EPA7600/R-15/119 UNITEC SENS-IT cience Citize Operating Procedure Office of Research and Development National Exposure Research Laboratory ------- EPA/600/R-15/119 | May 2015 | www.epa.gov/ord UniTec Sens-It Citizen Science Operating Procedure Ron Williams National Exposure Research Laboratory Office of Research and Development U.S. Environmental Protection Agency Research Triangle Park, NC, USA 27711 Amanda Kaufman ORISE Participant Oak Ridge Institute for Science and Education Oak Ridge, TN, USA 37831 Sam Garvey Alion Science and Technology Research Triangle Park, NC 27709 ------- CITIZEN SCIENCE Contents UniTec Sens-It 1 What Are VOCs? 1 What You Will Need 1 Data Acquisition System 1 I mportant Considerations 2 Preparing the Device 2 Making the Connections 2 Installing the Software 4 Configuring the Sampling Parameters 4 Routine Data Collection 7 Recording Data 7 Processing Data 8 For Additional Help 9 ------- ------- CITIZEN SCIENCE UniTec Sens-It The UniTec Sens-It is a small gas-sensing device that can measure volatile organic compounds (VOCs). This sensor is used to measure VOCs in applications such as urban air quality, roadside pollution, and (solid waste) landfill monitoring. This operating procedure explains what you need to do to collect high-quality VOC data using the Sens-It for your monitoring project. What Are VOCs? VOCs are common pollutants in both indoor and outdoor environments. VOCs are emitted as gases from many common household and office products including paints, floor wax, cleaning supplies, cosmetics, pesticides, building materials, home furnishings, copiers and printers, permanent markers, and glues and adhesives. Automotive fuels are also made up of organic chemicals, increasing VOC concentrations near roadways and urban areas. All of these products and sources can release organic compounds during use and sometimes during storage. These VOC compounds can have both short- and long-term adverse health effects. What You Will Need *I* UniTec Sens-It <* 12 volt (V) power supply *** Data acquisition (Daq) hardware (see below)—this operating procedure assumes use of a Personal Daq/55 (lOtech, Inc., Cleveland, OH) <• Personal computer (PC) system <* USB (Universal Serial Bus) cable Data Acquisition System A data acquisition system measures electrical or physical conditions—such as voltage, current, temperature, and pressure—and stores the information in digital form for analysis. Typically, signals from sensors are recorded, converted to digital information, and stored by a computer. The data acquisition system therefore consists of a sensor, data acquisition and measurement hardware, and a computer with programmable software. This procedure assumes the use of an lOtech Personal Daq/55 data acquisition module connected to the UniTec Sens-It and to a PC running a Windows 95 or higher operating system. By way of example, we have also included measurements of relative humidity (RH), temperature, and pressure in this procedure. The Personal Daq/55 uses DaqView software, which you will need to install on the PC before collecting data. If you are using other data acquisition hardware, procedures should be similar, but it is recommended that you consult your data acquisition module User's Manual for details of your specific configuration. ------- CITIZEN SCIENCE Important Considerations *!» The UniTec Sens-It is delivered already calibrated by the manufacturer. However, the UniTec Sens-It requires semi-annual (twice per year) calibration to function properly. The unit should be returned to the manufacturer for this service. *t* According to the manufacturer, the UniTec Sens-It sensor is not designed for indoor use, and its use indoors could lead to unreliable response and/or loss of calibration. *I* The UniTec Sens-It is 'powered-on' as soon as it is connected to the power source. To turn the unit off, simply disconnect it from the power source. The manufacturer recommends the UniTec Sens-It remain on, once operation begins, to prevent loss of calibration. If the sensor is left off for more than one day, let it run for 24 - 48 hours to stabilize. *J* The manufacturer notes that vapors from silicone rubber, bitumen, and oil-based