EPA/600/R-12/057
April 2012
Environmental Technology Verification
Pesticide Spray Drift Reduction
Technologies for Row and Field Crops
EVALUATION OF THE VERIFICATION PROTOCOL FOR LOW
AND HIGH SPEED WIND TUNNEL TESTING
Prepared by
RTI International
BRTI
INTERNATIONAL
USDA-ARS Alien Science & Technology
USDA
ALION
SCICNCE AND TtCHNOlOGY
Under a Cooperative Agreement with
U.S. Environmental Protection Agency
EW EW ET
-------
Environmental Technology Verification
Report
Pesticide Spray Drift Reduction
Technologies
EVALUATION OF THE VERIFICATION PROTOCOL FOR
LOW AND HIGH SPEED WIND TUNNEL TESTING
Prepared by
RTI International
Alion Science and Technology
USDA-ARS College Station
EPA EP-C-05-060/TO-52
EPA Project Manager
Michael Kosusko
Air Pollution Prevention and Control Division
National Risk Management Research Laboratory
Office of Research and Development
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
April 2012
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Notice
This document was prepared by RTI International (RTI) and its subcontractor Alion Science &
Technology (Alion), with funding from EPA EP-C-05-060/TO-52 from the U.S. Environmental
Protection Agency (EPA). The document has completed RTI/EPA's peer and administrative reviews and
has been approved for publication. Mention of corporation names, trade names, or commercial products
does not constitute endorsement or recommendation for use of specific products.
RTI International is a trade name of Research Triangle Institute.
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Foreword
The Environmental Technology Verification (ETV) Program, established by the U.S. Environmental
Protection Agency (EPA), is designed to accelerate the development and commercialization of new or
improved technologies through third-party verification and reporting of performance. The goal of the
ETV Program is to verify the performance of commercially ready environmental technologies through the
evaluation of objective and quality-assured data in order to provide potential purchasers and permitters an
independent, credible assessment of the technology that they are buying or permitting.
EPA established a Drift Reduction Technology (DRT) project under EPA's Environmental and
Sustainable Technology (ESTE) program, which itself is part of EPA's Environmental Technology
Verification (ETV) Program. Before the pesticide spray DRT generic verification protocol (GVP) is used
for verification testing, the draft protocol requires testing and evaluation. Results of testing will be used
to revise the draft DRT GVP. This report describes the evaluation of the draft protocol for pesticide spray
DRTs verification at low and high speeds.
All testing was performed in accordance with approved test/quality assurance plans that implement the
requirements of the generic verification protocol at the test laboratory.
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Availability of Report
Copies of this report are available from the following:
• RTI International
Engineering and Technology Unit
P.O. Box 12194
Research Triangle Park, NC 27709-2194
• U.S. Environmental Protection Agency
Air Pollution Prevention and Control Division (E343-02)
109 T. W. Alexander Drive
Research Triangle Park, NC 27711
Web Site: http://www.epa.gov/etv/vt-apc.html. (electronic copies)
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Executive Summary
Pesticide spray drift is defined as the movement of spray droplets through the air at the time of application
or soon thereafter from the target site to any non- or off-target site, excluding pesticide movements by
erosion, migration, volatility, or windblown soil particles after application. EPA established a Drift
Reduction Technology (DRT) project under EPA's Environmental and Sustainable Technology (ESTE)
program, which itself is part of EPA's Environmental Technology Verification (ETV) Program. Before
the pesticide spray DRT generic verification protocol (GVP) is used for verification testing, the draft
protocol requires testing and evaluation. Results from testing will be used to revise the draft DRT GVP.
This report describes the evaluation of the draft protocol for pesticide spray DRTs verification at low and
high speeds. This report provides stakeholders the validation data in a transparent manner so they can
provide U.S. EPA suggestions to revise and improve the GVP.
The goal of the DRT project is to test and verify the effectiveness of a variety of spray DRTs, and has the
ultimate goal of reducing unintentional exposures during the pesticide application process. In 2007, U.S.
EPA completed a draft protocol for the verification of pesticide spray DRTs for row and field crops.
Draft Generic Verification Protocol for the Verification of Pesticide Spray Drift Reduction Technologies
for Row and Field Crops (http://www.epa.gov/etv/pubs/600etv07021.pdf) was developed by U.S. EPA
with input and commentary from stakeholders that included academia, industry, and other government
agencies.
For the low- and high-speed tests, the validity of and applicability of the pesticide spray DRT protocol
were evaluated using two test nozzles and one reference nozzle. The two candidate nozzles tested were
an All 1003-VS nozzle (Teejet Technologies, Wheaton, IL) and a ULD 120-04 nozzle (Hypropumps,
New York, NY). The reference nozzle used for testing was an ASABE S572 nozzle associated with the
fine/medium boundary. Measurements of the droplet size distribution produced by the candidate test
systems were compared to the reference spray system based on the ASABE S572 standard for droplet
size. Wind tunnel and spray liquid conditions measurements were supplemental measures that established
the bounds of the spray size distribution data. Additionally, spray flux and deposition measurements were
collected during low-speed tests. The low-speed measurements were conducted by Alion personnel in a
low-speed wind tunnel environment in EPA's Aerosol Test Facility (ATF) at Research Triangle Park,
NC. High-speed tests were conducted in the high-speed wind tunnel (HSWT) at the USDA-ARS in
College Station, TX.
Data quality indicator goals (DQIGs) were established in the draft DRT protocol as criteria that provide
qualitative and quantitative attributes that useful for evaluating and, in some cases, controlling
environmental data quality. Evaluation of the feasibility of these criteria and identifying realistic
adjustment for the protocol were key goals of this testing effort.
The low-speed wind tunnel tests did not achieve all the spray size distribution, spray flux, and spray
deposition DQIGs included in the draft protocol. A combination of the nozzle orientation, low wind
speed, and large droplets produced by the nozzles contributed to the failure to meet numerous DQIGs.
However, the data collected were adequate for revising the low-speed wind tunnel portion of the DRT
GVP, the main goal of this research.
The high-speed wind tunnel tests achieved the most important DQIGs. Two DQIGs were not achieved.
The spray liquid and ambient temperature difference was greater than 2 °C for some tests. Also, spray
liquid flow rates were not recorded. Failure to achieve these two DQIGs did not affect overall data
quality or our ability to update the high-speed wind tunnel portion of the DRT GVP.
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Table of Contents
Page
1.0 Introduction 11
2.0 Test Description 12
2.1 Description and identification of DRTs 13
2.2 Spray material 13
2.3 Procedures and methods used in testing 13
2.3.1 Test facilities 13
2.3.2 Droplet sizing measurements 15
2.3.2.1 Spray characterization measurements - low-speed wind tunnel 16
2.3.2.2 Droplet sizing 2 m downwind - low-speed wind tunnel 16
2.3.2.3 Droplet sizing 60 cm downwind- high-speed wind tunnel 17
2.3.3 Spray flux and deposition measurements - Low-speed wind tunnel 17
3.0 Results 19
3.1 Low-speed wind tunnel test results 19
3.1.1 Spray characterization results 19
3.1.2 Droplet sizing 2 m downwind results 20
3.1.3 Spray flux and deposition results 22
3.2 High-speed wind tunnel test results 24
4.0 Verification of Performance 26
4.1 Quality assurance 26
4.1.1 Deviations 31
5.0 References 33
Appendix A LSWT Test Data
Appendix B HSWT Test Data
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
List of Figures
Page
Figure 1. Nozzles under test. Used with permission 13
Figure 2. EPA's aerosol wind tunnel (AWT) 14
Figure 3. AWT setup for low-speed DRT tests 15
Figure 4. Overview of HSWT with enclosure removed for clarity 15
Figure 5. Schematic diagram of the set up for droplet sizing measurements 2 m downwind 16
Figure 6. LSWT spray characterization results under static wind conditions 19
Figure 7. Example of LSWT spray characterization at the 2-meter flux plane and 20 cm height 22
Figure 8. LSWT spray flux 2 meters from nozzle (flux vs. height for three nozzles) 23
List of Tables
Table 1. Spray characterization droplet size data (means ± standard deviations) 60 cm below
nozzle 19
Table 2. Droplet size data (means ± standard deviations) 2 m downwind of nozzle at 1 m/s wind
speed 20
Table 3. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution
temperature for droplet sizing measurements (means ± standard deviations) at 2 m
downwind 21
Table 4. Results from flux measurements as ten-thousandths of applied (fraction x 104) at 2 m
downwind 22
Table 5. Results from deposition measurements as ten-thousandths of applied 23
Table 6. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution
temperature for flux and deposition measurements 24
Table 7. Droplet size data 60 m downwind of nozzle at specified wind speed 24
Table 8. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution
temperature for droplet sizing measurements (means ± standard deviations) at 60 m
downwind 25
Table 9. Data quality indicator goals for high-speed wind tunnel tests 26
Table 10. Data quality indicator goals for low-speed wind tunnel tests 28
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
List of Abbreviations and Acronyms
ADQ audit of data quality
ANSI American National Standards Institute
AS ABE American Society of Agricultural and Biological Engineers
ASHRAE American Society of Heating, Refrigerating, and Air Conditioning Engineers
ASME American Society of Mechanical Engineers
ASTM ASTM International, formerly American Society for Testing and Materials
ATF Aerosol Test Facility
AWT aerosol wind tunnel
°C degrees Celsius
cfm cubic feet per minute
cm centimeter
cp centipoise
CV coefficient of variance
DQIG data quality indicator goal
DQO data quality obj ective
DRT drift reduction technology
DVO.I droplet diameter (jim) at which 10% of the spray volume is contained in smaller
droplets
droplet diameter (|im) at which 50% of the spray volume is contained in smaller
droplets
droplet diameter (|im) at which 90% of the spray volume is contained in smaller
droplets
dyne/cm dynes per centimeter
EC emulsifiable concentrates
EPA United States Environmental Protection Agency
ESTE Environmental and Sustainable Technology Evaluations
ETV Environmental Technology Verification
fpm feet per minute
ft foot
gal/acre gallons per acre
gpm gallons per minute
GVP generic verification protocol
HELOS helium neon laser optical system
HETS human exposure test section
HSWT high-speed wind tunnel
Hz hertz
D
'vO.5
D
V0.9
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
in. inches
ISO International Standards Organization
kPa kilopascal
L liter
LSWT low-speed wind tunnel
m meters
mph miles per hour
min minute
mg milligram
mL milliliter
mm millimeter
ms millisecond
m/s meters per second
NIS nonionic surfactant
NIST National Institute of Standards and Technology
uL microliter
um microns
OPP Office of Pesticide Programs
ORD Office of Research and Development
PE performance evaluation
PES performance evaluation system
PMT photo multiplier transistor
psi pounds per square inch
QA quality assurance
QC quality control
QM quality manager
QMP quality management plan
QSM quality system manual
RH relative humidity
RTI Research Triangle Institute
s second
SD standard deviation
SNR signal to noise ratio
SOP standard operating procedure
STS sampler test section
TSA technical systems audit
T/QAP test and quality assurance plan
USDA-ARS United States Department of Agriculture - Agricultural Research Service
v/v volume/volume
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
Acknowledgments
The authors acknowledge the support of all those who helped plan and conduct the protocol evaluation
activities. In particular, we would like to thank Michael Kosusko, U.S. Environmental Protection
Agency's (EPA's) project officer, Bob Wright, EPA's quality manager, both of EPA's National Risk
Management Research Laboratory in Research Triangle Park, NC, and Clint Hoffman and Brad Fritz,
USDA-ARS, College Station, TX, for providing access to the USDA-ARS high-speed wind tunnel.
10
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
1.0 Introduction
Pesticide spray drift is defined as the movement of spray droplets through the air at the time of application
or soon thereafter from the target site to any non- or off-target site, excluding pesticide movements by
erosion, migration, volatility, or windblown soil particles after application. EPA established a Drift
Reduction Technology (DRT) project under EPA's Environmental and Sustainable Technology (ESTE)
program, which itself is part of EPA's Environmental Technology Verification (ETV) Program. The
objective of the ETV Program is to verify, with high data quality, the performance of technologies that
reduce pollution. The goal of the DRT project is to test and verify the effectiveness of a variety of spray
DRTs, and has the ultimate goal of reducing unintentional exposures during the pesticide application
process. In 2007, U.S. EPA completed a draft protocol for the verification of pesticide spray DRTs for
row and field crops. Draft Generic Verification Protocol for the Verification of Pesticide Spray Drift
Reduction Technologies for Row and Field Crops (http://www.epa.gov/etv/pubs/600etv07021.pdf) was
developed by U.S. EPA with input and commentary from stakeholders that included academia, industry,
and other government agencies.
Before ETV can implement the pesticide spray DRT generic verification protocol (GVP) for verification
testing, the draft protocol requires testing and evaluation. This report describes the evaluation of the draft
protocol for pesticide spray DRTs verification at low- and high-speeds. EPA, RTI, vendors, test facilities,
and other stakeholders will use this report to evaluate the pesticide spray DRT protocol and suggest
changes that will provide improvements.
ETV testing to validate the draft DRT protocol was conducted during a series of low-speed wind tunnel
tests in June 2009 by Alion Science & Technology, under contract with RTI, and high-speed wind tunnel
tests conducted in March 2009 by the United States Department of Agriculture - Agricultural Research
Service (USDA-ARS).
For the tests described here, the pesticide spray DRT protocol was evaluated for both low- and high-speed
applications, using two test nozzles and one reference nozzle. Low-speed is defined as a speed of the air
in the wind tunnel crossing the nozzle representative of ground application and high-speed is defined as
speed of the air in the wind tunnel crossing the nozzle representative of aerial application. The purpose of
this testing was to gather information and data for evaluating the applicability of the pesticide spray DRT
protocol for successfully testing commercially ready pesticide spray DRT nozzles that will be used for
aerial spraying and ground applications. Evaluation of the protocol through spray liquid formulation
modifications to the viscosity, surface tension or other characteristics was not conducted.
Section 2 of this report documents the DRTs tested, procedures used for the tests and the conditions over
which the tests were conducted. The results of the test are summarized and discussed in Section 3,
Quality Assurance and protocol recommendations are discussed in Section 4, and references are presented
in Section 5.
This report contains summary information and data from the tests; however, as the purpose of these tests
is to verify the protocol and test plan, no verification statement is included. Complete documentation of
the test results is provided in a separate data package report and an audit of data quality report. These
reports include the raw test data from product testing and supplemental testing, equipment calibrations
results, and quality assurance (QA) and quality control (QC) activities and results. Complete
documentation of QA/QC activities and results, raw test data, and equipment calibrations results are
retained in Alion and USDA files for seven years. All files and records will also be stored at U.S. EPA
indefinitely. Helium neon laser optical system (HELOS) data are included in Appendices A and B of
this report.
11
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
2.0 Test Description
The low-speed measurements in this report were conducted by Alion personnel in a low-speed wind
tunnel (LSWT) environment in EPA's Aerosol Test Facility (ATF) in Research Triangle Park, NC. High-
speed tests were conducted in the high-speed wind tunnel (HSWT) at the USDA-ARS in College Station,
TX. For the low- and high-speed tests, the validity of and applicability of the pesticide spray DRT
protocol were evaluated using two test nozzles and one reference nozzle. Measurements of the droplet
size distribution produced by the candidate test systems were compared to the reference spray system
based on the ASABE S572 standard for droplet size.
The DRTs were tested in accordance with Draft Generic Verification Protocol for the Verification of
Pesticide Spray Drift Reduction Technologies for Row and Field Crops1, Test/QA Plan for the Evaluation
of the Verification Protocol for High Speed Pesticide Spray Drift Reduction Technologies for Row and
Field Crops2 and Test/QA Plan for the Evaluation of the Verification Protocol for Low Speed Pesticide
Spray Drift Reduction Technologies for Row and Field Crops.3 These documents incorporated all
requirements for quality management, QA, procedures for product selection, auditing of the test
laboratories, and reporting format. The draft generic verification protocol describes the overall
procedures used for verification testing and defines the data quality objectives (DQOs). The test/QA
plans (T/QAPs) detail how the test organizations implemented and met the requirements of the protocol.
The primary performance measure for the evaluation of the pesticide spray DRT protocol will be derived
from droplet size distribution measurements. Droplet size is one of the most important factors affecting
spray applications, efficacy and drift potential. All nozzles and atomizers produce a range of droplet sizes
within a given spray. This droplet size spectrum (or distribution) typically may include some relatively
small droplets that may be more prone to drift than are their larger counterparts. There is general
agreement in the literature that droplets with diameter below less than 200um often pose the greatest risk
of spray drift in conventional applications. Therefore, minimizing the proportion of the spray volume that
is contained in droplets of this size may help mitigate spray drift risk. Some nozzles are more effective
than are others in producing narrower droplet size spectra with fewer small ("fine") droplets.
The basic experimental design was to measure the droplet size spectrum under targeted test conditions
with the DRT operating at the specified spray pressure, air speed, and the ambient environmental
conditions. Droplet size spectrum is the critical measurement for these tests. Droplet size measurements
of interest are the Dv0 5, Dv01, and Dv0 9. Dv0 5 is the volume median diameter (|om) where 50% of the
spray volume is contained in droplets of smaller diameter. Similarly, Dv01 and Dv0 9 describe the
percentage (10% or 90%, respectively) of the droplet volume in the specified size or less. Wind tunnel
and spray liquid conditions measurements are supplemental measures that establish the bounds of the
spray size distribution data.
Spray flux and deposition measurements are only applicable to the low-speed wind tunnel tests. For the
spray flux tests, monofilament lines approximately 2 mm in diameter were used as sample collectors.
These were extended horizontally across the wind tunnel at seven heights starting at 10 cm above the
synthetic turf that was on the wind tunnel floor and spaced in 10 cm increments. Droplet size was
measured 2 m downwind of the spray nozzle at the same seven heights as the flux measurements
Off-site spray drift and resulting downwind deposition of pesticide can be hazardous to nearby non-target
receptors. The results of testing to be conducted under this program are to be used to estimate downwind
deposition. For example, the testing results from wind tunnel testing (droplet size distribution and spray
flux) will be used as inputs to models that will estimate deposition downwind such as the dispersion
models, AGDISP or WTDISP.
12
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
To meet the DQO, at least three replicate experiments using each nozzle were performed. As required by
the DQO in the approved test plans, the product of this test design will be the measurement of a droplet
size distribution consisting of 32 or more droplet size bins for the specified operating range.
2.1 Description and identification of DRTs
One reference and two candidate nozzles were tested using the pesticide spray DRT protocol in low-speed
and high-speed wind tunnels. The reference nozzle used for testing was an ASAE S572 nozzle associated
with the fine/medium boundary and was a 110° flat-fan nozzle operated at 300 kPa (43.5 psi) and 1.18
L/min (0.31 gpm). USDA-ARS provided the reference nozzle for the LSWT tests.
The two candidate nozzles tested were an All 1003-VS nozzle (Teejet Technologies, Wheaton, IL) and a
ULD 120-04 nozzle (Hypropumps, New York, NY). These are shown in Figure 1. The All 1003-VS is
an induction nozzle that produces a "very coarse" spray, as defined by ASABE S572 (1999), at the
operating conditions defined in element Bl of the approved T/QAP. This nozzle is used extensively by
industry and its performance characteristics have been extensively studied. The All 1003-VS flow is 1.13
L/min (0.3 gpm). The ULD 120-04 is a dual air induction nozzle also extensively used by industry. The
ULD 120-04 nozzle produces a "coarse" spray at the operating conditions defined in element Bl of the
T/QAP. The ULD 120-04 flow is 1.51 L/min (0.4 gpm). Both test nozzles were operated at 300 kPa
(43.5 psi) for all tests.
Teejet All 1003-VS Hypropumps ULD 120-04 nozzle
(manufacturer photo) (manufacturer photo)
Figure 1. Nozzles under test. Used with permission.
2.2 Spray material
The material used for droplet sizing measurements was a deionized water solution containing a 0.25%
volume/volume (v/v) of a 90% nonionic surfactant (R-l 1, Wilbur-Ellis Company, San Antonio, TX). For
the flux and deposition measurements, uranine was added to the above solution to make an uranine
concentration of 3.6 g/L. The solution was sprayed with a FIMCO 300 agricultural sprayer with boom
(FIMCO Industries, North Sioux City, SD). Pressure at the nozzle was measured using a digital pressure
gauge (Ashcroft Inc., Stratford, CT).
2.3 Procedures and methods used in testing
2.3.1 Test facilities
Low-speed testing was conducted in the aerosol wind tunnel (AWT) at the U.S. EPA ATF in Research
Triangle Park, NC (Figure 2). The AWT system can produce a wide range of air velocities, particle sizes,
and aerosol loadings with controlled temperature and humidity. In plan view, the AWT is rectangular in
shape with outside dimensions of approximately 20 m by 14 m. Flow through the recirculating AWT
during all operations is counterclockwise. The graphic of the tunnel shows two test sections: the human
exposure test section (HETS) and the sampler test section (STS). The HETS was used for this series of
13
-------
Environmental Technology' Verification Report
Pesticide Spray DRTProtocol Evaluation - VI.0
Figure 2. EPA's aerosol wind tunnel (AWT).
experiments. The HETS has a cross section 3.7 in wide, 3.0 in high, and 9.0 in long, and the STS has a
cross section 1.8m wide, 1.4 m high, and 6 in long. The wind speed in the HETS can be varied from 0.1
to 1 rn/s (0.36 to 3.6 km/h) while the STS can range from 0.56 to 13.3 m/s (2 to 48 krn/h). Air speed in
the wind tunnel was measured with a CSAT3 sonic anemometer (Campbell Scientific). The AWT is
described in more detail in the approved low-speed DRT T/QAP. Wind runnel temperature and relative
humidity were measured by a HMT 333 Probe (Vaisala. Woburii. MA). Spray solution temperature was
measured using a digital thermometer (Model 14-648-12. Fisher Scientific. Pittsburgh. PA). The
equipment setup for testing DRTs in the low-speed tunnel is pictured in Figure 3.
High-speed testing was conducted in the HSWT at USDA-ARS located in College Station. TX. and
depicted in Figure 4. The USDA-ARS HSWT consists of a high-speed centrifugal blower powered by a
48.5 kw (65 hp) gasoline engine. The blower speed is controlled by adjusting the engine's throttle. The
high-speed air generated by the blower exhausts through a 30 x 30 cm outlet. Prior to leaving the outlet.
the high-speed air passes through air straighteuers mounted inside the tunnel. Airspeed is measured
directly at the outlet using a pitot tube attached to an airspeed indicator. A 30 cm section of aircraft boom
is mounted directly at the tunnel's outlet. The boom is affixed to a pan of linear slides and a linear motor
to allow it to be traversed vertically across the length of the outlet. The boom section is plumbed to a
pressurized spray tank. The center of the boom has a fitting to mount the required check valves and
nozzles. A pressure gauge is also plumbed to the boom to monitor pressure at the nozzle. A movable 40
x 40 cm Plexiglas tunnel is positioned in-hue with the airstreain flush against the runners outlet. This
section is rnoveable to allow access to the spray boom and nozzle. The Plexiglas tunnel has a pair of
access holes downwind of the nozzle through which the laser diffraction instrument operates. Additional
details on the USDA-ARS HSWT can be found in the approved high-speed DRT T/QAP (Reference 2).
14
-------
Environmental Technology' Verification Report
Pesticide Spray DRTProtocol Evaluation - VI.0
Figure 3. AWT setup for low-speed DRT tests.
Nozzle
HELOS
Sympatec
Fan
\
HELOS
Sympatec
Figure 4. Overview of HSWT with enclosure removed for clarity.
