FINAL REPORT
on
COAL CLEANING PREPARATION PLANT EMISSIONS
AT WESTMORELAND COAL COMPANY,
QUINWOOD, WEST VIRGINIA
to
ENVIRONMENTAL PROTECTION AGENCY
May 14, 1976
by
P. R. Webb, J. M. Pilcher, and J. A. Gieseke
BATTELLE
Columbus Laboratories
505 King Avenue
Columbus, Ohio 43201
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TABLE OF CONTENTS
INTRODUCTION 1
SUMMARY AND DISCUSSION OF SAMPLING RESULTS -. . 5
Particle Size Results . 5
Process Coal Sieve Results. 5
Particulate Collected by the Scrubber 7
Cyclone Catch Analyses 17
Scrubber Inlet Measurement Results. . . 24
Scrubber Outlet Results 24
Total Solids in Scrubber Outlet Water 29
Opacity Measurements 30
Data Applicable to All Five Runs 39
Trace Metal Results 41
LOCATION OF SAMPLING POINTS ... 41
Inlet to Venturi Scrubber 41
Outlet of Mist Eliminator . . . 44
PROCESS DESCRIPTION AND OPERATION ... ..... 47
Process Description ..... 47
Emission Control Equipment. 49
Process Operation 49
SAMPLING AND ANALYTICAL PROCEDURES. ............ 51
Coal Sample Collection Method. . 51
Scrubber Water Collection 53
Particle Sizing Methodology 55
Distribution Change Due to Drying 56
Effect of Ultrasonic Dispersion Compared Vith
Mechanical Dispersion 56
Ultrasonic Cleaning of Alundum Thimble 59
Relative Comparison—Particle Concentration ... 62
Representative Aliquots From Large
Electrolyte Volumes 63
Coal Particle Solubility 63
REFERENCES. 65
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TABLE OF CONTENTS
(Continued)
Page
APPENDIX A
COMPLETE PARTICUIATE RESULTS A-l
Sample Calculations--0utlet Run No. 4 A-6
APPENDIX Bl
VISIBLE EMISSIONS OBSERVATIONS DURING PARTICUIATE SAMPLING ... Bl-1
Summary and Discussion of Visible Emissions Bl-1
Method 9 Report Bl-3
APPENDIX B2
TOTAL VISIBLE EMISSION DATA B2-1
APPENDIX C
FIELD AND LABORATORY DATA RELATED TO PARTICUIATE SAMPLING ... C-l
Preliminary Data C-l
Sample Run Data C-7
Molecular Weight Calculations C-28
Field Analytical Data C-34
Sample Drying Data C-46
Visible Emission Field Data C-75
Cyclone Field Data C-166
APPENDIX D
SAMPLE COLLECTION LOG D-l
Sampling Task Log D-4
APPENDIX E
PROCESS OPERATION FIELD DATA E-l
APPENDIX F
SAMPLE IDENTIFICATION LOG F-l
APPENDIX G
CYCLONE SAMPLE LOG AND ANALYTICAL RESULTS G-l
APPENDIX H
DIAGRAM OF SAMPLE EQUIPMENT SERIES CYCLONES INCLUDING
CALIBRATION DATA H-l
APPENDIX I
DETAILED STANDARD SAMPLING AND ANALYTICAL PROCEDURES 1-1
Particle Size Analysis by Mine Safety
Appliance Particle Size Analyzer 1-4
LL
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TABLE OF CONTENTS
(Continued)
APPENDIX J
PROJECT PARTICIPANTS AND TITLES J-l
LIST OF TABLES
Table 1. Sieve Analyses of Coal Samples From West-
moreland Coal Company ..... 5
Table 2. Subsieve Particle Distribution of Westmoreland
Coal Company Samples by MSA Particle
Size Analyzer 8
Table 3. Size Distribution Comparison of Thimble
Catches and Scrubber Water Suspension by Coulter
Counter(From Westmoreland Coal Company 16
Table 4. Test Data 18
Table 5. Analytical Data For Particle Size Runs With
Multiple-Cyclone Sampler. ._.. . _. . ,_ 19
Table 6. Summary of Results of Particle Size Runs 20
Table 7. Inlet Measurement Results Summary (English Units) 25
Table 8. Inlet Measurement Results Summary (Metric Units). 26
Table 9. Outlet Measurement Summary Results
(English Units) 27
Table 10. Outlet Measurement Results Summary (Metric Units) 23
Table 11. Scrubber Water Analysis 29
Table 12. Frequency Observation Averages Exceeding Stated
Opacity for Particulate Sampling Only 31
Table 13. Frequency Observation Averages Exceeding Stated
Opacity for Total Opacity Data 3"2
Table 14. Opacity Observation Summary . 40
Table 15. Optical Emission Spectroscopy Analysis for
Trace Metals (Run No. 4) 42
Table 16. Traverse Port Locations—Inlet 45
Table 17. Traverse Port Locations—Outlet 46
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LIST OF TABLES
(Continued)
Page
Table 18. Production Rates (June 25, 1975). ......... 50
Table 19. Particles Generated From Ultrasonic Thimble
Cleaning, Coulter Counter Analyses 61
Table A-l. Inlet Results A-l
Table A-2. Outlet Results. A-3
Table A-3. Orsat Gas Composition Measured at Outlet Stack-
Westmoreland Coal Company, Quinwood, West Virginia. A-5
LIST OF FIGURES
Figure 1. Process Coal Sieve Analysis , 6
Figure 2. Subsieve Size Distribution of Process Coal by
Coulter Counter 9
Figure 3. Subsieve Size Distribution of Process Coal by
Mine Safety Appliance Particle Size Analyzer ... 10
Figure 4. Comparison of Run 2 Thimble Catch and
Associated Scrubber Water Suspension, Coulter
Counter Analyses ........ ... 12
Figure 5. Comparison of Run 4 Thimble Catch and
Associated Scrubber Water Suspension, Coulter
Counter Analyses 13
Figure 6. Comparison of Run 5 Thimble Catch and
Associated Scrubber Water Suspension, Coulter
Counter Analyses .......... 14
Figure 7. Comparison of Run 6 Thimble Catch and
Associated Scrubber Water Suspension, Coulter
Counter Analyses 15
Figure 8. Particle Size Distributions of Cyclone Catches
Coulter Counter Analyses 22
Figure 9. Sample Point Location. ..... 23
Figure 10. Opacity Observation Sites. . . 33
Figure 11. Run No. 1 Opacity Results as a Function of
Time of Day. 34
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LIST OF FIGURES
(Continued)
Page
Figure 12. Run No. 2 Opacity Results as a Function of
Time of Day 35
Figure 13. Run No. 3 Opacity Results as a Function of
Time of Day 36
Figure 14. Run No. 4 Opacity Results as a Function of
Time of Day. 37
Figure 15. Run No. 5 Opacity Results as a Function of
Time of Day. . 36
Figure 16. Inlet Stack Special Adapter With Gate Valve
Showing Position of Alundum Thimble Prior
to Sampling 43
Figure 17. Inlet Stack Geometry Showing Sampling Location
and Sample Point Configuration 45
Figure 18. Outlet Stack Geometry Showing Sampling Location
and Sample Point Configuration . 46
Figure 19. Exhausting-Type Fluidized-Bed Thermal Coal Dryer,
Showing Component Parts and Flow of Coal and
Drying Gases, Westmoreland Coal Company, Imperial
Smokeless Division, Quinwood, West Virginia ... 48
Figure 20. Coal Sample Collection Method 52
Figure 21. Schematic of Venturi Scrubber Water Flow System. . 54
Figure 22. Distribution of Dried and Undried Coal Samples
From a Thimble Catch, Coulter Counter Analyses . . 57
Figure 23. Comparison Distribution of Wet and Dry Sieved
Process Coal Samples 58
Figure 24. Comparison of Ultrasonic and Medicine Dropper
Dispersion Techniques, Coulter Counter Analyzer. . 60
Figure 25. Representative Aliquot Check of Large Solution
Volume Having High-Particle Density, Coulter
Counter Analyses 64
Figure H-l. Series Cyclone Sampling Apparatus Block
Diagram H-l
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LIST OF FIGURES
(Continued)
Figure H-2. Cut-off Point Versus Flow Rate Calibration
Curves for EPA Series Cyclone H-2
Figure H-3. Cyclone Collection Efficiency Calibration
Data H-3
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COAL CLEANING PREPARATION PLANT EMISSIONS
AT WESTMORELAND COAL COMPANY,
QUINWOOD, WEST VIRGINIA
by
P. R. Webb, J. M. Pilcher, and J. A. Gieseke
INTRODUCTION
In accordance with Section 111 of the Clean Air Act of 1970,
the Environmental Protection Agency is charged with the responsibility
of developing standards of performance for emissions from new stationary
sources (New_Source Performance Standards) which may contribute signi-
ficantly to air pollution, A standard of performance developed under
the Act for emissions of air pollutants must be based on the best emission
reduction systems that have been adequately demonstrated, taking into
account economic considerations.
The development of standards of performance utilizes emissions
data for pollutant sources in the particular industry being studied. In
response to comments on the proposed emission standards by the coal clean-
ing industry, the emission control systems (venturi scrubbers) of the
Westmoreland Coal Company, Quinwood, West Virginia, were selected by
IPA for an emission testing program to provide test data by which the
effectiveness of that emission control system could be compared with other
facilities previously tested.
The Westmoreland Coal Company contested the proposed standards
as a result of their preliminary tests which indicated that their specific
type of coal could present an emissions control problem not previously
considered by EPA. The Westmoreland data implied that the particle size
of the particulate matter entering the venturi scrubber device was finer
than had previously been acknowledged. The data indicated that one type
of coal (Sewell) processed at the Quinwood plant presented different size
characteristics than coal on which the proposed standards were based.
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In order to adequately evaluate these allegations, EPA decided to conduct
an extensive test program at the Quinwood facility.
Coal delivered to the plant is crushed to a variety of sizes and then
washed, screened, and separated by both water and concentration tables.
The coal washing occurs in a continuous process which reduces ash content
from 16 to 3 percent. The 0 x 3/8-inch size of coal of interest in this
study is dewatered by vacuum discs, then dried in a fluidized bed. Coal
drying is accomplished by use of flue gas (produced by a coal-fired
furnace) reduced in temperature by dilution air. The fluidized bed is
contained in a chamber loaded with 40 or more tnulticlones which separate
the coal from the fine dusts. Dust particles pass from the multielones
of the dryer through a high-pressure blower to a venturi scrubber, then to
a large mjsi^eiiminator, and finally out an 81-inch-diameter stack.
EPA requested Battelle-Colurabus to: sample particulate and gas-
eous emissions from the inlet and outlet stacks of the venturi scrubber
control device at the Westmoreland Coal Company, Quinwood, West Virginia.
The test program was conducted from June 18, through June 25, 1975
during the times the plant was processing Sewell coal. High mass loading
at the inlet required the use of an in-stack Alundum* thimble (in con-
junction with an EPA Method 5 train). Tests for particle size
distribution of the inlet particulate were made by EPA utilizing a special
multilpe-cyelone sampler. Grab samples of the process coal and ven-
turi scrubber water were taken simultaneously with the particulate and
gaseous measurements. The purpose of the aforementioned measurements
is to provide EPA with additional data for support of their standards
development efforts.
In order to evaluate the effect of particle size on the venturi
scrubber equipment it was necessary to determine the particle size dis-
tribution of the particulate matter entering the scrubber for each type
coal. Particle size comparison by sieve analysis was conducted on both
types of process coal (Sewell and Pocahontas). Particle sizes of the sus-
pended particulate at the scrubber inlet, suspended particulate in the
* Mention of trade names does not constitute endorsement or recommendation
for use by the Environmental Protection Agency.
-------
scrubber water, and <325 mesh process coal from the sieve analysis were
determined by Coulter Counter^ . A Mine Safety Appliance Particle Size
Analyzer^ was also used to determine the particle size of the <325 mesh
particulate in an effort to substantiate the test results as determined
by Coulter Counter. Particle size data, as presented in the figures
throughout this report , were determined from one aliquot per sample unless
otherwise noted.
Since the effectiveness of the venturi scrubber was in question rel-
ative to the process coal particle size, additional effort was placed on
determining venturi inlet particulate size distribution. A special IPA
series cyclone was used to futher evaluate the size cut of the inlet
particles.
Trace metals in Run No. 4 outlet emission samples were determined by
optical emission spectroscopy.
Present opacity of the outlet stack emissions was monitored by two
certified observers during the particulate sampling. The test program
was conducted to determine mass concentration levels and size distribu-
tions of particulate emissions during normal plant operation. Process
conditions were carefully observed and tests were performed only when the
process operations appeared to be operating normally. Process and/or
scrubber malfunctions occurred during Runs 2, 3, and 5 at which time the
particulate sampling was terminated. Opacity readings continued through-
out the entire period including times when high values were observed
because of scrubber malfunction.
A total of five outlet and six inlet runs were made for particulate
loading. Run No. 1 inlet was voided due to incorrect (Pocahontas) coal
being processed. Run No. 2 outlet was not considered valid due to an open
circuit in the probe heater and a leak in the filter which allowed some
particulate to pass through into the impinger catch. Run No, 3 inlet was
voided due to nonrepresentative sampling caused by incorrect placement of
the sampling nozzle and, therefore, incorrect sampling point location.
Inlet Runs No. 4, 5, and 6 and outlet Runs 3, 4, and 5 were essentially
References are given on page 65.
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simultaneous and considered valid. The following sections of this report
cover the summary of results, process description and operation, location
of sampling points, and sampling and analytical procedures.
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SUMMARY AND DISCUSSION OF SAMPLING RESULTS
Particle Size Results
Process Coal Sieve Results
The effectiveness of a venturi scrubber is, among other factors,
related to the particle size of the effluent to be scrubbed. To better
understand and evaluate the final outlet emission results of this study
it is pertinent to obtain a size distribution of the bulk process coal.
Figure 1 graphically depicts the sieve analysis results of two types of
coal processed by the Westmoreland Coal Company. (Run No. 1 is probably
an unknown composite of both Sewell and Pocahontas types of coal.) The
size distributions of the Sewell process coal used during outlet Runs 3,
4, and 5 show very good agreement. As indicated, the Sewell coal has a
mass mean diameter of 1000 \IM with approximately 3 to 4 percent being less
than 325 mesh (44 urn). The Pocahontas coal, as indicated in Figure 1,
is relatively smaller than the Sewell coal having a mass mean diameter
of 250 iua, but with approximately 4 percent being smaller than 325 mesh.
Table 1 is a tabular summary of the Sewell and focahontas sieve analysis
data.
TABLE 1. SIEVE ANALYSES OF COAL SAMPLES FROM
WESTMORELAND COAL COMPANY
Sieve Size
U.S. Sieve Screes Opening,
tfeffiixtf nan
4
8
16
30
50
100
200
325
Pan (-325)
4,760
2,380
1,190
590
297
149
74
44
<44
Far tie le Size
Range Collected
per Stage, IIB
>4760
2380-4760
1190-2380
590-1190
297-590
149-297
74-149
44-74
<44
Accumulative Weight-
percent Retained per
Stage and Smaller Stages
Run 1
100.0
90.3
72.5
54.0
38.5
25.2
^ 16.7
10.8
3.7
Rim 3
100.0
92.9
75.8
57.5
41.7
27.9
17.9
11.6
3.1
Run 4
100.0
91.0
72.4
53.4
38.2
25.7
17.1
11.3
2.9
Run 5 Pocahoucaa
99.9
91.S
73.1
53.9
38.3
25.2
16.4
10.S
3.9
100. 0
97.8
92.5
84.2
. 72.2
54.9
36.4
21.8
4.0
Note£ Rua No. 2 discarded
(a) Sample a lie approximately 900 grama* (2" Ib)
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98
95
90
80
70
6O
50
JC
"5
§
o>
3
E
3
u
jr
30
20
10
5
2
1
0.5
o
O Run 1
^ Run 3-i
4. Run 4
rv Run 5—'
Pocohantus1
Composite
Sewell ~
O.2
0.1
20
30 40
60 80 100
200 300 400 6OO 800 K3OO
Particle Diameter, micrometers
2000 3OOO 5000
FIGURE 1. PROCESS COAI, SIEVE ANALYSIS
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In order to evaluate the proportion of ultrafines (<2 yja) that is
of primary importance relative to venturi scrubber effectiveness, Coulter
Counter analyses of the subsieve fraction (<325 mesh) were performed for
the indicated runs. The results are shown in Figure 2, Again the size
distribution for the Sewell coal for outlet Runs 3, 4, and 5 show good
agreement, the mass mean diameter being approximately 17 pa and approxi-
mately 1 to 2 percent being less than 2 tun. The Focahontas coal has
more fines than the Sewell coal, with a mass mean diameter of approximately
12 \IM and approximately 2.5 to 3 percent being less than 2 i_un. Therefore,
with all other factors equal, the Sewell coal emissions are no more dif-
ficult to collect with venturi scrubber equipment than the Focahontas coal
emissions.
The Mine Safety Appliance Particle Size Analyzer results as depicted
»
in Figure 3 essentially substantiate the Coulter Counter results for the
Sewell samples but shows the Focahontas and Sewell with essentially an
equal size distribution except in the relatively smaller size fractions
where scatter in the data occurs. If one averages the MSA data in the
smaller size fraction, 2 to-3 percent of the size distribution is less
than 2 yjnj this agrees with the Coulter Counter data of Figure 2. Table
2 is a tabular summary of the Sewell and Focahontas results for size
measurements with the MSA Particle Size Analyzer.
Particulat^ Collected by the Scrubber
It is to be expected that the venturi scrubber used to clean partic-
ulate from the effluent gas stream will remove large particles more
efficiently than smaller particles. To directly measure such effects,
mass concentrations and size distributions are required for particles in
the gas stream entering the scrubber and in the scrubber water. Because
of the time averaging effect of scrubber water recirculation, a direct
measurement of particulate mass collected in the water over the inlet
gas sampling time was not possible. The scrubber water samples were col-
lected over a very short time interval and, hence, a time averaged value
for the particulate collected by the water prior to the sampling time
was determined.
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TABLE 2. SUBSIEVE PARTICLE SIZE DISTRIBUTION OF WESTMORELAND
COAL COMPANY SAMPLES BY MSA PARTICLE SIZE
ANALYZER(a)
Particle
Size, \m
60
50
40
35
25
20
15
12
10
8
6
4
2
1
0.8
Weight Percent of
Run 1
*• •
100.0
98.1
97.1
79.2
63.3
43.7
33.1
26.8
18.5
12.2
5.3
1.3
0
—
Run 3
*M <•»
100.0
97.6
95.3
79.2
63.4
46.7
31.9
25.8
22.5
15.5
6.4
0.7
0
--
Run 4
•>•
100.0
97.1
94.9
76.1
62.5
47.5
39.1
29.4
21.3
12.9
9.2
5.9
0
--
<44 pm Portion^)
Run 5
<•>«»
_-
100.0
97.2
78.3
65.0
48.3
38.5
30.8
21.7
14.0
8.4
4.9
0.7
0
Pocahontas
100.
97.
93.
91.
73.
57.
42.
32.
25.
17.
9.
4.
1.
0
--
0
5
7
2
3
5
9
9
0
1
6
6
3
Weight Percent of Total Sample^)
Run 1
« «•
3.70
3.63
3.59
2.93
2.34
1.62
1.22
0.99
0.68
0.45
0.20
0.05
0
—
Run 3
•»>•»
3.10
3.03
2.95
2.46
1.97
1.45
0.99
0.80
0.70
0.48
0.20
0.02
0
_-
Run 4
«M «M
2.90
2.82
2.75
2.21
1.81
1.38
1.13
0.85
0.62
0.37
0.27
0.17
0
—
Run 5
— —
—
3.90
3.79
3.05
2.54
1.88
1.50
1.20
0.85
0.55
0.33
0.19
0.03
—
Focahontaa
4.00
3.90
3.75
3.65
2.93
2.30
1.72
1.32
1.00
0.68
0.38
0.18
0.05
0
__
Note; Run No. 2 discarded.
(a) Sedimentation liquid—iaopropy1 alcohol; feed liquid—50 percent isopropyl alcohol, 50 percent heptane.
(b) Data are reported as less than indicated size.
o>
-------
O Run
Run 3—
Run 4
-J-Run 5-
Focahontas
0.6 0.8
4 6 8 10 20
Particle Diameter, micrometers
40 60
FIGURE 2. SUlillVE SIZE DISTRIBUTION OF PROCESS COAL
BY COULTER COUNTER
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10
01
9)
Run 4
^ Run 5-1
D Pocahontas
0.6 0.8 i
4 6 8 10 20
Particle Diameter, micrometers
4O 60
FIGURE 3. SUBSIEVE SIZE DISTRIBUTION OF PROCESS""COAL" BY"
. . MINE SAFETY APPLIANCE PARTICLE SIZE ANALYZER
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11
However, the samples were collected to determine if any differences be-
tween inlet suspended particulate and scrubber water particulate existed.
These differences could lead to significant inferences regarding scrubber
collection efficiency as dependent on particle size.
The size distribution curves given in Figures 4, 5, 6, and 7 allow
comparisons between suspended inlet particulate and scrubber collected
particulate for Runs 2, 4, 5, and 6, respectively. Inlet Runs 1 and 3 were
voided as explained in the Introduction. The results may appear to be
inconclusive because of the data in Figures 4 and 5, which show less partic-
ulate below about 2 |j,m in the scrubber water than in the inlet gas, and
Figures 6 and 7, which show the reverse. Table 3 is a tabulation of these
data. Within the error of the particle sizing methods, the data show
that the particle size distribution in the scrubber water is practically
the same as the distribution at the scrubber inlet. This result could
be predicted when the scrubber collects essentially all of the particulate
matter. Data of this type cannot be used to obtain size dependent col-
lection efficiencies. Any major impact on control effectiveness would
occur only if a sufficiently large fraction of the particulate material
had sizes too small for efficient collection. Size distributions for the
suspended inlet particulate indicate that only about 5 percent of the particles
have sizes below about 2 pja. This low fraction in the small size range
makes comparison impractical since the small sizes constitute a nearly
negligible portion of the particulate for measurement purposes. If, how-
ever, the differences between the curves are attributable to normal
scatter in the experimental data, as is likely, it can be concluded that
the overall efficiency is not sensitive to low collection efficiency for
these small sizes. This is because such a small fraction of the total
entering particles are smaller than the size where efficiency drops off.
Therefore, valid conclusions that can be drawn from these data are that
the venturi scrubber essentially collects all sizes of particulate in
excess of 2 y,m. The amount of particulate matter less than 2 micrometers
that reduces the scrubber's collection efficiency is not significantly
different for Sewell coal as compared with Pocahontas coal.
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12
/\ TH-2
Scrubber Water
0.6 0.8 I
4 6 8 10 20
Particle Diameter, micrometers
40 60
FIGURE 4. COMPARISON OF RUN 2 THIMBLE CATCH
AND ASSOCIATED SCRUBBER WATER SUSPENSION,
COULTER COUNTER ANALYSES
-------
13
D TH-4
Scrubber Water
0.6 0.8
4 6 8 10 20
Particle Diameter, micrometers
40 60
FIGURE 5. COMPARISON OF RUN 4 THIMBLE CATCH AND
ASSOCIATED SCRUBBER WATER SUSPENSION,
COULTER COUNTER ANALYSES
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14
QTH-5
Scrubber Water
0.6 as i
4 6 8 10 20
Particle Diameter, micrometers
40 60
FIGURE 6. COMPARISON OF RUN 5 THIMBLE CATCH AND
ASSOCIATED SCRUBBER WATER SUSPENSION,
COULTER COUNTER ANALYSES
-------
15
TH-6
Scrubber Water
O.I
as 0.8 i
4 6 8 10 20
Particle Diameter, micrometers
4O 60
FIGURE 7. COMPARISON OF RUN 6 THIMBLE CATCH AND
ASSOCIATED SCRUBBER WATER SUSPENSION,
COULTER COUNTER ANALYSES
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TABLE 3. SIZE DISTRIBUTION COMPARISON OF PARTICLES ENTERING
THE SCRUBBER AND PARTICLES CAUGHT BY THE SCRUBBER
WATER» WESTMORELAND COAL COMPANY
(Percent lessthan indicated size)
Particle
Size, jim
44.2
35.1
27.8
22.1
17.5
13.9
11.1
8.8
7.0
5.5
4.4
3.5
2.8
2.2
Run
Thimble
Catch
__
--
—
100.0
91.87
91.13
81.52
70.98
63.11
53.00
41.33
28.89
17.68
9.48
2
Scrubber
Water
_-
100.0
94.81
94.29
89.61
85.58
78.11
70.02
60.80
50.43
46.38
29.87
17.67
7.57
Run
Thimble
Catch
__
100.0
98.89
98.34
95.43
91.20
83.37
75.48
66.11
53.83
40.70
26.95
14.82
9.53
4
Scrubber
Water
100.0
97.88
96.82
94.70
91.25
85.94
79.47
70.03
60.75
51.00
38.41
26.71
14.15
5.93
Run
Thimble
Catch
__
—
100.00
98.27
97.11
92.78
86.78
79.04
69.67
57.55
40.95
24.51
12.36
5.54
5
Scrubber
Water
--
—
—
100.00
98.33
93.13
86.47
80.63
71.78
60.53
48.15
34.07
20.47
10.02
Run
Thimble
Catch
--
100.0
97.12
94.26
92.79
85.58
78.42
71.14
61.73
44.97
29.89
16.54
9.03
4.90
6
Scrubber
Water
--
100.0
98.96
93.24
90.90
81.54
74.45
67.52
58.60
48.65
38.03
27.83
14.83
7.61
(a) Size distribution of thimble particle catch and scrubber water particle suspension determined
by Coulter Counter using an aperture diameter of 100 pm, and a manometer volume of 500 P&.
-------
17
Cyclone Catch Analyses
Tests were conducted using a sample train consisting of two aluminum
cyclones followed by a glass fiber filter. The purpose of the tests was
to determine the mass loading of particulates less than 2.5 urn in diam-
eter. All tests were conducted at the inlet to the scrubber. The testing,
cyclones were developed by an independent contractor for the Environmental
Protection Agency. Since the equipment had not been previously used by
the tester, numerous problems were encountered until a sampling technique
was established. A total of 13 runs was conducted. During the first six
runs, problems were encountered with the testing; Runs 7-13 were valid
tests. However, during Runs 8, 10, and 12, the process was operating under
a light load. Furthermore, Run 13 was conducted when Type 7 Sewell sur-
face-mined coal was being processed.
Tables 4 and 5 summarize the test data and analytical data. Table 6
summarizes the test results. The tests were conducted at a nominal flow
rate of 1 acfm, yielding cut-off points of 2.5 and 1.0 pm for the first
and second cyclones, respectively. Therefore, the particulate less than
2.5-pjn diameter was calculated as the total mass minus the mass collected
in the first cyclone.
Two tests with a cascade impactor were attempted, but were not suc-
cessful. In one case, the stages were overloaded, and in the other case,
the collection substrates were knocked ajar.
Table 6 summarizes the test results. As previously noted, Tests 7-13
were considered the best tests as far as sampling procedures are concerned.
In performing the calculations, an average stack gas moisture (9.9 percent)
ftt-if^Jl
calculated from the five Alandum thimble^was used. The results presented in
Table 6 show a reasonable correlation between the Alundum thimble and cyclone
methods for determining particulate concentration of particles less than
2.5 um diameter. For cyclone Runs 7-13 the mass percent less than 2.5 um
ranged from 11.6 to 17.6 percent with an average of 14.5 percent. For
the Alundum thimble Runs 2, 4, 5, and 6, the mass percent less than 2.5 ym
ranged from 7 to 15 percent with an average value of 11.5 percent.
-------
TABLE 4. TEST DATA FOR PARTICLE SIZE RUNS WITH MULTIPLE-CYCLONE SAMPLER
Run
Number
1
2
3
4
5
6
7
8
9
10
11
12
13
Dace
6/18
6/19
6/19
6/20
6/20
6/23
6/23
6/25
6/25
6/26
6/26
6/26
6/26
Start Port
Time Identification
1800
1415
1715
1115
1445
1700
2000
1005
1255
1650
1225
1420
1550
S
S
S
E
E
E
E
E
E
S
S
E
S
Sample
Period
(minutes)
22
10
11
11
11
11
11
11
11
11
11
11
11
Meter
Volume
(aef)
22.345
8.000
10.520
7.230
9.050
8.675
8.600
8.520
8.525
__
7.895
8.600
8.715
Stack
Temp.
(b)
77.8
78.5
78.5
—
85.2
78.1
77.0
(a) Stack conditions.
(b) Used Incorrect sample nozzle.
CD
-------
Test
1
2
3
4
5
6
7
8?
9
10?
11
12?
13?
|
First
Cyclone
__
0.3349
1.7575
3.9237
3.6606
1 . 3006
1.1888
0.5013
1.2658
0.6590
1.6196
1.0512
0 . 5947
1
„ * 1 - 1 vja
fi t"1
. ~ „ £,"
« •»• ••ffrv*
i«*,»i_*i>*i
' -?'*i
:<.;£:
? •*
•> T-flf*
* \ iWft
^'""S
»-«- »y|
Second
Cyclone
_-
N/A
N/A
N/A
2.2320
0.1659
0.1346
0.0535
0.1166
0.0752
0.2217
0.1151
0,0771
TABLE 5. ANALYTICAL DATA FOR PARTICLE SIZE RUNS
WITH MULTIPLE-CYCLONE SAMPLER^*)
Filter
--
0.0620
0.1144
0.1266
0.0229
—
0.0450
0.0278
0,0383
0.0234
0.109
0.000
0.0386
First
Cyclone
Wash
__
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.0060
0.0035
0.0081
0.0059
0.0048
Second
Cyclone
Wash
• «.
