PEER REVIEW DRAFT- DO NOT CITE OR QUOTE A EPA June 2019 United States Office of Chemical Safety and Environmental Protection Agency Pollution Prevention Environmental Hazard Extended Data Extraction Supplemental Document For Draft Risk Evaluation of Cyclic Aliphatic Bromide Cluster (HBCD) CASRN NAME 25637-99-4 Hexabromocyclododecane 3194-55-6 1,2,5,6,9,10-Hexabromocyclododecane 3194-57-8 1,2,5,6-Tetrabromocyclooctane June, 2019 1 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE Table of Contents Table 1. On-topic aquatic toxicity studies that were evaluated for HBCD 3 Table 2. On-topic terrestrial toxicity studies that were evaluated for HBCD 54 2 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE Tabke 1. On-topic aquatic toxicity studies that were evaluated for HBCD CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. Aquatic Vegetation 25637-99-4 Green algae (Pseudokirc hneriella subcapitata) Fresh 24-hour ECio = >0.0037 mg AI/L (0.0037 is the mean of the Day 0 and Day 4 6.8 mg/L measurements) 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022, 3.38, 0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@au thor-year} High 1928298 25637-99-4 Green algae (P seudokirchne riella subcapitata) Fresh 24-hour EC50 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 24-hour EC90 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 48-hour EC10 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 48-hour EC50 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 3 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Green algae (P seudokirchne riella subcapitata) Fresh 48-hour EC90 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 72-hour EC10 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 72-hour EC50 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 72-hour EC90 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 96-hour EC10 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 96-hour EC50 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 4 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Green algae (P seudokirchne riella subcapitata) Fresh 96-hour EC90 = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Abundance (cell density); Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Green algae (Pseudokirchne riella subcapitata) Fresh 96-hour NOEC = >0.0037 mg AI/L 0.0015, 0.0022, 0.0032, 0.0046, 0.0068 mg/L (nominal); 0.0013, 0.0022,3.38,0.0042, 0.0064 mg/L (measured, Day 0) Static, Measured. Solvent: Dimethylformamide Population growth rate (area under growth curve) {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Diatom (Skeletonema costatum) Salt 72-hour EC50 = 0.0101 mg AI/L; Seawater, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 1927837 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC5o = 0.01 mg AI/L; Seawater, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC50 = 0.0122 mg AI/L; Rila Marine Mix, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC5o = 0.0118 mg AI/L; Rila Marine Mix, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (,Skeletonema costatum) Salt 72-hour EC5o = 0.01 mg AI/L; Instant Ocean sea salts, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (,Skeletonema costatum) Salt 72-hour EC5o = 0.01 mg AI/L; Instant Ocean sea salts, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC5o = 0.0113 mg AI/L; Utikem seawater compound, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC5o = 0.0113 mg AI/L; Utikem seawater compound, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) Walsh, 1987, 1927837@@auth or-year} High 5 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Diatom (Skeletonema costatum) Salt 72-hour EC50 = 0.0095 mg AI/L; HW Marine Mix, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Skeletonema costatum) Salt 72-hour EC50 = 0.009 mg AI/L; HW Marine Mix, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.07 mg AI/L; Seawater, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.08 mg AI/L; Seawater, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.38 mg AI/L; Rila Marine Mix, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.36 mg AI/L; Rila Marine Mix, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC5o = 0.15 mg AI/L; Instant Ocean sea salts, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (.Thalassiosira pseudonana) Salt 72-hour EC5o = 0.14 mg AI/L; Instant Ocean sea salts, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.1 mg AI/L; 40 fathoms marine mix, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.1 mg AI/L; 40 fathoms marine mix, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.09 mg AI/L; Utikem seawater compound, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.09 mg AI/L; Utikem seawater compound, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.05 mg AI/L; HW Marine Mix, Test 1 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 25637-99-4 Diatom (Thalassiosira pseudonana) Salt 72-hour EC50 = 0.04 mg AI/L; HW Marine Mix, Test 2 Not Reported Static, Measured, Solvent: Acetone Population change (change in N/change in time) {Walsh, 1987, 1927837@@auth or-year} High 6 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Blue-green Algae (Spirulina subsalsa) Fresh 168-hour BCF = 350 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable 2343690 134237-50-6 Green Algae (Scenedesmus acutus var. acutus) Fresh 168-hour BCF = 407 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable 134237-51-7 Blue-green Algae {Spirulina subsalsa) Fresh 168-hour BCF = 270 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable 134237-51-7 Green Algae (.Scenedesmus acutus var. acutus) Fresh 168-hour BCF = 469 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable 134237-52-8 Green Algae (.Scenedesmus acutus var. acutus) Fresh 168-hour BCF = 390 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable 134237-52-8 Blue-green Algae {Spirulina subsalsa) Fresh 168-hour BCF = 174 0.002 mg/L Static, Measured Residue; Bioconcentration {Zhang, 2014, 2343690@@auth or-year} Unacceptable Aquatic Invertebrates 3194-55-6 Water flea {Daphnia magna) Fresh 3-hour ECo = 1000 mg AI/L 0,0.01,0.1,1, 10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 1928267 3194-55-6 Water flea {Daphnia magna) Fresh 3-hour EC50 = >1000 mg AI/L 0, 0, 0.01,0.1, 1, 10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea {Daphnia magna) Fresh 3-hour EC100 = >1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea {Daphnia magna) Fresh 6-hour ECo = 1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea {Daphnia magna) Fresh 6-hour EC5o = >1000 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 7 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Water flea (Daphnia magna) Fresh 6-hour ECioo = >1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (,Daphnia magna) Fresh 24-hour ECo = 1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (,Daphnia magna) Fresh 24-hour EC50 = >1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (.Daphnia magna) Fresh 24-hour EC100 = >1000 mg AI/L 0, 0,0.01,0.1, 1, 10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (.Daphnia magna) Fresh 48-hour ECo = 1 mg AI/L ,0, 0,0.01,0.1,1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (.Daphnia magna) Fresh 48-hour EC50 = 146.34 mg AI/L 0,0.01,0.1,1, 10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 3194-55-6 Water flea (.Daphnia magna) Fresh 48-hour EC100 = >1000 mg AI/L 0, 0,0.01,0.1, 1,10, 100, 1000 mg/L Static, Nominal Behavioral: Swimming {BASF, 1990, 1928267@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 48-hour No Mortality/Immobility Concentration NR ZERO ~ 0.0032 mg AI/L 0, 0,0.0018,0.0021, 0.0023, 0.0024, 0.0032 mg/L Flow-through, Measured, Solvent: Dimethylformamide (DMF) Mortality, immobility {Wildlife Intl LTD, 1997, 1928297@@auth or-year} High 1928297 25637-99-4 Water flea (.Daphnia magna) Fresh 48-hour EC50 = >0.0032 mg AI/L 0, 0,0.0018,0.0021, 0.0023, 0.0024, 0.0032 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928297@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 48-hour NOEC = 0.0032 mg AI/L 0, 0,0.0018,0.0021, 0.0023, 0.0024, 0.0032 mg/L Flow-through, Measured, Solvent: DMF Mortality, Immobility {Wildlife Intl LTD, 1997, 1928297@@auth or-year} High 25637-99-4 Water flea (,Daphnia magna) Fresh 24-hour EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 1928243 25637-99-4 Water flea (.Daphnia magna) Fresh 48-hour EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 8 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Water flea (Daphnia magna) Fresh 96-hour EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 7-day EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 14-day EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (,Daphnia magna) Fresh 21-day EC50 = >0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality; Progeny counts/ numbers {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day NOEC = 0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day NOEC = 0.0056 mg AI/L; LOEC = 0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Progeny counts/numbers; Growth: Weight {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day LOEC = 0.0056 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Growth: Length {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day NOEC = 0.0031 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Growth: Length {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day MATC = 0.0042 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Growth: Length {Wildlife Intl LTD, 1998, 1928243@@auth or-year} High 25637-99-4 Water flea (.Daphnia magna) Fresh 21-day NOAEL = 0.0056 mg AI/L; LOAEL = 0.011 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Reproductive success (young per reproductive day); Growth: Weight {Drottar, 1998, 3809169@@auth or-year} High 3809169 9 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Water flea (Daphnia magna) Fresh 21-day NOAEL = 0.0031 mg AI/L; LOAEL = 0.0056 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Growth: Length {Drottar, 1998, 3809169@@auth or-year} High 25637-99-4 Water flea (Daphnia magna) Fresh 21-day MATC = 0.0042 mg AI/L 0, 0,0.00087,0.0016, 0.0031,0.0056,0.011 mg/L Flow-through, Measured, Solvent: DMF Growth: Length {Drottar, 1998, 3809169@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: Dimethyl sulfoxide (DMSO) 7-Ethoxyresorufin O-deethylase; Glutathione (reduced glutathione); DNA damage {Zhang, 2014, 2528343@@auth or-year} High 2528343 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 3-day LOAEL = 0.000086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 6-day LOAEL = 0.000086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione); Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day LOAEL = 0.000086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione) {Zhang, 2014, 2528343@@auth or-year} High 10 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day LOAEL = 0.000086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione) {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.0086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 3-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione); Lipid peroxidation; DNA damage {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 6-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage; Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day NOAEL = 0.00086 mg AI/L; LOAEL = 0.0086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage {Zhang, 2014, 2528343@@auth or-year} High 11 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.00086 mg AI/L; LOAEL = 0.0086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Gill tissue 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L ; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione (reduced glutathione); DNA damage {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 3-day LOAEL = 0.000086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 6-day LOAEL = 