EPA/600/2-9l/032b
July 1991
THE FATE OF TRACE METALS IN A ROTARY KILN
INCINERATOR WITH A SINGLE-STAGE IONIZING
WET SCRUBBER
Volume II — Appendices
By
D. J. Fournier, Jr. and L. R. Waterland
Acurex Corporation
Environmental Research Facility
Incineration Research Facility
Jefferson, Arkansas 72079
EPA Contract No. 68-C9-0038
Work Assignment 0-3
EPA Project Officer: Robert C. Thurnau
Technical Task Manager: Gregory J. Carroll
Waste Minimization, Destruction, and Disposal Research Division
Risk Reduction Engineering Laboratory
Cincinnati, Ohio 45268
RISK REDUCTION ENGINEERING LABORATORY
OFFICE OF RESEARCH AND DEVELOPMENT
U.S. ENVIRONMENTAL PROTECTION AGENCY
CINCINNATI, OHIO 45268
-------
NOTICE
The information in this document has been funded by the United States Environmental
Protection Agency under Contract 68-C9-0038 to Acurex Corporation. It has been subjected to
the Agency's peer and administrative review, and it has been approved for publication as an EPA
document. Mention of trade names or commercial products does not constitute endorsement
or recommendation for use.
ii
-------
Today's rapidly developing and changing technologies and industrial products and
practices frequently carry with them the increased generation of materials that, if improperly
dealt with, can threaten both public health and the environment. The U.S. Environmental
Protection Agency is charged by Congress with protecting the Nation's land, air, and water
resources. Under a mandate of national environmental laws, the agency strives to formulate and
implement actions leading to a compatible balance between human activities and the ability of
natural systems to support and nurture life. These laws direct the EPA to perform research lo
define our environmental problems, measure the impacts, and search for solutions.
The Risk Reduction Engineering Laboratory is responsible for planning, implementing,
and managing research, development, and demonstration programs to provide an authoritative,
defensible, engineering basis in support of the policies, programs, and regulations of the EPA
with respect to drinking water, wastewater, pesticides, toxic substances, solid and hazardous
wastes, and Superfund-related activities. This publication is one of the products of that research
and provides a vital communication link between the researcher and the user community.
This report describes a series of tests conducted at the EPA's Incineration Research
Facility to evaluate the fate of trace metals fed to a rotary kiln incinerator. The testing is an
extension of the work described in the EPA report, The Fate of Trace Metals in a Rotary Kiln
Incinerator with a Venturi/Packed Column Scrubber," and is similar to that work in all respects
with the exception of the air pollution control system utilized. For further information, please
contact the Waste Minimization, Destruction, and Disposal Research Division of the Risk
Reduction Engineering Laboratory.
E. Timothy Oppelt, Director
Risk Reduction Engineering Laboratory
-------
ABSTRACT
A 3-week series of nine pilot-scale incineration tests was performed at the U.S.
Environmental Protection Agency's (EPA's) Incineration Research Facility (IRF) in Jefferson,
AR, to evaluate the fate of trace metals fed to a rotary kiln Incinerator equipped with a single-
stage ionizing wet scrubber for control of particulates and acid gas. Test variables were kiln
temperature, ranging from 816° to 927°C (1500° to 1700°F); afterburner temperature, ranging
from 982° to 1204°C (1800° to 2200°F); and feed chlorine content, ranging from 0% to 8%.
The test results indicated that cadmium and bismuth were relatively volatile, with an
average of less than 40% discharged with the kiln ash. Arsenic, barium, chromium, copper, lead,
magnesium and strontium were relatively nonvolatile, with an average of greater than
80% discharged with the kiln ash. Observed relative metal volatilities generally agreed with the
volatilities predicted based on vapor pressure/temperature relationships, with the exception of
arsenic, which was much less volatile than predicted. Cadmium, bismuth, and lead were more
volatile at higher kiln temperature; the discharge distributions of the remaining metals were not
significantly affected by kiln temperature.
Enrichment of metals in the fine-particulate fraction was observed at the afterburner
exit, with an average of roughly 50% of the flue-gas particulate metal in the less-than-10-jim size
range. The distributions of the more-volatile metals were shifted to fine particulate more so than
those of the less-volatile metals. Both increased kiln temperature and the addition of chlorine
to the synthetic waste feed caused a shift of metals to fine particulate.
Apparent scrubber collection efficiencies for the metals averaged 22% to 71%, and were
generally higher for the less-volatile metals. The overall average metal collection efficiency was
43%. It should be noted that industrial applications of ionizing wet scrubbers are typically in
multiple stages and, as such, would be expected to collect metals more efficiently than the single-
stage scrubber at the IRF.
This report was submitted in fulfillment of Contract 68-C9-0038 by Acurex Corporation
under the sponsorship of the U.S. Environmental Protection Agency. This report covers work
conducted during July and August 1989.
iv
-------
TABLE OF CONTENTS
ABSTRACT iii
FOREWORD iv
APPENDIX A — INCINERATOR OPERATING DATA 1
Appendix A-l Control Room Operating Data 2
Appendix A-2 Operating Data Plots 35
Appendix A-3 Waste Feed Schedules 45
Appendix A-4 CEM Data Plots 68
APPENDIX B — SCRUBBER SLOWDOWN METALS DATA 78
APPENDIX C - ANALYTICAL LABORATORY REPORTS 115
Appendix C-l Sample Tracking Records 119
Appendix C-2 Metal Analysis Data 129
Appendix C-3 Volatile Organic Analysis Results 154
Appendix C-4 Ultimate Analysis Results 182
Appendix C-5 Flue Gas HC1 Train Analysis Results 185
APPENDIX D - SAMPLING TRAIN DATA SHEETS 187
APPENDIX E — AFTERBURNER PARTICULATE SIZING REPORT 215
APPENDIX F-VOSTGC/FID AND CI ANALYSIS PROCEDURES 253
v
-------
APPENDIX A
INCINERATOR OPERATING DATA
1
-------
Appendix A-l
Control Roam Operating Data
2
-------
Test 1 Control Rtxw 8-17-89
Flue ess Sampling 09(5 - 1315
Clay Metals alow-
Feed Feed dom Makeup IHS 1HS
Height
Height Hater
Hater
Kiln
In A3
IHS
IHS Inlet Exit
Auger
Uq. Kiln
A3
AB
AB
AB
se
se
se
Stack Stac
Stack Stack
Reading Reading
Flow
Flow
P.
xlt Exit Uq. Bldwn Gas
Gas Stack Feed Bay
pH 02
02
CO
C02
THC
02
THC
HQ*
02
CO
C02
THC
Tin
(lis)
(lbs) (gpt)
(gpi) (-in we) ("F) (?) (?) (?)
CF) CFJ (V
(V ('F)
(t)
(i) (pp) m (ppi)
(*] (h») (pp)
(*)
(*
(*) (m)
858
421
34.46
0.4
6.6
0.03
1571 1992
154
142
175
173
167
88
85
7.35 14.8
9
1
6.2
2.8
12.8
0.8
36
13.1
4
-0.4
91S
34S
24.1
0.4
6.6
0.03
15(9 2000
159
142
175
173
167
88
86
7.84 11.4
7.3
3
8.2
3
11.6
1.1
32
12.1
5.2
-0.5
930
358
23
0.4
6.6
0.03
1635 1995
160
142
175
173
167
89
86
7.47 12.1
7.9
1
7.6
2.8
12.2
0.9
37
12.4
5
-0.8
9(5
322
21.88
0.4
6.6
0.04
16(3 19B6
16b
149
176
173
167
89
87
7.45 13.1
7.9
2
7.8
2.6
12.2
0.8
36
12.5
4.9
-0.5
tooo
285
20.69
8.4
6.6
0.04
1632 1980
160
143
174
172
166
90
88
7.44 11.9
8.1
2
7.3
2.7
12.5
1.1
37
12.8
4.7
-0.9
1015
249.5
19.(4
0.4
6.6
0.04
1626 1977
161
142
174
172
166
91
88
7.(5 12.7
8.(
2
7.3
2.8
12.6
1.2
36
12.8
4.6
-0.7
1030
214
18.24
0.4
6.6
0.03
1634 1992
161
143
175
172
167
94
89
7.(3 11.7
7.8
1
7.6
2.8
12.2
1
36
12.4
4.9
-0.7
1045
178
17.02
0.4
6.6
0.03
16(8 1996
162
143
175
172
167
94
90
7.42 11.5
7.6
1
7.8
2.9
12.1
0.9
3? 12.4
4.8
-0.4
. , iioo
142
15.78
0.4
6.6
0.03
1657 2000
162
144
175
173
167
95
91
7.42 11.8
7.7
1
7.8
2.8
12.1
1.2
38
12.4
(.9
-0.6
1115
387.5
14.62
0.4
6.6
0.045
1641 1994
162
143
175
172
166
96
92
7.(5 13.6
6.(
2
7.2
2.3
12.5
1.2
38
12.8
4.6
-0.9
1130
353
13.46
0.4
6.6
0.04
1637 1986
162
142
175
172
166
96
92
7.(5 13.8
8.2
2
7.4
2.8
12.5
1.3
36
12.7
4.7
-0.5
1145
217.5
13
0.4
6.6
0.04
1644 1784
163
142
175
173
166
97
93
7.46 14.2
8.7
2
7.(
2.B
12.6
1.2
38
12.9
4.5
-0.9
1200
279
11.02
0.4
6.6
0.04
1646 1987
163
142
175
172
166
97
92
7.47 14.7
8.6
0
7.5
2.7
12.5
1.1
37
12.8
4.7
-0.5
1215
244
10
0.4
6.6
0.04
1645 1990
163
142
175
172
166
98
94
7.47 14.7
8.7
2
7.3
2.5
12.7
0.9
37
12.7
4.6
-0.1
1230
204
8.85
0.4
6.6
0.04
1657 1985
163
142
175
173
166
97
94
7.49 14.4
8.(
1
7.5
2.9
12.4
1.3
37
12.8
4.8
-0.5
1245
174
7.8
0.4
6.6
0.04
1661 1993
163
142
175
172
166
99
94
7.49 14.7
8.1
1
7.5
2.9
12.3
1.1
37
12.8
4.6
-0.6
1300
139
6.8
0.4
6.6
0.04
1664 1994
164
142
175
173
166
98
94
7.49 14.4
8.3
1
7.3
3.1
12.4
1.2
37
12.8
4.5
-0.6
1315
104
5.58
0.4
6.6
0.04
1673 1995
164
150
176
173
164
98
95
7.49 14.5
8
-1
7.6 0.38
12.4
1.3
3B
12.6
4.6
-0.3
1330
70
11.2
0.4
6.6
0.04
1677 1997
164
143
175
173
166
100
96
7.5 14
8.6
1
7.4
3
12.5
1.3
37
12.7
4.5
-0.3
1345
37
10
0.4
6.6
0.04
1674 1993
164
143
175
173
166
102
96
7.2 14.2
8.2
-1
7.2
3
12.4
1.1
38
12.8
4.6
-0.3
1400
13
8.84
0.4
6.6
0.04
1576 1979
165
143
174
171
166
101
97
7.59 17.7
11.3
-1
4.9
2.7
14.3
1.3
(9
14.4
3.2
-0.5
1415
13
8.84
0.4
6.1
D.04
1502 1994
165
143
174
171
166
102
97
7.68 17.8 10.8
-2
5.2
2.9
13.9
1.1
39
14
3.4
-0.4
1430
13
8.84
0.4
6.6
0.0(5
1434 1986
165
142
174
171
165
101
97
7.72 18.6 10.8
-2
5.2
2.9
14
1.3
37
14.1
3.4
-0.6
1445
13
8.84
0.4
6.6
0.(5
1372 19(8
165
142
174
171
165
104
97
7.74 18.6 10.9
-3
5.1
2.6
14
0.8
37
14.1
3.3
-0.7
(1)N1n:
37.0
5.58
0.4
6.8
0.03
1626 1784
160
142
174
172
164
89
87
7.20 11.5
7.6
-1
7.2
0.4
12.1
0.8
3b4 12.4
3.
4.5
-0.9
fex:
387.5
21.88
0.4
6.6
0.045
1677 2000
164
150
176
173
167
102
96
7.50 M.T
8.7
2
7.8
3.1
12.7
1.3 38.0
12.9
5.
4.9
-0.1
Avg:
211.7
13.26
0.4
6.6
0.04
1651 1978
162
143
175
172
166
96
92
7.(5 13.5
8.2
1
7.5
2.7
12.4
1.1
3 7.o 12.7
3.
4.7
-0.5
(1) During Flue Gas Saapllng
-------
Test 1 Bay Area 8-17-89
Flue Gas Sailing 094S - 1345 Quench Systea IKS APCS
Secondary APCS
Coapres. Hist Spray IMS IMS Carbon Carbon
Rota- Feed Pres. Pres. Pres. Air Hater Hater Iai'rer Outlet Inlet Purge 2nd farister Bed Exit 1st Bed
¦eter Pres. Flowate 1 2 3 Pres. Flow Flowrate Voltage Pres. Pres. Air Op HEPA Dp Op Pres. HEPA Op Te«p.
T1«e Mitels totals (gpn) (psl) (psl) (psl) (psl) (gpa) (V) (-in wc) (-in wc) (-In wc) (-1n *e) (-1n »e) (-In wc) (-In *c) (*F)
900
18
32
34
34
45
30
42
6000
2
1.5
0.4
2.5
0
0
3.7
160
915
60
S
18
32
34
34
45
30
45
9000
2
1.5
0.4
2.5
0
0
3.75
160
930
50
5
18
32
34
34
45
30
45
9000
2
1.5
0.4
2.5
0
0
4
160
945
60
5
18
32
34
34
45
30
45
9000
2
1.5
0.4
3
0
0
4
160
1000
SO
5
18
32
34
34
45
30
45
9000
2
1.5
0.4
3
0
0
4
160
1015
60
5
18
34
35
37
45
30
45
9000
2
1.5
0.4
3.5
0
0
4
160
1030
60
5
18
34
36
36
45
30
45
9000
2
1.5
0.4
3.5
0
0
4
160
1045
60
5
18
34
36
36
45
30
45
9000
2
1.5
0.4
3.5
0
0
4
160
1100
60
5
18
34
36
36
45
30
45
9000
2
1.5
0.4
3.5
0
0
4
160
1115
60
5
18
34
36
36
45
30
45
9000
2
1.5
0.4
4
0
0
4
160
1130
60
5
18
34
36
36
45
30
45
9000
2
1.5
0.4
4
0
0
4
168
1145
60
5
18
34
36
36
45
30
45
9000
1.5
1.5
0.4
3.75
0
0
4
160
1200
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3.5
0
0
4
160
1215
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3.7
0
0
4
160
1230
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
4
0
0
4
160
1245
60
5
11
35
37
37
45
30
45
9000
1.5
1.5
0.4
4
0
0
4
160
1300
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
4
0
0
4
160
1315
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3.5
0
0
4
160
1330
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3.5
0
0
4
160
1345
60
5
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3.5
0
0
4
160
1400
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
1415
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
1430
18
35
37
37
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
1445
18
3S
37
37
45
30
45
9000
1.5
1.5
0.4
3
0
8
4
160
(1)M1n:
60
5
18
32
34
34
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
Max:
60
5
18
32
34
34
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
Avg:
60
5
18
32
34
34
45
30
45
9000
1.5
1.5
0.4
3
0
0
4
160
(1) During Flue Gas Sampling
-------
Test 1 Gas Train 8-17-89
Flue Gas Sampling 0945 - 1345 Kiln Main Afterburner Main Kiln Pilot Afterburner Pilot
Total Kiln Gas Gas Kiln AB Gas Gas A8 Kiln K1 In Gas Gas AB A8 Gas Gas
Air Air Air A1r Air Pres. Pres. Gas A1r Pres. Pres. Gas Pilot Atom. Pres. Pres. Pilot Aton. Pres. Pres.
Plenum Static Flow Temp. Flow Static Oynamlc Temp. Flow Static Dynamic Temp. Air Air Static Dynamic Air Air Static Oynamic
Time (In trc) (In *c) (in wc) ('F) (In wc) (psl) (In wc) (*F) (in wc) (ps1) (In wc) (*F) (in we) (In wc) (in wc) (in wc) (In wc) (In wc) (in wc) (In wc)
900
44
40
1
104
2.0
2.5
0.3
78
5.8
7 1.25
78
0
4.5
0.5
0.05
0.4
4
8.5
0.25
915
44
40
1
104
2.0
2.6
0.2
78
5.8
7 1.2
78
0.05
4.5
0.5
0.05
0.4
4
8.5
0.25
930
44
40
0.9
104
1.9
2.6
0.15
78
5.8
7 1.2
78
0.05
4.5
0.5
0.05
0.4
4
8.5
0.25
945
44
40
0.9
106
1.8
2.6
0.2
80
5.8
7 1.2
80
0.05
4.5
0.5
0.05
0.4
4
8.5
0.25
1000
44
40
1
106
2.0
2.6
0.15
80
5.8
7 1.2
80
0.05
4.5
0.5
0.05
0.4
4
8.5
0.25
1015
44
40
1
108
2.0
2.6
0.15
82
5.3
7 1.2
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1030
44
40
1
108
2.0
2.6
0.15
82
5.3
7 1.2
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1015
44
40
1
108
2.1
2.6
0.15
82
5.3
7 1.2
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1100
44
40
0.9
110
2.0
2.6
0.15
82
5.3
7 1.2
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1115
44
40
0.9
110
2.0
2.6
0.15
82
5.3
7 1.2
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1130
44
40
0.9
110
2.0
2.6
0.15
82
5.3
7 1.2
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1145
44
40
U
110'
2.1
2.6
0.15
82
5.3
7 1.2
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.28
1200
44
40
0.9
112
2.1
2.6
0.15
84
5.3
7 1.2
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1215
44
40
0.9
112
2.1
2.6
0.15
84
5.3
7 1.2
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1230
44
40
0.9
112
2.1
2.6
0.15
84
5.3
7 1.2
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1245
44
40
0.9
112
2.1
2.6
0.15
84
5.3
7 1.2
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
13D0
43
40
0.9
112
2.1
2.6
0.15
86
5.3
7 1.22
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1315
43
40
0.9
112
2.1
2.6
0.15
86
5.3
7 1.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1330
43
40
0.9
112
2.1
2.6
0.15
86
5.3
7 1.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1345
43
40
0.9
112
2.1
2.6
0.15
86
5.3
7 1.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1400
43
40
0.9
112
2.1
2.6
0.25
86
5.3
7 '.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1415
43
40
0.9
114
2.1
2.6
0.25
86
5.3
7 1.25
86
0.05
4.5
0.J
0.05
0.4
4.2
8.5
0.28
1430
43
40
0.9
114
2.1
2.6
0.25
86
5.3
7 1.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
1445
43
40
0.9
114
2.1
2.6
0.25
8t>
5.3
7 1.25
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.28
(1)Wn:
43
40
0.9
106
1.8
2.6
0.15
80
5.3
7 1.20
80
0.1
4.5
0.6
0.05
0.40
4.0
8.5
0.25
Max:
44
40
1.0
112
2.1
2.6
0.20
86
5.8
7 1.25
86
0.1
4.7
0.5
0.05
0.40
4.2
8.5
0.28
Avg:
44
40
0.9
110
3.0
2.6
0.15
83
5.4
7 1.21
83
0.1
4.6
0.5
0.05
0.40
4.2
8.5
0.27
(1) during Flue Gas Sampling
-------
Test 2 Control Room 8-2-89
Flue 6as Stapling 0945 - 1330
Clay Metals Blow-
Feed Feed 2.
7.3
5
7.9
0 11.
0
42
11.6
8
5.1
0
140D
1200
30.64
0.5
6.2
0.05
1552 2043
167
153
178
174
168
115
8.36 0
7.6
6
7.6
0 11.
0
43
11.6
10
5.2
0.2
1415
1166
29.4
0.5
6.2
0.05
1530 2054
167
159
179
175
168
117
8.26 12.4
0.2
4
0.1
0 11.
0
41
11.9
9
5.3
0.1
1430
1136
28.32
0.5
6.2
0.05
1535 2050
167
153
178
174
168
117
8.07 12.4
0.1
2
0.2
0 0.
0
2
11.9
10
5.1
0.1
1445
1101
2720
O.S
6.2
0.05
1534 2047
167
153
178
174
168
115
7.97 12.3
0.1
2
0.2
0 20.
0
13
8.8
9
9.3
0
1500
1069.5
26.04
0.5
6.2
0.04
1534 2041
167
153
178
174
168
117
7.95
12.4
*103
3.4
0.2
-------
Test 2 Cont'd Control faa 1-2-89
Flue 6m Sanpllng 0945 - 1330
Clay Retail Blow-
Feed Feed dam Hakeup IKS INS
Hafght Itelght Hater Hater Kiln Kiln A3 IKS IK Inlet Exit Auger Llq. Kiln AB AS AS AB SE SE SE Stack Stack Stack St*...
Reading Reading Flow Flow Pres. Exit Exit L1q. 81dm Gas Gas Stack FeedpH02 02 COCC2THC02THCN0x02 C0C02THC
Tlw (lbs) (lbs) (flpf.) (gpa) (-In nc) (*F) (*F) (*F) (*F) (*F) (*F) CF) (*F) (t) (*) (pp.) (*) (p«.) (*) (v») (ppa) (*) (*) (t) (opn)
1515
1317
24.94
O.S
6.2
0.05
1528 2040
168
153
178
174
168
119
7.92
12.3
5
4.9
0.2
1530
1287
23.88
0.5
6.2
0.04
1510 2023
168
152
178
173
168
117
7.82
12.1
4
4.9
0
1545
1257.5
22.78
0.5
6.2
0.04
1524 2023
167
153
178
173
168
116
7.6
12.1
6
4.9
0
1600
1225.5
26.22
0.6
6.2
0.04
1527 2019
168
153
178
173
168
117
7.4
12.1
5
4.9
0.1
1615
1196'
20.52
0.6
6.2
0.04
1527 2013
168
153
177
174
167
116
7.27
12.1
5
5
0.1
1530
1164.5
19.4
0.6
6.2
0.04
1521 2011
168
152
178
173
16?
117
7.15
12.3
5
4.9
0.1
1645
1129
18.22
0.6
6.2
0.5
1523 2011
168
153
177
173
168
116
6.79
12
6
5
0
1700
1100.5
17.24
0.E
6.4
0.5
1527 2011
168
152
177
173
168
115
5.9
12.1
6
4.9
0
1715
1068.5
16.1
0.6
6.4
0.55
1541 2015
168
153
178
174
167
115
9.22
12.1
6
4.8
0
1730
1052
15.56
0.6
6.4
0.5
1622 1459
168
159
176
172
168
116
8.14
14.1
5
3.3
0.1
^ 1745
1052
15.56
0.6
6.4
0.7
1351 1785
167
153
171
167
164
117
8.16
15.9
6
2.3
0
1600
1052
15.36
0.6
6.4
0.7
1083 1502
161
149
164
160
158
114
8.76
17.8
237
1.6
0
1015
1052.5
15.56
0.6
6.4
0.15
951 1325
156
145
159
156
153
113
9.1
18
422
1.2
0.1
(OXint
1156.0
32.8
0.0
5.6
0.04
1459 1976
164
152
177
171
17
104
6.3 11.4
6.6 3.0 7.3 0.0
4.6
0.8 37.0
11.0
9.0
4.9
0.0
Max:
1420.5
49.8
0.6
6.2
0.06
1537 2025
167
153
179
174
169
114
9.2 14.0
8.2 5.0 8.4 0.C
11.9
0.0 47.0
12.2
11.0
8.1
0.3
Avgs
1306.5
41.5
0.5
6.2
0.05
1511 1999
165
153
17B
174
158
109
7.8 12.3
7.6 4.0 7.8 0.0
11.2
0.0 43.4
11.8
9.7
5.3
0.1
(I) During Flue On Stapling
-------
Test 2 Bay Area 8-2-83
Flue Gas Saapllng 0945 - 1330 Quench Systen IKS APCS
Secondary APCS
Coapres. Mist Spray IHS INS Carbon Carbon
Rota- Feed Pres. Pres. Pres. Air Hater Hater Ionizer Outlet Inlet Purge 2nd Dmlster Bed Exit 1st 8ed
Meter Pres. Flowrate 1 2 3 Pres. Flow Flowate Voltage Pres. Pros. A1r Dp HEPA Dp Op Pres. HEPA Op Teap.
Hoe totals totals (gpa) (ps1) (pel) (psl) (ps1) (gpa) (V) (-In wc) (-1n wc) (-In *) (-1n wc) (-In wc) (-In wc) (-In *) (*F)
845
18
45 45
45 20
20
3000
1 1
0.4
3
0
3
2.5
156
900
18
45 47
47 25
25
3000
1 1
0.4
3
0
3
2.5
156
915
18
45 47
47 25
25
3000
1 1
0.4
3
0
3
2.5
156
930
18
45 47
47 25
25
3000
1 0.5
0.4
3
0
3
2.5
156
945
55
5
18
45 47
47 25
25
3000
1 0.5
0.4
3
0
3
2.5
156
1000
57
5
18
45 47
47 25
25
3000
1 0.5
0.4
3
0
3
2.5
156
1015
5T
5
18
45 47
47 25
15
3000
1 0.5
0.4
3
0
3
2.5
156
1030
60
5
18
45 47
47 20
10
3000
1 0.5
0.4
3
0
2.5
2.5
158
1045
60
5
18
45 47
47 20
10
3000
1 0.5
0.4
2.5
0
2
2.5
158
1100
60
5
18
45 47
47 20
10
3000
1 0.5
0.4
2.5
0
2
2.5
158
1115
60
5
18
45 47
47 20
10
3000
1 0.5
0.4
2.5
0
2
2.5
158
1130
60
5
18
45 47
47 20
10
3000
1 0.5
0.4
2.5
0
2
2.5
158
1145
60
5
18
45 47
47 20
10
45
3000
1 0.5
0.4
3
0
2
2.5
158
1200
60
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
2
2.5
158
1215
60
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
2
2.5
158
1230
60
5
18
46 47
47 20
10
42
3000
1 0.5
0.4
3.5
0
1.5
2.5
158
1245
60
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1300
60
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1315
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1330
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1345
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1400
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
3
0
1.5
2.5
159
1415
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
4.5
0.5
1.5
2.5
159
1430
57
5
18
45 47
47 20
10
42
3000
1 0.5
0.4
4.5
0.5
1.5
2.5
159
1445
57
5
18
45 47
47 20
10
45
3000
1 0.5
0.4
5
0.5
1.5
2
159
1500
57
5
18
46 47
47 20
10
45
3000
1 0.5
0.4
5
0.5
1.5
2
159
1515
57
S
18
46 47
47 20
10
45
3000
1 0.5
0.4
5
0.5
1.5
2.5
160
1530
57
5
18
46 47
47 20
10
45
3000
1 0.5
0.4
5
0.5
1.5
2
160
1545
55
5
18
49 47
47 20
10
45
3000
1 0.5
0.4
5
0.5
1.5
2.5
158
1600
55
5
18
49 47
47 20
12
45
3000
t 0.5
0.4
4.5
0.5
1.5
2.5
158
-------
Test 2 cont'd Bay Area 3-2-89
Fluo 6as Saapllng 0945 - 1330 Quench Systm IHS APCS Secondary APCS
Conpres. Hist Spray IHS IMS Carbon Carbon
Rota- Feed Pres. Pros. Pres. A1r Hater Hater Ionizer Outlet Inlet Purge 2nd Denlster Bod Exit 1st Bed
aeter Pres. Flowate 1 2 3 Pres. Flow Flowrate Voltage Pres. Pres. Air Dp HEPA Op Op Pres. HEPA Op leap.
T1#e Metals Metals (gp») (psl) (ps1) (ps1) (psl) (gpm) (V) (-1n kc) (-1n we) (-1n nc) (-In we) (-1n wc) (-1n mc) (-In mc) (*F)
1615
55
5
18 49 4
47 20
12
45
3000
1
0.5
0.4
4.5
0.5
2
2.5
158
1630
55
5
18 49 4
47 20
12
45
3000
1
0.5
0.4
4.5
0.5
1.5
2.5
158
1645
55
5
18 49 4
47 20
12
45
3000
1
0.5
0.4
4.5
0.5
2
2.5
158
1700
55
5
18 49 4
47 20
12
4S
3000
1
0.5
0.4
4
0.5
1.5
2.5
1S8
1715
55
5
18 49 4
47 20
12
45
3000
1
0.5
0.4
4
0.5
1.5
2.5
158
1730
18 49 4
47 20
12
45
3000
1
0.5
0.4
4
0.5
1.5
2.5
158
1745
18 46 4
47 20
12
45
3000
1
0.5
0.4
5
0.5
2
2.5
154
1800
18 46 4
47 20
12
45
3000
1
0.5
C.4
5
0.5
2
2.5
149
181$
18 46 4
47 20
12
45
3000
1
0.5
V.4
5
0.5
1.5
2.5
144
(1)M1n:
55.0
5
18 45 4
47 20
10
42
3000
1.0
0.5
0.4
2.5
0.0
1.5
2.5
156
Max:
60.0
5
18 46 4
47 25
25
45
3000
1.0
0.5
0.4
3.5
0.0
3.0
2.5
159
Avfl:
58.9
5
18 45 4
47 21
12
42
3000
1.0
0.5
0.4
2.9
0.0
2.1
2.5
158
(1) During Flue Gas Saapllng
-------
Test 2 Gas Train 8-2-81
Flue 80s SMplin 0M5 - 1330
K1ln Hiln
Afterburnar Main
Kiln Pilot
Afterburnar Pilot
Total Kiln Gas Gas Kiln AB Gas Gas AS Kiln Kiln Gas Gas AB AS Gas Gas
Air Air A1r Air Air Pres. Pres. Gas Air Pres. Pres. 6as Pilot Aton. Pres. Pres. Pilot Atom. Pres. Pres.
Plenua Static FIom Teap. Flow Static Oynaalc reap. Flow Static Oynaalc Teap. Air Air Static Oynaalc A1r Air Static Oynaalc
Tlae (In nc) (In mc) (In k) ( F) (In nc) (pel) (In wc) ( F) (In nc) (ps1) (In nc) ( F) (In hc) (In nc) (1n nc) (in mc) (1n mc) (In nc) (In k) (In wc)
845
44
40
1
106
2.8
2.5
0.5
80
4.S
2.6 1
80
0.1
s
0.5
0.05
0.1
7.5
8.5
0.25
900
44
40
1
106
2.4
2.6
0.2
80
4.5
2.6 1
80
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
915
43
40
0.8
106
2.0
2.6
0.2
82
4.5
2.6 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
930
43
40
0.6
106
1.4
2.6
0.25
80
4.5
2.6 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
945
43
40
0.6
106
1.4
2.6
0.25
82
5
2.6 1
82
0.1
5
0.5
8.05
0.1
7.5
8.5
0.25
1000
43
40
0.6
108
1.4
2
0.25
82
5.2
2.6 1.1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1015
43
40
0.6
108
1.4
2
0.2
e:
5.2
2.6 1.1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1030
43
40
0.6
108
1.4
2
0.15
82
5.2
2.6 1.1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1045
43
40
0.8
10B
1.3
2.6
0.15
82
5.5
2.6 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1100
43
40
0.9
110
1.3
2.6
0.15
82
5.8
2.6 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1115
43
40
0.8
110
1.0
2.6
0.15
82
5.8
2.6 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1130
43
40
0.8
110
1.0
2.6
0.15
82
5.9
2.5 1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1145
43
40
0.8
112
0.9
2.6
0.15
B4
5.8
2.6 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1200
43
40
0.8
112
1.0
2.6
0.15
84
5.9
2.6 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1215
43
40
0.8
112
1.0
2.6
D.15
84
5.9
2.6 1
84
0.1
5
0.5
0.05
0.1
7.5
0.5
0.25
1230
43
40
0.8
112
1.0
2.6
0.15
86
5.9
2.6 1
86
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1245
43
40
0.8
112
1.0
2.6
0.15
86
5.9
2.9 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1300
43
40
0.8
112
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1315
43
40
0.8
112
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1330
43
40
o.e
112
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1345
43
40
o.e
112
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1400
43
40
0.8
114
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1415
43
40
0.8
114
1.0
2.6
8.15
16
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1430
43
40
1.8
114
1.0
2.6
0.15
86
5.9
2.4 1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1445
43
40
0.8
116
1.0
2.6
0.15
90
5.4
2.6 1
90
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1500
43
40
0.8
116
1.0
2.6
0.15
90
5.4
2.6 1
90
0.1
5
0.5
0.05
0.1
T.5
8.5
0.25
1515
43
40
0.8
116
1.0
2.6
0.15
SO
5.4
2.6 1
90
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1530
43
40
0.8
116
1.0
2.6
0.15
90
5.4
2.6 1
90
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1545
43
40
0.8
116
1.0
2.6
0.15
90
5.4
2.6 1
90
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
-------
Test 2 Cont'd 6k Train 1-2-89
Flue Gas Stapling 0945 - 1330 K1ln Main Afterburner Main Kiln Pilot Afterburner Pilot
Total Kiln Gas Gas Kiln AS Ga3 Gas A8 Kiln Kiln Gas Gas A3 AS Gas Gas
Air Air Air Air A1r Pres. Pres. Gas Air Pres. Pres. Gas Pilot Atom. Pres. Pres. Pilot Atom. Pres. Pres.
Plenua Static Flow Teop. Flow Static Oynaalc Temp. Flow Static Oynaalc Temp. Air A1r Static (tynaatc A1r Air Static Dynanlc
T1»e (In te) (In wc) (In nc) ( F) (In «) (psl) (in *c) ( F) (In *c) (ps1) (1n wc) ( F) (1n wc) (In wc) (In wc) (In «) (In nc) (In we) (In «) (1n nc)
1600
40
0.8
116
1.0
2.6
0.15
92
5.4
2.6
1
92
0.1
5
O.S
8.05
0.1
7.5
8.5
0.25
1615
40
0.8
116
1.0
2.6
0.15
92
5.4
2.6
1
92
0.1
5
O.S
0.05
0.1
7.5
8.5
0.25
1630
40
O.B
116
1.0
2.6
0.15
92
5.4
2.6
1
92
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
IMS
40
0.8
116
1.0
2.6
0.15
92
5.9
2.6
1
92
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1700
40
0.8
116
1.0
2.6
0.15
92
5.9
2.6
1
92
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1715
40
0.8
116
1.0
2.6
0.15
92
5.9
2.6
1
92
0.1
5
0.5
0.05
0.1
7.5
8.5
8.25
1730
40
0.1
11s
1.0
2.6
0.35
92
5.9
2.6
0.7
92
0.1
5
0.5
0.05
0.1
T.5
8.5
0.25
1745
40
0.8
116
1.0
2.6
0.2
92
5.9
2.8
0.55
92
0.1
4.7
0.5
0.05
0.1
7.5
8.5
0.25
1800
40
1
116
1.8
2.6
0.2
92
5.7
2.8
35
92
0.1
4.7
0.5
0.05
0.1
7.5
8.5
0.25
1815
40
0.9
116
1.8
2.6
0.2
92
6
3
0.3
92
0.1
4.7
0.5
0.05
0.1
7.5
3.5
0.25
_ (1)N1n:
40
0.1
106
0.9
2.0
0.15
82
5.DO
2.4
1.00
82
0.1
S.O
0.5
0.05
0.10
7.5
8.5
0.25
^ Rax:
40
0.9
112
1.4
2.6
8.25
86
5.90
2.9
1.10
86
0.1
5.0
0.5
0.05
0.10
7.5
8.5
0.25
Awg:
40
0.8
110
1.1
2.5
8.17
84
5.67
2.6
1.02
83
0.1
5.0
0.5
0.05
0.10
7.5
8.5
0.25
(1) During F
w Gas Stapling
-------
Test 3 Control Room 8-4-89
Flue Gas Sampling 1030 - 1330
Clay Metals Blow-
Feed Feed dom Mataup INS INS
Height
Height Hater
Hater
Kiln
Kiln AS
IHS
IHS Inlet Exit
Auger
Liq. Kiln
AS
A8
AS
AS
SE
SE
SE
Stack Stac
Stack Stack
Reading Reading
Flan
Flow
Pres.
Exit Exit Liq. Bldwn Gas
Gas Stack Feed
pH 02
02
CO
002
THC
02
THC
nom
02
CO
C02
THC
Tine
(lbs)
(lbs) (gpa)
(gp) (-in *) (*F) CF) ('F) (*F)
(*F) CF) CF)
CF)
(*)
(*) (PP») (*) (PP«)
(X) (mm) (ppa)
(*)
(t
(t) (PO)
93d
533.5
44.48
6.7
6
0.06
1696 1929
163
144
174
170
165
103
0 13
8.5
3
6.5
0
12.5
0.6
36
12.7
4.1
0
945
529
44.48
0.7
5.2
0.06
1552 1921
164
149
174
170
165
104
3.32 12.8
8.4
3
7.3
0.5
12.4
0.6
31
12.6
4.7
0
1000
0
44.32
0.7
6.2
0.06
1668 1923
164
150
175
171
165
104
0.9 12.5
8
1
6.8
0.3
12.3
0.7
33
12.5
4.3
0
1015
527.5
44.3
0.7
6.2
0.06
1699 1953
165
150
176
173
166
102
0.26 9.8
5.8
3
8.7
0.3
10.7
0
33
11.2
5.4
0.3
1030
502
44.3
0.7
6.2
0.06
1699 1953
165
151
176
173
167
103
8.78 10
5.8
3
6.8
0.2
10.7
1
41
11.2
5.4
0
1045
471.5
42.64
0.7
6.2
0.05
1704 1982
166
151
175
172
167
105
9.16 11.4
7
3
7.9
0.2
11.5
0.7
43
11.9
4
0
1100
440.5
41.44
0.7
6.2
0.06
1711 1968
166
150
175
173
164
104
9.04 11.2
7.1
5
7.9
0
11.5
1
40
11.9
4.9
0
1115
408.5
40.2
0.7
6.2
0.06
1728 1988
166
150
176
173
167
106
8.99 11.2
6.9
4
7.9
0
11.4
0.9
42
11.9
4.9
0
, 1130
374.5
38.96
0.7
6.2
0.05
1705 1991
166
149
175
173
167
105
8.88 11.9
7.3
3
7.9
0
11.8
1
41
12
4.8
0
» 1145
341.5
37.8
0.7
6.2
0.05
1704 1995
166
150
175
173
167
107
8.83 12
7.3
3
7.8
0
11.6
1
40
12
4.8
0
1200
307
36.5$
0.7
5.6
0.05
1713 1998
167
150
176
173
167
110
8.84 11.8
7.1
3
7.8
0
11.6
0.9
40
12
4.9
0
1215
272
35.3
0.7
6.2
0.05
1709 1998
167
152
176
173
168
108
8.76 11.8
7
4
8
0
11.6
0.6
39
11.9
4.8
0
1230
237
34.1
0.7
6.2
0.06
1696 2002
167
150
176
173
167
107
8.03 12.1
7.4
4
8.9
1
11.8
0.9
40
12
4.7
0
1245
202
32.8
0.7
6.2
0.07
1689 2011
167
150
177
174
167
110
8.7 12.6
8.1
3
7.4
0
11.9
0.7
38
12
4.9
0
1300
167
31.64
0.7
6.2
0.055
1708 2020
167
150
177
174
168
110
8.64 12.2
7.6
4
7.72
0
11.5
0.9
40
11.6
5.1
0
1315
132
30.42
0.7
6.2
0.07
1701 2015
167
151
177
174
168
111
8.6 13.2
V.5
3
7.6
1.3
11.7
0
38
11.9
5.1
0
1330
98
29.22
0.7
6.2
0.07
1733 2013
168
152
178
174
168
111
8.57 12.9
7.5
3
7.5
1.5
11.1
0
41
11.9
4.9
0
1345
88
28.12
0.7
6.2
0.06
1642 2015
168
153
178
173
168
112
8.59 13.9
8.3
3
6.5
1.9
12.5
0
40
12.6
4.3
0
1400
109.5
28.12
0.7
6.2
0.06
1634 2012
168
152
177
173
167
111
8.79 15.6 10.1
3
5.6
0
13.1
0
33
13.2
3.7
0
1415
109.5
28.1
0.7
6.2
0.06
1579 2001
169
152
176
173
167
111
8.93 15.6 10.3
3
5.4
0
13.3
0
31
13.2
3.6
0
1430
109.5
28.12
0.7
6.2
0.06
1541 1991
169
152
176
172
166
110
8.99 15.7 10.3
1
5.4
0
13.3
0
30
13.2
3.6
0
(1)Min:
98.0
29.2
0.7
5.6
0.05
1689 1953
165
149
175
172
164
103
8.0 10.0
5.8
3.0
7.4
0.0
10.7
0.0 38.0
11.2
2.
4.0
0.0
Max:
502.0
44.3
0.7
6.2
0.07
1733 2020
168
152
178
174
168
111
9.2 13.2
8.1
5.0
8.9
1.5
11.9
1.0 43.0
12.0
5.
5.4
0.0
Avg:
304.1
36.6
0.7
6.2
0.06
1708 1995
167
150
176
173
167
107
8.8 11.9
7.2
3.5
7.9
0.3
11.5
0.7 40.2
11.9
3.
4.9
0.0
(1) Owing Flue Gas Saapllog
-------
Test 3 Bay Area 8-4-09
Flue 6as Saaplfng 1030 - 1330 Quench Systea IK! APCS Secondary APCS
Conpres. Mist Spray IKS IMS Carbon Carbon
Itota- Feed Pres. Pres. Pres. Air Hater Hater Ionizer Outlet Inlet Purge 2nd Denlster Bed Exit 1st Bed
¦eter Pres. Flo*rate 1 2 3 Pres. Flow Flowrate Voltage(2) Pres. Pres. Air Op HfPA Dp Op Pres. HEPA Dp Temp.
Tine
Metals Metals
(psl)
(ps1)
(ps1)
(ps1)
(Of")
(V)
(-1n «) f-1n wc) (-in we) (-in wc) (—1n wc) (-In wc) (-In wc
(*F)
930
20
46
48
48
20
10
45
0
1
1
0.4
3.5
8
2.5
3
155
945
20
46
48
48
20
10
45
0
1
1
0.4
3.5
0
2.5
3
I5S
1000
20
46
48
48
20
10
45
0
1
1
0.4
3.5
0
2.5
3
156
1015
20
46
48
48
20
10
45
0
1
1
0.4
3.5
0
2.5
3
156
1030
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
3.5
0
2
2.5
158
1045
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
4.5
0
2.5
3
158
1100
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
4.5
0
3
3.5
158
1115
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
5
0.5
3
3
158
1130
to
4.5
20
46
48
48
20
10
45
0
1.5
1
0.4
5
0.5
3
3.5
158
114$
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
5.5
0.5
3
3.5
158
1200
60
4.5
20
46
48
48
20
10
45
0
1
1
8.4
5.5
0.5
3
3.5
156
_ 1215
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
5.5
0.5
3.5
3.5
158
w )23o
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
6
0.5
3
3.5
158
1245
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
6
0.5
3
3.5
158
1300
60
4.5
20
«S
48
48
20
10
45
0
1
1
0.4
5.5
0.5
2.5
3
158
131S
60
4.5
20
46
48
48
20
10
45
0
1
1
0.4
5.5
0.5
2.5
3
158
1330
60
4.5
20
46
49
48
20
10
45
0
1
1
0.4
5.5
0.5
2.5
3
158
1345
20
46
48
48
20
10
45
0
1
1
0.4
5
0.5
2
2.5
158
1400
20
46
48
48
20
10
45
0
1
1
0.4
5
0.5
2
2.5
158
1415
20
46
41
48
20
10
45
0
1
1
0.4
5.5
0.5
2
2.5
158
1430
20
46
48
48
20
10
45
0
1
1
0.4
5.5
0.5
2
2.5
158
(1)M1n:
60.0
4.5
20
46
48
48
20
10
45
0
1.0
1.0
0.4
3.5
0.0
2.0
2.5
158
Max:
60.0
4.5
20
46
48
48
20
10
45
0
1.5
1.0
0.4
6.0
0.5
3.5
3.5
158
Mn-.
60.0
4.5
20
46
48
48
20
10
45
0
1.0
1.0
0.4
5.2
0.4
2.8
3.2
158
(1) During Flue Gas Stapling
(2) Ionizer not operated during test
-------
last 3 Gas Train 8-4-89
Flue Gas Stapling 1030 -
1330
Kiln Main
Afterburner Main
Kiln Pilot
Afterburner Pilot
Total
Kiln
Gas
Gas
Kiln
A3
Gas
Gas
AS
Kiln
Kiln
Gas
Gas
A3
AS
Gas
Gas
Air
Air
Air
Air A1r
Pres.
Pres.
Gas
Air
Pres.
Pres.
6as
Pilot
Atod.
Pres.
Pres.
Pilot
Atoa.
Pres.
Pres.
Plenun
Static
Flow
Tea
Flow Static Dynaalc Tenp.
Flow Static Oynaaic Tenp.
Air
A1r
Static
Oynaaic
Air
Air
Static
Oynaaic
Tin (In nc)
(in nc) [in nc)
C
) (in nc) (ps1) (1n wc)
(*F) (in wc) (psi) (in *)
(*F) (in nc) (in nc) (In nc) (in nc) (In wc) (In nc) (in nc) (in «)
933
43
40
o.e
1
0 2.8
2.5
0.6
83
3.7
2.7
0.8
83
0.1
5
0.5
0.05
0.1
4.5
8.5
0.2
945
43
40
0.6
1
0 2.8
2.5
0.35
83
3.7
2.7
0.85
83
0.1
5
0.5
0.05
0.1
4.5
8.5
0.2
1000
43
40
1
1
0 2.8
2.5
0.35
83
5
2.7
0.9
83
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1015
43
40
1
1
0 2.9
2.5
0.4
83
5
2.6
1
83
0.1
5
0.5
0.05
0.1
4.5
8.5
(.25
1030
43
40
1
1
1 2.9
2.5
0.4
65
5
2.6
1
85
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
I04S
43
40
1
1
1 2.9
2.5
0.4
85
5.6
2.6
1.05
85
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1100
43
40
1.2
1
1 2.9
2.5
0.4
85
5.6
2.6
1.1
85
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1115
43
40
1.2
1
2 2.9
2.5
0.32
S5
5.6
2.6
1.1
85
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1130
43
40
1.2
1
4 2.9
2.6
0.35
88
5.6
2.6
1.1
88
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1145
43
40
1.2
1
4 2.9
2.6
0.35
88
5.6
2.6
1.1
88
0.1
5
0.5
0.05
C.I
4.5
8.5
0.25
1200
43
40
1.2
1
4 2.9
2.6
0.35
88
5.6
2.6
1.1
88
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
_ 1215
43
40
1.2
1
4 2.9
2.5
0.3
88
5.6
2.6
1.1
88
0.1
5
O.S
0.05
0.1
4.5
8.5
0.25
^ 1230
43
40
1.2
1
6 2.9
2.5
0.3
90
5.6
2.6
1.1
90
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1245
43
40
1.2
1
6 2.9
2.5
0.3
90
5.6
2.6
1.1
90
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1300
43
40
1.2
1
6 2.9
2.5
0.3
90
5.6
2.6
1.05
90
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1315
43
40
1.2
1
6 2.9
2.5
0.3
90
5.6
2.6
1.05
90
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1330
43
40
0.8
1
6 1.5
2.6
9.25
92
5.6
2.6
1
92
0.1
5
0.5
0.05
0.1
4.S
8.5
0.25
1345
43
40
0.8
J
6 1.5
2.6
0.35
92
5.6
2.6
0.95
92
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1400
43
40
0.8
1
6 1.5
2.6
0.35
92
5.6
2.6
0.95
92
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1415
43
40
0.8
1
6 1.5
2.S
0.35
92
5.6
2.6
0.95
92
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
1430
43
40
0.8
1
6 1.5
2.6
0.35
93
5.6
2.6
0.95
92
0.1
5
0.5
0.05
0.1
4.5
8.5
0.25
(1)Wn:
43
40
0.8
1
1 1.5
2.5
0.25
85
5.0
2.6
1.00
85
0.1
5.0
0.5
0.05
0.10
4.5
8.5
0.25
Max;
43
40
1.2
1
6 2.9
2.6
0.4D
92
5.6
2.6
1.10
92
0.1
5.0
0.5
0.05
0.10
4.5
8.5
0.25
Avj:
43
40
1.1
1
4 2.8
2.5
0.33
88
5.6
2.6
1.07
88
0.1
5.0
0.5
0.05
0.10
4.5
8.5
0.25
(1) During Flue 6ss Stapling
-------
Test I Control fan 8-1-89
Flue Gas Stapling 1100 - 1400
Clay Metals Slow-
Feed Feed down Makeup 1N5 INS
Height Height Hater Hater Kiln Kiln AB IKS IKS Inlet Exit Auger Llq. Kiln AB AB AB AB SE SE SE Stack Stack Stack Stack
teadlng Reading Flow Flow Pres. Exit Exit Llq. Bldwn 6as Gas Stack Feed pH 02 02 CO C02 THC 02 THC NOx 02 CO C02 THC
The (lbs) (lbs) (g
-------
Test 4 Bay Area 9-1-89
Flue Gas SwpHng 1100 - 1400 Querch System 1HS APCS
Secondary APCS
Conpres. Mist Spray IKS IKS IMS Carbon Carbon Carbon Carbon
Rota- Feed Pres. Pres. Pres. Air Hater Hater Ionizer Outlet Inlet Purge 2nd Dwtster Bed Exit 1st Bed
wter Pres. Flawrats 1 2 3 Pres. Flow Flow-ate Voltage Pres. Pres. Air Dp HEPA Dp Dp Pres. HEPA Dp T«p.
Tim (totals Metals (gpa) (pel) (pel) (ps1) (psf) (gpn) (gpn) (V) (-in wc) (-1n wc) (-1n «) (-In mc) (-In wc) (-1n «c)(-1n we (*F)
901
18
32
35
35
18
40
3000
1
1
0.4
5.5
0
4
3
158
915
15
18
35
37
38
20
30
3000
1
1
0.4
6
0
3.5
3
156
930
15
18
35
37
37
20
30
3000
1
1
0.4
6
0
3.5
3
158
945
60
5
18
35
37
37
15
35
3000
1
1
0.4
6
0
3.5
3
158
1000
60
4.5
18
35
37
37
15
35
3000
1
1
0.4
6
0
3
2
158
1015
60
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
3
158
1030
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
3
158
1045
18
35
35
35
15
25
3000
1
1
0.4
5.5
0
3
3
158
110Q
60
5
18
35
3T
37
15
25
3000
1
1
0.4
5.5
0
3
3
158
1115
60
5
18
35
37
37
15
25
3000
1
0.4
5.5
0
3
2.5
158
1130
60
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
2.5
158
„ 1145
60
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
2.5
158
* 1200
60
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
2.5
158
1215
CO
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
2.5
158
1230
60
5
18
35
37
37
15
25
3000
1
1
0.4
5.5
0
3
2.5
158
1245
58
5
18
35
37
37
15
50
3000
1
0.75
0.4
6
0
2
3.5
158
1300
60
5
18
35
35
35
15
50
3000
1
0.75
0.4
6.1
0
2
2.5
158
1315
18
35
35
35
15
50
3000
1
0.75
0.4
6
0
2
2.5
158
1330
60
5
18
35
35
35
15
50
3000
1
0.75
0.4
6
0
2
2.5
158
1345
18
35
35
35
10
20
3000
1
1
0.4
7
0.5
3
3
158
1400
60
5
18
35
35
35
15
20
300Q
1.5
1
0.4
7
0.5
3
3
158
1415
18
37
37
37
10
20
3000
1.5
1
0.4
7
0.5
3
3
158
1430
(0
5
18
35
35
35
16
20
3000
1.5
1
0.4
7
0.5
3
3
160
1445
60
5
18
35
35
35
16
20
3000
1.5
1
0.4
7
0.5
3
3
160
1500
18
3*
35
35
10
20
3000
1.5
1
0.4
7
0.5
3
3
160
(1)Nin:
58.0
5.0
18
35
35
35
10
20
3000
1.0
0.8
0.4
5.5
0.0
2.0
2.5
158
Mm:
60.0
S.O
18
35
37
37
16
50
3000
1.5
1.0
0.4
7.0
0.5
3.0
3.5
158
Avg:
59.8
5.0
18
35
36
36
15
32
3000
1.0
0.9
0.4
5.9
0.1
2.7
2.7
158
(1) During Flue Gas Sampling
-------
Test« Gas Twin 8-1-89
Flw Gas Stapling 1030 - 1400 Kiln Kaln Afterburner Haln Kiln Pilot Afterburner Pilot
Total Kiln Gas Gas Kiln AB Gas Gas AB Kiln Kiln Gas Gas AB AB Gas Gas
Air Air Air Air Air Pres. Pres. Gas A1r Pres. Pres. Gas Pilot Aton. Pres. Pres. Pilot Atom. Pres. Pres.
Plenum Static Flo* Tenp. Flow Static Oynoric Temp. Flow Static Dynamic leap. Air Air Static Dyn»1c Air Air Static Dyrwtlc
Tlae (1n wc) (1n *c) (In wc) ( F) (In wc) (psl) (In «c) ( F) (In wc) (psl) (In nc) ( F) (1n wc) (In kc) (1n te) (In wc) (In mc) (In wc) (In wc) (in wc)
901
44
42
1.2
106
4.0
2.5
0.85
2.6
2.7
0.85
0.2
5
0.5
0.05
0.1
5
8.5
0.25
91S
44
42
1.2
106
4.0
2.5
0.4
80
3.6
2.7
0.9
80
0.1
5
0.5
0.05
0.1
5
8.5
0.25
930
44
42
1,2
106
3.8
2.5
0.35
eo
3.6
2.7
90
80
0.1
5
0.5
0.05
0.1
5
8.5
0.25
945
44
42
1
106
3.0
2.5
0.4
80
3.6
2.7
0.9
86
0.1
5
0.5
0.05
0.1
5
8.5
0.25
1000
44
42
1
106
2.0
2.5
0.35
GO
4.6
2.7
0.95
80
0.1
5
0.5
0.05
0.1
5
8.5
0.25
1015
44
42
1
108
2.0
2.5
0.3
80
5
2.7
1
80
0.1
5
0.5
0.05
0.1
5
8.5
0.25
1030
44
42
1
108
2.0
2.5
0.3
82
5
2.7
1
82
0.1
5
0.5
0.05
0.1
5
8.5
0.25
1045
44
40
1
108
2.0
2.5
0.5
82
5
2.7
1.05
82
0.1
5
0.5
O.OS
0.1
7
8.5
0.25
1100
44
40
1
108
2.0
2.5
0.35
82
5
2.5
1.05
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1115
44
40
0.8
108
1.6
2.5
0.3
82
5
2.6
1.05
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1130
44
40
1
108
1.6
2.5
0.25
82
5.6
2.6
1
82
0.1
5
0.5
0.05
0.1
7.1
8.5
0.25
_ 1145
44
40
1
108
2.0
2.6
0.25
82
5.6
2.6
1
82
0.1
5
0.5
O.OS
0.1
7.5
8.5
0.25
1200
44
40
1
108
2.0
2.6
0.25
82
5.6
2.6
1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1215
44
40
1
108
2.0
2.6
0.25
82
5.6
2.6
1
82
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1230
44
40
1
110
2.0
2.6
0.25
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1245
43
40
1
110
2.0
2.6
0.24
84
5.6
2.6
1
84
0.2
5
0.5
0.05
0.1
7.5
8.5
0.25
1300
43
40
1
110
2.0
2.5
0.22
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1315
43
40
1
110
2.0
2.5
0.25
84
5.6
2.6
1
84
0.1
5
0.5
O.OS
0.1
7.5
8.5
0.25
1330
43
40
1
110
2.0
2.5
0.25
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1345
43
40
1
110
2.0
2.5
0.25
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1400
43
40
1
110
2.0
2.5
0.25
81
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1415
43
40
1
112
2.0
2.5
0.5
81
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1430
43
40
1
112
2.0
2.5
0.5
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1445
43
40
1
112
3.0
2.5
0.5
84
5.6
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
1500
43
40
1
114
3.0
2.5
0.5
84
2.7
2.6
1
84
0.1
5
0.5
0.05
0.1
7.5
8.5
0.25
(1)H1n:
43
40
0.8
108
1.6
2.5
0.22
82
5.0
2.5
1.00
82
0.1
5.0
0.5
0.05
0.10
7.1
8.5
0.25
Max:
44
40
1.0
110
2.0
2.6
0.35
84
5.6
2.6
1.05
84
0.2
5.0
0.5
0.05
0.10
7.5
8.5
0.25
Avg:
44
40
1.0
109
1.9
2.5
0.26
83
5.5
2.6
1.01
83
0.1
5.0
0.5
0.05
0.10
7.5
8.5
0.25
(1) During Flue Gas Sampling
-------
Tost 5 Control Ron 8-16-89
Flue 6k Sailing 0900 - 1245
Clay totals Blow-
Feed Feed down Makeup 1HS IMS
Height Height Hater Hater Kiln Kfln A8 IKS IKS [Met Exit Auger Liq. Kiln AB AB AS AB SE SE SE Stack Stack Stack Stack
Reading Raadlng Flow Flow Pres. Exit Exit L1q. Bldwn Gas Gas Stack Feed Bay pH 02 02 CO C02 THC 02 THCHQxW C0CO21HC
T1«b (lbs) (lbs) (gp.) (gp.) (-In *) ('F) («F) CF) {'F) (*F) CO (*F) (*F) (*F) (« (I) (pp) (*) (pp.) (I) (pp.) (pp.) (*) (*) (*) (pp.)
