ฃ?k - oi A"
MONITORING TO DETECT
PREVIOUSLY UNRECOGNIZED POLLUTANTS
IN SURFACE WATERS
APPENDIX
# ** \
I SIS I
% pRo^&
-------
r
TECHNICAL REPORT DATA
ฆ' .-k rcjj lAiWjetio-;! or. th< rrwnc b.-fore ionphn>ii:!
1.RM'CซT\C.
EPA-560/6-77-015A
i. T T ^ c A i\ i - a i * :
Monitoring to Detect Previously Unrecognized
Pollutants in Surface Waters--Appendix: Organic
Analysis Data
3. RL'CIPIfcNT'S ACCfcSS.Ot*NO.
5 REPORT DATE
July 1977
7 AUTHOR'S''
B. B. Ewing, E.S.K. Chian, J. C. Cook, C. A. Evans,
P. K. Hopke, E. G. Perkins, and J. C. Means
6 PERFORMING ORGANIZATION CODE
8. PERFORMING ORGAN 2ATION REPORT NO
a. *'ERtORMIN3 OW.-jANI2AT(ON NAVF AP.D ADDRESS
Institute for Environmental Studies
408 S. Goodwin Avenue
University of Illinois at Urbana-Champaign
JJrbana ,_I VM noi s_ 61801
1 2. 3ฐDN5L'H: \'G AGE NH NAME AND ACDRESa
United States Environmental Protection Agency
Office of Toxic Substances
Washington, D. C. 20460
15 SJf^LฃMfc\TARV NOTES
tO. PROGRAV ELEMENT NO.
11. CONTRACT/GRANT NO.
EPA 68-01-3234
13. TYPF OF REPORT AND PERIOD COVERED
Appendix to final report.
14 SPONSORING AGENCY CODE
'j c ' ฆ
ig. abstract
Samples of surface waters were collected from 204 sites near heavily industrialized
areas across the United States. The samples were analyzed for all contaminants
present at concentrations greater than one part per billion. Each water sample
was preconcentrated for analysis of organics in three fractions: volatile
organics by nitrogen-gas stripping and the less-volatile organics by extraction
with chloroform under both basic and acidic conditions. Organic constituents
were identified by gas chromatography/mass spectrometry and quantified by gas-
chronatographic techniques. Inorganic constituents were determined by spark-
source mass spectrometry, energy-dispersive x-ray fluorescence analysis, and
instrumental neutron activation analysis. For comparison with previous data from
the same sites, the samples were also analyzed for total chemical oxygen demand,
turbidity, conductivity, pH, color, oxidation-reduction potential, suspended
solids, and volatile suspended solids. Results of the inorganic analyses were
presented in previous quarterly progress reports. Final results of the organic
analyses are presented in this appendix to the final report.
KE Y WORDS AND DOvUPv'iCNT ANAw^ s s
d. DESCRIPTORS
DฃNTiPiERS'OPfc\ ENDED TERMS
Water quality
Trace contaminants
Water oollution
Organic compounds
Water analysis
Volatile organic
Water chemistry
compounds
Surface waters
Industrial pollution
Nationwide survey
?. D 1ST R I BU"*" ON STATEMENT
Unrestricted
Available from National Technical Infor-
mat.inn SPrvir.P. .Springfield. VA 7P1R1
COSATi I leld/Crijiip
8h
7b, 7c, 7e
119 EECURITY CLASS ,This Rtport)
Unclassified
?G. SECURITY CLASS fJili.t page)
Unclassified
AGES
KW -f\e \
EPA Form 2220-1 (3-73)
-------
EPA-560/6-77-0j.5.4
MONITORING TO DETECT PREVIOUSLY UNRECOGNIZED
POLLUTANTS IN SURFACE WATERS
APPENDIX: ORGANIC ANALYSIS DATA
INSTITUTE FOR ENVIRONMENTAL STUDIES
University of Illinois at Urbana-Champaign
Final Report
Contract No. 68-01-3234
July 1977
Project OfficerVincent J. DeCarlo
Prepared for
Office of Toxic Substances
U.S. Environmental Protection Agency
Washington, D.C. 20460
Document is available to the public through the National Technical Information
Service, Springfield, Virginia 22151
B. B. Ewing Principal
E. S. K. Chian Investigators
J. C. Cook
F. B. DeWalle
C. A. Evans
P. K. Hopke
J. H. Kim
E. G. Perkins
J. D. Sherwood
W. H. Wadlin
J. C. Means
Pv. Mil berg
)~CL,
-------
NOTICE
This report has been reviewed by the Office of Toxic Substances, EPA,
and approved for publication. Approval does not signify that the contents
necessarily reflect the views and policies of the Environmental Protection
Agency, nor does mention of trade names or commercial products constitute
endorsement or recommendation for use.
-------
1
TABLE B1
Organic Compounds Identified in Sample #1S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1 Dichloromethane 1
2 Acetone 2
3 Chloroform 30
4 Trichloro-trifluoroethane 5
5 Trichloroethylene 4
6 Benzene 3
7 Tetrachloroethylene 2
8 Toluene 2
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
10
1
5
9
12
8
2
45
4
4
14
43
4
4
11
35
6
15
14
14
7
6
7
2
4
2
TABLE B2
Organic Compounds Identified in Sample if 1A
Relative
Retention
Time Compounds in Acid Extract
0.435 Methyl-2-ethyl Hexanoate (IS)
0.780 Fatty Acid Methyl Ester C = 12
0.792 Methyl Trichlorophenyl Ether
0.826 Methyl Tetrachlorophenyl Ether
0.893 Methyl Myristate
0.926 Fatty Acid Methyl Ester C >_ 14
0.954 Fatty Acid Methyl Ester C >_ 15
+ Methyl Pentachlorophenyl Ether
0.978 Fatty Acid Methyl Ester C >_ 15
1.000 Methyl Palmitate
1.049 Fatty Acid Methyl Ester C >_ 16
1.061 ?
1.088 Dibutyl Phthalate
1.095 Methyl Stearate
1.131 ?
1.143 Fatty Acid Methyl Ester C >_ 19
1.186 Fatty Acid Methyl Ester C >_ 20
1.216 ?
1.232 Fatty Acid Methyl Ester C >_ 22
1.265 Fatty Acid Methyl Ester C _> 22
1.323 Diethyl Hexyl Phthalate
1.348 ?
1.366 ?
1. 388 C,,- - Terpineol
1.403 ?
1.418 Fatty Acid Methyl Ester C 26
1.451 ?
-------
Peak
1
2
3
4
5
6
?ak #
1
2
3
4
5
6
7
8
9
10
11
3
TABLE B3
Organic Compounds Identified in Sample #1B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
Xylene 19
Dibromo-chloroethane 14
Camphor (IS)
Diisobutyl Phthalate 1
Dibutyl Phthalate 1
Terpineol 1
TABLE B4
Organic Compounds Identified in Sample # 2S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Acetone 2
Chloroform 5
Trichloro-trifluoroethane 2
Trichloroethane 1
Bromo-dichloromethane 9
Trichloroethylene 2
Benzene 4
Dibromo-chloromethane 2
Tetrachloroethylene 1
Fluoro-dichloro-bromomethane 1
Toluene 2
-------
4
TABLE B5
Organic Compounds Identified in Sample it 2A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1
0.467
Methyl-2-ethyl Hexanoate (IS)
2
0.899
Methyl Myristate
2
3
1.000
Methyl Palmitate
4
4
1.105
Methyl Stearate
2
5
1.319
Diethyl Hexyl Phthalate
1
6
1.386
Terpi neol
1
TABLE B6
Organic Compounds Identified in Sample *2B
Relative
Retention Approximate
Peak H Time Compounds in Base Extract Level (PPB)
1 Tetrachloroethane 2
2 1,2-Diethoxyethane 2
3 Camphor (IS)
4 Terpineol 2
-------
Peak
1
2
3
4
5
6
7
8
9
10
11
5
TABLE B7
Organic Compounds Identified in Sample #3S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 1
Acetone 3
Trichloro-fluoromethane 6
Chloroform 8
Trifluoro-trichloroethane 3
Butane 6
Trichloroethylene 4
Benzene 2
Tetrachloroethylene 1
Toluene 1
Chlorobenzene 1
-------
6
TABLE B8
Organic Compounds Identified in Sample # 3A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1
0.519
Methyl-2-ethyl Hexanoate (IS)
--
2
1.000
Methyl Palmitate
3
3
1.055
?
3
4
1.085
Dibutyl Phthalate
1
5
1.091
Methyl Stearate
3
6
1.131
?
2
7
1.167
?
1
8
1.179
Fatty Acid Methyl Ester C ^ 20
2
9
1.213
9
10
1.262
?
2
11
1.319
Diethyl Hexyl Phthalate
6
12
1.349
?
2
13
1.365
?
3
14
1 .402
1
3
TABLE B9
Organic Compounds Identified in Sample if 3B
Relative
Retention Approximate
Peak if Time Compounds in Base Extract Level (PPB)
1 Tetrachloroethylene 2
2 Diethoxyethane 3
3 Dichlorobenzene 4
4 Camphor (IS)
5 --- ? i
-------
1
2
3
4
5
6
7
8
9
10
n
#
7
TABLE BIO
Organic Compounds Identified in Sample ง 4S
Relative
Retention
Time
Volatile Compounds
Approximate
Level (PPB)
Dichloromethane
Acetone
Trichlorofluoromethane
Chloroform
Tri chloro-trifl uoroethane
Pentane
Trichloroethane
Trichloroethylene
Benzene
Tetrachloroethylene
Toluene
2
3
6
9
3
2
1
2
1
1
1
TABLE Bll
Organic Compounds Identified in Sample # 4A
Rel ative
Retention
Time
Compounds in Acid Extract
Approximate
Level (PPB)
Sample 4A was destroyed and no quantitative data or
chromatogram is available.
-------
Peak
1
2
3
4
5
ak #
1
2
3
4
5
6
7
8
9
10
11
12
8
TABLE B12
Organic Compounds Identified in Sample # 4B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
Tetrachloroethylene
Camphor (IS)
Naphthalene (IS)
Unidentified Phthalate
Terpineol
11.3
3
1
TABLE B13
Organic Compounds Identified in Sample ง 5S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 2
Acetone 2
Tetrahydrofuran 1
Chloroform 100
Tri fl uoro-trichloroethane 1
Trichloroethane 1
Trichloroethylene 6
Benzene 2
Hexane 1
Tetrachloroethylene 4
Toluene 1
Chlorobenzene 1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
9
TABLE B14
Organic Compounds Identified in Sample ง 5A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.444
Methyl-2-ethyl Hexanoate (IS)
--
0.559
Camphor
8
0.894
Methyl Myristate
2
0.927
Fatty Acid Methyl Ester C >_ 14
1
0.951
Methyl Pentachlorophenyl Ether
2
1.000
Methyl Palmitate
12
1 .036
Hydrocarbon C 18
1
1.058
?
4
1.097
Methyl Stearate
9
1.182
Fatty Acid Methyl Ester C > 20
2
1.219
?
18
1.265
Fatty Acid Methyl Ester C >_ 22
5
1.326
Diethyl Hexyl Phthalate
8
1.349
?
8
1.365
?
7
1.386
?
1
1.402
?
2
1.419
?
2
1.453
1
2
-------
Peak
1
2
3
4
5
6
?ak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
10
TABLE B15
Organic Compounds Identified in Sample # 5B
Relative
Retention
Time
Compounds in Base Extract
Approximate
Level (PPB)
Tetrachloroethylene
Diethoxyethane
Camphor (IS)
2
4
Diethyl-Hexyl Phthalate
Terpineol
TABLE B16
Organic Compounds Identified in Sample # 6S
Relative
Retention
Time
Volatile Compounds
Approximate
Level (PPB)
Dichloromethane
Acetone
Tetrahydrofuran
Chloroform
Dioxane
Pentane
Trichloroethylene
Benzene
Hexane
Diisopropyl Ether
Tetrachloroethylene
Toluene
Ethylbenzene
Dichlorobenzene
2
4
1
1
1
1
6
2
1
1
4
2
1
1
-------
Peak ;
1
2
3
4
5
6
7
8
9
10
11
12
13
14
Peak
1
2
3
4
5
6
11
TABLE B17
Organic Compounds Identified in Sample # 6A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.463
Methyl-2-ethyl Hexanoate (IS)
__
0.791
Fatty Acid Methyl Ester C = 12
1
0.878
Fatty Acid Methyl Ester C > 13
1
0.900
Fatty Acid Methyl Ester C = 14
1
0.933
Fatty Acid Methyl Ester C > 14
2
0.955
Methyl Pentachlorophenyl Ether
1
1.000
Methyl Palmitate
10
1.060
7
2
1.097
Methyl Stearate
8
1.184
Fatty Acid Methyl Ester C 20
1
1.218
Fatty Acid Methyl Ester C > 21
6
1.264
Fatty Acid Methyl Ester C >_ 22
1
1.318
Diethyl Hexyl Phthalate
1
1.342
Fatty Acid Methyl Ester C > 24
2
TABLE B18
Organic Compounds Identified in Sample # 6B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
Tetrachloroethylene 3
Diethoxyethane 5
Camphor (IS)
? 1
Diethyl Hexyl Phthalate 1
Terpineol 4
-------
ak
1
2
3
4
5
6
7
8
9
10
n
12
13
14
15
16
17
18
19
20
21
12
TABLE B19
Organic Compounds Identified in Sample #7S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
? 1
Dichloromethane 30
Acetone 2
Butene 2
Trichloro-trif1uoroethane 30
Dichloroethylene 2
Cyclopentane 4
Tetrahydrofuran T
Diethyl Ether 5
Chloroform 30
Pentane 9
Hexene 5
Trichloroethylene 10
Benzene 7
Hexane 10
Tetrachloroethylene 1
Toluene 5
Acetophenone 2
Chiorobenzene 2
Nonene 1
Ethylbenzene 4
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
13
TABLE B20
Organic Compounds Identified in Sample # 7A
Relative
Retention
Time
0.558
0.766
0.851
0.919
0.962
1.000
1.049
1.081
1.143
1.151
1.177
1.210
1.215
1.239
1.270
1.332
1.365
1.386
Compounds in Acid Extract
Approximate
Level (PPB)
Methyl
C10 "
Methyl
Methyl
Methyl
Methyl
?
Methyl
?
-2-ethyl Hexanoate (IS)
Terpineol
-2(4-chlorophenoxy) Butanoate
Myri state
Pentachlorophenyl Ether
Palmitate
Stearate
Fatty Acid Methyl Ester C > 20
Fatty Acid Methyl Ester C > 22
Butyl benzyl Phthalate
Diethyl Hexyl Phthalate
Fatty Acid Methyl Ester C > 24
?
1
1
1
3
5
5
II
1
1
11
2
2
2
2
1
1
1
TABLE B21
Organic Compounds Identified in Sample if 7B
Relative
Retention
Time
Compounds in Base Extract
Approximate
Level (PPB)
1.000
1.180
Naphthalene (IS)
?
-------
1
2
3
4
5
6
7
8
9
10
n
#
14
TABLE B22
Organic Compounds Identified in Sample #8S (Field Stripped)
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane
2
Acetone
2
Trichlorofluoromethane
4
Chloroform
6
Pentane
6
Bromo-dichloromethane
4
Trichloroethylene
2
Benzene
2
Hexane
5
Toluene
1
Chlorobenzene
1
TABLE B23
Organic Compounds Identified in Sample #8A (Field Extracted)
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.560 Methyl-2-ethyl Hexanoate (IS)
-------
Pe
ak
1
2
*-ป
o
4
5
6
7
8
9
10
11
12
13
14
15
15
TABLE B24
Organic Compounds Identified in Sample ir8B (Field Extracted)
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000 Naphthalene (IS)
TABLE B25
Organic Compounds Identified in Sample $8S (Lab Stripped)
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Di chloromethane
3
Acetone
1
Butene
1
Tri chloro-f1uoromethane
3
Chloroform
10
Pentane
1
ฆ ?
1
?
1
Bromo-di chloromethane
7
Hexane
4
Benzene
6
Dibromo-chloromethane
3
Methyl Methacrylate
10
Furfural
2
Toluene
1
Chlorobenzene
4
-------
16
TABLE B26
Organic Compounds Identified in Sample # 8A (Lab Extracted)
Relative
Retention
Approximate
Peak #
Time
Compounds in Acid Extract
Level (PPB)
1
0.560
Methyl-2-ethyl Hexanoate (IS)
TABLE B27
Organic Compounds Identified in Sample P 8B (Lab Extracted)
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1
1.000
Naphthalene (IS)
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
17
TABLE B28
Organic Compounds Identified in Sample # 9S (Field Stripped)
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane
5
Acetone
4
Butene
1
Tri chloro-f1uoromethane
20
Dichloroethylene
1
Pentene Isomer
1
Tetrahydrofuran
1
Chloroform
20
Dichloroethane
1
Pentene Isomer
9
Trichloroethane
1
Pentane
2
Tri chloroethylene
5
Benzene
2
Hexane
12
Methyl-isobutyl Ketone
1
Tetrachloroethylene
1
To1uene
2
Ethyl benzene
1
-------
k #
1
2
3
4
5
6
7
8
9
0
1
2
3
'eak
1
2
3
4
5
6
7
8
9
18
TABLE B29
Organic Compounds Identified in Sample #9A (Field Extracted)
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.556 Methyl-2-ethyl Hexanoate (IS)
0.854 Methyl-2(4-chlorophenoxy) Butanoate 1
0.911 Methyl Myristate 2
1.000 Methyl Palmitate 6
1.048 ? 2
1.081 Methyl Stearate 10
1.104 Hydrocarbon C > 20 1
1.149 Hydrocarbon C >_ 22 1
1.176 ? 11
1.208 Fatty Acid Methyl Ester C >_ 22 2
1.258 Diethyl Hexyl Phthalate 3
1.277 Fatty Acid Methyl Ester C > 24 6
1.312 ^15 " Terpineol ฎ
TABLE B30
Organic Compounds Identified in Sample #9B (Field Extracted)
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
0.830 Dichlorobenzene Isomer 1
1.000 Naphthalene (IS)
1.106 Alkyl Acid Ester (R + R' >8) 1
1 .277 Cio ~ Terpineol 1
1.523 ? 4
1.583 Dibutyl Phthalate 4
1.602 Caffeine 4
1.852 Diethyl Hexyl Phthalate 3
1.924 C - Terpineol 3
15
-------
1
1
3
4
5
6
7
8
9
10
n
12
13
14
15
16
19
TABLE B31
Organic Compounds Identified in Sample # 9S (Lab Stripped)
Relati ve
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane
8
Acetone
4
Trichlorofluoromethane
20
Pentene
1
Tetrahydrofuran
1
Diethyl Ether
3
Chloroform
20
Pentane
10
Trichloroethane
1
Hexene
2
Trichloroethylene
4
Benzene
1
Hexane
10
Tetrachloroethylene
1
Toluene
2
Ethyl Benzene
2
-------
?ak ง
1
2
3
4
5
6
7
8
9
10
11
12
13
Peak
1
2
3
4
5
6
7
8
20
TABLE B32
Organic Compounds Identified in Sample # 9A (Lab Extracted)
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.558
Methyl-2-ethyl Hexanoate (IS)
__
0.850
Methyl-2(4-chlorophenoxy) Butanoate
1
0.911
Methyl Myristate
2
1.000
Methyl Palmitate
13
1.035
?
2
1.081
Methyl Stearate
19
1.149
Hydrocarbon C > 22
1
1.176
?
11
1.208
Fatty Acid Methyl Ester C 1 22
2
1.240
Butylbenzyl Phthalate
4
1.250
Diethyl Hexyl Phthalate
18
1.277
Fatty Acid Methyl Ester C l 24
6
1.312
C-|5 ~ Terpineol
9
TABLE B33
Organic Compounds Identified in Sample #9B (Lab Extracted)
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
0.830 Dichlorobenzene 1
1.000 Naphthalene (IS)
1.113 Alkyl Acid Ester (R + R" >_8) 1
1.522 ? 4
1.583 Dibutyl Phthalate 4
1.603 Caffeine 4
1-855 Diethyl Hexyl Phthalate 2
1.922 ^15 " Terpineol 2
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
21
TABLE B34
Organic Compounds Identified in Sample #1 OS
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 15
Acetone 6
Butene 1
Trichloro-fluoromethane 20
Dichloroethylene 1
Pentene 1
Tetrahydrofuran 6
Diethyl Ether 8
Chloroform 20
Trifluoro-trichloroethane 1
Dichloroethane 1
Pentane 10
Trichloroethane 8
Dioxane 1
Hexene 2
Dichloropropane 2
Trichloroethylene 10
Benzene 2
Dibromo-chloromethane 1
Hexane 12
Tetrachloroethylene 4
Toluene 2
Chlorobenzene 1
Ethyl benzene 1
-------
ak
1
2
3
4
5
6
7
8
9
10
11
22
TABLE B35
Organic Compounds Identified in Sample # 10A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.545 Methyl-2-ethyl Hexanoate (IS)
0.916 Methyl Myristate 6
1,000 Methyl Palmitate 104
1.040 Fatty Acid Methyl Ester C >_16 7
1.050 ? 15
1.080 Methyl Stearate 180
1.150 Fatty Acid Methyl Ester C ^ 18 23
1.170 ? 28
1.210 Fatty Acid Methyl Ester C ^ 20 8
1.260 Diethyl Hexyl Phthalate 7
1.318 C]5 - Terpineol 8
TABLE B36
Organic Compounds Identified in Sample #10B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000 Naphthalene (IS)
-------
1
2
3
4
5
6
7
8
9
10
n
12
23
TABLE B37
Organic Compounds Identified in Sample #11S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane
8
Acetone
1
Tetrahydrofuran
1
Diethyl Ether
1
Chioroform
5
Dichloroethane
1
Tri chloroethane
4
Bromo-dichloromethane
1
Dichloropropane
1
Trichloroethylene
5
Benzene
1
Tetrachloroethylene
4
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
24
TABLE B38
Organic Compounds Identified in Sample #11A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.590 Methyl-2-ethyl Hexanoate (IS)
0.833 Fatty Acid Methyl Ester C = 12 22
0.840 Methyl Trichlorophenyl Ether 14
0.850 Methyl-2-(4-chlorophenoxy) Butanoate 11
0.919 Methyl Myristate 24
0.960 Fatty Acid Methyl Ester C > 14
+ Methyl Pentachlorophenoxy Ether 24 (mix)
1.000 Methyl Palmitate 94
1.030 Fatty Acid Methyl Ester C >_ 16 12
1.045 ? 26
1.077 Methyl Stearate 131
1.113 Fatty Acid Methyl Ester C >_ 18 10
1.146 Methyl Arachidate 27
1.170 ? 49
1.208 Fatty Acid Methyl Ester C >_ 20 32
1.253 Diethyl Hexyl Phthalate 23
1.274 ? 25
1.289 ? 17
1.307 C-j5 Terpineol 21
TABLE B39
Organic Compounds Identified in Sample # 11B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000
1.862
Naphthalene (IS)
Diethyl Hexyl Phthalate
1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
25
TABLE B40
Organic Compounds Identified in Sample #12S (Nonchlorinated)
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 3
Acetone 1
Butene 3
Trichloro-fluoromethane 5
Dichloroethylene 1
Tetrahydrofuran 3
Diethyl Ether 10
Chloroform 20
Pentane 6
Trichloroethane 4
Dioxane 1
Tetrahydropyran 9
Trichloroethylene 4
Benzene 1
C5Hg0 or C6H]20 10
Methyl-tetrahydropyran 2
C5H10ฐ 0r C6H12ฐ 4
Tetrachloroethylene 5
Toluene 1
Acetophenone 1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
26
TABLE B41
Organic Compounds Identified in Sample #12S (Chlorinated)
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 3
Acetone 2
Butene 5
Trichloro-fluoromethane 4
Dichloroethylene 1
Tetrahydrofuran 4
Diethyl Ether 10
Chloroform 14
? 1
Pentane 2
Trichloroethane 6
Dioxane 2
Tetrahydropyran 9
Trichloroethylene 4
Benzene 2
Dimethylformamide 2
C5H8ฐ or C6H12ฐ 14
Methyl-tetrahydropyran 4
C5H10ฐ or C6H12ฐ 6
N,N-Dimethylacetamide 2
Tetrachloroethylene 4
Dichlorobenzene Isomer 2
Dichlorobenzene Isomer 2
-------
Peak
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
27
TABLE B42
Organic Compounds Identified in Sample # 12A
Relative
Retention
Time
Compounds in Acid Extract
Approximate
Level (PPB)
0.572
0.670
0.717
0.753
0.768
0.830
0.854
0.917
0.943
0.964
1.000
1.040
1.047
1.077
1.112
1 .137
1.148
1.175
1.208
Methyl-2-ethyl Hexanoate (IS)
Methyl Dichlorophenyl Ether
?