2.3.2 Droplet sizing measurements
At each test location, droplet sizing measurements for this study were conducted using that facility's
Sympatec HELOS-Vario laser diffraction droplet sizing system (Syrnpatec Inc.. Clausthal. Germany),
which use a 623 um He-Ne laser. The HELOS systems were fitted with an R5 lens, which resulted in a
15
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
dynamic size range of 0.5 um to 875 um in 32 sizing bins. Droplet sizing data measured included volume
median diameter (Dv0 5) and the 10% and 90% diameters (Dv01 and Dv0 9). HELOS is an acronym for
helium-neon laser optical system.
For low-speed tests, two types of droplet sizing measurements were made for each nozzle: spray
characterization in static air and drift characterization 2 m downwind at 1 m/s wind speed. For the high-
speed tests, drift characterization at a downwind distance of 60 cm at 120 mph (55.3 m/s) wind speed
(aerial application air speeds) was performed. Spray characterization measurements were not performed
at USDA.
2.3.2.1 Spray characterization measurements - low-speed wind tunnel
Spray characterization measurements were performed in the low-speed wind tunnel in static air.4 The
wind tunnel was run for sufficient time to allow stabilization at the temperature and relative humidity
(RH) set points described in the approved T/QAP prior to testing. The three nozzles tested were the
reference, All 1003-VS and ULD 120-04 nozzle. Droplet size measurement and classifications were
consistent with ASABE S572 except that all tests were conducted under the same conditions (e.g., spray
material, spray pressure, nozzle settings) and following the procedures outlined in the approved test plans.
The nozzle that defined the fine/medium category [flat fan 110° at 300 kPa (43.5 psi)] served as the
reference nozzle for all subsequent tests (low- and high-speed).
2.3.2.2 Droplet sizing 2 m downwind - low-speed wind tunnel
For the low-speed droplet sizing measurements 2 m downwind of the nozzle, the wind tunnel was set at 1
m/s, 25 °C, and 80% RH and run for sufficient time to allow it to stabilize. The spray nozzle of interest
was mounted on a sprayer boom attached to the internal wind tunnel traverse and oriented at 90° so that
the spray pattern was perpendicular to the wind.
The HELOS system was set up inside the HETS on two hydraulic lift carts and oriented across the width
of the test section (along the x-axis, also perpendicular to the wind). The two halves of the HELOS were
separated as far as possible while still mounted to the rail. The distance from the transmitting to the
receiving part of the instrument was 94.6 cm (as shown in Figure 5). A 2.6-m long, 1.8-m wide false
floor was constructed 54.5 cm above the wind tunnel floor and was covered with artificial turf grass. The
spray nozzle was positioned 60 cm above and 60 cm downwind of the leading edge of the false floor.
Sprayer boom
(attached to traverse)
1 x Nozzle
60 cm ™ 2.0 m
False floor covered
by artificial turf grass
*
1.8m
T
94.6 cm
-Laser path
Helos
Figure 5. Schematic diagram of the set up for droplet sizing measurements 2 m downwind.
16
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
The HELOS was positioned as close as possible to the downwind edge of the false floor with the laser
beam 10 cm higher than the turf grass surface. The hydraulic lift carts were used to raise and lower the
HELOS unit to obtain the required measurement heights (10, 20, 30, 40, 50, 60 and 70 cm higher than the
turf grass), and a level was placed on the rail connecting the two parts of the HELOS system to ensure
that the system was always level. In order to minimize the number of times the HELOS was moved up
and down, measurements for all of the nozzles were made at one position before moving the HELOS
system up to the next position.
2.3.2.3 Droplet sizing 60 cm downwind - high-speed wind tunnel
For the high-speed droplet sizing measurements 60 cm downwind of the nozzle, the wind tunnel was set
at 192 km/hr (120 mph, 53.3 m/s), ambient conditions and run for sufficient time to allow it to stabilize.
The spray nozzle of interest was installed in the wind tunnel at or near the centerline and oriented at 0° so
that the spray pattern was parallel to the wind. Nozzles were positioned in the center of the wind tunnel
to be free from edge effects. High-speed test procedures are outlined in the approved T/QAP.
For these tests, USDA collected data from the reference nozzle, four different ULD 120-04 nozzles and
three different All 1003-VS nozzles. For a separate study, USDA compared the variation between
nozzles of the same type. Although comparing nozzles of the same type was not part of the T/QAP, for
completeness, all collected data are presented here, however a discussion of any variation is not
presented.
2.3.3 Spray flux and deposition measurements - Low-speed wind tunnel
Spray flux and deposition measurements are only applicable to the low-speed wind tunnel tests. For the
spray flux tests, monofilament lines approximately 2 mm in diameter were used as sample collectors.
These were extended horizontally across the wind tunnel at seven heights starting at 10 cm above the turf
grass that was on the wind tunnel floor and spaced in 10 cm increments. Each end of the monofilament
line was supported in enclosed boxes within the AWT to prevent contamination of the unused portion of
sampling line.
Spray flux was measured 2 m downwind from the spray nozzle using monofilament line at the same
seven heights as the droplet sizing measurements (see Figure 2). On one side of the test section, fishing
reels with the monofilament line were secured at each height inside a specially-constructed cabinet
designed to protect the unexposed monofilament line from uranine exposure. Another cabinet on the
other side of the tunnel held a series of dowels covered by plastic drinking straws at each height to hold
the monofilament in place. A small piece of tape was used to attach the loose end of the monofilament to
the dowel. After each spray replication, the monofilament at each height was collected by hand-winding
onto plastic straws (0.6 cm dia. x 19 cm long). Prior to spray exposure, the monofilament line was
marked with a permanent marker at the location where it exited the cabinet holding the fishing reels. The
line was then wound onto the straw until the mark was reached. The straw with the line was removed
from the dowel and placed in a labeled plastic Whirl-Pak bag. The process of collecting the exposed
monofilament also spooled new line from the reel into the tunnel, which was then secured onto new
plastic straws on the dowels.
Spray duration for an experiment was 15 ± 0.5 s. This was an unintended deviation from the T/QAP
specification of 10 ± 0.5 s that was only realized after all of the tests were completed. However, the
longer spray time did not cause overloading of the monofilament lines or puddling on the Mylar cards.
Immediately after an experiment, the exposed monofilament line was collected into a labeled plastic bag,
and 30 mL of 0.0IN NaOH was added to the bag to dissolve the uranine into solution. The bag contents
were shaken for 10s before an aliquot of the liquid was removed for fluorometric analysis.
Spray drop deposition at multiple horizontal distances from the nozzle were collected simultaneously with
the spray flux volume samples. Deposition sampling onto 10 cm by 10 cm (100 cm2) Mylar cards.
17
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
(VWR part # 95017-735, GE Healthcare Biosciences, Piscataway, NJ) was used to measure horizontal
deposition within the wind tunnel. Mylar cards were placed directly downwind from the nozzle aligned
with the plume centerline on metal support stands located 2, 3, 4, 5 and 6 m downwind of the nozzle. The
cards were at a height of 0.1 m above the turf grass on the wind tunnel floor to avoid boundary layer
effects.
Immediately after an experiment, the exposed Mylar cards were collected and placed in a labeled plastic
bag. 30 mL of 0.0IN NaOH were added to the bag to dissolve the uranine into solution. The bag
contents were shaken for 10s before an aliquot of the liquid was removed for fluorometric analysis.
The relative fluorescence in a 5 mL aliquot of the extract was measured using a Turner digital fluorometer
(Model FM109515, Thermo Scientific, Waltham, MA) following standard operating procedures. The
fluorometer used a 12 x 75 mm round cuvette. A narrow band (NB360) excitation filter and emission
filter (NB460) were used. A calibration curve linking fluorescence units to mass of fluorescent material
was generated for each batch of 50 samples. The curve spanned the detection range of the fluorometer
and demonstrated linearity in the instrumentation response as a function of mass deposited. From this
curve, fluorescent tracer measurements were converted to the fraction of spray liquid applied.
18
-------
Environmental Technology- Verification Report
Pesticide Spray DRTProtocol Evaluation - Vl.O
3.0 Results
3.1 Low-speed wind tunnel test results
3.1.1 Spray characterization results
The management of pesticide drift exposure may involve careful consideration of many factors such as
the droplet size spectrum, spray release height, meteorological conditions, application practices, no-spray
buffer zones, tank mix physical properties, liquid temperature, and target characteristics. Managing these
factors can be complex, so focus is often placed on the major parameters of importance. For example.
droplet size is often the most important factor, so optimization of the size range to include relatively few
small droplets (by volume) can provide a major reduction in spray drift potential while maintaining
product efficacy for many application scenarios.
Table 1 presents the results from the nozzle spray characterization measurements without wind. The
results shown are the average of three replicate measurements. The DVO 5 of the reference nozzle spray
was 220.7 urn. Results are shown graphically in Figure 6.
Table 1. Spray characterization droplet size data (means ± standard deviations) 60 cm below the nozzle.
Nozzle
Reference
AI11003-
vs
Hypro ULD
120-4
Pressure
(psi)
43.5
43.5
43.5
Flow
(Lpm)
1.20
1.21
1.65
Replicate
1
2
3
1
2
3
1
2
3
DVO.-I
(Mm)
127.6
130.6
78.8
154.6
155.0
136.8
22.2
17.2
20.7
DVO.S
(Mm)
217.2
220.8
224.2
280.3
280.4
243.3
162.0
190.2
203.2
DvO.9
(Mm)
310.2
318.9
360.5
388.9
388.5
322.5
231.0
297.2
304.5
Statistic
Average
3D
CV
Average
SD
CV
Average
SD
CV
DVO.I
(Mm)
112.4
29.1
0.26
148.8
10.4
0.07
20.0
2.6
0.13
DVO.S
(Mm)
220.7
3.5
0.02
268.0
21.4
0.08
185.1
21.0
0.11
DvO.9
(Mm)
329.9
26.9
0.08
366.6
38.2
0.10
277.5
40.5
0.15
SD = standard deviation. CV = coefficient of variation
500-
400 -
?
e
.« 300 -
£
•
1200-
o
L.
C
100 -
0 -
1
LSWT Spray Characterization Results (static conditions)
^^^M
^^ ^^-^^
^^^~- ^^
^^^^
) 0.1 0.2 0.3 0.4 0.5 06 0.7 0.8 0.9
-»-REF 11003
-•- All 1003- VS
ULD 1 70-04
I
Cumulative Volume Fraction
Figure 6. LSWT spray characterization results under static wind conditions.
19
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
3.1.2 Droplet sizing 2 m downwind results
The measured droplet sizes for all three nozzles at the seven heights are shown in Table 2. For example,
spray characterization at a height of 20 cm is shown in Figure 7. The decrease in the size distribution at
heights lower than 30 cm (Hypro) or 40 cm (Teejet) identified the point where all DQIGs were achieved.
The very large droplet sizes measured at the higher positions resulted from extremely low optical
concentrations. No data were reported for the Hypro ULD 120-4 nozzle at 30 and 50 cm heights because
the optical concentration was so low that the HELOS could not detect and thus not report any data. All
size distribution data at 2 m were impacted by failure to achieve HELOS data collection data quality
indicator goals (DQIGs). The HELOS was operating normally and without operator error. The low wind
speed (1 m/s) and extremely large droplets generated by all nozzles caused HELOS minimum obscuration
to be less than 2% for 83% of measurements and percentage of drop volume in largest and smallest bins
to be > 1% in approximately 65% of measurements (See Table 10).
Wind speed, temperature, and relative humidity averages and standard deviations measured for each
nozzle over the three replicate droplet sizing measurements at 2 m downwind are given in Table 3.
Table 2. Droplet size data (means ± standard deviations) 2 m downwind of nozzle at 1 m/s wind speed.
Nozzle
Reference
AI11003-VS
Height
(cm)
70
60
50
40
30
20
10
70
60
Replicate
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
DVO.I
(Mm)
550.2
592.3
559.4
490.9
541.2
520.9
20.2
19.1
19.4
14.8
19.7
22.2
19.9
20.4
18.2
23.7
23.9
28.2
27.3
28.4
27.8
540.9
541.3
541.8
455.6
452.8
466.2
Dvo.s
(Mm)
660.0
666.1
661.2
647.8
657.5
653.1
39.9
38.0
37.3
43.1
45.8
46.1
48.1
47.3
44.6
56.9
54.5
54.4
52.0
52.9
52.7
652.9
652.9
652.8
618.8
609.1
626.4
Dvo.s
(Mm)
720.0
721.2
720.2
717.6
719.5
718.6
60.6
61.6
62.4
74.4
77.9
80.1
85.3
85.1
81.9
133.5
119.2
122.1
86.0
86.8
87.4
718.6
718.6
718.6
711.8
710.. 1
713.3
Statistic
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
DVO.I
(Mm)
567.3
22.2
0.04
517.7
25.3
0.05
19.6
0.6
0.03
18.9
3.7
0.20
19.5
1.2
0.06
25.3
2.5
0.1
27.8
0.5
0.02
541.0
0.9
0.00
458.2
7.1
0.02
Dvo.s
(Mm)
662.3
3.4
0.01
652.8
4.9
0.01
38.4
1.4
0.04
45.0
1.7
0.04
46.6
1.8
0.04
55.3
1.4
0.03
52.5
0.4
0.01
652.5
0.8
0.00
618.4
8.7
0.01
Dvo.s
(Mm)
720.5
0.7
0.00
718.6
1.0
0.00
61.5
0.9
0.02
77.5
2.9
0.04
84.1
1.9
0.02
125.0
7.6
0.06
86.7
0.7
0.01
718.5
0.2
0.00
711.7
1.6
0.00
20
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Nozzle
T
0
CM
T-
Q
_l
D
O
Q.
>,
I
Height
(cm)
50
40
30
20
10
70
60
50
40
30
20
10
Replicate
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
DVO.I
(Mm)
1.0
1.0
1.0
479.4
464.1
454.2
12.4
11.9
10.9
45.0
45.5
44.3
47.3
46.2
46.8
535.5
534.4
533.9
474.0
481.0
480.0
-
-
-
551.6
563.4
558.2
-
-
-
40.9
41.3
41.8
43.6
43.1
42.7
Dvo.s
(Mm)
2.9
2.9
2.9
644.0
646.3
634.1
55.2
54.7
54.9
75.6
76.1
75.8
83.9
83.0
83.1
648.4
647.3
646.6
636.6
634.1
629.7
-
-
-
657.6
661.0
656.9
-
-
-
67.0
67.8
69.2
73.9
73.4
73.6
Dvo.s
(Mm)
61.1
58.8
57.4
716.8
717.3
714.8
87.2
86.7
87.1
111.9
111.2
113.4
119.5
119.8
118.6
717.7
717.5
717.3
715.3
714.8
713.9
-
-
-
719.5
720.2
719.4
-
-
-
98.3
99.8
102.7
101.2
102.2
104.3
Statistic
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
DVO.I
(Mm)
1.0
0.0
0.01
465.9
12.7
0.03
11.8
0.8
0.06
44.9
0.6
0.01
46.8
0.6
0.01
534.6
0.8
0.00
478.3
3.8
0.01
-
-
-
557.7
5.9
0.01
-
-
-
41.3
0.4
0.01
43.1
0.5
0.01
Dvo.s
(Mm)
2.9
0.0
0.01
641.5
6.5
0.01
55.0
0.3
0.01
75.8
0.2
0.00
83.3
0.5
0.01
647.4
0.9
0.00
633.5
3.5
0.01
-
-
-
658.5
2.2
0.00
-
-
-
68.0
1.1
0.02
73.6
0.3
0.00
Dvo.s
(Mm)
59.1
1.9
0.03
716.3
1.3
0.00
87.0
0.3
0.00
112.2
1.1
0.01
119.3
0.6
0.01
717.5
0.2
0.00
714.7
0.7
0.00
-
-
-
719.7
0.4
0.00
-
-
-
100.3
2.3
0.02
102.6
1.5
0.02
SD = standard deviation, CV = coefficient of variation
Table 3. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution temperature for
droplet sizing measurements (means ± standard deviations) at 2 m downwind.
Nozzle
Reference
AI11003-VS
Hypro ULD 120-4
Pressure
(psi)
43.3 ±0.12
43.4 ±0.26
43.4 ±0.15
Wind speed
(m/s)
1.03 ±0.06
1.02 ±0.05
1.03 ±0.05
Air
Temperature
(°C)
24.9 ±0.05
24.9 ±0.05
25.0 ±0.05
Relative
Humidity
(%)
80.0 ± 0.62
79.9 ±0.73
79.8 ± 0.76
Solution
Temperature
(°C)
23.7 ± 0.82
23.7 ±0.80
23.7 ±0.83
21
-------
Environmental Technology' Verification Report
Pesticide Spray DRTProtocol Evaluation - VI.0
140
0.1 0.5
Cumulative Volume Fraction
0.9
•Reference
•AI1103-VS
ULD 120-4
Figure 7. Example of LSWT spray characterization at the 2-meter flux plane and 20 cm height.
3.1.3 Spray flux and deposition res ults
Results of flux measurements from inonofilarnent line are given in Table 4 as the average ± standard
deviation of three replicate measurements expressed as ten-thousandths of total applied spray volume
[(mass uranine recovered / total mass uranine sprayed) * 104]. Spray flux versus height at the 2-meter
flux plane is shown graphically for the three spray nozzles in Figure 8. Spray flux decreased with
increasing height, as expected. Spray flux was greatest for the reference nozzle and least for the Hypro
ULD 120^-4 nozzle.
Results of deposition measurements from Mylar cards calculated in the same manner are given in Table 5.
Spray deposition was decreased with distance from the source, as expected. At each distance, the largest
amount of deposition resulted from the reference nozzle, with the smallest amount from the Hypro ULD
120-4 nozzle.
Table 4. Results from flux measurements as ten-thousandths of applied (fraction - 104) at 2 m downwind.
Height
(cm)
70
60
50
40
Replicate
1
2
3
1
2
3
1
2
3
1
2
3
Reference
Flux
0.46
0.49
0.26
invalid
0.60
0.59
0.83
1.05
0.84
3.86
2.68
2.61
Average
SD
CV
0.40
0.12
0.31
0.59
0.01
0.02
0.91
0.12
0.14
3.05
0.70
0.23
AI11003-VS
Flux
0.19
0.18
0.42
0.19
0.15
0.23
0.22
0.17
0.23
0.29
0.24
0.18
Average
SD
CV
0.26
0.13
0.51
0.19
0.04
0.22
0.20
0.03
0.16
0.24
0.05
0.22
Hypro ULD 120-4
Flux
0.14
0.07
0.06
0.23
0.07
0.07
0.20
0.08
0.07
0.32
0.15
0.07
Average
SD
CV
0.09
0.05
0.54
0.13
0.09
0.74
0.11
0.07
0.64
0.18
0.13
0.53
-------
Environmental Technology' Verification Report
Pesticide Spray DRTProtocol Evaluation - VI.0
Height
(cm)
30
20
10
Replicate
1
2
3
1
2
3
1
2
3
Reference
Flux
14.64
22.40
19.98
30.12
32.16
29.67
61.08
103.02
110.32
Average
SD
CV
19.01
3.97
0.21
30.65
1.33
0.04
91.47
26.57
0.29
AI11003-VS
Flux
1.53
1.55
1.57
20.26
23.81
19.91
64.06
82.70
80.22
Average
SD
CV
1.55
0.02
0.01
21.33
2.16
0.10
75.66
10.12
0.13
Hypro ULD 120-4
Flux
0.41
0.16
0.20
4.86
4.66
6.16
18.68
19.39
19.87
Average
SD
CV
0.25
0.13
0.53
5.23
0.82
0.16
19.31
0.60
0.03
100
Flux as Fraction of Applied at 2 meters
20
30 40
Height (cm)
50
60
70
•Reference
•Hypro ULD 120-4
All1003-VS
Figure 8. LSWT spray flux 2 meters from the nozzle (flux vs. height for three nozzles).
Wind speed, temperature, and relative humidity averages and standard deviations measured for each
nozzle over the three replications measuring flux and deposition are given in Table 6. All of these
parameters were controlled to well within the requirements stated in the T/QAP.
Table 5. Results from deposition measurements as ten-thousandths of applied.
Distance
(m)
2
Replicate
1
2
3
Reference
Flux
32.22
25.30
22.97
Average
SD
CV
26.83
4.81
0.18
AI11003-VS
Flux
20.28
22.97
14.20
Average
SD
CV
19.15
4.49
0.23
Hypro ULD 120-4
Flux
0.74
1.65
1.93
Average
SD
CV
1.44
0.62
0.43
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Distance
(m)
3
4
5
6
Replicate
1
2
3
1
2
3
1
2
3
1
2
3
Reference
Flux
37.69
15.05
14.76
12.43
7.66
6.57
7.25
2.43
3.55
4.45
1.68
1.87
Average
SD
CV
22.50
13.16
0.58
8.89
3.11
0.35
4.41
2.52
0.57
2.67
1.55
0.58
AI11003-VS
Flux
5.71
9.05
2.99
2.72
4.48
1.9
1.54
1.45
1.88
0.78
0.76
1.74
Average
SD
CV
5.92
3.03
0.51
3.03
1.32
0.43
1.62
0.23
0.14
1.09
0.59
0.51
Hypro ULD 120-4
Flux
0.22
0.20
0.22
0.19
0.14
0.65
0.12
0.17
0.10
0.11
0.16
0.12
Average
SD
CV
0.21
0.01
0.06
0.33
0.28
0.87
0.13
0.04
0.30
0.13
0.03
0.21
SD = standard deviation, CV = coefficient of variation
Table 6. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution temperature for
flux and deposition measurements.
Nozzle
Reference
AI11003-VS
Hypro ULD 120-4
Pressure (psi)
(Avg ± SD)
43.4 ±0.06
43.5 ±0.10
43.6 ±0.26
Wind speed
(m/s)
(Avg ± SD)
1.00 ±0.01
1.00 ±0.05
1.00 ±0.01
Air Temp (°C)
(Avg ± SD)
25.0 ±0.06
25.0 ±0.06
24.5 ±0.31
%RH
(Avg ± SD)
80.4 ±0.21
80.0 ±0.17
80.0 ±0.53
Solution Temp
(°C)
(Avg ± SD)
21. 6 ±0.47
21.9±0.10
22.0 ±0.00
3.2 High-speed wind tunnel test results
The measured droplet sizes for all three nozzles used in the high-speed tests are shown in Table 7. For a
separate study, USDA compared the variation between nozzles of the same type. Although comparing
nozzles of the same type was not part of the T/QAP, for completeness, all collected data are presented
here.
Wind speed, temperature, and relative humidity averages and standard deviations measured for each
nozzle over during the high-speed wind tunnel tests are given in Table 8. All of these parameters were
controlled within the requirements stated in the T/QAP. Liquid flow rate data were not collected.
Table 7. Droplet size data 60 cm downwind of nozzle at specified wind speed.
