EPA/600/2-90/043b
September 1990
THE FATE OF TRACE METALS IN A
ROTARY KILN INCINERATOR WITH
A VENTURI/PACKED COLUMN SCRUBBER
Volume II — Appendices
By
D. J. Foumier, Jr., W. E. Whitworth, Jr., J. W. Let, and L. R. Waterland
Acurex Corporation
Environmental Systems Division
Incineration Research Facility
Jefferson, Arkansas 72079
EPA Contract No. 68-03-3267
Work Assignments 2-1 and 3-1
EPA Project Officer Robert C. Thumau
Technical Task Manager: Gregory J. Carroll
Waste Minimization, Destruction and Disposal Research Division
Risk Reduction Engineering Laboratory
Cincinnati, Ohio 45268
RISK REDUCTION ENGINEERING LABORATORY
OFFICE OF RESEARCH AND DEVELOPMENT
U.S. ENVIRONMENTAL PROTECTION AGENCY
CINCINNATI, OHIO 45268
-------
DISCLAIMER
The information in this document has been funded by the U.S. Environmental
Protection Agency under Contract No. 68-03-3267. It has been subjected to the Agency's peer
review and administrative review, and it has been approved for publication as an EPA document.
Mention of trade names or commercial products does not constitute endorsement or
recommendation for use.
ii
-------
FOREWORD
Today's rapidly developing and changing technologies and industrial products and
practices frequently carry with them the increased generation of materials that, if improperly
dealt with, can threaten both public health and the environment. The U.S. Environmental
Protection Agency is charged by Congress with protecting the Nation's land, air, and water
resources. Under a mandate of national environmental laws, the agency strives to formulate and
implement actions leading to a compatible balance between human activities and the ability of
natural systems to support and nurture life. These laws direct the EPA to perform research to
define our environmental problems, measure the impacts, and search for solutions.
The Risk Reduction Engineering Laboratory is responsible for planning, implementing,
and managing research, development, and demonstration programs to provide an authoritative,
defensible, engineering basis in support of the policies, programs, and regulations of the EPA
with respect to drinking water, wastewater, pesticides, toxic substances, solid and hazardous
wastes, and Superfund-related activities. This publication is one of the products of that research
and provides a vital communication link between the researcher and the user community.
This report describes an extensive series of tests conducted at the EPA's Incineration
Research Facility to evaluate the fate of trace metals fed to a rotary kiln incinerator. For
further information, please contact the Waste Minimization, Destruction and Disposal Research
Division of the Risk Reduction Engineering Laboratory.
E. Timothy Oppelt, Director
Risk Reduction Engineering Laboratory
iii
-------
ABSTRACT
A 5-week series of pilot-scale incineration tests, employing a synthetic waste feed, was
performed at the U.S. Environmental Protection Agency's (EPA) Incineration Research Facility
(IRF) to evaluate the fate of trace metals fed to a rotary kiln incinerator equipped with a venturi
scrubber/packed column scrubber. Completed were three tests to evaluate the valence state of
chromium in emissions and discharges as a function of valence state in the feed and feed
chlorine content, and eight tests to evaluate the fate of five hazardous constituent and four
nonhazardous constituent trace metals as a function of incinerator operating temperatures and
feed chlorine content.
Chromium test results indicated that when no chlorine was present in the feed, 95
percent of the measured chromium was discharged in the kiln ash, 1 to 2 percent in the scrubber
exit flue gas, and 3 percent in the scrubber Liquor. With chlorine in the feed, these fractions
were 84, 4, and 11 percent, respectively. Kiln ash contained negligible Cr( + 6) for all tests.
Scrubber exit flue gas Cr( + 6) as a fraction of total chromium was nominally 15 percent with no
feed chlorine, increasing to about 50 percent with chlorine-containing feed. The scrubber liquor
Cr( + 6) fraction was 20 to 30 percent with Cr( + 3) feed, increasing to about 60 percent with
Cr( + 6) feed.
Parametric trace metal test results confirm that cadmium, lead, and bismuth are
relatively volatile metals, based on normalized discharge distribution data. Less than 32 percent
of these metals were discharged in the kiln ash. Barium, copper, strontium, chromium, and
magnesium are relatively nonvolatile, with greater than 75 percent of their discharge amounts
present in kiln ash. Surprisingly, arsenic was found to be relatively nonvolatile. Apparent
scrubber collection efficiencies generally correlated with observed volatility. Volatile metals
exhibited collection efficiencies of 36 to 45 percent; nonvolatile metals, with the exception of
copper, exhibited collection efficiencies of 49 to 88 percent. Feed chlorine content had a major
effect on the observed volatility of cadmium, lead, and bismuth, with volatility increasing with
increased feed chlorine content. Afterburner exit flue gas particle size distributions shifted to
smaller size when chlorine was added to the feed.
The average mass balance closures around the kiln ash/scrubber discharge ranged from
48 to 96 percent for individual metals. Overall average closure was 71 percent. From past
experience, trace metals mass balance closure results for combustion sources are in the 30 to
200 percent range.
This report was submitted in fulfillment of Contract Number 68-03-3267 by Acurex
Corporation under the sponsorship of the U.S. Environmental Protection Agency. This report
covers work conducted during August and September, 1988.
iv
-------
TABLE OF CONTENTS
FOREWORD iii
ABSTRACT iv
APPENDIX A—INCINERATOR OPERATING DATA 1
APPENDIX B—ANALYTICAL LABORATORY REPORTS 46
APPENDIX C—SAMPLING TRAIN DATA SHEETS 187
APPENDIX D—VOST GC/FID ANALYSIS PROCEDURE 229
-------
APPENDIX A
INCINERATOR OPERATING DATA
1
-------
lest S
8-25-81
'-lay
Retals
Feed
Feed
Feed
Klin
Kiln
Kiln
lino
Hclqht
Height
Nntals
Exit
Gas
Air
Reading
Reading
Rotameter
Te«p
Ho.
Flo*
(lbs)
(lbs)
( f)
(scfh)
(r.c(h)
1045
321.0
IS 4
0
1553
450
12B50
1100
310.0
15.2
0
1416
260
6470
IMS
275.5
14.6
11
1436
210
(180
1110
210.S
13.9
II
1426
210
6230
IKS
20S.S
13.4
II
1480
220
6440
1200
l/l 0
13.0
II
1481
220
6470
1 ? IS
170.0
12.5
11
1979
210
6410
mo
326.0
12 0
II
1488
220
6410
1245
251.S
11 5
11
1S06
220
6470
1300
259 5
10.9
II
1510
200
5990
ISIS
223 0
10 3
11
1512
210
6180
13)0
188 S
9.8
II
1541
200
S600
1345
151 0
9.3
11
1548
190
5410
1100
361.0
8.9
II
1543
170
5050
141S
324. S
8.4
II
IS22
180
5050
1430
289.5
8.0
II
1509
170
5050
IMS
255 0
1.1
M
1509
110
5220
ISOO
220.0
7.4
II
I48S
180
5280
ISIS
186.0
7.1
11
ISIS
200
5760
IS30
I50.S
7 4
II
1528
190
5280
IS4S
115.0
1.1
II
1S33
180
5280
1600
80.0
6.7
II
1536
180
5310
16IS
118.0
6.1
11
1523
170
4810
1610
82.S
S.I
II
IS28
170
5050
1645
61 S
S3
0
1512
310
12140
Avg:
215 4
9 9
9.7
1524.8
211.6
6255.6
Hln:
67.5
S3
0.0 1416.0
170.0
4810 0
Max:
361.0
15.4
II.0
1979.0
450.0
12850.0
Make-up
BloNdonn
VentuM
Venturl
Packed
Packed
Liquor
Liquor
10 Fan
Hatnr
Hjter
F Ion Pressure
Coluim
Coluwi
pH
Imp
Inlet
tun.
Flo* Pressure
(gal)
(gp»)
(gp«)
(•«)
Cop®)
(•«)
<°F>
(V)
7933
0 7
18
23.0
31
1.0
6.92
162
22.0
8003
0.7
18
23.0
31
1.3
6.60
163
22 0
8060
0.7
18
22.0
31
1.0
1.69
164
22.0
8121
0.7
18
22.0
31
2.0
7 53
164
22.0
8188
0.7
18
22.0
31
2 0
6.00
163
22.0
0231
0 7
18
22.0
31
2.0
3.30
164
22.0
8303
0.7
18
22.0
30
2.5
6.60
164
22 5
8363
0 6
18
22.0
30
2.5
6.70
164
22.5
8419
0.6
18
22.0
30
2 5
7.20
164
22 5
8414
0 6
17
21 S
30
2 5
5.40
164
22.0
8527
0.6
17
21.5
30
2.5
8.30
165
22.0
8596
0.5
18
21.0
30
2.5
7.40
166
22.0
8653
OS
IB
21.0
30
3.0
6.90
166
22.0
8707
0.5
18
21.0
30
10
1.80
166
22.0
8767
0.5
18
21.0
30
3.5
• 50
167
22.0
8828
0.5
IS
21.0
31
3.S
4.45
164
22.0
8084
0.5
18
21 0
30
4.0
S.40
164
22.0
8743
0.5
18
21.0
30
4.0
7.10
164
22.0
9002
0.5
18
20.0
30
4.0
6.96
164
22.0
9057
0.5
18
20.0
32
4.0
7.17
164
22.0
9120
0.5
18
20.0
30
4.S
6.78
164
22.0
9172
OS
18
20.0
30
4.S
1.34
164
22.0
9230
0.5
18
20.0
30
4.5
1.02
164
22.0
9289
0.5
18
20.0
30
4 5
6.81
164
22.0
9344
0.5
18
19.0
30
S.O
6.82
164
23.0
86JR.4
0.6
17.9
21.2
30 4
3.1
6 83
164.2
22.1
7933.0
0.5
17.0
19.0
30.0
1.0
3.30
162.0
22.0
9344 0
0.7
18.0
23.0
32.0
S.O
8.80
167.0
23.0
-------
Test 5
8 75-88
Kiln
AB
Quench
AB
AB
AB
Pressurn
Pressuro
Water
Exit
t»lt
txit
1 Kit
Flo*
07
CU
CO?
U1IIC
(•«)
C«)
(qp»)
(t)
(pH
0)
(pp«)
0.040
0 70
17
8 3
0 0
7 6
0 J
0 0)0
0 70
17
0.9
0.0
7 7
•0 7
0.030
0.70
17
9.3
0 0
0.4
-0 1
0.030
0.70
1?
0.6
0.0
8 2
0 3
0.070
0 08
17
1.0
0.0
8 6
0 1
0 025
0.18
17
0 4
0.0
7.8
0 9
0 035
0 70
17
I.J
0.0
7.7
0 7
0 030
0.10
17
9 0
0.0
7.9
0.8
0.035
0 14
t7
1.1
0.0
7 9
0 9
0 035
0. IB
17
9.7
0 0
7.7
0 9
0.035
0.16
17
9.1
0.0
7 4
0.6
0.030
O.IS
17
9.6
0.0
7.1
0.4
0.030
0.16
17
9.9
0.0
7 0
1?
0.030
0 16
17
13.3
0.0
5 7
7 9
0.030
0 16
17
17.9
0.0
4 9
3 7
0.030
0.16
17
13.6
0.0
5?
7.8
0.030
0 16
17
7.1
0.0
8 6
19
0.030
0.16
17
7.1
0.0
8 4
18
0.035
0.16
17
7.1
0.0
8.4
2 0
0.035
0.16
17
7.7
0.0
8.3
1.7
0.040
0.16
17
7.S
0.0
8.8
I.I
0.040
0.16
17
7.6
0 0
1.6
1.6
0.040
0 16
17
7 7
0.0
8 3
1.9
0.040
0.16
17
7.0
0 0
8 3
16
0.050
0.16
13
5 1
0.0
7 6
16
0.033
0.17
17.0
II
0.1
7 7
1.4
0.070
0.00
17.0
S.I
0 0
4.9
¦0.3
0.050
0.70
13.0
13 6
0.0
8 8
7.9
jbbnr
Scrubbe
Scrubber
Scrubber
Scrubber
Stack
Stock
Stack
Stack
[*lt
Exi
txit
fcult
Exit
07
CO
C07
HIHC
CD
CO
NOx
HIHC
U1IIC
PP«)
(\
(PP»)
(PP»)
(PP»)
(*>
(ppa)
(V
(ppa. CH4)
0 0
5
0 0
2 9
-0.4
11.8
0.0
0.0
0.6
0 0
5
0.0
0.4
0.7
11.9
0.0
0.0
OS
0.0
5
44.0
0 6
0.0
11.8
0.0
0.0
0.5
0 0
5.
41 0
0.8
0 7
11.1
0.0
0.0
0.7
0.0
5
37.0
0 2
0.9
119
0 0
0.0
1.1
0 0
5.
46 0
0.4
0.7
11.9
0.1
0.0
0.1
0 0
5.
46 0
0.9
1.0
11.9
0.0
0.0
1.0
0.0
4
47 0
-0.2
0.7
III
0.0
0.0
0.5
0 0
5.
bl 0
-1.1
0.7
11.7
0 0
0.0
0 8
0.0
5
49.0
DO
0.0
17.0
0.0
0.0
0.1
0 0
5.
52 0
-0.3
0 2
11.1
0.0
0.0
0.2
0 0
5
48.0
-0 2
0.3
17.1
0.0
0.0
0.8
0 0
5
50 0
-0.3
0 7
17.7
0.0
0.0
0.8
0.0
5
50.0
-0 1
0.6
17 3
0.0
0.0
0.7
0 0
5.
48 0
-0.6
0.4
12.7
0.0
0.0
0.7
0.0
5
49.0
-0 6
0.2
17.1
0.0
0.0
0.6
0 0
5
47 0
0.8
0.4
17 1
0.0
0.0
0.7
0 0
5
46.0
-1.9
0.3
17.2
0.0
0.0
0.7
0 0
5
410
-0 6
0.5
17.7
0.0
0.0
0.4
0 0
5
45 0
-0 1
0.7
17.3
0.0
0.0
0.5
0.0
V
43.0
-7.7
-0.1
13.4
0.0
0.0
0.7
0.0
5
54 0
-1.7
0.7
11.9
0.0
0.0
0.6
0 0
5
55 0
-0.9
0.0
12.1
0.0
0.0
0.9
0.0
5.
54.0
19
0.1
17.1
0.0
0.0
0.3
0.0
5
510
-18
0.3
17 5
0.0
0.0
0.1
44 0
-0.7
0.3
17.1
0.0
0.0
0.5
0.0
2.7
•0.4
11.7
0.0
0 0
0.1
55 0
2.9
1.0
13.4
0.0
0.0
1.1
-------
lest 7
9 30-88
Clay
Metals
feed
Feed
Feed
Kiln
Kiln
Kiln
At)
AS
AB
Make-up
Bloodmn
Venturl
Venturf
Packed
Packed
Liquor
Liquor
ID Fan
IlM
Height
Height
Metals
Exit
Gas
Air
tx It
UaS
Air
Hater
Hater
flow Pressure
Coluan
Coluan
P«
leap
Inlet
Reading
Reading Rotorctor
leap
Flo.
Flax
leap
Flo*
Ho«
Cu»
flo» Pressure
(lbs)
(tlw)
(°f)
(sclh)
(scfh)
(°F)
(scfh)
(scfh)
(gal)
(gpn)
(«P»)
Cwc)
(OP*)
(V)
(°F)
C«)
910
387.5
18.9
0
1597
410
14140
2004
610
190(0
5472
15
19
10.0
30
13.0
7.14
163
71.0
MS
387 S
18.9
0
IS87
330
12140
1997
610
19060
5S49
IS
19
28.0
30
10.5
7.09
163
35.0
1000
307.5
18 0
0
146?
380
14030
1911
630
19060
5615
1.5
19
28 0
30
10.5
7.06
161
35.0
1015
381 5
18.7
0
IS83
430
IS4b0
1995
630
19060
5687
15
19
78.0
30
10.s
6.98
163
35.0
1030
307 5
18 7
0
1599
470
14850
1994
600
19060
5759
0.6
19
74.0
30
13.0
7.10
162
34 0
104S
363.5
18.5
II
1606
290
10750
2004
610
19060
5816
OS
19
73.0
30
I4.S
1.11
165
33.0
1100
378.5
IB 1
11
1600
760
9300
1998
630
19060
5878
0.5
19
73 8
30
14.0
6.3S
165
33.0
1115
793.0
17.8
II
1613
270
9540
1985
630
19060
5942
0 4
14
73.0
30
13.5
7.97
I6S
33 0
1130
»• s
17.3
11
1604
760
9090
1907
630
19060
6005
0.4
18
73.0
29
14.0
8.94
165
33.0
IKS
72S.S
16.9
II
1605
2 60
9800
1984
630
19060
6069
0.4
18
77.0
29
13.5
7.78
165
37.0
1700
108.5
16.6
11
1605
260
9070
1984
630
19060
6130
0.4
18
77.0
29
13.0
8.29
165
33.0
12 IS
157 0
16.1
11
1671
260
9300
1992
630
19060
6194
0 4
18
72 0
29
12.0
6.02
166
31.0
1230
119.0
IS 7
11
1610
740
8830
1996
630
19060
6247
0.4
18
27.0
79
12.0
1.14
166
31.0
IMS
84 S
IS 3
II
1614
740
8598
1896
6)0
19060
6308
0.4
18
22.0
79
11.5
7.04
165
11 0
1300
378.5
14.7
11
1607
730
8590
1993
630
19060
6380
0.4
18
73.0
79
12.5
7.42
165
31.0
1315
341.5
14.7
11
1613
740
8570
1992
630
19060
6443
0.4
18
73.0
79
12.0
6.76
165
31 0
1330
306.5
13.7
11
1618
740
8590
1992
630
19060
6506
0.4
18
72.0
79
12.0
1.04
165
31.0
1345
771.5
13 7
II
1670
750
0810
1993
630
19060
6565
0.4
18
77.0
29
12.0
6 66
165
31.0
1400
236.0
17.8
11
1619
740
8370
1995
630
19060
6628
0.4
18
73.0
79
12.S
7.21
161
31.0
MIS
701.0
17 3
11
1608
230
8120
1994
630
19060
6688
0.4
18
73.0
79
17.0
7.07
I6S
31.0
1130
166.0
11.9
II
1616
730
8120
1994
630
19060
6749
0.4
18
73.0
29
11.5
7.16
165
31.0
IKS
130 0
IIS
11
1619
730
8170
1993
630
19060
6814
0.4
18
73.0
29
12.0
7 20
165
31.0
IS00
125.0
11.6
0
1563
350
17770
1976
630
19060
6871
0.4
18
23.0
29
11.5
7.15
164
31.0
*vq:
765.5
IS 7
II
1599.5
784 8
10193.0
1984 5
677.0
19060 0
6187 6
0 6
18.1
72.8
29.3
12.3
1.21
164.3
31.7
Bin:
84 5
11. S
0.8
1467.0
730 0
8170 0
1896.0
600 0
19060.0
5472 0
0.4
14.0
10.0
29.0
10.5
6.02
161.0
21.0
Max:
387.5
18.9
II.0
1671.0
430.0
15450.0
7004.0
630.0
19060.0
6871.0
1.5
19.0
28.0
30.0
14.5
8.94
166.0
35.0
-------
Teit 7
830-88
«»0
Nln
hi
Kiln
AB
Quench
ts
ab
AB
11)
Pressure Pressure
Mater
txlt
Exit
[nil
C»lt
Flo*
02
CO
CO?
UIHC
C«)
C-c)
(W«)
(t)
(PK-)
(1>
(PP»)
0 070
a.?o
12
15
0.0
7.t
!.B
8.020
O.JO
12
i.o
0 0
7 2
0.1
e.ota
0.70
12
n
0.0
7 *
0.1
0.040
0.20
12
1.0
0.0
1.9
0 2
1.021
0 70
12
M
0 0
7 6
0 0
0.0)0
0 22
12
7.5
0.0
0.7
0.2
0.0)0
0.10
12
1.0
0.0
O.J
0.3
0.0)0
0.21
12
7.5
0.0
0.9
0.7
0.0)0
0 22
12
7.7
10
a.s
0.9
0.020
0 2?
12
7.9
0.0
o.t
0.5
0.0)5
0 ?I
12
II
0.0
ii
0.7
0.8)0
9 22
12
7.1
0.0
8.7
0.6
0.0)0
0 22
12
7 5
0.0
8.6
0.7
0.9)0
0.22
12
7.1
O.D
0 7
5.2
0.0)0
0.22
12
It
0.0
8.1
1.7
0.0)0
0 21
12
1.0
1.0
II
0.9
0.0)0
0 22
12
7 1
0.0
a.i
O.S
0.0)0
0.22
12
7.S
0.0
1.5
0.8
0.0)5
0.22
12
7 1
0.0
II
0.7
0.0)5
0.22
12
7.9
0 0
0.2
0.9
0.0)5
0 22
12
7 9
0.0
IS
1.0
0.0)0
0.22
12
7.1
0.0
a.i
1.5
0.040
0.22
12
9 1
0 0
7.1
1 >
: 0.0)0
0.21
12.0
a.o
0.0
1.2
1.0
¦ 020
0 00
(2.0
7.5
0.0
7.1
1 0
OHO
0.22
12.0
9.1
1.0
8.9
5.2
Uln Scrubbrr Scrubber Scrubber Scrubber Scrubber Stick Suck Stack Stack
0
*
Uit
Exit
Cxit
Exit
Exit
02
CO
CU2
HIHC
CO
CO?
HOx
NIHC
UIHC
(ppn)
U)
(PP«)
(PC")
(Pt»)
<*)
(Pf»)
HI
(pp«. CHI)
Kt.'SIKi:
:c»*r*rs*s:
rS = = =38SS3:
issrss
cr:=xrBZ3SB
0 0
5.3
15 0
0 4
2.1
12 3
310
7.9
0.2
0 0
4.9
19 0
0 3
2.5
12.8
)I.O
7.7
0.1
0 0
0.2
19 0
0 9
2.5
12.4
20.0
7 5
0.4
0 0
5.)
19.0
0 3
2.2
12.1
28.0
8.2
0.2
0.0
5 3
u.o
0 1
1.9
12.)
0.0
8.5
-0.7
0.0
to
51.0
-0 2
2.2
11.7
17.0
9.1
0.2
0 0
6 0
19.0
•0 1
1.9
11.9
2) 0
7.9
-0.2
0 0
e.i
51 0
32.5
2.0
11.6
0.8
8 8
-0.2
0.0
5 8
51.0
2 5
1.9
12.2
14.0
8.8
0.0
5.8
19.0
1.2
1.7
12.1
0.8
7.8
0.5
0.0
5.9
SJO
0.7
t.I
12.1
0.0
8 0
-0.)
0.0
It
45 0
-0.2
2 3
13.7
0 0
7.4
0.3
0.1
1 9
IS 0
-0 3
2.1
13.7
0.0
7 4
0.2
0 0
5 0
15 0
8.7
3.0
13.1
0.0
6.7
0.4
0.0
5 5
52 0
-0.2
2.7
12.5
2.0
5.6
-0.2
2 0
5 7
51.0
1.5
2.0
12.6
2.0
8 I
-0.2
2.0
5.6
52.0
o.o
18
12.5
0.0
2.9
0.8
0.0
5 7
5).0
0 2
1.9
12.1
0.0
7.5
0.5
0 0
5 5
5) 0
-0.1
1.7
12.8
0.0
7.4
-0.2
0.0
5 7
51.0
0.0
1.8
12.5
0.8
7.8
-0.1
0.0
5.8
52 0
0.0
2.0
12.4
0.0
7.4
-0.2
0 0
5 7
51 0
-0 5
1.7
12.1
0 0
7.0
0.0
0 0
< 9
54.0
-0 6
1.9
13.1
0.0
6 8
0.6
0.2
5 )
50.0
1.6
2.1
12. 5
7.4
7.7
0.0
0 1
0 2
45 0
-0 1
1.7
II.»
0.0
5 6
-0.7
2.0
6.1
54.0
32.5
3.0
13.8
34.0
9.1
0.6
-------
Test I
9-7-88
Clay
Natal*
Feed
Feed
Feed
Klin
Kiln
Kiln
AB
AB
AS
Make-up
Slowdown
Venturl
Venturl
Packed
Packed
Liquor
liquor
ID Fan
f 1ae
Height
Nelqht
Kotals
Exit
Gas
»lr
Lxlt
Air
Ma tor
Hater
Mo* Pressure
Colum
Colum
P«
leap
Inlet
Reading
Reading
Rotameter
leap
Flow
F Ion
leap
Ho.
Flow
tun
Flow Pressure
(lbs)
(lbs)
(°F>
(scfh)
(scfh)
(°F)
(scfh)
(scfh)
(gal)
(gp»)
(flP»)
(*«)
(gp«)
(•«)
<°F>
C«)
»tu;
=>"!"«
ntsssxsesi
--------
---------
----------
1030
3(7 0
17.0
0
1(82
590
15900
7700
630
1(7(0
13(7
2 5
. 18
21.0
30
13.0
7.24
166
32.0
1015
366.0
17.0
0
15(8
370
9980
2190
610
1(750
l(«6
OS
18
21.0
30
13.0
7.12
167
32.0
1100
333.5
17 4
11
l(l(
320
8390
2I9(
(30
1(7(0
1513
0.5
18
71.0
30
13.5
7 18
167
32.0
MIS
791.0
17.0
11
1(09
370
8350
2192
(30
1(700
1581
0 5
18
71 0
30
13.5
8.12
167
32.0
1130
763.5
16.1
11
KOS
310
8120
2166
(30
1(700
1(((
0.5
18
21.0
30
1(0
6.11
168
32.0
IMS
278.5
16.(
11
1593
300
8160
2K8
630
1(710
1712
0 5
18
21.0
30
13.8
7 13
167
32 0
1200
195.0
16.3
11
IS79
330
8890
7159
630
15900
1778
0.5
11
21.8
30
M.O
1.1?
167
32.0
ISIS
307.0
16 0
II
159)
350
9170
7170
630
15890
18(2
0.4
18
20.0
30
1(0
7.12
167
32.0
1730
355.0
15.1
11
IS9T
3(0
9170
7175
(30
15880
1906
0 4
II
20.0
29
MS
7.09
1(1
32.0
IMS
377.0
IS 4
11
1(16
3(0
9(10
7181
630
158(0
I9((
0 4
18
70.0
29
14.5
T. 26
1(8
32.0
1301
70(5
1(9
II
1(06
310
8710
7185
(30
ISR90
203(
0 4
18
20.0
29
14.5
7.34
1(7
32.0
1315
250. S
l( 4
II
1598
310
7990
7135
(JO
15850
209/
0.(
18
20.0
29
14.5
7.76
168
32.0
1330
215.0
13 9
11
1603
310
8050
7189
(30
15900
2160
0.3
18
19.0
79
14.5
7.71
1(8
31.0
1315
179.5
13.5
It
1587
300
8000
2180
(JO
15880
222(
0.3
18
19.0
79
ISO
6.(0
1(9
31.0
1(00
1M.0
13.1
11
I59(
300
7970
2178
(30
15850
2285
0.2
18
19.0
29
ISO
6.25
1(7
3(.0
IIIS
757.5
12.8
7
1586
350
9(50
2194
(30
15870
23(7
0.7
18
19.0
29
ISO
7.(1
1(9
3(0
1(30
721.5
12.6
7
1600
3(0
9770
2198
(30
15850
2(15
0.6
IB
19.0
29
15.0
7.(9
160
39.0
l((S
116.0
12.6
0
1603
3(0
89/0
2701
610
15800
2(8(
OS
18
19.0
30
15.0
7.IS
1(8
33.5
ISOO
1(9.0
12.0
0
1(21
330
87(0
7705
(30
157(0
2550
0.(
18
18.5
30
15.0
(.96
1(8
33.0
1515
IKS
11 7
0
1(32
3(0
9000
2210
(10
15800
2616
0.3
18
18.5
30
IS.O
7.29
1(7
32 S
IS30
79.0
17.3
II
1621
330
8800
2212
(30
15780
767(
0.3
18
18.5
30
15.0
7.10
1(7
32.5
15(5
0.0
0.0
0
1(03
(70
111(0
2202
(JO
15850
2139
0.3
18
18.S
30
15.0
7.16
167
32.5
Avg:
237.3
1(3
7.(
160(9
3(3 2
9151.(
2187.5
630.0
15950.0
20(2.6
0.5
18.0
19.8
29 6
14.4
7.IS
1(7.5
32.6
Hln:
0.0
0.0
0.0 1568.0
300.0
7910 0
2M8.0
630 0
157(0 0
13(2.0
0 2
18.0
18.5
29.0
13.0
6.18
1((.0
31.0
Rax:
367.0
17.8
11.0
1682.0
590.0
15900.0
2212 0
(30.0
1(760 0
2739.0
2.5
18.0
21.0
30.0
15.0
8.12
169.0
39.0
-------
lest I
9-7 8(1
Kiln
46
Quench
AB
(8
to
A8
Pressure Pressure
Water
Exit
Exit
L* It
Flcm
0?
CO
CO?
UIHC
(V.)
C«)
(«P«)
(*)
(pp»)
It)
(PP»)
0 075
0.17
IS
5 f
0 0
9 5
0 7
0.070
0.17
15
7.0
0.0
8 8
-0.1
0.070
0.17
IS
(0
0 0
9 8
-O.J
0.070
0.17
IS
6.7
0.0
9 6
-0 4
0.070
0.17
IS
ii
0.0
9 7
-0.7
0.070
0.17
IS
6 5
0 0
9.4
-0 7
0.070
0.17
IS
6 3
0.0
9 6
-0.3
0.070
0.17
IS
SO
0.0
9 7
•0.5
0.070
0.17
IS
(.0
0.0
10 0
0.6
0.070
0 1?
IS
5.7
0.0
9.9
0 7
0.070
0.17
IS
SO
0 0
9 9
-0 7
0.070
0 17
1S
s»
0.0
9 8
0.4
0.070
0 17
IS
S.J
0 0
9.7
0 7
0.070
0.17
IS
6 3
0.0
9 7
0?
0.070
0.17
IS
5.5
0.0
10.0
-0 7
0.070
0.17
IS
SI
0.0
10.?
0.7
0.070
0.17
IS
5.5
0.0
10 3
0.1
0.070
0 17
IS
5.4
0.0
10?
-0.3
0.070
0.17
IS
5 6
0.0
10 3
0.7
0.070
0.1?
IS
S 5
0.0
10 3
0.3
0.030
0 1?
IS
5 8
0 0
8.3
-0 1
0.030
0. IS
IS
7.J
0.0
8.3
0.4
0.071
0 1?
15 0
(.0
0.0
9.7
-0.1
0.070
0.1?
ISO
SI
0.0
8.3
-0 6
0.010
O.IS
ISO
7.3
0.0
10.3
0.7
Kiln Scrubbpr Scrubbc
Scrubber Scrubber Scrubber
Stack
Stack
Stack
Stack
Exit
Exit
Cxi
Exit
Exit
Exit
0?
CO
CO?
HTHC
07
to
CO
NOx
H1HC
UIHC
(\)
(ppn)
U
(ppn)
(PP»)
(PP«)
<*)
(PP")
(t)
(PP«. CH4)
12.7
0.0
6
71.0
7 1
0?
10.8
71.0
13 8
-0 4
14
0 0
6.
70 0
17
0.5
11 9
35 0
13 3
-0.3
1? 5
0 0
i
71 0
0 9
0.7
10 9
70.0
14 0
0 0
17 8
0.0
6
71.0
IS
0.5
11.0
71.0
14.S
-0.1
i j a
0 0
6
67 0
0.9
0 4
11 7
43.0
14 3
0.0
13.9
0 0
6.
70.0
0.4
0.4
11.4
30.0
13.9
0.6
14
0 0
6.
76 0
0.7
0 1
11.3
19.0
13.4
0 7
13.9
3.0
6.
76 0
0.4
0.6
11 3
?6.0
14.5
OS
14 0
3.0
6.
77.0
0.1
0.7
II.?
3S.0
14.1
0 6
13 6
7.0
6.
83 0
1.0
0.4
11.1
73.0
15.0
0.8
13 9
3.0
6
84.0
0 8
0.0
II.0
76.0
14.3
0.6
14 0
3 0
6.
77 0
0.5
-0.1
11.1
7.0
14.6
1.1
13 8
3 0
6
88.0
1.4
0.1
III
0.0
14.9
-0 1
14.0
3.0
6
79 0
0.5
0.0
11.1
0.0
14.6
0.3
14 0
10
6.
75.0
0.6
0.7
11.4
0.0
14?
0.8
1? 9
3.0
6.
73.0
1.4
0.3
10.7
14.0
14 0
1.1
13 7
3.0
6.
73.0
0.3
0.7
10.8
13.0
14.6
O.S
13?
7.0
6
87.0
1.1
0.1
10.9
3.0
14.6
IS
13.0
3 0
6
67.0
1 7
0.7
II 0
7.0
IS 0
1.4
13 0
7.0
6.
77.0
0 6
-0.1
11.0
9.0
14.9
1.0
13 3
7 0
5.
117.0
0 1
0.8
113
4.0
17 6
0.0
13 9
7.0
5.
78.0
0.8
0.0
11.5
3.0
12.8
-0.6
13 5
7.0
6
77.4
0.8
0.7
11.1
16.1
14.2
0.4
17.7
0 0
5.
67.0
0.1
-0.1
10.7
0.0
17.6
-0.6
14 7
7 0
6.
117 0
?.l
0.8
11.9
43.0
ISO
IS
-------
Test 9
9-9-88
Clay
Ratals
Feed
Feed
Feed
Klin
Kiln
Kiln
Ki In
AD
[ lae
Helqht
Helqht
Nctals
E«lt
Gas
Air
Aux Mr
txit
Reading
Reading
Rot meter
leap
Flo.
Flrn
FIdh
lemp
(lbs)
(lbs)
<°F)
(scfh)
(scfh)
(scfh)
(°F)
908
382.0
IT 9
0
1587
390
12570
0
1627
9IS
3S7.0
17.9
0
1631
410
12/90
0
1792
930
38?. 0
17.9
0
1587
380
11680
0
1813
94$
382.0
17.9
0
I59S
380
11950
0
1816
1000
382.5
17.9
0
1584
380
11900
0
1816
1015
382.5
0.0
0
1594
390
11390
0
ISIS
1030
382.5
13.8
0
1586
400
12130
0
1815
1045
383.0
13.2
0
1575
400
12190
0
1811
1100
365.0
12.7
11
1640
280
7680
7775
1788
IMS
330 0
13 4
11
1649
220
7880
7791
1112
1130
294.5
12.2
II
1600
220
7650
77R9
1797
IMS
260.0
11.9
II
1(03
220
7410
77(5
1799
COO
225.0
11.(
11
1598
230
7510
7766
1799
12 IS
190.0
11.3
II
1611
220
6940
77/5
1801
mo
iss.s
10.9
11
160t
220
8100
7763
1802
1245
116.0
10.6
II
1611
220
8360
7165
1805
1300
242.5
10.3
11
1611
220
8120
7760
1804
1315
308.5
9 9
11
1605
210
7410
7787
1806
1330
274.0
9 5
II
1607
210
7650
7743
1804
I34S
239 0
9.1
11
1608
210
7410
7761
1804
1400
204.0
8 1
11
1612
220
7810
7766
1804
1415
169.5
8 3
II
1605
210
7410
7768
1805
1430
235.0
7.9
11
1611
210
7410
7768
1794
1445
200.0
7.7
11
1611
210
7410
7773
1805
1500
165.0
11
11
1SI7
200
7180
7773
1798
1515
130 0
6.1
II
1603
210
7410
7761
1801
1530
118.0
6.7
0
1614
350
12610
0
1795
*vq:
269 6
11.2
7 3
1605 1
274 1
9109 3
5180.0
11104 7
Kin:
116.0
0.0
0.0
1S75.0
200 0
6940 0
0 0
17B8 0
Nan:
383.0
17.9
II.0
1649.0
410 0
12790.0
7791 0
1827.0
AB
A8
Makeup
filoadovn
Venturl
Venturl
Packed
Packed
Liquor
Liquor
Gal
Hr
Hater
Hater
flo.