Methyl Trichlorophenyl Ether
C-jq - Terpineol
Fatty Acid Methyl Ester C = 12
Methyl-2-(4-chlorophenoxy) Butanoate
Methyl Myristate
Fatty Acid Methyl Ester C >_ 14
Methyl Pentachlorophenyl Ether
Methyl Palmitate
Fatty Acid Methyl Ester C >_ 16
1
Methyl Stearate
?
?
Methyl Arachidate
?
Fatty Acid Methyl Ester C >_ 22
+ Methyl Dehydroabietate
5
8
10
15
4
4
18
31
26
117
19
27
173
24
23
25
60
90 (mix)
1.261
Diethyl Hexyl Phthalate
137
1.277
?
50
1.294
?
68
1.312
50
1.324
1
52
1.335
1
68
-------
1
2
3
4
5
6
7
8
9
#
28
TABLE B43
Organic Compounds Identified in Sample # 12B
Relative
Retention Approximate
11me Compounds in Base Extract Level (PPB)
0.810 Dichlorobenzene 16
1-000 Naphthalene (IS)
1-103 Alkyl Acid Ester (R + R' >_ 8) 2
1-620 Caffeine i
1.699 ? 9
1.754 ? 4
1.830 ? 2
1-873 Diethyl Hexyl Phthalate 1
1-952 C^ - Terpineol 1
TABLE B44
Organic Compounds Identified in Sample # 13S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Chloroform 8
Bromo-dichloromethane 4
Trichloroethylene 2
Benzene 3
Chiorobenzene 1
-------
29
TABLE B45
Organic Compounds Identified in Sample ฃ13A
Peak #
Relative
Retention
Time
Compounds in Acid Extract
Approximate
Level (PPB)
1
0.545
Methyl-2-ethyl Hexanoate (IS)
_ ^ _
2
1.000
Methyl Palmitate
1
3
1. 263
Diethyl Hexyl Phthalate
1
4
1.320
C-|^ - Terpineol
1
TABLE B46
Organic Compounds Identified in Sample #13B
Peak #
Relative
Retention
Time
Compounds in Base Extract
Approximate
Level (PPB)
1 1.000 Naphthalene (IS)
-------
1
2
3
4
5
6
7
8
9
10
11
k #
1
2
3
4
5
6
7
8
9
0
1
2
30
TABLE B47
Organic Compounds Identified in Sample *> 14S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Trichloro-fluoromethane
1
Neopentane
2
Chioroform
1
Trichloroethane
2
Hexene Isomer
1
Hexene Isomer
1
1-Bromo-l-chloroethane
1
Benzene
1
Dibromoethane
10
Methyl-isobutyl Ketone
2
Heptene
1
TABLE B48
Organic Compounds Identified in Sample P 14A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.557
Methyl-2-ethyl Hexanoate (IS)
--
0.853
Hydrocarbon C > 16
2
0.902
Hydrocarbon C > 18
2
0.919
Fatty Acid Methyl Ester C >_ 14
2
0.940
Hydrocarbon C > 18
1
1.000
Methyl Palmitate
2
1.078
Methyl Stearate
5
1.138
c16Hio (Pyrene?)
1
1.260
Diethyl Hexyl Phthalate
1
1.293
(CigH^) Benzanthrene
1
1.423
?
8
1.447
?
8
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
31
TABLE B49
Organic Compounds Identified in Sample #14B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
0.474
Di bromoethane
6
1.000
Naphthalene (IS)
--
1.235
Hydrocarbon C >_ 16
1
1.270
Hydrocarbon C >_ 16
1
1.346
Hydrocarbon C >_ 18
1
1 .625
Caffeine
2
1.657
Hydrocarbon C ^ 22
1
1.708
Hydrocarbon C >_ 22
1
1.741
C16H10 (pyrene)
1
1.856
Benzyl butyl Phthalate
1
1.887
Diethyl Hexyl Phthalate
4
1.944
Hydrocarbon C ;> 28
1
1.968
Terpineol
4
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
k #
1
2
3
4
5
32
TABLE B50
Organic Compounds Identified in Sample # 15S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane 1
Acetone 1
Trichloro-fl uorornethane 1
Dichloroethylene 2
Chloroform 1
Pentane 1
Dichloroethane 6
Trichloroethane 1
Hexene 4
Trichloroethylene 6
Benzene 2
Tetrachloroethylene 3
Chiorobenzene 1
TABLE B51
Organic Compounds Identified in Sample i 15A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.575 Methyl-2-ethyl Hexanoate (IS)
1.000 Methyl Palmitate 1
1-060 Methyl Stearate 1
1.250 Diethyl Hexyl Phthalate 5
1.300 C-jg - Terpineol 4
-------
Pe;
ak
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
33
TABLE B52
Organic Compounds Identified in Sample # 15B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1-000 Naphthalene (IS)
TABLE B53
Organic Compounds Identified in Sample #16S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
Dichloromethane
2
Acetone
1
Butene
1
Trichloro-fluoromethane
12
Dichloroethylene
2
Diethyl Ether
5
Chloroform
20
Pentane
8
Tetrahydropyran
3
Trichloroethylene
5
Benzene
4
Hexane
10
Tetrachloroethylene
4
Toluene
2
Chlorobenzene
1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
34
TABLE B54
Organic Compounds Identified in Sample # 16A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.579 Methyl-2-ethyl Hexanoate (IS)
0.770 C^g - Terpineol 10
0.850 Hydrocarbon C > 18
+ Methyl-2(4-chlorophenoxy) Butanoate 10 (mix)
0.900 Fatty Acid Methyl Ester C ^ 14 21
0.920 Fatty Acid Methyl Ester C > 14 20
0.960 Fatty Acid Methyl Ester C >_ 14
+ Methyl Pentachlorophenyl Ether 25 (mix.)
1.000 Methyl Palmitate 70
1.040 Fatty Acid Methyl Ester C >. 16 9
1.044 ? 29
1.070 Methyl Stearate 79
1.140 Fatty Acid Methyl Ester C >_ 18 34
1.170 ? 85
1.210 Fatty Acid Methyl Ester C > 20 33
1.250 Diethyl Hexyl Phthalate 50
1.257 ? 25
1.270 ? 35
1.280 ? 25
1.300 ? 30
1.320 ? 43
1.330 ? 41
-------
Peak
1
2
3
4
5
6
7
8
?ak H
1
2
35
TABLE B55
Organic Compounds Identified in Sample # 16B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
0.811
Di chlorobenzene
18
1.000
Naphthalene (IS)
--
1.102
^10 " TerP"'neo''
1
1.429
Dimethyl Biphenyl
1
1.594
Dibutyl Phthalate
1
1.618
Caffeine
1
1.873
Diethyl Hexyl Phthalate
1
1.952
C - Terpineol
15
1
TABLE B56
Organic Compounds Identified in Sample # 17S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
0.548 Dichloromethane 1
1.000 Chioroform 2
-------
1
2
3
4
5
6
?
8
9
10
11
12
13
14
15
16
36
TABLE B57
Organic Compounds Identified in Sample # 17A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.563
Methyl-2-ethyl Hexanoate (IS)
--
0.739
Methyl Trichlorophenyl Ether
12
0,763
C-|q - Terpineol
10
0.846
Methyl-2(4-chlorophenoxy) Butanoate
10
0.913
Fatty Acid Methyl Ester C = 14
7
1.959
Methyl Pentachlorophenyl Ether
43
1.000
Methyl Palmitate
81
1.062
?
10
1.075
Methyl Stearate
45
1.113
?
55
1.175
?
45
1.207
Methyl Dehydroabietate
37
1.213
Butylphthaiy1 butyl Glycol ate
48
1.261
Diethyl Hexyl Phthalate
85
1.277
Fatty Acid Methyl Ester C > 24
52
1.312
C-|g - Terpineol
104
-------
Peak
1
2
3
4
5
6
7
8
ik #
1
2
3
4
37
TABLE B58
Organic Compounds Identified in Sample # 17B
Relative
Retention Approximate
Time Compounds in Base Extract Level {PPB)
0.812 Dichlorobenzene 4
1.000 Naphthalene (IS)
1.112 o - Terpi neol 1
1.463 ? 1
1.623 Caffeine 2
1.843 ? 1
1.887 Diethyl Hexyl Phthalate 1
1.963 Terpineol 1
TABLE B59
Organic Compounds Identified in Sample # 18S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
1.000 Chloroform 13
1.307 Bromo-dichloromethane 2
1.569 Dibrorco-chloromethane 4
2.126 Toluene 1
-------
38
TABLE B60
Organic
Compounds Identified in Sample #
18A
Peak #
Relative
Retention
Time
Compounds in Acid Extract
Approximate
Level (PPB)
1
0.453
Methyl-2-ethyl Hexanoate (IS)
. 2
0.828
C^q - Terpineol
1
3
1.000
Methyl Palmitate
1
4
1.098
Methyl Stearate
1
TABLE B61
Organic Compounds Identified in Sample r
18B
Peak if
Relative
Retention
Time
Compounds in Base Extract
Approximate
Level (PPB)
1
1.000
Camphor (IS)
2
1.492
C-jq - Terpineol
3
3
1.968
Dibutyl Phthalate
1
4
2.385
Diethyl Phthalate
4
-------
39
TABLE B62
Organic Compounds Identified in Sample # 19S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
Sample #19 was not assayed for volatiles.
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
40
TABLE B63
Organic Compounds Identified in Sample #19A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.550 Methyl-2-ethyl Hexanoate (IS)
0.817 C^p - Terpineol 7
0.890 Methyl Myristate 5
0.948 Methyl Pentachlorophenyl Ether 10
1.000 Methyl Palmitate 61
1.024 ? 8
1.064 ? 5
1.106 Methyl Stearate 56
1.131 ? 17
1.143 Hydrocarbon C > 22 18
1.188 Hydrocarbon C >_ 24 20
1.213 ? 19
1.234 ? 52
1.277 Methyl Dehydroabietate 15
1.286 Fatty Acid Methyl Ester C >_ 22 35
1.316 Hydrocarbon C >_ 26 22
1.347 Diethyl Hexyl Phthalate 38
1.372 ? 27
1.396 Hydrocarbon C ^ 30 20
-------
41
TABLE B64
Organic Compounds Identified in Sample /H9B
Relative
Retention Approximate
Peak if Time Compounds in Base Extract Level (PPB)
1
1.000
Camphor (IS)
--
2
1.511
C.|Q - Terpineol
2
3
2.011
Dibutyl Phthalate
4
4
2.175
Hydrocarbon C > 22
1
5
2.258
Hydrocarbon C > 24
1
6
2.351
Butylphthalylbutyl Glycolate
3
7
2.461
Diethyl Hexyl Phthalate
1
TABLE B65
Organic Compounds Identified in Sample # 2OS
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 12
2 1.533 Benzene 2
3 2.221 Chlorobenzene 1
-------
42
TABLE B66
Organic Compounds Identified in Sample ง 20A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1 0.455 Methyl-2-ethyl Hexanoate (IS)
2 1.100 Methyl Palmitate "1
3 1.093 Methyl Stearate "I
TABLE B67
Organic Compounds Identified in Sample ^20B
Relative
Retention Approximate
Peak ง Time Compounds in Base Extract Level (PPB)
1.000 Camphor (IS)
-------
43
TABLE B68
Organic Compounds Identified in Sample ง 21S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1
0.862
Tetrahydrofuran
1
2
1.000
Chioroform
16
3
1.085
1,2-Dichloroethane
1
4
1.195
1,1,1-Trichloroethane
3
5
1.303
Tetrahydropyran
2
6
1.515
Trichloroethylene
1
7
1.543
Benzene
1
8
1.978
Dichlorobenzene
1
9
2.036
Tetrachloroethylene
2
10
2.127
Toluene
1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
44
TABLE B69
Organic Compounds Identified in Sample # 21A
Relative
Retention Approximate
Time Compounds in Acid Extract Level {PPB)
0.499
Methyl-2-ethyl Hexanoate (IS)
--
0.666
Hydrocarbon C > 14
1
0.899
Methyl Myristate
2
1.000
Methyl Palmitate
22
1.048
Fatty Acid Methyl Ester C > 16
3
1.058
?
3
1.091
Methyl Stearate
33
1.131
?
2
1.170
C16H10 Uomer
1
1.179
Fatty Acid Methyl Ester C >_ 20
10
1.200
Cl0H1o *somer
1
1.215
?
12
1.254
Methyl Dehydroabietate
4
1.261
Fatty Acid Methyl Ester
5
1.315
Diethyl Hexyl Phthalate
20
1.346
?
8
1.361
?
6
1.379
?
5
1.400
2
-------
1
2
3
4
5
6
7
k
1
2
3
4
5
6
7
8
45
TABLE B70
Organic Compounds Identified in Sample #218
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000
Camphor (IS)
--
1.405
Hydrocarbon C > 16
1
2.384
Diethyl Hexyl Phthalate
7
2.455
C18H12
1
2.701
?
1
2.739
?
8
2.799
7
6
TABLE B71
Organic Compounds Identified in Sample #22S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
0.485
Acetone
2
0.867
Tetrahydrofuran
1
1.000
Chloroform
22
1.072
1,2-Dichloroethane
1
1.172
1,1,1-Trichloroethane
1
1.393
1,2-Dichloropropane
2
1.481
Trichloroethylene
7
1.985
Tetrachloroethylene
1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
46
TABLE B72
Organic Compounds Identified in Sample # 22A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.438
Methyl-2-ethyl Hexanoate (IS)
0.787
Fatty Acid Methyl Ester C > 12
1
0.797
Methyl Trichlorophenyl Ether
1
0.815
Methyl-2{4-chlorophenoxy) Butanoate
1
0.827
Methyl Tetrachlorophenyl Ether
2
0.897
Methyl Hyristate
1
0.951
Methyl Pentachlorophenyl Ether
1
1.000
Methyl Pa Imitate
2
1.018
Alkyl Benzene
1
1.057
7
2
1.097
Methyl Stearate
3
1.185
Fatty Acid Methyl Ester C >_ 20
1
1.218
?
8
1.263
Fatty Acid Methyl Ester C >_ 22
4
1.318
Diethyl Hexyl Phthalate
2
1.324
?
2
1.339
?
2
1.364
?
1
1.385
C^ - Terpineol
1
1.400
1
-------
1
2
3
4
5
6
7
8
9
10
11
12
13
ปk
1
2
3
4
5
6
7
8
9
47
TABLE B73
Organic Compounds Identified in Sample ?? 22B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000 Camphor (IS)
1.313 Hydrocarbon 1
1.526 ? 3
1.609 ? 3
1.755 Diphenyl Ethane 3
1.800 Alkyl Phenyl Ether 4
1.889 ? 2
2.007 Dibutyl Phthalate 1
2.097 ? 1
2.147 C16H10 1
2.208 C16H,0 3
2.302 ? 2
2.432 Diethyl Hexyl Phthalate 5
TABLE B74
Organic Compounds Identified in Sample # 23S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
0.427
Dichloromethane
1
0.861
Tetrahydrofuran
2
0.959
Dichloroethylene
1
1.000
Chloroform
27
00
o
1,2-Dichloroethane
2
1.197
1,1,1-Trichloroethane
1
1.434
1,2-Dichloropropane
1
1.527
Trichloroethylene
5
2.054
Tetrachloroethylene
1
-------
48
TABLE B75
Organic Compounds Identified in Sample #23A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1
0.446
Methyl-2-ethyl Hexanoate (IS)
2
0.814
Methyl-2(4-chlorophenoxy) Butanoate
2
3
0.897
Fatty Acid Methyl Ester C = 14
2
4
0.951
Fatty Acid Methyl Ester C >_ 14
2
5
0.969
Alkyl Benzene
3
6
1.000
Methyl Palmitate
2
7
1.057
?
2
8
1.097
Methyl Stearate
3
9
1.215
6
10
1.264
Fatty Acid Methyl Ester C >_ 22
3
11
1.326
Diethyl Hexyl Phthalate
1
12
1.347
?
2
TABLE B76
Organic Compounds Identified in Sample f23B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 1.963 Dibutyl Phthalate 2
3 2.275 Butylphthalylbutyl Glycolate 6
4 2.374 Diethyl Hexyl Phthalate 2
-------
Peak
1
2
3
4
5
6
eak #
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
49
TABLE B77
Organic Compounds Identified in Sample # 24S .
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
0.954 Dichloroethylene 1
1.000 Chloroform 17
1.075 1,2-Dichloroethane 1
1.184 1,1,1-Trichloroethane 1
1.512 Trichloroethylene 2
2.036 Tetrachloroethylene 2
TABLE B78
Organic Compounds Identified in Sample # 24A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.436
Methyl-2-ethyl Hexanoate (IS)
0.812
Methyl-2(4-chlorophenoxy) Butanoate
2
0.933
Hydrocarbon C >_ 16
1
0.952
Methyl Pentachlorophenyl Ether
1
o
o
o
Methyl Palmitate
2
1.057
?
2
1.094
Methyl Stearate
3
1.215
?
9
1.254
?
3
1.269
?
1
1.318
Diethyl Hexyl Phthalate
1
1.342
?
3
1.363
Hydrocarbon C >_ 28
1
1.384
C,c - Terpineol
1 b
1
1.403
Hydrocarbon C ^ 30
1
1.436
Hydrocarbon C >_ 30
1
1.463
Hydrocarbon C >_ 30
1
-------
Peak
1
2
3
4
5
Peak
1
2
3
4
5
6
7
50
TABLE B79
Organic Compounds Identified in Sample # 24B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000 Camphor (IS)
1.991 Dibutyl Phthalate 2
2.356 Butyl benzyl Phthalate 1
2.411 Diethyl Hexyl Phthalate 1
2.522 C^ - Terpineol 1
TABLE B80
Organic Compounds Indentified in Sample # 25S
Relati ve
Retention Approximate
Time Volatile Compounds Level (PPB)
0.864 Tetrahydrofuran 2
0.954 Dichloroethylene 1
1.000 Chloroform 26
1.079 1,2-Dichloroethane 1
1.187 1,1,1-Trichloroethane 1
1.493 Trichloroethylene 1
1.998 Tetrachloroethylene 1
-------
51
TABLE B81
Organic Compounds Identified in Sample # 25A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1 0.448 Methyl-2-ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.058 ? 2
4 1.094 Methyl Stearate 3
5 1.206 ? 6
6 1.254 ? 2
7 1.321 Diethyl Hexyl Phthalate 1
8 1.346 ? 2
9 1.385 C15 " TerPineฐl ^
TABLE B82
Organic Compounds Identified in Sample #25B
Relati ve
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 2.013 Dibutyl Phthalate 1
3 2.441 Diethyl hexyl Phthalate 1
-------
Peak
1
2
3
4
5
6
7
Peak #
1
2
3
4
5
6
7
8
9
52
TABLE B83
Organic Compounds Identified in Sample # 26S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
0.395
Dichloromethane
1
0.957
Dichloroethylene
1
1.000
Chloroform
20
1.141
1,1,1-Trichloroethane
1
1.483
Tri chloroethylene
1
1.509
Benzene
1
1.983
Tetrachioroethylene
1
TABLE B84
Organic Compounds Identified in Sample # 26A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.468 Methyl-2-ethyl Hexanoate (IS)
0.951 Methyl Pentachlorophenyl Ether 1
1.000 Methyl Palmitate 2
1.057 ? 1
1.094 Methyl Stearate 3
1.215 ? 4
1.322 Diethyl Hexyl Phthalate 2
1.347 ? 2
1.386 C15 " TerPlrieol 2
-------
53
TABLE B85
Organic Compounds Identified in Sample *26B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 1.985 Dibutyl Phthalate 1
3 2.413 Diethyl Hexyl Phthalate 2
4 2.441 ? 1
5 2.530 C^g - Terpineol 4
6 2.647 ? 2
1 2.780 ? 2
TABLE B86
Organic Compounds Identified in Sample #27S
Relative
Retention Approximate
Peak ง Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
-------
Peak
1
2
3
4
5
6
Peak
1
2
3
4
54
TABLE B87
Organic Compounds Identified in Sample #27A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.468 Methyl-2-ethyl Hexanoate (IS)
0.960 C CI F n ^ 4 2
n x z
1.000 Methyl Palmitate 1
1.097 Methyl Stearate + C CI f , n % 4 4 (mix)
J n x z -
1.222 C CI F n -v- 4 2
n x z
1.319 Diethyl Hexyl Phthalate 1
TABLE B88
Organic Compounds Identified in Sample ฃ 27B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1.000 Camphor (IS)
1.977 Dibutyl Phthalate 2
2.397 Diethyl Hexyl Phthalate 1
2.513 C-j,- - Terpineol 1
-------
Peak
1
2
3
4
5
6
ปak #
1
2
3
4
5
6
7
8
9
10
11
55
TABLE B89
Organic Compounds Identified in Sample # 28S
Relative
Retention Approximate
Time Volatile Compounds Level (PPB)
1.000 Chloroform 18
1-189 1 ,1,1-Trichloroethane 1
1-516 Trichloroethylene 1
1-544 Benzene 1
2.031 Tetrachloroethylene 1
2.123 Toluene 1
TABLE B90
Organic Compounds Identified in Sample ง 28A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.464 Methyl-2-ethyl Hexanoate (IS)
0.907 ? 2
0.945 Methyl Pentachlorophenyl Ether 1
1.000 Methyl Palmitate 2
1.058 ? 2
1.095 Methyl Stearate 3
1.221 ? 4
1.329 Diethyl Hexyl Phthalate 2
1.357 ? 2
1.375 ? 1
1.397 ^15 ~ Terpineol 1
-------
56
TABLE B91
Organic Compounds Identified in Sample #28B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 1499 Cio - Terpineol 1
3 1.991 Dibutyl Phthalate 1
4 2.326 Butylphthalylbutyl Glycolate 2
5 2.432 Diethyl Hexyl Phthalate 3
6 2.466 ? 3
TABLE B92
Organic Compounds Identified in Sample i 29S
Relative
Retention Approximate
Peak # Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
2 1.504 Trichloroethylene 1
3 1.532 Benzene 1
-------
Peak
1
2
3
4
5
6
7
Peak
1
2
3
4
5
57
TABLE B93
Organic Compounds Identified in Sample ^ 29A
Relative
Retention Approximate
Time Compounds in Acid Extract Level (PPB)
0.451 Methyl-2-ethyl Hexanoate (IS)
1.000 Methyl Palmitate 2
1.056 ? 1
1.096 Methyl Stearate 2
1.223 ? 3
1.325 Diethyl Hexyl Phthalate 1
1.394 C-|5 - Terpineol 1
TABLE B94
Organic Compounds Identified in Sample f?29B
Relative
Retention Approximate
Time Compounds in Base Extract Level (PPB)
1-000 Camphor (IS)
1-962 Dibutyl Phthalate ]
2-386 Diethyl Hexyl Phthalate l
2.413 ? 1
2.502 Terpineol 2
-------
58
TABLE B95
Organic Compounds Identified in Sample ^30S
Relative
Retention Approximate
Peak ง Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 120
2 1.262 ? 10
3 1.507 Trichloroethylene 1
4 1.535 Benzene 1
5 2.230 Acetophenone 1
TABLE B96
Organic Compounds Identified in Sample #30A
Relative
Retention Approximate
Peak # Time Compounds in Acid Extract Level (PPB)
1 0.442 Methyl-2-ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.058 ? 1
4 1.094 Methyl Stearate 2
5 1.215 ? 3
6 1.321 Diethyl Hexyl Phthalate 1
7 1.385 Cis - Terpineol 1
-------
59
TABLE 897
Organic Compounds Identified in Sample *30B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 1.995 Dibutyl Phthalate 1
3 2.422 Diethyl hexyl Phthalate 1
4 2.457 ? 1
TABLE B98
Organic Compounds Identified in Sample ^31S
Relative
Retention Approximate
Peak ง Time Volatile Compounds Level (PPB)
1 1.000 Chloroform 14
2 1.535 Trichloroethylene 1
3 1.564 Benzene 1
4 1.995 Tetrachloroethylene 1
-------
60
TABLE B99
Organic Compounds Identified in Sample # 31A
Relative
Retention Approximate
Peak 4 Time Compounds in Acid Extract Level (PPB)
1 0.442 Methyl-2-ethyl Hexanoate (IS)
2 0.551 ? 1
3 0.567 ? 1
4 0.607 ? 1
5 1.000 Methyl Palmitate 3
6 1.092 Methyl Stearate 3
7 1.215 ? 2
8 1.261 Butylphthalylbutyl Glycolate 4
9 1.316 Diethyl Hexyl Phthalate 1
TABLE B100
Organic Compounds Identified in Sample # 31B
Relative
Retention Approximate
Peak # Time Compounds in Base Extract Level (PPB)
1 1.000 Camphor (IS)
2 2.409 Diethyl Hexyl Phthalate 1
3 2.527 C15 - Terpineol 2
-------
61
TABLE B101
Volatile Organic Compounds Identified in Sample No. 32S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.729 Dimethoxymethane 2
2 1.000 Chloroform 2
3 1.006 1,2-Dichloroethane 2
4 1.583 Benzene 1
5 2.295 Chloroben2ene 1
TABLE B102
Organic Compounds Identified in Acid Extract of Sample No. 32A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.464 Methyl-2-ethyl Hexanoate (IS)
2 1.000 Methyl PaImitate 3
3 1.094 Methyl Stearate 3
4 1.265 Butyl Phthalyl Butyl Glycolate 2
5 1.322 Diethyl Hexyl Phthalate 2
6 1.386 C-, c Terpineol 1
7 1.450 " ,
8 1.526 ? 1
-------
62
TABLE B103
Organic Compounds Identified in Base Extract of Sample No.32B
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
1.000
Camphor (IS)
2
1.107
7
4
3
1.207
Nitrotoluene
4
4
1.237
Chioro-Nitrobenzene
17
5
1.521
C-jq - Terpineol
1
6
2.043
Dibutyl Phthalate
1
7
2.398
Butyl Phthalyl Butyl Glycolate
1
8
2.511
Diethyl Hexyl Phthalate
49
9
2.648
C^ - Terpineol
1
TABLE B104
Volatile Organic Compounds Identified in Sample No. 33S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.735 Dimethoxymethane 1
2 0.868 Tetrahydrofuran 1
3 1.000 Chloroform 2
4 1.081 1,2-Dichloroethane 1
5 1.524 Trichloroethylene 1
6 2.047 Tetrachloroethylene 1
-------
63
TABLE B105
Organic Compounds Identified in Acid Extract of Sample No.33A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.483 Methyl-2-Ethyl Hexanoate (IS)
2 0.502 ? 1
3 0.955 ? 25
4 1.000 Methyl Palmitate 4
5 1.020 ? 1
6 1.103 Methyl Stearate 3
7 1.350 Diethyl Hexyl Phthalate 1
8 1.372 Fatty Acid Methyl Ester C _> 22 1
9 1.420 - Terpineol 2
-------
64
TABLE B106
Organic Compounds Identified in Base Extract of Sample No. 33B
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
0.827
Dichlorobenzene
3
2
1.000
Camphor (IS)
3
1.101
?