SOS
184.5
20.04
0.5
6.4
0.02
1686 2190
159
141
177
175
170
87
83
7.82 11.8
7.3
5
7.1
2.6 11.2
5.3 41
11.9
5
4.7
0
815
185
20.02
0.5
6.4
0.04
1689 2158
157
143
177
175
70
86
83
7.81 11.1
9.1
5
6.1
2.5 12.3
4.2 40
12.8
5
4.2
0
830
154
34.9
0.5
6.2
0.06
15S1 2106
158
141
176
209
169
89
83
6.16 11.5
8.8
5
6.9
2.5 12
3.8 44
12.5
5
4.8
0
US
117
34.16
0.4
6.4
0.04
1585 2119
158
144
171
191
170
89
84
7.87 10.3
7.9
4
7.6
2.8 11.4
4.1 41
11.9
4
5.2
0
900
81.5
33.56
0.4
6.4
0.04
1622 2106
158
141
176
190
170
89
85
7.13 10.5
8.5
2
7.1
2.5 11.7
3.8 42
12.3
4
4.9
0
915
326.5
31.9
0.4
6.6
0.04
1628 2100
159
141
176
174
169
90
86
7.11 10.6
8.5
6
7.2
2.6 12
4 42
12.4
5
4.9
0
930
290.5
30.74
0.4
6.6
0.035
1613 2108
159
141
176
175
169
90
87
7.48 11.4
8.2
5
7.3
2.7 11.8
3.7 44
12.5
5
5
0
945
252
29.46
0.4
6.6
0.035
1590 2107
159
141
176
174
169
92
88
7.28 11.5
8.6
5
7.2
2.4 11.9
3.6 43
12.4
5
4.9
0.7
tooo
217
28.34
0.4
6.6
0.03
1606 2187
160
141
176
174
169
91
89
7.18 11.1
8
6
7.5
2.8 11.6
3.4 43
12.1
4
5
0
10)5
181
27.22
0.4
6.4
0.03
1626 2130
160
141
176
179
167
91
89
7.47 11.2
8.6
5
7.2
2.8 11.8
3.9 43
12.3
4
4.9
0
55 1030
ISO
26.16
0.4
6.4
0.03
1627 2126
161
141
177
178
170
94
91
7.3 10.7
7.9
6
7.6
2.8 11.6
3.7 42
12.2
5
5
0
IMS
332
24.94
0.4
6.4
0.03
1629 2132
161
141
176
175
170
95
91
7.12 11
8
6
7.5
2.4 11.6
3.8 44
12.2
5
5.1
0
1100
297
23.78
0.4
6.4
0.03
1627 2132
161
141
177
175
170
95
92
7.29 11.3
7.9
5
7.5
2.7 11.6
3.3 44
12.1
4
4.9
0
1115
262
22.64
0.4
6.4
0.04
1625 2133
162
140
176
175
169
95
92
7.25 11.8
7.8
6
7.4
2.4 11.6
3.6 44
12.3
4
5
0
1130
225.5
21.4
0.4
6.4
0.04
1620 2137
162
140
170
174
170
96
92
7.17 11.8
7.9
6
7.5
2.7 11.6
3.6 44
12.1
3
5
0
1145
190
20.12
0.4
6.4
0.03
1632 2138
162
140
177
177
170
96
93
7.51 12.6
7.7
6
7.6
2.8 11.8
3.7 44
12.2
4
5
0
1200
154
18.82
0.4
6.4
. 0.03
1638 2142
162
143
177
175
170
98
94
7.17 12.3
7.6
7
7.9
2.5 11.6
3.6 45
12.1
t
5.1
0
1215
118
17.54
0.4
6.4
0.03
1641 2128
163
141
177
174
170
98
95
7.T 14
8.2
6
7.6
2.5 11.6
3.8 45
12.1
4
5
0
1230
84
16.34
0.4
6.4
0.04
1634 2123
163
140
176
174
16)
98
94
7.2 14.7
8.2
4
7.4
2.8 11.8
3.6 45
12.1
4
5
0
1245
48
15.06
0.4
6.4
0.04
1635 2123
163
140
176
175
169
97
95
7.2 13.9
8.3
4
7.3
2.5 11.8
3.5 44
12.3
7
4.9
0
1300
19.5
13.74
0.4
0.4
0.04
1546 2113
163
139
176
174
169
99
95
7.87 17.7
10
5
5.9
2.6 13.1
3.3 48
13.4
5
4
0
1315
22.5
13.66
0.4
6.4
0.04
1543 2125
164
139
176
174
169
99
95
8.36 16
9.8
5
5.8
2.5 12.8
3.4 42
13.2
5
3.9
0
1330
32.5
13.66
0.4
6.8
8.045
1494 2092
164
138
175
174
168
98
96
7.56 16.1 10.8
4
5.2
2.8 13.5
3.5 37
13.8
3
3.5
0
1345
32.5
13.66
0.4
6.8
0.045
1448 2038
166
138
174
173
167
99
96
7.34 16.3
11
3
5.1
2.8 13.7
3.2 35
13.9
3
3.5
0
(1)Nfn:
48.0
15.1
0.4
6.4
0.03
1590 2100
158
140
170
174
167
89
85
7.1 10.5
7.6
2.0
7.1
2.4 11.6
3.3 42.0
12.1
3.0
4.9
0.0
Max;
332.0
33.7
0.4
6.6
0.04
1641 2187
163
143
177
190
170
98
95
7.7 14.7
8.6
7.0
7.9
2.8 12.0
4.0 45.0
12.5
7.0
5.1
0.7
Avg:
200.6
24.3
0.4
6.5
0.03
1625 2128
161
141
176
176
169
94
91
7.3 11.9
8.1
5.3
7.4
2.6 11.7
3.7 43.8
12.2
4.6
5.0
0.0
(1) During Flue Gas Sailing
-------
Test 5 Bay Area 8-16-19
Flue 6k SaapUng 0900 - 1245 Quench Systan M APCS
Secondary APCS
Compres, Nlst Spray INS IKS IKS Carbon Carbon Carbon Carbon
Rota- Feed Pres. Pres. Pres. Air Hater Hater Ionizer Outlet Inlet Purge 2nd Bealster Bed Exit 1st Bed
¦eter Pres. Flowate 1 2 3 Pres. Flow Flcwrata Voltage Pres. Pres. Air Op HEPA Op Op Pres. HEPA Op Temp.
T1ro totals totals (gpa) (psf) (psf) (ps1) (ps1) (gpm) (gpm) (V) (-1n *c) (~1n tc) (-In tc) (-In wc) (-In tc) (-1n trc) (-tn wc) ( F)
806
IS
37
38
38
55
45
45
9000
1
1
0.4
3
0
0
3.5
160
815
18
36
38
38
55
45
45
9000
1
1
0.4
3
0
0
3.5
160
830
SO
5
18
36
38
38
55
IS
15
9000
1
1
0.4
3
0
0
4
1(0
845
60
4.75
18
36
38
38
55
45
45
9000
2
1.5
0.4
4
0
0
4
160
900
to
4.71
IS
36
38
38
55
45
45
9000
2
1.5
0.4
4.5
0
0
4.5
ISO
iis
60
4.5
18
36
38
38
55
45
45
9000
2
1.75
0.4
4.5
0
0
4.5
160
930
SO
4.S
18
36
38
38
55
45
45
5000
2
1.75
0.4
4
0
0
4.5
160
mi
SO
5
11
3S
31
38
53
38
45
3500
2
1.9
0.4
4.5
0
0
4.5
160
1000
60
S
IB
36
38
38
55
45
45
9500
2
1.75
0.4
5
0
0
4.5
160
1015
SO
S
18
3S
38
38
55
if
45
10000
2.16
1.75
0.4
3.5
0
0
4.5
160
1030
60
S
18
36
38
38
55
45
45
10000
2
1.9
0.4
3.5
0
0
4.5
160
- 1045
SO
5
18
36
38
38
55
45
45
10000
2
1.9
0.4
3.5
0
0
4.5
160
^ 1100
SO
5
18
36
38
38
55
40
45
10000
2
1.75
0.4
3
0
0
4.5
160
1115
60
5
18
36
31
38
55
40
45
10000
2
1.75
0.4
3.5
0
0
4.5
160
1130
SO
5
18
14
35
36
55
38
45
10000
1,9
2
0.4
3.75
0.5
0
4.5
160
1145
60
4.5
18
34
35
36
55
38
45
10000
2
2
0.4
3.25
0.5
0
4.5
160
1200
to
4.5
18
34
36
36
55
38
45
10000
1.9
1.75
0.4
3
0.75
0
4.5
160
1215
so
4.5
11
34
36
36
55
38
45
9000
1.9
1.75
0.4
3.5
1
0
4,5
160
1230
60
4.5
18
34
36
36
55
38
45
8000
2
1.9
0.4
3.5
1
0
4.5
160
rns
SO
4.5
11
34
36
36
55
38
45
7000
2
1.9
0.4
4
1
0
4.5
160
1300
18
34
36
36
55
. 38
45
5000
2
1.9
0.4
4
1
0
4.5
160
1315
18
34
36
36
55
38
45
9500
2
1.9
0.4
4
1
0
4.5
160
1330
18
31
36
36
55
38
45
9500
2
1.9
0.4
4
1
0
4.5
160
1345
18
34
36
36
55
38
45
9500
2
1.9
0.4
4
1
0
4.5
ISO
(l)Nlm
so
4.1
18
34
31
36
53
38
45
7000
1.9
1.5
0.1
3.0
0.0
0.0
4.5
160
Mix:
60
5.0
18
36
38
38
55
45
45
10000
2.2
2.0
0.4
5.0
1.0
0.0
4.5
160
Awf:
60
4.8
18
35
IT
37
55
41
45
9375
2.0
1.8
0.4
3.8
0.3
0.0
4.5
160
(1) During Flue Gas SaapUng
-------
Test S Gas Train 8-16-69
Flb.i Gas Saapling 9900
- 1245
K1In Main
Afterburner Main
Kiln Pilot
Afterburner Pilot
Total
Kiln
Gas
Gas
Kiln
AS
Gas
Gas
AB
Kiln
K11n
Gas
Gas
AS
AS
Gas
Gas
A1r
A1
Air
Air
Air
Pres.
Pres.
Gas
Alt-
Pres.
Pres.
Gas
Pilot
Atoa.
Pres.
Pres.
Pilot
Atoa.
Pres.
Pres.
Plenua
Statl
Flow
Teap.
Flow Static Oynaalc Temp.
Flow Static Oynaalc Teap.
A1r
Air
Static
Oynaalc
Air
Air
Static
Opualc
Tine (In mc) (In wc
(1n m)
(*F) (In wc) (ps1) (1n *c)
(*F) (1n wc) (ps1) (1n wc)
(*F) (In wc) (in wc) (In wc) (1n wc) (1n wc) (In k) (In wc) (in wc)
SG6
44
4
1.2
100
2.0
2.5
0.4
72
6.4
3.3
1.35
72
0.05
4.5
0.5
0.05
0.4
4
6.5
0.2E
SIS
44
4
1.2
100
1.6
2.6
0.2
72
6.5
3.3
1.35
72
0.05
4.5
0.5
0.05
0.4
4.5
8.5
0.25
830
44
4
1.2
100
1.6
2.6
0.2
72
6.4
3.3
1.35
72
0.05
4.75
0.5
0.05
0.4
4.5
8.5
0.25
845
44
4
1.2
102
2.3
2.6
0.2
74
6.4
3.3
1.4
74
0.05
4.75
0.5
0.05
0.4
4.5
8.5
0.25
900
44
4
1.2
102
2.3
2.6
0.2
74
6.4
3.3
1.4
74
0.05
4.75
0.5
0.05
0.4
4.5
8.5
0.25
915
44
4
1.2
104
2.3
2.6
0.2
76
6.4
3.3
1.4
76
0.05
4.75
0.5
0.05
0.4
4.5
8.5
0.25
930
44
4
1.2
104
2.9
2.6
0.2
76
6.4
3.3
1.4
76
0.05
4.75
0.5
0.05
0.4
4.5
8.5
0.25
94S
44
4
1.2
10$
3.0
2.6
0.2
78
6.2
3.3
1.4
78
0.05
4.5
O.S
0.05
0.4
4.5
8.5
0.3
1000
44
4
1.2
10S
3.0
2.6
0.17
78
6.1
3.3
1.45
78
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1015
44
4
1.2
108
3.0
2.6
0.17
78
6.1
3.3
1.45
78
1.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1030
44
4
1.2
108
3.0
2.6
0.17
80
6.2
3.3
1.45
80
8.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
s> 1045
44
4
1.2
108
3.0
2.6
0.17
80
6.2
3.3
1.45
80
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
3 1100
44
4
1.2
110
3.0
2.6
0.17
82
6.2
3.3
1.45
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1115
44
4
1.2
110
3.0
2.6
0.17
82
6.2
3.3
1.4S
82
0.05
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1130
44
4
1.2
110
3.0
2.4
0.17
84
6.1
3.3
1.45
84
0.05
4.5
8.5
0.05
0.4
4.25
8.5
0.25
1145
44
4
1.2
110
3.0
2.4
0.17
84
6.1
3.3
1.45
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1200
44
4
1.2
112
3.0
2.6
0.15
84
6.2
3.3
1.45
84
0.05
4.5
O.S
0.05
0.4
4.25
8.5
0.25
1215
44
4
1.2
112
3.0
2.6
0.15
84
6.2
3.3
1.45
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1230
44
4
1.2
112
3.0
2.6
0.15
84
6.2
3.3
1.45
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1245
44
4
1.2
112
3.0
2.6
0.15
84
6.2
3.3
1.45
84
o.os
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1300
44
4
1.2
112
3.0
2.6
0.35
86
6.2
3.3
1.45
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1315
44
4
1.2
112
3.0
2.6
0.35
86
6.2
3.3
1.45
86
O.OS
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1330
44
4
1.2
112
3.0
2.6
0.35
86
6.1
2.7
1.35
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1345
44
4
1.2
112
3.0
2.6
0.35
86
6.1
2.7
1.35
86
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
(l)H-fn:
44
4
1.2
102
2.3
2.4
0.15
74
6.1
3.3
1.40
74
1.1
4.5
0.5
0.05
0.40
4.2
8.5
0.25
Max:
44
4
1.2
112
3.0
2.6
0.20
84
S.4
3.3
1.45
84
0.1
4.7
0.5
0.05
0.40
4.5
8.5
0.30
Avgr
44
4
1.2
108
2.9
2.6
0.17
80
S.2
3.3
1.44
80
0.1
4.6
0.5
0.05
0.4D
4.3
8.5
0.25
(1) During Flue Gas Saapllng
-------
lest 6 Control Ron 8-15-89
Flue Gas Sanpllng 0945 - 1345
Clay Metals Star-
Feed Feed dan Makeup IMS INS
Height
Halght Hater
Hater
Kiln
Kiln AB
IKS
KS Inlet Exit
Auger
Llq. Kiln
AS
AB
AB
AB
St
SE
SE
Stack Stack Stock Stack
Reading Reading
Flow
Flow
Pres.
Exit Exit Lip. B
dwi Gas Gas Stack Feed Bay
pH 02
02
CO
C02
THC
02
THC
NOx
02
CO
002
THC
(lbs)
(lbs) (gpn)
(gpa) (-In wc) ('F) («F) (*F) (
F) CF) CF) CF)
CF) CF)
(*)
(*) (Pt») (*) (PH")
(*) (ppm) (PP
-------
Test S Bay Area (-15-89
Flue Gas Saoplfng 0945 - 1345 Quench Systea IMS APCS
Ccapres. Mist
Spray
IHS
Rota-
Feed
Pres.
Pres.
Pres.
Air
Hater
Hater
Ionizer
meter
Pres.
Flowate
1
2
3
Pres.
Flow
Flowate Voltage
T1m
Metal6 totals
(gp«)
(psi)
(psi)
(psi)
(psi)
(gp»)
(0P»)
(V)
849
18
38
40
40
55
35
45
9000
900
18
38
40
40
55
35
45
9000
915
57
3.5
18
38
40
40
55
35
45
9000
930
57
3.5
18
38
40
40
55
35
45
9000
945
57
3.5
18
38
40
40
55
35
45
9000
1000
57
3.5
18
38
40
40
55
35
45
9000
1015
57
3.5
18
38
40
40
55
35
45
9000
1030
57
3.5
18
38
40
40
55
35
45
9000
1045
57
3.5
18
38
40
40
55
35
45
9000
1100
57
3.5
18
38
40
40
55
35
45
9000
1115
57
3.5
18
38
40
40
55
35
45
9000
k> 1130
57
3.5
18
38
40
40
55
35
45
9000
1145
57
3.5
IB
38
40
40
55
35
45
9000
1200
57
3.5
18
38
40
40
55
35
45
9000
1215
57
3.5
18
38
40
40
55
35
45
9000
1230
57
3.S
18
38
40
40
55
35
45
9000
1245
57
3.5
18
38
40
40
55
35
45
9000
1300
57
3.5
18
38
40
40
55
35
45
9000
1315
57
3.5
18
38
40
40
55
35
45
9000
1330
57
3.5
18
38
40
40
55
35
45
9000
1345
57
3.5
18
38
40
40
55
35
45
9000
1400
18
38
40
40
55
35
45
9000
1415
18
38
40
40
55
35
45
9000
1430
18
38
40
40
55
35
45
9000
.(1)M1n:
57
3.5
18
38
40
40
55
35
45
9000
Max:
57
3.5
18
38
40
40
55
35
45
9000
Avg:
57
3.5
18
38
40
40
55
35
45
9000
(1) During Flue Qas Saapllng
Secondary APCS
IKS IKS Carbon Carbon Carbon Carbon
Outlet Inlet forge 2nd Denlster Bed Exit 1st Bed
Pres. Pres. Air Dp HEPA Op Op Pres. HEPA Op Tesp.
(-in wc) (-in «c) (-1n wc) (-In mc) (-in wc) (-In nc) (-In mc) (*F)
1
1
0.4
2.5
0
0
3
157
1
1
0.4
3
0
0
3
157
1
1
0.4
3
0
0
2.5
157
1
1
0.4
3
0
0
2.5
158
1
1
0.4
3
0
0
2.5
158
1
1
0.4
3
0
0
2.5
158
1
1
0.4
3.5
0
0
2.5
158
0.5
0.5
0.4
4
0
0
2.5
158
0.5
0.5
0.4
4
0
0
3
158
0.5
0.5
0.4
4
0.25
0
2
158
0.5
0.5
0.4
4
0.25
0
2
158
0.5
0.5
0.4
4
0.25
0
2
158
0.5
0.5
0.4
4
0.5
0
2.2
158
0.5
0.5
0.4
4
0.25
0
2.25
158
0.5
0.5
0.4
4
0.25
0
2.25
157
0.5
0.5
0.4
4
0,25
0
2.25
157
0.5
0.5
0.4
4
0.25
0
2.25
157
0.5
0.5
0.4
4
0.25
0
2.25
157
0.5
0.5
0.4
4
0.25
0
2.25
157
0.5
O.S
0.4
4
0.25
0
2.5
158
0.5
0.5
0.4
4
0.25
0
2.5
158
0.5
0.5
0.4
4
0.25
0
2.5
158
0.5
0.5
0.4
4
0.25
0
2.5
158
0.5
0.5
0.4
4
0.25
0
2.5
158
0.5
0.5
0.4
3.0
0.0
0.0
2.0
157
1.0
1.0
0.4
4.0
O.S
0.0
3.0
158
0.6
0.6
0.4
3.9
0.2
0.0
2.3
158
-------
Test 6 Gas Train 8-15-89
Flue Gas Stapling 0945 - 134$
Kiln Main
Afterburner Main
Kiln Pilot
Afterburner Pilot
Total Kiln Gas Gas Kiln A8 Gas Gas AB Kiln Kiln Gas Gas AS AB Gas Gas
A1r Air A1r Air Air Pres. Pres. Gas Air Pres. Pres. Gas Pilot Atom. Pres. Pres. Pilot Atoo. Pres. Pres.
Dynanfc Te«p. Air Air Static Dynaafc Air Air Static Dynamic
(in wc) (*F) (1n »c) (1n wc) (1n wc) (In ttc) (1n wc) (In nc) (1n nc) (In wc)
Plenufl Static Flow leap. Flow Static Dynaalc Te«p. Flo* Statf
T1ae (1n wc) (1n wc) (In hc) ('f) (1n wc) (psl) (In nc) (*F) (In wc) (psl
849
44
41
0.8
100
1.8
2.5
0.5
76
5.5
7 0.85
76
0.1
4.5
0.5
0.05
0.4
4
8.5
0.25
900
44
41
0.8
102
1.8
2.5
0.25
76
5.3
7 0.85
76
0.1
4.5
0.5
0.05
0.4
J.25
8.5
0.25
915
44
41
0.B
102
1.8
2.5
0.25
76
5.2
7 0.85
76
0.1
4.75
0.5
0.05
0.4
4.25
8.5
0.25
930
44
40
0.7
104
1.6
2.5
0.25
78
5
7 0.8
78
0.1
4.75
0.5
0.05
0.4
4.25
8.5
0.25
945
44
40
0.7
104
1.6
2.55
0.25
78
5
7 0.8
78
0.1
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1000
44
40
0.7
104
1.6
2.5
0.2
78
5
7 0.8
78
O.t
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1015
43
41
0.7
106
1.6
2.6
0.2
78
5
7 0.8
78
0.1
4.75
0.5
0.05
0.4
4.25
8.5
0.25
1030
43
40
O.T
105
1.6
2.6
0.2
80
5
7 0.8
80
0.1
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1045
43
40
0.8
108
1.6
2.6
0.2
81
5
7 0.78
81
0.05
4.5
0.5
0.05
0.4
4.2
8.5
0.25
1100
43
40
0.1
108
1.6
2.6
0.2
81
5
7 0.8
81
0.05
(.5
0.5
0.05
0.4
4.25
8.5
0.25
1015
43
40
0.1
109
1.6
2.6
0.2
81
5
7 0.8
81
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
M 1130
43
40
0.8
110
1.6
2.6
0.2
82
5
7 0.8
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
^ 1145
43
40
0.8
110
1.8
2.6
0.2
82
5
7 0.8
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1200
43
40
0.8
111
1.8
2.5
0.2
82
5
7 0.8
82
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1215
43
40
0.8
110
2.0
2.6
0.2
84
5
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1230
43
40
J.8
110
2.0
2.6
0.2
84
5
7 0.8
84
1.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1245
43
40
0.8
111
2.0
2.6
0.2
84
5
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1300
43
40
0.8
110
2.1
2.6
0.2
84
5
7 0.76
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1315
43
40
0.8
110
2.0
2
0.2
84
5
7 0.76
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1330
43
40
0.8
110
2.0
2.6
0.2
84
4.8
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1345
43
40
0.8
110
2.0
2.6
0.2
84
4.8
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1400
43
40
0.8
110
2.0
2.6
0.35
84
4.8
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1415
43
40
0.8
112
2.0
2.6
0.35
84
4.B
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1430
43
40
0.8
112
2.0
2.6
0.35
84
4.8
7 0.8
84
0.05
4.5
0.5
0.05
0.4
4.25
8.5
0.25
1445
43
40
0.8
112
2.0
2.5
0.4
84
4.8
7 0.98
84
0.05
4.5
0.5
0.05
0.4
4.25
4.5
0.25
(1)Nfn:
43
40
0.7
104
1.6
2.0
0.2
78
4.8
7 0.76
78
0.1
4.5
0.5
0.05
0.40
4.2
8.5
0.25
NlX:
44
40
0.8
110
2.0
2.E
0.3
84
5.0
7 0.80
94
0.1
4.7
0.5
0.05
0.40
4.2
8.5
0.25
Avg:
43
40
0.8
108
1.8
2.6
0.2
82
5.0
7 0.79
82
0.1
4.5
0.5
0.05
0.40
4.2
8.5
0.25
(1) During Flue Gss Sampling
-------
Test 7 Control Rooa 8-9-99
Flue 6as SaapUng 1039 - 1330
Clay Metals Blow-
Feed Feed down Makeup IKS INS
Height Height Hater Hater Kiln Kiln A8 IKS IHS Inlet Exit Auger Llq. Kiln A8 AB AB AS SE SE SE Stack Stack Stack Stack
Reading Reading Flow Flow Pres. Exit Exit Llq. Bldw Gas Gas Stack Feed Bay pH 02 02 CO C02 JHC 02 THC NQx 02 CO C02 THC
T1» (lbs) (lbs) (gpe) (gpa) (-In m) ('F) (*F) (V) (*F) (*F) (*F) (*F) (*F) (*F) (*) (*) (ppa) (t) (pp) (I) («¦) (pf») (I) (« (*) (pp.)
83S
455.5
48.12
0.5
6.2
0.05
15B0 1962
154
147
174
171
166
(4
77
6.25 14
9.6
3
6
0.5 13
3 0
30
13.3
3
3.9
0
845
455.5
48.1
0.5
7
0.05
1582 1971
154
148
175
172
166
65
77
6.28 13.9
9.4
4
6
0.6 13
2 0
31
13.2
4
4
0
900
455.5
48.1
0.5
5.8
0.04
1580 1971
155
145
174
171
166
84
78
7.36 13.9
9.4
5
6 19.2 13
1 0
31
13.2
2
3.9
0.2
915
433
48.1
0.5
5.6
0.05
1621 1961
155
145
176
171
166
84
80
5.87 12.2
7
4
8.3
1.5 11
1 0
36
11.5
3
5.4
0
939
397
46.74
0.5
6
0.06
1629 1965
156
150
175
171
167
85
81
7.85 11.4
8.1
5
7.1
0.2 11
6 0
44
12.3
4
4.8
0
945
404
46.2
0.5
7
0.05
1649 19B0
156
146
175
172
167
87
81
8.79 12.3
8.2
4
8
0.1 11
6 0
41
11.7
2
5.1
0
1000
371.5
45.06
0.5
5
0.045
1646 1996
156
148
175
172
168
87
82
8.63 11.9
7.3
5
7.9
0 11
2 0
45
11.6
3
5.2
0
10)5
338
44.52
0.5
7
0.045
1630 1998
157
148
176
173
167
88
83
8.73 12.3
7.3
4
8
0 11
2 0
36
11.6
3
5.3
0
1030
301
43.34
0.5
6.4
0.05
1637 2006
157
149
175
172
167
8S
83
8.58 12.2
7.2
5
7.5
0 11
2 0
45
11.6
3
5.3
0
K> 1045
254.5
42.2
0.5
5.2
0.055
1620 2014
157
146
176
173
169
89
84
8.52 12.6
7.5
5
7.9
0 11
4 0
44
11.8
3
5.2
0
1100
229
41.02
0.5
6.9
0.055
1612 2017
157
1S1
176
173
168
SO
35
8.5 12.9
7.8
4
7.7
0 11
4 8
45
11.8
4
5.5
0
1115
219
40.24
0.5
6.2
0.045
1704 1947
158
152
176
172
160
89
85
8.82 13.3
7.9
5
8
0 11
8 9
46
12.3
5.1
0
1130
186.5
39.6
0.5
63
0.05<
1594 2007
158
149
176
173
168
90
S6
8.54 12.6
7.3
5
8.3
0 11
4 0
45
11.6
3
5.3
5.8
1145
444.5
38.34
0.5
6.2
0.04
1631 2023
158
148
177
173
168
89
82
8.42 12
7.3
5
8
0 11
3 2.4
46
11.6
3
5.4
0
1200
410
37.22
0.5
6.2
0.045
1629 2033
159
148
177
173
169
90
87
8.37 12.6
7.6
5
7.9
0 11
5 2.9
46
11.9
3
5.4
0
1215
374
31.04
0
6.2
0.05
1615 2032
198
148
177
173
168
90
86
8.34 13
7.5
5
7.8
0 11
5 0
45
11.7
4
5.2
0
1239
337
34.82
0.5
6.2
0.045
1601 2020
159
148
176
173
168
90
87
7.91 12.8
7.8
6
7.8
0 11
6 0
44
11.9
5
5.3
0
1245
300
33.64
0.5
6.2
0.045
1617 2021
159
147
176
172
168
93
88
7.81 12.9
7.9
4
7.7
0 11
7 0
46
11.9
3
5.1
0
1300
265
32.5
0.5
6.2
0.05
1613 2022
159
148
176
173
168
93
88
7.49 12.9
7.9
6
8
0 11
5 0
44
11.8
3
5.3
0
1315
229
31.36
0.5
6.2
0.05
1615 2023
160
148
176
172
168
91
80
7.37 13
7.7
3
7.7
0 11
5 0
44
11.8
3
5.4
0
1330
193
29.98
0.5
6.2
0.05
1617 2027
160
148
176
173
168
92
88
7.21 12.8
7.8
7
7.7
0 11
6 0
44
11.8
5
5.3
0
1345
204
29.96
0.5
6.2
0.05
1650 2063
160
147
176
173
168
93
88
7.31 14.7
9.2
5
6.1
0 12
4 0
43
12.7
5
4.3
0
1400
204.5
29.94
0.5
6.4
0.04
1626 2076
160
154
177
173
168
92
88
7.34 14.8
S.2
6
6.2
0 12
4 0
42
12.6
4
4.2
0
1415
204
29.94
0.5
6.4
0.04
1620 2079
160
148
176
173
168
92
88
7.34 14.8
9.3
5
6.1
0 12
4 0
42
12.6
4
4.2
0
(1)N1n:
1S6.S
30.0
0.0
5.2
0.04
1594 1947
157
146
175
172
160
88
80
7.2 12.0
7.2
3.0
7.5
0.0 11
2 0.0 44.0
11.6
3.0
5.1
0.0
Max:
444.5
43.3
0.5
63.0
0.06
1704 2033
198
152
177
173
169
93
88
8.8 13.3
7.9
7.0
8.3
0.0 11
8 2.9 46.0
12.3
5.0
5.5
5.8
Avg:
288.7
36.6
0.5
10.6
0.05
1623 2015
161
148
176
173
167
SO
85
8.1 12.7
7.6
5.0
7.8
0.0 11
5 0.4 44.9
11.8
3.6
5.3
0.4
(1) During Flue 6ts Saapllng
-------
Test 7 Say Area 8-9-89
Flue Gas Saapllng 1030 - 1330 Quench Systen INS APCS
Compres. Mist
Spray
IHS
Rota-
Feed
Pres.
Pres.
Pres.
Air
Hater
Water
Ionizer
meter
Pres.
Flowrate
1
2
3
Pres.
FIon
Flowrate VoltagB
Tine
Metals Metals
(«P«)
(psl)
(PS1)
(psl)
(psi)
(flpm)
(gp»)
(V)
838
18
38
40
40
35
15
45
845
18
38
42
42
35
20
45
900
18
38
42
42
35
15
45
915
60
5
18
38
42
42
35
15
45
930
60
5
18
38
42
42
35
15
45
945
60
5
18
38
42
42
35
15
45
1000
60
5
18
38
42
42
35
15
45
9000
1015
60
5
18
38
42
42
35
15
45
9000
1030
60
5
18
38
42
42
35
15
45
9000
1045
60
S
18
38
42
42
35
15
45
9000
1100
60
5
18
38
42
42
35
15
45
9000
p 1115
60
S
18
38
42
42
35
15
45
9000
U 1130
60
5
IB
40
42
42
30
20
45
9000
1145
60
5
18
40
42
42
30
20
45
9000
1200
60
5
18
40
42
42
30
20
45
9000
1215
60
4.5
18
40
42
42
30
20
45
9000
1230
60
4.5
18
40
42
42
25
15
45
9000
1245
60
I.S
18
40
42
42
25
15
45
9000
1300
60
4.$
18
40
42
42
25
15
45
9000
1315
60
4.S
18
40
42
42
25
15
45
9000
1330
60
4.5
18
40
42
42
25
15
45
9000
1345
18
40
42
42
25
15
45
7000
1400
18
40
42
42
25
15
45
5000
1415
18
40
42
42
25
15
45
6000
(1}mn:
60
4.5
18
38
42
42
25
15
45
9000
Max:
60
5.0
18
40
42
42
35
20
45
9000
Avg:
60
4.8
18
39
42
42
30
17
45
9000
(1) during Flue Gas Saapllng
Secondary APCS
IHS 1HS Carbon Carbon Carbon Carbon
Outlet Inlet Purge 2nd Dewtster Bed Exit 1st Bed
Pres. Pres. Air Op HEPA Op Op Pres. HEPA Op Temp,
(-in nc) (-In wc) (-1n wc) (-In wc) (-1n «c) (-1n wc) (-In wc) (*F)
1
0.4
6.5
0
1.5
3
156
1
0.4
6.5
0
1.5
3
156
1
0.4
7
0
1.5
3
156
1
0.4
5
0
1
2.5
156
1
0.4
5.5
0
1
2.5
156
1
0.4
5
0
0.5
2.5
158
1
0.4
5
0
0.5
2.5
158
1
0.4
5
0
0
2.5
158
1
0.4
4.5
0
0
2.5
159
1
0.4
5
0
0
2.5
159
0.4
5.5
0
0
2.5
159
1
0.4
5
0
0
2
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0
0
2.5
159
1
0.4
5.5
0.5
0
2.5
159
1
0.4
5.5
0.5
0
2.5
159
1
0.4
5.5
0.5
0
2.5
159
0.5
0.4
5.5
0.5
0
2.5
159
0.5
0.4
5.5
0.5
0
2.5
159
0.5
0.4
5.5
0.5
0
2.5
159
0.0
0.4
4.5
0.0
0.0
2.0
159
1.0
0.4
5.5
0.5
0.0
2.5
159
0.9
0.4
5.3
0.1
0.0
2.5
159
-------
lest 7
Train
8-9 89
Flue Gas Samp)
ng 1030
- 1330
Kiln Main
Aft Grimmer Main
Kiln Pilot
Afterburner Pilot
Total
Kiln
Gjs
Gjs
Ki In
m
G)
-------
Test 8 Control Roon 8-11-89
Flue Gos Sampling 0830 - 1215
Clay Metals Blow-
Fend Feed dowi Makeup IHT> 1N!i
Weight
Keiqht Hater
Hater
Kiln
HI In M
IMS
m Inlet Exit
Auqer
liq. Kiln
/IB
m
AB
AD
S£
5E
SE
Stack Stack Stack Stack
Reading Reading
Flow
Flow
Pres.
Exit Fxit l.lq.
Blriwn Gos Cor
Stock feed Bay
P«
02
0?
CO
C02
THC
02
THC
NOx
02
CO(2)
C02
THC
Tim?
(lbs)
(lbs) (grn)
(gpn) {-In «) fF) (*F) (*F) (*F)
Cf) m
-------
Test 8 8ay Area 8-11-89
Tlue Gas Sampling 0830 - 1215 Quench Systea 1WS APCS Secondary APCS
Coopres. Hist Spray ItG INS IMS Carbon Carbon Carbon Carbon
Rota- Feed Pres. Pres. Pres. Air Hater Mater loolier (Xitlet Inlet Purge 2nd Demlster Bed Exit 1st Bed
jeter Pres. Flowrate 1 2 3 Pres. Flow Flowrato Voltage Pres. Pres. Air Op HEP/ Op Dp Pres. HEPA Op Tenp.
Time Metals totals (gpn) (psi) (psi) (psi) (psl) (flpm) (gpn) (V) (-1n wc) (-in wc) (-1n wc) (-1n wc) (-1n wc) (-In wc) (-In wc) (*F)
740
18
46
48
48
55
35
45
9000
1
1
0.4
4.5
0
0.5
3
158
fiOO
60
4.5
19
46
48
48
55
35
45
9000
1
1
0.4
5
0
0
3
158
815
SO
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5
0
0
3
158
830
60
4.5
16
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
159
845
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
159
900
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
6
0
0
3
159
915
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
159
930
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5.S
0
0
3
159
945
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
6
0
0
2.5
159
1000
60
4.5
18
46
48
4B
55
35
45
9000
1
1
0.4
5
0
0
3
15S
1015
60
4.5
18
46
48
4B
55
35
45
9000
1
1
0.4
5
0
0
2.5
159
kj 1030
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
159
60 1045
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5
0
0
3
159
1100
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5
0
0
3
160
1115
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
160
1130
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
6
0
0
3
ISO
1145
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
6
0
0
3
160
1200
60
4.5
18
46
43
48
55
35
45
9000
1
1
0.4
6.5
0
0
3
160
1215
60
4.5
18
46
48
48
55
35
45
9000
1
1
0.4
6.5
0
0
2.5
160
1230
18
46
48
48
55
35
45
9000
1
1
0.4
6.5
0
0
3
160
1245
18
46
48
48
55
35
45
9000
1
1
0.4
6.5
0
0
3
160
1300
18
46
48
48
55
35
45
9000
1
1
0.4
5.5
0
0
3
160
1315
18
46
48
48
55
35
45
3000
1
1
0.4
6
0.5
0
3
140
(l)Nin:
60
4.5
18
46
43
48
55
35
45
9000
1.0
1.0
0.4
5.0
0.0
0.0
2.5
159
Max:
60
4.5
18
46
48
48
55
35
45
9000
1.0
1.0
0.4
6.5
0.0
0.0
3.0
160
Avq:
60
4.5
18
46
48
48
55
35
45
9000
1.0
1.0
0.4
5.6
0.0
0.0
2.9
159
(1) During Flue Gas Sacpling
-------
Test 8 Gk Train 8-11-89
Flue Gas Sampling 0830 - 1215 Kiln Main Afterburner Main Kiln Pilot Afterburner Pilot
Total Kiln Gas Gas Kf in Afl to to Kiln Kiln Gas Gas A8 AS Gas Gas
Air Air Air Air Air Pres. Pres. Gas Air Pres. Pres. Gas Pilot Atom. Pres. Pres. Pilot Atom. Pres. Pres.
Plenun Static Flow Temp. Flow Static Dynamic Tetip. Flo* Static Dynarlc Temp. Air Air Static Dynamic Air A1r Static Dyiwnic
Tine (in wc) (In wc) (in wc) (*F) (in *c) (ps1) (in wc) (*F) (In wc) (psi) (in wc) (*F) (in «) (in nc) (in wc) (in wc) (in «) (in wc) (in wc) (in wc)
740 45
42
1
94
2.0
2.5
0.45
66
5.8
2.6
1
66
0.1
5
0.5
0.05
0.4
5
8.5
0.25
800 45
42
1
94
2.0
2.55
0.25
66
5.8
2.6
1
66
0.1
5
0.5
0.05
0.4
5
8.5
0.25
815 45
42
1
96
1.6
2.6
0.25
611
5.8
2.6
1
66
0.1
5
0.5
0.05
0.4
5
8.5
0.25
830 45
42
1
96
1.6
2.6
0.2
70
5.8
2.6
1
70
0.1
5
0.5
0.05
0.4
5
8.5
0.25
845 45
42
1
96
1.6
2.6
0.2
70
5.8
2.6
1
70
0.1
5
0.5
0.05
0.4
5
8.5
0.25
900 44
42
1
96
1.6
2.6
0.2
70
5.8
2.6
1
70
0.1
5
0.5
0.05
0.4
5
8.5
0.25
915 44
42
1
96
1.4
2.6
0.2
70
5.8
2.6
1
70
0.1
5
0.5
0.05
0.4
5
8.5
0.25
930 44
42
1
100
1.4
2.6
0.2
70
5.8
2.6
1
70
0.1
5
0.5
0.05
0.4
5
8.5
0.25
945 44
42
1
100
1.4
2.6
0.2
74
5.8
2.6
1
74
0.1
5
0.5
0.05
0.4
5
8.5
0.25
1000 44
42
1
100
1.4
2.6
0.2
74
5.B
2.6
1
74
0.<
5
0.5
0.05
0.4
5
8.5
0.25
1015 44
42
1
100
1.4
2.6
0.2
74
5.8
2.6
1
74
0.1
5
0.5
0.05
0.4
5
8.5
0.25
1030 44
42
1
106
1.4
2.6
0.2
77
5.8
2.6
1
77
0.1
5
0.5
0.05
0.4
5
8.5
0.25
>o 1045 44
42
1
106
1.4
2.6
0.2
77
5.8
2.6
1
77
0.1
5
0.5
0.05
0.4
5
8.5
0.25
1100 44
41
1
106
1.4
2.6
0.2
79
5.8
2.6
1
79
0.1
5
0.5
0.05
0.4
5
8.5
0.25
1115 44
41
1
106
1.4
2.6
0.2
79
5.8
2.6
1
79
0.1
5
0.5
0.05
0.4
5
8.5
0.25
1130 44
40
o.e
108
1.4
2.6
0.15
82
5.9
2.6
1.05
82
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
1145 44
40
0.8
108
1.4
2.6
0.15
82
5.9
2.6
1.05
82
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
1200 44
40
0.8
108
1.4
2.6
0.15
82
5.9
2.6
1.05
82
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
1215 44
40
0.8
10B
1.4
2.6
0.45
82
5.9
2.6
1.05
82
0.)
5
0.5
0.05
0.4
4.5
8.5
0.25
1230 44
40
0.8
110
1.4
2.6
0.45
84
5.9
2.6
1.05
84
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
1245 44
40
0.8
110
2.2
2.6
0.35
84
4.8
2.6
1
84
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
1300 44
40
0.8
110
2.2
2.6
0.25
84
4.8
2.8
0.55
84
0.1
5
0.5
0.05
0.4
4.5
8.5
0.25
(1)M1n: 44
40
0.8
96
1.4
2.6
0.15
70
5.8
2.6
1.00
70
0.1
5.0
0.5
0.05
0.40
4.5
8.5
0.25
Max: 45
42
1.0
108
1.6
2.6
0.45
82
5.9
2.6
1.05
82
0.1
5.0
0.5
0.05
0.40
5.0
8.5
0.25
Avg: 44
41
M
102
1.4
2.6
0.21
76
5.8
2.6
1.01
76
0.1
5.0
0.5
0.05
0.40
4.9
8.5
0.25
(1) During Flue G» Saapllng
-------
Test 9 Control Roan 7-28-19
Flue Gas Sampling 1230 - 1650
Clay Mstals Blow-
Feed Feed down Makeup INS IHS
Height Height Hater Hater Kiln Kiln AS lift IHS Inlet Exit Auger Llq. Kiln AS Afl A8 AO SE 5F. SF. Stack Stack Stack Stack
Reading Reading Flow Flow Pres. Exit Exit Llq. Bldwi Gas Gas Stack Feed ptl 02 02 CO C02 1IIC 02 1HC NOx 02 CO C02 THC
fine (lbs) (lbs) (gm) (gpn) {-in wc) (*F) (*F) (T) (T) (*F) ('F) (*F) (*F) (*F) (*) (t) (mm) (W («») (V (Pf«) (pp) W (I) (I) («*)
945
1306
50.76
0.5
5.8
0.05
1734 2058
165
150
179
175
169
:rr=zss?rs::
109 11.45
12.7
7.7
6
)
0
11.4
39
12.1
S
3.7
0
1000
1302.5
50.00
0.5
5.8
0.04
1534 2020
166
152
177
171
168
109
11.61
15.1
9.8
6
6
1.9
13
34
13.5
9
3.2
0
1015
1279.5
50.88
0.5
5.8
8.04
1558 1984
166
151
178
174
166
111
11.57
14
8.1
6
/.1
1.6
11.6
30
12.4
10
4
0
1030
1242
50.84
0.5
5.8
0.04
1589 1980
167
153
178
171
168
110
11
13.e
8.4
7
7.4
1.5
11.9
31
12.4
9
4.3
0
1015
1207.5
50.16
0.5
5.8
0.05
1611 1972
167
151
177
173
166
111
10.14
13.6
8.4
5
7.3
1.3
12
4?
12.6
14
4.4
0
1100
117
48.96
0.5
5.8
0.05
1488 1969
168
149
177
173
165
107
9.69
16.4
10.4
5
5.4
1.5
13.1
44
13.5
9
3.5
0
IMS
1192.5
48.74
o.s
5.8
0.05
1654 1990
168
150
178
174
165
107
9.62
14.6
8
27
6.6
0.9
11.8
53
12.4
9
4.1
0
1130
1161.5
40.79
0.5
5.8
0.05
1599 2004
168
150
179
174
166
108
9.43
13.7
7.3
6
8
0.8
11.1
4.8
36
11.8
9
5.1
1.7
1145
1129.5
47.96
0.5
5.8
0.05
1626 2011
168
151
179
174
166
108
9.21
14.2
7.6
6
7.8
1.2
18.7
1.8
S3
11.9
8
5.1
1.9
1200
1095
46.B8
0.5
5.8
0.04
1619 2023
169
152
180
175
166
109
9.02
13.9
5.6
7
8.7
1.2
10
1
52
11.1
9
5.5
1.4
1217
1060.5
45.58
0.5
5.8
0.05
1608 2018
169
153
179
174
167
109
8.85
14.2
7.8
7
7.3
1.4
17.6
1.1
49
12.2
9
4.9
1.4
1230
1033.5
44.7
0.5
5.8
0.05
1623 1918
169
156
180
174
167
110
8.75
14.7
7.9
6
7.6
1.4
11.6
0.6
51
12
9
5.1
1.4
1245
1033.5
44.1
0.5
5.8
0.08
1532 1961
169
151
178
173
166
110
8.13
16.1
9.8
6
5.8
1
12.8
0.6
43
13.1
9
3.9
1.4
1300
1007.5
44.08
O.S
5.8
0.08
1543 1965
169
149
177
172
166
110
8.75
16
10
7
5.6
1.1
13
0.6
42
13.2
9
3.0
1.4
1315
973.5
43.12
0.5
5.8
0.08
1598 1952
159
149
178
173
166
111
8.(3
14.9
8.2
6
7.3
1.4
11.6
0.6
53
12
10
4.8
1
1330
992
42
0.5
5.4
0.055
1618 1968
170
150
170
173
166
112
B.51
15.3
8
6
7.4
1.4
11.5
0.6
51
12
10
5.1
0.8
1350
1204
40.12
0.5
5.8
0.053
1604 1980
170
150
178
174
157
115
8.31
15.9
8.4
7
6.9
1.9
11.7
3
50
12.1
9
4.8
0.7
MOO
1186.5
39.48
0.5
5.2
0.03
1568 1977
170
150
170
173
167
114
8.3
15.8
8.1
7
7.3
2.3
11.5
4.9
47
12.1
10
5.1
0.8
1415
1151.5
38.22
0.5
5.4
0.03
1623 1904
170
ISO
178
174
167
114
8.22
14.3
7.7
7
7.3
5.3
11.3
0
49
11.7
9
5.1
0.8
1430
118
37.02
0.5
5.4
0.04
1640 19D6
170
150
170
173
167
113
8.14
14.4
7.9
6
7.6
9.4
11.3
0
50
11.8
11
5.1
0.6
1445
1084
35.82
0.5
5.4
0.03
1629 1972
170
150
178
174
167
116
8.08
11.3
7.8
6
7.7
4.9
11.2
0
49
11.8
9
5.3
0.07
15D0
1046
34.64
0.5
5.8
0.03
1643 1991
170
150
178
173
167
118
8.03
14.4
11.2
0
50
11.7
9
5.2
0.7
1520
1048
33.98
0.5
5.8
0.05
1696 1996
170
149
178
173
I6S
115
8.19
15.6
7.6
6
7
4.6
11.4
2.4
46
11.8
9
4.6
0.6
1530
1008
33.5
0.5
5.8
0.05
1620 2004
170
149
178
173
167
115
0.1
14.3
7.5
8
7.8
S.I
11.3
4.1
49
11.8
9
5.1
0.5
1545
974
32.24
0.5
5.8
0.05
1645 2000
170
150
178
173
167
116
7.96
14.4
7.8
11.8
7.9
5.2
11.3
4.1
48
11.9
10
5.2
0.4
1600
951.5
31.14
0.5
5.8
0.04
1541 2001
170
156
179
174
167
116
7.84
14.2
7.5
10
7.8
5.7
11.7
3.7
48
11.7
8
5.3
0.4
1615
918.5
29.9
0.5
5.8
0.05
1582 1996
170
ISO
177
173
167
116
7.8
14.9
8.3
11
7.2
7.3
11.8
3.8
49
12.2
11
5
O.S
1630
29.18
0.5
5.8
0.05
1709 2004
1/0
149
178
173
166
116
7.88
14.0
7.0
9
6.8
1.7
11.5
1.6
45
11.9
10
4.5
0.4
1650
905.5
29.14
0.5
5.0
0.05
1342 2010
170
149
177
173
167
114
7.95
15.5
0.7
7
6.3
1.5
11.9
1.7
42
12.4
10
4.2
0.4
-------
Test 9 Control Rood 7-28-89
Flue Gas Sampling 1230 - 1650
Clay Metals Blow-
Feed Feed dam Makeup IH5 INS
Height Height Hater Hater Kiln Kiln M IHS INS Inlet Exit kiqcr Llq. Kiln A9 AS A8 AB SE 3E SE Stack Stack Stack Stack
Reading Reading Flow Flow Pres. Exit Exit l.i'q. Bldwn Gas Gas Stack Feed pH 02 02 CO C02 THC 02 THC NOx 02 CO C02 THC
T1w> (lbs) (lbs) (gpnj (gp«) (-In wc) ('F) fF> CF) (*F) ('F) (*FJ ('F) (*F) (*F) (*) (\) (ppn) (\) (ppn) (I) (ppn) (ppn) (») (\) (I) (ppn)
1700
905
29.H
0.5
5.8
0.05
1449 1943
170
149
172
169
167
114
8.01
16.5
14.7 8
3.1
1.5
15.0
2 30
16.1
10
2.2
0.1
1715
905
29.06
0.5
5.8
0.08
1182 1628
164
146
167
162
160
112
8.16
18.2
15.7 8
2.4
1.1
17
2.4 10
16.9
10
1.8
0.1
1730
0
0
0.5
5.8
0.09
1015 1424
159
143
161
157
156
107
8.74
18.8
17.1 527
1.7
1.2
18
13.3 4
17.9
380
1.3
0.3
(1)M1n:
118.0
29.1
0.5
5.2
0.03
1532 1918
169
149
177
172
166
110
7.8
14.2
7.5 6.0
5.6
1.0
11.2
0.0 42.0
11.7
8.0
3.8
0.1
Max:
1242.0
50.8
0.5
5.8
0.08
1709 2023
170
156
180
175
168
118
11.0
16.4
10.4 27.0
8.7
9.4
18.7
4.9 53.0
13.5
14.0
5.5
1.9
Avg:
993.7
40.4
0.5
5.7
0.05
1613 1986
169
151
170
173
166
112
8.6
14.8
8.1 7.9
7.2
2.8
12.1
1.9 47.0
12.1
9.5
4.0
0.7
(1) Our^ng Flue Gas Sampling
u>
-------
Test 9 8ay Area 7-28-89
Flue 6as Sampling 1230 - 1650 Quench System IMS APCS
Secondary APCS
Compres. Nlst
Spray
IK>
IHS
Carbon
Carbon
Rota-
Feed
Pres.
Pres.
Pres.
Air
Hater
Hater Ionizer
(Xitlet
Inlet
Purge
2nd
Demister Bed Exit
1st
Bed
meter
Pres.
Flowate
1
2
3
Pres.
Flow
Flowrata Voltage
Pres.
Pres.
Air Dp
HEPA Dp
op
Pres.
HEPA Op
T««p.
Titne
Metals Metals
(gpn)
(PSl)
(Ps1)
(ps1)
(psi)
(0Pr») (V)
(-in wc) (-in wc) (-in wc) (-in wc) (-in wc) (-in nc) (-in wc) ("F)
930
20
18
38
38
39
39
28
40
1
1
0.4
7.5
0.5
4
3
160
945
20
18
38
38
39
39
28
40
1
1
0.4
7
0.5
4
3
160
1000
20
18
38
38
40
39
28
40
1
1
0.4
7
0.5
3.5
2.5
158
1015
20
18
38
38
40
39
28
40
1
1
0.4
9
0.5
3
2.5
158
1030
20
18
40
40
40
39
28
40
1
1
0.4
11
0.5
3
2.5
158
1045
60
4
18
40
40
41
39
28
50
1
1
0.4
11.5
0.5
3
2.5
158
1100
60
4
18
40
40
41
39
28
50
1
1
0.4
11
0.5
2.5
2
157
1115
18
40
40
41
39
28
50
1
1
0.4
10
0.5
2
2
157
1130
18
40
40
41
39
28
50
1
1
0.4
10.5
0.5
2
2
158
1145
60
4
18
40
40
40
38
28
50
0.6
0.5
0.4
10
0.4
1.5
1.5
158
1200
60
4
18
40
40
40
38
28
51
0.6
0.5
0.4
10.4
0.4
1.5
1.5
158
1215
60
4
18
40
40
40
38
28
51
0.6
0.5
0.4
12
0.4
1.5
2
158
1230
60
4
18
40
40
41
38
28
51
0.5
0.5
0.4
10.5
0.5
1.5
2
158
1245
18
40
40
42
38
28
50
1
0.5
0.4
9
0.5
1.5
2.2
157
1300
18
40
40
40
38
25
51
1
0.5
0.4
9.1
0.5
2
2
156
1315
60
4
18
40
40
40
38
25
51
1
0.5
0.4
7
0.5
2
2
156
1330
60
4
18
37
40
40
38
28
51
1
0.5
0.4
7
0.5
2
2
158
1400
60
4
18
40
40
40
58
28
51
1
0.5
0.4
7
0.5
2
2
158
1445
60
4
18
40
40
40
38
28
51
1
0.5
0.4
7.5
0.5
1.5
2
158
1430
60
4
ie
40
40
40
38
28
51
1
0.5
0.4
8
0.5
2
2
157
1445
60
4
18
40
40
40
38
28
51
1
0.5
0.4
8
0.5
2
2
157
1500
60
4
18
40
40
40
38
28
51
1
0.5
0.4
7.5
0.5
2
2
157
1530
60
2.5
ie
36
36
40
40
0
50
1
0.5
0.2
7.5
0.4
1.8
2
157
1545
60
3
18
30
36
40
40
0
50
1
0.5
0.2
7.5
0.4
1.8
2
157
1600
60
3.5
18
36
36
40
40
25
51
1
0.5
0.4
7.5
0.4
2
2
158
1615
60
3.5
18
36
36
40
40
25
50
1
0.5
0.4
7
0.3
2
2
157
1630
ie
35
35
37
40
25
50 3000
1
0.5
0.4
7
0
2
2
158
1645
18
35
35
40
38
50
1
0.5
0.4
7.S
0
2
3
157
-------
Test 9 Cont'd Bay Area 7-28-89
Flue Gas SawpHng 1230 - 1650 Quench System INS APC8
Secondary APCS
Compres. Hist
Spray
IHS
IH3
Carbon
Carbon
Rota-
Feed
Pres.
Pres.
Pres.
A1r
Hater
Hater
Ionizer
Outlet
Inlet
Purge
2nd
Demlster Bed Exit
1st Bed
netcr
Pres.
Flwrate
1
2
3
Pres.
Flow
Flowrate Voltage
Pres.
Pres.
Air Dp
HEPA Op
Op
Pres.
HEPA Dp Temp.
Time
Metals Metals
(BP")
(Ps1)
(ps1)
(Psl)
(Ps1)
(flpm)
(V)
(-in wc) (-In wo) (-In wc) (-In wc) (-In wo) (-in mc) (-In tuc) ( F)
1700
18
35
35
40
3D
60
3000
1
0.5
0.4
7.5
0
2
2 158
1715
18
35
35
40
38
60
1
0.5
0.4
8.2
0
2.5
2.5 158
1730
18
35
35
40
35
25
60
1
0.5
0.4
8.2
0
3
3 156
(1)N1n:
0.0
0.0
18
30
35
37
38
0
50
3000
0.5
0.5
0.2
7.0
0.0
1.5
2.0 156
Max:
60.0
4.0
18
40
<0
42
5ft
28
51
3000
1.0
0.5
0.4
10.5
0.5
2.0
3.0 158
Avg:
51.4
3.2
18
38
38
40
40
23
51
3000
1.0
0.5
0.4
7.8
0.4
1.9
2.1 157
(1) During Flue 6as Sanpllng
U1
U1
-------
Test 9 Gas Train 7-28-39
Flue Gas Sampling 1230 - H5C
Kiln Main
Afterburner Main
K11n Pilot
Afterburner Pilot
Total Kiln Gas Gas K11n A8 Gas Gas AS Kiln Kiln Gas Gas AS A8 Gas 0)S
Air A1r A1r A1r A1r Pres. Pres. Gas A1r Pres. Pres. Gas Pilot Atom. Pres. Pres. Pilot Atoa. Pres. Pres.
