SEPA
REGION 10 DIVE TEAM
www.epa.gov/region10/dive
EPA Region 10 Dive Team
Diver Assisted Site Assessment at the Columbia River Drum Site; Portland, OR, April 2007
What: The Superfund Environmental Cleanup Office/Site Assessment Unit requested assistance from
the EPA Region 10 Dive Team to collect samples for characterization of a drum dump site in the
Columbia River.
Why: Diver survey objectives were to: 1) map out the area of drums on the river bottom and 2) collect
core samples in and around the drums to determine their impact on the River relative to background
chemical concentrations.
Where: Columbia River, south channel between Lemon Island and Marine Drive (near the Portland
Airport).
When: Dive surveys were conducted April 24-26, 2007.
How: Due to river currents, divers were tethered and in constant communication with dive tenders.
Divers swept an 'arc' search pattern behind the boat up to 50 meters downstream, and worked their way
back to the dive platform. Divers took approximately 20 core samples as they encountered drums on the
bottom.
Results: Divers found that the river bottom was covered with debris, likely rolled into the river off
Marine Drive. More than two dozen drums/drum parts were encountered, all in an advanced state of
deterioration. Many drums had holes in them, and appeared to be filled with sand and silt. Sample
results may be found in the site investigation report - December 7, 2007 below.
Contact: Rob Pedersen (206) 553-1646, Pedersen.rob@epa.gov
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Photos:
The diver is under constant tether tension to maintain their position in the water; for example during
searching or taking a sample.
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Aerial photo of drum field.
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Diver preparing to enter the water with core tubes and caps in a 'goody bag'
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Divemaster Sean Sheldrake dons diver Rob Pedersen's AGA full face mask in preparation for drum
sampling.
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Tender/standby diver Tim Siwiec pulls the diver back towards the boat to continue the search pattern.
Return to EPA Region 10 Dive Team homepage.
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tX< TechLaw
Quality 6 IuItgrlIf
December 7, 2007
TO-002-06-07-0006-DCN120
Joanne LaBaw, Task Monitor
United States Environmental Protection Agency
1200 Sixth Avenue, Suite 900- M/S ECL 112
Seattle, WA 98101
Reference: Contract No. EP-S7-06-03
Dear Ms. LaBaw:
Please find enclosed the Final Drums-NE Marine Drive Site Inspection Report. Revision 3 (SI
Report) located in Portland. Oregon. This revised version of the report incorporates the
comments provided by EPA dated December 4, 2007. An electronic version of this deliverable,
formatted in Adobe Acrobat for Windows, was uploaded to the START Final Deliverables folder
on the United States Environmental Protection Agency (EPA) Region 10 FTP site. The SI
Report has been named according to the standard operating guidance (SOG).
If you have any questions or comments, please contact me at (770) 331-8761, the Project
Manager, Lesa Nelson, at (360) 871-8777, or the Site Assessment Group Leader, Alexis Ande, at
(360) 443-6575.
Sir ~
William R. (Ray) Doyle /
START-3 Program Manager
TechLaw. Inc.
Enclosure
cc: Sharon Nickels, EPA Project Officer, Seattle, WA
Elizabeth Burris, Central Files Administrator, TechLaw, Wheeling, WV
Alexis Ande, Site Assessment Group Leader, TechLaw, Port Orchard. WA
Lesa Nelson, Project Manager, TechLaw. Port Orchard, WA
Technical Direction Document No. 06-07-0006
Drums-NE Marine Drive Site
Final Site Inspection Report, Revision 3
Response to Comments Letter
ATLANTA . BOSTON . CHICAGO • DALLAS • DENVER • NEW YORK • OVERLAND PARK • PHILADELPHIA • SACRAMENTO . SAN FRANCISCO • SEATTLE • WASHINGTON, DC
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7411 Beach Drive East
Port Orchard, WA 98366
(360) 871-8750
Quality & Integrity
(360) 871-8763 FAX
wvvw.techlawinc.com
MEMORANDUM
TO-002-06-07-0006-DC N i 20
To:
From:
Joanne LaBaw, Task Monitor, EPA, Seattle, WA
William R. Doyle, START-3 Program Manager. TechLaw. Inc., Port Orchard. WA
Vl£Q>
Subject:
Site Recommendations Memorandum
Drums-NE Marine Drive
Site Inspection
Portland, Multnomah County. Oregon
Reference: Contract No.EP-S7-06-03
Technical Direction Document No. 06-07-0006
This recommendation memorandum has been developed for the Drums-NE Marine Drive Site (Site),
located in Portland, Multnomah County, Oregon as part of Site Inspection (SI). The Site consists of
contaminated sediment located beneath and within deteriorating drums and other debris found in the
Columbia River, in an area northeast of Portland International Airport and south of the Government
Island Complex.
Results of the SI documented the presence of heavy metals and semi-volatiles in the sediments, which
have been identified as the source. The area in and around the Site constitutes the habitat for Federally-
designated, protected or endangered species, including various anadromous fishes, fish-eating birds of
prey, and amphibians.
Further evaluation of the Site under CERCLA is recommended.
Please contact Alexis Ande, the Site Assessment Group Leader, at (360) 443-6575, or Lesa Nelson, the
TechLaw Project Manager, at (360) 871-8777, if you have any questions or comments regarding this
memorandum.
Enclosure
cc: Sharon Nickels, EPA Project Officer, Seattle, WA
Elizabeth Burris, Central Files Administrator, TechLaw, Wheeling, WV
Alexis Ande, Site Assessment Group Leader, TechLaw, Port Orchard. WA
Lesa Nelson, Project Manager, TechLaw. Port Orchard, WA.
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7411 Beach Drive East
Port Orchard, WA 98366
(360) 871-8750
(360) 871-8763 FAX
Quality 6 Integrity
www.techlawiiic.com
MEMORANDUM
TO-002-06-07-0006-DCN120
To:
Joanne LaBaw, Task Monitor, EPA, Seattle, WA
From:
William R. Doyle, START-3 Program Manager, TechLaw, Inc., Port Orchard, WA
Subject: Hazard Ranking System Score
Drums-NE Marine Drive
Portland, Multnomah County, Oregon
Reference: Contract No.EP-S7-06-03
Technical Direction Document No. 06-07-0006
A Hazard Ranking System (HRS) score of 50 was derived for the Drums-NE Marine Drive site
(Site) as part of a Site Investigation (SI). The Site is located Portland, Multnomah County,
Oregon, along the southern shoreline and within the Columbia River. The Site was reported to
Oregon Department of Environmental Quality (ODEQ) on September 28, 2005, by a city work
crew and is currently inactive. The Sherriff s deputies on-scene estimated that there were 400 to
500 rusty, 55-gallon drums, with no containment structures, located on the river bottom (ODEQ
2005). During the SI, approximately 32 drums in various states of disintegration and disrepair
were located in the Columbia River along the southern shoreline. The Site score is based on the
SI and, when necessary, professional assumptions.
The objective of this SI was to assess the Site's impact on the surface water. The groundwater
migration pathway, air migration pathway, and soil exposure pathway were not evaluated. The
HRS scoresheets, which were generated using QuickScore version 2.3 software, are attached.
The following information and assumptions were used to derive the score. The results in the SI
whose values were marked with a J were not adjusted.
Source:
Contaminated Sediment
Contaminated sediment located beneath the deteriorating drums and within the deteriorating
drums is considered to be the source at the Site. The drums themselves were not considered to be
a source because it was not possible to determine if they contained hazardous materials at the
time they were disposed of into the Columbia River due to their deteriorated condition. In
addition, the sampling results indicated that the levels of contaminants found in sediment
samples collected from the inside the drums were not higher than those found in the surrounding
sediments. For the purposes of this report, the sediment within the drums is assumed to have
been deposited by natural siltation. All samples collected from within the drums are also
considered part of the contaminated sediment source.
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Ms. Joanne LaBaw
December 7, 2007
Page 2
During the SI field event, seven samples were collected from within seven drums and seventeen
sediment samples were collected within the immediate vicinity of the drums. All of these
samples are considered part of the contaminated sediment source area. Of the sediments
collected from within the drums, the grain size analysis revealed that one of the seven drum
samples consisted of coarse sand/small gravel sediment and six of the seven drums samples
consisted of clay/silt sediments. Of the seventeen samples collected from the vicinity of the
drums, six consisted of coarse sand/small gravel sediments, and the remaining eleven samples
consisted of clay/silt sediments.
As the exact area of contaminated sediment is not known, the area of contaminated sediment is
assumed to be greater than (>) 0, resulting in an HWQ of 10. As there is no containment
structures associated with the contaminated sediment along the river bottom, the containment
value for the surface water pathway is 10.
Surface Water Migration Pathway:
An observed release to the surface water pathway was documented based on both direct
observation and chemical analysis. The source (contaminated sediment) is located
directly on the bottom of the Columbia River and therefore constitutes an observed
release by direct observation. In addition, sediment samples collected from within and in
the immediate vicinity of the drums contained elevated concentrations of contaminants
including barium, beryllium, cadmium, copper, mercury, silver, selenium, zinc,
acetophenone, bis (2-ethylhexyl) phthalate, and 4-methylphenol.
There are no drinking water intakes along the surface water pathway; therefore, there is
no actual contamination of a drinking water intake. In addition, there is no potential to
contaminate a drinking water supply within the Target Distance Limit (TDL). The
Columbia River is a major water recreation area, so a resource value of 5 was assigned in
the Drinking Water Threat portion of the surface water pathway.
For the Human Food Chain portion of the surface water pathway, actual contamination of
a fishery was documented by both direct observation and chemical analysis. The source
(contaminated sediment) is located in the surface water pathway (Columbia River), and is
presently in direct contact with the surface water. In addition, elevated concentrations of
mercury were detected in 10 sediment samples collected from within or in the immediate
vicinity of the drums. The concentration of mercury in these samples ranged from 0.021
to 0.039 J mg/kg. A toxicity/mobility factor used was 10,000 based on mercury as the
contaminant of concern.
The fishery and the Site are both located in the Columbia River. Therefore, actual
contamination of a fishery has occurred. Anadromous salmon, Steelhead Trout, and
Cutthroat Trout use the Columbia River as a migratory route between upstream spawning
areas and the Pacific Ocean (Fishman 2002). The area where the Site is located is
managed as a recreational and commercial fishery.
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Ms. Joanne LaBaw
December 7, 2007
Page 3
As mercury has a Bioaccumulation Potential factor value of 50,000 and the sampling
results document an actual contamination of a fishery, a Food Chain Individual (FCI)
score of 45 for a Level II fishery population was assigned.
To determine the Human Food Chain Population factor value, the total weight of fish
obtained from the area of the site was estimated. The lower Columbia River is 146 miles
long from the Bonneville Dam to the Pacific Ocean. In 2004, 43,418 Chinook Salmon;
I,335 Coho Salmon; 10,166 Steelhead Trout; 22 Cutthroat Trout; 27,525 White Sturgeon;
and 29 Green Sturgeon were caught during recreational fishing trips. According to local
guides, salmon range in weight from 10 to 50 pounds and market salmon average 20
pounds. Therefore, it was conservatively assumed that each fish kept weighed 20
pounds, resulting in a total of 1,649,900 pounds of fish obtained from the Lower
Columbia River at an average of 11,300 fish per mile. For the Commercial Gillnet
Fisheries for Zone 4, approximately 41 river miles, 74,114 pounds of Chinook Salmon;
II,937 pounds of Coho Salmon; 8,025 pounds of White Sturgeon; and 14 pounds of Shad
were caught. The total weight of fish caught for commercial uses in Commercial
Fisheries Zone 4 is 96,090 pounds, at an average of 2,344 pounds of fish per mile. Only
a portion of the fishery is subject to actual contamination from the source. As the Site is
not an entire mile, it was assumed that between 100 and 10,000 pounds of fish were
subject to actual Level II contamination from the Site, resulting in a Human Food Chain
Population factor value of 3.
The remainder of the TDL is subject to potential contamination. However, due to the
presence of Level II contamination and the low score for potential contamination of a
fishery, the Human Food Chain Population factor value for potential contamination of a
fishery was not calculated.
Evidence of evolutionary significant units (ESUs), federally endangered species, and
threatened species are located within the Site boundaries. An ESU is a distinctive group
of Pacific Salmon or Steelhead. NOAA Fisheries considers an ESU a "species" under the
Endangered Species Act. Anadromous salmon, Steelhead Trout, and Cutthroat Trout use
the Columbia River as a migratory route between upstream spawning areas and the
Pacific Ocean. The following ESUs are federally threatened and migrate upstream past
the Site: four ESUs of Chinook Salmon, one ESU of Columbia River Chum Salmon, one
ESU of Lower Columbia River/Southwest Washington Coho Salmon, and 4 ESUs of
Steelhead Trout. The Snake River Sockeye Salmon, a federally endangered species,
migrates through the area of the Site. The Southwest Washington/Lower Columbia River
Coastal Cutthroat Trout ESU is proposed for federal listing as a threatened species and is
found in the Columbia River in the Government Island Complex vicinity. Another federal
species of concern and a state sensitive species of undetermined status is the Northern
Red-Legged Frog. This species is found in the wetlands and slow moving streams on the
Government Island Complex. A pair of Bald Eagles, formerly a federal and state
threatened species, has a nest on Government Island and catch food in the Columbia
River. The Purple Martin, a state sensitive species, forages for insects over the Columbia
River in the Government Island Complex vicinity.
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Ms. Joanne LaBaw
December 7, 2007
Page 4
For the Sensitive Environment portion of the surface water pathway, actual
contamination of the above listed sensitive environments was documented by both direct
observation and chemical analysis. The source (contaminated sediment) is located in the
surface water pathway (Columbia River), and is presently in direct contact with the
surface water. In addition, elevated concentrations of mercury were detected in 10
sediment samples collected from within or in the immediate vicinity of the drums. The
concentration of mercury in these samples ranged from 0.021 J to 0.039 J mg/kg. A
toxicity/mobility factor used was 10,000 based on mercury as the contaminant of
concern. In addition to mercury, cadmium and silver are also present in elevated
concentrations in samples collected from the Site and also document actual
contamination of the sensitive environments.
A total of nine federally endangered, threatened, or proposed ESUs of salmon or trout
migrate past the Site. The point value for each species (or ESU) utilizing the Columbia
River as a migratory route through an area of observed contamination is 75. Mercury,
cadmium, and silver found in source sediment samples all document an observed release
to the sensitive environment, but cannot be used to establish Level I concentrations as the
samples were not surface water samples. In addition to the evidence of actual
contamination by chemical analysis, the Site is located directly in the Columbia River,
and constitutes an observed release by direct observation, resulting in a Level II
contamination designation by direct observation. Therefore, nine separate endangered or
threatened species, at 75 points each, migrate through an area of observed Level II
contamination, which results in a total target score of 675 for the sensitive environment
portion of the surface water pathway.
The surface water migration pathway is a combination of the three components, Drinking
Water, Human Food Chain, and Sensitive Environments. The score of the three
components is 0.60, 57.60, and 60.0. The uncapped score for the surface water pathway
is 810, the capped score is 100.
Using the surface water migration pathway score, the site score is 50. The SI focused on
the surface water pathway, so the groundwater migration, soil exposure, and air migration
pathways were not evaluated.
Please contact Alexis Ande, the Site Assessment Group Leader, at (360) 443-6575 or Lesa
Nelson, the TechLaw Project Manager, at (360) 871-8777 if you have any questions or
comments regarding HRS memo.
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**** CONFIDENTIAL ****
****PRE-DECISIONAL DOCUMENT ****
**** SUMMARY SCORESHEET ****
**** FOR computing projected hrs score ****
**** Do Not Cite or Quote ****
Site Name: Drums-NE Marine Drive Region: 10
City, County, State: Portland, Multnomah Evaluator: Lesa Nelson
OR
EPA ID#: ORNOO1002678 Date: 10/22/2007
Lat/Long: 45.5819 North,-122.5597 West T/R/S: 1 North/2 East/Section 9
Congressional District: 3
This Scoresheet is for: SI
Scenario Name: Contaminated Sediment
Description: Contaminated sediment located beneath deteriorating drums and within the deteriorated
drums located on the bottom of the Columbia River.
S pathway
S2 pathway
Ground Water Migration Pathway Score (Sgw)
Surface Water Migration Pathway Score (Ssw)
100
10000
Soil Exposure Pathway Score (Ss)
Air Migration Score (Sa)
S2gw + S2sw + S2s + S2a
10000
(S2gw + S2sw + S2s + S2a)/4
2500
V" (S2gw + S2sw + S2s + S2a)/4
50
Pathways not assigned a score (explain): Groundwater, soil exposure, and air migration pathways were not
scored due to the location of the Site within the Columbia River. The source (contaminated sediment (soil) is
not available to migrate to any of the other pathways.
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1.0 Table 4-1 —Surface Water Overland/Flood Migration Component Scoresheet
Factor categories and factors
Maximum Value Assigned
Value
550
Watershed Evaluated:
Drinking Water Threat
Likelihood of Release:
1. Observed Release 550 550
2. Potential to Release by Overland Flow:
2a. Containment 10
2b. Runoff 10
2c. Distance to Surface Water 5
2d. Potential to Release by Overland Flow [lines 2a(2b + 2c)] 35 0
3. Potential to Release by Flood:
3a. Containment (Flood) 10
3b. Flood Frequency 50
3c. Potential to Release by Flood (lines 3a x 3b) 500 0
4. Potential to Release (lines 2d + 3c, subject to a maximum of 500) 500 0
5. Likelihood of Release (higher of lines 1 and 4) 550
Waste Characteristics:
6. Toxicity/Persistence (a) 10000
7. Hazardous Waste Quantity (a) 10
8. Waste Characteristics 100
Targets:
9. Nearest Intake 50
10. Population:
10a. Level I Concentrations (b)
10b. Level II Concentrations (b)
10c. Potential Contamination (b)
10d. Population (lines 10a + 10b + 10c) (b)
11. Resources 5 5
12. Targets (lines 9 + 10d + 11) (b)
Drinking Water Threat Score:
13. Drinking Water Threat Score [(lines 5x8x12)/82,500, subject to a max of 100] 100
Human Food Chain Threat
Likelihood of Release:
14. Likelihood of Release (same value as line 5) 550
Waste Characteristics:
15. Toxicity/Persistence/Bioaccumulation (a)
16. Hazardous Waste Quantity (a)
17. Waste Characteristics 1000
Targets:
18. Food Chain Individual 50
19. Population
19a. Level I Concentration (b)
19b. Level II Concentration (b) 3
19c. Potential Human Food Chain Contamination (b)
19d. Population (lines 19a + 19b + 19c) (b) 3
20. Targets (lines 18 + 19d) (b) 48
Human Food Chain Threat Score:
21. Human Food Chain Threat Score [(lines 14x17x20)/82500, subject to max of 100] 100 57.6
Environmental Threat
Likelihood of Release:
22. Likelihood of Release (same value as line 5) 550 550
Waste Characteristics:
500000000
10
45
5
0.6
550
180
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23. Ecosystem Toxicity/Persistence/Bioaccumulation (a) 500000000
24. Hazardous Waste Quantity (a) 10
25. Waste Characteristics 1000 180
Targets:
26. Sensitive Environments
26a. Level I Concentrations (b)
26b. Level II Concentrations (b) 675
26c. Potential Contamination (b)
26d. Sensitive Environments (lines 26a + 26b + 26c) (b) 675
27. Targets (value from line 26d) (b) 675
Environmental Threat Score:
28. Environmental Threat Score [(lines 22x25x27)/82,500 subject to a max of 60] 60 60
Surface Water Overland/Flood Migration Component Score for a Watershed
29. Watershed Score0 (lines 13+21+28, subject to a max of 100} 100 100
Surface Water Overland/Flood Migration Component Score
30. Component Score (Ssw)c (highest score from line 29 for all watersheds evaluated) 100 100
a Maximum value applies to waste characteristics category
b Maximum value not applicable
c Do not round to nearest integer
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Site Inspection Report
Drums NE-Marine Drive
Portland, Multnomah County, Oregon
TDD: 06-07-0006
TechLaw, Inc.
Contract EP-S7-06-03
Region 10
STARTS
Superfund Technical Assessment and Response Team
Submitted To: Joanne LaBaw, Task Monitor
United States Environmental Protection Agency, Region 10
1200 Sixth Avenue Suite 900- M/S ECL 112
Seattle, Washington 98101
December 2007
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
TABLE OF CONTENTS
1.0 INTRODUCTION 1
2.0 SITE BACKGROUND 2
2.1 Site Description and Background 2
2.1.1 Proj ect Location 2
2.1.2 Site Description and Current Use 2
2.1.3 Site Ownership 3
2.1.4 Site Operations and Waste Characteristics 3
2.2 Previous Investigations 4
2.2.1 Multnomah County Sheriffs Office and Metro 4
2.2.2 Oregon Department of Environmental Quality 4
2.2.3 START Preliminary Assessment 4
2.3 Site Inspection Site Visit 5
2.3.1 Summary of SI Investigation Locations 5
2.3.2 Summary of Locations and Conditions of Drums 5
3.0 FIELD ACTIVITIES AND ANALYTICAL PROTOCOL 8
3.1 Sampling Objectives 8
3.2 Sediment Sample Methodology 8
3.2.1 Sediment Samples Collected by START-3 8
3.2.2 Sediment Samples Collected by the EPA Dive Team 9
3.3 Analytical Protocols 9
3.4 Global Positioning System 9
3.5 Investigation-Derived Waste 9
SAMPLE LOCATION 15
4.0 QUALITY ASSURANCE/QUALITY CONTROL 16
4.1 Satisfaction of Data Quality Objectives 16
4.2 Quality Assurance/Quality Control Samples 16
4.3 Project-Specific Data Quality Objectives 16
4.3.1 Precision 17
4.3.2 Accuracy 17
4.3.3 Completeness 17
4.3.4 Representativeness 17
4.3.5 Comparability 17
5.0 ANALYTICAL RESULTS REPORTING AND BACKGROUND SAMPLES 18
5.1 Analytical Results Evaluation Criteria 18
5.1.1 Analytical Sample Results Reporting 19
5.2 Background Samples 19
5.2.1 Sample Locations 19
5.2.1.1 Sample Results 19
6.0 POTENTIAL SOURCES 21
6.1 Source 21
i
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
7.0 MIGRATION PATHWAYS AND TARGETS 31
7.1 Surface Water Migration Pathway 31
7.2 Sediment Sample Locations 31
7.3 Sediment Sample Results 31
7.4 Targets 32
8.0 SITE SUMMARY AND CONCLUSIONS 36
8.1 Sources 36
8.2 Pathways 36
8.3 Targets 36
8.4 Conclusions 37
9.0 REFERENCES 38
LIST OF TABLES
TABLE Page
TABLE 3-1 Sample Collection Summary 10
TABLE 6-1 Inorganic Sediment Analytical Results 22
TABLE 6-2 Organic Sediment Analytical Results 26
LIST OF FIGURES
FIGURE Page
FIGURE 2-1 General Site Location 6
FIGURE 2-2 Aerial Photo with General Site Location 7
FIGURE 3-1 Sample Locations 15
FIGURE 7-1 15-Mile Target Distance Limit Map Downstream 34
FIGURE 7-2 15-Mile Target Distance Limit Map Upstream 35
LIST OF APPENDICES
APPENDIX
A PHOTOGRAPHIC DOCUMENTATION
B GPS SAMPLE LOCATION DATA
C DATA VALIDATION MEMOS and LABORATORY DATA
D SAMPLE PLAN ALTERATON FORMS
E EPA DIVE REPORT
li
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
LIST OF ACRONYMS
Acronvm
Definition
%R
spike % recovery
°C
degrees Celsius
ASTM
American Society for Testing and Materials
bgs
below ground surface
CERCLA
Comprehensive Environmental Response, Compensation, and Liability Act
cfs
cubic feet per second
CLP
Contract Laboratory Program
CLP AS
Contract Laboratory Program Analytical Services
CRQL
contract required quantitation limit
CRDL
contract required detection limit
cssw
Columbia South Shore Well Field
Datachem
Datachem Laboratories, Inc.
DQOs
data quality objectives
Ecology
Washington Department of Ecology
EPA
United States Environmental Protection Agency
ESU
evolutionary significant units
Fishman
Fishman Environmental Services, LLC
GPS
Global Positioning System
HRS
Hazard Ranking System
IDW
investigation-derived waste
MEL
Manchester Environmental Laboratory
Metro
Metro Regional Parks and Greenspaces Department
mg/kg
milligrams per kilogram
lig/kg
micrograms per kilogram
MS/MSD
matrix spike/matrix spike duplicate
NOAA
National Oceanic and Atmospheric Administration
NPL
National Priorities List
NRC
National Response Corporation
ODEQ
Oregon Department of Environmental Quality
PA
Preliminary Assessment
PAH
polyaromatic hydrocarbon
PCB
polychlorinated biphenyl
Ponar
Petite Ponar Dredge
PPE
probable point of entry
QA
quality assurance
QC
quality control
RM
river mile
RPD
relative percent difference
SARA
Superfund Amendments and Reauthorization Act
SI
Site Inspection
Site
Drums NE-Marine Drive Site
SOPs
Standard Operating Procedures
SQAP
Sampling and Quality Assurance Plan
SQL
sample quantitation limit
START-3
Superfund Technical Assessment and Response Team-3
SVOC
semivolatile organic compound
TAL
Target Analyte List
TDD
Technical Direction Document
TDL
target distance limit
TechLaw
TechLaw, Inc.
TM
Task Monitor
111
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
LIST OF ACRONYMS (CONTINUED)
Acronym Definition
TOC Total Organic Carbon
USGS United States Geological Survey
VOC volatile organic compound
iv
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
1.0 INTRODUCTION
Pursuant to the United States Environmental Protection Agency (EPA) Region 10 Superfund
Technical Assessment and Response Team-3 (START-3) Contract No. EP-S7-06-03 and
Technical Direction Document (TDD) No. 06-07-0006, TechLaw, Incorporated (TechLaw)
conducted a site inspection (SI) at the Drums-NE Marine Drive Site (Site) in Portland, Oregon.
The SI activities performed were conducted under the Comprehensive Environmental Response,
Compensation, and Liability Act (CERCLA) of 1980 and the Superfund Amendments and
Reauthorization Act (SARA) of 1986.
The objectives of this Site Inspection are to:
Document a threat or potential threat to public health or the environment posed by the
Site;
Assess the need for additional detailed investigation and/or response action at the Site;
and
Provide the EPA with adequate information to determine whether the site is eligible for
placement on the Nation Priorities List (NPL).
This document includes the site background information (Section 2), field sampling activities
and analytical protocols (Section 3), quality assurance and quality control criteria (Section 4),
background sample results (Section 5), potential sources (Section 6), migration pathways and
targets (Section 7), summary and conclusions (Section 8), and references (Section 9).
1
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
2.0 SITE BACKGROUND
2.1 Site Description and Background
The following subsections discuss the Site background, description, ownership history, and
operations. Information presented in this subsection is based on a review of Site background
information using EPA Region 10 and Oregon Department of Environmental Quality (ODEQ)
files.
2.1.1 Project Location
Site Name: Drums - NE Marine Drive Site (Site)
EPA Identification Number: ORNOO1002678
Location: 9000 Block of NE Marine Drive
County: Multnomah
Latitude: 45.5819 North
Longitude: -122.5597 West
Legal Description: Section 09, Township 01 North, Range 02 East
Bank Property Site Owner/ Port of Portland-
Contact: 121 Northwest Everett Street
Portland, Oregon 97209-4049
(503) 944-7000
River Bottom Site Owner/ State of Oregon Water Resources Department
Contact: 725 Summer Street Northeast, Suite A
Salem, Oregon 97301
(503) 986-0900
2.1.2 Site Description and Current Use
The Site is located in Portland, Multnomah County, Oregon, in the Columbia River, along the
southern shoreline (Figure 2-1 and Figure 2-2). The surrounding land is urban and industrial;
located southwest of the Site is Portland International Airport and north of the Site is the
Government Island Complex.
The Columbia River is tidally influenced. Tidal effects can be observed during low river flow up
to Warrendale, Oregon, approximately river mile 141 and around 30 miles east of Portland,
Oregon (van der Naald, et al. 2004). The Columbia River estuary has a salt wedge. A salt
wedge is formed in estuaries when salt waters (which are heavier) move inland on and near the
bottom and fresh waters (which are lighter) move toward the sound on top. A density gradient
(wall) is formed and the bottom waters have no way of replenishing oxygen unless a strong wind
mixes the waters together (Lerner et al. 2006). It has been reported that during high runoff
events and low tides, seawater protrudes five miles inland of the river mouth (Larsson, et al.
2006). During low runoff periods and high tides seawater can intrude up to 23 miles inland
(Larsson, et al. 2006). Under these conditions seawater influence on salinity can extend up to
river mile 37 due to the mixing of the salt wedge with river water (Larsson, et al. 2006). The
2
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Drums-NE Marine Drive Site
Site Inspection Report
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December 2007
Government Island Complex is located within river mile 111.5 (western part of the Government
Island Complex) and 118 (eastern part of the Government Island Complex) (Topinka 2006). The
Site is located just south of Lemon Island, which is located on the western part of the
Government Island Complex. The lower Columbia River is subject to annual flooding in late fall
and early winter when rains are the heaviest (van der Naald, et al. 2004). The average annual
flow for the Columbia River at The Dalles, Oregon is approximately 190,000 cubic feet per
second (cfs) (Washington State Department of Ecology (Ecology) 2006). The Dalles, Oregon is
located approximately 60 miles southeast of Portland, Oregon.
The Government Island Complex is 2,200 acres in area, and consists of Government Island,
Lemon Island, and McGuire Island (Fishman Environmental Services, LLC (Fishman) 2002).
The Government Island Complex is owned by the Port of Portland, except for 224 acres, which
are owned by the Metro Regional Parks and Greenspaces Department (Metro) (Fishman 2002).
These islands are only accessible by boat, and are state recreational areas (Fishman 2002). The
Government Island Complex supports wetland mitigation projects, recreation, and livestock
(Fishman 2002). Many federally and state threatened and endangered species live on these
islands (Fishman 2002). Details regarding federally and state threatened and endangered species
are found in the Surface Water Pathway section.
2.1.3 Site Ownership
According to the Oregon Admissions Act, the State of Oregon "shall have concurrent jurisdiction
on the Columbia and all other rivers and waters bordering the State of Oregon, so far as the same
shall form a common boundary to said State, and any other State or States now or hereafter to be
formed or bounded by the same; and said rivers and waters, and all the navigable waters of said
State, shall be common highways and forever free, as well as to the inhabitants of said State as to
all other citizens of the United States, without any tax, duty, impost, or toll therefore (Oregon
1859)...". Under the Oregon Admissions Act, the Columbia River belongs to the State of
Oregon from river mile 0 to river mile 309 (Oregon 2007).
The Port of Portland owns the banks of the southern shoreline of the Columbia River, Portland,
Multnomah County, Oregon with the following Property identifications: R317064, R317076,
and R317066 (Assessors 2007a, b, and c). The current use of the property is vacant and is zoned
as open space (Assessors 2007a, b, and c). There is a multi-use path located along the southern
Columbia River bank, just south of the Site.
2.1.4 Site Operations and Waste Characteristics
The Site was discovered and reported to ODEQ on September 28, 2005, by a city work crew. At
that time, it was estimated that there were 400 to 500 55-gallon drums with unknown contents
located along the Columbia River bottom. There were no original estimates as to the extent of
the drums but, according to Metro; they were spread over a fairly wide area (Kraten 2006a). It is
not known who owned, transported, or illegally disposed of the drums into the Columbia River;
as there are no known industrial uses of this stretch of river. Two samples were previously
collected from the Site and contained barium, chromium, polyaromatic hydrocarbons (PAHs),
phthalate, 2,4,6-Tribromophenol (a flame retardant chemical), semivolatile organic compounds
(SVOCs), poly chlorinated biphenyls (PCBs), cadmium, chromium, lead, and mercury (Specialty
Analytical 2005).
3
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
2.2 Previous Investigations
The following subsections discuss previous Site investigations, potential sources, and the
migration/exposure pathways and targets.
2.2.1 Multnomah County Sheriffs Office and Metro
The Site was reported to ODEQ on September 28, 2005, by a city work crew and is currently
inactive. The Sherriff s deputies on-scene estimated that there were 400 to 500 rusty, 55-gallon
drums, with no containment structures, located on the river bottom (ODEQ 2005).