Prossure
Colum
Colum
pH
leap
Flo*
Flo.
Cut.
Flo* Pressure
(sdh)
(scfh)
(gal)
(gp«)
(qp»)
C«c)
(0P»)
C«)
(°F)
700
883D
8042
0 5
19
27.0
29
5 0
7.05
162
4)0
13230
8062
0 2
19
27.0
29
5.0
6.99
162
430
13170
8100
0.5
19
27.0
29
5.0
6.96
163
470
13100
8145
0.5
19
27.0
29
5.0
6.90
165
400
12510
8189
0 5
19
26.S
29
5 0
6.88
164
310
12220
8231
0
19
26.5
29
SO
6.85
163
390
11930
8262
0
19
26.5
29
5.0
6.80
163
180
11520
8312
0.5
19
26 5
29
SO
6.82
162
340
12890
8350
0.4
19
27.0
29
6.0
6.It
163
470
19060
8390
0 4
18
20.5
28
7.5
6.16
164
470
19060
8442
0.4
18
24.5
21
7.2
6.36
1f3
470
19060
8483
0
18
24 S
21
T.J
5 91
164
470
19060
8533
0.5
11
25.0
28
1.0
6.12
163
470
19060
0882
0.5
IB
25.0
28
7.0
6.90
163
470
19060
8632
0.5
18
25.0
29
7.0
5.85
1t3
470
19060
8690
0.5
18
25.0
28
7.0
8.03
162
470
19060
8733
0.5
It
25.0
28
1.0
6 66
164
4/0
19060
8781
O.S
18
25.0
28
7.0
7.54
164
460
19060
8830
0.5
18
25.0
21
7.0
7.08
163
460
19060
8878
0.5
IB
25.0
28
7.0
7.01
164
470
19060
8934
O.S
18
25.0
28
7.0
7.46
164
460
19060
8973
0 5
18
25.0
28
7.0
1.20
164
460
19060
9822
0.5
18
25.0
28
7.0
7.60
164
460
19060
9071
0.5
18
25.0
28
7.0
6.87
163
460
19060
9120
O.S
IB
25.0
28
7 0
6.96
163
460
19060
9166
OS
IB
25.0
28
7.0
6 28
164
460
19060
9218
O.S
11
25.0
H
7.0
6.61
165
457.0
16753 5
8610 0
0 4
II 3
25.4
28.4
6 4
6.85
163.4
340 0
8830.0
8042 0
0.0
18.0
20.5
28.0
SO
5.85
162.0
780.0
19060 0
9218.0
0 5
19.0
27.0
29.0
7.5
8.03
165.0
-------
lest 9
9-9-88
ID Fan Kiln IB Quench AB AO «B At)
Inlet Pressure Pressure Hater [*lt lixlt [xtt Lxlt
FIok 0? CO CO? UIIIC
(V) (*«c) (V) (gpa) (*) (ppa) (t) (ppn)
30 0 O.OSO 0.1? 14 9.? 0 0 6 4 0.0
30.0 O.OSO 0 12 11 7.9 0 0 7.9 -0 1
30 0 O.OSO 0.1? 14 8 4 0.0 7 6 0 1
30.0 0 050 0.1? II 8.2 0.0 7.7 0.!
30 0 O.OSO 0.1? II I.S 0.0 7 6 0.?
30.0 0 050 0.12 II 0.6 00 M 0.3
30.0 O.OSO 0 12 II 0.6 0.0 7 1 0?
30 0 0.000 O.IS II 8.7 00 7.3 -0.3
30.0 0.035 0.06 II 7.8 0.0 fl 6 0 1
26.0 0.030 0.08 II 7.2 0 0 1.9 -0.2
30.0 0.030 O.Oi II 8.7 0.0 ft 7 0.6
29.0 0.03S 0.06 II 8.1 0.0 0.1 -0 6
29.0 0.030 0.06 II 1.4 0 0 S.I IS
29.0 0.030 0.06 II 8.7 0.0 8.1 0.1
30.0 0.030 0.08 13 8.5 0 0 0 1 0.2
30.0 0.030 0.08 II 8.5 0 0 8.1 -0.9
29.0 0.030 0.08 II 8 3 0.0 R 3 I I
30.0 0.030 0.08 II 8.8 0.0 8 0 0.1
30.0 0.030 0.01 II 8.5 00 79 1.2
30.0 0.030 0.01 II 1.5 00 7.8 -17
30.0 0 030 0.08 II 8.7 0.0 7 9 15
30.0 0.030 0.08 II 1.7 0.0 7 9 -1.5
30.0 0.030 0.00 II 8 7 0 0 1.9 -14
30.0 0.030 0.08 II 8.7 0 0 7 9 -1 6
30.0 0.030 0.08 14 9.1 10 7.6 -I.S
30.0 0.030 0.01 II 8.9 1.0 7.8 -1 6
30.0 0.03S 0.08 14 9.6 0.0 6.8 -1.6
«vq: 29.7 0.039 0.09 11.0 S.S 0.1 78 0.6
Kin: 26.0 0.030 0.06 13.0 7.2 0 0 6.4 1.7
Hex: 30 0 0.060 0.15 11.0 9.6 1.0 8.9 I.S
Kiln Scrubber Scrubber Scrubber Scrubber Scrubber
Stick
Stack
Stack
Stack
kxlt
lxlt
Exit
txlt
Cult
CxIt
02
CO
C02
HIHC
02
CO
C02
NOx
HIHC
UIIIC
(X)
(PP»)
(»)
(PP»)
(PP*)
(PP»)
(t)
(PP«)
(*)
(pp«, CH4)
14 0
1 0
4.3
0.0
1.3
1.3
13 7
22.0
9 9
0.0
13 0
2.0
5 4
46.0
1.3
1.0
12.5
22.0
12.5
0.2
13 0
0 0
5 2
47 0
0 6
1.0
12 6
13.0
11.7
0.2
13.1
1.0
S3
17.0
-0.6
0 7
12.7
IS 0
12.2
-0.1
13.9
10
1.9
45 0
2.7
0.7
13.0
21.0
117
13.0
13.9
0.0
1.8
43.0
0.2
12
13.1
9.0
11.6
-0.2
13.8
10
1.9
45 0
0 2
1.0
13.1
17.0
11.6
-0.2
13 8
2.0
18
45.0
0.1
1.3
13.3
19.0
11.1
-0.2
11.3
2 0
5 6
47 0
0 6
1.4
12.5
3.0
12.7
0.1
113
1.0
6 2
14.0
1.0
0.7
11.9
10.0
11.2
0.0
12.9
10
5.1
40 0
1.3
0.8
12.9
20.0
12.9
-0.1
12 9
2 0
5 6
12.0
19
-0.3
12.5
0.0
12.9
15
13 7
10
5.6
410
1.1
0.3
12.6
0.0
13.1
-0.1
12.7
3 0
5.7
41.0
16.6
-0.6
12.6
0.0
13.1
-0.2
12 6
2.0
5 6
41.0
20.7
-13
12.5
-11.0
12.7
-0.1
12.5
1.0
5.6
40.0
21.2
-2.0
12.5
2.0
12.2
0.0
12 6
1.0
5 5
40.0
22.8
-2 4
12.6
13.0
13 0
0.0
12.8
2 0
5.6
40.0
27 1
-1.5
12.8
8.0
12.0
0.1
12 7
2 0
5.6
44.0
25.5
-1.9
12.7
14.0
12 9
-0.S
12.7
10
5 5
43.0
25.7
-2.2
12.7
0.0
12.1
I.I
12.6
2 0
5 2
39.0
22.8
-2.5
13.3
0.0
12.0
0.0
12 6
3.0
5.3
44.0
25.1
-2 8
12.6
0.0
12.6
0.2
12.E
3.0
5 1
42 0
25.2
-2.9
12.5
8.0
12.2
-0.2
12 5
0.0
5.7
37.0
2S.5
-3.3
12.6
2.0
12.6
-0.3
12 9
3.0
5 5
42.0
21.2
-3.1
12.7
0.0
12.5
0.0
12 5
2.0
5.6
42.0
33.0
-3.3
12 6
0.0
12.0
-0 2
13.7
2.0
4.8
39.0
21.6
-3 2
13.1
1.0
11.1
0.0
12 9
16
5.3
41 0
12.8
-0.8
12.7
8.0
12.3
O.S
11.3
0 0
4 3
0.0
-0.6
-3.3
11.9
-11.0
9.9
-0 5
14.0
3 0
6.2
17.0
27.1
1.4
13.7
22.0
11 2
13.0
-------
test 4
9-14-00
Clay
Notals
Feed
Feed
feed Klin
Kiln
Kiln
Kiln
AB
I lie
Molqht
Nelqht
Detail Exit
Gas
Air
Auk Air
Uit
Reading
Reading
Rotoaeter leap
Moo
Flow
Hon
lenp
(lbs)
(lbs)
(°f)
(scfh)
(sclh)
(sclh)
(°M
900
384 5
19.6
11 IS07
320
11590
7032
1980
915
349 S
19 3
11 1609
220
7080
7820
1985
1930
315 5
19.0
11 1623
210
7410
7823
1990
I94S
201.0
18. 6
11 1(29
190
6100
1832
1994
1000
0.0
18.3
0 1501
100
(230
7804
1994
HIS
683.5
10 4
II 1517
260
10960
7111
1992
1130
045.0
17 »
II 1605
200
7100
7729
2012
1115
010.0
17 (
II 1603
190
6700
7/38
1999
1700
775.0
17.3
II 1625
100
6230
7729
1991
1715
731 5
17 0
II 1619
180
(230
7718
1989
1230
309.0
15.1
11 1507
110
6470
7707
1996
1245
274.0
16.5
II 1592
1(0
5990
7474
1994
1300
239 0
IS 3
0 1(03
100
5990
7786
1991
1)15
204.0
16 «
II 1606
170
5990
7776
2003
1330
1(9.0
15 0
11 1621
170
5990
7752
2008
13(5
134.5
15.3
II 1614
160
5620
7760
2011
1400
200.0
14.0
II 1606
1(0
57(0
7745
2008
14 IS
174.0
14.5
II 1602
170
5600
7744
2006
1430
139 5
14 0
11 1(10
170
5760
7734
2004
1445
105 0
13.6
0 1(03
170
5760
mi
2002
1500
(9 5
13.1
II 1(02
170
5760
7760
2001
1515
0.0
13.1
0 1599
300
12850
7756
2009
Avg:
335 7
16.5
9 0 1598 3
199.1
7033 2
7754.1
1998.1
Kin:
0.0
13 1
0.0 1507.0
160.0
5620.0
7474.0
1980.0
Max:
003.5
19.6
II.0 1(29.0
300.0
12050.0
7832 0
2012 0
AB
AB
Hake-up Bloodoon
Vpnturl
Venturl
Packed
G«
Air
Mater
Water
Flo*
Pressure
Coluan
1 loo
Floo
Cub.
Floo
(scfh)
(sclh)
(gal)
(BP")
(gp»)
r«c)
(flP«)
510
17990
1645
0.0
10
20.0
20
540
19060
1700
0 0
10
28 0
20
600
19060
1759
0.7
10
25.0
21
600
19060
1820
0.7
10
24.0
20
590
19060
1083
0.7
10
24.0
20
510
190(0
2168
0 7
10
24.0
20
610
19060
2236
0.7
10
24.0
20
580
19060
2294
0.5
18
24.1
21
580
19060
2340
0.5
10
24.0
20
580
19060
2407
0.5
10
24.0
20
580
19060
2465
0.4
10
24.0
20
580
19060
2524
0.4
10
24.0
20
580
19060
2584
0.4
17
24.0
27
600
19060
2630
0.4
17
24.0
27
610
190(0
2693
0.4
17
24.0
21
610
19060
2751
0 4
17
24.0
27
600
19060
2809
0.4
17
24.0
27
590
19060
2067
0.4
17
24.0
27
600
19060
2925
0.4
17
23 0
20
590
19060
2986
0.4
17
23.0
28
600
19060
3041
0.04
17
23.0
21
560
19060
3092
0.04
17
23.0
27
584.5
19011.4
2430.0
0 5
17.5
24.2
27.6
510.0
17990 0
1645.0
0.0
17.0
23.0
27.0
610 0
19060.0
3092 0
0.0
10.0
20.0
20.0
Packed
Coluan
Pressuri
C«
Liquor
PH
liquor
leap
(°f
165.
1(4.
-------
frwt 4
1 11-18
ID Fan
Kiln
Quench
m
*n
AO
Kiln Scrubber Scrubber Scrubber Scrubber Scrubber
Stack
Stack
Stack
Stack
Inlet CrKsure Preisuro
(later
[*it
Lull
C*H
tK f t
Lilt
[nit
l*
-------
lest 6
9-16-81
Clay
Netals
Feed
Feed
Feed
Kiln
Kiln
Kiln
Kiln
AR
Mm
Height
Melqht
Netals
l»lt
Gas
»lr
Aux Air
L* It
Reading
Reading
Rotoaeter
leap
F lo»
Flo*
Flow
7e»p
(lbs)
(lbs)
(°f)
(sclh)
(sclh)
(sclh)
(°F)
1015
392.0
13.1
1
1720
470
16400
0
2012
1030
373.5
12 1
II
1715
330
11430
7906
2016
1045
337 0
12.(
II
1(98
300
10120
7901
1912
MOO
301.0
12 6
11
1707
300
10490
1907
1995
1115
265.5
12.4
11
1671
270
9300
7905
1996
1130
239.5
12.1
11
1(87
270
9710
7906
1993
1145
196.0
11.7
11
1(99
270
9300
7907
1997
1200
Kl 0
11.3
II
1(90
270
9S40
7903
1998
1215
127.0
11 0
II
1(19
270
9540
7903
2000
1230
92.5
10.(
11
1(94
270
9540
7904
2004
1245
302 0
10 9
11
1(91
270
9540
7715
20D2
1300
347 5
9.7
II
1(80
270
9540
7710
1919
1315
312.S
9.3
11
1(94
260
9540
7716
1987
1330
278 0
9.0
II
1(12
270
9540
7702
1991
1345
244.0
S.t
11
1600
200
9670
76S6
1989
1400
209.5
1.2
II
1707
210
10250
769J
7010
1415
175.5
7.9
11
1709
210
10010
7689
2010
1430
152.5
T.7
1310
500
15(40
1694
170)
1445
132.5
7.5
11
1(94
320
11670
7686
1907
1500
98.0
7 4
11
1702
270
9780
7644
2010
1515
(3.5
7.0
II
1(93
270
9780
7637
2003
1530
40.0
6.1
0
1709
420
15450
7647
2013
Avo:
223.7
10.0
9.5
1(11.1
305.0
10752.3
7425.5
1983 9
Kin:
40.0
6 9
0.0
13(0 0
260 0
9300 0
0 0
1701 0
Rax:
392.0
13.1
11.0
1720.0
500.0
16400 0
7907 0
2016.0
AB *8 Make-up Blow)own Venturl Vonturl Packed Packed Liquor Liquor
Gas Mr Mater Hater Flo* Pressure Coluan Coluen pH 7oap
Flow Flo* Cud. FIok Pressure
(scfh) (sclh) (gal) (gpa) (gp») (•*) (gpa) |'k) (°F)
590 19080 S722 OS 17 25.0 25 II.5 7.15 166
590 19060 em 0.2 17 23.0 25 13 5 7.01 166
610 19060 0310 0.5 17 23.0 25 11.0 7.35 166
610 19060 0402 0.5 17 23.0 25 M.O 7.44 166
610 19060 0162 0.6 17 23.0 25 111 (.00 166
610 19060 052S 0 5 17 23.0 25 14.0 7.97 166
610 19060 6507 0.5 17 23.t 25 14.9 6.72 166
610 19060 0650 0 5 17 23.0 25 M.O 6.41 166
610 19060 >710 0.S 17 23.0 25 14.0 6.62 166
610 19060 0774 0.5 17 23.0 2S 14.0 7.05 166
500 19060 0036 0.5 17 23.0 25 14.0 7.20 167
510 19060 8195 0 2 17 23.0 25 14.0 7.27 166
510 19060 0950 0 2 17 23.0 25 13.S (.16 167
580 19060 9002 0.2 17 23.0 25 13.5 6.94 166
580 19060 9067 1.0 17 23.0 25 13.5 7.75 166
(to 19060 9153 1.0 17 23.0 25 13.5 7.08 166
600 19060 9218 0.5 17 23.0 25 13.5 6.60 166
670 16830 9281 0 5 17 23.0 25 15.0 7.42 155
630 190S0 9336 0.5 17 23.0 25 14.0 7.51 167
620 19060 9398 0.4 17 22.0 25 14.0 1.20 167
610 19060 9463 0.4 17 22.0 25 14.5 6.57 1(6
610 19060 9523 0 5 17 22 0 2S 14.5 7.04 167
605 0 18958.6 8868.1 0.5 17.0 23.0 25.0 13.1 7.14 165.7
510.0 16830.0 8222.0 0.2 17.0 22.0 25.0 11.5 6.41 155 0
670.0 19060.0 9523.0 1.0 17.0 25.0 25.0 15.0 8.20 167.0
-------
lest 6
9-16-88
ID Fan Kiln *8 Quench AB AB AH AB
Inlet Pressure Pressure
Hater
Exit
Exit
txf t
Exit
Hon
0?
CO
CO?
tunc
(V)
(•xe)
<•*)
(go«)
(*)
(PP")
<»l
(pp»)
35.0
0.030
0.10
18
7.2
0.0
0.0
1.4
34 0
0.030
0.13
18
(.4
0 0
0 0
1.4
34.0
0.030
0.12
18
7.0
0.0
0.0
17
34.0
0.030
0.12
18
7.5
0 0
9 2
0 6
34.0
0.030
0 12
18
7.4
0.0
9.0
1.5
34 0
0.030
0.12
18
7.4
0 0
8 9
15
34.0
0.070
0.12
14
1.1
0.0
I.I
13
35.0
0 020
0 12
14
7.2
0 0
9.1
1.5
34.0
0.020
0.12
18
1.3
0.0
9 5
1.4
34.0
0.020
0 12
18
6.9
o.o
9 1
1.0
34.0
0.020
0 12
II
1.1
0.0
87 0
14
34.0
0.020
0.12
18
7.6
0.0
8 8
1.4
34.0
0.020
0.12
18
7.5
0 0
8 8
1.4
34 0
0.020
0.12
18
7.6
0 0
8 8
1.4
34 0
0.020
0.12
18
7.6
0 0
8 6
1.2
34.0
0.020
0 12
18
7.4
0.0
8.9
0 9
34 0
0.020
0.12
18
7 4
0.0
8 7
0.6
35.0
0.000
0.12
18
15.9
10 0
3.1
0 2
14 0
0.020
0.12
18
6 3
0.0
9 5
0 1
34 0
0.020
0 12
18
6.8
0 0
9.2
0.5
34.0
0.020
0.12
18
7 3
0 0
8 8
0 2
34.0
0.020
0.12
18
8.6
0.0
7 5
0.2
Ave:
34 1
0.022
0.12
17.6
7.7
0 5
11.0
I.I
Htn:
34.0
0.000
0.10
14.0
6.3
0.0
0.0
0.2
Nan:
35.0
0.030
0.13
18.0
15.9
10.0
8/ 0
1.7
Kiln Scrubbor Scrubbe
Exit
Lxlt
Exit
Exit
Exit
Exl
(1?
CO
C02
NOx
HIHC
U1K
(»)
(PP«)
(X)
(PP«)
(PP»)
(PP»
Scrubber Scrubber Scrubber
52.0
64.0
47 0
47 0
46.D
56 0
55.0
53 0
53.0
51 0
58 0
54 0
53 0
50.0
53 0
58.0
53.0
43.0
66.0
57.0
68 0
6?.0
55.0
43.0
68.0
Stack
01
Stack
CO
Stack
C02
(t) (PP>)
ct::c:::t;:::ss:tf:tE;r:
12.1
11.6
11.8
11.8
12.?
12.2
12.2
12.1
12.1
12.2
12 4
12.3
12.4
12.2
12 3
12.1
12.0
14.»
11.0
11.4
11.6
11.2
197.0
118.0
187.0
201.0
149.0
184.0
190.0
198.0
204.0
196.0
186.0
191.0
182.0
195.0
194.0
212.0
200.0
192.0
187.0
195.0
192.0
181.0
5.1
12.1
191.2
19
II.0
149.0
43.0
14.9
212.0
-------
rest 10
9-20-88
Np
Km
915
950
915
1000
I01S
1030
1045
1100
1115
1130
II1S
1700
I7IS
1230
1245
1300
HIS
1330
13(5
1100
his
1130
14(5
1500
ISIS
1530
ISIS
1600
Ave:
Mfn:
fax:
Clay
Feed
Height He
Reading Read
(lbs) (
391 0
391.0
386 0
3515
316 0
281 0
746.0
711 0
111.0
142 0
101.0
387 S
353 0
318.0
783.0
298. S
711 0
180.0
143 5
1110
367.0
377.5
793 0
758.0
773.5
188.5
153.0
171.5
751 1
108.0
391.0
als
feei
,h
Feed
totals
Rotoaoter
0.0
Mln
Kiln
K1 In
m In
*0
U\\
Gas
Air
tux Air
Exit
Iwp
Flo*
Flon
F loa
lemp
.0..
(scfh)
(scfh)
(scfh)
<°F)
ZTZZZZ
- -
t -
1603
410
14710
0
1186
1605
420
14370
0
1985
1518
290
11190
7615
1984
1518
230
2360
1611
7017
1594
790
8590
7605
1992
IS96
730
8170
1608
2005
1607
750
8830
1630
2000
1588
7 JO
8590
7611
1989
1S9I
230
5890
1588
1992
I60S
750
9040
1585
2006
1616
230
5890
1593
2003
1619
230
8150
7588
70U5
1671
230
8360
1617
2005
IS6S
700
7010
7627
1999
1608
230
8590
7569
7001
1613
230
8360
1568
2003
1614
220
8170
1597
7007
1591
220
1180
7601
1919
1591
220
8120
7574
1996
1591
220
1910
7589
1998
1607
240
8590
7577
1990
1619
730
8360
7567
2001
1630
230
8360
1605
2004
1613
710
1880
(599
1499
1607
710
1100
1515
2000
1591
710
1880
1519
1999
1S99
740
8590
0
7000
IS04
720
8120
0
1998
S98.1
244.6
8393.6
6509 1
1973 6
504.0
200 0
2360 0
0 0
1499 0
630 0
420.0
14310.0
1638.0
7012.0
«e
AB
Make-up
Bloadown
Venturl
Vonturl
Packed
Packed
lias
Air
Hater
Hater
FIom Pressure
Coluan
Colum
:1ow
Ho.
Cu».
Flo* Pressure
:fh)
(sclh)
(0»1)
(9P»>
)
C«)
rrr"*
rrr-.T-Ti;:
570
19060
5871
15
20
25.0
30
II. 5
510
19060
5984
15
20
75.0
30
115
630
19060
6058
0.7
20
25.0
30
11.5
600
19060
6118
0.7
20
25.0
30
11.5
610
19060
6180
0.5
20
25.0
30
II 5
610
19060
6738
0 4
20
2S.0
30
11. S
610
19060
6794
0 4
20
23.0
30
11.5
610
19060
63S6
0 5
70
23 0
30
12. S
670
19060
6418
0.5
70
23.0
30
13.0
630
19060
6478
0.4
70
23.0
30
13.0
630
19060
6536
0.4
20
23.0
30
12.0
670
19060
6603
0.4
70
22 0
30
13.0
670
19060
6667
0.4
20
22.0
30
13.0
610
19060
6121
0.4
20
22.0
30
13.0
670
19060
6187
0.5
20
27.0
30
13 0
670
19060
6841
0.5
20
22.0
30
13.0
670
19060
6903
0.5
20
22.0
30
13.0
670
19060
6967
0.5
20
22.0
30
13.0
670
19060
1031
0.5
20
22.0
30
13.0
670
19060
1080
0.5
20
22.0
30
13.S
670
19060
1146
0.5
20
22.0
30
13.5
670
19060
1701
0 6
20
22.0
29
13.5
670
19060
7765
O.S
20
22.0
29
13.5
670
19060
7377
0.5
20
21.0
29
13 S
670
19060
1308
0.5
20
21.0
29
14. S
620
19060
1451
OS
20
21.0
29
14.5
670
19060
1517
0.4
20
71.0
29
14.S
670
19060
7568
0 4
20
21.0
29
14.5
615.7 19060.0
570 0 19060 0
630.0 19060 0
6747.3 0.6
5871.0 04
1568 0 1.5
70.0 77.6
70.0 71.0
70.0 25.0
29.1 12 9
79 0 II. S
30.0 14.S
-------
Test 10
9-20-99
!U Fan
K1ln
AB
Quench
AB
AU
«0
AU
Inlet Pressure Pressure
Hater
Exit
Exit
Exit
L«it
Flo*
02
CO
CO?
UIIIC
c«)
C«)
<*«)
(qpm)
(\)
(PP«)
(t)
(PP»)
3(0
0.010
0.12
19
0.0
7.7
-0.3
34 0
0.010
0.12
19
16
0 0
7 7
-0 3
](.0
0.020
0 10
19
6 7
0.0
9 4
0 1
34.0
0.020
0.10
l(
7.4
0 0
8 8
0 5
34 0
0 020
0.10
l(
7.3
0.0
9 3
0 2
33 0
0.020
0 10
M
7.2
0.0
9.4
0 5
33.0
0.020
0.10
l(
7.1
0 0
9 0
0.3
33 0
0.020
0.10
14
7 5
0 0
9 9
0 6
33.0
0 020
0.10
M
7.6
0 0
16
13
33 0
0.020
0 10
II
1.3
0.0
9.1
3 1
3? 0
0.020
0.10
14
7.2
0 0
9.9
-1.3
33 0
0 020
0.12
14
7 9
0.0
9.1
1.0
32.0
0.020
0.12
II
7 6
0.0
9.1
10
33.0
0.020
a. to
11
9 2
0.0
9 7
1.0
32.0
0.020
0.10
II
7.4
0.0
9 0
1.6
32.0
0.020
9.10
11
7.5
0 0
9.1
II
32.0
0.020
0.10
11
7.1
0.0
9 9
14
37 0
0.020
0.10
II
7.9
0 0
9.0
1.9
32 0
0.020
0. to
II
7 7
0 0
9 9
1.7
32.0
0.020
0.11
11
7 6
0 0
0.8
3.8
32.0
0.020
0.10
14
7.6
0 0
9 6
3 1
32.0
0.020
0.10
II
7.2
0.0
9.0
(2
32.0
0.020
0.12
14
7 6
0 0
9.7
11
32 0
0.020
0.10
14
7.7
0.0
9 0
3 0
33.0
0 020
0.10
II
7.7
0 0
9.7
2 1
33.0
0.020
0 10
II
7.9
0 0
9.5
2 5
33 0
0 020
0.10
H
7 1
0 0
1.1
13
33.0
0.020
0.10
II
9.9
0 0
6 9
3 2
Ave:
32.9
0.019
0.10
11 4
7.7
0 0
9.8
17
Hin:
32.0
0.010
0 10
14.0
6 7
0.0
6 9
1.3
NdX:
3(0
0.020
0.12
ISO
9.9
0 0
9 4
4.9
Kiln Scrubber Scrubber Scrubber Scrubber Scrubber St
txlt
lxlt
Uit
txlt
Exit
Exit
02 CO
C02 HIHC
O?
CO
C02
NOx
HTHC
UIIIC
(*)
(PP«)
(X)
(|>P«)
(PP»)
(pp«)
t> (PP»)
(*) (pp.. CH4)
rsr:esaeoi>::c:.
sscieatissecets
1? 1
1.0
5 5
49.0
0.2
0.7 1
.9 0.0
(.0 -0.5
12 1
2 0
5 6
19 0
0.1
0 8 1
.0 0.0
5.9 -0.5
13 4
1.0
7 1
57.0
0.2
0.3 1
.9 0.0
7.1 0.2
10.9
1.0
6.5
59 0
0.2
0.6 1
.S 0.0
6.2 0.3
10
1.0
6 4
49 0
0.0
0.7 1
.5 0.0
6 4 0.2
10.9
2 0
6.4
51 0
-0.2
0 6 1
.5 0.0
6.4 -0.2
III
1.0
6 4
52.0
-0.3
0.8 1
.7 0.0
6.2 -0.7
161.0
0.0
6.2
52 0
-0.2
0.6 1
.7 0.0
6.2 0.2
112
1.0
6 3
51 0
-0.3
0.6 1
8 0.0
6 2 -0.2
111
1.0
6 3
56 0
-0.3
0 6 1
.5 0.0
6.4 -0.7
11.0
0 0
6.3
61.0
-0 2
2 3 1
.8 0.0
5.9 -0.2
112
1.0
6.4
51.0
-0.2
0.8 1
.7 0.0
6.4 -0.6
11.3
2 0
6.5
51.0
-o.s
0.7 1
.6 0.0
6.5 -0.6
12 5
0.0
6 1
55.0
-0.4
0.7 1
.1 0.0
6.1 -0.4
114
1.0
6 4
59.0
-0.3
0 6 1
6 0.0
6 3 -0.7
11.5
0 0
6.5
55.0
-0.3
0.6 1
.7 0.0
6 2 -0.4
11.7
0 0
6 4
54.0
-0.3
0 6 1
.8 0.0
6.2 -0 4
117
1.0
6.2
56.0
-0 5
2.8 1
.6 0.0
6.1 -0.4
11/
2 0
6.3
53 0
-0.6
12 1
.7 0.0
6.3 -0.7
118
1.0
6.1
61.0
-0.6
It 1
7 0.0
6 4 -1.4
11.7
10
6 4
54 0
-0.5
0 6 1
.6 0.0
6.3 -0.2
11 3
1.0
6 3
54.0
-0.6
0.9 1
.6 0.0
6.4 -0.2
III
0 0
6 3
55 0
-0.7
0.6 1
.6 0.0
1.3 -0.4
117
3.0
M
51 0
-0.7
0.9 1
.6 0 0
6.4 -O.S
116
1.0
5.2
13.0
0.6
0.7 1
.8 0.0
6 2 -0.2
11.6
2 0
6.1
53 0
-0.7
0.6 1
.4 0.0
6.1 -0.5
III
1.0
6 5
45 0
-0.9
0 6 1
1 0 0
6.5 -0.6
114
1.0
1.9
55.0
-0.1
0.9 1
.0 0.0
5.3 -0.4
16 9
1.0
6.2
53 3
0.4
0.9 1
.6 0.0
6 3 -0.4
10.7
0 0
1.9
43 0
-0.9
0.3 I
.9 0 0
5.3 -14
161 0
3 0
7.1
61.0
0.2
2.9 1
.0 0.0
7.1 0.3
ck Suck Stac
-------
lest II
4-I2-8B
Clay
(totals
Feed
Feed
Feed
Kiln
Kiln
Kiln
K1ln
AO
Km
Height
Height
Netals
txlt
Gas
Air
Aux Air
Cxit
Reading
Reading Rotoaeter
lenp
F1o«
Flo*
Flo*
!o»p
(lbs)
(lbs)
(°F)
(scfh)
(scfh)
(scfh)
<°F)
901
364 5
23.3
0
1501
1120
14400
0
1996
915
357.0
73 2
II
1576
290
10490
7601
7003
J30
370 5
22 0
11
IS09
290
10250
7593
1994
915
204 .S
22 5
II
1507
270
9)40
7594
1939
1000
240 5
22.1
11
1509
270
9540
7559
1906
1015
213.5
21.7
II
1509
270
9740
7562
2006
1030
110.0
21.3
II
I60S
270
9540
7563
2000
1045
142.5
20.9
11
1600
260
9300
1562
1999
1100
107.0
20.4
11
1591
260
9540
7542
2001
IMS
72.0
20.0
II
1505
260
9540
7549
1999
1130
37! 0
19.0
II
1504
260
9540
7530
1999
IMS
240.5
19 3
II
1506
260
7340
7543
1997
1700
306.0
10.9
11
1507
760
9540
7526
1997
1215
271.0
10.4
11
1509
260
9100
7549
1993
1130
336.0
18.0
11
1509
250
9300
7541
1996
1215
201.0
17.4
II
IS36
260
9300
1527
1995
1300
165.5
16.9
tl
1507
210
9540
1551
1994
I3IS
131.5
16 5
11
1602
260
9540
7595
1996
1330
97.0
16.1
II
1607
270
9750
7565
1996
1345
62 0
15.7
II
1612
270
9740
7579
1999
1400
304.0
15.3
II
1507
260
9540
13455
2000
1415
345 0
14.9
11
1491
270
9510
U335
1997
1430
341.0
14.6
11
1392
270
9750
13461
1979
1445
279.5
14.1
II
1366
100
4310
13393
1005
1500
246.5
13.4
11
1249
150
3140
3240
1507
1515
200.5
12 9
II
1226
100
4050
3230
1451
1530
169.5
12.3
II
1292
190
3940
3230
1416
IS4S
147.0
12.0
0
1626
400
10250
0
1657
Ave:
232.0
II 0
10.2
1537.5
291 4
0927.5
7394 0
1919.2
Kin:
62.0
12 0
0.0
1226.0
150.0
1740 0
0.0
1416 0
Hsu:
304.0
23.3
11.0 1626.0
1120.0
14400.0
13461.0 2006 0
A8
AS
Wake-up 8loudDim
Vpnturl
Venturl
Packed
Packed liquor
Liquor
(idS
Air
Natnr
Hater
Flo* Pressure
Coluan
Coluan pH
leap
Flo*
Flow
Cue.