N/A
N/A
N/A
N/A
N/A
N/A
N/A
0.0076
0.0062
0.0089
0.0172
0.0098
Filter
Assembly
Wash
w-«
N/A
N/A
N/A
0.0085
—
0.0073
0.0048
0.0048
0.0040
0.0086
0.0070
0.0028
First
Cyclone
Total
__
0.3349
1.7575
3.9237
3.6606
1,3006
1.1888
0.5013
1.2718
0.6625
1.6277
1.0571
0.5995
Second
Cyclone
Total
--
N/A
N/A
N/A
2.2320
0.1659
0.1346
0.0535
0.1242
0.0814
0.2306
0.1323
0.0869
Filter
Total
__
0.0620
0.1144
0.1266
0.0314
--
0.0523
0.0326
0.0431
0.0274
0.1176
0.0070
0.0414
Total
--
0.3969
1.8719
4.0503
5.9241
—
1.3757
0.5874
1.4391
0.7713
1.9759
1.1964
0.7278
(a) All masses are reported in grams.
N/A Not Applicable.
-------
20
TABLE 6. SUMMARY OF RESULTS OF
PARTICLE SIZE RUNS-
Mass Loading, gr/scf
Run Number
Cyclones:
1
2
3
4
5
6
7
8
9
10
11
12
13
Alundum Thimbles:
1
2
4
5
6
Total
--
.84
3.02
9.54
11.13
--
2.73
1.18
2.90
--
4.30
2.39
1.43
2.73
1.79
2.89
3.23
2.67
Less than
2.5 M,m
-------
21
Figures 8 presents the particle size distribution of the cyclone
catches which were analyzed by electronic counter. Field data sheets are
presented in Appendix C. Cyclone sample identification and analytical
results are presented in Appendix G.
Figure 9 indicates the location of the sampling points. Because of
the design of the equipment only the first 22 points on each traverse
could be sampled. Each test (Runs 6-13) was conducted using two cyclones
in series with a back-up filter. The sampling rate was kept constant
during each test at a nominal flow of 1 acfm. Each test was conducted
across only one traverse and was only 11 minutes in duration. It was
necessary to limit each test to only one traverse because of the capaci-
ties of the cyclone collection cups.
Prior to each test the sample train was checked for leaks and then
inserted into the stack (with nozzle plugged) in order to allow the cyclones
to heat to stack temperature. After a 20-minute pre heat, the cyclones
were removed, the nozzle unplugged, the cyclones reinserted, and the test
begun.
The sample train was constructed so that the nozzle was inserted
directly into the first cyclone. The first cyclone was immediately fol-
lowed by the second cyclone and a back-up filter connected to the probe.
During sampling, both cyclones and filter were in-stack. A flexible hose
was used to connect the probe to a silica gel impinger, vacuum pump, and
dry gas meter, in that order. Figure H-l of Appendix H is a block diagram
of the cyclone and filter assembly. Figure H-2 shows the calibration
curves for the cyclones. Figure H-3 shows the calibration curves for each
cyclone and relates the particle cut-off size, yon, as a function of flow
rate.
The particulate catch of each cyclone was emptied from the collection
cup into a weighing vessel. All residual material was brushed into these
vessels using a camel hair brush. In addition, for Runs 9-13, acetone
rinses were conducted on the cyclones and filter holder.
-------
6O.O
Run 2
Run 7
Run 9
Run II
Run8
Run 7
Run 9
Run II
N>
O.OI
0,5 I 2
10
20 30 40 50 60 7O 80 9O
Percent Mass Less Than 0
95 98 99
99.9 99.99
FIGURE 8, PARTICLE SIZE DISTRIBUTIONS OF CYCLONE CATCHES,
COULTER COUNTER ANALYSES
-------
23
South
Port
Traverse points:
1
2
3
4
5
6
7
8
9
10
11
12
1 Inch
2.25
4
5.75
7.5
9.5
11.5
14
16.5
19.5
23.25
28.75
13
14
15
16
17
18
19
20
21
22
*23
*24
East
Port
43.25
48.75
52.5
55.5
58
60.5
62.5
64.5
66.25
68
69.75
71
*Not Sampled.
FIGURE 9. SAMPLE POINT LOCATION
-------
24
For several cyclone catches, the particle size distribution of
the collected material was determined using an electronic counter. The
sizing procedures used were the same as those employed for the Alundum
thimble particulate catches.
Scrubber Inlet Measurement Results
Tables 7 and 8 show computer output tabular summaries (in English
and metric units, respectively) of results of Runs 1 through 6, Run 3 being
aborted because of operator error. Runs 1 and 2 are not considered representa-
tive relative to outlet comparison but are being presented only as support
data to aid in ascertaining a better understanding of inlet sampling conditions.
Weight concentration for Runs 4, 5, and 6 ranged from 2.68 to 3.23 gr/dscf
(6144 to 7407 mg/Nm3 ) resulting in a mean of 2.93 gr/dscf (6728 mg/Nm3 ).
Isokinetic sampling for Runs 4 to 6 varied from 100 to 106 percent, in spite
of the undesirable working conditions encountered, which is well within the
desired limits of 100 * 10 percent for producing valid data.
Scrubber Outlet Results
Tables 9 and 10 show summarized data by computer (in English and metric
units, respectively) obtained at the outlet stack of the Westmoreland Coal
Company. Runs 1 and 2, as previously mentioned, are not considered representative
because of plant and/or BCL operator error, but have been presented as
additional support data.
For Runs 3 to 5, the dry catch (probe and filter) weight con-
centration results are 0.037, 0.059, and 0.035 gr/dscf (86.1, 134.5, and
80.6 mg/Nm3 , respectively. The impinger catch results for Runs 3 to 5
increased the weight concentrations an average of 25 percent, the total
catch (probe, filter, and impingers) being 0.054, 0.072, and 0.049 gr/dscf
(123.2, 164.6, and 112.9 mg/Nm3 ) , respectively.
-------
TABLE 7. INLET MEASUREMENT RESULTS SUMMARY (ENGLISH UNITS)
WESTMORELAND COAL COMPANY INLET RESULTS
RUN NO. ^
TEST OftTE
VOLUME OF GAS SAMPLED, OSCF*b)
PERCENT MOISTJRE BY VOLUME
AVERAGE STACK TEMPERATURE, F
STACK VOLUMETRIC FLOW RATE, DSCFnCc>
STACK VOLUMETRIC FLOW RATE, ACEM^
PERCENT ISOKINETIC
PERCENT EXCESS AIR
PERCENT OPACITY
FEED RATE, TQfJjS/HR
PAPTICULATES - PROBE, CYC, FILTER CATCH
MG
GR/flSCF -
GR/ACF -
LB/HR -
LB/TQN FEED
1
6/ia
•"•••««.i
11.2
166
136913
183212
98.6
1072
NA
ND
— . —
2.729
2.03R
3201.3
ND
2 %
6/19 6/20
BB.8 90. «*
7.0 9.1
16% 171
1%86«Q !%%0%1
19115«5 19Q09<»
q'l.b 100. 0
17B6 2k\l
NA NA
ND ND
9271.0 153ft8.0
1.7B5 2.888
1.3B7 2.187
2273.3 356«».l
ND ND
5
6/23
Y.o.n
10.7
202
138019
193875
106.1
??67
NA
ND
26167.0
3.225
2.29%
3812.9
ND
6
6/25
126.6
12.1
Ifll
135899
18800%
99.7
1595
NA
ND
20QB7.0
2.675
1.93?
311%. 2
ND
(&)
Average^1 '
119.0
10.6
185
137986
190657
101.9
2091
NA
ND
20540.0
2.929
2.138
3497
ND
ND - No Data
,(a) Run No. 3 aborted.
(b) Dry standard cubic feet at 70° F» 29.92 In. Hg.
(c) Dry standard cubic feet per minute at 70° F, 29.92 In. Hg,
Actual cubic feet uer minute.
NA - Not Applicable
in
-------
TABLE 8. INLET MEASUREMENT RESULTS SUMMARY (METRIC UNITS)
WESTMORELAND COAL COMPANY INLET RESULTS
PUN NO.
TEST 3ATF
VOLUME OF GAS SAMPLED, NCM ^
PERCENT MOTSTUPE BY VOLUME
AVFRAGE STACK TEMPERRTUPE, C
STACK VOLUMETRIC FLOW RATE, NCMM^ ' '"
f f,\
STACK VOLUMETRIC FLOW RATE, CMN l '
PERCENT ISDKINETIC
PERCENT EXCESS AIR
PERCENT OPACITY
FEFfl RATE, MTON/HR
PARTICULATFS - PROBE, CYC, FTLTER CATCH
MG
MG/NCM -
MG/CM -
KG/HR -
KG/MTON FEED
124
6/l« 6/19 6/20
3.3 2.5 2.6
11.2 7.0 9.1
7k 73 " 77
386? 1,191, "" £,063
5168 539? 5362
98 .6 94. 6 100.0
107? 1786 2411
NA NA NA
ND ND " " ND
18144.0 9271.0 _ 15368.0
6269.3 4099.4 5634.4
J» 6 BO .7 3 1 8 5 . 7 5 0 22. 5
f 452.1 1.031.2 1616.7
ND ND ND
5
6/23
3.9
10.7
94
"""3893
5469
106.1
2267
NA
ND
26167.0
7«»07.2
5268.2
1729.5
ND
6
6/25
3.6
12.1
B2
3833
5303
99.7
1595
NA
ND
20087.0
6144.3
44 3 7 . 2
1412.6
ND
Average
3.4
10.6
84
3930
5378
101.9
2091
NA
ND
20540
6728.6
4909.3
1586.3
ND
ND - No Data.
(a) Normal cubic meter (dry) 20.0 C, 760 mm Hg.
(b) Normal cubic meter per minute (dry) at 20,0 C, 760 mm Hg.
(c) Actual cubic meters per minute.
NA = Not Applicable
-------
27
TABLE 9. OUTLET MEASUREMENT SUMMARY RESULTS (ENGLISH UNITS)
MESr* iorLft,,a -nf,L rosov?Y 0"TirT Dr5nLTS
/?0 S/23 &/?•>
VOLUME OF GftS StMPLFDt OSCF^ 109.5 100.5 106.7 109.2 10i..O
P€
106.6
12.2
113.3
137629
183457
100.6
2091
19
KD
276.9
0.044
0.033
51.4
ND
" 363.2
0.058
0.044
68.5
ND
" 25.7
ND - No Data. ' ' " "
(a) Dry standard cubic feet at 70° F, 29.92 in. Hg.
(b) Dry standard cubic feet per minute at 70° F, 29.92 in. Hg.
(c) Actual cubic feet per minute.
(d) Average includes only Runs 3, 4, and 5.
(e) Opacity measured only during portion of run.
-------
28
TABLE 10. OUTLET MEASUREMENT"RESULTS SUMMARY (METRIC UNITS)
OUTLET 7FVJLTS
PUN SO.
TEST n.lTF
VOLU*£ Or G1S S&MPLFOt NTM (a)
PEPCFNT H*f)TST'J0E RY VOLUME
AVFRftCF. STOCK TEMPF&&TU9F, C
STftCK V)LUVET°IC FLOW POTE, NCM*i (b)
ST«C< VOLUM^T^IC FLOW 94TF. , CHf^c'
PERCENT rs-
-------
29
Inlet and outlet volumetric flow rates compare reasonably well
when considering the relatively poor inlet sampling location. Insufficient
downstream stack diameters from the inlet sampling location did not allow
sufficient time to establish a uniform flow profile; the end result being
a poor velocity profile which could be a reasonable explanation for the
inlet and outlet volumetric flow rate difference.
Moisture condensation in the outlet stack and reentrainment of water
droplets resulted in the effluent gases being supersaturated and, thus, the
stack gas moisture content of the gases was greater than the moisture cor-
responding to the dew point.
Complete particulate results by computer, which include additional
operational data, and sample calculations for outlet Run No. 4 can be seen in
Appendix A.
Total Solidsin Scrubber Outlet Water
Solids in the scrubber water samples were determined by passing
a 50-ml aliquot of the scrubber water through a tared 45-mm glass fiber filter.
The sample was then dried to a constant weight. Table 11 shows the results
for the indicated runs.
TABLE 11. SCRUBBER WATER ANALYSIS
Outlet
Run Ho.
2
3
4
5
Total Solids,
percent
7.64
8.69
7.74
6.94
-------
30
Opacity. Measurements
Visible emissions were observed by two BCL certified smoke
readers simultaneous with particulate sampling. During the five runs,
opacity values ranged from 10-30 percent. Particulate sampling was
terminated during periods of time when the venturi scrubber was malfun-
tioning. Opacity readings for the most part were taken during all periods.
A complete summary of the data is presented in Appendix B-l and B-2. Tables
12 and 13 are computer summaries of Appendices B-l and B-2 and list the
frequency each observer exceeded the stated opacities.
In order to make it easier to interpret this large amount of
data a graphic presentation of each run has been prepared and is presented
in Figures 11 through 15. Each graph shows the percent opacity as a
function of time of day for the total reading period for each test. Runs
3 and 5 have been divided into A and B sections because of relatively long
interruptions in opacity observations and also to facilitiate computer
data reduction. Also shown on the graphs, by means of horizontal arrows,
are the time periods during which "Particulate Sampling" occurred. These
graphs make it possible to quickly determine the ranges of visible emissions
during particulate sampling times for each of the five test runs. Because
opacity readings were continued when scrubber malfunctions occurred, abnormal
values of visible emissions may have been observed. Emphasis should be
placed only on the visible emission data obtained during particulate sampling.
Figure 11 shows the relative positions of the observation sites with respect
to the outlet stack and adjacent structures. Site B was used for opacity
reading in the mornings and Site A in the afternoons.
-------
TABLE 12. FREQUENCY OBSERVATION AVERAGES EXCEEDING STATED
OPACITY FOR PARTICUIATE SAMPLING ONLY
Run No. 1
Run No. 2
^'tOUiNCV OBSERVE? AV-SiGE Ft.lHEmcy f»S,3tfrf AV* }&<",£
' _x
30 X
25 <
28 X
1 SX
104
5*4
OX
CitOS SIATtO
PLCHQ S"
C
!j
w
3
6
7
7
OPACITY!
IYn»
u
J
2
5
7
7
7
t ji-"\Vi."' A V*- ^ A
»XC-LOS S1AI_1> UFAC1IVI LXoctOS ST4T=1 OPACITfl
PLCH9 SN^3P? " - pj^CH'?" SNVrR"
3cx ""'ID' ' § 3oy. 0— 0 —
25>< it 3 25.4 c 0
20X 17 17 - 2C'/. ' 0 " "•" 3 ~
- - - - — - _ ....
15< *8 19 15X " 5 <.
IPX 18 20 j^ 5 j;
"5%'""" IB" 20" "~ " 5X "" 5"" "t ~ --
^^ ... _„ ^ , .. _. ^^ - • - -5 • -• b
OJ
Run No. 4
cxcetos
""•J D X
25X
2 a x"
15X
10X
5X
ttX
STSTFH
0
a
0
c
21
21
21
i 004CITVI
i--
1
1
7
20
22
22
Run No. 5A
.. - , ., .VE=> flVr;RflQL
t'XCilOS STATin O^ftCITVl
30*4
2 OX
2 OX
1 •• X
I OX
5*
OX
0
0
0
0
a
a
6
0
3
t
*'
10 '
10
la
Run No. SB
FPcO',l£NCv r 1
-------
TABLE 13. FREQUENCY OBSERVATION AVERAGES EXCEEDING
STATED OPACITY FOR TOTAL OPACITY DATA
Run No. 1
FKECUf^CV Oa^fcHVErt AVERAGE
PtCHfl SNVDH
3ftfe 0 0
254 0 0
mO ?
IS* 3 5
10* 67
S* 7 7
ft* ? ¥
Run No. 4
?H£GU£NCY OHSEriv£R AVERAGE
PLC^H SNYDH
30% 3 0
2* 3
25% 6
15* 22
10% 27
' 5% ?7
ntt ml
Run No. 5A
t XO : ID SI ST IJ
i'LC^? Sf
c
25X 2
-------
33
Observation
Hillside
400
76'-8"
120
5
\
0'
r i
1
f*
\
4(
1
Observation
Site 'B
Hillside
Cross-Sectional View
N
Observation
Site A
2
3
Coal preparation;
cleaning and drying
process area
Venturi scrubber inlet stack
Effluent outlet stack
Top View
Observation
Site B
FIGURE 10. OPACITY OBSERVATION SITES
-------
34
50
4O
3°
-------
35
50
40
§ 30
0>
Q.
U
O
Q.
20
10
15
Run No. 2
Particulate sampling
16
•jtRun started at 14=48)
17 18
Time of Day, hours
19
FIGURE 12. RUN NO. 2 OPACITY RESULTS AS A FUNCTION OF TIME OF BAY
-------
5O
40
Particulate
samplings
Run No. 3
Particulate
sampling
§ 30
i—
Q)
Q.
U
o
O
10
JO
Run No. 3A data
l
_L
12 13 14
Time of Day, hours
Run No. 38 data
15
UJ
er>
17
FIGURE 13, RUN NO. 3 OPACITY RESULTS AS A FUNCTION OF TIME OF DAY
-------
37
50
40
c
«J
u
V
a.
u
o
o.
o
30
20
10
Run No, 4
Participate samplings
_L
15
16
17 18
Time of Day, hours
19
20
FIGURE 14, RUN NO. 4 OPACITY RESULTS AS A FUNCTION OF TIME OF DAY
-------
50
Run 5A
Run No. 5
RunSB
40
£ 30
o>
Q.
O
o
Q.
O
20
Jl
10
10
Particulote
/samplings
H f
II
12
13 14 15
Time of Day, hours
Particulate
sampling
16
u>
00
17
18
FIGURE 15. RUN NO. 5 OPACITY RESULTS AS A FUNCTION OF TIME OF DAY
-------
39
Data Applicable to All Five Suns
The following data, required by the EPA "Guidelines for Pre-
paring Summary of Visible Emissions", apply to all five of the test runs.
Type of Plant; Coal cleaning
Type of Discharge; Emissions from thermal dryer
Location of Discharge; Stack above dryer
Height of Point of Discharge; 76 feet, 8 inches
above ground level
Distance from Observer to Discharge Point;
Site A: 400 ft northwest of stack
Site B; 120 ft southeast of stack
Height of Observation Point;
Site A: 50 ft above base of stack
Site B; 40 ft above base of stack
Direction ofObserver from DischargePoint;
Site A: northwest of stack (in afternoon)
Site B: southeast of stack (in morning)
The remaining data called for in the EPA guidelines are different
for each run and are presented in Table 14. An examination of Figures 11
through 15 show the opacity ranges as follows.
Test Run 1 - Opacity ranged from about 8 to 18 percent
during the 50 minutes of observations prior
to sundown.
Test Run 2 - Opacity ranged from about 14 to 31 percent
during time of particulate sampling which
extended from 1448 to 1736 hours.
Test Run 3A - Opacity ranged from 22 to 31 percent.
Test Run 3B - Opacity ranged from 15 to 20 percent.
Test Run 4 - Opacity ranged from about 7 to 18 percent
during the times of particulate sampling
which were 1552 to 1655 hours and 1811 to
1917 hours.
Test Run 5A - Opacity ranged from about 17 to 25 percent
during the first two particulate sampling
periods .
Test Run 5B - Opacity ranged about 12 percent at the
start of the third particulate sampling
period.
-------
TABLE 14. OPACITY OBSERVATION SUMMARY
Description Description Wind
Run Date 24 Hr. Clock Observation of of Wind Velocity,
No. (1975) Time Site Background Sky Direction mph Color of Plume
Comments
Duration of
Observation
1/18/75 1809-1859
Sky
207. clouds from NNW 0-5 Black with steam
plume near atack
2 6/19/75 1510-1850 A
3A 6/20/75 0940-1300 B
3B 6/20/75 1504-1628 A
4 6/23/75 1530-1930 A
5A 6/25/75 1004-1400
SB 6/25/75 1430-1715
Sky
50% clouda from SW
Sky Overcast from NE 0-5
(100% clouds)
Sky Overcast from HE 0-5
(100% clouds)
Sky Overcast from NW 0-5
(100% Clouds) but variable
Sky Slightly over- from NE 0-5
cast
(10% clouds)
Sky Slightly over- from NE ' 0-5
cast
(10% clouds)
Black plume obscured
by attached steam
plume sometimes ex-
tending 200 ft above
stack
50 min;
discontinued
at sundown
(7:00 p.m.)
5-10 Black with steam
plume near stack
Black plume obscured 3 hrs, 40 min
by attached steam
plume up to 75 ft
above stack
Black with steam
plume attached
to stack
Black with steam
plume attached
to stack
Black with steam
plume attached
to stack
Black with steam
plume attached
to stack
Black with steam
plume attached
to stack
Black plume obscured
by attached steam
plume extending 100
to 200 ft above stack
Black plume obscured
by attached steam
plume extending 50
to 100 ft above stack
Black plume obscured
by attached steam
plume extending 75
to 250 ft above stack
Steam plume extended
50 to 125 ft above
stack
Steam plume extended
50 to 125 ft above
stack
3 hrs, 20 min **
o
1 hr, 24 min
4 hrs
3 hra, 56 min
2 hrs, 45 min
(a) Moved to ilte A at 1310 houra.
-------
41
Trace Metal Results
The catch from Run No. 4 was analyzed for trace metals and the
results are shown in Table 15. For the mast part these data are considered
to be representative of what one might expect from coal. The results must
be interpreted with consideration of mass for each sample. The ppm values,
as presented, tend to be misleading if one does not relate the indicated
ppm values to the associated sample mass(as presented at the bottom of the
table) to obtain the mass per sample of each element. The major constituents
based on the mass collected on probe and filter catch are iron, potassium,
sodium, and zinc. Relatively small amounts of other elemental constituents
were picked up in the acetone riase of the impingers but are insignificant
when considering their relative mass. Silicon, being the predominant metal,
is most likely present due to its occurrence in coal ash. However, some
portion of the silicon may represent fragments of filter picked up during
the probe-and-filter-holder acetone rinse.
LOCATION OF SAMPLING POINTS
Inlet to Venturi Scrubber
P articulate samples were collected from the scrubber inlet gases
using an Alundum thimble in conjunction with a standard EPA Method 5
rig. A rather large port consisting of a 6-inch-diameter nipple was
necessary to accept the special EPA series cyclone used to classify par-
ticle size. The cyclone had an overall height of 5-1/2 inches. Due to
the high pressure drop across the scrubber (30 inches water pressure),
it was necessary to fabricate a sealed holding chamber and sliding gate
valve assembly (Figure 16) so that the sampling probe could be inserted
into the stack against the high static pressure. The relatively large
holding chamber would not allow complete traversing of one stack diameter
-------
42
TABLE 15. OPTICAL EMISSION SPECTROSCOPY ANALYSIS
FOR TRACE METALS (RUN NO. 4), PPM
Element
Hg
Be
Cd
As
7
Mn
Ni
Sb
Cr
Zn
Ca
Pb
Se
B
F
Li
Ag
Sn
Fe
Sr
Na
K
Ca
SI
Mg
Ba
(a)
•441
-442
-443
-444
-445
-493
-494
-495
-496
(b)
-441(1)
—
1
<200
<200
30
10
50
<50
50
1,000
300
50
--
100
—
<600
<1
10
3,000
50
2,000
3,000
500
—
300
50
-441(2)
—
1
<200
<200
30
10
50
<50
50
1,000
300
50
--
200
—
<600
<1
10
3,000
20
2,000
3,000
500
—
300
50
Samples ^a»
-442
—
<1
<200
<200
30
200
100
<50
300
300
50
<20
—
200
_.
<600
150
<10
6,000
100
2,000
2,000
1,000
15,000
600
100
b)
-443
--
<1
<10
<10
<3
<3
<3
<10
<3
<20
<3
40
—
<3
--
<25
10
115
<3
10
115
45
370
100
45
3
-444
—
<1
<170
<170
<60
10
<60
<170
<60
600
<60
120
—
170
—
<570
30
570
400
<15
570
860
<60
1,700
<60
60
-445
-
i *•
<1
<285
<285
<95
70
190
<285
1,
-
-
95
950
900
190
-
280
-
<950
1,
2,
2,
1,
1,
1,
50
900
570
70
900
400
900
900
600
285
Descriptions of Sample Nos. 375-001-441 through -445 and
Blank Has. -493 through -496 are as follows:
Wt Vol
(Solid), (Liquid),
me ml
Glass fiber filters (2 each)
Acetone, wash of front half
Impinger catch and water rinse
Chloroform/ether extraction
Final acetone rinse of back half
54
.3/54.1
268.8
87.0
3.5
2.1
Glass fiber filter (3 each) 0
Acetone blank, Burdick and Jackson 0
Lot #7150
Demineralized double distilled water, OSU 1
Chloroform/ether, Baker A.R. 1
Backzround Subtracted.
.4
.6
.9
160
815
150
325
200
200
150
*
-------
43
6'
FIGURE 16. INLET STACK SPECIAL ADAPTER WITH GATE VALVE SHOWING
POSITION OF ALUNDUM THIMBLE PRIOR TO SAMPLING
-------
44
due to insufficient probe length; therefore, the second half of the stack
was traversed without the holding chamber. Working conditions were very
undesirable because of the hot exhaust gases (180-200 F) escaping through
the 6-inch-diameter nipple at approximately 300 cfm. During the second
half of each of the two stack traverses, the gate valve was opened, the
probe was inserted into the stack against the flow of hot exhaust gases,
the 6-inch pipe reducing coupling was threaded into the valve assembly,
and traversing continued.
Figure 17 shows the inlet stack geometry relative to sampling
locations. According to the December 23, 1971, Federa 1 Reg is t er
Method 1, sampling two diameters upstream and less than one diameter
downstream from a disturbance requires at least 48 sampling points, 24 on
a diameter as indicated on Figures 16 and 17. Specific distances for traverse
points are given in Table 16.
Outlet of Mist Eliminator
Farticulate and gaseous emissions were sampled at the outlet
of the mist eliminator. Figure 18 shows the geometry relative to the
sampling locations. According to the December 23, 1971, Federal Register.
Method 1, 22 sampling points per stack diameter were required relative to
the associated upstream and downstream stack diameters. Table 17 shows
specific distances for traverse point locations.
Prior to outlet particulate sampling, it was necessary to
install straightening vanes to reduce the cyclonic swirl caused by the
mist eliminator. This was accomplished by the insertion of two 8-foot
lengths of metal at right angles to each other as depicted in Figure 18.
-------
45
TABLE 16. TRAVERSE POET LOCATIONS—INLET
Flow
O
12'
Point
I
2
3
4
S
6
7
8
9
10
11
12
Percent
of
Diameter
1.1
3.2
5.5
7.9
10.5
13.2
K.I
19.4
23.0
27.2
32.3
39,8
Distance fron
Outside of Sin-
pie Port (a>, In.
41
42-1/8
44
45-3/4
47-5/8
49-1/2
51-5/8
54
56-5/8
59-5/8
63-1/4
68-5/8 •
Point
13
14
15
16
17
18
• 19
20
21
22
23
24
Percent
of
Dimeter
60.2
67.7
72.8
77.0
80.6
83.9
86.8
89.5
. 92.1
94.5
96.8
98.9
Distance troa
Outside of San-
pie PocttW, In
57-3/8
61-3/4
65-3/8
68-1/2
69
73-3/8
75-1/2
77-1/2
79-1/4
81
82-3/4
84
(*) Using "holding chamber".
(b) Using "»hort oippla".
Venturi
scrubber
FIGURE 17. INLET STACK GEOMETRY SHOWING SAMPLING LOCATION AND
SAMPLE POINT CONFIGURATION
-------
46
6-9
1
18-4'
Mist
eliminator
•Straightening
vanes
TABLE I?. TBAVERSE" POINT LOCATIONS — OUTLET
22-9'
Potnt
I
2
3
4
5
6
7
8
9
10
il
Percent
Hi
Diameter
1.1
3.5
6.0
8,7
11.6
14.6
18.0
21.8
26.1
31.5
39.3
Distance Icon
Outside of
Sample Fore, In.
6
7-7/8
9-7/8
12
14-3/8
16-3/4
19-1/2
22-5/8
26-1/8
30-1/2
36-3/4
Point
12
13
14
15
16
17
18
19
20
21
22
Percent
o£
. Diameter
60.7
68.5
73.9
78.2
82.0
85.4
88.4
91.3
94.0
96. 5
98.9
Dissaace fron
Outside of
Saople Pore, In.
54
£0-3/8
64-3/4
68-1/4
71-1/4
74
76-1/2
78-3/4
81
83
84-3/4
FIGURE 18. OUTLET STACK GEOMETRY SHOWING SAMPLING LOCATION
AND SAMPLE POINT CONFIGURATION
-------
47
PROCESS DESCRIPTION AND OPERATION
The Westmoreland Coal Company installation near Quirrwood, West
Virginia in Nicholas County thermally dries Pocahontas No. 3 Sewell and
Dorchester-Imboden coal. The demand for thermal drying is due to freight
rate savings, the elimination of handling problems due to freezing, and
the needs of the customer's process (coke ovens must control bulk density
and power plants must control plugging of pulverizers). A venturi scrub-
ber is used to control particulate emissions from the thermal dryer.
Tests for particulate emissions were conducted on the thermal dryer ex-
haust only during periods of typical plant operations.
Process Description
Coal is delivered to the plant and is crushed to a variety of
sizes. It is then washed, screened and separated by both water tables
and concentration tables. The coal washing is a continuous process and
reduces ash content from 16 percent to 3 percent.
