United States       Prevention, Pesticides    EPA712-C-98-083
         Environmental Protection    and Toxic Substances    January 1998
         Agency        (TS-788)
&EPA   Fate, Transport and
         Transformation Test
         Guidelines
         OPPTS 835.3180
         Sediment/Water
         Microcosm
         Biodegradation Test

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                           INTRODUCTION
     This guideline is one  of a  series  of test  guidelines that have been
developed by the Office of Prevention, Pesticides and Toxic Substances,
United States Environmental  Protection Agency for use  in the testing of
pesticides and toxic substances, and the  development of test data that must
be submitted to the Agency  for review under Federal regulations.

     The Office of Prevention, Pesticides and Toxic Substances (OPPTS)
has  developed this guideline through  a process of harmonization that
blended the testing  guidance  and requirements that  existed in the Office
of Pollution Prevention and  Toxics  (OPPT) and appeared in Title  40,
Chapter I,  Subchapter R of the Code of Federal Regulations  (CFR),  the
Office of Pesticide Programs (OPP) which appeared in publications of the
National Technical  Information Service (NTIS) and the guidelines pub-
lished by the Organization  for Economic Cooperation and Development
(OECD).

     The purpose of harmonizing these  guidelines  into a single set of
OPPTS guidelines is to minimize  variations among the testing procedures
that must be performed to meet the data  requirements of the U. S. Environ-
mental Protection Agency  under  the Toxic  Substances  Control Act  (15
U.S.C. 2601) and the Federal Insecticide, Fungicide and Rodenticide Act
(7U.S.C. I36etseq.).

     Final  Guideline Release: This guideline  is available from the U.S.
Government Printing Office, Washington, DC 20402 on The Federal Bul-
letin   Board.   By  modem  dial   202-512-1387,  telnet   and   ftp:
fedbbs.access.gpo.gov  (IP 162.140.64.19), or  call 202-512-0132 for disks
or paper copies.  This  guideline is also available electronically in ASCII
and PDF (portable document format) from EPA's World Wide Web  site
(http://www.epa.gov/epahome/research.htm) under the heading "Research-
ers and Scientists/Test Methods and Guidelines/OPPTS  Harmonized Test
Guidelines."

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OPPTS 835.3180   Sediment/water microcosm biodegradation test.
     (a) Scope—(1) Applicability. This guideline is intended to meet test-
ing  requirements   of both the  Federal  Insecticide,  Fungicide,  and
Rodenticide Act (FIFRA) (7 U.S.C. 136, et seq.) and the Toxic Substances
Control Act (TSCA) (15 U.S.C. 2601).

     (2) Background. The  source material used in developing this har-
monized OPPTS test guideline are the articles referenced under paragraphs
(e)(3) through (e)(9) and (e)(ll) through (e)(16) of this guideline.

     (b) Introductory  information—(1)  Prerequisites.  Sediment and
water containing a representative sample of the natural microbial commu-
nity from a test site of interest are required.

     (2) Guidance information. A preliminary study such as a shake-flask
test with site water and sediment (under paragraph (e)(l) of this guideline)
is  recommended to provide  preliminary information about the  fate of a
test compound. For example, a preliminary study may help identify those
fate processes such as volatilization that should receive close attention dur-
ing a microcosm study, and can provide guidance on sampling frequency
and dosing patterns. In addition, an activated sludge respiration inhibition
test (under paragraph (e)(10) of this guideline) is recommended to evaluate
potential adverse effects of a test substance on the natural microbial com-
munity  in the receiving environment.  This test measures respiration rate
under controlled conditions, and can help to obtain information on micro-
bial toxicity that may be important to microcosm design and set up.

     (3) Qualifying statements, (i)  This guideline establishes criteria of
minimum  acceptability for the development of sediment/water microcosms
for use in biodegradation studies. If the nature of a receiving environment
requires testing under strictly anaeraobic  conditions,  other test methods
may  be  more appropriate  (e.g.,  the   test   guideline   for  anaerobic
biodegradability referenced under paragraph (e)(17) of this guideline).

