United States
Environmental Protection
Agency
Office of Air Quality
Planning and Standards
Research Triangle Park. N'C 27" 11
EPA - 454/R-99-041c
August 1999
Air
®EPA
Integrated Iron and Steel Industry Final Report
Manual Testing
Volume III of III
Youngstown Sinter Company
Youngstown, Ohio
Clean
-------
Integrated Iron and Steel Industry
Final Report
Volume III of III
Appendices
Contract No. 68-D7-0068
Work Assignment 2-13
Youngstown Sinter Company
Youngstown, Ohio
Prepared for:
Michael K. Cioiek
Emission Measurement Center
Emission, Monitoring, and Analysis Division
Office of Air Quality Planning and Standards
U.S. Environmental Protection Agency
Research Triangle Park, North Carolina 27711
August 1999
*ERG
EASTERN
RESEARCH GROUP, INC
-------
Table of Contents
Appendix C Metals Laboratory Analysis Data
Appendix D Particulate Matter Laboratory Analysis Data
Appendix E Field Data Sheets
-------
Appendix C
Metals Laboratory Analysis Data
-------
CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Method 29 April 1996 Rev.
Client: Eastern Research Group
TLI Project Number: 43159A
Date: October 20,1997
This report should only be reproduced in full.
Any reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 25-Sept-96
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491
1
-------
Triangle Laboratories, Inc.
Case Narrative
October 20,1997
TLI Project#: 43159A
Overview
Twelve train samples, one blank train sample, and two DI water samples were analyzed
for arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), selenium (Se), and mercury (Hg). For all
analyses, the samples and associated QC samples were prepared and analyzed following
the guidelines of Method 29 April 1996 Rev. Results reported relate only to the items
tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:
Sample Receipt:
Twelve train samples, two blank train samples, two DI water samples, and five filters were
received without coolant on September 09,1997 under project# 43159 and in good condition.
Sample YCP-169 arrived with these samples, but was not listed on the client's chain-of-
custody. Per the client's request, this sample was not analyzed. Samples YCP-21, YCP-27,
YCP-33, YCP-44, and YCP-59 were missing from the shipment. Samples YCP-21, YCP-27,
and YCP-33 were later received at 22 °C on September 10,1997 under project# 43187 in
good condition. These samples arrived without coolant which resulted in the high temperature.
All samples (except the six filters) were combined and analyzed under project# 43159A. Only
the twelve train samples, one blank train sample, and two DI water samples were reported in
this data package.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), beryllium (Be), cadmium (Cd), chromium (Cr), manganese (Mn), nickel
(Ni), lead (Pb), antimony (Sb), and selenium (Se) concentrations were determined by
Inductively Coupled Plasma Emission Spectroscopy (ICP). Cobalt (Co) concentrations
for the back half samples were determined by Inductively Coupled Plasma Emission
Spectroscopy (ICP).
2
-------
Triangle Laboratories, Inc.
Case Narrative
October 20,1997
TLIProject#: 43159A
Cobalt (Co) concentrations for the front half samples were analyzed by Graphite Furnace
Atomic Absorption (GFAA).
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
The linear range for the instrument TJA 61E Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995. A calibration curve, based on a blank and one standard, is established for each
analytical run, followed by a check high standard and an initial calibration verification
(ICV). The check high standard does not deviate from the calibration curve by more than
5%. In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical run.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(IDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values of
1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs) except Ni. The following guidelines
may be used to assess analyte concentrations relative to the method blank: 1. Analyte
quantitations should be considered valid if the level of blank contamination is less than five
percent of the level detected in the field sample, 2. Analyte quantitations should be
considered estimated if the analyte level in the sample is five to twenty times the level of
the analyte in the blank, or 3. Analytes whose level in a sample is the same as or less than
five times the level detected in the associated blank should be considered present likely
due to laboratory contamination and not native to the sample. The contamination of Ni in
the front half samples is insignificant in comparison to the level of Ni in the native samples.
Please note that the concentration of the back half samples should be considered biased
high near the lower end of the calibration range due to possible contamination.
The analysis by ICP demonstrated negative cobalt (Co) concentrations for the front half
samples, therefore, the front half samples were reanalyzed and reported by Graphite
Furnace Atomic Absorption (GFAA).
Some samples were received near the 28 day sampling to analysis holding time for Hg,
therefore, the lab was unable to analyzed them within the holding time for Hg. All
samples were analyzed outside the 28 day sampling to analysis holding time for Hg and
within the six month sampling to analysis holding time for all other requested analytes.
3
-------
Triangle Laboratories, Inc.
Case Narrative
October 20,1997
TLI Project#: 43159A
Two missing blank components (YCP-44 and YCP-59) were not sent by the client,
therefore, two separate blanks were not prepared. Sample YCP-57 was used with samples
YCP-45 and YCP-46 in order to make a complete blank train sample.
The serial dilution result for Cr for the sample YCP-88,01,02 FH demonstrated a RPD
outside the QC control criteria of 10.0 percent, which indicates the presence of a
significant amount of interferents specific to these analytes in the native sample matrix.
Please note that the post-digestion spike (PDS) demonstrated a percent recovery within
the QC criteria. Also note that this sample should be considered biased low for Cr due to
matrix interferences.
A duplicate analysis was not reported for Co for sample YCP-89,07,08 FH which was
analyzed by GFAA. The GFAA instrument analyzes two separate aliquots of the sample
and averages the values for a final result. These two analyses agree within a RPD of 20%
or a second run is done for that sample. The ICP instrument analyzes one continuous
aliquot three times and averages the values for a final result. The ICP does not take two
separate aliquots, therefore a DA was performed.
The recoveries for the post-digestion spike (PDS) are not reported for Se for sample
YCP-03 BH and Pb for sample YCP-88,01,02 FH. The spike concentrations added were
insignificant in comparison to the levels of this analyte present in the native sample.
QC requirements:
The duplicate analyses for analytes analyzed by ICP cannot be considered valid qualifiers if
the concentrations of the analytes in the original and/or duplicate sample are not at least
ten times the respective RDLs. The RPDs for these analyses are indicated by or "
-------
Triangle Laboratories, Inc.
Case Narrative
October 20,1997
TLIProject#: 43159A
The quality control range for percent recoveries of laboratory control spiked samples is
The quality control range for percent recoveries of spiked samples is 75-125. If recoveries
are outside this range, a matrix effect is suspected.
If the analyte concentrations analyzed by GFAA in the native samples are less than five
times the respective RDLs, or if valid serial dilution analyses demonstrate RPDs outside
the ten percent quality control range, the percent recoveries of post-digestion spiked
samples is 75-125. If recoveries are outside this range, all matrix-related samples are
analyzed by the Method of Standard Additions (MSA). The MSA analysis for each
sample is reported only if the correlation coefficient value is at least 0.995.
By our interpretation, the analytical data in this project are valid based on the guidelines of
Method 29 April 1996 Rev. Any specific QC concerns or problems have been discussed in
the QC REMARKS section with emphasis on their effect on the data. Should Eastern
Research Group have any questions or comments regarding this data package, please feel
free to contact Project Scientist, Amy J. Boehm, at (919) 544-5729 ext.268.
For Triangle Laboratories, Inc.,
Report Preparation Quality Control
80-120.
Linda F.nes
Report Preparation Chemist
Brenda
Report Preparation Chemist
The total number of pages in this data package is;
5
-------
.yn-."
TRIANGLE LABORATORIES, INC.
LIST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Certification pending. Certificate
Number 0226-01. Accreditation for technical competence in Environmental Testing.(Including
Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AGX/TOX,
Volatiies, Pesticides, PCB's, BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management. Expires December 31, 1997.
Laboratory I.D. # 40950, Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21, 1997.
Certificate number OS-Q0397. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX.
State of California, Department of Health Services. Expires August 31, 1999. Certificate
#1922. Selected Metals in Waste Water; Volatiies, Semi-volatiles, and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Certification pending. Registration #
PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31, 1997. Certificate #NC 140.
Dioxin in drinking water.
Florida Department of Health and Rehabilitative Services, Expires June 30, 1998.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/FCB's
(GC) and Volatiies (GC/MS) in Environmental Samples. Environmental water ID HRS#
E87411.
Hawaii Department of Health. Expires March 1, 1998. Dioxin in drinking water. "Accepted"
status for regulatory purposes .
Revised 10/15/97 3M
Triangle Laboratories, Inc.
Printed 10/15/97 801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax * 919-544-5491 —
-------
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in drinking
water.
State of Kansas, Department of Health and Environment. Expires January 31, 1998.
Environmental Analyses/Non potable Water and Solid and Hazardous Waste. Method 1613
for drinking water. ID #'s - Drinking water and/or pollution control - E-215. Solid or Hazardous
Waste - E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires December
31, 1997. ID#90Q60. Dioxin in drinking water. '
Maryland Department of Health and Mental Hygiene, Expires September 30, 1998.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires June 3, 1998. Drinking water by
Method 1613.
Mississippi State Department of Health. No expiration date.. Dioxin in drinking water.
Montana Department of Health and Environmental Services. Expires December 31, 1997.
Dioxin in drinking water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until December 31, 1997. ID #67851. BNAs and Vclatiies. Dioxin in
drinking water.
State of New Mexico, Environment Department. Certification pending. Dioxin in drinking
water.
New York State Department of Health. Expires April 1, 1998. ID #11025. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires August 31, 1999. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management. Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatiles and volatiles; TCLP.
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31,1997. Certificate # R-076. Effective October 4, 1993. Dioxin in drinking water.
Revised 10/15/3? RM
Printed 10/15/9?
i
-------
Oklahoma Department of Environmental Quality. Expires August 31, 1998. Laboratory
#9612. Dioxin by 1613A, 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control.October 31,
1997. Certificate number #99040001 (drinking water). Expires August 31, 1999. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiies, and PCBs/pesticides
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractables for Solid
and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February 5,
1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit. Expires September 30, 2001. Permit No. S-
3790. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockbourne Landfill Site Investigation, Defense Distribution Depot Projects,
and assorted projects for the USACE North Pacific Division Laboratory.
U.S. EPA Region V, Expires November 14, 1999. Dioxin in drinking water.
U.S. EPA Region VIII, for the State of Wyoming. Expires November 13, 1997. Dioxin in
drinking water.
State of Utah, Department of Health. Expires December 31, 1997. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiies under RCRA; Volatiies
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30, 1998. ID # 00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 11, 1998. Lab
Accreditation Number C067. Scope of Accreditation applies to water analyses for
Polychlorinated Dibenzo-p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile)
Organics and Purgeable (Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1998. Dioxin in drinking water.
Lab I.D. 129
State of West Virginia, Department of Health. Expires December 31, 1997. Certificate No.
9923(C). Dioxin in drinking water.
Revised 10/15/97 RM
Printed 10/15/97
-------
State of Wisconsin, Department of Natural Resources. Expires August 31, 1998.
Laboratory ID Number 999869530. Certification for the following categories of Organics:
Purgeable, Base/Neutral, Acid, PCBs, and Dioxin. Expires November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1997. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
N.C. Department of Human Resources. Expires October 31, 1997. Registration number NC-
PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
Food & Drug Administration (FDA) Registration. Expires June 1998. ID #'s 001500
1053481. Annual registration of drug establishment. Annual registration of drug establishment.
OTHER
Clinical Laboratory Improvement Amendments (CLIA) Registration. Expires May 30, 1SS9.
ID # 34D0705123. Department of Health & Human Services, Health Care Financing
Administration.
U.S. EPA Large Quantity Hazardous Waste Generator. No expiration date. EPA ID
#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
North Carolina Radioactive Materials License. Expires April 30 1998. License No. 032-
0954-1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and
use such radioactive materials as designated.
North Carolina General License for Radiation Protection. No. expiration date. License No.
032-875-OG. The general license applies only to radioactive material contained in devices
which have been manufactured and labeled in accordance with specific requirements.
Rsvisad 10/15/97 RM
Printed 10/15/9?
-------
ABBREVIATIONS
BH - Back Haif
CCB - Continuing Calibration Black
CCV = Continuing Ciiihrarion Venficaooii
CHECK HS = Check High Standard
D = DUP = Analytical Duplicate (Prepared DnpficaTB)
DA - Duplicate Analysis
FH = Front Haif
FV = Fnai Digestate Volume
ICS - Tpifial Calibration Blank
ICV = Tpirini Calibration Verification
ICSAB = Interference Geek Solution (Solution AB)
I - Tnirini
F= Fjoai
Solution .A3 contains common imecferexas in addition to the anaiyte of interest.
DDL = Instrument Detection Limit
L = Serial Dilution
LCS = Laboratory Cociroi Spike Sample
MB = Method Blank
MPV = Mercury p^paration Volume
MS as Pre-digestion Spike
MSD - Prs-digestion Spike Duplicate ^
N/A = Not Applicable
N/Av = Not Available
N/V = Not Valid
PDS = Post-digestion Spike
%REC - Percent Recovery
RDL = Reporting Detection Limit
RPD = Relative Percent Difference
T = Analytical Triplicate (Prepared Triplicate; fcr Eg analysis by Method7471 only)
TV = Total Sample Volume
< = Anaiyte concentration in the sample is less than die respective RDL
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Analyte
Units
High Std
ICV/CCV
ICSAB
RDL
Wavelength
Ag
PPb
1000
500
500
1
3280
As
ppb
1000
500
500
5
1890
A1
ppb
1000
500
500000
50
3082
B
ppb
1000
500
500
7
2496
Ba
PPb
1000
500
500
2
4934
Be
ppb
1000
500
500
1
3130
Ca
ppb
1000
500
500000
60
3179
Cd
ppb
1000
500
500
1
2265
Ce
ppb
1000
500
500
3
4186
Co
ppb
1000
500
500
1
2286
Cr
ppb
1000
500
500
2
• ¦ 2677
Cu
ppb
1000
500
500
2
3247
Fe
ppb
1000
500
200000
40
2714
K
ppb
10000
5000
19000
220
7664
Li
ppb
1000
500
500
1
6706
Mg
ppb
1000
500
500000
30
2790
Mn
ppb
1000
500
500
2
2576
Mo
ppb
1000
500
500
2
2020
Na
ppb
10000
5000
5000
300
3302
Ni
ppb
1000
500
• 500
3
2316
P
ppb
1000
500
500
30
2149
Pb
ppb
1000
500
500
2
2203
Sb
PPb
1000
500
500
4
2068
Se
ppb
1000
500
500
3
1960
Sn
PPb
1000
500
500
13
1899
Sr
ppb
1000
500
650
1
4215
Ti
ppb
1000
500
500
8
3349
T1
ppb
1000
500
500
5
1908
V
PPb
1000
500
500
2
2924
Zn
ppb
1000
500
500
12
2062
Note: Use this reference page to review the raw data from the TJA 6IE Trace Analyzer.
This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV), continuing calibration verification (CCV), and the interference check solution
(ICS AB). In addition the reporting detection limit (RDL) and wavelength are reported for each
analyte.
Revision Date: 15-Jul-96
11
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CALCULATIONS FOR AIR SAMPLES
RESULTS FOR TRACE METALS (except mercury):
RESULT in p.g (Front Half) = ^ig/L * FV (mL) * DF
1000 mUL
n RESULT in p.g (Back Half & Impingers) = tig/L * TV (mL) * FV (mL) * DF
mL used * 1000 mL/L
FV = final volume in mL
TV = total volume in mL
DF = Dilution Factor
The RESULTS for combined Front Half & Back Half samples use the same calculation as the
Back Half & impinger samples.
RESULTS FOR MERCURY (Hg):
RESULT in Lig (Front Half) = |ig/L * (mL FV/mL aliquot) * MPV * DF
RESULT in ug (Back Half & Impingers) = ug/L * (mL TV/mL aliquot) * MPV * DF
MPV = mercury preparation volume = 0.1 L
%REC (Percent Recovery) for MS/MSD He spikes:
%REC = spike sample results - original sample results * 100
true spike sample results
NOTE: Original sample results less than the RDL are not used in calulations.
%REC (Percent Recovery) forPDS:
%REC = Spike sample ug/L conc. - original sample ug/L conc. * 100
spike conc. (|J.g/L)
%REC (Percent Recovery) for LCS/LCSD:
%REC = Spike sample p.g/L conc. * 100
spike conc. (jlg/L)
RPDs: RPD = 1 Result 2 - Result 1 I * 100
(Result 2 + Result l)/2 Rev. 2-Oct-96
12
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Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-88.01.02FH
TLI Sample ID:
182-30-1 GAB FH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Anatvte
Cone.
{uq/L}
rat,
Total Vol
mL
Used
rrt, ¦
Final Vol.
DSution
Factor
Total ug
Reai ft
As
15.051
n/a
N/A
100
1
1.51
Be
0.004
n/a
N/A
100
1
< 0.100
Cd
19.262
N/A
N/A
100
1
1.93
Co
6.400
N/A
N/A
100
1
0.640
Cr
103.558
N/A
N/A
100
1
10.4
Mn
173.130
N/A
N/A
100
1
17.3
Ni
68.332
N/A
N/A
100
1
6.83
Pb
1198.959
N/A
N/A
100
1
120
Sb
44.601
N/A
N/A
100
1
4.46
Se
44.639
N/A
N/A
100
1
4.46
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-88,01.02 FH L
TLI Samole ED:
182-30-1GAB FH L
Date Received:
September 09. 1997
Date Prepared:
September 18-24, 1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analvte
*4
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-03 BH
TLI Samole ID:
182-30-1C BH
Date Received:
September 09. 1997
Date Prepared:
Seotember 18-24.1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analyte
toU
Total Vol.
Final Vol.
Iipppl!
Totafug :
: Result
As
13.810
720
620
100
1
1.60
Be
-0.257
720
620
100
1
< 0.116
Cd
0.605
720
620
100
1
< 0.116
Co
4.594
720
620
100
1
0.534
Cr
110.762
720
620
100
1
12.9
Mn
238,203
720
620
100
1
27.7
Ni
20.123
720
620
100
1
2.34
Pb
38.587
720
620
100
1
4.48
Sb
2.902
720
620
100
1
< 0.465
Se
946.637
720
620
100
1
110
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
15
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-03 BH L
TLI Sample ID:
182-30-1C BH L
Date Received:
September 09.1997
Date Prepared:
September 18-24, 1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Analyte
Corse.
iuoL)
irL
TotafVol.
mL
Used
mL
Rnai Vol.
D8ut»n
Factor
Total ug
Result
As
3.270
720
620
100
5
< 2.90
Be
0.035
720
620
100
5
< 0.581
Cd
0.103
720
620
100
5
< 0.581
Co
1.155
720
620
100
5
< 0.671
Cr
23.054
720
620
100
5
13.4
Mn
49.757
720
620
100
5
28.9
Hi
5.032
720
620
100
5
2.92
Pb
8.133
720
620
100
5
4.72
Sb
0.533
720
620
100
5
< 2.32
Se
182.662
720
620
100
5
106
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ED:
YCP-89.07,08 FH
TLI Sample ID:
182-30-2GAB FH
Date Received:
September 09.1997
Date Preoared:
September 18-24.1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Cone.
Total Vol.
mL
wmmmB
mL
1 Final Vol.
Dilution
Factor
Result
As
14.342
N/A
m
100
1
1.43
Be
0.086
N/A
N/A
100
1
< 0.100
Cd
2.094
N/A
N/A
100
1
0.209
Co
4.800
N/A
N/A
100
1
0.480
Cr
158.262
N/A
N/A
100
1
15.8
Mri
180.853
N/A
N/A
100
1
18.1
Ni
115.421
N/A
N/A
100
1
11.5
Pb
1096.979
N/A
N/A
100
1
110
Sb
85.642
N/A
N/A
100
1
8.56
Se
80.201
N/A
N/A
100
1
8.02
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 14-Oct-97 at 01:57 PM
-------
Client: Eastern Research Group
Project Number: 431S9A
Sample Report
Client Sample ID:
YCP-89.07.08 FH DA
TLI Sample ID:
182-30-2GAB FH DA
Date Received:
Sentember 09. 1997
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analyte
Cone.
fuq/U
•• WL.
Total Vol.
mL
Used
mL
Final Vol.
D8ution
Factor
Total uq
Result
As
15.858
N/A
N/A
100
1
1.59
Be
0.063
N/A
N/A
100
1
< 0.100
Cd
2.353
N/A
N/A
100
1
0.235
Co
N/A
N/A
N/A
N/A
N/A
N/A
Cr
159.170
N/A
N/A
100
1
15.9
Mri
181.493
N/A
N/A
100
1
18.1
Ni
115.923
N/A
N/A
100
1
11.6
Fb
1103.107
N/A
N/A
100
1
110
Sb
85.807
N/A
N/A
100
1
8.58
Se
82.205
N/A
N/A
100
1
8.22
Triangle Laboratories, Inc.
801 Capitola Drive * Durbam, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 14-Oct-97 at 01:57 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-09 BH
TLI Samole ID:
182-30-2C BH
Date Received:
September 09.1997
Date PreDared:
Sentember 18-24. 1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone.
taU
mL
Total Vol.
mL
Used
.. mL .:
Final Vd.
Dilution
Factor
Total uq
Result
As
12.694
840
740
100
1
1.44
Be
-0.180
840
740
100
1
< 0.114
Cd
3.931
840
740
100
1
0.446
Co
1.376
840
740
100
1
< 0.156
Cr
124.709
840
740
100
1
..-14.2.
Mn
3101.524
840
740
100
1
. 352
Ni
29.126
840
740
100
1
Pb
59.633
840
740
100
1
6.77
Sb
0.864
840
740
100
1
< 0.454
Se
897.285
840
740
100
1
102
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
19
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-09 BH DA
TLI Sample ID:
182-30-2C BH DA
Date Received:
September 09. 1997
Date Prepared:
September 18-24. 1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Anatvte
Cone.
ml
Total Vol.
mL
Used
tri. .
Final Vol.
Diution
Factor
.Total tig
Result
As
12.983
840
740
o
o
1
1.47
Be
-0.231
840
740
100
1
< 0.114
Cd
3.949
840
740
100
1
0.448
Co
1.741
840
740
100
1
0.198
Cr
124.091
840
740
100
1
14.1
Mn
3086.906
840
740
100
1
350
Ni
29.469
840
740
100
1
3.35
Pb
58.995
840
740
100
1
6.70
Sb
0.055
840
740
100
1
< 0.454
Se
890.588
840
740
100
1
101
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
14-Oct-97 at 01:57 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Samole ID:
YCP-90.13.14 FH
TLI Samole ID:
182-30-3GAB FH
Date Received:
September 09. 1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Cone.
{ucj/L}
:: hi hrtfi
TotafVol.
rnL
Dilution
Factor
Total ug
Result
As
11.772
N/A
N/A
100
1
1.18
Be
0.066
N/A
N/A
100
1
< 0.100
Cd
1.156
N/A
N/A
100
1
0.116
Co
4.100
N/A
N/A
100
1
0.410
Cr
128.091
N/A
N/A
100
1
12.8
Mn
186.247
N/A
N/A
100
1
18.6
Ni
85.064
N/A
N/A
100
1
8.51
Pb
1158.789
N/A
N/A
100
1
116
Sb
63.693
N/A
N/A
100
1
6.37
Se
63.610
N/A
N/A
100
1
6.36
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:16 AM
21
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ED:
YCP-15 BH
TLI Sample ID:
182-30-3C BH
Date Received:
September 09.1997
Date Prepared:
September 18-24,1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone,
fag1}
mL
; Total Vol
mL
Used
mL
Final Vol.
Dilution
Factor
Total ug
Result
As
5.383
800
700
100
1
0.615
Be
-0.082
800
700
100
1
< 0.114
Cd
2.746
800
700
100
1
0.314
Co
0.344
800
700
100
1
< 0.114
Cr
91.342
800
700
100
1
10.4
Mn
577.793
800
700
100
1
66.0
Ni
26.342
800
700
100
1
3.01
Pb
65.347
800
700
100
1
7.47
Sb
0.405
800
700
100
1
< 0.457
Se
691.469
800
700
100
1
79.0
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-91.19.20 FH
TLI Sample ED:
182-30-4FAB FH
Date Received:
September 09. 1997
Date Prepared:
September 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Anatvte
Cone.
(W1)
mL
Total Vol
mL
Used
¦xrL
Final Vd.
D8uifc>n
Factor
Totals
Result
As
218.869
N/A
N/A
100
1
21.9
Be
-12.097
N/A
N/A
100
1
< 0.100
Cd
744.661
N/A
N/A
100
1
74.5
Co
29.700
N/A
N/A
100
10
29.7
Cr
2423.271
N/A
N/A
100
1
242
Mn
6269.022
N/A
N/A
100
10
6270
Ni
431.930
N/A
N/A
100
1
43.2
Pb
14800.228
N/A
N/A
100
10
14800
Sb
51.989
N/A
N/A
100
1
5.20
Se
311.994
N/A
N/A
100
1
31.2
Triangle Laboratories, Inc.
801 Capitoia Drive * Durham, North Carolina 27713 Printed: 07-Oct-97 at 10:16 AM
Tele: (919) 544-5729 * Fax: (919) 544-5491
-------
Client: Eastern Research Group
Pro ject Number: 43159A
Sample Report
Client Sample ED:
YCP-21 BH
TLI Samole ID:
182-58-1 BH
Date Received:
September 09. 1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone,
fuqrt.)
trt.
Total Vol.
mL
Used
mL
FinaiVof.
Dilution
Factor
Totaf u<3
Result
As
35.798
750
650
100
1
4.13
Be
-1.062
750
650
100
1
< 0.115
Cd
176.885
750
650
100
1
20.4
Co
97.456
750
650
100
1
¦~J1 .r
Cr
354.591
750
650
100
1
40.9
Mn
7448.916
750
650
100
1
859
Ni
88,758
750
650
100
1
10.2
Pb
33195.172
750
650
100
1
3830
Sb
1.574
750
650
100
1
< 0.462
Se
236.200
750
650
100
1
27.3
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-92.183.25.26 FH
TLI Sample ID:
182-30-5FGAB FH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Artalyte
111(^(^111
*
Total Vol.
Hi.
Factor
Total ug ¦...
Result :::
As
166.755
N/A
N/A
100
1
16.7
Be
-7.321
N/A
N/A
100
1
< 0.100
Cd
664.753
N/A
N/A
100
1
66.5
Co
82.300
N/A
N/A
100
2
16.5
Cr
2026.857
N/A
N/A
100
1
203
Mn
4895.973
N/A
N/A
100
10
4900
Ni
371.809
N/A
N/A
100
1
37.2
Pb
16746.617
N/A
N/A
100
10
16700
Sb
77.869
N/A
N/A
100
1
7.79
Se
183.454
N/A
N/A
100
1
18.3
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:16 AM
25
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-27 BH
TLI Sample ID:
182-58-2 BH
Date Received:
September 09. 1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analyte
Cove.
(uq/L)
rri
Total Vol
mL
Used
• mL .
Final Vol
D8utfc>n
Factor
Total uq
Result
As
48.146
820
720
100
1
5.48
Be
0.009
820
720
100
1
< 0.114
Cd
236.846
820
720
100
1
27.0
Co
11.548
820
720
100
1
1.32
Cr
307.456
820
720
100
1
35.0
Mn
7231.152
820
720
100
1
824
Ni
96.442
820
720
100
1
11.0
Pb
41239.508
820
720
100
1
4700
Sb
2.464
820
720
100
1
< 0.456
Se
376.042
820
720
100
1
42.8
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 14-Oct-97 at 01:57 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ED:
YCP-93,184,31.32 FH
TLI Sample ID:
182-30-6FGAB FH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analvte
K..., Cone.
(ml)
TctafVoi.
¦Oik->$*->¦¦¦¦ -::-
Used
mL
Final Vol.
OcUtiOR
Factor
: Totaf uq
Result
As
167.166
N/A
N/A
100
1
16.7
Be
-6.455
N/A
N/A
100
1
< 0.100
Cd
631.707
N/A
N/A
100
1
63.2
Co
93.200
N/A
N/A
100
2
18.6
Cr
2067.044
N/A
N/A
100
1
207
Mn
5238.502
N/A
N/A
100
10
5240
Ni
41'.619
N/A
N/A
100
1
41.2
Pb
16026.856
N/A
N/A
100
10
16000
Sb
69.565
N/A
N/A
100
1
6.96
Se
238.247
N/A
N/A
100
1
23.8
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
27
-------
Client: Eastern Research Group
Protect Number: 43159A
Sample Report
Client Sample ID:
YCP-33 BH
TLI Sample ID:
182-58-3 BH
Date Received:
September 09. 1997
Date Prepared:
September 18-24,1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone.
(uq/L>
mt
Total Vol.
mL
Used
mL
Final Vol.
Dilution
Factor
Totaf ug
Rest* ft
As
47.918
900
800
100
1
5.39
Be
0.043
900
800
100
1
< 0.113
Cd
194.676
900
800
100
1
21.9
Co
19,366
900
800
100
1
2.18
Cr
349.710
900
800
100
1
39.3
Mri
7792.857
900
800
100
1
877
Ni
117.651
900
800
100
1
13.2
Pb
42771.484
900
800
100
1
4810
Sb
2.149
900
800
100
1
< 0.450
Se
474.568
900
800
100
1
53.4
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-39.37,38 FH
TLI Sample ID:
182-30-7CAB FH
Date Received:
Seotember 09.1997
Date Prepared:
September 18-24,1997
Date Analvzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone.
mi)
. rht": ""¦¦'¦¦¦
TctafVol.
rrt' p-:
Final Vol.
D<son
Result
As
10.584
N/A
N/A
100
1
1.06
Be
0.159
N/A
N/A
100
1
< 0.100
Cd
-7.411
N/A
N/A
100
1
< 0.100
Co
2.100
N/A
N/A
100
1
0.210
Cr
125.615
N/A
N/A
100
1
12.6
Mn
211.206
N/A
N/A
100
1
21.1
Ni
89.245
N/A
N/A
100
1
8.92
Pb
170.306
N/A
N/A
100
1
17.0
Sb
70.267
N/A
N/A
100
1
7.03
Se
63.839
N/A
N/A
100
1
6.38
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
29
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-40.38 BH
TLI Sample ID:
182-30-7DB BH
Date Received:
September 09, 1997
Date Prepared:
September 18-24,1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Analyte
Cone. .
fool*
ni.
Total Vol.
mL
Used
mL
Final Vol.
Dilution
Factor
Total u<3
Result
As
-5.030
300
300
100
1
< 0.500
Be
0.084
300
300
100
1
< 0.100
Cd
1.189
300
300
100
1
0.119
Co
-0.897
300
300
100
1
< 0.100
Cr
10.982
300
300
100
1
1.10
Mn
745.005
300
300
100
1
74.5
Ni
4.392
300
300
100
1
0.439
Pb
89.827
300
300
100
1
8.98
Sb
1.230
300
300
100
1
< 0.400
Se
1.500
300
300
100
1
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-45.46.57FH
TLI Samole ID:
182-30-8 AB. 1 OA FH
Date Received:
September 09.1997
Date Prepared:
Seotember 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Aralyte
immm?
mL
Total Vol.
¦ mL
liliiilii"
Final Vd.
DSution
Factor
As
9.535
N/A
N/A
100
1
0.953
Be
0.100
N/A
N/A
100
1
< 0.100
Cd
-13.902
N/A
N/A
100
1
< 0.100
Co
3.300
N/A
N/A
100
1
0.330
Cr
131.468
N/A
N/A
100
1
13.1
Mn
56.285
N/A
N/A
100
1
5.63
Ni
84.906
N/A
N/A
100
1
8.49
Pb
-10.335
N/A
N/A
100
1
< 0.200
Sb
76.304
N/A
N/A
100
1
7.63
Se
67.563
N/A
N/A
100
1
6.76
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-47.45 BH
TLI Sample ID:
182-30-8CA BH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Anatvte
Cone.
(uq/U
mi
Total Vol.
mL
Used
mL
Final Vol.
D8ufion
Factor
Total us?
Result
As
-5.746
300
300
100
1
< 0.500
8©
0.070
300
300
100
1
< 0.100
Cd
-0.270
300
300
100
1
< 0.100
Co
-1.808
300
300
100
1
< 0.100
Cr
13.905
300
300
100
1
1.39
Mn
27.042
300
300
100
1
2.70
Ni
1.452
300
300
100
1
< 0.300
Pb
10.126
300
300
100
1
1.01
Sb
2.187
300
300
100
1
< 0.400
Se
-1.647
300
300
100
1
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 10:16 AM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Samole ID:
YCP-52.50.51 FH
TLI Samnle ID:
182-30-9CAB FH
Date Received:
September 09,1997
Date Prepared:
Sentember 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Artalvte
Cone.
{uq/U
Total Vol.
•• ni.
Used
mL
Final Vol.
DSution
Factor
Total uq
Result
As
9.968
N/A
N/A
100
1
0.997
Be
0.095
N/A
N/A
100
1
< 0.100
Cd
-0.082
N/A
N/A
100
1
< 0.100
Co
2.900
N/A
N/A
100
1
0.290
Cr
94.281
N/A
N/A
100
1
9.43
Mn
182.502
N/A
N/A
100
1
18.3
Ni
70.143
N/A
N/A
100
1
7.01
Pb
256.905
N/A
N/A
100
1
25.7
Sb
45.045
N/A
N/A
100
1
4.50
Se
40.307
N/A
N/A
100
1
4.03
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 01:58 PM
-------
Client: Eastern Research Group
Project Number: 431S9A
Sample Report
Client Sample ID:
YCP-53.51 BH
TLI Samole ID:
182-30-9DB BH
Date Received:
September 09.1997
Date Preoared:
Seotember 18-24,1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
AnaMe
Cone.
(uo/U
mL
Total Vol.
mL
Final Vol.
DSutlon
Factor
Total uq
As
-4.036
300
300
100
1
< 0.500
Be
0.069
300
300
100
1
< 0.100
Cd
3.323
300
300
100
1
0.332
Co
i
P
300
300
100
1
< 0.100
Cr
11.366
300
300
100
1
1.14
Mn
2856.354
300
300
100
1
286
Ni
6.990
300
300
100
1
0.699
Pb
1299.855
300
300
100
1
130
Sb
0.707
300
300
100
1
< 0.400
Se
5.248
300
300
100
1
0.525
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 01:58 PM
34
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-96.94.95 FH
TLI Samnle ID:
182-30-11CABFH
Date Received:
Sentemher 09. 1997
Dale Prepared:
SeDtember 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Printed: 07-Oct-97 at 01:58 PM
Analvte:
Cona
facyU
mL
Total Vol.
Used
Final Vol.
Dfortton
Factor
As
11.578
N/A
N/A
100
1
1.16
Be
0.128
N/A
N/A
100
1
< 0.100
Cd
-10.877
N/A
N/A
100
1
< 0.100
Co
11.300
N/A
N/A
100
1
1.13
Cr
138.486
N/A
N/A
100
1
13.8
Mn
120.736
N/A
N/A
100
1
12.1
Ni
103.955
N/A
N/A
100
1
10.4
Pb
66.160
N/A
N/A
100
1
6.62
Sb
82.037
N/A
N/A
100
1
8.20
Se
73.608
N/A
N/A
100
1
7.36
Triangle Laboratories, Inc.
801 Capitola Drive ~ Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
35
-------
Client: Eastern Research Group
Project Number: 431S9A
Sample Report
Client Sample ED:
YCP-97 BH
TLI Samole ID:
182-30-1 ID BH
Date Received:
Seotember 09.1997
Date Prepared:
Seotember 18-24,1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Anah/te
Cone.
«
mL
Tctal Vol.
Used
Final Vd.
As
-6.007
490
390
100
1
< 0.628
Be
0.064
490
390
100
1
< 0.126
Cd
0.570
490
390
100
1
< 0.126
Co
-1.286
490
390
100
1
< 0.126
Cr
12.078
490
390
100
1
1.52
Mri
106.967
490
390
100
1
13.4
Ni
7.792
490
390
100
1
0.979
Pb
50.396
490
390
100
1
6.33
Sb
-0.418
490
390
100
1
< 0.503
Se
-0.916
490
390
100
1
< 0.377
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 01:58 PM
-------
Client: Eastern Research Group
Protect Number: 43159A
Sample Report
Client Samole ID:
YCP-103.101.102 FH
TLI Samole ID:
182-30-12CAB FH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analvte
Tctaf Vol.
Used
_r
mL
Final Vol.
D8utk>n
j:il Mil
; Totafug
Result
As
11.162
N/A
N/A
100
1
1.12
Be
0.140
N/A
N/A
100
1
< 0.100
Cd
-8.110
N/A
N/A
100
1
< 0.100
Co
2.700
N/A
N/A
100
1
0.270
Cr
147.044
N/A
N/A
100
1
14.7
Mn
128.194
N/A
N/A
100
1
12.8
Ni
94.195
N/A
N/A
100
1
9.42
Pb
89.755
N/A
N/A
100
1
8.98
Sb
77.389
N/A
N/A
100
1
7.74
Se
69.850
N/A
N/A
100
1
6.98
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 01:58 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-104 BH
TLI SamDle ID:
182-30-12D BH
Date Received:
September 09.1997
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analvte
Cone,
(u oL)
mL
Total Vol
mL
Used
fnL
Final Vol.
D8ufc>n
Factor
Total uq
Result
As
-5.585
680
580
100
1
< 0.586
Be
0.036
680
580
100
1
< 0.117
Cd
1.788
680
580
100
1
0.210
Co
-0.613
680
580
100
1
< 0.117
Cr
59.943
680
580
100
1
7.03
Mn
2210.000
680
580
100
1
259
Ni
69.527
680
580
100
1
8.15
Pb
39.559
680
580
100
1
4.64
Sb
2.951
680
580
100
1
< 0.469
Se
-0.656
680
580
100
1
< 0.352
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 01:58 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-110.108.109 FH
TLI Samole ID:
182-30-13CAB FH
Date Received:
September 09.1997
Date Prepared:
Seotember 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
AnaMe
•••
iifll: "-M -.fnU xfa
-
Final Vol.
D&itior*
Factor
Result
As
10281
N/A
N/A
100
1
1.03
Be
0.097
N/A
N/A
100
1
< 0.100
Cd
-2.334
N/A
N/A
100
1
< 0.100
Co
2.400
N/A
N/A
100
1
0.240
Cr
128.654
N/A
N/A
100
1
12.9
Mn
106.480
N/A
N/A
100
1
10.6
Ni
84.906
N/A
N/A
100
1
8.49
Pb
212.334
N/A
N/A
100
1
21.2
Sb
68.238
N/A
N/A
100
1
6.82
Se
63.190
N/A
N/A
100
1
6.32
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 01:58 PM
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-111 BH
TT.I Sanwle ID:
182-30-13D BH
Date Received:
September 09.1997
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Cone.
mL
Final Vol.
Dilution
Factor
Result ^
As
-2.486
630
530
100
1
< 0.594
Be
0.051
630
530
100
1
< 0.119
Cd
1.810
630
530
100
1
0.215
Co
0.454
630
530
100
1
< 0.119
Cr
85.824
630
530
100
1
10.2
Mn
961.811
630
530
100
1
114
Ni
106.132
630
530
100
1
12.6
Pb
40.032
630
530
100
1
4.76
Sb
-0.759
630
530
100
1
< 0.475
Se
0.320
630
530
100
1
< 0.357
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 01:58 PM
40
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-161,159.160 FH
TLI Samole ID:
182-30- 14CAB FH
Date Received:
Seotember 09.1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
¦v.-;;..;. :
'•V>--Oond
iiiiiB
¦ --I
Final Vol.
U&rcon.
Factor
Total ug
As
10.285
N/A
N/A
100
1
1.03
Be
0.126
N/A
N/A
100
1
< 0.100
Cd
-12.339
N/A
N/A
100
1
< 0.100
Co
2.200
N/A
N/A
100
1
0.220
Cr
143.198
N/A
N/A
100
1
14.3
Mn
34.033
N/A
N/A
100
1
3.40
Ni
98.800
N/A
N/A
100
1
9.88
Pb
-14.557
N/A
N/A
100
1
< 0.200
Sb
85.380
N/A
N/A
100
1
8.54
Se
77.119
N/A
N/A
100
1
7.71
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
07-Oct-97 at 01:58 PM
41
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ED:
YCP-160.161 BH
TLI Sample ID:
182-30-14BCBH
Date Received:
September 09.1997
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06. 1997
Matrix:
Air
Analyte
Cone.
t*L
Iota} Vol.
mL
Used
rnL
Final Vol
Dilution
Factor
Total u<3
Result
As
-2.809
150
150
100
1
< 0.500
Be
0.084
150
150
100
1
< 0.100
Cd
0.146
150
150
100
1
< 0.100
Co
-0.670
150
150
100
1
< 0.100
Cr
4.712
150
150
100
1
0.471
Mn
15.171
150
150
100
1
1.52
Ni
0.449
150
150
100
1
< 0.300
Pb
11.974
150
150
100
1
1.20
Sb
-0.604
150
150
100
1
< 0.400
Se
-1.485
150
150
100
1
< 0.300
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713 Printed: 07-Oct-97 at 01:58 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
42
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-170 DI H20
TLI Samole ID:
182-30-15B
Date Received:
Sentember 09.1997
Date Prepared:
Seotember 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
AnaMe
Cone.
(uq/L>
mL
Total Vol.
mL "
Used
rrt
Final Vol.
Dilution
Factor
TotaJuq
Result
As
3,755
397
397
100
1
< 0.500
Be
0.074
397
397
100
1
< 0.100
Cd
-0.675
397
397
100
1
< 0.100
Co
-2.167
397
397
100
1
< 0.100
Cr
8.115
397
397
100
1
0.812
Mn
5.123
397
397
100
1
0.512
Ni
3.871
397
397
100
1
0.387
Pb
1.675
397
397
100
1
< 0.200
Sb
3.960
397
397
100
1
< 0.400
Se
3.009
397
397
100
1
0.301
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 15-Oct-97 at 08:26 AM
43
-------
Client: Eastern Research Group
Project Number: 43159A
Sample Report
Client Sample ID:
YCP-171 DIH20
TLI Sample ID:
182-30-15C
Date Received:
September 09. 1997
Date Prepared:
September 18-24.1997
Date Analvzed:
October 03-06.1997
Matrix:
Air
Artalyte
Cone.
'{uoO
rri_
Iota) Vol.
ml_
Usecf
ml
Final Vd.
D8utfc>n
Factor
Total ug
Result
As
5.790
367
367
100
1
0.579
Be
0.025
367
367
100
1
< 0.100
Cd
-1.526
367
367
100
1
< 0.100
Co
-5.312
367
367
100
1
< 0.100
Cr
16.217
367
367
100
1
1.62
Mn
5.310
367
367
100
1
0.531
Ni
7.916
367
367
100
1
0.792
Pb
10.822
367
367
100
1
1.08
Sb
5.370
367
367
100
1
0.537
Se
6.344
367
367
100
1
0.634
•
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
15-Oct-97 at 08:26 AM
44
-------
Client: Eastern Research Group
Project Number: 431S9A
OA: Serial
Dilution
Client Samole ED:
YCP-88.01.02FH
YCP-88.01.02 FH L
TLI Sample ID:
182-30-1GAB FH
182-30-1 GAB FH I ,
Date Prenared:
September 18-24.1997
September 18-24. 1997
Date Analyzed:
October 03-06,1997
October 03-06,1997
Matrix:
Air
Air
Native Sample
Serial Dilution
iiiiii
Artah/to
'ArKUVvC 1
Total uq
:ug/L
Gonc:
: Total ug .
Resuft
IPiOClfeiit
As
1.51
15.051
< 2.50
3.769
-------
Client: Eastern Research Group
Project Number: 43159A
QA: Serial Dilution
Client Sample ID:
YCP-03 BH
YCP-03 BHI.
TLI Samnle ID:
182-30-1C BH
182-30-10 BHL
Date Preoared:
Sentember 18-24, 1997
September 18-24.1997
Date Analvzed:
October 03-06. 1997
October 03-06.1997
Matrix:
Air
Air
Native Sample
Serial Dilution
Total ug
ugiL
Total ug
ugrt-
RPD
Anah/te
Resuit
Result
Conc.
As
1.60
13.810
< 2.90
3.270
-------
Client: Eastern Research Group
Project Number: 431S9A
QA: Duplicate
Client Sample ID:
YrP-X8.07.08 FH
YCP-88.07.08 FH DA
TLI Sample ID:
182-30-2GAB FH
182-30-2GAB FH DA
Date Prepared:
September 18-24.1997
September 18-24.1997
Date Analyzed:
October 03-06.1997
October 03-06. 1997
Matrix:
Air
Air
Sample
Duplicate
Analyte
Totalug
Result
Total uq
Resu#
mmmmt
Cone.
F
Bfi
As
1.43
14 342
1 59
15858
-------
Client: Eastern Research Group
Project Number: 43159A
OA: Duplicate
Client Samr>le ID:
YCP-09 BH
YCP-09BHDA
TLI Sample ID:
182-30-2CBH
182-30-2C BHDA
Date Prepared:
September 18-24. 1997
September 18-24.1997
Date Analyzed:
October 03-06. 1997
October 03-06.1997
Matrix:
Air
Air
Sample
Duplicate
Analvte
ug/l
. Totai ug
: Result
uq/L
RPD
As
1.44
12.694
147
12.983
-------
Client: Eastern Research Group
Pro ject Number: 43159A
QA: Matrix Spikes (Post-Digestion)
Client Samole ID:
YCP-88,01,02 FH PDS
TLI Sample ID:
182-30-1GAB FH PDS
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Post-Diqestion Spike
Post-Diqestion Spike Duplicate
Analvte
Recovered
Amount fucVU
Spike :
Amount fua/U
¦ ¦ %
Recovery
. Recovered
AmounHua/L)
Amount
ilfpff!
Recovery
As
60.32
50
91%
—
Be
46.22
50
92°/c
—
Cd
66.29
50
94%
Co
28.30
25
88%
...
Cr
153.99
50
101%
Mn
220.58
50
95%
Ni
115.37
50
94%
Pb
1230.97
50
Soike Low
_
Sb
92.78
50
96%
_
Se
89.28
50
89%
_
—
—
_
—
_
—
—
—
—.
—
—
—.
—
—
—
—
Triangle Laboratories, Inc.
801 Capitol a Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:23 AM
49
-------
Client: Eastern Research Group
Project Number: 43159A
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
YCP-03 BH PDS
TLI Samole ID:
182-30-1C BH PDS
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06.1997
Matrix:
Air
Post-Diqestion Spike
Post-Diqestion Spike Duplicate
Recovered
Spike
0/
/O.
Recovered
Spike
O'
SO
RPD
AnaJvte
Amount (ocvU
Amount {u#L)
Recovery
Amount (ua/U
Amount (uq/L)
Recovery
As
63.27
50
99%
—
Be
48.63
50
97%
—
Cd
49.17
50
98%
—
Co
53.78
50
98%
—
Cr
158.27
50
95%
—
Mn
285.04
50
94%
—
Ni
67.61
50
95%
—
Pb
86.30
50
95%
—
Sb
49.23
50
98%
—
Se
991.56
50
Spike Low
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitol a Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 07-Oct-97 at 10:23 AM
-------
Client: Eastern Research Group
Protect Number: 43X59A
QA: ICP Method Blank
TLI Sample ID:
43159A MB
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06,1997
Matrix:
N/A
Method Blank
¦; ¦ ,
Anafvte
Recovered,
Amount {ua/L)
nptor*Trin
limit (UOto ::
iliiiiilll-:
Fail
As
0.94
5
Pass
Be
0.07
1
Pass
Cd
-0.11
1
Pass
Co
-0.19
1
Pass
Cr
0.42
2
Pass
Mn
0.59
2
Pass
Ni
6.55
3
Fail
Pb
1.45
2
Pass
Sb
0.46
4
Pass
Se
-0.19
3
Pass
—
—
—
—
—
.—.
—
_
—
—
—
—
—
.—.
—
—
_
—
—
—
—
_
—
—
—
—.
—
—
—
_
—
_
—
—.
—
—
—
—
—
Triangle Laboratories, Inc.
801 CapitolaDrive* Durham, NC 2771 Printed: 14-Oct-97 at 01:57PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
51
-------
Client: Eastern Research Group
Project Number: 43159A
QA: GFAA Method Blank
TLI Samnle ID:
43159A MB
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06, 1997
Matrix:
N/A
Method Blank
Recovered
Detection
Pass or
AnaMe
Amount fuq/L)
limit fua/U
Fail
Co
0.40
1.5
Pass
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771 Printed: 15-Oct-97 at 08:26 AM
Tele: (919) 544-5729 * Fax: (919) 544-5491
-------
Client: Eastern Research Group
Project Number: 43159A
QA: ICP Lab Control Spikes
TLI Sample ID:
43159ALCS
Date Prepared:
September 18-24.1997
Date Analyzed:
October 03-06.1997
Matrix:
N/A
Lab Control Spike
Lab Control Spike Duplicate
RPD
Anili rtn
Anaivie
Recovered
AmourWuaO
Amour;? {uq/L>
Recovery
Recovered
Spike
Amount fuaM
liiiiil
; Recovery
As
51.03
50
102"A
¦
Be
47.36
50
95 °A
Cd
49.24
50
98"A
—
Co
49.32
50
m°/<
Cr
49.55
50
99"/,
—
Mn
49.56
50
9 9°A
Ni
56.73
50
113°A
Pb
50.52
50
101°y{
—
Sb
48.63
50
97%
Se
48.82
50
98%
—
...
—
—
...
—
—
—
...
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 14-Oct-97 at 01:57 PM
-------
Client: Eastern Research Group
Project Number: 43159A
QA: GFAA Lab Control Spikes
TLI Sample ID:
43159A LCS
Date Prepared:
September 18-24,1997
Date Analyzed:
October 03-06.1997
Matrix:
N/A
Lab Control Spike
Lab Control Spike Duplicate
Anahle
Recovered
AmourS (udl)
Spike .
Amount fuo'U
!*
Recover/
Recovered
Amount (uo/L)
Spike
AmotflTt (uq/Li
llliMlI
Recovery
F1PD
Co
49.70
50
99°/;
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
14-Oct-97
at
02:25 PM
54
-------
ient: Eastern Research Group
oiect Number, 4315PA
ample Report Page 1 of i
e Received:
September 09.1997
e Preoared:
Sentember 18-29.1997
e Analyzed:
SeDt. 26 & 30 & Oct 1 & 9.1997
TA FILE:
AB810. AB811. AB812 & AB817
xix:
Air
ANALYTE: Ha
upl RDL. 0,2
Analysis Method 29
Instrument: P E Zeeman 5100
Spike Cone. (tioU 5
CVAA ANALYTE SUMMARY REPORT
ntSamcielD
lirSAMPID - •
wmm
1Y
mmtm
FV
ml
AJK^Gt
Da. |
RESULT
RlSuLT
I
' j> > r-.r— rk
iSK«£*]S
;P-88,01,02 FH
182-30-1GAB
0.053
n/a
100
5
1
<
0.400
lP-88,01,02 FH D
182-30-1GABD
0.040
n/a
100
5
1
<
0.400
<
0.400
—
—
:P-03BH
182-30-1C
0.995
720
N/A
5
1
14.3
—
—
—
:P-03 BH D
182-30-1 CD
1.003
720
N/A
5
1
14.4
144
—
—
:P-04HNO3
182-30-1D
0.019
90
N/A
5
1
<
0.360
—
-
P-04 HN03 D
182-30-1DD
0.008
90
N/A
5
1
<
0.360
<
0.360
—
—
;p-05 KMnCH
182-30-1E
2224
238
N/A
5
1
10.6
—
—
-
P-05 KMn04 D
182-30-1E D
2.267
238
N/A
5
1
10.8
10.7
—
—
P-06 HCI
182-30-1F
0.048
295
N/A
5
1
<
1.18
—
—
—
P-06 HCI D
182-30-1F D
0.043
295
N/A
5
1
«
1.18
<
1.18
—
—
P-89,07,08 FH
182-30-2GAB
0.013
N/A
100
5
1
<
0.400
—
—
—
P-89,07.08 FH D
182-30-2GAB D
0.016
n/a
100
5
1
<
0.400
<
0.400
¦—
—
P-09 BH
182-30-2C
0.941
840
N/A
5
1
15.8
—
—
P-09 BHD
182-30-2CD
0.845
840
N/A
5
1
14.2
15.0
—
—
P-10HNO3
182-30-2D
0.024
76
N/A
5
1
<
0.304
_
—
—
P-10HNO3D
182-30-2DD
0.011
76
N/A
5
1
<
0.304
<
0.304
—
—
3-11 KMn04
182-30-2E
1.987
345
N/A
5
1
13.7
—
—
—
=-11 KMn04 D
182-30-2ED
1.928
345
N/A
5
1
13.3
13.5
—
—
'-12 HCI
182-30-2F
0.032
300
N/A
5
1
<
1.20
—
—
3-12 HCI D
182-30-2FD
0.019
300
N/A
5
1
<
1.20
<
1.20
—
•—
3-90,13,14 FH
182-30-3GAB
0.024
N/A
100
5
1
<
0.400
_
_
—
3-90,13,14 FH D
182-30-3GAB D
0.019
N/A
100
5
1
<
0.400
<
0.400
—
'-15 BH
182-30-3C
1.021
800
N^A
5
1
16.3
—
_
—
'-15 BHD
182-30-3CD
1.024
800
N/A
5
1
16.4
16.4
—
—
'-16HN03 :
182-30-3D
0.048
50
N/A
5
1
<
0.200
—
—
—
>-16HN03D
182-30-3D D
0.045
50
N/A
5
1
<
0200
<
0.200
—
—
»-17KMn04
182-30-3E
1.591
345
N/A
5
1
11.0
—
—
•-17KMn04D
182-30-3E D
1.524
345
N/A
5
1
10.5
10.7
—
—
'-18 HCI
182-30-3F
0.032
200
N/A
5
1
<
0.800
—
—
—
'-18 HCI D
182-30-3FD
0.027
200
N/A
5
1
<
0.800
<
0.800
*—
55
-------
ent: Eastern Research Group
liect Number: 43159.4
ample Report Page 2 of 7
i Received:
SeDtember09. 1997
i Prepared:
September 18-29. 1997
; Analvzed:
Sent. 26 & 30 & Oct 1 & 9. 1997
FA FILE:
AB810, AB811. AB812 & AB817
rix:
Air
ANALYTE: Ha
ucfl- RDL 0.2
Analysis Method: 29
Instrument: P E Zeeman 5100
Spike Conc. (ua/lJ 5
CVAA ANALYTE SUMMARY REPORT
¦ ma
CONG
: mi
TV
P-B
1PP
mi
, OIL
FAcrrop
Total uq
RESULT
Avg.;;
RESULT
RPD
IP-91,19,20 FH
182-30-4FAB
0.663
N/A
100
5
1
1.33
••
_
JP-91,19,20 FH D
182-3Q-4FABD
0.660
N/A
100
5
1
1.32
1.32
—
JP-21 BH
182-58-1
0.222
750
N/A
5
1
3.33
..
-
;P-21 BH D
182-58-1 D
0.211
750
N/A
5
1
3.17
3.25
—
—
;P-22 HN03
182-3Q-4C
0.021
70
N/A
5
1
< 0.280
—
—
;P-22 HN03 D
182-30-4CD
0.024
70
N/A
5
1
< 0,280
< 0.280
—
—
;P-23 KMn04
182-30-4D
1.754
305
N/A
5
1
10.7
—
_
;P-23KMn04D
182-30-4D D
1.644
305
N/A
5
1
10.0
10.4
—
—
;P-24 HCI
182-30-4E
0.043
275
N/A
5
1
< 1.10
—
-
-
;P-24 HCI D
182-30-4E D
0.032
275
N/A
5
1
< 1.10
< 1.10
—
—
JP-92,183,25,26 FH
182-30-5FGAB
0.211
N/A
100
5
1
0.422
—
—
—
;P-92,183,25,26 FH D
182-30-5FGAB D
0.211
N/A
100
5
1
0.422
0.422
—
—
IP-27 BH
182-58-2
0.257
820
N/A
5
1
4,21
—
—
-
:P-27 BH D
182-58-2 D
0.235
820
N/A
5
1
3.85
4.03
—
—
IP-28 HN03
182-30-5C
0.027
98
N/A
5
1
< 0.392
—
-
-
;P-28 HN03 D
182-30-5C D
0.027
98
N/A
5
1
< 0.392
< 0.392
—
—
;P-29 KMn04
182-30-5D
1.382
400
N/A
5
1
11.1
—
—
-
;P-29 KMn04 D
182-30-5D D
1.257
400
N/A
5
1
10.1
10.6
—
—
:P-30 HCI
182-30-5E
0.021
300
N/A
5
1
< 1.20
—
_
_
;P-30 HCI D
182-30-5E D
0.029
300
N/A
5
1
< 1.20
< 1.20
—
—
5P-93,184,31,32 FH
182-30-6FGAB
0.193
N/A
100
5
1
< 0,400
—
—
JP-93,184,31,32 FH D
182-30-6FGA3D
0.184
N/A
100
5
1
< 0.400
< 0.400
—
IP-33 BH
182-58-3
0.471
900
N/A
5
1
8.48
—
—
—
;P-33 BH D
182-58-3 D
0.436
900
N/A
5
1
7.85
8.16
—
—
:P-34 HN03
182-30-6C
0.008
126
N/A
5
1
< 0.504
—
-
-
:P-34HN03D
182-30-6C D
0.013
126
N/A
5
1
< 0.504
< 0.504
—
—
P-35 KMn04
182-30-6D
1.299
415
N/A
5
1
10.8
~
—
—
JP-35 KMn04 D
182-30-6D D
1.238
415
N/A
5
1
10.3
10.5
—
—
;P-36 HCI
182-30-6E
0.059
150
N/A
5
1
< 0.600
—
—
—
!P-36 HCI D
182-30-6E D
0.056
150
N/A
5
1
< 0.600
< 0.600
—
56
-------
ent: Eastern Research Group
>iect Number 43159A
imple Report Page 3 of 7
Received:
September 09.1997
Prepared:
September 18-29.1997
Analyzed:
Sept. 26 & 30 & Oct 1 & 9,1997
rA FILE:
AB810. AB811. AB812 & AB817
rix:
Air
ANALYTE: Ha
uytRDL- 0.2
Analysis Method: 29
Instrument: P E Zeeman 5100
Spike Cone. (uq/L)
CVAA ANALYTE SUMMARY REPORT
it Sample ID
TLfS/MPlD
w$m
£• Trt
-TV
ml
FV
ml J
AliqtraiS
OR.-
FACTOF
Total ug
RESULT
Avg.
:RESULT
FIPO
%REC
P-39,37,38 FH
P-39,37,38 FH D
182-30-7CAB
182-30-7CAB D
0.005
-0.003
N/A
N/A
100
100
5
5
1
1
<
<
0.400
0.400
<
0.400
-
-
P-404§£H~~
P-40,38 BH D *
182-30-7DB
182-30-7DB D
0.018
0.021
295
295
N/A
N/A
5
5
1
1
<
<
1.18
1.18
<
1.18
-
-
P-41 HN03
P-41 HN03 D
182-30-7E
182-30-7E D
0.193
0.166
50
50
N/A
N/A
5
5
1
1
<
<
0.200
0.200
<
0.200
-
-
P-42 KMn04
P-42 KMn04 D
182-30-7F
182-30-7F D
0.005
0.013
415
415
N/A
N/A
5
5
1
1
<
<
1.66
1.66
<
1.66
-
-
^ /•*— ¦ _ ^
Pt42,43 HCl ~ .
P-42,43 HCl D
182-30-7FG
182-30-7FG D
-0.005
-0.003
142
142
N/A
N/A
5
5
1
1
<
<
0.568
0.568
<
0.568
-
-
P-45,46.57 FH
P-45,46.57 FH D
182-30-8AB.10A
182-30-8AB.10AD
0.008
0.000
N/A
N/A
100
100
5
5
1
1
<
<
0.400
0.400
<
0.400
-
_
P-47,45 BH
P-47,45 BH D -
182-30-8CA
182-30-8CAD
0.021
0.000
300
300
N/A
N/A
5
5
1
1
<
<
1.20
1.20
<
1.20
-
-
P-45HN03 A"
P-45HN03D
182-30-8A
182-30-8A D
0.019
0.005
100
100
N/A
N/A
5
5
1
1
<
<
0.400
0.400
<
0.400
-
-
P-48,171 KMn04
P-48,171 KMn04D
182-30-8D.15C
182-30-80,15C D
0.003
0.008
400
400
N/A
N/A
5
5
1
1
<
<
1.60
1.60
<
1.60
_
-
P-48,49473 HCl
P-48,49,171 HCID
182-30-8DE.15C
182-30-8DE.15C D
-0.005
-0.008
268
268
N/A
N/A
5
5
1
1
<
<
1.07
1.07
<
1.07
-
—
P-52,50,51 FH
P-52,50,51 FH D
182-30-9CAB
182-30-9CAB D
0.011
0.005
N/A
N/A
100
100
5
5
1
<
<
0.400
0.400
<
0.400
—
—
P-53,51 BH (' ...
P-53,51 BH D \
182-30-9DB
182-30-9DB D
0.112
0.104
300
300
N/A
N/A
5
5
1
<
<
1.20
1.20
<
1.20
-
-
/,
=>-54 HN03
P-54HN03D ¦¦¦'.
*'
P-55,170 KMn04 '
=-55,170 KMn04 D
182-30-9E
182-30-9ED
0.091
0.070
64
64
N/A
N/A
5
5
1
1
<
<
0.256
0.256
<
0.256
_
-
182-30-9F.15B
182-30-9F.15B D
0.029
0.008
400
400
m
N/A
5
5
1
1
<
<
1.60
1.60
<
1.60
-
_
3-55,56,170 HCl
=-55,56,170 HCID
182-30-9FG,15B
182-30-9FG,15B D
0.003
-0.003
188
188
N/A
N/A
5
5
1
1
<
<
0.752
0.752
<
0.752
—
-
57
-------
ent: Eastern Research Group
)iect Number: 43159A
ample Report Page 4 of 7
Received:
September 09. 1997
Prepared:
September 18-29. 1997
Analyzed:
Sept. 26 & 30 & Oct. 1 & 9. 1997
TA FILE:
AB810. AB811. AB812 & AB817
rix:
Au-
CVAA ANALYTE SUMMARY REPORT
ANAI.YTE: Ha
uqIRDL 02
Analysis Method: 29
Instrument: P E Zeeman 5100
Spike Cone. (ua/lJ 5
nt Sarrole ID
TUSAMPID
ug/L
CONG
.• mt
TV
mirim
pv
ml
AOouot
fcML
FACTOF
Total ug
RESULT
Avg.
RESULT
SPD
%REC
)P-96,94,95 FH
182-30-11 CAB
0.027
N/A
100
5
1
<
0.400
_
/P-96,94,95 FH D
182-30-11 CAB D
0.005
N/A
100
5
1
<
0.400
<
0.400
—
/P-97 BH
182-30-11D
0.051
490
N/A
5
1
<
1.96
-
-
-
/P-97 BH D
182-30-11DD
0.035
490
N/A
5
1
<
1.96
<
1.96
—
iP-98 HN03
182-30-11E
0.005
50
N/A
5
1
<
0.200
«
-
-
/P-98 HN03 D
182-30-11ED
0.011
50
N/A
5
1
<
0.200
<
0.200
—
—
:P-99 KMn04
182-30-11F
0.075
122
N/A
5
1
<
0.488
—
-
-
^P-99 KMn04 D
182-30-11F D
0.064
122
N/A
5
1
<
0.488
<
0.488
*"
IP-100 HCI
182-30-11G
0.008
102
N/A
5
1
<
0.408
-
-
-
;P-100 HCI D
182-30-11GD
0.019
102
N/A
5
1
<
0.408
<
0.408
—
—
IP-103.101.102FH
182-30-12CAB
0.008
N/A
100
5
1
<
0.400
—
-
-
JP-103,101,102FHD
182-30-12CAB D
0.013
N/A
100
5
1
<
0.400
<
0.400
—
~~
yP-104 BH
182-30-12D
0.040
680
N/A
5
1
<
272
--
-
-
:P-104BHD
182-30-12D D
0.043
680
N/A
5
1
<
272
<
2.72
—
—
:P-105HNO3 -vvV
182-30-12E
0.008
80
N/A
5
1
<
0.320
--
-
-
iP-105 HN03 D '
182-30-12ED
0.008
80
N/A
5
1
<
0.320
<
0.320
—
—
)P-106 KMn04
182-30-12F
0.064
305
N/A
5
1
<
1.22
-
-
-
JP-106 KMn04D
182-30-12FD
0.061
305
N/A
5
1
<
1.22
<
1.22
—
iP-107 HCI
182-30-12G
0.019
260
N/A
5
1
<
1.04
-
-
-
;p-107 HCI D
182-30-12GD
0.005
260
N/A
5
1
<
1.04
<
1.04
—
~
IP-110,108,109 FH
182-30-13CAB
0.003
N/A
100
5
1
<
0.400
—
-
-
IP-110,108,109 FHD
182-30-13CAB D
0.003
N/A
100
5
1
<
0.400
<
0.400
—
:P-111BH
182-30-13D
0.045
630
N/A
5
1
<
252
-
-
-
:P-111BHD
182-30-13D D
0.035
630
N/A
5
1
<
252
<
2.52
—
2P-112 HN03 ¦ •
182-30-13E
0.008
64
N/A
5
1
<
0.256
~
-
-
:P-112HN03D
182-30-13ED
0.005
64
N/A
5
1
<
0.256
<
0.256
—
DP-113 KMn04
182-30-13F
0.094
305
N/A
5
1
<
1.22
—
-
-
3P-113 KMn04 D
182-30-13FD
0.094
305
N/A
5
1
<
1.22
<
1.22
—
—
3P-114HCI
182-30-13G
0.019
200
N/A
5
1
<
0.800
—
-
-
3P-114HCID
182-30-13GD
0.003
200
N/A
5
1
<
0.800
<
0.800
"
-------
;nt:
iect Number;
Eastern Research Group
43159A
imple Report
Page 5 of 7
Received:
September 09. 1997
Prepared:
September 18-29,1997
Analyzed:
Sept. 26 & 30 & Oct 1 & 9.1997
"A FILE:
AB81Q, AB811. AB812 & AB817
ix:
Air
ANALYTE: Ha
ua/LRDL 0.2
Analysis Method:
29
Instrument: P EZeemari 5100
Spike Cone. fug/U
CVAA ANALYTE SUMMARY REPORT
:• ug&.:
ft*
ms
mi
OIL
Total ug
Avg.
st Sarooie ID
Tl JSAMPID::
CONG
TV
FV
Afauo?
FACTOF
RESULT
liiRiii®
iSi
%REC
P-165,159,160 m
182-30-14GAB
0.011
N/A
100
5
1
< 0.400
P-165,159,160 FH D
182-30-14GAB D
0.019
N/A
100
5
1
< 0.400
< 0.400
—
—
P-160,161 BH
182-30-14BC
0.000
150
N/A
5
1
< 0.600
—
_
_
=-160,161 BHD
182-30-14BCD
0.003
150
N/A
5
1
< 0.600
< 0.600
-
-
3-162 HN03
182-30-14D
0.060
40
N/A
5
1
< 0.160
—
3-162 HN03D
182-30-14DD
0.024
40
N/A
5
1
< 0.160
< 0.160
-
-
3-163 KMn04
182-30-14E
0.000
285
N/A
5
1
< 1.14
__
—
3-163 KMn04 D
182-30-14ED
0.000
285
N/A
5
1
< 1.14
< 1.14
-
-
3-163,164 HCl
182-30-14EF
-0.013
130
N/A
5
1
< 0.520
_
3-163,164 HC! D
182-30-14EFD
-0.013
130
N/A
5
1
< 0.520
< 0.520
-
-
3-170 DIH20 v-
182-30-15B
0.043
397
N/A
5
1
< 1.59
—
3-170 Dl H20 D v ,
182-30-15BD
0.024
397
N/A
5
1
< 1.59
< 1.59
-
-
3-171 DIH20
182-30-15C
0.035
367
N/A
5
1
< 1.47
—
3-171 Dl H20 D V.
182-30-15CD
0.057
367
N/A
5
1
< 1.47
< 1.47
—
—
3-88,01,02 FH MS :'X'
182-30-1 GAB MS
4.960
N/A
100
5
1
9.92
99%
3-88,01,02 FHMSD",
182-30-1 GAB MSD
4.588
N/A
100
5
1
9.18
9.55
7.79%
92%
3-06 HCl MS Ci - : '
182-30-1F MS
4.604
295
N/A
5
1
27.2
—
92%
3-06 HCl MSD'
182-30-1F MSD
4.559
295
N/A
5
1
26.9
27.0
0.982%
91%
3-21 BH MS 5i.-
182-58-1 MS
5.176
750
N/A
5
1
77.6
99%
3-21 BH MSD ;
182-58-1 MSD
4.920
750
N/A
5
1
73.8
75.7
5.07%
94%
3-23 KMn04 MS ">:¦
182-30-4D MS
6.294
305
N/A
5
1
38.4
92%
'-23 KMn04 MSI? >.
182-30-40 MSD
6.058
305
N/A
5
1
37.0
37.7
3.82%
87%
3-41 HN03MS
182-30-7EMS
4.726
50
N/A
5
1
4.73
mr,
95%
3-41 HN03 MSD r. -
182-30-7E MSD
4.779
50
N/A
5
1
4.78
4.75
1.12%
96%
3-52,50,51 FH MS ..
182-30-9CAB MS
5.034
N/A
100
5
1
10.1
B _
101%
3-52,50,51 FH MSD
182-30-9CAB MSD
5.176
N/A
100
5
1
10.4
10.2
2.78%
104%
>-99 KMn04 MS
182-30-11F MS
5.361
122
N/A
5
1
13.1
_
107%
3-99 KMnQ4 MSD
182-30-11F MSD
5.329
122
N/A
5
1
13.0
13.0
0.599%
107%
59
-------
ienl:
oiect Number;
Eastern Research Group
431S9A
ample Report
Page 6 of 7
:e Received:
SeDtember09. 1997
:e Prepared:
September 18-29.1997
:e Analyzed:
Sect. 26 & 30 & Oct 1 & 9.1997
.TA FILE:
AB810. AB811. AB812 & AB817
trix:
Air
ANALYTE: Ha
ucvL RDl: 0.2
Analysis Method:
29
Instalment: P E Zeeman 5100
Spike Cone. (ua/U
CVAA ANALYTE SUMMARY REPORT
;nr Sample iD
TUSAMPfD :
S u&t •
COHC
mi
liil
' TPt
PV
mi
Aliquot
DiL
PACTOP
Total uq
SESULT
Avg.
: RESULT
: RPD
%PEC
:P-114HCIMS V'
182-30-13G MS
5.139
200
N/A
5
1
20.6
103%
3P-114 HCIMSD
182-30-13G MSD
5.096
200
N/A
5
1
20.4
20.5
0.840%
102%
3P-40.38 BH MS
182-30-7DB MS
4.946
295
N/A
5
1
29.2
—
—
99%
:P-40,38BH MSD^..
1 •
82-30-7DB MSD
4.930
295
N/A
5
1
29.1
29.1
0.324%
99%
DP-88,01,02 FHMS S-'
Frue Spike MS
5
N/A
100
5
1
10.0
—
—
HP-88,01,02 FH MSD :"
Frue Spike MSD
5
N/A
100
5
1
10.0
..
"
:P-06 HCI MS -, - 0i.
Frue Spike MS
5
295
N/A
5
1
29.5
3P-06 HCI MSD '
Frue Spike MSD
5
295
N/A
5
1
29.5
-
_
-
;P-21 BH MS ^
["rue Spike MS
5
750
N/A
5
1
75.0
:p-21 BH MSD
true Spike MSD
5
750
N/A
5
1
75.0
-
"
:P-23KMn04MS
["rue Spike MS
5
305
N/A
5
1
30.5
__
_
—
:P-23 KMn04 MSD .
Frue Spike MSD
5
305
N/A
5
1
30.5
—
-
—
;P-41 HN03 MS S'V-:'
frue Spike MS
5
50
N/A
5
1
5.00
—
__
__
:p-41 HN03 MSD c _
frue Spike MSD
5
50
N/A
5
1
5.00
-
:P-52,50,51 FH MS ^
frue Spike MS
5
N/A
100
5
1
10.0
—
—
HP-52,50,51 FH MSD "
"rue Spite MSD
5
m
100
5
1
10.0
—
-
-
DP-21 BH MS
frue Spike MS
5
122
N/A
5
1
12.2
:p-21 BH MSD ^ '
"rue Spike MSD
5
122
N/A
5
1
12.2
—
—
"
DP-27BH MS
"rue Spike MS
5
200
N/A
5
1
20.0
—
__
DP-27 BH MSD
"rue Spike MSD
5
200
N/A
5
1
20.0
~
-
2P-40.38 BH MS MS
"rue Spike MS
5
295
N/A
5
1
29.5
—
3P-40.38 BH MS MSD
"rue Spike MSD
5
295
N/A
5
1
29.5
—
—
—
GO
-------
«t:
iect Number:
Eastern Research Group
431S9A
mple Report
Page 7 of 7
Received:
September 09. 1997
Prepared:
September 18-29.1997
Analyzed:
Sept. 26 & 30 & Oct. 1 & 9.1997
A FILE:
AB810. AB811. AB812 & AB817
ix:
Air
ANALYTE: Ho
uq/LRDL: 0.2
Analysis Method:
29
Instalment: P E Zeeman 5100
Spike Cone. fua/U 5
CVAA ANALYTE SUMMARY REPORT
11?
"I""''::':;..
TUSAMP!D:
' X&L
CONC
rr*.
TV
'¦m
¦¦ FV
m,
sAfiqtiat
•~5ir*
FACTOF
: Total ag
RESULT
¦ Avg.