1
4
1.208
Nitrotoluene
1
5
1.244
Chioroni trobenzene
2
6
1.657
Dinitrotoluene
1
7
2.514
Diethyl Hexyl Phthalate
1
TABLE B107
Volatile Organic Compounds Identified in Sample No.
34S
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.719
Dimethoxymethane
3
2
0.862
Tetrahydrofuran
1
3
1.000
Chloroform
2
4
1.086
1,2-Di chloroethane
12
5
1.532
Trichloroethylene
2
6
2.053
Tetrachloroethylene
3
TABLE B108
Organic Compounds Identified in Acid Extract of Sample N0.34A
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
0.500
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
2
3
1.084
Methyl Stearate
2
4
1.289
Diethyl Hexyl Phthalate
1
-------
65
TABLE B109
Organic Compounds Identified in Base Extract of Sample No. 34B
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
2
2.037
Dibutyl Phthalate
1
3
2.499
Diethyl Hexyl Phthalate
2
4
2.630
C^ Terpineol
3
TABLE B110
Volatile Organic Compounds Identified in Sample No. 35S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.749
Dimethoxymethane
3
2
1.000
Chloroform
2
3
1.082
1,2-Dichloroethane
15
4
1.507
Trichloroethylene
1
5
2.004
Tetrachloroethylene
3
/
-------
66
TABLE Bill
Organic Compounds Identified in Acid Extract of Sample No.35A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.490 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 2
4 1.349 Diethyl Hexyl Phthalate 1
TABLE Bll2
Organic Compounds Identified in Base Extract of Sample No. 35B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE Bll3
Volatile Organic Compounds Identified in Sample No. 36S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.710 Dimethoxymethane 3
2 1.000 Chloroform 7
3 1.069 1 ,2-Dichloroethane 9
4 1.535 Trichloroethylene 1
5 2.063 Tetrachloroethylene 2
-------
67
TABLE B114
Organic Compounds Identified in Acid Extract of Sample No. 36A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 0.958 ? 19
3 1.000 Methyl Palmitate 6
4 1.099 Methyl Stearate 11
5 1.335 Diethyl Hexyl Phthalate 1
6 1.401 C]5 - Terpineol 1
TABLE B115
Organic Compounds Identified in Base Extract of Sample No. 36B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.380 Diethyl Hexyl Phthalate
-------
68
TABLE B116
Volatile Organic Compounds Identified in Sample No. 37S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.730 Dimethoxymethane 4
2 1.000 Chloroform 2
3 1.079 1,2-Dichloroethane 15
4 1.461 Trichloroethylene 1
5 1.917 Tetrachloroethylene 2
TABLE B117
Organic Compounds Identified in Acid Extract of Sample No. 37A
No.
Relative Approximate
Peak Retention /eVf{
Time Compound (ppb)
1 0.453 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.098 Methyl Stearate 5
-------
69
TABLE 3118
Organic Compounds Identified in Base Extract of Sample No. 37B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.897 ? 2
3 2.431 Diethyl Hexyl Phthalate 1
TABLE B119
Volatile Organic Compounds Identified in Sample No. 38S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
2
2
2
2
1
0.414
Dichloromethane
2
0.489
Acetone
3
0.722
Dimethoxymethane
4
1.000
Chloroform
5
1.087
1,2-Dichloroethane
6
1.447
1,2-Dichloropropane
7
1.537
Trichloroethylene
8
1.568
Benzene
9
2.050
Tetrachloroethylene
-------
70
TABLE B120
Organic Compounds Identified in Acid Extract of Sample No. 38A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.096 Methyl Stearate 3
TABLE B121
Organic Compounds Identified in Base Extract of Sample No.38B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.627 ? 2
-------
71
TABLE B122
Volatile Organic Compounds Identified in Sample No. 39S
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.491
Dichloromethane
8
2
0.759
Methylal
12
3
1.000
Chioroform
12
4
1.077
1,2-Dichloroethane
90
5
1.175
1,1,1-Trichloroethane
1
6
1.394
1,2-Dichloropropane
2
7
1.509
Trichloroethylene
24
8
1.973
Tetrachloroethylene
4
9
2.061
Toluene
1
TABLE B123
Organic Compounds Identified in Acid Extract of Sample No. 39A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.452 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 6
3 1.095 Methyl Stearate 8
4 1.327 Diethyl Hexyl Phthalate 1
-------
72
TABLE B124
Organic Compounds Identified in Base Extract of Sample No.39B
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(PPb)
1
1.000
Camphor (IS)
2
1.572
?
1
3
1.627
?
3
4
1.991
Dibutyl Phthalate
1
5
2.249
?
1
6
2.431
Diethyl Hexyl Phthalate
1
7
2.508
Unidentified Phthalate
1
8
2.684
?
1
9
2.833
?
1
TABLE B125
Volatile Organic Compounds Identified in Sample No. 40S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.524 Trichloroethylene 2
3 2.036 Tetrachloroethylene 1
-------
73
TABLE B126
Organic Compounds Identified in Acid Extract of Sample No. 40A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.467 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.099 Methyl Stearate 3
4 1.329 Diethyl Hexyl Phthalate 1
TABLE B127
Organic Compounds Identified in Base Extract of Sample No. 40B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.612 ? 2
3 2.416 Diethyl Hexyl Phthalate 2
4 2.662 ? 4
5 2.790 ? 2
-------
74
TABLE B128
Volatile Organic Compounds Identified in Sample No. 41S
p . r,RAlaV-Ve Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 6
2 1.500 Trichloroethylene 1
3 2.054 Tetrachloroethylene 1
TABLE B129
Organic Compounds Identified in Acid Extract of Sample No. 41A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.472 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 6
3 1.093 Methyl Stearate 6
4 1.326 Diethyl Hexyl Phthalate 2
5 1.458 ? 4
6 1.517 ? 3
-------
75
TABLE B130
Organic Compounds Identified in Base Extract of Sample No. 41B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.612 ? 1
3 2.420 Diethyl Hexyl Phthalate 1
4 2.662 ? 2
TABLE B131
Volatile Organic Compounds Identified in Sample No. 42S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 13
2 1.086 1,2-Dichloroethane 8
3 1.507 Trichloroethylene 4
4 2.053 Tetrachloroethylene 5
-------
76
TABLE B132
Organic Compounds Identified in Acid Extract of Sample No. 42A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.450
Methyl-2-Ethyl Hexanoate (IS)
--
2
1.000
Methyl Palmitate
5
3
1.096
Methyl Stearate
6
4
1.331
Diethyl Hexyl Phthalate
1
5
1.397
C-jg - Terpineol
1
6
1.466
?
2
7
1.546
?
2
TABLE B133
Organic Compounds Identified in Base Extract of Sample No. 42B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.850
Dichlorobenzene
3
2
1.000
Camphor (IS)
3
1.102
Nitrotoluene
7
4
1.236
Chioroni trobenzene
13
5
2.381
Diethyl Hexyl Phthalate
1
6
2.622
?
3
7
2.772
7
3
-------
77
TABLE B134
Volatile Organic Compounds Identified in Sample No. 43S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.535 Acetone 1
2 1.000 Chloroform 2
3 1.505 Trichloroethylene 2
TABLE B135
Organic Compounds Identified in Acid Extract of Sample No. 43A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.450
2
1.000
3
1.097
4
1.200
5
1.240
6
1.333
7
1.352
8
1.379
9
1.400
10
1.467
11
1 .549
Methyl-2-Ethyl Hexanoate (IS)
Methyl Palmitate 4
Methyl Stearate 3
?
Dioctyl Adipate
Diethyl Hexyl Phthalate
Diethyl Hexyl Phthalate
Diethyl Hexyl Phthalate
C-jg - Terpineol
-------
78
TABLE B136
Organic Compounds Identified in Base Extract of Sample No. 43B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.387 Diethyl Hexyl Phthalate 2
3 2.546 C-jg Terpineol 1
4 2.665 ? 2
5 2.801 ? 3
TABLE B137
Volatile Organic Compounds Identified in Sample No. 44S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.736 Dimethoxymethane 2
2 1.000 Chloroform 2
3 2.143 Dichlorobenzene 8
4 2.220 Dichlorobenzene 10
-------
79
TABLE B138
Organic Compounds Identified in Acid Extract of Sample No. 44A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
0.456
Methyl-2-Ethyl Hexanoate (IS)
ป ซ
2
0.496
Methyl-2,2-Dichloro-3-Methyl Butanoate
59
3
0.582
Dichlorinated Hydrocarbon C > 5
21
4
0.638
Dichlorinated Hydrocarbon C > 5
5
5
0.692
1
1
7
0.861
A1kyl Benzene
1
8
0.896
Methyl Myristate
2
9
1.000
Methyl Palmitate
5
10
1.100
Methyl Stearate
4
11
1.207
C-j g Terpene
2
12
1.279
Butyl Phthalyl Butyl Glycolate
1
13
1.339
Diethyl Hexyl Phthalate
1
TABLE B139
Organic Compounds Identified in Base Extract of Sample No.44B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.008 Dibutyl Phthalate 1
3 2.463 Diethyl Hexyl Phthalate 2
4 2.590 C15 Terpineol 1
-------
80
TABLE B140
Volatile Organic Compounds Identified in Sample No. 45S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.532 Acetone 1
2 1.000 Chloroform 4
3 1.559 Benzene 1
TABLE B141
Organic Compounds Identified in Acid Extract of Sample No. 45A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.450
Methyl-2-Ethyl Hexanoate (IS)
__
2
0.900
Methyl Myristate
2
3
0.959
Hexachloro-hexafluoropentane
1
4
1.000
Methyl Palmitate
6
5
1.099
Methyl Stearate
4
6
1.200
C-|5 Terpene
2
7
1.337
Diethyl Hexyl Phthalate
1
8
1.406
C-j5 - Terpineol
1
-------
81
TABLE B142
Organic Compounds Identified in Base Extract of Sample No. 45B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.991 Dibutyl Phthalate 1
3 2.384 Diethyl Hexyl Phthalate 2
4 2.566 C^5 Terpineol 1
5 2.691 ? 1
TABLE B143
Volatile Organic Compounds Identified in Sample No. 46S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.552 Acetone 1
2 1.000 Chloroform 2
3 1.534 Benzene 1
4 2.095 Dichlorobenzene 10
-------
82
TABLE B144
Organic Compounds Identified in Acid Extract of Sample No. 46A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.450
Methyl-2-Ethyl Hexanoate (IS)
--
2
1.000
Methyl Palmitate
5
3
1.099
Methyl Stearate
4
4
1.199
C-i r Terpene
2
5
1.282
CxC1yFz
1
6
1.331
Diethyl Hexyl Phthalate
1
7
1.392
C-j5 - Terpineol
1
TABLE B145
Organic Compounds Identified in Base Extract of Sample No. 46B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.427 Diethyl Hexyl Phthalate 1
3 2.551 C^g Terpineol 1
4 2.675 ? 1
5 2.831 ? 1
-------
83
TABLE B146
Volatile Organic Compounds Identified in Sample No. 47S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B147
Organic Compounds Identified in Acid Extract of Sample No. 47A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.095 Methyl Stearate 2
4 1.328 Diethyl Hexyl Phthalate 1
5 1.393 C15 - Terpineol 1
6 1.463 ? 1
7 1.552 ? 1
-------
84
TABLE B148
Organic Compounds Identified in Base Extract of Sample No.47B
Peak
No.
Relative
Retention
Time
Approximate
Level
Compound (ppb)
1
1.000
Camphor (IS)
2
2.399
Diethyl Hexyl Phthalate 1
3
2.516
C-J5 Terpineol 1
4
2.643
? 2
5
2.797
? 2
TABLE B149
Volatile Organic Compounds Identified in Sample No. 48S
Peak
No.
Relative
Retention
Time
Approximate
Level
Compound (ppb)
No peaks over 1 PPB.
TABLE B150
Organic Compounds Identified in Acid Extract of Sample No. 48A
Peak
No.
Relative
Retenti on
Time
Approximate
Level
Compound (ppb)
1
0.443
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
. Methyl Palmitate 1
3
1.096
Methyl Stearate 1
4
1.198
C-J5 Terpene 1
5
1.270
Butyl Phthalyl Butyl Glycolate 1
6
1.397
C-|[j - Terpineol 1
-------
85
TABLE B151
Organic Compounds Identified in Base Extract of Sample No.48B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.593 C,c Terpineol
I b
TABLE B152
Volatile Organic Compounds Identified in Sample Mo. ^9S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.531 Freon-11 1
2 1.000 Chloroform 2
3 1.508 Trichloroethylene 1
4 1.93ฃ Trichloropropane 2
5 1.986 Tetrachloroethylene 1
-------
86
TABLE B153
Organic Compounds Identified in Acid Extract of Sample No. 49A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.438
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
3
3
1.101
Methyl Stearate
4
4
1.232
CxC1yFz
2
5
1.279
Butyl Phthalyl Butyl Glycolate
3
6
1.336
Diethyl Hexyl Phthalate
1
7
1.403
C-|ฃ ~ Terpineol
1
TABLE B154
Organic Compounds Identified in Base Extract of Sample No. 49B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.025 Dibutyl Phthalate 1
3 2.478 Diethyl Hexyl Phthalate 2
-------
87
TABLE B155
Volatile Organic Compounds Identified in Sample No. 50S
Relative
Peak Retention
No. Time Compound
1 1.000 Chloroform 2
Approximate
Level
(ppb)
TABLE B156
Organic Compounds Identified in Acid Extract of Sample No. 50A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.447 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.096 Methyl Stearate 2
TABLE B157
Organic Compounds Identified in Base Extract of Sample No.50B
d t, DR<+laV-Ve Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.964 Dibutyl Phthalate 1
3 2.390 Diethyl Hexyl Phthalate 1
4 2.509 C-|^ Terpineol 1
-------
88
TABLE B158
Volatile Organic Compounds Identified in Sample No. 51S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.502
Acetone
3
2
0.835
Tetrahydrofuran
1
3
1.000
Chloroform
47
4
1.101
Pentane
1
5
1.233
Carbon Tetrachloride
2
6
1.302
Bromo-Di chloromethane
10
7
1.429
?
4
8
1.514
Trichloroethyl ene
1
9
1.559
Di bromo-Chloromethane
6
10
1.779
Tribromomethane
1
11
1.928
Bromobenzene
38
12
2.007
Tetrachloroethylene
2
13
2.108
Toluene
1
TABLE B159
Organic Compounds Identified in Acid Extract of Sample No. 51A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.454 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate
-------
89
TABLE B160
Organic Compounds Identified in Base Extract of Sample No.51B
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 1.000 Camphor (IS)
2 2.460 Diethyl Hexyl Phthalate 1
TABLE B161
Volatile Organic Compounds Identified in Sample No. 52S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.496 Trichloroethylene 2
3 1.986 Tetrachloroethylene 2
TABLE B162
Organic Compounds Identified in Acid Extract of Sample No. 52A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.445
Methyl-2-Ethyl Hexanoate (IS)
2
o
o
o
Methyl Palmitate
4
3
1.103
Methyl Stearate
4
4
1.247
Dioctyl Adipate
2
5
1.343
Diethyl Hexyl Phthalate
1
6
1.409
C15 - Terpineol
2
7
1.461
?
1
8
1.552
1
-------
90
TABLE B163
Organic Compounds Identified in Base Extract of Sample No.52B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Camphor (IS)
2
1.556
C^0 Terpineol
1
3
2.089
Dibutyl Phthalate
1
4
2.564
Diethyl Hexyl Phthalate
2
5
2.693
C,c - Terpineol
1 b
1
TABLE B164
Volatile Organic Compounds Identified in Sample No. 53S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.538
Acetone
1
2
0.769
Dimethoxymethane
8
3
0.895
2-Methyl Propanal
1
4
0.963
1,2-Dichloroethane
4
5
1.000
Chloroform
68
6
1.084
1,2-Dichloroethane
4
7
1.220
Carbon Tetrachloride
1
8
1.288
Bromo-Dichloromethane
12
9
1.425
?
1
10
1.493
Trichloroethylene
1
11
1.530
Dibromo-Chioromethane
10
12
1.666
Dichloro-Iodomethane
1
13
1.750
Tribromomethane
1
14
1.960
Dichlorobenzene
10
15
2.086
Dichlorobenzene
15
-------
91
TABLE B165
Organic Compounds Identified in Acid Extract of Sample No. 53A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.338 Diethyl Hexyl Phthalate 1
4 1.409 C-j5 - Terpineol 1
TABLE B166
Organic Compounds Identified in Base Extract of Sample No.53B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.658 C-|g Terpineol 3
3 2.053 Dibutyl Phthalate 1
4 2.511 Diethyl Hexyl Phthalate 2
5 2.643 C-|^ Terpineol 2
TABLE B167
Volatile Organic Compounds Identified in Sample No. 54S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.516 Trichloroethylene 2
3 1.559 Benzene 1
-------
92
TABLE B168
Organic Compounds Identified in Acid Extract of Sample No. 54A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(PPb)
1
0.450
Methyl-2-Ethyl Hexanoate
(IS)
2
1.000
Methyl Palmitate
1
3
1.103
Methyl Stearate
1
4
1.342
Diethyl Hexyl Phthalate
1
5
1 .409
C-jg - Terpineol
1
TABLE B169
Organic Compounds Identified in Base Extract of Sample No. 54B
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Camphor (IS)
2
2.053
Dibutyl Phthalate
1
3
2.505
Diethyl Hexyl Phthalate
1
TABLE B170
Volatile Organic Compounds Identified
in Sample No. 55S
Relati ve
Approximate
Peak
Retention
Level
No.
Time
Compound
(PPb)
1
1.000
Chloroform
2
2
1.488
Trichloroethylene
1
3
1.965
Tetrachloroethylene
1
-------
93
TABLE B171
Organic Compounds Identified in Acid Extract of Sample No. 55A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.097 Methyl Stearate 2
4 1.332 Diethyl Hexyl Phthalate 1
5 1.398 ^15-" Terpineol 1
TABLE B172
Organic Compounds Identified in Base Extract of Sample No. 55B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.955 Dibutyl Phthalate 1
3 2.373 Diethyl Hexyl Phthalate 1
TABLE B173
Volatile Organic Compounds Identified in Sample No. 56S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.531 Trichloroethylene 1
3 2.040 Tetrachloroethylene 1
-------
94
TABLE B174
Organic Compounds Identified in Acid Extract of Sample No.56A
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
0.432
Methyl-2-Ethyl Hexanoate
(IS)
2
1.000
Methyl Palmitate
3
3
1.097
Methyl Stearate
2
4
1.333
Diethyl Hexyl Phthalate
1
5
1 .400
C-jg - Terpineol
1
TABLE B175
Organic Compounds Identified in Base Extract of Sample No. 56B
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
2
2.048
Dibutyl Phthalate
2
3
2.506
Diethyl Hexyl Phthalate
2
4
2.637
C-|g Terpineol
2
TABLE B176
Volatile Organic Compounds Identified
in Sample No. 57S
Peak
No.
Relati ve
Retention
Time
Compound
Approximate
Level
(ppb)
1 1.000
2 1.493
3 1.966
Chloroform
Trichloroethylene
Tetrachloroethylene
1
2
2
-------
95
TABLE B177
Organic Compounds Identified in Acid Extract of Sample No. 57A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound (ppb)
1
0.439
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate 5
3
1.097
Methyl Stearate 5
TABLE B178
Organic Compounds Identified in Base Extract of Sample No. 57B
Relati ve
Approximate
Peak
Retenti on
Level
No.
Time
Compound (ppb)
1
1.000
Camphor (IS)
2
1.885
Dibutyl Phthalate 1
3
2.570
Diethyl Hexyl Phthalate 1
TABLE B179
Volatile Organic Compounds Identified in Sample No.58S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound (ppb)
1 0.499 Acetone
2 1.000 Chloroform
1
3
-------
96
TABLE B180
Organic Compounds Identified in Acid Extract of Sample No. 58A
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(PPb)
1
0.415
Methyl-2-Ethyl Hexanoate (IS)
_ _ _
2
0.890
Methyl Myristate
1
3
1.000
Methyl Palmitate
4
4
1.098
Methyl Stearate
4
5
1.137
Diethyl Hexyl Phthalate
1
6
1.404
^15 " TerPineฐl
1
TABLE B181
Organic Compounds Identified in Base Extract of Sample No. 58B
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
_ _ _
2
1.807
1
3
2.442
Diethyl Hexyl Phthalate
2
TABLE B182
Volatile Organic Compounds Identified in Sample No.
59S
Peak
No.