Flo*
Pressure
cfh)
(scfh)
(da')
(0P»)
(gp«)
('«)
(op*)
C»c)
(°F)
570
16450
3191
0.7
20
25.0
30
13.5 7.04
165
670
19060
3713
0.7
20
73.0
30
13.0 7.36
167
610
19060
0371
0.9
20
23.0
30
13 S 6.45
168
610
19060
3347
0.6
20
23.0
30
14 0 7.75
163
670
19060
3405
0 6
20
23.0
30
15.0 101
167
670
19060
3017
0.6
20
23.0
30
15.0 6.72
168
670
19060
0529
0.6
20
23.0
30
15.0 7.38
1(8
620
19060
0595
0.7
20
22.0
30
> 15.0 8 40
168
670
19060
3651
0.7
20
27 0
29
> 15 0 7.47
160
620
19060
0113
0.1
19
21.0
29
> 15.0 7.49
168
620
19060
0116
0 7
19
21.0
29
> 15.0 7.46
167
670
19060
8342
0.7
19
21.0
29
> 15.0 T.I2
163
670
19060
0904
0.7
19
21 0
29
> 15.0 7.07
168
670
19060
3964
0.7
19
21.0
29
> 15.0 0.37
168
670
19060
9026
0.7
19
70.0
29
> 15.0 7.07
168
670
19060
9001
0 7
19
20.0
29
> 15.0 5.84
168
620
19060
9161
0.1
19
20.0
29
> 15.0 4.99
167
670
19060
9715
0.7
19
20.0
29
> 15.0 8.18
168
620
19060
9212
0.7
19
20.0
29
> 15 0 S. 13
168
670
19060
93J9
0 7
19
20.0
29
> 15.0 8.35
168
670
19060
9396
0.7
19
20.0
29
> 15.0 7.52
168
670
19060
9972
0.7
19
20.0
29
> 15.0 7.79
170
630
19060
9530
0.6
19
20.0
29
> 15 0 7.94
171
90
5640
9601
0.6
19
20.0
29
> 15.0 8 49
161
00
5740
9648
0.4
19
16.0
29
65 S. 19
158
00
6520
9613
0.4
19
16.0
29
6.5 7.68
157
00
6350
9708
0.4
19
16.0
29
6 5 7.20
156
630
19060
9191
0.4
19
16.0
29
6.0 8.19
167
39 6
17199.3
8996.1
0.6
19.3
20.6
29.3
13.6 7 50
166.5
00.0
5640 0
8077 0
0.4
19.0
16.0
29.0
6.0 4.99
156.0
30.0
19060.0
9972.0
0.8
20.0
75.0
30.0
15.0 0.49
171.0
-------
fest II
S-27-00
ID Fan
m\n
AB
Quench
AB
AR
AR
AB
Inlet
Pressure Pressure
Hater
Exit
txit
txit
Lxit
Flo*
0?
CI)
CO?
U1HC
C«)
C"c)
C«)
(qp»)
(t)
(PP")
m
(PP»)
16 0
a o?o
0 10
11
8 7
0 0
7 b
12
33.0
0 020
0.12
10
6.6
10
9 3
1 2
34.0
0.020
0.12
18
7 6
10
A 9
0 6
34.0
0.020
0.12
18
7.7
0 0
9 6
-0 3
31 0
0.020
0.1?
10
7 5
0 0
8 9
-0.6
34.0
0 020
0.12
10
7.4
0.0
8 9
-0 7
34.0
0.020
0.12
10
7.2
0 0
9 1
-0 8
34 0
0.020
0.12
18
7.2
0 0
9 2
-0 9
34.0
0.020
0.12
10
7.6
0.0
8 8
0.1
34 0
0.020
0.12
18
7 7
0 0
8 8
0 5
34.0
0.020
0.12
18
7.7
0 0
8 8
0 6
34 0
0.020
0 12
18
7 8
0 0
8 7
-2 6
34.0
0 020
0.12
18
7.6
0 0
19
•3.0
34 0
0 020
0.12
18
7.8
0 0
8 6
-0.8
34.0
0.020
0.12
18
7.6
0.0
8 6
1.6
34.0
0.030
0 12
18
7 8
0 0
8 6
11
34.0
0.0?5
0.12
18
7.7
0 0
9 1
11
34.0
0.020
0.12
18
7 5
0 0
8 7
-0.3
34.0
0.020
0.12
18
7.7
0.0
8 5
0.2
34.0
S 020
0.12
18
7 5
0 0
8 8
0 4
34.0
0.020
0 12
18
8.0
0 0
8.5
-0.6
36.0
0.010
0.12
18
7.3
0.0
0 8
•0.1
36.0
0 000
0 10
18
7.1
0 0
9 2
-6.0
37 0
0.100
0.31
IB
14.4
33 0
3 0
-4 5
21.0
0.100
0 22
18
15 0
70 0
3 7
-0 7
21.0
0.100
0.22
18
14.6
49 0
4 3
1.1
710
0.100
0 22
18
14.0
91.0
4.6
-65.0
20.0
0 060
0.12
18
5 2
0 0
9 8
-63 0
32.4
0.035
0 14
18.0
0.5
7 5
8 1
-5.0
20.0
0.000
0 10
18 0
5 2
0 0
3 0
-65.0
37.0
0.180
0.30
18.0
15.0
96 0
9.8
16
Kiln
Scrubber
Scrubber
Scrubber
Scrubber
Scrubber
Stack
Stack
Stac
Stack
I* it
txit
lxit
txit
fxlt
Exit
02
CO
CO
HTHC
U?
f.O
CO?
NO*
H1HC
U1HC
(*)
(PP")
(\)
(PP»)
(PP">
(PP«)
m
(fH»)
IX
(ppa. CHI)
12.0
10
5 3
37.0
1.0
1.9
12.4
54.0
6.
-0.5
12 1
n
6 6
51 0
0.9
1.6
11.1
44.0
8.
0.0
10 9
2.0
6.0
40.0
I.I
1.7
11.7
42.0
7.
-0.4
10 9
10
5 9
43 0
0.9
1.1
11.8
31.0
7.
-0.2
11.7
3.0
5 9
46.0
0.6
1.0
11.9
47.0
7.
-0.6
113
3 0
6 2
45 0
0.8
0.9
11.8
39.0
7.
-0.2
10.9
4.0
6.0
46.0
0.8
I.I
118
55 0
74.
-0.8
111
3 0
5.1
44.0
0.7
1.0
12 1
37.0
7.
-0.4
114
3.0
5 9
46 0
0 9
0.9
11 9
32.0
7.
-0.2
114
4 0
5 7
45.0
0.7
0.6
12.0
16 0
7.
0.1
115
3 0
5.8
45.0
0.6
0.8
119
17.0
7.
-0.5
114
3 0
5.7
47.0
0.3
0.6
11.9
28.0
7.
-0.2
115
3 0
6.0
50 0
0.3
0.7
11.9
12.0
7.
-0.9
113
10
6.0
51 0
0.1
0.6
11.9
20.0
7.
-0.5
116
4.0
5.9
48.0
0.3
0.7
12.0
21.0
7.
-0.6
115
4.0
6.0
51 0
0.2
0.?
12.0
12.0
7.
0.0
11.5
3.0
6.1
49.0
0.2
0.2
11.8
18.0
7.
0.0
11.4
4.0
5 8
49 0
-0.2
0.3
11.9
33.0
7.
-0.1
11.3
3.0
6.0
46.0
-0.1
0.2
12.0
40.0
7.
-0.2
11.4
2 0
6 0
47.0
0.4
0 3
11.9
S4.0
1.
-0.4
11.5
3.0
5.8
48.0
0.4
0.6
12.0
41.0
7.
0.1
17.0
2.0
5 8
47.0
0.1
0 1
12.1
28.0
7.
-0.7
117
2 0
6 2
42.0
-0 2
0.?
11.7
20.0
7.
-0.6
14 0
11.0
2.1
17.0
0.4
1.4
16.7
33.0
3
-1.1
15 6
70 0
2.4
2? 0
0 8
1.5
17.0
45.0
3.
-0.5
14 5
33 0
3.0
24.0
0.7
1.3
16.5
70.0
3
-0.8
14.1
70 0
3.3
23 0
3.1
14
16.2
97.0
4
0.2
10 4
2 0
6.8
49.0
0.2
-0.1
10.0
278.0
7.
-3 1
118
7,1
5.5
47.6
0.6
0.8
12.5
45.1
9.
-0.5
10.4
1.0
2.1
17.0
-0.2
-0.1
10.0
12.0
3.
-3.1
15 6
70.0
6.8
5)0
3.1
1.9
17.0
278.0
74.
0.2
-------
lest )
9-26-18
Clay Notals
Feed
Feed
Feed
Klin
Kiln
Kiln
Kiln
AB
Km
Height
Nclqht
Metals
Exit
Gag
Air
Au* Air
t«n
Reading
Reading
Rotoaeter
7e*p
Flew
Flow
Flo.
leap
(lb*)
(lbs)
( f)
(scfh)
(scfh)
(scfh)
(°F)
0<5
375 5
10 4
0
1618
420
14950
0
1904
900
3*8.5
10.0
II
IS4I
280
5990
7692
2008
915
314.0
9.7
11
1583
280
6230
7679
1977
930
310.0
9 2
11
IS86
360
12490
7664
2011
91b
2TS.0
9 3
1581
440
15810
7656
1942
1000
218.0
9 3
955
110
7620
0
1609
1015
261.0
9.0
II
1604
350
12480
0
1970
1010
227 0
1.5
11
1596
310
10080
7639
2003
1045
193 0
S.I
II
1592
290
10520
9645
2003
1100
159.0
7.0
II
1597
380
10310
7617
1999
HIS
125.0
f.5
II
1603
280
10090
7599
2001
1130
91.0
6.1
II
1592
260
96J0
7(08
2004
ins
267.5
5.7
11
IS84
310
10720
7618
2004
1200
334.0
5.2
11
1580
280
10100
7594
2004
1215
300.0
4 1
11
1607
290
10350
7591
2007
1230
266.5
4.4
II
1605
270
9730
7678
2004
1245
232.5
3.1
11
1592
270
9700
7601
2008
1300
19).5
3.4
II
1587
270
9720
7588
2009
1315
1(4 5
3.0
11
1591
270
9700
7577
2004
1330
131.0
2.S
II
1595
270
9680
762 J
2000
1345
96.5
2.4
0
1603
260
9630
7600
2021
Ave:
234.3
6 6
1.9
1561.9
296.2
I0026J
6629 5
1979.6
Bin:
91.0
2.4
0 0
955.0
180.0
2620.0
0.0
1609.0
Max:
375.5
10 4
11.0
1618.0
440.0
IS8I0.0
9645.0
2021.0
AB
Att
Make-up
Blowdoan
Venturl
Venturl
Packed
Packed
Liquor
Liquor
Gat
Air
Hater
Hater
Flo* Pressure
Cotuan
Coluan
PH
leip
(Ion
F lo«
Cull
Flow
Pressure
scfh)
(scth)
(gal)
(qp»)
(?P»)
(¦«c)
(8P>)
(•«)
(°F>
ri::;::'::
560
19060
6032
0.7
19
25 0
21
12.0
7.14
165
670
19060
6104
0.7
19
25.0
28
12.5
6.86
166
630
19060
6157
0.4
15
20.0
21
>
IS
8.06
168
630
18130
6221
0.7
12
18.0
18
>
15
9.60
151
630
17960
6282
0.8
15
20.0
21
>
75
6.93
165
300
8140
6361
1.6
23
23.0
3S
>
15
7.61
144
630
18040
6(09
1.4
20
22.0
29
14.0
8.63
167
630
18100
6(81
14
20
22.0
29
14.5
8.42
168
620
17530
6551
1.4
20
22.0
29
>
15
5.95
167
610
17420
6617
0.8
20
22.0
29
14.5
6.64
167
610
17540
6680
0.7
20
22.0
29
14.5
6.47
167
610
17550
6741
0.6
20
22.0
29
14.0
7.24
167
620
17580
6807
0.6
20
22.0
29
14.5
7.85
168
610
175(0
6867
0.5
20
22.0
29
14.5
8 07
168
610
17470
6926
0.5
20
22.0
29
14.5
8.14
168
610
17510
6913
0.5
20
23.0
29
14.5
1.95
168
610
17490
7048
0.5
20
22.0
29
14.5
7.(9
168
610
17(40
7104
0.4
20
22 0
29
14 5
8.08
109
600
17720
7170
0.4
20
22.0
29
14.5
• 26
168
600
17700
1230
0 4
20
22.0
29
15 0
1.89
168
590
17410
7208
0.4
20
22.0
21
15.0
7.32
167
59/1
17407 1
6383 8
0.7
19.2
22.0
27.9
0.0
14.4
7.SI
1(2.6
300 0
8140.0
1230 0
0.4
12.0
18.0
18 0
0.0
12.0
5.95
109.0
630.0
19060 0
7288.0
16
23.0
25.0
35.0
0.0
ISO
9.60
168.0
-------
Test 3
9-26-08
ID Fan
K1 In
AB
Quench
*0
Inlet Pressure Pressure
Hater
Exit
Exit
Exit
Exit
Flo*
02
CO
C07
U1HC
C» c)
C»c)
C« c)
(qp«)
(t)
(PP«)
(*)
(Piw)
35 0
0.070
0.12
10
8 7
0.0
7 6
0.5
35.0
0.020
0.10
to
1.7
0.0
9 7
0 2
34.0
0.070
0.10
18
7.5
0 0
9.3
0 (
35 0
0.100
0.10
18
17.0
7.0
0.5
3 2
37.0
0.070
0 Oi
18
8.1
0.0
8 1
0 8
37.0
0.075
0.17
18
19 5
34.0
2 7
5 2
31.0
0.070
0 10
II
7 0
0 0
9.8
0 6
31.0
0.010
0.12
18
(8
0.0
9 1
0 5
3(0
0.070
0 17
18
7.2
0.0
9 5
0.8
34 0
0.070
0.12
18
7.3
0 0
8.9
0.6
34 0
0.070
0.12
14
7 3
0.0
9 4
0 8
31.0
0.070
0.12
18
7 5
0.0
9.3
0 9
31.0
0.010
0 17
18
7 J
0.0
9 3
0 9
3(0
0.010
0.12
11
7 5
0 0
9 7
0 8
3(0
0.070
0.12
18
7.1
0.0
9 2
0 6
34 0
0.020
0.12
18
7 3
0.0
8.9
0.3
3(0
0.070
0.12
18
7.4
0 0
9 0
0.7
3(0
0.020
0.12
IB
7.4
0.0
9.1
0.9
3(0
0.070
0.12
18
7.6
0.0
8 9
15
3(0
0.020
0.12
18
7.6
0 0
9.0
7.7
3(.0
0.020
0.12
18
7.9
0.0
8.1
3 3
Ave:
3(4
0.026
0.11
17.8
8.5
7.0
8.3
12
Kin:
34.0
0.010
0.06
14 0
6.8
0.0
0 5
0.7
Hax:
37.0
0.180
0.12
18.0
19.5
3(0
9.8
5.2
Klin Scrubber Scrubber Scrubber Scrubber Scrubber
Stack
Stack
Stack
Stack
Exit
Exit
Exit
Exit
Exit
Exit
02
CO
C02
HIHC
07
CO
C07
NOx
HIHC
U1HC
(t)
(PP")
(t)
(PP»)
(PP»)
(PP«)
(*)
-------
Test ?
9-28-88
Clay
Metals
Fred
Feed
Feed
K1ln
Kiln
Ki In
Klin
AB
Kac
Height
Height
Metals
Exit
Gas
Air
Aux Air
Unit
Reading
Reading
Bolometer
leap
Flo.
Floo
Flo«
leap
(lbs)
(lbs)
( F)
(scfh)
(scfh)
(scfh)
<°F)
eu
396.0
11.7
0
1591
400
14030
0
2005
900
372.5
113
II
1618
300
10520
7/54
2018
915
337.5
10.9
11
1588
220
7810
7749
2000
9)0
302.5
10.4
II
1579
220
8060
7744
2009
945
267 5
10.0
11
1602
240
0190
1724
2019
1000
232 5
8 9
11
1583
230
8200
7720
2005
1015
198.5
8.4
II
1584
230
8440
7699
2001
10J0
164 5
8.0
II
1603
2 JO
8260
7657
2000
1015
129 0
7 5
II
1600
230
8230
7fi 79
2000
MOO
96.5
7.0
II
1607
230
1420
1610
2000
1115
354.0
6.6
11
1601
230
79C0
1(39
1949
1130
319 5
6.1
II
1618
220
7810
7621
2001
IKS
285.0
5 7
II
1617
230
TRIO
7612
2006
1700
251 0
5.2
II
1603
210
7330
762b
2004
I?I5
218 0
4 8
11
1579
210
1390
1519
2001
1230
185.0
4 3
0
1511
220
7670
0
1993
Avg:
256.1
7.9
9.6
1592.8
240 6
8546.9
6713 3
2000 7
Kin:
96 5
4.3
0.0
1511.0
210.0
7330 0
0.0
1949.0
Rax:
396.0
11.7
11 0
1610.0
400.0
14030.0
1154 0
2019.0
AB
AB
Moke up
8)ovdo«n
Venturl
Venturl
Packed
Gas
Air
Mater
Hater
Floo
Pressure
Coluan
1 lo*
F low
Cua.
Flo*
scfh)
(scfh)
(gal)
(flP»)
(bp«)
(•«)
(0P«)
560
19060
4B6S
0.6
21
25.0
29
540
16020
4934
0 5
20
27 0
29
620
18240
4991
0 5
20
25.0
29
610
18250
5050
0.5
20
25.0
29
610
18000
5111
0 5
20
25.0
29
600
18490
5168
0.5
20
25.0
28
650
18440
5230
0.5
20
25.0
28
600
10490
5295
0 5
20
24.0
28.5
600
18440
5369
0.5
20
24.0
29
590
18370
5409
0 5
20
24 0
29
600
18450
5471
0.5
20
24.0
28
600
18460
5528
0.5
20
24.0
28
590
18450
5596
0.5
20
24.0
28
600
18440
5651
0.5
20
24.0
28
590
18310
5115
0.5
20
24.0
28
590
18370
5700
0.7
20
24.0
28
596 9
18272.5
5322 7
0.5
20.1
24.6
28.5
540.0
16020.0
4865.0
0.5
20.0
24.0
28.0
650 0
19060.0
5780.0
0.7
21.0
27.0
29.0
Packed
Column
'ressure
('«
Liquor
P«
L1quo
loo
(°F
166
166.
167.
-------
lest 7
9-28-19
IU Fan
Kiln
AB
Quench
AB
AS
All
AH
Inlet
Pressure Pressure
Nater
Exit
Exit
LxU
Exit
Floa
07
CO
CO?
UIHC
C«)
C»c)
C«)
(qp«)
<\)
(PP")
(t)
(f!|»)
55 0
0 070
0.17
18
11
0 0
7 1
0 3
35.0
0.070
0.16
18
1.7
on
8 0
0.0
35 0
0.070
0.17
18
6.7
7 0
10 1
0 7
35.0
0 0 JO
0.12
18
17
on
9 6
0 7
35.0
0.070
0.17
18
6.8
0.0
9 3
0 4
35.0
0.070
0.12
18
1.5
0 0
9 5
-0 7
35.0
0.070
0.17
18
7 4
0.0
9 7
¦0.5
31.0
0.030
0.17
14
1.4
so
9.1
-0.1
34.0
0.070
0.12
18
1.4
0 0
8 8
0.3
31.0
0.070
0.12
18
11
DO
8.8
-0 3
34.0
0.070
T). 17
18
7.5
0 0
9 3
-0.6
31.0
0.070
0.12
18
7 5
0.0
9.0
-0 6
31 0
0.070
0.12
18
7.4
0 0
9 0
0.3
31.0
0.070
0.12
18
7.4
0.0
8.8
-0 7
3(0
0.070
0.12
18
7.6
0.0
8 7
0 3
34.0
0.050
0.15
14
10.3
0.0
6 4
-0 7
Avq:
34 4
0.073
0.12
17.5
7.6
0.1
8 8
0 3
Kin:
34.0
0.070
0.12
14.0
6.7
0 0
6 4
-0.6
Nax:
35.0
0.050
0.16
18.0
10.3
2.0
10.
0 3
Kiln Scrubber Scrubber Scrubber Scrubber Scrubbe
Exit
Exit
Exit
Exit
Exit
Exit
U2
CO
C02 HIHC
O?
CO
C07
NOx
K1HC
UIHC
m
(PP«)
(»)
(PP«)
(PP")
(PP«)
(PP«)
(t) (pp.. CH4)
I? 1
1 0
5 4
35 0
0.1
1.3
17 7
2.0
6.9 0.6
10 2
7.0
1.7
22.0
0.5
1.0
11 4
0.0
8 0 -0.8
11 J
1.0
6 0
33 0
0.1
II
11.6
0.0
7.7 -1.8
113
10
6.1
36 0
0.7
1.6
11.7
0.0
7.7 -1.7
11.7
1.0
6 1
34.0
0.0
1.7
11.7
0.0
7 8 -0.9
114
2.0
5 9
35.0
0.2
1.0
11.9
0.0
7.5 -0.4
11.3
0 0
6 2
33.0
0 3
1.3
119
0.0
7.9 -0 1
11.5
1.0
6 2
36.0
0.3
I.I
12 1
0.0
7.8 -13
113
7 0
6.0
35.0
0.0
1.0
12 1
0.0
7 7 -12
11 4
7.0
6 0
34 0
0.7
7 1
12.1
0 0
7.5 -2.1
115
1.0
6.0
34 0
0.0
1.4
12.0
0.0
8.1 -0.9
11.1
2.0
6 0
35.0
0 7
1.3
12.0
0.0
7.7 -1.1
11.0
1.0
5 8
37 0
0.3
14
12 0
0.0
7.0 -1.0
116
0.0
5 9
31.0
0.3
13
12.2
0.0
7.3 -1.4
11/
2.0
5 8
38.0
0.7
1.0
12 3
0.0
7.3 -1.2
115
2 0
4.3
48 0
-0.1
1.0
13.0
0.0
56 -IB
114
13
5 6
35.1
0.2
1.3
12.0
0.1
7.5 -I.I
10.7
0.0
17
77.0
-0.1
1.0
11.4
0.0
5.6 -2.1
12.7
2.Q
6.2
48.0
0.5
2.1
13.0
2.0
8.1 0.6
Stack Stack
-------
lest I
9-29-88
Clay HetaU
Feed
Feed
Feed
Klin
Kiln
Kiln
Kiln
AB
Hie
Helqht
Helqht
Hotals
Cult
Gas
Air
Auk A1r
Exit
Reading
Reading Rotoaeter
leap
Flo*
Flo*
Flo*
lemp
(lbs)
(Ihs)
(°F)
(scfh)
(scfh)
(scfh)
(°f)
646
363.5
3.8
0
1597
410
14270
0
2005
900
344 5
3.1
II
1580
230
8120
7672
2004
9IS
311.5
2 6
11
1592
230
8120
7664
2008
9)0
278.5
1.7
II
1593
220
7880
7704
2011
945
24S.S
10
11
1593
230
7950
7697
2004
1000
211.5
2.8
II
IS92
230
8120
7678
2001
tots
177.0
2.2
11
1592
230
8100
7672
2001
1030
142.5
IB
II
1594
220
7840
76D6
1999
1045
108.5
13
11
1603
210
7650
7687
2002
not
292.0
0.8
11
1586
210
7650
7663
1991
MIS
257.5
0.4
II
1600
210
7650
7638
2001
1130
222 0
•0.1
11
1622
220
1650
7621
2002
IKS
117.5
-0.5
11
1601
210
7650
7596
2001
1200
152.0
-1.0
11
1623
210
1110
1S71
2002
1? IS
116.0
0.0
0
1324
220
7840
7559
1618
«vg:
227.3
1.3
9 5
1579.5
232 7
8760.0
7140 9
1976.7
Win:
108.5
-1.0
0.0 1324.0
210.0
7110 0
0.0
1618.0
Rax:
363.5
3.8
11.0
1623.0
410.0
14270.0
7704 0
2011.0
AO
AB
Make-up
BloNdovn
Venturl
Venturl
I>js
Air
Hater
Hater
Flow Pressure
Flo*
Flow
Cua.
(sclh)
(scfh)
(fl»l)
(giw)
(bp«)
C»c)
600
19060
1500
0 6
20
25.0
610
19060
1555
0.2
20
24.0
630
19060
1619
0.7
20
24.0
620
19060
1682
0.5
20
24.0
610
19060
1742
0 2
20
24.0
610
19060
1811
0 8
20
24 0
600
19060
1868
0.8
20
24.0
610
19060
1935
0.5
20
24.0
600
19060
1996
0.6
20
24.0
610
19060
2056
0.6
20
24 0
600
19060
3118
0.5
20
24.0
600
19060
2184
0 4
20
24 0
600
19060
2244
0.4
20
24.0
600
19060
2306
0.2
20
24.0
0
190
2359
0.5
20
25.0
568.0
17802.0
1998.3
0.5
20.0
24.1
0.0
190 0
1500.0
0 2
20.0
21.0
630 0
19060.0
3118.0
0 8
20.0
25 0
Packed
Packed
liquor
Liquor
Coluan
Coluan
pH
leap
Flo* Pressure
(0P»)
(•«)
(°F)
sese;:;
-------
-T-----
28
13.0
7 08
160
28
13.0
6.83
169
28
12.5
7.03
161
28
13.0
6 48
167
28
12.5
7.10
166
28
13.0
703
166
21
13.0
7.00
166
28
13.0
7.08
166
21
13.0
7.07
166
28
13.0
7 02
167
28
13.0
6.98
166
28
13.0
7.00
167
28
13.0
7.00
167
28
13.0
7.03
167
28
l(.0
7.11
155
28.0
13.0
6.99
166.0
28.0
12.5
6.48
155.0
28.0
14.0
7.11
169.0
-------
Test 1
9-29-88
ID Fan
K1ln
«B
Quench
*B
«8
AB
AB
K1 In Scrubber Scrubbe
Scrubber Scrubber Scrubber
Stack
Stack Stac
Stack
Inlet
Pressure Pressure
Hater
Exit
Exit
Exit
Lx 1
Exit
Exit
Exl
Exit
Exit
Exit
02
CO CO
HIHC
Ho*
02
CU
CO?
U1HC
0?
CO
CU
NOx
HIHC
U1HC
(V)
(•«)
C«c)
(gp*)
(t)
(pc»)
(PP»)
(*>
(pp»)
(1
(PP«)
(PP«)
(PP»)
<*)
(PP«) (*
(PP«. CH4)
35 0
0.010
0.12
18
8.3
0.0
7 9
-0 1
12 0
1.0
5
41.0
1.0
1.6
13.2
KCCZS'VtCft-SSC
35.0 6.
0.7
Il.l
0.010
0.12
18
6.9
0 0
11
-0 4
10.6
1.0
6
38.0
3.4
1.0
11.9
0.0 8.
2.6
310
0.010
0.12
18
6 9
0.0
9 3
¦0.2
10.9
2 0
6.
38 0
O.i
0.9
II t
0.0 8
1.6
34.0
0.010
0.12
18
7.1
0.0
9 1
-0.4
10.8
1.0
6.
31.0
0.2
0.8
11.8
20.0 8.
-0 7
34.0
0.010
0.12
18
7.3
0.0
9.0
-0.2
Il.l
10
6.
36.0
0 2
0.9
12.0
32.0 7
-0.1
24.0
0.020
0.12
IB
7.6
0.0
9 3
0.0
11.2
2.0
6.
35.0
0.2
0.9
12.0
22.0 5.
0.9
34 0
0.020
0.12
18
7 5
0 0
9.J
-0 2
III
1.0
6.
36.0
0.2
0.8
12 1
9 0 7
-0.7
34.0
0.020
0.12
18
7.8
0.0
9.1
0.1
11.4
1.0
6.
36.0
0 2
0.8
12.9
4.0 7.
0.1
34 0
0.070
0.12
18
7.5
0.0
9.0
-0 1
11.3
1.0
6.
36 0
0.2
0.8
12 1
0.0 7.
0.7
34 0
0.020
0.12
18
7.2
0.0
8.3
-0 9
114
1.0
5
36.0
0.2
0.9
12.2
0.0 7.
0 4
34 0
0.020
0.12
18
7.7
0.0
9.2
0.5
112
10
5.
40 0
0.0
0.9
12.0
12.0 7.
-16
34 0
0.020
0.12
18
7.2
0.0
9.0
-II
11.0
0.0
6.
35.0
0 0
0.8
11.8
1.0 8.
0.6
34.0
0 020
0.12
18
7 4
0.0
9 1
-1.3
III
0.0
39.0
0.1
0.6
12.1
6.0 7.
0.2
34.0
0.020
0.12
18
7.4
0 0
9.1
-1.4
111
0.0
6.
38.0
0.0
0.9
11.8
0.0 8.
0.2
36.0
0.120
0.31
18
10.1
0.0
5 1
1.1
15.4
9.0
2.
110
0 5
1.0
17.0
0.0 4.
0.7
33.5
0.023
0.14
18.0
7.6
0 0
8.8
-0.5
11.4
1.5
5
35.5
0.5
1.0
12.4
9.4 7.
0.4
24 0
0.010
0.12
18.0
6 9
0.0
5.1
1.4
10.6
0.0
110
0.0
0.6
11.6
0.0 4.
-1.6
36.0
0.120
0.31
18.0
10.1
0 0
9 4
0.1
15.4
9.0
6
41.0
3.4
1.8
17.0
35.0 8
2.6
-------
IOQO'
2 u
H iJO
ro
iS-
600
20"
0
500'
«£ 8
o
16'
8.5
y
S+arf-
—x~
9.5
~l 1
10.5
Timo of Doy (hr)
—I—
11.5
-r
rv s*-
12.
Figure A-l. Kiln operation for Test 1 (9/29/88)
-------
s I
rropane
Flow
(»ca/hr)
Air
Flow
(icm/hr)
Exit
°2
(X)
CO,
(X)
Exit
CO
(pps)
Exit
Temperature
<°C)
o
P 4
o ©
2 °
e o
o
©
ST rv
to
In
o
In
f-
4
fo
Ln
-------
1000 -
*>
u
3
¦" ? «J
M
U »_
600
20'
•h
MO*
U3 N
500"
—1
u
u 3 J3
-ti Q ^2
«£ 8
« ^
§ > 43
_« d
gC 8
o
16"
7?**-
S+ir-t
~r~
10
_T>
12
Time of Day (hr)
Figure A-.l Kiln operation for Test 2 (9/28/88)
£r,J
-------
^ 1°
4r-r Time of Day (hr)
Figure A-4. Afterburner operation for Test 2 (9/28/88)
-------
rv)
oo
1000
;u
M i"0
a
V
600
10'
0
500'
u * c
fpii Time of Day (fir)
12
¦A
I*"
,/a.
\
V
V-s^>—/
f\.
•A
» 111,1
'
i——^ •
(" /dtv C
n
^
—i— V
K-^-w , ,
' s i i i
Tir 14
r»J
Figure A-5. Kiln operation for Test 3 (9/26/88)
-------
a
«i
i-t
1300
900
500
P, §•
«^i
<->
nj ^
O M
ft
20
0
20
0
600
0
20
> **
a
~\r\
r
i .
r
n—
n
r
r
L
k .
(
1
*
a*'
CO*
\
Tri.1-
£-h>r ~t
10
S^cffyJ
12
Time of Ooy (hr)
Figure A-6. Afterburner operation for Tesl 3 (9/26/88)
T+s*- 14
£rj
-------
0£
Propane
How
(sra/hr)
Air
riow
(scn/hr)
Exit
Temperature
(°C)
-------
-
-
a
r^Uy ^ <¦
j/> ~t*rs r
cjh*4—
10 s-topftj 12
Time of Day (hr)
14
£>rJ>
16
Figure A-8. Afterburner operalion for Test 4 (9/14/88)
-------
zz
Propane
flow
(aca/hr)
Air
Flow
(scm/hr)
Exit
' o2
(Z)
Exit
Tcaperacure
(°C)
9- O
-I
O
o o
o
o
-------
10 12 U 18
Crt<*' t~ Time of Doy (hr) f'-J?
Figure A-10. Afterburner operation for Test 5 (8/25/88)
-------
Propane
Flow
(•ca/hr)
Air
Flow
(sca/hr)
Exic
02
(X)
Exit
Temperature
(°C)
« o
£ \\
sir r
" *
¦V
o
o
*<
$ 5\
^ *
i1
*
> °
X
a
*~
-------
1300
r
~1
12
/"'— y" ^ -t-
t -r (*-••< en~J
w1
1° -T?„t-
SiirJ-
14
Tlrno of Doy (hr)
Figure A-12. Afterburner operation for Tesl 6 (9/16/88)
"jrhffie,
J
1Ss-f- 18
f'J
-------
1000
0
500"
J 1 )
.«ja >yj//
p' ssbtL- A^f
O
16-
*»VOI |
I
14
10
~T~e
-------
LZ
Propane Air Exit Exit Exit Exit
Flow Flow 02 CC^ CO Temperature
(sca/hr) (scu/hr) (X) (X) (ppm) C°C)
w> u> «
_ H ~ o m a o
D °0 oo oo oo oo
-------
8£
Propan*
Flow
(fcm/hr)
£ ^
4
J
Air
Flow
(»c»/hr)
Exit
°2
(X)
Exit
Temperature
(°C)
V*
o
o o
1
L
o
o
J.
-J-
-------
r - , • • • i - %. + ¦ ¦ -j r
L A ^ ( - _ ( . ...
10
12
14
Time of Doy (hr)
T7--J- 18
Figure A-16. Afterburner operation for Test 8 (9/7/M)
-------
1000
3
" t ¦
ft
0
600
10"
0
500"
* I H
8
0
!*¦
4*
o
|s-
°C8
*v.
10
-Tru-h
i
12
~I
14
IB
Time of Doy (hr)
E,.J
Figure A-17. Kiln operation for Test 9 (9/9/88)
-------
1300
900
500
0
20
0
20
0
600
0
20
~r~
12
10
14
Time of Doy (hr)
Figure A-18. Afterburner operation for Test 9 (9/9/88)
f.J
IB
-------
Propane
FIov
C 81-%,'hr)
Air
Flow
(scm/hr)
Exit
°2
C)
Exit
Temperature
(°C)
t
-v .
3
3
1
o
O
C
s
u»
* o
o
O o
o o
73"
» *
Vv '
¦\S
*
u
1+
V
1
?*¦
\
a
o
o
-------
non
900
soo
¦¦ ¦
i
11
i
13
I
15
Time of Day (hr)
TZ
£.y
Figure A-20. Afterburner operation for Test 10 (9/20/88)
-------
1000
v
u
a
2 o
M Z°
m
600
20
M n H
0
500'
M
! oH
, 0~4 Q
(K U
0
16*
4*
———¦
\
n
~1
7~.+~ 10 12
j f -
"N ar Tlma of Day (hr)
Figure A-21. Kiln operation for Test 11 (9/22/88)
7>s^~14
-------
1300
900
500
0
20
_T_
10
I
12
Tims of Day (hr)
Figure A-22. Afterburner operation for Test 11 (9/22/88)
H
f r\J}
-------
APPENDIX B
ANALYTICAL LABORATORY REPORTS
In the following reports, each sample has been assigned a sample ID number which
consists of a letter prefix, eight numbers, and usually a one or more letter suffix. The prefix
denotes the sampling location as follows:
• A: Sample taken in the afterburner exit flue gas
• B: Sample of the scrubber blowdown
• E: Sample taken in the scrubber exit flue gas
• F: Sample of the incinerator feed
• Q: QA/QC sample prepared in the laboratory
• S: Sample taken in the stack gas
• T: Sample of the kiln ash
The first four digits of the eight-digit number represent the month and day the sample was
collected. The last four digits represent the 24-hour clock time the sample was collected. The
suffix denotes the sample type as follows:
• F: Filter sample
• FBK: Field blank sample
• FSK: Field spike sample
• II, 12, etc.: First impinger, second impinger, etc.