¦¦ RESIAT
: '»prv:
g-lREC
icd Blank
43159AMB1
0.000
iod Blank D
43159AMB1 D
0.000
—
—
-
-
-
—
—
43159ALCS1
4.756
—
_
—.
—
—
—
95%
3
43159ALCS1 D
5.032
-
-
-
-
-
101%
od Blank
43159AMB2
0.005
—
_
_
...
;od Blank D
43159AMB2D
0.000
—
-
-
"
—
-
43159ALCS2
5.139
—
_
103%
3
43159ALCS2D
5.280
"
—
»
-
-
-
106%
od Blank
43159AMB3
0.014
—
—
—
—
—
—
..
iod Blank D
43159AMB3D
0.038
"
-
-
-
"
-
~
43159ALCS3
5.534
_
_
111%
3
43159A LCS3D
5.753
"
-
-
-
-
"
_
115%
od Blank
43159AMB4
0.003
__
—.
od Blank D
43159AMB4D
-0,005
-
-
»
~
-
_
-
"
43159ALCS4
4.365
—
—
_
—
87%
3
43159ALCS4D
4.319
-
_
»
-
»
86%
iod Blank
43159AMB5
0.010
„
—
.....
iod Blank D
43159AMB5D
0.005
"
-
-
—
_
_
--
43159ALCS5
5233
—
__
_
105%
3
43159ALCS5D
4.941
—
—
—
-
—
99%
igle Laboratories, Inc.
Dapitola Drive * Durham, North Carolina 27713
(919) 544-5729 * Fax (919) 544-5491
Printed:
13~Ocf~97
at
01:31 PM
61
-------
Eastern Research Group COC
Younqstown Sintering Plant
CHAIN OF CUSTODY
RELINQUISHED BY«
RELINQUISHED BY =
Gcu*p H
XlM--
DATE-
DATE-
R] ft- 97
RECEIVED BY
RECEIVED BY
DATE
ATE:
SAMPLE ID
/ a
FIELD ID
SAMPLE TYPE
PRESERVATIVE
COMMENTS
ANALYSIS
YCP-01
YCP-
81297
M29-
SBOUTLET-
APR-
1
METHOD 29, SBOUTLET, RUN 1
ACETONE PROBE RINSE
Beaker # 1
266.5
404 5
YCP-02
YCP-
81297
M29-
SBOUTLET-
HN-
1
METHOD 29. SBOUTLET, RUN 1
NITRIC ACID PROBE RINSE
267.5
411,5
YCP-03
YCP-
81297
M29-
SBOUTLET-
BH-
1
METHOD 29, SBOUTLET, RUN 1
HN03/H202 BACK HALF
391.3
1126.7
YCP-04
YCP-
81297
M29-
SBOUTLET-
BHM-
1
METHOD 29. SBOUTLET, RUN 1
0.1NHNO3 RINSE - Hg
269.4
360.0
YCP-05
YCP-
81297
M29-
SBOUTLET-
KMnO-
1
METHOD 29, SBOUTLET, RUN 1
KMn04 IMPINGE RS
268.5
531.2
YCP-06
YCP-
81297
M29-
SBOUTIET-
HCl-
1
METHOD 29, SBOUTLET. RUN 1
8N HCI RINSE • Hg
270.5
595.2
YCP-07
YCP-
81397
M29-
SBOUTLET-
APR-
2
METHOD 29, SBOUTLET, RUN 2
ACETONE PROBE RINSE
Boaker # 2
267.2
326.2
YCP-D8
YCP-
81397
M29-
SBOUTLET-
HN-
2
METHOD 29. SBOUTLET. RUN 2
NITRIC ACID PROBE RINSE
270.8
480.6
YCP-09
YCP-
81397
M29-
SDOUTLET-
BH-
2
METHOD 29, SBOUTLET, RUN 2
HN03/H202 BACK HALF
391 1
1246.0
YCP-10
YCP-
81397
M29-
SBOU7LET-
BHM-
2
METHOD 29, SBOUTLET, RUN 2
0 1N HN03 RINSE • Hg
270.7
346.0
YCP-11
YCP-
31397
M29-
SEiOUTLET-
KMnO-
2
METHOD 29, SBOUTLET. RUN 2
KMn04 IMPINGE RS
268 7
648 7
. YCP-12
YCP-
81397
M29-
SBOUTLET-
HCI-
2
METHOD 29, SBOUTLET, RUN 2
8N HCI RINSE • Hg
268.9
606.2
YCP-13
YCP-
81497
M29-
SBOUTLET-
APR-
3
METHOD 29, SBOUTLET, RUN 3
ACETONE PROBE RINSE
Beaker # 3
266.7
375.0
YCP-14
YCP-
814S7
M29-
SBOUTLET-
HN-
3
METHOD 29, SBOUTLET, RUN 3
NITRIC ACID PROBE RINSE
267.4
375.4
YCP-15
YCP-
81497
M29-
SBOUTLET-
BH-
3
METHOD 29, SBOUTLET, RUN 3
HN03/H202 BACK HALF
391.7
1206,1
YCI-M6
YCP-
81497
M29-
S80UTIE1-
BHM-
3
METHOD 29. SBOUTLET. RUN 3
0 IN HN03 RINSE - Hg
267.3
316.6
YCP-17 ,
YCP-
81497
M29-
SSOUTL.E1 -
KMnO-
3
METHOD 29. SBOUTLET. RUN 3
KMn04 IMPINGERS
267.1
655.6
YCP-18
YCP-
81497
M29-
SBOUTLET-
HCI-
3
METHOD 29. SBOUTLET, RUN 3
8N HCI RINSE - Hg
267.1
491.3
YCP-19
YCP-
81297
M29-
SBINLET-
APR-
1
METHOD 29, SBINLET, RUN 1
ACETONE PROBE RINSE
Beaker # 11
266.7
457.8
YCP-20
YCP-
81297
M29-
SBINLET-
HN-
1
METHOD 29, SBINLET, RUN 1
NITRIC ACID PROBE RINSE
268.6
410.6
/YCP-21 S
YCP-
81297
M29-
S8INLET-
BH-
1
METHOD 29, SBINLET. RUN 1
HN03/H202 BACK HALF
391.3
1076.4
' YCP-22
YCP-
81297
M29-
SBINLET-
BHM-
1
METHOD 29, SBINLET, RUN 1
0.1NHNO3 RINSE - Hg
270.8
342.4
YCP-23
YCP-
81297
M29-
SBINLET-
KMnO-
1
METHOD 29, SBINLET, RUN 1
KMn04 IMPINGERS
269.6
607,4
YCP-24
YCP-
81297
M29-
SBINLET-
HCI-
1
METHOD 29, SBINLET, RUN 1
8N HCI RINSE - Hg
269.3
581.0
YGP-25
YCP-
81397
M29-
SBINIET-
APR-
2
METHOD 29, SBINLET. RUN 2
ACETONE PROBE RINSE
Beaker# 12
267,7
537.0
YCP-26
YCP-
81397
M29-
SBINLET-
HN-
2
METHOD 29, SBINLET, RUN 2
NITRIC ACID PROBE RINSE
266.5
554.0
Page 1
-------
kaaiviit ixcocaibii uiwup
WWW
rfcP-27/
YCP-
81397
M29-
SBINLET-
BH-
2
METHOD 29, SBINLET, RUN 2
HN03/H202 BACK HALF
391.6
1161.6
¥?^28
YCP-
81397
M29-
SBINLET-
BHM-
2
METHOD 29, SBINLET, RUN 2
0.1 N HN03 RINSE - Hg
267,5
365.3
YCP-29
YCP-
81397
M29-
SBINtET-
KMnO-
2
METHOD 29, SBINLET, RUN 2
KMn04 IMPINGERS
266.5
718.9
YCP-30
YCP-
81397
M29-
SBINLET-
HC!-
2
METHOD 29, SBINLET, RUN 2
8N HCI RINSE - Hg
267.1
605.4
YCP-31
YCP-
81497
M29-
SBINLET-
APR-
3
METHOD 29. SBINLET, RUN 3
ACETONE PROBE RINSE
Beaker# 13
267.3
495.3
YCP-32
YCP-
81497
M29-
SBINLET-
HN-
3
METHOD 29, SBINLET, RUN 3
NITRIC ACID PROBE RINSE
266.3
410.9
/?5p13~>
YCP-
81497
M29-
SBINLET-
BH-
3
METHOD 29, SBINLET, RUN 3
HN03/H202 BACK HALF
391.5
1295.3
YCP-34
YCP-
81497
M29-
SBINLET-
BHM-
3
METHOD 29, SBINLET, RUN 3
0.1 N HN03 RINSE - Hg
2665
394.5
YCP-35
YCP-
81497
M29-
SBINLET-
KMnO-
3
METHOD 29. SBINLET, RUN 3
KMn04 IMPINGERS
266.2
725.4
YCP-36
YCP-
81497
M29-
SBINLET-
HC!-
3
METHOD 29. SBINLET, RUN 3
8N HCI RINSE - Hg
267.5
438.6
YCP-37
YCP-
81397
M29-
SBOUTLET-
APR-
FB1
METHOD 29. SBOUTLET. FB1
ACETONE PROBE RINSE
Beaker # 4
269,3
369.0
YCP-38
YCP-
81397
M29-
SBOUTLET-
HN-
FBI
METHOD 29. SBOUTLET. FBI
NITRIC ACID PROBE RINSE
2694
3986
YCP-39
YCP-
81397
M29-
SBOUTLET-
F-
FBI
METHOD 29. SBOUTLET, FB1
FILTER
Filter« 080497-24
XX
XX
YCP-40
YCP-
81397
M29-
SBOUTLET-
BH-
FB1
METHOO 29, SBOUTLET. FB1
HN03/H202 BACK HALF
2682
573.2
YCP-41
YCP-
81397
M29-
SBOUTLET-
BHM-
FBI
METHOD 29, SBOUTLET. FB1
0 1N HN03 RINSE - Hg
269.4
3169
YCP-42
YCP-
81397
M29-
SBOUTLET-
KMnO-
FBI
METHOD 29. SBOUTLET. FB1
KMn04 IMPINGERS
269.4
752.3
YCP 43
YCP-
81397
M29-
SBOUTLET-
HCI-
FB1
METHOD 29. SBOUTLET, FB1
8N HCI RINSE - Hg
269.2
429.6
S*f€P-44^
YCP-
81397
M29-
SBOUTLET-
ACE-
RBI
METHOD 29, SBOUTLET, RBI
ACETONE
269.5
444.0
YCP 45
YCP-
81397
M29-
SBOUTLET-
HNO-
RBI
METHOD 29, SBOUTLET, RB1
0.1N HN03
269.3
739.8
\ ->.
YCP-
81397
M29-
SBOUTLET-
F-
RB1
METHOD 29, SBOUTLET, RBI
FILTER
Filter # 080497-01
XX
XX '
YCP-47
YCP-
81397
M29-
SBOUTLET-
BH-
RBI
METHOD 29. SBOUTLET, RBI
HN03/H202
268 4
567.3
YCP-48
YCP-
81397
M29-
SBOUTLET-
KMnO-
RB1
METHOD 29, SBOUTLET, RB1
KMn04
269.1
493.3
YCP-49
YCP-
81397
M29-
SBOUTLET-
HCI-
RBI
METHOD 29, SBOUTLET, RB1
8N HCI
268,9
510.2
YCP-50
YCP-
81397
M29-
SBINLET-
APR-
FB2
METHOD 29, SBINLET, FB2
ACETONE PROBE RINSE
Beaker # 5
268,2
387.0
YCP-51
YCP-
81397
M29-
SBINLET-
HN-
FB2
METHOD 29. SBINLET, FB2
NITRIC ACID PROBE RINSE
267.2
439.2
YCP-52
YCP-
81397
M29-
SBINLET-
F-
FB2
METHOD 29, SBINLET, FB2
FILTER
Filter U 080497-23
XX
XX
YCP-53
YCP-
81397
M29-
SBINLET-
BH-
FB2
METHOD 29, SBINLET, FB2
HN03/H202 BACK HALF
269.4
7958
YCP-54
YCP-
81397
M29-
SBINLET-
BHM-
FB2
METHOD 29, SBINLET, FB2
0.1NHNO3 RINSE - Hg
268.5
333.4
YCP-55
YCP-
81397
M29-
SBINLET-
KMnO-
FB2
METHOD 29, SBINLET, FB2
KMn04 IMPINGERS
268.7
691.5
YCP-56
YCP-
81397
M29-
SBINLET-
HC1-
FB2
METHOD 29, SBINLET, FB2
8N HCI RINSE - Hg
269.7
439.3
YCP-57
YCP-
81597
M29-
SBINLET-
ACE-
RB2
METHOD 29. SBINLET. RB2
ACETONE
Beaker #6
268.1
407.0
CP
OD
Page 2
-------
eastern Research Group COC
YCP-58
YCP-
81597
M29-
SBINLET-
HNO-
RB2
METHOD 29, SBINLET, RB2
0.1 N HN03
391.7
648.0
f?
YCP-
81597
M29-
SBINLET-
F-
RB2
METHOD 29, SBINLET, RB2
FILTER
XX
XX
YCP-60
YCP-
81597
M29-
SBINLET-
BH-
RB2
METHOD 29, SBINLET, RB2
HN03/H202
391.6
636.3
YCP-61
YCP-
81597
M29-
SBINLET-
KMnO-
RB2
METHOD 29, SBINLET, RB2
KMn04
391.2
650.3
YCP-62
YGP-
81597
M29-
SBINLET-
HCI-
RB2
METHOD 29, SBINLET, RB2
8N HCI
390.9
602.2
YCP-88
YCP-
81297
M29-
SBOUTLET-
F-
1
METHOD 29, SBOUTLET, RUN 1
FILTER S 080497-20
XX
XX
YCP-89
YCP-
81397
M29-
SBOUTLET-
F-
2
METHOD 29, SBOUTLET, RUN 2
FILTER #080497-15
XX
XX
YCP-90
YCP-
81497
M29-
SBOUTLET-
F-
3
METHOD 29, SBOUTLET, RUN 3
FILTER #080497-19
XX
XX
YCP-91
YCP-
81297
M29-
SBINLET-
F-
1
METHOD 29, SBINLET, RUN 1
FILTER # 080497-22
XX
XX
YCP-92
YCP-
81397
M29-
SBINLET-
F-
2
METHOD 29, SBINLET. RUN 2
FILTER # 080497-21 (1 of 2)
XX
XX
YCP-93
YCP-
81497
M29-
SB1NLET-
F-
3
METHOD 29, SBINLET, RUN 3
FILTER # 080497-05 (1 of 2)
XX
XX
YCP-94
YCP-
81597
M29-
BAGAOUT-
APR-
1
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
Beaker # 7
269.1
323.0
YCP-95
YCP-
81597
M29-
BAGAOUT-
HN-
1
METHOD 29, BAG A OUTLET, RUN
NITRIC ACIO PROBE RINSE
269.1
336.9
YCP-96
YCP-
81597
r 129-
BAGAOUT-
F-
1
METHOD 29, BAG A OUTLET, RUN
FILTER
Filler # 080497-08
XX
XX
YCP-97
YCP-
81597
M29-
BAGAOUT-
BH-
1
METHOD 29, BAG A OUTLET, RUN
HN03/H202
268 6
768,4
YCP-98
YCP-
81597
M29-
BAGAOUT-
BHM-
1
METHOD 29, BAG A OUTLET, RUN
0 1N HN03 RINSE - Hg
271.0
3223
YCP-99
YCP-
81597
M29-
BAGAOUT-
KMn04-
1
METHOD 29, BAG A OUTLET, RUN
KMri04 IMPINGEKS
270.1
601.6
YCP-100
YCP-
81597
M29-
BAGAOUT-
HCI-
1
METHOD 29. BAG A OUTLET, RUN
8N HCI RINSE - Hg
269.5
406.3
YCP-101
YCP-
81597
M29-
BAGAOUT-
APR-
2
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
Beaker # 8
268.3
324.5
YCP-102
YCP-
81597
M29-
BAGAOUT-
HN-
2
METHOD 29, BAG A OUTLET, RUN
NITRIC ACIO PROBE RINSE
268.6
372.2
YCP-103
YCP-
81597
M29-
BAGAOUT-
F-
2
METHOD 29, BAG A OUTLET. RUN
FILTER
Filter # 080497-06
XX
XX
YCP-104
YCP-
81597
M29-
BAGAOUT-
BH-
2
METHOD 29, BAG A OUTLET, RUN
HN03/H202
388.7
1089.7
YCP-105
YCP-
81597
M29-
BAGAOUT-
BHM-
2
METHOD 29, BAG A OUTLET, RUN
0 IN HN03 RINSE - Hg
268.6
348.0
YCP-106
YCP-
81597
M29-
BAGAOUT-
KMri04-
2
METHOD 29, BAG A OUTLET, RUN
KMn04 IMP1NGERS
268.3
610.6
YCP-107
YCP-
81597
M29-
BAGAOUT-
HCI-
2
METHOD 29, BAG A OUTLET, RUN
8N HCI RINSE - Hg
2694
517.8
YCP-108
YCP-
81697
M29-
BAGAOUT-
APR-
3
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
Beaker # 9
265.2
318.4
YCP-109
YCP-
81697
M29-
BAGAOUT-
HN-
3
METHOD 29, BAG A OUTLET, RUN
NITRIC ACID PROBE RINSE
265.5
344.9
YCP-110
YCP-
81697
M29-
BAGAOUT-
F-
3
METHOD 29, BAG A OUTLET, RUN
FILTER
Filter #080497-14
XX
XX
YCP-111
YCP-
81697
M29-
BAGAOUT-
BH-
3
METHOD 29, BAG A OUTLET, RUN
HN03/H202
389.1
1040,1
YCP-112
YCP-
81697
M29-
BAGAOUT-
BHM-
3
METHOD 29, BAG A OUTLET, RUN
0.1NHNO3 RINSE - Hg
266.6
333.6
YCP-113
YCP-
81697
M29-
BAGAOUT-
KMn04-
3
METHOD 29, BAG A OUTLET, RUN
KMn04 IMPINGERS
267.8
609,5
CD
Page 3
-------
Eastern Research Group COC
YCP-114
YCP-
81697
M29-
BAGAOUT-
HCI-
3
METHOD 29. BAG A OUTLET, RUN
8N HCI RINSE - Hg
266.1
486.2
YCP-141
YCP-
81597
M29-
BAGA
APR-
GPB1
ETHOD 29, BAGA, GLASSWARE Bl
ACETONE PROBE RINSE
Archived at ERG
268 5
310,1
YCP-142
YCP-
81597
M29-
BAGA
HCI-
GPB1
ETHOD 29, BAGA, GLASSWARE BL
8N HCI RINSE - Hg
Archived at ERG
269.1
462.8
YCP-143
YCP-
81597
M29-
BAGA
HN-
GBP1
ETHOD 29, BAGA, GLASSWARE BL
NITRIC ACID PROBE RINSE
Archived at ERG
268.9
329.1
YCP-144
YCP-
81597
M29-
BAGA
APR-
GPB2
ETHOD 29. BAGA, GLASSWARE BL
ACETONE PROBE RINSE
Archived at ERG
268.4
302.4
YCP-145
YCP-
81597
M29-
BAGA
BH-
GBP1
ETHOD 29, BAGA, GLASSWARE BL
HN03/H202
Archived at ERG
269.1
624,4
YCP-146
YCP-
81597
M29-
BAGA
HN-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
NITRIC ACID PROBE RINSE
Archived at ERG
268.1
399.9
YCP-147
YCP-
81597
M29-
BAGA
IMP
GBP1
ETHOD 29, BAGA, GLASSWARE BL
0.1N HN03 RINSE - Hg
Archived at ERG
268,7
336.2
YCP-148
YCP-
81597
M29-
BAGA
BH-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
HN03/H202
Archived at ERG
268.4
590.9
YCP-149
YCP-
81597
M29-
BAGA
KMn04-
GBP1
ETHOD 29. BAGA, GLASSWARE BL
KMn04 IMPINGERS
Archived at ERG
268.5
613.4
YCP-150
YCP-
81597
M29-
BAGA
IMP
GPB2
ETHOD 29, BAGA. GLASSWARE Bl
0 1N HN03 RINSE • Hg
Archived at ERG
268.6
370-5
YCP-151
YCP-
81597
M29-
BAGA
KMn04-
GPB2
ETHOD 29. BAGA. GLASSWARE Bl
KMn04 IMPINGERS
Archived at ERG
268.4
445.6
YCP-152
YCP-
81597
M29*
BAGA
HCI-
GPB2
ETHOD 29. BAGA, GLASSWARE BL
8N HCI RINSE - Hg
Archived at ERG
268.8
446.8
YCM59
YCP-160
YCP-
81697
M29-
BAGA-
APR-
FB
METHOD 29, INLET, FB2
ACETONE PROBE RINSE
Beaker S 10
275.8
326.4
YCP-
81697
M29-
RAGA-
HN-
FB
METHOD 29, INLET, FB2
NITRIC ACID PROBE RINSE
274 8
369.6
YCC-161
YCP-
81697
M29-
BAGA-
BH-
FB
METHOD 29. INLET, FB2
HN03/H202 BACK HALF
391.6
859.7
YCP-162
YCP-
81697
M29-
BAGA-
IMP
FB
METHOD 29, INLET, FB2
0.IN HN03 RINSE - Hg
268.4
309.8
YCP-163
YCP-
81697
M29-
BAGA-
KMnO-
FB
METHOD 29, INLET, FB2
KMn04 IMPINGERS
2684
5990
YCP-164
YCP-
81697
M29-
BAGA-
HCI-
FB
METHOD 29, INLET. FB2
8N HCI RINSE - Hg
268.4
411.5
YCP-165
YCP-
81697
M29-
BAGA-
F
FB
METHOD 29, INLET. FB2
FILTER
Filter # 080497-03
XX
XX
YCP-170
YCP-
81397
M29-
.
RB1
METHOD 29. REAGENT BLANK
Dl WATER
393.0
8038
YCP-171
YCP-
01597
M29-
.
RB2
METHOD 29, REAGENT BLANK
Dl WATER
391.1
795.9
YCP-178
YCP-
9/2/97
M29-
SBINIET
FILTER
RUN1
FILTER FOR YCP-21
FILTER
Filter # 082797-02
METALS
YCP-179
YCP-
9/2/97
M29-
SBINLET
FILTER
RUN2
FILTER FOR YCP-27
FILTER
Filter #082797-03
METALS
YCP-180
YCP-
9/2/97
M29-
SBINIET
FILTER
RUN3
FILTER FOR YCP-33 (1 of 2)
FILTER
Filter # 082797-04
METALS
YCP-181
YCP-
9/2/97
M29-
SBINLET
FILTER
RUN3
FILTER FOR YCP-33 ( 2 of 2 )
FILTER
Filter # 082797-05
METALS
YCP-182
YCP-
9/2/97
M29-
BLANK
FILTER
BLANK
FILTER BLANK
FILTER
Filter # 082797-01
METALS
YCP-183
YCP-
8/13/97
M29-
SBINLET
FILTER
RUN2
2nd Filter fo SBInlet Run 2 (2of2)
FILTER
Fitter # 080497-25 (2 of 2)
METALS
YCP-184
YCP-
8/14/97
M29-
SBINLET
FILTER
RUN3
2nd Filter to SBInlet Run 3 (2of2)
FILTER
Filter#080497-18 {2of2)
METALS
aA
CD
at
Page 4
-------
=TRIWJGLE LABORATORIES, INC, -- LOG IN RECORD/CHAIN OF CUSTODY^
Custody Seal : Absent
Chain of Custody s Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forma : N/A
Sample Seals; Absent
Container.,,: Intact
| TLI Project Number 43159
j Client: ERG02 - Eastern Research Group
Date Received
j 09/09/97
+
By
Book jj
I 30 II
Ice Chest/Box
NO COOLANT
| Carrier and Number j JIM MC
TLI Number,
.Client Sample ID
., .Client COC ID «
.. Matrix] To LAB [To STORAGE | To LAB | To STORAGE | To LAB | To STORAGE | To LAB | To STORAGE | DISPOSED f|
Location j Date/Init j Date/Init j Date/Init | Date/Init | Date/Init | Date/Init j Date/Init j Date/Init j Date/Init j|
„ 1 i i i i 1 1 i ! «
it
||l82-30-lA
II
YCP-01
YCP-01
BEAKER] 1 1 1 1
METALS LAB | 11 1 1
till
1 1 1 1 II
1 1 1 ' i II
1 \ 1 1 H
It
j|l82-30-lB
II
YCP-02
YCP-02
i J 1 1 1
PRl 1 1 ¦. 1 1
METALS LAB | | | | |
1 1 1 1 1
1 1 1 I ii
1 1 1 1 II
1 1 1 1 II
1 1 I 1 If
II"
||l82-30-lC
II
YCP-03
YCP-03
1 1 1 I 1
HH03/H2021 1 1 1 1
METALS LAB j j j j j
1 1 1 1 1
i 1 1 1 11
l I 1 l ll
ii l I ll
1 | • l If
H
||!82-30-lD
II
YCP-04
YCP-04
I I 1 I !
0.1N RN03} '"| | | |
METALS LAB j j j I I
1 ! I f I
i 1 1 I 11
1 1 1 1 II
1 1 1 1 II
1 t t 1 II
It
||l82-30-lE
ll
h
YCP-05
YCP-05
1 1 1 1 1
KMN04| 1 1 1 1
METALS LAB | | j | |
1 II 1 1
III! II
i i i i n
.i i i i ii
1 f \ •
II
||l82-30-lF
ll
1!
YCP-06
YCP-06
HCL| 1 1 1 1
METALS LAB | | | | |
1 1 1 1 1
1 i i 1 II
i i i i ii
i i i i ii
l 1 i i it
II
||l82-30-lG
II
H
YCP-88
YCP-B8
1 t 1 I 1
FILTER| 1 1 1 I
METALS LAB j | j j |
1 1 1 1 1
1 1 1 1 ii
i i i i ii
i i i i ii
II
||l82-30-2A
ll
H
YCP-07
YCP-07
1 i 1 1 1
BEAKER| | | | |
METALS LAB | j | j j
(1(11
I i 1 I il
i i i i ii
i - i i i ii
i i i i H
(I
||l82-30-2B
ll
ii
YCP-08
YCP-08
1 1 i I.I
PR| 1 1 1 1
METALS LAB | | | | |
I I 1 1
1 I 1 1 II
i i i i n
i i i i u
11
||l82-30-2C
ll
ii
YCP-09
YCP-09
I I 1 I 1
HN03/H2G2| | | | |
METALS LAB | j j j |
1 1 1 1 1
till II
i i i i ii
i i i i ii
I | i i ii
ii
||l82-30-2D
II
||
YCP-10
YCP-10
0.1NHN03| ill!
. METALS LAB | j j | j
1 1 1 1 1
1 1 1 1 11
1 1 1 1 11
1 1 1 1 II
III I it
II
||l82-30-2E
II
|l
YCP-11
YCP-11
KMN04| 1 I | I
METALS LAB | j | j j
1 | i | |
1 1 1 1 il
1 1 1 1 II
1 1 1 1 II
I | I i n
It
(|lB2-30-2F
II
B
YCP-12
YCP-12
HCL| 1 1 1 1
METALS LAB | | | | j
i 1 i I I
1 I i f ¦¦ —il
1 1 1 • 1 II
1 1 1 1 II
1 I 1 1 il
» 1 • • 1 1 "1 - N
||l82-30-2G
YCP-89
YCP-89
FILTER!
METALS LAB
|| Receiving Remarks:
YCP-21
filter
YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
arrived But is not listed on C.O.C.
||^Ajfl^.vc Remarks:
=Porm Revised 05/27/1997 -- Page 1 OF 8=
-------
Custody Seal
Chain of Custody
Sample Tags
Absent
Present
Absent
Sample Tag Numbers! Not Listed on Chain of Custody
SMO Forms : N/A
Sample Seals; Absent
Container,..: Intact
| TL1 Project Number 43159
j Client: ERG02 - Eastern Research Group
Date Received
1 1
I 09/09/97 | By
Book
I To STORAGE I
Date/Init j
Date/Init
Ice Chest/Box
NO COOLANT
| Carrier and Number I JIM MC
* ¦ « . '
j|TLI Number Client Sample ID Matrix| To LAB | To STORAGE] To LAB j To STORAGE| To LAB | To STORAGE| To LAB
||mR/H:CPM Client COC ID » Location j Date/Init | Date/Init j Date/Init j Date/Init j Date/Init | Date/Init j Date/Init
1 1 1 1 1
jjl82-30-3A
VCP-13
YCP-13
BEAKER)
METALS LAB
I
jjl82-30-3B
YCP-14
YCP-14
PR |
METALS LAB
j|l82-30-3C
yep-is
YCP-15
HN03/H202)
METALS LAB
jjl82-30-3D
YCP-16
YCP-16
0. 1NHN03 |
METALS LAB
||l82-30-3E
YCP-17
YCP-17
KMN04 |
METALS LAB
jjl82-30-3F
j|
j| 182-30-3G
YCP-18
YCP-18
HCL|
METALS LAB
YCP-90
YCP-90
FILTER)
METALS LAB
jjlS2-30-4A
YCP-19
YCP-19
BEAKER)
METALS LAB
jjl82-30-4B
YCP-20
PR |
1!
it
YCP-20
METALS LAB | j | | |
II 1 1 1
I 1 1 1 II
III 1 II
1!
j|l82-30-4C
II
ii
YCP-22
YCP-22
0.1NHN03| 1 1 1 1
METALS LAB 11111
III 1 1
1 1 1 il
i i i i ii
i i i i ii
Iff i it
H
||l82-30-4D
II
II
YCP-23
YCP-23
KMN041 I | | |
. METALS LAB | j j j |
1 1 1 1 1
i i1 il
iii i ii
i i i i n
if i ii
II
||l82-30-4E
II
||
YCP-24
YCP-24
hcl) 1 1 1 1
METALS LAB 1 1 1 I I
1 ! I 1 1
i i i i ii
i i i i n
i i i i ii
i i * i H
II
||l82-30-4P
II
||
YCP-91
YCP-91
FILTER) 1 1 1 1
METALS LAB j j j j j
1 1 1 1 1
i I \ I 11
j i i ¦ i n
iii i ii
i i i t ii
II
||l82-30-SA
II
I'm — Mid..,. • « 1. ' ¦ ¦ ITT
YCP-25
YCP-2S
1 1 1 1 1
BEAKER) I 1 1 I
METALS LAB j j j j j
• , • • 1 f i
ill II
iii i ii
iii i n
» 1 —i •,
Receiving Remarks:
YCP-21,YCP-2 7,YCP-3 3,YCP-4 4 ,YCP-59 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
Archive Remarks:
aamtmmxM
CP
-Form Revised 05/27/1997 -- Page 2 OF 8=
-------
| Book
Sample Seals: Absent
TLI Project Number 43159 ,
Client: GRG02 - Eastern Research Group
Custody Seal
Chain of Custody : Present
: Absent
: Absent
Sample Tags
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms
| 09/09/97 | By
: N/A
Date Received
Page
Carrier and Number | JIM MC
Ice Chest/Box
NO COOLANT
Matrix
To LAB
Date/Init
To STORAGE
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
TLI Number Client Sample ID
mR/H:CPM.
To LAB
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
DISPOSED
Date/Init
Location
Client COC ID
PR
YCP-26
YCP-26
82-30-5B
METALS LAB
KMN04
YCP-28
YCP-28
METALS LAB
HCL
YCP-29
YCP-29
182-30-5D
METALS LAB
FILTER
YCP-30
YCP-30
182-30-5E
METALS LAB
FILTER
YCP-92
YCP-92
182-30-5F
METALS LAB
FILTER
102-3O-5G
METALS LAB
BEAKER
YCP-31
YCP-31
182-30-6A
METALS LAB
PR
YCP-32
YCP-32
METALS LAB
.IN HN03
182-30-6C
YCP-34
YCP-34
METALS LAB
KMN04
182-30-6D
YCP-35
YCP-35
METALS LAB
HCL
YCP-36
YCP-36
182-30-6E
• METALS LAB
FILTER
YCP-93
YCP-93
METALS LAB
FILTER
METALS LAB
BEAKER
YCP-37
YCP-37
METALS LAB
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
Ar^lye Remarks:
'Form Revised 05/27/1997
Page 3 OP 8
-------
Custody Seal : Absent
Chain of Custody s Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms i N/A
Sample Seals: Absent
Container.,,! Intact
| TLI Project number 4 3159 ,
| Client; ERG02 - Eastern Research Oroup
|
| Date Received
09/09/97 | By
i
Book
| 102
| Page
30
Ice Chest/Box
NO COOLANT
II ' -
IITLI Number Client Sample ID v Matrix
jjmR/HiCPM, Client COC ID. .,,,,* Location
j Carrier and Number j JIM MC
i 1 i
To STORAGE|
Date/Init j
To LAB | To STORAGE | To LAB | To STORAGE
Date/Init j Date/Init j Date/Init j Date/Init
To LAB
Date/Ini t
To STORAGEI To LAB
Date/Init j Date/Init
DISPOSED
Date/Init
jjl82-30-7B
YCP-38
YCP-38
PR
METALS LAB
' I
j|i82-30-?C
YCP-39
YCP-39
FILTER
METALS LAB
H182-30-7D
YCP-40
YCP-4 0
HN03/H202
METALS LAB
jjl82-30-7E
YCP-41
YCP-41
Hg HN03
METALS LAB
jjl82-30-?F
YCP-42
YCP-42
Hg KMn04
METALS LAB
||l82-30-7<3
YCP-43
YCP-43
Hg HC1
METALS LAB
||182-3Q-8A
YCP-4S
YCP-45
0.1NHN03
METALS LAB
|jl82-30-8B
YCP-46
YCP-46
FILTER
METALS LAB
jjl82-30-8C
YCP-47
YCP-47
HN03/H202
METALS LAB
jjl82-30-8D
YCP-48
YCP-48
KMN04
METALS LAB
jjl82-30-8E
YCP-49
YCP-49
HCL
. METALS LAB
j|182-30-9A
YCP-50
YCP-50
BEAKER
METALS LAB
||l82-30-9B
YCP-51
YCP-51
PR
METALS LAB
j|!82-30-9C
II
II-
YCP-S2
YCP-52
FILTERj
METALS LAB
Receiving Remarks;
YCP-21
filter
YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
arrived But is not listed on C.O.C.
Archive Remarksi
" 1 p")'
"Form Revised 05/27/1997 -- Page 4 OF 8-=
CD
-------
Custody Seal :
Chain of Custody s
Sample Tags :
Sample Tag Numbers;
SMO Forms s
Absent
Present
Absent
Not Listed on Chain of Custody
N/A
Sample Seals: Absent
Container..,: Intact
| TLI Project Number 431S9 ,
| Client: ERG02 - Eastern Research Group
Date Recoived
09/09/97 j By
j Book
182
| Page
Ice Chest/Bo*
NO COOLANT
j Carrier and Number j JIM MC
I 30
j|TLI Number,.
||mR/H:CPM.
-f
.Client Sample ID...
,..Client COC ID
! , ¦=
Matrix| To LAB | To STORAGE | To LAB | To STORAGE| To LAB | To STORAGE| To LAB | To STORAGE| DISPOSED
Location j Date/Init j Date/lnit j Date/Init j Date/lnit j Date/Init j Date/Init j Date/Init j Date/Init j Date/Init
jjl82-30-9D
YCP-53
YCP-S3
HN03/H202|
METALS LAB
182-30-9E
YCP-54
YCP-54
Hg HN03|
METALS LAB |
182-30-9F
YCP-55
YCP-S5
Hg KMn04|
METALS LAB j
182-30-9C1
YCP-56
YCP-S6
Hg HClj
METALS LAB
jjl82-30-10A
YCP-S7
YCP-S7
BEAKER)
METALS LAB
jj 1S2-30-1QB
YCP-S8
YCP-S8
0.1NKN03 j
METALS LAB
||l82-30-10C
YCP-60
YCP-60
HN03/H202|
METALS LAB
jjl82-30-10D
I!
||l82-30-10E
YCP-61
YCP-61
KMN04 |
METALS LAB
YCP-62
YCP-62
HCL|
METALS LAB
||l82-30-HA
YCP-94
YCP-94
BEAKER|
METALS LAB
jjl82-30-llB
YCP-95
YCP-95
PR
METALS LAB
¦30-11C
YCP-96
YCP-96
FILTER
METALS LAB
H182-30-11D
YCP-97
YCP-97
KN03/H202
METALS LAB
||182-30-llE
II
IH
YCP-98
YCP-98
IMP 4 |
METALS LAB j
Receiving Remarks:
YCP-21
filter
,YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
arrived But is not listed on C.O.C.
Archive Remarks:
-ai
o
=Form Revised OS/27/1997 -- Page 5 OF 8=
-------
Custody Seal : Absent
Chain of Custody : Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain o£ Custody
SMO Forms : N/A
Sample Seals: Absent
Container,,.: Intact
| TLI Project Number 431S9 ,
| Client: ERG02 - Eastern Research Group
I
Book
182
j Date Received
1 1
| 09/09/97 | By
Page
30
Ice Chest/Box
NO COOLANT
| Carrier and Number | JIM MC
I ii, iiiI,.,. j u.lni J
j|TLI Number Client Sample ID , Matrlx| To LAB | To STORAGE| To LAB | To STORAGE
||mR/H:CPM. Client COC ID * Location,,, j Data/Init j Date/Inlt j Date/Init j Date/Inlt
To LAB j To STORAGE I To LAB
Date/Init | Date/Inlt j Date/Init
| To STORAGE |
j Date/Init j
DISPOSED
Date/Inlt
HI
jj 182-30" IIP
YCP-99
YCP-99
Hg KMn041
METALS LAB I
I
I
I
jjl82-30-110
YCP-100
YCP-100
Hg HC11
METALS LAB
j)l82-30-12A
YCP-101
YCP-101
BEAKER)
METALS LAB
jjl82-30-12B
YCP-102
YCP-102
PR |
METALS LAB |
jj 182- 30- 12C
YCP-103
YCP-103
FILTER |
METALS LAB
|j 182-30 -1213
YCP-104
YCP-104
HN03/H202 j
METALS LAB
jjl82-30-12E
YCP-10S
YCP-105
METALS LAB
IMP 4 j
jjl82-30-12F
YCP-106
YCP-106
KMN04 |
METALS LAB
j|l82-30-12Q
YCP-107
YCP-107
Hg UC1[
METALS LAB
jjl82-30-13A
YCP-108
YCP-108
BEAKER)
METALS LAB
||l82-30-l3B
YCP-109
YCP-109
PR)
METALS LAB
j|l62-30-l3C
YCP-110
YCP-110
FILTER)
METALS LAB
jjl82-30-13D
||
||l82-30-13E
il
If—
YCP-111
YCP-111
HN03/H202)
METALS LAB j
YCP-112
YCP-112
IMP 4
METALS LAB
Receiving Remarks:
YCP-21,YCP-27,YCP-3 3,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C,
Archive Remarks:
»Form Revised 05/27/1997 -- Page 6 OF 8=
-------
=TRIANGLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY=
Custody Seal : Absent
Chain of Custody : Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A
Sample Seals: Absent
Container...: Intact
TLI Project Number 43159 ,
Client: ERG02 - Eastern Research Group
Date Received
| 09/09/97 | By
-A 1
Ice Chest/Box
NO COOLANT
Carrier and Number j JIM MC
. '
||TLI Number.. .
Matrix
To LAB
To STORAGE
To LAB
To STORAGE
To LAB
To STORAGE
To LAB
To STORAGE
Date/Init
DISPOSED
Date/Init
...Client COC ID...
•
Date/Init
Date/Init
Date/Init
Date/Init
Date/Init
Date/Init
Date/Init
||182-30~13F
YCP-113
YCP-113
Hg KMn04
METALS LAB
||102-3O-13G
YCP-114
YCP-114
Hg HC1
METALS LAB
j|lB2-30-14A
YCP-159
YCP-159
BEAKER
METALS LAB
||l82-30-14B
YCP-160
YCP-160
PR
METALS LAB
• ¦
||l82-30-i4C
YCP-161
YCP-161
IMP 1,2,3
METALS LAB
jjl82-30-14D
YCP-162
YCP-162
IMP4
METALS LAB
||l82-30-14E
YCP-163
YCP-163
KMN04
METALS LAB
j|l82-30-14F
YCP-164
YCP-164
HCL
METALS LAB
**
[j 102-30-140
II
YCP-165
YCP-165
FILTER
METALS LAB
•
jjl82-30-15A
YCP-169
YCP-169
HPLC
METALS LAB
j|l82-30-15B
YCP-170
YCP-170
DI H20
• METALS LAB
||l82-30-15C
II
YCP-171
YCP-171
1ATER
METALS LAB
11
||102-3O-16A
YCP-178
YCP-178
FILTER
METALS LAB
|jl82-30-16B
"
YCP-179
YCP-179
FILTER
METALS LAB
t
i
i
ll — ¦
Receiving Remarks:
Archive Remarks:
YCP-21,YCP-27,YCP-33
filter arrived But i
,YCP-44 ,YCP-59 were missing
not listed on C.O.C.
from shipment.Also a YCP-169
=Form Revised 05/27/1997 -- Page 7 OF 8=
•vl
l\1
-------
Sample Seals: Absent
Container,,.! Intact
| tli Project Number 43159 ,
| Client: ERG02 - Eastern Research Group
Book
: Absent
Custody Seal
Chain of Custody : Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms
j Date Received
09/09/9? j B;
¦age
j Carrier and Number j JIM MC
Ice Chest/Box
NO COOLANT
To STORAGE I To LAB
Date/Init | Date/Init
To STORAGEj DISPOSED
Date/Init j Date/Init
| To STORAGEj To LAB
Date/Init j Date/Init j Date/Init
To STORAGE
Date/Init
Matrix
To LAB
Date/Init
To LAB
TLI Number Client Sample ID
Client COC ID.
Location
FILTER
METALS LAB
FILTER
YCP-181
YCP-181
METALS LAB
FILTER
METALS LAB
Receiving Remarks: YCP-21,YCP-27,YCP-33, YCP-4 4 ,YCP-59 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
Archive Remarks:
'Form Revised OS/27/1997 -- Page 8 OF 8-
li il
II Receiving Remarks: YCP-21, YCP-27, YCP-33, YCP-44 , YCP-59 were missing from shipment .Also a YCP-169 |j
jj filter arrived But is not listed on C.O.C. . |
II I!
II Archive Remarks: ||
I1 , Revised OS/27/1997 -- Page 8 OF n ¦ ¦ i i . "
CJ
-------
"TRIANGLE LABORATORIES, INC. -- LOG IN RECORD/CHAIN OF CUSTODY^
Custody Seal : Absent
Chain of Custody : Absent
Sample Tags : Absent
Sample Tag Numbers: Hot Listed on Chain of Custody
SMO Forma : N/A
Sample Seals; Absent
Container...: Intact
TLI Project Number 43187
Client: ERGO2 - Eastern Research Group
Date Received
09/10/97
Book
. | 182
|| Styro Cooler
NO COOLANT
Temp 22.0 C
| Carrier and Number j JIM MC
58
ll
||TLI Number.
||mR/H:CPM.
I
Matrix|
1
|
To LAB
11
To STORAGE
To LAB
i i
| To STORAGE
To LAB
To STORAGE|
Date/Init j
|
To LAB
" 1 i
To STORAGE
ll
DISPOSED ||
Client COC ID *
Location
Date/Init
Date/Init
Date/Init
| Date/Init
l
Date/Init
Date/Init
Date/Init
Date/Init ||
11
It"
||182-5B-1
II
YCP-21
REFER TO TLI PROJECT43159«
C02
WATER|
1
I
1
1
|
1
1
1
II
11
II
H -
|| 182-58-2
ll
YCP-27
REFER TO TLI PROJECT43159*
C02
1
WATER|
1
I
1
1
|
1
i
i
II
II
||
II
||l82-58-3
II
YCP-33
REFER TO TLI PROJECT431S9*
C02
1
WATER|
1
i
1
1
1
i
i
i
i
•
II
II
»
It— I i I \ I i < I I ll
ll 1 l l 1 1 1 1 1 1 ll
ll 1 1 1 1 1 1 1 1 1 II
ii i i i i i i i i i ii
!l
11
II
II
•.
1
1
i
I
1
I
1
. i
i
t
11
II
II
II
II
II
ll
i
1
l
i
1
1
I
I
i
i
i
i
II
11
II
II
II
11
II
i
1
1
•
1
1
1
i
1
i
i
' ' II
II
11
ii iii"i i m,i i i ,m 1 r u
II . 1 1 1 1 1 1 1 1 1 II
11 1 1 1 1 I 1 1 1 1 11
ii i i i i i i i i i ii
II
II
ll
1
1
i
1
I
l
i
i
ll
11
II
ii
II
II
II
1
1
•
¦
1
1
1
i
1
ll
II
11
ii • i i i i i i i i i it
II 1 1 1 1 1 1 1 1 t II
II 1 1 1 1 1 1 1 1 1 II
ii i i i - i i i i i i n
ii
II
11
ii
1
1
i
1
1
i
u
II
II
ii i i i i i i i i i ii
II 1 I 1 1 1 1 1 1 1 II
II I 1 1 1 1 ' 1 . t 1 1 II
II | | j j | ii i i ii
II 1 1 1 1 1 1 1 1 I - ||
11 1 I 1 1 1 I 1 1 1 11
II 1 1 I 1 1 1 1 I I H
r , ' i i i —i 1 i i i ii
II Receiving Remarks: NO COOLANT PRESENT WITH SAMPLES THUS THE HIGH TEMPERATURE, SAMPLES ARE PART OF TLI PROJECT #43159.
il
II
|| Archive Remarks:
13*
•Form Revised 05/27/1997 -- Page 1 OF 1=
-------
Client: Palbw Triangle Laboratories of RTP
3ole/ln>.: O^kmbov 7 . (919)544-5729
"llent Runil_ /)jeAd hw /
KJF • GFAA FI.AA CVAA
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lnl |
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¦ ml to ml FV + ul Sc
Initials:
-------
Client:
Date/lnt.;.
Triangle Laboratories of RTP
(919)544-5729
client Run# fihthod SM.SBotfne i, Pw 0-
CONT#
©
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4
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label /tfolS 0 -olf\
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labelI So!label iScfbo "JIC
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steynoaa orid-
redlssolve In ~ .
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volume
to 20 ml on
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'ith conc. HF
d conc. HN03
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int j22L
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I
j label 12 £ -30-o$label\W('
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mL
label int
final spk conc, pajQ
added ppb
Volume.
ISd
Date
'f
(One post digestion spk on BH (or GFAA)
mL
FH & BH Serial dilution performed
ml to ml FV + uL Sc
Initials:
-------
Client:
Date/lnt.:_
Triangle Laboratories of RTP
(919) 544-5729
Client Run# fefhtrf 8f\SP)0(JlTL£f, ^3
eg#
CONT#
©
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S
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Type: G or Q
label
label
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Date
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J
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®
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label
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3.
Date
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label "36~3f"
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final spk conc. Date
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ml
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ml to ml FV + uL Sc
Initials:
-------
Client:
Date/lnt.;.
Client Run# A^lod^, i-AJtgf I
Triangle Laboratories of RTP
(919) 544-5729
CONT#
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Filter
Type: G or Q
label
J&L30-4F
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label jM
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M jM , j
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(One post dlgesllon spk on DH lor GFAA)
abelint _MC.
Volume/0 O Date
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of Ko ppb
final spk conc.
added ,5 ppb
Date
FH & BH Serial dilution performed
ml to ml FV + uL Sc
Initials:
-------
Client:
Date/Int.;
Client Run# IflLBT^ ftUAjA
Triangle Laboratories of RTP
(919) 544-5729
ay
CONT#
CONT#
©
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Filter
Type: G or Q
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label ifiahSP~5A
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label-l^'^lumeDM'
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k$l
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s
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/Ith conc. HF
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label I *3-36 'SPM-A,&
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labellabel JM.-A
Volume Oflk Volume 10^
CONT#
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label
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' ml
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Aliquot B
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mL
m
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label
Volume
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Aliquot B:
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CONT#
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mi to ml FV + ul Sc
Initials:
-------
Cllent: Triangle Laboratories of RTP
Date/lnt.: (919)544-5729
Client Run# Mt-fhcd <9°i JIniETl Ruti 3
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Date/lnt,:.
Client Run#
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(919) 544-5729
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Initials:
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-------
Client:
Date/lnt.:.
Client Run# MtibOti LET ft FB 3. [glArft)
Triangle Laboratories of RTP
(919)544-5729
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Initials:
-------
Client:
Date/lnt.:_
Triangle Laboratories of RTP
(919)544-5729
Client Run# 9f\, bffafi DrfTLBTf UUN i
CONT#
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Triangle Laboratories of RTP
(919) 544-5729
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Initials:
-------
Client:
Date/int,;.
Client Run# MeMaj M "Pilfer pga C/3lc*"k)
Triangle Laboratories of RTP
(919) 544-5729
CONT #
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1 1
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-------
Client:
Date/lnt.:.
Triangle Laboratories of RTP
(919) 544-5729
Client Run#
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Date
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Date
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FH & BH Serial dilution performed
ml to ml FV + uL Sc
Initials:
-------
Client:
Date/lnt.:_
Triangle Laboratories of RTP
(919) 544-5729
Client Run#
JT #
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FH & BH Serial dilution performed
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Initials:,
-------
/
PAGE _ (p(p
INORGANICS SPIKE LOG
DATE
PROJECT#
SAMPLE IDs
ANALYTE
ORIGINAL
STANDARO
it
ORIGINAL
STANDARO
CONG.
(PPM)
SPIKE
SAMPLE
(HL)
FINAL
VOLUME
(mL)
SPIKE
SAMPLE
(PPB)
INITIALS
WITNESS
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43)54-A LCS
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3-W3-3
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L0
qa\forms\Incspke.log (08/22/96) 91
-------
SEE SPIKE LOG
TU* 43W4-
Spiking Standard Preparation
[SPIKING
from Spiking Standard
EXP date
Element
Standard
Orig. Std.
SpikefuLS
cone
ppike(uL)
cone
combined
ID
(ppm)
FvoI(IOOmL)
(ppm)
rVol(IOOmi)
tppts)
total
2/1 m
2-115-4
100
5000
5
1000
50
9/1/98
3-010-10
100
5000
5
1000
50
2/1/98
«
2-115-4
100
5000
5
1000
50
9/1/98
M
3-010-7
10000
950
95
1000
950
1000
2/1/98
3
2-115-4
100
5000
5
1000
50
2/1/98
3a
2-115-4
100
5000
5
1000
50
9/1/98
3e
3-010-10
100
5000
5
1000
50
9/1/98
la
3-010-10
100
5000
5
1000
50
9/1/98
Ja
3-012-7
10000
950
95
1000
950
1000
9/1/98
2d
3-010-10
100
5000
5
1000
50
9/1/98
Zo
3-010-10
100
5000
5
1000
SO
9/1/98
Zr
3-010-10
100
5000
5
1000
50
9/1/98
Zu
3-010-10
100
5000
5
1000
50
9/1/98
:e
3-010-10
100
5000
S
1000
50
9/1/98
-e
3-012-6
10000
950
95
1000
950
1000
2/1/98
<
2-115-4
1000
5000
50
1000
500
9/1/98
<
3-012-5
10000
1SOO
ISO
1000
1500
2000
9/1/98
^9
3-010-10
100
5000
5
1000
50
8/1/98
Wg
3-010-8
10000
950
95
1000
950
1000
9/1/98
\
92
-------
PAGE 1 OF 4
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 4315 9-A
Transfer From: IWLM
Initia
Released by:
Accepted by:
To: IA I
Date
1 MM
°i / 2H/ °<1
Time
23:_H5~
MILES.ID,
TLI No
Cust.Id
43159-A
-000
TLI Blank
TLI Method Blank
43159-A
-001
182-30-1A
YCP-01
43159-A
-002
182-30-1B
YCP-02
43159-A
-003
182-30-1C
YCP-03
43159-A
-004
182-30-ID
YCP-04
43159-A
-005
182-30-1E
YCP-05
43159-A
-006
182-30-1F
YCP-06
43159-A
-007
182 - 30 -1G
YCP-88
43159-A
-008
182-30-2A
YCP-07
43159-A
-009
182-30-2B
YCP-08
43159-A
-010
182-30-2C
YCP-09
43159-A
-011
182-30-2D
YCP-10
43159-A
-012
182-30-2E
YCP-11
43159-A
-013
182-30-2F
YCP-12
43159-A
-014
182-30-2G
YCP-89
43159-A
-015
182-30-3A
YCP-13
43159-A
-016
182-30-3B
YCP-14
43159-A
-017
182-30-3C
YCP-15
43159-A
-018
182-30-3D
YCP-16
43159-A
-019
182-30-3E
YCP-17
43159-A
-020
182-30-3F
YCP-18
43159-A
-021
182-30-3G
YCP-90
43159-A
-022
182-30-4A
YCP-19
43159-A
-023
182-30-4B
YCP-20
43159-A
-024
182-30-4C
YCP-22
43159-A
-025
182-30-4D
YCP-23
43159-A
-026
182-30-4E
YCP-24
43159-A
-027
182-30-4F
YCP-91
43159-A
-028
182-58-1
YCP-21
43159-A
-029
182-30-5A
YCP-25
dditional comments or instructions:
-XfrCOC (Rev 11/01/94:
93
-------
PAGE 2 OF 4
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 43159-A
Transfer From: IWLM
Released by;
Accepted by:
Init
To: IA I
Date,
9
. 4
°\I AJV
Time.<.
-2^> HS"
MILES.ID,
•
. TLI No
Cust.Id
43159-A
-030
182-30-5B
YCP-26
43159-A
-031
182-30-5C
YCP-28
43159-A
-032
182-30-5D
YCP-29
43159-A
-033
182-30-5E
YCP-30
43159-A
-034
182-30-5F
YCP-92
43159-A
-035
182-30-5G
YCP-183
43159-A
-036
182-58-2
YCP-27
43159-A
-037
182-30-6A
YCP-31
43159-A
-038
182-30-6B
YCP-32
43159-A
-039
182-30-6C
YCP-34
43159-A
-040
182-30-6D
YCP-35
43159-A
-041
182-30-6E
YCP-36
43159-A
-042
182-30-6F
YCP-93
43159-A
-043
182-30-6G
YCP-184
43159-A
-044
182-58-3
YCP-33
43159-A
-045
182-30-7A
YCP-37
43159-A
-046
182-30-7B
YCP-3 8
43159-A
-047
182-30-7C
YCP-39
43159-A
-048
182-30-7D
YCP-40
43159-A
-049
182-30-7E
YCP-41
43159-A
-050
182-30-7F
YCP-42
43159-A
-051
182-30-7G
YCP-4 3
43159-A
-052
182-30-8A
YCP-45
43159-A
-053
182-30-8B
YCP-46
43159-A
-054
182-30-8C
YCP-47
43159-A
-055
182-30-8D
YCP-48
43159-A
-056
182-30-8E
YCP-49
43159-A
-057
182-30-10A
YCP-57
43159-A
-058
182-30-9A
YCP-50
43159-A
-059
182-30-9B
YCP-51
ditional comments or instructions:
-XfrCOC (Rev 11/01/94)
94
-------
PAGE 3 OF 4
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 43159-A
Transfer From: IWLM To: IA I
Initial^. . Date.
Released by: _
Accepted by;
Mm
Time.
MILES. ID TLI No Cust. Id
43159-A
-060
182-30-9C
YCP-52
43159-A
-061
182-30-9D
YCP-53
43159-A
-062
182-30-9E
YCP-54
43159-A
-063
182-30-9F
YCP-55
43159-A
-064
182-30-9G
YCP-56
43159-A
-065
182-3 0-11A
YCP-94
43159-A
-066
182-30-11B
YCP-95
43159-A
-067
182 -3 0-11C
YCP-96
43159-A
-068
182- 3 0 -11D
YCP-97
43159-A
-069
182-30-11E
YCP-98
43159-A
-070
182-30-11F
YCP-99
43159-A
-071
182-30-11G
YCP-100
43159-A
-072
182-30-12A
YCP-101
43159-A
-073
182-30-123
YCP-102
43159-A
-074
182-30-12C
YCP-103
43159-A
-075
182 -3 0 -12D
YCP-104
43159-A
-076
182-3 0-12E
YCP-105
43159-A
-077
182-30-12F
YCP-106
43159-A
-078
182-30-12G
YCP-107
43159-A
-079
182-3 0 -13A
YCP-108
43159-A
-080
182-30-133
YCP-109
43159-A
-081
182-30-13C
YCP-110
43159-A
-082
182-30-13D
YCP-111
43159-A
-083
182-30-13E
YCP-112
43159-A
-084
182-30-13F
YCP-113
43159-A
-085
182 - 3 0 -13G
YCP-114
43159-A
-086
182-30-14A
YCP-159
4315 9-A
-087
182-3 0-14B
YCP-160
43159-A
-088
182-30-14C
YCP-161
43159-A
-089
182-30-14D
YCP-162
XfrCOC (Rev 11/01/94)
dditional comments or instructions:
95""
-------
PAGE 4 OF 4
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 43159-A
Transfer From: IWLM To: IA I
Initial/§V Date. ...... Time.
Released by:
1
Accepted by: n>M <\ / in/ «r? ^5-
MILES. ID TLI No Cust. Id
43159-A
-090
182-30-14E
YCP-163
43159-A
-091
182-3 0-14F
YCP-164
43159-A
-092
182 -3 0-14G
YCP-165
43159-A
-093
182-30-15B
YCP-170
43159-A
-094
182-30-15C
YCP-171
43159-A
-095
LCS
Lab Control Spike
XfrCOC (Rev 11/01/94)--
iditional comments or instructions:
96
-------
'V j*.- <"
v«--.
SB
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-------
* SEE SPIKE LOG
Spiking Standard Preparation
SPIKING
'rom Spiking Standard
EXP date
Element
Standard
Org. Std.
Spike(uL)
cone
Spike
1000
50
9/1/98
2o
3-010-10
100
5000
5
1000
50
9/1/98
Zr
3-010-10
100
5000
S I
1000
50
9/1/98
Zu
3-010-10
too
sooo
S I
1000
50
9/1/98
"B
3-010-10
100
5000
5 I
1000
50
9/1/98
z9
3-012-6
10000
950
95 {
1000
950
1000
2/1/98
<
2-115-4
1000
sooo
50 I
1000
500
9/1/98
<
3-012-5
10000
1500
150 |
1000
^500
2000
9/1/98
3-010-10
100
5000
S !
1000
50
8/1/98
3-010-8
10000
950
95 |
1000
950
1000
9/1/98
Mrs
3-010-10
too
SOOO
5 1
1000
50
9/1/98
yio
3-010-10
100
SOOO
5 j
1000
50
2/1/98
sia
2-115-4
100
5000
5 |
1000
50
8/1/98
via
3-010-9
100C0
1950
195 |
1C00
'.950
2000
9/1/98
3-010-10
100
5000
5 i
1000
50
9/1 /98
3b
3-010-10
too
5000
5
1000
50
9/1/98
3b
3-010-10
100
5000
5
1000
50
9/1/96
5e
3-010-10
100
5000
5
1000
50
9/1/98
R
3-010-10
100
SOOO
S
1000
50
9/1/98
n
3-010-10
100
5000
5
1000
50
9/1/98
3-010-10 .
100
5000
5
1000
50
9/1/98
zn
3-010-10 |
100
5000
5
1000
50
8/1/98
Zn
3-010-6 i
1000
1500
15 f
1000
ISO
200
iOCOul of the SpiKing Standard gives trie cistea cono. at tne aoove dements.
"Spike seoemiMy
Bemant Ong Std Spike(ul) cone
(ppm) Fvo*(1QOm (ppb)
Au
1000
140
1400
Ce
1000
30
300
U
1000
70
700
P
1000
100
1000
Pd
1000
160
1600
Ft
1000
300
3000
S
1000
350
3500
Si
toooo
350
35000
Sn
1000
20
200
Sr
1000
5
50
Spiking Standard 3-013-4
EXP: 11/26/97
Spiked by:
Pfeaigesecn-
PostCigesoon- " ' 1 V
93
-------
Analysis Report Suis»ary
Sun 10-05-97 06:55:31 PH page 1
i Sasple Naae
file
Method
Date
Tine OpID Type Node
1 STD1--SI-ANK—
100397
TKraratr
—
"A
~~AH
2 STD3
100397
TRIANGL2
10/03/97
23:07
y
IR
3 ST03
100397
TRIANGL2
10/03/97
23:12 DKH
CONC
4 CHECK L0
100397
TRIANGL2
10/03/97
23:16 DKJf'
8
CONC
5 ICV/CCV
100397
TRIANGL2
10/03/97
23:2UJKH
Q
CONC
6 IC8/CC8
100397
TRIANG12
10/03/97
23^ DKH
a
CONC
7 IC8/CC8
100397
TRIANG12
10/03/97
23:51 DKH
0
CONC
8 ICSA8
100397
TRIANG12
10/03/9^
23:56 DKH
s
CONC
9*43332A HB
100397
TRIANGL2
io/oy<7
00:13 DKH
s
CONC
10 43332A ICS
100397
TRIANGL2
10/pi/97
00:29 DKH
s
CONC
11 184-5-2
100397
TRIANGL2
10/04/97
00:44 DKH
s
CONC
12 184-5-2 D
100397
TRIAHGLZ'
40/04/97
00:49 DKH
s
CONC,
13 184-5-2 MS
100397
TRIAHfiK
10/04/97
00:54 DKH
s
CONC
14 184-5-2 NSD
100397
TRIAMGL2
10/04/97
00:5B DKH
s
CONC
15 184-5-2 PDS
100397
TRWNGL2
10/04/97
01:03 DKH
s
CONC
16 184-5-2 L
100397
/RIANG12
10/04/97
01:08 DKH
s
CONC
17 CHECK 9972
100397 /
TRIANGL2
10/04/97
01:13 DKH
s
CONC
18 ICV/CCV
100397
TRIANGL2
10/04/97
01:18 DKH
Q
CONC
19 IC8/CC8
100397
TRIAHGL2
10/04/97
01:23 DKH
9
CONC
20 ICSA8
.mm
TRIANGL2
10/04/97
01:28 DKH
9
CONC
21 43182 MB
/100397
TRIANGL2
10/04/97
01:39 DKH
S
CONC
22 43182 ICS >
/ 100397
TRIAHGL2
10/04/97
01:44 DKH
S
CONC
23 182-53-1,3 /
100397
TRIAHG12
10/04/97
01:48 DKH
8
CONC
24 182-53-1,3 W
100397
TRIANGL2
10/04/97
01:53 OKH
S
CONC
25 182-53-1,3 /
100397
TRIANGL2
10/04/97
01:58 DKH
S
CONC
26 182-53-2,5/
100397
TRIANGL2
10/04/97
02:03 DKH
s
CONC
27 182-53-2/3 DA
100397
TRIAHGL2
10/04/97
02:07 DKH
s
CONC
28 icv/ccy
100397
TRIAHGL2
10/04/97
02:14 DKH
Q
CONC
29 ICV/JJCT
100397
TRIANGL2
10/04/97
02:19 DKH
8
CONC
30 IC87CC8
100397
TRIANGL2
10/04/97
02:25 DKH
0
CONC
31 ZCB/CC8
100397
TRIANGL2
10/04/97
02:30 DKH
0
CONC
32%sir~
100397
IHlriNyL2'HJ7V4/ir
-0213o OCT
8—
—
33 STD1-8LANX
100397
TRIANGL2 10/03/97
19:12
X
IR
34 STD3
100397
TRIANGL2 10^03/97
19:16
X
IR
35 ST03
100397
TRIANGL2 10/03/97
19:21 DKH
9
CONC
36 CHECK LO
100397
TRIAKGL2 10/03/97
19:27 DKH
Q
CONC
57 ICV/CCV
100397
TRIAN6L2 10/03/97
19:31 DKH
Q
CONC
1AATHI
TftTAHf! 1*-
(i
—GWK
all ilU/UtU —
iU/V\3/ 7 <
39 IC8/CC8
100397
TRIAHG12
10/03/97
19:42 DKH
8
CONC
40 ICSA8
100397
TRIAHGL2
10/03/97
19:47 DKH
8
CONC
41 43159A H8
100397
TRIANGL2
10/03/97
20:03 DKH
S
CONC
42 43159A ICS
100397
TRIAHGL2
10/03/97
20:07 DKH
S
CONC
43 182-30-1A8
100397
TRIANGL2
10/03/97
20:12 DKH
S
CONC
44 182-30-1A8 POS
10039?
TRIANGL2
10/03/97
20:17 OKH
s
CONC
45 182-30-1A8 L
100397
TRIAHGL2
10/03/97
20:21 DKH
s
CONC
46 182-30-2A8
100397
TRIAHG12
10/03/97
20:26 DKH
s
CONC
47 182-30-2A8 M
100397
TRIAHGL2
10/03/97
20:31 DKH
s
CONC
48 182-30-3A8
100397
TRIANG12
10/03/97
20:35 DKH
s
CONC
49 182-30-4AB
100397
TRIANGL2
10/03/97
20:40 OKH
s
CONC '
50 182-30-5A8
100397
TRIANGL2
10/03/97
20:45 DKH
s
CONC
51 ICV/CCV
100397
TRIANGL2
10/03/97
21:24 DKH
8
CONC
52 ICB/CCB
100397
TRIAHGL2
10/03/97
21:31 DKH
0
COHC
53 182-30-6A8
100397
TRIANG12
10/03/97
21:39 DKH
s
CONC
ij:
r tV,, fftn •
,
-------
Analysis Report Suanary • Sun 10-05-97 06:55J1 Prt page
"» Saaple Naue File Method Date Tiae OpIO Type Node
78 IC6/CCB
79 182-30-8CA
80 182-30-908
81 182-30-110
82 182-30-120
83 182-30-1380
84 182-30-148C
85 ICV/CCV
86 IC8/CC8
87 ICSA8
88 43159B N8
89 431598 LCS
90 182-30-16A
91 182-30-16A P0S
92 182-30-16A L
93 182-30-168
94 182-30-168 DA
95 182-30-16C
96 182-30-160
97 182-30-161
98 1CV/C6¥
99 ICV/CCV
00 ICV/CCV
01 IC8/CC8
02 ICSA8
54 182-30-7A8 100397 TRIANGL2 10/03/97
55 182-30-8A8 100397 TRIANGL2 10/03/97
56 182-30-9W.~. 100397 TRIANGL2 10/03/97
57 182-30-ilflB • 100397 TRIAHGL2 10/03/97
58 182-30-12AB 100397 TRIANSL2 10/03/97
59 182-30-13A8 100397 TRIANGL2 10/03/97
60 182-30-14A8 100397 TRIANGL2 10/03/97
61 182-30-151 100397 TRIANGL2 10/03/97
62-182-30-15C 100397 T8IANGL2 10/03/97
63 ICV/CCV 100397 TRIANGL2 10/03/97
wmi—mm.zMfstfrr
65 ICB/CCB 100397 TRIANGL2 10/03/97
66 182-30-1C 100397 TRIAKGL2 10/03/97
67 182-30-1C P0S 100397 TRIANG12 10/03/97
68 182-30-1C L 100397 TRIAN6L2 10/03/97
69 182-30-2C 100397 TRIANGL2 10/03/97
70 182-30-20 OA • 100397 TRIAN6L2 10/03/97
71 182-30-3C 100397 TRIANGL2 10/03/97
72 182-58-1 100397 TRIANGL2 10/03/97
73 182-58-2 100397 TRIANGL2 10/03/97
74 182-58-3 100397 TRIANGL2 10/03/97
75 182-30-78 100397 TRIANGL2 10/03/97
76 ICV/CCV 100397 TRIANGL2 10/03/97
7 7 iw?7—TniAiici; 10/03/97-
DKH
DKH
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
TRIANGL2
TRIANGL2
TRIANG12
TRIANGL2
TRIAHGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANGL2
TRIANG12
TRIANGL2
TRIAHGL2
TRIAHGL2
TRIAHGL2
TRIANGL2
TRIANGL2
-WiMSfcJ
21:44
21:49
21:53
21:58
22:03
22:07
22:12 DKH S
22:17 DKH S
22 :"21
22:26
¦72732"
DKH S
DKH S
OKH
DKH
10/03/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
10/04/97
¦H/W/W-
22:48
22:54
22:59
23:03
23:08
23:13
23:17
23:22
23:27
23:31
23:36
23:41
15r?T
23:57
00:04
00:09
00:13
00:18
00:23
00:27
00:44
00:49
00:55
01:09
01:14
01:19
01:23
01:28
01:33
01:37
01:42
01:47
01:51
¦«h5fr-
OKH Q
OKH S
DKH S
DKH S
DKH S
DKH S
OKH S
OKH S
DKH S
DKH S
DKH Q
DKH Q
DKH Q
DKH S
DKH S
DKH S
DKH S
DKH S
OKH S
DKH Q
DKH Q
DKH 0
OKH S
DKH S
DKH S
OKH S
DKH S
DKH S
DKH S
OKH S
DKH S
OKH S
WM-
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-------
Analysis Re do r t
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Summary
File
Hon 10-06-97 02:41:46 AM page 1
Method Date Tine OdIO Type Mode
1 STD1-31ANK
100597
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20:39
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100597
TRIANGL2 10/05/97
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TRIANGL2 10/05/97
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13 183-59-1 0
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14 183-59-2A-C
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TRIANGL2 10/05/97
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15 183-59-3
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TRIANGL2 10/05/97
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s
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16 183-59-3 MS
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TRIANGL2 10/05/97
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s
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17 183-59-3 MSD
100597
TRIANGL2 10/05/97
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18 183-59-3 PDS
100597
TRIANGL2 10/05/97
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19 183-59-3 L
100597
TRIANGL2 10/05/97
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20 ICV/CCV
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0
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100597
TRIANGL2 10/05/97
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3
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22 43287A flB
100597
TRIAHGL2 10/05/97
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23 432S7E MB
100597
TRIANGL2 10/05/97
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24 43287E LCS
100597
TRIANGL2 10/06/97
00:00
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s
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25 183-59-iA
100597
TRIANGL2 10/06/97
00:04
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s
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26 183-59-4A 0
100597
TRIANGL2 10/06/97
00:09
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s
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27 183-59-4A MS
100597
TRIANGL2 10/06/97
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DKH
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28 183-59-4A MS0
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TRIANGL2 10/06/97
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29 183-59-4A PDS
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TRIANGL2 10/06/97
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0
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35 ICSA3
100597
TRIANGL2 10/06/97
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DKH
3
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36 182-30-4A3 X10
100597
TRIANGL2 10/06/97
01:52
DKH
S
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37 182-30-5AB X10
100597
TRIANGL2 10/06/97
01:56
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S
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38 182-30-6A8 X10
100597
TRIANGL2 10/06/97
02:01
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s
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39 ICV/CCV
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TRIAN6L2 10/06/97
02:10
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TRIANGL2 10/06/97
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S
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41 ICSA8
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-------
PAGE 1 OF.J
ICJOVrH'
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TRIANGLE LABORATORIES, INC.
Sample Preparation Tracking & Management Form
Client: Eastern Research Group (ERG02)
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PAGE 2 OF
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PAGE 3 OF y1 „
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PAGE 4 CFj/
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TRIANGLE LABORATORIES, INC. I
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PAGE 5 OF Jo
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PAGE 6 OF /
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PAGE 7 OF i
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Client: Eastern Research Group (ERG02)
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PAGE 8 OF
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Sample Preparation Tracking & Management Form
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qa\forms\hgspke.log (08/22/96)
ill
-------
PAGE (Q 5
MERCURY SPIKE LOG
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD U
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PP8)
INITIALS
WITNESS
<$91
-US4
5
5
tsa-36'lg W5
- J/i m">D
r
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4
4
\
»
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»
-
;
•
•
qa\forms\hgspke.log (08/22/96)
112
-------
MERCURY SPIKE LOG
PAGE Idlp
DATE
PROJECT #
SAMPLE IDs
ORIGINAL
SPIKE
CONC. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
_ FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PPB)
initials
WITNESS
Voam us'd
0-
h-bWi,
5
"5
USE
IfMi-/ 6mJ>
in #n$f>
m-m-ar m*>D
1
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m -<13-3 cms
/^a, -e£
>
UrliS^ Lcstb
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3-5/^4
S"
5"
1)51-
tg=2-so-7«i> /Hi'
15" 7,-3.') - 7 Si) AfJj)
1
/
1
^3Z7|
\
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[ g"J— *fi-~ 5~C a^j
rc /^so
- 4-3 - 7C- /MJ
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y
4 .
S
1/
\k
»
«
»
-
-
-
qa\f0rms\hg5pKa.log (08/22/96)
113
-------
iutoSaioler Reoort Table: HA448
Sun 10-05-97 06:58:28 PM page 1
able Nase: HA448 Autosaspler Type: TYPE TJA
ample Positions: 146/192 QC Positions: 13/19 t Sets: 2
inse Station location is rack -1, pos. -1.
— Racks —
ack it Type*"
Usage
»Pos Left
Analyses/Pos
1 Aux. (L) Rack
STD/QC/BLANK
13
10
2 Sample (16ns)
Samples
2 '
1
3 Saaple (I6mis)
Samples
48
1
4. Sasple (16am)
Samples
- 48
1
5 Sasple (I6nm)
Samples
48
1
-- Saaple Sets —
st# Type Prepare?
