United States       Prevention, Pesticides     EPA712-C-98-210
           Environmental Protection    and Toxic Substances     August 1998
           Agency         (7101)
&EPA    Health Effects Test
           Guidelines
           OPPTS 870.4100
           Chronic Toxicity

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                           INTRODUCTION
    This guideline is one  of a  series  of test  guidelines that have been
developed by the Office of Prevention, Pesticides and Toxic Substances,
United States Environmental  Protection Agency for use  in the testing of
pesticides and toxic substances, and the  development of test data that must
be submitted to the Agency  for review under Federal regulations.

    The Office of Prevention, Pesticides and Toxic Substances (OPPTS)
has developed this guideline through  a process of harmonization that
blended the testing  guidance  and requirements that  existed in the Office
of Pollution Prevention and Toxics (OPPT) and appeared in title 40, chap-
ter I, subchapter R of the Code  of Federal Regulations (CFR), the Office
of Pesticide Programs (OPP) which appeared in publications of  the Na-
tional Technical Information Service (NTIS)  and the guidelines published
by the Organization for Economic Cooperation and Development (OECD).

    The purpose of harmonizing these  guidelines  into  a single set of
OPPTS  guidelines is to minimize variations among the testing procedures
that must be performed to meet the data  requirements of the U. S. Environ-
mental Protection Agency  under the Toxic  Substances  Control Act  (15
U.S.C. 2601) and the Federal Insecticide, Fungicide and Rodenticide Act
(7U.S.C. I36,etseq.).

    Final  Guideline Release: This guideline is available from the U.S.
Government Printing Office,  Washington, DC 20402 on disks or paper
copies: call (202) 512-0132. This guideline is also available electronically
in PDF (portable document format) from EPA's World  Wide Web  site
(http://www.epa.gov/epahome/research.htm) under the heading "Research-
ers and Scientists/Test Methods and Guidelines/OPPTS  Harmonized Test
Guidelines."

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OPPTS 870.4100 Chronic toxicity.
     (a) Scope—(1) Applicability. This guideline is intended to meet test-
ing  requirements   of both  the  Federal  Insecticide,  Fungicide,  and
Rodenticide Act (FIFRA) (7 U.S.C. 136, et seq.) and the Toxic Substances
Control Act (TSCA) (15 U.S.C. 2601).

     (2) Background. The source material  used in developing this har-
monized OPPTS test guideline are 40 CFR 798.3260 Chronic  Toxicity;
OPP 83-1  Chronic Feeding—Two Species,  Rodent and Nonrodent (Pes-
ticide Assessment Guidelines, Subdivision F—Hazard Evaluation; Human
and Domestic Animals) EPA report 540/09-82-025, 1982; and OECD 452
Chronic Toxicity studies.

     (b) Purpose. The objective of a chronic toxicity study is to determine
the effects of a substance in a mammalian species following prolonged
and repeated exposure. A chronic toxicity study should generate data from
which to identify the majority of chronic  effects and to define long-term
dose-response  relationships. The  design and conduct of chronic toxicity
tests should allow for the detection of general toxic effects, including neu-
rological, physiological, biochemical, and hematological effects and expo-
sure-related morphological (pathological) effects.

     (c) Definitions. The definitions in section 3 of TSCA and in 40  CFR
Part 792—Good Laboratory Practice  Standards  (GLP)  apply  to this test
guideline. The following definitions also apply to this test guideline.

     Chronic toxicity is the adverse effects occurring as a  result of the
repeated daily exposure of experimental animals to a chemical by the oral,
dermal, or inhalation routes of exposure.

     Cumulative toxicity is the adverse  effects of repeated doses occurring
as a result of prolonged action on, or increased concentration of, the ad-
ministered test substance or its metabolites  in susceptible tissue.

     Dose in a chronic toxicity study is the  amount of test substance ad-
ministered daily via the oral, dermal or inhalation routes for a period of
at least 12  months. Dose  is expressed as weight  of the test substance
(grams, milligrams) per unit body weight  (BW) of test animal (milligram
per kilogram), or as weight of the test substance in parts per million (ppm)
in food or drinking water per day. For inhalation  exposure, dose is ex-
pressed as weight of the test substance per unit volume of air (milligrams
per liter) or as parts per  million per  day. For dermal exposure, dose is
expressed as weight of the test substance (grams, milligrams) per unit body
weight of the  test animal (milligrams  per kilogram) or as weight of the
substance per unit of surface area (milligrams per square centimeter) per
day.

     No-observed-effect-level  (NOEL)  is  the maximum dose used  in  a
study which produces no adverse effects. The NOEL is usually expressed

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in terms of the  weight of a test substance given daily per unit weight
of test animal (milligrams per kilogram per day).

