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The quarterly update of U.S. EPA's Homeland Security
Technology Testing & Evaluation Program (TTEP)

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EPA's Portable Pipe Loop to Enhance Water Security
Technology Evaluations

For almost 2 years, EPA has been in the process of designing
and fabricating a portable, recirculating pipe loop that can be
used to conduct a variety of research projects using biological
and chemical agents. In late January, fabrication of EPA's
portable pipe loop (PPL) was completed and in February it
was delivered to Battelle. As shown in the pictures below,
the pipe loop consists of two castor-mounted racks fabricated
almost entirely from 316L stainless steel. The equipment
rack contains a 20-gallon mixing tank, a 7.5 horsepower
centrifugal pump with a variable frequency drive capable of
providing flow rates ranging from 0.5-5.5 feet per second,
a flow meter, a peristaltic pump to be used for contaminant
injection, and a capture tank for single-pass experiments.

The piping rack contains approximately 95 feet of three
inch diameter stainless steel pipe. In addition, this rack is
equipped with eight sampling or instrument ports, optical
glasses for visual inspection of the water flow, removable
sections of pipe, and valve configurations that can allow
the use of some or all sections of the pipe. The PPL will be
used on an upcoming TTEP test of multi-parameter water
monitors. This evaluation will focus on the response of
water quality parameters to injections of toxic industrial
chemicals, biological agents, and chemical agents. If you
have questions, contact Dr. Jeff Adams (adams.jeff@epa.gov
or 513-569-7835) or Dr. Ryan James (jamesr||battelle.org or
614-424-7954).

Welcome to TTEP

The U.S. Environmental Protection Agency (EPA) is actively participating
in the national homeland security effort by ensuring the protection of the
nation's drinking water systems and the safety of the public in buildings
and other structures. EPA's Office of Research and Development's National
Homeland Security Research Center (NHSRC) has established the Technol-
ogy Testing and Evaluation Program (TTEP) to assist this effort, TTEP is
conducting third-party performance evaluations of commercially available
homeland security technologies, incorporating stakeholder guidance and
a high degree of quality assurance (QA) oversight, Questions about TTEP
should be directed to Mr. Eric Koglin (koglin.eric@epa.gov or 702-798-2332).

TTEP Water Security Stakeholder Meeting

On March 15, 2007, EPA's TTEP Water Security
stakeholder committee met at Battelle in Columbus,
OH. The stakeholders heard updates and added
technical insight pertaining to the evaluations of
ultrafiltration cartridges, multi-parameter water
monitors, and the expeditionary unit water purification
system. The committee also took part in a tour that
showcased the operation of the newly completed
EPA portable pipe loop. Discussions also prioritized
technology category areas for future evaluation.


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Comparison of Decontamination Methods for Bacillus Anthracis

In addition to evaluating methods and equipment for
decontaminating indoor environments following an
intentional release of a biological agent, EPA also evaluates
test methods for use in registration of pesticides, including
sporicidal products for the inactivation of Bacillus anthracis
spores - the biological agent responsible for anthrax.

To efficiently achieve related objectives, the EPA National
Homeland Security Research Center and the EPA Office of
Prevention, Pesticides and Toxic Substances (OPPTS) are
collaborating under TTEP to perform parallel efficacy testing
of fumigation and liquid decontamination technologies for
Bacillus anthracis Ames by using three different approaches
or standard methods.

The methods include:

•	AOAC Official Method 966.04, Sporicidal Activity of
Disinfectants: Alternative Method II

•	Determination of sporicidal efficacy using the quantitative
three step method as modified by OPPTS

•	Methods developed by Battelle, under the direction of
Dr. James Rogers, and used extensively under TTEP for
determining efficacy of decontamination technologies for
the inactivation of B. anthracis on building materials.

The investigation will answer the questions:

•	What is the efficacy of decontamination technologies
against spores of B. anthracis Ames as determined by the
three methods?

•	For a given decontamination technology, do the three test
methods for determining efficacy yield the same outcome?

•	For a given decontamination technology, is qualitative
analysis of biological indicators consistent with the efficacy
results from the three test methods?

The efficacy of various liquid and fumigant technologies
against spores of B. anthracis Ames and two surrogates (B.
subtilis and B. atrophaeus) will be evaluated at three different
contact times at a specified concentration, temperature, and
(for fumigants) relative humidity. Spores will be applied to
test coupons/carriers specified in the respective test methods.
Spore viability after a given treatment will be determined as
specified in the respective method.

For further information on TTEP decontamination methods
testing, contact

Dr. Shawn Ryan (ryan.shawn@epa.gov or 919-541-0699).

Testing of Screening Technologies for Use in EPA's All Hazards Receipt Facilities

Examples of Screening Technologies Tested

Testing was recently
completed under TTEP on
25 technologies that could
be used to screen samples
in EPA's All Hazards
Receipt Facilities (AHRF).

The EPA, U.S. Department
of Homeland Security,
and U.S. Department
of Defense have

established the AHRF for prescreening unknown and
potentially hazardous samples collected during suspected
terrorist events. The AHRF are intended to screen incoming
samples for chemical, explosive, and radiological hazards,
to protect laboratory workers from injury and facilities
from contamination, and to ensure the integrity of collected
samples. Screening technologies for use in the AHRF must
be rapid and qualitative, and preferably of relatively low
cost, but must provide accurate identification of hazardous
samples.

The screening technologies tested ranged from simple
test papers, kits, and color indicating tubes to hand-held
electronic detectors based on photoiomzation detection,
electrochemical sensors, ion mobility spectrometry, and
flame spectrophotometry (FSP). Testing involved challenges
with toxic industrial chemicals (TICs) (hydrogen cyanide,
cyanogen chloride, phosgene, arsine, hydrogen sulfide,
hydrogen peroxide, chlorine, and fluoride) and chemical

warfare agents (CWAs)
(sarin (GB), sulfur
mustard (HD), and VX)
in air, water, and/or on
test surfaces. Testing
was conducted with TIC
or CWA concentrations
that would be dangerous
to laboratory personnel,
and over a range of
temperature and relative humidity, and with interferences
present along with the TIC or CWA. For each screening
technology, the analysis time, operational characteristics,
and cost per sample were also evaluated.

Several of the tested technologies were able to accurately
detect the TICs and CWAs in air, though no single
technology was applicable to all the TICs and CWAs.
Few of the screening technologies were able to detect the
CWAs in water at the target concentrations used, but all
of the technologies tested for detection of VX on surfaces
provided accurate indications. The FSP detector tested was
notable in its relatively broad applicability to both TICs and
CWAs, and to air, water, and surface samples.

The final reports on the AHRF TIC and CWA testing will
be submitted to EPA in April. If you have questions about
AHRF testing, contact Mr. Eric Koglin (kogliii.crictf
epa.gov or 702-798-2332) or Dr. Thomas Kelly (kellyt@
battelle.org or 614-424-3495).


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