1. SuDDfer Tank*
Tank Presssure Concentration
Certified bv Certification date
2. Supplier,
Tank Presssure ,
Certified by
3. Supplier
Tank Presssure ,
Certified by
4. Suppfer_
Tank Presssure
Certified by ,
Tank f
Concentration _
Certification date
Tank*
Concentration _
Certification date
Tank #
Concentration _
Certification date
Date
Analyzer Type/
Analyzer Work.
Analyzer Zero
Analyzer Span
KnmnQrMw
^^o
AJT6
/.Of
,?*,
Model C,O i / DSCk_rv>4AJ si
inp Range () — /0*£
Control Setting (InttiaVFinal)
•a
1
Control Settinq (InitialTinat) /
Dsdvwy
f
$
$
f
Anrfyiw
FkwRile
6,5
o,$
0,$
6.5-
C^ll,
^^
/^"4
A63
^^
!,^
MWXKJ
,-0*02-
!,S*I
I.OP
O^k
Otvtexm irom
Reference Standards
1. Supplier Tank#
Tank Presssure Concentration
Certified by
2. Supplier
Certification date
Tank#
Tank Presssure Concentration
Certified by
3, Supplier
CerlSicalton date
Tank f
Tank Presssure Concentration
Certified by
l. Supplier^
Certification date
Tank #
Tat* Presssure Concartratian
Certified by
Certification date
Figure 4-1. CEM calibration data sheet.
Figure 4-1. CEM caltorafion data sheet.
-------
OEM CAUBRATION DATASHEET
O
Date
Analyzer Type/Model , t_2_
Analyzer Working Range ,„,,,,
Analyzer Zero Control Setting (initial/Final)
Analyzer Span Control Setting (InftiaVRnal)
KJTOWH Cyltrxto
ttetvwy
5"
5'Z
Reference Standards
1. Supplier
Tank Presssure _
Certified by
2. Supplier
Tank Pressure _
Certified by
3. Supplier
Tank Presssure _
Certifiedby
4. Supplier
Tank Presssure _
Certified by
D
Concentration _
Certification date
Tank*
Concentration _
Certification date
Concentration _
Certification date
Tank #
Concentration _
Certification date
n
Oate
GEM CALIBRATION DATA SHEET
Analyzer Typafl
Analyzer Workt
Analyzer Zero!
Analyzer Span
rrr
Z£*»
/O
f
Modal W^x I /^<~° /U_
ng Range <& "~ /&£> /y^\.
Sontrol Setting
Control Setting
Oeknty
$
£•
%
Initial/Final)
i
(IrtrSal/Rnari /
Analyzer
FowRaB
o.r
o.f
o*
-------
OEM CAUBRATION DATA SHST
Date
Analyzer Type/Model __jL£t5
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Rnal)
Analyzer Span Control Setting (InWaVfinal)
Q—
Known CyMv
Conamntet
Mwy
POK-IW
MMlund
/« 6
0,
-3.2.
/, t> qSO
Ad
O
oo
Reference Standards
Tank Presssure ,
Certified by
2. Supplier
Tank Presssura
Certified by
3. Supplier
Tank Presssure.
Certified by
4.
Tank Presssure,
Certified by
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Figure 4-1, CEM caltoratfen data sheet.
CEM CALIBRATION DATASHEET
Date
Analyzer Type/
Analyzer Work)
Analyzer Zero)
Analyzer Span
KmmCyMar
CVJ
naRanoe
Control Setting
Control Setting
CMwy
6
*
3
(Initial/Final)
-•
/
(Initial/final) /
Araiyzer
FkwFUM
,5
.6
-3
Msaaurad
ir.Ll
1o.[
7.7- • d
KOnMon
MMtUKHJ
/,M
z«.S
Z-Z-O
tm^^ma.
Heference Standards
1. Supplier Tank*
Tank Presssure Concentration
Certified by
2. Supplier
Certification date
Tank#
Tank Presssure Concentration
Certified by Certification date
3, Supplier
Tank*
Tank Prasssure Concentration
Certified by Certification date
4. Supplier
Tank*
Tank Presssure Concentration
Certified by Certification date
Figure 4-1. CEM calibration data sheet.
-------
Date
.X
3
GEM CALIBRATION DATASHEET
CEM CALIBRATION DATASHEET
0
CD
Analyzer Type/
Analyzer Worki
Analyzer Zero
Analyzer Span
Known CyMDv
/'
f -54
M
42,
Model C ' @J 1 ^(^-<^^
raRanoe ® " (
(Initial/Final)
/
(MafFmaD /
FbTa!
o.s
o-f
Q.£
©-5"
c^ZL
ff^O
A ^ C
*°lf
/^
KDwUfinn
POX-MI
Mamund
Conoeniration
0.0(7
f. 76
in
- 5G
(
-------
GEM CALIBRATION DATA SHEET
Date
AnalyzerType/Model fu u^f
Analyzer WoiWng Range
Analyzer Zero Control Setting (Irttial/Hnal)
Analyzer Span Control Setting (MaVRnaf)
Date
CEM CALBRATION DATASHEET
fH6,
- efCc3
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (InitialTtnal)
o
Known Cylinder
Gonoensnaem
tc
CMvwy
PUP*
5
o Reference Standstills
1, SuppBer
Tank Presssura ,
Certified by
2. Supplier
Tank Presssure _
Certified by
3. Supplier
Tank Presssure,
Cartifiadby
4. Supplier
Tank Prasssure
Certlfiedby
0-3
tft
Patnnt
Maaund
0,2.
CO
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Tank*
Concentration _
Certification date
Tank*
Concentration _
Certification date
rrr
a
Y5a
^0
Dstwty
^
1
°\
Ana^zar
FbwRan
f.OQ/,
l.o
(.5
Corsoeniraiion
^ 0
ltfL\
c}^
olfu«saaj«
c«r«««v
0
q-^-7
f/
Davwticn Irom
femwrnConoenirsi,
Beferenee Standards
1. Supplier Tank*
Tank Presssure Concentration
Certified by
Certification date
2. Supplier_
Tank Presssure
Certified by
3. Supplier,
Tank Pressure.
Certified by
4, Supplter_
Tank Presssure,
Certified by
Tank #
Concentration
Certification date
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Figure 4-1, CEM calibration data sheet.
Figure 4-1. CEM calibration data sheet
-------
O
Date
OEM CALIBRATION DATASHEET
Analyzer Type/Model ^z.
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (Initial/Final)
KncwnCylinaV
ll.'f
l°lA
2LO
Dfljhmy
P(P»9
^
£
f
Z>
Ana^ror
FBwRaB
. o"
^
. O
.5"
Meuurod
(7-7
H.^
^(. 3
%DnM)on
ofFultola
/9^
PtMHOSi
Meuurad
Conoomranon
nn
r
-------
o
rx>
Data
GEM CALBRATION DATA SHEET
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (InrflaVFmal)
Known Cylinder
Concentration
Mmy
f
5
AnilyTBf
FtowRaB
Reference Standards
1. Supplier
Tank Presssure
Certified by
2. Supplier_
Tank Presssure
Certified by
3. Supplier,
Tank Presssure .
Certified by
4. Supplier,
Tank Presssure
Certified by
Msaiuroo
Concefilraton
0
5(0
POM-BSI
Mumnd
Tank#
Concentration _
Certification date
Tank #
Concentration _
Certification date
Tank#
Concentration _
Certification date
Tank #
Concentration _
Certification date
0«viatjon torn
known Concen tat
Date
GEM CALBRATION DATASHEET
Analyzer Type/Model
Analyzer Working Range
Analyzer Zero Control Setting (Initial/Final)
Analyzer Span Control Setting (Initial/Final)
Known Cylinder
r
rO
/
DaSvxy
P«*i)
^
^
/
Analyzer
Ftowflae
- 0'
.S
.4
Moaitmd
o
lo-^
£.G
%D8VMni
ofFunicato
PoK-Mt
Meaund
Concemration
0.1-
/0,3
r.1
PDSHQffl%
Deviation from
known Gonowitrai
Reference Standards
1. Supplier
Tank Presssure .
Certified by
Z. Supplier,
Tank Presssure
Certified by
3. Supplier,
Tank Presssure
Certified by
4, Supp«er_
Tank Presssure
Certified by
Tank #
Concentration _
Certification date
Tank #
Concentration _
Certification date
Tank #
Concentration
Certification date
Tank#
Concentration _
Certification date
Figure 4-1. CEM calibration data sheet.
Figure 4-1. GEM calibration data sheet.
-------
o
Date
GEM CALIBRATION DATASHEET
GEM CALIBRATION DATASHEET
Data
Analyzer Worki
Analyzer Zero
Analyzer Span
Known CytWer
6
*(4>
-------
CEM CAUBRATIQN DATASHEET
CEM CAUBHATTON DATA SHEET
Data
Date
o
Analyzer Type/
Analyzer World
Analyzer Zeroi
Analyzer Span
KtwwCylMw
0
\-SC
f.rf
. $l
Model ^-^1' > iSfc**.**- 1>~* i
mRanoe
Sortrol Setting
Control Setting
Defivwy
5
~>
S
£
(IrtSial/Final)
/
(JniBaVFinal) /
Anolyxer
FtowfUn
.tT
/*
' O
-/
e^ZL
^0
J&-
^/
^^
liDoviMDn
Mawmd
0 -60
(. t{
1-00
^l^
OwWonhxn
Reference Standards
1. Supplier Tank*
Tank Presssure Concentration
Certified by
2. Supplier
Certification dale
Tank*
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank#
Tank Pressaire Concentration
Certified by
4. Supplier
Certification date
Tank#
Tank Presssure Concentration
Certified by
Certification date
Analyzer Type/
Analyzer Work!
Analyzer Zero i
Analyzer Span
Known CyStxfw
0
S(l
2-1 /
Model £ 6 / Ojf.dC.*! r*
npRanoe
3ont»l Setting
Control Setting
OtftNiy
PftHl)
6
5
*
Initial/Final)
ffb 75
/
(Initial'Finaf) /
Andyzw
FtowBas
-f
.£
.i
MMtuntd
0
^^
"""? jf^ C^
Hl(&^Vj» I
rf^H
Mautmd
Cono0nirxSon
u
,^o
27 \
Devteiiod from
known Cortownmt
Reference Standards
1. Supplier Tank*
Tank Presssure Concentration
Certified by
2. Supplier
Certification date
Tank *
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank#
Tank Pressaire Concentration
Certified by
4. Supplier
CerWicatton date
Tankf
Tank Presssure Concentration
Certified by
Certification date
Figure 4-1. CEM eataattondata sheet.
Figure 4-1. CEM caMbratton data sheet.
-------
GEM CALIBRATION DATASHEET
Date
O
en
Analyzer Typafl
Analyzer Worki
Analyzer Zero(
Analyzer Span
SET
0
(0
6
T *
Mfldal fj 0 / i
OlFuSKSi*
POM-MI
Mwnuml
a-r
(0,1
6-6
DwMonttorn
Reference Standards
1. Suoofer Tank*
Tank Presssure Concentration
Certified by
2. Supplier
Certification date
Tank #
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tank
#
Tank Pwsssura Concentration
Certified by
4. Supplier
Certification date
Tankf
Tank Presssure Concentration
Certified by Certification date
Oats ^.//i_/t«
Analyzer Type/
Analyzer Work!
Analyzer Zero
Analyzer Span
rrr
0
'(^ 0
__^1£_
GEM CALIBRATION DATASHEET
Model f^lff I ttfJr 1^1 f~H C~~
nq Ranoe
Control Setting
Control Setting
PM)
t
1
1
(Inttial^inal)
/
(Inttjal/Final) /
Ararat
L*
i
t
MMKIWI
^.
^3
*^
POMM
Meumd
^
^(^
10
Po«l«n%
OwMoninn
Reference Standards
1. Supplier Tank#
Tank Presssure Coneentratton
Certified by
2. Supplier
Certification date
Tank #
Tank Presssure Concentration
Certified by
3. Supplier
Certification date
Tankt
Tank Presssure Concentration
Certified by
4. Supplier
Cert»lcatton data
Tank*
Tank Presssure concentration
Certified by
Certification date
Figure 4-1. CEM calibration data sheet.
Figure 4-1. CEM calibration data sheet.
-------
S-.U,
Revision j
August 1995
Page 3 of 12
TABLE 4-1. BURN MATERIAL COMPOSITION
(^ON-RECYCLER_(%}) AVTD RECYCLER (%)
PAPER f
Newspaper, books and office paper 32.8 743.
11.1 ZSI .SO
1.6 172.. 43
10.3 2.13,60
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
3.3
61.9
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plasticizers e.g., cadium
PET#1 (bottle bill)
HDPE: #2, LDPE #4, and PP #5
PVC: #3
PS: #6
MIXED #1
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
10 ^
0.6
6.6
0.2
0.1
0.1
I 43. Si
M.SO
2.ZS
2.27
5.7 129.2?
3.7 e3.H!
1.1 ZH.9I
9.7 ZZS.9I
0.4 3.0 |
7.3 16 4. £3
1.7 3S. S3
1.1 2.4. HO
100.0 2274.45.
10.8 Ib/day
— L
10.4
4.5
0.3
0.3
3.7
6.9
4.0
1.0
3.7
100.0
3.3 Ib/day
WE IS-f-tT
a>~J*JL =4 AVID egc.ycLSK_
.
TABLE 4-1. BURN MATERIAL COMPOSITION
NON-RECYCLER (%) (AVTD RECYCLER (%)
PAPER
Newspaper, books and office paper
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plasticizers e.g., cadium
PET SI (bottle bill)
HDPE: #2, LDPE #4, and PP »S
PVC: #3
PS: #6
MIXED #7
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
IO/3/9S"
32.8
11.1
7.6
10.3
0.6
6.6
0.2
0.1
0.1
5.7
3.7
1.1
9.7
0.4
7.3
1.7
100.0
10.8 Ib/day
74. 8H
3.3
61.9
10.4 -2. 3 r. S3
4.5 10 2 .2.2
0.3 6 . S£
0.3 C. ?Z
3.7 W.&L
6.9 i^.te
4.0 90.JI
1.0 22.7,6
3.7 S3.92
-. 2.267.19a
100.0 : c
3.3 Ib/day
-I rid I 5? I „
-------
AVID
W/vsre
S/3O/3S"
TABLE 4-1. BURN MATERIAL COMPOSITION
PAPER
Newspaper, books and office paper
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
boxes
PLASTIC RESIN (all types may contain
trace chlorine or plasticizers e.g.} cadium
PET*1 (bottle bill)
HDPE: #2, LDPE #4, and PP #5
PVC: #3
PS: #6
MIXED »7
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bii!)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
NON-RECYCLER (%) (AVID RECYCLER (%T) =,
3,74. S~&
32.8
11.1
7.6
10.3
0.6
6.6
0.2
0.1
0.1
5.7
3.7
1.1
9.7
0.4
7.3
1.7
1.1
100.0
10.8 Ib/day
3.3
61.9
0.3
0.3
3.7
-7013,3 G
10.4 (179.99
' r/0.92
14.
3.7 419.60
6.9
4.0 H ?3. S-3
1.0 113. ?3
KI3.HS
100.0
3.3 Ib/day
BUTCH
0/1/95
TABLE 4-1. BURN MATERIAL COMPOSITION
NON-RECYCLER (%) AVID RECYCLER (%)
PAPER
Newspaper, books and office paper 32.8
Magazines and junk mail 11-1
Corrugated cardboarid and craft paper 7.6
Paperboard, milk cartons and drink 10.3
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plasticizers e.g., cadiurn
PET#1 (bottle bill) 0.6
HDPE: #2, LDPE #4, and PP #5 6.6
PVC: #3 0.2
PS: $6 0.1
MIXED #7 ' 0.1
FOOD WASTE 5.7
TEXTILE/LEATHER 3.7
WOOD (treated/untreated) 1.1
GLASS/CERAMICS
Bottles/Jars (Bottle bill) 9.7
Ceramics (broken plates and cups) 0.4
METAL - FERROUS
Iron - cans 7.3
NON-FERROUS
Aluminum - cans (Bottle Bill), 1-7
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe, 1.1
batteries)
PERCENT TOTAL 100.0
TOTAL WEIGHT GENERATED PER 10.8 Ib/day
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
3.3
61.9 "7019.4?
10.4 I I 79. SB
4.5 ' S-ll. ol
0.3 3,4.03
0.3 3.H.O?
6.9
1.0 113.73
3.7 HI3.7S-
TOT7H-; I I 3,4 I. T I <
100.0
3.3 Ib/day
-------
KJ-R-^CYoL- g"B BUTOf op
peep/«6o 3/0/35- TABLE4-1. BURN MATiauALCOj!8»osrrioN
('TTON-iRECYCLER (%T) AVTJD RECYCLER (%)
PAPER ~ ~
Newspaper, books and office paper
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plastidzers e.g., cadium
PET SI (bottle bill)
HDPE: #2, LDPE S4, and PP #S
PVC: #3
PS: #6
MIXED #7
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
32.S 2Z3I,7(
11.1 "7ST5-.2I
7.6
10,3
0.6 HO. S3
6.6 4H9.//
0.2 I3.£i
0.1 6. SO
0.1 6. go
5.7 3,4-7.93
3.7 _£ASV?$":
1.1 7^.33
9,7 6 6 O. O£.
0.4 z.7,35
7.3
1.7 I 1 ST. C7
100.0
10.8 Ib/day
3.3
61.9
10.4
4.5
0.3
0.3
3.7
6.9
4.0
1.0
100.0
3.3 Ib/day
reuse.
#5"
life
'•*•*?
3/1 2 /Elf TABLE 4-1. BURN atoTERIAL_COMPOaTION
PAPER
Newspaper, books and office paper
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plasticizers e.g., cadium
PET SI (bottle bill)
HDPE: #2, LDPE #4, and PP #5
PVC: B
PS: #6
MIXED «1
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROOS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
%T) AVID RECYCLER (%)
32.8
II.1
7.6
10.3
2.131. S3
7S5". 17
SiT. I I
-JOO.8O
0.6
6.6
0.2
0.1
0.1
5.7
3.7
1.1
9.7
0.4
7.3
1.7
1.1
TCTTM- ;
100.0
MO.7M
M^a.oir
13X1
6. S3
e.si
y«?7.6s
ZS-1.73
74.6?-
&6O. fs:
•2.7. 30
496.43
1 1 ST. V 1
•74. £3
. £8(0.01^,
„
10.4
4.5
0.3
0.3
„
3.7
6.9
4.0
1.0
3.7
100.0
10.8 Ib/day
3.3 Ib/day
-------
Ktsvision j
August 1995
Page 3 of 12
TABLE 4-1. BURN MATERIAL COMPOSITION
(^NON^MCTCLERj^^ AVID RECYCLER (%)
PAPER "fr %.
Newspaper, books and office paper • 7^3,30 32,8 R74S3O 3.3
Magazines and jynk mail Z.51.7S 11.1 O.2SI7S"
Corrugated cardboard and craft paper ("72., 37 7,6 o. H2 "S7
Paperboard, milk cartons and drink 2-^3.£0 10.3
boxes
!•»..£ I o.« 0
W9.69 6.6 0,14363
^•SH 0.2 O.CWS4
Z'*' 0,1 0. DD22?
2. 2? 0.1 O.O0227
S.7 O. !
83.923,7 O.OSS92
1M.951.1 O.
PLASTIC RESIN (all. types may contain
trace chlorine or plasticixers e.g., cadium
PET#1 (bottle bill)
HOPE: #2, LDPE #4, and PP #5
PVC; #3
PS; #6
MIXED #1
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL ~rmt~:
TOTAL WEIGHT GENERATED PER 10.8 Ib/day
HOUSEHOLD FOR DISPOSAL IN
BORN BARRELS
9,7 Q
9.D3-0.4 O, OO9O7
2.Z7O
10.4
4.S
0.3
0.3
3.7
6.9
4,0
1.0
3,7
100.0
3.3 Ib/day
Revision j
August 1995
Page 3 of 12
TABLE 4-1. BURN MATERIAL COMPOSITION
NON-RECYCLER (%) f AVID RECYCLES (%)
PAPER
Newspaper, books and office paper 32.8 7
Magazines and junk mail I I.I
Corrugated cardboard and craft paper 7,6
Paperboard, milk cartons and drink 10.3 lHO3,gg 61.9 t.HOT>?3
PLASTIC RESIN (all. types may contain
trace chlorine or plastidzers e.g., cadium
PET #1 (bottle bill)
HOPE: #2, LDPE #4, and PP #5
PVC: #3
PS: #6
MIXED #7
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
SON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
0.6
6,6
0.2
0.1
0.1
5.7
3.7
1.1
9.7
0,4
7,3
100.0
10.8 Ib/day
io.4
ioi.06 4.5
e.go 0.3
6.SO 0.3 O.O06SO
3.7 0.05^,92
6.9 0.