paint can interfere with normal sensor operation. Carefully assess the sensor's surrounding environment before collecting data and consider using protective housings of materials such as steel or unpainted aluminum. Preparing the Device Making the connections To collect data with the UniTec Sens-It, you first need to connect the device to a 12 V DC power supply and to a data acquisition module, commonly called a data logger, which will record the measurements. This procedure uses a Daq/55 data logger. The Daq/55 uses a USB cable for data collection (Figure 1). A single cable to a PC provides high-speed communication and power to the Daq/55. Use the four colored wires, shown in Figure 2, to connect the com- ponents as shown in Figure 3. Figure 1 ------- CITIZEN SCIENCE Gray: data logger Green: +V out Brown: +12 V DC power supply Gray: data logger ground Green: +Vout Temperature/ humidity/ pressure meter Brown: +12 V power supply Figure 3 ------- CITIZEN SCIENCE Installing the Software The only software required for monitoring VOCs with the UniTec Sens-It is the Personal DaqView software that operates the Daq/55 data acquisition module. This software must be installed on a computer that meets the following requirements: *J* PC with Pentium® processor and available USB port »> Microsoft Windows 95, version 4.00.950 b with USB supplement to OSR2.1, at a minimum (Note: Windows 98 or higher is strongly recommended) *!* 16 MBytes (Megabytes) of Random Access Memory (RAM) (Note: 32 MBytes or greater is recommended) *J* 'Energy Save' mode is disabled Procedure: Install Software 1. Insert the Personal DaqView software CD into the PC's CD-ROM drive and wait for the PC to automatically access the CD. 2. Select 'Personal Daq Support' from the Data Acquisition Software Master Setup screen. 3. Click'Start Install'. 4. When installation is complete, select the "Exit viewing Readme file" radio button for important information not available elsewhere. 5. Exit the program. 6. Remove the CD. 7. Shutdown the PC. Configuring the Sampling Parameters Sampling parameters must be specified in the Personal DaqView software before beginning data collection. In Windows, double click the 'Personal DaqView' icon to open the software. Once the program is running, the software will automatically identify the UniTec Sens-It and bring up the main control window (Figure 4). File View Acquire Device Joels indicators Help 4 ------- CITIZEN SCIENCE Procedure: Configure Channels 1. Click the 'Configure Channel Settings' button (<,§;) on the main control window toolbar, which will open the Channel Configuration window (Figure 5). (Note that the example also shows settings for humidity, temperature, and pressure.) 2. On the Analog Input tab, set Scale to 1.0 and Offset to 0.0 by double clicking in each field. 3. Press the Play button ( >) at any time during recording to update the Reading field in real time with the data from each channel. Control > i Analog Input | Frequency/Pulse Input Digital Input/Output p, i Usei Labei On H6c PD1 A01L UniTecSenslT On PD1 A01H Off pDi.Aoa. off PD1.A02H OH PD1_A03l RH On PD1.A03H Temp On PD1_AQ4L Piess On PD1 A04H Off PD1 A05L Off PD1 A05H Off ding Range Ur •10.0to10.0 V •100.010100,0 V •100 Olo 100.0 V •250to2SO V tf Single-ended/ Measi. Differential Dm Single-ended 110ms Single-ended 110ms Single-ended 110ms Single-ended 110ms "Jj™f* Scale Offset 1.0 00 10.0 0.0 10.0 0.0 10.0 00 Procedure: Configure Data Acquisition 1. Click the 'Configure Acquisition' button ((§)) on the main control window toolbar. 2. Select the 'Trigger' tab (Figure 6) and set Source to Immediate using the pull-down menu. 3. In the Averaging section of the screen, use the pull-down menu to set 'Type' to 'Block Average' and 'Count' to '32' as shown. This means that averages will be calculated and recorded for each block of 32 measurements. 