Nozzle
Ref
11003a
REF
11003
Pressure
(psi)
43
43
Speed
(m/s)
0
53.3
Angle
0
0
0
Rep
1
2
3
1
2
3
DVO.I
(nm)
79.5
80.1
79.4
96.91
96.21
96.91
DvO.5
(um)
177.8
182.1
179.0
210.86
209.86
211.45
DvO.9
(urn)
362.4
374.8
380.1
333.52
332.57
340.55
Statistic
Average
SD
CV
Average
SD
CV
DVO.I
(um)
79.7
0.4
0.00
96.68
0.40
0.00
DvO.5
(urn)
179.6
2.2
0.01
210.72
0.80
0.00
DvO.9
(Um)
372.4
9.1
0.02
335.55
4.36
0.01
24
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
ULD 120-
04X
ULD 120-
04Y
ULD 120-
04Y2
ULD 120-
04Z
AI11003-X
AI11003-Y
AI11003-Z
40
40
40
40
40
40
40
53.3
53.3
53.3
53.3
53.3
53.3
53.3
0
0
0
0
0
0
0
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
1
2
3
130.03
130.11
129.15
139.25
140.95
139.69
130.21
132.37
134.82
133.08
137.37
130.15
128.38
125.49
127.52
122.92
123.67
124.22
120.69
121.84
120.67
275.78
275.77
275.51
296.87
298.54
297.4
278.41
283.93
284.84
283.53
293.7
276.86
278.97
272.81
273.94
263.74
268.28
267.49
263.9
264.1
264.14
427.4
426.61
421.9
484.13
483.75
483.76
423.44
429.4
425.98
430.64
479.78
421.25
440.39
417.84
417.25
396.66
411.33
410.16
408.04
407.46
408.86
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
Average
SD
CV
129.76
0.53
0.00
139.96
0.88
0.01
132.47
2.31
0.02
133.53
3.63
0.03
127.13
1.48
0.01
123.60
0.65
0.01
121.07
0.67
0.01
275.69
0.15
0.00
297.60
0.85
0.00
282.39
3.48
0.01
284.70
8.48
0.03
275.24
3.28
0.01
266.50
2.43
0.01
264.05
0.13
0.00
425.30
2.97
0.01
483.88
0.22
0.00
426.27
2.99
0.01
443.89
31.43
0.07
425.16
13.19
0.03
406.05
8.15
0.02
408.12
0.70
0.00
aThese data were not collected during the HSWT tests. Data collected in February 2009 are reported. See Section 4.2.
SD = standard deviation, CV = coefficient of variation
Table 8. Nozzle pressure, wind speed, air temperature, relative humidity, and spray solution temperature for
droplet sizing measurements (means ± standard deviations) at 60 cm downwind.
Nozzle
Reference
AI11003-VS
Hypro ULD 120-4
Pressure
(psi)
43 ±0.0
40 ±0.0
40 ±0.0
Wind speed
(mis)
53.3 ±0.0
53.3 ±0.0
53.3 ±0.0
Air
Temperature
(°C)
21 .7 ±0.0
24.6 ± 0.0
24.6 ± 0.0
Relative
Humidity
(%)
66.3% ± 0.0
55.5% ± 0.0
55.5% ± 0.0
Solution
Temperature
(°C)
20. 3 ±0.0
23.9 ±0.0
23. 9 ±0.0
25
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
4.0 Verification of Performance
4.1 Quality assurance
The primary performance measures for the evaluation of the pesticide spray DRT protocol is derived from
the droplet size distribution measurements and flux at the 2-meter plane. The basic experimental design
was to measure the droplet size spectrum or flux under targeted test conditions with the DRTs operating
at specified spray pressures, air speeds, and the ambient environmental conditions. Wind tunnel and
spray liquid conditions measurements are supplemental measures that established the bounds of the spray
size distribution data. EPA, RTI, vendors, test facilities, and other stakeholders will use this report to
evaluate the pesticide spray DRT protocol and suggest changes that will provide improvements.
Data on calibration certificates for the flow meters, flow transducers, weights, low- and high-resolution
balances, thermometer, and humidity logger are maintained at Alion and USDA in a separate data
package.
To meet the DQO, at least three replicate experiments using each nozzle were performed. As required by
the DQOs in the approved test plans, the product of this test design was the measurement of a droplet size
distribution consisting of 32 or more droplet size bins for the specified operating range. Adherence to the
DQOs, as expressed through the achieving the Data Quality Indicator Goals (DQIGs), for the high- and
low-speed tests are presented in Tables 9 and 10, respectively.
As part of the GVP evaluation, an Audit of Data Quality (ADQ) was performed. Alion Science &
Technology audited their data from low-speed wind tunnel testing.5 RTI QA staff reviewed and approved
the low-speed wind tunnel testing ADQ. RTI QA personnel audited the high-speed wind tunnel data
collected at USDA.6 The EPA quality manager performed a Technical Systems Audit (TSA) of the low-
speed wind tunnel testing.7
Both Alion and RTI QA staff have reviewed the results of these tests and have found that the results did
not meet the overall data quality objective (DQO) as stated in each T/QAP. Failure to achieve the DQIGs
listed in Table 9 (high-speed wind tunnel) and Table 10 (low-speed wind tunnel) were the cause.
The failure to meet all high-speed and low-speed wind tunnel DQIGs did not have a significant impact on
the evaluation of the protocol. In fact, the difficulty meeting those DQIGs indicated the acceptance
criteria might be too stringent for those metrics. RTI suggests EPA ask the stakeholder panel if the
acceptance criteria for the DQIGs in question should be relaxed to keep the verification test cost
reasonable. If so, the stakeholders should propose new acceptance criteria for the DQIGs that were
achieved. Another possibility for the low-speed wind tunnel DQIGs is to obtain stakeholder input on
revising the GVP to include procedures for balancing wind tunnel air speed and expected spray size
distribution from a particular nozzle to insure sufficient spray material is transported to all heights at the
2-meter flux plane to achieve the existing DQIGs.
Table 9. Data quality indicator goals for high-speed wind tunnel tests
Parameter
Nozzle spray angle
Spray liquid pressure (nozzle
operating pressure)
Acceptance Criteria
Variation within ± 5% during
test
± 3.4 kPa of values specified in
the ASABE standard for
reference and evaluation
nozzles.
Met
DQIG?
Y N
/
/
Comments
26
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Parameter
Spray liquid temperature
Spray liquid flow rate
Dynamic surface tension of spray
liquid
Viscosity of spray liquid
Acceptance Criteria
Measured within 0.1 °C
± 0.04 L/min of values
specified in the ASABE
standard for reference and
evaluation nozzles.
52 ± 4 dynes/cm at surface
lifetime age of 10 to 20 ms for
test fluids with adjuvants. 70 ±
4 dynes/cm for water, if used
as test fluid
1.1 ±0.1 cPat20TC
Met
DQIG?
Y N
/
/
/
/
Comments
Data not submitted by
USDA
DROPLET SIZE DISTRIBUTION DQIGs
Spray volume in largest and smallest
droplet size class bands in laser
diffraction measurements
Number of size class bands for
reported data
Standard deviation around mean Dvo.s
for three replicate droplet size
measurements
Measured Dvo.s (volume median
diameter) , Dvo.i and Dvo.9 (i.e., the
droplet diameter bounding the upper
and lower 10% fractions of the spray)
Obscuration for spray measurements
across a spray diameter (for laser
diffraction systems)
Minimum obscuration for sampling to
achieve cross-section average spray
(e.g., start and end trigger using
traverse with laser diffraction
systems)
Sample size per replicate
measurement
Diode suppression (laser diffraction
systems)
< 1% of total volume in each
case (i.e., < 2% total of the
spray volume) - to be
achieved through selection of
appropriate lens and
instrument configuration for the
dynamic size range of the
spray being sampled
>32
Vary by less than ± 3% for
replicate measurements with
the same nozzle
Vary by less than ± 7% for
replicate measurements with
the same nozzle
< 60% unless corrected for
multiple scattering, whereupon
the report shall include the
measured obscuration, the
algorithm used to correct for
multiple scattering, and the
manufacturer-stated limits of
applicability for that algorithm.
2%
> 10,000 droplets for particle
counting instruments or
> 5 s for laser diffraction
instruments
Diodes may not be suppressed
(no channels may be killed)
/
/
/
/
/
/
/
/
Spray volumes in smallest
droplet size class band met
criterion. 80% of the spray
volumes in largest droplet
size class band were
greater than 1%.
Standard deviation of Dvo9
for HyproULD 120-04
replicate is 7.1%
27
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Parameter
Acceptance Criteria
Met
DQIG?
Y N
Comments
HSWT OPERATION DQIGs
Air speed inside wind tunnel
Wind tunnel cross section diameter
Wind tunnel ambient air temperature
Wind tunnel wet bulb/dew point
temperature or percent relative
humidity
Relative spray material and air
temperatures
Between 50 mph (22 m/s) and
180 mph (80 m/s), and
measured to an accuracy
within 5 mph (2 m/s), close to
nozzle location (with nozzle
absent). Acceptance criteria
between measurements ± 5%.
Cross-section at least three
diameters larger than spray
plume diameter (at size
distribution measurement
location).
Measured within 0.1 °C
Measured within ± 0.1 °C or ±
1%
Spray material temperature
must be within 2 ^C of the air
temperature to avoid
atomization anomalies.
/
/
/
/
/
Difference between spray
and air temperature was
2.5 °C for certain runs
Table 10. Data quality indicator goals for low-speed wind tunnel tests
Parameter
Acceptance Criteria
Met
DQIG?
Y N
Comments
DROPLET SIZE DISTRIBUTION MEASUREMENT DQIGs
Spray volume in largest and
smallest droplet size class bands
in laser diffraction measurements
Number of size class bands for
reported data
Standard deviation around mean
DVO .5 for three replicate droplet
size measurements
Measured Dvo.s (volume median
diameter), Dvo .1 and Dvo9 (i.e., the
droplet diameter bounding the
upper and lower 10% fractions of
the spray)
< 1% of total volume in each
case (i.e., < 2% total of the
spray volume) to be
achieved through selection
of appropriate lens and
instrument configuration for
the dynamic size range of
the spray being sampled
> 32
Vary by less than ± 3% for
replicate measurements
with the same nozzle
Vary by less than ± 7% for
replicate measurements
with the same nozzle
S
V
S
S
39% of values were
greater than 1%.
66% of all measured
values were above 3%
100% of all measured
values were above 7%.
28
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Parameter
Obscuration for spray
measurements across a spray
diameter (for laser diffraction
systems)
Minimum obscuration for
sampling to achieve cross-
section average spray (e.g., start
and end trigger using traverse
with laser diffraction systems)
Sample size per replicate
measurement
Diode suppression (laser
diffraction systems)
Spray nozzle height
measurement
Nozzle spray angle
Spray liquid pressure (nozzle
operating pressure)
Spray liquid temperature
Spray liquid flow rate
Dynamic surface tension of spray
liquid
Viscosity of spray liquid
Wind tunnel ambient air
temperature
Wind tunnel wet bulb/dew point
temperature or percent relative
humidity
Percent relative humidity (low-
speed wind tunnel)
Acceptance Criteria
< 60% unless corrected for
multiple scattering,
whereupon the report shall
include the measured
obscuration, the algorithm
used to correct for multiple
scattering, and the
manufacturer-stated limits of
applicability for that
algorithm.
2%
> 10, 000 droplets for
particle counting
instruments or
> 5 s for laser diffraction
instruments
Diodes may not be
suppressed (no channels
may be killed)
Within 5 mm (without
airflow)
Variation within ± 5% during
test
± 0.5 psi of values specified
in the ASABE standard for
reference and evaluation
nozzles.
Measured within 0.1 "C
± 0.04 L/min of values
specified in the ASABE
standard for reference and
evaluation nozzles.
52 ± 4 dynes/cm at surface
lifetime age of 10 to 20 ms
for test fluids with adjuvants.
70 ± 4 dynes/cm for water, if
used as test fluid
1.1 ±0.1 cPat20
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Parameter
Relative spray material and air
temperatures
Air speed inside wind tunnel
Sampling rate for air speed
Acceptance Criteria
Spray material temperature
must be within 2 "C of the
air temperature to avoid
atomization anomalies.
1 m/s measured accuracy
within 0.1 m/s, close to
nozzle location (with nozzle
absent).
Sampling should occur over
a measuring period of 30 s
Met
DQIG?
Y N
^
^
^
Comments
DRIFT POTENTIAL MEASUREMENT DQIGs
Spray duration for replicate
measurements
Spray duration for similar nozzle
types
Solvent volume for extraction of
tracer, if using collectors
Air speed inside wind tunnel
Sampling rate for air speed
Wind speed consistency in wind
tunnel working section
Wind tunnel working section
width
Wind tunnel turbulence
Wind tunnel ambient air
temperature
Wind tunnel wet bulb/dew point
temperature or percent relative
humidity
Percent relative humidity (low-
speed wind tunnel)
Minimum spray time of 5 s
for each replicate
measurement. Replicate
measurements for a nozzle
type should be within ± 5%
of mean time duration for a
given setup.
Similar nozzle types from
different vendors/
manufacturers should be
tested for similar time
duration, within ± 5%.
Within 5% of volume
required for analytical
recovery and assessments
1 m/s measured accuracy
within 0.1 m/s, close to
nozzle location (with nozzle
absent).
Sampling should occur over
a measuring period of 10 s
<5%
Minimum to avoid boundary
layer and blockage effects
<8%
Measured within 0.1 °C
Measured within ± 0.1 "C or
±1%, respectively
80% ± 5%
V
V
V
V
V
^
^
V
^
^
V
Local wind velocity
variability was not
measured according to
ISO 22856
Wind velocity variability
was not measured
according to ISO 22856
30
-------
Environmental Technology Verification Report
Pesticide Spray DRT Protocol Evaluation -Vl.O
Parameter
Relative spray material and air
temperatures
Acceptance Criteria
Spray material temperature
must be within 2 "C of the
air temperature to avoid
atomization anomalies.
Met
DQIG?
Y N
v'
Comments
4.1.1 Deviations
Except as noted below, the verification tests were conducted in accordance with the approved T/QAPs.2'3
The TSA found that the low-speed wind tunnel was properly equipped and data were collected as
specified in the T/QAP. RTI determined the high-speed wind tunnel had the proper equipment to collect
data as specified in the T/QAP. Deviations from the test plans and impact on data quality are described
below.
Low-Speed Wind Tunnel Test Deviations
• Low-speed spray test duration of 15 ± 0.5 s instead of 10 ± 0.5 s.
o The increased spray time did not overload the monofilament line or cause puddling on the
Mylar cards. Therefore, the change did not affect data quality.
• Duplicate spray deposition samples at were not collected as a quality control check.
o Horizontal spray deposition measurements are not an input to the AGDISP or WTDISP
models that will be used to evaluate spray drift approximately 100 m downwind of spraying
and cannot be used to confirm the quality of flux and droplet size distribution measurements
at the 2-meter flux plane. Taking these measurements during evaluation testing highlighted
their cost (an increase of 30% for each test). Given that they do not contribute to the long-
range drift calculation and are expensive, they will not be included in the revised protocol for
future testing using a LSWT, making further evaluation during this test irrelevant.
• The first test of low-speed flux measurements at 60 cm with the reference nozzle was invalid
because the monofilament line was accidentally shaken during collection.
o The shaking of the line dislodged collected spray droplets. In a real verification, the test may
need repeated. However, EPA will not use the flux data to verify AGDISP or WTDISP
model results. Therefore, the lost datum was not critical to the objectives of GVP evaluation.
Note that the invalid sample does highlight the purpose of the GVP evaluation: to identify
experimental procedures specified in the GVP that may increase the cost of verification.
High-speed Wind Tunnel Test Deviations
• USDA did not collect spray characterization with the reference nozzle.
o USDA high-speed wind tunnel availability was limited during GVP evaluation. Time
constraints prohibited collection of the data. Instead, historical data collected 1 month earlier
were used to characterize the spray size distribution from the reference nozzle. USDA
routinely collects spray characterization data with the reference nozzles. A history of size
distributions is available. The historical data are suitable for GVP validation.
• USDA did not collect spray liquid flow rate data.
o The fluid pressure in the system controlled the fluid flow at the test nozzle. Therefore, a
consistent volumetric flow of fluid was achieved throughout the test. The missing flow data
do not affect overall data quality.
31
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
• Pictures of the nozzles were not obtained by either laboratory, and USDA did not take pictures of
their HSWT test setup.
o This oversight did not affect data quality and the results of the GVP evaluation.
32
-------
Environmental Technology Verification Report Pesticide Spray DRT Protocol Evaluation -Vl.O
5.0 References
1. RTI International. Draft Generic Verification Protocol for the Verification of Pesticide Spray
Drift Reduction Technologies for Row and Field Crops, RTI International, Research Triangle
Park, NC, February 2007. Available at http://www.epa.gov/nrmrl/std/etv/pubs/600etv07021 .pdf.
2. RTI International. Test/QA Plan for the Evaluation of the Verification Protocol for High Speed
Pesticide Spray Drift Reduction Technologies for Row and Field Crops. RTI International,
Research Triangle Park, NC, March 2008.
http://www.epa.gov/nrmrl/std/etv/pubs/600etvll008.pdf
3. RTI International. Test/QA Plan for the Evaluation of the Verification Protocol for Low Speed
Pesticide Spray Drift Reduction Technologies for Row and Field Crops. RTI International,
Research Triangle Park, NC, May 2009.
http://www.epa.gov/nrmrl/std/etv/pubs/600etvll007.pdf
4. ASABE S572. Spray Nozzle Classification by Droplet Spectra. American Society of Agricultural
and Biological Engineers. St. Joseph, MI, August 1999.
5. Alion Science & Technology. Quality Assurance Data Review Report: Evaluation of the
Verification Protocol for Low Speed Pesticide Spray Drift Reduction Technologies for Row and
Field Crops. Alion Science & Technology, Research Triangle Park, NC, July 2009.
6. RTI International. Quality Assurance Data Review Report: Evaluation of the Verification
Protocol for High Speed Pesticide Spray Drift Reduction Technologies for Row and Field Crops.
RTI International, Research Triangle Park, NC, September 2009.
7. U.S. EPA. Findings from the Assessment of Quality and Technical Systems for EPA ESTE
Project, "Evaluation of the Verification Protocol for Low Speed Pesticide Spray Drift Reduction
Technologies for Row and Field Crops" U.S. EPA, Research Triangle Park, NC, July 2009.
33
-------
Appendix A
LSWT Test Data
-------
Transcribed by: Brixey
Alion Science and
Technology
Drift measurements
Nozzle Reference
Pressure 43.35
Height 10cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
27.31
28.39
27.77
27.82
0.54
1 .9%
psi
DVO.S
52.03
52.86
52.67
52.52
0.43
0.8%
Dvo.g
85.99
86.80
87.35
86.71
0.68
0.8%
Nozzle AI11003VS
Pressure 43.72
Height 10cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
47.32
46.21
46.75
46.76
0.56
1 .2%
Hypro
Nozzle 4
Pressure 43.26
Height 10cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
43.60
43.10
42.71
43.14
0.45
1 .0%
psi
DVO.S
83.93
82.97
83.08
83.33
0.53
0.6%
ULD 120-
psi
DVO.S
73.90
73.39
73.61
73.63
0.26
0.3%
Dvo.g
119.52
119.77
118.59
119.29
0.62
0.5%
Dvo.g
101.24
102.23
104.26
102.58
1.54
1 .5%
Reviewed
By: PY
Nozzle Reference
Pressure 43.4
Height 20 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
23.65
23.93
28.17
25.25
2.53
10.0%
DVO.S
56.85
54.48
54.44
55.26
1.38
2.5%
Dvo.g
133.58
119.26
122.10
124.98
7.58
6.1%
Nozzle AI11003VS
Pressure 43.54
Height 20 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
45.00
45.51
44.31
44.94
0.60
1 .3%
Nozzle Hypro ULD
Pressure 43.4
Height 20 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
40.93
41.31
41.76
41.23
41.31
0.34
0.8%
DVO.S
75.63
76.08
75.82
75.84
0.23
0.3%
120-4
DVO.S
67.02
67.80
69.19
67.69
67.93
0.91
1 .3%
Dvo.g
111.95
1 1 1 .27
113.40
112.21
1.09
1 .0%
Dvo.g
98.29
99.84
102.72
99.66
100.13
1.86
1 .9%
-------
Transcribed by: Brixey
Alion Science and Technology
Drift measurements
Nozzle Reference
Pressure 43.35
Height 30 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
19.94 48.07
20.44 47.25
18.22 44.61
19.53 46.64
1.16 1.81
6.0% 3.9%
Nozzle AI11003VS
Pressure 43.48
Height 30 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
12.42 55.24
11.92 54.70
10.94 54.92
11.76 54.95
0.75 0.27
6.4% 0.5%
Hypro ULD 120-
Nozzle 4
Pressure 43.28
Height 30 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
No
data
Signal too low
Dvo.g
85.26
85.13
81.88
84.09
1.92
2.3%
Dvo.g
87.21
86.68
87.09
86.99
0.28
0.3%
Dvo.g
Reviewed
By: PY
Nozzle Reference
Pressure 43.35
Height 40 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
14.82
19.67
22.17
18.89
3.74
19.8%
DVO.S
43.05
45.79
46.12
44.99
1.69
3.7%
Dvo.g
74.37
77.89
80.13
77.46
2.90
3.7%
Nozzle AI11003VS
Pressure 43.35
Height 40 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
501.18
479.40
464.08
454.17
474.71
20.47
4.3%
DVO.S
644.53
643.96
646.32
634.11
642.23
5.51
0.9%
Dvo.g
716.91
716.79
717.26
714.82
716.45
1.10
0.2%
Nozzle Hypro ULD 120-4
Pressure 43.38
Height 40 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
551.57
563.40
558.21
533.35
551.63
13.11
2.4%
DVO.S
657.57
661.02
656.93
649.15
656.17
5.01
0.8%
Dvo.g
719.51
720.20
719.39
717.83
719.23
1.00
0.1%
-------
Transcribed by: Brixey
Alion Science and Technology
Drift measurements
Nozzle Reference
Pressure 43.35
Height 50 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
20.19 39.92
19.07 38.00
19.39 37.27
19.55 38.40
0.58 1.37
3.0% 3.6%
Nozzle AI11003VS
Pressure 43.72
Height 50 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
0.99 2.95
0.98 2.92
0.98 2.91
0.98 2.93
0.01 0.02
0.6% 0.7%
Hypro ULD 120-
Nozzle 4
Pressure 43.28
Height 50 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I DVO.S
No
data
Signal too low
Dvo.g
60.60
61.62
62.38
61.53
0.89
1 .5%
Dvo.g
61.09
58.76
57.38
59.08
1.88
3.2%
Dvo.g
Reviewed
By: PY
Nozzle Reference
Pressure 43.07
Height 60 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
490.89
541.21
520.91
517.67
25.32
4.9%
DVO.S
647.78
657.54
653.13
652.82
4.89
0.7%
Dvo.g
717.56
719.51
718.63
718.57
0.98
0.1%
Nozzle AI11003VS
Pressure 43.08
Height 60 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
469.19
455.56
452.77
466.22
460.94
7.99
1 .7%
DVO.S
624.85
618.84
609.14
626.43
619.82
7.83
1 .3%
Dvo.g
712.97
711.77
710.12
713.29
712.04
1.44
0.2%
Nozzle Hypro ULD 120-4
Pressure 43.32
Height 60 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
474.03
480.99
479.97
478.33
3.76
0.8%
DVO.S
636.61
634.08
629.69
633.46
3.50
0.6%
Dvo.g
715.32
714.82
713.94
714.69
0.70
0.1%
-------
Transcribed by: Brixey
Alion Science and Technology
Drift measurements
Reviewed
By:
PY
Nozzle Reference
Pressure 43.46
Height 70 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
550.15
548.98
559.37
592.29
562.70
5.69
1 .0%
DVO.S
659.95
659.57
661.21
666.08
661.70
0.86
0.1%
Dvo.g
719.99
719.91
720.24
721 .22
720.34
0.17
0.0%
Nozzle AI11003VS
Pressure 43.1
Height 70 cm
Rep#
1
2
3
4
Average
sd
sd (%)
DVO.I
540.88
541.31
541.82
539.78
540.95
0.87
0.2%
Hypro
Nozzle 120-4
Pressure 43.7
Height 70 cm
Rep#
1
2
3
Average
sd
sd (%)
DVO.I
535.52
534.44
533.93
534.63
0.81
0.2%
DVO.S
652.90
652.91
652.82
651.34
652.49
0.77
0.1%
ULD
DVO.S
648.38
647.26
646.57
647.40
0.91
0.1%
Dvo.g
718.58
718.58
718.56
718.27
718.50
0.15
0.0%
Dvo.g
717.68
717.45
717.31
717.48
0.19
0.0%
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,12:4.:..,240
x10 = 12
x16 = 14'
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
n
7.60 um xso = 217.18 um x90 = 310.17 inn
'.40 urn xj4 = 289.66 urn xg9 = 371.66 um
— t
->—
1 |
,
n
c
-)
n
0
D
SMD = 186.05 um VMD = 217.71 urn
Sv =0.03 in2 cm3 V = 345.70 cnrg
1
i
•
i
•
3
D
4 6 8 10
Reference nozzle (110 deg flat fan)
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
20
40 60 80 100
particle size ^irn
200
400
600 800
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
U.OO
0.02
0.02
0.02
0.02
0.02
0.02
0.02
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.02
0.06
0.13
21
61
03
70
2.72
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qj/%
4.34
6.76
9.71
14.51
21.96
33.01
48.21
66.13
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
84.80
98.26
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 12:35:29
contamination: 0.00 %
trigger condition: 65 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
6.77 %
dispersing i
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 ranis', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.37
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,12:4.:..,i93
x10 = 130.60 um xso = 220.79 urn x90 = 318.94 um
x16 = 149.96 urn xg4 = 296.35 um X99 = 407.93 um
SMD = 162.61 um VMD = 222.64 urn
Sv = 0.04nrcm3 V =388.61 cm-g
100
90
70
c
60
£3
S
'£ 50
M
•o
j; 40
•a
J3
3 }0
10
4 6 8 10
Reference nozzle (1 10 deg flat fan)
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
20
40 60 80 100
particle size urn
200
400
600 800
h
0
0
0
0
0
0
0
0
/%
.15
.21
.21
.23
.25
.28
.31
.31
Xn Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference nieasiu-enient: 05-26 12:35:29
contamination: 0.00 %
trigger condition: 65 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.00
Q3/%
0.35
0.40
0.48
0.62
0.93
1.40
2.01
3.02
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
4.62
7.00
9.89
14.52
21.61
31.98
46.39
63.62
X,, HIM
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
82.56
96.07
99.53
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
6.90 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.37
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,12:4.:..,6i5
io =78
16 = 13-
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
84 urn x50 = 224.22 urn x90 = 360.49 um
..54 urn xg4 = 324.43 um 3199 = 496.90 urn
p
D I?I9 1
?l n D
n
1
D
1
a
a
I
SMD = 77.88 um VMD = 226.74 urn
Sv = 0.08 nr cm3 V = 797.76 cnr/g
1
c
D
a
i i
J
3
P
H
|
J_ J_
4 6 8 10 20
Reference nozzle (110 deg flat fan)
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 12:35:29
contamination: 0.00 %
trigger condition: 65 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 65s real time
user parameters:
Nozzle: Reference
Air Speed: 0.00
40 60 80 100
particle size urn
200
400
600 800
Q3/%
1.20
1.45
1.68
1.89
2.19
2.55
2.88
3.24
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
7.92
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
9.64
12.01
14.77
19.24
26.15
36.06
48.91
62.90
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
76.83
87.76
94.91
98.90
99.81
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
8.46 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.37
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
Xjo = 112.35 um Xso = 220.73 urn Xpo = 329.86 um
x16 = 143.30 uni xg4 = 303.48 um X99 = 425.50 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,12:4.:..,
SMD = 142.18 um VMD = 222.36 urn
Sv = 0.05m2 cm3 V =510.69 cm-g
Cumulative distribution Q3 / %
H
•— ' l-j u^ -U 'vi ON ^1 oo vp <
ooooooooooc
1
1
f
n
1
LiY 1
hi n n
n O
a $
g
a
r
LJ
,
1
c
m
m
D
i
•
a
a
i
j_ j_
4 6 8 10
Reference nozzle (110 deg flat fan)
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
20
40 60 80 100
particle size um
200
400
600 800
4.50
5.50
6.50
7.50
9.00
11.00
13.00
0.45
0.56
0.63
0.71
0.82
0.95
1.07
15.50
1.19
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/
i.