90.7Z 4J O.Q307Z
O2.6? 1.0 O.OZZ&g
f3,923.7 0.05392
100,0
3.3 Ib/day
-------
D
dn
otJ OP
2, s~JL4
August 1995
Page 3 of 12
PAPER
Newspaper, books and office paper
Magazines and junk mail
Corrugated cardboard and craft paper
Paperboard, milk cartons and drink
boxes
PLASTIC RESIN (all. types may contain
trace chlorine or plastidxers e.g., cadiuwi
PET#1 (bottle bill)
HDPE: #2, LDPE #4, and PP K
PVC: #3
PS; #6
MIXED #7
FOOD WASTE
TEXTILE/LEATHER
WOOD (treated/untreated)
GLASS/CERAMICS
. Bottles/Jars (Bottle bill)
Ceramics (broken plates and cups)
METAL - FERROUS
Iron - cans
NON-FERROUS
Aluminum - cans (Bottle Bill),
Aluminum foil, other Aluminum
Other Non-Iron (wire, copper pipe,
batteries)
PERCENT TOTAL
TOTAL WEIGHT GENERATED PER
HOUSEHOLD FOR DISPOSAL IN
BURN BARRELS
TABLE 4-1. BURN MATERIAL COMPOSITION
NON-RECYCLER(%), AVID RECYCLER (%) a,
. __ . g- . i
32.8
11.1
7,6
10.3
S6 i .
0.6 &8.0H
6.6 7^1 W
0.2 22.6?
0.1 1 1. 5V
0.1 (1,34
5.7 6H6. 33
3.7 4i9, SS1
1.1 \Z^.~»1
9,7 IO99.9!?
0.4 M s;~j>e
7,3 gZ.7.iZ
1.7 192.78
100.0
10,8 Ib/day
61.9
10.4 M ? 9.36
4.5 SI O. ?O
3. SB
6.9
4,0
1.0 111.4
3.7 4(3. SB
100.0
3.3 Ib/day
Table 4-1. BURN MATERIAL COMPOSITION
AVID RECVCLER
PAPER a,
a
(p Newspaper, books and office paper Z 2 31,71
(Z) Magazines and junk mail 75"5, 2'
(3) Corrugated cardboard and (craft paper s 17. (t-
(H) Paperboaid, rnilk cartons and drin
32,8 2,2 1-/7I
(g) PLASTIC RESIN (all types may contain
trace Cl or piastidzers e.g., Cd)
PET « (bottle bill)
© HDPE: #2, LDPE #4 and PP f 5
d&> PVC: #3
(f) PS: #6
© MKED #7
Ufi) FOOD WASTE
/^~\
(iU TEXTILE/LEATHER
@ WOOD (treated/untreated)
GLASS/CERAMICS
HO. 82. 0.6 0. OH 082-
13. 6 j 0.2 0. 0> T>6\
6
-------
Bottles/Jars (Bottle bill) .6 S3. 33 9,7 a .653 9 3
(Q) Ceramics (broken plates and cups) 2.7,27. Q,4 0, t>2 7- 2 2.
METAL - Ferrous
tsp Fe-cans M3C.63 ?J Q
NON-Ferrous
Al - cans (Botfle Bill), Al foil, other Ai 1/5". 67 1,7 O, I/S"^7 1,0
i . (g) Other Non-Fe (wire, copper pipe, batteries) ~?H-B'i I.I 0.07^8^ 3.7
PERCENT TOTAL _100.0 . 100.0
1 xss'/avi'
TOTAL WEIGHT GENERATED PER 10.8 Ib/day 3.3 Ib/day
HOUSEHOLD FOR DISPOSAL IN BURN
BARRELS
-------
APPENDIX E. SAMPLE CUSTODY SHEETS
Acurex
Environmental
Report To:
Bill To:
Tf-\eytejVe.
PROJECT srrc
Chain of Custody Record
Page,
SITE NAME
OLLEC
FIELD RUSH SAMPLE DATE/
SAMPLE ID FACTOR MATRIX TIME
"L
S"
REMARKS
•s/
ANALYSES
EROPROJEGTS'
OO \
DATE REPORT DUE
VERBAL/FAX/HARDCOPY
I/
REMARKS
LAB ID NO.
/tor lab use onlv)
RECEIVED BY: I DATE I TIME I RELINQUISHED BY: I DATE I TIME I RECEIVED BY: DATE
t^-W NOi rMn.,fe .
RELINQUISHED^: (\-/\ ~
/m^j- (^<^
DATE I TIME I RELINQUISHED E
DATE
DATE
LAB USE ONLY
RKM^S^
$JL
TIME
'*&>
AIRBILL NO.
OPENED BY:
DATE
TIME
TEMP 'C
SEALt
REMARKS " ," -!,,'-,!( :"
EPA/AEERL ONSITE LABORATORY SUPPORT CONTRACT
SAMPLE CHAIN OF CUSTODY RECORD
rev. 11/94
Page of:
Facility of Origin:
Facility of
b-
Destination
LJi
P reject: ( /
Samples Collected By:'
Field
Sample
ID
",Af\l ¥$
CM^7
j\\t7~ r/f
Sample Description:
use o^
W. c
-AiJAw
^^
A. n&ffH
" /
Comments:
Received By ft):
Date
and
Time
^
^^_
f
Analyses Requested
~?
f
1
«
~j
I
Daten"ime(1):
Disposal Information (Include Date. Time
Relinqt
Custodian,
Ished By (2):
Date/Time (2):
OSL Project #:
Request Resulls By:
Report Results To:
C - L^^Lffl5
For Problems Contact (Name/Phone #):
C. tote, fpt It^',^^
Remarks:
^fflO 7 ar*C«^
^F= 7^f a ^ c« 1
"
Relinquished By(1):
Received By (2): •
Lab ID:
Dateffime(l):
Date/Time (2):
and Comments):
E-l
-------
EPA/AEERL ONS1TE LABORATORY SUPPORT CONTRACT
SAMPLE CHAIN OF CUSTODY RECORD
rev. 11/94
Page of 3
-acility of Origin: Facility of Destination:
1-1 1 1 1 / ^"f3 /4. $\ 1 / M.
fuli/c^'S CJ^*/ /ft Ui ^ e *v
Project;
Samples Collected By;"
r - lAvo/^ r^sx^
Fieid
Sample
ID
AU * ?
Cw "^5
Sarnp!e Description:
AUk.Y*^- QtiM
<, 1/lr,'mi5, C«_
Date
and
Time
Analyses Requested
*-
V
«C
(
N*
I
OSL Project #;
Request Results By:
f
Report Results To:
/"* / "*f"
For Problems Contact (Name/Phone f ):
Remarks:
fir 1 (""£ ^i*'1
jfr / ^*7 /}
i
Comments:
Received Sy{l); Date/Time (1|:
Relinquished By (2):
DstefTime (2):
Relintwished By (1):
Received By (2); '
Disposal information (Include Date, Time, Custodian, and Comments!:
Lab ID:
Dale/Time (1):
OafefTifne (2): I, /
EPA/AEERL ONSITE LABORATORY SUPPORT CONTRACT
SAMPLE CHAIN OF CUSTODY RECORD
tev. 11/94
-aclfily of Origin: FaeMfiy of Desiinatson:
'rojecl; ft i /
Sahiples Collected By:'
Fteld ^
Sample
IO
A i i JVV*
Ai/1 «G
^ssJ^"
C^1^
"~\
Sample Description:
OMfM Gv-W<4r
"^^^v^ „ /# 7s~s-
Date
and
Time
^^7<
it
Analyses Requested
T
~^
t
0
o
I
Comments:
Received By (1(: Datemme (1j:
Relinquished By (2}:
Da en"ime (2):
SI Project n.
equest Resulis 3y:
Report Results To;
or Problems Contact {Name/Phone #}:
VA /
Remark-s:
IIT^JM
Received 8y (2): '
tab ID:
Daten"irne{1):
Da!e/Tima {2):
Disposal Information {Include Date, Time, Custodian, and Cornmentsl:
E-2
-------
ACUREX
Corporation
Report To:
Environmental Systems Division < /"/,, if,
BBTo:
4S15 ProspecEUS DftvB
Dulwn,NC 27713
{91SS 544-4535
\ -±
PROJECT SITE
SJTENAME r
Chain of Cyst
PO#
h
COLLECTED BY (Signalufs) ,' '
FIELD
SAMPLE ID
4
V ,'< .
RUSH
FACTOR
)
,
REMARKS
RECEIVED BY:
DATE
SAMPLE
MATRIX
TIME
DATE/
TIME
03
o:
u.
O
1
\
/,
AN
/
odxfi
ALYSES /
/ / >
II,
1 ,
ecord
~T
It
/ERO
"p'Roe
Paoe of
*T-£ ' - * *-' * ' " 'V %
^•3*^ ' ^ " ^ ^ ^
' DATE REPORT DUE
////// VERBAUFAXMARDCOPY
/
LL
RELINQUISHED BY:
3Aifc
/
LAB ID NO
REMARKS (lor lab me only}
RELINQUISHED BY
: TIME RECEIVED BY:
DATE
TIME
DATE 1 TIME
RaiNQUBHED BY. DATE TIME
LAB USE ONLY
RgSiVEDft^iUeSY:^ '
Wtfij TIMg
" * , *-
AlRBUtHO.
OPENSOBY:
. ... ..
DATE1 TIME
1
TEMP'C jS6Ai# - jCWWftON;
PW«®', ,•'•-..-'"'., ,-•'..
ACUREX
Corporation
FtepottTo:,^ .
Environmental Systems Division f • c • ii/~KJ_.
HI To:
4915Pt08[»ctusDnvfl
Durham, NO 27713
ffltS) 544-4535
Chain of Custody Record
Pane of
LAB USE ONLY
; "
OSffii,
OATE
CONPfTW
E-3
-------
APPENDIX F: ACUREX RAW DATA
Acurex-RTP Laboratory Results - Raw VOC Analytical Data
EPA Method TO14/8240 Compounds
Hewlett Packard 5890 GC / 5971 MSD; 30m x 0.53u DB-624 fused silica capillary
Tekmar LSC-2000 w/Carbotrap/Carbosieve SIM.
PQL = Practical Quantitation Limit
N/D = Not Detected
J = Detected @< PQL
N/A = Not Applicable
Sample Type
Test #
Master Index
Sample ID
Collection Date
Analysis Date
dichlorodifluoromethane
dichlorotetrafluoroethane
chloromethane
vinyl chloride
1,3-Butadiene
bromomethane
chloroethane
trichlorofluoromethane
Dichlorotrifluoroethane
Trichlorotrifluoroethane
1,1-dichloroethene
Acetone
Carbon Disulfide
methylene chloride
3-Methylpentane
1,1-dichloroethane
Butyl Methyl Ether
Cis-1,2-Dichloroethene
2-Butanone
Ethyl Acetate
chloroform
1,1,1-trichloroethane
carbon tetrachloride
benzene
1,2-dichloroethane
trichloroethene
1,2-dichloropropane
cis-1,3-dichloropropene
Dimehtyl Disulfide
4-Methyl-2-Pentanone
Octane
MDL
0.33
0.61
0.3
0.22
0.1
0.11
0.39
0.11
0.1
0.06
0.15
0.1
0.1
0.49
0.1
0.05
0.1
0.06
0.1
0.1
0.33
0.07
0.35
0.32
0.09
0.08
0.11
0.15
0.1
0.1
0.1
PQL
1.08
2.01
1
1
1
1
1.28
1
1
1
1
1
1
1.62
1
1
1
1
1
1
1.09
1
1.14
1.07
1
1
1
1
1
1
1
Can
1
3549
Avid
Recycler
1/31/95
3/1/95
NG/L
<148
<207
315
<75.7
370
<115
<78.4
<166
<184
<227
<117
535
<94.1
<103
<104
<119
<124
<117
<88.5
<107
<144
<161
<186
2437
<131
<162
<137
<136
<114
<121
<138
Can
2
3553
Avid
Recycler
2/1/95
3/2/95
NG/L
<136
<190
329
<69.6
146
<105
<72.0
<153
<169
<209
<108
336
<86.4
166
<96.2
<110
<114
<108
<81.2
<98.4
<133
<148
<171
917
<120
<148
<126
<125
<105
<111
<127
Can
3
3554
Hut
Blank
2/2/95
3/2/95
NG/L
<22.2
<31.1
<21.7
<11.3
<9.90
<17.2
<11.7
<24.9
<27.6
<34.0
<17.5
7.17
<14.0
<15.4
<15.6
<17.9
<18.5
<17.6
<13.2
<16.0
<21.6
<24.1
<27.9
<14.1
<19.6
<24.2
<20.5
<20.4
<17.1
<18.2
<20.6
Can
4
3555
Non
Recycler
2/3/95
3/2/95
NG/L
<182
<256
251
<93.2
186
<141
<96.5
<205
<227
<280
<144
1284
<115
<126
<129
<147
<152
<145
56
<132
<178
<199
<230
1684
<162
<199
<168
<168
<141
<149
<170
Can
5
3556
Non
Recycler
2/15/95
3/2/95
NG/L
<117
<164
111
<59.7
141
<90.9
<61.8
<131
<145
<179
<92.8
505
<74.3
<81.3
<82.7
<94.6
<97.9
<93.0
91.5
<84.6
<114
<127
<147
675
<103
<127
<108
<108
<90.4
<96.1
<109
F-1
-------
toluene
trans-1,3-dichloropropene
1,1,2-trichloroethane
tetrachloroethene
Butyl Acetate
1,2-dibromoethane
chlorobenzene
Nonane
ethyl benzene
m,p-xylene
o-xylene
Styrene
Pinene
1,1,2,2-tetrachloroethane
Decane
4-Ethyltoluene
1,3,5-Trimethylbenzene
1,2,4-Trimethylbenzene
Limonene
1,3-Dichlorobenzene
1,4-Dichlorobenzene
Benzyl Chloride
Undecane
1,2-Dichlorobenzene
Dodecane
1,2,4-Trichlorobenzene
Hexachlorobutadiene
Naphthalene
0.1
0.19
0.06
0.05
0.1
0.07
0.05
0.1
0.09
0.05
0.13
0.07
0.1
0.06
0.1
0.1
0.11
0.22
0.1
0.05
0.04
0.1
0.1
0.04
0.1
0.07
0.04
0.1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
1
934
<136
<163
<201
<141
<228
<136
<154
315
198
148
1061
<165
<204
<172
<146
<146
<146
<165
<178
<89.6
<153
<189
<178
<206
<131
<317
343
311
<125
<150
<184
<129
<209
<125
<141
123
<118
<118
426
<151
<187
<158
<134
<134
<134
<151
<164
<82.3
<141
<174
<164
<189
<120
<291
129
<16.7
<20.4
<24.4
<30.1
<21.0
<34.0
<20.4
<23.0
<19.2
<19.2
<19.2
<18.9
<24.7
<30.5
<25.7
<21.8
<21.8
<21.8
<24.7
<26.7
<13.4
<22.9
<28.3
<26.7
<30.8
<19.6
<47.4
<23.4
596
<168
<201
<248
<173
<280
<168
<190
403
<158
<158
1154
<203
<251
<212
<179
<179
<179
<203
<220
<110
<189
<233
<220
<254
<162
<390
250
311
<108
<128
<158
<111
<180
<107
<121
111
<101
<101
247
<130
<161
<135
<115
<115
<115
<130
<141
<70.7
<121
<149
<141
<162
<103
<250
105
F-2
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Avid-Recycler Test #1
Household Wastes
Trash #1
Trash Semivol #1
STRASH1B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
8/30/95
9/10/95
none
Bill Preston
Dennis Tabor
Presampling Surrogates
d10-Anthracene
Percent Recovery (%)
79.4
Post Sampling Surrogates
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
Percent Recovery (%)
15.9
47.5
34.9
59.5
70.6
107.9
Target Analytes
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
Total ug
ND
ND
ND
ND
ND
ND
91.2
1.1J
ND
Target Analytes
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
Total ug
ND
ND
ND
F-3
-------
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol 14.5
n-Nitrosopyrrolidine ND
Acetophenone 4.9J
Hexachloroethane ND
4-Methylphenol 25.9
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone ND
2,4-Dimethylphenol 10.8
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene 37.9
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene 6.7J
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
Target Analytes
Acenapthylene 15.9
1,4-Napthoquinone 2.4J
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene ND
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran 3.6J
F-4
-------
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene 4.1J
Diethyl pthalate 1.2J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene 19.3
Anthracene 3.8J
Di-n-butyl pthalate 3.8J
Isodrin ND
Fluoranthene 8.0J
3,3'-Dimethylbenzidine ND
Pyrene 10.6
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 3.4J
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene 6.7J
Chrysene 8.3J
di-n-octyl pthalate ND
Benzo (b) fluoranthene 5.8J
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene 1.3J
Benzo (a) pyrene 4.0J
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene 3.3J
Dibenz (a,h) anthracene 1.1J
Benzo (ghi) perylene 2.8J
Tentatively Identified Cmpds ret time (min) Total M9
Cyclotrisiloxane,hexamethyl- 6.47 17.1
Unknown 7.12 14.7
F-5
-------
Acetamide, N,N-dimethyl - 8.36 15.3
Unknown 12.41 17.1
Hexanoic acid, 2-ethyl 17.16 16.6
Cyclopentasiloxane, decameth 17.39 36.5
Unknown 19.99 14.8
Unknown 26.67 35.0
Unknown Hydrocarbon 27.59 53.2
1,6Anhydor-.beta.Dglucopyram 28.09 25.5
Unknown 30.57 16.6
Phenol, 2,6-bis(1,1-dimethyletr 33.59 26.7
Unknown Hydrocarbon 43.83 19.1
Unknown 44.93 84.3
Unknown sustit-Hexanedioic AI 45.39 107.1
Unknown Hydrocarbon 45.51 27.6
Unknown Hydrocarbon 45.59 23.8
Unknown 47.11 22.9
Unknown Hydrocarbon 53.03 18.5
NS = not spiked
j = detected below lowest calibration level
F-6
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Avid Recycler Test #2
Household Wastes
Trash #2
Trash Semivol #2
STRASH2B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
9/1/95
9/12/95
5x
Bill Preston
Dennis Tabor
Presampling Surrogates
d10-Anthracene
Percent Recovery (%)
98.4
Post Sampling Surrogates
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
Percent Recovery (%)
68.5
95.2
94.4
96.9
75.7
110.1
Target Analytes
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
Total ug
ND
ND
ND
ND
ND
ND
345.6
4.3J
ND
Target Analytes
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
ND
1.4J
6.6J
F-7
-------
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol 70.9
n-Nitrosopyrrolidine ND
Acetophenone 17.9J
Hexachloroethane ND
4-Methylphenol 122.5
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone ND
2,4-Dimethylphenol 18.5J
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene 229.0
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene 50.8
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
Target Analytes
Acenapthylene 51.9
1,4-Napthoquinone 3.4J
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene 3.7J
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran 12.7J
F-8
-------
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene 19.7J
Diethyl pthalate 2.0J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene 51.2
Anthracene 11.1J
Di-n-butyl pthalate 9.0J
Isodrin ND
Fluoranthene 9.6J
3,3'-Dimethylbenzidine ND
Pyrene 8.5J
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 3.3J
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene 1.8J
Chrysene 1.7J
di-n-octyl pthalate ND
Benzo (b) fluoranthene 1.5J
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene ND
Benzo (a) pyrene ND
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene ND
Dibenz (a,h) anthracene ND
Benzo (ghi) perylene ND
Tentatively Identified Cmpds ret time (min) Total M9
Cyclotrisiloxane, hexamethyl- 6.51 66.7
Unknown 7.12 66.6
F-9
-------
Unknown 7.36 101.4
Ethylbenzene 8.09 167.0
Unknown 8.37 73.8
Xylene isomer(s) 8.42 91.8
Phenylethyne 8.66 57.7
Styrene 9.20 292.1
Benzaldehyde 11.75 116.0
Unknown 12.41 130.4
Unknown Hydrocarbon 12.74 70.2
Indene 14.53 98.3
Unknown Hydrocarbon 16.08 58.0