Planus Static flat Temp. Flow Static Oynanfc Tsrp. flow Static Oynasic Tetp. Air Air Static Oynaalc Air Air Static Oynanlc
Hue (1n «c) (1n nc> (In m) (*F) (In w) (psl) (1n wc) (*F) (in wc) (psl) (in wc) (*F) (In nc) (in wc) (1n *c) (In we) (In tc) (1n *c) (In wc) (In wc)
1045
43
40
1
110
3.7
2.5
0.3
84
4
2.7
0.8
84
0.1
4.8
O.S
0.05
0.1
4.8
8.4
0.25
1100
43
40
0.8
110
2.6
2.S
0.3
85
4
2.7
0.85
85
0.1
4.7
0.5
0.05
0.1
4.8
8.4
0.25
i:is
43
40
0.8
111
2.6
2.5
0.5
4
2.7
0.9
0.1
4.7
0.5
0.05
0.1
4.8
8.4
0.25
1130
42
3)
0.7
112
2.2
2.55
0.33
06
4
2.7
0.88
86
0.05
4.8
O.S
0.05
0.05
4.8
6.4
0.25
1145
42
39
0.5
113
1.0
2.55
0.25
66
4
2.7
0.91
86
0.05
4.8
0.5
0.05
0.05
4.8
8.4
0.25
1200
42
39
0.25
113
1.0
2.6
0.25
87
4
2.7
0.88
87
0.06
4.5
0.5
0.05
0
4.6
8.4
0.25
1215
42
39
0.6
1.0
2.6
0.2
4.1
2.7
o.e
0.09
4.5
0.5
0.05
0.05
4.8
8.4
0.25
1230
42
39
0.6
114
1.0
2.6
0.3
89
4.1
2.7
0.9
89
0.1
4.5
0.5
0.05
0.1
4.8
8.5
0.25
1245
42
39
o.os
114
1.0
2.5
0.4
87
4.1
2.7
0.81
89
0.1
4.5
0.5
0.05
0.1
4.6
8.4
0.25
1300
42
39
0.6
114
1.0
2.5
0.4
90
4.1
2.7
0.65
90
0.1
4.5
0.5
0.05
O.OS
4.8
8.4
0.25
1315
42
39
0.6
116
1.0
2.6
0.3
90
4.1
2.7
0.83
90
0.1
4.5
0.5
0.05
0.05
4.8
8.4
0.25
1345
42
39
0.6
116
1.0
2.6
0.25
4.1
2.7
0.83
0.1
4.5
0.5
0.05
0.05
5
8.4
0.25
1400
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.83
0.1
4.5
0.5
0.05
0.05
4.8
8.4
0.25
1415
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.83
0.1
4.5
0.5
0.05
0,05
4.7
8.4
0.25
1430
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.85
0.1
4.5
0.5
0.05
0.1
4.7
8.4
0.25
1145
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.85
0.2
4.5
O.S
0.05
0.1
4.7
8.4
0.25
1500
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.85
0.2
4.5
0.5
0.05
0.1
4.7
8.4
0.25
1530
42
39
0.7
116
1.0
2.6
0.25
92
4.1
2.7
0.85
92
0.2
4.5
0.5
0.05
0.1
4.7
8.4
0.25
1545
42
39
0.7
116
1.0
2.5
0.25
4.1
2.7
0.85
0.2
4.5
0.5
0.05
0.1
4.7
8.4
0.25
1500
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.85
0.1
4.5
0.5
0.05
0.1
4.8
8.4
0.25
IE 15
42
39
0.7
116
1.0
2.6
0.25
4.1
2.7
0.95
0.1
4.5
0.5
0.05
0.1
4.6
8.4
0.25
1630
42
39
0.7
116
1.0
2.5
0.52
4.1
2.7
0.85
0.1
4.5
0.5
0.05
0.1
4.2
8.5
0.25
1555
42
39
0.7
116
1.0
2.5
0.45
05
4.1
2.7
0.85
85
0.1
4.5
0.5
0.05
0.1
4.8
8.5
0.25
1700
42
39
0.7
116
1.0
2.5
0.24
4.2
2.7
0.4
0.1
4.5
0.5
0.05
0.1
4.8
8.5
0.25
1715
43
49
0.5
112
2.0
2.6
0.2
5.2
2.8
0.4
0.1
4.5
0.5
0.05
0.1
5
8.5
0.25
1730
43
40
0.5
112
2.0
2.6
0.2
5.2
2.8
6.4
0.1
4.5
6.5
0.05
0.1
5
8.5
0.25
(1)M1n;
42
39
0.1
114
1.0
2.5
0.20
65
4.1
2.7
0.65
85
0.1
4.5
0.5
0.05
0.05
4.2
8.4
0.25
Max:
42
3)
0.7
116
1.0
2.6
0.52
92
4.1
2.7
0.85
92
0.2
4.5
0.5
0.05
0.10
5.0
8.5
0.25
Avg:
42
39
0.6
116
1.0
2.6
0.30
89
4.1
2.7
0.83
89
0.1
4.5
0.5
0.05
0.08
4.7
8.4
0.25
(1) During Flue Gas Saopllng
-------
Appendix A-2
Operating Data Plots
35
-------
TEST 1 (8/17/89)
OPERATION, EVENTS AND S/WPUNG
scnbber exit \OST 1—1 1—11—1
aftertxnrer V05T 1—1 I—11—1
stack N5 1 1
scnJ±er exit M5 1 —¦ !
aftfrti impr M17 I I
12
6
afterburner 02 (%)
11CD
1050
afterburner temp (Cj ^v
* 8
kiln 02
_J
kiln temp (df L
10
0
1 *\
metal fed (I) + + + + \
i ii 4- * _ \
325
0-
ddD^-DDDU
clay/organic fed (kgV. q D D
DpQ j | - | | .
8 10 12 H
Time of Day (hr)
36
-------
IEST 2 (8/2/89)
OPERATION, EVENTS AND SAMPLING
H H
feed Internets
scniter exit MUST
afterburner \GST
stack M5
scniter exit
I aftatLEDBLtilZ
breaker tripped
qterburner 02 (%)
inspected sanpling prcte
fi;rburner temp (C)
kjln
metal fed (I)
njorganic fed jf kaL n D ~ ~ D
Time of Day (hr)
37
-------
TEST 3 (8/4/89
OPERATION, EVENTS AND SAMPUNG
-IM
11
5
1125
feed intempts
scniaber.exit WET
afterbamer YDSI
stack NB
scniiher exit ^
—I afterturrET M17
• ifterburner 02 (X)
3 terburner temp (C)
w(c)
225
metal fed (I) , + + +
1—h H±-*
a
o
^/organic fed (kg) Q q D d
-0 1 ~ n
i
11
13
Time of Day (hr)
38
15
-------
TEST 4 (8/1/89)
OPERATION, EVENTS AND SAMPUNG
feed iitempts HI 1 l—1 H
stack W3ST 1 1 1 1 1 I
scrubber exit VOST HH HH 1—1
afterburner VG5T 1 1 1—H 1—1
stack N5 1 1
scnttifir exit h© | 1
afterburner M17 | — ——j
12
A
dlefburJr^pP^^
Vw^-
nyj
1000
ofterburner temp (C)
^^
17
8
kiln 02 (%) ^
9lb~
800
kiln temp
V—
;C)
"1
7
0
metal fed
/ +++++++
+ + + +
0) . *+t+' + +
250
n
' ' ~dooddd U
0D»°°
clay/orgonic fed (kg) D fflfl ^
D iDD " | | | | |
Time of Day (hr)
39
-------
TEST 5 (8/16/89)
OPERATION, EVENTS AND SAMPUNG
scurttEx exit VOST
afterburner VCST
stack M5
scatter exit M5
aftertumer M17
afterburner temo C)
inspected saipUng prdbe
clay/organic fed (kg)Q q q 0 n
13
Time of Day (hr)
40
-------
TEST 6 (8/15/89)
OPERATION, BENTS AND SAMPLING
scatter exit VOST
afterburner VtET
stack M5 h
saxtber exit M5 I
afterburner M17 I
afterburner 0
• ifterburner temp (C)
kiln temp (C)
metal fed (I) 4 + + +
+ +
+ +
++++++t
H—M-
350
lay/organic fed fkd n D D 0
n m fl "
~ n
~ D
D Q
~ D
D D
a a
T
10
12
I
H
Time of Day (hr)
41
-------
TEST 7 (8/9/89)
OPERATION, EVENTS AND SMPUNG
feed interrupts H
stack \£ET
scri-bber exit \CET
aftertxmner VOST
stack M5
scatter exit S5
aftertumgr M17
cfterburner 02 (%)
system autdcwi
(fferburner temp (C)
metal fed (I) +++ +
cay/organic fed (kgLn gom D °
^ ~ .nO UJU
10
12
H
Time of Day (hr)
42
-------
TEST 8 (8/11 /89)
OPERATION, MS AND SMPLJNG
I—I I—I I—I stack VOST
1—| I—| I—| scatter exit VCST
1—| 1—1 1—1 afterburner \£5T
1 1 stack K5 ,
!— 1 scnijber edx M5
1 1 aftertxn ner M17
a\ _ Fo,
a.
1150
aft
1050
srbumederr^^—I
18
10
950
000
kiln temp (C) j J
y
a
metal fed (I) + + + + * \
i i + t n '
300
do
a.
('/organic fed (|j) D ~ D
D n ? 1 i i i i
7 9 11 13
Time of Day (hr)
43
-------
TEST 9 (7/28/89)
OPE,RATION, EVENTS AND SAMPUNG
feed lntemxits i i
scrJ±er exit VOSt
afterburner VCST
stack K5
scatter exit ^
afterburner M17
replaced sarrplirg prcbe
inspected saiplirg pnre
urner 02
kiln shut cbnn
temp ((J)
rmtol fed I)
o w
Time of Day (hr)
44
-------
Appendix A-3
Waste Feed Schedules
45
-------
•ST 1, K0317B9
Tits Delta T
(tin)
' ORBANi: FEES
Clay Average emulative
Fed Feed rite Fed
llbl (lb/hr) lib)
903
O
0
0
0
915
12
24.0
130.0
24.0
9 JO
15
37.0
148,0
43.0
945
15
36.0
144.0
99.0
1CW
15
37.0
148.0
134.0
1015
15
35.5
142.0
171.5
1030
15
35.5
142.0
207.0
1045
15
34.0
144.0
243.0
hoc
15
34.0
144.0
279.0
1115
15
34.0
144.0
315.0 load hopper
1130
15
34.5
138.0
349.5
1145
15
35.5
142.0
335.0
1200
15
3B.5
154.0
423.5
1215
15
35.0
140.0
456.5
1230
15
40.0
140.0
498.5
1245
15
30.0
120.0
5 26 .5
1300
15
35.0
140.0
543.5
1315
15
35.0
140.0
596.5
1330
15
34.0
134.0
432.5
1345
15
33.0
132.0
445.5
1355
10
24.0
144.0
489.5
1JOO-U15 load happer, feedrate for 1045-1100 used
OEtercire total clay fed
421-142 = 279 values froi data sheet
3E7.5-13 = 374.5 values fro» data sheet
34 fed xliile loading happer
4B9.5 fed to kiln I agrees with data above)
445 total ash Height
47.4 Z feed clay recovered as ash
f Z clay fraction of feed
£ a. >"phr\} CMfJhr)
/A f-fe r-L or n -c/~" (jjS'D-l&S^ IHI.'J
£*rull~
Ooet-Ui HI. 7 6V.X7
46
£Uy
/*g<9
/fo.f
foZ.J
-------
TEST 1, K031789
METAL FEED
Tite Delta T Metal Metal Average Cueulative
Fed Fad Feedrate Fed
Ilia) (lb) (I) (l/hr) (1)
912
0
0
0
0
0
915
3
0.34
0.15
2.94
0.15
930
15
0.90
0.17
1.47
0.51
945
15
1.24
0.51
2.03
1.02
1000
15
1.20
0.49
1.96
1.51
10I5
15
1.20
0.49
1.96
2.00
1030
15
1.20
0.49
1.96
2.49
1045
15
1.22
0.50
1.99
2.99
MOO
15
1.24
0.51
2.03
3.50
HIS
15
1.14
0.47
1.90
3.97
M30
15
1.16
0.47
1.90
4.45
M45
15
1.14
0.47
1.90
4.92
1200
15
1.28
0.52
2.09
5.44
1215
15
1.02
0.42
1.67
5.B6
1230
15
1.15
0.47
1.88
4.33
1245
15
1.05
0.43
1.72
6.76
1300
15
• 1.00
0.41
1.63
7.17
1315
15
1.22
0.50
1.99
7.67
1330
15
1.22
0.50
1.99
8.17 load aetals
1345
15
1.22
0.50
1.99
8.46
1353
8
1.16
0.47
3.56
9.14
1315-1330 laid eetaW, feedrate for 1300-1315 used
Detereine the total fed
24.44-5,53=18.89 lbs,
11.22-B.8*= 2.JB lbs,
1.22 lbs,
7.72 I values froi data sheet
0.97 1 values froi data sheet
0.SO 1 fed «hile loading aetals
22.40 lbs,
9.1? 1 agrees with above
flhn^, f~eeJrtdfcz CI
SZrutier /,1S ...
0\Je.rrtA t' ^
47
-------
TEST 2, K0E02B9
liie Delta T
(¦in)
CLAY DREftMC FEED
Cli) fiver15e emulative
Fed Feedrate Fed
(lb) (Jb/hr) (IbJ
502
0
0.0
0.0
0.0
912
10
19.5
117.Q
19.5
92S
14
0.0
0.0
19.5
945
1?
J7.5
11J.4
57.0
1000
15
20.5
62.0
77.5
1015
15
32.5
130.0
110.0
1030
15
30.0
120.0
140.0
1045
15
33.0
132.0
173.0
i:o»
15
30.0
120.0
2C3.0
!:!5
15
32.0
12B.0
235.0
1130
15
26.5
106.0
261.5
1145
15
30.0
120.0
291.5
1200
15
30.0
120.0
321.3
1215
15
30.0
120.0
351.5
1230
!5
31.5
126.0
383.0
1245
15
31.5
126,0
414.5
1300
15
3B.5
154.0
453.0
1315
15
2B.0
112,0
461.0
1330
15
2£ .0
104.0
507.0
1345
15
29.5
119.0
536.5
1400
15
29.5
114.0
565.0
!4Ij
15
34.0
<36.0
599,0
1430
15
30.0
120.0
429.0
1445
15
35.0
140.0
664.0
150}
15
31.5
126.0
695.5
1515
!5
31.5
126.0
727.0
1530
15
30.0
120.0
757.0
1545
15
29.5
I1S.0
7B&.5
I MO
15
32.0
126.0
81B.5
1415
15
29.5
11S.0
B4B.0
1630
15
31.3
126.0
B79.5
1645
15
35.5
142.0
915.0
170ft
15
2B.5
114.0
943.5
1715
15
32.0
128.0
975.5
1724
9
11.5
110.0
992.0
CoiKnts; feed interrupts caused by the sere* feeder juainj
occurred froa 0912-092S and 0752-0956. This uterial reiained
od the scale, therefore no adjustienti to the clay feed data irere required.
120M215 load hopper, feedrate far 1145-1200 used
1500*1515 load hopper, feedrati for 1445-1500 used
yA i/c'"•I«. C. Zay
C fLlkr) Ckj-l/tr-) tl&Jkr-}
Ovo-wi) '*'-3 SXn 93 3
48
Sc.™e*,-r ooir- a * ss;i* ?3'J
HZ. I S3>-Za f/.f
-------
TEST 2, KQQ0297
Deteraine total clay fed
1477.3-1156 ¦ 321.5 values (roa data sheet
1413-104?.5 = 343.S values froi data sheet
1317-1052 = 245 values fro« data sheet
30 fed Mhile loading hopper
31.5 fed Mhile loading hopper
991,5 fed to til a [agrees h ith data above)
686 ash Height
2 I feed clay recovered as ash
? I clay fraction of feed
49
-------
TEST 2, K08C2B9
HETAL FEED
Tiae
Delta T
Hstal
Heta!
Average CueulatiYS
Fed
Fed Feedrate
Fed
din!
(lb!
(11
tl/hr!
(1)
930
0
0
0
0
0
945
15
0.B2
0.34
1.34
0.34
952
7
0.16
0.07
0.56
0.40
1002
10
0.00
0.00
0.00
0.40
1015
13
1.24
0.51
2.34
0.91
1030
<5
1.22
0.50
1.99
1.41
1045
15
1.22
0.50
1.99
1.90
1100
15
1.16
0.47
1.90
2.3B
1115
15
1.24
0.51
2.03
2.89
1130
15
1.12
0.46
1.83
3.34
1145
15
1.14
0.47
1.B6
3.81
1200
15
1.24
0.51
2.03
4.32
1215
15
1.16
0.47
1.90
4.79
1230
15
1.20
0.49
1.96
5.2B
1245
15
i.ia
0.4B
1.93
5.76
1300
15
1.14
0.47
1.B6
6.23
1315
15
1. IB
0.4B
1.93
4.71
1330
15
1.16
0.47
1.90
7.IB
1345
15
1.10
0.45
1.80
7,63
1400
15
1.02
0.42
1.67
B.05
1415
15
1.24
0.51
2.03
B.56
1'30
15
i.oe
0.44
1.77
9.00
1445
15
1.12
0.46
1.B3
9.46
1500
15
1.16
0.47
1.90
9.93
1515
15
1.10
0.45
1.B0
10.38
1530
15
1.06
0.43
1.73
10.B1
1545
15
1.10
0.45
1.B0
11.26
lbOO
15
1.16
0.47
1.90
11.74
1415
15
1.10
0.45
1.B0
12.19
1630
15
1.12
0.46
1.B3
12.64
IMS
15
1.18
0.4B
1.93
13.13
1700
15
0.9B
0.40
1.60
13.53
1716
16
1.6G
0.69
2.57
14.21
feeder Jaaied, subtract
0.24 lbs froi 0952
Coiaents: to account for aetals lost durin| serin feeder adjastients
foilOMing the jailing incident, 3 linutes of istils feed hive been subtracted
froi the reading iuediateljr prior to the jailing incident.
This is equivalent to 0.24 lbs.
Deteriine the tctal letal fed
50.5B-15.56 - 33.02 lbs, 14.31 1 values froi data sheet
0.1 1 lost daring feed jailing
14.21 1 fed to kiln (agrees nith data above) .
» AJert~*3« Cf/ht-)
^a/npfJfl£. * _
ServkU- ' f/o IS - lo>2$ 1.10
A-£+eriiurr*-er— f /OSLO - /53 7) {'*£
Oyef«ff f" ® a
-------
TEST 3, K9B04E9
CLAi 0RBANIC FEED
Tiie
Delta T
Clay
Average
Cuialative
Fed Feedrati
Fed
(•in)
(lb)
(Ib/hr)
(lb)
942
0
0.0
0.0
0.0
1015
33
4.0
10.9
1.0
1030
15
25.5
102.0
• 31.5
1045
IS
30.5
122.0
62.0
1100
15
31.5
121.0
93.5
1115
15
32.0
12S. 0
125.5
1130
15
34.0
131.0
159.5
1145
15
33.0
132.0
192.5
1200
15
34.5
13B.0
227.0
1215
15
35.0
140.0
212.0
1230
15
35.0
14D.0
297.0
1245
15
35.0
140.0
332.0
1300
15
35.0
140.0
347.0
1315
•5
35.0
140.0
402.0
1330
15
34.0
131.0
431.0
1342
12
30.0
- 150.0.
411.0
Conents: feed interrupts caused by the sere* feeder jawing
occurred three tiies betwen 0942 and 1024
Detsraine total day Jed
533.5-1B - 445.5 value froi data sheet
(agrees *ith data abavel
323 ash weight
69.4 I feel! clay recovered as ash
7£. J, Z clay fraction of feed
Sample} (H/hr) CkgjLr>) OL!h^_
flumes' (loll-iw) )Z+ ? M''9
ScrvLU*- €x*+~ Chio-)^2l), /£3.£ bo-t>°
Oyer*/! f/a3o-/2¥sl) /3& %
(7YZ-/o2°) 31 - f
6i,(>0
/01.7
I Oh 8
)OZ-^
30. _£
51
-------
TEST 3, K0304E9
METAL FEED
Ties
Delta T
Hetal
Hetal
Average Cutu!stive
Fed
Fed Feedrate
Fed
(¦in)
lib)
(1)
fl/fir)
(11
949
0
0.00
0.00
0.00
0.00
951
2
0.12
0.05
1.47
0.05
1013
22
0.00
0.00
• O.OO
0.05
1015
2
0.06
0.02
0.74
0.07
1025
0
0.00
0.00
0.00
0.07
1030
5
0.42
0.17
2.06
0.25
1045
15
1.24
0.51
2.03
0.75
1100
IS
1.20
0.49
1.96
1.24
1115
15
1.24
0.51
2.03
1.75
1130
15
1.24
0.51
2.03
2.26
1145
15
1.16
0.47
1.90
2.73
1200
15
1.24
0.51
2.03
3.24
1215
15
1.26
0.51
2.06
3.75
1230
15
1.20
0.49
1.76
4.24
1245
15
1.29
0.52
2.09
4.77
1300
IS
1. IB •
¦ 0.4B
1.93
5.25
1315
15
1.22
0.50
1.99
3.73
1330
15
1.20
0.49
1.94
6.24
1338
e
1.1ft
0.45
3.37
6.69
jDib°.i!s: feed interrupts caused by the sere* feeder jaiding
oicurred three ti ass betifssn 0942 tri 1024
Jetenirte the total eetal fed
<4.46-23.12 = 16.36 lbs, £.69 I values fro* the data sheet
[agrees with data above)
phnj, Aoer^ja. teJr-Je. U/^
burner //
-------
TEST 4, K0B0189
CLAY ORGANIC FEED
Tiee Delta. T Clay Average Cumulative
Fed Feedrate Fed
din) lib) (lb/hr) (lb)
906
9.1
0
0
0.0
0.0
915
9.25
9
14.0
93.3'
14.0
930
9.5
15
34.0
136.0
4B.0
945
9.75
15
33.0
132.0
B1.0
1000
10
15
32.0
I2B.0
113.0
1005
10.0B3
5
11.0
132.0
124.0
1010
10.146
5
0.0
0.0
124.0
1015
10.25
5
11.5
13B.0
135.5
1045
10.75
30
11.0
22.0
146.5
1100
11
15
IB. 5
71.0
165.0
1115
11.25
15
21.5
06.0
1B6.5
1130
11.5
15
27.5
110.0
214.0
1145
11.75
15
34.0
136.0
248.0
1200
12
15
32.5
130.0
2B0.5
1215
12.25
15
35.5"
142.0
316.0
1230
12.5
15
34.0
136.0
350.0
1245
12.75
15
34.0
136.0
3B4.0
1300
13
15
37.0
143.0
421.0
130?
13.15
9
17.0
113.3
43B.0
1323
13.3B -
!4
0.0
0.0
43B.0
1330
13.5
7
20.0
171.4
45B.0
1343
13.714
13
42.0
193. B
500.0
1350
13.333
7
0.0
0.0
500.0
1412
14.2
22
29.5
BO.5
529.5
23.5-2*21.5 (2 lbs spilled)
29.5-2=27.5 (2 lbs spilled)
load hopper
acre* feeder rate increased
Coisents: during this test, feed interrupts caused by the sere* feeder
jailing occurred several tiies as noted beloa. Feedrate adjustments for
cases nhen the aaterial did not reaain on the scale are noted bela*.
For those cases indicated nithout additional coiaeat, the laterial retained
on the scale and no adjustaent to the recorded data is required,
1005-1010 feeder janed
1015-1100 several jailing incidents, nights taken froi the recorded data
1100-1130 the feed port saipling plug was not replaced and soae of the
feed fell onto the scale and floor; lost of thi feed aaterial landed
an thi scale, however 4 lbs did spill on the floor and containisnt tray;
therefore the values reported for 1115 and 1130 have bain reduced by
a. lbs each to deteriine the atount fed to the kiln. Feedrates
agree »itb values determined usingJJstopKatch Jvrmy. *rF
1130-1145 reeoved spilled fead froi the scale;
feedrate tiled at 1140; leasured value of 136 lbs/hr Mas
used to deteraine that 34 lbs were fed during 1130-1145
53
-------
TEST 4, KOBC'Iif
1234-1245 load hopper, 'sail-ate far 1215-1250 ussd here
1309-1323 feeder jaatsc
1343-1350 retder jaaied
litertine total clay fti
1465.5-1242.5 - 218
1162 - 1040 = 102
1353 -1212,5 = 145.5
34
34
533.5
4
52S.5
34B
69.5 I
7&-Y I
values froi cata sheet
Mines frna data sheet
vain?? fro* data sheet
fed while cleaning scale
fsi while I oat in g hopper
total fed
spilled to ficor
Jei to kiln (agrees Mith data above)
ash wight
¦feed clay rscoverd as ash
day fraction of fetd
t£a.Mpht\a^
yrn€ f— (Ho2-t*os>
£c/~vLt>er- £x'"f~ OloV-niaJ
^i/eni fj
fii 4 & "tc-
(illhr)
tfj
1*7. O
/62.S
s~z if
¥7. OS
fro. tJTTen
ULjhr>
g7. O
97. O
7f.3
54
-------
TEST 4, K080139
ICTflL FEED
Tiie
Delta T
Natal
Netal
Average
Cumulative
Fed
Fed Feidrate
Fed
(linl
(lb)
(1)
(I/hr)
(11
93?
9.45
0
0.00
0.00
0.00
0.00
1000
10
21
1.64
0.67
1.91
0.67
1005
10.083
5
0.36
0.15
1.77
0.B2
feeder jawed, subtract
1015
10.25
10
0
0.00
0.00
0.82
0.24 lb; froi 1005
1030
10.5
15
0.26
0.11
0.43
0.92
1045
10.75
15
0.26
0.11
0.43
1.03
1109
11
15
0.72
0.29
1.16
1.32
1115
11.25
15
0.96
0.35
1.41
1.68
feed spill, letals reduced
1130
11.5
15
0.76
0.31
1.24
1.99
by 371
1145
11.75
15
1.24
0.51
2.03
2.49
1200
12
15
1.14
0.47
1.86
2.96
1215
12.25
15
1.26
0.51
2.06
3.47
1230
12.5
15
1.20
0.47
1.96
3.96
1245
12.75
15
1.22
0.50
1.97
4.46
1300
13
15
1.30
0.53
2.13
4.99
1309
13.15
9
0.36
0.15
0.98
5.14
feeder jaiaed, subtract
1323
13.333
14
O.OO
O.OO
0.00
5.14
0.24 lbs fros 130?
1330
13.5
7
0.49
0.20
I.SB
5.34
1343
13.717
13
1.12
0.46
2.11
5.79
feeder jaired, subtract
1350
13.333
T
0.00
0.00
0.00
5.79
0.24 lbs froi 1343
1405
14.003
15
1.42
0.58
2.32
6.3E
Couents: during this test, feed interrupts caused by the sere* feeder
jawing occurred several tiies a; noted. To account far letals lost during
feeder adjustsents rollciting jailing incidents, 3 ainutes of letals reed have
been subtracted froi the reading iiiediatsly prior to the jaaaing incident.
This is equivalent to 0.24 lbs per incident.
1015-1100 several jailing incidents, weights taken froi the recorded data
1100-1130 the feed pert tabling plug mi not replaced and mch af the
feed fell onto the scale and floar, the aiourt of letal fed to
the kiln was determined using inforiatinn fro* the clay feed;
the fesdrate nas 134 lbs/hr, therefore 40 lbs should lave been
fed; the clay scale data shoi 13 lbs were fed, therefore 25/66 lbs
(3711 did not reach the kiln; values used for 1115 2nd 1130
have been reduced by 372 froi the recorded values
Cetenine total aetal fed
43.52-31.26 = 17.24 lbs, 7.03 1 values froi data sheet
0.38 1 spilled
0.29 1 lost during feed jailing
6.30 1 fed tj kiln (agrees with data abevs)
Aftmrivrnar j -'*
overall A y,r
-------
TEST 5, KM!699
CLAY 0R5AN1C FEED
Tiie
Delta T
Clay
Averags
emulative
Fed Feedrate
Fed
(¦in}
t]t>)
tlb/hrl
lib]
21s
0
0
0
0
335
14
31. C
132.9
31.0
845
15
37.0
14S.0
6B.0
90?
15
35.5
142.0
1CJ.5
915
15
35.5
142.0
139.0 load hopper
930
15
34.0
144.0
175.0
945
15
3B.5
154.0
213.5
1000
15
35.0
140.0
249.5
1015
15
3b. 0
144.0
2E4.5
1 C*30
15
35.0
140.0
319.5 load hopper
1045
13
35.0
140.0
354.5 load hopper
UOO
15
35.0
140.0
305.5
1113
15
35,0
140.0
424.5
1130
15
35.5
142.0
460.0
1145
15
36.5
146.0
494.5
1200
15
36.0
144.0
532.5
1215
15
36.0
144.0
569.5
1230
15
34.0
134.0
602.5
1245
11
J3.0
144.0
636.5
1253
13
26.5
131.5
667.0
Conaer.tsi fes-arate for previous interval used during hspper loading
Detenine tcr.al cl
1B5-B1.5
326.5-1E1
332-19.5
~7l.f
/r>^o ^
tJr n
ScrMer- Eje.f fm- //er+«c FedraJe. , ^ a.
omA a^ cuf
/^J./ fO%'&
/V3-0 6^8i, /c9
-------
TEST 5, K08I6B?
NETAL FEEJ
Tiie
Delta T
Netil
Hetal
Average emulative
Fed
Fed Feedrate
Fed
(¦in)
(lb)
(1)
tl/hr)
(I)
921
0
0
0
0
0
030
9
0.54
0.22
1.47
0.22
B45
15
0.74
0.30
1.21
0.52
900
13
1.10
0.45
1.80
0.97
915
15
1.16
0.47
1.90
1.45
m
IS
1.16
0.47
1.90
1.92
945
15
1.2B
0.52
2.09
2.44
1000
15
1.12
0.46
1.83
2.90
1015
15
1.12
0.46
1.B3
3.36
1030
15
1.06
0.43
1.73
3.79
1045
IS
1.22
0.50
1.99
4.29
1100
15
1.16
0.47
1.90
4.77
1115
15
1.14
0.47
1.86
5.23
1130
15
1.24
0.51
2.03
5.74
1145
15
1.2B
0.52
2.09
6.26
1200
13
1.30
0.53
2.13
6.79
1215
15
1.2B
0.52
2.09
7.32
1230
15
1.20
0.49
1.96
7.81
in
15
1.28
0.52
2.09
B.33
1256
11
1.32
0.54
2.94
a.E7
•nine the total
istal fed
34.90-13.74 = 21.16 lbs
0.34 lbs fed before istal nas rsi'illed
21.7 1bs 8.S7 1 fed to kiln (agrees »iih data above)
trip I
£c ruL her- ty, +~ *)
After-Li, rn-e-r- (Jtl-JZoi}
0\j er-a. //
A TO
), 9*
A
57
-------
TEST 6, K0&1539
CLAY ORGAKIC F££D
Tiie
Delta T
Clay
Average
Cuaulati1
Fee Feedrats
Fed
(¦in)
lib!
llb/hrl
(lb)
E55
0
0
0
0
*00
5
10.5
126
10.5
915
13
3S
152
4B.5
930
15
35
140
63.5
945
15
37
148
120.5
1000
15
35
140
155.5
1315
15
03* 3
142
191
1030
15
35
140
226
1045
15
35
140
261
!1M>
15
35
140
296
1115
15
34.5
146
332.5
1130
15
3 i
•ii
36G.5
i:«
15
34
144
404.5
1200
15
35
140
439.5
1215
15-
35.5
142
475
1230
15
34
141
511
1245
15
34.5
135
545.5
1300
15
34.5
13B
5 B0
13!S
15
3s
144
616
133C
15
35
140
651
1345
15
35
140
6B6
14C'0
15
37
143
723
CosBents: fseoraies for previous interval used when hopper loaded
Detenine tctai clay fed
337-11! - 226 values frot data sheet
356.5-107 = 24?.5 values froi data sheet
353-210 = 143 values froi data sheet
35 fed while loading hopper
35 fed while loading hopper
34.5 fed Mhile loading hopper
723 fed to kiln (agrees with above)
474 ash weight
45.4 I feed clay recovered as ash
7^,/ I day fraction of feed
A\Jer-«'te f^ec^r-eJ^.
Sampling (fi/fc) Ckr/lr>) CUy fi-ac.'hon flLIh
/og.o
A*+*r turner Wl
£c.rVU<.r- £*,+- /*-?-* /a2 3
58
Ov^ra/f /VJ-Z. (.ISO ;&s,3
-------
TEST 6, K0315B9
¦1ETAL FEED
Tiae
Delta T
Netal
Metal
Average emulative
Fed
Fed Fesdrats
Fed
(tin)
(lb)
11)
ll/hr)
11)
995
0
0
0
0
0
915
10
0.40
0.16
0.9B
0.16
930
15
1.10
0.45
i.eo
0.61
915
15
1.14
0.47
1.B6
1.0B
1000
15
1.10
0.45
i.eo
1.53
1015
IS
1.12
0.46
1.83
l.?9
1030
15
i.oa
0.44
n 1.77
2.43
1045
15
1.12
0.46
1.83
2.39
Uto
15
1.10
0.45
1.30
3.33
1115
15
1.10
0.45
1.80
3.70
1130
15
i.oa
0.44
1.77
4.23
1145
15
1.10
0.45
1.90
4.68
1200
13
1.04
0.43
1.70
5.10
1215
15
1.06
0.43
1.73
5.53
1230
15
1.03
0.44
1.77
5.97
1243
15
1.06
0.43
1.73
6.41
1300
15
1.09
0.44
1.77
6.85
1315
15
1.10
0.45
1.80
7.30
1330
15
1.04
0.43
1.70
7.72
•345
< C
4 J
1.0S
0.44
1.77
a. 17
HOO
15
1.36
0.56
2.22
8.72
Determine the total «?ta! ted
41.2B-19.94 - 21.31 lbs B.72 1 fed to kiln (agrees «ith data above)
.£¦»./> A«3. e &<*a^r-
S>C'/~t/LL-e.r- (lQ! y~ ^^--0
Af-ber-Lur^er- stfoo}
&)J C ~"** f I
/. 7?
/. eo
).-?7
59
-------
TEST 7, K0BO939
CLAY 0RBANIC FEED
Tiie
Delta T
Clay
flvenqs
Cuculstive
Fed Feedrate
Fed
(tin!
lib)
(ib/hr)
lib)
906
0
0.0
0.0
0.0
915
9
22.5
150.0
22.5
930
15
36.0
144.0
53.5
936
4
14.0
140.0
72.5 assuee based on previous feedrate
945
0
0.0
0.0
72.5
1000
15
32.5
130.0
105.0
1007
7
15.0
129.6
120.0
1012
5
0.0
0.0
120.0 31.5-21.5=12 lbs reioved froi scale
1015
3
4.5
130.0
126.5
1030
15
37.0
14B.0
163.5 -
1045
15
36.5
144.0
200.0
noo
15
35.5
142.0
235.5
1103
3
4.0
120.0
241.5 £.e&J r
1113
10
0.0
0.0
241.5
1115
2
4.0
120.0
245.5
1130
15
32.5
130.0
278.0
1145
15
37.5
150.0
315.5 tiaed, load hopper
1200
15
34.5
135.0
350.0
1215
15
34.0
144.0
386.0
1230
15
37.0
14B.0
*23.0
1245
15
37.0
140.3
440.0 -
1300
15
35.?
140.0
495.0
1315
15
34.0
144.0
531.0
1331
16
36.0
135.0
567.0
Cscients: -fecc! interrupts caused by the sere* jailing occurred several tiies
ae noted. Feedrates Here checked regularly and agree Nith the values
indicated by the scale data, The value reported 1015 has been reduced
because so:e lateriil was reaoved froi the scale fcllwiing the incident.
The feedrate used *as adjusted to agree Kith the other wight data.
feeder jaued, value reported at 0745 indicates a Height increase,
previously indicated feedrate used
/£>c7-/e>/JL
feeder jaaaed, 12 lbs reeoved fro# scale
1103-1113 sys~fe 0*1 sS oujr> j -CecJ z^oJ(
1130-1145 load hopper, feedrate tiled at 113?, 1143, 1145
60
-------
TEST 7, K0SO9B9
Deteriine total clay fed
455.5-3J7
= 58.3
values frc» data sheet
404-1B6.5
= 217.3
values froi data sheet
~44.5-193
- 251.5
values frei data sheet
14
fed during feed/scale adjustient (0935)
37.5
fed Nhile loading hopper
37?
total fed
12
removed fro« scale following interrupt
567
total led to kiln [agrees xitli data above)
573
ash Height
64.fi I
feed clay recovered as ash
-?S.\
Z
clay fractior of fesd
C I CJ«Y akjk,
•S (k} Y
After-bur it g/~ (l02S~-UZfy /'//.(z ~ }6(r • ~7
.^Cr-vLlnr- (/CJ5~-^ VJ.J t^sSS" I°7-P-
oj^H la*'? 9L7
61
-------
TEST 7, Kd50?9?
IffTAL FEED
Tiie
deHj r
Metal
Metal
Average Emulative
Fed
Fed Feedrate
Fed
{(in)
(Ih)
(1)
Cl/hr)
(1)
915
0
0
0
0
0
930
15
1.36
0.56
2.22
0.56
934
6
0.30
0.12
1.23
0.68 feeder jaaied, subtract 0.24 lbs frot 9'
945
9
0.00
0.00
O.OO
0.6B
1000
15
1.14
0.47
1.66
1.14
1007
7
0.30
0.12
1.05
1.27 feeder jamed, subtract 0.24 lbs frot U
1015
B
0.00
0.00
0.00
1.27
1030
15
1. IB
0.48
1.93
5.75
1045
IS
1.14
0.47
1.86
2.21
1100
<5
1.19
0.49
1.95
2.70
1103
3
0.16
0.07
1.31
2.77 tyitei shutdown, so adjLstient required
1113
10
0.00
o.oo
O.OO
2.77
1115
2
0.11
0.04
1.35
2. p i
1130
15
1.14
0.47
l.Bi
Z.li
1145
IS
1.26
0.51
2.06
3.79
1200
15
1.14
0.47
1.96
4.26
1215
15
1.16
0.47
1.90
4.73
1230
15
1.22
0.50
1.99
5.23
1243
15
i.ie
0.40
1.93
5.71
1300
15
1.14
0.47
1.96
6.18
1355
15
1.14
0.47
1.36
6,64
1331
lo
1.38
0.56
2.11
7.21
1097
Coessfits: to account for istdls lost during s:re* fesder adjustients
fcl 1 owing jauing incide/t, 3 lir.utss of letals feed have been subtracted
fro¦ the reading iniediately prior to the Jailing incident.
This is equivalent to 0.24 lbs per incident.
Ds'.srsine total teUl fed
43.1-29.98 - IE. 12 lbs, 7.*0 1 valties fro# data sheets
(.20 1 lost daring feed jailing
7.20 1 fed to kiln (agrees with data above!
fii
uer-a^e. rse
,ns- (tfh^
^dS~t/LLe.r-
A rV"« fhurn &r~ (/oz.S~— /3—<\) J'?3>
-------
TESi 9, KPB11B9
The Delta T
(¦in)
CLAY QRSfllllC FEED
Clay Average emulative
Fed Feedrate Fed
(lbl (lb/hrl (It)
746
D
0
0
0
GOO
14
31.5
135.0
31.5
BIS
15
35.0
144.0
67.5
630
15
36.0
144.0
103.5
B43
15
33.0
140.0
139.5
700
15
36.0
144.0
174.5
915
15
35.0
140.0
209.5
930
15
54.0
136.0
243.5
945
15
34.0
136.0
277.5
1000
15
34.0
136.0
311.5 load hopper
1015
15
33.3
134.0
345.0
1030
15
34.0
136.3
379.0
1045
15
35.0
140.0
414.0
1100
15
36.0
144.3
450.0
1115
15
37.5
150.0
4B7.5
1150
15
37.5
150.)
525,0
1145
15
33.0
132.0
556.0
>209
15
36.5
146.0
594.5
1215
15
33.5
134.0
629.0
1223
13
31.0
143.1
659.0
IDOO-10',5
load hepper, feedrate for fjO-945
used
Detereir.e total day fed
43E.5-141 = 277.5
413.5-66 = 347.5
34 fed while loading fapa-r
659 fed tn kiln (agrees xith data alovel
433 total ash Height
19,5 I feed clay recovered as ash
7S.1/ I clay fractini of feed
A\)er~*%e. 9rvJh~ . _ . s.. /, \
< I „ \ fi // \ C'*i rr-aerTio*. ( Ib/hrO
A(-bdom*r~ £*'** iOJT-L
duiker- £*,+- (S3*-IOX) /37. ^ 6*'*8 /*J. <7
Osizcoli '*^7
-------
TEsT 6, K08U3?
KET AL FEED
7i ae
Delta T
Heta!
fletal
Average Cussilative
Fed
Fed Feedrate
Fed
lain)
(lb)
(I)
(1/hrl
(1)
300
0
0
0
0
0
B15
15
1.14
0.47
l.Bi
0.47
830
:5
1.12
0.46
1.83
0.92
845
15
l.li
0.47
1.90
1.40
900
15
1.20
0.49
1.96
1.89
915
15
1.1S
0.4B
1.93
2.37
930
15
1.16
0.47
1.90
2.84
945
15
l.li
0.47
1.90
3.32
1000
15
1.18
0.4B
1.93
3.60
1015
15
l.li
0.47
1.90
4.27
1030
15
1.10
o.4e
1.93
4.76
1045
15
Mi
0.47
1.90
5.23
1100
15
1.19
0.49
1.93
5.7!
1115
15
i.ie
0.4B
1.93
6.20
1130
15
1.18
0.48
1.93
6.68
1145
15
1.2b
0.51
2.06
7.19
1200
15
1.22
0.50
1.99
7.69
1215
15
1.16
o.4e
1.93
8.17
122B
13
1.30
0.51
2.45
8.70
Dsljmine the total retii fed
42.4s-21.16 = 21.3 lbs, E.70 1 fed to kiln (agrees with data above)
hnf
/\ \J e.rei^ £
Ex,+-
A -f-fc.r&ut~nG'~
0\)Crf~<* //
-/oj/)
(fcio
>¦92.
hU
hi?
64
-------
TBI 9, K072BB9
CLAV ORGANIC FEES
Tiie
Delta T
CUy
Average
Emulative
Fed Feedrate
Fed
(tin)
(lb)
(lb/br)
(lb)
957
0
0.0
0.0
0.0
1000
3
3.5
70.0
3.5
1015
15
23.0
92.0
26.5
1030
15
37.5
150.0
64.0
1045
15
34.5
138.0
98.5
1100
15
30.5
122.0
129.0
1102
2
4.5
135.0
133.5
1127
25
0.0
0.0
133.5
1130
3
6.5
130.0
140.0
1145
15
32.0
128.0
172.0
1200
15
34.5
130.0
206.5
1217
17
34.5
121.8
241.0
123B
31
27.0
52.3
268.0
1300
22
0.0
0.0
26B.0
1315
15
34.0
136,0
302.0
1330
15
34.0
136.0
336.0
1350
20
45.3
135.9
381.3
1400
10
17.5
105.0
393.3
1415
15
35.0
140.0
433. B
1430
15
33.5
134.0
467.3
144S
15
34.0
136.0
501.3
1500
IS
3S.0
144.0
537.3
1509
9
20.0
133.3
557.3
1524
IS
0.0
0.0
557.3
1530
S
13.5
135.0
570. B
1545
15
34.0
136.0
604.8
1G00
15
22.5
90.0
627.3
1615
15
33.0
132.0
660.3
1E24
9
12
BO.O
672.3
1E37
13
0
0.0
672.3
1639
2
1
30.0
£73.3
11-6.5=4,5 (4.5 lbs spilled)
(11 lbs recorded)
feeder jailed, spilled uteri*] reicved
froi seals [26 lbs recorded)
40-33.5=6.5 (6.5 lbs spilled)
(1500-1530, 40 lbs recordsd)
j£\ (k,M
A{+*r-Luni*r- (OaV-V*3 9) Jl7.f 5"
SorvLW £*>+~ 'l°J ??-J
Over*!! 65 ****? y7,Z
-------
TEST 9, M72BB9
CoNents: feed interrupts caused by the screw feeder jailing
occurred several tiies as noted belsv. Approximately, 35 lbs
of feed aaterial spilled during these incidents. Unlike Test 4,
the aaterial was collected in a bucket and moved froi the scale.
S:ale weight data were adjusted as noted to detenine the aioint
actually fed to the kiln.
1102-1125 (4.5 lbs reioved froi scale)
1239-1253
reicved froi the scale)
1509-1524 (6.5 lbs reioved froc scale)
1S24-1637 Clou weight loss daring this period indicates
that any spilled laterial retained on the scale)
1315-1350
(checked by tiling at 1414)
Detenine total clay fed
34
45.3
710.3
37
673.3
431
35
4S£
69.2
76.8
values froi data sheet
values froi data sheet
fed while loading hopper
fed while loading hopper
total fed
reioved froi scale during feed interrupts
fed to kiln (agrees with data above)
asti veight (not including overnight)
estiiated overnight (based on averages for other tests)
total ash weight
Z feed day recovery as asb
Z clay fraction of feed
66
-------
TEST 9, (072639
METAL FEES
Tiie
Delta T
Metal
Netal
Average
Cuiulative
Fed
Fed Feedrate
Fed
(¦in)
(lb)
(1)
(1/hr)
(1)
1042
0
0
0
0
0
1045
3
0.70
0.29
5.72
0.29
1100
15
1.04
0.43
1.70
0.71
1102
2
0.14
0.06
1.72
0.77
1136
34
0.00
0.00
O.OO
0.77
1145
9
0.78
0.32
2.13
1.09
1200
15
1.08
0.44
1.77
1.53
1217
17
1.20
0.49
1.73
2.02
123B
21
1.36
0.5E
1.59
2.57
1300
22
0.00
O.OO
0.00
2.57
1315
15
0.96
0.39
1.57
?.97
1330
15
1.12
0.46
1.83
3.42
1350
20
1.B3
0.77
2.30
4.19
1409
10
0.64
0.26
1.57
4.45
1415
15
1.2S
0.51
2.06
4.97
1430
15
1.20
0.49
1.96
5.46
1445
15
1.20
0.49
1.96
5.95
1500
15
1.18
0.49
1.93
G.43
1509
9
0.42
0.17
1.14
E.EO
1524
15
O.OO
0.00
0.00
6.60
1530
£
0.48
0.20
1.96
E.EO
1545
15
1.26
0.51
2.06
7.32
ieoo
15
1.10
0.45
1.90
7.76
1615
15
1.24
0.51
2.03
B.27
1624
9
0.52
0.21
1.42
B.49
feeder jaaied, subtract 0.15 lbs froi 1100
subtract O.OB lbs fro* 1102
feeder jaiied, subtract 0.24 lbs froi I23B
feeder jaaied, subtract 0.24 lbs froi 1503
feeder jaaied, subtract 0.24 lbs froa 1524
Coaients: to account for leials lost during screv feeder adjustments
following jailing incidents, 3 ainutes of aetals feed have bean subtracted
froi the reading iiaediately prior to the jailing incident.
This is equivalent to 0.24 lbs per incident.
Deteriine total letal fed
50.86-29.14 - 21.72 lbs, S.88 1 values froi data sheet
0,40 1 lost daring feed jailing
9.4B 1 fed to kiln (agrees with data above)
A**"'!*
Sc.ru hber- Ey<+- om- **0 1.91
\jrn-et
/ 67
0\j£f-a H ) V J
-------
Appendix A-4
CEM Data Plots
Kiln exit Orsat 02 readings
Date
Time
Kiln exit
02 (%)
28-Jul—89
11:40
11.5
12:29
14. 0
13 :25
11.9
14 :12
12.5
14:30
14.0
16:24
13.5
Average
12 .9
17-Aug—89
12 :43
12 .0
68
-------
TEST 1 (8/17/89)
CEM DATA - 02 AND COZ
(Gin 02 ^
irijp-c-'fcd k'h
froie.
AB 02
AB CO 2
Stock CO2
~r
T"
"1—
14
10 12
Time of Day (hr)
TEST 1 (8/1 7/89)
CEM DATA - CO AND NOx
SE NOx
Steel
AB CO
—i—
10
¦—T—
12
14-
Time of Day (hr)
69
-------
TEST 2 (8/2/89)
C£M OMA - 02 AND 002
/ncfie&fed? a"0= rhor*&r
S,d f^abe
*ee* irihzrrvflT/einS
Kiln 02
Stack 02
AB 02
AB CO 2
Stock C02
Tims of Day (hr)
*3 -
40 -
39
30
23 -
20 -
15
TEST 2 (8/2/89)
CEM DATA - CO AND NOx
h
se nox
A
My
10 § ack CO
AB CO
"win
LWVfH
—I—
1*
—r~
16
10
12
Tims of Day (hr)
IB
70
-------
*
w
e
3
TEST 3 (S/4/89)
CEM UTA - 02 AND CO2
Kiln 02
ack 02
HB C02
11
13
IS
Tims of Day (hr)
E
a
3
c
JO
"o
¦a
2
o
a
40
33 -
30
25
20
is H
10
s
SE NO*
TEST 3 (8/4/89)
CEM DATA - CO AND NO it
AB CO
ock CO
wvpf^M
v~A/vW
~r
11
13
15
Tim« of Day (hr)
71
-------
TEST 4 (8/1/89)
CEM DATA. - 02 AND C02
ee
Stock c
SE 02
Klin 02
AS OZ
AS C02
tock 002
6
10
12
14-
Time of Day (hr)
TEST 4 (8/1/89)
C£M DMA - CO AMD NOx
SE NOx
Stock CO
AB CO
12
14
10
8
Tim® of Doy (hr)
72
-------
s
s
X
£
a
TEST 5 (8/16/89)
C£M QMX — 02 AND 002
7
Kan 02
Stack 02
AB C02
ah a z
Stack CO 2
Tim* of Day (hr)
E
Q.
<3
2
a
a
TEST 5 (8/16/89)
CFV O.TA - CO AND NOx
SO
*3
40 -
35 -
JO
25
ZO
IS
10
6
SE NO*
AB CO
Stock CO
ii
~T
13
Trm« of Day (hr)
73
-------
TEST 6 (8/15/89)
CEM DMA - 02 AND C02
1
1
1
Kiln 02
Stack 02
1
5E 02
1
1
1
7 -
+ 3 :ock 0O2
B
10
12
14
Time of Day (hr)
TEST 6 (8/15/89)
CEM CATA - OO AND NO*
45
33 "
SE NO*
30
26 -
AB CO Instrument not in aervioe
2D -
Stack CO
-5
8
12
14
Tim« of Doy (hr)
74
-------
TEST 7 (8/9/89)
CEM DATA. ~ OZ ANO C02
1 Kiln 02
SE 02
Stack
A3 02
AH C02
Stock CQ2
ski/fJok/n
Time of Day (hr)
«0
TEST 7 (8/9/89)
CEM DATA - CO AND NO*
E
a
£>
m
2
«
o
*00 -
350
300 -
250 -
200
ISO
too H
90
O
-50
SE NO*
AB CO **w|1
Stock CO
T~
10
12
—I—
14.
Time of Day (hr)
75
-------
TEST 8 (8/1 1/89)
C£M DMA - 02 AMD C02
16
f ^ J 'Mn 02 -s-^
Stack 02
13 SE 02 3
7 -
6 JB CQ2
4 -
Stock CO
11
13
7
9
Time of Day (hr)
TEST 8 (8/1 1/89)
C£M DMA - 00 AND NO*
40 -
25 -
20 -
15
stock CO not tn
10
AS CO
-5
9
11
13
7
Uma of Day (hr)
-------
TEST 9 (7/28/89)
CEM DATA - 02 AND CD2
JrecJt
/ t$p*c~f~
-------
APPENDIX B
SCRUBBER BLOWDOWN METALS DATA
78
-------
TEST 4 (8/1/69) ARSENIC
MVHn oxmoowtf Q&KOanmm
o.a -
a» -
0.2 •
o.ia -
0.! -
O.M -
0 •
¦**¦^0699% r2-0*MBI
*UcUv» MriA - 0487
kiln temperature (F) = 1600
afterburner terrperature (F) = 2C0Q
feed cnlorine (wt %) = 4
liquor pH ~ 9.0
metal feedrate (rn^hr) = 2427
tlrrw Pnm Bat of MM tad (hr)
TEST 7 (8/9/89) ARSENIC
bcrubsoi Wjy*c&m ooNQcrrnmN
ran Bator
kiln tarperature (F) = 1S0Q
afterburner terperatxe ;c) = 2000
feed chlorine (wt 35) =4
liQLor pH =8.1
metal feedrate (ng/Tir) = 3218
TEST 8 (8/11/89) ARSENIC
oubij ia-osrma
kiln terrperature (F) = 1633
afterburner tarperature (F) - 23CC
feed chlorine (wt %) = 4
liquor pH - 6.6
metal feedrate (me/hr) = 2369
79
-------
TEST 2 (8/2/80) ARSENIC
9CKUSBBI UMKOOWN COMCOfTIWKM
E
0.4 -
OJ* -
2 4
Ttma Fiun Bat of Uriah M CM
TEST 3 (8/4/89) ARSENIC
sonuoirn aooDOWN oaiaofrxrai
0.35 -
aisaeoi n-o.aa
kiln tarpersture (F) = 1700
afterburner terpentine (F) = ZDOO
feed chlorine (wt %) =4
liqLor pH = 8.8
metal feedrate (rrg^-ir) = 3240
Tim* Ptwn ftal
-------
TEST 6 (8/15/89) ARSENIC
SCAUBBEK GLOWOOWN OONCEMTIWON
0.4
kiln tenperature (F)
= 16C0
afterburner taiperabjre (F) _ 1560
feed chlorine (wt %) = A
= 7.0
= 2898
0.33 -
¦3
0.3 "
liqjor pH
metal feedrate (mg/tir)
£
I
E
I
a,042S0< r2«0.9B43B
0.19 -
ifrrvlt - 0.078
009 -
0
2
Tlma From Start of IMdi had (hr)
TEST 5 (8/16/89) ARSENIC
SMUBKR SLOWDOWN OOMCDTWOWM
kiln tsnperature (F) = 1630
afte±urner tenperature (F) = 2125
feed chlorine (wt %)
liqior pH
metal feedrate (mg/hr)
03 -
I
J
e
,D47Bi r4«OJl7B7B
0.9 -
0.15 -
0.1 -
a
B
2
*
0
I
Tims Frwn ttot «f MM NM (hr)
81
-------
TEST 1 (8/17/89) ARSENIC
gORUIBCX &MIMWN COMCENTMMM
O,*
kiln hnrperature (F)
afterburner tarperature (F) = 2000
Teed chlnrire (v.t %)
liquor pH
rretal fesdrate (nq/hr)
0,30 -
OJ2S -
r2-O.SS320
0.1 -
IfrnR - OJ33I
a 09 -
3
0
I
a
4
9
Tlmd From tart of Mstol FMd
kiln tefTperature (F) = 1600
afterburner Laipmature (F) =
feed chlorine (wt 30 =8
liquor pH =0.1
ratal feedrale (rng/hr) = 2800
TEST 9 ("7/23/89) ARSENIC
¦LOWOVM CONCENTRATION
SOI
o.;
0.03BOSI ra«0.48340
datMtfon dhnrt
0.1 -
M«tali Ptttdt 1043-1924
O
s
a
Tint FV-om Start of Matalt r«»d
82
-------
TEST 4 (8/1/89) BARIUM
BOtUBWR SLOWDOWN CCMCOTIWON
kiln tavperatLoe (F) = IfflO
afteifcurner tsrperature (F) = 2000
feed chlorire (wt %) =4
liqucr pH = 9.0
retal feedrate (mg/hr) = 20562
TEST 7 (8/9/89) BARIUM
wammaa mxmoom cxmooamtam
kiln tenperatxie (F) = 1600
afterburner teTperature (F) = 200C
feed chlorine (wt %) =4
liquor pH =8.1
metal feedrate (rrg/hr) = 25950
TEST 8 (8/11/89) BARIUM
OJ-
kiln teiperature (F) = 1600
afterburner tenperature (F) = 2000
feed cMorine (wt %) =4
liqjor pH = 6.6
netal feedrate Ong/hr) = 18724
ChO
83
-------
TEST 2 (8/2/89) BARIUM
SCAUQBER OjOffOOWN OOKOOcnUJlO*
Tlmi nam Bart or Wdi tari (hrj
kiln tgiperature (F) = 1500
aftertximer temperature (F) = 200C
feed chlorine (wt %) - 4
liquor pH = 4
metal feedrata (rng/hr) - 26G85
TEST 3 (8/4/89) BARIUM
someni iuwdovm oonobitimion
kiln tsTperature (F)
afterburner temperature (F) = 2000
feed chlorine Ut %) = 4
= 3.8
= 27434
= 1700
liquor pH
metal feedrate (mg/hr)
«lnp«^) omnrii rj-0.*1128
o
2
Tim* tan tot of IMril fM (hf)
84
-------
TEST 6 (8/15/89) BARIUM
nUBBEH 9-OVfOOMN OON«THAJ»ON
1.4 -
1.1 -
1.9 -
1.1 -
1 -
OS -
0>B -
kiln terperature (F) = i£0
afterburner temperature (F) - 1S6C
feed chlorine [\,\t %) = 4
liquor pH = 7.0
metal feedrate (mg/hr) = 24662
0.7 -
OS -
03 -
*opr—o otuee; (MLflae2fi
0.4-
0.3 -
0.2 -
... , ——p- ....... 1
0 2 4.
Tkna Prom Slot of MAM Ftad (hr>
TEST 5 (8/16/89) BARIUM
EMUIHK ¦AWDWW OOMOORWIIOM
1.4
kiln terperature (F)
a-tertuuET tsnperature (F) = 2125
resd chlorine (wt %) = 4
= 7.3
= 25847
= 1600
i ja -
liquor dH
(TEtal f^sdrate (mg/hr)
oa -
0.7 -
rfiy nJTOPOi r2^.MI74
OJ -
a
4
o
1
9
9
Tlma Frarn Ctfft MM fM (hf)
85
-------
TEST 1 (8/17/S9) BARIUM
rational BjOwoowm oattoeniMKM
«|MI C.I7B7T1 n-OJ4TOT
kiln terrperature (F) = 1600
afterburner temperature (F) = 2X0
feed chlorine (wt %) =0
Liqjcr pH = 7.5
netal feedrate (rrg/hr) = 21759
T1n« Pram St«t of MM
Chrt
kiln tarperature (F) = 1630
afterburner terrperature (F) = 2CCO
faed chlorine (wit 96) =8
liqjor pH =8.1
mstal feectate (mc/hr) = 23140
1.*
1.9 -
T-a -
1.1
i
o.s -
o.a -
a7
o.e *
0*B -
O.4.