     (ii) This test guideline does not require any specific microcosm design
because design  and operation are compound and site specific.

     (iii) Performance of procedures discussed in this guideline may  in-
volve contact with hazardous materials  and  operation of potentially hazard-
ous equipment.  This guideline does not purport  to address all of the safety
concerns associated with its use. It is the responsibility of the user of this
guideline to establish appropriate safety and health practices and determine
the applicability of regulatory limitations prior to using this guideline.

     (4) Recommendations,  (i)  The use of 14C-labeled test substances is
recommended.

     (ii) The use of a mass-balance approach is recommended.

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     (c) Method — (1) Introduction, purpose, scope, relevance, applica-
tion, and limits of test — (i) Background. (A) The fate of chemicals re-
leased  to the environment may be evaluated in the  field or in laboratory
studies. Field studies can be used to obtain important  information about
the fate of chemicals in a particular ecosystem, but  have many disadvan-
tages. In field studies, environmental variables generally cannot be con-
trolled and the study may be subject to wide fluctuations in variables such
as temperature, rainfall, or  sunlight. It  is also  difficult in  many cases to
distinguish whether an observed effect  is a result of one fate process vs.
another, or a result of the interaction of more than one fate process. Micro-
cosms  may be used to replicate many of the processes affecting the fate
of a chemical in complex ecosystems.  These model systems provide an
opportunity to manipulate various test conditions and to observe the effects
of these alterations and their interactions on fate processes. Because micro-
cosms  are more easily replicated, effects  of environmental variability are
more easily studied than under field conditions. Finally, microcosms can
be used to examine the significance of various fate processes (e.g. hydroly-
sis  and biodegradation). This makes it possible to focus on critical proc-
esses and consider site-specific environmental situations.

     (B) This guideline provides guidance  on  the  development, use and
evaluation of microcosms  containing intact benthic sediment and overlying
water for laboratory evaluations of the fate  of chemical substances in the
aerobic aquatic environment.

     (C) Several  examples  of information on the fate  of  chemicals that
might be obtained from microcosm studies are:

     (7) The ability of a chemical substance to  persist in its original form
in a particular aquatic environment.

     (2) Relative importance of abiotic and biotic processes in determining
the fate of a chemical.
        The effect that partitioning  of a chemical  substance into benthic
sediment has on the ultimate fate of the compound.

     (ii) Definitions.  (A) Within this  guideline,  a  microcosm is  defined
as an intact, minimally  disturbed portion  of an ecosystem brought into
the laboratory for study under controlled experimental conditions.

     (B) Ultimate biodegradation is  any biologically mediated conversion
of an organic compound to inorganic compounds  (e.g.  CCh, H2o, etc.),
other products associated with normal  metabolic processes, and microbial
biomass.

     (C)  Primary biodegradation  is  any  biologically  mediated trans-
formation that  changes  the molecular structure  of the  parent chemical
compound.

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     (D) Within this guideline, a mass balance approach is one in which
the test substance's transport to or from and appearance in all applicable
media of the microcosm,  including sediment, overlying  water, interstitial
water, off-gases, and test equipment washings is determined, and formation
of 14C-labeled CCh is determined if radiolabeled parent compound is used.

     (iii) Reference substances. If required, methyl parathion or linear
alkylbenzene sulfonate  (LAS)  may be  used as an appropriate reference
standard with the shake flask and microcosm tests.

     (iv) Principle of the test method. Microcosms  are  laboratory test
systems designed to study fate processes such as biodegradation of chemi-
cal substances by  natural microbial communities.  Microcosms  contain
sediment and water that have been collected from test sites in a manner
that maintains the physical and biological integrity of the ecosystem under
study. Physical parameters such as lighting, mixing, and temperature may
be  controlled to simulate the environmental conditions  of the site from
which water and sediment samples are  collected. Test compounds are in-
troduced into the system either as a single dose or by continuous dosing
over the duration of testing.  The microcosms are sampled on a periodic
basis, and the water, sediment and off-gases (latter for volatile test com-
pounds)  are analyzed for disappearance of the parent compound (i.e. pri-
mary biodegradation) and, if feasible, appearance of metabolites. Measure-
ments of ultimate biodegradation may also be made.