Description
Method
IPos
Rackfr StartPos
1 Normal No
2 Normal No
-- Preparation Info —
"43159^1^
431598
TRIANGL2
TRIANGL2
36
10
2 1
2 37
its Uptake Uptake#2 Final
Oil.Factor
) Samples Prepared.
ick ill
>s Row
Col
Sample Name
Set i
SUsed
Type
1 1
1
STD3
-NA-
2
Standard !~
2 1
2
STD1-BLANX
-NA-
1
Standard
3 1
3
ICSA8
-NA-
3
QC Standard
4 1
4
CHECK LO
-NA-
1
QC Standard
5 1
5
ICV/CCV
-NA-
6
QC Standard
6 1
6
IC8/CC8
-NA-
6
QC Standard
'...19
Not
Used)
»
ck 82
s Ron
Col
Sample Name
Set 5
{Used
Type
1 1
1
43159A 118
1
-Hft-
Sasple
2 1
2
43159A ICS
1
-NA-
Sasple
3 1
3
182-30-1A8
1
-NA-
Saaple
4 1
4
*182-30-1A8 POS
1"
-NA-
Sasple
5 1
5
'182-30-1AB L
1
-NA-
Sasple
6 1
6
~182-30-2A8
1
-NA-
Sasple
7 1
7
•182-30-2AB OA
1
-NA-
Sasple
8 1
8
'182-30-3A8
1
-NA-
Sasple
9 1
9
"182-30-4A8
1
-NA-
Sasple
0 1
10
-182-30-5AB
1
-NA-
Sasple
1 1
11
—182-30-6AB
1
-NA-
Saaple
2 1
12
'182-30-7AB
1
-NA-
Sasple
3 2
1
182-30-8AB,«ck
-NA-
Sasple
4 2
2
*182-30-9AB
1
-NA-
Sasple
Co
VnA ^ S^PUj>
c c.
ft*5*"1-
O&A
u/t/V
(fM
lo| *\\1
C I#* OouV iiF
0 r tU V(t,uV if
* «• ttv»A fc£>
V .• } . T... L . r &
-------
jtoSaipler Report Table: HA448 ' Sun 10*05-97 06:58:28 PM page 2
ick 12
3S
Rox
Col
Sample Name
15
2
- 3
*182-30-1^8
16
2
4
' 182-30-12AB '
17
2
-fVl82-30-13AB
18
2
6
f 182-30-14AB
19
2
7
182-30-15B
20
2
8
182-30-15C
21
2
9
182-30-1C
22.
2
10
182-30—iC COS
23
2
11
182-30-1C L
24
2
12
182-30-2C
25
3
1
182-30-2C DA
26
3
2
182-30-3C
27
3-
3
182-58-1
28
3
4
182-58-2
29
3
5
182-58-3
30
3
6
182-30-78 »
31
3
7
182-30-8CA
32
3
8
182-30-908
33
3
9
182-30-110
34
3
10
182-30-120
35
3
11
182-30-13$)
36
3
12
182-30-148C
37
4
1
431598 MB
38
4
2
43159B LCS
39
4
3
182-30-16A
to
4
4
182-30-166 PDS
41
4
5
182-30-16ft L
42
4
6
182-30-16B
43
4
7
182-30-16B OA
44
4
8
182-30-160
45
4
9
182-30-160
46
4
10
182-30-16£
'47.
..48
Not Used)
ack S3
OS
Ron
Col
Saiple Name
J-
.48
Hot Used)
ack *4
OS
Ron
Col
Saaple Name
Set i
lUsed
Type
-Hfl-
Saaple
-Hfl-
Sample
-NA-
Saiple
-HA-
Saaple
-NA-
Saaple
-NA-
Saaple
-NA-
Saiple
-NA-
Saiple
-NA-
Sasple
-HA-
Saaple
-NA-
Saaple
-HA-
Saiple
-KA-
Saiple
-NA-
Sasple
-NA-
Saaple
-NA-
Saaple
-NA-
.Sasple
~NA-
Saaple
-NA-
Sasple
-NA-
Saaple
-HA-
Saiple
-NA-
Sa»ple
-NA-
Saiple
-NA-
Saiple
-HA-
Sample
-NA-
Sample
-NA-
Saaple
-NA-
Saaple
-NA-
Saaple
-HA-
Saiple
-NA-
Saaple
-HA-
\
Saiple
iUsed
Type
Set it lUsed Type
1...48 Not Used)
^ Q ^ V i v*^i if
-------
tandardization Rot. ' Fri 10-03-97 07:16*41 PH page 1
ethod:
TRIANSL2
Standard: STDl-
•BLANK
Ele#
Ag3280
A13082
AS1890
8_2496
8a4934
8e3130
Ga3179
Avge
.0000
.0029
-.0004
.0751
.0006
.0002
.0005
SDev •
.0001
.0000
.0001
.0015
.0000
.0000
.0000
IRSD
2t£T'
.7839
18.23
2.007
.2751
1.797
3.527
11
-.0000
.0029
-.0003
.0748
.0006
.0002
.0005
12
-.0000
.0028
-.0004
.0767
.0006 •
.0002
.0005
13
.0001
.0028
-.0004
.0737
.0006
.0002
.0005
Elem
Cd2265
Ce4186
C02286
Cr2677
CU3247
Fe2714
X 7664
Avge
-.0001
-.0000
-.0002
-.0001
.0028
.0001
3.937
5Dev
.0001
.0001
.0000
.0000
.0000
.0000
.030
tRSD
79.87
260.4
26.15
21.81
1.255
52.99
. 7726
11
-.0001
.0000
-.0002
-.0002
.0029
.0000
3.904
>2
-.0001
-.0001
-.0002
-.0001
.0028 "
.0001
3.944
13
-.0002
.0000
-.0001
-.0001
.0028
.0001
3.964
•lei
U6707
Hg2790
Hn2576
HO2Q20
Na3302
NI2316
PJ149
Wge
.0729
.0001
.0000
.0000
.0035
-.0022
-.0010
SQsv
.0006
.0000
.0000
.0000
.0021
.0002
.0000
;RSD
.7489
52.54
20.63
141.9
59.46
8.802
2.941
11
.0723
.0000
.0000
.0000
.0035
-.0022
-.0010
f2
.0730
.0001
.0000
.0001
.0015
-.0023
-.0011
13
.0733
.0001
.0000
.0000
.0057
-.0019
-.0011
;iei
2203-1
2203-2
Sb2068
1960-1
1960-2
Snl899
Sr4215
Ivae
.0011
.0001
.0005
-.0063
.0025
-.0006
.0003
IDev
.0001
.0001
.0001
.0010
.0001
.0001
.0000
IfiSO
10.19
53.72
26.48
15.31
1.846
8.818
3.762
ll
.0011
.0000
.0005
-.0073
.0025
-.0007
.0003
12
.0012
.0001
.0004
-.0060
.0026
-.0007
.0003
13
.0010
.0001
.0007
-.0055,
.0025
-.0006
.0003
'.leu
Ti3349
T11908
V.2924
Zn2062
Si2881
ivae
.0001
-.0005
-.0005
-.0000
.0659
IDev
.0001
.0000
.0000
.0000
.0086
iRSD
81.06
6.313
3.126
76.41
13.13
ll
.0000
-.0005
-.0005
-.0000
.0626
2
.0001
-.0005
-.0005
-.0000
.0757
13
.0002
-.0005
-.0005
-.0000
.0594
-------
Standardization Rpt.
Fri 10-03-97 07:16:41 PM page 2
IntStd 1
Bode *Counts
Elea Y
Wavier 371.030
fivge 2Sm-
SDev 605,2008
«SD .2352981
#1
256522
15000
12
257424
15000
13
257672
15000
11?
2 3 4 5 6 7
Tiae NOTUSED HOTUSED NOTUSED NOTUSED HOTUSED
15000
.0000000
.0000000
-------
Standardization Rot.
lethod:
TRIANGL2
.Standard: STD3
ilea
Aa3280
A13082
AS1890
Avge
.4165
.0190
.0538
SOev •
.0016
.0001
• .0001
MSP
.7924
.2500
11
.4182
.0191
.0539
12
.4161
.0189
.0536
13
.4152
.0188
.0538
Eleii
Cd2265
CI4186
C02286
Avge
.9615
.1174
.1082
SOev
.0014
.0002
.0001
wso
.1473
.1790
.1108
11.
.9610
.1172
.1082
«2
.9604
.1176
.1081
13
.9631
.1173
.1083
Ilea
Li6707
Mg2790
Hn2576
Avge
16.68
.0*210
.1344
SDev
.05
.0001
.0000
IRSD
.2788
.2669
.0234
11
16.73
.0211
.1344
12
16.66
.0210
.1344
13
16.64
.0210
.1343
Elem
2203-1
2203-2
S62068
flvai
.1888
.0926
.1259
SOev
.0005
.0005
.0002
WSO
.2779
.5302
.1943
il
.1893
.0922
.1259
12
.1883
.0926
.1256
13
.1889
.0931
.1261
Eles
Ti3349
T11908
V.2924
Avge
1.166
.0330
.0400
SDev
.001
.0005
.0000
IRSD
.0463
1.413
.0149
11
1.166
.0325
.0400
12
1.166
.0330
.0400
13
1.165
.0334
.0400
Fri 10-03-97 07:21123 PH page 1
6_2496
.2380
.0025
1.066
.2404
.2384
.2353
8a4934
.3054
.0003
.0883
.3057
.3054
.3052
Be3130
.2657
.0002
.0756
.2655
.2659
.2658
Ca3179
.0232
.0000
.0409
.0232
.0232
.0232
Cr2677
.1525
.0000
.0111
.1525
.1526
.1525
HO202Q
.0822
.0001
.1471
,0821
.0823
.0823
Cu3247
.1890
.0007
.3781
.1898
.1888 •
.1884
Na3302
.2387
.0033
1.389
.2413
.2399
• .2350
Fe2714
.0043
.0000
.1410
.0043
.0043
.0044
Ni2316
.3637
.0004
.1040
.3633
.3641
.3636
K.7664
23.97
.07
.2121
24.03
23.97
23.90
P.2149
.0223
.0001
.6789
.0222
.0225
.0224
1960-1
.2829
.0008
.2638
.2824
.2838
.2825 t
Zn2062
.1025
.0001
.1424
1960-2
.1667
.0002
.1450
.1666
.1665
.1670
Si 2881
.5193
.0032
.6075
Snl899
.1229
.0006
.4856
.1223
.1232
.1234
Sr4215
.8782
.0021
.2389
.8803
.8781
.8761
.1023 .5157
.1025 .5216
.1026 .5207
-------
Standardization Rpt.
Fri 10-03-97 07:21:23 Pfl
page 2
IntStd
1
2 3
4
5
6
7 -
'Mode
^Counts
Tine NOTUSED
NOTUSED
NOTUSED
NOTUSED
NOTUSED
Elei
Y-
—
—
—
—
May 1 en-
371.030
—
..
—
—
—
flvge
2mm-
15000
—
—
—
"
SDev
998.1509
.0000000 -
—
--
—
%RSD
.3896161
.0000000 -
—
—
—
—
tl
255041
15000
—
—
--
—
12
256667
15000
—
..
--
—
13
256857
15000
--
—
—
"
119
-------
nalysis Report' Averages . Sun 10-05-97 06:31:„45 PH page 1
ethod: TRIANGL2 Sample Nane: ST03 Operator: DKH
un Tiae: 10/03/97 19:21 Filename: 100397
ode: C0HC Type: Q Corr. factor: 1.00000
ab ID,: Cust. Sipl. ID.: Cust. ID..: 43159ft
less
Ag328G
A13082
AS1890
8_2496
8a4934
8e3130
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
993.3
995.1
1003.
0941.3
995.5
$90.9
Dev
1.433
8.224
4.354
11.38
.6488
4.435
RSO
.1443
..8265
".4342
1.709
.0652
.4476
le«s
Ca3179
Cd2265
Ge4186
Co2286
Cr2677
Cu3247
nits
ppb
ppb
ppb
ppb
ppb
ppb
i/ae
994.0
996.0
998.0
995.2
993.6
994.0
Dev
4.264
5.474"
1.085
3.117
3.595-
3.698
RSD
.429
.5497
.1087
.3132
.3618
.372
lens
Fe2714
K_7664
Li6707
Ha2790
Mn2576
Ho2020
nts
ppb
DOi
ppb
pob
ppb
ppb
i/ge
991.3
9.996
1003.
991.8
993.3
996.9
)ev
2.797
.0473
6.717
1.452
2.997
2.934
RSD
.2821
.4735
.67
.1464
.3017
.2943
teas
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
lits
pp»
ppb
Ppb
ppb
ppb
ppb
/ge
9.982
994.9
992.0
994.3
995.8
996.6
)ev
.1187
3.388
8.847
.3084
4.006
2.815
!SD
1.189
.3405
.8919
.031
.4023
.2825
lens
1960-1
1960-2
Pb2203
Sel96Q
Snl899
Sr4215
lits
ppb
ppb
ppb
ppb
ppb
ppb
;ge
998.0
995.1
995.3
996.1
994.0
987.8
)ev
1.11
2.618
2.687
1.548
6.559
.1926
U
.1112
.2631
.27
.1554
.6599
.0195
,e«s
Ti3349
T11908
V_2924
2n2062
*Si2SSl
lits
ppb
ppb
ppb
ppb
ppb
f§e
991.2
1004.
993.8
997.4
9803.
lev
1.98
9.415
2.7S8
7.286
50.66
ISD
.199?
.9377
.2776
.7305
.5168
121
-------
Analysis Report Averages
Sun 10-05-97 06:31:45 Pil page 3
lethod: TRIANGL2 Saaple Naie: ICV/CCV
Jun Tine: 10/03/97 19:31 Filename: 100397
Operator: OKH
Hode: COHC
Lab ID.:
Type: Q
Cust. S«pl. ID.
Corr. Factor: 1.00000
: Cust. ID.: 431-59A
Eleas
Units
Rvge
SDev
SRSO
Ag3280
ppb
500.6
.7135
.1425
A13082
ppb
496.8
5.225
1.052-
AS1890
ppb
508.7
2,859
.5621
B_2496
ppb
372.8
3,999
1.073
8a4934 8e3130
ppb ppb
496.4 494.1
.5362 1.251
.108 .2532 -
leas
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
Wge
498.1
499.1
495.2
497.1
497.1
496.8
SDev
.166
.6293
.3062
.7871
.3704
1.25
IRSD
.0333
.1261
.0618
.1583
.0745
.2515
[leas
Fe2714
K_7664
Li6707
, Hg2790
Mn2576
HO2020
Jnits
ppb
ppll
ppb
ppb
ppb
ppb
5vge
494.8
4.969
478.4
499.8
496.4
497.1
pev
2.083
.0268
2.839
4.109
.8808
2.648
sRSD
.421
.5391
.5934
.8221
.1774
.5326
tlems
Na33G2
NJ2316
P.2149
2203-1
2203-2
Sb2068
Units
PP»
ppb
ppb
PPb
ppb
ppb
!vge
4.380
497.3
499.0
496.1
497.0
499.7
SDev
.0967
1.004
1.89
2.495
2.307
1.26
Irsd
1.982
.2018
.3788
.5029
.4643
.2521
;leos
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
(nits
ppb
pcb
ppb
ppb
opb
ppb
tage
504.9
501.0
496.7
502.3
497.5
491.8
!Dev
1.422
3.098
2.04
2.121
,387
.5338
SRSD
.2817
.6184
.4108
.4223
.0778
.1085
;le»S
Ti3349
T11908
V.2924
Zn2062
#Si2881
Jnits
ppb
ppb
ppb
ppb
ppb
tvge
493.3
499.2
496.6
500.4
4531.
!Dev
.6856
6.088
.9402
,9849
2.608
iRSD
.139
1.22
.1893
.1968
.0576
i
-------
nalysi's Report Averages
Sun 10-05-97 06:31:45 PN page 4
ethod: TRIANGL2 Saiple Haie: IC8/CC8
un Time: 10/03/97 19:36 Filenaae: 100397
ode: CONC Type: 0 Corr. Factor:
ab ID.: Cust. S»pl. ID.: Gust,
Operator: DKH
1.00000
ID.: 43159A
' " -
leas
Ag3280
A13082
AS1890
8_2496
Ba4934
Be3130
tits
ppb
ppb
ppb
ppb
PPb
PPb
iqs
.3970
3.804
2.106
-174.4
J7^-
)ev
.4694
3.287
.506
"~J36
.1936
ISO
118.2
86.41 -
4.541
28.52
41.26 /
'.ess
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
lits
ppb
ppb
ppb
ppb
PPb
iDO
ige
.4077
.4750
.3311
.2977
.6685/
.5055
>ev
.4544
.1616
1.346
.2913
.09l/
.4446
1SD
111.5
34.03
406.5
97.84
1/71
87.97
e»s
Fe2714
X.7664
Li6707
«g279ft/
Nn2576
HO2020
its
ppb •
ppa
ppb
ppb/
ppb
ppb
ge
-1.705
.0111
.4711
JK 094
.4808
1.222
ev
3.795
.0067
•132
/l. 858
.1394
.9819
SD
222.6
60.83
28.0l/
169.8
28.99
80.36
ess
Na33Q2
Ni2316
p/l49
2203-1
2203-2
Sb2068
its
ppa
ppb
/Ppb
ppb
ppb
ppb
ge
.0265
.891JK
4.636
-.7727
.7222
-1.855
5V
.0376
.153/
4.307
1.948
1.634
.7767
30
142.3
im
92.91
252.1
226.3
41.86
5ms
1960-1 /
1960-2
Pb2203
Sel960
Snl899
Sr4215
its
ppb /
ppb
ppb
ppb
ppb
ppb
}8
-.0893
-.9047
.2244
-.6332
.6275
.4652
iV
4.299
1.73
.8502
1.075
L319_
.1491
>D
481V
191.2
370^
210.1
32.04
ms
Ti3349
T11908
V_2924
Zn2062
,Si2881
ts
ppb
ppb
PPb
ppb
ppb
ie
.4958
Q6.632
.5560
.7527
0-643.3
V
.0882
2.976
.4338
.1977
4.375
:0
17.8
44.87
78.02
26.27
.6801
122
-------
nalysis Report Averages • Sun 10-05-97 06:3*1:45 PH page 5
ethod: TRIAH612 Saiple Name: IC8/CC8 Operator: DKH
kit Tiie: 10/03/97 19:42 Filename: 100397
pde: CONC Type: Q Corr, Factor: 1.00000
ab ID,: Oust. S»pl. ID.: Oust, ID.: 43159ft
teis
Ag3280
A13082
Asl890
8_2496
8a4934
Be3130
its
ppb
ppb
ppb
ppb
ppb
ppb
ge
.0708
6.587
,7789
-228.6
.1052
-.1007
ev
.0299
.1853
1.674
2.594
.0338
.0512
iSD
42,27
2.814
215
1.134
32,18
50.84
e#s
Ca3179
Cd2265
C84186
Co2286
Cr2677
Cu3247
lits
PPb
ppb
ppb
ppb
ppb
ppb
p
-.8309
.0160
-.2282
-.1451
.1157
-.0447
BV
.4382
.0054
1.336
.2897
.0679
.1732
SD
52.74
33.61
585.5
199.7
58.74
387,2
ps
Fe2714
K_7664
Li6707
Hq2790
Mn2576
HO202Q
its
ppb
ppo
ppb
ppb
ppb
ppb
ge
-4.621
-.0213
.0723
2.010
.1040
-.1275
[v
6.075
.018
.0106
5.191
.0572
.1436
So
131.5
84.58
14,7
258.3
54.97
112.7
ms
Na3302
Ni2316
P_2149
2203-1
2203-2
Sb2068
ts
pp»
ppb
ppb
ppb
ppb
ppb
e
.0331
.6446
-.6361
-.4386
.0645
-2.196
}V
.0624
.2068
4,803
1.132
1.217
1.314
P
188.8
32.08
755.1
258.2
1886
59.84
!iS
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
Its
ppb
ppb
ppb
ppb
ppb
ppb
E
-.4869
-1.302
-.1030
-1.031
.7219
.0976
V
2.908
1.04
.5671
1.162
.6405
.033
f
597.2
79.9
550.5
112.8
88.72
33.79
1
IS
113349
T11908
V.2924
In2062
#Si2881
ts
ppb
ppb
ppb
ppb
'ppb
.0580
2.641
.0772
.1149
8-660.3
1
.0282
2.089
.2254
.2657
21.38
)
48.56
79.09
292
231.2
3.237
-------
lalysis Report Averages \ _ Sun 10-05-97 06:31:45 PH page 6
thod: TRIANGL2 Sanple Hate: ICSAB Operator: DKH
n Tiae: 10/03/97 19:47 Filename: 100397
de: CONC Type: Q Corr. Factor: 1.00000
b 10.: - Oust. Sipl. ID.: Cust. ID.: 43159ft
2as , Ag3280 A13082 Asl890 8_2496 8a4934 8e3130
its ppb ppb ppb ppb ppb ppb
38 538.5 504600. 529.6 341.3 515.7 484.6
3 V
1.186
1694
2.156
7.962
.7927
2.881
.2203
.3357-
,407
2.333
.1537
.5945
ins
Ca3179
Cd2265
Ce4186
C02286
Cr2677
Cu3247
its
ppb
ppb
ppb
ppb
ppb
ppb
18
454300.
473.3
497.7
469.6
475.2
542.5
!V
-2751
2.802
2.122
_2.289
2.929
1.23
SO
,6056
,5922-
.4262
.4874
.6163
.2267
is
Fe2714
K.7664
U6707
Hg2790
Hn2576
No2020
ts
ppb
pp#
ppb
ppb
ppb
• ppb
e
175000.
025.43
626.7
533800.
454.8
495.3
V
S40.6
.1016
2.697
1586
2.613
5.314
D
.4803
.3994
.4304
.2971
,5744
1.073
HIS
Na3302
N12316
P_2149
2203-1
2203-2
Sb2068
ts
ppm
ppb
ppb
ppb
ppb
ppb
e
5,568
451.6
551.9
494.5
478.0
514.1
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PH page 7
3thod: TRIAHSL2 Saiple Naae: 43159A MB Operator: DKH
in Tiee: lff/03/97 20:03 Filename: 100397
ide: CONC Type: S Corr. Factor: 1.00000
ib ID.: Cust. Snpl. ID.: Oust. 10.: 43159ft
J«S
AS1890
8e3130
Cd2265
C02286
Cr2677
Hn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
|ge
L.9367
L.0700
L-.1132
L-.1859
L.4245
L-.5921
1.529
.0285
.1007
.2647
.0894
.0191
SO
163.3
40.69
88.94
142.3
21.05
3.227
Los
Ni2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ae
6.549
11.447
L.4592
t-.1855
r
pv
.5062
.8155
.5624
.9038
50
7.73
56.36
122.5
487.2
-------
alysis Report Averages
Sun 10-05-97 06:3*1:45 PN page 8
thod: TRIAMGL2 Sample Naae: 43159A ICS Operator: DKH
n Tise: 10/03/97 20:07 filename; 100397
de:_C0HC Type: S Corr. Factor: 1.00000
b 10.: Cust. Stpl. ID.: Oust.- ID.: 43159ft
MS
Asl890
8e3130
Cd2265
Co2286
Cr2677
Mn2576
its
ppb
ppb
ppb
ppb
ppb
PPb
ie
51.03
47.36
49.24
49.32
49.55
49.56
!V
2.39
.2379
.3677
.6787
.2296
.2417
D
4.684
.5023
.7467
1.376
.4633 -
.4876
as
NI2316
Pb2203
Sb2068
Sel960
ts
ppb
ppb
PPb
ppb
e
56.73
50.52
48.63
48.82
V
.576
.4173
.3383
.3918
¦
D
1.015
.8261
.6957
.8025
-------
Analysis Report Averages
Sun 10-05-97 06:31:45 PH page 9
0-
lethod: TRIANG12 Saipls Haie: 182-30-Ab ^Operator: OKH
lun Tiie: 10/03/97 20:12 Filename: 100397"
(ode: CONC Type: S Corr. factor: 1.00000
.ab 10.: Oust. Sapl. ID.: Oust. ID.: 43159ft
.less
ftsl890
8e3130
Cd2265
Co2286
Cr2677
Mn2576
In its
ppb
ppb
ppb
ppb
ppb
ppb
Ne
15.05
1.0040
19.26
L-2S.79
103.6
173.1
bev
1.128
.0274
.417
.3777
.5179
.24
RSO
| "
7.497
684.3
2.165
1.464
.5001
.1386
leis
Ni2316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
ppb
PPb
W
68.33
1199.
44.60
44.64
|ev
.0224
3.377
2.04
2.449
.0328
.2817
4.575
5.486
»
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PM page 10
sthod: TRIAH612 Saaple Nate: 182-30-1^8 CDS Operator: DKH
un Tine: 10/03/9? 20:1? Filename: 100397
ode: COHC Type: S Corr. Factor: 1.00000
ab ID.: Cost. Sspl. ID.: Oust. ID.: 43159A
-J
[eras
AS1890
Be3130
Cd2265
Co2286
Cr2677
Bn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
>ge
60.32
46.22
66.29
23.37
154.0
220.6
)ev
1.16
.2802
.4352
.256
.2843
.965
ISO
1.922
.6062
.6566
1.095_
.1846
'.4375
e«s
Ni2316
Pb2203
Sb2068
Sel960
lits
ppb
ppb
ppb
ppb
-se
115.4
1231.
92.78
89.28
ev
.3889
6.978
1.558
1.61
;SD
.3371
.5669
1.679
1.804
*
-------
Analysis Report Averages
Sun 10-05-97 06:3*1:45 PM page 11
Method: TRIANGL2 Sample Na»e: 182-30-1AB L Operator: DKH
tun Tine: 10/03/97 20:21 Filenase: 100397
lode: C0NC Type: S Corr. Factor: 1.00000
Lab 10.: Cust. Sapl. 10.: Cust. ID.: 43159A
k •
• >y- -
Eless
Asl890
8e3130
Cd2265
Co2286
Cr2677
Nn2576
Inits
ppb
ppb
PPb .
ppb
ppb
ppb
Wge
L3.769
L.0756
3.854
L-5.798
26.67
25.76
!Dev
1.48
.0154
.1172
.0506
.395
.1046
»RS0 -
-
39.25 -
20.44
3.041
.8728
1.481
.2927
:iess
Ni2316
Pb2203
Sb2068
Sel960
Jnits
ppb
ppb
ppb
ppb
ivge
16.11
262.5
7.677
10.63
!Dev
.2162
1.833
2.449
1.069
tRSO
1.342 .
.6983
31.9
10.05
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PM page 12
ithod: TRIANGL2 Sample Naie: 182-30-2M Operator: OKH
In Tiae: 10/03/97 20:26 Filenaae: 100397
ide: COHC Type: S Corr. Factor: 1.00000
lb ID.: Cust. Sapl. ID.: Cust. ID.: 43159A
¦jy -
1
eas
ftsl890
883130
Cd2265
C02286
Cr2677
Nn2576
tits
ppb
ppb
ppb
ppb
ppb
ppb
ge
14.34
L.0861
2.094
L-54.74
158.3
180.9
«8V
3.274
.0229
.4574
1.362
1.497
1.234
SO
22.83
26.56
21.84
2.489
.9462
.6826
eas
Hi2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ge
115.4
1097.
85.64
80.20
ev
.4448
10.53
5.68
.3298
SO
.3853
.9596
6.632
.4113
-------
Analysis Report Averages
Sun 10-05-97 06:3*1:45 PH page 13
Si.
Method: TRIANGL2 Sample Name: 182-30-2^6 OA Operator: DKH .
kun Tiie: 10/03/97 20:31 Filenaie: 100397
Node: CQNC Type: S Corr. Factor: 1.00000
Lab ID.: Oust. S»pl. ID.: - Cust. ID.: 43159A
Eleas
AS1890
Be3130
Cd2265
Co2286
Cr2677
Hn2576
foils
ppb
ppb
ppb
ppb
ppb
ppb
jvge
15.86
L.0629
2.353
L-54.60
159.2
181.5
>Dev
2.433
.0129
.3813
1.003
.9901
.4898
iRSD
15.34
20.53
16.2
1.838
.622 -
.2699
Ileus
Ni2316
Pb2203
Sb2068
Sel960
Jnits
ppb
ppb
PPb
ppb
Ivge
115.9
1103.
85.81
82.21
IDev
.603
6.612
6.121
-1.698
SO
CO
.5202
.5994
7.133
2.065
-------
alysis Report Averages ' . Sun 10-05-97 06:31:45 PM page 14
a
thod: TRIANGL2 Saiple Naie: 182-30-3A8 Operator: DKH
n Tine: 10/03/97 20:35 fiienase: 100397
de: CONC Type: S Corr. Factor: 1.00000
b ID.: Oust. Sapl. ID.: Gust. ID.: 43159ft
3BS
AS1890
Be3l30
Cd2265
Co2286
Cr2677
Mn2576
its
ppb
ppb
ppb
PPb
ppb
ppb
JB
11.77
1.0664
1.156
1-39.13
128.1
186.2
5V
2.038
.0107
.21
.4692
1.083
.9696
SO
17.31
16.2
18.16
1.199
.8458 .
.5206
ins
Mi2316
Pb2203
Sb2068
Sel960
:ts
ppb
ppb
ppb
ppb
l«
85.06
1159.
63.69
63.61
IV
.8859
9.405
2.296
1.568
;d
1.041
.8117
3.604
2.465
*
-------
Analysis Report Averages Sun 10-05-97 06:31:45 PM page 15
Method: TRIANG12 Sample Naae: 182-30-4A8
ton Tine: 10/03/97 20:40 Filenane: 100397
lode: CONC Type: S Corr. Factor:
Lab ID.:
Cust. Smpl. IIT:
Cust.
Operator: 0KH
1.00000
10.: 43159A
El ems
Asl890
8e3130
Cd2265
C02286
Cr2677
Mn2576
Inits
PPb
ppb
ppb
ppb
ppb
ppb
Wge
218.9
L-12.10
744.7
37.10
2423.
H43330
!0ev
2.858
.1975
2.209
.4812
15.3
200.7
%RS0
"
1.306
1.632
.2967
1.297
.6314
.4631
I less
Ni2316
Pb2203
Sb2068
Sel960
Units
ppb
ppb
ppb
ppb
Ivge
431.9
HI13500.
51.99
312.0
jDev
3.288
791.2
3.33
3.792
iRSD
.7612
.6972
6.405
1.215
133
-------
»
alysis Report Overages Sun 10-05-97 06:31:45 PH page 16
J6
thod: TRIANGL2 Suple Ha»e: 182-30-5A8 Operator: OKH
1 Tiae: 10/03/97 20:45 Filenaae: 100397
ie: CONC Type: S Corr. Factor: 1.00000
) ID.: Cust. Sipl. ID.: Cust. ID.: 43159A
IBS
AS1890
8e3130
Cd2265
C02286
Cr2677
Hn2576
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
166.8
L-7.321
664.8
2.500
2027.
H35980.
V
2.779
.0351
4.395
.9524
17.67
337.7
D
1.666
.4796
.6611
38.09
.8719
.9385
OS
Ni2316
Pb2203
Sb2068
Sel960
ts
ppb
ppb
ppb
ppb
g
371.8
HI30300.
77.87
183.5
i
1.865
1453
.8269
3.945
)
.5017
1.115
1.062
2.15
-------
Analysis Report Averages
Sun 10-05-97 06:JU45 PH page 17
,Method: TRIANGL2 Sanple Nate: ICV/CCV
un Tiae: 10/03/97 21:24 Filenaae: 100397
*
Mode: CONC
j.ab ID.:
Type:
Oust.
Corr. factor:
Sfflpl. 10.:
Oust.
Operator: OKH
1.00000
10.: 43159A
——
Eleis
Af3280
A13082
AS1890
8_2496
Ia4934
8e3130
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
?vge
509.4
530.2
512.1
2536.
495.2
489.9
SDev
2.364
8.188
1.564
70.45
.2376
1.682
feRSO
.4641
1.544
,3055
2.778
.048
.3433
1
•lens
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
CU3247
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
vge
524.7
500.8
495.6
495.9
498.4
500.2
SDev
1.118
.8418
3.367
1.757
1.682
2.72
URSD
.2131
.1681
.6793
.3543
.3374
.5438
!le«s
Fe2714
K_7664
Li6707
Ng2790
Hn2576
HO2020
Jnits
ppb
ppi
ppb
ppb
ppb
ppb
Ivge
539.6
5.176
494.4
508.2
491.0
492.7
[Dev
4.476
.0729
6.665
1.746
.9999
1.315
iRSD
.8295
1.409
1.348
.3436
.2036
.2669
lens
Na3302
Ni2316
P_2149
2203-1
2203-2
S b 2 0 6 8
nits
ppin
ppb
ppb
ppb
ppb
ppb
vge
5.178
501.5
516.6
494.9
510.4
500.8
Dev
.1983
1.332
3.939
10.53
6.459
1.763
RSD
3.83
.2656
.7624
2.128
1.265
.352
¦le«s
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
[nits
ppb
ppb
ppb
ppb
ppb
PPb
ivge
508.3
505.2
505.3
506.3
489.5
489.8
.Dev
5.285
4.856
.8031
1.549
.4201
.321
KSD
1.04
.9611
.1589
.306
.0858
.0655
lens
T13349
T11908
V_2924
2n2062
»Si2881
bits
ppb
ppb
ppb
ppb
ppb
be
489.4
493.9
494.0
499.4
021310.
Dev
1.127
13.83
1.521
1.832
3563
fiSD
.2302
2.801
.3078
.3669
16.72
13o
-------
alysis Report Averages , Sun 10-05-97 06:31^45 PH page 18
thad: TRIAN612 Sa«ple Nane: IC8/CC8 Operator: DKH
n Time: 10/03/97 21:31 Filenaue: 100397
de: CONC
Type: 8
Corr. Factor:
1.00000
b 11T.i
Oust. Sipl. 10.:.
Oust.
10.: 4315$
2BS
Ag3280
A13082
As1890
8_2496
8a4934
8e3l30
its
PPb
ppb
ppb
ppb
ppb
ppb
38
.1486
27.28
1.280
1878.
.2706
".3602
JV
.2797
5.255
1.623
238.3
.1073
.1497
50
188.2
19.26
126.8
12.69
39.66
41.57
;bs
Ca3179
Cd2265
Ce4186
0O2286
Cr2677
CU3247
its
PPb
ppb
Ppb
ppb
ppb
ppb
je
-3.644
.1289
-.5031
-.0575
.7033
-.4565
iV
.3399
.0548
1.05
.0959
.0891
.518
5D
9.328
-42.49
208.7
166.7
12.67
113.5
its
Fe2714
K_7664
Li670?
Mg2790
Hn2576
HO2020
:ts
ppb
ppm
ppb
ppb
ppb
ppb
ie
-4.835
.0178
.2984
-1.411
.2543
.5901
!V
4.204
.0361
.0364
1.936
.1068
.4864
ID
86.95
203.3
12.21
137.2
42.01
82.43
IBS
Na3302
Hi2316
P.2149
2203-1
2203-2
Sb2068
ts
ppm
ppb
ppb
pob
PPb
ppb
ie
-.0057
1.316
.2764
.7651
-.8325
-.2528
V
.0811
.3908
1.696
.9715
.5993
1.29
:o
1431
29.7
613.7
127
71.99
510.3
OS
1960-1
1960-2
Pb2203
Ssl960
Snl899
Sr4215
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
3.492
-1.833
-.3005
-.0601
.7476
.2493
V
1.33
1.707
.5322
.7722
.5022
.1102
0
38.1
93.11
177.1
1286
67.18
44.21
ns
T13349
T11908
V_2924
Zn2062
»Si2881
ts
ppb
ppb
ppb
ppb
ppb
e
.1976
4.809
.5010
.3149
06410.
V
.0511
1.899
.2315
.4032
1126
D
25.85
39.5
46.2
128.1
17.56
-------
Analysis Report Averages
Sun 10-05-97 06:31:45 PM page 19
FC
•tVKrlC-CiltC
Mettled: TRIANGL2 Saiple Naae: 182-30-&B
Run Tiae: 10/03/97 21:39 Filenaae: 100397
node: CONC Type: S Corr. Factor:
Lab 10.: Cust.'Sapl. ID.:
Operator: DKH
1.00000
Cust. ID.: 43159A
Elans
Asl890
Be3130
Cd2265
C02286
Cr2677
Nn2576
Inits
PPb
ppb
ppb
ppb
ppb
ppb
}vge
167.2
L-6.455
631.7
10.38
2067.
H38270
30ev
1.79
.0817
.7905
.9523
.5973
52.44
SRSD
1.071
1.266
.1251
9.174
.0289
.137
:leas
Ni2316
Pb2203
Sb2068
Sel960
Inits
ppb
ppb
ppb
ppb
ivge
411.6
H125200.
69.57
238.2
iDev
.6746
73.8
6.493
1.954
tRSD
.1639
.059
9.334
.8203
-------
nalysis Report Averages
Sun 10-05-97 06:31 :_45 PM page 20
e.
athod: TRIANGL2 Sample Haae: 182-30-71)8 Operator: DXH
tin Tiae: 10/03/97 21:44 Filenaae: 100397
Jde: CONC Type: S Corr. Factor: 1.00000
lb ID.: Oust. Sipl. 10.: " Cust. 10.: 43159ft
lets
AS189Q
8e313Q
Cd2265
Co2286
Cr2677
Hn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
ig8
10.58
L.1588
L-7.411
1-42.61
125.6
211.2
lev
4*.
SO
GO
.0144
.1883
.068
.7733
10.41
ISO
4.711
9.056
2.541
..1597
.6156
4.929
,eis
Ni2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ge
89.24
170.3
70.27
63.84
ev
1.417
33.71
1.419
1.4 "
;S0
1.588
19.79
2.019
2.193
-------
Analysis Report Averages ' . Sun 10-05-97 06:31:45 PM page 21
Hethod: TRIANGL2 Sample Naae: lS2-30-_8fl8;»oh Qperator: OKH
jlun Ti«e: 10/03/97 21:49 Filenaie: 100397 *
Node: C0NC Type: S Corr. Factor: 1.00000
.ab ID.: Oust. Sapl. ID.: Cust. ID.: 43159A
• «
Eleis
AS1890
8e3130
Cd2265
C02286
Cr2677
Nn2576
[nits
ppb
ppb
ppb
ppb
ppb
ppb
»vge
9.535
1.1004
1-13.90
1-47.37
131.5
56.28
50ev
4.031
.0641
1.073
2.51
1.882
2.542
|RSD
42.28
63.86
7.718
5.299
1.431
4.516
¦leas
M12316
Pb2203
Sb2068
Sel960
inits
ppb
ppb
ppb
ppb
vge
84.91
1-10.34
76.30
67.56
biv
1.793
11.13
9.538
1.188
;RS0
2.112
107.7
12.5
1.759
»
-------
Analysis Report Averages
Sun 10-05-97 06:31 :„45 PM page 22
c.
Method: TRIAKGL2 Sanole Naue: 182-30-9^8 Operator: OKH
Run Tile: 10/03/97 21:53 filename: 100397
lode: C0HC Type: S _ Corr. Factor: 1.00000
Lab ID.: Cust. S«pl. 10.: Oust. ID.: 43159A
ileus
AS1890
Be3130
Cd2265
C02286
Cr2677
Mn2576
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
ivgs
9.968
L,0952
L-.0822
1-26.56
94.28
182.5
!Dev
3.877
.007
.1529
.4487
1.116
.5817
iRSO
38.89
7.305
-186.1
1.689
1.184
.3187
leas
Ni2316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
ppb
ppb
vge
70.14
256.9
45.04
40.31
-
Oev
.8167
3.042
1.36
2.289
.
RSD
1.164
1.184
3.019
5.679
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PH page 23
c,
ethod: TRIAHGL2 ..Sasple Naae: 182-30-1 Operator: DKH
pn Tine; 10/03/97 21:58 filename: 100397
ode: C0KC Type: S Corr. Factor: 1.00000
ab 10.: Cast. SipL 10.: Cust. ID.: 43159ft
lens
AS1890
Be3130
M2265
Co2286
Cr2677
Hn2576
uts
ppb
ppb
ppb
ppb
ppb
ppb
/ge
11.58
L.1275
L-10.88
L-39.35
138.5
120.7
)ev
3.119
.0434
.2811
.6677
.9102
.7549
ISO
26.94
34.03
2.584
1.697
.6572
.6253
eis
Ni23l6
Pb2203
Sb2Q68
Sel96Q
lits
ppb
ppb
ppb
ppb
ge
104.0
66.16
82.04
73.61
¦ev
.47J58
4.084
2.587
1.598
!SD
.4529
6.173
3.153
2.171
-------
Inalysis Report Averages " . Sun 10-05-97 06:3*1:45 PH page 24
e.
iethod: THIAHGL2 Saiple Hade: 182-30-12*AB Operator; OXH
!un Ti»e: 10/03/97 22:03 Filename: 100397
ode: COHC Type: S Corr. Factor: 1.00000_
ab -ID.: Cust. Sipl. 10.: Oust. 10.: 43159ft
leas
AS1890
8e3130
Cd2265
Co2286
Cr2677
Hn2576
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
11.16
L.1396
1-8.110
L-45.25
147.0
128.2
Dev
.6291
.0139
.2277
.2649
.7583
.8538
*SD
5.637
9.988
2.807
.5854
.5157
.666 .
Less
Hi2316
Pb2203
Sb2068
Sel960
lits
ppb
ppb
ppb
ppb
/ge
94.19
89.75
77.39
69.85
lev
.4699
4.11
.6045
.72
!SD
.4988
4.579
.7811
1.031
»
-------
Analysis Report Averages
Sun 10-05-97 06:31:45 PH page 25
t
Method: TRIANG12 Sample Na#e: 182-30-1&8 <^»-zl).Vite0perator: DKH
iun Time: 10/03/97 22:07 Filename: 100397
lode: COHG Type: S Corr. Factor: 1.00000
.ab 10.: Oust. Sipl. 10.: Cusl. 10.: 43159ft
lets
Asl890
Be3130
Cd2265
Co2286
Cr2677
Hn2576
nits
ppb
ppb
ppb
ppb
ppb
ppb
ivge
10.28
L.0974
L-2.334
L-41.63
128.7
106.5
Oev
.6646
.0301
.1773
.1973
.064
.5183
RSO
6.464
30.86"
7.6
-.4739
.0498
.4868
'lets
Hi2316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
ppb
ppb
vge
84.91
212.3
68.24
63.19
Oev
1.511
5.273
1.275
2.615
BSD
1.779
2.483
1.869
-4.139
143
-------
lalysis Report Averages
Sun 10-05-97 06:31:45 PM page 26
e. -
thod: TRIANGL2 Saaple Name: 182-30-14^8 Operator: DXH
n Ti«e: 10/03/97 22:12 Filename: 100397
de: CONC Type; S Corr. Factor: 1,00000
b 10.: Cust. Sapl. ID.: - Just. ID.: 43159A
SIS
Asl890
8e3130
Cd2265
Co2286
Cr2677
Hn2576
its
ppb
ppb
ppb
ppb
ppb
ppb
}e
10.29
L. 1264
1-12.34
L-50.98
143.2
34.03
JV
2.168
.0095
.2312
1.197
.1449
.0883
n
21.08
7.523
1.874
2.348
.1012
.2596
!BS
Ni2316
Pb2203
Sb206S
Sel960
ts
ppb
ppb
ppb
ppb
ie
98.80
1-14.56
85.38
77.12
V
.4249
3.415
2.687
2.084
D
.4301
23.46
3.147
2.702
144-
-------
malysis Report Averages
Sun 10-05-97 06:31:45 PM page 27
lethod: TRIANGL2 Saaple Nane: 182-30-158 Operator: OKH
|un Tiie: 10/03/97 22:17 Filename: 100397
ode: CQNC _ Type: S Corr. Factor: 1.00000
ab ID.: Cust. Sapl. ID,: Oust. ID.: 43159ft
*
lens
AS1890
Be3130
Cd2265
Co2286
Cr2677
Hn257fi
lits
ppb
ppb
ppb
ppb
ppb
ppb
*ge
L3.755
L,0742
L-.6749
L-2.167
8.115
5.123
Dev
2.362
.0111
.118
.0637
.0829
.0687
iSD
62-92
14.89 '
17.48
2.941
1.022
1.342
.ens
NI2316
Pb2203
Sb2Q68
Sel960
pits
ppb
ppb
ppb
ppb
[98
3.871
11.675
L3.960
3.009
5ev
.9014
.1933
1.582
1.375
•
*SD
23.29
11.54
39.94
45.68
*
145
-------
lalysis Report Averages ; » Sun 10-05-97 06:31.45 PH page 28
tthod: TRIANGL2 Saiple Ha»e: 182-30-15C Operator: DISH
in Tise; 10/03/9? 22:21 Filenaae: 10039?
da: CONC Type: S Corr. Factor: 1.00000
b ID.: Cust. Sapl. ID.: Oust. ID.: 43159A
eas
As 1890
8e3130
Cd2265
C02286
Cr2677
Hn2576
its
ppb
ppb
ppb
ppb
ppb
ppb
ge
5.790
1.0253
L-1.526
L-5.312
16.22
5.310
S¥
1.14
.0308
.1152
.2081
1.304
,0491
38
19.69
121.6
7.55
3.918
8.04
.9252
31S
Ni2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
J®
7.916
10.82
5.370
6.344
IV
.84?
1.641
1.97
1.293
ID
10.7
15.17
36.69
20.38
-------
inalysis Report Averages
Sun 10-05-97 06:31.45 PH page 29
lethod: TRIANGL2 Sample Nate: ICV/CCV Operator: OXH
lun Tiie: 10/03/97 22:26 Filename: 100397
(ode: C0NC Type: 0 Corr. Factor: _ 1.00000
tab 10.: Cust. Supl. ID.: Oust. ID.: 43159A
I -USF5"'
;iens Af3280 A13082 Asl890 8_2496 8a4934 8e3130
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
508.3
519.5
517.1
761.7
497.9
495.8
Oev
1.936
8.273
5.556
250.3
.4421
2.296
RSB
.3808
1.593
1.075
32.87
.0888
.4632'
lens
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
CU3247
nits
ppb
ppb
ppb
ppb
ppb
ppb
pge
501.4
504.5
500.5
498.2
508.1
498.2
Oev
.6434
1.112
1.909
1.513
1.142
1.642
RSO
.1283
.2204
.3814
.3037
.2247
.3297
less
fe2714
K_7664
Li6707
Mg2790
Hn2576
Mo2020
nits
ppb
m
ppb
ppb
ppb
ppb
517.7
4.989
475.0
499.1
494.4
497.2
Pev
5.026
.0425
3.66
2.466
1.509
2.425
RSO
.9707
.8516
.7705
.494
,3053
.4877
|eras
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
nits
ppm
ppb
ppb
ppb
ppb
ppb
/ge
4.853
507.3
518.1
482.5
506.0
506.7
bev
.1356
.5298
5.144
7.029
4.064
4.329
to
2.795
.1044
.9929
1.457
.8031
.8543
[ens
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
lits
ppb
ppb
ppb
ppb
ppb
ppb
rge
514.8
508.7
498.2
510.8
486.7
494.0
lev
1.897
1.797
.4628
1.392
3.112
.4232
[so
.3684
.3532
.0929
.2725
.6394
.0857
ens
Ti3349
T11908
V.2924
In2062
412881
jits
ppb
ppb
ppb
ppb
ppb
ige
494.5
SOI.5
498.6
504.9
8100300.
lev
.952
.8328
.9264
1.729
4713
ISO
.1925
.166
.1858
.3426
4.698
-------
lalysis Report Averages ' . Sun 10-05-97 06:31:45 PH page 30
thod: TRIANGL2 Saiple Haas: ICS/CCB ¦ Operator: OKH
n Time: 10/03/97 22:32 Filename: 100397
de: CONC Type: Q Corr. Factor: 1.00000
b ID.: " Cust. Supl. ID.: . Cust. 10.: 43159ft
ess
Ag3280
A13082
Asl890
8.2496
8a4934
8e3130
its
ppb
ppb
ppb
ppb
ppb
ppb
J8
.4700
23.78
2.090
472.7
.3960
".4810
sv
.4175
2.888
1.247
199
.1288
.1697
5D
88.83
12.14
59.67
42.1
32.53
35.27
'IBS
its
je
!V
;o
¦M
ts
e
v
D
Ca3175
M2265
JSii&r-
Uo2286
Cr2677
Cu3247
ppb
ppb
ppb
ppb
ppb
-2.619
-.0875
-.2609
-.8217
84.039
-.5347
,645
.0263
1.399 -
.1327
.8508
.2847
24.63
30.02
536.2
16.15
21.07
53^r
Fe2714
KJ664
Li6707
Hg2790
M2$iy
no2020
ppb
ppffl
ppb
ppb
PPT •
ppb
6.274
.0266
.4229
.6329
/.mi
.9741
7.322
.0211
.1064
2 Ml/
.1239
.3036
116.7
79.43
25.16
42jko
42.12
31.16
BS
ts
e
v
Na3302
PP»
.0595
.0808
135.8
Ni2316
ppb
2.998
.6021
20.08
P_2143
Wb/
.616
'2.434
36.79
2203-1
ppb
1.609
4.144
257.5
2203-2
ppb
-2.519
1.93
76.61
Sb2068
pob
2.583
1.585
61.35
SS
1960-1
1960-2
Pb2203
Sel960
Sftl899
ts
ppb /
/ppb
ppb
ppb
PPb
3
7.403
-2.946
-1.144
.5006
-2.252
/
2.6m
1.502
.3832
.2509
1.847
5
M.2
50.99
33.5
50.11
81.99
is
/ T13349
T11908
V.2924
Zn2062
•S12881
:s /
ppb
ppb
ppb
ppb
ppb
> I
.3941
85.775
1.151
Jii-
< (
.0874
—¦7 4wh6
.2421
7965
i
'¦«- jj , 1"
96.04
37.86
63.05
13.38
SN215
ppb
.3892
.1366
35.11
-------
Analysis Report Averages . Sun 10-05-97 06:31.45 PH page 31
ethod: IRIANGL2 Saiple Name: ICB/CCB Operator: OKH
uo Tiie: 10/03/97 22:48 Filename: 100397
Node: C0NC Type: Q Corr, Factor: 1.00000
iab ID.: Oust. SapL IIL: Oust. ID.: 43159A
less
Ag3280
A13082
Asl890
8_2496
Ba4934
Se3130
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
-.0430
25.21
3.202
1079.
.0110
'.1166
SDev
.1251
2.992
.715
241.4
.0571
.0201
IRSD
290.7
11.87
22.33
22.38
518.2
17.23
ileras
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
CU3247
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
-3.794
-.3224
-1.053
-.6409
1.706
-.629"
Dev
1.063
.0462
2.205
.6975
.5107
.2624
RSD
28.01
14.32
209.4
108.8
29.93
41.67
lens
Fe2714
K.7664
Li6707
Hg2790
Nn2576
Mo2020
nits
ppb
ppffl
ppb
ppb
ppb
ppb
Ivge
-2.620
.0150
.0442
-.0345
-.0656
.0055
pev
10.42
.0296
.0637
3.439
.0499
.3345
RSD
397.5
196.9
144.3
9969
76.05
6087
1
jlems
Na33Q2
Ni2316
P_2149
2203-1
2203-2
Sb2063
nits
PP®
ppb
ppb
ppb
ppb
ppb
-.0009
1.665
7.358
.5261
-1.194
.3631
)ev
.028
.3302
8.552
3.875
2.573
1.975
ISO
2960
19.84
116.2
736.5
215.5
543.8
lens
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
lits
ppb
ppb
ppb
PPb
ppb
ppb
vge
4.411
-4.804
-.6214
-1.735
-.3350
-.0028
iev
1.759
1.367
.8244
.444
1.034
.0222
b
39.88
28.45
132.7
25.58
308.6
792.4
8BS
Ti3349
T11908
V.2924
Zn2062
•Si 2881
iits
ppb
ppb
ppb
PPb
ppb
ge
-.0153
.6357
.5765
-.2530
827420.
)ev
.1261
2.908
.8509
.1168
3886
ISO
826.3
457.4
147.6
46.15
14.17
-------
lysis Report Averages
Sun 10-05-97 06:31:45 PM page 32
iOd: TRIANGL2 Saipls Naie: 182-30-1C Operator: OXH
Tiae: 10/03/97 22:54 Filename: 100397
: COHC Type: S Corr. Factor: 1.00000
ID.: Cust. Sapl. ID.: - Oust. 10.: 43159ft
s
flsl890
863130
Cd2265
C02286
Cr2677
Hn2576
s
ppb
ppb
ppb
ppb
ppb
ppb
13.81
L-.2S66
1.6051
4.594
110.8
238.2
3.001
.037
.3439
1.038
1.716
1.276
' 21.73
14.43
56.83
22.6
1.549
.5357
s
Ni2316
Pb2203
Sb2068
Sel960
s
ppb
ppb
ppb
ppb
20.12
38.59
12.902
946.6
1.66
.9481
3.519
3.281 "
8.249
2.457
121.3
.3466
»
-------
Analysis Report Averages
Sun 10-05-97 06:31 :.4S PH page 33
Sethod: TRIAHSL2 Sample Nans: 182-30-1C PDS Operator: DKH
[utt Tiae: 10/03/97 22:59 Filenaie: 100397
lode: C0NC Type: S Corr. factor: 1.00000
ab ID.: Cust. Sapl. ID.: Oust. ID.: 43159A"
:ieas
Asl890
8e3130
Cd2265
Co2286
Cr2677
Wn2576
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
63.27
48.63
49.17
53.78
158.3
285.0
Oev
1.056
.2346
.1974
.5552
.8157
1.091
RSD
1.669
.4825
.4014
1.032
.5154
.3829
le»s
Ni2316
Pb2203
Sb2068
Sel960
,nits
ppb
ppb
ppb
ppb
m
67.61
86.30
49.23
991.6
bev
.4826
1.339
2.35
3.15
RSO
.7138
1.551
4.773
.3177
I
151
-------
oalysis Report Averages " . Sun 10-05-97 06:31:45 PH page 34
ithod: TRIANG12 Sasple Nane: 182-30-1C I Operator: DKH
in Tiie: 10/03/97 23:03 Filename: 100397
de: CQNC Type: S ,£orr. Factor: 1.00000
ib ID.: Cust. S«pl. 10.: Oust. ID.: 43159A
ess
Asi890
8e3130
Cd2265
Co2286
Cr2677
Hn2576
its
PPb
PPb
ppb
ppb
ppb
ppb
ge
13.270
L.0350
L.1027
1.155
23,05
49.76
ev
1.243
.0155
.1118
.3366
.3263
.2091
50
38.02
44.18
108.8
29.13
' 1.415
.4203
5BS
N12316
Pb2203
Sb2068
Sel960
its
ppb
PPb
PPb
ppb
je
5.032
8.133
L.5325
182.7
!V
.3913
.6273
1.508
,9375
;o
7.777
7.714
283.2
.5133
-------
Analysis Report Averages . Sun 10-05-97 06:31 ;45 PM page 35
Method: TRIANG12 Saaple Nase: 182-30-2C Operator: DKH
I Run Tiae: 10/03/97 23:08 Filenaie: 100397
Mode: C0NC Type: S Corr. factor: 1.00000
.lab ID.: CustSnpl. ID.: Cust. ID.: 43159A
Eless
AS1890
8e3130
M2265
Co2286
Cr2677
Nn2576
Units
ppb
ppb
ppb
ppb
ppb
PPb
Avge
12.69
L-.1803
3.931
1.376
124.7
3102.
SDev
.9807
.016
.372
.6084
.86
12.61
«SO
7.726
8.878
9.464
44.22
.6896
.4067
Eleas
Ni2316
Pb2203
Sb2068
Sel960
Units
ppb
ppb
ppb
ppb
Avge
29.13
59.63
L.8637
897.3
SOev
1.12
t7071
1.369
5.086
%RSD
3.844
1.186
158.6
.5668
-------
nalysis Report Averages • Sun 10-05-97 06:31*45 PN page 36
ithod: TRIANS12 Saiple Ha«e: 182-30-2C DA Operator: DKH
in Ti»e: 10/03/97 23:13 Filenaie: 100397
ide: COHC Type: S Corr. Factor: 1.00000
lb 10,: " _ Cust. Sapl. ID.: Cust. ID.: 43159A
eis
AS1890
8e3130
Cd226S
Co2286
Cr2677
Mn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
ge
12.98
L-.2307
3.949
1.741
124.1
io87.
18V
1.28
.0071
.1737
.1731
.2327
4.928
SP
9.859
3.079
4.4
9.942
.1875
.1596
ens
HI2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ge
29.47
58.99
L.0549
890.6
ev
.5883
.7393
1.935
2.492
SO
1.997
1.253
3522
.2799
*
154
-------
malysis Report Averages
Sun 10-05-97 06:31^45 PH page 37
lethod: TRIANGL2 Sasple Naue: 182-30-3C Operator: DXH
iun Ti«e: 10/03/97 23:17 Filename; 100397
lode: C0NC Type; S Corr. Factor; 1,00000
iab 10.: Cost. Sapl. ID.: Cost. ID.: 43159ft
•lens As 1890 Be3130 Cd2265 Co2286 Cr2677 Nn2576
[nits ppb ppb ppb ppb ppb ppb
ivge 5.383 L-.0818 2.746 L.3438 91.34 577,8
!Dev 2.25 .0167 .1433 .4288 .7583 2.364
|RSB 41.79 20.36 5.218 124.7 " .8301 .4092
less Ni2316 Pb2203 Sb2068 Sel960
Inits ppb ppb ppb ppb
Ivge 26.34 65.35 L.4047 691.5
iDev 1.122 1.133 .8382 3.714
"~D 4.261 1.733 207.1 .5371 -
loo
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PH page 38
21hod: TRIAHGL2 Saaple Naie:-182-58-1 Operator: DKH
un Tine: 10/03/97 23:22 Filenaae: 100397
)de: COHC Type: S Corr. Factor: 1.00000
ib ID,: Cust. Sipl. ID.: Cost. I1L: 43159ft
.ess
AS1890
8e3130
Cd2265
C02286
Cr2677
Mn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
¦ge
35,80
1*1.062
176.9
97.46
354.6
7449.
lev
1.332
.0144
.9607
1.261
3.353
54.38
!SB
3.722
1.353
.5431
1.294
.9457
.73
eas
Ni2316
Pb2203
Sb2068
Sel960
its
ppb
PPb
ppb
ppb
ge
88.76
33200.
11.574
236.2
ev
.8547
378.8
1.501
3.014
SD
.9629
1.141
95.34
1.276
»
i
I
i
156
-------
nalysis Report Averages
Sun 10-05-97 06:31:45 PH page 39
ithod: TRIANGL2 Sa«ple Na«e: 182-58-2 Operator: DKH
in Tine: 10/03/97 23:27 Filename: 100397
ode: C0NC Type: S Corr. Factor: 1.00000
ab 10.: Cust. Sapl. 10.: Cust. ID.: 43159A
Asl890
Be3130
Cd2265
Co2286
Cr2677
Mn2576
ppb
ppb
ppb
ppb
ppb
ppb
48.15
L.0090
236.8
11.55
307.5
7231.
.2847
.0217
.4589
.2637
.9373
19.68
.5913
242.1
.1937
2.283
.3048
.2722
ens
Ni2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ge
96.44
41240.
L2.464
376.0
ev
.1126
242.1
1.189
1.382
ISO
.1168
.587
48.24
.3676
157
-------
ilysis Report Averages • Sun 10-05-97 06:3U45 PN page 40
hod: TRIANGL2 Saiple Haae: 182-58-3 Operator: OKI
i Tine; 10/03/97 23:31 filenaae: 100397
e: CONC Type: S Corr. Factor: 1.00000
¦ ID.: . Cust. Sapl. 10.: Cust. 10.: 43159ft
IS
Asl890
8e3130
Cd2265
C02286
Cr2677
Hn2576
ts
ppb
ppb
ppb
PPb
ppb
ppb
i
47.92
L.0428
194.7
19.37
349.7
7793.
V
1.173
.0167
1.117
.0792
1.945
36.59
)
2.449
39.06
.5737
.4088
.5561
.4696
as
Ni2316
Pb2203
Sb2068
Sel960
:s
ppb
ppb
ppb
ppb
;
117.7
42770.
L2.149
474.6
f -
.6635
231.9
.9202
1.611
)
.5639
.5421
42.83
.3396
158
-------
Analysis Report Averages
Sun 10-05-97 06:31145 PH page 41
lethod: TRIAH6L2 Saiple Naoe: 182-30-7B Operator: DKH
Iun Tiie: 10/03/97 23:36 Filenaae; 100397
lode: C0NC Type: S Corr. Factor: 1,00000
[ab ID.: Oust. Sipl. ID.: Oust. ID.: 43159A
leas
AS1890
8e3l30
Cd2265
Co2286
Cr2677
Mn2576
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
L-5.030
L.0839
1.189
L~.8965
10.98
745.0
Dev
.7436
.0063
.1207
.109
.0951
1.403
RSO
14.78
7.565
10.15
12.16
.8664
.1684
leas
Hi2316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
ppb
ppb
vge
4.392
89.83
11.230
11.500
Dev
.3222
16.85
.1771
1.665
RSD
7.335
18.76
14.39
111
ir>9_
-------
nalysis Report Averages
Sun 10-05-9? 06:31:45 Prt page 42
sthod: TRIAN6L2 Saaple Na#e: ICV/CCV ' Operator: OKH
jn Tiae; 10/03/97 23:41 Filename: 100397
sde: C0NC Type: Q Corr. Factor: 1.00000
lb ID.: Gust. Sapl. ID.: Oust. 10.: 43159ft
.ess
Ag3280
A13082
Asl890
B.2496
Ba4934
883130
litS
ppb
ppb
ppb
ppb
ppb
Ppb
ge
509.8
516.8
517.1
2060.
497.7
505.3
ev
.244
7.984
3.395
104.9
.4479
1.996
S9
.0479
1*545
.6563
5.094
.09
.3951
eis
Ca3179
Cd2265
Ce4186
C02286
Cr2677
CU3247
its
ppb
ppb
ppb
ppb
ppb
ppb
98
533.6
513.2
499.6
505.7
507.0
495.0
ev
16.98
1.454
1.795
.6317
- 1.758
1.737
SO
3.182
.2832
.3594
.1249
.3467
.3508
ins
Fe2714
K_7664
li6707
»g2790
«l»2576
HO2020
its
ppb
ppm
ppb
ppb
ppb
ppb
je
542.6
4.983
473.4
510.1
499.3
501.0
2V
22.76
.0308
4.951
2.693
.8384
.8339
iO
4.195
.6176
1.046
.5279
.1679
.1665
IBS
Ha3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
ts
ppm
ppb
ppb
ppb
ppb
ppb
ie
4.882
511.7
518.8
501.7
526.4
493.5
V
.1548
.7753
3.289
4.481
3.276
3.237
;0
3.17
.1515
.6339
.8931
.6223
.6558
IS
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
514.2
511.4
518.2
512.3
49S.6
489.8
V
1.606
4.881
3.677
2.911
.8979
.3055
J
.3123
.9544
.7095
.5681
.1812
.0624
IS
T13349
T119Q8
V.2924
Zn2062
»Si2881
ts
ppb
PPb
ppb
ppb
ppb
a
494.9
508.1
501.6
514.3
Q8730.
t
1.034
4.624
1.856
2.396
119.9
)
.2089
.9101
.37
.4658
1.374
-------
Analysis Report Averages
Sun 10-05-97 06:31 :.45 PH page 43
Method: TRIAHGL2 -Sasple Naie: I08/CC8 Operator: DKH
Run Tiae: 10/03/97 23:46 Filename: 100397
Mode: CQNC Type: 8 Corr. Factor: 1.00000
Lab ID.: Cust. Sapl. ID.: " _ Cust. ID.: 43159ft
Eleras
Units
hvge
5Dev
Ag3280
ppb
.3114
.2353
75.55
A13082
As1890
ppb
1.982
34.76
15.72
.9409
8a4934 Be3130
ppb__ ppfe-
.4861 '.5498
.1393 .1966
28.65 35.76
•leas
linits
ivge
bev
;RSD
Ca3179
ppb
.8970
1.862
207.6
Cd2265
ppb
.4430
.2061
46.52
Ce4186
ppb
.0410
.8429
2057
Co2286
ppb
.2451
.1228
50.1
Cr2677
Cu3247/
PP^
3137
.157
19.3
Elans
•nits
Ivge
|0ev
RSO
leas
nits
vge
bev
hso
leas
pits
vge
Jev
leas
hits
Ige
)ev
ISO
Fe2714
K_7664
U6707
Hg2790 >
/nn2576
ppb
ppn
ppb
ppb /
ppb
1.764
.0911
.6892
mi
.7389
4.214
.0166
.1421
AMI
.2812
238.9
18.2
20.61/
887.5
38.06
Na3302
Hi2316
mm
2203-1
2203-2
pOi
ppb >
4'ph
ppb
ppb
-.0321
1.11/
2.986
.5832
.9779
.0401
.2
-------
lalysis Report Averages . Sun 10-05-97 06:31 ^45 PM page 44
thod: TRIAHGL2 Sanple Na»e: IC8/CC8 Operator: DKH
n Tine: 10/03/97 23:57 Filenaae: 10S397
de: CONC Type: 0 Corr. Factor: 1.00000
b 10.: Cust. Sspl. ID.: Cust. ID.: 43159ft
!BS
Aq3280
A13082
AS1890
8.2496
8a4934
883130
its
ppb
ppb
ppb
ppb
ppb
ppb
)e
.0307
23.20
-.3650
1279.
.0192
11134
!V
.2022
2.911
.9912
25.62
.0591
.0426
!&-
658
12.55
271.6
2.003
.307.1
"37.55
as
Ca3179
Cd2265
Ce4186
C02286
Cr2677
CU3247
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
-3.208
-.0765
.1627
.0398
.1894
-1.317
V
.9379
.2552
.8517
.2174
.1861"
.1638
0
29.24
333.5
523.5
546.3
98.3
12.44
¦s
Fe2714
K_7664
Li6707
Hg2790
Hn2576
Ho2020
ts
ppb
ppn
ppb
ppb
ppb
ppb
3
-4.629
.0719
.2088
-1.300
.0091
-.0174
4
6.884
.0224
.0387
3.062
.0171
.7067
)
148.7
31.16
18.55
235.5
188.5
4063
ss Na3302 Ni2316
;s ppn ppb
! .0047 .9382
.0184 .7454
i 390.4 79.45
P.2149 2203-1
ppb ppb
3.381 1.010
6.828 2.653
202 262.6
2203-2 Sb2068
ppb ppb
-1.259 .1297
.9694 1.109
77.01 854.9
s
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
s
ppb
ppb
ppb
ppb
ppb
ppb
4.108
-3.345
-.5031
-.8628
.3621
.0064
2.438
2.667
.3003
.9704
.7746
.0131
59.34
79.74
59.68
112.5
213.9
204.6
s
Ti3349
T11908
V_2924
Zn2062
•SI2881
5
ppb
ppb
PPb
ppb
ppb
-.0558
2.281
.9595
.3540
84294.
.044
2.561
.4795
.122
943.5
78.83
112.3
49.98
34.47
21.97
-------
ilysis Report Averages
Sun 10-05-97 06:31 MS PH page 45
thod: TRIAN6L2 Saaple Na«e: 182-30-8CA
I Tiie: 10/04/97 00:04 Filenaee: 100397
ie: CONC Type: S Corr. Factor:
! ID.
Oust. Sapl. ID.
Cust,
Operator: DKH
1.00000
ID.: 43159A
IS
As 1890
Be3130
Cd2265
Co2286
Cr2677
Hn2576
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
1-5.746
1.0700
L-.2699
L-1.808
13.90
27.04
V
1.234
.0499
.1088
.3745
.4578
.1618
D
21.47
71.31
40.32
20.72
3.292
.5984
as
Ni2316
Pb2203
Sb2068
Sel960
ts
ppb
ppb
ppb
ppb
F
11.452
10.13
L2.187
L-1.647
1
V
.7878
.9918
1.043
.9552
p
54.27
9.794
47.69
58.01
-------
nalysis Report Averages ; • Sun 10-05-97 06:31-45 PH page 46
ethod: TRIAHS12 Sa»ple Haie: 182-30-9D8 Operator: OKH
un Tiie: 10/04/97 00:09 Filenaae: 100397
ode: CGNC Type: S Corr. Factor: 1.00000
ab ID.: Cost. Sipl. ID.: Gust. ID.: 43159ft
leas
AS1890
8e3130
Cd2265
Co2286
Cr2677
Hn2576
nits
ppb
ppb
ppb
ppb
ppb
ppb
'98
L-4.036
L.0694
3.323
L-.1141
11.37
2856.
ttev
1.145
.0237
.0968
.4941
.4215
7.724
KB
28.37
34.19
2.915
432.9
3.708 "
.2704
leas
Hi2316
Pb2203
Sb2068
Sel960
lits
ppb
ppb
ppb
ppb
'98
6.990
1300.
L.7074
5.248
)ev
.6492
9.357
1.39
1.458
?SD
9.287
.7198
196.5
27.78
-------
Analysis Report Averages
Sun 10-05-97 06:31:45 PH page 47
Method: TRIANG12 Sample Haae: 182-30-110 Operator; OKH
Run Tiae: 10/04/97 00:13 Filenaae: 100397
Mode: C0NC Type: S Corr. Factor: 1.00000
(tab 10.: Oust. Sapl. 10.: Cust. 10.: 43159A
Eleis
AS1890
Be3130
Cd2265
Co2286
Cr2677
Hn2576
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
toge
L-6.007
L.0644
L.5700
1-1.286
12.08
107.0
30ev
1.402
.0229
.0568
.1111
.6479
.2145
kRSD
23.14
35.55
9.972
8.643
5.364
.2005
ileus
Ni2316
Pb2203
Sb2068
Sel960
Jnits
ppb
ppb
ppb
ppb
jvge
7.792
50.40
L-.4183
L-.9156
iOev
.4631
1.282 -
1.251
2.023
»RS0
5.943
2.544
299.1
221
*
165
-------
lalysis Report Averages • Sun 10-05-97 06:31 i.45 PH page 48
thod: TRIANGL2 Sa«ple Nase: 182-30-12D Operator: OKH
n Ti»e: 10/04/97 00:18 Filenaie: 100397
de: CONG Type: S Corr. Factor: 1.00000
b ID.: C'ust^Sipl. ID.: Cust. ID.: 43159ft
eis
AS1890
Be3130
Cd2265
Co2286
Cr2677
Mn2576
its
ppb
ppb
ppb
ppb.
PPb
ppb
P
L-5.585
L.0361
1.788
L-.6129
59.94
2210.
8V
3.109
.0265
.114
.2583
.4768
.6815
59
55.68
73.23
6.379
42.14
.7955
.0308
JBS
N12316
Pb2203
Sb2068
Sel960
its
Ppb
ppb
ppb
ppb
3e
69.53
39.56
12.951
1-.6559
!V
.6118
1.271
.5936
1.136
50
.88
3.214
20.12
173.1
»
-------
Analysis Report Averages ' . Sun 10-05-97 06:31:45 PM page 49
fethod: TRIAMS12 Sample Haie: 182-30-lp Operator: DKH ,
im Tiie: 10/04/97 00:25 Filenaae: 100397
lode: CONC Type: S Corr. factor: 1.00000
~ab 10.: Cust. Sapl. ID.: - Cust. ID.: 431S9A
[leas
AS1890
6e3130
Cd2265
C02286
Cr2677
Hn2576
inits
ppb
ppb
ppb
ppb
ppb
ppb
ivge
L-2.486
1.0515
1.810
L. 4544
85.82
961.8
:Dev
.8879
.0092
.0527
.351
.3539
3.115
;RS0
35.71
17.9
2.913
77.13
.4124-
.3238
leas
Ni2316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
ppb
ppb
vge
106.1
40.03
L-.7590
L.3204
Dev
.7478
1.914
.2712
-1.497
RSD
.7046
4.781
35.73
467.2
*
-------
alysis Report Averages
Sun 10-05-97 06:31^45 PN page 50
thod: TRIANGL2 Saaple Haae: 182-30-14BC Operator: DXH
n Ti«e: 10/04/97 00:27 Filename: 100397
de: CONC Type: S Corr. Factor: 1.00000
b ID.: Oust. Sipl. ID.: Cust. ID.: 43152A
-
eos Asl890 Be3130 Cd2265 Co2286
its ppb ppb ppb ppb
ge L-2.809 L.0835 L.1456 L-.6699
ev 1.086 .0156 .1438 .3453
SO 38.65 18.72 98.81 51.55
ess
Hi2316
Pb2203
Sb2068
Sel960
its
ppb
ppb
ppb
ppb
ge
L.4489
11.97
L-.6042
L-1.485
5V
.1782
.9304
1.341
1.066
SD
39.69
7.77
221.9
71.75
Cr2677 Hn2576
ppb ppb
4.712 15.17
.0878 .3786
1.864 2.495
-------
lalysis Report Averages
Sun 10-05-97 06:31:45 PH page 51
pthod: TRIANGL2 Sample Naae: ICV/CCV
in Tiae: 10/04/97 00:44 Filenaoe: 100397
Dde: CONC
Type: 9 _ Corr. Factor:
Ooerator: DKH
1.00000
ib ID.:
Cust. Snpl. ID.:
Cust.