0.000086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione); Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 12 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day LOAEL = 0.000086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione) {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day LOAEL = 0.000086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione) {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.0086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 3-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Digestive gland 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Glutathione S- transferase; Superoxide dismutase (SOD) enzyme activity; Glutathione (reduced glutathione); DNA damage; Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 6-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Digestive gland 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage {Zhang, 2014, 2528343@@auth or-year} High 13 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Digestive gland 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage; Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day NOAEL = 0.00086 mg AI/L; LOAEL = 0.0086 mg AI/L; Digestive gland 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO DNA damage {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 1-day NOAEL = 0.00086 mg AI/L; LOAEL = 0.0086 mg AI/L; Digestive gland 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 3194-55-6 Japanese Littleneck Clam (Venerupis philippinarum) Salt 15-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L; Digestive gland 0.000086, 0.00086, 0.0086 mg/L Renewal, Not reported, Solvent: DMSO Lipid peroxidation {Zhang, 2014, 2528343@@auth or-year} High 25637-99-4 Japanese Littleneck Clam (Venerupis philippinarum) Salt 3-day LOAEL = 0.000086 mg AI/L 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Nominal, Solvent: DMSO Ferritin mRNA; Catalase mRNA; Dihydrodiol dehydrogenase mRNA; Cytochrome c oxidase subunit 1 mRNA; NADH: ubiquinone reductase (H(+)- translocating) mRNA {Zhang, 2014, 2528343@@auth or-year} Unacceptable 1928024 14 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day LOAEL = 0.000086 mg AI/L 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Nominal, Solvent: DMSO Ferritin mRNA; Catalase mRNA; Dihydrodiol dehydrogenase mRNA; C-type Lectin like mRNA; Elongation factor- 1 alpha mRNA; Hemocyanin subunit 2 mRNA {Zhang, 2014, 2528343@@auth or-year} Unacceptable 25637-99-4 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day NOAEL = 0.0086 mg AI/L 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Nominal, Solvent: DMSO Cytochrome c oxidase subunit 1 mRNA {Zhang, 2014, 2528343@@auth or-year} Unacceptable 25637-99-4 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day NOAEL = 0.000086 mg AI/L; LOAEL = 0.00086 mg AI/L 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Nominal, Solvent: DMSO NADH: ubiquinone reductase (H(+)- translocating) mRNA {Zhang, 2014, 2528343@@auth or-year} Unacceptable 25637-99-4 Japanese Littleneck Clam (Venerupis philippinarum) Salt 10-day NOAEL = 0.00086 mg AI/L; LOAEL = 0.0086 mg AI/L 0, 0.000086, 0.00086, 0.0086 mg/L Renewal, Nominal, Solvent: DMSO Purine nucleoside phosphorylase mRNA {Zhang, 2014, 2528343@@auth or-year} Unacceptable 25637-99-4 Sea urchin (Psammechinus miliaris) Salt 72 hours post fertilization NOAEL= 0.06416989 mg AI/L; Exp. A 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 1274149 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 72 hours post fertilization NOAEL = 0.032 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 2-4 days post fertilization NOAEL = 0.032 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. A 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (,Psammechinus miliaris) Salt 2-4 days post fertilization NOAEL = 0.032 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 15 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 2-4 days post fertilization ECso = 0.0453 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 7-9 days post fertilization NOAEL = 0.0320 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (,Psammechinus miliaris) Salt 7-9 days post fertilization ECso = 0.040407 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 14-16 days post fertilization NOAEL = 0.0325 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. A 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 14-16 days post fertilization EC50 = 0.056 mg AI/L; Exp. A 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 14-16 days post fertilization NOAEL = 0.0325 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (,Psammechinus miliaris) Salt 14-16 days post fertilization EC50 = 0.035mg AI/L; Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 16 days post fertilization NOAEL = 0.032 mg AI/L; LOAEL = 0.064 mg AI/L; Exp. A 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Develop- ment {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Sea urchin (.Psammechinus miliaris) Salt 16 days post fertilization NOAEL = 0.0058 mg AI/L; LOAEL = 0.016 mg AI/L Exp. B 0, 0.006,0.016, 0.032, 0.064 mg/L Renewal, Nominal, Solvent: DMSO Growth: Develop- ment {Anselmo, 2011, 1274149@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 96-hour NOEC = 0.8 mg AI/L; LOEC = >0.8 mg AI/L 0, 0,0.08,0.3,0.8 mg/L Renewal, Nominal, Solvent: DMSO Mortality {Shi, 2017, 3546057@@auth or-year} High 3546057 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 96-hour Kinetic BCF = 87,300 0, 0.002 mg/L Renewal, Nominal Residue; bioconcentration {Shi, 2017, 3546057@@auth or-year} High 16 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 96-hour Steady-State BCF = 63,400 0, 0.002 mg/L Renewal, Nominal Residue; bioconcentration {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 96-hour Lipid-Normalized Kinetic BCF = 78,400 0, 0.002 mg/L Renewal, Nominal Residue; bioconcentration {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 3-day NOAEL = 0.8 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Glutathione S- transferase mRNA; p53 mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 7-day NOAEL = 0.8 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Glutathione S- transferase mRNA; Catalase; p53 mRNA; Superoxide dismutase mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 14-day NOAEL = 0.3 mg AI/L; LOAEL = 0.8 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Glutathione S- transferase mRNA; 8- oxoguanine DNA glycosylase mRNA; p53 mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 3-day NOAEL = 0.3 mg AI/L; LOAEL = 0.8 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Catalase; 8- oxoguanine DNA glycosylase mRNA; Superoxide dismutase mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 14-day LOAEL = 0.3 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Catalase; Caspase-3 mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 7-day NOAEL = 0.3 mg AI/L; LOAEL = 0.8 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO 8-oxoguanine DNA glycosylase mRNA {Shi, 2017, 3546057@@auth or-year} High 17 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 3-day LOAEL = 0.3 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Caspase-3 mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 7-day LOAEL = 0.3 mg AI/L 0, 0, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Caspase-3 mRNA {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 10-day NOAEL = 0.8 mg AI/L; F0 generation 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Reproductive: Fecundity; Progeny counts/numbers; Sex ratio {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 10-day NOAEL = 0.8 mg AI/L; F1 generation 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Reproductive: Fecundity; Progeny counts/numbers; Sex ratio {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 20-day NOEC = 0.08 mg AI/L; LOEC = 0.3 mg AI/L; F0 generation; maturation period 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Growth, Developmental stage {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 20-day NOEC = 0.008 mg AI/L; LOEC = 0.03 mg AI/L; F1 generation; maturation period 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Growth, Developmental stage {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 20-day NOEC = 0.008 mg AI/L; LOEC = 0.03 mg AI/L; F0 generation; nauplius phase 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Growth, Developmental stage {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (Tigriopus japonicus) Salt 20-day LOEC = 0.008 mg AI/L; F1 generation; nauplius phase 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Growth, Developmental stage {Shi, 2017, 3546057@@auth or-year} High 25637-99-4 Harpacticoid Copepod (.Tigriopus japonicus) Salt 40-day NOEC = 0.8 mg AI/L 0, 0, 0.008, 0.03, 0.08, 0.3, 0.8 mg/L Renewal, Nominal, Solvent: DMSO Mortality {Shi, 2017, 3546057@@auth or-year} High 18 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Balic Macoma Or Clam (Macoma balthica) Salt 50-day LOAEL = 0.1 mg/L 0, 0.1, 0.25 mg/L Multiple routes, Nominal Nuclear abnormality: micronuclei; frequency of dead cells; Mean number of nucleoli; binucleated cells, formation of nucleoplasmic bridges, nuclear buds, occurrence of pleomorphic and hypertrophic cells {Smolarz, 2009, 1927697@@auth or-year} High 1927697 25637-99-4 Amphipod (.Hyalella azteca) Fresh 28-day NOEC > 1000 mg/kg dwt sediment 31,63, 125,250, 500 and 1,000 mg/kg dwt sediment (Nominal concentrations) Flow-through, Measured, Solvent: DMF range- finding study conducted in the presence of 2 % TOC. Further study details were not provided. reduced survivability {Thomas, 2003, 4269889@@auth or-year} High 4269889 25637-99-4 Amphipod (.Hyalella azteca) Fresh 28-day LOEC = 1000 mg/kg dwt sediment 31,63, 125,250, 500 and 1,000 mg/kg dwt sediment (Nominal concentrations) Flow-through, Measured, Solvent: DMF range- finding study conducted in the presence of 2 % TOC. Further study details were not provided. reduced survivability {Thomas, 2003, 4269889@@auth or-year} High 25637-99-4 Amphipod (.Hyalella azteca) Fresh 28-day NOEC = 1000 mg/kg dwt sediment 31,63, 125,250, 500 and 1,000 mg/kg dwt sediment (Nominal concentrations) Flow-through, Measured, Solvent: DMF range- finding study conducted in the presence of 5% TOC. Further study details were not provided. reduced survivability {Thomas, 2003, 4269912@@auth or-year} High 4269912 25637-99-4 Amphipod {Hyalella azteca) Fresh 28-day NOEC = 1000 mg/kg dwt sediment 31,63, 125,250, 500 and 1,000 mg/kg dwt sediment (Nominal concentrations) Flow-through, Measured, Solvent: DMF range- finding study conducted in the presence of 5% TOC. Further study details were not provided. reduced survivability {Thomas, 2003, 4269912@@auth or-year} High 19 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. Worm (Lumbriculus variegatus) Fresh 28-day NOEC = 3.1 mg/kg dry weight sediment 0.05, 0.5, 5, 50, and 500 mg/kg dry weight sediment, measured concentrations were ND, 0.2, 3.1,28.7, and 303.2 mg/kg dry weight. 28-day static test using dechlorinated tap water measured concentrations- 0,nd3, 0.25, 3.25, 29.25 and 311.35 mg/kg sediment dw; 40 worms per treatment; artificial sediment: 1.8% organic carbon, grain size 100-2000 jxm; Total number of worms {Oetken, 2001, 3809143@@autho r-year} High 3809143 Worm (Lumbriculus variegatus) Fresh 28-day LOEC = 28.7 mg/kg dry weight sediment 0.05, 0.5, 5, 50, and 500 mg/kg dry weight sediment, measured concentrations were ND, 0.2, 3.1,28.7, and 303.2 mg/kg dry weight. 28-day static test using dechlorinated tap water measured concentrations- 0,nd3, 0.25, 3.25, 29.25 and 311.35 mg/kg sediment dw; 40 worms per treatment; artificial sediment: 1.8% organic carbon, grain size 100-2000 |im; Total number of worms {Oetken, 2001, 3809143@@autho r-year} High Worm (Lumbriculus variegatus) Fresh 28-day NOEC = 28.7 mg/kg dry weight sediment 0.05, 0.5, 5, 50, and 500 mg/kg dry weight sediment, measured concentrations were ND, 0.2, 3.1,28.7, and 303.2 mg/kg dry weight. 