i.
i.
i.
2.
2
3.
4.
%
33
47
64
88
31
84
49
55
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
6.20
8.59
11.46
16.09
23.24
33.68
47.84
64.21
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
31.39
94.03
98.15
99.63
99.94
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 12:35:29
contamination: 0.00 %
trigger condition: 65 second scan •
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
7.38 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.37
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:25:13615
x10 = 13
Xi6 =161
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
6.77 um xso = 243.32 um x90 = 322.48 um
.59 uni xg4 =301.82um 3199 = 360.75 uni
I
6 8 10
20
1 _
40
_
IB T*
60 80
SMD = 205.26 um VMD = 235.67 urn
Sv =0.03ni2cm3 V = 292.3 Icnrg
^ ^ ^ ^ M ^
/«
^W
.
1
./
r
l_ • j
J
"
i
/
7
I
/
/
•
•
•
i
^ ^
,
100 200 400 600 SOO
particle size
AI11003VS
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
U.OO
0.02
0.02
0.02
0.02
0.02
0.02
0.02
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.02
0.02
0.02
0.02
0.09
0.21
0.40
0.77
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
1.52
2.84
4.57
7.58
12.72
21.20
35.01
56.18
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
85.89
100.00
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 13:22:59
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
2.80 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:27:37,ioo
.a
•o
.3
= 15
= 18:
100
90
80
70
60
50
40
30
20
10
0
t\
5.04 um XSQ = 280.41 um Xpo = 388.45 inn
.04 ^ni xj4 = 362.68 um xyg = 430.34 uni
•4
\
3-
-S
l-l
<
-s-
laJ_ll
8
hill • i
10
•— »J
2
LB-I
D
l-*-J
-C-
4
i-l
D
|J
to
L
6
•L
D
80
SMD = 235.57 fim VMD = 274.87 fim
Sv =0.03nrcm3 V =254. 70 cm- g
M ^ ^ ^ ^
E
./P
ll 1 1
7
.
7
i
/
/
J
j
i
I
i
i
.
P
,^
•
i
* ^
. .
100 200 400 600 800
particle size
AI11003VS
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
U.OO
0.02
0.02
0.02
0.02
0.02
0.02
0.02
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.02
0.02
0.02
0.02
0.02
0.11
0.24
0.51
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
.04
.96
3.16
5.28
8.96
15.14
25.06
39.58
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
60.08
84.96
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-26 13:22:59
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
2.36 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 innis', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:30:06,225
x10 = 154.59 um xso = 280.30 urn x90 = 388.91 um
x16 = 182.67 uni xg4 = 363.02 \im X99 = 430.39 um
SMD = 234.72 um VMD = 274.78 urn
Sv = 0.03m-cm3 V =255.63 cm-g
90
80
0?
f»» 70
e
o 60
'O
3
X>
'£ 50
M
U 40
•a
J3
3 30
ij 2ft
10
0
^
J
z
I
/
^
™
1
/
/
rf
/
/
/
1
/
B
»
pi
•
* ^
4 6 8 10
AI11003VS
no wind speed
nieasm-enient 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
40 60 80 100
particle size uni
200
400
600 800
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
U.OO
0.02
0.02
0.02
0.02
0.02
0.02
0.02
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.02
0.02
0.02
0.02
0.02
0.11
0.25
0.53
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
.07
.00
3.22
5.36
9.05
15.24
25.15
39.65
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
60.10
84.81
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-26 13:22:59
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
2.36 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:..:..,
x10 =14
XKJ = 17f
100
90
* 8°
g 70
| 60
'£ 50
M
•o
£ 40
•a
J3
P 30
0 20
10
n
8.80 um xs
i.77 urn X&
—c
—
\ i
i = 268.01 um Xpo = 366.61 um
t = 342.51 (wn X99 = 407.16 (im
,
n
D
SMD = 225.18 um VMD = 261.77 um
Sv =0.03nrcm3 V =267.55 cnrg
1
1
B
•
u 1
•
B
u
4 6 8 10
AI11003VS
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
20
40 60 80 100
particle size ^irn
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
U.OO
0.02
0.02
0.02
0.02
0.02
0.02
0.02
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.02
0.02
0.02
0.02
0.05
0.14
0.29
0.60
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
1.21
2.26
3.65
6.07
10.25
17.20
28.41
45.14
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
68.69
89.93
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 13:22:59
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ms
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 a cm
shape factor: 1.00
2.51 %
dispersing
rotor inclination:
stroke:
acceleration:
force:
0.00°
0.00 mni
0.00 mm, s', velocity: 0.00 mm, s
0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:53:26100
X16 —
.a
•o
.3
= 20
= 50.
100
90
80
70
60
50
40
30
20
10
0
4
67 uin xso = 203.18 um x90 = 304.50 inn
33 Jim xg4 = 288.07 (im XQ9 = 358.89 uin
»
H
rt
«
i
i
i
.-**^
• i
r1
i-
•
^4
fr-
•
•
•
I
t 6 S 10 20 40 60 80
SMD = 44.33 um VMD = 186.33 uin
Sv =0.14ni-/cm3 V = 1353.46 cm- £
• ^ • • ^ ^
J
*r
w^^
/
•
/
1
± 1
/
/
J
f
\
I
1
1
1
/
•
"
1
* ^
. ,
100 200 400 600 800
particle size
HyproULD 120-4
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
2.09
2.62
3.15
3.68
4.49
5.56
6.61
7.84
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
9.17
10.31
11.42
12.69
14.18
15.36
16.26
17.23
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
18.59
20.72
23.20
26. 96
32.48
41.12
54.53
71.92
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
90.18
100.00
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-26 13:48:05
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
4.86 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.30
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,13:56:06678
.a
•o
.3
= 17
= 32.
100
90
80
70
60
50
40
30
20
10
0
4
22 urn xso = 190.16 um x90 = 297.17 inn
20 jim xg4 = 278.77 (im X99 = 356.94 uin
*
I
r
<
i
i
K*^
_^»-
•
*^
, i
i '
i-^
•
-—I
1
•
ml
i
t 6 8 10 20 40 60 80
SMD = 42.17 um VMD = 173.71 um
Sv = 0.14nrcm3 V = 1422.84 cm- g
M M M M M ^
J
mT
,wr
'
,
m
/
i
± i
/
7
J
z
17
^
/]
/
i
•
I
^ F
. ,
100 200 400 600 800
particle size
HyproULD 120-4
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
1.76
2.35
2.98
3.64
4.65
6.02
7.37
8.98
v, iim
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
10.75
12.27
13.76
15.44
17.36
18.81
19.89
21.07
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
22.61
24.82
27.40
31.36
37.19
46.09
59.56
76.25
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
92.55
100.00
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 13:48:05
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
5.41 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.30
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,14:01:18162
.a
•o
= 22
= 65.
100
90
80
70
60
50
40
30
20
10
0
t\
23 urn xso = 162.04 urn x90 = 230.96 um
92 jim xg4 = 214.35 um x^ = 274.06 um
^
1
1
h
'
i
^
.^^
•-*-
-•-i
I—I
1—
I
-i
^
m
—
•
I
i
\ 6 8 10 20 40 60 80
SMD = 38.29 um
Sv =0.16nrcni3
•
I
I
m
I
1
1
!'
/I
/
.s
Y
i i
i
J
T
/
• 1
VMD = 148.41 ^im
Sm = 1566.91 cm- ^
• •__•__•_•_•__•
•
I
^ F
. ,
100 200 400 600 800
particle size uni
HyproULD 120-4
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
3.00
3.63
4.22
4.80
5.61
6.59
7.44
8.34
v, iim
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
9.20
9.87
10.49
11.23
12.18
13.08
14.01
15.41
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
17.56
20.67
24.21
30.58
42.46
61.24
84.43
98.38
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-26 13:58:46
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
4.37 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nmi/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.30
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-26,1.
*
g
M
•o
•a
J3
= 20
= 49.
100
90
80
70
60
50
40
30
20
10
0
A
04 urn xso = 185.13 urn x90 = 277.55 um
48 urn xg4 = 260.40 um 3199 = 329.96 urn
P
r
L
3
t 6 8
( H •
Q
• i
'
i
r
D
n
1
10 20 40 60 80
SMD = 41.60 um VMD = 169.48 urn
Sv =0.14ni-cm3 V = 1447.74 cm-^
1
i
1
B
3
1
. ,
100 200 400 600 800
particle size uni
HyproULD 120-4
no wind speed
measurement 60 cm below nozzle
spray pattern perpendicular to laser path
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
2.28
2.87
3.45
4.04
4.91
6.06
7.14
8.39
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
9.71
10.82
11.89
13.12
14.57
15.75
16.72
17.90
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
19.59
22.07
24. 94
29.64
37.38
49.48
66.17
82.18
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
94.24
100.00
100.00
100.00
100.00
100.00
100.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-26 13:.8:..
contamination: 0.00 %
trigger condition: 65 second single scan'
time base: 100.00 ins
start: button
valid: always
stop: 65s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
4.88 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nmi/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.30
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:37:47,271
XKI — 27
xw = 32.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
n
77 uin xso = 52.67 uin x90 = 87.35 uin
19^ini xg4 = 78.73^1111 xgg = 126.64 um
_i
iJ
Lj
L
mJ
imLu
hi. • • • i
•-•
f
f
/
l
i
/
P
V
m
/
/
'
/
/
'
SMD =45.15 urn
Sv =0.13nrcni3
• "*
1
i
VMD = 55.69 um
V = 1328.85 cnrVg
|
* "•
j_ j_
8 10
20
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.06
0.06
0.12
0.24
0.43
0.70
1.20
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Reference
Air Speed: 0.96
Qy
2.20
3.84
6.73
12.64
24.16
36.78
49.72
66.01
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
81.40
91.85
96.58
98.93
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.01 %
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:38:18oo6
XK, =28
xw =32.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
39 uin XSQ = 52.86 uin Xpo = 86.80 uin
53 jim xg4 = 78.22^1111 xgg = 124.37 um
d
•
I
A
I
jt _U
L _ _
6 8 10
•— *•
1
*-
1
^
/
1
1
/
F
i
/
/
i
•
/
i/
/
f
t
20 40 60 80
SMD =46.99 urn
Sv =0.13nrcni3
• • • ™
1 fl-"* *
1
I |
VMD = 55.90 urn
V = 1276.77 cni3/£
• •__«__^L_^i__«_^L__^
"
1
* ^
. ,
100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.05
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 17:28:38
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
0.44
1.90
5.35
12.21
23.44
36.02
49.41
66.07
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
81.75
92.24
96.88
99.07
100.00
100.00
100.00
100.00
X,, HIM
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.13 %
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:38:42,850
x10 =27
XKJ =31.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
£ 40
•a
J3
P 30
0 20
10
n
31 urn xso = 52.03 uin x90 = 85.99 um
79 jim xg4 = 77.37 um 3199 = 122.48 urn
_i
iJ
-i
t-
LmJ
imLu
hi -«-»-•-•'
ut
I
/
1
1
^
r
\
/
1
i
I
/
1
/
SMD =43.98 urn
Sv =0.14nrcni3
1
I
'
i
VMD = 54.80 um
V =1364.27 cm3/!
|
' *•
j_ j_
8 10
20
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
Xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.13
0.25
0.45
0.75
1.10
1.69
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
2.75
4.38
7.24
13.20
24.94
37.78
50.82
67.05
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Q3/%
82.35
92.79
97.33
99.24
99.82
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.14%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:3.:..,
xio = 27
xw =32.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
n
82 uin XSQ = 52.52 pin Xpo = 86.71 uin
17 jim xg4 = 78.11^1111 X99 = 124.50 uni
—c
—
\ 1
n
n °
c
D
[
I
[
a
I
SMD =45.37 urn
Sv =0.13nrcni3
D U r
VMD = 55.46 M
V = 1323.30
in
:nr g
6 8 10
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.02
0.06
0.13
0.23
0.39
0.60
0.98
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.l
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
1.80
3.37
6.44
12.69
24.18
36.86
49.98
66.38
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
81.83
92.29
96. 93
99.08
99.94
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.09%
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27, ll:36:24,ioo
"> O
Xjo ~~ *«»
xw =32.
100
90
* 8°
g 70
| 60
'£ 50
.-9
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
17 uin Xs
66 ^im X&
•4
\
i-l
L-d
1-
<
L*J
'
l^Lii
8
j = 54.44 uin x90 = 122.10 um
[ = 101.18um X99 = 178.12 (im
liLf-m^-
10
t*
r1
/
I
i
/
P
•
/;
/
/
,
•
/
q
•
20 40 60
i
>
so
SMD = 47.22 um
Sv =0.13nrcni3
1
— s
_^
^f
r"
1
VMD = 64.64 um
V = 1270.56 cnrVg
I
* "•
. .
100 200 400 600 800
particle size
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.15
0.37
0.69
1.04
1.59
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Reference
Air Speed: 1.11
2.52
3.94
6.48
12.03
23.24
35.38
47.30
61.20
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
72.80
80.32
85.26
90.80
96.26
99.18
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
2.83 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:37:48,78?
x10 =23
x16 =30.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
93 uin xso = 54.48 uin x90 = 119.26 urn
23 urn xg4 =98.80um 3199 = 176.85 uin
H
1
K
I |
•,• •
H-^-
I
•W
\
r"
A
{
^
'
/
/
i
•
/
/
i
, '
1
I
i
SMD = 26.54 um
Sv = 0.23 nr cm3
i jjj ~
mf
| '
i
VMD = 62.59 urn
S,,! = 2260.64 cm- /'£
|
* "•
j_ j_
8 10
20
40 60 80 100
particle size urn
200
400 600 800
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
4.25
4.61
4.84
5.01
5.17
5.35
5.55
5.93
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
Q3/%
6.78
8.24
10.77
15.71
25.12
36.07
47.31
60.88
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
72.85
80.97
86.14
91.56
96.62
99.28
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
3.15%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:39:13 709
x10 =23
x16 =30.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
A
65 urn xso = 56.85 urn x90 = 133.58 um SMD = 27.33 um
78 jim xg4 = 111.05 um xg9 = 199.94 urn Sv = 0.22 nr cm3
•
•
•
•.-
i 1 i 1 i 1 i 1 i
II m_
m-*-
^j
-•
ii i i
^
>
^P
f
*
I
f
A
/
i
2
Tf
*
^^•^
\
VMD = 67.44 um
V = 2195.24 cnrVf
I
' »•
^ 6 8 10 20 40 60 80 100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
3.95
4.41
4.77
5.05
5.37
5.72
6.05
6.54
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
Q3/%
7.39
8.68
10.83
15.10
23.72
33.97
44.50
57.15
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
68.57
76.86
82.27
87.99
93.84
98.13
99.66
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
3.72 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing i
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:3.:..,
x10 = 25
Xi6 =31.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
25 uin XSQ = 55.26 uin Xpo = 124.98 inn
22 Jim xg4 = 103.68 um 3199 = 184.97 uni
V
r
L
L
3
t 6 8
i n
D
D
|
10 20 40 60 80
SMD = 33.70 um
Sv = 0.19 in- cm3
£
LJ
J_ |
VMD = 64.89 |i
V = 1908.81
1
in
:nr £
. .
100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.
11.
.00
.00
13.00
15.50
2.73
3.01
3.20
3.40
3.64
3.92
4.21
4.69
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: WINDOX 5.4.2.0, HELD stabill
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
Q3/%
5.57
6.95
9.36
14.28
24.03
35.14
46.37
59.75
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
71.41
79.38
84.55
90.12
95.57
98.86
99.89
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
3.23 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing i
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:11:36,053
1 D
XjO ~~ lo
xw =24.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
22 urn xso = 44.61 uin x90 = 81.88 uin
74 um xg4 =71.02^1111 xyg = 144.99 um
HI
1
^
1
i
^
i
1-1
1 i
•[[*-•-
m-*
i
»
1
t
f
/
i
•
i
/
f
/
i
1
,
1
A
l
\
y*
i!
/
i
SMD =22.50 urn
Sv = 0.27 nr cni3
• ""^ ~*"
• ^
i i
VMD =48.11 um
V = 2666.84 cnr £
|
' *•
j_ j_
8 10
20
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
4.54
5.13
5.60
5.98
6.46
7.03
7.63
8.55
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiirenient: 05-27 13:08:15
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.07
Q3/%
10.15
12.50
16.28
23.42
36.62
50.74
63.88
77.25
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
87.15
93.36
96.44
98.20
99.20
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.79 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 rum s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:12:35,240
Xjo = 20.44 uin x$o = 47.25 uin Xpo = 85.13 um
xis =27.16 jim xj4 = 74.24 (im x$9 = 126.71 uni
SMD = 27.89 urn VMD = 50.44 um
Sv = 0.22nrcm3 V =2150.99 cnrVg
*
M
•o
•a
J3
uu
OQ
on
70
fiO
SO
10
30
->o
10
4
.
1
1
1
C
1
1
H
_ I
8
• -**-
M
10
»^"
2
•^
3
x1
1
j
/
•
4
1
/
'
0
1.
/
/
6
.
^
D
r
|
8(
) 1
30
2(
10
4C
0
6(_
0
r|l
I
*T*
800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
2.33
2.86
3.37
3.86
4.57
5.45
6.31
7.39
v, iim
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidatioii:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.07
Q3/%
8.83
10.63
13.47
19.32
31.83
46.02
59.31
73.29
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
84.69
92.55
96.59
98.93
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.92 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:12:59,412
x10 = 19
xi6 =26.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
94 urn xso = 48.07 uin x90 = 85.26 uin SMD = 26.70 um
94 jim xg4 = 74.61^1111 xgg = 128.11 urn Sv = 0.22 nr cni3
1
1
1
•l
«
'
I |
H^
•-*•
•-1
.x1
1
/
m
•
/
/
/
/
'
H
/
;
p
,c
,r
/
i
i
VMD = 50.81 um
V = 2246.87 cm2/!
1
* "•
. .
t 6 S 10 20 40 60 80 100 200 400 600 SOO
particle size
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
2.85
3.40
3.90
4.37
5.02
5.82
6.61
7.66
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.07
9.11
10.96
13.82
19.45
31.11
44.64
57.75
72.23
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
84.38
92.59
96.59
98.86
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.00%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:1.:..,
x10 = 19
xi6 =26.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
53 uin XSQ = 46.64 uin Xpo = 84.09 uin
28 ^ini xg4 =73.29(iiii xg9 = 133.27 uin
L
J
L
t 6 8
, • •
D D
•
c
]
U
t
_
l
10 20 40 60 80
SMD =25.70 urn
Sv = 0.24 in- cm3
D ° r
^ 1
VMD = 49.78 M
V = 2354.90
1
in
:m-/g
. .
100 200 400 600 800
particle size
cumulative distribution
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
3.
3.
4.
4.
5.
6.
6.
7.
24
79
29
74
35
10
85
87
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/
9.
11.
14.
20.
33.
47.
60.
74.
>/o
36
37
53
73
19
13
31
26
evaluation: WINDOX 5.4.2.0, HELD stabill
invalidation:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.07
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qj/%
85.41
92.83
96.54
98.66
99.73
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.90 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:04:52,271
xio =22
xw = 27.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
4
17 uin xso = 46.12 uin x90 = 80.13 uin
25 urn xg4 =71.04(im 3199 = 120.92 uni
LMJ
\
LJ
LJ
<
Lw
LI
IT!
^
m*
Jm
}
\
/
(
+
\
/
•
H
/
/
A
i
I!
/
i
8 10 20 40 60 80
SMD =32.91 urn
Sv =0.18nrcni3
^ i
VMD = 49.05 um
V =1823.31cni2/i
I
' *•
. .