On October 19, 2006, Multnomah County Sheriffs Office and Metro removed some old tires, a
car, and other trash from the Site. While on Site, Multnomah County Sheriffs Office and Metro
did some pre-inspections of the Site, with the assistance of a diver. The diver observed
approximately 200 drums in the channels, with some of the drums having large holes in them
(Kraten 2006b).
2.2.2 Oregon Department of Environmental Quality
ODEQ led an investigation on September 29, 2005. National Response Corporation (NRC), an
environmental consulting firm contracted to ODEQ, collected two samples at the Site: a
sediment sample and a sludge sample. No background samples were collected (Hyke 2006).
According to ODEQ, the drums, which were scattered over a fairly wide area, contained a
sludgy, flaky, green substance, and when the drums were disturbed they left a sheen in the water
(Greenburg 2006; Kraten 2006a). All of the drums observed appeared to be very old and
disintegrated (Hyke 2006).
The sediment sample was collected from along the water's edge, and the sludge sample was
collected from inside a partially-filled drum (Hyke 2006). The sediment sample contained
barium (51.5 milligrams per kilogram (mg/kg)), chromium (6.83 mg/kg), PAHs (concentrations
found between 137 to 2760 mg/kg), Bis(2-ethylhexyl)phthalate (325 micrograms per kilogram
(|ig/kg)), 2,4,6-Tribromophenol (a flame retardant chemical, 111 |ig/kg), SVOCs (concentrations
found between 73.9 and 105 |ig/kg), and Decachlorobiphenyl (a PCB, 94.9 |ig/kg) (Specialty
Analytical 2005). The sludge sample contained barium (71.8 mg/kg), cadmium (0.846 mg/kg),
chromium (11.4 mg/kg), lead (10.8 mg/kg), mercury (0.0244 mg/kg), bis(2-ethylhexyl)phthalate
(247 |ig/kg), 2,4,6-Tribromophenol (a flame retardant chemical, 98.2 |ig/kg), SVOCs
(concentrations found between 73.1 and 99.1 |ig/kg), volatile organic compounds (VOCs)
(concentrations found between 14.8 and 95.1 |ig/kg), and Decachlorobiphenyl (a PCB, 102
|ig/kg) (Specialty Analytical 2005). According to ODEQ, based on the analytical results, it was
likely that a release occurred.
2.2.3 START Preliminary Assessment
As part of an abbreviated Preliminary Assessment (PA), the EPA Task Monitor (TM) and
START-3 conducted a site reconnaissance inspection at the Site On September 8, 2006. The
EPA/START-3 team met with a representative of ODEQ in order to obtain additional Site
information. The team attempted to locate the area along the southern shoreline of the lower
Columbia River, where the drums were reportedly located. However, due to the high water
levels within the river at the time of the reconnaissance inspection, the drums were not observed.
4
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
On December 7, 2006, START-3 submitted the abbreviated PA report to the EPA TM. It was
recommended that a CERCLA SI conducted at the Site. It was also recommended that the Site
also be further evaluated to determine if any removal activities were warranted.
2.3 Site Inspection Site Visit
START-3 conducted sampling at the Site from April 23 to 27, 2007 in conjunction with the EPA
Dive Team.
A total of 33 sediment samples were collected and analyzed for SVOCs, PCBs, pesticides,
Target Analyte List (TAL) metals, mercury, total organic carbon (TOC), and grain-size. The
samples were analyzed either under the Contract Laboratory Program (CLP) contract or by
Manchester Environmental Laboratory (MEL). The CLP laboratory analyzed the samples for
SVOCs, PCBs, and pesticides. EPA Region 10 MEL analyzed the samples for TAL metals,
mercury, TOC, and grain size.
2.3.1 Summary of SI Investigation Locations
The objective of this SI was to determine if sediment has been impacted at or downstream of the
Site. A total of 33 sediment samples were collected and analyzed for SVOCs, TAL metals,
mercury, pesticides, PCBs, TOC, and grain size, to meet the SI objective. Of the sediment
sampling locations, seven were collected from within the drums themselves, 17 within the direct
vicinity of the drums, five were collected downstream of the Site, and four background samples
were collected.
2.3.2 Summary of Locations and Conditions of Drums
During the SI approximately 32 drums were located and confirmed to be in various stages of
disintegration; five of these drums were sampled during SI activities. The general location of the
drums is latitude 45.5819° north and longitude -122.5597° west. The exact numbers of drums
located in the area is not known, but reports range from 200 (according to the Multnomah
County Sheriffs Office diver) to 600 (according to the ODEQ Environmental Cleanup Site
Information Database Site Summary Report) (ODEQ 2007). Thirty-two drums were observed by
the EPA Dive Team. The conditions of these drums are as follows: five were intact with no
holes, two were intact with an obvious bulge, four were intact with holes, eight were rusted out
and barely intact, three were only partially intact, two were crushed, four only consisted of pieces
of drums scattered over the observed area,. No observations were provided of the remaining
four drums by the EPA Dive team due to low visibility.
Although sediment was observed in the drums, it cannot be stated definitively what the contents
of the drums were prior to their deposition on the river bottom. Due to the deteriorated nature of
the drums, it is possible that the sediment observed in the drums were deposited after the drums
deteriorated.
5
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Figure 2-1
General Site Location Map
Drums-NE Marine Drive,
Portland, Multnomah County,
Oregon
~ Site Location
£3 Waterbodies
Urban WA
[J Urban OR
N
10
^ Miles
TechLaw
Source: - Oregon Geospatial Enterprise Office
- Washington State Dept. of Ecology
Date: 09/27/07
Created by: MKS
-------
r &«i9§§3|£? C*$&!i?MiT-
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_ BwKWb.wa3ft«S!' ~;r" sS?F»Ffe Ir- '. ¦• ¦-«' yfr V-', 'Vj»
fs:"' -¦ ¦ i ! : ¦
Figure 2-2
Aerial Photo with
General Site Location Map
Drums NE Marine Drive
Portland, Multnomah County,
Oregon
Multnomah County, OR
it Site Locations
N
A
TechLaw
Source: TerraServer USGS 2002
Date: 09/27/07
Created by: MKS
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
3.0 FIELD ACTIVITIES AND ANALYTICAL PROTOCOL
3.1 Sampling Objectives
The sampling objective of this SI is to determine if Columbia River sediments have been
impacted by the release of contaminants. A total of 33 sediment samples were collected. All
samples were analyzed for SVOCs, TAL metals, mercury, PCBs, pesticides, TOC, and grain
size. Sample types and methods of collection are described below. A list of all samples collected
for fixed laboratory analysis under the SI is contained in Table 3-1 and the sample locations are
also shown in Figure 3-1. Photographic documentation of SI field activities is contained in
Appendix A.
A Sampling and Quality Assurance Plan (SQAP) was developed by START-3 and approved by
EPA prior to field sampling (TechLaw 2007). The SQAP was based on a review of background
information and interviews with site representatives. The SQAP describes the sampling strategy,
sampling methodology, and analytical program to investigate potential targets. Sample locations
were selected during the field sampling activities in conjunction with the EPA TM, START-3
Project Lead, and EPA Divers. Sample selection was based on the likelihood of proximity to the
drum area. Sample location selection also depended on the underwater visibility and the ability
to collect the sediment sample underwater with the river current. With few exceptions, SI field
activities were conducted in accordance with the approved SQAP. Deviations from the SQAP
were approved by the EPA and are described, when applicable in the sampling location
discussions in Section 6 and Section 7 and are also found in sample plan alteration forms
(SPAFs) located in Appendix D.
The START-3 SI field events were conducted from April 23 through April 27, 2007.
Alphanumeric identification numbers applied by START-3 to each sample location (e.g., DMD-
SD-01) are used in this SI report as the station location identifiers. Sample locations are
provided in Table 3-1. The sample locations specify the distance from the boat in nautical miles
in reference to the distance from the original Global Positioning System (GPS) Site location
provided by ODEQ.
3.2 Sediment Sample Methodology
Sediment samples were collected at the Site in accordance with the sampling methodologies and
standard operating procedures (SOPs) provided in the SQAP. Samples designated to be analyzed
for TAL metals were preserved as required by the SOP. A total of 33 sediment samples were
collected. Twenty-four sediment samples were collected from within the area of the drums;
seven of those samples were collected from sediment located inside of the drums themselves.
Five sediment samples were collected downstream of the Site, and four background sediment
samples were collected upstream of Site.
3.2.1 Sediment Samples Collected by START-3
The five downstream and three of the four background sediment samples were collected by
START-3. The fourth background was collected by the EPA Dive Team and is described in
Section 3.2.2. START-3 used a Petite Ponar Dredge (Ponar) to collect sediment samples from 0
to 6 inches below ground surface (bgs) in depth. Two to three volumes were collected from the
Ponar to obtain the required 24-oz of sediment for the samples. The sample material was placed
8
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
into a dedicated stainless steel bowl, excess water decanted, and sample material homogenized.
START-3 then placed the requisite aliquot of sample material into pre-labeled sample containers.
3.2.2 Sediment Samples Collected by the EPA Dive Team
Out of the total of 33 sediment samples obtained, the EPA Dive Team collected 26, including
two duplicates and one background. The EPA Dive Team collected seven of the sediment
samples from within the drums themselves (described as Drum Sample in Table 3-1); 17
sediment samples from close proximity of the drums (described as Drum Vicinity in Table 3-1),
including a duplicate sample; and one background sediment samples, upgradient of Site
influences. These samples were collected from 0- to 6-inches bgs in depth using a one foot long,
4-inch diameter, thin-walled, beveled corer. The EPA Dive Team then brought the corer to the
surface of the Columbia River and handed the corer and sample off to START-3. START-3 then
placed the sample material into a dedicated stainless steel bowl, decanted excess water, and
homogenized the sample material. The EPA Dive Report is located in Appendix E.
3.3 Analytical Protocols
Samples collected for SVOCs, PCBs, and pesticides were analyzed by Contract Laboratory
Program Analytical Services (CLPAS). Analytical methods for SVOCs, PCBs, and Pesticides
were completed using EPA Method SOMOl.l by Datachem Laboratories, Inc. (Datachem), in
Salt Lake City, Utah. Analyses for TAL metals and mercury were completed using EPA
Method 200.7/6010B and 200.8 by EPA MEL in Port Orchard, Washington. Analysis of TOC
was completed by EPA MEL using EPA Method 415.1. Analysis of grain size was completed
by EPA MEL using American Society for Testing and Materials (ASTM) D 421-85 (Standard
Practice for Dry Preparation of Soil Samples for Particle Size Analysis and Determination of Soil
Constants).
3.4 Global Positioning System
The GP-1650 DF, Garmin 276C, and the Garmin Handheld 60CS were utilized by START-3
personnel to record coordinates of all sample locations. The Trimble was not utilized due to
space constraints on the boat. GPS coordinates are provided in Appendix B.
3.5 Investigation-Derived Waste
Investigation-derived waste (IDW) generated during the SI sampling effort consisted of solid
sampling equipment (gloves) disposed of as non-hazardous waste through the City of Portland
solid waste program. No IDW generated during the SI sampling effort remains on site.
9
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Table 3-1
Sample Collection Summary
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
Cl.l*
Sample
II)
Matrix
Description
07174000
DMD-SD-01
J86R0
Sediment
Background Sample. Boat located 0.2 nautical miles
east of ODEQ GPS location. Sample collected
approximately 15 meters west of boat location.
Sediment consists of coarse sand/small gravel.
07174002
DMD-SD-02
J86R1
Sediment
Background Sample. Boat located 1.25 nautical
miles east of ODEQ GPS location. Sample collected
at boat location. Sediment consists of coarse
sand/small gravel.
07174003
DMD-SD-03
J86R2
Sediment
Background Sample collected 0.2 nautical miles
west of stormwater outfall. Boat located 2.59
nautical miles upstream from ODEQ GPS location.
Sample collected at boat location. Sediment consists
of coarse sand/small gravel.
07174004
DMD-SD-04
J86R3
Sediment
Downstream Sample. Boat located 0.5 nautical
miles downstream from ODEQ GPS location.
Sample collected at boat location. Sediment consists
of coarse sand/small gravel.
07174005
DMD-SD-05
J86R4
Sediment
Downstream Sample. Boat located 1 nautical mile
downstream from ODEQ GPS location. Sample
collected at boat location. Sediment consists of
coarse sand/small gravel.
07174006
DMD-SD-06
J86R5
Sediment
Downstream Sample. Boat located 1.5 nautical
miles downstream from ODEQ GPS location.
Sample collected at boat location. Sediment consists
of brown coarse sand/small gravel.
07174007
DMD-SD-07
J86R6
Sediment
Drum Vicinity Sample. Boat located at ODEQ GPS
location. Sample collected approximately 19
meters west of boat location. Sediment consists of
coarse sand/small gravel.
07174008
DMD-SD-08
J86R7
Sediment
Drum Vicinity Sample. Boat located at ODEQ GPS
location. Sample collected approximately 36
meters west of boat location. Sediment consists of
coarse sand/small gravel.
07174009
DMD-SD-09
J86R8
Sediment
Drum Vicinity Sample. Boat located 0.57 nautical
miles west of ODEQ GPS location. Sample
collected approximately 10 meters west of boat
location. Sample collected 6 inches south of a
rusted out drum. Sediment consists of clay/silt.
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
10
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Table 3-1 (Continued)
Sample Collection Summary
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
Cl.l*
Sample
II)
Matrix
Description
07174010
DMD-SD-10
J86R9
Sediment
Drum Sample. Boat located 0.57 nautical miles
west of ODEQ GPS location. Sample collected
approximately 18 meters west of boat location.
Sample collected from inside of a rusted drum. One
other drum observed in vicinity. Sediment consists
of clay/silt.
07174011
DMD-SD-11
J86S0
Sediment
Drum Vicinity Sample. Boat located 0.57 nautical
miles west of ODEQ GPS location. Sample
collected 23 meters west of boat location. Sediment
consists of coarse sand/small gravel.
07174012
DMD-SD-12
J86S1
Sediment
Drum Sample. Boat located 0.57 nautical miles
west of ODEQ GPS location. Sample collected 37
meters west of boat location. Sample collected from
inside a large intact drum. Sediment consists of
clay/silt.
07174013
DMD-SD-13
J86S2
Sediment
Drum Vicinity Sample collected just south of DMD-
SD-12. Boat located 0.57 nautical miles west of
ODEQ GPS location. Sample collected 37 meters
west of boat location. Sample collected from
sediment south of a large intact drum. Sediment
consists of clay/silt.
07174014
DMD-SD-14
J86S3
Sediment
Drum Vicinity Sample. Boat located 0.48 nautical
miles west of ODEQ GPS location. Sample
collected between 9 and 15 meters west of boat
location. Sample collected from sediment beneath a
crushed drum. Sediment consists of coarse
sand/small gravel.
07174015
DMD-SD-15
J86S4
Sediment
Drum Vicinity Sample. Boat located 0.48 nautical
miles west of ODEQ GPS location. Sample
collected approximately 18.5 meters west of boat
location. Sample collected from sediment adjacent
to a full intact drum. Sediment consists of coarse
sand/small gravel.
07174016
DMD-SD-16
J86S5
Sediment
Drum Sample. Boat located 0.78 nautical miles
west of ODEQ GPS location. Sample collected
approximately 50 meters west of boat location.
Sample collected from inside a 2/3 rusted drum with
paper thin side walls. Sediment consists of coarse
sand/small gravel.
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
li
-------
Table 3-1 (Continued)
Sample Collection Summary
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
Cl.l*
Sample
II)
Matrix
Description
07174017
DMD-SD-17
J86S6
Sediment
Drum Vicinity Sample. Boat located 0.78 nautical
miles west of ODEQ GPS location. Sample
collected approximately 31 meters west of boat
location. Sample collected from sediment adjacent
to a dilapidated drum. Sediment consists of clay/silt.
07174018
DMD-SD-18
J86S7
Sediment
Drum Vicinity Sample. Boat located 0.78 nautical
miles west of ODEQ GPS location. Sample
collected from approximately 16 meters west of boat
location. Sample collected from sediment in
between a 2/3 drum and an intact drum. Sediment
consists of clay/silt.
07174019
DMD-SD-19
J86S8
Sediment
Drum Sample. Boat located 0.74 nautical miles
west of ODEQ GPS location. Sample collected
approximately 44 meters west of boat location.
Sample collected from inside of a barely intact
drum. Sediment consists of clay/silt.
07174020
DMD-SD-20
J86S9
Sediment
Drum Sample. Boat located 0.74 nautical miles
west of ODEQ GPS location. Sample collected
approximately 27 meters west of boat location.
Sample collected from inside of a partially buried
drum with top exposed. Sediment consists of
clay/silt.
07174021
DMD-SD-21
J86T0
Sediment
Drum Sample. Boat located 0.71 nautical miles
west of ODEQ GPS location. Sample collected
approximately 45 meters west of boat location.
Sample collected from inside a drum, on its side,
deteriorated with hole on down slope side. Sediment
consists of clay/silt.
07174022
DMD-SD-22
J86T1
Sediment
Drum Vicinity Sample. Boat located 0.71 nautical
miles west of ODEQ GPS location. Sample
collected approximately 17 meters west of boat
location. Sediment consists of clay/silt.
07174023
DMD-SD-23
J86T2
Sediment
Drum Vicinity Sample. Boat located 0.67 nautical
miles west of ODEQ GPS location. Sample
collected approximately 35 meters west of boat
location. An intact drum is located 32 meters west
of sample. Sediment consists of clay/silt with some
metal shards.
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
12
-------
Table 3-1 (Continued)
Sample Collection Summary
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
C U>
Sample
II)
Matrix
Description
07174024
DMD-SD-24
J86T3
Sediment
Drum Vicinity Sample. Boat located 0.67 nautical
miles west of ODEQ GPS location. Sample
collected approximately 13 meters west of boat
location. Sediment consists of coarse sand/small
gravel.
07174025
DMD-SD-25
J86T4
Sediment
Drum Vicinity Sample. Boat located 0.62 nautical
miles west of ODEQ GPS location. Sample
collected approximately 30 meters west of boat
location. Sediment consists of clay/silt.
07174026
DMD-SD-26
J86T5
Sediment
Drum Vicinity Sample. Boat located 0.62 nautical
miles west of ODEQ GPS location. Sample
collected approximately 12 meters west of boat
location. Sediment consists of clay/silt.
07174027
DMD-SD-27
J86T6
Sediment
Downstream Sample. Boat located 1.5 nautical
miles from ODEQ GPS location. Sample collected
from boat location. Sediment consists of brown
coarse sand/small gravel. Duplicate for DMD-SD-
06.
07174028
DMD-SD-28
J86T7
Sediment
Drum Vicinity Sample. Boat located 0.78 nautical
miles west of ODEQ GPS location. Sample
collected approximately 31 meters west of boat
location. Sample collected from sediment adjacent
to a dilapidated drum. Sediment consists of clay/silt.
Duplicate for DMD-SD-17
07174029
DMD-SD-29
J86T8
Sediment
Drum Sample. Boat located 0.71 nautical miles
west of ODEQ GPS location. Sample collected
approximately 45 meters west of boat location.
Sample collected from inside a drum, on its side,
deteriorated with hole on down slope side. Sediment
consists of clay/silt. Duplicate for DMD-SD-21.
07174034
DMD-SD-30
J86W4
Sediment
Drum Vicinity Sample. Boat located 0.56 nautical
miles west of ODEQ GPS location. Sample
collected approximately 29 meters west of boat
location. Sediment consists of clay/silt.
07174035
DMD-SD-31
J86W5
Sediment
Drum Vicinity Sample. Boat located 0.56 nautical
miles west of ODEQ GPS location. Sample
collected approximately 10 meters west of boat
location. Sediment consists of clay/silt.
07174036
DMD-SD-32
J86W6
Sediment
Background Sample. Boat located 0.2 nautical miles
east of ODEQ GPS location and further south from
DMD-SD-01. Sediment consists of clay/silt.
13
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
-------
Table 3-1 (Continued)
Sample Collection Summary
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
C U>
Sample
II)
Matrix
Description
07174037
DMD-SD-33
J86W7
Sediment
Downstream Sample. Boat located 2.37 nautical
miles west of ODEQ GPS location. Sample
collected from boat location. Sediment consists of
clay/silt. Downstream Sample.
07174030
DMD-RB-01
J86W0
Water
Rinsate blank collected from the Ponar.
07174031
DMD-RB-02
J86W1
Water
Rinsate blank collected from a sampling spoon and
bowl.
07174032
DMD-RB-03
J86W2
Water
Rinsate blank collected from 2 corer lids (1 with
holes and 1 without) and one corer.
07174033
DMD-RB-04
J86W3
Water
Rinsate blank collected from a sampling spoon and
bowl.
KEY
CLP Sample ID = Contract Laboratory Program Organic tracking code. Inorganic code includes an M at the front.
DMD = Drams- NE Marine Drive
Dram Sample = Sample collected from sediment located in a dram
Dram Vicinity = Sample collected from within the area where the drams are located
EPA Sample ID = EPA Region 10 Regional sample tracking code
GPS = Global Positioning System
ODEQ = Oregon Department of Environmental Quality
Ponar = Petite Ponar Dredge
RB = Rinsate blank
SD = Sediment
Station ID = START-3 sample tracking code
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
14
-------
DMD-SD-19
DMD-SD-20
DMD-SD-29
DMD-SD-21
DMD-SD-25
DMD-SD-26
¦*¦ X- \vT NH
;¦»
"
Ih^H iKM
. o DMD-SD-31 '
DMD-SD-30
I | -:.HV,
DMD-SD-09
DMD-SD-10
DMD-SD-11
DMD-SD-13
3 OX)
00
Figure 3-1
Aerial Photo with
Sample Location Map
Drums NE Marine Drive
Portland, Multnomah County,
Oregon
Multnomah County, OR
Sample Points
N
TechLaw
Source: TerraServer USGS 2002
Date: 09/27/07
Created by: MKS
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
4.0 QUALITY ASSURANCE/QUALITY CONTROL
A total of 33 sediment samples were analyzed for the SVOC, TAL metals, mercury, PCBs,
pesticides, and TOCs. Organic analysis was performed in accordance with the USEPA Contract
Laboratory Program Statement of Work for Trace Organic Analysis SOMOl.l (EPA 2005).
TAL metals and mercury samples were analyzed by MEL in accordance with EPA Method
200.7/6010B and 200.8. TOC samples were analyzed by MEL in accordance with EPA Method
415.1. Specific quality assurance/quality control (QA/QC) requirements for analyses of the Site
samples are presented in the CLP statement of work and the project SQAP (TechLaw 2007).
All data from analyses performed were reviewed and validated by an EPA chemist. Data
qualifiers were applied, as necessary, according to statements of work, analytical methods, and
the following guidance:
U.S. EPA Contract Laboratory Program National Functional Guidelines for Inorganic
Data Review (EPA 2002).
U.S. EPA Contract Laboratory Program National Functional Guidelines for Organic Data
Review (EPA 1999).
Manchester Environmental Laboratory Quality Assurance Manual and Standard
Operating Procedures.
Copies of the data QA memoranda are included in Appendix C.
4.1 Satisfaction of Data Quality Objectives
The data quality objectives (DQOs) for this site were established using the Guidance for the
Data Quality Objective Process (EPA 2000). The data quality achieved during field sample
collected and sample analyses conducted at the laboratories produced sufficient data to meet
DQOs established in the SQAP (TechLaw 2007).
4.2 Quality Assurance/Quality Control Samples
Samples were collected or processed in the field to assist analysis of QA/QC measures. QC
samples included temperature blanks, three field duplicates, and four equipment rinsate blanks.
One temperature blank sample per shipment cooler was submitted. QC samples for all analyses
included matrix spike and matrix spike duplicates (MS/MSD) at a rate of one sample per 20
sample media.
4.3 Project-Specific Data Quality Objectives
The following describes the laboratories' ability to meet project DQOs for precision, accuracy,
and completeness, and the overall success of the field team and the laboratories at meeting
project DQOs for representativeness and comparability. The laboratory and field team were able
to meet the project DQOs for all samples except for rinsate blank samples DMD-RB-02 and
DMD-RB-03. DMD-RB-02 and DMD-RB-03 water samples were extracted for pesticides and
PCBs outside seven days of sample collection date. The temperature blank was also 12° Celsius
(°C), which is just outside of the acceptable limits of 2° to 10°C.
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4.3.1 Precision
Precision measures the reproducibility of the sampling and analytical methodology. Laboratory
and field precision is defined as the relative percent difference (RPD) between duplicate sample
analyses. The laboratory duplicate samples measure the precision of the analytical method.
The RPD values were reviewed for all samples. No sample results were qualified solely based on
laboratory duplicate QC outliers.
4.3.2 Accuracy
Accuracy measures the reproducibility of sampling and analytical methodology. Laboratory
accuracy is defined as the spike % recovery (%R). The %R for all inorganic compounds and
organic compounds met the criterion.
4.3.3 Completeness
Data completeness is defined as the percentage of usable data (usable data divided by the total
possible data). All laboratory data were reviewed for data validation and usability.
Out of a total of 3,589 SVOC, PCBs, and pesticide results, 142 (approximately 4% of the data)
were qualified as non-detects (U); 54 (approximately 1.5% of the data) were qualified due to
calibration; 40 (approximately 1.1% of the data) were qualified due to deuterated monitoring
compounds; and 59 (approximately 1.7% of the data) were qualified due to holding time failure.
Therefore, the project DQO for completeness of 90% was met.
4.3.4 Representativeness
Data representativeness expresses the degree to which sample data accurately and precisely
represent a characteristic of a population, parameter variations at a sampling point or
environmental condition. The number and selection of samples were determined in the field to
account accurately for site variations and sample matrices. The DQO for representativeness of
90% was met.
4.3.5 Comparability
Comparability is a qualitative parameter expressing the confidence with which one data set can
be compared to another. Data produced for this site followed applicable field sampling
techniques and specific analytical methodology as applied to sediment. The DQO for
comparability was met.
17
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5.0 ANALYTICAL RESULTS REPORTING AND BACKGROUND SAMPLES
This section describes analytical results reporting, the sample locations, and analytical results of
SI samples obtained from background samples. The sampling rationale and analytical results are
summarized in the following sections. Tables 6-1 and 6-2 summarize sediment sample analytical
results. Laboratory data sheets of results for all samples are located in Appendix C.
5.1 Analytical Results Evaluation Criteria
Analytical results presented in the summary tables 6-1 and 6-2 in section 6, show all compounds
detected above laboratory detection limits. Analytical results indicating significant
concentrations above background are considered elevated and will be indicated in bold and
underlined. For the purposes of this Site Inspection, significant/elevated concentrations are
defined, using Table 2-3 of the EPA Hazard Ranking System (HRS) model criteria for observed
release as follows:
• Equal to or greater than the sample's contract required quantitation limit (CRQL/CRDL),
or the sample quantitation limit (SQL) when a non-CLP laboratory was used; and
• Equal to or greater than the background sample's CRQL/CRDL or SQL when the
background concentration is below detection limits; or
• At least three times greater than the background concentration when the background
concentration equals or exceeds the detection limit.
MEL performed a thorough visual check of all 33 samples and determined that approximately
half were clay/silt samples and half were coarse sand/small gravel samples. MEL decided to do
two grain size fractions using the following representative samples: DMD-SD-03 (coarse
sand/small gravel) and DMD-SD-32 (clay/silt). The other 31 samples were then visually
compared to the two representative samples and were either determined to be clay/silt or coarse
sand/small gravel samples. The sediment samples were then organized into groups by TechLaw
START-3 and compared to similar background samples (e.g. coarse sand/small gravel and
clay/silt). Background samples DMD-SD-01, DMD-SD-02, and DMD-SD-03 consisted of
coarse sand/small gravel and were used for comparison for coarse sand/small gravel sediment
samples. Those samples composed primarily of clay/silt were compared to background sediment
sample DMD-SD-32. In the case where multiple background samples were collected for the
same matrix, the highest background value was used for comparison (i.e. within the sandy
sediments, three background samples were collected and the highest of the three background
concentrations for each constituent was used for comparison purposes).
The following qualifiers were used in data validation:
U The material was analyzed for but was not detected. The associated numerical
value is the sample quantitation limit.
J The associated numerical value is an estimated quantity because the reported
concentrations were less than the sample quantitation limits or because QC
criteria limits were not met.
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UJ The material was analyzed for, but not detected. The reported detection limit is
estimated because QC criteria were not met.
R The sample results are rejected (analyte may or may not be present) due to gross
deficiencies in QC criteria. Any reported value is unusable. Resampling and/or
reanalysis are necessary for verification.
5.1.1 Analytical Sample Results Reporting
Based on EPA Region 10 policy, evaluation of aluminum, calcium, iron, magnesium, potassium,
and sodium (common earth crust elements) is beyond the scope of this report. For this reason,
these elements are not discussed.
5.2 Background Samples
Background results are shown in the first column of the analytical results summary tables in this
section for comparison against source or target results. The background sample locations are
depicted in Figure 3-1.
5.2.1 Sample Locations
Four background samples were collected for the SI field sampling event upstream of Site. Due
to the distance of tidal influence along the Columbia River, it was not possible to be totally
removed from possible site influences. Multiple backgrounds were collected to take into account
the tidal influence and grain size. The three backgrounds collected also account for the
variability in local concentrations of contaminants.
DMD-SD-01 and DMD-SD-32 were collected 0.2 nautical miles upstream/east of the Site.
DMD-SD-01 sediment consisted of coarse sand/small gravel and DMD-SD-32 sediment
consisted of clay/silt. DMD-SD-02 was collected 1.25 nautical miles upstream/east of the Site
and consisted of coarse sand/small gravel. DMD-SD-03 was collected 2.59 nautical miles
upstream/east of the Site and the sediment consisted of coarse sand/small gravel.
5.2.1.1 Sample Results
The following eight TAL metals were detected in all coarse sand/small gravel background
sediment samples DMD-SD-01, DMD-SD-02 and DMD-SD-03: arsenic at concentrations of
0.54 to 1.9 mg/kg, beryllium (0.077 to 0.17 mg/kg), lead (1.3 to 3.18 mg/kg), chromium (5.57 to
20.4 mg/kg), copper (5.15 to 8.19 mg/kg), manganese (113 to 245 mg/kg), nickel (6.02 tol2.3
mg/kg), and zinc (23.2 to 42.7mg/kg). Overall, the highest concentrations were detected in
DMD-SD-01, which was also collected closest to the Site.
In addition to the eight TAL metals listed above, barium and cobalt were also detected in coarse
sand/small gravel background sample DMD-SD-01 at concentrations of 38.5 and 6.42 mg/kg,
respectively. Silver was detected in the coarse sand/small gravel background sediment sample
DMD-SD-03 at a concentration of 1.6 mg/kg. Mercury was not detected in any coarse
sand/small gravel background samples. Acetophenone, benzaldehyde, bis(2-ethylhexyl)
phthalate, 4-methylphenol, and methoxychlor were detected in the coarse sand/small gravel
background samples as well; however, all SVOCs, pesticides, and PCBs detected in background
samples were at concentrations well below the detection limit for that constituent.
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Background sample DMD-SD-32, consisted of clay/silt and was also collected near the Site.
Detected contaminants and concentrations are as follows: mercury (0.036 J mg/kg), arsenic (5.18
mg/kg), beryllium (0.93 mg/kg), cadmium (0.74 mg/kg), lead (9.84 mg/kg), silver (0.17 mg/kg),
barium (204 mg/kg), chromium (23.4 mg/kg), cobalt (13.7 mg/kg), copper (24.1 mg/kg),
manganese (848 mg/kg), nickel (25.2 mg/kg), and zinc (72.3 mg/kg). SVOCs detected in the
clay/silt background sample included acetophenone, bis(2-ethylhexyl)phthalate, 4-methylphenol,
and methoxychlor; all contaminants were detected below the CRQL.
The results can be found below in Tables 6-1 and 6-2. The tables are organized by sediment type
(i.e. sandy versus clayey) and sample location (i.e. drums samples).
20
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Site Inspection Report
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6.0 POTENTIAL SOURCES
Sampling locations, sampling rationale, and analytical results are summarized in the following
sections. Tables 6-1 and 6-2 summarize analytes detected at each potential source location
investigated. Laboratory analytical results for all samples are provided in Appendix C.