0-3
o.a
TEST 9 (7/28/89) BARIUM
sonuaam BLOWDOVM OONOCNTRATION
•top* -0.030971 ra-*D/
M«tor» io4a-iBS4
TWm Start of Matala FMd
-T-
O
86
-------
TEST 4 (8/1/89) BISMUTH
gomnan bjOKDONn oONCOmuaoM
10 -
kiln tarperatate (F)
afterburner toTperature (F) = 2000
feed chlorine (wt %)
liquor pH
metal feedrate (rng/hr)
0 -
unoi immis)
a
9
4
Tlrrm from lot of Mtfc* (h*^
TEST 7 (6/9/89) BISMUTH
oo«oo(TMraN
in -
kiln temperature (F)
a^tsroLaxer terperature (F) = 2D00
feed rMorlre (wt %)
liqiDr pH
metal feedrate (rrcAir)
= 1600
= 17216
'i.2KUj
0
2
4
TWm Prom Kart mt IMlif Pmmd (hr)
TEST 8 (8/11/89) BISMUTH
11
1
kiln ts'perature (F)
aftartumer tenpeiature (F) = 200n
feed chlorine (wt %)
liquor ph
netal feedrate (mg/hr)
= 1600
= 6.6
= 16562
I .Ot 32] OQJ7B4
0
9
O
4
Tfn» Pram MM (hf$
-------
TEST 2 (8/2/89) BISMUTH
SCRUBBER BLOMOOfM OOKCtMTIPnOM
o
J
e
0
1
E
J4370J ra*037IM
dot*bUoh iMi •
kiln tsiperature (F) = 150C
afterburner tarpeiature (F) _ 2000
feed chlorine (wt 230 =4
liqjor pH = 7.9
metal feedrate (iig/hr) = 22774
Tlma Pram Bart of MMi Fnd (hr)
TEST 3 (8/4/89) BISMUTH
OOMOCKTIWION
10 -
kiln tenpexatuDe (F) = 17D0
afterburner terperature (F) = 2000
feed chlorine (wt %)
liqjor pH
metal feedrate (mg/hr)
s -
= B.8
= 23830
0
4
2
Tlma From Sort of MrtAi (hr)
88
-------
TEST 6 (8/15/89) BISMUTH
OONCOinMION
10 -
kiln tarperature (F)
afterburner tsnperature (F) = 1860
feed chlorine (wt %) = 4
= 7.0
= 21600
= 1600
liquor pH
metal feedrate (rrg/hr)
O
9
Tlrrw Piun Start of Mtdi M (hi)
TESTS (8/16/89) BISMUTH
11
10
kiln temperature (F)
afterburner torperature (F) = 2125
feed chlorine (wt %) = 4
= 7.3
liqucr pH
metal feairate (mg/hr)
>l.4B0i rMJ6It3
0
0
a
!
2
4
a
Tina rrnn Etort of Mtot HmA 0w>
39
-------
TEST 1 (8/17/89) BISMUTH
KKU»Bt flLQ«DO«K OOttCEKTMnOlt
0.7*970; ra-asns
T\rm from Stat of Uatol
kiln tenperature (F) =• '600
afteibuiner terrperature (F) = 2X0
feed chlorine (wt %) =0
liquor pH = 7.5
metal feedrate (Tig/hr) = 18404
kiln temperature (F) = 1600
afterburner tenperatire (F) = 2000
feed chlorine (wt 35) =8
liqjor pH =8.1
metal feedrate (mg/hr)
TEST 9 (7/28/89) BISMUTH
sowunliu SLOWDOWN OONOCMTnATION
tivi« Ftoiti Stort of U«toi« r««d
50
-------
TEST 4 (8/1/39) CADMIUM
floauflag BtdwowN c«tctwn*nm
kiln tarperature (F)
afterburner tenperature (F) = 2CD0
feed chlorine (wt %) = b
= 9.0
= 548
= 1600
o.aa -
0,2 -
o.i a -
llqjor pH
metal feedrats (mg/hr)
0.14 -
0.1 -
c
I
I
.02880] r2-O£S740
0,08 -
0.02
4
a
2
Tlmi from Bat oT IMtfa M (hr}
TEST 7 (8/9/89) CADMIUM
muMot aowooww oanoBiTtmaH
kiln tsTperatxie CF) = 16C0
afterburner tsiperature (TO = xm
feed chlorine (irit %)
liquor
metal feedrate (nrg/hr)
o.aa -
0
J
1
J
= 680
0.12 -
0.1 -
•&CD970; r9«4L81l
0.08 -
4
0
9
ThrM From Bdrl of IMdi IM Ow)
TEST 8 (8/11/89) CADMIUM
kiln tenperature (PO.
afterburner tenperature (F) = 2000
feed chlorine (wt MD
liquor pH
metal ffeedrate (mg/hr)
= 1600
0.3 -
O.IB -
= 521
0.18-
#QQg aoa7BO| r2-O.84480
ai -
0.08 -
0.08 -
0.03 -
9
~
0
lima Flwn ftort of UUi IM (M
-------
TEST 2 (8/2/89) CADMIUM
scauuat buowoonn fionoomvooN
0.36 -
0.34-
kiln tenperab_re (F) = 1500
afteibumer tenperature (F) = 2000
o.a -
feed chlorine (wt SS] = A
o.ta -
liqjor pH = 7.9
0.10 -
metal feectate Cng/hr) = 684
0.14-
0.12-
0.1 -
aoa -
0.09 -
iapfttf.08B10; r2-038420
0.04-
0.09 -
0 4
(n«ridrt»ei Mi U Mwfon IrrA — 0.01 f >
0 9 4
lima Pttan Start vf hMdi fM |hr)
TEST 3 (8/4/89) CADMIUM
WRuaaai mowwwt oqmohtimion
«0»*-04>e7B0l r2M}.#8B77
Martian IM - ooom
kiln tenperaturs (F)
1730
afteitumer teroerafcuce (F) = 2CCD
feed chlorine ('Aft %) = A
liquor pH = 8.8
metal fesdrate (mg/hr) = 722
Tliw From mat of Midi M (M
92
-------
s
1
TEST 6 (8/15/89) CADMIUM
BCmiBB
0.1 B -
Q. < 4
04320! f3—OJJ3M1
OiGO "
0.04 -
0.02 -
kiln tenpsrature (F) = 1630
afteitxirrer terperature (F) = 1860
feed chlorire (wt %) = A
liquor pH = 7.0
metal feedrate Crrg/hr) = S59
Tima Pram Birt of htetcta fead (hr)
TEST 5 (8/16/89) CADMIUM
0.30 -
0.34 -
0.22 -
kiln temperature (FO = '6QQ
^ o.a -
afterburner temperature (F) - 2125
"• an -
feed dilarine (wt %) = 4
E 0.11-
liquor pH = 7.3
1 0,14-
metal feedrate (mg/hr) = 693
1 0,13-
c 0.1 -
ttapm OQgBOt (MJB703
I 0.01 -
1 O.Ofl -
0.04-
0.03 -1
0 -
V 1 1 1 \ » 1 1 \
I (V)
93
-------
O.M •
0.24-
0,72 -
aa -
0.1B-
0,f«
0,14 ~
0.12 -
0.1 -
aoo-
0.00 -
0.04
0,02
0
TEST 1 (8/17/89) CADMIUM
sttumea umbmn ooaooiTiiaioti
Tim* Fm Start of MM Mma (Ml
kiln tenperature (F) = :6X
afteitxiner temperature (F) = 2000
fed chlorine (ic± %) =0
liquor pH = 7.5
nretal fearate (mg/hr) = 593
kiln terrperature (F) = 1600
afterburner tsrperature (F) = 20D
feed chlorine (wt X) =8
liquor pH =8.1
metal fedrate (mg/hr) = 647
TEST 9 (7/28/89) CADMIUM
0.2B
O.S4
a.22 -
-
o.ia
Q.16 -
0.1-4 -
0.12
0.1
o.oe
O.O0 -
0.04 -
O.C32
o
BLOWDOMN aONGENmATION
tiop*^o^3ea2} rSMs^aaes
dtuotion rv^rt — 0.011
—i—
a
Mortals 104^-1824
TVn* Fbom Stdft of Matola Fm
-------
3
TEST 4 (8/1/69) CHROMIUM
aotUMCH KAWOOWN OOHCeiTIMXM
tk!!¦ 0.0 HW r3-0.3BI07
kiln tarperature (F) = 16CD
afterburner tsrrperature (F) = 3X0
feed chlorire (wit X) = 4
liqjor pH = 6.6
metals feedrate (mgAir) = 2677
Dm Pnm MKMUi KM Ow)
95
-------
TEST 2 (8/2/89) CHROMIUM
0.4
OJfl -
kiln tarperature (F); = 1500
afterburner tarperature (F) = 2000
feed diluriiK (wt %j -A
= 7.9
= 2084
OJ -
liquor pH
metal feedrate (mg/hr)
0.39 -
J OK ¦0,038101 rML7a0Ofi
s
I
0.1 -
a 0.003)
td
2
0
4
TVna fibwi mat or mmi M (hr)
TEST 3 (8/4/89) CHROMIUM
kiln teiperature (F) = "7C0
afterburner tarperature (F) = 2COO
feed chlorine (wt %)
liqjor pH
metal feeclrate (mg/hr)
o.ia -
•toM^oaion
0.09-
2
4
0
lima Pram fltvt of IMdi had (M
56
-------
TEST 6 (8/15/89) CHROMIUM
O.A
kiln tcnperature (f) = 16C0
afterburner tenpRrabure (F) = 186C)
Feed chlorine (wt %)
liqjor pH
retal fesdrate (mg/hr)
= 7.0
= 2507
4Op*a*O.(flS70l rM).0fB79
0.1 -
0.03 -
a
4
2
71nrn Frsti Kat of MMi (hr)
TEST 5 (8/1 6/89) CHROMIUM
0.4
kiln tarperature (F)
aftsitoumer tsiperature (F) = 2125
feed chlorine (wt %)
liqjor pH
iretal feectate (mg/hr)
= 1600
I
&
\
= 7.3
= 2677
0.1 -
0
4
2
firm Pwm Rat of Mrtol fM 0*0
97
-------
0.4
TEST 1 (8/17/89) CHROMIUM
EOHUOTKH «jO«DO*M OONGOfffWIOfi
I
OM -
0.3-
aw -
a.2 -
0.1 s-
o.t
0.00
0
0.013321 rM.PMO
kiln ta-perature (F) = :6J3[
aftsrtxuner terperature (F) = 2DOO
feed chlorine (wt %) =0
llcpor pH = 7.5
metal feecxate (mg/hr) = 2505
Tin* Ftom Start of IMal And CHf)
kiln teiperature (F) = 1600
afterburner tgrperature (F) = 2000
feed chlorine (wt %) -8
liquor pH =8.1
netal feectate (mg/hr).•- = 1981
TEST 9 (7/28/89) CHROMIUM
SGPtUOaeR SLOWDOWN OONOCNmATION
7im« fVw Start of Mstalt r««d
98
-------
TEST 4 (8/1/89) COPPER
9 -
ts-
r wawmMwi miwwi uuwamw»wt
14 .
t.7 -
t.e-
ab«MH3.27300] r»*0£74a4 '
i j -
»«~-
i j -
»~*-
i.i -
i -
&9-
OJS -
0.7 -
O J -
&9 -
0.4 —
0.3 -1
(W -
0.1 -
1 * i
0 2
4
kiln temperature (F) = 160D
afterburner tenperature (F) = 2KD
feed chlorine (wt %) - k
liquor pH =8.1
ratal fesjrate (rtg/hr) = /tlBD
Him Pfwn Hart of IK* IM (hr)
TEST 7 (8/9/89) COPPER
nUBBOt MWOOWW OOMOORMflM
1B4SII rMLOMO
kiln tenperature (F) = 1600
afterburner teiperaturs (F) = 2000
feed chlorine (ivt %) =4
liquor pF =8.1
metal feedrate {ng/hr) = 25190
TEST 8 (8/11/89) COPPER
-------
TEST 2 (8/2/89) COPPER
scMuasn notvom oomocxthoioh
D.09BI 01 13-O.IDTB
kiln taiperature (F) = 1500
afterburner teiperatxae (F) = 2000
feed drlcrine (wt %) = 4
liqjor pH = 7.8
metal feedrate (irg/hr) = 24962
Ttma Piwn laiaf
TEST 3 (8/4/89) COPPER
OS*
m» ran laiarNMi im M
kiln taiperature (F) = 1700
afterburner taiperature (F) = 20GC
feed chlorine (wt 35) =4
lionr pH = 8.8
metal feedrate (mg/hr) = 26187
100
-------
£
B
0
1
TEST 6 (8/15/89) COPPER
Bcmmai bjdmikmw cotnomKioN
doc. D.OBiaOl
kiln tsiperature (F) = 16C0
afterburner terrperature (F) = I8ffl
feed chlorine (wt %) =4
liquor pH = 7.Q
metal feedrate (mg/hr) = 240138
(M
TEST 5 (8/16/89) COPPER
I.B -
«DM-o.iaim i2-o,bidsi
D,3 -
kiln tenpeiature (F) = 16C0
afterburner tarperature (F) = 2125
feed chlorine (wt %) = 4
licjjor pH ^ 7.3
metal feedrate (mg/hr) = 24939
Una rram Bol ar
131
-------
TEST 1 (8/17/89) COPPER
SOKUaKX BLOWOOHm OOMXMTIWION
o.a -
0,2 -
kiln temperature (F) = 16D0
afteitjumer tarpsrature (F) = 2300
feed chlorine (wt %) =0
liquor pH = 7.5
metal feedrate (mg/hr) = 21161
Tim rnsm Blot of MM PMd (hr)
TEST 9 (7/28/89) COPPER
SCRUBBER BLOWDOWN CONCENTRATION
slope=0.19503; r2=0.94532
8lope=0.39949; r2=0.90902
slope=O.B2J7
0.6 -
kiln terperature (F) = 1600
afterburner terperature (F) = 2C00
feed chlorine (wt %) =8
liquor pH =8.1
metal feedrate (mg/hr) = 22791
Metala F««
-------
TEST 4 (8/1/89) LEAD
o.a
kiln tEnperatiire (F) = 1600
afterburner tarperabjre (F) _ 2000
Teed chlurine (mit %)
liqjor pH
iretal feedrate Org/hr)
5
s
8
I910| r9HS.MBl7
0.3 -
0.1
0
a
4
TTm» Fram Kvt of Mttflfc TWd (hO
TEST 7 (8/9/89) LEAD
M
0.7 -
kiln tenDersture (F)
= 160D
afterburner tarperature (F) - 2T0
feed chlorine (wt %)
llqjQE pH
metal feedratc Cng/Tir)
o.a -
0.4-
0.1-
c
i
0.2-
0.1
2
4
0
Ttona FBih Bat of Widi had (hO
TEST 8 (8/11/89) LEAD
OB
kiln tenperature (F)
afterburner taiperature (F) = 2QQC
feed chlorine (wt %)
liqLcr pH
riEtal feedrate (rng/tr)
= 1600
3
4
= 6.6
= 2777
e
i
0.1 -
0
4
a
Dm Pran Bart of IMA tad (hf)
-------
TEST 2 (8/2/89) LEAD
bmumoi vmoovM ooKcnnnmo*
i
&
Q.7 -
kiln tarperature (F) = 1500
(LA-
afteitumer teiperature (F) = 20GU
feed cnlorine (wt %) =4
OS -
liquor pH = 7.9
ratal feedrste (mg/hr) = 2818
o.««
OJ -
OJ -
^ dep^OjOISOi r2-0.!2182 —
a.i -
0 H
r , 1 \ |
a
> mart or
I 0«)
TEST 3 (8/4/89) LEAD
0.7 -
kiln terrperature (F)
afterburner tarperature (F) = 2000
feec chlorine (wt 90
liqir r pH
metal feectrata (irg/hr)
= 17C0
o
&
= 8.8
= 2940
1.000
0,1 -
4
O
2
Tkra rrrnn Bart of TTilrH tad (hr)
104
-------
TEST 6 (8/15/89) LEAD
aOBUMOl BLOWDOW OOOOP
-------
2
i
TEST 1 (3/17/89) LEAD
DQftUBOEX SLOWDOWN OOMCCMTIMnON
O.B -
0.2 -
¦tip^anaiii n-aamn
kiln tarpersture (F) = 1600
afterburner toerrperatxxe (F) = 2DCD
feed chlorine (wt %) =0
JiqLDr pH = 7.5
metal feedrste (ng/hr) = 2563
Tima Pram timt or iium naad
-------
TEST 4 (8/1/89) MAGNESIUM
acwwa aowpowH cotwonagion
Iftn* nam Rata* 1M» n>M Ow}
TEST 7 (8/9/89) MAGNESIUM
kiln tHTperature (F) = 1500
afterburner tarperature (F) - 200C
feed chlorine (wt %) = 4
liquor pH = 9.C
metal feedrate (mg/hr) = 1030
kiln tarperature (F) = 1600
afterburner taipertLrs (F) - 2000
feed chlorine (wt %) =4
liqLor pH =3.1
rretal Fmdrate (g/hr) = *226
Tim* mm MilMUi tad (hr)
TEST 8 (8/11/89) MAGNESIUM
kiln terperature (TO = 1600
afterburner temperature (F) = 2X0
feed chlorine (wt 35) = A
liqjor pH = 6.6
metal feedrate (tyhr} = 1203
Tkiw mm Kari of
\
1C7
-------
TEST 2 (6/2/89) MAGNESIUM
muagcn hjdmoown oomxxrnmm
11
'Kiln taiperature (F)
afteitiurrer terrperature (F) = ZJDO
feed chlorine (wt %)
liq_or pH
metal "eedrsr.e (g/hr)
= 1500
= 13
= 1034
dap^Q.2490; r9« 0.004X4
2
O
2
4
Tim Pram Owl of Itad
-------
TEST 6 (8/15/89) MAGNESIUM
Bo*usaex axMBMM ooNcanaaioa
Hi I4-0.I73BI
kiln tarperature (F) = 1600
afterixrner tarperature (F) = 1560
feed chlorine (wt %) =4
liqjor pH = 7.0
metal feectate (g/hr) = 1186
Tim* P»wn Out Of
TEST 5 (8/16/89) MAGNESIUM
i ooHoaawmi
kiln tarperature (F) = 1600
afterburner temperature (F) = 2125
feed chlorine (wt %) =4
liqjDr pH = 7.3
metal feedrate (g/hr) = 1169
109
-------
TEST 1 (8/17/89) MAGNESIUM
Hjmjooe* ouoaowm txmonnmmm
kiln tenperature (F)
afteibumer termerature (F) = 2000
feed chlorine (a! %) - ~
= 7.5
= 1209
to -
= 1600
liqjor fJH
metal feedrate (g/hr)
Mtari r^ojoao
Q
I
a
9
a
Tim from Hot of UM IM (hr)
kiln tsrperafcjre (F) = 1600
arteituiTei' taijjerature {-) = 2000
feed chlorine (wt %) =3
liquor pH =8
riEtal feedrate (g/hr) = 985
TEST 9 (7/28/89) MAGNESIUM
sonuaim gLotwovm ooNoeNmmaM
10 -
unsoi r:
Matofa rbadt 1
a
e
a
o
TVrtv Phjfn Start of Mvtals f«td
110
-------
TEST A (8/1/89) STRONTIUM
kiln tarperature (F)
afteiteunur laiperdlure (F) = 2000
feed chloric (ivt %)
liquor pH
metal feedrate (mg/hr)
0.7 -
= 9.0
= 21725
o.o -
OB -
1.011401 ixurati
OJ
0
2
4
TVrw Pram Bat of Itttdi mm (V)
TEST 7 (8/9/89) STRONTIUM
kiln tenperature (F)
afterburner tenpcrature (F) = 2C00
feed chlorine (wt %)
liquor pH
metal feedrate (mg/hr)
= 27271
OS-
0
a
4
Hrw Pram Bator Or)
TEST 8 (8/11/89) STRONTIUM
BMH BLUWWI OBMOBWHW
kiln tenperature (F)
afterburner tenperature (F0= 2000
feed chlarine (wt %)
liqjor pH
metal feedrate (mg/hr)
= IffiO
i.a-
= 6.6
= 20021
&B
a
4
O
TVn* mm ftst of fctttfa taatf
111
-------
TEST 2. (8/2/89) STRONTIUM
¦wiw auMoow oowoonmiiow
kiln terrperature (F) = 1500
afterburner terperature (F) = 2000
fscd :hlorire (wt %)
liquor pH
UEtal feedrste (mg/hr)
0.7 -
= 7.9
= 27018
dap— O.OaiaOl
0.3
a
2
4
TWn» from Start vf IMrtm Pwd (hr>
TEST 3 (8/4/89) STRONTIUM
'iuaaioi ra^Meai
OJ
a
4
9
Tim rmn i«t of mmm M M
112
-------
TEST 6 (8/15/89) STRONTIUM
wuamtom oaaaafiiMXM
04
kiln temperature (F)
= 1600
aftertumer tenperature (F) = 1853
feed chlorine (wt %) = 4
- 7.0
= 26028
0.7-
liquor pH
metal feecrate (mg/hr)
dapa PJtBTb r2-0«Wi
04 -
0
2
4
TWna pram Sat off IMA IM (hr)
TEST 5 (8/16/89) STRONTIUM
04
kiln temperature (F} = 1600
aftertumer taiperdtuiE (F) = 2125
feed chlorine (wt %)
liquor pH
metal feedrate (mg/hr)
0.7 -
2
&
= 7.3
= 27176
0.0 -
1 b
0.4-
D
1
9
3
9
4
Una Worn Kavt «f MaM IM (hr)
113
-------
'J
i
TEST 1 (8/17/89) ST^ON/flUM
I mOWDOWfl OOMCXIMTIM7IOM
^J,0143fe rft-O317B0
kiln teqperaluLK (F) = 1600
afterburner tarperature (F) = 20CC
feed chlorine (wt X) = 0
liquor pH = 7.5
iretaJ. feecrate (mg/ftr) - 22926
TVw Pram Suit td IMri
kiln tarperature (F) = 16CC
afterburner tan^rature (F) = 20CD
feed chlorire (wt %) = 5
liqjor pH =3.1
metal feedrate (ng/frr) = 2421
TEST 9 (7/28/89) STRONTIUM
SORUBBCK SLOWDOWN OONGCKTKATtON
Tlm« F> IXV > Start of Fitfl
114
-------
APPENDIX C
ANALYTICAL LABORATORY REPORTS
In the following reports, each sample has been assigned a sample ID number that
consists of a letter prefix, eight numbers, and usually a one or more letter suffix. The prefix
denotes the sampling location as follows:
• A: Sample taken in the afterburner exit flue gas
• B: Sample of the scrubber blowdown
• E: Sample taken in the scrubber exit flue gas
• F: Sample of the incinerator feed
• Q: QA/QC sample prepared in the laboratory
• S: Sample taken in the stack gas
• T: Sample of the kiln ash
The first four digits of the eight-digit number represent the month and day the sample was
collected. The last four digits represent the 24-hr clock time the sample was collected. The
suffix denotes the sample type as follows:
• F: Filter sample
• FBK: Field blank sample
• FSK: Field spike sample
• II, 12, etc: First impinger, second impinger, etc.
• M5: Method 5 train sample
• MSK: Matrix spike sample
115
-------
• PW: Probe wash sample
• Tl, T2: First sampling train, second sampling train
• V: VOST sample
Table C-l summarizes the sample ID numbers for the samples collected or prepared in
this test program.
116
-------
Table C-1. TEST PROGRAM SAMPLES COLLECTED/PREPARED
Sample Type
Test 1
Test 2
Test 3
Test 4
Test 5
Clay/organic liquid faed
F08161050
^08151055
F08161100
f (10011220
F08021030
F08021105
F0802I040
F08021045
F07311305
f 07311315
F08011215
F08160750
F08160800
F08150830
Aqueous metals spike solution
f'08171300
F08C21325
F0804I245
F0301I33S
F08161301
Kiln ash
T08171400
T08031350
T08041130
T08011400
T00161300
Kiln ash TCLP
r081714D0TCLP
T08031330TCLP
T08C41430TCIP
T0801 MOOTCIP
T08151300rCLP
Scrubber blowdonn
808170845
B03170956
80817105S
8081711S6
608171256
803171356
008020900
008021020
B08021120
803021220
808021320
608040900
808041000
B08041037
B03041137
808041237
808011337
B08010900
B 03011103
B08011203
U08011303
BOfl01M10
B08160805
008160913
B081610I3
808161113
B08161213
808161300
Multiple metals
train, afterburner exit
Probe wash
Filter (thimble)
First and second 1np1ngers
Third Inplnger
Fourth Impinger
Multiple metals
train, scrubber exit
Probe wash
Filter
First and second inpingers
Third Impinger
Fourth impinger
808171450
808171502
A0C17091I6H17PH
A08I70956H17T
A08170956M17I1I2
A08170956.H17 [3
A08170956.^17] 4
E08171002M5PW
£08171002H5F
E08171002M5I1I2
E08171002MSI3
E08171002H5I4
A08020950H17PW
AOD020950H17T
A08020950M171II?
A080209S0N17I3
A08020950M17I4
E08021015M5PN
E0802101SM5F
E08021015H5I112
E08021015M5I3
F.08021015M5I4
A080J1037H17PH
A08041037N17T
A08011037M17I112
A08041037M1713
A08041037M17I4
E08041040M5PN
E00041C40M5F
E08041C40M51112
E08011040M5I3
E08041040H5I4
A08011103M17PH
A080I1103M17F
A08011103M17I112
A08011103N17I3
A08011103M1714
E08011104M5PW
E080I1104M5F
5080111D4M5I112
(":0801110«M5I3
E08011104M5I4
A08160913H17PH
A08150913N17T
A08160913M17I1I2
A08160913N1713
A08160913M17I4
E08160925M5PH
E03160925M5F
E08150926M5I112
E08160926N5J3
E0816092SM514
Method 0030 trains
Afterburner exit
Scrubber exit
Stack
A08171017V
A08021043V
A08041107V
A08011117V
A08161033V
A08171016V
A08021120V
A08041141V
A08011220V
A03160954V
A0B171112V
A08021201V
A08041217V
A0801133BV
A08161109V
E08171066V
E08021012V
E08041106V
E08011119V
E08160952V
E08171046V
£08021118V
E08041144V
E00011215V
E08161032V
EC8171112V
E08021159V
1:08041219V
E08011338V
E08161190V
S08011118V
308011214V
S08011338V
-------
Table C-1. TEST PROGRAM SAHPI Ef. COI.LECTOD/PREPARED (CONTINUED)
Sample Type
Test 6
lest 7
Test 8
Test 9
Method Blank Matrix Spike
Clay/organic liquid feed
F08101000
F08101010
F030Q0800
F08090805
F08090805
F08090807
F07251620
(¦"07251823
MO9111340
Aqueous metals spike solution
Kiln ash
Kiln ash TCLP
Scrubber blowdown
Multiple netals
train, afterburner exit
Probe wash
Filter (thimble)
First and second impingers
Third impinger
Fourth ltnpinger
Multiple motals
train, scrubber exit
Probe wash
Filter
First and second impingers
Third impinger
Fourth impinger
Method 0030 trains
Afterburner exit
Scrubber exit
Stack
F081513045
T08151400
T0815l100rCLP
008150900
B08150957
608151057
808151157
B08151257
808151357
A08150957H17PW
A08150957M17T
A08150957M17I1I2
A03150957H17M
A08150957H171/
E081510I4M5PW
E08151014M5F
E081510MM5J112
E0815I0I4N5I3
£08151014H514
F08091J30
T08091330
T08091330TCLP
B0C090910
80(1091025
808091125
308091225
B08091325
A0B091025M17PH
A00091025M17T
A08091025M17I1I2
A0809I025M17I3
A08091025M17I4
E08091025M5PN
E08091025M5F
E083S1025H5I112
E0B091025HSI3
E08091025H5I4
F0ai11134
T08111230
T081 1 1230TCIP
808110758
1)08110530
803110930
B00111030
B08111130
1)081 1 1230
A08110830M17PW
A08110830N17T
AOS 1 10830H1711J 2
A08110830M17I3
A08110830M1714
E08110832M5PH
E08110832N5F
E081 10832M51112
E08110832M5I3
E08110832M514
F07201705
T07281639
T07231639TCLP
B07201002
UG7281321
BD7281521
U07281 S31
B07281S31
1)07281730
B07281830
A072B1234M17PN
A07231234N17T
A07281234H17]1]2
A07281234M17I3
A07281234M17J4
E07281234M5PH
E07281234M5F
E07281234M5I1J2
E07281234M5I3
E07281234M5J1
Q01161200F8K
Q08031330TMSK
Q08031330THSKD
Q0817H00MSK
Q08171400TMSKD
Q08161300BHSK
g08!613006NSKO
003121520BHSK
q03l21520UM:iKO
Q03151000A1MSK
Q03151000A1MGKD
Q03121511A2MSK
Q03121511A2MSKD
Q0 31215 0 OE1MSK
Q03121500E1NSKO
Q03121501E2MSK
Q03121501E2MSK0
A08151053V
A08091106V
AflOl10916V
A07281435V
Q07281530VF8K
Q07281S18VFSK
A08151140V
A08091202V
A08110958V
A07281530V
Q0801I338VFBK
1)08011214VF5K
A08151239V
A08091245V
A08111043V
A072B1618V
Q09021159VFBK
(J08021118VFSK
Q08011141VFBK
Q08041106VFSK
E08151052V
E0809110SY
G08110917V
E07281135V
Q03091106VF8K
Q00091202VFSK
E08151139V
E08D91202V
E08110958V
£07201530V
Q08110958VFBK
Q08110917VFSK
E08151314V
E08391244V
E08111041V
E07231613V
008151139VFBKT1 Q08151239VFSKT1
Q08160952VFBK
Q08161032VFSK
S08091105V
308110917V
Q08171016VF0K
Q0B171046VF3K
S00091202V
S0811095RV
508091244V
5081 1104IV
-------
Appendix C-l
Sample Tracking Records
119
-------
•/r^rv^x"
TC-T gjf*
I^d-edl£>cj3r/cr>^--
MT5:^- ll-?>
¦N ROTARY iM INCINERATION SZ7H IONIZING i£T £3S3£S
winir»— » i i
CLAY/Cr3ft*iiC
f n) jj#5. ... _
rO^lfemSokj^ft) rOS lb)o5o/;Q9[MOqO/ f-P3l(.- 105^ / 7<
ro«3 1 fc in S 5fR v a«u?.-p^lt. I0&5. rO< L> -/
as&y
?o & n 13 5 L s
/VA? ~
ioKi1f5blj S •'
gOS 11 12 5> (a 40 ft. VCS {CC-hiSIE;
157 i 1'i'D IflrlNG
3-RC :hri;i£E?:
4"ri IffltSS
Pf?]5t ?iiH
SA^_E Z&M SriAFrH'; HEL SAf?-_Ei
zn'Vllo ?5b> fi77
^nofi fc ni7[i^iqo-t- n/70^ (• *Psi7V.!?v-S
SETHGD 3 TWIN f-St£7
CSQDC yi;IU
FT!
Z-W1
E OS nips'.
!M>^
15" i M Irt-ISSES £ BgiVbci'
TRS ISPifcES £ e>^/Q/|8oab
47H InFIME? £ CSlUDDjj-
.fTIHDD 5 TRAM STACK
F=lBE »h£H i Dm 1041
FILTER c it iheyi
1ST 1,1-INSES
2fuj IfiriNS£3
3RD INPINSE3
"rSIi
K514 /
±ML
JM£.
2^0
ML
?e?K
32? Jj
32/^i
ic^nibci^. -en
= e Unto#
fp7}
«5I2
soxnio'f!
M5I3
120
-------
Mvi- w j" o i V^Y
•J=£=S-:?5 XSSSi
te=t .'(L'ffiS: 2^ Fee<^ mix *2.
^ s-z- 8*1
^j/t2 ZE~J?¦e^*-Jr/-Cte^a-^ 'c
RACE METflLS IN ROTARY KILN INEINESATICN «TH I&UZIKE WET SaffiES
SAHPLE TYPE
CLWOSeSMIC FEED
SAMPLE 1.3.
FO^aio
r C3Q2 \ P~5Q
Fb<*CA 1105
CBtfUE (SCHL VOA) ifes (14 HLj , SPURS ITH "25 "U EF3 t4ft t?
FOteUZ^P ^ rases naao ^ FdSOxiMii/ FOMUaao.
FQKCXlQ^O " FQ3Q\|03C> ^ Fomia36 F QfjQ3L »03Q
FO9C9.l\05'/ FO^a. VtDFS./ F \ t&cy^ FCPbail&R
hDUSsul? rETAL 3K r 0$f&\3Z5 10 t ^
rEgCl^to 10 KL
KILN ASH
kilh ash tclf
SiSLrrEH 3LSJD3W
I OgM35fl s KL w/
~o %C)3 135Q 40 riL m
T0SC3i335 3SfnL CvJes") ^
TQ^o^H^SMomL VO^ (.CtwMie.^
t r>9,o^1i3"6c> tll° T0103)53_5_
EO^lOq&O ¦/ bOSC£H>2D ML «Cfl iCCNNIEi
;o9C.3l i 030 •
E08r^a \ *-
Efi^n^\3.^o ^
sOSo^ J
E
.lEThDE' 17 TRS'N
TK-fSlE 'rILTS;
• :57 ^-=5-^^-
:FD IMPIfJSE.-:
4Tn rnPiNSEf.
?s3EE #=H
-•2HD-LW?-Ni=S
JGTHOE 5 RAM E-Dl£7
ksh tea
f:l~5
1ST k
3=1! la?:;-}©
4TB irflNGES
>Nt> xiA?moe?.
aoscao^o
ftO903> o^o
Aftg.0^oq5C>
a oS 0^0^50
rj^2v§^_
noso3> 50
e oqo2.iQ\ 5
iiH:
3#SK's fCL 5/SKFlEE
.(117"
H17Ii ^
J117I4 /
-117ft J
Tnni2
Ef>3C 1 IQiS
E_Dl8-DXJLDA5_—" /
E oftoa \ Ol £» *5i4^>
= 0'50?> 10 v *b-
fiTHDD 5 F.AIN STACK
?K= HASH.
FILTER
1ST iHriSGES
2*ffi ifiri«2
3RS I flP !.'££«
= oqcziD
SOSCX 10 57 *=F
&
>eps
_H57!l L ni\\^
V5^\i
_hAJLmlk_
i2l5 mis
iOsGtA\S ECS02 \CU5 ;g;i (_\G9rr\Va)
2 5c ng\s
' 3. 5 m-fr
"3 V) «M<>
£, ¦
:Q%02\P57 hs;i
3 O s; 03 \Q 5*7 h-3i:
- I 0 5-7 nE:3
5 St mVs
lb& j
O&l rnl G
7X"
121
-------
ill
ii
5:
CM
•#
if
aS
V
LL-
cr
51 WCP
v:;t
!;;§!»>
nL. »- u»
(It III I—
!1! H' S
3
Li!
hi
C
X
••2
-jOC
:7p O
05
a
K!
!t 3
-
til O
zt
a
c<
o
cc
Lu
ti.
\
ir>
'3-
ns
¦?
o
0<*
.o.Q
&
£
\
f
3^ it!
n
?
o
O
3
o
o
to
17%
o
r—
s
iS
o
m
-*-
»Q
>/)
t
o
o
3
<0
1
o
0
£ £ £
irir o
f0 -S K
Klr< C
O
*1"
Cj
Q
\
\
s
c
rf
c
T
0
VI
w
r
CIO
a
c
w
c
£
2p
«Tl
i!
II
r
tf
q
-b
C
V
0
>/>
©qif>
r
t\
i~ r-:
t
«1
c
*
o
00
o
i£i |C| »n III • 11 ill (II ill I'D
r
{0
o
t*
0
01
0
x -X
IH
Sig
3 £
&!
53® e
o ^
- o
o
>-
o
00
01
T
O
C
\
(J III I'l
rn cn
u id
u iti
uj m
s w ti
!!i 1,1 ^
-------
ro
-o
C7
t/\
P
J
o~
-n
a
c/
c
«-»
H
G>
f-
T
y
o-
J
I
CD
_p
fe'H
S3
S m
m !;i
•¦i
r:
s jii
(i
^ c ^
vX ^
Q
i
3* ,'fi
ft #
•" !ii
ar
s L"
:i: 51
to
£
O
oo
o
01
O
:x :r
l-U -tl
-P
(T
5.
CT
«XJ .Cij tr>
O
X5
3
o
bo
o
JI J1 Ji
0
en Lii f'Ji
M l-l M
ci ».i »—
n,
% ±~, &
*-\r. fcj
0tJ Ljj
3
iS R5
t? W !U
£
rr«
•V u
nl
''¦I rE
i_i
m rn
|T1
in
0
O
O
O
CCi
50
,-n,
dQ
O
o
o
O
—
^*
""
—
—
o
a
o
o
•F
4
4^
•¥¦
„
!*]
fi
; -i
o
c»o
C
O
w B S ^ Kl
ro
rO
c"y
>o
o
3,
3.
ir
C7
a>
o
0
-F
5? ifi
... S 3i
=8,., rri
ti:i -j* & -
ffi ~n
HI ;r I-' fd
<1 - I x-
Sr !3
!? ~
ri:. X
CJ
tA
o
:c-
O
cO
a
a O
Oi
(J
^_-
S-
cO
G~
cn
o
_>
O
c?
in
c
3
3,
3,
l/**
Li1
IS
ogf
0
eft
o
a
0l
s
0
t?
01
r
c
0
i/i
to 111 H) lu« rjf ro
.O
i0015?
c? °
JV
b
a
ai
o'c>
r/>,Cfl
a O
O
_n
(7 k?
oi
o
o
;t-
P
r!l
-I
Z>
k>
3
' II
C>
¦II
;?
&
a
CP
o-
O;
o
(7
£
5
£
3>
0
C
aJ
o
a
a
cr
LH
£
to
IJ1
c-
¦r*
—I
? pt
ji
P
D
i
\
r-
r-
n
£
p
ip ,
z
w'
£
-ri H -ri ro
O -c'
u» ['!
i.:i
aJ"
O
(CT
o
o
cx>
Ji
o
oi
J->
CM
U1
\\K:
i LH
p* o
U1 W
--1
!r-
n
Pi
i:iS
S5
a
c
s
ij-1
:ii
¦i£
5
i >i
Q
Ti
/a
CL-
><
"fcl
N>
(A
"tS
.V
-------
*?_?£!( . jt/" a
TE£7 1\; £tt S^r^p'^
^TS: <3 - |!«, ' ? 1 r
-?^i fV.-Ki :m .WTi«ff >:IL1 INC:®*j:CN W7H i*i:;r;G n'ET 5lRl5:£S
SSWl£ TV'PE sKi-Lt t.s. Lurwii wrs. vuw *ts u« ru S«jKfi;iit U2a !2.J t?A ;
CLAv^syiic fed -qaifr PIgQ £v3i J- = ^ i fcolSjyf OS ~ r0S)(,n7^/ 5__
?>\ o e> ,o, / /s'^r> >-./ c _
rAhPLi 1.5.
ESNiE «40«L VDA> £5 fu H.)
rSLSWITH US ft; PA ;40 1 V£S>
....
r<0 ? / 5 o S~3£> P Vis ;.OS
;S2J>_03e_^
*-£tSflgJjA/Fogrqflg?0
~g o f t* I O D—10
.10 ML ^
10 *L ¦/
KILN ASH TQ3jM2QP2iXRv3iJ ^
TiO 11 U I ^0 C*0 it v.:.a
K:LN T5L? T ft? Ha/VIP TIL.'
-S'.-Hir: ?.:iKi5i ? O ? ' O C Cg ^ 'y
jQ? >6) O *) ! 3 S
a£<3 / fr i Q I ^ .f
5Qgf to i I fjK
SO ^ f t, ta 13 <
En's i6i I3afe ^
> 1 b / /< nr: -. vca •c-jwii:'
"ET-5C :" 7Sh:>;
InifSLE '.F:L—.;
1:7 & IMC iseiNEK
35C !¥:«£?.
4~n TMPIKSS
PSOEE si;K
=a^ ae-jfi; ««©!•= el ?«!?¦-££
f>el!i*. oaj3_j^-r
fir* If* or/3 117:1^= a 03/^0/3 _«*:¦
fl.^S / ->^JL
^ i irc> °t / ^ mi"^, 7.3.5 ^>-~-JL
- ,-.9.1
HST-iCU 5 IRAi" £-DuC7
FfSE r^H ECff/fcg*
FILTErT
l£7 i >e !M?I."f;2;
3H> IMPiNS
47H I!«?InES
iOVbrt&t*
ISTr-QI- ; TRfilN FTfiK
rE2E IjfiB'H 2C1 X/fod93-(e
riL7£S
12" i(?:SS5
1HI' iSFiKE?.
3P5 i,¥:n»=
t
rSIlJ^Y /S5£~>rJ
H5I3 ZZOlt
fZli^
lysiiMao,
* /*?
~f£F
j^iL
tyS/CrOQaCt. r51<
j/» 5 0^09g(o
??t "Is 5
Ui hU s rWbMab
J5I!
~JS12
J15I3
V?k
-------
\,ZZZ.«~'"Z'S u!*!-|52V
TSiT (_p P<5 e d. f^v'i •£ & 3— Jz^./vyj/e- nTa~S/^hbc^7c^\_
DAT& §., s
Tri>Ci f5TSLt !H SOT^V sIlM WC3EWTI0I sITH IONIZING r'ET 5CR-J55ES
SV1P.S TrFi =*?«£ 1.3. CErIE «m VffiH i£3 <14 ft) Shl5FAI7H iHz 1> £=S '40 .« VGA)
C^.V/S3«iC FEE3 FOg f 0 lOQO RV3(i- r&<5 )6 ) OOO/'QR >OI &Q£> ;/F Q9 loiooo/ FQg/fi /Oafl
?0 S I 0 IQ I ft fry&ULFOqiO 1 O'l 0 'JD% 10 ) QI"D ~Fp^ 10 10 IV>f F .11, n^JIbil' c
F r r F ?
hK££KJ5 ,m£7hL SK F C3 I 5ja«tfcl0 X ^
KILN A3 iariiil '
bOG 1.5 A/nS *~7 O**S 1 f.177 o.. Q
1ST s :«¦ iJirlNSsr. *1711*' Sss^±J2^axX ^sis&q^i Hi-::
*0 31s:ss :^3l5Q<3 !5~/0<* fill ^ fac-|fftOnit >4 «!1
1F£ £A^l5'C>l+ r-513q yrnJ
nFTrffl 5 TTttIK ET'riCK
FSuBE SfiEH -09.15ld3*7 .ȣ=*
";'-TcS gQ^I5>Q^7 fl?. :
1ST Tr?iXtz?, igiJs sC>$i5 / b 3 "7 fEll
33 IH.-i.NS3 3?ii /K/r SnfrJS yo 3"7 H5i2
3RD ifPINiS jy S/ 0 V KSI3
125
-------
TEST SiJflBsr: 1 Fee i NWv a2 -rCc^/^-v-
MT£.
T?iC£ SZ1PLB !« ROTARY OLS iNCINEfcTICN MTH IOUZINS SET 33»ES>
3Aftf.£ TYri
CLAY/DPEfirii: F££D
:ftfi?L£ i.D.
rfiSd loSOO
rOqo^Q^O^
CDNfilE (40S. VOfi) l€3 CM HU SSLSShITH '125 H.) EPS '.40 ,t I'M)
-rfefcq p^oo i/f og,ogoftnoi/ rQ^M&^o/,- Cftoq D^OO
rn SCR 03Q.S /F050 q ase> q ? n n gft q/ fo3C5L£M5
F r F F
(QUEERS 1E7hL =K rzKO'liZAb!C M-gfA
.:Ofe^)J[^ / ;c ftuJa^ ^
KILN S2i
7 QS'J^ ^30 23 M
Til£OSJIjk&-i0 *- l/]A Cor^-,
KILN i=H TEL? t 0 % 05 \ 3 S O TOP
SEr.-JSrE^ a?i»I€«i 5 0? 01 Oil ft »/
eOSo
sovoii/a? ~:
pSQ.7J.A-x5 /
-£jLQ_9_L3L>SL_5_
3flgO*?MA54(. M yuh (C-3WIS?
i.W.
."STHOl !" T?.»!H
THiHri.: iFE^TE-!.'
1ST a 2ND 1M-INSER
~rC SP!tS3
4th iff issa
PROSE Wh£-
0*0^03 5 m"
OftO*) K)3. S H17Ilt/
o^oq ica ^ »i7i^
*f ~C*u ./
!i• / . r ^
SAMPii AfiG'JHT
sHAS^'i HCl SSf'.=LE:
mLSibSe^i
gtQ«v^\^
p% 5 ftvIS
t&1 *T> kit;i
S r=T"HC5 3 TRAIN =-I;X7 ,
PK2BE 'a'£H t OftM >0^.3 gj
FILTER ;o8&q >o*S jsF",
r~ ^ 1ST 4 2® Iff IfitER £0 86^10*5 tglX.
I 3kD Ifp'lNSS £DgC;qioaS H5I3 / .
v 4TH LtFINGER. i D^O°> )03>5 ?514
^ClOO T*-P -N'ltr ^o%C:^ lO'i.'i I**12.
rST-iDD 5 TRAIN ET.flCK
=rtiE£ WAS = Qgp^ \0^>D H5.SW
FILTES £Q'g5gUo'5b HaF
1ST IKriE-Efl
2J® ISPINcEr
3RD MP] SEER
5 55 ute.
3ot>irsi r
T6P"*S
3tt /n/S
E fi^cfl/oas nail (. 100 v^\ s )
"£0^ffl\0?>b *Sil
5 f5I2 t»%\S
S \ fc-SO ISI3 5C
\
126
-------
Ds^TH: <£ _ 11 - *2 ^
HACE *E7P1E IN SO-ASY <:!LN !«C!!€RATIGI "ITH 10rillim -*! KRiSEE?.
3™irLE TyfE sSirLS i.5. CSffifE <40KL VQS> S3 i!- ,*fc) SajSiTH U3 .1) H?A ;*<> ft. VQAi
a^/csstfi.: ™s --o<^oq og£t- *«3»a r os?a*>csos^q^/f/i9ng.^
JSTfti. =K F og II 11 ^4l 0 KL
re? ;> i) 20 n
Kllri A EH "15
/
r&iMJ&CE --
Tn,S f' la'r^' 1 v'jA
" f^)/ 1 ?>3 o TC--
S"r-5rH= 2t£«DCi»i 5C? 11 O ^.5 5? i/
?g f '.¦ r- .r? --i ¦•'
jg>t//»i^3 e> ^
rof// H3Q
-CJ^ It '3-3
17
40 vOA
SHAXt:'r 'CI ;sHF:£E
.".ETHJl- :? TH.«;S Sffts Ari>\'?iT
7K:rrLI iF:LTL:;.; ».0$<'0 3 30 .1177
s£t % 2® itfifSi?. Hng11 6 ttTinfos*. t ffoi^/^vuL ;o^)ios3Q *;?!-
*=:se?. r.i7:y «^/-q ^ P
JTK Tr?!f.s=r: afl«S;>flg.3& tiiTl^ TS!0 -v^JL.
PROH vtfEK AO$,, ^ S?^f. -¦;~;^
iSXiS ; TFAIR s-iS!
,-r£E£ 'JiSsH EOO llnff 3
FILTH S^-s: nov ? a-
l£7 t 2® ItFIKE?
TSD iif-IMl?
4Tr IfPlNSSS
s*/
^:/
ho
-------
-iwy, u s-' w » ^J\\
0,,
ACliPiX
¦==7 Ma-i==: °1 FecC N\ln 43
3kTes
TRACE f*E7?iE !.N ROTARY KILN ^INcRfiTIOtt 4ITH IGliZINS i£T SCF.U53K
a-.lPL: 7YP£ SW'JI l.j.
CLAY/C^£H>iIC "EES fQ*7X5 jbXO
rCT3(ftib2.3
'-usais * «•?!*. yukj *fcs <1* nL> . bKJ»»i ,rt ills .T) tr3 {«.* rs. vuA)
•0^735(^204073,»>/b30X F^225ib2oz F07JJ?ibao
«cf?ag;/fa23^o7amc23 XgQT3 5[*a3 / fS^smSZ
.~:hl ;K
• Cr7^Si705 iq ?i
:fa7j.^nob so a.
ILN r::H
-»r 1 ia- rcrv » l l: ri L' \
roll?:-"s. ^
TftlJ'ilbaR 40 *. viA
• 0*7 $ \ V?"^ ^ ' '-*-?
sO'7aS\Qt>2 ^
r-n^'jl-a tl>a^
5 0*7 23 i*U* ~
5Q"7ayg3\^
r™3jMZ<
= 0733 1-735—y
;C71il35_D_/
T072S^H-Q 25fAL Oles) ^
Ttm? IfcH-o Homl VOft CCckv^'.O
T^lb^O ~\C-L?
r CH 3 % lb5 j 40 ft W (lCNS-IE;
."nHOS TRAIfs sAK?L£ AH5Ji? SHftriOM*5 .-SL BAfiFLEE
7HIHELE A Cf72 *31:3 5 *-¥ S17i 0
1ST k -M wines "02713U3* M7U/ &D5wls *cnxwbH- i»,i?i: CVaomts)
3RE IIP'SEP rii~;5 ~ b7bm»-S
4^ TtPlr'SR Hi714 ^ R
FSCBE nigH ACli5jMi
'~Z)iS c
nETHGE- 3 TRflIK E-DUC7
?SCS SSSH E ^ *—
FILTEF: EOlasaSH !€? ^ — =•
1ST t 3(3 JKFIrSiS £Q>7 3 ?? 1^3% ,-g;-jiS t i 87 >nLc E rts:i (_\00 r*Ls)
7RD lifiHSSt • f?7 3 g ) 3^*f- \~5<3 N\i-t
4TH :f!»2 E CH 3 fe ^"SM- rtSI4^ rtL*
METHOD : TRAIN ETftCK
.-as WASH
FILTER
1ST WrlfisES
Ir?:S£EH
3RD Iff INKS
S &? a & >g
-/jp
//£ -/j
Js
H5H
s 0)^73
3 073^', Hao f5;2
SOU^IHOC K5I-
128
-------
Appendix C-2
Metal Analysis Data
129
-------
Results of Metals Analyses - IKS Trace Metals Burns
Saaple I0 1
Arsenic
Sarlua
Blsauth
Cadalua
Chroalua
Capper
Nagneslua
Lead
Strontlua
Clav/Oroartlc Llould Feed (aa/k«)
?
F0725I620
< 4.15
22.4
< 6.50
1.2
36.4
26.6
18,100
1.65
30.6
9
F0T251523
< 4.IS
24.9
< 6.50
1.14
37.7
27.3
18,900
1.65
30.6
i
F07311305
< 4.15
20.8
< 6.50
1.63
35.1
27.6
18.400
1.65
30.7
1
F07311315
< 4.15
23.3
< 6.50
1.13
35.1
25.6
18,600
1.65
30.7
y
F08011215
< 4.15
26.2
< 6.50
1.25
44.0
27.2
22,800
1.65
38.3
2.
F08011220
< 4.15
26.8
< 6.50
1.06
38.3
26.3
19,200
1.65
31.7
X
F88021030
< 4.15
24.6
< 6.50
1.13
38.3
25.3
18,900
1.E5
31.3
3
F0802I040
< 4.15
23.1
< 6.50
1.17
36.8
24.9
18,400
1.65
31.4
3
F08021045
< 4.15
23.8
< 6.50
1.26
31.7
27.0
19,700
1.65
32.4
2.
F08021105
< 4.15
23.9
< 6.50
1.99
37.0
25.6
18,300
1.65
31.6
Aaueous Netals Spike Solution (bq/L)
7
F07281705
1,600
12.500
11,900
318
N.R.I
12,200
N.R.
1,450
12,900
¥
F08D11338
1,480
11,800
11,000
292
N.R.
11,400
N.R.
1,350
12,200
2.
F0802T325
1,520
12,800
11,800
315
N.R.
12,208
N.R.
1,460
13,100
3
F08041245
1,520
13,000
11,980
324
N.R.
12,300
N.R.
1,478
13,300
7
F080912I1
S483
12,700
8920
301
N.R.
12,200
N.R.
1,440
13,100
?
F08111134
1,070
1,800
8,450
217
N.R.
0,670
N.R.
1,31D
9,170
1
F08151 345
1,620
12,900
12,000
322
N.R.
12,500
N.R.
1,470
13,300
6
F08151346
1,800
13,080
12,000
321
N.R.
12,500
N.R.
1,470
13,400
s'
F08161302
1,588
12,700
11,600
313
N.R.
12,208
N.R.
1,450
13,100
/
F88I7I301
1,290
10,400
9,390
255
N.R.
9,990
N.R.
1,188
10,700
Target Cones
1,590
12,700
12,700
311
93.2
12,700
N.R.
1,590
12,700
1 Recovery2
88.5
96.0
90.0
95.9
93.2
94.2
96.9
89.0
16.9
2 - Analysis not required (R.R.).
* - Recovery (I) based on a 5.00 ag/L spike addition to a 1:1 dilution of staple £21251623.
3 - eu ou'Mit*— • us a J IK ceJtfJ+jhr*a,
Saaple concentrations not corrected for recovery.
-------
Results of Metals Analyses
IMS Trace Metals Burns
Clay/Organic Lfquld Feed fo/kg)
S~^
5aaple 10 t
Arsenic
Barfue
aisnjth
Cedalua
Chroalue
Copper Magnesiua
Lead
Strontlue
'7
F08090800
4.65
21.8
< 3
85
1.31
42.9
25.8
19495
4.24
31.5
7
FC8090805
< 3.50
23.0
< 3
85
1.SS
40.3
25.3
1868T
3.59
30.4
9
F08IH805
< 3.50
21.3
< 3
IS
1.43
43.4
25.2
19541
3.52
31.8
%
5.40
25.2
< 3
85
1.57
40.9
25.1
18333
3.08
32.7
t,
F081010Q0
< 3.60
21.1
< 3
85
1.23
42.4
24.6
1940S
< 2.75
30.0
c
F08WCIO
3.60
20.8
< 3
85
1.29
35.5
23.2
17463
< 2.75
32.1
r
FD8150830
7.02
24.7
< 3
85
1.51
40.2
23.2
18683
2.SB
31.5
r
F08160750
5.80
21.4
< 3
85
1.40
44.0
23.4
18200
< 2.75
32.0
r
F0816080Q
< 3.SO
22.0
< 3
85
1.37
40.4
23.9
17512
4.18
30.8
/
F08161C50
5.57
21.4
< 3
85
1.24
52.2
27.5
19254
2.89
32.5
/
FC8161055
< 4.40
20.7
< 6
00
1.34
45.5
22.3
19356
4.31
29.7
j
F08161100
< 4.40
22.0
< 6
00
1.49
37.8
21.4
17822
4.41
29.0
Q09171700BSK3
< 4.40
21.B
< 6.00
1.25
88.0
15.2
39250
4.70
32.4
1309171701HSKD3
< 4.40
20.0
< 6.00
1.39
82.1
15.1
36965
4.63
31.5
ft
\ Recovery
99.4
>00
100
101
103
98.8
99.5
100
104
, - Analysts not required (N.R.).
2 - Recovery (4) based on a 5.00 m/L spike eddltlon to a 1:4 dilution of sbbdIb's T0B1T230TCLP ami
A0SD11I03M17-PW.
3 - Matrix spike contains Kg and Cr at a concentration of 20,000 cg/L, and 55.7 ng/L, respectively.
Sasple concentration not corrected for recovery.
131
-------
Results of Metals Analyses - IKS Trace Metals Burns
Kiln Ash Samples (mg/kg)
Sacple ID * Arsenic Bariun Bisnuth Cadaiun Chroaiua Copper HBflnesitn Lead Strontiun
1
T072E1639
55.2
296
123
2.27
109
407
32,900
82.3
312
7
T07261640
59.3
344
156
3.02
164
381
32.600
89.4
359
i
TDBOI',400
21.4
79.9
30.7
0.653
100
109
30,100
56.8
75.9
X
T03031330
54.2
207
207
3.66
109
306
31,600
76.1
214
X
70803T335
33.1
255
236
6.54
73.2
217
28,700
62.9
261
3
T0804H30
39.2
114
25.8
< 0.509
69.0
240
22.900
45.2
120
7
700091330
39.3
113
108
1.76
91.7
222
2S,200
51.5
123
9
TD8I11230
33.1
109
106
2.04
92.2
187
26,900
51.5
113
6
I0C151O0
3! .5
99.0
106
2.39
80.6
199
27,100
52.7
106
<
TO61E13O0
;C.O
112
53.5
1.14
86.1
207
27,200
50.0
125
/
TO0111400
34.5
95.5
63.2
< 0.390
46.8
253
17,400
24.2
134
t Recovery'"
98.5
9?.S
95.2
93.9
in
ICS
in
102
1 - Analysis not required (N.R.)
* - Recovery (t) based on a 5.00 m/L spike addition to a 1:4 dilution of saaple's TD72B1640
and T080S1330.