The coal that is thermally dried, the 3/8 x 0-inch coal or the
slack is dewatered by shaker tables and vacuum discs and then dried to
2.0 percent to 3.5 percent surface moisture in a thermal dryer. Coal
drying is accomplished by use of flue gas (produced by a coal-fired furnace)
reduced in temperature by dilution air. The emissions from the fluidized
bed thermal dryer are exhausted to a chamber loaded with 40 or more multi-
clones which separate much of the fine dust from the emissions. The finer
dust particles pass from the multiclones of the dryer through a high pres-
sure blower to a venturi scrubber and a demister where over 95 percent of
the particles are collected. The emissions to the atmosphere are ducted via
an 81-inch diameter stack. Figure 19 is a sketch of the thermal dryer
system. The design capacity of the thermal dryer is 270 ton/hr of coal at
approximately 250 P. The plant is usually operated at two-thirds to
three-fourths of this rate because of the moisture level. The actual
operating capacity of the dryer is limited by the tons of water evaporated
per hour rather than the amount of coal being processed. The plant runs
on a schedule of two 8-hour shifts and is typically closed on weekends.
-------
KEY
-».-.—Gasflow
Coalflow
Exhaust Fan
. Explosion Vent
Dust
o Hector
ischarge \
Bedplate 4s—7
Tempering
Louvers
00
Control
. Panel
Note: Sampling point
located at Dryer
feed conveyor belt
oc
i exhaust temperature and fan
pressure
+ drying chamber pressure and
tcinjicraturc
* hud pressure
H inlet preasure
FIGURE 19.
EXHAUSTING-TYPE FLUIDIZED-BED THERMAL COAL DRYER, SHOWING COMPONENT PARIS AND
FLOW OF COAL AND DRYING GASES, WESTMORELAND COAL COMPANY, IMPERIAL SMOKELESS
DIVISION, QUINWOOD, WEST VIRGINIA
-------
49
Emission Control Equipment
The thermal dryer exhausts into a cyclone separator where the
large particles are removed. Next, the exhaust is blown into the venturi
scrubber where the fine particles are impacted upon water droplets which
are removed from the effluent gases by the mist eliminator. From there,
die exhaust gases exit the mist eliminator and go out the stack. The
fan volume is rated at 134,000 cfm for the maximum design capacity of
270 ton/hr. The pressure drop across the venturi scrubber is 32 in. H20,
3 to 4 in. H2<3 attributable to the mist eliminator.
Process Operation
Samples were collected from the inlet and outlet gases to the
venturi scrubber control equipment. Opacity observations and dryer feed
*
samples were gathered concurrently. Each test run is described as follows.
June 18, 1975 - Refer Appendix E Run 1
Test went well with only one interruption that occurred
due to low feed. Also, Sewell No. 3 strip mined coal was used
for the majority of the time instead of Sewell deep-mined coal.
Though the data are not suitable for evaluation of Sewell No. 7,
they do provide an interesting comparison between the two coal
mining methods.
June 19, 1975 - Refer Appendix E Run 2
The test had only two interruptions but process operations
were unsteady. Feed to thermal dryer was discontinued, problems
with the water supply to the venturi scrubber were suspected, and
the supply of raw coal to the plant was inconsistent. These data
ace not typical of routine operation. Repairs were made to the
venturi scrubber water supply system prior to commencing the next
test.
June 20, 1975 - Refer Appendix E Run 3
The test was very good, even though it was necessary to
temporarily suspend sampling twice due to process malfunctions.
Process on the whole operated very smoothly, and during actual
testing was very consistent. The test data are representative
of typical operations.
*Run numbers are relative to outlet.
-------
50
June 23, 1975 - Refer Appendix E Run 4
Test was very good with no delays at all. High drying
chamber temperatures occurred for one-half hour from 4:45 to
5:20 p.m, but were not extreme,
June 24, 1975
Process shut down every half hour due to broken equip-
ment. There was no continuity to process whatsoever. Testing
was cancelled for the day.
June 25, 1975 - Refer Appendix E Run 5
Test very good. Sampling was interrupted briefly during
two short process delays. Drying chamber temperatures were a
bit high from 12:30 p.m. to 1:05 p.m. and from 4:40 p.m. to 5:03
p.m. but were not abnormal.
June 26, 1975 - Refer Appendix E
Several special inlet tests were done by Roy Neulicht.
The first and second tests were good with no problems. The
third and fourth tests had high but not normal drying chamber
temperatures. All tests were conducted during the processing
of Sewell No. 7 deep-mined coal except the fourth test which
was Park Sewell or Sewell No. 3 strip-mined coal.
The production for the second half of Test No. 5 (June 25, 1975)
was determined to be 180 ton/hr. The average process rate for that day,
however, was only 137.7 tpn/hr-because of production stoppages (see Table 18).
The rate during actual sampling was higher. The reason for this inconsistency
is that testing was never done during process malfunctions or slow ups be-
cause of the abnormally high drying chamber temperatures that occur. The
emission tests were conducted only during periods when conditions were
typical of routine operation and the data, therefore, are representative
of normal production,
TABLE 18. PRODUCTION RATES
(June 25, 1975)
Recorder
Westmoreland Coal Co,
EPA
EPA
EPA
Time Period
Both shifts
10:00 to 11:18
14:55 to 16:18
16:18 to 17:18
Amount Time,
minutes
1035
438
83
60
Process
Rate,
ton/bar
137.7
158.9
187.9
180.0
-------
51
SAMPLING AND ANALYTICAL PROCEDURES
Plant operations, by necessity, were monitored by EPA personnel
prior to and during all sampling to ensure the validity of the measure-
ments being presented in this report.
Standard EPA sampling methods, as reported in the December 23,
1971, Federal Register, were followed to obtain samples of gaseous
emissions for C02> GO, and 02. Samples of scrubber water and process
coal were taken under the direction of the EPA Project Officer. Sample
times are reported in the Sample Collection Log presented in Appendix D.
A temporary on-site lab facility was set up for equipment clean-
up. Due to the nature of the process, it was important to isolate, as
much as possible, the cleanup and analytical area from plant operations.
Analytical balances were set up in the temporary lab and mass
determination of BCL inlet and outlet samples and for the EPA cyclone catches
were determined on site after each run. All calculations pertinent to
isokinetic sampling were determined after each run to ensure results
were within EPA guidelines.
C_oal_Sample Colleetion Method
Representative samples of the process coal were collected for
sieve analysis during each run. Figure 20 depicts the process feed
system used at the Westmoreland Coal Company and also gives a pictorial
diagram of how coal sample aliquots were collected.
The conveyor pushes the coal into a large hopper where it is
fed into the dryer. The balk or large mass of the coal falls into the
hopper just as it passes the end of a stationary^ inclined ramp. As the
conveyor reaches the end of its travel and starts its return, additional
coal which has adhered to the conveyor surface is thrown off and appears
in the hopper as relatively fine particles.
-------
52
Coal samples
FIGURE 20. COAL SAMPLE COLLECTION METHOD
-------
53
The hopper outlet coal samples were collected from each of four
quadrants as depicted in Figure 20. The sample collector, fabricated ac-
cording to ASTM standards^ , was inverted and placed behind the stream of
coal as in Position 1. The collector was then turned upright and moved into
and through the stream of coal as in Positions 2,3, and 4. The sample
collector was emptied into a sample container and the collection method was
repeated for each of the other quadrants to obtain one composite sample.
Three samples were collected each 15 minutes during the entire particulate
sample run. The coal samples for each run were combined and a fraction was
removed for sieve analysis according to ASTM Standards^ .
Scrubber Water Collection
To develop a better understanding of the operation and effective-
ness of the venturi scrubber, samples of water which had passed through
the ventari were collected at the outlet of the scrubber sump. Figure 21
is a simple schematic depicting the basic flow pattern of the scrubber
system. As indicated, about 80 percent of the scrubber sump water is
recircalated back to the venturi for reuse while the other 20 percent is
sent to a static thickner where the particles collected in the scrubber
water settle by gravitational forces. The scrubber water sample to be used
for size distribution of the collected particles was taken from the 20
percent by-pass line as indicated. It is assumed that sufficient water
flow is maintained in the recirculation system to allow a representative
water sample to be collected relative to the associated outlet emission
sampling. If this assumption is valid then a comparison can be made of
the inlet particle size distribution and the associated particle size
measured in the scrubber water. However, it should be noted that the
particles collected in the scrubber water represent a time-averaged
representation of the particles removed from the gas stream. The volume
of the scrubber sump relative to the 20 percent discharge volume flow
would indicate the extent of time averaging involved relative to the gas
sampling time. Only if there exist steady-state scrubber operation and
-------
Straightening
vanes
Level
control
Makeup water
20% clarified
Scrubber sump
Overflow
to thick-
ener
8O% recirculated water
About 20% of scrubber water flow
Water pump
Ul
Scrubber
water sample
To static thickener
FIGURE 21. SCHEMATIC OF VENTURI SCRUBBER WATER FLOW SYSTEM
-------
55
an unchanging gas borne participate feed to the scrubber can the parti-
cles found in the scrubber be directly compared with gas samples for
evaluating scrubber performance.
Particle Sizing Methodology
farticulate samples were collected by sampling the venturi scrab-
ber inlet stack gases at an isokimetic rate into an Alundum thimble. During
sampling, the thimble was located in the stack and was at stack gas temperatures,
thereby minimizing condensation. Size distribution for particles collected
in the thimbles, in a cyclone sampler, and from bulk coal samples were de-
termined with a Coulter Counter^. A Mine Safety Appliance (MSA) Particle
Size Analyzer' ' complemented Coulter Counter data relative to <325 mesh
samples. The following questions were considered relative to analysis tech-
niques which, if not applied properly, could alter the reported particle
size distribution:
(1) What effect would sample drying have on the particle
size distribution?
(2) Would particle dispersion by ultrasonic vibration
alter the particle size distribution?
(3) What particle concentrations would be "generated" from
thimble breakup daring ultrasonic cleaning?
(4) If ultrasonic thimble cleaning were feasible because
of insignificant thimble particle concentration, would
it be possible to obtain a. representative aliquot
from a relatively large electrolyte volume?
(5) Since the MSA particle size analyzer utilizes various
fluids to determine particle size from settling
velocity, might the coal particles be soluble enough
in the fluids to affect their sizes?
Experimental efforts were undertaken to answer these questions so that a
valid experimental procedure for size distribution measurements could be
established. The following particle size distribution results are an
average of three runs per aliquot, which is a routine procedure for Coulter
Counter analyses. One aliquot per sample was taken for Coulter Counter
analyses and one aliquot per sample was taken for analyses by the Mine
Safety Appliance Particle Size Analyzer.
-------
56
Distribution Change Due to Drying (a)
It was determined by desiccator drying of samples collected
in thimbles at the scrubber inlet that they contained <1.0 percent mois-
ture; therefore, particle size change due to drying was expected to be
insignificant. This was verified by Coulter Counter size analyses as
shown in Figure 22. Only slight differences between the particle size
distribution curves of "undried" or "dried" samples are seen. These differences
are considered to be within experimental error and, hence, no effect of
coal sample drying was found.
The bulk process coal samples were wet when collected and,
therefore, a change in particle size distribution due to drying was
considered. An extra bulk feed coal sample was divided into two equal
portions according to ASTM standards^). One half was dried at 100 F
and sieved dry. The other half was sieved wet to determine if the. size
distribution would show a difference. Figure 23 shows the results of
these measurements which indicate essentially no difference except In the
pan catch (<325 mesh or <44 M-m) which shows a slightly higher catch for
the wet sieving. This could be attributed to experimental error or
possibly the loss of the relatively fine catch during the drying process.
Effect of Ultrasonic Dispersion
Compared with Mechanical Dispersion
Before particle dispersion by ultrasonic techniques could be
utilized, it was necessary to determine to what extent the particle size
distribution would be altered by ultrasonic dispersion techniques and
what procedures were sufficient to assure adequate dispersion. A sample
(a) The effects of drying on size distribution were determined with coal
samples which may not have been representative aliquots and, therefore,
the data can only be considered relative with respect to size distri-
bution and are valid only for evaluating drying effects.
-------
57
99.8
99.5
99
98
95
90
£.
.? 80
>, 70
c 60
0)
if 50
0)
°- 40
0)
~ 30
| 20
o
10
5
2
1
as
0.2
O.I
4
/
t
/
r
4
r~
S
r
&
^C
'/
q
(i
/
/
*{£/
**&
3
^ Und
O Dri
?'.
ried
ed
0.6 0.8 I
4 6 8 10 20
Particle Diameter, micrometers
40 60
FIGURE 22. DISTRIBUTION OF DRIED AND UNDRIED COAL
SAMPLES FROM A THIMBLE CATCH, COULTER
COUNTER ANALYSES
-------
.21
Q>
§
-------
59
aliquot of a thimble catch was placed in a dram vial containing the
wetting agent and electrolyte solution. Mixing was accomplished by
repeated filling and emptying of a medicine dropper (the usual technique
for dispersing particles prior to Coulter Counter sizing). A size dis-
tribution then was determined for an aliquot of this dispersion. The
dispersion was then subjected to ultrasonic vibration ; another aliquot
was removed, and a size distribution determined. Figure 24 depicts the
results of the two dispersion methods. Although slight differences
can be seen, the differences are within experimental error and it can be
concluded that either method of dispersion could be used without sub-
stantial error. (This conclusion applies only to the specific samples
of this task. Other materials could possibly respond differently depend-
ing on their morphology and wetting properties.) Particles from the
solutions used in the analysis by the Coulter Counter were collected on a
silver membrane filter and observed by means of a scanning electron
microscope for possible size differences in an additional effort to
verify that ultrasonic dispersion did not modify the particle size.
Electron photomicrographs were taken of representative areas of the
filters and it was observed from these photos that the particles are
essentially the same in number and size with and without ultrasonic
dispersion.
Ultrasonic Cleaning of Alundum Thimble
To determine the extent and nature of particle release from an
unused thimble, a new Alundum thimble was placed in 825 cc of 4.0 percent
sodium chloride (Coulter Counter electrolyte) and cleaned by ultrasonic
vibration for 30 minutes at a nominal frequency of 28 kHz + 1.5 kHz. This
procedure was repeated three times, each time using the same thimble in
clean electrolyte to determine if any change would occur in the rate of
particle generation. A size distribution by Coulter Counter was determined
from each 825-cc volume. Table 19 compares the total number of particles
generated each time by ultrasonic cleaning.
-------
60
99
QQ
9B
95
90
80
70
f, 60
'
/
L
>
/
a'
/
]
c Dispersed
Dropper Dispersed -
).2 0.3 0.4 Q6 0.8 2 3 4 6 8 10 2C
Particle Diameter, micrometers
FIGURE 24« COMPARISON OF ULTRASONIC AND MEDICINE
DROPPER DISPERSION TECHNIQUES , COUUTER
COUNTER ANALYZER
-------
61
TABLE 19. PARTICLES GENERATED FROM ULTRASONIC
THIMBLE CLEANING, COULTER COUNTER ANALYSES
Size,
Urn
22.0
17.5
14.0
11.0
8.8
7.0
5,5
4.4
3.5
2.8
2.2
1.7
Accumulative Number of
Than Indicated Size
Run 1
0
0
0
13
83
173
233
488
1,023
1,922
3,235
10,213
Run 2
2
3
16
38
51
130
231
393
690
904
1,548
3,765
Particles Larger
. * 10-3
Run 3
0
3
5
3
25
61
125
229
338
546
843
2,020
-------
62
It appears that the number of particles generated decreases with
each successive cleaning and begins to level off to some extent* One can
conclude from these data that thimble cleaning prior to use may reduce
error in the size-distribution data where relatively small sample catches
are expected.
Relative Comparison--
Partlcle Concentration
The importance of the relative concentration of thimble-generated
particles compared with collected coal particles in the particle population
being sized was determined. Sample contamination due to ultrasonic thimble
cleaning was found to be insignificant when determining size distribution if
a, sufficient sample mass was collected. Table 20 shows the total number of
particles generated during initial thimble cleaning is of the order of 10 x
10 and is significantly reduced with successive cleanings. For comparison,
it has been determined, during this study, that the total number of particles
in a measured aliquot of 2.16 mg of coal is of the order of 12 x 10 . During
this study, the thimble sample catch range was from 9,271 mg to 26,167 mg
(see Table 7). By ratio (9,271 mg:2.16 mg), the thimble sample particle
population is greater by at least a factor of the order of 4,000. Therefore,
it can be concluded that the relative number of particles generated by thimble
cleaning is insignificant by comparison with the mass contained in any of
the thimble samples collected during this study. As previously mentioned,
if one expects a relatively small thimble catch it would be advisable to
preclean the thimble several times before use to eliminate the possiblity of
a significant background particle contribution.
-------
63
Representative Aliquots From
Large Electrolyte Volumes
Thimble cleaning and particle dispersion were both accomplished
via ultrasonic vibration. The thimble contents were emptied into a beaker
containing 825 cc of isopropyl alcohol, the alcohol being used because of
its wetting characteristics. The thimble was then placed into the alcohol
bath and ultrasonically vibrated at a nominal frequency of 28 kHz - 1.5
kHz for 30 minutes. Obtaining a aliquot from three different beaker levels
while the particles are in suspension would give some identification of
possible stratification due to nonuniform mixing and check the representa-
tive nature of aliquot collection for analysis. Figure 25 depicts the
size distribution indicating that a representative aliquot can be selected
from a relatively large volume of solution with a very dense particle con-
centration if the suspension is maintained by ultrasonic mixing. A further
conclusion from these results is that the measurement technique is repeat-
able and random errors are small.
Coal Particle Solubility
Solubility of coal particles in the solutions used with the Mine
Safety Appliance Particle Size Analyzer was found to be negligible. The
operating principle of this device is essentially to measure the particle
sedimentation rate as a function of time in an appropriate liquid media.
The particles need to be thoroughly wetted and are placed in a feed liquid
prior to being placed in the sedimentation liquid. The feed liquid consisted
of 50 percent isopropyl alcohol and 50 percent heptane. A solubility check
for coal particles in this mixture was made by measuring weight loss during
the washing of a coal sample with a large excess of the solution. A weight
loss of 0.08 percent was found which is considered to be insignificant.
-------
64
as 0.8
4 6 8 10 20
Particle Diameter, micrometer
40 60
FIGURE 25. REPRESENTATIVE ALIQUOT CHECK OF LARGE
SOLUTION VOLUME HAViNG HIGH-PARTICLE DENSITY,
COULTER COUNTER ANALYSES
-------
65
REFERENCES
(1) Coulter Counter Industrial Model B Instruction Manual. Coulter
Counter Industrial Division, Franklin Park, Illinois 60131.
(2) Whitby, K. T., "A Rapid General Purpose Centrifuge Sedimentation
Method for Measurement of Size Distribution of Small Particles",
Mechanical Engineering Department, University of Minnesota, 1955;
presented at the 61st Annual Meeting of ASHRAE, Philadelphia,
Pennsylvania, January, 1955.
(3) Federal Register. December 23, 1971, Vol. 32, No. 247.
(4) 1974 Annual Book of ASTM Standards. Part 26, "Gaseous Fuels;
Coal and Coke, Atmospheric Analysis", American Society for
Testing and Materials, Philadelphia, Pennsylvania 19103, 1974.
(5) Federal Register. November 12, 1974, Vol. 39, No. 219.
-------
APPENDIX A
COMPLETE PARTICULATE RESULTS
-------
APPENDIX A
COMPLETE PARTICULATE RESULTS
TABLE A- 1. INLET. RESULTS
SMD CO.\L CCHPSNY I'fLET RESULTS
ON
TT
P3
RUN 'JO. I
TEST IStr ft/lH
SAMPLING TTMF, ?t» HTJP CLOC< FQO" il?5*
TO 2?09
SaMf>LIv!G MT77LE r^Ift Mi'TF.1?, I"'- 0.175
naaOMFTST(. pDC$SUSEf IN< H- -
? "•
fr/19 6/20
1157 ISIS
1613 1719
0.175 0.17*5
95 %
6
6/25
1710
ftBSOLUTE
27.12
P°cSS'JcE
IN. H?D
VOLUMF OP 0°Y *fi<^
G. StS HFTFR TFKPF^HTUaC» F
PM
VM
TM
VHSTO
VW TOTEL H20 C^LLTCTF'
SILICft GEL, "L
VWGfiS
Gas s&MSLEn AT
^0 CON?ITIONS» DS^F
2.32
IIS.!
inn
102.1.
271,3
12.9
2.53
PJ.U
. 0
27.61
2.11
126. P.
<$o.o
6.0
B1.9 125.0 115.6
171.0
315,5
15.0
315.2
pF.°r?MT
Br »
E TH STACK
10 MOLFCUL6= FRflCTION OF 0°Y GAS
V. 02 v"6l."uiE PFPCF'-JT O'PY" '
% r.O VOLUME PfCFNT OpY
x H2 VOLUME PERCENT-n»Y
X F 0 PE'^F^T fXCF.SS ^19 •
MHO MOLF fUL'*5* WFIGHT OF ST^C< jAS(
_OF STACK
rCTFr;T
1.7
~1 9~. 1
1.1
S.99
0.93
0.9'
"0.1
9.10
1.0
20". 0
0.1
7R.9
10.69 12.01
0."
0.1
79.1
22 6 f
HH MOtcnULaP
WET 'IAS IS
CP
TS
G. STaC<
27.*
1C.6
0,15
O."1?
171
202
"Vfl
0.9"
19.7
O.t
7 9.-3
15=55
2R.9
27.B"
1PI
-------
A-2
TABLE A-l. (Continued)
PST
PS
VS
ftS
ss
MOPFLa*-") C
°vn NO.
TEST HftTF
SdMPLJl»S
STSTTC
IN. MR.
STAC* ':•
• STSC< '
cowr TI
STACK a
• HOY STa
OftL C01S/SMY I^L^T RESULTS
1 ,
fc/11
TIME, 2<« HODS' CLOC< FR01 H25
TO ??T9
P»FSSUP.e OF STftCK GAS,
?.12
6S PPFSSUPB, l!l. HS ABS. ""~29. 72^'
6S VELOCITY AT STAC<
Of«5, FPH fii»^3
OF6, SO. TN. _ ._ ,'.t»0«>9._
C< r»AS VOLUMETRIC FLOW
? «» 5 6
S/19 6./20 fi/23 fi/2'5
13S7 1503 IfiOA 1120
Ifit3 1719 19i«l 1710
2.12 2.12 2.1? 2.12
?9.^ ?q.69 29.80 29.73
. ... .._. ... ^
6761* f)7?7 S^fjO 6^?
.._*ns«. 00** ^ ,069
AT STa'-na»o
Qfl
X I
2. P..
TC
MF
1C
CSN
r.as VOLUMETRIC FLOW
AT STflSK CONTITIO'IS, ACFM
136^13
183212
_0.??.C.EN_T_.pPA_CITY ;
UNTT Ff?n ofTE, TON5/H-"?
Pi°TIC'JLflTE--
FTLTER, "G
r»a?TTr.JLftTP~TOTftL, MG
5-p'CSTCH^
ND
...L.
ND
101.0
__B_
ND
19 135899
I 99.7
0 0
ND ND
.0
9271.0 1^369.0 2fit67.Q
0 2 F> { 6 7 . 0 2fl0^7.0
.0 " '.0' " .0
can
CAT
C ft U
CAW
PAX
PTT
PTT
FILTER,
pa°TTC'JLSTE--TOTAL, SP/SHF
PA'TICJLATP—P^n?F, CYCLCME,
»fti?TICJLATF--ooOBF, CYCLONE, AHO
FTLTE1?, LB/HO '
. _?.fJ
....2.7.29.
'2.016'
1201.3
3201.1
.0
J..7-SS_
1. 39 7
Y.397~
2.
J^.2Z5 ?«&7.5
2.675
2.29^ 1.972
3812.9 311<*. 2
3812. <» 3111.. 2
rr5?, LB/TON
P8=>T!C'JL&TF. — TOTiL. !.B/TON FEEH
ND
ND
ND
ND
ND
ND
ND
ND
ND
ND - No Data
-------
A-3
TABLE A-2. OUTLET 1ESTJLTS
CO^L
»Y
PUN NO.
TEST r>ftTc
r, Tl^e, Z<<
6-/19
6/20
F5.5
267.lt
12.7
99.?
W ...pPf)^srNT ^oi?.TJ.S!E"_.IN_5J-ftG.lL
8* VDLUHF
MD HOLFHULA? FPfiQTIO'l OF
•/. r.o? VOLUME PEPCPST
___^
G*S
PERCENT
X CO VOLUHF
'/. M? VILU^F
X~ C'fl PE^"6E"NT~?XCF5S~^i°~
MHH HOLFr.ULCR KFIGHT Ce
11.75
'"bVfliaT
1.7
"Tvn"
""" o"."i
~79 .1
"""to"?'*
29.0
11.1.0
19.§
•-—•--
"79"."?
•j-r-~-
1.0
"?dro"
O.'l
78.9
13.??
0 . 87
o.'n
o.i
79.1
29.0
_m-( MfiLFSU.LAR wEir.MT ar ^T_ac<_5ft_s,
ijET^"'usis"'" ' "
C«> PITftT Tljnc C(
TS aVS. STtCK TCMO£<>flTUnE
^JP V~CT" SAMPLING" on i NTS
27.7
'd.«5
ii.V
27.7
110
14(4
.2«..9
"2JT-f
it &'
" «.T""
2%9.2
12. 3
'41.95
0.9
l"9.7~
0.1
79.3
"""l5,"qeT
28.9
27. t>
O.R5
112
-------
A-4
TABU: A-2. (Continued)
WF?
PST
PS
VS
AS
03
OS
'/. n
TC
MF
MT
1C
CAN
nnn
car
CAU
caw
OAX
PTF
PTT
TMORFLArtrj Cf)AL r.fl1°AVY O'JTLFT PfSULTS
9UN NO. 1 ?
TEST "5TF, ' "'. '" ' " 6/n "V/iq"
SAMPLING n'MFt ?% HOIJP CLCTX FRfiH I'M 5 li»t»«
TO 220,3 m*,
^TiTfC PRESSURE CF STfcC< 3AS,
IM. HG. .HO .00
STACK GflS P°FS'3U0E» !N. »j 60S. " 27. 'i^ 37.57
ST?.C< G»*" VfLDHITY ST STftC<
CCHfHTIONS, FPM kqs+T «4ftD^
STfiCK flRF.a, S3. . IN. 5120 __5.12.0-..,.
P»PY ST5CK S-^S VOLU^ET«»IC FLOW
PftTF aT STasina00 CONTI TIO"!S« DSQF'1 " 1325£.3 1255.1^
STACK1 IS? VOLUMETRIC FLOW RATE
8T STA~K COMOTTTOK'St SCPM _ __ _ 175??3 163761.
PERCENT ISOKINETIC, ___ . ,.. __ ., I0*j.t» 133.3
PE^CE^T opsriTY 15 20
UNf, T" FFfo •?,". TE» TONS/H" ' ND ND
D8PT 1C JL ATE — -P^O^c » CYCL^MEt AST!
FILTF^, HG " 2i»U.«i 32*. l'
PAPTICJL«Tr--T3TftL, -S ?99.7 ^3.2
PERCENT IMPINOF* CATCK 19.5 zf>.*
PaRTIC'JLftTE--PE?nnF, CYCLP'IE, AMD
PH9TICULATF — TOT1L. GR/SCF ____ 0.0e«7 0.07?.
PARTICJLATE — P?08F, CYCLOfJE, AMD
FTLTF°t G0/fiCr 0,02^'" O.OW?
PARTTCULflTF. — TOT'-L, GP/SCF I). 035 0.05R
PftRTTCULATE — P'Ofr, 'CYCLONE:, ftv!0
PART TC jt.£TF--p='ooE» CYCLONE, ASJD
cTLT^o. L9/TOH F^FI " "ND ND
PSRTICJLATf — TOTiL, L^/TON ^EF.O ND ND
3 «4 5
6/?0 6/23 *>/25
Dqt.3 155? 1117
15?H 1^17 1657
.00 .00 .no
5l«.l SUI 51!»5
,5l?n _51?0 51 ?0
1393?0 IS^^P.^ 137815
110.5 103.1 a?.i
?5 1 3 20
ND ND ND
239.6 376. q ?1^.2-
3*4?. 9 kf>L. U 300. ?
30.1 13.3 25.6
0.0^7 0.
-------
A-5
TABLE A-3. ORSAT GAS COMPOSITION MEASURED AT OUTLET STACK-
WESTMORELAND COAL COMPANY, QUINWOOD, WEST VIRGINIA
Run
No.
QNC-1
QNC-2
QNC-3
QNC-4
QNC-5
Date,
1975 Time
6/18 1812-
1945
Average
6/19 1540-
1614
Average
6/20 1205-
1235
Average
6/23 1600-
1730
Average
6/25 1130-
1334
Average
C02,
1.7
1.7
1.7
1.7
0.9
0.9
0.9
0.9
1.0
0.9
1.1
1.0
0.7
0.8
0.9
0.8
1.0
0.7
1.0
0.9
S"
19.1
19.1
19.1
19.1
20.0
19.5
19.8
19.8
20.0
19.9
20.0
20.0
20.1
20.2
19.8
20.0
19.4
19.9
19.7
19.7
C0,(a) N2,
<0.1 79.2
<0.1 79.2
<0.1 79.2
<0.1 79.2
<0.1 79.1
<0.1 79.6
<0.1 79.2
<0.1 79.3
<0.1 79.0
<0.1 79.2
<0.1 78.9
<0.1 79.0
<0.1 79.1
<0.1 79.0
<0.1 79.3
<0.1 79.1
<0.1 79.6
<0.1 79.4
<0.1 79.3
<0.1 79.4
Molecular Weight of
Stack Gas (Dry Basis)
Run Avg., Ib/lb Mole
29.0
28.9
29.0
28.9
28.9
(a) Orsat detection limit.