6.1 Source
During the SI field event, seven samples were collected from within seven drums and seventeen
sediment samples were collected within the immediate vicinity of the drums. All of these
samples are considered part of the contaminated sediment source area. Of the sediments
collected from within the drums, the grain size analysis revealed that one of the seven drum
samples consisted of coarse sand/small gravel sediment and six of the seven drums samples
consisted of clay/silt sediments. Of the seventeen samples collected from the vicinity of the
drums, six consisted of coarse sand/small gravel sediments, and the remaining eleven samples
consisted of clay/silt sediments.
From within the coarse sand/small gravel fraction of the sediment samples, mercury was detected
at an elevated concentration of 0.016 mg/kg in drum sample DMD-SD-16; mercury was also
detected in four of the six samples collected from the drum vicinity (DMD-SD-11, DMD-SD-14,
DMD-SD-15, and DMD-SD-24) at concentrations between 0.021 J to 0.035 J mg/kg. Drum
vicinity sample DMD-SD-24 also contained elevated concentrations of barium (159 mg/kg),
beryllium (0.69 mg/kg), cadmium (0.80 mg/kg), copper (24.9 mg/kg) and silver (0.18 mg/kg),
There were no elevated SVOCs, pesticides, or PCBs detected within the coarse sand/small gravel
sediment samples (DMD-SD-07, DMD-SD-08, DMD-SD-11, DMD-SD-14, DMD-SD-15,
DMD-SD-16, DMD-SD-24).
From within the clay/silt fraction of the sediment samples, selenium was the only elevated TAL
metal constituent detected in drum sediment sample DMD-SD-12 at a concentration of 0.57
mg/kg; selenium was also detected at elevated concentrations ranging from 0.51 mg/kg to 0.76
mg/kg in drum vicinity sediment samples DMD-SD-09, DMD-SD-13, DMD-SD-17, DMD-SD-
18, and DMD-SD-23. Other TAL metals detected at elevated concentrations include barium
(156 mg/kg), beryllium (0.6 mg/kg), cadmium (0.62 mg/kg), copper (30.7 mg/kg), mercury (0.39
mg/kg), and silver (0.13 mg/kg) in sediment sample DMD-SD-17 and zinc in DMD-SD-25 at a
concentration of 290 mg/kg.
Elevated SVOCs detected within the clay/silt fraction of the sediment samples collected from
within the drums included acetophenone in sediment sample DMD-SD-29 at a concentration of
98J |ig/kg, bis (2-ethylhexyl) phthalate in DMD-SD-20 (99 J |ig/kg), and 4-methylphenol in
DMD-SD-10 and DMD-SD-29 at a concentration of 290 |ig/kg and 170 |ig/kg , respectively.
No SVOCs, pesticides, or PCBs were detected at elevated concentrations from the clay/silt
fraction of the sediment samples collected in the drum vicinity.
21
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-1
Inorganic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i>A II) NO.
07174
07174002
07174003
07174016
07174007
07I7400S
07174011
07174014
07174015
( I P II) NO.
JN6K0
.isr.ui
mi*:
J86S5
.IN6K6
•IN6K7
J86S0
J86S3
JN6S4
STATION NO.
DMD-SD-OI
DMD-SD-02
DMD-SD-03
I)\1I)-SI)-I6
l)\ll)-SI)-07
DMD-SD-OS
l)MI)-SI)-l 1
DMD-SD-14
DMD-SD-15
TAI. Mi-lals
Background Sampli-s
Drum Sampk-s
Drum Yk'inil\
(m»/k»)
(loarsc saild/Mliall »ra\d)
(coarse
U'oarsi- sand/small srawl)
sand/small
»ra\i-l)
Mercury
0.010 UJ
0.01 UJ
0.01 UJ
0.016 J
—
—
0.035 J
0.031 J
0.021 J
Arsenic
1.9
0.74
0.54
1.7
0.66
0.81
1.6
1.9
1.8
Beryllium
0.17
0.085
0.077
0.14
0.052
0.066
0.20
0.18
0.12
Cadmium
0.5 U
0.5 U
0.5 U
—
—
—
—
—
—
Lead
3.18
1.6
1.3
5.71
1.2
2.5
4.89
5.64
5.02
Selenium
0.5 U
0.5 U
0.5 U
—
—
—
—
—
—
Silver
0.05 U
0.05 U
0.05 U
—
—
—
—
—
—
Barium
38.5
28.3
26.4
51.1
19.6
27.8
69.8
67.4
50.3
Chromium
20.4
5.57
10.2
9.98
4.5
5.52
12.2
11.9
12.2
Cobalt
6.42
2.9
3.42
4.01
2.62
2.81
5.60
5.17
4.77
Copper
8.19
5.24
5.15
17.3
5.00
5.48
10.3
13.2
10.7
Manganese
245
113
115
128
121
127
173
170
150
Nickel
12.3
6.02
8.39
9.37
5.36
6.47
11.6
10.7
10.3
Zinc
42.7
27.6
23.2
37.4
20.0
19.7
49.2
46.4
41.0
22
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-1 (Continued)
Inorganic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i>.\ id \u.
07174002
07174003
07174024
07174004
07174005
07174006
07174027
( I P II) NO.
JN6K0
•isr.ui
mu:
mi3
•IN6K3
•IN6K4
JN6K5
•IN6K7
Sl;i 1 i Siimpks
I)ii\misIiv;iiii Siiinpk's
(lii;irsi- s;ill(l/s111;i 11
s«iiiil/sill;i 11 »r;i\i-|)
s«i 11 il/sill;iII ^r;iM-|)
Mercury
()()1() ( ]J
0.01 U.I
0.01 U.I
0.026 J
—
—
—
—
Arsenic
1.9
0.74
0.54
4.54
0.84
0.79
1.0
1.1
Beryllium
0.17
0.085
0.077
0.69
0.079
0.073
0.092
0.078
Cadmium
0.5 U
0.5 U
0.5 U
0.80
—
—
—
—
Lead
3.18
1.6
1.3
7.97
1.6
2.0
1.9
1.8
Selenium
0.5 U
0.5 U
0.5 U
—
—
—
—
—
Silver
0.05 U
0.05 U
0.05 U
0.18
—
—
—
—
Barium
38.5
28.3
26.4
159
29.0
35.6
39.0
30.1
Chromium
20.4
5.57
10.2
23.5
6.04
11.8
5.95
5.58
Cobalt
6.42
2.9
3.42
9.96
2.86
4.05
3.19
2.96
Copper
8.19
5.24
5.15
24.9
6.33
5.45
5.60
5.05
Manganese
245
113
115
365
129
137
148
136
Nickel
12.3
6.02
8.39
19.4
6.14
9.32
7.39
6.8
Zinc
42.7
27.6
23.2
64.5
25.0
32.9
28.5
28.0
23
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Drums-NE Marine Drive Site
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Table 6-1 (Continued)
Inorganic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i>A II) NO.
07174036
07174010
07174012
0717401')
07174020
07174021
0717402')
0717400')
07174013
07174017
( I P II) NO.
J86W6
.IS6K')
msi
JN6SN
.INKS')
•isr.ro
.ISMS
•IN6KN
JN6S2
JN6S6
STATION NO.
D.MD-SD-32
DMD-SD-IO
DMD-SD-12
DM D-SD-I')
DMD-SD-20
DMD-SD-21
DM D-SD-2')
DM D-SD-I 1')
DMD-SD-13
DMD-SD-17
TAI. Mihils
li;K'k^niiiii(l
Drum Siimpk's
Drum Yk'inil> S;ini|>k-s
(m»/k»)
Siiinpk's
Ul;i\/sill)
(ilii\/sili)
(il;i\/sill)
Mercury
0.036 J
0.091 J
0.029 J
0.031 J
—
0.064 J
0.101 J
0.038 J
0.059 J
0.039
Arsenic
5.18
2.3
4.32
5.2
2.1
2.1
2.1
5.86
5.75
3.32
Beryllium
0.93
0.24
0.55
0.24
0.12
0.32
0.33
0.81
0.78
0.6
Cadmium
0.74
—
1
0.54
...
0.6
0.6
0.97
0.88
0.62
Lead
9.84
8.35
7.98
6.65
9.14
6.93
6.9
9.39
8.74
7.71
Selenium
0.5 U
-
0.57
...
—
—
—
0.76
0.75
0.51
Silver
0.17
0.068
0.12
0.084
—
0.074
0.073
0.18
0.16
0.13
Barium
204
83.0
130
91.7
40.8
97.3
99.4
167
169
156
Chromium
23.4
13.9
21.7
13.9
15.7
13.0
13.8
24.8
21.9
21.8
Cobalt
13.7
6.03
9.33
11.3
5.53
6.64
6.94
12.1
11.3
10.2
Copper
24.1
29.9
22.7
51.7
8.89
21.3
21.7
32.9
31.5
30.7
Manganese
848
219
323
229
171
226
233
399
376
435
Nickel
25.2
13.6
18.5
29.6
11.3
13.2
13.5
23.3
21.6
20.3
Zinc
72.3
72.4
60.8
60.8
42.2
58.8
64.8
69.7
65.2
59.8
24
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Table 6-1 (Continued)
Inorganic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
1 l> \ II) NO.
07174036
07I740IN
07174022
07174023
07174025
07174026
07I7402S
07174034
07174035
07174037
( I P II) NO.
J86W6
J86S7
mil
•IN6T2
jsr. 14
•IN6T5
•IS6I7
•IN6W 4
J86W5
•JN6W 7
STATION
DM D-SD-32
DMD-SD-IS
DM D-SD-22
DMD-SD-23
DMD-SD-25
DMD-SD-26
DMD-SD-2N
DMD-SD-30
DMD-SD-31
DMD-SD-33
NO.
TAL Melals
liaek Samples
Dow nslreain
(ila\/sili)
(ila\/sill)
Sample
(ila\/sill)
Mercury
0 0 J
0.036 J
0.058 J
0.040 J
0.111 J
0.024
0.042 J
0.028 J
0.031 J
0.043 J
Arsenic
5.18
2.94
2.4
2.92
3.71
2.0
3.05
2.2
2.5
1.8
Beryllium
0.93
0.61
0.34
0.58
0.44
0.30
0.57
0.53
0.70
0.11
Cadmium
0.74
0.61
—
0.73
0.53
—
0.55
0.50
0.91
—
Lead
9.84
26.9
5.77
5.65
6.23
8.54
17.3
7.69
7.56
3.76
Selenium
0.5 U
0.51
—
0.5
—
—
—
—
—
—
Silver
0.17
0.12
0.079
0.12
0.077
0.061
0.11
0.10
0.13
—
Barium
204
138
86
158
126
97.1
140
132
158
54.2
Chromium
23.4
19.6
13.4
16.1
15.7
12.8
16.8
17.8
19.5
7.08
Cobalt
13.7
9.54
6.52
8.91
7.82
6.31
9.19
8.21
9.91
3.98
Copper
24.1
20.8
14.8
33.5
34.8
15.2
22.6
22.6
28.4
8.37
Manganese
848
398
221
310
1240
259
383
231
252
164
Nickel
25.2
20.5
12.7
16.2
16.7
12.1
17.5
18.6
20.3
7.85
Zinc
72.3
54.8
51.3
54.5
290
41.7
52.1
54.6
73.0
39.5
KEY:
= Non-detect
Bold and Underline = Concentration elevated when compared to background concentration(s), as defined in Section 5
CLP ID Number = Contract Laboratory Program sample identification number
DMD = Drums-NE Marine Drive
EPA ID Number = EPA Region 10 Regional EPA sample identification number
J = The analyte was positively identified. The associated numerical result is an estimate.
mg/kg = milligrams per kilogram
NO. = Number
SD = Sediment
Station ID = START-3 sample tracking code
TAL = Total Analyte List
U = The analyte was not detected at or above the reported result
25
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Table 6-2
Organic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i>A II) NO.
07174000
07174002
07174003
07174016
07174007
0717400X
07174011
07174014
07174015
07174024
( I P II) NO.
.isr.Ro
•isr.Ri
•ISf.R2
J86S5
JSf.kf.
.JNf»K7
.JN6S0
.ISf.SJ
.JS6S4
.1X613
STATION NO.
DMD-SD-01
DMD-SD-02
DMD-SD-03
DMD-SD-U.
DMD-SD-07
DMD-SD-ON
l).MI)-SI)-11
DMD-SD-14
DMD-SD-15
DMD-SD-24
All;il\ le
liackground Samples
Drum Samples
Drum \ icinih Samples
(coarse sand/small »ra\el)
(course saml/small gra\cl)
(coarse saml/small gra\cl)
Semivolatile Organic Compounds (jig/kg)
Acetophenone
71 J
20 J
32 J
50 J
20 J
21 J
25 J
17 J
19 J
45 J
Benzaldehyde
210 U
33 J
260 U
—
60 J
51 J
57 J
50 J
51 J
—
Benzo(a)anthracene
210 U
220 U
260 U
—
—
—
—
15 J
—
Benzo(a)pyrene
210 U
220 U
260 U
—
—
—
—
17 J
—
Benzo(b)fluoranthene
210 U
220 U
260 U
—
—
—
—
17 J
—
Benzo(g,h,i)perylene
210 U
220 U
260 U
—
—
—
—
—
—
Benzo(k)fluoranthene
210 U
220 U
260 U
—
—
—
—
8.2 J
—
Bis(2)-ethylhexyl)phthalate
33 J
220 U
28 J
31 J
—
—
—
24 J
23 J
Butylbenzylphthalate
210 U
220 U
260 U
—
—
—
—
—
—
Chrysene
210 U
220 U
260 U
—
—
—
—
12 J
—
Dimethy lphthalate
210 U
220 U
260 U
—
—
—
—
—
—
Di-n-butyl phthalate
210 U
220 U
260 U
—
—
—
—
—
—
Fluoranthene
210 U
220 U
260 U
—
—
—
—
30 J
—
4-Methylphenol
210 U
220 U
21 J
—
—
9.6 J
—
—
Naphthalene
210 U
220 U
260 U
—
—
—
—
8.0 J
—
Phenanthrene
210 U
220 U
260 U
—
—
—
—
14 J
—
Phenol
210 U
220 U
260 U
—
—
—
—
—
—
Pyrene
210 U
220 U
260 U
___
___
___
12 J
___
32 J
—
Pesticides and PCBs (ng/kg)
Beta-BHC
2.1 U
2.1 U
2.2 U
—
—
—
—
—
—
Heptachlor epoxide
2.1 U
2.1 U
2.2 U
—
—
—
—
—
—
Dieldrin
2.1 U
4.1 U
2.2 U
—
—
—
0.12 J
—
—
4,4'-DDE
4.1 U
4.1 U
4.2 U
—
—
—
0.36 J
0.23 J
—
Endosulfan II
4.1 U
4.1 U
4.2 U
—
—
—
—
—
—
4,4'-DDD
4.1 U
4.1 U
4.2 U
—
—
—
—
—
—
4,4'-DDT
4.1 U
4.1 U
4.2 U
—
—
—
0.21 J
—
—
Methoxychlor
0.46 J
0.46 J
22 U
0.27 J
—
—
—
—
—
Gamma-chlordane
2.1 U
2.1 U
2.2 U
___
___
___
0.17 J
___
___
—
Total Organic Carbon
mg/kg)
Total Organic Carbon
966
212
204
2,200
235
266
3,000
2,930
3,450
2,820
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
26
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-2 (Continued)
Organic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
1 l> \ II) NO.
(IP II) NO.
STATION NO.
07174000
.isr.ko
D.MD-SD-
01
07174002
•isr.ki
DMD-SD-02
07174003
mi*:
DMD-SD-03
07174004
•ISfikj
DMD-SD-04
07174005
•ISfiR4
DMD-SD-05
0717400ft
.JW.R5
l)MI)-si)-or.
07174027
mu7
DMD-SD-27
An:il\ le
liackground Samples
(coarse sand/small »ra\el)
Downstream Samples
(coarse sand/small »ra\el)
Semivolatile Organic Compounds (jig/kg)
Acetophenone
71 J
20 J
32 J
19 J
21 J
17 J
21 J
Benz aldehyde
210 U
33 J
260 U
35 J
29 J
34 J
51 J
Benzo(a)anthracene
210 U
220 U
260 U
—
—
—
—
Benzo(a)pyrene
210 U
220 U
260 U
—
—
—
—
Benzo(b)fluoranthene
210 U
220 U
260 U
—
—
—
—
Benzo(g,h,i)perylene
210 U
220 U
260 U
—
—
—
—
Benzo(k)fluoranthene
210 U
220 U
260 U
—
—
—
—
Bis (2-
ethylhexyl)phthalate
33 J
220 U
28 J
—
—
—
—
Butylbenzylphthalate
210 U
220 U
260 U
—
—
—
—
Chrysene
210 U
220 U
260 U
—
—
—
—
Dimethylphthalate
210 U
220 U
260 U
—
—
—
—
Di-n-butyl phthalate
210 U
220 U
260 U
—
—
—
—
Fluoranthene
210 U
220 U
260 U
—
—
—
—
4-Methylphenol
210 U
220 U
21 J
—
—
—
—
Naphthalene
210 U
220 U
260 U
—
—
—
—
Phenanthrene
210 U
220 U
260 U
—
—
—
—
Phenol
210 U
220 U
260 U
—
—
—
—
Pyrene
210 U
220 U
260 U
...
...
—
—
Pesticides and PCBs (jig/kg)
Beta-BHC
2.1 U
2.1 U
2.2 U
—
—
—
—
Heptachlor epoxide
2.1 U
2.1 U
2.2 U
—
—
—
—
Dieldrin
2.1 U
4.1 U
2.2 U
—
—
—
—
4,4'-DDE
4.1 U
4.1 U
4.2 U
—
—
—
—
Endosulfan II
4.1 U
4.1 U
4.2 U
—
—
—
—
4,4'-DDD
4.1 U
4.1 U
4.2 U
—
—
—
—
4,4'-DDT
4.1 U
4.1 U
4.2 U
—
—
—
—
Methoxychlor
0.46 J
0.46 J
22 U
—
—
—
—
Gamma-chlordane
2.1 U
2.1 U
2.2 U
...
...
—
—
Total Organic Carbon (mg/kg)
Total Organic Carbon
966
212
204
263
94
96
279
27
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-2 (Continued)
Organic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i>.\ id n.i.
07174036
07174010
07174012
0717401')
07174020
07174021
0717402')
07174009
07174013
07174017
( I P II) No.
J86W6
miw
JN6SI
JN6SN
.INKS')
mm
J86T8
mux
ms:
msr.
Si;i 1 i
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-2 (Continued)
Organic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
1 l>.\ II) NO.
07174036
071740 IS
07174022
07174023
07174025
07174026
0717402N
07174034
07174035
07174037
( I P II) NO.
J86W6
J86S7
mil
.isr. 12
jsr, 14
•IN6T5
JK6T7
.JNfiW 4
JNfiW 5
.1X6 \\ 7
Si ;i 1 it ill NO.
DM D-SD-32
DMD-SD-IS
DMD-SD-22
DMD-SD-23
DMD-SD-25
DMD-SD-26
DMD-SD-2S
DMD-SD-30
DMD-SD-31
DMD-SD-33
All;il> k-
liackgriiiind
(il;i\/sill)
Drum Ykinilv S;impk-s
Ul;i\/sill)
Dow nsliv;im
S;ini|>k'
U'l;i\/sili)
Semivolatile Organic Compounds (jig/kg)
Acetophenone
32 J
—
77 J
54 J
52 J
41 J
48 J
37 J
51 J
24 J
Benzaldehyde
260 U
—
—
—
—
—
—
—
83 J
Benzo(a)anthracene
260 U
—
12 J
—
—
—
—
—
—
Benzo(a)pyrene
260 U
—
—
—
—
—
—
—
—
Benzo(b)fluoranthene
260 U
—
15 J
—
14 J
—
—
—
—
Benzo(g,h,i)perylene
260 U
—
—
—
—
—
—
—
—
Benzo(k)fluoranthene
260 U
—
—
—
—
—
—
—
—
Bis (2-
28 J
—
77 J
39 J
49 J
20 J
45 J
19 J
23 J
—
ethylhexyl)phthalate
Butylbenzylphthalate
260 U
—
—
—
—
—
—
—
—
—
Chrysene
260 U
—
13 J
—
11 J
—
—
—
—
—
Dimethy lphthalate
260 U
—
67 J
—
—
—
—
—
—
—
Di-n-butyl phthalate
260 U
—
—
—
21 J
8.8 J
—
—
—
—
Fluoranthene
260 U
—
13 J
—
—
—
—
—
—
—
4-Methylphenol
21 J
—
—
—
—
—
—
—
—
19 J
Naphthalene
260 U
—
—
—
—
—
—
—
—
—
Phenanthrene
260 U
—
—
—
12 J
—
—
—
—
—
Phenol
260 U
—
—
—
—
—
—
—
—
—
Pyrene
260 U
—
21 J
...
19 J
—
___
___
___
___
Pesticides and PCBs (jig/kg)
Beta-BHC
2.6 U
—
—
—
—
—
—
—
—
—
Heptachlor epoxide
2.6 U
—
—
—
—
—
—
—
—
—
Dieldrin
5.1 U
—
0.21 J
0.18 J
—
0.054 J
—
—
—
—
4,4'-DDE
5.1 U
—
—
—
—
—
—
—
—
—
Endosulfan II
5.1 U
—
—
—
—
—
—
—
—
—
4,4'-DDD
5.1 U
—
—
—
—
0.14 J
—
—
—
—
4,4'-DDT
5.1 U
—
—
—
—
—
—
—
—
0.60 J
Methoxychlor
0.37 J
—
1.6 J
0.77 J
0.61 J
—
—
0.44 J
—
—
Gamma-chlordane
2.6 U
—
...
...
—
0.062 J
___
—
—
___
Total Organic Carbon (mg/kg)
Total Organic Carbon | 2,750
7,310
5,300
6,610
7,140
2,070
11,700
3,250
10,900
3,100
29
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Table 6-2 (Continued)
Organic Sediment Analytical Results
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
= Non-detect
Bold and Underline = Concentration elevated when compared to background concentration(s), as defined in Section 5
CLP ID No. = Contract Laboratory Program sample identification number
DMD = Drums-NE Marine Drive
EPA ID No. = EPA Region 10 Regional EPA sample identification number
J = The analyte was positively identified. The associated numerical result is an estimate
mg/kg = Milligrams per kilogram
No. = Number
PCBs = Polychlorinated biphenyls
SD = Sediment
Station ID = START-3 sample tracking code
(ig/kg = Micrograms per kilogram
U = The analyte was not detected at or above the reported result
UJ = The analyte was not detected at or above the reported estimated result. The associated numerical value is an estimate of the quantitation limit of
the analyte in the sample.
30
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
7.0 MIGRATION PATHWAYS AND TARGETS
The following section describes the surface water migration pathway and potential targets within
the site's range of influence. The groundwater, air migration, and soil exposure pathways are
not being evaluated as part of this SI. Therefore, the only pathway discussed is the surface water
migration pathway.
7.1 Surface Water Migration Pathway
¦ Environmental Setting and Surface Water Flow
The Site lies within the Columbia Slough watershed. The two-year, 24-hour rainfall for the
Site is 2.52 inches (National Oceanographic and Atmospheric Administration (NOAA)
1973). The mean annual precipitation for Portland, Oregon for April is 2.33 inches and 1.97
inches for May (National Weather Service 1999). The Site is located directly within the
Columbia River with no containment structures. There are no known drinking water intakes
along the target distance limit (TDL).
The Columbia River is tidally influenced. Tidal effects can be felt during low river flow up
to Warrendale, Oregon, approximately river mile 141 and around 30 miles east of Portland,
Oregon (van der Naald, et al. 2004). The Columbia River estuary has a salt wedge. It has
been reported that during high runoff events and low tides, seawater protrudes five miles
inland of the river mouth (Larsson, et al. 2006). During low runoff periods and high tides
seawater can intrude up to 23 miles inland (Larsson, et al. 2006). Under these conditions
seawater influence on salinity can extend up to river mile 37 due to the mixing of the salt
wedge with river water (Larsson, et al. 2006). The lower Columbia River is subject to annual
flooding in late fall and early winter when rains are the heaviest (van der Naald, et al. 2004).
The average annual flow for the Columbia River at The Dalles, Oregon, is approximately
190,000 cfs (Ecology 2006). The Dalles, Oregon, is located approximately 60 miles
southwest of Portland, Oregon.
The Site TDLs are shown in Figures 7-1 and 7-2. Because the lower Columbia River is
tidally-influenced, with the tidal influx of approximately 141 nautical miles, the TDL extends
downstream for 15 nautical miles and also extends upstream for an additional 15 nautical
miles from the probable point of entry (PPE).
7.2 Sediment Sample Locations
Seven sediment samples were collected from within the drums themselves, 17 in the immediate
vicinity of the drums, and five downstream from the Site. The drums and the surrounding
sediments are located within the Columbia River. Therefore, any elevated contaminants detected
either within the drums, in the vicinity of the drums, or downstream of the Site, constitute an
observed release to the Columbia River. The specific locations of the sediment samples are
provided in Figure 3-1.
7.3 Sediment Sample Results
The TAL metal sample results are depicted in Table 6-1 and SVOC, pesticide/PCB and TOC
sample results are located in Table 6-2. Only detected contaminants are included in the tables.
31
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
All sediment samples were categorized according to the sample matrix (either coarse sand/small
gravel or clay/silt) and compared to similar background samples. When more than one
background sample of the matrix was collected, the highest concentration of the constituent
within the set of samples was used for comparison purposes.
Overall, the following contaminants were detected at elevated concentrations in sediment
samples: barium, beryllium, cadmium, copper, lead, mercury, silver, selenium, zinc,
acetophenone, 4-methylphenol, and bis(2-ethylhexyl)phthalate.
For the coarse sand/small gravel sediment samples (collected from the drum vicinity and within
the drums), elevated TAL metals were detected in five samples (DMD-SD-11, DMD-SD-14,
DMD-SD-15, DMD-SD-16, and DMD-SD-24). Elevated contaminants and their concentrations
included: barium (159 mg/kg), beryllium (0.69 mg/kg), cadmium (0.80 mg/kg), copper (24.9
mg/kg), mercury (0.0121 J to 0.035 J mg/kg), and silver (0.18 mg/kg). No SVOCs, pesticides, or
PCBs were found at elevated concentrations in the coarse sand/small gravel sediment samples.
Although TAL metals were detected in the drum vicinity and drum samples, no TAL metals
were detected at elevated concentrations in downstream sediment samples.
From within the clay/silt fraction of the sediment samples, selenium was detected in five samples
collected from the drum vicinity and from within the drums (DMD-SD-09, DMD-SD-12, DMD-
SD-13, DMD-SD-17, DMD-SD-18, and DMD-SD-23) at concentrations ranging from 0.51
mg/kg to 0.76 mg/kg. Elevated concentrations of mercury (0.39 mg/kg), barium (156 mg/kg),
beryllium (0.6 mg/kg), cadmium (0.62 mg/kg), copper (30.7 mg/kg) and silver (0.13 mg/kg)
were detected in one sediment sample collected from within the drum vicinity (DMD-SD-17).
An elevated concentration of zinc was detected in sediment sample DMD-SD-25 collected from
the drum vicinity (290 mg/kg). Although TAL metals were detected in the drum vicinity and
drum samples, no TAL metals were detected at elevated concentrations in downstream clay/silt
fraction sediment samples.
SVOCs detected at elevated concentrations in the clay/silt fraction of sediment samples included
acetophenone in DMD-SD-29 (98J |ig/kg), bis(2-ethylhexyl)phthalate in DMD-SD-20 (99 J
|ig/kg) and 4-methylphenol in DMD-SD-10 and DMD-SD-29 (290 |ig/kg and 170J |ig/kg,
respectively), all of which were collected from within the drums. No SVOCs were detected at
elevated concentrations in drum vicinity or downstream samples.
PCBs and pesticides were not detected at elevated concentrations in the coarse sand/small gravel
sediment samples, nor were they found in the clay/silt sediment samples. The complete data set
is located in Appendix C.
7.4 Targets
Located north of the Site is the Government Island Complex, which encompasses approximately
2,200 acres, and consists of Government Island, Lemon Island, and McGuire Island (Fishman
2002). The Government Island Complex is owned by the Port of Portland, except for 224 acres,
which are owned by the Metro (Fishman 2002). These islands are only accessible by boat, and
are state recreational areas (Fishman 2002). The Government Island Complex supports wetland
mitigation projects, recreation, and livestock (Fishman 2002). Many federally and state
32
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
threatened and endangered species live on these islands (Fishman 2002). Details regarding
federally and state threatened and endangered species are discussed below.
Anadromous salmon, Steelhead Trout, and Cutthroat Trout use the Columbia River as a
migratory route between upstream spawning areas and the Pacific Ocean (Fishman 2002). There
are four evolutionary significant units (ESUs) of Chinook Salmon, one ESU of Columbia River
Chum Salmon, one ESU of Lower Columbia River/Southwest Washington Coho Salmon, and 4
ESUs of Steelhead Trout, which migrate past the Government Island Complex (Fishman 2002).
There is also the Snake River Sockeye Salmon, a federally endangered species, which migrates
past the Government Island Complex (Fishman 2002). The Southwest Washington/Lower
Columbia River Coastal Cutthroat Trout ESU is proposed for federal listing as a threatened
species and is found in the Columbia River in the Government Island Complex vicinity (Fishman
2002). According to NOAA, a salmon stock are considered a distinct population and hence a
"species" under the Endangered Species Act, if it represents an ESU of the biological species
(NMFS 1991).
Recreational fishing occurs on the Columbia River, and many fish are kept and consumed
(Melcher 2006). There were a total of 421,686 fishing trips on the lower Columbia River in
2004 (Takata, et al. 2005). From these fishing trips, 43,418 Chinook Salmon, 1,335 Coho
Salmon, 10,166 Steelhead Trout, 22 Cutthroat Trout, 27,525 White Sturgeon, and 29 Green
Sturgeon were kept (Takata, et al. 2005).
There are no tribal fisheries within the Site TDL (Gartzke 2007). Commercial Drift Gillnet
Fishing occurs within the Sites TDL and the species of fish caught are Chinook Salmon, Coho
Salmon, White Sturgeon, and Shad (Case 2007b). The Site is located within Columbia River
Commercial Fisheries Zone 4, which starts at river mile (RM) 87.5 and goes to RM 129, for a
total of 41.5 RM (Case 2007a). The number of pounds for various fishes caught in 2006 for
Commercial Fisheries Zone 4 is as follows: 76,114 pounds of Chinook Salmon; 11,937 pounds
of Coho Salmon; 8,025 pounds of White Sturgeon; and 14 pounds of Shad (Case 2007b).
Another federal species of concern and a state sensitive species of undetermined status is the
Northern Red-Legged Frog. This species is found in the wetlands and slow moving streams on
the Government Island Complex (Fishman 2002). A pair of Bald Eagles, a federally and state
threatened species, have a nest on Government Island and catch food in the Columbia River
(Fishman 2002). The Purple Martin, a state sensitive species, forages for insects over the
Columbia River in the Government Island Complex vicinity (Fishman 2002).
The entire island is located within the 15-mile TDL of the Site, and although all 2000 feet of
wetlands in the area are located north of the Government Island Complex, tidal influences could
potentially move and deposit contaminants at any point on or near these wetlands.
33
-------
Figure 7-1
15-Mile Target Distance Limit
Map Downstream
Drums NE Marine Drive
Portland, Multnomah County,
Oregon
Down-Stream TDL
~ PPE
n End TDL
Note; The Columbia River is assumed to be
tidaiiy influenced in this region therefore
TDL provided up and down stream of PPE
N
2
D Miles
TechLaw
Source: TerraServer USGS 1975
Date: 09/27/07
Created by: MKS
-------
*Su
Figure 7-2
15-Mile Target Distance Limit
Map Upstream
Drums-NE Marine Drive
Portland, Multnomah County,
Oregon
Up-Stream TDL
~ PPE
n End TDL
Note; The Columbia River is assumed to be
tidaiiy influenced in this region therefore
TDL provided up and down stream of PPE
N
D Miles
TechLaw
Source: TerraServer USGS 1975
Date: 09/27/07
Created by: MKS
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
8.0 SITE SUMMARY AND CONCLUSIONS
In April, 2007, START-3 conducted SI field sampling activities at the Site in
Multnomah County, Oregon. The Site was discovered in September 2005 and is
inactive. The SI objectives focused on the surface water pathway, therefore, only
samples were collected.
