United States
Environmental Protection
Agency
Office of Air Quality
Planning ar.d Standards
Research Triangle Park, NC 27711
EPA-454/R-00-Q40b
September 2000
Air
EVALUATION OF PARTICULATE MATTER
ERA (PM) CONTINUOUS EMISSION
MONITORING SYSTEMS (CEMS)
Final Report
Volume 2—Appendices for Initial
Correlation Tests
-------
Volume 2—Appendices for Initial Correlation Tests
Table of Contents
ICa! Appendix A—Process Operating Conditions
ICal Appendix B—Computer Results for M17 Tests
ICal Appendix C—M17 Field Sampling Data Sheets
ICal Appendix D—M17 Field Laboratory Particulate Weight Data
ICal Appendix E—M17 Post-Test Calibration Sheets
ICal Appendix F—PM CEMS Data for Each Run
ICal Appendix G—Statistical Analysis Data and Graphs for PM CEMS
MRI-<5PPTMt47
-------
ICal Appendix A
Process Operating Conditions
MRI-aPPT*47
-------
o
e.
1*1
Run i1Q
Time 9:oo
Parameters
Steam How (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (!b/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp {deg F)
Baghouse Outlet Temp {deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #11
Time 12:00
Parameters
Steam Flow (klb/hr)
Steam Temp {deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrale Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #10 Avg Run #10 Low Run #10 High
9:15
9:30
9:45
10:00 10:15 10:30 10:45
283.2
963
27OOO
2,9
3.6
3.7
1.4
132380
133370
188.3
185.7
6.8
-24.1
4.79
271.1
970
26341
29
3.4
3.7
1.6
127088
129776
192.1
189.7
7.3
-23.9
276.5
959
32727
3.4
3.7
3.8
2.7
130964
132113
188.4
169.6
7.2
•24
277.4
946
30000
3.6
3.8
4.1
2.8
127390
131200
183.3
1B8.4
6.6
-23.1
277.5
949
29189
3.6
4.1
3.9
2.9
127437
133623
185
189.2
7.1
-23.4
278
951
27892
3.8
3.7
4.3
3.5
12908S
129873
187,3
188.2
6.6
-22.6
264.7
933
24545
4.0
3.9
3.7
4.5
126703
128137
184.9
187.1
7.2
-16.4
273.2
935
24545
3.8
3.6
4.1
3.9
128382
128125
185.2
184.5
6.7
-22.8
275.2
951
27755
3.5
3.7
3.9
2,9
128676.3
130777.1
186.8
187.8
6.9
-22,5
264.7
933
24545
2.9
3,4
3.7
1.4
126703
128125
183.3
184.5
6.6
-16.4
283.2
970
32727
4.0
4,1
4.3
4.5
132380
133623
192.1
189.7
7.3
-24,1
12:15 12:30 12:45 13:00 13:15 13:30
266.2
945
25714
4.5
4,3
5.3
4
132675
133330
188.4
185.5
7
-24
4.56
234.3
945
27692
4.2
3.8
5.4
3.3
132431
131660
182.3
185.5
7.1
-24.1
278.4
942
25714
3,7
3.3
4.3
3.6
132283
133324
185,6
185.4
6.8
-24.3
282
942
27000
3.7
3.3
4.4
3.5
132673
132610
182.6
186.5
7.3
-24.1
250.4
932
20377
5.0
5.5
4.7
,4.8
115976
115410
188.1
182.9
5,5
-19.9
281.7
935
24545
3,8 '
3.6
4.7
3
133128
133154
184.1
181.8
7,1
-23.2
277.2
952
29189
3.6
3.3
4.8
2.6 '
131603
132039
185.2
184.3
6.8
-23.1
Run #11 Avg Run #11 Low Run #11 High
274.3
941,9
25747.3
4.1
3.9
. 4.8
3.5
130096.3
130218.1
185.2
184.6
6.8
-23,2
250.4
932
20377
3.6
3.3
4.3
2,6
115976
115410
182.3
181.8
5.5
-19.9
284.3
952
29189
5
5.5
5.4
4.8
133128
133330
188.4
186,5
7.3
-24.3
-------
I
I
Time
Parameters
Steam Flow (klb/hr)
Steam Temp {deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
Easl Undergrate Air Flow (Ib/hr)
West Undergrats Air Flow {Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Time
Parameters
Steam Flow (kib/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Iniet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H20)
ID Fan Suet. Press, (in H2O)
Opacity
Run #12
14:45
270,1
949
27000
3.6
3.2
44
3.2
130569
132483
233.8
185.1
6.5
-23.5
s.ss
Run #13
9:15
234
955
21600
6.3
6
6.4
5.5
114100
117348
185.6
178.3
5,6
-19.7
3.72
16:00
284,8
955
27692
3,3
2,9
4.3
2.8
131814
130016
1866
181.6
7,6
-24.1
9:30
255,4
969
28421
3.4
32
4.6
2,5
117597
116331
185,7
. 179,7
6.6
•20.2
16:15
278.2
955
28421
3.4
2.9
4.1
3.2
130379
12B762
187.1
182.2
7.4
-23.7
9:45
282. B
951
28421
3.4
2.7
4.9
2.7
130220
130445
186.6
180.1
10
-22.7
15:30
280.9
958
28421
3.2
2.5
4
3.1
130434
129020
185.6
183.4
7.4
•23.7
10:00
281
S47
30000
3.0
2.5
3.8
2,8
133604
1345E1
132.1
179.4
7.5
-24,5
15:45
284.4
962
27692
2.9
1.7
3.8
3.T
131097
130523
IBS
183.7
8.5
-24.6
10:16
284.8
955
30857
3.1
2.5
3.9
2.8
136208
135010
185.8
176.7
7.2
-24.5
16:00
284.6
965
30000
2.7
1.3
3.6
3.1
129606
131413
183
185
12.1
-24.6
10:30
282
954
27692
3.1
2.3
3.7
3.2
136799
135483
185.8
184,6
8.7
-24,4
16:15
286.1
S60
28421
2.9
1.7
3.5
3.4
131545
130925
183.4
186.2
8.1
-24.5
10;45
277.1
956
28421
3.4
3.1
3.6
3.5 '
133241
132107
184.2
188.3
6.3
-24
16:30
279.6
952
26341
3.3
2
3.8
4.2
130419
132538
186.1
185,1
7.5
-24.4
Run #12 Avg Run #12 Low Run #12 High
282.2
957.0
27998.5
3.2
2.3
3.9
3.3
130732.9
130833.6
191.7
184.0
8.1
-24.1
Run #1 3 Avg
271.0
955.3
27916.0
3.5
3.0
4.3
3.3
128824.1
128753.6
185,1
180.9
7.4
-22.9
278.2
949
26341
2.7
1.3
3.5
2.8
129606
129020
183
181.6
6.5
-23.5
286.1
965
30000
3.6
3.2
4.4
4.2
131814
132538
233.8
186.2
12.1
-24.6
Run #1 3 Low Run #13 High
234
947
21600
3.0
2.3
3.6
2.5
114100
116331
182.1
176.7
5.6
-19.7
284.8
869
30857
5.3
5
5.4
5.5
136799
135483
186.6
188.3
10
-24.5
-------
o
E.
I
Run #14
Time 12:15
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #15
Time 15:45
Parameters
Steam Flow (klb/hr)
Steam Ternp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #14 Avg Run #14 Low Run #14 High
12:30 12:45 13:00 13:15
13:30 13:45
14:00
275.6
957
27000
3.1
3.3
3.5
2.5
129500
130341
1843
185.7
5.7
•22,5
4.51
274.5
950
27000
3.2
3,7
3.8
2.1
127550
129564
184.2
184.8
6.7
•22,4
277.7
953
34839
3.0
3.8
3,7
1,5
130375
129997
184.6
184.3
6.1
•22.6
279.5
947
27000
3.0
3.9
3,7
1.5
131702
130779
1B3.9
184.3
5.8
-22.6
284.5
946
27692
2.8
3.4
3,7
1.4
133631
134053
184.4
1B8.fi
7.8
•24
281.2
956
28421
3.0
3.6
3.4
2
134088
132940
180.7
188.7
S.9
•16.9
285.8
949
28421
2.8
3,5
3.1
1.3
136027
132574
1B5.9
160.7
7.3
•24.1
291.5
966
29189
2.3
2.8
3.2
1
13721S
135173
183.1
190.S
6.8
-24
281.3
951.8
28695.3
2.9
3.5
3.5
1.7
132511.0
131927.6
183.9
186.9
6.6
-22.4
274.5
946
27000
2.3
2.8
3.1
1
127500
129564
180.7
184.3
5.7
-16.9
291.5
957
34839
3.2
3.9
3.8
2.5
137215
135173
185.9
190.7
7.6
-24.1
Run #15 Avg Run #15 Low Run #15 High
16:00 16:15 16:30 16:45 17:00 17:15 17;30
280.5
949
27000
3.0
3.7
3.6
1.6
133514
1322E2
184.3
180.7
7-1
-23.9
5,27
279.4
952
24545
2.8
3.2
3.S
1.5
133199
133234
184.4
180.8
6.1
-23,4
2802
951
24545
3,0
3.7
3.4
2
132974
132027
184.4
1822
6.7
-23.4
283.7
948
27000
2,6
3.4
2.8
1.6
135467
132902
184,8
179.8
6.8
-24.1
285.5
948
24000
2.7
2.4
3.5
2.2
134134
133192
188.4
181.5.
6,9
-23.9
284.2
954
27000
2,4
2.1
3.3
1.9
135871
132718
184.2
180,5
7,4
•24.1
2875
951
27000
2,7
3,4
3.2
1.6 '
134064
133622
183.9
180.6
6.8
-23.9
285.8
9S5
25714
2.7
3
3.3
1,8
135890
135092
184.8
S81.3
7.3
-24.3
283.3
951.0
25850.5
2.7
3.1
3.3
1.8
134389.1
133129.9
184.7
180.9
69
-23.9
279.4
948
24000
2.4
2.1
2.8
1.5
132974
132027
183.9
179.8
6.1
•23.4
287.2
955
27000
3,0
3,7
3.6
2.2
135890
135092
186.4
182.2
7.4
-243
-------
w
Run #16
Time 9;oo
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Time
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coat Flow (Ib/hr)
Boiler 02s (Avg)
west
central
east
East Undergrate Air Row (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2Q)
ID Fan Suet. Press, (in H2O)
Opacity
Run #16 Avg Run #16 Low Run #16 High
9:15
9:30
9:45
10:00 10:15 10:30 10:45
266.2
942
26341
3.9
3.5
4.2 '
4
124225
129757
185.4
178
6.6
-24.1
3.71
Run #17
12:30
271,4
950
24545
3.7
3.9
4.2
3.1
130145
129989
183
179.6
6.7
-22.4
' 3.54
276.7
953
28421
3.4
2.8
4.7
2.6
133948
132197
185.2
173.9
6.6
-23,5
12:45
377.2
953
27692
3.7
4
4.1
3.1
134460
134130
182.8
180.2
as
-22.6
287
858
36000
2.8
2
4
2.4
135580
135959
186
179.8
6.9
-24
13:00
282,4
953
27000
3.E
3.5
3.8
3.1
136585
135309
187,5
180.3
6,3
-23.7
284.2
957
28421
3.Q
2.7
3.9
2.3
136456
134408
184.1
181.1
' 6.9
-24.1
13:15
275,7
957
2S341
3.9
4.6
4
3.2
134045
131S82
185.2
180.4
6.6
-23.2
287.4
955
36000
3.0
3.1
3.8
2
137647
136618
184.9
178.4
6.2
•23.9
13:30
286.9
954
26341
3.5
3.5
4,3
2.6
138127
13555S
185.7
179.5
7.2
-24.1
281.5
637
26341
3.2
3.4
3.7
2.4
136632
133927
182.7
1B0.2
6.9
-23.8
13:45
281.9
952
28421
3,5
3.4
4.1
2,9
135336
132755
193.2
177.2
7.2
•23.7
287.6 282.8
950 951
28421 29189
3.1 3.5
3.4 4.3
3.7 4
2.2 2.2
136796 135747
135847 134180
175.4 181.1
180.4 181.2
6.8 6.4
-24.2 -24.2
14:00
283,5
953
27692
3.3
3.2
3.7
3,1 '
134772
133821
185.7
182.9
6,9
-24
281.7
950.4
29891.8
3,2
3.2
4,0
2.5
134628.9
134111.6
183.1
179.8
6,7
-24.0
Run #1 7 Avg
279,9
953.1
26861.7
3,6
3.7
4.0
3.0
134781,4
133363.0
186,1
180.0
7,2
-23.4
266.2
937
26341
2.8
2
3.7
2
124225
129757
175.4
178
6.2
-23.5
287.6
958
36000
3.3
4.3
4.7
4
137647
136618
186
181.2
6,9
-24.2
Run #17 Low Run #17 High
271.4
950
24545
3.3
3.2
3.7
2.6
130145
129989
182.6
177.2
6.3
-22.4
286.9
957
28421
3.9
4.6
4.3
3.2
138127
135555
193.2
182.9
9.5
-24.1
-------
o
E.
Run #18
Time 1S:45
Parameters
Steam Flow (klb/hr)
Steam Temp {deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
wesl
central
east
East Undergrate Air Row (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity 3.92
Run #19
Time 9:30
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Goal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #18 Avg Run #18 Low Run #18 High
16:00 16:15 16:30 16:45 17:00 17:15 17:30
281.9
954
27632
3.5
3
3.8
3.7
133593
133711
183.6
180.5
7
286.6
957
29189
3.0
1.8
4.1
3.2
135786
134098
178.2
179.9
7.4
-24.1
285. S
950
27692
2.9
1.4
3,5
3.9
134048
135737
1856
181.4
7.6
-24.4
282.9
942
28421
3.9
3.4
4.4
134609
134841
185.9
181.5
8.1
-19.6
285.3
950
28421
4.1
4.4
3.8
134081
134383
183.3
180.2
7
-24.3
282.8
944
28421
4.2
3.8
4,6
133778
132152
185.4
181.2
7.7
-24.4
284.5
958
29189
4.1
4.3
3.9
134199
132461
180.9
180,2
7.9
-33.3
282.8
350
29189
4.2
4.4
4
131876
133174
182.4
179.5
8.7
-23.1
284.0
950.6
28526.8
3.7
2.1
4,0
3.9
133996.3
133819.6
183.2
180.6
7.4
-23.3
281.9
942
27692
2.9
1.4
3.4
3.2
131876
132152
178.2
179.5
6.7
-19,6
286.6
958
29189
4.2
3
4.4
4.6
135786
135737
185.9
181.5
8.1
-24.4
Run #19 Avg Run #19 Low Run #19 High
9:45
10.00 10:15 10:30 10:45 11:00 11:16
2B2.7
9E6
28421
2.7
2.9
3.4
1.9
134378
135298
186.5
179.5
5.9
-22.6
4.01
281 4
857
29189
2.9
3.4
3.4
2
134700
135296
185.3
179.2
6.8
-23.8 •
285.4
954
Z918S
2.9
3.2
4
1,5
134628
(35190
184.4 '
180
5.9
-22.5
282,2
949
28421
3.1
3.8
3.9
1.6
134833
136399
185.6
180.1
8.8
286.3
951
28421
3.0
3.6
4
1.3
135626
135618
182.8
179.6
6,1
•22.8
284,1
952
30857
3.0
3,5
3.8
1,7
137442
134252
185.2
180.6
6.6
-23.6
277.2
951
27000
3.2
4.1
4.1
1.4 '
133744
133401
185.2
179.1
6,2
-23.1
271.7
944
24545
3.6
4.6
4.1
2.1
133474
131819
188.6
179.1
5.7
-22,5
281.4
951.8
28255.4
3.1
3.6
3.8
1.7
134853.1
134659.1
185.2
179,7
6.3
-23.0
271.7
944
24545
2.7
2.9
3.4
1.3
133474
131819
182,8
179.1
5.7
-22.5
286.3
957
30857
3.6
4.6
4.1
2.1
137442
136399
186,6
180.6
6.8
-23.6
-------
n
e.
Time
Parameters
Steam Row (klb/hr)
Steam Temp (deg F)
Coal Flow (ib/hr)
Boiler O2s (Avg)
west
central
east
East Underrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp {deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Tims
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s {Avg)
west
central
east
Easl Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Sucl. Press, (in H2O)
Opacity
Run #20
e 13:00
'S
r) 273.6
:) 957
') 27000
|) 3.5
>t 4.7
it 4.5
it 1.2
') 133318
') 131886
:) 184.8
) 180.3
) 7.1
} -23.3
185.3
> 178.3
I 6.7
I -23.9
' 4.14
13:15
282.8
955
30857
4.4
4.8
3.9
13SJ64
136248
184.7
180.4
7.3
-24
16:45
280,3
950
27000
3.1
3
3,3
3.1
134756
133840
186.2
180.7
6.8
-23.6
13:30
287.4
948
27692
4.2
4.4
3,9
135401
136334
185.4
179.2
7
•23.9
17:00
282.8
956
2S189
3.1
2.B
3.9
2.7
13352$
1339S8
184.7
180.6
8.7
•23.5
13:45
281.7
947
26341
4.3
4.9
3.7
136065
135929
185.2
180.4
6.4
-23.9
17:15
281.1
950
27692
34
3.3
3.6
3.3
135845
134608
134.8
181
6.7
-24
14:00
284.2
954
28421
4.4
43
4.4
136013
134453
185.5
181.4
7.2
•23.8
17:30
278.1
943
27000
34
3.2
4
3.1
133040
133694
179.1
180,8
6.6
-24.2
14:15
277.6
954'
25116
4.5
5.1
4.1
131920
133549
184.8
179,4
6.8
-23
17:45
282.6
949
27000
3,5
3.2
3,1
4.3
131675
130955
183.1
178.8
G.9
-24.1
14:30
289.4
949
28421
4.2
4.3
4.1
135971
13S607
184.7
180.5
6.7
-23.6
18:00
276.4
956
25714
3.2
3.4
3.4
2.9 '
131575
128824
182.9
18O.6
6.5
-23.5
14:45
268.7
949
26341
4.5
4.9
4.1
127137
1284EO
184.3
180.1
6.S
'22.1
Run #20 Avg Run #20 Low Run #20 High
280.7
951.6
27523.6
4.2
4.7
4.1
1.2
133998,6
134057.0
185.0
180.2
6.9
-23.5
268.7
947
2511B
3.5
4.3
3.7
1.2
127137
128450
184.6
179.2
6.4
-22.1
289.4
957
30857
4.6
5.1
4.5
1.2
136§71
136334
185.5
181,4
7.3
-24
Run #21 Avg Run #21 Low Run #21 High
281.0
950.4
27227.S
3.3
3.1
3.5
3.2
133560,0
133113.3
183,7
180.2
6.7
-23.8
276.4
943
25714
3.0
2.6
3.1
2.7
131575
128824
179.1
178.8
6.5
-23.5
285,8
956
29189
3.5
3.4
4
4.3
135845
135914
186.2
181
6.9
-24.2
-------
!~- 1
O
s.
i
w
Time
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coat Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Time
Run #22
9:00
286.8
949
28421
3.3
3.7
4
2.2
137924
136574
185.4
179.S
6.7
-23.8
4,25
Run #23
12:00
9:15
287
956
27000
3.2
3,6
4
.1.9
137726
136021
185,2
178,4
7.1
-24.2
12:15
9:30
291.4
946
29189
3.0
3.3
• 3.6
2.2
139S86
140126
184,7
178.7
7.1
-24.4
12:30
9:45
294.1
S47
30000
3.0
3.1
3.1
2.7
138921
138528
185,3
179,7
7
-24.2
12:45
10:00
282.6
950
3.1
3.8
3.1
2.3
138256
135816
183.1
179.7
6.5
-23.7
13:00
10:15
279.9
946
25714
3.5
3.9
3,9
2.8
135016
134285
134,7
179.3
6,4
-23.1
13:15
10.30
280.9
950
27692
34
3.8
3,9
2.5
134176
133902
185
178.7
6.1
-23.1
13:30
10:45
275
954
28341
3.4
4.5
3.6
2.2
133695
133948
184.8
180.1
7.2
-23.8
Run #22 Avg
284.6
949.8
27765.3
3.2
3.7
3.7
2.4
136925,0
136150.0
184.8
179.3
6.8
-23.8
Run #23 Avg
Run #22 Low
275
946
25714
3.0
3.1
3.1
1.9
133695
133902
183.1
178.4
6.1
-23.1
Run #22 High
294,1
956
30000
3.6
4.5
4
2.8
139686
140126
185,4
180.1
7.2
-24.4
Run #23 Low Run #23 High
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undergrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (In H2O)
ID Fan Suet. Press, (in H2O)
Opacity
269.4
852
27000
3.7
4.5
5
1.5
130233
130408
185.3
179,2
6.9
-22.8
4.11
283.6
947
2454S
4.0
4.7
4.7
2.5
121390
12S469
134.4
179.6
6.5
-22.3
266.9
954
27692
3.6
4.1
4.9
1.9
128572
129336
219.4
180.2
6.8
-22.6
269.2
950
27692
3,4
4
4.3
1.9
128353
127528
184.1
179.6
6
-21.6
268.2
952
23478
3.2
4
4.2
1.5
129835
127609
183.4
180
S.3
-21.8
271.8
961
24545
3.3 '-
4,1
4.3
1.5
130124
129356
1852
179.4
6.3
-18.4
268.1
947
2S714
3.4
4.2
4.3
1.8 '
130686
128955
185.5
179.5
5.6
-21,9
268.2
950.4
25809.4
3.5
4.2
4.5
1.8
128456.1
128523.0
189.6
179.6
6.3
-21.6
263.5
947
23478
3.2
4
4.2
1.5
121390
125469
183.4
179.2
5.6
-18.4
271.8
954
27692
4.0
4.7
5
2.5
130686
130408
219.4
180,2
6.9
-22.8
-------
CO
e
5
Run #24
Time 15:15
Parameters
Steam Flow (klb/hr)
Steam Temp (deg F)
Coal Flow (Ib/hr)
Boiler O2s (Avg)
west
central
east
East Undergrate Air Flow (Ib/hr)
West Undargrate Air Flow (Ib/hr)
Baghouse Inlet Temp (deg F)
Baghouse Outlet Temp (deg F)
Baghouse DP (in H2O)
ID Fan Suet. Press, (in H2O)
Opacity
Run #24 Avg Run #24 Low Run #24 High
15;30 15:45 16:00 16:15 16:30 16:45
17:00
281.3
955
27692
2.7
2..S
3,5
2,1
130768
130833
186.2
179
6.6
-23.5
5.39
278.6
849
27000
3.1
2.9
4,3
2.2
129071
130871
183
180.5
7.3
-235
283.8
963
30000
3.0
2.S
4.8
2
130724
129900
185.6
179.7
7.5
-23.2
282.8
945
25116
2.9
2.3
4
2.5
129406
12S089
186.9
180.8
7.3
-23.2
281.8
953
276S2
3.3
2,7
3.8
3.3
130319
128860
186.4
179.8
7.1
-23.6
276.6
951
26341
3.3
1.9
4.4
3.6
129327
130675
186.4
179.9
6.1
-23.3
280.2
946
14026
3.0
1.3
4.6
3.1
129680
129477
186
177.8
7.7
-23.4
280.8
947
15882
2.6
1.4
3.8
2.6
130238
131060
185.3
180.8
7.4
-23.1
280.7
949.9
24218.6
3.0
2.2
4.1
2.7
129941.4
130108.1
186.1
179.8
7.1
-23.4
276.6
945
14026
2.6
1.3
3.5
2
129071
128860
185.3
177.8
6.1
-23.1
283,8
655
30000
3.3
2.9
4.6
3.6
130766
131060
188
180.9
7.7
-23.6
-------
ICal Appendix B
Computer Results for M17 Tests
MW-GPFWWHB-flZ-f!? Appendices Coven. WPD
-------
-------
FILE NAME - RIOA
S.UN # - 10 - Method 17 TRAIN A for PM
LOCATION - Unit 2 A Baghouse Outlet Duct
DATE - 07/15/99 Time: 0855-1044
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic ?eet)= 758.680
Final Meter Volume (Cubic Feet)= 819.283
»feter Factor= 1.011
?inal Leak Rate (cu ft/min)= 0.005
Set Meter Volume (Cubic Feet)= 61.270
3as Volume (Dry Standard Cubic Feet)- 59.258
Barometric Pressure (in Hg)= ' 30.04
Static Pressure (Inches'H20)= -24.71
Percent Oxygen= 5.0-
Percent Carbon Dioxide= 14.6
•foisture Collected (ml)- 184.0
Percent Water= 12.8
\verage Meter Temperature (F) = 90
Average Delta H (in H20)= 1.45
Average Delta P (in H20) = 1.690
Average Stack Temperature (F)= 194
Dry Molecular Weight= 30.54
fet Molecular Weight= 28.94
Werage Square Root of Delta P (in H2Q) = 1.2170
's Isokinetic= 100.7
?itot Coefficients 0.84
Sampling Time (Minutes)= 100.0
fozzle Diameter {Inches)= 0.186
stack Axis il (Inches)= - 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= • 26.13
stack Velocity (Actual, Feet/rain)= 4,692
?low Rate {Actual, Cubic ft/rain)= 122,566
7low rate (Standard, Wet, Cubic ft/min)= 93,352
Plow Rate (Standard, Dry, Cubic ft/min!= 81,441
Particulate Loading - Front Half
?articulate Weight (g)= 0.0648
?articulate Loading, Dry Std. (gr/scf)= 0.0168
Particulate Loading, Actual (gr/cu ft)= 0.0112
Mission Rate (lb/hr)= 11.75
To Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:06:51
Corr. to 7% O2 & 12% C02
0.0147 0.0138
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - RIGA
RUN # - 10 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 0855-1044
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)=
Final Meter Volume (Cubic Meters)=
Meter Factor=
Final Leak Rate (cu m/min) =
Net Meter Volume (Cubic Meters)~
Gas Volume (Dry Standard Cubic Meters}=
Barometric Pressure (mm Hg)=
Static Pressure (mm H20)=
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
Average Meter Temperature (C)=
Average Delta H (ram H20)=
Average Delta P (mm H20)=
Average Stack Temperature fC)=
Dry Molecular Weight=
Wet Molecular Weight=
Average Square Root of Delta'P (mm H20)=
% Iso)cinetic=
PROG.=VER 05/27/89
07-22-1999 12:06:51
21.483
23.199
1.011
0,0001
1.735
1.678
763
-628
5.0
14.6
184.0
12.8
32
36.B
42.9
90
30.54
28.94
£.1334
100.7
Pitot Coefficient- 0.84
Sampling Time (Minutes}= 100.0
Nozzle Diameter (mm) = 4.72
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,430
Flow rate (Actual, Cubic m/min)= 3,471
Flow rate (Standard, Wet, Cubic m/min)= 2,543
Flow rate (Standard, Dry, Cubic m/min)= 2,306
Particulate Loading - Front Half
Particulate Weight (g)= 0.0648
Particulate Loading, Dry Std. (mg/cu m)= 38.6
Particulate Loading, Actual (mg/cu m)= 25.7
Emission Rate (kg/hr)= 5.34
No Back Half Analysis
Corr. to 7% 02 & 12% C02
33.8 31.7
ICal APPENDIX B
-------
FILE NAME - R10A
RUN # - 10 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 0855-1044
PROJECT # - 4702.02.04.09
Point f
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12;GS:51
Delta P
in. H20)
2
2
1
0
0
2
2
2
0
0
2
2
2
2
0
2
2
2
1
0
2
2
1
1
0
.400
.100
.900
.730
.040
.300
.400
.300
.880
.180
.700
.800
.400
.000
.260
.600
.400
.400
.700
.350
.400
,200
.700
.000
.100
Delta H
(in.
2.
1.
1.
0.
0.
1.
2.
2.
0.
0.
2 .
2.
2.
1 .
0.
2.
2.
2.
1.
0.
2.
1.
1.
0.
0.
H20)
00
80
60
61
03
90
00
00
74
15
30
40
10
70
22
20
10
10
50
30 '
10
90
50
87
08
Stack
(F)
190
191
193
194
196
193
193
195
195
196
194
195
195
195
194
194
195
195
194
194
194
194
194
193
192
T Meter T
In(F)
78
77
79
81
82
81
85
88
90
91
90
93
96
98
98
97
98
100
102
103
101
102
104
104
104
Out (F)
77
78
78
78
79
80
81
82
83
84
85
86
87
88
89
90
91
92
92
93
94
95
95
96
97
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3785 3.3214 0.0000 0.0571
PROBE RINS
IMPINGERS
Probe Rinse Blank (rag/ml)=
Final Wt.
(g) (g)
3.5778 3.5701
0.0000 0.0000
Tare Wt. Vol.
(ml)
25.4
0.0
O.OCOO
Impinger Blank (mg/ml)= O.OOCO
Net Wt
(g)
0.0077
0.0000
ICal APPENDIX B
-------
FILE NAME - R10B
RUN ft - 10 - Method 17 TRAIN E for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 0857-1046
PROJECT # - 4702.02.04.09
Initial Meter Volume (Oabic Feet)= 995.405
Final Meter Volume (Cubic Feet3= 1055.943
Meter Factor= 0.988
Final Leak Rate (cu ft/rain)= 0.002
Net Meter Volume (Cubic Feet)= 59.812
Gas Volume (Dry Standard Cubic Peet)= 58.3S9
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20)= -24.71
Percent Oxygen= 5.0
Percent-Carbon Dioxxde= 14.€
Moisture Collected (ml)= 188.8
Percent Water= , 13.2
Average Meter Temperature (F}= 85
Average Delta H (in H2Q) = - 1.49
Average Delta P (in H20)= 1.724
Average Stack Temperature (F)- 195
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.88
Average Square Root of Delta P (in H2Q}= 1.2282
% Isokinetic= ' 101.0
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= 66. Q
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet}= 26.13
Stack Velocity (Actual, Feet/rain]=• 4,742
Flow Rate (Actual, Cubic ft/min)= 123,885
Flow rate (Standard, Wet, Cubic ft/min}= 94,259
Flow Rate (Standard, Dry, Cubic ft/min)= 81,797
Particulate' Loading - Front Half
Particulate Weight (g)= 0.0667
Particulate Loading, Dry Std. (gr/scf)= 0.0176
Particulate Loading, Actual (gr/cu ft)-" 0.0116
Emission Rate Ub/hr) = 12.34
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:07:43
Corr. to 7% 02 & 12% C02
0.0154 0.0145
ICal APPENDIX B
-------
* * METRIC UNITS * *
PILE NAME - R10B
RUN # - 10 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DAT1 - 07/15/99 Time: 0857-1046
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 28.186
Final Meter Volume (Cubic Meters)= 29.900
Meter Factor= 0.988
Final Leak Rate (cu m/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1.694
Gas Volume (Dry Standard Cubic'Meters)= . 1.653
Barometric Pressure (mm Hg)= 763
Static Pressure (mm H20)= -S2S
Percent Oxygen= 5 . 0
Percent Carbon Dioxide= 14.6
Moisture Collected (tnl)« 188.8
Percent Water= 13.2
Average Meter Temperature (C}= 29
average Delta H (mm H20)= 37.8
Average Delta P (mm H20)= 43.8
Average Stack Temperature (C)= 90
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.88
Average Square Root of Delta P (mm H20)=' 6.1900
fe Isokinetie= .. 101.0
Pitot Coefficient^ 0.84
Sampling Time (Minutes)= 100.0
STozzle Diameter (mm) = - 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,445
Flow rate (Actual, Cubic m/min)= 3,508
Flow rate (Standard, Wet, Cubic m/min)= 2,669
Flow rate (Standard, Dry, .Cubic m/min)= 2,316
Particulate Loading - Front Half
Particulate Weight (g)= O.OS67
?articulate Loading, Dry Std. (mg/cu m)= 40.4
?articulate Loading, Actual (mg/cu m)= 26.6
Emission Rate (kg/hr)=- 5.60
to Back Half Analysis
PROG.=VER OS/27/89
07-22-1999 12:07:43
Corr.
to 7% O2
35.3
12% C02
33.2
ICal APPENDS B
-------
FILE NAME - R10B
ROT # - 10 - Method 17'TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 0857-1046
PROJECT # - 4702,02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:07:43
Delta P
(in
2.
2.
2.
1.
0.
2.
2.
2.
0.
0.
2.
2.
1.
0.
0.
2.
2.
2.
0.
0.
2.
2 .
2.
1.
0.
. H20S
700
600
400
400
620
500
500
200
600
120
500
200
800
710
060
700
200
400
680
120
900
900
000
900
390
Delta H
(in.
2.
2.
2.
. 1.
0.
2.
2.
1.
0.
0.
2.
1.
1.
0,
0.
2.
1.
2.
0.
0.
2.
2.
1.
1.
0.
H20)
30
20
10
20
52
10
10
90
51
10
20
90
60
61
05
30
90
10
59
10
50
50
80
70
34
Stack
(F)
191
193
194
196
196
196
195
195
196
196
194
195
195
196
195
195
195
195
194
195
195
194
194
193
192
T Meter T
InCF)
77
78
79
79
80
81
82
84
85
86
86
86
88
89 '
89
89
89
91
92
93
93
92
94
95
95
Out (F)
77
78
78
78
78
78
79
. 80
80
81
82
82
83
' 84
84
85
85
86
87
88
88
88
89
89
90
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
Cg) (g) (g) (g)
o.oooo o.oooo o.oooo o.oooo
3.3692 3..3149 0.0000 0.0543
Final Wt. Tare Wt.
(g) (g)
PROBE RINSE 3.7590 3.7466
IMPINGBRS 0.0000 0.0000
Probe Rinse Blank (tng/ml}= 0.0000
Impinger Blank (mg/ml)= 0.0000
Vol.
(ml)
37.5
0.0
Net Wt,
(g)
0.0124
0.0000
ICal APPENDIX B
-------
FILE NAME - R11A
RUN # - 11 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1147-1336
PROJECT # - 4702.02,04,09
Initial Meter Volume (Cubic Feet)= 819.525
Final Meter Volume (Cubic Feet)= 879.100
Meter Factor= 1.011
Final Leak Rate (cu ft/min)- 0.007
Net Meter ¥olume (Cubic Feet)= 60.230
Gas Volume (Dry Standard Cubic Feet)= 57.170
Barometric Pressure (in Hg)= 30.05
Static Pressure (Inches H20)= -26.45
Percent Oxygen= 5.0
Percent Carbon Dioxide= 14.5
Moisture Collected (ml)- 176.2
Percent Water= 12.7
Average Meter Temperature (F)« 101
Average Delta H (in H20)= 1.40
Average Delta P (in H20)= • 1.642
Average Stack Temperature (F)= 191
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.93
Average Square Root of Delta P (in H20)= 1.1964
i Isokinetic= 100,9
Pitot Coe£ficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= • 0.184
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,609
Plow Rate (Actual, Cubic ft/mini= 120,415
?low rate (Standard, Wet, Cubic ft/min)= 91,840
Plow Rate (Standard, Dry, Cubic ft/min}= 80,198
Particulate Loading - Front Half
Particulate Weight (g)= 0.0687
Particulate Loading, Dry Std. (gr/scf)= 0.0185
Particulate Loading, Actual (gr/cu ft)= 0.0123
Emission Rate (Ib/hr)- . 12.72
fo Back Half Analysis
PROG.=VER OS/27/89
07-22-1999 12:11:03
Corr. to 7% 02 & 12% CO2
0.0162 0.0153
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R11A
RIOT # - 11 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1147-1336
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters}- 23.206
Final Meter Volume (Cubic Meters)= 24.893
Meter Factor= 1.011
Final Leak Hate (cu m/min)= 0.0002
Net Meter Volume (Cubic Meters)= 1.705
Gas Volume (Dry Standard Cubic Meters)= ' 1.619
Barometric Pressure (mm Hg)= . 764
Static Pressure (mm H20)= -672
Percent Oxygen= 5 . 0
Percent Carbon Dicxide= ' 14.5
Moisture Collected (ml)= . 176.2
Percent Water- 12.7
Average Meter Temperature (C)= 38
Average Delta H (mm H20)= 35.6
Average Delta P (mm H20)= 41.7
Average Stack Temperature !C)= 88
Dry Molecular Weight= ' 30.52
Wet Molecular Weight* . 28.93
Average Square Root of Delta P (mm H20)= 6.0295
% Isokinetic= 100.9
Pitot Coefficients 0.84
Sampling Time (Minutes)= 100.0
Nbzzle Diameter (mm)- 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= ' 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,405
Flow rate (Actual, Cubic m/min)= ' 3,410
Flow rate (Standard, Wet, Cubic m/min)= 2,601
Flow rate (Standard, Dry, Cubic m/min}= 2,271
Particulate Loading - Front Half
Particulate Weight .(g)= 0.0687
Particulate Loading, Dry Std. (mg/cu m)= 42.4
Particulate Loading, Actual (mg/cu m)= 28.3
Emission Rate (kg/hr)= 5.77
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:11:03
Corr. to 7% 02 & 12% C02
37.1 35.1
ICal APPENDIX B
-------
FILE NAME - R11A
RUN # - 11 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1147-1336
PROJECT tt - 4702.02.04.09
Point #
1
2
3
4
s
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:11:03
Delta P •
(in. H20)
2.400
2.100
1.800
0.630
0.050
2.600
2.500
2.000
1.000
0.300
2.700
2.700
2.800
1.200
0.330
2.600
2.300
1.700
1.500
0.250
2.400
2.200
2.200
0.720
0.060
Delta H
(in.
2.
1.
1.
0.
0.
2.
2.
1.
0.
0.
2.
2.
2.
1.
0.
2.
2.
1.
X
0.
2.
1.
1.
0.
0.
H20)
00
80
50
52
04
20
10
70
84'
25
30
30
40
00
28
20
00
50
30
21
10
90
90
61
05
Stack
(F)
190
190
191
191 '
190
188
192
192
193.
191
192
193
194
192
192
192
190
188
187
187
187
190
191
191
189
T Meter T
In(F)
93
92
94
96
96
96
98
101
103
103
102
103
106
108
107
105
106
108
109
110
1C8
109
111
112
111
Out (F)
93
93
93
93
93
94
94
95
95
96
96
97
97
98
99
99
100
100
101
101
102
102
103
103
104
Fraction
DRY CATCH
FILTER
Fraction
PROBE RINSE
CMPINGERS
Final Wt. Tare Wt. Blank Wt. Net Wt
(g) (g) (g> (g)
0.0000 0.0000 0.0000 0.0000
3.3457 3.2909 0.0000 0.0548
Final Wt. Tare Wt.
(g) (g)
3.8842
0.0000
?robe Rinse Blank (mg/ml)=
Cmpinger Blank (mg/ml)= 0.0000
3.8703
0.0000
0,0000
vol.
(ml)
50.6
0.0
Net Wt
(g)
0.0139
0.0000
ICal APPENDIX B
-------
FILE NAME - RUB
RUN # - 11 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1149-1338
PROJECT # - 4702.02.04,09
Initial Meter Volume {Cubic Feet)= 56.158
Final Meter Volume (Cubic Feet)= 118.876
Meter Factor= 0.988
Final Leak Rate (cu ft/min)= 0.003
Net Meter Volume {Cubic Feet)- 61.965
Gas Volume'(Dry Standard Cubic Feet)= 59.526
Barometric Pressure (in Hg)= 30.06
Static Pressure (Inches H20}= -26.45
Percent Oxygen= 5.0
Percent Carbon Dioxide= 14.5
Moisture Collected (ml)"* 188.6
Percent Water= • 13. o
Average Meter Temperature (F)= 94
Average Delta H (in H20)= 1.56
Average Delta P (in H20) = 1.738
Average Stack Temperature (F)= 191
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.89
Average Square Root of Delta P (in H20)= 1.2311
% Isokinetic= 101.3
Pitot Coefficient^ 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.185
Stack Axis #1 (Inches)= , 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,748
Flow Rate (Actual, Cubic ft/min5= 124,032
Flow rate (Standard, Wet, Cubic ft/min)= 94,547
Flow Rate (Standard, Dry, Cubic ft/min)= 82,270
Particulate Loading - Front Half
Particulate Weight (g) = 0.0694
Particulate Loading, Dry Std. {gr/scf)= 0.0180
Particulate Loading, Actual (gr/cu ft)= 0.0119
Emission Rate (lb/hr)= 12.66
No Back Half Analysis
PROG.=VER 06/27/89
07^22^1999 12:11:51
Corr. to 7% 02 & 12% C02
0.0157 0.0149
10
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - RUB
RUN # - 11 - Method 17 TRAIN 3 for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1149-1338
PROJECT # - 4702,02.04.09
Initial Meter Volume (Cubic Meters)= 1.590
Final Meter Volume (Cubic Meters)= 3.356
Meter Factor= 0.9S8
Final Leak Rate (cu m/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1,755
3a.s Volume (Dry Standard Cubic Meters)= 1.686
Barometric pressure (mm Hg)= 764
Static Pressure (mm H20)= . -672
PROG.=VER 06/27/89
07-22-1999 12:11:51
Percent Oxygen= 5 . 0
Percent Carbon Dioxide= 14.5
Moisture Collected (ml)= 188.S
Percent Water= 13.0
Average Meter Temperature (C)= 35
Average Delta H (mm H20)= 39.7
?\verage Delta P (mm H20)= 44.2
Average Stack Temperature (C)= 88
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.89
Average Square Root of Delta P (mm H20)= 6.2048
tr Isokinetic= 101.3
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100,0
Sfozzle Diameter (mm)= 4.70
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Mecers)= 1.448
Rectangular Stack
Stack Area '(Square Meters) = 2.427
Stack Velocity (Actual, m/min}= 1,447
?low rate (Actual, Cubic m/min}= 3,512
Flow rate (Standard, Wet, Cubic m/min)= 2,677
Flow rate (Standard, Dry, Cubic m/min)= 2,330
?articulate Loading - Front Half
Particulate Weight (g)= 0.0694
Particulate Loading, Dry Std. (mg/cu m)= 41.2
Particulate Loading, Actual (mg/cu m)= 27.3
2mission Rate (kg/hr)= 5.75
to Back Half Analysis
Corr.
to 7% 02
3S.O
£.12% C02
34.1
ICal APPENDIX B
11
-------
FILE NAME - RUB
*ROT # - 11 - Method 17 TRAIN B for PM
LOCATION - Unit 2 A Baghouse Outlet Duct
DATE - 07/15/99 Time; 1149-1338
PROJECT # - 4702.02.04.09
PROG.=VER 06/27/89
07-22-1999 12:11:51
Point #
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Delta P
j_
2
2
2
1
0
2
2
1
1
0
2
2
2
0
0
2
2
1
0
0
2
2
2
1
0
n. H20)
.800
.700
.500
.800
.370
.700
.700
.800
.100
.180
.600
.200
.200
.650
.040
.500
.300
.500
.700
.100
.800
.900
.100
.900
.320
Delta H
(in.
2.
2.
2.
1 .
0.
2.
2.
1.
.0.
0.
2.
' 2.
2.
0.
0.
2.
2.
1.
0.
0.
2.
2.
1.
1.
0.
H20)
50
40
20
60
33
40
40
SO
99
16
30
00
00
58
03
30
10
40
64
09
60
60
90
70
29
Stack
(F)
190
191
191
191
191
191
192
192
192
191
193
193
1S4
192
192
192
189
188
187
188
190
191
191
191
189
T Meter T
In(F)
89
89
90
91
92
93
93
94
95
96
95
95
97
98
98
97
97
98
99
99
99
99
100
100
101
Olit
.0130
.0000
12
ICal APPENDIX B
-------
FILE NAME - R12A
RUN # - 12 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1439-1626
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 879.722
Final Meter Volume (Cubic Feet)- 941.593
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.013
Net Meter Volume (Cubic Feet)= 62.653
3as Volume (Dry Standard Cubic Feet}= 58.894
Barometric Pressure (in Hg)= 30.02
Static Pressure (Inches H2Q!= -26.68
Percent Oxygen= 4.5
Percent Carbon Dioxide= 14.8
Moisture Collected (ml)= 206,0
Percent Water= 14.1
Average Meter Temperature (F!= 105
Average Delta H (in H20)= 1.48
Average Delta P (in H20}= 1.676
Average Stack Temperature (F)- 190
Dry Molecular Weight= . 30.55
Wet Molecular Weight= 28.77
Average Square Root of Delta P (in H20)= 1.2083
fc Isokinetic= . 102.1
Pitot Coefficient= 0.84
Sampling Time (Minutes)~ 100.0
Nbzsle Diameter (Inches)= 0.186
Stack Axis #1 (Inches)= . 66.0
Stack Axis #2 {Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/trdn) - 4,669
Flow Rate (Actual, Cubic ft/tnin) = ' 121,987
Flow rate (Standard, Wet, Cubic ft/rain)= 92,982
Flow Rate (Standard, Dry, Cubic ft/min}= 79,830
Particulate Loading - Front Half
Particulate Weight (g)= 0.0810
Particulate Loading, Dry Std. (gr/scf)= 0.0212
Particulate Loading, Actual (gr/cu ft)= 0.0139
Emission Rate (lb/hr)= 14.49
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:12:3!
.Corr. to 7% 02 & 12% C02
0.0180 0.0172
ICal APPENDK B
13
-------
* * METRIC UNITS
FILE NAME - R12A
RIM # - 12 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1439-1628
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)=
Final Meter Volume (Cubic Meters)=
Meter Factor=
Final Leak Rate (cu m/min)=
Net Meter Volume (Cubic Meters)=
Gas Volume (Dry Standard Cubic Meters)=
Barometric Pressure (mm Hg)=
Static Pressure (mm H20)=
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
Average Meter Temperature (C)=
Average Delta H (mm H20)=
Average Delta P (mm H20-) =
Average Stack Temperature (C)=
Dry Molecular Weight=
Wet Molecular Weight=
Average Square Root of Delta P (mm H20)=
% Isokinetic=
Pitot Coefficient=
Sampling Time (Minutes)=
Nozzle Diameter (mm) =
Stack Axis #1 (Meters)=
Stack Axis #2 (Meters)=
Rectangular Stack
•Stack Area (Square Meters)=
Stack Velocity (Actual, m/min) =~
Flow rate (Actual, Cubic m/min)=
Flow rate (Standard, Wet, Cubic m/min)=
Flow rate (Standard, Dry, Cubic m/min)=
Particulate Loading - Front Half
Particulate Weight (g)=
Particulate Loading, Dry Std, (mg/cu m)=
Particulate Loading, Actual (mg/cu m)=
Emission Rate (kg/hr}=
No Back Half Analysis
PROG.=V1R OS/27/89
07-22-1999 12:12:39
24.910
26.565
1.011
0.0004
1.774
1.668
763
-678
4.5
14 .8
206.0
14.1
41
37.7
42.6
88
30.55
28.77
6.0895
102.1
0.84
100.0
4.72
1.676
1.448
2.427
1,423
3,454
2,633
2,261
0.0810
48.6
31.8
6.58
Corr. to 7% 02 & 12% C02
41.2 39.4
14
ICal APPENDIX B
-------
FILE NAME - R12A
RUN # - 12' - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1439-1628
PROJECT # - 4702.02.04.09
Point f
1
2
3
4
5
6
• 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG,=VER 06/27/89
07-22-1999 12:12:39
Delta P
(in. H20)
2.400
2.100
1.900
0.650
0.040
2.500
2.500
1. 900
0,880
0.100
2.600
2.700
2.600
0.990
0,400
2.600
2.600
2.100
1.800
0.300
2 .500
2.400
2.300
0,900
0.140
Delta H
(in. H2Q)
2 .10
1.80
1.70
0.57
0.03
2.20
2 .20
1.70
0.78
0.08
2.30
2.40
2.30
0.88
0.35
2.30
2.30
1.90
1.60
0.26
2.20
2.10
2.10
0.80
0.12
Stack
(F)
192
191
191
189
187
187
188
188
189
187
187
189
190
189
189
189
190
191
191
191
190
192
192
191
190
T Meter T
In(F)
98
98
100
102
103
100
103
106
108
108
loe
108
110
112
112
110
112
113
114
114
112
113
114
115
114
Out (F
98
98
98
98
99
99
B9
100
100
101
102
102
103
103
104
104
105
105
106
106
106
107
107
107
108
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
(g) (g) (g) (g)
o.oooo o.oooo o.oooo o.oooo
3.3954 3.3263 0.0000 0.0691
Final Wt. Tare Wt. Vol. Net Wt,
(g) (g) (ml) (g)
PROBE RINSE 3.5600 3.5481 43.5 0.0119
IMPINGERS 0.0000 0.0000 0.0 0.0000
Probe Rinse Blank (mg/ml)= 0.0000
Impinger Blank (mg/ml)= 0.0000
ICal APPENDIX B
15
-------
FILE NAME - R12B
RUN # - 12 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1441-1630
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet}= 119.105
Final Meter Volume (Cubic Feet)= 179.978
Meter Factor= 0.988
Final Leak Rate (cu ft/min)• 0.005
Net Meter Volume (Cubic Feet)= 6D.143
Gas Volume (Dry Standard Cubic FeetS= 57,243
Barometric Pressure (in Hg) = 30.02
Static Pressure (Inches H205= -26.68
Percent Qxygen= ' 4.5
Percent Carbon Dioxide* 14.8
Moisture Collected (ml)= 211.0
Percent Water= 14.8
Average Meter Temperature (F)= 98
Average Delta H (in H20)= 1.49
Average Delta P (in H20)= 1.675
Average Stack Temperature (F)= 190
Dry Molecular' Weight= 30.55
Wet Molecular Weight= 28,69
Average Square Root of Delta P (in H20)= 1.204Q
% Isokinetic= 102.5
Pitot Coefficient= 0.84
Sampling Time (Minutes)» 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis fl (Inches)= . ' 66.0
Stack Axis #2 (Inches)= . 57.0
Rectangular Stack
Stack Area (Square Feet)= ' 26.13
Stack Velocity (Actual, Feet/min)= 4,662
Flow Rate (Actual, Cubic ft/min)= 121,795
Flow rate (Standard, Wet, Cubic ft/min)= 92,739
Flow Rate (Standard, Dry, Cubic ft/min)= 79,020
Particulate Loading - Front Half
Particulate Weight (g)= O.Q819
Particulate Loading, Dry Std. (gr/scf)= 0.0220
Particulate Loading, Actual (gr/cu ft)= 0.0143
Emission Rate (lb/hr}= 14.92
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:13:32
Corr. to 7% O2 & 12% C02
0.0187 0.0179
16
ICal APPENDK B
-------
* * METRIC UNITS * *
FILE NAME - R12B
RUN ft - 12 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Bagiiouse Outlet Duct
DATE - 07/15/99 Time; 1441-1630
PROJECT # - 4702.02.04.09
Initial Meter Volume {Cubic Meters)= 3,373
Final Meter Volume (Cubic Meters)= 5.096
Meter Factor= 0.988
Final Leak Rate (cu m/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1.703
3as Volume (Dry Standard Cubic Meters)= 1.621
Barometric Pressure (mm Kg)= 7S3
Static Pressure (mm H20)= • -678
Percent Oxygen= 4 .5
Percent Carbon Dioxide= 14.8
Moisture Collected (ml}= 211.0
Percent Water= ' 14.8
Average Meter Temperature (C)= 37
Average Delta H (mm H20)= 37.8
Average Delta P (mm H20}= 42.5
Average Stack Temperature (C)= 88
Dry Molecular Weight= 30.55
«?et Molecular Weight= 28.69
\verage Square Root of Delta P (mm H20)= 6.0681
'•s Isokinetie= 102.5
Pitot Coefficients 0.84
sampling Time {Minutes)= 100.0
tozzle Diameter (mm)= 4.67
Stack Axis #1 (Meters)= ' 1.676
Stack Axis #2 (Meters3= 1.448
Rectangular Stack
stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,421
?low rate (Actual, Cubic m/min)= 3,449
flow rate (Standard, Wet, Cubic m/min)= 2,626
••low rate (Standard, Dry, Cubic m/min) = 2,238
'articulate Loading - Front Half
'articulate Weight (g)= 0.0819
'articulate Loading, Dry Std. {mg/cu m)= 50.5
?articulate Loading, Actual (mg/cu m)- 32.8
Emission Rate (kg/hr)= 6.77
Jo Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:13:32
Corr. to 7% O2
42.9
& 12% CO2
41.0
ICal APPENDK B
-------
FILE NAME - R12B
RUN # - 12 - Method 17 TRAIN B for PM
LOCATION ~ Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1441-1S30
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
• 7
8
9
10
11
12
13
14
15
16
17
18
• 19
20
21
22
23
24
25
Fraction
DRY CATCH •
FILTER
Fraction
PROBE RINSE
IMPINGERS
Impinger Blank (mg/ml)= 0.0000
PROG,=VER 06/27/89
07-22-1999 12:13:32
Delta
P Delta H
in. H203 (in. H20)
2.700
2.600
2.400
l.QOO
0.270
2.600
2.200
2.000
1.100
0.180
2.400
2.100
2.100
0 .700
0.040
2.600
2.600
1.600
0.920
0.100
2.700
2.800
2.100
1.900
0.160
Blank
2.40
2.30
2.10
0.88
0.24
2.30
2.00
1.80
0.90
0.16
2.10
1.90
1.90
0.62
0.03
2.30
2.30
1.40
0.82
0.08
2 .40
2.50
1.90
1.70
0.14
Final Wt.
(g)
0.0000
3.4181
Final Wt .
(g)
4.0235
0.0000
( mg/ml }= 0.
Stack
(F)
194
191
191
189
188
187
188
188
188
188
189
190
'190
190
190
191
191
191
191
191
193
193
192
192
191
Tare Wt
(g)
0.0000
3.3451
Tare Wt
(g)
4.0146
0.0000
0000
T Meter
IniF} Out
94
94
95
96
97
97
97
99
100
100
100
100
101
102
102
101
101
102
103
103
102
102
104
104 1
104 1
. Blank Wt.
(g)
o.ocoo
0.00 00
Vol.
[ml)
38.2 0
0.0 0
T
(F)
94
94
94
94
94
95
95
95
95
96
97
96
97
97
98
98
98
98
99
99
99
99
99
00
00
Net Wt
(g)
0.0000
0.0730
Net Wt
(g)
.0089
.0000
18
ICal APPEKTOX B
-------
FILE NAME - R13A
RON # - 13 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/39 Time: 0905-1055
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 942.875
Final Meter Volume (Cubic Feet)= 1001.400
Xfeter Factor- 1.011
Final Leak Rate (cu ft/min)= 0.008
Set Meter Volume (Cubic Feet)= 59.169
3as Volume (Dry Standard Cubic Feet)= • 57.629
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20)= -27.il
Percent Oxygen= 5.8
Percent Carbon Dioxide= 13.6
Moisture Collected (ml)= ' 165.6
Percent Water= 11.9
Average Meter Temperature (F)= • 86
Average Delta H (in H20)= 1.38
Average Delta P (in H20}= 1.685
Average Stack Temperature (F)= 186
Dry Molecular Weight= 30.41
ifet Molecular Weight- 28.93
Average Square Root of Delta P (in H20}= 1.2064
\ Isokinetic= 99.7
Pitot Coefficients 0.84
Sampling Time (Minutes)= 100.0
Sozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= ' 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,637
Flow Rate (Actual, Cubic ft/min)= 121,151
Flow rate (Standard, Wet, Cubic ft/min]= 92,838
Flow Rate (Standard, Dry, Cubic ft/rain}= 81,771
Particulate Loading - Front Half
Particulate Weight (g)- 0.0284
Particulate Loading, Dry Std. (gr/scf)= 0.0076
Particulate Loading, Actual (gr/cu ft)= 0.0051
Emission Rate (lfc/hr)= 5.32
No Back Half Analvsis
PROG.=VER 06/27/89
07-22-1999 12:14:26
Corr. to 7% 02 & 12% CO2
0.0070 0.0067
ICal APPENDIX B
19
-------
* * METRIC UNITS * *
FILE NAME - R13A
RIOT # - 13 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 0905-1055
PROJECT f - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= ' 26.698
Final Meter Volume (Cubic Meters)= 28.356
Meter Factor^ 1.011
Final Leak Rate (cu m/min!= 0.0002
Net Meter Volume (Cubic Meters)= 1.675
Gas Volume {Dry Standard Cubic Meters)= 1.632
Barometric Pressure (mm Hg)= • 763
Static Pressure (ram H20) = . -689
Percent Oxygen= 5.8
Percent Carbon Dioxide= 13.6
Moisture Collected (ml)= 165,5
Percent Water= 11.9
Average Meter Temperature (C)= • 30
Average Delta H (mm H20)= ' 35.0
Average Delta P (mm H20)= 42.8
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.41
Wet Molecular Weight= 28.93
Average Square Root of Delta P (mm H20)= 6.0802
% Isokinetic= • 99.7
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (ram)= 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)- • 2.427
Stack Velocity (Actual, m/min)= • 1,413
Flow rate (Actual, Cubic m/min)= 3,431
Flow rate (Standard, Wet, Cubic m/min)= 2,629
Flow rate (Standard, Dry, Cubic m/min)= 2,315
Particulate Loading - Front Half
Particulate Weight (g)- 0.0284
Particulate Loading, Dry Std. (mg/cu m)= 17.4
Particulate Loading, Actual (mg/cu m) « 11.7
Emission Rate (kg/hr)= 2.41
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:14:26
Corr.
to 7% O2
16.0
12% C02
15.4
20
ICal APPENDIX B
-------
FILE NAME - R13A
R.UN # - 13 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time:^0905-1055
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:14:26
Delta P
(in. H20)
2,400
2.200
1.700
0.510
0.030
2.100
2.200
2.000
0.830
0.100
2.900
2.800
2.700
1.700
0.260
2.700
2.800
2.400
1.500
0.300
2.SOO
2.300
2.000
0.950
0.140
Delta H
(in. H20)
2.00
1.80
1.40
0.41
0.02
1.70
1.80
1.60
0.68
0.08
2.40
2.30
2.20
1.40
0.21
2.20
2.30
2.00
1,20
0.24
2.10
1.90
1,60
0.78
0.11
Stack
(F)
183
181
183
184
185
184
IBS
184
185
184
184
186
185
184
183
183
183
182
184
187
191
195
193
194
194
T
If "^ \
n (c i
77
77
79
81
82
81
83
86
88
88
85
88
91
93
93
90
92
94
95
96
94
95
98
98
98
Meter T
Out (F
77
77
77
78
78
78
79
80
81
81
82
82
83
83
84
85
85
8S
86
87
87
88
89
89
90
rraction
DRY CATCH
^ILTER
fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3016 3.2780 0.0000 0.0236
Final Wt. Tare Wt. Vol.