Saeple concentrations not corrected for recovery
132
-------
Results of Hetals Analyses - IKS Trace Hetals Burns
Afterburner Exit Flue Gas
Saopled with Method 17 partfcle trains
Saaple ID t
Arsenic BjHub 81south Cadalun ChroofuB Copper Hagneslua Lead Strontlua
Iaainaar Contents Ow/Ll
SA07281234W17-
A07281234N17-
yA07281234*17-
' ^08011103X17-
~*080111031(17-
. ~HOM11103H17-
^ A08020950M17-
. A08C20S50M17-
^j/AOB020950M17-
/'/A08041037M17-
> ^08041037X17-
(/iW804l037H17-
/•/A0B091D25H17-
-------
Results of Metals Analyses - IKS Trace Metals Burns
Afterburner Exit Flue 6as
Sanpled with Method 17 Particle Assessment Sanpling Trains
Sample ID
Arsenic Barlun Bisouth Cadnius Chromiun Copper Nagnesfu# Lead Strontium
Iapinqer Contents (fig/D
S A08110830H17-
-------
Results of Metals Analyses - IHS Trace Metals Burns
Afterburner Exit Hue Gas
Sampled with Method 17 particle trains
Sasple 10 t Arsenic Bar'un Bisiwth Cadaiun ChroB-'un Copper Hagnesiu» Lead Strontiui
Proba Washes (ac/tra1n)
-ri
~"A07281234H17-PW
0.168
0.0473
0.95S
0.474
2.42
3.48
3.68
0.41
5.057)
-r V
~%ff8fl711C3M17-PH
0.184
0.C 294
1.53
0.456
4.55
2.15
1.80
0.133
0.5336
1* X
~M802Q»E0Hn-PH
0.295
0.342
0.781
0.364
0.902
2.51
2.37
0.219
0.456
VA@BM1037N17-Pt<
0.435
0.373
3.01
0.620
0.673
2.53
3.35
0.312
0.52!
-r~7
~JW8891025K17-PN
0.0391
0.0399
0.169
0.142
0.425
0.744
C.790
0.0243
0.0572
/i0811C830H17-W
o.tst
0.181
1.60
0.416
10.8
1.96
4.83
0.195
0.266
TC
~tf08150957H17-PW
5.95)
0.984
7.01
1.95
16.8
7.17
tS!
1.66
1.35
TiT
~i0816ll913*17-PH
0.252
0.C59S
3.30
0.735
10.8
2.95
2.68
0.373
0.C680
Tl
l/«08t7D9E6H17-PH
0.761
8.115
rswi
US
14.J
3.14
6.94
0.547
0.182
i Recovery 2
99.9
101
93
102
106
99.5
103
101
103
1 - Analyses not required
2 - Recovery [\) based on
Sjuple concentrations not
(NX)
a 5.00 its
carrecte<
i/L spike addition to a 1:1 dilution of sanple A080111D3M.17-P*
I for recovery.
135
-------
Results of Hetals Analyses
IKS Traee Hetals Burns
Afterburner Exit Flue 6as
Stapled Kith Method 17 Particle Trains
Saeple ID t
Arsenic
Sariu#
Bisauth
Cadalua
ChroaluB
Copper
Nagneslua
Lead
Strontiua
Particulate Fraction (sg/kq)
A07281234N17
2 UB
26.1
30.5
30.1
54.2
160
728
1391
91.8
40.4
2 - 4 ui
209
40.4
253
436
1035
3008
2441
536
41.9
4 - It un
275
71.2
219
472
638
3118
4444
539
92.B
10 - 30 ua
165
67.0
118
311
643
22BS
3566
383
91.9
30 us
EB.6
28.9
75.4
107
293
104B
1774
150
38.2
A08C11103K17
2 un
< 11.6
22.1
< 19.9
4.38
33.1
1B7
414
9.95
36.6
2 - 4 ua
24.4
35.4
30. S
26.6
83.8
394
B45
37.1
37.8
4 - 10 un
242
73.4
90.7
53.3
249
984
3965
57.0
91.6
10 - 30 ut
132
84.0
82.6
37.4
180
835
3964
38.8
104
30 us
24.S
11.2
< 10.7
4.19
1U
267
332
13.0
16.2
i Recovery
S5.S
99.3
95.4
97.2
97.3
9S.2
91.9
99.8
100
J - Analysis not required (N.R.).
* - Recovery [\) based on I 5.00 aw/L spike addition to a 1:4 dilution of saaole's A0T2G1234R17—F1I and
E1005D922H5-I4.
Sacple concentration not corrected for recovery.
136
-------
Results of Ratals Analyses
IHS Trace Metals Burns
Afterburner Exit Flue Gas
Saapled with Method 17 Particle Trains
Saapla 10 1
Arsenic
Barlua
Blsauth
Cadalua
Chroalua
Copper
Hagnesiua
Load
Strontlua
Particulate Fraction faq/kq)
A08020950R17
*
2 UB
< 16.3
37.9
< 28.1
6.18
36.3
166
354
< 9.56
35.3
2 - 4 ua
62.4
37.1
84.9
114
333
824
990
73.0
41.6
4 - 10 ua
92.5
35.9
71.7
168
339
1004
111G
91.8
38.5
10 - 30 ua
156
73.S
195
107
215
636
2454
157
72.3
30 ua
19.5
1B.6
19.5
17.1
543
440
692
35.6
26.0
A08041Q37N17
2 us
8.51
20.7
14.9
9.92
56.5
290
337
18.7
23.1
2 - 4 ua
294
49.9
138
139
318
1432
1997
153
75.2
* - 10 ua
366
62.3
165
172
431
1823
2972
166
89.4
10 - 30 ua
53.1
58.1
63.1
26.9
242
622
1037
45.0
76.2
30 ub
15.4
10.2
21.0
9.2B
198
216
229
21.1
14.7
% Recovery
95.8
99.0
95.4
97.2
97.3
96.2
98.9
99.8
100
1 - Analysis not required (N.R.).
2 - Recovery (%) based on a 5.00 bo/1 solke addition to a 1:1 dilution of sbbdIb's A072B1234H17-F14 and
E10C50922MS-I4.
5aaple concentrations not corrected for recovery.
137
-------
Results of Metals Analyses
IMS Trace Mstils Burns
Afterburner Exit Flue Gas
Saaplad with Method IT Particle Trains
Sanple ID 1
Arsenic
8ar1ui
Blsat/th
Cadaiua
Chroalua
Copper
Hagneslua
Lead
Strontlun
Particulate Fraction foc/ko)
A08D91025K17
2 ua
< 9.95
21.1
< 17.1
9.60
54.4
182
321
1D.8
30.1
-T7
2 - 1 ua
309
75.9
233
420
522
2262
2636
248
104
4 - 10 un
154
84.2
302
683
472
2768
4B25
30B
102
10 - 3d ua
122
69.5
346
208
596
1586
2928
124
130
3D ua
84.3
36.1
398
131
857
1062
1256
142
49.0
AOB110G3GN17
2 ua
< 15.5
18.2
< 23.3
9.31
118
263
249
21.2
21.2
T8
2 - 4 ua
338
71.3
213
819
724
3507
2347
760
100
4 - tO us
55$
75.3
416
15S8
1168
5125
4442
864
97.4
-
10 - 30 ua
182
111
958
370
3(95
2781
3831
332
155
30 un
27.1
33.2
3564
16S
Eat
1232
1435
271
44.7
t Recovery
96.3
98.8
96.4
97.9
100
86.4
99.2
99.6
100
' - Analysis not required (N.R.).
2 - Recovery l\) based on a 5.SO h/L strike addition to a 1:1 dilution of ssnole's E10050922H5-I4.
A0B110830N17-F4, and A0728T23JRTFF14.
Saiple concentrations not corrected for recovery. '
138
-------
72
-rr
Results of totals Analyses
[MS Trace Ratals Burns
Afterburner Exit Flue 6as
Stapled vith Hethod 17 Particle Trains
Staple 10 t
Arsenlo
Barlue
Blsauth
Ccdalua
Chroalua
Capper
tajneslue
Lead
Strontiua
Particulate Fraction fea/Vol
A08150857M17
2 ua
< 11.0
12.8
16.4
9.19
55.3
152
360
17.1
21.0
2 - 4 ua
283
85.S
297
214
257
1779
3980
278
89.6
4 - ID ua
565
104
484
397
358
2858
8877
432
122
10 - 34 ua
120
• 95.7
152
79.1
324
965
3860
81.1
124
3D ua
30.5
40.9
300
44.1
784
530
1202
76.0
5S.8
A08160913N17
2 ua
< 11.7
18.7
< 17.5
1.92
15.4
140
210
7.35
20.8
2 - 4 ua
88.6
38.5
46.4
13.0
57.0
422
845
23.0
35.2
4 - 10 u»
301
32.3
189
48.2
211
1088
2E99
67.8
37.9
10 - 30 ua
143
78.0
< 114
29.5
23?
1132
240?
197
102
3D ua
17.7
7.43
58.6
211
202
263
195
22.3
11.5
\ Recovery
98.0
98.1
96.9
98.9
102
95.8
99.7
100
100
J - Analysis not required (N.R.).
1 - Recovery (I) based on a 5.00 bo/L srfke addition to a 1:1 dilution of sanDle's A072B1234H17-F14 and
A03110830NI7-fl.
Sanple concentrations not corrected for recovery.
139
-------
Results of totals Analyses
IKS Tract Netals Burns
Afterburner Exit Flue 6as
Saipled vfth Method 17 Particle Trains
Saiple ID t
Arsenic
Barlun
Bfsnuth
Cadalua
Chroalua
Capper
Magneslui
Lead
Stronttui
Particulate Fraction (»g/kq)
A08170956H17
2 UD
< 13. D
19.8
156
8.75
101
125
231
15.2
21.8
2 - 4 ua
121
63.7
4253
150
412
731
1688
106
92.7
4 - ID ua
291
55.4
9005
382
955
1108
3439
219
76.2
10 - 30 ui
1(4
66.2
4863
361
2230
1354
3728
255
85.3
30 ua
43.3
25.D
2557
154
cm
765
1268
139
30.8
t Recovery
98.0
98.7
96.9
98.9
102
S5.8
99.7
100
100
' - Analysis not required (N.R.).
2 - Recovery (t) based on a 5.00 nq/L spike addition to a 1:4 dilution of sample's A07281234K17-F14 and
A08110830M17-F4.
Sample concentrations not corrected for recovery.
140
-------
Results of Metals Analyses
IMS Trace Rati It Bums
& Afterburner CxitPut Oar
m Saaplad with NrnJinJ 17 Pamela T>aira ¦
Saaple 10 1
Arsenic
Barlua
Bisauth
Cadnlua
Chroalua
Copper
Magnesfua
Lead
Strontlui
UnHred Clav (M/kfl)
K08211100
2 ua
< 27.1
<5.7
190
15.8
119
397
17541
40.4
72.1
2 - 4 ua
< 16.3
32.0
91.6
8.04
85.1
255
17206
26.7
53.1
4 - 10 ub
< 18.5
41.3
91.4
10.8
103
327
25051
31.2
70.5
10 - 30 ui
< 7.66
24.S
22.9
4.22
69.4
220
18768
< 5.33
44.6
30 ua
< 2.30
15.3
5.71
1.17
39.4
50.4
7078
5.48
21.5
Unffred Clav (rca/throttle)
N08211100
2 UK
< 0.00770
0.0130
D.0540
0.00450
0.0339
0.113
4.99
0.0115
0.0205
2 - 4 ua
< 0.00770
0.0151
0.0433
0.00380
0.0402
0.121
8.13
0.0126
0.0251
4 - 10 ua
< D.00770
0.0168
0.0372
0.00440
0.0418
D.133
10.2
0.0127
0.0287
10 - 30 ua
< 0.00690
0.0223
0.0206
0.00380
0.0625
0.198
16.9 < 0.00480
0.0402
30 ua
< 0.00630
0.045S
0.0171
0.00350
0.118
0.151
21.2
0.0164
0.0645
! Recovery
96.9
98.9
98.3
98.8
102
97.8
92.4
99.0
102
' - Analysis not required (N.R.).
2 - Recovery (*1 based on a S.DD aa/l selke addition to a 1t4 dilution of sanole's A08110B30K17-F4 and
N08211100F1S.
Sanple concentrations not corrected for recovery.
141
-------
Results of Metals Analyses
INS Trace Metals Bums
Afterburner Exit Flue Gas
Sanpled with Method 17 Particle Trains
Staple 10 S
Arsenic
Eariua Bisauth
Cadslua
Chrofllua
Copper
Nagnsslun
Lead
Strontlua
Particulate Fraction (aq/tSrottlel
A0726123«N17
¦7^1JhJ
< 2 ua
5.00163
0.0(191 0.00180
0.00339
0.0100
0.M55
0.0879
0.00574
0.00253
2 - 4 ua
0.0214
0.00114 0.0259
0.0447
0.106
D .308
0.250
0.0549
0.00(29
4 - 10 ua
0.01 DO
1.0101 0.0550
0.120
0.213
0.793
1.13
0.137
0.0236
10 - 30 ua
0.0366
0.0135 0.0234
0.0619
0.I2B
0.155
0.710
a.0762
0.0186
> 30 ua
0.0373
0.0190 0.0497
O.ITOB
0.193
0.691
1.17
0.09B5
0.0252
A080T1103M17
< 2 IB <
0.00053
0.00111 < 0.0010
0.0D022
0.00166
0.00941
0.0208
0. [10050
0.00184
J - < ua
0.00201
O.0D29I 0.00251
0.00220
O.OOS89
0.0324
0.0S95
0.00305
0.00311
4 - 10 ua
0.0532
D.0I61 0.0199
0.0117
0.0546
0.216
M7D
0.0125
0.0201
10 - 30 ua
0.02BT
0.D1B2 0.0179
O.OOB1
0.0391
0.1SI
1.159
O.OOS4
0.0225
> 3D ua
0.0232
D.D104 c t.ODID
0.00 39
0.106
0.248
1.309
0.0121
0.0151
1 Recovery
95.S
89 95.4
97.2
97.3
96.2
98.9
19.8
100
1 - Analysis not required (NJ.)
2 ^ Recovery ft) based an a 5.00 m/L spike addition to a 1:4 dilution of staple's A072B1234M17F14 and
E10050922H5-I4.
Saople concentrations not corrected for recovery.
142
-------
Results of Metals Analyses
IKS Trace Metals Burns
Afterburner Exit Flue Gas
Saapled with Method 17 Particle Trains
Staple ID t Arsenic Barilla Bissuth Cadniua Chroalua Copper Magneslua Lead Strontlua
Particulate Fraction (eg/throttle)
*08020950*17 ^
< 2 ua < 0.00059 0.00135 < C.8010 0.00022 0.00129 0.00651 0.0126 < 0.00034 0.D0129
2 - 4 ua 0.00318 0.00163 8.00433 0.00501 0.0170 0.0420 8.0505 C.00372 0.00212
4 - 10 us 0.00654 0.00254 0.00507 0.0119 0.0240 0.0710 0.0709 0.00649 0.00272
10 - 30 ua 0.0177 - 0.00021 0.0218 0.0312 0.0S68 0.190 0.274 0.0175 0.00807
> 30 ua 0.0105 0.0101 0.0106 0.0093 0.295 0.239 0.376 0.0199 0.0141
A08041037W17
< 2 ua 0.000611 0.00146 0.00105 0.00070 0.00393 0.0205 0.0238 0.00132 0.00163
2 - 4 ua 0.0517 0.0091 (.0252 0.0254' 0.0579 0.261 0.364 0.0279 0.0137
4 - 10 ua 0.0634 0.0108 0.02BE 0.0299 0.0747 0.316 0.515 0.0287 0.0155
10 - 30 ua 0.0085 0.0093 0.0101 0.0043 0.0387 0.0995 0.1S6 1.0072 0.0122
> 30 un 0.0154 0.0102 0.0211 0.0093 8.199 0.216 0.230 0.0212 0.0147
* Recovery 95.8 99.0 95.4 S7.2 97.3 96.2 98.9 99.8 100
I - Analysis not required (N.R.).
Recovery (A) based on a 5.00
EIO05C922J&-I4.
Saaple concentrations not corrected for recovery.
' - Recovery ill besetl on a 5.00 aq/L spike addition to a 1:4 dilution of sample's A07281234M17FW and
EIO05C922J&-I4.
143
-------
Results of totals Analyses
INS Trees Hetali Burns
Afterburner Exit Flu® Gas
Stapled with Method 17 Particle Trains
Saaple ID t Arsenic Bariui Bisauth Cadaius Chroaiua Copper Plajnesiua Lead Strontiua
Particulate Fraction fag/throttle)
A0899102SN1T Tejf y
< 2 ua <
0.00058
0.00123 <
B.0010
0.00055
1.00317
0.0106
0.9187
0.00063
0.00177
2 - 4 ua
0.0435
0.0117
0.032)
0.0593
0.0737
0.319
0.372
0.0350
0.0147
4 - 10 ua
e. 129
0.0239
1.0058
0.194
0.134
0.785
1.37
0.0876
0.0290
10 - 30 ua
0.0149
0.0110
0.0(25
0.0255
0.0733
0.195
1.360
0.0152
(.0160
> 30 ua
0.0457
0.01S5
0.215
D.0709
0.455
0.575
0.681
0.0173
0.0256
A09110330N17
tiS.
&
< 2 ua <
O.OOOC7
0.00078
<0.0010
0.00040
0.00505
0.0113
0.D107
0.00091
0.00091
2 - 4 ua
0.0333
0.0082
0.0325
0.09(2
0.0833
0.41S
0.270
0.0874
0.0115
4 - 10 ua
0.121
0.0153
0.0900
9.345
0.253
1.11
0.962
0.187
0.0211
10 - 30 ua
0.0194.
0.0118
0.102
8.0394
0.372
0.296
0.408
0.0353
0.C165
> 30 ua
0.0145
0.0179 1
toil
F 8.0912
m
0.654
0.773
0.146
0.0241
X Recovery
96.3
99.8
36.4
97.9
100
96.4
99.2
99.6
100
] - Analysis not retired (N.R.).
* - Recovery ft) based on a 5.00 aa/l soike addition to a 1:1 dilution of sasole's AOB110830H17F4.
£10050922X5-14, end A072812J
Saaple concentration not corrected for recovery.
144
-------
Results of Metals Analyses
IKS Trace Hetals Burns
Afterburner Exit Flue Gas
Saipled with Method 17 Particle Trains
Sample ID 1
Arsenic
Ssrlua
Bisauth
Cadaloa
Chroalua
Capper
Magnesiua
Lead
Strontlia
Particulate Fraction (eq/throttle)
A08150957K17
< 2 ua <
0.00067
0.0C097
0.0011S
0.00056
0.00337
0.00929
0.0219
0.D0104
0.00128
2 - 4 ua
0.0442
(.1103
0.0464
0.0334
0.0402
0.278
0.522
0.0(35
0.0140
4 - 10 ua
0.119
0.0218
0.102
0.0836
0.0754
0.602
1.87
0.0911
0.0258
10 - 30 ua
0.01B6
0.0155
0.0236
0.0123
0.0504
0.150
0.600
0.0126
0.0192
> 30 ua
0.0191
0.0256
0.188
0.0276
0.491
0.332
S.7S3
1.0476
0.0351
AO8160913N17
/¦a-shS.
< 2 u# <
0.DC0E7
0.0C1C7
< 0.0010
0.00011
0.00094
0.Q0B03
0.0120
0.000(2
0.00119
2 - < u*
0.00337
0.00150
0.00228
0.00064
O.0C280
0.0207
0.0115
0.00113
0.00173
4 - 10 ua
0.002B2
0.003C3
0.0177
0.00452
0.0198
0.102
0.253
0.00536
0.00355
10 - 30 ua
0.0150
0.0062
< 0.0120
0.0031
0.C249
0.119
0.253
< 0.0048
0.0108
> 30 un
0.0164
0.0069
0.0544
0.0071
0.188
0.241
0.181
0.O2O7
0.0107
% Recovery
SB .0
98.7
9E.S
98.9
102
95.8
99.7
100
109
] - Analysis not required (N.R.).
1 - Rs:overv ft) based on a 5.00 naA selke addition to a 1:4 dilution of sassle't AD7J81234M17F1I and
A0B110830N17F4.
Sample concentrations not corrected for recovery.
145
-------
fasults of Hetals Aralysas
IMS Trace fetal s Burns
Afterburner Exit Flue Gat
Saapled alth Method 17 Particle Twins
Saaplo ID t Arsenic Birltn 81sauth Cadalua Chrorlui Copper Magneslua LNd Strontfua
Particulate Fraction fag/throttle)
A0917DS56MI7
< 2 in
< B.03067
0.00102
0.00800
0.09045
0.00521
0.00644
0.0119
0.00078
0.00112
2 - 1 ui
8.0145
0.0017
0.514
0.0181
0.0498
0.0883
0.201
0.0128
0.0112
4 - 10 im
0.0581
0.0112
1.82
0.0773
0.193
0.224
0.695
0.0443
0.0154
10 - 30 ua
0.0492
0.0117
1.30
0.0)65
0.596
0.362
0.99S
0.0582
0.0228
> 30 ui
0.0550
0.0317
3.25
0.196
IS1
0.972
1.61
0.177
0.0391
t Recovery
98.9
98.7
9S.5
98.9
1D2
95.8
99.7
109
100
1 - Analysit not required (N.R.).
* - Recovery (*) based on a 5.00 nq/L spike addition to a 1:4 dilution of senate's A072S1234M17FM and
A06110930M17FI.
Saaple concentrations not corrected for recovery.
146
-------
Results of Metals Analyses - IWS Trace Netals Burns
Scrubber Er.it Flue Gas Sampled with Method 5 Multiple Hetuls Trains
7^
Sample ID I Arsenic Bariiw Biinuth Csdntuir Chromlu# Copper Magnesium Lead Strontium
Probe Washes (ma/train)
<7
E07201234K5PW < 0.0068
0.C003
0.116
0.0105
< 0.0065
0.102
0.0907
0.0231
0.0096
E08110B32HS»/r0. 0324
0.0099
4.13
0.242
0.0453
1.17
0.217
0.307
0.G2
-------
Results of Metals Analyses - IKS Trace Metals Burns
Scrubber Exit. Flue Gas Sasplerf with Method 5 Multiple Metals Trains
Sanple ID 8
Arsenic
Barfiw
Bisn/th
Cadaiua Chrosiua
Copper
Magnesiuo
Lead
Strontiun
1
E872B1234M5I112
0.075
0.042
—
0.009
*/
E0B011104M5III2
—
—
—
—
—
0.032
0.023
—
—.
X
E08021015H5I111
—
0.058
—
—
—
0.080
0.634
—
0.080
3
E08041040N51112
—
0.C50
—
—
—
0.086
0.699
—
0.086
7
E08091025K5J1I2
—
0.070
—
—
—
0.501
0.930
—
0.119
4
£08110832X51112
—
0.0S7
—
—
—
0.321
0.762
—
0.095
6
E08151D14K5J112
—
0.059
—
—
—
0.452
0.823
—
0.1D3
r
E0B150S2SH5I112
—
0.063
—
—
—
0.323
0.786
—
0.091
/
EOS 171 DO 2H51122
—
0.064
—
—
—
D.2B0
1.646
—
0.086
7
E07281234H5I3
—
0.025
—
—
0.025
0.100
0.077
0.014
Y
£08011104H513
—
—
—
—
—
0.039
0.041
—
—
2
E08D21015M5I3
—
0.059
—
—
—
0.079
0.644
—
0.062
Z
E08041040K513
—
0.050
—
—
—
0.0BD
0.696
—
O.OB7
7
E080S1025N5I3
—
0.087
—
—
—
0.556
1.09
—
0.136
Z
E08110B32M5I3
—
0.077
0.246
—
—
D.385
0.903
—
0.110
6
EOB151014M5I3
—
0.093
—
—
—
0.540
1.05
—
0.129
s
E081S0926M5I3
1
0.094
0.107
—
—
8.383
0.964
—
0.11B
}
E08I71002M5I3
—
0.091
0.130
—
—
0.357
0.913
—
0.110
?
E0726 T234M5I4
—
0.020
—
—
—
0.046
0.036
0.059
—
4
E08011104N5I4
—
0.026
—
—
—
0.050
0.41
—
—
a
E0B021015H5I4
—
0.067
—
—
—
0.097
0.696
—
8.0B0
3
E0SQ41040N5I4
—
0.240
—
—
—
0.346
3.20
—
C.377
7
ED8091025M5I4
—
0.106
—
—
—
0.625
1.26
—
0.150
g
EOB110B32N5I4
—
0.106
0.271
—
—
0.515
1.U
—
0.13T
L
E0B151014M514
—
0.106
—
—
—
0.617
1.23
—
0.141
r
E0B16D926H5I4
—
0.093
—
—
—
0.3T9
1.06
—
0.120
/
E08171002M5I4
—
0.109
—
—
—
0.38B
1.13
—
0.123
X Recovery*
Detection lieit
96.5
0.077
SB.1
0.020
96.5
0.099
96.S
0.0090
SB.2
8.063
95.0
D.010
98.7
0.0027
100.
o.oss
99.9
0.0087
' - Analyte concentration < detection llrlt,
2 - Recovery based on a 5.00 egA spike addition to a 1:4 dilution of saoples E0B1T1D02H533 and E0B151014H5PM.
Saeple concentration were not earrected for recovery. 148
-------
Results of Metals Analyses - IWS Trace Metali Burns
Scrubber Slowdown Liquor (ng/L)
Pas* 1 of 3
Sanple ID t Arsenic Barfua Blswtti Cadafua Chratlui Copper Nagneslua Lead Strontlua
/B07281002 —1 0.2B5 0.941 — — B.726 J.67 0.304 J.295
607281324 0.125 0.373 2.22 0.051 — 2.41 4.95 I.S8 0.350
\ 601281424 0.120 0.370 4.44 0.085 — 2.65 8.13 1.58 0.371
807261531 0.158 0.396 6.75 0.137 — 2.95 6.70 1.8$ 0.405
607281631 0.203 0.438 7.25 0.162 0.11) 3.00 7.79 1.50 0.4(4
807281730 0.276 0.46S 6.58 0.145 0.212 2.87 7.77 1.44 0.472
B07281830 0.215 0.463 4.05 0.090 — 2.01 6.78 0.934 0.456
f308313900 — 0.329 0.390 0.015 — 0.330 6.40 0.093 0.4SB
( 306311103 — 0.258 1.40 0.035 — 1/04 4 . 25 0.404 0.357
808011203 0.124 0.274 2. $6 0.050 — 1.34 4.80 0.543 0.327
1 BOaOI'303 0.192 0.419 5.13 0.091 — 1.69 8.38 0.695 0.354
\808C11410 0.255 0.382 6.63 0.110 0.129 1.83 7.06 0.737 0.386
'B0BC2C900 — 0.229 — — — 1.193 3.62 — 0.407
608021020 . — 0.309 1.31 0.935 0.106 0.552 4.85 0.125 0.50S
2^ "f 808021120 — 0.266 0.313 — — 0.290 4.35 — 8.481
608021220 — 0.386 1.50 0.041 0.150 0.629 S.84 0.145 0.577
B08021320 0.130 0353 2.06 0.052 0.177 0.566 4.13 0.133 0.551
/mmm — 0.265 o.isi o.cn — o.zos 4.38 0.117 0.479
I 608041000 — 0.274 — — — 0.175 4.21 — 0.481
\B
V j.
\"
\ei
\(
0.397 0.700
^ 8080»1037 — 0.505 0.458 0.122 — 1.7B 6.02
808041137 0.109 0.304 2.30 0.062 0.365 1.03 5.31 0.259 0.435
\ 608041237 0.264 0.559 S.59 0.123 0.08B 1.53 8.02 0.474 0.530
\e08041337 0.3TO 0.470 8.61 0.177 0.108 1.98 9.56 0.6B9 0.612
/806090910 — 0.417 0.39S 0.014 — 0.827 8.39 1.091 0.794
J B08091025 0.123 0.205 1.26 0.033 — 0.951 6.62 1.177 0.557
? 808091125 0.152 0.309 2.76 0.054 0.089 1.17 7.48 0.292 0.696
\ B08091225 0.290 0.495 5.81 0.127 0.071 1.44 9.44 0.412 0.661
B08091325 0.219 0.372 4.81 0.100 0. 120 1.38 7.67 0.418 0.604
149
-------
Results of Mewls Analyses - INS Trace Metals Bums
Scrubbar Blowiiwi Liquor (ig/L)
(cont'd)
Page 2 of 3
"7^3-/~ Sasple IP S Arsenic Barfui Biswth Cacaiua Chrociua Copper WagnesiuB Lead Strantiua
2
r-
808110758
B08110830
B08110930
BOB 111030
BOB T11130
808111230
/B0815D30D
j 808150857
B08151057
808151157
B08151257
\fl08151357
B981ED805
908160913
B08161013
BD816-113
BOC161213
608161300
'B0817084S
808170955
BOB 171355
B08171I66
BB8171256
808171356
108171430
B081T1502
\ 806171536
\B0fll7ieiO
0.080
0.432
0.483
0.026
0.059
0.085
0.612
0.864
0.074
1
0.113
0.524
1.69
0.067
0.058
8.187
0.55S
2.44
0.077
0.117
9.722
0.567
3.53
1.109
0.205
0.251
0.790
5.01
0.148
0.277
—
0.269
—
—
0.077
0.107
0.790
0.074
—
0.099
D.444
2.22
0.079
0.080
0.162
0.466
3.46
0.1D5
8.184
0.200
0.(66
3.65
D.125
0.201
0.239
0.762
7.90
0.211
0.360
0.07B
0.269
0.401
0.024
C.074
0.125
0.289
1.30
0.038
0.124
0.160
0.668
3.54
0.075
0.163
0.201
1.18
4.84
0.101
0.232
0.270
1.33
5.80
0.149
0.311
0.313
0.932
10.3
0.223
0.374
1
0.310
0.506
0.018
—
0.073
0.355
1.03
0.028
—
0.087
0.477
1.68
0.041
—
0.129
0.639
2.36
(.047
—
9.162
1.01
3.64
1.077
—
0.1 97
1.06
4.15
0.086
0.057
J.171
0.885
4.0T
0.085
0.074
0.200
o.aoo
(.01
0.080
(.073
0.282
0.417
6.86
6.013
0.103
0.280
0.653
T.14
0.101
0.100
150
0.697
10.9
0.267
0.838
0.78S
10.5
0.216
1.17
0.811
8.40
O.IBO
0.935
0.839
9.24
0.255
0.921
0.929
8.20
0.273
0.645
1.04
8.42
0.372
0.871
0.525
4.37
0.050
0.4S6
1.29
6.21
0.188
0.641
1.03
7.15
0.210
0.645
1.02
7.55
0.232
0.647
0.934
7.44
0.251
0.643
1.32
9.34
0.141
0.709
0.447
4.62
0.096
0.495
0.654
4.57
0.221
0.504
0.843
5.34
0.324
0.553
0.931
6.04
0.392
0.659
1.13
6.77
0.(82
0.643
1.65
7.79
0.762
0.870
0.586
4.97
0.OB9
0.563
0.711
6.00
0.112
0.638
0.698
(.08
0.101
0.(03
0.636
6.35
0.077
0.585
0.722
6.03
0,114
0.692
0.552
7.76
0.101
0.633
0.601
7.63
0.117
0.626
0.571
6.19
0.097
0.625
0.B75
4.13
0.T12
0.6(2
0.911
4.77
0.719
0.704
-------
Page 3 of 3
Results of Metals Analyses - IMS Trace totals Sums
Scrubber Slowdown Liquor (ioA)
(cont'd)
Saiple 10 t Arsenic Sarlua Blsauth Cadalua Chroalua Copper Nagneslua Lead Strontlua
08171643
B0I171720
B081T17S5
308172030
0.288
0.373
5.49
0.091
0.089
0.B42
4.27
0.709
0.649
0.294
0.35D
5.58
0.077
0.085
0.764
4.14
0.6(3
0.614
0.258
0.351
5.05
0.073
0.094
0.781
4.37
0.563
0.(04
0.230
0.805
3.44
0.057
—
0.552
4.26
0.352
0.585
% Recovery 2 97.8 S3.8 92.8 94.7 94.4 95.2 93.8 92.8 94.0
Detection Unit 0.97 0.0083 0.12S 0.011 0.082 0.01 1 0.0013 0.041 0.0052
1 - Analyte value < detection Haft.
2 - Recoveries were determined froa a 5.00 ug/aL aatrlx spike addition to saaple 307281531.
Saaple concentrations Mere not corrected for I recovery.
151
-------
Results of Metals Analyses
IKS Trace Hetals Burns
Kiln Ash TCLP Extracts (nfl/L)
Sample ID t
Arsenic
Barium
Bisauth
Cadotiun
Chroeiun
Copper
Nagnesiun
Lead
Strontlus
TQ7281633-TCLP
0.109
0.327
<
0.130
< 9.010
< 8.093
1.01
91. E
0.069
0.626
T07287640-TCLP
0.231
0.EE7
<
0.130
0.012
< 0.083
1.64
109.0
0.067
1.42
T0901liOO-TCLP
0.124
1.12
<
0.130
< 0.010
< 0.083
1.84
100.9
0.067
1.71
TC 3031330—TCLP
0.157
0.848
<
0.130
< 0.010
< 0.083
1.60
103.0
0.051
1.63
r08031335-TCLP
0.280
0.559
<
0.130
< 0.01G
< 0.083
1.36
61.9
0.057
0.967
T0804U30-TCLP
0. US
0.505
<
0.130
< 0.010
< 0.OB3
1.05
109.0
0.090
1.13
I08091330-TCLP
< 0.088
0.94!
<
0.120
0.020
0.155
0.768
228.0
<
0.053
1.40
TOfi11123C-TCLP
0.219
0.528
<
9.120 < 0.0090
< 0.074
0.S73
70.1
<
0.063
0.BO5
T08151400-TCLP
0.1S4
0.629
<
0.120 < O.OC9C
< 0.074
1.32
96.0
<
0.063
1.17
T08161330-TCLP
0.150
0.508
<
0.120 < C.0090
< O.O'U
1.47
92.9
<
C.063
0.878
T08171400-TCLP
0.09S
0.S3S
<
0.120 0.019
< 0.074
1.20
171.0
<
0.CS3
1.48
t Recovery
96.5
98.2
102
97
96.6
97.6
103
97.8
102
! - Analysis not required (N.R.).
z - Recovery (I) based hi a 5.00 mg/L. spike addition to a 1:4 dilution of sanple's T0B1123QTCLP
and T07281S4Q.
Sample concentrations not corrected for recovery.
152
-------
Results of Metale Analyses - IWS Trace Metals Burns
Metals Matrix Spike and Matrix Spike Duplicates
Sarnie 9
Arsenic Barium Bismuth Cadmium Chromium Copper Magnesium Lead Strontium
Kiln Ash firqAo)
QD81714C0TMSK
C0817U0OTMSKD
Target
Scrubber Blowdown Liquor (mc/t)
51.8
184
136
19.0
94.5
<77
24070
27.2
272
51.9
212
144
18.8
93.8
459
23503
29.0
304
69.0
199
126
4.26
93.6
506
17413
48.4
268
Q031215203K5K
QD3-.215208MSKO
Targe:
0.262
0.254
0.313
0.904
0.917
0.932
9.81
9.91
10.3
0.227
0.231
0.223
0.341
0.357
0.374
Afterburner Exit Flue Gas Method 17 Multiple Metals Trains
lingers i and ? So!ution teics/l)
0D31510 0 OA 1MS K
Q03I51000A1MSKD
target
0.939
1.02
3.982
0.320
0.337
0.316
1S.S
20.7
19.5
0.781
0.833
1.10
55.9
60.1
53.7
1.53
1.55
I.S5
8.02
8.50
7.93
7.59
7.73
7.75
6.B5
7.31
6.67
C.702
0.698
0.762
1.45
1.55
1.47
0.653
0.665
0.670
0.154
0.165
0.145
Inai.ioers 3 and 4 Solution (mq/L
<)03:?1511A2MSK
QA03ul511A?
-------
Appendix C-3
Volatile Organic Analysis Results
154
-------
USEPA CRF
AOJKEX CQOTf;fiTJON
ANALYTICAL LABORATORY
TRACE METALS TEST SERIES
FEED ANALYSIS
UE/3W. T^t-Y -cut y •/ ru- A 7
COflFOUND FQL F07Z51620 F07251423 "F07J1I305 F07JUM5 F08011215 FOB011220 F&B02103C' F0BO21040
tCUNE
0,024
1,1-DCEANE
0,0315
DUJR0F0RI1
0.0318
1,1,1-TEEAME
0.0255
cai
0.03
BENZENE nSK
0.0279
CL3-EENE HSK
0.P297
1,2-DCPKANE
0.02BB
EDCtl
0.0318
t-l,3-PE'€
0.0169
TOLUENE NSK
0.0243
OCTANE SuRR
0.03
C-1.3-FENE
0.0153
1,1,2-TCEANE
0.01-27
CL4-EENE HSK
C. 03.24
a-BZ HSK
0.0265
ET-B2
0.027
NONANE ISTD
0.03
BfflfflFGRK
0.0424
4-BFB SURR
0.03
KCANE ISTD
0.03
1,3-KB I
0.02B3
1,4-DCBZ
0.0273
1,2-DCBZ
0.0348
(>!*> *•'<
-frJi J-*1 - > 3< ** 3' 5,0
T^P- / -
^g.i O
1I.04X 12, m IB. 157. 17.04)1 17.95* 14.B8X 18.40!! I9.39X
5.71X t.VH 3.11X 2.98* 3.02X 2.93Z' 3.23? 3.142
5.131 6.02% 2.932 2.771 2.872 2.84X 3.14* 3.052
ANALYSIS DATEi 0-7-39 B-7-89 8-B-89 8-B-B9 8-14-89 8-14-89 S-14-69 B-18-B9
FOC's REPORTED IN X.
155
-------
LSEPA CRT
AClflEI CORPORATION
AWU.YTICAL LABORATORY
TRACE flETflLS TEST SERIES
FEED ANALYSIS
u3/3)x -nj-i T^x. fix--? rz>7 rTJft ru-r 'T^C "7X>6
COOPOMD PflL F08021045 F08021105 FOEWOflOO F08OT9805 F08090B06 FOB090807 F05101000 F0810I010
HElflft C. 024
1, J-DCEANE 0.0313
M.OROFORH 0.0318
1.1.1-TCEANE 0.0255
CCL4 0,03
BENZENE HSK 0.927?
CLH3E K3K 0.0297
1.2-DCPRW€ 0.0288
BD01 0.034B
t-l,3-PENE 0.0189
TOLUENE UK 0.0243 1&.31X 1A.40Z 19.941 17.J3Z 1B.79Z 17.B0Z 19.2U 1&.39X
OCTANE SURR 0.03
c-l,3-P£?e 0.0153
1.1.2-TCEANE 0.0327
CL4-EENE fISK 0.0324 2.91J 2.B17. 3.221 2.69Z 3.442 3.1« . 3.30Z 2.7K
CL-BZ ASK 0.02B5 2.79* 2.79Z 3.091 2.B0Z 3.1 OX 2.B0Z 3.252 2.73Z
ET-B2 0.027
NONANE 1STD 0.03
BRCMDFOKN 0.0424
4-EFB SURR 0.03
DECA'C ISTD 0.03
1.3-DCBZ 0.028B
lt4—DCBZ 0.0273
1,2-DCBZ 0.0318
ANALYSIS DATE: B-1B-B9 &-10-B9 8-1B-B? 3-1B-B9 8-18-89 B-18-B9 8-1S-B9 B-lB-89
POHC's REPORTED IN X.
156
-------
U5EPA CRT
ACUREX CORPORATION
ANALYTICAL LABORATORY
TRACE ItTALS TEST SERIES
»-EED ANALYSIS
UG/3IL -rLa-s~ rz^-r 7~sh iZstl
COMPOUND
P3L
F08150830
F08I40750
FOBl&OBOO
HEX WE
0.024
1,l-DCEANE
0.0315
DLDfiCFORrt
0.0318
1,1,1-TCEANE
0.0255
cm
0.03
BENZENE HSK
0.027?
CL3-EDE HSK
0.0297
1,2-UCFRANE
0.02E8
Bttfl
0.034B
t-i,3-pec
0.0159
TOLUENE NSK
0.0213
IB. 571
IS.14*
17.261
OCTANE SURR
0.03
c-l,3-PE)£
0.0153
1,1,2-TCEAfE
0.0327
CH-EEfC HSK
0.0324
3,412
3.W
3.171
EL-BZ HSK
C. 0285
3.1 OX
2.B2T
3. MX
ET-BZ
0.027
NONANE ISTD
0.03
BfiDMDFOfW
0.0426
4-BFB SURR
0.03
OECWff ISTD
O.OJ
1,3-CCPZ
0.0283
1,4-DCBZ
0.0273
1,2-ICBZ
0.034B
ANALYSIS DATE:
B-1B-B9
B-lB-ffl
POHC's REPORTED IN Z.
157
-------
USEPA CRF
aajREI CCRFOflfiTiDN
ANALYTICAL LABORATORY
TRACE KETALS TEST SERIES
rEEO ANALYSIS
5PIH I RECOVERY
U6/3UL *1 12 »3 #1 S5 #6 #7 «8
COMPOUND P3L (109111310 MM111340 H09111340 1109111340 HWII1340 H091H340 H09111340 NW111340
ICIAHE 0.024
1,1-OCEAJt 0.0315
attKTOfirt 0.03X8
1.1.1-TCEANE 0.0255
EL4 0,03
BENZENE (ISC 0,0277
Q.3-EENE HSK 0.0297
|..:-DCPRBNE 0.0298
BOQi 0.03W
M.3-FENE 0.0169
TOLUENE KSK 0.0143 g 16.382 20.30* 19.322 18.32* 16.99* 17.98* IB.62* 16.282
OCTANE SL«S 0.03 Tj.T Sf. o zf.f S2.1 ZS~.f -?S-,e
c-J,3-PEf£ . 0.0153
1.1.2-TCEWE 0.0327
CL4-EM H3K 0.0324 3.25* 3.76* 3.30* 3.367. 3,73* 3.26* 3.80* 2.99*
ll-BZ MSK 0.0285 2.9B* 3.56V. 3.50* 3.23* 3.4
-------
USEfA CRf
AOJREI CWPCfWnON
A*tn!ML UKSflTtW
TWICE fETfiLE TEST SER.'ES
FEED AWPLV3IS
SPIKE t RECOVER*
UG/3UL
1? •
130
COMFOJHD
FQL
M07U1340
N09U13W
KKNE
0.024
1,1-DCEflrt
0.0315
CHDROFOM1
0.0518
l.i,i-TCEANE
0.0255
ecu
0.03
KHZENE riSk
0.0277
CL3-E3E «SK
0.0297
1,2-DCPftAHE
0.0268
BDCfl
0.0348
t-l,3-F£f£
0.0189
TOLUENE HSK
0.0243
19.471
l&.87i
ociac SUSR
0.03
J-J.7
¦7-?. 7
c-l,3-FENE
O.015J
1,1,2-TCEANE
0.0127
Q.4-EENE N5K
0.0324
3.92:
1091
CL-SZ K3K
0.0263
3.547.
3.017.
ET-BZ
0.027
NWWNE 157!)
0.C3
BRCWFOKfl
0.0424
4-EFS SUFfi
0.03
DECAtiE ISTD
0.03
1,3-DCEZ
0.028S
l,4-CC52
0.0273
1.2-DC32
0.0J4B
flfWLYSIS MTE:
9-12-6?
?-12-89
AUJ-
3. £~0
3.17
-7.2.
?. JL
-?.z
£2 J, 70
2>. ?*2
3.
*y.t %
/?*/». ¦
9^'^Z
POHC'5 reported in %.*>!&
f\JJ ^QO Gr ¥>'**¦
C /ya Ar-e&fyzJ S<*~y>f~
159
-------
~T«sf- / iJas-r-
I'jcPfl CRF
ACLREI CORPORATION
ANALYTICAL LA3DfMTDRV
TRACE MTTM.S TEST SERIES
TEST DATE: B-17-B?
A'JfiLYB15 DATE: fl-17-69
YS-o
yt.o
96,9
dscn
ug/dscs
ug/d.tj
ug/dscn
ug/tisca
ug/dseo
us/dscm
ug/ds:a
OWOUND
PQL
E0S171016V
E0817JM6V
EM171112V
A08171017V
A08171044V
A09171112V M9171046VFSK
Ml- /03b
/a iO-ilOD
f/0& - nii
ton-/a>t
/O Vo-i/60
y/a- »±i
OWE
1.20
1.71
2.41
1.23
2.33
0.00
1.12
1,1-DCEME
1.58
2.38
4.01
2.51
0.00
0.00
0.00
DLOROFORf,
1.59
4.11
5.41
4.03
O.OCi
1.72
B.25
1.1.1-TCEANE
1.28
0.00
0.00
0.00
0.00
0.00
0.00
CCL4
1.50
0.00
0.00
0.00
5.71
3.40
0.54
BENZENE MSK
1.40
7.70
14.06
5.17
0.00
0.00
0.00
1001
CLJ-EEJE K3S
1.4?
0,00
0.00
0.00
0.00
0.00
0.00
119%
1,2-KPRflNE
1.44
0.00
1.70
0.00
0.00
0.00
0.00
BDCH
1.74
0.00
O.OO
o.oo
0.00
0.00
0.00
t—1,3—PENE
0.95
o.oo
0.00
0.00
C.OO
0.00
0.00
tolloe msk
1.21
11.53
11.64
54.30*
7.60
35.59*
16.41"
937.
DCTAt SURP
1.50
107*
107%
1051
100%
ion
851
101*
c-l,J-P£KE
0.75
0,00
0.00
O.OO
0.00
0.00
0.00
l,l,Z-TEȣ
1.64
0.00
0.00
0.00
0.00
o.oo
u.00
CL4-EE>E MSK
1-62
0.00
0.00
<1.00
0.00
O.OCI
0.00
1007.
CL-BZ «5K
1.43
1.48
1.33
1.29
0.00
0.00
0.00
96%
ET-rZ
1.35
0.(0
1.27
0.00
0.00
0.00
0.00
tONANE ISTO
1.50
10B2.
1067.
1042
101%
100%
811
102%
BRMFKK
2.13
O.OO
O.OC
O.OO
0.00
0.00
c.oo
4-BFB SJRR
1.50
93%
767.
4B7.
767.
947,
677.
101*
DECANE 1STD
1.50
ioex
1C3X
m
98*
102 i
84%
103%
1,3-DCBZ
1.44
0.00
0.00
0.00
0.00
0.00
0.00
l,»-X6Z
1.37
0.00
0.00
0.00
0.00
0.00
0.00
1,2-OCBZ
1.74
0.00
0.00
c.oo
0.00
0.00
0.00
REPORTED IN % RECOVESV:
-SURRQEATES <5URS)
-IKTEWttL STANDARDS (ISTD5
-MATRIX SPIKE (NSKI
A BOTES LEVEL flSDVE POL.
(PRACTICAL QUANTITATION LIMIT)
160
-------
USEFA CRF
AC1JFEX COftPORATIDN
ANALYTICAL LABORATORY
TRACE HETflLS TEST SERIES
TEST DATE: B-17-a«J
ANALYSIS IATE: 6-17-89
COMPOUND
~ SCI
P9L
Ug/dSCl
GOS171016VFBK
SURROGATES
US/3UL
HEXANE
1.1-OCEflfC
CHLOROFORM
1.1.1-TCEfiNE
CCL4
BQCETIE MSK
CL3-EEJE MSK
1.2-BCfRANE
BDC.1
t-l,3-Ft>£
TDLlSf MSK
OCTAf€ SUfiR
c-l,3-PSNE
1.1.2-TCEANE
0.4-EBs'E MSK
CL-3Z ICK
ET-PZ
NONANE ISTD
BREH2F0R.1
4-ErB SlflJ?
DECANE ISTD
1.3-X3Z
1.4-DCSZ
1,2-XBI
1.20
1.58
1.5?
1.28
1.50
1.40
1.4?
1.44
1.74
0.95
1.21
1.50
0.75
1.64
1.62
1.43
1.35
1,50
2.13
1.50
1.50
1.44
1.57
1.74
1037.
1077.
1047.
107:
QCTWf
4-BFB
0.300
0.300
ISTD
USrtUL
mm o.3w
DECANE 0,300
MATRIX SPIKE
UG/3UL
EENZENE 0.321
CL3-EENE 0.2:3
TOLUENE 0.340
CL-4-EEHE 0.334
0,-Bt 0.336
fiEPGSTED IN 2 RECOVERY:
-SUFJEGflTES (SUES)
-INTERNAL STpM'ARK !1STD)
-MATSIX SPIKE (ttSO
* DENOTES LEVEL ABOVE RJL.
(FftPCTICAL SUAMITATIGN LIMIT;
161
-------
I^r u, yo^T
US EPA utF
ACUREH CfftPORATIDN
ANALYTICAL LAKSflTEW
TRACE METALS TEST SERIES
TEST DATE: 8-2-85
AWLYS1S DATE i
B-2-S9
tO. 7
Yo.i
fO. 2
37. 7
*0. 6
dsci
ug/dscn
ug/dscit
ug/dsca
ug/dsca
ug/risca
ug/dsca
ug/dscfl
COMPOUND
PQL
EOB021042V
E0B021118V
E08021159V
A0S0I1043V
A08021120V
A09021201V
Q9e02111BVFSK
JnVJ-lfO*.
l/IX-lflg
/Lrr~/±>9
/aY3-/A}i
ifSLes ~/s*/o
HEJfANE
1.20
3.80
3.58
0.00
1.94
0.00
2.01
1,1—DCEANE
1.58
5.71
2.49
1.66
0.00
0.00
2.68
M-OROFOftM
1.59
109.93"
28.34"
19.06"
5.18
1.58
5.22
1,1,1-TCAie
1.28
0.00
0.00
0.00
0.00
0.00
0.00
cat
1.50
0.00
0.00
1.67
0.00
1.99
0.00
BEN2ENE MSK
1.40
3.39
5.81
2.57
1.40
0.00
4.49
101%
CL3-SJC MSK
1.4?
0.00
0.00
0.00
0.00
0.00
0.00
117%
1,2-DCPKAHE
1.44
0.00
o.oo
0.00
O.OO
0.00
0.00
BDCtl
1.74
20.17"
36.97"
36.43"
0.00
0.00
1.49
t-1,3-PENE
0.95
1.01
0.00
0.00
0.00
o.oo
0.00
TOLUENE MSK
1.21
243.S1A
21.il"
12.44"
120.44"
4.64
54.10"
57%
OCTA(€ SURft
1.50
10c/!
100Z
1042
m
101%
97%
96%
c-l,3-pe£
0.75
2.85
0.00
0.00
0.00
0.0(1
1.09
1,1,2-TCsANt
1.64
0.00
0.00
0.00
0.00
0.00
O.CC
CL4-EEJE KSK
1.62
40.39*
3.52
2.59
22.05"
2.32
11.29
1047.
CL-SZ MSK
1.43
22.47"
2.50
1.97
17.56"
1.10
8.86
92%
E7—32
1.35
1.72
2.46
0.00
0.00
O.OO
0.00
NQNfiNE ISTi;
1.50
103%
1027.
1032
100%
100%
9t>%
94%
BRCflL'FDftH
2.13
7.42
77.55"
109.77"
3.55
2.32
3.18
4-pra suss
1.50
102%
837.
ee%
95%
-------
USEPA CRF
flCURH CORPORATION
ANALYTICAL LABORATORY
TRACE HE7AL3 7EST SERIES
TEST DATE: 8-2-39
ANALYSIS DATE: 9-2-09
dsca
ug/dsca
SURROGATES
COOTUM)
POL
00302115WFSK
US/3UL
HEIANE
1.20
OCTANE 0.300
1,1-DCEANE
1.58
4-BFB 0.300
CHLQRQFGRfl
1.59
1,1,1-TCEAIC
1.28
co.4
1.50
EENZEJC HSK
1.40
ISTD
QJ-ED£ HSK
1.49
U6/3UL
1,2-KrRANE
1.44
EfOcn
1.74
NONANE 0.300
t-l,3-PEJE
0.95
DECAIC 0.300
TOLUEH KSK
1.21
OCTAS SIER
1.50
1041
c-l,3-KKE
0.75
1,1,2-TCEANE
1.64
MATRIX SPIKE
CL4-E3E HSK
1.62
UG/3U.
CL-BZ H£K
1.43
E7-5Z
1.35
BENZENE 0.321
HONANE ISTD
1.50
1012
CL3-EEME 0.253
BROMtFGPil
2.13
TOLUENE 0.360
4-6r5 SIFS
1.50
1041
CL4-EEJC 0.336
D£CAf£ ISTD
1.50
1027.
CL-DZ 0.336
1,2-DCSZ
1.44
1,4-DCB!
1.37
1,2-DCSZ
1.74
REPORTS) IN 2 RECOVERY;
-SIjRSOSATeb (SURR)
-INTERNAL STANDARDS (2STD)
-MATRIX SPIKE !«£K)
A DENOTES LEVEL ABOVE P3L.
{PRACTICAL QUANTITATION LIMIT)
-------
UStPA CRF
ACL'REX CGr.rMATIDN
ANS.VT1CAL LABGKP.TNY
TRACE HETALS 7c57 SLR IE a
TEST DATE: B--5-E3?
ANALYSIS DATE:
E-4-89
WJ
rt. 7
dsca
ug/dscs
ug/osc»
ug/dsca
ug/dsca
ug/dscn
ug/dsca
ug/dsc#
Ca«X»ffl
PCL
E0B041106V
E0BO41144V
E03041219V
A0BO4I1O7V
floeo4n4iv
A08041217V
008041106VFSK
))OL'Ha-t
>W-/2oi
HE3ANE
1,20
1.21
1.99
3.33
1.89
0.00
0.00
1,1-DCEAKE
1.53
0.00
o.oo
0.00
0.00
0.00
0.00
CHLOROFORM
1.5?
10.98
0.00
5.33
3.37
2.00
0.00
1,1,1-TEEANE
1.28
0.00
o.oo
0.00
0.00
0.00
0.00
ecu
1.50
0.00
2.11
O.OO
2.33
0.00
0.00
BENZENE KSK
1.40
2.30
1.84
2.02
0.00
0.00
0.00
6V,
EL3-EENE HSX
1.49
0.00
0.00
0.00
O.OCi
0.00
0.00
m
1,2-DCrFWtiE
1.44
0.00
0.00
0.00
0.00
0.0(1
0.00
HOI
1.74
6.9s
6.49
9.35
0.00
0.00
0.00
i-I,3-rEN£
0.95
0.00
0.00
0.00
0.00
0.00
o.oo
TDLUSNE ft=K
1.21
29.32''
14.97*
12.43'
34.93"
30,
-------
USEPA C3F
ACUKEI CCRPCfiflTiCW
ANALYTICAL LABORATORY
TFJCE (CTALS TEST SERIES
TEST DATE: 8-4-39
ANALYSIS DATE: 0-4-B9
dscs
ug/dsca
SURROGATES
COWKJND
POL
QO8041144VFBK
UB/3UL
fEXANE
1.20
OCTAfE 0.3CO
1,1—DCEANE
1.58
4-3FB 0.300
CHLOROFORM
1.59
1,1,1-TCEANE
1.28
ca4
1.50
BENZENE HSK
1.40
ISTD
CL3-EENE MSK
1.49
UG/3UL
1,2-DCPRANE
1.44
BDQ1
1.74
NCNAfC 0.300
t-i,3-rEJE
0.95
DECANE 0.300
TOLUENE MSK
1.21
OCTANE SUftR
1.50
1021
c-l,3-r3€
0.75
1,1,2-TCEfltt
1.44
MATRIX SPIKE
CL4-EENS K3K
1.62
UG/3UL
CL-S2 KEK
1.43
ET-3Z
1.35
BENZENE 0.321
NCNANE ISTD
1.50
1042
CL3-EENE 0.25S
BRCMGFGRM
2.13
TOLOiE 0.360
4-BF8 SUSR
1.50
1053!
CL4-ELNE 0.336
DECAJE ISTD
1.50
1032
CL-BZ 0.336
1,3-DCBZ
1.44
1,4-DCBZ
1.37
1,2-DCBZ
1.74
REPORTS/ IN X REC2VESY:
-SUfiROSATEs (SUSR)
—IWTERHAL STANDARDS (ISTD)
—MATRIX SPIKE (MSK)
A DEMOTES LEVEL ABOVE PQL.
(PRACTICAL QUANTITATION LIMIT)
165
-------
/csT. 7 I/'
USEfl! C0*t£'J5TI0-ll ft£=EASCH FACtLI"V
M3LYTICU. LfBOWTOfiY
TMC5 NETfllS TEST SERIES
TEST DATE: B-l-89
ANALYSIS WTE: 8-1-e?
90 J
'/S-.2 26.?
-u»/esc*
COfWUM) " POL
ug/escs
EOSOl1119V
U! T-/H1
ug/cicn
E08011215V
/\s/
ug/dscn
E0S01133SV
ug/dscn
S03mi»8v
Uj/dHCS
SOS0U214V
ug'dscs ag/dscs
308011338V A080U1I7V
/J3p-/>r.t ml'1,2.1
ug/dsce
A06011220V
/Jja - /J
HEXANE
1.20
4.09
1.49
3.16
B.97
1.05
5.51
1.31
1.49
1,1-DCEANE
1.5a
0.00
0.00
0.00
15.64
1.82
9.49
0.00
0.00
CHLGRQF3W1
1.5?