Cyclopentasiloxane, decameth 17.39 126.2
Benzole Acid 18.68 58.2
Napthalene, 1-methyl- 22.77 64.5
Unknown 26.67 85.8
Unknown Substi HexadioicAci 45.37 170.1
Unknown Pthalate 50.43 67.1
NS = not spiked
j = detected below lowest calibration level
F-10
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Hut Blank
Household Wastes
Trash #3
Trash Semivol #3
STRASH3B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
9/6/95
9/12/95
none
Bill Preston
Dennis Tabor
Presampling Surrogates
d10-Anthracene
Percent Recovery (%)
69.3
Post Sampling Surrogates
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
Percent Recovery (%)
7.5
12.6
11.1
13.5
10.7
14.3
Target Analytes
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
Total ug
ND
ND
ND
ND
ND
ND
78.7
ND
ND
Target Analytes
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
Total ug
ND
ND
1.9J
F-11
-------
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol ND
n-Nitrosopyrrolidine ND
Acetophenone ND
Hexachloroethane ND
4-Methylphenol ND
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone ND
2,4-Dimethylphenol ND
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene 1.0J
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene ND
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
Target Analytes
Acenapthylene ND
1,4-Napthoquinone ND
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene ND
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran ND
F-12
-------
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene ND
Diethyl pthalate 3.6J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene ND
Anthracene ND
Di-n-butyl pthalate 2.8J
Isodrin ND
Fluoranthene ND
3,3'-Dimethylbenzidine ND
Pyrene ND
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 1.5J
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene ND
Chrysene ND
di-n-octyl pthalate ND
Benzo (b) fluoranthene ND
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene ND
Benzo (a) pyrene ND
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene ND
Dibenz (a,h) anthracene ND
Benzo (ghi) perylene ND
Tentatively Identified Cmpd ret time (min) Total [ig
Acetamide, N,N-dimethyl 8.29 35.1
F-13
-------
Xylene isomer(s) 8.44 13.0
Unknown 12.41 21.5
Unknown Hydrocarbon 13.04 9.7
Unknown 17.11 15.9
Cyclopentasiloxane,decametf 17.39 23.0
Cyclopentasiloxane,decametf 22.29 22.1
Unknown Hydrocarbon 25.03 12.1
Unknown Siloxane 26.67 11.1
Unknown Hydrocarbon 27.58 12.6
Unknown substituted amide 37.88 20.7
Unknown substituted amide 41.39 14.0
Unknown substituted amide 41.77 24.2
Unknown 43.84 14.6
Unknown 44.82 15.4
Unknown substituted amide 44.99 202.5
Unknown substit-Hexanedioii 45.42 167.1
Unknown Phthalate 50.44 63.4
Unknown Phthalate 51.27 69.5
Unknown 51.82 25.5
NS = not spiked
j = detected below lowest calibration level
F-14
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Non Recycler Test #4
Household Wastes
Trash #4
Trash Semivol #4
STRASH4B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
9/12/95
9/20/95
2X
Bill Preston
Dennis Tabor
Presampling Surrogates
d10-Anthracene
Percent Recovery (%)
80.48
Post Sampling Surrogates
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
Percent Recovery (%)
1.1
6.9
4.4
9.4
12.5
17.0
Target Analytes
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
Total ug
ND
ND
ND
ND
ND
ND
120.0
ND
ND
Target Analytes
1,4-Dichlorobenzene
1,2-Dichlorobenzene
Benzyl Alcohol
Total ug
ND
ND
3.5J
F-15
-------
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol 27.8
n-Nitrosopyrrolidine ND
Acetophenone 2.8J
Hexachloroethane ND
4-Methylphenol 47.5
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone ND
2,4-Dimethylphenol 14.0
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene 30.0
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene 5.5J
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
Target Analytes
Acenapthylene 22.7
1,4-Napthoquinone 1.6J
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene 1.2J
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran 4.3J
F-16
-------
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene 5.8J
Diethyl pthalate 2.9J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene 21.1
Anthracene 4.4J
Di-n-butyl pthalate 2.8J
Isodrin ND
Fluoranthene 6.7J
3,3'-Dimethylbenzidine ND
Pyrene 7.0J
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 3.0J
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene 2.0J
Chrysene 2.5J
di-n-octyl pthalate ND
Benzo (b) fluoranthene 2.5J
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene ND
Benzo (a) pyrene 2.2J
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene 1.5J
Dibenz (a,h) anthracene ND
Benzo (ghi) perylene 1.6J
Tentatively Identified Cmpds ret time (min) Total M9
2-Furancarboxaldehyde,5meth 11.68 25.8
2Cyclopenten1one,2-hydroxy3 13.85 45.6
F-17
-------
Unknown 16.18 57.6
Unknown 19.15 33.3
14:36-Dianhydro-alpha-d-gluc( 19.97 44.4
Phenol, 4-ethyl-2-methoxy- 21.61 27.1
Butylated Hydroxytoluene 27.69 23.9
Unknown 27.96 45.9
Unknown 28.23 22.1
Unknown 28.68 39.6
Benzene, 1,1' -(1,3-propanedi} 31.31 23.0
Hexadecanoic Acid 37.72 42.7
OleicAcid 41.06 25.3
Unknown 44.93 179.4
HexanedioicAcid,bis(2-ethylhe 45.38 215.3
Unknown 46.30 21.8
Unknown Pthalate 47.64 186.5
Unknown Pthalate 50.43 75.6
Unknown 51.81 38.5
NS = not spiked
j = detected below lowest calibration level
F-18
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Non-Recycler Test #5
Household Wastes
Trash #5
Trash Semivol #5
STRASH5B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
9/12/95
9/20/95
2X
Bill Preston
Dennis Tabor
Presampling Surrogates
Percent Recovery (%)
d10-Anthracene
96.5
Post Sampling Surrogates
Percent Recovery (%)
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
51.2
83.0
74.6
80.9
72.1
92.4
Target Analytes
Total ug
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
ND
ND
ND
ND
ND
ND
113.6
1.7J
ND
F-19
-------
Target Analytes Total [i
1,4-Dichlorobenzene ND
1,2-Dichlorobenzene ND
Benzyl Alcohol 8.3J
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol 23.6
n-Nitrosopyrrolidine ND
Acetophenone 8.8J
Hexachloroethane ND
4-Methylphenol 76.8
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone 41.1
2,4-Dimethylphenol ND
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene 77.3
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene 10.4J
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
F-20
-------
Target Analytes
Acenapthylene 20.4
1,4-Napthoquinone 1.2J
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene 1.1J
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran 3.8J
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene 5.1J
Diethyl pthalate 2.0J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene 16.8J
Anthracene 3.4J
Di-n-butyl pthalate 17.0J
Isodrin ND
Fluoranthene 4.9J
3,3'-Dimethylbenzidine ND
Pyrene 5.4J
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 4.2J
F-21
-------
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene 1.5J
Chrysene 1.8J
di-n-octyl pthalate ND
Benzo (b) fluoranthene 1.5J
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene ND
Benzo (a) pyrene 1.3J
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene ND
Dibenz (a,h) anthracene ND
Benzo (ghi) perylene ND
Tentatively Identified Cmpd ret time (min) Total [i
Unknown 7.14 183.9
Unknown 8.36 87.3
2-Cyclopenten-1-one, 2-meth 9.64 57.8
2-Furancarboxaldehyde,5-me 11.70 69.4
Unknown 11.80 55.5
2Cyclopenten-1-one,2hydrox\ 13.92 95.1
Unknown 16.22 65.5
Phenol,2-methoxy-4-methyl 19.17 72.7
Phenol, 4-ethyl-2-methoxy- 21.62 63.3
HexadecanoicAcid,bis(2ethyl 45.36 57.6
Unknown Pthalate 50.35 70.7
Unknown Pthalate 50.44 110.7
Unknown Pthalate 50.81 55.5
Unknown Pthalate 50.91 58.0
Unknown Pthalate 51.19 55.5
Unknown Pthalate 51.81 53.1
Unknown Pthalate 51.92 70.1
Unknown Pthalate 52.29 56.5
NS = not spiked
j = detected below lowest calibration level
F-22
-------
APPCD Organic Support Laboratory
Household Waste - Semi volatile Analysis
Project:
Sample Id:
Sample Name:
MS Data File:
Method:
Comment:
Field Blank
Household Wastes
Trash #6
Trash Semivol #6
STRASH6B
SW846-Method 8270
Date Acquired:
Date Sampled:
Date Extracted:
Dilution factor:
Analyst:
QC reviewer:
8/30/96
9/12/95
9/20/95
none
Bill Preston
Dennis Tabor
Presampling Surrogates
Percent Recovery (%)
d10-Anthracene
96.4
Post Sampling Surrogates
Percent Recovery (%)
2-Fluorophenol
d5-Phenol
d5-Nitrobenzene
2-Fluorobiphenyl
2,4,6-Tribromophenol
d14-Terphenyl
54.7
76.8
83.6
83.5
70.2
94.0
Target Analytes
Total ug
n-Nitrosomethylethylamine
Methyl Methanesulfonate
n-Nitrosodiethylamine
Bis-(2-Chloroethyl) ether
Ethyl Methanesulfonate
Aniline
Phenol
2-chlorophenol
1,3-Dichlorobenzene
ND
ND
ND
ND
ND
ND
10.2
ND
ND
F-23
-------
Target Analytes Total [i
1,4-Dichlorobenzene ND
1,2-Dichlorobenzene ND
Benzyl Alcohol 2.3J
Bis (2-Chloroisopropyl) ether ND
2-Methylphenol ND
n-Nitrosopyrrolidine ND
Acetophenone ND
Hexachloroethane ND
4-Methylphenol ND
n-Nitrosodi-n-propylamine ND
Nitrobenzene ND
1-Nitrosopiperidine ND
Isophorone ND
2,4-Dimethylphenol ND
Bis (2-chloroethoxy) methane ND
2,4_Dichlorophenol ND
1,2,4-Trichlorobenzene ND
Napthalene ND
2-Nitrophenol ND
2,6-Dichlorophenol ND
Hexachloropropene ND
4-Chloroaniline ND
Hexachlorobutadiene ND
n-Nitrosodi-n-butylamine ND
4-Chloro-3-methyl-phenol ND
2-Methylnapthalene ND
Isosafrole ND
1,2,4,5 Tetrachlorobenzene ND
Hexachlorobutadiene ND
2,4,6-Trichlorophenol ND
2,4,5-Trichlorophenol ND
2-Choronapthalene ND
1,3 Dinitrobenzene ND
2-Nitroaniline ND
3-Nitroaniline ND
Safrole ND
F-24
-------
Target Analytes
Acenapthylene ND
1,4-Napthoquinone ND
Dimethylpthalate ND
2,6-Dinitrotoluene ND
Acenapthene ND
1-Napthylamine ND
2-Napthylamine ND
4-Nitroaniline ND
2,4-Dinitrophenol ND
Dibenzofuran ND
Pentachlorobenzene ND
2,4-Dinitrophenol ND
2,3,4,6-Tetrachlorophenol ND
4-Nitrophenol ND
Fluorene ND
Diethyl pthalate 1.3J
4-Chlorophenyl phenyl ether ND
2-Methyl-4,6-dinitrophenol ND
5-Nitro-o-toluidine ND
Diphenylamine ND
Diallate ND
1,3,5-Trinitrobenzene ND
4-Bronophenyl phenyl ether ND
Phenacetin ND
Hexachlorobenzene ND
4-Aminobiphenyl ND
Dinoseb ND
Pentachlorophenol ND
Pentachloronitrobenzene ND
Phenanthrene ND
Anthracene ND
Di-n-butyl pthalate 3.1J
Isodrin ND
Fluoranthene ND
3,3'-Dimethylbenzidine ND
Pyrene ND
Chlorobenzilate ND
p-Dimethylaminoazobenzene ND
2-Acetylaminofluorene ND
Benzyl butyl pthalate 2.8J
F-25
-------
Target Analytes
3,3'-Dichlorobenzidine ND
Benzo (a) anthracene ND
Chrysene ND
di-n-octyl pthalate ND
Benzo (b) fluoranthene ND
7,12-Dimethylbenz (a) anthracene ND
Benzo (k) fluoranthene ND
Benzo (a) pyrene ND
3-Methylcholanthrene ND
Indeno (1,2,3-cd) pyrene ND
Dibenz (a,h) anthracene ND
Benzo (ghi) perylene ND
Tentatively Identified Cmpc ret time (min) Total [i
Ethyl benzene 8.14 7.9
Xylene isomer(s) 8.45 8.6
Benzaldehyde 11.77 14.1
Cyclotetrasiloxane, octameth 12.41 13.0
Hexanoic acid, 2-ethyl - 17.12 17.9
Unknown Hydrocarbon 25.03 7.9
2,5-Cyclohexadiene-1,4dioni 26.67 8.8
Unknown Hydrocarbon 27.59 8.0
Butylated Hydroxytoluene 27.68 21.2
Phenol, 2,6-bis (1,1-dimethyli 33.58 11.8
Phosphonic acid, dioctadecyl 43.84 7.6
Unknown subst. Hexanedioic 45.39 129.9
(Carbethoxyethylidine) triphe 47.57 40.5
Unknown Phthalate 47.64 63.7
Unknown Phthalate 49.82 11.2
Unknown Phthalate 50.11 9.4
Unknown Phthalate 50.34 10.5
Unknown Phthalate 50.44 203.4
Unknown Phthalate 51.82 31.0
NS = not spiked
j = detected below lowest calibration level
F-26
-------
ALDEHYDES AND KETONES
PQL = Practical Quantitation Limit
N/D = Not Detected
J = Detected @< PQL
N/A = Not Applicable
DL = Diluted Result
NR = Not Required
E = Estimated value
Test#
Sample ID
Analysis Date
formaldehyde
acetaldehyde
acrolein
acetone
propionaldehyde
crotonaldehyde
butyraldehyde
benzaldehyde
isovaleraldehyde
valeraldehyde
o-tolualdehyde
m-tolualdehyde
p-tolualdehyde
hexaldehyde
2, 4 -dimethyl benzaldehyde
1
Avid
Recycler
#4
09/09/95
H9
2.6
1.83
<0.25
4.11
0.63
<0.25
0.43
2.06
<0.25
<0.25
<0.25
<0.25
1.4
<0.25
<0.25
ESTIMATED EMISSIONS OF ALDEHYDES AND
Test#
formaldehyde
acetaldehyde
acrolein
acetone
propionaldehyde
crotonaldehyde
butyraldehyde
benzaldehyde
isovaleraldehyde
valeraldehyde
o-tolualdehyde
m-tolualdehyde
p-tolualdehyde
hexaldehyde
2, 4 -dimethyl benzaldehyde
1
Avid
Recycler
0.0434
0.0305
<0.0042
0.0686
0.0105
<0.0042
0.0072
0.0344
<0.0042
<0.0042
<0.0042
<0.0042
0.0234
<0.0042
<0.0042
2
Avid
Recycler
#5
09/09/95
H9
0.75
0.53
<0.25
2.95
<0.25
<0.25
<0.25
0.38
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
KETONE (g/Kg)
2
Avid
Recycler
0.0112
0.0079
<0.0037
0.0441
<0.0037
<0.0037
<0.0037
0.0057
<0.0037
<0.0037
<0.0037
<0.0037
<0.0037
<0.0037
<0.0037
3
Hut
Blank
#6
09/09/95
pg
<0.25
<0.25
<0.25
3.38
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
3
Hut
Blank
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
NA
4
Non
Recycler
#7
09/09/95
pg
29.5
27.8
2.56
14.9
7.63
3.22
<0.25
8.41
0.98
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
4
Non
Recycler
1.229
1.1581
0.1066
0.6207
0.3179
0.1341
<0.0104
0.3504
0.0408
<0.0104
<0.0104
<0.0104
<0.0104
<0.0104
<0.0104
5
Non
Recycler
#8
5\2\96
pg
13.2
13.9
<0.25
7.57
3.28
<0.25
<0.25
5.85
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
<0.25
5
Non
Recycler
0.491
0.5171
<0.0093
0.2816
0.122
<0.0093
<0.0093
0.2176
<0.0093
<0.0093
<0.0093
<0.0093
<0.0093
<0.0093
<0.0093
F-27
-------
ESTIMATED
HCI data
Test
No.
1
2
3
4
5
ESTIMATED
Test
No.
1
2
3
4
5
HCI EMISSIONS (g/Kg)
Test Conditions DATE
Avid Recycler 8/30/95
Avid Recycler 9/1/95
Hut Blank 9/6/95
Non Recycler 9/8/95
Non Recycler 9/12/95
HCN EMISSIONS (g/Kg)
Test Conditions DATE
Avid Recycler 8/30/95
Avid Recycler 9/1/95
Hut Blank 9/6/95
Non Recycler 9/8/95
Non Recycler 9/12/95
ug HCI
550
260
4.7
22
6.3
ug HCN
33.7125
24.7953
-0.6284
32.8109
14.9944
Mass burnned
Kg
8.1
8.8
0
2.6
3.9
Mass burnned
Kg
8.1
8.8
0
2.6
3.9
Vm,std
2.426
2.512
2.615
1.691
2.7
Vm,std
CUFT
2.0483
2.2362
2.5447
1.6688
2.6648
HCI cone.
mg/M3
8.006
3.655
0.063
0.459
0.082
HCN cone.
mg/M3
0.5812
0.3915
-0.0087
0.6943
0.1987
Estimated
HCI Emissions
g/kg
3.281
1.508
NA
0.4814
0.08636
Estimated
HCN Emissions
g/kg
0.2382
0.1615
na
0.7277
0.2083
F-28
-------
PARTICULATE DATA
Test
No.
1
2
3
4
5
Test
No.
1
2
3
4
5
Test
No.
1
2
3
4
5
Test
No.
1
2
3
4
5
Test
No.
1
2
3
4
5
Test
No.