(g) (g) (ml)
'ROBE RINSE 3.9103 3.9055 41,8
:MPINGERS o.oooo o.oooo o.o
'robe Rinse Blank (mg/ml)= 0.0000
Impinger Blank Emg/ml)= 0.0000
Net Wt,
-------
FILE NAME - RI3B
RUN # - 13 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 0907-1057
PROJECT # - 4702,02.04,09
Initial Meter Volume (Cubic Feet)= 193.304
Final Meter Volume (Cubic Feet)* 253.291
Meter Factor= 0.988
Final Leak Rate (cu ft/min)« 0.003
Net Meter Volume (Cubic Feet)= 59.267
Gas Volume (Dry Standard Cubic Feet)= 57.813
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20}= -27.11
Percent Oxygen= 5 . 8
Percent Carbon Dioxide= 13.6
Moisture Collected (ml)= 165.2
Percent Water= 11.9
Average Meter Temperature (F)= 85
Average Delta H (in H20)= 1.49
Average Delta P (in H20)= 1.674
Average Stack Temperature (F) = 187
Dry Molecular Weight= 30.41
Wet Molecular Weight= 28.94
Average Square Root of Delta P (in H20}= 1.2018
% Isokinetic= 99.4
Pitot Coefficient= 0.84
Sampling Time (Minutes)- 100.0
Nozzle Diameter (Inches)= 0.185
Stack Axis #1 (Inches)= . 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,623
Flow Rate (Actual, Cubic ft/min)= 120,778
Flow rate (Standard, Wet, Cubic ft/min)= 92,393
Flow Rate (Standard, Dry, Cubic ft/min)= 81,433
Particulate Loading - Front Half
Particulate Weight (g)= 0.0279
Particulate Loading, Dry Std. (gr/scf)= 0.0074
Particulate Loading, Actual (gr/cu ft)= 0.0050
Emission Rate (Ib/hr)- 5.19
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:15:12
Corr. to 7% O2
0.0068
& 12% C02
0.0066
22
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R13B
RUN If - 13 - Method 17 TRAIN E for PM
LOCUTION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 0907-1057
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 5.474
Final Meter Volume (Cubic Meters)= 7.172
Meter Factor** 0.988
Final Leak Rate (cu m/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1.678
3as Volume (Dry Standard Cubic Meters)= 1.637
Barometric Pressure (mm Hg)» 763
Static Pressure (mm H20)= -689
PROG.=VER 06/27/89
07-22-1999 12:15:12
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml}=
Percent Water=
5 . 8
13 . 6
165.2
11.9
Average Meter Temperature (C)= 30
^•verage Delta H (mm H20)= 37.8
Average Delta P (mm H20}= 42.5
Average Stack Temperature (C)= 86
Dry Molecular weight= 30.41
Afet Molecular Weight= 28.94
Average Square Root of Delta P (mm H20}= 6.0571
I Isokinetic= 9S.4
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Mozzle Diameter (mm)= 4.70
Stack Axis #1 (Meters)= 1,676
3tack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,409
Flow rate (Actual, Cubic m/rain)= 3,420
Flow rate (Standard, Wet, Cubic m/min}= 2,616
Flow rate (Standard, Dry, Cubic m/min)= 2,306
Particulate Loading - Front Half
Particulate Weight (g)= 0.0279
Particulate Loading, Dry Std. (mg/cu m)= 17.0
Particulate Loading, Actual (mg/cu m}= 11.5
Emission Rate (kg/hr)= 2.35
So Back Half Analysis
Corr. to 7% 02 &. 12% C02
15.7 15.0
IGal APPENDIX B
23
-------
FILE NAME - R13B
RUN ft - 13 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 0907-1057
PROJECT ft - 4702.02,04.09
Point #
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
IS
17
IB
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:15:12
Delta P
(in. H20)
2.800
2.200
2.000
1.000
0.220
2.100
2,100
1.700
0.750
0.180
2.600
2.300
2.000
0.720
0.040
2.700
2.600
2.400
0.830
0.180
2.700
2.900
2.600
2.100
0.140
Delta H
(in
2
1
1
0
0
1
1
1
m
1
0
0
2
2
1
0
0
2
2
2
0
0
*-i
<£
2
2
J_
0
. H2 0 }
.50
.90
.80
.87
.19
.90
.90
.50
.66
.14
.30
.00
.80
.64
.03
.40
.30
.20
.74
.16
.40
.60
.30
.90
.12
Stack
(P)
183
183
185
186
185
135
135
IBS
185
185
185
186 .
134
184
183
1S3
183
185
186
191
198
195
195
196
194
T Meter T
In(F)
77
77
78
79
SO
81
SI
83
85
B6
85
86
88
89
90
89
90
92
93
94
93
94
95
98
98
Out (F)
76
76
77
77
77
79
79
79
80
81
82
82
83
84
85
86
85
86
87
88
89
89
90
91
92
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.2835 3.2596 O.COOO 0.0239
Final Wt
(g)
PROBE RINSE 3.5891
IMPINGERS 0.0000
Probe Rinse Blank {mg/ml}=
Tare Wt.
(g)
3 .5851
0.0000
0.0000
Vol.
(ml)
36.7
0.0
Net wt,
(g)
0.0040
0.0000
Irapinger Blank (tng/ml}= 0.0000
24
ICal APPENDIX B
-------
FILE NAME - R14A
RUN # - 14 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Eaghouse Outlet Duct
DATE - 07/16/99 Time: 1211-1400
PROJECT # - 4702,02.04.09
Initial Meter Volume (Cubic Feet}= 1.518
Final Meter Volume (Cubic Feet}= 62.188
Meter Faetor= 1.011
Final Leak Rate (cu ft/min)= 0.005
Net Meter Volume (Cubic Feet)= 61.23S
3as Volume (Dry Standard Cubic Feet}= 58.444
Barometric Pressure [in Hg)= 30.06
Static Pressure (Inches H20)= -25.81
Percent Oxygen= 4. 7
Percent Carbon Dioxide= 14 . 6
Moisture Collected (ml)= 186.8
Percent Water= 13.1
Average Meter Temperature (F)= ' 98
Average Delta H (in H20)= 1,46
Average Delta P (in H20)= 1.672
Average Stack Temperature EF)= 192
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.89
iverage Square Root of Delta P (in H20}= 1.2034
I Isokinetic= 100.7
Pitot Coefficients 0.84
Sampling Time (Minutes)= 100,0
Nozzle Diameter {Inches)= 0.186
Stack Axis #1 (Inches>= 66.0
Stack Axis #2 (Inches)- 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/rain)= 4,642
Flow Rate (Actual, Cubic ft/'min) = 121,263
Flow rate (Standard, Wet, Cubic ft/rain)= 92,420
?low Rate (Standard, Dry, Cubic ft/min)= 80,327
?articulate Loading - Front Half
?articulate Weight (g>= 0.0337
Particulate Loading, Dry Std. (gr/scf)= 0.0089
Particulate Loading, Actual (gr/cu ft)= 0.0059
3mission Rate (lb/hr)= .6.11
So Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:15:57
Corr. to 7% O2 &• 12% C02
0.0076 0.0073
ICaJ APPENDIX B
25
-------
* * METRIC UNITS •* *
FILE NAME - R14A
RUN # - 14 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 1211-1400
PROJECT # - 4702.02.04,09
Initial Meter Volume (Cubic Meters)= 0.04S
Final Meter Volume (Cubic Meters)= 1.761
Meter Factor= l.on
Final Leak Rate (cu m/rrtin) = 0.0001
Net Meter Volume (Cubic Meters)= 1.734
Gas Volume (Dry Standard Cubic Meters)= 1.655
Barometric Pressure (mm Hg)= 764
Static Pressure (mm H20)= -656
PROG.=VER 06/27/89
07-22-1999 12:15:57
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
4.7
14.6
186.8
13.1
Average Meter Temperature (C)= 36
Average Delta H (mm H2Q) = 37.1
Average Delta P (mm H20}= 42.5
Average Stack Temperature (C)= 89
Dry Molecular Weight= .30.52
Wet Molecular Weight= 28.89
Average Square Root of Delta P (ram H20)= 6.Q64B
% Isokinetic= 100.7
Pitot Coefficient** 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm) = . 4.72
Stack Axis #1 (Meters!- 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,415
Flow rate (Actual, Cubic m/min)= 3,434
Flow rate (Standard, Wet, Cubic m/min)= 2,617
Flow rate (Standard, Dry, Cubic m/min)= 2,275
Particulate Loading - Front Half
Particulate Weight (g}= 0.0337
Particulate Loading, Dry Std. (mg/cu m)= 20.4
Particulate Loading, Actual (mg/cu ra)= 13.5
Emission Rate (kg/hr)~ 2.78
No Back Half Analysis
Corr. to 7% O2 & 12% C02
17.5 16.7
26
ICal APPENDIX B
-------
FILE NAME - R14A
RUN # - 14 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE -. 07/15/99 Time: 1211-1400
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:15:57
Delta P
in. H20)
2
2
1
0
0
2
2
2
0
0
2
2
2
1
0
2
2
2
1
0
2
2
2
0
0
.400
.100
.800
.630
.030
.300
.400
.200
.720
.100
.600
.500
.700
.200
.300
.700
.700
.000
.900
.330
.600
.300
.300
.880
.120
Delta H
(in.
2.
i.
1.
0 .
0 .
2.
2.
-i
,L (
0.
0.
2.
2,
2 .
1.
0.
2.
2.
1.
1.
0.
2.
2.
2.
0.
0.
H20)
10
80
60
54
02
00
10
90
62
OS
30
20
40
00
26
40
40
70
70
28
30
00
00
76
10
Stack
(F)
191
191
191
191
189
189
190
190
190
189
190
190
191
191
191
191
193
194
195
195
194
197
197
197
195
T Meter T
In(F)
91
91
93
95
95
93
96
99
100
100
96
100
102
104
104
102
103
106
106
107
104
105
107
109
107
Out (F)
90
90
91
91
91
91
92
93
92
93
93
94
94
95
95
96
95
97
97
98
98
98
99
100
100
Fraction
DRY CATCH
FILTER
fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g> Cg) (gl (g)
0,0000 0.0000 0.0000 0.0000
3.3091 3.2797 0.0000 0.0294
Final Wt. Tare Wt. Vol. Net Wt,
(g) (g) (ml) (g)
?ROBi RINSE 3.4393 3.4350 35.4 0.0043
EMPINGERS 0.0000 0.0000 0.0 0.0000
Probe Rinse Blank (mg/ml)= 0.0000
Empinger Blank (rag/ml)= 0.0000
ICal APPENDIX B
27
-------
FILE NAME - R14B
RUN # - 14 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1213-1402
PROJECT t - 4702.02.04.09
Initial Meter Volume (Cubic Feet}= 253,506
Final Meter Volume (Cubic Feet}= 314.949
Meter Factor** 0.988
Final Leak Rate (cu ft/min)= 0.001
Net Meter Volume (Cubic Feet)= 60.706
Gas Volume (Dry Standard Cubic Feet)= 57.S67
Barometric Pressure (in Hg)= ' 30.06
Static Pressure (Inches H20)= -25.81
Percent Oxygen= 4 . 7
Percent Carbon Dioxide= 14.6
Moisture Collected (ml}= 190.1
Percent Water= 13.4
Average Meter Temperature (F)= 100
Average Delta H (in H20)« 1.51
Average Delta P (in. H20}= 1.S97
Average Stack Temperature (F)= 193
Dry Molecular Weight= ' 30.52
Wet Molecular Weight= . 28.84
Average Square Root of Delta P (in H20}= 1.2156
% Isokinetic= 100.9
Pitot Coefficients . 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= . 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet}= 26.13
Stack Velocity (Actual, Feet/min)= 4,695
Flow Rate (Actual, Cubic ft/min)= 122,652
Flow rate (Standard, Wet, Cubic ft/min}= 93,382
Flow Rate (Standard, Dry, Cubic ft/ndn}« 80,831
Particulate Loading - Front Half
Particulate Weight (g)= . 0.0356
Particulate Loading, Dry Std. (gr/scf)= 0.0095
Particulate Loading, Actual (gr/cu ft}= 0,0063
Emission Rate (Ib/hr)= 6.59
Ho Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:16:45
Corr. to 7% 02 & 12% C02
0.0082 0.0078
28
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R14B
RUN # - 14 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time': 1213-1402
PROJECT i - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 7.178
Final Meter Volume (Cubic Meters)= 8,918
Hater Factor= 0.988
Final Leak Rate (cu m/min)= O.OOCO
Net Meter Volume (Cubic Meters)= 1.719
Gas Volume (Dry Standard Cubic Meters)= 1.633
Barometric Pressure (mm Hg)= 764
Static Pressure (mm H20) = -656
Percent Oxygen= 4 , 7
Percent Carbon Dioxide= 14.6
Moisture Collected (ml5= 190.1
Percent Water= 13.4
Average Meter Temperature (C}= 38
Average Delta H (mm H20)= 33.3
Average Delta P (mm H20}= 43.1
Average Stack Temperature (C)= 89
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.84
Average Square Root of Delta P (mm H20)= 6.1263
% Isokinetic= 100.9
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= . 4.67
Stack Axis #1 (Meters)= 1.S76
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area'(Square Meters)=' 2.427
Stack Velocity (Actual, m/min)= 1,431
Flow rate (Actual, Cubic m/min)= 3,473
Flow rate (Standard, Wet, Cubic m/min)= 2,644
Flow rate (Standard, Dry, Cubic m/min)= • 2,289
Particulate Loading - Front Half
Particulate Weight (g)= 0.0356
Particulate Loading, Dry Std. (mg/cu m)= 21.8
Particulate Loading, Actual (mg/cu m)= 14.4
Emission Rate (kg/hr)= 2.99
No Back Half Analysis
PROG.-VER 06/27/89
07-22-1999 12:16:46
Corr. to 7% O2 & 12% C02
18.7 17.9
ICal APPENDIX B
29
-------
FILE NAME - R14B
RUN # - 14 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/15/99 Time: 1213^1402
PROJECT # - 4702.02.04.09
Point
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:16:46
Delta P
(in. H20)
2.700
2 .700
2.000
1.800
0.300
2.500
2.300
1.800
1.000
0.160
2.400
2.100
2,000
0.620
0.030
2.600
2.300
1.900
0.950
0.120
2.800
3.000
2.100
2.000
0.240
Delta H
(in. H20)
2.40
2.40
1.80
1.60
0.26
2.20
2.00
1.60
O.B8
0.14
2.10
1.90
1.80
0.55
0.02
2.30
2.00
1.70
0.84
0.10
2.50
2.70
1.90
1.80
0.21
Stack
(F)
191
192
191
191
190
190
190
190
190
189
190
190
191
191
192
193
194
195
195
197
198
198
197
198
196
T Meter T
In(P)
94
94
95
9S
98
9B
93
100
101
101
ICO
101'
103
104
104
103
104
105
IDS
107
105
106
103
109
110
Out (F)
93
93
94
94
94
95
95
96
96
97
98
98
98
99
99
100
100
101
102
102
103
103
103
104
105
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt . Net Wt ,
Eg) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.350S 3.3197 0.0000 0.0309
Final Wt . Tare Wt .
(g) (g)
PROBE RINSE 3,7862 3.7815
IMPING1RS 0.0000 0,0000
Probe Rinse Blank (mg/ml)= 0.0000
Irapinger Blank (mg/ml}= 0.0000
Vol.
(roll
38.0
0.0
Net Wt.
(g)
0.0047
0.0000
30
ICal APPENDIX B
-------
FILE NAME - R15A
RIM # - 15 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 1543-1732
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 63.282
Final Meter Volume (Cubic Feet)= 124.231
Meter Factor= 1,011
Final Leak Rate {cu ft/min)= O.OQ3
STet Meter Volume (Cubic Feet}= 61.619
3as Volume (Dry Standard Cubic Feet)= 58.381
Barometric Pressure (in Hg)= 30.00
Static Pressure (Inches H20)= -26.41
Percent Qxygen= 4.7
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 184.7
Percent Water= 13 . 0
Average Meter Temperature. (F)= 101
Average Delta H (in H20)= 1.46
Average Delta P (in H20}= . 1.738
Average Stack Temperature (F)= • 186
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.90
Average Square Root of Delta P (in H20}= 1.2255
k Isokinetic= 100.6
Pitot Coefficient= • 0.84
Sampling Time (Minutes)= 100.0
Sozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet}= 26.13
Stack Velocity (Actual, Feet/minJ= 4,713
Flow Rate (Actual, Cubic ft/miri)= 123,138
Flow rate (Standard, Wet, Cubic ft/min)= 94,347
Flow Rate (Standard, Dry, Cubic ft/min)= 82,112
Particulate Loading - Front Half
Particulate Weight (g)= 0.0369
Particulate Loading, Dry Std. (gr/scf)= 0.0097
Particulate Loading, Actual (gr/cu ft)= 0.0065
Emission Rate (lb/hr)= 6.85
So Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:20:58
Corr. to 7% O2 & 12% C02
0.0084 0.0080
ICal APPENDIX B'
31
-------
* * METRIC UNITS * *
FILE NAME - R15A
RUN # - 15 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 1543-1732
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 1.792
Final Meter Volume (Cubic Meters)= 3.518
Meter Factor= . 1.011
Final Leak Rate (cu m/min)= . 0.0001
Net Meter Volume (Cubic Meters)= 1.745
Gas Volume (Dry Standard Cubic Meters)= 1.653
Barometric Pressure (mm Hg)» 762
Static Pressure (mm H20)= -671
PROG.=V£R 06/27/89
07-22-1999 12:20:58
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (nil) =
Percent Waters
4.7
14.6
184.7
13.0
Average Meter Temperature (C)= 38
Average Delta H (mm H20)= 37.2
Average Delta P {mm H20)= 44.2
Average Stack Temperature (C)= 86
Dry Molecular Weight= 30.52
Wet Molecular Weight= ' 28.90
Average Square Root of Delta P (mm H20)= 6.1764
% Isokinetic= 100.6
Pitct Coefficient- 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter !mm)= , 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,437
Flow rate (Actual, Cubic m/min)= 3,487
Flow rate (Standard, Wet, Cubic ra/tnin) = 2,672
Flow rate (Standard, Dry, Cubic m/min)= 2,325
Particulate Loading - Front Half
Particulate Weight (g)= 0.0369
Particulate Loading, Dry Std. (mg/cu m)= 22.3
Particulate Loading, Actual (mg/cu m)= 14.9
Emission Rate (kg/hr)= 3.11
No Back Half Analysis
Corr, to 7% 02
19.2
& 12% C02
18.3
32
ICal APPENDIX B
-------
FILE NAME - R15A
RUN # - 15 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 1543-1732
PROJECT # - 4702.02.04.09
Point f
1
2
3
4
5
5
. 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:20:58
Delta P
; in , H2 0 }
2.000
2.500
2.200
0.800
0.040
2.600
2.600
1.700
0.900
0.120
2.700
2.900
2.900
1.900
0.240
2.800
2.700
2.300
1.400
0.280
2.500
2 .300
2.100
0.900
0.080
Delta H
(in. H2Q)
1.70
2.10
1.80
0.67
0.03
2.20
2.20
1.40
0.75
0.10
2.30
2.50
2.40
1.60
0.20
2.40
2.30
1.90
1.20
0.23
2.10
1.90
1.80
0.76
0.06
Stack
(F)
185
186
187
187
186
186
186
187
188
186
186
185
187
188
187
184
185
186
186
186
186
186
186
187
187
T
In{F)
99
98
98
100
100
98
102
104
105
103
101
102
104
105
IDS
103
104
105
105
105
102
104
105
10S
105
Meter T
Out (F)
99
98
97
98
98
97
98
98
98
98
98
98
98
98
99
99
98
98
99
99
99
99
99
99
99
Fraction
DRY CATCH
FILTER
Fraction
PROBE RINSE
IMPINGERS
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
o.oooo o.oooo o.oooo o.oooo
3.4018 3.3723 0.0000 0.0295
Final Wt.
(g)
3.7163
0.0000
Tare Wt. Vol.
Probe Rinse Blank (mg/ml)=
Impinger Blank £mg/ml)= 0.0000
(g)
3.7089
0.0000
0.0000
(ml)
37.0
0.0
Net Wt,
(g)
0.0074
0.0000
ICa! APPENDIX B
33
-------
FILE NAME - R15B
RUN # - 15 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghcmse Outlet Duct
DATE - 07/16/99 Time: 1545-1734
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 315.155
Final Meter Volume (Cubic Feet)- 379.115
Meter Factor= ' 0.988
Final Leak Rate (cu ft/min)= 0.001
Net Meter Volume (Cubic Feet)= 63.192
Gas Volume {Dry Standard Cubic Feet}= 59.5S5
Barometric Pressure (in Hg) = 30.00
Static Pressure (Inches H20}= -26.41
Percent Oxygen= 4 .7
Percent Carbon Dioxide= 14.6
Moisture Collected (ml}= 193.0
Percent Water= 13.2
Average Meter Temperature (F) = 104
Average Delta H (in H20)= 1.62
Average Delta P (in H20) = 1.762
Average Stack Temperature (F)= 187
Dry Molecular Weight = 30.'52
Wet Molecular Weight= 28.87
Average Square Root of Delta P (in H20)= 1.2370
% Isokinetic= . 100.9
Pitot Coefficients ^ 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.185
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,762
Flow Rate (Actual, Cubic ft/min)= 124,396
Flow rate (Standard, Wet, Cubic ft/min)= 95,258
Flow Rate (Standard, Dry, Cubic ft/rain)= 82,645
Particulate Loading - Front Half
Particulate weight (g)= 0.0357
Particulate Loading, Dry Std. (gr/scf)= 0.0092
Particulate Loading, Actual (gr/cu ft)= 0.0061
Emission Rate (lb/hr)= 6.54
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:54:00
Corr. to 7% O2 & 12% C02
0.0079 0.0076
34
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R15B
RUN # - 15 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/1S/99 Time: 1545-1734
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters )= 8,924
Final Meter Volume (Cubic Meters) = 10.735
feter Factor= 0.988
Final Leak Rate (eu m/min) - 0.0000
Set Meter Volume (Cubic Meters )- 1.789
3as Volume (Dry Standard Cubic Meters) = 1,687
Barometric Pressure (mm Hg) = 762
Static Pressure (mm H20}= -671
Percent Oxygen= 4 , 7
Percent Carbon Dioxide= 14.6
yioisture Collected (ml)= 193.0
Percent Water= ' 13.2
Average Meter Temperature (C) = 40
Average Delta H (mm H20)= 41.1
Average Delta P (mm H20}= 44.8
Average Stack Temperature (C) = 86
Dry Molecular Weight= 30.52
(Jet Molecular Weight= 28.87
Average Square Root of Delta P (ram H20}= 6.2341
' - 4.70
Stack Axis #1 (Meters) « 1.676
Stack Axis #2 (Meters) = ' 1.448
Rectangular Stack
Stack Area (Square Meters) = - 2.427
Stack Velocity (Actual, m/min) = 1,451
Plow rate (Actual, Cubic m/min) = 3,523
?low rate (Standard, Wet, Cubic m/min) = 2,697
Flow rate (Standard, Dry, Cubic m/min) = 2,340
Particulate Loading - Front Half
Particulate Weight (g) = 0.0357
Particulate Loading, Dry Std. (mg/cu m) = 21.2
Particulate Loading, Actual (mg/cu m) = 14,1
2mission Rate (kg/hr) = 2.97
So Back Half Analysis
Corr. to 7% O2 & 12% CO2
18.2 17,4
ICal APPENDIX B
35
-------
FILE NAME - R15B
RIM # - 15 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/16/99 Time: 1545-1734
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:54:00
Delta P
in. H2Q)
2
2
2
1
0
2
2
2
0
0
2
2
2
0
0
2
2
2
0
0
2
2
2
1
0
.700
.500
,500
.500
.220
.700
.400
.000
,830
.180
.500
.400
.000
.720
.060
.800
,700
.300
,730
.120
.700
.800
.700
,700
.300
Delta H
(in.
2.
2.
2.
1.
0.
2.
2.
1,
0.
0,
2,
2.
1.
0.
0.
2.
2.
2.
0,
0.
2.
2.
2.
1.
0.
H20)
50
30
30
40
20
50
20
80
76
16
30
20
80
€6
05
50
50
10
67
11
50
60
50
60
27
Stack
(F)
186
187
188
187
135
136
1B7
1S8
187
186
186
186
187
187
166
185
186
187
187
187
186
186
1S7
187
187
T Meter T
In(P)
101
101
102
102
103
103
103
105
106
106
105
104
106
107
107
105
105
106
107
107
106
105
107
108
109
Out (F)
101
101
101
101
100
101
101
101
102
102
102
102
102
103
103
103
102
103
103
103
104
103
104
104
105
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt
(g) (g) Cg) (g)
0.0000 0.0000 0.0000 0.0000
3.3467 3.3144 0.0000 Q..Q323
Final Wt. Tare Wt. Vol. Net Wt
(g) {g5 (ml) (g)
PROBE RINSE ' 3.6S07 3.6873 42.5 0.0034
1MPIHGERS 0.0000 0.0000 0,0 0.0000
Probe Rinse Blank (nig/ml) = 0.0000
Irapinger Blank (mg/ml) = '0.0000
36
ICal APPENDIX B
-------
FILE NAME - R16A
RUN # - 16 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 0851-1041
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 124.784
Final Meter Volume (Cubic Feet)= 192.882
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.009
Net Meter Volume (Cubic Feet)= 68.847
Gas Volume (Dry Standard Cubic Feetj= 66.648
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20)= -26.68
PROG.=VER 06/27/83
07-22-1999 12:54:46
Percent Qxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
5.1
14.6
217.1
13.3
Average Meter Temperature (F)= 90
Average Delta H (in H20}= 1.86
Average Delta P (in H20)= 1.745
Average Stack Temperature (F)= 185
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.87
Average Square Root of Delta P (in H20)= '1.2328
I Isokinetic= 100.8
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
tozzle Diameter (Inches)= 0.196
Stack Axis $1 (Inches)= 66.0
Stack Axis #2 {Inches)= 57.0
Rectangular Stack
Stack Area {Square Feet>= 26.13
Stack Velocity (Actual, Feet/min)= 4,738
Flow Rate (Actual, Cubic ft/min)= 123,784
Flow rate (Standard, Wet, Cubic ft/rain)= 95,069
Flow Rate (Standard, Dry, Cubic ft/min)= 82,423
Particulate Loading - Front Half
Particulate Weight (g)= 0.0086
Particulate Loading, Dry Std. (gr/scf}= 0.0020
Particulate Loading, Actual (gr/cu ft) = 0.0013
Smission Rate (lb/hr)= 1.40
tfo Back Half Analysis
Corr. to 7% O2 & 12% C02
0.0017 0.0016
KM APPENDIX B
37
-------
* * METRIC UNITS * *
FILE NAME - R16A
RIOT # - 16 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 0851-1041
PROJECT # - 4702.02,04,09
Initial Meter Volume {Cubic Meters)= 3.533
Final Meter Volume (Cubic Meters)= 5.452
Meter Factor= 1.011
Final Leak Rate (cu m/rain)= 0.0003
Net Meter Volume (Cubic Meters)- 1.949
Gas Volume (Dry Standard Cubic Meters)= 1.887
Barometric Pressure (mm Hg)= 763
Static Pressure (mm H20)= -678
Percent Oxygen= 5 .1
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 217.1
Percent Water= 13.3
Average Meter Temperature (C)= 32
Average Delta H (mm H20)= 47.1
Average Delta P (mm H20)= 44.3
Average Stack Temperature (C) = . 85
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.87
Average Square Root of Delta P (mm H20)= S.2133
% Isokinetic= . 100.8
Pitot Coefficient^ 0.84
Sampling Time (Minutes!= 100.0
Nozzle Diameter (mm)» - 4.98
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min) = 1,444
Flow rate (Actual, Cubic m/min)= 3,505
Flow rate (Standard, Wet, Cubic m/min)= - 2,692
Flow rate (Standard, Dry, Cubic m/min)= 2,334
Particulate Loading - Front Half
Particulate Weight (g)= 0.0086
Particulate Loading, Dry Std. (mg/cu m)= 4.6
Particulate Loading, Actual (mg/cu m)= 3.0
Emission Rate (kg/hr)= 0 . 64
No Back Half Analysis
PROG.=VER OS/27/89
07-22-1999 12:54:46
Corr. to 7% 02 & 12% C02
4.0 3.7
38
iCal APPENDED B
-------
FILE NAME - R16A
RUN # - 16 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 0851-1041
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG,=VER OG/27/89
07-22-1999 12:54:47
Delta P
(in. H20)
2.400
2.300
2.100
0.620
0 .050
2.500
2.600
1.700
0.850
0 .120
2.800
3.000
2.2QO
1.8CO
0.4CO
2. SCO
2.700
2.500
1.400
Q.340
2.500
2.400
2.500
0.950
0.100
Delta H
(in.
2 .
2.
2.
0.
0.
2.
2.
1.
0.
0.
3.
3.
2.
1.
0.
3.
2.
2.
1.
0.
2.
2.
2.
1.
0.
H20-)
50 '
40
20
65
05
70
60
80
90
12
00
20
40
90
42
00
90
70
50
35
70
60
70
00
10
Stack
(P)
184
184
184
184
183
183
184
185
186
185
185
186
IBS
187
187
187
184
185
186
186
186
185
185
186
186
T Meter T
InCF)
81
82
84
85
86
85
88
91
92
92
90
94
95
97
97
96
95
99
100
100
97
97
101
102
101
Out(F)
81
81
81
82
82
83
84
84
85
85
85
86
87
87
88
88
89
89
90
90
91
91
92
93
93
Fraction
DRY CATCH
FILTER
Fraction
Final Wt..Tare Wt. Blank Wt. Net Wt.
(gS (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3506 ' 3.3444 0.0000 0.0062
Final Wt. Tare Wt.
(g) (g)
PROBE RINSE 3.7232 3.7208
IMPINGERS 0.0000 0,0000
Probe Rinse Blank (tug/ml) = 0.0000
Impinger Blank (ir.g/ml) = 0.0000
Vol
(ml)
32.4
0.0
Net Wt,
(g)
0.0024
0.0000
ICal APPENDIX B
39
-------
PILE NAME - RISE
RUN # - 16 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time:0853-1043
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet5= 389.822
Final Meter Volume (Cubic Feet5= 460.231
Meter Factor- 0.988
Final Leak Rate (cu ft/min)= 0.002
Net Meter Volume (Cubic Feet)= 69.564
Gas Volume (Dry Standard Cubic Feet)= 67.438
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20}= -26.68
PROG.=VER 06/27/89
07-22-1999 12:55:31
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
Average Meter Temperature (F)=
Average Delta H (in H20)=
Average Delta P (in H20}=
Average Stack Temperature (F)=
Dry Molecular Weight=
Wet Molecular Weight**
Average Square Root of Delta P
% Isokinetic=
(in H20)=
14.6
221.7
13.4
89
2,01
1.784
186
30.54
28.86
1.2453
101.1
Pitot Coefficient= 0.84
Sampling Time • (Minutes}= 100.0
Nozzle Diameter {Inches)= 0.196
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity -{Actual, Feet/rain)= 4,789
Flow Rate (Actual, Cubic ft/miri)= 125,104
Flow rate (Standard, Wet, Cubic ft/min)= 96,017
Flow Rate (Standard, Dry, Cubic ft/min)- . 83,143
Particulate Loading - Front Half
Particulate Weight (g)= . 0.0087
Particulate Loading, Dry Std. {gr/scf)= 0.0020
Particulate Loading, Actual (gr/cu ft)= 0.0013
Emission Rate (lb/hr)= 1.42
No Back Half Analysis
Corr. to 7% O2 & 12% C02
0.0017 0.0016
40
ICal APPENDK B
-------
* * METRIC UNITS * *
FILE NAME - R16B
RUN # - 16 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time:0853^1043
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 11.038
Final Meter Volume (Cubic Meters)= 13.032
Meter Factor= 0.988
Final Leak Rate (cu ra/min)= ' 0.0001
Net Meter Volume [Cubic Meters)= 1.970
Gas Volume (Dry Standard Cubic Meters)= 1.910
Barometric Pressure (mm Hg)= 763
Static Pressure (mm H20}= ' -678
Percent Oxygeii=
Percent Carbon Dioxide=
Moisture Collected (ml}=
Percent Water=
5.1
14.6
221.7
13.4
PROG.=VER 06/27/89
07-22-1999 12:55:31
Average Meter Temperature (C)= 32
Average Delta H (mm H20)= 51.0
Average Delta P (mm H20)= 45.3
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28,85
Average Square Root of Delta P (mm H20}= 6.2759
% Isokinetic= 101.1
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= 4.98
Stack Axis fl (Meters)= 1.67S
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters3= 2.427
Stack Velocity (Actual, m/min)'= 1,460
Flow rate (Actual, Cubic m/min)= 3,543
Flow rate (Standard, Wet, Cubic m/min)= 2,719
Flow rate (Standard, Dry, Cubic m/min)= 2,354
Particulate Loading - Front Half
Particulate Weight (g)= 0.0087
Particulate Loading, Dry Std. (mg/cu m)= 4.6
Particulate Loading, Actual (mg/cu m)= 3.0
Emission Rate (kg/hr)= • 0.64
Ho Back Half Analysis
Corr. to 7% O2 & 12% CO2
4.0 3.7
ICal APPENDIX B
41
-------
FILE NAME - R16B
RUN t - 16 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time:0853-1043
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER OS/27/89
07-22-1999 12:55:31
Delta P
in . H2 0 3
2.800
2. 600
2.500
1.300
0.330
2.600
2.600
2.000
0.980
0.140
2.500
2.400
2.100
0.700
0.040
2.800
2.300
2.500
0.800
0.120
2.800
3,000
2.300
2.100
0.300
Delta H
(in.
3.
2.
2.
1.
0.
2.
2.
2.
1.
0.
2.
2.
2.
0.
0.
3.
2.
2.
0.
0.
3.
3.
2.
2.
0.
H20)
10
SO
80
50
36
90
90
20
10
15
80
70
40
79
04
20
60
80
91
13
20
40
60
40
34
Stack
(F)
184
185
184
186
184
184
185
186
186
185
185
187
187
187
185
186
184
186
187
186
185
186
186
187
187
T Meter T
In(F)
80
81
81
83
84
85
85
87
89
91
90
SO
92
94
95
94
94
9S
93
98
98
97
99
101
102
Out(F)
80
80
80
84
81
81
82
83
84
85
86
86
37
88
89
90
90
91
92
92
93
93
94
95
95
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
Cg) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3169' 3.3100 0.0000 0.0069
Final Wt. Tare Wt.
Cg) (g)
PROBE RINSE 3.3603 3.3585
IMPINGERS 0.0000 0.0000
Probe Rinse Blank £mg/ml)= 0.0000
Irapinger Blank (mg/ml)= 0.0000
Vol.
(ml)
34.6
0.0
Net Wt.
(g)
0.0018
0.0000
42
ICal APPENDIX B
-------
FILE NAME - R17A
RIM # - 17 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1222-1411
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 193.064
Final Meter Volume (Cubic Feet!= 260.430
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.004
Net Meter Volume (Cubic Feet)= 68.107
Gas Volume (Dry Standard Cubic Feet)= 65.000
Barometric Pressure (in Hg) = 30.04
Static Pressure (Inches H20)= -25.51
PROG.=VER 06/27/89
07-22-1999 12:56:11
Percent Oxygen= . 5.0
Percent Carbon Dioxide= 14 . 6
Moisture Collected (ml)= 191.6
Percent Water= 12.2
Average Meter Temperature (F)= 98
Average Delta H (in H20)= 1.77
Average Delta P (in K20}= 1.748
Average Stack Temperature (F)= 185
Dry Molecular Weight= 30.54
Wet Molecular Weight= 29.01
Average Square Root cf Delta P (in H2Q)= 1.2376
% Isokinetic= 99.8
Pitot Coefficient= 0.84
Sampling Time (Minutes) = 100.0
Nozzle Diameter ( Inches) = - 0.193
Stack Axis #1 (Inches) = 66.0
Stack Axis #2 ( Inches) = ' 57.0
Rectangular Stack
Stack Area (Square Feet}- 26.13
Stack Velocity (Actual, Feet/rain) = 4,738
Flow Rate (Actual, Cubic ft/miri) = 123,783
Flow rate (Standard, Wet, Cubic ft/min)= 95,366
Flow Rate (Standard, Dry, Cubic ft/min)= 83,740
Particulate Loading - Front Half
Particulate Weight (g) = 0.0074
Particulate Loading, Dry Std, (gr/scf)= 0.0018
Particulate Loading, Actual (gr/cu ft)= 0.0012
Emission Rate (lb/hr)= 1.26
No Back Half Analysis
Corr. to 7% O2 & 12% C02
0.0015 0.0014
ICal APPENDIX B
43
-------
* * METRIC UNITS * *
FILE NAME - R17A
RUN # - 17 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1222-1411
PROJECT # - 4702.02.04.09
Initial Meter Volume {Cubic Meters)= 5.467
Final Meter Volume (Cubic Meters)= 7.374
Meter Factor= 1.011
Final Leak Rate (cu m/min)= ' 0,0001
Net Meter Volume (Cubic Meters)= 1.929
Gas Volume (Dry Standard Cubic Meters)= 1.841
Barometric Pressure (mm Eg)- 763
Static Pressure (mm H205= -648
Percent Oxygen= 5 . 0
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 191.6
Percent Water= 12.2
Average Meter Temperature (C)= 36
Average Delta H (mm H2Q5= 45.0
Average Delta P (mm H20)= 44.4
Average Stack Temperature (C)= - 85
Dry Molecular Weight= 30.'54
Wet Molecular Weight= 29.01
Average Square Root of Delta P (ram H2Q)= 6.2375
% Isokinetic= 99,8
Pitot Coefficient= 0.84
Sampling Time (Minutes)» 100.0
Nozzle Diameter (mm)= 4.90
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,444
Flow rate (Actual, Cubic m/min)= 3,505
Flow rate (Standard, Wet, Cubic m/min)= 2,700
Flow rate (Standard, Dry, Cubic m/min)= 2,371
Particulate Loading - Front Half
Particulate Weight (g)= 0.0074
Particulate Loading, Dry Std. (mg/cu m)= 4.0
Particulate Loading, Actual (rng/cu m) = 2.7
Emission Rate (kg/hr)= 0.57
No Back Half Analysis
PROG.=VER OS/27/89
07-22-1999 12:56:11
Corr. to 7% O2
3.5
& 12% C02
3.3
44
ICal APPENDIX B
-------
FILE NAME - R17A
RUN # - 17 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1222-1411
PROJECT # - 4702.02,04,09
Point #
1
2
3
4
5
6
• 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:56:11
Delta P
in, H20)
2,500
2,100
1.800
0.730
0.050
2.600
2.600
2.300
0.780
0.120
2.800
2.900
2.100
2.000
0.330
2.600
2.700
2.500
1.400
0.420
2.500
2.300
2.500
0.920
0.160
Delta H
(in.
2.
2.
1.
0.
0.
2.
2.
2.
0.
0.
2.
2.
2.
2.
0.
2,
2.
2.
1.
0.
2.
2.
2.
0.
0.
H20)
50
10
80
73
05
60
60
30
79
12
80
90
10
00
33
70
80
60
40
43
60
30
60
94
16
Stack
(F)
186
186
185
183
183
183
136
186
196
185
185
185
186
186
187
186
185
183
182
182
184
189
189
186
184
T Meter T
In(F)
91
92
93
95
95
94
96
100
101
100
97
99
103
104
105
102
104
105
106
106
103
104
. 106
107
107
Out (F)
91
91
91
91
91
SI
92
93
93
94
94
94
94
95
96
96
97
97
97
98
98
98
98
98
99
Fraction
DRY CATCH
FILTER
fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
(g) (g) (gS Eg)
0.0000 0.0000 0.0000 0.0000
3.3081 3.3021 0.0000 0.0060
?ROBE RINSE
CMPINGERS
Probe Rinse Blank (wig/ml)*
Final Wt. Tare Wt.
(g) (g)
3,5388 3.5374
0.0000 0.0000
Vol.
(ml)
23.3
0.0
0.0000
Empinger Blank (mg/mi;
0.0000
Net Wt.
(g)
0.0014
0.0000
ICal APPENDIX B
45
-------
FILE NAME - R17B
RIM # - 17 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1224-1413
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 468.423
Final Meter Volume (Cubic Feet)= 535.962
Meter Factor= 0.988
Final Leak Rate (cu ft/min)= 0.002
Net Meter Volume (Cubic Feet}= 66.729
Gas Volume (Dry Standard Cubic Feet)= S3.558
Barometric Pressure (in Hg)= 30.04
Static Pressure (Inches H20)= -25.51
Percent Oxygen= 5 . 0
Percent Carbon Dioxide= 14.6
Moisture Collected (ml}= 222.6
Percent Water= • '14.2
Average Meter Temperature (F)- 99
Average Delta H (in H20)= 1.85
Average Delta P (in H20)= 1.714
Average Stack Temperature (F) = 186
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.76
Average Square Root of Delta P (in H20)= 1.2109
% Isokinetic= 101.6
Pitot Coefficient= 0.84
Sampling Time (Minutes!= 100.0
Nozzle Diameter (Inches)= 0.193
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)- 57.0
Rectangular Stack
Stack Area (Square Feet)- 26.13
Stack Velocity (Actual, Feet/min)« 4,657
Flow Rate (Actual, Cubic ft/min}= 121,674
Flow rate (Standard, Wet, Cubic ft/min}= 93,671
Flow Rate (Standard, Dry, Cubic ft/min)= 80,407
Particulate Loading - Front Half
Particulate Weight (g)= 0.0072
Particulate Loading, Dry Std. (gr/scf)= 0.0017
Particulate Loading, Actual (gr/eu ft)= 0.0012
Emission Rate (Ib/hr)= 1.20
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 12:57:12
Corr. to 7% O2 & 12% C02
0.0015 0.0014
46
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R17B
RUN # - 17 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1224-1413
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)- 13.264
Final Meter Volume (Cubic Meters}= 15.176
Meter Factor= 0.988
Final Leak Rate (cu ra/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1,889
Gas Volume (Dry Standard Cubic Meters)= 1.800
Barometric Pressure (mm Eg) = 763
Static Pressure (mm H20)= -648
Percent Oxygen= • 5.0
Percent Carbon Dioxide= 14.6
Moisture Collected (ml}= 222.6
Percent Water= 14,2
Average Meter Temperature (C}= 37
Average Delta H (mm H20)= 47.0
Average Delta P (mm H20)= 43.5
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.76
Average Square Root of Delta P (mm H20)= 6.1028
% Isokinetic= 101.6
Pitot Coefficient- 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= 4.90
Stack Axis fl (Meters)= 1.S76
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,420
Flow rate (Actual, Cubic m/min)= 3,445
Flow rate (Standard, Wet, Cubic m/min)= 2,552
Flow rate (Standard, Dry, Cubic m/min)= 2,277
Particulate Loading - Front Half
Particulate Weight (g)= 0.0072
Particulate Loading, Dry Std. (mg/cu m)= 4.0
Particulate Loading, Actual (mg/cu m)= 2,6
Emission Rate (kg/hr)= 0.55
"So Back Half Analysis
PROG,=VER 06/27/89
07-22-1999 12:57:12
Corr. to 7% 02 & 12% CO2
3.5 3.3
ICal APPENDIX B
47
-------
FILE NAME - R17B
RUN # - 17 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1224-1413
PROJECT # - 4702.02,04.09
Point t
1
2
3
4
5
6
• 7
8
9
10
11
12
13
14
IS
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 12:57:12
Delta P
in. H20)
2.700
2.000
2.300
1.500
0.200
2.600
2.500
2.200
0.950
0.100
2.600
2.400
2.000
0.680
0.030
2.700
2.700
1.700
0.820
0.080
2.900
3 .000
2.200
1.800
0.200
Delta H
{in.
2.
2.
2.
1.
0.
2.
2.
2.
1.
0.
2.
2.
2.
0.
0.
2.
2.
1.
0.
0.
3.
3.
2.
2.
0.
H20)
90
10
50
60
21
80
70
40
00
10
80
SO
20
73
03
90
90
90
89
08
10
20
40
00
21
Stack
(F)
186
186
184
184
185
187
187
186
186
185
185
186
186
186
186
186
184
183
182
183
189
189
188
136
185
T Meter T
In(F)
93
93
94
95
96
96
97
99
100
101
100
99
102
103
103
102
101
104
105
105
104
104
106
107
107
Out (F)
93
93
93
93
93
94
94
95
95
96
, 97
96
97
97
99
99
98
99
100
101
101
100
101
101
102
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
(g) (9> ^ (g)
0.0000 0.0000 0.0000 0.0000
3.2851 3..2795 0.0000 0.0056
Final Wt. Tare Wt.
(g) lg)
PROBE RINSE 3.7969 3.7953
IMPINGERS 0.0000 0.0000
Probe Rinse Blank (mg/ml)= 0.0000
Impinger Blank (mg/ml)= 0.0000
Vol.
(ml)
33.7
0.0
Net Wt
(g)
0.0016
0.0000
48
ICal APPENDIX B
-------
FILE NAME - R18A
RUN # - 18 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time; 1540-1729
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet}= 261.719
Final Meter Volume (Cubic Feet)= 329.599
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.006
Net Meter Volume (Cubic Feet)- 68.627
3as Volume (Dry Standard Cubic Feet)= 64.769
Barometric Pressure (in Hg)= 29.99
Static- Pressure (Inches H20)= -27.21
Percent Oxygen= 5 .1
Percent Carbon Dioxide= 14.5
Moisture Collected (ml)= 200.0
Percent Water= 12.7
Average Meter Temperature (F)= 103
\-verage Delta H (in H20)= 1.84
Average Delta P (in H20)= ' 1.703
Average Stack Temperature (P}= 186
Dry Molecular Weight= 30.52
*let Molecular Weight= 28.93
Average Square Root of Delta P (in H20)= 1.2049
I Isokinetic= 99.9
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Tozzle Diameter (Inches)= 0.196
Stack Axis" #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/rnin) = 4,S37
Plow Rate (Actual, Cubic ft/min)= 121,129
Plow rate (Standard, Wet, Cubic ft/min)= 92,609
?low Rate (Standard, Dry, Cubic ft/min)= 80,850
Particulate Loading - Front Ealf
'articulate Weight (g)» 0.0090
Particulate Loading, Dry Std. (gr/scf)= 0.0021
?articulate Loading, Actual (gr/cu ft)= 0.0014
Emission Rate (lb/hr)= 1.48
To Back Half Analysis
PROG.=VER Qo/27/89
07-22-1999 13:02:21
Corr. to 7% 02 & 12% C02
0.0019 0.0018
ICal APPENDIX B
49
-------
* * METRIC UNITS * *
FILE NAME - R18A
RIM # - 18 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1540-1729
PROJECT ft - 4702.02,04.09
Initial Meter Volume (Cubic Meters)= 7.411
Final Meter Volume (Cubic Meters)= 9.333
Meter Factor= 1.011
Final Leak Rate {cu tn/min) = 0.0002
Net Meter Volume (Cubic Meters)= 1,943
Gas Volume (Dry'Standard Cubic Meters)= 1.834
Barometric Pressure (mm Hg)= 762
Static Pressure (mm H20)= -691
Percent Oxygen= 5 .1
Percent Carbon Dioxide= 14.5
Moisture Collected (ml)= 200.0
Percent Water= 12.7
Average Meter Temperature (C}= 39
Average Delta H (mm H20)= 46.7
Average Delta P (mm H20} = 43.3
Average Stack Temperature (C)= ' 86
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.93
Average Square Root of Delta P (mm H20) = 6.0727
% Isokinetic= 99.9
Pitot Coefficient= .0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)- . 4.98
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters}= • 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min} = 1,413
.Flow rate (Actual, Cubic m/min)= 3,430
Flow rate (Standard, Wet, Cubic m/min)= 2,622
Flow rate (Standard, Dry, Cubic m/min!= 2,289
Particulate Loading - Front Half
Particulate Weight (g)= 0.0090
Particulate Loading, Dry Std. (mg/cu m)= 4.9
Particulate Loading, Actual (mg/cu m)= 3.3
Emission Rate (kg/hr)= 0.67
No Back Half Analysis
PROG.=VER 06/27/89
•07-22-1999 13:02:21
Corr. to 7% O2 & 12% CO2
4.3 4,1
50
ICal APPENDIX B
-------
FILE NAME - R18A
RUN # - 18 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1540-1729
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
fraction
3RY CATCH
PROG.=VER CS/27/89
07-22-1999 13:02:21
rraction
'ROBE RINSE
:MPINGERS
Delta
•P Delta H
(in. H20) (in. H20)
2.500
2.500
2.000
0,680
0.030
2.500
2.200
2.300
0,850
0.040
2.600
2.400
2.600
2.400
0.250
2.SOO
2.400
2.300
1.500
0.240
2.500
2 .200
2.100
0.840
0.040
Blank
2.70
2.70
2.10
0.72
0.03
2.70
2.40
2.50
0.91
0.04
2.80
2.60
- 2.80
2.60 .
0.27
2.80
2.60
2.50 '
1.60
0.26
2.70
2.40
2.30
0.91
0.04
Final Wt .
(g)
0.0000
3.3S50
Final Wt .
(g]
3,8610
0.0000
(rag/ml 3 = 0.
Stack T Meter T
(F)
184
185
186
187
186
186
186
186
187
'186
186
186
187
188
187
187
185
186
186
186
186
185
186
186
185
Tare Wt .
(g)
0.0000
3,3583
Tare Wt .
-------
FILE NAME - R18B
RIM # - 18 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1542-1731
PROJECT # - 4702.02,04.09
Initial Meter Volume (Cubic Feet)- 539.689
Final Meter Volume {Cubic Feet)= 610.119
Meter Factor= 0.9S8
Final Leak Rate (cu ft/min)= 0.001
Net Meter Volume (Cubic Feet!= 69.585
Gas Volume (Dry Standard Cubic Feet!= 65.557
Barometric Pressure (in Hg)= 29.99
Static.Pressure (Inches H20)= -27.21
Percent Oxygen= 5.1
Percent Carbon Dioxide= 14.5
Moisture Collected (ral}= - 227.0
Percent Water= ' 14.0
Average Meter Temperature (F)= 104
Average Delta H (in H20)= 1.98
Average Delta P (in H20)= 1.729
Average Stack Temperature (F)= 186
Dry Molecular Weight= . 30.52
Wet Molecular Weight= 28.77
Average Square Root of Delta P (in H20)= 1.2197
% Isokinetic= . 101.1
Pitot Coefficient- 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.196
Stack Axis #1 (Inches)= . 66.0
Stack Axis t2 {inches)= 57.0
Rectangular stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)- 4,707
Flow Rate (Actual, Cubic ft/min)= 122,980
Flow rate (Standard, Wet, Cubic ft/min)= 94,006
Flow Rate (Standard, Dry, Cubic ft/min)= 80,825
Particulats Loading - Front Half
Particulate Weight (g) = 0.0088
Particulate Loading, Dry Std. (gr/scf)- 0.0021
Particulate Loading, Actual (gr/cu ft)= 0.0014
Emission Rate (Ir>/hr3 = 1.43
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 13:03:08
Corr. to 7% 02
0.0018
£12% CO2
0.0017
52
ICal APPENDDC B
-------
* * METRIC UHITS * *
FILE NAME - R18B
RUN # - 18 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1542-1731
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)- 15.282
Final Meter Volume (Cubic Meters)= 17.276
Meter Factor^ 0.988
Final Leak Rate Ecu m/min)= 0.0000
Met Meter Volume (Cubic Meters}= 1.970
3as Volume (Dry Standard Cubic Meters)= 1.856
Barometric Pressure (mm Hg)= 762
Static Pressure (mm H20)- . -691
Percent Oxygen= 5.1
Percent Carbon Dioxide= 14.5
Moisture Collected (ml}= 227.0
Percent Water= 14.0
PROG,=VER 06/27/89
07-22-1999 13:03:08
Average Meter Temperature (C) = 40
Average Delta H (mm H20)= 50.4
Average Delta P (mm H20)= 43.9
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.52
Wet Molecular Weight= 28.77
Average Square Root of Delta P (mm H2Q) = 6.1472
\ Isokinetic= 101.1
Pi-tot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Mozzle Diameter (mm)= . 4.98
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)'= 1,435
Flow rate (Actual, Cubic m/min)= 3,482
Plow rate (Standard, Wet, Cubic m/min)= 2,662
Flow rate (Standard, Dry, Cubic m/min)= 2,289
Particulate Loading - Front Half
Particulate Weight (g)= 0.0088
Particulate Loading, Dry Std. (mg/cu m)= 4.7
Particulate Loading, Actual (mg/cu m)= 3.1
Emission Rate (kg/hr)= ' 0.65
So Back Half Analysis
Corr. to 7% 02
4.2
& 12% C02
3.9
ICal APPENDIX B
53
-------
FILE NAME - RISE
RUN # - 18 - Method 17 TRAIN E for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/17/99 Time: 1542-1731
PROJECT # - 4702,02.04.09
PROG.^VER 06/27/89
07-22-1999 13':03:08
Point #
1
2
3
4
5
6 '
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
Delta P
(in. H20)
2
2
2,
1,
800
800
300
300
0,260
2.800
2.600
1.900
0.820
0.060
2,600
2.200
2.000
0.770
0.060
2.500
2.400
2.300'
0.900
O.OSO
2.700
2.300
2.700
1.800
Delta H
in.
3.
3.
2.
1.
0.
3.
3.
2.
0.
0.
3.
2.
2.
0.
0.
2.
2.
2.
1.
0.
3.
2.
3.
2.
H20)
20
20
€0
50
29
20
00
20
93
06
00
50
30
88
OS
90
80
60
00
OS
10
70
10
10
0.300
0.34
Stack
(F)
184
186
187
187
185
185
186
187
187
186
187
186
187
187
18S
185
186
187
187
186
186
186
186
186
186
In(F)
97
98
99
100
102
102
102
105
105
106
105
105
108
109
109
107
108
110
111
111
110
110
111
112
113
Meter T
Out (P)
97
97
97
98
98
99
99
100
100
101
102
102
103
103
104
104
104
105
106
106
107
106
106
107
107
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt
(g) (g)
0.0000 0.0000
3.3462 3,3391
Final Wt. Tare Wt
(g! «g)
PROBE RINSE 3.4080 3.4063
IMPINGERS 0.0000 0.0000
Probe Rinse Blank (mg/ral)= 0.0000
Irapinger Blank (mg/ml)= 0.0000
Blank Wt. Net Wt,
(g) (g)
0.0000 0.0000
0.0000 0.0071
Vol.