     (v)  Quality criteria—(A) Reproducibility. Microcosms  containing
sediment and water samples  collected simultaneously from the same site
should provide for adequate reproducibility between replicate microcosms,
provided that standard testing conditions are strictly  observed.  Variability
may be greater when sediment and water samples are collected at different
test sites or at  the  same sites over different time intervals. The presence
of organisms other than microorganisms (e.g.,  amphipods)  in sediment/
water samples  may also cause  significant  changes to occur in the sedi-
ments, and therefore complicate test results.

     (B) Sensitivity. The sensitivity of the test is dependent upon the dos-
ing protocol, adequate control of specific testing conditions,  and the analyt-
ical methods used.

     (C) Specificity. This  method is  applicable to various classes of inor-
ganic and organic  compounds. The specific type of test compound used
should be considered in selecting an appropriate microcosm design, testing
protocol, and analytical technique.

     (D) Possibility of standardization. Standardization of all aspects of
microcosm testing is difficult,  but minimum criteria for acceptability  are
provided by this guideline. Specific microcosm designs and testing proto-
cols should be  selected based on the type of test compound used and  the
environmental conditions at the test site.

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     (E) Possibility of automation. Not foreseen.

     (2) Description of test procedure— (i) Physical/chemical site char-
acterization—(A)  Sediment/water.  To ensure that  aerobic, sediment/
water microcosms  adequately replicate the environmental  habitats  from
which they are  derived  and  to  identify important environmental factors
that could potentially affect the rate or extent of biodegradation of a chemi-
cal substance, physical/chemical characteristics of the site of collection
should be determined. These include:

     (7) Physical characteristics. Light intensity and photoperiod, tem-
perature, total suspended solids (TSS), etc.

     (2) Chemical  characteristics. Dissolved oxygen (DO), total organic
carbon (TOC), dissolved organic carbon (DOC), alkalinity, conductivity,
pH, redox gradient,  etc.

     (B)  Site contamination. Because certain contaminants  can adversely
affect the fate (e.g. rate or extent of biodegradation) of a chemical sub-
stance, it is recommended that  to the extent  possible collection sites be
screened for the presence, identity, and extent of contamination by the
test chemical or close chemical  analogs and the following chemical sub-
stances: Pesticides,  PCBs and other hazardous substances, heavy metals.

     (ii) Design  features—(A) Size. Microcosms vary in size from a frac-
tion of a liter to  several hundred  liters. A microcosm should be sufficiently
large  to permit  removal of water and sediment samples  without signifi-
cantly affecting surface area to volume ratios over the course of an experi-
ment, and to readily accommodate monitoring probes and mixing appara-
tus where necessary.  Alternatively,  smaller microcosms may be used in
sufficient numbers  to allow for destructive sampling. Small microcosms
(i.e. containing several hundred  milliliters  or less of site  water and sedi-
ment) may be the most appropriate for studies of chemical fate processes
such as biodegradation and sorption.

     (B)  Alternative methods  for establishing microcosms. (7) One
method of establishing a sediment/water microcosm is to use a sediment
coring device which becomes the microcosm vessel. A glass tube of suit-
able  size  (e.g.  approximately  3.5  cm  in diameter  and 40 cm in length)
is  inserted into the  sediment to a depth equal to or greater than the depth
of biological activity.  The top of the tube is closed with a silicone stopper.
The tube is removed  from the sediment and closed with  another silicone
stopper. After the cores  are transported back to the laboratory, additional
site water (i.e. collected separately) may be added to the microcosm as
necessary to  achieve  the desired sediment surface area to water volume
ratio.