     Target organ is any organ of a test animal showing evidence of an
effect induced by a test substance.

     (d) Limit test. If a test at one dose level of at least 1,000 mg/kg
BW (expected human exposure may indicate the need for a higher dose
level), using the  procedures described for this study, produces no observ-
able toxic effects and if toxicity would not be expected based upon data
of structurally related  compounds,  a full study using three dose  levels
might not be necessary.

     (e) Test procedures—(1) Animal selection—(i) Species and strain.
Testing  should be performed with two mammalian species, one a rodent
and the  other a nonrodent. The rat is the preferred rodent species and the
dog is the preferred nonrodent species. Commonly used laboratory strains
should be employed.  If other mammalian  species are used,  the tester
should provide justification/reasoning for their selection.

     (ii) Age/weight. (A) Testing should  be started with  young healthy
animals as soon as possible after weaning and acclimatization.

     (B) Dosing  of rodents should generally begin no later than 8 weeks
of age.

     (C)  Dosing  of dogs should  begin between 4 and 6 months of age
and in no case later than 9 months of age.

     (D) At commencement  of the study, the weight variation of animals
used should be within 20 percent of the mean weight for each sex.

     (E) Studies  using prenatal or neonatal animals may be recommended
under special conditions.

     (iii) Sex. (A) Equal numbers of animals of each sex should be used
at each dose level.

     (B) Females should be nulliparous and nonpregnant.

     (iv) Numbers. (A) For rodents, at least 40 animals (20 males and
20 females)  and for nonrodents (dogs) at least  8 animals (4 females and
4 males) should  be used at each dose level and concurrent control group.

     (B) If interim sacrifices are planned, the number should be increased
by the number of animals scheduled to be sacrificed during the course
of the study.

     (C) The number of animals  at the termination of the study must be
adequate for  a meaningful and valid statistical evaluation of chronic  ef-

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fects. The Agency must be notified if excessive early deaths or other prob-
lems  are encountered that might compromise the integrity of the  study.

     (D) To avoid bias, the use of adequate randomization procedures for
the proper allocation of animals to test and  control groups is required.

     (E) Each animal should be assigned a unique identification number.
Dead animals, their preserved organs and tissues, and microscopic slides
should be identified by reference to the unique numbers assigned.

     (v)  Husbandry. (A) Rodents  may be group-caged by  sex, but  the
number of animals  per cage  must not interfere with clear observation of
each animal. The biological properties of the test substance or toxic effects
(e.g., morbidity,  excitability) may indicate  a need for individual caging.
Rodents should be housed individually in dermal  studies and during expo-
sure in inhalation studies. Caging should be appropriate to the nonrodent
species.  However, it is recommended that dogs  are housed  individually.

     (B) The temperature of  the experimental animal rooms  should be at
22 + 3 °C.

     (C) The relative humidity of the experimental animal rooms should
be 50 + 20 percent.

     (D) Where lighting is artificial, the  sequence  should be 12 hours light/
12 hours dark.

     (E) Control and test animals should be fed from the  same batch and
lot. The feed should be analyzed to  assure adequacy of nutritional require-
ments of the species tested  and for impurities that might influence  the
outcome of the test. Animals should be fed and  watered ad  libitum with
food replaced at least weekly.

     (F) The study should not be initiated until animals have been allowed
a period of acclimatization/quarantine  to  environmental  conditions, nor
should animals  from outside sources be  placed on test without an adequate
period of quarantine. An acclimation period of at least 5  days is  rec-
ommended.

     (2)  Control and test substances,  (i) Where necessary, the test sub-
stance is dissolved or suspended in  a suitable vehicle. If a vehicle or dilu-
ent is needed it should not elicit toxic effects  itself nor substantially alter
the chemical or toxicological properties of the test substance.  It is  rec-
ommended that wherever possible the use of an aqueous solution be  the
first choice, followed by consideration of solution in oil, and finally, solu-
tion in other vehicles.

     (ii) One  lot of the test substance should be used, if possible, through-
out the duration  of the study, and  the  research sample should be  stored
under conditions that maintain its purity and stability. Prior to the initiation

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of the study, there should be a characterization of the test substance, in-
cluding the purity of the test compound,  and,  if technically feasible, the
names and quantities of contaminants and impurities.

     (iii) If the  test or control  substance  is to be incorporated into  feed
or another vehicle, the period  during which the test substance is stable
in such a mixture should be determined prior to the initiation of the study.
Its homogeneity and concentration should be determined prior to the initi-
ation of the study and periodically during the  study.  Statistically random-
ized samples of the mixture should be analyzed to ensure that proper mix-
ing,  formulation, and storage procedures are being followed, and that the
appropriate concentration of the test or control  substance is  contained in
the mixture.