7.87
5.0S
3.78
25.20*
6.90
5.74
4.01
1.45
1.28
1.96
0.00
0.00
0.00
0.00
0.90
O.CO
0.00
cai
1.50
0.00
0.00
0,00
O.OO
0.00
0.00
5.81
0.00
&H2ENE K3K
1.40
6.02
3.24
3.15
17.89*
10.93
8.40
4.C9
1.35
13-EENE r!SK
• 1.49
0.00
O.OO
0,00
0.00
2.12
1.39
0.0(1
0.00
1,2-DCPRANE
i.44
0.00
O.OO
0.00
0.00
0.00
O.OO
0.00
0.00
B&ZM
1.74
6.02
2.28
4,55
5.59
4.98
5.17
0.00
2.51
t-I,S-PEE
0.55
O.OO
0.00
0.00
0.00
O.OO
0.00
0.00
0.00
TOLUtfS tec
1.21
352.85*
215,35*
267.14*
363.40*
276.10"
225.49*
677.11*
5.30
OCTANE SLfX
1.50
hot
1073!
1062
lid*
952
104%
ion
1022
c-l,3-PENE
0.75
0.00
0.00
0.00
7.63*
0.00
O.OO
0.00
C.OO
1,1,2-TCEANE
1.64
0.00
0.00
0.00
O.OO
0.00
0.00
0.00
0.00
CL4-E3G M3.'
1.42
02.42*
30.94"
57.12*
190.97*
162.B1*
133.36*
173.60*
1.86
CL-E2 (EK
1.43
51. W
26.76''
47.03*
39.33*
20.35*
16.44*
122.6?*
0.00
£1-32
ll vO
4.8?
0.00
1.61
5.43
2.80
2.02
0.00
0.90
NffiMNE 1ST?
1.50
1072
107.
1012
1082
m
S4X
1012
ioir.
SfiCf"W1
2.13
]0i>.48*
187.71'
67,39"
25.74*
13.55
22.12*
2.31
1.91
4-BF3 SUK?
1.50
952
95*
57X
110'/.
/15T
\ my.
VL
962
DECME ISTD
1.50
291 y.
1022
m
1922
) 23V,
961
1012
l,5-£-2Z
1.44
C.OO
C.OO
0.00
0.00
o.co
0.00
0.00
0.00
1,4-DCSI
1.37
O.OO
0.00
0.00
0.00
0.00
0.00
0.00
0.00
1,2-PCEi
1.74
0.00
0.00
0.0(1
0.00
0.00
O.OO
0.00
0.09
REPCPJtl IS 2 SKOVtRV:
-SUWOSflTEa
-KftTRlX SPIKE (IBC)
JUL
•Hrvk^/. A*-*"-"
' DENOTES LEVEL ABOVE PQt.
(PftfiCTIWL ffJANTITATIW LIMIT)
166
-------
USE?A COMBUSTION RESEARCH FftCIL
ANALYTICAL USCWTGRY
TRACE /ETAL3 TEST HHIE3
TEST WiTE: 8-1-39
ANALYSIS DATE- e-l-B9
&
dsca
3o. U
ug/dsca
ug/ascs
ug/dsca
SURffQSATES
C3POUW)
POL
A080I133SV Q03C11338VFBX 808011214VFSX
/JW-/.»sV
US/3U.
HEXANE
1.20
0.00
OCTAI€ 0.300
1,1-OCEAfc
1.50
0.00
4-6FB 0.300
CHLOROFORM
1.59
2.10
1,1,1-TCEANE
1.28
0.00
CCL4
1.30
3.37
2.51
EENZENE MSK
1.40
0.00
1072
ISTD
CL3-EEJC HSK
1.4?
0.00
1212
US/oU.
1,2-XPME
1.44
0.00
3DCN
1.74
O.M
NQNANE 0.300
t—1,3-PEKE
C.95
0.00
PECAfJE 0.300
TOLiaE tt£K
1.21
21.95*
3.57
102Z
OCTANE SLflfi
1.50
96X
92*
100Z
c-l,3-P0€
0.75
0.00
1,1,2-TCEANE
l.H
O.M
MATRIX SPIKE .
CL4-EENE HSK
1.62
4.14
10EZ
US/3UL
CL-B2 HSK
1.43
2.97
95X
ET-BZ
1.35
O.OO
BENZENE 0.321
NGNftS 1STD
1.50
947.
m
99X
CL3-EENE 0.258
BftOflOFQKH
2.13
2.25
TOLUENE 0.340
4-bfb sura
1.50
967.
m
104JC
CL4-EENE 0.336
DECAJiE ISTD
3.30
95Z
887.
1011
CL-3Z 0.336
1,3-DCBZ
1.44
0.00
1,4-CCBZ
1.37
0.00
1,2-SCBZ
1.74
c.co
(SPORTED IN 7. RECOVERY;
—9USR0BATES (EURR'J
-IHTERHAL STANDARDS (I3TD)
—MATRIX SPIKE
-------
(JEEPA CK7
tam CORPORATION
Af&LVTICAL LAEORATGRY
TRACE METALS TEST SES1ES
TEST DATE: B-16-89
ANALYSIS DATE: E-I4-89
?Z£
"Ti^u.. i
vz ^
n.7
Y7J
*2/
drCfi
ug/dscn
119/dsM
ug/dsca
ug/tfeci
ug/d'c.i
ug/dsai
ug/d-ca
pa
E0B140952V
E08141032V
E0B141109V
AOS141033V
AO3140954V
AO814U09V Q0S141032VFSK
?s-a-io/a-
/
-------
USEFA CRF
AOJREX CORPORATION
ANALYTICAL LABORATORY
TRACE METALS TEST SERIES
TEST DATE: B-1S-89
ANALYSIS MTEi 8-16-89
dscn
ug/dscg
SURROGATES
COMPOUND
PQL
Q03140952VF3K
UG/3UL
raws
1.20
QCTW€ 0.300
1,l-DCEAKE
1.5B
4-EFB 0.300
CHOfiiFufiJi
1.59
1,1,1-TCEANE
1.28
ca.4
1.50
ENZENE KSK
1.40
ISTD
CL3-EENE KSK
1.49
UG/3UL
1,2-DCPftANE
1.44
BDCN
1.74
NONAfE 0.300
t-l,3-r2£
0.95
Dtcae o.3co
TOLUENE
1.21
OCTANE SURR
1.50
1547.
c-l,3-PENE
0.75
1,1,2-TCEAtC
1.64
MATRIX SPIKE
CL4-EENE KSK
1.62
US/311
CL-SZ (6K
1.43
ET-B2
1.35
BENZENE 0.321
NONANE 13TE
1.50
iOoA
CL3-EENE 0.2^8
EfiOHOFORM
2.13
TOLUENE 0.3eO
4-5FB SURR
1.50
mx
CL4-EE)C 0.336
DECANE ISTD
1.50
1062
CL-BZ 0.336
.1,3-DCBZ
1.44
114-DCBI
1.37
1,2-DCBZ
1.74
REPORTED IN I RECGVERY:
-SURROGATES (SURR)
-INTERNAL STAHDARDS (ISTT5
—MATRIX SPIKE WSK!
* DEMOTES LEVEL ABOVE PQL.
(PRACTICAL QUANTITATION LIMIT)
169
-------
/ b V/ ^J '
1;SE5h Enr
ACLSEX CiKPORATJQM
mniCflL LABORATORY
TRACE HETSLS TEST ERIES
TEST DATE: 8-1I
5-29
ANALYSIS SATE:
B-15-39
£JW)
SO. 2,
U.O-
Y&.0
r. 7
Y2,0
*7,®
n. t>
dsre
Ug/dSTH
119/dK®
ug/cscin
ug/dsce
ug/dscti
uc/dscs
ug/dici
COMPOUND
PQL EOS151052VT1
E08151139VT1
E08151239VT1
E03131314VT1
AOB151053VT1
A08151140VT1
ftCe!51£3^v!Tl
/aTJ »///.7
U%9-iao-7
'^3f-nr^f
/W-/7jy
MS" 2-///¦$
>EXA?£
1.20
8.59
4.42
4.3E
3.42
1.57
1.87
1.30
1,1-KEAfE
1.58
7.48
0.00
0.00
0.00
0.00
0.00
0.00
CHLOROFORM
1.59
7.97
5.B2
3.61
7.29
4.56
2.12
10.70
1,1,1-TCEWE
1.23
0.00
0.00
0.00
0.00
0.00
0.00
0.00
CCL4
1.50
O.to
2.51
0.00
3.36
0.00
0.00
0.00
BENZENE HSK
1.40
47.22"
17.6"
4'.. 51*
5.E4
5.37
0.00
2.44
0.3-EEff NEK
1.4"?
0.00
0.00
O.OO
0.00
0.00
O.OO
0.00
1.2-XFSttNE
1.44
0.00
0.00
2.07
0.00
0.00
0,00
0.00
ElCFI
1.74
c.oo
17.24
4.92
14.72
0.00
0.00
0.00
t-1,3-PENc
0.95
0.00
0.00
0.00
0.00
0.00
0.00
0.00
TOLUEME HSK
1.21
26.05"
5.40
11.67
*.35
19.34"
O OT
4.92
OCTANE SLRft
1.50
125>.
113%
122%
106*
' 102*
103V.
1012
C-!.3-?Efit
0.72
0.00
O.OO
0.00
0.00
0.00
0.00
C.OO
l,I,2-TCsS«
1.64
1.99
0.00
O.OO
0.00
0.00
0.00
0.00
CL4-EENE K5K
1.62
B.70
3.00
4.51
2.01
3.B4
1.54
o.co
a-32 K5K
l.*3
7.75
2.11
6.14
1.97
2.67
0.00
0.00
ET-5Z
1.35
2.44
0.00
0.00
0.00
O.OO
0.00
0.00
tONttE IETP
1.50
1203
E3K
1227.
109*
93*
9n
102*
BSOHOFDRM
2.1-3
s.oo
67.49
34. V-
76.25'-
2. B3
0.00
4.14
4-BFB SL'w
1.50
1067.
23/.
105*
94*
537.
797.
93*
DECffC I5TD
1.50
1187.
372
1172
lira
75*
87*
1002
1,3-DCBZ
1.4*
0.00
0.00
0.00
0.00
0.00
0.00
0.00
1,4-X3Z
1.37
25.18"
0.00
0.00
0.00
0.00
0.00
0.00
1,2-DCSZ
1.74
0.00
0.00
O.OO
0,00
0.00
0.00
0.00
REPORTED IN * RECOVEfiY:
-KJfcRCeSTES tSUFK)
-INTERNAL STSWBhRDS (137T-)
-IttTrtiX SPIK2 ItSK)
* DENOTES LEVEL MOVE POL.
(PRACTICAL QUANTITATION LIMITJ
170
-------
USEPA CTF
fiCMEX CORFffifiTiON
ANALYTICAL LABOnAT3!Y
TRACE HETAL3 ItST SERIES
TEST DATE; 8-15-89
ANALYSIS DATEl B-15-B9
CfflffKKD
dsca
POL
ug/dici
3O0151239VFSKT1
QOSl^lSWFSCTl
SUBROGATES
U6/JUL
WXANE
1.20
OCTANE 0.300
1.53
4-BFB 0.350
CUtSDFORM
1.5?
1,1,1-TCEtoE
1.29
co.4
1.50
0.03382
3»Z3E nSK
1.40
10SX
ISTD
CL3-ESNE M5K
:.49
1222
US/3UL
1,2-KPiMNE
1.44
BEM
1.74
NGNANE 0.300
i-l,3-?EME
0.95
DECftJC 0.300
TOLIESE HSK
1.21
7&Z
OCTANE SURR
1.50
1017.
c-l,3-FtNE
0.75
1,1,2-TCEANE
1.44
MATftll FPIKE
CL4-EEfE K5K
l.o2
1097.
UG/3UL
CL-32 M5K
1.43
947.
ET-BZ
!.35
BENZENE 0.321
NO
-------
-TUtl
usr'Pf awajsrioN research facility
AMYTICSL LAKRATGRY
TRPCE METALS TEST SERIES
TEST DATE! S-9-39
ANALYSIS DATE!
cortpoio
8-9-39
frJ
(&-)
tezn
POL
uo/dscs
E0B09I104V
/vj
«.*¦
ug/iisc« ui/dsen
E090'120"v E0809l244V»
- /- JJ-
V# s"
ug/dscn
S0B0911O5V
H-6-AVi
92,^ v?jt v/-f
ug/clscm uj/dsai ug/dEco
SOS091202V S0K 91244V A03091106V
ug/dsee
A06091202V
130 J-/JJ
hEXAME
1.20
0.00
i:n
7.55
3.42
2.29
1.43
0.00
1,1-DCME
1.58
O.OO
0.00
0.00
0.00
0.00
0.00
0.00
DtOfiOfOftn
1.59
5.94
17.20
22.45
14.51
14.54
4.9E
13.17
1,1,1-TCEAK
1.26
0.00
0.00
2.79
2.33
0.00
0.00
0.00
ca«
1.50
2.12
o.co
0.0-5
0.00
O.'ji'
0.00
9.99
BENZENE KSK
1.40
0.00
. 2.34
102.15
139.49
90.34
40.47
4.41
0.3-EENE YSK
1.49
0.00
0.00
0.00
0.00
0.00
0.00
O.OO
1,2-DCHMNE
1.44
0.00
0.00
5.45
5.7S
2.91
1.72
0.00
boc?i
1.74
6.38
2.49
16.45
15.78
13.14
0.00
0.00
t-l,J-PENE
0.95
0.00
0.00
0.00
0.00
0.00
0.00
o.co
TOLUSfE KSK
1.21
9.52
13.45
545.50
544.41
434.25
44.40
4. OS
OCTANE 3PR
:.£C
961
1057.
1142
113X
104X
1017.
1017.
c-l,2-PEME
0.75
0.00
0.00
0.00
0.00
0.00
0.00
0.00
1,1,2-TCEANE
1.64
0.00
0.00
o.oo
0.00
0.00
O.OO
0.00
G.4-EEN". hsk
1.42
2.67
3.07
157.90
137.71
124.ES
35.17
0.00
CL-BZ HSK
1.43
0.00
2.39
53.20
50.73
37.56
13.44
0.00
ET-BL
1.33
0.00
0.00
3.40
3.05
2.55
0.00
O.OO
NCtF.fe ISTT
1.50
in.
1077.
i:i7.
1077.
997.
1017.
977.
»M0?03H
2,13
25.52
149.44
29.85
22.71
Id. 99
0.00
0.00
4-BF3 SURR
1.55
241!
962
9EZ
SEX
AH
94X
82X
KCANE IETD
1.50
61*
1131
121a
1132
87X
1052
95X
1,3-DCBZ
1.44
0.00
0.00
o.oc
0.00
0.00
0.00
0.00
M-dbz
1.37
0.00
0.00
0.00
0.00
0.00
0.00
0.00
1,2-PCBZ
1.74
0.00
0.00
C.00
0.00
0.00
0.00
0.00
SURRQSATES REPORTED IK
ISTD PEPCfiTED IS X.
KSK REPORTED IN 1.
* StfflE LOST
172
-------
USEPA CGflBUSTION RESEARCH FftC
ANALYTICS LABORATORY
TRACE HETAL5 TEST SERIES
TEST DATE; 3-9-39
ANALYSIS DATE: B-9-99
n.v
-'y/dsca ug/dsra ug7dsca ug/dsca SURROGATES
CCTU® * PQL A0B091245V 008091202VFSK QOeWlMVFBK U6/IUL
HEXANE
1.20
1.46
OCTANE 0.300
1,1-DCEANE
1.58
0.00
4-BFB 0.300
M-QROFORfl
1.59
16.91
2.06
1,1,1-TCEANE
1.25
0.00
CCL4
1.50
11.29
2.39
BENZENE KSK
1.40
4.67
lOiZ
ISTD
CL3-EBC m
1.49
0.00
1202
U6/3UL
1,2-DCPRk?€
1.44
O.OO
sDCM
1.74
0.00
NONANE 0.300
t-1,3-P£WE
0.95
0.00
BEChNE 0.300
TOLUENE MSK
1.21
4.16
962
OCTANE SL'Sft
1.50
102:
103*
95%
c-l,3-PENE
0.75
0.00
1,1,2-TCEhNE
1.64
0.00
MATRIX SPIKE
CL4-EENE NSK
1.42
0,00
1072
UB/3UL
CL-BZ KSK
1.43
0.(30
931-
ET-flZ
1.35
0.00
BENZENE 0.321
NGNANE ISTD
1.3)
1062
1C5X
1027.
CL3-EENE 0.253
BftfflfirQRN
2.13
O.OC
2.34
TOLUENE 0.360
4-BFB 3UPS
1.50
91*
1097.
1042
CL4-EENE 0.336
DECANE ISTD
1.50
1012
1102
1042
CL-BZ 0.336
1,3-DCBZ
1.44
0.00
1,4-DCSZ
1.37
0.00
1,2-DCSZ
i.74
0.00
SURRQShTES reported in s.
iSTD REPQSTED iN 2.
KSK REPGftTED IN 2.
* SAMPLE LOST
173
-------
E \J;
.n
3-
0.00
0.00
O.OO
9.09
0.00
S2.45*
0.00
O.M
838.33*
1J9.IS*
23.14*
67.33"
0.00
1697.25"
0.00
4.60
464.73"
207.44'
3.95
HOI
45.41*
1B5X
103X
0.00
0.00
0.00
30.53*
25.05*
71.97"
34.71*
105.54*
940.50*
134,39*
26.72*
79.E5*
5.43
1563.51*
1647.
2.94
5.15
425.52*
IS. 26*
5.53
123/;
37*
1137.
10BV.
0.00
0.00
0.00
01.
1.17
0.00
13.28
0.00
9.16
3.14
0.00
0.00
0.00
0.00
4.B9
102%
O.OO
2.20
1.24
0.90
0.00
102Z
0.00
99*
0.00
0.00
0.00
)-e+k ef'&uc-L/>*r
Z/JLJ
L
1.57
0.00
7. ^
O.OO
7.08
4.79
0.00
0.00
O.OO
0.00
32.65*
1021
0.00
0.00
5.73
4.50
0.00
-------
USEPA COMBUSTION RESEkSCH FACIL
ANALYTICAL LArORATW
TRACE KFTAL3 TEST SERIES
TEST DATE: 6-r-fi?
ANALYSIS DATE: B-9-09 fg,X-
dscn ug/
-------
-71
l/2-s"
USEFA CRF
ACUREX COfifWATlDN
ANALYTICAL LABORATORY
TRACE fETALS TEST SERIES
TEST DATE: 7-28-B? •
fj at>
ANALYSIS DATE: 7-2£-e?
1
1
l^s
w yr*
3Z
-------
USEPA CSF
ACUREX CORFSfiflTICN
ANALYTICAL LABORATORY
TRACE ICTALS TEST SERIES
TEST DATE: 7-23-59
AMALYS15 DATE: 7-2S-89 4 7-31-
dscn
ug/dsca
SUPKCGATE3
COrfOUKD
PQL
007281530VFBK
L6/3UL
fOAJC
1.29
3.02
OCTANE 0.300
1,1-DCEANE
1.53
4-BFB 0.300
CHLQRDFDRM
1.59
19
1,1,1-TTEfttC
1.28
ccl4
1.50
SENZEfC HSK
1.40
2.69
ISTD
a3-EE>C tt£K
1.49
UG/3UL
1,2-DCPRANE
1.44
BOCtl
1.74
fCNANE 0.300
t-l,3-PENE
0.95
DECANE 0.300
TOLUENE H3K
1.21
1.47
OCTfWE SLKR
1.50
1017.
c-1,3-PENE
0.75
1,1,2-TCEAME
l.e4
MATRIX SPIKE
CL4-EENE ,MSK
1.62
U6/3JL
CL-Bl KSK
1.43
ET-BZ
1.15
BECENE 0.321
NCNANE IETD
1.50
101Z
CL3-tE>i£ 0.258
BRDK3F0W1
2.13
TOLUENE 0.3i0
4-3F3 SUW
1.50
1032
CL4-£Ef£ 0.336
DECANE ISTD
1.50
1022
CL-BI 0.336
1,3-ECBZ
1.44
1,4-DCBZ
1.37
I.2-DCS2
1.74
REPORTED IN 1 PECOVEP.Y:
-SJRRGGA7ES
-------
US£PA IRF
ACUREX CORP
ANALYTICAL LABORATORY
TRACE METALS TEST SERIES
ftSH ANALYSIS
9
?
Y
3
a
X
7
s
UG/G
UG/E
US/B
UG/6
UG/6
UG/G
US/5
UG/G
UG/G
COMPOIMD
PQL
TO720I&3?
T07?81MO
T03011400
T08041430
T08031330
T08031335
T06091330
T0B1I12
HBANE
80
ND
ND
NO
ND
ND
ND
ND
KD
1,1-DCEANE
105
ND
ND
ND
M)
ND
ND
W>
ND
DiOROFORM
106
Nfl
ND
ND
KD
ND
ND
ND
ND
1,1,1-TCEANE
65
ND
ND
ND
ND
ND
ND
ND
ND
CCL4
100
ND
ND
Nil
WD
ND
ND
ND
ND
BENZEJE
93
ND
ND
ND
ND
ND
ND
ND
ND
CL3-£Ef£
99
NT)
ND
ND
ND
ND
ND
ND
14)
1,2-DCPRANE
96
ND
ND
ND
ND
ND
ND
ND
ND
KM1
116
ND
ND
ND
ND
ND
ND
ne
ND
1—1,3—FENE
63
ND
ND
ND
ND
ND
ND
ND
ND
TM.UENE
81
ND
ND
NE
ND
ND
ND
NE
Iffl
c-1,J-PENE
51
ND
ND
ND
ND
ND
ND
ND
ND
1,1,2-TCESNE
109
ND
ND
ND
ND
ND
ND
ND
ND
CL4-EENE
108
ND
ND
ND
ND
ND
ND
ND
NT'
CL-BZ
95
ND
ND
ND
1®
ND
ND
ND
ND
ET-B2
90
ND
(ID
ND
NT'
ND
ND
ND
ND
BWMOFDfiK
142
ND
ND
ND
ND
ND
ND
ND
1,3-CCBZ
96
ND
HD
ND
ND
ND
ND
ND
ND
1,4-DCE'Z
91
ND
ND
ND
ND
ND
ND
ND
NIi
1,2-DCBZ
116
ND
ND
ND
ND
ND
Ml
NC
ND
ANALYSIS DATE:
B-7-89
E-7-S9
B-3-89
8-8-39
6-16-89
E-16-B9
B-J 6-89
8—IB-
~WD DENOTES LEVELS BELOW F-QL
IPRACTICAL QUANTITATION LIMIT!
-------
USEPA IRF
ACUREX CORP
ANALYTICAL LABORATORY
TRACE METALS TEST SERIES
ASH ANALYSIS
US/G
COMPOUND POL
3 6 l
UG/G ue/s UG/6
TQ8121300 T08151400 T0817HO0
HEXWt
80
ND
ND
ND
1,1-DCEANE
105
NO
ND
ND
CHLOROFORM
106
ND
ND
nd
1,1,1-TCEANE
B5
ND
ND
ND
CCL4
100
ND
ND
ND
BENZENE
93
ND
ND
ND
CL3-EENE
99
ND
ND
ND
1,2-DCPRANE
96
ND
ND
ND
BDCN
116
ND
ND
ND
t-t,3-PENE
63
ND
ND
ND
TOLUENE
61
ND
ND
ND
c-1,3-PENE
51
ND
ND
ND
1,1,2-TCEANE
109
ND
ND
ND
G.4-EENE
JOB
ND
ND
ND
CL-BZ
95
ND
ND
ND
ET-BZ
90
MD
ND
ND
BROftOFORfl
142
ND
ND
ND
1,3-DCBZ
96
M)
ND
ND
1.4-DCB2
91
Nli
ND
ND
1.2-DCBZ
116
ND
ND
ND
ANALYSIS DATE:
8-18-89
8-18-89
8-19-
««D DENOTES LEVELS BELOW PQL
(PRACTICAL QUANTITATION LIMIT)
179
-------
USEPA IRF
flNALiTlCAL LABOftfTCRY
TRACE METALS TEST SKIES
BLQWJOMN ATMLV5IS
"TSs'T"5
r
i
2.
1
~7
B
£
uj/L
ug/L
ug/L
ug/L
ug/L
ug/L
U9/L
ug/L
ug/L
COMPOUND
POL
BO7201631
B06011410
808021320
B0B041337
B08091323
B0S111230
B08141530
80915131
HEXANE
4.BO
ND
Nil
ND
M)
ND
ND
ND
ND
1,1-DCEANE
£.30
NO
ND
ND
ND
ND
ND
ND
ND
CHLOROFORM
6.36
ND
ND
ND
>ffl
ND
10.06
ND
ND
1,1,1-TCEANE
5.10
ND
ND
ND
ND
ND
ND
ND
ca.4
6.00
ND
ND
ND
ND
ND
ND
ND
ND
BENZENE
5.56
»
ND
W
ND
ND
ND
ND
ND
CL3-EENE
5.94
ND
ND
ND
ND
NE
ND
ND
ND
1,2-BCPRANE
5.74
ND
M)
ND
ND
ND
ND
ND
ND
BDCH
6.96
43.6
ND
13.S
ND
16.09
21
ND
i
t-!,3-PENE
3.7B
NO
ta
ND
ND
ND
ND
ND
NI
TOLUENE
4.86
ND
ND
ND
ND
ND
ND
ND
ND
c-l,3-FO£
3.06
ND
ND
ND
ND
ND
ND
ND
ND
1,1,2-TCEWC
6.54
ND
ND
f£
ND
ND
ND
ND
ND
CL4-EENE
6.48
ND
ND
ND
ND
ND
ND
ND
ND
CL-BZ
5.70
ND
ND
NE
ND
ND
ND
ND
ND
ET-BZ
5.40
ND
ND
ND
ND
ND
MJ
ND
ND
BROHDFORM
9.52
85.2
13
26.2
67
39.6
9.56
ND
ND
1,3-ECBZ
5.76
ND
ND
ND
ND
ND
ND
ND
ND
i,4-raz
5.46
ND
ND
ND
ND
ND
ND
ND
ND
1.2-tCEZ
6.94
HD
ND
fffl
ND
ND
NC
ND
ND
ANALYSIS DATE: 6-7-B9 8-7-89 6-B-B? 8-8-89 6-16-89 B-1B-09 3-18-S9 9-10-99
~ND DENOTES VALUES BELOW P3L
(PRACTICAL QUANTITATION LIMIT;
180
-------
UStPA FRF
ANALYTICAL LABORATORY
TRACE fETALS TEST SERIES
BLDMDOWJ A'ttLYSIS
jT
I
ug/L
ug/L
ug/L
COMPOUND
POL
B0E1613Q0
BOB171356
HEXWE
4. BO
rc
ND
1,1-DCEANE
6.30
NO
ND
CHLOROFORM
6.36
39.8
ND
1,1,1-TCEANE
5.10
ND
ND
ca.4
6.00
ND
Ml
BENZENE
5.58
NO
ND
CL3-EENE
5.94
ND
ND
1,2-DCPRANE
5.76
ND
ND
BDCfl
6.96
29.2
ND
t-|,3-PENE
3.7B
NO
ND
TDLIENE
4.86
ND
ND
c-l,3-PEK£
3.06
ND
W)
1,1,2-TCEANE
6.54
ND
ND
Q.4-EENE
6.46
ND
CL-BZ
5.70
ND
ND
ET-BZ
5.40
ND
BRONFORM
8.52
ND
Iffl
1,3-DCBZ
5.76
ND
ND
1,4-DCBZ
5,46
ND
ffi)
1,2-DCBZ
6.96
ND
ND
ANALYSIS DATE:
8-IB-89
8-1B-89
«NE DENOTES VALUES BELOW POL
(FRACTICAL QUANTITATION LIMIT;
-------
Appendix L-4
Ultimate Analysis Results
182
-------
HARRY W GALBRAITH, RM.O
CHAIRMAN or TNC BOaUD
KENN ETN I. WOODS
PRESIDENT
GAIL. R. MUTCHENS
CXCCUTIVK VICt. FHESIDCNT
VEJ.MA M. RUSSELL
•EcncTAiir^mcAmuMtM
P.O. BOX 51610
KNOXVIU.E, TN 37950-1610
GAL.E>It9<£ITH
Jla&oKxto'iiE.i., line.
QUANTITATIVE MICROANALYSES
ORGANIC - INORGANIC
615/546-1335
2323 SYCAMORE OR.
KNOXVILLE, TN 3792M750
Ms. Joan Bess
Acurex Corporation
Highway 65 North, NCTR Bldg. 45
Jefferson, Arkansas 72079
October 3, 1989
Received: September 12th
Dear Ms. Bass:
Analysis of your compounds gave the following results:
t
Your #,
Our #,
% C,
% H,
% CI,
% O
F08151050
H-7070
20.55
2.74
< 0.008
7.87
1
F08161055
H-7071
22.82
2.62
< 0.008
7.15
1
F08161100
H-7072
20.46
2.99
< 0.009
7.13
JL/.lg 2'*^
Sincerely yours,
GALBRATTH LABORATORIES, INC.
TSail R. Hutchens v
Exec. Vice-President
GRHssc
183
:TTER AND SHIPMENTS BY U.S. MAIL • P.O. BOX 81il0. KNOXVILLE.TN J7»5O-1«10. OTHER CARRIERS - 293J SYCAMORE DR. KWOXVII
ESTABLISHED ItBO
HTJO
-------
KA*"V W- 0ALBWAITW. PH.O
CHMRN4N Or TMf •CAWS
KENNKTH «. WOODS
MtimrNT
GAIL. A. HUTCHINB
lltcumi WICC- MIHBIMT
VELMA M. HJ»»CLL
•CCMCrAAY/rauauMtM
^CciLoxatozis^ fJne.
P.O. BOX 5I6IO
KNOXVILLE, TN 37950-1«10
QUANTITATIVE MICROANALYSES
ORGANIC - INORGANIC
• 18/046-1333
2323 fiYCAMORC DR.
KNOXVILLE. TN 37921-1750
Ms. Joan Bass
Acurex Corporation
Highway 65 North, NCTR Bldg. 45
Jefferson, Arkansas 72079
September 26, 1989
Received: September 12'
PO#: EN25S12Z
Dear Ms. Bass:
Analysis of your compounds gave the following results: 4oy
:/.n
J-3 2. (Jf C.i
*t=e
Your #,
Our #,
% C,
% H,
% CI,
% O,
tc
7
F0725162D
H-7051
19.09
2.19
6.27
7.68
njr
7
FC7251623
H-7D52
15.20
2.24
5.94
5.58
/
FC7311305
H-7053
21-70
2.80
3.49
6.54
/
F07311315
H-7054
21.74
2.44
3.15
8.89
20.&
/
F08011215
H-7055
19.21
2.B4
3.05
8.59
2
F08011220
H-7056
20.33
2.57
3.06
8.06
rt.JEJ
F08O21O3O
H-7057
*717.97^,
2.40
3.33
7.20
3
F08021040
H-7058
/
! 20.63
2.97
3.71
7.77
3o.o3
FOB021045
H-7059 i
19.42
2.70
2.16
8.49
.2.
F08Q21105
H-70S0
W 12.19
1.45
2.30
7.63
7
F0S09O800
H-7061
16.73
2.28
2.43
6.89
17. «J
7
F08D90805
H-7062
17.32
2.29
3.73
5.39
7 2.4
z./y x.io
2..S/ Ut
?.2g 2.fg t>./-
tKTTf H AND iHfPMtWTS tY U.S. MAIL • P.O. BOX KNOXVfLLC« TN S7t50'1#10. OTHER CARRIERS • 2321 trCAMORS DR« KNOXVlLLK.TN J7»2l*t?Se
KSTAfeLtSHCD !•«© ^
-------
Appendix C-5
Flue Gas HC1 Train Analysis Results
185
-------
US EPA IRF
IWS Trace Metals Test Series
Chloride Ion Analysis
Sample ID #
Test
mg CI"
mg ClVdscm
A07281234IH2
9
57,960
3812
E07281234I112
450
154
S07281400I1
4.13
S07281400I2
< 1.86
< 6.4
50728140013
<1.46
Aoaomo3iii2
4
45,540
1963
E080111041112
< 14.05
<4.7
S08011150n
< 2.4
S0801115012
< 3.5
< 5.7
S08011150I3
< 1.65
A08020950I112
2
50,730
2320
£0802101511I2
< 14.37
< 4.8
S08021057I1
< 3.5
S08021057I2
<1.65
< 5.1
S08021057I3
< 0.75
AOB0410371112
3
27,900
1370
E08041040I1I2
< 14.50
< 4.9
S08041108I1
< 3.35
S08041108I2
<2.67
< 5.6
S08041108I3
< 2.2
A08091025I112
7
42,180
2214
£080910251112
<9.55
< 3.1
S08091030I1
<3.75
S0809103012
<4.10
< 6.1
S08091030I3
<0.50
A08110830I1I2
8
67,950
< 2863
E0811083211I2
<1.42
< 0.5
S0811083711
< 10
S0811083712
< 10
< 7.3
S08110837I3
< 10
A08150957I112
6
53,680
1774
E08151014I1I2
<3.35
<1.1
S08151037I1
<3.82
S08151037I2
<2.90
<5.2
S08151037I3
< 0.34
A08160918I112
5
64,600
2316
EQ8160926I112
14.2
4.6
S08160925J1
< 3.10
S08160925I2
<2.98
< 5.4
S08160925I3
<2.66
A08170956I112
1
6,120
207
E08171002I1I2
<1.38
< 0.45
S08171041I1
<3.38
S08171041T 2
<3.34
< 5.7
S08171041I3
<2.48
186
-------
APPENDIX D
SAMPLING TRAIN DATA SHEETS
Sampling trains are designated by ED numbers in the following data sheets. The ID
code for each train follows the sample coding scheme described in Appendix C.
187
-------
' C5
-t I
CALCULATED RESULTS FOR SAMPLE #
fl0317095SHMl7
Plant: CRF Ucdated
Perfcrred by:
C.KIN6
Data: 3/17/39 Printed 0^/02/83
Test No./TyMi
A0517035M117
lsokir 3ticity
i I
=
23.9
Sanole Lrcation: AFTERBURNER
Start/Stoo Tine:
0955-135B
Petered Sajiole Gas VoIueb (scf)
V(i std)
=
1044.08
(see)
VI* std)
3
29.5S£
~
EVE™.
r.s;-' ^"2= ^low, c?*"1-. 'isz;)
2(sl
=
ct;
(calc.)
std cond. (dscra/ninlGIs)
13.2
Nozzle DiMeter, Actual linl
Ntd)
1.49
ictual (acfu)
0(a)
S
3E£9
Pitol Tube Correction Factor
C(D)
0.34
actual (acs/nin)
3(a)
s
92.3
545 Meter Correction Factor
(alpha)
1.03
Particulate Loading, dry (gr/dscf)
CIs std)
s
0.0463
Stack (Duct) Diamlons I in) i
S 7* OSIgr/dscf) C(s std)
s
0.0512
Radius (if round!
R
8 7< D2(i;o/d5CB) CIs std)
=
117
Length (if rectangular)
L
20
Particulate Emission Rate (lb/hr)
£(d)
s
0.234
Width (if rectangular!
U
12
ikg/hr)
Eta)
=
0.115
Area of Stack (sg ft)
Pis)
(l.USSfi
)
Stack Bas Hater Vapor Proportion
fi(HO)
=
3. OSS
1 of Saiple Points
1
£
Molecular Height of Stack Gas, Dry
Bid)
•
29. 51
Total Sailing Tine (nin)
(theta)
( 242.00
)
Met
H(s)
a
SB. 49
Bsroeetric Pressure (in Hg)
Plb)
30.02
Stack Pressure, absolute (in Hg)
P(s)
¦
30.01
Stack Pressure (in H20)
Ptstack)
-o.oe
Averace Stack Velocity (ft/sec)
V(s avg)
a
32.7
Gas Hater Initial Reading (cu ft]
113.4
Gas Meter Final Reading (cu ft)
1296,7
Net Bas Suple Voiuaa (cu Ft)
VW
(1113.30
)
Vol of Liquid Collected 1ml)
VI (c)
2150.77
Vol of Liq £ std. Conds. (scf)
V(m std)
(101.237
1
Wt. of Filter Particulate (cu)
2.08
Ht. of Probe fesh Particulate (at)
1.05
¦It of Coibired Particulate (gti)
N(s)
( 3.1300
)
BE Concentration (by COt)
»
G.36
EJ2 Concentration (iiy CEM)
*
7.34
CO Concentration (by C-M)
*
0
X Corcentration (by diff. 1
%
( B4.30
)
Saiple
Point
Ssplc
TOTALS
dClock !Velocity. Orifice
Tin (Head, dP!Meter, riH
(nin) !(in H20)!(in M20)
124 I 0.072
US I 0.072
0 1 0
2.2
2.2
0
Stack
Tbbd
(degFI
Sis Meter
Tea): tdajF)
in ! out
2000
2000
0
203
203
0
-4—
242
0.14 ! 4.4000 ! 4000.0 i 406.0
120
120
0
SORT(dP! I FIELD DATA AVERAGES FOR SAMPLE I
I
iVelocity Head Chc)
0.2683 SOrifice fteter Reading Chc)
0.2663
0.0000 IStack Temperature (deg F)
— ! (deg D
(Meter Temperature
!Root-Wean-Square dP
(deg F)
(deg C)
(V)
A081709SWW7
dPtavgl = 0.072
dHiavg! = 2.200
T(s avg) = 2000.0
T(s avg] = 1093.3
Tie avg) = 161.5
T(a avg) = 71.9
SaRT(dP) = 0.268
240.0 ! 0.5367
188
-------
ISOKINETIC RESULTS
CALCULATED RESULTS FDR SAMPLE 1 —
E0E17100315
Plant: CRF Updated 12/09/B9
Ferforned by: J.MILLS
Date: 03/17/89 Printed 12/09/99
Test No./Type: E08171C02N5
Iso.cineticity
X 1
s
102.7
Saaple Locaticn: SCRUBBER EXIT
Start/Stop Tiae: 1002-1153
Metered Sacple Gas Voluie (scf)
Vic std)
3
109.03
(sen)
V'i std)
r
3.03E
PARAMETER
SYMBOL
VALIC
Stack Gas Flow, std cond. (dszfsi)
Qts)
~
1359
— r
Nsule Diaeeter, Actual (in)
Nld)
.:
0.375
actual (acftt)
> w • a.
Q (a)
s
2632
Pi tot Tube Correction Factor
C(p)
0.84
actual (aca/ainl
a (a)
=
71.5
6as Meter Correction Factor
(alpha)
1.03
Particulate Loading, dry (gr/dscf) C(s std)
=
0.0044
Stack (Duct) Disensions (in);
6 U G2(gr/dscf) C(s std)
=
0.0376
Radius (if round)
R
7
8 11 02!iig/dsca) C
-------
/
-------
~T&.k
ISOKINETIC RESliTS
CALCliATED RESULTS FOR StWPLE 1 —
A0B92&95OKN17
Plant: CRF Uodated
Perforned by:
C.KING
Data: 3/05/39 Printed 09/02/89
Test No./ryoei
HCfl02O95ttH17
Isokinetieity
* I
=
95.4
SaE^le Location: AFTEFBURMER
Stsrt/Steo Tiee:
0950-1:27
Metered Saiole Gas Voluae (scf)
V(i std)
=
772.32
(sea)
V(« std)
=
£1.870
PARAMETER
SrtBOL
VALUE
Stack Gas Flo*, std cond. (dscfe)
B(c)
=
589
leal:.)
std cord. !dsca/«;n)Q(s)
=
16.7
Nozzle Oiurstsr, Pcttial tinl
K(d)
MB
actual (acfa)
0(a)
U
2837
Pitot Tube Correction Factor
C(o)
0.S4
actual iaco/iin)
Ota)
*
82.0
Gas Heter Correction Factor
lalptia)
1.03
Pa-t:cula:e Losing, dry (gr/dscf) C(s std)
S
0.0230
Stack (Curt) Dimensions (in):
0 71 02(gr/dscf) C(s stc)
3
0.0305
Radius (if round)
R
8 7< 02(ng/dsca) C(s std)
C
70
Length (if rectangular!
L
20
Particulate Eaission flats Ub/hrl
E(ol
-
0.146
Width (if rectangular)
H
12.25
(kj/hr)
E(p)
a
C.06S
Urea of Stack (sq ft)
ft's)
1.70134 )
Stack 6as Water Vapor Proportion
R(*o)
3
0.056
1 of Saule Points
1
3
Molecular Uaight of Stick Sas, Dry
N(d)
a
29.51
Total Sampling Ti» (sin)
(theti)
196.00
Uet
M(s)
m
28.66
Btroaetric Pressure (in H;>
P(b)
30.01
Stack Pressure, absolute (in Hg)
P(s)
0
30.01
Stack Pressure (in KSOI
P(stack)
-0.01
Average Stack Velocity [ft/sec)
V(s avg)
a
20.4
Gas Meter Initial Reeding (cu ft)
375.7B1
Gas Meter Final Reading (c« ft)
1259.70
Nit Sas Saaple Maluae (cu ft)
V(«)
883,93 >
Vol of Liquid Collected (>i)
Vile)
972.79
Vol of Liq 9 Std. Cords, (scf)
V(a stdi
<5.789
Ut. of Filter Particulate (5a)
0.82
kt. of Probe Hash Particulate (90)
0.63
kt of Coebined Particulate (go)
lip)
1.4500
GZ Concentration (by C3I)
1
7.7
CC2 Concentration (by CEH)
I
7.5
CO Concentration (by CEK)
%
0
N2 Concentration (by diff.)
%
84.80
Saaple ! dClock I Velocity! Orifice
1 Stark
Gas
Meter
SSRTIdP)
FIELD DATA AVERAGES FOR SAMPLE t —
B08020950M17
Point 1 Tias IHead, dP!Meter,dH
! leap
Teas
tdegF)
! (lin) 1(in H20l!(in H20)
! (cegF)
in
out
Velocity Heal Ctc)
dP(avg)
3
0.055
1 ! 4 1 0.055 t 2.B
i 2000
200
130 1 0.2345
Orifice Meter Reading Cue)
dH(avg)
a
2. BOO
0 1 5 ! 0,055 1 2.8
i 2000
200
130
0.2345
0 ! 1B7 1 0.055 ! 2.B
! 2000
210
140
0.2345
Stack Teaperature (deg F)
T Cs avg)
=
5000.0
! ! 1
i
(deg C)
T(s avg)
=
1093.3
— :— 1— 1—
(later Teaperatsre (deg FJ
T(i avn)
¦
168.3
! ! I
!
(deg O
T(a avg)
m
75.7
— i— !— —
— I— 1— 1—
1—
1 ' "
_____
Roct-Mean-Square dP Cms)
SORT (dPi
0.235
TOTALS ! 196 I 0.17 1 8. WOO
: £000.0
£10.0
400.0
0.7036
191
-------
T^r A
ISOKINETIC RESULTS
CALCULATED RESULTS FOR SfltPLE «
E03021015M5
Plant: CRF Updated 12709/B9
Performed by:
JOE MLLS
tote: 08/02/B9 Printed 12/09,'39
Test No./Type:
EC8021015M5
Satple Location: SCRUBBER EXIT
Start/Step Tire:
1015-1233
PARANE1ER
SYMBOL
VALUE
(fair.)
Nozzle Dianeter, Actual {in)
N(d)
0.403
Pilot Tuhe Correction Factcr
C(p)
0.B4
6a5 Deter Correction Factor
(alpha)
1.02
5fc%ck (Duct) Dimensions {in):
Radius (if round)
R
7
Length (if rectangjlar)
L
0
Width (if rectangular)
H
0
Area of Stack (sq ft)
A(s)
(1.06901
1 of Sample Points
I
13
Total Stapling Tiae (ain)
(theta)
141.00
Baroeetric Pressure Cin Hg)
P(bJ
30.01
StJCk Pressure ! in H20I
Plstack)
-0.04
Gas Meter Initial Reading (cu ft)
314.B9B
Gas Meter Final Reading (cu ft)
427.119
Net Gas Sanple Volume (cu ft)
V(a)
( 112.22 )
Vol of Liquid Collected (all
UI (c)
1512.74
Vol of Liq ( Std, Ccnds. (scf)
V(h std)
( 71.205 )
ilt. of Filter Particulate tga)
0.0454
kt. of Probe Uash Particulate (gs!
0.01
Wt of Coffined Particulate tga)
H(p)
( 0.0554
)
G2 Concentration (by CEM)
X
11.7
C02 Concentration (by CEM)
I
5.S
CO Concent rat ion (by CEM)
7.
0
N2 Concentration (by diff.)
7.
{ 33.20 )
Saople 1 dClnck !Velocityi Orifice
1 Stack
I Gas
Hater ISQRT(dP)
Point ! Tine IHead, d?,Meter,CH
1 Teiu
! Teip
(deaF) !
I (sin) (in H20) i (in K2C)
1 (degF)
1 in
i out !
1 ! 2 1 0.IS ! 2.4
! 170
: 120
1 97 1
0.4243
1 r 9 ! 0.1B : 2.4
: 170
! 120
! 97 !
0.4243
2 ! 10 ! 0.1B 1 2.4
! 170
127
! 9B I
0,4243
3 ! 10 ! 0.1B ! 2.4
i 170
! 132
! 100 !
0.4243
4 ; 10 ! 0.1B : 2.4
! 170
: 135
: 104 !
0.4243
5 ! 10 ! 0.IB ! 2.4
: 170
1 133
! 107 :
0.4243
6 : 10 I 0.1B ! 2.4
! 170
1 139
: 109 !
0.4243
7 ! 10 ! 0.1B ! 2.4
! 170
! 140
: no !
0,4243
cvi
CD
o
O
00
: 170
: 140
! 112 :
0.4243
1 ! 10 ! 0.2 ! 2.65
! 170
: 140
: 112 i
0.4472
2 ! 10 ! 0.2 ! 2.65
: 170
! 142
! U3 :
0.4472
3 : 10 ! 0.21 ! 2.8
! 170
144
114 I
0.45B3
4i io i o.2i : :.b
170
i 143
! 115 :
0.4533
5 ! 10 1 0.22 5 2.9
! 170
: 145
i 115 !
0.4690
6 ! 10 : 0.23 ! 3.1
: 170
» ,
: 146
l
i 116 :
> 1 _
0.4796
Isokinetic i ty
ftotei-ed Saaple Gas Volute
Stack Gas Finn, std cond.
std cond.
actual
actual
Particulate Loading, dry
Z I
(scf) Via
(see) V(a
Idscfn) Q(s)
(dsci/ainlOIs)
(acta) Q(a)
(ace/Bin) Q(a)
(gr/dscf) C(s
« 71 02
-------
ISOriNETIC RESULTS
CALCULATED RESLITS FDR 3AKPLE » —
SC8021057M5
Plant: CRF Jpdated 12/09/8?
Ferfcraed by;
SH5R0N Ki <5
Date: CB/02/a? Printed 12/09/8?
Tsst Na./Type:
50302105' 5
lufcineticity
V. I
93.5
Saiple Lccations STACK
Start/Stop Tiae:
1057-120:
Metered Sasple Gas VdIlk tscf)
V(o stc! •
10.47
[sen)
Via std) =
1.144
PARAMETER
SYH30L
VALUE
Stark Gas Flott, std cortd. (dscfa)
Q(s)
loot
(calc.)
std :or.d. ldscr/min)Q(s) =
2a.5
Nazzle Diaaster, Actual (in)
N(d)
0.37S
actual larfn)
Q(d)
175B
Pitot Tube Corfrctiui Factor
Clp)
0.81
actual laci/mn) QUJ =
49.8
Gas feter Corractinn Factor
(alpha)
1.02
Participate Loading, dry (gr/dscf) C(s std) =
0.0080
Stack (Curt) Disensions (in):
e 71 C2tgr/dscf) Cts std) =
0.0121
Radius (if round)
H
7
e 7Z QZIag/dscz) C(i std) -
3
Length (if rectancular)
L
0
Particulate Emission Rate (Ib/hr)
tip) =
0.04?
Width (if rectangular)
U
0
(kg/hr)
E (p)
0.011
Area of Stack (sq ft)
fits)
(I.06701
)
Stack 3as Hater Vapor Proportion
E(ho)
0.319
1 af Saiple Points
1
12
Molecular Height of Stack Sas, Dry
H(d)
27.2S
Total Saopling Tise Uiin)
Ithsta)
( iC.OO )
Wet
M(s)
25. Aii
EaronEtric Pressure (in He)
P(b)
JC.01
Stack Pressure, absoljtc (in Hg)
PI 5)
30.01
Stack Pressure (.n H20I
P(stack)
0.05
Average Stack Velocity (ft/sec)
Vis avgi -
27.4
Sas Meter Initial Reading (cu ft)
352.273
Bas Hater Final Reading (cu ft)
595.511
Net Sas Sample Volume (cu ft)
V(B)
( 43.24
)
Vcl cf Liquid Collected (il) VI(c) 403.1
Vol of Liq 6 Std. Conds. (sell V(h std) ( 18.974 )
Ht. cf Filter Particulate (go) 0.000?
Ht. of ProbE WasJi Particulate 0.02
Ht of Conbinad Particulate (o«) H(pl ( 0.020? )
02 ConcePtration (by CEPIJ I 11.8
C02 Concentration Iby CEM) Z 4.?
CO Concentration (by CEH) T 0
N2 Concentration Iby diff.) I t 63.30 )
Saaple
dClDtk .'Velocity! Orifice
Stack
Sas
flEter
SDRTIdP!
1FIELD DATA AVERAGES FOR SAMPLE t —
S090210S7M5
Point
Tlae 'Head, dPIM*ter,dH
Teap
Teop
(cegF)
1
(¦in) t(in K2Q)',(in H20)
IdegF)
in
out
IVelotity Head
(*HC)
bP(avg)
0.173
1
5 1 0.17 : 1.7
170
103
102
0.4123
I Orifice Meter Reading
CMC)
dHCavg!
=
1.733
2
5 1 0.17 ! 1.7
170
118
I 102
0.4123
1
3
5 1 0,19 ! 1.7
170
124
104
0.4359
(Stack Teaperature
(deg F)
T(5 avg)
=
170,0
4
5 ! 0.19 ! 1.9
170
128
! 105
0.435?
;
(deg D
T(s avg)
_
76.7
5
5 ! 0,17 ! 1.7
170
131
i 108
0.4123
1
6
5 1 0.17 i 1,7
170
132
110
0.4123
IMeter Teaperature
(dig F)
T(g avg)
a
117.4
j
5 1 0.17 1 1.7
170
133
! 112
0.4123
j
(deg CI
T(a avg)
-
43.5
2
5 ! 0.17 ! 1.7
170
133
113
: 0.4123
!
3
5 I 0.17 ! 1.7
170
134
: 114
0.4123
IRoot-Mean-Square &
Cxc)
SQRT(dP)
*
0.422
4
5 ! 0.19 ( 1.7
170
133
: U6
0.4359
I
5
5 0.19 ! 1.7
170
13i
! 117
' 0.4359
!
6
5 : 0.19 i 1.7
170
137
: lis
: 0.4359
J
0
0 ! 0 ! D
0
0
! 0
: 0.0000 1
0
. 0 ! 0 ! 0
0
0
: a
: 0.0000
*
i
0
0 ! 0 ! 0
0 .• ;
0
0
! 0
¦ 0.0000
i
•
*
»
•
1 V t l
:—
1
" '
I
1
1
;
i
S
-i
TOTALS
60
2.14 ! 20.8000 i 2040.0 ! 1544.0 1321.0 1 5.0656 1
193
-------
3
I5CHIJCTIC REEU.TS CALCULATED RESULTS FOR SftKPLE It — A0aO4)037MU7
Plant: CRf Updated Performed byi OWRLY KINS
Datei 1/04/69 Printed 09/02/89
Test Ko./Tyoe: A08041037HX17
lsokineticity
X I
=
101.7
Sanale Location; fFTESBUIPER
Starfc/Stoo Tinrj 1037-1324
Metered Sanole Bas Voluos (scf)
V(n stri)
¦
719.35
(sea)
V(g std)
s
20.370
PflRMETER
SYH3QL
VflUJE
Stack 0£s Flo*, std cond. (dsTfnl
Q(s)
—
604
(caic.)
std cond. (dica/ain)Q(s)
m
17.1
Nozzle Diacptcr, Actual (in)
Nld)
1.43
actual (acfa)
0(a)
3039
Pitot Tube Correction Factor
CId)
0.84
actual (aco/ain)
~ (a)
a
86.1
Eas Meter Correction Factor
(alpha)
1.03
[•articulate Loading, dry (cr/dscf) C(s ltd)
=
0.0621
Stack (Duct) Dlnnsioni (in) i
8 7t D2(gr/dscf) C(e std)
=
0.062S
Radius (if round!
R
9 7* D2(i3/dsca) C(s std)
=
143
Length (if rectangular)
L
20
Particulate Eaiision Rate (lb/hr)
E(0)
=
0.321
Width (if rectangular)
U
12.25
(kg/hrJ
E(p>
a
0.146
Pre* of Stack (sq ft)
fl(s)
(1.70138 )
Stack Gas Uatir Vapor Proportion
B (hd>
a
0.C7S
1 of Saiple Points
1
2
Molecular height of Stack Eas, Dry
Hid)
=
23.53
Total Sainling Tire tain)
(theta)
I 167.00 )
Wet
N(sJ
=
26.66
Baroaetric Pressure (in Hg)
P(b)
29.98
Stack Pressure, absolute (in H;i
P(s)
=
29.97
Stack Pressure (in ffiO)
P (stack)
-0.08
ftveragD Stick Velocity (ft/sec)
VI5 avg)
=
29.6
5k Meter Initial Reading leu ft)
239.706
Sas Meter Final Reading (cu ft)
1079.71
Nat Bis Saiple Voluie (cj ft)
Via)
( 620.01 )
Vol of Liquid Collected (nl)
Vol of Liq 9 Std, Cands. (scf)
lit. of Filter Particulate (ga)
IK. of Praba Hash Particulate (ga)
lit of Coabiried Particulate lga)
VI (c)
V!* std)
HCp)
125*1.02
( 55.027 )
1.612B
1.28
t 2.B92B )
02 Concentration (by CQf) X 7.1
CCS Concentration (by 01) t 7.8
CO Concentration (by CEM) i 0
ME Concentration thy diff.> < t B5.10 )
Suple
Point
dClock
Tin
(¦in)
1 I
2 I
113
»
Saiple :
I-
TDTftLS I
167
Velocityl Orifice
Head, dPIHeta-.iH
(in H20)I(in H2D)
0.06 I
0.06 i
Stack
Teap
(degF)
2000
2000
Gas Meter
Teap (dejF)
in ! cut
SORT(dP)
200 I
Eio:
' i
:
i
120 I 0.244°
132
0,2449
FIELD DflTfi RVERABE9 FDR S3NPLE * -
AOBC41037MI7
Velocity Head
(*»c)
df(svj)
e
0.060
Orifice Hater Reading
(¦nc)
dH(ivg)
a
3.000
Sta:k Teawrature
(deg F)
T(s avg)
=
2000.0
(de; C)
T(s avg)
s
1093.3
Heter Tea^erature
(deg F)
T(a avg)
S
165.5
(deg C)
T(a avg)
=
74.2
Root Hear Square dP
(Sic)
SaRT(dP)
¦
0.24S
1 ( 1 1 1 ¦
0.12 : 6.0000 i 4000.0 I 410.0 : 252.0 ; 0.4895 i
194
\
-------
ISOKINETIC RESLLT5
Plant: CRF Updated
CflLCLUTED SE3U.TS FOR SAWLE II
E0304104CH5
IZ/U7/39 Pgrforned bv:
JOE .iias
Date! 03/04/99 Printed 12/09/B9
Test No./Type:
E0604104015
Satole Location; SCRUBBER EXIT
Start/Step
Tiae:
1040-1236
FASWETER
SM1B0L
VALUE
Icalc.)
Noz:le Dianeter, Actual (in)
Nfd)
0.403
Pi tot Tube Correction Factor
CIpl
0.84
6as Meter Correction Factor
(alpha)
1.32
Stack CXict) Diuensicns (in):
Radius !if round)
R
7
Length (if rectangular)
L
0
Width (if rectangular)
N
0
Area of Sta;k (&q ft)
AI5)
1.06901
1 of Saople Points
«
13
Total Saddling Ti* Inin)
1 the ta)
114,00
Ba.-raetric Pressure (ir. Hg)
P(b>
29,98
Stack Pressure (in-H20)
?lstack)
-0.03
Bas fe:er Initial Reading (cu ft)
427.572
Gas feter Final Reading (cu ft)
539.578
Net Gas Saople Voluw leu ft)
Vln)
: 112.01
I
Vol of Liquid Collected (ill
VI Ic)
1506.12
Vol of Liq ( Std. Cords. Iscf)
VIh ltd)
( 70.9B7 )
Ut. of Filter Particulate Iga)
0.0365
Wt. of Prob? Hash Particulate (gel
0,03
Ut of Combined Particulate (g#)
nip)
1 C.0665 )
02 Concentratim [by CEfD
i
11.9
CC2 Corcoitration (by CEMI
i .
4.9
CO Concentration (by CEfl)
X
0
fC Concentration (by diff.)
i
1 83.20
)
Saaple i dClntk IVelocity! Orifice
! Stack
! Gas
Heter ISQRTldP)
Paint ; Tisi IHead, dPi Meter, dH.
! Teop
1 Teop
(degF) !
! loin) !(in H20)!(in H20!
! (degF)
! in
1 cut :
¦ 4-. A... .. —- —
1 I
2 ;
3 I
4 I
5 !
&:
1 i
2 I
3 !