ID.: 4315
iems
Ag32B0
A13082
Asl890
B.2496
8a4934
Be3130
lits
ppb
ppb
PPb
ppb
PPb
ppb
i ge
508.2
521.0
518.0
589.2
496.1
500.9
)6V
.3706
5.74
1.718
5.892
1.065
4.288
ISO
.0729
1.102
-.3316
1
.2146
.8561
.eas
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
lits
ppb
ppb
ppb
ppb
ppb
ppb
-ge
498.0
508.1
494.9
501.0
501.2
496.2
)ev
3.153
3.827
3.136
3.039
3.703
1.62
ISO
.6331
.7533
.6336
.6065
.7388
.3265
e»s
Fe2714
K_7664
Li6707
Mg2790
Hn2576
MO2020
lits
ppb
ppm
ppb
ppb
ppb
ppb
-ge
501.0
4.942
474.8
501.2
495.2
496.2
iev
7.211
.0181
3.127
3.391
3.069
4.009
RSD
1.439
.3656
.6586
.6767
.6198
.8079
ems
Na3302
Ni2316
P_2149
2203-1
2203-2
Sb2068
nits
ppip
ppb
PPb
ppb
PPb
ppb
¦ge
4.853
505.5
521.2
491.1
514.3
488.0
lev
.0743
3.201
5.935
.7056
5.313
4.642
ISO
1.531
.6331
1.139
.1437
1.033
.9513
less
1960-1
1960-2
Pb2203
Sel960
Sn1899
Sr4215
lits
ppb
ppb
ppb
ppb
PPb
ppb
vge
518.1
513.4
506.6
515.0
489.4
488.8
>ev
2.469
4.235
3.778
2.769
3.196
1.14
p
.4766
.8249
.7457
.5376
.653
.2332
ens
Ti3349
T11908
V_2924
Zn2062
,Si2881
lits
ppb
ppb
ppb
PPb
ppb
ge
493.2
504.6
498.1
506.2
5032.
)ev
2.647
6.149
3.475
5.271
66.56
!SD
.5367
1.219
.6976
1.041
1.323
1R9
-------
ilysis Report Averages ; • Sun 10-05-97 06:31 ;45 PM page 52
hod: TRIANG12 Saaple Haat: IC8/CCB Operator: DKH
i Ti#e: 10/04/97 00:49 Filenane: 100397
e: CONC Type: 6 Corr. Factor: 1.00000
i ID.: Cust. Sapl, 10.: Oust. 10.: 43159A
iJS^"
OS
Ag3280
A13082
Asl890
8_2496
Ba4934
Be3130
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
.4676
24.45
1.327
30.67
.4992
.5798
V
.3998
4.293
.7063
4.552
.094
.1473
6
85.49
17.56
53.23
14.84
18.82
25.4
,1S
Ca3179
Gd2265
Ce4186
C02286
Cr2677
Cu3247
ts
ppb
ppb
ppb
ppb
Ppb
ppb
'6
-2.419
.4600
-.1950
.6703
.6418
-.5379
V
.4539"
.1478
.9893
.0431
.1187
.2206
0
18.76
32.12
507.3
6.43
18.5
41.02
OS
fe2714
XJ664
ti6707
mm
Pln2576
Ho2020
ts
ppb
ppi
ppb '
ppb
ppb
ppb
e
1.474
.0931
.6785
2.058
.4741
1.498
V
5.144
.022
.07
2.257
.1062
.6762
D,
348.9
23.63
10.32
109.7
22.4
45.14
ns
Na3302
Ni2316
P_2149
2203-1
2203-2
Sb2068
ts
ppi
ppb
ppb
ppb
ppb
ppb
e
.0831
1.560
7.318
.0892
-1.074
3.589
V
.1408
.1298
2.333
2.374
1.223
1.992
0
169.3
8.32
31.88
2660
113.9
55.51
as
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
ts
ppb
ppb
ppb
ppb
ppb
ppb
e
3.256
-3.708
-.6864
-1.389
1.787
.4811
V
1.923
1.497
.8071
.797
1.266
.1049
0
59.07
40.35
117.6
57.37
70.88
21.8
as
Ti3349
T11908
V.2924
Zn2062
~Si2881
ts
ppb
ppb
ppb
ppb
ppb
e
.4955
4.448
1.468
.8561
Q-141.6
V
.0862
4.721
.1929
.0993
31.26
0
17.39
106.1
13.14
11.6
22.07
-------
Analysis Report Averages ¦ Sun 10-05-97 06:31,45 PH page 53
Method: TRIANGL2 Saaple Na«e: ICSAB Operator: DKH
Run Tine: 10/04/97 00:55 Filename: 100397
Mode: CONC Type: 0 Corr. Factor: 1.00000
Lab ID.: " _ Oust. Sapl, ID.: Oust. ID.: 43159A
Eless
Ag3280
A13082
Asl890
8_2496
824934
Be3130
Units
ppb
ppb
ppb
ppb
ppb
ppb
Avge
544.8
505800.
533.8
553.5
514.3
489.3
SDev
1.251
3758
4.029
6.369
.9676
2.806
*RS8
.2296
.743
.7547
1.151
.1881
.5734
Elias
Ca3179
Cd2265
Ce4186
C02286
Cr2677
CU3247
Units
ppb
ppb
ppb
PPb
ppb
PPb
Avge
457000.
480.4
500.6
475.1
480.9
542.7
SDev
3026
1.509
1.317
1.811
2.907
3.67
IRSD
.6621
.3141
.2631
.3811
.6045
.6762
Elems
Fe2714
K_?664
U6707
Hg2790
Nn2576
No2020
Units
ppb
PPB
ppb
PPb
ppb
ppb
Avge
177800.
025.13
615.8
539900
455.3
498.7
SDev
563
.1375
4.351
94.57
2.066
1.471
IRSD
,3167
.5471
.7065
,0175
.4539
.295
|Eleas
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
Units
PP«i
ppb
PPb
ppb
ppb
ppb
Avge
5.530
461.6
554.8
494.2
488.7
514.8
SDev
.0715
1.506
16.23
1.475
8.632
3.078
%RS0
1.294
.3262
2.926
.2985
1.766
.5979
Eleas
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr 4215
Units
ppb
PPb
ppb
ppb
PPb
ppb
Avge
548.9
529.2
490.6
535.8
504.1
504.8
SDev
7.083
5.996
5.299
3.02
4.475
.6384
IRSD
1.29
1.133
1.08
.5637
.8878
.1265
Eleas
Ti3349
T11908
V.2924
Zn2062
«Si2881
Units
ppb
ppb
ppb
ppb
ppb
'Avge
493.4
518.2
492.8
453.8
5057.
SDev
1.042
9.822
2.03
5.004
84.31
IIRSD
.2112
1.895
.412
1.103
1.667
171
-------
utoSampler Report Table: HA449
Hon 10-06-97 02:42:47 AM
page 1
able Name: HA449 Autosanpler Type: TYPE TJA
ample Positions: 171/192 QC Positions: 13/19 * Sets: 3
inse Station location is rack -1. dos. -1.
— Racks —
ack it Type
Usaae
ftPos Left Analvses/Pos
Aux. (I) Rack
Sample (16mm)
Sample (16mm)
Sample (16mm)
SamDle (16mm)
STD/0C/8LANK
Saaoles
Samples
Saaoles
Samples
-- Sample Sets —
sttt Tvoe PreDare? OescriDtion
13
27
48
48
48
10
1
1
1
1
Method #Pos Rack# StartPos
1 Normal
2 Normal
3 Normal
¦- Preparation Info —
;t)t Uotake Uptake#2
3 Samples Prepared,
ick #1
43237A
43287E
Tf59A~3
Final
TRIANGL2
TRIANGL2
TRIANGL2
10
8
3
Oil. Factor
I
II
19
)S
Row
Col
Sampie Name
Set S
ttUsed
Type
1
1
1
STD3
-NA-
2
Standard I-
2
1
2
STD1-BLANK
-NA-
1
Standard
3
1
3
ICSAB
-NA-
4
QC Standard \
4
1
4
CHECK 10
-NA-
1
QC Standard
5
1
5
ICV/CCV
-NA-
4
QC Standard
6
1
6
IC3/CCB
-NA-
4
9C Standard
1..
.19
Not
Used)
I-GO-CI'
i- GO
D 1 \
(
to (-S1C7
ick #2
is
Row Col
Sample Name
Set it JUsed
Type
1
1 1
43287A MB
1 -NA-
Sample
2
1 2
43287A LCS
1 -NA-
Sample
3
1 3
183-59-1
1 -NA-
Sanple
4
1 4
183-59-1 D
1 -NA-
Saaple
5
1 5
183-59-2A-C
1 -NA-
Sample
6
1 6
183-59-3
1 -NA-
Sample
7
1 7
183-59-3 MS
1 -NA-
Sample
8
1 8
183-59-3 MSD
1 -NA-
Saaole
9
1 9
183-59-3 PDS
1 -NA-
Sample
0
1 10
183-59-3 L
1 -NA-
Saacle
.1
1 11
43287E MB
2 -NA-
Sample
.2
1 12
43287E LCS
2 -Nfl-
Sanole
.3
2 1
183-59-4A
2 -NA-
Saaole
-------
*ut.oSaapler Report Table: HA449
?ack 12
Hon 10-06-97 02:42:47 AM
oaae 2
'OS
Ron
Col
Sample Nane
Set 1
iUsed
Type
14
2
2
183-59-4A D
2
-NA-
Saaole
15
2
3
183-59-4A MS
2
-Hft-
Saaple
16
2
4
183-59-4A USD
2
-NA-
Saiple
17
2
5
183-59-4A PDS
2
-NA-
Saaple
18
2
6
183-59-43 L
2
-NA-
Saiple
19
2
7
182-30-4^8 X10
I 3
-NA-
Sample
20
2
8
182-30-^8 X10
I 3
-HA-
Sanple
21
2
9
182-30-6A8 X10
i 3
-NA-
Saiole
22...48 Not Used)
lack 13
'os Ron Col Sample flame
1...48 Not Used)
Set i SUsed Tvoe
ps Row Col Sample Name
(1...48 Not Used)
I
lack 15
'os Row Coi Saaole Haute
Set it iUsed Tvoe
Set » ttUsecf Tvoe
1...48 Not Used)
-------
aivsis Report Averages
Hon 10-06-97 02:30:48 AN page 1
thoa: TRIANGL2 Sanole Name: STD1-BLANK Qoeraior;
n Time: 10/05/97 20:39 Filename: 100597
de: IR Tyoe: X Corr. Factor: 1.00000
b ID.: Oust. Smol. ID.: Cust. 10.:
8«S
Ag3280
A13082
Asl890
B.2496
8a4934
8e3130
its
count
count
count
count
count
count
ae
.00002
.00387
-.00023
.02206
.0006
.00047
sv
.00011
.00009
.00004
.00089
.00001
0
50
563.426
2.52544
20.8632
4.07692
1.68582
1.95036
BUS
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
its
count
count
count
count
count
count
ge
.00043
-.00013
-.00013
-.00012
-.00008
.00189
;y
.00001
.00009
.0002
.00003
.00003
.00001
SO
4.25429
70.3826
152.38
26.2113
43.8662
1.05434
2IDS
Fe2714
K_ 7 664
H6707
Mg2790
Mn2576
MO2020
its
count
count
count
count
count
count
je
.00002
3.83064
.07435
.00004
.00002
0
3V
.00002
.04123
.00068
.00002
0
.00003
SD
93.3868
1.07635
.92019
57.6132
37.0984
636.322
JIBS
Na3302
Ni2316
P.2149
2203-1
2203-2
S&2068
its
count
count
count
count
count
count
38
.00255
-.00125
-.00073
.00135
-.00005
.00025
iV
.00181
.00006
.00005
.00023
.00007
.00004
3D
70.8362
5.01478
6.99547
17.3465
140.76
15.8494
JiS
1960-1
1960-2
Snl899
Sr4215
T13349
T11908
its
count
count
count
count
count
count
ie
-.00374
.00153
-.0003
.00029
-.00001
-.0004
JV
.00017
.00012
.00009
.00001
.00003
.00002
SO
4.6237
8.20747
30.1705
4.01458
251.289
7.31095
>«s
VJ924
2n2062
Si2881
its
count
count
count
je
-.00027
.00001
.07488
!V
.00001
.00001
.00734
>0 4.11306 88.4421 9.31227
174
-------
na.lysis Report Averages
Mon 10-06-97 02:30:48 fill
page 2
;ethod: TRIANGL2 Samole Name: STD3
!un Tine: 10/05/9? 20:44
ode: IR
ab ID.:
Type: X
Cust. SibdI .
ID.
Operator:
Filename: 10059)
Corr. Factor:
: Cust, ID.
1.00000
isms
Ag3280
A13082
As 1890
8_2496
Ba4934
8e3130
nits
count
count
count
count
count
count
vge
.30372
.01542
.03954
.14577
.22132
.18651
Dev
.00116
.00018
.00006
.00049
.00013
.00091
RSD
1
.38469
1.1931
.15215
.34291
.0625
.49026
lens
Ca3179
Cd2265
Ce4136
Co2286
Cr2677
Cu3247
nits
count
count
count
count
count
count
im
.01724
.70253
.08565
.07732
.1117
.13701
bev
.00006
.00313
.00023
.00038
.00051
.00075
RSD
.40299
.44577
.27504
.4929
.4573
.54971
lems
Fe27l4
X_7664
Li6707
Mg2790
I1n2576
Mo2020
nits
count
count
count
count
count
count
vge
.00316
22.4733
15.2067
.01536
.09731
.059
pev
.00003
.12177
.12005
.00004
.0004
.00038
RSD
1.19666
.54185
.7895
.28016
.41265
.64583
lems
Na3302
Ni2316
P_2149
2203-1
2203-2
Sb2Q68
•iits
count
count
count
count
count
count
/ ge
.20364
.26237
.01676
.13041
.06877
.09177
)ev
.00291
.00075
.00005
.00039
.0009
.00031
j!SD
1.42934
.28313
.31786
.30212
1.31917
.33858
lems
1960-1
1960-2
Snl899
S r4215
T13349
T11908
its
count
count
count
count
count
count
!
-------
nalysis Report Averages
Hon 10-06-97 02:30:48 AN
page 3
ethod: TRIANGL2 Saiple Name: ST03 Operator: DKH
un Tine: 10/05/97 20:48 Filenaae: 100597
Dde: C0HC Type: 0 Corr. Factor: 1.00000
ab ID.: Oust. Snpl. ID.: Oust. ID.: 43287A
lens
Ag3280
A13082
Asl890
8_2496
Ba4934
mm
lits
ppb
ppb
ppb
ppb
pop
ppb
/ge
998.9
1002.
1001.
979.1
1000.
994.6
)ev
2.502
15.66
3.907
3.975
i.496
6.219
iSD
.2505
1.563
.3905
.406
.1495
.6253
teas Ca3179 Cd2265 Ce4186 Co2286 Cr2677 Cu3247
lits ppb ppb DDb ppb ppb ppb
we 997.5 998.9 1000. 999.3 998.5 1000.
)ev 5.834 6.146 4.324 5.337 6.208 4.963
?SD .5848 .6153 .4322 .5341 .6218 .4961
ems
Fe2714
K_76o4
Li67G7
Hg2790
Mn2576
Ho2020
lits
Dpb
DPB
ppb
ppb
pob
ppb
ige
1001.
10.01
1001.
996.9
998.7
1004.
lev
11.43
.0673
8.642
2.196
5.369
5.405
!SD
1.143
.672
.8636
.2202
.5375
.5381
ems
Na3302
Ni23i6
P.2149
2203-1
2203-2
Sb2063
lits
ppn
ppb
ppb
ppb
pob
DDb
ige
9.945
999.8
994.6
1000.
999.9
997.5
>ev
.1003
4.885
3.836
2.268
13.15
2.235
ISO
1.009
.4886
.3857
.2267
1.315
.224
ens
1960-1
1960-2
Snl899
Sr4215
Ti3349
111908
lits
DDb
ppb
ppb
ppb
ppb
ppb
ge
1001.
998.7
1000.
993.5
996.5
1027.
'ev
4.501
7.345
6.821
1.764
3.639
27.16
SO
.4496
.7354
.6818
.1776
.3652
2.646
ens
V_2924
Zfl2062
Si2381
Pb2203
Sel960
its
DDD
pob
DDb
PDb
DDD
ge
998.8
999,4
9875.
1000.
999.5
ev
4,132
10.27
32.64
8.057
4.206
SO
.4137
1.028
.3306
.8056
.4209
If* £*
/o
-------
Analysis Report Averages
Hon 10-06-97 02:30:48 All page 32
iethod: TRIANGL2 Sample Name: ICV/CCV
un Tine: 10/06/97 00:49 Filenane
lode: CONC
.ab ID.:
Type: Q
Cust. SuidI,
10.
100597
Corr. Factor:
Cust.
ID
Operator: DKH
1.00000
43287E
.lens
Ag328Q
A13082
As 1890
8_2496
8a4934
8e3130
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
514.2
465.5
523.7
371.7
510.6
513.2
Dev
3.659
15.88
3.013
2.308
1.211
1.23
RSD
.7117
3.411
.5753
.621
.2371
.2397
lens
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
'nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
507.1
505.5
501.9
519.6
504.9
509.5
¦Dev
.72
1.322
1.618
.5622
.2025
4.312
RSD
.142
.2615
.3223
.1082
.0401
.8464
leas
Fe2714
K_7 664
L i 6707
MQ2790
Hn2576
MO2020
nits
DCD
pom
oob
ppb
ppb
opb
vge
510.0
5.220
501.2
510.6
509.6
506.3
Dev
5,74
.0147
1.702
3.107
• 7lo4
1.684
RSD
1.125
.2814
.3396
.6084
. H06
.3326
lems
Na3302
Hi 2316
P.2149
2203-1
2203-2
Sb2068
nits
ppi
ppb
ppb
ppb
pob
PPD
vge
5.133
503.7
508.6
524.6
502.4
509.9
Oev
.1019
1.288
1.646
4.515
2.573
1.007
|rsd
1.967
.2557
.3236
,8o08
.5121
,1974
leas
1960-i
1960-2
Pb2203
Sel960
Snl899
Sr4215
nits
ppb
PpD
ppb
ppb
pob
ppb
vge
534.0
513.6
509.8
523.7
534.9
495.8
Dev
8.604
3.668
.7062
3.128
1.409
.8505
RSD
1.611
.7074
.1385
.5973
.2634
.1715
lens
T13349
111908
V_2924
2n2062
Si2881
flits
ppb
ppb
ppb
pob
ppb
|/ge
495.3
513.6
508.3
522.9
93317.
uev
.445
20.09
.244
2.143
49.75
RSD
.0898
3.911
.048
.4099
1.5
-------
inalysis Report Averages
Hon 10-06-97 02:30:48 AH page 33
lethod: TRIANGL2 Sample Naie: ICB/CCB Ooerator: DKK
;un Tirae: 10/06/97 01:00 filename: 100597
ode: C0HC Tyoe: 0 Corr, factor: 1.00000
ab ID.: Cust. Sapl. 10.: Cust. ID.: 43287E
less
Ag32S0
A13082
AS1890
B.2496
8a4934
Be3130
nits
ppb
PPb
ppb
_cat
unfc
Ppb
vge
.0728
Q-63.45
1.716
-152.2
.0897
Dev
.2579
9.305
2.124
.8616
.0436
>0765
RSD
354.3
14.67
123.8
.5662
48.61 ~
'li.01
lens
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
CU3247
nits
ppb
ppb
ppb
ppb ,,
'pob
PPb
vge
5.167
-.0027
1.002
.4021
-.2107
1.120
)ev
.8695
.0646
2.054
,.1827
.3179
.4253
RSD
16.83
2405
205 ,
'*45.43
150.9
37.98
lens
Fe2714
K_7o64
Li670 7
Iig2790
Mn2576
Mo2020
lits
ppb
PP« /
/ppb
pcb
ppb
ppb
^3.9
61.88
903.6
88.36
30.99
.eis
Ni2516
P.2149
2203-1
2203-2
Sb2063
lits
DDI».
ppb
opb
ppb
Dpb
DDb
»ae
-.0807
1.058
6.139
-4.035
1.168
1.015
ev
.0692
.8997
2.367
2.312
.346
1.53
ISO
85.81
85.02
38.56
57.3
29.62
150.8
ens
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
i ts
ppb
ppb
ppb
ppb
ppb
ppb
ge
.0512
-2.291
-.5644
-1.511
-1.364
.0496
ev I
2.459
.8208
.5898
.5204
2.126
.0126
SD \
^ 4808
35.82
104.5
34.44
155.8
25.49
ems
T13349
111908
VJ924
Zn2062
Si2881
X
its
ppb
PPb
ppb
pob
ppb
ge
.1260
85.327
-1.062
-.2780
0-1760.
IV
.1046
2.336
.5266
.1073
7.005
SD
83
43.86
49.6
38.58
.3981
n
flf*
I
173
-------
Inalysis Report Averages
Hon 10-06-97 02:30:48 AH page 34
ethod: TRIANGL2 Sample Naae: ICB/CC8 Operator: OKH
Un Time: 10/06/97 01:35 Filename: 100597
ode: CONC Type: 0 Corr. Factor; 1.00000
ab ID.: Cust. S#pl. ID.: Cust. 10.: 43287E
lens
Ag3280
A13Q82
AS1890
B_2496
8a4934
Be3130
nits
ppb
pob
ppb
ppb
pob
ppb
vge
.2549
8-50.91
.3651
-154.0
.0346
-.6850
Dev
.0922
9.438
1.899
3.503
.0949
.0581
RSD
36.17
18.54
520.1
2.275
274.3
8,484
le»s
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
nits
ppb
ppb
ppb
ppb
ppb
ppb
/ae
3.159
-.1202
.5775
-.0699
-.3972
1.643
)ev
1.431
.1561
2.984
.7117
.3612
.3603
RSO
45.29
129.9
516.7
1018
90.94
21.93
Lems
Fe2714
K_7664
Li6707
Ng279Q
Mn2576
HO2020
nits
ppb
ppm
ppb
pob
Dob
ppb
/ge
-1.106
-.0127
-.0426
-1.274
-.0230
.4920
Sev
8.081
.0307
.0674
6.145
.0475
.5719
m
731
242.5
158.4
482.3
206.9
116.2
[ems
Na3302
Ni23i6
P.2149
2203-1
2203-2
Sb2063
aits
ppm
ppb
ppb
pob
DDb
EDO
/ge
.0906
.0077
-.9336
-2.039
1.006
-.8875
)ev
.0529
.8674
1.879
5.303
.9217
1.059
jSD
58.35
11300
201.3
260.1
91.61
119.3
Lems
1960-1
1960-2
Pb2203
Sel960
Sn1899
Sr4215
tits
Dpb
DDb
cob
pob
DDb
DDb
toe
-2.125
-1.969
-.0078
-2.021
-1.887
-.0014
iev
1.013
3.448
1.589
2.012
.5425
.0371
ISO
i
47.66
175.1
20390
99.53
28.75
2686
ems
T13349
T11908
V.2924
mm
SI2S81
[its
ppb
ppb
ppb
pcb
ppb
ioe
.1491
4.793
-1.462
-.6902
8-1764.
iev
.1421
3.685
.9502
.4019
6.243
SO
95.27
76.87
65
58.24
.3539
-------
inalysis Report Averages
Hon 10-06-97 02:30:48 ftN page 35
sthod: TRIANGL2 Sample Kane: ICSA8 Operator: DKH
:un Time: 10/06/97 01:41 Filename: 100597
ode: C0NC Type: Q Corr, Factor; 1.00000
ab 10,: Gust. Smpl. ID.: Gust, 10.: 43287E
lens
ftg3280
A13Q82
Asl890
8.2496
8a4934
Be3130
nits •
ppb
ppb
ppb
ppb
ppb
ppb
vge
534.4
512400.
523.5
366.1
513.3
491.4
Oev
3,845
6230
2.221
.6211
2.304
2.326
RSD
.7195
1.216
.4242
.1697
.4488
.4733
leas
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
nits
DOb
ppb
ppb
pob
oob
DDb
vge
446900.
466.6
492.5
478.8
471.4
538.9
3ev
1610
2.119
.6333
1.868
1.099
5.828
RSD
.3602
.4541
.1286
.3902
.2331
1.081
ieos
fe2714
K_7664
Li6707
Mg2790
Mn2576
MO2020
nits
ppb
opm
ppD
ODD
ppb
ppb
/ge
175000.
825.64
627.2
530300.
457.0
492.8
3ev
365.9
.1885
4.733
1366
1.625
3.144
}SD
.2091
.7351
.7547
.2576
.3555
.6379
I ems
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb20o8
lits
pom
ppb
ppb
PPb
ppb
ppb
/ge
5.942
451.7
547,4
524.4
468.3
511.8
lev
.2139
1.713
21.63
6.302
9.702
6.462
!SD
3.6
.3793
3.951
1.202
2.069
1.263
.ens
1960-1
1960-2
Pb2203
Sei9o0
Snl899
Sr4215
lits
ppb
ppb
ppb
ppb
ppb
DDb
'ge
561.6
520.2
487.3
534.0
531.1
498.4
lev
13.78
7.225
4.388
1.857
7.535
1.9
ISO
2.454
1.389
.9004
.3477
1.419
.3811
ems
T i 3349
T11908
V.2924
2n2062
Si2881
its
DDb
ppb
ppb
ppb
pob
•ge
482.6
497.0
488.9
458.6
93335.
•ev
.3954
27.91
1.566
4.587
40.01
:SD
.0819
5.616
.3204
1
1.2
ISO
-------
halysis Report Averages
Hon 10-06-97 02:40:35 AM
page 1
pthod; TRIANG12 Sample Nase: 182-30-4^8 X10 Operator: OKH
bn Tiae: 10/06/97 01:52 Filename: 100597
Dde: CONC
3b ID.:
Type:
Oust,
Ssol. 10.
Corr. Factor: 1.00000
: Oust. 10.: 43159A
cviV, \o c,-•}n
lens
Asl890
8e3130
Cd2265
Co2286
Cr2677
«n2576
jits
ppb
ppb
ppb
DDb
ppb
ppb
ige
23.45
L-2.197
85.65
5.389
290.9
6269.
)ev
1.705
.0415
.4863
.4276
1.111
18.49
{SO
7.27
1.89
.5678
7.934
.382
.295
ess
H12316
Pb2203
Sb2068
Sel960
lits
ppb
ppb
ppb
ppb
|ge
54.38
14800.
5.608
51.11
1.348
57.21
.8882
3.053
?SD
2.48
.3865
15.84
5.974
1S1
-------
nalysis Report Averages Hon 10-06-97 02:40:35 AM page 2
Ffc
»Or
Bthod: TRIAHGL2 Sample Nane: 182-30-5AB X10 Operator: DKH
un Tine: 10/06/9? 01:56 Filenaae: 100597
Dde: C0NC Type: S Corr. Factor: 1.00000
ab ID.: Cust. Sapl. ID.: Oust. ID.: 43159A
lets
As 1890
8e3130
Cd226S
Co2286
Cr2677
Hn2576
nits
pob
ppb
ppb
ppb
ppb
ppb
/ge
19.25
L-1.694
76.49
1.850
238.5
4896.
)ev
1.565
.0374
.3244
.4449
.9006
1.622
?SD
8.131
2.208
.4241
24.05
.3776
,0331
Lams
Ni2316
Pb2203
Sb2068
Sel960
lits
pob
ppb
pcb
ppb
m
45.51
16750.
7.792
33.50
>ev
.5131
37.6
.61
1.318
5S0
1.127
.2245
7.829
3.934
132
-------
nalysis Report Averages
Hon 10-06-97 02:40:35 AM page 3
|ethod: TRIANGL2 Saaple Name: 182-30-&8 X10 Operator: DKH
(in Time: 10/06/97 02:01 Filenaae: 100597
ode: CONC Type: S Corr. Factor: 1.00000
ab ID.: Cust. SibdI. ID.: Cust. ID.: 43159A
Vf\U
lems
Asl890
8e3130
Cd2265
Co2286
Cr2677
Mn2576
lits
ppb
ppb
ppb
ppb
ppb
ppb
tge
19.48
L-1.565
70.96
2.575
243.0
5239.
)ev
2.827
.0065
.935
.437
4.867
93.24
}SD
14.51
.4134
1.318
16.97
2.003
1.78
lems
Ni2316
Pb2203
Sb2068
Sel960
lits
ppb
ppb
ppb
ppb
/ge
50.43
16030.
8.120
41.09
)ev
1.151
288.5
1.263
3.16
RSD
2.282
1.8
15.56
7.691
-------
lalvsis Report Averages
Hon 10-06-97 02:30:48 AH page 39
ithod: TRIANGL2 Samcle Name: ICV/CCV Operator: DKH
jn lime: 10/06/97 02:10 Filename: 100597
)de: CONC Tyoe: 0 Corr. factor: i.00000
lb ID.: Cust. Sfflpi. ID,: Oust, 10.: 43159A
.ens
Ag3280
A13082
AS1890
8_2496
8a4934
8e3130
u ts
ppb
ppb
ppb
ppb
ppb
ppb
-------
Analysis Report Averages
lion 10-06-97 02:30:48 AM page 40
Method: TRIANGL2 Samole Name: ICB/CCB Operator: OKH
[un Tiie: 10/06/97 02:15 Filename: 100597
lode: CONC Type: 8 Corr, Factor: 1.00000
ab ID,: Cust. Sipl. 10.: Oust. ID.: 43159A
•lens
Ag3280
A13082
AS1890
8J496
Sa4934
8e3130
nits
pob
ppb
ppb
ppb
ppb
ppb
!vge
.5749
Q-63,82
.3657
-136.9
.3795
-.4787
SDev
.4107
6.783
1.668
3.799
.0519
.101
,RSD
71.44
10.63
456
2.774
13.67
21.1
.lens
Ca3179
Cd2265
Ce4186
C02286
Cr2677
CU3247
{nits
ppb
ppb
Dob
ppb
pob
ppb
vge
13.31
.4885
1.703
.3038
.0423
1.460
iDev
2.049
.0586
.5006
.2791
.4756
.525
iRSD
15.4
11.99
29.4
91.89
1125
35.95
Ileitis
Fe2714
K_7 664
Li6707
PSg2?90
Mn257o
HO2020
inits
pcb
pom
pob
ppb
ppb
oob
tvge
8.455
.0203
.3686
1.612
.6411
Q2.i 50
pev
.7985
.0328
.0728
1.768
.183
.6808
,RSD
9.444
161.7
19.75
109.7
28.55
31.94
ieis
Ha3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
nits
opm
ppb
ppb
ppb
ppb
ppb
vge
.0995
.4490
3.567
-2.036
3.364
1.317
iDev
.073
.1087
2.12
2.848
.8472
2.218
pSD
73.43
24.22
59.44
139.9
25.19
168.4
Jems
1960-1
1960-2
Pb2203
Sel960
Snl399
Sr4215
pits
ppb
ppb
ppb
00b
ppb
ppb
vge
-1.385
-.3538
1.566
-.6972
. 2725
.3301
Dev
2.82
1.234
.3929
1.749
1.082
.0719
Irso
203.6
348.8
25.1
250.9
397
21.78
t
leis
Ti3349
T11908
V_2924
Zn2062
Si2881
Inits
ppb
ppb
ppb
ppb
ppb
h8
.3958
015.64
-.6701
.2672
0-1362.
Oev
.0524
4.009
.379
.1075
16.44
5SD
13.24
25.64
56.55
40.24
1.207
-------
nalvsis Reoort Averaaes Mon 10-06-97 02:30:48 All page 41
ethod: TRIANGL2 Sample Name: ICSA8 ODerator: DKH
un Time: 10/06/97 02:22 Filename: 100597
ode: C0HC TyDe: 0 Corr. Factor: 1.00000
ab ID.: Cust. Smpl. ID.: Cust. ID.: 43159A
leas
Ag3280
A13082
AS1890
8.2496
8a4934
8e3130
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
531.5
510100.
520.9
378.9
513.3
490.6
Dev
1.162
4342
2.38
6.889
.3917
4.976
RSD
.2187
.8513
.4569
1.818
.0763
1.014
less
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
nits
ppb
ppb
ppb
ppb
ppb
pDb
vge
444600.
467.7
493.2
478.4
471.2
537.6
Dev
4574
4.699
2.276
4
4.901
4.298
RSD
1.029
1.005
.4615
.836
1.04
.7996
lems
Fe2714
K_76o4
Lio707
Mg2790
Mn25 76
Mo2020
nits
ppb
ppm
ppb
ppb
ppb
ppb
vge
174300.
825.71
629.3
528100.
454.3
492.5
Dev
1346
.0458
1.309
1795
3.951
/
0.^0
RSD
.772
.178
.208
.3399
.8686
1.275
lems
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
nits
ppm
ppb
DDb
ppb
ppb
DDD
vge
5.842
452.8
535.7
526.8
466.7
509.4
Dev
.2118
4.146
9.465
5.451
15.62
5.083
RSD
3.625
.9156
1.767
1.035
3.346
.9979
lems
1960-i
1960-2
Pb2203
Sel960
Snl399
Sr4215
nits
ppb
ppb
ppb
ppb
ppb
ppb
vge
565.3
511.6
486.7
529.5
531.3
496.2
Dev
18.22
15.96
8.638
4.932
9.622
.6731
RSD
3.224
3.12
1.775
.9315
1.809
.1356
lems
Ti3349
111908
V_2924
Zn2062
Si2881
nits
ppb
ppb
Dpb
ppb
ppb
vge
481.4
505.8
488.7
458.4
03698.
Dev
2.676
22.27
3.739
9.543
29.3
RSD
.5559
4.403
.765
2.082
.7923
-------
Element Files CO.=SEL
Loc. Concentration
0
1
6
7
8
9
10
11
12
13
14
15
16
17
IS
19
£0
£1
£2
£3
£4
40
50.0 ug/L
100.0 ug/L
ID/We i ght File: EB163. IDW
So 1ut i ons
lc|i>tT7
Calib. Blank / Diluent
Stock / Recovery Stock
Stock j-CsO-lP
ICV=30ug/L |~C»0"\Or
CCV=60ug/L I-GO- w 0
CHECK LO
/ ICB /
t-Co-%P
CCB
I
43159ft
43159ft
¦*182—30-
»182—30-
*182—30-
*182-30-
«>18£—30-
>-18£~30-
18£-30-
#*182-30-
182-30-
Plfi£-30-
* 182—30-
^182-30-
t182-30-
* 182-30-
182-30-
182-30-
MB
LCS
¦1AB
•lftB
£AB
•3AB
4AB
•5AB
•&AB
•7AB
•SAB,.£>#.
•SAB
1 1AB
¦ 12AB
13AB
•14AB
15B
¦ISC
L
X10
Modifier 1
- ft SJdti ti* V(vvj\ if fcfii
° = V A * ,OL^ iSi.
ft- vf MS
9 - (L 11* Fifcut vf SO
<,of lOo. eoto*^
0iM io|tK7
1S7
-------
llement Files CO. GEL
lement: Co
'rint Data: Main+Suppl.
Vint: Calib. Curve+Elem.
finalyst: HOLSTE n
Peak Storage: 1 Repl./Sample
Params.
NSTRUMENT: 4100 ZL
lave length: £40.7 Peak
~ ignal Type: Single Beam
lead Time: 3.0
Sample Replicates: 2
standard Replicates: £
Technique: HGA Version: 7.30
SI it: 0.£0 Low
Signal Measurement: Peak Area
Read Delay: 0.® BOC Time: 2
Spike Replicates: Same as Sample
ALIBRATION:
Solutions i
ID
Cone
ILocat ionlVolumelDiluentI Modifier I
I Volume
Diluent Location: 0
Modifier #1 Location: 40
Calibration Units; ug/L
Calibration Type; Nonlinear
Modifier #2 Location:
Sample Units: ug/L
#1
m
alib. Blank
1STD BLANK !
1
0 1
10
10
1 5
standard i
1STD i=£5ug/L I
£5. 0 1
1 1
5
15
i vj
standard 2
1STD £=50ug/L 1
50. 01
1 1
10
10
1 5
standard 3
i STD 3=100ug/L 1
100. 0!
2 I
10
10
1 5
eslope Std.
1 Res 1 ope 50ug/L 1
50. 01
1 I
10
10
I 5
amples
1 |
— J
1
10
10
I S
urnace Time/Temperature Program:
teplTemp Ramp Hold
njection Temp: £0
Gas F1owtRead I Gas Type
1
I 110
1
20
£50 I
1 Norm
£
I 130
1
C'Cr
£58 I
I Norm
3
1 1400
5
£0
£50 I
I Norm
4
1 £400
0
4
0 1
* I Norm
5
1 £500
1
5
£50 1
1 Norm
I
Pipette Speed: 1005<
Extraction System: On
EQUENCE:
tep Action and Parameters
1 Pipet diluent + modifier
£ Run HGA steps 1 to End
1 + spike + sample/std
HECKS:
ecalibration Type;
ocations: None
Rutozero Only
one. Above Calibration Action: Dilute & Reanalyze After 1 Rep
lternate Sample Volumes < uL) : 5,2,1
un Alternate Volume Blanks: No
f -/-RSD > £0.0 and Concentration > 5 then Retry 1 times
heck %RSD on: Samples + Standards + Spikes + QC Samples
ecovery Measurements:
uL of 50 ug/L Standard at Location 1 Gives £5.0 ug/L
easure Recovery on Samples: 9-10
dd to QC Samples: Yes % Recovery Limits: 75 to 125
183
-------
~ I
ft/S I QC Sample I Cone. Limits
Loc.I ID I Lower Upper
4 ICV=30ug/L £7.0 33.0
0 ICB -2.0 £.0
5 CCV=60ug/L 48.0 72.0
0 CCB -2. 0 2. 0
Run Periodic QC Samples: Every 10
Dut of Limit fiction: Print Message Only
IftfterI PeriodicI fit I Count As I
Check I End I Sample I
ICalibl
X
X
X
X
X
X
latrix Check Calculations:
Difference for Dupls: No Locations:
t Recovery for Spike: No Locations;
Cone:
183
-------
ement File: CO.GEL
ite: 10/05/97
tta Files EB163.DAT
(chnique: HGA
Element : Co
Times 19:1£
ID/Wt File: UNTITLED
Calib. Type; Nonlinear
Wavelengths £40. 7
Slit: 0.S0 L
Lamp Currents 30
Energy: 44
ID: STD BLANK
Seq. No.: 00001
A/S Pos. s 0
Date: 10/05/97
. dispensed: 10 from 0, 5 from 40, 10 from 0
¦plicate 1 Times 19:14
>ak Area (A—s): 0.017 Peak Height (A)
ank Corrected Pk Area
-------
Auto-sera performed.
JCc
*
-------
tandard number 3 applied. C100.03
orrelation coefficient: i.00000
"fiisolau Calibration - C:\ftft If ~
S3 S3
«
• •
a
J3sz
e.
Jam
X 4.0000
£ , g*W = Q.vm 1 ,
.0 Concentration 4911.9
*
192
-------
Element File: CO. GEL
'ate: 10/05/97
ata File: EB163.DAT
'echnique: HGft
Element: Co
Time: £0:13
ID/Wt File: EB163.IDW
Calib. Type: Nonlinear
Wavelength: £40.7
Slit: 0.£0 L
Lamp Current: 30
Energy: 43
ID: ICV=30ug/L
Seq. No.
00009
ft/S Pos.: 4
Date: 10/05/9'
L dispensed: 10 from 0, 5 from 40, 10 from 4
leplicate 1 Time: £0:15
leak Area (ft—s) : 0.097 Peak Height (ft) : 0. 1£8
llank Corrected Pk ftrea (ft-s) : 0.091
.oncentrat ion (ug/L ): 30.1
|L dispensed: 10 from 0, 5 from 40, 10 from 4
teplicate £ (Peak Stored) Time: £0:18
•eak ftrea (ft-s) : 0. 096 Peak Height (ft) : 0. 131
lilank Corrected Pk ftrea (ft—s): 0.091
oncentration (ug/L ): 30.0
!ean Cone (ug/L ) : 30. 1
C sample is within range £7.0 •
SD: 0.08
RSD ('/.): 0. £6
5. 0
ID: ICB
Seq. No.: 00010
ft/S Pos.
0
Date: 10/05/97
^L dispensed: 10 from 0, 5 from 40, 10 from 0
Replicate 1 Time: £0:£0
•eak ftrea (ft-s): 0.007 Peak Height (ft): 0.018
l>lank Corrected Pk ftrea (ft—s): 0. 00£
oncentration (ug/L ): 0. &
iL dispensed: 10 from 0, 5 from 40, 10 from 0
eplicate £ (Peak Stored) Time: £0:£3
eak ftrea (ft—s): 0.008 Peak Height (ft): 0.0£3
Hank Corrected Pk ftrea (ft-s): 0.00£
oncentration (ug/L ): 0.8
lean Cone (ug/L ): 0.7
C sample is within range -£.0 -
SD: 0.07
RSD ('/•): 10.54
i. 0
ID: CHECK LO Seq. No. : 00011 ft/S Pos. : 6 Date: 10/05/97
tL dispensed: 10 from 0, 5 from 40, 10 from 6
(eplicate 1 Time: £0: £5
eak ftrea (ft-s): 0.0£1 Peak Height (ft): 0.038
Hank Corrected Pk ftrea (ft—s): 0.016
oncentration (ug/L ): 5.1
L dispensed: 10 from 0, 5 from 40, 10 from 6
feplicate £ (Peak Stored) Time: £0:£8
eak ftrea (ft—s): 0.0£3 Peak Height (ft): 0.037
lank Corrected Pk ftrea (ft-s): 0.017
Concentration (ug/L ): 5.7
193
-------
iSU m *.«¦
r\oy \ /* ; z f m f
IDs 43159ft MB
Seq. No.s 00®U
A/S Pos. : 7
Dates 10/05/97
L dispensed! 10 from 0, 5 from 40, 10 from 7
eplicate 1 Time: 20:30
eak Area (A-s): 0.007 Peak Height
-------
i r\ w w i
;uwcu r- rv ni eo \i
vim It*
Concentration (ug/L ): £7.8
jL dispensed: 5 from 0, 5 from 4(2, 5 from 1, 10 from 9
Replicate 2 (Peak Stored) Times 20:48
Peak Area (A—s): 0.092 Peak Height (A) : 0. life
slank Corrected Pk Area (A-s): 0.087
Concentration (ug/L > 5 28.7
lean Cone (ug/L )
W
Recovery is 87.3*4,
SD: 0. fe3
RSD{%)s
O '—»>>
^ Hl-7-^1 Ct
/'V'W'VW'V
a
o ID: 182-30-^8 L ^^^Seq. No
A# A/A# A* A» A» A# Ar A# A* A# A* A» A# A* A#'*V A* A*
a
'V/ ^\/ Af Af A* A/ A/ A/ A* A# "
* A< A* Ar A# A* A# A* A* Ar A* A» A# A# A# A* A*1 A# A^ A* A* A# A* Ar *"
00016
A/S Pos. : 10
Date: 10/05/9"
sL dispensed: 10 from 0, 5 from 40, 10 from 10
Replicate 1 Time: £0:51
eak firea (ft—s): 0.011 Peak Height (A): 0.022
ilank Corrected Pk Area (A-s) : 0.005
Concent rat i on (ug/L ) : 1.7
iL dispensed: 10 from 0, 5 from 40, 10 from 10
Replicate £ (Peak Stored) Time; 20:53
eak Area (A-s): 0,010 Peak Height (A); 0. 0£2
lank Corrected Pk Area (A~s>: 0.005
oncentration (ug/L ): 1.6
lean Cone (ug/L ):
1.6
SD : 0. 1 eC
Do ID: 182-30-1*AB L MR Seq. No. : 00017 A/S Pos. : 10
| ^ it- i-m
iL dispensed: 5 from 0, 5 from 40, 5 from 1, 10 from 10
Replicate 1 Time: £0:56
Peak Area (A-s) : 0.076 Peak Height (A): 0.099
^lank Corrected Pk Area (A-s): 0.071
Concentration (ug/L ): 23.2
iL d i spen sed: 5 from 0, 5 from 40, 5 from 1, 10 from 10
Replicate 2 (Peak Stored) Time: 20:59
j'eak Area (A-s): 0.075 Peak Height (A): 0.095
plank Corrected Pk Area (A-s): 0.0/0
concentration (ug/L ): £2.9
RSD C/.): 7.10
* *\e '\»A#'VA# A# A# A# A< A# A/A# A* A* A
Date: 10/05/9"
jlean Cone (ug/L )
Recovery is 85.5%
3. 0
SD: 0.2;
A^ A# A# A# Ar A* A* A* A/ A* A* A# A* A^ A# A^ A* A# A# A# A# Ar *
:o IDs 182—30—^AB*=*Seq. No.: 00018 A/S Pos.: 11
[L dispensed: 10 from 0, 5 from 40, 10 from 11
Replicate 1 Time; 21:01
:'eak Area (A-s) : 0. 021 Peak He i ght (A) s 0.031
ilank Corrected Pk Area (A-s): 0.01fe
Concentration (ug/L ): 5.2
iL dispensed: 10 from 0, 5 from 40, 10 from 11
RSD (%) s 0.97
A/ A# A# A» A# A/ A^ A» A* A# A* l\r A* A* A* A* A* A^ A>» A# A
Date: 10/05/97
195
-------
'eak Area (A-s) : 8.019 Peak Height (A): 0. 028
(lank Corrected Pk Area (A-s): 0.014
Concentration (ug/L >; 4.4
lean Cone (ug/L >: 4.8 SD: 0.54 RSD<54): 11.13
:o IDs 18£-30-3ta Seq. No.: 00019 A/S Pos. : 12 Date: 10/05/9"
iL dispensed: 10 from 0, 5 from 40, 10 from 1£
leplicate 1 Time: £1:06
¦eak Area (A—s) : 0.018 Peak Height (A) s 0. 0E8
lank Corrected Pk Area (A-s): 0.013
Concentration (ug/L ) : 4. 1
L dispensed: 10 from 0, 5 from 40, 10 from 1£
leplicate £ (Peak Stored) Tine; £1:09
eak Area (A-s): 0.018 Peak Height (A): 0.0£9
lank Corrected Pk Area (A-s): 0.012
oncentrat i on (ug/L ) : 4.0
ean Cone (ug/L ): 4.1 SD: 0.07 RSD(%): 1.81
A/t\r ''W *\s '"w r\s
o ID: 18£-30-4AR- 9«r.—Me^~i2u2jg£0 A/S Pos. : 13 Date: 10/05/97
L dispensed: 10 from 0, 5 from 40, 10 from 1;
ample abs. is greater than that of the largest standard,
e p 1 i cat el T i mi&4 21:11
eak Area (A-s): 0.491 P^k Height (A); 0.529
lank Corrected Pk Area (A—s): 0.486
oncentration (ug/L ): 190.0
*\j «"Vi\[ A/*S~t e\i jr\s *\s *\j f\?
o ID: 182—30-4AB Sec< No.: 00021 A/S Pos.: 13 Date: 10/05/97
L dispensed: 15 from 0, 5 fj/om 40, 5 from 13
eplicate 1 / Time: 21:13
eak Area (A-s); 0.306 / Peak Height (A): 0.441
lank Corrected Pk Area /(A-s) : 0.301
oncentration (ug/L )/ 106.4 Corrected Cone (ug/L ): £12.8
L dispensed: 15 fp^m 0, 5 from 40, 5 from 13
eplicate 2 (Pealf Stored) Time: 21:16
eak Area (A-s) :/0. 306 Peak Height (A): 0.318
lank Corrected/Pk Area (A-s): 0.300
oncentration /fug/L ): 106.0 Correct ed Cone (ug/L ) : 212.0
ean Cone (ug/L )s 106.2 SD: 0.25 i RSD(%): 0.24
orreeted ConcN^Zt Ls_J2JL£.Jl jlfcjK H S70
j "V *V *V*W 'V 'W'W *V r\e 'N/ 'V'W /l
o ID; CCV=60ug/L Seq. No. ; 00022 A/S Pos. s 5 Date; 10/05/97
L dispensed: 10 from 0, 5 from 40, 10 from 5
eplicate 1 Time: 21:18
eak Area (A-s); 0.164 Peak Height (A): 0.207
lank Corrected Pk Area (A-s): 0.159
198
-------
.iL dispensed; 10 from 0, 5 from 40, 10 from S
Replicate S (Peak Stored) Time: £1:£1
Jeak Area (A-s): 0.168 Peak Height (A): 0.207
Jlank Corrected Pk Area (A-s): 0.163
Concentration (ug/L ): 54.9
lean Cone < ug/L ); 54. 1 SD: 1. 10
3C sample is within range 48. 0 - 7£. 0
RSD<%>! £.04
ID: CCB
Seq. No.: 000£3
A/S Pos. : 0
tL dispensed: 10 from 0, 5 from 40, 10 from 0
Replicate 1 Time: £1:23
:'eak Area
-------
f V
-A
ID: 1SS—3©—6AB ^iwc^iiec Seq. No.
00026
A/S Pos•
L dispensed: 10 from 0, 5 from 40, 10 from 15
ample abs. is greater than that of the largest standard.
leplicate 1 Time: 21:35
eak Area (A-s): 0.445 Peak Height : 0.265
oncentration (ug/L ): 92.1
ean Cone (ug/L ); 93.2
orreeted Cone (ug/L ): 186.4
Time: 21:40
Peak Height (A): 0.326
Corrected Cone (ug/L ): 184.3
SD: 1.52 RSD<*> : 1.63
„,V,V«V£
-------
;o id: iaa-30-^AB Seq. No. : 80030 ft/S Pos. : 18
kL dispensed! 10 from 0, 5 from 40, 10 from lfl
Replicate 1 Time: 21:5£
:'eak ftrea
-------
mcentration (ug/L ): £.3
10 from ®, 5 from 40, 10 from 21
Time: 22:09
Peak Height (A): 0.021
0.008
_ dispensed:
?plicate £ (Peak Stored)
>ak Area (A—s> : 0.013
Lank Corrected Pk Area : 3.98
Seq. No.: 00034
A/S Pos.: 5
Date: 10/05/97
- dispensed: 10 from 0, 5 from 40, 10 from 5
?plicate 1 Time: ££:11
sak Area (A-s) : 0. 170 Peak Height (A)
lank Corrected Pk Area (A-s): 0.1&4
Dncentrati on (ug/L ): 55.3
_ dispensed: 10 from 0, 5 from 40, 10 from 5
=plicate £ (Peak Stored) Time: £2:14
?ak Area (A-s): 0.167 Peak Height (A)
Lank Corrected Pk Area (A-s): 0.162
aneentration (ug/L ): 54.5
?an Cone (ug/L ): 54.9 SD; 0.58
2 sample is within range 48.0 — 72.0
0. £11
0. £0£
RSD ("/•)
1. 0S
V'W'V "
ID: CCB
Seq. No.: 00035
A/S Pos.
0
Date; 10/0b/97
_ dispensed: 10 from 0, 5 from 40, 10 from 0
eplicate 1 Time: ££:16
eak Area (A-s): 0.010 Peak Height (A)
lank Corrected Pk Area (A-s): 0.005
oncentrat i on (ug/L ): 1.6
L dispensed: 10 from 0, 5 from 40, 10 from 0
0. 019
eplicate £ (Peak Stored)
eak Area (A-s): 0.008
lank Corrected Pk Area (A-s)
oncentration (ug/L ): 1.0
0.00:
ean Cone (ug/L );
C sample is within range
1.3
Time: £2:19
Peak Height (A)
SD: 0.45
0. 030
0
o ID: 182-30—14^8- Seq. No.
0003S
A/S Pos.
£2
RSD (54) : 35.75
Dates 10/05/97
L dispensed: 10 from 0, 5 from 40, 10 from 22
eplicate 1 Time: £2:21
eak Area (A-s): 0.012 Peak Height (A): 0.0£5
lank Corrected Pk Area (A-s): 0.006
oncentration (ug/L ): 2.1
L dispensed: 10 from 0, 5 from 40, 10 frot
200
-------
:'eak Prea (ft-s): 0.013
Blank Corrected Pk Area (ft-s)
Concentration
-------
o ID: CCB Seq. No.; 00040 ft/S Pos.: 0 Date; 10/05/97
L dispensed: 10 from 0, 5 from 40, 10 from 0
eplicate 1 Time; £2:41
eak Area (A-s > ; 0.017 Peak Height (ft): 0.©25
lank Corrected F'k Area (A—s) : 0.012
ancentration (ug/L___J-s— —
_ dispensed: 10 from 0, 5 from 40^/10 from 0
•plicate 2 (Peak Stored) Time: 22:44
;ak Area (A-s>: 0.010 Peak Height (ft): 0. 0£5
Lank Corrected Pk Area (A.-0 : 0.004
incentrat i on \t *V 'V *V
-------
:o IDs 182-30-4^8 X10 Seq. No. : 00043 A/S Pos. ; 13 Date: 10/05/9*
,iL dispensed; 10 from 0, 5 from 40, 10 from 13
Replicate 1 Time: 23:54
Peak Area (A-s): 0.090 Peak Height (A): 0.151
Hank Corrected Pk Area (A—s): 0.085
"oncentrat i on (ug/L ): 27.9
JiL dispensed: 10 from 0, 5 from 40, 10 from 13
Replicate 2 (Peak Stored) Time: 23:57
•'eak Area : £8.84
|c sample is within range —£.0 - £.0
203
-------
/Weight File: AS310.IDW
mpie Volume: 100 ml
Analyst: RICHARDS
Nominal Weight: 1.0 g
Loc. Sample ID Weight Dilution
M£-
0 STO SLK
1 ST01=0.2ug/L
2 3TD2=0.5ucj/l
3 STD3=1.Oug/L
i ST04=2.Oug/L
5 ST05=5.Oug/L
6 ST06-10. Oug/L
7 icv=4.Oug/L n£.
3 ICS
9 CHECK LO
10 431S9A MSi
11 43159A ME1 D
12 431S9A LC31
13 43159ft LCS1 D =»e<»-7-q?tc
14 L32-30-1GA6
15 182-30-lGAb 0
16 132-30-iC.flc MS
17 1 O ^ ~ O U~ 1 S."5 M 8 HoO
13 CCVI=6.Oug/L
19 CCB1
20 132-30-j3A3
21 132 -30-2-3Ac D
22 132-30-3GA8
23 182-30-jGAS 0
24 132-30-4FAE
25 132-30-4FAB 0
26 132-30-3FGA8
27 182-30-3F6A6 I
23 L32-30-oFGA£
29 132-30-6 FiSAB 0 ^ ^ . tl ckuhl ^
3 0 <„CV 2 = b.0uo/L
31 CC82
32 132-30-70A6
33 132-30-7CA3 0
34 132-30-38¦IOiV&i'i u:
33 132-30-Sfcl0:,on0 t>
36 132-30-9CA8
37 I82-30-9CA3 D
38 182-30-9CA3 MS
39 182-30-9CAB MSD
40 182-30-11CA3
41 182-30-11CA8 D
42 CCV3=6. Ouq/._
43 CC83
44 132-30-12CAB
45 182-30-12CA8 0
46 182-30-13CA6
47 182-30-13CAB D
#8 182-30-UGAB
49 182-30-14GA6 0
50 182-30-1C
51 182-30-1C 0
52 182-30-2C
53 182-30-2C 0
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Loc
110
111
112
113
114
115
116
117
113
119
120
121
122
124
l?c,
126
127
128
129
130
131
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136
L37
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50
51
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56
57
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S2
S3
S4
>5
Sample ID Weight Oilution
01?-
182-30-5D
182-30-5D D
182-30-5E
182-3C-5E 0
CCV9=6.Oug/L
cce<5
182-30-6C
182-30-60 0
182-30-6D
182-30-60 D
182-30-6E
182-30-6E D
182-30-11£
1S2-30-1 ie o i-oir-u
CCV 10=6. Oug/L ——— ~ * ' '
CCB10
43159A MB2
43159A ME2 D
4 315 "A LO 5 2 -aa-io-l hi te
4315°A LCS1 D ¦»# tc
182-30-LIF
182-30-11F 0
132-30-1IF MS
10v-3O-llh riSO o ^ ^ ^
CCVl:6.0uc/L
CCBl
132-30-11G
182-30-1K? 'j
1S2-30-12E
182-30-12E 0
182-30-12;"
182-30-12F C
lS2-30-12'3
182-30-12G 0
182-30-13E
182-30-13E 0
CCV2- 6.Oug/L
CCB2
1S2-30-13F
182-30-13F 0
182-30-13G
182-30-13G D
182-30-8A
182-30-8A D
182-30-80-15C
182-30-8D-15C
182-30-14E
182-30-14E 0
CCV3-6 .Ouq./L
CC83
182-30-7F
182-30-7 F 0
132-30-80E15C
182-30-80E15C
182-30-9FG158
182-30-9FG15B
y olfr - ^4 («*?
208
-------
,cc.
Sample ID
66
182-30-7FG
!67
182-3Q-7FG D
68
182-30-14EF
69
182-30-14EF D
70
CCV4-6.Ouq/L -
71
CCB4-
•72
182-30-13G MS
73
182-30-13G MSO
74
182-30-9F158
182-30-9F15B 0
CCV5=6.Oug/L
^7
CCB5
Weight Oilution
l-Olt-H
R ja,(
-------
Element File: HG_.ME:.
Element; Ha2
Print Data: Main+Suppl.
Print: Calib. Curve
Remarks :
STANOfiROS= 3-013-3
QC= 3-018-4
Analyst: RICHARDS
Peak Storaqe: None
H
1 1-4-77
INSTRUMENT: 5100
Technique: MHS Version: 7.01
Wavelength: 253.7
Peak
Slit: 0.7 Low
Signal 1yoe: AA
Signal Measurement: Peak Height (5)
Read Time; 30.0
Read Delay: 1.0 80C Time: 2
Sample Reclicates:
x
3ta ncla rd Reo 1 icate
s: 1
:LAME:
:lame Type: Air
Flame Censor: On
)xidant Flow: 10.0
L/iiin
Fuel Flow: 2,0 L/min
;alIBRhTIOH:
Solutions !
i
[0
Core
t
:aiib. 61-jnk ! ¦; T 0
8 LK
i
tanaard 1 ,'310
1
o.200:
tanc-5 rd 2 ;CF0
9
0.500!
tandcrc 3 15TO
i.ooc;
tanda-d * IS TO
*
:,ooc:
tandard 5 13TO
c
5.000!
tandard 6 |3F0
6
'.u.ooc;
Calibration Units
• ug/L
Sample Units: ug/L
Calibration Type:
Linear
atrix Check Calculations:
Difference for Duols: No Locations:
Recovery for Spike: No Locations:
.one
20S
-------
I
ement File: HG_.M£l Element: Hg2 Wavelength: 253."
Oate: 09/26/97 Time: 09:35 Slit: 0.7 L
Ita File: AE810.DAT ID/Wt File: AB810.I0W Lamp Current: 0
chniaue: MHS Calib. Type: Linear Energy: 72
Remark 1: STANDAR0S= 3-018-3
mark 2: QC= 3-01S-4
f^lTtc
Ho2 ID: STD 8LK Seq. Ho.: 00003 A/S Pos.: — Oate: 09/26/97
Ha2
fclicate 1 Time: 09:3c-
Peak Area (A-s): -0,005 Peak Height (A): -0.001
#nk Corrected Pk Height (A): -0.001
centration lug/L ): -0.022
Aigto- ze ro oe rformec.
X
Hc2 ID: STD1=0.2uq/L Sec. No.: 00004 A/S Pos.: — Oate: 0°/26<'9~
•;Woie abs. is greater than that of the largest standard.
Replicate 1 Time: 09:38
PJ|k Area (A-s;: 0.170 Peak Height (A): C.QOi
Bijnk Corrected Pk Height (A): 0.007
Concentration ncentration (ug/L i: 1.017
aRard number 3 applied. [l.OOOj
>rrelation coefficient: 0.99988 5lope: 0.0363
|
10: ST0a-2.Oug/L Seq. No.: 00007 A/S Pos.: — Oate: 09/26/97
nfBe abs., is greater than that of the largest standarc.
offcate 1 Time: 09:42
I
i~C<
| 209
-------
eak Area (A-s r. 1.74-S Peak Height (A); 0.075
lank Corrected Pk Height (A): 0.075
oncentration (ug/L ): 2.054
tandard number 4 applied. [2.000]
orrelation coefficient: 0.99979 Slope: 0.0370
32 ID: STD5=5.0ug.'L Seq. No.: 00008 A/S Pos.: — Date: 09/26/9"
amole abs. is greater than that of the largest standard.
;plicate 1 Time: 09:43
;ak Area (A-s): 4.435 Peak Height (A): 0.199
.ank Corrected Pi- Height (A): 0.199
>ncentration iug/L ): 5.372
.andard number 5 applied. C5.000J
>rrelation coefficient: 0.99927 Slope: 0.0393
2 ID: 3TQ6 = L0. Ouq/L Seq. No.: 00009 A/S Pes.: — Date: 09--'26/'3~
mple abs. is greater than that of the largest standsre
p 1 icate 1 r ime : 09:4-4
ak Area ( A-s i: 8. 597 Peak Height (fit: o. 36'*
3n;< Corrected Pk Height ( A >: 0.369
icentration (ug/L <: 9.391
andard number * applied. [10.000]
'relation coefficient: 0.9991° Slope: 0.037 5
210
-------
ft
1
ement File: HG_.MEL Element: Hg2 Wavelength: 253."
te: 09/26/97 Time: 09:45 Slit: 0.7 L
ta File: AB810.DAT ID/Wt File: A8810.IDW Lamp Current: 0
chnique: MHS Calib. Type: Linear Energy: 72
Remark 1: STANDARDS: 3-018-
jmark 2: QC= 3-018-4
N
Display Calibration - C:\AA_USER\ftft_FILES\ELEMEHT\HG_.MEL
4
8.369.
|
1
i x-*
!
i /
' ' n
J3 1 00
C i /
!
i
I
I jglA Linear
| M Cflrr Coef , e.999-19
Slope I 8.0375
0.0 ^ Concentration 10.000
\
211
-------
g2 10: rCV=4,Qug/L Seq. No.:
splicate 1
sak Area (A-s): 3.485
lank Corrected Pk Height (A): 0.148
xicsntration (ug/L ): 3.954
OuulO A/S Pos.: — uate: 09/26/9/
Time: 09:48
Peak Height (A): 0.148
32 ID: ICB Seq. No.: 00011 A/S Pos.: — Date: 09/26/9"
jplicate 1 Time: 09:49
>ak Area (A-s ): 0.016 Peak Height (A): 0.001
.ank Corrected Pk Height (A); 0.001
incentration (ug/L ): 0.016
2 ID: CHECK LO Seq. No.: 00012 A/S Pos.: -- Date: 09/26/9"
Dlicate i Time: 09:50
ak Area (A-s): 0.18? Peak Height (A): 0.00"
ank Corrected Pk Height (A): 0.007
ncentration (ug/L ): 0.193
ID: 43159ft MB! Seq. No.: 00013 A/S Pos.; — Date: 0?/2i/9-
~licate i
3k Area (A-s !: 0.0QT
ank Corrected Pk Height (A):
-centration (ug/L ): 0.000
riffle: 09:51
Peak Height (A): O.OQQ
0.000
2 ID: 4 3159A ME1 0 Seq. No.: 00014 A/S Pos.: — Oate: 09/26/9"
Diic.ate 1 Time: 09:52
ik A i~ea I A-s?: 0.002 Peak Height (A): 0.000
ink Corrected Pk Height (A): 0.000
icentration (ug/L !: 0.000
10: 43159A LCS1 Seq. No.: 00015 A/S Pos.: — Oate: 09/26/9"
)iicate I Time: 09:53
,k Area (A-s): 4.235 Peak Height (A): 0.178
,nk Corrected Pk Height (A): 0.178
centration (ug/L J: 4.756
ID: 431S9ALCSl D„ Seq. No.:
licate 1
k A rea (A—s 3: 4.435
nk Corrected Pk Height (A): 0.189
centration (ug/L ): 5.032
00016 A/S Pos.: — Date: 09/26/9"
Time: 09:55
Peak Height (A): 0.189
ID: 182-30-1GAE Seq. No.: 00017 A/S Pos.: — Date: 09/26/9"7
919
-------
I
plicate 1
Peak Area (A-s): 0.056
¦.ank Corrected Pk Height
Jpncentration (ug/L ): 0.
Time: 09:56
Peak Height (A): 0.002
(A): 0.002
053
ID: 182-30-1GAB D
3eq. No.: 00018
A/S Pos.
Reolicate 1
Iak Area ( A-s ): 0.041
ank Corrected Pk Height
Concentration (ug/L !: 0.
Time: 09:57
Peak Height (A): 0.002
(A): 0.002
040
I
Hq
g2 ID: 182-30-1GAB MS
Id lie,ate 1
ak Area (A-s »: 4.38c
Blank Corrected Pk Height
(Jncentration (ug/L !: 4,
Seq. No.: 00019 A/S Pos.
Time: 09:53
Peak Height (A): 0.186
(A): 0.186
960
Date: 09/26/9"
Date: 09/26/9"
I
3pr
i-O-lGAB HS0
3ea. Nc.: 00020
A/? Pos
Replicate i
Iak Area c ft-s >: 4 .104
ank Corrected Pk Height
ncentration
-------
:oncentration (ug/L ): O.Olt
Ig2 ID: 182-30-3GAB
Seq. No.: 0002!
A/S Pos,
Date: 09/26/9:
leplicate 1
eak Area (A-s ): 0.023
'lank Corrected Pk Height (A): 0,001
oncentration (ug/L ): 0.024
Time: 10:05
Peak Height (A): 0.001
10: 182-30-3GA6 0
Seq. No.: 00026 A/3 Pos
Date: 09/26/9"
epiicate 1
eak Area (A-s): 0.01S
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.0lc
T i me: 10:06
Peak Height (Al: 0.001
ID: 182-30-4 FAB
Seq. No.: 00027
Pos. :
Date: 09/26/9"
2Dlicats 1
;ak Area (A-s': 0.597
Lank Corrected Pk Height (A): 0.02S
5ncentration (ug/L ): 0.663
T iime: 10:07
Peak Height ( A : 0.
ID: 132-30-4FAB D
Seq. No.: 0002;
^ r,
H / C- r'uc
Date: 09/26/9"
>Dlicats 1
¦ak Area (A-s): 0.597
.ank Corrected Pk Height (A): 0.025
¦ncentration (ug/L ): 0.660
Time; 10:OS
Peak Height (A): 0.0.
10: 132-30-5FGAB
Sea. No.: 00029
A/S Pos.:
Date: 0 9/26/9.
olicate 1
ak Area (A-s ): u.19?
ank Corrected Pk Height (A): 0.008
ncentration (ug/L ): 0.211
Time: 10:10
Peak Height (AS: 0.008
2 10: 1S2-30-SFGAB D
Seq. No.: 00030 A/S Pos,
Plicate 1
jk Area (A—s): 0.191
ank Corrected Pk Height (A): 0.008
icentration (ug/L ): 0.211
Time: 10:11
Peak Height (A): O.OOS
Oate: 09/26/9"
ID: 182-30-6FGAB
Seq. No.: 00031 A/S Pos
Date: 09/26/9"
)licate 1
:k Area (A-s ;: 0.177
ink Corrected Pk Height (A): 0.007
icentration (ug/L ): 0.193
Time: 10:13
Peak Height (A!: 0.00"
214
-------
I
Hg2 ID: 132-3Q-6FGAB D Sea. No.: 00032 A/3 Pos.: — Date: 09/26/97
Solicate 1 Time: 10:14
reak Area (A-s): 0.166 Peak Height (A): 0.007
Blank Corrected Pk Height (A): 0.007
Concentration (ug/L ): 0.184
tJ2 ID: CCV2=6.0ug/L Seq. No.: 00033 A/S Pos.: — Date: 09/26/9"
Replicate 1 Time: 10:15
ik Area (A-s): 5.032 Peak Height (A): 0.221
ink Corrected Pk Height (A): 0.221
Tncentration iug/L }: 5.890
I
f
31a
t
1
ID: CCB2 Seq. No.: 00034 A/3 Pos.: ~ Date: 09/26/9"
ilicate 1 rime: 10:19
ik Area i fl-s !: 0.00? Peak Height (Ai: 0.001
Blank Corrected Pk Height t A): 0.001
icentration (ug/L ): O.Ql0
Ha2 10: 132-3Q-7CAS See;. No. : QOOoS A/3 Pos. : — Dal
lb i ieate i Time: 10:21
Peak Area (ft—s. ): O.OOt Peak Height (A:: 0.000
81bnk Corrected Pk Height i A >: 0.000
C0K
icentration (ug/L ): 0.00 5
H* ID: 182-30-7CA8 D Seq. No.: 0003t A/3 Pos.: — Date: 09/26/9"
«
Reo
I
3m.(
2on<
I
Ho 2
I
31ar
I
¦
'eo.
1;
I
I
Reo i icate 1 T ime : 10 : 22
pftk Area (a-s ): 0.003 Peak Height (A): -0.000
SBiink Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.003
W.iofc
Ho 2 ID: 1 * 2 - 30-8810ASA Sea. No.: 000;-T A/S Pos . : — 0.3
^ ec
RB iic.ste 1 T ime : 10 : 2 3
PHsk Area (A-s): 0.002 ~Jeak Heigrt i a •; 0.001
Blank Correctec Pk Height >. A ): 0.000
C^cent ration (ug/L ): 0.003
* lk%, tofc
H«§ IC". 152- 30- i Q'i? •^"^lec . *o. . 00023 A/2 Pea.: — Oat;
I
'eolioa-e i "i.ne: 10:24
Ares ' k~» v. 'JO;.- Pea:- Height *. A : 0.000
,:ih C-: r tad PV Height (A:: 0.000
»c*rrtrstior i uq.. •_ ;: 0.000
30-^3 Air Seq. No. : CO03? A,3 .: — Date: 09/26/9"
215
-------
i IC-z. *l'£ i
P^cLK Hi" ~r 3 ¦ ,w^"~5 ) I Q . -iO
SiaiM<. Corrected Pk Height (A);
Concentration (ug/L ): 0.011
Time: 10:25
Peak Height (A): 0.000
0.000
Hg2 10: 182-30-9CA8 D Sea. No.:
Replicate 1
Peak Area (A-s): 0.011
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
Hg2 ID: 182-30-9CAB MS Sea. No.:
Replicate 1
Peak Ares tA—s ): 0.010
81ank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.013
00040 A/3 Pos.: — Date: 09/26/97
Time: 10:26
Peak Height (A): 0.000
00041 A/S Pos.: — Date: 09/26/5"
Time: 10:27
Peak Height (A): 0.D01
Vi
Hg2 ID: 132-30-9CAB MS Seq. No.: 00042 A/S Pos.: — Date: 09/26/9"
Seo1icate i Time: 10:38
Peah Area (A-si: 4 .427 Peak Height (A): 0.18'-
Slank Corrected Pk Height (A): 0.1-39
Concentration (ug/L ): 5.05-
-ig2 10: 182-30-9CAB H3D Seq. No.:
dedicate 1
3eak Area (A-sj: 4.43^
3lank Corrected Pk Height i A ): 0.194
Concent ration (ug/L ): 5.176
00u4j A/; hos.: — gate: Qy / ibrt '
Time: 10:39
Peak Height (A): 0.19^
-ig2 ID: 132-50-llCAB Sec. No.: 00044 A/S Pos.: — Date: 09/26/9"
'.eolicate 1 Time: 10:40
Jeak Area
-------
Icentration (ug/L .): 5.668
-ifj ID: CCB3
^mlicate i
3*. Area ( A-s ): 0.022
jflnk Corrected Pk Height
Concentration (ug/L ): 0.
Seq. No.: 0004 7 A/S Pos.
(ft): 0.
021
001
Time: 10:43
Peak Height (A): 0.001
Date: 09/26/9"
ig2 ID: 182-30-12CAB
Seq. No.: 00048
^^jlicate 1
3eak Area (A-s ): 0.013
ik Corrected Pk Height
sentration (ug/L ): 0.
(A): 0
008
,000
I
}epi
Cone:'
I
l
10: 182-30-12CAE: 0
Replicate i
Area (A-s;: 0.012
ik Corrected Pk Height
;.o"ncentration (ug/L ): 0.
(A): 0
013
001
ID: I82-30-13CAB
'.^¦.icate l
3i=B: Area (A-s): 0.001
Slank Corrected Pk Height
-c*ent ration (ug/L ): 0.
(A): 0,
003
000
A/3 Pos.: —
Date: 09/26/9"
Time: 10:44
Peak Height (A): 0.000
Seq. No.: 0004 9
Pos
Date: 09/26/9-
T i me: 10:43
Peak Height (A-: 0.001
Seq. No.: 000 50
ft/3 Pos
Date: 09/2t-..
7i;ine: 10:47
Peak Height (A); 0.000
Jem
ID: 182-30-13CA8 D
Seq. No.: 00051
Date: 09/26.
PilCct^C X.
3eak Area (A-s): 0.007
JlBik Corrected Pk Height
-Jk
i line: 10:47
Peak Height (A): 0.000
pentration (ug/L ): 0
(A;: 0.
003
000
I
ID: 182-30-146A8
Seq. No.: 00052 A/3 Pos.: — Date: 09/26/9"
lei^icate 1
'el Area (A-s): 0.007
Si™ k Corrected Pk Height
".oncentration (ug/L ): 0.
Time: 10:49
Peak Height (A): 0.000
(A): 0.
011
000
Ig2 ID: 182-30-14GA8 0
.icate 1
'e?R A rea ( A—s ): 0.004
ilank Corrected Pk Height
¦ojentration (ug/L ): 0.
Sec. No.: 00053 A/S Pos.: -- Date: 09/26/9:
(A): 0.
019
001
Time: 10:50
Peak Height (A): 0.001
217
-------
Hg2 ID: 182-30-1C
Date: 09/26/9'
Reolicate l
Peak Area (fl-s i: 0.83?
Blank Corrected Pk Height (A):
Concentration (ug/l ); 0.995
Time: 10:51
Peak Height (A): 0.037
0.037
Hg2 ID: 132-30-1C 0 Seq. No.: 00055 A/S Pos.: — Date: 09/26/9T
dedicate 1 Time: 10:52
Psak Area (A-s): 0.90? Peak Height (A): 0.03S
Blank Corrected Pk Height (ft): 0.038
Concentration iug/L !: 1.003
Hg2 ID: 1S2-30-2C Seq. No.: 00056 A/3 Pos.: ~ Date: 09/26/9"
P-eo 1 icate 1 T ime: 10: 53
Peak Area (A— ? i: 0.837 Peak Height (A): 0.035
Blank Corrected Pk Height (A): 0.035
Concentration (ug/L 0.941
He2 10: 182-30-2C D Sea. No.: 00057 A/3 Pos.: — Date: 09/26/*"
Reolicate 1 Time: 10:54
Peak Area (A-s ): 0.765 Peak Height (A): 0.03C
3lank Corrected Pk Height (A): 0.032
Concentration (ug/L ): 0.845
Hg2 ID: CCV4=6.0ug/L Seq. No.: 00056 A/S Pos.: — Date: 09 '26/9"
Seolicate 1 T i me: 10:55
Deak Area (A-s): 4.943 Peak Height (A;: 0.211
Blank Corrected Pk Height (A): 0.211
Concentration (ug/L !: 5.625
ig2 ID: CC84 Sea. No.: 00059 A/3 Pos.: — Date: 09/26/?