100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.92
1.21
1.53
1.86
2.39
3.16
4.01
5.22
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:02:42
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
7.00
9.32
12.90
19.80
33.30
47.95
61.66
76.18
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
87.63
94.56
97.67
99.34
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.40 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:05:44,334
x10 = 19
xi6 =26.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
4
67 uin xso = 45.79 pin x90 = 77.89 uin
37 jim xj4 = 69.64^1111 xyg = 120.58 urn
_l
[
fcJ
J
L.
<
LMJ
LI
ll1
8
^^^
•T
m^
•
j^
1
y
/
/
T
\
i
/
B
*
Ml
Lr
H
A\
\
•
T "
^
i
10 20 40 60 80
SMD = 33.05 pm
Sv =0.18nrcni3
H* *
^ |
VMD = 48.20 jim
V =1815.39cnrVg
I
* ^
. .
100 200 400 600 800
particle size
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.42
0.74
1.16
1.67
2.57
3.91
5.31
7.07
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 15:02:42
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
9.15
11.33
14.35
20.36
33.58
48.50
62.63
77.59
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
88.80
95.01
97.76
99.35
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.41 %
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:06:11,881
Xjo = 14.82 uin x$o = 43.05 uin Xpo = 74.37 um
xis = 22.65 jim xj4 = 66.20 um x$9 = 136.40 uin
SMD = 24.52 urn VMD = 45.69 um
Sv =0.24nrcm3 V =2447.01 cnvVg
*
M
•o
•a
J3
uu
OQ
on
70
fiO
SO
10
30
->o
10
o
4
1
.
•l
-'
•
f
1
1
|^|
I |
8
I-*'*'"
10
m-*
2
•^
^
•
S
i
/
{
4
/
0
/
1 1
|
/
f
60
MM
•^
;:!
i
so
MJ^-M—I
i
100
2(
10
4C
0
6(_
0
r|l
I
*T*
. .
800
particle size
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
2.56
3.29
4.05
4.81
5.94
7.40
8.78
10.46
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:02:42
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Q3/%
12.52
14.87
18.33
25.16
38.96
53.87
67.56
81.28
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
90.46
94.77
96.79
98.50
99.60
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.36 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:0.:..,
1 .
XjO ~~ lo
xw =25.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
A
88 uin xso = 44.99 uin x90 = 77.47 uin
42 urn xg4 = 68.96 urn 3199 = 125.97 urn
a
9
S
V i
t 6 8
_ •
|
•
c
•
c
1
J
u
10 20 40 60 80
SMD =30.16 urn
Sv = 0.20 nr cm3
D U r
1
VMD = 47.65 M
V =2028.57
1
in
:nr £
. .
100 200 400 600 800
particle size
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
1.30
1.75
2.25
2.78
3.63
4.82
6.03
7.58
ii Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
9.56
11.84
15.19
21.77
35.28
50.11
63.95
78.35
evaluation: WINDOX 5.4.2.0, HELD stabill
invalidation:
reference measurement: 05-27 15:02:42
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 0.96
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
88.96
94.78
97.41
99.06
99.87
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.39 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:25:06459
x10 = 19
xw =23.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
39 uin xso = 37.27 uin x90 = 62.38 uin SMD = 23.60 um
76 jim xg4 = 56.51 um x^ = 101.50 um Sv = 0.25 nr cm3
1
1
1
*1
1
1 i
IT*^*
m-*
}
M
1
/
1
(
1
4
•
"
1
/
t
J
I
1
/
•
•
•m
^^
i
VMD = 43.31 um
V = 2542.77 cm3/!
|
i i-
j_ j_
S 10
20
40 60 80 100 200
particle size ^ini
400 600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
2.99
3.51
3.99
4.43
5.04
5.79
6.53
7.54
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidatioii:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
9.15
12.02
18.17
30.76
50.62
67.50
79.90
90.12
\i, Illll
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
96.00
98.45
99.17
99.17
99.17
99.17
99.17
99.17
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.15%
dispersing method: Defaii
Q3/%
99.17
99.17
99.17
99.17
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:25:34,365
z1( = 19
xw =23.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
4
07 urn xso = 38.00 uin x90 = 61.62 uin SMD = 23.41 um
97 Jim xg4 = 56.30 \im x^ = 84.27 urn Sv = 0.26 nr cm3
3
•
1
h
1
I |
^-^
•-^
?
/
/
^
1
J
f
I/
•
/
/
1
/
rnjrPT
1
VMD = 39.22 um
V = 2563.3 IcnrVg
1
* *•
. .
t 6 S 10 20 40 60 80 100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
3.09
3.63
4.12
4.57
5.20
5.97
6.75
7.80
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Reference
Air Speed: 1.11
Q3/%
9.48
12.19
17.59
29.20
48.84
66.33
79.71
91.00
Xi, mil
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
97.38
100.00
100.00
100.00
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.13 %
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:29:18865
xjo =20
xw =25.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
4
19 ii m
55 ^ini
-1
H
HI
1
1
t 6
xso = 39.92 um x90 = 60.60 uin
Xg4 = 56.00 um xgs = 73.34 um
1 1 _J
i •— •"*
Q_
•-^
•
•^
1
^
/
j
\
I
r
i
/
i
i
i
1
•
i \
n
A\
SMD =26.17 pm
Sv = 0.23 in- cm3
VMD = 39.94 um
V = 2293.07 cm2/!
1
* *•
8 10 20 40 60 80 100 200 400 600 800
particle size um
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3/'
2 _
2.
3.
3.
4.
5.
6.
7.
>/o
00
50
00
49
22
16
OS
23
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/'
8.
10.
14.
24.
43.
63.
79.
92.
>/o
77
95
99
14
54
55
44
43
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.14%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mui/s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:2.:..,
xio = 19
xw =24.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
55 urn XSQ = 38.39 uin Xpo = 61.53 urn
43 jim xg4 = 56.27 um xgg = 86.37 um
f
L
I
3
i • 5
D
c
•
[
!
D
r
a
Voft
|
SMD =24.39 urn
Sv = 0.25 nr cm3
I
i i
VMD = 40.82 ii
V = 2466.38
|
in
j_ j_
8 10
20
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
\.l Illll
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/'
2 ,
3.
3.
4.
4.
5.
6.
7.
'/o
69
22
70
17
82
64
45
52
\i, Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs
9
11
16
28
47
65
79
91
/%
.13
.72
.92
.03
.67
.79
.68
.20
evaiuarion: WINDOX 5.4.2.0, HELD stabill
revalidation:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
Air Speed: 1.11
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
97.80
99.48
99.72
99.72
99.72
99.72
99.72
99.72
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.14%
dispersing method: Defaii
Qj/%
305.00
365.00
435.00
515.00
615.00
735.00
875.00
99.72
99.72
99.72
99.72
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umis
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:02:28975
xjo =52
xie = 55'
100
90
^ 70
c
60
£3
S
'S 50
M
•o
sj 40
•a
J3
3 30
10
0
t\
0.91 um xso = 653.13 urn x90 = 718.63 um SMD = 60.63 um VMD = 613.03 urn
k68 urn xg4 = 708.80 um x^ = 733.36 um Sv = 0.10nrcm3 V =989.63 cm- g
™ ™
-
I
ill , 1 , . . m Mti^
i
' T
r
I
_
7
•
/
l]
\ 6 8 10 20 40 60 80 100 200 400 600
—
800
particle size
cumulative distribution
x,, inn
4.50
5.
6.
7.
9.
11.
13.
15.
50
50
50
00
00
00
50
Q3/°/o
3.35
3
4
4
4
4
4
4
.78
.13
.13
.13
.13
.13
.13
Xi, Mill
18.50
21.
25.
30.
37.
45.
52 .
6q
2 .
50
00
00
50
00
50
50
Q3/
4.
4.
4.
4.
4.
4.
4.
4.
'/o
13
13
13
13
13
13
13
25
V"
75
90
105
125
150
180
215
255
m
.00
.00
.00
.00
.00
.00
.00
.00
Qj/%
4.93
5
S
5
5
5
5
5
.38
.38
.38
.38
.38
.38
.38
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.00
x., inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
5.38
5.38
5.38
8.95
26.72
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.07
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:02:578%
= 541.21 uin xso = 657.54 urn x90 = 719.51 uin
= 576.53 um xg4 = 710.21 um x^ = 733.45 um
SMD = 637.23 um VMD = 644.42 urn
Sv = 0.01m-cm3 V = 94.16 cm-g
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
20
10
0
*
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xi, Illll
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, Illll
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
Qj/%
0.00
0.00
1.06
5.55
22.54
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.07
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:03:23584
xio =49
xie = 531
100
90
* 8°
g 70
| 60
S
'S 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
0.89 um xso = 647.78 um x90 = 717.56 um
..77 uni xg4 = 707.09 um 3199 = 733.26 uni
•
I
*
i
.*, i.
6 8 10
20
T
40
6
9 80
SMD = 613.50 um VMD = 626.29 um
Sv = 0.01nrcm3 V = 97. 80 cm- g
™ ™
100 200
^
/
I
' 7*
1
fl
fl
P
/
/
,
\\
i l
400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
Qj/%
0.00
0.26
3.71
12.71
31.21
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.07
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:0.:..,
x10 = 517.67 um xso = 652.82 urn x90 = 718.56 inn
xis = 554.66 uni xj4 = 708.70 urn xg9 = 733.36 uni
SMD = 437.12 um
Sv = 0.04 nr cm3
VMD = 627.91 um
V = 393.86 cm- g
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
(
1
D 1 a 1 a i
5i a a
a a
o c
0
n
i;
a
n
(9
n a g n
n
p
n
a
a
Typ]
j_ j_
10
20
40 60 80 100
particle size uni
200
400
600 SOO
cumulative distribution
Q3/%
50
50
6.50
7.50
1.12
1.26
1.38
9.
11.
.00
.00
13.00
15.50
38
38
38
38
1.38
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.00
Q3/%
.38
.38
.38
.38
.38
.38
.38
1.42
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
1.64
1.79
1.79
1.79
1.79
1.79
1.79
1.79
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
Qj/%
1.79
1.88
3.38
9.07
26.82
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umis
force: 0.00 N
Pressure: 43.07
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 592.29 um xso = 666.08 urn x90 = 721.22 um
x16 = 619.22 uni xg4 =712.95 urn X99 = 733.62 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:11:53053
SMD = 658.41 um VMD = 660.77 urn
Sv = 0.01nrcm3 V = 91.13 cm- g
90
80
s? u°
rn 70
g, «>
o 60
'S 50
M
0 40
•a
J3
3 ?n
^ 7fl
10
0:
t\
j.
\
i
J
B
him
8
10
2
3
4
0
6
J
80
100
2(
10
4C
0
,•
6(_
•
0
r*
|
|
!
I
i
80
-p
0
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, inn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.02
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
x.. inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
0.00
12.94
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.07 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.46
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 559.37 um xso = 661.21 urn x90 = 720.24 um
x16 = 597.81 urn xg4 = 711.39 um x^ = 733.52 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:12:19,725
SMD = 646.96 um VMD = 651.68 um
Sv =0.01 in2 cm3 V = 92. 74 cm- g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 }fl
^ ">0
10
0:
t\
j.
\
i
J
B
him
8
10
2
3
4
">
6
J
80
100
2(
10
4C
0
J
/
6(_
1
7*
0
r^
(
|
'
J
1
I
so
-p
0
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.02
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
3.07
18.68
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.07 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.46
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:12:45,334
x10 = 548.98 um xso = 659.57 um x90 = 719.91 um
x16 = 586.85 nin xg4 =710.86 urn X99 = 733.49 urn
SMD = 642.68 um VMD = 648.34 um
Sv = 0.01nrcm3 V = 93.36 cm-g
90
80
* u°
rn 70
g, /u
o 60
•a °u
.n
'£ 50
M
u 40
> -tu
•a
J3
3 }fl
u ->0
10
0:
t\
j.
\
i
J
B
him
8
10
2
3
4
0
6
J
80
100
2(
10
4C
0
•
/
7
6(_
,
1
"
0
r*
f
|
J
I
80
-p
0
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.02
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.10%
Qj/%
0.00
0.00
0.00
4.62
20.46
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.46
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 550.15 um xso = 659.95 um x90 = 719.99 inn
x16 = 588.86nni xg4 =710.98 urn X99 = 733.50 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:13:10,896
SMD = 643.26 um VMD = 648.85 urn
Sv = 0.01nrcm3 V = 93.27 cm-g
100
90
70
c
60
£3
£
'£ 50
M
•o
u 40
•a
J3
3 }0
10
ol * I* 1*1*1 '*
8 10
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Qj
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, mn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.02
Xi, mil
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
x.. inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
4.55
20.05
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.13 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.46
Orientation: 90.00
-------
Synrpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 562.70 um x50 = 661.70 um x90 = 720.34 inn
x16 = 598.19nni xg4 =711.55 urn X99 = 733.53 urn
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:1.:..,
SMD = 647.83 um VMD = 652.41 urn
Sv = 0.01 nr cm3 V = 92.63 cm- g
100
90
80
* U°
rn 70
g, «>
o 60
•a °u
.n
'£ 50
M
u 40
> -tu
•a
J3
3 }fl
0 ->o
10
0
—f
1—
^~
u
D
} P
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Qj
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, inn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.l
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Reference
AirSpeed: 1.02
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
x.. inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
3.06
18.03
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.09 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.46
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:31:56,865
x10 =46
xi6 =54.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
75 uin xso = 83.08 uin x90 = 118.59 inn
33^1111 xj4 =111. 32 urn xgg = 145.75 uni
i
6 8 10
__•
I— 1
1
_
^1
1
^
1
L
f
A
,
U i
20 40 60 80
SMD =72.03 urn
Sv = 0.08 nr cm3
•^
f
1
J
f
]
I
VMD = 82.91 urn
V = 832.93 cnr, g
I
' »•
,
100 200 400 600 800
particle size
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.04
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs
0
0
0
2
4
8
14
23
1%
.18
.45
.98
.15
.81
.72
.21
.99
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
39.01
59.43
78.78
95.29
99.76
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:32:23,006
x10 =46
XKJ = 53.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
£ 40
•a
J3
P 30
0 20
10
0
t\
21 urn xso = 82.97 uin x90 = 119.77 um
71 jim xj4 = 112.49 um xgg = 147.41 um
i
6 8 10
__•
I— 1
1
_
^
1
./
1
M'
L
T
>
,
I
r
\
u i
20 40 60 80
SMD = 71.83 um
Sv = 0.08 nr cm3
_^"
f
7
/
•
/
f
1 |
VMD = 83.13 um
V = 835.36 cm2, g
I
* ^
,
100 200 400 600 800
particle size
cumulative distribution
Xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.04
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Q3/%
0.16
0.44
0.98
2.20
4.98
9.08
14.79
24.75
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
39.56
59.20
77.82
94.31
99.54
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.77 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing i
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:32:47318
io =47
16 =54.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
n
32 uin xso = 83.93 uin x90 = 119.52 um
93 jim xj4 = 112.47 um xgg = 146.81 urn
_i
iJ
L*J
I* Ji
b • •
•— H.
__|
|^l
P
J
s
1
*
f
/
1
i
\
tl
'
.
\ t
SMD = 72.83 um
Sv = 0.08 nr cm3
-^
r
j
I
t
r
f
i
i i
VMD = 83.79 um
V = 823.88 cnr/g
|
' »•
j_ j_
6 8 10
20
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
X., Illll
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.04
Xi, Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs
0
0
0
2
4
8
13
23
/%
.17
.43
.95
.07
.60
.36
.68
.22
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
37.96
58.20
77.65
94.66
99.64
100.00
100.00
100.00
\., Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.85 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,17:3.:..,
x10 =46
xi6 =54.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
n
76 urn xso = 83.32 uin x90 = 119.29 uin
33 jim xj4 =1 12.09 um xg9 = 146.65 uni
•^
—
n c
a
1
1
SMD = 72.23 um
Sv = 0.08 nr cm3
•
VMD = 83.28 M
V = 830.72 a
in
ir g
8 10
20
40 60 80 100
particle size pirn
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.04
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 17:28:38
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Q3/%
0.17
0.44
0.97
2.14
4.80
8.72
14.23
23.99
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
38.84
58.94
78.08
94.75
99.65
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:25:3028?
x10 =44
xi6 =50.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
31 uin Xjo = 75.82 uin Xpo = 113.40 inn
60 ^ini xj4 = 103.48 um xgg = 147.70 uin
1
6 8 10
I—I
1
m
1
/*
/
m
i
•-/
L
I
f
\
j^U i
20 40 60 80
SMD = 67.62 nm
Sv = 0.09 nr cm3
Wt
/
•
r
i
i i
VMD = 77.52 urn
V = 887.28 cnr/g
I
* *•
| |
100 200 400 600 SOO
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.05
0.25
0.80
2.16
5.41
10.47
17.88
30.66
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
AirSpeed: 1.05
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
48.86
69.86
85.60
96.08
99.30
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.74%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.54
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:25:55,021
xio =45
Xi6 =51.
100
90
* 8°
g 70
| 60
S
'S 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
51 uin xso = 76.08 urn x90 = 111.27 um
64 um xg4 = 102.28 fim x^ = 142.42 um
i
6 8 10
x1
•— •^'l™ 1
/
•
•
f
/
20 40 60
i
tj
i
so
SMD = 68.43 um
Sv = 0.09 nr cm3
«• •
, •
lr
J-
1
1
VMD = 77.28 fim
Sm = 876.77 cnr/g
• •__«__^L_^i__«_^L__^
"
1
^ F
. ,
100 200 400 600 800
particle size
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.05
Q3/%
0.00
0.09
0.43
1.57
4.65
9.50
16.84
29.65
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
48.40
70.70
86. 94
96.70
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.79%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.54
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:26:21,037
io =45
16 =51.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
00 uin xso = 75.63 uin x90 = 111.95 um
Hum xg4 = 102.59 urn x^ = 146.42 (im
I
I
Li __
6 8 10
20
i--B'"
_
I
S
1
j
m
/
1
c
1
1
/
'
LJ i
40 60 80
SMD = 67.85 um
Sv = 0.09 nr cni3
m^
f
m
'
'
|
VMD = 77.22 um
V = 884.32 cnrYg
I
' ^
i
100 200 400 600 800
particle size
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V, 11111
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference nieasiu-enient: 05-27 11:02:03
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.05
Q3/%
0.03
0.16
0.63
1.94
5.11
10.00
17.37
30.31
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
49.09
70.79
86.53
96.51
99.42
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.76%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.54
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:2.:..,
x10 =44
Xi6 =51.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
n
94 urn xso = 75.84 uin x90 = 112.21 fun
12 jim xj4 = 102.78 um xyg = 145.51 uin
—c
—
r
a
a
n
D
SMD = 67.97 um
Sv = 0.09 nr cm3
D
•
VMD = 77.34 u
V = 882.79 a
in
ir g
8 10
20
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
AirSpeed: 1.05
0.03
0.17
0.62
1.89
5.06
9.99
17.36
30.21
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
48.78
70.45
86.36
96.43
99.57
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.76%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.54
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:24:40740
x10 =10
x16 =30.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
94 uin xso = 54.92 uin x90 = 87.09 uin
66^1111 xg4 =79.97^111 xgg =1 15.66 um
J
1
^
1-
4
1-
1
l-l
1 i
-— *—•— '
l__
•~»
il i
m*
H
t^
_
/
^
1
1
/
i
f
(
i
SMD =21.62 urn
Sv = 0.28 nr cm3
1
i
VMD = 54.29 um
V =2775.51cm2/i
|
* ^
j_ j_
S 10
20
40 60 80 100 200
particle size ^ini
400 600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
5.45
6.40
7.25
8.00
8.97
10.03
10.88
11.72
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
Air Speed: 0.99
12.51
13.18
13.97
15.52
20.91
32.17
45.84
63.02
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
79.81
92.45
97.86
100.00
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.48
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:25:06490
X10 = 11
XKJ =31.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
£ 40
•a
J3
P 30
0 20
10
0
92 uin xso = 54.70 uin x90 = 86.68 um
32 jim xg4 =79.32^1111 xyg =1 15.63 um
-1
H
1
h
1
K
1
IB!
1 i
u m
1 — •— «-
m=*
il i
*^
H
t^
m
1
/
/
1
•
l\
\
SMD =22.14 urn
Sv = 0.27 nr cm3
I
VMD = 54.22 um
V =2710.35 cm2 ^
|
' *•
j_ j_
8 10
20
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
5.21
6.12
6.93
7.65
8.59
9.62
10.45
11.27
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
Air Speed: 0.99
12.05
12.71
13.49
15.03
20.51
32.09
46.14
63.70
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
80.48
92.71
97.87
100.00
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.48
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:25:30,615
xio = 12
xw =32.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
42 uin xso = 55.24 uin x90 = 87.21 uin
19 Jim xg4 =80.03^1111 xg9 = 116.29 urn
-1
1-
1
\-
^
h
-1
l-l
I |
H-^
!— m-*
fc*
ii i
•m-*
M
i^"
_
/
i
/
/
f
1
/
i
J
i
SMD =22.95 urn
Sv = 0.26 nr cm3
1
i
VMD = 54.82 urn
V = 2614.09 cnr g
|
* ^
j_ j_
6 S 10
20
40 60 80 100
particle size ^ini
200
400 600 SOO
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
4.78
5.68
6.50
7.25
8.25
9.36
10.26
11.14
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:08:15
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: All 1003VS
Air Speed: 0.99
Q3/%
11.92
12.53
13.18
14.50
19.64
31.13
45.17
62.79
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qj/%
79.80
92.33
97.70
100.00
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.48
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,13:2.:..,
Z1( = 11
Xi6 =31.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
76 urn xso = 54.95 uin x90 = 86.99 uin
39 ^ini xg4 = 79.77 uin xyg = 115.86uni
~i
c
c
i
c
r i
i
I 6 8
B
i
• •
a c
n
u
1
10 20 40 60 80
SMD =22.24 urn
Sv = 0.27 in- cni3
D ° r
^ 1
VMD = 54.44 u
V =2699.98
I
in
:m-/g
. .
100 200 400 600 800
particle size
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
5.15
6.07
6.89
7.64
8.61
9.67
10.53
11.38
V, 11 111
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaiuarion: \VTNDOX 5.4.2.0, HELD stabil.l
invalidation:
reference nieasiirenient: 05-27 13:08:15
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.99
Q3/%
12.16
12.81
13.54
15.02
20.35
31.80
45.71
63.17
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
80.03
92.50
97.81
100.00
100.00
100.00
100.00
100.00
\,, Hill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.81 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.48
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 454.17 um xso = 634.11 urn x90 = 714.82 um
x16 = 516.95 urn xg4 = 702.72 um KM = 732.98 urn
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:56:29975
SMD = 282.79 um VMD = 580.65 um
Sv = 0.02 nr cm3 V =212.17 cm- g
90
80
* U°
rn 70
g, «>
o 60
•a °u
.n
'£ 50
M
u 40
> -tu
•a
J3
3 ?n
0 ->o
10
n
A
<
8
10
2
3
|
•
4
1
0
l~'
*
6
9
80
I
100
2(
10
4C
•
0
/
•
/
/
61
,
1
m
'
1
0
f
/
1
sc
-p
0
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, uin
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
0.00
0.00
0.00
0.51
2.78
5.55
7.42
8.26
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.00
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
8.26
8.26
8.26
8.26
8.26
8.26
8.26
8.26
x.. inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
8.26
8.26
8.26
15.51
40.53
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.82 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
Xjo = 464.08 um XSQ = 646.32 urn Xpo = 717.26 um
x16 =533.16uni xg4 = 706.62 um X99 = 733.23 urn
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:56:59 584
SMD = 294.66 um VMD = 591.17 um
Sv = 0.02 in2 cm3 V = 203.63 cm- g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 }fl
^ 7ft
10
4
<
8
10
2
3
,
pi
4
-'
0
•
6
9
i i 1 1
80
1 1
100
2(
10
4C
0
•
/
1
61
/
^
/
0
T
|
.