• M5: Method 5 train sample
• MSK: Matrix spike sample
• PW: Probe wash sample
46
-------
• T1, T2: First sampling train, second sampling train
• V: VOST sample
47
-------
MAftllV «* CAl»®»AlTW Pa O
»r t*i ae*«e
KINNHH • WOCOI
MiueixT
«*!L ¦ MUfCMfHS
KftCUTlvC »IC« »«t»lOt"T
VELMA M Hy|||
nc«r*«> rtiiti,
GALBR-tfrTH
J^aJroiaiczU.*, Unc.
P.O. box sieio
KNOXVIcLC. TN J7»I0-I«I0
QUANTITATIVE MICROANALYSES
ORGANIC - INORGANIC
«IB/S«a-13JS
33si SYCAMORE DR.
KNOXVILLC. TN 37921-17!
Ms. Joan Bass
Acurex Corporation
Highway 65 North
NCTR Building 45
Jefferson, Arkansas
72079
November 28, 1968
Received: October 31st
Dear Ms. Bass:
Analysis of your compounds gave the following results:
Your t,
Our #,
% C,
% H,
9b CI,
% O,
F08300840
C-7425
8.43
1.87
2.85
9.38
F08300850
C-7426
13.94
2.17
3.2£
9.96
F08300900
C-7427
17.70
2.43
3.17
S.40
F08311615
C-7428
12.99
1.96
3.05
9.04
F09090830
C-7429
13.87
2.09
3.37
8.41
F09130830
C-7430
14.91
2.18
0.31
10.12
F09130845
C-7431
16.67
2.45
< 0.01
9.18
F09130930
C-7432
16.88
2.49
0.03
8.16
F09160830
C-7433
14.94
2.14
3.07
9.51
F09160840
C-7434
14.59
2.22
3.09
8.63
F09160850
C-7435
12.02
1.81
2.90
9.65
F09200830
C-7436
11.08
1.83
2.94
9.71
F09200840
C-7437
15.52
2.22
2.17
8.23
F09200850
C-7438
13.93
2.03
2.88
10.39
F09211435
C-7439
0.88
1.78
S.83
8.98
F09211440
C-744D
14.08
1.82
5.83
8.91
irTTfK A*D»»IFM»MT« »TUJ. »»ll ¦ *.0. IO> S«IQ. UXOHVIIII. TM 10. OT*f» C»¦ »ll»S • »»JJ IVCAHOM D*. IK«> Villi TN J7»:
tmT»»Li»»io »»o
48
-------
Ms. Joan Bass
Page 2
November 28, 1988
Your #,
Our *,
% C,
% H,
% CI,
% O,
F09211445
C-7441
9.52
1.62
5.63
9.76
F09231410
C-7442
12.59
1.49
5.72
9.22
F09231420
C-7443
8.95
1.62
5.73
7.93
F09271515
C-7444
15.45
2.11
0.13
9.22
F09271520
C-7445
15.12
2.24
0.08
11.00
FD9271525
C-7446
16.53
2.43
0.06
9.54
F083J1600
C-7447
16.29
2.19
3.53
9.09
Sincerely yours,
GALBRAITH LABORATORIES, IHC-
Exec. Vice-President
GRH-.sc
49
OALSRAITH LABORATORIES- INC.
-------
ACUREX
'^Corporation
Environmental Systems Division
Acurex - CRF November 9, 1988
Acurex ID: 8810006
Client PO: 8328
Page 1 of 5
Attention: Larry Waterland
Subject: Analysis of 5 VOST Traps and 1 VOST Condensate Sample,
Received 9/22/88.
VOST traps were analyzed for purgeable organic compounds according to
the standard VOST protocol (Method 5040 Test Methods for Evaluating
Solid Waste EPA SW846 3rd. Ed., 1986). Results are presented in Table 1.
The method can be summarized as follows:
Traps are spiked with an internal standard and then desorbed
for ten minutes at 180"C. The desorbed compounds are swept
through a purging vessel containing 5 mL of water to retain
any HC1 and then onto an analytical trap for focusing. The
analytical trap i6 heated and back flushed with heliuir. to
desorb the purgeables onto a chromatographic column. The gas
chromatograph is temperature programmed to separate the
purgeables which are then detected with a mass spectrometer.
The VOST condensate sample was analyzed for purgeable organic compounds
according to U.S. EPA Method 8240 (Test Methods for Evaluating Solid
Waste - SW846, and Ed.,1962). Results are presented in Table 2. The
method can be summarized as follows:
Helium is bubbled through a 5-ml water sample in organic free
water contained in a specially designed purging chamber. The
purgeable volatile organic compounds are efficiently
transferred from the aqueous phase to the vapor phase. The
vapor is swept through a sorbent column where the purgeables
are trapped. After purging is completed, the trap is heated
and back flushed with helium to desorb the purgeables onto a
gas chromatographic column. The gas chromatograph is
temperature programmed to separate the purgeables that are
then detected with a mass spectrometer.
*65 Ciy0« Avem* *0 Bo» 70*4 Mountain V«w. CA 9*039 <418)961-3700 Tatoi &2SM1 FA* jai&j 964 SUS
50
-------
Acurex-CRF
B810006
Page 2 of 5
Qualitative identification of the priority pollutants is performed
initially using the relative retention tines and the relative
abundance of three unique ions. The entire mass spectrum is checked
before any final identifications are recorded. Quantitative analysis is
performed by the internal standard method using a single characteristic
ion and response factors obtained from a dally calibration standard. In
the tables, an entry such as "<5" means that the compound was not found
at a level above the laboratory's reporting limit. The reporting limit,
which is based on EPA reporting levels, has been corrected for any
sample dilution.
Prior to analysis, every sample is spiked with surrogate compounds as
part of Acurex's Quality Control Program. These compounds simulate the
behavior of compounds of interest and confirm that acceptable
recoveries are being achieved on every sample. The results of surrogate
recoveries are reported with the sample results.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Submitted by: WtdfAMjt 31m
Michael Flanagan
Research Chemist
Approved by:
Robej^ DeRosier
Client Services Manager
Submitted by: 1 fe. hm: Approved by:
/^harilei^h Main/gi
GC/MS Supervisor
T:
David R. Taylor, Pp
Manager, Quality Assurance
These results ware obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
51
-------
c
Acurex-cRF
8810006
Table 1. VOST Results Page 3 of 5
Acurex-CRF Sampl* ZD
Q0920
E0920
E0920
Q0920
1329
1328
1054
1056
VFSK
VT2
VT2*
VFBX
8240 Coapounds
ng/pair
ng/pair
ng/pair
ng/paii
Chloroaethane
43
<10
66
<10
Broaoaethane
<10
<10
<10
<10
Vinyl chloride
<10
<10
<10
<10
Chloroethane
<10
<10
<10
<10
Trichlorofluoroaethane
660
42
49
390
1,1-Dichloroethene
400
(137%)
<5
<5
<5
Acetone
<5
17
<5
25
Carbon disulfide
<5
<5
<5
11
Methylene chloride
36
9
<5
37
trans-1,2-Dichloroethene
<5
<5
<5
<5
1,1-Dichioroethane
<5
<5
<5
<5
2-Butanone
<5
<5
<5
<5
Chloroform
<5
330
53
<5
1,1,1-Trichloroethane
200
(64%)
<5
<5
<5
Carbon tetrachloride
<5
15
<5
<5
Benzene
160
(65%)
15
<5
<5
1,2-Dichloroethane
<5
<5
<5
<5
Trichloroethene
<5
<5
<5
<5
1,2-DichIcropropane
<5
<5
<5
<5
Bromodichloronethane
<5
380
95
<5
trans-l,3-Dichloropropene
<5
<5
<5
<5
4-Methyl-2-pentanone
<5
<5
<5
<5
Toluene
170
(71%)
300
200
<5
cis-l,3-Dichloropropene
<5
<5
<5
<5
1,1,2-Trichloroethane
<5
<5
<5
<5
Tetrachloroethene
190
(84%)
55
31
<5
2-Hexanone
<5
<5
<5
<5
Dibronochloronethane
-------
Table 1. VOST Results (Continued)
Acurex-CRT Sample ID
Acurex-CBF
8810006
Page 4 of 5
£0920
1430
Dup
Method
VT2*
Spike
Spike
Blank
824 0 Compounds
ng/pair t Recov
1 Reeov
ng/pair
Chlorcmethane
NQ
NS
NS
<10
Bromoaethane
HQ
NS
NS
<10
Vinyl chloride
NQ
NS
NS
<10
Chloroethane
NQ
NS
NS
<10
Trichlorofluoronethane
NQ
NS
NS
<5
1,1-Dichloroethene
NQ
120
104
<5
Acetone
NQ
NS
NS
-------
Acurex-CRF
881:006
Page 5 of 5
Table 2. Volatile Organic Reault*
Acurex-CRT Sample ZD
E0920
Method
Storage
Dup
1510VT2
Blank
Blank
Spike
Spike
824 0 Compounds
ug/L
ug/L
ug/L
% Recov
1 Recov
Chloroaethane
<10
<10
<10
NS
NS
Bromomethane
<10
<10
<10
NS
NS
Vinyl chloride
<10
<10
<10
NS
NS
Chloroethane
<10
<10
<10
NS
NS
Methylene chloride
27
<5
<5
NS
NS
Trichlorofluoromethane
<5
<5
<5
NS
NS
1,1-Dicfcloroether.e
<5
<5
<5
150
150
1,1-Dichloroethane
<5
<5
<5
NS
NS
trans-l,2-Dichloroethene
<5
<5
<5
NS
NS
Chloroform
<5
<5
<5
NS
NS
1,2-Dichloroethane
<5
<5
<5
NS
NS
1,1,1-Trichloroethane
<5
<5
<5
NS
NS
Carbon tetrachloride
<5
<5
<5
NS
NS
B r onod i ch 1 o r oine t h a n e
<5
<5
<5
NS
NS
1,2-Dichloropropar.e
<5
<5
<5
NS
NS
trans-l,3-Dichloropropene
<5
<5
<5
NS
NS
Trichloroethene
<5
<5
<5
120
120
Benzene
<5
<5
<5
130
130
DifcrojsochloroiTiethane
<5
<5
<5
NS
NS
1,1,2-Trichloroethane
<5
<5
<5
NS
NS
cis-1,3-Dichioropropene
<5
<5
<5
NS
NS
2-Chloroethylvinylether
<10
<10
<10
NS
NS
Bromofonr.
<5
<5
<5
NS
NS
1,1,2,2-Tetrachloroethane
<5
<5
<5
NS
NS
Tetrachloroethene
<5
<5
<5
NS
NS
Toluene
6
<5
<5
130
130
Chlorobenzene
<5
<5
<5
120
120
Ethylbenzene
<5
<5
<5
NS
NS
Dichlorobenzenes
<5
<5
<5
NS
NS
Date Analyzed
Surrogates
10/6/88 10/6/88 10/6/88
Percent Recoveriee (%)
10/6/8B 10/6/88
l,2-Dichloroethane-d4
Toluene-d8
p-Bromofluorobenzene
123
114
102
90
101
94
88
101
99
105
97
94
110
98
97
NS - Not spiked
54
-------
/¦S ACUREX
Corporation
Environmental Systems Division
Acurex - CRF November 2, 1988
Acurex ID: 8810013
Client PO: 8327
Page X of 8
Rev. 12/21/88
Attention: Larry Waterland
Subject: Analysis of 23 Samples, Received 9/27/88.
Water samples were analyzed for requested metal¦ using inductively
coupled argon plasma spectroscopy or atonic absorption spectroscopy
following Methods for Chemical Analysis of Water and Wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
Soil samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2. Sample T0920 1558 was
rerun for barium and the data confirmed (see page 7).
Samples B08251354, T08301450, and T09161625 could not be analyzed
because the bottles were broken in transit.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Subaitted by: iC^> Approved by: <-
Maryann Gambino ftob^ft Defcosii
;ier
Supervisor, Inorganic Chemistry Client Services Manage:
Approved by
David R. Taylor,
Quality Assurance Manager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages*
4SS CiyO» *••*>*. P.O Bo« 1Q** Meunuw Vmm. CA MOW cam 961S70C Mi 325961 H'Si »64 !i'4S
55
-------
urex-CRF
'10013
Page 2 of 8
Rev. 12/21/8B
Table 1.
Metals Results
Acurex-CRF
Sanple
ZD
EPA
Kethod
£0825
1211M5
11 t 12
2082S
1211X5
13
E0B25
1211M5
14
EOS 2 5
1211M5
PW
AOE25
1200
11 t 12
Parameter
B9/L
ag/L
ag/L
ng/L
ag/L
Arsenic
Barium
Bisautft
Cadnium
ChromiuD
Copper
Lead
Magnesium
Strontium
206.2
200.7
200.7
200.7
200.7
200. 7
200.7
<0.01
0.023
<0.1
<0.01
0.011
0.029
<0.01
0.11
0.02
<0.01
0.046
0.29
<0.01
0.011
0.038
<0.01
0.21
0.04
<0.01
0.04
0.39
0.088
0.13
0.14
0.55
0.91
0.11
<0.05
<0.05
1.3
<0.05
0.85
0.42
0.02
<0.25
0.1
0.062
0.59
2.2
1.1
98
9.1
1.2
2.0
0.2
Sample vclume (jt.L)
.
1310
150
265
39
1240
Volume used (mL):
100
100
100
20
100
Dilution factor:
1
1
1
5
1
Chloride aliquot*
(mL) :
100
—
—
—
100
Note: Dilution factors are already incorporated in data above.
* - Aliquot taken at CRF, not included in above •ample volume.
56
-------
Aeurex-i-r
8810013
Page 3 of t
Rev. 12/21/88
Table i.
Metals Results
Acurex-CRF Sample
ID
AOS 2 5
AOS 2 5
AOS 2 5
1200
1200
1200
BOS 2 5
BOB2S
13
14
m
1124
1254
EPA
Parameter
Method
stg/L
mg/L
mg/L
mg/L
ULf/L
Arsenic
206.2
<0.01
<0.02
0.19
0.036
0.065
Barius
200.7
0.29
0.61
<0,02
1.2
0.87
Bismuth
<0.1
0.26
2.1
1.1
3.3
Cadaium
200.7
0.031
0.32
2.1
0.14
0.28
Chromium
200.7
0.091
0.36
0.87
0.094
0.2
copper
200.7
0.19
0.82
8.2
1.2
1.1
Lead
2 00.7
0.036
2.2
2.6
0.68
1.4
Hagnesiuc
200.7
0.71
2.4
3.0
20
23
Strontiua
C.l
0.28
<0. 02
2.4
1.9
Sample volume {reI.)
295
92
116
2 SO
265
Voluir.e used (mL):
100
50
50
100
100
Dilution factor:
1
2
2
1
1
Note; Dilution factors are already incorporated in data above.
57
-------
Ar-ur -~RF
oelOCU
Page 4 of 8
Table l. Metals Results
Acurex-CRF Sample ZD E0825
E0825 1211M5
1211M5 11 4 12
Parameter
EPA
Method
BOB25
14S4
mg/L
B0825
1554
mg/L
BOB 2 5
1630
mg/L
11 4 12
Spile*
% Recov
Dup
Spike
RPD
Arsenic
206.2
0.058
0.15
0.13
86
5.9
Barium
200.7
0.97
0.87
0.83
97
0.56
Bismuth
4.7
3.1
2.1
88
17
Cadmium
200.7
0.52
0.33
0.27
101
0.3
Chromium
200.7
0.42
0.39
0.29
97
0.24
Copper
200.7
4.8
2.4
2.2
92
0.47
Lead
200.7
2.7
1.9
1.4
104
1.9
Magnesium
200.7
26
23
20
91
0.52
Strontius
1.9
1.8
1.7
101
0
Sample volur.e £nL) :
255
260
260
1310
1310
Volume used (ir.L.) :
100
100
100
100
100
Dilution factor:
1
1
1
1
1
Note: Dilution factors are already incorporated in data above.
58
-------
Table 1. Kerala Results
Acur«v--->-
BBlOOij
Page 5 of 8
Rev. 12/21/86
Acurex-CRF sample ID
Blank
EPA
——
Parameter
Method
ag/L
Arsenic
206.2
<0.01
Bariua
200.7
<0.01
Bismuth
0.36
Cadmium
200.7
<0.01
Chromium
200.7
<0.01
copper
200. 7
<0. 01
Lead
200.7
0.0017
Magnesium
200.7
<0.05
Strontium
<0.01
Method
Method Detection
Liait
mg/L
0.01
0.01
0.1
0.01
0.01
0.01
0.001
0.05
0.01
Sample volur.e (cL) : 100
Volume used (mL): 100
Dilution factor: 1
Note: Diiutior. factors are already incorporated in data above.
59
-------
Acurex-CRF
8810013
Page 6 of 8
Rev. 12/21/8B
Table 2. Metals Results
Acur«x-CR7 Sample ZD
E0825
00926
1211
1240
TOE 2 5
TO907
T0909
M5F
TBK
1636
1530
1520
Parameter
EPA
Method
ag/fllt
ag/fllt
mg/kg
mg/kg
mg/kg
Arsenic
7060
0.033
<0.001
27
18
21
Barium
6010
0.057
0.016
24
68
43
Bisiruth
2.4
0.038
20
25
13
Cadmium
6010
0.2
<0.001
<1
<1
<1
Chromiua
6010
0.16
0.008
93
55
82
Copper
6010
3.0
0.007
240
180
210
Lead
6010
1.5
0.0022
4.9
5.0
2 . 0
Magnesium
6010
5.9
0.58
39000
20000
27000
Strontium
0.025
0.15
74
75
160
60
-------
Acurex-CRF
8810013
Page 7 of 8
Rev. 12/21/88
Table 2. Metals Results
Acurex-CRf Sample ID
T0825
T0825 1636
T0914
TO920
T0922
1636
Dup
1500
1558
1539
Spike
Spike
EPA
Parameter
Method
ng/fcg
ag/kg
lag/kg
% Recov
RPD
Arsenic
7060
27
21
29
125
6.5
Barium
6010
24
360
36
106
1.3
Bismuth
41
21
51
136
13
Cadmium
6010
<1
<1
<1
86
1.7
Chromium
6010
75
66
75
93
5
copper
6010
200
200
190
137
5.7
Lead
6010
3.7
3.0
3.4
111
18
Magnesium
6010
27000
22000
25000
81
5.1
Strontiun
82
120
120
129
7.6
61
-------
Acurex-CRF
8810013
Page 8 of 8
Rev. 12/21/88
Table 2. Metals Results
Acurex-CRF Sample ID
Method
Method
Detection
rni
Blank
Limit
Paraaeter
tr A
Method
ag/L
ng/Kg
Arsenic
7060
<0.01
1
Barium
6010
<0.01
1
Bismuth
<0.1
10
Cadmium
6010
<0.01
1
Chroaiur:
6010
<0.01
1
Copper
6010
0.01B
1
Lead
6010
0.0018
0.1
Magnesium
6010
<0.05
5
Strontium
<0.01
1
62
-------
£
ACUREX
Corporai
Corporation
Environmental Systems Division
Acurex - CRT
November 2, 1968
Acurex ID: 8810014
Client PO: 8327
Page 1 of 5
Rev. 12/21/88
Attention: Larry Water-land
Subject: Analysis of 15 Water Samples, Received 9/29/88.
Water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
v
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. Zn no event shall Acurex be liable for
special or consequential damages.
Approved bv:
Maryaim Ganbino
Supervisor, Inorganic Chemistry
Robert DeRosier
Client Services Manager
Approved
MiDyMtKM PO BbiTOM MoukU* Vot.CA M03S M15I961-5700 T»tti 325S6' »**
63
-------
Acurex-CRF
88100X4
Page 2 of 5
Tabic X. Metals Results
Acurex - CRT Sample ID
EPA
Method
B0830
1114
BO830
1214
BOS 30
1314
BO830
1414
B0830
1444
Parameter
mg/L
Bg/L
«g/L
mg/L
mg/L
Arsenic
Bariun
Bismuth
Cadsiua
Chromium
Copper
Lead
Magnesium
Strontiuit
206.2
200.7
200.7
200.7
200.7
200. 7
200.7
1.7
0.34
2.6
2.8
3.0
21
4.1
95
1.5
0.076
0.97
3.2
0.23
0.24
2.3
1.7
18
1.2
0.2
1.1
5.5
0.38
0.46
3.7
2.5
24
1.2
0.22
1.3
3.5
0.32
0.36
2.6
1.5
20
1.2
0.14
1.2
3.4
0.47
0.44
2.9
1.7
22
1.2
Sanple volume (ciL) :
126
190
222
244
225
Volume used (mL):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
Note: Dilution factors are already incorporated in data above.
64
-------
Acurex-CRF
8810014
Page 3 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex - CRT Saaple ID
E0830
EO830
ZO830
EOS 30
A0830
1117K5
1117M5
1117M5
1117M5
1114
11 6 12
13
24
PVr
11 i 12
Parameter
£ r A
Method
mg/l
mg/l
mg/L
mg/l
mg/L
Arsenic
206.2
<0.01
<0.01
<0.02
<0.05
0.039
Barium
200.7
0.02
0.041
0.062
<0.05
4.4
Bissuth
0.22
0.3
0.42
<0.5
2.0
Cadmiun
200.7
<0.01
<0.01
<0.02
0.073
0.51
Chromium
200.7
<0.01
<0.01
<0.02
<0.05
410
Copper
200.7
0.029
0.06
0.14
1.7
6.2
Lead
200.7
<0.01
<0.01
0.0039
0.016
2.1
Magnesium
200. 7
0.066
0.23
0.5
<0.25
7.4
Strontium
<0.01
0.04
0.08
<0.05
0.25
Sair.ple volume (nL)
:
13B0
420
115
68
1125
Volume used (siL) :
100
100
50
20
100
Dilution factor:
1
1
2
5
1
Chloride aliquot*
(nL) :
100
—
—
—
100
Note: Dilution factors are already incorporated in data above.
• - Taken at CRF, not included in sample volume listed above.
65
-------
Table 1. Metals Results
Acurex-C^F
88* ">014
Page 4 of 5
Rev. 12/21/88
Acurex - CRF Sample ID
EOS 30
E0830 1117,5
A0830
AOS 30
AOS 30
1117,5
11 k 12
1114
1114
1114
XI & 12
Dup
TBI
13
X4
PW
Spike
Spike
Paraaeter
trn
Method
mg/l
ng/L
mg/L
1 Recov
RPD
Arsenic
206.2
0.013
<0.01
0.023
95
3.3
B&riuc
200.7
1.5
0.16
0.66
101
3.6
Bismuth
0.96
0.59
0.59
93
14
Cadmium
200.7
0.083
0.042
0.047
106
2.8
Chronium
200.7
0.23
0.044
0.081
102
2.8
Copper
200.7
0.54
0.31
0.82
96
3.6
Lead
200 .7
0.22
0.062
0.41
104
11
Kagnesiuir.
200.7
0.57
0.36
7.8
95
4.5
Strontium
0.05
0.04
0.83
105
2.9
Sar.ple volume (jnL) :
Volume used (&L):
Dilution factor:
670
100
1
600
100
1
205
100
1
1380
100
1
1380
100
1
Note: Dilution factors are already incorporated in data above.
66
-------
Acurex-CRF
8810014
Pag* 5 of 5
Rev. 12/21/88
Table 1. Metal* Results
Acurex - CRT Sample ID
Method
Method
Detection
Blank
Limit
EPA
Paraneter
Method
mg/L
mg/L
Arsenic
206.2
<0.01
0.01
Barium
200.7
<0.01
0.01
Bismuth
0.14
0.1
Cadmium
200.7
<0.01
0.01
Chromium
200.7
<0.01
0.01
Copper
200.7
0.013
0.01
Lead
200.7
<0.001
0.001
Magnesium
200.7
<0.05
0.05
Strontium
<0.01
0.01
Sample voluiae (p,^) : ' 100
Volume used (mL): 100
Dilution factor: 1
Note: Dilution factors are already incorporated in data above.
67
-------
/\ ACUREX
Ar^ CorDorati
Corporation
Environmental Systems Division
Acurex - CRF
October 21, 1968
Acurex ID: 8810015
Client PO: 83 27
Page l of 5
Rev. 12/21/88
Attention: Larry Materland
Subject: Analysis of 12 Water Samples, Received 9/27/88.
Water samples ware analyzed for requested metals using inductively
coupled Argon Plasma Spectroscopy or atonic absorption spectrometry
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
«6S C>yaa Annu* PO Btu 70*4. Mount** vww. CA »«C38 HIS) (61-S700 32S&61 n>5)»6*Si«:
Maryapn Gambino
Supervisor, Inorganic Chemistry
Client Services Manager
68
-------
Table 1. Metals Results
Acurex-CRF Saaple ID
Parameter
Chromium (hex.)
EPA
Hethod
B0926
1040
(SBD6)
ag/L
0.13
B0926 B0926
1140 1240
(SBD6) (SBD6)
Acurex
8810015
Page 2 of 5
Rev. 12/21/88
B0926 E0926
1331 1055
(SBD6) (RKS PORT)
ag/L
0.099
mg/L
0.31
ag/L
0.4
ng/L
2.6
Sample volume, Total (aL):
sample volume, Used (nL):
Sample weight, Ash (aig) :
Sample volume. Chloride* (aL):
140
100
144
100
152
100
ISO
100
154
100
Aliquot taken at CRF, not included in total volume.
69
-------
*<
udlOOXS
Page 3 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF sanple ZO
E0926 E0926 E0926 A0926 A0926
1047 1047 1047 1039 1039
M5T2I-1 M5T2I-2 M5T2I-3 M5T2I-1 M5T2I-2
EPA
Parameter Method ag/L ng/L mg/L ng/L mg/L
Chromium (hex.) 0.061 0.044 0.015 0.01 <0.003
Sample volume, Total (&L): 1045
Sample volume, Used (bL): 100
Sample weight, Ash (»g):
Sample volume, Chloride* (mL): SO
* - Aliquot taken at CRF, not included in total volume.
315 182
100 100
so
232 158
IOC IOC
50 50
70
-------
Table 1. Metals Results
Acurex-CRF sample ID
Acur*>
8810015
Page 4 of 5
Rev. 12/21/88
A0926
1039
M5T2I-3
Parameter
Chromium (hex.)
EPA
Method
Bg/L
<0.006
T0926
1345
RV284 Spike
ag/L % Recov
Dup Method
Spike Blank
RPD
0
nig/L
<0.003
0.012
102
Sample volume, Total (aL) :
Sair.ple volune, Used (aL) :
Sar.ple weight. Ash (ag) :
Sample volune, Chloride* (aL):
87
50
400
100
100
1045
100
1045
100
100
100
* - Aliguct taken at CRF, not included in total volume.
71
-------
Acurex
8810015
Page 5 of 5
Rev. 12/21/88
Table l. Metals Results
Acurex-CRF Sample ID
Method
Detection
Limit
EPA
Parameter Method ®g/L
Chromium (hex.) 0.003
72
-------
ACUREX
Corporation
Environmental Systems Division
Acurax CRF October 18, 1966
NCTR Bid. 45 Acurex ID: 8810016
Jefferson, AH Client PO: 8327
Page 1 of 5
Rav. 12/21/88
Attention: Larry Waterland
Subject: Analysis of 14 Water Samples, Received 9/30/88.
Water samples were analyzed for requested natals using inductively
coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
If you should have any technical questions, please contact Robert DeFosie:
at (415)961-5700.
Submitted by: J/- > s.'o t~ Approved by:
Karyaftn Gambino Robert DeRcsier
Supervisor, Inorganic Chemistry Client Services Manage:
Approved by: |^>
David R. Taylor, PhD/j
Quality Assurance MaMger
These results were obtained by following standard laboratory
procedures; the liability of Acurax Corporation shall not exceed the
amount paid for this report. In no event shall Acurax be liable for
special or consequential damages.
>e; Cri« PO BOi 70U Mn;mim V>» CA W03H I41S)MI'370G TtHi MiM' f*« l«!5> il*5
73
-------
Table 1. Metals Results
ACUREX CRT Sample IB
ACUREX CRF
8810016
Page 2 of 5
Rev. 12/21/88
Parameter
Chroaiua (hex.)
EPA
Method
218.4
B0928
0932
0.032
B0928
1032
¦5/1"
0.09
10928
1132
¦f/L
0.072
B0928
1229
¦g/L
0.067
F0928
0950
wg/L
0.93
Sample volume, Total (ml.)
Sanple volune, Used (ust)
Saisple weight. Ash (sg)
Aliqyot taken for chloride
analysis* (ssL):
136
100
134
100
150
100
140
100
136
100
* - Taken at CRF, before shipment of sanple.
74
-------
ACUREX CRF
B810016
Page 3 of 5
Rev. 12/21/68
Table l. Metals Results
ACUREX CRF Sample 10
E0928 E0926 E0928 A0928 A0928
0940M5 0940M5 0940M5 0931M5 0931M5
<1-1,T2) (1-2,T2) (1-3,T2) (I-1.T2) (1-2,T2)
Parameter Method mg/L mg/L ag/L mg/L ag/L
Chromium (hex.) 218.4 0.006 0.032 0.007 0.46 <0.003
Sample volume. Total (mL) : 1140 305 165 400 156
Sample volume, Used (aL): 100 100 100 100 100
Sample weight, Ash (ag):
Aliquot taken for Chloride
analysis4 (mL): 50 50 — 50 50
* - Taker, at CRF, before shipment of sair.ple.
75
-------
Parameter
Chromium (hex.)
Table 1. Metals Results
ACUREX CRT Sanple IS
ACUREX CRF
6810016
Page 4 of 5
Rev. 12/21/88
EPA
Method
A0928
0931M5
(1-3,T2)
T0928
1231
Q0929
0830FSK
£0928
0940M5
Q0929 (I-1.T2)
0831FSK Spike
ng/L
0.029
mg/h
0.063
ag/L
0.97
ag/L
1.6
% Recov
94
218.4
Sample volume, Total (bL):
Saaple volume, Used (»L):
Sample weight, Ash (mg):
Aliquot taker; for Chloride
analysis*
-------
Table 1. Metals Results
ACUREX CRF Saaple ID
Method
DUP METHOD Detection
SPIKE BLANK Limit
Parameter Method RPD ag/L ng/L
Chromium (hex.) 218.4 6.2 <0.003 0.003
Sample volume. Total (bLJ: 1140 100
Sample volume, Used (mL) : 100 100
Sample weight, Ash (mg): -- —
Aliquot taken for Chloride
analysis* (mi;:
* - Taken at CRF, before shipment of sample.
77
-------
/N ACUREX
Corporation
Environmental Systems Division
Acurex - CRF October 13, 1988
Acurex ZD: 8810017
Client PO: 8327
Page 1 of 5
Rev. 12/20/88
Attention: Larry Katerland
Subject: Analysis of 14 Samples, Received 9/30/88.
Water samples were analyzed for requested metals using inductively
coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Submitted by:_
jl
Maryanp 'Gambmo
Supervisor, Inorganic Chemistry
Approved bv. >~c
Robert DeRosier
Client Services Manager
Approved by:
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
4«5 Clyde Av«nu«. PO Bai 70*4. Mount*it v»« C* »403B (41S> #«lS70O Tmmi 32JW FA* <4l», 964 S14J
78
-------
Acurex-CRf
8810017
Page 2 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex - CRF Sample ID
EPA
Method
B0929
0908
B0929
100S
B0929
1108
B0929
1159
Q0929
1030
BSK
Parameter
mg/L
mg/L
mg/L
ng/L
mg/L
Chromium (hex.)
218.4
0.028
0.1
0.28
0.23
0.19
Sample volume,
Total (mLJ:
151
151
150
144
50
Sample volume,
Used (bL):
100
100
100
100
25
Sample Keigh
t, Ash (g):
—
79
-------
#icurex-CP
881001/
Page 3 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex - CRT Sample ID
£0929 £0929 £0929
F0929 T0929 0920 0920 0920
0908 1200 MS1-1 M5I-2 M5I-3
EPA
Paraaeter Method mg/L iig/L mg/L mg/L ng/L
Chromium (hex.) 218.4 2700 0.067 <0.003 0.014 <0.003
Sample volume. Total (mL): 115 400 1460 385 17<
Sample volume, Used (mL): 100 100 100 100 100
Sar.ple Weight, Ash (g) : 100
Sanple volume. Chloride* (mL): 50 50
* - Taken at CR~, net included in total reported in this report.
80
-------
Table 1. Metals Results
Acurex - CRT staple ID
Parameter
Chrostiua (hex.)
EPA
Method
218.4
A0929
0507
M5I-1
af/L
0.11
A0929
0907
M5I-2
mg/L
0.026
Acurex—.- .
8810017
Page 4 of S
Rev. 12/21/86
£0929
A0929
Q0929
0920
0907
1400
M5I-1
m i-3
TSK
Spike
WQ/lj
Bg/L
% Recov
0.014
2.7
94
Sample volume, Total (mL) ¦' 360 145
Sample volume, Used (oL): 100 100
Saisple Weight, Ash (g) :
Sacple volume, Chloride* <»L)i 50 50
137 400 1460
100 100 100
100.22
• - Taken at CRF, not included in total reported in this report.
81
-------
Table 1. Metals Results
Acurex - CRT sample ID
Parameter
Chromium (hex.)
EPA
Method
£0929
0920
MSI-1
KSD
RPD
24
Method
Method Detection
Blank Limit
ag/h
<0.003
»g/L
0.003
21B.4
Sample volume, Total (biL)
Sample volume. Used (rL)
Sample Weight, Ash (g)
1460
100
100
100
82
-------
ACUREX
Ar~* Coroorat
rr> Corporation
Efwironftierv*"! Systems Division
Acurex - CRF
November 1, 1988
Acurex ID: 8810018
Client PO: 8327
Page l of 5
Rev. 12/21/88
Attention: Larry Waterland
Subject: Analysis of 1? Water Samples, Received 10/4/88.
Water sanples were analyzed for requested netals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
445Cy
-------
Aeurex-CRF
8810016
Page 2 of 5
Table l. Metals Results
Acurex-CRF Sample ID
B0907
B0907
B0907
B0907
B0907
1135
1235
1335
1435
1529
EPA
Paraaeter
Method
mg/b
mg/L
mg/L
ng/L
ng/L
Arsenic
206.2
0.068
0.087
0.11
0.15
0.13
Barium
200.7
1.1
1.2
1.2
1.4
1.3
Bismuth
2.2
3.1
3.4
4.6
2.8
Cadmium
200.7
0.14
0.19
0.21
0.37
0.28
Chromium
200.7
0.27
0.37
0.39
0.68
0.59
Copper
200.7
2.4
2.7
2.0
3.6
2.9
Lead
200.7
1.9
2.2
1.5
2.4
1.7
Magnesium
200.7
16
18
16
22
19
Strontium
1.9
2
1.9
2
1.7
Sample volume (mL):
236
232
210
235
220
Volume used (mL):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
Kote: Dilution factors are already incorporated in above data.
84
-------
Acurex-CRF
8810016
Page 3 of 5
Rev. 12/21/88
Table l.