^eoiicate 1 Time: 10:56
3eak Area (A-s>: 0.027 Peak Height (A ): 0.001
31ank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.029
ta2 ID: 182-30-3C Seq. No.:
Reolicate 1
Jeak Area (A-s): 0.90°
3lank Corrected Pk Height (A): 0.033
Concentration (ug/L ): 1.021
00060 A/S Pos.: — Date: 09/26/9
Time: 10:58
Peak Height (A): 0.03S
ID: 132-30-3C 0 Seq. No.: 00061 A/S Pos.: — Date: 09/26/97
218
-------
sol,
2ak
lw
I
eoiicate 1
eak Area (A-s): 0.857
1JBk Corrected Pk Height (A): 0.03*
D™entr3tion (ug/L ): 1.024
Time: 11:05
Peak Height (A 1: 0.03£
ID: 182-5S-1
Sea. No.: 00062
A/S Pos.: —
Date: 09/26/9"
etj^icate 1
sM Area (A-s): 0.203
iJflk Corrected Pk Height (A): 0.00S
Dncentration (ug/L ): 0.222
Time: 11:06
Peak Height (A): 0.008
I
ID: 182-58-1 0
Seq. No.: 0006'
A/3 Pos.
Date; 09/26/9"
Jioate 1
Area (A-s): 0.197
lnceritration 'ug/L i: 5.17c,
7 i iTie : 11:09
PeaK Heiqht <: A): 0.19a
3D: 182-58-1 M3D
Seq. No.: 00065 A/3 Pos
Date: 09/26/9"
Iicate 1
Area (A-s): 4.313
Lank Corrected Pk Height i A): 0.185
;ntration (ug/L ): 4.920
Time: 11:10
Peak Height (A): 0.18 5
i:
i
ID: 182-58-2
Sea. No.: 00066 A/S Pos.: — Date: 09/26/9"
'CWxcaxe 1
:ak Area (A-s): 0.237
« Corrected Pk Height ifi): 0,010
r
Time: 11:11
Peak Heiaht (A): 0.010
>r^ntration (ug/L ): 0.257
1
ID: 182-58-2 D
Sea. No.: 00u6? A/S Pos.
Date: 09/26/97
©licate 1
*Area (A-s): 0.216
Corrected Pk Height (A): 0.009
sncentrstion (ug/L J: 0.235
Time: 11:12
Peak Height (A): 0.00Q
ID: 182-58-3
Seq. No.: 00068 A/S Pos
a" (
icata 1
Area (A-s ); 0.425
ank Corrected Pk Height (A); 0.018
Time: 11:14
Peak Height (A): 0.018
I
Date: 09/26/97
219
-------
Concentration (ug/L 5: 0.471
Hg2 ID: 182-58-3 D Seq. No.; 00069 A/S Pos.: — Date; 09/26/9"
^eolicate 1 Time: 11:15
=>eak Area (A-s)r 0.394 Peak Height (A): 0.016
31ank Corrected Pk Height (A): 0.016
Concentration (ug/L ): 0.436
J.c2 ID: CCV5=6.Oug/L Seq. No.: 00070 A/S Pos.: — Date: 09/26/97
-------
Hq;
ID: 182-30-130
Sea. No.: 00076 A/S Pos.:
Date: 09/26/9"
icate 1
Peak Area (A-s ): 0.040
B^nk Corrected Pk Height (A): 0.002
icentration (ug/L ): 0.045
Time: 11:24
Peak Height (A): 0.002
I
ID: 132-30-130 0
Seq. No.: 00077 A/3 Pos.: — Date: 09/26/9:
Replicate 1
Area (A-s): 0.038
3^nK Corrected Pk Height (A): 0.001
Concentration iug/L ): 0.035
Time: 11:25
Peak Height (A): 0.001
I
t
anl-
I
ID: 182-30-1D
Seq. No.: 0007S A/3 Po=
Date: 09/26/9"
teBI icate 1
Area (A-s?: 0.014
Slank Corrected Pk Height (A): 0.001
o*entration (ug/L ): 0.01°
Time: 11:26
Peak Height (Ai: 0.00.5
ID: 182-30-ID D
Seq. No.: 0007°
A/3 Pos.:
Date: 09/Zb'e-
efn icate 1
eak Area (A-s !: 0.012
l
-------
teolicate 1
>eak Area (A-s ): 0.02?
ilank Corrected Pk Height (A); 0.
concentration (ug/L ): 0.02?
001
Time: 11:32
Peak Height (A): 0.001
ID: 182-30-1F
Sea. No.: 00084
A/S Pos,
Date: 09/26/9"
epiicate 1
eak Area (A-s): 0.050
lank Corrected Pk Height (A):
oncentration (ug/L ): 0.048
Time: 11:33
Peak Height (A): 0.002
0.002
32 10: 132-30-1F 0 Sea. No.: 00085 A/S Pos.: — Date: 09/26/9"
?clicate 1 Time: 11:36
?ak Area (A-s): 0.039 Peak Height (A): 0.002
'.ank Corrected Pk Height (A); 0.002
)ncentration (ug/L ): 0.043
•2 10: 182-30-IF MS Sec.. No.:
olicats 1
ak Area (A-s): 4.16-'
ank Corrected Pk Height (A): 0.173
ncentratioR (ug/L ); 4.604
OOOSt- A/3 Pos.: — Date: 09/26/9"
Time: il;37
Peak Height (Ac 0.173
2 ID: 132-30-IF HS0 Sea. No.: 0008? A/S Pos.: — Oats: 09/26/9"
olicats 1 Time: 11:33
ik Area (A-si: 4.08£ Peak Height (A): 0.171
ink Corrected Pk Height (A): 0.171
icentration (ug/L ): 4.559
10: 182-30-20 Seq. No.:
¦lioate 1
k Area (A-s): 0.031
nk Corrected Pk Height (A): 0.001
cent ration (ug/L ): 0.024
00088 A/S Pos.: — Date: 09/26/9"
Time: 11:39
Peak Height (A): 0.001
10: 132-30-2D 0 Sea. No.: 00089 A/S Pos.: — Date: 09/26/9"
licate 1 Time: 11:40
< Area (A-s): 0.018 Peak Height (A): 0,000
ik Corrected Pk Height (A): 0.000
:entration (ug/L ): 0.011
ID: 182-30-2E Seq. No.:
. icate 1
Area (A-s): 1.750
k Corrected Pk Height (A): 0.07 5
00090 A/S Pos.: — Date: 09/26/9"
Time: 11:41
Peak Height (A): 0.075
999
-------
:J(tration (ug/L ): 1.987
l
ID: 182-30-2E 0
Seq. No.: 00091 A/3 Pos
Oate: 09/26/«
Li^ate i
; B-ea (A-s ): 1.713
ikftorrected Pk Height (A): 0.072
:etitration i uq/L ): 1.928
Time: 11:43
Peak Height (A): 0.072
I
ID: 182-30-2F
Seq. No.: 00092 A/S Pos.
Date: 09/26/^
i*te 1
Hrea !A-s i: 0.037
kXorrected Pk Height (.A): 0.001
eMration (ug/L ): 0.032
Time: 11:44
Peak Height (A): 0.001
I
D: 132-30-2F 0
Seq. Ho.: 00093 A/S Pos.:
Oate: 09/26'"'°
icate i
iijisa •' A-s : 0. Oz8
kMorrected Pk Height !A): 0.001
=rffratiori (ug/L >: 0.01°
Fiitie: 11:45
Peak Heighx (A): C.001
1
te
a (A-s ): 4.723
; Corrected Pk Height (A): 0.201
m^ation (ug/L ): 5.355
D: CCV7=6.0ug/l
cs 1
Seq. No.: 00094 A/S Pos.:
Oate: 09/26/*?
Time: 11:3-6
Peak Height (A): 0.201
ID: CC8?
Seq. No.: 0009;
A/3 Pos.:
Oate: 09/26/9
ds 1
Area (A-s ): 0.02^
frrected Pk Heiqht (A): 0.001
ation (ug/L ): 0.016
%
1
Time: 11:47
Peak Height (A): 0.001
|: 132-30-30
cate 1
(A~S): 0-0-5
cBhrected Pk Height (A): 0.002
itration (ug/L ): 0.043
Seq. No.: 00096 A/S Pos.:
Date: 09/26/9
Time: 11:43
Peak Height (A): 0.002
-f
ID: 132-30-30 D
Sea. No.: 00097 A/S Pos.:
Date: 09/26/9
:aB 1
srll (A-s): 0.042
Corrected Pk Height (A): 0.002
itfiltion (ug/L ): 0.045
Time: 11:49
Peak Height (A): 0.002
*
-------
Hg2 ID: 182-30-3E Sea. No.: 00098 A/S Pos.: — Date: 09/26/97
Replicate 1 Time: 11:50
Peak Area (A-s ): 1.414 Peak Height (A): 0.060
Slank Corrected PR Heiqht (A): 0.060
Concentration (ug/t ): 1.591
Hg2 ID: 182-30-3E 0 Seq. No.: 00099 A/S Pos.: — Date: 09/26/97
Replicate 1 Time: 11:51
Peak Area (A-s): 1.366 Peak Height (A): 0.057
Blank Corrected Pk Height (A): 0,057
Concentration (ug/L ): 1.524
Hg2 ID: 182-30-3F Seq. No.: 00100 A/3 Pos.: — Date: 09/26/9"
Reolicate 1 Time: 11:52
3eak Area (A-s): 0.034 Peak Height (A): 0.001
31ank Corrected Pk Heiqht (A): 0.001
Concent ration (ug/L ): 0.032
Ig2 ID: 182-30-3F 0 Seq. No.: 00101 s/S Pos.: — uate: 0'?''26'?~
leDlicate 1 Time: 11:53
eak Area ( A-s ): 0.02° Peak Height. ( Ai: 0.001
lank Corrected Pk Height (A>: 0.001
oncentration (ug/L ): 0.027
?2 ID: 132-30-4C Seo. No.: 00102 A/3 Pos.: — Date: 09/:6/9"
solicate 1 T ime: 11:54
2ak Area (A-s): 0.02t Peak Height (A): 0.001
lank Corrected Pk Heignt (A): 0.001
oncentration (ug/L ): 0.021
i2 ID: 132-30-4C D Seq. No.: 00103 A/S Pos.: — Date: 09/26/9'
•clicate 1 Time: 11:55
ak Area (A-s ): 0.G29 Peak Height (A): 0.001
ank Corrected Pk Height (A): 0.001
ncentration (ug./L ): 0.024
2 ID: 182-30-40 Seq. No.: 00104 A/S Pos.: — Date: 09/26/97
olicate I 'Time: 11:56
ak Area (A-s): 1.575 Peak Height (A): 0.066
ank Corrected Pk Height (A): 0,066
icentration (ug/L ); 1.754
ID: 182-30-4D 0 Seq. No.: 00105 A/S Pos.: — Date: 09/26/97
224
-------
A]
licate 1
Peak Area (A-s): 1.470
nk Corrected Pk Height
Time: 11:57
Peak Height (A); 0.06'
:v
cm centration Cug/L ): 1
(A): 0.062
644
Replicate 1
3^|k Area (A-s): 4.704
3k Corrected Pk Heiqht
oncentr3tion (ug./L ): 5,
ID: CCV8=6.Oug/L
Seq. No.: 00106 A/S Pos.:
Date; 09/26/9"
(A): 0.200
329
Time: 11:59
Peak Height (A): 0.200
1
ID; CCE3
Seq. No.: 00107
A/S Pos
Date: 09/26/9•
.icate 1
A res i A-s ): 0.02 >3
!lank Corrected Pk Height
:olfentration tug/L ): 0.
Time: 12:00
Peak Height (A): 0.00J
!
(A): 0.001
024
Qi
ID: 132-30-40 HS
3eq. No.: 00103 A/S Pos.:
Date: 09/26/9'
e™ icate 1
eak Area (A-s): 5.634
iJBk Corrected Pk Height
owentration tug/L !: 6.
:¦
JiW
I
rime: 12:01
Peak Height iA ): 0.23<
(A): 0,236
294
ID: 182-30-40 M30
Seq. No.: 00109
.cate 1
Area (A-s): 5.433
Corrected Pk Heiqht
>ncentration (ug/L ): 6.
iA): 0.227
058
Time: 12:02
Peak Height (A): 0.227
Date: 09/26/9"
I
ID: 182-30-4E
Seq. No.: 00110 A/S Pos.:
D Beats L
ak Area (A-s): 0.053
Corrected Pk Height
nsHntration (ug/L ): 0.
(A): 0.002
043
rime: 12:04
Peak Height (A): 0.002
Date: 09/26/9T
2^ ID: 132-30-4E D
3licate 1
3rW*rea (A-s): 0.033
a® Corrected Pk Height
icentration (ug/L ): 0,
Seq. No.: 00111
A/S Pos.:
Time: 12:05
Peak Height (A): 0.001
(A): 0.001
032
Date: 09/26/9-
ID: 132-30-5C
Seq. Nc
ooii;
A/S Pos.
Date: 09/26/97
illlfcate 1
k'Jirea (A-s): 0.023
nk Corrected Pk Height (A): 0.001
Time: 12:06
Peak Height (A): 0.00]
I
225
-------
Concentration (ug./L ): 0.027
ig2 ID: 182-30-3C D Seq. No.: 00113 A/S Pos.: — Date: 09/26/97
teplicate i Time: 12:07
•eak Area (A-s ): 0.027 Peak Height (A): 0.001
ilank Corrected Pk Height (A): 0.001
oncentration (ug/'L ): 0.027
g2 ID: 182-30-5D Seq. No.: 00114 A/S Pos.: — Date: 09/26/9"
eplicate 1 Time: 12:08
eak Area (A-s): 1.233 Peak Height (A): 0.052
lank Corrected Pk Height (A): 0,052
oncentration (ug./L ): 1.332
?2 ID: 132-30-SD D Seq. No.:
?Dlicate 1
•al- Area (A-s): 1.154
.ank Corrected Pk Height (A): 0.04-7
>ncentration ! ug./L ): 1.257
00115 A/S Pos.: — Date: 09/26/9
Time: 12:09
Peak Height (A ); 0.04 7
2 ID: 182-30-5E Seq. No.:
olicate 1
3k Area 'A-s j: 0.031
ank Corrected Pk Height (A): 0.001
ice nt rat ion (ug/'L ): 0.021
0011c- A/S Pos.: — Date: 09/26/97
Time: 12:10
Peak Height (A): 0.001
? ID: 182-30-5E D Seq. No.: 00117 A/S Pos.: — Date: 09/26/97
:1ica te 1 Time: 12:12
tk Area (A-s ): 0.024 Peak Height (A): 0.001
ink Corrected Pk Height (A): 0.001
icentration (ug/L .): 0.029
ID: uCV9=6.0ug/L Seq. No.:
licate 1
k Area (A-s): 4.922
nk Corrected Pk Height (A): 0.212
centration (ug/L ): 5.663
00118 A/S Pos.: — Date: 09/26/97
Time: 12:13
Peak Height (A): 0.212
ID: CCB9 Seq. No.:
Licate 1
I Area (A-s): 0.016
ik Corrected Pk Height (A): 0.000
rent ration (ug/L ): 0.011
00119 A/S Pos.: — Date: 09/26/97"
Time: 12:15
Peak Height (A): 0.000
-------
a2 ID: 182-30-6C
Seq. No,: 00120 A/S Pos.:
Date: 09/26/9"
1
eijicate 1
eak Area (A-s): 0.016
luk Corrected PR Heiqht (A): 0.000
oiBentration (ug/L ): 0.008
Time: 12:16
Peak Height (A): 0.00G
I
ID: 132-30-6C 0
Seq. No.: 00121 A/S Pos.
Date: 09/26/9"
eolicats 1
Area (A-s ): 0.015
lw< Corrected Pk Heiqht (A): 0.001
Dncentration (ug/L ): 0.013
Time: 12:17
Peak Height (A): 0.001
ID: 1S2-30-6D
Seq. No.: 00122 A/S Pos.: — Date: 09/2&/9"
icate i
Area (A-s): 1.167
lank Corrected Pk Height (A): 0.049
xtent ration ¦ ug/L J: 1. 2V?
Time: 12:13
Peak Height (A): 0.04^
ID:
I
sk
I
1
50-oD 0
Seq. No.: 00123 A/S Pos.: — Date: 0-/26/9"
'oTLcate I
;ak Area (A-s): 1.120
.aft Corrected Pk Heignt (A : 0.046
>n«ntration i ug/L ): 1.238
Time: 12:i9
Peak Height (A): 0.04.;
50-6E
Seq. No.: 00124 A/S Pos.: — Date: 09/26/9'
~ ycate i
aArea (A—s ): 0.05^
aM Corrected Pk Heiqht (A): 0.002
ncentration (ug/L ): 0.059
Time: 12:20
Peak Height (A): 0.001
ID: 182-30-6E 0
s Mpate 1
ak Area (A-s;: 0.053
ank Corrected Pk Heiqht (A): 0.002
¦xJptration (ug/L ): 0.056
Seq. No.: 00125 A/S Pos.: — Date: 0972t/9"
Time: 12:21
Peak Heiaht (A»: 0.002
2 fl ID: 182-30-11E
I
Seq. No.: 0012& A/3 Pos.:
micate 1
ik^rea A-s <: 0.012
?rB Corrected Pk Heiqht (A): 0.000
lcWtration ( ug/L ): 0.005
Time: 12:22
Peak Heiqht (A j: 0.000
Date: 0?/26.;9"
[D: 1S2-30-11E D
Seq. No.: 0012? A/S Pos,
I
Date: 09/26/9"
221
-------
. iOctte 1
. Area i A-s j: 0.014
lk Corrected Pk Heicjnt (A):
:e nx rat 1 on i. ug / L J: 0. C11
Time: 12:23
Peak He iaht (A ): 0.000
0.000
ID: CCV10=6.Qug/L Seq. No.:
.icate i
Area (A-s): 4.989
ik Corrected Pk Height (A): 0.213
entration (ug/L ): 5.679
00128 A/S Pos.: — Date: 09/2
Tiitie: 12:24
Peak Height (A): 0.213
ID: CCB10 Seq. No.: 00129 A/S Pos.: — Date: 09/2fc/9~
icate i Time: 12:25
Area (A-s): 0.030 Peak Height (A): 0.001
R Corrected Pk Height (A): 0.001
entration (ug/L ): 0.021
ID: 43159A ME 2 Sec. No.: 00130 A/3 Po-=.: — Date: 09/26/?*"
icar.s J. Time: 14:00
Are?. (A-s): 0.006 Peak Height < A i: 0.000
k Corrected Pk Height (A): 0.000
entration (ug/L ): 0.005
10: 43159A HB2 D Seq. No.: 00131 A/S Pos.: — Date: 09/26/9""
icate 1 lime: 14:01
Area (A-s): 0.006 Peak Height (A): 0.000
k Corrected Pk Height (A): 0.000
antration (ug/L ): 0.000
ID: 43159ALCS2 Sea. No.: 00132 A/3 Pos.: — Date: 09/26/9"
^ to •1-^1 tC
icata 1 Time: 14:03
Area (A-s): 4.558 Peak Height (A): 0.193
< Corrected Pk Height (A): 0.193
=ntration (ug/L ): 5.139
ID: 43159A LCS2 0 _ Seq. No.:
•X? ec
icate 1
Area (A-s): 4.661
< Corrected Pk Height (A): 0.198
2ntration (ug/L }: 5.280
00133 A/S Pos.: — Date: 09/26/97
Time: 14:03
Peak Height (A): 0.198
ID: 182-30-11F Seq. No.:
icate 1
Area (A-s): 0.081
t Corrected Pk Height (A): 0.003
00134 A/S Pos.; — Date: 09/26/97
T ime: 14:04
Peak Height (A j: 0.003
228
-------
cWitration (ug/L ): 0.075
I
ID: 182-30-11F 0
Seq. No.; 00135 A/S Pes.:
Date: 09/26/9"
Ijpate 1
kpjrea (ft-s ): 0.060
nK Corrected Pk Height
castration (ug/L ): 0.
Time: 14:05
Peak Height (ft): 0.002
I
v A
I
1
(ft): 0.002
0fe4
ID: 132-30-11F MS
1
1 ^ate 1
k Area (A-s ): 4.6S3
ntoCorreoted Pk Height
c»t ration (ug/L !: 5.
D: 132-30-11F MSD
Seq. No.: 00136 A/S Pos.:
Date: 09/26/9:
Time: 14:06
Peak Height (A): 0.201
(A ): 0,201
3fcl
Seq. No.: 00137 A/3 Pos.:
Date: 09/26/9"
iicate 1
kiBrea ( A-s ): 4 .696
njcorreoted Pk Height
ce n t ra 11 on ( ug / L ): 5
Time: 14:u7
Peak Height (A): 0.200
A ) ; 0.200
I
-flc
;
10: CCVl=fr,0u:
Seq. No.: 00138
P'X
Date: 09/2b<":
i Bate 1
k ™rea (A-s): 5.292
nk Corrected Pk Heiaht
;fr"ioniu9/L :5
¦I
iicate 1
k area (A-s); 0.031
nMcorreoted Pk Height
cwrtration (ug/L ): 0.
Time: 14:08
Peak Height (A!: 0.
(A): 0.222
909
,10: C-CB1
Seq. No.: 0013°
Pos.:
Date: 09/26/9"
Time: 14:10
Peak Height (A): 0.001
(A): 0.001
021
010: 182-30-116
l^ate 1
< Brea (A-s ): O.Olt-
nk^Oorrected Pk Height
:entration (ug/L ): 0.
Seq. No.: 00140
Pos. :
(A): 0.000
008
Time: 14:11
Peak Height (A): 0.000
Date: 09/26/9"
ID: 182-30-11G D
Seq. No.: 00141 A/3 Pos.:
¦4s1
: Mrs
ilcXc
~
I
lifcte i
< wrea (A-s ): 0.023
ik^orrected Pk Height
;ration (ug/L ): 0.
(A): 0.001
019
Time: 14 til-
Peak Height (A): 0.001
Date: 09/26/9"
229
-------
2 ID: 132-30-12E
Date: 09/26/97
plicate 1
ak Area (A-s): 0.010
ank Corrected Pk Height (A):
ncentration (ug/L ): 0.008
Time: 14:13
Peak Height (A): 0.000
0.000
2 ID: 182-30-12E D Seq. No.:
dlicate 1
ik Area (A-s): 0.008
ink Corrected Pk Height (A): 0.000
icentration (ug/L ): 0.008
00143 A/3 Pes.: — Date: 09/26/97
Time: 14:14
Peak Height (A): 0.000
ID: 182-30-12F Seq. No.:
licate 1
k Area (A-s): 0.064
nk Corrected Pk Height (.A): 0.002
centration (ug/L ): 0.064
00144 A/S Pos.: — Date: 09/26/97
Time: 14:IS
Peak Height (A): 0.002
10: 182-30-12F D Seq. No.: 00145 A/S Pos.: — Date: 0*/26/9T
licate 1 Time: 14:15
< Area (A-s): 0.060 Peak Height (A): 0.002
ik Corrected Pk Height (A): 0.002
:entration (ug/L ): 0.061
10: 182-30-126 Seq. No.:
icate 1
Area (A-s): 0,009
k Corrected Pk Height (A): 0.001
entration (ug/L ): 0.019
00146 A/S Pos.: — Date: 09/26/9
Time: 14:16
Peak Height (A): 0.001
10: 132-3Q-12G 0 Seq. No.:
icate 1
Area (A-s): 0.007
< Corrected Pk Height (A): 0.000
?ntration (ug/L ): 0.005
00147 A/S Pos.: — Date: 09/26/97
Time: 14:17
Peak Height (A): 0.000
10: 182-30-13E Sea. No.:
.oate I
A rea (A—s ): 0.004
: Corrected Pk Height (A): 0.000
ntration (ug/L ): 0.008
00148 A/S Pos.: — Date: 09/26/97
Time: 14:19
Peak Height (A): 0.000
ID: 182-30-13E D Seq. No.: 00149 A/S Pos.: — Oate: 09/26/97
230
-------
Replicate i Time; 14:19
Peak Area (ft-s): 0.006 Peak Height (A): 0.000
sBnk Corrected Pk Height (A): 0.000
C
-------
Concentration (ug/l ): 0.019
Hg2 ID: 182-30-8A 0 Seq. No.: 00157 A./S Pos. : — Date: 09/26/9"
Replicate 1 Time: 14:28
Peak Area (A-s): 0.001 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0,000
Concentration (ug/L ): 0.005
Hg2 ID: 1S2-30-8D-1SC Sea. No.: 00158 A/S Pos.: — Date: 09/26/9":
Replicate 1 Time: 14:29
Peak Area (A-s): -0.002 Peak Height (A); 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
Ha2 ID: 132-30-30-15C 0 Seq. No.: 0015° A/S Pos.: — Date: Q9/2t>/9'
Reolicate 1 Time: 14:3u
Peak Area (A-s ;: 0.003 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.00S
Ha2 10: 132-30-14E Seq. No.: 00160 A/S Pos.: — Date; 09/26/?"
Replicate 1 "irce: 14:31
^eak Area (A-s): 0.002 Peak Height (A): 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
Hg2 ID: 132-50-14E D Seq. No.: 00161 A/S Pos.: — Date: 09/26/9"
Replicate I Time: 14:32
3eak Area (A-s): 0.005 Peak Height (A); 0.000
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.000
4g2 ID: CCV3=6.0ug/L Seq. No.: 00162 A/S Pos.: — Date: 09/26/9:
Replicate I Time: 14:33
>eak Area (A-s): 5.247 Peak Height (A): 0.22S
Blank Corrected Pk Height (A): 0.228
Concentration (ug/L ): 6.083
ta2 ID: CCB3 Seq. No.: 00163 A/S Pos.: — Date: 09/26/91
Replicate 1 Time: 14:34
5eak Area (A—s ): 0.028 Peak Height (A): 0.001
3lank Corrected Pk Height (A): 0.001
ioncentration (ug/L ): 0.032
232
-------
q2 10: 182-30-7F Sea. No.: 00164 A/S Pos.: — Date: 09/26/97
¦
eJBicate i Time: 14:35
eak Area (A-s): 0.014 Peak Height (A): 0.000
Corrected Pk Height (A): 0.000
eventration (ug/L ): 0.005
I
ID: 182-30-7F D Sep. No.: 00165 A/S Pos.: — Date: 09/26/9:
leplicate i Time: 14:36
¦e® Area ( A-s): 0.016 Peak Height (A): 0.001
ilp»k Corrected Pk Height (A): 0.001
:oncentration (ug/L ): 0.013
IgP ID: 132-30-8DE15C Seq. No.: 00166 A/S Pos.: — Date: 09/26/9'
-------
•plicate i
iak Area (A-s): -0.001
.ank Corrected Pk Height (A):
sncentration (ug/L ): -0.003
Time: 14:44
Peak Height (A): -0.000
-0.000
i2 ID: 182-30-14EF Seq. No.:
splicate 1
iak Area (A-s): -O.O'll
.ank Corrected Pk Height (A): -0.001
jncentration (ug/L ): -0.013
00172 A/S Pos.: ~ Date: 09/26/9"
Time: 14:45
Peak Height (A): -0.001
i2 ID: 182-30-1+EF D Seq. No.: 00173 A/S Pos.: — Date: 09/26/91
•plicate 1 Time: 14:46
•ak Area (A-s): -0.016 Peak Height (A): -0.001
.ank Corrected Pk Height (A): -0.001
mcentration (ug/L ): -0.013
(2 10: CCV4=6.0ug/L Seq. No.: 00174 A/3 Pos.: — Date: 09726/?'
'plicate 1 Time: 1^:46
•ak Area (A-s ): 5.195 Peak Height (A?: 0.228
.ank Corrected Pk Height (A): 0.228
>ncentration (ug/L !: 6.064
\7 10: CC84 Seq. No.:
;d 1 icate 1
iak Area ( h-s ): 0.020
.ank Corrected Pk Height (A): 0,001
>ncentration ( ug/L ): 0.032
00175 A/S Pos.: — Date: 09/26/'?"
Time: 14:47
Peak Height (Ac 0.001
i2 ID: 1S2-30-13G MS Seq. No.: 00176 A/3 Pos.: — Date: 09/26/9"
•plicate l Time: 14:48
iak Area (A-s): 4.457 Peak Height (A.): 0.193
.ank Corrected Pk Height (A): 0.193
>ncertration (ug/L ): 5.139
l2 ID: 182-30-136 MS0 Seq. No.: 00177 A/S Pos.: — Date: 09/26/9"
iplicate 1 Time: 14:49
:ak Area (A-s): 4.561 Peak Height (A): 0.191
.ank Corrected Pk Height (A): 0.191
ncentration (ug/L ): 5.096
|2 ID: 182-30-9F15B Seq. No.: 00178 A/S Pos.: -- Date: 09/26/97
•Dlicate I Time: 14:50
:ak Area (A-s): 0.030 Peak Height (A): 0.001
.ank Corrected Pk Height (A): 0.001
234
-------
icentration (ug/L ): 0.02°
I
ID: 182-30-9F15B D Sea. No.: 00179 A/S Pos.: -- Date: 09/26/9:
licate 1 rime: 14:51
K Area (A-s): 0.014 Peak Height (A): 0.000
ank Corrected Pk Height (A): 0.000
centration (ug/L ): 0.008
Hg2 ID: CCV5=6.0ug/L Seq. No.: 00180 A/S Pos.: — Date: 09/26/9:
licate 1 Time: 14:52
Peak Area (A-s): 5.285 Peak Height (Ai: 0.228
»nk Corrected Pk Height (A): 0.228
centration (ug/L ): 6.069
f
ID: CC85 Sea. No.: 00181 A/3 Pos.: — Date: 09/26/9!
Reolicate 1 rime:_,14:53
Ftatk Area (A-s): 0.028 Peak Height (A): 0.001
cjank Corrected Pk Height (A); 0,001
Concentration (ug/L ): 0.024
-------
I0/Weight File: A8811.IDW
Sample Volume: 100 mL
Analyst: RICHARDS
Nominal Weight: 1.0 g
-OC .
0
1
3
4
5
6
-7
3
9
10
11
12
13
14
15
16
17
IS
19
20
21
22
4m O
24
25
26
27
23
29
30
31
32
33
34
35
36
37
38
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
Sample ID
STD 8IK
sl^H)l=0.2ug/L
~*ST02=Q. 5ug/L
ST03=1.0ug/L
STD4=2.Oug/L
STD5=5.Oug/L
STD6=10.Oug/L
ICV=4. 0ug./l
IC8
CHECK LO
43159A h83
43159A
43159A
43159A
43159A
182-30-9E
L82-30-9E
182-30-9E
182-30-9E
182-30-7E
1S2-30-7E
CCV1=6.Oug/L -
CC81
182-30-14D
182-30-140 0
182-30-15B
132-30-158 0
182-30-15C
182-30-ISC D
CCV2=6.Oug/L
CC32
43231 ME1
43231 M81 D
43231 LCS1
43231 I.CS1 D
183-3-2C
183-3-2C D
183-3-2C MS
133-3-2C USD
183-3-1B
183-3-1B 0
CCVl=t>. Oug./ L -
CC81
183-3-1C
183-3-1C D
183-3-1D
133-3-10 DX10
183-3-10 DDX10
183-3-IE
183-36-1E D
183-3-2B
183-3-2E 0
183-3-2D
183-3-2D D
Weight
Dilution
3-OIS--7
3-oi%-r 1M171"*-
LCSJO
>re-p^P
cla
GV> tO
,/9?
"V ots- —Br
> t. -rf ''M"
-------
Sample ID
Weight
Oilution
55
58
65
I
63
I
I
75
I
78
i
81
f
85
«
88
I
91
98
105
108
1|
CCV2-6.Qug/L -
CCB2
183-3-2E >"i
.^a3-3-2£ 0 Z
""183-3-30
183-3-3C 0X5
183-3-3C 00X5
183-3-3C MSX5
183-3-3C M30X5
133-3-2F
183-3-2F 0
CCV3=6.Oug/L
CC83
183-3-38
183-3-38 0
183-3-30
133-3-30 0
183-3-3E v
183-3-3E 0/
183-3-3F
133-3-3F
CCV4-6.Oug/L
CC34
43231 MB2
43231 M82
43231 LCS
43231 LCS
v*
'*?
3-ot5r-
to
w
Krr
3-o(r^r
i|sd(qi
0
u
182
-4B
133-3-48 0
1S3-3-4C
183-3-4C 0
183-3-4C MSX2
183-3-4C HS0X2
CCV1=6.Oug/L —
CC61
183-3-40
183-3-40 0
183-3-4E
183-3-4E 0
183-3-4F
133-3-4F 0
183-3-5B
183-3-53 0
183-3-5C
183-3-5C D
CCV2 = 6.Oug/L
CCB2
183-3-50
183-3-50 0
183-3-5E
183-3-5E D
183-3-6C
183-3-6C 0X5
183-3-6C 00X5
183-3-6C MSX5
183-3-6C MS0X5
237
-------
Lcc
110
111
112
113
114
115
116
117
113
119
120
121
122
123
124
125
126
127
12S
129
130
131
132
133
134
135
136
137
138
139
140
141
142
143
144
145
146
147
148
149
Sample ID
Weight
(Dilution
183
183-
CCV3
CCB3
sgy -
183
183'
183
183'
183
183
183
183'
133
183
183
CCV4
CC34
183-
183-
183-
183
183'
1S3-
133-
183-
183
183-
CCV'5
CC35
183-
183-
183
183-
183
183
183
183-
183-
CCV6
CCB6
3-6B
3-6B D _
6.Oug/L -
3-60
3-6D D
3-c£
3~6E D
3-6F
3-6F D-
3-7B
3—7B D
3-7C
3-70 0X5
3-7C D0X5
-6.Oug/L
70 0
7E
3-7E 0
3-7E MS
3-7E MSO
3-7F
3-7F 0
3-86
3-85 0
=6.Oug/L
3-SC
3-8C 0X5
3-80 DDKS
3-80
3-80 D
3-36
3-8E D
3-8F
J-8F D
:6.Oug/L
l-o(r-r
viok
-------
.ement File: HG_.MEL
: Hq2
'ift Data: Hain+Suppl.
"im: Calib. Curve
.¦marks:
tOAROS= 3-018-7
3-0iB,^E.
{SjKUMENT: 5100
nJp.ength: 253.7 Peak
.gnal Type: AA
Lme: 30.0
i Replicates: 1
Replicates: i
L^pj Type: Air
-------
lenient File: HG_ . MEL
ate: 09/30/97
ata File: fiB811.DAT
echniaue: MHS
emark 1: STANDARDS: 3-
emark 2:_.J.Q£= 3-018-8
Element: Hg2
Time: 09:27
I0/Wt File: AB811.IDW
Calib. Type: Linear
Wavelength: 253."
_ Slit: 0.7 L
Lamp Current: 0
Energy: 72
g2 ID: STO SLK Seq. No.: 00003 A/S Pos.: — Date: 09/30/97
eplicate 1 Time: 09:28
eak Area (A-s); 0.002 Peak Height (A): -0.001
lank Corrected Pk Height (A): -0.001
oncentration (ug/L ): -0.026
uto-zero performed.
g2 ID: ST01=0.2ug/L Seq. No.:
eolicate 1
sak Area (A-s): 0.148
lank Corrected Pk Height (A): 0.006
oncentration (ug/L ): 0.160
tandard number 1 applied. [0.200]
~ .-relation coefficient: 1.00000
00004 A/S Pos.: — Date: 09/30/9*7
rime: 09:29
Peak Height (A): 0.OOt
Slope: 0.0281
g2 ID: STD2=0.5ug/L Seq. No.: 00005 A/S Pos.: -- Date: 09/30/9r
ample abs. is greater than that of the largest standard.
splicate 1 Time: 09:31
eak Area (A-s): 0.403 Peak Height (A): 0.016
lank Corrected Pk Height (A): 0.016
oncentration (ug/L ): 0.579
tandard number 2 applied. [0.500]
orrelation coefficient: 0.99265 Slope: 0.0320
32 10: 3T03-1.Oug/L Seq, No.: 00006 A/S Pos.: — Date: 09/30/97
ample abs. is greater than that of the largest standard.
eplicate 1 Time: 09:32
sak Area (A-s): 0.915 Peak Height (A); 0.037
lank Corrected Pk Height (A): 0.037
oncentration (ug/L ): 1.164
tandard number 3 applied. [1.000]
orrelation coefficient: 0.99169 Slope: 0.0362
32 ID: STD4=2.Oug/L Seq. No.:. 00007 A./S Pos.: -- Date: 09/30/97
ample abs. is greater than that of the largest standard.
splicate 1 Time: 09:33
eak Area (A-s): 1.749 Peak Height (A): 0.070
-------
irllf
icen
irJLr
itW Corrected Pk Height (A): 0.070
icentration < ug/L ): 1.941
irHferd number 4 applied, [2.000.1
-relation coefficient: 0.99822 Slope: 0.0354
2 10 : ~~S T05 - 5 . Ouq/ L Sec. No.: 00008 ' A/S Pes . : — Date: 09/30/97
ncS? abs. is qreater than that of the largest standard.
Dffcate 1 " Time: 09:35
ik Area (A-s): 4.656 Peak Height (A): 0.18-
arM Corrected Pk Height (A-}: 0.189
n
-------
Element File; HG_.M£L
Date: 09/30/97
Data File: A8811.QAT
Technique: HHS
Remark 1: STANDARDS^ 3-013-7
Remark 2: 3-018-8
Element: Hg2
Time: 09:34
I0/Wt File: AB811.IDW
Calib. Type: Linear
Wavelength: 2 53.7
Slit: 0.7 L
Lamp Current: 0
Energy: 72
N
Display Calibration - C:\ftA_USER\flfl_FILES\ELEMENT\HS_.HEL
0.370
0)
G
.X"
Linear
Corn. Coef.: 8.99982
Slope: 0,8371
Concentration
18.008
1
242
-------
E^ment File: HG_.MEL
Die: 09/30/97
oMa File: AB811.DAT
Technique: HHS-
R«'ark i: STANDARDS- 3-018-7
FlBark 2:.-i^ 3-018-8*
Element: Hg2'
Time: 09:38
IO/Wt File: A8811.IDW
Calib. Type: Linear
Wavelength: 253.7
Slit: 0.7 L
Lamp Current: 0
Energy: 72
Hi
10: ICV=4.0ug/L
Seq. No.: 00010
Reolicate 1
pBk Area (A=-s ): 3.815
Swlnk Corrected Pk Height (A): 0.157
Concentration (ug/L ): 4.229
I
Hq2
I
ID: ICB
Sea. No.
ftBlicate i
Peak Area (A-s ): 0.015
S^nk Corrected Pk Height (A): 0.001
cBce.itration (ug/L ): 0.014
ft/3 Pos.: —
00011
A / S Pos
Time: 0^:41
Peak Height (A): 0.001
Oate: 09/30/97
Time: 09_;39
Peak Height (A):" 0.157
-Date: 09/30/97
Rep 1icate 1
tk Area (A-s): 0.194
8*nk Corrected Pk Height (ft): 0.008
Concentration (ug/L ): 0.20S
I
Rep.
»r
:onc
f
31ar
I
ID: CHECK LO
Seq. No.: 000I2
Po;
Oate: 09/30/9"
Time: 09:42
Peak Height (A): 0.008
ID: 43159A HBl
Seq. No,
Oate: 09/30/9:
R® 1 icate 1
P®k Area (A-s): 0.009
8lank Corrected Pk Height (A): 0.001
Cgfcentration (ug/L ): 0.014 4
Time: 09:46
Peak Height (A!: 0.001
He
ID: 43159A MB3 D
Seq. No.: 00014
A/S Pos.: —
Date: 09/30/9:
RUl icate i
Peak Area (A-s): 0.018
3®nk Corrected Pk Height (A): 0.001
C®cent ration ( ug/L ): 0.038
Time: 09:47
Peak Height (A): 0.001
HI
ID: 43159A LCS3
Seq. NoT: 00015 A/S Pos.: —
Date: 09/30/9"
Reolicate T
Pl|k Area (A-s): 3.251
Blink Corrected Pk Height (A)f
Concentration (ug/L ): 3.574
Time: 09:48
Peak Height (A): 0.132
\eO
A
Ha2 10: 43159A LCS3
Seq. No.: 00016 A/S Be
Date: 09/30/97
243
-------
Replicate
3eak AreaCA^): 3.207
31ankj>?rrected Pk Height-
Co.
Time: 10:04
Peak Height (A): 0.134
Wit'
i 7
(A): 0.134
ID:._Jjo-159A LCS3
Seq. No.: 00017 . A/S Pos.
Oats: 09/30/9'
Reolicate 1
3eak Area (A-s ): 5.7S9
3lank Corrected Pk Height (A); 0.238
Concentration (ug/L ): 6.436
Time: 10:11
Peak Height (A).: 0.238
Hg2 ID: 43159A LCS3 JT Seq.
No.: 00018
A/S Pos.: —
Date: 09/30/9"
Replicate 1
3eak Area (A-s): 4.965
Blank Corrected Pk Height (A): 0,
Concentration (ug/L ): 5.534
205
Time: 10:13
Peak Height (A): 0.20!
ID; 43159A LC^D^
Seq. No.: 00019
A/S Pos.: —
Date: 09/30/9"
Replicate 1
3eak Area (A-s): 5.02?
Blank Corrected Pk Height (A): 0.213
Concentration (ug/L ): 5.753
Time: 10:19
Peak Height (A): 0.21*
Hg'
ID: 182-30-9E
Seq. No,: 00020
A/S Pos.
Date: 09/30/9"
Replicate 1
^eak Area (A-s): 0.100
Slank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.111
Time: 10:21
Peak Height (A): 0.004
Hg2 10: 132-30-9E D Seq.*No.: 00021 A/S Pos.: -- Oate: 09/30/9"
Replicate 1 Time: 10:22
Peak Area (A-s): 0.086 Peak Height (A): 0.004
Slank Corrected Pk Height (A): 0.004
Concentration (ug/L .): 0.100
Hg2 ID: 182-30-9E MS Seq. No.: 00022 A/S Pos.: — Oate: 09/30/97
Replicate 1 Time: 10:23
Peak Area (A-s): 4.535 Peak Height (A): 0.190
Blank Corrected Pk Height (ft): 0.190
Concentration (ug/L ): 5.131
Hg2 ID: 182-30-9E hSD Seq. No.: 00023 A./S Pos.: — Date: 09/30/9"
Replicate 1 Time: 10:24
Peak Area (A-s): 4.407 Peak Height (A): 0.183
Blank Corrected Pk Height (A): 0.183
244
-------
>rfcntration (ug/L ): 4.944
ID: 1S2-30-7E Seq. No.: 00024 A/S Pos.: — Date: 09/30/9:
;afcLcate 1 - Time: 10:25
Area ): 0.183 Peak Height (A): 0.007
Lank Corrected Pk Height (A): 0.007
jn^ntration ( ug./L ): 0.200
32 ID: 182-30-7E D Seq. No.: 00025 A/S Pee.: — Date: 09/30/9:
I
epBicate 1 Time: 10:26
2ak Area (A-s); 3.280 Peak Height (A): 0.138
1*< Corrected Pk Height (A): 0.138
X
Drfcntration (ug/L ): 3.736
I
splic
iM (
Law<
>nce
I
|2
53K
ID: CCV1=6.Oug/L Seq. No.: 00026 A/S Pos.: — Date: 09/30/97
spjjioate 1 Time: 10:30
Area (A-s): 5.025 Peak Height (A): 0.210
1JH< Corrected Pk Heignt (A): 0.210
Dncentration ( ug/L ): 5.664
ID: CCB1 Seq. No.: 00027 A/3 Pos.: — Date: 09/30/9:
3»icate 1 Time; 10:31
Area iA-s ): 0.039 Peak Height (A): 0.00'
l
-------
2 ID: 182-30-156 D ' Seq. No.: 00031 ' A/S Pos.: — Date: 09/30/97
Dlicate i Time: 10:40
ak Area (A-s.): 0.017 Peak Height (A): 0.001 _
ank Corrected Pk Height (A), 0.001
ncentration (ug/l ): 0.024
2 ID: 132-30-15C Seq. No.: 00032 A/S Pos.: — Date: 09/30/9"
plicate 1 rime: 10:42
ak Area (A-s): 0.022 Peak Height (A): 0.001
ank Corrected Pk Height (A): 0.001
nceritration (ug/L ): 0.035
2 ID: 182-30-15C D Seq. No.: 00033 A/S Pos.: — Date: 09/30/9-
¦plicate 1 Time: 10:43
ak Area (A-s): 0.045 Peak Height (A): 0.002
ank Corrected Pk Height (A): 0.002
>ncentration (ug/L ): 0.057
i2 10: CCV2=6.Oug/L Seq. Mo.:
»Dlicate 1
»ak Area (A-s): 4.370
.ank Corrected Pk Height (A): 0.191
>ncentration (ug/L ): 5.150
00034 A/3 Pos . : — Date: 09/30/9""
Time: 10:44
Peak Height (A): 0.191
32 ID: CCB2 Seq. No.: 00035 A/3 Pos.: — Date: 09/30/9T
JDlicate 1 Time: 10:45
2ak Area (A-s): 0.035 Peak Height (A): 0.001
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.038 *
a2 ID: 43231 M81 Seq. No.: 00036 A/S Pos.: — Date: 09/30/97
eplicate 1 Time: 10:46
eak Area (A-s): 0.028 Peak Height (A): 0.001
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.030
g2 ID: 43231 H81 D Sea. No.: 00037 A/S Pos.: — Date: 09/30/97
eoiicate 1 Time: 10:47
eak Area (A-s): 0.025 Peak Height (.A): 0.001
lank Corrected Pk Height (A): 0.001
oncentration (ug/L ): 0.027
g2 ID: 43231 LCS1 Seq. No.: 00038 A/S Pos.: — Date: 09/30/97
246
-------
0/We igh t File: A £ 812.10 W
airiole volume: 100 mL
Analyst: P. ICHAP33
Nominal WeiQ'ht: 1.0"
yz
3
3T0S=5.Oug/
3106=10.0ug/L
^7
ICv=4.0ug/L
¦5
ECS
o
CHECK LO
10
43159A M84
11
43159A MB4 D
12
43159ft LC34
13
43159A LCS4 D
14
132-30-7E
15
182-30-7E D
16
132-30-7E MS
1?
182-30-7E MSD
18
132-30-9E
1?
182-30-9E 0
20
CCV1-6.Oug/L
21
CCB1
432338 M3
? 7.
43233E ME 0
24
43233 LCS
25
43233 LCS D
26
133-5-1
27
183-5-1 0
28
183-5-1 MS
2?
183-5-1 MSD
30
7CLP 8LK
31
TCLP ELK D
32
CCV1=6.0ug/L ¦
33
CCB1
34
43231 M83
35
43231 hB3 D
36
43231 LCS3
37
43231 LCS3 D
38
1S3-3-1D
39
183-3-1D D
40
183-3-2E
41
183-3-2E D
42
183-3-2E MS
43
183-3-2E MSD
44
CCV1=6. Oug/'L
45
CCB1
46
183-3-2F
47
183-3-2F 0
43
183-3-3E ,
49
183-3-3E 0
50
183-3-3F
51
183-3-3F D
52
183-3-1EF
53
183-3-1EF D
•'b- ^(2- j0|t)97
n/2_ l&ji ]H7
2-oft-
7, -o(°t- z- rvw2" /Dff I?y
3"°^'^ rw£- '7
^ ^I'h7
-------
Loc
54
55
56
57
58
59
60
61
62
63
64
65
66
67
63
69
70
71
72
73
74
Sample ID ~ ' Weight 0ilution "
183-3-5EF
183-3-5EF D
CCV2=6.0ug/L
.J&B2
183-3-6F
1S3-3-6F D
183-3-SC
133-3-3C DX2
I33-3-SC 00X2
183-3-8D
183-3-30 D
183-3-8E
183-3-8E 0
183-3-8E MS
2^ 0|C/- Z- ^ «»/i/v
183-3-8E MSG
CCV3=6.0ug/L — ^ -CfV Z- '/
CCS 3
133-3-8F
133-3-SF 0 ^
CCV4=6.0ug/L —— Z-Ciy-l ^ w/ / 7
CCE4
*
248
-------
JL* _ „_.*L
Element: Hq2
P®nt Data; Main+Suppl.
P^nt: Calib. Curve
Remarks:
r
I^TRUMENT: 5100
wB-elength: 253.7 Peak
S™nal Type: AA
Read Time: 30.0
sflple Replicates: 1
sBndard Replicates: 1
Analyst: RICHARDS
Peak Storage: None
iafi/9 7
Technique: MHS Version: 7.01
Slit: 0.7 Low
Signal Heasurement: Peak Height (5)
Read Delay: 1.0 80C Time: 2
F^HE:
FMme Type: Air
Oxidant Flow; 10.
L/niin
flame Sensor: On .
Fuel Flow: 2.0 L/ min
C«I BRAT ION:
™lutions
r
ib. Blank
SBndard 1
Standard 2
SBndard 3
s®ndard 4
ntterd, 5.
iriaard &
ID
3TO 8IK
3 TO i
ST0 2
STO 3
3TD A
I
Calibration Units: ug/l
tlibration Type: Linear
Cone
0.200
0.500
1.000
2.000
A-QPA
ID.00Q
Sample Units: ug/
:rix Check Calculations:
Hfference for Dupls; No
Recovery for Spike: Ho
Locations:
Locations:
Cone
*
249
-------
Element File; HG .rtEL
Date: 10/(51/97 ~
Data File: AB812.0AT
Technique: MHS
Remark 1: STANDARDS: 3-019-
Remark 3-019-2
Element: Ha2
Time: 09:25
IO/Wt File: AB812.I0W
Calib. Type: Linear
Wavelenath: 253.?
Slit: 0.7 L
Lamp Current: 0
Energy: 72
Hq2 10: 3T0 3IK Seq, No.: 00003 A/S Pos.: — Oate: 10/01/97
Replicate 1 Time: 09:27
Peak Area (A-s): -0.004 ~ Peak Height (A): -0.001
Blank Corrected Pk Height (A): -0.001
Auto-zero performed.
Hg2 ID: STDl=0.2ug/L Seq. Ho'.: 00004 A/S Pos.: — Date: 10/01/9"
Replicate ¦ i Time: 09:2S
Peak Area (A-s): 0.162 Peak Height (A): 01007
Blank Corrected Pk Height (A): 0.00 7
Standard number 1 applied. [0.200J
Correlation coefficient: 1,00000 Slope: 0.0331
Hg2 10: ST02-0.5uq/L Seq. No.: 00005 A/S Pos.: — Date: 10/01/97
Sample abs. is greater than that of the largest standarc.
Replicate 1 Time: 09:29
Peak Area (A-s): 0.407 Peak Height (A): 0.017
Blank Corrected Pk Height (A): 0.017
Concentration (ug/L ,): 0.503
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99999 Slope: 0.0333
Hg2 ID: STD3=1.0ug/L Seq. No.: 00006 A/S Pos.: — Date: 10/01/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 09:30
3eak Area (A-s): 0.854 Peak Height (A): 0.036
31ank Corrected Pk Height (A): 0.036
Concentration (ug/L ): 1.085
standard number 3 applied. [1.000J
Correlation coefficient: 0.99780 Slope: 0.0355
-ig2 ID: STD4=2.0ug/L Seq. No.: 00007 A/S Pos.: — Date: 10/01/97
Sample abs. is greater than that of the largest standard.
teplicate 1 Time: 09:32
>eak Area (A-s): 1.759 Peak Height (A): 0.075
Jlank Corrected Pk Height (A): 0.075
:oncentration (ug/L ): 2.101
-------
I '•
ic^elation coefficient: 0.99899 Slope: 0.0369
IQ2
ID: STD5=5.0ug/
Seq. Ho.: 00008 A/S Pos.
ab.s^-is greater than that of the largest standard,
leplicate 1 Time: 09:33
Area (A-s ): 4.364 Peak Height (A): 0.188
ik Corrected Pk Height (A): 0.188
Concentration (ug/L J: 5.095
iBii-
fdard number 5 applied. [5.000]
elation coefficient: 0.99983 Slope: 0.0375
Date: 10/01/97
1c
ID: Sr06-10.0ug/L
Seq. No.: 00009
A/S Pos.:
Date: 10/01/97
>a|®le abs. is greater than that of the largest standard.
l«.icate 1 Time: 09:34
>eWi Area (A-s): 8.781 Peak Height (A): 0.37 5
Jl^nk Corrected Pk Height (A): 0.375
pent ration (ug/L ): 10.011
Standard number 6 applied, [10.000]
:f eL"lon coefficient: ™
Slope: 0.037 5
251
-------
lenient File: HG .MEL
Element: Hg2
Wavelength: 253.7
ite: 10/01/97
Time: 09:35
Slit: 0.7 L
ita File: ASS12.DAT
ID/Wt File: AB812.IDW
Lamp Current: 0
jchniaue: MHS
Calib. Type: Linear
Energy: 72
¦mark 1: STANDARDS: .3-019-1
mark 2:.^ae= 3-019-2
H Display Calibration - C:\fS_USER\Hfl_FILES\ELEHEHT\HG_.MEL
~
0.3751 ^S6
.X
X
X'
0 . pK
£ ^ S5
1 /
! _
i Mn - Linear
| 54 Corr. Coef.: 0.99996
Slope; BJ375
0.8 Concentration 10.000
252
-------
E^ment File: HG ..MEL Element: Ha2 Wavelength: 253.7
3A?: 10/01/97 Time: 09:37 Slit: 0.7 L
File: A8812.0AT TD/Wt File: ABS12.IDW Lamp Current: 0
technique: HHS Calib. Type: Linear Energy: 72
^•ark 1: srAN0ARQS= 3-019-1 " -
:Jferk 2:.^fi&= 3-019-2
I
ID: ICV = 4.Oug/L Seq. No.: OQOIO A/S Pes.: —. Oate: 10/01/97
*«=»lic3te 1 Time: 09:37
3«Bk Area (A-s): 3.529 Peak Height (A): 0.152
3irank Corrected Pk Height (A): 0.152
Concentration (ug/L ): 4,052
-Icj2 ID: ICS Seq. Mo.: 00011 A/3 Pos. : — Oate; 10/01/9'
5^|licate 1 Time: 09:41
3eak Area (ft-s): -0.001 Peak Height (A): 0.000
3tank Corrected Pk Height (A): 0.000
;entration (ug/L ): 0.005
I
10: CHECK LO Seq. No.: 00012 A/3 Pes.: — Oate: 10/01/9*
5eolioate 1 Time: 09:42
3>^k Area (A-s): 0.155 Peak Height (A): 0.006
3|(nk Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.163
t
-IdY ID: 4-3159A MB4 Ssq. Ho.: 00013 A/S Pos.: — Date: 10/01/97
R*licate 1 Time: 09:43
Area (A-s): -0.001 Peak Height (A): 0.000
31ank Corrected Pk Height (A): 0.000
Ccjpentration (ug/L ): 0.003 *
icA 10: 43159A MB4 0 Seq. No.: 00014 A/S Pos.: — Oate: 10/01/9"
R^Tlicate 1 Time: 09:44
Deak Area (A-s): -0.004 Peak Height (A): -0.000
3®ik Corrected Pk Height (A): -0.000
:entration (ug/L ): -0.00
1
ID: 43159A LCS4 Seq. No.: 00015 A/S Pos.: — Date: 10/01/97
Ra|licate 1 Time: 09:45
Area (A-s): 3.808 Peak Height (A): 0.164
B*nk Corrected Pk Height (A): 0.164
Concentration-(ug/L ): 4.365
f
ig2 ID: 43159A LCS4 D Seq. No.: 00016 A/S Pos.: — Date: 10/01/97
I 253
-------
eclicate 1
eak Area (A-s): 3.752
lank Corrected Pk Height (A):
oricentration (ug/L ): 4.319
Time: 09:47
Peak Height (A): 0.162
0.162
g2 ID:JLS?-30-7E Seq. No.:
eplicate 1
eak Area (A-s ): 0.170
lank Corrected Pk Height (A): 0.007
oncentration (ug/L ); 0.193
00017 . A/S Pos.: -- Date: 10/01/97
Time: 09:48
Peak Height (A): 0.007
g2 ID: 182-30-7E D Seq. No.: 00018 A/S Pos.: -- Date: 10/01/97
eplicate 1 Time: 09:49
eak Area (A-s): 0.15-4 Peak Height (A): 0.006
lank Corrected Pk Height (A): 0.006
oncentration (ug/L ): 0.166
g2 ID: 182-30-7E MS Sea. No.: 00019 A/S Pos.: — Oate: 10/01/9:
eoiicate ,L Time: 09:50
eak Area (A-s): 4.154 Peak Height (A): 0.177
lank Corrected Pk Height (A): 0.177
oncentration ( ug/ L ): 4.726
32 ID: 182-30-7E MSD Seq. No.: 00020 A/S Pos.: — Oate: 10/01/?:
eplicate 1 Time: 09:51
eak Area (A-s): 4.088 Peak Height (A): 0.179
lank Corrected Pk Height (A): 0.179
oncentration (ug/L ): 4.779
32 ID: 182-30-9E Seq.*No.: 00021 A/S Pos.: — Date: 10/01/97
epiicate 1 Time: 09:52
eak Area (A-s): 0.081 Peak Height (A3: 0.003
lank Corrected Pk Height (A): 0.003
oncentration (ug/L ): 0.091
32 ID: 182-30-9E 0 Seq. No.: 00022 A/S Pos.: — Date: 10/01/97
eplicate 1 Time: 09:53
eak Area (A-s): 0.067 Peak Height (A): 0.003
lank Corrected Pk Height (A): 0.003
oncentration (ug/L ): 0.070
32 ID: CCVl-t.Oug/L Seq. No.:
eplicate 1
sak Area (A-s): 5.276
lank Corrected Pk Height (A): 0.228
00023 A/S Pos.: — Date: 10/01/97
Time: 09:54 -
Peak Height (A): 0.228
254
-------
concentration (ug/L ): 6.082
I;
ID: CC81
Seq. No.: 00024 fi/S Pos.
Date: 10/01/97
t plicate 1
ak brea.Ja&-s ): 0.025
Blank Corrected Pk Height
3ncentration (ug/L ): 0.
Time: 09:55 ~ -
Peak Height (A): 0.001
E
Ipj
ec
(A): 0.001
027
ID: 43233B ME
Seq. No.: 00025 A/8 Pos.
Date: 10/01/97
"eplicate I
Peak Area (A-s J: -0.001
¦lank Corrected Pk Height
Concentration (ug/L ): 0
Time: 10:02
Peak Height (A): 0.000
(A): 0.000
.003
I
ID: 43233E MB 0
Seq. No.: 00026
A/S Pos.: —
Date: 10/01/9"
l
eolicata' 1
eak Area (A-s): -0.002
lank Corrected Pk Height
orcertration (ug/L ): 0.
Time: 10:03
Peak Height (A): 0.000
Hg2 10: 43233 LCS
Jsplicate 1
Peak Area (A-s): 3.S43
fank Corrected Pk Height
ncentration (ug/L ): 4.
(A): 0.000
000
Sea. No
(A): 0.167
458
0002?
A/3 Pos.
03te; 10/01'9"
Time: 10:04
Peak Height (A): 0.167
I
ID: 43233 LCS 0
Replicate 1
«=ak Area (A-s): 3.710
lank Corrected Pk Height
Concentration (ug/L ): 4.
Seq. N-:
(A): 0.157
196
00028 A/S Pos..: —
Time: 10:06
Peak Height (A): 0.157
Date: 10/01/9:
t
ID: 183-5-1
Seq. No.: 00029
A/S Pos.: —
Date: 10./01/9:
¦aplicate 1
Ifeak Area (A-s): 0.016
Blank Corrected Pk Height
•oncentration (ug/L ): 0.
Time: 10:07
Peak Height (A): 0.001
(A): 0.001
024
«
,g2 ID: 183-5-1 D
Seq. No.: 00030 A/S Pos.
.eplicate 1
Peak Area (A-s): 0.008
I lank Corrected Pk Height
^ncentration (ug/L ): 0,
(A): 0.000
011
I
Time: 10:08
Peak Height (A): 0.000
Date: 10/01/9:
255
-------
ID/Weight File: AB817.IDW
Sample Volume: 100 mL"
Analyst: RICHARDS
Nominal Weight: 1.0
g
Loc.
0
1
2
3
4
5
6
. 7
8
9
10
11
12
13
14
15
16
17
IS
19
20
21
22
23
24
25
26
27
2S
29
30
31
32
33
34
35
36
37
3S
39
40
41
42
43
44
45
46
47
48
49
50
51
52
53
Sample ID
STD BLK
^_STD 1 = 0. 2ug/ L
"STD2=0.5ug/L
STD3=1.Oug/L
STD4=2.Oug/L
STD5=5.Oug/L
STD6=10.Oug/L
ICV=4.Oug/L
ICB
CHECK LO 5
43159A MB4
43159A MBi D
43159A LCS4*
43159A LCS4 D
132-30-780^
182-30-
182-30-7B
182-30-7B,
132-30-SflC^
132-30-sic.VD
CCV1-6.Oug/L
CCB1 ^
152-30-9&p> ¦>»>«> wia:
182-30-98*© D 1
182-30-14SC
182-30-14BC D
CCV2=6.0ug/L
CCB2
43271 MB2
43271 MB2 D
432 71 LCS2
43271 LCS2 D
153-43-3D
182-43-3D D
183-43-5C
183-43-5C D
183-43-5C MS
183-43-5C MSD
CCV1=6.Oug/L
CCB1
183-43-5AB
183-43-5AB D
133-43-5D
1S3-43-5D D
183-43-5E
183-43-5E DX5
183-43-5E DDX5
183-43-5F
183-43-5F D
. 183-43-6AB
183-43-6AB D
CCV2 = 6.Oug/L
CC82
183-43-oC
We igh t
Dilution
I*
h/v
1
_O2.0
tofrhi
I 0;
/?/??
3-02,^' ^
rw£-
lafrfa
-------
I
Sample ID
Weight
Dilution
55
i6
58
|o
61
>2
3
4
I
O D
1
6
7
63
1
I
I;
75
I'
78
183-43-6C D
183-43-6D
183-43-6D 0
_,183-43-6E
" 183-43-6E DX2
183-43-6E DDX2
183-43-6F
153-43-6F D
183-43-7A8
.183--43-7A6" D
CCV3=6.Oug/L
CCB 3
184-43-7C
134-43-7C
154-43-7C
184-43-7C MSO
1S3-43-7D
133-43-7D D
133-43-7E
183-43-7E DX5
LS3-43-7E 00X5
183-43-7F
183-43-7F 0
D
MS
CCV4 = 6
CCS 4
. Oug/i
1-
7
s
Oi°
0/9f?7
257
-------
Element File: HGMEL
: 1emen t: Hg2
'rint Data: Main+Suppl.
3rint: Calib. Curve
iemarks :
STANDARDS = 3-020-5
QC~ 3-020-6
Analy s t: R1CH ARDS
Peak Storage: None
-K
to
9
*(??
INSTRUMENT: 5100
Wavelength: 253.7 Peak
signal Type: AA
-------
a2
ID: STD BLK
Sea . No . : -OOOCX
A/S Pos.-: —
Jflicate 1
eak Area (A-s'): 0.004
l^nk Corrected Pk Height (A): 0.000
ofcentration (ug/L ): 0.00S
H *
Date: 10/09/9"7
T ime: 08:20
Peak Height (A): 0.000
f:
:ero performed.
ID: STDi-0.2ug/L
Sec. No.
00004
A/S Pos.: --
Date: 10/09/9"
ejlicate 1
= ak Area (A-s ) : 0.167
Corrected Pk Height (A): 0.008
oftentration (ug/L ): 0.197
T ime: 08:21
Peak Height (A): 0.008
f;
;ari(
I
tandard number 1 applied. [0.200]
oB~elation coefficient: 1.00000
Slope: 0.0^76
1
ID: STD2=0.5ug/L
Sea. No.: 00005
A/S Pos.:
Date: 10/09/9"
ample abs. is greater than that of the largest standard,
icate 1 Time: 03:22
Area (A-s): 0.430 Peak Height (A): 0.018
lcTnk Corrected Pk Height (A): 0.01c
iQCentration (ug/L ): 0.4SS
»
I
tJfidard number 2 applied. [0.500!
orrelation coefficient: 0.99977
Slope: 0.0368
3o
ID
STD3=1.Oug/L
Seq. No.: 00006
A/'S Pos.: --
Date: 10/09/9 7
ill:
:
ar»le abs. is greater than that of the largest standard.
icate 1 Time: 08:23
=ak Area (A-s): 0.851 , Peak Height (A): 0.036
L^k Corrected Pk Height (A): 0.036
:™entration (ug/L ): 0.988
t^dard number 3 applied. [1.000]
DiBelation coefficient: 0.99992
Slope: 0.0365
ID: STD4-2.Oug/L
Seq. No.: 00007
A/S Pos.:
Date: 10/09/9"
ample abs. is greater than that of the largest standard.
[icate 1
A rea (' A-s ) : 1 . 722
Lank Corrected Pk Height (A): 0.074
Dt*entration (ug/L ): 2.036
;fl
an
1
an
1
Time: 08:24
Peak Height (A): 0.074
landard number 4 applied. [2.000]
Dcrelation coefficient: 0.99990
Slope: 0.0370
259
-------
Hg2
ID: STD5 = 5.Oug/'L
Seq
Mo.
00008
A/S Pas,
Date: 10/09/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 08:25
Peak Area (A-s): 4.365 Peak Height (A): 0.192
Blank Corrected PK Height (A): 0.192
Concentration (ug/L ): 5.177
Standard number 5 applied. [5.000]
Correlation coefficient: 0.99982
Slope: 0.0381
Hg2-
ID: STDo=10.Oug/L
Seq. No.: 00009
A/S Pos.:
Date: 10/09/9:
Sample abs. is greater than that of the largest standard.
Replicate 1
Peak Area (A-s): 8,911
Blank Corrected Pk Height (A): 0.385
Concentration (ug/L ): 10.108
Time: 08:27
Peak height (A): 0.385
Standard number 6 applied. [10.000]
Correlation 'coefficient: 0.99994
Slope: 0.0384
»
260
-------
Element File: HG_.MEL Element: Hg2 _ Wavelength: 253.7
C^te: 10/09/97 " Time: 03:27 * Slit: 0.7 L
CMta File: A6817.DAT IO/Wt File: AB817.IDW Lamp Current: 0
rechnique: MHS Calib. Type: Linear Energy: 72
Re
1
mark 1: STANDARDS^ 3-020-5
mark 2: QC= 3-020-6
H Display Calibration - C:\fift_USER\fiH_FILES\ELEMENT\HG_.MEL
0,3851
W j rtf*
| ,.-^S5
./"*
gi". Linear
S4 Corf. Coef.: 0.99994
S3 Slope; 0.0384
0.0 Concentration 10.000
I
I
t'
ID: ICV=4.Oug/L
Seq. No.: 00010
A/S Pos.: --
f plicate 1
ak Area (A-s): 3.572
Blank Corrected Pk Height (A): 0.153
Incsntration ( ug/L ) : 3.974
Time: 03:2°
Peak Height (A): 0.153
I
f-^2
fSp.
ID: ICB
Seq. No. : 00011
"plicate 1
Peak Area (A-s): 0.019
Sank Corrected Pk Height (A): 0.000
ncentration (ug/L ): 0.010
A/S Pos.: --
Time: 08:30
Peak Height (A): 0.000
Date: 10/09/97
Date: 10/09/9"
ID: CHECK LO
Seq. No.: 00012 A/S Pos.:
Date: 10/09/9"
Replicate 1
ik Area (A-s): 0.180
lank Corrected Pk Height (A): 0.008
Concentration (ug/L ): 0.196
Time: 08:32
Peak Hei'gRt (A): 0.00S
261
-------
Hg2 ID: 43159A Seq. No.: 00013 A/S Pos
Replicate 1
Peak Area (ft-s ) : 0.009
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.010
Time: 08:33
Peak Height (A): 0.000
Date: 10/09/97
Hg2 ID: 43159A MB/i"D Seq. No.: 00014 A/S Pos.
Date: 10/09/9:
Replicate 1
Peak Area (A-s i: 0.003
Blank Corrected Pk Height (A): 0.000
Concentration (ug/L ): 0.005
Time: 08:34
Peak Height (A): 0.000
Hgl
ID: 43159A LCS^* a-v** Seq. No.: 00015* A/S Pos. : -•
Date: 10/09/9"
Replicate i
Peak Area (A-s): 4.548
Blank Corrected Pk Height (A): 0.201
Concentration (ug/L ): 5.233
Time: OS:35
Peak Height (A): 0.201
ID: 43159A LCS^O
Af, ,v
£€
No.: 00016
Replicate 1
Peak Area (A-s): 4 . 3S2
Blank Corrected Pk Height (A)
Concentration (ug/L ): 4.941
0. 190
Pos
T ime: 08:36
Peak Height (A): 0.190
Da K
10/09/9-'
Ha2
ID: 182-30-7fr&c**lv,s"q"!tfc
be<
No
00017 A/S Pos
Date: 10/09/9"
RepLicate 1
Peak Area (A-s); 0.023
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L' ): 0.01B
Time: 08:37
Peak Height (A): 0.001
¦ae
Hg2 ID: 182-30-7-6-9 D
Replicate 1
Peak Area (A-s): 0.024
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.021
Seq. No.: 00018 A/S Pos.: --
Time: 08:38
Peak Height (A): 0.001
Date: 10/09/97
Hg2 ID: 182-30-7-&& MS
Seq. No.: 00019 A/S Pos.: -¦
Date; 10/09/97
Replicate 1
Peak Area (A-s): 4.425
Blank Corrected Pk Height (A): 0.190
Concentration (ug/'L ) : 4.946
Time: 08:39
Peak Height (A): 0.190
Tift
Hg2 ID: l82~30-7*B€r MSD Seq. No.
00020 A/S Pos.: -•
Date: 10/09/97
262
-------
I
Plicate 1
eak Area (A-s_): 4.384
lank Corrected Pk Height (A): 0.189
eventration (ug/t ) : 4.930
Time: 08:40
Peak Height (A); 0.189
.ID: 182-30~8Ae- Seqr No.: 00021 A/S Po?
Date: 10/09/9"
teolicate 1
§k Area (A-s): 0.029
nk Corrected Pk Height (A): 0,
:oncentration (ug/L ): 0.021
Time: 08:41
Peak Height (A): 0.001
0.01
P -H
fa2 ID: 182-30-8A6- D
Seq. No.: 00022
A/S Pos.:
Date: 10/09/9"
^•licate 1
3Sk Area (A-s): 0.005
Blank Corrected Pk Height (A): 0.000
^cjjcentration (ug/L ): 0.000
Time 03:42
Peak Height (A): 0.000
•l<
ID: CCV1=6.Oua/L
Seq. No.: 00023 A/S Pa:
Date: 10/09/9"
Replicate 1
:,«k Area (A-s): 5.525
ilnk Corrected Pk Height (A): 0
Concentration (ug/L ): 6.395
246
I
1
ID: CCB1
'.•licate 1
Area (A-s): 0.025
Blank Corrected Pk Height (A): 0,
acentratian (ug/L ): 0.016
001
X
Ha2
i
Time: 08:43
Peak Height (A): 0.246
Seq. No.: 00024 A/S Po;
Time: 08:44
Peak Height (A); 0.001
Date: 10/09/9"
68
ID: 182-30- .«ra •<1 icate 1
pRtk Area (A-s): 0.004
Blank Corrected Pk Height (A): 0.
000
00027
A/S Pes.
Time: 08:47
Peak Height (A): 0.000
Date: 10/09/9"
263
-------
Concentration (ug/L ):'0.000
Hg2 ID: -132-30-14SC D Seq. No . : 00028 A/S Pas.: — Date: 10/09/9"
Rsplicate 1 . Time: 08:48 —
Peak Area (A-s): 0.004 ~ Peak Height (A): 0.000
Blank Co=rr-ec ted Pk Height (A): 0.000
Concentration (ug/L ): 0.003
Hg2 ID: CCV2-6.Oug/L Seq. Ho.: 00029 A/S Pos.: -- Date: 10/09/9"
Replicate i Time; 08:49
Peak Area (A-s): 5.201 Peak Height (A): 0.224
Blank Corrected Pk Height (A): 0.224
Concentration (ug/L ): 5.831
Hg2 ID: CCB2 Seq.- No.: 00030 A/S Pos.: -- Date; 10/09/9"
Replicate 1 Time: 08:50'
Peak Area (A-s): 0.023 Peak Height (A): O.OOi
Blank Corrected Pk Height (A): O.OOi
Concentration (ug/L ): 0.021
Hg2 ID: 43271 MB2 Sec. No.: 00031 A/S Pos.: — Date: 10/09/9"
Replicate i Time: 08:51
Peak Area (A-s): 0.003 Peak Height (A): -0.000
Blank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.005
Hg2 ID: 43271 MB2 0 Seq. No.: 00032 A/S Pos.: ~ Date: 10/09/9"
Replicate 1 Time: OS:52
Peak Area (A-s): 0.002 t Peak Height (A); -0.000
8 lank Corrected Pk Height (A): -0.000
Concentration (ug/L ): -0.003
Hg2 ID: 43271 LCS2 Seq. No.:
Replicate 1
Peak Area (A-s): 4.406
Slank Corrected Pk Height (A): 0.194
Concentration (ug/L ); 5.053
Hg2 ID: 43271 LCS2 D Seq. No.:
Replicate 1
Peak Area (A-s): 4.053
Blank Corrected Pk Height (A): 0.173
Concentration (ug/L ): 4.507
00033 A/S Pos.: — Date: 10/09/97
Time: OS:53
Peak Height (A): 0.194
00034 A/S Pos.: -- Date: 10/09/97
Time; 08:56
Peak Height (A): 0.173
oq 4
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CASE NARRATIVE
Analysis of Samples for the Presence of Trace Metals
Method 29 April 1996 Rev.