4 I
5 I
6 :
&:
0.27
0.28
0.28
0.2B
0.28
C.27
0.27
0.28
0.27
0.2E
0.27
0.27
0.27
3.6 ,
3.7
3.7
3.7
3.7
3.6
3.6
3.7
3.4
3.7
3.6
3.6
3.4
170
170
170
170
170
170
170
170
170
170 I
170 !
170 I
170 !
Isukineticity
Retired Saajle Gas Volute
Stack Git Flow, std ccnd.
9td ccrd.
actual
actual
Particulate Loading, dry
X i = 99.4
Iscf) Vln std) = 1C4.«&
(sen) Vln std) = 2.958
;dsrf«i) Qls) ¦ :1I3
(dscra/ir.inlQH) « 31.5
;acfu> Qla) = 2226
iaca/ain) 0(a) ~ 63.0
tgr/dscf) CIs std) = 0.009B
t IX 02:gr/dscf> C(s std) = 0.0151
e 77. 0Z(«9/«!slbI CU s.tc! - 33
Particulate Eaission Rate Clb/hr) Elfil = 0.094
ikg/hr) Elp) = 0.042
Stack 6as Mater Vapor Proportion
Molecular Weijnt of Stack Eas, Dry
Met
Stack Pressure, absolute tin Bg)
Average Stack Velocity (f;/sec)
B(ho1
11(d)
n(s)
Pis)
Vis avg)
0.405
29.24
24.70
29.98
34.7
106 !
123 !
133 1
138 !
141 !
112 !
137:
146 :
147 !
147 1
148 :
>48 :
149 I
93 !
93
79 !
105
1C9 1
112
113
117
118
119
119
120
120
C.5196
0.5292
0.5292
0.5292
0.5292
0.5196
0.5194
0.5292
0.5196
0.5292
0.5196
0.51%
0.5196
IVelocity Head
11
'.Orifice Meter Reading
1
'.Stack Temperature
I
I
iHster Tenperature
t
I
I
iRaot-ftean-Square dP
'mc>
KC)
E0B04IO40N5
dP(avg) = 0.275
dHtavg) « 3.646
deg F!
deg C)
deg F!
deg C)
l"ic)
T(s avg) ¦=
T ts avg) *
T(« a^g) ¦
Tie avg) =
170.0
76.7
123.5
50.9
SQRTIdP) = 0.524
TOTALS ! 114 ! 3.37 ! 47.4000 ! 2210.0 I 1775.0 ! 1437.0 I 6.3122
195
-------
T~s+ 3
ISOKINETIC RESULTS
CALCLIATED RESULTS FOR SAMPLE » —
S09C4110IM5
Plant: CRT Updated 12/09/07
Perforted by: 3. KING
Date: 0B/04/B7 Printed 12/07/89
Test Nc./Type: 503041103MS
Isckineticity
* I
=
105.2
Sample Location: STACK
Start/Stop Tine: 1103-1208
Metered Sample Gas Voluae (scf)
V(ii std)
=
51.45
(sea)
V(m std)
=
1.463
PAfiAfETER
SYMBOL
VAL1£
Stack Gas Flow, std cond. (dscfm!
0(5)
1142
(calc.)
std cond. (dsca/sirlQis)
=
32.3
Nozzle Diameter, Actual (in)
N(d)
0.375
actual (acfa)
D'a)
3
2196
Pitot Tube Correction Factor
Clp)
3.B4
actual (acs/sin)
0(a)
=
62.2
Sas tteter Correction Factor
(alpha)
1.03
Particulate Loading, dry (gr/dscf) C(» std)
=
0.0102
Stack (IXict) Dimensions (in);
8 IX (E(gr/dscf) C(s std)
S
0.0155
Radius (if round)
R
7
£ Tl 02(«g/dsca) C(s std)
=
35
Length (if rectangular)
L
0
Particulate Enission Rate (lb/br)
E(p)
a
0.100
Width (if rectangular)
K
0
Ckg/hr)
E(p)
=
0.045
Area of Stack (sq ft)
A(s)
(1.06901 )
Stack Gas Hater Vapor Proportion
B(ho)
=
0.331
1 of Sasple Points
>
12
Holeajlar Weight of Stack Gai, Dry
M(d)
c
29.22
Total Sampling Tine (sin)
(tbeta)
( 60.00 !
Net
Mis)
s
24.95
Baronetric Pressure (in Hg)
P(b)
29.98
Stack Pressure, absolute (in Hg)
P(s!
I
29.99
Stack Pressure (in H20)
P(stacic)
0.05
Average Stack Velocity (ft/se:)
V (s avg)
m
34.2
Sas Meter Initial Reading (cu ft)
396.696
Eas fleter Final Reading (cu ft)
451.168
Net Gas Sample Voluae leu ft)
Vd)
( 54.47 )
Vol of Liquid Collected (al> VI(c) 675.34
Vol of Liq S Std. Conds. (scf) VIh sfcd) ( 31.738 )
Nt. of Filter Particulate !ga) 0.9141
Wt. of Probe Kasfi Particulate tga) 0.02
Wt of Cosbined Particulate (go) nip) ( 0.0341 )
02 Caicentration (by CEID I 11.6
C02 Concentration (by CEM) I 4.7
CO Concentration (by 31) I 0
N2 Concentration (by diff.) 1 ( Bo.50 )
Saiple
dClock 1 Velocity!
Orifice !
Stack
6as
Meter
SQRTidP! 1FIELD DATA AVERAGES FOR SAHPLE > -
S03041103M5
Point
Ti«e (Head, dP!Heter,dH
Teop
iMp
(degF)
;
(din) Kin H20)i(in H20)
« •
tdegF)
in
out
'.Velocity Head
Chc)
S>(avg)
=
0.270
1
5 ! 0.27 1
2.7
170
101
94
1 1 '1 1
0.5196 iOrifice Pleter Reading
Pwc!
dH(avg)
2.700
2
Z ! 0.27
2.7
170
107
94
1 0.5196 1
3
5 0.27
2.7
170
115
77
! 0,5176 '.Stack Tecperature
(deg F)
T(5 avg)
=
170.0
4
5 ! 0.27
2.7
170
122
100
'. 0.5196 !
(deg C)
T(S avg)
=
76.7
5
5 1 0.27 I
2.7
170
129
103
0.5176 i
6
5 ! 0.27
2.7
170
131
107
1 0.5176 IHeter Teajpraturp
(tteg F)
T(i avgl
=
118.3
1
5 ! 0.27
2.7
170
136
112
1 0.5196 I
(deg 0
T(i avg)
=
47.7
2
5 ! 0.27
2.7
170
13a
114
: 0.5196 ;
3
5 ! 0.27
2.7
170
140
116
! 0.5196 !Root-Mean-Square dP
Chc)
S®lT(dP)
=
0.520
4
5 ! 0.27
2.7
170
140
118
0.5176 !
5 ! 0.27
2.7
170
141
120
1 0.5196 1
6
5 ! 0.27
1 1
l 1
2.7
170
142
122
S 0.5176 ;
• — 1
1 1
Saaple
I
1
t i
l .
i t
i *
» «
i
i i
TOTALS
60 1 3.24
32.4000
2040.0
1542.0
1297.0
! 6.2354 i
196
-------
ISCKINtTiC fESJLTS
Plant: CRF Undated terforaed by: C.KIfG
Date: B/Ol/Bf Printed 03/02/69 Test No./Typei fl080111(flH«!7
Saeale Location! ftfTERJJfffJER Start/Eton Timet 1103-1405
PfiWttETES
SYMBOL
VflLUE
(calc.)
Kc2zle Disaster, Actual iin)
N(d)
1.49
Pitot Tube Correct:or Factor
C(D)
0.B4
6as leter Correction Factor
[alpha)
1.03
Stack (Duct) Diiensicns [in):
Radius (if round)
S
Length (if rectangular)
L
20
Widih (if rectangular)
U
12.25
Area or Stack (sq ft)
fl(s)
(1.70138
1 of Saiale Points
1
2
Total Saapling Ti«e (am)
Itheta)
( 182.00
Baroaetric Pressure (in Hg)
P(b)
30
Stack Pressure (in ISO)
P(stack)
-0.01
Bas Keter Initial Reading (cu ft)
436.91
Gas Meter Final Reading (cu ft)
1372.98
Net Eas Saipli Voluse (cu ft)
Via)
( 936.07
Vol of Liquid Collected (at)
VHc)
891.49
Vol of Liq 1 Std. Ccnds. Iref)
V(m std)
( 41.962
Wt, of Filter Particulat® (ge)
1.51
Ht, of Probe Hash Particulate (g«)
0.43
Ut oc Coabined Particulate (]sl
H(p)
< 1.9400
CflLCUJJra HEEULTS FOfl SAMPLE I
AO 3011103^17
Isckineticity
i I
-
106.4
Metered Saaole Gjs Veluie
(Kf)
Vln std)
=
313.03
(sra)
Via std)
=
S3.195
Stack Gas Flo*, std ccnd.
Idscfa)
Gist
S
£03
std cond.
(risai/rinlGts)
=
17.1
actual
(aefs)
01a)
3
2946
actual
(aca/ain)
Ola)
=
83.4
Particulate Loading, dry
(or/dscf) CIs std)
3
0.0365
8 It (KCqr/dscf) CIs std)
-
0.0368
» It 02(i;/dscc) CIs std)
64
Particulate Emission Rats
!lb/hr)
E(o)
-
0.189
(ItS/hr)
Elp)
S
0,066
Stack Bas Uater Vapor Proportion
B(mo)
s
0.049
Molecular Height of Stack Sm, Dry
K(d)
a
29.50
Met
H(s)
m
2B.94
Stack Pressure, absolute (in Hg)
Pis)
K
30.00
Average Stack Velocity (ft/sec)
Vis avg)
3
28.9
02 Concentration (by CD!) * 7,1
CG2 Concentration (by CEH) i 7.6
CO Concentration (by CEH) t O
N2 Concentration (by diff.) % < 85.30 )
Saaple
Point
dClock
Tiae
(¦inl
IVelxity! Orifice
I Head, dP!Meter, dH
Kin H20)l(in K2DI
Stack
Ten
(degF)
Eas Meter
Trap (degFl
in ! out
33
159
0
TDTKJi !
182
0.C57
0.057
0
2000
2000
0
193 :
134 :
0.2387
Orifice Meter Heading
Cnc)
dHlavg) =
3.000
200 1
143 i
0.2387
0 !
0 !
0.0000
Siaclt Teaperatar*
(dag F)
T(e avg) x
2000.0
o.n i 6.0000: 4000.0: mo: 277.0: 0.4775
SQRT(dP)
FIELD DflTA AVERAGES FOfi SAKPlE « — A08011103MH17
Velocity Head
fuel
dP(avg)
0,057
{deg C! 7(5 avg) = 1093.3
Meter Teaperature
Root-ttean-Square dP
(deq F'.
(deg C)
Cue)
T'a avi)
Tli avg)
SSRT(dP)
1(7.5
75.3
0.239
197
-------
7 es+" y
ISOKINETIC RESULTS
Plant! CftF Updated 12/C9/B9 Performed by: GREG KILL
Dates OB/Ol/B? Printed 12/09/S9 Test Xo./Type: E0BCIM04H5
CALCULATED RE5LLTS FOR SAMPLE K— E0831I104H5
Isnkineticity
7. I
= 100.1
Sasple Lxation: SCRUBBER ECU
Start/Stop Tide:
1104-13!?
Metered Saeple Gas Valuae Ixfl
V(n std)
= 103.40
(sen)
Via std)
= 2.9BI
PARAMETER
SYMBOL
VALUE
Stack Eas Flow, std cand. (dscfa)
Q(s)
1051
(calc.)
std cond. (dscn/aiiilQIsI
29.B
Nozzle Disaster, Actual {in)
N(dJ
0.403
actual (a:fi)
a:ai
= 2074
Pitot Tube Correction Factor
C(p)
0.34
actual (sen/(tin)
B!a)
= 5a. e
Gas neter Correction Factor
(alpha)
1.52
Particulate Leading, dry (gr/dscf) C(s std)
= 0.0226
Stack (Duct) Dinensinns (in):
t U lEfgr/dscf) C(« std)
= 0.0327
Radius (if round)
R
7
? 71 Q2(ii9/(Jsca) C(s std)
75
Length (if rectangular)
L
0
Particulate Eaissim Rate (lb/hr)
E(pl
» C. 204
KidWi (if rKtanjular)
H
0
(kg/hr)
E(p)
= 0.092
Area of Stark (sq ft)
A(s) (1.04901 )
Stack Sas Mater Vapor Propo-tion
BInj)
= C.401
1 of Saeplf Points
1
:i
Kclecular Msight of Stack Gas, Dry
M(d)
= 29.24
Total Stapling Tine Coin)
(tfieta) (
121.00 1
Met
M(s)
= 24.73
Baruaetric Pressure (in Hg)
P(b)
30
Stick Pressure, absolute (in hg)
P(s)
= 30.00
Stack Pressure tin H20)
P(stack)
-0.03
Average Stack Velocity (ft/sec)
V(s Jvg)
= 32.4
Gas Meter Initial Reading leu ftl
200.047
Gas Meter Final Reading (cu ft)
312.0B2
Net Gas Saaple Voluae (cu ft)
V(i)
112.04 )
Vol of Liquid Collected (alt
unci
1499.98
Vol of Liq 8 Std. Conds. (set!
V(N std) ( 70.59?
Mt. of Filter Particulate
-------
1*3+ i
ISOKINETIC RESULTS
CALCULATED RESULTS FOR SAMPLE # —
50801I1S0K5
Plant: CRF Updated 12/09/39
Performed by: SHflKBJ KING
Date! C8/0I/OT Printed 12/09/39
Test No. /Type: SOBOU150M5
Isokineticity
r. i
101.9
Sanple Location: STACK
Start/Stop Time: 1150-1255
stared Sanple Gas Voluae (scf)
Vlfi std) »
46.40
(sea)
Via std) *
1.316
PARAMETER
SYMBOL
VALUE
Stack Gas FIom, std cond. (dscfo)
Qls)
1060
(calc.l
std cord. (dscn/ain)Q(s) »
30.0
Nozzle DiMeter| Actual (in)
N(d)
0.375
actual (acfe)
q(a)
196B
Pitot Tuts Correction Factor
C(p)
0.84
actual (aco/nin)
Ella) *
55.7
6as Meter Correction Factor
(alpha)
1.03
Particulate Leading, dry (gr/dscfl C(s std) =
o.ou:
Stack (Duct) Dinenslons lin):
? 77. D2(gr/dscf!
C(s std) =
0.0160
Radius (if round)
R
7
9 71 D2(ag/dECi) C(s std) *
37
Length (if rectangular)
L
Particulate Eiissicn Rate (lb/hr)
E(p)
0.100
Width (if rectangular)
H
(kg/hr)
E (~)
0.044
Area of Stack (sq ft)
A(s) (1.06901 )
Stack 0as Hater Vapor Proportion
B (ho)
0.3b3
1 of Staple Points
I
12
Molecular Neight of Stack Gas, Dry
Kid)
29.24
Total Samp ling Tina (ninl
(theta) (
60.00 )
Met
H(s)
25.16
Earcaatric Pressure (in Hj)
P(b)
30
Stack Pressure, absolute (in Hq)
Pis)
30.00
Stack Pressure (in H2D)
P(stack)
0.06
Average Stadt Velocity (ft/sec)
Vis avg) =
30.7
5as Meter Initial Reading leu ft)
301.89
Gai Meter Final Reading (cu ft)
350.893
fet Gas Satfla Voluse (cu ft)
Vial (
49.00 )
Vol of Liquid Collected (al)
VI Ic)
562.13
Vcl of Liq S Std. Coids. (scf)
V(m std) ( 26.459 )
Wt. of Filter Particulate Ign)
0.0133
Nt. of Probe Nash Particulate (go)
0.02
Wt of Cccoined Particulate (ga)
Hip) 1 0.0333 )
~2 Concentration (by CEM)
1
11.3
C02 Concentration (by CEM)
I
4.9
CO Concentration (by CEM)
X
0
f<2 Concentration (by diff.)
I (
B2.E0 )
aaqple t dClock '.Velocity! Orifice
! Stack 1
Gas
Meter
SORT(dP)
IFIELL DATA AVERAGES FOR SAMPLE * -
E0801J150MS
" Point ! Tiae IHead, dP!Meter,dH
'¦ Teap
Teap
(degF)
:
1 (ain! : (in H20)! (in H20!
! (degF)
in
out
!Velocity Head Cue)
t
dP(avg) =
0.220
1 ! 5 : 0.22 ! 2.2
: 166
101
94
0.4490
•
lOrlfice Meter Reading Cwc)
dHiavg] «
2.200
2 5 ! 0.22 ! 2.2
! 167
112
97
0.4690
1
1
3 5 ! 0.?2 ! 2.2
: 167
114
106
0.4690
!Stack Teaperature (deg F)
T(s avg) =
164.2
4 1 5 ! 0.22 ! 2.2
i 166
123
104
0.4490
! (deg C)
T(s avg) *
74.5
5 ! 5 i 0.22 S 2.2 ! 164
129
106
0.4690
1
1
6 ! 5 ! 0.22 ! 2.2
! 166
133
107
0,4690
1 Meter Teiperature (deg F)
T(a avg) =
117.B
1 1 5 ! 0.22 ! 2.2
: 166
135
107
0.4690
1 (deg 0
T(a avg) =
47.6
2 ! 5 ! 0.22 ! 2.2
; 166
136
109
0.4690
1
3 1 5 i 0.22 ! 2.2
: 166
138
111
0.4670
IRanfe-Mean-Square dP ("«)
SffiT(dP) =
0.469
1 1 5 1 0.22 ! 2.2
1 166
139
114
0.4490
:
5 ! 5 ! 0.22 : 2.2
! 166
140
115
0.4470
6 3 1 0.22 ! 2.2
l l i
—mmmm 1 _^ i 1
1 " 1 1
166
1
l
1
1 _
1
140
0
116
0.4690
i —1 _
i
1
i
i
»
i
*
•
i
»
TOTALS 1 £0 i' 2.64 1 24.4000
I 1994.0
1540.0
1286.0
5.&2B5
•
*
i
199
-------
I est*
ISOKINETIC RESULTS
CALCULATED KE3ULTS FDR SAMPLE I
A08160313XM17
Plant: CRF lodated
Perforced by:
C.KING
Datei B/16/89 Printed 09/02/e9
Test Nc./Tyaei
A09160913JW17
Isokireticity
* I
=
95.0
Sanple Location: RFTIRBUflNER
Start/StoD Tine:
C913-1300
Ketered 5anp]e Eas Voluse (scf)
V<1 Std)
3
535.19
(sen)
Vtu std)
-
27.838
PttfiWrtEfl
BYfiJQL
VOLUfc
Stack Gas Flow, std cord, (dscfa)
Ois)
=
838
(sale.)
std cord. (dsn/»n)C(s)
z
18.1
Nozzle Diateter, Actual (in)
N(d)
1.48
actual (acfa)
C(a)
=
3460
Pitot Tube Comet ion Factor
CCd)
0.84
actual taca/ain) Ola)
98.0
Gas tfcter Correction Factor
(alpha)
1.03
Particulate Loading, dry (jr/dsef) CIs ctd)
=
0.0306
Stick (Duct) Dimensions (in):
0 7* 02(gr/dscf) C(» std)
=
0.0335
Radius (if roondJ
H
? It 02(ig/dsci) C(s std)
=
77
length (if rectangular)
L
20
Particulate Emission Fata (Ib/hr)
E(s)
0.167
Uidth (if rectangular)
U
12
Ckg^hr)
E(p)
=
0.076
Area of Stack (si) ft)
A Is)
(1.66666
)
Stick Gas Water Vapor Proportion
B(ho)
¦
0.073
1 of Staple Points
1
2
Kolecular Weight of Stack Sas, Dry
H(d)
a
29. W
Total Supling Tin Iain}
(theta)
( 227.00
)
Uet
M(s)
3
26.66
Birwtric Pressure (in Hjl
PCb)
29.96
Stack Pressure, absolute (in Hg)
Pis)
¦
29.97
Stark Presare (in H20)
P(stack)
-o.oa
Rverage Stack Velocity tft/seci
V(s avg)
=.
34.6
6as Meter Initial taadim) (ci ft]
971.073
Gas Meter Final Reading leu ft)
2103.3
Net Gas Staple Value (eti ft)
Via)
(1132.43
)
Vol of Liquid Collected (si)
VI (c)
1MB. 83
Vol of Llq t Std. Conds. Isef)
V(N BtdJ
( 77.610
1
Wt, of Filter Particulate (ga)
1.406
Wt» of Probe Hash Particulate leu)
0.55
Wt of Ccabincd Particulate (gal
M(p)
I 1.9560
)
OS Concentration (fa/ CEM)
i
8.21
COS Corcentration (by UK)
J
7.35
CO Concentration (fay CEKI
i
0
tC Concentration (fay diff.)
i
( S4.U
1
Sa^ile
dClock
Velocity!
Orifice !
Stick !
6as
Meter ISORKdPJ
Point
Tlte
Head, dP!Meter, dH !
Teap 1
Teap
(4ejFl !
(¦in)
(in HS0)!
lin H20) !
IdegFl !
in
! oat 1
1
170
0.075
£.2 1
2200 1
199
1 140 1 0.2739
2
57
0.073 (
2.2 i
2200 i
199
140 1 0.2739
0
0
0 I
0 1
0 1
O
! 0 ! 0.0000
Suple
-+-
Toms
227 \ 0.15
4.4000 : 4400.0
336.0 : 260.0 : 0.5477
FIELD MIA AVERAGES FOR SAMPLE 1 —
A08I60913MMJ7
Velocity Heal
<*NC)
dP(avj)
=
0.075
Orifice Meter Reacing
Cue)
dH(avg)
a
2.200
Stack Teagerature
-------
-fZs*-
ISOKINETIC RESULTS
CALCULATES RESULTS FOR SA.1PLE 1 —
E08160926T15
Plant: CKF Updated 12/07/09
Pei'foro;d by: G.HILL, J
'ILLS
Bate: 08/16/89 Printed 12/09/8?
Test No./Type: E0816092y
:>
Isokineticity
7. [
104.5
Sajple Location: SCRUBBER EXIT
Start/Stop Tiae: 0924-1104
Metered Sjnple Gas Volute (scf)
V(n iUi) =
109.il
(sea)
V(r. std) =
I.0°0
FfiRfllETER
SfllftL
VALUE
S:aci 533 Flow, std cond. (cszfn)
Q(s)
1314
(calc.i
std ennd. (dscn/jiinlQIs) =
37.2
Nozzle Diaaeter, Actual (in)
N(d)
0.403
actual (acfn)
g(a)
2640
Pitnt Tube Correction Factor
C(p)
0.04
actual (aca/ain) Q(a) -
74.7
Gas lleter Correction Factor
(alpha!
1.03
Particulate Loading, dry (gr/dscf) CIs std) =
0.0170
Stack (Duct! Diaensicns (in):
« 77. Q2(gr/dscfI C(s std) =
0.0256
Ridim (if rcu.id)
R
7
6 7S (Kliig/dsral C(s «5td) =
59
Length (if rectangular)
L
Particulate Emission Rate (lb/hr)
E(p)
0.191
Width (if rectangular)
N
(kg/hr)
E(p)
0.0E7
Area of Stack (sq ft)
fl(s) (L.06901 )
Stack Sas Mater Vapor Proportion
3 (NO) =
0.411
1 af Saople Points
•
12
Molecular Weight of Stack Gas, Dry
H(dl =
29.26
Total Sampling Tiae tain)
(thsta) (
96.00 )
Met
(1(5)
24.64
Barcoetric Pressure (in Hg)
P(b)
29.98
Stack Pressure, absolute (in Hg)
P(s)
29.98
Stack Pressure (in H20)
PUtack;
-0.03
Average Stack Velocity (ft/sec)
V(s avg) =
41.2
Gas Meter Initial Reading
t
1
1
1
TOTALS : 96 I 4.65 1 55.8100
! 1992.0
1542.0
1262.0
7.4692
1
201
-------
)is~^ ^
ISOKINETIC RESULTS
Plant: CKF Lpdated 12/09/09 Performed by:
Bite: 08/16/89 Printed 12/09/89 Test No./Type:
Saiole Location: STACK Start/Stop-Tiae:
I.HILLS
S08160926M5
0926-1037
PARAMETER
SVMBQL
VALUE
(calc.)
Nozzle Diaoeter, Actual (in)
N(d)
0.375
Pilot Tube Correction Factor
C(pl
0.S4
Gas fleter Correction Factor
lalpha)
1.01
Stack (Suet) Dimensions (in):
Radius (if round)
a
7
Length (if rectangular)
L
Width (if rectangular)
W
Area of Stack [sq ft)
A(s)
(1.06901 )
1 cf Suple Points
t
12
Total Saapling Tine lain)
(theU)
40.00 )
Barooetric Pressure (in Hg)
Ptb)
29.98
Stack Pressure (in H2C)
P(stacfc)
0.C6
Gas Meter Initial Reading (cu ft)
915.119
Gas Meter Final Reading (cu ft)
971 Bfil
Net Sas Saaple Vol use (cu ft)
Via!
( 60.76 )
Vol of Liquid Collected (¦])
VI (c)
73.6S
Vol of Liq 6 Std. Cords, (scf)
V(* std)
( 34.299 )
Ut. of Filter Particulate Iga)
0.023
Ht. of Probe Wash Particulate
Average Stick Velocity (ft/sec)
B(m)
(1(d)
11 (s)
Pis) =
V(s avq) =
0.376
29.2B
25.04
29.98
40.5
FIELD DATA AVEFA6ES FOR SAfHE «
Velocity Head (*h;]
9)6160926(6
dF(avg) = 0.179
Stack Teiperature
Keter Teaperature
Root-}1ean-Square dP
1212.0 I 7.:
Cue)
(deg F)
ideg C)
(deg F)
(deg C)
Cue)
dH(avg) =
T(s avg) ¦
T(s avg! =
3.641
170.0
76.7
T(a avg) ¦ 114.9
T(« avg) = 46.0
SQTT(dP) = 0.616
202
-------
¦Tift I
ISWINsTIC RESULTS
CALCULATED RESULTS FOR SfiHPLE » —
P081503571017
Plant: CRF Undated
Perforsed by:
C.KING
Dates 3/15/39 Printed 05/02/03
Test No./Type:
fl0S150357(W17
Isokineticity
i I
=
99.2
Sauls Location: flFTER9liflNER
Start/Stoo Tine:
09S7-1400
Metered Sanole 3as VoIum tscf)
Via std!
¦
10G8.71
(sck)
V(e std!
=
30.Ei3
PARAMETER
SVKBOL
VfiLUE
Stack Gas FIon, std cond. (dscfa)
0(5)
=
519
(calc.I
std cond. Cdscn/einHHsl
*
17.5
Nozzle Diaaetsr, Actual (in)
N!d)
1.4a
actual (acfs)
0(a)
=
3233
Pitot Tube Correction Factor
C(3)
0.84
actual !ac«/ain)
QUI
=
91.7
Em Meter Correction Factor
(alpha)
1.03
Particulate Loading, dry (gr/dscf) C(s std)
0.0560
Stack (Duct) Diversions (in):
£ It 02(gr/dscf) C(s std)
=
0.0629
Radius (if round)
R
9 7* D2
3
£9.99
Stack Pressure (in ICO)
P(stack)
-0.08
fiverage Stack Velocity (ft/sec)
Vis avg)
=
32.4
Gas Meter Initial Reading (cu ft)
749.041
Cat Keter Final Reading (cu ft)
1362.51
Net 5u Sanjle Vol urn (cu ft)
V(e)
(1213,48
)
Vol of Liquid Collected (al) VI(c) 2044.61
Vol of Liq i Std. Conds. V(h std) (133. B95 )
Wt. of Filter Particulate (gal 1.473
Wt. of Probe Wash Particulate IgiJ 2.4
Wt of Combined Particulate (gel Hip) I 3.87% )
02 Concentration (by CEHI X B.52
002 Concentration (by UK) % 7.39
CO Conceniration (by CEMI 1 0
« Concentration (by diff.) * (64.10)
Sample
1 dClock
'iVelocity
Orifice
! Stack
Eas
Meter
SORT (dP)
FIELD MTA WERA6ES FD3 SflAPLE * —
A081S09S7RM17
Point
1 Tins
Iriead, eP
Neter,dH
Tnp
Tbko
(decF)
1 (sin)
Kin K20)
(in H20)
1 fdegF)
in
out
Velocity Head
CMC)
dPtavg)
a
0.070
1
i 113
! 0.07
2.2
I 2000
203
120
0.2646
Orifice Meter Reading
(¦*:)
dH(avg)
=
2.200
0
1 130
: o.o7
2.2
2000
203
123
0.2645
0
! 0
: o
0
0
0
0
0.0000
Stack Teeoerature
Ideg F)
Tts avg)
-
2000.0
0
1
1
(deg C)
T(s avg)
st
1093.3
1
•
Meter Temperature
(deg F)
T(e ivj)
3
1BS.3
i
1
—
(deg CI
T(a avg)
=
72.4
1
1
1
1
1
1
Root-Mean-Square dP
("hcI
SORT(dP)
=
0.265
Saiple
1
1
1
i—
«
1
1
TDTKJ
1 243
: o.i4
4.4000
4000.0
406.0
243.0
0.5232
203
-------
~T^±-+- L
ISOKINETIC RESULTS
CALCULATED R-iSJLTS FDR SAMPLE 1 —
EO0151CI4M5
Plant: CRF Updated 12/OT/S7
Perforsed by:
J.KILLS
Date: 03/15W Printed 12/09/39
Test No./Type:
E98J51014MS
liokineticity
7. I
?B.B
Saaple Location; SCRUBBED EXIT
Start/Stop Tine:
1014-1223
Metered Sa*ple 9ai Voljne (scf)
V(« std) *
155.23
(sen!
Via std) •
2.980
PARAMETER
SYN30.
VALUE
Stack Gas Flaw, std cond. (dscfffl)
Q is)
1CS5
(calc.)
std cond. fdsca/iiiniQ
I
204
-------
" 1 6
ISOtCINETIC RESULTS
CALCULATED RESULTS ,-Ofi SAfPLE 1 —
S0815!037M5
Plant: CFF Updated 12/09/39
Perforied by: S.Klhffi
Date: 08/15/fi? Printed 12/09/69
Tes: No./Type: S08I510J7M5
Isokineticitv
X 1
2
100.2
Satple Location: STACK
Start/Stop Tine: 1037-1142
Hetsred Sacple Gas Vcluae (scf)
Via std)
=
4/. 74
(sen)
V(s std)
M
1.332
PARAMETER
SYtlBGL
VALUE
Stack Eas Flw, std cond. (dscfn)
U(s)
=
110S
Icalc.i
Std cond. (Gsc«/ain)fl(s!
=
31.4
Nozzle Diameter, Actual tin)
HCd)
0.375
actual !acfa)
a (a)
=
1974
Pitct Tube Correction Fa:tor
C(p)
0.B4
actual (acn/ain)
QlaJ
=
55.9
Gas Meter Correction Factor
(alpha!
1.01
Particulate Loading, dry (gr/ds:f) C(s std)
=
0.0399
Stack (Euctl Disensions (in):
« n 0/tgr/dscf) C(s std)
=
0.0659
Rajius Cif round)
R
7
£ 71 Q2(fij/dsCB) C(s std)
=
151
Length (if rectangular)
L
Particulate Enicsion Rate (lb/hr)
E(p)
=
0.379
Width 'If rectangular)
•4
(kg/hr)
E(p)
=
0.172
Area of Stack !sq ft)
fl(s)
(1.04901 )
Stack Gas Mater Vapor Proportion
Elwo)
=
0.339
1 of Satple Points
>
12
Molecular Height of Stack Gas, Dry
Hid)
=
29.27
Total Saiplinj Ti«e (tin)
(tteta)
( 60.00 )
Met
Mis)
=
23.45
Barooetric Pressure (in Hg)
Ptb>
30
Stack Pressure, absolute (in Hg)
PCs)
=
30.00
Stack Pressure lin H2D)
PIstack)
0.05
Average Stack Velocity (ft/sec)
V!s avg)
30.0
Eis Metgr Initial Reading (cu ft)
B44.I61
Gas Meter Final Reading leu ft)
914.875
N?t Gas Sanple Voluoe !cu ft)
Via)
( 50.71 )
Vol of Liquid Collected (al)
VI
519.70
Vol of Liq 6 Std. Conds. (scf)
V!m std)
( 24.466 J
Ut. of Filt»r Particulate (gil
0.0135
Nt. of Probe Hash Particulate (gi)
0.11
Ut of CoaMned Particulate tgi)
fl(p)
( C,1235 )
~2 Concentration (by CHI)
y.
12.52
C02 Concentration (by CEM)
1
4.B2
CO Concentration (by CEM)
I
0
N2 Concentration (by diff.)
I
( 82.6b )
Saiple
Foint
i
dClock !Velocity! Orifice
Ti«e IHead, dPINeter.dH
(lin) Kin H2D!! (in H20)
Stack 1
Teap !
(CegF) !
Eas
Teap
in
Hater iSCUMF) {FIELD DATA AVERAGES FOR SAMPLE <
(degF) 1 !
1 out ! 'Velocity Head I'm:}
1
1
5 S 0.25
2.4
164 :
92
: B41
0.L000 iOrifice Meter Reading
(*k=)
2
5 1 0.25
2.4
164 1
107
1 87 *
o.: ;oo i
3
5 ! 0.Z2
2.1
164 i
119
89:
0.-::?0 'Stack Tec^ierature
!deg F)
4
5 1 0.22
2.1
164 !
122
91 !
0.«iW 1
(deg C)
5
5 ! 0.22
2.1
164 !
126
1 95 !
0.^90 1
6
5 1 0.22
2.1
164 !
127
! 97 ;
0,- 590 ifteter Teaperature
(deg F)
1
5 1 0.22
2.1
264 i
129
i ioi !
0.'f?0 1
(deg C)
2
5 ! 0.22
2.1
164 1
130
I 103 I
0.- 590 :
3
S ! 0.22
2.1
164 1
132
; 1051
0, '490 IRoot-lfean-Square dP
Cue)
4
5 1 0.22
2.1
:64 1
133
1 106 !
O.'otO 1
3
5 1 0.22
2.1
164 1
134
! 107 1
0. i90 !
6
5 i 0.22
2.1
164 1
135
: 107:
0. j90 '
Saaple
-4-
10TALS !
60
2.70 i 25.80CO 1966.0 i 14B6.0 ! 1172,0
dPIavg) =
dHlavq) =
T(s avg) =
T(s a»()) =
TI» dvg) =
T (« avg) =
EQHr(dP) =
C. 225
2. ISO
164.0
73.?
110.8
43.B
0.474
5,-904 i
205
-------
ISOKINETIC R31/JS CALCULATED RESULTS FOR SAM3LE # — A0ftO9i025M17
Plant: CRF Lfodaied Perforwd by! C.KING
Date! fl/09/89 Printed 09/02/63
Test No./
Type:
A08091025IW17
Isakineticity
i I
=
90.6
Saiole Location: HFTERBURNER
Start/Stop Tire:
1025-1330
Metered Sanple Gas Voluae
(scf)
Vis std)
a
672.59
(sen)
V(« std)
=
19.049
PARAMETER
SYKB0L
VALUE
Stark Gas Flow, std cond.
(dscfn)
Ots)
=
610
Icalc.)
std cond.
(dsan/ainlQIs)
3
17.3
Naizle Diawter, Actual (in)
N(d)
1.46
actual
(acfa)
3(a)
S
2950
Pitot Tube Correction Factor
C(o)
0.84
actual
(acn/ain)
~ (a)
=
63.5
6as Meter Correction Factor
(alpha)
1.03
Particulate Loading, dry
(gr/dscf)
C(i std)
a
0.0423
Stack (Duct) Dinensions (in)¦
(• 7% G2(gr/dscf) Els std)
3
0.0442
Radius (if roindl
R
9 7t 02(»g/dsco)
C(s std)
=
101
Length !if rectangular)
L
20
Particulate Emission Rate
(lb/hr)
E(g)
=
0.221
Width (if rectangular)
U
15
fkg/hr)
Elp)
=
0.100
Area of Stack (sq ft!
fl(s)
(1.6666b
)
Stack Gas Nate- Vapor Proportion
B(*o)
B
0.042
» of Saaple Points
1
3
Molecular Height of Stack Gas, Dry
Mid)
=
29.56
Total Saipling Tine (sin)
(theta)
( 170,00
)
Uet
Mis)
V
29.07
Barometric Pressure (in Hg)
P(b)
30.1
Stack Pressure, absolute tin Hg)
P(s)
3
30.09
Stcch Pressure (in H2D)
PI stark)
-O.C8
Average Stack Velocity (ft/sec)
VIg avg)
=
29.5
Sas Meter Initial Reading (cu ft)
61.334
Bas Meter Final Reading (cti ft)
BOI.B34
Net Gas Saapls VoIuk (c
-------
ISOKINETIC RESULTS
Plait: CFF Updated 12/09/S9 Fe-fon»ed by: J MILLS
Dike: 03/09/69 Prinked 12/09/89 Test No./Type: E08MIQ23H5
Sanple Location: SCSL3BER EXIT Start/Step Tire: 1025-17.46
PARAMETER 5VNML VALUE
Icalc.)
Ko;:le Diaieter, Actual tinl N(d) 0.403
Pitat Tube Correction Factor C(p) 0.04
Gas Meter Correction Factor (alpha) 1.02
Stack (Diet) Dimensions (in)!
Radius (if round) R 7
Length (if rectangular) L
Width (if rectangular) W
Area of Stack !sq ft) AIs) (1.0o901 )
I of SaJtpli Paints I 12
Total Sampling Tite (rain) Itheta) ( 123.30 )
Barooetric Pressure (in Hg) Pib) 30.1
Stack Pressure (in H2Q) PlstacO —0.03
Eas Meter Initial Reading (cu ft) 540.105
Gas Meter Final Spacing Icl ft) 655.5B5
Net Gas Staple Vclune (cu ft) V(n) ( 113.40 I
CALCULATED RESULTS FOR SAffLE II — E0BC"?lCl25fC
Isokinetic:ty
x :
100.2
Metered Saaple Gas V'aluae
(scf)
V(o std) =
108.92
(sen)
V(o std) =
3.064
Stack Gas Flex, std CJnd.
(dacfci!
0(51
1046
std cond.
(dsc«/nin)Q(s) -
29.6
actual
(acfi)
0(d)
2049
actual
(aco/nir.)
Ola)
58.0
Particulate Loading, dry
(gr/dscf)
C(s std) =
0.0107
S 77. D2(gr/dscf;
C(s std) =
0.CL53
e n 02(eg/dsci) C(s std) -
36
Particulate Enissior, Rate
(lb/iir)
E(pl =
0.096
(kg/t»r)
E(p)
0.044
Stack Gas kater Vapor Proportion
B(no) =
0.395
Mjlecular Keight of Stack 6as, Dry
Mid)
Z9.30
Net
MSs)
24. B4
Stack Pressure, absolute (in Hgi
Pis)
30.1C
Average Stack Velocity (ft/sc:)
Vis ayg) ¦
32. C
Vol 3f Liquid Collected l«l) Vl!c) 1503.35
Vol of Liq G Std. Cords, (scf) Viw std) ( !
Ut. of Filter Particulate (go) 0.06S8
Ut. of Probs Nash Particulate Cgn) 0,01
Wt of Combined Particulate (gal M(p) ( 0.075B 1
02 Concentration Cty CEM) I 11.48
C02 Concentration (by CEM) % 5.16
CD Concentration Iby CEH) X 0
N2 Concentration (by diff.) '!¦ ( 33.26 )
5anple
dClcck !Velocity
Orifici
Stick
Gas
Meter
SSFT(dP) [FIELD DATA AVERAGES FOR SAIPLE i -
508091029B
Point
Tife IHead, dPIMeter,dH
Tpap
Teop
(degF)
!
loin! !(in H2D!
(in H2D)
(oegF)
in
out
•Velocity Head
•
(V)
dPIavg) s
0.235
1
10 : 0.24
3.24
170
39
83
0.4B99 iOrifice Meter Resting
<"kc)
dKavg) =
1.169
2
10.5 : 0.24
3.24
170
118
86
0.4899 i
3
1D.5 ! 0.24
3.24
170
127
93
3,4099 iStack Teeperature
(deg F)
T(s avq! =
170.0
4
10.5 i 0,23
3.37
170
132
90
¦D.5(iOO !
(deg C)
Tts avg) =
76.7
5
10.5 ! 0.24
3.24
! 170
136
105
3.4899 1
6
10.5 ! 0.23
XI
i 170
141
107
3.4796 !Meter Teeperature
Idey F)
T(a avgl =
118.3
1
10.3 ! 0.23
3.1
1 170
139
111
ii.4796 !
(dag 0
T(a avg) =
47.9
2
10.3 ! 0.23
3.1
! 170
140
112
0.4796 !
3
10.5 : 0.23
3.1
! 170
140
113
0.4796 IRoot-Naar-Square dP
1 %c)
SQRTId?) =
0.485
4
10.5 ! 0.23
3.1
! 170
141
114
0.4796 !
5
10.5 I 0.23
3.1
! 170
142
114
0.4796 !
6
10.5 i 0.23
3.1
.
! 170
1
»
142
115
0.4796 !
t
TOTALS
125.5 ! 2.82
33.0300
: 20
-------
ISOKINETIC RESULTS
CALCULATED RESULTS FDR SSKPLE « — E03OT1030PE
Plant: CKF Ubdateri 12/09/89
Feroroed by: S.KJN3
Date: 08/09/99 Printed 12/09/89
Test No./Type: S0809103CM5
Isofcineticity t I
=
105.4
Saaple location: STACK
Start/Stop Tiae: 1050-1145
Me tared Saqile Gas Valune (scf) V(a std!
9
<8.11
(sen) Via std)
8
1.342
PAfi«£TEJ»
SYMBOL
VALUE
Stack Gas FIoh, std ccnd. (dscfn) 0(s)
=
1041
(calc.)
std ccnd. (dsci/ainlOis)
=
30.0
Nozzle Diameter, Actual (in)
N(d)
0.175
actual iacfi) 0(a)
¦
2070
Pi tot Tube Correction Factor
Clp)
o.e<
actual (aco/ain) C(al
zz
28.6
Gas Meter Correction Factor
(alpha)
1.02
Particulate Loading, cry fgr/dsci! C(s, std)
-
o.coa:
Stack (Duct) intensions (in):
0 77. C2(gr/dscf) C(s std)
S
0.0123
Radius (if round)
fi
7
6 71 02(ec/dsci) C(s std)
=
28
Length (if rectangular)
L
Particulate Emission Rate (lb/hr! Elp)
=
0.073
Width (if rectanaular)
U
(kj/hr! El p)
=
0.033
Ares of Stack (sq ft!
A!s)
(1.06901 )
Stack Eas kater Vacor 'mcortion B-nc)
=
0.392
Total Sampling Tice (aim
(theta)
( £0.00 )
Uet M(5)
24.ea
Baronctric Pressure (in Hy)
P(b)
. J0.1
Stack Pressure, absolute (in Hg! Pis)
=
30.10
Stack Pressure (in H20)
Plstact!
0.C6
Average Stack Velocity (ft/sec! V(a avg)
=
32.3
Gas Meter Initial Reading leu ft!
5R2.239
Gas Peter Final Reading (cu ft!
632.120
Net Sas Saaple Vjluae (cu ft)
Via)
( 49.67 !
Vol uf Liquid Collected <«U
VI (cl
659.44
Vol of Llq ! Std. Conds. iscfi
'/Cm std!
( 11.040 1
Wt. of Filter Particulate Cjib)
0.0152
Ut. of Probe Hash Particulate tea)
0.0!
Wt cf Coabined Parti:ulate 1 FIELD DATA AVERAGES FOR SATPLE « —
S06C91030N5
Point
Tiee '.Head, dP!tl»ter,dH
Teip
Teap
(degn
1 !
tain) '.(in H20M
!in H20)
(liegF)
in
3u;
: {Velocity Head
Cnc!
JPiavg) =
0.240
1
5 0.24 !
2.2
173
09
85
1 0.4899 'Orifics Meter Reading
Cue!
dH(avg) =
2.200
2
: 5 I 0.24 !
2.2
170
101
96
! 0.4899 !
3
5 ! 0.24 !
2.2
170
107
86
1 0.4399 IStack Temperature
(deg F!
T(s avg! =
170.0
4-
5 ! 0.24 !
2.2
170
109
89
i C.4899 1
(deg C)
T(s avg) =
76.7
5
5 ! 0.24 :
2.2
170
Ui
71
i C.4B99 !
6
5 ! 0.24 1
2.2
170
115
93
! C.4B99 INeter Temperature
ideg F)
T(» avg) =
104.6
1
5 ! 0,24 !
2.2
170
ne
96
! 0.4B99 i
ideg C)
T(i avg! =
40.3
2
I 1 1 0.24
2.2
170
:22
9e
1 C.4899 1
2
4 : 0.24 !
2.2
170
118
90
! 0.4899 IRoot-Kean-Square dP
Cur)
sqKT(dP) =
0.490
T
! 3 ! 0,24
2.2
170
123
100
0.4899 !
4
5 ! 0.24
2.2
17C
124
101
! 0.4899 !
5
! 5 ! 0.24
2.2
170
125
103
! 0.4899 !
6
5 ! 3.24 !
i "" " "" " 1 "" i
1 I
2.2
17C
126
103
S 0.4B9?
1 1
1 1
• 1
TOTALS
: AO i 3.12
26.6010
2210.0
14GB. 0
1231.0
6.3687 !
208
-------
TZ6-t g
ISOKINETIC RSULTS
CfiLCULPTcE RESULTS FOR SAMPLE » —
PM11C330K.*;7
Plant: CRF Undated
Perforied byl C.K1KS
Date: flVi:\B3 Printed 0S/02/69
Test No./Tyw: flOflll0830WI7
Isokire;:city
* I
= 101.5
Sarnie Location: ftFTERSUSNER
Start/StoD Tisei 0830-I230
Metered Sjpale Bas Volune
(scf J
Via std)
= 838.07
(swl
V(a std)
= 23.732
PfiR#£TER
SVHBOL
VALUE
Stack £.13 Flo*, std rord.
(dscfn)
Q(s)
4BO
(calc.1
std cord.
(dsca/ninlDls)
= 13.6
Nozzle Diaieter, Actual (in)
N(d)
1.49
actual
(acfaJ
11(a)
= 8432
Pltot Tube Correction Factor
C(s)
0.34
actual
(acs/tiinj 0(a)
= 52.9
Sas Meter Correction Factor
(alpha)
1.0J
Particulate Lcadinn, dry
(gr/dacf) CIs ltd)
» 0.04(7
Sack (Duct! Dlasrmicna (in):
» 7t D2(gr/dscf) C(s std)
» 0.0507
Radius (if round)
R
8 7< DS(ag/dsca) CIs std)
116
Length lif rectangular!
L
20
Particulate Enissior Rate
(lb/hr)
E(p)
« 0.192
Width (if rectangular)
U
12
(kg.'hr)
E(p)
S O.OE7
Area of 9tack (sc ft)
A(s)
(I.&6666 )
Stack Gas Water Vapor Proportion
B(wo)
• 0,083
< of Saaple Points
1
1
Molecular Weight of Stack Gas, Dry
NId)
= 29.S3
Total Saspling Tiae (Bin)
(tbeta)
I 240.00 )
Wet
H(sJ
« 23.57
Baroaetric Pressure (in Hg)
P(b)
30.02
Stack Pressure, absolute (in Hg)
Pis)
= 3C.01
Stack Pressure (in HSQ)
PUtack)
-0.06
Average Stack Velocity (ft/sec)
Vis avg)
= 24.3
Bas Meter Initial fading (cu ft)
803. S32
Sas Heter Final Heading (cu ft)
1743.43
Net Gas Saaple Volw (cu ft)
Vial
( 939.50 )
Mil of Liquid Collected (el) VKrl ISM. 57
Vol cf Liq 9 Std. C*
-------
l7s-h &
ISOKINETIC RESULTS
CALCLLATED RE3U.T3 FOR SAIFLE 1 — E08U03321S
Plant: CRF Updated 12/07/89
Performed by: J MILLS
Date: Ofl/I1/89 Printed 12/09/87
Test No./Type: E03110832M5
Isokinetic!ty 7. I
103.2
SaaplB Location: SCSUaSER EXIT
Start/Stop Tine: 0032-1030.S
Metered Sample Eas Vcluoe (scf) V(c std)
=
106.15
(sea) V;» std)
=
3.006
PflRfiMETER
SYK3QL
VALUE
Stack Gas Flow, std cond. (dscfa! Q!s)
=
1076
icalc.)
std cond. (dscn/ninJQlsl
30.5
Norzle Oia«eter, Actual (in!
Nfd)
0.403
actual (acfsi) Q(a)
=
2144
Pitct Tube Correction Factor
Clp)
0.84
actual (acm/jiin) 9(a)
=
61.7
Gas Meter Correction Factcr
(alpha)
1.02
Particulate Loading, dry (gr/dscf) CIs std)
=
0.0230
Stack IDjct) Dleensions (in):
§ 77. (Klgr/dscf) CIs std)
=
0.0353
Radius lif roundI
R
7
§ 71 D2(»g/dsca) CIs std)
3
El
Length (if rectangular)
L
0
Particulate Emission Rate (lb/hr) E(p)
=
C.212
Uidtti (if rectangular)
U
0
(kg/hr) E(p)
=
C.096
Area of Stack Isq ft)
fl(s)
(1.06901 )
Stack Eas Water Vapsr Proportion Blue)
=
0.4C3
1 of Saaple Points
1
13
Molecular Weight of Stack Sas, Dry Mid)
=
29.27
Total Saipiinj Tine lain)
(thata)
( 115.50 )
Met n<5)
V
24.72
BaraMtri: Pressure tin Hg)
P(b)
30.02
Stack Pressure, absolute (in Hg) P(s)
=
30.02
Stark Pressure (in H2Q)
P(stack)
-0.04
Average Stack Velocity (ft/sec) Vis avj)
=
33.4
Gas Meter Initial Reading leu ft)
657.451
Sas Mete* Final Reading (cu ft)
769.455
Net Gas Sanjle Valuae !cu ft)
V(n)
( 112.00 )
Vol of Liquid Collected (fill
VI (c)
1524.43
Vol of Lie i Std. Conds. (scf!
V(m std)
( 71.755 )
Ut. aJ Filter Particulate (on)
0.0492
Mt. of Probe Nash Particulate (go)
0.11
Ut of Contained Particulate !ga)
Mp)
( 0.1562 )
02 Concentration (by CEH)
I
11. BB
CD2 Concentration (by CEH)
X
4.97
CD Coice.it'-atior (by CEH)
1
0
N2 Concentration (by diff.)
I
( 83.15 )
Satple
dClock
IVslocity! Orifice
Stack !
6as
Heter
SORT(dP) IFIELD DATA AVERAGES FOR SAfPLE 1 -
E09110832K5
Point
Tine
IHaad, dP!lieter,dH
Ten 1
Teap
(degF)
2
(sin)
Kin H2G)Min H20!
(deoF) !
in
out
!Velocity Head
("HC)
dP(avg)
-
0.255
1
9.5
! 0.27
3.63
170 :
90
81
! 0.5196 JDrifice Heter Reading
<"wc)
cH(avg)
=
3.44E
2
9.5
! 0.27
3.65
170 !
117
85
1 0.5196 1
3
9.5
! 0.27
3.65
170 !
123
88
; 0.5196 'Stack Teaperature
(deg F)
T!s avg)
«
170.0
4
9.5
1 0.27
3.65
170 I
129
94
! 0.5196 !
(deg 0
Tls avg)
=
76.7
5
9.5
! 0.26
3.51
170 !
132
9V
! 0.5099 !
6
9.5
I 0.26
3.51
170 :
134
102
! O.5099 !Meter Tesperature
(deg F)
Tin aval
=
114.7
1
9,5
I 0.26
3.51
170 1
123
103
! 0.5099 !
(deg 0
Tic avg)
=
4b. 0
2
9.5
: 0.25
j. 37
170 1
137
106
: o.5000 :
3
9.5
: 0.25
3.37
170 :
137
108
! 0.5000 1 Root-fear,-Square dP
t'Kl
SORT(CP)
¦
C. 505
4
9.5
: 0,24
3.24
170 5
138
109
1 0.4999 i
5
9.5
! 0.24
3.24
170 !
138
111
! 0.4399 !
6
! 9.5
: 0.24
3.24
170 1
139
111
1 0.4399 !
6
1.3
l __M#
: 0.24
3.24
170 !
138
111
I 0.4899 1
1 t
1 —™"
• —
¦
1
1 I
1 1
i I
TOTALS
115.5 : 3.32 44,8300 i 2210.0 ! 1675.0 1308.0 ! 6.567B
213
-------
TZz-t $
ISOKINETIC RESULTS
CALCULATED RiSULTS FOR £,WLE 1 —
S08110B37
Pi ant: CflF Updated 12/09/39
Performed by: B.I11LL
Dates 08/I1/B9 Printed 12/09/39
Test to./Type: 308110837
Isokinetic!t/
X I
99.7
Saiple Location: STACK
Sta-t/Stop Tire: CS37-0940
Metered Sanple 6as Volure (scf)
V(n s;d) =
4B.G9
(sea)
Vt« Sid) =
1.362
tARAt£TER
SYMBOL
VALUE
Stack Gas Flow, std cone, (dscfm;
0(5)
1)21
icalc.)
std cond. (csc«/air.l0(s) =
31.S
Noizle Diameter, Actual (in)
N(dl
0..S/5
actual (acful
0(a)
2140
PitDt Tube Corre:tion Factor
C(p;
0.B4
actual (ac«/nin!
Ola)
60.6
Gas Keter Correction Factor
(alpha)
1.02
Particulate Loading, dry (gr/dscf) Cts std) *
0.0121
Stick (Duct) Divisions (in):
0 77, 02(gr/Cscf) C(s std) =
0,0195
Radius (if round)
R
7
8 71 02(sg/dscii) C(s std) =
45
Length (if reUangiilar)
L
Particulate Emission Rate (lb/hr)
E(p)
O.lli
Width (if rectangular)
W
(kg/hr)
E(p)
0.353
Area of alack Isq ft!
A(s; (1.C6901 )
Stack Gas Water Vapor Proportion
B(ko1
0,377
I of Baaple Paints
~
12
Molecular Weight of Stack Sas, Dry
N(d) =
29.29
Total Sailing Tine (ginl
(thetal (
60. HI )
Uet
Mis!
25,03
Baroaetric Pressure (in Hg)
P!b)
30.52
Stack Pressure, absolute (in Ho)
P(s)
30.02
Stack Pressure (in H2DJ
P(stack)
0.06
Average Stack Velocity (ft/sec)
Vts avg) =
33.4
6as lister Initial Rsadinj (cu ft)
£32,241
Gas Meter Final Reading (cu ft!
6B2.6B2
Net Gas Saiiale Volute (cJ ft)
Vl«] (
50,12 )
Vol of Liquid Collected (si)
VII c!
617.75
Vol of Lie S Std. Conds. (scf)
V(« std) ( 29.077 )
Wt. of Filter Particulate (git)
0.0077
Ht. of Probe Hash Particulate )gn)
O.OJ
Wt of Cocbined Particulate (go)
N(p) ( 0.0377 )
C2 Concentration (by CEfl)
I
12.33
CQ2 Concentration (by CEN)
1
4.97
CO Concentration (by CEfD
I
0
N2 Concentration (by diff.)
X
82.70 ;
Saople ; dClock {Velocity! Orifice
! Stack
Gas
Heter !SCRT(dP)
IF1ELD DATA AVERAGES FDR SAMPLE 1 -
S08110S37
Paint ! Tise '-Head, c'PIMeter.dH
1 Tetp
Te»p
(degF)
1
1
! (Din) Kin H2C)!(in H2QI
: (dejFI
in
DUt
!Velo;ity Head ("ncl
dP(avg) ¦
0.258
1 ! 5 ! 0,2£ ! 2.(1
! 170
B9
39
0.5C97
IDrifice Heter Reading ("«;)
dHlavg) «
2.375
2 ! S I 0,24 ! 2.4
1 170
92
90
o.:o9?
1
3 i S : 0.26 : 2.4
! 170
115
92
0.5099
[Stack Teeperature (deg F)
T (s avg) =
17C.0
4 1 5 0.26 ! 2.4
1 170
121
93
0.5097
I (deg 0
T(s avg) ¦
76.7
5 ! 5 1 0.2i 2.4
170
125
95
0.5099
1
6 ! 5 1 0.24 ! 2.4
! 170
126
99
0.5099
!Meter Teeaerature (Jeg F)
T(« avg) =
109.6
1 1 5 1 0.2f> ! 2.4
: 170
124
97
0.5099
! (deg C)
T(» avg) =
43.1
1 ! 5 : 0.26 1 2.4
1 170
131
100
0.5-599
1
3 i 5 ! 0.24 ! 2.4
! 170
133
102
0.5099 iRoot-Nean-Square dP l"*c)
SERT(dF) =
C.507
4 ! 5 ! 0.25 ! 2.J
! 170
134
102
0,5000
I
5 ! 5 ! 0.25 ! 2.3
! 170
136
103
0.5000
!
6 ! 5 1 0.23 ! 2.3
* ! "L-' {"¦ ¦ !
-- ! »
(.-n_» t mmm (
170
136
104
" 1
0.5000
"
i
«
i
«
i
i
•
i
TOTALS ! 40 1 3.09 ! 28.5000
1 2040.0
1464.0
1166.0
6.C«91
'i
•
i
211
-------
¦TU+ ?