     (3)  Control groups. A concurrent control group is required.  This
group should be an untreated or sham-treated control  group or, if a vehicle
is used in administering the test substance, a vehicle control  group. If the
toxic properties  of the vehicle are not known or cannot be made available,
both untreated and vehicle control groups are required.

     (4) Satellite group.  A satellite group of 40 animals  (20 animals per
sex) for rodents and 8 animals  (4 animals per sex) for nonrodents  may
be treated with the high-dose level for 12 months and observed for revers-
ibility, persistence, or  delayed occurrence of toxic effects  for a post-treat-
ment of appropriate length, normally not less than 28  days. In addition,
a control group  of 40  animals (20 animals per sex) for rodents and 8 ani-
mals  (4 animals per sex) for nonrodents should be added to the satellite
study.

     (5) Dose levels and dose  selections, (i)  In chronic  toxicity tests, it
is desirable to determine a dose-response relationship as well as a NOEL.
Therefore,  at least three dose levels with a control group and, where appro-
priate, a vehicle control (corresponding to the concentration of the vehicle
at the highest exposure level) should be used. Dose levels should be spaced
to produce  a gradation of effects. A rationale must be provided for the
doses selected.

     (ii) The highest-dose level  should elicit signs of toxicity without sub-
stantially altering  the  normal life span  of the animal.  The  highest  dose
should be determined based on the findings from a 90-day study to ensure
that  the  dose used is  adequate  to assess  the chronic toxicity  of the test
substance.  Thus, the selection of the highest dose to be tested is dependent
upon changes observed in several toxicological parameters in  subchronic
studies. The highest dose tested need not exceed 1,000 mg/kg/day. If der-
mal  application  of the test substance produces  severe skin irritation,  then
it may be necessary either to terminate the study and  choose a lower high-
dose  level  or to reduce the dose level.  Gross  criteria for defining severe
irritation would  include ulcers, fissures,  exudate/crust(eschar), dead tissue,

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or anything leading to destruction of the functional integrity of the epider-
mis (e.g.  caking, open sores, fissuring, eschar). Histological criteria for
defining severe irritation would include follicular and interfollicular crust,
microulcer, mild/moderate  degeneration/necrosis,  moderate/marked epi-
dermal edema, marked dermal edema, and marked inflammation.

    (iii) The intermediate dose levels should be spaced to produce a gra-
dation of toxic effects.

    (iv) The lowest-dose level should produce no evidence of toxicity.

    (6) Administration of the test substance. The three main routes of
administration are oral, dermal,  and inhalation. The  choice  of the route
of administration depends upon the physical  and  chemical characteristics
of the test substance and the form typifying exposure in humans.

    (i)  Oral studies. Ideally, the animals should be  dosed by gavage or
with capsules on a 7-day per week basis for a  period of at least 12 months.
However, based primarily on practical considerations, dosing by gavage
or capsules on a 5-day per week schedule is acceptable. If the test sub-
stance is administered via in the drinking water or  mixed in the diet, expo-
sure should be on a 7-day per week basis.

    (ii) Dermal  studies. (A) Preparation of animal skin. Shortly before
testing,  fur should be clipped from not less than  10 percent of the body
surface area for application of the test substance. In order to dose approxi-
mately  10 percent of the body surface, the area  starting at the  scapulae
(shoulders) to the wing of the ileum (hipbone) and  half way down the
flank  on each side of the animal should be shaved. Shaving  should  be
carried  out approximately 24 hours before dosing. Repeated clipping or
shaving is usually needed at approximately weekly intervals. When clip-
ping or shaving the fur, care  should be taken to avoid  abrading the skin
which could alter its permeability.

    (B) Preparation of test substance. Liquid  test substances are generally
used undiluted, except as indicated in paragraph (e)(5)(ii) of this guideline.
Solids should be pulverized when possible. The substance should be moist-
ened  sufficiently  with water or,  when necessary,  with a suitable vehicle
to ensure good contact with  the skin. When a vehicle is used, the influence
of the vehicle on toxicity of, and penetration  of the skin by, the test sub-
stance should be  taken into account.The volume of application should be
kept constant, e.g. less than 100 (j,L for the mouse and less than 300 (iL
for the  rat. Different concentrations of test solution  should  be prepared
for different dose levels.