(ml)
37.5
0.0
Net Wt,
(g)
0.0017
0,0000
54
ICal APPENDIX B
-------
FILE NAME - R19A '
RUN # - 19- Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 0928-1117
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 330.577
Final Meter Volume (Cubic Feet}= 389.719
Meter Factor- 1.011
Final Leak Rate (cu f t/min) = 0.003
Net Meter Volume (Cubic Feet)= 59.793
Gas Volume (Dry Standard Cubic Feet)= 57.465
Barometric Pressure (in Hg) = 30.00
Static Pressure (Inches H20)= -25.24
Percent Oxygen= 5 . 2
Percent Carbon Dioxide= 14.6
yioisture Collected (ml)= 183.7
Percent Water= 13.1
Average Meter Temperature (F)= 93
Average Delta H (in H20)= 1.40
Average Delta 'P (in H20)= - 1.709
Average Stack Temperature (F)= 185
Dry Molecular Weight= 30.54
ffet Molecular Weight= 28.90
Average Square Root of Delta P (in H20)= 1.2139
\ Isokinetic= 99.9
PROG.=VER 06/27/89
07-22-1999 13:03:53
Pitot Coefficient= . 0.84
Sampling Time (Minutes) = . 100.0
Jozsle Diameter ( Inches) = 0.184
Stack Axis #1 ( Inches) - , 66,0
Stack Axis #2 ( Inches) = 57.0
Rectangular Stack
Stack Area (Square Feet}= 26.13
Stack Velocity (Actual, Feet/min) = 4,657
Flow Rate (Actual, Cubic f t/min)- 121,657
?low rate (Standard, Wet, Cubic ft/rain) = 93,684
?low Rate (Standard, Dry, Cubic f t/min) = 81,424
'articulate Loading - Front Half
?articulate Weight (g) = 0.0404
?articulate Loading, Dry Std. (gr/scf)- 0.0108
Particulate Loading, Actual (gr/cu ft)= 0.0072
Smission Rate (Ib/hr) = 7.55
to Back Half Analysis
Corr. to 7% O2 & 12% CO2
0.0096 0.0089
ICal APPENDIX B
55
-------
* * METRIC UNITS * *
FILE NAME - R19A
RUN i - 19- Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 0928-1117
PROJECT # - 4702,02,04,09
Initial Meter Volume (Cubic Meters)= 9.361
Final Meter Volume (Cubic Meters)= 11.035
Meter Factor= 1.011
Final Leak Rate feu m/min) = 0.0001
Net Meter Volume (Cubic Meters)= 1.693
Gas Volume (Dry Standard Cubic Meters)= 1.627
Barometric Pressure (mm Hg) = 752
Static Pressure (mm H20)= -641
PROG.-VER OS/27/89
07-22-1999 13:03:53
Percent Oxygen= 5 .2
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 183.7
Percent Water= 13 .1
Average Meter Temperature (C) = 34
Average Delta H (mm H20)= 35.5
Average Delta P (mm H20)= 43.4
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.90
Average Square Root of Delta P (mm H20)= 6.1179
% Isokinetie= 99.9
Pitot Coefficient- 0.84
Sampling Time (Minutes)= . 100.0
Nozzle Diameter (mm)= . 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2,427
Stack Velocity (Actual, m/min)= 1,419
Flow rate (Actual, Cubic -m/min) = 3,445
Flow rate (Standard, Wet, Cubic m/min)= 2,653
Flow rate (Standard, Dry, Cubic m/min)= 2,306
Particulate Loading - Front Half
Particulate Weight (g)= 0.0404
Particulate Loading, Dry Std. (mg/cu m)= 24.8
Particulate Loading, Actual (mg/cu m)- 16.6
Emission Rate (kg/hr} = 3.43
Ho Back Half Analysis
Corr, to 7% 02
22.0
&, 12% C02
20.4
56
ICal APPENDIX B
-------
FILE NAME - R19A
ROT # - 19- Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 0928-1117
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:03:53
Delta P
[in. H20)
2.300
2.200
2.000
0.700
0.040
2 .500
2.200
2.300
0.800
0.120
2.700
2.800
2.700
1.900
0.220
2,600
2.600
2.400
1.900
0.220
2.400
2.200
2.100
0.720
0.100
Delta H
(in. H20)
1.90
1.80
1.60
0.57
0.03
2.00
1.80
1.90
0.65
0.09
2.20
2.30
2.20
1.60
0.18
2.10
2.10
2.00
1.60
0.18
2.00
l.SO
1.70
0.59
o.oa
Stack
(F)
184
185
185
185
184
184
185
185
185
184
185
186
186
185
185
185
186
186
185
184
183
185
186
186
185
T Meter T
In{F)
85
86
87
83
89
88
90
93
95
95
93
95
97
100
100
98
98
101
102
103
99
100
102
104
102
Out (F)
85
85
85
86
86
86
86
87
87
88
88
89
90
91
91
92
92
93
93
93
84
94
94
95
95
fraction
)RY CATCH
faction
Final Wt. Tare Wt. Blank Wt. Net Wt
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3056 3.2704 0.0000 0.0352
Final Wt. Tare Wt.
(g) (g)
'ROBE RINSE 3.8354 3.8302
:MPINGERS o.oooo o.oooo
3robe Rinse Blank (rug/ml) = O.COOO
Impinger Blank (tug/ml) = O.QOOC
Vol.
(ml)
53.0
0.0
Net Wt
(g)
0.0052
0.0000
ICal APPENDIX B
57
-------
FILE NAME - R19B
RIM # - 19 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Bacrhouse Outlet Duct
DATE - 07/18/99 Time : "0930-1119
PROJECT # - 4702.02.04,09
Initial Meter Volume (Cubic Feet)= €10.344
Final Meter Volume (Cubic Feet}- 671.292
Meter Factor= 0.988
Final Leak Rate {cu ft/min)= 0.002
Net Meter Volume (Cubic Feet)- 60.217
Gas Volume (Dry Standard Cubic Feet)= 57.903
Barometric Pressure (in Hg}= 30.00
Static Pressure (Inches H205= -25.24
Percent Oxygen= 5 . 2
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)- 18S.8
Percent Water= 13.2
Average Meter Temperature (F)= 92
Average Delta H (in H20)» 1.51
Average Delta P (in H20)= 1.700
Average Stack Temperature {F)= 185
Dry Molecular Weight= 30.54
Wet Molecular Weight= ' 28.89
Average Square Root of Delta P {inH20)= 1.2101
% Isokinetic= 100.0
Pitot Coefficient^ 0.84
Sampling Time (Minutes) = 100.0
Nozzle Diameter (Inches) = 0.185
Stack Axis #1 ( Inches! = - 66.0
Stack Axis #2 ( Inches) - 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min) =
PROG,=VER 06/27/89
07-22-1999 13:04:59
Flow Rate (Actual, Cubic f t/min) =
4,645
, = 121,356
Flow rate (Standard, Wet, Cubic ft/rain) = 93,376
Flow Rate (Standard, Dry, Cubic f t/min) = 81,059
Particulate Loading - Front Half
Particulate Weight (g)=
Particulate Loading, Dry Std. (gr/scf)=
Particulate Loading, Actual (gr/cu ft)=
Emission Rate {lb/hr)«
No Back Half Analysis
0.0394
0.0105
0.0070
7.28
Corr. to 7% 02
0.0093
Sc 12% C02
0.0086
58
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R19B
RUN f - 13 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 0930-1119
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 17.283
Final Meter Volume -{Cubic Meters)= 19,008
Meter Factor= 0.988
Final Leak Rate (cu tn/min) = 0.0001
Net Meter Volume (Cubic Meters)= 1.705
3as Volume (Dry Standard Cubic Meters)= 1.640
Barometric Pressure (mm Hg)= 762
Static Pressure (mm H20)= -641
Percent Oxygen= 5.2
Percent Carbon Dioxide= 14.6
Moisture Collected (ml}= 186.8
Percent Water= 13.2
PROG.=VER 06/27/89
07-22-1999 13:04:59
Average Meter Temperature (C)=
Average Delta H (mm H20)=
Average Delta P (ram H20)=
Average Stack Temperature (C}=
Dry Molecular Weight=
Molecular Weight*
Average Square Root of Delta P (ram H20)=
t Isokinetic=
34
38.2
43.2
85
30.54
28.89
6.0988
100.0
?itot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= 4.70
Stack Axis ftl (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= 1,416
?low rate (Actual, Cubic m/min) = 3,435
Plow rate (Standard, Wet, Cubic m/min)= 2,644
?low rate (Standard, Dry, Cubic m/min)= 2,295
?articulate Loading - Front Half
?articulate Weight (g)= 0.0394
Particulate Loading, Dry Std. (mg/cu m)= 24.0
Particulate Loading, Actual (mg/cu m)= 16.0
Mission Rate (kg/hr)= 3.30
?o Back Half Analysis
Corr. to 7% O2 & 12% C02
21.3 19.8
ICal APPENDIX B
59
-------
FILE NAME - R19B '
RUN # - 19 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 0930-1119
PROJECT # - 4702,02.04.09
Point
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19 '
20
21
22
23
24
25
PROG.=VER OS/27/89
07-22-1999 13:04:59
Delta P
(in. H20)
2.700
2.700
2.300
1.300
0.180
2.600
2.300
1.900
0.850
0.100
2.500
2.400
1.900
0.660
0.050
2.600
2.300
2.500
0.850
0.120
2.700
2. €00
2.800
1.300
0.300
Delta E
(in.
2.
2.
2.
«L •
0.
2.
2.
J. .
0.
0.
2.
2.
1.
0.
0.
2.
2.
2.
0.
0.
2,
2.
2.
1.
0.
H2G)
40
40
00
10
15
30
00
70
75
08
20
10
70
59 -
04
30
10
20
76
10
40
30
50
20
27
Stack
(F)
185
185
186
185
184
186
186
186
185
184
184
185
185
185 -
185
186
187
187
185
184
186
187
187
186
185
T Meter T
In(P)
84.
85
85
87
88
89
89
91
92
93
93
93
95
97
98
96
97
99
100
100
99
100
101
102
103
Out (F)
84
84
84
85
85
86
86
87
88
88
89
90
91
91
92
93
93
94
95
95
96
96
96
97
98
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt,
(g) (g) (g) Ig)
0.0000 0.0000 0.0000 0.0000
3.3038 3.2690 0.0000 0.0348
Final Wt. Tare Wt.
(g) (g)
PROBE RINSE 3.7352 3.7306
IMPINGERS 0.0000 0.0000
Probe Rinse Blank (rag/ml)= 0.0000
Impinger Blank (tng/ral)= 0.0000
Vol.
(ml)
40.9
0.0
Net Wt,
(g)
C.0046
O.OODO
60
Kal APPENDIX B
-------
FILE NAME - R2QA
SUN # - 20 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1259-1448 •
PROJECT # - 4702.02.04.09
Initial Meter Volume {Cubic Feet)= 389,970
Final Meter Volume (Cubic Feet)- 452.137
*leter Factor= 1.011
Final Leak Rate (cu ft/min!= 0.010
tfet Meter Volume (Cubic Feet)= £2.851
3as Volume (Dry Standard Cubic Feet)= 59,507
3aroraetric Pressure [in Hg) = IB.SB
Static Pressure (Inches H20)= -23.89
Percent Oxyge,n= 5 . 2
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 223.6
Percent Water= 15.0
\verage Meter Temperature (F)= 101
Average Delta H (in H20}= 1.50
\verage Delta P (in H2Q3= 1.736
Average Stack Temperature (F)= 186
Dry Molecular Weight** 30.54
•fet-Molecular Weight= 28.66
Werage Square Root of Delta P (in H20)= 1.2317
\ Isokinetic= 101,5
?itot Coefficients 0.84
Sampling Time (Minutes)** 100.0
Nozzle Diameter (Inches)= 0.186
stack Axis #1 (Inches)= , 66.0
stack Axis #2 (Inches)= 57.0
Rectangular Stack
stack Area (Square Feet}= 26.13
Stack Velocity (Actual, Feet/min)= 4,741
?low Rate (Actual, Cubic ft/min)= 123,848
?low rate (Standard, Wet, Cubic ft/min)= 95,550
?low Rate (Standard, Dry, Cubic ft/min)- 81,183
Particulate Loading - Front Half
Particulate Weight (g)= 0.0253
Particulate Loading, Dry Std. (gr/scf}= 0.0068
Particulate Loading, Actual Egr?cu ft]= 0.0045
3mission Rate £lb/hr)= 4.74
tfo Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 13:05:38
Corr. to 7% 02 £ 12% C02
0.0060 0.0056
ICal APPENDIX B
61
-------
* * METRIC UNITS * *
FILE NAME - R20A
RUN # - 20 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1259-1448
PROJECT # - 4702,02.04.09
Initial Meter Volume (Cubic Meters)= 11.042
Final Meter Volume (Cubic Meters)= 12.803
Meter Factor= 1.011
Final Leak Rate (cu ra/min)= 0.0003
Net Meter Volume (Cubic Meters)= 1.780
Gas Volume (Dry Standard Cubic Meters)= 1.685
Barometric Pressure (mm Hg)= 761
Static Pressure (mm H20)= -607
PROG.=VER 06/27/89
07-22-1999 13:05:38
Percent Qxygen= 5 .2
Percent Carbon Dioxide= 14 . €
Moisture Collected (tnl)= 223.6
Percent Water= 15.0
Average Meter Temperature (C) = 38
Average Delta H (mm H20)= 38.2
Average Delta P (mm H2Q) = . 44.1
Average Stack Temperature (C)= 85
Dry Molecular Weight* 30.54
Wet Molecular Weight** 28.66
Average Square Root of Delta P (mm H20)= 6.2074
% Isokinetic= 101.5
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= 4.72
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min5= 1,445
Flow rate (Actual, Cubic m/minj= 3,507
Flow rate (Standard, Wet, Cubic m/min)= 2,706
Flow rate (Standard, Dry, Cubic m/min)= 2,299
Particulate Loading - Front Half
Particulate Weight (g)= 0.0263
Particulate Loading, Dry Std. (mg/cu m)= 15.6
Particulate Loading, Actual (mg/cu m)= 10.2
Emission Rate (kg/hr)= 2.15
No Back Half Analysis
Corr. to 7% 02 & 12% C02
13.8 12.8
62
ICal APPENDIX B
-------
FILE NAME - R20A
RUN # - 20 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATS - 07/18/99 Time: 1259-1448
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
- 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:05:38
Delta P
;in. H20)
2.400
2.200
1,900
0.690
0.030
2.600
2.500
2.000
1.100
0.180
2.800
2.800
2.800
1.300
0.300
2.700
2.600
2.100
1.800
0.250
2.400
2,500
2.400
0.880
0.180
Delta H
(in
2
1
1
0
0
2
2
1
0'
0
2
2
2
1
0
2
2
1
1
0
2
2
2
0
0
. H20)
.10
.90
.60
.59
.02
.20
.20
.70
.95
.15
.40
.40
.40
.10
.26
.40
.30
.80
.60
.21
.10
.20
.10
.77
.15
Stack
(F)
185
186
186
186
184
186
184
184
186
186
186
186
186
186
187
187
186
185
185
186
186
186
185
184
185
T Meter T
In(F)
93
94
96
98
98
96
99
101
103
103
101
102
105
107
107
105
106
108
108
110
108
109
111
112
111
Out (F)
93
93
93
94
93
94
95
95
96
96
96
97
97
98
99
99
' 99
100
100
101
101
102
102
103
104
fraction
DRY CATCH
FILTER
?raction
?ROBE RINSE
[MPINGERS
Final Wt. Tare Wt. Blank Wt. Net Wt,
(g) (g) (g) (g)
0.0000 O.OOOG 0.0000 0.0000
3.2800 3.2576 0.0000 0.0224
Final Wt
(g)
3.6921
0.0000
'robe Rinse Blank (wig/ml) =
Tare Wt. Vol.
(g) (ml)
3.6882 35.1
0.0000 0,0
0.0000
Net Wt.
(g)
0.0039
0.0000
Impinger Blank (rag/ml)= 0.0000
ICal APPENDIX B
63
-------
FILE NAME - R20B
RIM # - 20 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1301-1450
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 678.559
Final Meter Volume (Cubic Feet}« . 741.084
Meter Pactor= 0.988
Final Leak Rate (cu ft/min)= 0.002
Net Meter Volume (Cubic Feet)= 61.775
•Gas Volume (Dry Standard Cubic Feet)= 58.453
Barometric Pressure (in Hg)= 29.98
Static Pressure (Inches H20}= -23.89
Percent Oxygen= 5 .2
Percent Carbon Dioxide= 14.6
Moisture Collected (ml)= 226.8
Percent Water** 15.5
Average Meter Temperature (F)= 101
Average Delta H (in H20)= 1.55
Average Delta P (in H20)= 1.749
Average Stack Temperature EF)= 186
Dry Molecular Weight= 30.54
Wet Molecular Weight= 28.61
Average Square Root of Delta P (in H20)= 1.2357
% Isokinetic= 102.0
Pitot Coefficients 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches}= . 66.0
Stack Axis t2 {Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.,13
Stack Velocity (Actual, Feet/min)= . 4,763
Flow Rate (Actual, Cubic ft/min)= 124,422
Flow rate (Standard, Wet, Cubic ft/min)= 95,910
Flow Rate (Standard, Dry, Cubic ft/min)=* 81,091
Particulate Loading - Front Half
Particulate Weight (g)= 0.0275
Particulate Loading, Dry Std. (gr/scf)= 0.0072
Particulate Loading, Actual (gr/cu ft)= 0.0047
Emission Rate (lb/hr)= 5.03
No Back Half Analysis
PRQG.=VER 06/27/89
07-22-1999 13:06:21
Corr. to 7% 02 & 12% C02
0.0054 0.0060
64
icai APPENDIX: B
-------
* * METRIC UNITS * *
FILE NAME - R20B
RUN # - 20 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1301-1450
PROJECT f - 4702.02,04.09
Initial Meter Volume (Cubic Meters)= IS.214
Final Meter Volume (Cubic Meters)- 20.985
Meter Factor= 0.988
Final Leak Rate (cu m/min)= 0.0001
Net Meter Volume (Cubic Meters)= 1.749
Gas Volume (Dry Standard Cubic Meters)= 1.655
Barometric Pressure (mm Eg}= 7S1
Static Pressure (mm H20)= -607
PROG.=VER 06/27/89
07-22-1999 13:06:21
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
5.2
14.6
226.8
15.5
Average Meter Temperature {C}= 38
Average Delta H (mm H20}= 39.3
Average Delta P (mm H20)= 44.4
Average Stack Temperature (C}= 86
Dry Molecular Weight- 30.54
Wet Molecular Weight= 28.61
Average Square Root of Delta P (mm H20)= S.227S
% Isokinetic= 102.0
Pitot Coefficient^ 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= . 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)- 1,452
Flow rate (Actual, Cubic m/min)= 3,523
Flow rate (Standard, Wet, Cubic m/min)= 2,716
Flow rate (Standard, Dry, Cubic m/min)= 2,296
Particulate Loading - Front Ealf
Particulate Weight (g)= 0.0275
Particulate Loading, Dry Std. (mg/cu tn)= 16.6
Particulate Loading, Actual (mg/cu m)= 10.8
Emission Rate (kg/hr)= 2.29
No Back Half Analysis
Corr. to 7% 02 & 12% C02
14.7 13.7
ICal APPENDIX B
65
-------
FILE NAME - R20B
RUN # - 20 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1301-1450
PROJECT # - 4702.02,04.09
Point #
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:06:21
Delta P
in. H20)
2.600
2.700
2.400
1.900
0.370
2.600
2.600
1.900
1.000
0.170
2.600
2.200
2.200
0.700
0.040
2.70'0
2.700
1.600
0.850
0.100
2.700
2.SOO
2.200
1.700
0.300
Delta H
(in.
2.
2.
2.
1.
0.
2.
2.
1 .
0.
0.
2.
1.
1.
0.
0.
2.
2.
1.
0.
0.
2.
2.
2.
1.
0.
H205
30
40
10
70
32
30
30
70
88
14
30
90
90
S2
03
40
40
40
75
03
40
60
00
50
26
Stack
(F)
186
187
187
186
185
185
185
185
187
187
187
186
186
187
187
187
186
185
186
186
187
186
185
186
186
T Meter T
In(F)
94
95
95
97
SB
99
99
101
102
102
102
102
104
105
105
104
105
107
107
108
106
107
108
109
110
Out (F)
94
94
94
95
95
96
96
97
97
98
99
99
99
100
100
101
101
102
102
103
103
103
104
104
104
Fraction
DRY CATCH
FILTER
Fraction
PROBE RINSE
IMPINGERS
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g> Cg> (g)
0.0000 0.0000 0.0000 0.0000
3.3376 3..3137 0.0000 0.0239
Final Wt. Tare Wt. Vol. Net Wt,
(g) (g) (ml) (g)
3.6964 3.6928 33.7 0.0036
0.0000 0.0000 0.0 0.0000
Probe Rinse Blank (rag/ml)= 0.0000
Impinger Blank (rag/ml)= 0.0000
66
ICal APPENDIX B
-------
FILE NAME - R21A
RUN # - 21 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1617-1806
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 453.291
Final Meter Volume (Cubic Feet)= 513.459
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.004
Net Meter Volume (Cubic Feet)= 60.830
Gas Volume (Dry Standard Cubic Peet)= 57.428
Barometric Pressure (in Hg)= 29.94
Static Pressure (Inches H20)= -26.55
Percent Oxygen= 5.4
Percent Carbon Dioxide* 14.1
Moisture Collected (ml)= 197.1
Percent Water= 13.9
Average Meter Temperature (F)= 101
Average Delta H (in H20}= 1.44
Average Delta P (in H20)= 1.721
Average Stack Temperature (F)= 185
Dry Molecular Weight= 30.47
ftet Molecular Weight^ 28.74
\verage Square Root of Delta P (in H20)= 1.2144
's Isokinetic= 100.7
?itot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= 66.Q
Stack Axis tt2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,686
?low Rate (Actual, Cubic ft/min)= 122,433
7low rate (Standard, Wet, Cubic ft/min)= 93,711
Tlow Rate (Standard, Dry, Cubic ft/min)= 80,670
?articulate Loading - Front Half
'articulate Weight (g)= 0.0238
?articulate Loading, Dry Std. (gr/scf)= 0.0064
Articulate Loading, Actual (gr/cu ft)- 0.0042
Emission Rate (lb/hr)= 4.41
Jo Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 13:07:02
Ccrr. to 7% O2 & 12% C02
0.0057 0.0054
ICal APPENDIX B
67
-------
* * METRIC LTSITS * *
FILE NAME - R21A
RUN # - 21 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1617-1806
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 12.835
Final Meter Volume (Cubic Meters}= 14.539
Meter Factor= 1.011
Final Leak Rate (cu m/tnin)= 0.0001
Net Meter Volume (Cubic Meters)= 1.722
Gas Volume (Dry Standard Cubic Meters)= 1.626
Barometric Pressure (mm Hg)= 760
Static Pressure (ram H20)= -674
PROG,=VER 06/27/89
07-22-1999 13:07:02
Percent Oxygen= 5.4
Percent Carbon Dioxide- 14.1
Moisture Collected {ml)= 197.1
Percent Water= 13.9
Average Meter Temperature (C)= 39
Average Delta H (mm H20)= 35.6
Average Delta P (ram H20)= 43.7
Average Stack Temperature (C)= 85
Dry Molecular Weight= 30.47
Wet Molecular Weight= 28.74
Average Square Root of Delta P (ram H20)= 6.1205
% Isokinetics 100.7
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm) = . 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis §2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2,427
Stack Velocity (Actual-, m/min) = 1,428
Flow rate (Actual, Cubic m/min)= 3,467
Flow rate {Standard, Wet, Cubic m/min}= 2,S54
Flow rate (Standard, Dry, Cubic m/min)= 2,284
Particulate Loading - Front Half
Particulate Weight (g)= O.Q238
Particulate Loading, Dry Std. (mg/cu ra)= 14.6
Particulate Loading, Actual (mg/cu TO)= 9.6
Emission Rate (kg/hr)= 2.00
No Back Half Analysis
Corr. to 7% 02
13.1
12% C02
12.5
68
ICal APPENDIX B
-------
FILE NAME - R21A
RON # - 21 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1617-1806
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
IS
17
18
19
20
21
22
23
24 •
25
PROG.=VER 06/27/89
07-22-1999 13:07:02
Delta P
!in. H20)
2.400
2,200
2.000
0.720
0.040
2.600
2.300
2 .400
0.780
0.150
2.700
2.700
2.900
1.200
0.220
2.800
2,700
2.300
1.400
0.220
2.500
2.400
2.400
0.950
0.050
Delta H
(in. H20)
2.00
1.80
1.70
0.60
0.03
2.20
1.90
2.00
0.65
0.12
2.30
2.30
2.40
1,00
0.18
2.30
2.30
1.90
1.20
0.18
2.10
2,00
2.00
0.79
0.04
Stack
CF)
185
185
•184
184
184
184
187
186
184
185
184
186
187
186
186
186
185
186
IBS
184
186
185
185
18S
186
T Meter T
In(F)
97
98
99
101
101
99
102
103
106
105
102
104
106
108
107
103
104
107
108
108
104
105
106
1G7
107
Out (F)
97
97
97
97
97
98
98
98
99
98
99
99
100
100
100
100
99
100
100
100
100
99
100
100
100
?raction
DRY CATCH
FILTER
Fraction
PROBE RINSE
CMPINGERS
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g! (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3112 3.2914 0.0000 0.0198
Final Wt.
(g)
3.5230
0.0000
Tare Wt
(g)
3.5190
0.0000
Probe Rinse Blank (rag/ml)= 0.0000
Cmpinger Blank (mg/ml)= 0.0000
Vol.
(ml)
35.7
0.0
Net Wt,
(g)
0 .0040
0.0000
ICal APPENDIX B
69
-------
FILE NAME - R21B
RUN # - 21 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time:~1619-1808
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)=
Final Meter Volume (Cubic Feet}=
Meter Factor=
Final Leak Rate (cu ft/min)=
Net Meter Volume {Cubic Feet)=
Gas Volume (Dry Standard Cubic Feet}=
Barometric Pressure (in Hg)=
Static Pressure (Inches H20)=
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent -Water= •
Average Meter Temperature (F)«
Average Delta H (in H20)=
Average Delta P (in H20)=
Average Stack Temperature (F)=
Dry Molecular Weight=
Wet Molecular Weight=
Average Square Root of Delta P (in H2Q)=
% Isokinetic=
Pitot Coefficient=
Sampling Time (Minutes)=
Nozzle Diameter (Inches)=
Stack Axis #1 (Inches5«
Stack Axis #2 (Inches)=
Rectangular Stack
Stack Area (Square Feet5=
Stack Velocity (Actual, Feet/min)=
Flow Rate (Actual, Cubic ft/rain)=
Flow rate (Standard, Wet, Cubic ft/min)=
Flow Rate (Standard, Dry, Cubic ft/min)=
Particulate Loading - Front Half
Particulate Weight (g)=
Particulate Loading, Dry Std. tgr/scf)=
Particulate Loading, Actual (gr/cu ft)=
Emission Rate (lb/hr)=
Mo Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 13:07:45
746.002
810.070
0.988
0.001
63,299
59.557
29.94
-26.55
5.4
14.1
209.5
14.2
104
1.63
1.796
186
30.47
28.70
1.2457
101.1
0.84
100.0
0.185
66.0
57.0
26.13
4,812
125,712
96,150
82,484
0,0236
0.0061
0.0040
4.31
to 7% O2 & 12% C02
0.0055 0.0052
70
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R21B
RUN # - 21 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghcuse Outlet Duct
DATE - 07/18/99 Time: 1519-1808
PROJECT # - 4702.02.04,09
Initial Meter Volume (Cubic Meters)= 21.124
Final Meter Volume (Cubic Meters)= 22.93B
Meter Factor= , 0.988
Final Leak Rate (cu m/min)= 0.0000
!Tet Meter Volume (Cubic Meters) = 1.792
3as Volume (Dry Standard Cubic Meters)= 1.686
3arometric Pressure (mm Hg)= 760
static Pressure (mm H20}= -674
Percent Oxygen= 5.4
Percent Carbon Dioxide= 14.1
toisture Collected (ml)= 209.5
Percent Water= 14.2
PROG.=VER 06/27/89
07-22-1999 13:07:46
Iverage Meter Temperature (C)= 40
iverage Delta H (mm H20)= 41,5
Average Delta P (mm H20)= 45.6
Average Stack Temperature (C)= 85
)ry Molecular Weight= 30.47
fet Molecular Weight= 28.70
Average Square Root of Delta P (mm H20)= 6.2781
fe Isokinetic= 101.1
Jitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Jozzle Diameter (mm)= 4,70
Stack Axis #1 (Meters)= 1.S7S
Stack Axis #2 (Meters^= 1.448
Rectangular' Stack
Stack Area {Square Meters)= 2.427
stack Velocity (Actual, m/min)= 1,467
rlow rate (Actual, Cubic m/min)= 3,560
rlow rate (Standard, Wet, Cubic m/min)= 2,723
rlow rate (Standard, Dry, Cubic m/min)= 2,336
'articulate Loading - Front Half
'articulate Weight {g)= 0.0236
'articulate Loading, Dry StcL (mg/cu m)= 14.0
'articulate Loading, Actual (mg/cu m)= 9.2
Emission Rate
-------
FILE NAME - R21B
RIM # - 21 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/18/99 Time: 1619-1808
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:07:46
Delta P
(i
2
2
2
1
0
2
2
2
0
0
2
2
2
0
0
2
2
1
0
0
2
2
2
2
0
n . H2 0 5
.800
.800
.200
,900
.200
.600
.500
.400
.900
.140
.500
.200
.200
.580
.050
.700
.800
.800
.850
.100
,800
.600
.700
.100
.270
Delta H
in
2
2
2
1
0
2
2
2
0
0
2
2
2
0
0
2
2
1
0
0
2
2
2
1
0
. H20)
.50
.50
.00
.70
.13
.40
.30
,20
.81
.12
.40
.00
.00
,61
.04
.50
.50
.60
.77
.OS
.60
.40
,50
.90
.24
Stack
(F)
186
185
184
185
186
187
186
185
185
186
186
186
187
186
185
186
186
186
186
185
186
186
186
186
186
T Meter T
In(F)
99
99
100
101
102
103
103
104
106
106
105
105
106
107
108
106
106
107
108
108
107
107
108
109
109
Out (F)
99
99
99
99
100
100
100
100
101
102
102
102
102
103
103
103
103
103
104
104
104
104
104
105
105
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.2892 3.2692 0.0000 0.0200
Final Wt. Tare Wt. Vol. Net Wt,
(g) (g) (ml) (-g)
PROBE RINSE 3.7292 3.7256 27.5 0.0036
IMPINGERS 0.0000 0.0000 0.0 0.0000
Probe Rinse Blank (mg/ml)= 0.0000
Impinger Blank {mg/ml)= 0.0000
72
KM APPENDIX B
-------
FILE NAME - R22A
RUN # - 22 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 0858-1047
PROJECT # - 4702.02.04,09
Initial Meter Volume (Cubic Peet}= 515.155
Final Meter Volume (Cubic Feet)= 575.121
Meter Factor= 1.011
Final Leak Rate (cu ft/rain)= 0.008
Net Meter Volume (Cubic Feet)= 60.626
Gas Volume (Dry Standard Cubic Feet)= 58.432
Barometric Pressure (in Eg)= 29.95
Static Pressure (Inches H20J= -27.01
Percent Oxygen- 5.0
Percent Carbon Dioxide= 14.7
Moisture Collected (ml)= 193.5
Percent Water= 13.5
PROG.=VER 06/27/89
07-22-1999 13:14:09
Average Meter Temperature (F)= 90
Average Delta H (in H20)= 1.45
Average Delta P (in H20)= 1.722
Average Stack Temperature (F)= 184
Dry Molecular Weight= 30.55
Wet Molecular Weight- 28.86
Average Square Root of Delta P (in H20)= 1.2171
% Isokinetic= 99.8
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
iozzle Diameter {Inches)= 0.186
Stack Axis #1 (Inches)= , 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,685
Flow Rate (Actual, Cubic ft/min) = 122,391
Flow rate (Standard, Wet, Cubic ft/min)= 93,750
Flow Rate (Standard, Dry, Cubic ft/min)= 81,101
Particulate Loading - Front Half
'articulate Weight (g)= 0.0377
?articulate Loading, Dry Std. (gr/scf)= 0.0099
Particulate Loading, Actual (gr/cu ft)= 0.0066
Mission Rate (Ib/hr)= 6.91
to Back Half Analysis
Corr. to 7% 02 & 12% CO2
0.0087 0.0081
ICal APPENDIX B
73
-------
* * METRIC UNITS * *
PILE NAME - R22A
ROT # - 22 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 0858-1047
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 14.587
Final Meter Volume (Cubic Meters)= 16.285
Meter Factors 1.011
Final Leak Rate (cu m/min)= 0.0002
Net Meter Volume (Cubic Meters)= 1.717
Gas Volume (Dry Standard Cubic Meters)= 1.655
Barometric Pressure (mm Hg)= 761
Static Pressure (ram H20}= -686
Percent Oxygen= 5. 0
Percent Carbon Dioxide= 14.7
Moisture Collected {ml}= 193.5
Percent water= 13.5
Average Meter Temperature (C)= 32
Average Delta H (mm H20)= 36.8
Average Delta P (mm H20}= 43.7
Average Stack Temperature (C}= 85
Dry Molecular Weight* . 30.55
Wet Molecular Weight= 28.86
Average Square Root of Delta ? (mm H20)= 6.1338
% Isokinetic= 99.8
Pitot Coefficient 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (mm)= , 4.72
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters-! = 2.427
Stack Velocity (Actual, m/min)= 1,428
Plow rate (Actual, Cubic m/min)= 3,466
Flow rate (Standard, Wet, Cubic m/min)= 2,655
Flow rate (Standard, Dry, Cubic m/min)= 2,297
Particulate Loading - Front Half
Particulate Weight (g)= 0.0377
Particulate Loading, Dry Std. (mg/cu m)= 22.8
Particulate Loading, Actual (mg/cu m)= 15,1
Emission Rate (kg/hr)= 3.14
No Back Half Analysis
PROG.=VER 06/27/89
07-22-1999 13:14:09
Corr. to 7% O2
19.9
12% C02
18.6
74
ICal APPENDIX B
-------
PILE NAME - R22A
RUN # - 22 - Method. 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 0858-1047
PROJECT # - 4702,02.04.09
Point #
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:14:09
Delta P
( in . H2 0 )
2.500
2,200
2.000
0.730
0.050
2.500
2.700
2.300
0.780
0.100
2.900
2.900
2.700
1,800
0.200
2.700
2.500
2.300
1.300
0 .280
2.600
2.300
1.800
0.800
0.100
Delta H
(in. H20)
2.10
1.80
1.70
0.61
0.04
2.10
2.30
1.90
0.65
0.08
2.40
2.40
2.30
1.50
0.16
2.30
2.10
2.00
1.10
0.23
2.20
2.00
1.50
0.68
0.08
Stack
(F)
181
186
IBS
184
183
182
185
185
184
185
185
185
184
184
185
184
184
184
185
185
184
184
184
185
184
T Meter T
In(F)
.82
83
85
87
87
86
88
91
92
92
91
93
94
96
93
94
95
97
98
97
94
97
100
101
100
Out (F
82
82
83
83
84
84
84
85
86
86
86
87
87
88
89
89
90
90
90
91
91
91
92
93
93
fraction
)RY CATCH
^ILTER
faction
Final Wt. Tare Wt. Blank Wt. Net Wt,
Cg> (g) (g> (g)
0.0000 C.OOOO 0.0000 0.0000
3.2863 3.2533 0.0000 0.0330
Wt
Final
(g)
RINSE 3 .3638
:MPINGERS o.oooo
>robe Rinse Blank (mg/ml}=
[mpinger Blank (rag/ml)= 0.0000
0
Tare
(g)
3.3591
0.0000
0000
Wt.
Vol.
(ml)
47.2
0.0
Net Wt.
(g)
0.0047
0.0000
ICal APPENDIX B
75
-------
FILE NAME - R22B
RUN ft - 22 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 0900-1049
PROJECT f - 4702.02.04.09
Initial Meter Volume (Cubic Peet}=
Final Meter Volume (Cubic Feet)=
Meter Factor=
Final Leak Rate (cu ft/min)=
Net Meter Volume (Cubic Feet}=
Gas Volume (Dry Standard Cubic Feet}=
Barometric Pressure (in Hg)=
Static Pressure (Inches H203=
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ml)=
Percent Water=
Average Meter Temperature (F) =
Average Delta H {in H20)=
Average Delta P (in H2Q) =
Average Stack Temperature (F) =
Dry Molecular Weight*
Wet Molecular Weight=
PROG.=VER 06/27/89
07-22-1999 13:14:49
Average Square Root of Delta P
% Isok±netic=
Pitot Coefficients
Sampling Time (Minutes)=
Nozzle Diameter (Inches)=
Stack Axis #1 (Inches)=
Stack Axis #2 (Inches)=
Rectangular Stack
Stack Area (Square Feet)=
[in H20) =
Particulate Loading - Front Half
Particulate Weight {g)=
Particulate Loading, Dry Std.
-------
FILE NAME - R22B
RUN f - 22 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 0900-1049
PROJECT # - 4702.02.04.09
PROG,=VER 06/27/89
07-22-1999 13:14:49
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
IS
17
18
19
20
21
22
23
24
25
Delta P
in
2.
2.
2.
1.
0.
2.
2.
2.
0.
0.
2.
2.
2.
0.
0.
2,
2.
2.
0.
0.
2.
2.
2.
1.
0.
. H20)
700
600
500
400
300
700
300
100
860
080
SOO
300
000
770
040
£00
500
300
S€0
200
BOO
800
6QQ
900
300
Delta H
(in.
2.
2.
2.
1.
0.
2.
2.
1.
0.
0.
2.
2.
1.
0.
0.
2.
2.
2,
0.
0.
2.
2.
2.
x .
0.
H20)
30
20
10
20
25
30
00
80
73
06
20
00
70
66
03
20
20
00
74
17
40
40
20
60
26
Stack
(F)
182
186
186
184
183
184
185
185
184
185
185
185
184
185
. 185
185
185
185
186
186
185
185
186
186
IBS
T Meter T
In(F>
82
82
83
84
85
86
87
88
90
91
90
91
93
94
95
93
94
96
97
97
96
97
98
100
101
Out (F
82
82
82
82
83
84
84
84
85
86
87
87
88
89
90
90
91
91
92
92
93
93
94
94
95
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g)
-------
FILE NAME - R23A
RUN # - 23 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/29 Time: 1150-1339
PROJECT # - 4702,02.04.09
Initial Meter Volume (Cubic Feet}= 575.666
Final Meter Volume (Cubic Feet)= 634.533
Meter Factor= 1.011
Final Leak Rate (cu ft/min)= 0.009
Net Meter Volume (Cubic Feet}= 59.515
3as Volume (Dry Standard Cubic Feet)= 56.412
Barometric Pressure (in Hg)= 29,94
Static Pressure (Inches H20)= -24.27
PROG.=VER OS/27/89
07-22^1999 13:15:36
Percent Oxygen=
Percent Carbon Dioxide=
Moisture Collected (ral)=
Percent Water=
5.0
14.8
177.9
12.9
Meter Temperature (F)= 99
Average Delta H (in H20}= 1.35
Average Delta P (in H20)= 1.S38
Average Stack Temperature (F)- 185
3ry Molecular Weight= 30.57
Vet Molecular Weight= 28.94
Average Square Root of Delta P (in H20)= 1.1903
I Isokinetic= 99.8
Pitot Coefficient- 0.84
Sampling Time (Minutes)= • 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,562
?low Rate (Actual, Cabic £t/min)= 119,180
Plow rate (Standard, Wet, Cubic f -t/min) = 91,819
?low Rate (Standard, Dry, Cubic" ft/rain)= 79,944
Particulate Loading - Front Half
Particulate Weight (g)= 0.0210
Particulate Loading, Dry Std. (gr/scf)= 0.0057
Participate Loading, Actual (gr/cu ft)= 0.0038
Emission Rate (lb/hr)= 3.93
to Back Half Analysis
Corr. to 7% 02 & 12% CO2
0.0050 0.0046
ICal APPENDIX B
79
-------
* * METRIC UNITS * *
FILE NAME - R23A
RUN # - 23 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1150-1339
PROJECT # - 4702.02.D4.09
Initial Meter Volume (Cubic Meters)= 16.301
Final Meter Volume (Cubic Meters]= 17.967
Meter Factor= 1.011
Final Leak Rate (eu m/min)= 0.0003
Net Meter Volume (Cubic Meters)= 1.S85
Gas Volume (Dry Standard Cubic Meters)= 1.597
Barometric Pressure (mm Hg)= 760
Static Pressure (mm H20}= -616
PROG.«VER 06/27/89
07-22-1999 13:15:35
Percent Oxygen= 5.0
Percent Carbon Dioxide= 14.8
Moisture Collected {ral)= 177.9
Percent Water= , 12.9
Average Meter Temperature (C)= 37
Average Delta H {mm H20)= 34.5
Average Delta P (mm K20}= 41.6
Average Stack Temperature {C)= 85
Dry Molecular Weight= - 30.57
Wet Molecular weight= 28.94
Average Square Root of Delta P (mm H20)= 5.9988
% Isokinetic= 99.8
Pitct Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter {mm)- . 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/min)= ' 1,390
Plow rate (Actual, Cubic m/min)= 3,375
Flow rate (Standard, Wet, Cubic m/min) = 2,600
Flow rate (Standard, Dry, Cubic m/min)= 2,264
Particulate Loading - Front Half
Particulate Weight (g)= 0.0210
Particulate Loading, Dry Std. (mg/cu m)= 13.1
Particulate Loading, Actual (mg/cu m)= 8.8
Emission Rate (kg/hr)- 1.78
No Back Half Analysis
Corr. to 7% O2
11.5
& 12% C02
10.7
80
KM APPENDIX B
-------
FILE NAME - R23A
RUN # - 23 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1150-1339
PROJECT # - 4702.02,04.09
Point ft
1
2
3
4
5
6
• 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:15:36
Delta P
(in. H20)
2
2
1
0
0
2
2
2
0
0
2
2
2
1
0
2
2
2
1
0
2
2
2
0
0
.800
.000
.800
.680
.050
.600
.300
.100
.800
.050
.500
.400
.600
.700
.300
.400
.300
.300
.300
.220
.400
.200
.200
.800
.150
Delta H
(in
2
1
1
0
0
2
1
1
0
0
2
2
2
1
0
2
1
1
1
1
0
2
1
1
0
0
. H20i
.30
.50
.50
.56
.04
.20
.90
.70
.66
.04
.10
.00
.20
.40
.25
.00
.90
.90
.10
.18
.00
,80
.80
.67
.12
Stack
) (F3
184
185
165
184
184
184
185
185
186
185 '
185
184
185
186
185
185
186
186
185
185
185
186
186
184
183
T Meter T
ln(F)
92
93
95
97
97
97
99
101
102
101
99
100
103
105
105
103
104
1G5
105
105
104
104
106
108
107
Out(F)
92
92
93
93
94
94
95
95
95
96
96
96
97
97
98
98
98
98
99
99
99
100
100
100
101
Fraction
DRY CATCH
?ILTER
fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.2315 3.2128 0.0000 0.0187
Final Wt. Tare Wt. Vol. Net Wt.
(g) (g) (ml) (g)
PROBE RINSE 3.3269 3.3246 34.3 0.0023
[MPINGERS 0.0000 0.0000 0.0 0.0000
?robe Rinse Blank (mg/ml}= 0.0000
[mpinger Blank (mg/ml)= 0.0000
ICal APPENDIX B
81
-------
FILE NAME - R23B
RUN f - 23 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATS - 07/19/99 Time: 1152-1341
PROJECT # - 4702.02,04.09
Initial Meter Volume (Cubic Feet)- 872.288
Final Meter Volume (Cubic Feet)= 932.231
Meter Factor= 0.988
Final Leak Rate (cu ft/min)= 0.000
Net Meter Volume (Cubic Feet)= 59.224
Gas Volume (Dry Standard Cubic Feet)= 56.038
Barometric Pressure (in Hg)= 29.94
Static Pressure (Inches H2GJ= -24.27
Percent Oxygen= ' 5.0
Percent Carbon Dioxide^ 14.8
Moisture Collected (ml)= 185.8
Percent Water= 13 . 5
Average Meter Temperature (F)= 100
Average Delta H (in H20}= 1.45
Average Delta P (in H20)= 1.604
Average Stack Temperature (F)= 185
Dry Molecular Weight- 30,57
Wet Molecular Weight= • 28.87
Average Square Root of Delta P (in H20)= 1.1723
% Isokinetic= 100.2
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.185
Stack Axis #1 (Inches)= - 66.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area {Square Feet)= 26.13
Stack Velocity (Actual, Feet/min)= 4,500
Flow Rate (Actual, Cubic ft/min)= 117,565
Flow rate (Standard, Wet, Cubic ft/min)= 30,519
Flow Rate (Standard, Dry, Cubic ft/min)= 78,292
Particulate Loading - Front Half
Particulate Weight (g)= 0.0207
Particulate Loading, Dry Std. (gr/scf)= 0.0057
Particulate Loading, Actual (gr/cu ft)= C.0038
Emission Rate (lb/hr)= 3.82
Ho Back Half Analysis
PROG.=VER OS/27/89
07-22-1999 13:16:15
Corr. to 7% O2
0.0050
& 12% C02
0.0046
82
ICal APPENDIX B
-------
* * METRIC UNITS * *
FILE NAME - R23B
RUN. # - 23 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1152-1341
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 24.700
Final Meter Volume (Cubic Meters)= 26.397
Meter Factor= 0.988
Final Leak Rate (cu m/min)= 0.0000
Net Meter Volume (Cubic Meters)= 1.677
3as Volume (Dry Standard Cubic Meters)= 1.587
Barometric Pressure (mm Hg)= 760
Static Pressure (mm H20>= -616
PROG.=VER CS/27/89
07-22-1999 13:1S:15
Percent Oxygen= 5,0
Percent Carbon Dioxide= 14,8
Moisture Collected (ml!= 185.8
Percent Water= 13,5
Average Meter Temperature (C}= ' 38
Average Delta H (mm H20}= 35.9
Average Delta P (mm H20)= 40.7
\verage Stack Temperature (C) = • 85
Dry'Molecular Weight= 30.57
•Tet Molecular Weight= 28.87
Average Square Root of Delta P (mm H20)= 5.9083
's Isokinetie= 100.2
Pitot Coef£icient= 0.84
sampling Time (Minutes)= 100.0
Jozzle Diameter (mm)= - 4.70
Stack Axis #1 (Meters)= 1.676
=tack Axis f2 (MetersJ= 1.448
lectangular Stack
Stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/rnin) = 1,372
rlow rate (Actual, Cubic m/min)= 3,329
?low rate (Standard, Wet, Cubic m/min)= 2,563
?low rate (Standard, Dry, Cubic m/min)= 2,217
Particulate Loading - Front Half
'articulate.Weight (g)= 0.0207
'articulate Loading, Dry Std. (mg/cu m)= 13.0
^articulate Loading, Actual (mg/cu m)= 8.7
Emission Rate (kg/hr)= 1.73
lo Back Half Analysis
Corr. to 7% O2 & 12% C02
11.4 10.6
ICal APPENDIX B
83
-------
FILE NAME - R23B
RUN ft - 23 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1152-1341
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
. 7
' 8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:16:15
Delta P
in. H20)
2
2
2
1
0
2
2
1
0
0
2
2
1
0
0
2
2
2
0
0
2
2
2
1
0
.600
.400
.300
.400
.260
.400
.100
.800
.820
.050
.500
.100
.800
.520
.040
.400
.000
.200
.730
.070
.500
.400
.600
.BOO
.210
Delta K
(in.
2.
2.
2.
1
0.
2.
1.
1 .
0.
0.
2.
1. .
X .
0.
0.
2.
•q
2.
0,
0.
2.
2.
2.
1
0.
H20)
30
10
10
30
23
20
90
60
73
04
30
90
60
56
03
20
80
00
66
06
30
20
40
60
19
Stack
(F)
185
185
185
185
185
185
185
185
186
185
186
185
185
186
185
185
187
186
186
185
185
186
186
185
184
T Meter T
ln(F)
94
94
95
96
98
98
99
100
101
102
101
101
103
104
104
103
103
105
106
106
105
105
107
108
109
Out (F
S3
93
S3
94
94
95
95
96
97
97
98
98
98
•• 100
100
100
100
101
102
102
102
102
103
103
104
Fraction
DRY CATCH
FILTER
Fraction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3339 "3.3156 '0.0000 0.0183
Final Wt. Tare Wt.
(g) (g)
PROBE RINSE 3.4133 3.4109
IMPINGERS O.QOOO 0.0000
Probe Rinse Blank (mg/ml)= 0.0000
Impinger Blank (mg/ml)= 0.0000
Vol.
(ml)
32.7
0.0
Net Wt,
(g)
0.0024
0.0000
84
ICal APPENDIX B
-------
FILE NAME - R24A
RUN # - 24 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1509-1658
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 637.184
Final Meter Volume (Cubic Feet)= 697.063
Meter Factor= 1.011
Final Leak Rate (cu £t/min)- 0.006
Net Meter Volume (Cubic Feet)= 60.538
Sas Volume (Dry Standard Cubic Feet)= 56.789
Barometric Pressure (in Hg)= 29.88
Static Pressure (Inches H20)= -25.88
Percent Oxygen= 5.0
Percent Carbon Dioxide= 14,8
yioisture Collected (ml)= 195.4
Percent Water= .13.9
Average Meter Temperature (F) = 104
Average Delta H (in H20)= 1.41
Average Delta P(inH20)= 1.629
Average Stack Temperature (F) = 185
Dry Molecular Weight= 30.57
net Molecular weight- 28.82
Average Square Root of Delta P (in H20)= 1.1850
\ Isokinetic= 100.1
Pitot Coefficients 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter EInches)= 0.186
stack Axis #1 (Inches)= . S6.0
Stack Axis #2 (Inches)= 57.0
Rectangular Stack
Stack Area (Square Feet)= 2S.13
Stack Velocity (Actual, Feet/min)= 4,567
Flow Rate (Actual, Cubic ft/min)= 119,306
Plow rate (Standard, Wet, Cubic ft/min)= 91,305
Flow Rate (Standard, Dry, Cubic ft/min)= 78,572
Particulate Loading - Front Half
Particulate Weight (g)= 0.0460
Particulate Loading, Dry Std. (gr/scf)= 0.0125
Particulate Loading, Actual (gr/cu ft)= 0.0082
Emission Rate (lb/hr)- 8.40
tfo Back Half'Analysis
PROG.=VER 06/27/89
07-22-1999 13:16:55
Corr. to 7% 02 & 12% C02
0.0109 0.0101
ICal APPENDIX B
85
-------
* * METRIC UNITS * *
FILE NAME - R24A
RUN # - 24 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1509-1658
PROJECT # - 4702.02,04.09
Initial Meter Volume (Cubic Meters)= 13.043
Final Meter Volume (Cubic Meters)= 19.738
Meter Factor= 1.011
Final Leak Rate (cu m/min)= 0.0002
Net Meter Volume (Cubic Meters)= 1.714
Gas Volume (Dry Standard Cubic Meters)= 1.608
Barometric Pressure (mm Hg)= 759
Static Pressure (mm H20)= -657
PROG.=VER 06/27/89
07-22-1999 13:16:55
Percent Oxygen= 5 .0
Percent Carbon Dioxide= . 14.8
Moisture Collected fml)= . 195.4
Percent Water= 13.9
Average Meter Temperature
-------
PILE NAME - R24A
RUN # - 24 - Method 17 TRAIN A for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 150S-1658
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
5
6
1
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:16:55
Delta ?
[in. H2Q)
2.400
2.300
2.000
0.700
0.040
2.400
2.100
2.100
0.750
0.080
2.800
2.400
2. 500
1.500
0.300
2.600
2.400
2.300
1.400
0.260
2.500
2.100
2.000
0.730
0.070
Delta H
(in. H20)
2.10
2.00
1.70
0.60
0,03
2.10
1.80
1.80
0.64
0.06
2.40
2.10
2.20
1.30
0.25
2.20
2.10
2.00
1.20
0.22
2.20
1.80
1.70
0.63
o.os
Stack
CF)
185
185
185
185
185
185
185
185
185
185
185
187
187
187
186
186
186
186
18€
184
184
184
183
183
184
T Meter T
In(F)
101
102
103
104
103
101
103
104
105
106
103
107
107
109
108
106
107
IDS
110
109
107
108
110
110
109
Out (F)
101
101
101
101
101
100
100
101
101
101
101
101
101
102
102
102
102
102
102
103
102
103
103
103
103
fraction
5RY CATCH
'ILTER
'raction
Final Wt. Tare Wt. Blank Wt. Net Wt.
(g) (g) (g) (g)
0.0000 0.0000 0.0000 0.0000
3.3859 3..3452 0.0000 0.0407
Final Wt. Tare Wt. Vol. Net Wt.
(g) {g} (ml) fg)
>ROBE RINSE 3.5600 3.5547 28.2 0.0053
:MPINGERS o.oooo o.oooo o.o o.oooo
!robe Rinse Blank (rag/ml)= 0.0000
'mpinger Blank (rag/ml)= 0,0000
ICai APPENDIX B
87
-------
FILE NAME - R24B
RUN # - 24 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1511-1700
PROJECT f - 4702.02.04.09
Initial Meter Volume (Cubic Feet)= 932.737
Final Meter "Volume (Cubic Feet}= 993.985
Meter Factor= • 0.988
Final Leak Rate (cu ft/min)= . 0.004
Net Meter Volume (Cubic Feet}= 60.513
Gas Volume (Dry Standard Cubic Feet)= 56.738
Barometric Pressure (in Hg)= 29.88
Static Pressure (Inches H20)= -25.88
PROG.=VER 06/27/89
07-22-1999 13:17:51
Percent Oxygen- . 5.0
Percent Carbon Dioxide= 14.8
Moisture Collected (ml)= 199.2
Percent Water= 14.2
Average Meter Temperature (F)= 104
Average Delta H (in H20)= ' 1.48
Average Delta P (in H20)= 1.691
Average Stack Temperature (F}= 185
Dry Molecular Weight= 30.57
Wet Molecular Weight= 28,78
Average Square Root of Delta P (inH20)= 1.2099
% Isokinetic= 100.3
Pitot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
Nozzle Diameter (Inches)= 0.184
Stack Axis #1 (Inches)= • 66.0
Stack Axis #2 (Inches)- 57.0
Rectangular Stack
Stack Area (Square Feet)= 26.13-
Stack Velocity (Actual, Feet/niin}- 4,666
Flow Rate (Actual, Cubic ft/tninj= 121,893
Flow rate (Standard, Wet, Cubic ft/min}= 93,262
Flow Rate (Standard, Dry, Cubic ft/min)= 80,028
Particulate Loading - Front Half
Particulate Weight (g)= 0.0452
Particulate Loading, Dry Std. (gr/scf}= 0.0123
Particulate Loading, Actual (gr/cu ft)« 0.0081
Emission Rate (lb/hr)= 8.41
No Back Half Analysis
Corr. to 7% O2
0.0107
& 12% C02
0.0099
ICal APPENDIX B
-------
* * METRIC UNITS * *
?ILE NAME - R24B
3.UN # - 24 - Method. 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1511-1700
PROJECT # - 4702.02.04.09
Initial Meter Volume (Cubic Meters)= 26.411
?inal Meter Volume (Cubic Meters)= 28.145
*feter Factor= 0.988
?inal Leak Rate (cu m/rnin) = 0.0001
ffet Meter Volume (Cubic Meters)= 1.713
5as Volume (Dry Standard Cubic Meters)= 1.S07
Barometric Pressure (mm Hg) = 759
Static Pressure (ram H20)= -657
Percent Oxygen= 5.0
Percent Carbon Dioxide= 14.8
toisture Collected (ml)= 199.2
Percent Water= 14.2
Average Meter Temperature (C)= 40
Iverage Delta H (mm H20)= 37.€
Average Delta P (mm H20)= 43.0
Average Stack Temperature (C) = 85
5ry Molecular Weight^ 30.57
«Tet Molecular Weight= 28.78
Average Square Root of Delta P (mm H2Q) = 6,0975
i> Isokinetic= 100.3
PROG.=VER 06/27/89
07-22-1999 13:17:51
?itot Coefficient= 0.84
Sampling Time (Minutes)= 100.0
fozzle Diameter (mm)= 4.67
Stack Axis #1 (Meters)= 1.676
Stack Axis #2 (Meters)= 1.448
Rectangular Stack
stack Area (Square Meters)= 2.427
Stack Velocity (Actual, m/rain)= 1,422
?low rate (Actual, Cubic tn/min) = 3,452
riow rate (Standard, Wet, Cubic m/min)= 2,641
.'low rate (Standard, Dry, Cubic m/min) = 2,265
Particulate Loading - Front Half
Particulate Weight (g)= 0.0452
?articulate Loading, Dry Std. (mg/cu m)= 28.1
Particulate Loading, Actual (mg/cu m)= 18.5
Mission Rate (kg/hr)= 3.82
sfo Back Half Analysis
Corr. to 7% O2 & 12% C02
24.6 22.8
ICal APPENDIX B
89
-------
FILE NAME - R24B
RUN # - 24 - Method 17 TRAIN B for PM
LOCATION - Unit 2A Baghouse Outlet Duct
DATE - 07/19/99 Time: 1511-1700
PROJECT # - 4702.02.04.09
Point #
1
2
3
4
S '
6
- 7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
PROG.=VER 06/27/89
07-22-1999 13:17:51
Delta P
(in. H20)
2. 700
2.500
2.000
1.300
0.250
2.600
2.500
1.800
0.820
0.120
2.500
2.100
1.900
0.730
0.080
2.500
2.500
2.500
0.950
0.050
2.700
2.700
2.500
1.600
0.280
Delta H
(In.
2.
2.
»L *
1 .
0.
2.
2.
1.
0.
0.
2.
1.
1.
0.
0.
2.
2.
2.
0.
0,
2.
2.
2.
1.
0.