1
2
3
4
5
Test Condi
Avid Recy
Avid Recy
Hut Blank
Non Recyc
Non Recyc
final Pa
INHg
29.68
29.36
29.69
29.47
29.82
Final Wt
mg
16.99
9.57
0.05
16.21
18.08
final T
K
308.2
304.7
302.4
301.9
301.9
coarse
Qstd
1.77
.1-77
1.79
1.78
1.79
fine(PM-2;
Concentrat
ug/mA3
1.581e+4
8682.579
39.386
1.914e+4
1.411e+4
DATE
8/30/95
9/1/95
9/6/95
9/8/95
9/12/95
final T
deg. C
35.2
31.7
29.4
28.9
28.9
Run Time
minutes
77
79
90
60
90
Seas avg
mm Hg
753.872
745.744
754.126
748.538
757.428
initial
total Qa
16.38
16.38
16.27
16.24
16.14
coarse
Catch
ug
3620
3010
30
3150
4250
RUN #
1
2
3
4
5
Seas avg
in Hg
29.68
29.36
29.69
29.47
29.82
equation
coarse m
2.3675
2.3675
2.3675
2.3675
2.3675
Seas avg
K
308.1
304.7
302.7
300.5
299.95
final
total Qa
16.39
16.38
16.26
16.3
16.22
coarse(2.£
Concentrat
ug/mA3
1209.67
1445.58
16.55
1157.02
1368.62
coarse rot
initial
7
7
7
7
7
Seas avg
deg. C
35.1
31.7
29.7
27.5
26.95
equation
coarse b
0.10647
0.10647
0.10647
0.10647
0.10647
SAMPLER
ID
1
2
3
4
5
total
Qavg
16.39
16.38
16.27
16.27
16.18
total(PM-1
Volume
(m3, STP)
1.21
1.242
1.43
0.953
1.442
total rot
initial
23
23
23
23
23
coarse
filter #
4
6
7
10
12
equation
total m
1.13214
1.13214
1.13214
1.13214
1.13214
DATE
30-Aug-9J
1-Sep-95
6-Sep-95
8-Sep-95
12-Sep-9£
total
Qstd
15.72
15.72
15.89
15.89
16.02
total (PM-1
Concentrat
ug/mA3
17027
10128
56
20305
15485
initial Pa
IN Hg
29.68
29.36
29.69
29.47
29.82
Tare Wt
mg
0
0
0
0
0
equation
total b
-3.8465
-3.8465
-3.8465
-3.8465
-3.8465
RUN #
1
2
3
4
5
fine
Qavg
14.54
14.54
14.44
14.45
14.37
Concentrat
PM 2.5
mg/m3
15.82
8.68
0.04
19.15
14.12
initial T
deg. C
35
31.7
30
26.1
25
Final Wt
mg
3.62
3.01
0.03
3.15
4.25
initial Pa
mm Hg
753.872
745.744
754.126
748.538
757.428
initial
coarse Qa
1.84
1.84
1.83
1.82
1.81
fine
Qstd
13.95
13.95
14.11
14.11
14.23
Concentrat
PM 10
mg/m3
17.03
10.13
0.06
20.31
15.49
coarse rot
final
7
7
7
7
7
fine
filter #
3
5
8
9
11
initial T
K
308
304.7
303
299.1
298
final
coarse Qa
1.84
1.84
1.83
1.82
1.81
fine(PM-2.5)
Volume
(m3, STP)
1.074
1.102
1.269
0.847
1.281
Estimated
Emis. PM 2.5
g/kg
6.93
3.58
N/A
20.07
14.8
Tot rot
final
23
23
23
23
23
Tare Wt
mg
0
0
0
0
0
final Pa
mm Hg
753.872
745.744
754.126
748.538
757.428
coarse
Qavg
1.84
1.84
1.83
1.82
1.81
fine
Catch
ug
16990
9570
50
16210
18080
Estimated
Emis. PM 10
g/kg
7.46
4.18
N/A
21.28
16.23
F-29
-------
APPENDIX G. WCL&R RAW ANALYTICAL DATA
CHLOROBENZENES(SIM)
CHLOROBENZENES(SIM)
Raw Data
1,3
1,4
1,2
1,3,5
1,2,4
1,2,3
1,2,3,5
1,2,4,5
1,2,3,4
1,2,3,4,5
1,2,3,4,5,6
TOT
TOT
TOT
TOT
TOT
Data Corrected b>>
1,3
1 ,4
1,2
1,3,5
1,2,4
1,2,3
1,2,3,5
1,2,4,5
1,2,3,4
1,2,3,4,5
1,2,3,4,5,6
TOT
TOT
TOT
TOT
TOT
RunName:
Ace. Num.:
Units:
Dichlorobenzene
Dichlorobenzene
Dichlorobenzene
Trichlorobenzene
Trichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
Dichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
Dilution Factor (DF=10)
RunName:
Ace. Num.:
Units:
Dichlorobenzene
Dichlorobenzene
Dichlorobenzene
Trichlorobenzene
Trichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
Dichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
NYS-DOH Analyses
SIM Chlorobenzenes Estimated Emissions mg/Kg
(taken from #'s corrected for dilution factor)
1,3
1,4
1,2
1,3,5
1,2,4
1,2,3
1,2,3,5
1,2,4,5
1,2,3,4
1,2,3,4,5
1,2,3,4,5,6
TOT
TOT
TOT
TOT
TOT
RunName:
Ace. Num.:
Units:
Dichlorobenzene
Dichlorobenzene
Dichlorobenzene
Trichlorobenzene
Trichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
Dichlorobenzene
Trichlorobenzene
Tetrachlorobenzene
Pentachlorobenzene
Hexachlorobenzene
Run 1
Avid
Recycler
S1109J
9582042
mg/kg
0.016
0.0067
0.051
0.002
0.0339
0.0477
0.0107
0.0109
0.0393
0.0371
0.0345
0.0643
0.1001
0.051
0.0371
0.0345
Run 1
Avid
Recycler
S1109J
9582042
pig
4091.515
1714.85
13055.74
522.4778
8675.252
12209.78
2724.627
2795.489
10052.11
9489.454
8837.573
16438.94
25614.15
13047.61
9489.454
8837.573
Run 1
Avid
Recycler
S1109J
9582042
pig
40915.15
17148.5
130557.4
5224.778
86752.52
122097.8
27246.27
27954.89
100521.1
94894.54
88375.73
164389.4
256141.5
130476.1
94894.54
88375.73
Run 2
Avid
Recycler
S1109H
9582043
mg/kg
0.2448
0.0919
0.3365
0.0298
0.2575
0.3057
0.0788
0.0411
0.163
0.1622
0.0625
0.5666
0.7048
0.2318
0.1622
0.0625
detection
limit
522.697
356.6881
390.2794
286.9338
397.7631
299.52
206.6413
146.0564
176.3292
151.5241
179.5857
356.6881
397.7631
146.0564
151.5241
179.5857
detection
limit
5226.97
3566.881
3902.794
2869.338
3977.631
2995.2
2066.413
1460.564
1763.292
1515.241
1795.857
3566.881
3977.631
1460.564
1515.241
1795.857
Run 3
Hut
Blank
S1109F
9582044
mg/kg
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
%
recovery
80.99012
80.99012
80.99012
72.70316
72.70316
72.70316
84.59205
84.59205
84.59205
85.66898
77.47478
80.99012
72.70316
84.59205
85.66898
77.47478
%
recovery
Run 4
Non
Recycler
S1109I
9582045
mg/kg
0.0076
0.0032
0.1074
<0.0077
0.0468
0.0457
0.0197
0.0277
0.0686
0.0727
0.0309
0.1065
0.1074
0.0985
0.0727
0.0309
Run 5
Non
Recycler
S1109G
9582046
mg/kg
0.0596
0.0313
0.1616
0.0042
0.0519
0.0452
0.0117
0.0121
0.0342
0.0331
0.0131
0.2196
0.1178
0.0487
0.0331
0.0131
Run 2
Avid
Recycler
S1109H
9582043
pig
68961.05
25897.91
94790.55
8395.963
72540.66
86094.88
22182.83
11588.96
45910.47
45681.51
17595.26
159588.8
198513.8
65296.43
45681.51
17595.26
Run 2
Avid
Recycler
S1109H
9582043
pig
689610.5
258979.1
947905.5
83959.63
725406.6
860948.8
221828.3
115889.6
459104.7
456815.1
175952.6
1595888
1985138
652964.3
456815.1
175952.6
Field
Blank
S1109E
9582047
mg/kg
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
detection
limit
459.3976
313.4927
343.016
253.0192
350.7488
264.1177
183.4277
129.6487
156.5208
134.7458
160.111
313.4927
350.7488
129.6487
134.7458
160.111
detection
limit
4593.976
3134.927
3430.16
2530.192
3507.488
2641.177
1834.277
1296.487
1565.208
1347.458
1601.11
3134.927
3507.488
1296.487
1347.458
1601.11
%
recovery
92.14957
92.14957
92.14957
82.44824
82.44824
82.44824
95.29755
95.29755
95.29755
96.33631
86.8982
92.14957
82.44824
95.29755
96.33631
86.8982
%
recovery
from semi-v
Test #
1
2
3
4
5
-------
CHLOROBENZENES(SIM)
Run 3
Hut
Blank
S1109F
9582044
pig
0
1646.161
7098.595
0
319.1828
213.3781
0
447.5452
1359.607
0
0
8133.782
602.5493
1573.729
0
0
Run 3
Hut
Blank
S1109F
9582044
piq
0
16461.61
70985.95
0
3191.828
2133.781
0
4475.452
13596.07
0
0
81337.82
6025.493
15737.29
0
0
)l worksheet
Tm,l
deqF
93.0000
88.0000
86.0000
85.0000
71.0000
detection
limit
505.2492
344.7818
377.2517
271.6796
376.6168
283.5966
196.7343
139.054
167.8755
145.9244
175.1753
344.7818
376.6168
139.054
145.9244
175.1753
detection
limit
5052.492
3447.818
3772.517
2716.796
3766.168
2835.966
1967.343
1390.54
1678.755
1459.244
1751.753
3447.818
3766.168
1390.54
1459.244
1751.753
Tm,f
deqF
110.0000
104.0000
102.0000
96.0000
93.0000
%
recovery
83.78694
83.78694
83.78694
76.78528
76.78528
76.78528
88.85189
88.85189
88.85189
88.95647
79.42537
83.78694
76.78528
88.85189
88.95647
79.42537
%
recovery
Tm,avq
deqF
101.5000
96.0000
94.0000
90.5000
82.0000
Pbar
in Hq
29.6800
29.3600
29.6900
29.4700
29.8200
Run 4
Non
Recycler
S1109I
9582045
piq
618.9072
259.3512
8702.19
0
3790.352
3702.182
1595.473
2248.007
5563.909
5891.054
2503.031
8634.888
8706.856
7984.38
5891.054
2503.031
Run 4
Non
Recycler
S1109I
9582045
piq
6189.072
2593.512
87021.9
0
37903.52
37021.82
15954.73
22480.07
55639.09
58910.54
25030.31
86348.88
87068.56
79843.8
58910.54
25030.31
dH
N/A
N/A
N/A
N/A
N/A
detection
limit
1180.67
805.6887
881.5646
624.085
865.1401
651.46
486.2616
343.6951
414.9322
366.4252
427.2697
805.6887
865.1401
343.6951
366.4252
427.2697
detection
limit
11806.7
8056.887
8815.646
6240.85
8651.401
6514.6
4862.616
3436.951
4149.322
3664.252
4272.697
8056.887
8651.401
3436.951
3664.252
4272.697
DGM.i
657.996
698.305
742.676
792.224
824.043
%
recovery
35.85531
35.85531
35.85531
33.42653
33.42653
33.42653
35.94816
35.94816
35.94816
35.42583
32.56342
35.85531
33.42653
35.94816
35.42583
32.56342
%
recovery
DGM.f
698.142
742.578
792.023
823.987
871.218
Vm
ft3
40.146
44.273
49.347
31.763
47.175
Run 5
Non
Recycler
S1109G
9582046
piq
6609.231
3470.189
17928.3
470.3578
5758.157
5013.621
1301.565
1344.071
3795.367
3676.073
1457.453
24365.55
13068.29
5407.796
3676.073
1457.453
Run 5
Non
Recycler
S1109G
9582046
piq
66092.31
34701.89
179283
4703.578
57581.57
50136.21
13015.65
13440.71
37953.67
36760.73
14574.53
243655.5
130682.9
54077.96
36760.73
14574.53
Run Time
min
72.0000
79.0000
60.0000
60.0000
90.0000
detection
limit
485.7693
331.4887
362.7068
266.0395
368.7982
277.7091
182.6475
129.0973
155.8551
135.291
158.6534
331.4887
368.7982
129.0973
135.291
158.6534
detection
limit
4857.693
3314.887
3627.068
2660.395
3687.982
2777.091
1826.475
1290.973
1558.551
1352.91
1586.534
3314.887
3687.982
1290.973
1352.91
1586.534
%
recovery
87.1469
87.1469
87.1469
78.41315
78.41315
78.41315
95.70461
95.70461
95.70461
95.94813
87.69661
87.1469
78.41315
95.70461
95.94813
87.69661
%
recovery
Air into hut
M3
45949
45949
45949
45949
45949
Vlass Burnnec
Ib
17.6000
19.3000
N/A
5.8000
7.8000
Field
Blank
S1109E
9582047
piq
0
0
7378.773
0
318.4678
259.907
0
603.9728
1760.061
1506.002
0
6743.684
663.6247
2061.86
1506.002
0
Field
Blank
S1109E
9582047
piq
0
0
73787.73
0
3184.678
2599.07
0
6039.728
17600.61
15060.02
0
67436.84
6636.247
20618.6
15060.02
0
Mass burnned
Kq
8.0
8.8
N/A
2.6
3.5
detection
limit
436.5846
297.9251
325.9823
240.6586
333.6139
251.2149
177.3234
125.3342
151.312
128.1072
152.1533
297.9251
333.6139
125.3342
128.1072
152.1533
detection
limit
4365.846
2979.251
3259.823
2406.586
3336.139
2512.149
1773.234
1253.342
1513.12
1281.072
1521.533
2979.251
3336.139
1253.342
1281.072
1521.533
Vmstd
cu ft std
37.4330
41.2400
46.6509
29.9946
45.7845
-------
_ NYSfDOH Analyses
-Full Scan Semivolatiles
-------
Endrm aldehyde
OCTACQSANE
DOTRIACONTANE
HEXATRIACONfTANE
TETRACQNTAHE
NYS DOH Analys
Estimated Emiss
-------
TETRADECANE
OCTADECANE
TETRACOSANE
DOTRIACONTANE
HEXATRIACQNTAHE
TETRACONTANE
-------
PAH's(SIM)
PAH's(SIM)
Raw Data
RunName:
Ace. Num.:
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(123cd)pyrene
Dibenzo(ah) anthracene
Benzo(qhi)perylene
Data Corrected by Dilution Factor (DF=100)
RunName:
Ace. Num.:
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(123cd)pyrene
Dibenzo(ah) anthracene
Benzo(qhi)perylene
NYS DOH Analyses - SIM PAHs
Estimated PAH Emissions mq/Kq
(taken from #'s corrected by dilution factor)
RunName:
Ace. Num.:
Units:
Naphthalene
Acenaphthylene
Acenaphthene
Fluorene
Phenanthrene
Anthracene
Fluoranthene
Pyrene
Benzo(a)anthracene
Chrysene
Benzo(b)fluoranthene
Benzo(k)fluoranthene
Benzo(a)pyrene
lndeno(123cd)pyrene
Dibenzo(ah) anthracene
Benzo(qhi)perylene
Run 1
Avid
Recycler
S1115E
9582042
mq/kq
4.0279
2.7065
0.2394
1.4757
2.8379
0.6066
1.4921
1.6695
1.1356
1.6461
1.6200
0.5209
1.1234
1.0391
0.3795
0.9877
Run 1
Avid
Recycler
S1115E
9582042
PG
103039
69235.87
6125.239
37749.99
72597.59
15516.37
38168.81
42709.07
29049.77
42109
41441.33
13326.17
28737.18
26582.8
9707.446
25267.07
Run 1
Avid
Recycler
S1115E
9582042
PG
10303900
6923587
612523.9
3774999
7259759
1551637
3816881
4270907
2904977
4210900
4144133
1332617
2873718
2658280
970744.6
2526707
Run 2
Avid
Recycler
S1115C
9582043
mq/kq
6.3651
4.0440
0.7793
3.1838
3.8527
0.9337
1.4626
1.3768
0.4294
0.4644
0.5407
0.1238
0.2385
0.2981
0.0675
0.2811
detection
limit
10.86434
10.19921
17.03119
13.39614
8.332902
5.634816
5.980981
5.74234
4.96437
5.81791
5.542581
5.668317
5.579842
5.651843
5.209414
5.911573
detection
limit
1086.434
1019.921
1703.119
1339.614
833.2902
563.4816
598.0981
574.234
496.437
581.791
554.2581
566.8317
557.9842
565.1843
520.9414
591.1573
Run 3
Hut
Blank
S1115A
9582044
mq/kq
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
%
recovery
182.2631
102.3762
93.2366
86.51323
83.45888
124.0761
79.06458
79.85149
87.72358
75.36241
75.62285
73.48492
86.93133
70.77049
72.90847
64.94457
%
recovery
Run 4
Avid
Recycler
S1115D
9582045
mq/kq
18.9598
13.6424
0.9578
4.7756
8.9946
2.3724
5.1917
6.1419
3.1364
3.5588
3.7585
1.6424
3.1275
2.7997
0.4861
2.8148
Run 5
Non
Recycler
S1115B
9582046
mq/kq
16.1032
8.9577
0.5780
2.5360
5.6546
1.2910
2.9436
3.5157
1.3425
1.5136
1.5016
0.4085
1.1167
0.9547
0.1595
1.1340
Run 2
Avid
Recycler
S1115C
9582043
PG
179284.3
113907.5
21950.55
89677.34
108517.2
26298.6
41195.95
38780.1
12095.87
13080.26
15229
3488.019
6717.77
8396.619
1901.785
7916.835
Run 2
Avid
Recycler
S1115C
9582043
PG
17928430
11390750
2195055
8967734
10851720
2629860
4119595
3878010
1209587
1308026
1522900
348801.9
671777
839661.9
190178.5
791683.5
detection
limit
11.01419
12.12625
17.89212
13.98332
10.21779
6.398817
7.572286
7.27887
7.346935
7.086832
6.831847
6.715067
6.558836
6.000705
5.825322
5.654373
detection
limit
1101.419
1212.625
1789.212
1398.332
1021.779
639.8817
757.2286
727.887
734.6935
708.6832
683.1847
671.5067
655.8836
600.0705
582.5322
565.4373
%
recovery
179.7833
86.10712
88.75028
82.88044
68.06311
109.2617
62.44929
62.99527
59.27538
61.86851
61.35175
62.03003
73.95567
66.65612
65.1999
67.8987
%
recovery
Test #
1
2
3
4
5
Tm,1
deq F
93.0000
88.0000
86.0000
85.0000
71.0000
-------
PAH's(SIM)
Run 3
Hut
Blank
S1115A
9582044
PG
8132.516
1158.149
670.1941
2081.133
7357.299
335.6656
1566.539
1 1 48.146
117.3241
173.4325
58.24945
16.05725
26.36956
46.29071
0
267.2384
Run 3
Hut
Blank
S1115A
9582044
PG
813251.6
115814.9
67019.41
208113.3
735729.9
33566.56
156653.9
114814.6
11732.41
17343.25
5824.945
1605.725
2636.956
4629.071
0
26723.84
Tmf
deq F
110.0000
104.0000
102.0000
96.0000
93.0000
detection
limit
14.19539
10.78083
17.68765
13.94055
8.842547
5.81766
6.401401
4.836822
6.043521
6.156858
5.982893
5.639664
5.689225
5.063799
4.953957
4.661927
detection
limit
1419.539
1078.083
1768.765
1394.055
884.2547
581.766
640.1401
483.6822
604.3521
615.6858
598.2893
563.9664
568.9225
506.3799
495.3957
466.1927
Tmavq
deq F
101.5000
96.0000
94.0000
90.5000
82.0000
%
recovery
139.4938
96.85303
89.77621
83.13468
78.6487
120.1765
73.87193
94.80076
72.05939
71.21357
70.05737
73.85826
85.25995
78.98887
76.66808
82.3532
%
recovery
Pbar
in Hq
29.6800
29.3600
29.6900
29.4700
29.8200
dH
N/A
N/A
N/A
N/A
N/A
Run 4
Avid
Recycler
S1115D
9582045
PG
153689
110585.8
7763.678
38710.82
72910.56
19230.88
42083.73
49786.78
25423.57
28847.89
30466.48
13313.24
25351.24
22694.28
3940.652
22817.06
Run 4
Avid
Recycler
S1115D
9582045
PG
15368900
11058580
776367.8
3871082
7291056
1923088
4208373
4978678
2542357
2884789
3046648
1331324
2535124
2269428
394065.2
2281706
DGM.i
657.996
698.305
742.676
792.224
824.043
detection
limit
15.04103
11.4754
11.20832
8.961942
7.553902
5.064929
6.982581
7.510361
7.080887
7.381904
6.996623
6.787716
6.670903
6.412132
6.172674
6.221316
detection
limit
1504.103
1147.54
1120.832
896.1942
755.3902
506.4929
698.2581
751.0361
708.0887
738.1904
699.6623
678.7716
667.0903
641.2132
617.2674
622.1316
DGM.f
698.142
742.578
792.023
823.987
871.218
%
recovery
131.6511
90.99087
141 .6743
129.3183
92.06563
138.0367
67.72336
61.05357
61.50251
59.39549
59.90688
61.36613
72.71326
62.37921
61.53093
61.71115
%
recovery
Vm
ft3
40.146
44.273
49.347
31.763
47.175
Run Time
min
72.0000
79.0000
60.0000
60.0000
90.0000
Run 5
Non
Recycler
S1115B
9582046
PG
178637
99369.93
6411.987
28132.17
62728.27
14320.92
32654.52
39000.41
14893.17
16791.04
16657.49
4531.346
12388.18
10591
1769.718
12580.29
Run 5
Non
Recycler
S1115B
9582046
PG
17863700
9936993
641198.7
2813217
6272827
1432092
3265452
3900041
1489317
1679104
1665749
453134.6
1238818
1059100
176971.8
1258029
detection
limit
12.94158
11.43486
12.00363
8.859126
7.274786
5.223923
6.655731
6.808775
6.767602
6.525594
6.374431
6.244509
6.273292
5.879669
5.665074
5.496382
detection
limit
1294.158
1143.486
1200.363
885.9126
727.4786
522.3923
665.5731
680.8775
676.7602
652.5594
637.4431
624.4509
627.3292
587.9669
566.5074
549.6382
Air into hut
M3
45949
45949
45949
45949
45949
%
recovery
153.0082
91.31342
132.2876
130.8192
95.59795
133.8354
71.04911
67.34461
64.34959
67.18956
65.75423
66.70433
77.32193
68.02828
67.04421
69.85042
%
recovery
i/lass Burnnec
Ib
17.6000
19.3000
N/A
5.8000
7.8000
Mass burnne
Kq
8.0
8.8
N/A
2.6
3.5
Vm.std
cu ft std
37.4330
41.2400
46.6509
29.9946
45.7845