     (2) Alternatively, an intact  core may be obtained in the field and ex-
truded into a microcosm vessel  in the laboratory. A simple and effective

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coring device can be made from clear, acrylic pipe.  The coring device
is inserted into the sediment to a depth equal to or greater than the depth
of biological activity. The coring device is closed with stoppers as noted
above and  the  core is returned to the laboratory. The bottom stopper  is
removed and the core is inserted into the microcosm vessel. The top stop-
per is removed and the coring device is lifted out of the microcosm leaving
the sediment core intact. For large water volume to sediment surface area
ratios, the coring device may be placed in a glass dish (e.g. a crystallization
dish) having a diameter slightly larger than the corer, and the entire assem-
bly (core, corer, and dish) placed into the microcosms.

    (C)  Diagrams of representative  microcosms. Figures  1, 2  and  3
present  a representative  selection of microcosm designs that  are appro-
priate for conducting sediment/water microcosm bio degradation tests.

    Figure 1. Ecocore Microcosm (under paragraph (e)(12) of this guide-
line)

    Figure 2.  Sediment/Water System (under paragraph  (e)(13) of this
guideline)

    Figure 3. Flow-Through Microcosm (under paragraph (e)(14) of this
guideline)

    (iii) Preparation—(A) Reagents—(7) Water. Water for the micro-
cosm  shall be collected from above or nearly above the site of sediment
core collection. Water  may be collected by hand bucketing, grab sample,
or pumping.  Water samples shall be  transported to the  test facility with
minimum delay. If water must be held in the laboratory overnight, it may
be kept  at room temperature  and  gently stirred.  Where necessary (e.g.
flow-through microcosm test), larger quantities of site  water may be held
for longer periods of time  at 4 °C. Prior to use in an aerobic, sediment/
water microcosm test, water should be brought to  the test temperature ±2
°C and gently stirred.

    (2) Sediment cores. Sediment cores shall be collected in such a man-
ner as to preserve to the extent possible the structural integrity of the sam-
ple, including the redox gradient and the benthic community.

    (B)  Materials—(7)  Sampling  containers.  In  order to minimize
leaching  of plasticizers and other contaminants into the water, sampling
containers shall be composed  of materials such as glass or fluorocarbon
plastics (e.g. Teflon®).

    (2)  Microcosm  construction materials.  Microcosms shall be  com-
posed of inert fluorocarbon plastics (e.g. Teflon®) and/or glass. If rubber
stoppers  are used, they shall be composed of silicone rubber.

    (iv) Procedure  for setting up and  maintaining microcosms—(A)
Control  microcosms—(7) Sterile control microcosms.  Use of  sterile

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control  microcosms permits determination of the relative importance of
biotic and abiotic processes in the fate of a test compound.

     (2) Other control microcosms. If necessary, solvent control micro-
cosms, glucose-amended controls, and controls containing other standard
reference compounds such as aniline  should also be used.

     (B) Dosing microcosms. (7) To the extent possible,  the method and
pattern of applying a test substance to a microcosm should reflect the re-
lease pattern expected in the natural environment.

     (2) Microcosms may be maintained in either flow-through or static-
renewal modes.  For the latter, a fixed percentage of microcosm water is
replaced with fresh site water at appropriate time intervals. A single (i.e.
pulse) dose of test compound may be applied in conjunction with either
of these modes. For a pulse dose in a flowing  system,  the relationship
between molecular turnover (partial  replacement) time and the flow rate
and  volume of the microcosm chamber has been described by Sprague
(under paragraph (e)(15) of this guideline)
        For flow-through systems  employing relatively large concentra-
tions of test compounds, a pump or headbox/siphon arrangement is rec-
ommended. All parts of the pump and delivery tubing that come into con-
tact with either the test compound  or diluent water should be composed
of inert materials to minimize sorption of the test substance.