8.1 Sources
Contaminated sediments located around, beneath and within the deteriorating drums are
considered to be the source at the Site. The drums themselves were not considered to be a source
because it was not possible to determine if they contained hazardous materials at the time they
were disposed of into the Columbia River due to their deteriorated condition.
The extent of the contaminated sediment is not known. Elevated contaminants detected within
the source include: barium, beryllium, cadmium, copper, mercury, silver, selenium, zinc,
acetophenone, bis(2-ethylhexyl)phthalate, and 4-methylphenol.
8.2 Pathways
Contaminants may have migrated to the surface water pathway via a release from the sediments.
To determine if the surface water pathway has been impacted by the release of the sediments,
START-3 collected 29 sediment samples from the Columbia River in the vicinity or downstream
of the drums; four background samples were collected for comparison purposes. All Site and
downstream samples were categorized as either coarse sand/small gravel or clay/silt and
compared to the appropriate background for that matrix. Within the coarse sand/small gravel
category, three background samples were collected; one background sample was collected within
the silt/clay category. For each constituent, the highest background concentration was used for
comparison purposes to downstream samples. Elevated contaminants detected within close
proximity of the drums included barium, beryllium, cadmium, copper, mercury, silver, selenium,
and zinc. These results can be found in Tables 6-1 and 6-2.
8.3 Targets
Evidence of ESUs, federally endangered species, and threatened species are located within the
area of the Site. According to NOAA, a salmon stock are considered a distinct population and
hence a "species" under the Endangered Species Act, if it represents an ESU of the biological
species (NMFS 1991). Anadromous salmon, Steelhead Trout, and Cutthroat Trout use the
Columbia River as a migratory route between upstream spawning areas and the Pacific Ocean
(Fishman 2002). There are four ESUs of Chinook Salmon, one ESU of Columbia River Chum
Salmon, one ESU of Lower Columbia River/Southwest Washington Coho Salmon, and 4 ESUs
of Steelhead Trout, which migrate past the Government Island Complex (Fishman 2002). There
is also the Snake River Sockeye Salmon, a federally endangered species, which migrates past the
Government Island Complex (Fishman 2002). The Southwest Washington/Lower Columbia
River Coastal Cutthroat Trout ESU is proposed for federal listing as a threatened species and is
found in the Columbia River in the Government Island Complex vicinity (Fishman 2002).
Portland,
currently
sediment
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Recreational fishing occurs on the Columbia River, and many fish are kept and consumed
(Melcher 2006). In 2004, 43,418 Chinook Salmon, 1,335 Coho Salmon, 10,166 Steelhead Trout,
22 Cutthroat Trout, 27,525 White Sturgeon, and 29 Green Sturgeon were caught for recreational
purposes (Takata, et al. 2005). There are no tribal fisheries within the Site TDL (Gartzke 2007).
Commercial fisheries within the Site's TDL include Chinook Salmon, Coho Salmon, White
Sturgeon, and Shad (Case 2007a). In 2006, a total of 76,114 pounds of Chinook Salmon, 11,937
pounds of Coho Salmon, 8,025 pounds of White Sturgeon, and 14 pounds of Shad were caught
in Columbia River Commercial Fisheries Zone 4 (Case 2007b).
Another federal species of concern and a state sensitive species of undetermined status is the
Northern Red-Legged Frog. This species is found in the wetlands and slow moving streams on
the Government Island Complex (Fishman 2002). A pair of Bald Eagles, a former federally and
state threatened species, have a nest on Government Island and catch food in the Columbia River
(Fishman 2002). The Purple Martin, a state sensitive species, forages for insects over the
Columbia River in the Government Island Complex vicinity (Fishman 2002). No wetlands are
located within the 15-mile TDL of the Site.
8.4 Conclusions
Results of the SI indicate that sediments at the Site are a source of contamination to the surface
water pathway. The SI documents that contaminants were detected in the sediment samples at
elevated concentrations.
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
9.0 REFERENCES
Ashton. David, April 17, 2007. Telephone conversation between David Ashton, of Port of
Portland; and Lesa Nelson, of TechLaw, Incorporated (TechLaw) Port Orchard, Washington,
RE: Drums - NE Marine Drive.
Case, Doug, October 11, 2007a. Telephone conversation between Doug Case, of Oregon
Department of Fish and Wildlife Columbia River Fisheries Assistant Project Lead; and Lesa
Nelson, of TechLaw, Port Orchard, Washington, RE: Drums-NE Marine Drive Commercial
Fisheries.
Case, Doug, October 11, 2007b. Email from Doug Case, of United States Fish and Wildlife
Columbia River Commercial Fisheries Assistant Project Lead; to Lesa Nelson, of TechLaw, Port
Orchard, Washington, RE: Commercial within the 15-Mile TDL of Drums - NE Marine Drive.
Fishman Environmental Services, LLC (Fishman), March 7, 2002. Government Island
Management Plan, prepared for Port of Portland Property and Development Services.
Gartzke, Stacy, September 19, 2007. Telephone conversation between Stacy Gartzke, of United
States Fish and Wildlife Fisheries Division; and Lesa Nelson, of TechLaw, Port Orchard,
Washington, RE: Commercial and Tribal Fisheries within the 15-Mile TDL of Drums - NE
Marine Drive.
Greenburg, Michael, October 24, 2006. Telephone conversation between Michael Greenburg, of
ODEQ; and Lesa Nelson, of TechLaw, Port Orchard, Washington, RE: Drums - NE Marine
Drive.
Hoffman, Richard, March 21, 2007. Telephone conversation between Richard Hoffman, of City
of Vancouver Water Department; and Lesa Nelson, of TechLaw, Port Orchard, Washington, RE:
City of Vancouver groundwater locations.
Hyke, Bob, October 24, 2006. Telephone conversation between Bob Hyke, of NRC
Environmental; and Lesa Nelson, of TechLaw, Port Orchard, Washington, RE: Drums - NE
Marine Drive.
Kraten, Steve, November 2, 2006a. Telephone conversation between Steve Kraten, of Portland
Oregon Metro Regional Parks and Greenspaces Department (Metro); and Lesa Nelson, of
TechLaw, Port Orchard, Washington, RE: Drums - NE Marine Drive.
Kraten, Steve, October 24, 2006b. Telephone conversation between Steve Kraten, of Portland
Oregon Metro; and Lesa Nelson, of TechLaw, Port Orchard, Washington, RE: Drums - NE
Marine Drive.
Larsson, Ingrid; and Mark Sytsma, October 2006. Ballast Water Management on the Columbia
River. Prepared by Center of Lakes and Reservoirs, Portland State University. Prepared for the
Puget Sound Action Team.
38
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Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
Lerner, Ed K. and Brenda Wilmoth Lerner, Gale Group, Inc., September 18, 2007. "Salt
Wedging." World of Earth Science. eNotes.com.
Melcher, Kevleen, August, 18, 2006. Telephone conversation between Kevleen Melcher, of
Oregon Department of Fish and Wildlife; and Lesa Nelson, of TechLaw, Port Orchard,
Washington, RE: Fisheries in the Lower Columbia River.
Multnomah County Oregon Division of Assessment and Taxation (Assessor), January 29, 2007a.
Portland Maps Detail Report Property ID R317064.
Multnomah County Oregon Division of Assessment and Taxation (Assessor), January 29, 2007b.
Portland Maps Detail Report Property ID R317076.
Multnomah County Oregon Division of Assessment and Taxation (Assessor), January 29, 2007c.
Portland Maps Detail Report Property ID R317066.
National Marine Fisheries Service (NMFS), National Oceanic and Atmospheric Administration
(NOAA), and Department of Commerce, November 21, 2007. Policy on Applying the
Definition of Species under the Endangered Species to Pacific Salmon, Docket Number
9100248-1255
NOAA, 1973. Precipitation-Frequency Atlas of the Western United States, Volume II-Oregon.
National Weather Service, 1999. Portland's Monthly and Annual Precipitation, Wettest and
Driest.
Oregon Department of Environmental Quality (ODEQ), December 22, 2005. ODEQ Facility
Summary Report for Location 91141.
, March 2007. Environmental Cleanup Site Information Database Site Summary Report -
Details for Site ID 4544, Drums - NE Marine Drive.
Portland Water Bureau, 2007. The Columbia South Shore Well Field Wellhead Protection
Program.
Specialty Analytical, October 12, 2005. Sample Analysis for Marine Drive Drums/18400,
prepared for Bob Hyke, NRC.
State of Oregon (Oregon), February 14, 1859. Oregon Admissions Act, Act of Congress
Admitting Oregon into the Union, Section 2 Jurisdiction over waters forming boundary of state;
use of navigable waters as free highways.
39
-------
Drums-NE Marine Drive Site
Site Inspection Report
Revision 3
December 2007
, last updated March 13, 2007. Public Ownership of Submerged and Submersible Land,
Oregon's Publicly-Owned Waterways, on-line.
http://www.oregon.gov/DSL/NAV/navigwaterways.shtml
Takata, Howard; and James Watts, December 2005. The 2004 Lower Columbia River and Buoy
10 Recreational Fisheries.
TechLaw, April 2007. Region 10 START-3 Final Sampling and Quality Assurance Plan
Revision 1, Drums-NE Marine Drive Site, United States Environmental Protection Agency.
United States Environmental Protection Agency (EPA), October 1999. EPA Contract
Laboratory Program National Functional Guidelines for Organic Data Review, OSWER 9240.1-
05A-P, PB 99-963506, EPA 540/R-99/008.
, August 2000. Guidance for the Data Quality Objectives Process, EPA QA/G-4, Office
of Research and Development, Washington, D.C., EPA/600/R-96/055.
. July 2002. USER A Contract Laboratory Program National Functional Guidelines for
Inorganic Data Review. OSWER 9240.1-35, EPA 540-R-01-008.
, May 2005. EPA Contract Laboratory Program Statement of Work for Organic
Analysis, Multi-Media, Multi-Concentration, SOM01.1.
Topinka, Lyn, October 2006. Lewis and Clark's Columbia River- 200 years later "Government
Island", LewisClarkColumbiaRiver/Regions/Places/governmentisland.html.
United States Geological Survey (USGS), completed 1991. Oregon Water Science Center
Hydrologic Studies Portland Basin Ground-Water Study Project Description.
, 1993. A Description of Hydrogeologic Units in the Portland Basin, Oregon and
Washington, prepared in cooperation with City of Portland Bureau of Water Works,
Intergovernmental Resource Center, and Oregon Water Resources Department.
van der Naald, Wayne; Cameron Duff; and Robert Brooks, December 2004. Evaluation of Fall
Chinook and Chum Salmon Spawning Below Bonneville Dam.
Washington State Department of Ecology (Ecology), 2006. Columbia River Facts and Maps.
Prepared by Columbia River Water Management Program.
40
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APPENDIX A
PHOTOGRAPHIC DOCUMENTATION
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Pholo
Dnvclion
Sik- l.ocalion
IX'scriplmn
\umlvr
I'aci nu
View of ODEQ GPS Location taken from NE
1
North/
ODEQ GPS
Marine Drive. Location Identified using Garmin
Northeast
Location
Hand Held 60CS
9
North/
ODEQ GPS
View of Flag along the Columbia River Shore
z,
Northeast
Location
identifying ODEQ GPS Location
0.5 Miles East of
View of Flag along NE Marine Drive, marking 0.5
3
North/Nort
ODEQ GPS
Miles east of ODEQ GPS Location. Location
heast
Location
measured using START-3 Suburban odometer.
1.5 Miles East of
View if Flag along NE Marine Drive, marking 1.5
4
North/
ODEQ GPS
Miles east of ODEQ GPS Location. Location
Northeast
Location
measured using START-3 Suburban odometer.
View if Flag along NE Marine Drive, marking 1.0
1.0 Miles East of
Miles east of ODEQ GPS Location at a stormwater
North/
ODEQ GPS
outfall. Location measured using START-3
Northeast
Location
Suburban odometer.
1.5 NM west
6
from ODEQ GPS
View of Neal Amick collecting sediment samples
Northeast
Location
DMD-SD-06 and DMD-SD-27 on EPA Boat.
1.5 NM west
7
from ODEQ GPS
View of Portland Shore taken from DMD-SD-06
South
Location
and DMD-SD-27 sample locations.
1.0 NM west
8
from ODEQ GPS
View of Portland Shore taken from DMD-SD-05
South
Location
sample location.
1.0 NM west
9
from ODEQ GPS
View of Vancouver Shore taken from DMD-SD-05
North
Location
sample location.
0.5 NM west
10
from ODEQ GPS
View of Portland Shore taken from DMD-SD-04
South
Location
sample location.
0.5 NM west
11
from ODEQ GPS
View of Government Island Complex taken from
North
Location
DMD-SD-04 sample location.
2.76 NM east
12
from ODEQ GPS
View of Stormwater Outfall located on the Portland
Southwest
Location
Shore.
2.76 NM east
13
from ODEQ GPS
View of Stormwater Outfall located on the Portland
Southwest
Location
Shore.
2.76 NM east
14
from ODEQ GPS
View of Stormwater Outfall located on the Portland
Southeast
Location
Shore taken from DMD-SD-03 Sample Location.
2.76 NM east
Zoomed in view of Stormwater Outfall located on
15
from ODEQ GPS
the Portland Shore taken from DMD-SD-03 Sample
Southeast
Location
Location.
1
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Pholo
Dnvclion
Sik- l.ocalion
IX'scriplmn
\umlvr
I'aci nu
2.76 NM east of
16
ODEQ GPS
View of the Portland Shore taken from DMD-SD-03
South
Location
Sample Location.
2.76 NM east of
17
ODEQ GPS
View of the Government Island Complex taken
North
Location
from DMD-SD-03 Sample Location.
2.76 NM east of
18
ODEQ GPS
View of the 1-205 Bridge taken from DMD-SD-03
West
Location
Sample Location.
2.76 NM east of
19
ODEQ GPS
Zoomed in view of the 1-205 Bridge taken from
West
Location
DMD-SD-03 Sample Location.
1.25 NM east of
20
ODEQ GPS
View of the 1-205 Bridge taken from DMD-SD-02
West
Location
Sample Location.
1.25 NM east of
21
ODEQ GPS
View of the Portland Shore taken from DMD-SD-02
South
Location
Sample Location.
1.25 NM east of
22
ODEQ GPS
View of a possible outfall located on the Portland
South
Location
Shore taken from DMD-SD-02 Sample Location.
1.25 NM east of
23
ODEQ GPS
View of a possible outfall located on the Portland
Southeast
Location
Shore.
500 feet east of
24
ODEQ GPS
View of EPA Dive Team Preparing a diver to enter
West
Location
the water at first Diver Drum Survey Location.
500 feet east of
25
ODEQ GPS
View of Portland Shore taken from the first Diver
South
Location
Drum Survey Location.
500 feet east of
26
ODEQ GPS
View of the Government Island Complex taken
North
Location
from the first Diver Drum Survey Location.
500 feet east of
Full extent Zoom view of an unknown vehicle
27
Southeast
ODEQ GPS
Location
spraying an unknown liquid along the Portland
Shore from the first diver survey location
500 feet east of
Medium extent Zoom view of an unknown vehicle
28
Southeast
ODEQ GPS
Location
spraying an unknown liquid along the Portland
Shore taken from the first diver survey location
500 feet east of
View of an unknown vehicle spraying an unknown
29
ODEQ GPS
liquid along the Portland Shore taken from the first
Southeast
Location
diver survey location
30
ODEQ GPS
View of the Columbia River west of DMD-SD-07
West
Location
and DMD-SD-08 Sample Locations.
2
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Pholo
Dnvclion
Sik- l.ociilion
IX'scriplmn
\umlvr
I'aci nu
31
ODEQ GPS
View of Portland shore taken from DMD-SD-07
South
Location
and DMD-SD-08 Sample Locations.
View of the Government Island Complex taken
32
ODEQ GPS
from DMD-SD-07 and DMD-SD-08 Sample
North
Location
Locations.
33
ODEQ GPS
View of DMD-SD-07 and DMD-SD-08 Samples in
Down
Location
the sample corers.
34
View of EPA Diver Sean Sheldrake uploading the
N/A
N/A
ODEQ site summary photographs.
35
View of EPA Diver Sean Sheldrake uploading the
N/A
N/A
ODEQ site summary photographs.
0.57 NM west of
36
ODEQ GPS
View of Portland Shore taken from DMD-SD-09 to
South
Location
DMD-SD-13 Sample Locations.
0.57 NM west of
View of the Government Island Complex taken
37
ODEQ GPS
from DMD-SD-09 to DMD-SD-13 Sample
North
Location
Locations.
0.57 NM west of
38
ODEQ GPS
View of EPA Diver entering water at DMD-SD-09
West
Location
to DMD-SD-13 Sample Locations.
0.57 NM west of
39
ODEQ GPS
View of DMD-SD-09 Sample located in the sample
Down
Location
corer.
0.48 NM west of
40
ODEQ GPS
View of Portland Shore taken from DMD-SD-14
South
Location
and DMD-SD-15 Sample Locations.
0.48 NM west of
View of the Government Island Complex taken
41
ODEQ GPS
from DMD-SD-14 and DMD-SD-15 Sample
North
Location
Locations.
0.91 NM west of
View of Portland Shore taken from DMD-SD-16,
42
ODEQ GPS
DMD-SD-17, DMD-SD-18, and DMD-SD-28
South
Location
Sample Locations.
0.91 NM west of
View of EPA Diver entering water at DMD-SD-16,
43
ODEQ GPS
DMD-SD-17, DMD-SD-18, and DMD-SD-28
West
Location
Sample Locations.
View of Vancouver Shore and the Government
44
0.91 NM west of
Island Complex taken from DMD-SD-16, DMD-
ODEQ GPS
SD-17, DMD-SD-18, and DMD-SD-28 Sample
North
Location
Locations.
0.74 NM west of
45
ODEQ GPS
View of Portland Shore taken from DMD-SD-19
South
Location
and DMD-SD-20 Sample Locations.
0.74 NM west of
View of the Government Island Complex taken
46
ODEQ GPS
from DMD-SD-19 and DMD-SD-20 Sample
North
Location
Locations.
3
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Pholo
Dnvclion
Sik- l.ociilion
IX'scriplmn
\umlvr
I'aci nu
0.74 NM west of
47
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
19 and DMD-SD-20 Sample Locations.
0.71 NM west of
48
ODEQ GPS
View of Portland Shore taken from DMD-SD-21,
South
Location
DMD-SD-22, and DMD-SD-29 Sample Locations.
0.71 NM west of
View of the Columbia River taken from DMD-SD-
49
ODEQ GPS
21, DMD-SD-22, and DMD-SD-29 Sample
West
Location
Locations.
0.71 NM west of
View of the Government Island Complex taken
50
ODEQ GPS
from DMD-SD-21, DMD-SD-22, and DMD-SD-29
North
Location
Sample Locations.
0.67 NM west of
51
Southwest
ODEQ GPS
Location
View of a tire floating down the Columbia River.
0.67 NM west of
52
ODEQ GPS
View of Portland Shore taken from DMD-SD-23
South
Location
and DMD-SD-24 Sample Locations.
0.67 NM west of
53
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
23 and DMD-SD-24 Sample Locations.
0.67 NM west of
View of the Government Island Complex taken
54
ODEQ GPS
from DMD-SD-23 and DMD-SD-24 Sample
Northwest
Location
Locations.
0.62 NM west of
55
ODEQ GPS
View of Portland Shore taken from DMD-SD-25
South
Location
and DMD-SD-26 Sample Locations.
0.62 NM west of
56
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
25 and DMD-SD-26 Sample Locations.
0.62 NM west of
View of the Government Island Complex taken
57
ODEQ GPS
from DMD-SD-25 and DMD-SD-26 Sample
North
Location
Locations.
0.56 NM west of
58
ODEQ GPS
View of Portland Shore taken from DMD-SD-30
South
Location
and DMD-SD-31 Sample Locations.
0.56 NM west of
59
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
30 and DMD-SD-31 Sample Locations.
0.56 NM west of
View of the Government Island Complex taken
60
ODEQ GPS
from DMD-SD-30 and DMD-SD-31 Sample
North
Location
Locations.
0.2 NM east of
61
South
ODEQ GPS
Location
View of Portland Shore taken from DMD-SD-01.
4
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Pholo
Dnvclion
Sik- l.ocalion
IX'scriplmn
\umlvr
I'aci nu
0.2 NM east of
62
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
01.
0.2 NM east of
63
ODEQ GPS
View of the Government Island Complex taken
North
Location
from DMD-SD-01.
0.2 NM east of
64
ODEQ GPS
East
Location
View of the 1-205 Bridge taken from DMD-SD-01.
0.2 NM east of
65
ODEQ GPS
Location and
South of DMD-
South
SD-01
View of Portland Shore taken from DMD-SD-32.
2.37 NM west of
66
ODEQ GPS
Southeast
Location
First attempt to photograph an Osprey.
2.37 NM west of
67
ODEQ GPS
Zoomed in view of an Osprey Nest located on Mile
South
Location
Marker 16 Post.
2.37 NM west of
68
ODEQ GPS
Zoomed in view of an Osprey in an Osprey Nest
East
Location
located on Mile Marker 16 Post.
2.37 NM west of
69
East
ODEQ GPS
Location
View of old pilings taken from DMD-SD-33.
2.37 NM west of
Zoomed in view of an Osprey in an Osprey Nest
70
ODEQ GPS
located on Mile Marker 16 Post taken from DMD-
Northeast
Location
SD-33.
2.37 NM west of
71
ODEQ GPS
North
Location
View of Vancouver Shore taken from DMD-SD-33.
2.37 NM west of
72
ODEQ GPS
View of the Columbia River taken from DMD-SD-
West
Location
33.
5
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 1. ODEQ GPS Location. Facing
NE. 1250 hours. April 23, 2007.
Photo 2. ODEQ GPS Location marked
by a red flag. Facing NE. 1252 hours.
April 23, 2007.
6
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 3. Approximately half a mile upstream from the ODEQ GPS
Location, measured using the TechLaw, Inc. Suburban Odometer.
Facing NE. 1300 hours. April 23, 2007.
HHHMHMl
Photo 4. Approximately one and a half miles upstream from the ODEQ
GPS Location, measured using the TechLaw, Inc. Suburban odometer.
Facing NE. 1310 hours. April 23, 2007.
7
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 5. Approximately one mile upstream from the ODEQ GPS
Location and location of a storm outfall. Facing NE. 1315 hours.
April 23, 2007.
Photo 6. Approximately One and a half
nautical miles downstream from the
ODEQ GPS Location. Samples DMD-
SD-06 and DMD-SD-27. Facing NE,
1610 hours. April 23, 2007.
8
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 7. Approximately One and a half nautical miles downstream from the
ODEQ GPS Location. Samples DMD-SD-06 and DMD-SD-27. Facing S.
1620 hours. April 23, 2007.
Photo 8. Approximately one nautical mile downstream from the ODEQ GPS
Location. Sample DMD-SD-05. FacingS. 1719 hours. April 23, 2007.
9
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 9. Approximately one nautical mile downstream from the ODEQ GPS
Location. Sample DMD-SD-05. Facing N. 1720 hours. April 23, 2007.
Photo 10. Approximately a half nautical mile downstream from the ODEQ
GPS Location. Sample DMD-SD-04. Facing S. 1810 hours. April 23,
2007.
10
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 11. Approximately a half nautical mile downstream from the ODEQ
GPS Location. Sample DMD-SD-04. Facing N. 1811 hours. April 23,
2007.
Photo 12. Approximately 2.76 nautical miles upstream from the ODEQ GPS
Location at the storm outfall. Facing SW. 0820 hours. April 24, 2007.
11
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 13. Approximately 2.76 nautical miles upstream from the ODEQ GPS
Location at the storm outfall. Facing SW. 0820 hours. April 24, 2007.
Photo 14. Approximately 2.76 nautical miles upstream from the ODEQ GPS
Location slightly downstream from the storm outfall. Sample DMD-SD-03.
Facing SE. 1030 hours. April 24, 2007.
12
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 15. Approximately 2.76 nautical miles upstream from the
ODEQ GPS Location slightly downstream from the storm outfall,
zoomed in to full extent. Sample DMD-SD-03. Facing SE. 1031
hours. April 24, 2007.
¦If.
Photo 16. Approximately 2.76 nautical miles upstream from the
ODEQ GPS Location slightly downstream from the storm outfall.
Sample DMD-SD-03. FacingS. 1032 hours. April 24, 2007.
13
-------
Drums-NE Marine Drive
Site Assessment.
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 17. Approximately 2.76 nautical miles upstream from the ODEQ
GPS Location slightly downstream from the storm outfall. Sample
DMD-SD-03. Facing N. 1033 hours. April 24, 2007.
Photo 18. Approximately 2.76 nautical miles upstream from the ODEQ
GPS Location slightly downstream from the storm outfall. Sample
DMD-SD-03. Facing W. 1034 hours. April 24, 2007.
14
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 19. Approximately 2.76 nautical miles upstream from the ODEQ
GPS Location slightly downstream from the storm outfall. Sample
DMD-SD-03. Facing W. 1035 hours. April 24, 2007.
Photo 20. Approximately 1.25 nautical miles upstream from the ODEQ
GPS Location. Sample DMD-SD-02. Facing W. 1105 hours. April 24,
2007.
15
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 21. Approximately 1.25 nautical miles upstream from the ODEQ
GPS Sample DMD-SD-02. FacingS. 1105 hours. April 24, 2007.
~
Photo 22. Approximately 1.25 nautical miles upstream from the ODEQ
GPS Location, zoomed in to full extent. Sample DMD-SD-02. Facing S.
1105 hours. April 24, 2007.
16
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 23. Approximately 1.25 nautical miles upstream from the ODEQ
GPS Location, slightly downstream from a potential outfall. Facing SE.
1105 hours. April 24, 2007.
^r,
i .
2
1
J
m
A
w Mb
N
Photo 24. Approximately 500 feet upstream from the ODEQ GPS
Location, EPA Divers first drum survey location. Facing W. 1030
hours. April 25, 2007.
17
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 25. Approximately 500 feet upstream from the ODEQ GPS
Location, EPA Divers first drum survey location. Facing S. 1105 hours.
April 25, 2007.
Photo 26. Approximately 500 feet upstream from the ODEQ GPS Location,
EPA Divers first drum survey location. Facing N. 1105 hours. April 25,
2007.
18
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 27. Approximately 500 feet upstream from the ODEQ GPS
Location. Unknown vehicle spraying an unknown liquid along the
Columbia River bank, zoomed into full extent. Facing SE. 1140
hours. April 25, 2007.
Photo 28. Approximately 500 feet upstream from the ODEQ GPS
Location. Unknown vehicle spraying an unknown liquid along the
Columbia River bank, zoomed into medium extent. Facing SE.
1140 hours. April 25, 2007.
19
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 29. Approximately 500 feet upstream from the ODEQ GPS Location.
Unknown vehicle spraying an unknown liquid along the Columbia River
bank. Facing SE. 1140 hours. April 25, 2007.
Photo 30. South of ODEQ GPS Location. Samples DMD-SD-07 and
DMD-SD-08. Facing W. 1209 hours. April 25, 2007.
20
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 31. South of ODEQ GPS Location. Samples DMD-SD-07 and
DMD-SD-08. FacingS. 1209 hours. April 25, 2007.
Photo 32. South of ODEQ GPS Location. Samples DMD-SD-07 and
DMD-SD-08. Facing N. 1209 hours. April 25, 2007.
21
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 33. South of ODEQ GPS Location. Samples DMD-SD-07 and
DMD-SD-08 located in the sample corers, on a rack, on the boat. Facing
SW. 1250 hours. April 25, 2007.
Photo 34. EPA Diver Sean Sheldrake pulling up ODEQ site summary
photographs. 1257 hours. April 25, 2007.
22
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 35. EPA Diver Sean
Sheldrake pulling up ODEQ site
summary photographs. 1257 hours.
April 25, 2007.
Photo 36. Approximately 0.57 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-09, DMD-SD-10, DMD-SD-11,
DMD-SD-12, and DMD-SD-13. Facing S. 1342 hours. April 25, 2007.
23
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
— mi
- ' .
—
Photo 37. Approximately 0.57 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-09, DMD-SD-10, DMD-SD-11,
DMD-SD-12, and DMD-SD-13. Facing N. 1342 hours. April 25, 2007.
Photo 38. Approximately 0.57 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-09, DMD-SD-10, DMD-SD-11,
DMD-SD-12, and DMD-SD-13. Facing W. 1342 hours. April 25,
2007.
24
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 39. Approximately 0.57 nautical miles downstream from ODEQ
GPS Location. Sample DMD-SD-09 in the sample corer. Facing SW.
1342 hours. April 25, 2007.
Photo 40. Approximately 0.48 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-14 and DMD-SD-15. Facing S.
1605 hours. April 25, 2007.
25
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 41. Approximately 0.48 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-14 and DMD-SD-15. Facing M,
1605 hours. April 25, 2007.
Photo 42. Approximately 0.91 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-16, DMD-SD-17, DMD-SD-18, and
DMD-SD-28. FacingS. 0900 hours. April 26, 2007.
26
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 43. Approximately 0.91 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-16, DMD-SD-17. DMD-SD-18, and
DMD-SD-28 Facing W. 0900 hours. April 26, 2007.
Photo 44. Approximately 0.91 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-16, DMD-SD-17, DMD-SD-18, and
DMD-SD-28. Facing N. 0900 hours. April 26, 2007.
27
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 45. Approximately 0.74 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-19 and DMD-SD-20. Facing S.
1120 hours. April 26, 2007.
Photo 46. Approximately 0.74 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-19 and DMD-SD-20. Facing N.
1120 hours. April 26, 2007.
28
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 47. Approximately 0.74 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-19 and DMD-SD-20. Facing W.
1120 hours. April 26, 2007.
Photo 48. Approximately 0.71 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-21, DMD-SD-22, and DMD-SD-29.
FacingS. 1215 hours. April 26, 2007.
29
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 49. Approximately 0.71 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-21 and DMD-SD-22. Facing W.
1215 hours. April 26, 2007.
Photo 50. Approximately 0.71 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-21 and DMD-SD-22. Facing N.
1215 hours. April 26, 2007.
30
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 51. Approximately 0.67 nautical miles downstream from ODEQ GPS
Location. Floating Tire. Facing SW. 1326 hours. April 26, 2007.
Photo 52. Approximately 0.67 nautical miles downstream from ODEQ GPS
Location. Samples DMD-SD-23 and DMD-SD-24. Facing S. 1330 hours.
April 26, 2007.
31
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 53. Approximately 0.67 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-23 and DMD-SD-24. Facing W.
1330 hours. April 26, 2007.
Photo 54. Approximately 0.67 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-23 and DMD-SD-24. Facing NW.
1330 hours. April 26, 2007.
32
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 55. Approximately 0.62 nautical miles downstream from
ODEQ GPS Location showing bikers on the bike path. Samples
DMD-SD-25 and DMD-SD-26. Facing S. 1410 hours. April 26,
2007.
Photo 56. Approximately 0.62 nautical miles downstream from
ODEQ GPS Location showing diver approximately 40 meters
downstream. Samples DMD-SD-25 and DMD-SD-26. Facing W.
1410 hours. April 26, 2007.
33
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 57. Approximately 0.62 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-25 and DMD-SD-26. Facing N.
1410 hours. April 26, 2007.
Photo 58. Approximately 0.56 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-30 and DMD-SD-31. Facing S.
1515 hours. April 26, 2007.
34
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 59. Approximately 0.56 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-30 and DMD-SD-31. Facing W.
1515 hours. April 26, 2007.
Photo 60. Approximately 0.56 nautical miles downstream from ODEQ
GPS Location. Samples DMD-SD-30 and DMD-SD-31. Facing N.
1515 hours. April 26, 2007.
35
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 61. Approximately 0.2 nautical miles upstream from ODEQ GPS
Location. Sample DMD-SD-01, further north from DMD-SD-32.
Facing S. 1550 hours. April 26, 2007.
Photo 62. Approximately 0.2 nautical miles upstream from ODEQ GPS
Location. Sample DMD-SD-01, further north from DMD-SD-32.