-------
DIOXINS&FURANS
DIOXINS
Raw Data
2,3,7,8
1,2,3,7,8
1,2,3,4,7,8
1,2,3,6,7,8
1,2,3,7,8,9
1,2,3,4,6,7,8
1,2,3,4,6,7,8,9
2,3,7,8
1,2,3,7,8
2,3,4,7,8
1,2,3,4,7,8
1,2,3,6,7,8
2,3,4,6,7,8
1,2,3,7,8,9
1,2,3,4,6,7,8
1,2,3,4,7,8,9
1,2,3,4,6,7,8,9
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
RunName:
Ace. Num.:
Units:
TCDD
PCDD
HXCDD
HXCDD
HXCDD
HPCDD
CCDD
TCDF
PCDF
PCDF
HXCDF
HXCDF
HXCDF
HXCDF
HPCDF
HPCDF
CCDF
TCDD
PCDD
HXCDD
HPCDD
CCDD
TCDF
PCDF
HXCDF
HPCDF
CCDF
Dioxins Estimated Emissions mg/
2,3,7,8
1,2,3,7,8
1,2,3,4,7,8
1,2,3,6,7,8
1,2,3,7,8,9
1,2,3,4,6,7,8
1,2,3,4,6,7,8,9
2,3,7,8
1,2,3,7,8
2,3,4,7,8
1,2,3,4,7,8
1,2,3,6,7,8
2,3,4,6,7,8
1,2,3,7,8,9
1,2,3,4,6,7,8
1,2,3,4,7,8,9
1,2,3,4,6,7,8,9
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
TOT
RunName:
Ace. Num.:
Units:
TCDD
PCDD
HXCDD
HXCDD
HXCDD
HPCDD
CCDD
TCDF
PCDF
PCDF
HXCDF
HXCDF
HXCDF
HXCDF
HPCDF
HPCDF
CCDF
TCDD
PCDD
HXCDD
HPCDD
CCDD
TCDF
PCDF
HXCDF
HPCDF
CCDF
-------
DIOXINS&FURANS
detection
limit
547.8298
524.1453
326.2867
721.6475
665.0846
914.0431
1093.724
564.0241
416.0442
279.8903
161.2787
429.0861
508.4325
474.1448
589.3259
292.0344
984.812
547.8298
524.1453
777.3826
914.0431
1093.724
564.0241
416.0442
432.9395
589.3259
984.812
%
recovery
32.93007
32.28075
64.99279
27.27908
27.27908
26.56907
26.56907
28.73859
36.2672
58.86966
74.94148
27.91722
27.91722
27.91722
26.86749
58.12655
26.56907
32.93007
32.28075
27.27908
26.56907
26.56907
28.73859
36.2672
27.91722
26.86749
26.56907
Run 4
Non
Recycler
S1201B
9582051
FG
0
0
0
0
0
0
36206.25
81.4449
90.38368
189.4431
94.15799
137.1508
109.5357
0
200.8506
0
0
0
0
0
0
36206.25
3053.077
1926.789
890.4613
200.8506
0
detection
limit
247.3892
255.5139
343.4269
452.0172
416.588
509.4293
609.5718
235.3899
209.4154
273.0515
168.9539
274.7962
325.6114
303.6528
320.8476
364.1525
548.8713
247.3892
255.5139
486.9279
509.4293
609.5718
235.3899
209.4154
277.2641
320.8476
548.8713
%
recovery
79.76701
72.43469
67.54543
47.63932
47.63932
52.14645
52.14645
75.32534
78.81535
66.0086
78.25227
47.68387
47.68387
47.68387
53.9821
50.9907
52.14645
79.76701
72.43469
47.63932
52.14645
52.14645
75.32534
78.81535
47.68387
53.9821
52.14645
Run 5
Non
Recycler
S1204A
9582052
FG
0
0
0
0
0
0
35320.14
0
0
0
83.76806
0
0
0
3798.874
0
0
0
0
0
0
35320.14
781.3995
0
609.0528
3798.874
0
detection
limit
290.2659
300.8679
355.1034
518.0936
477.4853
596.4506
713.6996
288.8616
247.0053
282.8823
192.9251
310.7979
368.2706
343.4352
3756.798
379.0972
642.6303
290.2659
300.8679
558.1075
596.4506
713.6996
288.8616
247.0053
313.5891
3756.798
642.6303
%
recovery
58.95879
53.34893
56.65209
36.04564
36.04564
38.62555
38.62555
53.23284
57.95001
55.25605
59.43153
36.56324
36.56324
36.56324
3.998261
42.47801
38.62555
58.95879
53.34893
36.04564
38.62555
38.62555
53.23284
57.95001
36.56324
3.998261
38.62555
-------
Estimated PCB Emissions
Raw Data
COMPOUND
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-1 9 (2,2',6-TRICHLOROBIPHENYL)
BZ-1 2 (3,4-DICHLOROBIPHENYL) (Surrogate)
BZ-1 8 (2,2',5-TRICHLOROBIPHENYL)
BZ-1 5, BZ-1 7
BZ-24, BZ-27
BZ-1 6, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-4 7 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,5'-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, DCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,5'-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-1 1 9 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-1 15
BZ-85, 4,4'-DDE
BZ-1 36
BZ-77, BZ-1 10
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-1 51 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-1 35
BZ-1 07 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-1 23, BZ-1 49
BZ-1 18
BZ-1 34
BZ-1 22 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-1 46
BZ-1 53
BZ-132, BZ-105
BZ-1 41 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-1 79
BZ-1 37
BZ-1 30, BZ-1 76
BZ-1 38
BZ-1 58
BZ-1 29
BZ-1 78
BZ-1 75
BZ-1 87
BZ-1 83
BZ-1 28
BZ-1 67
Run 1
Avid
Recycler
9582048
ng
47.0000
580.0000
2.0000
0.4000
0.4000
31.0000
12.0000
0.4000
330.0000
INTERFER
INTERFER
54.0000
18.0000
68.0000
1 1 .0000
5.6000
17.0000
0.4000
33.0000
1 1 .0000
35.0000
1 1 .0000
19.0000
64.0000
12.0000
0.4000
50.0000
0.4000
340.0000
0.4000
16.0000
INTERFER
24.0000
2.2000
0.4000
13.0000
9.3000
10.0000
12.0000
8.0000
1 1 .0000
4.0000
3.2000
6.0000
21.0000
0.4000
10.0000
7.2000
0.4000
1 1 .0000
3.1000
14.0000
0.4000
16.0000
18.0000
0.4000
39.0000
21.0000
1 1 .0000
4.3000
6.4000
10.0000
15.3000
7.4000
0.4000
0.4000
0.4000
12.0000
3.0000
0.4000
12.0000
1 1 .0000
0.4000
5.7000
5.3000
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
Run 2
Avid
Recycler
9582049
ng
21.0000
2.0000
76.0000
0.4000
0.4000
33.0000
22.0000
0.4000
65.0000
0.4000
INTERFER
INTERFER
26.0000
23.0000
26.0000
0.4000
12.0000
0.4000
41.3000
16.0000
33.0000
7.9000
15.0000
INTERFER
INTERFER
0.4000
31.0000
0.4000
INTERFER
0.4000
14.0000
0.4000
10.0000
1.4000
1.3000
0.4000
5.0000
9.2000
10.0000
4.0000
7.4000
2.4000
2.5000
4.8000
1 7.0000
0.4000
8.0000
3.5000
0.4000
5.0000
1.3000
10.0000
5.6000
12.0000
2.1000
0.4000
22.0000
11.0000
0.4000
0.4000
3.4000
2.9000
3.5000
4.0000
0.4000
0.4000
0.4000
5.7000
0.4000
1.1000
0.7000
0.4000
9.9000
2.5000
1.5000
LT
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
Run 3
Hut
Blank
9582050
ng
2.0000
2.0000
2.0000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
INTERFER
INTERFER
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
1.6000
0.4000
0.4000
0.4000
0.4000
INTERFER
INTERFER
0.4000
1.0000
1.2000
0.4000
0.4000
INTERFER
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.9000
1.6000
0.4000
1.5000
0.4000
0.4000
0.8000
0.4000
0.4000
0.4000
0.4000
0.4000
1.1000
0.4000
1.0000
0.4000
0.4000
0.4000
0.4000
0.7000
0.7000
0.4000
0.4000
0.4000
INTERFER
0.7000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
LT
LT
LT
Run 4
Non
Recycler
9582051
ng
33.0000
2.0000
68.0000
0.4000
0.8000
52.0000
0.4000
0.4000
0.4000
0.4000
0.4000
60.0000
32.0000
17.0000
28.0000
0.4000
15.0000
0.4000
62.0000
0.4000
30.0000
0.4000
24.0000
76.0000
INTERFER
0.4000
28.0000
0.4000
0.4000
0.4000
9.0000
31.0000
0.4000
2.4000
8.0000
0.4000
2.5000
5.4000
11.0000
8.6000
5.1000
1.7000
3.9000
4.2000
16.0000
0.4000
4.4000
2.1000
0.4000
5.4000
0.4000
7.5000
0.4000
8.2000
4.0000
0.4000
15.0000
6.7000
0.4000
0.4000
2.4000
INTERFER
4.8000
2.6000
0.4000
0.4000
0.4000
6.0000
0.4000
0.4000
0.4000
0.4000
7.2000
2.6000
0.4000
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
LT
Run 5
Non
Recycler
9582052
ng
150.0000
2.0000
160.0000
0.4000
3.0000
110.0000
43.0000
0.4000
50.0000
13.0000
17.0000
81.0000
43.0000
0.4000
50.0000
0.4000
36.0000
0.4000
72.0000
48.0000
66.0000
0.4000
60.0000
160.0000
24.0000
0.4000
87.0000
0.4000
INTERFER
INTERFER
23.0000
INTERFER
54.0000
3.9000
0.4000
0.4000
9.8000
1 1 .0000
23.0000
4.6000
8.1000
3.5000
9.3000
12.0000
21.0000
0.4000
2.1000
6.2000
0.4000
1 1 .0000
3.2000
17.0000
7.3000
20.0000
5.0000
0.4000
32.0000
16.0000
7.3000
0.4000
4.0000
12.0000
5.5000
4.4000
1.8000
0.4000
0.4000
8.9000
1.4000
0.4000
5.1000
20.0000
6.6000
0.4000
4.3000
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
-------
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209 (DECACHLOROBIPHENYL) (Surrogate)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
Estimated emissions mq/Kq
COMPOUND
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surroqate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-1 9 (2,2',6-TRICHLOROBIPHENYL)
BZ-1 2 (3,4-DICHLOROBIPHENYL) (Surroqate)
BZ-1 8 (2,2',5-TRICHLOROBIPHENYL)
BZ-1 5, BZ-1 7
BZ-24, BZ-27
BZ-1 6, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-4 7 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,5'-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, DCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,5'-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-1 1 9 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-1 15
BZ-85, 4,4'-DDE
BZ-1 36
BZ-77, BZ-1 10
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
0.4000
6.5000
5.8000
INTERFER
6.8000
0.4000
4.5000
2.9000
31.0000
0.4000
5.0000
0.4000
INTERFER
0.4000
5.9000
9.7000
1 1 .0000
7.8000
INTERFER
INTERFER
3.7000
464.0000
905.0000
1090.0000
Run 1
Avid
Recyder
9582048
mq/kq
0.0185
0.2288
0.0008
0.0002
0.0002
0.0122
0.0047
0.0002
0.1302
interfer
interfer
0.0213
0.0071
0.0268
0.0043
0.0022
0.0067
0.0002
0.0130
0.0043
0.0138
0.0043
0.0075
0.0253
0.0047
0.0002
0.0197
0.0002
0.1342
0.0002
0.0063
interfer
0.0095
0.0009
0.0002
0.0051
0.0037
0.0039
0.0047
0.0032
0.0043
0.0016
0.0013
0.0024
0.0083
0.0002
0.0039
0.0028
0.0002
0.0043
0.0012
0.0055
0.0002
LT
LT
LT
LT
LT
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
0.4000
4.5000
1.9000
INTERFER
0.4000
0.4000
0.4000
1.2000
0.4000
0.4000
1.8000
0.4000
INTERFER
8.0000
2.0000
0.4000
0.4000
1.1000
INTERFER
0.4000
2.7000
450.0000
950.0000
1150.0000
Run 2
Avid
Recycler
9582049
mq/Kq
0.0077
0.0007
0.0280
0.0001
0.0001
0.0121
0.0081
0.0001
0.0239
0.0001
interfer
interfer
0.0096
0.0085
0.0096
0.0001
0.0044
0.0001
0.0152
0.0059
0.0121
0.0029
0.0055
interfer
interfer
0.0001
0.0114
0.0001
interfer
0.0001
0.0052
0.0001
0.0037
0.0005
0.0005
0.0001
0.0018
0.0034
0.0037
0.0015
0.0027
0.0009
0.0009
0.0018
0.0063
0.0001
0.0029
0.0013
0.0001
0.0018
0.0005
0.0037
0.0021
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
0.4000
INTERFER
0.4000
INTERFER
0.4000
0.4000
0.4000
0.4000
1.0000
0.4000
0.4000
0.4000
INTERFER
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
400.0000
790.0000
1130.0000
Run 3
Hut
Blank
9582050
mq/Kq
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
0.4000
2.1000
1.2000
INTERFER
0.4000
0.4000
1.7000
0.4000
14.0000
0.4000
0.4000
0.4000
INTERFER
0.4000
0.7000
1.2000
0.4000
0.4000
2.3000
0.4000
1.0000
470.0000
1000.0000
1040.0000
Run 4
Non
Recycler
9582051
mq/Kq
0.0408
0.0025
0.0841
0.0005
0.0010
0.0643
0.0005
0.0005
0.0005
0.0005
0.0005
0.0742
0.0396
0.0210
0.0346
0.0005
0.0186
0.0005
0.0767
0.0005
0.0371
0.0005
0.0297
0.0940
interfer
0.0005
0.0346
0.0005
0.0005
0.0005
0.0111
0.0383
0.0005
0.0030
0.0099
0.0005
0.0031
0.0067
0.0136
0.0106
0.0063
0.0021
0.0048
0.0052
0.0198
0.0005
0.0054
0.0026
0.0005
0.0067
0.0005
0.0093
0.0005
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
EE
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
2.7000
7.8000
7.7000
34.0000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
0.4000
3.1000
INTERFER
1 1 .0000
1.4000
2.5000
3.8000
2.4000
0.4000
INTERFER
0.4000
520.0000
830.0000
1140.0000
Run 5
Non
Recycler
9582052
mq/Kq
0.1344
0.0018
0.1434
0.0004
0.0027
0.0986
0.0385
0.0004
0.0448
0.0117
0.0152
0.0726
0.0385
0.0004
0.0448
0.0004
0.0323
0.0004
0.0645
0.0430
0.0592
0.0004
0.0538
0.1434
0.0215
0.0004
0.0780
0.0004
interfer
interfer
0.0206
interfer
0.0484
0.0035
0.0004
0.0004
0.0088
0.0099
0.0206
0.0041
0.0073
0.0031
0.0083
0.0108
0.0188
0.0004
0.0019
0.0056
0.0004
0.0099
0.0029
0.0152
0.0065
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Estimated emissions mq/Kq
COMPOUND
BZ-1 51 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-1 07 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-1 23, BZ-1 49
BZ-1 18
BZ-1 34
BZ-1 22 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-1 46
BZ-1 53
BZ-132, BZ-105
BZ-1 41 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-1 79
BZ-1 37
BZ-1 30, BZ-1 76
BZ-1 38
BZ-1 58
BZ-1 29
BZ-1 78
BZ-1 75
BZ-1 87
BZ-1 83
BZ-1 28
BZ-1 67
BZ-1 85
BZ-1 74
BZ-1 77
BZ-1 71, BZ-202
BZ-1 56
BZ-1 73, BZ-1 57, IUPAC-201
BZ-1 72
BZ-1 97
BZ-1 80
BZ-1 93
BZ-1 91
IUPAC-200
MIREX
BZ-1 70, BZ-1 90
IUPAC-199
BZ-203, BZ-1 96
BZ-1 89
BZ-1 95
BZ-1 94
BZ-206
BZ-209 (DECACHLOROBIPHENYL) (Surroqate)
BZ-1 4 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-1 66, BZ-1 75
Run 1
Avid
Recycler
9582048
mq/kq
0.0063
0.0071
0.0002
0.0154
0.0083
0.0043
0.0017
0.0025
0.0039
0.0060
0.0029
0.0002
0.0002
0.0002
0.0047
0.0012
0.0002
0.0047
interfer
0.0043
0.0002
0.0022
0.0021
0.0002
0.0026
0.0023
interfer
0.0027
0.0002
0.0018
0.0011
0.0122
0.0002
0.0020
0.0002
interfer
0.0002
0.0023
0.0038
0.0043
0.0031
interfer
interfer
0.0015
0.1831
0.3571
0.4301
su - suspicious result, analyst suqqested poor confirmation
It - less than
nr - not required for analysis
ee - estimated result
interfer - peak interference, could not quantify
LT
LT
LT
LT
LT
NR
LT
LT
LT
LT
LT
LT
Run 2
Avid
Recycler
9582049
mq/Kq
0.0044
0.0008
0.0001
0.0081
0.0040
0.0001
0.0001
0.0013
0.0011
0.0013
0.0015
0.0001
0.0001
0.0001
0.0021
0.0001
0.0004
0.0003
interfer
0.0001
0.0036
0.0009
0.0006
0.0001
0.0017
0.0007
interfer
0.0001
0.0001
0.0001
0.0004
0.0001
0.0001
0.0007
0.0001
interfer
0.0029
0.0007
0.0001
0.0001
0.0004
interfer
0.0001
0.0010
0.1656
0.3495
0.4231
LT
LT
LT
LT
LT
LT
LT
NR
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
Run 3
Hut
Blank
9582050
mq/Kq
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
Run 4
Non
Recycler
9582051
mq/Kq
0.0101
0.0049
0.0005
0.0186
0.0083
0.0005
0.0005
0.0030
interfer
0.0059
0.0032
0.0005
0.0005
0.0005
0.0074
0.0005
0.0005
0.0005
interfer
0.0005
0.0089
0.0032
0.0005
0.0005
0.0026
0.0015
interfer
0.0005
0.0005
0.0021
0.0005
0.0173
0.0005
0.0005
0.0005
interfer
0.0005
0.0009
0.0015
0.0005
0.0005
0.0028
0.0005
0.0012
0.5812
1.2367
1.2862
LT
LT
LT
LT
LT
LT
LT
LT
LT
NR
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
EE
Run 5
Non
Recycler
9582052
mq/Kq
0.0179
0.0045
0.0004
0.0287
0.0143
0.0065
0.0004
0.0036
0.0108
0.0049
0.0039
0.0016
0.0004
0.0004
0.0080
0.0013
0.0004
0.0046
interfer
0.0179
0.0059
0.0004
0.0039
0.0024
0.0070
0.0069
0.0305
0.0004
0.0004
0.0004
0.0004
0.0004
0.0004
0.0004
0.0028
interfer
0.0099
0.0013
0.0022
0.0034
0.0022
0.0004
interfer
0.0004
0.4660
0.7439
1.0217
LT
LT
LT
LT
NR
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Metals
Metals
Metals Quantities in Sample Media (filter blank or reagent blank as appropriate subtracted from all sarr
metal
Cu
Ni
Zn
Pb
Mg
Al
Se
Ba
Be
Ag
Cd
As
Cr
Hg
Run 1
Avid Recycler
total ug
on filter
40.20
1.30
50.60
0.96
8.20
588.00
<1.00
<0.10
<0.04
0.07
0.17
2.00
0.54
<0.04
n/a= not analyzed
Run 2
Avid Recycler
total ug
on filter
17.00
<0.20
7.00
7.30
<0.20
6.80
<1.00
<0.10
<0.04
<.04
0.18
5.50
0.54
<0.04
*no data because of broken sample
Run 3
Hut Blank
total ug
on filter
0.26
<1.24
<8.2
<0.36
<8.8
<8.2
<1.00
0.64
<0.04
<.04
0.02
<0.02
0.32
<0.02
Total of Particulate Phase Metals: Filter and HNO3
Run 4
non-Recycler
total ug
on filter
1.90
<0.20
<0.80
0.66
2.80
2.20
<1.00
1.09
<0.04
0.06
0.21
3.80
<0.20
<0.04
Rinse
Run 5
non-Recycler
total ug
on filter
0.44
<0.20
<0.80
0.16
<2.0
6.00
<1.00
0.65
<0.04
<.04
0.04
0.19
0.20
0.11
Filter
Blank
total ug
on filter
0.64
1.20
8.20
0.36
8.80
8.20
<1
0.20
<.04
<.04
<.02
<.02
0.82
<.04
metal
Cu
Ni
Zn
Pb
Mg
Al
Se
Ba
Be
Ag
Cd
As
Cr
Hg
Note: Where two values, one a nondetect and one a detect were totaled, the absolute values were totaled and a less then sign was applied if the non
total
metal*
Cu
Ni
Zn
Pb
Mg
Al
Se
Ba
Be
Ag
Cd
As
Cr
Hg
Run 1
Avid Recycler
total ug
41.10
2.20
51.70
1.12
8.95
588.50
<1.25
0.28
<0.05
0.08
0.37
2.04
0.65
<0.04
Run 2
Avid Recycler
total ug
18.10
0.55
9.00
7.52
<0.7
7.30
<1.25
0.24
<0.05
<0.05
0.22
5.84
0.61
<0.04
Run 3
Hut Blank
total ug
0.38
<1.35
<10.05
<0.47
<10.7
<21.95
<1.25
0.71
<0.05
<0.05
0.04
0.03
0.34
<0.02
Run 4
non-Recycler
total ug
1.90
<0.20
<0.80
0.66
2.80
2.20
<1.25
1.09
<0.04
0.06
0.21
3.80
<0.20
<0.04
Run 5
non-Recycler
total ug
0.78
0.34
0.10
0.30
<2.5
6.50
<1.25
0.79
<0.05
<0.05
0.05
0.21
0.24
0.11
Filter and
Reagent Blank
total ug
1.54
2.10
9.30
0.52
9.55
22.00
<1.25
0.38
<.05
<.05
<.026
<.028
0.93
<.04
*total metal = solid metal + nitric rinse, where numbers less than detection limits were added at detection li
mit
Note when adding a less then quantity and an actual detected value from two fractions result reported withoug a less
Filter blank has been subtracted from all samples including hut blank.
EQUATIONS USED:
Total ug/sample (filter) = (ug/l sample-ug/l blank)*0.05 I (0.1 I for Hg)*4 (1/4 filter digested)
Total ug/sample (HN03 or HCI) = (ug/l sample-ug/l reagent blank)*0.05l (0.1 I fo
rHg)
G- 13
-------
Metals
Total Particulate Metals Concentration in Facility ,
mg/M3
metal
cone.