-------
A-6
Sample Calculations—Outlet Run No. 4
1. Volume of dry gas sampled at standard conditions(a), dscf
p
17.7 x V (p,+ rp—7) 17.7 x 109.2 (27.68 + r|~)
v = mV P—13.6' = 13«6 = 99 9 dscf
mstd (Tm + 460) (83 + 460)
2. Volume of water vapor at standard conditions(D), scf
V = 0.0474 x V = 0.0474 x 318.6 = 15.1 scf
wgas w
3. Percent moisture in stack gas
100 x V
Wgas _ 100 x 15.1
V + V 99.2 + 15.1
mstd wgas
4. Mole fraction of dry gas
., _ 100 - 7. M _ 100 - 13.2 _
Md " 100~ 100" °'
5. Molecular weight of dry stack gas
= (7oC02 x -j^) + (%02 x ~) + [ (%CO
(0.8 x ) + (20.0 x ) + (79.2 x -j||) - 28.9
6. Molecular weight of wet stack gas
MW = MW, x M, + 18(1 - M.) = 28.9 x 0.87 + 18(1 - 0.87) = 27.5
d d d
(a) Dry standard cubic feet at 70 F, 29.92 in. Hg.
(b) Standard conditions at 70 F, 29.92 in. Hg.
-------
A-7
7. Stack gas velocity at stack conditions,
= 4,360 x ,/ APs x (Ts -f 460)
1/2
27.68 x 27.5
8. Stack gas volumetric flow rate at standard conditions^ ', dscfm
_ °'123 X Vs x As X Md x Ps _ 0.123x 5.179 x 5.120 x 0.87 x 27.68
Qs (T + 460) 116 + 460
= 135,983 dscfm
9. Stack gas volumetric flow rate at stack conditions, acfm
0.05645 x Qs(Ts + 460) ^^ x ^3.9* (U6 + 4&Q)
X_ ~ TJ „ -1. ~ -)-T £Q „ f\ Q-) 10i*,I//
a r x M, Z/.oo x O.o7 -
S d
10. Percent isokinetic
1,032 x (T + 460) x Vm
_ _ _= 1.032 x (116 + 460) x 99.2
Va x T. x P x M, x (D )2 5,179 x 132 x 27.68 x 0.87 x (0.186)2
S t S fl tl
104
11. Particulate — probe, cyclone, and filter, gr/scf
Q * 0.0154 x ~~£— = 0.0154 x 3-7r|*| = 0.059 gr/dscf
S** V^.^ 7? »•&
mstd
(c) v APS x (T8 + 460) is determined by averaging the square root of the
product of the velocity head (Aps) and the absolute stack temperature
from each sampling point.
(d) Dry standard cubic feet per minute at 70 F, 29.92 in. Hg.
-------
A-8
12. Particulate--total, gr/dscf
m ,fil ,
Cao = 0.0154 x ^— = 0.0154 x ^ 2 " 0.072 gr/dscf
mstd
13. Particulate—probe, cyclone, and filter at stack conditions, gr/acf
= 17'7 X °an X Ps X Md _ 17.7 x 0.059 x 27.68 x 0.87 _ . ...
at (T + 460) ~ (116 + 460) *
S
14. Particulate—total at stack conditions, gr/kcf
r 17.7 x Cap x PS x Md 17.7 x 0.072 x 27.68 x 0.87 n n,, . _
Caw = (T +460)= (116 + 460) = °'°53 gr/acf
S
15. Particulate--probe, cyclone, and filter, Ib/hr
C = 0.00857 x C x Q = 0.00857 x 0.059 x 135,983 = 68.2 Ib/hr
aw an s
16. Particulate--total, Ib/hr
C = 0.00857 x C x Q = 0.00857 x 0.072 x 135,983 = 83.5 Ib/hr
2X ciO S
Note: The calculated values obtained from these equations will not
reproduce the computer results which reflect 14 place accuracy
for each computation.
-------
APPENDIX B-l
VISIBLE EMISSION OBSERVATIONS
DURING PARTICULATE SAMPLING
-------
APPENDIX B-l
VISIBLE EMISSION OBSERVATIONS
DURING PAETICULATE SAMPLING
Summary and Discussion of VisibleEmissions
A computer tabular summary of the field data reduced
to 6-minute averages is included in Appendix B-l and B-2, Appendix B-l
includes only data obtained during particulate sampling, whereas Appendix
B-2 includes the data for all observations for the entire reading period.
The Federal Register, Vol. 39, No. 219, November 12, 1974 ( is the method
used for obtaining the visible emissions data.
The average opacity for each of two certified observers
is determined for each successive 6-minute period consisting of the minute
shown under "Time" in the left column plus the next 5 minutes. Each 6--
minute running average is derived from a total of 24 readings (one reading
every 15 seconds for 6 minutes), The average values of opacity are not
reported for the last 5 minutes of data because it is not possible to com-
pute a full 6-minute average. The tables show the average for the two
observers and the deviations from the average for each observer, all re-
ported to the nearest 0.1 percent.
Tables 12 and 13, presented in the body of the report,
are computer summaries of Appendix B-l and B-2 and list the frequency each
observer exceeded the stated opacities. The method of computer data
reduction for these tables is as follows.
At the end of the moving time base average
there is a listing of the number of times the 6-minute
average for each observer, A^» exceeds 30, 25, 20, 15,
10, and 0 percent opacity. However, the 6-minute
averages listed here are exclusive, and the listing
begins with the greatest opacity. By exclusive, it
is meant that once a 6-minute average is listed, the
readings encompassed in that 6-minute time period are
not used in any other average. Because of the nature
-------
Bl-2
of the moving time base averages A. , this means that
Given: AQ, A^ A2, A3, A^
where A is the 6-minute average of an observer
for the time period beginning at 0800 and
A-i is the 6-minute average of the observer
for the time period beginning at 0801, etc.
Then: If the 6-minute average AIQ is listed as
exceeding 30 percent opacity, the moving
time base averages Ac through An and A-,,
through A., - are excluded from any other
listing, fhus when A is listed. A .
a m~j
through A_i e must be excluded from the listing.
The emissions were observed above the stack leading from
the thermal dryer. This stack was 81 inches in diameter (6,75 feet) and
the top of the stack was 76 feet, 8 inches above ground level. Most of
the readings were taken in the afternoon from an observation point about
400 feet northwest of the stack and 50 feet above the base of the stack.
The observation point for a smaller number of readings taken in the morning
was about 120 feet southeast of the stack and 40 feet above the base of
the stack.
A steam plume was attached to the stack for most of the
time and extended anywhere from a few feet to 300 feet above the stack.
Comments regarding attached steam plumes is discussed in Appendix I.
-------
:THOJ 9 C"POCT
PLANT
LOCAT
OAT£ J
TIȣ
18J9
"isi-y
1611
1112
1813
1814
.HIS..
1816
1*17
1813
iai9
i«2f
1*21
182Z
1823
18?*.
1925
1826
. 1827,
1829"
1829
1S3C
I'lSl
I1* 12
1633
1834
1635
1836
1«37
1838
1839
1«4>
181,1
1842
1843
1844
:
ION*
:s?t
— -.
fii
PLCM;
16.
17.
17.
17.
16.
If.
.15.
15.
15.
15.
15.
15.
. 15,
1%.
13.
13.
13.
13.
.!•••.
14.
14.
15.
IS.
15,
1«,
14.
Id.
12.
11.
11.
1C.
9.
9.
9.
«.
10.
Hif. T ICKcLANl) COAL i
TUi'JUOOO '4 VIRGIN
Run NO i
>/ 18/75. _
OOSiRrfEO
f*
V,
/£?AG; OPACITY A
I SNVOR
_..2l.
iJ .
21,
21.
*!? .
20.
2 J .
H.
Id.
17 ,
17.
1".
19.
2 i .
21.
21. :
16. C
15.U
lto.5
!>•• 5
1"«.5
15.?
15.4
!<«»*)
11,. «
I1*. 8
14.7
I1*, 2
13. *
!<.. v
1 I.!*
12.7
If. 1
11.5
11. i
ia.% •
-?. i
-1.7
-1. 9
-1.9
-2 . 0
-2.3
-2.3
-1.5
-t.C
-.9
-1 .«.
-2.4
-3.1
-1..3
-3.5
-2.3
-.5
-.1
-.1
C. J
-.2
-.3
-.8
-.8
-1.1
-1.9
-2.3
-3.1
-3. "»
-3.5
-2.9
-2.3
-2.1
-1.3
2.1 16<*5 1,» 12. ll«fc ~*^ *'
1.7 lfl^f li « li» 13.9 •!.*» I.*1
1.9 I»fe7 9. 11. li*7 -2.* ^.2"J
1.1 1848 fl. !•«, 11. f -3.1 3.1
I.i 18<,9 7, 15. 1 «.••'' "3«6 3"?
2.1 185. 7. l<*. I-'7 -3.6 ,».&
2.*. 1851 6. U. . ... . 9.7 -3.2 3.2
2.3 1«32 fr. 11. 9., -2.5 2.5
1 5 lflcl 6. lj « 1.2 -1.9 . *O. _. .
l.J 1854 6. 9- 7«7 -1*3 1»3
.^
1.4
2.4
3.1
(^ £, , _ __ . _
fc.O
3.5
2.3
.5
.1
.1
* ^
, .2
.3
.8
.8
1.1
1.9
2.3
3. 1
3.4
3.5
2.9
2.3
2. 1
1.3
to
M
I
-------
WiSTHO»£LftNf) Ct»4L CO
LOCATION! QUINk.OCn W
'£°A TESTt RUN. NO
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.15 ~ 10.
:lt 10.
,17 10.
:18 11.
.19 12.
20 _li.
21 11.
.22 12.
i23 12.
,2« It.
;2S 11.
26 11.
i27 11.
28 11.
:29 11.
30 12,
,31 12.
•32 ...11,.
;33 12.
'3«. 12.
35 11.
36 11,
,37 11.
SUV Ok
' 13.
12.
12.
12.
1*.
13.
13.
13,
11.
13.
._ l*»»
iu .
!<, .
1 •« .
1 * r
U.
!«• •
l<*«
...If.
1U ,
H».
m.
i«f .
i ^ ,
iu ,
I1*,
!«•»
15.
i<*»
I* •
I1*.
!«,,
!•».
l-».
15.
15 .
15 .
15.
1".
15.
15..
15.
!•">.
I'.
IE, ,
16 .
•">;
11. r
I 1, "
11. .1
ll.u
11.6
1 1. 1
11.'
1 1 . *
11.9
1?.3
I?.1)
12,^
1 2.6 •
1 2. £
13. 0
1?. 1
11.9
12.1
6.9 . . •
6,4
7.1?
6.1
6. "
11,1
1 1.9
""12.0
12,3
1 1. 0
1?. ?
12. 1
13.0
13.1 ~ ' -
t'.l
1 ?. ft
12,9
13,1
13«^
1 *. "»
13. "5
1 I, I*
13.?
13.3
I 3.*-
13.'
13.?
13.;.
IT'-" 1>!r,-n/-r "fl TH L- ')i~,TH
i , \ e r : .
- u H
-,t
- ,6
- » (,
-.7
-.1
-.5
- , ^
-1,5
•1.5
•1. 0
•1.3
-1,5
-1.6
•1.6
•1. *»
•1,9
•1.9
•?. 9
-'5,9
•6,9
•7.0
•6.8
•F. . "J
•1.1
•1,9
•2.0
•1.7
•1.5
•1.5
•l.i*
•I.I,
•1.3
•1,5
•i . a
•1.9
•2.1
•2, 1
•2.0
•1,7
•1, «
•2.0
•1.7
"2,0
•2,2
Vr" V 1/If.T TOM
S '1 V t* ••
.'.
• 6
. *«
.7
.c,
.8
* -**
1. C
1.5
l.G
1. C
.c
.6
.6 .
. <•
,9
1.9
2.0
fe» 9
6.9
7,0
(•. 8
h. H
i.a
1.9
2. C
1.7
1.5
1,5
l.i*
1. k
1.3
1,5
1.8
1.9
2,1
2.3
2.0
1,7
1,1
2.C
1.7
2.3
2.2
Tl'ic
1636
1F19
1* %C
1C M
1 6<«?
16«-3
16-t
it<,5
lfii.fi
1 fc*,7
1 6tifl
1 6<«9
1650
1651
1652,
1 653
Ifi&b
IfeES
1656
1*57
1658
16P9
1700
17G1
1702
1703
A
•"LOH
12.
!?.
!?•
12.
1.?.
12.
11.
11.
1G.
11.
11.
11.
11.
11.
H.
11.
.10.
-0.
-0.
-0.
-0 L
-0.
-0.
-0.
-0.
-0.
_l70"•" ;
1,1 TV f-VV.-.
1 !>.*
IS.1*
1 3, *
1 J. r<
1 1. T
11,?
1 1. '
12. 7
13. U
12,*
1?. 5
12.1
11.7
13.1
12.8
12.7
1C. 6
11.?
-.3
-.0
-•o
-.0
-.0
-.0
-.0
-.0
-.0
-.0-
-.0
(/ -•«:
ij; I ? tr£.
O(_pMB
-2,1
-2.1
-2, 1
-1.9
-1,9
-1.6
-i « <5
-1.9
-2.0
-i.a
-1.5
-1.7
-1.0
-1,1
-1.9
-2. 2
-2.7
-8,1
-10.6
-11.3
Q.O
0.0
0.0
0.0
0.0
0.0
0.0
0.0
3.0
0.0
C.Q
0.0
-------
APPENDIX B-2
TOTAL VISIBLE EMISSION DATA
-------
9 REPOKT
PI. ftKTt WESTMOHELSI^G CO«L CO
UOCATIOM . 20, 18.3
17. 21. 18.8
17. 21. IB. 6
1*. 20. 18,2
i*. 20. iaa
_..!*« ,20,^ 17,6
H!
" l&l"
P.
n,
n.
.. 1.4. . ....
U.
u.
IS.
. 14,
14.
1?.
11.
11.
4*
9.
lal
19.
IB.
17.
I/,
18.
20.
21.
21.
20.
15.
15.
15,
16.
15.
16 1 '
16^
16.
17.
17,
16.
15.
14,
13,
12.
16.9
16, 5
16.0
16.1
16,4
16,9
17,3
16.9
16.5
16,0
15,4
"uls
14.5
15.2
15,4
U.9
14, B
14.8
14,7
14.2
13.8
14,0
13.4
12.7
12.1
11.5
11.0
10.8
:NQTH
OBS£R\
PLCHH
-2,5
-2.1
-2.1
-1.9
-2.U
-2.3
...-2.4
-2.3
-1.5
-1.0
-.9
-1.4
-2,4
-J.I
-4.0
-4.0
-3.5
-Is
-.1
-.1
.0
-.2
-.3
-Is
-1,1
-1.9
-2.3
-3.1
-3,4
-3.5
-2.9
-2,3
-2.1
-1,3
If.* DEVIATION
SNYDH
2,5 . .
2.1
2.1
1.9
2,0
2.3
.. 2.4
2.3
1.5
1.0
.9
1,4
. 2,4
3.1
4.0
4,0
3.5
2.3
.5
.1
.1
0.0
.2
.3
... .8
.8
1.1
1.9
2.3
3.1
3.4
3.S
2.9
2,3
2.1
1.3
HEFEKKNCt PATHLENGIHI 7. ft.
QBSEHvPO PATH I.IMJTH
CHSEHVEH
TIME AVERAGE OPACITY *VE«AO£ CBSErtVEW DEVIATION »fION
PLTHH SNYOU PLCHR SNYDR
1P4S in. 12. 11.4 -.9 ,9
Ifl46 In. 12. 10.9 -1.4 1.4
1*47 . 9. . . 13, 10.7 , -2.0 . .2,0 .._
Ifi4g A, 14. 11.0 -3.1 3,1
1*49 7, 15, 10.9 -3,6 3.6
1*50 ?, 14. 10.7 -3.6 3,6
1«51 6. 13. 9,7 -3,2 3,2
If 52 6. 11. 9,0 -2,5 2,5
1*53 *,, 10, , 8,2 _ -1,8 .. 1.8
1*54 *. 9. 7.7 -1,3 1,3
• • - • • -- •" • -
• . • • •' ' --• •
- • - .-.:•-
. . ... ... .... ,..; . ..
8 ii
i '
APPENDIX
3IBLE EMI5
m
H w
-------
PI ttnTi »F. SIMOrftL^C CUfil CO
UOCATICKI aulN*UCO * VIH6TMA
E°a TfSTt RUN N(J 2
TTM£
1*10
1*51 1
1*12
1*13
1*J4
1*15
1*16
1*17
1*V9
1*20
1*21
1*22
1*23
1*24
1*2S
1S26
1*27
1*26
1*29
l*3o
1*31
1S32
1*33
1*34
1*35
1*36
1*37
1*38
1*3Q
1*4Q
1*41
1*42
1*43
1*44
1*45
OHSfKvFc PAT*
AVEHAGE OPACITY A«E«Al
PLrnrt
17,
l*»
is.
•'•'I*. •
14.
.14..*
11,
"'u.'-"""
14,
14.
14.
14.
14,
n.
14.
1*.
10,
1C,
10. .'
19.
19.
in.
1*.
17.
1*.
' 1*.
U.
n.
11.
17,
l'«
. U. ""
-.1*.
I*1.
IB.
19.
SNYOH
Id.
18,
16.
15.
14,
14,
14...,
16,
17,
17.
18.
18.
18. -.„
17.
19.
22.
24.
26,
28, ... _ ...
29,
27.
25.
24.
22.
20,
19.
20.
20,
19.
18.
20.
24.
26.
28.
30.
3i>.
17,5
16,7
15.7
14.9
13.9
13.6
13.S
li.O
15,5
15.3
15.8
15.8
IS.fl
15,1
16,4
18.9
21,0
22.6
23,6
23.9
82.9
21,5
20.6
19.4
17.9
17,1
16.9
16.4
15.0
14.9
16,6
19,1
20,9
22,9
23.9
2i,4
CHSEHVEH DEVIATION
TTMg
ftVEHAGE OPACITY
SNYQi*
OPACITY AVERAGING PEHIOOI 6 WIN.
T1HE BASt 1NTENVAH 1 «lN.
OBSEHVEO PATHLENOTMI 7« ft*
HEF£MENCE PATMtENfcTHl 7. FT,
PATM LENGTH
QHSESVER DEVIATION
PLCHH SfcYOR
AVERAGE
17, S
16,7
15.7
14,9
13.9
13.6
13.S
15,0
15,5
15.3
15.0
15,8
IS.fl
15,1
16,4
18.9
21,0
22.6
23,6
23.9
82.9
21,5. •
20.6
19.4
17.9
17,1
16.9
16.4
15.0
14.9
16,6
19,1
20,9
22,9
23.9
24,4
. ,'B
.8
.7
.3
.1
.1
.6
-1.3 '
-l.l
-1.6
-1..7
-2.1
-2.3
-2.0
-2,4
-3,0
-3.3
-3.9
. -4.5.
-4.7
-4,4
-3.1
-3.1
-2.7
' -2.3
-2.3
-2,7
-3,9
-3.S
-3.2
..-3.9 '•
-4.7
-5,1
-S.4
-S.7
-5,6
.8
.8
.7
.3
.1
.1
,6
1.3
1.1
1.6
1,7
2.1
2.3
2.0
2.4
3.0
3,3
3.9
4.5
4.7
4.4
3.1
3.1
2.7
2.3
2,3
2.7
3.9
3.5
3.2
3.9
4.7
5.1
5,4
5,7
5.6
1*46
1*47
1*48
1*51
1*52
1*53
1*54
1*56
1*57
1*58
1*59
1*00
1*01
1*02
1*04
1*05
l*0t
1*07
1*08
1*09
1*10
1*11
1*12.
1*14
1*15
1*16
1*17
1*18
1*19
1*20
1*2J
1*22
1*23
1*25
1*26
1*?7
1*20
1*29
163Q
1631
H.
1Q*
2l!
21.
2?.
24.
2*.
2*.
2*.
24.
2?. '
21.
19.
le.
21.
23.
21 .
21.
21.
2i!
21.
21 ,
. 1* *__...
1*.
1*1 .'
1*.
1*.
1*.
i*.
1*.
1".
17.
1*.
19.
2ft.
2". .
24,
2*.
2«*
29,
27.
25.
24.
24.
2S.
28.
32.
34.
36.
37.
3S.
33,
32.
31.
31.
33.
36,
36,
36,
36. .
35.
33.
32.
31.
29.
28. ...
27,
25.
24.
23. ,
23,
23!
23,
23.
23.
22.
22.
22,
23.
23.
27.
28.
23, i
<22.7
22.3
21.7
• • - 25,3
27,7
29.7
30.9
30.9
29,4'
27,6
26.1
24.7
26.8
29.1
28,9
28.6
29,1
29.1
27.4
26,5
26.1
24,4
_, . 22.6
21.4
20,4
19,4
19,1
19,4
......; '--.'1^3
18,4
19.6
20.4
20.0
14.8
19.9
20.6
21.4
22.6
25,4
27,2
26,6
-5.0
-4,0
-3.1 ...
-2.3
-1.7
-2.3
-3.0
-4.0
-4.7
-5.3
-6,4
-5,8
-5,3
-5.5
-5.9 ._..
-6.5
-5.9
-6,8
-7,4
-7.3
-6.6
-5.7
-5.9
-5,8
-5,3
-.4,8
""-5 Is'".
-4,0
-4.6
-4.1 •'•
-4.0
„ -3.9
-4.1
-4.5
-3.7
-2.9
: -2.7
-2.3
-2,0
-1.7
-l.fl
" -2.2
-1,7
-Is
5,0 ' „ ,
4.0
2.3 ""• ~~" ' •
1.7 .: . . .;. ... . . .
2.3
3.0 -.; . : . ;-.;,.-.-,— ,
4.0
4,7
5.3
6,4 - .
5.8 :
' 5.3 '
S.5
5.9 __ _.„ . . _. -..
6,5
5,9
6.8
,'- N>
* »3 i
5.7
5,9
S.fl
4,8
. 5,3 ...
5.3
4,8 .
4,6
4,0
3,9 .. .._ . '_.
4,1
4,5 -•• ' - . .
3.8
2,9 -- •..-...
2,7
2.3 ' ' • '• . -'. .:
2.0
1.7
1,8
1,7
.9
.3
-------
JN NO 2 (CONTINUED)
'TMg AVERAGE OPACITY
SMYOH
30.
30.
30.
30.
30.
30.
29.
26.
23.
21.
18.
lo.
14.
14.
15.
14.
14,
13.
14,
14.
14,
15.
15.
17,
IV,
22.
25.
28.
31,
32.
31.
31.
32.
32.
31.
32,
32.
32.
31.
31.
30.
29.
27.
26.
25.
25.
PATH
.6.13
.634
*35
.636
'37
.'36
639
>4Q
'42
'43
.'44
>46
.'47
f48
>50
.'51
'53
'54
665
.656
'57
'58
*59
.700
701
702
703
704
705
706
707
708
.709
710
711
712
713
7U
715
716
717
3n.
3).
30.
31.
31.
39.
2*.
20,
111
14.
14.
1«.
17.
17,
IS.
n*
n.
n.
is.
i*.
19.
81.
24.
27.
20.
29.
3n,
31.
39.
39.
3?.
39,
31.
3ft.
29.
2P.
27.
2*.
2A.
2*.
2*.
V t" AOr.
29.6
30.1
30.3
30.1
30.5
30.6
30. •»
26.2
21.7
18.3
15.4
14.9
14.0
15.2
16.2
15.7
15.3
14.3
14.4
13.6
13.6
14,2
14.0
15.7
17,9
20.6
23.0
25.9
29,0
29.9
30.4
30.7
31.7
31.9
31.6
32.0
32.0
31.5
30.8
30.3
2B.6
27,7
26.4
26.1
25.6
25.2
CHSEhVEH
PLCHH SN
0.0
.3
.3
.3
.3
.4
1.2
-.3
-1,4
-2.3
-2.9
-1.1
-.0
.9
1.3
1.4 -
1.4
,9
.4
-.3
-.7
-.8
-.a
-.9
-1,5
-1.7
-2.0
-2.2
-2.3
-i.a
-1,0
-.7
-.4
.2
,:)
.1
.1
-.4
-.4
-.9
-.9
-.8
-.7
.3
.6
.7
UE'
YOH
0.0
-.3
••3
-.3
".3
-.4
1.2
.3
1.4
2.3
2.9
1.1
.0
-.9
1.3
1.4
1.4
-.9
-.4
.3
.7
.8
,fl
.9
1.5
1.7
2,0
2.2
2,3
1.8
1.0
.7
.4
-.2
-.3
-.1
-.1
.4
.4
.9
.9
.8
.7
-.3
-.6
-.7
DEVIATION
TIME
AVtHACiE OPACITY
PLCHH
1 71 e
1719
1 7?0
1721
17?2
1723
1 724
17?5
1 7?6
1727
1726
1729
173Q
1731
1732
1733
1734
1735
1736
1737
1736
1735
1740
1741
1742
1743
1 74^
1745
1746
1747
174fl
1749
1750
1751
1752
1753
1754
1755
1756
1757
1758
1759
1POQ
l"0l
Ifl02
1P03
27.
27.
2*.
2"».
2?,
2i .
19.
19.
19.
2ft.
2n.
2n.
19.
in.
1*.
14.
11.
I?.
1?.
11.
11,
11.
14.
14.
14.
IS.
1*.
17.
17.
in.
19. .
19.
19.
20.
2ft.
19.
in.
1*.
1*.
is.
11.
11.
in.
-n.
-0,
-n.
26.
26.
26.
26.
25,
24.
24,
25.
26,
27.
26.
27.
26,
24.
22,
20.
18.
17,
16.
15.
14,
14,
14.
13.
14,
15.
16.
17.
19..
20.
20,
20.
21.
22.
21.
20.
20.
19.
IB.
17.
16.
14.
11.
-0.
-0.
-0.
26.6
26.3
24.4
23.3
22.6
21.8
21. H
22.5
23.5
23.4
23.2
22.3
21.0
19.0
16.8
15.3
14.5
14.0
13.6
13.2
13.4
13.9
13.6
14.0
14.7
16.1
16.9
17,9
19.0
19.4
19.9
20.2
20.8
20.5
19.6
19.1
17.5
16.9
15.8
14.4
13.4
10,6
-.0
-.0
-.0
LENGTH
CHSEHVER DEVIATION
PLCHrt SNVOS
.7 -.7
.3 -.3
-.3 .3
-1.1 1.1
-1.6 1.6
-l.B 1.8
-2.6 2.6
-3.0 3.0
-3,3 3.3
-3.1 3.1
-3,0 3,0
-3,4 3.4
-3.3 3,3
-3.3 3.3
-2.9 2,9
-3.0 3.0
-2.8 2,8
-2.4 2.4
-1.7 1.7
-1.1 1.1
-.7 ,7
-.2 .2
.1 -.1
.4 -.4
-.0 .0
-.1 .1
.1 -.1
-.3 .3
-.8 ,8
-1.1 1.1
-.7 .7
-.5 .5
-.8 .8
-.8 .8
-.5 .5
-.6 .6
-.9 .9
-1.0 1.0
-1.1 1.1
-1.1 1.1
-1.5 1,5
-.9 .9
-.6 ,6
0.0 0.0
0.0
0.0
0.0
0.0
-------
I'lVIT
RUN NO 2 (CONTINUED)
PATH LENGTH
CBSEWVEH
TIME
1014
IPOS
JBOfr
1P07
1P08
IP 09
IP 1-0
IP 11
1P12
1P13
1P14
1«15
1°1 6
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1"19
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1"26
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1P32
1«33
1P34
1«35
1»36
1P37
1«38
1P39
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1P43
1P44
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RUN 3A (CONTINUED)
p
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1151
1152
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1154
1155
1156
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PI ANT I
WESTMORLAND COAL CO
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1.1
1.7
1.6
,9*
1.0
.9
,7
.7
1,0
1,6
1.9
2.1
OPACITY AVLHAB1MJ HE*IQD» 6
fIHE BASE INTEHVAL! 1 MIN.
OBSERVED PATHLENGTHI 7* FT.
RIFEHENCE PATHl-ENSTH« .. 7. fT.
•36SEHVFU
LENGTH
TTM'E AVERAGE OPACITY AVEHftGE
1*0 6
Id 07
1*08
1*09
1*10
1*11
1*12
1*13
1*14
1*15
1*16
1*17
1*18
1*19
1*20
1*21
1*22
1*23
1*?4
1*25
1*26
1*27
1*26
1*29
1*30
1*31
1*32
1*33
1*34
1*35
1*36
1*37
1*38
1*3?
1*4;)
1*41
If 42
1*43
1*44
1*45
1*46
1647
1*48
1*49
1*5(3
1*51
PLrHW
in.
1ft.
in.
in.
in.
in.
in.
in*
11.
1?.
11.
11.
14.
11.
. 1*. .
1?.
11.
11.
in.
in.
in.
in.
in.
Id.
in.
11.
l'»
1?.
1?.
171.
!.?.
11.
lit
11.
n.
i?.
i?.
\y *
11.
u.
in.
9.
9.
Q.
1.
9.
SNYDH
14,
15,
15,
14.
14.
u.
1 J.
13.
I*.
is.
16,
17.
18,
_. 18.
18,
18,
19.
18,
18,
....17.....
16.
16.
13.
14.
14,
. 1*.. .
14.
14,
14,
15.
14.
1*.
14.
14,
13.
13,
12.
11.
9.
8.
8.
6.
6.
6.
6.
12.2
12.4
12.4
12.2
' -"-12.1
11. 6
11.6
11.9
., ... .„ '12.7 .
13,6
14,2
14, S
. 15,2
' ; 15.3.
15.0
"' ." l4,9-~~
14.8
14.7
14.4
14,2
__. 13.9'.
13,2
13.0
12.4
12,2
12, S
„ ... .. 12.9
12.7
12,6
12.9
13.1
12.6
_. - , 12,4 ...