1 |
so
-p
0
particle size
cumulative distribution
j/UB
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, inn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
0.00
0.00
0.00
0.15
1.51
4.14
6.74
8.64
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.00
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
8.64
8.64
8.64
8.64
8.64
8.64
8.64
8.64
x., inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Q3/%
8.64
8.64
8.64
12.37
32.34
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.78 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 ranis', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:57:25,881
x10 = 479.40 um xso = 643.96 urn x90 = 716.79 um
x16 = 532.48 Mm xg4 = 705.87 Mm X99 = 733.18 Mm
SMD = 319.05 um VMD = 595.19 uin
Sv = 0.02nrcm3 V = 188.06 cm-g
100
90
70
c
60
£3
S
'£ 50
M
•o
j; 40
•a
J3
3 }0
10
8 10
40 60 80 100
particle size urn
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.15
1.36
3.62
5.76
7.30
\i, Illll
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
7.30
7.30
7.30
7.30
7.30
7.30
7.30
7.30
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.76 %
Qj/%
7.30
7.30
7.30
12.17
34.10
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:57:54,943
i=
.a
•o
= 50
= 53'
100
90
80
70
60
50
40
30
20
10
1.18 um xso = 644.53 urn x90 = 716.91 um SMD = 361.89 um VMD = 603.87 urn
'.36 MUI xg4 = 706.05 um x^ = 733.19 um Sv = 0.02 nr cm3 V =165. 80 cm- g
™ ™
oLftJLtf
4
1 1*1*1 l|
6 8
10
-
h-ll-»-a
40 60
80
I
\
•
^/
' r*
A
u
1
a
*
/
/
1
i i i i i i i i i
100 200 400 600
1 1
so
0
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.07
0.87
2.58
4.34
5.66
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
66
66
66
ee
66
66
66
5.66
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.79 %
Q3/%
5.66
5.66
5.66
10.91
33.68
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Synrpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:5.:..,
x10 = 474.71 um x50 = 642.23 um x90 = 716.45 inn
x16 = 529.99 nin xg4 =705. 31 urn X99 = 733.14 uni
SMD = 314.60 um VMD = 592.72 urn
Sv = 0.02nrcm3 V = 192.41 cnrg
100
90
70
c
60
£3
£
'£ 50
M
•o
j; 40
•a
J3
3 ^0
10
8 10
40 60 80 100
particle size ^im
200
400
600 800
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.l
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.22
1.63
3.97
6.06
7.47
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
7.47
7.47
7.47
7.47
7.47
7.47
7.47
7.47
X,, HIM
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.79 %
Q3/%
7.47
7.47
7.47
12.74
35.16
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nmi/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.35
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:34:45475
10 = 0.98 urn xso = 2.91 um
16 = 1.27 um xj4 =4.87um
100 - | .mi 1 1
Cumulative distribution Q3 / %
*- 10 Uj 4^ 'Vi O -J 00 O
oooooooooo
:
T
K
Im —
.
, .
I 6 8
X90
XQO
= 57.38 um
= 1 79.68 um
-tit
•
SMD =2.94 urn
Sv = 2.04 nr cm3
l
i i
VMD = 16.68 um
S,,, = 20396.98 cm- g
1
I
10 20 40 60 80 100 200 400 600 800
particle size uni
cumulative distribution
\.i um Qj/%
4.50 83.12
5.50 85.52
6.50 85.91
7.50 85.92
9.00 85.92
11.00 85.92
13.00 85.92
15.50 85.92
V, Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.96
Q3/%
85.92
85.92
85.92
85.92
85.92
85.92
88.13
91.96
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
97.00
97.00
97.00
97.00
97.00
99.02
99.02
99.02
X., II III
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
99.02
99.02
99.83
99.83
99.83
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.09 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:35:19928
x10 =0.$
xw =1-2
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
>8 ii in xjo = 2.92 um Xpo = 58.76 um
7 urn xg4 = 5.06 fim xg9 = 367.40 uni
~i
1"
1
, .
\ 6 8
.
S
B'
m*
i
SMD =2.96nin
Sv = 2.03 in2 cm3
• •-*-"-
i
• i
• \
VMD = 17.37 jim
S,,, = 20287.8 Icm2/g
— H — H H H — H
— 1
•
1
'
I
10 20 40 60 80 100 200 400 600 800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
82
84
85
85
35
85
85
35
/%
.74
.98
.34
.36
.36
.36
.36
.36
Xi, IMIl
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
85.36
85.36
85.36
85.36
85.36
85.36
87.45
91.52
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference nieasiu-enient: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.96
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qj/%
96.82
96.82
96.82
96.82
96.82
98.97
98.97
98.97
\., Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
98.97
98.97
99.82
99.82
99.82
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.12%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:35:47334
x10 =0.$
x16 =1.2
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
>9 ii in xjo = 2.95 um Xpo = 61.09 um
3 urn xg4 = 6.07 fan xg9 = 374.73 urn
J
W
\
, .
\ 6 8
•
/
f
i
SMD = 3.00 uin
Sv = 2.00 nr cm3
• H-iK*
i
• i
• \
VMD = 18.68 fim
S,,, = 20009.58 cnr g
— H — H H m — H
— ~
•
1
'
I
10 20 40 60 80 100 200 400 600 800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
81
83
84
84
'34
84
84
84
/%
.53
.79
.15
.18
.18
.18
.18
.18
Xi, IMIl
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
84.18
84.18
84.18
84.18
84.18
84.18
86.13
90.63
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.96
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
96.55
96.55
96.55
96.55
96.55
98.87
98.87
98.87
v inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
98.87
98.87
99.80
99.80
99.80
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.12%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS Particle Size Analysis
W2NDOX5
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875jim 2009-05-27,15:3.:..,
0.25% R-ll in water
x10 =0.$
xw =1-2
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
A
>9 ii in xjo = 2.93 um Xpo = 59.08 uin
3 um xg4 = 5.33 um xyg = 307.27 uin
i
i
L
i
, .
I 6 8
t
3
0
a
rjl'
i
10 20 40 60 80
SMD = 2.97 uin VMD = 17.57 um
Sv = 2.02nr/cm3 V = 20231.46 cnr/g
D a i
D
^ i
LJ
r1
J
U
1
1
I
100 200 400 600 800
particle size
cumulative distribution
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
82.46
84.76
85.13
85.15
85.15
85.15
85.15
85.15
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
85.15
85.15
85.15
85.15
85.15
85.15
87.24
91.37
evaluation: WINDOX 5.4.2.0, HELD stabil.l
invalidation:
reference measurement: 05-27 15:23:12
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
Air Speed: 0.96
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
96.79
96.79
96.79
96.79
96.79
98.95
98.95
98.95
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
98.95
98.95
99.82
99.82
99.82
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.11 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.72
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:56:37,428
x10 = 46
xi6 =50:
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
6.22 um Xjo = 626.43 um Xpo = 713.29 inn
..Slum xg4 = 700.26 um XQ9 = 732.83 uni
j
•
fl
I
•
I
• 11
6 8 10
20
i
40
60 80
SMD = 476.02 um VMD = 604.78 um
Sv = 0.01nrcm3 V = 126.05 cm- g
^ ^
100 200
• |
~ .
•
.•
/
/
1
/
1
1 r*
I
\
\
\
/
/
• i
400 600 800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.21
.21
.21
.21
.21
.21
.21
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.21
0.21
0.21
0.21
0.21
0.21
0.21
0.21
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003 VS
AirSpeed: 1.10
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
0.21
0.21
0.21
0.21
0.21
0.21
0.21
0.21
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.21
0.68
4.84
18.07
44.74
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.08
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:57:06053
Xjo = 45
xi6 =48^
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
2.77 urn
k93 um
•
J
p
j
p
xso = 609.14 um x90 = 710.12 um
XM = 695.19um xog = 732.51 \im
It -fl
h- • • i
•— •-
m-t
\— i
p
•
j
i
pi
•,
if
SMD = 101.52 um VMD = 584.09 UB
Sv =0.06nrcm3 V = 591.01cm2
•
>!-• • 1
1— •-
• |
1— 1
^r
i
/
1
f
A
*
1 *T
\\
\
I
\
/i
i
/
, i
1 1 1
n
>t
8 10
40 60 80 100
particle size ^ini
200
400
600 SOO
cumulative distribution
h
i
2
2
2
2
2
2
2
/%
.84
.10
.10
.10
.35
.35
.35
.35
Xn Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003 VS
AirSpeed: 1.10
Q3/%
2.35
2.35
2.35
2.35
2.35
2.35
2.35
2.35
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
2.35
2.35
2.35
2.35
2.35
2.35
2.35
2.35
x,, mil
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
Q3/%
2.35
2.64
6.69
21.61
51.77
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.08
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:57:32,975
x10 = 455.56 um xso = 618.84 urn x90 = 711.77 inn
x16 = 490.12 uni xg4 = 697.83 um X99 = 732.68 um
SMD = 111.05 um VMD = 590.69 um
Sv = 0.05 nr cm3 V = 540.29 cm- g
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
*
40 60 80 100
particle size ^im
200
400
600 SOO
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
1.71
1.96
1.96
96
96
96
96
1.96
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.10
Q3/%
96
96
96
96
96
96
96
1.96
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
1.96
1.96
1.96
1.96
1.96
1.96
1.96
1.96
x,, HIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
Qj/%
1.96
2.33
6.43
20.32
48.35
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.08
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 469.19 um xso = 624.85 urn x90 = 712.97 uin
x16 = 504.03 uni xg4 = 699.75 um X99 = 732.80 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:57:58443
SMD = 471.42 um VMD = 604.75 uin
Sv = 0.01 nr cm3 V = 127.28 cnr/g
90
80
0?
f»» 70
c
o 60
'O
3
X>
'£ 50
M
U 40
•a
J3
3 30
ij 2ft
10
4
j
I
<
'
klf
8
10
2
o
4
0
6
J
80
100
2C
10
Ii
_
4C
^
0
/
/
/
1
1
/
6(_
I
1
0
r*
|
!
I
8C
-p
0
particle size
cumulative distribution
j/UB
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.22
.22
.22
.22
.22
.22
.22
Xi, uin
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.10
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
0.22
0.22
0.22
0.22
0.22
0.22
0.22
0.22
x.. inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.22
0.41
4.11
17.89
45.53
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.08
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 460.93 mn xso = 619.82 urn x90 = 712.04 um
x16 = 495.40 uni xg4 = 698.26 um X99 = 732.70 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:5.:..,
SMD = 290.00 um VMD = 596.08 urn
Sy = 0.03 m-/cm3 S,,, = 346.16cnrg
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 ?n
o 20
10
n
4
f
.
1
r
1
t
[•
1
f
3 I
8
hi n n
10
n n
2
a c
3
1
a
4
,
0
P
6
n
9
n
80
100
2(
10
3
B
n
4C
n
0
6(_
n
0
|
. .
soo
particle size
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/°/o
0 . 8 9
1.12
1.12
1.12
1.18
1.18
1.18
1.18
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/
1.
1.
1.
1.
1.
1.
1.
1.
J/o
18
18
18
18
18
18
18
13
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.10
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
1.18
1.18
1.18
1.18
1.18
1.18
1.18
1.18
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
1.18
1.51
5.52
19.47
47.59
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.08
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:18:54318
= 539.78 urn xso = 651.34 urn x90 = 718.27 inn
= 564.47 uni xg4 = 708.23 um x^ = 733.33 um
SMD = 634.36 um VMD = 640.31 um
Sv = 0.01nrcm3 V =94.58 cm- g
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
20
10
0
*
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.36 %
Qj/%
0.00
0.00
0.00
3.98
28.28
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.10
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:19:23240
= 541.82 uin xso = 652.82 urn x90 = 718.56 uin
= 567.67 uni xg4 = 708.70 um x^ = 733.36 um
SMD = 636.14 um VMD = 641.92 urn
Sv = 0.01 nr cm3 V = 94.32 cm- g
90
80
0?
rn 70
g, /u
c
o 60
'G
3
X>
'£ 50
.3
u 40
•a
3 30
ij 2ft
10
4
D
I
<
J
'
B
hi.
8
10
2
o
4
">
6
J
80
100
2(
10
4C
0
^
1
/
/
'
61
1
•
'
0
T
f
|
1
SO
-p
0
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, II III
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.39 %
Qj/%
0.00
0.00
0.00
3.77
26.99
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.10
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:19:5028?
= 541.31 uin xso = 652.91 urn x90 = 718.58 um
= 567.45 MUI xg4 = 708.73 um X99 = 733.36 uni
SMD = 635.97 um VMD = 641.83 uin
Sv = 0.01 nr cm3 V = 94.34 cm- g
100
90
SO
70
60
50
40
30
20
10
0
i=
.a
•o
8 10
40 60 80 100
particle size um
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xi, mil
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, Illll
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.41 %
dispersing method: Defaii
Qj/%
0.00
0.00
0.00
3.96
26.91
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 umi s
force: 0.00 N
Pressure: 43.10
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 540.88 um xso = 652.90 urn x90 = 718.58 um
x16 =567.16 uni xg4 = 708.73 um X99 = 733.36 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:20:16365
SMD = 635.79 um VMD = 641.70 urn
Sv = 0.01nrcm3 V =94.37 cm-g
*
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
20
10
0
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Qj
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
4.09
26.92
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.42 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.10
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 540.95 um xso = 652.49 urn x90 = 718.50 um
x16 = 566.69 uni xg4 = 708.60 um X99 = 733.35 urn
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:..
SMD = 635.57 um
Sv =0.01nrcm3
VMD = 641.44 um
V = 94.40 cm- g
90
80
s? u°
rn 70
g, «>
o 60
'S 50
M
0 40
•a
J3
3 ?n
^ 7fl
10
0
—f
1—
^—
u
D
H rj
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: All 1003VS
AirSpeed: 1.01
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
3.95
27.28
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.39 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mms
force: 0.00 N
Pressure: 43.10
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:48:35,037
io =42
16 =49.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
71 uin xso = 73.61 uin x90 = 104.26 inn
14 jim xg4 =98.74^111 3199 = 129.01 uni
6
S 10
r
20
H
/
•
'
40
1
!
/
i
60
!
Jy
I
/
'
i
so
SMD = 65.49 um
Sv = 0.09 nr cm3
«• •
'
|j|f
r
/
i
VMD = 74.10 fim
Sm =916.11 cm- g
• •__•__•__•_•_•__•
100 200
400
•
I
* ^
600 800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, uin
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
0.04
0.18
0.66
2.15
6.10
11.71
19.48
33.10
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:35:09
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.99
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
52.12
74.49
90.80
98.81
100.00
100.00
100.00
100.00
x., inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.08%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nim/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.26
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:49:02 100
x10 =43
xi6 =49.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
10 uin Xjo = 73.39 uin Xpo = 102.23 fun
53 Jim xg4 = 96.89^111 XQ9 = 123.10 uni
1
6 8 10
20
t -1
K
H
|
^
r
Lf
H
1
II
/
i
I
/
1 1
40 60 80
SMD = 65.34 jim
Sv = 0.09 nr cm3
~J
f
I
i i
VMD = 73.31 urn
V = 918.23cnr/g
1
' »•
| |
100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 16:35:09
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.99
Q3/%
0.02
0.14
0.59
2.08
5.95
11.37
19.04
32.84
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
52.54
76.26
93.12
99.62
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.10%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.26
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:49:27115
x10 =43
xi6 =49.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
60 uin xso = 73.90 urn x90 = 101.24 inn
93 jim xg4 =96.28(im xgg = 121.43 urn
I
I
Li __
6 8 10
20
_
1
/
i _• i 1
j
1
/
J
1
/
,
1
f
/
I i
40 60 80
SMD = 65.63 um
Sv = 0.09 nr cm3
/^
"
j
J
|
VMD = 73.25 um
V =914. 19 cm2, g
I
* "•
1
100 200 400 600 800
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 16:35:09
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.99
Q3/%
0.00
0.13
0.56
1.94
5.66
11.00
18.60
32.12
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
51.73
76.39
94.56
99.96
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.08%
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.26
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:4.:..,
x10 =43
xi6 =49.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
n
14 uin xs
53 jim X&
—c
—
1 = 73.63 uin x90 = 102.57 um
t =97.31nni X99 = 124.52 (im
j-
n
n
c
u
a
I
SMD = 65.49 um
Sv = 0.09 nr cm3
a
VMD = 73.55 u
V = 916.17 a
in
ir g
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
QV
0
0,
0.
2.
5,
11
19
32,
%
.02
.15
.60
.06
.90
.36
.04
.69
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:35:09
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
Air Speed: 0.99
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
52.13
75.71
92.83
99.46
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.09%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.26
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:18:18,084
Xjo = 41
x16 =47.
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
t\
23 uin xso = 67.69 uin x90 = 99.66 uin
07 jim xg4 =91.04(im x^ = 134.05 (im
i
6 8 10
t
,-*
•
}
/
1
t
I
1
T '
J/
Jp
/
T
20 40 60 80
SMD =61.78 urn
Sv =0.10nrcni3
1 ^ » •
f
L
P -
VMD = 69.46 fim
Sm = 97 1.22 cm-, g
• •__•__•__•_•_•__•
•
I
* F
. ,
100 200 400 600 SOO
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.07
Q3/%
0.00
0.08
0.56
2.48
6.95
13.09
23.63
40.81
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
62.96
83.28
93.72
98.43
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.04%
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 rtmi/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:18:48,115
x10 = 41.76 urn xso = 69.19 urn x90 = 102.72 um
x16 = 47.57 jim xg4 =94.94^111 X99 = 138.86 um
*
M
•o
•a
J3
SMD = 63.06 um VMD = 71.27 um
Sv = 0.10nrcm3 V =951.46 cnr/g
1UU
90
on
70
60
SQ
40
30
in
10
0
H1
i
i
1
'
/
•
f
/
/
/
j
,(
f
1
mr*
..W-
/
(
1
r|l
I
*T*
i
6 8 10
20
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, urn
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference nieasiu-enient: 05-27 11:02:03
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.07
Q3/%
0.00
0.06
0.47
2.27
6.58
12.60
22.50
38.68
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
59.82
80.19
91.76
97.76
100.00
100.00
100.00
100.00
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.13 %
dispersing method: Defaii
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 41.31 um x5o = 67.80 urn x90 = 99.84 um
X16 =47.07 jim xj4 =91.30(im xg9 = 134.31 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:19:18271
SMD = 61.99 urn VMD = 69.59 um
Sv = 0.10nrcm3 V = 967.97 cnr/g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 }fl
^ 7ft
10
n
A
<
8
10
2
3
•
4
1
0
/
1
1
1
60
/
j
.,
'
I/
i
80
' . ' '
/
t
P -
100
P •
2(
•
10
pi
• — i
!•-
4C
-•
0
PI
6(_
•
0
|
* *
800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, IIIM
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
0.00
0.03
0.38
2.23
6.83
13.07
23.69
40.68
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.07
\i, inn
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
62.68
83.08
93.63
98.41
100.00
100.00
100.00
100.00
X., II III
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.18%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 uini
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:19:43,943
xjo =40
x16 =46.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
0
t\
93 urn xso = 67.02 uin x90 = 98.29 uin
73 Jim xg4 = 89.57^1111 xgg = 131.92 um
1
6 8 10
20
r
•
}
J
i
J
/
/
/
c
1
t
/
1 1
40 60 80
SMD = 61.38 pm
Sv =0.10nrcni3
• • ™
* i •
|
|
VMD = 68.72 fim
Sm = 977.48 cm-, g
• •__•__•__•_•_•__•
•
1
* *•
,
100 200 400 600 800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.01
0.30
2.19
7.06
13.50
24.36
41.83
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.07
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
64.43
84.58
94.39
98.62
100.00
100.00
100.00
100.00
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.26%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 ruin
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,11:1.:..,
z1( =41
x16 =47.
100
90
* 8°
g 70
| 60
S
~S 50
M
•o
% 40
•a
J3
P 30
0 20
10
n
31 uin xso = 67.92 uin x90 = 100.12 uin
11 Jim xj4 = 91.71^1111 X99 = 134.78 jim
—c
—
r
a
D
[
a
n
I
SMD = 62.05 urn
Sv = 0.10 in- cm3
a r
•
VMD = 69.76 M
V = 967.03 a
in
ir g
8 10
20
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, mil
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qj/%
0.00
0.04
0.43
2.30
6.85
13.06
23.55
40.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 11:02:03
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
user parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.07
\i, HIM
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
62.47
82.78
93.38
98.30
100.00
100.00
100.00
100.00
x., inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
100.00
100.00
100.00
100.00
100.00
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
1.15%
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 nini/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.40
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:48:28,021
Xjo = 533.35 um x$o = 649.15 um x9o = 717.83 um
x16 = 557.71 um xg4 = 707.53 um KM = 733.28 um
SMD = 630.24 um VMD = 636.95 um
Sv = 0.01nrcm3 V = 95.20 cm- g
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
20
10
0
*
8 10
40 60 80 100
particle size fini
200
400
600 800
cumulative distribution
Xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, HIM
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.94 %
Qj/%
0.00
0.00
0.00
5.48
30.11
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.38
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:48:57850
= 558.21 um x50 = 656.93 um x90 = 719.39 um
= 584. 14 Mm xj4 = 710.02 Mm xgg = 733.44 uin
SMD = 645.90 um VMD = 649.54 um
Sv = 0.01nrcm3 V = 92.89 cm-g
100
90
SO
70
60
50
40
30
20
10
0
i=
.a
•o
I
••a
-3
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stnbill
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.00
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xi, Illll
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, Illll
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.94 %
Qj/%
0.00
0.00
0.00
0.00
23.14
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 ranis', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.38
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 563.40 um xso = 661.02 urn x90 = 720.20 um
x16 = 598.20 uni xg4 = 711.33 um x^ = 733.52 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:49:26,771
SMD = 648.71 um VMD = 652.73 urn
Sv = 0.01 nr cm3 V = 92.49 cm- g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 ?n
^ ~>o
10
0:
t\
j.
\
i
J
B
him
8
10
2
3
4
0
6
J
80
100
2(
10
4C
0
|
.
/
6(_
|
1
f
0
r^
f
|
)
so
-p
0
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
1.65
18.90
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.92 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.38
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 551.57 um xso = 657.57 urn x90 = 719.51 um
x16 = 581.99 uni xg4 =710.22 urn X99 = 733.45 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:49:52,646
SMD = 642.77 um VMD = 647.73 urn
Sv = 0.01nrcm3 V = 93.35 cm- g
*
100
90
8°
70
60
~S 50
M
•o
% 40
•a
J3
30
20
10
0
*i*Li4
8 10
20
40 60 80 100
particle size ^ini
200
400
600 SOO
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
2.79
22.51
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.92 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.38
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,14:4.:..,
xlc =55
XKJ = 58(
100
90
* 8°
g 70
| 60
'£ 50
M
•o
5; 40
•a
J3
P 30
0 20
10
0
1.63 um xso = 656.17 urn x90 = 719.23 uin
1.51 urn xg4 = 709.77 um 3199 = 733.42 uni
—t
i—
SMD = 641.90 um VMD = 646.74 um
Sv = 0.01nrcm3 V = 93.48 cm- g
1
n
n
1 r
8 10
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 13:28:25
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
2.48
23.66
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.93 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.38
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 479.97 um xso = 629.69 um x90 = 713.94 um
x16 = 517.68 urn xg4 =701.30 urn X99 = 732.89 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:50:57,193
SMD = 498.30 um VMD = 610.74 um
Sv = 0.01nrcm3 V = 120.41 cm-g
90
80
* U°
rn 70
g, «>
o 60
•a °u
.n
'£ 50
M
u 40
> -tu
•a
J3
3 ?n
0 ->o
10
0:
t\
j
\
<
111
8
10
2
3
4
0
6
J
80
100
2C
10
Ii
m
4C
•
0
/
,
'
61
,
f
1
0
f
I
'
1
|
8C
-p
0
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.17
.17
.17
.17
.17
.17
.17
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/
0.