4. Set 'Scan Rate' in the 'Acquisition Parameters' section of the same screen to '1.875 sec'. This will result in a text file being updated every minute with an average of 32 immediate measurements taken 1.875 seconds apart. ------- CITIZEN SCIENCE 5. Under the 'Post-Trigger" tab (Figure 7), use the pull-down menu to set 'Stop On' to 'Duration'. Then set 'Duration' to '1440 Scans'. This will create a text file that stops updating after 1440, 1-min measurements, or 24 hours. Configure Ac Pre-T rigger J figger || Posl-T rigger Source: j Immediate Channel: F Condition: |Rising Threshold: Hysteresis: Figure 6 Averaging Type: Count: Block Average *\ \32 Acquisition Parameters Min. Period: 0.858 sec Max. Period: 1500.000 sec ScanRate: | 1.875 ^j sec l~~ Continuous Calibration (• Period ^ Overrange Protection : Frequency J Cancel Trigger ! Post-Trigger Pre-Trigger Stop On: | Duration Duration: \ 1440 ; Scans Figure 7 Averaging Type: Count: | Block Average Vj J32 _-J Acquisition Parameters — Min. Period: 0.858 sec Max. Period: 1500.000 sec Scan Rate: f 1.875 "Hfsec Continuous Calibration V Overrange Protection <* Period 1 Frequency UK. | Cancel Procedure: Configure Data Destination 1. Click the 'Configure Data Destination' button (®) on the main control toolbar. 2. In the Configure Data Destination window (Figure 8), assign a Folder where you want the data to be stored. 3. Create a File name to contain the data. 4. Use the 'Auto Rearm' feature to create a sequence of text files so that recording of data will continue with the creation of a new file after the Stop On duration set in step 5 of Configure Acquisition has been reached. Each file created using Auto Rearm will have a number appended to the end of the file name that indicates its position in the sequence as shown in Figure 8. ------- CITIZEN SCIENCE Configure Data Destination Folder: | C: \Program Files\pDaqView WpplicationsSDATAWS Cl I \ File' D265 05-31 -13.BIN Browse... Conversion Formats F i Q LJ r6 8 w ^^^^^^^^^^^^^^^H . ^^^^^^^^^•1 17 Auto Rearm Starting Index: | 0 ^Tj S tailing File: D 265 05-31 -1 3_0. B 1 N Ending File: D265Q5-31-13_99.BIN li OK il Cancel Routine Data Collection Once the data logger is properly connected to the PC and the UniTec Sens-It, the system is ready to begin collecting data. Recording Data The Personal Daq/55 records the signals received from the UniTec Sens-It as voltage (V) in a text file that can be transferred easily to spreadsheet software for simple processing. The Daq/55 records time, date, and the output of any sensors connected to it, including VOC concentration from the UniTec Sens-It, measured in volts, as 1-min averages (Figure 9). The values for each property (e.g., time, date, etc.) are separated, or 'delimited', by tabs. Any non- alphanumeric character can be used to separate the values, but the most common delimiters are the comma, tab, and colon. Most spreadsheet programs are able to read data from a text file in a delimited format. If you are using a data acquisition module other than the Daq/55, consult the User's Manual for the delimiter character used by your system to separate data. Time 13 13 13 13 13 13 13 13 13 13 13 13 13 13 3L3 :19 :20 :21 :22 :23 :24 :25 :26 :27 :28 :29 :30 : 31 :32 ^^ :17 :17 :17 :17 :17 :17 :17 :17 :17 :17 :17 :17 :17 :17 ^^^^_ Figure 9 Date 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 4/7/2014 UniTecSenslT V 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 3. 9842416-001 9646816-001 9388296-001 9215066-001 9116176-001 9047386-001 8977466-001 8940536-001 8857996-001 8857276-001 8776906-001 8743706-001 8739676-001 8769126-001 8838636-001 8858106-001 8881316-001 RH V 4. 5. 4. 4. 4. 4. 4. 4. 4. 4. 5. 5. 5. 4. 5. 5. 5. 9982646+001 0004216+001 9993026+001 9967276+001 9938426+001 9953386+001 9973906+001 9980326+001 9977956+001 9993526+001 0006746+001 0003886+001 0014286+001 9984336+001 0000316+001 0002156+001 0007766+001 Temp V 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 2. 5376506+001 5375796+001 5378836+001 5392926+001 5398646+001 5388656+001 5378756+001 5378276+001 5377986+001 5365876+001 5362616+001 5358476+001 5356626+001 5362916+001 5355196+001 5356226+001 5350426+001 Pressure V 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 5. 7524916-001 7426206-001 7681036-001 7459316-001 7471806-001 7468346-001 7441786-001 7468566-001 7504986-001 7488736-001 7471196-001 7500396-001 7517616-001 7498736-001 7531616-001 7513336-001 7507686-001 ------- CITIZEN SCIENCE Procedure: Acquire Data 1. In Windows, double click the 'Personal DaqView' software icon to open the software. 