Cu
Ni
Zn
Pb
Mg
Al
Se
Ba
Be
Ag
Cd
As
Cr
Hg
Run 1
Avid Recycler
mg/M3
0.000030
0.000002
0.000038
0.000001
0.000007
0.000434
<0. 001 151
0.000000
<0. 000046
0.000000
0.000000
0.000002
0.000000
<0. 000037
Run 2
Avid Recycler
mg/M3
0.014982
0.000455
0.007450
0.006225
<0. 002069
0.006042
<0. 001 035
0.000199
<0. 000041
<0. 000041
0.000182
0.004834
0.000505
<0. 000033
Run 3
Hut Blank
mg/M3
0.000269
<0. 0001 43
<0. 000573
<0
<0.00179
<0
<0. 000895
0.000508
<0. 000036
<0. 000036
0.000029
0.000021
0.000240
<0. 000029
Total Estimated Particulate Phase Metals Emissiot
metal
Cu
Ni
Zn
Pb
Mg
Al
Se
Ba
Be
Ag
Cd
As
Cr
Hg
Run 1
Avid Recycler
8/30/95
g/Kg
0.015015
0.000804
0.018888
0.000409
0.003270
0.215000
<0. 000457
0.000102
<0. 00001 8
0.000029
0.000135
0.000745
0.000237
<0. 00001 5
Run 2
Avid Recycler
9/1/95
g/Kg
0.006176
0.000188
0.003071
0.002566
<0. 000853
0.002491
<0. 000426
0.000082
<0. 00001 7
<0. 00001 7
0.000075
0.001993
0.000208
<0. 00001 4
Run 3
Hut Blank
9/6/95
g/Kg
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
Mr
Run 4
non-Recycler
mg/M3
0.002043
<0. 00021 5
<0. 00086
0.000710
0.003010
0.002365
<0. 001 344
0.001172
<0. 000054
0.000065
0.000226
0.004085
<0. 00021 5
<0. 000043
IS
Run 4
non-Recycler
9/8/95
g/Kg
0.002164
<0. 000228
<0. 000911
0.000752
0.003189
0.002506
<0. 001 424
0.001242
<0. 000057
0.000068
0.000239
0.004329
<0. 000228
<0. 000046
Run 5
non-Recycler
mg/M3
0.000541
0.000236
0.000069
0.000208
<0. 001 734
0.004507
<0. 000867
0.000548
<0. 000035
<0. 000035
0.000035
0.000146
0.000166
0.000076
Run 5
non-Recycler
9/12/95
g/Kg
0.000573
0.000250
0.000073
0.000220
<0. 001 837
0.004776
<0. 00091 8
0.000580
<0. 000037
<0. 000037
0.000037
0.000154
0.000176
0.000081
G- 14
-------
Metals
pies, including hut blank - Nitric rinse not done yet anc
Run 1
Avid Recycler
total ug
HN03 Rinse
0.90
0.90
1.10
0.16
0.75
<0.50
<0.25
0.18
<0.01
<0.01
0.20
0.04
0.11
n/a
Jetect had a greater i
detection limits
0.20
0.80
2.50
1.25
0.05
0.05
0.20
0.04
hen sign.
Run 2
Avid Recycler
total ug
HN03 Rinse
1.10
0.35
2.00
0.22
<0.50
<0.50
<0.25
0.14
<0.01
<0.01
0.04
0.34
0.07
n/a
bsolute value.
Run 3
Hut Blank
total ug
HN03 Rinse
0.12
0.11
<1.85
0.11
<1.9
<13.75
<0.25
<0.07
<0.01
<0.01
0.02
0.01
0.02
n/a
Run 4*
non-Recycler
total ug
HN03 Rinse
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
n/a
check JJ nun
Run 5
non-Recycler
total ug
HN03 Rinse
0.34
0.14
0.20
0.14
<0.50
<0.50
<0.25
0.14
<0.01
<0.01
0.01
0.02
0.04
n/a
ibers)
Reagent
Blank
total ug
HN03 Rinse
0.080
0.135
1.850
0.039
1.900
13.750
<.25
0.070
<.01
<.01
0.006
0.008
0.120
n/a
G- 15
-------
Metals
from mercury sheet
Vm,std
ft3
38.38
42.69
49.34
32.87
50.96
Air into hut
CUFT/MIN
1622.5
1622.5
1622.5
1622.5
1622.5
Run Time
min
70
79
90
60
90
Mass burnned
Kg
8.1
8.8
0.0
2.6
3.9
Test
No.
1
2
3
4
5
Test Conditions
Avid Recycler
Avid Recycler
Hut Blank
Non Recycler
Non Recycler
DATE
34941.0
34943.0
34948.0
34950.0
34954.0
G- 16
-------
ESTIMATED GASEOUS MERCURY EMISSIONS (g/Kg)
Mercury
ESTIMATED GASEOUS MERCURY EMISSIONS
Test
No.
1
2
3
4
5
Test Conditions
Avid Recycler
Avid Recycler
Hut Blank
Non Recycler
Non Recycler
Media Blank
na = not applicable
DATE
8/30/95
9/1/95
9/6/95
9/8/95
9/12/95
comb = combined with impinger catch for i
Test #
1
2
3
4
5
Tm,1
deg F
92.0000
87.0000
84.0000
83.5000
73.5000
moisture from r2 1 0ml collect!
Tm,f
deg F
96.0000
97.5000
96.0000
93.0000
87.5000
d
(g/Kg)
RUN #
1
2
3
4
5
nalysis
Tm.avg
deg F
94.0000
92.2500
90.0000
88.2500
80.5000
TLI Data
Impinger
Catch
ug Hg
<4.00
<4.00
<4.00
<4.00
<4.00
<4
Pbar
in Hg
29.6800
29.3600
29.6900
29.4700
29.8200
NYS DOH data
HCI
Rinse
ug Hg
comb.
<.1
<.1
0.3200
<.1
<.1
Total
Vapor Phase
Catch
< ug Hg
4.0000
4.1000
4.1000
4.3200
4.1000
4.1000
Mass burnned
Kg
8.1
8.8
0.0
2.6
3.9
na
dH
0.8500
0.8500
0.8500
0.8500
0.8500
G-17
-------
ESTIMATED GASEOUS MERCURY EMISSIONS (g/Kg)
Vm.std
ft3
38.3753
42.6854
49.3420
32.8684
50.9606
na
Yd
1.0293
1.0293
1.0293
1.0293
1.0293
Hg cone.
ug/M3
3.6819
3.3929
2.9351
4.6426
2.8419
na
DGM.i
34.2940
77.2320
121.7320
172.1690
205.9160
Estimated
Hg emissions
< g/kg
1.430E-03
1.354E-03
na
4.758E-03
2.989E-03
na
DGM.f
73.6620
121.3580
171.9680
205.7750
256.6820
Vm
ft3
39.3680
44.1260
50.2360
33.6060
50.7660
Run Time
min
70.0000
79.0000
90.0000
60.0000
90.0000
Impinger
Hg cone.
mg/ft3
0.0001
0.0001
0.0001
0.0001
0.0001
Hg det. limit
ug
4.00
4.00
4.00
4.00
4.00
Air into hut
CUFT/MIN
1622.5000
1622.5000
1622.5000
1622.5000
1622.5000
Mass Burnned
Ib
18.0000
20.2000
N/A
7.0000
9.0000
G-18
-------
Raw Ash Data
PCDD/PCDF, PCB, CB Method blank for ash
2,3,7,8-TETRACHLORODIBENZODIOXIN
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
OCTACHLORODIBENZOFURAN
TOTAL TETRACHLORODIBENZODIOXINS
TOTAL PENTACHLORODIBENZODIOXINS
TOTAL HEXACHLORODIBENZODIOXINS
TOTAL HEPTACHLORODIBENZODIOXINS
TOTAL TETRACHLORODIBENZOFURANS
TOTAL PENTACHLORODIBENZOFURANS
TOTAL HEXACHLORODIBENZOFURANS
TOTAL HEPTACHLORODIBENZOFURANS
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-19 (2,2',6-TRICHLOROBIPHENYL)
BZ-12 (3,4-DICHLOROBIPHENYL)(Surrogate)
BZ-18 (2,2',5-TRICHLOROBIPHENYL)
BZ-15, BZ-17
BZ-24, BZ-27
BZ-16, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
1 9 PG/G
19 PG/G
24 PG/G
21 PG/G
20 PG/G
29 PG/G
53 PG/G
17 PG/G
14 PG/G
18 PG/G
15 PG/G
15 PG/G
18 PG/G
17 PG/G
19 PG/G
22 PG/G
32 PG/G
19 PG/G
19 PG/G
21 PG/G
29 PG/G
43 PG/G
14 PG/G
15 PG/G
19 PG/G
2.5 NG/G
2.5 NG/G
2.5 NG/G
0.5 NG/G
152 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
INTERFER NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
G-79
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-47 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,51-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, OCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,51-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-119 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-115
BZ-85, 4,4'-DDE
BZ-136
BZ-77, BZ-110
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-151 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-107 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-123, BZ-149
BZ-118
BZ-134
BZ-122 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-146
BZ-153
BZ-132, BZ-105
BZ-141 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-179
BZ-137
BZ-130, BZ-176
BZ-138
BZ-158
BZ-129
BZ-178
BZ-175
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
G-20
PL
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
BZ-187
BZ-183
BZ-128
BZ-167
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209(DECACHLOROBIPHENYL)(Surrogate)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
2 NG/G
154 NG/G
36 NG/G
41 NG/G
48 NG/G
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
PL
PL
G-21
-------
Raw Ash Data
SVOC method blank for ash
ACENAPHTHENE
ACENAPHTHYLENE
ACETOPHENONE
2-ACETYLAMINOFLUORENE
ALDRIN
4-AMINOBIPHENYL
ANTHRACENE
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(ghi)PERYLENE
BENZO(a)PYRENE
BENZYL ALCOHOL
HCH,ALPHA
HCH,BETA
HCH,DELTA
HCH,GAMMA (LINDANE)
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
CHLORDANE, GAMMA ISOMER
4-CHLOROANILINE
CHLOROBENZILATE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
4,4'-DDD
4,4'-DDE
4,4'-DDT
DIALLATE
DIBENZOFURAN
DIBENZ(A,H)ANTHRACENE
DI-N-BUTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3'-DICHLOROBENZIDINE
330
330
330
660
330
660
330
6600
6600
6600
6600
6600
6600
6600
330
330
330
3
330
330
2
2
2
2
330
330
1600
330
330
330
330
330
330
330
330
330
330
330
330
3
330
330
2
2
330
330
330
330
G-22
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
J
LT
LT
LT
LT
-------
Raw Ash Data
2,4-DICHLOROPHENOL
2,6-DICHLOROPHENOL
DIELDRIN
DIETHYLPHTHALATE
DIMETHOATE
DIMETHYLPHTHALATE
P-DIMETHYLAMINO-AZOBENZENE
3,3'-DIMETHYLBENZIDINE
7,12-DIMETHYLBENZ(A)ANTHRACENE
2,4-DIMETHYLPHENOL
1,3-DINITROBENZENE
2-METHYL-4.6-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
DIPHENYLAMINE
DISULFOTON (Di-Syston)
ENDOSULFAN I
ENDOSULFAN II
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ETHYL METHANESULFONATE
BIS(2-ETHYLHEXYL)PHTHALATE
FAMPHUR
FLUORANTHENE
FLUORENE
HEPTACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE (C-46)
HEXACHLOROCYCLOPENTADIENE (C-56)
HEXACHLOROETHANE
HEXACHLOROPROPENE
INDENO(1 ,2,3-cd)PYRENE
ISODRIN
ISOPHORONE
ISOSAFROLE
KEPONE
METHAPYRILENE
METHOXYCHLOR
METHYL METHANESULFONATE
METHYL PARATHION
3-METHYLCHOLANTHRENE
2-METHYLNAPHTHALENE
2-METHYL PHENOL
3. OR 4-METHYLPHENOL
NAPHTHALENE
1,4-NAPHTHOQUINONE
330
330
3 jiG/KG
330
660
330
660
330
330
330
330
1600
1600
330
330
660
330
660
330
330
330
330
660
14
660
330
330
330
330
330
330
330
330
330
2
660
330
330
660
3300
330
330
330
330
330
330
330
330
330
G-23
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
1-NAPHTHYLAMINE
2-NAPHTHYLAMINE
2-NITROANILINE
3-NITROANILINE
4-NITROANILINE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIETHYLAMINE
N-NITROSOSDIMETHYLAMINE
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-BUTYLAMINE
N-NITROSOMETHYL-ETHYLAMINE
N-NITROSOPIPERIDINE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSOPYRROLIDINE
5-NITRO-O-TOLUIDINE
DI-N-OCTYL PHTHALATE
PARATHION, ETHYL
PENTACHLOROBENZENE
PENTACHLORONITROBENZENE
PENTACHLOROPHENOL
PHENACETIN
PHENANTHRENE
PHENOL
P-PHENYLENEDIAMINE
PHORATE
PRONAMIDE
PYRENE
SAFROLE
1,2,4,5-TETRACHLOROBENZENE
2,3,4,6-TETRACHLOROPHENOL
THIONAZIN
O-TOLUIDINE
TOXAPHENE
1,2,4-TRICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
PYRIDINE
ALPHA-PICOLINE
ANILINE
BENZIDINE
ENDRIN KETONE
1,3,5-TRINITROBENZENE
4-NITROQUINOLINE 1-OXIDE
CHLORDANE, ALPHA ISOMER
330
330
1600 jiG/KG
1600
660
330
330
1600
9900
66
160
330
330
6600
330
330
330
330
330
330
330
1600
660
330
330
330
330
330
330
330
330
330
330
330
66
330
820
330
3300
3300
330
1600
33
330
1200
1600
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
G-24
-------
Raw Ash Data
Composite Ash for Avid Recycler
2,3,7,8-TETRACHLORODIBENZODIOXIN
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
OCTACHLORODIBENZOFURAN
TOTAL TETRACHLORODIBENZODIOXINS
TOTAL PENTACHLORODIBENZODIOXINS
TOTAL HEXACHLORODIBENZODIOXINS
TOTAL HEPTACHLORODIBENZODIOXINS
TOTAL TETRACHLORODIBENZOFURANS
TOTAL PENTACHLORODIBENZOFURANS
TOTAL HEXACHLORODIBENZOFURANS
TOTAL HEPTACHLORODIBENZOFURANS
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-19 (2,2',6-TRICHLOROBIPHENYL)
BZ-12 (3,4-DICHLOROBIPHENYL)(Surrogate)
BZ-18 (2,2',5-TRICHLOROBIPHENYL)
BZ-15, BZ-17
BZ-24, BZ-27
BZ-16, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
31 PG/G
230 PG/G
270 PG/G
420 PG/G
300 PG/G
4000 PG/G
9600 PG/G
830 PG/G
1000 PG/G
2500 PG/G
2300 PG/G
2100 PG/G
2900 PG/G
810 PG/G
12000 PG/G
1400 PG/G
8200 PG/G
2500 PG/G
4100 PG/G
5600 PG/G
7600 PG/G
25000 PG/G
21000 PG/G
19000 PG/G
17000 PG/G
2.5 NG/G
43 NG/G
2.5 NG/G
0.5 NG/G
132 NG/G
2.1 NG/G
3.7 NG/G
5.4 NG/G
135 NG/G
0.5 NG/G
6.6 NG/G
32 NG/G
0.5 NG/G
12 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
1.5 NG/G
0.5 NG/G
2.2 NG/G
0.5 NG/G
G-25
LT
SU
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-47 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,5'-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, OCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,5'-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-119 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-115
BZ-85, 4,4'-DDE
BZ-136
BZ-77, BZ-110
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-151 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-107 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-123, BZ-149
BZ-118
BZ-134
BZ-122 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-146
BZ-153
BZ-132, BZ-105
BZ-141 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-179
BZ-137
BZ-130, BZ-176
BZ-138
BZ-158
BZ-129
BZ-178
0.5 NG/G
5.3 NG/G
0.5 NG/G
0.5 NG/G
3.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
2.6 NG/G
1.8 NG/G
1.8 NG/G
INTERFER NG/G
0.5 NG/G
1.8 NG/G
0.5 NG/G
0.5 NG/G
1 NG/G
0.5 NG/G
1.6 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
3.4 NG/G
0.5 NG/G
0.4 NG/G
2.2 NG/G
1.5 NG/G
0.5 NG/G
0.5 NG/G
1.2 NG/G
1.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
3.4 NG/G
1.2 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1.7 NG/G
G-26
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
PL
LT
PL
LT
LT
LT
PL
PL
LT
PL
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
BZ-175
BZ-187
BZ-183
BZ-128
BZ-167
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209(DECACHLOROBIPHENYL)(Surrogate)
PICES (Surrogates)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
SOLIDS, DRY
ACENAPHTHENE
ACENAPHTHYLENE
ACETOPHENONE
2-ACETYLAMINOFLUORENE
ALDRIN
4-AMINOBIPHENYL
ANTHRACENE
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(ghi)PERYLENE
41 NG/G
0.5 NG/G
1.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
0.9 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
2.5 NG/G
0.5 NG/G
1.6 NG/G
0.6 NG/G
1.1 NG/G
1.4 NG/G
2.8 NG/G
131 NG/G
NG/G
38 NG/G
42 NG/G
41 NG/G
PERCENT
5000 |iG/KG
5000 |iG/KG
480 |iG/KG
9900 |iG/KG
5000 |iG/KG
9900 |iG/KG
5000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
62 |iG/KG
78 |iG/KG
1 1 0 |iG/KG
120 |iG/KG
G-27
LT
LT
PL
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
I\R
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
J
J
BJ
-------
Raw Ash Data
BENZO(a)PYRENE
BENZYL ALCOHOL
HCH, ALPHA
HCH, BETA
HCH, DELTA
HCH, GAMMA (LINDANE)
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
CHLORDANE, GAMMA ISOMER
4-CHLOROANILINE
CHLOROBENZILATE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
4,4'-DDD
4,4'-DDE
4,4'-DDT
DIALLATE
DIBENZOFURAN
DIBENZ(A,H)ANTHRACENE
DI-N-BUTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3'-DICHLOROBENZIDINE
2,4-DICHLOROPHENOL
2,6-DICHLOROPHENOL
DIELDRIN
DIETHYLPHTHALATE
DIMETHOATE
DIMETHYLPHTHALATE
P-DIMETHYLAMINO-AZOBENZENE
3,3'-DIMETHYLBENZIDINE
7,12-DIMETHYLBENZ(A)ANTHRACENE
2,4-DIMETHYLPHENOL
1,3-DINITROBENZENE
2-METHYL-4.6-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
DIPHENYLAMINE
DISULFOTON (Di-Syston)
ENDOSULFAN I
ENDOSULFAN II
78
5000
26
26
26
26
5000
110
24000
5000
5000
5000
5000
5000
5000
5000
5000
5000
76
5000
5000
50
5000
170
120
160
190
88
54
5000
92
5000
50
110
9900
5000
9900
5000
5000
5000
5000
25000
25000
5000
5000
9900
5000
9900
5000
G-28
|iG/KG
|iG/KG
|iG/KG
jiG/KG
|iG/KG
J
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
J
BJ
BJ
J
J
J
LT
J
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ETHYL METHANESULFONATE
BIS(2-ETHYLHEXYL)PHTHALATE
FAMPHUR
FLUORANTHENE
FLUORENE
HEPTACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE (C-46)
HEXACHLOROCYCLOPENTADIENE (C-56)
HEXACHLOROETHANE
HEXACHLOROPROPENE
INDENO(1,2,3-cd)PYRENE
ISODRIN
ISOPHORONE
ISOSAFROLE
KEPONE
METHAPYRILENE
METHOXYCHLOR
METHYL METHANESULFONATE
METHYL PARATHION
3-METHYLCHOLANTHRENE
2-METHYLNAPHTHALENE
2-METHYL PHENOL
3. OR 4-METHYLPHENOL
NAPHTHALENE
1,4-NAPHTHOQUINONE
1-NAPHTHYLAMINE
2-NAPHTHYLAMINE
2-NITROANILINE
3-NITROANILINE
4-NITROANILINE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIETHYLAMINE
N-NITROSOSDIMETHYLAMINE
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-BUTYLAMINE
N-NITROSOMETHYL-ETHYLAMINE
N-NITROSOPIPERIDINE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSOPYRROLIDINE
5-NITRO-O-TOLUIDINE
DI-N-OCTYL PHTHALATE
PARATHION, ETHYL
5000
5000
5000 jiG/KG
9900
360
9900
68
78 jiG/KG
5000
5000
170
5000
5000 jiG/KG
5000
5000
140
9900
5000
5000
9900
50000
5000
5000
5000
5000
160
120
5000
650
5000
5000
5000
25000
25000
9900
5000
5000
25000
660
990
2500
5000
5000
99000
5000
5000
5000
55
5000
G-29
LT
LT
LT
LT
BJ
LT
J
J
LT
LT
J
LT
LT
LT
LT
BJ
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
J
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
-------
Raw Ash Data
PENTACHLOROBENZENE
PENTACHLORONITROBENZENE
PENTACHLOROPHENOL
PHENACETIN
PHENANTHRENE
PHENOL
P-PHENYLENEDIAMINE
PHORATE
PRONAMIDE
PYRENE
SAFROLE
1,2,4,5-TETRACHLOROBENZENE
2,3,4,6-TETRACHLOROPHENOL
THIONAZIN
0-TOLUIDINE
TOXAPHENE
1,2,4-TRICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
SOLIDS, DRY
ARSENIC IN DRY SOLIDS
SELENIUM IN DRY SOLIDS
MERCURY IN DRY SOLIDS
BERYLLIUM IN DRY SOLIDS
SILVER IN DRY SOLIDS
BARIUM IN DRY SOLIDS
CADMIUM IN DRY SOLIDS
COBALT IN DRY SOLIDS
CHROMIUM IN DRY SOLIDS
COPPER IN DRY SOLIDS
IRON IN DRY SOLIDS
MANGANESE IN DRY SOLIDS
NICKEL IN DRY SOLIDS
STRONTIUM IN DRY SOLIDS
TITANIUM IN DRY SOLIDS
VANADIUM IN DRY SOLIDS
ZINC IN DRY SOLIDS
MOLYBDENUM IN DRY SOLIDS
LEAD IN DRY SOLIDS
ANTIMONY IN DRY SOLIDS
TIN IN DRY SOLIDS
THALLIUM IN DRY SOLIDS
ALUMINUM IN DRY SOLIDS
CALCIUM IN DRY SOLIDS
POTASSIUM IN DRY SOLIDS
MAGNESIUM IN DRY SOLIDS
SODIUM IN DRY SOLIDS
PYRIDINE
ALPHA-PICOLINE
290 jiG/KG
5000 jiG/KG
25000 jiG/KG
9900 |iG/KG
290 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
76 |iG/KG
5000 |iG/KG
140 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
990 |iG/KG
120 |iG/KG
54 |iG/KG
170 |iG/KG
93 PERCENT
310 MG/KG
1 MG/KG
0.11 MG/KG
1 MG/KG
25 MG/KG
187 MG/KG
3 MG/KG
12 MG/KG
286 MG/KG
3780 MG/KG
4390 MG/KG
525 MG/KG
18 MG/KG
104 MG/KG
716 MG/KG
35 MG/KG
10900 MG/KG
17 MG/KG
168 MG/KG
MG/KG
226 MG/KG
MG/KG
92900 MG/KG
97400 MG/KG
5050 MG/KG
2860 MG/KG
5400 MG/KG
870 |iG/KG
190 |iG/KG
G-30
j
LT
LT
LT
J
LT
LT
LT
LT
J
LT
J
LT
LT
LT
LT
J
J
J
LT
LT
LT
LT
I\R
I\R
J
J
-------
Raw Ash Data
ANILINE 5000 jaG/KG LT
BENZIDINE 24000 jaG/KG LT
ENDRINKETONE 500 jaG/KG LT
1,3,5-TRINITROBENZENE 5000 |iG/KG LT
4-NITROQUINOLINE 1-OXIDE 18000|iG/KG LT
CHLORDANE, ALPHA ISOMER 24000 |iG/KG LT
G-31
-------
Raw Ash Data
Composite Ash for Non-recycler
2,3,7,8-TETRACHLORODIBENZODIOXIN
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
OCTACHLORODIBENZOFURAN
TOTAL TETRACHLORODIBENZODIOXINS
TOTAL PENTACHLORODIBENZODIOXINS
TOTAL HEXACHLORODIBENZODIOXINS
TOTAL HEPTACHLORODIBENZODIOXINS
TOTAL TETRACHLORODIBENZOFURANS
TOTAL PENTACHLORODIBENZOFURANS
TOTAL HEXACHLORODIBENZOFURANS
TOTAL HEPTACHLORODIBENZOFURANS
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-19 (2,2',6-TRICHLOROBIPHENYL)
BZ-12 (3,4-DICHLOROBIPHENYL)(Surrogate)
BZ-18 (2,2',5-TRICHLOROBIPHENYL)
BZ-15, BZ-17
BZ-24, BZ-27
BZ-16, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
9 PG/G
53 PG/G
44 PG/G
74 PG/G
56 PG/G
630 PG/G
690 PG/G
220 PG/G
270 PG/G
690 PG/G
480 PG/G
490 PG/G
670 PG/G
150 PG/G
2100 PG/G
170 PG/G
560 PG/G
490 PG/G
740 PG/G
1300 PG/G
1300 PG/G
8200 PG/G
6600 PG/G
4600 PG/G
2900 PG/G
4.9 NG/G
42 NG/G
22 NG/G
0.5 NG/G
161 NG/G
2.1 NG/G
4.7 NG/G
3.8 NG/G
18 NG/G
5.6 NG/G
7.4 NG/G
6.3 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.7 NG/G
0.9 NG/G
0.5 NG/G
0.9 NG/G
1.5 NG/G
0.5 NG/G
G-32
su
su
LT
LT
LT
LT
LT
PL
-------
Raw Ash Data
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-47 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,51-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, OCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,51-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-119 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-115
BZ-85, 4,4'-DDE
BZ-136
BZ-77, BZ-110
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-151 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-107 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-123, BZ-149
BZ-118
BZ-134
BZ-122 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-146
BZ-153
BZ-132, BZ-105
BZ-141 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-179
BZ-137
BZ-130, BZ-176
BZ-138
BZ-158
BZ-129
BZ-178
BZ-175
1.3 NG/G
0.5 NG/G
0.5 NG/G
1.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1.2 NG/G
1.7 NG/G
0.5 NG/G
1 7 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
2.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1.3 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1.9 NG/G
0.5 NG/G
0.5 NG/G
1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
3.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
47 NG/G
G-33
LT
LT
LT
LT
LT
LT
LT
LT
PL
LT
LT
LT
LT
LT
LT
LT
PL
PL
LT
PL
LT
LT
PL
PL
PL
LT
PL
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
BZ-187
BZ-183
BZ-128
BZ-167
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209(DECACHLOROBIPHENYL)(Surrogate)
PICES (Surrogates)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
SOLIDS, DRY
ACENAPHTHENE
ACENAPHTHYLENE
ACETOPHENONE
2-ACETYLAMINOFLUORENE
ALDRIN
4-AMINOBIPHENYL
ANTHRACENE
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(ghi)PERYLENE
BENZO(a)PYRENE
0.5 NG/G
1.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.6 NG/G
0.6 NG/G
3.4 NG/G
144 NG/G
NG/G
40 NG/G
47 NG/G
47 NG/G
PERCENT
5000 |iG/KG
61 |iG/KG
1400 |iG/KG
9900 |iG/KG
5000 |iG/KG
9900 |iG/KG
80 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
94 |iG/KG
5000 |iG/KG
5000 |iG/KG
160 |iG/KG
5000 |iG/KG
G-34
LT
LT
PL
LT
LT
LT
LT
LT
PL
PL
LT
LT
LT
LT
LT
PL
LT
LT
LT
I\R
LT
J
J
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
BJ
LT
-------
Raw Ash Data
BENZYL ALCOHOL
HCH,ALPHA
HCH,BETA
HCH,DELTA
HCH,GAMMA (LINDANE)
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
CHLORDANE, GAMMA ISOMER
4-CHLOROANILINE
CHLOROBENZILATE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
4,4'-DDD
4,4'-DDE
4,4'-DDT
DIALLATE
DIBENZOFURAN
DIBENZ(A,H)ANTHRACENE
DI-N-BUTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3'-DICHLOROBENZIDINE
2,4-DICHLOROPHENOL
2,6-DICHLOROPHENOL
DIELDRIN
DIETHYLPHTHALATE
DIMETHOATE
DIMETHYLPHTHALATE
P-DIMETHYLAMINO-AZOBENZENE
3,3'-DIMETHYLBENZIDINE
7,12-DIMETHYLBENZ(A)ANTHRACENE
2,4-DIMETHYLPHENOL
1,3-DINITROBENZENE
2-METHYL-4.6-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
DIPHENYLAMINE
DISULFOTON (Di-Syston)
ENDOSULFANI
ENDOSULFAN II
ENDOSULFAN SULFATE
5000 jiG/KG
26 jiG/KG
26 jiG/KG
26
26
5000
5000
24000
5000
5000
5000
5000
5000
5000
5000
5000
5000
220
5000
5000
50
5000
350
150
130
5000
5000
5000
5000
5000
5000
50
5000
9900
5000
9900
5000
5000
5000
5000
25000
25000
5000
1100
9900
5000
9900
5000
5000
G-35
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
J
BJ
BJ
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
-------
Raw Ash Data
ENDRIN
ENDRIN ALDEHYDE
ETHYL METHANESULFONATE
BIS(2-ETHYLHEXYL)PHTHALATE
FAMPHUR
FLUORANTHENE
FLUORENE
HEPTACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE (C-46)
HEXACHLOROCYCLOPENTADIENE (C-56)
HEXACHLOROETHANE
HEXACHLOROPROPENE
INDENO(1,2,3-cd)PYRENE
ISODRIN
ISOPHORONE
ISOSAFROLE
KEPONE
METHAPYRILENE
METHOXYCHLOR
METHYL METHANESULFONATE
METHYL PARATHION
3-METHYLCHOLANTHRENE
2-METHYLNAPHTHALENE
2-METHYL PHENOL
3- OR 4-METHYLPHENOL
NAPHTHALENE
1,4-NAPHTHOQUINONE
1-NAPHTHYLAMINE
2-NAPHTHYLAMINE
2-NITROANILINE
3-NITROANILINE
4-NITROANILINE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIETHYLAMINE
N-NITROSOSDIMETHYLAMINE
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-BUTYLAMINE
N-NITROSOMETHYL-ETHYLAMINE
N-NITROSOPIPERIDINE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSOPYRROLIDINE
5-NITRO-O-TOLUIDINE
DI-N-OCTYL PHTHALATE
PARATHION, ETHYL
PENTACHLOROBENZENE
5000
5000
9900
310
9900
170
120
5000
5000
5000
5000
5000
5000
5000
120
9900
5000
5000
9900
50000
5000
5000
5000
5000
400
670 |iG/KG
5000
2400
5000
5000
5000
25000
25000
9900
5000
5000
25000
9900
990
2500
5000
5000
99000
5000
5000
5000
5000
5000
5000
G-36
LT
LT
LT
BJ
LT
J
J
LT
LT
LT
LT
LT
LT
LT
BJ
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
J
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
PENTACHLORONITROBENZENE
PENTACHLOROPHENOL
PHENACETIN
PHENANTHRENE
PHENOL
P-PHENYLENEDIAMINE
PHORATE
PRONAMIDE
PYRENE
SAFROLE
1,2,4,5-TETRACHLOROBENZENE
2,3,4,6-TETRACHLOROPHENOL
THIONAZIN
0-TOLUIDINE
TOXAPHENE
1,2,4-TRICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
SOLIDS, DRY
ARSENIC IN DRY SOLIDS
SELENIUM IN DRY SOLIDS
MERCURY IN DRY SOLIDS
BERYLLIUM IN DRY SOLIDS
SILVER IN DRY SOLIDS
BARIUM IN DRY SOLIDS
CADMIUM IN DRY SOLIDS
COBALT IN DRY SOLIDS
CHROMIUM IN DRY SOLIDS
COPPER IN DRY SOLIDS
IRON IN DRY SOLIDS
MANGANESE IN DRY SOLIDS
NICKEL IN DRY SOLIDS
STRONTIUM IN DRY SOLIDS
TITANIUM IN DRY SOLIDS
VANADIUM IN DRY SOLIDS
ZINC IN DRY SOLIDS
MOLYBDENUM IN DRY SOLIDS
LEAD IN DRY SOLIDS
ANTIMONY IN DRY SOLIDS
TIN IN DRY SOLIDS
THALLIUM IN DRY SOLIDS
ALUMINUM IN DRY SOLIDS
CALCIUM IN DRY SOLIDS
POTASSIUM IN DRY SOLIDS
MAGNESIUM IN DRY SOLIDS
SODIUM IN DRY SOLIDS
PYRIDINE
ALPHA-PICOLINE
ANILINE
5000 jiG/KG
25000 jiG/KG
9900 jiG/KG
8 1 0 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
180 jiG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
990 |iG/KG
5000 |iG/KG
38 |iG/KG
5000 |iG/KG
99 PERCENT
69 MG/KG
1 MG/KG
0.1 MG/KG
0.8 MG/KG
8 MG/KG
119 MG/KG
2 MG/KG
5 MG/KG
92 MG/KG
343 MG/KG
3560 MG/KG
152 MG/KG
13 MG/KG
117 MG/KG
1740 MG/KG
32 MG/KG
721 MG/KG
16 MG/KG
32 MG/KG
MG/KG
104 MG/KG
MG/KG
82400 MG/KG
139000 MG/KG
3110 MG/KG
2530 MG/KG
3450 MG/KG
600 |iG/KG
160 |iG/KG
5000 |iG/KG
G-37
LT
LT
LT
J
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
I\R
I\R
J
J
LT
-------
Raw Ash Data
BENZIDINE 24000 jaG/KG LT
ENDRINKETONE 500 jaG/KG LT
1,3,5-TRINITROBENZENE 5000 |iG/KG LT
4-NITROQUINOLINE 1-OXIDE 18000|iG/KG LT
CHLORDANE, ALPHA ISOMER 24000 jaG/KG LT
G-38
-------
Raw Ash Data
Metals from Avid Recycler
SOLIDS, DRY
ARSENIC IN DRY SOLIDS
SELENIUM IN DRY SOLIDS
MERCURY IN DRY SOLIDS
BERYLLIUM IN DRY SOLIDS
SILVER IN DRY SOLIDS
BARIUM IN DRY SOLIDS
CADMIUM IN DRY SOLIDS
COBALT IN DRY SOLIDS
CHROMIUM IN DRY SOLIDS
COPPER IN DRY SOLIDS
IRON IN DRY SOLIDS
MANGANESE IN DRY SOLIDS
NICKEL IN DRY SOLIDS
STRONTIUM IN DRY SOLIDS
TITANIUM IN DRY SOLIDS
VANADIUM IN DRY SOLIDS
ZINC IN DRY SOLIDS
MOLYBDENUM IN DRY SOLIDS
LEAD IN DRY SOLIDS
ANTIMONY IN DRY SOLIDS
TIN IN DRY SOLIDS
THALLIUM IN DRY SOLIDS
ALUMINUM IN DRY SOLIDS
CALCIUM IN DRY SOLIDS
POTASSIUM IN DRY SOLIDS
MAGNESIUM IN DRY SOLIDS
SODIUM IN DRY SOLIDS
92 PERCENT
320 MG/KG
1 MG/KG
0.1 MG/KG
0.9 MG/KG
9 MG/KG
185 MG/KG
3 MG/KG
1 1 MG/KG
300 MG/KG
4910 MG/KG
4390 MG/KG
541 MG/KG
22 MG/KG
102 MG/KG
820 MG/KG
37 MG/KG
11500 MG/KG
17 MG/KG
164 MG/KG
MG/KG
228 MG/KG
MG/KG
101000 MG/KG
94600 MG/KG
5000 MG/KG
2870 MG/KG
5410 MG/KG
LT
LT
LT
LT
LT
I\R
I\R
G-39
-------
Raw Ash Data
Matrix Spike of Non-Recycler
2,3,7,8-TETRACHLORODIBENZODIOXIN
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
OCTACHLORODIBENZOFURAN
TOTAL TETRACHLORODIBENZODIOXINS
TOTAL PENTACHLORODIBENZODIOXINS
TOTAL HEXACHLORODIBENZODIOXINS
TOTAL HEPTACHLORODIBENZODIOXINS
TOTAL TETRACHLORODIBENZOFURANS
TOTAL PENTACHLORODIBENZOFURANS
TOTAL HEXACHLORODIBENZOFURANS
TOTAL HEPTACHLORODIBENZOFURANS
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-19 (2,2',6-TRICHLOROBIPHENYL)
BZ-12 (3,4-DICHLOROBIPHENYL)(Surrogate)
BZ-18 (2,2',5-TRICHLOROBIPHENYL)
BZ-15, BZ-17
BZ-24, BZ-27
BZ-16, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
820 PG/G
1200 PG/G
780 PG/G
780 PG/G
890 PG/G
1500 PG/G
1600 PG/G
970 PG/G
510 PG/G
1300 PG/G
1300 PG/G
1400 PG/G
1600 PG/G
950 PG/G
3000 PG/G
1200 PG/G
2000 PG/G
1200 PG/G
1800 PG/G
3500 PG/G
2200 PG/G
7000 PG/G
6600 PG/G
7600 PG/G
4600 PG/G
45 NG/G
38 NG/G
19 NG/G
0.5 NG/G
129 NG/G
0.9 NG/G
1.7 NG/G
2.7 NG/G
14 NG/G
0.5 NG/G
1.7 NG/G
3.9 NG/G
2.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
0.8 NG/G
0.5 NG/G
2 NG/G
0.5 NG/G
G-40
*
su
su
LT
LT
INT
LT
LT
LT
LT
PL
LT
-------
Raw Ash Data
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-47 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,5'-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, OCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,5'-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-119 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-115
BZ-85, 4,4'-DDE
BZ-136
BZ-77, BZ-110
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-151 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-107 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-123, BZ-149
BZ-118
BZ-134
BZ-122 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-146
BZ-153
BZ-132, BZ-105
BZ-141 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-179
BZ-137
BZ-130, BZ-176
BZ-138
BZ-158
BZ-129
BZ-178
8.6 NG/G
3.8 NG/G
0.5 NG/G
0.5 NG/G
1.4 NG/G
0.5 NG/G
0.5 NG/G
13 NG/G
1 NG/G
1.1 NG/G
0.5 NG/G
1 5 NG/G
0.5 NG/G
12 NG/G
0.5 NG/G
0.5 NG/G
0.6 NG/G
0.5 NG/G
1.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1 NG/G
0.5 NG/G
7.3 NG/G
0.5 NG/G
1.6 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
8.3 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
8.4 NG/G
0.5 NG/G
G-47
*
LT
LT
LT
LT
LT
LT
EE
LT
LT
PL
LT
LT
PL
LT
*
LT
LT
PL
LT
LT
LT
PL
*
LT
PL
LT
LT
PL
LT
LT
PL
PL
LT
*
LT
-------
Raw Ash Data
BZ-175
BZ-187
BZ-183
BZ-128
BZ-167
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209(DECACHLOROBIPHENYL)(Surrogate)
PICES (Surrogates)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
SOLIDS, DRY
ACENAPHTHENE
ACENAPHTHYLENE
ACETOPHENONE
2-ACETYLAMINOFLUORENE
ALDRIN
4-AMINOBIPHENYL
ANTHRACENE
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(ghi)PERYLENE
39 NG/G
0.5 NG/G
1.7 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
8.6 NG/G
0.5 NG/G
1.2 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
1.1 NG/G
1 1 NG/G
128 NG/G
NG/G
33 NG/G
32 NG/G
39 NG/G
PERCENT
13000 |iG/KG
91 |iG/KG
1200 |iG/KG
9900 |iG/KG
5000 |iG/KG
9900 |iG/KG
1 1 0 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
100 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
G-42
LT
LT
PL
LT
LT
LT
LT
PL
LT
*
PL
LT
LT
LT
LT
PL
LT
PL
*
I\R
J
J
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
-------
Raw Ash Data
BENZO(a)PYRENE
BENZYL ALCOHOL
HCH,ALPHA
HCH,BETA
HCH,DELTA
HCH,GAMMA (LINDANE)
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
CHLORDANE, GAMMA ISOMER
4-CHLOROANILINE
CHLOROBENZILATE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
4,4'-DDD
4,4'-DDE
4,4'-DDT
DIALLATE
DIBENZOFURAN
DIBENZ(A,H)ANTHRACENE
DI-N-BUTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3'-DICHLOROBENZIDINE
2,4-DICHLOROPHENOL
2,6-DICHLOROPHENOL
DIELDRIN
DIETHYLPHTHALATE
DIMETHOATE
DIMETHYLPHTHALATE
P-DIMETHYLAMINO-AZOBENZENE
3,3'-DIMETHYLBENZIDINE
7,12-DIMETHYLBENZ(A)ANTHRACENE
2,4-DIMETHYLPHENOL
1,3-DINITROBENZENE
2-METHYL-4.6-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
DIPHENYLAMINE
DISULFOTON (Di-Syston)