0.
0.
0.
0.
0.
0.
0.
>/o
17
17
17
17
17
17
17
17
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: 15 second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.10
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
0.17
0.17
0.17
0.17
0.17
0.17
0.17
0.17
Xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Q3/%
0.17
0.31
3.25
15.26
43.03
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 mm
acceleration: 0.00 mm s', velocity: 0.00 uim s
force: 0.00 N
Pressure: 43.32
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 480.99 um xso = 634.08 urn x90 = 714.82 um
x16 = 519.74uni xg4 = 702.71 um X99 = 732.98 um
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:51:28,178
SMD = 489.60 um VMD = 613.55 um
Sv = 0.01nrcm3 V = 122.55 cnr/g
90
80
s? u°
rn 70
g, «>
o 60
'S 50
M
u 40
> -tu
•a
J3
3 }fl
^ 7ft
10
0:
t\
j
\
i
•
<
i
•
•
• ii
8
10
2
3
4
0
6
J
80
100
2C
10
_
4C
9
0
/
,
/
/
6(_
,
1
m
'
1
0
f
[
I
8C
-p
0
particle size
cumulative distribution
X., Illll
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.19
0.19
0.19
0.19
0.19
0.19
0.19
Xi, Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/'
0.
0.
0.
0.
0.
0.
0.
0.
>/0
IS
19
19
19
19
19
19
19
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
revalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.10
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
0.19
0.19
0.19
0.19
0.19
0.19
0.19
0.19
v inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Q3/%
0.19
0.41
3.54
14.78
40.54
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nmi/s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.32
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:51:54,600
x10 =47
XKJ = 51i
100
90
g 70
c
60
£3
S
'S 50
M
•o
sj 40
•a
J3
3 30
10
0
t\
4.03 um xso = 636.61 urn x90 = 715.32 um SMD = 599.54 um VMD = 614.12 urn
>.76 MUI xg4 =703. Slum x^ = 733.03 um Sv = 0.01nrcm3 V = 100.08 cnr/g
™ ™
.
*
I
ri, i.
I 6 8 10 20 40 60 80
I
_^
/
/
,•
1
•
/
' f*
/
!
B
1
J
1
f
\
100 200 400 600
i
800
particle size
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xi, Illtl
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabill
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.10
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X.. Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.65
4.67
15.59
39.02
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 ranis', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.32
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
x10 = 478.33 um xso = 633.46 urn x90 = 714.69 um
x16 = 518.06 uni xg4 =702.51 urn X99 = 732.97 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,15:5.:..,
SMD = 529.15 um VMD = 612.80 urn
Sv = 0.01nrcm3 V =114.35 cnr/g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
M
0 40
•a
J3
3 }fl
^ 7ft
10
0
— r
—
,
n
n
n
8 10
40 60 80 100
particle size ^ini
200
400 600 800
cumulative distribution
X., Illll
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.12
0.12
0.12
0.12
0.12
0.12
0.12
Xi, Mill
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/'
0.
0.
0.
0.
0.
0.
0.
0.
>/0
12
12
12
12
12
12
12
12
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 15:48:35
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.10
\i, um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
0.12
0.12
0.12
0.12
0.12
0.12
0.12
0.12
v inn
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Q3/%
0.12
0.46
3.82
15.21
40.86
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.00 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressiu-e: 43.32
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:25:31,678
X M
Cumulative distribution Q3 /% » £
— II II
*- to OJ 4- VI O\ -J 00 « O u, ...
OOOOOOOOOOO^jjJ
3.93 um xso = 646.57 urn x90 = 717.31 um SMD = 628.77 um VMD = 635.29 um
>.S9um XM = 706.70 urn KM = 733.23 um Sv = 0.01 m-/cm3 V = 95.42 cnr/g
^ ^
^
L-d
1-
^
I
•
1 r*
I
ffl
I
M
u
f
/
/
i
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
v, um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.04
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.34 %
Qj/%
0.00
0.00
0.00
4.83
32.15
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:25:58,818
xjo = 534.44 um x50 = 647.26 um x90 = 717.45 inn
x16 = 556.80 uni xg4 = 706.92 um 3199 = 733.25 urn
100
90
SO
70
60
50
40
30
20
10
0
SMD = 629.44 um VMD = 635.92 urn
Sv = 0.01 nr cm3 V = 95.32 cm- g
i=
.a
•o
I
••a
-3
8 10
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stnbill
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.04
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.32 %
dispersing method: Defaii
Qj/%
0.00
0.00
0.00
4.78
31.62
100.00
100.00
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Syncpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:26:2328?
Xjo = 535.52 um Xjo = 648.38 um x9o = 717.68 um
x16 =558.53uni xg4 = 707.28 um X99 = 733.27 um
SMD = 630.64 urn VMD = 637.01 um
Sv =0.01 in2 cm3 V = 95. 14 cm- g
90
80
s? u°
rn 70
g, /u
o 60
'S 50
.-9
0 40
•a
J3
3 }fl
^ 7ft
10
0:
t\
j.
\
i
J
B
him
8
10
2
3
4
0
6
J
80
100
2(
10
4C
0
•
J
'
61
!
i
"
0
r*
f
I
i
SO
-p
0
particle size
cumulative distribution
xo/um
50
50
6.50
7.50
9.00
11.00
13.00
15.50
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V, HIM
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ms
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.04
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
X,, IIIII
305.00
365.00
435.00
515.00
615.00
735.00
875.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.30 %
Qj/%
0.00
0.00
0.00
4.65
30.73
100.00
100.00
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 rums', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Synpatec GmbH
System-Partikel-Technik
HELOS (H2297) & SPRAYER, R5: 0.5/4.5...875fim
0.25% R-ll in water
Xj0 = 534.63 um xso = 647.40 urn x90 = 717.48 um
x16 = 557.07 uni xg4 = 706.97 urn 3199 = 733.25 uni
HELOS Particle Size Analysis
W2NDOX5
2009-05-27,16:2.:..,
SMD = 629.62 um
Sv =0.01nrcm3
VMD = 636.07 urn
V = 95.30 cm- g
90
80
s? u°
rn 70
g, «>
o 60
'S 50
M
0 40
•a
J3
3 ?n
^ 7fl
10
0
—f
1—
^~
a
H r
8 10
20
40 60 80 100
particle size ^ini
200
400
600 800
cumulative distribution
D/UE
4.
5.
6.
7.
9.
11.
13.
15.
I
50
50
50
50
00
00
00
50
Q3
0
0
0
0
0
0
0
0
/%
.00
.00
.00
.00
.00
.00
.00
.00
Xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
evaluation: \VTNDOX 5.4.2.0, HRLD stabil.1
invalidation:
reference measurement: 05-27 16:10:04
contamination: 0.00 %
trigger condition: IS second scan •
time base: 100.00 ins
start: button
valid: always
stop: 15s real time
nser parameters:
Nozzle: Hypro ULD 120-4
AirSpeed: 1.04
Xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
V Mill
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qj/%
0.00
0.00
0.00
4.75
31.50
100.00
100.00
product: 0.25% R-ll in water
density: 1.00 g cm3
shape factor: 1.00
-opt-
0.32 %
dispersing method: Defaii
rotor inclination: 0.00 °
stroke: 0.00 nun
acceleration: 0.00 nini s', velocity: 0.00 mm s
force: 0.00 N
Pressure: 43.70
Orientation: 90.00
-------
Flux Data
-------
Validation of the Verification Protocol for Low Speed Pesticide Spray Drift Reduction Technologies for Row and Field Crops
Flux and Deposition Measurements
Date Analyzed:
Nozzle ID
6/1/2009
Testl
Analyst
Run#
Transcribed by:
Corbett
1
ZD
Reviewed By
PY
Sample ID
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
STANDARDS
Std
Std
Std
Std
Std
Blk
Position
Blk
Spk
10cm
20cm
30cm
40cm
50cm
60cm
70cm
Blk
Spk
2 m
3m
4 m
5 m
6 m
100ng/ml
50 ng/ml
10 ng/ml
5 ng/ml
1 ng/ ml
Fluoro meter
Reading 1
(ng/mL)
-0.54
115.25
72.5
4.95
0.50
0.24
0.13
0.14
-0.54
72.47
20.01
9.22
4.99
2.23
103.19
52.19
9.02
5.00
1.00
-0.37
Fluorometer
Reading 2
(ng/mL)
-0.54
114.82
72.31
4.95
0.50
0.24
0.13
0.14
-0.58
72.43
20.01
9.22
4.99
2.23
103.03
52.3
9.02
4.97
1.01
-0.37
Average
Reading
(ng/mL)
-0.54
115.035
72.41
103.11
Total
Volume
(mL)
30
60
30
30
30
30
30
30
30
30
30
30
30
30
Total Mass
(ng)
-16.20
6918.30
2188.35
164.70
31.20
23.40
20.10
20.40
-16.80
2190.30
617.10
293.40
166.50
83.70
ng/ml
103.48
52.62
9.39
5.36
1.38
Comments
Matrix
Spk
Cone
(ng/mL)
%
Recovery
( Accu racy)
Run Parameters
Room Temperature
Solution Temp
Nozzel Pressure
Wind Tunnel Velocity
Wind Tunnel Temp
Wind Tunnel RH
Spray Flow rate
Run Time
Uranine Cone in spray
21.4°C
22.0 °C
43.5 psi
1.04 m/sec
25.0 °C
79.8 %
1200 mL/min
15 sec
3.6 g/L
-------
Validation of the Verification Protocol for Low Speed Pesticide Spray Drift Reduction Technologies for Row and Field Crops
Flux and Deposition Measurements
Date Analyzed:
Nozzle ID
6/1/2009
Test 1
Analyst
Run#
Corbett
2
Transcribed by:
ZD
Reviewed By
PY
Sample ID
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
STANDARDS
Std
Std
Std
Std
Std
Blk
Position
Blk
Spk
10cm
20cm
30cm
40cm
50cm
60cm
70cm
Blk
Spk
2m
3m
4 m
5m
6m
100ng/ml
50 ng/ml
10 ng/ml
5 ng/ml
1 ng/ ml
Fluoro meter
Reading 1
(ng/mL)
-0.54
99.12
85.18
5.03
0.32
0.06
0.00
0.12
-0.54
82.14
32.03
15.59
4.65
2.19
103.19
52.19
9.02
5.00
1.00
-0.37
Fluorometer
Reading 2
(ng/mL)
-0.54
99.00
85.18
5.03
0.32
0.06
-0.01
0.12
-0.58
82.14
32.03
15.55
4.65
2.19
103.03
52.30
9.02
4.97
1.01
-0.37
Average
Reading
(ng/mL)
-0.54
99.06
85.18
5.03
0.32
0.06
-0.005
0.12
-0.56
82.14
32.03
15.57
4.65
2.19
103.11
52.25
9.02
4.985
1.005
-0.37
Total
Volume
(mL)
30
90
30
30
30
30
30
30
30
30
30
30
30
30
Total Mass
(ng)
-16.20
8931.60
2571.60
167.10
25.80
18.00
16.05
19.80
-16.80
2481.00
977.70
483.90
156.30
82.50
ng/ml
103.48
52.62
9.39
5.36
1.38
Comments
Matrix
Spk
Cone
(ng/mL)
% Recovery
(Accuracy)
Run Parameters
Room Temperature
Solution Temp
Nozzel Pressure
Wind Tunnel Velocity
Wind Tunnel Temp
Wind Tunnel RH
Spray Flow rate
Run Time
Uranine Cone in spray
21.5 °C
21.9 °C
43.6 psi
0.95 m/sec
25.0 °C
80.1 %
1200 mL/min
15 sec
3.6 g/L
-------
Validation of the Verification Protocol for Low Speed Pesticide Spray Drift Reduction Technologies for Row and Field Crops
Flux and Deposition Measurements
Date Analyzed:
Nozzle ID
6/1/2009
Test 1
Analyst
Run#
Corbett
3
Transcribed by:
ZD
Reviewed By
PY
Sample ID
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
STANDARDS
Std
Std
Std
Std
Std
Blk
Position
Blk
Spk
10 cm
20cm
30cm
40cm
50cm
60 cm
70cm
Blk
Spk
2m
3m
4m
5m
6m
100ng/ml
50 ng/ml
10ng/ml
5 ng/ml
1 ng/ml
Fluorometer
Reading 1
(ng/mL)
-0.54
96.24
71.16
5.11
0.12
0.27
0.29
0.96
-0.54
50.42
10.22
6.26
6.18
5.72
103.19
52.19
9.02
5.00
1.00
-0.37
Fluorometer
Reading 2
(ng/mL)
-0.54
95.93
71.12
5.11
0.12
0.27
0.29
0.96
-0.58
50.73
10.22
6.30
6.22
5.72
103.03
52.3
9.02
4.97
1.01
-0.37
Average
Reading
(ng/mL)
-0.54
96.085
71.14
5.11
0.12
0.27
0.29
0.96
-0.56
50.575
10.22
6.28
6.20
5.72
103.11
52.25
9.02
4.985
1.005
-0.37
Total Volume
(mL)
30
90
30
30
30
30
30
30
30
30
30
30
30
30
Total
Mass
(ng)
-16.20
8663.85
2150.40
169.50
19.80
24.30
24.90
45.00
-1 6.80
1534.05
323.40
205.20
202.80
188.40
ng/ml
103.48
52.62
9.39
5.36
1.38
Comments
Matrix Spk
Cone (ng/mL)
% Recovery
(Accuracy)
Run Parameters
Room Temperature
Solution Temp
Nozzel Pressure
Wind Tunnel Velocity
Wind Tunnel Temp
Wind Tunnel RH
Spray Flow rate
RunTime
Uranine Cone in spra\
21.2 °C
21.8 °C
43.4 psi
0.95 m/sec
24.9 °C
80.1 %
1200 mL/min
15 sec
3.6 g/L
-------
Sample ID
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
osition ci
10
20
30
40
50
60
70
Ref
9.88
3.31
2.05
0.33
0.10
0.06
0.04
Average
All Runs
(mg)
Testl
8.17
2.30
0.17
0.03
0.02
0.02
0.03
Test 2
2.09
0.56
0.03
0.02
0.01
0.01
0.01
Std Dev
Ref Test 1 Test 2
2.87
0.14
0.43
0.08
0.01
0.00
0.01
1.09
0.23
0.00
0.01
0.00
0.00
0.01
0.06
0.09
0.01
0.01
0.01
0.01
0.01
Ref
29.1%
4.3%
20.9%
22.9%
13.6%
2.0%
30.6%
CV
Testl
13.4%
10.1%
1.4%
22.3%
15.6%
21.8%
50.6%
Test 2
3.1%
15.6%
53.0%
71.6%
64.3%
73.5%
54.5%
Sample ID
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
'osition n
2
3
4
5
6
Ref
2.90
2.43
0.96
0.48
0.29
Average
Testl
2.07
0.64
0.33
0.18
0.12
Test 2
0.16
0.02
0.04
0.01
0.01
Std Dev
Ref Test 1 Test 2
0.52
1.42
0.34
0.27
0.17
0.49
0.33
0.14
0.02
0.06
0.07
0.00
0.03
0.00
0.00
Ref
17.9%
58.5%
35.0%
57.2%
58.1%
CV
Testl
23.5%
51.3%
43.5%
13.9%
51.4%
Test 2
42.8%
6.4%
87.0%
29.7%
21.2%
-------
| Reviewed by: |PY
Sample ID
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Monofilament Line
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Position
Blk
Blk
Blk
Blk
Blk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Blk
Blk
Blk
Blk
Blk
Fluorometer
Reading 1
(ng/mL)
0.38
-0.54
-0.55
-0.52
-0.55
3.19
1.19
1.31
1.38
1.34
10.74
8.91
8.09
13.99
8.49
8.38
-0.54
-0.46
-0.52
-0.41
-0.52
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Mylar Card
Spray Solution
Spray Solution
Spray Solution
STANDARDS
Std
Std
Std
Std
Blk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Spk
Blk
Blk
Blk
50 nq/ml
10 nq/ml
5 ng/ml
1.15
1.04
1.06
1.06
1.06
8.49
8.66
8.77
8.52
8.38
8.49
-0.32
-0.32
-0.32
50.35
9.91
4.91
-0.59
Fluorometer
Reading 2
(ng/mL)
0.35
-0.54
-0.55
-0.52
-0.55
3.15
1.19
1.34
1.38
1.34
10.7
8.95
8.09
14.02
8.52
8.31
-0.54
-0.46
-0.52
-0.41
-0.52
Average
Reading
(ng/mL)
0.37
-0.54
-0.55
-0.52
-0.55
3.17
1.19
1.33
1.38
1.34
10.72
8.93
8.09
14.01
8.51
8.35
-0.54
-0.45
-0.52
-0.41
-0.52
Total
Volume
(mL)
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
30
Total
Mass
(ng)
10.95
-16.20
-16.50
-15.60
-16.50
95.10
35.70
39.75
41.40
40.20
321.60
267.90
242.70
420.15
255.15
250.35
-16.20
-13.80
-15.60
-12.30
-15.60
Matrix
Spk Cone
(ng/mL)
50
50
49.7
49.7
49.7
354
354
354
354
354
354
01
Recovery
(Accuracy)
190%
71%
80%
83%
81%
91%
76%
69%
119%
72%
71%
1.15
1.08
1.06
1.06
1.06
8.49
8.63
8.77
8.56
8.38
8.52
-0.32
-0.32
-0.32
49.96
9.91
4.91
-0.59
1.15
1.06
1.06
1.06
1.06
8.49
8.65
8.77
8.54
8.38
8.51
-0.32
-0.32
-0.32
50.16
9.91
4.91
-0.59
30
30
30
30
30
30
30
30
30
30
30
34.50
31.80
31.80
31.80
31.80
254.70
259.35
263.10
256.20
251.40
255.15
-0.32
-0.32
-0.32
nq/ml
50
50
49.7
49.7
49.7
354
354
354
354
354
354
69%
64%
64%
64%
64%
72%
73%
74%
72%
71%
72%
Average
-10.77
1 01 %
83%
-14.70
65%
73%
-0.32
SD
12.15
50%
19%
1.62
2%
1%
0.00
cv
-113%
49%
23%
-11%
4%
2%
0%
Date
5/31/2009
6/1/2009
6/2/2009
6/2/2009
6/2/2009
5/31/2009
6/1/2009
6/2/2009
6/2/2009
6/2/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
5/31/2009
6/1/2009
6/2/2009
6/2/2009
6/2/2009
5/31/2009
6/1/2009
6/2/2009
6/2/2009
6/2/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
6/3/2009
6/2/2009
6/2/2009
6/2/2009
-------
Mylar Card
100.0%
90.0%
80.0%
70.0%
60.0%
o
50.0%
40.0%
30-0%
20.0%
10.0%
0.0%
0.01
0.10
1.00
10.00
Average for all Runs (mg)
-------
Sample preparation: RTI Repeat of Mylar and MF Line
Supplies:
Prepared 0.01 N NaOH is located on bench behind hood 427A-01, to the left of the sink.
Amber vials for curve, spike solutions and sample extracts are located beside the NaOH.
Concentrated uranine is under hood 427A-01.
Mylar cards and monofilament string are in the bench next to the vials.
Pipettes and glassware are in the 427A in marked drawers and cabinets. Please clean after use.
Experiment:
Prepare the following solutions from the concentrated uranine solution located under the hood in 427A-01. Store all
solutions in the capped amber vials in the drawer marked "Owen - Vials in for analysis," which is the third drawer
down on the fluorometer bench by the window.
Five point curve:
400 ng/mL
lOOng/ml
50 ng/ml
lOng/ml
5 ng/ml
Two Spike Solutions
50 ng/mL
350 ng/mL
Mylar Spike Samples
Spike two mylar cards with ImL of the 50 ng/mL spike solution.
Spike two mylar cards with ImL of the 350 ng/mL spike solution.
Allow all 4 cards to sit in hood overnight to dry.
Transfer mylar cards to ziplock bags.
Extract samples one at a time as follows:
Add 30 mL 0.01 N NaOH to the bag
Shake/agitate bag for 10 seconds
Transfer extract to amber vial and label
Monofiliment Spike Samples
Cut four, 1 meter lengths of monofilament line and transfer each line into a ziplock bag.
Spike two bags with ImL of the 50 ng/mL spike solution.
Spike two bags with ImL of the 350 ng/mL spike solution.
Extract samples one at a time as follows:
Add 30 mL 0.01 N NaOH to the bag
Shake/agitate bag for 10 seconds
Transfer extract to amber vial and label
Ziplock Bag Spike Samples
Spike two empty ziplock bags with ImL of the 50 ng/mL spike solution.
Spike two empty ziplock bags with ImL of the 350 ng/mL spike solution.
Extract samples one at a time as follows:
Add 30 mL 0.01 N NaOH to the bag
Shake/agitate bag for 10 seconds
Transfer extract to amber vial and label
30 mL of 0.01N NaOH will be added to the bag to dissolve the uranine into solution. The bag contents will be
shaken for 10 seconds before an aliquot of the liquid is removed for fluorometric analysis (Section B4).
Analysis:Analyze all samples in duplicate.
-------
RTI Results
Sample ID Type
B1
B2
B5
B6
B3
B4
Blank bag
Blank bag
Blank w line
Blank w line
1 MF Line
2 MF Line
3 MF Line
4 MF Line
Blank with mylar
Blank with mylar
5 Mylar Cord
6 Mylar Cord
7 Mylar Cord
8 Mylar Cord
; (ng/mL)
0
0
50
50
350
350
50
50
350
350
Fluorometer
(ng/mL)
1st
0
0
0
0
1.56
1.60
12.01
11.30
0.02
0.01
1.73
1.85
11.30
10.39
Reading
2nd
0
0
0
0
1.55
1.60
12.00
11.25
0.02
0.01
1.73
1.85
11.29
10.38
Averagi
1.56
1.60
12.01
11.28
1.73
1.85
11.30
10.39
% Diff % Recovery
100% Recovery Percent Recovery
2nd Average (Expected Value) (Expected-Actual)/Expected * 100
1.67
1.67
11.67
11.67
1.67
1.67
11.67
11.67
7
4
-3
3
-4
-11
3
11
93%
96%
103%
97%
104%
111%
97%
89%
-------
Appendix B
HSWT Test Data
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 13:1.:..,...
DvlO= 96.67 Dv50= 210.72 Dv90= 335.55
%<100 urn = 10.78 %<200 urn = 45.57
Relative Span = 1.13
I
.2
T3
ID
.3
o
100
90
80
70
60
50
40
30
20
10
0
i
i i
J.IJ.IJ.J.J.L
i
Id....
D
D
1 1
_FE'_
M 1
1 1
/
/
/
/
i*
1
,' }
D 7
,fr
1 l
*
j
i
J
f
f
/
a
1
I
1
-
"
.
0
'n
A
.
\\
\\
\\
\
\
\\
1
L
1 J
:
:
-
•
D uk
| 1.75
| 1.50
: 1 25
- i nn
-
: 0.50
E 0.25
5 000
a
-B
•5
Q
10 20 40 60 80 100
particle size/ \j.m
200
400 600 800
Optical Concentration = 3.45
user parameters:
Nozzle: 11003
Pressure: 43.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 71. 10 F
Relative Humidity: 66.30 %
Solution Temp: 68.60 F
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Qs/%
0.00
00
00
00
00
00
00
00
xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/%
0.00
0.09
0.22
0.46
0.93
1.55
2.32
3.58
xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
5.53
8.44
11.94
17.50
25.78
37.30
51.77
68.00
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qs/%
84.45
95.37
99.59
100.00
100.00
100.00
100.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,13:13:29,400
DvlO= 96.91
%<100 um =
Relative Span
100
10.72
= 1.12
Dv50= 210.86 Dv90= 333.52
%<200 um = 45.50
20 40 60 80100
particle size / um
200
400 600 800
Optical Concentration = 3.39
user parameters:
Nozzle: 11003
Pressure: 43.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 71.10 F
Relative Humidity: 66.30 %
Solution Ternp: 68.60 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
1 .