    (4) The test substance may be dissolved in a carrier and the resulting
stock  solution metered into flowing diluent water. Ideally, the carrier
should be dissolved in sterile diluent water. Peristaltic pumps using sili-
cone rubber tubing may be  used for adding diluent water. However,  it
is not recommended that these be used to deliver stock solutions because
sorption of test  compound to  the tubing may be  significant. A syringe
pump with glass syringes and inert plastic (fluorocarbon) plungers and tub-
ing is  more desirable  for introducing a test compound and carrier into
flowing diluent water.

    (5) If the test compound is insoluble in water, but  soluble  in  a
nontoxic, water-miscible solvent,  it should be dissolved in the minimum
volume of carrier or solvent required to form a  homogeneous stock solu-
tion of known concentration. Carriers other than water that are acceptable
in aquatic toxicity testing may be used, including acetone, ethanol, meth-
anol,   diethyl   sulfoxide,    ethylene   glycol   monomethyl   ether,
dimethylformamide, and triethylene glycol (under paragraph (e)(2) of this
guideline).  Care should be  taken that an increased organic carbon load
due to the addition of a carrier does not significantly affect the test results.
In addition, if a carrier or solvent is used, a control microcosm should
be established to assess the effect of the  solvent  on microbial activity.

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     (6} If the  test compound  is added continuously, the stock solution
and delivery lines should be kept free of microbial contamination to avoid
degradation of the test compound before it reaches the microcosm.

     (C)  Test compound concentration. The  test compound concentra-
tion^) shall approximate the expected ambient environmental concentra-
tion. Solubility in  water of the test compound, analytical detection limit,
and toxic effects on microbiota in the microcosm should be considered
in the selection of the test compound concentration. A preliminary shake-
flask study (under paragraph (e)(l) of this guideline) and/or a  microbial
respiration inhibition test (under paragraph (e)(10) of this guideline) may
aid in identifying an appropriate concentration.

     (D) Temperature. It is recommended that  microcosms be maintained
at field temperature ±2  °C. However, specific circumstances may suggest
that another temperature may be more appropriate. The microcosms should
be placed in a water bath to maintain a constant temperature.

     (E) Lighting. (7) It may be desirable to control the quantity  and qual-
ity of light entering the microcosms. Light intensity  may be  adjusted to
a level that is  equivalent to the average light  intensity  on the  sediment
surface in the natural system from which the core was obtained. The pre-
ferred source of artificial light is a xenon lamp since its spectrum is closest
to that of sunlight.

     (2) Photoperiod may  be  controlled by the  use of simple timers.
Photoperiod is  usually  fixed at some arbitrary ratio  (e.g. 12 h of light
and 12 h of dark), or is maintained at ambient field conditions.

     (F) Mixing. Mixing of the microcosm water shall be adequate to uni-
formly distribute the test chemical  in the water column  but not so great
as to resuspended sediment. Mixing can be accomplished with pumps, aer-
ation, or stirrers. Use of glass or fluorocarbon plastic (e.g. Teflon®) stirrers
attached to small motors is recommended.  Simple aeration of microcosm
water is  often  unsatisfactory because it may cause significant  losses of
volatile test substance and may result in uneven mixing.

     (v) Microcosm replication techniques. A detailed discussion of tech-
niques for determining adequate microcosm replication and  appropriate
statistical  treatment of the  relevant test data is beyond the scope of this
guideline. However, treatment microcosms must be established in triplicate
for each identified dose (e.g.  1 ppm, 10 ppm, 1,000 ppm), and control
microcosms in duplicate for each identified type of control (e.g.  sterile
control, solvent control, glucose-amended control), to be minimally accept-
able for this test guideline.

     (vi)  Microcosm sampling techniques—(A) Monitoring  physical/
chemical  characteristics. To ensure the functional capability of the sedi-
ment/water microcosms and to maintain environmental conditions that ade-

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quately represent those of the receiving environment, it is recommended
that to the extent that they are applicable, certain physical/chemical charac-
teristics (listed in paragraph (c)(2)(i)(A) of this guideline) be monitored
over the course of the test.

