United States
                    Environmental Protection
                    Agency
National Kisk Management
Research Laboratory
Cincinnati, OH 45268
                    Research and Development
EPA/600/SR-95/113     February 1996
& EPA      Project  Summary
                    New Chemical Alternatives  for  the
                    Protection  of Stratospheric Ozone
                    Darryl D. DesMarteau and Adolph L. Beyerlein
                      Chlorofluorocarbons (CFCs) and their
                    brominated analogs (halons) are rec-
                    ognized as potent contributors to deple-
                    tion of the Earth's stratospheric ozone
                    layer. By international agreement, such
                    chemicals are to be phased out of the
                    worldwide market. Additionally,  certain
                    partially halogenated  CFCs (or
                    hydrochlorofluorocarbons, HCFCs)
                    have likewise  been recognized as
                    stratospheric ozone depleters and are
                    also to be phased out of production
                    by developed countries in a step-wise
                    progression over the period 1996 to
                    2030.
                      Because of the enormous commer-
                    cial importance of the CFCs,  HCFCs,
                    and halons,  and because few  chemi-
                    cals were readily available or had been
                    proven  acceptable for use in  the nu-
                    merous applications  in which the
                    ozone-depleting substances were em-
                    ployed, the U. S. Environmental  Pro-
                    tection Agency and the Electric Power
                    Research Institute sponsored a study
                    of additional potential alternative chemi-
                    cals.
                      This study focused on the investiga-
                    tion of  fluorinated  derivatives  of pro-
                    pane and butane to determine  if syn-
                    thesis routes of such compounds were
                    feasible and economical, and to mea-
                    sure the physical properties needed to
                    evaluate the  compounds as  alterna-
                    tives. This work resulted in the  investi-
                    gation of 25 compounds including 15
                    hydrofluorocarbons (MFCs), 9  HCFCs,
                    and 1 hydrofluoroether (HFE). Several
                    of the compounds studied had not been
                    previously synthesized and, for many
 of those which had been reported in
 the literature, this study resulted in im-
 proved synthesis  methods. Also, most
 compounds which had a prior litera-
 ture reference had only a boiling point
 measurement. This study,  in addition
 to the synthesis  effort, resulted in a
 sizeable body of thermophysical  prop-
 erty data for each chemical.
  This Project Summary was developed
 by  the National Risk Management Re-
 search Laboratory's Air Pollution Pre-
 vention and Control Division, Research
 Triangle  Park, NC,  to  announce key
 findings of the research project that is
 fully documented in a separate report
 of the same title (see Project Report
 ordering information at back).

 Introduction
  Twenty-four fluorinated propane and bu-
 tane derivatives and one fluorinated ether
 were evaluated as possible alternatives for
 CFCs and long-lived HCFCs. Boiling  points
 for  these chemicals range from -34.6 to
 76.7°C. Therefore,  these chemicals pro-
 vide potential  alternatives  for a  broad
 range of applications, e.g.,  as refriger-
 ants, foam blowing agents, and solvents.
 Emphasis is on hydrogen-containing com-
 pounds that are expected to have finite
 atmospheric lifetimes which reduce their
 global warming potential. Sixteen of the
 chemicals  investigated contain no chlo-
 rine or bromine and therefore have zero
 ozone depletion potential. The remaining
 nine chlorine-containing chemicals were
 selected for investigation before regula-
 tory restrictions were imposed on HCFCs.
 Nevertheless, the low chlorine content of

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the nine  HCFCs studied, coupled with a
finite atmospheric  lifetime,  may  in some
cases yield an alternative with a negligible
ozone depletion potential.
  Selection  and evaluation  of the com-
pounds as alternatives require: (1) a knowl-
edge  of  appropriate physical properties
and (2) possible synthesis routes. Both of
these requirements were investigated in
this research. This study emphasized syn-
thesis routes using  relatively  inexpensive
commercially available starting materials
and  established  synthesis  procedures
(chlorination, hydrogenation, and addition
of hydrogen fluoride) which  are carried
out industrially. This is  important in order
for a chemical to be an economically vi-
able alternative for other than a small spe-
cialty market.

