United States Environmental Protection Agency National Risk Management Research Laboratory Research Triangle Park, NC 27711 Research and Development EPA/600/SR-95/163 December 1995 EPA Project Summary Interlaboratory Study of a Test Method for Measuring Total Volatile Organic Compound Content of Consumer Products E. E. Rickman, Jr., G. B. Howe, and R. K. M. Jayanty The full report describes results of an interlaboratory study to estimate re- peatability (precision of analyses per- formed by a single laboratory) and re- producibility (precision analyses per- formed by different laboratories) of a consumer products volatile organic compound (VOC) measurement method based on EPA Method 24 (for VOCs in surface coatings). (NOTE: Consumer products are significant sources of VOCs, which are precursors to the for- mation of ozone in photochemical smog.) This Project Summary was developed by EPA's National Risk Management Research Laboratory's Air Pollution Prevention and Control Division, Re- search Triangle Park, NC, to announce key findings of the research project that is fully documented in a separate report of the same title (see Project Report ordering information at back). Overview The Clean Air Act Amendments of 1990 require the reduction of VOC emissions in consumer products, which have been iden- tified as a "major" source and will be sub- ject to future regulations. Since EPA has no established method for determining VOC content in consumer products, this study focused on achieving that goal. EPA Method 24 has been modified so that it is viable for measurement of VOC in con- sumer products. The interlaboratory study examines the precision of the modified EPA Method 24, used for analysis of VOC content in consumer products, with that of EPA Method 24, used for determining VOC content in paints and coatings. As a result of the study, further modifications were made. As anticipated, dense foams were difficult to analyze; therefore, this category of consumer products was not included in the interlaboratory study. The mean method repeatability was found to be 2.7 weight percent VOC, and the mean method reproducibility was found to be 4.8 weight percent VOC. Method repeatability ranged from 0.2 to 4.4 weight percent VOC, and reproducibility ranged from 0.6 to 11.9 weight percent VOC. The precision of the consumer products VOC method for consumer product samples is similar to that of EPA Method 24 applied to surface coatings. Results show that the consumer products VOC method is suit- able for analyzing the volatile content of a wide variety of consumer products. ------- £. E. Rickman, Jr., G. B. Howe, and R. K. M. Jayanty are with Research Triangle Institute, Research Triangle Park, NC 27709. J. Kaye Whitfield is the EPA Project Officer (see below). The complete report, entitled "Interlaboratory Study of a Test Method for Measuring Total Volatile Organic Compound Content of Consumer Products," (Order No. PB96-121652; Cost: $27.00, subject to change) will be available only from: National Technical Information Service 5285 Port Royal Road Springfield, VA 22161 Telephone: 703-487-4650 The EPA Project Officer can be contacted at: Air Pollution Prevention and Control Division National Risk Management Research Laboratory U.S. Environmental Protection Agency Research Triangle Park, NC 27711 United States Environmental Protection Agency National Risk Management Research Laboratory (G-72) Cincinnati, OH 45268 Official Business Penalty for Private Use $300 BULK RATE POSTAGE & FEES PAID EPA PERMIT No. G-35 EPA/600/SR-95/163 ------- |