; .12.6
12.7
12.5
12.4
11.8
. . 10,8 .
10. 1
9.3'. '
8.3
7.4
7,4
7.5
7.6
OBSEHVE« DEVIATION
PLCHH
-2,0
-2.2
-2,2
-2,0
-1.9
-1,6
- .V
- .5
- .5
- .6
- .5
- .7
-1.7
' -2.2
-2.7
-3.0
-3,5
-3.9
-4.0
-3.8
.-3.4
-3.2
-3.0
-2.4
-2,2
-1.7
-1.3
-1,0
-.9
-1.3
-1.5-
-1.8
-1.6
-i.a
-1.5
-.8
-,7
-.1
0.0
.7
1 . 1
.8
1.4
1.4
1.3
1.6
SMYOR
2.0
2.2
2.2, ...:.
2.0
1.9
1.6
1*6 •
1.5
1.5
1.6
1.5
1,7
1.7
2,2
'....2,7:
3.0
3.5
3.9
4.0
3.8
... .3,4 '.
3.2
3.0
2.4
2.2
1.7
1.3
1.0
-.9
1.3
1.5
1.8
..,". 1.6 ......
1.8
l.S
.a
.7
.1
0.0
-.7
-1.1
-l!4
-1.4
-1.3
-1.6
N>
00
-------
RUN MO A (CONTINUED^ OHSFHVEC P6TH LENGTH
PATM LENGTH
TTME
AVERAGE OPACITY
«VEHft(ik'
CHStHVt'H DEVIATIOM
PLCHW 5I\YI)«
1*52
1*53
1*54
1*55
1*56
1657
1*58
1*59
170Q
1701
1702
1703
1704
1705
I70t
1707
1708
170,
1?1Q
1711
1712 .
1713
1714
1715
1716
1717
171 g
1719
172Q
1721
1722
1723
1725
1726
1727
1728
1729
173Q
1731
1732
1733
1734
1735
1'36
1737
9.
in.
in.
in,
in,
in.
in.
It.
11.
11.
n.
in.
9.
n,
' « «
a.
A,
9*
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In,
In,
4.
ft.
7.
7,
7.
A,
°.
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9.
P.
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7,
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9 •
1 *
,
1 ,
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A*
6,
6.
6.
6.
6,
1.
8,
9.
9,
9.
9.
B,
7.
6.
6,
t>*
6,
6,
6,
6,
6.
6.
7.
7.
K,
7.
e,
8.
8,
8.
?,
7.
7,
7.
7.
B.
8,
9.
8.
8.
9,
9,
9,
9.
10,
U.
7,b
7,B
8.3
8.3
8.3
a, s
9,1
10. 0
9,9
10.0
9.8
9.0
a.o
7.3
7.4
7,3
7.4
7.8
8,2
8.2
7.8
7.6
7,4
7.0
7,3
7,2
7,7
8.2
8,3
8,8
8.6
8.6
8.4
8.3
8.1
7,9
7.7
7.6
.. 7,0
6,7
6.9
7,1
7,1
7,1
8,1
8.2
1.7
2.2
2,1
2.1
2.1
l.S
,9
.8
.9
.8
l.o
l.o
1.1
1.0.
,9
1.0
.9
1 .4
1.8
l.B
1.8
i.i
.5
.1
-.2
-.1
-,2
.1
.8
1.3
1.*
1.4
1,6
1.7
1,0
,4
-.2
-.9
-1.1
-1.7
-1.9.
-2.1
-2.1
-2.1
-2.3
-2.*
-1.7
-2.2
-2.1
-2.1
-2.1
-1.5
-."J
-.A
-.9
-.8
-1.0
-1.0
-1.1
-1.0
-.9
-1.0
-.9
-1.4
-1.8
-1.8
-1,8
-1.1
-»S
-.1
.2
,1
,2
-.1
-.8
-1.3
-1.4
-1.4
-1,6
-1,7
-1.0
-.4
.2
.9
1,1
1.7
1.9
2.1
2.1
2,1
2,3
2,4
TTMf
173e
1 735
174Q
1 141
174J
1743
1744
1745
1746
1747
1748
1749
1750
P5J
1752
1753
1754
1755
1756
1757
1758
1759
1»OQ
1P01
1»02
Ifl03
JP04
1P05
100£
1*07
1S08
1*09
IPlO
Idl
1P12
1P13
1"14
IP) 5
1*16
lfll 7
ipie
1*19
l*2o
1*2}
1«22
1*23
PirHM ;
*.
7.
a.
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RUN NO 4 (CONTINUED) OeSE«vFC
AVERAGE OPACITY
PLCHH SNYUH
1P?4
1»30
1*47
in.
in.
in.
in.
in.
in.
in.
in.
in.
in.
in!
1ft.
In.
11*
11,
1?«
u!
IS
11.
11.
11.
a.
12.
12.
13.
13.
12.
12.
11.
12.
11.
11.
11.
13!
U.
14.
15.
16.
17.
ia!
1P4S
1«5Q
1*51
1 "52
1P53
1*54,
Ip55
1*56
1»57
1*58
1*59
1900
1001
1002
1903
1004
1005
1006
1007
1008
1909
IS.
is. .
IS.
IS.
IS.
•\*»
IS.
IS.
IS.
is.
is,
is.
IS.
is.
IS.
IS.
Is.
is.
is.
1 A.
13.
18.
19.
19.
19.
20.
21.
21.
20.
18.
1 7.
16.
15.
15.
15.
15.
IS.
15.
15.
15.
. 15.
IS.
LENGTH
CHStHv/EH DEVIATION
PLCHH SNYUH
OBSEHVFC PATH LENGTH
CHSEHVEH
10.3
10.5
10.6
10.7
10,9
10.9
11.4
11.4
11.0
10.8
10.6
10.9
10. S
10.3
_ ... 10.5
11.3
12.1
12.6
13.4
14.5
...;„ 15.4
IS. 9
16.4
16.4
16,4
16.5
......'_ 16.6
17.1
17.1
17.5
17.9
17.8
17,3
16.6
16.1
15.6
15.1
14.9
14,8
14.8
14.8
14,9
15.0
15.0
14.6
14.2
-.3
-.5
-.6
-./
-.9
-.9
-1.4
-1.4
•1.0
-.8
-.6
T.9
-.5
-.3
-.5
-.6
-.6
-.3
-.3
-.5
-.6
-.9
-1.4
-1.4
-1.4
-1.5
- 1 . 8
-2.1
-2.1
-2.5
-2.9
-2.8
-2.3
-1.6
-1.1
-.6
-.1
.1
.2
.2
.2
.1
0.0
0.0
-.4
-.a
.3
,s
.4
.7
.9
.9
1.4
1.4
1,0
.8
.6
.9
.5
.3
.5
.6
.6
.3
.3
,S
,6
.9
1.4
1.4
1.4
1.5
1.8
2.1
2.1
2.5
2.9
2.8
2.3
1.6
1.1
.6
.1
-.1
-.2
-.2
-.2
-.1
0.0
0.0
.4
.8
TlMf AVEHACiE OPACITY ftVEHAG
1Q10
IQ11
1012
10)3
1014
1015
191$
1917
1916
1919
1020
1021
1022
1933
10.24
PLrHH
1 ^.
I'.
11.
10.
10.
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11.
10.
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11.
1?.
li.
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SNYUH
IS.
15.
14.
14.
14.
13.
' 13.
14.
14.
15.
1-6.
17.
ia.
19.
2.0,
13.8
13.1
13.5
12.1
11.9
11.6
11.6
11.8
... 12.1
12.3
12.9
14.0
14.9
15,7
.1.6*5-
'<£• OHSEWVE« DEVIATION
PLCHH
-1.3
-1.5
-1.7
-2.1
-1.9
-1.6
-1.6
-1.8
. -2.1
-2.3
-2,9
-3.1
-3.2
-3.2
„.:_ -3.1
SNYOR
1.3
1.5
1.7
2.1
1.9
1.6
1.6
1.8
2.1 .
2.3
2.9
3.1
3,2
3,2
,__L 3.1 --•
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-------
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13 :»
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lull
1312
1C13
1C15
1015
1317
1018
1C19
1C20
1C22
1023
i12<.
1025
1026
1127
13?8
1C23
1G33
Iu31
1032
1033
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1035
1036
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_J.339
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16, 23,
16,
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16,
15.
15,
15,
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17.
16.
19.
21.
23.
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25.
25.
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-------
APPENDIX C
FIELD AM) LABORATORY DATA RELATED
TO PABIICULATE SAMPLING
Preliminary Data
Sample Run Data
Molecular Weight Calculations
Field Analytical Data
Sample Drying Data
Visable Emission Field Data
Cyclone Field Data
-------
C-l
Preliminary Data
-------
C-l
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if
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-------
r
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C-2
TRAVERSE POINT LOCATION FOR CIRCULAR DUCTS
PLANT
DATE
SAMPLING LOCATION _
JNSIDE OF FAR WALL TO ,
OUTSIDE OF NIPPLE, (DISTANCE A) _
INSIDE OF NEAR WALL Ttt
OUTSIDE OF NIPPLE, (DISTANCE B) _
STACK I.D., (DISTANCE A - DISTANCE B).
NEAREST UPSTREAM DISTURBANCE
NEAREST DOWNSTREAM DfSTJJJ®/
•CAmii ATOR C ,£. t
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SCHEMATIC OF SAMPLING LOCATION
TRAVERSE
POINT
NUMBER
FRACTION
OF STACK I.D.
STACK I.D.
PRODUCT OF
COLUMNS 2 AND 3
(TO NEAREST 1/8 INCH)
DISTANCE B
TRAVERSE POINT LQCAT101
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(SUM OF COLUMNS *i5)
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PLANT
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-. EPA (Our)
' . 4/72
-------
C-28
Molecular Weight Calculations
-------
" DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATE
COMMENTS:
SAMPLING TIME (24-hr CLOCK)
SAMPLING LOCATION /%,
SAMPLE TYP
£ • / Z
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, EPA fDur) 230
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT.
DATE,
x'
*~
COMMENTS;
SAMPLING TIME (2ihr CLTCK).
SAMPLING LOCATION
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28/ioo
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MOLECULAR WEIGHT OF
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PL, Ib/lb-mole
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,.,6
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EPA (Dui) 230
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT,
DATE_
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2 O
SAMPLING TIME (2«-hr CLOCK) /2i
SAMPLING LOCATION _jfVvin_£/
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EPA IDui) 230
4/72
-------
DRY MOLECULAR WEIGHT DETERMINATION
PI.ANT
DATE
SAMPLING TIME (24-hr CLOCK*
SAMPLING LOCATION
— ?7/
SAMPLE TYPE(('8AG)INTEGRATED, CONTINUOUS)
ANALYTICAL METHOD '
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02 READING)
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NET
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TOTAL .'
MOLECULAR WEIGHT OF
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6,00
2Z °\ 7
6 0 ' ' J
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ro
EPA (Duf) 230
4/72
-------
DRY MOLECULAR WEIGHT DETERMINATION
PLANT
DATE
( f>v ijun-i ft f <-.)>vtoWevt*yj vJ ) fV •»
COMMENTS:
SAMPLING TIME (24-hr CLOCK) \I'.X> 1**!+* > I 3'.
(O iCf k»~f •'Yf * ±^
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SAMPLE TYP^jBAGplNTEGRAJJED, CONJJNUOUS),
ANALYTICAL METHOD Ll
AMBIENT TEMPERATURE
OPERATOR Hc^g(Yv
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EPA (Our) 230
4/72
-------
G-34
Field Analytical Data
-------
035
ANALYTICAL DATA
PLANT
SAKPUKG LOCATION
SAKPLE TYPE i:
EUli NUMBER
f*ic"£ir MO ?***,§ • >^ 5-*'f '^*~
CLLAffur laHii • "*-*- - '-*
.
FRONT HALF
ACETONE \VASH OF NOZZLE^PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALF OF BILTER HOLDER
FILTER NUMBER _^
tare _J
net
.:i r? , y
CONTAINER.
CONTAINER
LABORATORY RESL'L'
FRONT HALF SUBTOTAL
BACK HALF
KPINGER CONTENTS AND WATER WASH OF
CONTAINER.
1MPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF LMPINGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
Rinse
voluaes ml nl
MOISTURE "
LY.PINGERS ^1 2 -
FIHAL vo[.ir;.E 32.1- m| //-^ mj
INITIA! V01 Iir:,? ' e c m! ' O 0
NFTVnil!V,R ^ '- ^-.mJ '5 ml
SILICA GEL
FINAI V.FIHHT /£3'*V E E
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EPA (Out) 231 "-'-"-
ETHER-CHLORO
EXTRACTION
CONTAINFR
BACK HALF
TOTAL WEI
ml
$ ml
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f
8
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FORM ' . -
SUBTOTAL
f,HT
ml ml
ml nil ^
ml ... . , ml -" '.';"•- p
TOTAL KOISTURE ^ 7/' ^
-------
C-36
ANALYTICAL DATA
PL AKT >*J £3 rfo^
^ a '- c2> *
DATE >*gve i'ff C^TS - -fW.*.f
SAILING LCCATiCN <3 <"-vv^ ** , iV • Vg*'
SAMPLE TYPE
OX NU.V.5ER
CLEAN-UP HAN _
CO;",*£,NTS:
FRONT HALF
ACETONE WASH OF NOZZLE, PfiOEE, CYCLONE {BYPASS)/
FLASK, FRONT HALF OF FIliTER HOLDER
T*'V_ /"
FILTER NUmBER !
tare JO
net
CONTAINER
CONTAINER
LABORATORY RESULTS
:RONT HALF SUBTOTAL
r«
BACK HALF
HflPINGER CONTENTS AND V-ATER V.'ASH OF
InlPINGERS, CONNECTORS. AND BACK
HALF OF FILTER HOLDER
ACETONE V;ASK OF LV.PINGEHS. CO?JKECTORS,
AND BACK HALF Or FILTER HOLDER
Rinse
voluces
WRINGERS
vni lir:.F i / O ml
ml
ETHER-CHLOROFORM
BACK HALF SUBTOTAL
V.-CJGHT
!_ Hi-
ml
ml
jal
,
5
ml
* /-• iN'r'.Ai vni n:,'E t 9 9 , ml
NET Vfil HV.F fD mi
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HET WEIGHT 2 f »* {
EPA (Dm) 231
4/72
/OO
?0 ml
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9
6
T ml
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e TOT
ml
jal
TOTAL KOKTURE
-------
C-37
ANALYTICAL DATA
.
XlVr^:T:,-:~'
* * V"
DATE
$ Am? LI KG LOCATION
SATaPLE TYPE
RUN NUMBER
SAMPLE BOX NU,',3ER
CLEAN-UP MAN
FRONT HALF
UBORATCRY RESULT
ACETONE VASH Or NOZZLE, PRC3E, CYCLONE (BYPASS),
FLASK, FRONT KAL.4OF FILTER HOLDER
FILTER NUMBER g'\3
tare
net
r*f
CONTAINER.
.
CONTAINER
FRONT HALF SUBTOTAL
BACK HALF -
G8P1HGER CONTENTS ANDTATER WASH OF
BSP1NGERS, COiuiECTCRS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF CuPIKGERS. CONNECTORS,
AND BACK HALF OF FILTER HOLDER
Rinse
voltnes
MOISTURE
GfiPINGERS ...... 1
FINAL VOLUME J. • -ml
CONTAINER
ETHER-CHLOROFORM.
EXTRACTION •
CONTAINER
BACK HALF SUBTOTAL
TOTAL WEIGHT
.ml
JBl
iifirifii vni II:,-.F '*«
fiFT vni ICF
SILICA GEL
FIN A! WF1CHT
INITIAL V'tiGHT &7'
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EPA (D«) 231
. ml /
ml
f
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1
>d &
ml ml
| « J
I *
£ f
.ml '._.
TOTAL KOISTURE
-------
ANALYTICAL DATA
SAKPLIKG LOCATOR ^flaP, W. (/A,
S«.'.?LE TYPE T
BtlHMIiy.RFR
SAmPLEEOXNUV.BER
CLEAN-UP MAN_
FRONT HALF
f ILJ
'I
3
ACETONE Vi'ASH OF NOZZLE. PRC3E, CYCLONE (BYPASS),
FLASK, FRONT HALF dp FILTER HOLDER
**i,
FILTER NUMBER 0» '
tare
net
COMMENTS:
CONTAINER
CONTAINER
FRONT HALF SUBTOTAL
LABORATORY RESULTS
r?
BACK HALF
WRINGER CONTENTS AND Y/ATER \VASH OF
HiPINGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF I.Y.PINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
volumes
MOISTURE
,IHPINGERS 1 2
vrfs FINAL VOLU«.E '_211_ ml
mi
ml
ETHER-CKLOROFORrJ
CONTAINER.
BACK HALF SUBTOTAL
TOTAL WEIGHT
ml
ml
JDl
,*' INITIAL VOLU".E
\ NETVOLUV.E
- FINAL WEIGHT
\ 7.' INITIAL Y.'EIGHT
-^-r"NET WEIGHT
EPA (Dui) 231
&
1 3 3 ml if ml '
ItOT.ff
+11'* t { 8
4^>^*e E «
' 7> * g 8 R
S*1
.ml ._.
4 5 , •• 6
jal .
TOTAL MOISTURE 1*2'
-------
C-39
ANALYTICAL DATA
PLANT._JsL£
JUN231375
FRONT HALF
.
COfi'i'iEKTS:
RUH mn.'RCR TH-j? frV^feic^ , «utr-
SAKPLE BOX NUMBER '^, "*
CLEAN-UP MAN • ^WaT
I P.
ACETONE BASH OF HOZZLE. PROBE, CYCLONE {BYPASS},
FLASK, FRONT HALF OF FILTER HOLDER V
- . f
/. lW ^ittl
tare 0.
net 9
LABORATORY RESULTS
CONTAINER.
CONTAINER
r*
-
- ""
FRONT HALF SUBTOTAL
r?
BACK HALF
IMPINGER CONTENTS AND WATER WASH Or
WPiHGERS, CONNECTORS. AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF ttPINGERS, COHKECTORS,
AND BACK HALF OF FILTER HOLDER
Rinse
volumes
MOISTURE
KPINGERS'
FINAL VOLUME
INiTI'.L -yOLU:,*;!
NET VOLUulE
ml
l/,f ml
'£ c ml
ml
8
GEL
FINAL WEIGHT
INITIAL WEIGHT
NET WEIGHT
EPA (Dai) ?31
4/72
ml
ml
CONTAINER
ETHER-CHLOROFORa
EXTRACTION
COKTAIHER
BACK HALF SUBTOTAL
TOTAL WEIGHT
ml
.ml
J3l
-
*
^_ml
OC
jal
.ml .__^
TOTAL E01STURE_ZA£/ *~...
_rs
-------
ANALYTICAL DATA
COi'iY,ENTS:
^r^— ^JUN 2/cia/\ -JUN?:
$,V,'pi !Nn i nr.ATsn:,1 C?L' ;»c ;<•>-• en W . V
S^KPIFTYPF P*RTi«,C S.-U" PlSTR,«
RUN fJiiMRFf? T~H-~ £» • (s> ^ I TH HH
S&:,'.PI F RHX ?/li',*RFR ^ , «5^W : vnnir.'.F /c^ mi ltd
KETVOI ll'.'F ,,'?' H ' ml ^"2-
XN^^ 7 * '* ^*2*t
SILICA GEL . !
FINAL V-'Ei-HT ^*- -<^J^MJCit_ Zf*>— "7-c*^t ^^ '/^
'^ ^v^l^^^/i^SG^v- ^^7q7f
3j7li(0 *j./A^ /Ji^tr—i^ /./I <(T_p_ , ^ .^ , ^ -..
»Le '•• • : '• - -T2^!/""^ 't***7***-?^' ' JL,
^^3 • , f£t£*. ^M^lhi^T ,c'-*-^ /-J"
^i'tf-r- ••••:'- ;- .".' " :-\,"-r\:: ••>•:•. •••"•''.-• •-.
-^ P«(ff '• '•'•••• ' '••'• ' LABORATORY RES'JL
\ vJ
Ef^PASSl. CONTAINER
-7 . •
CONTAINER
5,4^ *
/ * .....
L: ?W; FRONT HAI FSURTOTM
/
CONTAFWFR, '
" . ETHER-CHLORCFOR»: . • '• :: ••'•
FXTRAC-Tin??
CONTAI'-'FR " '; "•'"'
BACK HALF SUBTOTAL ' '• - - "" "
.'•-' TOTA1 V.'FIRHT - ' ' • ;
il ml _n\l , ml
/ t*< 1^-\ ?***- -
3« '• • 4 5 6
ml -^ nil ml .' «1 /
C1 /"^ f/\~ (j/
<• ' ' « ""^ **
ml ^ m) T^l m) r~
WU "
E £
E ' -5 - •~l
p r TOTAL 1,-OlSTURE "JJ»- ""
TS
' 5
p.*
r|
r»C
r*;
f"*T
1
t
-------
.C-41,
ANALYTICAL DATA
PLANTJ^L
DAT? QQ»-'C 15.;^?r- W£ Q i-1-.•_-.••*
SAMPLING LOCATION $'* "'^33 £> , Verr '.z7o
r ACETONE WASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
'i FLASK, FRONT HALF OF FILTER HOLDER
j^w£-| (-
,- _^^ __v
FILTER NUu'BER £_
tare
- net
JL£!i_9
ff-
'"BACK HALF
IMPINGER CONTENTS AND WATER WASH OF
RlPINGtRS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER
ACETONE WASH OF WRINGERS, CONNECTORS,
AND BACK HALF OF FILTER HOLDER
A'iffr^T '*^
ml
volunscs
MOISTURE "~
IKPINGERS I 2
FINAL VOLUME ___H^L. ml /?"3
INITIAL VOLUME __J±iL ml fc°
NET VOLUME L
ml
COto.ENTS:
LABORATORY RESULTS
CONTAINER
ml
ml
SILICA GEL'
f FINAL WEIGHT
-£~ INITIAL WEIGHT
_±ZJl'g
f ^f-a I
— I
— I
U*&' EPA (Out) 231
V^' 4/72
CONTAINER
r«
FRONT HALF SUBTOTAL
CONTAINER
ETHER-CHLOROFORM
BACK HALF SUBTOTAL
L WEIGHT
j»l
.ml
jil
ml
jnl
jnl
-\_/ ml
TOTAL r,;01STURE_££/'f':
-------
ANALYTICAL DATA
PLANT
75"
i *> uicoO
SAKPLSNG LOCATION
SAMPLE TYPE *Vft*cuuft*V
RUN NUMBER S.
- "2.
SAKPLE BOX NUMBER
CLEAN-UP MAN
FRONT HALF
ACETONE WASH OF NOZZLE, PROBE, CYCLONEfBYPASS),
FLASK; FRONT HALF^OF FILTER HOLDER^
NUMBER 9- Urtb ': 6-^
tare ^-.?fc^3 g - e- 3'
net ^/. 3*>i
COKTAIliER
LABORATORY RESULTS
FRONT HALF SUBTOTAL
BACK HALF
COffTAlNER
IMPINGERS, CONNECTORS, AND BACK ,
HALF OF FILTER HOLDER
ACETONE WASH OF tuiPlNGERS CONNECTORS
^ AND BACK HALF OF FILTER HOLDER /
H - . flf L • •
' / jl&ts'- ^rs ^
* ' { *w4\'r^
volumes / ml ml
MOISTURE / '
IKPINGERS 1 2 3
FtNAl vni IIF.-F AiC" m| /^^ ml *
INITIAI vmilMF /* ^
NFTVHMI---F /^' c' ml ^/fc ^l /
.. 'SILICA GEL , •
FINN VrfinHT ^"°3' g E
INITIAL \VpinHT ^T/- e g £
\ NETV-TIGHT , */'*E P.
ETHER-CHLOROFORM ; , "•'. •'..: ••..•; ' .
FXTRAr-TinN • ''-'"' • "• ":;'; ' ''•'•''. "-
CONTA!«FR , ~?
BACK HALF SUBTOTAL --
TDTA1 WFIRHT "i
nil ml ml
4 5 ' 6x_
isil /ml >^ |»1 i/
^X" '"^
ml ml ml ' • f^"1
1
1 ^ _ ,
£ TOTAL KOISTURE 2. 4' ^» c
EPA (Dui> 2]
4/72
-------
C-43
ANALYTICAL DATA
PI ANT
DATE
SAMPLING LOCATE
SAMPLE TYPE r^*
RUN HtiaaER ^ *'
C - 3
SAMPLE SOX NU:.-3ER.
CLEAN-UP MAN §
/~», t —
cv">-
t> Co
"&" i
/
CO;.".'ENTS:
? O
/ ^V-^c*». A^uf.'&^f V-?s**
FRONT HALF • .
ACETONE WASH OF NOZZLE, PROBE,-CYCLONE (BYPASS),
t?r^ FLASK, FRONT HALF OF FILTER HOLDER
CONTAINER
CONTAINER
FRONT HALF SUBTOTAL _
."**« c^-t^
BACK HALF
-
IMPING ER CONTENTS AND Yi'ATER Y/ASH OF
IHPIHGERS, CONNECTORS, AND BACK
HAI F Or FILTER HOLDER
trPTHMF \Vfitu OF lY°l?tMFrft COf'N'FCTQRS
AND BACK HALF OF FILTER HOLDER
-
n.in5e
volwnes ml ml
MOISTURE
RSPINGERS 1 2
F|MAI VO! tI"F ^ f $ ml / ? G> ml
IhiiTifl! vnilir.'F /'«. ml /cc
NFTV^HlVf , ml ,r,l
, , r ^?,^v *** JF Gtf 4^*. * *"
SILICA GEL ^
FINAt V,'FI"HT if-J'Tg g
r INITU»I v.TiniiT *irJ?£i g .
HFT V'P'OUT 2^ '^g B
EPA(Dur)231
4/72
CONTAINER • . ri]mi •. ••"'•• ----- - -
• "ETHER-CHLOROFORM "•'•' ':'"\\-'" "'••'•: ',
•" FXTRACTION ' ''•" ' '-;c**:";': ' " ' ; ' ', ' '•
• ^j';':Ji • • ' • ' • "
'• " cnNTAtNFR - ' - •' v -*-'•-"• '"- •• -
BACK HALF SUBTOTAL '
• *•
TOTAI V.'FIRHJ
nil ml ml
3.4 5 "->:- 6
* ml , / pi /ml ~/
ml fnl ''• ml
' -- • • • v • " ' '
X
• I
g TOTAL KOISTURE ^« '•
\ s'
f -
'„ _r?
.;
w«
(~r
-***»«» -
El
r
-------
C-44'
ANALYTICAL DATA
JUN
LING I
LE TYPE
WUK3£R_
A&
.•t *ID P< r **
Ui"Ur JI'AH.
NT HALF
11 i i M *i-—! «, - '".[--
lETONE Y.'ASH OF NOZZLE, PROBE, CYCLONE (BYPASS),
FLASK, FRONT HALrJJF FILTER HOLDER
LTER NUMBER -0 > M 5 Q S .._
tare
net
;K HALF • ' .;-.;:: ,\*-
'INGER CONTENTS AND WATER V/ASH OF
IMPIHGERS, CONNECTORS, AND BACK
HALF OF FILTER HOLDER . ../. -.- :
AND BACK HALF OF FILTER HOLDER
volumes
STURE
ml
CONTAINER A;
k£r—*j ^V*.
'1-
•iy^
;.--^U,
'COHTA!HER"ii±I
FRONT HALF SUBTOTAL
ETHER-CHLOROFORM'
BACK HALF SUBTOTAL
WEIGHT
p»l
ml
ml-
'INAL VOLUmE .
\L VOLUME,
.mi
.ml
ml
t00
ml
'•3
ml
4 ;
.-; 6
JCAGEL
:!. g
HITIAL T:
IET WEIGHT
'A (Dm) 231 „
4/72
2-7"
I
• I
3i «? '&
TOTAL MOISTURE 3'Z- *
-------
C-45
ANALYTICAL DATA
DATE.
SA?u?LlKG LOCATION _ki
SAmPLE TYPE f.verted
RUN HUmBER__Qjl£l
SAfuPLE BOX NUMBER
-.CLEAK-UP. MAN
.--.c''
FRONT HALF
ACETONE Y/ASH OF NOZZLE, PROBE, CYCLO.'.'E (BYPASS),
FLASK, FRONT HALF OF RkTtR HOLDER J
FILTER NUMBER
tare
. net
-------
C-46
Sample Drying Data
-------
34
to
C-47
___
20
i 25
3O
Work Performed by%
Tirb or Purpose;
.
.}j
Project No.j 2.g/2-l7/V Dare of Work:
£&Xt/L?$.
Continued from:
S*u*pur
£.0.Q
AV '
' P^xJl • T"W, ; P ••*#•*«*.
1 ***?*•<
' i • 1
jgvsuw, , : i i
• ! . ! i • •
5^771
i I J
—_ m_P> — %j*.
Hf.C
^ we
w c
vw
10
15 i I | ' 20 !
25
i i !
30
Entered by:
Date:
Continued to:
Performances of this work observed by:
Disclosed to and understood by me:
Date:
Date:
-------
10
15
2O
25
3O
Work Performed by:
Title or Purpose:
.
Date of Work: 9**^* ''ll^f-
Continued from:
.we t«
w cu
10
15
._ 2O
1WC I
_25
J-OCI1
30
1O
15
20
25
3O
Entered by:
Date:
Continued to:
Performances of this work oiiserved by:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
1O i
15
20
i " 25
30
Work Performed by:
TiHe or Purpose:
No-
Continued from: /b, 3 S
5 rf*=Jft_
77.