Client: Eastern Research Group
TLI Project Number: 43159B
Date: October 15,1997
This report should only be reproduced in full.
Any partial reproduction of this report requires permission from
Triangle Laboratories, Inc.
Rev. 07-May-97
Triangle Laboratories, Inc.
801 Capitola Drive P.O. Box 13485
Durham, NC 27713-4411 Research Triangle Park, NC 27709-3485
919-544-5729 Fax #919-544-5491 1
-------
Triangle Laboratories, Inc.
Case Narrative
October 15,1997
TLIProject#: 43159B
Overview
Five filter samples were analyzed for arsenic (As), beryllium (Be), cadmium (Cd), cobalt
(Co), chromium (Cr), manganese (Mn), nickel (Ni), lead (Pb), antimony (Sb), selenium
(Se), and mercury (Hg). For all analyses, the samples and associated QC samples were
prepared and analyzed following the guidelines of Method 29 April 1996 Rev. Results
reported relate only to the items tested.
OC Remarks
The release of this set of data by Triangle Laboratories, Inc. was authorized by the Quality
Control Chemist who has reviewed each sample data package individually following a
series of inspections/reviews. When applicable, general deviations from acceptable QC
requirements are identified below and comments are made on the effects of these
deviations upon the validity and reliability of the results. Specific QC issues associated
with this particular project are:
Sample Receipt:
Twelve train samples, two blank train samples two DI water samples, and five filter were
received at ambient temperature on September 9,1997 under project 43159 in good condition.
Sample YCP-169 arrived with this batch of samples, but was not listed on the client's
chain of custody. YCP-169 was not analyzed per the client's request. Samples YCP-21,
YCP-27, YCP-33, YCP-44, and YCP-59 were missing from the sample shipment.
Samples YCP-21, YCP-27, and YCP-33 were later received at 22 °C on September 10,
1996 under project # 43187 in good condition. The six filters were reported under project #
43159B. Only the six filter samples were reported in this data package.
Sample Preparation:
Laboratory documentation of the sample preparation is included in the data package.
Instrumentation:
Arsenic (As), beryllium (Be), cadmium (Cd), cobalt (Co), chromium (Cr), manganese
(Mn), nickel (Ni), lead (Pb), antimony (Sb), and selenium (Se) concentrations were
determined by Inductively Coupled Plasma Emission Spectroscopy (ICP).
Mercury (Hg) concentrations were determined by Cold Vapor Atomic Absorption
(CVAA).
The linear range for the instrument TJA 6IE Trace Analyzer was based on four standards
and a blank, which established a correlation coefficient value greater than or equal to
0.995. A calibration curve, based on a blank and one standard, is established for each
analytical run, followed by a check high standard and an initial calibration verification
-------
Triangle Laboratories, Inc.
Case Narrative
October 15,1997
TLI Project #: 431S9B
(ICV). The check high standard does not deviate from the calibration curve by more than
5%. In addition, continuing calibration verifications (CCVs) are performed throughout
the analytical run.
A Reporting Detection Limit (RDL) is used instead of an Instrument Detection Limit
(EDL). The spectrometer and atomic absorption instruments can achieve low detection
limits between 0.2-8 ppb levels for many analytes. Triangle Labs is using RDL values of
1-10 times the IDL as detection limits for reporting purposes.
Data Review:
All analytes found in the method blank (MB) are detected at a level equal to or less than
the respective Reporting Detection Limits (RDLs).
The recoveries for the post-digestion spike (PDS) are not reported for Cr and Mn for the
sample YCP-178. The spike concentrations added were insignificant in comparison to the
levels of these analytes present in the native sample.
The pre-digestion spike (MS) for Mercury (Hg) for the sample YCP-178 demonstrated a
percent recovery slightly outside the QC criteria, which does not indicate significant
matrix effects specific to this analyte in the native sample matrix. Please note that the pre-
digestion spike duplicate (MSD) met the QC criteria for this analyte.
The sample was analyzed within the 28 day sampling to analysis holding time for Hg and
within the six month sampling to analysis holding time for other analytes.
QC requirements:
The duplicate analyses for analytes analyzed by ICP cannot be considered valid qualifiers if
the concentrations of the analytes in the original and/or duplicate sample are not at least
ten times the respective RDLs. The RPDs for these analyses are indicated by or "
-------
Triangle Laboratories, Inc.
Case Narrative
October 15,1997
TLIProject#: 43159B
For serial dilution analyses which are valid qualifiers, the quality control RPD is ± 10.0
percent. If RPDs are outside this range, interferences are suspected.
The quality control range for percent recoveries of laboratory control spiked samples is
The quality control range for percent recoveries of spiked samples is 75-125. If recoveries
are outside this range, a matrix effect is suspected.
By our interpretation, the analytical data in this project are valid based on the guidelines of
Method 29 April 1996 Rev. Any specific QC concerns or problems have been discussed in
the QC REMARKS section with emphasis on their effect on the data. Should Eastern
Research Group have any questions or comments regarding this data package, please feel
free to contact Project Scientist, Amy J. Boehm, at (919) 544-5729 ext.268.
For Triangle Laboratories, Inc.,
Quality Control
80-120.
Brenda H/Bell
Linda F. Jones
Report Preparation Chemist
Report Preparation Chemist
The total number of pages in this data package is:
-------
TRIANGLE LABORATORIES, INC.
UST OF CERTIFICATIONS AND ACCREDITATIONS
ENVIRONMENTAL
American Association for Laboratory Accreditation. Certification pending. Certificate
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Waste Water, Sol/Haz Waste, Pulp/Paper, and Air Matrices) Parameters are AOX/TOX,
Volatiies, Pesticides, PCB's, BNA's, and Dioxin/Furan. Method 1613 for Drinking Water.
State of Alabama, Department of Environmental Management Expires December 31, 1997.
Laboratory I.D. # 40950. Dioxin in drinking water.
State of Alaska, Department of Environmental Conservation. Expires December 21, 1997.
Certificate number OS-00397. Dioxin in drinking water.
State of Arizona, Department of Health Services. Expires May 26, 1998. Certificate
#AZ0423. Drinking Water for Dioxin, Dioxin in WW and S/H Waste.
State of Arkansas, Department of Pollution Control and Ecology. Expires February 18,
1998. Pulp/paper, soil, water, and Hazardous Waste for Dioxin/Furan; AOX/TOX.
State of California, Department of Health Services. Expires August 31, 1999. Certificate
#1922. Selected Metals in Waste Water: Volatiies, Semi-volatiles. and Dioxin/furan in WW and
Sol/Haz Waste. Dioxin in drinking water.
State of Connecticut, Department of Health Services. Expires September 30, 1997.
Registration # PH-0117. Dioxin in drinking water.
Delaware Health and Social Services. Expires December 31, 1997. Certificate #NC 140.
Dioxin in drinking water.
Florida Department of Health and Rehabilitative Services. Expires June 30, 1998.Dioxin in
DW. Drinking Water ID HRS# 87424. Metals, Extractable Organics (GC/MS), Pesticides/PCB's
(GC) and Volatiies (GC/MS) in Environmental Samples. Environmental water ID HRS#
E87411.
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status for regulatory purposes .
Revised 9/18/97 RM
Printed 9/18/97
-------
Idaho Department of Health and Welfare. Expires November 30, 1997. Dioxin in drinking
water.
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Environmental Analvses/Non potable Water and Solid and Hazardous Waste. Method 1613
for drinking water. ID #'s - Drinking water and/or pollution control - £-215. Solid or Hazardous
Waste-E-1209.
Commonwealth of Kentucky, Department for Environmental Protection. Expires December
31, 1997. ID#90060. Dioxin in drinking water.
Maryland Department of Health and Mental Hygiene. Expires September 30, 1997.
Certification #235. Drinking water by Method 1613A.
State of Michigan, Department of Public Health. Expires March 31, 1998. Drinking water by
Method 1613.
Mississippi State Department of Health. No expiration date.. Dioxin in drinking water.
Montana Department of Health and Environmental Services. Expires December 31, 1997.
Dioxin in drinking water.
State of New Jersey, Department of Environmental Protection and Energy. Extended by
state. Temporary certificate until December 31.1997. ID #67851, BNAs and Volatiles. Dioxin in
drinking water.
State of New Mexico, Environment Department Certification pending. Dioxin in drinking
water.
New York State Department of Health. Expires June 30, 1997. ID #11026. Environmental
Analyses of non-potable Water, Solid and Hazardous Waste. Method 1613 in DW.
State of North Carolina, Department of Environment Health and Natural Resources
Expires August 31, 1999. Certificate # 37751. Dioxin in drinking water.
State of North Carolina, Department of Environment, Health, and Natural Resources,
Division of Environmental Management Expires December 31, 1997. Certificate # 485.
Metals, pesticides & PCBs, semi-volatites and volatiles; TCLP.
North Dakota State Department of Health and Consolidated Laboratories. Expires
December 31,1997. Certificate # R-076. Effective October 4,1993. Dioxin in drinking water.
Revised 9/18/97 RM
Primed 9/18/97
-------
Oklahoma Department of Environmental Quality. Expires October 31, 1997. Laboratory
#9612. Dioxin by 1613A. 8290 and 8280.
State of South Carolina, Department of Health and Environmental Control. Expires June
30, 1997. Certificate number #99040001 (drinking water). Expires August 31,1999. Certificate
number #99040002 (other parameters). Dioxin/Furans, BNA, Volatiles, and PCBs/pesticides
under Clean Water Act, 2,3,7,8-TCDD for Drinking Water, and Organic extractabies for Solid
and Hazardous Waste.
State of Tennessee. Department of Environment and Conservation. Expires February S,
1999. ID #02992. Method 1613 Drinking water only.
U.S. Department of Agriculture Soil Permit Expires September 30, 2001. Permit No. S-
3790. Under the authority of the Federal Plant Pest Act, permission is granted to receive
foreign soil samples for use in laboratory analysis.
U.S. Army Corps of Engineers. Expires November 30, 1997. Validated to perform methods
8280 & 8290 for Lockboume Landfill Site Investigation, Defense Distribution Depot Projects,
and assorted projects for the USAGE North Pacific Division Laboratory.
U.S. EPA Region V. Expires November 14,1999. Dioxin in drinking water.
U.S. EPA Region VIII, for the State of Wyoming. Expires November 13, 1997. Dioxin in
drinking water.
State of Utah, Department of Health. Expires December 31,1997. Certificate Number E-166.
Certification for the following parameters: Semi-Volatiles and Volatiles under RCRA; Volatiles
under Clean Water Act; Dioxin/furans by Method 8280; Drinking water for Dioxin by Method
1613; Metals including Mercury and Microwave Digestion.
Commonwealth of Virginia, Department of General Services, Division of Consolidated
Laboratory Services. Expires June 30,1998. ID # 00341. Dioxin in drinking water.
State of Washington, Department of Ecology. Expires September 1998. Lab Accreditation
Number C067. Scope of Accreditation applies to water analyses for Poly chlorinated Dibenzo-
p-dioxins and Polychlorinated Dibenzofurans, BNA Extr (Semivolatile) Organics and Purgeable
(Volatile) Organics.
State of Washington, Department of Health. Expires April 30, 1998. Dioxin in drinking water.
Lab I.D. 129
State of West Virginia, Department of Health. Expires December 31, 1997. Certificate No.
9923(C). Dioxin in drinking water.
Revised 9/18/97 RM
Printed 9/18/97
-------
State of Wisconsin, Department of Natural Resources. Expires August 31, 1998.
Laboratory ID Number 999869530. Certification for the following categories of Organics:
Purgeable, Base/Neutral. Add, PCBs, and Dioxin. Expires November 14, 1999. Laboratory ID
999869530. Dioxin in drinking water.
PHARMACEUTICAL
Drug Enforcement Agency (DEA). Expires November 30, 1997. Registration number
RT01195835. Controlled substance registration for schedules 1,2,3,3N,4,5.
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PT 0000 0031. North Carolina controlled substances registration. Application submitted for
renewal.
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OTHER
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Administration.
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#NCD982156879. Permit indicates that the laboratory is a large generator of hazardous waste.
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0954-1. License authorizes the licensee to receive, acquire, own, possess, transfer, import and
use such radioactive materials as designated.
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032-875-OG. The general license applies only to radioactive material contained in devices
which have been manufactured and labeled in accordance with specific requirements.
Revised 9/18/97 RM
Printed 9/18/97
-------
ABBREVIATIONS
BH = Back Half
CC3 » Coccsuisg CaSbrarion. Blank
CCV = Concxuiing Caiibrarioa Vniftdfinu.
CHECXHS = Check HIgil Standard
D ss DC? = Analytical PTpifnrr (Regared Dcpfiqg)
DA = Duplicate Analysis
FH = Front Half
FV = Esal Digestaie Volume
IC3 = Tr""ai Citibrarion Blank
ICV* = Initial Calibration Veriacaaoii
ICS AB = Interference Cbeck Sotaaon (Solution AB)
f = Tntrtai
F= Final
Soiucoo AB contains common wsersxem in addition to the anaiyte of interest.
EDL = Instrument Detecaon Limn
L ss Senai Dilution
LCS =s Laboratory Control Sofia Sample
MB = Method Blank
MPV ss Mercury Preparation. Volume
MS = Pre-digestion Spike
MSD = Pre-digestion Spike Diro&snB#
N/A = Not Aroiicable
N/Av = Not Available
N/VssNbt Valid
FDS =s Post-digestion Spike
%REC = Percent Recovery
RDL =s Reporting Detection Lin*
RPD = Relative Percent Difference
T = Analytical Triplicate (Piqjaied Tripficatr, tarHganatysisby Medsod7471 oniy)
TV=Total Sample Votame
-------
STANDARD CONCENTRATIONS
for the TJA 61E TRACE ANALYZER
Analyte
Units
HlghStd
ICV/CCV
ICSAB
RDL | Wavelength
Ag
ppb
1000
500
500
1
3280
As
ppb
1000
500
500
5
1890
Ai
ppb
100©
500
500000
50
3082
B
ppb
1000
500
500
7
2496
Ba
ppb ^
1000
500
500
. 2
4934
Be
ppb
1000
500
500
1
3130
€a
ppb
1000
500
500000
60
¦ .1.3179
Cd
ppb
1000
500
500
1
2265
€e
ppb
1000
500
;500
;¦ 3
4186
Co
ppb
1000
500
500
1
2286
Cr
; ppb
1000
500
* f 500:
m
. --mi m
Cu
ppb
1000
500
500
2
3247
Fe
ppb
1000
500
200000
40
2714
K
ppb
10000
5000
19000
220
7664
¦ Li : -
ppb
1000 =
500
500
1
6706
Mg
PPb
1000
500
500000
30
2790
ppb
1000
500
500
2
2576
Mo
ppb
1000
500
500
2
2020
Na /'
:ppb -K
10000
5000
5000
300
3302
Ni
ppb
1000
500
500
3
2316
. ; v;.p.. ....
ppb
1000
500
500
30
Pb
ppb
1000
500
500
2
2203
Sb
ppb
1000
500
500
..?4: :
2068
Se
ppb
1000
500
500
3
1960
• p
ppb ?
! iooo
500
; 500
:•
1899
Sr
ppb
1000
500
650
1
4215
ppb
1000
500
500
9
T1
ppb
1000
500
500
5
1908
^ v ¦
ppb
1000
500
500
2
2924
Zn
ppb
1000
500
500
12
2062
Note: Use this reference page to review the raw data from the TJA 61E Trace Analyzer.
This page includes the standard concentrations for the check high standard, initial calibration
verification (ICV), continuing calibration verification (CCV), and the interference check solution
(ICSAB). In addition the reporting detection limit (RDL) and wavelength are reported for each
analyte.
Revision Date: 15-M-96
10
-------
CALCULATIONS FOR AIR SAMPLES
RRSTTT TS FOR TRACE METALS fexcent mercury):
RESULT in Llg (Front Half) = Ug/L * FV fmL) * DF
1000 mUL
^ RESULT in Jig (Back Half & Impingens) = fis/L * TV (mL) * FV (mL) * DF
mL used * 1000 mLL
FV = final volume in mL
TV = total volume in mL
DF = Dilution Factor
The RESULTS for combined Front Half & Back Half samples use the same calculation as the
Back Half & impinger samples.
RESULTS FOR MERCURY (En):
RESULT in fig (Front Half) = \x.z!L * (mL FV/mL aliquot) * MPV * DF
RESULT in [ig (Back Half & Impingers) = p.g/L * (mL TV/mL aliquot) * MPV * DF
MPV = mercury preparation volume = 0,1 L
%REC (Percent Recovery) for MS/MSD Hg spikes:
%REC = spike sample results - original sample results * 100
true spike sample results
NOTE: Original sample results less than the RDL are not used in calulations.
%REC (Percent Recovery) for PDS:
%REC = Spike sample itg/L cone, - original sample tig/L conc. * 100
spike conc. Oig/L)
%REC (Percent Recovery) forLCS/LCSD:
%REC = Spike sample ^.g/L conc. * 100
spike conc. (Jlg/L)
RPDs: RPD = 1 Result 2 - Result 1 1 * 100
(Result 2 + Result l)/2 Rev. 2-Oct-96
11
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Sample ED:
YCP-178
TLI SamDle ED:
182-30-16A
Date Received:
Sentember 09.1997
Date Preoared:
September 18.1997
Date Analvzed:
October 03-04.1997
Matrix:
MM TRAIN
Analvte
•\-:'-x!C0nc.'''
tutyU
mL
TotaJ Vol.
IliliL.:; &
Final Vol.
D8utjon
Factor
Totalug
: Resuft : v
As
42.134
N/A
N/A
100
1
4.21
Be
CM
CO
1
m
N/A
100
1
< 0.100
Cd
7.688
N/A
WA
100
1
0.769
Co
0.903
N/A
N/A
100
1
< 0.100
Cr
250.8®
N/A
N/A
100
1
25.1
Mn
1891.264
N/A
N/A
100
1
189
Ni
42.480
N/A
N/A
100
1
4.25
Pb
131.643
N/A
N/A
100
1
132
Sb
-1.004
N/A
N/A
100
1
< 0.400
Se
83.177
N/A
N/A
100
1
8,32
»
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 14-Oct-97 at 01:08 PM
12
-------
Client: Eastern Research Group
Protect Number: 43159B
Sample Report
Client Sample ID:
YCP-178 L
TLI Sample ID:
182-30-16A L
Date Received:
September 09.1997
Date Prepared:
September 18.1997
Date Analvzed:
October 03-04.1997
Matrix:
MM TRAIN
Analvte
IllPriii
Total Vol.
I; : ml. : :jj
¦
i - Rnal\feL
factor : '
. Total ug.
Result
As
11.009
m
N/A
100
5
5.50
Be
-0.076
N/A
N/A
100
5
< 0.500
Cd
0.550
n/a
N/A
100
5
< 0.500
Co
-0.544
m
N/A
100
5
< 0.500
Cr
51.146
N/A
N/A
100
5
25.6
Mn
368.407
N/A
N/A
100
5
184
Ni
11.035
N/A
N/A
100
5
5.52
Pb
26.708
N/A
N/A
100
5
13.4
Sb
0.415
n/a
N/A
100
5
< 2.00
Se
19.697
N/A
N/A
100
5
9.85
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713 Printed: 13-Oct-97 at 12:49 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
13
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Sample ID:
YCP-179
TLI Samole ED:
182-30-16B
Date Received:
September 09.1997
Date Preoared:
September 18,1997
Date Analyzed:
October 03-04.1997
Matrix:
MM TRAIN
Analvte :
Cone. :
fool)
Total Vol-
mL
# Used : :
. : ml * •
Final Vol.
Diutior* ¦
Factor
TdafuQ;
As
29.054
N/A
N/A
100
1
2.91
Be
-1.026
N/A
N/A
100
1
< 0.100
Cd
9.177
N/A
N/A
100
1
0.918
Co
-0.166
N/A
N/A
100
1
< 0.100
Cr
260.619
N/A
N/A
100
1
26.1
Mn
1722.979
N/A
N/A
100
1
172
Ni
49.097
N/A
N/A
100
1
4.91
Pb
261.609
N/A
N/A
100
1
26.2
Sb
-4.378
N/A
N/A
100
1
< 0.400
Se
98.890
N/A
N/A
100
1
9.89
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 » Fax: (919) 544-5491
Printe± 13-Oct-97 at 12:49 PM
14
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Samole ED:
YCP-179 DA
TLI Samole ID:
182-30-16B DA
Date Received:
Seotember 09.1997
Date Preoared:
September 18.1997
Date Analyzed:
October 03-04.1997
Matrix:
MM TRAIN
fifiaa
Rnaf Vol.
sr.
¦¦¦¦¦¦
Result
As
26.904
n/a
N/A
100
1
2.69
Be
-1.031
N/A
N/A
100
1
< 0.100
Cd
9.681
N/A
N/A
100
1
0.968
Co
-0.356
N/A
N/A
100
1
< 0.100
Cr
260.801
N/A
N/A
100
1
26.1
Mn
1724.823
N/A
N/A
100
1
172
Ni
48.572
N/A
N/A
100
1
4.86
Pb
263.129
N/A
N/A
100
1
26.3
Sb
-6.928
N/A
N/A
100
1
< 0.400
Se
97.690
N/A
N/A
100
1
9.77
••
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed:
13-Oct-97 at 12:49 PM
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Sample ID:
YCP-180
TLI Samole ID:
182-30-16C
Date Received:
Sewember 09.1997
Date Prepared:
Sewember 18.1997
Date Analvzed:
October 03-04. 1997
Matrix:
MM TRAIN
: Arsalvte :
Cone.
———
tasr-:
?; Final Vd.
Diutior*
Factor
Totafuq ¦
Result
As
20.116
m
N/A
100
1
2.01
Be
-0.062
m
N/A
100
1
< 0.100
Cd
0.884
N/A
N/A
100
1
< 0.100
Co
-1.358
m
N/A
100
1
< 0.100
Cr
48.038
N/A
N/A
100
1
4.80
Mn
156.910
N/A
N/A
100
1
15.7
Ni
14588
N/A
N/A
100
1
1.43
Pb
69.563
N/A
N/A
100
1
6.96
Sb
-0.8(12
N/A
N/A
100
1
< 0.400
Se
46.133
N/A
N/A
100
1
4.61
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713
Tele: (919) 544-5729 * Fax: (919) 544-5491
Printed: 13-Oct-97 at 12:49 PM
16
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Samole ID:
YCP-181
TLI Samole ID:
182-30-16D
Date Received:
Seotember 09.1997
Date Prepared:
Seotember 18,1997
Date Analvzed:
Oaober 03-04.1997
Matrix:
MM TRAIN
Analvte
vy.Rhai Vdl.
: DSutkjn
¦¦¦: factor :
Total uq:
Result
As
21.761
N/A
N/A
100
1
2.18
Be
-0.208
n/a
N/A
100
1
< 0.100
Cd
2.311
N/A
N/A
100
1
0.231
Co
-1.341
N/A
N/A
100
1
< 0.100
Cr
88.634
N/A
N/A
100
1
8.86
Mri
324.012
N/A
N/A
100
1
32.4
Ni
17.479
N/A
N/A
100
1
1.75
Pb
254.724
N/A
N/A
100
1
25.5
Sb
-0.729
N/A
N/A
100
1
< 0,400
Se
54.026
N/A
N/A
100
1
5.40
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713 Printed: 13-Oct-97 at 12:49 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
17
-------
Client: Eastern Research Group
Project Number: 43159B
Sample Report
Client Sample ID:
YCP-182
TLI Sample ED:
182-30-16E
Date Received:
September 09.1997
Date Prepared:
September 18.1997
Date Analvzed:
October 03-04.1997
Matrix:
MM TRAIN
Analvte
I.Cone: :
: foot*
• • a;-
Total \tofc
Final Vol.
DSufon
. . Factor
Totaiuq
Resuit
As
23.961
m
N/A
100
1
2.40
Be
0.102
m
N/A
100
1
< 0.100
Cd
-0.260
m
N/A
100
1
< 0.100
Co
-1.319
m
N/A
100
1
< 0.100
Cr
12.013
WA
N/A
100
1
120
Mri
9.872
N/A
N/A
100
1
0.987
Ni
10.495
m
N/A
100
1
1.05
Pb
6.726
N/A
N/A
100
1
0.673
Sb
2.295
N/A
N/A
100
1
< 0.400
Se
40.226
WA
N/A
100
1
4.02
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, North Carolina 27713 Printed: 13-Oct-97 at 12:49 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
18
-------
Client: Eastern Research Group
Project Number: 43159B
OA: Serial Dilution
Client Samcle ID:
YCP-178
YCP-178 L
FLI Samnle ID:
182-30-16A
182-30-16 A L
Date Prepared:
Sentember 18.1997
Senrember 18.1997
Date Analyzed:
October 03-04.1997
October 03-04.1997
Vfatrix:
MM TRAIN
MM TRAIN
Native Sample
Serial Dilution
RPD
AnaMe
gppjjHI
¦¦ 1
>\..,Conc.-'
As
4.21
42.134
5.50
11.009
-------
Client: Eastern Research Group
Project Number: 43159B
QA: Duplicate
Client Samnle ID:
YCP-179
YCP-179 DA
TLI Samole ID:
182-30-16B
182-30-16B DA
Date Prepared:
September 18. 1997
Sentember 18. 1997
Date Analvzed:
October 03-04.1997
October 03-04.1997
Matrix:
MM TRAIN
MM TRAIN
Sample
Duplicate
Total ug
ug/L
Total ug
ug/L
RPD
Analyte
Result
Cone.
Rest#
Cone.
As
2.91
29 054
2.69
26 904
-------
Client: Eastern Research Group
Project Number: 43159B
QA: Matrix Spikes (Post-Digestion)
Client Sample ID:
YCP-178PDS
TLI Sample ID:
182-30-16APDS
Date Prepared:
September 18,1997
Date Analyzed:
October 03-04.1997
Matrix:
MM TRAIN
Post-Diaestion Spike
Post-Diaestion Spike Duplicate
: : RPD
Anaivte
Recovered
Airount fua/lV
spiifiii
Amountiua/U
liiiiPei*!
Reca^red::|
: Amount (uq/U
Spike
Amount (uo?L)
ii:;s -
:Recove*v:
As
92.17
50
100%
—
Be
49.08
50
98%
—
Cd
58.55
50
102%
—
Co
51.15
50
102%
—
Cr
298.15
50
Soike Low
—
Mn
1913.59
50
Spike Low
—
Ni
92.72
50
100%
—
Pb
181.35
50
99%
—
Sb
50.29
50
101%
—
Se
151.57
50
137%
—
,—
—
—
—
—
—
_
—
—
—
—
—
—
_
—
—
__
_
—
,—
—
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 27713 Printed: 13-Oct-97 at 01:03 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
21
-------
Client: Eastern Research Group
Project Number: 43159B
QA: Method Blank
TLI Samde ID:
43159B MB
Date Prepared:
September 18,1997
Date Analvzed:
October 03-04.1997
Matrix:
MM TRAIN
Method Blank
Analvte
Recovered
Amount TutyLV
: Limit {uqiU
Passor
Fail
As
-0.69
5
Pass
Be
0.09
1
Pass
Cd
-0.15
1
Pass
Co
-0.44
1
Pass
Cr
0.41
2
Pass
Mri
0.46
2
Pass
Ni
-0.72
3
Pass
Pb
0.93
2
Pass
Sb
-0.88
4
Pass
Se
-1.00
3
Pass
—
—
—
—
¦
—
—
—
—
—
—
—•
—
—
—
—,
—
—
—
_
_
—
—
_
Triangle Laboratories, Inc.
801 Capitola Drive * Durham, NC 2771 Printed: 13-Oct-97 at 01:03 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
22
-------
Client: Eastern Research Group
Project Number: 43159B
QA: Lab Control Spikes
TLI Sample ID:
43159B LCS
Date Prepared:
September 18,1997
Date Analyzed:
October 03-04.1997
Matrix:
N/A
Lab Control SDike
Lab Control SDike DuDlicate
Recovered
Spike
%
Recovered
Spike
:¦ ¦ %
RPD
Anaivte
Amount (uq/L)
Amount (uq/L)
: Recovery
Amount (uq/U
Amount (uq/L)
Recovery
As
45.87
50
9?%
Be
46.15
50
92°/c
—
Cd
47.91
50
96%
—.
Co
47.80
50
96%
.—.
Cr
48.57
50
97%
—
Mn
48.02
50
96%
—
Ni
47.82
50
96%
Pb
48.60
50
97%
—
Sb
48.00
50
96%
—
Se
45.02
50
90%
.—
—
—
_
—
—
—
.—
.—
—.
_
_
—
.—
.—
—
_
—
Triangle Laboratories, Inc.
801 Capitola Drive* Durham, NC 27713 Printed: 13-Oct-97 at 01:03 PM
Tele: (919) 544-5729 * Fax: (919) 544-5491
23
-------
ient:
Eastern Research Group
oiect Number:
43159B
ample Report
e Received:
September 09, 1997
e Prepared:
September 18-24,1997
e Analyzed:
September 24.1997
TAHLE:
AB809
trix:
MM TRAIN
ANALYTE: Ha
ua/L RDL: 0.2
Analysis Method:
29
Instalment: P E Zeeman 5100
Soike Cone. fuo/Ll
CVAA ANALYTE SUMMARY REPORT
KrtSamoie !D
TUSAMP'D
liiil
II iif
iWEill
Slil
mi
A'kjuot
DJL
FACFOF
Total uq
liiisiit
Ava
illiisiiSS
RPD
! ¦¦ %REC
C-178
182-30-16A
0.099
N/A
100
5
1
< 0.400
C-178D
182-30-16AD
0.097
N/A
100
5
1
< 0.400
< 0.400
—
-
C-179
182-30-16B
0.140
N/A
100
5
1
< 0.400
—
—
C-179D
182-30-16B D
0.132
N/A
100
5
1
< 0.400
< 0.400
-
-
C-180
182-30-16C
0.048
N/A
100
5
1
< 0.400
__
—
C-180D
182-30-16CD
0.051
N/A
100
5
1
< 0.400
< 0.400
—
-
C-181
182-30-16D
0.040
N/A
100
5
1
< 0.400
—
C-181 D
182-30-160 D
0.043
N/A
100
5
1
< 0.400
< 0.400
-
-
C-182
182-30-16E
0.156
N/A
100
5
1
< 0.400
—
—
C-182D
182-30-16ED
0.142
N/A
100
5
1
< 0.400
< 0.400
—
—
C-178 MS
182-30-16A MS
6.621
N/A
100
5
1
13.2
_
_
132%
C-178 MSD
182-30-16A MSD
5.770
N/A
100
5
1
11.5
12.4
13.7%
115%
C-179 MS
True Spike MS
5
N/A
100
5
1
10.0
—
..
C-179 MSD
True Spike MSD
5
N/A
100
5
1
10.0
—*
~
ithod Blank
43159B MB
0.030
_
ithod Blank D
43159BMBD
0.013
-
-
-
-
-
-
-
--
S
43159BLCS
5.284
—
—
—
106%
SD
43159BLCSD
5.088
—
—
—
—
102%
angle Laboratories, Inc.
1 Capitola Drive * Durham, North Carolina 27713 Printed: 14-Oct-97 at 03:14 PM
le: (919) 544-5729 * Fax: (919) 544-5491
24
-------
Eastern Research Group COC
Younqstown Sintering Plant
CHAIN OF CUSTODY
RELINQUISHED BY =.
RELINQUISHED BY ¦»
hf
DATE'
DATE'
*?; 9 -97
win
RECEIVED BY
RECEIVED BY:
3^
DATE
IO
CVf
SAMPLE ID
FIELD ID
SAMPLE TYPE
PRESERVATIVE
' COMMENTS
ANALYSIS
YCP-01
YCP-
81297
M29-
SBOUTLET-
APR-
1
METHOD 29. SBOUTLET, RUN 1
ACETONE PROBE RINSE
Beaker # 1
266.5
404.5
YCP-02
YCP-
81297
M29-
SBOUTLET-
HN-
1
METHOD 29, SBOUTLET, RUN 1
NITRIC ACID PROBE RINSE
267.5
411.5
YCP-03
YCP-
81297
M29-
SBOUTLET-
BH-
1
METHOD 29, SBOUTLET, RUN 1
HN03/H202 BACK HALF
l
391.3
1126.7
YCP-04
YCP-
81297
M29-
SBOUTLET-
BHM-
1
METHOD 29, SBOUTLET, RUN 1
0.1NHNO3 RINSE - Hg
269.4
360.0
YCP-05
YCP-
81297
M29-
SBOUTLET-
KMnO-
1
•..METHOD 29, SBOUTLET, RUN 1
KMn04 IMPINGERS
268.5
531.2
YCP-06
YCP-
81297
M29-
SBOUTLET-
HCI-
1
METHOD 29, SBOUTLET. RUN 1
8N HCI RINSE - Hg
270.5
595.2
YCP-07
YCP-
81397
M29-
SBOUTLET-
APR-
2
METHOD 29. SBOUTLET. RUN 2
ACETONE PROBE RINSE
Beaker # 2
267.2
326.2
YCP;08
YCP-
81397
M29-
SBOUTLET-
HN-
2
METHOD 29, SBOUTLET, RUN 2
NITRIC ACID PROBE RINSE
.
270.8
480.6
YCP-09
YCP-
81397
M29-
SBOUTLET-
BH-
2
METHOD 29, SBOUTLET, RUN 2
HN03/H202 BACK HALF
391.1
1246.0
YCP-10
YCP-
81397
M29-
SBOUTLET-
BHM-
2
METHOD 29. SBOUTLET, RUN 2
0.1 N HN03 RINSE - Hg
270.7
346.0
YCP-11
YCP-
81397
M29-
SBOUTLET-
KMnO-
2
METHOD 29, SBOUTLET. RUN 2
KMn04 IMPINGERS
268.7
648.7
YCP-12
YCP-
81397
M29-
SBOUTLET-
HCI-
2
METHOD 29, SBOUTLET. RUN 2
8N HCI RINSE - Hg
*
268.9
606.2
YCP-13
YCP-
81497
M29-
SBOUTLET-
APR-
3
METHOD 29, SBOUTLET, RUN 3
ACETONE PROBE RINSE
. Beaker # 3
266.7
375.0
YCP-14
YCP-
81497
M29-
SBOUTLET-
HN-
3
METHOD 29, SBOUTLET, RUN 3
NITRIC ACID PROBE RINSE
267.4
375.4
YCP-15
YCP-
81497
M29-
SBOUTLET-
BH-
3
METHOD 29, SBOUTLET, RUN 3
HN03/H202 BACK HALF
391.7
1206.1
YCP-16
YCP-
81497
M29-
SBOUTLET-
BHM-
3
METHOD 29, SBOUTLET, RUN 3
0.1N HN03 RINSE - Hg
267.3
316.6
YCP-17
YCP-
81497
M29-
SBOUTLET-
KMnO-
3
METHOD 29, SBOUTLET. RUN 3
KMn04 IMPINGERS
267.1
655.6
YCP-18
YCP-
81497
M29-
SBOUTLET-
HCI-
3
METHOD 29. SBOUTLET. RUN 3
8N HCI RINSE - Hg
267.1
491.3
YCP-19
YCP-
81297
M29-
SBINLET-
APR-
1
METHOD 29. SBINLET, RUN 1
ACETONE PROBE RINSE
Beaker #11
266.7
457.8
YCP-20
YCP-
81297
M29-
SBINLET-
HN-
1
METHOD 29, SBINLET. RUN 1
NITRIC ACID PROBE RINSE
268.6
410.6
/YCP-21
YCP-
81297
M29-
SBINLET-
BH-
1
METHOD 29, SBINLET. RUN 1
HN03/H202 BACK HALF
391.3
1076.4
' YCP-22
YCP-
81297
M29-
SBINLET-
BHM-
1
METHOD 29. SBINLET, RUN 1
0.1NHNO3 RINSE - Hg
270.8
342.4
YCP-23
YCP-
81297
M29-
SBINLET-
KMnO-
1
METHOD 29. SBINLET. RUN 1
KMn04 IMPINGERS
269.6
607.4
YCP-24
YCP-
81297
M29-
SBINLET-
HCI-
1
METHOD 29. SBINLET. RUN 1
8N HCI RINSE - Hg
269.3
581.0
YCP-25
YCP-
81397
M29-
SBINLET-
APR-
2
METHOD 29. SBINLET, RUN 2
ACETONE PROBE RINSE
Beaker# 12
267.7
537.0
YCP-26
YCP-
81397
M29-
SBINLET-
HN-
2
METHOD 29. SBINLET. RUN 2
NITRIC ACID PROBE RINSE
266.5
554.0
Page 1
-------
Eastern Research Group COC
CO
CM
(^?CP-27/
YCP-
81397
M29-
SBINLET-
BH-
2
METHOD 29, SB1NIET, RUN 2
HN03/H202 BACK HALF
391.6
1161.6
YCP-
81397
M29-
SBINLET-
BHM*
2
METHOD 29, SBINLET, RUN 2
0,1 N HN03 RINSE-Hg
267.5
365.3
YCP-29
YCP-
81397
M29-
SBINLET-
KMnO-
2
METHOD 29, SBINLET, RUN 2
KMn04 IMPINGERS
266.5
718.9
YCP-30
YCP-
81397
M29-
SBINLET-
HCi-
2
METHOD 29, SBINLET, RUN 2
8NHCI RINSE-Hg
267.1
605.4
YCP-31
YCP-
81497
M29-
SBINLET-
APR-
3
METHOD 29, SBINLET. RUN 3
ACETONE PROBE RINSE
Beaker# 13
267.3
495,3
YCP-32
YCP-
81497
M29-
SBINLET-
HN-
3
METHOD 29, SBINLET, RUN 3
NITRIC ACID PROBE RINSE
266.3
410.9
/ycp3~>
YCP-
81497
M29-
SBINLET-
BH-
3
METHOD 29, SBINLET, RUN 3
HN03/H202 BACK HALF
391.5
1295.3
YCP-34
YCP-
81497
M29-
SBINIET-
BHM-
3
METHOD 29, SBINLET, RUN 3
0.1NHNO3 RINSE - Hg
266.5
394.5
YCP-35
YCP-
81497
M29-
SBINIET-
KMnO-
3
METHOD 29, SBINLET, RUN 3
KMn04 IMPINGERS
266.2
725,4
YCP-36
YCP-
81497
M29-
SBINLET-
HCI-
3
METHOD 29, SBINLET, RUN 3
8N HCI RINSE - Hg
267.5
438.6
YCP-37
YCP-
81397
M29-
SBOUTIET-
APR-
FB1
METHOD 29, SBOUTLET, FBI
ACETONE PROBE RINSE
Beaker # 4
269,3
369.0
YCP-38
YCP-
81397
M29-
SBOUTLET-
HN-
FBI
METHOD 29, SBOUTLET, FB1
NITRIC ACID PROBE RINSE
269.4
398,6
YCP-39
YCP-
81397
M29-
SBOUTIET-
F- .
FBI
METHOD 29, SBOUTLET, FBI
FILTER
Filter« 080487-24
XX
XX
YCP-40
YCP-
81397
M29-
SBOUTLET-
BH-
FBI
METHOD 29, SBOUTLET, FB1
HN03/H202 BACK HALF
268.2
573.2
YCP-41
YCP-
81397
M29-
SBOUTLET-
BHM-
FB1
METHOD 29, SBOUTLET, FBI
0.1 N HN03 RINSE • Hg
269.4
316.9
YCP-42
YCP-
81397
M29-
SBOUTLET-
KMnO-
FBI
METHOD 29, SBOUTLET. FBI
KMn04 IMPINGERS
269.4
752.3
YCP-43
YCP-
81397
M29-
SBOUTLET-
HCI-
FB1
METHOD 29. SBOUTLET, FBI
8N HCI RINSE - Hg
269.2
429.6
YCP-
81397
M29-
SBOUTLET-
ACE-
RB1
METHOD 29, SBOUTLET, RB1
ACETONE
•
269.5
444,0
YCP-4S
YCP-
81397
M29-
SBOUTIET-
HNO-
RB1
METHOD 29, SBOUTLET, R81
0.1 N HN03
269.3
739.8
YCP-
B1397
M29-
SBOUTLET-
p.
RB1
METHOD 29, SBOUTLET, RB1
FILTER
Filter #080497-01
XX
XX '
YCP-47
YCP-
81397
M29-
SBOUTLET-
BH-
RB1
METHOD 29, SBOUTLET, RB1
HN03/H202
268.4
567.3
YCP-48
YCP-
81397
M29-
SBOUTLEI-
KMnO-
RB1
METHOD 29, SBOUTLET, RB1
KMn04
269.1
493.3
YCP-49
YCP-
81397
M29-
SBOUTLET-
HCI-
RB1
METHOD 29, SBOUTLET, RB1
8N HCI
268.9
510.2
YCP-SO
YCP-
81397
M29-
SBINLET-
APR-
FB2
METHOD 29, SBINLET, FB2
ACETONE PROBE RINSE
Beaker # 5
268.2
387.0
YCP-51
YCP-
81397
M29-
SBINLET-
HN-
FB2
METHOD 29, SBINLET, FB2
NITRIC ACID PROBE RINSE
267.2
439,2
YCP-52
YCP-
81397
M29-
SBINIET-
F-
FB2
METHOD 29, SBINLET, FB2
FILTER
Filler # 080497-23
XX
XX
- YCP-53
YCP-
81397
M29-
SBINLET-
BH-
FB2
METHOD 29, SBINLET, FB2
HN03/H202 BACK HALF
269.4
795.8
YCP-54
YCP-
81397
M29-
SBINLET-
BHM-
FB2
METHOD 28, SBINLET, FB2
0,1 N HN03 RINSE - Hg
268.5
333.4
YCP-55
YCP-
81397
M29-
SBINLET-
KMnO-
FB2
METHOD 29, SBINLET, FB2
KMn04 IMPINGERS
268.7
691.5
YCP-56
YCP-
81397
M29-
SBINLET-
HCI-
FB2
METHOD 29, SBINLET. FB2
8N HCI RINSE - Hg
269.7
439.3
YCP-57
YCP-
81597
M29-
SBINLET-
AGE-
RB2
METHOD 29. SBINLET, RB2
ACETONE
Beaker # 6
268.1
407.0
Page 2
-------
Eastern Research Group COC
rv
c\t
YCP-58
YCP-
81597
M29-
SBINLET-
HNO»
RB2
METHOD 29. SBINLET, RB2
0.1N HN03
391.7
648.0
YCP-
81597
M29-
SBINLET-
F-
RB2
METHOD 29, SBINLET. RB2
FILTER
XX
XX
YCP-60
YCP-
81597
M29-
SBINLET-
BH-
RB2
METHOD 29, SBINLET, RB2
HN03/H202
391.6
636.3
YCP-61
YCP-
81597
M29-
SBINLET-
KMnO-
RB2
METHOD 29, SBINLET, RB2
KMn04
391.2
650.3
YCP-62
YCP-
81597
M29-
SBINLET-
HCI-
RB2
METHOD 29, SBINLET. RB2
8N HCI
390.9
602.2
YCP-88
YCP-
81297
M29-
SBOUTLET-
F-
1
METHOD 29, SBOUTLET, RUN 1
-
FILTER # 080497-20
XX
XX
YCP-89
YCP-
81397
M29-
SBOUTLET-
F-
2
METHOD 29, SBOUTLET, RUN 2
FILTER M 080497-15
XX
XX
YCP-90
YCP-
81497
M29-
SBOUTLET-
F-
3
METHOD 29, SBOUTLET, RUN 3
FILTER # 080497-19
XX
XX
YCP-91
YCP-
81297
M29-
SBINLET-
Ff
1
METHOD 29, SBINLET. RUN 1
FILTER # 080497-22
XX
XX
YCP-92
YCP-
81397
M29-
SBINLET-
F-
2
METHOD 29, SBINLET, RUN 2
FILTER # 080497-21 (1 of 2)
XX
XX
YCP-93
YCP-
81497
M29-
SBINLET-
F-
3
*• METHOD 29. SBINLET, RUN 3
FILTER # 080497-05 (1 of 2)
XX
XX
YCP-94
YCP-
81597
M29-
BAGAOUT-
APR-
1
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
Beaker # 7
269.1
323.0
YCP-95
YCP-
81597
M29-
BAGAOUT-
HN-
1
METHOD 29, BAG A OUTLET, RUN
NITRIC ACID PROBE RINSE
269.1
336.9
YCP-96
YCP-
81597
M29-
BAGAOUT-
F-
1
METHOD 29. BAG A OUTLET. RUN
FILTER
Filter # 080497-08
XX
XX
YCP-97
YCP-
81597
M29-
BAGAOUT-
BH-
1
METHOD 29. BAG A OUTLET, RUN
HN03/H202
268.6
768.4
YCP-98
YCP-
81597
M29-
BAGAOUT-
BHM-
1
METHOD 29, BAG A OUTLET, RUN
0.1NHNO3 RINSE - Hg
271.0
322 3
YCP-99
YCP-
81597
M29-
BAGAOUT-
KMn04-
1
METHOD 29, BAG A OUTLET, RUN
KMn04 IMPINGERS
270,1
601.6
YCP-100
YCP-
81597
M29-
BAGAOUT-
HC!-
1
METHOD 29, BAG A OUTLET, RUN
8N HCI RINSE - Hg
269.5
406.3
YCPJ01
YCP-102
YCP-_
YCP-
81597
81597
M29-
BAGAOUT-
APR-
2
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
. BoakorM 8
268.3
324.5
M29-
BAGAOUT-
HN-
2
METHOD 29. BAG A OUTLET, RUN
NITRIC ACID PROBE RINSE
268.6
372.2
YCP-103
YCP-
81597
M29-
BAGAOUT-
F-
2
METHOD 29. BAG A OUTLET, RUN
FILTER
Filler It 080497-06
XX
XX
YCP-104
YCP-
81597
M29-
BAGAOUT-
BH-
2
METHOD 29, BAG A OUTLET, RUN
HN03/H202
388.7
1089.7
YCP-105
YCP-
81597
M29-
BAGAOUT-
BHM-
2
METHOD 29, BAG A OUTLET. RUN
0.1N HN03 RINSE-Hg
268.6
348,0
YCP-106
YCP-
81597
M29-
BAGAOUT-
KMn04-
2
METHOD 29, BAG A OUTLET. RUN
KMn04 IMPINGERS
268.3
610.6
YCP-107
YCP-
81597
M29-
BAGAOUT-
HCi-
2
METHOD 29, BAG A OUTLET, RUN
8N HCI RINSE - Hg
269.4
517.8
YCP-108
YCP-
81697
M29-
BAGAOUT-
APR-
3
METHOD 29, BAG A OUTLET, RUN
ACETONE PROBE RINSE
Beaker # 9
265.2
318.4
YCP-109
YCP-
81697
M29-
BAGAOUT-
HN-
3
METHOD 29, BAG A OUTLET, RUN
NITRIC ACID PROBE RINSE
265.5
344,9
YCP-110
YCP-
81697
M28-
BAGAOUT-
F-
3
METHOD 29, BAG A OUTLET. RUN
FILTER
Filler # 080497-14
XX
XX
YCP-111
YCP-
81697
M29-
BAGAOUT-
BH-
3
METHOD 29, BAG A OUTLET, RUN
HN03/H202
389.1
1040.1
YCP-112
YCP-
81697
M29-
BAGAOUT-
BHM-
3
METHOD 29, BAG A OUTLET, RUN
0.1NHNO3 RINSE-Ho
266.6
333.6
YCP-113
YCP-
81697
M29-
BAGAOUT-
KMn04-
3
METHOD 29. BAG A OUTLET, RUN
KMn04 IMPINGERS
267.8
609.5
Pa/ml
-------
Eastern Research Group COC
00
CM
YCP-114
YCP-
81697
M29-
BAGAOUT-
HCI-
3
METHOD 29, BAG A OUTLET, RUN
8N HCI RINSE - Hg
266.1
486.2
YCP-141
YCP-
81597
M29-
BAGA
APR-
GPB1
ETHOD 29, BAGA, GLASSWARE BL
ACETONE PROBE RINSE
Archived at ERG
268.5
310.1
YCP-142
YCP-
81597
M29-
BAGA
HCI-
GP81
ETHOD 29, BAGA, GLASSWARE BL
8N HCI RINSE - Hg
Archived at ERG
269.1
482.8
YCP-143
YCP-
81597
M29-
BAGA
HN-
GBP1
ETHOD 29, BAGA, GLASSWARE BL
NITRIC ACID PROBE RINSE
Archived at ERG
268.9
329.1
YCP-144
YCP-
8159?
M29-
BAGA
APR-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
ACETONE PROBE RINSE
Archived at ERG
268.4
302.4
YCP-14S
YCP-
81597
M29-
BAGA
BH-
GBP1
ETHOD 29, BAGA, GLASSWARE BL
HN03/H202
Archived at ERG
269.1 •
624.4
YCP-146
YCP-
81597
M29-
BAGA
HN-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
NITRIC ACID PROBE RINSE
Archived at ERG
268.1
399.9
YCP-147
YCP-
81597
M29-
BAGA
IMP
GBP1
ETHOD 29, BAGA, GLASSWARE BL
0.1NHNO3 RINSE - Hg
Archived at ERG
26B.7
336.2
YCP-148
YCP-
81597
M29-
BAQA
BH»
GPB2
ETHOD 28, BAGA, GLASSWARE BL
HN03/H202
Archived at ERG
28S.4
590.9
YCP-149
YCP-
81597
M29-
BAGA
KMn04-
GBP1
ETHOD 29, BAGA, GLASSWARE Bl
KMn04 IMPINGERS
Archived at ERG
268.5
613.4
YCP-150
YCP-
81597
M29-
BAGA
IMP
GPB2
ETHOD 29, BAGA, GLASSWARE BL
0.1NHNO3 RINSE - Hg
Archived at ERG
268.6
370.5
YCP-151
YCP-
81597
M29-
BAGA
KMn04-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
KMn04 IMPINGERS
Archived at ERG
268.4
445.6
__YCP-152_
YCP-159
YCP-
81597
81697
M29-
BAGA
HCI-
GPB2
ETHOD 29, BAGA, GLASSWARE BL
8N HCI RINSE - Hg
Archived at ERG
268.8
446.8
YCP-
M29-
BAGA-
APR-
FB
METHOD 29, INLET, FB2
ACETONE PROBE RINSE
Beaker # 10
275.8
326.4
YCP-160
YCP-
81697
M29-
BAGA-
HN-
FB
METHOD 29, INLET, FB2
NITRIC ACID PROBE RINSE
274.8
369.6
YCP-161
YCP-
81697
M29-
BAGA-
BH-
FB
METHOD 29, INLET, FB2
HN03/H202 BACK HALF
391,6
8597
YCP-162
YCP-
81697
M29-
BAGA-
IMP
FB
METHOD 29. INLET, FB2
0.1N HN03 RINSE - Hg
268.4
309,8
YCP-163
YCP-
81697
M29-
BAGA-
KMnO-
FB
METHOD 29, INLET, FB2
KMn04 IMPINGERS
-
268.4
599.0
YCP-164
YCP-
81697
M29-
BAGA-
HCI-
FB
METHOD 29. INLET, FB2
8N HCI RINSE - Hg
268.4
411.5
YCP-165
YCP-
81697
M29-
BAGA-
F
FB
METHOD 29, INLET, FB2
FILTER
Filter U 080497-03
XX
XX
YCP-170
YCP-
81397
M29-
.
RB1
METHOD 29, REAGENT BLANK
Dl WATER
393.0
803 8
YCP-171
YCP-
81597
M29-
.
RB2
METHOD 29, REAGENT BLANK
Dl WATER
391.1
795.9
YCP-178
YCP-
9/2/97
M29-
SBINLET
FILTER
RUN1
FILTER FOR YCP-21
FILTER
Filter (8 082797-02
METALS
YCP-179
YCP-
9/2/97
M29-
SBINLET
FILTER
RUN2
FILTER FOR YCP-27
FILTER
Filter #082797-03
METALS
YCP-180
YCP-
9/2/07
M29-
SBINLET
FILTER
RUN3
FILTER FOR YCP-33 (1 of 2)
FILTER
Filter # 082797-04
METALS
YCP-181
YCP-
9/2/97
M29-
SBINLET
FILTER
RUN3
FILTER FOR YCP-33 ( 2 o» 2)
FILTER
Filter« 082797-05
METALS
YCP-182
YCP-
9/2/97
M29-
BLANK
FILTER
BLANK
FILTER BLANK
FILTER
Filler U 082797-01
METALS
YCP-183
YCP-
8/13/97
M29-
SBINLET
FILTER
RUN2
2nd Filter fo SBInlet Run 2 (2of2)
FILTER
Filter #080497-25 (2 of 2)
METALS
YCP-184
YCP-
8/14/97
M29-
SBINLET
FILTER
RUN3
2nd Filter fo SBInlet Run 3 (2of2)
FILTER
Filter # 080497-18 (2 of 2)
METALS
Page 4
-------
LABORATORIES, INC. -- LOO IN RECORD/CHAIN OF CUSTODY'
| TLI Project Number *3159 ,
[ Client! ER002 - Eastern Research Group
Custody Seal
Chain of Custody i Present
Sample Tags < Absent
Sample Tag Numbersi Not Listed on Chain of Custody
SMO Forms ! N/A
Sample Seals: Absent
Container...i Intact
i Absent
j 09/09/97 j By-
Date Received
Carrier and Number I JIM MC
Ice Chest/Box
NO COOLANT
To STORAGEj To LAB
Date/Init j Date/Init | Date/lnit
Matrix) To LAB
|TLI Number Client Sample ID
||mR/H:CPM Client COC ID.
To STORAGE| DISPOSED
Date/lnit | Date/Init
To STORAGE I To LAB
Date/lnit | Date/lnit
To STORAGE
| Date/Init j Date/Init
Location
BEAKER
YCP-01
YCP-01
METALS LAB
YCP-02
YCP-02
PR
METALS LAB
j| 182-3Q-1C
YCP-03
YCP-03
METALS LAB
0.1N UNO3
YCP-04
YCP-04
METALS LAB
KMN04 j
YCP-05
YCP-05
METALS LAB
HCL|
182-30-1F
YCP-06
YCP-06
METALS LAB
FILTER
METALS LAB
YCP-07
YCP-07
METALS LAB
PR
METALS LAB
KN03/H202
182-30-2C
METALS LAB
YCP-10
YCP-10
• . METALS LAB
KMN04
YCP-11
YCP-11
METALS LAB
HCL
METALS LAB
FILTER
YCP-89
YCP-B9
METALS LAB
Receiving Remarks! YCP-21.YCP-27,YCP-33,YCP-44 ,YCP-B9 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
U 'Archive Remarks s
'Form Revised 05/27/1997 -- Page 1 OF
li I I. I M, I ..." ¦ TRIANGLE LABORATORIES, INC. -- LOO IN RECORD/CHAIN OF CUSTODY • (fi ij '
II Custody Seal i Absent Sample Seals: Absent | TLI Project Number 43159 , I BookCjjj
| Chain of Custody i Present Container...! Intact j Client! ERG02 - Eastern Research Group | f
jj Sample Tags < Absent I I H2 I
jj Sample Tag Numbers i Not Listed on Chain of Custody | 1 1 a_)i/J j/8" 1
j SMO Forms ! N/A * j Date Received | 09/09/97 j By fax /? A?T '*3" II
ii 1 1 < v! rv rns if j H
II Ice Chest/Box NO COOLANT | Carrier and Number | JIM MC | 30 ||
||TLI Number Client Sample ID f Matrix) To LAB | To STORAGE| To LAB | To STORAGE) To LAB | To STORAGE| To LAB | To STORAGE) DISPOSED ||
|jmR/ll:CPM Client COC ID * Location j Date/Init j Date/Init | Date/Init j Date/Init | Date/lnit j Date/lnit | Date/Init j Date/lnit j Date/Init jj
|| 1 1 1 1 1 1 ) 1 ) 1
|| 182-30- 1A YCP-01 BEAKER) I I I I I I I I 0
jj YCP-01 METALS LAB j I • " I I I I I I I I
II— 1 1 1 — 1 1 —! 1 1 1 II
||l82-30-lB YCP-02 PR j | I I I I I I I H
jj YCP-02 METALS LAB j | j j j I I I j It
|| 1 1 1 1 1 1 1 1 1 1|
|| 182-3Q-1C YCP-03 IM03/H202) I I I I I I I I I
jj YCP-03 METALS LAB j j j I I i i I 1 I
|| 1 1 1 , 1 1 ] 1 1 1|
||l82-30-lD YCP-04 0. IN HN031 | | | | | | | | |
jj YCP-04 METALS LAB j j | I I j j ) I ' II
|| 1 1 j t_| 1 1 1 1 1 1
II182-30-1E YCP-05 KMN041 I I I I I I I I II
II YCP-05 METALS LAB I I I I I I I I I I!
|| 1 1 1 , 1 —| 1 1 1 1|
|| 182-30-1F YCP-06 , HCL| I I I I I I I I II
|| YCP-06 METALS LAB | j | j ) | | | | ||
|| 1 1 1 1 1 1 1 1 1
||l82-30-lG YCP-88 FILTER| I I I I I I I I II
jj YCP-88 METALS LAB 1111111111
II 1 1 1 1 1 1 * 1 h- 1 II
||l82-30-2A YCP-07 • BEAKER| I I I I I I I I II
jj YCP-07 METALS LAB j j j | j 1*1 I I II
n ; 1 1 1—; 1 1 1 1 1 II
||l82-30-2B YCP-08 PR| | I I I I I I II
jj YCP-08 METALS LAB j | I I I I I I II
-------
LOO IN RECORD/CHAIN OF CUSTODY
| TLI Project Number 43159 ,
| Client: ERG02 - Eastern Research Group
TRIANGLE LABORATORIES, INC.
Sample Seals: Absent
Container...: Intact
Custody Seal
Chain of Custody : Present
Sample Tags
Sample Tag Numbers: Not Listed on Chain of Custody
: N/A
Absent
Absent
09/09/97 j By
Page
Date Received
SMO Forms
Carrier and Number j JIM MC
Ice Chest/Box
NO COOLANT
DISPOSED
Date/Init
To STORAGE
Date/Init
Matrix
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
TLI Number
mR/H:CPM.
....Client Sample ID
Client COC ID.
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
Location
BEAKER
82-30-3A
YCP-13
YCP-13
METALS LAB
YCP-14
YCP-14
PR
METALS LAB
HN03/H202
82-30-3C
YCP-15
YCP-15
METALS LAB
YCP-16
YCP-16
82-30-3D
METALS LAB
KMN04
82-30-3E
YCP-17
YCP-17
YCP-18
YCP-18
HCL
82-30-3F
METALS LAB
FILTER
182-30-3G
YCP-90
YCP-90
METALS LAB
YCP-19
YCP-19
BBAKCR
162-30-4A
METALS LAB
YCP-20
YCP-20
METALS LAB
0.1NHN03
YCP-22
YCP-22
182-30-4C
METALS LAB
YCP-23
YCP-23
182-30-4D
• . METALS LAB
YCP-24
YCP-24
HCL
METALS LAB
FILTER
182-30-4F
YCP-91
YCP-91
METALS LAB
YCP-25
YCP-25
BEAKER
182-30-5A
METALS LAB
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
Archive Remarks:
'Form Revised 05/27/1997
Page 2 OF
182-30-5A YCP-25 BBAKER| I j I I j I I j II
YCP-25 METALS LAB I I I I I I I I I H
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Also a YCP-169 ||
filter arrived But is not listed on C.O.C. jj
II
Archive Remarks: II
.. 05/27/1997 -- Page 2 OF 8 'I
-------
=TRIANGLE LABORATORIES, INC. -- LOO IN RECORD/CHAIN OF CWSTODY«=
Custody Seal s Absent
Chain of Custody i Present
Sample Tags : Absent
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forma i N/A
Sample Sealsi Absent
Container...: Intact
| TLI Project Number 43159 ,
| Clienti ERQ02 - Eastern Research Group
j Date Received
09/09/97
A
Page ||
|| Ice Chest/Box
NO COOLANT
jjTLI Number Client Sample ID
j|mR/H;CPM Client COC ID «
=f=
.Matrix
Location....
To LAB I To STORAGE
Date/lnit | Date/Init
j Carrier and Number j JIM MC
I ¦1 " 1 1 i I"
I To STORAGE I To LAB
To LAB I To STORAOE | To LAB
Date/Init j Date/Init | Date/Init | Date/Init J Date/Init
+
+
To STORAGE
Date/Init
DISPOSED U
Date/Init |j
182-30-5B
YCP-26
YCP-26
PR
METALS LAB
182-30-5C
YCP-28
YCP-28
KMN04
METALS LAB
jj 182-30-5D
YCP-29
YCP-29
HCL
METALS LAB
I|l82-3Q-SE
YCP-30
YCP-30
FILTER
METALS LAB
182-30-SF
II
YCP-92
YCP-92
FILTER
METALS LAB
182-30-5(3
YCP-183
YCP-183
FILTER
METALS LAB
y182-30 - 6 A
||
||lB2-30-6B
II
YCP-31
YCP-31
BEAKER
METALS LAB
YCP-32
YCP-32
PR
METALS LAB
jjl82-30-6C
YCP-34
YCP-34
.IN HH03
METALS LAB
+TT
182-30-6D
YCP-35
YCP-35
KMN04
METALS LAB
-Hr
182-30-6E
YCP-36
YCP-36
HCL
METALS LAB
182-30-6F
II
YCP-93
YCP-93
FILTER
METALS LAB
|jl82-30-60
YCP-184
YCP-184
FILTER
METALS LAB
j|182-30-7A
YCP-37
YCP-37
beaker)
METALS LAB j
1.
Receiving Remarks!
|| -Archive Remarks;
YCP-21,YCP-27,YCP-33,YCP-4 4 ,YCP-59 were mining from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
Revised 05/27/1997 -- Page 3 OF 8»
-------
•TRIANGLE LABORATORIES, INC. -- LOO IN RECORD/CHAIN OP
J Custody Seal
jj Chain of Custody i Present
|j Sample Tags
: Absent Sample Sealsi Absent
Container.,.: Intact
i Absent
Sample Tag Numbers: Not Listed on Chain of Custody
s N/A
| TLI Project Number 43159
j Cllentt ERG02 - Eastern Research Group
Bo<
09/09/97 j By
Date Received
Page
SMO Forms
Ice Chest/Box
Carrier and Number I JIM HC
NO COOLANT
To STORAGE j To LAB j To ST0RA0E j DISPOSED
Date/Init j Date/Init j Date/Inlt j Date/Inlt
|TLI Number.. ....Client Sample ID
jmR/HiCPM.
.Matrix
To LAB
Date/Inlt
To STORAGE
Date/Inlt
To STORAGE
Date/Inlt
To LAB
Date/Inlt
Location
Client COC ID
PR
METALS LAB
FILTER
METALS LAB
HN03/H202
182-30-7D
YCP-40
YCP-40
METALS LAB
Hg HN03
METALS LAB
182-30-7F
METALS LAB
Hg HC1
182-30-70
METALS LAB
YCP-4S
YCP-45
METALS LAB
YCP-46
YCP-46
FILTER
METALS LAB
182-30-8C
YCP-47
YCP-47
METALS LAB
|jlB2-30-8D
KMN04
METALS LAB
j|l82-30-8E
YCP-49
YCP-49
HCL
¦ METALS LAB
X82-30-9A
METALS LAB
METALS LAB
|jl82-30-9C
YCP-S2
YCP-52
FILTER
METALS LAB
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 .YCP-59 were missing from shipment.Also a YCP-169
filter arrived But Is not listed on C.O.C.
|| Archive Remarks i
¦Form Revised 05/27/1997 -- Page 4 OF
(, ' " >¦ i.i. " - 'TRIANGLE LABORATORIES, INC. -- LOO IN RECORD/CHAIN OF CUSTODV«= ¦ ' "¦
j Custody Seal s Absent Sample Seals: Absent | TLI Project Number 43159 , j Bocw*f
|| Chain of Custody : Present Container...: Intact j Client: ERG02 - Eastern Research Group | |
|j Sample Tags : Absent | | 182 ||
|| Sample Tag Numbers: Not Listed on Chain of Custody | 1 1 /ji. —II
jj SMO Forms : N/A j Date Received j 09/09/97 j By A-pG /L-,/fo/7/y* pag* I
II— ¦ 1 1 ' '/ /tfVI/ */ 1 H
II Ice Chest/Box NO COOLANT | Carrier and Number | JIM MC v | 30 H
li- - • 1 1 1 I I " i ~ I— • •' "1 I ' 1 """ i I -¦¦¦¦¦ '-:j jj
||TLI Number.. ....Client Sample ID Matrix) To LAB | To STORAGE| To LAB | To STORAGE) To LAB | To STORAGE) To LAB ) To STORAGE) DISPOSED ||
jjmR/H:CPM. Client COC ID * Location j Date/Init j Date/Inlt | Date/Init j Date/Inlt j Date/Init j Date/Inlt j Date/Init j Date/Init j Date/Init j
|| 1 1 1 1 ^ ) 1 1 1|
||l82-30-7B YCP-38 PRl 1 I I I I I I I II
jj YCP-38 METALS LAB j j • j j j j j I I II
II H 1 1 1 1 : 1 1 1 1 —II
||l82-30-7C YCP-39 FILTER) ) I I I I I I I II
H YCP-39 METALS LAB I . I I I I I I I I II
|| 1 1 1 1 , 1 1 1 1 11
(1182-30-7D YCP-40 HN03/H202) I I I I I I I I II
|| YCP-40 METALS LAB j j | j j j j j j jj
|| 1 1 1 , , , 1 1 , 1|
||l82-30-7E YCP-41 Hg HN03) "I I I I | I I ) | '
|| YCP-41 METALS LAB j j | I I I I I I • II
lb 1 1 1 : 1 1— 1 1 1 1 II
||l82-30-7F YCP-42 Hg KMn041 | | | I I I I I II
jj YCP-42 METALS LAB j | | j j j | j j ||
II 1 1 1 1 1 —-h ) 1 1 1|
||182-30-70 YCP-43 ^ Hg HC11 I I I I I I I I II
jj YCP-43 METALS LAB I I I I I I j I I H
jjl82-30-8A YCP-45 0.1NHN03 j 111111111
jj YCP-45 METALS LAB i I I I I I I i I II
|| 1 1 1 1 ) 1—» 1 1 1 1|
||l82-30-8B YCP-4 6 • FILTER I I I I I I ) I I 0
jj YCP-4S METALS LAB ' j j ) j j 1*1 I I II
II : 1 1 1 1 : 1 1 1 ; 1 1 II
|| 182-30 -8C YCP-47 HN03/H202| I I I I I I I I H
jj YCP-47 METALS LAB j j j j j jil I II
jjlB2-30-8D YCP-48 KMN04 j j j j 1 I ) [ I D
II YCP-48 METALS LAB I I I I I I I I I II
||_ . 1 1 1 1 1_ 1 1 ^ J 1|
||182 -30-8E YCP-49 HCL| I I I ( I ) I I II
II YCP-49 METALS LAB I I I I i I I I i R
ii 1 1 1—* 1 1 1 1 1 1 n
||l82-30-9A YCP-50 BBAKEr) | | | j - j j ) j j|
j) YCP-50 METALS LAB j j j j j j ) 1*1 II
II ; 1 1 1 ¦ 1 1 1 1 1 1 II
||1B2-3D-9B YCP-S1 PR) | | | ) j j )• j ||
jj YCP-51 METALS LAB 1111111118
II h 1 1 1 1 ) H 1 1 II
||l82-30-9C YCP-52 FILTER) | | | | j | j ) |
|| YCP-52 METALS LAB I I I I I I | I I II
II . ' ' 1 ' 1 ' ' a
|| Receiving Remarks: YCP-21, YCP-27, YCP-33, YCP-44 .YCP-59 were missing from shipment .Also a YCP-169 |
|| filter arrived But Is not listed on C.O.C. jj
II II
|| Archive Remarks: ||
«« 1 1 =»Form Revised 05/27/1997 -- Page 4 OF 8- i , ¦ fl
-------
CO
CO
HN03/H202j
METALS LAB
XMN04
METALS LAB "
HCL
METALS LAB
MBTALS LAB
YCP-95
YCP-95
182-30-11B
. METALS LAB
FILTERj
METALS LAB
YCP-97
YCP-97
METALS LAB
IMP 4 j
182-30-11E
YCP-98
YCP-98
METALS LAB
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 ,YCP-59 were missing from shipment.Alio a YCP-1S9
filter arrived But is not listed on C.O.C.
¦Archive Remarks:
¦Form Revised 05/27/1997 -- Page 5 OF 8>
-------
I," ' » ¦ " TRIANGLE LABORATORIES, INC. -- LOO IN RECORD/CHAIH OF CUSTODY- " ¦ ¦ .. ( ' - ' ,|
| Custody Seal : Absent Sample Sealsi Absent | TLI Project Number 431S9 , | Book l*F
jj Chain of Custody ; Present Container...! Intact j Client i ERG02 - Eastern Research Group | jK^
jj Sample Tags s Absent j j 182 f
|| Sample Tag Numbers: Not Listed on Chain of Custody | 1 1 xV*\ j II
SMO Forma : N/A | Date Received j 09/09/97 j By // /WjL^ „ - / j Page j|
ii 1 1 .—m mrns)' i n
|| Ice Chest/Box NO COOLANT | Carrier and Number | JIM MC C I 30 0
I)TLI Number Client Sample ID , Matrix) To LAB | To STORAGE) To LAB | To STORAGE| To LAB | To STORAGE| To LAB | To STORAGE| DISPOSED ||
jjmR/HsCPM. Client COC ID » Location j Date/Inlt j Date/Inlt j Date/Inlt j Date/Inlt j Date/Inlt j Date/Inlt j Date/Inlt j Date/Inlt j Date/Init jj
II 1 1 1 1 1 1 1 1 1 II
||l82-30-llF YCP-99 Hg KMn041 | I I I I I I I II
j| YCP-99 METALS LAB j i • " I I i I I I "I II
II 1 1 1 \ 1 1 I 1 1 II
||182~30-11Q YCP-100 Hg HC1| | II I I I I I II
jj YCP-100 METALS LAB j j j j j j j j j jj
|| 1 1 1 1 , 1 1 1 1 1|
|| 162-30 - 12A YCP-101 BEAKER) I I I I I I I I II
jj YCP-101 METALS LAB | j | 1-1 I j j I li
jjl82-30-12B YCP-102 PR| j j j j j j j j jj
jj YCP-102 METALS LAB j j j I I I I I I * jj
|| 1 1 1 ! 1 1 1 1 1 1 1|
|| 182-30- 12C YCP-102 FILTER) I I I 1 I I I I II
jj YCP-103 METALS LAB i I I j I I I I | jj
I! 1 1 1 1 , , , 1 1|
||l82-30-12D YCP-104 1Q403/1I202) I I I I I I I I II
|j YCP-104 METALS LAB j j j j j j j j j ||
|| 1 , , , , , , , , ,|
|| 182-30-12E YCP-10S IMP 4| | | ) j | | | | ||
jj YCP-105 METALS LAB j j j j j j j j j jj
jjl82-30-12F YCP-106 • KMN04 j 111111111
jj YCP-106 METALS LAB j j j j | j *. j j j j
II ¦ : 1 1 1 1 : 1 1 1—1 1 1 II
11182-30-120 YCP-107 Hg HC1) I I 1 I I I I I II
jj YCP-107 METALS LAB j j j j j j j j j jj
|| 1 1 1 J hr 1 1 ) ) 1|
||l82-30-13A YCP-108 BEAKER) I I I I 1 I I I II
jj YCP-108 METALS LAB j j j j j j j j I jj
IH 1 1 1 1 1 1—— 1 1 h II
||!82-30-13B YCP-109 PR I I t f I I I I I tl
jj YCP-109 • METALS LAB I j j j j j j j j j|
|| 1 1 1 ; 1 1 1 1 h H II
||l82-30-13C YCP-110 FILTER| I I I I I I I I II
jj , YCP-110 METALS LAB j j j j j j j j * j j|
|| : ? 1 1 1 1 1 1 ) 1 1 II
||l82-30-13D YCP-111 HN03/H2O2| | | | I I I I' I ¦ II
jj YCP-111 METALS LAB j j j j j j j j j li
II * 1 1 1 1 1 1 H 1 1 II
||l82-30-13E YCP-112 IMP 4) i I I ) t I I I II
|j YCP-112 METALS LAB j j j j I I i I i II
jl .... , ¦ »i ¦!.. I , » i i i i i i ij
jj Receiving Remarks t YCP-21, YCP-27.YCP-33, YCP-44 , YCP-S9 were mlsalng from shipment .Also a YCP-169 ||
jj filter arrived But la not listed on C.O.C. jj
II II
|| -Archive Remarks: ||
i; , . ¦¦ , >i . ¦¦ ¦ Form Revised 05/27/1997 -- Page 6 OF 8- ¦ ¦ ¦¦ ¦ > 'I
-------
IMP4 j
182-30-HD
YCP-162
YCP-162
METALS LAB
KMH04
METALS LAB
IICL
JB2-30-14F
MBTftliS wsn
182-3Q-14Q
YCP-165
YCP-165
HETALS LAB
||lB2-30-15A
HPLC
METALS LAB
DI H20
182-30-15B
YCP-170
YCP-170
• HETALS LAB
1ATERj
182-30-15C
METALS LAB
FILTER)
182-3Q-1SA
FILTER)
1II82-30-16B
METALS LAB
|| Receiving Remarks: YCP-21, YCP-27, YCP-33, YCP-44 ,YCP-59 were missing from shipment .Also a YCP-169
filter arrived But is not listed on C.O.C.