    (C) Administration of test substance. The duration of exposure should
be at  least for 12 months. Ideally, the animals should be treated with test
substance for at least  6 h/day  on a 7-day per  week basis. However, based
on practical considerations,  application on a  5-day per week basis is ac-

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ceptable. Dosing should be conducted at approximately the same time each
day. The test  substance should be  applied uniformly over the treatment
site. The surface area covered may be less for highly toxic substances.
As  much of the area  should be covered with as thin and uniform a film
as possible. For rats,  the test  substance may be held in contact with the
skin with a porous gauze dressing and nonirritating tape if necessary. The
test site should be further covered in a suitable manner to retain the gauze
dressing plus test substance and to  ensure that the animals cannot ingest
the test substance. The application  site should not be  covered when the
mouse is the species  of choice. The test substance  may be wiped from
the skin after the six-hour exposure period to prevent ingestion.

     (iii) Inhalation studies. (A) The animals should be exposed to  the
test substance  for 6 h/day on  a 7-day per week basis,  for a period of at
least 12 months. However, based primarily on practical considerations, ex-
posure for 6 hours per day on a 5-day per week basis is acceptable.

     (B) The animals should be tested in dynamic inhalation equipment
designed to sustain a minimum air flow of 10 air changes  per hour, an
adequate oxygen content of at least 19 percent,  and uniform conditions
throughout the exposure chamber. Maintenance of slight negative pressure
inside the chamber will prevent leakage of the test substance into surround-
ing areas. It is not normally necessary to measure chamber oxygen con-
centration if airflow is adequate.

     (C) The selection of a dynamic inhalation chamber should be appro-
priate for the test substance and test system. When a whole body chamber
is used, individual housing must be used to  minimize  crowding of the
test animals and maximize their exposure to the test substance. To ensure
stability of a chamber atmosphere, the total volume  occupied by the test
animals should not exceed 5 percent of the volume  of the test chamber.
It is recommended, but not required, that nose-only or head-only exposure
be used for aerosol studies in order to minimize oral  exposures due to
animals licking compound off their fur. The animals should be acclimated
and heat stress minimized.

     (D) The temperature at which the test is performed should be main-
tained  Sit 22 ±2 °C. The relative humidity should be maintained between
40-60  percent, but in certain instances (e.g.,  use of water  vehicle) this
may not be practicable.

     (E) The rate of  air flow should be monitored continuously but re-
corded at least three times during the exposure.

     (F) Temperature  and humidity  should be monitored continuously but
should be recorded at least every 30 min.

     (G) The actual concentrations of the test  substance should be meas-
ured in the breathing zone. During the exposure period, the actual con-

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centrations of the test substance should be held as constant as practicable,
monitored continuously or intermittently depending on the method of anal-
ysis. Chamber concentration may be measured using gravimetric or analyt-
ical methods, as appropriate. If trial run measurements are reasonably con-
sistent (±10 percent for liquid aerosol, gas,  or  vapor; + 20 percent  for
dry aerosol), then two measurements should be sufficient. If measurements
are not consistent, three to  four measurements should be taken. Whenever
the test substance is a formulation, or it is  necessary  to formulate the test
substance with a vehicle for aerosol generation,  the analytical concentra-
tion must be reported for the total formulation, and not just for the active
ingredient (AI).  If, for example, a  formulation contains 10 percent AI and
90  percent inerts,  a  chamber  of analytical  limit  concentration   of
2 mg/L would consist of 0.2 mg/L of the AI. It is not  necessary to analyze
inert ingredients provided  the  mixture at the animal's  breathing zone is
analogous to the formulation; the grounds for this conclusion must be pro-
vided in the study report.  If there is some difficulty measuring chamber
analytical concentration  due  to precipitation,  nonhomogeneous mixtures,
volatile components, or other factors, additional  analysis  of inert compo-
nents may be necessary.

     (H) During the development  of the generating system, particle size
analysis should be performed to establish the stability of aerosol concentra-
tions with respect to particle size. The mass median aerodynamic diameter
(MMAD) particle size range should be between 1-3 (im. The particle size
of hygroscopic materials should be small enough when dry to  assure that
the size of the swollen particle will still be within  the 1-3 (im range. Meas-
urements  of  aerodynamic  particle size  in the   animal's  breathing zone
should be measured during a trial run. If MMAD  values for each exposure
level are within 10 percent of each other, then two measurements  during
the exposures  should be  sufficient. If pretest measurements are not  within
10  percent of each  other,  three to four measurements should be  taken.

     (I) Feed should be withheld during exposure.  Water may also be with-
held during exposure.

     (7) Observation period,  (i) Animals should  be observed for a  period
of at least 12 months.

     (ii) Animals in a satellite group (if used)  scheduled for follow-up ob-
servations should be kept  for  at least 28 days further  without treatment
to detect recovery from, or persistence of, toxic effects.