25__
3O_
i 5
1O
is ! i ! : 20
i 25
; Entered by:
Date:
Continued to:
'Performances of this work observed by:
Disclosed to and understood by IB:
Date:
Date:
Date:
Date:
-------
Work Performed by:
Title or Purpose: T^ ^LD
.050
Project No.
„ t*.?of.to*r*
var* ...)...-•:
of
Continued from
A*
;0
CX? hi,
1 0 WOO
JO
&KV-
-1.5
2O
25
51
10
15
20
2S
30
30
ed by:
Date:
to:
finances of this work observed by:
• Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
38
C-51
1,0
ts
20
2S I I I I 3.
Work Performed by:
•: IT* *****/
Project No.
Z7 /if Pare of Wor
Title or Purpose:
CWtf I
9
Continued from:
l^^jC^^
"
--4JL
M*>
.?*
ful.
p,
A I-
: j ; ,\V&C- \$0
3gy^gi-,§^ufcw A. Arf>£X 3i^^3. \:?^^Ui,tcL^Q
to
1'5 f |
20
25
Entered by:
Continued to:
-f^-
Performances of this work observed by
Disclosed to and understood by me:
Date:
Dale;
Date:
Date:
-------
Vork Performed by
fitle or Purpose:
/ -^"^ U
' Project No. $?f?2-
FcO> S%ciK /IA^H-M.^
y Date of Work;
Continued from:
ff
4=-
=J—J.
.10
!
|
_15
.. $+«?£-
20
^
25
.3C
t.O
! 15
2O
25
30
ered iy:
Date:
Continued to:
formances of this work observed by:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
10
15
20
25
Work Performed by:
/\
C-53 ,
Project No.)! 'IS H ' >• ?' ^ Date of Work:
, Continued from:
""
10^
£^ Ttf-3,
- 3
10
is :
20
25 !
31
Entered ty:
Date:
Continued to:
Performances of this work observed by:
Disclosed to and understood by me:
Date: •
Date:
Date:
Date:
-------
41
10
15
i 20
25
30
Work Performed
Title or Purpose:
C-54
'*"' s Pr°'ect No. $.1312 - » 7 « V Pate of Work:
Continued from:
/
J ''
(Se
«r* •
10
15 {
: 20 i
25
I 30
ntBfed by:
'erformances of this work otaved by:
Date:
Continued to:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
X
*
(•)
(b)
(c)
not
•
Imping* \.o ,
Set No.
1 Total 84.
Mass
Imping, ^-j
Set No. —
2 1*1
EBK-2 0.7
y±l 1|5ii!f
2&£
" * 3 &M
\^
±i
4
IfeS
U2I
, ??•/
QMO-5 |.^f
\3rtf«tmg Front
Half
\ ?»4m9 Back
n Half
3$a»l S«3 30* •/
?2,
Ml?
V
set of samples
all 5 runs, U
} Fiber glass
) W'lter and w
n/., S
*l (J[j
, (Backgroun
iis sample .s
filter. (2i
iter rinse c
rr. ^. Ethor gx,trocj:iQn. from
f the im'pinger jars and cc
^•(^
•^
il
169— L
11-0
n«
— •>•
^-
Ji
» * • jp»
EBK-6 |.o
Xl:2._ og Front
X Half
\ y.'^.reg Back
/ Half
id)
et does not include a. probe & nozzle wash,
Acetone rinse of nozzle, glass probe, 8, front
>f impingers, back half of filter holder &
the water and water rinse of the impingers,
mnectors.
Date;
-------
44
l I 1 is"
j ......... 1O
I , i 15
20
I ZS
30
Work Performed by:
C-56
Project No. )J 2^7 1
Date of Work:
Titte or Purpose: ' r
Ru/K:f*^$Mc~ d
Continued from-.
EPA NoTFinal
S-75-001
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
U) Fiber Glass
f.ilter
Filter M<
o[2) Acetone rinse of
nozzle, probe, &
filter holder
Evap. dish No
Total vol. jfP ml.
I-'
5(3) Water & water
! rinse from
f imping, conn. &
l- back half of
filter holder
Evap. dish No
r Total vol. J7£p_ Ml
>o;4) Chloroform &
ether extract.
of (3) above.
(extracted first}
Evap. dish No
Total vol. ^ ml
25'
Final acetone *
rinse of imping.
jars and connec.^,(
Evap. dish No.^21
Total vol»3/" ml
0.i31t>-
80$
-t/K
_.
. 07?
V,
3
e*&k
"^
kf-f^^
'46.
3O
I'O
15
20
25,
Entered by:
Date:
Continued to:
Performances of this work ofiserveo1 by:
Disclosed to and understood iy me:
Dati:
Date:
Date:
Date:
-------
u-:>7
10
15
20
25 !
Work Performed by:
Project No. JJ 1%1 *
Date of Work:
Title or Purpose:
Continued from:
EPA No. Final
S-75-OQ1
U) Fiber Glass
f.llter
Filter Nc
1O[2) Acetone rinse of
nozzle, probe, &
front half of
. filter holder
Evap. dish No
Total vol.f2£_ral.
ISL
[3} Water & water
rinse from
imping, conn. &
back half of
filter holder
Evap. dish No.
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
r
L
i
i
r Total vol. &ef ml!
,°X) Chloroform & 7
ether extract.
of (3) above.
{extracted first^v
Evap. dish No.&M "^
Total vol. ml
25,
.5) Final acetone
rinse of imping,
jars and connec,J.'V
Evap. dish No.fJV
Total vol. 31* ml
•* H if 4"7, 4 ( w.itW n
3^3C, 5^' ^**A
'
'
;
^^W lt-1 ^L~
cnJ. A^M.-
t^jt^f-
3Q_
> 1
1 s i
1 i 10 I t
! t;5
I
20 | |
! 25 i
1 :
Entered bj;
Date:
Continuei to:
Performances of this work observed by:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
C-58
10
15
20
25
3C
Work Performed by:
'" ..... " .....
Title or Purpose:
Project No.
--
Q N C *
1- 2?
Date of
Continued from:
EPA No. Final
S-75-001
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
[1) Fiber Glass
filter
Filter N
Al.3735
D.
Acetone rinse of
nozzle, probe, &
front half of
filter holder
Evap. dish No
Total vol./lV ml.
- t
'3) Water & water
rinse from
imping, conn. &
back half of
filter holder
Evap. dish No
i Total vol. _
',4) Chloroform &
ether extract.
of (3) above..
(extracted first)
Evap. dish No.
Total vol. ml
5,0 *^ -•
47.
I
'5) Final acetone
rinse of imping.
jars and connec^t^-
Evap. dish No. £_
Total
! ! 5
10 !
15
20 i
25
30
Performances of this wort observed by:
Date:
Date:
Date:
Disclosed to and understood by me:
Continued to:
Date:
Date:
-------
50
C-59
all 5 .10 15 .'20 ! 25 |
ifiF jT tts
Work Performed by: 4^7^^ Project No. Date of Work:
Title or Purpose: 0 V C - :jg*Mj$- 0^^"~ 1 Continued from:
. ./ i !
i :
_ S-
1) Fiber Glass
f.llter
Filter lfo«J?*£'4
0 2) Acetone rinse of
front half of ,
filter holder^gj*
E van * d 1 sh No A ^^^
Total vol. /ft^ mi,
s.
3) Water & water
~ rinse from
— imping, conn* &
•back half of
filter holder
— Evap, dish No,
,'0 Total vol, 9 S ml
4} Chloroform &
of (3) above*
(extracted first^
* P* **A5n MO, M
_ Total vol. ml
:s
5) Final acetone
r~ rinse of imping.
L jars and connec.
| Evap. dish No,
j~~ Total vol. 3*5" '..»1
o
EPA No,1 Final Tare Weight Remarks —
75-001 Wt. Change
grams grains mg
; 1
-*/4f Sr-f^S^ ' o> "50,0 ' W'5 \ i08tt^
-4*fa o>mw 1 0* wft siti ^
, •** '. 1
' 1 . . '
t :
^Wi~ *' ' • ch"
Lr
^ : :
•$* tv«JU*JL ^
^im?, ^vqlft ¥4< 707^ g-j.o tZ&CT^Z.
> M %*9 *^^^v^* £> * ' Cj> tf i**4f*
A^t ' ft I — a +•
. Z'^t^
ft* :
». '•
rftftf. 5).!J7^ ft* r?33 ^ ?.. < ;
• • :
i :
— yv/^47. ?t9^r ^7- 36 ^"/ 5. /
0 i { 5 | 10 | IS i 20 | | i 25 | |
Entered 6jf: OT>V!-»V~ Date: Continued to:
Performances of this work observed by: Disclosed to and understood by me:
Date: Date:
Date: Date:
-------
30
•JL
—10
JLS
*/!« A**
25
.30
30
Work
Title or I
10-
15..
20-
25_
i
i
i
i
30
o !
.
I ! 5
10
1
I
1
[
: 1
I i is 1 i 20 : .
Pnnti
-------
52
Work Performed by?
C-61
10 i
15
20
25 <
3(
Project No.
Dare of Work:
Title or Purpose: (5 '-j C ^|^v> *f^ W MC *5 Continued from:
A**. Ju*>« If, (^ -*<«•'*"»",
-,-.,-,-„„,, . «. .....
c FA wo * r* i ndi i are wo inn » Ke raarx s
S-75-001 Wt. Change
—
1} Fiber Glass
filter
J Filter lto.QMG-5-*-
° 2) Acetone rinse of
nozzle, probe, &
front half of
filter holder QfjC^I
Evap. dish No .-""'>*
Total vol. ;ff__ml.
5
3) Water & water
rinse from
imping, conn. &
back half of ^
filter holder ^^
Evap. dish No. __
,0 Total vol. Jfo>?-ml
"4) "Chloroform &
: ether extract.
: of (3) above,
r (extracted firstK,
— Hvap. dish No. Q *
Total vol. jsl
,5) Final acetone
j- rinse of imping.
_: jars and connecj£4<
-Evap. dish No.fr .\
Total vol. 5?5" ffll
grams grams ' mg
f- • : : ; ;
-V5*/ ^.j^SJo7' 6.- 11 5J %*?• O ^2 &Mt\«.
O>' HcWt* • a. Hit 3*}.;% ^>^~ *}&•#
-•'—'.:
it Cl^ , / itjt^A.**^ —
-453 ,
SI 2SA3. fl /t>57
-------
C-62 _,.,
! ! ! 5 1 • | ! 10 | i ; 15 | 1 1 20 • i ! * 25 | | i 30
Work Performed by^f^j^/MfV ' Project No. Date of Work:
Title or Purpose: U^^JijK. ^*^W*%3Vj-" <^H£ it ^TEJC, 5(.^fl/J^C Continued from: ;
i
S-
) Fiber Glass
filter
Filter No. &*.
:) Acetone rinse of
nozzle, probe, &
front half of
filter holder Q£®
Evap. dish No, *
Total vol.**0 ml.
i) Water & water
rinse from
imping, conn. &
back half of
filter holder<3££j.
Evap. dish No._J3_
Total vol. 200 ml
») Chloroform &"
ether extract.
of (3) above.
(extracted first^.§»«
Evap. dish No. °jf .
Total vol. tso ml
>*
5) Final acetone
rinse of imping.
jars and connec.
Evap. dish No.
Total vol. ral
EPA No.1 Final
75-001 Wt.
grams
•i
—UGt~3.
,t ' • \
6/1*
-4^
i
I
Tare nsi'jht Remarks
Change
grams mg
I j :
1 - '
: -••'.' ' - ; 1 • • ' . .. - •
' ' • ' -• '.i •• •• ••••'• '.
j *«
i ^ .
4/*' *^1&O 6 , y Qutf^J-v^l*' * ^StcX^'K.
• V-vTCT^*£ >%«• /!^***-**-'
' i ' -
• j
'
! '
i '
i f%.jjLf**jt
_ •?>"» \j1rf1* ff$^_ / / « £/
i/Q
-------
54
C-63
10
15
20
25
Work Performed by;
Project No.
Title or Purpose?
Xt"L«» /\.vUf'.'.. ~t~«»*Ar i; t-T -i'i
Date of Work:
Continued from:
Ci--'.'_.:
EPA No. Final
S-75-001
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
1) Fiber Glass
f.ilter
I Filter Mo._
102) Acetone rinse of
, nozzle, probe, &
' front half of
|~ filter holderwc.&
!_ Evap. dish No. ^
P Total vol. G ml.
is
3) Water & water
rinse from
\_ imping, conn, &
back half of
filter holder
: Evap. dish No.
Total vol. __mlj
Z04) Chloroform & "
,_ ether extract.
\ of (3) above.
- (extracted first)
_ Evap. dish No.
Total vol. ml
25
5) Final acetone
rinse of imping.
jars and connec.
Evap. dish No.
Total vol. ml
30
10
IS
20
25
Entered by:
Performances of this work observed by:
Date:
Date:
Date:
Continued to:
Disclosed to and understood by me:
Date:
Date:
-------
C-64
10
15
20
25
Work Performed by:
Title or Purpose:
Project
- gff ft ~/
1* tf j'?
-1116 Date of Work;
Continued from:
EPA No. Final
S-75-Q01
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
1) Fiber Glass
f.ilter
Filter Mo.
102) Acetone rinse of *
nozzle, probe| &
front half of
- filter holdertft^
Evap. dish No.
Total vol./ l*y- ml.
is
3} Water & water *
rinse from
imping, conn. &
back half of ,
" filter holder -&*>
Evap. dish No. £,
Total vol. f?Q_ml
4"5~ChIorbform & ^
• ether extract.
j of (3) above.
*~ (extracted
;.. Evap. dish
Total vol. ml
5) Final acetone
rinse of imping.
jars and connec^i, ~^°S"
Evap. dish
Total
/..,
o- 3
30
10
15 • 1
2O
25
Entered
Date:
Continued to:
Performances of this work observed by:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
C-65
57
10
15
i 20 <
, 25 I ! f
31
Work Performed by:
Title or Purpose:
£"0 ft .
Project No, JIlfT. I -1**7} Date of Work:
» 2. &//•?/? c Continued from?
EPA No. Final
grams
) Fiber Glass
filter
Filter No.
>) Acetone rinse of *
nozzle, probe, &
front half of -,
filter holder 0*
Evap. dish No*
Total vol." ^ mi.
1) Water & water
" rinse from
imping, conn. &
back half of
filter holder ^s*
Evap. dish No.
Total vol. Mo ml
Tare
grams
Weight
:har
ing
Remarks
7/7/7J'
.f l^_(.J
ether extract.
of (3) above,
(extracted firstly
Evap. dish No.£_J
Total vol. ml
j) Final acetone
rinse of imping. -h
jars and connec.it>—
Evap. dish No.fff^
Total vol. ff- ml
30
47.
61.
57,42^7
1O
15
2O
25
b»:
Bats:
Continued to:
Performances ol this work oiserved hy:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
58
G-66
10
15
2O
yg
Work Performed by: ffa
Title or Purpose:
^/fe>. Project No. )1 t^H- 2 7/f Dare of Work:
-— * •
€& K ^ t $** ** ^ (s/l^/l S Continued from:
. . « i • ,.'.'••
EPA No.
S-75-001
Final
Wt.
grams
Tare
grants
Weight
Change
mg
Remarks
5 1) Fiber Glass
filter
Filter No.
io2) Acetone rinse of
Q nozzle, probe, &
~~ front half of
U filter holder
Evap. dish No.^
Total vol./'$£> ml.
3) Water & water
!— rinse from
! imping, conn. &
j back half of
t- filter holder ff.^
! Evap. dish No.
I Total vol. _
20 4) ChTorbform 8.
ether extract.
of (3) above,
— (extracted first^
_ Evap. dish No.J^J
"~ Total vol. ml
25
5} Final acetone
!_ rinse of imping.
I jars and connec..^},
j~ Evap. dish No.ff_J
U Total vol. -ry ml
48
30_
3 1 !
5
1 I i t'O ! | | 1.5 | 1
j 20
1
1 25 |
|
1
. Entered by:
Date:
Continued to:
Performances of this wort observed by;
Disclosed to and understood by me:
Date:
Date:
Date:
-------
0^67
1O
IS I [
59
j 20
25
3C
Work Performed by:
TUIe or Purpose:
Project No.
y"
Dare of Work:
Continued from?
EPA No.' Final
S-75-Q01
L) Fiber Glass
filter
Filter No.
Wt.
grans
Tare
grass
Weight
Change
mg
Remarks
• dbff*.
I
2} Acetone rinse of
nozzle, probe, 8. '^27
half of
filter holder
Svap. dish Ho»
Total vol. IT" ml.
3) Water & water
rinse from
imping, conn. &
back half of
filter
Evap. dish
Total vol. 5"¥o ml
4} Chloroform &
ether extract*
of (3) above.
(extracted first),|
Evap. dish No.ffl'g
Total vol._ mi
__:_. ^.m/ o^ ^J^.:
5) Final acetone
rinse of imping. -
jars and connec«^ y^
Evap, dish No. ^ .T
Total vol.
30
43.3254
'~
# .
^
10
15
20 • i \ | 25
Entered by:
Performances of this work observed by:
Date:
Continued to:
Disclosed to and understood by me:
Date:
Date:
Date:
-------
60
C-68
10
15
20 I
25
Work Performed by: fyou^fr
1 Project No, J 14 7 2' if ^
' - »»-
Title or Purpose; ' • £6K-B £~Q K*~ J Cs/W*? $
| 1
Dare of Work:
Continued from:
• r s
EPA No.' Final
; S-75-001
Wt.
grams
Tare
grams
Weight
Change
mg
Remarks
i) Fiber Glass
filter
— Filter No.
10 2) Acetone rinse of
- nozzle, probe, &
front half of
"filter holder
Evap* dish No.
Total vol.
ml.
is
3) Water & water
rinse from .
- imping, conn. &
back half of C
T" filter ' ' "
•-Evap. dish
Total vol. $~/o ml
4} Chloroform &
— ether extract.
of (3) above.
"•" (extracted first)^
^- Evap. dish No.^71
Total vol. ml
25
Final acetone
rinse of imping,
.Jars and connec.KJ$
Evap. dish No'.^
-Total vol.f ml
47.01 gr
30.
10
15
20
25
Entered by:
Date:
Continued to:
Performances of this work observed by:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
G-69
10
15
i 20 I
i I 25
I i
Work Performed by;
Project No,
Date of Work:
Title or
} Fiber GJ
filtei
Filter *
} Acetone
nozzle,
front ha
filter h
Evap. di
Total vc
J Water &
rinse f
imping.
back hal
filter h
Evap. di
Total vo
^"CHTbrofo
ether ex
of (3) a
(extracte
Evap. dis
Total vo
>) Final ac
rinse of
jars and
Evap. di
Total vo
30
o
Entered by:
Performances
Purpose:
£'&<- C, £&f\*b C/V3/7C- Continued from;
S-
Lass
i
to.
rinse of
probe, &
llf Of J
[Older £0"
sh No.
!»„_& SL ml
water
rota
conn. &
f of
older ,.gK"
sh Mo.^
1. f f 2u g
no & ~
xrac v*
OwV9.
d first)}
h No. ^
1* ml
etone
imping.
_ %* IslO
sh No.
1.3%o ml
-
•
•
j
,-
^
v»
^
i
3
J~
'r.
*•!
^
1
EPA No.'
75-001
.•
^Hl
I
j
^
•* yr® ',
\ •
i
i
i
i
4f,*/
90;n ^| a,O.
I /
W '•
(\
^f7. 6ff>— J W
i
I
j
At 90
i
I
i
i ' :
i 5
1 1.0 i
of this work observed by:
15 |
Date:
I*1? i
- i
20 _ /-Z? ;
f
i j 20 j | [ 25 I I i
Continued to:
Disclosed to and understood by me:
Date:
Date:
Date:
Date:
-------
62
C-70
10
15
2O I
30
f 5 ? f
f..... _.
^
loll
v
1'IS 9?
gg.
'Vur
47-
10
15
20
25
3O
Performances of this worl observed by:
Date:
Date:
Date: 7. ^-9^
Continued to:
Disclosed to and understood by me:
Date:
Date:
-------
C-71
1O
15
20
25
Work Performed by?
Title or Purpose:
Project No. 1.
Date of Work;
( t
Continued from,-
•%
CJUT.
1O.
6.
15_
20
25
o.tiSI
30
0 !
i « !
',° I
I
I
I
I 1S
I
20
-
| i 25. i
Entered by: \/v~\!
Date:
Continued to:
Performances of this work ooserved by
Date:
Disclosed to and understood by me:
Date:
Date:
Date:
-------
Westmoreland CoalCo«
C-72 Quinwood, West Virginia
June 30, 1975
MASS COLLECTED CN THE OUTLET SIDE OF THE VEOTURI SCRUBBER
Run
Mumbei
QNC-1
QNC-2
QNC-3
QNQ-4
QNC-5
Date
Vv,
*fy
H
fc*,
%%-
Acetone
wash of
Probe ^
&
r- .«•"
ITS
J«. f
i«»V
103-4
IW
2^-^
iff*
1 17- 8
. - .
Corrected &-)
for acetone
blank ^5.
-^xa^s:- <^^^
I63-*
-vJ^ 2tf " «-35-*3
I 8t •'* '
t>Jlx z-^J *- tf.?^*^
(03.0
4jva^| • 4*11*+y
2iS'5
f'l^-- o.l*
117. 4
Filter
Catch
mg
so, f
52'6 mi
J7.1 ^'"
fc5-7 , fj
7C,<}
M'l ,^-f
5^f./ .
$7,0 ?(,.f
37-S7
Total
Mass, "vuj"
front half
•ir.5
2fM'
*"/• '
«fe
32^. / ' X
a$?p-'/
2 3 ? ' ^
/•r*
J76.1?
is?-"1
2/4.50
V
f ?? ? 1
-------
C-73
10
15 i i
65
20 i I | • 25 I I I
Work Performed by:
Work:
Title or Purpose:
VJ ftjk . Continued from;
•
C wore __ fftnat
P«»iC
F<«AL
_.* 57J-.**f-j — *~ " -• —
c rD ' *f\*Mf+,
P8?> i
i
V 1
IS -.
44.5175-
25
* o.
30
10
15
2O !
25
Entgreii by:
Date:
Performances of this work observed By:
Continuefl to:
Disclosed to and by me:
Date:
Bati:
Date:
Date:
-------
66
1O
C-74
IS
20
25
Work Performed by:
[ Title or Purpose;
Prefect No
Date of Work: vj
(Lut/gj£-ft-_
Continued from:
CTfr)
fe^ $ C
1O_
7-J
$7.
17.
57.
15.
. 1577
gf.
33.
25
30L
<$.'
1O
i 15
20
25
EntereiJ 6)f:
Date:
Continued to:
Performances of this work observed by:
Date:
Disclosed to and understood by me:
Data:
FhtP-
-------
C-75
Visible Emission
-------
PAGE / OF 3
C-76
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY
LOCATION .
OBSERVER
TEST NUMBER • /
DATE
TYPE FACILITY do/
OBSERVER CERTIFICATION DATE ,xl -A. , ...1.7
• OBSERVER AFFILIATION
POINT OF EMISSIONS •
.
y ^^ /., .^.
'
COOTROL DEVICE
HEIGHT OF DISCHARGE POINT
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period of time, additional
recordings should ba sade as applicable.
CLOCK TIME INITIAL
' " J.
OBSERVER LOCATION
Distance- to Discharge <*7^-0~Q
Direction from Discharge S^®*
Height of Observation Point t-5*~<9
BACKGROUND DESCRIPTION S^ ^
_: ' a.m.
r j~
"X. - _t*S t & J-
tfetJ- ( *A*-c
( %& ^ <~. /*
FINAL : a.m.
_^&_ '*•$>"/ p.m.
' -J '}
^esrf? \ ••" js —*>•• f a x
^vvN
WEATHER CONDITIONS
• Wind Direction
Wind Speed &
Ambient Temperature •
SKY CONDITIONS (clear,
overcast, "L clouds, etc,)_
PLUME DESCRIPTION
Color __
Distance Visible _
MINUTES OF MONCOMPLIANCE
ffi —
-------
C-77
OBSERVATION RECORD
PAGE 2- OF
COMPANY '//•> / .'w. / -'J.. '
LOCATION X? „.>>.—' :>/._•/*
OBSERVER
TYPE FACILITY C. -
TEST NUMBEE_
DATE .71. ,<
/
POINT OF EMISSIONS
Hr
0
5
_*>
j>
^
i)
j-
A
^
:3
3
Mln
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
-. _
1 STEAM PLUME
Seconds (check if aoolicable)
0
<>"
»<•
/f
;f
?a
/r
/o
r<
/,f
/r
^r
x^"
//
<5"
xf
/<
15
/C
/,r
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/f
<
>•<
^j
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^
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••*
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/$
'<
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sf>
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x/
/r
xf
X<5
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tf
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30
?v^
' /'
. S
• ( s
/.r
/o
/r
//
20
/r
//
/•?
/^
/^
Xf
/o
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/r
/r
x
45
/r
'^
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/r
/ ^r
r ?
? .•?
'£
: S
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.' 1
/-°
/r
/<
x/
>r
Xf
/r
-'<3
VO
Af
2-0
/r
2*9
/,f
x/
/r
//
//>
Attached
&r/!fV *f*t f
Detached
COMMENTS
X5 '. a 7 /v1-^
/ - //5
,< '. .//
/< ' /-L.
f ' 'J
/• x^X
4- /r
/ . '£
\ ' ' 7
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^ "-0
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^ 7< iU,,/ ^ ^.,«-
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X ?f
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< T-u
i ' 33
f :.?c/
^ • jr
-------
C-78
PAGE 3 OF
COMPANY
TEST NUMBER
DATE . T-, •
/
OBSERVATION RECORD
(Cont.)
' OBSERVER
LOCATION <)• >.-...-.
TYPE FACILITY
POINT. OF EMISSIONS
,'-/.-,*..
Hr
Min
Seconds
STEAM PLUME
(check if applicable)
15
30
45
Attached
DeCached
COMMENTS
30
Af
/r
31
32
/O
33
34
/a
35
36
'O
3?
so
/O
38
39
40
41
( '
42
S'
43
X
44
S" S
< .- .r J
45
46
to
47
/o
/O
48
S
A -S7
49
6 •
50
s
51
_52_
21-
54
_55_
56_
57
-------
PAGE / 0!.' 8
C-79
RECORD OF VISUAL DETERMINATION OF OPACITY
TYPE FACILITY
CONTROL DEVICE
COMPANY /?^« ^ .x.' -'*>•./ /C .* / 4*.
LOCATION :%.,.;t,.^
TEST NUMBER J?
DATE
HOURS OF OBSERVATION
OBSERVER
OBSERVER CERTIFICATION DATEy»:/«y 27.-
OBSERVER AFFILIATION
POINT OF EMISSIONS
/
HEIGHT OF DISCHARGE POINT
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period o£ time, additional
recordings should be made as applicable.
CLOCK TIME
INITIAL
a .m.
p .m.
FINAL
a .m.
OBSERVER LOCATION
Distance to Discharge
Direction from Discharge
J"~-
Height of Observation Foint^
BACKGROUND DESCRIPTION
WEATHER CONDITIONS
j«*»
Wind Direction
Wind Speed
Ambient Temperature
SKY CONDITIONS (clear,
overcast, % clouds, etc.)_
PLUME DESCRIPTION
Color _
Distance Visible __
MINUTES OF NONCOMPLIANCE
,
xfd)
/
&...*
^J r
j&^>
* /'"
-------
C-80
OBSERVATION RECORD
PAGE 2. OF ?
LOCATION
TEST NUMBER
DATE .
/9
OBSERVER
TYPE FACILITY
/""X-...
POINT OF EMISSIONS
Hr
&
2_
o_
£L
Min
Seconds
j STEAM PLUME
(check if applicable)
15
30
45
Attached
Detached
COMMENTS
JO
/r
20
.?
J.-/3
10
s ••
o
ft
/o
/P
10
11
3
12
10
?. 1, V
13
14
15
/O
/r
16
17
18
/.' i
19
//*
to
20
S'30
21
22
70
20
"io
23
10
.5
24
25
26
27
23
Jo
J
28
3-
29
J
-------
C-81
PAGE 3"
COMPANY.
LOCATION
-------
C-82
PAGE *S OF
TEST NUMBER
DATE ^Tui.
OBSERVATION RECORD
COMPANY >//. , J^ , , , /„ ... / C « /
LOCATION ^,'h.
OBSERVER
TYPE FACILITY
J
POINT OF EMISSIONS
/ Pr y g-X
f
"- ...
-
Hr
/
/
^
/
/
/
,/
/
,
7»
•
/
,
/
/
/
/
/
/
/
/
/
/
/
/
/
/
/
,
/
1
Min
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
Seconds '
0
/r
£. Q
*>•£
,s
1*
f"?
/o
r 1
lo
,r
/<•
} /}
' \
/.r
/<-
5 A
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,(
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13
,g
75
?:?
7-5"
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?r
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15
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C-83
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PAGE / OF
e-87
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY ^X - ^,,• - .- - '../ - — ' HOURS OF OBSERVATION ^ > . ,
LOCATION C:.-.-.,«-r-/ :.-_•/ :• •» OBSERVER _/_^f.~ •• -> .r?.•-•./.
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PATE *S"-f ~ * /=f7r OBSERVER AFFILIATION /T.
TYPE FACILITY C -, ' C /, ~ .. .. , POINT OF EMISSIONS
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Record the following information prior Co and upon completion of observations at
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-------
COMPANY
TEST NUMBER
DATE v 7f,
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LOCATION (^ .*
C-89
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/ OBSERVER
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C-90
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G-93
PAGE ? OF /
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C-94
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COMPANY
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C-95
PAGE y OF /
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DATE J73
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OBSERVATION REC01U3
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C-99
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COMPANY
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DATE .