Relative
Retention
Time
. Compound
Approximate
Level
(ppb)
1 1.000 Chloroform
2 1.937 Bromobenzene
1
3
-------
97
TABLE B183
Organic Compounds Identified in Acid Extract of Sample No. 59A
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(PPb)
1
0.393
Methyl-2-Ethyl Hexanoate (IS)
_ _
2
1.000
Methyl Palmitate
4
3
1.102
Methyl Stearate
3
4
1.334
Diethyl Hexyl Phthalate
2
5
1.400
C-j g - Terpineol
2
TABLE B184
Organic Compounds Identified in Base Extract of Sample No. 59B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.047 Dibutyl Phthalate 3
3 2.505 Diethyl Hexyl Phthalate 1
4 2.632 C^g Terpineol 1
-------
98
TABLE BT 85
Volatile Organic Compounds Identified in Sample No. 60S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.471
Acetone
1
2
1.000
Chloroform
30
3
1.124
Pentane
2
4
1.304
Ethyl Acetate
1
5
1.343
Bromo-Dichloromethane
5
6
1.484
Di chloropropane
1
7
1.575
Trichloroethylene
1
8
1.619
Benzene
1
9
1.642
Di bromo-Chloromethane
1
10
2.216
Toluene
2
TABLE B186
Organic Compounds Identified in Acid Extract of Sample No. 60A
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
0.442
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
4
3
1.103
Methyl Stearate
3
4
1.343
Diethyl Hexyl Phthalate
1
-------
99
TABLE B187
Organic Compounds Identified in Base Extract of Sample N0.6OB
Relative
Peak Retention
No. Time Compound
1 1.000 Camphor (IS)
2 1.517 C-|q Terpineol 1
3 2.477 Diethyl Hexyl Phthalate 1
Approximate
Level
(PPb)
TABLE B188
Volatile Organic Compounds Identified in Sample No. 61S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.519 Trichloroethylene 1
3 1.696 Hexane 1
-------
100
TABLE B189
Organic Compounds Identified in Acid Extract of Sample No. 61A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.450
Methyl-2-Ethyl Hexanoate (IS)
--
2
1 .000
Methyl Pal mi tate
4
3
1.097
Methyl Stearate
4
4
1.266
Methyl Dihydroabietate
3
5
1.278
Fatty Acid Methyl Ester C > 22
3
6
1.308
Hydrocarbon C > 26
2
7
1.339
Diethyl Hexyl Phthalate
2
8
1 .360
Fatty Acid Methyl Ester C > 24
5
9
1 .387
Hydrocarbon C > 28
3
10
1 .442
Fatty Acid Methyl Ester C > 26
8
11
1.481
Hydrocarbon C > 8
4
-------
101
TABLE B190
Organic Compounds Identified in Base Extract of Sample N0.6IB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.903 Anthracene 1
3 2.059 Dibutyl Phthalate 1
4 2.203 C16H10 2
5 2.266 c16H10 3
6 2.537 Diethyl Hexyl Phthalate 2
7 2.583 C18H12 1
8 2.594 C18H12 1
9 2.669 C-|5 Terpineol 1
TABLE B191
Volatile Organic Compounds Identified in Sample No. 62S
Relative Approximate
Peak Retention . Level
No. Time Compound / (ppb)
1 0.864 Tetrahydrofuran 3
2 1.000 Chloroform 4
3 1.082 1,2-Dichloroethane 10
4 1.187 Bromo-Dichloromethane 2
5 1.537 Trichloroethylene 2
6 1.936 4-Methyl-2-Ethyl-l,3-Dioxolane 1
7 2.007 1,1,2,2-Tetrachloroethane 1
8 2.045 Tetrachloroethylene 2
-------
102
TABLE B192
Organic Compounds Identified in Acid Extract of Sample No.62A
Relative Approximate
Peak Retention Level
No. Tine Compound (ppb)
1 0.442 Methyl-2-Ethyl Hexanoate (IS)
2 0.894 Methyl Myristate 6
3 0.948 Fatty Acid Methyl Ester C >_ 15 2
5 1.000 Methyl Palmitate 16
6 1.070 C-|^ Terpene 2
7 1.206 C-| ^ Terpene 7
8 1.282 Butyl Phthalyl Butyl Glycolate 6
9 1.343 Diethyl Hexyl Phthalate 2
10 1.412 C15 - Terpineol 1
TABLE B193
Organic Compounds Identified in Base Extract of Sample No.62B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.018 Dibutyl Phthalate 2
3 2.059 Dibutyl Nonanedioate 2
4 2.365 Butyl Phthalyl Butyl Glycolate 3
5 2.477 Diethyl Hexyl Phthalate 2
6 2.606 Cu Terpineol 1
-------
103
TABLE B194
Volatile Organic Compounds Identified in Sample No. 63S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.872
Tetrahydrofuran
2
2
1.000
Chloroform
6
3
1.075
1,2-Dichloroethane
9
4
1.368
Bromo-Dichloroethane
9
5
1.506
Trichloroethylene
3
6
1.895
Ethyl Methyl Dioxolane
1
7
1.970
1,1,2,2-Tetrachloroethane
1
8
2.007
Tetrachloroethylene
2
TABLE B195
Organic Compounds Identified in Acid Extract of Sample No. 63A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.431
Methyl-2-Ethyl Hexanoate (IS)
2
0.890
Methyl Myristate
6
3
0.945
Fatty Acid Methyl Ester C >_ 14
1
4
1.000
Methyl Palmitate
19
5
1.091
Methyl Stearate
13
6
1.128
?
3
7
1.164
C.| g Terpene
3
8
1.177
Diisobutyl Phthalate
3
9
1.204
C-|5 Terpene
3
10
1.225
?
2
11
1.277
Butyl Phthalyl Butyl Glycolate
23
12
1.341
Diethyl Hexyl Phthalate
3
13
1.362
Fatty Acid Methyl Ester C >_ 24
1
-------
104
TABLE B196
Organic Compounds Identified in Base Extract of Sample No. 63B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.260 Benzothiazole 6
3 1.555 C^ Terpineol 1
4 2.066 Dibutyl Phthalate 1
5 2.424 Butyl Phthalyl Butyl Glycol ate 4
6 2.540 Diethyl Hexyl Phthalate 2
TABLE B197
Volatile Organic Compounds Identified in Sample No. 64S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.882
Tetrahydrofuran
4
2
1.000
Chloroform
10
3
1.081
1,2-Dichloroethane
8
4
1.366
Bromo-Dichloroethane
1
5
1.512
Trichloroeth.ylene
4
6
1.840
?
1
7
1.910
Ethyl-Methyl Dioxolane
1
8
1.986
1,1,2,2-Tetrachloroethane
1
9
2.020
Tetrachloroethylene
2
-------
105
TABLE B198
Organic Compounds Identified in Acid Extract of Sample No. 64A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.416
Methyl-2-Ethyl Hexanoate (IS)
2
0.887
Methyl Myrsitate
2
3
1.000
Methyl Palmitate
6
4
1.091
Methyl Stearate
4
5
1.198
Terpene
3
6
1.219
?
1
7
1.271
Butyl Phthalyl Butyl Glycolate
1
8
1.341
Diethyl Hexyl Phthalate
2
9
1.411
C-|g - Terpineol
1
TABLE B199
Organic Compounds Identified in Base Extract of Sample No. 64B
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
...
2
1.286
Benzothiazole
2
3
1.549
C.|q Terpineol
1
4
2.053
Dibutyl Phthalate
1
5
2.523
Diethyl Hexyl Phthalate
1
6
2.654
C-|g Terpineol
1
-------
106
TABLE B200
Volatile Organic Compounds Identified in Sample No. 65S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.456 Dichloromethane 2
2 0.876 Tetrahydrofuran 15
3 0.957 1,2-Dichloroethylene 3
4 1.000 Chloroform 20
5 1.086 1,2-Dichloroethane 9
6 1.193 1,1,1-Trichloroethane 2
7 1.382 Bromo-Chloroethane 1
8 1.431 1,2-Dichloropropane 1
9 1.522 Trichloroethylene 8
10 1.678 1-Bromo-2-Chloropropane 2
11 1.792 Tribromomethane 2
12 1.846 ? 2
13 1.921 Ethyl-Methyl Dioxolane 8
14 1.991 1,1,2,2-Tetrachloroethane 3
15 2.028 Tetrachloroethylene 6
TABLE B201
Organic Compounds Identified in Acid Extract of Sample No. 65A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.434 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.097 Methyl Stearate 3
4 1.228 ? 1
5 1.280 Butyl Phthalyl Butyl Glycolate 1
6 1.341 Diethyl Hexyl Phthalate 2
-------
107
TABLE B202
Organic Compounds Identified in Base Extract of Sample No. 65B
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 1.000 Camphor (IS)
2 1.177 Bromopropyl Benzene 3
3 1.544 Cp^H,. 2
4 1.595 ? 3
5 1.744 C-|q Camphenol 2
6 1.876 C10 Camphenol 2
7 2.047 Dibutyl Phthalate 1
8 2.511 Diethyl Hexyl Phthalate 1
TABLE B203
Volatile Organic Compounds Identified in Sample No. 66S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.451 Dichloromethane 2
2 0.877 Tetrahydrofuran 15
3 0.957 1,2-Dichloroethylene 2
4 1.000 Chloroform 14
5 1.085 1 ,2-Dichloroethane 9
6 1.186 1,1,1-Trichloroethane 1
7 1.506 Trichloroethylene 8
8 1.655 l-Chloro-2-Bromopropane 1
9 1.773 Tribromomethane 1
10 1.826 ? 1
11 1.895 Ethyl-Methyl Dioxolane 12
12 1.970 1,1,2,2-Tetrachloroethane 2
13 2.007 Tetrachloroethylene 6
-------
108
TABLE B204
Organic Compounds Identified in Acid Extract of Sample No. 66A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.429 Methyl-2-Ethyl Hexanoate (IS)
2 0.670 Trichloroanisole 1
3 0.890 Methyl Myristate 3
4 0.900 Methyl Dichlorophenoxy Acetate 1
5 0.920 Methyl Dichlorophenoxy Acetate 1
6 0.948 Pentachloroanisole 1
7 0.969 Methyl-2(4-chlorophenoxy)Butanoate 2
8 1.000 Methyl Palmitate 8
9 1.009 C-j ^ Terpene 2
10 1.058 ? 2
11 1.101 Methyl Stearate 5
12 1.207 C-| ^ Terpene 3
13 1.231 ? 3
14 1.281 Butyl Phthalyl Butyl Glycolate 19
15 1.345 Diethyl Hexyl Phthalate 2
16 1.369 ? 2
17 1.415 C^ - Terpineol 2
TABLE B205
Organic Compounds Identified in Base Extract of Sample No. 66B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.552 C5HioC12 2
3 1.604 ? 1
4 2.069 Dibutyl Phthalate 2
5 2.424 Butyl Phthalyl Butyl Glycolate 10
6 2.540 Diethyl Hexyl Phthalate 1
-------
109
TABLE B206
Volatile
Organic Compounds Identified in Sample No.
67S
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.459
Dichloromethane
2
2
0.882
Tetrahydrofuran
5
3
1.000
Chioroform
6
4
1.075
1,2-Dichloroethane
8
5
1.182
1,1,1-Trichloroethane
1
6
1.509
Trichloroethylene
8
7
1.652
1-Chloro-2-Bromoethane
3
8
1.777
Tribromomethane
1
9
1.991
Ethyl-Methyl Dioxolane
4
10
1.986
1,1,2,2-Tetrachloroethane
6
11
2.018
Tetrachloroethylene
9
TABLE B207
Organic Compounds Identified in Acid Extract of Sample No. 67A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(PPb)
1
0.440
Methyl-2-Ethyl Hexanoate (IS)
-
2
0.897
Methyl Myristate
1
3
0.953
Fatty Acid Methyl Ester C > 14
1
4
1.000
Methyl Palmitate
10
5
1.051
1
6
1.097
Methyl Stearate
10
7
1.328
Diethyl Hexyl Phthalate
2
8
1.393
C-|g Terpineol
1
9
1.460
?
1
-------
110
TABLE B208
Organic Compounds Identified in Base Extract of Sample No.67B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.562 Diethyl Hexyl Phthalate 2
3 2.688 C-j5 Terpineol 1
4 2.821 ? 1
5 2.975 ? 1
TABLt B2Uy
Volatile Organic Compounds Identified in Sample No. 68S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.439
Dichloromethane
2
2
0.881
Tetrahydrofuran
1
3
0.951
1,2-Dichloroethylene
2
4
1.000
Chloroform
4
5
1.035
1,2-Dichloroethane
1
6
1.183
1,1,1-Trichloroethane
1
7
1.512
Trichloroethylene
4
8
1.975
1,1,2,2-Tetrachloroethane
1
9
2.002
Tetrachloroethylene
4
10
2.056
Dichlorobenzene
8
11
2.179
Dichlorobenzene
8
-------
in
TABLE B210
Organic Compounds Identified in Acid Extract of Sample No. 68A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.422 Methyl-2-Ethyl Hexanoate (IS)
2 0.800 Methyl Laurate 1
3 0.867 Methyl Myristate 2
4 1.000 Methyl Palmitate 6
5 1.027 ? 1
5 1.068 Methyl Stearate 5
6 1.301 Diethyl Hexyl Phthalate 3
TABLE B211
Organic Compounds Identified in Base Extract of Sample No. 68B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.646 Unidentified Phthalate
3 2.024 Dibutyl Phthalate
4 2.439 Diethyl Hexyl Phthalate
5 2.576 Cnc Terpineol
lb
6 2.713 ?
7 2.861 ?
-------
112
TABLE B212
Volatile Organic Compounds Identified in Sample No. 69S
Peak
No.
Relati ve
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.442
Dichloromethane
1
2
0.881
Tetrahydrofuran
1
3
1.000
Chioroform
12
4
1.081
1,2-Dichloroethane
3
5
1.184
1,1,1-Trichloroethane
3
6
1.509
Trichloroethylene
10
7
1.975
1 ,1,2,2-Tetrachloroethane
9
8
2.013
Tetrachloroethylene
8
TABLE B213
Organic Compounds Identified in Acid Extract of Sample No. 69A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(PPb)
1
0.450
Methyl-2-Ethyl Hexanoate (IS)
_ _ _
2
0.800
Methyl Laurate
2
3
0.900
Methyl Myristate
4
4
1.000
Methyl Palmitate
11
5
1.062
Hydrocarbon C > 18
2
6
1.102
Methyl Stearate
9
7
1.204
C-j ^ Terpene
3
8
1.264
Hydrocarbon C > 24
2
9
1.279
Butyl Phthalyl Butyl Glycolate
2
10
1 .339
Diethyl Hexyl Phthalate
2
-------
113
TABLE B214
Organic Compounds Identified in Base Extract of Sample No. 69B
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
1.000
Camphor (IS)
2
2.027
Dibutyl Phthalate
1
3
2.463
Diethyl Hexyl Phthalate
1
4
2.593
C^5 Terpineol
1
5
2.675
Hydrocarbon C > 30
1
6
2.720
?
2
7
2.897
?
2
TABLE B215
Volatile Organic Compounds Identified in Sample No. 70S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.080 1,2-Dichloroethane 2
3 1.514 Trichloroethylene 2
4 2.018 Tetrachloroethylene 4
-------
114
TABLE B216
Organic Compounds Identified in Acid Extract of Sample No. 70A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.445
Methyl-2-Ethyl Hexanoate (IS)
--
2
0.533
Hexachlorobutadiene
1
3
0.895
Methyl Myristate
9
4
0.952
Pentachloroanisole
2
5
1.000
Methyl Palmitate
28
6
1.036
Fatty Acid Methyl Ester C 16
5
7
1.054
Fatty Acid Methyl Ester C ^ 16
7
8
1.105
Methyl Stearate
29
9
1.129
17
10
1.207
C-jg Terpene
7
11
1.219
?
7
12
1.228
Hydrocarbon C > 22
9
13
1.249
Dioctyl Adipate
20
14
1.270
Hydrocarbon C > 22
9
15
1 .285
8utyl Phthalyl Butyl Glycolate
12
16
1.355
Diethyl Hexyl Phthalate
1264
17
1.432
Hydrocarbon C > 26
13
18
1 .456
43
19
1.526
Hydrocarbon C > 28
14
20
1.559
Hydrocarbon C > 30
21
-------
115
TABLE B217
Organic Compounds Identified in Base Extract of Sample No. 70B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.803
Hexachloroethane
1
2
1.000
Camphor (IS)
3
1.028
Hexachlorobutadiene
1
4
1.517
Hydrocarbon C >_ 14
9
5
1.539
Hydrocarbon C > 14
13
6
1.630
Hydrocarbon C ^ 16
12
7
1.730
Hydrocarbon C ^ 16
11
8
1.786
Hydrocarbon C >_ 18
6
9
1.865
Hydrocarbon C 18
11
10
1.910
Hydrocarbon C >_ 18
8
11
1.938
Hydrocarbon C >_18
16
12
2.051
Dibutyl Phthalate
14
13
2.118
Hydrocarbon C > 20
21
14
2.160
Unidentified Phthalate
4
15
2.200
Hydrocarbon C ^ 20
8
16
2.260
Hydrocarbon C > 20
4
17
2.290
Hydrocarbon C ^ 20
4
18
2.326
Dioctyl Adipate
14
19
2.360
Hydrocarbon C 22
3
20
2.398
Butyl Phthalyl Butyl Glycolate
14
21
2.472
Diethyl Hexyl Phthalate
2347
22
2.635
Hydrocarbon C >_ 30
13
23
2.685
?
65
24
2.730
Hydrocarbon C >_ 30
200
25
2.815
Unidentified Phthalate
7
26
2.854
Hydrocarbon C 30
34
27
2.882
Hydrocarbon C 30
13
28
2.921
?
92
-------
116
TABLE B218
Volatile Organic Compounds Identified in Sample No. 71S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.067 1,2-Dichloroethane 2
3 1.444 Trichloroethylene 3
4 1.893 1,1 ,2,2-Tetrachloroethane 1
5 1.924 Tetrachloroethylene 3
-------
117
TABLE B219
Organic Compounds Identified in Acid Extract of Sample No. 71A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.428
Methyl-2-Ethyl Hexanoate (IS)
--
2
0.778
Methyl Laurate
2
3
0.820
C.jQ Terpineol
2
4
0.892
Methyl Myristate
3
5
0.931
Fatty Acid Methyl Ester C 14
1
6
0.946
Pentachloroanisol e
1
7
1.000
Methyl Pal mi tate
9
8
1 .039
Unidentified Phthalate
1
9
1.051
Fatty Acid Methyl Ester C ^ 16
1
10
1.096
Methyl Stearate
11
11
1.201
r Terpene
1 5
1
12
1.245
Dioctyl Adipate
2
13
1.275
Butyl Phthalyl Butyl Glycolate
2
14
1.305
Butyl Benzyl Phthalate
1
15
1.335
Diethyl Hexyl Phthalate
2
16
1.356
Fatty Acid Methyl Ester C > 22
2
17
1.374
Dioctyl Phthalate
2
18
1.400
C.| ^ Terpineol
3
19
1.476
1
2
20
1.559
?
6
-------
118
TABLE B220
Organic Compounds Identified in Base Extract of Sample Mo. 71B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Camphor (IS)
2
1.508
C^0 Terpineol
3
3
1.610
Hydrocarbon C >_ 14
3
4
1.708
Hydrocarbon C > 16
3
5
1.805
Hydrocarbon C > 16
3
6
1.903
Diisobutyl Phthalate
9
7
2.000
Dibutyl Phthalate
20
8
2.038
Diisobutyl Nonanedioate
4
9
2.060
?
8
10
2.069
Hydrocarbon C >_ 20
5
11
2.157
Hydrocarbon C >_ 20
6
12
2.238
Hydrocarbon C >_ 22
9
13
2.270
Dioctyl Adipate
10
14
2.314
Hydrocarbon C ^ 22
5
15
2.335
?
4
16
2.384
Butyl Phthalyl Butyl Glycolate
15
17
2.438
Diethyl Hexyl Phthalate
19
18
2.459
Hydrocarbon C >_ 24
5
19
2.508
Dicyclohexyl Phthalate
7
20
2.529
Hydrocarbon C >_ 26
5
21
2.562
C-jg Terpineol
12
22
2.600
Hydrocarbon C > 26
5
23
2.638
?
6
24
2.670
Hydrocarbon C >_ 28
4
25
2.692
?
8
26
2.746
Hydrocarbon C >_ 28
7
27
2.784
Hydrocarbon C ^ 28
7
28
2.843
7
20
-------
119
TABLE B221
Volatile Organic Compounds Identified in Sample No. 72S
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
1.000
Chioroform
2
2
1.081
1,2-Di chloroethane
2
3
1.514
Trichloroethylene
2
4
1.986
1 ,1 ,2 ,2-Tetrachloroethane
1
5
2.018
Tetrachloroethylene
2
TABLE 8222
Organic Compounds Identified in Acid Extract of Sample No. 72A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.437 Methyl-2-Ethyl Hexanoate (IS)
2 0.882 ? 1
3 0.895 Methyl Myristate 1
4 1.000 Methyl Palmitate 2
5 1.099 Methyl Stearate 3
6 1.277 Butyl Phthalyl Butyl Glycol ate 1
7 1.337 Diethyl Hexyl Phthalate 1
-------
120
TABLE B223
Organic Compounds Identified in Base Extract of Sample No. 72B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
O
o
o
Camphor (IS)
--
2
1.525
C-|q - Terpineol
1
3
2.034
Dibutyl Phthalate
3
4
2.374
Butyl Phthalyl Butyl Glycolate
3
5
2.486
Diethyl Hexyl Phthalate
33
6
2.620
C-|5 Terpineol
3
TABLE B224
Volatile Organic Compounds Identified in Sample No. 73S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.075 1,2-Dichloroethane 1
3 1.504 Trichloroethylene 1
4 2.007 Tetrachloroethylene 1
-------
121
TABLE B225
Organic Compounds Identified in Acid Extract of Sample No. 73A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.433
Methyl-2-Ethyl Hexanoate (IS)
2
0.780
Methyl Laurate
3
3
0.819
C-jq Terpineol
6
4
0.894
Methyl Myristate
2
5
1.000
Methyl Palmitate
7
6
1.096
Methyl Stearate
5
7
1 .338
Diethyl Hexyl Phthalate
1
TABLE B226
Organic Compounds Identified in Base Extract of Sample No. 73B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.517 C-|0 Terpineol 1
3 2.018 Dibutyl Phthalate 1
4 2.463 Diethyl Hexyl Phthalate 1
-------
122
TABLE B227
Volatile Organic Compounds Identified in Sample No. 74S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.080 1,2-Dichloroethane 2
3 1.996 Tetrachloroethylene 1
TABLE B228
Organic Compounds Identified in Acid Extract of Sample No. 74A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.435 Methyl-2-Ethyl Hexanoate (IS)
2 0.813 C.|0 Terpineol 3
3 1.000 Methyl Palmitate 4
4 1.098 Methyl Stearate 3
5 1.330 Diethyl Hexyl Phthalate 5
6 1.402 C-jg Terpineol 1
-------
123
TABLE B229
Organic Compounds Identified in Base Extract of Sample No. 74B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.511 C-|q Terpineol
TABLE B230
Volatile Organic Compounds Identified in Sample No. 75S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Chloroform
2
1.095
1,2-Dichloroethane
3
1.330
Brono-Di chloromethane
4
1.615
Dibromo-Chloromethane
5
2.009
Dichlorobenzene
6
2.103
Toluene
7
2.259
Dichlorobenzene
-------
124
TABLE B231
Organic Compounds Identified in Acid Extract of Sample No. 75A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
0.440
Methyl-2-Ethyl Hexanoate (IS)
_ _ .