Experimental Procedure
  Except for one hydrofluoroether (HFE-
125),  which was obtained  commercially
with  98% purity and then  repurified,  all
samples  employed for property measure-
ments  were synthesized  with  at least
99.5% purity. Synthesized chemicals were
identified and their purity  checked by a
combination  of  nuclear magnetic reso-
nance spectrometry, high  pressure Fou-
rier transform infrared spectrometry,  gas
chromatography, and mass  spectrometry.
Melting  point, boiling point, vapor pres-
sures below the boiling point,  critical tem-
perature, critical  density, liquid densities,
and  heat of vaporization  at the boiling
point were measured for all 25  compounds.
For four  compounds  (HFE-125,  HFC-
227ea, HFC236ea,  and HFC-245cb), the
vapor pressure was measured as a func-
tion of temperature to within 1% accuracy
from below the boiling point to the critical
temperature.
   Vapor density in  the liquid-vapor coex-
istence region and vapor pressure between
the boiling point and the  critical point were
estimated by a  modified  corresponding
states technique.  The reference fluid  for
the modified corresponding states calcu-
lations was  commercially available HFC-
134a (1,1,1,2-tetrafluoroethane),  and the
equation  of state used for the reference
fluid  was the modified Benedict-Webb-
Rubin equation. Heats of vaporization be-
tween the boiling point  and critical point
were calculated from the heat of vaporiza-
tion at the  boiling point, the boiling point
temperature, and the critical temperature.
Ideal gas heat capacities and vapor-phase
thermal conductivities were estimated by
functional group additivity methods.

Results
  Table 1 lists the 25 compounds investi-
gated by ASHRAE (American  Society of
Heating,  Refrigerating and Air-Condition-
ing  Engineers) refrigerant code designa-
tion and by chemical formula.

Table 1. Compounds Investigated by ASHRAE
Refrigerant Designation and Chemical Formula
Compound
(ASHRAE Code)
HFE-125
HFC-227ea
HFC-227ca
HFC-236fa
HFC-236ea
HFC-236cb
HFC-236ca
HFC-245fa
HFC-245ca
HFC-245cb
HFC-254cb
HFC-329ccb
HFC-338eea
HFC-338cca
HFC-338ccb
HFC-347ccd
HCFC-225ba
HCFC-225da
HCFC-226da
HCFC-226ea
HCFC-234da
HCFC-235ca
HCFC-243da
HCFC-244ca
cy-HCFC-326d
Chemical
Formula
CF3OCF2H
CF3CHFCF3
CF3CF2CF2H
CF3CH2CF3
CF3CHFCF2H
CF3CF2CFH2
CF/YCF2CF2H
CF3CH2CF2H
CHF2CF2CFH2
CF3CF2CH3
CF2HCF2CH3
CF3CF2CF2CF/Y
CF3CFHCFHCF3
CHF2CF2CF2CF/Y
CF3CF2CF2CFH2
CF3CF2CF2CH3
CF3CFCICFHCI
CF3CHCICF2CI
CF3CHCICF3
CF3CHFCF2CI
CF3CHCICFHCI
CF3CF2CH2CI
CF3CHCICH2CI
CF//CF2CH2C/
cy-(CFJ3CHCI
  Table 2 lists the 25 compounds studied
along with their boiling  point (Tb),  melting
point (TJ, heat of vaporization at the boil-
ing  point (AH  ), critical temperature (Tc),
critical  pressure (Pc), critical density (dc),
and liquid heat capacity at 40°C (Cpl).