Facing W. 1550 hours. April 26, 2007.
36
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 63. Approximately 0.2 nautical miles upstream from ODEQ GPS
Location. Sample DMD-SD-01, further north from DMD-SD-32.
Facing N. 1550 hours. April 26, 2007.
Photo 64. Approximately 0.2 nautical miles upstream from ODEQ GPS
Location. Sample DMD-SD-01, further north from DMD-SD-32.
Facing E. 1550 hours. April 26, 2007.
37
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 65. Approximately 0.2 nautical miles upstream from ODEQ GPS
Location. Sample DMD-SD-32, further south from DMD-SD-01.
FacingS. 1610 hours. April 26, 2007.
Photo 66. Approximately 2.37 nautical miles downstream from ODEQ
GPS Location. Attempted to photograph of an Osprey located mile
marker 16. Facing SE. 0946 hours. April 27, 2007.
38
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 67. Approximately 2.37 nautical miles downstream from ODEQ
GPS Location. An Osprey nest located mile marker 16. FacingS. 0946
hours. April 27, 2007.
Photo 68. Approximately 2.37 nautical miles downstream from ODEQ
GPS Location. An Osprey in its nest located mile marker 16. Facing E.
0946 hours. April 27, 2007.
39
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 69. Approximately 2.37 nautical miles downstream from ODEQ
GPS Location, view of old pilings. Sample DMD-SD-33. Facing E.
0946 hours. April 27, 2007.
Photo 70. Approximately 2.37 nautical miles downstream from ODEQ
GPS Location, zoomed in view of mile marker 16 with an Osprey and an
Osprey nest. Sample DMD-SD-33. Facing NE. 0946 hours. April 27.
2007."
40
-------
Drums-NE Marine Drive
Site Assessment
Photographic Log
April 23 to April 27, 2007
Portland Oregon
Photo 11. Approximately 2.37 nautical miles downstream from ODEQ GPS
Location. Sample DMD-SD-33. Facing N. 0946 hours. April 27, 2007.
Photo 72. Approximately 2.37 nautical miles downstream from ODEQ GPS
Location. Sample DMD-SD-33. Facing W. 0946 hours. April 27, 2007.
41
-------
APPENDIX B
GPS SAMPLE LOCATION DATA
-------
Appendix B
Global Positioning System Coordinates
Sample Locations
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
Garmin Hand
II)
Station II)
CLP II)
CP-1650 1)1-
Garni in 276C
Held 60CS
15 meters west of
15 meters west of
15 meters west of
J86R0
DMD-SD-01
MJ86R0
45.5800, -122.5556
45.5801, -122.5565
45.5800, -122.5556
J86R1
DMD-SD-02
MJ86R1
45.5722, -122.5339
N/A
45.5723,-122.5340
J86R2
DMD-SD-03
MJ86R2
45.5649, -122.5031
N/A
45.5650,-122.5031
J86R3
DMD-SD-04
MJ86R3
45.5882, -122.5678
N/A
45.5882,-122.5678
J86R4
DMD-SD-05
MJ86R4
45.5929, -122.5775
N/A
45.5930,-122.5776
J86R5
DMD-SD-06
MJ86R5
45.5980, -122.5872
N/A
45.5978, - 122.5873
19 meters west of
19 meters west of
19 meters west of
J86R6
DMD-SD-07
MJ86R6
45.5823, -122.5593
45.5823, -122.5593
45.5823, - 122.5593
36 meters west of
36 meters west of
36 meters west of
J86R7
DMD-SD-08
MJ86R7
45.5823, -122.5593
45.5823, -122.5593
45.5823, - 122.5593
10 meters west of
10 meters west of
J86R8
DMD-SD-09
MJ86R8
45.5871, -122.5687
N/A
45.5871, - 122.5687
18 meters west of
18 meters west of
J86R9
DMD-SD-10
MJ86R9
45.5871, -122.5687
N/A
45.5871, - 122.5687
23 meters west of
23 meters west of
J86S0
DMD-SD-11
MJ86S0
45.5871, -122.5687
N/A
45.5871, - 122.5687
37 meters west of
37 meters west of
J86S1
DMD-SD-12
MJ86S1
45.5871, -122.5687
N/A
45.5871, - 122.5687
37 meters west of
37 meters west of and
and slightly south
slightly south of
of DMD-SD-12
DMD-SD-12
J86S2
DMD-SD-13
MJ86S2
45.5871, -122.5687
N/A
45.5871, - 122.5687
Between 9 and 15
Between 9 and 15
meters west of
meters west of
J86S3
DMD-SD-14
MJ86S3
45.5870, -122.5686
N/A
45.5870, -122.5686
18.5 meters west of
18.5 meters west of
J86S4
DMD-SD-15
MJ86S4
45.5870, -122.5686
N/A
45.5870, -122.5686
1
-------
Appendix B
Global Positioning System Coordinates
Sample Locations
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
II)
Station II)
(IP II)
(;i»-l650 1)1-
(iarmin 276C
(iarmin Hand
Held 60CS
J86S5
DMD-SD-16
MJ86S5
50 meters west of
45.5897, -122.5747
N/A
50 meters west of
45.5897, -122.5747
J86S6
DMD-SD-17
MJ86S6
31 meters west of
45.5897, -122.5747
N/A
31 meters west of
45.5897, -122.5747
J86S7
DMD-SD-18
MJ86S7
16 meters west of
45.5897, -122.5747
N/A
16 meters west of
45.5897, -122.5747
J86S8
DMD-SD-19
MJ86S8
44 meters west of
45.5894,-122.5739
N/A
44 meters west of
45.5894, -122.5739
J86S9
DMD-SD-20
MJ86S9
27 meters west of
45.5894,-122.5739
N/A
27 meters west of
45.5894, -122.5739
J86T0
DMD-SD-21
MJ86T0
45 meters west of
45.5890, -122.5731
45 meters west of
45.5890, -122.5731
45 meters west of
45.5891, -122.5731
J86T1
DMD-SD-22
MJ86T1
45 meters west of
45.5890, -122.5731
45 meters west of
45.5890, -122.5731
45 meters west of
45.5891, -122.5731
J86T2
DMD-SD-23
MJ86T2
35 meters west of
45.5887, -122.5722
35 meters west of
45.5887, -122.5722
35 meters west of
45.5887, -122.5722
J86T3
DMD-SD-24
MJ86T3
13 meters west of
45.5887, -122.5722
13 meters west of
45.5887, -122.5722
13 meters west of
45.5887, -122.5722
J86T4
DMD-SD-25
MJ86T4
30 meters west of
45.5883, -122.5714
30 meters west of
45.5883, -122.5714
30 meters west of
45.5883, -122.5714
J86T5
DMD-SD-26
MJ86T5
30 meters west of
45.5883, -122.5714
30 meters west of
45.5883, -122.5714
30 meters west of
45.5883, -122.5714
J86T6
DMD-SD-27
MJ86T6
45.5980, -122.5872
N/A
45.5978, - 122.5873
J86T7
DMD-SD-28
MJ86T7
31 meters west of
45.5897, -122.5747
N/A
31 meters west of
45.5897, -122.5747
J86T8
DMD-SD-29
MJ86T8
45 meters west of
45.5890, -122.5731
45 meters west of
45.5890, -122.5731
45 meters west of
45.5891, -122.5731
2
-------
Appendix B
Global Positioning System Coordinates
Sample Locations
Drums-NE Marine Drive Site
Portland, Multnomah County, Oregon
i:i»a
Sample
(iarmin Hand
II)
Station II)
(IP II)
(;i»-l650 DI-
(iarmin 276C
Held 60CS
29 meters west of
29 meters west of
J86W4
DMD-SD-30
MJ86W4
N/A
45.5876, -122.5702
45.5877, - 122.5702
10 meters west of
10 meters west of
J86W5
DMD-SD-31
MJ86W5
N/A
45.5876, -122.5702
45.5877, - 122.5702
14 meters west of
14 meters west of
J86W6
DMD-SD-32
MJ86W6
45.5800, -122.5558
45.5800, -122.5586
No available satellites
J86W7
DMD-SD-33
MJ86W7
45.5995,-122.6019
N/A
45.5996, - 122.6019
J86W0
DMD-RB-01
MJ86W0
N/A
N/A
N/A
J86W1
DMD-RB-02
MJ86W1
N/A
N/A
N/A
J86W2
DMD-RB-03
MJ86W2
N/A
N/A
N/A
J86W3
DMD-RB-04
MJ86W3
N/A
N/A
N/A
3
-------
APPENDIX C
DATA VALIDATON MEMO AND LABORATORY DATA
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345;
Matrix:
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
(SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Level: (LOW/MED) LOW
% Moisture: 4 0
Lab Sample ID: 7120009015
(g/mL) £_
Lab File ID: NAF04C15
Extraction: (Type) SONC
Decanted: '(Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—r—
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: . (Y/N) Y_
(uL) GPC- Factor: 2.0
pH: 7.4.
Date Analyzed: 05/15/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND .
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
550
0
100-02-7
4-Nitrophenol
550
U
132-64-9
Dibenzofuran
28 0
' U
121-14-2
2,4-Dinitrotoluene
280
U
84-66-2
Diethylphthalate
280
u
86-73-7
Fluorene
, 28 0
u
7005-72-3
4-Ch-lorophenyl-phenylether
280
u
100-01-6
4-Nitroaniline
550
¦¦ u
534-52-1
4,6-Dinitro-2-methylphenol
550
u
86-30-6
N-Nitrosodiphenylamine1 '
280
u
95-94-3
1/-2, 4, 5-Tetrachlorobenzene
.280
u
101-55-3
4-Bromophenyl-phenylether
280
a
118-74-1
Hexachlorobenzene
280
u
1912-24-9
Atrazine
280
u
87-86-5'
Pentachlorophenol
550
u
,85-01-8
Phenanthrene ¦
280
u
120-12-7
Anthracene
280
u
86-74-8
Carbazole
280
u
8 4-7 4-2
Di-n-butylphthalate
28 0
u
206-44-0
Fluoranthene
280
u
129-00-0
Pyrene
280
u
85-68-7
Butylbenzylphthalate
280
u
91-94-1
3,3'-Dichlorobehzidine
280
u
56-55-3
Benzo(a)anthracene
280
u
218-01-9
Chrysene
: 2 8 0
u
117-81-7 .
Bis(2-ethylhexyl)phthalate
45
. J
117-84-0
Di-n-octylphthalate
280
u
205-99-2
Benzo(b)fluoranthene
280
u ¦
207-08-9
Benzo(k)fluoranthene
280
U-
50-32-8
Benzo(a)pyrene
280
u
193-39-5
Indeno(1,2,3-cd)pyrene
280
u
53-70-3
Dibenzo(a,h)anthracene
'280
u
191-24-2
Benzo(g,h,i)perylene
280
u-
58-90-2
2,3,4,6-Tetrachlorophenol
. ' 280
u
1 Cannot be separated from Diphenylamine
Z.'// / /?K3
SOM01.1 (5/20'
33 P
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS' ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA .SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc. »
Lab Code: DATAC ; Case No. : 3634 5- >. Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL I
Sample wt/vol: 30 . 0 (g/mL) g
Contract: EP-W-05-026
No. :
SDG No.: J8 6R0
Lab Sample ID: 7120009015
Lab File ID: NAF04C15
Level: (LOW/MED) LOW
% Moisture :• 4 0
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
~~
Injection Volume: 1.0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7.4
Date Analyzed: 05/15/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg
CAS NUMBER
vCOMPOUND NAME
RT
EST. CONC.
Q
471-43-2
Ethane, 1,l-dichloro-2,2-difluoro-
3.99
440
JN
Unsaturated Hydrocarbon
4.09
120
Jhi
Polycyclic hydrocarbon
19.15
670
jN
Polycyclic hydrocarbon
. 24.71
510
¦
E966796*
Total Alkanes
N/A
,750
j .
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26,
27
28
2 9
30
2EPA-designated Registry Number.
SOM01.1
I5/20$3)1
-------
ID - FORM I SV-1
SEMIVOLATILE.ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6T0
Lab Name: DataChem Laboratories, Inc:
Lab'Code: DATAC Case No.: 36345:
_ - Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009016
(g/mL) q_
Lab File ID: NAB10C16
Level: (LOW/MED) LOW
% Moisture: 3 9
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 5
Injection Volume: 1. 0
(uL) Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6_;_1
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7 ~
Benzaldehyde
280 Q-&
¦3- 0
108-95-2 ¦
Phenol
280
* u
111-44-4
Bis(2-chlproethyl)ether
280
U
95-57-8
2-Chlorophenol
280
U
95-48-7
2-Methyl-phenol
280
U
108-60-1 ¦
2,2'-Oxybis(1-chloropropane)
280
u
98-86-2
Acetophenone
98
J
106-44-5
4-Methylphenol
17.0
"¦ J
621-64-7
N-Nitroso-di-n-propylamine
280
u
67-72-1.
Hexachloroethane
280
U '
98-95-3 ¦'
Nitrobenzene
280
u
78-59-1
Isophorone
280
u
88-75-5
2-Nitrophenol
280
u
105-67-9
2,4-Dimethylphenol
280
u
111-91-1
Bis(2-chloroethoxy)methane
280
u
120-83-2
2,4-Dichlorophenol
280
u
91-20-3
Naphthalene
280
u
106-47-8
4-Chloroaniline
280
u
87-68-3
Hexachlorobutadiene
280
u
105-60-2
Caprolactam
280
¦ u
59-50-7
4-Chloro-3-methylphenol
280
u
91-57-6
2-Methylnaphthalene
280
u
77-47-4
Hexachlorocyclopentadiene
280
U . '
88-06-2
2, 4, 6-Trichlorophenol
280
u
95-95-4
2,4,5-Trichlorophenol
280
u
92-52-4
1,1'-Biphenyl
280
u
91-58-7
2-Chloronaphthalene
280
u
88-74-4
2-Nitroaniline
540
u
131-11-3
Dimethylphthalate
280
u
606-20-2
2, 6-Dinitrotoluene
280
u
208-96-8
Acenaphthylene
280
u
99-09-2
3-Nitroaniline
540
u
83-32-9
Acenaphthene
28 0
u
£>/(
SOM01.1 (5/20'
m
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
¦ J86T8
Lab Name: DataChem Laboratories, Inc; i. Contract: EP-W-05-026
Lab Code: DATAC . Case No. : 3634 5; >¦ Mod. Ref No
Matrix: (SOIL/SED/WATER) SOIL ' ¦ j
SDG No.: J8 6R0
Lab Sample ID: 7120009016
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 39
(g/mL) g_
Lab File ID: NAB10C16
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—f
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6^1 ^
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kq) ug/kg
Q
51-28-5
2,4-Dinitrophenol
540
UJ
100-02-7
¦4-Nitrophenol"
540
U
132-64-9
Dibenzofuran
280
U
121-14-2
2,4-Dinitrotoluene
280
u
84-66-2
Diethylphthalate
280
u
86-73-7
Fluorene
' ¦ 280
u
7005-72-3
4-Chlorophenyl-phenylether
280
u
100-01-6
'4-Nitroaniline
540
u
534-52-1 '
4,6-Dinitro-2-methylphenol
540
u
86-30-6
N-Nitrosodiphenylamine1 ¦
280
u
95-94-3
1,2,4,5-Tetrachlorobenzene
28 0
u
101-55-3
4-Bromophenyl-phenylether
280
u
118-74-1
Hexachlorobenzene
280
u
1912-24-9
Atrazine
280
u
87-86-5
Pentachlorophenol
540
u
85-01-8
Phenanthrene
280
u
120-12-7
Anthracene
280
u
86-74-8 !
Carbazole
280
u
84-74-2
Di-n-butylphthalate
280
u
206-44-0
Fluoranthene
- 10
J
129-00-0
Pyrene
12
J ¦
85-68-7
Butylbenzylphthalate
280
u
91-94-1
3, 3'-Dichlorobenzidine
280
u
56-55-3
Benzo(a)anthracene
280
u
218-01-9
Chrysene '
280
¦ u
117-81-7
Bis (2-ethylhexyl)phthalate
50
J
117-84-0
Di-n-octylphthalate
280
u-
205-99-2
Benzo(b)fluoranthene
280
u
207-08-9
Benzo(k)fluoranthene
280
u
50-32-8
Benzo(a)pyrene
280
u
193-39-5.
Indeno(1,2,3-cd)pyrene
280
u
53-70-3
Dibenzo(a,h)anthracene
280
u
191-24-2
Benzo(g,h,i)perylene
280
u
58-90-2
2,3,4,6-Tetraahlorophenol
280
TJ
¦Cannot be separated from Diphenylamine.
i l"n.
SOM01.1 (5/20'
-------
IK- FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86T8
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 39
Lab Sample ID: 7120009016
(g/mL) £_
Lab File ID: NAB10C16
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
~~f—
Injection Volume: 1.0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC' Factor: 2 . 0
PH: 6.1
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg
CAS NUMBER
,COMPOUND NAME
RT
EST. CONC.
Q
01
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 . 02
560
JN
02
Unsaturated Hydrocarbon
4 . 22
240
JN
03
123-08--0
Benzaldehyde, 4-hydroxy-
7 . 64
180
JN
04
544-63-8
Tetradecanoic acid
11.13
140
JN
05
61886-66-6
3-Eicosyne
12.17
170
JN
06
5129-60-2
Pentadecanoic acid, 14-methyl-, methyl e
12.51
130
JN
07
2416-20-8
Hexadecenoic acid,- Z-ll-
12. 63
260
- JN
08
57-10-3 .
n-Hexadecanoic acid
12 . 77
600
- JN
09
100008-91-0
2'-Methoxy-N-methyl-2-oxo-2-phenylethyla:
13.10
140
JN
10
Unknown aromatic
13.76
190
J(si
11
2529-03-5
1.alpha., 4a.alpha., 8a.beta.-Decehydro-
13. 96
190
JN
12
35599-77-0
Tridecane', 1-iodo-
15.64
370
JN
13
52078-56-5
11-Tricosene
15.69
1-70
JN
14
941-69-5 -
N-Phenylmaleimide
•15. 99
: 130
JN
15
73105-83-6
Methyl 2,8-dimethyltridecanoate
16.09
150
JN
16
Unknown oxyhydrocarbon
16.30
260
JN
17
50838-19-2
2-Propenoic acid, 3-[bis(1,1-dimethyleth
16.50
180
JN
18
Unknown oxyhydrocarbon
16. 87
310
JiM -
19
Unknown oxyhydrocarbon
17 . 09
230
20
111-61-5
Octadecanoic acid, ethyl ester
17.25
150
JN
21
14811-95-1
1,19-Eicosadiene
17-. 59
350
JN
22
72.06-21-5
5-Octadecene, (E)-
18.17
200
JN
23
Polycyclic hydrocarbon
19.18
460
JN
24
100012-93-0
Z-9-Tetradecenal
19. 32
. 250
JN
25
57-88-5
Cholesterol
20. 70
.420
JN
2 6,
83-47-6 '
.gamma.-Sitosterol
23.50
150
JN
27
2435-53-2
3, 5-Cyclohexadiene-l,2-dione, 3,4, 5,6-te
23.70
490
JN
28
6095-82-5
2,4, 6-Trimethylphenyl isothiocyana'te
23.87
120,
JN
29
Polycyclic hydrocarbon
24.58
610
Jh
30
Polycyclic hydrocarbon
24 .78
360
Jtt
E9667962
Total'Alkanes
N/A
1200
J H
!EPA-designated Registry Number.
£>/i i£r
SOMOl.'l (
5/20§£)6
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
Lab Name:.DataChem Laboratories, Inc;. Contract: EP-W-05-026
Lab Code: DATACCase No.: 36345 v Mod. Ref No.: SDG No.: J8 6R0
Matrix: .(SOIL/SED/WATER) SOIL | ¦ - ' Lab Sample ID: 7120009017
Sample wt/vol: 30 . 0 ; (g/mL) q ¦ ¦ Lab File ID: NAB11C17
Level: (LOW/MED) LOW Extraction:. (Type) SONC
% Moisture: 32 Decanted:' (Y/N) N Date Received: 04/30/2007
Concentrated Extract Volume: 500 (uL) Date Extracted: 05/01/2007
—f : :
Injection Volume: 1.0 (uL) GPC Factor: 2.0 Date.-Analyzed: 05/10/2007
, GPC Cleanup: (Y/N).Y pH: 7.8 Dilution Factor: 1.0 ¦
CAS NO.,
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7 '
Benzaldehyde
2 SO-**
¦/(' f.&f SOM01.1 (5/2
EPA SAMPLE NO.
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA' SAMPLE NO.
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-02.6
Lab Code: DATAC ~ Case No.: 36345: v Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level:' (LOW/MED) LOW
% Moisture: 32
Lab Sample ID:.7120009017
(g/mL)
Lab File ID: NAB11C17
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5Q0 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2.0
Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y_
pH:
Dilution Factor: 1.0
CAS NO.
COMPOUND'
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
51-28-5
2,4-Dinitrophenol
.480
UT
100-02-7
4-Nitrophenol
480
u
132-64-9
Dibenzofur-an
250
u
121-14-2
2,4-Dinitrotoluene
250
u
84-66-2
Diethylphthalate
250
u
86-73-7
Fluorene
250
U-.
7005-72-3
4-Chlorophenyl-phenylether
250
u
100-01-6
4-Nitroaniline
480
u
534-52-1
4,6-Dinitro-2-methylphenol
480
u
86-30-6
N-Nitrosodiphenylamine1
250
u
95-94-3
1,2,4,5-Tetrachlorobenzene
250
u
101-55-3
4-Bromophenyl-phenylether
250
u
118-74-1
Hexachlorobenzene
250
u
1912-24-9
Atrazine
250
u
87-86-5
Pentachlorophenol
4 80
u
85-01-8.
Phenanthrene
250
u
120-12-7 ,
Anthracene
¦ 250
u
8 6-7 4-8
Carbazole
250
u
84-74-2
Di-n-butylphthalate
250
u
206-44-0
Fluoranthene
250
u
129-00-0
Pyrene
250
u
85-68-7
Butylbenzylphthalate
250
u
91-94-1
3, 3'-Dichlorobenzidine
250
u
56-55-3
Benzo(a)anthracene . .
250
u
218-01-9
Chrysene
250
u •
117-81-7
Bis(2-ethylhexyl)phthalate
19
J
117-84-0
Di-n-octylphthalate
250
u
205-99-2
Benzo(b)fluoranthene
250
u
207-08-9
Benzo(k)fluoranthene
250
u
50-32-8
Benzo(a)pyrene
250
u
193-39-5
Indeno(1,2,3-cd)pyrene
250
u
53-70-3
Dibenzo(a,h)anthracene
250
u
191-24-2
Benzo(g,h,i)perylene
250
u
58-90-2
2,3,4,6-Tetrachlorophenol
250
u
1Cannot be separated from Diphenylamine
somoi.i (5/2ony)
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS.DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86W4
Lab Name: DataChem Laboratories, Inci.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009017
(g/mL) g_
Lab File ID: NAB11C17
Level: (LOW/MED) LOW
% Moisture: 32
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—t—
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.8
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg•
CAS NUMBER
COMPOUND NAME
RT
EST.¦CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-'
4 . 01
260
JN ¦
Pdlycyclic hydrocarbon
19.18
510
JM
Polycyclic hydrocarbon
24.78
' 440
jM
E9667962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
3.0
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
2 6'
27
28
29
30
2EPA-designated Registry Number.
SOM01.1 (5/20o")
i?f,7
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5
Lab Name: PataChem Laboratories, Inc:
Lab Code: DATAC Case No'. : 36345;
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Mod.
Contract: EP-W-05-026
Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009018
(g/mL)
Lab File'ID: NAB12C18
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—r—
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7\3
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
¦COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7
Benzaldehyde
4-5-
108-95-2
Phenol
270
U
111-44-4
Bis(2~chloroethyl)ether
270
U
95-57-8
2-Chlorophenol .
270
u
95-48-7
2-Methylphenol
270
u
108-60-1
2, 2'-Oxybis(1-chloropropane)
270
u
98-86-2
Acetophenone
. f 51
J
106-44-5
4-Methylphenol
270
" u
621-64-7
N-Nitroso-di-n-propylamine
270
u
67-72-1
Hexachloroethane
270
u
98-95-3
Nitrobenzene
27 0
u
78-59-1
Isophorone
270
u.
88-75-5
2-Nitrophenol
270
u
105-67-9
2, 4-Dimethylphenol
27 0
u
111-91-1
Bis(2-chloroethoxy)methane
¦ 270
u
120-83-2
2,4-Dichlorophenol
270
u
91-20-3 ' '
Naphthalene'
270
¦ u
106-47-8
4-Chloroaniline
270
u
87-68-3
Hexachlorobutadiene
270
u
105-60-2
Caprolactam
27 0
u
'59-50-7
4-Chloro-3-methylphenol
270
u
91-57-6
2-Methylnaphthalene
270
¦ u
77-47-4
Hexachlorocyclopentadiene
270
¦ u
•88-06-2
2, 4,'6-Trichlorophenol
27 0
u
95-95-4
2,4,5-Trichlorophenol
270
u
92-52-4
1, 1'-Biphenyl'
270
' u
91-58-7
2-Chloronaphthalene
270
u
88-74-4
2-Nitroaniline
520
u
131-11-3
Dimethylphthalate
270
u
606-20-2
2,6-Dinitrotoluene
270
u
208-96-8
Acenaphthylene
270
u
99-09-2
3-Nitroaniline
520
u
83-32-9
Acenaphthene
270
u
SOM01.1 (5 / 2 0*0 5)'
m
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5
Lab Name: DataChem Laboratories, Inc:.
Lab Code: DATAC .Case No.: 36345
Contract: EP-W-05-02'6
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 36
Lab Sample ID: 7120009018
(g/mL) g_
Lab File ID: NAB12C18
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
¦ pH: 7.3 .
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
51-28-5
2,4-Dinitrophenol
520
UX
100-02-7
4-Nitrophenol
520
u
132-64-9
Dibenzofuran
270
u
121-14-2
2,4-Dinitrotoluene
.270
u
84-66-2
Diethylphthalate
270
u
86-73-7
Fluorene
270
u
7005-72-3
4-Chlorophenyl-phenylether
270
u
100-01-6
4-Nitroaniline
520
" u
534-52-1
4,6-Dinitro-2-methylphenol
520
u
86-30-6
N-Nitrosodiphenylamine1
270
u
95-94-3
1,2,4,5-Tetrachlorobenzene
270
. u
101-55-3
4-Bromophenyl-phenylether
27 0
u
118-74-1
Hexachlorobenzene
270
u
1912-24-9
Atrazine
270
u
87-86-5
Pentachlorophenol
520
u
85-01-8
Phenanthrene
270
u
120-12-7
Anthracene
270
u
86-74-8
Carbazole
¦ 270
u
84-74-2
Di-n-butylphthalate
270
u
206-44-0
Fluoranthene
270
u
129-00-0 .•
Pyrene
270
u -
85-68-7
Butylbenzylphthalate
270
u
91-94-1
3, 3'-Dichlorobenzidine
270
u
56-55-3
Benzo(a)anthracene
270
u
218-01-9
Chrysene
270
u
117-81-7
\
Bis(2-ethylhexyl)phthalate
23
J
117-84-0
Di-n-octylphthalate
270
u
205-99-2
Benzo(b)fluoranthene
270
u
207-08-9
Benzo(k)fluoranthene
270
u
50-32-8
Benzo(a)pyrene
270
u
193-39-5
Indeno(1,2,3-cd)pyrene
270
u
53-70-3
Dibenzo(a,h)anthracene
• 270
u
191-24-2
Benzo(g,h,i)perylene
270
u
58-90-2
2,3,4,6-Tetrachlorophenol
270
u
1 Cannot be separated from Diphenylamine
sm01'1 <5/20'
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS .
EPA SAMPLE NO.
J86W5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 3634 5. y Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL , 1
Sample wt/vol: 30.0 (g/mL) g
Contract: EP-W-05-026
No. :
SDG No.: J8 6R0
Lab Sample ID: 7120009018
Lab File ID: NAB12C18
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) S.ONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5Q0 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y_
pH: 7 . 3
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.01
.200
JN
Polycyclic hydrocarbon
19.17
610
JN
Polycyclic hydrocarbon
24.76
500
1
E9667 962
Total Alkanes
N/A
290
J
01
02
03
0-4
05
06
. 07
08
0 9
10
' 11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26'
27
28
29
30
?EPA-designated Registry Number.
(\\/cR
SOM01.1 (5/20'
m
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W6
Lab Name: DataChem Laboratories, Inc; i.
Lab Code: DATAC Case No.: 36345: I;
Matrix: (SOIL/SED/WATER) SOIL j
Sample wt/vol: 30 . 0
Mod.
Contract: EP-W-05-026
Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 712.0009019
(g/mL)
Lab File ID: NAB13C19
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) -Y_
(uL) GPC Factor: 2 . 0
' pH: 1^3
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7
Benzaldehyde '
26a 3-?
T?-U
108-95-2
Phenol
260
u
111-44-4
Bis (2-chloroethyl)ether
260
u
95-57-8
2-Chlorophenol -
260
u
95-48-7
2-Methylphenol
260
u
108-60-1
2,2'-Oxybis(1-chloropropane)
2 60
u
98-86-2
Acetophenone
32
J
106-44-5
4-Methylphenol
21
" J
621-64-7
N-Nitroso-di-n-propylamine
260
u
67-72-1
Hexachloroethane
. 260
u
98-95-3
Nitrobenzene
260
u
¦78-59-1
Isophorone
260
u
88-75-5
2-Nitrophenol
260
u
105-67-9
2,4-Dimethylphenol ' *
260
u
111-91-1
Bis(2-chloroethoxy)methane
260
u
120-83-2
2,4-Dichlorophenol
260
u
91-20-3
Naphthalene
260
U .
106-47-8
4-Chloroaniline
260
U
87-68-3
Hexachlorobutadiene >
260
U
105-60-2
Caprolactam
260
u
59-50-7
4-Chioro-3-methylphenol
260
u
91-57-6
2-Methylnaphthalene
260
u
77-47-4
Hexachlorocycl'opentadiene
260
u
88-06-2
2,4,6-Trichlorophenol
260
u
95-95-4
2,4,5-Trichlorophenol
260
U
92-52-4
1,1'-Biphenyl
260
u
91-58-7
2-Chloronaphthalene
260
u
88-74-4
2-Nitroaniline
510
u
131-11-3
Dimethylphthalate-
260
;u
606-20-2
2,6-Dinitrotoluene
260
u
208-96-8
Acenaphthylene
260
u
99-09-2
3-Nitroaniline
510
• u
83-32-9
Acenaphthene
• 260
u
X
£/( (/a?
somoi.i (5/20037
w
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8
Lab Name: DataChem Laboratories, Inc.. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345: >¦ Mod.. Ref No.: SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL , i Lab Sample ID: 7120009019
Sample wt/vol: 30 . 0 (g/mL) g Lab File ID: NAB13C19
Level: (LOW/MED) LOW. . ¦ . Extraction: (Type) SONC
% Moisture:'3jv Decanted: (Y/N) N ¦ Date Received: 04/30/2007 . __
Concentrated Extract Volume: 5Q0 ' (uL) Date Extracted: 05/01/2007 '
Injection Volume: 1.0 (uL) GPC Factor: 2 . 0 Date Analyzed: 05/10/2007
GPC Cleanup: (.Y/N) Y pH:' 7 . 3 . Dilution Factor: 1. 0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
510
UJ"
100-02-7
4-Nitrophenol .
510
u
132-,64-9
Dibenzof-uran
260
u
121-14-2
2, 4-Dinitrotoluene
260
' u
84-66-2
Diethylphthalate
2 60
u
86-73-7
Fluorene
260
u
7005-72-3
4-Chlorophenyl-phenylether
260
u
100-01-6
4-Nitroaniline
510
u
534-52-1
4,6-Dinitro-2-methylphenol
510
u
86-30-6'
N-Nitrosodiphenylamine1
260
u
95-94-3
1,2,4,5-Tetrachlorobenzene
260
u
101-55-3
4-Bromophenyl-phenylether
260
u
118-74-1
Hexachlorobenzene
260
u
1912-24-9
Atrazine
260
u
87-86-5
Pentachlorophenol
510
u
85-01-8
Phenanthrene
2 60
u
120-12-7
Anthracene
260
u
86-74-8
Carbazole
260
u '
84-74-2
Di-n-butylphthalate
260
u
206-44-0
Fluoranthene
260
u
129-00-0
Pyrene
260
u
85-68-7
Butylbenzylphthalate
260
u
91-94-1 •
3,3'-Dichlorobenzidine
260
u
56-55-3
Benzo(a)anthracene
260
u
218-01-9
C-hrysene
260
U -
117-81-7
Bis(2-ethylhexyl)phthalate
28
J
117-84-0
Di-n-octylphthalate
2 60
U
205-99-2 .