2
0.816
C-jq Terpineol
2
3
1.000
Methyl Palmitate
6
4
1.039
Hydrocarbon C > 18
1
5
1.103
Methyl Stearate
4
6
1.139
Hydrocarbon C > 20
1
7
1 .184
Hydrocarbon C > 20
1
8
1.226
Hydrocarbon C > 22
1
9
1.269
Hydrocarbon C > 22
1
10
1.281
Butyl Phthalyl Butyl Glycolate
1
n
1.311
Hydrocarbon C > 24
1
12
1.341
Diethyl Hexyl Phthalate
1
13
1.389
Hydrocarbon C > 26
1
14
1.407
C^ Terpineol
1
TABLE B232
Organic Compounds Identified in Base Extract of Sample No. 75B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.521 C-|q Terpineol 2
3 2.000 Dibutyl Phthalate 1
4 2.486 Diethyl Hexyl Phthalate 1
-------
125
TABLE B233
Volatile Organic Compounds Identified in Sample No. 76S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.554 Trichloroethylene 1
TABLE B234
Organic Compounds Identified in Acid Extract of Sample No. 76A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.440 Methyl-2-Ethyl Hexanoate (IS)
2 0.817 C^q Terpineol 2
3 0.898 Methyl Myristate 1
4 1.000 Methyl Palmitate 3
5 1.099 Methyl Stearate 3
6 1.347 Diethyl Hexyl Phthalate 3
-------
126
TABLE B235
Organic Compounds Identified in Base Extract of Sample No. 76B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.521 C1Q - Terpineol 4
3 2.020 Dibutyl Phthalate 1
4 2.459 Diethyl Hexyl Phthalate 1
5 2.620 C-|5 - Terpineol 1
6 2.711 ? 2
7 2.859 ? 2
TABLE B236
Volatile Organic Compounds Identified in Sample No. 77S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 15
2 1.562 Trichloroethylene 1
-------
127
TABLE B237
Organic Compounds Identified in Acid Extract of Sample No. 77A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.432 Methyl-2-Ethyl Hexanoate (IS)
2 0.780 Methyl Laurate 2
3 0.893 Methyl Myristate 2
4 1.000 Methyl Palmitate 4
5 1.098 Methyl Stearate 3
6 1.333 Diethyl Hexyl Phthalate 1
7 1.399 C-| g Terpineol 1
8 1.467 ? 1
9 1.535 ? 1
TABLE B238
Organic Compounds Identified in Base Extract of Sample No. 77B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.543 C^q - Terpineol 1
3 2.054 Dibutyl Phthalate 1
4 2.508 Diethyl Hexyl Phthalate 1
5 2.766 ? 1
6 2.900 ? 2
-------
128
TABLE B239
Volatile Organic Compounds Identified in Sample No. 78S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 10
2 1.076 1,2-Dichloroethane 5
3 1.519 Trichloroethylene 3
4 1.959 Tetrachloroethylene 2
TABLE B240
Organic Compounds Identified in Acid Extract of Sample No. 78A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.412 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.103 Methyl Stearate 2
4 1.339 Diethyl Hexyl Phthalate 1
TABLE B241
Organic Compounds Identified in Base Extract of Sample No. 78B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.548 C-|Q - Terpineol 1
3 2.062 Dibutyl Phthalate 1
4 2.508 Diethyl Hexyl Phthalate ">
-------
129
TABLE B242
Volatile Organic Compounds Identified in Sample No. 79S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.975 Dichlorobenzene 3
TABLE B243
Organic Compounds Identified in Acid Extract of Sample No. 79A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.435
Methyl-2-Ethyl Hexanoate (IS)
2
0.816
C^q Terpineol
1
3
1.000
Methyl Palmitate
2
4
1.098
Methyl Stearate
2
5
1.321
Diethyl Hexyl Phthalate
1
TABLE B244
Organic Compounds Identified in Base Extract of Sample No. 79B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.516 C-jg - Terpineol 3
3 2.027 Dibutyl Phthalate 1
4 2.457 Diethyl Hexyl Phthalate 1
-------
130
TABLE B245
Volatile Organic Compounds Identified in Sample No. 80S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(PPb)
1
1.000
Chloroform
2
TABLE B246
Organic Compounds Identified in Acid Extract of Sample No. 80A
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 0.435 Methyl-2-Ethyl Hexanoate (IS)
2 0.818 Ciq Terpineol 4
3 0.869 C15 Alcohol 4
4 0.922 C16 Alcohol 3
5 0.976 C]7 Alcohol 1
6 1.000 Methyl Palmitate 5
7 1.027 C18 Alcohol 1
8 1.078 Cig Alcohol 1
9 1.093 Methyl Stearate 3
10 * 1.164 C2Q Alcohol 1
11 1.206 C21 Alcohol 1
12 1.248 C22 Alcohol 1
13 1.343 Diethyl Hexyl Phthalate 1
-------
131
TABLE B247
Organic Compounds Identified in Base Extract of Sample No. 80B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.667 Diethyl Hexyl Phthalate 1
3 2.800 C-jg - Terpineol 1
4 2.981 ? 1
5 3.095 ? 1
TABLE B248
Volatile Organic Compounds Identified in Sample No. 81S
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 1.000 Chloroform 14
2 1.528 Trichloroethylene 2
-------
132
TABLE B249
Organic Compounds Identified in Acid Extract of Sample No. 81A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.450 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.098 Methyl Stearate 3
4 1.260 Methyl Dehydroabietate 1
5 1.328 Diethyl Hexyl Phthalate 1
6 1.396 Ci5 Terpineol 1
7 1.461 ? 1
8 1.541 ? 1
TABLE B250
Organic Compounds Identified in Base Extract of Sample No. 81B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.508 Diethyl Hexyl Phthalate 1
3 2.635 C15 - Terpineol 1
4 2.773 ? ฐ>
5 2.945 ? 3
-------
133
TABLE B251
Volatile Organic Compounds Identified in Sample No.
82S
Relative
Approximate
Peak
Retention
Level
No.
Time Compound
(ppb)
1
1.000 Chloroform
12
TABLE B252
Organic Compounds Identified in Acid Extract of Sample
No. 82A
Relative
Approximate
Peak
Retention
Level
No.
Time Compound
(PPb)
1
0.345 Methyl-2-Ethyl Hexanoate (IS)
2
1.000 Methyl Palmitate
1
3
1.101 Methyl Stearate
2
4
1.348 Diethyl Hexyl Phthalate
4
TABLE B253
Organic Compounds Identified in Base Extract of Sample No. 82B
Relative
Approximate
Peak
Retention
Level
No.
Time Compound
(PPb)
1
1.000 Camphor (IS)
...
2
1 .565 C-jg - Terpineol
1
3
2.102 Dibutyl Phthalate
1
4
2.579 Diethyl Hexyl Phthalate
1
-------
134
TABLE B254
Volatile Organic Compounds Identified in Sample No. 83S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
2 1.500 Trichloroethylene 2
TABLE B255
Organic Compounds Identified in Acid Extract of Sample No. 83A
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 0.424 Methyl-2-Ethyl Hexanoate (IS)
2 0.819 C-|g Terpineol 2
3 0.890 Methyl Myristate 1
4 1.000 Methyl Palmitate 5
5 1.104 Methyl Stearalte 4
6 1.347 Diethyl Hexyl Phthalate 1
7 1.415 C15 Terpineol 1
-------
135
TABLE B256
Organic Compounds Identified in Base Extract of Sample No. 83B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.528 Diethyl Hexyl Phthalate 1
TABLE B257
Volatile Organic Compounds Identified in Sample No. 84S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.498 Trichloroethylene 1
TABLE B258
Organic Compounds Identified in Acid Extract of Sample No. 84A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.430 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.105 Methyl Stearate 2
4 1.354 Diethyl Hexyl Phthalate 1
-------
136
TABLE B259
Organic Compounds Identified in Base Extract of Sample No. 84B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE 8260
Volatile Organic Compounds Identified in Sample No. 85S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.958
Dichloroethylene
1
2
1.000
Chloroform
2
3
1.078
1,2-Dichloroethane
1
4
1.182
1,1,1-Trichloroethane
1
5
1.506
Trichloroethylene
3
6
1.980
1,1,2,2-Tetrachloroethane
1
7
2.017
Tetrachloroethyl ene
3
f
/
I
-------
137
TABLE B261
Organic Compounds Identified in Acid Extract of Sample No. 85A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.100 Methyl Stearate 5
4 1.347 Diethyl Hexyl Phthalate 2
TABLE B262
Organic Compounds Identified in Base Extract of Sample No. 85B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.558 C-|g - Terpineol 2
3 2.024 Diphenyl Benzene 1
4 2.070 Dibutyl Phthalate 1
5 2.535 Diethyl Hexyl Phthalate 2
-------
138
TABLE B263
Volatile Organic Compounds Identified in Sample No. 86S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.431
Dichloromethane
1
2
0.879
Tetrahydrofuran
1
3
0.953
Dichloroethylene
1
4
1.000
Chloroform
10
5
1.079
1,2-Dichloroethane
1
6
1.184
1,1,1-Trichloroethane
1
7
1.511
Trichloroethylene
5
8
1.991
1,1,2,2-Tetrachloroethane
3
9
2.028
Tetrachloroethylene
12
-------
139
TABLE B264
Organic Compounds Identified in Acid Extract of Sample No. 86A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.419
Methyl-2-Ethyl Hexanoate (IS)
2
0.666
Trichloroanisole
1
3
0.766
Methyl Laurate
1
4
0.888
Methyl Myristate
5
5
0.899
Methyl Dichlorophenoxy Acetate
6
6
0.927
Methyl Dichlorophenoxy Acetate
5
7
0.967
Methyl-Trichlorophenoxy Acetate
5
8
1.000
Methyl PaImitate
10
9
1.061
?
2
10
1.103
Methyl Stearate
11
11
1.139
Diphenyl Sulfone
4
12
1.207
C1 6H10
8
13
1.234
?
6
14
1.271
Methyl Dehydroabietate
5
15
1.350
Diethyl Hexyl Phthalate
24
16
1.416
C,c Terpi neol
1 D
1
-------
140
TABLE B265
Organic Compounds Identified in Base Extract of Sample No. 86B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Camphor (IS)
2
1.574
C-jq - Terpineol
4
3
1.734
Diethyl Phthalate
5
4
2.013
Diisobutyl Phthalate
4
5
2.119
Dibutyl Phthalate
5
6
2.208
?
2
7
2.552
Unidentified Phthalate
1
8
2.611
Diethyl Hexyl Phthalate
15
9
2.741
C-|5 - Terpineol
1
10
2.877
?
2
11
3.049
?
5
TABLE B266
Volatile Organic Compounds Identified in Sample No. 87S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.084 1,2-Dichloroethane 1
3 1.511 Trichloroethylene 1
4 2.027 Tetrachloroethylene 1
-------
141
TABLE B267
Organic Compounds Identified in Acid Extract of Sample No. 87A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
Methyl-2-Ethyl Hexanoate (IS)
Methyl Laurate 1
C.JQ Terpineol 2
Methyl Myristate 1
Pentachloroanisole 1
Methyl Palinitate 8
Methyl Stearate 8
Diethyl Hexyl Phthalate 1
C-jcj Terpineol 1
1
0.425
2
0.765
3
0.814
4
0.887
5
0.945
6
1.000
7
1.104
8
1.351
9
1 .421
TABLE B268
Organic Compounds Identified in Base Extract of Sample No. 87B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.071 Dibutyl Phthalate 1
3 2.562 Diethyl Hexyl Phthalate 10
4 2.828 ? 2
5 2.990 ? 2
-------
142
TABLE B269
Volatile Organic Compounds Identified in Sample No. 88S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.456 Dichloromethane 1
2 0.954 Dichloroethylene 1
3 1.000 Chloroform 8
4 1.483 Trichloroethylene 10
5 1.777 Bromobenzene 7
6 1.970 Tetrachloroethylene
TABLE B270
Organic Compounds Identified in Acid Extract of Sample No. 88A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.425 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.099 Methyl Stearate 1
4 1.268 Methyl Dehydroabietate 4
5 1.341 Diethyl Hexyl Phthalate 1
6 1.410 C-j g Terpineol 1
-------
143
TABLE B271
Organic Compounds Identified in Base Extract of Sample No. 88B
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Camphor (IS)
2
2.539
Diethyl Hexyl Phthalate
1
3
2.636
Hydrocarbon C >_ 26
2
4
2.676
C-|5 - Terpineol
2
TABLE B272
Volatile Organic Compounds Identified in Sample No.
89 S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.927
Dichloroethylene
1
2
1.000
Chioroform
4
3
1.084
1,2-Dichloroethane
1
4
1.138
Pentane
1
5
1.222
Cyclohexane
1
6
1.576
Trichloroethylene
1
7
2.128
Tetrachloroethylene
1
8
2.382
Dichlorobenzene
12
-------
144
TABLE B273
Organic Compounds Identified in Acid Extract of Sample No. 89A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.408
Methyl-2-Ethyl Hexanoate (IS)
2
0.851
?
1
3
0.888
Methyl Myristate
1
4
1.000
Methyl Palmitate
3
5
1.103
Methyl Stearate
2
6
1.348
Diethyl Hexyl Phthalate
1
7
1 .417
C-| 5 Terpineol
1
TABLE B274
Organic Compounds Identified in Base Extract of Sample No.89B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.639 Diethyl Hexyl Phthalate
-------
145
TABLE B275
Volatile Organic Compounds Identified in Sample No.90S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.136 Pentane 1
TABLE B276
Organic Compounds Identified in Acid Extract of Sample No.90A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
0.402
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
5
3
1.108
Methyl Stearate
3
4
1.354
Diethyl Hexyl Phthalate
1
TABLE B277
Organic Compounds Identified in Base Extract of Sample No.90B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.125 Dibutyl Phthalate 3
3 2.617 Diethyl Hexyl Phthalate 2
4 2.253 C^ - Terpineol 2
-------
146
TABLE B278
Volatile Organic Compounds Identified in Sample No. 91S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.195 Cyclohexane 1
3 1.663 Hexane 1
TABLE B279
Organic Compounds Identified in Acid Extract of Sample No. 91A
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.361
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
5
3
1.012
C^ Terpene
2
4
1.106
Methyl Stearate
8
5
1.119
C-jg Terpene
2
6
1.213
C-jg Terpene
1
7
1.353
Diethyl Hexyl Phthalate
1
-------
147
TABLE B280
Organic Compounds Identified in Base Extract of Sample No. 91B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.594 Diethyl Hexyl Phthalate 1
3 2.728 C15 - Terpineol 2
TABLE B281
Volatile Organic Compounds Identified in Sample No. 92S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 31
2 1.214 Cyclohexane 2
3 1.573 Trichloroethylene 1
-------
148
TABLE B282
Organic Compounds Identified in Acid Extract of Sample No. 92A
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(PPb)
1
0.400
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
4
3
1.102
Methyl Stearate
2
4
1.121
C^ Terpene
2
5
1.210
C^ Terpene
1
TABLE B283
Organic Compounds Identified in Base Extract of Sample No. 92B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.111 Dibutyl Phthalate 1
3 2.595 Diethyl Hexyl Phthalate 1
4 2.734 C^ - Terpineol 1
TABLE B284
Volatile Organic Compounds Identified in Sample No.93S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(PPb)
1
1.212
Cyclohexane
1
-------
149
TABLE B285
Organic Compounds Identified in Acid Extract of Sample No. 93A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.399 Methyl-2-Ethyl Hexanoate (IS)
2 0.888 Methyl Myristate 2
3 1.000 Methyl Palmitate 8
4 1.015 C-j 5 Terpene 1
5 1.104 Methyl Stearate 2
6 1.121 C-j ^ Terpene 3
7 1.212 C15 Terpene 4
8 1.348 Diethyl Hexyl Phthalate 1
TABLE B286
Organic Compounds Identified in Base Extract of Sample No.93B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.294 C-jg Hydrocarbon
3 1.413 C^g Hydrocarbon
4 1.531 C^ Hydrocarbon
5 .2.527 Diethyl Hexyl Phthalate
6 2.651 C.|g - Terpineol
-------
150
TABLE B287
Volatile Organic Compounds Identified in Sample No.94S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 30
2 1.211 Cyclohexane + 1,1,1-Trichloroethane 1
3 1.349 Bromo-Dichloromethane 3
4 2.007 Toluene 1
TABLE B288
Organic Compounds Identified in Acid Extract of Sample No. 94A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.229 Dichlorobutane 3
2 0.341 Dichlorobutane 1
3 0.400 Methyl-2-Ethyl Hexanoate (IS)
4 0.416 Dichlorobutane 1
5 0.498 Trichloropentane 1
6 0.688 C-|5 Hydrocarbon 1
7 0.752 C-jg Hydrocarbon 1
8 0.816 C.|7 Hydrocarbon 1
9 1.000 Methyl Palmitate 1
10 1.351 Diethyl Hexyl Phthalate 1
-------
151
TABLE B289
Organic Compounds Identified in Base Extract of Sample No. 94B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Camphor (IS)
2
1.429
C-jg Hydrocarbon
1
3
1.544
C-j y Hydrocarbon
1
4
2.550
Diethyl Hexyl Phthalate
1
5
2.649
C-| 5 Terpineol
1
TABLE B290
Volatile Organic Compounds Identified in Sample No.95S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.211
Cyclohexane + 1,1,1-Trichloroethane
1
-------
152
TABLE B291
Organic Compounds Identified in Acid Extract of Sample No.95A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.221
Dichlorobutane
1
2
0.340
Dichlorobutane
1
3
0.421
Methyl-2-Ethyl Hexanoate (IS)
4
0.689
C-|5 Hydrocarbon
1
5
0.755
C^g Hydrocarbon
1
6
0.814
C^ Hydrocarbon
1
7
0.880
Methyl Myristate
1
8
1.000
Methyl Palmitate
6
9
1.009
C-jg Terpene
2
10
1.102
Methyl Stearate
2
11
1.116
C^ Terpene
5
12
1.206
C-jg Terpene
4
13
1.281
Butyl Phthalyl Butyl Glycolate
2
14
1.340
Diethyl Hexyl Phthalate
1
-------
153
TABLE B292
Organic Compounds Identified in Base Extract of Sample No.95B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1 .000
Camphor (IS)
--
2
1.531
C-|7 Hydrocarbon
1
3
2.056
Dibutyl Phthalate
1
4
2.405
Butyl Phthaiyl Butyl Glycolate
1
5
.2.515
Diethyl Hexyl Phthalate
2
6
2.642
C^5 - Terpineol
1
TABLE B293
Volatile Organic Compounds Identified in Sample No. 96S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chioroform
1
2
1.211
Cyclohexane + 1,1,1-Trichloroethane
1
3
1.567
Tri chloroethylene
13
4
2.005
Toluene
1
-------
154
TABLE B294
Organic Compounds Identified in Acid Extract of Sample No. 96A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.433 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 2
4 1.343 Diethyl Hexyl Phthalate 1
TABLE B295
Organic Compounds Identified in Base Extract of Sample No.96B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B296
Volatile Organic Compounds Identified in Sample No.97S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.181
Cyclohexane
1
-------
155
TABLE B297
Organic Compounds Identified in Acid Extract of Sample No. 97A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
0.361
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
2
3
1.106
Methyl Stearate
1
4
1.120
C15 Terpene
1
5
1.212
Terpene
1
6
1.285
Butyl Phthalyl Butyl Glycolate
1
7
1.350
Diethyl Hexyl Phthalate
1
TABLE B298
Organic Compounds Identified in Base Extract of Sample No.97B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.125 Dibutyl Phthalate 2
3 2.493 Butyl Phthalyl Butyl Glycolate 36
4 2.617 Diethyl Hexyl Phthalate 2
5 2.747 Ci5 " TerP"ineol 1
-------
156
TABLE B299
Volatile Organic Compounds Identified in Sample No. 985
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.175 Cyclohexane
TABLE B300
Organic Compounds Identified in Acid Extract of Sample No. 98A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.402 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.288 Butyl Phthalyl Butyl Glycol ate 4
4 1.346 Diethyl Hexyl Phthalate 1
TABLE B301
Organic Compounds Identified in Base Extract of Sample No.98B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.615 Diethyl Hexyl Phthalate 1
3 2.752 C^ - Terpineol 1
-------
157
TABLE B302
Volatile Organic Compounds Identified in Sample No.99S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.174 Cyclohexane 4
TABLE B303
Organic Compounds Identified in Acid Extract of Sample No. 99A
Relative
Approximate
Peak
Retention
Level
No.
T ime
Compound
(ppb)
1
0.379
Methyl-2-Ethyl Hexanoate (IS)
2
0.663
Trichloroanisole
1
3
1.000
Methyl Palmitate
3
4
1.104
Methyl Stearate
2
5
1.346
Diethyl Hexyl Phthalate
1
6
1 .367
Fatty Acid Methyl Ester C ^ 24
1
7
1.416
C,c Terpineol
1 b
1
-------
158
TABLE B304
Organic Compounds Identified in Base Extract of Sample No.99B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.530 Diethyl Hexyl Phthalate 1
3 2.657 C-|^ - Terpineol 1
TABLE B305
Volatile Organic Compounds Identified in Sample No. 100S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.433
Ethanethiol
19
2
0.491
Acetone
1
3
0.857
Di-isopropyl Ether
1
4
1.000
Chioroform
46
5
1.079
Butanal
6
6
1.159
Cyclohexane
2
7
1.424
Dimethyl Disulfide
19
8
1 .466
Benzene + Trichloroethylene
1
9
2.155
C-jq Terpene
1
10
2.187
C-jq Terpene
85
-------
159
TABLE B306
Organic Compounds Identified in Acid Extract of Sample No.lOOA
Relative Approximate
Peak Retention Level
Mo. Time Compound (ppb)
1
0.610
Hydrocarbon C > 14
1
2
0.662
C15H24
8
3
0.670
Hydrocarbon C > 16
1
4
0.752
Hydrocarbon C > 16
1
5
0.770
Fatty Acid Methyl Ester C 12
1
6
0.802
Hydrocarbon C > 18
1
7
0.811
Hydrocarbon C > 18
5
8
0.871
Hydrocarbon C > 18
6
9
0.886
Fatty Acid Methyl Ester C 14
7
10
0.907
Tetrachloroanisole
1
11
0.931
Hydrocarbon C > 20
1
12
0.943
Fatty Acid Methyl Ester C > 15 +
Pentachloroanisole ~~
4
13
0.976
Fatty Acid Methyl Ester C > 15
2
14
1.985
Hydrocarbon C > 20
1
15
1.000
Methyl Palmitate
34
16
1.033
Fatty Acid Methyl Ester C > 16
12
17
1.051
Fatty Acid Methyl Ester C > 17
7
18
1.099
Methyl Stearate
62
19
1.138
Hydrocarbon C > 22
13
20
1.150
Fatty Acid Methyl Ester C 19
5
21
1.156
Terpene C 15
5
22
1.171
^21^32^2 Pimarate Isomer
16
23
1.186
^21^32^2 Methy] Pimarate Isomer
27
24
1.201
Fatty Acid Methyl Ester C 20
58
25
1.210
^21H32^2 Pimarate Isomer
18
26
1.224
^21^32^2 Pimarate Isomer
22
27
1.236
^21^32^2 Pimarate Isomer
36
28
1.275
?
340
29
1.305
?
5
30
1.311
?
5
31
1.326
Fatty Acid Methyl Ester C > 23
8
-------
160
TABLE B306, cont.
Organic Compounds Identified in Acid Extract of Sample No.lOOA (continued)
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
32
1.344
Diethyl Hexyl Phthalate
18
33
1.365
Fatty Acid Methyl Ester C > 24
36
34
1.383
?
16
35
1.398
?
18
36
1.404
?
18
37
1.413
Terpineol C 15
8
38
1.425
?
10
39
1.443
Fatty Acid Methyl Ester C > 26
12
40
1.478
?
5
41
1.569
^21^32^2 Pimarate Isomer
3
-------
161
TABLE B307
Organic Compounds Identified in Base Extract of Sample No.lOOB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.384
Diterpene C^H^
9
2
0.520
Diterpene C-jgH^g
6
3
0.627
Diterpene
3
4
0.881
Terpineol C 10
13
5
0.994
Hydroxylborneol
31
6
1.000
Camphor
7
1 .041
Diterpene C^H^
59
8
1.101
Dimethyl Styrene
29
9
1.136
Hydrocarbon C > 14
1
10
1.189
Hydrocarbon C > 14
27
11
1.255
Hydrocarbon C > 14
1
12
1.279
Triterpene
12
13
1.326
Hydrocarbon C > 14
14
14
1.397
Triterpene C-j^^
24
15
1.456
Hydrocarbon C > 16
17
16
1.498
Hydrocarbon C > 16
24
17
1.563
Hydrocarbon C > 16
50
18
1.581
Hydrocarbon C > 16
2
19
1.622
Triterpene
2
20
1.699
Hydrocarbon C > 18
23
21
1.770
?
3
22
1.812
Hydrocarbon C > 18
15
23
1.924
Hydrocarbon C 20
18
24
1.948
Terpene C 15
5
25
1.996
Hydrocarbon C > 20
9
26
2.031
Hydrocarbon C >_ 20
12
27
2.061
?
3
28
2.078
?
3
29
2.132
Hydrocarbon C >_ 22
12
30
2.144
Dibutyl Phthalate
10
31
2.209
?
10
-------
162
TABLE B307, cont.
Organic Compounds Identified in Base Extract of Sample No.lOOB (continued)
Peak
No.