'H20)
30
30
70
10
21
30
20
60
71
10
20
80
70
€4
07
20
20
20
83
04
40
40
20
40
24
Stack
(P)
185
185
185
185
185
185
135
135
185
185
187
187
186
186
185
186
186
186
186
185
185
184
183
184
186
7 Meter T
In(F)
99
99
100
101
102
102
103
104
105
106 '
105
105
107
108
108
107
107
109
110
110
108
108
110
111
111
Out (F
98
99
99
99
100
100
100
101
101
102
102
102
103
103
104
104
104
105
105
105
105
105
106
106
107
Fraction
DRY CATCH
FILTER
Fraction
Final Wt . Tare Wt . Blank Wt . Net Wt
0.0000
3.3124
0.0000
3.2717
PROBE RINSE
IMPINGERS
Probe Rinse Blank (mg/tnl)
Final Wt. Tare Wt.
(g)
-------
ICal Appendix C
M17 Field Sampling Data Sheets
MW.OPPT*47(B-
-------
-------
40 CFR 60, APPENDIX A, METHOD 1 -
LOCATION OF TRAVERSE POINTS IN A RECTANGULAR DUCT
MRl Project No.
Client/Source:
Source Location:
Sampling Location:
Date:
4702.02.04,09
U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Rocky Mount, North Carolina
BaghousaJFabric Fiiter) Outlet Duct
-7-8-79
For Run Numbers: All
'« A-5
A-4
A-3
e A-2 «
A-1
o
tO
to
! 57 inches
Compass Direction )**•
Flow is away from observer and is downward
r' '»•
Inside of far wall to outside of port (Distance A):
Inside of near wall to outside of port {Distance 8);
Traverse distance (A - B):
internal duct dimension normal to traverses:
Equivalent diameter:
Cross-ssctionai area of'duct:
Number of test ports:
Distance between port centers:
Distance of nearest flow disturbance upstream from ports:
Distance of nearest flow disturbance downstream from ports:
Number of test points per traverse (i.e., per port):
Distance between test points on a traverse:
Dimensions obtained by/from: direct measurements and blueprints
Data recorded by:
COMMENTS:
gt.o
11,. 0
66.0
57.0
61.17
26.125
5
11.4
82
128
5
13.2
inches
inches
inches
inches
inches
square feet
inches
inches
inches
inches
DUCTRECT.WPD October 14, 1998 («», DUCTRECVWFD July 2, 19991
ICal APPENDIX C
-------
SAMPLING NOZZLE CALIBRATION CHECK DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cugentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter) Outlet Duct
Nozzle !.D. Number or
Dedicated Sampling
Train Number
Nozzle Type
(Shape and Material
of Construction]
Three Measured Diameters, inches
D1 D2 D3
Average
Diameter,
inches
Measured By
Date
if
0J9&
o
EL
fe
*0
I
n
it
7
COMMENTS:
HOZZtCAX.WrD April 29, 1S9B |r«v. NOZZLCAKWPD July 2, 19991
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
£
o
Run No, fO Date
- &L
Project No, ,
Client Ctt^
Source
Sampling Location.,i
Operator.
Record data every
Barometer No. V
Barometric Pressure
Elevation to Metar Boxes.
Meter Box Phar _%
minutss
. in Hg
ft
Elevation to Sampling Loc.
Sampling Locatio/P
Static Pressur
. in Hg
ft
, in Hg
>/
H20
Train A No. ________________A~-L^i^Z2^l^_
Probe No. A Length: /** ft
Nozzle No. flltf* /!• Tip Dia, rffi in
Pitot Tube No. 4- C. .> 9^
Stack Thermocouple No, ?/#V"*A
Filter Holder No. 3
Filtar Assembly No. /&
Imoinaer Box No, A "I
Umbilical/lmpincjer Hookup Hff^ty
Umbilical No. 4/*3<2'>
Meter Box No. f\J \&
DGM Correction (Y) // <£'//_
Orifice Meter fiHffi /£ £V
Train 6 No. O ~~ / Tip Dia. , tUftf in
Pilot Tube No. £? C, "*f
Stack Thermocouple No. "J/53r" 0
Filter Holder No. H*
Filter Assembly No. / '
Imoinaar Box No, fl~£~
Umbilioal/lmpinqer Hookup HnJ^~
Umbilical No, /J*5&- f
Meter Box No, /\J "~/f
DGM Correction (Y) 1 7}?$
Orifice Meter AH® f'r*?&0
page 1 ol.
Traversa Point Layout
Assumed Moisture
Assumed %CO2
. %02
T
Time (24 Hr)
Pass or Fail
— /— ^. — • — — . i " ^— — •
Train A Pitot Tuba Pressure Measurement System Leak Checks
Initial
dyyi
Final
,(,03
j Q*«4^
Initial
Final
Initial
Final
initial
Final
|
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
df¥g
Final
&H
pWJ>
Initial | Final
1
Initial
Final
Initial i Final
i
Initial
Final
Train A Sampling System Leak Cr
Time (24 Hr)
Vacuum, in Ha
Leak Rate, ufm
Initial
o^t
&
.*•?
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
M
( A
,005
Initial
Final
initial
Final
Initial
1 — r
j
1 1
Final
Initial | Final
]
^_L
Remarks and Notes: List any other equipment requiring calibration below.
M17DPG1.WPD Juiy 2, 1998
TRAIN B
Meter Volume at Stait of Run
Metar Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
-------
Run No,
Date
Sampling Location
Project No.
/ucf &vff«'
page
f of
Operator.
Sampling Data for Method 17 Train A No. $ "/
Traverse
Point
Sampling
Time,
min,
t,
8-
Clock
Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
k_£
\toof.
/Cff /,
Velocity
Head
Orifice Pressure
Differential
(AH),
in. HO
Silica Gal
Impinger
Outlet [
Temp.,
°F
Sampling Data for Method 17 Train B No.
•7-7
-71
f/
57
a
o&rt l/tfof.
J3^^
1!
J3L
2S_
57
52-
&*L
mn
jsJL.
•7
fff
*?#
JjL
Af
n
fr
&L.
ft
2.3-
X2.
/.&•
J3$
1W
ffft-
83
tort
fff
n
•2,7
£5
*-
^ZL
-------
Date
Run No.
Project No.,
Sample Type (J/iuhPF§I3i, Single-Point)
Flow Control Device (J^ajvejCritical Orifice)
Method 5 Meter Box No. f/'^G
MSB Pump Type
MSB Pump No.__
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
-l5~??__ Client/Source £*
Sampling Location
Operator.
Bag Type
Method SB Train No. _
MSB Flow Meter Type
MSB Flow Meter No.
. Sample No.
A/-A
Desired Sampling Rate _
Leak Check Before Sampling
Total Sampling Time f?
cc/min
£7
Flow Rate, cc/min: Average
Estimated Total Sample Volume
After Sampling
min Average Flow Meter Reading
Highest
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start Stop
Sampling Sampling
Sampling
Remarks and Notes
1.0
#9 /?
1*0
fffrff
"3,0
yassAMP.wPD June 18.1988
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BV ORSAT
o
Run No,
Project No,
Sampling Location _.
Analysis Start Time
Sample Type (Bag, GrSB]
Analyst __
Date
Sample ^kf.
Orsat Leak Check Before Analysis:
Burrete Ao Change in 4 Minutes
Pipettes /rf& Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete ^j^& Change in 4 Minutes
Pipettes /fo Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Nat is actual reading
minus actual O2 reading)
1
Actual
Reading
1 &&
2 JSf'S~ •
3
1 06.3-
2 j#p,5""
3
1
2
3
Net
Value
J5,15
5>c>
2
Actual
Reading
1 />-d&>
2 /%£.
3
1 /96
2 /$,&
3
1
2
3
Net
Value
/7'fs
j£@
3 >^/
Actual
Reading
1 M& M^
2 /^ Mi
3
1 &£ }9,t>
2 /?£ 1$,^
3
1
2
3
Net
Value
*»
/*46
&$
Average
Net
Value
{% v/v)
/4^£
£",&
Acceptance Criteria per Method 3B
CO2 >4% 0.3% v/v
<4% 0,2% v/v
02 >15% 0.2% v/v
<1&% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
M3BANAL.WPO May 28, 1993
-------
40 CFR BO, APPENDIX A, METHOD 17 - PARTICIPATE MATTER TRAIN [Ml 7)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02,04.09
Client/Source: U.S. EPA OAGPS EMAO EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. JO Sampling Train A No, ../*J./y~f1 tmpinger Box A No..
Sampling Train B No. /*}}'*?*'% Impinger Box B No.,
Set-up person(s): J .' Stj^rylP^i _ Date:
Transfer to Sampler: .
Relinquished By J, •fn.ts'mzir-i Received By £2. <$/•/ 'h' a Date/Time
...... _ TRAIN COMPONENT __ REAGENT __ , _ LOADING DATA
. ... TRAIN A . TR AIM B
Sampling Nozzle (Quartz)* Nozzle I.D. No. /*)*•?' i"2- SVj 7-7
Filter Assembly and Holder* • Filter Assembly No. _ Xo /y
Filter Type: Whatman 334-AH
Probe (31 6 SS) Filter Holder Mo. & _ V
Sampie Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off • •
" • Initial Weights (grams)**
1st Impinger (Mod-GBSS 100 mis ASTM Type I Water ' ' _
U-Connector (A!
2nd Smpinger (GBS) 100 mis ASTM Type 1 Water
U-Connector (B)
3rd Impinger !Mod-QBS) Empty _
U-Connector !CS
4th Impinger (Mod-QBS) "200 g indicating silica gel • 7/ fy &ys,7
Impinger Outlet Connector Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon8 tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impinger inlet sealed with glass blank-
off,
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17DSUP.WPD May 13, 19SS (rev. MI17DSUP1.WPD July 2, 19931
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /& Sampling Train A No. SZ?/~?-*} Impinger Box A No..
Sampling Train B No. Slffs7-<& Impinger Box B No. _
Transfer for Recovery:
Relinquished By JPLj&^jf-feg _ Received By t),• &fj**3* Date/Time
Sample recovery person(s): &>QQ2 '. jff 004
PM Description/color: &1<3C/*- J?Jsts<
TRAIN RINSES;
Sample Number: /£ 001 />& 003
Simple Bottle Tare Wt. _
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. with Acetone Rinsss
Net Acetone Sample Wt. '
Sample Bottle Final Wt. /r/7 f*r? with added Water Rinses
Net Water Sample Wt.
* Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow wit!
ASTM Type I watsr rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until aftei
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M15DSCV.WPD May 13, 1999 (rev. M17DRCV1.WPD Jyly 2. 1998)
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
page 1 of.
Run No. /f Date f-ff-f
Project No.
Client £T<»«t*
y/'^.-^z-
AiV
sj
Source i&rkjx,^, "iti
*u
Sampling Loca
Operator ^
Record data 8'
Barometer No
Barometric Pr«
Elevation to IV
Meter Box Pbtf
Elevation to S
Sampling Loot
Static Pressur
Time (24 Hr)
Pass or Fail
tion "yuxef- CWf Lit
3WP»w
/ery T minu
W%~(0f
sssure jQtCtf in
eter Boxes 3^*
•?
*T
V
---^-^-^
\ « ^
^
5^r
^\
1 I
^
>^/
\
/
t-J «-- • <-J i— J pv
A 0 0 17 £
Traverse Point Layout
y % Assumed %CO, ^^7>i<%O, ftf $**>
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial Final Initial
irw
Final initial
Final
Initial
Final
Initial
Final
Ji") Jr4
Train B Pitot Tube Pressure Maasuremant System Leak Checks
Initial
fn^
Final
/?¥?
L,^*^
Initial
Final
Initial
—
Final
Initial Final
Initial
Final
Train A Sampling System Leak Cfhaeks
Time (24 Hr!
Vacuum, in Hg
Leak flate, cfm
Initial
(\lb
if
.00%
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Firm!
l^J
-------
Run No.
Date
JL
Sampling Location
Project No.
Operator &
page.
I of
Sampling Data for Method 17 Train A No. A -2-
10
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. U_
Date
Project No,.
Sample Type
Single-Point)
Client/Source
Sampling Location
Operator
IX
Flow Control Device
-------
40 CF/? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
1
n
Run No.
Project No.
Sampling Location
Analysis Start Time /&&"&•
Date
Sample J^cfT
Sample Type (Bag,J3fatrl .
Analyst 3<5*
2 y^x?*'
3
1
2
3
Net
Value
J#,£y~
&,O
Average
Net
Value
(% v/v}
J&3~
&?&
Acceptance Criterjp per Method 3B
C02 >4%0,3%v/v 02 ^15% 0.2% v/v CO
<4% 0,2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.WPD M»y 28, «989
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.03
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter) Outlet Duct
Run No. /' Sampling Train A No.
Sampling Train B No.,
Set-up person(s): (J.
Transfer to Sampler: s
Relinquished By O
Impinger Box A No..
Impinger Box B No..
Date:
Received By O,
Date/Time
'••jf-
TRAIN COMPONENT
JEAGENT
LOADING DATA
TRAIN A
TRAIN 8
Sampling Nozzle {Quartz)*
Filter Assembly end Holder*
Filter Type: Whatman 934-AH
Probe {316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle l.D. No.
Filter Assembly Wo.
Fitter Holder No.
8
initial Weights (grams)**
1st Impingsr (Mod-GBS) 100 mLs ASTM Type I Water
U-Conneetor (A)
2nd Impingar (GBS) 100 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Jmpinger (Mod-GBS) "200 g indicating silica gel
Impinger Outlet Connector
Connector t.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon* tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered hera.
Component Changes After Set-up And Before Recovery And Other Comments:
M17PSUP.WPD May 13, 1M8 Irev, M17DSUP1.WPD Julv 2.1988!
ICal APPENDIX C
13
-------
40 Cf/7 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (Ml 7)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR! Project No. 4702.02,04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No. Xffi/:?^/?
Sampling Train B No. S??J'7''&
Transfer for Recovery:
Relinquished By •Dt&fiT-h'^) Received By .
Impinger Box A No.
Impinger Box B No.
Date/Time
Sample recovery person(s):
Weights below are in grams.
•J>
Date: ^7-
BACK HALF RECOVERIES
TRAIN A
JRAIN.-B-
Impinger: 1st
Final Wt.
Initial Wt.
Net Wt. ..
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th
1st
2nd
3rd
4th
*,*
Biue
% Blue
TRAIN A
TRAIN B
001
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt,
Components Rinsed*: nozzle, fitter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt.
Sample Bottle Final Wt.
Net Water Sample Wt,
^004
003
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean, if any residue remains in a component, follow witi
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
7
M17DfiCV,Wra May 13, 19B9 (rev, M17DRCV1.WPD July 2, 1998}
14
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
EL
o
Run No, (?" Date f^/7-^ff
Project No. ¥fa2-#
d ient CtsijlfrH^C-f ^.
S
Source t3«K-&#*®V 2-*-'
Sampling Location i"*t/
/».(?>
Record data every
Barometer No. V^
Barometric Pressure '
^^^f
minutes
«*/
tot03 JnHq
Elevation to Meter Boxes 77 ft
Meter Box Pb:l
Elevation to Sampling Lc
Sampling Location Pfc,r
Static Pressure ' — J2£-
Train
Initial
Time (24 Hr) 7P"5 |
Pass or Fail
3>. y^-yy in H2O Assumed
@
/,XP?<9
Moisture /£-*•&
Train B No,
Probe No.
25
£
Nozzle No.ffff-Tft
Pilot Tube No, ^
Stack Therrnocoupl
Filter Holder No.
Filter Assembly No
Impinger Box No,
Umbilical/lmpinger
Umbilical No. A/
^/^?
Leng
. Tip Dia
e No. '
-7
. W
$-
Q\:J*_
cp <%*>
/
5T
ft
in
f
5
Hookup Ujf'fa-
'&'/
Meter Box No, /v ff
DGM Correction (Y) _&-t.'i
Orifice Meter AH@ /.
% Assumed %CO, /^O %
A Pilot Tuba Pressure Maasurement System Leak Checks
=inal ! Initial Final
m
Initial
Final
Initial
Final
Initial
Final
,rt
e:
/
jx
A
/
\
page 1
<
\
\ "
•*-.
of f
*">N?
"" 1 ? \
Jl/'
' '^1
LJ \^ ~-u—"Cj — tr~ '
ft 13 c -p g
Traverse Point Layout
o, 5:5
Train B Pitot Tube Pressure Measurement System Leak Checks
initial
(fLa
Final
f4%
J^4_
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train A Sampling System Laak Checks
Time (24 Hr)
Vauiium, HI HB
Leak Rats, cfm
Initial
i^fn-
f
-------
Date
Sampling Location
Project No.
Operator.
page.
J_of.
Sampling Data for Method 17 Train A No. /L ~/
Remarks and Notes;
M17DPB2.WPD July2, 1398
16
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No.
Project No. _
Sample Type
luIti-Pojrrp Single-Point)
Flow Control Device (ft£|lve[£JCrrtical Orifice)
Method 5 Meter Box No. //-/eg
M3B Pump Type ~L
MSB Pump No
Client/Source
Sampling Location
Operator
Bag Type
Sample No.
Method 3B Train No. _
MSB Flow Meter Type
MSB Flow Meter No.
Desired Sampling Rate .
Leak Check Before Sampling
Total Sampling Time
cc/min
After Sampiing g_
Flow Rate, cc/min: Average _
Estimated Total Sample Volume ,
min Average Flow Meter Reading
Highest
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
ft 91
M3BSAMP.WPD JynB IB, 1998
17
ICaJ APPENDIX C
-------
oo
E
o
40 CF/? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Project No,
Sampling Location _
Analysis Start Time
Sample Type (Bag, G«rtJS
Analyst
Date
SamplBjW,
Orsat Leak Check Before Analysis:
Burrete /^> Change in 4 Minutes
Pipettes S^o Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete A'P Change in 4 Minutes
Pipettes _/?^ Change in 4 Minutes
Analysis
Gas
CO,
Oj (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
2 j*/ $f
3
1 W3
2 /9'3
3
1
2
3
Net
Value
/yj
44*
2
Actual
Reading
2 /# &"
3
1 /9.3
2 /f,J
3
1
2
3
Net
Value
JM
tf*&~
3
Actual
Reading
2 t?,?
3
1 /9.J
2 /^^y
3
1
2
3
Net
Value
,*r
*£&'
Average
Net
Value
(% v/v)
M+
&£>"
Acceptance Criteria per Method 3B
CO2 > 4% 0.3% v/v O2 £15% 0.2% v/v CO 0.3% v/v
<4% 0.2% v/v <15% 0.3% v/v
Remarks and Notes:
M3BANAL.WPD Ma^ 28, 1399
•7 In If i
-------
40 CFfi 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRASN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EM AD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No, /£* Sampling Train
Sampling Train
Set-uo oersonfs}; w? Swx-xw-
Transfer to Sampler:
Relinquished By J» SMT'JVI^T-
TRAIN COMPONENT
A No. ^y/7'79
B NO. syy/y-j?
Received By £/*
REAGENT
imainqer Box A No. r? "/
Imoinaer Box B No, &~j
Date: #7*/5"-^?
&1fS"f~"Tin Date/Time £>7-J&"-"9*^ S&£>O
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman &34-AH
Probe (316 SS) :
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Mozzle I.D. Mo. /^V/^^-
Iter Assembly No. _
Filter Holder No.
Initial Weights (gramsl**
1st Impinger !Mod-GBS) 100 mis ASTM Type I Water
U-Connector (A) . : • .•
2nd Impinger (GBS) 100 mLs ASTM Type i Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-QBS) "200 g indicating silica gel
>)
Impinger Outlet Connector
Connector I.D. No.
"i2(>
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impingsr inlet seated with glass blank-
off.
** Initial weights of additional componants exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
7//7/ff
M17DSUI».WPD May 13. 1999 (rev. M17OSUP1.WPO July 2. 19SS)
ICal APPENDIX C
19
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR! Project No, 4702,02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
4 Sarnpiing Train A No,
Sampling Train B No.
Transfer for Recovery:
Relinquished By D> '^/>>>
Sample recovery person(s): t/«
Weights below are in grams.
-Q
Impinger Box A No.
Impinger Box B No.
Received Bv
Datenime
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt. .
Initial Wt. .
Net Wt. /?£7
2nd
3rd
V9&5"
4th
1st
2nd
3rd
4th
7,7
Total Condensate Coliactsd:
Description and/or color:
% Blue
% Blue
FRONT HALF RECOVERIES.
TRAIN A
TRAIN B
/*% 002
001
FILTER ASSEMBLY:
. Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt.
Components Rinsed'*; nozzle, filter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt.
Sample Bottle Final Wt.
Net Water Sample Wt.
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 Times or more until perceivably clean. If any residue remains in a component, follow wit!
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afta
the bottle is weighed with all of the acetone rinses.
COMMENTS:
fS
M17DRCV.WPO May 13, 1899 (,ev. M17DRCV1.WPD July 2, 1999)
20
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
E.
1
n
Run No. P
Project No.
Client _
Source
Data
Sampling Location
Operator
Record data every
Barometer No.
Baruiiielriu Pressure
Elevation to Meter Boxes
Meter Box P,
Elevation to Sampling Loc,
Sampling Locati
S/,
Static Pressur
Train A No. 4"^ /PS?-*?
Probe No. 4 Lerath: /# ft
Nozzle No, rtff?-£ Tio Dia. '^«7 in
Pilot Tuba No. /f Cp .&i
Stack Thermocouole No, ^ ' yf~ **"
Filter Holder No. /
Filter Assembly No, •2.V
Impinger Box No. /?-'2_
Urnbilical/tnipiiiuer Hookup M,ff^-
Umbilical No. /«/#" ^
Meter Box No. /V f&
DGM Correction (Y) f~Oi]
Orifice Meter AH P t. 8^ *>
Train B No. __fc*=_ /W-8
Probe No. # Lenoth: /tf ft
Nozzle Ho.lVf^"^ Tio'Dia. -/f'5" in
Pilot Tube No. "B Cf ' ^l
Stack ThermocouDle No; "T/45* ^
Filter Holder No. ~Z-
Filter Assembly No. 'IS
Impinaer Box No. a~2~
Umbilical/lmpifiper Hookup &fff 1
Umbilical No. /V^"-/
Mater Box No. jM ff
DGM Correction (Y! ~~ jf^-* 6«K^
Traverie Point Layout
Initial Final Initial Final
Time (24 Hr]
Vacuum, in Hg
Leak Rate, cfm
Initial
/l#fc
rf
,ara3
Fin a i Matar Volume
initial Meter Volume
Leak Check Volume
Final
lt>W '
10
_^^i^
Initial
Final
initial
Final
Initial
Final
Initial
I
Final
Train B Sampling System Leak Checks
Time (24 Hr}
Vacuum, in Hg
Leak Rate, cfm
Initial
JJiuSS^&iJiiL^
Final Mater Volume
Initial Meter Volume
Non-sample Volume
F
^
in1
nal
(5
3
_^
Initial
:
Final
Initial
i
I
j
t
Final
Initial
Final
Initial
• • •
Final
Remarks and Notes: List any other equipment requiring calibration below.
M17DPO1.WPO July 2. 1993
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Voiume
Adjusted Firiel Volume
[00 f~ Nfe-
-------
Run No.
Date
-/&-?*?
Sampling Location
Project No,
Operator
page .
of
Sampling Data for Method 17 Train A No. A-_Z-_
Traverse
Point
Sampling
Time,
min,
Clock
Time
(24-Hr)
Dry Gas Meter Reading
-------
Date
Run No. /3
Project No. _
Sample Type {<|$ujti-Ppjrv£pSingle~Paint}
Flow Control Device |Vaivg) Critical Orifice]
Method 5 Meter Box No. X//C"
MSB Pump Type
i ~J~
MSB Pump No. A/-fa
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
-/I?"?'? Client/Source £c'*ie*sh-\
Sampling Location
Operator
Bag Type
Sample No,
Method 38 Train No. _
MSB Flow Meter Type
MSB Flow Meter No.
Desired Sampling Rate
Leak Check Before Sampling,
Total Sampling Time
-------
40 C«? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
O
fe
s
n
Run No.
Project No.
Sampling Location
Analysis Start Time //3£>
Date
Sample Ma,
ff/9
Sample Type (Bag, firsts).
Analyst £
Orsat Leak Check Before Analysis;
BurreteJ& Change In 4 Minutes
Pipettes sri* Change in 4 Minutes
Orsat Leak Check After Analysis;
Burrete tfe> Change in 4 Minutes
Pipettes W& Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual Oz reading)
1
Actual
Reading
1 /$,&
2 /%£>
3
1 /V
2 y^y
3
1
2
3
Net
Value
/j£fe>
£",%
1
Actual
Reading
1 /?^
2 /JKJ-
3
1 /£y
2 /?,y
3
1
2
3
Net
Value
/££
•&.y
3
Actual
Reading
1 /?•&
2 X^1,^-
3
1^^
2 /£/
3
1
2
3
Net
Value
/3,&
jSTJ*
Average
Net
Value
(% v/v)
/5t<^
^S"
Acceptance Criteria per Method 3B
COZ >4% 0.3% v/v
<4% 0,2% v/v
02 ^15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
M3BANAL.WfD May 28. 1399
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTiCULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No, 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location; Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No,
Sampling Train B No.
Irnpinger Box A No,
Imptnger Box B No.
Set-up personls):
Transfer to Sampler;
Relinquished By f),
Date:
TRAIN COMPONENT
Received By €?,
REAGENT ..._.
Date/Time
J.QAD1MG.DATA
TRAIN A
,TRAIN_B_
Sampling Nozzle fQuartz)*
Filter Assembly and Holder*
Filter Type: Whatman 334-AH-
Probe I316SS1
Sample Transfer/Vacuum Line
Male 1st jmpinger Inlet Blank-Off
Wozzle I.D. ho.
Filter Assembly No
fitter Holder No.
1st Impinger (Mod-GBS) 100 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS! 100 rnLs ASTM Typo \ Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
. U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gei
Impinger Outlet Connector
Connector I.D. No.
Initial Weights (grams)*
* Before and after sampling; Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon* tape, and
entirs filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
Mt70SUP.«VPD May 13. 1399 (rev. M170SUP1.WHJ July 2, 1899)
ICal APPENDIX C
25
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
2 Impinger Box A No..
[ Impinger Box B No.,
Sampling Train A No.,
Sampling Train B No,.
Transfer for Recovery:
Relinquished By j7. &fiTf>r> Received By .
Sample recovery person(s): J
Weights below are in grams.
Date/Tima
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
&V.9
4th
1st
2nd
3rd
4th
. %Blue
% Blue
FRONT HALF RECOVERIES
TRAIN A
...TRAI.N....B
/-? 001
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt.
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. _
Net Acetone Sample Wt, _
Sample Bottle Final Wt.
Net Water Sample Wt,
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow witl
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
f J
M17DRCV.WPD May 13. 1899 Ireu. M17DRCV1.WPO July 2. t9S9!
26
ICaJ APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
e.
o
Run No. 17 Date.
Project No.
Client
Source ,
Sampling Location,
Operator
Record data every
Barometer No,
minutes
Barometric Pressure
Elevation to Meter Boxes _
Mater Box Pm, j?
in Hg
J£:
•W
. in Mg
ft
\No. ' /£•"/ J&S7V&
No, /i1 Lanath: / in
uba No. ,4- Cp . of
Thermocouple No, JfSff.'A
-\older No. *)
Assembly No. "££>
er Box No. A "/
cal/lmpinaer Hookup (An "*>;
cal No. V "55^3
Box No. /4/JC3
Correction (Y) /-£»//
Meter AHi> ffff^O
Train B No. (?^f /&S7~&
Probe No. Q Length: Ks ft
Nozzle No./Jtr?-' f5 Tip Dia. £?¥ in '
PitotTubeNo. f3 Cp ^fi1/ i
Stack TliennocQuple No. 3lS"S''"O
Filter Holder No. 7*
Filtar Assembly No, ^"J?"
Impinqer Box No. ^ - /
Umbilical/tmninaer Hookuo L?tt-'^'~2-
Umbilical No. A/ July 2, 1S93
Meter Volume at Start of Run
Meter Voluma at End of Run
Total Leak Check Volume
Adjusted Final Valuma
-------
Run No. /•/
Date T-jg.-ff
Sampling Location
Project No. f" "
Operator.
page.
of ;
Sampling Data for Method 17 Train A No. A V
Traverse
Point
3-
Sampling Clock
Time,
min.
Time
(24-Hr!
Dry Gas Meter Reading
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No.
Project No,,
Sample Type (My}i!"^2l5^' Single-Point)
Flow Control Device?5&£_
Method 3B Train No. .
MSB Flow Meter Type
MSB Flow Meter No.
Sample No,
Desired Sampling Rate _
Leak Check Before Sampling.
Total Sampling Time ^5
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
& After Sampling
min Average Flow Meter Reading .
•g
-------
o
e,
J5
n
Run No.
40 CFR 60, APPENDIX A, METHOD 3B. GAS ANALYSIS BY ORSAT
•7-M
Project No.
Sampling Location _
Analysis Start Time
Sample Type (Bag, iJKrtJf.
Analyst t//
Date
Samplejikr,
Orsat Leak Check Before Analysis;
Burrete "& Change in 4 Minutes
Pipettes Afo Change in 4 Minutes
Orsat Leak Check After Analysis;
Burrete _/*& Change in 4 Minutes
Pipettes >^ig Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual 02 reading}
1
Actual
!__Reading
!Atf
2 W,&
3
1 /2j£
2 J9/3
3
1
2
3
Net
Value
f9tf?
f/^7
2
Actual
Reading
i/#>
2 /W
3
1 /93
2 tf,3
3
1
^2
3
Net
Value
/?'&>
Y>7
3
Actual
Reading
1 W,t*
2 M,£?
3
1 J*J
2 )93
3
1
2
3
Net
Value
W,&
*J,~l
Average
Net
Value
{% v/v)
/1t-t>
V, 7
Acceptance Criteria per Method 3B
C02 >4%0.3%v/v
<4% 0.2% v/v
O2 ^15% 0,2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
MJBANAL.VMPD May 2B. 1899
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /y
Set-up personis); .
Transfer to Sampler:
Relinquished By s
Sampling Train A No.
Sampling Train B No.
Impinger Box A No. /? ~ /
Impinger Box B No. J& ^"j
Date;
Received By
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
/£ /5>"
TRAIN. A
..TRAIN B..
Sampling Nozzle {CuartzJ*
Filter Assembly and Holder*
Filter Type; Whatman S34-AH
Probe (318 SS)
Sample Transfer/Vacuum Lins
Male 1st Impinger Inlet Blank-Off
Kozrlf I D. Nn.
Filter Assembly No.
Filter Holder No.
1st Impinger (Mod-GBS) 100 mLs ASTM Type I Water
U-Connector (A)
2nd tmpinger (GBS) 100 mLs ASTM Type 1 Water'
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
Impinger Outlet Connector
Connector 1.0. No.
Initial Weights (grams)**
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc® bag. 1 st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Commants:
M17OSUP.WPD Msy 13, 1898 (rev. M17DSUP1.WPD July 2, 1999
ICd APPENDIX C
31
-------
40 CFR 60, APPENDIX A, METHOD 17 - PART1CULATE MATTER TRAIN (Ml 7)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
T Sampling Train A No..
Sampling Train B No..
Transfer for Recovery:
Relinquished By £•*» &J"rrT»*~> Received By.
Irnpinger Box A No.
Impinger Box B No.,
DatefTime
Sample recovery psrson{s):
Weights below are in grams.
a> •
Date:
BACKHALFRECDVEBIES
TRAIN A
TRAIN B
Impinger; 1st
Final Wt, .730*5
Initial Wt,
Net Wt.
2nd
3rd
4th
1st
2nd
3rd
Total Condensate Collected:
Description and/or color:
4th
***.>
^93.2
% Blue
% Blue
gRONT HALF RECOVERIES .
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt,
Components Rinsed*: nozzie, filter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt,
Sample Bottle Final Wt.
Net Water Sample Wt.
with Acetone Rinses
with added Water Rinses
* Acetone rinses with brushing 3 times or mare until perceivably clean. If any residue remains in a component, follow wit
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afte
the hottie is weighed with all of the acetone rinses.
COMMENTS:
M17DRCV.WPO May 13, ISBStrev. M17DRCV1.WPD July 2. 1999)
32
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
n
s
n
Run No
Client
Source
o, Date
t No. ti1OZ-'~Cil
{satmbW
i 1 %^ ^vis^*^**" t^-*^*
ina Location w^T 0
tor ScnUf
U
d data every
leter No. V4-'1*'
letric Pressure "30 «
ion to Meter Boxes
Box PtM 1»5, a
ion tG Sampling Loo.
ing Location P^r 3°
-HMf
'wfM"
minutes
C^ in Ha
^ ft
in Ha
^f ft
» * <> in Ha
Train A No. fl "2-'
Probe No. ft- Lenath: (° ft
Nozzle No. M (1 'tr Tip Dia. , /ffJf in
PitotTubeNo. fl Cc ,ff
Stack Thermocouple No. *??7?~^
Fitter Holder No, £?
Filter Assembly No. '^-'S
Impingar Box No. /rV"2-
Umbilical/lmDinaer Hookup MfjT-
Umbilical No, ^v/^'*^
Meter Box No. /\/ [a
DGM Corraction (Y! [f^H
Orifice Meter AH@ _ff ff
Train B No. I)""?-*-
Probe No. 1? Lenath: r*$Tfc
Filter Holder No. 5"
Filter Assembly No. ^-7
Impinqar Box No. R>"2-
Umbilical/imDinaBr Haokuo t< fr *"/
Umbilical No. Al ^^ " /
Meter Box No. N/ M
DGM Corraction (Y) O. ?%&
Orifice Meter AH@ fr 9&
page 1 of f_
/f. p. e p
Traverse Point Layout
Static Pressure
H2O Assumed Moisture
/"2 -
% Assumed %CO,
5; <
Time (24 Hr!
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
Final
p*°
!
Initial
Final
Initial I Final
Initial
Train
Final
A Sarr
Initial
ipiing £
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
• K1^6
ystem
LeakC
Final
(7tV
necks
Initial
Final
Initial
Final
Initial
Final
Initial Lfinal
1 1
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
tftf
^_JX_^^-
^ 1
Final Meter Volume
Initial Mater Volume
Leak Check Volume
Final
(I'M
la
.Off*)
Initial
Final Initial
j
Final
Initial
1 -
LUZZH]
1
Final
Initial Final
CO
CO
Train B Sampling System Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, dm
Initial
iWi
IS
g0
Final Meter Volume
Initial Meter Volume
Non-sample Volume
LZ
Final
n<-
,a2f
Initial
Final
Initial
Final | Initial
!
I
Final
Initial j Final
|
Remarks and Notes: List any other equipment requiring calibration below.
f$
7/nhi
JBAlfcLA
TRAIN B
MI7OPG1.WPO July 2, 1999
Meter Volume at Start of Run
M0ter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
&
-------
Run No.
Date
Sampling Location
Project No.
2*
page.
/ nf 1
Operator
Sampling Data for Method 17 Train A No. A '
Traverse
Point
Sampling
Time,
min.
Clock
Time
(24-Hri
tftft
Dry Gas Meter Reading
I-
J^
•zs?
A?
we
•76
'/./*
z, ;
99
f
H9-.fr
3
79
&0&_0,
«£/
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date 7-
Run No.
Project No.
Sample Type (6&jJth£siDi? Single-Point)
Flow Control Device (tf|ive^Critical Orifice)
Method 5 Meter Box No. /v-/^
M3B Pump Type
MSB Pump No,_
Client/Source t—•«"?<
Sampling Location fa?)
Operator un^ff-1^
Bag Type ^"&e//,.lv/
Method 38 Train No, _£
MSB Flow Meter Type _
MSB Flow Meter No. f.
2a ,
Sample No.
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time ffi
cc/min
After Sampling __
Flow Rate, cc/min: Average
Estimated Total Sample Volume .
. min Average Flow Meter Reading
Highest
Lowest
liters
Time
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
*>.*
1.*
/6ft
(70
r
M38SAMP.WPD June 18, 1998
ICal' APPENDIX C
35
-------
O5
40 CF/? 60. APPENDIX A. METHOD 3B, GAS ANALYSIS BY ORSAT
o
Run No,
Project No.
Sampling Location _
Analysis Start Time
Sample Type (Bag, Qzefrrf_
Analyst
Orsat Leak Check Before Analysis:
Burrete A-^tf Change in 4 Minutes
Pipettes Svf& Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete At> Change in 4 Minutes
Pipettes _/*£___ Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 /£
3
1 J?,3
2 /^y
3
1
2
3
Net
Value
/M^!
¥.7
3
Actual
Reading
1 j£&
2 /#.£
3
*i J?**9 *i?
i jf *v-^Pt
2 ^..J
3
1
2
3
Net
Value
//*-£
y4. 7
Average
Net
Value
(% v/v)
/^,&
^''7
Acceptance Criteria per Method 3B
C02 >4% 0,3% v/v Oz £15% 0,2% v/v CO
<4% 0,2% v/v <15% 0,3% v/v
0.3% v/v
Remarks and Notes:
7/n/??
M3BANAL.V/rO May 28, 1938
-------
40 CFR-6Q, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN tfi?. Received By ____{?>
Impinger Box A No..
Impinger Box B No, _
Data: 07-
Date/Time
TRAINCQMPQNENT
REAGENT
LOADiNG DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
1st Impinger (Mod-QBS) TOO mLs ASTM Type 1 Water
U-Connector (A)
2nd Impinger (GBSf 100 mLs ASTM Type i Water
U-Conneotor (^\
3rd Impinger (Mod-QBS) Empty
U-Connector (C)
4th Impinger (Mod-GBSI "200 g indicating silica gel
impinger Outlet Connector
Connector I.D. No.
Initial Weights (grams!**
* Before and after sampling; Nozzie inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impinger inlet sealed with glass blank-
off.
*** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17DSUP.WPD May 13, 1339 (rev, M17DSUP1.WPD July 2. 1SS9)
37
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTtCULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter! Outlet Duct
Run No.
Sampling Train A No. J&S7 -
Sampling Train B No.
Irnpinger Box A No.
Impinger Box B No.
Transfer for Recovery:
Relinquished By f?,
Received By.
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date;
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt,
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th
6-93.7
2nd
3rd
S3*?
ff.t
4th
% Blue
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt.
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt.
Sample Bottle Final Wt,
Net Water Sample Wt.
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow witl
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample battle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M17DRCV.WPD May 13. 1B99 (rev, M17DRCV1.WPD Julv 2, 1989)
38
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
EL
1
B
o
CO
Run No.
Project No.
Client.^Vy/*:
Source .
Sampling Location.
Oparator ywn .(^
Date -M2l±L
Record data every ~
Barometer No. V 2ftf f
Barometric Pressure
Elevation to Meter Boxes.
Meter Box Ph.. ±
minutes
, g.7
. in Hg
ft
Elevation to Sampling Loc.
Sampling Location (j
Static Pressure
in Hg
ft
in MQ
Train A No. rt'l /ftS?-*?
Probe No. 4- Lenoth: (* ft
Nozzle No. Mr?-1"** Tip Dm.Cf-l'it> In
Pitot Tuba No. A- Cp t^f
Stack Thermocouple No. jfi9^ "
Filter Holder No, (f
Filter Assembly No, ?c/
Impinaer Box No, A ~!
Urnhilinal/lmpinqer Hookup / 'jtf'*)'
Umbilical No, fJ ">&"' 3
Meter Box No, hJ I&
DQM Correction (Y) /,^fl
Orifice Mater AH@ /, ff°t
Train B No. ^- { iff?)"?--i&
Probe No. /9 Length: /O
Nozzle No. ^ 'ft'" Tip Dia. fl-^
Pitot Tube No, fi C - ?/
Stack Thermocouple No. 7^*?* ^ ~o
Filter Holder No. "7
Filter Assembly No. *? /
Imuifiuer Box No. /?•""/
Umbilical/lmpinger Hookup ^^"J^-
Umbilioal No. /^ ^*- /
Meter Box No. A>M'
DGM Correction (Y! 0.9?9~
Orifice Meter AH@ f* 96>
ft
in
paga 1 of
/ HL n
1 T
0 ,
fM
' 5
'
•••»-
^
jy
A ft <" p C"
Traverse Point Layout
Assumed Moisture
% Assumed %CO,
,%02.
llimela^hWI
Pass or Fail
Time (24 Hr!
Vacuum, in Hg
Leak Rats, cfrn
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
CfHG
Final
!o«rt
(3**»
r
Initial
ff¥ft
I*J
,004
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Initial
Final
Final
(^
\lr
,00s]
Initial
Final
Initial
Initial
Tralr
Final
Initial Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
-------
Run No.
Date _ *7j
Sampling Location
Project No. *-f*Jff
Operator .
page
( of
Sampling Data for Method 17 Train A No, Ar '
Traverse
Point
Sampling Clock
Time, Time
(24-Hr)
Dry Gas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Vslocity
Head
txi
S"?
'fff
fW"
Mt>Z.
•?•?
ti t&rt
VMt-
ng.ot,
s$fr
££-
ff
t.
/
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No.
Date 7-f?-W
Project No. ¥70*- -
Sample Type (jMulti-PointXSingle-Point)
Flow Control DeviceCJValvg/'Critical Orifice!
Method 5 Meter Box No. AJ^/O
MSB Pump Type T>f^
MSB Pump No. AJ-*
Client/Source £-°f\
5_2
Sampling Location
Operator &ri-t+^-
Bag Type
Sample No.
Method 3B Train No.
MSB Flow Meter Type
MSB Flow Meter No.
Desired Sampling Rate "3
Leak Check Before Sampling.
Total Sampling Time f5
cc/min
; After Sampling
. min Average Flow Meter Reading
Flow Rate, cc/rnin: Average
Estimated Total Sample Volume
Highest _
liters
foe
Lowest
Time
(24-Hr)
Flow
Meter
Reading
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
•3.*
3.0
.1.0
3.0
5. o
-3.0
Re-
M3BSAMP.WPD Jura 18. 199i
ICal APPENDIX C
41
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Pate
n
o
Project No.
Sampling Location _j
Analysis Start Time
Sample Type (Bag, fitair).
Analyst Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /tf? Change in 4 Minutes
Pipettes "V . Change in 4 Minutes
Analysis
Gas
CO2
-
02 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
1 ttfj*
2 W&
3
1 S9,7
2 Jft?
3
1
2
3
Net
Value
/¥•&
&J
2
Actual
Reading
1>W£
^/ f^rt
3
1 -M?
2 >^7
3
1
2
3
Net
Value
/¥>
J
3
Actual
Reading
1 /&;£
2 JjS^'
3
1 J$?
2 /$fy
3
1
2
3
Net
Value
Sv.&
-£M>
Average
Net
Value
(% v/vj
s&,c~
^~jj
C0
Acceptance Criteria per Method 3B
>4%0.3%v/v 02 2:15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BAHAL.WPD May 28, t
-------
40 CFfi 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MR] Project No. 4702.02.04,09
Client/Source; U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rooky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /iff Sampling Train A No, /2JJ/^erj impinger Box A No..
Sampling Train B No. /??/*y ~$3 Impinger Box B No.,
Set-up person(s): u.- £'Lts'.fr>&f~> Date:
Transfer to Sampler:
Relinquished By JA cSW.^ 5V? Received By &:&*'_*'?'/"' 1 Date/Time e7-S7~49
TRAIN COMPONENT __ REAGENT __ LOADING DATA
TRAIN A TRAIN 8
Sampling Nozzle (Quartz)* "' Nozzle 1 D. No.
Fitter Assembly and Holder* Fitter Assembly No. 3t> _ & /
Filter Type: Whatman 934-AH • .
Probe (31 6 SS) Filter Holder No. ^ _ ^
Sample Transfer/Vacuum Line • . . : .
Male 1st Impinger Inlet Blank-Off
Initial Weights (grams)**
1st impinger fMod-GBSl 100 mLs ASTM Type I Water ' '
U-Connector (Al
2nd Impinger {GBSI 100 mLs ASTM Type i Water
U-Connector (B)
3rd Impinger (Mod-GBSJ Empty
U-Connector (C) y/}
4th Impinger (Mod-GBS) "200 g indicating silica gel fir
Impinger Outlet Connector Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon* tape, and
entire filter assembly holder with filter assembly and nozzle placed in Zipioc® bag. 1st impinger inlet sealed with glass blanfc-
off.
* * Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
Ml7DSUP.WPD May 13, 1999 (rev. M17DSUP1.WPD July 2, t9SSl
43
ICal APPENDIX C
-------
40 CFR 50, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702.02,04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. /& Sampling Train A No. XfVv */? impinger Box A No,
Sampling Train B No. &S»T-r>'*> Received Bv t). &&Sjrr*&r* Date/Time,
Sample recovery person(s): •r»gx> Date;
Weights below are in grams.
BACK HALF RECOVERIES
TRAIN A TRAIN B
Impinger 1st 2nd 3rd 4th 1st 2nd 3rd 4th
Final Wt. -?&$-® &06r£ ¥929 -7??£ .
Net Wt. iP'j'}
Total Condensate Collected:
Description and/or color:
% Blue . ' . . • % Blue
FRONT HALF RECOVERIES
TRAIN A •'_ •_ TBAIN ,B
FILTER ASSEMBLY: , • '• \
Sample Number:
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt,
Components Rinsed*; nozzle, filter holder front
Sample Bottle Gross Wt. with Acetone Rinses
Net Acetone Sample Wt.
Sample Bottle Rnal Wt, Sf& /*"& with added Water Rinses
Net Water Sample Wt.
* Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow witl
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afta
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M17DBCV.WPD Moy 13, 1339 (rev, M17DRCV1.WPD July *. 19991
44
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No.
Project No,
Client
Source
Data
Sampling Location T/
Operator (a^rfrv^-
Record data every «-f minutes
Barometer No. ^^/gj
Barometric Pressure 70»0 _j_.
Elevation to Meter Boxes ^ H
Meter Box Ph., <^P/Otf
.in Hg
ft
in Hg
ft
Elevation to Sampling Loc. n
Sampling Location P,,,, ?" < &1 m Hg
Static Pressure -IS^S*/ jn n
Train A No, / '"^
Probe No. ft- Length: \fi ft
Nozzle No>^>""?"-£- Tip Dia. . /e:tRm 1 Aak C
Final | Initial
jiM_L^_
ffa^J I
Final
fmrkQ
Initial
Final
Initial
Final
Initial
Final
. 1
I
n
Time (24 Hr)
Vacuum, in Hy
Laak Rate, cfrn
Initial
UHv
I1?
, *p°\
Final Meter Volume
Initial Matar Voluma
Leak Check Volume
Final
ftfl^
w
-J
Initial
Final
Initial
Final
Initial
"•
Final
Initial
Final
Train B Sampling System Leak Checks
Initial
Time (24 Hr} | fltf\
Vacuum, (n Hg
Leak Rate, cfm
rf
Final Meter Volume
Initial Mater Volume
Non-sample Volume
Final
im<\
Initial
[^ }
,#
ft-
Final
Initial
_____Final [ Initial
Final
Initial
Final
Remarks and Notes; List any other equipment requiring calibration below.
M1?OCai,WPO July 2, 1899
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
-------
Run No.
Date
Sampling Location
Project No,
of 1
Operator.
Sampling Data for Method 17 Train A No. A "i-
Remarks and Notes;
M17DPQ2.WPD July 2, 1S39
46
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No,_£Z_
Project No. _
Sample Type fl^ulti-Pohry Single-Point!
Flow Control Devicec!^Sv§^)Critical Orifice)
Method 5 Meter Box No. AS-/&
MSB Pump Type
MSB Pump No,
Client/Source
t^
Sampling Location
Operator
Bag Type
&?
£**
Sample No.
Method SB Train No. .
MSB Flow Meter Type
MSB Flow Meter No.
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time
-------
CO
o
40 CFft 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No. // = __ Date
Project No. ¥"?#&&3,&*/.c9 SampleJ>k3T
Sampling Location _,
Analysis Start Time
Sample Type (Bag, Qtsbf,
Analyst il
Orsat Leak Check Before Analysis;
Burrate ./Kb Change in 4 Minutes
Pipettes A/& Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete />€> Change in 4 Minutes
Pipettes Svk Change in 4 Minutes
Analysis
Gas
C02
02 (Net is actual reading
minus actual C02 reading]
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 /*>.£
2 /$><&
3
1 /$*•£
2 j9,&
3
1
2
3
Net
Value
/&&
&£»
2
Actual
Reading
1 X^.
2 sy.ls
3
1 J9.L
2 Jf,&
3
1
2
3
Net
Value
/#,&
&i>
3
Actual
Reading
1 /^
2 /4<^
3
1 /9.t
2 j&&
3
1
2
3
Net
Value
J&fr
&>&
• Average
Nat
Value
{% v/v)
ML
&"•€>
Acceptance Criteria per Method 3B
CO2 >4%0.3%v/v 02 ^15% 0.2% v/v CO
<4% 0.2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.VUPD May 28. 1S93
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTiCULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No, 4702.02,04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogerrtrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
jf2 Impinger Box A No..
S Impinger Box B No. _
Run No, /? Sampling Train A No,
Sampling Train 8 No,
Set-up person(s): £>-'J Received By
Date:
Date/Time * T
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*"
Filter Assembly and Holder* • '
Filter Type: Whatman 934-AH
Probe(316SS>
Sample Transfer/Vacuum Line
Male 1 st impinger Inlet Blank-Off
Nozzle I.D. No,
Fitter AssemblyNo.
Filter Holder Mo.
SB
Initial Weights (grams)**
1st Impinger [Mod-QBS! 100 mis ASTM Type I Water
U-Connector (AS
2nd Impinger (GBS) 100 mis ASTM Type I Water'
U-Connector (B)
3rd Impinger [Mod-GBSl Empty
U-Connector (C)
4th Impinger [Mod-GBS| "200 g indicating silica gel
Impingor Outlet Connector
Connector I.D, No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc8 bag. 1 st impingar inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17DSUP.WPD May 13, 1999 (rsv.M17DSUP1.WPD July 2, 1998)
ICal APPENDIX C
49
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No, 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogenirix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No. S?_
Sampling Train A No..
Sampling Train B No.,
Transfer for Recovery.'
Relinquished By /?.
Received By J,
Impinger Box A No.
Impinger Box B No..
Date/Time
Sample recovery personls):
Weights below are in grams.
Date:
BACK HALF RECOVERIES,
TRAIN A
TRAIN B
1st
79S.1
Impinger:
Final Wt.
Initial Wt.
Net Wt,
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th
1st
2nd
3rd
4th
7,4
% Blue
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number: /7002
PM Description/color: ................... h)ysJ
TRAIN RINSES:
Sample Number: /7001
Sample Bottle Tare Wt.
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. _
Net Acetone Sample Wt. _
Sample Battle Final Wt.
Net Water Sample Wt.
with Acetone Rinsss
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow witl
ASTM Type ! water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M170RCV.WFD May 13. 1993 (rev. M17DRCV1 ,WPD July 2, 1988)
50
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR MiTHOD 17 TRAINS
o
en
Run No.
Project No.
Client _
Source
\~s
Sampling Location.
Date
J
T
Record data every
Barometer No. .
Barometric Pressure 3
Elevation to Meter Boxes
Meter Box Ph,r
minutes
in Hg
_ ft
Elevation to Sampling Loc.
Sampling LocationJJ,.,,
Static Pressure
in Hg
ft
Train A No. rf
Probe No. /&•
Nozzle No. ff/7'^
Pilot Tube No, fi
Stack Thermocouple
Filter Holder No,
Fitter Assembly No.
Impinaer Box No.
Umbilical/lmpinger H
Umbilical No. &
Mater Box No.
DGM Correction (Y)
Orifice Meter AH@
V &?/?-&
Length: ^K ft
Tip Dia. tfib in
C %¥
No. "^i^fi^A
3
*ty
ft-l
QOkup/.*/W
/fi^/
d-fo a
ro
f,%?
51 fT
-/ ,/V/V-S
Probe No. H Lenqth: '^ ft
Nozzle No,/tfl"7''l Tip Dia. « A?^ in
Pilot Tube No. /J Cp ,^f
Stack Thermocouple No. ;'T? 'Q
Filter Holder No, f
Filter Assembly No, "5S
Impinger Box No. P"~ '
Umbilical/lmpinaer Hookup Lltf "\t^
Umbilical No. fd liCf •- /
Meter Box No. flJ—lt
DGM Correction !Y> ff , ^S
Orifice Meter AH@ fr^
in Hg
in H,O Assumed Moisture
page 1 of,
Traverse Point Layout
% Assumed %CO5
%o,
p, —
Trai
1 Initial
jrimeJ24JHrHj^^
Pass or Fail j
n A Piti
Final
K14
at Tube Pressure Measurement System Leak Checks
Initial
/35XH I
Final
Initial
Final
Initial | Final
j
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/«r
Final
rri€
f&Q*>
Initial
Final
Initial
Final
Initiel
Final
Initial
Final
Train A Sampling System Leak Checks
Time (24 Hr>
Vacuum, in Hg
Leak Rate, cfm
Final Meter Vc
Initial
15"") 1
ft
\ »«
lume
Initial Meter Volume
Laak Check Volume
Final
r?1t
H ,
,ooO
Initial
Final
Initial
Final
Initial
,
Final
Initial
Final
Remarks and Notes: List any other equipment requiring calibration below.
M17DPG1.WPD July 2, IB33
TRAIN A
TRAIN B
M«ter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
(tie,
o
-------
Run No, /">?
Date l-h-ll
Sampling Location tSs <>*
Project No.
Operator _
page.
/ of
Sampling Data for Method 17 Train A No. $ ""/
1
Sampling
Time,
Dry Gas Meter Reading :
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No.
Project No., _ _
Sample Type ((Multi-Point^) Single-Point]
Flow Control Device i^glvg) Critical Orifice)
Method 5 Meter Box No..
MSB Pump Type ffi^**-
MSB Pump No. /A/x?
Client/Source
Sampling Location fe*
Operator £%rf-ff~~-
Bag Type
.•2*.
Sample No.
Method 3B Train No. _.A/ftr
MSB Flow Meter Type
MSB Flow Meter No.
Desired Sampling Rate _
Leak Check Before Sampling,
Total Sampling Time 96"
cc/min
Flow Rate, cc/min; Average .
Estimated Total Sample Volume
After Sampling
. min Average Flow Meter Reading
3OO Highest ,lOfr
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
rite
M3BSAMP.WPO June II, 139S
ICal APPENDIX C
53
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
E
I
o
Date
Run No..
Project No. V?esz,e>#.0Vtc9 Sample
Sampling Location £Va»'»^^&*£>*'_<*>*'•*.*•
Analysis Start Time
Sample Type jBag,J3*abf
Analyst _
Orsat Leak Check Before Analysis:
Burrete />^ Change in 4 Minutes
Pipettes Afo Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrele />y , Change in 4 Minutes
Pipettes /l/i? Change in 4 Minutes
Analysis
Gas
CO,
O2 {Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 /Vx5»"
2 Wig"
3
1 /?.£
2 /#£
3
1
2
3
Net
Value
/f'*
&'t
2
Actual
Reading
i M<*"
2 ^^
3
1 "^>
2 /£,£•
3
1
2
3
Net
Value
/#<£
(5^ /
3
Actual
Reading
1 /*fc$-
2 y'*^'*'
3
\J*6
2 y^^-
3
1
2
3
Net
Value
/#«£'*'
c5^ /
Average
Net
Value
(% v/v)
;»4^£""'
A.
S^J
Acceptance Criteria per Method 3B
COZ >4% 0.3% v/v
<4% 0.2% v/v
0, £15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
M3BAI4AL.WPD May 28, 1993
-------
40 CFR 60, APPENDIX A, METHOD 17 - PART1CULATE MATTER TRAIN [Ml 7!
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MR I Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter} Outlet Duct
Sampling Train A No.
Sampling Train B No.
Set-up person(s): v»
Transfer to Sampler:
Relinquished By t),
Impinger Box A No. Xy -
Impinger Box 8 No. j£~'•
Date:
Received By
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder* • :
Filter Type: Whatman 934-AH
Probe 1316 SS)
Sample Transfer A/a cuum Line
Male 1 st Impinger Inlet Blank-Off
Nozzle I.D. No.
Filter Assembly No.
Filter Holder No.
1st Impinger (Mod-CBS) 100 mLs ASTM Type I Water
U-Connector (A) -
2nd Impinger (GBS) 100 mLs ASTM Type \ Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger IMod-GBS) "200 g indicating silica gel
Initial Weights (grams)**
&M9
SftJ
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlet opening and filter assembly holder .outlet opening covered with Teflon* tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc® bag. 1 st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M170SUP.WPD May 13, 19BS (rev. M17DSUP1.WTO July 2, 1S98I
55
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (Ml 7)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR! Project No, 4702.02,04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
f_ Sampling Train A No,.
Sampling Train B No..
Transfer for Recovery:
Relinquished By J2> &SJ nr>V» Received By .
Impinger Box A No.
Impingar Box 8 No,
Date/Time
Sample recovery person(s):
Weights below are in grams,
A/I
Date;
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt.
Initial Wt.
Net Wt.
Total Condensate Collected:
Description and/or color:
2nd
&ST?
4th
1st
2nd
3rd
4th
/AS"
i D
% Blue
% Blue
FRONT HALF RECOVERIES -
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number: &QQ2
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt.
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt.
Sample Bottle Rnal Wt. Jfft
Net Water Sample Wt.
004
Jg 003
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivsbly clean. If any residue remains in a component, follow witf
ASTM Type I water rinses with brushing until perceivably clears. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M17DRCV.WPD May 13, 1833 (m. Ml 7DRCV1 ,WPD Juiy 2, 199SI
56
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
n
e.