Conclusions
  From the data acquired in this study, it
appears that several of the chemicals syn-
thesized  are  worthy of consideration  as
alternatives to the ozone-depleting CFCs
and  HCFCs.  Table 3  presents selected
apparent best candidate alternatives from
this study based on a comparison of their
thermophysical properties with  those of
commercially important CFCs and  HCFCs
and the fact  that  these candidates have
zero ozone depletion potentials. Also, pref-
erence was given to fluorinated propanes
over fluorinated  butanes on the premise
that the latter would likely be more expen-
sive to produce (cost generally correlates
with  total  fluorine  content) and  that,  for
insulation foam production, the butane de-
rivatives would likely  have higher vapor
thermal conductivities than the  propane
derivatives. These presumptions are some-
what tenuous, however,  and the possibil-
ity that  certain of the fluorinated butanes
may be excellent  candidates should not
be discounted.
  No fluorinated propane derivatives with
as low a boiling point as that of CFC-12
(dichlorodifluoromethane,  Tb  =  -29.8°C)
were found.  After some searching, HFC-
245cb was synthesized with a  boiling point
of -18.3°C.   Its  critical temperature of
108.5°C compares well with the  critical
temperature  of CFC-12 (112°C). There-
fore, HFC-245cb might  be  an alternative
for CFC-12 for some applications as would
HFC-227ca and -227ea with boiling points
of-16.3 and -18.3°C, and critical tempera-
tures of 106.3 and 102.8°C, respectively.
  HFE-125, with a boiling point of -34.6°C
and critical temperature of 80.7°C, appears
to be the best  candidate  alternative  for
CFC-115( 1,1,1,2,2-pentafluorochloroethane,
Tb = -39.2°C, Tc = 79.9°C)  and  HCFC-22
(difluorochloromethane, Tb = -40.6°C, T  =
96.15°C).
  HFC-245ca and -245fa with  boiling
points  of  25.0 and  15.3°C  and critical
temperatures of 178.4 and  157.5°C,  re-
spectively, are promising candidates to
replace CFC-11 (fluorotrichloromethane,
T  = 23.8°C, T  = 198.1°C), HCFC-123
(1,1,1-trifluoro-2,2-dichloroethane, T  =
27.9°C,  Tc = 183.8°C),  and HCFC-141b
(1-fluoro-1,1-dichloroethane, Tb = 32.2°C,
Tc = 204.2°C) as a refrigerant in low pres-
sure chillers and/or as a blowing agent in
the manufacture  of polyisocyanurate  in-
sulation foam. All HFC-245 isomers pos-
sess a hydrogen content sufficient to pos-
sibly render them borderline flammable.
Therefore, the  flammabilities  of these
chemicals should be evaluated.
  A  number of  CFC-114  (1,1,2,2,-
tetrafluoro-1,2,-dichloroethane, Tb = 3.7°C,
Tc =  145.7°C)  alternatives are  possible
from the  chemicals synthesized. HFCs-
236ea,  -236fa, and -236cb with boiling
points  of  6.5, -1.1, and -1.4°C, respec-
tively, and HFC-254cb with a boiling point
of -0.8°C  are  especially attractive. How-
ever, the relatively high  hydrogen-to-fluo-
rine  atom ratio  of HFC-254cb poses  a
flammability concern for  this compound.