" Archive Remarks:
¦Form Revised 05/27/1997 -- Page 7 OF
jj . YCP-171 METALS LAB j j j j | | j 1*1 1
|| 1 1 1 1 1 1 , 1 1 1
||182-3Q-1$A YCP-178 FILTER) I I I I I I I* I I
H YCP-178 HETALS LAB j j j j j j j j j |
II 1 1 1_ 1 1 1 _] 1 1 g
jjl82-3Q-16B YCP-179 FILTER) 111111111
|j YCP-179 METALS LAB 11111111)8
i; —1 ' 1 1 1 ' — ¦ ii
II Receiving Remarks: YCP-21, YCP-27, YCP-33, YCP-44 ,YCP-59 were missing from shipment .Also a YCP-169 |
|| filter arrived But is not listed on C.O.C. J
I! II
|' Archive Remarks: ||
H ii i j ¦ i ¦¦¦ Form Revised 05/27/1997 -- Page 7 OF 8m -i m ¦ J
-------
Receiving Remarks: YCP-21,YCP-27,YCP-33,YCP-44 ,YCP-59 vera missing from shipment.Also a YCP-169
filter arrived But is not listed on C.O.C.
I!
' Archive Remarks:
¦Form Revised 05/27/1997 -- Page 8 OF
j; * 1 ¦ * 1 11 11 3
II Receiving Remarks: YCP-21, YCP-27, YCP-33, YCP-44 ,YCP-59 vera missing from shipment .Also a YCP-169 |
jj filter arrived But is not listed on C.O.C. - |j
ii g
||' Archive Remarks: H
I1 ,,» i „ ¦' i i "Form Revised 05/27/1997 -- Page 8 OF 8^- —»¦¦¦ i . ¦....... — ...1
-------
e@!PY («•«• Y/Mt
Book
LOO IN RECORD/CHAIN OF CUSTODY"
¦TRIANGLE LABORATORIES, INC.
TLI Project Number 43187
Clienti ERGO2 - Eastern Research Group
Sample Seals: Absent
Container...! Intact
Custody Seal
Chain of Custody > Absent
Sample Tags
Sample Tag Numbers: Not Listed on Chain of Custody
SMO Forms : N/A
: Absent
: Absent
09/10/97
Date Received
58
Carrier and Number I JIM MC
Styro Cooler
Temp 22.0 C
NO COOLANT
DISPOSED H
Date/Init |j
To STORAGE
Date/Init
||TLI Number Client Sample ID
||mR/H:CPM Client COC ID.
To LAB
Date/Init
Matrix
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
To LAB
Date/Init
To STORAGE
Date/Init
Location
HATER
182-56-1
YCP-21
REFER TO TLI PROJECT43159*
C02
HATER
182-58-2
YCP-27
REFER TO TLI PROJECT43159*
C02
182-58-3
YCP-3 3
REFER TO Tlil PROJECT43159*
HATER
C02
Receiving Remarks: NO COOLANT PRESENT HITH SAMPLES THUS THE HIGH TEMPERATURE. SAMPLES ARE PART OF TLI PROJECT S43159.
Archive Remarks:
It
¦Form Revised 05/27/1997
Page 1 OF 1'
|| j' j j | j j j i i
II Receiving Remarks: NO COOLANT PRESENT HITH SAMPLES THUS THE HIGH TEMPERATURE. SAMPLES ARE PART OF TLI PROJECT 043159. j|
H II
II . II
|| Archive Remarks: , ||
P ¦ ¦ ¦ Form Revised 05/27/1997 -- Page 1 OF 1 'I ¦
-------
tojecl II *j2> 15^ P)
:"eni: Eas fam 'Resen^eM Qroup Triangle Laboratories of RTP
'ole/lnt.: q|lalp
added ppb
FH & OH Serial dilution performed
< ml lo ml FV ul Sc
-------
'rojecl //_
^llonl;
*13151 8
ICP
1 C5
Anotyles CT5
GI:AA II. AA CVAA
)ate/Inh
Triangle Laboratories of RTD
(919) 544-5729
silent Run/? YCsP " ll^j
•i
CONT II
©
CONT II
CQNMI
Filler .1
/pe: G or Q
Ace lone
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label J
label
CONT J/
CONT II.
11 Ig Implngets
I-IN03
Back Half
Rinse
Impinge r
1N03
CONT H
CONT «
KMNCM
MCI
lateel
label
Volume
Volume.
Volume
.Desslcale lo
^dryness and
' redlssolve In
IjOml con I-IN03
Inl
Dale
Reduce
volume
lo 20 ml on
holplale
Inl
rowave dig';
h conc. HF
conc. IIN03
re
Dale
:|
Microwave dig Inl
with'conc. HF
and conc. IINQ3 .Dale
I
For Melals
label.
For Hg
I
label
Volume
Volume,
Combine cllgeslales
label
Fronl Half Dlgeslale
Jl
label
I label i
abel
Volume ml
Allquol A
Allquol 13
Inl
Volume . ml
1 Allauol A 1
i Allquol B ;
i Inl •
Volume ml
Allauol A
V
Allauol B *
Inl
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• Dale i
Dale
Add
=5?
Reduce Volume lnl._
lo 20 ml. on
Holplale Dale,
(Duplicate Analysis of Each
Sample
(I
1
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ul S£
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label
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and 1-1202
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i~~
label
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i label
Inl
Volume.
Dale,
! Volume.
Dale
Add
600 ul Sc
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Allquol A:.
Allquol B:_
Allquol A:
Aliquot D:.
i /t Melal
'
belj©!^ In! A
jlume 1 M Dale
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& BM Posl dla. sok.
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ii label if*-*0»M |n|
! i
jj! Volume (0^ ml Dale ffafll?
| Allquol A: ^ ml
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100 mis
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I final spk conc. Dale
i added ppb
I label
• Volume.
Inl
Dale
Fl| & 0H Seilal dllullon performed
< ml lo ml FV i ..... ul Sc
-------
Project li
Client:
1,
b\ff\ 5
ICP
Analyles
GFAA II. A A CVAA
O
~ate/lnt.:.
Triangle Laboratories of RTD
(919) 544-5729
Client Runil VtP-ISO
w
com ii
CD
CQNT II
CONTH
CONf II
Tiller 4
ype: G or Q
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label
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GONTII,
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IIN03
KMNCM
MCI
label.
label
Volume
Volume
Volume
.Desslcale lo
'dryness ancl
' recJIssolve In
I;Oml con I-IN03
Inl
Dale
Reduce
volume
lo 20 ml on
holplole
Inl
Dale
rowave dig',
hcone, HF•
conc. IINQ3
Microwave dig
Inl
wllh'conc. HF
and conc. I-IN03
.Dale
i
For Melals
I
label
Volume
For l-lg
I
label
Volume
Combine dlgeslales
label
Fronl l-lalf Dlgeslale
_1
t
label
i label •
: iabel
Volume ml
Allquol A
i
Allquol 0
Inl
= Volume . ml i
i Allquol A :
; Allauo} D !
i Inl
¦ Volume ml
1 Allquof A
1 Allquol D '
S Inl
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lDale:" i
; Dale
(Duplicate Analysis of Each
Reduce Volume Int..
lo 20 ml. on
1-lotplalo Dale.
Sample
('
1
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I
/l Motol
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Volume 16b Ml
i
l-lolplalo dig 'nl.
will- MN03
and 11202 Dale.
label.
Inl
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500 ul Sc
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Volume
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s mL
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/Kir* «r^lt/n 'I'1
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label
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i
i Volume_
Dale
(Orvo nr»tl
-
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added
HI & UH Serial dllulion performed
¦ ml lo ml FV +. ul Sc
-------
3rojecl II l)3 ihty 0
Cllenh .
Date/lnt.:
Analylns
ICP • GIAA FI.AA CVAA
Triangle Laboratories of RTP
(919)544-5729
lent Runtf ^fC-P '/%!
conf ii
CD
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Volume
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±
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CONT II
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-------
Project l/_
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L
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GI:AA II.AA CVAA
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(919)544-5729
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-------
PAGE Lfl
INORGANICS SPIKE LOG
DATE
PROJECT #
SAMPLE 10s
ANALYTE
ORIGINAL
STANDARD
#
ORIGINAL
STANDARD
CONC.
(PPM)
SPIKE
SAMPLE
ftiL)
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INITIALS
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qa\forms\inospke.log (08/22/96)
43
-------
Hi# 43154-B
* SEE SPIKE LOG
Spiking Standard Preparation
SPIKING
from Spiking Standard
EXP dote
3emew
Standard
Orig. Std.
SpiKe(uL)
cone
fSpiWuL)
cone
combined
10
(ppm)
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(ppm)
FVddOOmO
(ppb>
total
2M/98
*9
2-115-4
100
5000
5
I 1000
so
mm
%
3-010-10
100
5000
S
I 1000
50
2/1 /9S
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2-115-4
100
5000
5
1000
50
9/1/98
M
3-010-7
10000
950
95
1000
950
1000
2/1/98
3
2-11S-4
100
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1000
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2/1/98
3a
2-115-4
100
5000
s
1000
50
9/1/98
3a
3-010-10
100
5000
s
1000
50
9/1/98
¦•A
3-010-10
100
5000
5
1000
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9/1/98
3-012-7
10000
950
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9S0
1000
9/1/98
•i
3410-10
100
9000
5
1000
50
9/1/98
20
3-010-10
100
SOOO
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1000 -
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9/1/98
>
3-010-10
100
5000-•
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9/1/98
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9/1/98
3-010-10
100
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9/1/98
3-012-6
10000
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2/1/98
<
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9/1/98
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150
1000
1500
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9/1/98
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1 100
5000
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8/1/98
*9
3-010-8
10000
950
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1000
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9/1/98
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100
5000
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1000
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9/1/98
Mo
3-010-10
100
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5
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2/1/98
Ms
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100
5000
5
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8/1/98
Ma
3-010-9
10000
1950
195
1000
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5
1000
so
9/1/98
n
3-010-10
100
SOOO
5
1000
50
9/1/98
3-010-10
100
5000
5
1000
50
9/1/98
s>
3-010-10
100
5000
5
1000
50
8/1/98
y%
34104
1000
1500
15
1000
ISO
200
1000uc of tne SpiKing Standard gives me listed sonc. of Sie above dements.
Spiking Standard 3-013-3
EXP; 11/26197
7
Postdigestien-
"Spike seperately
Sement
Orig Std
Spike(uL)
cone
(ppm)
FvddOOm
(POM
Au
1000
140
1400
C»
1000
30
300
u
1000
70
700
p
1000
100
1000
Pd
1000
180
1800
Pt
1000
300
3000
S
1000
350
3500
Si
10000
350
35000
Sn
1000
20
200
Sr
1000
S
50
/
I
44
-------
PAGE 1 OF 1
Released by:
Accepted by:
TRIANGLE LABORATORIES, INC.
Transfer Chain-of-Custody Form
Project 43159-B
Transfer From: IWLM To: IA I
Initials.. Date.......
S(l6 J? / jZ/31
Time...
J3_:3Q fH
13 3o
MILES.ID.
......
. TLI_No
Cust.Id
43159-B
-000
TLI Blank
TLI Method Blank
43159-B
-001
182-30-16A
YCP-178
43159-B
-002
182-30-16B
YCP-179
43159-B
-003
182-30-16C
YCP-180
43159-B
-004
182-30-16D
YCP-181
43159-B
-005
182-30-161
YCP-182
43159-B
-006
LCS
LAB CONTROL SPIKE
;ional comments or instructions:
-XfrCOC {Rev 11/01/94)--+
45
-------
'ir;'.
3-Sr%l|i ;.
-- t~"C~ 92P''Z-
tsA
* " /.^,<
0^
lA\57
?5 91
lZA_
L\l\*2.
\lk^lhlP^5
£>lo-Ai:
jSKso-ic fta<
idllSfuL
V2.-J0- I4A
V
r
¦Jr-
T
J
\Js
Jk
HS sly
s^SD
.4-0)3'4
{'
>(*H
~r
Co**-
iP
\ 1 •>*& 1^ ^
vPv l
-------
* SEE SPIKE LOG
Spiking Standard Preparation
SPIKING
from Spiking Standard
EXP date
Element
Standard
Orig. Std.
SciKefuLS
cone
Bpike(uL)
cone
combined
10
fppm)
FvotnOC.TL)
ippm)
FVat(lOOml)
(PPb)
total
2/1/98
*9
2-115-4
100
sooo
5
1000
50
9/1/98
3-010-10
100
5000
5
j 1000
50
2/1/98
2-115-4
100
sooo
5
1000
50
9/1/98
U
3-010-7
10000
950
95
1000
950
1000
2/1/98
3
2-115-4
100
5000
5
1000
50
2/1/98
3a
2-115-4
100
5000
5
1000
SO
9/1/98
ie
3-010-10
100
5000
5
1000
50
9/1/98
2a
3-010-10
100
5000
5
I 1000
50
9/1/98
3a
3-012-7
10000
950
95
I 1000
950
1000
9/1/98
Dd
3*010-10
100
5000
5
| 1000
SO
9/1/98
:o
3-010-10
100
5000
5
! 1000
SO
9/1/98
>
3-010-10
100
5000
5
1000
50
9/1/98
3u
3-010-10
100
SOOO
5
1000
50
9/1/98
:e
3-010-10
100
SOOO
5
1000
50
9/1/98
-8
3-012-6
10000
9S0
95
1000
950
1000
2/1/98
<
2-115-4
1000
SOOO
SO
1000
500
9/1/98
<
3-012-5
10000
1500
150
1000
1500
2000
9/1/98
Wg
3-010-10
100
5000
s
1000
50
8/1/98
ug
3-010-8
10000
950
95 |
1000
950
1000
9/1/98
Wtri
3-010-10
100
SOOO
5
1000
50
9/1/98
Wo
3-010-10
100
5000
5
1000
50
2/1/98
Ma
2-115-4
100
5000
S
1000
50
B/1/98
Ma
3-010-9
10000
1950
195 I
1000
1950
2000
3/1/98
Mi
3-010-10
100
5000
5 I
1000
so
J/1/98
sb
3-010-10
100
SOOO
5
1000
50
3/1/98
3b
3-010-10
100
SOOO
5
1000
50
J/1/98
>e
3-010-10
100
5000
5
1000
50
1/1/98
h
3-010-10
100
5000
S
100Q
50
1/1/98
n
3-010-10
100
5000
S
1000
50
1/1/98
V
3-010-10
100
5000
5
1000
SO
1/1/98
Zn
3-010-10
100
5000
5
1000
so
1/1/98
In
3-010-6
1000
1500
15 1
1000
150
200
1OOCut. or me SptKtrsg Standard gives me listed cone, of tne acove elements.
"Spike seperatety
9em«nt Orig Std Spi^efuL) cone
ippm) Fvol(lOOm (ppb)
Au
1000
140
1400
Ca
1000
30
300
Li
1000
70
700
P
1000
100
1000
Pd
1000
160
1600
Pt
1000
300
3000
S
1000
350
3500
Si
10000
350
35000
Sn
1000
20
200
Sr
1000
5
50
Spiking Standard 3-013-4
EXP: 11126/97
Spiked by:
PreageMon-
PostCigetuon- cW^(T)
47
-------
Analysis ReDort
t Sanoie Naie
Summary
File
Sun 10-C3-2/ 06:55:51 Pft page
Method Date Time OciD Type ttode
1 STDl'SL-ANK—
100397
"TIOT6tt
"t0/03/??
-M-
—M
2 STD3
100397
TRIANGL2
10/03/97
23:07
X
/ IR
5 ST03
100397
TRIANGL2
10/03/97
23:12
DKH
CONC
4 CHECK LO
100397
TRIANGL2
10/03/97
23:16
dk/
0
CONC
5 ICV/CCV
100397
IRIANGL2
10/03/97
23:21,
o
CONC
6 1C8/CCB
100397
TR1ANGL2
10/03/97
23^6
DKH
&
CONC
7 ICB/CCB
100397
TRIANGL2
10/03/97
,23:51
DKH
Q
CONC
8 ICSAB
100397
TRIANGL2
10/03/9/
23:56
DKH
Q
CONC
9 43332A MB
100397
TRIANGL2
10/04/97
00:13
DKH
S
CONC
10 43332A ICS
100397
TRIANGL2
10/jW/97
00:29
DXH
S
CONC
11 184-5-2
100397
TRIANGL2
10704/97
00:44
DKH
S
CONC
12 184-5-2 0
100397
TRIAN6L2/
40/04/97
00:49
DKH
S
CONC
13 184-5-2 NS
100397
TRIANGi?
10/04/97
00:54
DKH
S
CONC
14 184-5-2 USD
100397
TRIAXGL2
10/04/97
00:58
DKH
S
CONC
15 184-5-2 PDS
100397
TftWNGl2
10/04/97
01:03
DKH
S
CONC
16 184-5-2 L
100397
/TRIANGL2
10/04/97
01:08
DKH
S
CONC
17 CHECK 9972
100397/
TRIANGL2
10/04/97
01:13
DKH
S
CONC
18 ICV/CCV
1003*?
TRIANGL2
10/04/97
01:18
DKH
0
CONC
19 ICB/CCB
100397
TRIAN6L2
10/04/97
01:23
DKH
8
CONC
20 ICSAB
.mm
TRIANGL2
10/04/97
01:28
DKH
0
CONC
21 43182 N8
/mm
TRIANGL2
10/04/97
01:39
DKH
S
CONC
22 43182 ICS
/ 100397
TRIANGL2
10/04/97
01:44
DXH
S
CONC
23 182-53-1,3 /
100397
TRIANGL2
10/04/97
01:48
DKH
S
CONC
24 182-53-1,3 PCf
100397
TRIANGL2
10/04/97
01:53
DXH
S
CONC
25 182-53-1,3 /
100397
TRIANGL2
10/04/97
01:58
DKH
s
CONC
26 182-53-2.5/
100397
TRIANGL2
10/04/97
02:03
DKH
s
CONC
27 182-53-2/5 DA
100397
TRIANGL2
10/04/97
02:07
DKH
s
CONC
28 ICV/Cc/
100397
TRIANGL2
10/04/97
02:14
DKH
8
CONC
29 ICV/pCT
100397
TRIAHGL2
10/04/97
02:19
DKH
0
CONC
30 IttfcCB
100397
TRIANGL2
10/04/97
02:25
DXH
8
CONC
31 K8/CCB
100397
TRIANG12
10/04/97
02:30
DXH
Q
CONC
32%SffT~
100397
ikiHNbU WjVifTi
u2:So
liKH
8~
—ee#v
33 STD1-BLAHK
100397
TRIANGL2 10/03/97
19:12
X
IR
34 STD3
100397
TRIANGL2 10/03/97
19:16
X
IR
35 STD3
100397
TRIANG12 10/03/97
19:21 0KH
a
CONC
36 CHECK LO
100397
IRIANGL2 10/03/97
19:27 DKH
8
CONC
37 ICV/CCV
100397
TRIANGL2 10/03/97
19:31 DKH
8
CONC
\AA7Q7
10 • 7i.
MH
(1
rnwc
5U itofvvli
iv/vO/ 7 J
* VUIIV
39 ICB/CCB
100397
TRIANG12
10/03/97
19:42
DXH
0
CONC
40 ICSAB
100397
TRIANGL2
10/03/97
19:47
DXH
0
CONC
41 43159A H8
100397
TRIANGL2
10/03/97
20:03
DKH
s
CONC
42 43159A ICS
100397
TRIAHGL2
10/03/97
20:07
DXH
s
CONC
43 182-30-1AB
100397
TRIANGL2
10/03/97
20:12
DXH
s
CONC
44 182-30-1A8 POS
100397
TRIANGL2
10/03/97
20:17
DXH
s
CONC
45 182-30-1AB I
100397
TRIANGL2
10/03/97
20:21
DKH
s
CONC
46 182-30-2A8
100397
TRIANGL2
10/03/97
20:26
DKH
s
CONC
47 182-30-2AB OA
100397
TRIANGL2
10/03/97
20:31
DKH
s
CONC
48 182-30-3A8
100397
TRIAHGL2
10/03/97
20:35
DKH
s
CONC
49 182-30-4A8
100397
TRIANGL2
10/03/97
20:40
DKH
s
CONC
50 182-30-5A8
100397
TRIAHGL2
10/03/97
20:45
DXH
s
CONC
51 ICV/CCV
100397
TRIANGL2
10/03/97
21:24
DXH
8
CONC
52 IC8/CC8
100397
TRIANSL2
10/03/97
21:31
DXH
8
CONC
53 182-30-6A8
100397
TRIANG12
10/03/97
21:39
DKH
s
CONC
o: =<• ^
vytM
10'
v
-------
lysis Report Summary Sun 10-05-97 06:55:31 Pet Daae 2
Sample Nans File Method Date Tiae OpID Tvpa Mode
182-30-7A8
182-50-8A8
182-30-9A8
182-30-11AB
182-33-1208
182-30-13A8
1S2-30-14AB
182-30-158
182-30-15C
ICV/CCV
-mfm-—
ICB/CCB
182-30-1C
182-30-1C POS
182-30-1C L
182-30-2C
182-30-2C OA
182-30-3C
182-58-1
182-58-2
182-58-3
182-30-78
ICV/CCV
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100391.
TRIANG12
TRIANG12
TRIANGL2
TRIANGL2
TRIANG12
TRIAN612
TRIANGL2
TRIANGL2
TRIAH6L2
TRIANGL2
-TBIMKI ?
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
10/03/97
4zfwfrr
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
100397
TRIANGL2 10/03/97
TRIANGL2 10/03/97
TRIANGL2 10/03/97
TRIAK6L2 10/03/97
TRIANGL2 10/03/97
TRIAHGL2 10/03/97
TRIAN6L2 10/03/97
TRIAHGL2 10/03/97
TRIAHGL2 10/03/97
TRIAHGL2 10/03/97
TR1ANGL2 10/03/97
TRIAHGL2 10/03/97
21:44 0KH
21:49 0KH
21:53 OKH
21:58 DKH
22;03 OKH
22:07 OKH
22:12 OKH
22:17 OKH
22:21 DKH
22:26 DKH
72:32 DKF
22:48 DKH
22:54 DKH
22:59 OKH
23:03 OKH
23:08 DKK
23:13 DKH
23:17 OKH
23:22 OKH
23:27 OKH
23:31 OKH
23:36 DKH
23:41 DKH
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
IPC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
CONC
¦mm—
ICB/CCB
.—100397
100397
¦ iniANGLg
TRIANGL2
10/03/97 -
10/03/97
-23TW
23:57
W
DXH
0
cone
CONC
182-30-8CA
100397
TRIANGL2
10/04/97
00:04
DKH
s
CONC
182-30-908
100397
TRIANGL2
10/04/97
00:09
DKH
s
CONC
182-30-UD
100397
TRIANGL2
10/04/97
00:13
OKH
s
CONC
182-30-120
100397
TRIAHGL2
10/04/97
00:18
DKH
s
CONC
182-30-1380
100397
TRIANGL2
10/04/97
00:23
DKH
s
CONC
182-30-14BC
100397
TRIANG12
10/04/97
00:27
DKK
s
CONC
ICV/CCV
100397
TRIANGL2
10/04/97
00:44
OKH
0
CONC
IC8/CC8
100397
TRIANGL2
10/04/97
00:49
DKH
0
CONC
ICSAB
100397
TRIANGL2
10/04/97
00:55
OKH
Q
CONC
431598 118
100397
TRIANGL2
10/04/97
01:09
OKH
S
CONC
431598 ICS
100397
TRIANGL2
10/04/97
01:14
OKH
s
CONC
182-30-16A
100397
TRIANGL2
10/04/97
01:19
OKH
s
CONC
182-30-16A POS
100397
TRIANGL2
10/04/97
01:23
DKH
s
CONC
182-30-16A L
100397
TRIANGL2
10/04/97
01:28
OKH
s
CONC
182-30-168
100397
TRIANGL2
10/04/97
01:33
DKH
s
CONC
182-30-168 OA
100397
TRIANG12
10/04/97
01:37
OKH
s
CONC
182-30-16C
100397
TRIANGL2
10/04/97
01:42
DKH
s
CONC
182-30-160
100397
TRIANGL2
10/04/97
01:47
DKH
s
CONC
182-30-16E
100397
TRIANGL2
10/04/97
01:51
OKH
s
CONC
•t rv (rnt
? AA7T7
tutau^in
i A /fli h?
rwu
_Q
pflHf -
i \*v i uu'r
lUUi> / /
ui. jit
icv/ccv—-—
iilv&il
I KiHnblZ 1U/U4/7/
8
uum;
ICV/CCV
100397
TRIANGL2 10/04/97
02:34 OKH
a
CONC
ICB/CCB
100397
TRIANGL2 10/04/97
02:44 OKH
0
CONC
ICSAB
100397
TRIANGL2 10/04/97
03:00 OKH
Q
CONC
49
-------
PAGE
MERCURY SPIKE LOG
DATE
PROJECT#
SAMPLE IDs
ORIGINAL
SFIKE
CONG. (Hg)
STANDARD #
WORKING
STANDARD
PREPARED
FROM
SPIKE
AMOUNT
(mL)
SPIKE
SAMPLE
(PP9)
INITIALS
WITNESS
4SIT?
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f)
'5"
P0£
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3^01 b-~¥
5"
S
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S'
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le hs
iBrf-ff- -?e M-U
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r
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43oZ7 ££i6
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r\/2^
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(
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i
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i/
'
50
qa\forms\hgspke.log (08/22/96)
-------
AiitoSantier Report Table: HA443 Sun 10-05-9? 06:58:23 PH oaoe I
Table Name: HA448 ftutosanolsr Type: TVPE TJA
Saiioie Positions: 146/192 fiC Positions: 13/19 ? Sets: 2
Rinse Station location is rack -l. dds. -I.
— Racks —
Rack i Type Usage iPos left Analyses/Pos
1
flux, |L) Rack
STD/OC/'BLAM
13
10
2
Saiple (16m)
Saioles
2
1
3
Sample (16m)
Saiples
48
1
4
Saiole (16m)
Saioles
48
1
5
Saiple (16m)
Sanies
48
1
- Samoie Sets
Sett Type
Prepare? Description
Method IPos Rack! StartPos
43 59A
431598
1 Noraal
2 Normal
— Preparation Info —
Setl Uptake UptakeS2 final
No Sasples Prepared.
Rack il
TRIANGL2 36
TRIANGL2 10
Oil.factor
1
37
Pos Row
Col
Saaple Naae
Set I
itlsed
Type
1 1
1
ST03
-NA-
2
Standard !-<®QS P
2 1
2
STD1-BLANK
-NA-
1
Standard
3 1
3
ICSAB
-NA-
3
QC Standard \~Ccrl ?
4 1
4
CHECK 10
-NA-
1
QC Standard
5 1
5
ICV/CCV
-NA-
6
QC Standard V-C.o-6v ^
6 1
6
IC8/CC8
-NA-
6
QC Standard
(7...19
Not
Used)
Rack 12
Pos Row
Col
Saiple Naae
Set i
iUsed
Type
1 1
1
43159A H8
1
-Nfi-
Saiioie
2 1
a
L
43159A ICS
1
-NA-
Saaple
3 1
3
182-30-1A8
1
-NA-
Saiple
4 1
4
182-30-1AB POS
1
-NA-
Sanple
5 1
5
182-30-1A8 t
1
-NA-
Saaple
6 1
6
182-30-2A8
1
-Hft-
Saiple
7 1
7
182-30-2A8 OA
1
-NA-
Sasple
8 1
8
182-30-3A8
1
-NA-
Saaple
9 1
9
182-30-4A8
1
-NA-
Sasple
10 1
10
182-30-5A8
1
-NA-
Saaple
11 1
11
182-30-6A8
1
-NA-
Sa#ple
12 1
12
182-30-7A8
1
-NA-
Saiple
13 2
1
182-30-8A8
1
-NA-
Saaple
14 2
2
182-30-9A8
1
-NA-
Saaple
ffM
i
51
-------
Sun 10-05-97 06:58:28 PH page 2
¦
i
1
B
2
ml:
I
i
i
i
I
I
I;
I
I
f
R.
l
I
s Row
»I7
18
|19
20
21
¦22
F
24
.25
26
n
28
129
30
31
132
33
34
35
|36
»37
38
139
40
41
142
43
44
45
[46
147,,
ack #3
Rack #4
1...48 Hot Used)
Col
Samcie Na»e
Set i
iUsed
Type
3
182-iO-llAB
1
-NA-
Samole
4
1S2-50-12A8
1
-NA-
Sample
5
182-30-13A8
1
-NA-
SatiDle
6
182-30-14A8
1
-NA-
Saaole
T
1
182-30-156
1
-NA-
Sample
8
182-30-15C
1
-NA-
Sample
9
182-30-LC
1
-NA-
Sanple
10
182-30-1C PCS
1
-NA-
Sample
11
182-30-1C L
1
-HA-
Sample
12
182-30-2C
1
-HA-
Saaole
1
182-30-2C DA
1
-HA-
Sample
2
182-30-3C
1
-NA-
Sample
3
182-58-1
1
-Nft-
Sample
4
182-58-2
1
-NA-
Sample
5
182-58-3
1
-HA-
Sample
6
182-30-78
1
-NA-
Sample
7
182-30-8CA
1
-NA-
Sample
8
182-30-9DB
1
-NA-
Sasple
9
182-30-110
1
-NA-
Sasple
10
182-30-12D
1
-NA-
Sample
11
182-30-1380
1
-NA-
Sanple
12
182-30-148C
1
-NA-
Saiple
1
431595 N8
2
-NA-
Saaple
2
431598 ICS
2
-NA-
Sasple
3
182-30-16A
2
-NA-
Sample
4
1B2-30-16A P0S
2
-NA-
Sample
5
182-30-16A L
2
-HA-
Sample
6
182-30-168
2
-NA-
Sample
7
182-30-168 OA
2
-NA-
Sample
8
182-30-16C
2
-NA-
Sample
9
182-30-160
2
-NA-
Sanple
10
182-30-16 E
2
-HA-
Saaple
Not Used)
Col
Sample Name
Set $
#(Jsed
Type
Not Used)
Col
Saiple Nane
Set #
IUsed
Type
-------
Stanaardiration Rot.
Fri iO-03-^7 0/;16:4i PM oaae 1
Hstnoa:
TRIANGL2
Standard: STOl-
SlANK
ilea
Ag32S0
A13082
Asl89Q
B_249fc
634934
8e3130
Ca3179
Avgs
.0000
.0029
-.0004
.0751
.0006
.0002
.0005
SDev
.0001
.0000
.0001
.0015
.0000
.0000
.0000
%ftSD
273.8
.7839
18.23
2.007
.2751
1.797
3.527
*1
-.0000
.0029
-.0003
.0748
.0006
.0002
.0005
S2
-.0000
.0028
-.0004
.0767
.0006
.0002
.0005
13
.0001
.0028
-.0004
.0737
.0006
.0002
.0005
ElSB
Cd2265
Ce4186
C02286
Cr2677
CuJ247
Fe2714
K.7664
Avge
-.0001
-.0000
-.0002
-.0001
.0028
.0001
3.937
SDev
.0001
.0001
.0000
.0000
.0000
.0000
.030
SRSO
79.87
260.4
26.15
21.81
1.255
52.99
.7726
11
-.0001
.0000
-.0002
-.0002
.0029
.0000
3.904
12
-.0001
-.0001
-.0002
-.0001
.0028
.0001
3.944
13
-.0002
.0000
-.0001
-.0001
.0028
.0001
3.964
Eles
U6707
Hg2790
Hn2576
NO2020
Na3302
Ni2316
P.2149
Avge
.0729
.0001
.0000
.0000
.0035
-.0022
-.0010
SDev
.0006
,0000
.0000
.0000
.0021
.0002
.0000
%RSD
.7489
52.54
20.63
141.9
59.46
8.802
2.941
51
.0723
.0000
.0000
.0000
.0035
-.0022
-.0010
12
.0730
.0001
.0000
.0001
.0015
-.0023
-.0011
13
.0733
.0001
.0000
.0000
.0057
-.0019
-.0011
Elen
2203-1
2203-2
Sb2068
1960-1
1960-2
Snl899
Sr4215
ftVQS
.0011
.0001
.0005
-.0063
.0025
-.0006
.0003
SDev
.0001
.0001
.0001
.0010
.0001
.0001
.0000
«S0
10.19
53.72
26.48
15.31
1.846
8.818
3.762
»1
.0011
.0000
.0005
-.0073
.0025
-.0007
.0003
12
.0012
.0001
.0004
-.0060
.0026
-.0007
.0003
*3
.0010
,0001
.0007
-.0055
.0025
-.0006
.0003
Elen
Ti3349
T11908
V.2924
Zn2062
Si2881
Avge
.0001
-.0005
-.0005
-.0000
.0659
SDev
.0001
.0000
.0000
.0000
.0086
*RSD
81.06
6.313
3.126
76.41
13.13
11
.0000
-.0005
-.0005
-.0000
.0626
12
.0001
-.0005
-.0005
-.0000
.0757
13
.0002
-.0005
-.0005
-.0000
.0594
-------
^ndardimion Rot. Fri 10-03-97 07:16:41 Prt oaae 2
¦tStd 1 2 3 4 5 6 7
™de founts Time NOTUSED HOIUSED NOTUSED NOTUSED NOTUSED
Oea Y
Wvlen 371.030
Hoe 257206 15000
SDev 605.2008 .0000000 -
|SD .2352981 .0000000 -
il 256522 15000
*257424 15000
257672 15000
-------
Standardization Rot.
fri 10-03-97 07:21:23 PN
cage 1
Method: TRIAN6L2 Standard: ST03
El en
Aa3280
A13082
AS1890
B.2496
Ba4934
683130
Ca3179
flvas
.4165
.0190
.0538
.2380
.3054
.2657
.0232
SDev
.0016
.0001
.0001
.0025
.0003
.0002
.0000
MSD
.3769
.7924
.2500
1.066
.0883
.0756
.0409
il
.4132
.0191
.0539
.2404
.3057
.2655
.0232
12
.4161
.0189
.0536
.2384
.3054
.2659
.0232
13
.4152
.0188
.0558
.2353
.3052
.2658
.0232
Els#
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
FS2714
K.7664
Avge
.9615
.1174
.1082
.1525
.1890
.0043
23,97
SDev
.0014
.0002
.0001
.0000
.0007
.0000
.07
%RSD
.1473
.1790
.1108
.0111
.3781
.1410
.2721
ii
.9610
.1172
.1082
.1525
.1898
.0043
24.03
12
.9604
.1176
.1081
.1526
.1888
.0043
23.97
13
.9631
.1173
.1083
.1525
.1884
.0044
23.90
Elan
H6707
Ha2790
Hn2576
NO2020
Na3302
Ni2316
P.2149
Awe
16.68
.0210
.1344
.0822
.2387
.3637
.0223
SDev
.05
.0001
.0000
.0001
.0033
.0004
.0001
IRSO
.2788
.2669
.0234
.1471
1.389
.1040
.6789
«1
16.73
.0211
.1344
.0821
.2413
.3633
.0222
12
16.66
.0210
.1344
.0823
.2399
.3641
.0225
<3
16.64
.0210
.1343
.0823
.2350
.3636
.0224
Eleo
2203-1
2203-2
S&2068
1960-1
1960-2
Snl899
Sr4215
Avge
.1888
.0926
.1259
.2829
.1667
.1229
.8782
SOev
.0005
,0005
.0002
.0008
.0002
.0006
.0021
*RS0
.2779
.5302
.1943
.2638
.1450
.4856
.2389
11
.1893
.0922
.1259
.2824
.1666
.1223
.8803
12
.1883
.0926
.1256
.2838
.1665
.1232
.8781
13
.1889
.0931
.1261
.2825
.1670
.1234
.8761
Elen
H3349
T11908
VJ924
Zn2062
SI2881
Avge
1.166
.0330
.0400
.1025
.5193
SDev
.001
.0005
.0000
.0001
.0032
«SD
.0463
1.413
.0149
.1424
.6075
11
1.166
.0325
.0400
.1023
.5157
12
1.166
.0330
.0400
.1025
.5216
83
1.165
.0334
.0400
.1026
.5207
-------
sndaraizition Rot.
Fri 10-03-97 07:21:23 ?n
I
tStd 12 3 4 5 6
de founts Time HOTUSED HOTUSEO NOTUSEO NQTUSED
ties Y
Ivlen 371.030 --
ge 25&188 15000
SDev 998.1509 .0000000 --
SO .3396161 .0000000 --
I
»1 255041 15000
*256667 15000
256857 15000
cage 2
7
HOTUSEO
-------
Aoaiysis Recort Averages
Sun 10-05-97 06:31:45 Pfl page i
Method: TR1AN612 Saaoie Name: 5TDS Operator: DKH
Run Time: 10/03/97 i~:21 Filename: 100397
Mode: C0NC Type: 0 Corr, Factor: 1.00000
Lab ID.: Oust. SidI. 10.: Oust. 10,: 43159A
Eleis
Knits
Avge
SDev
%RSD
El ens
Units
Avge
SOev
*RSD
Elems
Units
Avge
SOev
IRSD
Eless
Units
Avge
SOev
tRSD
Eleis
Jnits
Avge
SOev
tRSD
ilens
Jnits
wge
sDev
;RS0
Ag3280
pDb
993.3
1.433
.1443
Ca3179
ODD
994.0
4.264
.429
Fe2714
ppb
991.3
2.797
.2821
Na3302
opa
9.982
.1187
1.189
1960-1
ppb
998.0
1.11
.1112
Ti3349
ppb
991.2
1.98
.1997
A13082
ppb
995.1
6.224
.8265
Cd2265
ppb
996.0
5.474
.5497
K_7664
SCR
9.996
.0473
.4735
Ni2316
ppb
994.9
3.388
.3405
1960-2
ppb
995.1
2.618
.2631
T11908
cpb
1004.
9.415
.9377
Asl890
ppb
1003.
4.354
.4342
Ce4186
ppb
998.0
1.085
.1087
L16707
pob
1003.
6.717
.67
P.2149
ppb
992.0
8.847
.8919
Pb2203
ppb
995.3
2.687
.27
V.2924
ppb
993.8
2.758
.2776
B.2496
pob
8941.3
11.38
1.209
Ca2286
ppb
995.2
3.117
.3132
Mg2790
pob
991.8
1.452
.1464
2203-1
ppb
994.3
.3084
.031
Sel96Q
ppb
996.1
1.548
.1554
2n2062
ppb
997.4
7.286
.7305
8a4934
Dob
995.5
.6488
.0652
Cr2677
ppb
993.6
3.595
.3618
Hn2576
ppb
993.3
2.997
.3017
2203-2
ppb
995.8
4.006
.4023
Snl899
ppb
994.0
6.559
.6599
Si2881
ppb
9803.
50.66
.5168
8e3130
ppb
990.9
4.435
.4476
CU3247
ppb
994.0
3.698
.372
HO2020
ppb
996.9
2.934
.2943
Sb2068
ppb
996.6
2.815
.2825
Sr4215
ppb
987.8
.1926
.0195
56
-------
Analysis Report Averages
Sun K-0:-?7 06:31:45 PM cage 51
(Method: TRIANGL2
Run Time: 10/04/97
Mode: CONC
.Lab ID.:
I
E
I
m
§
u..
tv
D
*R
l
Elems
¦Units
(ftvge
SDev
¦IRSO
Elems
.Units
ftvge
SDev
Jlens
Units
^vge
BDev
*RSD
Elems
Jnits
Avge
SOev
feRSO
K
Av
~
IF
f
IW
SD
I
Elans
pnits
ftvge
SDev
&RSD
Eleas
Jin its
Avge
~Dev
Sample Hame:
00:44
Type: 8
Oust, SiddI, ID
ICV7CCV
filename: 1003^7
Corr. Factor:
Cyst,
Operator: OKH
1.00000
ID.: 43159ft
opb
508.2
.3706
.0729
A13082
pcb
521.0
5.74
1.102
Asl890
ppb
518.0
1.718
.3316
8.2496
ppb
589.2
5.892
1
8a493i
DDD
496.1
1.065
.2146
Be3130
pcb
500.9
4.288
.8561
Ca3179
Cd2265
Ce4186
C02286
Cr2677
Cu3247
ppb
ppb
ppb
ppb
opb
ppb
498.0
508.1
494.9
501.0
501.2
496.2
3.153
3.827
3.136
3.039
3.703
1,62
.6331
.7533
.6336
.6065
.7388
.3265
Fe2714
K_7664
Li6707
Ng2790
Hn2576
NO2020
ppb
ppi
ppb
ppb
ppb
pcb
501.0
4.942
474.8
501.2
495.2
496.2
7.211
.0181
3.127
3.391
3.069
4.009
1.439
.3656
.6586
.6767
.6198
.8079
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
ppa
ppb
ppb
ppb
opb
ppb
4.853
505.5
521.2
491.1
514.3
488.0
.0743
3.201
5.935
.7056
5.313
4.642
1.531
.6331
1.139
.1437
1.033
.9513
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
ppb
ppb
ppb
opb
opb
ppb
518.1
513.4
506.6
515.0
489.4
488.8
2.469
4.235
3.778
2.769
3.196
1.14
.4766
.8249
.7457
.5376
.653
.2332
Ti3349
T11908
V_2924
Zn2062
Si2881
ppb
ppb
ppb
ppb
ppb
493.2
504.6
498.1
506.2
5032.
2.647
6.149
3.475
5.271
66.56
.5367
1.219
.6976
1.041
1.323
57
-------
Analysis Seoort
Averages
Sun 10-05-97 06:31:45 PM page 52
Method: TRIANGL2 Saisoia Name: IC3/CCB Operator: OKH
Run lime: 10/04/97 00:49 filenase: 100397
node: C0HC Type: a Corr. Factor: 1.00000
Lab ID.: Oust. Sapl. ID.: Oust. ID.: 43159A
Elans
Units
Avge
SOev
*RSD
Eless
Units
Avge
SDev
IRSD
Eleras
Units
ftvge
SDev
tRSD
Elests
Units
ftvge
SDev
%RSD
Eleis
Units
Avge
SDev
IRSD
Eleas
Units
ftvge
SDev
IRSD
Ag3280
ppb
.4676
.3998
85.49
Ca3l79
ppb
-2.419
.4539
18.76
Fe2714
ppb
1.474
5.144
348.9
Na3302
ppa
.0831
.1408
169.3
1960-1
ppb
3.256
1.923
59.07
Ti3349
ppb
.4955
.0862
17.39
A13082
ppb
24.45
4.293
17.56
Cd2265
ppb
.4600
.1478
32.12
K_7664
ppn
.0931
.022
23.63
M12316
ppb
1.560
.1298
8.32
1960-2
ppb
-3.708
1.497
40.35
T11908
ppb
4.448
4.721
106.1
As 1890
ppb
1.327
.7063
53.23
L16707
ppb
.6785
.07
10.32
PJ149
ppb
7.318
2.333
31.88
Pb2203
ppb
-.6864
.8071
117.6
VJ924
ppb
1.468
.1929
13.1*
8_2496
ppb
30.67
4.552
14.84
«g2790
ppb
2.058
2.257
109.7
2203-1
ppb
.0892
2.374
2660
8a4934
ppp
.4992
.094
18.82
Cr2677
pDb
.6418
.1187
18.5
Mn2576
ppb
.4741
.1062
22.4
2203-2
ppb
-1.074
1.223
113.9
8e3130
ppb
.5798
.1473
25.4
Cu3247
DDb
-.5379
.2206
41.02
HO2020
ppb
1.498
.6762
45.14
Sb2068
ppb
3.589
1.992
55.51
SN215
ppb
.4811
.1049
21.8
Sel960 Sn 1899
ppb pob
-1.389 '1.787
.797 1.266
57.37 70.88
2n2062 S12881
ppb ppb
.8561 Q-141.6
.0993 31.26
11.6 22.07
Ce4186 Co2286
pob ppb
-.1950 .6703
.9893 .0431
507.3 6.43
58
-------
na.iysis Resort Averages Sun 10-05-97 06:31:45 PI1
lethoc: TRIANGL2
Jun Time: 10/04/97
Mode: CONC
Lab ID.:
I 6
u
no
I
Sample Name: ICSAB Operator: QKH
00:55 Filename: 100397
Type: 6 Corr. Factor: 1.00000
Cust. Smpi. ID.:
Cust. ID.: 43159A
Elems
Ag3280
A13082
As 1890
B_2496
8a4934
8e3130
Inits
ppb
ppb
ppb
ppb
ppb
ppb
|vge
544.3
505800.
533.3
553.5
514.3
489.3
SDev
1.251
3758
4.029
6.369
.9676
2.806
iRSD
.2296
.743
.7547
1.151
.1881
.5734
f
Id
v
I
lems
Ca3179
Cd2265
Ce4186
o
r»o
oo
o--
Cr2677
Cu3247
inits
ppb
ppb
ppb
ppb
ppb
ppb
[vge
457000.
480.4
500.6
475.1
480.9
542.7
bev
3026
1.509
1.317
1.811
2.907
3.67
RSD
.6621
.3141
.2631
.3811
.6045
.6762
(lens
Units
!vge
Dev
RSD
I:
Av
ID
R
(less
nits
Avge
I Dev
RSD
(lens
nits
vge
SDev
Irsd
I
Elens
I nits
vge
Dev
«SD
Fe2714
K_7664
Li6707
Mg2790
Hn2576
Mo2020
ppb
ppm
ppb
ppb
ppb
ppb
177800.
Q25.13
615.8
539900.
455.3
498.7
563
.1375
4.351
94.57
2.066
1.471
.3167
.5471
.7065
.0175
.4539
.295
Na3302
Ni2316
P_2149
2203-1
2203-2
Sb2068
ppa
ppb
PPb
ppb
ppb
ppb
5.530
461.6
554.8
494.2
488.7
514.8
.0715
1.506
16.23
1.475
8.632
3.078
1.294
.3262
2.926
.2985
1.766
.5979
1960-1
1960-2
Pb2203
Se1960
Snl899
Sr4215
ppb
ppb
ppb
ppb
ppb
ppb
548.9
529.2
490.6
535.8
504.1
504.8
7.083
5.996
5.299
3.02
4.475
.6384
1.29
1.133
1.08
.5637
.8878
.1265
Ti3349
T11908
V_2924
Zn2062
Si2881
ppb
ppb
ppb
ppb
ppb
493.4
518.2
492.8
453.8
5057.
1.042
9.822
2.03
5.004
84.31
.2112
1.895
.412
1.103
1.667
-------
Analysis neoort Averages
Sun 10-05-97 06:21:52 PM
cage 1
lethod: TRIAN6L2 Saaole Nane: 431598 MB Operator: OXH
tan Tibs: 10/04/97 01:09 filenaae: 10039?
lode: C0NC ivoe: S Corr. Factor: 1.00000
.ab ID.: Cust. Sapl. ID.: Cust. ID.: 43159B
lens ftsl890 8e3130 Cd2265 Co2286 Cr2677 I1n2576
Inits ppb ppb ppb ppb ppb ppb
ivge L-.6948 L.0887 L-.153S L-.4425 L.4121 L.4566
!0ev .1128 .0365 .04 .1178 .3671 .026
RSO 16.24 41.2 26.06 26.61 89.07 5.69
leas
N12316
Pb2203
Sb2068
Sel960
nits
ppb
ppb
pob
ppb
ivoe
L-.7160
1.9267
L-.8814
L-.9954
Dev
.6181
.8056
.4715
.9104
RSO
86.33
86.94
53.49
91.46
-------
¦uvsis Reoort Averages
Sun 10-05-^7 06:21:52 PH
cage 2
tftoa: TRIANGL2 Saiole Na»e; 4-3159B ICS
Time: 10/04/9? 01:14 Filename: 100597
^ode: CONC
Eft
e
V10
Elems
I
SOev
10
IS
Units
te
v
Operator: DM
Type: S
Corr. Factor:
1.00000
Cust. Srcpi. ID.:
Cust.
ID.: 431598
As 1890
Be3i30
Cd2265
Co2286
Cr2677
Mn2576
cpb
ppb
DCS
DDb
ppb
ppb
45.87
46.15
47.91
47.80
48.57
48.02
.6588
.185
.4976
.4967
.4279
.1305
1.436
.4009
1.039
1,039
.8811
.2718
Ni2316
Pb2203
Sb2068
Sel960
ppb
ppb
ppb
ppb
47.82
48.60
48.00
45.02
.4891
.9573
.6179
.8984
1.023
1.97
1.287
1.995
61
-------
inaiysis Resort Averages
Sun iO-05-97 06:21:52 PH
page 3
ethos: TRIANGL2 Sasple Name: 182-30-16A Ooerator: DKH
,un Tiae: 10/04/97 01:19 Filename: 100397
ode: C0NC Tyoe: S Corr. Factor: 1.00000
.ab 10.: Oust. Sopl. ID.: Cist. ID.: 431598
lens
ftsl890
Se3130
Cd2265
Co2286
Cr2677
Hn2576
'nits
ppb
ppo
ppb
ppb
ppb
ppb
vae
42.13
1*1.132
7.688
1.9026
250.9
1891.
:Dev
8.428
.0267
.5779
.4159
1.12
12.36
RSD
20
2.36
7.516
46.08
,4464
.6537
leas
Hi2316
PP2203
Sb2068
Sel960
nits
ppb
ppb
ppb
ppb
ivge
42.48
131.6
L-1.004
83.18
Oev
.676
1.003
.9143
4.568
,RSD 1.591 .7621 91.1 5.492
62
-------
I
I
Mo
i
aivsis neaort
Averaoes
Sun 10-05-97 06:21:52 PM
oaas 4
stnoa: TRIANGL2 Samoie Name: 182-30-16A PDS
lin «me: 10/04/97 Oi:23 Filename: 100397
Mode: CONC
ab ID.:
Type: S
Oust. Sad. ID.;
Corr. Factor:
Ooerator: DKH
1.00000
Cust. ID.: 431598
Eleis
As1890
883130
Cd2265
C02286
Cr2677
Hn2576
Biits
ppb
ppb
ppb
ppb
ppb
ppb
™ ge
92.17
49.08
58.55
51.15
298.1
1914.
SDev
1.52
.3307
.2688
.2889
1.678
12.27
MSQ
1.649
.6738
.459
.5648
.5627
.641
Elens
Ni2316
Pb2203
Sb2068
Sel960
Mts
ppb
ppb
ppb
ppb
vge
92.72
181.3
50.29
151.6
W)ev
.2617
.2781
1.663
2.125
IRSD
.2822
.1533
3.307
1.402
63
-------
Analysis Report Averages
Sun 10-05-97 06:21:52 PM
Melhoa: TRIANGL2 Samole Name: 182-30-16A L Ooerator: DKH
Sun line: 10/04/97 01:28 Filename: 100397
Mode: C0NC Tyoe: S Corr. factor; 1.00000
Lab ID.: Gust, SbdI. ID.: Cust. ID.: 431598
Elems
Units
ftvge
SDev
%RSD
ftsl890
DD0
11.01
2.363
21.46
8e3130
ppb
L-.0757
.0495
65.35
Cd2265
PPb
L.5500
.1166
21.2
Co2286
ppb
L-.5436
.2905
53.44
Cr2677
PPb
51.15
.6394
1.25
Hn2576
ppb
368.4
1.231
.3341
Eleas
Ni2316
Pb2203
Sb2068
Sel960
Units
ppb
ppb
PPb
ppb
ftvge
11.04
26.71
1.4149
19.70
SDev
.8358
.5309
1.038
.153
iRSD
7.574
1.988
250.1
.777
-------
alysis Recort Averages
Sun 10-05-^7 06:21:52 PM cage o
I
flod
I
ssthod: TRIAMGL2 Samole Na«ie:
jn Time: 10/04/97 01:33
"ode: C0NC
Lab ID.:
iype: S
Cust. Sid!, ID,
182-30-165
F i ieriame: 100397
Corr, Factor:
Cust.
Qcerator: DXN
1.00000
431598
El ems
Asl8?0
8e3l30
Cd2265
Co2286
Cr2677
Hn2576
¦nits
ppb
pob
DOS
ppb
pDb
pDb
Jvge
29.05
L-1.026
9.177
1.-. 1660
260.6
1723.
SDev
2.014
.0094
.5306
.263
2.565
15.39
ARS0
6.932
.913?
5.782
158.4
.9843
.8933
Reus
Ni2316
Pb2203
SD2068
Sel960
Units
ppb
ppb
ppb
ppb
l/ge
49.10
261.6
L-4.378
98.89
Rev
.4101
.5778
.8385
3.047
.8353
.2208
19.15
3.082
65
-------
Analysis Report Averages
Sun 10-05-97 06:21:52 PM page 7
Method: TRIANGL2 Saioie Name: 182-30-168 DA Operator: OKH
Sun Tine: 10/04/97 01:37 Filenarae: 100397
Mode: CONC Type: S Corr, Factor: 1.00000
Lab ID.: Cust. SbdI. ID.: Oust. ID.: 431S9B
El ens
AS1890
mm
CU2265
C02286
Cr2677
fln257o
Units
ppb
PPb
ppb
ppb
PPb
ODD
Avge
26.90
1-1.031
9.681
L-.3559
260.8
1725.
SDev
1.368
.0264
.3571
.1981
.8493
8.558
IRSD
5.086
2.558
3.689
55.66
.3257
,4962
Elems
Ni2316
Pb2203
S&2068
Sei960
Units
pob
pob
ppb
DDb
ftvge
48.57
263.1
L-6.928
97,69
SDev
.7402
2.327
.6833
1.223
IRSD
1.524
,8844
9.864
1.252
66
-------
Hr,aiysis Reoort Averages
Sun 10-05-97 06:21:52 PM
page 8
I
I
I
Wl
Method:
TRIANGL2
Saioie Nans: 182-30-16C
Operator:
Run Time
: 10/04/97 01:42
filename:
1003<7
Mode: CQNC
Type: 5
Corr. factor:
I.00000
lab ID.:
Oust. Sinpl. ID.:
Oust.
ID.: 431598
Elems
As 1890
8e3130
Cd2265
C02286
Cr2677
Mn2576
Units
ppb
ppb
ppb
ppb
pcb
pcb
jAvge
20.12
L-.0620
L.8340
L-1,358
48.04
156,9
SOev
.5819
.0197
.1106
.3086
.4239
.3982
,%RSD
2.893
31.87
12.51
22.72
.8824
.2537
'Elems
Ni2316
Pb2203
Sb2068
Sel960
Units
ppb
ppb
ppb
ppb
Iftvge
14.29
69.56
L-.8019
46.13
BDev
.3183
.0799
2.365
1.112
IRSD
2.227
.1149
294.9
2.411
67
-------
Analysis fieoort
Averages
Sun 10-05-97 06:21:52 PM
page 9
Method; IRIANGL2 Sasoie Nane: 182-S0-160 Oceratcr: DKH
Run Time: 10/04/97 01:47 filenaae: 100597
Mode: C0NC lyoe: S Corr. Factor: 1.00000
Lab ID.: Cust. Sspi. ID.: Cust. ID.: 43159B
Eleis
Units
Avge
SDev
IRSD
Elens
Units
Avge
SDev
IRSD
AslS90
ppb
21.76
1.645
7.561
Ni2316
ppb
17.48
.4308
2.464
863130
ppb
L-,2082
.0165
7.921
PP2203
ppb
254.7
1.648
.6471
Cd22o5
ppb
2.311
.0719
3.109
SP2068
ppb
L-.7289
1.326
181.8
Co2286
ppb
L-1.341
.1553
11.59
Sel960
ppb
54.03
.6835
1.265
Cr2o77
ODD
88.63
.315
.9195
Hn2576
ppb
324.0
1.929
.5954
68
-------
ifialvsis Recort Averages
Sun 10-05-9? 06:21; 52 ?ft page 10
[lethod: T8IAN5L2
Jun line: 10/04/97
Mode: CONC
Lab ID.:
t
l
Sample Naae
01:51
Type: 5
Cust. Saoi. ID
182-30-ioE
Filename: 100397
Corr. Factor:
Cust.
Operator: DKH
1.00000
ID.: 431598
Elems
AsiS90
Be3130
M2265
Co228o
Cr2677
Mn2576
Inits
ODD
spb
DDb
DSD
psb
DDb
|vce
23.96
L-1019
L-.2604
L-1.319
12.01
9.872
SDev
.5897
.0194
.0561
.1545
.3117
.1281
tfiSD
2.461
19.09
21.54
11.71
2.595
1.297
Ileus
Ni2516
Pb2203
Sb2068
Sel960
JJni ts
ppo
ppb
ppb
ppb
Ivge
10.50
6.726
12.295
40.23
wev
.4483
1.347
1.009
2.494
*RSD
4.272
20.03
43.98
6.199
6£
-------
Analysis Report Averages
Sun 10-05-97 06:21:52 PH page 11
Method: TRIAN6L2 Saiole Name: 1CV/CCV Operator: OKH
Run Ti§e: 10/04/97 01:56 Filename: 100397
Mode: C0NC Tyoe: Q Corr. Factor: 1.00000
lab ID.: Cust. Supl. ID.: Cust. ID.; 431598
Elenss
Ag3280
A13082
AS1B90
8.2496
3a4934
883130
Units
ppb
ppb
00b
ppo
pob
ppb
flvgs
0345.7
0314.9
0353.0
272.7
0336.0
0338.0
SDev
277.7
365.8
281.1
442.5
270.8
271.4
SRSD
80.35
116.2
79.61
—ttTTo"
80.27
El ems
Ca3179
Cd2265*
Ce4l86
C02286
Cr2677
Cu3247
Units
ppb
pob
ppb
ppb
ODb
ppb >
Avge
0341.0
0343.2
337.2
0338.9
9344.1
033^y
SOev
263.4
275.2
268.2
270.7
272.5
m.i
IRSD
77.25
80.18
79.52
79.89
79.19 ,
/83.85
Eleas
Units
Avge
SDev
IRSD
Eleas
Units
Avge
S08V
IRSD
Eleas
Units
ftvge
SDev
%RS0
Eleas
Units
Avge
SDev
IRSD
Fe2714
ppb
0383.6
298.7
77.87
K.7664
ppn
83.654
1.978
54.13
U6707
ppb
0327.4
235.9
72.03
Ng2790
ppb
033^
4
79.79
576
ppb
3335.8
268.8
80.06
N12316
ppb
8344.
273
7/38
149
ppb
Q353.2
268.5
76.04
2203-1
ppb
328.6
281.5
85.67
Na3302
Pb2203
Sil960
ppb
8383.9
222
57.83
Snl899
ppb
8328.7
260.3
79.19
Sr4215
8332.1
.Ti3349
0334.1
8343.4
262.1
76.33
MO2020
ppb
8335.5
268.4
2203-2 Sb2068
ppb ppb
392.1 8335.8
182 268.4
46.42 79.92
V_2924
ppb
0340.4
264.4
77.66
ppb
8343.
273.7
79.61
ppb
660530.
25520
48.77
N
uV
voV
-------
fiysis Reoort Averages
Sun i0-05-e7 06:21:52 PH oage 12
hod: TRIANGL2
R^Iime: 10/04/97
Hode; CONC
1,
to
1
Hode:
l^ID
Elems
1
SDev
igt
£lMS
Ujits
ft
jjfns
Units
Ie
Sas
ts
Avae
I
|
SDev
I
Eless
SMV
lD
ins
ts
re2714
Na3302
pps
4.802
.0987
2.056
Sample toe: ICV/CCV Operator: 0KH
02:02 filename: 100397
Ivpe: C Corr. Factor: 1.00000
Cust. SbdL ID,: Cust. ID.: 431598
Ag3280
A13082
AS1890
8.24%
634934
8e3130
ppb
ppb
ppb
ppb
ppb
ppb
513.5
525.9
520.0
852.8
498.6
502.8
2.561
11.53
1.424
147.9
1.533
2.562
.4987
2.193
.2739
—J&7r~
.3395
Ca3179
ppb
499.9
3.286
.6573
Cd2265 Ce4186
ppb ppb
509.0 496.7
2,212 2.822
.4346 .5682
K.7664 Li6707
ppi ppb pof
4.863 469.5 /500.3
.0218 4.756/ 2.588
H12316
ppb
SIC
1/563
<<3061
Co2286
Cr2677
PPD
509
2 J^9
1978
Mn2576
2203-1
ppb
489.4
3.801
.7767
2203-2
ppb
508.3
1.767
.3475
3.595
.6985
.3166
.0631
Si2881
2n2062
ppb
509.4
5.364
1.053
091570
Sb2068
ppb
498.9
.4415
.0885
1960-2 PO2203 Sel960 Snl899 Sr4215
ppb ppb ppb ppb
514.6 502.0 516.3 487.9 491.6
.1767
O
^ ft
ho 4
-------
Anaiysis Report Averages
Sun iO-05-^7 06:21:52 PK pap 13
Hsthoo: TRIAN6L2 Saoiole Name: ICV/CCV ODerator: D*r
Sun Tine: 10/04/97 02:34 Fiiefiame: 10039/
Mode: CQNC Type: Q Corr. Factor: 1.00000
Ub ID.: Cust. Sapl. ID.: Cust. ID.: 431S9B
Eless
Units
Avge
SDev
IRSD
Elems
Units
Avge
SDev
IRSD
Ag3280
ppb
512.3
2.633
.514
Ca3179
ppb
498.2
1.84
.3693
A13082
ppb
532.1
10.42
1.957
Cd2265
ppb
505.2
1.554
.3076
fts!890
ppb
516.7
.808
.1564
Ce4186
ppb
494.4
.8722
.1764
8.2496
ppb
2045.
122
5.964
C02286
ppb
500.2
1.424
.2846
8a493i
ppb
495.6
.834
.1683
Cr2677
ppb
502.7
1.89
.376
8e3130
ppb
498.2
1.751
.3515
Cu3247
ppb
500.0
3.335
.6669
Elfiis
Fe2714
K_7664
U6707
Ng2790
Mn2576
Ho2020
Jnits
ppb
PPB
ppb
ppb
ppb
ppb
}vae
490.0
4.929
474.4
500.4
495.9
495.4
SDev
6.145
.034
3.022
.8907
1.31
1.59
tRSD
1.254
.6902
.6371
.178
.2643
.3209
•lens
Na3302
Hi2316
P.2149
2203-1
2203-2
Sb2068
Jnits
PP®
ppb
ppb
ppb
ppb
ppb
5vge
4.885
506.3
517.7
490.8
508.6
492.4
SDev
.1073
2.216
4.391
4.689
6.927
2.389
IRSD
2.197
.4377
.8481
.9554
1.362
.4852
;le«s
1960-1
1960-2
Pb2203
Sel960
Snl899
Sr4215
Jnits
ppb
ppb
ppb
ppb
ppb
ppb
ivge
514.7
510.7
502.7
512.0
484.6
488.5
!Dev
3.383
3.065
3.06
2.258
3.336
.3432
iRSD
.6573
.6002
.6088
.4409
.6884
,0703
:ie«s
U3349
T11908
V_2924
Zn2062
Si2881
inits
ppb
PPb
ppb
ppb
ppb
ivge
492.7
496.3
497.1
505.6
037360.
;Dev
.7631
10.46
.5107
3.233
3119
;RSD
.1549
2.107
.1027
.6395
8.349
71
-------
nalysis Re do r t Averages Sun 10-05-97 06:21 :52 PM cage
I
MO
I
thod: TRIANGL2 Satiole Name:
n Tine: 10/04/97 02:44
Mode: C0NC
ab ID.:
Elems
Kits
ge
SDev
Elems
(its
ge
ev
WSD
leas
Units
ev
%RSD
«ess
its
Avge
Kev
SD
(lens
[its
vge
(ev
SD
El ess
I its
ge
SDev
Type: 0
Oust. S#pl.
ICB/CC8
Filenasie: 100397
Corr. Factor:
ID.: Cast. ID
Ooerator: OKH
1.00000
431598
Ag3230
A13082
ftsl890
8.2496
8a4934
8e3130
ODD
ppb
ccb
ODD
ppb
ppb
-.0786
31.28
1.888
1976.
.0936
.2301
.4351
5.254
1.527
143.9
.0122
.0399
553.9
16.8
80.86
7.283
13.04
17.33
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
ppb
ppb
ppb
ppb
ppb
ppb
-3.845
-.1505
.1952
-.3339
1.204
-.6844
.9689
.0551
.4561
,2329
.2551
.369
25.2
36.6
233.7
69.77
21.19
53.92
Fe2714
K.7664
Li6707
Mg2790
Hn2576
MO2020
ppb
ppn
ppb
ppb
ppb
ppb
-2.765
.0629
.2489
.2085
.0157
.0592
2.758
.0175
.0106
1.874
.0181
.5317
99.74
27.82
4.267
899.1
115
897.5
Na3302
Ni2316
P.2149
2203-1
2203-2
Sb2068
ops
ppb
ppb
ppb
ppb
ppb
-.0425
2.237
7.006
-1.617
-1.498
.9307
.0933
.3687
4.545
1.926
2.259
.8699
219.5
16.48
64.87
119.1
150.8
93.47
1960-1
1960-2
Pb2203
Sel960
81)1899
Sr4215
ppb
ppb
ppb
ppb
ppb
ppb
4.014
-3.173
-1.538
-.7799
.2936
.0849
.1527
.2332
1.027
.1611
.5348
.0264
3.804
7.35
66.77
20.65
182.2
31.06
Ti3349
T11908
V.2924
Zn2062
SI2S81
ppb
ppb
ppb
ppb
ppb
.0627
4.257
.7327
.1579
Q19460.
.0233
3.695
.1954
.1124
1906
37.1
86.8
26.67
71.2
9.796
72
-------
Analysis Report
Averages
Sun l(K5"7 06:21:52 PM page
Method: TRIANGL2 Saaple Nans: ICSA8 Operator: OKH
Run Time: 10/04/97 03:00 filena«e: 100397
Mode: CONC Type: C Corr. Factor: 1,00000
Lab 10.: Cust. Snpl. 10.: Cust. ID.: 431598
Eleis
Ag3280
A13082
ftsl890
8.2496
Ba493i
083130
Units
ppb
ppb
ppb
ppb
ppb
ppb
ftvge
548.3
506600.
538.4
3584.
514.8
490.9
SDev
.4325
1351
.0963
86.16
.5125
2.683
IRSD
.0789
.2667
.0183
2.404
.0996
.5466
El ens
Ca3179
Cd2265
Ce4186
Co2286
Cr2677
Cu3247
Units
ppb
ppb
ppb
ppb
opb
pob
ftvge
460800.
483.3
503.0
477.6
485.2
544.6
SDev
2419
2.308
1.137
2.098
2.578
.973
IRSD
.5249
.4775
.226
.4393
.5313
.1787
Elens
Fe2714
X.7664
Li6707
Ha2790
Hn2576
HO202Q
Units
ppb
ppn
ppb
ppb
ppb
PPb
ftvge
178400.
824.83
607.9
542400.
459.5
501.2
SDev
646.3
.0768
1.732
1027
2.009
2.601
IRSD
.3622
.3092
.2849
.1893
.4373
.519
Eleis
Units
Avge
SOav
IRSD
Eleas
Units
Avge
SDev
%RS0
Elenis
Units
Avge
SOav
IRSD
Na3302
ppB
5.457
.0857
1.571
1960-1
ppb
548.8
9.923
1.808
Ti3349
ppb
495.4
1.611
.3252
Ni2316
ppb
464.9
1.833
.3942
1960-2
ppb
530.7
6.944
1.308
111908
ppb
519.0
10.76
2.074
PJ149
ppb
558.7
11.72
2.098
Pb2203
ppb
492.2
3.108
.6314
V.2924
ppb
494.6
1.981
.4005
2203-1
ppb
495.7
4.684
.9449
Sel960
ppb
536.7
3.059
.5698
In2062
ppb
457.9
2.613
.5707
2203-2
ppb
490.4
6.969
1.421
SnlS?^
ppb
503.7
3.659
.7264
Si2881
pob
0130SO
896.2
6.851
Sb2068
ppb
518.9
5.036
.9705
Sr4215
ppb
505.8
.6583
.1301
-------
D/Weignt File: A8S09.IDW
ample Volume: 100 mL
finalyst: RICHARDS
Nominal Weigfit: 1.0 g
Loc. Sample ID Weight Dilution
5TD ELK
-*^srroi=G72ug/L
STD2=0.5ug/'l
4 STD4=2.0ug/L
5 ST05=5.0ug/'L
6 STD6=10.Oug/L
3 STD3=1.0ug/L - r> 11 -1 rY\&-
STfUr? Dua/I > "t> ^' ' 1
STD6=10.0ug/L „ . |c-,
ICV=4.0ug/L ^|XV+' ^
7
S ICS
9 CHECK LO
10 43182 MB
11 43182 MB D
12 43182 LCS
13 43182 LCS D
14 182-53-1-3
15 182-53-1-3 D
16 182-53-4
17 182-53-4 D
18 182-53-4 MS
19 182-53-4 MSD z-on-ft ^ iN"/??
20 CCVl=6.0ug/'L —
21 CCB1
22 132-53-2-5
23 182-53-2-5 D
24 182-53-6
25 182-53-6 D
26 CCV2=6.0uq/L —
27 CCB2
28 431598 MB
29 43159 MB D
30 43159 LCS
31 43159 LCS D
32 182-30-16A
33 182-30-16A D
34 182-30-16A M3
35 182-30-16A MSD
36 182-30-168
37 182-30-16B D
38 CCVl=6.0ug/L
39 CCB1
40 182-30-16C
41 182-30-16C 0
42 182-30-16D
43 182-30-16D 0
44 182-30-16E
45 182-30-16E D
46 CCV2=6.0ug/L
47 CCB2
48 43048 MB
49 43048 MBD
50 43048 LCS
51 43048 LCS 0
52 181-18-13B
53 181-18-138 D
2-0n
voo-? (^7
-------
Sample [D
Weight Dilution
181-18-13 M3
181-18-13 MSD I ,
ccvir^oug/L — 3-Di7-£ ^ ^lzflciy
-------
I
I
I
I
I
I
I
I
I
I
Element File: H6_.MEL
Element: Hq2
Print Data: Main+Suppl.
Print: Calib. Curve
Remarks:
STANDARDS: 3-017-7
GC= 3-017-8
INSTRUMENT: 5100
Wavelength: 253.7 Peak
Signal Type: AA
Read Time: 30.0
Sample Replicates: 1
Standard Replicates: 1
Analyst: RICHARDS
Peak Storage: Hons
5
Technique: MHS Version: 7.01
Slit: 0.7 Low
Sighal Measurement: Peak Height (5)
Read Delay: 1.0 80C Time: 2
FLAME:
Flame Type:
Air
Flame Sensor: On
Oxidant Flow
: 10.0'
L/min
Fuel Flow: 2'.0 L/min
CALIBRATION:
*
Solutions
1
1
\
10
! Cone |
1 1
Calib. Blank
! S TO
BLK
1 1
( -- ^
Standard 1
I STD
1
: 0.2001
Standard 2
ST0
i.
! 0.500!
Standard 3
I STD
3
! i.oooj
.Standard 4
! STD
4
! 2.000!
Standard 5
! STD
c
! 5.000!
Standard 6
,'STO
6
! io.ooo!
1 Calibration
Units:
ug./L
Sample Units: ug/L
1 Calibration
Type:
Linear
¦iatrix Check Calculations:
« Difference for Duels: No
% Recovery for Spike: No
Locations:
Locations:
Cone;
76
-------
Element File: HG_.MEL
Date: 09/24/9 7
Data File: AB809.0AT
Technique: MH3
Remark-i: STANDARDS^ 3-
Remark 2: >3C = 3-017-8'
Element; Hg2
Time: 15:19
I0/Wt File: A8809.IDW
Calib. Type: Linear
Wavelength: 253.'
3lit: 0.7 L
Lamp Current: 0
Energy; 72
Ha2 10: STO BLK Sea, No.: 00003 A/S Pes.: — Date: 09/24/97
Replicate l Time: 15:22
Peak Area (A^s ): -0.000 -Peak Height EA); 0.000
Blank Corrected Pk Height (A): 0."000
Concentration (ug/L ): 0.000
Auto-zero performed. .
Ha2 ID: STDl=0.2ug/L Seq. No.: 00004 A/3 Pos.: — Date: 09/24/9"
Sample abs. is greater than that of the largest standard.
Replicate 1 " Time: 15:23
Peak Area (A-s): 0.162 Peak Height (A): 0.006
Blank Corrected Pk Height (A): 0.006
Concentration tug/L ): 0.286
Standard number 1 applied. [0.200]
Correlation coefficient: 1.00000 Slope: 0.0316
Kg2 ID: STD2=0.Sug/L Seq. No.: 00005 A/3 Pos.: — Date: 09/24/97
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:24
Peak Area (A-s): 0.402 Peak Height (A): 0.017
Blank Corrected Pk Height (A): 0.017
Concentration (ug/L ): 0.533
i
Standard number 2 applied. [0.500]
Correlation coefficient: 0.99348 Slope: 0.0334
Hg2 ID: STD3=1.0ug/L Seq. No.
Sample abs. is greater than that of t
Replicate 1
-Peak Area (A-s): 0.824
Blank Corrected Pk Height (A): 0.035
Concentration (ug/L ): 1.044
Standard number 3 applied. [1.000]
Correlation coefficient: 0.99916
Hg2 ID: STD4=2.0ug/L Seq. No.