D
Run No.
Project No.
Client jCfo.
Source
Date
Sampling Location
Operator
Record data every
Barometer No. ^
Barometric Pressure *?£
Elevation to Meter Boxes _
Metar Box PK,r %*'<
minutes
'b in Hg
•2-t ft
Elevation to Sampling Loc. *"<
Sampling Location Pbll 'faiOP
Static Pressure —L£->t%V-
.in Hg
_ ft
in Hg
jn H2o
Train A No. A'^ J&J7-S?
-Probe No. /f Lenath: /O
Imcinaer Box No, A*'1'
Umbilical/lmDinaer Hookup £/# 1-
Umbilical No. A/^J?'^
Meter Box No, /1>|C>
DQM Correction IYS /^CV/
Orifice Meter &H@ /, ^
Train B No. fr*1- MH7-&
Probe No. /i Length: K> ft
Nozzle Noytf f7'^5" Tip Dia. » W3 in
Pilot Tube No. & Cp *5V
Stack Thermocouple No. '%9?-ft
Filter Holder No. 3"
Filter Assembly No, / /
Imoinaar Box No, fi'-2-
Umbilical/lrnDinaer Hookup Lfff ~~ {
Umbilical No. A/ 5"
paga 1 of.
Travorse Point Layout
Assumed Moisture
Assumed %CO2.
Time (24 Hr)
Pass or Fail
Time «24 Hri
Vauuum, in Ha
Train
initial
cW
A Pilot Tuba Pressure Measurement System Leak Checks
-inal
\fr"
foaf*
Initial
#"?!$
ri
Leak Hate, cfm | t5lQ—
Final Meter Volume
Initiai Meter Volume
Leak Check Volume
Initial
Final
Final
filO
^
_(00't>
Initial
Final
Initial
Trais
Final
Initial
Final
Train B Pilot Tuba Pressure Measurement System Leak Checks
Initial
(JftJ
Final
__
t*s»*
Initial
Final
Initiai
Final
Initial
Final
Initial Final
i A Sampling System Leak Cnecks
Initial Final
Initial
Final
Initial
Final
Initiai
Final
en
Remarks and Notes: List any other equipment requiring calibration below.
M17DPGI.WPD July 2. 1899
Meier Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
TRAIN B
S-n
-------
Run No.
Date
Sampling Location
Project No.
page.
X of /
Operator
Sampling Data for Method 17 Train A No.
Dry Gas Meter Reading
(VJ, ft2
Orifice Pressure
Velocity Differential Stack
Head !AH), Temp.
(,
in. H,0 f Desired V Actual i °F
Dry Gas Meter
Temperature
ft
°F
Sampling Data for Method 17 Train B No.
Silica Gel
Imptnger
Outlet
Temp.,
43
r/
f
^L
ff.rt
•2.--J
2-0*)
ft
53
•gg-
16*1
ML.
5V
6.1S
93
J^.
iL
0,0ft-
fan.
Jd
J^_
left)
ifC?
f;
92-
fT
95"
•a.
2^.
^-S
jJfiZ.
C..S
T^T
_£A_
Remarks and Notes:
M17OPS2.WPD July 2, 19i»
* -135
58
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date.
Run No, i
Project No..
Sample Type.^jujthPomtj Single-Point)
Flow Control Deviee^fValve) Critical Orifice)
Method 5 Meter Box No. /»/-f
-------
o>
o
o
E.
fe
o
40 Cffl 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No. /" Date _
Project No. 4?fff,0SZ0*&9 SampleJikrrL
Sampling Location _
Analysis Start Time
Sample Type {Bag,.&!at5T
Analyst *)t__ -
Orsat Leak Check Before Analysis:
Burrete /vb Change in 4 Minutes
Pipettes..../?j? Change in 4 Minutes
Orsat Leak Check After Analysis;
Burrete /^P Change in 4 Minutes
Pipettes W& Change in 4 Minutes
Analysis
Qas
C02
Oz (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
\ JiM
2 SM
3
1 /#,$"
2 Sfy#
3
1
2
3
Net
Value
&.Z—
2
Actual
Reading
\/V4
2 Jtty
3
^ /^cf
2 /ftf
3
1
2
3
Net
Value
S¥&
cSVZ—
3
Actual
Reading
1 /#£
2 xX^
3
1 //^
2 /^./
3
1
2
3
Net
Value
/&.&
if, Z—
Average
Net
Value
(% v/v)
;&.&
^7^__
Criteria pejr
CO2 > 4% 0,3% v/v
<4% 0.2% v/v
^15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
M3BANALWPO May 28. 19B»
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702,02,04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
. _ Sampling Train A No.
Sampling Train B No.
Set-up person(s): *J' •$u^'j
Transfer to Sampler:
Relinquished By Jt. £>U/"s?i3ii*>
Impinger Box A No. S3' S?
Impinger Box B No. £3~^
Date:
TRAIN COMPONENT
Received By,
REAGENT
t &/'> rr~'
Date/Time
LOADINGDATA
TRAIN A
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probs [316 SS)
Sample Transfer/Vacuum Lins
Male 1st Impinger Inlet Blank-Off
-. ' 'Nozzle I,D. No,
". Filter Assembly No,
Filter Holder No.
TRAIN B
3-7
Initial Weights (grams)**
1st Impinger (Mod-GBS) 1 00 rnis ASTM Type I Water
U-Connector (A|
2nd Impinger (GBS) 1 00 mLs ASTM Type I Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger [Mod-GBS) "200 g indicating silica gel
Impinger Outlet Connector
Connector 1.0. No.
VH-t
* Before and after sampling; Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon® tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag, 1st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here,
Component Changes Aftar Set-up And Before Recovery And Other Comments:
M170SUP.WPD May 13, !999 |rev. M17DSUP1.WPD July 2, 1i93t
ICal APPENDIX C
61
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTiCULATE MATTER TRAIN (Ml7)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR! Project No. 4702,02,04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rooky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
JL Sampling Train A No. .
Sampling Train B No,.
Transfer for Recovery:
Relinquished By &,G'ft'r't~*jn Received By .
Smpinger Box A No..
Imptngar Box B No. .
Date/Time
Sample recovery person(s):
Weights below are in grams.
cJ .>
Date:
BACK HALF RECOVERIES
TRAIN A_
TRAIN B
Impinger: 1 st 2nd
Final Wt. *?J"33 &tff#
Initial Wt, &&0'JL & O/'O
3rd
4th
1st
2nd
3rd
4th
Total Condensate Collected:
Description and/or color:
•Sff.9
% Slue
% Blue
FRONT HALF RECOVERIES
TRAIN A
TRAIN B
FILTER ASSEMBLY:
Sample Number: /9o02
PM Description/color: j?)"3$fc
TRAIN RINSES:
Sample Number: /^001
Sample Bottle Tare Wt. rffi
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. ________
Net Acetone Sample Wt.
Sample Bottle Final Wt.
Net Water Sample Wt. ,
with Acetone Rinses
with added Water Rinses
* Acetone rinses with brushing 3 times or more until perceivably ciean. If any residue remains in a component, follow witl
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses,
COMMENTS:
MT7DRCV.WPD May 13, 1999 (lev. M170RCV1 .WPD July 2, IMS)
62
ICel APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
E.
fe
n
Os
CO
Run No,
Project No.
Client
Source
Sampling Location
Operator ^/rv
Date
Record data every ?
Barometer No, V got-/1
minutes
(
Barometric Pressure ^6
Elevation to Meter Boxes _
Meter Box P0.
Elevation to Sampling Loc,
Sampling Location P,
Static Pressure
inHg
ft
.in Hg
ft
.in Hg
Train A No. ft f /»/?-#
Probe No. /)- Lenqth: \O ft
Nozzle No. /*t/"7 "/'Z-'Tip Dia. '/%# in
Pilot Tube No. A q, /£¥
Stack Thermocouple No. "*>\6$'R
Filter Holder No. fc
Filter Assemblv No. "T$
Impinqer Box No, A-*"^
Umbilical/lmpinner Hookup I/ H^S Length: (° ft
Nozzle No. tttfl't^ Tip Dia. . fS'f in
Pilot Tuba No. D> CD $*
Stack Thermocouple No. _.*5.J33.'.v____
Filter Holder No. 7
Filter Assemblv No. "^«f
Impinqer Box No. ty* f
Umbiiical/lmDinqer 1 lookup i/K1rV
Umbilical No, A*'^'/
Meter Box No, /(/ -//
DGM Correction /,?f
page 1 of.
Traverse Point Layout
Asaurned Moisture
% Assumed %C03
Train A Pitot Tuba Pressure Measurement System Leak Checks
Initial
Tirna (24 Hr) j fm")
Pass or Fail
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Final
lH*ft
Initial
J^V>_
Initial
fM\
|£T
.00
Final Meter Volume
Initial Meter Volume
Leak Check Volume
Final
Final
ml1'
^
.0
Q
Initial
Final
__ ,
Initial
Trair
_
Final Initial Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/2^]_
~( A Sampling System Leak d
nal Initial
I
t
Final ; Initial
1^06 \
hecks
Final
Final
Initial
Initial
Final
Final
Initial 1
1
L
Final
Initial Final
Initial
Final
Train B Sampling System Leak Checks
Time 124 Hrl
Vacuunri, in Hg
Leak Rate, cfm
Initial
\TSft
IT
0(51-
Final Meter Volume
Initial Meter Volume
Non-sample Volume
Final
iHft
r>
,o
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Remarks and Nates: List any othar equipment requiring calibration below.
M17DPGI.WPO July 2, 1939
.TRAIN A
TRAIN B
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
-------
Bun No.
Date "2.
Sampling Location &s
Project No.
L£..
page.
of
Operator
Sampling Data for Method 17 Train A No,
M17DPG2.WPO July 2, 19B9
64
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No._
Project No.
Sample Type\(ft/[ult^PoiriiL/Single-Point}
Flow Control Devic^JVajye^Critical Orifice)
Method 5 Meter Box Ho,_Mll£.
MSB Pump Type PAffdre^r
MSB Pump No. A/-&
Client/Source
V
Sampling Location
Operator _Q_
Bag Type U
Sample No.
Method 3B Train No. A/4
MSB Row Meter Type
MSB Flow Meter No.
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time _
. cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
i^ After Sampling
min Average Flow Meter Reading
2£2 Highest.
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
5**
-5.0
ffat
J.G
ifft
M3BSAMP.WPD June 18, 1398
ICal APPENDIX C
65
-------
40 Cffl 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
n
e.
o
Run No.
Date
Project No.
Sampling Location _j
Analysis Start Time
Sample Type {Bag,J3«rto1.
Analyst
#9 Sample XXI?
Oa-}**' &#
Orsat Leak Check Before Analysis:
Burrete__A^|> Change in 4 Minutes
Pipettes /Vr? Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete __^t^ Change in 4 Minutes
Pipettes r^v Change in 4 Minutes
Analysis
Gas
C02
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 0^ reading)
1
Actual
Reading
1 ;&,
2 /*J,£
3
1 /«£/
2/<3> &
r /•&
3
1
2
3
Net
Value
/^t£f
&"£-
2
Actual
Reading
1 /tf.fr
2 /&,&
3
1 /ft/
2 /9J
3
1
2
3
Net
Value
•ty*i-
<5V2»
3
Actual
Reading
1 X^
2 Xi^^
3
1 /£/
2 /^/
3
1
2
3
Net
Value
^£4^
z-
Average
Net
Value
(% v/v)
X'*',^.
^'2-
Acceptance Criteria per Method 3B
COZ >4%0.3%v/v O2 ^15% 0,2% v/v CO
<4% 0,2% v/v <15% 0.3% v/v
0.3% v/v
Remarks and Notes:
M3BANAI_WS»D May 18. »999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN {M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02,04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rooky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Impinger Box A No. *>& ~J _
_ Impinger Box B No. ..... £-}
Bun No. £@ Sampling Train A No.
Sampling Train B No.
Set-up person(s): J •>«&»/.»».?''?
Transfer to Sampler:
Relinquished By €?,&fif^i^
-$__
Date: f 7 -
Received By .__ J,
Date/Time
TRAIN COMPONENT
REAGENT
LOADiNG DATA
TRAIN A
TRAINS
Sampling Nozzle (Quartz)*
Filter Assembly and Holder* '
Filter Type: Whatman 934'AH
Probe {31 6 SS) ,
Sample Transfer/Vacuum Una
Male 1st Irnpinger Inlet Blank-Off
Nozzle I.D. No,
Fitter Assembly No.
Filter Holder No.
1st Impinger !Mod-GBS) 100 mLs ASTM Type 1 Water
U-Connector (A) ..
2nd Impinger (GBS) 100 mLs ASTM Type I Water
U-Connector SB)
3rd Impinger !Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica ge!
Initial Weights (grams)**
* Before and after sampling: Nozzle inlet opening and filter assembly holder outlet opening covered with Teflon" tape, and
entire filler assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17DSUP.WPD May 13. 1898 (rev. Ml7DSUP1.«Vro July 2, 199SI
ICal APPENDIX C
67
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702,02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No..
Transfer for Recovery:
Relinquished By D. 6
Received By *J-
Impinger Box A No..
Impinger Box B No. ,
Date/Time
Sample recovery person(s):
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt.
Initial Wt.
Nat Wt.
Total Condensate Collected:
Description and/or color:
2nd
3rd
4th
1st
2nd
3rd
4th
9,9
% Blue
FRONT HALf RECOVERIES.
TRAIN A.
TRAIN B
FILTER ASSEMBLY:
Sample Number: && 002
PM Description/color:
TRAIN RINSES:
Sample Number:
Sample Bottle Tare Wt,
004
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. _______
Net Acetone Sample Wt.
Sample Bottle Final Wt. JV/9
Net Water Sample Wt.
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, follow wit
ASTM Type I water rinses with brushing until percaivabiy clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M17DRCV.WPD May 13. 19BS (rov. M17DRCV1.WPD July 2, 1SS9)
68
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
n
w
D
en
CO
Run No. 7-f pate 7^/^'1?^
Project No. ^rfffl' ~£>Z-
Client iix>OL*\4"Vr ( K
Source USAWti^v 1~^-
SamDlinq Location \p*£3' Owfrv
Operator SfiTt"**-
Record data every T
Barometer No. ^f2-°'i-(
Barometric Pressure >flr" '
Elevation to Mater Boxes ^S
Meter Box PUI I%rT.\
Elevation to Sampling LOG, 3.
Samolinn Location P^ 'JM/4'
Static Pressure &f S*ST> . %0, C"
page -1 of.
L-J U U LJ
Traversa Point Layout
! Time (24 Hr)
I Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
(WL-
Final
JSI^
Initial
p&\
Final
Initial
final
Initial
Final
Initial
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
..l.w-_
Final
tin
Djt^A
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Train A Sampling System Leak Checks
Time J24 Hr)
j Vacuum, in Hg
[j£2!L52i?iJ:l!!L
Initial
"ftp*
l<»
,00
I Final Meter Volume
j Initial Meter Volume
1 Leak Check Volume
1 1
Final
13 1\
"?
^^Ja^
Initial
Final
[
Initial
Final
Initial
j
s
j
Final
Initial
Final
Train B Sampling System Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Final Meter Vc
Initial
Final
fan |3ffj
t$
tii
lume
Initial Meter Volume
Non-sampla Volume
o
|S
^^°®L^
Initial
Final
r^ '-
j
Initial
Final
Initial
Final
Initial
Final
Remarks and Notes; List any other equipment requiring calibration below.
M17DPG1.WO July.a, 1999
TRAIN A
TRAIN B
Meter Volume at Start of Run
Meter Volume at End of Run
Total Leak Check Volume
Adjusted Final Volume
-------
1^-
Run No.
Data
Sampling Location
Project No.
Operator
1
page.
of
Sampling Data for Method 17 Train A No. A j
Traverse
Point
Sampling
Time,
O
Clock
Time
(24-Hr)
Dry Sas Meter Reading
(VJ, ft3
Initial
Desired
Actual
Velocity
Head
(Ap),
in. H20
Orifice Pressure
Differential
(AH5,
in. HO
Desired Actual
Stack
Temp.
Dry Gas Meter j
Temperature
Inlet Outlet
Pump
Vacuum,
in, Hg
Silica Gel
Impinger
Outlet
Temp.,
UL
2X>
7
¥
£Z.
Z.a
/sf
H,
ffrf
tof I 9?
_Z_
f
VI
9? <9Sf
£-
£2.
2,?
?S
52-
£ -? W
f±£-
¥79,/f
&
..
<& nry
^-^\.,-j~*--
•/Vs.*
sffl
aff
/&&
A?
, ?/
/
tf
9-
J^L.
A./?
-7
AL
5*
aft
ft/
•z,?
Seo
J^_
•z ,
IT/! .
•S..V
0,'??
ISO
f&f.
y
Sampling Data for Method 17 Train B No,
Remarks
M170PQ2.WPD July I, 1889
70
ICal APPENDIX C
-------
Run No. _g/ Date 7-f$-r7
Project No. tfIOZ -02-
Sample Type si^ytfcEoint) Single-Point)
Flow Control Device ^ajve) Critical Orifice)
Method 5 Meter Box No._/vS£ '
MSB Pump Type J
MSB Pump No,
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
:££l£2 Client/Source ^-gf-'
Sampling Location
Operator &t*$L-
Bag Type f2
"V
?x
Sample No.
Method 3B Train No. A/A
MSB Flow Meter Type
MSB Flow Meter No. /
Desired Sampling Rate 7^
Leak Check Before Sampling,
Total Sampling Time _
, cc/min
min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
After Sampling
Average Flow Meter Reading
Highest _
Lowest
. liters
Time
(24-Hr)
Flow
Mater
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
^£L
-*,,£>
.*
M3BSAMP.WPO June 18, !89S
ICal APPENDIX C
71
-------
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
I
w
o
Run No.
Project No.
Sampling Location _
Analysis Start Time
Sample Type (Bag,
Analyst Change in 4 Minutes
Pipettes *We Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete Ak Change in 4 Minutes
Pipettes A*b Change in 4 Minutes
Analysis
Gas
CO2
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual Oz reading)
1
Actual
Reading
1 /*;
2 ;&,/
3
1 /£*,.£"
2 JQ.S'
3
1
2
3
Net
Value
y^/
j-
2
Actual
Reading
1 ^*V
2 /K/
3
1 ypksr
2 ^a^"
3
1
2
3
Net
Value
MS
&.y
3
Actual
Reading
1 /*>,/
2,My
3
1 >£5-
2 y^^dT'
3
1
2
3
Net
Value
/*V
;57V-
Average
Net
Value
{% v/v)
;&/
^^
Acceptance Criteria per Method 3B
C02 >4% 0.3% v/v
0.2% v/v
02 2:15% 0.2% v/v
<15% 0.3% v/v
CO 0,3% v/v
Remarks and Notes:
M3IANM..WPD May 28. 1BS9
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric filter) Outlet Duct
Run No.
/ Sampling Train A No.
Sampling Train B No.
Set-up person(sj: _
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTiCULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MR] Project No. 4702.02.04.09
'.Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter! Outlet Duct
Run No. &f Sampling Train A No. sflP-/?''''' Impinger Box A No,.
Sampling Train B No. *$?/'?'£ Impinger Box B No..
Transfer for Recovery:
Relinquished By J7> £>Si"rf>r* Received By ** • £jts;r**&-r* Date/Time
Sample recovery person(s): ^?P^> Date;
Weights below are in grams.
BACK HALF RECOVERIES
TRAJMLA ; .TEAIN B
Impinger: 1st 2nd . 3rd 4th 1st 2nd 3rd . 4th
Final Wt. *?<¥&>£* &/V.9 &&J "?¥$:£ ' gifcL,
Initial Wt.
Net Wt. ./J?^_^L (t'M: ''® ^--a /•a''0 &? &•&.
Total Condensate Collected:
Description and/or color:
% Blue % Blue
FRONT HALF RECOVERIES
TRAIN A TRAIN B
FILTER ASSEMBLY;
Sample Number: &/ 002
PM Description/color: .A'te'jS^
TRAIN RINSES:
Sample Number: ft 001 glj 003
Sample Bottle Tart Wt. _
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt. „ with Acetone Rinses
Net Acetone Sample Wt,
Sample Bottle Final Wt. /Y7?. S**7 with added Water Rinses
Net Water Sample Wt. .
Acetone rinses with brushing 3 times or more until pereeivably clean. If any residue remains in a component, follow witl
ASTM Type I water rinses with brushing until pereeivably clean. Do not add any water rinses to the sample bottle until afte
the bottle is weighed with all of the acetone rinses.
COMMENTS:
M17DRCV.WPD Maf 13, 1999 (rev. M17DRCV1.WPD July 2. 1988t
74
ICal APPENDIX C
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
E.
fe
•fl
o
-•J
en
Run No,
Project No.
Client o
Source
Sampling Location
Operator
Date
Record data every _
Barometer No.
Barometric Pressure
Elevation to Meter Boxes
Meter Box Pt.
minutes
Elevation to Sampling Lac. j
Sampling Location Pt.,
Static Pressure
Train A No. ft '/ rf?/7~/9
Probe No. /£• Lenath: /<5? ft
Nozzle No .Ot ft- ft- Tip Dia. ,/?& in
Pilot Tube No. flt Cp , ?f
Stack Thermocouple No. "?/^?J /f
Filter Holder No. 1
Filter Assembly No. V2.
Impinqer Box No. A-—I
Umbitical/lmpinaer Hookup U rf *>0
Umbilical No. y~ 1 Wrf-^
Probe No. & Lenqth: f& ft
Nozzle No, Wf'?-^ Tip Oia. , / CB ./^
Stack Thermocouple No. "3/f3-P
Filter Holder No. ¥
Filter Assembly No. fo
Irnpinqef Box No. ft ^f
Umbilical/lrnpinafir Hookup 1/1 17 *>i -
Umbilical No. /Jfa-l
Meter Box No. A/ If
DQM Correction (Y> Gtfffi
Orifice Meter AH@ {tfC>
page 1 of.
Traverse Point Layout
Assumed Moisture /¥•-(?
Assumed %CO2 ffs:
Time (24 Hri
Pass or Fail
Train A Pitot Tube Pressure Measurement System Leak Checks
Initial
Final
jM*>
AM
f
Initial
Final
Initial
Final
—
Initial
Train
Final
A San-
Initial
ipting S
Final
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial i Final
^^T^Y
lassos
ystam Leak Checks
Initial 1 Final
!
r
Initial
Final
Initial
Final
Initial
Final
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial
08ft
<5
* ®&
Final Meter Volume
Initial Meter Volume
Lsak Check Volume
Final
fc^I
[£.
.&(}%
Initial
Final
Initial
Final
Initial
Final ! Initial
I
!
i
Final
Remarks and Notes; List any other equipment requiring calibration below.
M17DPB1 .WPD July 2, 1999
Meter Volume at Start of Run
Meter Volume at End of Run
Tola! Leak Check Volume
Adjusted Final Volume
o
-------
Bun No.
Date 7
Sampling Location $£**&**• 23 P^g
Project No. t/7&~>~ -.
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. $-1- Date
Project No, _
Sample Type(l|Wlulti-PoTnt^Single-Point)
Flow Control Device;-f^alye\ Critical Orifice) Bag Type
Method 5 Meter Box No.
MSB Pump Type 'Jtfy
M3B Pump No. A'-!
A/- ft
Client/Source
Sampling Location
Operator (£',$_"-.,
Method 3B Train No. _j
MSB Flow Meter Type
M3B Flow Meter No.
Desired Sampling Rate 2
Leak Check Before Sampling
Total Sampling Time
. cc/min
0
mn
Flow Rate, cc/min: Average,
Estimated Total Sample Volume
After Sampling
Average Flow Meter Reading
Highest _
liters
Sample No.
Lowest
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
t /u
foft
fec~ f / \ Q,—i—
M38SAMP.WPO June 18, 1998
ICal APPENDIX C
11
-------
oo
n
n
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No..
Project No.
Sampling Location _
Analysis Start Time
Sample Type (Bag,
Analyst
Date
Sample_H»r
Orsat Leak Check Before Analysis:
Burrete /y& Change in 4 Minutes
Pipettes A/o Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete Wo Change in 4 Minutes
Pipettes /*&_ Change in 4 Minutes
Analysis
Gas
C02
02 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1/+{^
2/j-J Jaf
/7-&
3
1 S9.8
2 /&*&
3
1
2
3
Net
Value
s^./
£~*O
2
Actual
Reading
1 S*fJ
2 M?
3
1 S9-?
2 /$,'?
3
1
2
3
Net
Value
/?• 7
&IO
3
Actual
Reading
1 /y-7
2 ^7
3
^J9.7
2 /$,7
3
1
2
3
Net
Value
/¥. 7
lS~.Ll
Average
Net
Value
(% v/v)
/4/.J?
£~,O
Acceptance Criteria per Method 3B
CO2 > 4% 0.3% v/v O2 £15% 0.2% v/v CO
<4% 0.2% v/v <15% 0,3% v/v
0.3% v/v
Remarks and Notes:
M3BANAL.WPO May 28, 1893
-------
40 CFft 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No, 4702.02.04.09
Client/Source,' U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location; Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter} Outlet Duct
Sampling Train A No,
Sampling Train B No.,
Impinger Box A No.
Impinger Box B No, _
Set-up person(s):
Transfar to Sampler;
Relinquished By J. 6 u /&*&>* Rsceivad By
Date:
Date/Time
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type; Whatman 934-AH
Probe {316 S3! ' •
Sample Transfer/Vacuum Line
Male 1st Impinger inlet Blank-Off
Mozzie J.D. No.
Fitter Assembly Mo.
'Filter Holder No.
1 st Impinger (Mod-CBS) 100 mis ASTM Type I Water
U-Conneotor (Al
2nd Impinger (GBS) 100 mLs ASTM Type I Water
U-Conneotor (B)
3rd Impinger (Mod-GBS) Empty
U-Connactor iC)
4th Impinger (Mod-GBS) "200 g indicating silica get
Impinger Outlet Connector
Connector I. D. No,
Initial Weights (grams)**
* Before and after sampling: Nozzie inlet opening and filter assembly holder outlet opening cowered with Teflon* tape, and
entire filter assembly holder with filter assembly and nozzle placed in Zipioc* bag, 1 st impinger inlet sealed with glass blank-
off.
*"* Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17DSUP.WPD May 13, IS
, M17DSUP1.WPO July 2, 1S39)
79
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702.02.04.03
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fibric Fitter) Outlet Duct
Run No. *<•*- Sampling Train A No, yw/xyy Impinger Box A No, /J-s
Sampling Train B No. ^?/7-& Impinger Box B No, £~)
Transfer for Recovery:
Relinquished By &• gy/r^ry Received By ___7^9_-9^_
Sample recovery person(s): v- £>t/s'srr•
-------
•rl
W
o
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
Run No,.
Project No.
Client Co.
Source
Date
>- 1&.
Sampling Locatio
Operator M
Record data every
Baromatar No.
minutes
Barometric Pressure £i
Elevation to Meter Boxes,
Meter Box P,,.
. in Hg
_ ft
rb«i
Elevation to Sampling Loc. ^y
Sampling Location Ebat 1r\.f n
JnHg
ft
.in Hg
Train A No. /^'^"" S&/7-&
Probe No, /f Length: A? ft
Nozzle No, fttf--(r Tip Dia. '/:?*/ in
Pitot Tubs No, AT C ,fjf
Stack Thermocouple No, "b ' 1* 'ft
Filter Holder No. ^3
Meter Box No. r (O1
DGM Correction IY) f'Otl
Orifice Meter AHP /» #?
Train B No. /3-vZ- 'j&S?-&
Probe No, ft Length: /£? ft
Nozzle No. itorf'Q Tip Dia. •/?£" in
Pitol Tube No. fk Cp -Sf"
Stack Thermocouple No. V n "n
Filter Holder No. <"
Filter Assembly No. 4"9
Impingsr Box No. /•? """^
Umbilioal/lmpinger Hookup f^-Jj '
Umbilical No. ** $& /
Mater Box No, /V //
DGM Correction (Yl
-------
Run No.
Date •
Sampling Location
Project Mo.
page.
/ of /
Operator,
Sampling Data for Method 17 Train A Wo. A -2-
Traverse
Point
Sampling
Time,
Clock
Time
(24-Hr)
rtf*
Dry Gas Meter Reading
?
91
ff
552-
9-7
¥
D- 5 2V-
ftt.
^ rv
f
/5V
¥
ai-
-7
*•
59
^2fc-
X
cT
5"
5T
t&l.
A--
<£ f
~sf'r*>.t*?
Z.o
AS-
72-
-r
V
K- S
TT
0./Z- O.SZ-
fcf
f
Sampling Data for Method 17 Train B No.
M17BPS2.WPO Jtiy 2, 1999
82
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Date
Run No. j.
Project No.
Sample Type ^Mufti^Pjoj5&, Single-Point]
Flow Control Device^f^ajve) Critical Orifice)
Method 5 Meter Box No. /V ~fsj
M3B Pump Type P/yi/'?>*----~
MSB Pump No. A/iiO
Client/Source
Sampling Location
_ ' s"
Operator £*?
Bag Type ^fe
2ff
Sample No.
Desired Sampling Rate
Leak Check Before Sampling.
Total Sampling Time.
_.<£?
mn
Flow Rate, cc/min: Average ;
Estimated Total Sample Volume
Method 3B Train No. _
MSB Flow Meter Type
MSB Flow Meter No. _
. cc/min
After Sampling
Average Flow Meter Reading
Highest _j3fL2
Lowest
liters
Time
(24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
f/fr
^r
1
M3BSAMP.WPD June 18,1898
ICal APPENDIX C
83
-------
co
-C-
40 Cf/? 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
n
R
o
Run No.
Project No,
Date
Sample-Mcr:
Sampling Location VmS %/? S
Analysis Start Time
Sample Type (Bag,
Analyst £/
Orsat Leak Check Before Analysis:
Burrete /vfo Change in 4 Minutes
Pipettes <^b Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete tff Change in 4 Minutes
Pipettes Jr&. Change in 4 Minutes
Analysis
Gas
C02
02 (Net is actual reading
minus actual C02 reading)
CO (Net is actual reading
minus actual 02 reading)
1
Actual
Reading
1 j*r
2 /ts.f
3
1 /9£
2 tf.f
3
1
2
3
Net
Value
/*}f
3
1 J4.f
2 /9f^
3
1
2
3
Net
Value
>*K
AcceotancB Criteria per Method 3B
CO2 >4% 0.3% v/v
<4% 0,2% v/v
02 2:15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes:
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN (Ml?)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRi Project No. 4702,02.04,09
Client/Source: U.S. EPA OAQPS EWAD EMC / Cogentrix Unit ZA
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter] Outlet Duct
Run No.
Sampling Train A No.
Sampling Train 8 No.
Set-up persons):
Transfer to Sampler:
Relinquished' By y*
Impinger Box A No..
Impinger Box B No. _
Date:
Received By
Darte/Tima
TRAIN COMPONENT
REAGENT
LOADING DATA
TRAIN A
TRAIN B
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 934-AH
Probe (316 SS)
Sample Transfer/Vacuum Line
Male 1st Impinger Inlet Blank-Off
. .Nozzle I.D. No,
.: Filter Assembly No.
Fitter Holder No,
Initial Weights [grams)**
1st impinger IMod-GBS) 100 mLs ASTM Type I Water
U-Connectar (A) • :
2nd impinger (GBS) 100 mLs ASTM Type J Water
U-Conneetor (B)
3rd Impinger |Mod-GBSS Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling: Nozzle inlst opening and filter assembly holder outlet opening covered with Teflon81 tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc* bag. 1 st impinger inlet sealed with glass blank-
off.
** initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M11DSUPAVPO May IS, t99» (rev. M17DSUP1.WPO July 2, 199S!
JCal APPENDIX C
85
-------
40 CFR 60, APPENDIX A, METHOD 17 - PART1CULATE MATTER TRAIN (M17)
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MFU Project No. 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC ( Cogentrix Unit 2A
Source Location; Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
f Sampling Train A No.,
Sampling Train B No..
Transfer for Recovery:
Relinquished By &_'_ &/"tfrf~e* Received By .
Sample recovery personfs}: *//
Waights below are in grams.
Irnpinger Box A No.
Impinger Box B No.
Date/Time
Date;
BACK HALF RECOVERIES
.TRAIN. A
TRAIN B
Impinger: 1st
2nd
3rd
4th
2nd
3rd
4th
Initial Wt. &£&,J ^£"?,& ^^
NetWt. X5V, ^ &t3 /
Total Condensate Collected:
Description and/or color:
cJt-**' cje-sS cj!*.
TRAIN A
FILTER ASSEMBLY:
1,j
.S' .,:!•
::>::::-:;:-;;:;.S ;-.;:,:::-
2*f^':':''-'':''':-':
SiSC ,~:
iitisjpRO
&S*:;:..
";:'*y
^^^^5J*x
sfl^M
'&yj»^
::-s, S«;
:>i5??S^'
IsSolSfe
:«•"",,,%
•i!:yi^?>£:ii':i;
•:'-';.:::.:::':S;.::.-,:^
fei;,. Y '^
^•XW&:s,.Jt
< «f;:«*-""r^i*
i; ;N;ss:';'sj;;^4
Bf ;:.•«»!«:!•«?:•«.:-.-
ssjfe. -:">g;fiK
5il'""5;If ;' ,,,
'•<7SV,. ;.,:.»?;.-:":;?:;;-?:.
S;K;r:j:::-;S:;:;s::K5a:;
?iX^*
:,»3,ft;
;«s*
f&j?
. m?
::?::,:::
ES®
? 649.7 4&7.&- 7/3>*it
f-
-------
FIELD SAMPLING DATA FOR METHOD 17 TRAINS
O
E.
I
O
Run No. 2
Project No,
Client Ccc
Source
Sampling Location
Operator
Date
Record data every *r
Barometer No. y ^-/ 0 /
Barometric Pressure
Elevation to Mater Boxes
Meter Box Ph,r
minutes
.in Hg
ft
Elevation to Sampling Loc.
Sampling Location Pbw ^
Static Pressure
•H
.in Hg
ft
X_inHg
-I'S.S.S' inHjO
Train A No. 4 "f S^S?^
Probe No. fa Lenath: (° ft
Nozzle No. Mn'fa Tip Dia. ./$& in
Pilot Tube No. fir C0 f&H
Stack Thermocouple No. "^hf'A
Filter Holder No. 6>
Filter Assembiv No. *f&
Impinger Box No, $ ~!
Umbilical/lmpinflar Hookup 4<^*?0
Umbilical No. fJ'iO'*)
Meter Box No, A/ IO
DGM Correction IY> /.£ / 1
Orifice Meter &Hi> ^f4?
Train B No, 0-1 SW~g
Probe No. -t> Lenath: f° ft
Nozzle No. Wr7'l*> Tip Dia. ,/Bf in
Pilot Tube No. P Cp 'cP^
Stack Thermocouple No. "Jf^t 'f^
Filter Holder No. 7
Filter Assembly No. ^/7
impinger Box No. /•> "/
UmbilicaMmpinqer Hookup l{ ft ^l^
Umbilical No. V^'i
Meter Box No. f\j M
DGM Correction !Y> (7,95:?
Orifice Meter AH@ /'^
page 1 of.
VJ
Traversa Point Layout
Assumed Moisture
% Assumed %CO,
Time (24 Hr)
Pass or Fail
Train A Pitot tube Pressure Measurement System Leak Checks
Initial
^———j
Final
i-JO*>
Initial
Final
Initial
Final
Initial
Train
Final
A Sarr
Initial
ipling £
Final
ystam
Train B Pitot Tube Pressure Measurement System Leak Checks
Initial
/"fH?
Leak C
Final
11^
necks
Initial
Final
Initial
Final
Initial
Final
Initial
Final
Time (24 Hrt
Vacuum, in Hg
Initial
M(0
ff)
Leak Rate, cfm , O'O
Final Meter Volume
Initial Meter Volume
Leak Cheuk Vulume
4
Final
not
['L
.<*%>
Initial
Final
Initial
Final
Initial
Final
]
1
!
)
|
Initial
Final
CO
Train B Samplinrj System Leak Checks
Time (24 Hr)
Vacuum, in Hg
Leak Rate, cfm
Initial Final Initial Final Initial . F na! Initial Final Initial Final
W/'f I'fo'h
1^! l(i
e,et{ ,00^
Final Mater Voluma
Initial Meter Volume | j j
Non-sample Volume j ]
Remarks and Notes: List anv olher equipment requiring calibration below. TRAIN A TRAIN B
Meter Volume at Start of Run ($ )
-------
Run No.
Date "7
Sampling Location xitfe'-a
Project No. j^^-. 0A_
page.
1 of
Operator _
Sampling Data for Method 17 Train A No.
Ramarks
M170PQ2.WPD Jyly2, 199S
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 3B
INTEGRATED GAS SAMPLING DATA
Run No. g-V
Date
Project No.
Sample Type
inJ, Single-Point)
Client/Source
Sampling Location
Operator (£>>.tr~-:
Flow Control Device (Valve) Critical Orifice! Bag Ty p e
^•se^S-"—""'^
Sample No.
Method 5 Meter Box No.
MSB Pump Type *?>'
MSB Pump No._^t/;'/C
Method 3B Train No. J±
MSB Flow Meter Type _,
MSB Flow Meter No.
Desired Sampling Rate '3?a'-
Leak Check Before Sampling.
Total Sampling Time _ ^7_
cc/min
Flow Rate, cc/min: Average
Estimated Total Sample Volume
z After Sampling
, min Average Flow Meter Reading
l*?g Highest
Lowest
"2-t?
liters
Time
! 24-Hr)
Flow
Meter
Reading
Start
Purge
Start
Sampling
Stop
Sampling
Sampling
Remarks and Notes
V
V?
/t,'/f
fcffT [/'•f"-~
3 c/
M3BSAMP.WPD Jyn> IS, 1938
ICal APPENDIX C
89
-------
8
o
E.
o
40 CFR 60, APPENDIX A, METHOD 3B, GAS ANALYSIS BY ORSAT
Run No.
Project No.
Sampling Location _
Analysis Start Time
Sample Type {Bag, fitato)
Analyst c/. £
Data
Sample Mar
Orsat Leak Check Before Analysis;
Burrete xV^ Change in 4 Minutes
Pipettes /fa Change in 4 Minutes
Orsat Leak Check After Analysis:
Burrete /Vfr Change in 4 Minutes
Pipettes A^o Change in 4 Minutes
Analysis
Gas
CO2
O2 (Net is actual reading
minus actual CO2 reading)
CO (Net is actual reading
minus actual O2 reading)
1
Actual
Reading
1 /<£?
2 /^
3
1 /9J
2 tf.f
3
1
2
3
Net
Value
//,4% 0.3% v/v
<4% 0.2% v/v
02 ^15% 0.2% v/v
<15% 0.3% v/v
CO 0.3% v/v
Remarks and Notes;
M38Af4AL.WPD May 28. 1999
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTiCULATE MATTER TRAIN (Ml7)
FIELD LABORATORY TRAIN SET-UP DATA FOR TWO TRAINS
MRI Project No. 4702.02.04,09
Client/Source: U.S. EPA QAQPS EMAD EMC / Cogentrix Unit 2A
Source Location; Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train B No.
Set-up person(s):
Transfer to Sampler:
Relinquished By ______ jrirrir?
REAGENT
Date/Time
LOADING DATA
TRAIN A
Sampling Nozzle (Quartz)*
Filter Assembly and Holder*
Filter Type: Whatman 334-AH
Probe (316 SS}
Sample Transfer/Vacuum Line
Male 1 st Impinger Inlet Blank-Off
. , Nozzle i,D. No.
Filter Assembly No
filter Holder Mo,
Initial Weights (grams!**
1st Impinger (Mod-GBS) 100 mLs ASTM Type I Water
U-Connector (A)
2nd Impinger (GBS) 100 mLs ASTM Type ! Water
U-Connector (B)
3rd Impinger (Mod-GBS) Empty
U-Connector (C)
4th Impinger (Mod-GBS) "200 g indicating silica gel
Impinger Outlet Connector
Connector I.D. No.
* Before and after sampling; Nozzle iniet opening and filter assembly holder outlet opening covered with Tefion8 tape, and
entire filter assembly holder with filter assembly and nozzle placed in Ziploc® bag. 1 st impinger inlet sealed with glass blank-
off.
** Initial weights of additional components exchanged during the run also entered here.
Component Changes After Set-up And Before Recovery And Other Comments:
M17OSUP.WTO May 13. 1899 (rav. M17DSUP1.WPD July 2. 19991
91
ICal APPENDIX C
-------
40 CFR 60, APPENDIX A, METHOD 17 - PART1CULATE MATTER TRAIN (M17!
FIELD LABORATORY SAMPLE RECOVERY DATA FOR TWO TRAINS
MRI Project No. 4702-02.04,09
Client/Sourcs: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Run No.
Sampling Train A No.
Sampling Train 6 No.
Transfer for Recovery;
Relinquished By f?*
Received By ••)•
Impinger Box A No,
Impinger Box B No.
Date/Time
Sample recovery person(s);
Weights below are in grams.
Date:
BACK HALF RECOVERIES
TRAIN A
TRAIN B
Impinger: 1st
Final Wt.
Initial Wt.
Net Wt. /£>'?,!«?"
% Blue
% Blue
FRQNTH ALF 3ECOV ERl ES
...T_RAIM_A_
TRAIN B
FILTER ASSEMBLY:
Sample Number:
PM Description/color:
TRAIN RINSES;
Semple Number:
Sample Bottle Tare Wt.
Components Rinsed*: nozzle, filter holder front
Sample Bottle Gross Wt.
Net Acetone Sample Wt.
Sample Bottis Final Wt.
Net Water Sample Wt.
SSV004
with Acetone Rinses
with added Water Rinses
Acetone rinses with brushing 3 times or more until perceivably clean. If any residue remains in a component, fallow witf
ASTM Type I water rinses with brushing until perceivably clean. Do not add any water rinses to the sample bottle until aftei
the bottle is weighed with all of the acetone rinses,
COMMENTS:
M17DftCV.WPD M«y13, 1999 [rev. M17ORCV1 .WPD July 2. 1S99)
92
ICal APPENDIX C
-------
ICai Appendix D
M17 Field Laboratory Particuiate Weight Data
MRt-OPPTWTO-02-fl? Appendices Covers.WPD
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR I Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst: -^£, •- _
Filter Size and Type; 47mm diameter, Whatman 934-AH glass fib^r inter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 "C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. ..,$&_ ..... , ..... Assembly No. J& _ Sample No.
Gross Wt. Date Time Comments:
&,$¥?£> 67-JV-99
Assembly Gross Weight used foi data entry:
Assembly Tare Weight from Tare Weight Data:
Run No, && ...... Assembly No. ../*? _ ; Sample No.
Gross Wt. Date . -Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. /&J9 Assembly No. Vj* _ Sample No. /£>&£> '2-
Grass Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Wsight Data:
NOTE: Control and, blank assembly weight data and balance check data are documented on other forms,
MBIPMFIX.WPD June S. 1S98 irev. MI7PMFI1.WPD July 2, 1999)
ICal APPENDIX D
-------
PART1CULATE MATTEF! IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No, 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse [Fabric Filter) Outlet Duct
Sampling Team Leader; Jim Surman Analyst:
Filter Size and Type; 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. /& & Assembly No. . ^. JV Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weiyht Data:
Run No. /// Assembly No.. £> Sample No.
Gross Wt. Date • Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. Assembly No. _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry: _ 3 •>
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other farms.
MSIPMFiX.WPD June S, 1998 lr«v. M17PMFI1.WPD July 2. 1S99!
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC I Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader; Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiBer filter
Filter Lot No. 29439A
Assembly Components; filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment; Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. /£/$ Assembly No. «ff^.._ Sample No. _ /#£>'£> *2-~^_
Gross Wt. Date Time Comments:
3,39 f*J
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data;
Run No, /£?& Assembly No. £~3 ..... ' Sample No. J1ZO&
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry;
Assembly Tare Weight from Tare Weight Data:
Run No. /« Assembly No. Sample No.
Gross Wt, Date Time Comments:
S, 3
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tars Weight Data:
NOTE; Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMF1X.WPD June S, 1388 Irev. M17PMFI1.WPD July 2. 1999]
JCal APPENDIX D
-------
' PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber fifier
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. /SB Assembly No. Z?&" Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry ">£*.
Assembly Tare Weight from Tare Weight Data:
Run No. *< Assembly No. *? Sample No.
Gross Wt. Date Time • Comments:
Assembly Gross Weight used for data entry;
Assembly Tare Weight from Tare Weight Data:
Run No. J* Assembly No. Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry.
Assembly Tare Weight from Tare Weight Data: 3t3s 7 /
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMRX.WPD June 6, 1898 irev. M17PMFi1,WPD July 2, 1998!
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 4702,02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric filter} Outlet Duct
Sampling Taam Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber fflter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. f&
-------
PARTiCULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR I Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghouse (Fabric Filter} Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type; 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No, 29439A
Assembly Components; filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. > Assembly No. __£/. _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tore Weight Data:
Run No. Assembly No, • Sample
Gross Wt. Date , Time ! Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No. /7S Assembly No. £3 Sample No.
Gross Wt. Date Time Comments;
Assembly Gross Weight used for data entry: _*f •'**&< $/
Assembly Tare Weight from Tare Weight Data;
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M51PMF1X.WPO JuneS, 1998 lrev.M17PMFI1.WPD July 2, 19391
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter} Outlet Duct
Sampling Team Leader: Jirn Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 31 B stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Bun No. ' Assembly No. . Sample No.
Gross Wt. Date Time Comments:
Assembiy Gross Weight used for data entry: *-*-
Assembly Tare Weight from Tare Weight Data: __3_*
Run No. "_ Assembly NQ-. S' " Sample No.
Gross Wt, Data .Time Comments:
Assembly Gross Weight used for data entry: ^*U4*dr "2—
Assembly Tare Weight from Tare Weight Data:
Run No. » Assembiy No, ,_ Sample No.
Gross Wt. . Date Time Comments:
07 -/ 9-49
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFIX.WPD June S, 1S98 (rev. M17PMF11.WPD July 2. 1933)
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR! Project No. 4702,02,04.03
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Rlter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No, /^^ Assembly No. 37 Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data: „
Run No. 0 • Assembly No. e Sample No,
Gross Wt. Date " Time • Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data: 3 '*
Run No. *?&&_ Assembly No. 3 9 Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M51PMFIX.WPD June 6, 1998 Irew. M17PMFit.WPO July 2, 19991
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MR! Project No, 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location; Rocky Mount, North Carolina
Sampling Location: Baghouse jFabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiberrilter
Riter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
No. Assembly No. Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
Run No, &S& Assembly No. &/ Sample Mo,
Gross Wt. Date . Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data: ..... J
No. Assembly No. * Sample No.
Qross Wt. Date Time Comments;
. &J&3 6730 -99
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data: &*
NOTE: Control and blank assembly weight data and balance check data are documented on other forms.
M5IPMFBC.WPD June 5, 1998 (re*. M17PMB1.WPO July 2. 19S9)
ICal APPENDIX D
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 4702.02.04,09
ClientrSource: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot Ho. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight,
Weight Unit: grams
Run No. * Assembly No, Sample No.
Gross Wt. Date Time Comments:
3,2933
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
-------
PARTICULATE MATTER IN FILTER ASSEMBLY ANALYSIS DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location; Baghause (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
_
_
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment; Heat at 105 °C for 3 hours, desiccate and weigh to a constant weight.
Weight Unit: grams
Run No. Assembly No. Sample No.
Gross Wt, Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
No. il Assembly No. ' " Sample No.
Gross Wt. Date ' Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data;
Run No. _ Assembly No, _ Sample No.
Gross Wt. Date Time Comments:
Assembly Gross Weight used for data entry:
Assembly Tare Weight from Tare Weight Data:
NOTE; Control and blank assembly weight data and balance check data are documented on other forms,
M5IPMF1X.WPO JuneS, 1998 (rev. M17FMFI1.WFD July 2. 1989)
ICal APPENDIX D
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MRI Project No. 4702.02.04.09
Sampling Team Leader: Jirn Surmart Analyst: //,
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Rlter Lot No. 29439A
Assembly Components: fitter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Time Started; £>g£>O
Balance Check before filter assembles are weighed:
Balance Used: A*!0 £A-Jff0A
Weight Value; /«^
Bafance Reads: /, Pt>0_O
_Assemblv No.
y
-7
8
Je
/*?
First Weighing
Second Weighing
Third Weighing
Average Weight
or Weight to be
Used as the Tare
&3&V7
2,34 fa
3,3 tfo
Balance Check after filter assemblies are weighed:
Balance Reads: ,
COMMENTS:
12
MSIFILTX.WPD June 4, 1S98 irav. M17FILT1.WPO July 2, 1993)
ICal APPENDIX D
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MR! Project No, 4702,02.04.09
Sampling Team Leader: Jim Surman
Analyst:
Filter Size and Type; 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: £"^?'^ 1'\ ~??
Tims Started: -'./•$??
Balance Check before filter assembles ara weighed:
Balance Used: Mettler AE20C, MRI #10586
Weight Value: 2 + 1 grams 2 + 1 grams
Balance Reads: ~3>_O
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MRI Project No. 4702.02,04.09
Sampling Team Leader: Jim Surman
Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless steel filter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: &<%-&
Time Started:
Balance Check before filter assembles are weighed:
Balance Used: Mettler AE20G, MRI #10586
Weight Value: 2 + 1 grams 2 + 1 grams
Balance Reads: ;
Assembly No.
2 + 1 grams
First Weiejhma
Second Weiahina
hird Weiahinq
1
Balance Check after fills? assemblies ara weighed:
Balance Reads: __^j£LLJ_jL2.JL /'
COMMENTS:
Average Weight
or Weight to be
Used as the Tare
^IFII^.WM j,,,,4, .S9S,IS...W7F
ICal APPENDIX D
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MRI Project No. 4702.02,04.09
Sampling Team Leader: Jim Surrnan Anaiyst:
Filter Size and Type; 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No, 29439A
Assembly Components: filter, aluminum foil gasket, and 31 6 stainless steel fiiter support
Filter Assembly Treatment: Heat at 105 °C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: _
Time Started: _ _ _
Balance Check before fiiter assembles are weighed:
Balance Used: Mettler AE20C, MRI #10586
Weight Value: 2 + 1 grams 2 + 1 grams 2 + 1 grams
Balance Reads: 1,(?0& [ : ._._ :iii:i: f.^7 ^
Average Weight
or Weight to be
Asse-mblv No. First Weighing Second Weighing Third Weighing Used as the Tare
tfl
-XL
m
J £7 U-f
o
5 27/7
Balance Check after filter assemblies are weighed:
•y G) Cj Q •••*> ."1
Balance Reads; _' < l ' ' 2
COMMENTS:
MSIHrrX.WPD .Mm i ',B9B Irflv. Ml 7FILT1 .WPD June 30, 139H: 1 r
ICal APPENDIX D
-------
FILTER ASSEMBLY TARE WEIGHT DATA
MR! Project No. 4702.02.04.09
Sampling Team Leader: Jim Surman ' Analyst:
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Fitter Lot Nc. 29439A
Assembly Components: filter, aluminum foil gasket, and 316 stainless stsei filter support
Filter Assembly Treatment: Heat at 105 "C for 3 hours, desiccate, and weigh to a constant weight.
Weight Unit: grams
Date: b~%f •'ffi 1 ~f
Time Started: ^<7t?
Balance Check before filter assembles sre weighed:
Balance Used: Mettler AE200, MR! #10586
Weight Va'ue: 2 + 1 grams 2 -I- 1 grams • 2 + 1 grams
Balance Reads: ___j3i^£J Sfy-ooO \
Average Weight
or Weight to be
Assembly No... First Weiohina Second Weighing Third Weighing Used as the Tare
_1
Balance Check after filter assemblies are weighed:
Balance Reads: Z - 5ll"i \$&\
-?. 7
COMMENTS:
M-ilrlLTX WPf; June 4. 1SS8 ifsv. M17WLT1 WPD June 3CL 1SSS)
16
ICal APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghcuse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-rnL Teflon*
Acetone Lot No, &O3&3 Water Lot No.
Sample Treatment: Acetone' and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-fi!tered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No, srf Beaker No. /£> Sample No..
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
A. - - Sample + Rinses Wt,
B. - Water Wt. from Recovery Data: O
C. Acetone Wt. (A - B):
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight.from Tare Weight Data:
Combined Blank = {(Water Blank x B) + (Acetone Blank x D))/{B + D) = O mg/mL
Volume (B + D) for data entry = ^gj?1 mLs
Comments:
Run No. Ve? Beaker No. s/ Sample No.
Sample Volume + Acetone Rinses of .Bottle Beaker Liner + Sample Residue Weights
Start . . . end ., , Gross Wt Date Time
Beaker + Liner + Sample + Rinses Wt. /jg£»:Z . '• ^b^^__ £7-^-91^
Beaker + Liner Tare Wt. /C&r&
A. Sample + Rinses Wt.
B. Water Wt. from Recovery Data:,
C. Acetone Wt. (A - ,B1: .
D. Acetone W1./0.79 = mLs Acetone: ,
Beaker Liner + Residue GroWWeigrYt"Hied for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank - ((Water Blank x B) + (Acetone Blank x D))/(B + D] = ,.^ O mg/rnL
Volume (B + D} for data entry = *$3,"7 rnLs
Comments:
Run No. /0S7 Beaker No, ..,, .ZiT Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner4-Sarnple-f Rinses Wt,
Beaker + Liner Tare Wt. Sf&,Q
A, - - Sample + Rinses Wt,
B, .,..., Water Wt, from Recovery Data;
C. Acetone Wt. (A - Bl:
D. Acetone Wt.10.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = {(Water Blank x B) + (Acetone Blank x D))/(B + D) = ,. tf> mg/mL
Volume (B + D] for data entry = . .S?JTV mLs
Comments;
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
MSIf»MRiX,WP0 JunsS, 1998 (rev. M17PMRI1.WPD July 2, 1989) -|-J
ICal APPENDIX D
-------
PART1CULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No, 4702.02.04,09
Client/Source: U.S. EPA OAQPS EW1AD EMC I Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. _....JS&_'3&3_ Water Lot No,
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight,
Weight Unit: grams
Run No.
/& & Beaker No. s9 Sample No..
Sample Volume + Acetone Rinses of Bottle Beaker Liner •*• S ample Jjes,icju.eWejghtg
start end Gross Wt, Date Time
Beaker + Liner + Sample + Rinses Wt,
Beaker + Liner Tare Wt. __/<&&^J_
A. Sample .+ Rinses Wt.
B, Water Wt. from Recovery Data:
C. Acetone Wt. (A - B):
D. - - - - Acetone Wt.yO.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry."
Beaker Liner Tare Weight.from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D)}/(3 •* D] = <3> mg/mL
Volume (B 4- D) for data entry = &7.L mLs
Comments:
Run No. //& Beaker No. Zf& Sample No,
Sample Volume +. Acetone Rinses nf Bottle ' . . Beaker jjner +• Sample Residue Weights
start \ . end : Gross JA/t. Date Time
Beaker + Liner + Sample + Rinses Wt. /t?A*?
Beaker + Liner Tare Wt. ?&*£ •
A. ....... Sample 4- Rinses Wt.
B. Water Wt. from Recovery Data: .
C. - Acetone Wt. (A ~,B)r
D. - - - - Acetone WtJO.TS = mLs Acetone:
Beaker Liner + Residue GrdSS"Wo!ght"used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))y(B + D) = O mg/mL
Volume (B + OS for data entry = -fyd,^ rnLs
Comments:
Run No. //& Beaker No. *•
-------
PARTfCULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type; 25OmL Teflon*
Aeatone Lot No. &f3^"J Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. ./XV7 Beaker No. «*•*• ^~ Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner 4-Sample + Rinses Wt. .X*?^ ~?
Beaker + Liner Tare Wt. ?ff>3
A. Sample + Rinses Wt.
B, - Water Wt. from Recovery Data:
C. Acetone Wt, (A - B):
D, Acetone Wt./0.79 = mLs Acetone:
Beaker Liner 4- Residue Gross Weight used for data entry:
Beaker Liner Tare Weight.frorn Tare Weight Data:
Combined Blank = ({Water Blank x 81 + (Acetone Blank x D))/(B + D) = O mg/mL
Volume {B + D) for data entry = f/^S" mLs
Comments:
Run No. / Beaker No. .....'. ....... -' Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start .. end : Gross Wt. _ Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
A, Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C, Acetone Wt. (A - SI:
D. Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue GrossfWe'ig'Evf'Used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) +• (Acetone Blank x D))/(B + D) = O mg/mL
Volume (B + D) for data entry = •3^,'S. mLs
Comments:
Run No, /<•?/?" Beaker No. ** *r Sample No. S3O&*
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. S&7*
A. ------------- Sample + Rinses Wt.
B. Water Wt. from Recovery Data;
C. Acetone Wt, (A - B):
D. - - - - Acetone WI./0.79 = mLs Acetone:
..