Benzo(b)fluoranthene
260
u
207-08-9
Benzo(k)fluoranthene
260
u
50-32-8
Benzo(a)pyrene
260
u
193-39-5
Indeno(1,2,3-cd)pyrene
260
u
53-7 0-3
Dibenzo(a,h)anthracene
260
u
191-24-2
Benzo(g,h,i)perylene
2 60
u
58-90-2 .
2,3,4,6-Tetrachlorophenol
260
u
1 Cannot be separated from Diphenylamine
£l/l,/3=? SOM01.1 (5/2cftSP
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-02
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Lab Sample ID: 71200090.19
(g/mL)
Lab File ID: NAB13C19
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N.)
(uL) GPC Factor: 2 . 0
pH: 7_i3
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 . 01
¦ 210
JN
Uriknown aromatic
7 .18
120
¦
Polycyclic hydrocarbon
19.16
670
JN
Polycyclic hydrocarbon
24 .75
4 9.0
E9667 96 2
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
¦ 16
17
18
19
20
21
22
23
24
25
2 6-
27
28
29
30
!EPA-designated Registry Number.
/S.
(I /ci
SOM01.1 (5/20
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345.
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 19
Lab Sample ID: 7120009001
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A023,21070514B023
Date Received: 04/30/2007 " __
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date- Analyzed: 05/15/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7V4
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) IL
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or.ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.1
u
319-85-7
beta-BHC
2.1
u
319-86-8
delta-BHC
2.1
u
58-89-9
gamma-BHC (Lindane)
<2.1
tfPU'
76-44-8
Heptachlor
2.1
u
309-00-2
Aldrin
2.1
u
1024-57-3
Heptachlor epoxide
2.1
u
959-98-8
Endosulfan I
2.1
u
60-57-1
Dieldrin
4.1
u
72-55-9
4,4'-DDE
4,1 9.042
cfPLi
72-20-8
Endrin
4.1
U
33213-65-9
Endosulfan II
4.1
U
72-54-8
4,4'-DDD
4.1
U
1031-07-8
Endosulfan sulfate
4.1
U
50-29-3
4,4'-DDT
4.1
U
72-43-5
Methoxychlor
0.46
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde
'4.1
u
5103-71-9
alpha-Chlordane
2.1
u
5103-74-2
gamma-Chlordane
'2.1
u
8001-35-2
Toxaphene
210
u
SOM01.1 (5/2®®7
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET'
EPA SAMPLE NO.
J86S5
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DAT AC Case No. : 3 6345: Mod. Ref No. : ' SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ! Lab Sample ID: 7120009002
Sample wt/vol; 30.0 (g/mL) g . Lab File ID: 21070514A024, 21070514B024
% Moisture: 19 Decanted: (Y/N) N_ Date Received: 04/30/2007 :
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 ___ (uL) Date Analyzed: 05/15/2007
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 6.5 Sulfur Cleanup: (Y/N) r^_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kq) ug/kg
Q
319-84-6
alpha-BHC
2.1
U
319-85-7
beta-BHC
2.1
u.
319-86-8
delta-BHC
2.1
u
58-89-9
gamma-BHC (Lindane)
2J 0.064
J-Pd
76-44-8
Heptachlor
. 2.1
U
309-00-2
Aldrin
2.1
U
1024-57-3
Heptachlor epoxide
2.1
U
959-98-8
Endosulfan I
' 2.1
U
60-57-1
Dieldrin
1 0 rQ!}4
cfPLi
72-55-9
4,4'-DDE
,4J ¦0-r-3r2*
cfPci
72-20-8
Endrin
4.1
U
33213-65-9
Endosulfan II
4.1
u
72-54-8
4,41 -DDD
^4: ( &. 0 80
Jf u
1031-07-8
Endosulfan sulfate
4.1
u
50-29-3
4,4'-DDT
1 0". 2 6
ifp'Li
72-43-5
Methoxychlor
0.27
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde
-4.1
u
5103-71-9
alpha-Chlordane
2.1
u
5103-74-2
gamma-Chlordane
2,1 Q-r&rt
jpU
8001-35-2
Toxaphene
210
u
fyf'X/b}
SOM01.1 (5/2(5®0
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories,- Inc.
1 1 j—
Lab Code: DATAC Case No.: 363451
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 38
Lab Sample ID: 7120009003
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 21070514A025,21070514B025
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date Analyzed: 05/15/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6.8
Dilution Factor: 1. 0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/'kg) ug/kg
Q
319-84-6 '
alpha-BHC
2.7
u
319-85-7
beta-BHC
2.7
u
319-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane)
2^ &T-0W
jpU
76-44-8
Heptachlor
2,1- &-r2-e
cfPU
309-00-2
Aldrin
2.7
,u
1024-57-3
Heptachlor epoxide
2.7
u
959-98-8
Endosulfan I
2.7
u.
60-57-1
Dieldrin
5.3
u
72-55-9
4,4'-DDE
5,3 frreee
72-20-8
Endrin
5.3
u
33213-65-9
Endosulfan II
S3 frr&W
72-54-8
4,4'-DDD
5.3
u
1031-07-8
Endosulfan sulfate
5.3
u
50-29-3
4,4.'-DDT
S.3 0^-34
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345 Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ; Lab Sample ID: 7120009004
Sample wt/vol: 3 0.0 (g/mL) g Lab File ID: 21070514A026,21070514B026
% Moisture: 30 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
t
Injection Volume: 2.0 (uL) GPC Factor: 2 .0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 6.9 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.4
U
319-85-7 .
beta-BHC
2.4
u
319-86-8
delta-BHC
2.4
u
58-89-9
gamma-BHC (Lindane)
2.4
u
76-44-8
Heptachlor
2.4
u
309-00-2
Aldrin
2.4
u
1024-57-3
Heptachlor epoxide
2.4
u
959-98-8
Endosulfan I
2.4
- u
60-57-1
Dieldrin
4.7
u
72-55-9
4,4'-DDE
4.7
u
72-20-8
Endrin
4.7
u
33213-65-9
Endosulfan II
4.7
u
72-54-8
4,4'-DDD
4.7
u
1031-07-8
Endosulfan sulfate
4.7
u
50-29-3
4,4'-DDT
4.7
u
72-43-5
Methoxychlor
24
u
53494-70-5
Endrin ketone
4.7
u
7421-93-4
Endrin aldehyde
,4.7
u
5103-71-9
alpha-Chlordane
2.4
u
5103-74-2
gamma-Chlordane
2,4 Q-rQ*r4r
(J
8001-35-2
Toxaphene
240
u
C(t2-Jcq
SOM01.1 (5/2(gg6
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S8
Lab Name: DataChem Laboratories , Inc .. Contract: EP-W-05-026 ¦
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' i Lab Sample ID: 7120009005 /
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 21070514A027,21070514B027
% Moisture: 29 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/.2007 .
Injection Volume: 2.0 (uL) GPC Factor: 2 .0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 5.3 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kq) uq/kq
Q
319-84-6
alpha-BHC
2.4
u
319-85-7
beta-BHC
2,4 e-rw
•jp u
319-86-8
delta-BHC
2.4
u.
58-89-9
gamma-BHC (Lindane)
2.4
u
76-44-8
Heptachlor
.2.4
u
309-00-2
Aldrin
2.4
u
1024-57-3
Heptachlor epoxide
0.12
J
959-98-8
Endosulfan I
2.4
u
60-57-1
Dieldrin
4.7
u
72-55-9
4,4'-DDE
1.1
J
72-20-8
Endrin
4.7
u
33213-65-9
Endosulfan II
4,:f&rW9
¦»()
72-54-8
4,4'-DDD
1031-07-8
Endosulfan sulfate
4.7
u
50-29-3
4,4'-DDT
41-
jp d
72-43-5
Methoxychlor
0.63
J
53494-70-5
Endrin ketone
4.7
u
7421-93-4
Endrin aldehyde
4.7
u
5103-71-9
alpha-Chlordane
2.4
u
5103-74-2
gamma-Chlordane
2v4 0^6
ifPU
8001-35-2
Toxaphene
240
u
SOM01.1 (5/2 6(859
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026 ¦
Lab Code: DATAC Case No. : 3634:5: Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ! Lab Sample ID: 7120009006
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 2107 0514A028, 21070514B02 8
% Moisture: 19 . Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2.0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 6_J5 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:.
(ua/L or uq/kq) uq/kq
Q
319-84-6
alpha-BHC
2.1
U
319-85-7
beta-BHC
2.1
U
319-86-8
delta-BHC
2.1
U
58-89-9
gamma-BHC (Lindane)
2.1
U
76-44-8
Heptachlor
2.1
U
309-00-2
Aldrin
2.1
U
1024-57-3
Heptachlor epoxide
2.1
U
959-98-8
Endosulfan I .
2 .1
u
60-57-1
Dieldrin
4.1
u
72-55-9
4,4'-DDE
4.1
u
72-20-8
Endrin
4.1
' u
33213-65-9
Endosulfan II
4.1
u
72-54-8
4,4'-DDD
4.1
u
1031-07-8
Endosulfan sulfate
4.1
u
50-29-3
4,4'-DDT x
4.1
u
72-43-5
Methoxychlor
0.44
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde
-4.1
u
5103-71-9
alpha-Chlordane
2.1
u
5103-74-2
gamma-Chlordane
. 0.066
J/
8001-35-2
Toxaphene
210
u
SOM01.1 ,(5/25(&2
-------
1G - FORM I PEST
PESTICIDE ORGANICS.ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T0
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-Q5-026
Lab Code: DATAC Case No. : 3634$ Mod. Ref No. : - SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ; Lab Sample ID: 7120009007
Sample wt/vol: 30.0 (g/mL) g ¦ Lab File ID: 21070514A029,21070514B029
% Moisture: 40 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC ; Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
. p - .
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 5.9 Sulfur Cleanup: (Y/N) N _____
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.8
u
319-85-7
beta-BHC
"2,8 8-. 13-
tjp Lj
319-86-8
della-BHC
2.8
U
58-89-9
gamma-BHC (Lindane)
2.8
U
76-44-8
Heptachlor
2.8
U
309-00-2
Aldrin
2.8
U
1024-57-3
Heptachlor epoxide
2.8
u
959-98-8
Endosulfan I
2.8
u
60-57-1
Dieldrin
5"«Ser3r0
(J
72-55-9
4,4'-DDE
1.2
J/
72-20-8
Endrin
5.5
u
33213-65-9
Endosulfan II
0.42
J?'
72-54-8
4,4'-DDD
i?p-U
1031-07-8
Endosulfan sulfate
0.34-
. Ji
50-29-3
4., 4"-DDT
S,5o-r&5
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc,
Lab Code: DATAC Case No. : 3634$
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 33
Lab Sample ID: 7120009010
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A032,21070514B032
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date Analyzed: 05/15/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7^0
Dilution Factor; 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND . ,
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.5
U
319-85-7
beta-BHC
2.5
U
319-86-8
delta-BHC
2.5
U
58-89-9
gamma-BHC (Lindane)
2.5
u
76-44-8
Heptachlor
2.5
u
309-00-2
Aldrin .
2.5
u
1024-57-3
Heptachlor epoxide
.2.5
u. .
959-98-8
Endosulfan I
2.5
u
60-57-1
Dieldrin
0.21
J /
72-55-9
4,4'-DDE
<4-, <3 0T2-4-
tfp u
72-20-8
Endrin
4.9
u
33213-65-9
Endosulfan II
4.^ 0-r-©s3
ifp«J
72-54-8
4,4'-DDD
Q-r3r4
tfPU
1031-07-8
Endosulfan sulfate
4.9
u
50-29-3
4,4'-DDT
4,^
U
72-43-5
Methoxychlor
1.6
jjf
53494-70-5
Endrin ketone
4.9
u
7421-93-4
Endrin aldehyde
•4.9
. u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2
gamma-Chlordane
2, 5" 0-r±i
¦39 (J
8001-35-2 .
Toxaphene
250
u
SOM01.1 (5/2
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA.SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories , Inc , Contract: EP-W-05-026 .
Lab Code: DATAC Case No.: 36345; Mod. Ref No.: - SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ;¦ ' Lab Sample ID: 7120009011
Sample wt/vol: 30.0 (g/mL) g Lab File ID: 21070514A033,21070514B033
% Moisture: 36 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7 .1 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.6
,u
319-85-7
beta-BHC
2.6
u
319-86-8
delta-BHC
2.6
u
58-89-9
gamma-BHC (Lindane)
2.6
u
76-44-8
Heptachlor
2.6
u
309-00-2
Aldrin
2.6
u
1024-57-3
Heptachlor epoxide
2.6
u
959-98-8
Endosulfan I
2.6
u
60-57-1 ..
Dieldrin
0.18
jf
72-55-9 '
4,4'-DDE
S, 1 0T±1.
72-20-8
Endrin
5.1
u
33213-65-9
Endosulfan II
0.14
J
72-54-8
4,4'-DDD
5 .1
u
1031-07-8
Endosulfan sulfate
5.1
u
50-29-3
4,4'-DDT
s,t 0^
jp u
72-43-5
Methoxychlor
0.77
J/
53494-70-5
Endrin ketone
5.1
u
7421-93-4
Endrin aldehyde
¦5.1
u
5103-71-9
alpha-Chlordane
2.6
u
5103-74-2
gamma-Chlordane
2^0-^0-
t»(J
8001-35-2
Toxaphene
260
u
£ /rz/si
SOM01.1 (5 / 2 5®1
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories, Inc Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345: Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' i Lab Sample ID: 7120009012 __
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 21070514A034,21070514B034
% Moisture: 37 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
> ¦ f
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7_J3 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kg) ug/kg
. Q
319-84-6
alpha-BHC
2.7
U
319-85-7
beta-BHC
2.7
U
319-86-8
delta-BHC
2.7
U
58-89-9
gamma-BHC (Lindane)
"23- 0.057'
.JP u
76-44-8
Heptachlor
- 2.7
U
309-00-2
Aldrin
2.7
U
1024-57-3
Heptachlor epoxide
2 .7
U
959-98-8
Endosulfan I
2.7
U
60-57-1
Dieldrin
5.2
U
72-55-9
4,4'-DDE
5.2
u
72-20-8
Endrin
5.2
U
33213-65-9
Endosulfan- II
5.2
u
72-54-8
4,4'-DDD
5.2
u
1031-07-8
Endosulfan sulfate
5.2
u
50-29-3
4,4'-DDT
5.2
U '
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5.2
u
7421-93-4
Endrin aldehyde
-5.2
u
5103-71-9
alpha-Chlordane
.2.7
u
5103-74-2
gamma-Chlordane
2.1- e-rt*
tSP-U
8001-3 5-2
Toxaphene
270
u
SOM01.1 (5/2C&S4
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories , Inc .
Lab Code: DATAC Case No. : 3 6345
. Contract: EP-W-05-026
Mod. Ref No. :
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 32
Lab Sample ID: 7120009013
(g/mL) g_
Decanted:.(Y/N) N
Lab File ID: 21070514A035,21070514B03 5
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date Analyzed: 05/15/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6.8
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.5
u
319-85-7
beta-BHC
2.5
u
319-86-8
delta-BHC
2.5
u
58-89-9
gairima-BHC (Lindane)
2.5
u
76-44-8
Heptachlor
2.5
u
309-00-2
Aldrin
2.5
u
1024-57-3
Heptachlor epoxide
2.5
u
959-98-8
Endosulfan I
2.5
u
60-57-1
Dieldrin
4.9
u
72-55-9
4,4'-DDE
4,^ e-r^e
72-20-8
Endrin
4.9
u
33213-65-9
Endosulfan II
4.9
u
72-54-8
4,4' -DDD '•
Iff.(J
1031-07-8
Endosulfan sulfate
4.9
u
50-29-3
4,4' -DDT
4.9
u
72-43-5
MetHoxychlor
0.61
J/
53494-70-5
Endrin ketone
4.9
u
7421-93-4
Endrin aldehyde
•4.9
u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2
gamma-Chlordane
2,5" 9-r-&&5
Jjpti
8001-35-2
Toxaphene
250
u
SOM01.1
(5/2
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc , Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345; Mod. Ref No.: _____ SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL i Lab Sample ID: 712.0009014
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 21070514A03 6,21070514B036
% Moisture: 23 Decanted: (Y/N) N Date Received: 04/30/2007 ____
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7 . 5 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
319-84-6
alpha-BHC
2.2
. U
319-85-7
beta-BHC
2.2
u
319-86-8
delta-BHC
2 .2
u
58-89-9
gamma-BHC (Lindane)
2.2
u.
76-44-8
Heptachlor > ' ,
2.2
u.
309-00-2
Aldrin
2.2
u
1024-57-3
Heptachlor epoxide
2.2
u
959-98-8
Endosulfan I
2.2
u
60-57-1
Dieldrin
0.054
J/
72-55-9
4,4'-DDE
TfP'U
72-20-8
Endrin
~ 4.3
u
33213-65-9
Endosulfan II
4.3
u
72-54-8
4,4'-DDD
0.14
J
1031-07-8
Endosulfan sulfate
4.3.
u
50-29-3
4,4'-DDT
t»U
72-43-5
Methoxychlor
ZZe~r35
53494-70-5
Endrin ketone
4.3
u
7421-93-4
Endrin aldehyde
. '4 .3
u
5103-71-9
alpha-Chlordane
2.2
u
5103-74-2
gamma-Chlordane
0. 062'
iJ/
8001-35-2
Toxaphene
220
u
SOM01.1 (5/2 ©60
EPA SAMPLE NO.
J86T5
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ;
Sample wt/vol: 30.0 (g/mL) cr
I
% Moisture: 40 Decanted: (Y/N) N_
Lab Sample ID: 7120009015
Lab File ID: 21070514A037,21070514B037
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date Analyzed: 05/15/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7.4
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ucr/kq) uq/kq
Q
319-84-6
alpha-BHC
2.8
U
319-85-7
beta-BHC
2.8
u-
319-86-8..
delta-BHC ,
2.8
u
58-89-9
gamma-BHC (Lindane)
Z 3 067
ifPL!
76-44-8
Heptachlor.
2.8
u
309-00-2
Aldrin
2.8
u
1024-57-3
Heptachlor epoxide
2,8 B~r24
:
959-98-8
Endosulfan I
-
TfP U
60-57-1
Dieldrin
5.5
u
72-55-9
4,4'-DDE
1.3
j/
-J
to
1
O
1
CD
Endrin
0.30
j
33213-65-9
Endosulfan II
<5,5"
jp (j
72-54-8
4,4'-DDD
5.5
u
1031-07-8
Endosulfan sulfate '
5.5
u
50-29-3
4,4'-DDT
2.8
j
72-43-5
Methoxychlor
28
u
53494-70-5
Endrin ketone
5.5
u
7421-93-4
Endrin aldehyde
•5.5
u
5103-71-9
alpha-Chlordane
2.8
u
5103-74-2
gamma-Chlordane
2.8
u
8001-35-2
Toxaphene
280
u
SOM01.1 (5/2C&63
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
1 r —
Lab Code: DATAC Case No. : 3 6345 Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL . ' ' Lab Sample ID: 7120009016 -
Sample wt/vol: 30,0 (g/mL) g Lab File ID: 21070514A038, 21070514B03 8
% Moisture: 39 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC ¦ Date Extracted: 05/01/2007
Concentrated Extract Volume: ,10000 (uL) Date Analyzed: 05/15/2007
f 1 .
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 6.1 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.8
u
319-85-7
beta-BHC
0.37
j
319-86-8
delta-BHC
2 . 8
u
58-89-9
gamma-BHC (Lindane)
2.8
u
76-44-8
Heptachlor
2.8
u
309-00-2
Aldrin
2.8
u
1024-57-3
Heptachlor epoxide
2.8
u
959-98-8
Endosulfan I
2.8
u
60-57-1
Dieldrin
0.39
J
72-55-9
4,4'-DDE
1.1
J
72-20-8
Endrin
5.4
u
33213-65-9
Endosulfan II
JP u
72-54-8
4,4'-DDD
S.4- 0-r^
•tJP (J
1031-07-8
Endosulfan sulfate
5.4
u
50-29-3
4,4'-DDT
VS:4 9^^
JPU
72-43-5
Methoxychlor
.(J
53494-70-5
Endrin ketone
5.4
u
7421-93-4
Endrin aldehyde
.5.4
• u ' . .
5103-71-9
alpha-Chlordane
2.8
u
5103-74-2
gamma-Chlordane
2,Sr 0^6
•JPU
8001-35-2
Toxaphene
280
u
SOM01.1 (5/2®6©
EPA.SAMPLE NO.
J86T8
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W4
Lab Name: DataChem Laboratories , Inc < Contract: EP-W-05-026 '
Lab Code: DATAC . Case No. : 36345: Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL I Lab Sample ID: 7120009017
Sample wt/vol: 30 . 0 (g/mL) g Lab File ID: 21070514A039, 21070514B039
% Moisture: 32 Decanted: (Y/N) N . Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: ,10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2. 0 (uL) GPC Factor: 2 .0 Dilution Factor: 1.0
GPC Cleanup: . (Y/N) Y pH: 7^8 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.5
U
319-85-7
beta-BHC
2.5
U
319-86-8
delta-BHC
2.5
U
58-89-9
gamma-BHC (Lindane)
2.5
u
76-44-8
Heptachlor
2.5
u
309-00-2
Aldrin
2.5
u
1024-57-3
Heptachlor epoxide
2.5
u
959-98-8
Endosulfan I
2.5
u
60-57-1
Dieldrin
4.8
u
72-55-9
4,4'-DDE
4.8
u
72-20-8
Endrin
4.8
u
33213-65-9
Endosulfan II
' 4.8
u
72-54-8
4,4'-DDD
4.8
u .
1031-07-8
Endosulfan sulfate
4.8
u
50-29-3
4,4'-DDT
4.8
u
72-43-5
Methoxychlor
0.44
J/
53494-70-5
Endrin ketone
4. 8
u
7421-93-4
Endrin aldehyde
•4.8
u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2
gamma-Chlordane
2,5" W4
is? U
8001-35-2
Toxaphene
2 50
u
V,
SOM01.1 (5/2(£c69
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5
Lab Name: DataChem Laboratories, Inc; Contract: EP-W-05-026
Lab Code: DATAC Case No.: 3 6345:. Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL I Lab Sample ID: 7120009018
Sample wt/vol: 30.0 (g/mL) g • Lab File ID: 21070514A040, 21070514B040
% Moisture: 36 Decanted: (Y/N) N Date Received: 04/30/2007 ¦
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: ,10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7^3 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.7
u
319-85-7
beta-BHC
2.7
u
319-8,6-8
delta-BKC
2.7
u
58-89-9
gamma-BHC (Lindane)
2.7
u
76-44-8 '
Heptachlor ,
2.7
u
309-00-2
Aldrin
r
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5RX
Lab Name: DataChem Laboratories, Inc,
Lab.Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 3 6_
Lab Sample ID: 7120009018RX
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070517A020,21070517B020
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/14/2007
Concentrated Extract Volume: jLOOOO
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
(uL) Date Analyzed: 05/18/2007
Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y_
pH: 7.3
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ucf/kg) ug/kg
Q
319-84-6
alpha-BHC
2.7
U
319-85-7
beta-BHC
2.7
U
31S-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane)
2.7
u
76-44-8
Heptachlor
2.7
u
309-00-2
Aldrin
2.7
u
1024-57-3
Heptachlor epoxide
2.7
u
959-98-8
Endosulfan I
2.7
u
60-57-1
Dieldrin
5.2
u
72-55-9
4,4'-DDE
5.2
u .
72-20-8
Endrin
5.2
u
33213-65-9
Endosulfan II
5.2.
u
72-54-8
4,4'-DDD
5.2
u
1031-07-8
Endosulfan sulfate
5.2
u
50-29-3
4,4'-DDT
5.2
' u.
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5 .2
u
7421-93-4
Endrin aldehyde
•5.2
u
5103-71-9
alpha-Chlordane
2.7
u
5103-74-2
gamma-Ch1ordane
0.066
J
8001-35-2
Toxaphene
270
u
Cfrzjot
SOM01.1 (5/2(8)15
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W6
Lab Name: DataChem Laboratories, Inc.. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 3 6345; Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL i Lab Sample ID: 7120009019 ___
Sample wt/vol: 30.0 (g/mL) g Lab File ID: 21070514A041, 21070514B041
% Moisture: 36 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7.3 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS: -¦
(ug/L or ucr/kg) uq/kcr
Q
319-84-6
alpha-BHC
2.6
u
319-85-7
beta-BHC ¦ - ' '
2.6
u
319-86-8
delta-BHC
2.6
u
58-89-9
gamma-BHC (Lindane)
2.6
jpU
76-44-8
Heptachlor
2.6
u
309-00-2
Aldrin
2.6
u
1024-57-3
Heptachlor epoxide
2.6
u
959-98-8
Endosulfan I
2.6
u
60-57-1
Dieldrin
5.1
¦ u
72-55-9.
4,4'-DDE
5.1
u
72-20-8
Endrin
5.1
u
33213-65-9
Endosulfan II
5.1
u
72-54-8
4,4'-DDD
. 5.1
u
1031-07-8
Endosulfan sulfate
5.1
u
50-29-3
4,4'-DDT
5.1
u
72-43-5
Methoxychlor .
0.37
J/
53494-70-5 .
Endrin ketone
5.1
u
7421-93-4
Endrin aldehyde
•5.1
u
5103-71-9
alpha-Chlordane
2.6
u
5103-74-2
gamma-Chlordane
2.6
u
8001-35-2
Toxaphene
2 60
u
SOM01.1 (5/2 05)13
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc ^ ¦ Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : . SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ; Lab Sample ID: 7120009001 ¦
Sample wt/vol: 30.0 (g/mL) q • Lab File ID: 20070515A03 8, 2 0070515B038
% Moisture: 19 ; Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) 1 Date Analyzed: 05/16/2007
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: T-Jk Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
41
u
11104-28-2
Aroclor-1221
41
u
11141-16-5
Aroclor-1232
41
u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-1262 .
41
u
11100-14-4
Aroclor-1268
41
u
SOM01.1 (5/2(886
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345; Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ; Lab Sample ID: 7120009002
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 20070515A039 ,20070515B039
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume:. 10000 (uL) Date Analyzed: 05/16/2007
f , ¦
Injection Volume: 2.0 (up GPC Factor: 2 . 0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 6.5 Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kg) ug/kg
Q
12674-11-2
Aroclor-1016
41
u
11104-28-2
Aroclor-1221
41
u
11141-16-5
Aroclor-1232
41
u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-1262
41
u
11100-14-4
Aroclor-1268
41
u
6//z/o7
SOM01.1 (5/2(g^9
EPA SAMPLE NO.
J86S5
-------
1H - FORM I ARO .
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories, Inc.,
Lab Code: DATAC Case No', : 36345';
Contract: EP-W-05-026
Mod. Ref No . :
SDG No.: J86R0
(g/mL) g_
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 38 Decanted
Extraction: (Type) SONC
Lab, Sample ID: 7120009003
(Y/N) IL
Lab File ID: 20070515A040,20070515B040
Date Received: 04/30/2007
Date Extracted: 0.5/01/2007
(uL)
Concentrated Extract Volume: 10000
"f - - -
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH; 6J3
Acid Cleanup: (Y/N) Y .
Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS
(uq/L or ua/kcr) ug'/ka
Q
12674-11-2
Aroclor-1016
53
U
11104-28-2
Aroclor-1221
53
U
11141-16-5
Aroclor-1232
53
U
53469-21-9
Aroclor-1242
53
U
12672-29-6
Aroclor-1248
53
U
11097-69-1
Aroclor-1254
53
U
11096-82-5
Aroclor-1260
53
U
37324-23-5
Aroclor-1262
53
u
11100-14-4
Aroclor-1268
53
u
€> /t z/c^f
SOM01.1 (5./2<8f($2
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc..
Lab Code: DATAC Case No.: 3 634'5;
Contract: EP-W-05-026
Mod. Ref No. :
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 30
Lab Sample ID: 7120009004
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 2 0070515A045,20070515B045
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) , Date Analyzed: 05/16/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 6_j_9
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO..
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q.
12674-11-2
Aroclor-1016
47
U
11104-28-2
Aroclor-1221
47
U
11141-16-5
Aroclor-1232
47
U
53469-21-9
Aroclor-1242
47
u
12672-29-6
Aroclor-1248
47
u
11097-69-1
Aroclor-1254
47
u
11096-82-5
Aroclor-1260
47
u
37324-23-5
Aroclor-1262
47
u
11100-14-4
Aroclor-1268
47
u
SOM01.1 (5/28333
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc; Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod.. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL j Lab Sample ID: 7120009005 ¦
Sample wt/vol: 30.0 (g/mL) g • Lab File ID: 20070515A046, 20070515B046
% Moisture: 29 __ Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: ,10 000 (uL) Date Analyzed: 05/16/2007
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 5 . 3 Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
47
U
11104-28-2
Aroclor-1221
47
U
11141-16-5
Aroclor-1232
47
. U
53469-21-9
Aroclor-1242
47
U
12672-29-6
Aroclor-1248
47
u
11097-69-1
Aroclor-1254
47
u
11096-82-5
Aroclor-1260
47
u
37324-23-5
Aroclor-1262
47
u
11100-14-4
Aroclor-1268
47
u
SOM01.1 (5/2®$8
EPA SAMPLE NO.
J86S8
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO..
J86S9
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No. : 3634^
Contract: EP-W-0.5-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 19
(g/mL) g_
Decanted: '(Y/N) N_
Extraction: (Type) SONC
Concentrated Extract Volume:,10000
Injection Volume: 2.0 (uL) GPC Factor: 2 .0
GPC Cleanup: (Y/N) Y pH: 6.5
Acid Cleanup: (Y/N) Y
Lab Sample ID: 7120009006
Lab File ID: 20070515A047,2 0070515B047
Date Received: 04/30/2007 ' .
Date Extracted: 05/01/2007
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N.
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kg) uq/kq
Q
12674-11-2
Aroclor-1016
41
U
11104-28-2
Aroclor-1221
41
U
11141-16-5
Aroclor-1232
41
u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-1262
41
u
11100-14-4
Aroclor-1268
41
u
£>/)zJoJ
SOM01.1 (5/^^)
-------
1H - FORM I ARO
aroclor Organics analysis data sheet
EPA SAMPLE NO.
J86T.0
Lab Name: DataChem Laboratories, InCi
Lab Code: DATAC Case No. : 3 6345
Matrix
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 40 Decanted: (Y/N) N_
Lab Sample ID: 7120009007
(g/mL) g_
Lab File ID: 20070515A048,2 0070515B048
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: KlOOOO
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH: 5^9
Acid Cleanup: (Y/N) Y
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) IL
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
55
u
11104-28-2
Aroclor-1221
55
u
11141-16-5
Aroclor-1232
55
u
53469-21-9
Aroclor-1242
55
u
12672-29-6
Aroclor-1248
55
u
11097-69-1
Aroclor-1254
55
u
11096-82-5
Aroclor-1260
55
u
37324-23-5
Aroclor-1262
55
u
11100-14-4
Aroclor-1268
55
u
6//z/o7
SOM01.1 (5/gpf4)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc». Contract: EP-W-05-026
Lab Code: DATAC . Case No.: 36345 Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL , 1 Lab Sample ID: 7120009010
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 2 0070515A051, 20070515B051
% Moisture: 33 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2.007
Concentrated Extract Volume: ?10000 (uL) Date Analyzed: 05/16/2007
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1.0 ;
GPC Cleanup: (Y/N) Y pH: 7JD Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
49
U
11104-28-2
Aroclor-1221
49
U
11141-16-5
Aroclor-1232
49
u
53469-21-9
Aroclor-1242
49
u
12672-29-6
Aroclor-12'48
49
u .