28-day static test using dechlorinated tap water measured concentrations- 0,nd3, 0.25, 3.25, 29.25 and 311.35 mg/kg sediment dw; 40 worms per treatment; artificial sediment: 1.8% organic carbon, grain size 100-2000 |im; Large vs small worms {Oetken, 2001, 3809143@@autho r-year} High Worm (Lumbriculus variegatus) Fresh 28-day NOEC = 3.1 mg/kg dry weight sediment 0.05, 0.5, 5, 50, and 500 mg/kg dry weight sediment, measured concentrations were ND, 0.2, 3.1,28.7, and 303.2 mg/kg dry weight. 28-day static test using dechlorinated tap water measured concentrations- 0,nd3, 0.25, 3.25, 29.25 and 311.35 mg/kg sediment dw; 40 worms per treatment; artificial sediment: 1.8% organic carbon, grain size 100-2000 |xm; Large vs small worms {Oetken, 2001, 3809143@@autho r-year} High Aquatic Vertebrates 20 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 1837-91-8 Rainbow trout (Oncorhynchus mykiss) Fresh 2-hour NOAEL = 27.877 mg AI/L 0, 27.877 mg/L Ln vitro, Nominal Insulin-like growth factor 1 mRNA; Signal Transducer and Activator of Transcription protein 5 {Reindl, 2011, 3586425@@auth or-year} High 3586425 25637-99-4 Bluegill (Lepomis macrochirus) Fresh 24-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal, Solvent: Acetone Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} High 1928289 25637-99-4 Bluegill (,Lepomis macrochirus) Fresh 48-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal, Solvent: Acetone Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} High 25637-99-4 Bluegill (.Lepomis macrochirus) Fresh 96-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal, Solvent: Acetone Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} High 25637-99-4 Bluegill (,Lepomis macrochirus) Fresh 96-hour NOEC = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal, Solvent: Acetone Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} High 25637-99-4 Bluegill (.Lepomis macrochirus) Fresh 96-hour NR-ZERO = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal, Solvent: Acetone Abnormal behavior {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} High 3194-55-6 Zebrafish (Danio rerio) Fresh 72-hour NOAEL = 32 mg AI/L 0, 32 mg/L Static, Nominal Thyroxine {Thienpont, 2011, 1062065@@auth or-year} Low 1062065 25637-99-4 Bluegill (.Lepomis macrochirus) Fresh 24-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} Unacceptable 1928239 21 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Bluegill (Lepomis macrochirus) Fresh 48-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} Unacceptable 25637-99-4 Bluegill (,Lepomis macrochirus) Fresh 96-hour LC50 = >100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} Unacceptable 25637-99-4 Bluegill (.Lepomis macrochirus) Fresh 96-hour NOEC = 100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal Abnormal behavior {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} Unacceptable 25637-99-4 Bluegill (,Lepomis macrochirus) Fresh 96-hour NR-ZERO = 100 mg AI/L 0, 0, 10.0, 18.0, 32.0, 56.0,100.0 mg/L Static, Nominal Mortality {Great Lakes Chem Corp, 1994, 1928289@@auth or-year} Unacceptable 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 24-hour LC50 = >0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured. Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 3586422 ! 928298 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 48-hour LC50 = >0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 72-hour LC50 = >0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 96-hour LC50 = >0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 96-hour NOEC = 0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 22 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 96-hour NR-ZERO = >0.0025 mg AI/L 0, 0,0.00075,0.0015, 0.0023, 0.0023, 0.0025 mg/L Flow-through, Measured, Solvent: DMF Mortality {Wildlife Intl LTD, 1997, 1928298@@auth or-year} High 3194-55-6 Zebrafish Not 47-hour NOAEL = 0.128 mg 0,0.001,0.013,0.128 Renewal, Nominal, Hatching rate {Wu, 2013, High 1927533 (Danio rerio) reported AI/L mg/L Solvent: DMSO 1927533@@auth or-year} 3194-55-6 Zebrafish Not 47-hour NOAEL = 0.013 mg 0,0.001,0.013,0.128 Renewal, Nominal, Heart rate {Wu, 2013, High (Danio rerio) reported AI/L; LOAEL = 0.128 mg AI/L mg/L Solvent: DMSO 1927533@@auth or-year} 3194-55-6 Zebrafish Not 59-hour LOAEL = 0.001 mg 0,0.001,0.013,0.128 Renewal, Nominal, Heart rate {Wu, 2013, High {Danio rerio) reported AI/L mg/L Solvent: DMSO 1927533@@auth or-year} 3194-55-6 Zebrafish Not 71-hour LOAEL = 0.001 mg 0,0.001,0.013,0.128 Renewal, Nominal, Heart rate; T-box {Wu, 2013, High {Danio rerio) reported AI/L mg/L Solvent: DMSO 5amRNA; Homeobox protein Nkx-2.5 mRNA 1927533@@auth or-year} 3194-55-6 Zebrafish Not 71-hour NOAEL = 0.001 mg 0,0.001,0.013,0.128 Renewal, Nominal, Cardiac {Wu, 2013, High {Danio rerio) reported AI/L; LOAEL = 0.013 mg AI/L mg/L Solvent: DMSO arrhythmia 1927533@@auth or-year} 23 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 3194-55-6 Zebrafish (Danio rerio) Not reported 71-hour NOAEL = 0.128 mg AI/L 0,0.001,0.013,0.128 mg/L Renewal, Nominal, Solvent: DMSO ATPase, Ca++ transporting, cardiac muscle, slow twitch 2a mRNA; Troponin T type 2a (cardiac) mRNA; myH6 expression; End-diastolic Volume; Stroke volume; Caspase 3; Actin, alpha, cardiac muscle la mRNA; Myosin, heavy chain 6, cardiac muscle, alpha mRNA; Cardiac output; End-systolic Volume; Mortality; Abnormal; whole malformation rate {Wu, 2013, 1927533@@auth or-year} High 3194-55-6 Zebrafish {Danio rerio) Not reported 71-hour NOAEL = 0.013 mg AI/L; LOAEL = 0.128 mg AI/L 0,0.001,0.013,0.128 mg/L Renewal, Nominal, Solvent: DMSO ATPase, Ca++ transporting, cardiac muscle, slow twitch 2b mRNA; Ryanodine receptor 2a (cardiac) mRNA {Wu, 2013, 1927533@@auth or-year} High 134237-52-8 Zebrafish (Danio rerio) Fresh 44-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, 1.0 mg/L Renewal, Nominal, Solvent: DMSO Heart rate {Du, 2012, 1927610@@auth or-year} High 1927610 134237-52-8 Zebrafish (Danio rerio) Fresh 68-hour LOEC = 0.01 mg AI/L 0, 0.01,0.1, 1.0 mg/L Renewal, Nominal, Solvent: DMSO Hatching success {Du, 2012, 1927610@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 92-hour NOEC = 0.1 mg AI/L; LOEC = 1 mg AI/L 0, 0.01,0.1, 1.0 mg/L Renewal, Nominal, Solvent: DMSO Heart rate {Du, 2012, 1927610@@auth or-year} High 24 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Zebrafish (Danio rerio) Fresh 92-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Length {Du, 2012, 1927610@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 92-hour LOEC = 0.01 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Mortality {Du, 2012, 1927610@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 116-hour LOEC = 0.01 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal. Malformation rate {Du, 2012, 1927610@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 116-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Reactive oxygen species; Caspase 3; Caspase 9 {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 44-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Heart rate {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 68-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Hatching success {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 92-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Length; Heart rate; Mortality {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 116-hour LOEC = 0.01 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal. Malformation rate {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 116-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Reactive oxygen species {Du, 2012, 1927610@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 116-hour NOEC = 0.1 mg AI/L; LOEC = 1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Caspase 3; Caspase 9 {Du, 2012, 1927610@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 44-hour NOEC = 0.1 mg AI/L; LOEC = 1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Heart rate {Du, 2012, 1927610@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 68-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Hatching success {Du, 2012, 1927610@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 92-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Heart rate {Du, 2012, 1927610@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 92-hour NOEC = 0.1 mg AI/L; LOEC = 1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Length; Mortality {Du, 2012, 1927610@@auth or-year} High 25 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Zebrafish (Danio rerio) Fresh 116-hour NOEC = 0.01 mg AI/L; LOEC = 0.1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal. Malformation rate {Du, 2012, 1927610@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 116-hour NOEC = 0.1 mg AI/L; LOEC = 1 mg AI/L 0, 0.01,0.1, l.Omg/L Renewal, Nominal, Solvent: DMSO Reactive oxygen species; Caspase 3; Caspase 9 {Du, 2012, 1927610@@auth or-year} High 3194-55-6 Zebrafish {Danio rerio) Fresh 92-hour LOAEL = 0.05 mg AI/L 0,0.05,0.1,0.5,1.0 mg/L Aquatic-not reported, Nominal, Solvent: DMSO Heart rate; bax mRNA; Mortality {Deng, 2009, 1927716@@auth or-year} High 1927716 3194-55-6 Zebrafish {Danio rerio) Fresh 92-hour NOAEL = 0.05 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.05,0.1,0.5,1.0 mg/L Aquatic-not reported, Nominal, Solvent: DMSO Growth: Length; Reactive oxygen species; Caspase- 3 mRNA expression profile; Caspase-9 mRNA expression profile; Growth: Abnormal malformation rate {Deng, 2009, 1927716@@auth or-year} High 3194-55-6 Zebrafish {Danio rerio) Fresh 92-hour NOAEL = 0.5 mg AI/L; LOAEL = 1 mg AI/L 0,0.05,0.1,0.5,1.0 mg/L Aquatic-not reported, Nominal, Solvent: DMSO p53 mRNA; E3 ubiquitin-protein ligase; Bcl-2- binding component 3 mRNA; Bcl-2 mRNA; Apoptotic protease- activating factor 1 mRNA; Caspase- 3 mRNA induction; Caspase-9 mRNA induction {Deng, 2009, 1927716@@auth or-year} High 25637-99-4 Zebrafish {Danio rerio) Fresh 96-hour LOAEL = 0.002 mg AI/L 0, 0.002,0.01,0.1, 0.5,2.5,10 mg/L Renewal, Nominal, Solvent: DMSO Hatch delay {Hu, 2009, 1927732@@auth or-year} High 1927732 25637-99-4 Zebrafish {Danio rerio) Fresh 96-hour NOAEL = 10 mg AI/L 0, 0.002,0.01,0.1, 0.5,2.5,10 mg/L Renewal, Nominal, Solvent: DMSO Mortality {Hu, 2009, 1927732@@auth or-year} High 26 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Zebrafish (Danio rerio) Fresh 96-hour NOAEL = 0.1 mg AI/L; LOAEL = 0.5 mg AI/L 0, 0.002,0.01,0.1, 0.5,2.5, lOmg/L Renewal, Nominal, Solvent: DMSO Malondialdehyde {Hu, 2009, 1927732@@auth or-year} High 25637-99-4 Zebrafish (Danio rerio) Fresh 96-hour NOAEL = 0.002 mg AI/L; LOAEL = 0.01 mg AI/L 0, 0.002,0.01,0.1, 0.5,2.5, lOmg/L Renewal, Nominal, Solvent: DMSO Heat shock protein 70 {Hu, 2009, 1927732@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 5-day NR-ZERO = 0.000017- 0.0003 mg AI/L 0, 0,0.000017- 0.0003 mg/L Flow-through, Measured, Solvent: Methanol Mortality {Lower, 2008, 3618094@@auth or-year} High 3618094 25637-99-4 Atlantic salmon (Salmo salar) Fresh 5-day NOAEL = 0.00005 mg AI/L; Exp. 1 0, 0.000005, 0.00005 mg/L Flow-through, Nominal, Solvent: Methanol Growth: Length; Growth: Weight; Gonado somatic index {Lower, 2008, 3618094@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 5-day NOAEL = 0.00005 mg AI/L; Exp. 2 0, 0, 0.000005, 0.00005 mg/L Flow-through, Nominal, Solvent: Methanol Growth: Length; Growth: Weight; Gonado somatic index {Lower, 2008, 3618094@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 5-day NOAEL = 0.000017- 0.0003 mg AI/L 0, 0,0.000017- 0.0003 mg/L Flow-through, Measured, Solvent: Methanol Condition index: 5-day freshwater dosing period, 3- day transfer to salt water; Sodium potassium ATPase; 5-day freshwater dosing period, 3-day transfer to salt water; Thyroxine; 5-day freshwater dosing period, 3- day transfer to salt water; Triiodothyronine; 5-day freshwater dosing period, 3- day transfer to salt water {Lower, 