Beaker Liner + Residue Gross Weight used for data entry: 3s
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x DH/(B + D) = P__ mg/mL
Volume (B + Dl for data entry = ^/,& mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5JPVIR!X,WI"D Jung 5, 1998 Srev. M17PMRH,WPD Juiy 2,19991 -| Q
ICal APPENDIX D
-------
PARTiCULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MR! Project No, 4702,02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. &$3&- "3_ Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit; grams s
&'-m s* t
Run No. S3B Beaker No. £?& Sample No. gfa^g^jg'^?
Sample Volume + Acetone Rinses of Settle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /ffA 7
Beaker •+• Liner Tare Wt.
A. ----- - Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C. ,- - Acetone Wt. (A - B):
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))/(B 4- D} = O mg/mL
Volume (B + D} for data entry = 3&'~7 mLs
Comments; . •
Run No. /¥?? Beaker No. )
B. Water Wt. from Recovery Data: ,
C. Acetone Wt. (A - BS;..,
D. - - - - Acetone Wt./0.79 = mLs Acetone: ,
Beaker Liner + Residue GrdsS'We'igW Used for data entry:
Beaker Liner Tare Weighlfrom Tars Weight Data:
Combined Blank = ((Water Blank x B! + (Acetone Blank x DH/(B + D] = u mg/mL
Volume (B + D) for data entry = ,3(5T*/_ mLs
Comments:
Run
Beaker
A -
B, -
C -
D. -
No. W& Beaker No. &7
Samole Volume + Acetone Rinses of Bottle
stert
+ Liner + Sample + Rinses Wt. JlTff-'Z. -
Beaker + Liner Tare Wt, /&•£?. ~y*~
Sample + Rinses Wt. 3
Water Wt. from Recoverv Data:
Acetona Wt (A - BV $
Acetone Wt./0.79 = mLs Acetone: >5
Sample No.
end
~
•... i "••-"
'&, C>
d>
*&,D
'&P
JV&frZ*)
Beaker Liner -•
Gross Wt,
3>?$te
3".. y&itZ
f- Samole Residue Weiahts
Date Time
07-/j-<)9 SJZo
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))/{B -t- D) = O mg/mL
Volume [B + D) for data entry = 3-£">® mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
nn M5IPMR1X.WPD June S, 1998 (rev. M17PMRI1.WPD July 2. 1999!
ICal APPENDIX D
-------
PART1CULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. J?£3fe3 Water Lot No,
Sample Treatment: Acetone and water samples evaporated it ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. /&P7 Beaker No. j%? Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. /P^V -— 3>7J& 'Z~ /7^/~^9 JJZQ
A. Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C. Acetone Wt. !A - B): .
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weightjrom Tare Weight Data:
Combined Blank = {{Water Blank x B) + (Acetone Blank x D)}/(B 4- D) = O mg/mL
Volume (B * D> for data entry = >37>& mLs
Comments:
Run No. AS" 0 Beaker No. "ff? • Sample No.
Sample_Volurne + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end " Gross Wt. Date Time
Beaker4-Liner-!-Sample4-Rinses Wt. S#P*6f • -"—" *3jl#?&'7
Beaker 4-Liner Tare Wt.
A, .......... Sample + Rinses Wt.
B. Water Wt. from Recovery Data:. r_
C. Acetone Wt. (A - $fo.;^33~3fi.
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner 4- Residue Gross Weight used for data entry:
Beaker Liner Tare Weight'from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))/(B 4- D) = O mg/mL
Volume (B + D] for data entry = •y.ffkS"' mLs
Comments:
Run No. /t>S7 Beaker No. ^36. Sample No.
Sample Volume + AcetoneJiinses of Bottle Beaker Liner + Sample_Residue Weights
start end Gross Wt. Date Time
Beaker + Liner4-Sample + Rinses Wt. /'3A& ~^,_.,..,,, _^.?«<^?-....J 67*•&-$? SSXO
Beaker 4- Liner Tare Wt. /£jg.^ 3> 7&3J
A. Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C. - Acetone Wt. (A - B): Zg"^
D, - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))/(B -f D) = C mg/mL
Volume (3 + Dl for data entry = 5&*j mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
MSIPMRIX.WPD Jun« 5, 199fl i«f, M17PMH11 ,WPD July 2, 19991 . n-l
ICal APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA '
MR! Project No. 4702.02,04.09
Client/Source: U.S. EPA OAQPS EMAD EMC I Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. SO 3^3 Water Lot No.
LsdhtSff*
/">"•
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. /&& Beaker No. 3V Sample No.
Sample Volume -f Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt.. Date Time
Beaker4-Liner + Sample + Rinses Wt,
Beaker + Liner Tare Wt.
A. Sample + Rinses Wt.
B. Water Wt. from Recovery Data: • O
C. Acetone Wt. (A - B): _
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ({Water Blank x B) + (Acetone Blank x D))/(B + D) = O mg/mL
Volume (B + D) for data entry = !&#,& mLs
Comments: .
Run No, ///7 Beaker No. "35*- Sample No
Sample Volume + Acetone Rinses of Bottle : Seaker Liner+ . SampleResidue Weights
start . end , , Gross Wt, Date Time
Beaker + Liner + Sampie + Rinses Wt.
Beaker 4-Liner Tare Wt,
A. ------- Sample + Rinses Wt.
B. ------ Water Wt. from Recovery Data:
C, Acetone Wt. (A - Bj:
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank - ((Water Blank x B) + (Acetone Blank x D|)/(B + D) - £>. mg/mL
Volume (B + DS for data entry = £3:"3 mLs
Commsnts;
Run No, s/z? Beaker No. 3^3 Sample No.
S_arnple_Volume + Acetone Rinses of Bottle Beaker Liner + -Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample-f Rinses Wt,
Beakers Liner Tare Wt.
A. -- Sampie + Rinses Wt.
B. Water Wt. from Recovery Data: _ :__ O ,
C. Acetone Wt. (A - B):
D. Acetone Wt.10.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry: 3 >
Beaker Liner Tare Weight from Tare Weight Data: 3->
Combined Blank = ({Water Blank x Bl + (Acetone Blank x D))/{B + D) = & _ mg/mL
Volume (B + D) for data entry = &3 '>? mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms,
22 MS1PMRIX.WPD June 5, 1993 (rev, M17PMRII.WPD Juiy 2, 1999)
ICal APPENDIX D
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surrnan
Beaker Liner Size and Type; 250-mL Teflon®
Acetone Lot No. v
Analyst:
Water Lot No.
Sample Treatment; Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-fi!tered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No.
Beaker No. 3 &
Sample No.
Sample Volume + Acetone Rinses of Bottle
start end
Beaker + Liner-(-Sample-t-Rinses Wt. /•We.-D ~—
Beaker + Liner Tare Wt.
A.
B,
Bsaker Liner + Sample Residue Weights
Gross Wt. Date Time
79 //Z-D
£>
.......... Sample + Rinses Wt.
Water Wt. from Recovery Data:
C. .............. Acetone Wt. [A - B]:
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight. from Tare Weight Data:
Combined Blank = ((Water Blank x B) 4- (Acetofie Blank x D)!/{B + D> =
Volume tB +• D) for data entry =
Comments:
a
mg/mL
mLs
Run No.
Beaker No.
Sample No.;
Sample Volume
Acetone Rinaea of.Bottte ' •
start . " end
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
A. Sample
Beaker Liner
Gross Wt.
Sample Residua Weights
Date Time
+ Rinses Wt.
B, Water Wt. from Recovery Data:
C. Acetone Wt. (A - B):
D. - - - - Acetone Wt./0.79 = mLs .,
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank - ((Water Blank x B) 4- (Acetone Blank x D))/(B + D) =
Volume {B -r D) for data entry =
Comments:
mg/mL
mLs
Run No,
Beaker No. ,,,,<5t4JL_
Sample No.
Sample Volume -r Acetone Rinses of Bottle
start . end
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt.
A.
Beaker Liner
Gross Wt.
Sample Residue Weights
Date Time
Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C. Acetone Wt. (A - B|:
D. - - - - Acetone Wt./0.79 = mLs Acetone;
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x 8) + (Acetone Blank x D))/(B + D) = .
Volume (8 + D) for data entry =
Comments:
&S3S+
o
mg/mL
mLs
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMRIX.WPD June 6. 1998 (rev. M17PMR11.WPD July 2. 1S991
ICal APPENDIX D
23
-------
PARTICULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04.03
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon® _ '
Acetone Lot No. &'£>&&•% Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. /vO Beaker No. v s Sample No.
Sample Volume + Acetone Rinses of Bottle . Beaker Liner + Sample Residue Weights
start end Gross Wt. Data Time
Beaker + Liner + Sample 4- Rinses Wt. //£">3
Beaker + Liner Tare Wt. 8$"?. —— 3,
A. Sample + Rinses Wt. 3£3
B. Water Wt. from Recovery Data: O
C. - - Acetone Wt. (A - B(:
D. Acetone WU0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data;
Combined Blank = ((Water Blank x B} - (Acetone Biank x Dl)/(B + D) = D mg/mL
Volume (B 4- 0} for data entry = *}£// mLs
Comments: ' •
Run No. yP/v Beaker No. '«•>;? -Sample No.
Sample Volume + Acetone Rmsos of Bottle . . ' BeakerJJner 4- Sample-Residue Weights
start ' end ' " , Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt. /SSSTo
Beaker + Liner Tare Wt. .^/Jt^JuJiS— - -—""" ...-•- . &' &&P& £>'J~S&-39r ^9Gf"
A. - - Sample + Rinses Wt. ^7-7 ..
B. Water Wt. from Recovery Data: O . -
D. - - - - Acetone Wt./0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data: £?> fo &&:%>
Combined Blank =••(Water Blank x B) 4- (Acetone Blank x DJ]/(B + D| = O mg/mL
Volume (B + D) for data entry = &S"* J mLs
Comments:
Ru
n No. r?O& Beaker No. 3*?
Sample No.
Samole Volume + Acetone Rinses of Bottle
Beake
A.
B.
C.
D.
start
r + Liner -•- Sample + Rinses Wt. /3<%i&"
Beaker + Liner Tare Wt. X,L-
33/7
Z?O0 O3
Beaker Liner 4- Sample Residue Weiahts
Gross Wt. Date Time
&*&'';?&*/ £>y*-j*$'~&$ fl^jD
gls&i^&y g)7-J''?-l$ty ^^fi^"
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blank x B) + (Acetone Blank x D))/(B + D) = _^s.0_ mg/mL
Volume (B + D) for data entry
Comments: //
NOTE: Contro! liner and reagent blank weight data and balance check data are documented on other forms.
24 M6IPMRIX.WPO June 5. 19SS (r
-------
PART1CULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter! Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon*
Acetone Lot No. Qi? 3^3 Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. jxspf Seaker No. W Sampie No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner..+_ Sample Residue Weights
start end Gross Wt. Date _ Time
Beaker + Liner4-Sample-t- Rinses Wt,
Beaker + Liner Tare Wt.
A Sample + Rinses Wt.
B. ---.,. Water Wt. from Recovery Data:
C. Acetone Wt. (A - B):
D. Acetone Wt./0.79 = mLs Acetone: 3^7
Beaker Liner -f Residue Gross Weight used for data entry: j*:-
Beaker Liner Tare Weight from Tare Weight Data: 3*
Combined Blank = ((Water Blank x B) + {Acetone Blank x D))/(B + D) = C> mg/mL
Volume (B * D! for data entry = ^ST'7 mLs
Comments: ' ' .'
Run No. Z mg/mL
Volume (B + D! for data entry = %*7fS mLs
Comments:
Run No. f^yy? Beaker No. ¥**• Sample. No.
Sample Volume + Acetone Rinses of Bottle BeakerJJner 4- Sample..Residue Wgights
start end Gross Wt. Date . _ Time
Beaker + Liner -(-Sample + Rinses Wt.
Beaker + Liner Tare Wt.
A. - Sample -I- Rinses Wt. J?.x£J?
B. — --- Water Wt. from Recovery Data:
C, Acetone Wt. [A - B):
D. Acetone Wt./0.79 = mLs Acetone: "^-^
Beaker Liner + Residue Gross Weight used for data entry: ;
Beaker Liner Tare Weight from Tare Weight Data: *
Combined Blank = ((Water Blank x B) + (Acetone Blank x D)}/{B + D) - O mg/mL
Volume {B + D) for data entry = .4^^ mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
M5IPMWX.WPD Jyn«5, 19S8 (raw. M17PMRI1.WPD July 2, 1399) 25
ICal APPENDIX D
-------
PART1CULATE MATTER (FRONT-HALF) RINSES ANALYSIS DATA
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon® _ /'.
Acetone Lot No. Sp 3&3 Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA*fiItered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. X^M ... Beaker No, v3 Sample No.
Sample Volume 4- Acetone Rinses of Bottle * Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner+ Sample +Rinses Wt.
Beaker + Liner Tare Wt.
A. Sample + Rinses Wt.
B. Water Wt. from Recovery Data:
C, Acetone Wt. (A - B):
Acetone Wt./0,79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data;
Combined Blank = ((Water Blank x B) + (Acetone Blank x 0)}/(B + D} = O mg/mL
Volume (B + Dj for data entry = #&J mLs
Comments:
Run No. yg/7 Beaker No. vty :.., Sample No.
Sample Volume ± Acetone Rinses of Bottle ' • Beaker Liner + Sample Residue Weights
start " end Gross Wt. Date . Time
Beaker + Liner+ Sample +Rinses Wt. JS-jftf -'• . .._ 3'"3
Beaker-i-Liner Tare Wt. S&Jtf' 33
A. Sample + Rinses Wt. __|S
B. Water Wt. from Recovery Data: £>
C. Acetone Wt. (A - B}:
0. — - Acetone WH./Q.79 = mLs Acetone:
Beaker Liner 4- Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:
Combined Blank = ((Water Blenk x B) + (Acetone Blank x D))/{B + D) = O mg/mL
Volume {B + D} for data entry = y<43 mLs
Comments:
Run No. *?3 & Beaker No. ^ff" Sample No. £?3£>D'3
Sample Volume + Acetone Rinses of Bottle Beaker Liner jh...Sample Residue.Weights
start end Gross Wt, Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker •+- Liner Tare Wt. _j^ifi(Jl__ ~ 3,4*33..
A. - - - Sample + Rinses Wt. j-^Qr
B, Water Wt. from Recovery Data:
C. Acetone Wt. (A - B):
D. - - - - Acetone Wt./G,79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:
Beaker Liner Tare Weight from Tare Weight Data:,
Combined Blank = ({Water Blank x B) + (Acetone Blank x D))/(B -I- D) = C? mg/mL
Volume {B + B) for data entry = &S?f7 mLs
Comments:
NOTE: Control liner and reagent blank weight data and balance check data are documented on other forms.
OR MBIPMRIX.WPO JuneS, 199B (rev. M17PMRI1.WPO July 2. 1989)
ICal APPENDIX D
-------
PART1CULATE MATTER (FRONT-HALF] RINSES ANALYSIS DATA
MRI Project No. 4702.02.04,09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst:
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No, J&&34ri3 Water Lot No.
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Weight Unit: grams
Run No. &<¥ff Beaker No. ^t> Sample No.
Sample Volume + Acetone Rinses of Bottle Beaker Liner + Sample Residue Weights
start end Gross Wt. Date Time
Beaker + Liner + Sample + Rinses Wt.
Beaker + Liner Tare Wt. SP/'"^ ——....
A. ------- Sample + Rinses Wt.
B, - Water Wt. from Recovery Data:
C. Acetone Wt. (A - B}:
D. Acetone Wt/0.79 = mLs Acetone:
Beaker Liner + Residue Gross Weight used for data entry:,
Beaker Liner Tare Weight, from Tare Weight Data:
Combined Blank = {{Water Blank x B) + (Acetone Blank x D)»/(B + D> = O mg/mL
Volume (B + D} for data entry = £',
ICal APPENDIX D
-------
PARTICULATE MATTER CONTROLS ANALYSIS DATA
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman __ Analyst;
Balance: $M& :£& - s'i&Pj '
Weight Unit: grams
Control Filter Assembly Weights & Balance Checks:
Assembly No. _J[3___ NIST Weight(s): - Assembly No. <=>f* x NIST Weight(s):
Original Tare Wt.: &]3.*J&>"7 Original Tare Wt.: _J
Current Wt. Date Time Balance Reading Current Wt. Date Time Balance Reading
Comments:
Control Beaker Liner Weights & Balance Checks:
Beaker No. ^"^ NIST Weights): ' - Beaker No. -S^y £_ NIST Weight(s):
Original Tare Wt,: _3*&'793 ' ' ' Original Tare Wt.:
2^_
Current Wt. Date Time Balance Reading' 'Cffiffint Wt. Date Time Balance Reading
t>7 -
Comments:
Controls are filter assemblies and beaker liners selected from the original prepared lots that are used for sampling and analysis. The1*
are processed along with the assemblies and liners containing samples during analysis, i.e., they are heated, desiccated, and weighec
along with the assemblies and liners containing samples. The results are not used for correcting analytical data, but are useful it
monitoring changes between original tare weights and weights obtained during analysis of samples. Significant changes couh
indicate problems in maintaining relatively constant environmental conditions in the laboratory, processing procedures not replicatint
those used when tare weights were obtained, instrumentation calibration drift, and desiccant deterioration.
Each time filter assemblies or beaker liners are weighed, the balance is checked for accuracy by weighing NIST certified weight;
approximating the weights of the assemblies or liners.
M6IPMCOX.WPD JuneS, 1SB8 (rev. M17PMC01.WPD July 2. 1S98I
28
ICal APPENDIX D
-------
PARTICIPATE MATTER CONTROLS ANALYSIS DATA
MR! Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse [Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman _ Analyst;
Balance;
Weight Unit: grains
Control Filter Assembly Weights & Balance Checks:
Assembly No. J^> NIST Weight(s): Assembly No. 3& NIST Weight(s|;
Original Tare Wt.: 3,&3_y/ Original Tare Wt.: _J
/^
Current Wt. Date Time Baianrfe Reading Current Wt. Date Time Balance Reading
Comments:
Control Beaker Liner Weights & Balance Checks:
Beaker No. 3& N|ST Weightfs): 'Beaker No. &&* NIST Weight(s):
Original Tare Wt.: <=#. 4S0&3 Original Tare Wt.: £•
Current Wt. Date Time Balande Reading Current Wt. Date Time Balances' Reading
£?£?£>
*3-9 9
67-&-W
/;(?£> V®
Comments:
Controls are filter assemblies and beaker liners seiectad from the original prepared lots that are usad for sampling and analysis. They
are processed along with the assemblies and liners containing samples during analysis, i.e., they are heated, desiccated, and weighed
along with the assemblies and liners containing samples. The results are not used for correcting analytical data, but are useful in
monitoring changes between original tare weights and weights obtained during analysis of samples. Significant changes could
indicate problems in maintaining relatively constant environmental conditions in the laboratory, processing procedures not replicating
those usad when tare weights wers obtained, instrumentation calibration drift, and desiccant deterioration.
Each time filter assemblies or beaker liners are weighed, the balance is checked for accuracy by weighing NIST certified weights
approximating the weights of the assemblies or liners.
M5IPMCQX.WPD June 5 1998 Irev. M17PMCO1.WHD July 2, 19991
29
ICal APPENDIX D
-------
BEAKER LINER TARE WEIGHT DATA
MR! Project No. 4702.02.04.09
Sampling Team Leader: Jim Surman
Beaker Liner Size and Type; 250-mL Teflon®
Analyst:
Beaker Liner Treatment: Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
Weight Unit: grams
Date: £>t>
COMMENTS:
MSIBBAKX.WPO June 4, 1998 [fev. M17BEAK1,WPD July 2, 19931
30
ICal APPENDIX D
-------
BEAKER LINER TARE WEIGHT DATA
MRI Project No. 4702,02.04.09
Sampling Team Leader: Jim Surrnan
Beaker Liner Size and Type: 250-mL Teflon®
Analyst;
Beaker Liner Treatment: Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
Weight Unit: grams
Time Started:
Balance Check before beaker liners are weighed:
Balance Used: ^WP &%•*/£&/?
Weight Value:
Balance Reads: ~"
Beaker Liner in
Baaker I.D. No.
ffS
First Weiahina
Second Weiahina
Third Weiahina
Average Weight
or Weight to be
Used as the Tare
3, '
30
3 -
Jf ,, •
33
.. 330*
Balance Check after beaker liners are weighed:
Balance Reads: /,£>/>(>(> /,t?DQO
COMMENTS:
MSIBGAKX.WPD Juno 4, 1988 (rev. M178EAK1 ,WPD July 2,1989)
ICal APPENDIX D
31
-------
BEAKER LINER TARE WEIGHT DATA
MR! Project No. 4702.02.04.09
Sampling Team Leader: Jim Surman Analyst:
/ &
Beaker Liner Size and Type: 250-mL Teflon® /
Beaker Liner Treatment: Wash to clean, rinse with Dl water, dry at 105 °C, insert into glass beakers previously
cleaned in the same manner, desiccate for 24 hours, and weigh to a constant.
Weight Unit: grams
Date:
Time Started:
Balance Check before beaker liners are weighed:
Balance Used: y%»2?
Weight Value:
Balance Reads: £
Average Weight
Beaker Liner in or Weight to be
Beaker1.D. No. First Weighing Second Weighing Third Weiohino .Used as the Tare
3, ?36&
3# 3,
39 3.
3S33ZL
67 3>7&2^ 3>7&3%
Balance Check after beaker liners are weighed:
Balance Reads: X-
COMMENTS:
MSIBEAKX.WPD June4. Ii98 {rev. M17BEAK1 WPD July 2. 1S9SJ
32
ICal APPENDIX D
-------
PART1CULATE MATTER REAGENT BLANK ANALYSIS DATA
MRI Project No. 4702,02.04.09
Client/Source; U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Sampling Team Leader: Jim Surman Analyst;
Beaker Liner Size and Type: 250-mL Teflon®
Acetone Lot No. />£> 3&>3 Water Lot No,
Sample Treatment: Acetone and water samples evaporated at ambient temperature and pressure in an
enclosure with HEPA-filtered air; then, desiccated and weighed to a constant weight.
Filter Size and Type: 47mm diameter, Whatman 934-AH glass fiber filter
Filter Lot No. 29439A
Assembly Components; filter, aluminum foil gasket, 316 stainless steel filter support
Filter Assembly Treatment: Heated at 10S °C for 3 hours, desiccated and weighed to a constant weight.
Weight Unit: grams
Acetone Blank Determination: For Run No.(s) J Beaker No. C^ Sample No.
Acetone Reagent Blank Sample Volume Beaker Liner. + Sample Residue Weights
Gross Wt. Date Time
Beaker + Liner + Acetone Sample Wt. /ffi.?; 3, 8-?8(* £>y~st>~$ 7 3>g;fS"7
-------
40 CFR 60, APPENDIX A, METHOD 17 - PARTICULATE MATTER TRAIN [Ml7)
FIELD REAGENT BLANK PREPARATION DATA
MRI Project No. 4702.02.04.09
Client/Source: U.S. EPA OAQPS EMAD EMC / Cogentrix Unit 2A
Source Location: Rocky Mount, North Carolina
Sampling Location: Baghouse (Fabric Filter) Outlet Duct
Blank(s) Prepared By: *r Date; 0?~0&^&
Weights below are in grams.
Sample Bottle Tare Bottle Gross Net Sample
Reagent Blank Description . Number Weight __ Weight Weight
Acetone for paniculate matter
Volume needed: "IQOmLs
Lot Number: &O36-3 /005
Acetone for particulate matter
Volume needed: 10QmLs
Lot Number: _ 005
ASTM Type I water for particulate matter
Volume needed: 100 mLs
" Lot Number: _ •
ASTM Type I weter for particulate matter" , .
Volume needed: 100 mLs
Lot Number: _ ' 006
Filter Assembly for particulate matter
Type: Whatman 934-AH
Filter Assembly Number:
Filter Lot Number: #?& j 007
Filter Assembly for particulate matter
Type: Whatman 934-AH
Filter Assembly Number;
Filter Lot Number: 007
NOTE: Lots may be identified above by a manufacturer's lot number or by the date of reagent preparation. If different lots of
a particular reagent are used, indicate the applicable test and/or run number(s) and sampling location(s) where the train(s)
loaded and/or recovered with that reagent are used (i.e., list each reagent blank sample number with the applicable test
and/or run nurnbertsy and sampling location(s) belowi.
Sample Number(s) For Test and/or Run Humberts) For Sampling Lgcatipnfs).
COMMENTS: /*et*»~* '* 9$ &*r
' Jj/nffJ -fy
M17DBLK.WPD May 13, 1B89 !rov. M17DBLK1.WPD July 2, 19991
34
ICal APPENDIX D
-------
ICal Appendix E
W117 Post-Test Calibration Sheets
MRJ-OPPTO4703-02-07 Appendices Covtrs.WPD
-------
ON SITE MERCURY BAROMETER READING CORRECTION
AND ANEROID BAROMETER CALIBRATION CHECK ATTEST LOCATION
Mercury Barometer Description: Prince Model 453, S/N W13559
Mercury Barometer Location: Plant Control Room
Distance Of Barometer From Test Site: 0.00 miles
Altitude Of Barometer Above Sea Level: 124.0 feet
Latitude (north): 36 degrees, 0.00 minutes
Facility: Cogentrix of Rocky Mount, North Carolina
Test Site And Sampling Location: Unit 2A Baghouse Outlet Duct
MRI Project No. 4702.02.04,09
Date: 07/20/99
Time: 1130
Readings Obtained By: J. Surman
•Observed Barometer Reading: 30.03 in. Hg
Mercury Column Temperature: 71 CF
Correction For Temperature: -0.11 in. Hg
Reading Corrected For Temperature: 29.92 in. Hg
Correction For Gravity: -0.03 in. Hg
Temperature Corrected Reading Corrected For Gravity: 29.89 in. Hg
Aneroid Barometer I.D. No.: Y-2101
Reading Before Adjustment: 29.89 in. Hg
Calibration Check Result: within 0.1 in. Hg
Reading After Adjustment; " in. Hg
Remarks:
BAROMETR.WK4 10/19/98 (rev, BAR04702.WK4 07/22/99 01:27PM)
ICal APPENDIX E
-------
/ff
/ 1
b
/jo
v
/
ICal APPENDIX E
-------
ON SITE MERCURY BAROMETER REA05HG CORRECTION
AND ADJUSTED BAROMETRiC PRESSURE AT TEST LOCATION
Mercury Barometer Description: Princo Model 453, S/N W13559
Mercury Barometer Location: Ptent Control Room
Distance Of Barometer From Test Site:
Altitude Of Barometer Above Sea Level:
Latitude (north):
0.00
124.0 feet
36 degrees,
0.00 minutes
Facility; Cogentrfce of P,oeky Mount, North Carolina
Teat Site And Sampling Location: Unit 2A Baghouse Outlet Duct
MRI Project No. 4702.02.04.09
Dale: 07/20/99
Time: 1130
Readings Obtained By: J.Surman
Observed Barometer Reading: 30.03 in. Hg
Mercury Column Temperature: 71 T
Correction For Temperature: -0.11 in. Hg
Reading Corrected For Temperature: 29.92 in. Hg
Correction For Gravity: -0.03 in. Hg
Ternperatyre Corrected Reading Corrected For Gravity;
29.89 in. Hg
Aneroid Barometer I.D. No.: Y-2101
Reading Before Adjustment: 29.89 in. Hg
Calibration Check Result: within 0.1 in. Hg
Reading After Adjustment:
in. Hg
Remarks:
6AROMETR.WK4 10/19/88 (rev. BARO47Q2.WK4 07/20/89 11:45 AM)
ICal APPENDIX E
-------
METHOD 5 METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
MRI Project No.
Date:
Operator:
_j470_2-C2-04^9_
7-20-99
D, Nea!
Metering Console No. |
Previous Dry Gas Meter Factor (Y): 1
Calibrated Critical Ortflce No. i
N10
1.011
D19
_Crjttgal_Ortf)ce Coefficient in English Units (K1):
Ambient Temperature Meter No.
J051210__
Y-0815
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, *F:
Initial Inlet Temperature, °F
Final Inlet Temperature, °F
Initial Outlet Temperature, "F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter Delta-H, inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, °F
Final Ambient Temperature, °f
Avg. Critical Orifice Inlet Temperature (tamb), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std, ft3
Dry Gas Meter Gas Volume {Vm (std)), std. ft.3
Dry Gas Meter Calibration Factor (Y)
Orifice Meter Delta-H@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter Delta-H@
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
Y= 1.019439290348411
Run 1
1 f-" S.V t, " f A
705299" '
" "711.960
6661
:A
009%'
PASS
Run 3 |
*' Mil'' ^--*
71*8 640
" 725.329
6.689 i
/ . ' '•"'.' ' '','
92.0
93.0
88.0
89.0
90.5
600
1450
2989
,.>-•* <'
85'4
842
848
18
j_ •*' " '
6560 "
8.432
1.020
1.829
0"05%"°
PASS
Remarks:
CRORCALB.WK4 10/24/96 (rev. 4702N10.WK4 07/20/99 10:17 AM)
ICal APPENDIX E
-------
METHOD i METERING CONSOLE CALIBRATION
CRITICAL ORIFICE BRACKETING DATA
MR! Project No.
Date:
Operator:
Metering Console No.
Dry Gas Meter Factor (Y):
Orifice Used for trie Calibration:
Ambient Temperature Meter No.
Note: Critical orifice coefficients are
4702-02-04-09 Critical Orifice Being Evaluated
7-20-99 .Critical Orifice No.
D. Nea!
i N10
D19
Critical Orifices Used For Bracketing
firsLOrifce
; 1.019 I Critical Orifice No.
D19
j Y-0815
In English units.
Coefficient (K1)
Second Orifice
Critical Orifice No
Coefficient (K1)
D16
044410
D24
0.65490
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft3
Net Dry_Gas Meter Gas Volume (Vm), ft a
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, °F:
Initial Inlet Temperature, °F
Final Inlet Temperature, "F
Initial Outlet Temperature, "F
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm). 'F
Time, seconds
Orifice Meter Delta-H, inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F;
Initial Ambient Temperature, °F
Final Ambient Temperature, °F
Average Critical Orifice Inlet Temperature (lamb), *F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std. ft3*
Dry Gas Meter Gas Volume (Vm (std)), std. ft.3
Factor (Y) Obtained With Bracketing Orifice
CRITICAL ORIFICE ACCEPTABILITY
Criterion: All Ys Must Be Within 2% Of Alt Other Ys
Larger % Difference Between Dry Gas Meter Factor (Y)
And Factor (Y) Obtained. With The Bracketing Orifice
Larger % Difference Between Factors (Ys)
Obtained With Bracketing Orifices
Acceptability Result
First Onfice
U- . '.,.,,.., :.-.-,'.,
732.300
[ 738.148" '
5848
"' 94.6
Second Orifice
•~ .1 '** « ~" L '" '
736.504
747.149 !
8.645 "
*t -'\ . V i
'ge.o" "
95.0 I 99.0
91.0 92.0
91.0 j 93.0
92.8
600
1.100
.^_ 29.89
85 8 '
86.6
86.2
18
568-!
5.595
"1015
, *V •
035%
6.26%
[ 95.0 |
600
2,500
_;29.89__ __
868
874
87.1
18
8.371
8.266
~ 1".013
0.62%
, • • fit ' ' ,* -
All Orifices Are Acceptable
Remarks:
CRORBRKT.WK4 10/24/96 (rev. 4702N10B.WK4 07/20/99 10:24 AM)
ICal APPENDIX E
-------
CONSOLE CALIBRATION WORKSHEET
Job No , 7 /<*>-• 0J- " Oi-6 /
Date f-^-ff
Performed By & . /J&Jil-
Console No ,
Orifice No,
K Factor
///o
0/9
0.£t>t
Barometer J"^• ^ ? in. Hg . Previous Y /< &//
NOTE: Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring mercury manometer up
to 18.0 in, Hg. Record mercury manometer and console vacuum
gauge readings below. Insert critical orifice into console
sample orifice. Set console vacuum gaug'e at 18,0" in. Hg. +/-
the console vacuum gauge correction factor calculated below.
Mercury manometer readings: tJ/& + /\/^ = 18.0 In. Hg.
Console vacuum gauge reading: - /^/x] In. Hg,
Console vacuum gauge correction factor: /o - 3 In. Hg.
RUN #1 RUN #2 RUN #3
DGM Initial Volume:
Initial:
Final. . ...
^3«-?V
DGM Inlet Temperature: Tv*-'1
Initial: 88
Final: ?3
DGM Outlet Temperature: , „-
Initial: 8i B7 ' BB
Final: &' 67 fif
Time of run f In Seconds ) : £&* 60s £06
Orifice Delta H (in. H20) :
Room Temperature:
Initial
Final
&V.B
Pump Vacuum (in. Hg ): 18.0 __JilJL__ 18.0
Calibration Rccords\Calibnirion Forms^concahvs4d.d«e Revised 02/03/W
ICal APPENDIX E
-------
CONSOLE BRACKETING WORKSHEET
Job No. e/jO^Qd-oV-Q Console No,
Date 7-^~g>-ff _ Bracketing Orifice No , 1
Performed By ft.ff*^ _ K Factor O.
Calibration Orifice No, £/9 Bracketing Orifice No. 2
New Y Factor /.*/ K Factor 6.
Barometer $'?<&?' in . Hg .
NOTE : Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring, mercury manometer up
to 18.0 in. Hg . Record mercury manometer and console vacuum
gauge . readings below. Insert critical orifice into console
sample orifice. Set console vacuum gauge at 18,0 in. Hg, +/-
the console vacuum gauge correction factor calculated below,
Msrcury manometer readings: /J/.ff + ^>/^ = 18 . 0 in. Hg ,
Console vacuum gauge reading: - /J/ic in. Hg .
Console vacuum gauge correction factor: /$.o in, Hg,
RUN #1 RUN #2
DGM Initial Volume;
Initial:
Final: 738 JW T11. /
DGM Inlet Temperature:
Initial:
Final:
DGM Outlet Temperature:
Initial: *?/ f.
Final: f/
Time of run ( In Seconds ) : &&*•
Orifice Delta H(in. H2O) : /, /
Room Temperature:
Initial: &S-O
Final: 86. b $7,1
Pump Vacuum (in. Hg ): 18 , 0 18.0
Calibration Recor^\6Uibnrtion Forms\caHlUrlUn4d,doc Revised 02/03/99
1
ICal APPENDIX E
-------
Job No,
M5 CONSOT.K POST TEST CHEOCT.TST
Date
Console No.
Performed By
6 / GO*-'
Place a check (in black ink) in the space provided after the
required checks are performed,
!• ,.u,N. Perform positive leak check of Delta H manometer,
- (See back of this sheet.)
\
Leak check Delta P manometer.
__///jQ_ Clean pump.
__v__ Clean muffler jar(s).
v
Inspect/refill oiler jar.
6,- \> Calibrate DGM thermocouples:
Npte : Reading must be
Within +/-5.4°F
DGM Inlet : [
DGM Outlet: (
Reference
Thermometer*
°F
^nrf
'xfynrf
DGM
Thersnocouple
°F
7.
8,
\
Digital clock/timer in place and functional.
y Vacuum check. (Leak check at 25 in. Hg , vacuum. Leak
rate should be zero, )
__M_ Check indicator lights.
10. v Check thermocouple switched.
11. V Check fan.
12. y Check pump heater,
Check heat controllers,
13
V
Check Orsat pump and rotair.eter.
If any of the above items were replaced or repaired, please
document that information below:
* Reference Thermometer :
ij, Serial Number:
Catilir.Ltiim Records\Calibration Forms\M5check.doc
Revised 10/28/99
ICal APPENDIX E
-------
Procedure for positive leak check Dalta H manometer:
10
Pump mustnot be run prior to this test. Pump needs to be
cool in order to get an accurate reading.
Pump pressure and vacuum lines must be connected to console,
Null, switch on console must be in the down position so
solenoid valve is open to the sampling stream as it is
during testing.
Plug meter exhaust and clamp off bottom tube from exhaust
which goes to the Orsat pump.
Plug sample orifice.
Close main flow control valve.
Open fine control valve.
Disconnect right side Delta H manometer tub© on front of
console.
Blow into tubing until manometer reads 5 to 7 inches of
water, and clamp off.
There should be no change in manometer reading,
Make certain you remove plug and..... clamp,, Jfr-om.-ne,t.gr._exh.aus±
jinnigdistgly after this test to avoid., damage fco the m.eter_
DUMB when pump..is started UP!
caiibrec\mS«*eck 03/09/9S
ICal APPENDIX E
-------
METHOD S METERING CONSOLE CALIBRATION WITH CRITICAL ORIFICE
MRI Project No.
Dale:
Operator:
4702-02-04-09
7-20-99
D. Neal
r Metering Console No.
Previous Dry Gas Meter Factor (Y):
Calibrated Critical Orifice No.
Critical Orifice Coefficient in English Units («'):
|| Ambient Temperature Meter No.
1 Nil
0.988
D19
0.51210
Y-0815
CALIBRATION GAS VOLUME DATA
Initial Dry Gas Meter Gas Volume, ft.3
Final Dry Gas Meter Gas Volume, ft.3
Net Dry Gas Meter Gas Volume (Vm), ft.3
CALIBRATION CONDITIONS DATA
Dry Gas Meter Temperature, '°F:
Initial Inlet Temperature, °F
Final Inlet Temperature, "f
Initial Outlet Temperature, °f
Final Outlet Temperature, °F
Average Dry Gas Meter Temperature (tm), °F
Time, seconds
Orifice Meter Delta-H, Inches w.c.
Barometric Pressure, in. Hg
Critical Orifice Inlet (Ambient) Temperature, °F:
Initial Ambient Temperature, "F
Final Ambient Temperature, "F
Avg. Critical Orifice Inlet Temperature (lamb), °F
Pump Vacuum, in. Hg
COMPUTED CALIBRATION RESULTS
Critical Orifice Gas Volume (Vcr (std)), std. ft.3
Dry Gas Mater Gas Volume (Vm (std)), std. fta
Dry Gas Meter Calibration Factor (Y)
- Orifice Meter Delta-H@
AVERAGE CALIBRATION RESULTS
Average Dry Gas Meter Calibration Factor (Y)
Average Orifice Meter Deita-H@
CALIBRATION RESULTS COMPARISON
Criterion: Y Must Be Within 2% Of Average Y
Percent Difference Of Y From Average Y
Tolerance Result
COMPARISON WITH PRETEST RESULTS
Criterion: Y Must Be Within 5% Of Previous Y
% Difference Of Average Y From Previous Y
Tolerance Result
Y= 1 .02259081 761 1001
Run1
" ' 1,006.701
1,013.332
6.631
t ' w , V -
v,' . • _ . • ,,
88.0
89.0
87.0
87,0
87.8
' 600
1 500
29.89
85.4
84.8
85.1
18
6558
, 6.40i
1.023
1.903
cck '*,-• * :•'•'/,/• iw '
1.023
1.901
0,06%'
PASS
$ ' ~° V * J
'3.51%""
PASS
Run 2
^ * ' J" r \ ' *
*tt*i*:» - »»* V "V" I
1,013.332
1,019.976
6.644
""890 "
90.0
88.0
88.0
88.8
600
1 500
2989
., ^ _ t „ f," j ~"
86.0 " I
86.2
85.6
18
- ••• ~ < '•,^,"'
6*555
6.410
1.023
1.901
•-V ' " (i.
0.00%"
PASS
Run3
" 1,019976*"
1,026.638
6662
" k & "• « „ • f
f r-» *• ~
9i'.d'
92.0
89.0
90.0
90.5
600
1 500
29 89 _^ ^ ^
' 86.4
87.2
86.8
18
t- ^t^"!^ -_^. / i,
" 6.548 '
6.406
1.022
1.899
" 006%'
PASS ;
Remarks:
CRORCALB.WK4 10/24/96 (rev. 4702N11.WK4 07/20/99 10:32 AM)
10
ICal APPENDIX E
-------
CONSOLE CALIBRATION WORKSHEET
Job No,
Date
--£¥-*?/
Performed By 0*
Barometer ffit $ (
Console No.
Orifice No.
K Factor
////
in. Hg . Previous Y
-> 1 S3
NOTE: Prior to running calibration, connect mercury manometer
to sample orifice. Turn on pump and bring mercury manometer up
to 18,0 in. Hg. Record mercury manometer and console vacuum
gauge readings below. Insert critical orifice into console
sample orifice. Set console vacuum gauge at 18.0 in. Hg. +/-
the console vacuum gauge correction factor calculated below.
Mercury manometer readings: A//4 + _///?_. = 18.0 In. Hg,
In. Hg.
DGM Initial Volume:
Initial:
Final:
DGM Inlet Temperature:
Initial:
Final:
DGM Outlet Temperature:
Initial:
Final:
Time of run ( In Seconds ):
Orifice Delta H (in. R,0) :
Room Temperature;
Initial:
Final;
Pump Vacuum (in. Hg );
im gauge
>rrectioi
RUN #1
reading: - A//X
i factor: /&.0
RUN #2
>J /fl/2.73i
/9/i.xi J^l;Jtjv
88
Bf
gq ft
87
81
$8
86
£00 &0
/•£
//?
9)-
ff?
9*
&00
. >
18 , 0
Calibratton ReeordsiCalibration Forms'concalws^d.itnc
ICal APPENDIX E
Revised 02/03/99
11
-------
MS CONSOLE POST TEST CHECKLIST
Job No,
Date
7-70-
Console No.
Performed By
Place a check (in black ink) in the space provided after the
required checks are performed,
\ Perform positive leak check of Delta H manometer.
(See back of this sheet.)
2.
3.
4 .
5.
6.
\-Leak check Delta P manometer.
fJl& Clean pump. .'
\ Clean muffler jar(s).
v Inspect/refill oiler jar.
V Calibrate DGM thermocouples;
Mote: Reading must be
^iJ_hin_:f:/-5 . 4°F
7 . %
DGM Inlet:
DGM Outlet:
Reference
Thermometer*
^£3,3
DGM
Thermocouple
63
83
8 ,
\
10
11
12
13
14 ,
\
\,
V
Digital clock/timer in place and functional.
Vacuum check, (Leak check at 25 in. Hg. vacuum. Leak
rate should be zero . )
Check indicator lights,
Check thermocouple switched.
Check fan.
Check pump heater.
Check heat controllers,
"Check Orsat pump and rotameter.
If any of the above items were replaced or repaired, please
document that information below:
* Reference Thermometer :
Serial Number: .A
12
Calibration Record$\Calibrartan F»mis\M5cl)cck.doc
Hewed 10/28/98
ICal APPENDIX E
-------
Procedure for positive leak check Delta H manometer:
2
3
10
Pump must not be run prior to this test, Puinp needs to be
'cool in order to get an accurate reading,
Pump pressure and vacuum lines must be connected to console.
Null switch on console must be in the down position so
solenoid valve is open to the sampling stream as it is
during testing,
Plug meter exhaust and clamp off bottom tube from exhaust
which goes to the Orsat pump.
Plug sample orifice.
Close main flow control valve,
Open fine control velve,
Disconnect right side Delta H manometer tube on front of
console,
Blow into tubing until manometer reads 5 to ? inches of
water, and clamp off,
There should be no change in manometer reading.
Make ^certain you remove plug and clamp from meter exhaust
immediately _ after this test £.Q. . avoid damage JQ the Meter
pump when pump is started UP f
ralibree\m5eheek 03/09/98
ICal APPENDIX E
13
-------
STACK THERMOCQOPr.E CALIBRATION DATA FORM
No. ¥7Q>-~0>'Q'i-ffct Stack Thermocouple No, 3 T88
Date 7- P-0~?fProbe No, /^
Performed By 0-_/*/&#i-
Avg, Stack Temp, (°F)
Pyrometer No.
Reference Instrument; Hart Scientific Model No. 9100A, Serial
No. 84414 Dry-well, HDRC Handheld Block A, This instrument
is calibrated in accordance with ITS-90 and ANSI/NCSL Z540-1
Reference Instrument
Temp. ( TF )
Pyrometer Temp,
(f)
Temp. Difference
(T)
Temp. Difference
(87
;ref, Temp., F -f 460) - (pyro. Temp., F + 460
(ref. Temp., F + 460)
X 100 < 1,5%
Calibration Rec»rds\CaHbra(ion F»mis\STCHttrt.dnc
Revised 10/29/98
14
ICal APPENDIX E
-------
STACK, THERMOCOUPLE CALIBRATION DATA FORM
Job No.
Date
7
-Jo -99
Stack Thermocouple No. - 3(£84
Probe No. ft
Performed By
Pyrometer No,
3zL<£ _///€>
Avg, Stack Temp. (°F)
Reference Instrument: Hart Scientific Model No. 910QA, Serial
No. 84414 Dry-well, HDRC Handheld Block A. This instrument
is calibrated in accordance with ITS-90 and ANSI/NCSL 2540-1
Reference Instrument
Temp.(T)
Pymmeler Temp,
(*F)
Temp.
Temp. Dlffere»ce
fref. Temp., F + 460) - (pyro. Temp,, F + 460
(r e f. Temp., F + 460)
X 100
1,5%
Calibration RcrairiMCalibrartoB F»rms\STCHartdoe
ICal APPENDIX E
Revised 10/29/9$
15
-------
Type S Pitot Tube Inspection Data Form
Pitot Tube #:
Probe #:
Date: 7-3? ^F?
Job#:
Performed By:
Pitot tube assembly level?
Pitot tube openings damaged?
Y .= _t
z = A sin Y
to = Asin6
Calibration required?
Comments;
Yes
Yes (explain below)
A =
(in); (< 0.125 in)
M; (< 0.03125 in)
Yes
y No
No
No
(in)
16
hLonpludiraf OB
^ Tuse Axis
Note:
1.05 Dt
I A I
Facs
L.
-------
Type S Pitot Tube Inspection Data Form
Pitot Tube #: f\ Date: 'Y^^rt Performed By: ^nj^_
Probe #: j4- Job#: 1^2 -dZ-
Pitot tube assembly level? >^ Yes
Pitot tube openings damaged? Yes (explain below) s
«, - 0 • (
Pi = 2- ° (<5 °). Pa ~ ^ ° (^ °)
Y =^6 °, 9 -/'V*' A = ^ ^ (m)
z = A sin Y ^r ^J/7" v(ia); (< 0. 125 in)
u = Asin6 6,Qfy0% (in); (< 0.03125 in)
PA= tfffyf? (in), PB= O^'l^ • (in), Dt= ' ^-2:
No
<" No
? (in)
Calibration required? » Yes V' No
Comments:
Longitwiinrf n iv
TufoAxis ->_C-2L.
Longitudinal n ^
A TuoeAxis —nT'~—: =J:
PA
A - Side Plane
l.QSD,:
B-Side Hans
0.48 CM «D;< 0.95 CM
(sen.)
Transverse
Tube AM
TT At>rB ~C V I ..jL
Transvarss
Tube Axis
Calibration
flI/18/99
ICal APPENDIX E
17
-------
GOOSENECK THERMOCOUPLE CALIBRATION DATA FORM
Job No,
Bate
Pyrometer No,
A/,'/
Reference Thermometer
Performed By
ZM>rJ Serial Number
Calibration Method; Direct comparison of gooseneck thermocouple
with reference thermometer in ambient air,
Cmue-neck
T,C, No.
/
3%
Leak Check & Check
Valve P«s»/No-pass
firs '
fi<$
' Ret. Tl^njaometer -
Temperature (°F)
(m^)=/^er
fort)--&JF
„
Fyrometer Temp.
(*F)
ff3
B3
Temp. Difference
+/-2°F
0,3" f
o.z'f
Calibration Recor«b\CaBb ration F»rms\Gnlccal.(loc
Revised 10/2S/98
18
ICal APPENDIX E
-------
GOOSENECK TKRPMOCniTPT.F CALIBRATION DATA FORM
Job No.
Date
y"?&3-~ &2 "°V-OY Pyrometer No. C0-*JJcicl ///o
7"(^3i77 Reference Thermometer f~l7At&£3iZ**)Q
Xj. . /> ft
Performed By £/. As£4L<. /{ w^'Seriai Number /5~- *
^-/^
f
Calibration Method: Direct comparison of gooseneck thermocouple
.with reference thermometer in ambient air.
Goose-neck
T.C.No.
n
30
'K
Leak Check & Cheek
y^jj
j?
r«jj
/^//
Ret Thermometer
Temperature ( *F ) •
^,oc>/a^°F
ffa.a r.h^^/2
^. c\-fM*f
Pyrunieier Teinp.
^3
^3
*3
Terap. DilTei^nce
^/-2*F
,, *• frf
*A'F
a, A 7~
Calibration
urznsVGalcoiiLduc
Revised 10/2S/9S
ICal APPENDIX E
19
-------
ICal Appendix F
PM GEMS Data for Each Run
MRI-OFPTVR4TO3-02-U7 Appendices Co»m.WPD
-------
-------
Correlation Testing - Run 10: Medium-High PM concentration - 1st correlation test run
7/15/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc degC_
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
11.88
11.15
11.64
11.97
12.04
12,16
11.52
11.92
10.74
10.50
10,25
10.73
13.96
14.52
14.54
10,62
11.04
11.29
11.56
11.93
11.58
11.98
11.07
10.96
11.35
10.61
10.79
10.99
11.23
9.66
10.21
11.20
12.94
14.16
14.88
9.87
10.07
10.91
9.97
11.14
11.41
11.74
11.58
11.26
11.63
11.40
11.22
11.65
10.63
18.56
18.58
18.52
19.49
19.84
17.61
19.81
20.83
24.28
28.18
28.36 -
21.19
17.40
19.72
21.19
23.26
24.91
24.94
20.17
18.94
18.89
18.55
17.22
17.70
18.00
16.43
16.92
17.63
19.00
25.54
24.64
21.28
16.10
18.58
18.80
19.63
21.61
22.24
17.79
17.56
17.50
18.91
16.66
18.48
19.52
17.22
18.40
18.58
19.99
12.48
12.48
12.48
12.48 '
12.48
12.48
12.48
12.48
12.48
12.48
12.48
12.48
12.48
12.31
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
11.71
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11,53
10.93
10.83
11.04
11.04
10.72
10.83
10.86
10.89
10.78
10.68
10.68
10.68
10.68
10.78
11.93
13.30
13.32
13.05
13.47
13.37
12.59
11.62
11.62
10.68
10.57
10.47
10.57
10.57
10.47
10.57
10.57
10.68
10.68
10.68
10.78
10.68
10.68
10.78
10.68
10.78
10.68
10.68
10.68
10.78
10.78
10.57
10.68
10.78
10.89
1.05
1.04
1.06
1.06
1.03
1.04
1.04
1.04
1.03
1.02
1.02
1.02
1.02
1.03
1.14
1.27
1.27
1.24
1.28
1.27
1.21
1.11
1.11
1.02
1,01
1.00
1.01
1.01
1.00
1.01
1.01
1.02
1.02
1.02
1.03
1.02
1.02
1.03
1.02
1.03
1.02
1.02
1.02
1.03
1.03
1.01
1.02
1.03
1.04
86
86
86
86 '
86
86
87
88
88
88
88
88
88
88
88
88
89
90
90
90
89
88
'88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
ICal APPENDIX F
-------
9:44
9:45
9;46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:33
10:34
10:35
9.49
10.26
11.21
11.93
14,11
14.84
11.00
9.88
10.23
9.84
11.08
11.54
11.86
10.80
11.39
11.05
10.93
10.99
10.96
11.80
9.61
9.62
10.62
10.73
13.38
13.66
11.42
9.95
9.99
9.69
10.53
11.74
11,79
11.03
11.88
12.19
11.93
12.06
11.91 '
12.54
10.72
10.43
11.14
11.33
14.55
14.81
14.02
9.26
9.78
9.94
10.61
11.78
23.98
24.40
23.98
16.10
17.94
19.18
19.39
20.65
22.57
19.96
17.96
18.14
18.79
16.82
17.89
17.97
18.03
17.60
1B.54
18.31
21 .34 .
24.76
23.77
16.63
17.03
17.65
17.47
20.29
20.83
20.53
17.66
18.91
19.00
17.65
19.53
20.08
20.80
19.39
20.86
21.13
24.46
29.11
30.28
21.91
19.06
19.78
19.90
18.61
20,98
22.99
18.20
18.90
11.53
11.25
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
11.09
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.45
11.53
11.53
11.52
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.83
11.93
11.93
11.93
11.92
11.93
11.93
11.93
11.93
11.93
11.93
10.89
10.89
10.78
10.89
10.89
10.89
10.89
10.89
10.89
10.78
10.68
10.68
10.78
10.78
10.78
10.68
10.47
10.68
10.68
10.68
10.57
10.57
10.57
10.68
10.68
10,78
10.89
10.89
10,89
10.89
10.99
11.10
10.99
10.99
11.10
11.10
11.10
10.99
10.99
10.99
10.89
10.47
10.47
10.57
10.47
10.57
10.57
10.78
10.99
11.10
11.20
11.41
1.04
1.04
1.03
1.04
1.04
1.04
1.04
1.04
1.04
1.03
1.02
1.02
1.03
1.03
1.03
1.02
1.00
1.02
1.02
1.02
1.01
1.01
1.01
1.02
1.02
1.03
1.04
1.04
1.04
1.04
1.05
1.06
1.05
1.05
1.06
1.06
1.06
1.05
1.05
1.05
1.04
1.00
1.00
1.01
1.00
1.01
1.01
1.03
1.05
1.06
1.07
1.09
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
TCal APPENDIX F
-------
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
Average
Minimum
Maximum
Run 10
M17
Results
Train A
Train B
Average
1 1 .96 20.38
1 1 .77 1 9.78
11.64 18.19
11.75 19.16
11.67 18.80
10.95 16.87
11.28 18.39
11.33 18.80
10.40 21.61
9.49 25.36
10.16 26.86
11.40 20.06
9.26 16.10
14.88 30.28
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
25.63
26.63
26.13
11.93
11.93
12.16
12.40
12.40
12.40
12.40
12.40
12.40
12,40
12.40
12.40
12.40
12.40
12.40
12.08
11.12
11.12
11.13
11.13
11.13
11.12
11.13
11.13
11.13
11.13
11.13
11.13
11.13
11.74
10.97
12.48
F904K
For F904K
&RSD
mg/dscrn
38.6
40.4
39.5
11.20
11.20
11.31
11.10
10.74
10.41
10.72
10.93
10.93
10.83
10.93
10.95
10.41
13.47
Moisture
1.07
1.07
1.08
1.06
1.03
1.00
1,03
1.05
1.05
1.04
1.05
1.05
1.00
1.28
Moisture
%
12.8
13.2
13
88
88
88
88
87
86
86
86
86
86
86
87.84
86.00
90.00
Temp
190
iCal APPENDIX F
-------
Correlation Testing - Run 11: Medium-High PM concentration - 2nd correlation test run
7/15/99 ESCP5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc degC
11:47
11:48
11:49
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
11.34
10.90
11.26
11.58
10.92
10.29
10.19
10.41
11.58
13.27
14,05
11.18
9.85
10.11
10.14
10.68
11.09
11.75
10.44
11.42
11.31
11.87
11.43
11.56
12.31
11.11
10.30
10.56
10.42
14.14
15.41
15.14
10.69
10.82
11.74
11.78
11.86
13.02
12,98
12.50
12.97
13.22
12.30
12.12
13.02
12.53
10.47
11,10
12.31
18.90
17.23
18.06
18.71
10.33
24,52
26.05
25.48
17.23
17.57
18.33
18.55
20.74
21.52
20.08
17,55
17,45
18.35
16.08
17.82
19.39
19,69
19.00
19.72
20,29
22.12
29.59
29.98
26.71
18.76
20.83
22.90
23.02
25.09
27.16
21.85
20.80
21.79
21.88
19.27
21.43
22.33
20.08
20.77
22.15
24.64
30.52
33.31
31.93
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.25
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10,97
10.97
10.97
12.58
13.12
13.12
13.12
13.13
13.12
13.12
13.12
13.12
13.12
13.12
13.12
10.83
10.52
10.62
10.72
10.83
10.83
10.83
10.93
10.83
10.72
10.83
10.83
10.72
10.72
10.62
10.72
10.83
10.83
10.72
10.83
10,83
11.14
10.83
11.04
10.83
10.83
10.72
10.83
10.83
10.93
11,14
11.14
11.14
11.24
11.24
11.14
10.93
10.93
10.83
10.93
10.93
10.83
10.62
10.72
10.72
10.83
10.83
10.93
11.04
1.04
1.01
1.02
1.03
1.04
1.04
1.04
1.05
1.04
1.03
1.04
1.04
1.03
1.03
1.02
1.03
1.04
1.04
1.03
1.04
1.04
1.07
1.04
1.06
1.04
1.04
1.03
1:04
1.04
1.05
1,07
1.07
1.07
1.08
1.08
1.07
1.05
1.05
1,04
1.05
1.05
1.04
1.02
1.03
1.03
1.04
1.04
1.05
1.06
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
" 86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
ICal APPENDIX F
-------
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15'
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13.25
15.81
16.92
11.88
11,00
11.19
12.05
12,04
12.07
12.58
11.39
11.96
12.30
11.41
12.27
12.25
12.36
9.96 '
10.60
9.88
11.26
13.25
13.28
11.78
9.18
9.54
9.83
11.37
11.71
12.62
10.69
10.43
11.86
12.32
12.11
12.08
12.02
11.94
11.76
9.92
10.80
11.01
12.46
14.89
14.73
11.10
10.33
10.71
11.28
11.29
11.75
12.17
19.06
22.21
22.72
22.03
25.15
25.30
22.90
20.53
20,44
20.11
18.55
19.63
21.01
19.27
20.05
20.77
21.28
26.17
28.69
27.52
16.24
17.23
18.21
17.17
19.27
20.35
18.52
18.55
19.38
20.44
18.01
17.33
19.30
21.10
22.12
18.91
20.95
20.38
22.06
27.46
28.87
29.41
17.59
20.02
20.29
19.69
21.40
24.10
20.14
18.63
18.76
19.87
13.12
12.93
12.72
12.72
12.72
12.72
12.73
12.72
12.72
12.72
12.72
12.73
12.72
12.72
12.56
12.08
12.08
12.08
12.08
12.08
12.08
12.08
12.08
12.08
12.08
12.08
12.08
11.88
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.28
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
10.93
11.07
10,99
10.89
10.89
10,89
10.89
10.89
10,98
10.93
10,83
10.93
11.04
10.83
10.93
10.93
10.62
10.52
10.31
10.20
10.10
9.99
10.20
10.41
10.93
11.45
11.51
12.01
12.01
11.91
11.70
11.60
11.70
11.60
11.49
11.18
11.18
11.18
10.97
10.87
10.87
10.87
10.87
10.89
11.14
11.04
11.04
10.93
10.93
10.83
11.04
11.24
1.05
1.06
1.05
1.04
1.04
1.04
1.04
1.04
1.05
1.05
1.04
1.05
1.06
1.04
1.05
1.05
1.02
1.01
0.99
0.98
0.97
0,96
0.98
1.00
1,05
1.10
1.11
1.16
1.16
1.15
1,13
1.12
1.13
1.12
1.11
1.08
1.08
1.08
1.05
1.05
1.05
1.05
1.05
- 1.05
1.07
1.06
1.06
1.05
1.05
1.04
1.06
1.08
86
87
88
88
88
88
88
88
88
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
85
86
86
86
86
86
86
86
86
ICal APPENDIX F
-------
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
Average
Minimum
Maximum
Run 11
M17
Results
Train A
Train B
Average
11.31 18.06
1 2.48 1 9.57
1 2.48 20.98
12.03 20.20
12.49 21.01
12.53 21.61
13.03 22.27
9.98 28.66
10.36 33.01
10.78 32.08
12.00 21.94
11,76 21.62
9.18 15.08
16.92 33.31
ESC P5B DR 300-40
For P5B &
300-40
mg/acrn
28.22
27.29
27.755
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.81
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
12.25
11.71
10.25
13.13
F904K
For F904K
&RSD
mg/dscm
42.4
41.2
41.8
11.24
11.45
11.45
1 1 .24
11.35
11.45
11.39
11.18
11.08
10.97
10.77
10.96
9.99
12.01
Moisture
1.08
1.10
1.10
1.08
1.09
1.10
1.10
1.08
1.07
1.06
1.04
1.05
0.96
1.16
Moisture
%•
12.7
13
12.85
86
86
86
86
86
86
84
84
84
84
84
85.74
84.00
88.00
Temp
186
ICaJ APPENDIX F
-------
Correlation Testing - Run 12: High PM concentration - 3rd correlation test run
7/15/99 ESCP5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
14:39
14:40
• 14:41
14:42
14:43
14:44
14:45
14:46
14:47
14:48
14:49
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:59
15:00
15:01
15:02
15:03
15:04
15:05
15:06
15:07
15:08
15:09
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
15:22
15:23
15:24
15:25
15:26
15:27
12.61
12.89
12.54
13,15
13.61
12.22
11.30
11.67
12,12
14,86
16.48
16.73
10.35
11.07
11.03
12.06
12.41
12.97
12.82
12.52
13.39
13.50
13.37
12.98
13.85
12.62
10.98
11.42
11.98
14,26
16.57
16.80
12,26
11.05
11.18
11.45
12.70
13.22
13.93
12.69
13.75
13.39
' 13.46
13.19
14.13
14.46
11.47
11.94
12.49
20.65
22.15
19.93
21.13
23.05
26.41
33.37
32.89
30.88
21.04
23.29
22.87
23.23
25.72
26.65
22.90
21.49
22,39
23.14
19.24
21.94
22.87
22.09
22.84
24.10
25.45
32.89
35.83
32.80
19.66
23.65
24.85
23.71
26.41
27.67
25,60
23.05
23.65
23.47
22,27
23.14
23.95
22.99 .