11097-69-1
Aroclor-1254
49
u
11096-82-5
Aroclor-1260
49
u
37324-23-5
Aroclor-1262
49
u
11100-14-4
Aroclor-1268
49
u
SOM01.1 (5/$4>?)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 36
Lab Sample ID: 7120009011
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 2 0070515A052,20070515B052
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume:f10000
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH: 7.1
Acid Cleanup: (Y/N) Y_
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12.674-11-2
Aroclor-1016
51
U
11104-2 8-2
Aroclor-1221
51
U
11141-16-5 '
Aroclor-1232
51
u
53469-21-9
Aroclor-1242
51
u
12672-29-6
Aroclor-1248
51
u
11097-69-1
Aroclor-1254
51
u
11096-82-5
Aroclor-1260
51
u
37324-23-5
Aroclor-1262
51
u
11100-14-4
Aroclor-1268
51
u
SOM01.1 (5/$®0)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc;. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ; Lab Sample ID: 7120009Q12
Sample wt/vol: 30.0 (g/mL) g Lab File ID: 20070515A053 ,20070515B053
% Moisture: 3,7 Decanted: (V/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: ,,10000 (uL) Date Analyzed: 05/16/2007
Injection Volume: 2 . 0 (uL) GPC Factor: 2.0 Dilution Factor : 1. 0
GPC Cleanup: (Y/N) Y pH: 7.8 Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/ka) ug/kg
Q
12674-11-2
Aroclor-1016
52
. U
11104-28-2
Aroclor-1221
52
u
11141-16-5
Aroclor-1232
52
u
53469-21-9
Aroclor-1242
52
u
12672-29-6
Aroclor-1248
52
u
11097-69-1
Aroclor-1254
52
u
11096-82-5
Aroclor-1260
52
u
37324-23-5
Aroclor-1262
52
u
11100-14-4
Aroclor-1268
52
u
SOM01.1 (5/^^)
EPA SAMPLE NO.
J86T3
-------
1H - FORM I ARO '
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inci.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 3 0.0
% Moisture: 32
Lab Sample ID: 7120009013
(g/mL) g_
Decanted:. (Y/N) N_
Lab File ID: 20070515A054,2 0070515B054
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: ,.10000 (uL)
Injection Volume: 2.0 (uL) GPC Factor: 2 .0
GPC Cleanup: (Y/N) Y pH: 6^8
Date Analyzed: 05/1672007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N)' N_
Acid Cleanup:. (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Arbclor-1016
49
U
11104-28-2
Aroclor-1221
49
U •
11141-16-5
Aroclor-1232
49
U
53469-21-9
Aroclor-1242
49
u
12672-29-6
Aroclor-1248
49
u
11097-69-1
Aroclor-1254
49
u
11096-82-5
Aroclor-1260
49
u
37324-23-5
Aroclor-1262
49
u
11100-14-4
Aroclor-1268
49
u
SOM01.1 (5/%gf)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T5
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 3634§
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 23
Lab Sample ID: 71200.09014
(g/mL) g
Decanted: (Y/N) N_
Lab File ID: 20070515A055,20070515B055
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: .10000
Injection Volume: 2 . 0 (uL) GPC Factor:
GPC Cleanup: (Y/N) Y pH:. 7 . 5
(uL)
2.0
Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y
CAS NO. •
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kcj) ug/kg
Q
12674-11-2
Aroclor-1016
43
U
11104-28-2
Aroclor-1221
43
u
11141-16-5
Aroclor-1232
.43
u
53469-21-9
Aroclor-1242
43
u •
12672-29-6
Aroclor-1248
43
u
11097-69-1
Aroclor-1254
43
u
11096-82-5
Aroclor-1260
43
u
37324-23-5
Aroclor-1262
43
u
11100-14-4
Aroclor-1268
43
u
C/lx/iof
SOM01.1 (5/^(50)
-------
l&.&P-r PtccH
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc..
Lab Code: DAT AC Case No.: 36345
¦ Contract: EP-W-Q5-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: ,40
Lab Sample ID: 7120009015
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 20070515A056,20070515B056
Date Received: 04/30/2007 ¦
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: ,10000
(uL)
Date Analyzed: 05/16/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: l_Jk
Dilution Factor: 1. 0
Sulfur Cleanup: (Y/N) ,.N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ua/kq) uq/ka
Q
12674-11-2
Aroclor-1016
55
U
11104-28-2
Aroclor-1221
55
U
11141-16-5
Aroclor-1232
55
u
53469-21-9
Aroclor-1242
55
u
12672-29-6
Aroclor-1248
55
u
11097-69-1
Aroclor-1254
30
JS
11096-82-5
Aroclor-1260
55
u
37324-23-5
Aroclor-1262
55
u
11100-14-4
Aroclor-1268
55
u'
/Ijl/
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
l&foPr
EPA SAMPLE NO.
J86T7RE
Lab Name: DataChem Laboratories, Inc..
Lab Code: DATAC Case No.: 3634$
Contract: EP-W-05-026
Mod. Ref No. : ¦
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 40
Lab Sample ID: 7120009015RE
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 2 0070515A072,2 0070515B072
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: f10000
Injection Volume: 2 . 0
GiPC. Cleanup: (Y/N) Y_
Acid Cleanup: (Y/N) Y_
(uL) Date Analyzed: 05/17/2007
(uL) GPC Factor: 2 . 0
pH:
Dilution Factor: 1.0.
Sulfur Cleanup: (Y/N) N.
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) ug/kq
Q
12674-11-2
Aroclor-1016
U
11104-28-2
Aroclor-1221
u
11141-16-5
Aroclor-1232
u
53469-21-9
Aroclor-1242
u
12672-29-6
Aroclor-1248
u
11097-69-1
Aroclor-1254
33
J
11096-82-5
Aroclor-1260
u
37324-23-5
Aroclor-1262
u.
11100-14-4
Aroclor-1268
u
4>//Z /irj.
SOM01.1 (5/^p7)§)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T8 .
r
Lab Name: DataChem Laboratories, Inc.. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : . SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' j - Lab Sample ID: 7120009016
Sample wt/vol: 30.0 (g/mL) q . Lab File ID: 20070515A057, 20070515B057
% Moisture: 39 _ Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC ' Date Extracted: 05/01/2007 . ,
Concentrated Extract Volume: .10000 (uL) Date Analyzed: 05/16/2007
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1.0
GPC Cleanup: (Y/N)' Y pH: 6.1 Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
54
U
11104-28-2
Aroclor-1221
54
u
11141-16-5
Aroclor-1232
54
u
53469-21-9
Aroclor-1242.
54
u
12672-29-6
Aroclor-1248
54
u
11097-69-1
Aroclor-1254
54
u
11096-82-5
Aroclor-1260
54
u
37324-23-5
Aroclor-1262
54
u
11100-14-4
Aroclor-1268
54
u
SOM01.1 (5/5pJ)g)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W4
Lab Name: DataChem Laboratories, Inc..
Lab Code: DATAC Case No. : 36345
Contract: EP-W-05-Q26
Mod. Ref.No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL i
Sample wt/vol: 3 0 . 0 (g/mL) q
% Moisture: 32 Decanted: (Y/N) N
Lab Sample ID: 7120009017
Lab File ID: 20070515A058,20070515B058
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: .10000
(uL) Date Analyzed: 05/16/2007
Injection Volume2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7.8
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) IL
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
48
U
11104-28-2
Aroclor-1221
48
U
11141-16-5
Aroclor-1232
48
u
53469-21-9
Aroclor^-1242 -
48
u
12672-29-6
Aroclor-1248
48
u
11097-69-1
Aroclor-1254
48
u
11096-82-5
Aroclor-1260
48
' u
37324-23-5.
Aroclor-1262
48
' u
11100-14-4
Aroclor-1268
48
u
SOM01.1 (5/$^)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345
. Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 36
Lab Sample ID: 7120009018
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 20070515A059,20070515B059
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
(uL) Date Analyzed: 05/16/2007
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.3
Dilution Factor: 1.0
Sulfur .Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ua/kq) ug/kq
Q
12674-11-2
Aroclor-1016
52
U
11104-28-2
Aroclor-1221
52
U
11141-16-5
Aroclor-1232
52
U
53469-21-9
Aroclor-1242
52
U
12672-29-6
Aroclor-1248
52
U
11097-69-1
Aroclor-1254
52
u
11096-82-5
Aroclor-1260
. 52
u
37324-23-5
Aroclor-1262
52
u
11100-14-4
Aroclor-1268
52
u
SOMOl.l (5/2$$%)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
ZiFoH VfioN Jto5*
EPA SAMPLE NO.
J86W5RX
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345
. Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' j
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 36 Decanted: (Y/N) N_
Lab Sample ID: 7120009018RX
Lab File ID: 20070517A021,20070517B021
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/14/2007
(uLJ
Concentrated Extract Volume: 10000
f
Injection Volume: 2.0 (uL) GPC Factor: 2 .0
GPC Cleanup: (Y/N) Y pH: 7.3
Acid Cleanup: (Y/N) Y
Date Analyzed: 05/18/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ucr/kcr) ug/kg
Q
12674-11-2
Aroclor-1016
52
U
11104-28-2
Aroclor-1221
52
U
11141-16-5
Aroclor-1232
. 52
U
53469-21-9
Aroclor-1242
52
u
12672-29-6
Aroclor-1248
52
u
11097-69-1
Aroclor-1254
52
u
11096-82-5
Aroclor-1260
52
u
37324-23-5
Aroclor-1262.
52
u
11100-14-4
Aroclor-1268
52
u
SOM01.1 (5/3J>fJ7)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W6
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345
Matrix: (SOIL/SED/WATER) SOIL (
Sample wt/yol: 30.0
% Moisture: 36
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Lab Sample ID: 7120009019
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 20070515A060,2007 0515B060
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume:r10000
Injection Volume: 2 . 0
(uL)
Date Analyzed: 05/17/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7.3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
51
U
11104-28-2
Aroclor-1221
51
U
11141-16-5
Aroclor-1232
51
u
53469-21-9
Aroclor-1242
51
u
12672-29-6
AroClor-1248
51
u
11097-69-1
Aroclor-1254
51
U '
11096-82-5
Aroclor-1260
51
u
37324-23-5
Aroclor-1262
51
u
11100-14-4
Aroclor-1268
51
u
6/ix/oj.
SOM01.1 (5/^fg)g)
-------
USSl
%PR0^0
-------
Data Validation Report
Drum NE Marine Drive SI
Case 36345 SDG J86R0
Page 3 of6
detected in all of the samples. Detected Target .compounds in the samples at concentrations less than the CRQLs
were qualified as estimated, "J". • .
Single-component pesticides detected at concentrations with variability of >30% but were <60% between the
primary and confirmatory columns, RTXCLP and RTXCLP2, were reported and qualified estimated, "J". .
Variability >60% were reported as non-detected, "U", at an elevated reporting limits (CRQL) due to
chromatographic interferences. When applicable, all of the "J" and "P" qualifiers applied by the laboratory were
crossed-out by the reviewer.
Blanks - Acceptable
The frequency of analysis of blanks and surrogate recovery criteria were met by all of the blanks analyzed. There
were only trace amount of one target compound (Endrin Aldehyde) detected in some of the pesticide instrument
blanks. Since it was substantially lower than the CRQLs and there were no target compounds detected, none of
the data was qualified on this basis.
Analytical Sequence - Acceptable
All of the standards, blanks, samples, and QC samples were analyzed in accordance with the SOW specified
analytical sequence. The retention times as monitored by the internal standards (SVOCs) and surrogates
(Pesticides) were within the specified RT windows. All of the sample analyses were within an acceptable 12 hour
QC period and were bracketed by a technically acceptable CCV check standards. None of the data was qualified
on this basis.
Surrogates/Deuterated Monitoring Compound Recoveries
Surrogates or deuterated monitoring compounds (DMCs) are known concentrations of isotope-labeled acid and
base/neutral or polynuclear hydrocarbon compounds added to the field and QC samples prior to extraction for
SVOC analyses to monitor the laboratory's performance and efficiency during sample processing, extraction and
analysis. The following is the list of DMCs/surrogates added to all field and QC samples prior to sample
extraction:
DMCs (Soil SVOCs)
Recovery
Limits (%)
DMCs (Soil SVOCs)
Recovery
Limits (%)
Phenol-d5 (PHL)
1.7-103
Dimethylphthalate-d6 (DMP)
43-111
Bis(2-chloroethyl)ether-d8 (BCE)
12-98
Acenapthylene-d8 (ACY)
20-97
2-chlorophenol-d4 (2CP)
13-101
4-Nitrophenol-d4 (4NP)
16-166
4-Methylphenol-d8 (4MP)
8-100
Fluorene-dlO (FLR)
40-108
Nitrobenzene-d4 (NBZ)
16-103
4,6-Dinitro-2-methylphenol-d2 (NMP)
1-121
2-Nitrophenol-d4 (2NP)
16-104
Anthracene-dlO (ANC)
22-98
2,4-Dichlorophenol-d3 (DCP)
23-104
Pyrene-dlO (PYR)
51-120
4-Chloroaniline-d4 (4CA)
1-145
Benzo(a)pyrene-dl2 (BAP)
43-111
-------
Data Validation Report
Drum NE Marine Drive SI
Case 36345 SDG J86R0
Page 5 of 6
spiking mix during the extraction step. The re-extraction confirmed the results from the first extraction were ok
and the original results were picked for reporting purpose by the reviewer. None of the pesticide and PCB data
were qualified on this basis. i ¦ .
Matrix Spike/Matrix Spike Duplicate (MS/MSD) / Lab Control Spike/Spike Duplicate (LCS/LCSD)
- Acceptable
Samples J86R9 was designated for MS/MSD analyses for SVOCs, Pesticides and PCB's. 0 SVOC, 2 of 12
Pesticides, 1 of 2 PCB Matrix Spike or Spike Duplicates were out. Because none of the spiking compounds were
detected in any of the samples and the LCS/LCSD was ok, none of the data was qualified by the reviewer on this
basis.
Internal Standards - Acceptable
The acceptance criteria for internal, standards (IS) are +/-30 seconds for retention time (RT) shifts and
-50% to +100% of the IS area as compared to the IS RT and area of the daily continuing calibration standard. All
of the results met the IS area and RT shift criteria.
Compound Identification
All of the detected target compounds were within the retention time windows. The SVOC detections met the
USEPA spectral matching criteria and were judged to be acceptable. Likewise, the pesticide/PCB detections were
confirmed on a second dissimilar column and were acceptable.
Florisil Cartridge Check - Acceptable
The frequency of analysis and the recovery criteria for florisil used during Pesticides/PCB clean-up were met.
None of the data were qualified on this basis.
Gel Permeation Chromatography (GPC) Check - Acceptable
The frequency of analysis and the recovery criteria for GPC used during Pesticides/PCB clean-up were met. None
of the data were qualified on this basis.
Tentatively Identified Compounds '
Chromatographic peaks in the samples' SVOC runs that are not target compounds, surrogates or internal
standards with areas > 10% of the nearest IS must be tentatively identified by the laboratory using a mass spectral
search of the NIST library.
Common laboratory artifacts and peaks that are found in both the sample and the blanks were crossed out by the
reviewer and flagged unusable, "R". The rest of the TICs identified by the lab on the Form I were qualified as
tentatively identified at estimated concentrations, "JN", with an unknown bias.
Laboratory Contact
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc..,;
Lab Code: DATAC Case No.: 36345';
Matrix:
Contract:' EP-W-05-026
Mod. Ref No. :
SDG No.: J8 6R0
(SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 19
(g/mL)
Decanted: (Y/N) N
Concentrated Extract Volume: 500
f
Injection Volume: 1 • 0
GPC Cleanup: (Y/N)' Y_
(uL) GPC Factor: 2 . 0
pH : 7_;_4
Lab Sample ID: 7120009001
Lab File ID:- NAA04C01
Extraction: (Type) SONC
Date Received: 04/30/2007
(uL) Date Extracted: 05/01/2007
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
u
108-95-2
Phenol
¦ZlC^A-
•J Lf
111-44-4
Bis'(2-chloroethyl) ether
210
U
95-57-8
2-Chlorophenol
210
U
95-48-7
2-Methylphenol
210
U
108-60-1
2,2'-Oxybis(1-chloropropane)
. 210
U
98-86-2
Acetophenone
¦ 71
. J
106-44-5
4-Methylphenol
210
- U
621-64-7
N-Nitroso-di-n-propyla-mine
210
U
67-72-1
Hexachloroethane
210
U
9.8-95-3
Nitrobenzene
210
U
78-59-1
Isophorone
210
u
88-75-5
2-Nitrophenol
210
u
105-67-9
2,4-Dimethylphenol
210
u
111-91-1
Bis (2-chloroethoxy)methane
'210
u
120-83-2
2,4-Dichlorophenol
210
¦ u
91-20-3
Naphthalene
210
u
106-47-8
4-Chloroaniline
210
u
87-68-3
Hexachlorobutadiene
210
u
105-60-2
Caprolactam
L .210
u
59-50-7
4-Chloro-3-methylphenol
210
u
91-57-6
2-Methylnaphthalene
210
u
77-47-4
Hexachlorocyclopentadiene
210
u
88-06-2
2,4,6-Trichlorophenol
210
u
95-95-4
2,4,5-Trichlorophenol
: 210
u
92-52-4
1,1'-Biphenyl
210
u
91-58-7
2-Chloronaphthalene
210
u
88-74-4 -
2-Nitroaniline
410
u
131-11-3
D'imethylphthalate
210
u '.
606-20-2
2,6-Dinitrotoluene
210
u
208-96-8
Acenaphthylene
¦ ¦ 210
. u
99-09-2
3-Nitroaniline
410
u
83-32-9
Acenaphthene
210
•U
f/o7
SOM01.1 (5/200
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc,
Lab Code: DATAC Case No.: 36345 i;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (S01L/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7120009001
(g/mL) cj__
Lab File ID: NAA04C01
Level: (LOW/MED) LOW
% Moisture: 19
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7_^4
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
410
U
100-02-7
4-Nitrophenol
410
U
132-64-9
Dibenzofuran
210
u
121-14-2
2,4-Dinitrotoluene
210
u
84-66-2
Diethylphthalate
210
u
86-73-7
Fluorene
. 210
u
7005-72-3'
4-Chlorophenyl-phenylether
210
u
100-01-6
4-Nitroaniline '
410
- u
53-4-52-1 '
4,6-Dinitro-2-methylphenol
410
u
86-30-6
N-Nitrosodiphenylamine1
210
u
95-94-3
1,2,4,5-Tetrachlorobenzene
210
u
101-55-3
4-Bromophenyl-phenylether
. 210
u
118-74-1
Hexachlorobenzene
210
u
1912-24-9
Atrazine
210
u
87-86-5
Pentachlorophenol
410
u
85-01-8
Phenanthrene
210
u
120-12-7
Anthracene
210
u
86-74-8
Carbazole
210
u.
84-74-2
Di-n-butylphthalate
210
u
206-44-0
Fluoranthene
210
u
129-00-0
Pyrene
210
u
85-68-7
Butylbenzylphthalate
210
u
91-94-1
3,3'-Dichlorobenzidine
210
u
56-55-3
Benzo(a)anthracene
210
U ¦
218-01-9
Chrysene
210
U
117-81-7
Bis(2-ethylhexyl)phthalate
33
J
117-84-0
Di-n-octylphthalate
210
u
205-99-2
Benzo(b)fluoranthene
210
u
207-08-9
Benzo t-k) fluoranthene
210
U
50-32-8
Benzo(a)pyrene
210
u
193-39-5
Indeno(1,2,3-cd)pyrene
210
u
53-70-3
Dibenzo(a,h)anthracene
210
u
191-24-2
Benzo (g, h, 'i) perylene
210
u
58-90-2
2,3,4,6-Tetrachlorophenol
210
u
1 Cannot be separated from Diphenylamine
• . 6,/n/d^ SOM01-L (5/2oo4)6
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories,- Inc:.
Lab Code: DATAC- Case No. : 36345;:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009001
(g/mL) cj_
Lab File ID: NAA04C01
Level: (LOW/MED) LOW
% Moisture: 19
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
f
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC'Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: TjA
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.02
740
JN
.Unsaturated Hydro-carbon
4.11
110
JnI
Polycyclic hydrocarbon
19.15
470
JN
Polycyclic hydrocarbon
24.70
250
J M
•• . ' -
. ' 'V
E9667 962
Total Alkanes
N/A
390
J
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26,
27
.28
29
30
2EPA-designa.ted Registry Number.
<2^
SOM01.1 (5/2003)
4>7
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6S5
Lab Name: DataChem Laboratories, Inc;. ¦ Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345 Mod. Ref No.: SDG No.-: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL i Lab Sample ID: 7120009002
Sample wt/vol: 30.0 (g/mL) g Lab File ID: NAA05C02
Level: (LOW/MED) LOW Extraction: (Type) SONC
% Moisture: .19 Decanted: (Y/N) N Date Received: 04/30/2007
Concentrated Extract Volume: 500 ; (uL) Date Extracted: 05/01/2007
r
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0 Date Analyzed: 05/09/2007 .
GPC Cleanup: (Y/N) Y pH: 6. 5 . Dilution Factor: 1. 0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
ZIO ^3"
3-U,
108-95-2
Phenol
2IO &
3- {J
111 -4'4-4
Bis"(2-'chloroethyl) ether
210
U
95-57-6
2-Chlorophenol
210
U
95-48-7
2-Methylphenol
210
U
108-60-1
2,2'-Oxybis(1-chloropropane)
210
U
98-86-2
Acetophenone
50
J
106-44-5
4-Methylphenol
210
- u
621-64-7
N-Nitroso-di-n-propylamine'
210
u
67-72-1
He'xachloroethane
210
u ¦
98-95-3
Nitrobenzene
210
u
78-59-1
Isophoron'e
210
u
88-75-5
2-Nitrophenol ,
210
. u
105-67-9
2,4-Dimethylphenol
210
u
111-91-1
Bis(2-chloroethoxy)methane
210
u
120-83-2
2,4-Dichlorophenol
210
¦ u
91-20-3
Naphthalene
. 210
u
106-47-8
4-Chloroaniline
210
u
87-68-3
Hexachlorobutadiene
210
' u
105-60-2
Caprolactam
210
u
59-50-7
4-Chloro-3-methylphenol
210
u
91-57-6
2-Methylnaphthalene .
210
u
77-47-4
Hexachlorocyclopentadiene
210
u
88-06-2
2,4,6-Trichlorophenol
210
u
95-95-4
2,4,5-Trichlorophenol
210
u ¦
92-52-4
1, 1'-Biphenyl
210
u.
91-58-7
2-Chloronaphthalene -
210
u
88-74-4
2-Nitroaniline
410
u
131-11-3
Dimethylphthalate
' 210
u
606-20-2
2,6-Dinitrotoluene
210
u
208-96-8
Acenaphthylene
210
u
99-09-2
3-Nitroaniline
410
u
83-32-9
Acenaphthene
210
u
SOM01.1 (5/2005*)®
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S5
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case.No.: 36345 •
Matrix:
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
(SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Level: (LOW/MED) LOW
% Moisture: 19
Lab Sample ID: 7120009002
(g/mL)
Lab File ID: NAA05C02
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—P
Injection Volume: 1.0
(uL) Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 6.5
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kg) uq/kq
Q
¦51-28-5
'2, 4-Dinitrophenol
410
U
100-02-7 •
4-Nitrophenol
410
U
' 132-64-9
Dibenzofuran
'210
u
121-14-2
2,4-Dinitrotoluene
.210
U ¦ '
84-66-2
Diethylphthalate
210
u
86-73-7
Fluorene
210
u
7005-72-3
4-Chlorophenyl-phenylether
210
u
100-01-6'
4-Nitroaniline
410
" u
534-52-1
4,6-Dinitro-2-methylphenol
410
u
86-30-6
N-Nitrosodiphenylamine1
210
u
95-94-3
1,2,4,5-Tetrachlorobenzene
.210
u
101-55-3
4-Bromophenyl-phenylether
210
u
118-74-1
Hexachlorobenzen'e
. 210
u
1912-24-9
Atrazine
210
u
87-86-5'
Pentachlorophenol
410
u
85-01-8
Phenanthrene
210'
u
120-12-7
Anthracene
210-
u
86-74-8
Carbazole
210
u
84-74-2
Di-n-butylphthalate
210
U '
206-44-0
Fluoranthene
210
u
129-00-0
Pyrene
210
u
85-68-7
Butylbenzylphthalate
. 210
u
'91-94-1
3,3'-Dichlorobenzidine
210
u
56-55-3 :
Benzo(a)anthracene
210
u
218-01-9
Chrysene
210
u
117-81-7
Bis(2-ethylhexyl)phthalate'
31
J
117-84-0
Di-n-octylphthalate
210
u
205-99-2
Benzo(b)fluoranthene
210
a
207-08-9
Benzo(k)fluoranthene
210
u.
50-32-8
Benzo(a)pyrene
210
u
193-39-5
Indeno (1, 2,'3-cd) pyrene
210
u
53-70-3
Dibenzo(a,h)anthracene
210
u
191-24-2
Benzo(g,h,i)perylene
210
u-
58-90-2
2,3,4,6-Tetrachlorophenol
210
u
1 Cannot be separated from Diphenylamine
SOM01.1 (5/200
&
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET'
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86S5
Lab Name: DataChem Laboratories, . Inc;.
Lab Code: DATAC Case No.: 36345 Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Contract: EP-W-05-02 6
No. :
SDG No.: J8 6R0
Lab Sample ID: 7120009002
(g/mL) £_
Lab File ID: NAA05C02
Level: (LOW/MED) LOW
% Moisture: 19
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL) Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor:' 2.0
pH: _6J5
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.02
660
JN
Unsaturated Hydrocarbon
4.11
140
JSi
Polycyclic hydrocarbon
19.14
390
JN
Polycyclic hydrocarbon
24 .70
250
JM
¦
E9667962
Total Alkanes
N/A
610
J
01
02
03
04
05
06
07
08
09
10
11
12
•13
14
15
16
17
18
19
20
21
22
23
24
25
26,
27
28
29
30
!EPA-de.signated Registry Number.
6Q
fc> 7 s^01"1 (5/2005)
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories, Inc;. i,
Lab Code: DATAC Case No.: 3634 5
Matrix: (SOIL/SED/WATER) SOIL i
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009003
Sample wt/vol: 30.0
(g/mL) cj_
Lab File ID: NAA06C03
Level: (LOW/MED) LOW
% Moisture: 38
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—f—
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH:.6_1J
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS"NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
2rk> »
& (J
108-95-2
Phenol
27O
d-U
111-44-4
Bis (2-chloroet.hyl) ether
270
V
95-57-8
2-Chlorophenol
270
U
95-48-7
2-Methylphenol
270
u
108-60-1
2,2'-Oxybis(1-chloropropane)
270
u
98-86-2
Acetophenone
60
J
106-44-5
4-Methylphenol
270
u .
621-64-7
N-Nitroso-di-n-propylamine
270
u
67-72-1
Hexachloroethane
270
u
98-95-3
Nitrobenzene
270
u
78-59-1
Isophorone
270
u
88-75-5
2-Nitrophenol
270
u
105-67-9
2,4-Dimethylphenol
270
u
111-91-1
Bis(2-chloroethoxy)methane
270
u
120-83-2
2,4-Dichlorophenol , -
270
u
91-20-3
Naphthalene
270
u
106-47-8
4-Chloroaniline
270
u
87-68-3
¦Hexachlorobutadiene
270
' U
105-60-2
Caprolactam
270
u
59-50-7
4-Chioro-3-methylphenol
270
u
91-57-6
2-Methylnaphthalene
' . 270
u
77-47-4
Hexachlorocyclopentadiene
270
u .
88-06-2
2,4,6-Trichlorophenol
270
u
95-95-4
2,4,5-Trichlorophenol
270
u
92-52-4
1,1'-Biphenyl
270
u
91-58-7
2-Chloronaphthalene
270
u
88-74-4
2-Nitroaniline
530
u
131-11-3
Dimethylphthalate
270
u
606-20-2
2,6-Dinitrotoluene
270
u
208-96-8
Acenaphthylene
270
u
99-09-2
3-Nitroaniline
530
u
83-32-9
Acenaphthene
270
u
&/(l /c~4
SOM01.1 (5/2005)'
^)3
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6S6
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC ¦ Case No.: 36345
Matrix: (SOIL/SED/WATER) SOIL . i
Sample wt/vol: 30. 0
Level: (LOW/MED) LOW
% Moisture: 38 Decanted: (Y/N) N
' Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009003
(g/mL) g_
Lab File ID: NAA06C03
Extraction: (Type) SONC
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—r—
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
¦pH: 6.8
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS¦NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
530
U
100-02-7
4-Nitrophenol-
530
U
' 132-64-9
Dibenzofuran
270
u
121-14-2
2,4-Dinitrotoluene
270
u
84-66-2
Diethylphthalate
270
u
86-73-7
Fluorene
270
u
7005-72-3
-4-Chlorophenyl-phenylether
270
u
100-01-6
4-Nitroaniline
" 530
¦¦ u
534-52-1
4,- 6-Dinitro-2-methylphenol
530
u
86-30-6
N-Nitrosodiphenylamine1
270
u
95-94-3
1,2,4,5-Tetrachlorobenzene
270
u
101-55-3
4-Bromophenyl-phenylether ¦
270
u
118-74-1
Hexachlorobenzene
- 270
u
1912-24-9-
Atrazine
¦270
u
87-86-5 ,
Pentachlorophenol
530
u
85-01-8
Phenanthrene
270
u
120-12-7
Anthracene
270
u
86-74-8
Carbazole
270
u
84-74-2
Di-n-butylphthalate
270
u
206-44-0
Fluoranthene
270
UT
129-00-0
Pyrene
270
u T
85-68-7
Butylbenzylphthalate
270
u
91-94-1
3, 31-Dichlorobenzidine
270
u ¦
56-55-3
Benzo(a)anthracene
270
UT
218-01-9
Chrysene
270
UT
117-81-7
Bis(2-ethylhexyl)phthalate
41
J'
117-84-0
Di-n-octylphthalate
270
U
205-99-2
Benzo(b)fluoranthene
270
. UT
207-08-9
Benzo(k)fluoranthene
270
UJ
50-32-8
Benzo(a)pyrene
. 270
UZJ"
193-39-5
Indeno(1,2,3-cd)pyrene
270
UT
53-70-3
Dibenzo(a,h)anthracene
270
UT
191-24-2
Benzo(g,h,i)perylene
270
UT
58-90-2
2,3,4,6-Tetrachlorophenol ;
27 0
u
1 Cannot.be separated from Diphenylamine
6./I //O f
SOM01.1 (
5/200?)4
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 3 634 5;
Matrix: (SOIL/SED/WATER) SOIL
?
Sample wt/vol: 30. 0 (g/mL) £
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009003
Lab File ID: NAA0 6C03
Level: (LOW/MED) LOW
% Moisture: 38
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—F~
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: '(Y/N) Y_
(uL) GPC Factor: 2.0
pH: 6.8
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
¦ COMPOUND NAME
RT
EST. CONC.,
Q
79-34-5 '
Ethane, 1., 1, 2, 2-tetrachloro-
4.01
630
JN
Unsaturated Hydrocarbon
4.11
140
JN
119-93-7
[1,1' -Biphenyl]-4,4'-diamine, 3,3'-dimet
13.76
120
JN
Polycyclic hydrocarbon
19.14
570
J,V
Pol-ycyclic hydrocarbon "
24 .70
'390
J,\l
,
' ¦
E9667962
Total Alkanes
N/A
680
J
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
.26.
27
28
29
30
2EPA-designated Registry Number.
G/ll/ol SOM01.1 (5/200^?
-------
ID - FORM I SV-.l
SEMI VOLATILE ORGAN-ICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc;
Lab Code: DATAC Case No.: 36345;
Matrix:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
(SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009004
(g/mL) g_
Lab File ID: NAA07C04
Level: (LOW/MED) LOW
% Moisture: 30
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6_;_9
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
2.4o *9
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6S7
Lab Name: DataChem Laboratories, Inc.:
Lab Code: DATAC Case No.; 36345;
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Level: (LOW/MED) LOW-
% Moisture: 30
(g/mL) g_
Decanted: (Y/N) N
Concentrated Extract Volume: 50.0
(uL)
Injection Volume: 1. 0
GPC Cleanup: (Y/N) ;Y_
(uL) GPC Factor: 2 ¦ 0
pH: 6^9
Lab Sample ID: 7120009004
Lab File ID: NAA07C04
Extraction: (Type) SONC
Date Received: 04/30/2007
Date Extracted: 05/01/2007
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
4 70
u
100-02-7
4-Nitrophenol
470
u
132-64-9
Dibenzofuran
240
u
121-14-2
2,4-Dinitrotoluene
240
u
84-66-2
Diethylphthalate .