2008, 3618094@@auth or-year} High 27 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Atlantic salmon (Salmo salar) Fresh 5-day NOAEL = 0.00005 mg AI/L 0, 0.000005, 0.00005 mg/L Flow-through, Nominal, Solvent: Methanol Trans-epithelial voltage gradient; Accessory reproductive fluid; Testosterone {Lower, 2008, 3618094@@auth or-year} High 25637-99-4 Atlantic Fresh 5-day LOAEL = 0.000005 0, 0, 0.000005, Flow-through, Nominal, 11- {Lower, 2008, High salmon (Salmo salar) mg AI/L 0.00005 mg/L Solvent: Methanol Ketotestosterone; 17,20beta- Dihydroxy-4- pregnen-3-one 3618094@@auth or-year} 25637-99-4 Atlantic salmon (Salmo salar) Fresh 30-day NOEC = 0.000011 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Mortality, Growth: length; Condition Factor {Lower, 2008, 3618094@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 30-day LOEC = 0.000011 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Gill Na+/K+ ATPase activity; Plasma T4 {Lower, 2008, 3618094@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rams) Fresh 14-day NOAEL = 0.5 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Pentylresorufin O-deethylase; Reactive oxygen species; 7- Ethoxyresorufin O-deethylase; Thiobarbituric acid reactive substances; Protein carbonyls; DNA damage; Superoxide dismutase (SOD) enzyme activity; Glutathione disulfide (oxidized glutathione) {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 28-day NOAEL = 0.1 mg AI/L; LOAEL = 0.5 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Pentylresorufin O-deethylase; 7- Ethoxyresorufin O-deethylase; Superoxide dismutase (SOD) enzyme activity {Zhang, 2008, 1927768@@auth or-year} High 1927768 28 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 42-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Measured, Solvent: DMSO Pentylresorufin O-deethylase; 7- Ethoxyresorufm O-deethylase; Thiobarbituric acid reactive substances {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 28-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Reactive oxygen species; Protein carbonyls; DNA damage; Glutathione disulfide (oxidized glutathione) {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 42-day NOAEL = 0.001 mg AI/L; LOAEL = 0.01 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Reactive oxygen species; Protein carbonyls; DNA damage; Superoxide dismutase (SOD) enzyme activity {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 28-day NOAEL = 0.5 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Thiobarbituric acid reactive substances {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 42-day LOAEL = 0.001 mg AI/L 0, 0.001,0.01,0.1, 0.5 mg/L Renewal, Nominal, Solvent: DMSO Glutathione disulfide (oxidized glutathione) {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 42-day 34 mg/kg O.OOlmg/L Renewal, Nominal, Solvent: DMSO Residue; whole body HBCD concentration, wet weight {Zhang, 2008, 1927768@@auth or-year} High 25637-99-4 Chinese Rare Minnow (Gobiocypris rants) Fresh 42-day 654 mg/kg 0.5 mg/L Renewal, Nominal, Solvent: DMSO Residue: whole body HBCD concentration, wet weight {Zhang, 2008, 1927768@@auth or-year} High 29 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Atlantic salmon (Salmo salar) Fresh 7-day NOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Triiodothyronine; Thyroxine; Sodium potassium ATPase {Lower, 2007, 1927956@@auth or-year} High 1927956 25637-99-4 Atlantic salmon (Salmo salar) Fresh 14-day NOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Triiodothyronine; Thyroxine; Sodium potassium ATPase {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 21-day NOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Triiodothyronine; Thyroxine; Sodium potassium ATPase {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 28-day NOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Triiodothyronine; Sodium potassium ATPase {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 28-day LOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Thyroxine; {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 7-day LOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Smell/Sniff {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 17-day LOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Smell/Sniff {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 29-day LOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Smell/Sniff {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Atlantic salmon (Salmo salar) Fresh 30-day NOAEL = 0.000011 mg AI/L 0, 0.000011 mg/L Flow-through, Measured, Solvent: Methanol Mortality; Growth: Length; Growth: Weight; Condition index {Lower, 2007, 1927956@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 5-day LOAEL = <500 mg Al/kg bdwt 0, < 500 mg/kg bdwt Intraperitoneal, Nominal Cytochrome P1A {Ronisz, 2004, 192782 l@@auth or-year} High 1927821 30 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 5-day NOAEL = <500 mg Al/kg bdwt 0 50, < 500 mg/kg bdwt Intraperitoneal, Nominal DNA Adducts; 7- Ethoxyresorufm O-deethylase; Glutathione S- transferase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 5-day NOAEL = <500 mg Al/kg bdwt; Exp. 1 0, 50, < 500 mg/kg bdwt Intraperitoneal, Nominal Liver somatic index; Glutathione reductase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 5-day NOAEL = <500 mg Al/kg bdwt; Exp. 2 0, < 500 mg/kg bdwt Intraperitoneal, Nominal Liver somatic index; Glutathione reductase; Catalase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 28-day NOAEL = 50 mg Al/kg bdwt; LOAEL = <500 mg Al/kg bdwt 0, 50, < 500 mg/kg bdwt Intraperitoneal, Nominal Liver somatic index; 7-Ethoxy- resorufin O- deethylase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 28-day NOAEL = <500 mg Al/kg bdwt 0, 50, < 500 mg/kg bdwt Intraperitoneal, Nominal Glutathione reductase; Catalase; Glutathione S- transferase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 5-day LOAEL = 50 mg/kg bdwt; Exp. 1 0, 50, < 500 mg/kg bdwt Intraperitoneal, Nominal Catalase {Ronisz, 2004, 192782 l@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 5 days post fertilization LOAEL = 0.005 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Heart rate {Hong, 2014, 2343684@@auth or-year} High 2343684 25637-99-4 Indian Medaka Salt 8 days post LOAEL = 0.005 mg 0, 0.005,0.02, 0.05 Renewal, Nominal, Heart rate; {Hong, 2014, High (Oryzias melastigma) fertilization AI/L mg/L Solvent: DMSO Uncharacterized arginine/ serine- rich coiled-coil 1 mRNA 2343684@@auth or-year} 25637-99-4 Indian Medaka Salt 5 days post NOAEL = 0.02 mg 0, 0.005, 0.02, 0.05 Renewal, Nominal, Growth: {Hong, 2014, High (iOryzias melastigma) fertilization AI/L; LOAEL = 0.05 mg AI/L mg/L Solvent: DMSO Abnormal; SV- BA distance 2343684@@auth or-year} 31 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization NOAEL = 0.005 mg AI/L; LOAEL = 0.02 mg AI/L 0, 0.005, 0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal; SV- BA distance; Coiled coil domain containing 106 protein mRNA; Uncharacterized transmembrane and coiled-coil domain family 3 mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 5 days post fertilization NOAEL = 0.05 mg AI/L; LOAEL = 0.2 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO Caspase 3; Interleukin-1 beta {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization NOAEL = 0.05 mg AI/L; LOAEL = 0.2 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO Caspase 3; Caspase 8; Caspase 9; p53 mRNA; Interleukin-1 beta {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 5 days post fertilization NOAEL = 0.2 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO Caspase 8; Caspase 9 {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 5 days post fertilization NOAEL = 0.02 mg AI/L; LOAEL = 0.05 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO p53 mRNA; Tumor necrosis factor-alpha {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt First fry NOAEL = 0.05 mg AI/L; LOAEL = 0.2 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO p53 mRNA; Interleukin-1 beta; Tumor necrosis factor- alpha {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 8 days post fertilization NOAEL = 0.2 mg AI/L 0, 0.02,0.05,0.2 mg/L Renewal, Nominal, Solvent: DMSO Tumor necrosis factor-alpha {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 6 days post fertilization NOAEL = 0.005 mg AI/L; LOAEL = 0.02 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO 8-Oxo-2'-deoxy- guanosine {Hong, 2014, 2343684@@auth or-year} High 32 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization LOAEL = 0.05 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Uncharacterized polycomb protein mRNA; Uncharacterized short-chain de- hydrogenase/redu ctase family mRNA; 40S ribosomal protein SAmRNA; Brain-type fatty acid binding protein mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization NOAEL = 0.02 mg AI/L; LOAEL = 0.05 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Ribo se-pho sphate pyrophosphate kinase mRNA; Uncharacterized bromodomain and WD repeat domain containing 3 mRNA; Uncharacterized parvalbumin beta- like mRNA; Ubiquitin- conjugating protein (E2)-like mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 8 days post fertilization NOAEL = 0.005 mg AI/L; LOAEL = 0.02 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Uncharacterized myosin regulatory light chain mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization LOAEL = 0.005 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Choriogenin L mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 8 days post fertilization LOAEL = 0.02 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Vitellogenin 2 mRNA {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (iOryzias melastigma) Salt 8 days post fertilization NOAEL = 0.05 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Vitellogenin-like protein {Hong, 2014, 2343684@@auth or-year} High 33 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 17 days post fertilization NOAEL = 0.02 mg AI/L; LOAEL = 0.05 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Growth: Abnormal; malformations {Hong, 2014, 2343684@@auth or-year} High 25637-99-4 Indian Medaka (Oryzias melastigma) Salt 17 days post fertilization NOAEL = 0.05 mg AI/L 0, 0.005,0.02, 0.05 mg/L Renewal, Nominal, Solvent: DMSO Mortality; Hatching success; Hatchout time {Hong, 2014, 2343684@@auth or-year} High 134237-52-8 Indian Medaka (Oryzias melastigma) Salt 5-day post fertilization NOAEL = 0.0084- 0.0163 mg AI/L; LOAEL = 0.0165- 0.0324 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0084- 0.0163 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 3350507 134237-52-8 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0165- 0.0324mg AI/L; LOAEL = 0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Growth, abnormal. SV- BA distance; Interleukin 1 beta mRNA; Tumor necrosis factor mRNA {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0084- 0.0163 mg AI/L 0, 0.0084-0.0163, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Caspase 3 {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0084- 0.0163 mg AI/L; LOAEL = 0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Caspase 8; Caspase 9 {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (Oryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0084- 0.0163 mg AI/L; LOAEL = 0.0165- 0.0324 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO p53 mRNA {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (iOryzias melastigma) Salt >8-< 17-day post fertilization NOAEL = 0.0017- 0.0324 mg AI/L; LOAEL = 0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO p53 mRNA, newly hatched larvae; Interleukin 1 beta mRNA, newly hatched larvae; Tumor necrosis factor mRNA; newly hatched larvae {Hong, 2015, 3350507@@auth or-year} High 34 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Indian Medaka (Oryzias melastigma) Salt 6-day post fertilization NOAEL = 0.0017- 0.0324 mg AI/L; LOAEL = 0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO 8-Oxo-2'- deoxyguanosine {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (Oryzias melastigma) Salt 17-day post fertilization NOAEL = 0.0017- 0.0324 mg AI/L; LOAEL =0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Growth: Abnormal; Malformation rate {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Indian Medaka (Oryzias melastigma) Salt 17-day post fertilization NOAEL =0.1212- 0.1568 mg AI/L 0, 0.0084-0.0163, 0.0165-0.0324, 0.1212-0.1568 mg/L Renewal, Measured, Solvent: DMSO Mortality; Hatching rate {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 5-day post fertilization LOAEL = 0.1326- 0.1845 mg AI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0082- 0.0145 mg AI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.021- 0.0341 mg AI/L; LOAEL = 0.1326- 0.1845 mg AI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Growth, abnormal. SV- BA distance; p53 mRNA; Tumor necrosis factor mRNA {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0082- 0.0145 mg AI/L 0, 0.0082-0.0145, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Caspase 3; Caspase 9 {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0082- 0.0145 mg AI/L; LOAEL = 0.1326- 0.1845 mg AI/L 0, 0.0082-0.0145, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Caspase 8 {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (Oryzias melastigma) Salt >8-< 17-day post fertilization NOAEL = 0.021- 0.0341 mg AI/L; LOAEL = 0.1326- 0.1845 mg AI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO p53 mRNA, newly hatched larvae; Tumor necrosis factor mRNA, newly hatched larvae {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0082- 0.0145 mg AI/L; LOAEL = 0.0205- 0.0341 mg AI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Interleukin 1 beta mRNA {Hong, 2015, 3350507@@auth or-year} High 35 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Indian Medaka (Oryzias melastigma) Salt >8-< 17-day post fertilization NOAEL = 0.1326- 0.1845 mgAI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Interleukin 1 beta mRNA, newly hatched larvae {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (iOryzias melastigma) Salt 6-day post fertilization NOAEL = 0.021- 0.0341 mg AI/L; LOAEL = 0.1326- 0.1845 mgAI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO 8-Oxo-2'-deoxy- guanosine {Hong, 2015, 3350507@@auth or-year} High 134237-51-7 Indian Medaka (Oryzias melastigma) Salt 17-day post fertilization NOAEL = 0.1326- 0.1845 mgAI/L 0, 0.0082-0.0145, 0.0205-0.0341, 0.1326-0.1845 mg/L Renewal, Measured, Solvent: DMSO Growth: Abnormal, Malformation rate; Mortality; Hatching rate {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (iOryzias melastigma) Salt 5-day post fertilization LOAEL = 0.0097- 0.0141 mgAI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0097- 0.0141 mgAI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Heart rate {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (Oryzias melastigma) Salt 8-day post fertilization NOAEL = 0.024- 0.0375 mg AI/L LOAEL = 0.1252- 0.1684 mgAI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Growth, Abnormal; SV- BA length; Tumor necrosis factor mRNA {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization LOAEL = 0.0097- 0.0141 mgAI/L 0,0.0097-0.0141, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Caspase 3 {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (iOryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0097- 0.0141 mgAI/1; LOAEL = 0.1252- 0.1684 mgAI/L 0,0.0097-0.0141, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Caspase 8; Caspase 9 {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (Oryzias melastigma) Salt 8-day post fertilization NOAEL = 0.0097- 0.0141 mgAI/L; LOAEL = 0.0237- 0.0375 mg/AI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO p53 mRNA; Interleukin 1 beta mRNA {Hong, 2015, 3350507@@auth or-year} High 36 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Indian Medaka (Oryzias melastigma) Salt >8-< 17-day post fertilization NOAEL = 0.024- 0.0375 mg AI/L; LOAEL = 0.1252- 0.1684 mg AI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO p53 mRNA, newly hatched larvae; Interleukin 1 beta mRNA, newly hatched larvae; Tumor necrosis factor mRNA, newly hatched larvae {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (Oryzias melastigma) Salt 6-day post fertilization NOAEL = 0.024- 0.0375 mg AI/L; LOAEL = 0.1252- 0.1684 mg AI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO 8-Oxo-2'- deoxyguanosine {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (Oryzias melastigma) Salt 17-day post fertilization NOAEL = 0.024- 0.0375 mg AI/L; LOAEL = 0.1252- 0.1684 mg AI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Growth: Abnormal. Malformation rate {Hong, 2015, 3350507@@auth or-year} High 134237-50-6 Indian Medaka (iOryzias melastigma) Salt 17-day post fertilization NOAEL = 0.1252- 0.1684 mg AI/L 0,0.0097-0.0141, 0.0237-0.0375, 0.1252-0.1684 mg/L Renewal, Measured, Solvent: DMSO Mortality; Hatch rate {Hong, 2015, 3350507@@auth or-year} High 134237-52-8 Zebrafish (.Danio rerio) Fresh 7-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cyplbl mRNA; 7-Ethoxyresorufin O-deethylase; Cytochrome P1A messenger RNA; Aryl hydrocarbon receptor lb mRNA {Du, 2015, 3350537@@auth or-year} High 134237-52-8 Zebrafish (Danio rerio) Fresh 21-day LOAEL = 0.001 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cyplbl mRNA {Du, 2015, 3350537@@auth or-year} High 3350537 134237-52-8 Zebrafish {Danio rerio) Fresh 7-day NOAEL = 0.001 mg AI/L; LOAEL = 0.01 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; Aryl hydrocarbon receptor la mRNA; Aryl hydrocarbon receptor 2 mRNA {Du, 2015, 3350537@@auth or-year} High 37 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Zebrafish (Danio rerio) Fresh 21-day NOAEL = 0.001 mg AI/L; LOAEL = 0.01 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; 7- Ethoxyresorufm O-deethylase; Cytochrome P1A messenger RNA; Aryl hydrocarbon receptor la mRNA; Aryl hydrocarbon receptor lb mRNA; Aryl hydrocarbon receptor 2 mRNA {Du, 2015, 3350537@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 21-day NOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Liver somatic index; Mortality {Du, 2015, 3350537@@auth or-year} High 134237-51-7 Zebrafish (Danio rerio) Fresh 7-day NOAEL = 0.001 mg AI/L; LOAEL = 0.01 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cyplbl mRNA; Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; Aryl hydrocarbon receptor la mRNA; Aryl hydrocarbon receptor 2 mRNA {Du, 2015, 3350537@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 21-day NOAEL = 0.001 mg AI/L; LOAEL = 0.01 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cyplbl mRNA; Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; Cytochrome P1A messenger RNA; Aryl hydrocarbon receptor lb mRNA {Du, 2015, 3350537@@auth or-year} High 38 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Zebrafish (Danio rerio) Fresh 7-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Cytochrome P1A messenger RNA; Aryl hydrocarbon receptor lb mRNA {Du, 2015, 3350537@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 21-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Aryl hydrocarbon receptor 2 mRNA {Du, 2015, 3350537@@auth or-year} High 134237-51-7 Zebrafish (Danio rerio) Fresh 21-day NOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Aryl hydrocarbon receptor la mRNA; Liver somatic index; Mortality {Du, 2015, 3350537@@auth or-year} High 134237-50-6 Zebrafish Fresh 7-day NOAEL = 0.001 mg 0,0.001,0.01,0.1 Renewal, Nominal, Cyplbl mRNA; {Du, 2015, High {Danio rerio) AI/L; LOAEL = 0.01 mg AI/L mg/L Solvent: DMSO Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; Aryl hydrocarbon receptor la mRNA; Aryl hydrocarbon receptor lb mRNA 3350537@@auth or-year} 134237-50-6 Zebrafish Fresh 21-day NOAEL = 0.001 mg 0,0.001,0.01,0.1 Renewal, Nominal, Cyplbl mRNA; {Du, 2015, High {Danio rerio) AI/L; LOAEL = 0.01 mg AI/L mg/L Solvent: DMSO Cytochrome P450, family 1, subfamily C, polypeptide 1 mRNA; Aryl hydrocarbon receptor la mRNA; Aryl hydrocarbon receptor lb mRNA; Aryl hydrocarbon receptor 2 mRNA 3350537@@auth or-year} 39 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Zebrafish (Danio rerio) Fresh 7-day NOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Aryl hydrocarbon receptor 2 mRNA {Du, 2015, 3350537@@auth or-year} High 134237-50-6 Zebrafish (Danio rerio) Fresh 21-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO 7-Ethoxyresorufin O-deethylase; Cytochrome P1A messenger RNA {Du, 2015, 3350537@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 7-day NOAEL = 0.01 mg AI/L; LOAEL = 0.1 mg AI/L 0,0.001,0.01,0.1 mg/L Renewal, Nominal, Solvent: DMSO Cytochrome P1A messenger RNA {Du, 2015, 3350537@@auth or-year} High 134237-50-6 Zebrafish Fresh 21-day NOAEL = 0.1 mg 0,0.001,0.01,0.1 Renewal, Nominal, Liver somatic {Du, 2015, High {Danio rerio) AI/L mg/L Solvent: DMSO index; Mortality 3350537@@auth or-year} 134237-52-8 Zebrafish {Danio rerio) Fresh 7-day NOAEL = 0.02284 mg Al/kg 0.00084, 0.02284 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 1403364 134237-52-8 Zebrafish {Danio rerio) Fresh 14-day NOAEL = 0.02284 mg Al/kg 0.00084, 0.02284 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; 7- Ethoxyresorufm O-deethylase; T4 outer ring deiodinase enzyme activity; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 56-day LOAEL = 0.02284 mg Al/kg 0.00084, 0.02284 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; T4 outer ring deiodinase enzyme activity; Thyroid gland epithelial cell height {Palace, 2010, 1403364@@auth or-year} High 40 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Zebrafish (Danio rerio) Fresh 7-day LOAEL = 0.02284 mg Al/kg 0.00084, 0.02284 mg/kg Food, Measured; lipid- corrected 7-Ethoxyresorufin O-deethylase {Palace, 2010, 1403364@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 56-day NOAEL = 0.02284 mg Al/kg 0.00084, 0.02284 mg/kg Food, Measured; lipid- corrected 7-Ethoxyresorufin O-deethylase; Liver somatic index; Uridine diphosphate glucuronyl transferase, UDP glucuronyl transferase {Palace, 2010, 1403364@@auth or-year} High 134237-52-8 Zebrafish Fresh 168- NOAEL = 0.02284 0.00084, 0.02284 Food, Measured; lipid- Growth: Weight {Palace, 2010, High {Danio rerio) day *(112- day depuration period after 56-day exposure) mg Al/kg mg/kg corrected 1403364@@auth or-year} 134237-51-7 Zebrafish {Danio rerio) Fresh 7-day NOAEL = 0.01184 mg Al/kg 0,0.01184 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 14-day NOAEL = 0.01184 mg Al/kg 0,0.01184 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; 7- Ethoxyresorufm O-deethylase; T4 outer ring deiodinase enzyme activity; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 56-day NOAEL = 0.01184 mg Al/kg 0,0.01184 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 41 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Zebrafish (Danio rerio) Fresh 56-day LOAEL = 0.01184 mg Al/kg 0, 0.01184 mg/kg Food, Measured; lipid- corrected Thyroxine; 7- Ethoxyresorufm O-deelliylase; T4 outer ring deiodinase enzyme activity; Uridine diphosphate glucuronyl transferase, UDP glucuronyl transferase {Palace, 2010, 1403364@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 7-day LOAEL = 0.01184 mg Al/kg 0, 0.01184 mg/kg Food, Measured; lipid- corrected 7-Ethoxyresorufin O-deethylase {Palace, 2010, 1403364@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 168-day* (112-day depuration period after 56-day exposure) NOAEL = 0.01184 mg Al/kg 0,0.01184 mg/kg Food, Measured; lipid- corrected Growth: Weight rate {Palace, 2010, 1403364@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 7-day NOAEL = 0.02914 mg Al/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 14-day NOAEL= 0.02914 mg Al/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroxine; 7- Ethoxyresorufm O-deelliylase; T4 outer ring deiodinase enzyme activity; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 42 