     (B) Water samples. (7) Two replicate water samples shall be col-
lected from each microcosm at  dosing time  (after an appropriate mixing
period) and periodically thereafter. Sampling regimes for both static and
flow-through systems should be designed  according  to the expected dis-
appearance rate of the parent compound.

     (2) To characterize sorption and/or volatilization  of the chemical sub-
stance during the start-up and initial phase of the microcosm test, it may
be appropriate to collect water samples at  frequent intervals initially (e.g.
at 0,  1, 3, 6,  12,  and 24 h) and  at less frequent intervals (e.g. 1, 4,  7,
14, 24, 36 days) thereafter.

     (3) The duration of microcosm testing should be limited to 60  days
or less, unless specific  circumstances and microcosm  function warrant
longer operation. During this time,  the microcosm should be monitored
to ensure its viability and stability (under paragraph (e)(ll) of this guide-
line).

     (4) A preliminary study such as a shake-flask test  (under paragraph
(e)(l) of this guideline), using site water and sediment, is recommended
to help identify a sampling protocol that  is  appropriate for  the specific
site and test parameters.

     (C) Sediment samples. Sediment samples shall be collected periodi-
cally during the test. To determine the importance of partitioning to sedi-
ment, it is recommended that sediment samples be  collected initially  at
frequent intervals  (e.g. 0, 12 h), and at less frequent intervals (e.g.  1,  4,
7, 14, 24,  36 days) thereafter.  Sediment samples shall be collected in trip-
licate from each treatment microcosm, and in duplicate from each control
microcosm,  for each time interval and test concentration. If the diameter
of the sediment core is  sufficiently large  for repeated sampling without
disturbing the sediment/water interface, this  may be accomplished at a
minimum  by collecting one sample  from each of the triplicate  treatment
microcosms for each concentration of test substance. However, it should
be noted that such a sampling design may not be statistically optimal, since
the extent of sample  variability  for  each treatment microcosm  is not
known. If the  nature of the sediment or the  diameter of the core is  such
that  disturbance of the sediment is  a  likely  consequence of  sampling, it
is recommended that the study design include three times as many treat-
ment microcosms  as there are sampling times, such that treatment micro-
cosms are destructively sampled in triplicate.

     (D) Additional sampling. All of the test substance added to the mi-
crocosm during the study should be accounted for by mass balance. The

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use of radiolabeled test compound  is therefore recommended. Potential
losses of test substance and transformation products to the atmosphere may
be evaluated by trapping and sampling off-gases using sampling techniques
described by Bourquin et  al.  (under paragraph (e)(3) of this guideline),
and in the U.S. Environmental Protection Agency Test Guideline for a
site-specific microcosm test (under  paragraph  (e)(16) of this guideline).
The significance of volatilization and sorption can also be evaluated based
on preliminary tests  and sterile controls, and should  be accounted for in
the design of the microcosm.

    (vii) Analytical methods. Detailed discussion of compound-specific
analytical methods is beyond the scope of  this guideline.  Gas chroma-
tography (GC) and high performance liquid  chromatography (HPLC) are
suitable for the quantification of many  test compounds. Use of appro-
priately radiolabeled  test  substances is  recommended, especially when
quantifying  mineralization  or  identifying  degradation products that need
further characterization by conventional analysis.

    (d) Data  and reporting.  (7) A  mass balance shall be determined for
the test substance describing  its fate, including its  transport to or from
and appearance in all applicable media of the  microcosm. Where appro-
priate,  the media should include at  a minimum the following: sediment,
overlying water,  sediment core washings, resin traps for volatile com-
pounds, KOH  or other standard solvent used as  a trap for 14C-labeled CCh
from parent compound, and test equipment  washings. Analysis of these
components should account for >80 percent of the initial added concentra-
tion of 14C-labeled substrate or parent compound (under paragraph (e)(4),
(5), (6), (7), (8), (9), (12), and (13) of this guideline). A spreadsheet format
may be useful  for reporting data.