Relati ve
Retenti on
Time
Compound
Approximate
Level
(ppb)
32
2.245
Hydrocarbon C > 22
3
33
2.256
?
7
34
2.292
?
2
35
2.345
Hydrocarbon C > 24
10
36
2.376
Hydrocarbon C > 24
7
37
2.384
?
51
38
2.404
Hydrocarbon C > 24
3
39
2.422
?
40
40
2.434
?
4
41
2.446
?
5
42
2.570
Hydrocarbon C > 26
3
43
2.630
Diethyl Hexyl Phthalate
3
44
2.750
Terpineol C 15
3
-------
163
TABLE B308
Volatile Organic Compounds Identified in Sample No. 101S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.176 Cyclohexane 1
TABLE B309
Organic Compounds Identified in Acid Extract of Sample No.lOlA
Relative
Approximate
Peak
Retenti on
Level
No.
T i me
Compound
(ppb)
1
0.412
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
5
3
1.103
Methyl Stearate
3
4
1.212
C-|^ Terpene
1
5
1.288
Butyl Phthalyl Butyl Glycolate
3
6
1.352
Diethyl Hexyl Phthalate
1
-------
164
TABLE B310
Organic Compounds Identified in Base Extract of Sample No.lOlB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.541 Diethyl Hexyl Phthalate 1
3 2.666 C^ - Terpineol 1
TABLE B311
Volatile Organic Compounds Identified in Sample No. 102S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.265 Dioxolane 1
3 1.821 Bromobenzene 20
-------
165
TABLE B312
Organic Compounds Identified in Acid Extract of Sample NO.102A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.415 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.064 ? 1
4 1.106 Methyl Stearate 2
5 1.237 ? 2
6 1.349 Diethyl Hexyl Phthalate 2
7 1.415 C-jg Terpineol 1
TABLE B313
Organic Compounds Identified in Base Extract of Sample No.102B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.535 Diethyl Hexyl Phthalate
-------
166
TABLE B314
Volatile Organic Compounds Identified in Sample No. 1035
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.074 1,2-Dichloroethane 1
3 1.554 Dichlorobenzene 1
4 1.644 Dichlorobenzene 21
TABLE B315
Organic Compounds Identified in Acid Extract of Sample NO.103A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.423 Methyl-2-Ethyl Hexanoate (IS)
2 0.888 Methyl Myrsitate 1
3 1.000 Methyl Palmitate 2
4 1.106 Methyl Stearate 1
-------
167
TABLE B316
Organic Compounds Identified in Base Extract of Sample No. 103B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B317
Volatile Organic Compounds Identified in Sample NO.104S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Chloroform
1
2
1.073
1,2-Dichloroethane
1
3
1.477
Tri chloroethylene
1
4
1.964
Tetrachloroethylene
2
5
2.100
Acetophenone
1
-------
168
TABLE B318
Organic Compounds Identified in Acid Extract of Sample No.l04A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.213
Dichlorobutane
13
2
0.332
Dichlorobutane
1
3
0.405
Methyl-2-Ethyl Hexanoate (IS)
--
4
0.463
Dichlorobutane
4
5
0.494
Tri chlorobutane
185
6
0.567
Trichloropentene
92
7
0.619
Trichlorohexane
31
8
0.683
Dichloroheptane
4
9
0.777
Trichlorohexane
1
10
1.000
Methyl Palmitate
3
11
1.106
Methyl Stearate
2
12
1.348
Diethyl Hexyl Phthalate
1
TABLE B319
Organic Compounds Identified in Base Extract of Sample No. 104B
Relative Approximate
Peak Retention Level
No. Time Compound. (ppb)
No peaks over 1 PPB.
-------
169
TABLE B320
Volatile Organic Compounds Identified in Sample No.l05S
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
1.000
Chloroform
3
2
1.076
1,2-Dichloroethane
2
3
1.238
Carbon Tetrachloride
2
4
1.433
Trichloropropane
1
5
1.514
Trichloroethylene
3
6
2.022
Tetrachloroethyl ene
22
TABLE B321
Organic Compounds Identified in Acid Extract of Sample No.105A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(PPb)
1
0.391
Methyl-2-Ethyl Hexanoate
(IS)
2
0.887
Methyl Myristate
3
3
0.945
Pentachloroanisole
2
4
1.000
Methyl Palmitate
4
5
1.064
?
1
6
1.104
Methyl Stearate
4
7
1.141
?
1
8
1.205
^21^32^2 Methyl P1'rriarate
Isomer
1
9
1.229
*"21^32^2 Methyl Pimarate
Isomer
2
10
1.242
?
5
11
1.278
Methyl Dihydroabietate
5
12
1.352
Diethyl Hexyl Phthalate
2
13
1.376
Fatty Acid Methyl Ester C
1 22
1
14
1.422
C,r Terpineol
2
-------
170
TABLE B322
Organic Compounds Identified in Base Extract of Sample No. 105B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.843
?
1
2
1.000
Camphor (IS)
__
3
1.106
?
3
4
1.285
N,N-Diethylaniline
3
5
1.319
Chloroprene Dimer
3
6
1.676
Diethyl Phthalate
2
7
2.040
Dibutyl Phthalate
1
8
2.498
Diethyl Hexyl Phthalate
1
TABLE B323
Volatile Organic Compounds Identified in Sample N0.IO6S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 5
2 2.007 Tetrachloroethylene 5
3 2.078 C8Hu 1
-------
171
TABLE B324
Organic Compounds Identified in Acid Extract of Sample No.106A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.397 Methyl-2-Ethyl Hexanoate (IS)
2 0.550 CgH-jg Isomer 3
3 0.894 Methyl Myristate 2
4 0.948 Pentachloroanisole 2
5 0.985 ? 4
6 1.000 Methyl Palmitate 6
7 1.106 Methyl Stearate 6
8 1.139 ? 1
9 1.203 Fatty Acid Methyl Ester C >_ 20 1
10 1.230 ? 1
11 1.252 Methyl Dehydroabietate 1
12 1.261 Butyl Phthalyl Butyl Glycol ate 1
13 1.348 Diethyl Hexyl Phthalate 2
14 1.370 Fatty Acid Methyl Ester C > 22 1
15 1.418 C-|^ Terpineol 2
16 1.449 Fatty Acid Methyl Ester C >_ 24 1
-------
172
TABLE B325
Organic Compounds Identified in Base Extract of Sample No. 106B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.531
CgH-jg Isomer
3
2
0.830
?
1
3
1.000
Camphor (IS)
4
1.107
?
1
5
1.322
Chloroprene Isomer
1
6
1.508
Hydrocarbon C >_ 16
2
7
1.571
Dinitrotoluene
22
8
1.662
7
17
9
1.690
7
20
10
1.769
7
5
11
1.865
7
2
12
2.051
Dibutyl Phthalate
1
13
2.086
Caffeine
1
14
2.408
Butyl Phthalyl Butyl Glycolate
1
15
2.465
Hydrocarbon C >_ 28
1
16
2.521
Diethyl Hexyl Phthalate
17
2.544
Hydrocarbon C >_ 29
1
18
2.617
Hydrocarbon C > 30
1
19
2.645
C^ Terpineol
20
2.685
Hydrocarbon C > 31
1
21
2.758
Hydrocarbon C >_ 32
1
22
2.837
Hydrocarbon C > 33
1
23
2.922
Hydrocarbon C ^ 34
1
24
2.970
Hydrocarbon C > 35
1
-------
173
TABLE B326
Volatile Organic Compounds Identified in Sample No. 107S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 5
2 1.492 Trichloroethylene 1
3 1.991 Tetrachloroethylene 2
TABLE B327
Organic Compounds Identified in Acid Extract of Sample No.T07A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.414 Methyl-2-Ethy1 Hexanoate (IS)
2 0.887 Methyl Myristate 1
3 1.000 Methyl Palmitate 3
4 1.107 Methyl Stearate 4
5 1.293 Fatty Acid Methyl Ester C 22 1
6 1.375 ? 1
-------
174
TABLE B328
Organic Compounds Identified in Base Extract of Sample No.l07B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.484 ? 1
3 2.541 Diethyl Hexyl Phthalate 3
4 2.666 C-| 5 Terpineol 1
TABLE B329
Volatile Organic Compounds Identified in Sample N0.IO8S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform
2 1.517 Trichloroethylene 2
-------
175
TABLE B330
Organic Compounds Identified in Acid Extract of Sample N0.IO8A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.439 Methyl-2-Ethyl Hexanoate (IS)
2 0.900 Methyl Myristate 2
3 1.000 Methyl Palmitate 5
4 1.121 Methyl Stearate 3
5 1.230 Terpene 2
TABLE B331
Organic Compounds Identified in Base Extract of Sample No. 108B
Relative
Peak Retention
No. Time Compound
1 1.000 Camphor (IS)
2 1.740 Diethyl Phthalate 4
3 2.431 Butyl Phthalyl Butyl Glycol ate 2
Approximate
Level
(ppb)
-------
176
TABLE B332
Volatile Organic Compounds Identified in Sample No.1095
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
1.000
Chloroform
1
TABLE B333
Organic Compounds Identified in Acid Extract of Sample No.l09A
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.425
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
3
3
1.104
Methyl Stearate
2
4
1.208
C-|g Terpene
2
TABLE B334
Organic Compounds Identified in Base Extract of Sample No. 109B
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(ppb)
1
2
3
1.000
2.129
2.618
Camphor (IS)
Dibutyl Phthalate
Diethyl Hexyl Phthalate
1
1
-------
177
TABLE B335
Volatile Organic Compounds Identified in Sample No.llOS
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.024 1,2-Dichloroethane 1
3 1.317 Bromo-Dichloromethane 2
4 1.778 Bromobenzene 13
TABLE B336
Organic Compounds Identified in Acid Extract of Sample No.llOA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.105 Methyl Stearate 1
4 1.350 Diethyl Hexyl Phthalate 1
-------
178
TABLE B337
Organic Compounds Identified in Base Extract of Sample No. HOB
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
No peaks over 1 PPB.
TABLE B338
Volatile Organic Compounds Identified in Sample No. Ills
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.900 Dichloroethylene 4
2 1.000 Chloroform 10
3 1.068 1,2-Dichloroethane 2
4 , 1.548 ? 1
-------
179
TABLE B339
Organic Compounds Identified in Acid Extract of Sample No.lllA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.411 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 5
3 1.102 Methyl Stearate 2
4 1.346 Diethyl Hexyl Phthalate 2
TABLE B340
Organic Compounds Identified in Base Extract of Sample No. 111B
p i R^la tive Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.569 Diethyl Hexyl Phthalate 2
3 2.700 C-jj. Terpineol 2
4 2.837 ? 1
5 3.001 ? 1
-------
180
TABLE B341
Volatile Organic Compounds Identified in Sample No. 112S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.074 1,2-Dichloroethane 1
3 1.400 Trichloropropane 1
4 1.801 Dichlorobenzene 12
5 1.896 Dichlorobenzene 8
6 2.096 Dichlorobenzene 15
TABLE B342
Organic Compounds Identified in Acid Extract of Sample N0.112A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.376 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.105 Methyl Stearate 1
4 1.346 Diethyl Hexyl Phthalate 1
-------
181
TABLE B343
Organic Compounds Identified in Base Extract of Sample No. 112B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.943 Atrazine 1
3 2.617 Diethyl Hexyl Phthalate 2
TABLE B344
Volatile Organic Compounds Identified in Sample No. 113S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.069 1,2-Dichloroethane 2
3 1.408 Trichloropropane 1
4 1.482 Trichloroethylene 1
5 1.930 Tetrachloroethylene 7
-------
182
TABLE B345
Organic Compounds Identified in Acid Extract of Sample No.113A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.415 Methyl -2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.102 Methyl Stearate 1
TABLE B346
Organic Compounds Identified in Base Extract of Sample No. 113B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.573 Diethyl Hexyl Phthalate 1
-------
183
TABLE B347
Volatile Organic Compounds Identified in Sample No. 1145
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.067 1,2-Dichl oroethane 1
3 1.392 Trichl oropropane 1
4 1.950 Tetrachloroethylene 2
TABLE B348
Organic Compounds Identified in Acid Extract of Sample No.114A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.426 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate <1
3 1.099 Methyl Stearate 1
-------
184
TABLE B349
Organic Compounds Identified in Base Extract of Sample No. 114B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.045 Dibutyl Phthalate 2
TABLE B350
Volatile Organic Compounds Identified in Sample Mo. 115S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 87
2 1.068 1,2-Dichloroethane 1
3 1.304 Bromo-Dichloromethane 8
4 1.403 Trichloropropane 1
5 1.477 Trichloroethylene 1
6 1.555 Dibromo-Chloromethane 4
7 1.964 Tetrachloroethylene 1
-------
185
TABLE B351
Organic Compounds Identified in Acid Extract of Sample No.llSA
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl -2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
TABLE B352
Organic Compounds Identified in Base Extract of Sample No. 115B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.079 Dibutyl Phthalate
TABLE B353
Volatile Organic Compounds Identified, in Sample N0.116S
Relative Approximate
>eak Retention fhl
No. Time Compound (.PP&;
1 1.000 Chloroform 1
2 1.068 1,2-Dichloroethane 1
-------
186
TABLE B354
Organic Compounds Identified in Acid Extract of Sample N0.II6A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.425 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.104 Methyl Stearate 1
TABLE B355
Organic Compounds Identified in Base Extract of Sample No. 116B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B356
Volatile Organic Compounds Identified in Sample No.117S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
187
TABLE B357
Organic Compounds Identified in Acid Extract of Sample No. 117A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.440 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate
TABLE B358
Organic Compounds Identified in Base Extract of Sample No. 117B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.614 C-|^ Terpineol 1
TABLE B359
Volatile Organic Compounds Identified in Sample No. 118S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.627 Bromobenzene 10
-------
188
TABLE B360
Organic Compounds Identified in Acid Extract of Sample N0.II8A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.428 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.097 Dibutyl Phthalate 1
4 1.103 Methyl Stearate 4
5 1.344 Diethyl Hexyl Phthalate 3
TABLE B361
Organic Compounds Identified in Base Extract of Sample No. 118B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
189
TABLE B362
Volatile Organic Compounds Identified in Sample No. 119S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.471 Trichloroethylene 1
TABLE B363
Organic Compounds Identified in Acid Extract of Sample No.H9A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.327 Methyl-2-Ethyl Hexanoate (IS)
2 0.463 Trichloropentane 23
3 0.553 Trichloropentane 12
4 0.611 Trichlorohexane 15
5 0.679 Trichloroheptane 9
6 1.000 Methyl Palmitate 2
-------
190
TABLE B364
Organic Compounds Identified in Base Extract of Sample No. H9B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.149 Dibutyl Phthalate 1
TABLE B365
Volatile Organic Compounds Identified in Sample No. 120S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
-------
191
TABLE B366
Organic Compounds Identified in Acid Extract of Sample NO.120A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
TABLE B367
Organic Compounds Identified in Base Extract of Sample No. 120B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B368
Volatile Organic Compounds Identified in Sample No. 121S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform i
-------
192
TABLE B369
Organic Compounds Identified in Acid Extract of Sample N0.121A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.162 C6 Alcohol 2
2 0.281 Cy Alcohol 2
3 0.370 Cg Alcohol 6
4 0.406 Methyl-2-Ethyl Hexanoate (IS)
5 0.449 Cg Alcohol 8
6 0.526 C1Q Alcohol 15
7 0.596 C^ Alcohol 10
8 0.666 C-J2 Alcohol 8
9 0.731 C-|2 Alcohol 8
10 0.795 C]4 Alcohol 9
11 0.859 C.| ^ A1 cohol 5
12 0.917 C16 Alcohol 4
13 0.972 C]7 Alcohol 2
14 1.000 Methyl Palmitate 1
15 1.028 C18 Alcohol 2
16 1.083 C]9 Alcohol 2
17 1.132 C2Q Alcohol 2
18 1.181 CZ1 Alcohol 2
19 1.226 C22 Alcohol 2
20 1.272 C23 Alcohol 2
21 1.315 C24 Alcohol 1
-------
193
TABLE B370
Organic Compounds Identified in Base Extract of Sample No. 121B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B371
Volatile Organic Compounds Identified in Sample No. 122S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chloroform
1
TABLE B372
Organic Compounds Identified in Acid Extract of Sample N0.122A
Relative Approximate
Peak Retention ^evei
No. Time Compound \PPO)
1 0.414 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate
-------
TABLE B373
Organic Compounds Identified in Base Extract of Sample No. 122B
Relati ve
Approximate
Peak
Retention
Level
No.
Time Compound
(ppb)
No peaks over 1 PPB.
TABLE B374
Volatile Organic Compounds Identified
in Sample No. 123S
Relative
Approximate
Peak
Retention
Level
No.
Time Compound
(PPb)
1
1.000 Chloroform
2
TABLE B375
Organic Compounds Identified in Acid Extract of Sample No.l23A
Relative
Approximate
Peak
Retention
Level
No.
Time Compound
(PPb)
1
0.449 Methyl-2-Ethyl Hexanoate
(IS)
2
1.000 Methyl Palmitate
2
3
1.102 Methyl Stearate
1
-------
195
TABLE B376
Organic Compounds Identified in Base Extract of Sample No. 123B
Relative
Peak Retention
No. Time Compound
No peaks over 1 PPB.
Approximate
Level
(ppb)
TABLE B377
Volatile Organic Compounds Identified in Sample No. 124S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
-------
196
TABLE B378
Organic Compounds Identified in Acid Extract of Sample N0.124A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.401 Methyl-2-Ethyl Hexanoate (IS)
2' 0.897 Methyl Myristate 1
3 1.000 Methyl Palmitate 3
4 . 1.018 C-jq Terpineol 2
5 1.067 ? 2
6 1.109 Methyl Stearate 4
TABLE B379
Organic Compounds Identified in Base Extract of Sample No. 124B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.565 Diethyl Hexyl Phthalate
-------
197
TABLE B380
Volatile Organic Compounds Identified in Sample No. 125S
Relative Approximate
Peak Retention Level
No. Time Compound {ppbj
1 1.000 Chloroform o
TABLE B381
Organic Compounds Identified in Acid Extract of Sample No.125A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.423 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.100 Methyl Stearate 2
-------
198
TABLE B382
Organic Compounds Identified in Base Extract of Sample No. 125B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.914 Atrazine 1
3 2.088 Dibutyl Phthalate 2
4 2.452 Butyl Phthaiy 1 Butyl Glycolate 1
TABLE B383
Volatile Organic Compounds Identified in Sample No. 126S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 2.298 Bromobenzene 5
-------
199
TABLE B384
Organic Compounds Identified in Acid Extract of Sample N0.126A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.433 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
TABLE B385
Organic Compounds Identified in Base Extract of Sample No. 126B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B386
Volatile Organic Compounds Identified in Sample No. 127S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chloroform
1
-------
200
TABLE B387
Organic Compounds Identified in Acid Extract of Sample No.l27A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.111 Methyl Stearate 5
TABLE B388
Organic Compounds Identified in Base Extract of Sample No. 127B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.942 Atrazine
-------
201
TABLE B389
Volatile Organic Compounds Identified in Sample No. 128S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 40
2 1.357 Bromo-Dichloroethane 10
3 1.633 Dibromo-Chloromethane 8
4 2.232 Dichlorobenzene 10
TABLE B390
Organic Compounds Identified in Acid Extract of Sample N0.128A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B391
Organic Compounds Identified in Base Extract of Sample No. 128B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
202
TABLE B392
Volatile Organic Compounds Identified in Sample No. 129S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
TABLE B393
Organic Compounds Identified in Acid Extract of Sample No. 129A
Relative
Peak Retention
No. Tine Compound
No peaks over 1 PPB.
Approximate
Level
(ppb)
TABLE B394
Organic Compounds Identified in Base Extract of Sample No. 129B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.058 Dibutyl Phthalate 2
-------
203
TABLE B395
Volatile Organic Compounds Identified in Sample No. 130S
Peak
Relative
Approximate
Retention
Level
No.
Time
Compound
(PPb)
1
1.000
Chloroform
18
2
2.159
Acetophenone
2
TABLE B396
Organic Compounds Identified in Acid Extract of Sample No. 130A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.431 Methyl - 2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.104 Methyl Stearate 1
4 1.208 C-| g Terpene 1
-------
204
TABLE B397
Organic Compounds Identified in Base Extract of Sample No. 130B
Relative Approximate
Peak Retention ( Level
No. Time _Compound (ppb)
No peaks over 1 PPB.
TABLE B398
Volatile Organic Compounds Identified in Sample No. 131S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.448 Dimethyl Disulfide 1
-------
205
TABLE B399
Organic Compounds Identified in Acid Extract of Sample No.131A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 4
3 1.092 Dibutyl Phthalate 1
4 1.101 Methyl Stearate 4
5 1.275 Diethyl Hexyl Phthalate 7
TABLE B400
Organic Compounds Identified in Base Extract of Sample No. 131B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.906 Atrazine 1
3 2.028 ? 1
4 2.074 Dibutyl Phthalate 1
5 2.682 Diethyl Hexyl Phthalate 1
-------
206
TABLE B401
Volatile Organic Compounds Identified in Sample No. 132S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 15
2 2.076 Toluene 3
TABLE B402
Organic Compounds Identified in Acid Extract of Sample N0.132A
Relative i Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.424 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 5
3 1.031 C]8 Alcohol 1
4 1.101 Methyl Stearate 5
5 1.132 C2Q Alcohol 1
6 1.350 Diethyl Hexyl Phthalate 1
-------
207
TABLE B403
Organic Compounds Identified in Base Extract of Sample No.l32B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.994 Atrazine
3 2.129 ?