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Zebrafish (Danio rerio) Fresh 56-day NOAEL = 0.02914 mgAI/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected Triiodothyronine; Thyroid gland epithelial cell height; Liver somatic index {Palace, 2010, 1403364@@auth or-year} High 134237-50-6 Zebrafish (Danio rerio) Fresh 56-day LOAEL = 0.02914 mgAI/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected Thyroxine; 7- Ethoxyresorufm O-deelliylase; T4 outer ring deiodinase enzyme activity; Uridine diphosphate glucuronyl transferase, UDP glucuronyl transferase {Palace, 2010, 1403364@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 7-day LOAEL = 0.02914 mgAI/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected 7-Ethoxyresorufin O-deethylase {Palace, 2010, 1403364@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 168-day* (112-day depuration period after 56-day exposure) NOAEL= 0.02914 mgAI/kg 0.00047,0.02914 mg/kg Food, Measured; lipid- corrected Growth: Weight {Palace, 2010, 1403364@@auth or-year} High 25637-99-4 Rainbow trout {Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (edible tissue) = 6,531 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 1928244 25637-99-4 Rainbow trout {Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (edible tissue) = 4,650 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout {Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (non-edible tissue) = 20,726 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout {Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (non-edible tissue) = 12,866 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 43 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (whole body) = 13,085 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Steady-State BCF (whole body) = 8,974 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Kinetic BCF (edible tissue) = 14,039 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Kinetic BCF (edible tissue) = 9,826 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Kinetic BCF (non- edible tissue) = 30,242 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (iOncorhynchus mykiss) Fresh 35-day Kinetic BCF (non- edible tissue) = 23,303 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (iOncorhynchus mykiss) Fresh 35-day Kinetic BCF (whole body) = 21,940 0.00018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 35-day Kinetic BCF (whole body) = 16,450 0.0018 mg/L Flow-through, Measured, Solvent: Acetone Residue; Bioconcentration {Wildlife Intl LTD, 2000, 1928244@@auth or-year} High 134237-52-8 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Mortality; Weight; Length; Condition {Palace, 2008, 1409610@@auth or-year} High 1409610 44 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 34 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-52-8 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 36 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery:muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-52-8 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 38 NOAEL = 0.005 mg/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-52-8 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 46 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue; intestine tissue, viscera tissue, liver tissue {Palace, 2008, 1409610@@auth or-year} High 134237-52-8 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 46 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: gallblad der tissue, thyroid tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-52-8 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 34 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Type II iodothyronine deiodinase {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 32 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Mortality, Weight, Length, Condition {Palace, 2008, 1409610@@auth or-year} High 45 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 34 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 36 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 38 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 46 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, intestine tissue, liver tissue {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 38 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 46 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery, gallbladder tissue, thyroid tissue, viscera tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-51-7 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 34 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Type II iodothyronine deiodinase {Palace, 2008, 1409610@@auth or-year} High 46 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 32 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Mortality, Weight, Length, Condition {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 34 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood; Type II iodothyronine deiodinase {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 36 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery:muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (iOncorhynchus mykiss) Fresh > 32-day, measured on day 38 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 46 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: muscle tissue, gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 38 NOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery: gallbladder tissue, thyroid tissue, intestine tissue, viscera tissue, liver tissue, blood {Palace, 2008, 1409610@@auth or-year} High 134237-50-6 Rainbow trout (Oncorhynchus mykiss) Fresh > 32-day, measured on day 46 LOAEL = 0.005 mg Al/kg 0, 0.005 mg/kg Food, Nominal; Solvent: Corn oil Thyroxine; % recovery, blood {Palace, 2008, 1409610@@auth or-year} High 47 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Common sole (.Solea solea) Salt 6-day NOEC = 0.25 mg/L 0, 0,0.025,0.08, 0.25 mg/L Renewal, Nominal; Solvent: DMSO Hatching success {Foekema, 2014, 2343709@@auth or-year} High 2343709 25637-99-4 Common sole {Solea solea) Salt 6-day exposure* followed by 34-day obs. In clean water Internal Effect Concentration (IEC)5o = >12,400 mg/kg lipid weight 2,280 - 12,400 mg/kg lipid weight Renewal, Measured Mortality; Growth: completion of metamorphosis {Foekema, 2014, 2343709@@auth or-year} High 134237-52-8 Zebrafish (Danio rerio) Fresh 42-day NOAEL = 0.04482 mg Al/kg 0, 0.00486, 0.04482 mg/kg dry wt Food, Measured Growth: Weight; % Lipid {Du, 2012, 1927579@@auth or-year} High 1927579 134237-52-8 Zebrafish {Danio rerio) Fresh 42-day NR-ZERO = 0.04482 mg Al/kg 0, 0.00486, 0.04482 mg/kg dry wt Food, Measured Mortality {Du, 2012, 1927579@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 42-day BMF = 7.61 0.0048 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 134237-52-8 Zebrafish {Danio rerio) Fresh 42-day BMF = 7.76 0.04482 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 42-day NOAEL = 0.04748 mg Al/kg 0, 0.00452, 0.04748 mg/kg dry wt Food, Measured Growth: Weight; % Lipid {Du, 2012, 1927579@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 42-day NR-ZERO = 0.04748 mg Al/kg 0, 0.00452, 0.04748 mg/kg dry wt Food, Measured Mortality {Du, 2012, 1927579@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 42-day BMF = 11.63 0.00452 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 134237-51-7 Zebrafish {Danio rerio) Fresh 42-day BMF = 7.34 0.04748 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 42-day NOAEL = 0.04576 mg Al/kg 0, 0.00443, 0.04576 mg/kg dry wt Food, Measured Growth: Weight; % Lipid {Du, 2012, 1927579@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 42-day NR-ZERO = 0.04576 mg Al/kg 0, 0.00443, 0.04576 mg/kg dry wt Food, Measured Mortality {Du, 2012, 1927579@@auth or-year} High 134237-50-6 Zebrafish {Danio rerio) Fresh 42-day BMF = 29.71 0.00443 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 48 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Zebrafish (Danio rerio) Fresh 42-day BMF = 12.33 0.04576 mg/kg dry wt Food, Measured Residue: biomagnification {Du, 2012, 1927579@@auth or-year} High 25637-99-4 Threespine Stickleback (Gasterosteus aculeatus) Salt 30-day NOAEL = 0.0003 mg AI/L 0, 0.00003, 0.0003 mg/L Flow-through, Nominal, Solvent: Acetone DNA methylation {Aniagu, 2008, 1412194@@auth or-year} Low 1412194 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 33-day NOEC = 0.0037 mg AI/L 0, 0, 0.00025, 0.00047, 0.00083, 0.0018, 0.0037 mg/L Flow-through, Measured. Solvent: Acetone Hatching success {Drottar, 2001, 4796184@@auth or-year} This study needs to be reviewed 4796184 25637-99-4 Rainbow trout (Oncorhynchus mykiss) Fresh 61-day NOEC = 0.0037 mg AI/L 0, 0, 0.00025, 0.00047, 0.00083, 0.0018, 0.0037 mg/L Flow-through, Measured. Solvent: Acetone Mortality; Growth: Weight; Growth: Length; Time to Swim-up {Drottar, 2001, 4796184@@auth or-year} 134237-52-8 Common Carp (Cyprinus carpio) Fresh 60-day Kinetic BCF (gill) = 237 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 2343723 134237-52-8 Common Carp (iCyprinus carpio) Fresh 60-day Kinetic BCF (viscera) =584 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (muscle) = 221 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp (Cyprinus carpio) Fresh 60-day Kinetic BCF (skin) = 227 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp (Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (gill) = 950 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (viscera) = 1,730 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (muscle) = 1,220 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-52-8 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (skin) = 1,610 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (gill) = 322 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 49 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Common Carp (Cyprinus carpio) Fresh 60-day Kinetic BCF (viscera) = 642 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp (iCyprinus carpio) Fresh 60-day Kinetic BCF (muscle) = 187 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp (iCyprinus carpio) Fresh 60-day Kinetic BCF (skin) = 204 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp (Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (gill) = 1,290 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp (Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (viscera) = 1,900 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (muscle) = 1,030 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-51-7 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (skin) = 1,440 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (gill) = 8,580 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (viscera) = 11,500 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (muscle) = 5,570 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Kinetic BCF (skin) = 6,400 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (gill) = 34,500 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (viscera) = 34,200 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 134237-50-6 Common Carp {Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (muscle) = 30,700 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 50 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Common Carp (Cyprinus carpio) Fresh 60-day Lipid-Normalized Kinetic BCF (skin) = 45,200 0, 0.001 mg/L Renewal, Measured Residue; Bioconcentration {Zhang, 2014, 2343723@@auth or-year} High 25637-99-4 Starry, European Flounder (Platichthys flesus) Brackish Fresh 78-day NOAEL = 3000 mg/kg lipid diet with 800 mg/kg TOC sediment OR 0 mg/kg lipid diet with 8000 mg/kg TOC sediment Diet (mg/kg lipid)/sediment (mg/kg total organic carbon): 0/0; 0.3/0.08; 3/0.8; 30/8; 300/80; 3000/800; 0/8000 Multiple routes (diet and sediment), Nominal, Solvent: Acetone Thyroxine; Aromatase; 7- Ethoxyresorufm O-deethylase; Triiodothyronine; Benzylresorufm O-deethylase; Pentylresorufin O-deethylase {Kuiper, 2007, 1412802@@auth or-year} High 1412.302 25637-99-4 Starry, European Flounder (.Platichthys flesus) Brackish 78-day NOAEL = 30 mg/kg lipid diet with 8 mg/kg TOC sediment; LOAEL = 300 mg/kg lipid diet with 80 mg/kg TOC sediment Diet (mg/kg lipid)/sediment (mg/kg total organic carbon): 0/0; 0.3/0.08; 3/0.8; 30/8; 300/80; 3000/800; 0/8000 Multiple routes (diet and sediment), Nominal, Solvent: Acetone Residue: a- HBCD concentration in muscle; P-HBCD concentration in muscle {Kuiper, 2007, 1412802@@auth or-year} High 25637-99-4 Starry, European Flounder (.Platichthys flesus) Brackish 78-day LOAEL = 0.3 mg/kg lipid diet with 0.08 mg/kg TOC sediment Diet (mg/kg lipid)/sediment (mg/kg total organic carbon): 0/0; 0.3/0.08; 3/0.8; 30/8; 300/80; 3000/800; 0/8000 Multiple routes (diet and sediment), Nominal, Solvent: Acetone Residue; y-HBCD concentration in muscle {Kuiper, 2007, 1412802@@auth or-year} High 134237-52-8 Rainbow trout (Oncorhynchus mykiss) Fresh 168-day (56-day exposure to treated food then 112 days untreated food) BMF = 7.2 0.0003, 0.02284 mg/kg Food, Measured; Lipid- corrected Residue; biomagnification {Law, 2006, 1443861@@auth or-year} Low 1443861 51 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Water Type Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Rainbow trout Fresh 168-day BMF = 4.3 0.0003,0.01184 Food, Measured; Lipid- Residue; {Law, 2006, Low (Oncorhynchus mykiss) (56-day exposure to treated food then 112 days untreated food) mg/kg corrected biomagnification 1443861@@auth or-year} 134237-50-6 Rainbow trout Fresh 168-day BMF = 9.2 0.0003,0.02914 Food, Measured; Lipid- Residue; {Law, 2006, Low (iOncorhynchus mykiss) (56-day exposure to treated food then 112 days untreated food) mg/kg corrected biomagnification 1443861@@auth or-year} Amphibians 25637-99-4 African clawed frog (Xenopus laevis) Fresh 1-day NOAEL = 6.417 mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 2-day NOAEL = 6.417mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 938764 25637-99-4 African clawed frog (Xenopus laevis) Fresh 3-day NOAEL = 6.417 mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 4-day NOAEL = 6.417 mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 5-day NOAEL = 6.417 mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 6-day NOAEL = 6.417 mg AI/L 0, 0.64, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Developmental: Tail resorption {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 8-day NOAEL = 0.642 mg AI/L 0, 0.64 mg/L Renewal, Nominal, Solvent: DMSO Cell proliferation {Schriks, 2006, 938764@@autho r-year} Unacceptable 25637-99-4 African clawed frog (Xenopus laevis) Fresh 8-day NR-ZERO = 0.642 mg AI/L 0, 0.64 mg/L Renewal, Nominal, Solvent: DMSO Mortality {Schriks, 2006, 938764@@autho r-year} Unacceptable 52 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE 53 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE Table 2. On-topic terrestrial toxicity studies that were evaluated for HBCD CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. Terrestrial Vegetation 134237-52-8 Corn (Zea mays) Hydroponic 3-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 1927583 134237-52-8 Corn (Zea mays) Hydroponic 7-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 12-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 24-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y- H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 54 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Corn (Zea mays) Hydroponic 72-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 96-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 7-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 12-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 72-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 55 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Corn (Zea mays) Hydroponic 96-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots; Growth: Inhibition of seed germination; Growth: Inhibition of root biomass; Growth: Inhibition of shoot biomass; Growth: Root elongation; Growth: Shoot elongation {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 3-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-52-8 Corn (Zea mays) Hydroponic 24-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Histone H2AX mRNA: Relative y-H2AX level in roots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 3-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 56 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Corn (Zea mays) Hydroponic 7-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 12-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 24-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 57 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Corn (Zea mays) Hydroponic 72-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 96-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 3-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-51-7 Corn (Zea mays) Hydroponic 72-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots {Wu, 2012, 1927583@@au thor-year} High 58 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Corn (Zea mays) Hydroponic 96-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots; Growth: Inhibition of seed germination; Growth: Inhibition of root biomass; Growth: Inhibition of shoot biomass; Growth: Root elongation; Growth: Shoot elongation {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 3-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 7-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 59 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Corn (Zea mays) Hydroponic 12-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 24-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 72-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots, Radical relative intensity in shoots; Histone H2AX mRNA: Relative y-H2AX level in roots {Wu, 2012, 1927583@@au thor-year} High 60 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Corn (Zea mays) Hydroponic 96-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in roots; Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 96-hour LOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Reactive oxygen species: Radical relative intensity in shoots; Growth: Inhibition of seed germination; Growth: Inhibition of root biomass; Growth: Inhibition of shoot biomass; Growth: Root elongation; Growth: Shoot elongation {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 3-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Histone H2AX mRNA: Relative y-H2AX level in roots, Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 134237-50-6 Corn (Zea mays) Hydroponic 72-hour NOAEL = 0.002 mg/L 0, 0.002 mg/L Hydroponic solution application, Nominal Histone H2AX mRNA: Relative y-H2AX level in shoots {Wu, 2012, 1927583@@au thor-year} High 25637-99-4 Corn (Zea mays) Filter paper 4-day LOAEL = 0.002 mg/L 0, 0.002,0.005, 0.01,0.02,0.05 mg/L Renewal, Nominal, Solvent: Methanol Growth: Root biomass; Growth: Root length; Growth: Shoot biomass; Germination {Wu, 2016, 3350472@@au thor-year} High 3350472 61 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 Corn (Zea mays) Filter paper 4-day NOAEL = 0.002 mg/L; LOAEL = 0.005 mg/L 0, 0.002,0.005, 0.01,0.02,0.05 mg/L Renewal, Nominal, Solvent: Methanol Growth: Shoot length; Histone H2AX mRNA: Root {Wu, 2016, 3350472@@au thor-year} High 25637-99-4 Corn (Zea mays) Filter paper 4-day NOAEL = 0.005 mg/L; LOAEL = 0.01 mg/L 0, 0.002,0.005, 0.01,0.02,0.05 mg/L Renewal, Nominal, Solvent: Methanol Histone H2AX mRNA: Shoot {Wu, 2016, 3350472@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (root) =0.550 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber, Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 3350492 134237-52-8 Bread Wheat (.Triticum aestivum) Natural soil 1-week BCF (stem) = 0.100 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (leal) = 0.157 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (root) = 0.961 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (stem) = 0.203 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (leaf) = 0.259 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 62 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (root) = 1.27 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber, Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (stem) = 0.284 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (.Triticum aestivum) Natural soil 3-week BCF (leaf) = 0.473 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (root) = 1.99 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (.Triticum aestivum) Natural soil 4-week BCF (stem) = 0.472 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (leaf) = 0.755 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (root) = 1.10 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (stem) = 0.231 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 63 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (leaf) = 0.134 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (root) = 1.36 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (.Triticum aestivum) Natural soil 2-week BCF (stem) = 0.315 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (leaf) = 0.175 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (.Triticum aestivum) Natural soil 3-week BCF (root) = 2.07 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber, Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (stem) = 0.514 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (leaf) = 0.335 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (root) = 3.08 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 64 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (stem) = 0.842 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (leaf) = 0.604 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (.Triticum aestivum) Natural soil 1-week BCF (root) = 1.28 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 1-week BCF (stem) = 0.286 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (.Triticum aestivum) Natural soil 1-week BCF (leaf) = 0.141 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (root) = 1.63 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (stem) = 0.405 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 2-week BCF (leaf) = 0.225 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 65 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (root) = 2.13 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 3-week BCF (stem) = 0.606 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (.Triticum aestivum) Natural soil 3-week BCF (leaf) = 0.337 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (root) = 3.21 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (.Triticum aestivum) Natural soil 4-week BCF (stem) = 0.880 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 4-week BCF (leaf) = 0.663 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Bioconcentration {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 1-week TF = 0.177 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 2-week TF = 0.206 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber, Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 66 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 3-week TF = 0.203 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-52-8 Bread Wheat (Triticum aestivum) Natural soil 4-week TF = 0.216 0, 0.0628 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (.Triticum aestivum) Natural soil 1-week TF = 0.202 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber, Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 2-week TF = 0.224 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (.Triticum aestivum) Natural soil 3-week TF = 0.242 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-51-7 Bread Wheat (Triticum aestivum) Natural soil 4-week TF = 0.264 0, 0.0908 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 