00006 A/S Pos.: — Date: 09/24/97
i largest standard.
Time: 15:26
Peak Height (A): 0.033
Slope: 0.0346
00007 A/S Pos.: — Date: 09/24/97 "
Sample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:27
-------
I
ak Area (A-s): 1.724 Peak Height (A): 0.074
Blank Corrected Pk Height (A): 0.074.
Jncent ration ( ug/L ): 2.143
Standard number 4 applied. [2.000]
rrelation coefficient: 0.99865 _ Slope: 0.0365
I
n
ID; ST05=5.0ug/L Seq. No.: 00008 A/3 Pos.: — Date: 09/24/97
ample abs. is greater than that of the largest standard.
Replicate 1 Time: 15:29
fak. Area (A-s): 4.517 Peak Height (ft): 0.194
ank Corrected Pk Height (.A): 0.194
Concentration (ug/L ): 5.325
Ilandard number 5 applied. [5.0001
orrelation coefficient: 0.99929 Slope: 0.0385
I
ID: ST06=10.Dug/L Seq. No.: 00009 A/S Pos.: — Date: 09/24/97
¦tmple abs. is greater than that of the largest standard.
^plicate 1 Time: 15:30
Peak Area (A-s): 8.54-9 Peak Height (ft): 0.370
Mank Corrected Pk Height (A): 0.370
¦>ncentration (ug/L ): 9.627
^andard number 6 applied. [10.000]
Brrelation coefficient: 0.99961 Slope: 0.0374
-------
Element File: HG_.M£L Element: Hg2 Wavelength: 253.
Date-: 09/24/97 Time: 15:31 Slit: 0.7 L
Data File: ABS09.QAT I0/Wt File: A8309.IDW Lamp Current: 0
Technique: MHS Calib. Type: Linear Energy: 72
Remark 1: STANDAROS= 3-017-7
Remark. 2: QQ~ 4-017-3' -
H
Display Calibration - C:\fiflJSER\flfl_FILES\ELEMEHT\HG_,HEL
t
8.370! Xw
.jr <50
X-""
.
1
1 - .P^c
.2 ! **
^ -
^M Corn. Coef.: 0.99961
jgga , ,
0.0 Concentration 10.000
I
-------
I
Element File: HG_.HEL
Element: Hg2
Wavelength: 253.7
late-: -09/24/97
Time: 15:32
Slit: 0.7 L
lata File: A88Q9.QAT
ID/Wt File: A8809.IDW
Lamp Current: 0
Technique: MHS
Calib. Type: Linear
Energy: 72
lie mark 1: STANDARDS: 3-017-7
lemark 2:J3G= -3~&i7-8
'
I
ID: ICV=4.Gug/L
Seq. No.: 0Q010
A/3 Pos.
Oate: 09/24/97
(eolicate 1
eai-c Area (A-s): 3.473
lank Corrected Pk Height (A): 0.156
Concentration fug/L ): 4.181
Time: 15:33
Peak Height (A): 0.156
I
Hg2 ID: ICB Seq. No.
Jeplicate 1
Peak Area (A-s): 0.023
^lank Corrected Pk Height (A): 0.001.
Concentration (ug/l ): 0.019
00011 A/S Pos.: —
Time: 15:34
Peak Height (A): 0.001
Oate: 09/24/97
ID: CHECK LO
Seq. No.: 000i:
A/S Pos.:
Oate: 09/24/9*
Reolicate 1
|=ak Area (A-s>: 0.180
lank Corrected Pk Height (A): 0.008
Concentration (ug/t ): 0.212
I
"a;
Time: 15:39
Peak Height (A): 0.008
10: 43182 MB
Seq. No.: 00013
t plicate 1
ak Area (A-s): 0.016
Blank Corrected Pk Height (A): 0.001
Jncentration (ug/l ): 0.013
t:
c
ID: 43182 MB 0
splicate 1
Peak Area (A-s): 0.015
tank Corrected Pk Height (A): 0.001
ncentration (ug/l ): 0.016
A/S Pos.
Date: 09/24/9:
Time: 15:40
Peak Height (A): 0.001
Seq. No.: 00014 A/S Pos.
Time: 15:4-1
Peak Height (A): 0.001
Date: 09/24/9:
ID: 43182 LCS
Seq. No,: 00015 A/S Pos.;
Date: 09/24/9:
Replicate 1
ftak Area (A-s): 5.072
•Lank Corrected Pk Height (A): 0.241
Concentration (ug/l ): 6.441
Time: 15:43
Peak Height (A): 0.241
Hg;
ID: 43182 ICS D
Seq. No.; 00016 A/S Pos.
Date: 09/24/97
-------
Replicate 1
Peak Area (ft-s): 4.753
Blank Corrected PR Height (A);
Concentration (ug/L ): 5.936
Time: 15:44
Peak Height (A): 0.222
0.222
Hg2 ID:^4318,2_J-CS DD , Seq. No'.: 00017 ^ A/S Pos.: — Date: 09/24/9"
Reolicate 1 Time: 15:54
Peak Area (A-s): 4.507 Peak Height (A): 0.207
Blank Corrected Pk Height (A): 0.207
Concentration (ug/L ): 5.531
Hg2 ID: 182-53-1-3 Seq. No.: 00018 A/S Pos.: — Date: 09/24/97
Replicate 1
Peak Area (A-sl: 0.02S
Blank Corrected Pk Height (A):
Concentration (ug/L ): 0.030
Time: 15:55
Peak Height (A): 0.001
0.001
Hg2 ID: 182-53-1-3 0 Seq. No'.: 00019 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 15:56
Peak Area (A-s): 0.014 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.016
Hg2 ID: 182-53-4 Seq. No.: 00020 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 15:57
Peak Area (A-s): 0.755 Peak Height (A): 0.034
Blank Corrected Pk Height (ft): 0.034
Concentration (ug/L ): 0.915
Hg2 ID: 182-53-4 D Seq.; No.: 00021 A/S Pos.: — Date: 09/24/9"
Replicate 1 Time: 15:59
Peak Area (A-s): 0.741 Peak Height (A): 0.035
Blank Corrected Pk Height (A): 0.035
Concentration (ug/L ): 0.929
Hg2 ID: 182-53-4 MS Seq. No.: 00022 A/S Pos.: -- Date: 09/24/97
Replicate 1 Time; 16:00
Peak Area (A-s): 5.766 Peak Height (A): 0.272
8lank Corrected Pk Height (ft): 0.272
Concentration (ug/L ): 7.281
Hg2 ID: 182-53-4 KSD Seq. No.: 00023 A/S Pos.: — Date: 09/24/97
Replicate 1 - Time: 16:01
Peak Area (A-s): 5.623 Peak Height (A): 0.277
Blank Corrected Pk Height (A): 0.277
-------
I
I
oncentration (ug/L ): 7.404
g2 ID; CCVl=6,0ug/L
K eplicate ' 1 -
eak Area_J36cs.Li_S.Oi7
Blank Corrected Pk Height
oncentration (ug/L ): 5
Seq. No.: 00024 A/3 Pos.
I
1
(A): 0.220
.875
~2 ID: CCB1
.eplicate 1
Peak Area (A-s): 0.028
¦lank Corrected Pk Height
concentration (ug/L '): 0.
(A): 0.001
032
Date: 09/24/97
Time: 16:04
Peak Height (A): 0.220'
Seq. Ho.: 00025 A/S Pos.:
Time: 16:05
Peak Height (A): 0.001
Date: 09/24/9:
I
ID: 182-53-
Seq. No.: 00026 A/S Pos.
(eplicate 1
eak Area (A-s): 0.019
lank Corrected Pk Height
Concentration (ug/L ): 0.
(A): 0.001
032
Time: 16:07
Peak Height (A): 0.001
Date: 09/24/9"
ID: 182-53-
D
Seq. No.: 00027 A/S Pos.
Beplicate 1
peak Area (A-s): 0.018
Ilank Corrected Pk Height
oncent rat ion (ug/L ): 0.
(A): 0.001
027
I
ID: 182-53-6
Replicate 1
(ak Area (A-s): 0.411
ank Corrected Pk Height
ncentration (ug/L ): 0.
I
Time: 16:08
Peak Height (A): 0.001
Seq. No.: 00028 A/S Pos.: —
Time: 16:09
Peak Height (A): 0.018
(A): 0.018
486
Date: 09/24/97
Date: 09/24/97
ID: 182-53-6 0
Seq. No.: 00029 A/S Pos.
Date: 09/24/9;
*plicate 1
£ak Area (A-s): 0.422
Blank Corrected Pk Height
oncentration (ug/L ): 0.
I
(A): 0.019
510
Time: 16:10
Peak Height (A): 0.019
Hg2 . ID: CCV2=6.0ug/L
^plicate 1
Peak Area (A—s): 5.069
tank Corrected Pk Height
ncentration (ug/L ): 5.
Seq. No.: 00030 A/S Pos.:
Date: 09/24/97
Time: 16:11
Peak Height (A): 0.222
(A): 0.222
928
-------
Hg2 ID: CCB2 Seq. No.: 00031 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 16:12
Peak Area (A-s ): 0.030 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration .(ug/L '): 0.032,-
Hg2 ID: 43159B MB Seq. No.: 00032 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 16:14
PeaK "Area (A-s): 0.024 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.030
Hg2 ID: 43159 MB D - Seq. No.: 00033 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 16:14
Peak Area (A-s): 0.018 Peak Height (A): 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.013
Hg2 ID: 43159 LCS Seq. No.: 00034 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 16:16
Peak Area (A-s): 4.498 Peak Height (A): 0.19S
Blank Corrected Pk Height (A): 0.198
Concentration (ug/L ): 5.284
Hg2 ID: 43159 LCS D Seq. No.: 00035 A/S Pos.: — Date: 09/24/97
Replicate 1 Time: 16:16
Peak Area (A-s): 4.265 Peak Height (A): 0.190
Blank Corrected Pk Height (A): 0.190
Concentration (ug/L ): 5.088 j
Hg2 ID: 182-30-16A Seq. No.:
.Replicate 1
Peak Area (A-s): 0.089
81ank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.099
00036 A/S Pos.: — Date: 09/24/97
Time: 16:19
Peak Height (A): 0.004
Hg2 ID: 182-30-16A D Seq. No.: 00037 A/S Pos.: — Date: 09/24/97
Repiicate 1 Time: 16:21
Peak Area (A-s): 0.086 Peak Height (A): 0.004
81ank Corrected Pk Height (A): 0.004
Concentration (ug/L ): 0.097
Hg2 ID: 182-30-16A MS Seq. No.: 00038 A/S Pos.
Date: 09/24/9"
-------
I
Replicate 1
¦Peak Area (A-s ): 5.025
J81ank Corrected Pk Height (A): 0.247
Concentration (ug/L ): 6.621
T-ime: 16:27
Peak Height (A): 0.247
lta2
10: -4~82-30'-16A MSO'
1
Sea. No.: 00039 A/S'Pos.: —
feeo1icate
B^eak Area (A-s ): 4.737
Blank Corrected Pk Height (A): 0.216
j^oncentration (ug./L ): 5.770
I
ID: 182-30-16B
dedicate 1
Peak Area (A-s): 0.129
¦Blank Corrected Pk Height (A): 0.005
Concentration (ug/L ): 0.140
Date: 09/24/eak Area (A-s): 0.025
ftlank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.027
Time: 16:46
Peak Height (A): 0.230
Seq." No.: 00043 A/S Pos.: — Date: 09/24/97
Time: 16:47
Peak Height (A): 0.001
fig 2 ID: 182-30-16C
Seq. No.: 00044 A/S Pos.: -- Date: 09/24/9!
(
i
,epl icate 1
eak Area (A-s): 0.051
lank Corrected Pk Height (A): 0.002
oncentration (ug/L ): 0.048
Time: 16:49
Peak Height (A): 0.002
Hg;
10: 182-30-16C 0
|teplicate 1
Peak Area (A-s): 0.051
lank Corrected Pk Height (A): 0.002
Seq. No.: 00045 A/S Pos.
Time: 16:50
Peak Height (A): 0.002
i
Date: 09/24/97
-------
Concentration (ug/l ): 0.051
Hg2 ID: 182-30-16D Seq. No.: 0004-6 A/S Pos. : — Oate: 09/24/9"
Replicate 1 _ Time: 16:51 -
Peak Area _('ft-s): 0.039 ; Peak Height (A): 0.002-
Slank Corrected Pk Height (A): 0.002 "*
Concentration (ug/L ): 0.040
Hg2 ID; 182-30-160 0 Seq. No.; 00047 A/S Pos.: — Date: 09/24/9"
Replicate 1 Time: 16:53
Peak Area (A-s): 0.035 Peak Height (A): 0.002
Blank Corrected Pk Height (A): 0.002
Concentration (ug/L •): 0.043
Hg2 ID: 182-30-16E Seq. Mo.: O0O48 A/S Pos.: — Date: 09/24/9"
Replicate 1 • _ Time: 16:54
Peak Area (A-s): 0.136 Peak Height (A): 0.006
Blank Corrected Pk Height (A): 0.006
Concentration (ug/L ): 0.156
Hg2 ID: 182-30-16E D
Seq. No.: 00049 A/S Pos.
Date: 09/24/97
Replicate 1
Peak Area (A-s): 0.125
Blank Corrected Pk Height (A):
Concentration (ug/L ): 0.142
0.005
Time: 16:56
Peak Height (A);
0.005
Hg;
ID: CCV2=6.0ug/i
Seq. No.: 00050 A/S Pos.
Date: 09/24/91
Replicate 1
Peak Area (A-s): 5.083 -•
Blank Corrected Pk Height (A): 0.222
Concentration (ug/L 5: 5.939
Time: 16:58
Peak Height (A); 0.222
Hg2 ID: CCB2 Seq. No.: 00051 A/S Pos.: — Date; 09/24/97
Replicate 1 Time: 16:59
Peak Area (A-s): 0.028 Peak Height (A): 0.001
Slank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.027
Hg2 ID: 43048 MB Seq. No.: 00052 A/S Pos.: — Oate: 09/24/97
Replicate 1 Time: 17:01
Peak Area (A-s): 0.022 _ Peak Height (A); 0.001
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.019
-------
I
I
I
ID: 4304S M80
Sea. No.: 00052
A/3 Pos.:
Date: 09/24/9"
Replicate 1
Peak Area (A-s): 0.021 _
Blank Corrected Pk Height (A); 0.001
Concentration (ug/L ): 0.021-
Time: 17:02
Peak Height (A): 0.001
I
ID: 43048 LCS
Seq. No.: 00054
A/3 Pos.
Replicate 1
I Peak. Area (A-s): 4.624
81ank Corrected Pk Height (A): 0.205
Concentration (ug/L ): 5.494
Time: 17:04
Peak Height (A); 0.205"
I
Hg2 ID: 43048 LCS '0
Seq. No.: 00055 A/3 Pos,
I
i
I
Replicate 1
eak Area (A-s): 4.241
Blank Corrected Pk Height (A): 0.194
oncentration (ug/L ): 5.190
Time: 17:06
Peak-Height (A): 0.194
Date: 09/24/9"
Date: 09/24/97.
10: 181-18-138
l"19'
Replicate 1
—Peak Area (A-s): 0.027
¦Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.024
Seq. No.: 00056
A/S Pos.: —
Time: 17:GS
Peak Height (ft;
Date: 09/24/91
0.001
ig2 ID: 181-13-13B D
Seq. No.: 00057
A/S Pos.: —
Date: 09/24/9"
¦Replicate 1
B-Naak Area (A—s): 0.020
Blank Corrected Pk Height (A): 0.001
..Concentration (ug/L ): 0.024 ;
Time: 17:09
Peak Height (A): 0.001
Hgi
ID: 181-18-13 (IS
Seq. No.: 00058 'A/S Pos.: —
Replicate 1
Peak Area (A-s): 4.447
^lank Corrected Pk Height (A): 0.197
Concentration (ug/L ): 5.273
Time: 17:10
Peak Height (A): 0.197
Date: 09/24/97
fD^.181-18-13 MS0
Seq. No.: 00059
A/S Pos.
Date: 09/24/97
Repiicate 1
JPeak Area (A-s): 0.083
Blank Corrected Pk Height (A): 0.004
concentration fng/i n 11
Tirne: 17:12
_Peak Height (A): 0.004
X
I
i
ID: 181-18-13 MSD
Seq. No.: 00060 A/S Pos.
Date: 09/24/9"
86
-------
Replicate 1
Peak Area (A-s): 5.164
Blank Corrected Pk Height (A): 0.236
Concentration (ug./L ): 6.309
Hg 2 ID i j£.V 1=6_J) ug / L
Replicate 1
Peak Area (A-s): 5.174
Blank Corrected Pk Height (A): 0.224
Concentration (ug./L ): 6.001
Hg2 ID: CCB1
Replicate 1
- Peak Area (A-s): 0.041
Blank Corrected Pk Height (A): 0.001
Concentration (ug/L ): 0.038
Time: 17:13
Peak Height (A): 0.236
Date: 09/24/97
Time: 17:20
Peak Height (A): 0.224
Date: 09/24/97
Time: 17:21
Peak Height (A): 0.001
Seq. No.: 00061 „ A/S Pos.: —
Seq. No.: 00062 A/S Pos.: —
-------
Appendix D
Particulate Matter Laboratory Analysis Data
-------
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Appendix E
Field Data Sheets
-------
Facility: WCI
Date: 08/12/97
Location: SBH/lnlet
Run Number: 1
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.30
Absolute Stack Pressure (in H20)
27.09
Stack Static Pressure (in H20)
-30.00
Average Stack Temperature (°F)
257.53
Stack Area (sq in)
14364.00
Actual Meter Volume (cu ft)
107.497
Average Meter Pressure (in H20)
0.67
Average Meter Temperature (°F)
90.61
Moisture Collected (g)
140.10
Carbon Dioxide Concentration (%V)
2.0
Oxygen Concentration (%V)
18.5
Nitrogen Concentration (%V)
79.5
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.150
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.415
Standard Metered Volume (dscf)
99.613
Standard Metered Volume (dscm)
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
0.938
Dry Molecular Weight
29.06
Wet Molecular Weight
28.37
Stack Gas Velocity (fpm)
5375.30
Stack Gas Velocity (mpm)
1638.39
Volumetric Flow Rate (acfm)
536186.52
Volumetric Flow Rate (acmm)
15184.80
Volumetric Flow Rate (dscfm)
335019^
Volumetric Flow Rate (dscmm)
^948^75
Percent Isokinetic
10CTT0'
Percent Excess Air
738.85
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/13/97
Location: BH/lnlet
Run Number: 2
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.06
Absolute Stack Pressure (in H20)
26.85
Stack Static Pressure (in H20)
-30.00
Average Stack Temperature (°F)
218.96
Stack Area (sq in)
14364.00
Actual Meter Volume (cu ft)
104.344
Average Meter Pressure (in H20)
0.58
Average Meter Temperature (°F)
78.21
Moisture Collected (g)
111.60
Carbon Dioxide Concentration (%V)
2.0
Oxygen Concentration (%V)
18.5
Nitrogen Concentration (%V)
79.5
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.150
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.408
Standard Metered Volume (dscf)
97_86X
sJiamMiZGMh*.
Standard Metered Volume (dscm)
, 2.772
Stack Moisture (%V)
5.10
Mole Fraction Dry Stack Gas
0.949
Dry Molecular Weight
29.06
Wet Molecular Weight
28.50
Stack Gas Velocity (fpm)
4821.75
Stack Gas Velocity (mpm)
1469.67
Volumetric Flow Rate (acfm)
480969.91
Volumetric Flow Rate (acmm)
13621.07
Volumetric Flow Rate (dscfm)
318534^4
Volumetric Flow Rate (dscmm)
<9020.91
Percent Isokinetic
Percent Excess Air
738.85
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/14/97
Location: BH/lnlet
Run Number: 3
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.10
Absolute Stack Pressure (in H20)
26.89
Stack Static Pressure (in H20)
-30.00
Average Stack Temperature (°F)
216.67
Stack Area (sq in)
14364.00
Actual Meter Volume (cu ft)
109.508
Average Meter Pressure (in H20)
0.61
Average Meter Temperature (°F)
80.08
Moisture Collected (g)
157.20
Carbon Dioxide Concentration (%V)
2.0
Oxygen Concentration (%V)
18.0
Nitrogen Concentration (%V)
80.0
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.150
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.430
Standard Metered Volume (dscf)
103.200
Standard Metered Volume (dscm)
r^.923
Stack Moisture (%V)
Mole Fraction Dry Stack Gas
0.933
Dry Molecular Weight
29.04
Wet Molecular Weight
28.30
Stack Gas Velocity (fpm)
5116.05
Stack Gas Velocity (mpm)
1559.37
Volumetric Flow Rate (acfrn)
510326.07
Volumetric Flow Rate (acmm)
14452.43
Volumetric Flow Rate (dscfm)
3335QfL§5
Volumetric Flow Rate (dscmm)
Percent Isokinetic
104.68
Percent Excess Air
573.98
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/15/97
Location: BH/ A-Outlet
Run Number: 1
Sample Type: Metals
Total Sampling Time (min)
120.0
Corrected Barometric Pressure (in Hg)
29.00
Absolute Stack Pressure (in H20)
28.99
Stack Static Pressure (in H20)
-0.10
Average Stack Temperature (°F)
161.50
Stack Area (sq in)
4071.50
Actual Meter Volume (cu ft)
87.194
Average Meter Pressure (in H20)
1.83
Average Meter Temperature (°F)
75.67
Moisture Collected (g)
65.30
Carbon Dioxide Concentration (%V)
0.5
Oxygen Concentration (%V)
20.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.215
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.686
Standard Metered Volume (dscf)
82t3^
Standard Metered Volume (dscm)
V 2.332
Stack Moisture (%V)
3.60
Mole Fraction Dry Stack Gas
0.964
Dry Molecular Weight
28.90
Wet Molecular Weight
28.51
Stack Gas Velocity (fpm)
3638.28
Stack Gas Velocity (mpm)
1108.95
Volumetric Flow Rate (acfm)
102869.90
Volumetric Flow Rate (acmm)
2913.28
Volumetric Flow Rate (dscfm)
81625.16
Volumetric Flow Rate (dscmm)
C. 2311.62
Percent Isokinetic
94.26
Percent Excess Air
5513.72
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/15/97
Location: BH / A-Outlet
Run Number: 2
Sample Type: Metals
Total Sampling Time (min)
120.0
Corrected Barometric Pressure (in Hg)
29.00
Absolute Stack Pressure (in H20)
28.99
Stack Static Pressure (in H20)
-0.10
Average Stack Temperature (°F)
132.08
Stack Area (sq in)
4071.50
Actual Meter Volume (cu ft)
88.117
Average Meter Pressure (in H20)
1.72
Average Meter Temperature (°F)
83.71
Moisture Collected (g)
50.60
Carbon Dioxide Concentration (%V)
0.0
Oxygen Concentration (%V)
21.0
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.215
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.683
Standard Metered Volume (dscf)
8J„976
Standard Metered Volume (dscm)
< 2.322
Stack Moisture (%V)
2.83
Mole Fraction Dry Stack Gas
0.972
Dry Molecular Weight
28.84
Wet Molecular Weight
28.53
Stack Gas Velocity (fpm)
3477.25
Stack Gas Velocity (mpm)
1059.87
Volumetric Flow Rate (acfm)
98317.05
Volumetric Flow Rate (acmm)
2784.34
Volumetric Flow Rate (dscfm)
82&50.47
Volumetric Flow Rate (dscmm)
<"2337.83
Percent Isokinetic
92.81
Percent Excess Air
-16380.66
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/16/97
Location: BH/ A-Outlet
Run Number: 3
Sample Type: Metals
Total Sampling Time (min)
120.0
Corrected Barometric Pressure (in Hg)
28.61
Absolute Stack Pressure (in H20)
28.60
Stack Static Pressure (in H20)
-0.10
Average Stack Temperature (°F)
120.42
Stack Area (sq in)
4071.50
Actual Meter Volume (cu ft)
82.506
Average Meter Pressure (in H20)
1.44
Average Meter Temperature (°F)
87,04
Moisture Collected (g)
85.50
Carbon Dioxide Concentration (%V)
0.0
Oxygen Concentration (%V)
21.5
Nitrogen Concentration (%V)
78.5
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.215
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.627
Standard Metered Volume (dscf)
75.£38
Standard Metered Volume (dscm)
2.131
Stack Moisture (%V)
5.09
Mole Fraction Dry Stack Gas
0.949
Dry Molecular Weight
28.86
Wet Molecular Weight
28.31
Stack Gas Velocity (fpm)
3174.82
Stack Gas Velocity (mpm)
967.69
Volumetric Flow Rate (acfm)
89765.96
Volumetric Flow Rate (acmm)
2542.17
Volumetric Flow Rate (dscfm)
74089.99
Volumetric Flow Rate (dscmm)
<. 2098.23
Percent Isokinetic
94,90
Percent Excess Air
-2827.83
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
:acility: WCI
Date: 08/15/97
.ocation: BH/ A-Outlet
Run Number: 1
Sample Type: Metals
Total Sampling Time (min)
120.0
Corrected Barometric Pressure (in Hg)
29.00
Absolute Stack Pressure (in H20)
28.99
Stack Static Pressure (in H20)
-0.10
Average Stack Temperature (°F)
161.50
Stack Area (sq in)
:
Actual Meter Volume (cu ft)
'87.194
Average Meter Pressure (in H20)
1.83
Average Meter Temperature (°F)
75.67
Moisture Collected (g)
65.30
Carbon Dioxide Concentration (%V)
0.5
Oxygen Concentration (%V)
20.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.215
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.686
Standard Metered Volume (dscf)
82.330
Standard Metered Volume (dscm)
2.332
Stack Moisture (%V)
3.60
Mole Fraction Dry Stack Gas
0.964
Dry Molecular Weight
28.90
Wet Molecular Weight
28.51
Stack Gas Velocity (fpm)
3638.28
Stack Gas Velocity (mpm)
1108.95
Volumetric Flow Rate (acfm)
- 234457.28
Volumetric Flow Rate (acmm)
.. 6554:87
Volumetric Flow Rate (dscfm)
- 1.83666761
Volumetric Flow Rate (dscmm)
,520TTT6
Percent Isokinetic
94.26
Percent Excess Air
5513.72
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (lb/hr)
0.00
-------
Facility: WCI
Date: 08/15/97
Location: BH/A-Outiet
Run Number: 2
Sample Type: Metals
Total Sampling Time (min) 120.0
Corrected Barometric Pressure (in Hg) 29.00
Absolute Stack Pressure (in H20) 28.99
Stack Static Pressure (in H20) -0.10
Average Stack Temperature (°F) __ 132.08
Stack Area (sq in) — - jJ4efn?8
Actual Meter Volume (cu ft) 88.117
Average Meter Pressure (in H20) 1.72
Average Meter Temperature (°F) 83.71
Moisture Collected (g) 50.60
Carbon Dioxide Concentration (%V) 0.0
Oxygen Concentration (%V) 21.0
Nitrogen Concentration (%V) 79.0
Dry Gas Meter Factor 0.9840
Nozzle Diameter (in) 0.215
Pitot Constant 0.84
Average Sampling Rate (dscfm) 0.683
Standard Metered Volume (dscf) 81.976
Standard Metered Volume (dscm) 2.322
Stack Moisture (%V) 2.83
Mole Fraction Dry Stack Gas 0.972
Dry Molecular Weight 28.84
Wet Molecular Weight 28.53
Stack Gas Velocity (fpm) 3477.25
Stack Gas Velocity (mpm) 1059.87
Volumetric Flow Rate (acfm) 221213.36
Volumetric Flow Rate (acmm) 6264.76
Volumetric Flow Rate (dscfm) 185738.56
Volumetric Flow Rate (dscmm) 5280/12
Percent Isokinetic 92.81
Percent Excess Air -16380.66
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0,00
-------
facility: WC!
Date: 08/16/97
.ocation: BH/ A-Outlet
*un Number: 3
Sample Type: Metals
Total Sampling Time (min) 120.0
Corrected Barometric Pressure (in Hg) 28.61
Absolute Stack Pressure (in H20) 28.60
Stack Static Pressure (in H20) -0.10
Xverage Stack Temperature (°F) 120^2
Stack Area (sq in) 9460.88
\ctual Meter Volume (cu ft) 82,506
Average Meter Pressure (in H20) 1.44
Average Meter Temperature (°F) 87.04
Vloisture Collected (g) 85.50
3arbon Dioxide Concentration (%V) 0.0
Dxygen Concentration (%V) 21.5
Nitrogen Concentration (%V) 78.5
Dry Gas Meter Factor 0.9840
Nozzle Diameter (in) 0.215
Pitot Constant 0.84
Average Sampling Rate (dscfm) 0.627
Standard Metered Volume (dscf) 75.238
Standard Metered Volume (dscm) 2.131
Stack Moisture (%V) 5.09
Mole Fraction Dry Stack Gas 0.949
Dry Molecular Weight 28.86
Wet Molecular Weight 28.31
Stack Gas Velocity (fpm) 3174.82
Stack Gas Velocity (mpm) 967.69
Volumetric Flow Rate (acfm) 201973.42
Volumetric Flow Rate (acmm) 5719.89
Volumetric Flow Rate (dscfm) 166702.48
Volumetric Flow Rate (dscmm) 4J2MfS
Percent Isokinetic 94.90
Percent Excess Air -2827.83
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0.00
-------
:acility: WCI
Date: 08/12/97 , j
.ocation: BH/lnlet jc_
*un Number: 1
Sample Type: Metals
Total Sampling Time (min) 240.0
Corrected Barometric Pressure (in Hg) 29.30
Absolute Stack Pressure (in H20) 27.09
Stack Static Pressure (in H20) -30.00
Werage Stack Temperature (°F) 257.53
Stack Area (sq in) - 9160.88
\ctual Meter Volume (cu ft) 107.497
\verage Meter Pressure (in H20) 0.67
Average Meter Temperature (°F) 90.61
Moisture Collected (g) " 140.10
Carbon Dioxide Concentration (%V) 2.0
Dxygen Concentration (%V) 18.5
Mitrogen Concentration (%V) 79.5
3ry Gas Meter Factor 0.9840
Mozzle Diameter (in) 0.150
3itot Constant 0.84
Average Sampling Rate (dscfm) 0.415
Standard Metered Volume (dscf) 99.613
Standard Metered Volume (dscm) 2.821
Stack Moisture (%V) 6.22
Vlole Fraction Dry Stack Gas 0.938
Dry Molecular Weight 29.06
/Vet Molecular Weight 28.37
Stack Gas Velocity (fpm) 5375.30
Stack Gas Velocity (mpm) 1638.39
Volumetric Flow Rate (acfm) 341962.03
Volumetric Flow Rate (acmm) 9684.36
Volumetric Flow Rate (dscfm) 213664.28
Volumetric Flow Rate (dscmm) 6050.97
Percent Isokinetic 100.70
Percent Excess Air 738.85
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0.00
-------
Facility: WCI
Date: 08/13/97 \
Location: BH/lnlet SfwM b^hx*<-
Run Number: 2
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.06
Absolute Stack Pressure (in H20)
26.85
Stack Static Pressure (in H20)
-30.00
Average Stack Temperature (CF)
218.96
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
104.344
Average Meter Pressure (in H20)
0.58
Average Meter Temperature (CF)
78.21
Moisture Collected (g)
111.60
Carbon Dioxide Concentration (%V)
2.0
Oxygen Concentration (%V)
18.5
Nitrogen Concentration (%V)
79.5
Dry Gas Meter Factor
0.9840
Nozzle Diameter (in)
0.150
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.408
Standard Metered Volume (dscf)
97.867
Standard Metered Volume (dscm)
2.772
Stack Moisture (%V)
5.10
Mole Fraction Dry Stack Gas
0.949
Dry Molecular Weight
29.06
Wet Molecular Weight
28.50
Stack Gas Velocity (fpm)
4821.75
Stack Gas Velocity (mpm)
1469.67
Volumetric Flow Rate (acfm)
306746.70
Volumetric Flow Rate (acmm)
8687.07
Volumetric Flow Rate (dscfm)
203150.98
Volumetric Flow Rate (dscmm)
5753.24
Percent Isokinetic
104.06
Percent Excess Air
738.85
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
-acility: WCI
Date: 08/14/97
vocation: BH/lnlet
Run Number: 3
Sample Type: Metals
Total Sampling Time (min) 240.0
Corrected Barometric Pressure (in Hg) 29.10
Absolute Stack Pressure (in H20) 26.89
Stack Static Pressure (in H20) -30.00
Average Stack Temperature (°F) 216.67
Stack Area (sq in) 9160.88
Actual Meter Volume (cu ft) 109.508
Average Meter Pressure (in H20) 0.61
Average Meter Temperature (°F) 80,08
Moisture Collected (g) 157.20
Carbon Dioxide Concentration (%V) 2.0
Oxygen Concentration (%V) 18.0
Nitrogen Concentration (%V) 80.0
Dry Gas Meter Factor 0.9840
Nozzle Diameter (in) 0.150
Pitot Constant 0.84
Average Sampling Rate (dscfm) 0.430
Standard Metered Volume (dscf) 103.200
Standard Metered Volume (dscm) 2.923
Stack Moisture (%V) 6.70
Mole Fraction Dry Stack Gas 0.933
Dry Molecular Weight 29.04
Wet Molecular Weight 28.30
Stack Gas Velocity (fpm) 5116.05
Stack Gas Velocity (mpm) 1559.37
Volumetric Flow Rate (acfm) 325469.09
Volumetric Flow Rate (acmm) 9217.28
Volumetric Flow Rate (dscfm) 212954.17
Volumetric Flow Rate (dscmm) 6030.86
Percent Isokinetic 104.68
Percent Excess Air 573.98
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0.00
-------
-acility: WCI
Date: 08/12/97 _ . / . M±
vocation: Stack b°jh«n. o- e
Run Number: 1
Sample Type: Dioxin
Total Sampling Time (min) 240,0
Corrected Barometric Pressure (in Hg) 29,26
Absolute Stack Pressure (in H20) 29.26
Stack Static Pressure (in H20) -0.04
Average Stack Temperature (°F) 250.19
Stack Area (sq in) - 9160.88
Actual Meter Volume (cu ft) 228.017
Average Meter Pressure (in H20) 2.63
Average Meter Temperature (°F) 99,53
Moisture Collected (g) 341.40
Carbon Dioxide Concentration (%V) 0.5
Oxygen Concentration (%V) 20.5
Nitrogen Concentration (%V) 79.0
Dry Gas Meter Factor 0.9960
Nozzle Diameter (in) 0.193
Pitot Constant 0.84
Average Sampling Rate (dscfm) 0.878
Standard Metered Volume (dscf) 210.832
Standard Metered Volume (dscm) 5.971
Stack Moisture (%V) 7.09
Mole Fraction Dry Stack Gas 0.929
Dry Molecular Weight 28,90
Wet Molecular Weight 28.13
Stack Gas Velocity (fpm) 6452.52
Stack Gas Velocity (mpm) 1966.73
Volumetric Flow Rate (acfm) 410491.39
Volumetric Flow Rate (acmm) 11625.12
Volumetric Flow Rate (dscfm) 277213.98
Volumetric Flow Rate (dscmm) 7850.70
Percent Isokinetic 99.23
Percent Excess Air 5513.72
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0.00
-------
Facility: WCI
Date: 08/13/97
Location: Stack
Run Numb 2
Sample Ty Dioxin
Total Sampling Time (min) 120,0
Corrected Barometric Pressure (in Hg) 29.00
Absolute Stack Pressure (in H20) 29.04
Stack Static Pressure (in H20) 0.60
Average Stack Temperature (°F) 245.69
Stack Area (sq in) 9160.88
Actual Meter Volume (cu ft) 107.856
Average Meter Pressure (in H20) 2.27
Average Meter Temperature (°F) 79.38
Moisture Collected (g) 146.70
Carbon Dioxide Concentration (%V) 0.5
Oxygen Concentration (%V) 20.5
Nitrogen Concentration (%V) 79.0
Dry Gas Meter Factor 0.9960
Nozzle Diameter (in) 0.193
Pitot Constant 0.84
Average Sampling Rate (dscfm) 0.854
Standard Metered Volume (dscf) 102.513
Standard Metered Volume (dscm) 2.903
Stack Moisture (%V) 6.32
Mole Fraction Dry Stack Gas 0.937
Dry Molecular Weight 28.90
Wet Molecular Weight 28.21
Stack Gas Velocity (fpm) 6188.65
Stack Gas Velocity (mpm) 1886.30
Volumetric Flow Rate (acfm) 393704.79
Volumetric Flow Rate (acmm) 11149.72
Volumetric Flow Rate (dscfm) 267835.10
Volumetric Flow Rate (dscmm) 7585.09
Percent Isokinetic 99.88
Percent Excess Air 5513.72
Concentration (g/dscm) 0.00
Concentration (kg/hr) 0.00
Concentration (ppmv) 0.00
Emissions (Ib/hr) 0.00
-------
Facility: WCI
Date: 08/13/97 , / j
Location: Stack
Run Number: 3
Sample Type: Dioxin
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.00
Absolute Stack Pressure (in H20)
29.04
Stack Static Pressure (in H20)
0.60
Average Stack Temperature (°F)
233.63
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
224.147
Average Meter Pressure (in H20)
2.53
Average Meter Temperature (°F)
81.05
Moisture Collected (g)
358.40
Carbon Dioxide Concentration (%V)
3.5
Oxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9960
Nozzle Diameter (in)
0.193
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.886
Standard Metered Volume (dscf)
212.543
Standard Metered Volume (dscm)
6.019
Stack Moisture (%V)
7.37
Mole Fraction Dry Stack Gas
0.926
Dry Molecular Weight
29.26
Wet Molecular Weight
28.43
Stack Gas Velocity (fpm)
6249.71
Stack Gas Velocity (mpm)
1904.91
Volumetric Flow Rate (acfm)
397589.40
Volumetric Flow Rate (acmm)
11259.73
Volumetric Flow Rate (dscfm)
272116.18
Volumetric Flow Rate (dscmm)
7706.33
Percent Isokinetic
101.91
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCi
Date: 08/14/97 ^ ,/ j _ hi
Location: Stack 3Tw^
Run Numb 4
Sample TV Dioxin
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.04
Absolute Stack Pressure (in H20)
29.08
Stack Static Pressure (in H20)
0.60
Average Stack Temperature (°F)
235.66
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
222.820
Average Meter Pressure (in H20)
2.51
Average Meter Temperature (°F)
89.59
Moisture Collected (g)
310.80
Carbon Dioxide Concentration (%V)
3.5
Oxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9960
Nozzle Diameter (in)
0.193
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.868
Standard Metered Volume (dscf)
208.287
Standard Metered Volume (dscm)
5.899
Stack Moisture (%V)
6.57
Mole Fraction Dry Stack Gas
0.934
Dry Molecular Weight
29.26
Wet Molecular Weight
28.52
Stack Gas Velocity (fpm)
6245.02
Stack Gas Velocity (mpm)
1903.48
Volumetric Flow Rate (acfm)
397290.73
Volumetric Flow Rate (acmm)
11251.27
Volumetric Flow Rate (dscfm)
273811.90
Volumetric Flow Rate (dscmm)
7754.35
Percent Isokinetic
99.25
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/15/97 ». / / hS
Location: Stack J?W
Run Number: 5
Sample Type: Dioxin
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
28.96
Absolute Stack Pressure (in H20)
29.00
Stack Static Pressure (in H20)
0.60
Average Stack Temperature (°F)
232.06
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
222.592
Average Meter Pressure (in H20)
2.41
Average Meter Temperature (°F)
86.34
Moisture Collected (g)
297.40
Carbon Dioxide Concentration (%V)
3.5
Oxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9960
Nozzle Diameter (in)
0.193
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.869
Standard Metered Volume (dscf)
208.642
Standard Metered Volume (dscm)
5.909
Stack Moisture (%V)
6.30
Mole Fraction Dry Stack Gas
0.937
Dry Molecular Weight
29.26
Wet Molecular Weight
28.55
Stack Gas Velocity (fpm)
6112.46
Stack Gas Velocity (mpm)
1863.08
Volumetric Flow Rate (acfm)
388858.13
Volumetric Flow Rate (acmm)
11012.46
Volumetric Flow Rate (dscfm)
269443.87
Volumetric Flow Rate (dscmm)
7630.65
Percent Isokinetic
101.03
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
:acility: WCI
)ate: 08/12/97
r l I
.ocation: Stack Stwi/
*un Number: 1 /
ample Type: Metals
rotal Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.26
Absolute Stack Pressure (in H20)
29.23
Stack Static Pressure (in H20)
-0.40
Werage Stack Temperature (°F)
246.09
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
224.695
Werage Meter Pressure (in H20)
2.77
Werage Meter Temperature (°F)
99.06
Jloisture Collected (g)
368.50
Carbon Dioxide Concentration (%V)
3.5
Dxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9880
Nozzle Diameter (in)
0.193
3itot Constant
0.84
Werage Sampling Rate (dscfm)
0.860
Standard Metered Volume (dscf)
206.501
Standard Metered Volume (dscm)
5.848
Stack Moisture (%V)
7.76
dole Fraction Dry Stack Gas
0.922
Dry Molecular Weight
29.26
Net Molecular Weight
28.39
Stack Gas Velocity (fpm)
6473.79
Stack Gas Velocity (mpm)
1973.21
/olumetric Flow Rate (acfm)
411844.44
/olumetric Flow Rate (acmm)
11663.43
/olumetric Flow Rate (dscfm)
277479.87
/olumetric Flow Rate (dscmm)
7858.23
Percent Isokinetic
97.10
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
Facility: WCI
Date: 08/13/97 jj.
Location: Stack wl
Run Number: 2
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure (in Hg)
29.00
Absolute Stack Pressure (in H20)
29.04
Stack Static Pressure (in H20)
0.60
Average Stack Temperature (°F)
238.50
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
213.980
Average Meter Pressure (in H20)
2.55
Average Meter Temperature (°F)
77.34
Moisture Collected (g)
341.00
Carbon Dioxide Concentration (%V)
3.5
Oxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9880
Nozzle Diameter (in)
0.193
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.844
Standard Metered Volume (dscf)
202.664
Standard Metered Volume (dscm)
5.739
Stack Moisture (%V)
7.35
Mole Fraction Dry Stack Gas
0.926
Dry Molecular Weight
29.26
Wet Molecular Weight
28.43
Stack Gas Velocity (fpm)
6326.64
Stack Gas Velocity (mpm)
1928.36
Volumetric Flow Rate (acfm)
402483.68
Volumetric Flow Rate (acmm)
11398.34
Volumetric Flow Rate (dscfm)
273586.26
Volumetric Flow Rate (dscmm)
7747.96
Percent Isokinetic
96.65
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
:acility: WCI
Date: 08/14/97 „ , /
_ocation: Stack Shawl
Run Number: 3
Sample Type: Metals
Total Sampling Time (min)
240.0
Corrected Barometric Pressure {in Hg)
29.04
Absolute Stack Pressure (in H20)
29.08
Stack Static Pressure (in H20)
0.60
Average Stack Temperature (°F)
230.91
Stack Area (sq in)
9160.88
Actual Meter Volume (cu ft)
209.885
Average Meter Pressure (in H20)
2.48
Average Meter Temperature (°F)
86.61
Moisture Collected (g)
283.00
3arbon Dioxide Concentration (%V)
3.5
Oxygen Concentration (%V)
17.5
Nitrogen Concentration (%V)
79.0
Dry Gas Meter Factor
0.9880
Nozzle Diameter (in)
0.193
Pitot Constant
0.84
Average Sampling Rate (dscfm)
0.815
Standard Metered Volume (dscf)
195.672
Standard Metered Volume (dscm)
5.541
Stack Moisture (%V)
6.38
Mole Fraction Dry Stack Gas
0.936
Dry Molecular Weight
29.26
Wet Molecular Weight
28.54
Stack Gas Velocity (fpm)
6224.21
Stack Gas Velocity (mpm)
1897.14
Volumetric Flow Rate (acfm)
395967.06
Volumetric Flow Rate (acmm)
11213.79
Volumetric Flow Rate (dscfm)
275333.02
Volumetric Flow Rate (dscmm)
7797.43
Percent Isokinetic
92.72
Percent Excess Air
519.01
Concentration (g/dscm)
0.00
Concentration (kg/hr)
0.00
Concentration (ppmv)
0.00
Emissions (Ib/hr)
0.00
-------
%ERG
Traverse Point Location Fen m
Eastern Research Group, Inc.
Plant
yoo*Av£ro»JtJ
Sample Ports
iraormation
Number 1 I.D, (in)
Date
sltflq*
j
Sampling Location
B P*c"r4tou'b ( -ft Oi'Tlfi-T.
"
Total Duct Depth (Distance A)
£> '
U
A
(Inside Far Wall to Outside of Nipple/Port)
Nipple/Port Length (Distance B)
3"
(Inside Near Wall to Outside End of Nipple/Port)
Stack Depth (Dist A - Dist B) | 5 y "
Stack Width (If rectangular) —
Nearest Upstream Disturbance '
Nearest Downstream Disturbance | i £1
Schematic of Sampling Location
(Cross Section of Duct)
1
2 • f • '3 f- 4
• ¦
Traverse
Point
Number
Percent Fraction
of Stack ID
Stack
ID
(in)
Product of Columns
2 & 3
(to nearest 1/8 inch)
Distance
B
(in)
Traverse Point Location
from Outside of Nipple
(sum of columns 4 & 5)
A -I
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*ERG
Eastern fios«c*ch ©
-------
*ERG
Eastern Research Group. Inc.
Preliminary Velocity Traverse Form and Cyclonic Flow Check
Plant
O/CT
Date Vj//n . . /
Location ! Sftaid fatsb'K Odfaft
Stack ID (in)
Barometric Pressure (in Hg)
Ambient Temperature (°F)
Static Pressure (in H20)
Operators
Checked By |
Schematic of Traverse Point Layout
(Cross Section of Duct)
Traverse
Point
Number
Velocity
Head
AP. fin H20)
Stack
Temperature
ts, m
Cyclonic
Row
Angle (* °)
Traverse
Point
Number
Velocity
Head
AP. (in H20)
Stack
Temperature
Ts, f F)
Cyclonic
Row
Anqle (± °)
ft / 1 i
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-------
Eastern Resennch Group, Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
XAD Trap Number
(
Meter Box Number
fi-Vi
fh-M
dvHd ShfoJ, 41.
1
Date
t-t/j-n
Filter Heater Setting (°F)
Meter delta H @
7. 7(;n>
Operator
Probe Length & Type
DGM Factor (Y)
Ma
Sampling Location
frjcr
Probe Heater Setting (°F)
Nozzle Type & ID (in.)
(/9'<
Sample Type
TpLTaJ
Minimum Sample Volume (ft3)
Ambjfnt Temperature (°F)
Q*ci*
Run Number
/' -
Initial Leak Check
Xifcumed Moisture (% H20)
Static Pressure (±) (in. H20)
-.0'/
Final Leak Check (><0/
(0''
K-Factor
Barometric Pressure (in, H20)
Diagram of Duct
Read and record all data every minutes
Gas
Meter
Reading.
(Vm),ft3)
velocity
Head
((delta Ps)
in.H20)
Orifice Pressure
Differentia
(delta H, in,H20)
Adsorbent
Trap
Temp.
(°F)
Dry Gas Meter
Impmger
Exit
Temp.
(°F)
Sampling
Time
gjcl
Clock
Time
(24hr)
Stack
Probe
Temp.
F)
Pump
Vacuum
(in.Hg)
Traverse
Point -
Number
nlet
(Tm in)
Outlet
(Tm out)
Desired
Actual
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Comments:
-------
Page of
Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Numbef
/j >-y
Gas
Meter
Reading
Velocity
Head
(delta Ps)
in.H2Q)
7,-r f],
Stack
Ts
m,
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
w
tea
Probe
Temp.
If)
Filter
Temp,
Adsorbent
Trap
Temp.
rn
Dry Gas Meter
Inlet
(T?In)
Outlet
(Tm out)
Impinger
Exit
Temp.
VT
Pump
Vacuum
(in.Hg)
s
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Comments:
-------
Eastern Research Group, Inc.
MODIFIED METHOD 5 DATASHEET
Page 1 of
Plant
V'
XAD Trap Number
Meter Box Number
OMit SfwJ&A
X
Date
Filter Heater Setting (°F)
Meter delta H @
/- 70$
Operator
Probe Length & Type
n
DGM Factor (Y)
'/fe^jmed Moisture (% H20)
Static Pressure (±) (in. H20)
/*/£
Final Leak Check
K-Factor
Barometric Pressure (in. H20)
fA.oh
Diagram of Duct
Read and record all data nverv 7 minutes
T raverse
Point
Number
23
Sampling
Time
W
7T
Clock
Time
(24hr)
1WV
Gas
Meter
Reading
((Vm),ft3)
, L
Velocity
Head
((delta Ps),
in,H20)
79 rp
Stack
Orifice Pressure
Differential
(delta H, in,H20)
Desired Auual
sz:
Probe
Temp.
CF)
I if"
Filter
Temp.
CF)
JJT
Adsorbent
Trap
Temp.
fF)
I51
Dry Gas Meter
Inlet Outlet
(Tmin) (Tmout)
Impinger
Exit
Temp.
(*F)
Pump
Vacuum
(in.Hg)
7Wo
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Page of
Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Number
Sampling
Time
(min)
Clock
, Time
<24hr)
Gas
Meter
Reading
((Vm),tt3)
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
CF)
Orifice h
Differ
(delta H,
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IH.H20)
Actual
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Temp,
(°F)
Filter
Temp.
CF)c
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CF)
Dry Ga
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(Tm in)
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(Tm out)
Impinger
Exit
Temp.
CF)
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Vacuum
(in.Hg)
;
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Comments:
-------
Eastern Research Group, Inc.
mv*«5T
MODIFIED METHOD r> DATA SHEET
Run
Page 1 of
Plant
XAD Trap Number
Meter Box Number
A-9f
/ //.
U'l
V 1
Date
fan-?-?
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t&rtp
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Sample Type
19 MM J
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W
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(24hrL_
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Run Number
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Sample Type
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Dry Gas Meter
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Clock
Time
Stack
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Comments:
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Number
Sampling
Time
(min)
O
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Clock
Time
(24hr)
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Run Number
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Sample Type
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Page,
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Dry Gas Meter
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.m out)
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Eastern Research Group, Inc.
MODIFIED METHOD 5 DATASHEET
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Page 1 of
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" v-7
7FW
Plant
Date
Operator
Sampling Location
Sample Type
Run Number
Static Pressure (t) (in. H2Q)
H
WrcF
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XAD Trap Number
Filter Heater Setting (°F)
Probe Length & Type
(V9,
Probe Heater Setting (°F)
Minimum Sample Volume (ft3)
Initial Leak Check
Final Leak Check
7^
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Meter delta H @
PGM Factor (Y)
Nozzle Type & ID (in.)
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Assumed Moisture (% H2Q)
K-Factor
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Schematic of Traverse Point Layout
Read and record all data every ' / AT minutes
Diagram of Duct
Gas
Meter
Reading
((Vm),ft3
Velocity
Head
((delta Ps),
in.H20)
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
Adsorbent
Trap
Temp.
(°F)
Dry Gas Meter
Impinger
Exit
Temp.
Clock
Traverse
Point
Number
Sampling
Time
(min)
Stack
Probe
Temp.
(°F)
Pump
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(in.Hg)
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Outlet
(Tm out)
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Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Number
Sampling
Time
mini
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Clock
Time
(24hf)
Gas
Meter
Reading
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in,H20)
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Ts
°F)
of
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Probe
Temp.
(°F)
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f)
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mpinger
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Eastern Research Group. Inc.
MODIFIED METHOD 5 DATA SHEET
mm
Run
Page 1 of /
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Plant
f
XAD Trap Number
Meter Box Number
5fhJr\J
Date
Filter Heater Setting fF)
Weter delta H @
/, /
Operator
Mka
Probe Length & Type
OGM Factor (Y)
x rxp
Sampling Location
ffiicA
Probe Heater Setting (*F)
Nozzle Type & ID (in.)
. /?1
Sample Type
Minimum Sample Volume (ft3)
Ambient Temperature (°F)
Run Number
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Final Leak Check £>0
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K-Factor
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Velocity
Head
((delta Ps)
in.H20)
Gas
Meter
Reading
((Vm5,ft3)
Orifice Pressure
Differentia
(delta H, in.H20)
Desired Actual
Adsorbent
Trap
Temp
(°F)
Dry Gas Meter
Impinger
Exit
Temp.
F)
Sampling
Time
min)
Clock
Time
(24hr)
Stack
Ts
(°F)
Probe
Temp.
(°F
Filter
Temp.
(°F)
Traverse
Point
Number
Pump
Vacuum
in.Hg)
Inlet
(Tm in)
Outlet
(Tm out)
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Location
Run Number
1
Date
Sample Type
Operator
Page.
of
Traverse
Point
Number
Sampling
Time
FA
Clock
Tim
mdlL
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Gas
Meter
Reading
71,L~>
Velocity
Head
((delta Ps),
in.H2Q)
Stack
Ts
*F)
Orifice Pressure
Differential
(delta H, in.M20)
Desired Actual
Probe
Adsorbent
Trap
Temp.
(°F)
Dry Gas Meter
Inlet
JTffiM.
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Comments:
-------
Eastern Research Group, Inc.
MODIFIED METHOD 5 DATASHEET
Run
Page 1 of
Plant
WC1
XAD Trap Number
Meter Box Number
oUtyf
1
? h .
Date
Filter Heater Setting CF)
Meter delta H @
f, 7IS'
Operator
Probe Length & Type
fl'Z/fO
DGM Factor (Y)
Sampling Location
Probe Heater Setting (°F)
\t$bh£
Nozzle Type & ID (in.)
Sample Type
M<.h7i
Minimum Sample Volume (ft3)
Ambient Temperature (°F)
Run Number
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Number
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Time
(mtn)
jtz
tt
Clock
Time
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Gas
Meter
Reading
((Vm),ft3)
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
CF)
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
Probe
Temp,
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Filter
Temp.
CF)
Adsorbent
Trap
Temp.
CF)
Dry Gas Meter
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Page of
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7r
Date
%'&¦ 77
Sample Type
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Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
Gas
Meter
Reading
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Velocity
Head
((delta Ps),
in,H20)
Stack
Ts
CF)
Orifice F
Differ
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ential
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Filter
Temp,
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Temp.
CF)
Dry Ga
Inlet
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-------
Eastern Research Croup, Inc.
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
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XAD Trap Number
Meter Box Number
-
/Zkl/l7
Date
7
Filter Heater Setting (°F)
Meter delta H @
y.-fzsi
Operator
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DGM Factor (Y)
L
Sampling Location
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Point
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Time
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Run Number
Date
Sample Type
Operator
Page of.
Traverse
Point
Number
Sampling
Time
(min)
f £
Clock
Time
(24hr)
Gas
Meter
Reading
((Vm),ft3)
Velocity
Head
((delta Ps),
in.H2Q]_
Stack
Ts
(°F)
JW
Orifice Pressure
Differentiel
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t
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2zl
Filter
Temp.
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Trap
Temp,
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Dry Gas Meter
Inlet
(Tm in)
Outlet
(Tm out)
W—
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Exit
Temp.
Pump
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Comments:
-------
Eastern Research Group, Inc.
MODIFIED METHOD 5 DATA SHEET
V/
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3-72f
Run
/
Page 1 of
iQ
Plant VoJijc o W(J i
(tf-«V
MB=3P«p Number
Meter Box Number
rl-32
« 1 '
} -
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Date
stfoh*
Filter Heater Setting (°F)
1<>o
Meter delta H @
tsz s
Operator
Probe Length & Type
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DGM Factor (Y)
Sampling Location
Probe Heater Setting (°F)
lSo
Nozzle Type & ID (in.)
,iSo
Sample Type
La
Minimum Sample Volume (ft3)
t/jA
Ambient Temperature (°F)
>S°r
Run Number
I
Initial Leak Check
to"
Assumed Moisture (% H20)
Static Pressure (±) (in. H20)
-3 4,0
Final Leak Check
K-Factor
«^'o>
Barometric Pressure (in. H20)
aq.30
1 i) l|f o. Diagram of Duet
Read and record all data every
minutes
Gas
Meter
Reading,ir-a
EfVm),ft3)*
ate
Velocity
Head
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in.H20)
Orifice Pressure
Differential
delta H, iri.H20
Desired Actual
Adsorbent
Trap
Temp.
F)
Dry Gas Meter
Impinger
Exit
Temp
CF)
Traverse
Point
Number
Sampling
Time
(mln
Clock
Probe
Pump
Vacuum
in.Hg)
nlet
(Tm in)
Outlet
Tm out)
\~i! So
1h
M
S
'WfW
2
5
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Comments:
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Location
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fYl&j-cii £
Run Number
Operator
Page J of t3-
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24 hr)
q» n
mre
3as
Meter
Reading
Velocity
Head
((delta Ps),
in.H20)
I *27.
Stack
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
U.
HI
Probe
Temp.
m
Filter
Temp,
XE
Adsorbent
Trap
Temp,
rp
—^
Dry Gas Meter
Inlet Outlet
(Tmin) (Tmout)
Impinger
Exit
Temp,
(°F)
Pump
Vacuum
(in.Hg)
~^7f
'«p
m
a
m
I
fy
32:
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fir ,
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Mi
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Z> '2r
tft 2<*
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Comments:
-------
%
-"vi
Eastern teieart^Group, Inc.
jg*?*
MODIFIED METHOD 5 DATA SHEET
>4*1 " IV) f-J! f Q
[Pagefl^ ^
Plant x' " \Jl)tUfliftfl
<01 iMdS/
XAD Trap Number
Meter Box Number
fir
/' " '\ ?J
Date / .P7
p/ii?-)?
Filter Heater Setting (°F)
246
Meter delta H @
1 a'Jd
Operator
Probe Length & Type
ft'A-Mm
DGM Factor (Y)
Sampling Location
Probe Heater Setting ("F)
Nozzle Type & ID (in.)
.16#
Sample Type
fVyr'sLOlj^r
Minimum Sample Volume (ft3)
AVA
Ambient Temperature (°F)
Run Number
s
Initial Leak Check
a DIS$l/
Assumed Moisture (% H20)
Static Pressure (±) (in. H20)
m— "%Q
Final Leak Check
K-Factor
Barometric Pressure (in. H20)
"zn>o\p
Diagram of Duct
Read and record all data every.
minutes
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
iUoi
its
Gas .
Meter
Reading
w
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
(°F)
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
12
zr
Probe
Temp.
(°F)
m.
Filter
Temp.
(•F)
Adsorbent
Trap
Temp.
(°F)
SE
Dry Gas Meter
Inlet
(Tm in)
Outlet
(Tm out)
impinger
Exit
Temp.
CF)
fib
u
Jffi
J1L
&
4£
125
-fh
U-
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&
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35
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lik
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3&H.
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i
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J2££
Uoo
JS*
Comments:
-------
Plant
jmvHtnOh
Location
Run Number
3-
Date
' Mnjai
Sample Type
Operator
2-W
Page of
Dry Gas Meter
Impmger
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
Adsorbent
Trap
Temp
m
Gas
Meter
Reading
((Vm),ft3)
Velocity
Head
((delta Ps),
in.H2Q)
Pump
Vacuum
('"•Hg)
Probe
Temp
m
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
24hr)
Stack
Inlet Outlet
(Tmin) . (Tmout)
1U,{
W
(MUZ
m
1
| o 7 k S
pi nfli
Comments;
: (2) tbiiM fct H''^0
W.Cdn.vy- (mor}
v r*it\~?
^ Q?)t O I I £k* (Kir £4/5w4"* UjP
-------
Eastern Research Group, Inc.
(7, syo
MODIFIED METHOD 5 DATASHEET
0^[%7e
Page 1 of
Plant AftHMt*
f4f}m
%AD Trap Number
Meter Box Number
Date / 1
Filter Heater Setting (°F)
Meter delta H @
Operator
4?i UJ
Probe Length & Type
DGM Factor (Y)
Sampling Location
tir m*
Probe Heater Setting (°F)
Nozzle Type & ID (in.)
a
Sample Type
toft (p
Minimum Sample Volume (ft3)
Ambient Temperature (°F)
/
Run Number
Initial Leak Check
DsDopm"
Assumed Moisture (% H20)
Static Pressure (±) (in. H20)
~>fO
Final Leak Check
K-Factor
Barometric Pressure (in. H20)
Diagram of Duct
Read and record all data every
Velocity
Head
((delta Ps)
in.H20)
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
Adsorbent
Trap
Temp.
(°F)
Dry Gas Meter
Impinger
Exit
Temp
(*F>
Gas
Meter
Reading
«Vm?Tft3)
Sampling
Time
(min)
Clock
Time
(24hr
Stack
Ts
(°F)
Probe
Temp.
(°F)
Pump
Vacuum
(in.Hg)
Traverse
Point
Number
Outlet
(Tm out)
1
I
WW
m
i
M
4
£
2±c3
imj-m
Comments:
-------
Page jL. of.
Location
# J- Run Number
Sample Type
Operator
Orifice Pressure
Differential
(delta H, in.H20)
Adsorbent
Trap
Temp
m
Dry Gas Meter
Impinger
Exit
Temp.
CO
Gas
Meter
Reading
Velocity
Head
Probe
Temp.
m
Pump
Vacuum
(in.Hg)
Traverse
Point
Number
Sampling
Time
min
Clock
Time
Inlet Outlet
(Tmin) (Tmout)
{(delta Ps),
in.H2Q)
Desired
Actual
i
wnTu
ao%Khnc)
ivfjr
m
TUqv
Emm?
Comments:
tsuh <# ¦
-------
Eastern Research Group, Inc.
v,
MODIFIED METHOD 5 DATA SHEET
Run
Page 1 of
Plant
Yo o >'«6rSbu> J S
^AQ Trap Number f \ ft—
J* %
Meter Box Number
A -3C
fallen*. f\
Date
8 Iisfo*
Filter Heater Setting (°F)
2Sq
Meter delta H @
1-823
Operator
ivwvl (V)
Probe Length & Type
S
DGM Factor (Y)
Sampling Location fWdoJ-*
e A oom+ ¦
Probe Heater Setting (°F)
t£Q
Nozzle Type & ID (in.)
."LIS
Sample Type
Minimum Sample Volume (ft3)
Ambient Temperature (°F)
TO'
Run Number
1
Initial Leak Check
Assumed Moisture (% H20)
s*%
Static Pressure (±) (in. H20)
- o. i " 4<3
Final Leak Check
K-Factor
Barometric Pressure (in. H20)
m oo
Diagram of Duct
Read and record alt data every.
minutes
Traverse
Point
Number
Sampling
Time
(min)
£L
Clock
Time
(24hr)
\V-C€>
Gas
Meter
Reading
„((Vm).ft3)
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
(°F)
Orifice Pressure
Differential
(delta H, in.H20)
Desired Actual
Probe
Temp.
(°F)
W7
_ly |
Filter
Temp.
(°F)
S3
Adsorbent
Trap
Temp.
(°F)
Dry Gas Meter
Inlet
(Tm in)
Outlet
(Tm out)
Impinger
Exit
Temp.
(°F)
Pump
Vacuum
(in.Hg)
r if
Jh
40-
&IT7
&
-3
£
h
m
9
S*(-ti
pff?
sr
m
u.
3^7
53
a
^21
72:
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#-
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m
71?
till
SEa.
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His
ift
Mi
UflLXl*
1.^
dAh
am
iT
&
IT
77,r-
jj£.
t
_S5l
tx
-------
Page of
Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
Gas
Meter
Reading
«Vm),ft3)
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
CF)
Orifice F
Differ
(delta H,
Desired
'ressure
ential
in,H20)
Actual
Probe
Temp.
(°F)
Filter
Temp.
(°F)
Adsorbent
Trap
Temp.
CF)
Dry Ga
Inlet
(Tm in)
s Meter
Outlet
(Tm out)
Impinger
Exit
Temp.
(*F)
Pump
Vacuum
(in.Hg)
Comments:
-------
i-i/ rv
Oa- vlo
Eajtem Research Group, Inc.
MODIFIED METHOD 5 DATA SHEET
o
jt
LS - / V
>1 */»
Run
Page 1 of
Sz.
Plant
XAD TraftNumber
Meter Box Number
&^U fi
Date J J
7
Filter Heater Setting (°F)
Meter delta H @
Operator
yy,,VU?t/lDtiU.
Probe Length & Type
DGM Factor (Y)
Sampling Location %
A-nu-b
Probe Heater Setting (°F)
O-CD
Nozzle Type & ID (in.)
Sample Type
Minimum Sample Volume (ft3)
Ambient Temperature (*F)
"~7p'
Run Number
3-
Initial Leak Check
.OjL&lW
Assumed Moisture {% H20)
Static Pressure (±) (in. H20)
— dA^bi
Final Leak Check
K-Factor
/Aj&
Barometric Pressure (in. H20)
Diagram of Duct
minutes
Read arid record all data every /fi
Gas
Meter
Reading
•^((Vm),ft3)
Velocity
Head
((delta Ps),
in.H20)
Orifice Pressure
Differentia
delta H. in.H20
Adsorbent
Trap
Temp,
(°F)
Dry Gas
Meter
Impinger
Exit
Temp
(*F)
Traverse
Point
Number
Sampling
Time
QSiDl
Clock
Time
QM
Stack
Ts
CF)
Probe
Temp.
CF)
Pump
Vacuum
(in.Hg)
Inlet
(Tm in)
Outlet
(Tm out)
Desired
Actual
t
$
I
, <£*'
Comments:
-------
Page of
Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
Gas
Meter
Reading
((Vm),ft3)
Velocity
Head
{(delta Ps),
in,H20)
Stack
Ts
CF)
Orifice F
Differ
(delta H,
Desired
'ressure
ential
in.H20)
Actual
Probe
Temp.
CF)
Filter
Temp.
Cf)
Adsorbent
Trap
Temp.
CF)
Dry Ga
Inlet
(Tm in)
s Meter
Outlet
(Tm out)'
Impinger
Exit
Temp.
CF)
Pump
Vacuum
(in.Hg)
Comments:
-------
MODIFIED METHOD 5 DATA SHEET
Run
Plant
4k-
-------
Page of
Plant
Location
Run Number
Date
Sample Type
Operator
Traverse
Point
Number
Sampling
Time
(min)
Clock
Time
(24hr)
Gas
Meter
Reading
((Vm),ft3)
Velocity
Head
((delta Ps),
in.H20)
Stack
Ts
(°F)
Orifice F
Differ
(delta H,
Desired
'ressure
ential
in.H20)
Actual
Probe
Temp.
(°F)
Filter
Temp.
(°F)
Adsorbent
Trap
Temp.
m
Dry Ga
Inlet
(Tm in)
s Meter
Outlet
(Tm out)
Impinger
Exit
Temp.
(°F)
Pump
Vacuum
(in.Hg)
Comments:
-------
CNk7 !
K-FACTOR CALCULATION FORM
Plant
Yod
Operator
mok-[C GWa-A
Date
Used for runs
Location/Sampling Train
C„ (S-typc: 0.84; Std: 0.99)
Pb (barometric pressure at location)
Dn (nozzle diameter, Inches)
«\°[3
Bw (moisture in gas stream, fractional percent)
i o $
Pm (barometric pressure at meter, Hg) =
(Average AH / 13.6) + Pb
AH@ (pressure differential of orifice in meterbox, H^O)
hfOi
t.l-zs
Ps (stack pressure, in. Hg) =
Pb ± (stack static pressure (in. HgO) / 13.6)
~ -7 "
- 0.3
Ts (average stack temperature, °R) =
no "F+ 460 = °R
700
Tm (average meter temperature, ° R) =
Tamblert +2CfF + 460 =_°R
e>
( D O
Md (molecular weight of stack gas, dry, ib/Ib-mole) =
(0.44 x %CO,) + (032 x%02) + (0.28 x %N>)
i
-------
*ERG
Traverse Point Location Fgi m
Eortem Resoofcft Group. Inc.
Plant
Date
Yoc> O&cxi o *) Suuxe
-------
Velocity Traverse Form
Plant __J
Date
Location
Stack ID (in)
Barometric Pressure (in Hg)
Ambient Temperature (°F)
Static Pressure (in H2Q)
i operators I
Schematic of Traverse Point Layout
(Cross Section of Duct)
Traverse
Point
Number
Velocity
Head
LP, (in H20)
Stack |
Temperature
Ts, rn
Traverse
Point
Number
Velocity
Head
6P, (in H20)
Stack
Temperature
Ts, CP)
I
wERG
-------
feERG
Eastern Research Group. Inc.
Preliminary Velocity Traverse Form and Cyclonic Flow Check
Plant
Date
Location
(Sun-as^ £7fywJp
Stack ID (in)
Barometric Pressure (in Hg)
Ambient Temperature (°F)
Static Pressure (in H2Q)
Operators
Checked By
l o X H
13-3 0
1$'
_Z_IM
n i
* •< < *
¦% x * y
r * *
K * /
2
ft
3
6
2
Schematic of Traverse Point Layout
(Cross Section of Duct)
Traverse
Point
Number
Velocity
Head
APj(ih H20)
Stack
Temperature
Ts, (°F)
Cyclonic
Flow
Anqle (± °)
Traverse
Point
Number
Velocity
Head
AP, (in H20)
Stack
Temperature
Ts, (°F)
Cyclonic
Flow
Angle (± °)
A - / J
i
*
i
1
0
|
5
(9
|
¥
V ^7
s2-"3T) a
)
i
0
"2
o
0
|
4
^¦3-
7-3d
0
i
|
I
£- 1
c
|
2
-£. (o
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n
w
3
S3
Mb-
c
i
p^- (p
c
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X
P- \
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1
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* h 1
0
!
S29-7
c
I. (p
c
'•3^
2ZS.^
- 3 o
At?/
/m.
Average of Absolute Values of All Angles >20° Require Alignment Approach Sampling.
-------
feERG
Eosforn Research Sroup, Inc.
Preliminary Velocity Traverse Form and Cyclonic Flow Check
Plant
Date
Location
A-
Stack ID (in)
I y V/1 t t
Barometric Pressure (in Hg)
* /%%Al
Ambient Temperature (°F) |
Static Pressure (in H20)
Operators
LuJ
Checked By
Schematic of Traverse Point Layout
(Cross Section of Duct)
Traverse
Point
Number
Velocity I Stack j Cyclonic
Head Temperature Flow
AP, (in H20) 1 Ts, (°F) 1 Anqle (± °)
Traverse 1 Velocity
Point j Head
Number 1 AP, (in H20)
Stack
Temperature
Ts, (°F)
Cyclonic
Row
Anqle (± °)
a - |
LABS !
i
i
V-
I !/> ?—
*
1 (p ^L
if
,kn
j in ^
$
1
fa
tftlr
|
|
I
I
* Average of Absolute Values of All Angles >20° Require Alignment Approach Sampling.
-------
K-FACTOR CALCULATION FORM
Plant
%-jd-CTOalnf ittJM-
Operator
fWuM-l
Date
Used for runs
\ -s
Location/Sampling Train
fir Di'Tuff -
C„ (S-type: 0.84; Std: 0.99)
Pb (barometric pressure at location)
Dn (nozzle diameter, inches)
Bw (moisture in gas stream, fractional percent)
Pm (barometric pressure at meter, Hg) =
(Average AH / 13.6) + Pb
. z&u 29 c 0
AH@ (pressure differential of orifice in meterbox, 1^0)
1
Ps (stack pressure, in. Hg) =
Pb ± (stack static pressure (in. 1^0) / 13.6)
2.%
Ts (average stack temperature, °R) =
kl_"F + 460 = °R
& 1 £
Tm (average meter temperature, * R) =
Ta„ + 2CF + 460 = — °R
Md (molecular weight of stack gas, dry, Ib/lb-mole) =
(0.44 x %CQ,) + (032 x %Oj) + (028 x %N,)
2M-W
Ms (molecular weight of stack gas with water vapor, Ib/lb-mole) =
[ty, x (1 - QJ] + [18xEU]
K= (846.720)(Dn)4(AH@)(Co)2(l-Bw)2(Md/Ms)(P1/Pm)(Tm/Ts)
l-%2
AH = KAP
Correlation Chart
1
2
3
AH
AP
AH
AP
AH
AP
Comments;
-------
feERG
— K-FACTOR CALCULATION FORM
Plant
7 O
Operator
bo)
Date
Used for runs
t-3
Location/Sampling Train
iUM^t StR~iaJ b •
Ce (S-type: 0.84; Std: 0.99)
Pb (barometric pressure at location)
X^.3o
Dn (nozzle diameter, inches)
•Hi , i$o
Bw (moisture in gas stream, fractional percent)
. o $,
Pm (barometric pressure at meter, Hg) =
(Average AH / 13.6) + Pb
AH@ (pressure differential of orifice in meterbox, H^O)
\.n s
Ps (stack pressure, in. Hg) = ___ ij /s
Pb ± (stack static pressure (in. H^O) / 13.6) HvU
j* t £" 23-.0?
Ts (average stack temperature,0 R) =
^°F+ 460 = °R
K3
Tm (average meter temperature, ° R) = a p
Tamblent +20*F + 460 =_*R iu°
^ b £i
Md (molecular weight of stack gas, dry, Ib/lb-mole) =
(0.44 x %C02) + (032 x %Q.) + (0.28 x %N,)
iH-0
Nt. (molecular weight of stack gas with water vapor, lb/lb-mole) =
1M,x(1-BU)] + [18xBU]
2%.%
K= (846.720)(D„)4(A H@)(CJ\l-BJ2(M^(P^JCr,1/r,)
fD>
I
AH = KAP
Correlation Chart
1
2
3
AH
AP
AH
AP
AH
AP
Comments:
W 7 V /
7 - o
------- |