4 2.185 Dibutyl Phthalate
5 2.682 Diethyl Hexyl Phthalate
6 2.817 C^5 Terpineol
TABLE B404
Volatile Organic Compounds Identified in Sample No. 133S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
2 1.273 Cyclohexane 1
3 1.506 Dimethyl Disulfide 1
-------
208
TABLE B405
Organic Compounds Identified in Acid Extract of Sample N0.133A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.431 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Pa Imitate 2
3 1.104 Methyl Stearate 3
TABLE B406
Organic Compounds Identified in Base Extract of Sample No. 133B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.104 Dibutyl Phthalate 1
3 2.575 Diethyl Hexyl Phthalate 1
4 2.708 C-|g Terpineol 1
-------
209
TABLE B407
Volatile Organic Compounds Identified in Sample No. 134S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B408
Organic Compounds Identified in Acid Extract of Sample No.l34A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.430 Methyl-2-Ethyl Hexanoate (IS)
2 0.908 ? 2
3 1.000 Methyl Palmitate 5
4 1.089 Dibutyl Phthalate 4
5 1.110 Methyl Stearate 4
6 1.126 C^ Terpene 3
7 1.218 C-|^ Terpene 2
8 1.288 Butyl Phthalyl Butyl Glycolate 3
-------
210
TABLE B409
Organic Compounds Identified in Base Extract of Sample No. 134B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.117 Dibutyl Phthalate 1
3 2.590 Diethyl Hexyl Phthalate 1
4 2.725 C-|cj Terpineol 1
TABLE B410
Volatile Organic Compounds Identified in Sample No. 135S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.071 1,2-Dichloroethane 2
3 1.547 Benzene 3
-------
211
TABLE B411
Organic Compounds Identified in Add Extract of Sample No. 135A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.391 Kethyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Paliritate 2
3 1.107 Methyl Stearate 1
4 1.359 Diethyl Hexyl Phthalate 1
TABLE B412
Organic Compounds Identified in Base Extract of Sample No. 135B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.576 C1Q Terpineol 1
3 2.506 Diethyl Hexyl Phthalate 1
-------
212
TABLE B413
Volatile Organic Compounds Identified in Sample No. 136S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.071 1 ,2-Dichloroethane 3
3 1.296 Dichlorobenzene 1
TABLE B414
Organic Compounds Identified in Acid Extract of Sample No. 136A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.373 Methyl-2-Ethyl Hexanoate (IS)
2 0.814 C^q Terpineol 1
3 1.000 Methyl Palmitate 6
4 1.100 Methyl Stearate 3
5 1.343 Diethyl Hexyl Phthalate 4
-------
213
TABLE B415
Organic Compounds Identified in Base Extract of Sample No.136B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (15)
2 1.516 C.|q Terpineol 1
TABLE B416
Volatile Organic Compounds Identified in Sample No. 137S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.490 Benzene 2
3 1.630 Hexane 2
-------
214
TABLE B417
Organic Compounds Identified in Acid Extract of Sample No. 137A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.379
Methyl-2-Ethyl Hexanoate (IS)
--
2
0.818
C-jq Terpineol
2
3
0.912
C10 Terpineol
2
4
1.000
Methyl Palmitate
5
5
1.100
Methyl Stearate
2
6
1.118
C-|5 Terpene
.1
7
1.205
C^ Terpene
1
8
1.341
Diethyl Hexyl Phthalate
1
TABLE B418
Organic Compounds Identified in Base Extract of Sample No. 137B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.500 Diethyl Hexyl Phthalate 1
-------
215
TABLE B419
Volatile Organic Compounds Identified in Sample No. 138S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.501 Benzene 1
3 1.636 Hexane 1
TABLE B420
Organic Compounds Identified in Acid Extract of Sample No. 138A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.380 Methyl-2-Ethyl Hexanoate (IS)
2 0.823 C^q Terpineol 1
3 0.891 Methyl Myristate 3
4 0.S47 Fatty Acid Methyl Ester C >_ 14 1
5 1.000 Methyl PaImitate 13
6 1.094 Methyl Stearate 6
7 1.332 Diethyl Hexyl Phthalate 2
-------
216
TABLE B421
Organic Compounds Identified in Base Extract of Sample No. 138B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.495 Diethyl Hexyl Phthalate 4
TABLE B422
Volatile Organic Compounds Identified in Sample No. 139S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.467 Acetone 1
2 0.817 Pentene 1
3 1.000 Chloroform 40
4 1.302 Bromo-Dichloromethane 7
5 1.479 Trichloroethylene 5
6 1.555 Dibromo-Chloromethane 7
-------
217
TABLE B423
Organic Compounds Identified in Acid Extract of Sample No. 139A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.380 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 1
4 1.341 Diethyl Hexyl Phthalate 1
5 1.407 C^ Terpineol 4
TABLE B424
Organic Compounds Identified in Base Extract of Sample No. 139B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
218
TABLE B425
Volatile Organic Compounds Identified in Sample No. 140S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.302 Chloroprene 1
3 1.490 Trichloroethylene 1
4 2.077 Toluene 2
TABLE B426
Organic Compounds Identified in Acid Extract of Sample No. 140A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.193 1,1 ,2,2-Tetrachloroethane 1
2 0.401 Methyl-2-Ethyl Hexanoate (IS)
3 1.000 Methyl Palmitate 3
4 1.101 Methyl Stearate 5
-------
219
TABLE B427
Organic Compounds Identified in Base Extract of Sample NO.140B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B428
Volatile Organic Compounds Identified in Sample No. 141S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.386
Dichloromethane
2
1.000
Chloroform
3
1.219
Carbon Tetrachloride
4
1.493
Trichloroethylene
5
2.084
To!uene
-------
220
TABLE B429
Organic Compounds Identified in Acid Extract of Sample No. 141A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
"1 0.390 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.099 Methyl Stearate 3
4 1.338 Diethyl Hexyl Phthalate 1
TABLE B430
Organic Compounds Identified in Base Extract of Sample No. 141B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.570 Diethyl Hexyl Phthalate 1
-------
221
TABLE B431
Volatile Organic Compounds Identified in Sample No. 142S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.357 Dichloromethane 1
2 0.423 Acetone 3
3 1.000 Chloroform 3
4 1.061 1,2-Dichloroethane 1
5 1.091 Methacrylonitrile 1
6 1.187 Carbon Tetrachloride 2
7 1.258 Bromo-Dichloromethane 1
8 1.400 Trichloroethylene 1
9 1.409 Benzene 1
10 1.476 Bromo-Trichloropropane 2
11 1.931 Toluene 1
TABLE B432
Organic Compounds Identified in Acid Extract of Sample No. 142A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.390 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.098 Methyl Stearate 1
4 1.337 Diethyl Hexyl Phthalate 3
-------
222
TABLE B433
Organic Compounds Identified in Base Extract of Sample No. 142B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.115 Diethyl Hexyl Phthalate
TABLE B434
Volatile Organic Compounds Identified in Sample No. 143S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1, PPB.
-------
223
TABLE B435
Organic Compounds Identified in Acid Extract of Sample No. 143A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.419 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.102 Methyl Stearate 1
TABLE B436
Organic Compounds Identified in Base Extract of Sample No. 143B
Relative Approximate
Peak Retention Level
No. T i me Compound (ppb)
1 1.000 Camphor (IS)
2 2.057 Dibutyl Phthalate 1
jTABLE B437
Volatile Organic Compounds Identified in Sample No. 144S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 2
-------
224
TABLE B438
Organic Compounds Identified in Acid Extract of Sample No. 144A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.339 Diethyl Hexyl Phthalate 1
TABLE B439
Organic Compounds Identified in Base Extract of Sample N0.144B
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
No peaks over 1 PPB.
TABLE B440
Volatile Organic Compounds Identified in Sample No. 145S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 43
2 1.236 Carbon Tetrachloride 3
3 1.330 Bromo-Dichloromethane 7
4 1.599 Dibromo-Chloromethane 5
-------
225
TABLE B441
Organic Compounds Identified in Acid Extract of Sample No. 145A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.326
1,1,2,2-Tetrachloroethane
1
2
0.492
Methyl-2-Ethyl Hexanoate (IS)
--
3
1.000
Methyl Palmitate
4
4
1.091
Methyl Stearate
4
5
1.238
Dioctyl Adipate
86
6
1.335
Diethyl Hexyl Phthalate Isomers
4
7
1.354
Diethyl Hexyl Phthalate Isomers
6
8
1.372
Diethyl Hexyl Phthalate Isomers
17
9
1.381
Diethyl Hexyl Phthalate Isomers
26
10
1.406
C-|5 Terpineol
1
TABLE B442
Organic Compounds Identified in Base Extract of Sample No. 145B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
226
TABLE B443
Volatile Organic Compounds Identified in Sample No. 146S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.279 Bromo-Dichloromethane 1
TABLE B444
Organic Compounds Identified in Acid Extract of Sample No. 146A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.271 1,1,2,2-Tetrachloroethane 1
2 0.412 Methyl-2-Ethyl Hexanoate (IS)
3 1.000 Methyl Palmitate 5
4 1.088 Dibutyl Phthalate 1
5 1.099 Methyl Stearate 2
-------
227
TABLE B445
Organic Compounds Identified in Base Extract of Sample No. 146B
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
No peaks over 1 PPB.
TABLE B446
Volatile Organic Compounds Identified in Sample No. 147S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.422 Acetone 1
2 1.000 Chloroform 38
3 1.319 Bromo-Dichloromethane 14
4 1.583 Dibromo-chloromethane 4
-------
228
TABLE B447
Organic Compounds Identified in Acid Extract of Sample No. 147A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 5
3 1.089 Dibutyl Phthalate 1
4 1.100 Methyl Stearate 3
5 1.236 Dioctyl Adipate 4
6 1.340 Diethyl Hexyl Phthalate 1
TABLE B448
Organic Compounds Identified in Base Extract of Sample No. 147B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.011 Dibutyl Phthalate 1
3 2.461 Diethyl Hexyl Phthalate 1
-------
229
TABLE B449
Volatile Organic Compounds Identified in Sample No. 148S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.359 Bromo-Dichloromethane
TABLE B450
Organic Compounds Identified in Acid Extract of Sample No. 148A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.341 1,1,2,2-Tetrachloroethane
2 0.430 Methyl-2-Ethyl Hexanoate (IS)
TABLE B451
Organic Compounds Identified in Base Extract of Sample No. 148B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.011 Dibutyl Phthalate 1
-------
230
TABLE B452
Volatile Organic Compounds Identified in Sample No.149S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 6
2 1.500 Benzene 2
TABLE B453
Organic Compounds Identified in Acid Extract of Sample No. 149A
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1 0.418 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.009 C-j 5 Terpene 1
4 1.100 Methyl Stearate 2
TABLE B454
Organic Compounds Identified in Base Extract of Sample No. 149B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
231
TABLE B455
Volatile Organic Compounds Identified in Sample No. 150S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.402 Dichloromethane 2
2 1.000 Chloroform 2
TABLE B456
Organic Compounds Identified in Acid Extract of Sample No. 150A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.108 Methyl Stearate 1
TABLE B457
Organic Compounds Identified in Base Extract of Sample No. 150B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
232
TABLE B458
Volatile Organic Compounds Identified in Sample No. 151S
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
No peaks over 1 PPB.
TABLE B459
Organic Compounds Identified in Acid Extract of Sample No. 151A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 0.850 ? 102
3 0.955 ? 64
4 1.000 Methyl Palmitate 11
5 1.102 Methyl Stearate 4
TABLE B460
Organic Compounds Identified in Base Extract of Sample No. 151B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.449 Diethyl Hexyl Phthalate 1
-------
233
TABLE B461
Volatile Organic Compounds Identified in Sample No. 152S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B462
Organic Compounds Identified in Acid Extract of Sample No. 152A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.419 Methyl -2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 6
3 1.098 Methyl Stearate 3
4 1.329 Diethyl Hexyl Phthalate 2
TABLE B463
Organic Compounds Identified in Base Extract of Sample No. 152B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.009 Dibutyl Phthalate
-------
234
TABLE B464
Volatile Organic Compounds Identified in Sample No. 153S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 24
2 1.335 Bromo-Dichloromethane 4
3 1.588 Dibromo-Chloromethane 4
TABLE B465
Organic Compounds Identified in Acid Extract of Sample No. 153A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.362 Cg Alcohol 2
2 0.435 Methyl-2-Ethyl Hexanoate (IS)
3 0.471 Cg Alcohol 7
4 0.543 C1Q Alcohol 8
5 0.610 Cii A1cohol 9
6 0.676 C-|2 Alcohol 7
7 0.740 C13 Alcohol 6
8 0.800 C]4 Alcohol 8
9 0.861 C15 Alcohol 5
10 0.921 C16 Alcohol 4
11 0.976 C]7 Alcohol 1
-------
235
TABLE B466
Organic Compounds Identified in Base Extract of Sample N0.153B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B467
Volatile Organic Compounds Identified in Sample No. 154S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B468
Organic Compounds Identified in Acid Extract of Sample No. 154A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
236
TABLE B469
Organic Compounds Identified in Base Extract of Sample No. 154B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2. 2.043 Diethyl Hexyl Phthalate 2
TABLE B470
Volatile Organic Compounds Identified in Sample No. 155S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B471
Organic Compounds Identified in Acid Extract of Sample No. 155A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.412 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.105 Methyl Stearate 2
4 1.187 Unidentified Phthalate 3
5 1.146 Diethyl Hexyl Phthalate 4
-------
237
TABLE B472
Organic Compounds Identified in Base Extract of Sample No.155B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B473
Volatile Organic Compounds Identified in Sample No. 156S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 29
2 1.330 Bromo-Dichloromethane 2
3 1.588 Dibromo-Chloromethane 2
TABLE B474
Organic Compounds Identified in Acid Extract of Sample No.l56A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.107 Methyl Stearate 2
-------
238
TABLE B475
Organic Compounds Identified in Base Extract of Sample No. 156B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.023 Dibutyl Phthalate 2
3 2.470 Diethyl Hexyl Phthalate 1
TABLE B476
Volatile Organic Compounds Identified in Sample No. 157S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.500 Trichloroethylene
-------
239
TABLE B477
Organic Compounds Identified in Acid Extract of Sample No. 157A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.434 Methyl-2-Ethyl Hexanoate (IS)
2 0.910 C-|5 Terpene 1
3 1.000 Methyl Palmitate 3
4 1.102 Methyl Stearate 3
TABLE B478
Organic Compounds Identified in Base Extract of Sample No.157B
Peak
No.
Relative
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
2
2.023
Dibutyl Phthalate
5
3
2.415
Hydrocarbon C >_ 24
1
4
2.470
Diethyl Hexyl Phthalate
2
5
2.559
Hydrocarbon C > 26
1
6
2.597
C-jg Terpineol
2
7
2.631
Hydrocarbon C >_ 28
1
8
2.696
Hydrocarbon C >_ 28
1
9
2.774
Hydrocarbon C > 30
1
10
2.857
Hydrocarbon C 30
1
-------
240
TABLE B479
Volatile Organic Compounds Identified in Sample N0.158S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.000 Chloroform 5
TABLE B480
Organic Compounds Identified in Acid Extract of Sample No. 158A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 0.896 Methyl Myristate 6
3 1.000 Methyl Palmitate 16
4 1.107 Methyl Stearate 2
TABLE B481
Organic Compounds Identified in Base Extract of Sample No.l58B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
241
TABLE B482
Volatile Organic Compounds Identified in Sample No. 159S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B483
Organic Compounds Identified in Acid Extract of Sample No. 159A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 6
3 1.103 Methyl Stearate 4
TABLE B484
Organic Compounds Identified in Base Extract of Sample No. 159B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
242
TABLE B485
Volatile Organic Compounds Identified in Sample No. 160S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.000 Chloroform
TABLE B486
Organic Compounds Identified in Acid Extract of Sample No. 160A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B487
Organic Compounds Identified in Base Extract of Sample No. 160B
Relative . Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
243
TABLE B488
Volatile Organic Compounds Identified in Sample No.161S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B489
Organic Compounds Identified in Acid Extract of Sample No. 161A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B490
Organic Compounds Identified in Base Extract of Sample No. 161B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
244
TABLE B491
Volatile Organic Compounds Identified in Sample No. 162S
Relati ve
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chioroform
2
TABLE B492
Organic Compounds Identified in Acid Extract of Sample No. 162A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B493
Organic Compounds Identified in Base Extract of Sample N0.162B
Relative
Peak Retention
No. Time Compound
Approximate
Level
(ppb)
No peaks over 1 PPB.
-------
245
TABLE B494
Volatile Organic Compounds Identified in Sample No. 163S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B495
Organic Compounds Identified in Acid Extract of Sample No. 163A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.321 1,1,2,2-Tetrachloroethane 1
2 0.420 Methyl-2-Ethyl Hexanoate (IS)
3 1.000 Methyl Palmitate 2
TABLE B496
Organic Compounds Identified in Base Extract of Sample No.l63B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.496 Diethyl Hexyl Phthalate 1
-------
246
TABLE B497
Volatile Organic Compounds Identified in Sample No.164S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B498
Organic Compounds Identified in Acid Extract of Sample No.l64A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B499
Organic Compounds Identified in Base Extract of Sample No. 164B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.983 Diisobutyl Phthalate 4
3 2.092 Dibutyl Phthalate 7
-------
247
TABLE B500
Volatile Organic Compounds Identified in Sample No. 165S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.846 Tetrahydrofuran 3
2 1.000 Chloroform 4
3 1.618 Hexanol 2
TABLE B501
Organic Compounds Identified in Acid Extract of Sample No. 165A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B502
Organic Compounds Identified in Base Extract of Sample No. 165B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
248
TABLE B503
Volatile Organic Compounds Identified in Sample No. 166S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B504
Organic Compounds Identified in Acid Extract of Sample No. 16(5A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B505
Organic Compounds Identified in Base Extract of Sample No. 166B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
249
TABLE B506
Volatile Organic Compounds Identified in Sample No.l67S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.390 Dichloromethane 5
2 1.465 Benzene 1
TABLE B507
Organic Compounds Identified in Acid Extract of Sample No. 167A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.387 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.288 Butyl Phthalyl Butyl Glycolate 2
TABLE B508
Organic Compounds Identified in Base Extract of Sample No. 167B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
250
TABLE B509
Volatile Organic Compounds Identified in Sample No. 168S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.879 Tetrahydrofuran 318
2 0.949 1 ,2-Dichloroethane 4
3 1.000 Chloroform 9
4 1.440 Trichloroethylene 188
5 1.546 Methyl-t-Butyl Ketone 1
6 1.919 Tetrachloroethylene 45
7 2.025 Dichlorobenzene 2
TABLE B510
Organic Compounds Identified in Acid Extract of Sample N0.I68A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.349
1 ,1 ,2,2-Tetrachloroethane
1
2
0.434
Methyl -2-Ethyl Hexanoate (IS)
3
0.568
Pentachlorobutene
1
4
0.678
CxHyClz, x ^ 4, z^5
6
5
0.705
CxHyC1z' X - 4' 1 - 5
7
6
0.781
Pentachloroethane
1
7
0.933
Hexachlorobenzene
3
8
0.969
?
2
9
1.000
Methyl Palmitate
3
10
1.103
Methyl Stearate
2
11
1 .140
?
1
12
1.255
?
3
13
1.346
Diethyl Hexyl Phthalate
1
-------
251
TABLE B511
Organic Compounds Identified in Base Extract of Sample No. 168B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.580
Tetrachloroethane
44
2
0.762
Hexachloroethane
3
3
0.784
Tetrachlorobutadiene
5
4
0.817
Tetrachlorobutadiene
7
5
0.878
Pentachlorobutadiene
6
6
0.917
Tetrachlorobutadiene
11
7
0.934
Pentachlorobutadiene
5
8
0.955
Pentachlorobutadiene
38
9
0.972
Hexachlorobutadiene
22
10
1.000
Camphor (IS)
11
1.016
Pentachlorobutene
64
12
1.083
Pentachlorobutene
27
13
1.127
Hexachlorobutene
21
14
1.182
Hexachlorobutene
17
15
1.221
CxHyC1z' x - 4' z - 5
99
16
1.271
CxHyClz, x > 4, z > 5
100
17
1.359
CxHyCl z, x > 4, z >_ 5
14
18
1.387
CHC1 , x > 4, z > 5
x y z - -
3
19
1.409
CHC1 , x > 4, z > 5
x y z - -
13
20
1.448
Pentachloroethane
1
21
1.503
Pentachloroethane
2
22
1.691
Hexachlorobenzene
4
23
2.420
Diethyl Hexyl Phthalate
2
-------
252
TABLE B512
Volatile Organic Compounds Identified in Sample No. 169S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.877 Tetrahydrofuran 2
TABLE B513
Organic Compounds Identified in Acid Extract of Sample No. 169A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.352 1 ,1,2,2-Tetrachloroethane 1
2 0.431 Methyl-2-Ethyl Hexanoate (IS)
3 1.000 Methyl Palmitate 5
4 1.021 ? 1
5 1.104 ? 2
6 1.239 ? 4
7 1.376 ? 1
-------
253
TABLE B514
Organic Compounds Identified in Base Extract of Sample N0.169B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 1.147 2-Methyl Thiobenzothiazole 3
3 1.413 Diethyl Hexyl Phthalate 1
TABLE B515
Volatile Organic Compounds Identified in Sample No. 170S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B516
Organic Compounds Identified in Acid Extract of Sample No. 170A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 3
3 1.065 ? 1
4 1.108 Methyl Stearate 3
5 1.244 ? 3
-------
254
TABLE B517
Organic Compounds Identified in Base Extract of Sample No. 170B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.081 Dibutyl Phthalate 1
3 2.561 Diethyl Hexyl Phthalate 1
TABLE B518
Volatile Organic Compounds Identified in Sample No. 171S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
255
TABLE B519
Organic Compounds Identified in Acid Extract of Sample No. 171A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.306 C? Alcohol 1
2 0.324 Dichlorobutene 1
3 0.420 Cg Alcohol 1
4 0.420 Methyl-2-Ethyl Hexanoate (IS)
5 0.468 Cg Alcohol 2
6 0.543 C1Q Alcohol 2
7 0.612 C^ Alcohol 2
8 0.678 C-J2 Alcohol 3
9 0.742 C13 Alcohol 3
10 0.805 C]4 Alcohol 3
11 0.865 C^ g Alcohol 3
12 0.892 Methyl Myristate 1
13 0.922 C16 Alcohol 3
14 0.979 C1? Alcohol 4
15 1.000 Methyl Palmitate 12
16 1.033 C^g Alcohol 6
17 1.084 C]9 Alcohol 4
18 1.102 Methyl Stearate 16
19 1.129 C2Q Alcohol 7
20 1.180 C21 Alcohol 5
21 1.222 C22 Alcohol 6
22 1.267 C23 Alcohol 4
23 1.309 C24 Alcohol 3
24 1.348 Diethyl Hexyl Phthalate +
C2g Alcohol 3
25 1.387 C26 Alcohol 2
26 1.414 C Terpineol 1
-------
256
TABLE 3520
Organic Compounds Identified in Base Extract of Sample No.171B
Peak
No.
Relati ve
Retenti on
Time
Compound
Approximate
Level
(ppb)
1
1.000
Camphor (IS)
_
2
2.019
Dibutyl Phthalate
1
3
2.500
Diethyl Hexyl Phthalate
1
TABLE B521
Volatile Organic Compounds Identified in Sample No.
172S
Peak
No.
Relati ve
Retention
Time
Compound
Approximate
Level
(ppb)
No peaks over 1 PPB.
TABLE B522
Organic Compounds Identified in Acid Extract of Sample No. 172A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0. 342
1,1,2,2-Tetrachloroethane
1
2
0.421
Methyl-2-Ethyl Hexanoate (IS)
3
1.000
Methyl Palmitate
6
4
1.107
Methyl Stearate
8
5
1.355
Diethyl Hexyl Phthalate
6
-------
257
TABLE B523
Organic Compounds Identified in Base Extract of Sample No. 172B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B524
Volatile Organic Compounds Identified in Sample No. 173S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 4
TABLE B525
Organic Compounds Identified in Acid Extract of Sample No. 173A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.411 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.107 Methyl Stearate 1
-------
258
TABLE B526
Organic Compounds Identified in Base Extract of Sample No. 1 73B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.001 Dibutyl Phthalate 2
TABLE B527
Volatile Organic Compounds Identified in Sample No. 174S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chloroform
1
TABLE B528
Organic Compounds Identified in Acid Extract of Sample No. 174A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
259
TABLE B529
Organic Compounds Identified in Base Extract of Sample No. 174B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B530
Volatile Organic Compounds Identified in Sample No.l75S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B531
Organic Compounds Identified in Acid Extract of Sample No. 175A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.427 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.104 Methyl Stearate 1
-------
260
TABLE B532
Organic Compounds Identified in Base Extract of Sample No.1755
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B533
Volatile Organic Compounds Identified in Sample No. 176S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.397 Dimethyl Sulfide 1
2 0.673 Dimethoxymethane 3
3 1.000 Chloroform 1
4 1.459 Dimethyl Disulfide 1
TABLE B534
Organic Compounds Identified in Acid Extract of Sample N0.176A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Methyl Palmitate 6
2 1.104 Methyl Stearate 3
3 1.120 ^15" Terpene 1
-------
261
TABLE B535
Organic Compounds Identified in Base Extract of Sample N0.176B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.082 Dibutyl Phthalate 1
3 2.563 Diethyl Hexyl Phthalate 1
TABLE B536
Volatile Organic Compounds Identified in Sample No. 177S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
262
TABLE B537
Organic Compounds Identified in Acid Extract of Sample No. 177A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.426 Methyl-2-Ethyl Hexanoate (IS)
2 0.475 Cg Alcohol 1
3 0.543 C]0 Alcohol 1
4 0.607 Cn Alcohol 1
5 0.678 C12 Alcohol 4
6 0.739 C13 Alcohol 3
7 0.801 C-|4 Alcohol 3
8 0.862 C]5 Alcohol 2
9 0.920 C16 Alcohol 2
10 0.975 C17 Alcohol 1
11 1.031 C]8 Alcohol 1
TABLE B538
Organic Compounds Identified in Base Extract of Sample No. 177B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor
2 2.589 Diethyl Hexyl Phthalate 1
-------
263
TABLE B539
Volatile Organic Compounds Identified in Sample No. 178S
Relative Approximate
Peak Retention Level
No. Time Compound {ppb)
1.000 Chloroform
TABLE B540
Organic Compounds Identified in Acid Extract of Sample N0.178A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.522 C]0 Alcohol 2
2 0.595 C.|.| Alcohol 3
3 0.667 C]2 Alcohol 2
4 0.731 C]3 Alcohol 3
5 0.796 C^ Alcohol 3
6 0.858 C^5 Alcohol 2
-------
264
TABLE B541
Organic Compounds Identified in Base Extract of Sample N0.178B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.578 Diethyl Hexyl Phthalate 1
TABLE B542
Volatile Organic Compounds Identified in Sample Mo. 179S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
.000 Chloroform 8
TABLE B543
Organic Compounds Identified in Acid Extract of Sample No. 179A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.408 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 2
3 1.105 Methyl Stearate 1
-------
265
TABLE B544
Organic Compounds Identified in Base Extract of Sample No.l79B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.606 Dichlorobutane 5
2 1.000 Camphor (IS)
TABLE B545
Volatile Organic Compounds Identified in Sample No.180S
Peak
No.