1-week TF = 0.218 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 2-week TF = 0.244 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 67 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 3-week TF = 0.280 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High 134237-50-6 Bread Wheat (Triticum aestivum) Natural soil 4-week TF = 0.269 0, 0.0984 mg/kg dry soil Multiple routes within environmental exposure chamber Measured, Solvent: Methylene chloride Residue; Translocation factor (TF: [stem]/ [root]) {Zhu, 2016, 3350492@@au thor-year} High Terrestrial Invertebrates 3194-55-6 Earthworm (Eisenia fetida) Artificial soil 0-4-day NOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Growth: rate {Shi, 2015, 2965902@@au thor-year} High 2965902 3194-55-6 Earthworm (Eisenia fetida) Artificial soil 4-7-day NOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Growth: rate {Shi, 2015, 2965902@@au thor-year} High 3194-55-6 Earthworm (.Eisenia fetida) Artificial soil 7-10-day NOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Growth: rate {Shi, 2015, 2965902@@au thor-year} High 3194-55-6 Earthworm (.Eisenia fetida) Artificial soil 10-14-day NOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Growth: rate {Shi, 2015, 2965902@@au thor-year} High 3194-55-6 Earthworm (Eisenia fetida) Artificial soil 14-day NOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Growth: rate; Catalase mRNA {Shi, 2015, 2965902@@au thor-year} High 3194-55-6 Earthworm (Eisenia fetida) Artificial soil 14-day NOAEL = 200 mg Al/kg; LOAEL = 400 mg Al/kg 0, 0, 50,100, 200, 400 mg/kg dry soil Static, Nominal, Solvent: Acetone Superoxide dismutase mRNA; HSP70 mRNA {Shi, 2015, 2965902@@au thor-year} High 134237-52-8 Earthworm (Eisenia fetida) Natural soil 21-day BAF = 3.77 0, 0.172 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low 3350510 134237-52-8 Earthworm (Metaphire guillelmi) Natural soil 21-day BAF = 1.16 0, 0.172 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low 134237-51-7 Earthworm (Eisenia fetida) Natural soil 21-day BAF = 2.28 0, 0.156 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low 134237-51-7 Earthworm (Metaphire guillelmi) Natural soil 21-day BAF = 2.81 0, 0.156 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low 68 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Earthworm (Eisenia fetida) Natural soil 21-day BAF = 21.8 0, 0.186 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low 134237-50-6 Earthworm (Metaphire guillelmi) Natural soil 21-day BAF = 6.21 0, 0.186 mg/g dry soil Static, Measured, Solvent: Unspecified Residue; Bioaccumulation {Li, 2016, 3350510@@au thor-year} Low Terrestrial Vertebrates 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 0.06 mg/L; LOAEL = 0.6 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Cytochrome P450 2H1 mRNA; UGT- 1A9; Fatty acid- binding protein 10- A, liver basic mRNA; Cyto- chrome P450 3A37 mRNA {Crump, 2008, 14081 ll@@au thor-year} High 1408111 134237-50-6 Domestic chicken ('Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 0.006 mg/L; LOAEL = 0.06 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Cytochrome P450 2H1 mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 0.06 mg/L; LOAEL = 0.6 mg/L 0, 00.006, 0.06, 0.6, 1.9,6.4 mg/L In vitro, Nominal, Solvent: DMSO UGT- 1A9; Fatty acid-binding protein 10-A, liver basic mRNA; Cyto- chrome P450 3A37 mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Xenobiotic-sensing orphan nuclear receptor (CXR) mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 1.9 mg/L; LOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Transthyretin (pre- albumin, amyloid- osis type I) mRNA; Thyroid hormone responsive spot 14 alpha mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Trans- thyretin (pre- albumin, amyloid- osis type I) mRNA {Crump, 2008, 14081 ll@@au thor-year} High 69 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-50-6 Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 1.9 mg/L; LOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Thyroid hormone responsive spot 14 alpha mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 HBCD- Technical Mixture Domestic chicken ('Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 0.06 mg/L; LOAEL = 0.6 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Thyroid hormone responsive spot 14 alpha mRNA; Cyto- chrome P450 2H1 mRNA; Cyto- chrome P450 3A37 mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 HBCD- Technical Mixture Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 0.06 mg/L; LOAEL = 0.6 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Thyroid hormone responsive spot 14 alpha mRNA; Fatty acid-binding protein 10-A, liver basic mRNA; Cyto- chrome P450 2H1 mRNA; Cyto- chrome P450 3A37 mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 HBCD- Technical Mixture Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO UGT- 1A9 {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 HBCD- Technical Mixture Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 36-hour NOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO UGT- 1A9; Trans- thyretin (pre- albumin, amyloid- osis type I) mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-50-6 HBCD- Technical Mixture Domestic chicken (Gallus domesticus) Culture of embryonic hepatocytes 24-hour NOAEL = 1.9 mg/L; LOAEL = 6.4 mg/L 0, 0, 0.006, 0.06,0.6, 1.9, 6.4 mg/L In vitro, Nominal, Solvent: DMSO Transthyretin (pre- albumin, amyloid- osis type I) mRNA; Fatty acid-binding protein 10-A, liver basic mRNA {Crump, 2008, 14081 ll@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 1-day NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 1927629 70 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Domestic chicken (Gallus domesticus) Diet 4-day NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 8-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 11-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 16-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (iGallus domesticus) Diet 21-day, 1 day depuration LOAEL = 0.001 mg A/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day, 3 days depuration LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day, 8 days depuration LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 21-day, 18 days depuration LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Abdominal fat {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 1-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 71 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Domestic chicken (Gallus domesticus) Diet 4-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 8-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 11-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 16-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day LOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (iGallus domesticus) Diet 21-day, 1 day depuration NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day, 3 days depuration NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day, 8 days depuration NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 21-day, 18 days depuration NOAEL = 0.001 mg Al/kg food 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioaccumulation in Liver {Fournier, 2012, 1927629@@au thor-year} High 134237-52-8 Domestic chicken ('Gallus domesticus) Diet 21-day BCF (egg yolk) = 0.4 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioconcentration {Fournier, 2012, 1927629@@au thor-year} High 72 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 134237-52-8 Domestic chicken (Gallus domesticus) Diet 21-day BCF (liver) = 0.3 0, 0.001 mg/kg food Food, Nominal, Solvent: Rapeseed oil Residue: Bioconcentration {Fournier, 2012, 1927629@@au thor-year} High 25637-99-4 American Kestrel (Falco sparverius) Diet 4 weeks prior to pairing, continuing through incubation until 2 days prior to hatch LOAEL (males and females) = 0.51 mg Al/kg food 0, 0.51 mg/kg- bw/day Food, Nominal, Solvent: Safflower oil Decreased activity, general: measured during courtship, measured at 5 days after pairing {Marteinson, 2012, 1927590@@au thor-year} High 1927590 25637-99-4 American Kestrel (Falco sparverius) Diet 4 weeks prior to pairing, continuing through incubation until 2 days prior to hatch LOAEL (males) = 0.51 mg/kg-bw/day 0, 0.51 mg/kg- bw/day Food, Nominal, Solvent: Safflower oil Decreased activity, general and flying measured during brood-rearing; Courtship behavior: Reduced vocalizations, effect observed throughout courtship; Pair- bonding nesting behavior: Reduced Displays; Care of young, nest attentiveness: Reduced frequency of entry into nest- box and Decreased food retrieval {Marteinson, 2012, 1927590@@au thor-year} High 73 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 American Diet 4 weeks LOAEL (females) 0, 0.51 mg/kg- Food, Nominal, Courtship behavior: {Marteinson, High Kestrel (Falco prior to = 0.51 mg/kg- bw/day Solvent: Safflower oil Reduced 2012, sparverius) pairing, continuing through incubation until 2 days prior to hatch bw/day vocalizations, effect observed only at 5 days after pairing, Reduced courtship displays, effect observed at 5 days after pairing; Pair- bonding nesting behavior: Increased displays; Care of young, nest attentiveness: Increased frequency of entry into nest- box and Increased food retrieval 1927590@@au thor-year} 25637-99-4 American Diet 4 weeks LOAEL = 0.51 0, 0.51 mg/kg- Food, Nominal, Reduced mass of {Marteinson, High Kestrel {Falco prior to mg/kg-bw/day bw/day Solvent: Safflower oil first egg; Care of 2012, sparverius) pairing, continuing through incubation until 2 days prior to hatch young, nest attentiveness: Incubation nest temperature 1927590@@au thor-year} 74 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. 25637-99-4 American Kestrel (Falco sparverius) Diet 75 days: 3 weeks prior to pairing, continuing through incubation until first chick hatched LOAEL = 0.51 mg Al/kg food 0, 0.51 mg/kg- bw/day Food, Nominal, Solvent: Safflower oil Residue: Accumulation in Eggs; Reproductive: Decreased time to first egg laid after pairing, decreased clutch size, decreased egg volume per clutch, decreased egg volume per pair, decreased egg mass per clutch, Decreased egg mass at mid-incubation, Increased egg weight loss at mid- incubation {Fernie, 2011, 1401837@@au thor-year} High 1401837 25637-99-4 American Kestrel {Falco sparverius) Diet 75 days: 3 weeks prior to pairing, continuing through incubation until first chick hatched NOAEL = 0.51 mg Al/kg food 0, 0.51 mg/kg- bw/day Food, Nominal, Solvent: Safflower oil Lipid concentration in eggs; Repro- ductive: Egg shell thickness, Overall hatching success (number of hatchlings), Overall reproductive success (number of fledglings per brood/number of eggs per female), Fertility (percentage fertile eggs laid per female), Elatching success (percentage hatchlings of fertile eggs per female), Fledgling success (percentage fledglings of hatchlings per female) {Fernie, 2011, 1401837@@au thor-year} High 75 ------- PEER REVIEW DRAFT- DO NOT CITE OR QUOTE CAS RN Test Species Media Duration End- point Conc(s) Test Analysis Effect(s) References Data Quality Ratings HERO ID. American kestrel (F. sparverius) Diet exposed 21-day LOAEL 3.27 ng/g ww (low exposure) Food, Nominal, Solvent: Safflower oil Reproduction {Marteinson, 2010, 1927669@@au thor-year} High 1927669 American kestrel (F. sparverius) Diet exposed 21-day LOAEL 15.61 ng/g ww (high exposure) Food, Nominal, Solvent: Safflower oil Reproduction {Marteinson, 2010, 1927669@@au thor-year} High American kestrel (F. sparverius) Diet exposed 21-day LOAEL 0.51 mg/kg-day HBCD dissolved in safflower oil was injected into the brains of dead cockerels daily; kestrels fed from the cockerels ad libitum and received a dose of approximately 0.51 mg/kg-day. Increased testes weight in unpaired males {Marteinson, 2011, 1927624@@au thor-year} High 1927624 76 ------- |