     (8) Observation of animals, (i) Observations should  be  made at least
twice each day for morbidity  and mortality.  Appropriate actions  should
be taken to minimize loss of animals to the study (e.g., necropsy or  refrig-
eration of those animals found dead and  isolation or  sacrifice of weak
or moribund animals).  General clinical  observations should be made  at
least once a day, preferably at the  same time each day, taking into consid-

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eration  the peak period of anticipated effects  after dosing.  The  clinical
condition of the animal should be recorded.

     (ii) A careful clinical examination should be made at least once prior
to the initiation of treatment (to allow for within subject comparisons) and
once weekly during treatment in all animals. These observations should
be made outside the home cage, preferably in a  standard arena, and at
similar  times on each occasion. Effort should be made to ensure that vari-
ations in the observation conditions are minimal. Observations should be
detailed and carefully recorded, preferably using scoring systems, explic-
itly defined by the testing laboratory.  Signs  noted  should include,  but not
be limited  to, changes in skin, fur, eyes, mucous membranes, occurrence
of secretions  and excretions  and autonomic activity (e.g.,  lacrimation,
piloerection, pupil size, unusual respiratory pattern). Changes in gait, pos-
ture  and response to handling as well as the presence of clonic or tonic
movements, stereotypies (e.g., excessive grooming, repetitive circling)  or
bizarre  behavior (e.g., self-mutilation, walking  backwards) should be  re-
corded.

     (iii) Once, near the end of the first year of the exposure period and
in any  case not earlier than in month 11, assessment of motor activity,
grip  strength, and sensory reactivity to stimuli of different types (e.g., vis-
ual, auditory, and proprioceptive stimuli) should be conducted in rodents.
Further  details  of the procedures  that could be followed are  described in
the references listed under paragraphs (h)(2), (h)(6), (h)(8), (h)(9), (h)(10),
and (h)(17) of this guideline.

     (iv) Functional  observations  conducted  towards the end  of the study
may be omitted when data on functional observations are available from
other studies and the daily clinical observations did not reveal any func-
tional deficits.

     (v) Exceptionally, functional observations may be omitted for groups
that otherwise reveal signs of toxicity to an extent that would significantly
interfere with functional test performance.

     (vi) Body  weights  should be recorded individually  for all animals
once prior  to the administration of the test substance, once a  week during
the first 13 weeks of study  and  at least once  every 4 weeks thereafter,
unless signs of clinical toxicity suggest more frequent weighing to facili-
tate monitoring of health status.

     (vii) Measurements of feed consumption should be determined weekly
during the first 13 weeks  of the study and at approximately monthly inter-
vals  thereafter  unless health  status or body  weight changes dictate other-
wise. Measurements of water consumption  should be determined at  the
same intervals  if the test substance is administered in the drinking water.

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     (viii) Moribund animals should be removed and sacrificed when no-
ticed and the time of death should be recorded as precisely as possible.
All survivors should be sacrificed at the end of the study period.

     (9) Clinical pathology. Hematology, clinical chemistry, and urinal-
ysis should be  performed on 10 rats per sex per group, and on all non-
rodents. In rodents, the parameters should be examined at approximately
6 month intervals during the conduct of the study and at termination. If
possible, these  collections should be from the same animals at each inter-
val. In nonrodents, the parameters should be examined once  or twice prior
to initiation of treatment,  at 6-month intervals  during the conduct of the
study,  and at termination. If hematological  and biochemical effects  were
seen in the subchronic study, testing should also be performed at 3 months.
Overnight fasting of animals prior to blood sampling is recommended.

     (i) Hematology. The recommended parameters  are red blood cell
count,  hemoglobin concentration,  hematocrit,  mean corpuscular volume,
mean  corpuscular hemoglobin,  and mean  corpuscular hemoglobin con-
centration, white blood cell  count,  differential leukocyte  count, platelet
count,  and a measure of clotting potential,  such as prothrombin time or
activated partial thromboplastin time.

     (ii) Clinical chemistry. (A) Parameters which are considered appro-
priate to all studies are  electrolyte  balance, carbohydrate metabolism, and
liver and kidney function. The selection of specific tests will be influenced
by observations on the mode of action of the substance and  signs of clini-
cal toxicity.

     (B) The recommended clinical chemistry determinations are potas-
sium,  sodium,  calcium (nonrodent),  phosphorus  (nonrodent),  chloride
(nonrodent), glucose, total cholesterol, urea nitrogen,  creatinine,  total pro-
tein, total bilirubin (nonrodent),  and albumin. More than two hepatic en-
zymes, (such as alanine  aminotransferase, aspartate aminotransferase, alka-
line    phosphatase,   sorbitol   dehydrogenase,   or   gamma   glutamyl
transpeptidase)  should  also be measured. Measurements of addtional en-
zymes  (of hepatic or other origin) and bile acids, may also be useful.