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PAGE / OF ^
C-100
RECORD OF VISUAL DETERMINATION OF OPACITY
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COMPANY lA^jJ-sx 3 re '*^J da *, / HOURS OF OBSERVATION
LOCATION //^/Ai^^ 4< /x£ OBSERVER
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Record the following information prior to and upon completion of observations at
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-------
COMPANY
e-ioi
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C-102
OBSERVATION RECORD
I» / OBSERVER
PAGE 3 OF
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PAGE jS'OF 9
C-104
OBSERVATION RECORD
LOCATION
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DATE
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DATE
C-105
OBSERVATION RECORD
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PAGE 7 OF ^
OBSERVATION RECORD
COMPANY
V^r-x* A. V
LOCATION
TEST NUMBER
DATE .T
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DATE . ^,. .
PAGE
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C-108
OBSERVATION RECORD
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C-109
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY1/,/t - -'-,:-.,,- '•„ J C»* /
LOCATION Q!t. u ,^ rW isS,
TEST NUMBER _^T
DATE v ~7>>i,, 1 .<%" /'
TYPE FACILITY ^^ • ...C./<*•*+'•.**
CONTROL DEVICE l/^^J-.,,, C^t.^
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OBSERVER CERTIFICATION DATS
OBSERVER AFFILIATION ^ <^
POINT OF EMISSIONS
1 7 /
HEIGHT OF DISCHARGE POINT
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period of time, additional
recordings should be made as applicable.
CLOCK TIME
INITIAL /O -.o^ a.m. FINAL : a.m.
. • p.m. m^Z_:^J p.m.
OBSERVER LOCATION
Distance to Discharge
Direction from Discharge
Height of Observation Point
BACKGROUND DESCRIPTION
WEATHER CONDITIONS
Wind Direction
Wind Speed
Ambient Temperature
SKY CONDITIONS (clear,
overcast, % clouds, etc.)
PLUME DESCRIPTION
Color
Distance Visible
MINUTES OF NONCOMPLIANCE
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PACK £, OF
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COMPANY
PAGE V OF
C-112
OBSERVATION RECORD
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, . PAGE /"OF
C-113
OBSERVATION RECORD
COMPANY
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PAGE 4 OF
C-114
OBSERVATION RECORD
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C-115
OBSERVATION RECORD
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DATE
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C-116
OBSERVATION RECORD
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PAGE 9 OF /
C-117
OBSERVATION RECORD
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C-118
OBSERVATION RECORD
.COMPANY
OBSERVER
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PAGE // OF /1^
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PAGE, /1^-OF /_jj<^
C-120
OBSERVATION RECORD
COMPANY
LOCATION
TEST NUMBER
DATE t
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PAGE / OF 3 '
C-121
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY U>.ft, of/I.. rl To,, / Cr.
LOCATION '£,.,,„ uyo/J UA l/«
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DATE .-, '•*>-7$
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OBSERVER AFFILIATION p^Tfl/L ^ /^ X« L !-
POINT OF EMISSIONS -fi .... / r?^M, yr
HEIGHT OF DISCHARGE POINT 76 Z^~
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each source. If observations are made over an extended period of time, additional
recordings should be made as applicable.
CLOCK TIME
INITIAL
a.m.
FINAL
a.m.
:- G "*
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DATE
OBSERVATION RECORD
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COMPANY
LOCATION
TEST NUMDER
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C-123
OBSERVATION RECORD
(Cone.)
PAGE_3 OF •?
A
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TYPE FACILITY
POINT OF EMISSIONS
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32
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PAGE /OF
C-124
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY {/J »;
.x >,-/.?
OBSERVER CERTIFICATION PAlE A*r'. / 75
OBSERVER AFFILIATION RtiJS'f/+ ' 1, L>*. ./-. *
POINT OF EMISSIONS T/. .«,„../ P/^r
HEIGHT OF DISCHARGE POINT
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period of time, additional
recordings should be made as applicable.
CLOCK TIME
INITIAL
3 '•
a.m.
p.m.
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Color
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MINUTES 0? NONCOMPLIANCE
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£-/~~
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-------
COMPANY
LOCATION
TEST NUMBER
DATE
(, //
PAGE J-OF
C-125
OBSERVATION RECORD
(*«, Co
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to. 'A
TYPE FACILITY (^-.A /
POINT OF EMISSIONS
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C-126
PAGE 3
OBSERVATION RECORD
(Cont.)
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C-127
OBSERVATION RECORD
PAGE q OF
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C-128
OBSERVATION RECORD
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DATE
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C-129
OBSERVATION RECORD
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C-130
PAGE /> OF O
TEST NUMBER
DATE
OBSERVATION RECORD
(Cont.)
COMPANY \\.- rf...«i* ) A... r) /P/-. /
LOCATION ^ . ^ UA3Q ^ K/ I >, .
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COMPANY
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TEST NUMBER "T-
DATE (ff ,
-
C-131
OBSERVATION RECORD
(Cont.)
J fa OBSERVER
LU. tJe
TYPE FACILITY
PAGE ST OF
POINT OF EMISSIONS
Q
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Min
30
31
32
33
34
35
36
37
38
39
40
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44
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46
47
43
49
50
51
52
53
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PAGE / OF
C-132
RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY VtA^fccxv/»>*. <* /!><,/ ^ "HOURS OF OBSERVATION .
LOCATION ^ui'X^eoJ tU U<. OBSERVER A- S^./ric.
TEST NUMBER g _ OBSERVER CERTIFICATION DATE /.W'. / 4
DATE 6 'A o/?.g _ OBSERVER AFFILIATION .5^7^ /^> •*•./»«.. /?^
TYPE FACILITY c'W / <^ LjU/.v* ^/*~^ POINT OF EMISSIONS
CONTROL DEVICE j j^. j g ^. >5 *- ^ I ~v HEIGHT OF DISCHARGE POINT
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period of time, additional
recordings should be made as applicable.
CLOCK TBCE INITIAL 9 ;3^ a.m. FINAL _ : _ a.m.
p.m. i y .; f ^ p.m.
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SKY CONDITIONS (clear,
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MINUTES OF NONCOMPLIANCE
-------
COMPANY
LOCATION c? H .
TEST NUMBER
DATE ,
C-133
OBSERVATION RECORD
(Cont.)
OBSERVER
TYPE FACILITY
PAGE
OF / 2-
POINT OF EMISSIONS
fS.*,**Jt
Hr
Min
STEAM PLUME
Seconds (check if aoolicable)
0 15 30 45 Attached Detached
COMMENTS
30
31
32
33
34
35
36
37
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C-134
OBSERVATION RECORD
PAGE 3 OP / 2_
COMPANY
LOCATION
TEST NUMBER_
DATE (~f
/a..* -a
OBSERVER
CQ.
TYPE FACILITY
POINT OF EMISSIONS
Hr
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0
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28
-------
COMPANY
LOCAT ION
TEST NUMBER
DATE
C-135
OBSERVATION RECORD
(Cont.)
OBSERVER
PAGE
UJ
O-,**-»»
TYPE FACILITY
POINT OF EMISSIONS
Q,
Hr
Min
. STEAM PLUME
Seconds (check if aoollcable)
0 15 30 45 Attached Detached
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-------
COMPANY
LOCATION Qtl .
TEST NUMBER
PATE
PAGE
OF
0136
OBSERVATION RECORD
OBSERVER
/Cea~y- Z^-s^*, m^^v
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POINT OF EMISSIONS
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COMPANY
LOCATION
TEST NUMBSR_
DATE /
C-137
OBSERVATION' RECORD
(Cont.)
OBSERVER
PAGE
OF /2-^
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TYPE FACILITY
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0138
OBSERVATION RECORD
PAGE
OF
COMPANY
LOCATION On.*,
TEST NUMBER
DATE
3
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. OBSERVER
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-------
0139
OBSERVATION RECORD
(Coat.)
PAGE J OF
COMPANY LC-.. .'*.,, /i_ I Oc*.f f ^ OBSERVER CZ-^-l: ,,..id..
LOCATION- £^:.v ....... ..' 'w '.',. * TYPE FACILITY Ccesf ' fj**-* ~« 'P/4~s$"
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OF
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each source. If observations are made over an extended period of time, additional
recordings should be asade as applicable.
CLOCK TIME
INITIAL : a.m.
^ ; g»O p.m.
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COMPANY U.
C-141
OBSERVATION RECORD
•» / OBSERVER
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LOCATION QfJ,\ - -W -'i..;,.
TEST NUMBER ^ ''{**,
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COMPANY
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TEST
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TEST NUMBER
/./..T
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C-142
OBSERVATION RECORD
(Cont.)
--. "'„ OBSERVER
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POINT OF EMISSIONS
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-------
PAGE / j OF /^
OBSERVATION RLCORJD
COMPANY
LOCATION
TEST NUMBER
DATE
A
1 f^y. /
OBSERVER
TYPE FACILITY
POINT OF EMISSIONS
Hr
Min
STEAM PLUME
Seconds, (check if .applicable)
0
15|30
45
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COMMENTS
/r,
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0
10
11
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18
19
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21
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27
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-------
PAGE
C-144
TEST NUMBER
DATE
RECORD OF VISUAL DETERMINATION OF OPACITY
HOURS OF OBSERVATION
COMPANY / ' •• *'l M <:./* /Vuv J Coo-/ d
LOCATION
vJL,
TYPE FACILITY
CONTROL DEVICE
>j/u
OBSERVER
OBSERVER CERTIFICATION DATE_
OBSERVER AFFILIATION Q_»~fk, fl« A/;***./>•?
POINT 0? EMISSIONS
HEIGHT OF DISCHARGE POINT
Record the folicv;ii\g information prior to and upon completion cf observations at
each source. If observations ars made over an extended period of time, additional
recordings should be. aadc as applicable.
CUOCK TIME
INITIAL
a .m.
p >m.
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; 3 .&. p»m.
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-------
PAGE .2- OF
0145
OBSERVATION RECORD
(Cont.)
COMPANY \iJtr
LOCATION {^.;.,vJ««J UJ. \/« TYPE FACILITY /I./ ^^ .,;^ pi, . ~/
TEST NUMBER V POINT OF C-IISSIONS *Tt&s^* \ Dr.!* r
DATE
Hr
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6>t
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30
31
32
33
34
35
36
37
38
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40
41
42
43
44
45
46
47
43
49
50
51
52
53
54
55 "•
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COMPANY
LOCATION
TEST NUMBER
DATE 6
0146
OBSERVATION RECORD
OBSERVER
PAGE
OF
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(JU.
TYPE FACILITY
£ j
POINT OF EMISSIONS -ft
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-------
COMPANY
LOCATION
TEST NUMBER
DATE
0147
OBSERVATION RECORD
(Cont.)
/£, / £j
OBSERVER
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la
TYPE FACILITY
PAGE
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-------
PACK 4 OF
C-1A8
OBSERVATION MCCKO
COMPAQ
MCATT.ON
TEST NUMBER
DATE
OBSERVER
TYPE FACILITY
POINT OF EMISSIONS
Hr
£' o
Min
j STEAM FLUME
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-------
C-149
PAGE L OF $?
OBSERVATION RECORD
(Cont.)
COMPANY
,
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1 /
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-------
C-151
OBSERVATION RECORD
(Cone.)
PAGE V O
~Y
^-\
COMPANY kJ^T^O/f/0^/ fr
BATE £
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41
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43
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-------
0152
OBSERVATION Ri-CCUD
Ul' <*f
-^_
COMPANY
LOCATION
u ^
<", J UJ> U «
TEST MJK3i:R_
DATE &/i
tl
OBSERVER
TYPE FACILITY f*~*. '
POINT OF EMISSIONS
Hr
1
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—
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0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
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-------
PAGEj OF )3
C-153
. RECORD OF VISUAL DETERMINATION OF OPACITY
COMPANY ^^fl^Jo^J fl>a./ da HOURS OF OBSERVATION
LOCATION . , . ., ^ M J uj, \Ji OBSERVER
TEST NUMBER < _ OBSERVER CERTIFICATION DATE /) -*-'„ /
SATE 6>A.4/T< _ OBSERVER AFFILIATION fl^-fkr//* <*Ju *./>**
TYPE FACILITY fW/ (*Lt^.^. » POINT OF EMISSIONS
CONTROL DEVICE U^^-fu.fl uJL^ HEIGHT OF DISCHARGE FODTr >£
Record the following information prior to and upon completion of observations at
each source. If observations are made over an extended period of time, additional
recordings should be made as applicable.
CLOCK TIME
INITIAL /g :&',
*
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BACKGROUND DESCRIPTION u_
WEATHER CONDITIONS
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overcast, % clouds, etc.) /o 7*> <*/o
FLUME DESCRIPTION
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MINUTES OF NONCOMPLIANCE
-------
COMPAKCfJ^,
LOCATION
TEST NUMBER
DATE d, fa *
C-154
OBSERVATION RMCCUD
OBSERVER
±~ OF , »>
TYPK FACILITY ...C0+..f
POINT OF- EMISSIONS
'T
Hr
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-------
C-155
PAGE_J OF /'/
COMPANY
TEST NUMBER
DATE £
/
OBSERVATION RECORD
(Cont.)
OBSERVER
5~A,W«
TYPE FACILITY faj
OF EMISSIONS
P.
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30
31
32
33
34
35
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-------
C-156
OBSERVATION RMCCRU
COMPAQ1
LOCATION
TEST NUMBER
DATE /
(jQ. LA
OBSERVER
TYPE FACILITY
d*
POINT OF EMISSIONS
Hr
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m
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15 |30i ••••j 'Attached I Datachr.d
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-------
COMPANY
LOCATION
TEST NUMBER
DATE
0157
OBSERVATION RECORD
(Cent.)
PAGE
OBSERVER
TYPE FACILITY da*/
POINT. OF EMISSIONS 7J
OF )3
P
& >
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\J
49
00 /c
50
74 r?
51
$0
1C
52
53
7^ .
54
55
-?
-------
C-158 /
OBSERVATION RliCCIlD
COKPAW
LOCATION
TEST MUMPER
DATE .
/ -
OBSERVER
TYPE FACILITY
6!*y
fL
POINT OF EMISSIONS fj^^J j) ryfjt
Hr
Min
STEAM PLUME
Seconds fcheck if .ipgl icahlg)
15
3 OK-3
10
Attached Decachod
CO^EOTS
25
50
-f-J
fP
r
1C?
10
. J
A
11
3D
12
20
•20
13
14
o
•To /=
15
16
' P'/
17
JO 2&
18
19
20
ff
l LO '
21
22
70
23
2k
2C9C
25
26
27
28
50
Sff /"•/"
29
-------
COMPANY
LOCATION
TEST NUMBER
DATE* fe/g.
C-159
OBSERVATION RECORD
(Cont.)
OBSERVER
PAGE 7 OF/3
CO. 14
A 0 ,J
CgW. O A-v/g^y^
TYPE FACILITY
POINT OF EMISSIONS -TJ ^
/}*•-/ #
Hr
I I STEAM PLUME
Seconds (check If applicable)
Min
0
30
45
Attached
Detached
COMMENTS
30
< -7 X
31
32
33
70
34
35
36
37
-J.C3
•?<£?
38
39
IV
40
10
41
42
25
A3
'*
45
50
46
.0-
47
43
49
50
.tie
51
53
54
55
56
3d"'
57
o
-------
COMPAQ
TEST NUHBER_
DATE & /-2<
«/«..,/ ft* I
C-160
OBSERVATION RliCOUD
OBSERVER
>. U
TYPE FA CI Lin'
POINT OF EMISSIONS
"S
*<***-
/
Lfeu
Hr
in
I ' STEAM PLUME
Seconds (chftc!:.__ ifj applicable)
l.S.30|^j_
^
Attached
COMt-ENTS
SLO
$<>
7
8
10
10
11
12
13
X
14
15
16
•71
17
18
a?
19
10
TO
feoff
20
10
TO
21
22
23
24
25
35
TOO
^<5 ,., •
26
too Ft
27
r
28
•.« - -^
29
$6
-------
COMPANY
LOCATION
TEST NUMBER
DATE fe/.
C-X61
OBSERVATION RECORD
(Cont.)
PAGE ^ OF /3
(L>« / do
OBSERVER
£*. j J *
UJ<
TYPE FACILITY^./
POINT OF EMISSIONS
Q-.
Hr
Mln
Seconds
STEAM PLUME
(check if applicable)
0 15 30
45 Attached
Detached
COMMENTS
30
31
3- 'J .:
32
33
30
CO
/C/
34
35
36
37
38
1C
39
40
*/»
41
42
43
44
45
pe
46
47
I $ O-t?
43
49
Ino
50
10
/ c - -
51
0?
16
52
53
¥
54
55
56
57
25
/Co
so
-------
C-162
COMPANY UJ fjn . a r - JL >
LOCATION
TEST MUMPER
DATE _ £ ./
6
OBSERVATION RECORD
(Cont.)
Co OBSERVER
TYPE FACILITY CQ&.
POINT OF EMISSIONS
J
y*.
[)^^
Hr
Min
Seconds
STEAM PLUME
Ccheck if apolicablc)
15 30
45 Attached
Detached
COMMENTS
_30_
31
10
r-r
rr
'i* f'^C> s»v >
..,«..[_
2
•*
-75
JD
75
34
35
FT
35
37
38~
39
40
11
-|3
r
43
yo
to
46
4/
/o
to
43
X
49
/o
50
51
<*)
52
K
/O
>r
53
'10
54
10
55
if
'0
56
57
\t
/O
in
-------
I'AU.
OBSERVATION RliCOllD
COMPANY
€06. I
LOCATION
LQ- \}9
TEST NUMBER £
DATE £/3
ZJT.
OBSERVER
TYPE FACILITY
/ f/,A .v>*, Pf, . f
POINT OF EMISSIONS
_
\ ..-. ,.. * ft D y v s
Hr
Min
STEAM PLUME
Seconds fc.heck if applicable;)
0
W-i
Attached
Detached
COMMENTS
H-
/o
A
fl
/o
/£?
It
>•/«
11
Lf/51'i
_7
8
/f
ft
fO
/>• t.
Ao
11
10*
12
f?
13
/
14
As
K
ict
/^f
16
17
18
19
t
21
22
23
24
25
26
27
28
"IF"
i<,\\4
-------
COMPANY
LOCATION
TEST NUMBER ^
DATE 6/?
C-164
OBSERVATION RECORD
(Cont.)
OBSERVER
UJ>
TYPE FACILITY
S
' -a y.
. / '(?
POINT OF EMISSIONS
... p/w
Hr
Min
STEAM PLUME
Seconds (check if applicable)
0
15
30
45
Attached
Detached
COMMENTS
i
-74
-
31
32
I*W£
33
34
35
36
£./£
37
/5
38
39
/
|40
41
42
43
75^
44
<2>
45
<*
46
47
,5 to
o A
43
£
IV
49
/f
/f
<
51
52
/5/5
53
54
fQ
55
56
Q
•tf
57
7/7
tf
3c 3
•77
-------
COMPANY
LOCATION
TEST NUMBER
DATE
C-165
OBSERVATION RECORD
OBSERVER
AO
6U.
TYPE FACILITY
PAGE \\ OF /
POINT OF EMISSIONS
Hr
Min
STEAM PLUME
Seconds (check if applicable)
30
1C
15
30
45
pp
Attached
Detached
COtt-lENTS
2-0
10
>=
3:
la
M
30
?0
1C
10
11
-zo
30
12
13
1C
14
15
16
17
18
19
20
HZ
22
23
24
25
26
27
28
29
*iC
20
-------
C-166
Multiple-Cyclone Particle
Size Field Data
-------
IMPACTOR IDENT.
OPERATOR/J
PORT NO.
AMB.
C-167
FIGURE 4
FIELD DATA
DATE (*/(&/"
PROBE DEPTH
STACK TEMP.
(^IN STACK/C^JT-OF-
STACK
PITOT DELTA P
NOZZLE DIA. "^
GAS METER END
GAS METER START
METERING ORIFICE TEMP.
PJSMARKS: %
GAS VELOCITY
IMPACTOR DELTA P.
RUN CODE NO. /
SAMPLING LOCATION
STACK PRES.
IMPACTOR
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
?-7 try* *
TOTAL SAMPLING TIME
& si, /»..->
METERING ORIFICE AP
PRESS. AT METERING ORIFICE
-------
C-168
FIGURE 4
FIELD DATA
IMPACTOR IDENT.
OPERATOR
PORT NO.
AMB. PRES.
DATE b
j
PROBE DEPTH
STACK TEMP.
---- ^x .
IN STA^K/0OT-OF- STACK
PITOT DELTA P
NOZZLE DIA.
GAS METER END
GAS METER START
METERING ORIFICE TEMP.
GAS VELOCITY
IMPACTOR DELTA P.
RUN CODE NO.
SAMPLING LOCATION
STACK(PRES.
IMPACTOR TEMP.
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE AP
PRESS. AT METERING ORIFICE
REMARKS:
' ,r-H
-r s
*za.
(o^>
Ot-e*-~^ —
/4ce»^
^
vJ""V'-^L^-<-4*.>- »
-------
C-169
FIGURE 4
F I E L D D A T A
IMPACTOR IDENT.
OPERATOR
PORT NO.
AMB. PRES. <^z~7. 07
^IN STACKyOUT-p0F-STACK*
PITOT DELTA P
NOZZLE
GAS METER END
GAS METER START
METERING ORIFICE TEMP.
REMARKS:
DATE
PROBE DEPTH
STACK TEMP.
GAS VELOCITY
IMPACTOR DELTA P.
RUN CODE NO. **
SAMPLING LOCATION
STACK PRES
IMPACTOR TEMP.
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE AP
*RESS. AT METE'RING ORIFICE
\ \Y^.
-------
U-l/U
FIGURE 4
FICLD DATA
/
DATE
PROBE DEPTH
£-^V?V-c_-c-d^
STACK TEMP.
IMPACTOR IDENT
OPERATOR
PORT NO.
AMB. PRES.
IN STACK/OUT-^OF-STACK
PITOT DELTA P ' GAS VELOCITY
NOZZLE DIA ~"
GAS METER END
GAS METER START 5 "7 7-
IMPACTOR DELTA P.
METERING ORIFICE TEMP
REMARKS :
RUN CODE NO.
SAMPLING.LOCATION
STACK
IMPACTOR TEMP.
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
y//j
TOTAL SAMPLING TIME //
METERING ORIFICE AP x
- PRESS. AT METERING ORIFICE
-------
DATE »'
OPERATOR
PORT NO.
AMB. PRES. *Z~7. 6*7
IN STACK/OUT^0F-STACK
PITOT DELTA P * GAS VELOCITY
NOZZLE DIA. ^/^ -"7/1^ IMPACTOR DELTA P.
GAS METER END 3.
GAS METER START
METERING ORIFICE TEMP.
REMARKS: %
/
RUN CODE NO.
SAMPLING _LOCATION
STACK PRES.
IMPACTOR TEM
SCALPING CYCLONE(S) •^
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME //*»•/.
METERING ORIFICE AP
PRESS. AT METERING ORIFICE
-------
FIGURE 4
FIELD DATA
DATE
PROBE
STACK TEMP
IMPACTOR IDENT.
OPERATOR
PORT
AMB. PRES.2Z-7&8
IN STACK/OUT-^DF-STACK
PITOT DELTA P ' GAS VELOCITY
NOZZLE DIA^/o 3^" IMPACTOR DELTA P.
GAS METER END 3/3.«$?cDG
GAS METER START *?0^~- "2-O
METERING ORIFICE TEMP.
REMARKS: ^
RUN CODE NO. ~~7C
SAMPLING LOCATION
STACK PRES.
IMPACTOR TEMP^
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE AP
PRESS, AT METERING ORIFICE
6
/o
I 2.0
-------
C-173
FIGURE 4
F I E LD DATA
DATE
PROBE
STACK TEMP.
IMPACTOR IDENT.
OPERATOR
PORT NO.
AMB. PRES. 2 V-
IN STACK/OUT-^3F-STACK
PITOT DELTA P ' GAS VELOCITY
NOZZLE DIA. •**/£ %,¥i-"&MP ACTOR DELTA P.
GAS METER END 3 0 CA r/
-------
IMPACTOR IDENT.
OPERATOR
PORT N
AMBRES
PITOT DELTA P
NOZZLE DIA.
GAS METER END 3^3.35.5-.
GAS METER START 333. <
METERING ORIFICE TEMP.
C-174
FIGURE 4
FIELD DATA
J- " RUN CODE NO. /£>
SAMPLING LOCATION
STACK PRES.
IMPACTOR TEMP.
*\ SCALPING CYCLONE(S)
GAS VELOCITY , IMP. FLOW RATE
IMPACTOR DELTA P. ^- START "TII4E
PROBE DEPTH
STACK TEMP.
s
f <0s&/
TOTAL SAMPLING TIME
3 t^s^j
METERING ORIFICE AP
PRESS. AT METERING ORIFICE
REMARKS
<£~^"X
rf*y3 z?x«-a-^
i
s. Gig,
^^
>=
-------
C-175
FIGURE 4
FICLD DATA
IMPACTOR IDENT.
OPERATOR
PORT NO.
DATE G/
PROBE DEPTH
AMB. PRES.^7. o,\ STACK TEMP.
' '• . /^Z
IN STACK/OUT^OF-STACK
PITOT DELTA P * GAS VELOCITY
NOZZLE DIA.j**(0 3Jtu ' IMPACTOR DELTA P.
GAS METER END 3 £2
GAS METER START 3/i/.,
METERING ORIFICE TEMP.
REMARKS:
A A '~^~
oe-i»-* fr^JL^s-t^J
RUN CODE NO.
SAMPLING LOCATION
^.*j
STACK
IMPACTOR TEMP.
SCALPING CYCLONE (S) *"~
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE AP,
PRESS. AT METERING ORIFICE
MVH
"2.
1.
6
S
' \*
)i
.S
a
3
. -^
7
/o
i S
^^^
4T '
*-
*
<:
-^ •
^c^
-------
FIGURE 4
FIELD DATA
IMPACTOR IDENT .
OPERATOR
PORT NO.
AMB. PRES.
DATE
PROBE
STACK TEMP.
STACK/OTp'^OF-STACK
PITOT DELTA P ' GAS VELOCITY
IMPACTOR DELTA P.
KOZZLE
GAS METER END
GAS METER START
METERING ORIFICE TEMP.
S^.
REMARKS:
RUN CODE NO.
SAMPLING LOCATION
STACK PRES.
IMPACTOR TEMP.
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE
-PRESS. AT METE'RING ORIFICE
)
*
r
5? .£>
-------
C-177
FIGURE 4
FIELD DATA
IMPACTOR IDENT.s£)o*r (
OPERATOR
PORT N
AMB. P
I /
DATE
PROBE DEPTH
STACK TEMP.
IN STACK/0UT-OF-STACK
PITOT DELTA P ' GAS VELOCITY
NOZZLE DIA^'O V'fe IMPACTOR DELTA P.
^~-
GAS METER END,
GAS METER START
METERING ORIFICE TEMP.
RUN CODE NO. J 0 C
SAMPLING LOCATION
STACK
IMPACTOR TEMP.
s-
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
n
METERING ORIFICE AP
3*. & "
PRESS. AT METERING ORIFICE
REMARKS:
£*y>
-r
6
1
\o
Y
1
IT. o
-------
FIGURE 4
FIELD DATA
DATE
PROBE DEPTH
STACK TEMP.
C*
START TIME
IMPACTOR
OPERATOR
PORT NO.
RUN CODE
s- SAMPLING LOCATION
f STACK PRES.
IMPACTOR TEMP.
IN STACK^OUT-^DF-STACK SCALPING CYCLONE(S)
-plfOT DELTA P '2>,± * GAS VELOCITY IMP. FLOW
NOZZLE DIA. j ^ ^rs IMPACTOR DELTA P.
GAS METER END 3 3>3»- G-STi ' < TOTAL SAMPLING TIME
GAS METER START 3 3>3. ^SO f METERING ORIFICE, ^P
METERING ORIFICE TEMP. .. PRESS. AT METE*RING ORIFICE
REMARKS:
I I *»•>,
- Q _
0
^r^—
C f
Q=
-------
DATE
PROBE DEPTH
•"'V ' 'j^g^ ^*F~U *****'€***}
STACK TEMP.
C-179
FIGURE 4
FIELD DATA
IMP ACTOR IDENT. jA**/
OPERATOR
PORT
AMB.
^-~
IN STACK/0UT-OF-STACK
,*—•—«^^ r^****'^
PITOT DELTA P " GAS VELOCITY
NOZZLE DIA.jt,d 3//to" IMPACTOR DELTA
GAS METER END 3-SV. / :
GAS METER START 3V'3-
METERING ORIFICE TEMP.
REMARKS:
RUN CODE NO. ((
SAMPLING LOCATION
STACK PRES.
IMPACTOR TEMP.
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE AP
PRESS. AT METERING ORIFICE
>9
)SV~*^~yr
-------
FIGURE 4
FIELD DATA
IMPACTOR IDENT.
OPERATOR/^
-------
C-181
FIGURE 4
FIELD DATA
DATE
PROBE
STACK TEMP.
IMPACTOR
OPERATORS?
PORT
AMB.
'fN STAC#/OUT-OF-STACK
PITOT DELTA P ' GAS VELOCITY
NOZZLE DIA. 3J •' «fc/0 IMPACTOR DELTA P.
GAS METER
GAS METER
METERING ORIFICE TEMP.
REMARKS:
RUN CODE NO.