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Table 2.  Boiling Point, Melting Point, Critical Properties, Heat of Vaporization at the Boiling Point, and
         Liquid-Phase Heat Capacity for the 25 Compounds Studied.
Compound
HFE-125
HFC-227ea
HFC-227ca
HFC-236fa
HFC-236ea
HFC-236cb
HFC-236ca
HFC-245fa
HFC-245ca
HFC-245cb
HFC-254cb
HFC-329ccb
HFC-338eea
HFC-338cca
HFC-338ccb
HFC-347ccd
HCFC-226da
HCFC-226ea
HCFC-235ca
HCFC-244ca
HCFC-225da
HCFC-225ba
HCFC-234da
HCFC-243da
cy-HCFC-326d
Tb(°C)
-34.6
-18.3
-16.3
-1.1
6.5
-1.4
12.6
15.3
25.0
-18.3
-0.8
15.1
25.4
42.5
27.8
15.1
14.1
17.6
28.1
54.8
50.8
51.9
70.1
76.7
38.1
Tm(°C)
-156.1
-126.8
-140.3
-94.2
-146.1
-105.4
-123.3
-102.1
-73.4
-81.1
-121.1
-122.3
-91.5
-91.0
-119.4
-124.9
-119.6
-134.0
-85.0
-101.8
-130.3
-132.7
-98.0
-71.6
-94.8
(kJ/mof)
21.92
22.29
23.69
25.66
26.83
25.25
26.59
27.96
29.21
23.59
24.86
26.71
27.79
31.13
26.36
25.82
24.64
26.26
27.57
31.07
25.89
29.38
31.70
30.86
28.69
TC(°C)
80.7
102.8
106.3
130.6
141.1
130.1
155.2
157.5
178.4
108.5
146.1
140.2
148.5
186.4
160.5
144.2
158.2
158.3
170.3
221.0
206.2
212.9
242.5
251.9
196.9
Pc (kPa)
3253
2943
2874
3177
3533
3118
3405
3623
3855
3264
3753
2391
2475
2792
2552
2570
3024
2939
3084
3714
3006
3074
3353
3496
2749
dc (kg/m3)
584
580
594
556
571
545
558
529
529
499
467
600
581
578
562
532
591
584
550
525
589
586
552
514
515
cpl
(kJ/kg °C)
1.327
1.258
1.254
1.371
1.304
1.438
NA
1.422
1.454
1.457
1.590
1.223
NA
1.333
1.342
1.383
1.207
1.205
1.275
1.160
1.087
1.087
1.176
1.234
1.158
NA = not available
Table 3. Selected Possible Alternatives for Commercially Important CFCs and HCFCs
CFCorHCFC
To Be Replaced
ASHRAE Code
of Alternative
Chemical Formula
of Alternative
       Chemical Name
       of Alternative
CFC-11,
HCFC-123,
HCFC-141b

CFC-12
CFC-114
CFC-115,
HCFC-22
 HFC-245ca
 HFC-245fa
 HFC-227ea
 HFC-227ca
 HFC-245cb

 HFC-236ea
 HFC-236fa
 HFC-236cb
 HFC-254cb

 HFE-125
 CF/YCF2CFH2
 CF3CH2CF2H
 CF3CHFCF3
 CF3CF2CF/y
 CF3CF2CH3

 CF3CHFCF2H
 CF3CH2CF3
 CF3CF2CFH2
 CF/YCF2CH3

 CFjOCF/Y
1,1,2,2,3-pentafluoropropane
1,1,1,3,3-pentafluoropropane
 1,1,1,2,3,3,3-heptafluoropropane
 1,1,1,2,2,3,3-heptafluoropropane
 1,1,1,2,2-pentafluoropropane

 1,1,1,2,3,3-hexafluoropropane
 1,1,1,2,2,2-hexafluoropropane
 1,1,1,2,2,3-hexafluoropropane
1,1,2,2-tetrafluoropropane

 pentafluorodimethylether

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   D. DesMarteau and A. Beyerlein are with Clemson University, Clemson, SC 29634.
   N. Dean Smith is the EPA Project Officer (see below).
   The complete report, entitled "New Chemical Alternatives for the Protectin of
    Stratospheric  Ozone," (Order No.  PB95-260220; Cost  $27.00,  subject to
    change) will be available only from:
           National Technical Information Service
           5285 Port Royal Road
           Springfield, VA 22161
           Telephone: 703-487-4650
   The EPA Project Officer can be contacted at:
           Air Pollution Prevention and Control Division
           National Risk Management Research Laboratory
           U.S. Environmental Protection Agency
           Research Triangle Park, NC 27711
United States
Environmental Protection Agency
National Risk Management Research Laboratory (G-72)
Cincinnati, OH 45268

Official Business
Penalty for Private Use $300
      BULK RATE
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         EPA
   PERMIT No. G-35
EPA/600/SR-95/113

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