     (C) If a test chemical has an effect  on the hematopoietic system,
reticulocyte counts and bone marrow cytology may be indicated.

     (D) Other  determinations that should be carried out if the test chemi-
cal is known or suspected  of affecting related  measures include  calcium,
phosphorus,  fasting   triglycerides,  hormones,   methemoglobin,   and
cholinesterases.

     (iii) Urinalysis. Urinalysis  for rodents should be performed at the
end  of the study using  timed urine collection.  Urinalysis for nonrodents
should be  performed prior to treatment, midway through treatment and
at the end of the study using timed urine collection. Urinalysis determina-

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tions include: appearance, volume, osmolality or specific gravity, pH, pro-
tein, glucose, and blood/blood cells.

     (10) Ophthalmological examination. Examinations should be made
of all animals using an ophthalmoscope or equivalent device prior to the
administration of the test  substance  and at termination  of the  study  on
10 rats  of each sex in the high-dose and control groups and preferably
in all nonrodents, but at least the control and high-dose  groups  should
be examined. If changes in eyes are detected, all animals  should be exam-
ined.

     (11) Gross necropsy, (i) All  animals should be subjected to  a full
gross necropsy which includes examination of the external surface of the
body, all orifices, and the cranial, thoracic and abdominal cavities and their
contents.

     (ii) At least the liver, kidneys,  adrenals, testes, epididymides, ovaries,
uterus,  nonrodent thyroid  (with parathyroid),  spleen,  brain, and heart
should be weighed wet as soon as possible after dissection to avoid drying.
The lungs  should be weighed if the test substance is administered by the
inhalation route.

     (iii) The following organs and tissues, or representative samples there-
of,  should be  preserved  in a suitable  medium  for  possible  future
histopathological examination:

     (A) Digestive  system—salivary  glands, esophagus,  stomach, duode-
num,  jejunum,  ileum,  cecum, colon, rectum, liver, pancreas, gallbladder
(when present) .

     (B) Nervous  system—brain (multiple  sections, including  cerebrum,
cerebellum and medulla/pons), pituitary, peripheral nerve  (sciatic or tibial,
preferably in close proximity to the muscle), spinal cord (three levels, cer-
vical, mid-thoracic and lumbar), eyes (retina, optic  nerve).

     (C) Glandular system—adrenals, parathyroid,  thyroid.

     (D) Respiratory system—trachea, lungs, pharynx, larynx, nose.

     (E) Cardiovascular/hematopoietic system—aorta, heart, bone marrow
(and/or fresh aspirate), lymph nodes (preferably one lymph node covering
the route of administration and another one distant from the route of ad-
ministration to cover systemic effects), spleen.

     (F)  Urogenital system—kidneys,  urinary  bladder,  prostate,  testes,
epididymides, seminal vesicle(s), uterus, ovaries, female mammary gland.

     (G) Other—all gross lesions and masses, skin.

     (iv) In inhalation studies, the entire respiratory tract, including nose,
pharynx, larynx, and paranasal sinuses should be examined and preserved.

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In dermal studies, skin from treated and adjacent control skin sites should
be examined and preserved.

     (v) Inflation of lungs and urinary bladder with a fixative is the optimal
method for preservation of these tissues. The proper inflation and fixation
of the lungs in inhalation studies is considered essential  for appropriate
and valid histopathological examination.

     (vi) Information from clinical pathology and other in-life data should
be considered before microscopic examination, since they may provide sig-
nificant guidance to the pathologist.

     (12) Histopathology. (i)  The following histopathology should be per-
formed:

     (A) Full histopathology on the  organs and tissues (listed under para-
graph (e)(ll)(iii) of this  guideline)  of all rodents  and nonrodents in the
control  and high-dose groups, and  all rodents  and nonrodents that died
or were  killed  during the  study. The  examination  should  be extended to
all animals in all dosage groups if treatment-related changes are observed
in the high-dose group.

     (B) All gross lesions  in all animals.

     (C) Target tissues in all animals.

     (ii)  If the  results show substantial alteration of the animal's normal
life span, or other effects that might compromise the significance of the
data, the next lower levels should be examined fully as described in para-
graph (e)(12)(i) of this guideline.

     (iii) An attempt should be made to correlate gross  observations with
microscopic findings.

     (iv) Tissues  and organs  designated for  microscopic  examination
should be fixed in 10 percent buffered formalin or a recognized suitable
fixative as  soon as necropsy is performed and no less than 48 hours  prior
to trimming.