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0.
0.
0.
0.
1.
n
3.
00
09
21
45
92
54
30
55
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
5.
8.
11.
17.
25.
37.
51 .
68.
50
40
88
41
68
20
72
05
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
84.
95.
100.
100.
100.
100.
100.
»/0
7 2
83
00
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,13:14:03,246
DvlO= 96.21 Dv50= 209.86 Dv90= 332.57
%<100 urn = 10.90 %<200 um = 45.92
Relative Span =1.13
100
8 10
20 40 60 80100
particle size / um
200
400 600 800
Optical Concentration = 3.50
user parameters:
Nozzle: 11003
Pressure: 43.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 71.10 F
Relative Humidity: 66.30 %
Solution Ternp: 68.60 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
1
n
3
.00
.09
.22
.46
.94
.56
.33
.60
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
5.
8.
12.
17.
26.
37.
52.
68.
58
53
08
70
06
63
13
42
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
84.
95.
100.
100.
100.
100.
100.
«/0
97
92
00
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,13:14:44,515
DvlO= 96.91
%<100 um =
Relative Span
100
10.72
= 1.15
Dv50= 211.45 Dv90= 340.55
%<200 um = 45.29
8 10
20 40 60 80100
particle size / um
200
400 600 800
Optical Concentration = 3.44
user parameters:
Nozzle: 11003
Pressure: 43.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 71.10 F
Relative Humidity: 66.30 %
Solution Ternp: 68.60 F
Solution: Rate: 0.00 g/acre
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
5.
6.
1 .
9.
11.
13.
15.
00
50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0.
0.
0.
0.
1.
n
3.
00
09
22
46
94
56
32
58
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
5.
8.
11.
17.
25 .
37.
51 .
67.
52
40
87
38
61
07
46
54
xo/um Qj/°/o
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
83.
94.
98.
100.
100.
100.
100.
65
37
78
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:1.:..,...
DvlO= 129.76
%<100 urn = 5.57
Relative Span = 1.07
Dv50= 275.69 Dv90= 425.30
%<200 urn = 26.05
I
.2
u
1
90
80
70
60
50
40
30
20
10
n
i
i i
J.IJ.IJ.J.J.L
i
Id....
-nj
g
1
=.
T T|
D
fill
1
ff
„/"
I X" *
I""""
I
)
j
f
y
j
f
1
1
j
j
0
"
u
,
„
U
"
rp'i '
5
I
E
\
...
D
1 1
1 -1
D Ut
: 2 25
" 7 00
- ^--""
: 1 75
j 1.50
i i 95
: j 00
I n 7S
: 0 50
j 0.25
i nnn
10 20 40 60 80 100
particle size/ \j.m
200
400 600 800
I
I
Optical Concentration =3.96
user parameters:
Nozzle: Hypro ULD120-04 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Q3/%
0.00
00
00
00
00
00
00
00
21
25
30
37
45
52
62
00
00
50
00
50
50
Qs/%
0.00
0.00
0.09
0.24
0.52
0.85
1.24
1.87
xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
2.86
4.35
6.18
9.13
13. 68
20.48
30.22
43.05
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
Qs/%
59.85
78.20
91.91
98.87
100.00
100.00
100.00
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:15:00,659
D\10= 130.03
°/o<100 urn = 5.54
Relative Span = 1.08
Dv50= 275.78 Dv90= 427.40
%<200 um = 26.01
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.99
user parameters:
Nozzle: Hypro ULD120-04 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.24
.51
.84
.22
.85
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
6.
9.
13.
20.
30.
43.
83
32
14
09
63
43
20
03
xo/um Qj/°/o
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
59.
78.
91.
98.
100.
100.
100.
80
01
46
22
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:15:29,850
D\10= 130.11
°/o<100 urn = 5.53
Relative Span = 1.08
Dv50= 275.77 Dv90= 426.61
°/o<200 um = 25.98
100
*
a
fa
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.96
user parameters:
Nozzle: Hypro ULD120-04 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.24
.51
.83
.22
.85
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
6.
9.
13.
20.
30.
43.
83
31
13
07
61
41
16
01
xo/um Qj/°/o
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
59.
78.
91.
98.
100.
100.
100.
84
10
62
38
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:16:37,703
DvlO= 129.15
°/o<100 urn = 5.65
Relative Span = 1.06
Dv50= 275.51 Dv90= 421.90
°/o<200 um = 26.15
100
*
a
fa
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.92
user parameters:
Nozzle: Hypro ULD120-04 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 004
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.25
.53
.87
.26
.91
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
6.
9.
13.
20.
30.
43.
91
42
27
24
80
60
31
10
xo/um Qj/°/o
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
59.
78.
92.
100.
100.
100.
100.
92
49
65
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:1.:..,...
DvlO= 139.97 Dv50= 297.60 Dv90= 483.88
%<100 um = 4.69 %<200 um = 22.22
Relative Span = 1.16
100
90
^ 80
CO
? 70
'I 60
I
.2
T3
ID
3
50
40
30
I 20
10
J
J
1
A\
1 1
LaA
i
Id....
-nj
La J
a
1
',
T T|
D
fill
i
^
/
D '
| °
"
1
/
f
jr
f
1
1
f
m/
D
n
i
c
n
•'
D
D
"
r, 1
i
"va
--
-: 1.75
:: l 50
.-
:: 1 25
-- i nn
•-
:i
- 0.50
--
- 025
Is ooo
CO
a
I
Q
10
20 40
particle size
60 80 100
200
400 600 800
Optical Concentration = 3.27
user parameters:
Nozzle: Hypro ULD120-04 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Q3/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
xo/um
18.50
21.50
25.00
30.00
37.50
45.00
52.50
62.50
Qs/%
0.00
0.00
0.08
0.21
0.44
0.73
1.06
1.59
xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
2.42
3.67
5.20
7.69
11.55
17.39
25.83
37.12
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Qs/%
52.24
69.62
84.32
93.61
98.25
100.00
100.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:18:06,912
DvlO= 140.95 Dv50= 298.54 Dv90= 483.75
%<100 urn = 4.59 %<200 um = 21.98
Relative Span =1.15
100
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.47
user parameters:
Nozzle: Hypro ULD120-04 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0.
0.
0.
0.
0.
1.
1.
00
00
08
20
43
71
03
55
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
3.
5.
7.
11.
17.
25.
36.
36
59
10
56
39
18
58
83
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
51.
69.
84.
93.
98.
100.
100.
«/o
96
45
29
66
29
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:18:40,421
DvlO= 139.69
°/o<100 urn = 4.71
Relative Span = 1.16
100
*
a
fa
Dv50= 297.40 Dv90= 483.76
°/o<200 um = 22.28
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.26
user parameters:
Nozzle: Hypro ULD120-04 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
\li Illll
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.08
.21
.45
.73
.07
.60
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Q3/%
2
3
5
7
11
17
25
37
.44
.69
.23
.72
.60
.45
.90
.19
\ , .mil
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
52 .
69.
84.
93.
98.
100.
100.
«/o
30
64
33
63
30
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:19:13,990
DvlO= 139.25
°/o<100 urn = 4.75
Relative Span = 1.16
Dv50= 296.87 Dv90= 484.13
°/o<200 um = 22.39
100
*
a
fa
2.25
8 10
20 40 60 80100
particle size / um
200
400 600 800
Optical Concentration = 3.08
user parameters:
Nozzle: Hypro ULD120-04 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.08
.21
.45
.74
.08
.62
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
3.
5.
7.
11.
17.
26.
37.
46
72
27
78
68
55
02
34
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
52 .
69.
84.
93.
98.
100.
100.
«/o
46
76
35
55
17
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:3.:..,...
DvlO= 132.47
%<1QQ urn = 5.32
Relative Span = 1.04
Dv50= 282.40 Dv90= 426.27
%<200 urn = 24.82
Cumulative distribution Q3 / %
^ts>oj-i^L/ia> V
\H
y
A
A
\
n
PI F
H
N
I
1
J\
b
°> J
D U^
i2.50
: 2 25
" 7 00
- ^--""
: 1 75
j 1.50
i i 95
:
i n vs
: 0 50
j 0.25
i nnn
I
I
10 20 40 60 80 100 200
particle size/
400 600 800
Optical Concentration =3.92
user parameters:
Nozzle: Hypro ULC120-04 Y2
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Qs/%
0.00
00
00
00
00
00
00
00
21
25
30
37
45
52
62
00
00
50
00
50
50
Qs/%
0.00
0.00
0.09
0.23
0.50
81
19
80
xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
2.74
4.16
5.90
8.71
13.05
19.53
28.79
41.05
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
Qs/%
57.39
76.31
91.94
99.88
100.00
100.00
100.00
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:32:58,603
D\10= 130.21
°/o<100 urn = 5.55
Relative Span = 1.05
Dv50= 278.41 Dv90= 423.44
°/o<200 um = 25.69
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.99
user parameters:
Nozzle: Hypro ULC120-04 Y2
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.24
.52
.85
.25
.89
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
6.
9.
13.
20.
29.
42.
87
35
16
06
55
25
78
28
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
58.
77.
92.
100.
100.
100.
100.
«/o
76
45
48
00
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:33:31,256
DvlO= 132.37
°/o<100 urn = 5.36
Relative Span = 1.05
Dv50= 283.93 Dv90= 429.40
°/o<200 um = 24.66
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.83
user parameters:
Nozzle: Hypro ULC120-04 Y2
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.24
.50
.83
.21
.82
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
5.
8.
13.
19.
28 .
40.
77
20
93
73
03
44
58
67
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
56.
75.
91.
99.
100.
100.
100.
«/o
3 0
52
26
65
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:34:05,409
D\10= 134.82
°/o<100 urn = 5.06
Relative Span = 1.02
Dv50= 284.84 Dv90= 425.98
%<200 urn = 24.11
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.94
user parameters:
Nozzle: Hypro ULC120-04 Y2
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
vriim
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.08
.22
.46
.76
.12
.69
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2
3
5
8
12
18
28
40
.59
.94
. 62
.34
.56
.90
.01
.19
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
56.
75.
92.
100.
100.
100.
100.
«/o
62
95
08
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:2.:..,...
DvlO= 133.53
%<100 urn = 5.23
Relative Span = 1.09
Dv50= 284.70 Dv90= 443.89
%<200 urn = 24.47
I
.2
u
1
90
80
70
60
50
40
30
20
10
0
1
J
J
1
1 1
U.UL
i
id
-n-
1
0
T T|
D
•rU
i
*
/
\' l
' B^-""
"
J
f
j
/
2
/
/
f
f
a
,
u
i
„«
°
i
D i
,
a
1
I
ft
\
,
L
] .
-: 2 25
"" 7 00
-- ^--""
-: 1 75
-i 1 SO
-= 1 25
-: 1 00
-i n vs
-: 0 50
-i n ?s
•h n nn
2 4 6 8 10 20 40 60 80 100 200 400 600 800
I
Optical Concentration =3.39
user parameters:
Nozzle: Hypro ULD120-04 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
particle size/ \j.m
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Qs/%
0.00
00
00
00
00
00
00
00
21
25
30
37
45
52
62
00
00
50
00
50
50
Qs/%
0.00
0.00
0.09
0.23
49
81
18
77
xo/jim
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
2.70
4.10
5.80
8.57
12.83
19.23
28.40
40.53
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
Qs/%
56. 62
74.85
89. 62
97.93
99.42
100.00
100.00
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:20:55,937
DvlO= 133.08
°/o<100 urn = 5.26
Relative Span = 1.05
Dv50= 283.53 Dv90= 430.64
°/o<200 urn = 24.56
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.03
user parameters:
Nozzle: Hypro ULD120-04 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
5.50
6.50
7.50
9
vriim
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.23
.49
.81
.18
.78
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
5.
8.
12.
19.
28.
40.
71
12
84
62
90
31
50
72
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
56.
75.
90.
100.
100.
100.
100.
«/o
98
59
96
00
00
00
00
Qj/%
0.00
0.00
0.00
0.00
.00 0.00
11.00 0.00
13.00 0.00
15.50 0.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmaun(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:21:28,131
DvlO= 137.37
°/o<100 urn = 4.89
Relative Span = 1.17
100
Dv50= 293.70 Dv90= 479.78
%<200 urn = 23.01
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 2.92
user parameters:
Nozzle: Hypro ULD120-04 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
5.50
6.50
7.50
9
vriim
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.08
.22
.46
.75
.10
.66
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2
3
5
8
12
18
26
38
. 52
.82
.42
.01
.03
.06
.12
.20
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
53.
70.
85.
93.
98.
100.
100.
«/o
45
71
05
90
25
00
00
Qj/%
0.00
0.00
0.00
0.00
.00 0.00
11.00 0.00
13.00 0.00
15.50 0.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmaun(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:22:21,028
DvlO= 130.15
°/o<100 urn = 5.55
Relative Span = 1.05
Dv50= 276.86 Dv90= 421.25
°/o<200 um = 25.84
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 4.22
user parameters:
Nozzle: Hypro ULD120-04 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 004
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
1
.00
.00
.09
.25
.52
.86
.25
.88
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
2 .
4.
6.
9.
13.
20.
29.
42.
86
34
15
07
58
33
97
67
xo/um Qj/°/o
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
59.
78.
92.
99.
100.
100.
100.
43
26
87
90
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:2.:..,...
DvlO= 127.13
%<100 urn = 5.97
Relative Span = 1.08
Dv50= 275.24 Dv90= 425.16
%<200 jim = 26.49
u
1
90
80
70
60
50
40
30
20
10
0
1
^
j
1
i i
L.UL
1
id
-n-
L n J
a
1 1
«
D
D
1
0
T T|
D
1
7
^
' '^ j-/*/l
a
1
7
J
7
^
t
/
~3
n
"
,
| I f
1 f
u
V
n
\
\
\
\
]
1
\
_
]..
a,
1 -1
' J
: 2 25
- 9 00
: 1 75
j 1.50
: 1 95
: 1 00
i n vs
: 0 50
j 0.25
! n nn
2 4 6 8 10 20 40 60 80 100 200 400 600 800
particle size/ \j.m
CO
&
I
,g
• <2
T3
Q
Optical Concentration =3.33
user parameters:
Nozzle: Teejet All 1003 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Qs/%
0.00
00
00
00
00
00
00
00
21
25
30
37
45
52
62
00
00
50
00
50
50
Qs/%
0.00
0.00
0.10
0.26
57
94
38
08
xo/jim
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
3.15
4.72
6. 60
9.61
14.20
20.98
30. 62
43.27
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
Qs/%
59.93
78.32
92.18
98.91
99.81
100.00
100.00
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:25:03,418
DvlO= 128.38 Dv50= 278.97 Dv90= 440.39
%<100 jim = 5.87 %<200 um = 25.82
Relative Span =1.12
100
*
a
fa
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.02
user parameters:
Nozzle: Teejet AI 11003 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0
0
0
0
0
1
2,
.00
.00
.10
.26
.57
.94
.38
.06
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
4.
6.
9.
13.
20.
29.
42.
11
64
48
40
85
45
86
22
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
58.
76.
89.
96.
99.
100.
100.
«/o
44
09
51
72
44
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:25:32,831
DvlO= 125.49
°/o<100 urn = 6.14
Relative Span = 1.07
Dv50= 272.81 Dv90= 417.84
%<200 um = 27.11
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 4.18
user parameters:
Nozzle: Teejet AI 11003 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
2
.00
.00
.09
.26
.57
.95
.39
.11
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
4.
6.
9.
14.
21.
31.
44.
21
83
79
91
62
55
29
03
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
60.
79.
93.
100.
100.
100.
100.
«/o
79
40
44
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:26:02,443
DvlO= 127.52
°/o<100 urn = 5.92
Relative Span = 1.06
Dv50= 273.94 Dv90= 417.25
%<200 um = 26.52
100
*
a
fa
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 2.80
user parameters:
Nozzle: Teejet AI 11003 X
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xo/um
4.50
5.50
6.50
7.50
9.00
11.00
13.00
15.50
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0
0
0
0
0
1
2,
.00
.00
.10
.26
.57
.94
.38
.07
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
4.
6.
9.
14.
20.
30.
43.
12
67
54
54
12
95
70
56
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
60.
79.
93.
100.
100.
100.
100.
«/o
56
46
58
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:2.:..,...
DvlO= 123.60
%<1QQ urn = 6.35
Relative Span = 1.06
cx
I
.2
T3
ID
.3
O
Dv50= 266.50 Dv90= 406.05
%<2QQ urn = 28.24
90
80
70
60
50
40
30
20
10
0
1
l
i i
.I.U.L.UL
i
iu —
u
«QJ
n -
0
2 4 6 8 10 20
.u-
4
ii
3
*
D
1 1
V
1
J
7
\\'_ ^
ft —
i
"
1
1
0
X
i
1
i
i
i
f
„
0
n
,
L1 r '
yf
n
\
I
\
\
I
±
\
H
1
\
1 1 _
" r
U I.U
60 80 100 200 400 600 80C
i 225
" 7 00
- ^--^^
: 1 75
j 1.50
: 1 25
: 1 00
" 0 75
-
: 0 50
j 0.25
S 0.00
)
I
I
particle size
Optical Concentration =3.18
user parameters:
Nozzle: Teejet All 1003 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP_00.
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.OOF
cumulative distribution
xo/um
4.
5.
6.
7.
9.
11.
13.
15.
50
50
50
50
00
00
00
50
Qs/%
0.00
00
00
00
00
00
00
00
21
25
30
37
45
52
62
00
00
50
00
50
50
Qs/%
0.00
05
15
32
65
04
51
24
xo/um
75.00
90.00
105.00
125.00
150.00
180.00
215.00
255.00
Qs/%
3.36
5.02
7.02
10.23
15.12
22.38
32. 63
46.00
xo/um
305.00
365.00
435.00
515.00
615.00
735.00
875.00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffmann@ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
Qs/%
63.43
82.33
95.39
100.00
100.00
100.00
100.00
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:27:51,656
DvlO= 122.92
°/o<100 urn = 6.39
Relative Span = 1.04
Dv50= 263.74 Dv90= 396.66
°/o<200 um = 28.75
100
*
a
fa
8 10
20 40 60 80100
particle size / jim
200 400 600 800
Optical Concentration = 3.23
user parameters:
Nozzle: Teejet AI 11003 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Temp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
0
1
2
.00
.00
.10
.26
.59
.98
.45
.20
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
5.
7.
10.
15.
22.
33.
46.
34
02
07
34
35
76
23
88
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
64.
84.
97.
100.
100.
100.
100.
»/0
7 2
19
04
00
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:28:23,068
DvlO= 123.67
°/o<100 urn = 6.37
Relative Span = 1.07
Dv50= 268.28 Dv90= 411.33
°/o<200 um = 27.96
100
*
a
fa
8 10
20 40 60 80100
particle size / Jim
200 400 600 800
Optical Concentration = 3.09
user parameters:
Nozzle: Teejet AI 11003 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Ternp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
1
1
2
.00
.08
.18
.36
.69
.09
.55
.29
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3
5
7
10
15
22
32
45
.41
.05
.04
.21
.05
.20
.29
.44
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
62 .
81.
94.
100.
100.
100.
100.
«/o
60
17
51
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009 03 30,15:28:51,403
DvlO= 124.22 Dv50= 267.49 Dv90= 410.16
%<100 urn = 6.30 %<200 um = 28.00
Relative Span = 1.07
100
*
a
fa
8 10
20 40 60 80100
particle size / um
200 400 600 800
Optical Concentration = 3.20
user parameters:
Nozzle: Teejet AI 11003 Y
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Ternp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
vriim
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
1
1
2
.00
.07
.17
.35
.67
.06
.51
.24
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
4.
6.
10.
14.
22.
32.
45.
34
98
96
12
97
17
38
67
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
62 .
81.
94.
100.
100.
100.
100.
«/o
95
62
61
00
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clmt.hoffinann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
IJC j~\A United States Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875um
2009-03-30, 15:3.:..,...
DvlO= 121.07
%
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:30:04,209
DvlO= 120.69
°/o<100 urn = 6.69
Relative Span = 1.09
Dv50= 263.90 Dv90= 408.04
°/o<200 um = 29.13
100
*
a
fa
8 10
20 40 60 80100
particle size / Jim
200 400 600 800
Optical Concentration = 3.05
user parameters:
Nozzle: Teejet All 1003 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 001
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Ternp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0.
0.
0.
0.
0.
1.
1.
2.
00
08
18
37
72
14
62
40
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
5.
7.
10.
15.
23.
33.
46.
57
30
39
72
77
19
57
94
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
64.
82.
94.
100.
100.
100.
100.
«/o
14
29
8 3
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:30:33,375
DvlO= 121.84
°/o<100 urn = 6.54
Relative Span = 1.08
Dv50= 264.10 Dv90= 407.46
%<200 um = 28.92
100
*
a
fa
8 10
20 40 60 80100
particle size / Jim
200 400 600 800
Optical Concentration = 3.10
user parameters:
Nozzle: Teejet All 1003 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 002
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Ternp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
1
1
2
.00
.07
.17
.35
.68
.09
.56
.31
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
5.
7.
10.
15.
22 .
33.
46.
46
16
22
52
55
97
39
84
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
64.
82.
94.
100.
100.
100.
100.
«/0
18
45
89
00
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
-------
LJSDA IJnlt*d S'*1*8 Department Ol Agriculture
Agricultural Research Service
USDA - ARS - Aerial Application Group
College Station, TX
EPA DRT Tests - Mar 2009
HELOS (H1780) & SPRAYER, R5: 0.5/4.5...875fim
2009-03-30,15:31:02,525
DvlO= 120.67 Dv50= 264.14 Dv90= 408.86
%<100 urn = 6.69 %<200 um = 29.10
Relative Span = 1.09
100
8 10
20 40 60 80100
particle size / Jim
200
400 600 800
Optical Concentration = 2.78
user parameters:
Nozzle: Teejet All 1003 Z
Pressure: 40.00 psi
Air Speed: 120.00 MPH
Orientation: 0.00 deg
Rep: REP 003
Air Temp: 76.20 F
Relative Humidity: 55.50 %
Solution Ternp: 75.00 F
cumulative distribution
Xn Mil)
4 .50
.50
.50
.50
.00
.00
13.00
15.50
5.
6.
7.
9.
11.
Qj/%
0.00
0.00
0.00
0.00
0.00
0.00
0.00
0.00
\,i Illll
18.
21.
25.
30.
37.
45.
52 .
62.
50
50
00
00
50
00
50
50
Qj/%
0
0
0
0
0
1
1
2
.00
.08
.18
.37
.71
.12
.61
.39
\n. Mill
75.
90.
105.
125.
150.
180.
215.
255.
00
00
00
00
00
00
00
00
Qs/%
3.
5.
7.
10.
15.
23.
33.
46.
56
30
39
72
77
18
55
87
xo/um
305.
365.
435.
515.
615.
735.
875.
00
00
00
00
00
00
00
Qj/'
64.
82.
94.
100.
100.
100.
100.
»/o
00
11
70
0 0
00
00
00
Contact Information:
Clint Hoffmann: 979.777.0815, clint.hoffhiann(S)ars.usda.gov
Brad Fritz: 979.260.9227, brad.frtiz@ars.usda.gov
------- |