22.36
25.78
26.26
33.22
37.84
36.85
13.76
13.76
13.76
13,76
13.76
13.76
13.76
13.76
.13.76
13.76
13.76
13.76
13.52
12.80
12.80
12.80
12.80
12.80
12,80
12.81
12.80
12.80
12.80
12.80
12.80
12.80
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
12.56
10.78
10.89
10.75
10.83
10.93
11,04
11.04
11.14
11.14
11.04
11,04
11.14
11.14
11.24
11.24
11.24
11.28
11.28
11.28
11.28
11.28
11.28
10.97
11.08
11.18
11.08
11,08
11.08
11.08
11.08
11.08
11.18
11.18
11.28
11.18
11.18
11,28
11.28
11,28
11.18
11.28
11,18
10,87
11.08
11.08
11.18
11.18
11.08
11,14
1.03
1.04
1.03
1.04
1.05
1.06
1.06
1.07
1.07
1.06
1.06
1.07
1.07
1.08
1.08
1.08
1.09
1.09
1.09
1,09
1.09
1,09
1.06
1,07
1.08
1.07
1.07
1,07
1.07
1.07
1.07
1.08
1.08
1.09
1.08
1.08
1,09
1.09
1.09
1.08
1.09
1.08
1.05
1,07
1.07
1.08
1.08
1.07
1.07
88
88
87
86
86
86
86
86
86
86
86
86
86
86
86
86
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
86
ICal APPENDIX F
-------
15:28
1559
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51-
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
15:15
15:16
16:17
16:18
16:19
13.80
16,67
17.69
14.74
11.71
12.14
12.99
13,23
14.34
14.77
14.32
14.87
15.05
15.54
14.32
15.13
15.81
13.34
13.24
13.85
13.79
17.30
18.16
17.62
11.97
12.35
13.02
12.93
14.10
15.43
15.00
15.51
16.20
16.58
14.72
16.37
16.29
13.78
13.22
14.00
14.11
16.52
18.39
19.50
11.85
11.82
12.74
12.74
14.02
14.66
14.81
14.31
24.64
24.79
26.20
26.98
29.05
30.16
30.52
25.51
2629
27.13
25.00 •
25.96
27,85
28.15
25.39
27,85
29.32
34.48
40.66
40.27
33.40
27.40
28.84
30.37 '
29.59
31.72
34.51
26.05
27.40
28.21
29.35
26.26
28.69
29.89
27.28
29.20
30.16
32.80
42.67
42,13
37.69
25.57
28.63
28.69
29.23
32.17
34.96
28.57
26.86
28.30
29.59
23.92
12,56
13.10
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.28
13.96
14.63
14.53
14.63
14.63
14.63
14.64
14.64
14.63
14.63
14.63
14.63
14.63
14.83
15.43
15.43
15.43
15.43
15.44
15.43
15.44
15.43
15.43
15.43
15.43
15.43
15.44
17.11
17.11
17.11
17.11
17.11
17,11
17.11
17.11
17.11
17.11
17.11
11.24
11.14
11.24
11.35
11.14
11.24
11.35
11.24
11.24
11.24
11.24
11.24
11.35
11.14
11.24
11.14
11.24
11.24
11.14
11.24
11,35
11.14
11,24
11.24
11,24
11.14
11.24
11.24
11.24
11.24
11.24
11.24
11.24
11.24
10.93
11.14
11.04
10.93
10.93
11.04
11.04
11.04
11.04
11.14
11.14
11.14
11.24
11.24
11.24
11.24
11.14
11.14
1.08
1.07
1.08
1.09
1.07
1.08
1.09
1.08
1.08
1.08
1.08
1.08
1.09
1.07
1.08
1.07
1.08
1.08
1.07
1,08
1.09
1.07
1.08
1.08
1.08
1,07
1.08
1.08
1.08
1.08
T.08
1.08
1.08
1,08
1.05
1.07
1.06
1.05
1.05
1,06
1.06
1.06
1.06
1.07
1.07
1.07
1.08
1.08
1.08
1.08
1.07
1.07
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
ICal APPENDIX F
-------
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
,16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
Average
Minimum
Maximum
Run 12
M17
Results
Train A
Train B
Average
14.99 26.65
14.75 27.70
14,42 24.94
14,85 27.52
14.40 29.20
14.46 30.52
11.81 38.02
13,21 38.50
13.15 38.98
1 5.28 22.48
17.55 26.56
13,88 ' 27,83
10.35 19.24
19.50 42.67
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
31.77
32.78
32.275
17.11
17.11
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
14.96
15.67
15.91
15.91
15.91
15.91
15.51
15.91
15.91
15.91
15,91
15.91
15,91
15,91
14,49
12.56
17.11
F904K
ForF9Q4K
&RSD
mg/dscm
48.6
50.5
49.55
11.14
11.14
10.83
11.04
11.14
11.14
11.04
11.04
11,04
11.14
11.04
11.15
10.75
11,35
Moisture
1.07
1.07
1.04
1.06
1.07
1.07
1.06
1.06
1.06
1.07
1.06
1.07
1.03
1.09
Moisture
%
14.1
14.8
14.45
86
86
86
86
86
86
86
86
86
86
86
85.47
84.00
88.00
Temp
186
ICd APPENDIX F
-------
Correlation Testing - Run 13; Medium PM concentration - 4th correlation test run
7/16/99 ESCP5B Durag 300-40 Durag F904K Moisture g/aem H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C_
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:15
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26 '
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
10.56
11.68
11.90
8.80
8.84
9.03
8.14
9.01
9.23
9.52
7.76
7.68
8.15
7.82
8.18
8.03
8.26
8.57
8.62
8.45
8.80
8.71
9.00
9.55
9.69
9,96
9.88
9.92
10.19
9.96
8.83
9.27
9.68
10.73
11.82
12.80
9.81
9.19
8.94
9.82
9.79
10.12
10.82
8.56
9.20
9.07
9.36
9.55
10.30
14.20
16,52
16.30
17.09
17.32
17.45
14.96
13.48
13.29
13.71
10.49
10.94
11.30
11.41
11.75
12.06
11.59
11.77
11.69
11.70
12.60
12.79
14.08
15.17
15.88
16.38 -
15.20
15.69
15.07
16.27
20.41
20.44
21.70
12.89
14.90
15.39
16.00
18.15
18.58
17.05
14.99
15.35
15.73
14.08
12.76
12.64
12.84
13.83
16.55
8.17
8,17
8.17
8.17
8.17
8.17
8.17
8.17
8,17
8.17
8.17
8.17
7.91
7.13
7.13
7.13
7.13
7.13
7.13
7,13
7.13
7.13
7.13
7.13
7.13
7.13
8.80
8,80
8.81
8.81
8.81
8.81
8.81
8.81
8.81
8.81
8.81
8.81
10.40
10.40
10.40
10.30
10.40
10.50
10.71
10.91
10.50
11.02
11.22
11.32
11.60
11.39
11.28
10.97
10.77
10.66
10.66
10.87
11.08
11,39
11.60
11.80
11.80
11.60
11.08
10.87
10.56
10.30
10,40
10.71
11,02
11.22
11.53
11.74
11.74
11.65
11.60
11.49
11.39
11.18
11.18
11.08
11.08
11.18
11.28
11.28
11.49
1.01
1.01
1.01
1.00
1.01
1.03
1.04
1.06
1.02
1.07
1.09
1,10
1.12
1.10
1.09
1.06
1.04
1.03
1.03
1.05
1.07
1.10
1.12
1.14
1.14
1.12
1.07
1:05
1.02
1.00
1,01
1.04
1.07
1.09
1.12
1.14
1.14
1.13
1.12
1.11
1.10
1.08
1.08
1.07
1.07
1.08
1.09
1.09
1.11
82
82
82
82
82
82
82
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
. 84
84
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
84
84
84
10
KM APPENDIX F
-------
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10;27
10:28
10:29
10:30
10:31
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10.47
10.44
9.94
9.96
10.61
9.48
9.34
10.06
9.62
12.42
12.62
12.53
8.90
9.61
8.96 .
9.00
9,95
10.12
9.47
9.23
9.42
9.44
9.09
9.32
9,42
8.67
8.48
8,75
8.94
10.79
11.29
11.38
8.07
8.57
8.62
8.12
8.88
9.31
8.94
8.40
8.78
8.95
9.38
9.46
9.39
9.56
9.31
9.36
9.44
10.74
12.32
12.66
16.46
16.49
15.57
16.39
16.75
19.81
23.74
23.83
17.77
15.69
17.44
17.98
17.20
19.29
19.78
14.09
15.42
15.48
14.66
14.22
14.13
13.94
13.93
14.55
14.57
15.58
19.51
19.28
17.20
12.78
13.50
14.16
14.69
15.89
16.79
13.29
12,18
12.58
14.03
11.26
13.03
13.39
13.12
13.73
14.62
15.55
17.44
20.71
20.23
14.51
15.30
15.67
8.81
9.29
9.45
9,45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.45
9.29
9.13
9.13
9.13
9.13
9.13
9.13
9.13
9.13
9.13
9.13
9.13
9.13
8.85
8,02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.41
8.41
8.41
8.41
8.41
8.41
8.41
B.41
8.41
8.41
8.41
11.60
11.39
11.49
11.58
11.53
11.53 .
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.43
11.53
11.63
11.74
11.63
11.84
11.84
11.74
11.32
11.43
11.32
11.32
11.22
11,22
11.22
11.22
11.22
11.24
11.18
10.97
10.77
10.59
10.62
10.62
10.44
10,57
10.68
10.78
10.78
10.68
10.78
10.78
10.68
10.68
10.78
10.78
10.89
11.10
1.12
1,10
1.11
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.12
1.11
1.12
1.13
1.14
1.13
1.15
1,15
1.14
1.10
1.11
1.10
1.10
1.09
1.09
1.09
1.09
1,09
1.09
1.08
1.06
1.04
1.02
1.02
1.02
1.00
1.01
1.02
1.03
1.03
1.02
1.03
1.03
1.02
1.02
1,03
1.03
1.04
1.06
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
83
84
84
84
85
86
86
87
88
88
88
88
88
88
88
88
88
88
88
88
88
ICal APPENDIX F
11
-------
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
11:07
11:08
11:09
11:10
11:11
11:12
11:13
11:14
Average
Minimum
Maximum
10.34
9.01
9.24
8.82
10.05
10.55
10.60
9.85
9.69
9.60
9.62
i.60
7.68
12.80
ESC PBB
18.73
18.40
19.42
17.35
15,60
15.34
15.96
13.75
14,62
14.40
14.58
15.45
10.49
23.83
DR 300-40
8.41
8.40
9.01
9,21
9.21 •
9.20
9.20
9.21
9.21
9.21
9.21
9.21
9.21
9.20
9.21
9.05
8.89
8.89
8.89
8.89
8.89
8.89
8.89
8.89
8,89
8.89
8.89
8.89
8.58
7,13
9,45
F904K
11.10
11.10
11.10
10.89
10.68
10.36
10.47
10.57
10.78
10.68
10.57
11.10
10.30
11.84
Moisture
1.06
1.06
1.06
1.04
1.02
0.99
1.00
1.01
1,03
1.02
1.01
1.07
Q-.99
1.15
88
88
88
88
88
88
88
88
88
88
88
84.07
82.00
88.00
Temp
Run 13
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
11.74
11.48
11.61
For F904K
&RSD
mg/dscm
17.4
17
17.2
Moisture
iTi
11.9
11.9
183
12
ICal APPENDIX F
-------
Correlation Testing - Run 14: Medium PWI concentration - 5fh correlation test run
7/16/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acrn H2O Temp,
Time raw mA raw ra mA raw mA % Vdc degC
12:12
12:13
12:14
12:15
12:16
12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:56
12:59
12:59
9.46
9.71
8.80
9.30
9.40
9.76
11.76
12.93
12.08
8.87
9.33
9.29
8.83
10.07
10.15
9.96
8.50
9.56
9.56
9.64
9.09
9.70
10.26
8.91
8.84
9.09
8.97
11.15
11.97
12.31
8.59
8.81
8.58
8.96
9.48
9.76
9.54
9.02
9.33
9.69
9.20
9.23
9.53
9.47
8.59
9.13
9.20
10.03
10.08
15.54
16.05
16.96
22.69
21.46
18.37
14.19
14.97
18.46
15.67
18.16
18.39
15.23
15.23
14.99
14.68
11.92
14.14
14.90
15.05
15.02
14.93
15.74
16.54
21.76
22.12
19.24
13.75
14.34
14.45
14.90
16.82
17.57
15.12
14.18
15.34
15.63
12.42
14.07
14.73
14.60
14.92
15.54
16.63
19.72
21.64
21.40
16.06
16.09
8.65
8.65
8.65
8,65
8.65
8.65
8,65
8.65
8.65
8.65
8.65
8.65
8.65
8.49
8.49
8,49
8.49
8.49
8.49
8.49
8.49
8.49
8.49
8.49
8.49
8.49
9.27
9.53
9.53
9.53
9.53
9.53
9.53
9.53
9.53
9.53
9.53
9.53
9.53
10.83
10.93
11.04
10.93
11.04
11.04
11.04
11.04
10.93
10.93
10.93
10.93
10.93
10.93
10.93
10.83
10.93
11.14
11.14
11.04
10.72
10.93
11.04
10.83
10.83
10.93
10.93
10.83
11.04
11.14
11.24
11.35
11.24
11.14
11.14
11.14
11.04
10.83
11.04
11,04
10.83
10.93
10.93
11.04
11.14
11.04
11.04
11.04
11.04
1.04
1.05
1.06
1.05
1.06
1.06
1.06
1.06
1.05
1.05
1.05
1.05
1.05
1.05
1.05
1.04
1.05
1.07
1.07
1.06
1.03
1.05
1.06
1.04
1.04
1.05
1.05
1.04
1.06
1.07
1.08
1.09
1.08
1.07
1.07
1.07
1.06
1.04
1.06
1.06
1.04
1,05
1.05
1.06
1.07
1.06
1.06
1.06
1.06
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
ICaS APPENDIX F
13
-------
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
1 3:41
1 3:42 •
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
12.25
12.48
9.97
9.32
9.23
8.83
9.66
9.67
10.06
8.80
8.64
8.74
9.86
10.25
10.40
10.17
10,25
10.21
9.95
9.31
9.24
10.20
10.84
13.03
12.88
11.93
9.40
9.34
9.05
10.14
10.36
11.38
9.74
10.04
10.39
10.04
10.36
10.31
10.33
9.29
9,75
9,43
10.69
13.15
13.97
12.94
9.54
9.69
9.35
10.19
10.47
11.16
15.88
15.76
19.12
17.79
18.16
16.45
15.15
15.12
15.72
13.09
12.22
12.54
15.07
16.21
16.56
16.02
16.73
17.08
18.40
23.89
25.03
24.22
14.33
16.23
17.35
19.66
19.54
19.58
17.47
15.66
16.06
16.90
15.13
16.09
16.29
15.57
17.16
17.46
18.55
22.45
25.60
25.96
15.77
16.90
17.22
18.10
20.11
19.90 '
19.30
16.17
16.16
16.60
9.53
8.51
8.17
8.17
8.17
8.17
8.17
8.17
8.17
8,17
8.17
8.17
8.17
8.17
8.05
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
7.93
8.89
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9,85
9.85
9.85
9.85
9.85
9,87
9,93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
11.04
11.04
10.93
10.83
10.93
10.83
10,83
10,93
11.04
10.93
10.93
10.93
11.04
11.04
11.04
10.72
10.83
10.93
10.93
10.83
10.85
10.99
10.89
10.78
10.78
10.68
10.78
10.78
10.68
10.78
10.89
10.89
10.78
10.99
10.99
10.68
10.68
10.78
10.68
10.68
10.57
10.78
10.81
10.84
10.84
10.84
10.84
10.84
10.74
10.84
10.84
10.84
1,06
1.06
1.05
1.04
1.05
, 1.04
1.04
1.05
1.06
1.05
1.05
1.05
1.06
1.06
1,06
1.03
1,04
1.05
1.05
1.04
1.04
1.05
1.04
1.03
1.03
1.02
1.03
1.03
1.02
1.03
• 1.04
1.04
1,03
1.05
1.05
1.02
1.02
1.03
1.02
1.02
1.01
1.03
1.03
1.03
1.03
1.03
1.03
1.03
1.02
1.03
1.03
1.03
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
86
85
86
86
87
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
88
89
90
90
90
90
90
90
90
90
90
14
ICal APPENDIX F
-------
13:52
13:53
13:54
13:55
13:56
13:57
13:58
13:59
14:00
14:01
14:02
14:03
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
14:14
14:15
14:16
14:17
14:18
14:19
Average
Minimum
Maximum
Run 14
M17
Results
Train A
Train B
Average
10.06 15.97
10.12 15.86
10.20 16.18
10.44 16,38
9.76 16.24
10.05 17.09
10.59 17,83
9.36 22,09
9.43 26.44
10.73 26.47
9.94 1 9.57
10.01 17.22
8.50 11.92
13.97 26.47
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
13.48
14.36
13,92
9.93
9.93
10.08
10.08
10.08
10.08
10.08
10.08
10.08
10.08
10.08
10.08
10,08
10.08
10.08
10.45
10.57
10.57
10,57
10.57
10.57
10.57
10.57
10.57
10-57
10.57
10.57
10.57
9.24
7.93
10.57
Fi04K
For F904K
&RSD
mg/dscm
20.4
21.8
21.1
10.84
10,95
11.05
10.84
10.84
10.80
10,89
10,92
10.84
10.74
10.74
10.92
10.57
11.35
Moisture
1.03
1.04
1.05
1.03
1.03
1.03
1.04
1.04
1.03
1.02
1.02
1.05
1.01
1.09
Moisture
%
13.1
13.4
13,25
90
90
90
90
90
89
88
89
90
90
90
87.09
86,00
90.00
Temp
189
ICal APPENDIX F
15
-------
Correlation Testing - Run 15: Medium PM concentration - 6th correlation test run
7/16/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw rnA raw ra mA raw mA % Vdc deg C
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
16:29
16:30
16:31
9.42
10.41
10.64
13,64
14.24
13.21
9.78
9.99
10,11
9.94
10.89
11.35
10.55
10,41
10.44
10.83
9.95
10.15
10.37
9.85
9.25
9.67
10.03
13,11
13,42
14.12
9.76
9.61
9.92
9.73
10,82
10.78
11.32
9.55
10.23
10.50
10.21
9.85
9.88
9.83
9.15
9.12
10.16
11.27
12.71
12.95
10.80
9.20
9.59
26.11
26.26
20.68
18.42
19.96
24.22
21.55
21.76
22.24
16.91
18.18
18.27
17.98
15.77
17.21
17.41
16.39
17.92
18.61
20.05
26.26
25.60
23.74
17.29
18.13
18.73
24.82
20.62
21.73
17.32
17.03
17.95
18.13
14.65
16.17
16.95
16.10
16.97
17.59
18.61
23.11
24,94
24.94
17.00
17.12
17.83
24.73
21.07
20.26
10,65
10.65
.10.65
10.65
10.65
10.65
10.65
10.65
10.65
10.65
10,65
10,65
10.65
9.59
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.37
9.49
' 9.51
9.60
9.60
9.60
9.60
9.60
9.60
9.60
9.61
9.60
9.60
9.60
11.28
11.18
11.18
11.08
11.08
11.18
11.18
11.18
11.18
11.08
11.18
11.18
11.18
11.28
11.49
11.49
11.18
11.39
11.28
11.39
11.28
11.43
11.22
11.22
11.32
11.22
11.28
11.28
11.28
11.08
11.28
11.28
11.39
11.39
11.60
11.60
11,49
11.60
11,49
11.49
11.38
11,49
11,49
11.48
11.32
11.32
11.43
11.32
11.46
1.09
1,08
1.08
1.07
1.07
1.08
1.08
1.08
1.08
1.07
1.08
1.08
1.08
1.09
1.11
1.11
1.08
1.10
1.09
1.10
1.09
1.11
1.09
1.09
1.10
1.09
1.09
1:09
1.09
1.07
1.09
1,09
1.10
1.10
1.12
1.12
1.11
1.12
1.11
1.11
1.10
1.11
1.11
1.11
1.10
1.10
1.11
1.10
1.11
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
83
16
ICal APPENDIX F
-------
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:04
17:05
17:06
17:07
17:08
17:09
17:10
17:11
17:12
17:13
17:14
17:15
17:16
17:17
17:18
17:19
17:20
17:21
17:22
17:23
9.24
10.44
10.63
10.66
10.63
10.07
10.12
10.19
10.50
9.92
10.39
9.08
9.33
9.42
11,30
12.19
12.83
11.48
9.58
9.31
9.38
9.58
10.08
10.62
10.13
9,57
10.04
10.48
9.54
10.64
10.21
9.37
10.23
10.09
10.46
12.46
13.09
14.97
9.17
9.96
9.55
9.03
. 9.94
10.61
10.43
9.49
10.49
10.30
9.71
9.64
10.37
9.60
18.67
17.71
17.20
17.37
15.86
16.19
16.62
16.02
16.58
17.30
17.98
21.76
25.36
24.88
19.12
16.65
18.10
21.85
19.93
19.96
18.91
15.77
16.41
17.19
15.21
15.74
16.28
16.75
14.87
17.09
17.81
20.71
24.19
25.75
21.91
16.28
17.36
47.02
18.22
20.02
20.02
15.74
16.13
16.65
16.25
14.83
16.34
16.57
15.20
16.45
17.04
18.77
9.78
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
10.33
9.29
9.29
9.29
9.29
9.29
9,29
9.30
9.29
9.29
9.30
9.29
9.29
9.29
9.71
9.85
9.85
9.85
9.85
9.85
9.85
9.85
9.85
• 9.85
9.85
9.85
9.85
10.37
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
11.18
11.28
11.18
11.18
11.18
11.18
11.39
11.28
11.28
11.39
11.39
11.39
11.49
11.39
11.49
11.49
11.49
11.60
11.43
11.53
11.43
11.56
11.60
11.60
11.49
11.39
11 .39
11.39
11.08
11.28
11.28
11.39
11.39
11.28
11.28
11.18
11.18
11.28
11.28
11.39
11.39
11.49
11.70
11.49
11.49
11.28
11.28
1128
11.08
11.28
11.39
11.39
1.08
1.09
1.08
1.08
1.08
1.08
1.10
1.09
1.09
1.10
1.10
1.10
1.11
1.10
1.11
1.11
1.11
1.12
1.11
1.12
1.11
1.12
1.12
1.12
1.11
1.10
1.10
1.10
1.07
1.09
1.09
1.10
1.10
1.09
1.09
1.08
1.08
1.09
1.09
1.10
1.10
1.11
1.13
1.11
1.11
1.09
1.09
1.09
1.07
1.09
1.10
1.10
84
84
84
84
84
84
84
84
84
84
'84
84
84
84
84
84
84
84
82
82
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
ICal APPENDIX F
17
-------
17:24
17:25
17:26
17:27
17:28
17:29
17:30
17:31
17:32
17:33
17:34
17:35
17:36
17:37
17:38
17:39
17:40
17:41
17:42
17:43
17:44
17:45
17:46
17:47
17:48
17:49
17:50
Average
Minimum
Maximum
9.21
9.44
10.91
12.79
13.23
13.90
12.10
9.91
9,74
9,32
10,28
10,54
9.03
14,97
ESC PSB
24.10
25.75
24.16
16.28
17.59
18.70
24.64
20.77
21.28
18.21
17.40
19.36
14.65
47.02
DR 300-40
10.88
10.48
9.29
9.29
9.29
9.29
9.29
9,30
9.29
9.29-
9,29
9.29
9.29
9.29
9.30
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
9.98
9.29
10.88
F904K
11.28
11.39
11.28
11.28
11.39
11,49
11.49
11.60
11.49
11.49
11.60
11.35
11.08
11.70
Moisture
1.09
1.10
1.09
1.09
1.10
1.11
1.11
1.12
1.11
1.11
1.12
1.10
1.07
1.13'
84
84
84
84
84
84
84
84
84
84
' 84
83.77
82.00
84,00
Temp
Run 15
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
14.88
14.05
14.465
For F904K
&RSD
mg/dscm
22.3
21,2
21.75
Moisture
_
13.2
13.1
183
18
ICal APPENDIX F
-------
Correlation Testing - Run 16: Low PM concentration • 7th correlation test run
7/17/99 ESCP5B Durag 300-40 Durag F9Q4K Moisture g/acm H20 Temp.
Time raw mA raw ra mA raw mA % Vdc deg_C
8:51
8:52
8:53
8:54
8:55
8:56
8:57
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
9:15
9:16
9:17
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
6.03
6,02
6.78
6.21
6.08
6.06
6.17
6.45
5.97
6.08
6.10
5.92
5.78
5.81
5.81
5.77
5.77
5.80
5.72
5.72
5.71
5.75
5.85
5.79
5.99
6.00
6.07
5.88
6,03
5.85
6.03
5.98
5.57
5.57
5.63
5.75
5.78
6.48
5.76
5.81
5.81
5.75
5.82
5.67
5.78
5.87
5.83
6.07
5.94
8.56
6.65
6.73
6.03
6.51
7.69
8.30
8.59
6.62
6.72
6,59
6.56
6.04
6.04
6.17
6.24
6.15
6.15
6.43
6.96
7.07
6.57
5.80
5.47
5.67
7.06
7.13
7.27
6.91
6.25
6.23
6.88
5.37
5.41
5.43
5.95
6.03
6.87
6.11
6.00
6.07
7.00
7.46
7.19
6.85
5.53
5.60
5.76
6.93
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
4.50
4.50
4.50
4.50
4.50
4.50
4.50
4.50
4.50
4,50
4.50
4.50
4.50
4.86
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
14,10
14.10
13.69
14.41
14.31
13.49
12.05
11,94
11.12
11.32
11.43
11.43
11.63
11.74
11.80
11.39
11.58
11,53
11.63
11.63
11,53
11.74
11.63
11.63
11.63
11.63
11.63
11.63
11.53
11,63
11,53
11.48
11.60
11.49
11.49
11.70
11.80
11.80
11.49
11.70
11.60
11.60
11.39
11.53
11.53
11.53
11.43
11.53
11.53
1.37
1.37
1.33
1.40
1.39
1.31
1.17
1.16
1.08
1.10
1.11
1.11
1.13
1.14
1,14
1.10
1.12
1.12
1.13
1.13
1.12
1.14
1,13
1.13
1.13
1.13
1.13
1,13
1,12
1,13
1.12
1.11
1.12
1.11
1.11
1.13
1.14
1.14
1.11
1.13
1.12
1,12
1.10
1.12
1.12
1.12
1.11
1.12
1.12
82
82
82
82 '
82
82
82
82
82
82
82
82
82
82
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
ICal APPENDIX F
19
-------
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53 .
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
6.08
6.00
5.71
5.93
5.97
6.17
5.58
5.74
5.76
5.81
5.70
5.72
5.79
5.87
5.65
5.75
5.87
5.80
6.05
5.96
5.82
5.95
5.75
5.70
5.91
5.89
5.79
5.60
5.56
5.56
5.64
5.61
5.85
6.10
5.88
5.89
5.83
5.82
5.79
5.72
5.74
5.79
5.85
5.90
5.97
6.41
5.94
6.05
5.80
5.91
6.02
6.16
7.46
7.33
6.63
6.63
6.46
6.38
5.57
5.89
5.93
5.96
5.95
6.06
6.00
6.70
6.94
6.84
6.60'
5.42
5.71
6.43
6.66
7,13
7.63
6.02
6.34
6.18
6.07
5.40
5.33
5.36
5.42
5.45
6.01
6.64
6.21
6.55
6.12
6.24
6.82
7.18
7.29
7.29
5.60
5.66
5.84
7.B4
- 7.46
7,80
7.10
6.63
6.36
6.83
4.94
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.78
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
4.42
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.17
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
4.97
11.69
11.60
11.60
11.70
11.60
11.50
11.49
11.60
11.60
11.39
11.39
11.60
11.50
11.70
11.70
11.70
11:55
11.74
11.74
11.84
11.84
11.74
11.53
11.74
11.74
11.63
11.53
11.53
11.53
11.60
11.60
11.49
11.49
11.60
11.60
11.39
11.50
11.60
11.70
11.70
11.80
11.59
11.84
11.63
11.63
11.63
11.63
11.67
11.60
11.60
11.60
11.49
1.13
1.12
1.12
1,13
1,12
1.12
1.11
1.12
1.12
1.10
1.10
1.12
1.12
1,13
1.13
1.13
1.13
1.14
1.14
1.15
1.15
1.14
1.12
1.14
1.14
1.13
1.12
1.12
1.12
1.12
1:12
1.11
1.11
1.12
1.12
1.10
1,12
1.12
1.13
1.13
1.14
1.13
1.15
1.13
1.13
1.13
1.13
1.13
1.12
1.12
1.12
1.11
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
83
84
84
84
84
20
ICal APPENDIX F
-------
10:32
10:33
10:34
10:35
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
Average
Minimum
Maximum
Run 16
M17
Results
Train A
Train B
Average
5.58 5.47
5,57 5.57
5.62 5.47
5.70 5.55
5.58 5.54
5.70 5.69
5.81 5.19
5.79 6.18
5.92 6.70
5.81 6.24
5.88 6.34
6.21 6.56
5.87 6,42
5.56 5.33
6.78 8.59
ESC P5B DR 300-40
For P5B &
300-40
rng/acm
3.03
3.02
3.025
4.97
5.01
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.04
4.42
5.77
F904K
For F904K
&RSD
mg/dscm
4.6
4,6
4.6
11.49
11.39
11.39
11.49
11.39
11.39
11,60
11.60
11.39
11,49
11,63
11.32
11.72
11.12
14.41
Moisture
1.11
1.10
1.10
1.11
1.10
1.10
1.12
1.12
1.10
1.11
1.13
1.10
1.14
1,08
1.40
Moisture
%
13.3
13.4
13.35
84
84
84
84
84
84
84
84
84
84
82
82
83.04
82.00
84.00
Temp
181
ICal APPENDIX F
21
-------
Correlation Testing - Run 17: Low PM concentration - 8th correlation test run
7/17/99 ESCP5B Durag 300-40 Durag F9Q4K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
5.83
5.58
5.44
5.43
5.43
5.55
5.65
5.64
5.59
5.60
5.64
5.67
5.58
5.66
5.68
5.59
5.72
5.79
6.05
5.89
5.90
6.03
5,75 :
5.80
5.87
5.56
5.45
5.45
5.53
5.45
5.49
5.49
5.51
5.62
5.81
5.81
6.45
5.96
5.80
5.85
5.64
- 6.39
5.73
5.91
5.94
5.96
6.16
5.86
5.91
6.09
5.56
5.27
5.28
5.25
5.55
6.13
5.88
6.16
5.95
5.90
5,98
6.80
7.07
6.99
5.94
5.39
5.46
6.29
7.07
7.21
7.84
6.44
6.19
6.14
6.24
5.29
5.32
5.37
- 5.43
5.44
5.50
5.45
5.83
6.17
6.35
6.72
6.82
6.41
7.03
7.49
7.65
7.44
6.33
5.65
5.78
7.51
7.22
7.50
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.90
4.78
4.66
4.66
4.66
4.66
' 4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.66
4.68
4.74
4.74
4.74
4.74
4.74
4,74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
11.18
11.28
11.39
11.28
11.28
11.49
11.60
11.70
11.49
11.65
11.53
11.53
11.22
11.12
11.12
11.12
11.12
11.12
11.18
11.18
11.28
11.28
11.49
11.39
11.39
11.39
1139
11.39
11.39
11.28
11.28
11.28
11.18
11.39
11,60
11.60
11.28
11.39
11.39
11.39
11.28
11.39
11.28
11.08
10.87
10.66
10.77
10.87
11.08
1.08
1.09
1.10
1.09
1.09
1.11
1.12
1.13
1.11
1.13
1.12
1.12
1.09
1.08
1.08
1.08
1.08
1.08
1.08
1.08
1.09
1.09
1.11
1.10
1.10
1.10
1.10
1.10
1.10
1.09
1.09
1.09
1.08
1.10
1.12
1:12
1.09
1.10
1.10
1.10
1.09
1.10
1.09
1.07
1.05
1.03
1.04
1.05
1.07
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
22
ICal APPENDIX F
-------
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
13:58
13:59
14:00
14:01
14:02
14:03
5.76
5.80
5,77
5,99
5.81
5.50
5.50
5.47
5.57
5.67
5,79
5.78
5.68
5.80
5.82
6,41
5.73
5.87
6,74
5.85
5.78
6.72
5.95
5,95
5.86
5.78
5.92
5.86
5.65
5,52
.5.54
5.64
5.70
5.95
5.74
5.69
5.71
5.57
5.71
5.77
5.87
5.90
5.91
6.18
6.11
5.92
5.85
5.76
5.97
6.06
5.95
5.72
7.47
6.25
6.22
7.18
5.74
5.37
5.39
5.43
5.62
6.10
6.24
6.27
6.21
6.39
6.47
7.53
7.55
7.58
7.13
5.65
5.80
7.01
7.44
7.73
8.48
6.35
6,41
6.35
6.25
5.56
5,59
5,89
6.05
7.10
6.17
6.14
6.27
7.90
7.35
7.36
6.71
5.75
5.92
7.48
7.82
7.69
7.63
6.58
6.95
6.90
6.84
6.12
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
4.90
• 4,90
4.90
4.90
4.90
4.90
4,90
4.90
4.90
4.90
4.90
4.90
4.90
5.38
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.54
5.34
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5.14
5,14
5.14
5.14
5.14
11.18
11.39
11.49
11.49
11.49
11.49
11.39
11.28
11.49
11.60
11.49
11.39
11.49
11.49
11.49
11.39
11.70
11.60
11.49
11.34
11.22
11.22
11.12
11.32
11.43
11.74
11.63
11.53
11,53
11.53
11.63
11.74
11.84
11.63
11,43
11.43
11.32
11.12
11.12
10.97
10.97
10.97
11.08
11.08
11.13
11.35
11.45 •
11.35
11.32
11.49
11.49
11.49
1.08
1.10
1.11
1.11
1.11
1.11
1.10
1,09
1.11
1.12
1.11
1.10
1.11
1.11
1.11
1.10
1.13
1.12
1.11
1.10
1.09
1.09
1.08
1.10
1.11
1.14
1.13
1.12
1.12
1.12
1.13
1.14
1.15
1,13
1.11
1.11
1.10
1.08
1.08
1.06
1.06
1.06
1.07
1.07
1.07
1.09
1.10
1.09
1.09
1.11
1.11
1,11
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
84
84
84
84
84
86
86
86
86
85
84
84
84
ICal APPENDIX F
23
-------
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
14:14
14:15
14:16
14:17
14:18
14:19
14:20
14:21
14:22
14:23
14:24
14:25
14:26
14:27
14:28
14:29
14:30
Average
Minimum
Maximum
5.76
5.84
5.71
5.73
5.76
5.66
5.62
5.64
5.75
5.84
5.78
5.43
6.74
ESC P5B
6.14
6.60
6.11
6.14
6.34
7.11
7.30
7.37
6.97
5.73
6.44
5.25
8.48
DR 300-40
5.30
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.77
5.78
5.77
5.77
5.77
5.77
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
5.09
4.66
5.78
F9Q4K
11.49
11.39
11.39
11.49
11.43
11.53
11.53
11.63
11.63
11.43
11.36
10.66
11.84
Moisture
1.11
1.10
1.10
1.11
1.11
1.12
1.12
1.13
1.13
1.11
1.10
1:03
1.15
84
84
84
84
82
82
82
82
82
82
83.47
82.00
86.00
Temp
Run 17
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
2.72
2.64
2.68
For F904K
&RSD
mg/dscm
4
4
4
Moisture
12J2
14.2
13.2
182
24
ICai APPENDIX F
-------
Correlation Testing - Run 18: Low PM concentration - 9th correlation test run
7/17/99 ESC P5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc . deg _C_
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27
16:28
5.88
5.88
6,04
6,25
6.04
6.03
6.19
6.07
6.12
6.55
5.76
5.88
5.91
6.45
5.90
5.87
5.97
5.77
5.76
5.88
5.99
5.92
6.38
6.38
6.01
6.08
5.87
5.99
6.05
6.18
6.09
5,97
6,05
6.47
5.93
5.99
6.01
6,49
5.83
5.91
6.09
5.95
6.09
6.48
6.04
6.28
5.96
5.83
6.10
5.95
6.08
6.12
8.59
8.33
8.49
8.50
7.33
7.11
7.44
6.32
6.63
6.63
6.87
6.71
6.83
7.52
8.21
8.38
8.10
6.87
6.19
7,51
8.61
8.13
8.27
8,20
7.15
7.20
7,36
6,80
6.77
6,78
6,94
6.79
6.87
7,16
9.86
8.77
8.71
7.50
6.10
6.36
8.21
8.17
8.61
9.23
7.05
7.42
5.45
5.45 '
5.45
5.45
" 5.45
5.45
5.45
5.45
5.45
! 5.45
5.45
5.45
5.33
4.97
4.98
4.97
4.97
4.97
4.97
4.97
4.98
4.98
4.98
4.98
4.97
4.98
5.45
5.45
5,45
5,45
5.45
5.45
5.45
5.45
5.45
5.45
5.45
5,45
11.32
11.32
11.32
11,22 '
11.24
11.28
11.08
11.18
11.18
11.18
11.18
11.28
11.39
11.28
11.39
11.49
11.39
11.39
11.39
11.60
11.49
11.49
11.32
11.32
11.22
11.32
11.28
11.28
11.28
11.28
11.28
11.28
11.39
11.28
11.08
11.18
11.39
11.39
11.60
11.60
11.49
11.39
11.39
11.49
11.28
11.49
11.18
11.28
11.18
• 1.10
1.10
1.10
1.09
1.09
1.09
1.07
1.08
1.08
1.08
1.08
1.09
1.10
1.09
1.10
1.11
1.10
1.10
1.10
1.12
1.11
1.11
1.10
1.10
1.09
1.10
1.09
1.09
1.09
1.09
1.09
1.09
1.10
1.09
1.07
1.08
1.10
1.10
1.12
1.12
1.11
1.10
1.10
1.11
1.09
1.11
1.08
1.09
1.08
82
82
82
82
83
84
84
84
84
84
• 84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
ICal APPENDIX F
25
-------
16:28
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:03
17:04
17:04
17:05
17:06
17:07
17:08
17:09
17:10
17:11
17:12
17:13
17:14
17:15
17:16
17:17
17:18
6,20
6.10
5,95
6,50
6.13
5.86
5.78
5.92
6.28
5.71
5.75
6.06
5.91
5.88
6.59
5.98
5.96
6.00
5.84
5.95
5.95
5.94
5.83
5.83
5.88
5.83
5.81
5,71
6.41
5.81
5.74
6.31
5.88
6.46
5.96
6.88
5.92
5.83
5.96
5.99
5.67
5.81
5.88
5.86
5,71
5.81
5.86
5.77 '
5.76
5,76
6.26
5.68
7,28
7.00
6,72
7.99
6.92
6.62
6.81
6.88
7.69
8.58
8.44
7.90
6.16
6.13
7.47
7.55
8.10
8,12
8.80
7.08
7.02
6.96
6.36
6.49
6.55
6.53
6.48
6.60
7.39
8.20
8.04
8.24
5.91
6.35
6.05
7.00
6.72
6.78
8.04
8.10
7.58
6.83
6.93
6.76
6.18
6.40
6.53
6.39
6.49
6,79
7.79
7.88
5.45
5,75
5.85
5.85
5,85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.85
5.34
4.82
4.82
4.82
4.82
4,82
4.82
4.82
4.82
4.82
4.82
4.82
4.82
4.88
5.05
5.05
5.05
5.06
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.05
5.11
5.30
5.30
5.30
5,30
5.30
5.30
5.30
5,30
5.30
11.18
11.18
11.18
11.18
11.28
10.97
11.18
11.28
11.28
11,28
11.39
11.49
11.39
11.49
11.49
11.39
11.49
11.49
11.36
11.43
11.48
11.49
11.49
11.39
11.39
11.08
11.18
11.18
11.18
11.08
11.18
11.28
11.18
11.28
11.28
11.28
11.28
11.28
11.39
11.49
11.18
11.39
11.39
11.39
11.49
11.60
11.60
11.39
11.39
11.28
11.18
10.97
1.08
1.08
1.08
1.08
1.09
1.06
1.08
1.09
1.09
1.09
1.10
1.11
1.10
1.11
1.11
1.10
1.11
1.11
1.10
1.11
1.11
1.11
1.11
1.10
1.10
1.07
1.08
1.08
1.08
1.07
1.08
1,09
1,08
1.09
1,09
1.09
1.09
1,09
1,10
1.11
1.08
1,10
1,10
1.10
1.11
1,12
1,12
1.10
1.10
1.09
1.08
1.06
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
26
ICal APPENDIX F
-------
17:19
17:20
17:21
17:22
17:23
17:24
17:25
17:26
17:27
17:28
17:29
17:30
17:31
17:32
17:33
17:34
17:35
17:36
17:37
17:38
17:39
17:40
17:41
17:42
17:43
17:44
17:45
17:46
17:47
17:48
Average
Minimum
Maximum
Run 18
M17
Results
Train A
Train B
Average
5.6fi 8,00
6.07 7.96
5.76 6.00
5.84 5,95
5.80 6.01
6.89 7.61
5.99 7,83
6.02 8.22
5.72 7.59
5.80 6.80
5.91 7.03
5.97 6.83
6.00 7.28
5.67 5.91
6.89 9.86
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
3,27
3,12
3.195
5.30
5.30
5.30
5.30
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
4.74
5.16
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.30
5.21
4.74
5.85
F904K
For F904K
&RSD
mg/dscm
4.9
4.7
4.8
11.08
11.08
11.18
11.28
11.39
11.49
11.49
11.70
11.49
11.49
11.43
11.63
11.33
10.97
11.70
Moisture
1.07
1.07
1.08
1.09
1.10
1.11
1.11
1.13
1.11
1.11
1.11
1.13
1.10
1.06
1.13
Moisture
%
12.7
14
13.35
84
84
84
84
84
84
84
84
84
84
82
82
83.79
82.00
84,00
Temp
183
ICal APPENDIX F
27
-------
Correlation Testing - Run 19; Mid PM concentration - 10th correlation test run
7/18/99 ESCP5B Durag 300-40 Durag F9Q4K Moisture g/acm H2O Temp,
Time raw mA raw ra mA raw mA % Vdc deg C
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:56
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10.25
10.49
10,16
10,62
11,00
10.96
11.45
12.23 •
12.51
12.54
12.58
12.37
12.72
12.17
12.06
11.48
11.17
11.71
15.34
16.33
15.54
10.92
10.91
12.22
11.44
12.54
12,99 .
11.40
10.51
10,37
10.63
10.89
11.23
12.09
11.92
11.52
11.53
11.70
11.79
10.59
10.77
11.34
12.19
15.31
16.16
14.10
10.81
11.01
10.90
15.15
15.43
16.14
16.86
16.76
16.35
16.98
17.50
22.48
22.33
22.33
21.22
21.82
22.57
25.84
29.86
28.57
22.75
19.66
20.23
23.20
22,63
25.84
26.71
18.16
19.01
19.18
18.85
15.85
16.58
16.31
16.30
18.52
21.01
21.61
20.35
20.59
20.44
21.64
25.69
28.78
27.76
18.11
20.17
20.68
23.11
23.74
25.12
23.47
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
9.93
10.77
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
10.41
9.77
9.77
9.77
9.77
9.77
9.77
9.77
9.77
9.77
9.77
9.77
9.77
10,07
11.74
11.77
11.80
11.70
11.70
11.60
11.60
11.60
11.70
11.70
11.39
11.49
11.60
11.70
11.70
11.70
11.84
11.74
11.63
11.63
11.74
11,53
11.63
11.63
11.53
11.56
11.70
11.80
11.91
11.91
11,91
11.91
11.91
11.91
11.91
11.70
11.76
11.84
11.84
11.63
11.63
11.63
11.53
11.53
11,63
11.63
11.80 .
11.80
11.80
1.14
1.14
1,14
1.13
1.13
1.12
1.12
1.12
1.13
1.13
1.10
1.11
1.12
1.13
1.13
1.13
1.15
1.14
1.13
1.13
1.14
1.12
1.13
1.13
1.12
1.12
1.13
1.14
1.15
1.15
1.15
1.15
1.15
1.15
1.15
1.13
1.14
1.15
1.15
1.13
1.13
1.13
1.12
1.12
1.13
1.13
1.14
1.14
1.14
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
84
84
84
28
ICa] APPENDIX F
-------
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:32
10:34
10:35
10:36
10:36
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
11:07
11:08
11.40
12.18
12.93
11.88
10.09
10.27
10.30
10,33
10.27
10.48
10.86
10.93
11.03
12.20
12.20
12.31
12.36
12.23
12.38
12.15
11.12
12.56
12.48
13.76
16.55
18.02
13.89
11.33
11.11
10.72
12.32
12.59
12.77
11.24
10.29
10.90
11.41
11.70
12.22
12.19
11.85
12.38
12.09
11.32
11,70
11.78
13.33
16.83
17.42
12.89
11.33
11.94
18.94
19.25
19.93
18.43
15.74
15.47
15.16
16.21
16.61
16.80
16.98
17.18
17.80
21.94
22.00
22.33
22.15
23.08
23.11
23.89
29.95
31.24
33.40
20.35
20.83
22.51
25.06
25.93
25.18
24.01
20.02
19.42
18.94
16.65
15.48
15.75
18.25
20.53
20.50
19.57
21,04
21.28
23.05
27.37
29.41
28.96
18.01
19.84
21.49
22.33
26.47
26.14
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.79
10.25
10.25
10.25
10.25
10.25
10.25
10,25
10.25
10.25
10.25
10.25
10.25
10.25
10.43
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97
10.97.
10.97
10.97
10.97
10.08
10.08
10.08
10.09
10.08
10.08
10.08
10.08
10.08
10.08
10.08
10.08
11.80
11.91
11,80
11.70
11.60
11,70
11.67
11.74
11.84
11.74
11.74
11.74
11.94
12.15
12.18
12.18
11.94
11.84
11.84
11.84
11.70
11.70
11.60
11.70
11.60
11.70
11.60
11.70
11.70
11.70
11.80
11.80
11.91
11.76
11.74
11.74
11.53
11.74
11.74
11.53
11.43
11.63
11.53
11.63
11.65
11.70
11.70
11.60
11.60
11.60
11.70
11.60
1.14
1.15
1.14
1.13
1.12
1.13
1.13
1.14
1.15
1.14
1.14
1.14
1.16
1.18
1.18
1.18
1.16
1.15
1.15
1-15
1.13
1.13
1.12
1.13
1.12
1.13
1.12
1.13
1.13
1.13 .
1,14
1.14
1.15
1.14
1.14
1.14
1.12
1.14
1.14
1.12
1.11
1.13
1.12
1.13
1.13
1.13
1.13
1.12
1.12
1.12
1.13
1.12
84
84
84
84
84
84
83
82
82
82
82
82
82
82
83
83
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
ICal APPENDIX F
29
-------
11:09
11:10
11:11
11:12
11:13
11:14
11:15
11:16
11:17
11:18
11:19
11:20
11:21
11:22
11:23
11:24
11:25
11:26
11:27
11:28
11:29
11:30
11:31
11:32
• 11:33
11:34
11:35
Average
Minimum
Maximum
Run 19
M17
Results
Train A
Train B
Average
10.50 23.11
12.65 20,56
12.55 19.42
13.10 20.95
12.14 17.62
10.95 15.85
10.69 16.02
10.59 16.45
10.52 17.81
10.81 16.62 .
10.85 17,24
12.00 20.93
10.09 15.15
18.02 33.40
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
16.51
16.05
16.33
10.09
11.41
11.85
11.85
11.85
11.85
11.85
11.85
11.85
11.85
11.85
11.85
11.85
11.85
10.61
9.37
9.37
9.37
9.37
9.37
9.37
.9.37
9.37
9.37
9.37
9.37
9.37
10.48
9.37
11.85
F904K
For F904K
&RSD
mg/dscm
24.8
24
24.4
11.49
11.70
11.80
11.70
11,60
11.48
11.53
11.74
11.63
11.63
11.43
11.71
11.39
12.18
Moisture
1.11
1.13
1.14
1.13
1.12
1.11
1.12
1.14
1.13
1.13
1.11
1.13
1.10
1.18
Moisture
%
13.1
13.2
13.15
84
84
84
84
84
84
82
82
82
82
82
83.13
82.00
84.00
Temp
182
30
ICal APPENDIX F
-------
Correlation Testing - Run 20: Mid-Low PM concentration - 11th correlation test run
7/18/99 ESC P5B Durag 300-40 Durag F9G4K Moisture g/acm H2O Temp,
Time raw mA raw rs mA raw mA % Vdc deg C
12:59
13:00
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:26
13:26
13:27
13:28
13:29
13:30
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
9.79
9.57
9,45
9.85
9.47
8.96
9.80
9,57
11.04
12.68
13.16
10.90
9.88
10.45
10.72
10.15
10.79
11.22
9.39
10.00
10.06
10.14
9.92
10.15
9.94
8.86
9.07
9.32
9.91
12.17
12.69
13.83
9.16
9.62
9.79
9.71
10.41
10.91
9.80
9.97
10.22
10.32
9.91
10,51
10.58
9.75
9.65
10.32
9.46
15.37
14.55
15.46
15,82
17.65
21.43
23.32
24.16
15.02
16.36
16.86
20.26
21.25
21.94
19.36
17.07
16.95
17.44
15.66
15.93
16.38
15.95
16.84
16.88
17.08
20,86
24.76
24.40
17.56
14.90
17.03
18.82
18.04
19.87
20.59
15.22
16.08
16.84
16.25
15.76
16.43
16.96
16.38
16.97
17.34
19.96
24.88
23.47
22.18
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.55
8.65
8.B5
• 9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
9.05
8.97
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73-
8.73
11.80
11.60
11.91
11.91
12.01
11.91
11.80
11.80
11.60
11.70
11.70
11.60
11.70
11.80
11.80
11.91
11.91
12.01
11.80
11.91
11.91
11.63
11.63
11.94
11.94
11.94
11,84
11.84
11.84
11.84
11.74
11,63
11.63 •
11.77
11.70
11.80
11.80
11.80
11.70
11.80
11.91
11.91
11.39
11.70
11.80 •
11.80
11.91
11.91
11.91
1.14
1.12
1.15
1.15
1.16
1.15
1.14
1.14
1.12
1.13
1.13
1,12
1.13
1.14
1.14
1.15
1.15
1.16
1.14
1.15
1.15
1.13
1.13
1.16
1.16
1.16
1.15
1..15
1.15
1.15
1.14
1.13
1.13
1.14
1.13
1.14
1.14
1.14
1.13
1.14
1.15
1.15
1.10
1.13
1.14
1.14
1.15
1.15
1.15
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
ICal APPENDIX F
31
-------
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
13:58
13:59
14:00
14:01
14:02 .