    (2) The rate constant for the loss of the test compound from the water
column can be determined, assuming first-order kinetics, from a  plot of
In C vs. t:

    In C = kit + a

where  C is the test compound concentration,  a is the Y-axis intercept,
and t is time.  The rate constant is ki, which is determined as the best-
fit slope of a  liner regression of In  C vs. t. The half-life (ti/2) can then
be determined by use of the following equation:

                  ti/2 = 0.693/ki

    (3) Reports should account for any unusual observations  as well as
include where  applicable the following information:

    (/) Date the study began and ended.

    (//) Name and address  of testing laboratory.

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     (///) Principal investigator(s).

     (/v) Staff members actually conducting the test.

     (v) Full description of the experimental design and procedures, includ-
ing a description of the test equipment.

     (v/) Identity of the test substance, percentage of active ingredient, mo-
lecular structure, and radiolabel placement.

     (v//) Manufacture and lot number of the test substance.

     (v///) Physical and chemical properties of the site.

     (ix) Results of all plate counts.

     (jc) Principal mathematic equations.

     (xi) Residue data or contamination profile of sediment and water.

     (xii) Results of trapped volatiles and CCh analyses.

     (xiif) Residue decline curves (i.e. loss of parent compound).

     (jc/v) Metabolite characteristics as determined by TLC, HPLC or other
analytical technique  suitable for  identifying  metabolites; identity of each
metabolite with >10 percent yield.

     (xv) Incubation temperature;  photoperiod and lighting conditions.

     (xvi) Materials balance, rate constants, half-lives.

     (xvii) Concentration of dissolved 14C-labeled CCh in water.

     (xviii) Dates and results of QA/QC audits.

     (xix) Location of raw data.

     (xx) Complete description of any deviation from the established test
guideline.

     (xxi) Experimental test system monitoring data  including TOC,  pH,
lighting, temperature, etc.

     (e)  References. (1)  American  Society for Testing and  Materials
(ASTM), ASTM Method E1279-89: Standard test method for biodegrada-
tion by a shake-flask die-away method. Philadelphia, PA (1989).

     (2)  American Society for Testing and Materials  (ASTM), ASTM
Method E729-88a: Standard guide for conducting acute toxicity tests with
fishes, macroinvertebrates, and amphibians. Philadelphia, PA (1989).

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    (3) Bourquin A.W. et al., An artificial microbial ecosystem for deter-
mining effects and fate of toxicants in a salt-marsh environment. Devel-
opmental Industrial Microbiology 10: 185-191 (1977).

    (4) Clark J.M. and Matsumura F., Metabolism of toxaphene by aquat-
ic sediment and a camphor-degrading pseudomonad. Archives of Environ-
mental Contamination and Toxicology 8: 285-298 (1979).

    (5) Giddings J.M. et al.,  Transport and fate of anthracene in aquatic
microcosms. In: Microbial Degradation of Pollutants in Marine Sediments
(Bourquin A.W. and Pritchard P.H., eds.). Gulf Breeze,  FL: U.S. EPA
Office of Research and Development, Environmental Research Laboratory,
pp. 312-320. EPA-600-979-012 (1979).

    (6) Heitkamp M.A.  and Cerniglia  C.E., Effects of chemical structure
and exposure on the microbial degradation of polycyclic aromatic hydro-
carbons in freshwater and  estuarine ecosystems.  Environmental and Toxi-
cological Chemistry 6: 535-546 (1987).

    (7) Heitkamp M.A. et al., Fate and metabolism of isopropylphenyl
diphenyl phosphate in fresh water. Environmental Sciience and Technology
18: 434-439 (1984).

    (8) Jensen K. et al., The use of ecocores to evaluate biodegradation
in marine sediments. Water Air Soil Pollution 39: 89-99 (1988).

    (9) O'Neill E.J.  et al., Effects of  lugworms and seagrass on kepone
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