2. Using the main control toolbar, ensure all sampling parameters are properly configured for channel, acquisition, and data destination as described above. 3. Click the record button ( jy) on the toolbar to begin recording data. Data acquisition will continue until the sequence specified using Auto Rearm is complete. Processing Data To process the data collected from the UniTec Sens-It, you will need to transfer the text file created by the data logger into a spreadsheet. When using the Daq/55, data are stored as tab- delimited text files that can be imported into a spreadsheet. We have assumed the use of Microsoft Excel spreadsheet software for this procedure. Procedure: Process Data 1. Open a new Microsoft Excel spreadsheet and select Data > Get External Data > From Text. 2. When prompted, use Windows Explorer to navigate to the folder containing the text file previously specified in the 'Configure Data Destination' window. 3. When prompted, in the next screens select 'Delimited' and 'Tab-delimited'. 4. Press 'Finish' to display the data in columns in the Excel spreadsheet (Figure 10). m B *> - IJ HOME ""OFD Clipboard r; INSERT PAGE LAYOUT FORMULAS DATA REVIEW VIEW Calibri * |ll B I U - 83 - • A" ft-.fi Font A2 1 Time 2 3 13 4l 13 5 13 6 7 8 9 10 11 12 13 14 15 16 13 13 13 13 13 13 13 13 13 13 13 17 13 18 13 • ~^ B Date f. A' - = = «" ee tjf Wrap Text ^ Merge & Center - r; Alignment r; UniTecExceUn - E DEVELOPER General $ - % . | -S8 , Number c UniTecSensIT V 19:17 4/7/2014 20:17 4/7/2014 21:17 4/7/2014 22:17 4/7/2014 23:17 4/7/2014 24:17 4/7/2014 25:17 4/7/2014 26:17 4/7/2014 27:17 4/7/2014 28:17 4/7/2014 29:17 4/7/2014 30:17 4/7/2014 31:17 4/7/2014 32:17 4/7/2014 33:17 4/7/2014 34:17 4/7/2014 3.98E-01 3.96E-01 3.94E-01 3.92E-01 3.91E-01 3.90E-01 3.90E-01 3.89E-01 3.89E-01 3.89E-01 3.88E-01 3.87E-01 3.87E-01 3.88E-01 3.88E-01 3.89E-01 D RH V 5.00E+01 5.00E+01 5.00E+01 5.00E+01 4.99E+01 5.00E+01 5.00E+01 5.00E+01 5.00E+01 5.00E+01 5.00E-I-01 5.00E+01 5.00E+01 5.00E+01 5.00E+01 5.00E+01 E Temp V 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 2.54E+01 F Pressure V 5.75E-01 5.74E-01 5.77E-01 5.75E-01 5.75E-01 5.75E-01 5.74E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 5.75E-01 Figure 10 ------- CITIZEN SCIENCE For Additional Help Sens-It Installation Guide, UniTec Sri, www.unitec-srl.com, last accessed May 13, 2015. Personal Daq/50 Series: USB Data Acquisition Modules, User's Manual, lOtech, Inc., 25971 Cannon Road, Cleveland, OH 44146-1833, http://www.mccdaq.com/PDFs/manuals/personal daqSO series.pdf, last accessed May 13, 2015. The purpose of this document is to provide general operating guidelines and the U. S. Environmental Protection Agency (EPA) does not assume any liability regarding any aspect of its use. Reference herein to any specific commercial products, process, or service by trade name, trademark, manufacturer, or otherwise, does not necessarily constitute or imply its endorsement, recommendation, or favoring by the EPA. The views and opinions of authors expressed herein do not necessarily state or reflect those of the EPA, and shall not be used for advertising or product endorsement purposes. The EPA assumes no liability associated with any errors in the suggested procedures, errors potentially made by the instrument in questions, user misuse of the instruments or data collected, or costs due to any damage the instrument might experience under any circumstance or use. This user guide is specific to the make/model, and version number of the instrument identified in the document and is not generalizable to any other sensor. The users should understand that they should develop operating guidelines specific to their own research needs and any general document of this nature would be limited in meeting their full need. ------- ------- x>EPA United States Environmental Protection Agency PRESORTED STANDARD POSTAGE & FEES PAID EPA PERMIT NO. G-35 Office of Research and Development (8101R) Washington, DC 20460 Official Business Penalty for Private Use $300 "V Recycled/Recyclable Printed on paper that contains a minimi 50% postconsumer fiber content processed chlorine free minimum of ------- |