Relati ve
Retention
Time
Compound
Approximate
Level
(ppb)
1
1.000
Chloroform
2
2
1.065
1,2-Dichloroethane
1
-------
266
TABLE B546
Organic Compounds Identified in Acid Extract of Sample No.l80A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.426 Methyl-2-Ethyl Hexanoate (IS)
2 0.742 C]3 Alcohol 1
3 0.804 C14 Alcohol 2
4 0.862 C,c Alcohol 2
1 D
5 0.920 C,c Alcohol 2
16
6 0.978 C]7 Alcohol 2
7 1.000 Methyl Palmitate 4
8 1.031 C]8 Alcohol 1
9 1.086 C]g Alcohol 1
10 1.108 Methyl Stearate 3
11 1.135 C2Q Alcohol 1
12 1.181 r Alcohol 1
2 i
13 1.227 C22 Alcohol 1
14 1.273 C23 Alcohol 1
15 1.353 Diethyl Hexyl Phthalate 2
TABLE B547
Organic Compounds Identified in Base Extract of Sample No.lSOB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.645 Dichlorobutane 3
2 1.000 Camphor (IS)
3 2.532 Diethyl Hexyl Phthalate 1
-------
267
TABLE B548
Volatile Organic Compounds Identified in Sample No. 181S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 1.177 1,1,1-Trichloroethane 1
TABLE B549
Organic Compounds Identified in Acid Extract of Sample No. 181A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.481 Methyl-2-Ethyl Hexanoate (IS)
2 0.904 C^ Terpene 1
3 1.000 Methyl Palmitate 3
4 1.120 C-J5 Terpene 2
5 1.278 Methyl Dehydroabietate 1
6 1.352 ? 1
7 1.447 ? 1
TABLE B550
Organic Compounds Identified in Base Extract of Sample No.181B
Relative
Peak Retention
No. Time Compound
1 1.000 Camphor (IS)
2 2.606 Diethyl Hexyl Phthalate
Approximate
Level
(PPb)
-------
268
TABLE B551
Volatile Organic Compounds Identified in Sample No.l82S
n i n^eJatl'-ve Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
2 1.783 Bromobenzene 3
TABLE B552
Organic Compounds Identified in Acid Extract of Sample No. 182A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.426 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 5
3 1.089 ? 4
4 1.095 Dibutyl Phthalate 3
5 1.102 Methyl Stearate 6
6 1.230 ? 11
7 1.346 Diethyl Hexyl Phthalate 2
-------
269
TABLE B553
Organic Compounds Identified in Base Extract of Sample No.l82B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.627 Dichlorobutane 2
2 1.000 Camphor (IS)
3 2.558 Diethyl Hexyl Phthai ate 1
TABLE B554
Volatile Organic Compounds Identified in Sample N0.183S
p.-i, nRoeJaVVe Approximate
Peak Retention Level
Nฐ- Time Compound (ppb)
1 1.000 Chloroform 1
2 1.425 1,2-Bromo-Chloroethane 2
3 1.725 Dibromoethane 4
4 1.949 Methyl Ethyl Dioxolane 1
5 2.114 Tetrachloroethylene 1
6 2.421 Acetophenone 1
TABLE B555
Organic Compounds Identified in Acid Extract of Sample N0.183A
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.379
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
3
3
1.107
Methyl Stearate
2
4
1.352
Diethyl Hexyl Phthalate
1
-------
270
TABLE B556
Organic Compounds Identified in Base Extract of Sample No.l83B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.473 Oichlorobutane 4
2 1.000 Camphor (IS)
3 2.105 Dibutyl Phthalate 1
4 2.585 Diethyl Hexyl Phthalate 2
TABLE B557
Volatile Organic Compounds Identified in Sample No. 184S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.879 Tetrahydrofuran 1
2 1.000 Chloroform 12
3 2.146 Toluene 1
TABLE B558
Organic Compounds Identified in Acid Extract of Sample N0.184A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.305 1 ,1 ,2,2-Tetrachloroethane 2
2 0.415 Methyl-2-Ethyl Hexanoate (IS)
3 1.000 Methyl Palmitate 2
4 1.108 Methyl Stearate 2
5 1.235 ? 1
-------
271
TABLE B559
Organic Compounds Identified in Base Extract of Sample No. 184B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.689 Diethyl Hexyl Phthalate 1
TABLE B560
Volatile Organic Compounds Identified in Sample No. 185S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.948 Diethyl Ether 4
2 1.000 Chloroform 11
TABLE B561
Organic Compounds Identified in Acid Extract of Sample N0.185A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.420 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.065 ? 13
4 1.116 Methyl Stearate 1
5 1.174 ? 2
6 1.371 Diethyl Hexyl Phthalate 1
-------
272
TABLE B562
Organic Compounds Identified in Base Extract of Sample No. 185B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.542 Dichlorobutane 3
2 1.000 Camphor (IS)
3 2.607 Diethyl Hexyl Phthalate 1
TABLE B563
Volatile Organic Compounds Identified in Sample No. 186S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B564
Organic Compounds Identified in Acid Extract of Sample N0.I86A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.103 Dibutyl Phthalate 1
4 1.110 Methyl Stearate 1
5 1.349 Diethyl Hexyl Phthalate 1
-------
273
TABLE B565
Organic Compounds Identified in Base Extract of Sample No.186B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.557 Dichlorobutane 9
2 1.000 Camphor (IS)
TABLE B566
Volatile Organic Compounds Identified in Sample No. 187S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 3
2 2.239 Toluene ]
TABLE B567
Organic Compounds Identified in Acid Extract of Sample N0.187A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
274
TABLE B568
Organic Compounds Identified in Base Extract of Sample No.l87B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B569
Volatile Organic Compounds Identified in Sample No. 188S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
1.000
Chioroform
2
2
1.157
1,1 ,1-Trichloroethane
4
3
1.414
Dimethyl Disulfide
1
4
1.452
Trichloroethylene
3
5
1.959
Tetrachloroethylene
13
6
2.029
Toluene
2
-------
275
TABLE B570
Organic Compounds Identified in Acid Extract of Sample N0.188A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.411
Methyl-2-Ethyl Hexanoate (IS)
--
2
0.487
?
1
3
0.521
Hydrocarbon C > 8
1
4
0.554
Hydrocarbon C > 8
1
5
0.591
Hydrocarbon C > 10
1
6
0.621
Hydrocarbon C > 10
1
7
0.654
Hydrocarbon C > 10
1
8
0.688
Hydrocarbon C > 10
4
9
0.751
Hydrocarbon C > 12
6
10
0.775
Hydrocarbon C > 12
4
11
0.806
Hydrocarbon C > 12
8
12
0.815
Tetrachloroanisole
10
13
0.873
Hydrocarbon C >_ 14
17
14
0.887
Methyl Myristate
10
15
0.918
Methyl Naphthoate
3
16
0.933
Hydrocarbon C > 16
12
17
0.945
Pentachloroanisole
14
18
0.988
Hydrocarbon C > 16
1
19
1.000
Methyl Palmitate
30
20
1.021
?
5
21
1.042
Hydrocarbon C > 18
17
22
1.058
?
20
23
1.073
?
5
24
1.109
Methyl Stearate
87
25
1.142
?
23
26
1.160
?
17
27
1.182
Methoxy Carbonyl Benzophenone
27
28
1.203
35
29
1.212
C16H10
2
30
1.224
1
37
31
1.239
?
35
-------
276
TABLE B570, cont.
Organic Compounds Identified in Acid Extract of Sample N0.I88A (continued)
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
32
1.269
?
15
33
1.279
7
82
34
1.318
7
18
35
1.330
Fatty Acid Methyl Ester C
1 20
3
36
1.351
Diethyl Hexyl Phthalate
31
37
1.360
?
80
38
1.369
Fatty Acid Methyl Ester C
! 24
39
39
1.388
7
20
40
1.400
Hydrocarbon C >_ 28
10
41
1.409
7
35
42
1.418
7
40
43
1.427
?
31
44
1.446
7
45
45
1.457
7
27
46
1.482
7
42
47
1.497
7
9
48
1.536
7
33
49
1.558
7
10
50
1.567
7
27
51
1.582
7
12
-------
277
TABLE B571
Organic Compounds Identified in Base Extract of Sample N0.188B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Campho r (IS)
--
2
1.049
?
3
3
1.146
?
2
4
1.214
Hydrocarbon C >_ 12
1
5
1.287
Methyl Naphthalene
1
6
1.317
Methyl Naphthalene
1
7
1.348
Hydrocarbon C > 12
3
8
1.378
Indole
11
9
1.438
Dimethyl Naphthalene
3
10
1.470
Dimethyl Naphthalene
3
11
1.531
?
3
12
1.592
Biphenyl
2
13
1.732
Methyl Acenaphthene
2
14
1.787
Diethyl Phthalate
2
15
1.806
1
16
2.007
Phenanthrene
1
17
2.032
Diisobutyl Phthalate
2
18
2.147
?
4
19
2.184
Dibutyl Phthalate
8
20
2.221
Caffei ne
6
21
2.276
Hydrocarbon C > 20
5
22
2.312
Hydrocarbon C > 20
1
23
2.349
C16H10
1
24
2.373
Hydrocarbon C > 22
1
25
2.416
C16H10
1
26
2.440
Hydrocarbon C 22
1
27
2.465
Hydrocarbon C >_ 22
1
28
2.489
Hydrocarbon C > 22
1
29
2.550
Hydrocarbon C >_ 24
2
30
2. 574
Hydrocarbon C > 24
1
-------
278
TABLE B571, cont.
Organic Compounds Identified in Base Extract of Sample N0.I88B (continued)
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
31 2.636 Hydrocarbon C > 24 2
32 2.691 Diethyl Hexyl Phthalate 4
33 2.709 Hydrocarbon C 26 1
34 2.752 Hydrocarbon C 26 1
35 2.825 C-^ Terpineol 4
36 2.910 ? 3
37 2.989 ? 3
38 3.069 ? 10
39 3.173 ? 13
TABLE B572
Volatile Organic Compounds Identified in Sample No. 189S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Chloroform 1
-------
279
TABLE B573
Organic Compounds Identified in Acid Extract of Sample No.lB9A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.400 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.342 Diethyl Hexyl Phthalate 1
TABLE B574
Organic Compounds Identified in Base Extract of Sample No.l89B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.692 Diethyl Hexyl Phthalate
-------
280
TABLE B575
Volatile Organic Compounds Identified in Sample No. 190S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.412
Acetone
3
2
0.956
Diethyl Ether
1
3
1.000
Chloroform
3
4
1.544
7
2
5
1.619
Benzene
4
6
1.882
Bromobenzene
8
7
2.194
Tetrachloroethylene
1
8
2.282
Toluene
1
TABLE B576
Organic Compounds Identified in Acid Extract of Sample No.l90A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
0.356
Methyl-2-Ethyl Hexanoate (IS)
2
0.684
?
1
3
0.753
?
1
4
0.798
Methyl-2-(4-chlorophenoxy) Butanoate
2
5
0.809
Tetrachloroanisole
1
6
0.944
Pentachloroanisole
1
7
1.000
Methyl Palmitate
2
8
1.062
?
5
9
1.098
Dibutyl Phthalate
2
10
1.104
Methyl Stearate
5
11
1.113
Caffeine
3
12
1.234
7
15
13
1.278
?
. 5
14
1.375
?
8
-------
281
TABLE B577
Organic Compounds Identified in Base Extract of Sample No.l90B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
1.000
Camphor (IS)
--
2
1.856
?
1
3
2.284
Dibutyl Phthalate
2
4
2.317
Caffeine
4
5
2.389
Hydrocarbon C >_ 20
1
6
2.422
?
1
7
2.759
?
6
8
2.837
Diethyl Hexyl Phthalate
3
9
3.133
1
1
TABLE B578
Volatile Organic Compounds Identified in Sample No. 191S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.490 Acetone 2
2 1.110 Methyl Ethyl Ketone 23
3 2.274 Benzaldehyde 1
-------
282
TABLE B579
Organic Compounds Identified in Acid Extract of Sample No. 191A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(PPb)
1
0.400
Methyl-2-Ethyl Hexanoate (IS)
...
2
0.804
Methyl-2-(4-chlorophenoxy) Butanoate
12
3
0.817
Tetrachloroanisole
14
4
0.872
Hydrocarbon C > 14
21
5
0.887
Methyl Myristate
30
6
0.933
Hydrocarbon C >_ 16
33
7
0.948
Pentachloroanisole
24
8
0.982
Fatty Acid Methyl Ester C > 15
5
9
1.000
Methyl Palmitate
252
10
1.033
25
11
1.040
Fatty Acid Methyl Ester C > 16
45
12
1.055
Fatty Acid Methyl Ester C > 17
49
13
1.064
7
13
14
1.107
Methyl Stearate
425
15
1.143
Fatty Acid Methyl Ester C > 18
34
16
1.159
Fatty Acid Methyl Ester C > 18
48
17
1.180
7
32
18
1.204
Fatty Acid Methyl Ester C > 20
70
19
1.216
?
8
20
1.235
7
95
21
1.284
7
40
22
1.293
Fatty Acid Methyl Ester C >_ 22
66
23
1.353
Diethyl Hexyl Phthalate
34
24
1.378
?
57
25
1.506
?
53
26
1.595
?
79
-------
283
TABLE B580
Organic Compounds Identified in Base Extract of Sample No.191B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.549
Dichlorobutane
3
2
1.000
Camphor (IS)
--
3
1.181
Hydrocarbon C > 10
1
4
1.310
Hydrocarbon C > 12
1
5
1 .421
Hydrocarbon C > 12
1
6
1.473
Hydrocarbon C > 12
1
7
1.532
Hydrocarbon C > 14
3
8
1.549
Hydrocarbon C > 14
3
9
1.661
Hydrocarbon C > 14
18
10
1.729
?
13
11
1.755
Hydrocarbon C > 16
12
12
1.748
Hydrocarbon C > 16
15
13
1.819
Hydrocarbon C > 16
20
14
Co
Hydrocarbon C > 16
59
15
2.029
Hydrocarbon C > 18
59
16
2.088
Dibutyl Phthalate
60
17
2.182
Hydrocarbon C 20
38
18
2.217
Hydrocarbon C 20
48
19
2.270
?
123
20
2.339
Hydrocarbon C 22
41
21
2.469
Hydrocarbon C 24
18
22
2.515
Hydrocarbon C 24
20
23
2.586
Diethyl Hexyl Phthalate
58
24
2.703
C-|g Terpineol
35
-------
284
TABLE B581
Volatile Organic Compounds Identified in Sample No.l92S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B582
Organic Compounds Identified in Acid Extract of Sample No. 192A
Peak
No.
Relative
Retention
Time
Compound
Approximate
Level
(ppb)
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
16
17
18
19
20
0.400
0.602
0.672
0.738
0.801
0.861
0.921
0.979
1.000
1.030
1.084
1.099
1.105
1.129
1.181
1.226
1.271
1.287
1.310
1.352
Methyl-2-Ethyl Hexanoate (IS)
C-ji Alcohol
C-|2 Alcohol
C-J2 Alcohol
C-J4 Alcohol
C-jg Alcohol
C-jg Alcohol
C-jy Alcohol
Methyl Palmitate
C-|g Alcohol
C-jg Alcohol
Dibutyl Phthalate
Methyl Stearate
CgQ Alcohol
C2-| Alcohol
Cgg Alcohol
C^^ Alcohol
Butyl Phthalyl Butyl Glycolate
C24 Alcohol
Diethyl Hexyl Phthalate
5
7
9
12
15
13
5
5
4
2
?.
3
2
2
1
1
1
1
2
-------
285
TABLE B583
Organic Compounds Identified in Base Extract of Sample No. 192B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.645 Dichlorobutane 1
2 1.000 Camphor (IS)
3 2.076 Dibutyl Phthalate 2
4 2.437 Butyl Phthalyl Butyl Glycolate 1
5 2.553 Diethyl Hexyl Phthalate 3
TABLE B584
Volatile Organic Compounds Identified in Sample No.193S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
286
TABLE B585
Organic Compounds Identified in Acid Extract of Sample No.193A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.430 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.096 Dibutyl Phthalate 1
4 1.102 Methyl Stearate 1
5 1.346 Diethyl Hexyl Phthalate 1
TABLE B586
Organic Compounds Identified in Base Extract of Sample N0.193B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.570 Dichlorobutane 4
2 1.000 Camphor (IS)
3 2.106 Di butyl Phthalate 1
4 2.595 Diethyl Hexyl Phthalate 1
TABLE B587
Volatile Organic Compounds Identified in Sample N0.194S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
287
TABLE B588
Organic Compounds Identified in Acid Extract of Sample N0.194A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.370 1,1,2,2-Tetrachloroethane 1
2 0.442 Methyl -2-Ethyl Hexanoate (IS)
3 0.504 C9 Alcohol 3
4 0.561 C1Q Alcohol 2
5 0.623 Cn Alcohol 2
6 0.685 C-|2 Alcohol 3
7 0.847 C]3 Alcohol 3
8 0.807 C14 Alcohol 2
9 0.866 Clc Alcohol 1
I b
10 0.923 C16 Alcohol 1
11 0.979 C1? Alcohol 1
12 1.000 Methyl Palmitate 2
13 1.032 C]8 Alcohol 1
14 1.083 C]9 Alcohol 1
15 1.100 Dibutyl Phthalate 1
16 1.105 Methyl Stearate 1
17 1.130 C^q A1cohol 1
18 1.175 C2] Alcohol 1
19 1.219 C22 Alcohol 1
20 1.343 Diethyl Hexyl Phthalate 1
-------
288
TABLE B589
Organic Compounds Identified in Base Extract of Sample No.194B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 1.000 Camphor (IS)
2 2.789 Diethyl Hexyl Phthalate 2
TABLE B590
Volatile Organic Compounds Identified in Sample N0.195S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
289
TABLE B591
Organic Compounds Identified in Acid Extract of Sample No.l95A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1
0.410
Methyl-2-Ethyl Hexanoate (IS)
--
2
1.000
Methyl Palmitate
4
3
1.064
2
4
1.097
Dibutyl Phthalate
1
5
1.107
Methyl Stearate
2
6
1.238
?
2
7
1.351
Diethyl Hexyl Phthalate
1
TABLE B592
Organic Compounds Identified in Base Extract of Sample No.l95B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.642 Dichlorobutane 3
2 1.000 Camphor (IS)
3 2.499 Diethyl Hexyl Phthalate 4
-------
290
TABLE B593
Volatile Organic Compounds Identified in Sample No.l96S
Relative
Peak Retention
No. Time Compound
No peaks over 1 PPB.
Approximate
Level
(ppb)
TABLE B594
Organic Compounds Identified in Acid Extract of Sample N0.196A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.410 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.105 Methyl Stearate 1
TABLE B595
Organic Compounds Identified in Base Extract of Sample N0.196B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.666 Dichlorobutane 6
2 1.000 Camphor (IS)
3 2.462 ? 1
-------
291
TABLE B596
Volatile Organic Compounds Identified in Sample No.197S
Relati ve
Approximate
Peak
Retention
Level
No.
Time
Compound (ppb)
No peaks over 1 PPB.
TABLE B597
Organic Compounds Identified in Acid Extract of Sample No.l97A
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound {ppb)
1
0.352
1,1,2,2-Tetrachloroethane 1
2
0.430
Methyl-2-Ethyl Hexanoate (IS)
3
1.000
Methyl Palmitate 3
4
1.102
Methyl Stearate 3
TABLE B598
Organic Compounds Identified in Base Extract of Sample No.197B
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound (ppb)
1
0.637
Dichlorobutane 7
2
1.000
Camphor (IS)
3
2.451
? 2
-------
292
TABLE B599
Volatile Organic Compounds Identified in Sample No.l98S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B600
Organic Compounds Identified in Acid Extract of Sample N0.198A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.919 C]6 Alcohol 1
2 1.976 C17 Alcohol 1
3 1.000 Methyl Palmitate 1
4 1.027 C18 Alcohol 1
TABLE B601
Organic Compounds Identified in Base Extract of Sample N0.198B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
293
TABLE B602
Volatile Organic Compounds Identified in Sample N0.199S
Relative
Approximate
Peak
Retention
Level
No.
Time
Compound
(ppb)
1
0.502
Butadiene
2
2
1.000
Chioroform
1
TABLE B603
Organic Compounds Identified in Acid Extract of Sample
No.199A
Relative
Approximate
Peak
Retenti on
Level
No.
T ime
Compound
(ppb)
1
0.420
Methyl-2-Ethyl Hexanoate (IS)
2
1.000
Methyl Palmitate
2
3
1.104
Methyl Stearate
1
TABLE B604
Organic Compounds Identified in Base Extract of Sample
No.199B
Relative
Approximate
Peak
Retenti on
Level
No.
Time
Compound
(PPb)
1 0.656 Dichlorobutane
2 1.000 Camphor (IS)
4
-------
294
TABLE B605
Volatile Organic Compounds Identified in Sample No.200S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B606
Organic Compounds Identified in Acid Extract of Sample No.200A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.280 Dichlorobutane 1
2 0.362 Dichlorobutane 1
3 0.431 Methyl-2-Ethyl Hexanoate (IS)
4 1.000 Methyl Palmitate 1
TABLE B607
Organic Compounds Identified in Base Extract of Sample No. 200B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.653 Dichlorobutane 7
2 1.000 Camphor (IS)
-------
295
TABLE B608
Volatile Organic Compounds Identified in Sample No.201S
Relative Approximate
Peak Retention Level
No. T i me Compound (ppb)
No peaks over 1 PPB.
TABLE B609
Organic Compounds Identified in Acid Extract of Sample No.201A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.396 Methyl-2-Ethyl Hexanoate (IS)
2 0.758 ? 1
3 0.804 C14 Alcohol 1
4 0.891 Methyl Myristate 2
5 1.000 Methyl Palmitate 2
6 1.103 Methyl Stearate 2
-------
296
TABLE B610
Organic Compounds Identified in Base Extract of Sample No.20TB
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.659 Dichlorobutane 1
2 1.000 Camphor (IS)
3 2.481 Diethyl Hexyl Phthalate 1
TABLE B611
Volatile Organic Compounds Identified in Sample No.202S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
TABLE B612
Organic Compounds Identified in Acid Extract of Sample No.202A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
No peaks over 1 PPB.
-------
297
TABLE B613
Organic Compounds Identified in Base Extract of Sample No.202B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.644 Dichlorobutane 3
2 1.000 Camphor (IS)
TABLE B614
Volatile Organic Compounds Identified in Sample No.203S
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1.000 Chloroform
TABLE B615
Organic Compounds Identified in Acid Extract of Sample No.203A
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.443 Methyl-2-Ethyl Hexanoate (IS)
2 1.000 Methyl Palmitate 1
3 1.096 Methyl Stearate 1
-------
298
TABLE B616
Organic Compounds Identified in Base Extract of Sample No.203B
Peak
No.
Relative
Retenti on
Time Compound
Approximate
Level
(ppb)
1
0.631 Dichlorobutane
5
2
1.000 Camphor (IS)
3
2.409 Butyl Phthalyl
Butyl Glycolate 3
TABLE
B617
Volatile Organic Compounds
Identified in Sample No.204S
Peak
No.
Relative
Retention
Time Compound
Approximate
Level
(ppb)
No peaks over 1
PPB.
TABLE
B618
Organic Compounds Identified in Acid Extract of Sample No.204A
Peak
No.
Relative
Retention
Time Compound
Approximate
Level
(ppb)
1
2
3
0.420
0.815
1.000
Methyl-2-Ethyl Hexanoate (IS)
C.|0 Terpineol
Methyl Palmitate
1
1
-------
299
TABLE B619
Organic Compounds Identified in Base Extract of Sample No.204B
Relative Approximate
Peak Retention Level
No. Time Compound (ppb)
1 0.639 Dichlorobutane 3
2 1.000 Camphor (IS)
3 1.532 C^g Terpineol 3
4 2.412 ? 1
-------