ENDOSULFANI
ENDOSULFAN II
5000 jiG/KG
5000 jiG/KG
26 jiG/KG
26
26
26
5000
5000
24000
5000
5000
5000
5000
5000
23000
5000
17000
5000
240
5000
5000
50
5000
350
5000
5000
5000
5000
10000
5000
5000
5000
50
5000
9900
5000
9900
5000
5000
5000
5000
25000
25000
9100
5000
9900
5000
9900
5000
G-43
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
ENDOSULFAN SULFATE
ENDRIN
ENDRIN ALDEHYDE
ETHYL METHANESULFONATE
BIS(2-ETHYLHEXYL)PHTHALATE
FAMPHUR
FLUORANTHENE
FLUORENE
HEPTACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE (C-46)
HEXACHLOROCYCLOPENTADIENE (C-56)
HEXACHLOROETHANE
HEXACHLOROPROPENE
INDENO(1,2,3-cd)PYRENE
ISODRIN
ISOPHORONE
ISOSAFROLE
KEPONE
METHAPYRILENE
METHOXYCHLOR
METHYL METHANESULFONATE
METHYL PARATHION
3-METHYLCHOLANTHRENE
2-METHYLNAPHTHALENE
2-METHYL PHENOL
3. OR 4-METHYLPHENOL
NAPHTHALENE
1,4-NAPHTHOQUINONE
1-NAPHTHYLAMINE
2-NAPHTHYLAMINE
2-NITROANILINE
3-NITROANILINE
4-NITROANILINE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIETHYLAMINE
N-NITROSOSDIMETHYLAMINE
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-BUTYLAMINE
N-NITROSOMETHYL-ETHYLAMINE
N-NITROSOPIPERIDINE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSOPYRROLIDINE
5-NITRO-O-TOLUIDINE
DI-N-OCTYL PHTHALATE
PARATHION, ETHYL
5000
5000
5000 jiG/KG
9900
1000
9900
230
170 jiG/KG
5000
5000
5000
5000
5000
5000
5000
5000
9900
5000
5000
9900
50000
5000
5000
5000
5000
530
620
5000
2000
5000
5000
5000
25000
25000
9900
5000
5000
23000
9900
990
2500
5000
5000
99000
16000
5000
5000
5000
5000
G-44
LT
LT
LT
LT
BJ
LT
J
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
J
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
PENTACHLOROBENZENE
PENTACHLORONITROBENZENE
PENTACHLOROPHENOL
PHENACETIN
PHENANTHRENE
PHENOL
P-PHENYLENEDIAMINE
PHORATE
PRONAMIDE
PYRENE
SAFROLE
1,2,4,5-TETRACHLOROBENZENE
2,3,4,6-TETRACHLOROPHENOL
THIONAZIN
0-TOLUIDINE
TOXAPHENE
1,2,4-TRICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
SOLIDS, DRY
ARSENIC IN DRY SOLIDS
SELENIUM IN DRY SOLIDS
MERCURY IN DRY SOLIDS
BERYLLIUM IN DRY SOLIDS
SILVER IN DRY SOLIDS
BARIUM IN DRY SOLIDS
CADMIUM IN DRY SOLIDS
COBALT IN DRY SOLIDS
CHROMIUM IN DRY SOLIDS
COPPER IN DRY SOLIDS
IRON IN DRY SOLIDS
MANGANESE IN DRY SOLIDS
NICKEL IN DRY SOLIDS
STRONTIUM IN DRY SOLIDS
TITANIUM IN DRY SOLIDS
VANADIUM IN DRY SOLIDS
ZINC IN DRY SOLIDS
MOLYBDENUM IN DRY SOLIDS
LEAD IN DRY SOLIDS
ANTIMONY IN DRY SOLIDS
TIN IN DRY SOLIDS
THALLIUM IN DRY SOLIDS
ALUMINUM IN DRY SOLIDS
CALCIUM IN DRY SOLIDS
POTASSIUM IN DRY SOLIDS
MAGNESIUM IN DRY SOLIDS
SODIUM IN DRY SOLIDS
PYRIDINE
ALPHA-PICOLINE
5000 jiG/KG
5000 jiG/KG
25000 jiG/KG
9900 |iG/KG
1100 |iG/KG
20000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
15000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
990 |iG/KG
13000 |iG/KG
12000 |iG/KG
31 |iG/KG
PERCENT
69 MG/KG
1.2 MG/KG
0.1 MG/KG
10.4 MG/KG
8 MG/KG
499 MG/KG
10 MG/KG
97 MG/KG
123 MG/KG
388 MG/KG
3820 MG/KG
246 MG/KG
109 MG/KG
115 MG/KG
1930 MG/KG
125 MG/KG
859 MG/KG
16 MG/KG
128 MG/KG
MG/KG
103 MG/KG
MG/KG
87300 MG/KG
147000 MG/KG
3230 MG/KG
2530 MG/KG
2970 MG/KG
660 |iG/KG
150 |iG/KG
G-45
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
I\R
LT
I\R
I\R
J
J
-------
Raw Ash Data
ANILINE 5000 jaG/KG LT
BENZIDINE 24000 jaG/KG LT
ENDRINKETONE 500 jaG/KG LT
1,3,5-TRINITROBENZENE 5000 |iG/KG LT
4-NITROQUINOLINE 1-OXIDE 18000|iG/KG LT
CHLORDANE, ALPHA ISOMER 24000 |iG/KG LT
* - matrix spike of 10 ng/g
G-46
-------
Raw Ash Data
Matrix Spike Duplicate of Non-Recycler
2,3,7,8-TETRACHLORODIBENZODIOXIN
1,2,3,7,8-PENTACHLORODIBENZODIOXIN
1,2,3,4,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,6,7,8-HEXACHLORODIBENZODIOXIN
1,2,3,7,8,9-HEXACHLORODIBENZODIOXIN
1,2,3,4,6,7,8-HEPTACHLORODIBENZODIOXIN
OCTACHLORODIBENZODIOXIN
2,3,7,8-TETRACHLORODIBENZOFURAN
1,2,3,7,8-PENTACHLORODIBENZOFURAN
2,3,4,7,8-PENTACHLORODIBENZOFURAN
1,2,3,4,7,8-HEXACHLORODIBENZOFURAN
1,2,3,6,7,8-HEXACHLORODIBENZOFURAN
2,3,4,6,7,8-HEXACHLORODIBENZOFURAN
1,2,3,7,8,9-HEXACHLORODIBENZOFURAN
1,2,3,4,6,7,8-HEPTACHLORODIBENZOFURAN
1,2,3,4,7,8,9-HEPTACHLORODIBENZOFURAN
OCTACHLORODIBENZOFURAN
TOTAL TETRACHLORODIBENZODIOXINS
TOTAL PENTACHLORODIBENZODIOXINS
TOTAL HEXACHLORODIBENZODIOXINS
TOTAL HEPTACHLORODIBENZODIOXINS
TOTAL TETRACHLORODIBENZOFURANS
TOTAL PENTACHLORODIBENZOFURANS
TOTAL HEXACHLORODIBENZOFURANS
TOTAL HEPTACHLORODIBENZOFURANS
BZ-1 (2-CHLOROBIPHENYL)
BZ-2 (3-CHLOROBIPHENYL)
BZ-3 (4-CHLOROBIPHENYL)
BZ-10, BZ-4
2,4,5,6-TETRACHLORO-m-XYLENE (Surrogate)
BZ-7, BZ-9
BZ-6 (2,3'-DICHLOROBIPHENYL)
BZ-8, BZ-5
HEXACHLOROBENZENE
BZ-19 (2,2',6-TRICHLOROBIPHENYL)
BZ-12 (3,4-DICHLOROBIPHENYL)(Surrogate)
BZ-18 (2,2',5-TRICHLOROBIPHENYL)
BZ-15, BZ-17
BZ-24, BZ-27
BZ-16, BZ-32
BZ-29 (2,4,5-TRICHLOROBIPHENYL)
BZ-26 (2,3',5-TRICHLOROBIPHENYL)
BZ-25 (2,3',4-TRICHLOROBIPHENYL)
BZ-31 (2,4',5-TRICHLOROBIPHENYL)
BZ-28 (2,4,4'-TRICHLOROBIPHENYL)
BZ-20, BZ-33, BZ-53
BZ-51 (2,2',4,6'-TETRACHLOROBIPHENYL)
BZ-22 (2,3,4'-TRICHLOROBIPHENYL)
790 PG/G
1200 PG/G
770 PG/G
750 PG/G
860 PG/G
1400 PG/G
1500 PG/G
950 PG/G
450 PG/G
1100 PG/G
1200 PG/G
1300 PG/G
1400 PG/G
880 PG/G
2300 PG/G
1000 PG/G
1700 PG/G
1200 PG/G
1700 PG/G
3300 PG/G
2000 PG/G
6300 PG/G
5400 PG/G
6400 PG/G
3600 PG/G
42 NG/G
37 NG/G
21 NG/G
0.5 NG/G
146 NG/G
1.3 NG/G
4.1 NG/G
3.5 NG/G
1 1 NG/G
4.3 NG/G
3.8 NG/G
3.8 NG/G
43 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
1.6 NG/G
0.5 NG/G
2.1 NG/G
0.5 NG/G
9.4 NG/G
G-47
*
su
su
LT
INT
LT
LT
LT
LT
LT
LT
*
-------
Raw Ash Data
BZ-45 (2,2',3,6-TETRACHLOROBIPHENYL)
BZ-46 (2,2',3,6'-TETRACHLOROBIPHENYL)
BZ-39 (3,4',5-TRICHLOROBIPHENYL)
BZ-52 (2,2',5,5'-TETRACHLOROBIPHENYL)
BZ-49 (2,2',4,5'-TETRACHLOROBIPHENYL)
BZ-47 (2,2',4,4'-TETRACHLOROBIPHENYL)
BZ-48 (2,2',4,5-TETRACHLOROBIPHENYL)
BZ-44 (2,2',3,51-TETRACHLOROBIPHENYL)
BZ-37, BZ-42, BZ-59
BZ-41, BZ-64
BZ-40 (2,2',3,3'TETRACHLOROBIPHENYL)
BZ-67 (2,3',4,5-TETRACHLOROBIPHENYL)
BZ-63, OCS
BZ-74 (2,4,4',5-TETRACHLOROBIPHENYL)
BZ-70 (2,3',4',5-TETRACHLOROBIPHENYL)
BZ-66, BZ-95
BZ-91 (2,2',3,4',6-PENTACHLOROBIPHENYL)
BZ-56, BZ-60
BZ-92 (2,2',3,5,51-PENTACHLOROBIPHENYL)
BZ-84 (2,2',3,3',6-PENTACHLOROBIPHENYL)
BZ-90, BZ-101
BZ-99 (2,2',4,4',5-PENTACHLOROBIPHENYL)
BZ-119 (2,3',4,4',6-PENTACHLOROBIPHENYL)
BZ-83 (2,2',3,3',5-PENTACHLOROBIPHENYL)
BZ-97 (2,2',3',4,5-PENTACHLOROBIPHENYL)
BZ-87, BZ-115
BZ-85, 4,4'-DDE
BZ-136
BZ-77, BZ-110
BZ-82 (2,2',3,3',4-PENTACHLOROBIPHENYL)
BZ-151 (2,2',3,5,5',6-HEXACHLOROBIPHENYL
BZ-135
BZ-107 (2,3,3',4',5-PENTACHLOROBIPHENYL)
BZ-123, BZ-149
BZ-118
BZ-134
BZ-122 (2',3,3',4,5-PENTACHLOROBIPHENYL)
BZ-146
BZ-153
BZ-132, BZ-105
BZ-141 (2,2',3,4,5,5'-HEXACHLOROBIPHENYL
BZ-179
BZ-137
BZ-130, BZ-176
BZ-138
BZ-158
BZ-129
BZ-178
BZ-175
1 NG/G
0.5 NG/G
0.5 NG/G
1.3 NG/G
0.5 NG/G
0.9 NG/G
0.5 NG/G
0.9 NG/G
1.2 NG/G
0.5 NG/G
9.7 NG/G
0.5 NG/G
9.4 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
1.9 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
1 NG/G
0.5 NG/G
8.3 NG/G
0.5 NG/G
1.9 NG/G
0.5 NG/G
0.5 NG/G
0.8 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
9.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.9 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
9.3 NG/G
0.5 NG/G
45 NG/G
G-48
LT
LT
LT
LT
LT
LT
*
PL
LT
LT
LT
PL
LT
*
PL
PL
LT
PL
LT
LT
LT
LT
*
LT
PL
LT
LT
LT
LT
LT
PL
PL
LT
*
LT
-------
Raw Ash Data
BZ-187
BZ-183
BZ-128
BZ-167
BZ-185
BZ-174
BZ-177
BZ-171, BZ-202
BZ-156
BZ-173, BZ-157, IUPAC-201
BZ-172
BZ-197
BZ-180
BZ-193
BZ-191
IUPAC-200
MIREX
BZ-170, BZ-190
IUPAC-199
BZ-203, BZ-196
BZ-189
BZ-195
BZ-194
BZ-206
BZ-209(DECACHLOROBIPHENYL)(Surrogate)
PICES (Surrogates)
BZ-14 (3,5-DICHLOROBIPHENYL)
BZ-65 (2,3,5,6-TETRACHLOROBIPHENYL)
BZ-166, BZ-175
SOLIDS, DRY
ACENAPHTHENE
ACENAPHTHYLENE
ACETOPHENONE
2-ACETYLAMINOFLUORENE
ALDRIN
4-AMINOBIPHENYL
ANTHRACENE
AROCLOR 1016
AROCLOR 1221
AROCLOR 1232
AROCLOR 1242
AROCLOR 1248
AROCLOR 1254
AROCLOR 1260
BENZO(a)ANTHRACENE
BENZO(b)FLUORANTHENE
BENZO(k)FLUORANTHENE
BENZO(ghi)PERYLENE
BENZO(a)PYRENE
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
9.3 NG/G
0.5 NG/G
1.1 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.5 NG/G
0.7 NG/G
0.8 NG/G
1 1 NG/G
141 NG/G
NG/G
36 NG/G
40 NG/G
45 NG/G
PERCENT
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
9900 |iG/KG
5000 |iG/KG
9900 |iG/KG
1 1 0 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
99000 |iG/KG
100 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
5000 |iG/KG
G-49
LT
LT
LT
PL
LT
LT
LT
LT
LT
LT
*
PL
LT
LT
LT
LT
PL
LT
LT
PL
*
I\R
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
-------
Raw Ash Data
BENZYL ALCOHOL
HCH,ALPHA
HCH,BETA
HCH,DELTA
HCH,GAMMA (LINDANE)
4-BROMOPHENYL PHENYL ETHER
BUTYL BENZYL PHTHALATE
CHLORDANE, GAMMA ISOMER
4-CHLOROANILINE
CHLOROBENZILATE
BIS(2-CHLOROETHOXY)METHANE
BIS(2-CHLOROETHYL)ETHER
BIS(2-CHLOROISOPROPYL)ETHER
4-CHLORO-3-METHYLPHENOL
2-CHLORONAPHTHALENE
2-CHLOROPHENOL
4-CHLOROPHENYL PHENYL ETHER
CHRYSENE
4,4'-DDD
4,4'-DDE
4,4'-DDT
DIALLATE
DIBENZOFURAN
DIBENZ(A,H)ANTHRACENE
DI-N-BUTYL PHTHALATE
1,2-DICHLOROBENZENE
1,3-DICHLOROBENZENE
1,4-DICHLOROBENZENE
3,3'-DICHLOROBENZIDINE
2,4-DICHLOROPHENOL
2,6-DICHLOROPHENOL
DIELDRIN
DIETHYLPHTHALATE
DIMETHOATE
DIMETHYLPHTHALATE
P-DIMETHYLAMINO-AZOBENZENE
3,3'-DIMETHYLBENZIDINE
7,12-DIMETHYLBENZ(A)ANTHRACENE
2,4-DIMETHYLPHENOL
1,3-DINITROBENZENE
2-METHYL-4.6-DINITROPHENOL
2,4-DINITROPHENOL
2,4-DINITROTOLUENE
2,6-DINITROTOLUENE
DIPHENYLAMINE
DISULFOTON (Di-Syston)
ENDOSULFANI
ENDOSULFAN II
ENDOSULFAN SULFATE
5000 jiG/KG
26 jiG/KG
26 jiG/KG
26
26
5000
5000
24000
5000
5000
5000
5000
5000
5000
5000
5000
5000
240
5000
5000
50
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
50
5000
9900
5000
9900
5000
5000
5000
5000
25000
25000
5000
5000
9900
5000
9900
5000
5000
G-50
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
ENDRIN
ENDRIN ALDEHYDE
ETHYL METHANESULFONATE
BIS(2-ETHYLHEXYL)PHTHALATE
FAMPHUR
FLUORANTHENE
FLUORENE
HEPTACHLOR
HEPTACHLOR EPOXIDE
HEXACHLOROBENZENE
HEXACHLOROBUTADIENE (C-46)
HEXACHLOROCYCLOPENTADIENE (C-56)
HEXACHLOROETHANE
HEXACHLOROPROPENE
INDENO(1,2,3-cd)PYRENE
ISODRIN
ISOPHORONE
ISOSAFROLE
KEPONE
METHAPYRILENE
METHOXYCHLOR
METHYL METHANESULFONATE
METHYL PARATHION
3-METHYLCHOLANTHRENE
2-METHYLNAPHTHALENE
2-METHYL PHENOL
3- OR 4-METHYLPHENOL
NAPHTHALENE
1,4-NAPHTHOQUINONE
1-NAPHTHYLAMINE
2-NAPHTHYLAMINE
2-NITROANILINE
3-NITROANILINE
4-NITROANILINE
NITROBENZENE
2-NITROPHENOL
4-NITROPHENOL
N-NITROSODIETHYLAMINE
N-NITROSOSDIMETHYLAMINE
N-NITROSODIPHENYLAMINE
N-NITROSODI-N-BUTYLAMINE
N-NITROSOMETHYL-ETHYLAMINE
N-NITROSOPIPERIDINE
N-NITROSO-DI-N-PROPYLAMINE
N-NITROSOPYRROLIDINE
5-NITRO-O-TOLUIDINE
DI-N-OCTYL PHTHALATE
PARATHION, ETHYL
PENTACHLOROBENZENE
5000
5000
9900
1000
9900
230
5000
5000
5000
5000
5000
5000
5000
5000
5000
9900
5000
5000
9900
50000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
5000
25000
25000
9900
5000
5000
25000
9900
990
2500
5000
5000
99000
5000
5000
5000
5000
5000
5000
LT
LT
LT
BJ
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
-------
Raw Ash Data
PENTACHLORONITROBENZENE
PENTACHLOROPHENOL
PHENACETIN
PHENANTHRENE
PHENOL
P-PHENYLENEDIAMINE
PHORATE
PRONAMIDE
PYRENE
SAFROLE
1,2,4,5-TETRACHLOROBENZENE
2,3,4,6-TETRACHLOROPHENOL
THIONAZIN
0-TOLUIDINE
TOXAPHENE
1,2,4-TRICHLOROBENZENE
2,4,5-TRICHLOROPHENOL
2,4,6-TRICHLOROPHENOL
PYRIDINE
ALPHA-PICOLINE
ANILINE
BENZIDINE
ENDRIN KETONE
1,3,5-TRINITROBENZENE
4-NITROQUINOLINE 1-OXIDE
CHLORDANE, ALPHA ISOMER
* - matrix spike of 10 ng/g
5000
25000
9900
1100
5000
5000
5000
5000
15000
5000
5000
5000
5000
5000
990
5000
12000
5000
50000
50000
5000
24000
500
5000
18000
24000
LT
LT
J
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
LT
G-52
-------
Raw Ash Data
Synthetic QC for Metals
SOLIDS, DRY
ARSENIC IN DRY SOLIDS
SELENIUM IN DRY SOLIDS
MERCURY IN DRY SOLIDS
BERYLLIUM IN DRY SOLIDS
SILVER IN DRY SOLIDS
BARIUM IN DRY SOLIDS
CADMIUM IN DRY SOLIDS
COBALT IN DRY SOLIDS
CHROMIUM IN DRY SOLIDS
COPPER IN DRY SOLIDS
IRON IN DRY SOLIDS
MANGANESE IN DRY SOLIDS
NICKEL IN DRY SOLIDS
STRONTIUM IN DRY SOLIDS
TITANIUM IN DRY SOLIDS
VANADIUM IN DRY SOLIDS
ZINC IN DRY SOLIDS
MOLYBDENUM IN DRY SOLIDS
130
160
5.41
77
78
184
117
83
88
86
6160
218
127
40
173
61
131
77
PERCENT
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
MG/KG
I\R
LT
G-53
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TECHNICAL REPORT DATA
Please read Instructions on the reverse before completing)
1. REPORT NO.
EPA/600/R-97-134b
3. RECIPIENT'S ACCESSION NO.
4. TITLE AND SUBTITLE
Evaluation of Emissions from the Open Burning of
Household Waste in Barrels, Volume 2.
Appendices A-G
5. REPORT DATE
November 1997
6. PERFORMING ORGANIZATION CODE
7. AUTHOR(S)
Paul M. Lemieux
8.PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AND ADDRESS
10. PROGRAM ELEMENT NO.
See Block 12
11. CONTRACT/GRANT NO.
68-D4-0005, Acurex
Environmental Corporation
1 OYPE OF'REPORT ANtTpfRloD COVERED
12. SPONSORING AGENCY NAME AND ADDRESS
EPA, Office of Research and Development
Air Pollution Prevention and Control Division
Research Triangle Park, NC 27711
Final: 9/95 - 4/97
14. SPONSORING AGENCY CODE
EPA/600/13
15. SUPPLEMENTARY NOTES
APPCD project officer is Paul M. Lemieux, Mail Drop 65, 919/541-
0962. Volume 1 is the basic technical report.
16. ABSTRACT
The report gives results of a detailed emissions characterization study, undertaken to examine,
characterize, and quantify emissions from the simulated burning of household waste material in
barrels. The study evaluated two waste streams: that of an avid recycler, who removed most of the
recyclable content from the waste stream prior to combustion; and that of a non-recycler, who
combusts the entire stream of household waste. Estimated emissions were developed in units of
mass emitted per mass of waste burned. Continuous gas samples were analyzed for oxygen, carbon
dioxide, carbon monoxide, nitric oxide, and total hydrocarbons. Gas-phase samples were collected
using SUMMA canisters and analyzed by gas chromatography/mass spectroscopy (GC/MS) for
volatile organic compounds (VOCs). Extractive samples from the combined particulate- and gas-
phase were analyzed for semivolatile organic compounds (SVOCs), polycyclic aromatic
hydrocarbons (PAHs), polychlorinated biphenyls (PCBs), chlorobenzenes (CBs), polychlorinated
dibenzo-p-dioxins and polychlorinated dibenzofurans (PCDDs/PCDFs), aldehydes and ketones,
hydrogen chloride (HC1), hydrogen cyanide (HCN), and metals. Emissions of particulate matter
(PM) with aerodynamic diameters of 10 micrometers or less (PM10) and of 2.5 micrometers or less
(PM2.5) were also measured.
17.
KEY WORDS AND DOCUMENT ANALYSIS
DESCRIPTORS
b. IDENTIFIERS/OPEN ENDED TERMJ
c. COSATI Field/Group
Pollution
Combustion
Garbage
Wastes
Sewage
Refuse
Emission
Circulation
Pollution Prevention
Stationary Sources
Household Wastes
Recycling
13B
21B
14G
18. DISTRIBUTION STATEMENT
Release to Public
19. SECURITY CLASS (This Report)
Unclassified
21. NO. OF PAGES
134
20. SECURITY CLASS (This Page)
Unclassified
22. PRICE
EPA Form 2220-1 (9-73)
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