     (f) Data and reporting—(1) Treatment  of results,  (i)  Data should
be summarized in tabular form, showing for each  test group the number
of animals  at the start of the test, the number of animals showing lesions,
the types of lesions and  the percentage of animals displaying  each type
of lesion.

     (ii) When applicable, all observed results (quantitative  and qualitative)
should be evaluated by an appropriate statistical method.  Any generally
accepted statistical methods may be used; the statistical methods including
significance criteria should be  selected during the design of the study.

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     (2) Evaluation of study results. The findings of a chronic toxicity
study should be evaluated in conjunction with the findings of preceding
studies and considered in terms of the toxic effects as well as the necropsy
and histopathological findings. The evaluation will include the relationship
between the dose  of the test substance and  the presence,  incidence, and
severity of abnormalities (including behavioral and clinical  abnormalities),
gross lesions,  identified target organs, body weight changes,  effects on
mortality and any other general or specific toxic effects.

     (3) Test report. In addition to the reporting requirements as specified
under 40 CFR part 792, subpart J, 40 CFR part  160, and the OECD Prin-
ciples of GLP (ISBN 92-64-12367-9), the following specific information
should be reported:

     (i) Test substance characterization should include:

     (A) Chemical identification.

     (B) Lot or batch number.

     (C) Physical properties.

     (D) Purity/impurities.

     (ii) Identification and composition of any vehicle used.

     (iii) Test system should contain data on:

     (A)  Species and  strain  of  animals used and rationale for selection
if other than that recommended.

     (B) Age including body weight data and  sex.

     (C) Test environment including cage conditions, ambient temperature,
humidity, and light/dark periods.

     (D) Identification of animal diet.

     (E) Acclimation period.

     (iv) Test procedure should include the following data:

     (A) Method of randomization used.

     (B) Full description of experimental design and procedure.

     (C) Dose regimen including levels, methods, and volume.

     (v) Test results.

     (A) Group animal data.  Tabulation of toxic response data by species,
strain, sex and exposure level for:

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     (7) Number of animals exposed.

     (2) Number of animals showing signs of toxicity.

     (3) Number of animals dying.

     (B) Individual animal data.  Data should be  presented as summary
(group mean) as well as for individual animals.

     (7) Time of death during the  study or whether animals survived to
termination.

     (2) Time of observation of each  abnormal sign and  its  subsequent
course.
        Body weight data.

     (4) Feed and water (if collected) consumption data.

     (5) Achieved dose (mg/kg/day) as a time-weighted average if the test
substance is administered in the diet or drinking water.

     (6) Results of ophthalmological examinations.

     (7) Results of hematological tests performed.

     (8) Results of clinical chemistry tests performed.

     (9) Urinalysis tests performed and results.

     (Iff) Results of observations made.

     (11} Necropsy findings,  including absolute  and relative (to body
weight) organ weight data.

     (72) Detailed description of all histopathological findings.

     (13) Statistical treatment of results, where  appropriate.

     (iv) In addition,  for inhalation studies the following should be re-
ported:

     (A) Test conditions. The following exposure  conditions must be re-
ported:

     (7) Description of exposure apparatus including design, type, dimen-
sions, source of air,  system for generating particulate and aerosols, method
of conditioning air, treatment of exhaust  air and the method of housing
the animals in a test chamber.

     (2) The equipment for measuring temperature, humidity, and particu-
late aerosol concentrations and size should be described.

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     (B) Exposure data. These data should be tabulated and presented with
mean values  and a measure of variability  (e.g., standard deviation)  and
should include:

     (7) Airflow rates through the inhalation equipment.

     (2) Temperature and humidity of air.

     (3) Actual (analytical or gravimetric) concentration in the breathing
zone.

     (4) Nominal concentration (total amount of test substance  fed  into
the inhalation equipment divided by volume  of air).

     (5) Particle size distribution, calculated MMAD, and geometric stand-
ard deviation (GSD).

     (6) Explanation as to  why  the  desired chamber concentration and/
or particle size could not be achieved (if applicable) and the efforts taken
to comply with this aspect of the guidelines.

     (g) Quality control. A system should be developed and maintained
to assure  and  document adequate performance of laboratory staff  and
equipment. The study must be conducted in compliance with GLP regula-
tions as described  by the Agency (40 CFR parts 160 and 792), and the
OECD principles of GLP (ISBN 92-64-12367-9).

     (h) References. The following references should be consulted for ad-
ditional background information on this test guideline:

     (1) Benitz, K.F. Measurement of Chronic Toxicity. Methods of Toxi-
cology. Ed. G.E. Paget. Blackwell, Oxford, pp. 82-131 (1970).