Metals Results
Acurex-CRF Sample
ZD
£0907
£0907
F0823
FOB 30
F0907
1157M5
1157M5
POl
1331
114B
1241
11, 12
13
Ir A
Parameter Method
ng/L
¦g/L
mg/L
mg/L
mg/L
Arsenic 206.2
2300
2400
2400
<0.01
<0.01
Barium 200.7
1800
2400
2500
0.028
0.056
Bisouth
6600
7400
9400
0.2
0.29
Cadsiusi 200.7
410
530
520
<0.01
<0.01
Chromium 200.7
2300
2900
3100
0.015
0.011
Copper 200.7
23000
30000
32000
0.17
0.23
Lead 200.7
2400
3100
3200
<0.001
<0.001
Magnesium 200.7
3400
4300
4400
<0.05
0.62
Strontium
11000
14000
15000
<0.01
0. 06
Sample volune (nL):
—
—
—
920
220
Volume used (nL):
2
2
2
100
100
Dilution factor:
50
50
50
1
1
Chloride aliquot* (sL):
—
—
—
100
—
Note: Dilution factors are already incorporated in above data.
~ - Aliquot taken at CRF, not included in above Banple volume.
85
-------
Acurex-CRF
6810018
Page 4 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF Sample ID
E0907
£0907
A0907
A0907
A0907
1157M5
1157M5
1129M17
1129M17
1129M17
Vfik
14
pw
11, 12
14
PW
Parameter
£rn
Method
mg/L
mg/L
mg/L
mg/h
mg/L
Arsenic
206.2
<0.02
<0.
05
0.027
<0.01
<0.02
Barium
200.7
0. 087
<0.
05
5.1
0.67
<0.02
Bismuth
<0.2
<0
i.5
1.8
0.99
0.64
Cadmium
200.7
<0.02
<0.
05
0.22
0.069
0.28
Chromium
200.7
0.025
0
1.2
161
0.26
0.7
Copper
200.7
0.38
0.
78
4.2
0.61
7.9
Lead
200.7
0.0057
0.
11
1.3
0.17
0.16
Magnesium
200.7
0.98
<0.
25
2.8
1.1
1.3
Strontium
0. 06
<0.
05
0.16
0.11
<0.02
Sample volume (ir.L)
:
122
59
1061
305
90
Volume used (mL):
50
20
100
100
50
Dilution factor:
2
5
1
1
2
Chloride aliquot*
(mL) :
--
—
100
—
—
Note: Dilution factors are already incorporated in above data.
* - Aliquot taker, at CRT, not included in above sample volume.
86
-------
Acurex-CRF
8B10018
Page 5 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF Sample ZD
E0907
E0907
1157M5
1157M5
Method
11, 12
11, 12
Method
Detection
Spike
KSD
Blank
Limit
Paraneter
&rA
Method
% Recov
RPD
mg/L
mg/L
Arsenic
206.2
81
1.6
<0.01
0.01
Barium
200.7
105
3.0
<0.01
0.01
Bisnuth
90
15
<0.1
0.1
Cadrium
200.7
105
0. 94
<0.01
0.01
Chromium
200. 7
104
2.2
<0.01
0.01
Copper
200.7
99
2.3
<0.01
0. 01
Lead
200.7
106
6.7
<0.001
0.001
Kagnesiur.
200.7
97
2.4
<0.05
0.05
Strontium
109
0.94
<0.01
0.01
Sample volume (aL):
920
920
100
Volume used (nL):
100
100
100
Dilution factor:
1
1
1
Note: Dilution factors are already incorporated in above data.
87
-------
ACUREX
Corporation
Environmental Systems Division
Acurex - CRT November 8, 198B
Acurex ID: 8810019
Client PO: 8327
Page 1 of 5
Rev. 12/21/88
Attention: Larry Waterland
Subject: Analysis of 5 Solid Samples, Received 10/4/88.
Filter samples and solid samples were analysed for requested metals
using Inductively Coupled Argon Plasma Spectroscopy or atomic
absorption spectrometry following Test Methods for Evaluating Solid
Waste. The EPA method employed is listed alongside of the parameter.
Samples were prepared using EPA method 3050 by digesting the sample in
acid prior to analysis. The results are presented in Tables l and 2.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Approved by: J. .-/»« 325#«1 r*K <«15! 96* S'«S
88
-------
Acurex-CRF
B810019
Page 2 of 5
Rev. 12/21/68
Table 1. Metals Results
Acurex-CRF Sample ID
£0830 E0907
1117
1157
Dup
Method
M5
M5
Spike
Spike
Blank
Parameter
trA
Method
¦g/filt
ng/filt
% Recov
RPD
ng/L
Arsenic
7060
0.048
0.037
77
19
<0.01
Barium
6010
0.018
0.023
104
3.7
0.035
Bisauth
2.3
1.6
64
16
<0.1
Cadniun
6010
0.34
0.22
93
0.44
<0. 01
Chromium
6010
0.09
0.12
94
0.99
0.026
Copper
6010
2.7
2.1
94
2.2
<0.01
Lead
6010
1.5
1.0
100
0
<0.05
Magnesium
601C
0.66
0.74
122
13
1.3
Strontium
0.15
0.17
104
23
<0. 01
89
-------
Acurex-CRf
8610019
Page 3 of 5
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF Sample ZD
Method
Detection
Limit
EPA
---
Parameter
Method
mg/kg
Arsenic
7060
l
Barium
6010
l
Bismuth
10
Cadmium
6010
l
Chromium
6010
i
Copper
6010
l
Lead
6010
5
Magnesium
6010
5
Strontium
90
-------
Acurex-CRF
8810019
Page 4 of s
Table 2. Metals Results
Acurex-CRF Sample ZD
T0926
1345
EPA
Parameter Method ag/kg
Chroisiua 6010 75
T0929
T0929
1200
T092S
T0929
1200
Dup
1231
1200
Spike
Spike
ag/kg
¦g/kg
t Fecov
RPD
110
86
115
7.9
91
-------
Table 2. Metals Results
Acurex-CRF Sanpla ZD
Method
Method Detection
Blank Limit
Parameter Method ag/L mg/kg
Chromium 6010 <0,01 1
Acurex-CRF
8810019
Page 5 of 5
92
-------
ACUREX
if* Corporation
Environmental Systems Division
Acurex - CRT
November 8, 1988
Acurex ID: 8810031
Client PO: 8327
Page 1 of 6
Rev. 12/21/88
Attentions Larry Katerland
Subject: Analysis of 17 samples, Received 10/6/88.
Water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table l.
Filter samples were analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. Zn no event shall Acurex be liable for
special or consequential damages.
Chemistry
Approved by:
Robert DeRosier
Client Services Manager
Clyw *«•"«« P.o Bo. 70m. Mo«nU» Mn CA MD3S <«1S! #€1S70O T«*> 325961 FAX mil »64
93
-------
c
Acurex-CRF
8810031
Page 2 of 6
Table l. Metals Results
Acurex-CRF sample
ID
EPA
Kethod
B0909
1125
B0909
1225
B0909
1325
B0909
1425
B0909
1520
Parameter
ng/L
mg/L
ng/L
mg/L
ng/L
Arsenic
Barium
Bismuth
Cadmium
Chromium
Copper
Lead
Magnesium
Strontium
206.2
200.7
200.7
200.7
200.7
200.7
200.7
0.023
0.8
0.92
0.071
0.095
0.81
0.61
9.4
0.88
0.052
0.93
2.7
0.19
0.29
1.8
1.5
21
1.1
0.075
0.85
3.1
0.28
0.47
2.3
1.9
25
1.1
0.089
0.81
2.7
0.23
0.36
1.7
1.2
21
1.1
0.077
0.79
2.0
0.29
0.4
1.8
1.1
20
1.0
Sample volume (mL)
194
234
212
224
230
Volume used (mL):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
Chloride aliquot*
(mL) :
—
—
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Aliquot taken at CRF, not included in above sample volume.
94
-------
' Acurex-CRF
88X0031
Pag* 3 of 6
Rev. 12/21/88
Tabls 1. Metals Results
Acur«x-CRF Sample ID
£0909 E0909 E0909 E0909
F0909 1126M5 1126M5 1126K5 1126M5
1300 1-1,1-2 1-3 1-4 PW
Parameter
EPA
Method
ag/L
»g/L
»g/L
ag/L
mg/L
Arsenic
206.2
2300
<0.01
<0.01
<0.02
<0.05
Barium
200.7
2S00
0.028
0.061
0.1
<0.05
Bismuth
11000
0.47
<0.1
<0.2
<0.5
Cadmium
200.7
540
<0.01
<0.01
0.029
0. 069
Chromium
200.7
3000
0.013
0.013
0.023
0.053
Copper
200.7
31000
0.46
0.21
0.18
0.71
Lead
200.7
3100
<0.001
<0.001
0.0027
0.075
Magnesium
200.7
4600
0.13
0. 6
1.2
<0.25
Strontium
16000
<0.01
<0.01
<0.02
<0.05
Sample volume (mL)
,
1050
228
108
80
Volume used (mL) :
2
100
100
50
20
Dilution factor:
50
I
1
2
5
Chloride aliquot*
(mL) :
..
100
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Aliquot taken at CRF, not included in above sample volume.
95
-------
Acurex- i-.F
8810031
Page 4 of 6
Rev. 12/21/88
Table x. Metals Results
Acurex-CRF Supple ZD
A0909
A0909
A0909
A0909
£0909
1122M17
1122M17
1122M17
1122M17
1126K5
1-1,1-2
1-3
1-4
PVf
Spike
Parameter
£. f A
Method
ag/L
¦g/L
mg/L
mg/L
% Recov
Arsenic
206.2
<0.01
<0.01
<0.01
0.031
86
Barium
200.7
5.3
2.1
0.29
0.11
104
Bismuth
3.0
<0.1
<0.1
4.8
83
Cadmium
200.7
1.0
<0.01
<0.01
2.7
102
Chromium
200.7
810
0.31
0.15
50
102
Copper
200.7
19
0.23
0.23
19
84
Lead
200.7
6.6
0.016
0.0086
4.1
122
Magnesium
200.7
6.5
1-4
0.99
120
98
Strontium
0.11
0.05
<0.01
0.21
103
Sample volume (mL)
,
815
524
580
200
1050
Volume used (r.L) :
100
100
100
100
100
Dilution factor:
1
1
1
1
1
Chloride aliquot*
(mL) :
100
—
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Aliquot taken at CRF, not included in above sample volume.
96
-------
A -jx-CR T
8810031
Page 5 of 6
Rev. 12/21/88
Table 1. Metals Results
Aeurex-CJtF Sample 10
EPA
Parameter Method
Arsenic 206.2
Barium 200.7
Bismuth
Cadaiun 200.7
Chromium 200.7
Copper 200.7
Lead 200.7
Kagnesiun 200.7
Strontium
E0909
1126M5
Method
Dup
Method
Detection
Spike
Blank
Limit
RPD
mg/L
®g/ L
4.2
<0. 01
0.01
0.93
<0.01
0.01
0.77
<0.1
0.1
1.7
<0.01
0.01
0.77
<0.01
0.01
2.0
<0.01
0.01
2.1
<0.001
0.001
1.4
<0.05
0.05
3.3
<0.01
0.01
Sample vclune (mL): 1050 100
Volume used (mL;: 100 100
Dilution factor: 1 1
NOTE: Dilution factors are already incorporated in above data.
97
-------
Acurex-rRF
BB10031
Page 6 of 6
Table 2. Metals Results
ACurex-CRF Sample XD
E0909
Method
1126
Dup
Method
Detection
M5F
Spike
Spike
Blank
Lin it
EPA
Parameter
Method
ag/filt*
t Recov
RPD
mg/L
mg/kg
Areenic
7060
0.039
77
19
<0.01
1
Bariut
6010
0. 016
104
3.7
0.035
1
Bismuth
1.4
64
16
<0.2
20
Cadmium
6010
0.27
93
0.44
<0.01
1
Chromium
6010
0.041
94
0.99
0.026
1
Copper
6010
2.1
94
2.2
<0.01
1
Lead
6010
1.4
100
0
<0.05
5
Hagnesium
6010
0.64
122
13
1.3
5
Strontium
0.14
104
23
<0.02
2
~ - 0.1 liter after digestion
98
-------
ACUREX
Ar x Corporation
Environmental Systems division
Acurex - CRF November 17, 1988
Acurex ZD: 8810035
Client PO: 8327
Page 1 of €
Rev. 12/21/88
Attention: Larry Waterland
subject: Analysis of 17 sasples, Received 10/6/88.
water sasples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
The filter sample was analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Submitted by: ^ ^— Approved by:
^bambino Robert DeRosier
Inorganic Chemistry Client Services Manager
Approved by:
David R. Taylor, PhC
Quality Assurance Ml
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. Zn no event shall Acurex be liable for
special or consequential damages.
4 Ji Clyoe »»ou«. PO Bo« 70*4 Moun&m v««r. C* M039 (4i5IM'-$T00 '«'•« 3J5»ei F*x |41J>964 5>4*
99
-------
Acurex-CRF
8810035
Page 2 of 6
Rev. 12/21/86
Table l. Metals Results
Acurex-CRF Sample ID
B0914 B0914 B0914 B0914 B0914
0928 1140 1240 1340 1440
Parameter
EPA
Method
mg/L
mg/L
mg/L
mg/L
¦g/L
Arsenic
206.2
<0.01
0.07
0.11
0.14
0.18
Barium
200.7
0.45
0.31
0.3
1.6
1.6
Bismuth
0.24
0.6
1
1.3
2
Cadmium
200.7
0.02
0.05
0.07
0.1
0.16
Chromium
200.7
0. 06
0.17
0.21
0.29
0.34
Copper
200. 7
0.25
0.32
0. 34
0.42
0.46
Lead
200.7
0.031
<0.001
0.039
<0.001
<0.001
Magnesiuin
200.7
6
7.4
8.8
13
15
Strontium
0.4
0.53
0.58
0.63
0. 68
Sample volune (mL):
214
232
242
228
236
Vclune used (mL):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
NOTE: Dilution factors are
incorpora
ted in above results.
100
-------
Acurex-CRF
8810035
Page 3 of 6
Rev. 12/21/68
Table 1. Metals Results
Acurex-CRF Sample ID
E0914
£0914
E0914
E0914
F0914
0932M5
0932M5
0932M5
0932H5
0947
1-1,1-2
1-3
1-4
PW
Parameter
is FA
Method
ag/L
ag/L
ng/L
ag/L
ag/L
Arsenic
206.2
2800
0.02
<0.01
<0.01
<0.05
Bariu&
200.7
2300
<0.01
0.05
0.04
<0.05
Bismuth
10000
<0.1
<0. 1
<0.1
<0.5
Cadaiun
200.7
605
<0.01
<0.01
<0.01
<0.05
Chromium
200.7
3100
<0.01
<0.01
0.01
0.25
Copper
200.7
29000
<0.01
0.06
0.06
0.17
Lead
200. 7
3400
<0.001
<0.001
<0.001
0.014
Magnesium
200.7
4600
0.06
0.23
0. 25
<0.25
Strontium
18000
<0.01
0.05
0.02
<0.05
Sair.ple volume (nL) :
—
1096
405
270
75
Volume used (r.L) :
2
100
100
100
20
Dilution factor:
50
1
1
1
5
NCTE: Dilution factors are incorporated in above results.
101
-------
Acurex-CRF
8810035
Page 4 of 6
Rev. 12/21/88
Table 1.
Metals Results
Acurex-CRF Sample
ID
A0914
A0914
A0914
A0914
0928M17
0928M17
0928H17
0928M17
1-1,1-2
2-3
1-4
PW
Spike
EPA
Parameter
Method
mg/L
¦g/L
WJ/L
ng/L
% Recov
Arsenic
206.2
0.27
<0.01
<0.01
0.03
86
Barium
200.7
0.5
0.1
0.05
0.02
97
Bismuth
19
<0.1
<0.1
0.47
123
cadniun
200.7
0.31
<0.01
<0.01
0.91
103
Chromius
200.7
310
<0.05
0.031
2.2
97
Copper
200.7
6.8
0.08
0.07
0. 61
92
Lead
200.7
1.8
0.013
0.0086
0.21
105
Magnesium
200.7
8.5
0.21
0.2
4.2
94
Strontium
0.1
<0.01
0.02
0.06
108
Sample volume (ir.L)
:
1200
750
740
190
1096
Volume used (mL):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
NOTE: Dilution factors are incorporated in above results.
102
-------
Acurex-CRF
8810035
Page 5 of 6
Rev. 12/21/88
Table l. Metals Results
Acurex-CRF Sample ID
Method
Dup Method Detection
Spike Blank Limit
Parameter
EPA
Method
RPD
ag/L
"9/t
Arsenic
206.2
9.2
<0.01
0.01
Barium
200.7
7.6
<0.01
0.01
Bismuth
37
<0.1
0.1
Cadmium
200.7
5.2
<0.01
0.01
Chromium
200.7
6.5
0.011
0.01
Copper
200.7
7.6
<0.01
0.01
Lead
200.7
11
<0.001
0.001
Magnesiun
200.7
5.3
<0.05
0.05
Strontiur.
5.1
<0.01
0.01
Sample volume (mL):
1096
100
Volume used (mL):
100
100
Dilution factor:
1
1
NOTE: Dilution factors are incorporated in above results.
103
-------
Acurex-CRF
8810035
Pag* 6 of 6
Rev. 12/21/88
Table 2. Metals Result*
Acurex-CRT Saaple ZD
E0914
Method
0932
Dup
Method
Detection
VBi
M5F
Spike
Spike
Blank Unit
Parameter
M»trn
Method
*g/filt
t Reeov
RPD
mg/h *g/filt
Arsenic
7060
0.01
77
19
<0.01
0.005
Bariua
6010
0.01
104
3.7
0.035
0.001
Bisruth
0.49
64
16
<0.2
0.02
Cadaium
6010
0.08
93
0.44
<0.01
0.001
Chrosiua
6010
0.04
94
0.99
0.026
0. 001
Ccpper
6010
0.04
94
2.2
<0.01
0.001
Lead
6010
0.033
100
0
<0.001
0.0001
Magnesium
6010
0.4
122
13
1.3
0. 005
Strontium
0.1
104
23
<0.02
0.002
104
-------
£
ACUREX
Corporation
Environmental System* Division
Acurex - CRF December 14, 1968
Acurex ID: 8810038
Client PO: 8327
Pag* 1 of 6
Attention: Larry Waterland
Subject: Analysis of IS Samples, Received 10/10/88.
Samples B09161309 and B09161409 were broken upon arrival.
water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atonic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
The filter sample was analyzed for requested metals using Inductively
Coupled Argor Plasaa Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRcsier
at (411)961-5700.
Submitted by:
-m.
6.
MaryannlCambino
Supervisor, Inorganic Chemistry
Approved by: '
Robert DeRosier
Client Services Manager
Approved by:
David R. Taylor, Ph
Quality Assurance
ager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
4§s Cl»0« *0 Sol to**. M0UM»« v«w C* MOie l«1S>Kl'S7D0 !•»> tttM' FA» l«14l 86* S1J5
105
-------
I rex-CRF
6810038
Page 2 of 6
Table 1. Metal* Results
Acurex-CRF Sample ID
£0916
B0916 B0916 B0916 F0916 1119M5
1109 1209 1525 1120 1-1,1-2
Parameter
EPA
Method
ng/L
ng/L
ag/L
mg/L
ng/L
Arsenic
206.2
0.14
0.078
0.23
2900
<0.01
Barium
200.7
1.4
1.1
2.9
2400
0.018
Bismuth
2.5
1.1
2.4
11000
<0.1
Cadmium
200.7
0.2
0.12
0.38
540
0.013
Chromium
200.7
0.22
0.13
0.35
2900
<0.01
Copper
200. 7
1.6
1.1
1.4
30000
0.11
Lead
239.2
1.1
0.69
0.93
3000
0.052
Magnesium
2 CO. 7
18
14
17
4500
<0.05
Strontium
1.9
2.1
1.4
15000
<0.01
Sample volume (mL):
228
244
236
—
1320
volume used (r,L) :
100
100
100
2
100
Dilution factcr:
1
1
1
50
1
Chloride aliquot (r,
L) :*
—
—
—
..
100
KCTE: Dilution factors are already incorporated in above results.
* - Taken at CRF, not included in above saaple volume.
106
-------
Acurex-CCF
881003?
Page 3 of 6
Tabla 1. Metals Results
Acuiex-CRF Sample ZD
E0916
E0916
E0916
A0916
A0916
1119H5
1119M5
1119M5
1110M17
1110M17
1-3
1-4
PW
1-1,1-2
1-3
EPA
Parameter
Method
mg/L
mg/L
mg/L
mg/L
mg/L
Arsenic
206.2
0.011
<0.01
<0.05
0.11
<0.01
Barium
200.7
0.027
0.041
<0. 05
4.8
0.82
Bismuth
0.34
<0.1
<0.5
5.2
<0.1
Cadmium
200.7
0.053
0.024
<0.05
0.25
<0.01
Chromium
200.7
0.015
0.013
0.16
290
0.14
Copper
200.7
0.44
0.27
0.14
5.5
0.15
Lead
239.2
0.15
0.11
0.11
1.9
0. 019
Magnesium
200.7
0.12
0.22
<0.25
13
0.4
Strontiun
<0.01
0.02
<0. 05
0.16
0.02
370
ICO
1
NOTE: Dilution factors are already incorporated in above results.
* - Taker, at CKF, not included in above sample volume.
Sample volume (itiL) :
Volume used (r.L) :
Dilution factor:
Chloride aliquot (rr.L):*
420 184
100 100
1 1
49 1330
20 100
5 1
1
107
-------
c
Acurex-
8810036
Page 4 of 6
Table 1. Metals Results
Acur«x-CRF Staple ID
E0916
E0916
A0916
A0916
1119M5
1119M5
1110M17
1110M5
1-1,1-2
1-1,1-2
Method
PPl
1-4
PW
Spike
MSD
Blank
Parameter
m* PM
Method
ag/L
ag/L
% Recov
RPD
ng/L
Arsenic
206.2
<0.01
0.062
88
3.4
<0.01
Barium
200.7
0.13
0.012
105
2.7
<0.01
Bismuth
<0.1
4.0
98
0.97
<0.1
Cadmium
200.7
<0.01
1.5
106
2.5
<0.01
Chrorciur.
200. 7
0.078
5.2
108
2.6
<0.01
Copper
200.7
0.12
13
102
2.4
<0. 01
Lead
239.2
0.0089
1.3
116
6.4
<0.001
Magnesium
200.7
0.26
17
103
0.97
<0. 05
Strontiup.
0.02
0.03
106
3.1
<0. 01
Sawple vclurae (»L):
270
224
1320
1320
100
Voluire used (jr.L,) :
100
100
100
100
100
Dilution factor:
1
1
1
1
1
NOTE: Dilution factors are already incorporated in above results.
108
-------
Table 1. HatsIs Results
Acurex-CRF Sample ID
Method
Detection
Liait
EPA
Parameter Method mg/L
Arsenic 206.2 0.01
Bariuci 200.7 o.oi
Bismuth o.l
Cadnuuir. 200.7 0.01
Chromium 200.7 0.01
Copper 200.7 0.01
Lead 239.2 0.001
Magnesium 200.7 0.05
Strontium 0.01
109
-------
Acurex-CRF
881003o
Page 6 of 6
Table 2. Metals Results
Acurex-CRF Sample ID
E0916 Method
1125H5 Dup Method Detection
F Spike Spike Blank Limit
Parameter
EPA
Method
mg/filt
1 Recov
RPD
mg/L
»g/f i11
Arsenic
7060
0.079
70
3.6
<0.01
0.001
Barium
6010
0.019
91
1.2
0.033
0.001
Bisnuth
1.8
93
1.1
<0.1
0.01
Cadmiun
6010
0.3
91
2.5
<0.01
0. 001
Chror.ium
6010
0.086
89
0.87
0.022
0.001
Ccpper
6010
2.5
77
1.9
0.019
0. 001
Lead
6010
1.3
95
1.7
<0.05
0.005
Kagnesiur.
6010
0.69
102
4.3
1.3
0.005
Strontiur.
0.16
123
14
<0.01
0.001
110
-------
ACUREX
'£
Robert DeRosier
Client Services Manager
Approved by:
111
-------
Acurex-CRF
8810043
page 2 of 6
Rev. 12/21/8B
Table 1. Metals Results
Acurex-CRF Sanple ID
B0920
B0920
B0920
B0920
B0920
1014
1114
1214
1314
1514
EPA
Paraneter
Method
mg/L
mg/L
mg/L
mg/L
mg/L
Arsenic
206.2
<0.01
0.06
0.12
0.14
0.14
Barium
200.7
0.83
1.5
1.3
1.4
1.2
Bismuth
0.72
2.1
4.3
4.0
4.0
Cadmium
200.7
0.05
0.27
0.4
0.4
0.48
Chroaiua
200.7
0.07
0.21
0.47
0.55
2.1
copper
200.7
0.65
1.3
2.6
2.8
2.8
Lead
200.7
0.29
0.81
1.5
1.2
1.1
Magnesium
200.7
7.3
13
16
17
15
Strontium
1.0
1.4
1.4
1.2
0.92
Sair.ple volume (rnL) :
236
232
229
212
246
Volume used (it>L):
100
100
100
100
100
Dilution factor:
1
1
1
1
1
NOTE: Dilution factors are already incorporated in above data.
112
-------
Acurax-CRF
881004 3
Page 3 of 6
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF Sanple ID
E0920 £0920 E0920
B0920 F0920 1045M5 1045M5 1045M5
1558 1022 1-1,1-2 1-3 3-4
EPA
Parameter Method mg/L mg/L mg/L mg/L mg/L
Arsenic
206.2
0.11
3600
<0.01
<0.02
<0.0S
Barium
200.7
2.3
2500
0.08
0.04
0.06
Bisrcuth
2.1
11000
0.2
<0.2
<0.5
Cadmiuin
200.7
0.64
640
<0.01
<0.02
<0.05
Chrousiup.
200.7
0.42
3300
<0.01
<0.02
0.05
Copper
200.7
1.1
30000
0.88
0.12
<0.05
Lead
200.7
<0.001
3500
0.02
0.036
0.031
Magnesium
200.7
13
4900
0.93
0.26
0.36
Strontium
1.0
19000
0.06
<0.02
<0.05
Sanple volune (r.L) : 232 —
Volume used (itL) : 100 2
Dilution factor: 1 50
Chloride aliquot* (mL):
NOTE: Dilution factors are already incorporated in above data.
* - Aliquot taken at CRF, not included in sample volume listd above.
1360
139
102
100
50
20
1
2
5
100
—
113
-------
Acurex-CRF
881004 3
Page 4 of 6
Rev. 12/21/88
Table 1.
Metals Results
Acurex-CRF
Sample
ID
EPA
Method
E0920
104SMS
PW
A0920
1014M17
1-1,1-2
A0920
1014H17
1-3
A0920
1014M17
1-4
A0920
1014M17
PW
Parameter
mg/L
*g/L
¦g/L
ng/L
mg/L
Arsenic
Barium
Bismuth
Cadmium
Chromium
Copper
Lead
Magnesium
Strontium
206.2
200.7
200.7
200.7
200. 7
200. 7
200. 7
<0.05
<0.05
<0.5
<0.05
0.06
<0.05
0.016
<0.25
<0.05
0.18
4.9
16
0.7
1500
17
6.4
14
0.16
0.02
0.81
2.1
0.13
0.24
0.71
0.31
0. 36
0.03
0.02
2.4
2.7
0.14
4.1
0.93
0.46
0.69
0.05
2.1
0.4
8.2
4.0
140
42
8.2
150
1.1
Sar.ple
volune (nL):
76
1380
455
475
90
Volune used (nL):
20
100
100
100
20
Dil
utior. factor:
5
1
1
1
5
Chloride a
liquot* (nL):
—
2
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Aliquot taken at CRT, not included in sample volume listd above.
114
-------
Acurex-CRF
8810043
Page 5 of 6
Rev. 12/21/88
Table 1. Metals Results
Acurex-CRF Sample ZD
E0920
£0920 1045K5
1045M5 1-1,1-2 Method
1-1,1-2 Dup Method Detection
Spike Spike Blank Liait
Parameter
EPA
Method
1 Recov
RPD
ag/L
ug/L
Arsenic
206.2
89
9.3
<0.01
0.01
Barium
200.7
93
4.2
<0.01
0.01
Bismuth
84
7.4
<0.1
0.1
Cadmium
200.7
101
2.9
<0.01
0. 01
Chromium
200. 7
97
3.9
<0.01
0.01
Copper
200.7
83
2.9
<0.01
0.01
Lead
200.7
109
5.1
<0.001
0.001
Magnesium
200.7
91
2.8
<0.05
0.05
Strontium
107
2.6
<0.01
0.01
Sample
volume (mL) :
1360
1360
100
Volume used (mL! :
100
100
100
Dilution factor:
1
1
1
KCTE: Dilution factors are already incorporated in above data.
115
-------
Aeure::-CRF
BB10043
Page 6 of 6
Rev. 12/21/88
Table 2. Metals Results
Acurex-CRF Sample ID
E0920 Method
1045 Dup Method Detection
M5F Spike Spike Blank Limit
Parameter
EPA
Method
mg/filt
* Recov
RPD
mg/L
¦g/filt
Arsenic
7060
0.02
70
3.6
<0.01
0.005
Barium
6010
0.01
91
1.2
0.033
0.001
Bismuth
0.8
93
1.1
<0.1
0.01
Cadmium
6010
0.13
91
2.5
<0.01
0.001
Chromium
6010
0.04
89
0.87
0.022
0.001
Copper
6010
0.99
77
1.9
0.019
0.001
Lead
6010
0.49
95
1.7
<0.05
0.005
Magnesium
6010
0.42
102
4.3
1.3
0.005
Strontium
0.1
123
14
0.29
0.001
116
-------
ACUREX
'
-------
Acurex-Ci1
881004 8
Page 2 of 6
Table 1. Metals Results
Acurex-CRF Sample ID
Parameter
EPA
Method
B0922
0942
B0922
1042
B0922
1142
B0922
1242
B0922
1343
nig/L
ng/L
ng/L
mg/L
mg/L
Arsenic
206.
2
0.015
0.1
0.11
0.13
0.15
Barium
200.
7
0.B
1.3
1.4
1.4
1.1
Bismuth
1.3
4.8
5. B
5.2
6.0
Cadmium
200.
7
0.096
0.35
0.35
0.4
0.42
Chromium
200.
7
0.14
0.43
0.56
0.65
0.73
Copper
200.
7
1.1
3 . 3
4.5
4.6
5.0
Lead
239.
2
0.75
1.5
1.9
1.9
1.8
Magnesium
200.
7
7.8
14
18
17
15
Strontium
1.2
1.5
1.6
1.6
1.2
Sample volume (mL):
234
206
216
238
228
volume used ,'r.L) :
100
100
100
100
100
Dilution factor:
1
1
1
1
1
NOTE: Dilution factors are already incorporated in above data.
118
-------
c Acurex-CRF
eei:c48
page 3 of 6
Table l. Metals Results
Aculjx-CRF Sample ID
E0922
E0922
E0922
E0922
F0922
0950 M5
0950 M5
0950 M5
0950 M5
Pft*
1050
1-1,1-2
1-3
1-4
PW
Parameter
£rA
Method
mg/L
*g/L
n>9/l
ag/L
ag/L
Arsenic
206.2
3300
<0.01
<0.01
<0.01
<0.05
Barium
200.7
2300
0.015
0.041
0.046
<0.05
Biscuth
11000
<0.1
<0.1
0.15
<0.5
cadmium
200.7
540
<0.01
<0.01
<0.01
<0.05
Chromium
200.7
2900
<0.01
<0.01
<0.01
0.084
Copper
200.7
30000
<0.01
0.023
0. 044
0.2
Lead
239.2
3000
0.0061
0.0026
0.007
0.046
Magnesium
200. 7
4300
<0. 05
0.26
0.64
0.43
Strontium
17000
<0.01
<0.01
0.06
<0.05
Sample volume (nL):
—
1025
335
248
53
Volume used (ir.L) :
2
100
100
100
20
Dilution factor:
50
1
1
1
5
Chloride aliquot (mL):»
—
100
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Taken at CRT, not included in above sample volume.
119
-------
Ac ~F
88i.00-i
Page 4 of 6
Table l. Metals Results
Acurex-CRF Sample ID
EPA
Method
A0922
0942 Ml7
1-1,1-2
A0922
0942 M17
1-3
A0922
0942 M17
1-4
A0922
0942 M17
PW
Spike
Parameter
*g/L
ng/L
ng/L
mg/L
% Reeov
Arsenic
Barium
Bismuth
Cadmium
Chromium
Copper
Lead
Magnesiun
Strontiuia
206.2
200.7
200.7
200.7
200.7
239.2
200.7
0.55
3.0
19
0.75
740
21
6.4
7.4
0.08
<0.01
1.2
0.15
<0.01
0.7
0.17
0.011
1.6
0.15
<0.01
0.15
<0.1
<0.01
0.25
0.12
0.0081
1.2
0.1
0.65
<0.05
2.0
3.4
3.4
49
6.2
14
<0.05
94
96
114
98
9B
95
100
97
117
Sample volume (»L
* .
1100
410
530
212
1025
Vcluse used (r,L) :
100
100
100
20
100
Dilution factor:
1
1
1
5
1
Chloride aliquot
fml.) : *
100
—
—
—
—
NOTE: Dilution factors are already incorporated in above data.
* - Taken at CRF, not included in above sample volume.
120
-------
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Dup Method Detection
Spike Blank Limit
EPA
Parameter
Method
RPD
ng/L
mg/L
Arsenic
206.2
5.3
<0.01
0.01
Barium
200.7
3.9
<0.01
0.01
Bismuth
13
<0.1
0.1
Cadmium
200.7
4.3
<0.01
0.01
Chromium
200.7
2.9
<0.01
0.01
Copper
20C.7
4.0
<0.01
0.01
Lead
239.2
3.4
<0.001
0.01
Magnesium
2 CO. 7
2.2
<0.05
0.05
Strontiur.
6.3
<0.01
0.01
Sample volume (ir.L) :
1025
100
Volume used (mL):
100
100
Dilution factor:
1
1
NOTE: Dilution factors are already incorporated in above data.
121
-------
.-2>-CPr
6 B1004 o
Page 6 of
Table 2. Metals Results
Acurex-CRF Sample ID
£0922 Method
0930 Oup Method Detection
M5F Spike Spike Blank Limit
Parameter
EPA
Method
mg/filt
% Recov
RPD
ng/L
ng/filt
Arsenic
7060
0.055
70
3.6
<0.01
0.001
Bariun
6010
0.012
91
1.2
0.033
0.001
Bismuth
2.4
93
1.1
<0.1
0.01
Cadmium
6010
0.33
91
2.S
<0.01
0.001
Chromium
6010
0.087
89
0.87
0.022
0.001
Copper
6010
5.2
77
1.9
0.019
0.001
Lead
6010
2.0
95
1.7
<0.05
0. 005
Magnesium
6010
0.73
102
4.3
1.3
0. 005
Strontium
0. 085
123
14
0.29
0. 001
122
-------
^ ACUREX
A Corporation
Environmental Systems Division
Acurex-CRF November 21, 1988
Acurex ID: 8810052
Client PO: 8327
Page 1 of 6
Attention: Larry Waterland
Subject: Analysis of 13 Hater and 1 Filter Sample, Received 10/14/88.
water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
The filter sample was analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosier
at^(415)961-5700.