14:03
14:04
14:05
14:06
14:07
14:08
14:09
14:10
14:11
14:12
14:13
14:14
14:15
14:16
14:17
14:18
14:19
14:20
14:21
14:22
14:23
14:24
14:25
14:26
14:27
14:28
14:29
14:30
14:31
14:32
14:33
14:34
14:35
14:36
14:37
14:38
14:39
11.66
11.99
13.05
9.25
9.62
9.13
9.41
10.42
11.10
11.57
9.70
10.43
8.78
8,40
8.21
8.47
8.47
8.04
7.81
8.36
8.38
9.71
10.23
9.59
8.13
8.29
8.59
8.02
8.56
8.67
8.23
8.01
8.27
8.35
7.82
8.38
8.40
8.24
8.11
8.13
9.30
8.87
10.28
9.87
9.44
8.21
7.99
7.78
8.27
8.59
8.70
7.50
15.31
16.50
17.78
17.92
20.32
20.35
16.13
16.13
16.71
18.54
14.13
16.97
12.63
12.53
12.34
12.59
12.83
15.22
17.70
17.45
13.56
11.60
12.28
12.93
15.24
15.56
15.79
11.61
12.11
12.20
12.66
11.15
11.81
11.94
11.67
12.08
12.81
13.34
16.72
17.84
17.29
10.90
12.56
12.89
15.91
15.27
15.82
13.88
11.93
11.91
12.42
9.55
8.73
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.81
8,89
8.89
8.89
8,90
8.89
8.90
8.89
8.89
8.89
8.89
8.89
8,89
8.17
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.23
6.57
6.57
6.57
6.57
6.57
6.58
6.57
6.57
6.57
6.57
6.57
11.80
11.70
11.80
11.80
11.80
11.91
11.80
11.91
11.80
11.80
11.91
12.01
12.01
11.50
11.70
11.80
11.91
12.01
11.91
11. BO
11.80
11.70
11.70
11.70
11.70
11.70
11.80
11.91
11.89
11.77
11.80
11.91
11.91
11.91
11.60
11.70
11.91
12.01
11.80
11.91
11.80
11.80
11.91
11.60
11.49
11.60
11.70
11.60
11.80
11.80
11.63
11.53
1.14
1.13
1.14
1.14
1.14
1.15
1.14
1.15
1.14
1.14
1.15
1.16
1.16
1.12
1.13
1.14
1.15
1.16
1.15
1.14
1.14
1.13
1.13
1.13
1^13
1.13
1.14
1.15
1.15
1.14
1.14
1.15
1.15
1.15
1.12
1.13
1.15
1.16
1.14
1.15
1.14
1.14
1.15
1.12
1.11
1.12
1.13
1.12
1,14
1.14
1.13
1.12
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
32
ICal APPENDIX F
-------
14:40
14:41
14:42
14:43
14:44
14:45
14:46
14:47
14:48
14:49
14:50
14:51
14:52
14:53
14:54
14:55
14:56
14:57
14:58
14:59
15:00
15:01
15:02
15:03
• 15:04
15:05
15:06
15:07
Average
Minimum
Maximum
Run 20
M17
Results
Train A
Train B
Average
7,48 9.63
7.52 9.49
7.91 10.61
8.35 11.54
8.19 11.74
8.15 11.40
8.14 11.23
7.89 11.72
7.97 12.18
7.55 13,56
7.70 14.17
9.45 15.80
7.48 9.49
13.83 24.88
ESC P5B DR 300-40
For P58 &
300-40
mg/acm
10.22
10.82
10.52
6.57
6.58
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.13
7.50
7.62
7.62
7.62
7.62
7.62
7.61
7.61
7.61
7.62
7.61
7.62
7.62
8.07
6.57
9.05
F904K
For F904K
&RSD
mg/dsem
15.6
16.6
16.1
11.74
11.63
11.74
11.89
11.91
11.70
11,70
11.60
11.49
11.49
11.39
11,78
11.39
12.01
Moisture
1.14
1.13
1.14
1,15
1.15
1.13
1.13
1.12
1.11
1.11
1,10
1.14
1,10
1.16
Moisture
%
15
15.5
15.25
82
82
82
84
84
84
84
84
84
84
84
83.68
82.00
84.00
Temp
183
ICal APPENDIX F
33
-------
Correlation Testing - Run 21: Mid-Low PM concentration - 12th correlation test run
7/18/99 ESCP5B Durag 300-40 Durag F904K Moisture g/acmH2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:25
16:26
16:27 •
16:28
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
15:42
16:43
16:44
16:45
16:46
16:47
16:48
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:04
17:05
17:06
8.46
8.40
8.66
9.12
9.80
10.65 •
10.73
9.04
8.93
8.52
8.24
8.00
9.16
10.22
8.31
8.76
8.62
8,80
8.63
9.00
8.66
8.28
8.47
8.80
9.36
10.38
10.66
9.28
8,26
8.08
7.93
8.59
8.82
9.03
8.37
7.45
7.73
8.55
8.86
8.84
8.56
8.64
8.93
10.17
8.17
8.46
8.45
8.90
10.65
15.06
18.85
18.43
17.95
11.30
12.21
13.06
16.39
16.76
16.60
13.56
12.78
13.07
14.71
11.91
12.70
12.92
12.21
13.35
13.52
13.98
16.61
17.69
17.89
12.20
12.28
12.80
15.46
16.87
16.14
14.64
12.57
12.51
12.97
11.09
10.39
10.38
11.94
13.05
13.64
12.54
13.57
13.78
15.75
17.30
18.45
18.66
13,01
12.16
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.65
8.63
8.57
8.57
8.57
8.57
8.57
8,57
8.57
8.57
8.57
8.57
8.57
8.57
8.57
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
12.01
11.91
12.01
12.11
12.22
12.11
12.22
12.08
12.05
12.15
12.05
12.05
11.94
11.74
11.84
11.94
11,91
11.80
11.80
11.70
11.91
11.70
11.80
11.91
11.80
11.91
11.91
12.01
12.01
12.01
11.91
12.01
11.91
11.91
11.96
11.94
11.94
12.08
12.32
12.22
11.91
12.01
11.91
11.80
11.80
11.91
11.91
11.91
12.01
1.16
1.15
1.16
1.17
1.18
1.17
1.18
1.17
1,17
1.18
1.17
1.17
1.16
1.14
1.15
1.16
1.15
1.14
1,14
1.13
1.15
1.13
1.14
1.15
1.14
1.15
1.15
1.16
1.16
1.16
1.15
1.16
1.15
1,15
1.16
1.16
1.16
1.17
1.19
1.18
1.15
1.16
1.15
1.14
1.14
1.15
1.15
1.15
1.16
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
.84
84
84
84
83
82
82
83
84
84
84
84
84
84
84
84
84
84
84
34
ICal APPENDIX F
-------
17:07
17:08
17:09
17:10
17:11
17:12
17:13
17:14
17:15
17:16
17:17
17:18
17:19
17:20
17:21
17:22
17:23
17:24
17:25
17:26
17:27
17:28
17:29
17:30
17:31
17:32
17:33
17:34
17:35
17:36
17:37
17:38
17:39
17:40
17:41
17:42
17:43
17:44
17:45
17:46
17:47
17:48
17:49
17:50
17:51
17:52
17:53
17:54
17:55
17:56
17:57
17:58
10.77
9.90
8.65
8.22
8.40
8.66
9.01
9.52
8.32
8.65
8.50
8.44
8.11
8.34
8.56
8.04
7.87
8.61
8.64
10.60
10.94
10.87
8.61
8.79
9.24
8.47
9.13
9,26
8.74
8.70
8.55
8.61
8.16
8.88
8.74
8.41
8,66
8.16
8,80
10.03
12.06
11.07
8.64
8.83
8.46
9.97
9.14
9.55
9.05
8.53
8.91
8.93
13.01
13.97
16.59
17.13
16.52
12.95
13.11
13.62
13.04
13.47
12.71
12.52
12.46
12.87
12.91
15.53
18,06
17.88
14,04
12,07
12.85
14.74
16.31
17.38
18.46
13.47
13.17
13.34
12.99
12.42
12.81
12.79
12.35
13.22
13.53
15.00
18.98
18.42
16.48
12.23
13.75
13.43
15.15
16.90
16.70
13.93
13.13
13.20
14.24
11.44
13.14
13.82
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
8.02
• 8.02
8.02
7.59
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7,45
7,45
7.45
7.45
7.45
7.81
8.17
8.17
8.18
8.17
8.17
8.17
8.17
8,17
8,17
8.17
8.17
8.17
8.07
7.77
7.77
7,77
7.78
7.77
7.77
7.77
7,77
7.77
7,77
7.77
7.77
11.91
11.91
11.91
11.80
11.70
11.80
11.80
11.70
11.70
11.70
11.91
11.70
11.91
12.01
12.11
12.00
11.84
11.84
11,84
11.63
11.65
11.70
11.60
11.80
11.80
11.80
11.91
12.01
12.01
12.01
12.11
12.01
11.60
11.91
11.89
11.84
11.74
11.74
11.84
11.74
11.84
11.74
11.74
11.77
11.80
11.70
11.80
11.80
11.70
11.80
11.91
12.01
1.15
1.15
1.15
1.14
1.13
1.14
1.14
1.13
1.13
1.13
1.15
1.13
1.15
1.16
1.17
1.16
1.15
1.15
1.15
1.13
1.13
1.13
1.12
1.14
1.14
1.14
1.15
1.16
1.16
1.16
1,17
1.16
1.12
1.15
1.15
1.15
1.14
1.14
1.15
1.14
1.15
1.14
1.14
1.14
1.14
1.13
1.14
1.14
1.13
1.14
1.15
1.16
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
ICal APPENDIX F
35
-------
17:59
18:00
18:01
18:02
18:03
18:04
18:05
18:06
18:07
18:08
1
8.79
9.00
8.97
9.16
8.43
8.24
8.81
8.68
10,30
10.56
13.08
13.48
13.97
15.29
16,96
18.24
17.90
12.78
12.25
13.25
7.77
7.77
7.77
7.77
7.77
7.77
7.77
7.77
7.77
7.77
7.77
7,77
7.77
7.77
11.70
11.91
11,91
11,70
11,60
11.60
11.60
11.70
11.76
11.94
1.13
1.15
1.15
1.13
1.12
1.12
1.12
1.13
1.14
1.16
84
84
84
84
84
84
84
84
83
82
Average
Minimum
Maximum
8.97
7.45
12.06
ESC P5B
14.32
10.38
18.98
DR 300-40
8.05
7.45
8.65
F904K
11.88
11.60
12.32
Moisture
1.15
1:12
1.19
83,53
82.00
84.00
Temp
182
Run 21
For P5B &
M17 300-40
Results mg/acm
Train A
Train B
Average
9.65
9.18
9.415
For F9Q4K
&RSD
mg/dscm
14.6
14
14.3
Moisture
%
13.9
14.2
14.05
36
ICal APPENDIX F
-------
Correlation Testing - Run 22; Mid-High PM concentration - 13th correlation test run
7/19/99 ESC P5B Durag 300-40 Durag F9G4K Moisture g/acm H2O Temp.
Time raw mA raw ra mA raw mA % Vdc deg C
8:58
8:59
9:00
9:01
9:02
9:03
9:04
9:05
9:06
9:07
9:08
9:09
9:10
9:11
9:12
9:13
9:14
,9:15
9:16
9:17
9:17
9:18
9:18
9:19
9:20
9:21
9:22
9:23
9:24
9:25
9:26
9:27
9:28
9:29
9:30
9:31
9:32
9:33
9:34
9:35
9:36
9:37
9:38
9:39
9:40
9:41
9:42
9:43
9:44
11.65
13.34
13.59
14.10
11.94
12,64
13.31
• 13.43
12.21
13.40
13.31
12.33
12,42
12.56
13.21
15.53
17,10
16.92
11.87
11.89
11.53
12.20
11.71
12.59
13.93
14.30
12.99
11.80
11.87
11.94
13,00
13.73
13.53
13.00
12.97
13.22
13.45
11.98
13.48
11.91
13.85
17.71
18.32
15.20
13.03
12.15
13.95
13.15
13.96
22.57
20.92
22.09
22.54
17.26
23.14
22.96
23.59
21.82
24.46
24.13
27.31
32.65
33.94
29.05
21.10
23.26
27.76
25.78
28.81
28.75
30.19
29.23
24.31
23.62
23.74
20.53
18.06
18.80
19.00
21.94
24.34
24.55
23.11
24.94
25.30
26.35
32.92
35.05
36.10
23.80
24.10
24.16
26.56
30.01
30.46
29.20
22.42
22.36
11,36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
10.21
9.93
9.93
9.93
9.93
9.93
9,93
9.93
9.93
9.93
11.22
11.43
11.46
11.39
11.49
11.60
11.70
11.70
11.60
11.70
11.60
11.60
11.60
11.67
11.63
11.74
11.84
11.84
11.84
11.84
11.84
11.63
11.53
11.63
11.63
11.63
11.74
11.74
11.63
1 1 .74
11.74
11.84
11.94
11.55
11.63
11.74
11.74
11.74
11.63
11.53
11.53
11.63
11.65
11.80
11.70
11.70
11.70
11.80
11.80
82
82
83
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
83
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
37
ICal APPENDIX F
-------
9:45
9:46
9:47
9:48
9:49
9:50
9:51
9:52
9:53
9:54
9:55
9:55
9:57
9:58
9:59
10:00
10:01
10:02
10:03
10:04
10:05
10:06
10:07
10:08
10:09
10:10
10:11
10:12
10:13
10:14
10:15
10:16
10:17
10:18
10:19
10:20
10:21
10:22
10:23
10:24
10:25
10:26
10:27
10:28
10:29
10:30
10:31
10:32
10:33
10:34
10:35
10:36
13.66
12.48
12.66
13.21
12.73
12.23
12.37
13.68
12.00
12.89
13.05
12.57
16.30
17.25
15.59
11.59
11.80
13.30
12.00
13.84
13.24
12.26
12.07
12.12
12.66
11.87
12.15
12.23
12.56
11.79
11.72
12.60
14.66
17.26
17.19
12.90
11.88
11.61
11.50"
13.00
12.98
13.17
10.85
11.15
11.15
11.07
11.19
11.50
11.63
12.02
12.11
13.63
22.27
21.07
21.82
22,27
22.45
20.98
22.81
24.55
27.31
32.41
32.41
25.75
21.55
23.11
26.59
27.58
28,54
29.89
21.52
22.48
22.12
21.55
19,81
21.34
22.15
21.19
23.02
22,87
25.45
30.97
30.88
30.04
19.21
21.70
23.74
23.95
27.37
29.77
24.73
22.27
20.98
21.85
18.20
16.67
17.07
18.52
17.76
18.31
18.53
19.63
22.63
24.91
9.93
9.93
9.93
10.41
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.88
10.97
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
11.05
10.79
10.01
10.00
10.01
10.00
10.00
10.00
10.00
10.01
10.01
10.00
10.00
10.01
10.01
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.36
11.91
11.91
11.94
11.63
11.32
11.43
11.43
11.43
• 11.43
11.43
11.53
11.53
11.43
11.53
11.53
11.53
11.48
11.49
11.38
11.43
11.22
11.32
11.43
11.53
11.53
1 1 .22
11.53
11.53
11.43
11.22
11,43
11.34
11.49
11.49
11.49
11.70
11.60
11.70
11.70
11.60
11.38
11.53
11.32
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.63
11.74
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
38
ICal APPENDIX F
-------
10:37
10:38
10:39
10:40
10:41
10:42
10:43
10:44
10:45
10:46
10:47
10:48
10:49
10:50
10:51
10:52
10:53
10:54
10:55
10:56
10:57
10:58
10:59
11:00
11:01
11:02
11:03
11:04
11:05
11:06
Average
Minimum
Maximum
Run 22
M17
Results
Train A
Train B
Average
13.80 24.73
13.53 23.08
13.62 24.61
13.57 25,27
13.12 26.80
12.31 31.99
12.66 33.04
13.45 33.13
14.83 22.69
16.78 21.52
1 8.00 22.42
14.96 25.72
12.02 27.31
13.16 24.54
10.85 16.67
18.32 36.10
ESC P5B DR 300-40
For P5B &
300-40
mg/acrn
15.1
15.67
15.385
11.36
11.36
11.36
11.36
10.77
10.57
10.57
10.57
10,57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
10.57
11.49
12.40
12.40
12.40
12.40
12.40
12.40
12.40
12.40
12.40
12.40
12.40
12.40
10.95
9.93
12.40
F904K
For F904K
&RSD
mg/dscm
22.8
23.7
23.25
11.63
11.43
11.32
11.32
11.43
11.32
11,28
11.28
11.39
11. 2B
11.18
11.27
11.27
11.56
11.18
11.94
Moisture
Moisture
%
13.5
13.7
13.6
82
82
82
82
82
82
84
84
84
84
84
84
84
82.69
82.00
84.00
Temp
181
39
ICal APPENDIX F
-------
Correlation Testing - Run 23: Mid PM concentration - 14th correlation test run
7/19/99 ESCP5B Durag 300-40 Durag F904K Moisture g/acm H2O Temp,
Time raw mA raw ra mA _raw rnA % Vdc degC
11:50
11:51
11:52
11:53
11:54
11:55
11:56
11:57
11:58
11:59
12:00
12:01
12:02
12:03
12:04
12:05
12:06
12:07
12:08
12:09
12:10
12:11
12:12
12:13
12:14
12:15
12:16
. 12:17
12:18
12:19
12:20
12:21
12:22
12:23
12:24
12:25
12:26
12:27
12:28
12:29
12:30
12:31
12:32
12:33
12:34
12:35
12:36
12:37
12:38
8.90
8.83
8.87
9,07
9.18
9.54
10.29
10.18
10.20
9.81
9.81
10.17
9.08
9.57
9.35
9.72
11.36
12,20
11.44
9.27
9.41
11.86
8.92
9.83
10.10
9.31
8.29
8.49
8.17
8.30
8.69
9.51
9.54
9.58
9.28
9.58
9.94
9.46
9.28
8.83
9.30
10.63
11.38
11.92
9.56
8.93
9.26
8.40
9.37
12.23
12.89
12.72
12.88
14.02
13.92
16.44
16.39
16.69
15.29
16.86
16,44
20.98
23.20
22.81
18.43
14.87
15.46
17.88
18.19
20.05
20.14
14.04
14.24
14.70
14.36
11.20
11,27
11.23
11,60
12,10
14.31
14.79
15.60
14.76
15.21
15.49
17.02
21.64
20.95
20.29
13.26
14.16
15.37
18.06
18.41
18.52
14.78
14.54
7,77
7.77
7.77
7.77
7,77
7.77
7.77
7,77
7.77
7.77
7.77
7.77
7.77
9.05
9.0S
9.05
9,05
9.05
9,05
9,05
9.05
9.0S
9.05
9.05
9.05
9.05
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
7.45
11.12
11.12
11.27
11.28
11.28
11.28
11.60
11.60
11.28
11.49
11,38
11,22
11.22
11.12
11.12
11.12
11.12
11.14
11.18
11.18
11.08
11.18
11.12
11.12
11.12
11.12
11.12
11.22
11.32
11.32
11.32
11.43
11.43
11.43
11.18
11.24
11.28
11.39
11.28
11.39
11.49
11.49
11.49 .
11.46
11.43
11.43
11.53
11.43
11.53
82
82
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
83
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
84
83
84
84
84
84
84
84
84
83
82
82
82
82
82
40
TCai APPENDIX F
-------
12:39
12:40
12:41
12:42
12:43
12:44
12:45
12:46
12:47
12:48
12:49
12:50
12:51
12:52
12:53
12:54
12:55
12:56
12:57
12:58
12:59
13:00 -
13:01
13:02
13:03
13:04
13:05
13:06
13:07
13:08
13:09
13:10
13:11
13:12
13:13
13:14
13:15
13:16
13:17
13:18
13:19
13:20
13:21
13:22
13:23
13:24
13:25
13:26
13:27
13:28
13:29
13:30
9.64
10.20
8.34
8.61
8,91
8.57
8.96
9.57
9.78
10.07
10.49
9.84
9.81
9.85
8.82
9.21
9.41
9.71
11.55
12.22
11.69
9.45
9.45
8.82
8.92
9.56
9.74
9.80
8.25
8.94
9.31
9.60
9.18
9.16
9.38
9.34
8.31
9.10
9.21
9.80
10,91
11.40
10.65
9.37
9.00
9.70
9.35
9.65
10.05
9,61
8.47
8.58
13.93
15.03
11.30
11.61
12.75
12.04
12.44
13.38
15.67
15,74
15.87
15.72
16,42
16.45
20.44
21.79
22.30
15.31
14.69
15.08
19,84
19.84
20.08
18.60
14.19
14.48
15.46
13.58
11.43
12,28
14.22
14.47
1425
14.84
15.17
15.60
19.51
20.44
19.81
14.52
13.72
14.69
18.13
18.18
18.13
18.28
14.35
14.79
15.53
14.79
12.19
12.20
7.45
8.41
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.73
8.53
8.33 .
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.33
8.49
8.97
8.97
8.97
8.97
8.97
8.97
8.97
8.97
8,97
8,97
8.97
8.97
8.97
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
7.22
11.53
11.53
11.53
11.32
11.32
11.32
11,22
11.32
11.48
11.39
11.28
11,14
11.22
11.22
11.22
11.22
11,02
11.22
11.12
11.22
11.24
11.18
1 1 .28
11.18
11.18
11.28
11.18
11.28
11.28
11.28
11.39
11.49
11.28
11.39
11.49
11.36
11.32
11.32
11.22
11.22
11.12
11.12
11.02
11.14
11.08
11.18
11.28
11.28
11.28
11.18
11.18
11.22
82
82
82
82
82
82
82
82
84
84
84
83
82
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
83
82
82
82
82
82
82
82
83
84
84
84
84
84
84
84
82
41
real APPENDIX F
-------
13:31
13:32
13:33
13:34
13:35
13:36
13:37
13:38
13:39
13:40
13:41
13:42
13:43
13:44
13:45
13:46
13:47
13:48
13:49
13:50
13:51
13:52
13:53
13:54
13:55
13:56
13:57
13:58'
Average
Minimum
Maximum
Run 23
M17
Results
Train A
Train B
Average
8.97 12.03
8.61 12.30
8,69 12.67
9.15 13.20
9.84 15.82
9.95 15.74
9.46 16.14
9.49 14.59
9.48 15.56
9.64 16.09
9.57 15.68
8.17 11.20
12.22 23.20
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
8.82
8.69
8.755
7.22
7.22
7.45
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7.53
7,53
7.53
7.53
7.61
7.69
7.69
7.69
7.70
7.69
7.70
7.70
7.70
7.69
7.69
7.69
7.70
8.08
7.22
9.05
F904K
For F904K
&RSD
mg/dscm
13.1
13
13.05
11,22
11.32
11,32
11,32
11.53
11.43
11.32
11.53
11.43
11.43
11.29
11.02
11.60
Moisture
Moisture
%
12.9
13.5
13.2
82
82
82
82
82
82
82
82
82
82
82.87
82.00
84.00
Temp
181
42
ICaJ APPENDIX F
-------
Correlation
7/19/99
Time
15:10
15:11
15:12
15:13
15:14
15:15
15:16
15:17
15:18
15:19
15:20
15:21
• 15:22
15:23
15:24
15:24
15:25
15:25
15:26
15:27
15:28
15:29
15:30
15:31
15:32
15:33
15:34
15:35
15:36
15:37
15:38
15:39
15:40
15:41
15:42
15:43
15:44
15:45
15:46
15:47
15:48
15:49
15:50
15:51
15:52
15:53
15:54
15:55
15:56
Testing -
ESC P5B
raw mA
19.04
15.54
12.31
12.39
12.62
14.28
14.70
15.03
14.18
14.31
14.59
14.85
14.56
14.37
15.32
14.48
14.01
13.90
13.01
14.11
15.31
18.64
19.70
14.74
12.03
12.34
12,06
13.28
14.27
14.28
13.02
13.54
13.72
13.57
13.41
13.90
14.84
12.31
11.73
12.82
13.93
16.35
18.13
17.16
12.23
12.80
12.45
13.57
14.55
Run 24: High PM concentration - 15th
Durag 300-40 Durag F904K Moisture
raw ra mA raw mA %
30.88
98.14
34.45
32,44
31.06
27.43
27.58
28.09
23.83
25.45
26.65
25.96
26.32
27.49
30.37
31.51
34.93
35.26
41,92
39.76
25.96
26.86
28.48
69.25
29.92
31.63
29.08
25.00
25.90
26.62
22.21
23.89
25.03
24,58
24.34
25.72
27.10
34.69
40,03
39.07
29.38
25.06
26.32
31.66
30.01
31.66
33.94
26.62
27.31
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.81
12.80
12.80
12.80
12.73
12.73
12.73
12.73
12.73
12.72
12.73
12.73
12.73
12.72
12.73
12.73
12.72
11.83
11.52
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11.53
11,49
11.60
11.60
11.60
11.49
11.53
11.63
11.67
11.60
11.60
11.49
11.49
11.39
11.39
11.49
11.39
11.39
11.39
11.39
11.49
11.49
11.39
11.39
11.28
11.49
11.60
11.60
11.60.
11.69
11,53
11.56
11.56
11.70
11.49
11.60
11.70
11.80
11.80
11,70
11.70
11.60
11.56
11.63
11.53
11.53
11.46
11.49
11.60
11.49
correlation test run
g/acm H2O Temp.
Vdc deg C
84
84
84
84
84
82
82
83
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
83
83
84
84
84
84
84
84
84
84
84
83
82
82
82
83
84
84
84
ICal APPENDIX F
43
-------
15:57
15:58
15:59
16:00
16:01
16:02
16:03
16:04
16:05
16:06
16:07
16:08
16:09
16:10
16:11
16:12
16:13
16:14
16:15
16:16
16:17
16:18
16:19
16:20
16:21
16:22
16:23
16:24
16:23
16:26
16:27
16:28
16:29
16:30
16:31
16:32
16:33
16:34
16:35
16:36
16:37
16:38
16:39
16:40
16:41
16:42
16:43
16:44
16:45
16:46
16:47
16:48
15.47
14,26
14.90
15.74
15.49
13.65
15.75
15.37
13.59
13.11
13,71
15.29
17.59
19.07
18,82
12.33
12.94
12.37
12.82
14.30
14.54
14.63
13.04
14.49
14.78
13.54
14.02
14.46
13.88
13.24
13.36
14.15
14.97
18.96
19.53
14.24
11.95
12.71
12.45
14.35
15.14
16.05
13.86
14.82
15.50
14.87
14.16
15.29
15.31
12.02
12.70
13.12
28.12
26.11
26.29
27.55
28.18
26.41
28.57
28.72
32.89
42.25
38.92
34.09 •
23.56
27.28
32.53
27.40
33.10
31.21
27.40
25.72
26.95
25.03
24.01
25.39
26.65
25.45
27.85
27.79
30.07
39.22
39.88
39.76
22.99
27.67
28.90
33.01
32,35
33.25
31.60
27.61
28.81
29.62
23.80
26.95
27.19
26.80
28.93
29.29
31.18
41.32
43.66
44.32
11.52
12.16
12.80
12.80
12.81
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.80
12.58
11.93
11.93
11.93
11.93
11.93
11.93
11.92
11.93
11.93
11.93
11.93
11.93
11.93
12.48
12.48
12.48
12.48
12.48
12.48'
12.48
12.48
12.48
12.48
12.48
12.48
12.48
12.61
12.65
12.65
12.65
12.65
12.65
12.65
12.64
12.65
12.64
12.65
11.60
11.39
11.39
11.39
11.49
11.18
11.28
11.39
11.39
11.28
11.39
11.39
1 1 ;39
11.49
11.39
11.48
11.39
11.43
11.22
11.43
11.48
11.49
11.49
11.49
11.49
11.28
11.49
11.60
11.60
11.70
11.70
11.80
11.70
11.70
11.69
11.63
11.53
11.63
11.53
11.74
11.74
11.84
11.84
12.05
11.94
11.74
11.84
11.94
11.94
11.94
11.84
11.84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
84
84
84
84
84
84
84
84
84
84
84
84
84
84
84
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
82
44
ICal APPENDIX F
-------
16:49
16:50
16:51
16:52
16:53
16:54
16:55
16:56
16:57
16:58
16:59
17:00
17:01
17:02
17:03
17:04
17:05
17:06
17:07
17:08
17:09
17:10
17:11
17:12
17:13
17:14
17:15
17:16
Average
Minimum
Maximum
Run 24
M17
Results
Train A
Train B
Average
15.63 28.57
17.85 27.25
19.43 29.95
16.30 34.15
13.59 33.79
13.06 35.68
12.93 34.66
14.58 28.21
15.50 29.59
16.09 29.71
14.45 26.53
14.50 30.88
11.73 22.21
19.70 98.14
ESC P5B DR 300-40
For P5B &
300-40
mg/acm
18.84
18.47
18.655
12.64
12.65
12.76
12.80
12.81
12.80
12.80
12.80
12.80
12.81
12.80
12.80
12.80
12.81
12.80
13.12
13.44
13.44
13.44
13.44
13.44
13.44
13.43
13.44
13.44
13.44
13.44
13.43
12.57
11.52
13.44
F904K
For F904K
&RSD
mg/dscrn
28.6
28.1
28.35
11.84
11.84
11.74
11.63
11.53
11.53
11.56
1170
11.70
11.60
11.60
11.57
11.18
12.05
Moisture
Moisture
%
13.9
14.2
14.05
82
82
82
82
82
82
83
84
84
84
84
83.38
82.00
84.00
Temp
182
45
ICal APPENDIX F
-------
ICal Appendix G
Statistical Analysis Data and Graphs for PM OEMS
MRl-OPPT*4T03-<2-0? Appendices Covers, WPD
-------
Definitions of Terms in Correlation Statistical Calculations Tables
Column headings for linear correlations:
x Signal in rnA
y Corresponding PM concentration from reference test method
Predicted PM concentration based on linear correlation
\2
ylin
(x-xbar)A2
(y-ybar)A2
(x-xbar)(y-ybar)
CJAW
Chigh
(X; - X)
(*» - *)0>,- - y)
lower confidence interval for the predicted concentration y at point X;
upper confidence interval for the predicted concentration y at point Xj
confidence interval as a percent of the emissions limit
n
n'
1+=(£Z*L'
npnme
kt
Tlow
Thigh
T " f, where u,,. and yf are taken from Table I and f=n- 2
lower tolerance interval for the predicted concentration y at point xs
upper tolerance interval for the predicted concentration y at point xs
tolerance interval as a percent of the emissions limit
Confidence interval:
Tolerance interval:
y ± kT • SL
(x-x)2
ICal APPENDIX G
-------
Other variables shown:
N number of observations
xbar mean of x, x
ybar mean of y, *
s
Syy
3OC
a =
Sxx
S
constant (slope) in linear equation y = ax + b,
b constant (y-intercept) in linear equation y = ax + b, -^
R linear correlation coefficient
•=!
Sxy '=1
tf value oft from Table I for f degrees of freedom, where f = n - 2
vf value of v from Table I for f degrees of freedom, where f = n - 2
EL PM emissions limit
SL scatter of values around the linear correlation
Column headings for polynomial correlations:
x Signal in mA
y Corresponding PM concentration from reference test method
yquad Predicted PM concentration based on polynomial correlation
X2 X:2
ICal APPENDIX G
-------
X3 X;3
X4 X;4
XY xj,
X2Y ^
/"*_ ~\2
(yhat-y)2 O'-W
delta CD + 2C,Xj +(2C2+C3)xi2 + 2C4Xj3 + Csx,4
Clow lower confidence interval for the predicted concentration y at point X;
Chigh upper confidence interval for the predicted concentration y at point Xj
CI% confidence interval as a percent of the emissions limit
ri =
nprime
kt
kr = u , • vf
" * , where un. and vf are taken from Table I and f = n - 2
Tlow lower tolerance interval for the predicted concentration y at point xt
Thigh upper tolerance interval for the predicted concentration y at point x;
TI% tolerance interval as a percent of the emissions limit
y i t f • s V A
Confidence Interval: } q
Tolerance Interval:
y±kT-sq
Other variables, .shpw^n:
N number of observations
SI
5, = E (^-)2
S2 /=1
ICal APPENDIX 0
-------
c _ y
3 £~j
S3 w
S4
S5
S6
S7 '=1
DETA detA - nS2S4 - S2S2S2 + S,S3S2 - S3S3n + S2SjS3 - S4S
bO constant in polynomial equation, y = b0 + bpc + b2x2
b, , /C/ C* O _i_ O *C O , L OOO CCC *CJCC "C^I
Q \^5^2|"-*4 ^1*^3^*7 ^263 ~ 7 ^22 ™ 3^*3^5 "" *^I4I"
bl constant in polynomial equation, y = bc + b,x + b2x2
b, — (nS6S4 + S5S3S2 + S2SjS7 - S2 S6S2 - S7S3n- S4S|S
b2 constant in polynomial equation, y = b0 + bpt + b2x2
D^ "™~ \nQ2*™*7 O]OgSl2 Oci.!5ii~H *" OT OnjJ^ *" (^jkSgH ™ M'rwt1
ybar mean of y
f degrees of freedom, f = n-3
sq scatter of the y values around the polynomial curve
1
vf . value of v for f degrees of freedom from Table I, where f = n-3
JCal APPENDIX G
-------
EL PM emissions limit
cO ' (S2S4-S32)/D
el (S3S2-SiS4)/D
c2 (SA-S/yD
c3 (nS4-S22)/D
c4 (SiS2-nS3)/D
c5 (nSz-S^/D.
D n(S2S4-S32)+S1(S3S2-S,S4)+S2(S1S3-S22)
sy ,71-1
r I
V F
polynomial correlation coefficient, * y
ICal APPENDIX G
-------
ESC P5B - Linear
o
G!
S!
o
Emission Limit = 17 mg/acm
10
mA
12
14
» Initial Corr.
ylin
Cllow
Clhigh
Tl low
Tl high
16
-------
ESC P5B - Linear
O
Run
17
16
18
21
20
23
13
14
15
19
22
24
sum
N
xbar
ybar
a
b
R
x(mA)
5.78
5.B7
6,00
8.97
9.45
9.57
9.60
10.01
10.54
12.00
13,16
14.50
12,93
115.45
12
9.6208
10.6629
1.8883
-7.5042
0.964421
y (mgfacm)
Initial Coir.
2.68
3.03
3.20
9.42
10.52
8.76
11.61
13.92
14,47
16.33
15.39
13.66
127.955
ylin
3.4102
3.5802
3.8257
9.4339
10.3403
10.5669
10.6236
11.3978
12,3986
15.1555
17.3460
19,8763
17
Sxx
Syy
Sxy
f
«
vf
EL
(x-xbar)A2
14.7520
14.0688
13.1104
0.4236
0.0292
0,0026
0.0004
0.1515
0,8449
5.6604
12.5267
23.8063
1 1.262441
B5. 3757
327.3011
161.2157
10
2.228
1.593
17
(y-ybar)*2 (x-xbar)(y-ybar)
63.7270
58.3378
55.7698
1 .5573
0.0204
3.6401
0.8970
10.8086
14.4558
32.1158
22.2981
63.8734
30.6511
28.6486
27.0401 '
0.8122
0.0244
0.0970
-0.0197
1 ,2675
3,4947
13.4829
16.7122
38.9947
SL
Cllow
1.7048
1.9016
2.1855
8.432B
9.3656
9.5940
9.650B •
10.4147
11.3697
13.8520
15.7297
17.8483
15.4366
1.512479
CI high
5.1156
5.2587
5.4658
10.4353
11.3151
11.5399
11.5964
12.3809
13.4275
1 6.4590
18.9622
21.9043
18.5634
CI%
10.0318
9.8738
8.6479
5.6901
5.7339
5.7233
5.7224
5.7828
6.0525
7.6678
0.5074
11.9293
9.1966
nprltne
3.9044
4.0303
4.2213
11.3257
11.9510
11.9956
11.9993
11.7499
10.7263
6.6830
4.3470
2.761 1
4.6458
un'
1.295
1.295
1.295
1.203
1.199
1.199
1.1 99
1.199
1.203
1.233
1.295
1.340
1266
kt
2.0629
2.0629
2.0629
1.9164
1.9100
1.9100
1.9100
1.9100
1.9164
1.9642
2.0629
2.1343
2.0167
Tllow
0,2901
0.4600
0.7055
6.5355
7.4515
7.67B1
7.7347
8.5089
9.5001
12.1848
14.2258
16.6477
13.9497
71 high
6.5304
6.7003
6,9458
12.3324
13.2292
13.4558
13.5124
14,2866
15.2971
18.1263
20.4861
23.1049
20.0503
Tl%
18,3538
18.3538
18.3538
17.0499
16.9932
16.9932
16.9932
16.9932
17.0499
17.4751
18.3538
18.9916
17.9428
O
-------
CO
ESC P5B - Polynomial
25
I
o
y=-16.06+3.79x-0.098xA2
20
Emission Limit = 17 mg/acm
-5
* Initial Corr.
yquad
Ci low
Clhigh
Tl low
Tl high
mA
-------
o
E.
I
tn
ESC P5B - Polynomial
y (mg'aem}
Run
17
16
18
21
20
23
13
14
15
19
22
24
x[mA)
5.78
5.87
6.00
6.97
9.45
8.57
8.60
10,01
10,54
12.00
13,16
14,50
N
S1
S2
S3
54
85
86
S7
DETA
60
b1
b2
Initial Coir.
2,68
3.03
3,20
9.42
10,52
8.76
11.61
13.82
14.47 •
16.33
15.39
18.66
12
115,46
1196.100B
13167.B849
15Z24S.27
127.955
1392.24945
15817.5113
750939.371
-1S.OS
3,781
-0.098
yqufld
2.5854
2.8241
3.1659
10.0755
11,0302
11.2818
11.3193
12.0870
13.0306
15.34SB
1i,8879
1B.S41S
X2 X3 X4
33.4084 193.1006 1116.121
34.4569 202.262 1167.276
36 216 12B8
80.4609 721.7343 6473.956
89.3025 843.9086 7B74.B37
81 .8849 876.4675 8387.784
B2.16 SB4.736 8493.488
100.2001 1003.003 10040.08
111.0916 1170.905 1234134
144 1728 20736
173.1858 2279.122 29993.25
210.25 3048.625 44205.06
19
sq 1.32742
Vf 1.645
tl 2.262
EL 17
XV
15.4B04
17.75675
19.17
84.45255
93.414
83.78535
111.456
139.3382
152.4611
195.96
202.4666
270.4978
cO
01
02
C3
C4
05
D
XSY
B9.534S1
104.2321
115.02
757,5394
938,4623
801.8258
1069.978
1S94.78B
1608.94
2351.52
2684.46
3822.214
11,5962
-2.4324
0.1193
0.5277
-0.02S5
0,0014
750939,4
(ylMt-y)2
0.0069
0.0404
0.0008
0.4363
0,2601
8.2840
0.0845
3.3K»
2.0575
0.9666
2.2588
0.0883
delta
0.3531
0.3296
0,2889
0,1469
0.1515
0.1522
0.1523
0.1628
0.1502
0.1548
0.25Si
0.697B
sy
r
Cllow
0.8013
1,1003
1.5243
8.9245
9.861S
lO.OKB
10,1474
10.0133
11.8871
14.1845
15.3570
15,8332
S.45478
0,86984
Clhlgh
4.3696
4. 54 78
4.8076
11 £265
12.1988
12.4331
12.4811
13,2606
14,1841
16.5272
18,4188
20,8133
Cl%
10.4949
10.1400
9.6567
6.7707
6,8745
6.8899
6.8930
6.9040
6.8441
6.9491
9.0051
14,7846
n*
2.83S3
3.0341
3.3454
6.8051
6.6012
6.5717
£.5658
6.8449
6.6699
6.4602
3.6470
1.4330
unf
1.3400
1.3400
1.3400
1.2330
1.2330
1.Z330
1.2330
1.2330
1.2330
1.2470
1.2950
1.4330
M
8.2043
2.2043
2.2043
2.0283
2,0283
2.0283
2.0283
2,0283
2.0283
2.0513
2.1303
2.3573
TItow
-0.3406
-0.1020
0.2399
7.3831
8.3378
8,5694
8.8269
93946
10,3382
12,6229
14,0601
16.2124
TIMgh
6.5115
5.7501
6.0820
12.7679
13,7226
13.9542
14.0118
14.7793
15.7230
1B.C6BB
19.7157
21.4706
Tl%
17,2120
17.2120
17.S1SO
15.8378
15.8376
15.8378
15,8378
1B.837B
16,8378
18,0174
16.6339
18.4095
y-yb«r2
63.7270
58,3378
55.7698
1.SS73
0.0204
3.6401
0.8970
10,6086
14,4SS8
32,1158
22.2981
83,8784
ybar
10.66291ST
O
-------
Durag DR 300-40 - Linear
30 i
o
c.
is
"0
tn
o
Emission Limit = 17 mg/acm
* Initial Core.
ylin
CHow
• Clhigh
Ti low
TI high
-------
M
o
Durag DR 300-40 -
Run
16
17
18
21
13
23
20
14
15
.19
22
24
limit
sum
N
xbar
ybar
a
b
H
Linear
y (mg/acm)
X (mA) Initial Corr. ylln
6.42
6.44
7.28
14.32
16.45
15.68
15.8
17.22
19.36
20.93
24.54
30.88
25. 13
194,32
12
18.19333
10.66202
0.708998
-0,81812
0.954697
3.03
2.68
3.20
9.42
11.61
3.76
10.52
13.92
14.47
16.33
15.39
18.66
127.955
3.7336
3.7478
4.3434
9.3347
10.1359
10.2990
10.3840
11.3808
12.9081
14.0212
16.5807
21.0757
17
Sxx
Syy
Sxy
f
tf
vf
EL
(x-xbar)A2
95.5180
95.1275
79.4475
3.5094
0.5525
0.2635
0.1547
1.0540
10.0278
22.4360
69.6668
215.6982
79,6894
593.45607
327.30107
420.75903
10
2.228
1.593
17
(y-ybar)A2 (x-xbar)(y-ybar;
58.3378
63,7270
55.7698
1.5573
0.8970
3,6401
0.0204
10.6086
14.4558
32.1158
22.2981
63.8734
74.6479
77.8600
66.5640
2.3378
-0.7040
0,9794
0.0562
3.3439
12.0399
26.6431
39,4137
117.3771
SL
Cl low
1,8589
1.8756
2,5756
8.2016
9.0348
8,2011
9,2874
10.2842
11.7072
12.7010
14.8813
13.5403
15.2292
1,702464
CI high
S.6084
5.6200
6.1112
10.4679
11.2370
11.3988
11.4807
12.4974
14.1089
15.3414
18.2801
23.61 1 1
18. 7703
Cl%
11.0279
11.0130
10.3987
6.B656
6.4769
6.4581
6.4B1 1
6.5093
7.0639
7.7658
9.8864
14.9141
10,4165
rprlme
4.0936
4.1046
4.6039
11.2049
11.8674
11.3364
11.9626
11,7498
9.9770
8.2550
4.9819
2.2382
4,5882
un*
1.295
1.295
1.266
1.203
1.199
1.199
1.199
1,199
1,208
1.223
1.266
1,433
1.266
kt
2.0628
2.0629
2.0167
1.9164
1.9100
1.9100
1.9100
1.9100
1.9243
1.9482
2.0167
2.2828
2.0167
Tllow
0.2216
0.2358
0.9100
6.0722
6.8842
7.0472
7.1323
8.1391
9,6319
10.7044
13.1473
17.1694
13.5666
Ti high
7,2457
7.2599
7.7768
12.5973
13.3876
13.5507
13.6358
14-6425
16.1842
17.3380
20.0141
24.9621
20.4334
Tl%
20,6593
20.6593
20.1966
19,1916
19.1278
19.1278
19,1278
19.1278
19.2713
19.5106
20.1866
22.8608
20, 1366
-------
i-o
Durag DR 300-40 - Polynomial
25
O
y=-5.29+1.33x-0.018xA2
20
Emission Limit = 17 mg/acm
15-
•* Initial Corr.
yquad
'Ctlow
'Glhigh
---TIlow
Tlhigh
mA
-------
o
E.
5
I
ir«g DR 30O-4Q -
Run
16
17
13
21
13
23
20
14
18
1§
22
24
x{mA)
6.42
8.44
7.28
14.32
15.45
15.88
15.80
17.22
19.36
20.93
24,54
30.83
25.S9
H
81
S2
83
84
S5
ss
S7
OETA
M
b1
b2
Polynomial
y (mg/acm)
Initial Con.
303
2.88
3.2O
942
11.61
8.76
10.52
13.82
14.47
16.33
15.38
18.66
12
194.32
3740.1446
81097.2906
1B20300.73
127B55
2492.777
53842.7473
31S003122
-S.29
1.331
-0.018
yqnod
2,5172
2.5392
3.4500
100862
10.9855
11 1K9
112547
123017
13.7427
14.6*1
16.5490
18.6708
17.0006
X2 X3 X4
41.2184 264.6093 1698.7916
41.4736 267.0900 1720.0695
52.9984 385.8284 2808.8304
205.0624 2938,4936 42050,5879
238.7025 3687,9536 58978,8835
245.8624 3855.1224 60448.3197
249.64CO 3944.3120 82320.1296
298.6284 5106.Z1SO 87929.0920
374.8096 7256,3139 (404822353
438.0649 9188.6884 1S1900.85B6
602.2118 14778.2727 362B6B.8112
9S3.S744 29448.3775 909304.1363
SS4JSS4 167S9.S777 -428Ba?.9S83
(9
sq 1,3778
vf 1645
tf 2212
EL= 17
XV
19.420S
17,2692
23,2586
134.8226
179.3745
137.2784
166.2160
289.7024
280.0424
341.7868
377.6478
57S.0684
CO
Bl
c2
c3
04
si
D
XZY
124.8796
111.1492
1S93299
1930.8625
2771 .3360
2152.5253
2628.2128
4127.6753
B421.6S09
7153.5998
0265.02SS
17788.9304
US 19869
-0.2217033
0.00181945
0.028745S2
-0.0007B22
2.2S08E-OS
3IS003122
f/ha|.y)2
0.2578
0,0138
0,0650
0,4506
0.3901
S.7978
0.5397
2.6189
O.S218
2.8728
1.3548
0.0003
delta
0.3478
0.345B
0.2730
0.128B
0,1349
0.1360
0.1366
0.1432
0.1490
0.1529
O.200B
0.8514
0.2395
sy
r
01 low
0.8129
0,8398
1.9*00
9.0493
9.B246
10.0972
10.1865
1 1.5063
12.6273
13 5651
IS, 2541
16.0043
IS.S8B3
6.4S4782
0.9721B8
ClhiLih
4.2215
42386
4.9801
11.123Z
12.0463
12.2285
12.3228
13.3951
14.8589
15,8252
17B440
21.3373
TS.4/SO
Cl%
10.0252
9,9905
8.882S
6.0997
6.2402
6.26B7
8.2838
6.4317
6.5608
6.6473
78173
156853
fi.aias
n"
2.8752
2.B817
3,6625
7,7666
7.4206
7,3536
7,3195
6.9855
6.7132
6.8397
4.9808
1.1745
4.174S
un"
1.3400
1,3400
1.2950
1.2230
1,2330
1.2330
1,2330
1.2330
1.2330
1.2330
1.2660
1.4330
I.2SSO
kt
2.2043
2,2043
2.1303
2.0118
2,0283
2.0283
2,0283
2.0283
8.0883
2.0283
2.0828
S3573
1.13O3
mow
•0.2989
•0.2769
0,7285
7.5180
8,3942
8.5716
8.6634
9,7104
11.1514
12.1039
13.9884
15.659S
14.2791
TlhlgH
5.3333
5.3553
8,1716
12.8585
13.5767
13.7541
13,6459
14.8930
16.3339
17.2864
19.2098
21.6824
19.7122
TI%
16.58S4
16,5654
16,0091
15,1191
15,2427
15,2427
15,2427
15.2427
15.2427
15.B427
15.6506
17.7151
IS 009!
y.ybsrz
58,3378
63,7270
55,7698
1 .5573
0.8970
3.6401
0.0204
10,6063
14.4SS8
32.1163
22,2981
S3.8734
ytai
o
-------
Durag F904K - Linear
3
o
y = 3.37x-12.38
Emission Limit = 25.5 mg/dscm
Initial Corr.
y!in
- C! low
Clhigh
T! low
T! high
10
12
tnA
-------
a
"d
Durag F904K - Linear
Hun
18
1?
18
21
20
23
13
14
15
19
22
24
sum
N
xbar
ybar
a
b
R
x(mA)
5.04
5.09
5.21
8,05
8,07
8.08
8,58
9.24
9,90
10.48
10,95
12,57
J 1.2422
101.34
12
8.445
16-075
3,36943
-12.3798
0.9876
y (mg/dscm)
Initial Corr.
4.60
4.00
4.80
14.30
16.10
13.05
17.20
21.10
21.75
24.4D
23.25
28.35
192.9
ylin
4,6021
4.7706
5.1749
14.7441
14.8115
14.8452
16.5299
18.7537
21.2471
22.9318
24.5154
29.9739
25.5
Sxx
Syy
Sxy
f
tt
vf
EL
(x-xbar)'Z
11.5940
11.2560
10.4652
0.1560
0.1 406
0.1332
0.0182
0.6320
2.3562
4.1412
6.27SO
17.0156
7.8244
64.1835
747.0925
216.2615
10
2.228
1.593
25.5
(y-ybarj*2
131.6758
145.8056
127.1266
3.1506
0.0006
9.1506
1.2656
25.2506
32.2053
69.3056
51.4808
150.6756
(ic-xbat)(y-ybar)
39.0724
40.5116
36.4746
0.7011
-0.0094
1.1041
0.1513
3.9949
8.7111
16.9414
17,8734
50.6344
SL
Cllow
3.0487
3.2327
3.6741
13.8586
13.9273
13.9616
15.6556
17.8308
20.1895
21.7692
235287
28.1891
24.1303
1.3S7039
Ci high
8.1555
6,3084
6,6757
15.6295
15,6957
15.7288
17.4042
19.6766
22,2946
24.0944
25,8021
31 .7586
SS.8697
Cl%
6.0918
6.0307
5.8854
3,4723
3.4675
3.4651
3.4286
3.6193
4.1081
4.5592
5.0458
6.9990
5.3715
nprime
3.7883
3.8654
4.0587
11.6599
11.6926
11.7084
11.9593
10.7319
8.3303
6.7634
5.5218
2.8699
4.8723
un"
1.295
1.295
1.295
1.199
1.1 89
1.199
1.199
1.203
1.223
1.233
1.247
1.340
1.286
kt
2.0629
2.0629
2.0629
1.9100
1.8100
1.9100
1.9100
1.9164
1.9482
1.9642
1.9885
2.1346
2.0167
Tllow
1 .8026
1.9711
2.37E4
12.1521
12,2195
12.2532
13.9379
16.1531
18.6032
20.2663
21.8197
27.0771
22.7632
II High
7.4016
7.S701
7.9744
17.3360
17,4034
17.4371
19.1218
21.3543
23.8909
25.5972
27.2111
32.8706
20.2363
T1%
10.9784
10.9784
10.9784
10,1645
10.1645
10.1645
10.1648
10.1984
10.3680
10.4528
10.5714
1 1 .3599
10.7325
o
-------
Durag F904K - Polynomial
Of] _
OK
l*-4
EL
Sv *2A
m °
z M
1^ -
O 15
m
5,
0.
*
y = -19.13 + 5.12x- 0.1 1x^2
>
s '*
>s . '
•** « '
Emission Limit = 25.5 mg/dscm x . • ' ^s^
~j* * ^**^ " * *"*
'" f'^ . .-•'''*
'' --'><'' s'
S • ••><••'"'''
, x .' ./ * * ^
x • +^''' ''
,''.•*/.*'' '''
'*.•'/•''''
s' .'" / ''^x
x^ -•/•*' ^
X ,' vX ,« X
X .' >X ,' X
X .' -X . X
J^ * J-^ X II*1*
X ,•' ^ .' X
''.••'/.'•'''
/..->X-x
-'XV'>X
•"x^"'
1 6 8 10 12 1
*• Initial Corr.
yquad
ai«...
low
ahirih
niyn
Tl [OW
T! high
4
mA
-------
Durag F904K * Polynomial
Run
16
1?
18
21
20
23
13
14
1i
19
22
24
M(mAJ
5.04
6.09
S.21
8.05
8.07
8.08
B.SR
9.24
9.9i
10.48
10.9S
12.57
N
81
E2
83
S*
S5
S6
S7
OETA
bo
bl
b2
Initial Con.
4.60
4.00
4.80
14,30
16.10
13.05
17.20
21.10
21.75
24.40
23.25
88.3S
12
101.34
819.9988
8840.6555
68790.0270
132.9
1845,302
18358,9575
290261.4723
-19,13
5.121
-0.105
yquad
4.0178
4.2207
4.705S
15.2374
1S.3B80
1 S.4003
17.0866
1S.2322
21.8290
23.01 59
24.3657
2B.B6S8
xz
25.4016
25,9081
27.1441
64.B025
65.1249
S5.B864
73.6164
85.3776
99.8004
109.8304
11H.B02S
15B-OQ48
I
sq
vf
X3 X4, XY XZY
12B.0241 B45.2413 23.1840 118.8474
131,6722 871J2S6 20.3600 103.6324
141.42W 736.8022 25.0080 130.2917
521.6001 41P8.3640 115.11SO 92B.67SB
S2S.S579 4241.2526 129.8270 1048.5109
827.5141 4262.3140 10S.4440 BS1.9S7S
631,6287 5410.3743 147.5760 12868021
78BJB8Q 12BB.334S 194.BB40 1801,4874
994.012O 9920,239? 217DBSO 2186.3087
1181.0226 120SS.7168 2SS.7120 2879.8618
1312.9324 14376.8095 284.5875 2787.7331
1988.12)6 24965.8484 386,3995 4479,4389
9 at) 12.1601
01 -2.9788
I.Z539 c2 0.1706
C3 fl.7%49
t.S45 e4 -0.0443
(yliol-y)2
0,3369
0.0487
0.0089
0.9949
0.6387
55238
001PB
3.488R
0.0488
1,9157
1.2448
0.09T8
delta
0.3462
0.331 S
0.2994
0.1 895
0.1SS8
0.1598
0.1 SB3
0.1483
0.1392
0.1495
0.1865
0.7624
Cllow
2,3424
2,5812
3.1473
14.1802
M.22BS
14,2826
15.9S38
18.13SS
20.4667
21.9147
23.1360
26.1765
Cl high
5.6932
5.8GC3
6J2S38
16.4347
16.5035
16S37i
18.2194
20.3288
22.5914
24.1172
25,8954
31.1491
Cl%
8 .5703
6,4286
6.1106
4.4598
4.4609
4.4814
4.4423
4.3005
4.1862
4,3186
4.8228
9.7503
n*
2.8886
3.0165
3,3386
6.2S97
6.2668
6.2651
S.3191
8.7427
7.1844
S.E8B3
8.36SO
1.3117
un'
1.S40
' 1.340
1.340
1,247
1.247
1,247
1,247
1.233
1.233
1.233
1.2fi8
1.433
M
2J043
2,2043
2,2043
2.0S13
2.0S13
2.0513
2.0B13
2.0283
8. 0283
2.02B3
2.0B28
2.3S73
Tllow
15429
1 .4458
1 .1306
12.7151
12.7837
12.8179
14.6048
16.6788
18.9757
20,4828
a 1.7440
256053
Tlhlgh
6.7927
6.9956
7.4805
17.6798
17.9484
17.9826
19.6689
21.785S
24.0824
26.5693
28,8874
31.6303
T1%
10.882 1
10.8821
10.8821
10.1288
10.1288
10.12B8
10.12S8
10.0131
10.0131
10.0131
10.2811
11.6373
y-yB»r2
131 ,6768
145.8058
127.1258
3.1506
0.0008
9.1508
1.26S8 "
25.2506
32,3058
88,3058
SI .4808
180.8756
sy B.2412
i P. 3383
tl 2.262 OS 0.0027
EL
D 280281.4723
25.B
ybar
-------
Tests for best regression fit Ff (12) = 5.12
Durag F904K
Polynomial vs. Linear (dropped 3 values)
FfBG 2.620414 less than Ff(12), so linear is better
Durag DR 300-40
Polynomial vs. Linear (dropped 3 values)
Ff DLS 8.757966 greater than Ff(12), so polynomial is better
ESC P5B
Polynomial vs. Linear (dropped 3 values)
Ff ELS 3.982S99 less than Ff(12), so linear is better
18
ICal APPENDIX G
-------
TECHNICAL REPORT DATA
(Please read Instructions on reverse before completing)
1. REPORT NO- 2,
EPA-454/R-00-040b
4. TITLE AND SUBTITLE
EVALUATION OF PARTiCULATE MATTER CONTINUOUS EMISSION
MONITORING SYSTEMS
Volume 2
7. AUTHOR® Dan Bivins
Emission Monitoring and Analysis Division
9. PERFORMING ORGANIZATION NAME AND ADDRESS
U.S. Environmental Protection Agency
Office of Air Quality Planning and Standards
Research Triangle Park, NC 27711
12. SPONSORING AGENCY NAME AND ADDRESS
Director
Office of Air Quality Planning and Standards
Office of Air and Radiation
U.S. Environmental Protection Agency
Research Triangle Park, NC 27711
3. RECIPIENT'S ACCESSION NO.
3. REPORT DATE September 2000
6. PERFORMING ORGANIZATION CODE
8. PERFORMING ORGANIZATION REPORT NO,
10, PROGRAM ELEMENT NO.
11. CONTRACT/GRANT NO.
68-D-98-027
13. TYPE OF REPORT AND PERIOD COVERED
Final
14. SPONSORING AGENCY CODE
EPA/200/04
15, SUPPLEMENTARY NOTES
16. ABSTRACT
This final report describes an extended field demonstration of three particulate matter (PM) continuous
emission monitoring systems (CEMS) at a coal-fired boiler equipped with a lime slurry scrubber and
baghouse for air pollution control. The primary objectives of the field study were to: (1) demonstrate whether
the PM CEMS could provide reliable and accurate data over an extended period, (2) evaluate the PM CEMS
for durability, data availability, and setup/maintenance requirements, and (3) determine whether the PM
CEMS satisfy all the requirements of draft PS-11 and the quality assurance (QA) criteria specified in draft
Procedure 2, or determine if changes are needed in the requirements of PS-11 and/or Procedure 2. This
report presents the results of the study involving two different PM CEMS technologies (light scatter and beta
_gauge) at _the_cpal-fired boiler. The report consists of five separate volumes.
17. . KEY WORDS AND DOCUMENT ANALYSIS
a. DESCRIPTORS
PS-11
Mettai 17
Procedure 2
Moisture CEMS
Demonstration
Particulate Matter
PM CEMS
IS, DISTRIBUTION STATEMENT
Release Unlimited
b. IDENTIFIERS/OPEN ENDED TERMS'
Air Pollution control
19. SECURITY CLASS (Report)
Unclassified
20. SECURITY CLASS (Page)
Unclassified
e. COSATI Field/Group
21. HO, OF PAGES
22, PRICE
PA Form 2220-1 (Rev. 4-77) PREVIOUS EDITION IS OBSOLETE
------- |