     (2) Crofton K.M.,  Howard J.L., Moser  V.C., Gill M.W., Leiter L.W.,
Tilson H.A., MacPhail, R.C. Interlaboratory  Comparison of Motor Activity
Experiments:   Implication   for   Neurotoxicological    Assesments.
Neurotoxicol. Teratol.  13, 599-609. (1991)

     (3) D'Aguanno, W. Drug Safety Evaluation—Pre-Clinical Consider-
ations. Industrial Pharmacology: Neuroleptic. Vol. I, Ed. S. Fielding  and
H. Lai. Futura, Mt. Kisco, NY. pp. 317-332  (1974).

     (4) Fitzhugh,  O.G. Chronic  Oral Toxicity, Appraisal of the Safety
of Chemicals in Foods, Drugs and Cosmetics.  The Association  of Food
and Drug Officials of the United States, pp. 36-45 (1959, 3rd  Printing
1975).

     (5) Food  Safety Council. Proposed System for Food Safety Assess-
ment. Prepared by the  Scientific Committee,  Food Safety Council. Food
and Cosmetic Toxicology. Vol. 16, Supplement 2. (December 1978).

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     (6) Gad S.C.  A Neuromuscular Screen for Use in Industrial  Toxi-
cology.  Journal of Toxicology and Environmental Health. 9, 691-704.
(1982)

     (7) Goldenthal, E.I.  and D'Aguanno, W.  Evaluation of Drugs, Ap-
praisal of the Safety of Chemicals in Foods, Drugs, and Cosmetics. The
Association of Food and Drug Officials of the United  States, pp. 60-67
(1959, 3rd Printing 1975).

     (8) International Programme  on  Chemical Safety.  Principles and
Methods for the Assessment of Neurotoxicity  Associated with Exposure
to Chemicals. Environmental Health Criteria Document No. 60. (1986)

     (9) Meyer  O.A., Tilson H.A.,  Byrd W.C., Riley M.T.  A Method for
the  Routine Assessment of Fore- and Hind-Limb Grip Strength  of Rats
and Mice. Neurobehav.  Toxicol. 1, 233-236. (1979)

     (10) Moser V.C., McDaniel K.M., Phillips P.M. Rat Strain and  Stock
Comparisons using a Functional Observational Battery: Baseline Values
and Effects of Amitraz. Toxicol. Appl.  Pharmacol. 108, 267-283 (1991)

     (11) National Academy of Sciences. Principles  and Procedures  for
Evaluating the Toxicity of Household Substances,A report prepared by the
Committee for the Revision of NAS Publication 1138, under the auspices
of the Committee on Toxicology, National Research Council, National
Academy of Sciences, Washington, DC (1977).

     (12) National  Center for Toxicological Research. Appendix B, Report
of Chronic  Studies Task  Force Committee, April 13-21,  1972. National
Center for Toxicological Research, Rockville, MD (1972).

     (13)  Organization  for  Economic  Cooperation  and  Development.
Guidelines for Testing  of Chemicals, Section 4-Health  Effects, Part 452
Chronic Toxicity Studies,  Paris (1981).

     (14) Page, N.P. Chronic  Toxicity  and Carcinogenicity Guidelines.
Journal of Environmental Pathology and Toxicology.  11:161-182 (1977).

     (15) Schwartz, E. Toxicology of Neuroleptic Agents. Industrial Phar-
macology:  Neuroleptic. S. Fielding and H. Lai. Futura, Mt.  Kisco, NY
pp. 203-221 (1974).

     (16) Toxicity  and Clinical Trial Subcommittee, Committee on Safety
of Medicine. (November 1977).

     (17) Tupper, D.E., Wallace R.B. Utility of the Neurologic Examina-
tion in Rats. Acta. Neurobiol. Exp. 40, 999-1003 (1980).

     (18) United States  Pharmaceutical Manufacturers Association. Guide-
lines for the Assessment of Drug and Medical  Device Safety in Animals.
(1977).

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     (19) Weingand K., Brown G., Hall R.  et al. (1996).  Harmonization
of Animal Clinical Pathology  Testing in  Toxicity and Safety Studies.
Fundam. andAppl. Toxicol. 29:198-201.

     (20) World Health Organization (WHO). Guidelines  for Evaluation
of Drugs for Use in Man. WHO  Technical Report Series No. 563.

     (21) World Health Organization (WHO). Part I. Environmental Health
Criteria 6, Principles and Methods for Evaluating the Toxicity of Chemi-
cals. WHO, Geneva (1978).

     (22) World Health Organization (WHO). Principles for Pre-Clinical
Testing of Drug Safety, WHO  Technical Report Series No. 341. WHO,
Geneva (1966).
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