Submitted by: Approved by:
Robert DeRosier
Client Services Manager
Approved
Manager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
445 Cryd* Av»nu«. PO Bo* Mountain Vi»w. CA 9*039 t*i3i ®6*-5?00 T»i*i 325ft€i FAX I*1ftift64-514£
123
-------
Acurex
8B10052
Pag* 2 of €
Table 1.
Metals Results
Acurex-CRF Sample ZD
EPA
Parameter Method
B0926
1039
B0926
1139
B0926
1239
B0926
1330
F0926
1053
mg/L
mg/L
ag/L
mg/L
mg/L
Chromium 200.7
0.56
0.40
l.l
1.3
3200
Sample volume (ml):
156
142
156
160
139
Volume used (nL)
100
100
100
100
50
Dilution factor:
1
1
1
1
2
Chloride aliquot* (r,L) :
—
—
—
—
—
NOTE: Dilution factors are already
incorporated
in above
data.
• - Aliquot taken at CRF. Not included in above sample volume.
124
-------
Acurex
8810052
Page 3 of 6
Table 1. Metals Results
Aeurex-CRF Sample ID
£0926 E0926 E0926 E0926 A0926
1047 1047 1047 1047 1039
K5T1-I1 M5T1-I2 H5T1-I3 HStl-PW M5T1-I1
Parameter Method mg/L sg/L mg/L >?/L ag/L
Chromium 200.7
0.02
0.03
0.04
1
1
o t
• «
H |
1
1
0.13
Sample volume (ml):
520
335
290
74
87
Volume used (mL):
100
100
100
20
20
Dilution factor:
1
1
1
5
5
Chloride aliquot* (ml,):
50
50
50
—
50
NOTE: Diiutior. factors are already incorporated in above data.
* - Aliquot taken at CRT. Not included in above sample volume.
125
-------
Acur?
8810052
Page 4 of 6
Table 1. Metals Results
Acurax-CRF Sample ID
E0926 £0926
A0926 A0926 A0926 1047 1047
1039 1039 1039 K5T1-I1 M5T1-I1
M5T1-I2 M5T1-I3 K5T1-FW Spike MSD
EPA
Parameter Method
mg/L
»g/L
ng/L %
» 1
• 1
O 1
Q 1
< i
i
i i
RPD
Chromium 200.7
0.1
1.7
0.07
98
1.6
Sample volume
-------
Acurex
6810052
Page 5 of 6
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Method Detection
Blank Limit
Parameter Method mg/L mg/L
Chromium 200.7 <0.01 0.01
Sample volume (mL): 100
Volume used (mL): 100
Dilution factor: 1
NOTE: Dilution factors are already incorporated in above data.
127
-------
Acurex
8810052
Page 6 Of 6
Table 2. Metals Results
Acurex-CRF Sample 2D
£0926 Method
1047 Pup Method Detection
K5T1F Spike Spike Blank Limit
Parameter Method ng/filt % Recov RJ>D ag/L asg/filt
Chromium 6010 0.11 91 0.8? <0.01 0.1
128
-------
A acurex
Corporation
Environmental Systems Division
Acurex - CRF December 15, 1988
Acurex ID: 88100S6
Client PO: 6327
Page 2 of €
Attention: Larry Waterland
subject: Analysis of 13 water and l Filter Sample. Received 10/1*7/88.
water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
The filter sample was analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid waste. The EPA method
er.ployed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosie:
at (415)961-5700.
Submitted by: ^ f Approved by:
Maryann bambino 1— j£^Robert
Super\r/tspr, Inorganic Chemistry
Approved by
David R. Taylor, Pi
Quality Assurance fainager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
«85C>yecA»*nu«.PO Ba> 7(W4 MsumamVK.CA M03( (41MM1-S700 32SW r*x <415) 9fr«
129
-------
Acurex-CRF
8810056
Page 2 of 6
Table l. Metals Results
Acurex-CRF Sample ID
B0928 B0928 B092S B0928 F0928
0931 1031 1131 1228 0949
EPA
Parameter Method
mg/L
ag/L
ag/L
ag/L
ag/L
Chromium 200.7
0.13
0.32
0.39
0.41
3100
Sanple volume (nL) :
146
142
136
142
138
Volume used (ir.L) :
100
100
50
100
50
Dilution factor:
1
1
2
1
2
NOTE: Dilution factors are
already
incorporated
in above
data.
130
-------
Acurex-CRF
8810056
Page 3 of 6
Table 2. Metals Results
Acurex-CRF Sample 2D
E0928 £0928 E0928 E0928 A0928
0940 0940 0940 0940 0931
M5T1(I-1)M5T1(1-2)HST1(1-3) M5T1PW M3T1(I-1)
Parameter
EPA
Method
mg/l
ag/L
¦g /i»
ag/L
ag/L
Chromium
200.7
0.05
0.015
0.015
<0.05
0.04
Sanple volume (mL):
880
400
365
50
110
Volume used (nL):
100
100
10C
20
50
Dilution factor:
1
1
1
5
2
NOTE: Diluticr. factors are already incorporated in above data.
131
-------
A^urex-CRF
6810056
Page 4 of 6
Table 1.
Hetals Results
Acurex-CRF Sample
ID
EPA
Kethod
A0928 A0928
0931 0931
M5T1(I-2)M5T1(1-3)
A0928
0931
M5T1PW
Spike
Cup
Spike
Parameter
mg/L
JSf/L
mg/L
1 Recov
RPD
Chromium
200.7
0.053
0.069
<0.05
101
0.19
Sample volume (mL)
.
13 C
110
42
880
880
Vcluae used (r.L) :
50
50
20
100
100
Dilation factor:
2
2
5
1
1
NOTE; Dilution factors are already incorporated in above data.
132
-------
Acurex-CK;
8810056
Page 5 of 6
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Method Detection
Blank Limit
Parameter Method ng/h ug/L
ChroKiuio 200.7 <0.01 0.01
Sample volume (mL): 100
Vcluir.e used (wL) : 100
Dilution factor: 1
NOTE: Dilution factors are already incorporated in above data.
133
-------
Ac-^e!. * "
8P1. J56
Page 6 of 6
Table 2. Metals Results
Atarex-CRF Sample ID
£0928 Method
0f40 Dup Mathoi Detection
H5T1F Spike Spike Blank Limit
Parameter Method mf/filt * Recov MPD ag/L ag/filt
Chromium 6010 0.0S1 89 0.8? <0.01 0.1
134
-------
/S ACUREX
Corporation
Environmental Systems Division
Acurex - CRF December 15, 19B8
Acurex ID: 6810057
Client PO: 8327
Page 1 of 6
Attention: Larry Waterland
subject: Analysis of 13 water and l Filter sample, Received 10/17/88.
water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table 1.
The filter sample was analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
Submitted bv: ^ 1 ( ' y' ' <1 ^ ^Approved by: P&L-&
Maryann bambino Robert DeRosier
Superv^s6r, Inorganic Chemistry Client Services Manager
T-
Approved by
David R. Taylor,
Quality Assurance
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
ClyO* AMnu* PO Boi 7044.Moufitw V«*C* K03B (4i5iM< S700 Tmi 325961 Ms |
-------
' v'.:-C3F
88100i>7
Page 2 of 6
Table 1. Metals Results
Acurex-CRF Sample ZD
B0929 B0929 B0929 B0929 F0929
0907 1007 1107 1158 0929
EPA
Parameter Method
mg/L
mg/L
ag/L
ag/L
mg/L
Chroir.iura 200,7
0.11
0.19
0.37
0.44
3000
Sanple volume (mL):
146
138
144
154
128
Volur.e used (r.L) :
100
100
100
100
50
Dilution factor:
1
1
1
1
2
NOTE: Dilution factors are
already
incorporated
in above
data
136
-------
Acure>-CRF
881005 <
Page 3 of 6
Table 1- Metals Results
Acurex-CRF Sample ID
£0929 E0929 E0929 A0929 A0929
0920 0920 0920 090? 0907
M5Tl(I-l)M5Tl(I-2)MSTl(I-3) M5T1PW M5T1(I-1)
EPA
Parameter Method »g/L ng/L ng/L mq/L mg/L
Chromiuri 200.7 0.025 0.013 0.023 <0.1 0.061
134
100
1
NOTE: Dilution factors are already incorporated in above data
Sample volurae (&L!: 910 410 400 34
Vcluse used (nL): 10C 100 100 10
Dilution factor: 1 1 1 10
137
-------
Acurex-CRF
8810057
Page 4 of 6
Table 1. Metals Results
Acurex-CRF Sa»ple ID
A0929 A0929 A0929
0907 0907 0907 Dup
M5T1(l-2)M5Tl(I-3) M5T1PW Spike Spike
EPA
Parameter Method
mg/L
ng/L
»g/L %
Recov
RPD
Chromium 200.7
0.1
0.095
<0.5
105
1.9
Sair.ple volur.e (r.L) :
126
100
10
910
910
Volune used (rL):
50
50
2
100
100
Dilution factor:
2
2
50
1
1
NOTE: Dilution factors are
already
incorporated
in above
data
138
-------
Acurex-CRF
B810057
Page 5 of 6
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Method Detection
Blank Limit
Parameter Method ag/L ng/L
Chromium 200.7 <0.01 0.01
Sample volume (roL): 100
Vclur.e used (ir.I) : 100
Dilution factor: 1
NOTE: Dilution factors are already incorporated in above data
139
-------
Acurev-CRF
8810057
Page 6 of 6
Table 2. Metals Results
Acurex-CHF Sample ID
E0929 Method
0920 Dup Method Detection
M5T1F SpiXe Spike Blank Limit
Parameter Method ng/filt % Jtecov RPD ng/L mg/filt
Chronium 6010 0.045 89 0.87 <0.01 0.1
140
-------
ACUREX
Corporation
Environmental Systems Division
Acurex - CRF December 15, 1988
Acurex ID: 8810058
Client PO: 8327
Page 1 of 2
Attention: Larry Waterland
Subject: Analysis of 1 Soil Sample, Received 10/17/88.
This sample was received as a replacement for the one on
traveller 8810013 that arrived broken.
Soil samples were analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sar.ple in acid prior to
analysis. The results are presented in Table 1.
If you should have any technical questions, please contact Robert DeRosie:
at (415)961-5700.
Submitted by: I^ jCpproved by:
Maryanh (iambino Robert DeRosier
Superv^edjr, Inorganic Chemistry client Services Manager
Approved bv: iJ>o. ]
David R. Taylor,
Quality Assuranc
These results were obtained by following standard laboratory
procedures; the liability of Acurex corporation shall not exceed the
amount paid for tbis report. Zn no event shall Acurex be liable for
special or consequential damages.
4B5 Ofd* Annua. PO.Boi 7044. Mount»«V»w CA M03S (416)061-5700 T»». 3J5»«i F»X (4iS> 964H4S
141
-------
Acurex-CRF
8610058
Page 2 of 2
Table 1. Metals Results
Acurex-CRF Sample ID
Method
T0830 Dup Method Detection
1450 Spike Spike Hank Lialt
Parameter
EPA
Method
»f/kf %
Recov
RFC
»g/L
Bf/kg
Arsenic
7060
16
124
18
<0.01
1
Barium
6010
42
111
6.9
<0.01
1
Bisauth
23
91
3.6
<0.1
10
cadniur
6010
<1
98
9.1
<0. 01
1
Chroniun
6010
79
115
11
<0.01
1
Copper
6010
220
91
18
<0.01
1
Lead
"420
7
117
11
<0.001
0.1
Magrsesiun
6310
28000
100
3.4
<0.05
5
Strontiun
160
104
20
<0.01
1
142
-------
/*v ACUREX
T"' Corporation
Environmental Systems Division
Acurex-CRF
December 15, 1988
Acurex ID: 8810079
Client PO: 8327
Page 1 of 5
Attention: Larry Waterland
Subject: Analysis of 2 Soil and 3 Filter Samples, Received 10/27/88.
Soil samples vere analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Haste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 1.
The filter samples were analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 2.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential danages.
Chenistry
Approved by:>£^>
Client Services Manager
485 C*yat A««nue PO Boi 7044. Mourimi Vhw CA M03» (41S)M1-S70C IMi 125961 FAX (
-------
Acurex-CRF
8610079
Page 2 of 5
Table 1. Metals Results
Acurex-CRF Saaple ID
AOS 2 5
A0920
1200
1014
Dup
Spike
Method
M17
THETA
Spike
Blank
EPA
Parameter
Method
ng/kg
¦g/kg
% Recov
RPD
mg/h
Arsenic
7060
26
330
109
25
<0.01
Bariun
60X0
28
<10
107
2.7
<0.01
Bismuth
520
300
112
10
<0.1
cadmium
6010
73
700
10S
5.5
<0.01
Chroniuir,
6C10
42000
720
102
29
<0.01
Copper
6C10
410
5100
132
22
<0.01
Lead
7421
270
880
125
4 .1
0.0014
Kagnesiun
6010
2200
3000
106
3.2
<0.05
Strontiua
<10
20
108
3.7
<0.01
144
-------
*rurex-CRF
o810079
Page 3 o£ 5
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Detection
Limit
EPA
--------
Parameter
Method
mg/kg
Arsenic
7060
l
Barium
6010
l
Bismuth
10
Cadmium
6010
l
Chromium
6010
l
Copper
6010
l
Lead
7421
l
Magnesium
6010
5
Strontium
1
145
-------
Acurt •CRF
8610079
Page 4 of 5
Table 2. Metals Results
Acurex-CRF Sample ID
A0926 A0928 A0929
1039 0931 0907 Dup
M5F M5F M5F Spike Spike
Parameter Method »g/filt ng/filt ng/filt % Recov % RPD
Chronium 6010 0.047 0.039 0.01 89 0.87
146
-------
AC-r< CRF
8B10C""»
Page 5 of 5
Table 2. Metals Results
Acurex-CRF Sample ID
Method
Method Detection
Blank Limit
EPA ——— ———
Parameter Method mg/L mg/filt
Chroiriun 6010 0.022 0.001
147
-------
/N ACUREX
'T^ Corporation
Environmental Systems Division
Acurex - CRF December 15, 1988
Acurex ID: 8811023
Client PO: 83Z7
Page 1 of 4
Attention: Larry waterland
Subject: Analysis of 11 soil Samples, Received 11/4/88.
Soil samples were analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table l.
If you should have any technical questions, please contact Robert DeRosier
at (415)961-5700.
V A-i/ /C " ¦
Submitted by: (¦¦'{ Approved by: ~
Maryanji-'Gambino Robert DeRosier
Supervisor, Inorganic Chemistry Client Services Manager
Approved by
David R. Taylor, EH1D.
Quality Assurance-Manager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
««S Ciyda *0 Bw 7044. Mountain v»w CA S403S t«1S) MVB700 Talai 12BM1 »*s |«1J< M SKS
148
-------
Acurf"-CR"
8811023
Page 2 of 4
Table 1. Metal6 Results
Acurex-CRF Sample 10
Paraneter
EPA
Method
F1103
0924
ag/kg
71103
0927
ag/kg
F1103
0929
ag/kg
F1103
0932
ag/kg
F1103
0933
ag/kg
Bismuth
12
KA
NA
NA
NA
Chromium
6010
55
51
S3
54
S5
Lead
7421
3.7
2.B
2.9
3.1
2.3
Magnesiuts
6010
23000
21000
22000
22000
22000
Strontium
37
34
32
33
30
N'A - Not analyzed
149
-------
Acurex-cr.
8811023
Page 3 of
Table 1. Metals Results
Acurex-CRF Sample ID
Parameter
EPA
Method
F1103
F1103
F1103
rno3
F1103
0934
0937
0939
0941
0943
ag/kg
ng/kg
«g/kg
»g/l«g
ssg/kg
NA
NA
NA
NA
NA
55
54
50
50
52
3.2
3.5
3.0
2.5
NA
23000
22000
20000
22000
NA
33
36
33
35
NA
Bismuth
Chromium
Lead
Magnesium
Strontium
6010
7421
6010
NA - Hot analyzed
150
-------
Table 1. Metals Results
Acurex-CRF Sample ID
Acurex-CRF
8811023
Pag* 4 of 4
Parameter
EPA
Method
Method
F1103 Dup Method Detection
0945 Spike SpiXe Blank Limit
mg/kg t Recov RPD ag/L »g/kg
Bismuth
NA
86
12
<0.1
10
Chromium
6010
54
94
2
<0.01
1
Lead
7421
NA
118
3.4
0.0032
0.1
Magnesium
6010
NA
102
0.042
<0.05
5
Strontium
NA
105
2.8
<0.01
1
NA - Not analyzed
151
-------
/* ACUREX
'T' Corporation
Environmental Systems Division
Acurex - CRF December 20, 198 8
' Acurex ID: 8812009
Client PO: 8327
Page 1 of 4
Attention: Larry Waterland
Subject: Analysis of 1 Solid Sample, Received 12/2/88.
water samples were analyzed for requested metals using inductively
coupled argon plasma spectroscopy or atomic absorption spectroscopy
following methods for chemical analysis of water and wastes. The EPA
method employed is listed alongside of the parameter. Samples were
digested according to EPA protocol prior to analysis. The results are
presented in Table l.
If you should have any technical questions, please contact Robert DePosie:
at (415)961-5700.
Submitted by: /A !o... Approved by: *¦ //-A-,
Maryjusn Gambino Robert DeRosier
Supervisor, Inorganic Chemistry Client Services Manager
Approved by
David R, Taylor,
Quality Assurancfettanager
These results were obtained by following standard laboratory
procedures; the liability of Acurex corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
Clyo* *«nu«. P.o Bo< rou. Mountain vm CA M039 <»iSl®«vJ700 1a»» M5»6i FAX (415)964 5145
152
-------
Acurex-CRF
8812009
Page 2 of 4
Parameter
Chroniua (hex.)
Table 1. Metals Results
Acurex CRT Sample ZD
EPA
Method
Q1130
STANDARD
8806
Q0929
Q0929
012S0
CR03
096-2
0830
0831
FBK *0.2 PPM
RE-RUN
FSK
FSK
ag/L ag/L
ag/L
ag/L
ag/L
0.57
0.22
0.89
2.7
3.1
218.4
Sample Volume (siL) :
Voluae used (r.L) :
Dilution factor:
Sair.ple weight (g) :
400
50
2
100
100
1
400
20
5
100
400
20
5
100
KCTE: Dilution factors are already incorporated in above data.
153
-------
Acurex-CRF
B812009
Page 3 of 4
Table l.
Metals Results
Acurex CRF Sasp1¦ ID
EPA
Parameter Method
Q0929
1030
BSX
T0929
0906
Q0929
1400
TSK
SpDce
Dup
Spike
mg/L
¦9/L
mg/L
% Spike
RPD
Chroniua (hex.} 218.4
0.49
3100
2.3
75
7.3
Sample Volune (bL):
50
115
400
400
400
Volume used (mL):
25
--
20
50
50
Dilution factor:
4
5000
5
2
2
Sair.ple weight (g) :
—
—
100
100
100
NOTE: Dilution factors are already incorporated in above data.
154
-------
Acu.JX-CRF
8811009
Page 4 Of 4
Table 1. Metals Results
Acurex CRF Sample ID
2nd CR+6 Method
Method STANDARD Detection
Blank §0.2 PPM Liait
Parameter Method ag/L ag/L ag/L
Chromium (hex.) 218.4 <0.003 0.2 0.003
Sample Volume (mL): 100
Voluse used (bL): 100
Dilution factor: l
Sample weight (g): —
NOTE: Dilution factors are already incorporated in above data.
155
-------
jT\ ACUREX
"Coroorati
Corporation
Environmental Systems Division
Acurex - CRF
January 26, 1939
Acurex ZD: 8612065
Client PO: 8327
Page 1 of 7
Attention: Larry Katerland
Subject: Analysis of 24 Trace Hetal Staples, Received 12/13/88.
Samples were analyzed for requested metals using Inductively
Coupled Argon Plasma Spectroscopy or atomic absorption spectrometry
following Test Methods for Evaluating Solid Haste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 3050 by digesting the sample in acid prior to
analysis. The results are presented in Table 1.
If you should have any technical questions, please contact Robert DeRos:er-
st (415)961-5700.
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. Zn no event shall Acurex be liable for
special or consequential damages.
Submitted
Approved b
Approved bv; J ~ <
Robert DeRosier
Client Services Manager
Clyto Mnui, *0 Bei 70*4 Mountain V»w CA »403» (413) 961-5700 1M»< 32S96' FAX |4i$i »64-5i45
156
-------
Acurex- "
681206-
Page 2 of 7
Table l. Metals Results
Acurex-CRF Sample ZD
A0830 A0830 A0830 A0830 A0907
1114 1114 1114 1114 1129
1-1BF 1-17P 1-16F l-14F,etc 2-18F
Parameter
EPA
Method
...
ag
ag
og
ng
mg
Arsenic
7060
0.
0013
0.011
0.027
0.044
<0.001
Barium
6010
<0
.001
0.0014
0.0022
0.0046
<0.001
Bismuth
0
.038
<0.01
<0.01
0.024
<0.01
Cadmium
6010
0.
0017
0.016
0.035
0.068
<0.001
Chromium
6010
0.
0099
0.069
0.18
0.31
0.002
Copper
6010
0.03
0.19
0.39
0.86
0.0075
Lead
7421
0.
0025
0.017
0.033
0.075
0. 0C1
Magnesium
6010
0
.081
0.34
0.79
1.4
0.012
Strontium
<0
.001
<0.001
0.003
0. 006
<0.0C1
Sample
Used (g) :
All
All
All
All
All
157
-------
Acurex-CRF
8812065
Page 3 of 7
Table 1. Metals Results
Acurex-CRF Sample ZD
A0907
A0907
A0907
A0909
A0909
1129
1129
1129
1122
1122
2-17F
2-16F
2-14F,«tC
3-18F
3-17F
Paraaeter
LrA
Method
ng
ng
ng
mg
Arsenic
7060
0.0013
0.038
0.024
0.0021
0.051
Barium
6010
<0.001
0.0028
0.0027
0.02
0.0047
Bismuth
0.024
<0.01
<0.01
<0.01
0.032
Cadmium
6010
0.0037
0.079
0.05
0.0056
0.16
Chroaium
6010
0.012
0.24
0.18
0.0074
0. 089
Copper
6010
0.042
0.94
0.77
0.093
1.4
Lead
7421
0.0071
0.21
0.12
0.018
0.57
Magnesium
6010
0.056
1.2
0.89
0.24
2.5
Strontiun
<0.001
0.003
0.003
<0.001
0. 005
Sample
Used (g) :
All
All
All
All
All
158
-------
j -CRF
Page 4 of 7
Table l. Metals Results
Acurex-CR>
Sample
ID
A0909
A0909
A0914
A0914
A0914
1122
1122
0928
0928
0928
3-16F 3
-14F,etc
4
-18F
4-17F
4-16F
Parameter
£rn
Method
mg
*g
*g
*g
mg
Arsenic
7060
0.033
0.021
<0
.001
<0.001
0.0092
Barium
6010
0.0033
0.0061
<0
.001
<0.001
0.0013
Bismuth
0.016
0.055
<0.01
<0.01
0.23
Cadmium
6010
0.11
0.055
<0
.001
<0.001
0.022
Chromiua
6010
0.052
0.073
<0
.001
<0.001
0.02
Copper
6010
0.9
0.63
0.
0062
0.0048
0.057
Lead
7421
0.3
0.16
0.
0002
0.0008
0. 021
Magnesium
6010
2.0
4.4
<0
.005
0.014
C. 36
Strontium
0.003
0.015
<0
.001
<0.001
<0.001
Sanple
Used (g):
0.1
All
All
All
All
159
-------
•^urex-CRF
9812.265
Page 5 of 7
Table 1. Metals Results
Acurex-CRT sample 1J
A0914
A0916
A0916
A0916
A0916
0928
1110
1110
1110
1110
4-14F,etc
5-1BF
5-17F
5-16F
5-14F,etc
Paraneter
LfA
Method
¦g
ng
ag
¦g
n*g
Arsenic
7060
0.0087
0.0011
0.024
0.17
0.076
Sariuo
6010
0.0016
<0.001
0.0016
0.0053
0.0064
Bismuth
0.21
<0.01
0.022
0.1
0.3
Cadaiua
6010
0.019
0.0022
0.052
0.37
0.18
Chromium
6010
0.084
0.005
0.044
0.18
0.5
Copper
6010
0.15
0.025
0.42
2.8
1.6
be&d
7421
0.023
0.005
0.13
0.87
0.42
Kagnesiui
6010
C.49
0.058
0.42
2.5
3.7
Strontiuir,
<0.001
<0.001
<0.001
O.OOB
C. 017
Sarcple
Used (g):
All
All
All
All
All
160
-------
»'.ur V--
8812u65
Page 6 of 7
Table 1. Metals Results
Acurex-CRF Sanple ZD
A0922 A0922 A0922 A0922
0942 0942 0942 0942
6-18F 6-17r 6-16F 6-14F,«tC SpiXe
Paraaetar
EPA
Method
Bg
¦g
ng
ag %
Recov
Arsenic
7060
<0.001
0.01
0.063
0.03
105
Barius
6010
<0.001
0.0011
0.0034
0.0038
100
Bismuth
<0.01
0.02
0.046
0.09
92
Cadaium
6010
0.0032
0.042
0.21
0.081
110
ChroEium
6010
0.004S
0.035
0.16
0.31
105
Copper
6010
0.052
0.6
3.3
1.2
92
Lead
7421
0.014
0.22
1.1
0.37
ioe
Magnesiua
6010
0.054
0.29
1.4
1.1
81
Strontium
<0.001
<0.001
0.003
0.004
97
Sample
Used (g):
All
All
All
All
0.1
161
-------
Acurex-Co
8812065
Page 7 of 7
Table 1. Metals Results
Acurex-CRF Sample ID
Method
Method Detection
Spike Blank Limit
Parameter
EPA
Method
RPD
mg/L
¦g/kg
Arsenic
7060
S.6
<0.01
1
Barium
eoio
3.7
<0.01
1
Bismuth
22
<0.1
10
Cadmium
6010
3.9
<0.01
1
Chromium
6010
6.0
<0.01
1
Copper
6010
4.1
<0.01
1
Lead
7421
3.5
<0.001
0.1
Magnesium
6010
9.7
<0.05
5
Strontium
3.0
<0.01
1
Sample
Used (g):
0.1
_ —
162
-------
£\ ACUREX
Corporation
Environmental Systems Division
Acurex - CRF January 26, 1989
Acurex ID: 8901023
Client PO: 8327
Page 1 of 2
Attention: Larry Waterland
Subject: Analysis of 1 Soil Sanple, Received 1/11/89.
The soil saaple was analyzed for requested metals using Inductively-
Coupled Argon Plasma Spectroscopy or atonic absorption spectrometry
following Test Methods for Evaluating Solid Waste. The EPA method
employed is listed alongside of the parameter. Samples were prepared
using EPA method 30SO by digesting the sample in acid prior to
analysis. The results are presented in Table 1.
If you should have any technical questions, please contact Robert DeRosier
at (413)961-5700.
Submitted by; j - Approved by: •—"
Maryana-^Janbino Robert-'DeRosier
Supervisor, Inorganic Cheaistry Client Services Manage:
jc«L«ar
Approved by:
David R. Taylor, .Pf-D.
Quality AssurancdLtlanager
These results were obtained by following standard laboratory
procedures; the liability of Acurex Corporation shall not exceed the
amount paid for this report. In no event shall Acurex be liable for
special or consequential damages.
4a5ClyO>«Mftu«.P.C few 70*4. Mountain Vc.C* MMB (41S)861-S'00 IMu USM1 FAX: («1S> B64 SUS
163
-------
Acurex-CFF
8901023
Page 2 of 2
Table 1. Metals Results
Acurex-CRF Saaple ID
10916
Method
1625
Dup
Method
Detection
1PPA
(RV 43)
Spike
Spike
Blank Limit
Paraoeter
Method
Bg/kg
% Recov
RPD
ng/L ng/kg
Arsenic
7060
17
117
19
<0.01
1
Barium
6010
47
BO
2.1
<0.01
1
Bismuth
16
101
27
<0.1
10
caditiua
6010
<1
93
0.32
<0.01
1
Chrociua
6010
85
90
3.1
<0.01
1
Copper
6010
280
72
1.3
0.026
1
Lead
7420
3.8
104
1.6
<0.001
0.1
Magnesium.
6010
28000
84
7.3
<0.05
5
Strontiur
170
72
4.3
<0.01
1
sar.ple
Used (g) :
1.0
1.0
1.0
164
-------
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pa.
-------
APPENDIX C
SAMPLING TRAIN DATA SHEETS
In the following, sampling trains are designated by ID numbers. The ID code for each
train follows the sample coding scheme described in Appendix B.
187
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I9KICTTC KBITS
CaflJLflTO C5U.TS RR SftdS • — E0K312UJS
Plait! or UBdrtid X/HJti
*i ics vera.
' •: O/a/M Print* 09/5J/M
Tut Nb/Tyvi ED6S1211B
IioUiatleity ' 1 1 •
tt.0
*1» Location! SOUK* BRET
Mart/Stc* Tii»i 1211-154]
Mtarad Saa#J. En Ma («fl Via atd) •
141U
(¦a) Vis M) •
4.13
WWfclUI
snea.
HUE
Slack 6k Flw, iU cord. Wtcfi) B(i) •
1100
kilc.)
ltd end. (ass/mUQft) ¦
U.2
•onlt PlMlai i fciuil (in)
1UI
0.E7
actaal Itchl S(t) •
H74
PItot Tula Corrartlon Victor
C(»)
0.M
actual (aatai) B 02(*/dm :y Hid) •
25. W
Total SMlinf Tia IrirO
ItTwta)
I 204.00 !
W ait) ¦
25.30
ttromtric Prmmn tin Hg)
Ptb)
30
Start Pimai, idaoliW tin 1^1 P(») •
25.85
5l«k kmn (in ICD)
P(ftack)
-<
Stack Vliocity Ift/Mc) V(t arj) ¦
32.3
Ba tatar Iritul Hadirf in ft)
9*4.571
6n Natar final badiiq (n ft)
11B.9I
Nvt Su SmcIi Vsltaa lev ft)
Via)
( 111,34 1
Vol of Liquid Callaetad (all
Vile)
1707.5
Vol «f Liq 1 Sit. CandL laef)
Via atdl
1 00.391 )
Mt. of Filtar PartiwUta Ijw)
0.0332
V* of Sro4» kuft Pirtievlita (ga)
e.o:
f Co^inad Particulatv (ja)
Rip)
I 0.MS )
S Ctnctntratiw (by QX) » 12.2
SZ Covnlrftien (b 1
117 1
ObOTI 1
(dq C)
T(i «n' ¦
K.2
i :
SI 0.21 !
l.S 1
1*0 1
138 1
lit 1
0.5099 ;
2 !
8
! 0.S 1
l.M I
no:
138 1
IK !
O.SOOO into- imm
ttn idq Fi
Tta «1> ¦
1Z2.I
l:
a
: o.2S i
LH :
IB 1
US 1
117 1
0.9000 1
un o
Tla (vg) •
SO. 5
4 i
a
: o.!S i
i.« 1
110 1
at i
117:
0.9000 I
wr*0 (•*)
BTTUP) •
0.419
I I I I I I I I
I— :— I— i— i— i— I— i
— i— i— i— i— i— i— i— |
! ! 1 I I I I I
I ! I I I I I I
— i— i— i— i— i— i— i— :
WU ! 8» ; is ! 14,4200 ! 1440.0 ! 10CC.0 : *010 I 1.9142 I
191
-------
ISCKIICnC KBITS
cnnLRTEs «9u.re rat me i —
S062J125SO
Pljrti OF Uptoto* ctm/u
fcrfwaa
*•
M mas
- 1 01/2S/U Print!# 09/11/M
Toot No. Aypoi
90S3USH
q Iaokinatirity
1 1 •
99.1
. „lt Lacitiorj STKCX
SUrt/Stoe Tlaai
19-1333
IMtvai Saaelt to *>!» (Kf)
Via (t<) •
31.94
(a)
Via aUI ¦
0.9CS
WftlU
iracL
vuc
Stack Em Fla, tM and. UefD
Bit) •
127
lealc.)
(U co«L Un/un)BI*) •
S.4
Iksalt DUvtr, Actul (in]
lid)
0.337
KtUll -tlnUta uadint, try l^/aacf) C(t fU) *
4.000
Stact (Dirt! ffmaiona dali
t 7» Cll |U) •
& 0134
Mia (if road)
1
7
t 7X 02(*/4nl Cll iM) >
31
lentil fif rectangular)
L
0
Pvticilata £nmor liti (Ih^Tr)
Els) ¦
0.0(1
iidtt (if ractangvltrl
V
0
(kg/?r)
E(p) •
0.027
fr«* of Stick [M ft)
R(i)
11.0(901
Stack Sac knar Vaeor ^ooortim
IUa> •
0.341
1 of Sunli taints
1
12
Italnlr IhigM of Stan Gn, Dry
««l •
a. 3!
ToUl Saaeling Tib tain)
(that*)
I tc.00 I
IM
m«) >
25.40
Iwtrie kmn (in Hg!
P(b)
X
Stack PpMMrm, ataolutl (in Hg)
PlD •
25.79
Start Hunil (in (GO!
P(ft*U
-0.01
D*«-a«> SUai Wlocity (ft /me)
Vd «vg! •
213
Su Wit Initial Haading (cn ft)
7.3U
tas %tar Final teading (n ft)
42.101
Mt Saa Saaalt Voliaa (n ft)
VOl
< 3*. 7* )
fcl of '.inid >ollictid la])
VI (e) .
3E2.U
Vol of Uq • Std. Condi. (acf)
VI. ttd!
1 17.070 )
W. of Filtv Particulate (go)
0.0077
Ht. of Pratt Haih Particulati !pi>
0.01
' Cotfinad Particvlati t|a)
« •
47.2
2 1 S f #.11 1 0.4* 1
IK
134 1
110 1
0.BI7 I
3 ! s: 0.111 0.SS
IK
134 !
ioa i
0.3317 lltaM tali Suia • H> I'ic)
SRTUP) >
S.3U
4 •• 3 1 0.11 1 0.IX i
IK
134 1
in i
0.3317 1
s ; 3 : an i o.et
U0
133 1
112 !
0l3S7 1
t! s i 0.11 : &us:
IK
133 1 113 1 0.D17 I
O O 4
111(11
linn
niiii
TDTIli : U : 1.M 1 12.4120 1
11(0.0
isq.0 :
1775.0 1
4.3610 1
192
-------
rswicnc csjlts e&OL/nn peutj oh ewu • — AouaiiiMn
lint: OF ' Uocrtad 09/07/11
fuimm
by:
C. KM 1 L tilU.
jrt., 04/30/48 Printed 05/19/88
Tttt Ho./Tyooi
A0U0111MI7
IiaUvtieity
> 1
S3.}
Saale Leeaiioni CFTOOUJ9ES
Stari/Stos Tin:
1U4-1U1
ItrUmj Siooil Cm fclaa (jcf)
Via rtd)
712.(7
(KB)
Vto na)
20.111
PflfWCTO
SMO.