ISOKINETIC RESULTS
W-CJLflTEP RESULTS FOR SrfflRE 1 —
A07281234WI!7
PI ant 1 CRr Undated
Parforsed by!
CHflRLY KINS
Data: 07/28/83 Printed 03/02/59
Test Nc./Tyoe:
P0728l234tS17
Iso'«ireticity
< I
»
35.4
Saigle Location! fiF7ER8URJi':R
Start/Stoo Tire:
1234-1639
fleterpd Emd1s Gat Voluae tc-f)
V(n std)
=
336.95
(set)
V(s std!
=
15.205
PARAKETER
svkbol
Vffi.DE
Stack En Flow, std cond. tdscfn)
0(s)
=
553
(calc.)
std con). [ssci/oirilCIs)
15.7
Ngule Oiaeeter, fclaal (:n)
N(d)
1.49
actual (aefs)
Dial
-
2771
Pi tot Tube Correction Factor
C(o)
0,84
actual (actr/min) C(a)
a
78.5
Sis fcter Corrsctlon Fsctor
(alpha)
1.03
Particulate Loading, Cry (pr/dscf) C(s std)
=
0.0509
Stack (Duct) Di Mrs ions (in):
B 7i 02(gr/dscf) C(s std)
=
0.(55?
- Radius iif round)
R
0 7* 02(Bg/dsra) C(s std)
s
12b
Length (if rectangular)
L
20
Particulate Emission Rate (lb/he)
E(o)
=
0.241
Width Iif rectangular)
W
12.25
(kg/hrj
E(p]
=
O.109
Rrea of Stack (sg ft)
A(s)
(1.70138
)
Stack Gas Water Vapor Proportion
B(ho)
s
0.072
1 of Siipli Points
1
3
Molecular Weight of Stark Gas, Dry
N(d)
=
29.52
Total Supling Tin (mini
ithetal
< 145.00
)
Hat
M(s)
=
28. £.9
Baroaetric Pressure (in Hg)
P(t)
30
Stack Pressure, absolute (in Hg)
P(s)
=
30. CO
Stack Pressure (in K3))
P:sta;k)
-0.01
Overage Stalk Velocity (ft/sec)
Vis avg)
=
27.1
Bas Neter Initial Readino (cu ft)
B12.475
fus Heler Final Reading (cu ft!
HIE. 9
Nat Gas Saiple Voluae (cu ft)
.'(«)
( E23.43
)
Vol of Liquid Collected (si)
VII;)
891.49
Vol of Liq 9 Std. Conds. (scf)
V(* std)
( 41.562
)
Ut. of Filter Particulate (get)
1.28
Ift. of Probe Wash Particulate (gs)
0.49
Ut of Combined Particulate (9*1
Mpl
( 1.7700
)
32 Concentration (by CEK) X S. 1
CD? Concentration (by CEH) I 7.5
CO Concentration (by CEH) J 0
N2 Concentration (by diff.) X ( B4.40 )
dClock
Tin
(¦in)
1 t
0.05 !
3 !
2000 !
205
45 :
0,05 :
3 1
2000 i
eo4
99 !
0.05 i
3 1
2000;
205
TOTALS !
us
Velocity
Head, dP
(in H20)
Orifice ! Stack
Meter, ifH ! Teop
(in )£fl) ! idegF)
GdS Ifeter SERTIdP) (FIELD M7A DVERflKS FOR SAMPLE I -
Teap tdBjF) ! !
fl072B123M«17
oat
!Velocity Head
150 I 0.2236 1 Orifice teter Raiding
146
153
0.2236 I
0.223S !Stack Tsaoeraturs
Meter Tenperature
Rcot-Meair-Sqnare dP
0.15 I 3.0000 ! 6000.0 ! 614.0 1 <51.0 I 0.6708
Cue)
dP(avg)
CMC)
dHllvg)
(deg F]
T<3 avg)
(deg D)
T(s avg)
(deg F)
"(1 avg!
(dec :i
T(a avg!
Cnc)
SQRT(dP)
0.050
3.000
2000.0
1093.3
177.5
BO. 8
0.224
2",2
-------
tc-S-r- 7
ISOKINETIC RESATS
CALCULATED RESULTS FOR SAMPLE « —
E07231234M5
Plant: CRF" Updated 12/07/89
Performed by: J.MILLS
Date: 07/26/99 Printed 12/09/89
Test No./Type: EC728t2J:
•3
isokineticity
X I
97.3
Sauie Location: 3CRLT3KR EXIT
Start/Btop Tine:
1234-160:
Metered Sanple Gas Valine (scf)
V(e stdl =
103.29
tscml
V(i std) =
2.925
PARAMETER
SYKBCL
VALUE
Stack Gas Flow, std cond. (dscfn)
Qls)
696
Ccalc.
std cand. idsra/flin)0(s! -
25.4
Nozzle Diaaeter, Actual (in)
N(d)
0.403
actual !acfa!
0(a)
•74!
Pilot Tube Correction Factor
C(p)
0.84
actual (acm/ciin)
Q(a)
49.3
Gas Meter Correction Factor
(alpha)
1.02
Particulate Loading, dry (gr/dscf! C(s std) =
0.01S3
Stack (Duet) Dimensions (in):
€ 77. 02(gr/dscf> C(s std) =
0.0273
Radius (if round)
R
7
£ IX D2(ng/d5cn) C(s std) =
62
Length (if rectangular)
L
0
Particulate Eaission Rate tlb/,ir)
E(p)
0.141
Uidth (if rectangular)
H
0
(kg/hrl
E(p)
0.064
Area of Stack
M(p) ( 0.1225 )
D2 Concentration (by CEM)
I
11.6
C02 Concentration (by CEM)
'L
4.9
CO Concentration (ay CEM)
1
0
Concentration (by diff.)
I
B3.60 J
Saaple dClcck 1 Velocity! Orifice
I Stack
Gas
Meter
¦CRT(dF)
! FIELD EATA AVERAES FOR SAMPLE » -
E07281234M5
Paint 1 Tice IHead, dP!Meter,dH
! Teip
Teop
CdeoF)
!
! (ain) !(in K20)'(in H20)
! (degF)
in
out
¦ Velocity Head Cue)
dPIavgi =
0.170
1 : 1 ; 0.17 ! 2.3
166
116
103
3.4123
1
IDrifice Meter Reading Cue)
ifrilavg) =
2.300
1 ! 13 ! 0.17 I 2.3
! 166
116
103
0.4123
1
2 ! 15 C.17 ! 2.3
166
131
104
0.4123
IStatk Taaperature (deg F)
TIs avg) =
166.0
3 : 15 : 0.17 ! 2.3
! 166
141
107
0.4123
! (deg C)
lis avg) =
74.4
4 : 15 : 0.17 ! 2.3
! 166
148
117
0.4123
1
5 ! 15 ! 0.17 ! 2.3
! 166
152
122
0.4123
IMeter Teoperature (dig F)
T(a avg) =
12S.6
6 ! 15 1 0.17 i 2.3
! 166
154
125
0.4123
! (deg C)
TIs ivo) =
53.7
1 1 19 1 0.17 ! 2.3
166
140
124
0.4123
;
1 ! 15 ; 0.17 : 2.3
! 166
158
127
0.4123 'iRoot-Mear-Sq'Jiire dP ("nc!
SQSTldPl =
0.412
2 : 19 1 0.17 ! 2.3
¦1 ! t " ' ' "™
1 166
t
1
156
120
0.4123
1
t
1
1
1 1
——
1
s
1
1
t
TOTALS
143 ! 1.70 1 23.0000 ! 1660.0 I 1412.0
1160.0 4.1231
213
-------
?
ISOKINETIC RESULTS
CALCULATED RESULTS FOR SAMPLE * —
S0728WOOM5
Plait: CfiF Updated 12/09/89
Performed by;
GREG HILL
[ate: 07/23/89 Printed 12/09/89
Test No./Type:
S0728110W5
lsokinetic:ty
I I
=
97.5
Sasple Location: STACK'
Start/Stop Ticei
1400-1505
Metered Sonple 5as Voluse Iscf)
Via std)
=
40.89
!scra)
Via std)
-
1.15B
PARAMETER
SYMBOL
VALUE
Stack Gas Flow, std cond. Idscfm)
Qls)
=
975
Icalc.)
std cord. (dsca/ein)QIs)
=
27.6
Nazcle Diaaeter, Actual (in)
Ntdi
0.375
actual lacfa!
Ola)
a
1714
Fitot Tube Correction Factor
C(p)
0.84
actual laca/itin)
Ola)
s
4B.5
Gas Meter Correction Factor
(alpha)
1.03
Particulate Leading, dry (gr/dscf)
C(s std)
C.0156
Stack (Duct) Dinensions (in):
3 77. 02!gr/dscf) Cis std)
0.0240
Radius (if round)
R
7
§ 72 02(ag/dsca)
C(s std)
=
55
Length (if rectangular)
L
Particulate Erissicn Rate (lb/hr)
E < p)
s
0.131
Width (if rectangular!
M
tkg/hr)
Elp)
b
0.059
Area o' Stack !sq ft)
flts)
(1.06901
)
Stack Gas Hater Vapor Proportion
B(ko)
=
C.328
1 of Saaple Points
1
12
Molecular Height of Stack Gas, Dry
M(d)
c
29.31
Total Sampling Tine (mm)
(theta)
( 40.00 )
Met
Mis)
-
25.60
Barcoetric Pressure (in Hg)
P(b)
30
Stack Pressure, absolute (in Hg!
Pis)
=
30.00
Stack Presaire (in H20!
P(stack J
0.06
Average Stack Velocity !ft/sec!
V(s avg)
=
26.7
6as deter Initial Reading (ci ft)
259.091
Gas Meter Final Reading (cu ft)
301.655
Nat Gas Sarple Voluae (:u ft)
Vln)
( 43.56
)
Vol Df Liquid Collected (nl) VI(c) 423.7
Vol of Liq S Std. Conds. (set! V(h std) ( 19.944 )
U't. al Filter Particulate (go) 0.0214
Wt. a1 Frabe Nash Particulate Ion) 0.02
Wf of Ccthinei! Particulate (o«! die) f 0.0414 )
02 Concentration (by CEM) t 11.?
C02 Concentration (by CEM) 1. 5.2
CO Concentration (by CENJ 1 0
fC Concsntration (by diff.) It ( 82.90 )
Saaple ! dClock IVelCEity! Orifice ! Stack
Foir.t i Tins I Mead. dPSneter.dH ! Trap
i (cin) Kin H20)l(in H23) ! (deoF)
Gas
Ten
in
Meter
(degF)
i out
1 1
3
0.17 !
1.7 ! 266
103
103
0.412:
2 !
5
0.17 :
1.7 i 166
111
106
0.4123
"7 1
1
5
0.17 !
1.7 ! 166
121
106
0.4123
4 :
5
0.17 !
1.7 ; 166
130
110
0.4123
5 i
5
0.17 !
1.7 ! 166
132
113
0.4123
6 ;
5
0.17
1.7 ; 166
136
115
0.4123
1 !
5
0.17 1
1.7 : 166
113
113
0.4123
2 ;
J
0.17
1.7 I 166
133
113
1 0.4123
z :
5
0.17
1.7 i 166
141
124
0.4123
4 :
e
¦j
: o.i7
1.7 1 16c
136
12a
! 0.4123
5 i
5
0.17
1.7 ! 166
145
13
! 0.4123
6 !
i
5
: o.i7
~ i
i ~
1
i
i 1 1
i _ ,,
i
1.7 1 166
147
0
130
; 0.4123
1
1
1
.
TOTALS !
6G
1 2.04
20.4000 1 1992.0
1568,0
1388.0
! 4.9477
SORTCdP? iFlEJ) DATA AVERAGES FOR SAMPLE S
Velocity M&ad ("wc>
Orifice deter Reading C*l
13tack; Teeperatu-e
¦Meter Tenperature
IRoot-dean-Square dP Cnc)
(dag F)
tdeg C)
Ideg F)
(deg 0
S072B1400H5
dP(avo) = 0.170
dHUvgj = 1.700
T(s avg) ¦ 166.0
T(s avg) = 74.4
Tin avg) * 123.2
Tl» avj) = 50.6
SORT(dP) = 0.412
214
-------
APPENDIX E
AFTERBURNER PARTICULATE SIZING REPORT
215
-------
BAHCO ANALYSIS
FOR
ACUREX CORPORATION
OCTOBER, 1989
ETS, inc.
A subsidiary of ETS International, Inc.
3140 CHAPARRAL DR.. SW
SUITE C-103
ROAKOKE. VA 24018
Pollution Control Consultants
Specializing In
Toxic Emission Measurement and Control
ETS CONTRACT NO: 89-208-L
216
-------
TABLE OF CONTENTS
PAGE
1.0 INTRODUCTION 1
1.1 BACKGBOUND 1
1.2 OBJBCTIVE 1
1.3 TEST PROGRAM 1
2.0 SUMMARY OF PARTICLE SIZING RESULTS 2
2.1 PARTICULATE CATCHES 3
2.2 UNFIRED AUTODRY SAMPLE 3
3.0 SAMPLE CLASSIFICATION 4
4.0 CALIBRATION 4
LIST OF TABLES
TABLE I - SUMMARY OF PAHTICLB SIZB DISTRIBUTION 6
TABLE II - MASS MEDIAN DIAMBTER VALUES 7
LIST OF FIGURES
FIGURES 1-9 - PARTICLE SIZE DISTRIBUTION GRAPHS 8-16
LIST OF APPENDICES
APPENDIX A - BAHCO DATA AND RBSULTS 17
APPENDIX B - CALIBRATION DATA 28
APPENDIX C - SAMPLE CHAIN-OF-CUSTODY 32
APPENDIX D - CALCULATIONS 35
217
-------
1, D INTRODUCTION
1.1 Background: ETS, Inc. received ten particulate samples from
Acurex Corporation in August, 1989. The samples were identified
as follows:
SAMPLE
1
ACUBEX CODE
A07281234F
SAMPLE
LOCATION
AFTERBURNER
ETS CODE
3778 D
2
A08011103F
AFTERBURNBR
3779
D
3
A08020950F
AFTERBURNER
3780
D
4
A08041037F
AFTERBURNER
3781
D
5
A08091025 F
AFTERBURNER
3782
D
6
A08110830F
AFTERBURNER
3783
D
7
A08150957F
AFTERBURNER
3784
D
8
A08160913F
AFTERBURNER
3785
D
9
A08170956F
AFTERBURNER
378B
D
10
M08211100
AUTO-DRY
3787
D
The first nine samples were particulate catches recovered
from an Alundun thimble. The last sample consisted of unfired
Autodry material.
1.2 Objective: The purpose of the test program was to charac-
terize the particle size distribution of each sample into nine
weight fractions based on particle size.
1.3 Test Program: The test program consisted of the following
subparts:
(i) Particle size distributions for each of the ten samples
were determined by centrifugal classification using a
218
-------
No. 6000 Bahco Micro Particle Classifier.
The testing was conducted in accordance with the
procedures outlined in ASMS PTC 28-1956.
(ii) The particle throw-offs (fines) for each of the eight
stages of the Bahco analyses were retrieved from the
particle classifier and placed into individual glass-
vials. This provided a total of nine fractional
samples for each starting sample, with each fraction
representing a different particle size range.
(iii) The unfired Autodry sample was sieved to remove all
particles less than 150 microns (100 mesh screen). The
fraction of the particles smaller than 150 nicrons was
subjected to the Bahco analysis described in subpart
(i).
(iv) The density of the unfired Autodry sample was determined
for the less-than-150 nicron fraction. This value was
then applied to the Bahco data for all ten samples to
correlate terminal velocities with particle diameters,
(v) A dedicated calibration of the Bahco particle classifier
was conducted using standard samples prepared by the
National Air Pollution Control Administration/Public
Health Service.
2.0 SUMMARY OF PARTICLE SIZING RESULTS
Table I lists the particle size distributions far each of
the seven samples, while Figures 1 through 9 graphically show the
particle distributions for each sample except the Autodry
219
-------
sample. Mass median values derived from graphical interpolations
are presented in Table II. Raw data for the Bahco analysis may
be found in Appendix A.
Strickly speaking, the Bahco analysis classifies according
to the particle terminal velocity distribution, and not by
particle diameter. The conversion of the terminal velocities
into actual particle sizes may be performed using Stokes' Law,
which must assume a uniform specific gravity for the particles.
A generalized formula based on Stokes' Law is given in Appendix
D.
2.1 Particulate Catches: The mass median particle sizes for the
nine particulate catch samples ranged from 16.5 microns for
sample A08091025F to B4 microns for sample A0B170956F. These
values assume a uniform density of 2.51 grams/cm3 (sifted
Autodry).
2.2 Unfired Autodrv Sample; The unfired Autodry sample was
screened through a 150 micron sieve (100 mesh) before performing
the Bahco analysis. 2.29> of the sample was found to be less
than 150 microns (i.e., 97.8k was greater than 150 microns).
Only the fraction less than 150 microns was subjected to the full
Bahco analysis.
Density determinations of the sieved sample gave a value of
2.51 grams/cm3.
220
-------
3.0 SAMPLE CLASSIFICATION
Appendix C contains listings of all of the sample classifi-
cations generated by the Bahco analyses.
The Bahco analyses classified each sample into the nine
different fractions based on particle size. This classification
was accomplished by using different sized throttle spacers in the
Bahco classifier. Each throttle produced a different air flow
through the instrument, thus providing the means of the particle
separation by terminal velocity distribution.
Throttles with sizes of lBmm, 17mm! 16am, 14mm, 12mm, 8mm,
4mm, and Omm {no throttle) were used. The sample was subjected
to the throttles sequentially with the 18mm throttle first and
the 0mm throttle last. Each throttle separated the dust sample
into two portions - a fine "throw-off", and a course "residue".
The throw-offs were recovered for each throttle and placed into
separate vials, while the residues for each throttle were placed
back into the machine to be subjected to the next lower throt-
tle. The residue for the last throttle (Onus) was retrieved and
placed into a glass vial.
4.0 CALIBRATION
The Bahco Centrifugal Classifier was calibrated in accor-
dance with section 5.11 of the ASMS PTC 28-1965. Three sets of
standard samples were used in t>»* calibration. These standards
were obtained from the Power Test Code Committee No. 28 of the
221
-------
ASMB.
Data and results for the calibration are contained in
Appendix B. All terminal velocities and particle diameters used
in this report were derived from this calibration.
WHITTBN BY
APPROVED BY:d
John D. McKenna
222
-------
TADLE I
SUMMARY OF PARTICLE SI7.K DISTRII3UTIONS
iCUMULATIVK '4 LKSS TilAH STATED SIZES)
SAMPLE
ID
1. 05
3.64
ICO
1*^
|oi
I'ARTICLK
11.04
SIZE MICRONS
16.77 30.43
38. 00
41 . 67
15_0
A07281234F
4.9
12.9
32. 0
30. 7
44.6
40.4
50.3
52.5
96.
A08011103F
3-4
8.0
23. 5
28. 3
34.2
37.9
40.6
42.2
98.
A08020950F
4.4
10.7
19.4
25.2
20.9
33. 1
37. 1
39.5
96.
A08041037F
4.4
15. 9
2G.8
30.0
33.4
36.9
39.4
41.2
98.
AOQO S1025 r
5. 1
17.4
42. 1
45.9
50. 3
52.0
54.5
55.3
93.
A0B110B30F
4.2
15.5
36.7
40.1
44.3
47.2
49.5
50.8
83.
A08150957F
5.0
18.0
35.4
38.9
43.6
48.2
50.8
52. 9
96.
A081G0913F
4.6
8.8
16.2
IB.6
21.9
24.7
26.7
28. 2
98.
A08I70956F
2.7
9.0
19.G
23.1
29. 0
33.5
35.6
37. 0
76.
M08211100
0.2
0.5
0.8
0.8
1.1
1.4
1.5
1.5
2.
-------
TABLE II
MASS MBDIAN DIAMETER VALUES
SAMPLE I.D. MASS MEDIAN fmicrons)*
1 A07281234F 32.0
2 AO8011103F 51.5
3 A08020950F 51.5
4 A08041037F 53.5
5 A08091025F 16.5
6 A08110830F 39.5
7 A08150957F 33.0
8 A08160913F 90.0
9 A0817095SF B4.0
10 M08211100 NA
* From Figures 1 through 9
224
-------
PARTICLE SIZE DISTRIBUTION
IOOO,
ninrif
-:;j in;
-TintMH
sa «*i?, ™
mmm
ILiiEilli
:
}\
is ib is ho sb to 7b &o ee
CUMULATIVE I LESS THAN STATED SIZE
FIGURE 1 - SAMPLE NO. A072B1234F
225
-------
PARTICLE SIZE DISTRIBUTION
:ensnsRisnnRRaBss3i;
iniMnaHiNBinifainraifliuml
CUMULATIVE S LESS THAN STATED SIZE
FIGURE 2 - SAMPLE NO. A08011103F
226
-------
PARTICLE SIZE DISTRIBUTION
CUMULATIVE 2 LESS THAN STATED SIZE
FIGURE 3 - SAMPLE NO. A0802095QF
771
-------
iooo
PARTICLE SIZE DISTRIBUTION
TIT
}= i±it
I
CUMULATIVE S LESS THAN STATED SIZE
FIGURE 4 - SAMPLE NO. A08041037F
228
-------
1000,
PARTICLE SIZE DISTRIBUTION
LIU i
qoo+=
700JH
itfflij
I
mm
ml Ml]
—¦ ¦ i""*" *"
I
£tzi2£tijil
ttr:rn;i
m:
CUMULATIVE % LESS THAN STATED SIZE
FIGURE 5 - SAMPLE NO. A03091025F
229
-------
KMKI1LU SIZE DISTRIBUTION
mm m
EH IE
I
m
*
5
i? ZD X 10 SO to TO eo B? 10
CUMULATIVE % LESS THAN STATED SIZE
FIGURE 6 - SAMPLE NO. A08110830F
230
-------
PARTICLE SIZE DISTRIBUTION
CUMULATIVE I LESS THAN STATED SIZE
FIGURE 7 - SAMPLE NO. A08150957F
231
-------
PARTICLE SIZE DISTRIBUTION
CUMULATIVE 2 LESS THAN STATED SIZE
FIGURE 8 - SAMPLE NO. A08160913F
232
-------
PARTICLE SIZE DISTRIBUTION
f nnnm
Ht
a
IS
1S2.
1
CUMULATIVE 1 LESS THAN STATED SIZE
FIGURE 9 - SAMPLE NO. A08170956F
233
-------
APPENDIX A
BAHCO DATA AND RESULTS
234
-------
BAHCQ DATA AND RESULTS
Sample I. D. iA07281234F
Sample Type:AFTERBURNER
Client :ACUREX CORPORATION
Contract :89-233-L
-NOTE: All sample duet veights Include pan velght.
CENTRIFUGE DATA
PAN WEIGHT (grans): 2.58067
AS-IS SAMPLE WT(gms): 3.66535
-100 MESH SAMPLE (gmu): 3.82103
BAHCQ SAMPLE (gins) : 3. 82105
DENSITY DATA
FLASK VOLUME (ml) : SO
FLASK HEIGHT Cgma> : 40.83494
SAMPLE «¦ FLASK (grams) i 42.57438
LIQUID DENSITY (gm/cc) i 0.7869
FLSK+LIQU.+SAMP. (grams): Bl.37573
PERCENT LESS THAN
100 MESH
96. 45
CALCULATED DUST DENSITY
2. 510
CUMULATIVE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LES5 THAN
DIAMETER
THROTTLE
(grams)
lft/aec)
SIZE
(microns)
18
3.75851
0. 62
4.89
1. 85
17
3.£5611
2. 41
12. 91
3. 64
16
3.40182
16.2
32.81
9. 45
14
3.32622
22. 1
38. 73
11. 04
12
3.25175
51.0
44. 56
16.77
B
3.20271
168
48.40
30. 43
4
3.17818
262
50.32
38.00
0
3.15074
o.Hol 313
52. 46
41.67
•70 3
= -5^
/,2-17 69
235
-------
BAHCO DATA AND RESULTS
Sample I.D.IAQaO11103F
Sample TypesAFTERBURNER
Client :ACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust velghts Include pan weight.
CENTRIFUGE DATA
PAK WEIGHT (grsmB)i
AS- IS SAMPLE WTCgira):
-100 MESH SAMPLE (gme)
BAHCO SAMPLE C graa> >
PERCENT LESS THAH
100 MESH
2.64138 ^
4. 14035^
4. 111243
4.11043
98. 00
iJT~ !* Y^
DENSITY DATA
FLASK VOLUME (ml)
FLASK WEIGHT (graa>
SAMPLE ~ FLASK (grama)
LIQUID DENSITY (gm/cc]
FLSK+LIQU.*SAMP.(grama)
CALCULATED DUST DENSITY
CUMULATIVE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LESS THAN
DIAMETER
THROTTLE
< grama)
(ft/aec)
SIZE
(microns)
IS
4.06022
0.62
3. 35
1.85
17
3. 97796
2.41
6. 84
3. 64
16
3. 75856
16. 2
23. 47
9. 45
14
3. 66642
22. 1
28. 29
11. 04
12
3. 59807
51.0
34. 18
16.77
8
3.54187
166
37. 93
30. 43
4
3. 50144
262
40. 63
36.00
C
3. 47804
315
42. 19
41.67
236
-------
BAHCO data and results
Sample I.D.tAO8020950F
Sample Type:AFTERBURNER
Client sACUREX CORPORATION
Contract :89-208~L
NOTE: All sample dust veighte Include pen veight.
CENTRIFUGE DATA
PAN WEIGHT (grains):
PERCENT LESS THAN
100 MESH
2.57282
AS-IS SAMPLE VfT(gins) : 3.3B474
-100 MESH SAMPLE (gras)j 3.35815
BAHCO SAMPLE(gnaJ: 3.35815
96. 73
DENSITY DATA
FLASK VOLUME Ctrl) i 50
FLASK WEIGHT (gme) : 40.8349a
SAMPLE * FLASK (grams) i 42.57450
LIQUID DENSITY (gm/cc) : 0.7869
FLSK»LIQU. *SAMP. (grams); 81. 37373
CALCULATED DUST DENSITY = 2.510
CUMULATIVE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LESS THAN
DIAMETER
THROTTLE
(grama)
(ft/sec)
SIZE
(microns)
IS
3.32257
0. 62
4.38
1. aa
17
3.27158
2. 41
10. 66
3. 64
18
3.20088
16.2
19.37
9. 45
14
3.15391
22. 1
25. 16
11. 04
12
3.123S1
51. 0
28.89
16. 77
8
3.08322
160
33. 12
30. 43
4
3.05686
262
37. 11
38.03
0
3.03774
315
39.46
41. 67
237
-------
BAHCO DATA AND RESULTS
Sample I. D. ; AO8041037F
Sample Type:AFTERBURNER
Client sACUREX CORPORATION
Contract J89-208-L
NOTE: All sample dust weights include pan "eight.
CENTRIFUGE DATA
PAN WEIGHT (grans):
AS-IS SAMPLE VT(gma):
-100 MESH SAMPLE (gma)
BAHCO SAMPLE (gins) :
PERCENT LESS THAN
100 MESH
2. 55241
4.14108 ^
4. 11914
4.11914
98. 62
DENSITY DATA
FLASK VOLUME (ml)
FLASK WEIGHT (gms)
SAMPLE ~ FLASK (grans)
LIQUID DENSITY (gm/ec)
FLSK+LIQU.-SAMP, (grans)
CALCULATED DUST DENSITY =
• 52
40.83494
42.57456
0. 7S(>9
81.37573
2.510
S^yk Jf.
CUMULATEE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LESS THAI
DIAHETER
THROTTLE
(grams >
(ft/aec)
SIZE
(microns)
18
4.04857
0. 62
4. 44
1. 85
17
3.86828
2. 41
15. 92
3. 64
15
3.69297
16. 2
26. 83
9. 45
14
3.64281
22. 1
29. 98
11. 04
12
3.58798
51. 0
33.43
16.77
8
3.53292
168
36. 90
30. 43
4
3. 493
262
39. 41
38. 00
0
3. 46534
315
41. 15
41. 67
238
-------
BAHCO DATA AND RESULTS
Sample I.D. :AO809102SF
Sampla Type:AFTERBURNER
Client tACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust Heights Include pan weight.
CENTRIFUGE DATA
PAN WEIGHT (grams)c
2.5736B
AS-IS SAMPLE WT(gme): 3. 72236
-100 MESH SAMPLE (gma): 3.64418
BAHCO SAMPLE(gna):
PERCENT LESS THAN
100 MESH
3.64413
93. 19
DENSITY DATA
FLASK VOLUME (ml) : 50
FLASK HEIGHT (gma) I 40.8349^
SAMPLE ~ FLASK (grams) : 42.57450
LIQUID DENSITY
-------
BAHCO DATA AND RESULTS
TZJ-?
Sample I. D. j AD8110830F
Sample Type:AFTERBURNER
Client i ACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust weights include pan weight.
CENTRIFUGE DATA
PAN WEIGHT
SIZE
(microns)
18
3.38962
0. 62
4. 21
1. 65
17
3.274S7
2. 41
15. 50
3. 64
16
3. 058
16.2
36. 73
9.45
14
3. 02362
22. 1
40. 10
11.04
12
2. 38126
51.0
44. 26
16.77
8
2.95157
168
47. 17
30. 43
4
2.92807
262
49. 47
38.00
0
2.91473
315
50.78
41.67
2^0
-------
3AHCQ DATA AND RESULTS
Sample I.D. iAOB150957F
Sample Type:AFTERBURNER
Client iACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust weights Include pan weight.
CENTRIFU3E DATA
DENSITY DATA
PAN WEIGHT (grams):
AS-IS SAMPLE WT(gma):
-100 MESH SAMPLE (gnu):
BAHCO SAMPLE(gna}:
2. 56034 i/
3.769S5
3. 72034
3. 72034
FLASK VOLUME
-------
BAHCQ DATA AND RESULTS
Sample I.D. :AO8160913F £
Sample Type:AFTERBURNER
Client -.ACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust weights Include pan weight.
CENTRIFUGE DATA
PAN WEIGHT (gramaJ:
AS-IS SAMPLE WT(gnis)i
-100 HESH SAMPLE (gms)i
BAHCO SAMPLE(gms):
PERCENT LESS THAN
100 MESH
2.59758
3.83176
3.dl159
3.81159
98. 37
4 '-m'?
DENSITY DATA
FLASK VOLUME (ral> : §V
FLASK WEIGHT (gme) : 40.8349-)
SAMPLE «• FLASK (grams) : 42.57456
LIQUID DENSITY (gra/cc) j 0.76
(ft/sec)
SIZE
(microns)
18
3.75442
0.62
4. 63
1. 85
17
3.70532
2.41
8. 61
3. 64
16
3.61158
16. 2
16. 21
9. 45
14
3.58143
22. 1
18. 65
11.04
12
3.541G7
51.0
21. 87
16.77
8
3.50646
166
24. 72
30.43
4
3.48253
262
26. 66
38. 00
0
3.46408
315
28. 16
41.67
242
-------
BAHCQ DATA AND RESULTS
Sample I.D.:AO8170536F
Eampj.^ Type: AFTERBURNER
Client :ACUREX CORPORATION
Contract :89-208-L
NOTE: All sample dust weights Include pan weight.
CENTRIFUGE DATA
PAN WEIGHT (grama):
AS-IS SAMPLE WT(gmc)i
-100 HESH SAMPLE (gma);
BAHCO SAMPLE (gins) :
2.53046 ~
4. 44234
3.99127
3. 99127
PERCENT LESS THAN
120 MESH
76. 41
DENSITY DATA
FLASK VOLUME (ml) : 50
FLASK WEIGHT (gins) : 4®.8349^
SAMPLE *¦ FLASK (grains) : 42. 57453
LIQUID DENSITY (grn/cc) : 0.7Q&H
FLSK-LIOU.~SAMP.(grama)t 61.37573
CALCULATED DUST DENSITY » 2. 510
CUMULATIVE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LESS THAN
DIAMETER
THROTTLE
(groins)
lit/sea)
SIZE
(microns)
18
3.93982
0. 62
2. £9
1. as
17
3.B1896
2, 41
9.01
3. 64
16
3.£1685
16. 2
19.58
9. 45
14
3. 35024 '
22. 1
23.07
11.04
12
3.43704
51. 0
28. 99
16.77
8
3.34952
168
33. 57
30. 43
4
3.31008
262
35.63
38.00
0
3.28334
315
37. 03
41.67
243
-------
BAHCO DATA AND RESULTS
Sample I. D. :MO8211100
Sample Type:AUTO-DRY
Client :ACUREX CORPORATION
Contract : 39-208-1.
NOTEi All- sample dust weights Include pan weight.
CENTRIFUGE DATA
PAN WEIGHT (grama) I
16.30223
AS-IS SAMPLE VT(graa): 249.812
-100 MESH SAMPLE (gusli 21.3G133
BAHCO SAMPLE ( gins) : 19.59630
PERCENT LESS THAN 2.17
1019 MESH
DENSITY DATA
FLASK VOLUME Cnl) : = 0
FLASK WEIGHT Cgms) : 40.834S^)
SAMPLE ~ FLASK (grama) « 42.5745R
LIQUID DENSITY (gm/cc) : 0.78£?
FLSK*LIQU. ~SAMP. (grans)i 81.3757^
CALCULATED DUST DENSITY « 2.£"LD
CUMULATIVE
TERMINAL
PERCENT
PARTICLE
RESIDUE
VELOCITY
LESS THAN
DIAMETER
THROTTLE
(grama )
(ft/sec)
SIZE
(microns >
18
19.3124
0. 52
0. 19
1. 85
17
18.8398S
2. 41
0. 50
3. 64
16
18.43267
1G.2
0. 77
9.43
14
18.29934
22. 1
0. 85
11.04
12
17.95873
SI. 0
1. 08
16.77
a
17.53238
isa
1. 3G
30. 43
4
17.38282
262
1. 46
36. 00
0
17.30254
315
1. 51
41. 67
244
-------
APPENDIX B
CALIBRATION DATA
'245
-------
CALIBRATION DATA
Throttle
Mass - grans
(Includes
Pan Weight)
Number
*1
#2
#3
Sample Wt.
7.70646
B.61152
10.00248
Pan Wt.
2.S9622
2.61382
2. 61686
Residues
is
7. 06994
8.02004
9.21866
17
6. 35338
7.14928
7.97369
16
4.65917
5.07683
5.60361
14
4.35017
4.68564
5.13493
12
3.63278
3.87235
4.14492
a
3. 04404
3.13772
3.23414
4
2. 88137
2.95072
3.01598
e
2.82317
2. 87983
2.93041
CALIBRATION RESULTS
Throttle
Cumulative
Weight
Percent Less
Than Size
Number
#1
#2
#3
Average
18
12.456
9.862
10.613
10.977
17
26.478
24.380
27.469
26.109
16
59.631
58.934
59.560
59.375
14
65.678
65.456
65.90S
65.660
12
79.716
79.016
79.310
79.348
8
91. 237
91.265
91.642
91.331
4
94.420
94.383
94.596
94.468
0
95.559
95.565
95.755
95.626
EQUATION FOR PARTICLE DIAMETER
Stokes' Law Equation for Particles in Airt
Log(D) = 0.5705 - 1/2 x Log(p) «• 1/2 x Log (V)
vhere p = average dust density
Average Density p « 2.6
Throttle
X Less
Terminal
Partiole
Number
Than Size
Velocity
Diameter
18
10.977
0.62
1. 8
17
26.109
2.41
3. 6
16
59.375
16. 2
9. 3
14
65.680
22.1
10. 8
12
79.348
51.0
16. 5
8
91. 381
168
29. 9
4
94.466
262
37. 3
0
95.626
315
40. 9
246
-------
77.^/g 1/
oIl
n 2Mt
lis.T-
^ 2Z. r
fl S"/. O
S ibV
7 Zfc 2_
0 3/S"
-------
APPENDIX C
SAMPLE CHAIN-OF-CUSTODY
248
-------
SAMPLE CLASSIFICATIONS
Each sample was classified into the following sub-samples after
the analyses:
1.
4 100 Mesh
2.
18 Thottle Throw-off
3.
17 Throttle Throw-off
4.
16
5.
14
6.
12
7.
8
8.
0
9.
0 Residue
249
-------
Acurnx Corporation Laboratory
US EPA Conbustion flcsoarch Facility
Clmln of Custody Kocord
Pro J. i>o. Project None
^)rv.m.c l vOvcfeSL.0./i X U31>
fj / /
A/ / /
Ax/ / /
Samplers (Signature)
(/ -
Station Nunbor
Data
Tina
INI 1 I9'""
"o
1/
V
Sanple
Location
No. of
Con-
tainers
Af /
$/ /
/ Reoarka
Mnwiamr-
1.1^4
/iCWtlpu rnPt-
|
J
J
j_
~7
V
J
—
bpp er\f.ln.«LP J Lpl4?r
Aovchionr-
V/'/fTi
(in H
'1 « 4
/
Cor ftna.1 "/-o bf drmp
'jjifci'i
015B
<« if
1
' i
fi090*7F
slSf
/o^7
k "
1
J\o -ru»t v-in\ woi mjoiliut
3o«J Btoi »T rt*«icrti7 -Wij PSo&fM 5/il/yl
AOfTfS
sytys?
c>*?57
it ''
1
I7 09%r.
l/'lkl
H ' 1
i
>/
0756
,, H
I
V
_'0«J TfH JiMM. Mti MISUW1117
aSb& S»S 4 r GJWJi.n.7 Tlfu CiVifrCM M71IK1
A\fW ^ ; ttncj
3-JiX 0
hofj
l/
P~n r»
(
y
—
>
—
—
—
Relinquished by:
(Signature)
<3£~J!a®3
Uate/TJaa
/
/
r7rv.
rt
J
U
(•
scelvcd by:
ilenature)
RoJ 1 nifiiJ shod by:
(Signature)
Ci.«r-2L.^ focuxii
Doto/Tine
ia.O«>
/
/
Received by: ofJ ®/cl/8't
(Slenature) wztlofl
(bJltw' '2uX>—
Relinquished byV
(Signature)
lJate/Tiise
/
/
/
icelvcd by:
Slenoturc)
IftyliKjulbliud by:
(Signature)
Date/Tine
/
/
/
ReccJvod by:
(Sienature)
Jlel 1 ncjulsited by:
(Signature)
bule/Tlme
/'
/
/
Received for Dule/Tlmo
laboratory by(SicnattireJ /
toinarks:
-------
APPENDIX D
CALCULATIONS
251
-------
BAHCO PARTICLE SIZING CALCULATIONS
log(D) = 0.5705 + 0.5 x (log(v) - log (SG))
2. Cumulative Percent Less Than Size
» Wo - W q x 0^55
Wo
hvfwvun' v''w,
D = Partiae ¦'diameter, microns
SG = Specific gravity of dust
C% «¦ Cumulative percent of dust less than stated size
C150 = Percent of bulk sample less than 100 mesh (150 microns)
wo <¦ Weight of 5ahco sample, g-ams
WR = Weigh: of residue for a particular throttle, grams
v = Terminal velocity of particles at each throttle, in./min.
t
Throttle" y
la 0.62
17 2.41
16 16.2
14 22.1
12 51.0
Q 168
4 262
0 315
252
-------
APPENDIX F
VOST GC/FID AND CI" ANALYSIS, PROCEDURES
i
253
-------
Page 1 of 6
Revised 4-6-89
XRF Standard Operating Procedure
for Analyzing VOS7 Tubes
Apparatus
A. Thermal Desorptlon Dnlt
The thermal desorptlon unit for VOST cartridges, (MuTech desorbtion
unit with NuTech 320 controller) is capable of thermally desorbing
the sorbent resin tubeB. It is also capable of heating the tubes
to 180+ 10C with flow of interference-free nitrogen or helium
through the tubes.
B. Purge-and-Trap Unit
The purge - and - trap unit (Tekmar) conslstB of three separate
pieces of equipment; the sample purger, trap, and the desorber. It
should be capable of meeting all requirements of Method 5030 (sw 846,
2nd Ed.) for analysis of purgeable organic conpounds from water.
C. GC/FID System
The Hewlett Packard 5880A Series gas chromatograph Is equipped with
a flame ionization detector (F.I.D.). The column used Is a fused
silica capillary gas chromatographic column (DB-624 30n x 0.53am I.D.
x SftLm film thickness).
Procedure for Thermal Desorptlon of VOST Tubes
The VOST tubes are logged In the VOST record book when they Bre brought
Into the lab, by tube number and sample Identifier number. Then the
following steps are executed:
1. The caps are taken off the VOST tubes. Internal standards(s) are
added, typically 0.3ftg of each compound In methanol solution at
0.lag/ml.
Z. Reducing unions (1/4" to 1/16" SS) are placed on the tubes plus 1/16"
connecting tubing.
3. The VOST tubes are connected to the NuTech carrier lines for desorb
gas flow In the opposite direction sample was taken, and checked for
tightness, while NuTech thermal deBorptlon unit (TDU) valve is in
desorb position.
254
-------
Page 2 of 6
Revised 4-6-89
4. Then the VOST tubes are placed In the NuTech TDD and heated to 180C+
IOC with Interference-free heliua through the tubes at 40ml/ain.
5. VOST tubes are desorbed and purged for fifteen (15) ainutes through
the sparger onto the Tekaar chealcal trap.
6. When the Tekaar reaches the desorb cycle the NuTech TDU valve Is
switched to the vent position and allowed to vent for forty five (45)
ainutes at 100 al/aln for cleaning purposes. Water In the sparger
is drawn off, discarded, and replaced with S.Oml of fresh cold tap
water.
7. During dcsorbtlon and cleaning period, samples are being analyzed
by FID GC, and the fresh water in the uparger Is being pre-purged
in preparation for the next analytical run.
3. Apparatus Setoolnts
A. Thema1 Desportlon Unit (NuTech with 320 NuTech controller)
The theraal desorptlon unit oonslst of three asln heating zone9; the valve,
lines, and desorber, all of which are maintained at 180C+ IOC. There
Is a heliua flow of 40 ai/ain when In desorb cycle and flow of 100 al/nin
when In vent cycle.
B. Tekaar Purge and Trap Unit
The purge and trap consists of a series of autonatic steps.
1. Standby -
2. Purge ready -
3. Purge -
During this step the Tekaar chealcal trap is allowed to
cool to 30C.
The Tekaar chealcal trap at 30C is ready to start purge
of the VOST tubes in the thernal desorptlon unit onto
the Tekaar chealcal trap.
During this cycle, the VOST tubeB are purged for fifteen
(15) ainutes with 40 al/ain of heliua gas through the
sparger, onto the Teknar chealcal trap. The purger or
sparger holds five als of interference-free water.
4.Desorb preheat- The Tekaar chealcal trap is preheated to 100C, taking
about fifteen seconds to reach tenperature.
5. Desorb - For four ainutes at 180C the Teknar trap Is desorbed
onto the Q.C. coluan with flow rate of 5 als/aln of
organic free heliua.
255
-------
Page 3 of 6
Revised 4-6-89
6. Bake - For seven minutes at 215C and 40 nls/ain the Tekmar
chemical trap Is vented out the back of the Tekmar for
cleaning purposes.
C. PC/FID Svstea
Gas ehroaatograph: The Hewlett Packard 5880 series ehroaatograph
Is temperature progr;43«ed to separate the analytes which ore
quantitated with a flane ionization detector (24QC) using Multilevel
external standardization (ISTD), Oven temperature is held at 35C
for six Minutes, then increased to 140C at 4C/aln» then held for
ten ainutes. Interference-free heliua carrier gas is set at 5
¦ls/nin. Prior to analysis, every saaple is spiked with Internal
standard and surrogate compounds. These coapounds nay simulate the
behavior of compounds of interest and confira that acceptable
recoveries are being achieved on every saaple. The results of
internal standards and surrogate recoveries (*) are reported with
the saaple results.
4. External Standard Calibration Procedure
For all analytes at interest, e.g. Table 1. prepare calibration standards
at a ainiaium of three (3) concentration levels by staking appropriate
dilutions of a stock standard at 1.Ofig/ftL Methanol. The concentration
levels sight be, e.g. 3.0, 0.3, and .03 total fSg per 3 8L injected.
Each calibration standard is injected onto the exit end of the VOST
tubes (3JL Injection), O.SmL of water is added in an effort to minle
flue gas samples, and the analysis is conducted noraally. Tabulate
response factor against aaount injected for each target analyte.
Mass Injected tftel
Response factor - Peak height
1) The ratio of aaount injected (fig) to response (PkHt) is defined as
the response factor RF, which is calculated for each analyte at each
standard concentration. If the percent relative standard deviation
(XRSD) of the response factors for each analyte Internal standard,
and surrogate is less than 20k over the working range, linearity can
be assuaed. If linearity cannot be established, recallbratlon at
three levels aust be performed.
2) The working response factors aust be verified on each working day
by the analysis of one or aore calibration standards. It the
response faetor for any target analyte varies froa the predicted
response factor by aore than ± 30*, the systea aust be recalibrated
at that level.
Percent Difference R, X 100
Where: Rj - Response factor fro* proceeding analysis
Kg - Response faetor froa succeeding analyses.
256
-------
Page 4 of 6
Revised 8-20-88
Table 1
f
| Conpound
1
1
| Abbrev.
i
I
[1,1-Dlchloroethylene
1
|1.1-DCEENE
(Methylene Chloride
|M/C
[t-1.2-Dlchloroethylene
|t-1.2-DCEENE
|HEXANE
|Hexane
|1,l-Dlchloroethane
j1¦1-DCEANE
jCHLOROFORM
jchlorofora
[1.1.1-Trlchloroethane
|1.1.1-TCEAKE
jCarbon Tetrachloride
j CCL4
jBENZENE
(Benzene
|1,2-Dlchloroethane
j1,2-DCEANE
ITrlchloroethylene
j CL3-EENE
|1,2-Dlchloropropane
j1,2-DCPRANE
jBroaodlchloroaethana
j BDCM
|t—1,3-Dlchloropropylene
|t-1,3-DCPENE
|TOLUENE ,
jToluene
I0CTAKB
|Octane
|c-l,3-Dichloropropylene
|C-1,3-DCENE
|1,1,2-Trlchloroethane
11,1.2-TCEANE
|Tetrachloroethylane
|CL4-EENE
jchlorobenzene
j CL-BZ
(Ethylbenzene
|Et-BZ
|BROMOFORM
|Bromoform
j 4-Bronofluorobenzene
j4-BFB
|1,1,2,2-Tetrachloroethane
jCL-EANE
j1,3-Dichlorcbenzene
j1,3-DCBZ
j1,4-Dlchlorobenzene
j1,4-DCBZ
j1,2-Dlchlorobenzene
j1,2-DCBZ
257
-------
Page 5 of 6
Revised 4-6-89
Dally Performance Checks
1) Calibrate the sy6tem (midlevel standard) immediately prior to conducting
any analyses. A aldlevel standard Bust also be Injected at the end of the
analysis sequence. The response factor for each analyte to be quantitated
must not exceed 30k difference when compared to the Initial standard of
the analysis sequence. If this criteria Is exceeded, Inspect the G.C.
system to determine the cause and perfora whatever Maintenance is
necessary before recalibrating and proceeding with subsequent sample
analysis.
2) Verify retention tine windows (update daily) for eacb analyte; retention
times for dally calibration aust be within ± .08 ain. of prior
calibration standards for all target analytes.
3) Tentative identification of an analyte occurs when a peak froa a sample
falls within the daily retention tine window.
4) Validation of GC systea qualitative performance: use the dally retention
tine windows for each enalyte to evaluate tfcis criterion. If any of the
standards falls outside its daily retention tine window, the systea is out
of control. Deteraine the cause of the problem and correct the problem.
5. Quality Control
1) The quality control program consist of an initial denonstratlon of
laboratory capability and an ongoing analysis of VOST field spike
tube pairs, to evaluate and document data quality. The laboratory
will maintain records to docuaent the quality of the data generated.
Ongoing data quality cheoks are sonpared Kith established
perforaance criteria to deteraine If tbe results of analyses meet
the DQO of the applicable burn series test plan for analytes of
interest as well as surrogate and Internal standard conpounds. When
results of field spikes indicate atypical method performance, a
quality control check standard (Supelco) Bust be analyzed to confira
that the measurements were perforated in an In- control mode of
operation.
2) Before processing any sanples. tbe analyst should demonstrate
through the analysis of VOST tubes, that interferences froa the
analytical systea, glassware, SS VOST tubes, and OFW are under
control. Blank samples should be treated in the same manner as
samples.
3) Consistent with the applicable burn series test plan/QAPP, for each
analytical batch, (up to 20 samples) a blank, field spike and a
field spike duplicate aust be analyzed. The blank and spiked
sanples aust be carried through all stages of analysis. Field spike
solutions will be prepared independently of calibration standards
as dictated by the applicable test plan/QAPP.
258
-------
Page 6 of 6
Revised 4-6-89
4) The experience of the analyst performing gas chromatography Is
invaluable to the success of the analysis. Each day that analysis
is performed, the daily calibration saaple should be evaluated to
determine If the chromatographic system is operating properly.
Questions that Bhould be asked are; Do the peaks look normal?; Is
the response obtained conparable to the response from previous
calibrations?
Careful examination of the standards chromatogram can Indicate whether the
coluan is still good, the desorbtlon lines are leaking, 6 port valve clogged,
etc... If any major changes are made to the analytical system (e.g. column
changed), recalibration of the system must take place.
Required Instrument QC
1) Require that the * RSD vary by <20% when comparing calibration factors to
determine If the 3 point calibration is linear.
2) +. 30* difference when comparing dally response of a given analyte versus
the initial response. If the limit Is exceeded, you must recalibrate.
3) Establishment of retention time windows, and that all succeeding standards
in an analysis sequence must fall within the daily retention time window
established by the first standard of the sequence.
To establish the ability to generate acceptable accuracy and precision, the
analyst must perform the following operation.
1) A quality (QC) check sample concentrate is required containing each
analyte of interest. The QC check sample concentrate may be prepared from
pure standard materials or purchased as certified solutions.
If prepared by the laboratory, the QC check sample concentrate must be
made using stock standards prepared independently from those used for
calibration.
The concentration of the QC check sample concentrate is highly dependent
upon the analytes being investigated. Prior to any analysis each pair of
VOST tubes will be spiked with A/10 1STD (O.Sfig) of nonane and decane.
Prior to any sample being taken each pair of VOST tube will be spiked with
2 surrogate standards (4-Bromofluorobenzene and Octane).
Analysis of purgeable compounds in samples other than VOST. e.g., scrubber
blowdown water, bottom ash, and primary waste feed; Is accomplished using
the PAT/GC-FID methods of this SOP coupled with sample preparation
techniques found in Method 5030, SW 846-Test Methods for Evaluating Solid
Waste, 3rd Ed., November 1986.
259
-------
Page 1 of 2
RevlBed 9-9-88
Standard Operation Procedure for CL - Analysis
A. Calibration
lOOOppm CL - standard - place 1.649 reagent grade NaCL (oven dry, store
In desslcator) in a 1L volumetric flask. Dissolve It In about 500nl
distilled water, dilute to the nark.
1. Prepare lOOppm and lOppm standards by serial dilution of the lOOOppn
standard. Add 2ml ISA (ionic straight adjustor) per 100ml standard.
2. Place the electrodes In the lOppm standard. Set the function switch to
MV. Stir thoroughly, wait for a stable potential reading, and record.
3. Rinse the electrodes, blot dry, and place them in the lOOppm standard.
Stir thoroughly, wait for a stable potential reading, and record.
4. Rinse the electrodes, blot dry and place them in the lOOOppn standard.
Stir thoroughly wait for a stable potential reading, and record.
5. Plot the millivolt reading (linear axis) against concentration (log axis)
on semilogarlthaic paper.
B. Sample Analysis
1. Transfer 50 to 100ml of sample to a 150ml beaker. Add 2ml ISA to each
lOOnl sanple.
2. Rinse the electrode, blot dry and place then in the sanple. Stir
thoroughly. Record the millivolt reading when stable. Determine the
unknown concentration from the calibration curve.
3. Check calibration every fourth sample if the ambient temperature has not
changed. Simply place the electrode in the mid-range standard (lOOppm).
When the reading is stable* compare to the original reading recorded in
step A 3 above. If the readings differ by more than 2.0 mv or If the
ambient temperature bas changed repeat steps 2-5 above. Prepare a new
calibration curve dally.
C. Electrode Slope Determination
1. Put 100ml di6tllled water and 2ml ISA into a 150ml beaker. Turn 701A
function switch to MV position. Place the electrodes In the solution.
260
-------
Page/ 2 of 2
Revised 9-9-88
2. Pipette lal of lOOOppm standard Into the solution. Stir thoroughly. When
the reading Is stable, read the electrode potential In millivolts and
record.
3. Add lOsls of lOOOppm standard. Stir thoroughly. When the reading la
stable read the electrode potential In millivolts and record.
4. Determine the difference between the first and second potential readings.
Correct electrode operation is Indicated by a difference of 87+2, assuming
the solution temperature la between 20 and 25C. If the change In
potential is not within the range, repeat steps 1-3.
D. Measuring HintB
Allow all standards and samples to cone to the same temperature for precise
measurement.
Stir samples and standards during measurement. For best results stir at
a rate that will not cause a vortex.
Between measurements rinse and blot dry the electrodes with a clean dry
tissue to prevent solution carryover.
If electrode response Is slow the membrane may be coated with deposits.
Restore performance by polishing using polishing strips. Polish the
electrode sensing element with a circular notion for about 30 seconds.
Rinse and soak in a standard solution for about 5 minutes before use.
Quality Control
1. For each analytical batch of samples; a blank, replicate, and a matrix
spike will be performed. For example, a test series that comprises eight
burns will require no less than; three blanks, three replicates, and three
matrix spike.
2. Calibration check readings may differ by no more than ±2.0 mV from the
value established by the daily calibration curve. If this limit Is
exceeded, a new calibration ourvc will be prepared, and samples whose
measurements are In question will be reanalyzed.
3. An Intramural check samples, estimated to be at or near the regulatory
action level, will be analyzed with each analytical batch of samples.
Acceptance criteria will be dictated by the applicable test plan/QAPP.
261
-------
TECHNICAL REPORT DATA ,
(PIccse read Instructions on Ihc reverse before compteri"
!. REPORT NO. 3.
EPA/600/2-9l/032b
3.
4. TITLE AND SUBTITLE
THE FATE OF TRACE METALS IN A ROTARY KILN INCINERATOR
WITH A SINGLE-STAGE IONIZING MET SCRUBBER - Volume II
Apperdices
5. REPORT DATE
July 1991
6. PERFORMING ORGANIZATION COOE
7. AUTHORS]
D. J. Fournier, Jr.
L. R. Waterland
8.PERFORMING ORGANIZATION REPORT NO.
9. PERFORMING ORGANIZATION NAME AN o AOORESS
Acurex Corporation
Jefferson, AR 72079
r
Id. PROGRAM ELEMENT NO.
1 1. CONTRACT/CHANT NO.
68-C9-C038
12. SPONSORING AGENCY NAME AMD ADDRESS
Risk Reduction Engineering Laboratory—Cin., OK
Office of Research and Development:
U. S. Environmental Protection Agency
Cincinnati, Ohio 45268
13. TYPE OF REPORT AND PERIOD COVERED
Project Report
14. SPONSORING AGENCY COOS
EPA/600/14
15. SUPPLEMENTAR V NOTES
Gregory 'J. Carroll FTS: 684-7948 Commercial: 513/569-7948
18. A8STHACT - _
— series or pilot-scale incineration tests was performed at EPA's Incineration Research
Facility (IRF) in Jefferson, Arkansas, to evaluate the fate or trace metals fed to a rotary kiln
incinerator equipped with an ionizing wet scrubber (IWS) for particulate and acid gas control.
Test variables were kiln temperature, ranging from 816° to 927°C (1500° to 1700'F); afterburner
temperature, ranging from 982° to 1204°C (1800° to 2200°F); and feed chlorine content, rangL'i
from 0 to 8 percent. The test program evaluated the fate of five hazardous constituent trace
metals (arsenic, barium., cadmium, chromium, and lead) and four nonhazardous constituent
trace metals (bismuth, copper, magnesium, and strontium)..* ^ '+• L"v> &r<;-C:*w
The test results indicate that cadmium and bismuth were relatively volatile, with an
average of less than 40 percent discharged with the kiln ash. 'Arsenic, barium, chromium,
copper, lead, magnesium, and strontium were relatively nonvolatile, with an average of greater c
than 80 percent discharged With the kiln ash. Observed relative metal volatilities generally
agreed with the volatilities predicted based on vapor pressure/temperature relationships, with
the exception of arsenic which was much less volatile than predicted. The volatility of cadmium,
bismuth, and lead increased as kiln temperature was increased; the discharge distributions of the
remaining metals were not significantly affected by changes in kiln temperature. Apparent
scrubber collection efficiencies for the metals averaged 22 to 71 percent, and were generally
higher for Ihe less volatile metals. The overall average metal collection efficiency was 43 percent.
17. ' • KEY WORDS AND DOCUMENT ANALYSIS
J. DESCRIPTORS
b. IDENTIFIERS/OPEN ENDED TERMS
C. COSATI Field/Croup
Incineration
Hazardous Waste
Trace Metals
Partitioning
Particle Size Distribution
Air Pollution Control Equipment
Emissions
18. DISTRIBUTION STATEMENT
RELEASE TO PUBLIC
1'J. SECURITY i.LASS fThil fitportl
UNCLASSIFIED
21. NO, OF PAGES
267
20. SECURITY CLASS iTh/i ptfti
UNCLASSIFIED
22. PRICE
------- |