SAMPLING LOCATION
STACK
IMPACTOR
SCALPING CYCLONE(S)
IMP. FLOW RATE
START TIME
TOTAL SAMPLING TIME
METERING ORIFICE
PRESS. AT METERING ORIFICE
lo
s~. a
-------
APPENDIX D
SAMPLE COLLECTION LOG
-------
APPENDIX D
SAMPLE COLLECTION LOG
6/18/75 - Sieve Sample Collection Times for Westmoreland Coal Company,
Quinwood No. 2 Preparation Plant
Samples collected by Mr. Jack Tabor
(Three sweeps used for this test per each time)
Start - 1810 to 1815
1825 to 1830
1855 to 1900
1910 to 1915
1925
1940
1955
2010
2040
2110
2140
2200
to 1930
to 1945
to 2000
to 2015
to 2045
to 2115
to 2145
to 2203
1st bag
2nd bag
Stop,
Involves No. 7 and
No. 3 collection.
6/19/75 - Sieve Sample Collection Times for Westmoreland Coal Company,
Quinwood No. 2 Preparation Plant
Samples collected by Mr. Jack Tabor
(Three sweeps used per each time for this test)
Start - 1500
1515
1530
1545
Hold
1615
1630
1645
1700
1730 Stop.
Involves only No. 7 coal.
-------
D-2
6/20/75 -
Sieve Sample Collection Times for Westmoreland Coal Company,
Quinwood No. 2 Preparation Plant
Samples collected by Mr. Jack Tabor
(Three sweeps used per each time for the test)
Start - 0940
0955
Hold
1100
1115
1130
Hold
1215
1230
1245
Hold
1500
1515
Involves only Mo. 7 coal
Stop,
6/23/75 - Sieve Sample Collection Times for Westmoreland Coal Company.
Quinwood No. 2 Preparation Plant
Samples collected by Mr. Jack Tabor
(Three sweeps used per each time during the test)
Start - 1600 involves only No. 7 coal
1630
1645
1700
Hold
1805
1820
1835
1850
1905
1920 Stop.
-------
D-3
6/25/75 - Sieve Sample Collection Times for Westmoreland Coal Company,
Quittwood No. 2 Preparation Plant
Samples collected by Mr. Jack Tabor
(Three sweeps used for this test per each time)
Start - 1105 , „ .. ,
.,-- Involves No. 7 and
coal collection
Hold
1230
1245
1300
1315
Hold
1555
1610
1625
1640
1655
1710 Stop.
Scrubber Water Sample Collection Times
Date Time
6/19/75 1530
6/20/75 Not Available
6/23/75 1840
6/25/75 Not Available
-------
SAMPLING TASK LOR
Plant
Date
— I'
Plant Location
Recorded by
-/
Comments
Run
Sampling location Clock Time Elapsed Sample
(Port) Pollutant Began Ended Time (mln) Nos.
JUUJL.
3V-*- / 3
Woo
64
S&VTH*
Or
2-
fir r /
/£.(.
•f
,/
- 34 £**<*>**«
-------
Plant
Date
Comments
SAMPLING TASK LOR
Plant Location
Recorded by
"id*.
Sampling location Clock Time Elapsed Sample
Run (Port) Pol 1 utant Began Ended Time (min) Nos.
-/>
/SV3
If
It
nn
96
3-?- y-y
r
o
~U1
- 3. 6
/PS ?
fio-j
-------
SAMPLING TASK LOG
Plant
Date
Plant Location
Recorded by
Comments
Run
Sampling location Clock Time Elapsed Sample
(Port) Pollutant Began Ended Time (mln) Nos.
/r
6
/*¥?
a
ON
f
/7/0
1704 A
-------
Plant
Date
uun
.Tte&ih^A
Plant Location
Recorded by
'
Coments
Sampling location Clock Time Elapsed Sample
Run (Port) Pollutant Began Ended Time (min) llos.
.\
s*
>f
o
I
--~J
A
? r~- ff' •/>.;, (t
/ /
-------
Plant
Date
U V
SAMPLING TASK LOG
Plant Location
. Recorded by
X v
Comments
Sampling location
Run (Port)
Clock Time Elapsed
Pollutant Began Ended Time (min)
Sample
Nos.-
• W~~
ly
W^ PJK& W.*fcfliv\»
MWlflP**
v
>A
7!
o *
•»\
to
htlyv^
r\i^
f
I
a
-------
Plant k/ vut£.ku\
Date ~ -^
Comments
Run
SAMPLING TASK LOR
___ • Plant Location _
__ Recorded by >
Sampling location
rx.
lP_ort]
Clock Time Elapsed . Sample -
Pollutant Began Ended Time (min) Nog. .
f
O
Oi-ttirt /
-^.d^T r.f.+fi - A
CKl . l£ *~^ Jj • ^f./
it(, A^-
'/A
A, -^ x
11-
~v\
i t
.
c
76
-------
Date
v 0
f^-ft Y
Plant Location
Recorded by
o /t ;?.-!• -nf / /(/
Comnents
Run
Sampling location Clock Time Elapsed
(Port) Pollutant Began Ended Time (min)
.Sample-fj
Hps. 1
"•f^/oftJlti cAflu
'\_ ^
fa
«~ 30.
;o-
.ttQ r/M;
-------
* LUh
Plant. LO-JL*
Date
- ,i's - 1 S
' •' -A/L
Plant Location'
Recorded by
i XA.VUI
'
t £•, (J ^ •
x
Comments
Run
Sampling location " ,. Clock Time Elapsed Sample*
(Port) Pollutant Benan Ended Time (min) NQS.
fr
(min)
'
JUki '/
' V
/.'U
al, A 0-Aa
//.
/ c
y
- / ?
f
H H "
ft ., -
u
• 1-1?
A
' /
A
f^U.
c \x
u>-i\L
/•
,iV
4i
-------
Plant
Date
<• ?
Plant Location
Recorded by
h' r
s-*1 m.v\j..vn
. .'lW v '
Comments
Run
Sampling location Clock Time Elapsed Sample^
(Port) Pollutant Began Ended Time (min) Mos. '
*
eke? £L. (
n*.
Aoi
c
c.-tlVl- /V
- -6
/m
/
—">.•
—**•
•^:
.c
It 2-*
-
*-" ilki '
c>n
hi (tax
AA/v ^ . Mt-
../-rf:\
...A AS JL
!-JK J.A^.
-------
APPENDIX E
PROCESS OPERATION FIELD DATA
-------
«M<« J f'?|lv .•-•* ftr-'f*'• r,lr,0.
JZ
ove
V
VI
To
SI
H
H
ib
I
. o .
zo
V7
JS
If!
#
1
1-1
4
,oU'
1«
1
-
0
1
-
1
-
-
5
i
a
1
n
•s
Jffi
s
1
-
.«,
;
^
3
5
vw
i
t-
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-------
APPENDIX F
SAMPLE IDENTIFICATION LOG
-------
APPENDIX F — SAMPLE IDENTIFICATION LOG
Fartlculate samples
collected on outlet
-side, Met.hod 5 • •«•.
SAMPLE LCO
IDENTIFICATION
Weotmorelc.-ui •: *•
Quinwoo3, V.'. Vi;
Coal Cloanlrr- P*.
June
EPA NO.
411
412
.. 413
.. 414
- 416
417
Dato Sample
.
i Dlacription
6/l8lGlass fiber filter
Acetone ,probe rinse
Impineer water+rins€
.
6/19
"*" ' r ' ' "
418 1
419
420
431
432
433
, 434
435
"6/20
441 6/23
442
443
444
$%5- '
j
452 I
454
'*•""" • • "*r- i
.. 455
w, - |
Final
Glass
Aceto
Impin
0hlor
Fin.
. „
Glas
Acet
acetone rinse
fiber filter
ne, probe .rinse
ger water+rlnse
o/Ether Ext.
Acet. rlns, bac
s fiber filter
one probe rinse
Run Romarlco
No. . i
QNC-1 :
n .-...-
it
" "f
n . j
I . t
QNC-2 2 filters
« contains-^IO ml condensate
11 filter leaked, dust In 1st iaj
" i
^ " ... .
_ j. ,,, . Tllll T . . __ i
tQNC-3 -3 filters
Imping, water + rinse . j
Chloro/Ether Ext.
Fin. acet rlns , bac
Glas
kceto
Impl
Ohio
j Flna
!
a fiteer filter
ne probe rinse
nger water * ri
ro/Ether Ext.
I acetone ^ rinse
6/26 ^ Gl-ass fiber filter
[
!F [ -
I
t
Q^NC-4 2 filters
ii '
ise +
t
t
QNC-5 2 filters
l Acetjone proberinse '
- - 4 - ••• j- - - - •• -j -
i Implnger water + riftse i
f
• i
,
Ohio
Flna
ro/Ether Ext , .. .
1 acetone rinse
......... j,
i ;
:._.._, : .J
-------
Clean-up Background
Evaluation Samples
SAMPLE LC3
IDENTIFICATION
EPA Ho.
S-75-CQ1-
Datof
i
-401
402
; 6/17
"
- . 403 j "
404 i "
405
406
tl
6/1
407 "
408 "
409
410
,, 421
42?
,i . 423
424
425
426
427
428
•" "~ ~
fl
II
6/18
6/19 I
j 429
430
1
4^6 '•
._ 437 ,
438 |
439 :
440 '
-.- H
6/20.
I
3amplc
Glas
Ace
Impl
Chic
Flna
fGlas
Acet
Impj
-C.K1...
! Dlccription
a fiber filter
t. rinse, probe
nger Water+rins
ro/Ether Extof .
1 Acetone rinse
s filer filter
one rinse .probe
naer HoQ+rlnse
ro/Ether» T^-jct. .
Flnall Acetone rinse
Glas
Acet
..IlPl
Colo
Eina
Glas
Acet
.ispi
.Chlo
Flna'
«
_Glas
Acet
Impi
a fiber filter
one probe rinse
tiger HgOj-rlnse
ro/Ether Ext.
L_Ac.eJtone_ rJjnse
s fiber filter
one probe rinse
nger HoO+rinse
£ l - -
PO/Ether-£jtk, —
1 Acetone .rinse
s fiber fJJLte_r_
one probe wash
ng waters rinse
[•- - •
Chloro/Ether. j;xt ,_.. .
Final Acetone rinse
"~ [--"--•;
Run
No.
Romarl
EBK-1 i Glasswai
• it
e «
3 " -
1!
EBK-2
it
it
it
EBK-3
»
ii
ii
ii
TFQV h
Ji.a|v— ^r
Run No.
Class w
Glasswaz
Run No.
Glass w.
Clean-
.. Clean
II
j
" i.
II
II
r
EBK-5 ' Clean-i
ti
L.
"" H '
II
II
rel^r.d Coil Co.
Quinv/ood, ";. Vir-inic.
Coal Clcar.ifi-; l^'J.ant
June 1975
Clean-up after Run # QNC-1
QNC-2
;j
-------
F-3
Clean-up Background,
Evaluation Samples SAMPLE LOG
IDENTIFICATION
Westmoreland Coal Go
Qulnwood, w. Virginia
Coal Cleaning Plant
June 1975
EPA No.
3-7^-001 .
446
44?
448
449
450
493
494
- /495"l
^ I
496
i
,
-»-
Date
6/2^5
6/25
f
Sample Description
mass fiber filter
Acetone, probe rlns«
Implnger water ,rins
Chloro/Ether Ext,
Final acetone rinse
BLANKS
Run
No.
ESK-6
Remarks
01ean-ur» after Run * q:;<
Glass fiber filter BLANKS 3 ea.
200 rol Acetone blank
200 ml distillsd water
Burdick & Jackson distilled in glass,
Lot No» 7150
BLANK OSU prepared by OSU
Chloroform 4 Ether BLAIiK
. „
i-4
-------
F-4
Grab samples of
dryer feed, scrubber
water, & process •
.n3 Coal Co.
Qulnwood, '". Virginia
Coal C3oar..4.fwc Plant
EPA NO.
Dato£
Sample
i Dlscriptlon
553
..6/19.
564 I 6/23
__j vi/_fi
J66_
58
-Coa] ..
Dryer feed f4 btla.
Z feed to dryer
Coal feed to dryer
Re turn wa t e r from_ae m J, B tg a%.__.
Run
No.
Renarko
""Collected 1800
—itotal wt. 2.36 Kg
: Total sample discarded-
" "
6/1SL
_6/20.
6/231 Eetu!rn water from d'emlster!
Return water frome demister
_jue. o/fc.'/- JT.CUU
-_583 ....
i/i!'
•
,_J
dlt
\
I .. •
-
.
i
*-zi wet^ei- ii-om g^eraister
to— to be used
v>f -O^ ' (
i
• •• • --
•
p "blend of Pocahoritls and
gal)Sewell # atrip
run. -
-------
APPENDIX G
CYCLONE SAMPLE LOG AND ANALYTICAL RESULTS
-------
APPENDIX G
-,- , ,j_
i. .'. _.,..L ....,.-, 4-..-1-
!•*• /»;. < ,>.t-'s. ' '•
— CYCLONE SAMPLE LOG AND ANALYTICAL RESULTS
Westmoreland Coal Co,
""•] 'J Qulnv/ood, W« Virginia
w^H. „;:•.,; Coal Cloaning- Fla,nt •
-------
'G-2
SAMPX-S IXXJ
IDENTIFICATION
Westmoreland Coal Go.
Qulnwood, w, Virginia
Coal Cleaning Plant
Ho.
Date sample Description
Run
No.
Remarks
F.
/PC,
••
/oc
roe
tfb
FT
0 D c| O
/oc
0-
/.
o,
o.
//C
y 2
IfC
o
A /j^i. £>*S*>1=,tf
ifC
0 • (70
o.
O .
Z c
0 , o \ 7.
/2-C
a.
o.
¥77
O-
-------
APPENDIX H
DIAGRAM OF SAMPLE EQUIPMENT SERIES CYCLONES
INCLUDING CALIBRATION DATA
-------
APPENDIX H
To Pump
Back-up filter
Cyclone 2
Nozzle
Cyclone 1
FIGURE H-l. SERIES CYCLONE SAMPLING APPARATUS BLOCK DIAGRAM
-------
d "£-l:-: Ssii '^'S^ii;?^
j-:!=::;l::i:! T"
::i;.:r..; :|;:. :: ; i :;: . !:.;
1.5
,2 2.5 ,3 .4 .5 .6 .7 .8 .9
2.5 3
Flowrate (ac£m)
FIGURE H-2.
CUT OFF POINT VERSUS FLOW RATE CALIBRATION
CURVES FOR EPA SERIES CYCLONE
-------
H-3
B
S-i
0)
4J
0)
w
•H
ft
0)
t—I
u
S-i
CQ
E-
<
C
2
i-
E-
0
-------
APPENDIX I
DETAILED STANDARD SAMPLING AND ANALYTICAL PROCEDURES
-------
APPENDIX
DETAILED STANDARD SAMPLING AND ANALYTICAL PROCEDURES
The sampling procedures described in the December 23, 1971,
issue of the Federal Register. Methods 1, 2, 3, and 5, have been used
as a reference for the source emission measurements conducted at West-
moreland Coal Company, Quniwood, West Virginia.
For scrubber inlet sampling, an Alundum thimble was added to
the standard Method 5 sampling train. This thimble was located between
the nozzle and the probe (as shown in Figure 16) and was inside the stack
during sampling.
Sample-port location, for the most part, is determined from
stack geometry so that representative samples may be obtained for deter-
mining particulate emissions. Any restrictions or alterations in the
stack gas flow must be considered. (Stack sampling locations are given
in the main body of this report.)
After selecting the appropriate stack sampling location, number,
and position of sampling points as described in Method 1, a preliminary
traverse of the stack was completed to determine the average Ap and average
gas temperature. These data were then used, with the aid of a nomograph,
to determine the appropriate nozzle diameter which would allow for iso-
klnetic sampling at an air flow rate consistent with proper sampling train
operation.
The sample trains were prepared for operation as outlined in
Method 5. The glass filters and Alundum thimbles used for particulate
collection were desiccated for 24 hours and the tare weight determined.
During the sampling period, isokinetic flow was maintained by
adjusting the sampling flow rate to compensate for stack Ap and tempera-
ture variations. Field data for all runs are presented in Appendix C.
After the completion of each test and the recording of the
appropriate field data, the inlet and outlet sampling trains were removed
from their respective platforms and taken to the temporary field labora-
tory. The probe assembly was removed from the sampling train; the ends
were plugged and the probe allowed to cool. The Pyrex tube and stainless
-------
1-2
steel nozzle were then thoroughly cleaned with a nylon brush and rinsed
with reagent-grade acetone into a precleaned screw-cap glass container.
The glass filter used at the outlet location was removed from
its holder and placed into a desiccator for drying. Mass values were
determined after 24 hours.
The side of the glass filter holder facing the probe was rinsed
with reagent-grade acetone and emptied into the probe-acetone-wash container.
The weight of acetone and wash residue (after drying) and the net filter
weight comprise the total mass of the collected sample. The weight increase
of Drierite in the fourth impinger plus the net condensed liquid in the first
three impingers was used to determine the stack gas moisture content.
Samples of the acetone used to clean the glassware were taken
from each container that was used in the field to determine the amount
of residue from blank acetone.
Cyclone catches (collected by EPA) were desiccated and mass values
determined after 24 hours.
Special handling of the inlet thimble -catch was necessary in that
particle-size distribution was to be made on the particulate. After re-
moving the thimble from its holder and a mass value determined, the thimble
and contents were placed in a plastic bag and sealed. Agglomeration during
routine drying could possible alter the size distribution, therefore, the
thimble catch was not desiccated. The thimble and special EPA multiple-
cyclone catches were returned to Battelle-Columbus for an extensive
laboratory study to determine factors, if any, which could alter or in-
fluence the particle-size data. The results of this study and the techniques
used to obtain sample aliquots are reported in the body of the report.
In summary, the techniques described in the body of the report which
have been used to evaluate various aspects of particle sizing methodology,
essentially indicate that routine techniques, when using a Coulter Counter'- ',
can be employed when determining particle-size data from coal samples.
For this study the wetting agent used was TRITON X100 and the electrolyte
was 4 percent sodium chloride.
-------
1-3
(2)
The Mine Safety Appliance particle size analyzer used for
sizing the <325 mesh bulk coal samples employed an isopropyl alcohol
for the sedimentation liquid and a proportion of 50 percent isopropyl;
50 percent heptane for the feed liquid (See this Appendix for information
relating to the theory of operation of the Coulter Counter and the MSA
particle size analyzer).
Visible emissions data were determined by two certified observers
using EPA Method 9 as a guide. All pertinent data, as required, were
recorded and is contained in Appendix C. For the most part, an attached
steam plume was present during the visible emission readings. As described
in EPA Method 9 , paragraph 2.3.1, the opacity observations were made
beyond the point in the plume where water vapor was no longer visible.
Pertinent data, regarding distances from the stack exit to the observa-
tion point are recorded on the field data forms, Appendix C, and also
in the body of the report.
There were short periods of time when only one observer was
reading visible emissions, therefore, during those time periods, the
computer data summary (B-l and B-2) reflect averages which are low by a
factor of two. However, the data plots which relate the time of day to
percent opacity (Figures 11-15) show the average data of the two observers,
or where pertinent, the data when one observer was reading.
-------
1-4
PARTICLE SIZE ANALYSIS
by
MINE SAFETY APPLIANCE PARTICLE SIZE ANALYZER
portance of Particle Size Analysis
As industrial development and competition continues
a rapid pace, particle technglogy problems have also
ItipHed. Most of the time it is found that particle size
tribution measurement provides the key to a scientific
utton.
In spite of a long felt need for satisfactory size
ilyzers and the development of a. great diversity of
truments and techniques, no single instrument has been
veloped which has sufficient accuracy, convenience of
erjtion and flexibility to truly be called a universal size
ab'Z'jr, The resulting lack of standardization has lead
endless confusion and misapplication of good, but
nited, techniques. Therefore, the reason for design and
velopment of the MSA Particle Size Analyzer can best
appreciated by discussing briefly- the size analysis
oblem along with the important analytical methods.
ie Particle Size Analysis Problem
Particles of industrial and scientific importance range
om the coarse sand or gravel size down to submicro-
opic size. The measurement of sieve size particles
ibove 200 mesh or 74 microns) does not present much
F a problem. It is the subsieve particles between approxi-
ately 0.1 and 40 microns which represent the greatest
roblem. Most airborne dusts, paint pigments, and many
ours, chemicals,'Pharmaceuticals, etc. He within this size
inge. Measurement in this range is difficult for several
rasons:
First, is the fact that the relatively broad size distri-
utions of most powders of interest makes it practically
^possible to make an accurate conversion of microscope
ount size analysis to the weight distributions that are
isually desired.
Secondly, most powders contain just enough sub-
nicron particles so that the limit of resolution of the
ight microscope, the slowness of gravity sedimentation
md the deaggregation problems of the elutriation methods
nake these methods relatively unsatisfactory in the sub-
nicron range. On the other hand, all centrifuge methods
:annot analyze powders containing particles above 5
•nicrons.
The characteristics of the most important size analysis
methods are varied and frequently conflicting in results.
The MSA Particle Size Analyzer
U can be seen that the MSA Particle Size Analyzer
strikes perhaps the best compromise between range,
accuracy, sj>ce«l, cost ami utility of any instrument avail-
able at present. The instrument embodies the research and
experience of a number of largs industrial firms as -*ell
as the University of Minnesota where the original
development took place.
It has been used successfully to measure the size
distributions of practically every powdered ma-erial of
industrial importance. It is also being used for ihe size
analysis of less than milligram quantities of airborne
dusts sampled by impinging or filtering through hSzh
efficiency media.
Because of its sj;eeJ and convenience it is p^r'ia:--? the
only available iniJru.-.-.ent, at pr^enl, suite i for .j'_i'!',y
control purposes in the subraicron size ranges,
Principles of Operation
In common with all sedimentation size ar.diysis
methods, this instrument utilizes the relationship between
particle settling velocity and particle size known, derived
from Stoke's law.
For gravity this is:
Equation I
t = 18.37 x 108 u0h
(p-Po> 8 d2 "*
where t = time in sec. to settle a distance h in cm.
uo = absolute viscosity-poise
p ss: particle density — gm/cm
Po — Sedimentation liquid density—gm/cm
d s= particle size — micron
g s= gravitational constant = 980 cm/sec
From Equation I it is seen that the time to settle a
given distance is inversely proportional to the square of
the particle size and a function of the viscosity and of
particle and liquid density. Because it requires about 24
hours for a 1 micron particle of 2.7 gm/cc density to
settle 10 cm. in water, centrifugal force is required to
reduce the settling time of submicron particles to a
reasonable value. This is why the MSA Particle Size
Analyzer utilizes both gravity settling for the coerce
particles and centrifugation for the fine.
The settling rate of the particles can be sensed in a
variety of ways. This method utilizes a special centrifuge
tube with a small capillary at the bottom. The particle
size distribution is calculated from the ratio of the ob-
served sediment height in the capillary at times corres-
ponding to the desired particle sizes; to the height after
alt particles have settled. Though simple, this method
sensing, in combination with the sedimentation from a
layer, makes it possible to use centrifuges having short
radii, without Increasing the complexity of calculation.
-------
1-5
Outline of Procedure
The basic procedure is illustrated in Figure 1 ant] is described therein:
Basic steps in particle analysis with MSA Particle Size Analyzer
Tr«n»f«c suspen
sion to fei
Pfs
Trmnnfer fesdinj
cha.T.b«r to cen-
trifuge tube.
e f*eiiri
ehanb-fr, U?.v,ir.<
•harp Uyur of *-.*•
peniian on '.op of
8
Read sediment
height under jrra v-
ity in projector «t
precalculated
times*
6
Transfer to first
centrifuge and run
for precalcutated
time, then remove
•nd read in pro-
jector.
Transfer to suc-
cessive centrifuge
•peeds or centri-
fuges us called for
on schedule until
run is complete.
Sue distribution
11 obtained from
aedtmeat height
d«t», tnd tabula-
ted M shoHO in
Table I md plot.
ted ** in Figure
Figure 1
The complete Instrument includes centrifuge tubes,
feeding chamber, an optical tube projector, one or more
special centrifuges and tube handling and cleaning
accessories. To provide the greatest flexibility at the
lowest cost consistent with the requirements of each
application, the major component?, such as projector and
centrifuges, have been designed as separate units. The
method may be established with a minimum investment
and then expanded by the addition of additional centri-
fuges, etc. Below are described the different units
available and the combinations recommended for such
applications.
Measuring rods are useful for rapidly measuring out
enough powder for a run when the disperation of the
of the powder is performed in the feeding chamber. The
scoop provided will be approximately correct for most
materials, but different hole volumes may be required for
materials of different bulk densities.
For the analysis of some fine powders and for the
analysis of atmospheric dust samples, it is desirable to
have available a commercial high speed centrifuge. This
is used for concentrating dilute suspensions of particles
end for determining size distribution and points.
Centrifuges
To meet the critical requirements of size analysis
methods, four special centrifuges (300, 6004200, 1800
and 3600 r.p.m.) have been designed. These centrifuges
have the following special features:
1. Constant speed obtained by use of a high quality
hysteresis type synchronous motor.
2, Stable starting and stopping characteristics having
a maximum rate of acceleration of 5 radians per
see. This is obtained by the correct combination
of inertia, starting current, aerodynamic resistance
and friction introduced by an electromagnetic
brake,
3. Ability to be stopped and started by an interval
timer without manual adjustment of any speed
control device.
4. Reliability resulting from simple rugged design and
absence of electronic controls.
A voltage regulator may also be used so that starting
and stopping calibrations are maintained. This should be
a constant voltage transformer with an output of 250VA,
A.C.
Variable resistors are provided for adjusting the
starting time of the centrifuge. The procedure for check-
ing and adjusting the acceleration U discussed in the
maintenance section of this manual.
-------
1-6
PARTICLE SIZE ANALYSIS
by
MODEL "B" COULTER COUNTER
1, The Coulter Counter determines the number and size of particles
suspended in an electrically conductive liquid. This is done by forc-
ina the suspension to flow through a small aperture having an immersed
electrode on either side.
2. As a. particle passes through the aperture, it changes the res is'
ance between the electrodes. This produces a voltage pulse of shore
duration having a magnitude proportional to particle volume. The ser-
ies of pulses is then electronically scaled -and counted.
_ vacuum
-H--GS
•scope
_, COUNTCR "START-STOP"
i
DIGITAL
REGISTER
3, When the vacuum stopcock is opened, a controlled external vacuun
initiates flow from the beaker through aperture and unbalances the mer-
cury siphon. Closing the stopcock then isolates the system from the
external vacuum, and the siphoning action of the mercury continues the
sample flow.
4. The advancing mercury column makes contact with start and stop
probes to activate the electronic counter. The probes are placed pre-
cisely 50, 500, or 2000 microliters apart, providing a constant sample
volume for all counts.
5. The voltage pulses are amplified and fed to a threshold circuit
an adjustable threshold level. If this level is reached or ex-
ceeded by a pulse, the pulse is counted. The threshold level is in-
dicated on an oscilloscope screen by a brightening of the pulse seg-
ments above the threshold facilitating the selection of appropriate
counting levels.
6. By taking a series of counts at selected threshold levels, data
are directly obtained for plotting cumulative frequency (larger than
s*ated size) versus particle size. Integration of all or part of the
resultant curve provides a measure of the particle content of the sus-
-------
1-7
7. Before plotting, the counts are first corrected for coincident
particle passages (doublets, triplets, etc.). These corrections are
quite precise, and if kept to a moderate level (say, 5 or 10 percent),
the overall accuracy of measurement of particles becomes a function of
the number counted. The large numbers of particles counted (tens of
thousands), provides low statistical deviation.
8. The pulse height and instrument response are essentially pro-
portional to particle volume, and to fluid resistivity for particles
up to 30 or **0 percent of the aperture diameter. The particle resist-
ivity has very little or no effect.
9. The principle does not permit significant discernment of par-
ticle shape, and results are expressed in spherical equivalents. This
proves to be valid, as sufficiently high numbers of particles are
counted to assure an averaging of orientations of particles traversing
the aperture.
10. In the main, the theoretical bases of the Coulter Counter are
quite simple, and "side effects" are notably few in number and small
in their influence on the results. The accuracy of the measurements
is not limited by the instrument, but is simply a matter of the degree
of care exercised in its use.
11* The instrument is inherently simple to calibrate.
-------
APPENDIX J
PROJECT PARTICIPANTS AND TITLES
-------
APPENDIX J
PROJECT PARTICIPANTS AND TITLES
FieldTeam
Paul R. Webb, Senior Technologist (Team Leader)
William C. Baytos, Scientist
Donald Hupp, Technician
Justin McNulty, Chemist
J. Mason Pilcher, Mechanical Engineer
Fred L. Rice, Technician
Ronald E. Snyder, Biologist
James J. Tabor, Technician
Karl W. Turner, Technician
David A. Trayser, Mechanical Engineer
Administrative and Technical Support
Richard E. Barrett, Program Manager and Associate Section Manager
Stephen D. Ban, Section Manager
James A. Gieseke, Research Leader
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APPENDIX
TEST LOG
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APPENDIX 1C
TEST LOG
June 16, 1975
June 17, 1975
June 18, 1975
Jane 19, 1975
June 20, 1975
June 23, 1975
June 24, 1975
June 25, 1975
June 26, 1975
Transport equipment to test site area.
Arrive at test site
Set up field lab, sampling equipment at outlet
Run velocity traverses at inlet and outlet
Redesign inlet sampling ports.
Complete inlet sampling setup
Rerun velocity traverse at outlet with new
straightening vanes
Particulate runs QNC-1 and TH-1
Dryer feed sample,
Particulate runs QNG-2 and TH-2
Dryer feed sample
Scrubber water sample.
Particulate runs QNC-3 and TH-4 (Run TH-3 aborted)
Dryer feed sample
Scrubber water sample.
Particulate runs QNC-4 and TH-5
Dryer feed sample
Scrubber water sample.
No sampling due to plant operational problems.
Particulate runs QNC-5 and TH-6
Dryer feed sample
Scrubber water sample
Remove and pack field lab and sampling equipment
Transport to Columbus.
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