«i£
Stack In Hoa, (U Bond. Uwfm)
Oil)
S»9
(sale)
¦U cord (daca/mt)0li)
13.6
DonSt Kattf, MuJ (in)
««)
i.a
act ml (acfal
0(1)
27M
Pitot Tubt Cernetlon Factor
CO)
&M
actul (acm/nn) 8(a)
7LI
Sai Wtir Cwrwtion Factor
(alpha)
6.31
tartinUtt Uadinfc *7 (p/dKf) C(a ltd)
0.09U
Slack ®gct> Sianios (in) i
• 7* (E(|r/tacf) C(* ltd)
0.0US
Itadia (if round)
>
» Tf Q2(q/4sa) C(» (U)
1*6
Lfrftn (if rietanpilar)
I
20
Participate EmniSR tett (lb/lr)
E(P)
o.zn
Hidtk tif netangilir)
H"
12.25
(kj/)r>
E(p)
0.127
frm of Stak l«o ft)
Alt)
(1.701*
1
1
Stack it** Vatr Vapor toocrtion
Km)
0.073
t of Sopli Peinti
1
1
Rolacilar Mei|ht of Stack 6a, Dry
Xld)
a. 16
Total Saplin| Tw lain)
Ithotl)
( :?7,ao
Hit
*(»)
a. it
Sinvtne ftum (in Hj)
P(b!
a.e
Back Imm, ataalnta (in H(l
P(»)
2J.H
St act Prawn (in H2Q>
P(itaek)
-a oe
(Hvift Stic* Velocity (ft/MC)
Vli avj)
27.2
Sai Ibrter Initial Rndin( (ci ftl
SO. 3
Sai kir Final b^iiq (cv ft)
1235.1
Nrt 6aa Sanle Volae in ft)
V(a)
I ttt.M
Ml of Uouid CoUactid HI)
Vo! of Us t Ste. Co*. («ef)
'*. of Filttr Par*ieuUt» I go)
.. of Crota Uun Particulate (gal
vt of Coelnto Particulate lg«)
Vi(c) 122.99
Via ltd) ! 54.064 I
0.%
1,16
<(p) I 2.7W 1
OS Csmntration (by CO) t 7, S3
SK CoiwntTjtioii (by CO) l LB
CD toemtratien (by CEX1 < 0
•e Conetntration (by diff.) I ( SiS7 )
Saasla
dCloek
IMlocity! O-ifin
Stack
6m
Iktv !SBFT(fl?J
HEJ MTP M»E3 FDD SMU « -
MU0U14W7
Point
Tia
Itaad, dPHWttr.dH
Ta*
Tap
tain)
Mip «Dli(in teO)
totjf)
in
i Otft )
Vilodty *
ad
(•«)
•
0.000
1
197
; 0.06! M
2000
170
Ul 0.22X
0*ifict Map feadinf
('«!
«
4.400
|_
—
_
1^—
Stct Tape
ntn
Ullf F)
T(* «v|)
•
2DOG.0
! 1—
¦
Uq P
T(t avjl
¦
109X3
IMa* Tape
p(ia«
(M| F1
Tfct» 6
pvi m
Oe)
¦IT UP)
¦
0.E24
ICTUS
197
: 0-05 : *.4000
eoeo.n
tlB.0
m.r : a.i?s
193
-------
isomeric estis
BLOUTB) IBU.1S ft* SOUS i —
EM30U17M
siti Of UnUtad 09/05/M
t^rrw*i
t/fi ics voTa.
urt.: tt/jom Print* 09/19/M
tim mb»Ayoai eououitw
iMkiiwtirity
t:
106.3
San la Uutioru SCUKX OUTLET
Start/Stop Tia: 1117-1354
MM San la Eai Vtolia larO
Vll ltd) •
123.29
(Dl__
Vii itd)_«
i mi
prwctei
stm
WLUE
Stick Sat Fla, tU cord. Utcfa)
ait) •
1175
kale.)
ltd en*. Ua/)Ul9lllL _ •
113
Vozzlt Bijvtv, Mail 1 in)
Hid)
o.»
actual ttefi .
Bia) *
2392
Pitct Tuti Cdmeticn Fetor
C(p)
0.M
actaal Usa/oik)
S(a) •
S7.7
hi Drtor Gametic" Factor
(al0u)
0.99
IrMcslfta loading, dry (gr/tttf) C(i (td) *
0.00t2
St*k (Dirk! timjn lin)i
1 7* Ely/Birn C(i ltd) ¦
0.0)00
ladiaa (if romdl
1
7
1 H Blq/lol
C(i ltd) •
23
Unjth (if rtctarnular)
L
—
Particular Eaiwia bt> Ub/hr)
Eis) •
0.0(2
Width (if rvrtafulv)
U
—
(kj/hr)
E(pl
0.928
Saaplr Itoluaa It* ft)
V(al
( 132.9! )
v»i of Lio-ie Coliaetid (¦» VI(cl I7«&.2S
Vol of Lis • StiS. Condt. lief) Via ltd) I 82.196 !
of ^iJtfr Particulata lp) 0.0495
.. of Pi*0Da Uatt Particular !{¦) 0
* of Ceninrt Pirtinlfli ![«! P(f) ( 0.0495 )
.02 Cirantration (by CDU J 12.34
Cu? Concfftrttion (by E2U < 7.47
CO Csncvntrition (by COO < 0
* Cafemtratiofi (by iiff.) I f JO.111
Saali I flCloe* !
Wccity: frifict
Stack |
Saa i
IMP :BRT(df>) :FHLD MTR PVONSES TO SWU • -
Eouoi:i7ie
Point 1
7i« Ifead, dPIMtr.M 1
Tw
Tap
(oqn :
i
lain) 1
(in H2B)!(in m) !
ida«n :
in :
ovt 1
IMlacity H
Md
(•«)
0l(W|) •
0.314
1 :
IS 1
0.2 !
1.95 I
lac:
m i
7b :
6.5000 la-ifict I*
Ic- teadii
lie)
0Mav|) •
2.435
2 :
19 !
0.3 1
2.34 i
in :
lu :
e i
0.5477 1
3 1
19 :
0.33 I
£.57 :
IB i
123 1
9» t
0.5743 1Stack Tan
iratrf
i*n f>
Tit iv|} •
1B.0
t:
is :
0.3 :
2.14:
IB 1
IB 1
9S !
0.5477 i
(*| 0
T(a avg) ¦
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* 1 •
so.7
Saapla Laeatiam AFTB&ftG
(tart/Stop Ttei 119-139
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»
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25.99
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225.125
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E0907HS7
laofcmticity
t I
1X7
Sagli Looticnt SDUSEJ) OUTLET
Start/Stoo Tiaai
1157-1417
latarao t«Bli Cm uolw ttcfi
Via Cwictin Ftctr
C<«>
6.84
acta*l (an/ciO 0(a) •
70.2
Sat %*tr Caractio* Faetor
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LOOM
Stack Ooetl Sinnam liiOi
t 71 Of(p/(acfl C(a txai •
0.0171
lidiin (if md)
1
7
1 71 02(i(/dn) C(i stdl ¦
40
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L
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Els)
0.10]
Hitftd (if ractafalv)
U
(k{/hr)
£(p) •
0.047
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«(•)
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!(¦>! •
0.323
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»
1
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25.58
Total Sopllai Tia lain)
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25.77
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s
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29. B
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313.422
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Ut of Coabinrt Particulati y S30 1 L4
CO Comtrttien (0* C80 I 0
K tocMritm (by diff.) t ( 71.10 )
Soslt I Clock IVilocity; frifict i Stack ! Sat nmp iSOTUO SFXELD KTfi MSE5 fW SfWU « - E0907U57
ftjint I Tim iMaad, rfP!Artar,#< i Tav ! Top (MgFl I I
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II 17 I OlU 1 £.71 I UO I IB I Ml 0.3M Mftv T^itn Uq n Tto «i> • 1B7.0
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197
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i
urUi 09/07/M trintad 09/lt/M
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sqiE
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L
—
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0.0SS
Witftti (if raetai«tlar>
H
—
(kj/hr) E(p) •
0.010
ffrw of Stick (¦) ft)
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Stack la Mr Viper Proportion K
14
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f
4.4
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t
0
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Plmti OF Uodiitd 09/07/M hrhred byi LUIS
«>«'« Print«J 09/24/tt
Tort tte./Tywi BO«niZ9K7
lutiiaticity
» 1
AS
Stasia Ucrtiaii AFitSMB
Start/Sloo Tia»t 1129-1323 •.
tatarad &«el« to Vblta :
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DUULATcS EUR KH StCU • —
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3.144
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Stack Sa> Floa, fW ccrd (tefi)
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114)
0.357
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Clf)
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actaal (m/ain) 0(a) •
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8
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7
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L
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£10) •
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y
(Mr)
EIS) •
0.014
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0.3S2
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•
8
felacalar Mifit of Stwk Sat, Ory
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B.t0
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25.72
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32.7
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3M.11
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S0S.B3
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Via)
in.io i
Vol Of ilplli CoilEtae (ill
VI lei
1339.11
Vol o* .a 1 Stt. CarA. itcf)
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j
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ie Cumuli alio* lO¥ tiff,)
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1.970
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172
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127 1
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77.8
ii 191 OiS: I I
172
108 1
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0.3000
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130:
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199 !
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108 1
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lei! i Vf Upditrf 01/07/M tm fined Sjrl J. KILLS
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SH09II49S laokiiatirity
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IC3.1
Suplt Location SflB
Start/Stop Tiai
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tailnlit* Losing, *7 fyr/dscfl Cis ltd) •
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1 7* Si^/Mcf) C(i (td) «
6.0142
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I 7
( TJ Q2(jg/dm Cta itd) •
33
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Elp) •
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If
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tip) •
6.03
(m of stack lie ft)
All) (1.04901
Stack Sm Hrtar Vaar Pn*ortion
Kasl •
C.XI
1 of Saslt tainti
1 12
Macular *lfrt of Stadi lai, >f
1(d) •
21 «0
Total Supltiq Tia» (nil)
(ttwtal ( 60.00
m
Nit) •
2S.1S
kroMtrlc Prnurt dn Hg)
Bfb) a. 87
Stacx Prmirt, aDwlgta (in Hj>
PlI) •
a. 16
Stick Praiun (in IOT
P(rtjct) -cm
Owagt Stack V*lgcitj (ft/aacl
Via a»j) ¦
2M
Baa Mar Initial toad in (CM ft)
770.91
tai Nritr Final laacint (n ft)
606. ses
M Sm Saalt Velu* (ex ft)
v(i> ( an)
to] of Liquid Ce!lf?tM lall
VI (c) MS.3S
Vol of Lug • Std. CflflCft. (acf)
VI. tU) ( ts. 7*1 1
i. of filter °artiNlat» lj*l
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O.ol
Ht of Zoisiiad Particglata ls»l
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S Cmv.tration (bgr CDO
I iZ.it
32 COTCfnt'ation (by CEA
* L3S
a uwculution lbr CEO
I 0
•C Ciwwil ration (by tfi rf.)
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T(a a*|) •
42.1
1
is
i 0.34 ! 2.72 1
itt
IS
109
0.SI21 1
—
_
1 |__ |
1—
—
— Ifeul tan Suiwi tf
(*K)
anm •
0.3T,
120 : 2.75 : 2.S08 : U2M i m.ti 772.0 ; *.72*
209
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I
ISXHCTi: iEULTS CflLOUITQ SESU.TS To SHKK£ I — 999201 i2SS
»t; cr IMatid 9/21/M ifrfgrme bri J.MUS
9/WM n/ZSM
1»»t te./Tjoti
sazonae
lukiioticitv
J 1
104.3
SmbIi Lacttiaa STflDt • -
ittrt/SlM Tut!
1125-122
MM faMl* In VbiM (Kf>
Y<» tid)
49.02
(wm)
via nci
l.Jtt
MMCIE1!
s*m
Wi£
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qui
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(calc.)
0.3S7
actual licfii
Q«)
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0.M
act Ml lam/ai*> id)
111
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1
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0.0109
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t 7» 02(*7<*cfi Cll (tC)
0.0205
(acid If round)
«
7
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Lfnffi (if r*ctn|ui€01
Ptitacw
-0.06
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V(« avj)
3S.3
Sit Iktcr Initial Itaadim (cv ft)
BH.6M
fiu Urtr* Final Baadirq If. ft)
944.931
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v»l of Lib I Ste. Corft. («c?) Vu «d> < 30.S31 )
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5 : 0.3 : IX
; ifi£
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79
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104
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1 0.5477
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BLQLaiD 8E9ULT5 «* S*P-£ t —
A0£2094au7
An: Of UoCitK 9/21/U
te-farwe tiyi C.KH6
^P<: 09/£/» Primid 09/2J/M
T*«1 tto-rfyoil (*»K«ai7
Uskinfticity
* I •
100.3
S«b1» Unticni inuiaWOI
SUrt/Itnc Tim 0948-1342
Mnd SaDit oa Al«a (tcf)
Via rtt) •
(KM
Via ltd) •
it.m
ww»m
ma
HUE
St«c* tu Hon. ltd eord. (Mcfm)
Bdl •
SS4
(eile.)
¦td end. Mn/uMOii) •
15.1
konlt Ihuvtir, ftrtul lin)
Did)
1.23
•etui (icfi)
fi(4j •
2713
Pitot Tiua Correction Factor
C(o)
0.14
Ktul (as/tin) BUI •
T&.9
itt %?«r Comctio* >«rtor
Ultfvi)
an
Pirtinlltd losing, dry (|r/dKf) C(l (td) •
0.I00S
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F1£H D6I6 WSBSS TO BPJ 1 -
D0SZ094917
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d'ltvj) ¦
0.044
i ! 240: o.ow ; 4.4
2000
1 171 : 1(2
6.2191
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sMtavf) •
4.400
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Th ivj) »
2000.0
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—
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(U{ C)
T(« «
10S13
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Td m|) •
ltt.S
i -i i
—
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—
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7(a «V|) •
74.7
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1 1 1 1 1 1 1 1 1 1 1 i
tnm l»w B»i» 1 tP Cac)
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0.219
nuns : Me : o.os I 4.4000
: tooo.0
: 17:.0 ; K2.0
0.2: r.
211
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ISCKICTi: SSU.T5
OLCuunQ results rot *mu * —
Eoszonon
Of Uttttrt f/23/U
«¦: 9/22/S8 Print «l 09/23/M
torhnm
It VcSTflL
T*it lta./Ty»i
E0K2M50B
Iwkinrticity
* i •
S4.6
SaasU Ueationi SCHEHX t»/T-£T
Start/SIss Ti«>
0950-US4
ftnms Sanli &•> Voliat iKf)
Vll ftfl •
101.32
(a)
VI* vte) ¦
2.M3
mncra
im
MUS
SlKt (a Flo* tt< cwd. (nefi)
G(«)
1220
icale.)
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3*. J
fcjzli DiMtte-, fctul tin)
»<«>
0.373
actul (tcfi)
Bla) •
1 71 02(fr/Mcf) Cts lt«l •
0.0225
tills (If round)
II
7
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—
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Els) •
0.133
Hidt.1 lif rtetifljulir)
V
—
Els) •
0.019
ftva of St act (M ft)
Alt)
(1.06901
\
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Stack En Hatr Vasor ft^wrtion
lino) •
0.406
• of Suslt »Dlrrti
1
•
RolKulv Might ef Start Su, Dry
Rid) •
B.64
Total Saaolirf Tib Inn)
( 120.00
m
*l») •
24.51
latMtrie ft-Wliff* llfl H{)
0(6)
30
Start Ci mm ». anoluti (m Mj)
P(ll ¦
23.13
StcV kflin (ii N2D1
0(«tart)
•e
It^rni Start velocity (ft/we)
»(f a*j) •
34.1
Ml MP Initial flHCIKt (CM ft)
•57.10*
(at Ittfr Final IfcWint (n ft)
iooe.««
tmt Bit Saagli vtoliat (ru ft!
VII)
i ni.%
Vol trf Lime CoiiretW <¦:) Vllcl 1472.2.
Vo; cf Lie I S:e. C«nci. Itc*) Vi» ito> ( 63.2?? )
#of Filter Pi*seuiat« ijii 0.086
e* Vr&f iliVl Pirtipilite (p) C.Ul
of Caiiws Paliculitt I pi Hi) I C. CSdO 1
(E Ccrersritio* lb> £E» « 11.9
Cup CuiLiiitritic Ity d1 * 7.3
CC Cocvntritiar (by CE?r> 1 0
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: (d»jF)
in
out
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0.334
1
15
0.35
2.1
: 166
S3 :
Ifi
O.S916
Drlfici Mitr toadtnf
(¦*)
(Wl«vj) •
2.(70
2
15
0.33
2.S
166
130 1
% 1
0.5916
3
15
C.B
2.1
166
137 1
10* :
C.5916
Start Taontin
(oaf F)
T(» •«]) ¦
166.0
4
IS
0.34
L7£
166
139 1
110:
0.3U1
(Mf C)
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74.4
4
13
0.32
£.56
166
123
110 1
0.5657
3
19
0.32
£.56
166
1*3 :
114 s
0.3657
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ill 6
2
15
0.32
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166
145
116 :
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1
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0.32
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166
1*7 1
117 1
0.5657
1
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0.571
•
—
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turns
120
2.17 ;
H.3600
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1059.0 :
a. 01
*.6207
212
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W
rswticnc sslis
SOLUTE) BSU.TS FW SOUS • —
S0S211OJ
CJF U001t»d 9/23/tt
(•rforw syt
J.HILLS
V" 9/22/M ^xnie 09/23/M
t«t M. /7yS»l
SDS22D0W5 lislciMticity
» 1 »
102.5
Sail tautioni STACK
Start/Stod TlSI
110S-12ZS
Mtmd toll in Voiiaa (Kf)
Via its) •
47.21
(ks:
Via ftsl •
1.377
KWKTB1
SVWL
«U£
Stick in Floa, ttd raid. (Mcfa)
Bill ¦
1111
(Stic.)
its raid. <&a/nnlC(t> •
33.S
•call Diiatar, fctwt (in)
Hid)
0.3S7
actul (tcfi)
otu •
uu
Mot Into Cornel ion F»ctor
C(0)
0.*
¦ctaa] laca/nni
e«i •
U.2
Bu Mar CoTKtion Factor
(tlpfca)
1
tartinlata Uadiflf, »nr l|rW) C(i no) •
O.OI67
Stick Ouct) Dimiom (in)i
# Tf 02!(r/Mcf) C(» «td) •
0.0114
tac.s (if rowid)
I
7
~ 7* 02(^/omi) CIi «t«l •
31
Ungth (if netmjular)
L
to-tinl*ti Innion lita In ft)
Vttl
( si.a)
Sfcl of Liquid Ccllteitd (si)
VI !c)
645.51
Vol of Li; t Sto. Condi. Itcf)
Via lit)
( 30.572 )
Ht. of Fjltir Pirt:cUat» <)•>
C.C324
c4 #ro0» i*»"i BirtmUt* (e»>
0
~)f Qmiiwi PrticulKi (gi)
»(»l
I 0.0326 )
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10922110905
taint 1 Tii» !NMd« dP'%t»r, »<
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: (am) : (in (0)! ijn KDl
(My*)
1 IB '
out
(VilKity Wtf Cue)
gp(i*9> ¦
0.300
l : St 0.3 : £.46
ltt
96 !
91 :
0.S477 :Orifict %tr- Ming ("*l
Wltv;) «
2.4(0
2 ! Si 0.3 : L*i
ltt
: 113:
92 1
0.5477 i
3 : 5 : 0.3 ; 2.46
lit
: 123 1
94 1
0.S477 :{tK« lanntn F)
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166.0
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is :
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•JAjWfTIC «SHT3 CRXULATQ KSU.TS RS SMU I — MKUOSSSTl
S Of IWitm 5/21/M
hrfomd byi
C.MI6
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Daft: 09/2S/M Prinkad 09/24/M
Tflvt «o,/Tir*i
•OK1035CTI
JMiliaticity
* J »
9S.3
imbIi ucttiam tFTEnunex
St«rt/5teo Twi
1035-1330
Urtirai Saavlt im Volaa (atfl
V(1 ltd) •
17, SI
(tea)
Via (U) •
2.751
MHC1U
STMOL
*U£
SUdi ia Floa, ltd eond. (dttfw)
tit) ¦
(90
(calc.)
ft« card. •
19.3
*onl« Aetul tin)
*M)
0.57
actual (acta)
Qla) •
34)4
Bitot T«t( Corraftiofi farter
Cte)
0.M
aetul (m/um BU) *
19.0
Gas Wi» Ui itrtiow Factor
Ul*4)
0.»7
Prtmlato Loading, dry (jr/rtcf) Co «t(l •
(.0194
Star* Uhct) tHMraiom linl:
1 71 D2mn I in Hjl
Pit)
10.1
Stack 1*1 laaira. astcluta (In Hgl
P(»l
30.09
Stack »rM»urt fin «fl)
P<(t«dO
-0.04
hrqi Stock Mlgcity (ft/aoc)
V(» «*5l •
34.2
6a* Orttr Initial Rtaein? (n ft)
969.7E5
Sa* %tvr Final foadinf (cu ft)
1042.19
Nit Sat Saaslt Vglm (n ft)
V(»)
t 112.43
I
Mai of Liome Celloctod ta!)
VI (c)
IX. 07
1s\ r> Lis 1 Std. Carte, (left
v(. (tm
1 9.041
)
Filtfr Otrtieulata (p)
O.0J74
Sroda Va«\ °«rt'.njati tf»l
0.03
* e' Cortiwt Part icu liti (ga)
*
: dm) ! Iin «0) Mm «0I
(••jF)
in
out
velocity (*ac)
0P(av|l •
0.0«0
i 1 Ml 1 0.06 1 US
1000
142
129
0.24a
frifieo Mtr iMdint l*ac)
tfHIav;) •
1.130
ti 6 : o o
0
8
0
0.0000
— i~ i— :—
—
—
—
Stack laaritar* Mif Fl
TO «;) •
2000.0
— |— |—
——
(»n 0
T(i (V|) ¦
1093.3
— i— ;— i—
—
—
Mar liomtn lo«| f)
T (a tvf) •
135.3
t 1
—
—
—
—
U
TO Mf) •
57. S
IIIIIIMInll
—
tot-tertnm <•*!
WT10) •
0.2U
xtsls : mi : o.oe i i.imo
2000.0
142.0
129.0
0.2121
214
-------
£
•3ETIC salts
OF UodltfS 9'Jl/M P»i turn! by! . C.KIC
Sttti 09/am PrintM warn metiaoen
EasU Ucitioni «FT0BW»C1 SUrt/Sto# Tiai 1035-1330
0L04JITB RE5U.TS mi SMPti ( — P092610SST2
Iiouwtmty
%tirM halt 6a Vela
(Kf)
lua)
* 1
vtt ncl
Via ltd
mnemi
sm
VOJX
Stic* 6a» Flos, sU eeirf. WirU 0<«)
666
(c«lc.I
ttd eon*. (MOB/ainlSUl
16.9
fenlo Diaator, Actual (inl
RIO
0.57
oetul lacfai Sit)
3S3
Pttot Tuat Corpcetion fictar
CIO)
0.14
Ktai (aa/ntO On)
99.6
Sa Wt» Corbel lo» Factor
UlM)
i.oe
Partmlatt loading, try l(T/ttcfl cif ltd)
0.0000
Stack !ftrtl Diataiora (inli
1 n 0i(gr'osf) C(l no)
0.0000
todi7 k
J0.1
Stock PrMtvt, IMOlvtt (in Pit)
30.09
Stac« frrttun (in tCQ)
Plotack)
-0.0#
towr*fi SUM VtlXity (ft/MC) VII «vjl
34.5
6m %tir Initial RtMin; In ft)
MS. 72
6as Final toading (eu ft)
1006.92
lilt £m infli Vols In ft)
V<«)
( 111.20 1
Mil ef lituit CcUortfd til)
VI (C)
307
Vol of Liq 1 StiL Caret, (icf)
VI. std)
1 14.450 I
Fiitor P«rtic\ilati (jit
0
1W>f Prota Uttfi PvtieuHtl (jfl
0
o* CoOinad Particular (|a)
»<0)
I 0.0000 )
tE Corcmtratioi (by C£M)
1
7. J
CE Concirtration Iby SEX)
i
9.3
CQ Concwtritim (by CB0
(
0
>G Connntration (by fliff. 1
i
I 6140 1
10X1
101.42
£.172
1
I
1
\
\
Sawl»
Point
Clack
Tim
lain)
vilocit y
Hm£, HP
I in «Ct
141
0
0.06
0
Orifict : Stick I
A»t|P,W ! Tms
(if, «9> S <*t*>
1.15
0
141
0.06
1.1500
2000
0
2000.0
6u
Tas (Mffl
In
142
0
142.0
out
i^tloclty I
ia
o
ia.o
0.2622 ((Hfico Mir teodiat
0.0000 ;
— (Stack Tanmttrt
IIMtp T^srttw*
— (toot »¦> tamfi
dHu^l •
1.150
(at f)
(oag CI
7(1 t*l> •
7(» »*|) •
2000.0
1063.3
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Tl* i*|) •
IS.5
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0.263
215
-------
ISKDCTIt KBITS
Plait: OF Ub&itad VZVtt »i fini) tyi H.WJTSL
Cite: 9/2S/» Print* 09/2VH left Ns./T|ra»l EOEtltHTTl
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nw. mux
(ctlc.)
MM) ft. 257
Clpl 0.14
Ulph*) Olfl
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tenia Di tarter, fctu) (ta)
Pit* Tube Correction
fin Artw terceti* Fid or
9tck QHet) timmimm lifOi
Mia (if round)
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kitftk [if r«etn(glirl
ku ef St jo tic ft)
I ef Stale tointa
Tottl Steeling Tla (sin)
Inwtric ft e»«me tin H()
Stick fcvnvrt In, NEC)
Bt> Me Uititl Retdif* <« ft)
fin Ifcter Finti (biding (ru ft)
Mrt S« Stwlr Vol we lev ft)
«(f)
11.06901 )
0 »
(t*U) t 120.00 I
KM 3D. 1
Kit**) -e
12.221
121.516
( 113.30 I
Uokirvttelty
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t 1
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m
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IhtPtgi Stic* Viloeity ih/mc)
Km)
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Nit)
Pdl
V(» ev
9L6
105.32
tm
w»
39.0
Mt
63. J
0.0104
0.0161
r
0.123
0.036
0b 335
n.68
25.76
29. B
3L3
V(e)
Mol of Liqmif CellKted 111)
Vol ef liq I St a. Condi, (erf I
M, nf Filtr- Pirticvlitt (je)
(ft. ef Profit Kitfi Pirtiwltte (gi)
CoaOinad Ptrticultti (gal
VI (cl 1134.13
V(» ltd) ( 51*16 )
0.0615
0.01
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OS Concentntivi (by CEX) » 11.17
CQ2 Concentration (by £EX) i 7.5
CC Concent'ilion (by CD*) 1 0
K Contentrition (by diff.) t ( 00.53 1
Suple :
Claefc 1
Mlocity!
tt-ific» :
SUek (
fin
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K»l(H7Tl
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Ti» :
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1
i
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out 1
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0.330
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0.35
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r kadlni
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2. HO
2 !
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0.35 1
2.4 I
1(6 1
116 1
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123 1
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0.5916 ItUet T«r
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166.0
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is :
0.35 :
Li 1
116 t
125 ;
11 1
0.5916 1
(At| O
Tl« trjl ¦
74.4
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0.B 1
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166 i
103 :
95 t
0.9916 1
3:
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lit 1
126 1
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0.5916 IMMr l^ai
it«i
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106.1
I :
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0.35 !
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ii6 :
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103 1
0.9)16 I
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T(a e*i> •
41.2
1 !
15 I
0.35 1
LI 1
116 1
127:
103 I
0.9916 1
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1-
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(*¦)
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0.992
TCi
120
i ¦. 1
LK> : 22.4000 ; 1328.0 I W.0 i 760.0 I 4.7329 I
216
-------
isxDcnc nans
caoursD ra.n rai mu • —
COS2S1047T2
Pint: OF Uoutod 9/23/11
P*r!uml byi
9/2&/H Print* 09/24/M
Tut to /T^ioi
B9861047T2 lakiMtintr
» [ •
10t. 4
9' Nations SCtUBEJt OtTUT
Stri/Hoe Tumi
1047-1250
Mn«Wi6aWa (sf)
V(a its) •
101.70
(oca)
V(a its) •
2. M0
MMC1EI
mm.
MJ£
tat ia Flos, «M ewd. (Mcfi)
!(•) •
1223
(T4lC.)
¦to end. Un/mnHllo) *
34.7
feuilf Oiaator, fcrtiul (in)
*!d)
0.357
act a«l Ucfo)
D(l)
2503
Pi tot Tute Cumttion factor
Cto)
0.14
artwJ lacB/nnJ BU) •
70.9
6m (fete* Comet ion Fartar
Ultfia)
0.99
hrticil»t» lading dry (^tftcf) C(i ltd) •
0.0000
Stick Dart) Siamion (inlt
1 7* CB(gr/4Kf) C(i ltd) ¦
0.0000
Mia lif renl
«
7
• 71 Blq/Ma) C(i Mil •
0
Unjtli lif nctnftlv)
L
—
Particsltto Eaiioion Uli (Ik/hrl
E(s) •
0.000
Vim (if ractwfultr)
y
—
Itq/hn)
l(R) •
0.000
(Hi of Stick Ik ft)
R(»)
(1.06901
Sticsi (a atr Vtoor Prooortion
K«l ¦
0.420
1 of Sue2> Pointt
t
1
telanlar Might of Mock lav >7
¦id) •
29. U
ToUl Sapling Tia lain)
ttn«U)
( 120.00
at
R(l)
24.77
kraotnc Innn tin
Plb)
30.1
Stack Imn, aoaclnU (in Hgl
Pl|) »
29. e
Start Pmiwn 11r tfiDi
P(ttack)
-2
ftortfi Stick Mlocity (ft/ac)
»(» «VJ) •
39.0
fia fctor Initial n»u)int (« ft)
435.(£3
Su Krtor Final Rnbi^ (c
0
« Conrwrtration (by diff.)
*
( 00.53
Saplo : (Clock !Velocity! >ifitt
suet
Su
Mrr- isaetieP) ifi&ft wa acmes t» shwie ~ -
E092S1047T2
Point 1 Tia DM, tfPIM(rt«(
To*
1 T«*
Mtgf) i
1
! (ain) 1 (in WD)! (in 10)1
Mo«F)
! in
out !
(Vilocity toad t*ie)
dP(t«tl •
0.350
1 : 15 : 0.S ! Lt
i6t i n
75 1
0l39U StHfia totv Coding !*ic)
LI00
2 ! 15 1 0.35 ! M
Hi 1 114
11 !
o.nii :
1 : 15 1 0.3! ! £.1
ltt
I 123
90 ;
0.5911 IStack Taarotw* Idog F)
T(i ivg) •
ltt.0
4 i 15 1 0.E i LI
lit
1 I2t
% :
0.5916 1 (df« CI
T(» t»p) ¦
74.4
* : 15 1 0.35 1 LI
IK
! 103
« !
0l99U !
3 i 15 i 0.3! ! LI
IK
ia
101 1
0.3511 IIMar TaantOT Uog F)
T(a arj) •
1CS.0
2 1 15 ! 0.3! 1 LI
ltt
IX
103:
0.5914 t m% U
T(a i«|l •
40. S
11 15 I 0.35 ! LI
Itf 1 121
104 !
0.9118 1
1—
0.5S2
1 1 l« 1 1
1—
1—
1—
— 1— 1
TCTSJ ! 120 ; LB ! 22.4000
1321.0
: 13L0
741.0 :
4.7129 ;
217
-------
SKSCTIC IBU.15
ouumB kslts Fa imu t —
¦0BI11496
Pint: Of UDdatad VU/U
fei liial
J. Mils
9/2S/M *Mwe ovzvie
Itft te./Typi
anauoe
laokinvticitjr
t 1 ¦
V.t
Ucatiau PACK
SUrt/tW liai
11«-1»3
Mnd Saslt Sh Ww tmf)
Via atd) •
4171
)
8U) ¦
(237
Pi tot Tito Corartion F«tw
C(p)
ObM
¦tail (o/nii) «U) >
03.1
8a Iktir Cmctian Factor
UlgtaJ
1
Mptinlft* UKui. *n
0.0SS
IHl of Start taq- R)
«(!> (1.06901 )
sue* 6m Httr v*£*y ft-DBTiia*
I(hd) •
0.311
1 ef Socl> teinta
1
U
klnlv Ifeipt ef ttact S«, Dry
1(d) •
a. 73
Total Sueling Tia (Bin)
(tlMtll
to. 00 )
ttt
Hit) •
2L00
ferostric frauw* (in H|)
PlbJ
30.1
Start >aam/i. atoslvta (in «c>
Pill •
30.09
Stack Pr»»*jr» tin US)
Pirtact)
-0.00
flwnta Etart Mlcrity Ift/nc)
V(i of! *
35. i
¦b tetar Initial feeding
to] ef Liquid Ce21aetad lal)
VI (el
«i09
Vsl ef L:q # Std. larto. Iiefl
V<« ltd) ( 23.210 )
tft. ef Filtf Particvlatt (p)
0.0357
«. of Prate kuft Particulatr ([¦)
0
Coabinati Partimlati (gal
*lp> 1 0.0357 I
Ot Coimtrilion (bjr tXX)
1
12.01
US Cancffitritign (by CEX)
t
7.1
CO tmaHniim (kgr CEX:
1
0
C Cemttritien (by diff.)
* (
10.19 )
! Clack Hfrlocity! Orifia
ttlrii I
sm m«p itarrupi ifihj ktr mmses fw ana t -
wstiitse
feint 1 Tin I Mid,
T»W I
tm
<*gF) 1
i
! tall! Kin recniin «D> 1 1
In 1
•St 1
ItolKity Haad i'k!
dPInf) •
0.190
ii si 0.3: thk
Mfi 1
107 1
14 1
0.3477 lOifie* fetar kadi* (•*)
W(tV|> •
2.460
II SI &3 1 L*i
m i
US 1
m i
0.5477 !
J : s i 0.31 t«i
i6£ :
117 1
It !
0.3477 iltae* Th» ilw F)
Tli av^l •
166.0
*! s: 6.31 m
lit i
ill 1
10 1
0b3477 1
(0q 0
T(t a*|) •
74.4
5 1 5 ! 0.3 ! &«4
IK 1
US 1
« 1
0.3477 1
1 ¦' SI 0.3 ! £.4(1
IK 1
III 1
»i
0.3477 !
IMv Taprihn Ua; F7
Td »»|l •
103.4
it s: 0.11 {.«
ltt 1
to i
W 1
0.5477 1
Uq D
T(a t»|) •
4ai
1 ! 3 1 6.3 1 L4t
lit 1
121 1
B 1
0.3477 1
3 1 S ! 0.3 1 t« 1
lit 1
ill 1
K 1
*3477 1
fca,4 8mu ¦
-------
iHxaenc saiis olqutb wits ra* m*£ • — w2ao«tw?i
"niti CS UoMtad 9/a/M
Parfa'atd bri LKI«
Ji 09/21/H Prirtad 10/01/W
TKt to./Tyai flOSSOUliCTl
IsolUTWtlcity
* I
K.7
Sacli lootiom fr-ltnaiWCS
It art/St oo Tiaai 0131-1230
•atarae Sasla bi VoIm tacfl
Via *t«)
100.49
laal
via ttd)
LM
RMKTO
STHO.
VfUJE
Stack Eat Flaa, ltd COM. laaefa)
S(tl
m
(etlc.)
ltd com.
0.S2
actual lacfal
8lk)
MtS
Pitet Tub» Cwwction factor
C!s)
«.M
actaal lacs/an) 9(i)
99.0
Gu Hatar Conteiioi Factor
talfha)
0.97
PvtinUt* Loading, dry I|r/dicf) Cli ltd
0.0100
Stack (fcrt) Olaaraion (mil
t 7» 02 C<* itc)
0.0101
lacia ii' round)
1
—
1 7* (Elag/dtca) Ci. its)
23
Ldnjth lif netmjular)
L
n
Partinlau Eoaatan lata I1&/V)
Elai
0.060
Width (if rKiuquitr)
*
i2.es
Ikj/hrt
tip)
0.067
fm of Start Im ft)
«(¦)
(1.70131 1
Stack Sal katar Vaoor Praasrtian
IM
0. «./
1 of Stasia Points
•
1
Roimlar kaipt of Stack Sat, Ory
K(d!
B.7«
Total Saapiinq Tiaa Inn)
Ithata)
I 17100 1
Mat
Kill
H.H
Wro»(rir P-aaturi !m Kj)
Pit)
a. 9
Stan Pmm. atasluta (in Hg)
CIS)
a.w
Stack Praism (in 1C0!
Pittart;
-C.01
Ovarigt Stan Valocity (ft/aacl
vis avj)
M.2
Su Aftar Initial Raiding (« ft)
M.32
Sat Katar cim1 biding in ft)
198. Wi
%t 6u Sa»U Volua (n ft)
V(al
< IW.09 1
Vol of liauid Collactad (all
Vile)
153.77
Vol of Lie t Std. CskIi. <«cf)
Via ste)
1 7.2:3 )
Ut. of 'ilt^ Particular! Ip)
0.063
of tola lias* Pftirulatr (gal
0
¦t of Cottmae Part irulitt (pj
No)
1 O.ObSO )
B Cwcantratiw lby HX1 t 7.2
32 IsiCTrtrati* liy CP!) t S.1
CC CercmriUrn (by CSX) I 0
•C C«»nh-«»ioB (Iff diff.) * ( U.T0
Sael* ; Clock
toiRt ! Tib
: (am)
l :
0 :
JT9
0
Molarity! Drtfica I Start
Hue, cP:wtr,W : 7tm
(in NEQ): tin tfiOl ! (dqFl
loe :
0 :
i.:: : 2000
0 I 0
Tm
in
IS
0
out
113
D
S0*Tld»)
0.O&
0.0000
V»lXltr MM
Oifica War taading
Sim inritn
Mrir Tantn
FIELD MTfi MMBS fW 5*11 • -
(¦«)
C«)
tors f)
(oaf CI
Uf« Fl
lot; ~
(•*»
#09309311011
dPlavf) • 0.080
dHlavp) • 1. ISO
T(a a«f) • 8000.0
Til rtf) ¦ 1091J
T(a a»fl • 122.3
T(a (*j) • 90.3
¦ET(df>) • 0.2U
TTBU I 17*
0.0* I 1.1S00 1 2000.0
132.0
HID
219
-------
<£l
IHXiCIC SSL'S
' int: CSF UMitld 5/J1/88 Perfored feyi
41 09/28/88 OrixtM 10/03/88 Tilt to./Tyoti
iHBlr uulini 8F7EBWOI St«rt/Sto(> Tim:
C&auTQ SHITS TO S*U I .
W928OTJIW2
C-tlC
B09e»0931CT2
0931-12JO
mmcTEi
SML WLLE
(e«le. >
•on 1« Siavtir, fetiui (in)
Nidi
C.S
Oitot Tub* Camction ftetar
C(9)
0.M
Ga Kftr- Cornet i an Fietor
(|]*»)
Stick (Suet) OiMmicra tin)i
(if rrot)
t
—
Litgfi (if nctwtvlip)
I
20
MitftM (if ffcttngalar)
V
12.29
ft* of Stirt (h ft)
Adl
(1.70138 1
t of Susli Pointi
«
1
TeUl Soslin; Tin <»in)
(t*»t»)
( 179.00 )
Eiroartric Prnwr* (in Hfl
P(o1
29.9
StuV B-mi-l (in «DI
dr;jc«>
-0.08
C«i %1»T Iritul biiirn in ft!
8.3H
Su Wr :im! !c« ft)
i»*.873
Mt 6u Susif Uoltu* (n. ft)
Vt»)
1 <|L2 )
Wo', of L:c.it Collirtw i»D
VUe) '
176.«
Vol 0' Lij 1 5td. Cones, (k'1
Vi» ftc)
1 8.3M 1
*. 0' *i!trr Pi-ticuUSi )j»)
0
Of °roa» NUN Cifticultl Ifl)
0
». of Corsiwd Pi^inliti ([«)
*(:.
( e.oooo i
E Conntntior toy 2*1
1
7.2
S3 Concntritiei (Sy £3)
(
9.1
CO Conemtritiof (ty 3")
t
0
IB CsmntritiOT (Sy c:".)
f
( 8170 I
iiodiwticity
JKUnd Sail bm VoIm
EUci So Hob, it* cart.
st* cod.
Ktul
•etui
Barttcsliti latfint, fry
t:
(icfl Via cti)
l«a) vi* ltd!
(McfW 0!»
(Aca/moait)
Ucfa) B
I 7( Biq/Ma) Cli ill)
S«rtlculBI Em II10* toll (Itfnr) £ij)
IlH/np) Eill
Stick Su Hit «r Vubp Preaortic
Rolmlir Miip! of SUrt Su, Brjr
UK
Stick PntKn, iMoluti (in hj)
Ovwiji Stm Viloeity ift/iicl
9iM0)
»(C)
til)
Pit)
Vit l«T
1OC.6
104.13
1071
457
19.7
MM
99.1
O.OOW
O.OOSO
a
o.xn
0.000
0.071
S.7*
2191
29. £3
3>. J
Stfi*
: Clock
IVflocityl 0r:fis»
Sttr*
Su
•Wfr
arid?) data atopcs mu » -
fl03a«31T£
faint
: Tib
!Mh0, OPIIktfr,^
Tm
Tm
(«»t?l
:
(•in)
Kir «Dl!(m >80)
id»r)
in
Ht
;Velocity HM
l*«)
•
0,080
1
171
: o.oe : i.:5
2000
130
107
3.23a :9rifiEt SMiirj
I'«e!
¦
:.:S0
0
: 0
: c : 0
0
0
0
0.0000 :
Is»5 ?!
Til «VJ)
¦
2000.0
_
1— 1^—
—
—
— !
I«t CI
T(i »»f)
¦
10U.3
;
• 1
_
— Iltotr I«wtirt
lei? f)
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•
119.:
—
!—
1—
—
—
—
!
(»; Q
Til IVf)
•
~8.;
• '•
l-tei
BRTW)
•
0.282
j
| ;
—
1 1
WHS : :79 ¦ c.m : l.isoc: 2000.0
I !
1J3.0 ; ;S7.0 : 0,2828 ;
220
-------
isaocnt sults
BUUnB CULTS FED SWJ • —
E092S09MH11
' CSF MittC 9/23/M
^rfarwQ byi
U.<€Tfl
>..<1 Prints 10/03/M
T«t he. /TyT*[
E0926094GK371
llMirnicitf
% 1
)«.:
Soglt Location in H/TLsT
Start/Stea TiMt
OM-1200
%Kirn! SttSlt Cu VoluH (Kf)
Via eg)
ll-.U
lu)
v
11(4
Ictlc.)
ttd csMi lascm/un)0ls)
33.5
fault DiMtir, Retail tin)
•(d)
0.357
ictul ticfo)
OU)
£J71
mat Tut» Comctiai funor
Clo)
0.14
Kt<*l (io/liri Oil)
67.1
Ea Wf Comrtiw Fictor
(alrtu)
0.99
to-tinlil< LaMinii try {jrltieft Cla ltd!
O.OOU
StKk (Diet) fovaiora linli
t Ti Q2lp/MCf) Cll lt(!l
0.C139
bdiu (If retnri)
t
7
1 7* S2lq/dia)
:i» ato
32
Lm^tn (if nctirjdar)
L
—
l>«rtiMlitt Emmon let II had
Els)
0.089
Uiatn (if p*rt«m«ltr)
fc* of 5t*t <»q ft)
V
#!«)
11.0(901
Ikfl/hr)
E(g)
o.m:
)
Start Sa> Mitv Vaaor Pmortion
8(«o)
0.403
• of Susit Seintt
•
9
Halmlar Wgnt af Stan Stv >¦>
Old)
a. 72
Totil SMBJino Tin Inn)
ItlWtl)
1 133.00
)
l«t
• Itl
24.97
ltre»trie fcwwra tin h[>
P!M
29.9
Start Pimm, ataluta (in Hg)
Pli)
a. is
Stttn 9rn*rt rq (cm ft)
247.101
m Bo Suelt *>lu> (n ft)
VI*)
1 121.11
1
Vol of Liquid Co 11 let •« 111! Vl(e) litt.9i
Vei cf Lie I Ste. Cntfi. lief) vu its) ( 7&.S62 I
- of ci:tl- >ir»)Cn;«tt (5«) 0.06*4
af °ro» Ut" taiiruli't Ipi C
in of Goasitfc Bartiwlita (7*1 ato) I C.OeM )
C2 toctmpjtion (&y 3S) t '.11
22 Comfit ton ISy 231! » 7.7
CD Ooncmrjtion Ity E»! t 0
m ConcfHfitim (Sy <»~•.) » ( SC.£0 )
tacit
Pwiti*
Clan
Til
lain)
IVliOCity! Ifrlfiet
l%ad, *s:%t»r,<«
Htn H3D>! (in mi
IS
IS !
IS
13 :
is
CLE !
0.32 1
as :
0.32 :
0.31 s
13 1 ft.li :
IS I 0.11 I
0.E :
4.B :
Li
Li
2.6
2.4
2.5
2.3
Li
2.3
2.3
1BTSLS
IS
2.13 1 E.9000
Sttet
Tag
latjF)
ltt
tu
ltt
lit
ltt
ltt
ltt
IK
ltt
1494.0
6** xrtp
Ima leijt)
ifi I art
04
in
11s
122
113
1a
is
ia
1)0
1063.0
SHTIOO) :;iE£ Dfitfl MCMGE5 R* S»*S • - r09ao»4O«5Tl
70 !
71 !
K i
94 I
* I
100 I
101 I
103 !
104 I
0.3657
0.5437
0.3SS7
0.307
&SU
O.SH
:s*loci
-------
75XPCT1: DESULTB OLOUIES IE9LTS FGR MMU t — EOKam»Ji
'«ti OF Uodatad »/23/M Pr fuaad by] li.VSTCL
•t: K/WU Prixtrf 10/03/K
Ton fe./Ty»i
EOKKMOSTi laokinfticity
11
1(19.0
Shb:> Lscitiwi scwbe* anur
Jtirt/Stao Timi
09*0-1200 wng Smlt in Voliaa (irf)
V(« Its] •
112.21
(*e»
VI. itc!) •
3.in
MROCm
smoa.
ML1C
Stack to Flo^ ltd com. (ftefal
aid •
117*
(ctlc.)
ltd com. (ncm/iinlBii] ¦
312
tozzli Diavtar, Actual (in)
N(el
0.357
actaal lac*!)
Ola) •
£37*
Pilot TuSt Corr*tiwi Factor
CIS)
0.M
aRwl [(Villi 3(a) »
17.2
Su Nrtr Corrrctiwi Factor
dim)
1.03
Pa-ticoiitt Laadiif, dry (jr/Mcf) C(» its! •
C.H0O
Start Oct) hvsigra Unit
I Tt 02(p>otefi C(» rtdl »
0.0000
tadiia (if round)
a
7
1 ft Klq/dn) Cli rtel •
0
Lrifth (if mtnfgin
i
Paniculata iaitaiaa fata (lortw)
Elgl ¦
0.000
Dioth (if •ictnfvlir)
N
IkJ/hr)
E (o)
o.ow
fen of itKt lie ft)
DID
11.0190!
Start lai katir Vanr (Vooortion
1(a) •
0.41C
• of Saala Poirrta
•
1
lolacular toifftt of Stark Bat,
aim
S.72
Total Swlinq 7ii* din)
Ithfti)
1 13S.X
k*t
k(»l •
24.91
laroMtnc Prwaort (in hjl
Pie)
29.9
Stack kirnn, atioluta (in H{)
Bid ¦
a. ?3
Starh ^awur* (in ICJI
Platack)
¦S
fciragi Stack Wlocity (ft/M5)
V(« avj) ¦
37.C
Sas %tf Initial Saadinj In ft)
5M.7J9
Su katar Final Ifcadinj in ft I
tel. 122
kdt 6*1 Saala VoIum icy ft)
¥(•)
1 ULU
Vol of Liguie Colltctad nil
VI ic)
1US.U
Vol «f Liq I St*. CcrM. Ik')
Vim (td!
(mc?i
of 'iltfr Part'.cuUtt tp>
0
of 9ro» Hun "articulata Ifi)
0
K «' Cottinod Farticiiatt Ija)
*!»:
1 o.oooo
IS Csnctntrition (by CO)
t
12.1
CS2 Ccncwtration I Sy CD)
s
7.7
C3 Conrtntrilign (try 2*)
<
0
IB Corewt«ti<*i ISy olff. 1
t
< tt.20 )
&Mplt : Clock Vtlccitf (Hfict
: Stick
ia
wtr-
:S8r(S») (Plan MTR Mams TO SflWt£ » -
E09eB0S*0«T2
tend ! Tim dPiNrttr.dH
1 Taw
Tm
M*F)
! ;
: tan) : (in WC>! (in «ll
1 (d»jF)
in :
out
iMIocity Hnd Ccl
d9(av|) *
0.314
1 1 IS ) 0.32 ! Li
IK
10 !
70
I 0.3&57 :(Hfin Wr hading (*ic)
d"
'(a a»j) •
1U.0
~ : 15 1 M8 ! Li
IU
U2 ;
S5
1 0.3EJ7 1 («•( D
T<» «*{! •
7*,«
4 ! 15 ! 0.31 1 2.5
IU
120 :
100
: a. 55M :
3> IS ' 0.31 1 i.3
IU
IB 1
in
! 0.S3CI IIMar %artln (do; F)
Tla avjl •
106.S
2 : 13 : Mi : 2.3
Itf
12! :
us
: aati : uot o
T(a arg) •
*1.5
1 ! 15 : OlJI : 2.3 1 IU
130 :
197 1 I.3SI 1
»! 15 : 8.31 : e.3
jl III II III
S JL I J. i i 11 JL i JL
tot
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1312
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37.1
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Mid)
0.337
actual (acfa)
S(ai
2261
Hist Tote Correction Factor
C(e>
0.64
actatl lac*/tin) 9(a)
64.0
6a* Mar Comet ion Factor
(altfia)
1
Pptirclati LNdinti *7 (gr/tfacfl C(l atdl
0.0116
StKk tBctl DiMnaiora (in)i
1 7* Q21|r/«acfl C(a ltd)
0.0112
ladin (if round)
1
7
1 71 Slag/Ma
1 C(t tie)
Lanftti (if ractnfvlv)
I
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C(D)
0.130
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u
(k|yiir)
tie)
0.053
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0.312
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t
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29.9
Stack ftiaauia, afiaolata (in
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29.19
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Pittart)
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V(» (yf)
33.3
6u IWtir Initial ftaadi«if Icy ft)
70.074
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121.944
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via)
( 31.17 )
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~2 Csneantratton < By En t 12.1
B8 Concwfrrition (By CDl) i 7.7
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te Coneantration (by d:ff.) % ( 10.8) )
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3 I 0.3 ! S.46 ¦ 166 ! 119 I 16 I 0.3477 1
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(icfl
V(l ltd)
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(aai
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•
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(ncfil
B(a)
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rsc eve.
lO(a/asn)Bla)
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teula Diavtir, fctaal linl
Mfd>
OlB
actoil
(icfil
B(a)
•
3*se
Piiot 1m» ComEtisn fictar
Ctal
9.H
actual
(¦a/air) Bla)
•
H.9
So wtir Correction Factor
U1M>
0.S7
tvtlctlat* Ua«in|, try
Ifr/ewf) C(i (ttf)
¦
0.0064
Stick Ott) tipfim (in)i
1 7* K(r/*cf) C<» »M>
¦
0.0091
Um (if rortl
1
1 71 Btq/oacml Cli its)
¦
21
Unjtii (if rtct«^ul«r)
L
20
tarticul«t( laiBion tata
(19/iWJ
E(a)
•
8.051
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V
12.25
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11.70134 )
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0.072
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1
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me)
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29. ra
Total Saoiiiq Tiaa tain)
(thcta)
( 110.00 )
m
N(»)
•
2191
lifowtrir »r»i»w* (in H(>
P(3)
X
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P(«)
•
a. 99
Slack *rnvn < if IfiD)
0(«t«*>
-o.oe
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V(« av|)
9
M.2
tu Mr- Initial feadinc of CcwiflM farticulata Ijal "Is) I 5.0590 I
H CotCTMritier toy CD) » 7.35
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(«ac C)
Uf F)
Ma| 0
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¦ 0.040
«*(•*}! • 1.150
T(» «rj) • 2000.0
Til «y?I • 1052.3
Tla tvfl • 132.0
T<« (vj) ¦ 55.1
oaten • Mta
TC^U
lfiO
o.fli : i.isoo t tooo.0 i ui.o
1210 I 0.2828
224
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* i •
Yi. 7
Suola lacnioM
(FTBBWO
Stirt/Stoa 'wi 0907-1157'
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vti its) ¦
ICC. ss
i«o)
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ma.
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Stack 8a Flaa, ltd nnd. «tcf»)
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€!9
(caie.)
ru eve. lam/ain/Qli) •
u.e
boclt DiBTttf,
Waal (in)
NIC)
0.52
actual tacfi)
B(a) •
m;i
Pitet 7us» Ca» Facta-
CIs)
0.M
actual (acWBin) B(t) •
M.9
i« *rttr Corrtetion Factor
Ulffta)
1.02
Partiealata Loading, try Ifr'fKf) C<« ltd ¦
0.0000
Stac* (>rt) 0i»
Him hiOi
# 71 Slp/Mcf) Cli »to) ¦
0.0000
Radio lif nxml)
R
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t 7» C2(^/en) Cla (tc) ¦
0
Lnjtl lif rtetaifuiar)
L
»
0«rtim!it« Emmoft Jata ilvirl
E(3)
0.000
Width (if TCtnfulir)
V
12.23
(k(/l»)
[(g) •
o.oco
(Ha of Staex Ik ft 1
Alt)
<1.70138 )
Stan Sii Hatir Vmr Prooorttor
B1 BO) •
0.070
• c' Stasia Ccmtt
•
1
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Rid) •
25.75
Tctal Sanling Tin (ltd)
it itta)
( 180.00 1
tot
*(»! •
au
larowtrie frwwr* 1 in Hj)
Bib)
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0
e Coienrrttton (by biff.)
*
( &3.S5 )
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ilaet
it% Mttr
:BWTldc)
riufi USt« M3fes SfiU'J. * -
mn <•«-)
O'(trg) ¦
0.080
1 : 180
0.06 1 1.15
200C
: 138 : lis
! 0.2K8 iOrifiet «r toadii* c«e!
#• ta»?) •
1.156
o : o
0 : «
0
: 0 1 0
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—
i—
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1—
(OtQ CI
Tit avj) »
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T(» a*j) •
1(6.5
Ulf D
Tl» a*») •
S2.5
4——. '
II II IN II III
1 II 1 1 1 1 1 1 1 1 1
fart Waapt Camri s9 (*«)
SWT ISO) •
0.283
Wft_3 ! ISO
0.08 : 1.1500
noa.0
; 138.0 i 115.0
: t.tm
225
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cunurn doits ran m** ~ —
£032*Ssi>.5Tl
"uti C!F Uxitad 9/23/66
By i
II 09/29/86 Prin* 10/03/16
Twt ko. fjnt:
IOS290520WT1
Iieluraticity
» I ¦
10*. i
tall Locitiom SOUKS OTVET
Stnt/Stoe Tim
0920-11*1
aatm hnoit h> Vaina lief)
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lie.79
(lea)
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3.1M
WWEiHI
m
VOIJE
Stic* ia Floi. lie cane. (dacfu
Dial •
1221
lnle.1
rte cart, (daa/uniOli) *
J*.i
ttozzii Diaatir, Actual (in)
N(d)
0.357
actual «cM
3(1) ¦
2177
Pito*. Tut* Cerractiwi FiCtor
C(e)
O.S*
actual In/in; D(i) *
47.3
Em Mir Cmctien Victor
(alriu)
0.99
Pirtmltti LoallnQ, try lfr/llcfl Cli »M! *
1,0069
StKk Ortl Bivalent linli
1 71 izir/Mrfl Cli ita) ¦
0.0136
hots H' fount)
1
7
t 71 02laf/£ua>
Cli Bttfl •
SI
Lanfth (if rartrsular)
L
Ovtiralat* Salman fata tlb'M
E<») ¦
0.033
iiJtti (if fWtmtJlir)
M
—
(kf/V)
fill »
0.0*2
fcii of Stirt In ftl
nil)
11.06901
Sim iu Hatv Vigor Prooortiw
flao) •
0.330
• of Stall Point!
i
1
Poitcular wi|ht of Stic* hs, try
*IC) ¦
29.71
roUi Soolinf *i" («ir)
Ithtta)
1 136.00
m
«(•) •
25.1 J
fenatnr Nun tin H{)
»(M
30
Stm »rmr CD)
J
0
16 Ceiemfitior l&yiliff.)
»
I 79.S3 I
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i 122:
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Sttrt/Stoc Ifati
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via «ta)
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In)
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sma
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tenia Ititmttr, Act Ml (in)
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CL337
actual (acfi)
81*)
au
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C(a)
O.M
an oil (Ka/*in> fit)
87.8
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Ulpfia)
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laHieilata Loading try (fr/Ncf> Cli rtd)
c.oooo
Sack (Act) Dianiaa tin) i
t Tt K Cit ate)
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1
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1210
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14.3
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N(tf)
0.357
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Bla)
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C
0.64
actual (act/rinl (It)
64.8
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i
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0.C1SS
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tin)
0.373
1 of ShdIi toititt
1
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29.79
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1 60.00 )
fan
Mat
JS.37
laroa»tric (in N$)
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30
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1H.613
fits »«r- Final toaOinf (r ft)
179.539
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Via)
< 32.73 1
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V.lc)
63«.»l
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(a.afcj i
Wt. of filtr Particular Igi)
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( 0.0533 )
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11. B'
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1
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2.4i ;
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120 :
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129 :
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1
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Tl» a»fl • 74.4
T(( «v?) ¦ 1C15
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TBTBLS
hi }.io : a.soo : ise-o : i4i7.o : iou.c; 6.57T7
228
-------
APPENDIX D
VOST GC/FID ANALYSIS PROCEDURE
229
-------
c
Page 1 of 6
Revised 9-20-88
CRF Standard Operating Procedure
for Analyzing VOST Tubes
Apparatus
A. Thermal Desorption Unit
The thermal desorption unit for inside/inside VOST stainless steel
cartridges, (NuTech desorbtion unit with NuTech 320 controller) is
capable of thermally desorbing the sorbent resin tubes. It is
also capable of heating the tubes to 180* 10*C with flow of
interference-free nitrogen or helium through the tubes.
8. Puroe-and-Trao unit
The purge - and - trap unit (Tekmar) consists of three separate
pieces of equipment; the sample purger, trap, and the desorber.
It should be capable of meeting all requirements of Method 5030
(sw 846, 2nd Ed.) for analysis of purgeable organic compounds from
water.
C. GC/FID System
The Hewlett Packard 58S0A Series gas chromatograph is equipped
with a flame ionization detector (F.I.D.). The column used is a
fused silica capillary gas chromatographic column (D8-624 30m x
0.53mm I.D. x 3|iLm film thickness).
Procedure for Thermal Desorption of VOST Tubes
The VOST tubes are logged in the VOST record book when they are brought
into the lab, by tube number and sample identifier number. Then the
following steps are executed:
1. The caps are taken off the S.S. replica I/I glass design tubes
(fabricated locally and field tested at the CRF). Internal
standards(s) are added, typically 0.3yg of each compound in
methanol solution at O.img/al.
2. Reducing unions (1/4" to 1/18" SS) are placed on the tubes plus
1/16" connecting tubing.
3. The VOST tubes are connected to the NuTech carrier lines for
desorb gas flow 1n the opposite direction sample was taken, and
checked for tightness, while NuTech thermal desorption unit (TDU)
valve is in desorb position.
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Page 2 of 6
Revised 9-20-88
4. Then the VOST tubes are placed in the NuTech TDU and heated to
180*Ci 10*C with interference-free helium through the tubes at
40ml/min.
5. VOST tubes are desorbed and purged for fifteen (15) minutes
through the sparger onto the Tekmar chemical trap.
6. When the Tekmar reaches the desorb cycle the NuTech TDU valve is
switched to the vent position and allowed to vent for forty five
(45) minutes at 100 ml/min for cleaning purposes. Hater in the
sparger is drawn off, discarded, and replaced with 5.0s>l of fresh
cold tap water.
7. During desorbtion and cleaning period, samples are being analyzed -
by FID GC, and the fresh water in the sparger is being pre-purged
in preparation for the next analytical run.
3. Apparatus Setooints
A. Thermal Desportion Unit (NuTech with 320 NuTech controller)
The thermal desorption unit consist of three main heating zones; the
valve, lines, and desorber, all of which are maintained at 180*C+ 10*C.
There is a helium flow of 40 ml/min when in desorb cycle and flow of 100
rnl/min when in vent cycle.
B. Tekmar Purge and Trap Unit
The purge and trap consists of a series of automatic steps.
1. Standby - During this step the Tekmar chemical trap is allowed
to cool to 30*C.
2. Purge ready - The Tekmar chemical trap at 30*C is ready to start
purge of the VOST tubes in the thermal desorption
unit onto the Tekmar chemical trap.
3. Purge - During this cycle, the VOST tubes are purged for
fifteen (15) minutes with 40 ml/min of helium gas
through the sparger, onto the Tekmar chemical trap.
The purger or sparger holds five mis of
interference-free water.
4. Desorb preheat - The Tekmar chemical trap is preheated to 100*C,
taking about fifteen seconds to reach temperature.
5. Desorb
For four minutes at 180*C the Tekmar trap is
desorbed onto the G.C. column with flow rate of 5
mls/min of organic free helium.
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Pag* 3 of 6
Revised 9-20-86
6. Bake - For seven ainutes at 21S*C and -0 als/min the Tekmar
cheaical trap is vented out the back of the Tekaar for
cleaning purposes.
C. GC/FID Svstea
Gas chronatograph: The Hewlett Packard 5880 series chronatograph
is temperature prograaaed to separate the analytes which are
quantitated with a flame ionization detector (240*C) using
Multilevel external standardization (ESTD). Oven temperature is
held at 3S*C for six ainutes, then increased to 140*C at 4*C/ain,
then held for ten ainutes. Interference-free helium carrier gas
is set at 5 mls/min. Prior to analysis, every sample is spiked
with internal standard and surrogate compounds'. These conpounds
nay simulate the behavior of conpounds of interest and confirm
that acceptable recoveries are being achieved on every sample.
The results of internal standards and surrogate recoveries (%) are
reported with the sample results.
i. External Standard Calibration Procedure
For all analytes of interest, e.g. Table i, prepare calibration
standards at a minimum of three (3) concentration levels by making
appropriate dilutions of a stock standard at methanol. The
concentration levels might be, e.g. 3.0, 0.3, and .03 total mq per 3 Mi-
injected.
Each calibration standard is injected onto the exit end of the VOST
tubes {3pL injection}, 0.5mL of water is added in an effort to mimic
flue gas samples, and the analysis is conducted normally. Tabulate
response factor against amount injected for each target analyte.
Mass injected (uq)
Response factor ¦ Peak height
1} The ratio of amount injected (yg) to response (PkHt) is defined as
the response factor RF, which is calculated for each analyte at
each standard concentration. If the percent relative standard
deviation (*RSD) of the response factors for each analyte,internal
standard, and surrogate is less than 20% over the working range,
linearity can be assuaed. If linearity cannot be established,
racalibration at three levels aust be perforaed.
2) The working response factors aust be verified on each working day
by the analysis of one or aore calibration standards.
response factor for any target analyte varies from the predicted
response factor by aore than ~ 30%, the systea aust be
recalibrated at that level.
Percent Difference R1 X 100
Where: P.; . Response factor from preceeding analysis
R2 * Response factor from succeeding analyses.
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Table 1
Compound
Abbrev.
11.1-Dichloroethylene
IHethylene Chloride
j t-1.Z-Dichloroethylene
|HEXANE
! 1, 1-0ichloroethane
|CHLOROFORM
11,1,1-Trichloroethane
iCarbon Tetrachloride
I BENZENE
11.2-Dichloroethane
|Tr i ch1oroethy1ene
. 11,2-Dichloropropane
Bromodichloromethane
;t-l,3-Dichloropropylene
|TOLUENE
!OCTANE
lc-1,3-Dichloropropylene
|l,1,2-Tr1chloroethane
[Tetrachloroethylene
|Ch1orobenzene
[Ethylbenzene
: BROMOFORM
;4-Bronofluorobenzene
|1,1,2,2-Tetrachloroethane
11.3-Dichlorobenzene
|1,4-Dichlorobenzene
j1,2-Dichlorobenzene
|1,1-OCEENE
|M/C
j t-1,2-OCEENE
|Hexane
11.1-OCEANE
(ChloroforB
|1,1.1-TCEANE
| CCL4
|8enzene
11.2-DCEANE
ICL3-EENE
11, 2-DCPRANE
(BOOM
j t-1,3-DCPENE
I Toluene
[Octane
IC-1,3-OCENE
11,1,2-TCEANE
ICL4-EENE
| CL-BZ
| Et-BZ
iBromoform
(4-BFB
|CL-EANE
|1/3-DCBZ
11,4-DCBZ
|1,2-OCBZ
233
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Page S of 6
Revised 9-20-88
Daily Performance Checks
1) Calibrate the system (midlevel standard) immediately prior to
conducting any analyses. A aidlevel standard aust also be
injected at the end of the analysis sequence. The response factor
for each analyte to be qgantitated aust not exceed 30k difference
when compared to the initial standard of the analysis sequence.
If this criteria is exceeded, inspect the G.C. systea to determine
the cause and perfora whatever Maintenance is necessary before
recalibrating and proceeding with subsequent sample analysis.
2) Verify retention time windows (update daily) for each analyte:
retention tiaes for daily calibration Bust be within * .08 Bin. of
prior calibration standards for all target analytes.
3) Tentative identification of an analyte occurs when a peak from a
sample falls within the daily retention tine window.
4) Validation of GC system qualitative performance: use the daily
retention time windows for each analyte to evaluate this
criterion.. If any of the standards falls outside its daily
retention time window, the system 1s out of control. Determine
the cause of the problem and correct the problem.
5. Quality Control
1) The quality control program consist of an initial demonstration of
laboratory capability and an ongoing analysis of VOST field spike
tube pairs, to evaluate and document data quality. The laboratory
will maintain records to document the quality of the data
generated. Ongoing data quality checks are compared with
established performance criteria to determine if the results of
analyses meet the DQO of the applicable burn series test plan for
analytes of interest as well as surrogate and internal standard
compounds. When results of field spikes indicate atypical method
performance, a quality control check standard (Supelco) must be
analyzed to confirm that the measurements were performed in an
in-control mode of operation.
2) Before processing any samples, the analyst should demonstrate
through the analysis of VOST tubes, that interferences from the
analytical system, glassware, SS VOST tubes, and OFW are under
control. Blank samples should be treated in the same manner as
samples.
3) Consistent with the applicable burn series test plan/QAPP, for
each analytical batch, (up to 20 samples) a blank, field spike
and a field spike duplicate aust be analyzed. The blank and
spiked samples must be carried through all stages of analysis.
Field spike solutions will be prepared independently of
calibration standards as dictated by the applicable test
plan/QAPP.
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Page 6 of 6
Revised 9-20-88
4) The experience of the analyst performing gas chromatography is
invaluable to the success of the analysis. Each day that analysis
is performed, the daily calibration sample should be evaluated to
determine if the chromatographic system is operating properly.
Questions that should be asked are: Do the peaks look nonaal?; Is
the response obtained comparable to the response froa previous
calibrations?
Careful examination of the standards chroaatograa can indicate
whether the eoluan is still good, the desorbtion lines are
leaking, 6 port valve clogged, etc... If any aajor changes are
aade to the analytical systea (e.g. eoluan changed), rectiibretion
of the systea aust take place.
Reouired Instrument PC
1) Require that the t RSD vary by <20* when comparing calibration
factors to determine if the 3 point calibration is linear*.
2) + 30* difference when comparing daily response of a-given analyte
versus the initial response. If the limit is exceeded, yo« aust
recalibrate.
3) Establishment of retention time windows, and that all succeeding
standards in an analysis sequence must fall within the .-daily
retention time window established by the first standard of the
sequence.
To establish the ability to generate acceptable accuracy and precision,
the analyst must perform the following operation.
1) A quality (QC) check sample concentrate is required cdntaiming
each analyte of interest. The QC check sample concentrate may be
prepared from pure standard materials or purchased as certified
solutions.
If prepared by the laboratory, the QC check sanple concentrate
must be aade using stock standards prepared independently froa
those used for calibration.
The concentration of the QC check sample concentrate is highly
dependent upon the analytes being investigated. Prior to any
analysis each pair of VOST tubes will be spiked with A/10 ISTD
(0.3pg) of nonane and deeane. Prior to any saaple being taken
each pair of
VOST tube will be spiked with 2 surrogate standards
(4-Bromofluorobenzene and Octane).
Analysis of purgeable compounds in samples other than VOST, e.g.,
scrubber blowdown water, bottom ash, and primary waste feed; is
accomplished using the PST/GC-FIO methods of this SOP coupled with
sample preparation techniques found in Method S030, SM 846-Test
Methods for Evaluating Solid Haste, 3rd Ed., November 1986.
235
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TECHNICAL REPORT OAT A
(Fleas* rrtJ lintrucnofi cm the n\tne btfert eomfile
1 REPORT NO J.
EPA/600/2 - 90/04 3b
3
«. title *no subtitle
The Fate of Trace Petals
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