240
U '
86-73-7
Fluorene
240
U
7005-72-3 '
4-Chiorophenyl-phenylether
240
u
100-01-6
4-Nitroaniline
470
u
534-52-1
4,6-Dinitro-2-methylphenol
470
u
86-30-6
N-Nitrosodiphenylamine1
240
U'
95-94-3
1,2,4,5-Tetrachlorobenzene
240
u
101-55-3
4-Brompphenyl-phenylether
240
u
118-74-1
Hexachlorobenzene
240
¦u
1912-24-9
Atrazine
240
u
87-86-5
Pentachlorophenol
470
u
85-01-8
Phenanthrene
240
u
120-12-7
Anthracene
240
u
86-74-8
Carbazole
240
u
84-74-2
Di-n-butylphthalate
240
¦ u
206-44-0
Fluoranthene
240
UJT
129-00-0
Pyrene
240
UT
85-68-7 .
Butylbenzylphthalate
24o «
91-94-1
3,3'-Dichlorobenzidine
240
U
56-55-3
Benzo(a)anthracene
240
UT
218-01-9
Chrysene
24 0
UJ
117-81-7
Bis(2-ethylhexyl)phthalate
240 3^
JU .
117-84-0
Di-n-octylphthalate
240
U
205-99-2
Benzo(b)fluoranthene
.240
u;r
207-08-9
Benzo(k)fluoranthene
240
UJ
50-32-8
Benzo(a)pyrene
240
u J
193-39-5
Indeno(1,2,3-cd)pyrene
240
uy
53-70-3
Dibenzo(a,h)anthracene
240
uj
191-24-2
Benzo(g,h,i)perylene
240
UJ
58-90-2
2,3,4,6-Tetrachlorophenol
240
u
1 Cannot be separated from Diphenylamine
ft
©-?
SOMOl.l (5/200
li°
-------
. IK - FORM I SV-TIC .
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS.
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026 ,
Mod. Ref No.:
SDG No.: J8 6R0
.Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample. ID: 7120009004
(g/mL)
Lab File ID: NAA07C04
Level: (LOW/MED) LOW
% Moisture: 30.
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 ¦ 0
pH: 6.9
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
¦CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
cas number;
COMPOUND. NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.01
580
JN
19026-94-9
Unsaturated Hydrocarbon
4 .10
190
JN
2,5-Methano-lH-indene, octahydro-
15.41
280
JN
Polycyclic hydrocarbon
19.14
570
JN
Polycyclic hydrocarbon
24 . 70
300
JN
E9667962
Total Alkanes
N/A
600
J
01
' 02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
2 6-
27
28
29
30
2EPA-designated Registry Number.
C-flilol- SOM01.1 (5/200?)1
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6S>0
Lab Name: DataChem Laboratories, Inc: i. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345;;.' Mod. Ref No.:'
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 ¦ 0
Lab Sample ID: 7120009005
(g/mL)
Lab File ID: NAA08C05
¦Level: (LOW/MED) LOW
% Moisture: 29
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 5.3
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS. NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7 '
Benzaldehyde
£40 44
108-95-2
Phenol ¦
24o 2*
JU ¦
111-44-4
Bis(2-chloroethyl)ether
240
u
95-57-8
2-Chlorophenol
240
u
95-48-7
2-Methylphenol
240
u
108-60-1
2,2'-Oxybis(1-chloropropane)
24 0
u
98-86-2
Acetophenone
51
J-
106-44-5
4-Methylphenol
240
¦' u
621-64-7
N-Nitroso-di-n-propylamine
240
u
67-72-1
Hexachloroethane
240
u
98-95-3
Nitrobenzene
240
u
78-59-1
Isophorone
24 0
u
88-75-5
2-Nitrophenol
240
u
105-67-9
2,4-Dimethylphenol
240
u
111-91-1
Bis(2-chloroethoxy)methane
240
u
120-83-2
2,4-Dichlorophenol
240
u
91-20-3
Naphthalene
240
u
106-47-8
4-Chlorpaniline '
240
u
87-68-3
Hexachlorobutadiene
240
u
105-60-2
Caprolactam
240
u
59-50-7
4-Chloro-3-methylphenol'
240
u
91-57-6
2-Methylnaphthalene
240
u ¦
77-47-4
Hexachlorocyclopentadiene
240
u
88-06-2
2,4,6-Trichlorophenol
240
. u
95-95-4
2,4,5-Trichlorophenol
240
u
92-52-4
1,1'-Biphenyl
240
u
91-58-7
2-Chloronaphthalene
240
u
88-74-4
2-Nitroaniline
470
u
131-11-3
Dimethylphthalate
240
u
606-20-2
2,6-Dinitrotoluene
240
u
208-96-8
Acenaphthylene
240
u
99-09-2
3-Nitroaniline
470
0
83-32-9
Acenaphthene
240
u
-6/r/o?
SOM01.1 (5/2005)
WP
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S8
Lab Name: DataChem Laboratories, Inc. ;
Lab Code:. DATAC Case No. : 36345
_ Contract: EP-W-05-026.
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0 __
Lab Sample ID: 7120009005
(g/mL) g_
Lab File ID: NAA08C05
Level: (LOW/MED) LOW
% Moisture: 29
Extraction; (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y
(uL)
Date Extracted: ,.05/01/2007
(uL) GPC Factor: 2,0
pH: 5.3
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
'. Q
51-28-5
2, 4-Dinitrophenol
470
U '
100-02-7
4-Nitrophenol
470
U
132-64-9
Dibenzofuran
240
u
121-14-2
2,4-Dinitrotoluene
240
u
84-66-2
Diethylphthalate
' - 240
u
86-7.3-7 '
Fluorene
240
u
7005-72-3
4-Chlorophenyl-phenylether
240
u
100-01-6
4-Nitroaniline
470
u
534-52-1
4,6-Dinitro-2-methylphenol
470
u
86-30-6
N-Nitrosodiphenylamine1
240
u
95-94-3
1,2,4,5-Tetrachlorobenzene
240
u
101-55-3
4-Bromophenyl-phenyl'ether
240
u
118-74-1
Hexachlorobenzene
240
u
1912-24-9
Atrazine
240
u
87-86-5
Pentachlorophenol
470
u
85-01-8
Phenanthrene
15
J
120-12-7
Anthracene •
240
u
86-74-8
Carbazole
240
u
84-74-2
Di-n-butylphtha'late
42
J
206-44-0
Fluoranthene
.24
J
129-00-0
Pyrene
16
J
85-68-7
Butylbenzylphthalate •
¦ 240
u
91-94-1
3,3'-Dichlorobenzidine
240
u
56-55-3
Benzo(a)anthracene
2*0 *2
I? (j
218-01-9
Chrysene
15
J
117-81-7
Bis(2-ethylhexyl)phthalate
59
J
117-84-0
Di-n-octylphthalate
¦ 240
u
205-99-2
Benzo(b)fluoranthene
18
J .
207-08-9
Benzo(k)fluoranthene
8.5
J
50-32-8
Benzo(a)pyrene
24 0
UT
193-39-5
Indeno(1,2,3-cd)pyrene
240
UJ
53-70-3
Dibenzo(a,h)anthracene
240
UJ-
191-24-2 ¦
Benzo(g,h,i)perylene
240
UJ
58-90-2
2,3,4,6-Tetrachlorophenol |
240
u
Cannot be separated from Diphenylamine
^2^
SOM01.1 (5/20fly)
w
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY' IDENTIFIED COMPOUNDS
Lab.Name: DataChem Laboratories, Inc;. i. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345v Mod. Ref No.:
EPA SAMPLE NO.
J0 6S8
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009005
(g/mL)
Level: (LOW/MED) LOW
% Moisture: 29
.Lab File ID: NAA08C05
Extraction:' (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH : 5_;_3
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
' 4 . 01
610
JN
Urisaturated Hydrocarbon
4 .11
100
JN
Polycyclic hydrocarbon
.15.16
1.00
JN
100018-99-0
Benzoxazole, 2-[(2,3-dihydro-3,5-dimethy
15. 67
98
JN
100013-00-0
Z-17-Nonadecen-l-ol acetate
17.55
' 130
JN
Polycyclic hydrocarbon
19.14
480
JM
100013-97-0
3-Methylaminocarbonyl-l,2-diphenyl-cyclo;
22.29
' . 170
" JN
100018-94-0
4,4,6a,6b,8a,11,11,14b-Octamethyl-l, 4, 4a
23. 63
220
JN
Polycyclic hydrocarbon
24 . 50
190
JM
Polycyclic hydrocarbon
2-4.71
310
JN
E9667962
Total.Aikanes
N/A
900.
J
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
.16
17
18
19
20
21
22
23
24
25
2 6'
27
28
29
30
!EPA-designated Registry Number.
£>/(t/dl SOM01.1 (5/20
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 3634 5; Mod. Ref No.: SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL i Lab Sample ID: 7120009006
Sample wt/vol: 30.0 (g/mL) q ¦ Lab File ID:. NAA09C06 ^
Level: (LOW/MED) LOW " Extraction: (Type) SONC
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/30/2007
Concentrated Extract Volume: 5^0 (uL) Date Extracted: 05/01/2007
Injection Volume: 1. 0 (uL). GPC Factor: 2 . 0 Date Analyzed: 05/09/2007
GPC Cleanup: (Y/N) Y pH: 6.5 ' Dilution Factor: 1. 0
CAS NO.
COMPOUND.
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7
Benzaldehyde
2/0 63-
¦ 6- a
108-95-2
Phenol - ' '
210 +$
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3634 5-
Matrix: (SOIL/SED/WATER) SOIL , 1
Sample wt/vol: 30.0
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009006
(g/mL) g_
Lab File ID': NAA09C06
Level: (LOW/MED) LOW
% Moisture: 19-
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007,
Concentrated Extract Volume: 5Q0 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/09/2007
GPC Cleanup: (Y/N) Y_
pH: 6. 5
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kg
Q
51-28-5
2,4-Dinitroptienol
'410
U
100-02-7
4-Ni.trophenol
410
¦ U
132-64-9 -
Dibenzofuran
210
U
121-14-2
2,4-Dinitrotoluene
210
U-
84-66-2
Diethylphthalate
¦ 210
u
86-73-7
Fluorene
210
u
7005-72-3
4-Chlorophenyl-phenylether
210
u
100-01-6
4-Nitroanilirie •
410
u
534-52-1
4,6-Dinitro-2-methylphenol
410
u
86-30-6
N-Nitrosodiphenylamine1
210
u
95-94-3
1,2,4, 5-Tetrachlorobenzene
210
u
101-55-3
4-Bromophenyl-phenylether
21.0
u
118-74-1 •
Hexachlorobenzene
¦ 210
u
1912-24-9
Atrazine
210
U"
.87-8 6-5
Pentachlorophenol .
410
U
85-01-8
Phenanthrene
9.3
J
120-12-7.'
Anthracene
210
• u
86-74-8
Carbazole
210
u
84-74-2
Di-n-butylphthalate
43
J
206-44-0
Fluoranthene
¦ 15
J
129-00-0
Pyrene
12
J
85-68-7
Butylbenzylphthalate
210
¦ u
91-94-1
3,3'-Dichlorobenzidine
210
u
56-55-3
Benzo(a)anthracene
ZlO
J u
218-01-9
Chrysene
9.8
J
117-81-7
Bis(2-ethylhexyl)phthalate
99-
J
117-84-0
Di-n-octylphthalate
210
u
205-99-2
Benzo (b)fluoranthene
21:0
UJ
207-08-9
Benzo(k)fluoranthene
210
U.X
50-32-8
Benzo(a)pyrene
210
UT '
193-39-5
Indeno(1,2,3-cd)pyrene
210
UT
53-70-3
Dibenzo(a,h)anthracene
210
UJ
191-24-2
Benzo-(g, h, i) perylene
. 210
UT
58-90-2
2,3,4,6-Tetrachlorophenol
210
u
1 Cannot be separated from Diphenylamine
£ /... £
SOM01.1
¦ 135
(5/2005)
-------
IK - FORM I SV-TIC
SEMIVOLATILE O'RGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc;.
Lab Code: .DATAC ¦ Case No. : 3 634 5 •
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Lab Sample ID: 7120009006
(g/mL)
Lab File ID: NAA0 9C0 6
Level: (LOW/MED) LOW
% Moisture: 19
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
-f-
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6.5
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS: (ug/L or ug/kg) uq/kq.
CAS NUMBER
COMPOUND NAME
RT
EST,. CONC.
Q
01
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 .02
740
JN
02
Cyclic hydrocarbon
4 .07
170
JM
03
103-82-2
Benzeneacetic acid
6.57
120
JN
04
544-63-8
Tetradecanoic acid
11.14
' 280
. JN
05
102608-53-7
3,7,11,15-Tetramethyl-2-hexadecen-l-ol.
12.16
230
JN
06
112-62-9
9-Octadecenoic acid (Z)—, methyl ester
12.34
180
JN
07
7132-64-1
Pentadecanoic acid, methyl ester
12.50
220
- JN
08
100012-92-0.
Z-ll-Tetradecenoic acid
12.63
560
JN
09
57-10-3
n-Hexadecanoic acid
12.77
1200
JN
10
Unknown aromatic
13.09
120
JM
11
Unknown oxyhydrocarbon
13.23
130
JN
12
69009-90-1
1,1'-Biphenyl, bis(1-methylethyl)-
13.89
220
JN
13'
100012-92-0 ¦
Z-8-Methyl-9-tetradecenoic acid
13. 95
220
JN
14
18801-00-8
Anthracene, 2-(1,1-dimethylethyl)-
14.55
86
JN
15
511-15-9
2-Phenanthrenol, 4b, 5, 6, 7, 8', 8a, 9,10-octa!
14 . 97
'84
JN
16
18435-45-5 1
1-Nonadecene
16.27
410
JN
17
100012-91-0
E-15-Heptadecenal
16.47
220
JN
18
Unknown oxyhydrocarbon
16.70
120
J(4
19
22412-97-1
Dodecanoic acid, tetradecyl ester
16.83
420
JN
20
Unknown oxyhydrocarbon
17 .06
360
JM
21
1639-05-0 .
2-Pentanethiol, 4-methyl-
17.30
130
JN
22
4602-84-0
2,6,10-Dodecatrien-l-ol, 3,7,11-trimethy
17.38
100
JN
23
Unknown oxyhydrocarbon
17.47
210
' JM
24
638-66-4
Octadecanal
17.54
630
JN
25
78563-70-9
3-Ethyl-2-methyl-6-n-propyl-4-(2-furyl)p
18.22
160
JN
2 6>.
638-66-4
Octadecanal
19.28
400
JN •
27
100020-97-0
17-(1,5-Dimethylhexyl)-10,13-dimethyl-2,
20.59
360
JN
28
83-47-6
.gamma.-Sitosterol
23.37
660
JN
29
471-68-1
Olean-12-ene
23 . 64
470
JN
30
19890-84-7
Longifolenaldehyde
24 .51
800
JN
E9667962
Total Alkanes
N/A
2900
M
^EPA-designated Registry Number.
SOM01.1 (5/2005)
3?i6
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA "SAMPLE NO.
J86T0
Lab Name: DataChem Laboratories, Inc: ¦>. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345: y Mod. Ref No.: '' SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL' l Lab Sample ID: 7120009007
Sample wt./vo-l: 30. 0 (g/mL) g ¦ ¦' Lab File ID: NAA10C07
Level: (LOW/MED) LOW Extraction: (Type) SONC
% Moisture: £0 Decanted: (Y/N) N Date Received: 04/30/2007
Concentrated Extract Volume: 5^0 __ (uL) Date Extracted': 05/01/2007
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0 ' Date Analyzed: 05/09/2007
GPC Cleanup: (Y/N) Y pH: 5.9 Dilution Factor: 1. 0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7 "
Benzaldehyde
28b *5
£F (J
108-95-2
Phenol
2.8V 2$
t? u
111-44-4 '
Bis (2-chloroethyl)ether
280
U
95-57-8
2-C.hlorophenol
280
u
95-48-7 ¦
2-Methylphenol
280
u
108-60-1
2,2'-Oxybis(1-chloropropane)
.280
u
98-86-2
Acetophenone
56
J
106-44-5
4-Methylphenol
280
" u ¦
621-64-7
N-Nitroso-di-n-propylamine
280
u
67-72-1
Hexachloroethane
280
. u
98-95-3 '
Nitrobenzene
. 280
u
78-59-1
Isophorone
280
u
88-75-5
2-Nitrophenol
280
u
105-67-9
2, 4-Dimethylphenol
280
u
111-91-1
Bis(2-chloroethoxy)methane
280
u
120-83-2
2,4-Dichlorophenol
280
u
91-20-3
Naphthalene
280
u.
106-47-8
4-Chloroaniline
280
u
87-68-3
Hexachlorobutadiene
¦ 280
u
105-60-2
Caprolactam
280
u
59-50-7
4-Chloro-3-methylphenol
280
u
91-57-6
2-Methylnaphthalene
28 0
u
77-47-4
Hexachlorocyclopentadiene
280
u
88-06-2
2,4,6-Trichlorophenol
280
u
95-95-4
2,4,5-Trichlorophenol
280
u
92-52-4
1,1'-Biphenyl
280
u .
91-58-7
2-Chloronaphthalene
280
u
88-74-4
2-Nitroaniline
550
u
131-11-3
Dimethylphthalate
• . 280
u
606-20-2 '
2,6-Dinitrotoluene
280
u
208-96-8
Acenaphthylene
280
u
99-09-2
3-Nitroaniline
550
u
83-32-9
Acenaphthene
28 0
u
SOM01.1 (5/20
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T0
Lab Name: DataChem Laboratories, Inc.'
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009007
(g/mL) g_
Lab File ID: NAA10C07
Level: (LOW/MED) LOW
% Moisture: 40
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5Q0 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/09/2007
GPC Cleanup: (Y/N) Y_
pH: 5.9
Dilution Factor: 1.0
CAS NO.
COMPOUND ,
CONCENTRATION UNITS:
(uq/L or uq/kg) uq/kg
Q
51-28-5
2,4-Dinitrophenol
550
U
.100-02-7
4-Nitrophenol
550
U
132-64-9
Dibfcnzofuran
280
U
121-14-2
2,4-Dinitrotoluene
280
u
84-66-2
Diethylphthalate
280
u
86-73-7'
Fluorene
280
u
7005-72-3
4-Chlorophenyl-phenylether
280
u
100-01-6
4-Nitroaniline
550
u
534-52-1
4,6-Dinitro-2-methylphenol
550
U'
86-30-6
N-Nitrosodiphenylamine1
280
u
95-94-3
1,2,4,5-Tetrachlorobenzene
280
u
101-55-3 -
4-Bromophenyl-phenylether
280
u
118-74-1
Hexachlorobenzene
280
u
1912-24-9
Atrazine
280
u
87-86-5
Pentachlorophenol
550
u
85-01-8
Phenanthrene
280
u
120-12-7
Anthracene
280
u
86-74-8 .
Carbazole
280
u
84-74-2
Di-n-butylphthalate
21
J
206-44-0
Fluoranthene
280
UT
129-00-0
Pyrene
280
UJ
85-68-7
Butylbenzylphthalate
14
J
91-94-1
3,3'-Dichlorobenzidine
280
u
56-55-3
Benzo(a)anthracene
280
UJ
218-01-9
Chrysene
280
UX
117-81-7
Bis(2-ethylhexyl)phthalate
41
J
117-84-0
Di-n-octylphthalate
28 0
U
205-99-2
Benzo(b)fluoranthene
280
UJ
207-08-9
Benzo(k)fluoranthene
280
UJ
50-32-8
Benzo(a)pyrene
280
ux
193-39-5
Indeno(1,2,3-cd)pyrene
280
UJ
53-70-3
Dibenzo(a,h)anthracene
280
UJ
191-24-2
Benzo(g,h,i)perylene
280
UJ
58-90-2
.2,3,4,6-Tetraehlorophenol
• ' 280
U .
1 Cannot be separated from Diphenylamine
£/> I /kl
SOM01.1 (
5/2 0?)f)^
-------
IK - .FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86TQ
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345;
Contract: EP-W-05-026
Mod.1Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Lab Sample ID: 7120009007
(g/mL) g_
Lab File ID: NAA10C07
Level: (LOW/MED) LOW
% Moisture: 40
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received:. 04/30/2007
Concentrated Extract Volume: 500
—r—
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) ,'Y_
(uL) GPC Factor: 2.0
pH: 5.9
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 . 01
720
JN
Unsaturated. Hydrocarbon
4.11
160
JN
Unknown aromatic
7.18
260
J#4
Unsaturated Hydrocarbon
7.40
210
JH
4706-81-4
2-Tetradecanol
12.27
1300
JN
Unknown amide
12.87
130
629-54-9
Hdxadecanamide
14.17
130
- JN
90949-53-4
7-Nonenamide
15.0 6
1600
JN
143-22-6
Ethanol, 2-[2-(2-butoxyethoxy)ethoxy]-
15.40
150
JN
Polycyclic hydrocarbon
19.14
490
JM
Polycyclic¦hydrocarbon
24 .70
440
JN
E9667962
Total Alkanes
N./A
3200
J
01
02
03
04
05
06
07
08
09
10
11
•12
13
14
15
16
17
18
19
20
21
22
23
24
25
26,
27
28
29
30
?EPA-designated Registry Number.
SOM01.1 (5/20057
53)5
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc.;
Lab' Code: DATAC Case No.: 36345;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7120009010
(g/mL) g_
Lab File ID: NAA14C10
Level: (LOW/MED) LOW
% Moisture: 33
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y
(uL) GPC Factor: 2.0
pH: 2^0
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION'UNITS:
(uq/L or ug/kg) ug/kg
Q
'100-52-7 ¦
Benzaldehyde
Z5~0~Mr
¦j(J
108-95-2
Phenol
2S O '35
111-44-4
Bis(2-chloroethyl)ether
250
U
95-57-8
2-Chlorophenol
250
U
95-48-7
'2-Methylphenol
. 250
u
108-60-1
2, 2 ' ^-Oxybis (1-chloropropane)
250
u
98-86-2
Acetophenone
77
J
106-44-5
4-Methylphenol
250
.. y
621-64-7
N-Nitroso-di-n-propylamine
250
u
67-72-1 :
Hexachloroethane
250'
u
98-95-3
Nitrobenzene
250
u
'78-59-1
Isophorone
250
u
88-75-5
2-Nitrophenol
250
u
105-67-9
2,4-Dimethylphenol
250
u
111-91-1
Bis(2-chloroethoxy)methane
250
. u
120-83-2
2,4-Dichlorophenol
.250
u
91-20-3'
Naphthalene
. 250
' u
106-47-8.
4-Chloroaniline.
250
u
87-68-3 '
Hexachlorobutadiene
250
u
105-60-2 ¦
Caprolactam ¦
250
u
59-50-7
4-Chloro-3-methylphenol
250
u
91-57-6
2-Methylnaphthalene
250
u
77-47-4
Hexachlorocyclopentadiene
250
. u
88-06-2
2, 4, 6-Trichlorophenol,
.250
u
95-95-4
¦2,4,5-Trichlorophenol
250
u
92-52-4
1,1'-Biphenyl '
. 250
u
91-58-7
2-Chloronaphthalene ¦
250
u
88-74-4
2-Nitroaniline
490
u
131-11-3
Dime'thylphthalate
250
u
606-20-2
2,6-Dinitrotoluene
250
u
208-96-8
Acenaphthylene
250
u
99-09-2
3-Nitroaniline
490
u
83-32-9
Acenaphthene
250
u
' xfrN
l£/t I /o^
SOM01.1 (
5/20?!£
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc:.
Lab Code: DATAC Case No.: 36345
_ Contract: EP-W-05-02 6
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7120009010
(g/mL) g_
Lab File ID: NAA14C10
Level: (LOW/MED) LOW
% Moisture: 33
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume:' 500
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 2j^0
Date Analyzed: 05/09/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND ..
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
490
U
100-02-7
4-Nitrophenol
.4 90
U
: 132-64-9
Dibenzofuran
250
u
121-14-2
2,4-Dinitrotoluene
250
u
84-66-2
Diethylphthalate
250
U ¦
86-73-7
Fluorene
250
u
7005-72-3
4-Chlorophenyl-phenylether
250
u
100-01-6
4-Nitroaniline ¦
490
•" u
534-52-1
4,6-Dinitro-2—methylphenol ¦ •
490
u
86-30-6
N-Nitrosodiphenylamine1
250
u
95-94-3 <
1,2,4,5-Tetrachlorobenzene
.250
u
101-55-3 .
¦4-Bromophenyl-phenylether
250-
u
118-74-1
Hexachlorobenzene
250
U'
1912-24-9
Atrazine
250
u
87-86-5
Pentachlorophenol
• 490
u
85-01-8
Phenanthrene
250
u
120-12-7
Anthracene
250
u
86-74-8
Carbazole
250
u
84-74-2
Di-n-butylphthalate
67
J
206-44-0
Fluoranthene
• 13
J
129-00-0
Pyrene '
: 21
J '
85-68-7
Butylbenzylphthalate
250
u
91-94-1
3,3'-Dichlorobenzidine
250
u
56-55-3
Benzo(a)anthracene
12
J
218-01-9
Chrysene
13
J
117-81-7
Bis(2-ethylhexyl)phthalate
77
J
117-84-0
Di-n-octylphthalate
250
u
205-99-2
Benzo.(b)fluoranthene
15
J
207-08-9
Benzo(k)fluoranthene
250
u
50-32-8
Benzo(a)pyrene
250
u
193-39-5
Indeno(l,2,3-cd)pyrene
250
u
53-70-3
Dibenzo(a, h)anthracene
250
u
191-24-2
Benzo(g,h,i)perylene
250
U . -
58-90-2
2,3,4,6-Tetrachlorophenol
250
U"
1 Cannot be separated from Diphenylamine
£>/((/&?- SOM01. ! (5/2C&17
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
Lab Name: DataChem Laboratories, Inc. ». Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345 \ Mod. Ref No.:
EPA SAMPLE NO'.
J86T1
SDG No.:¦J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Level: (LOW/MED) LOW
% Moisture: 33
Lab Sample ID: 7120009010
(g/mL) g_
Lab File ID: NAA14C10
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5^0
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
(uL) ¦Date Extracted: 05/01/2007
¦ Date Analyzed: 05/09/2007
GPC Cleanup: (Y/N) Y^_
pH: 7 . 0
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.03
530
JN
. Unsaturated Hydrocarbon
4.11
110
JW
2416-20-8
Hexadecenoic acid, Z-ll-'
12 . 62
320
JN
57-10-3
n-Hexadecanoic acid
12 .76
310
JN
Unknown oxyhydrocarbon
16.84
150
JiM
67860-04-2
Oxirane, heptadecyl-
- 17.54
210
JN
Polycyclic hydrocarbon
19.14
530
JN
Unknown oxyhydrocarbon
' 19.27
- 120
J<\1
Polycyclic hydrocarbon
24.49
160
JNi
Polycyclic hydrocarbon
24 .70
470
¦ jM
-
E9667 962
Total Alkanes
N/A
1100
j
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
2.5
2 6*
27
28
29
30
2EPA-designated Registry Number.
/' i iV)' ?
SOM01.1
(5/20?3)8
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA.SHEET
EPA SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories, Inc'i.
Lab Code: DATAC Case No.: 36345; t
Matrix; (SOIL/SED/WATER) SOIL i
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009011
Sample wt/vol: 30 . 0
(g/mL)
Lab File ID: NAB05C11
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) S.ONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—r—
Injection Volume: 1. 0
(uL) Date Extracted: 05/01/2007
GPC Cleanup: (Y/N)
(uL) GPC Factor: 2 . 0
pH: 7_J.
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7 '
Benzaldehyde¦
Z60 ¦6-6'
•cf- (J
108-95-2
Phenol
260
U ¦
111-44-4
Bis(2-chlproethyl)ether
260
U
95-57-8
2-Chlorophenol
2 60
U
95-48-7
2-Methylphenol
¦ 260
u
108-60-1
2,2'-Oxybis(1-chloropropane)
260
u
98-86-2
Acetophenone
54
j
106-44-5
,4-Methylphenol
260
- u
621-64-7
N-Nitroso-di-n-propylamine
260
u
67-72-1
Hexachloroethane
260
U '
98-95-3
Nitrobenzene.
260
u
78-59-1
Isophorone
260
u
88-75-5-
2-Nitrophenol
260
u
105-67-9
2, 4-Dimethylphenol
260
u
111-91-1
Bis(2-chloroethoxy)methane
260
u
120-83-2
2,4-Dichlorophenol
260
u
91-20-3
Naphthalene
,260
u
106-47-8
4-Chloroaniline
260
u .
87-68-3.
Hexachlorobutadiene
260
u
105-60-2
Caprolactam
260
u
59-50-7
4-Chloro-3-methylphenol
260
u
91-57-6
2-Methylnaphthalene
260
u
77-47-4
Hexachlorocyclopentadiene
260
u
88-06-2
2,4,6-Trichlorophenol
260
u
95-95-4
2,4,5-Trichlorophenol
260
u
92-52-4
1,1'-Biphenyl
260
u
91-58-7
2-Chloronaphthalene
260
u
88-74-4 ¦' •
2-Nitroaniline
510
u
131-11-3
Dimethylphthalate
260
u
606-20-2
2,6-Dinitrotoluene
260
u
208-96-8
Acenaphthylene
260
' u
99-09-2
3-Nitroaniline
510
u
83-32-9
Acenaphthene
260
u
6 /it fat
SOM01.1 (5/2024)2
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories, Inc.1 i. Contract: EP-W-05-02 6
Lab Code: DATAC Case No.-: 36345; 1; Mod. Ref No.:
Matrix: (SOIL/SED/WATER) SOIL r
SDG No.: J8 6R0
Lab Sample ID: 7120009011
Sample wt/vol: 30. 0
Level: (LOW/MED) LOW
% Moisture: 36
(g/mL)
Decanted: (Y/N) N
Concentrated Extract Volume: 50,0
(uL)
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.1 '
Lab File ID: NAB05C11
Extraction: (Type) SONC
Date Received: 04/30/2007
Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/.kq
Q
51-28-5-
2,4-Dinitrophenol
510
urr
100-02-7
4-Nitrophenol
510
U
132-64-9
Dibenzofuran
260
u
1-21-14-2
2,4-Dinitrotoluene
260
V
84-66-2
Diethylphthalate
260
u
86-73-7
Fluorene
260
u
7005-72-3
4-Chlorophenyl-phenylether
260
u
100-01-6
4-Nitroaniline
510
- u
534-52-1
4,6-Dinitro-2-methylphenol -
510
u
86-30-6
N-Nitrosodiphenylamine1
260
u
95-94-3 -
1,2,4,5-Tetrachlorobenzene
260
u
101-55-3
4-Bromophenyl-phenylether
2 60
u
118-74-1
Hexachlorobenzene
¦ 260
u
1912-24-9
Atrazine
2 60
u
87-86-5
Pentachlorophenol
510
u
85-01-8
Phenanthrene-
2 60
u
120-12-7
Anthracene
2 60
u
86-74-8
Carbazole
' 260
u '
84-74-2
Di-n-butylphthalate
260
u
206-44-0
Fluoranthene
' 260
¦ u
129-00-0
Pyrene
260
u
85-68-7
Butylbenzylphthalate
' 13
J
91-94-1
3, 3'-Dichlorobenzidine
260
u
56-55-3
Benzo(a)anthracene
260
u
218-01-9
Chrysene
260
u
117-81-7
Bis(2-ethylhexyl)phthalate
39
J
117-84-0
Di-n-octylphthalate
260'
u
205-99-2
Benzo(b)fluoranthene
260
u .
207-08-9
Benzo(k)fluoranthene
260
u
50-32-8
Benzo(a)pyrene
260
. u
193-39-5
Indeno(1,2,3-cd)pyrene
260
u
53-70-3
Dibenzo(a,h)anthracene
260
'U
191-24-2
Benzo(g,h,i)perylene
260
u
58-90-2
2,3,4,6-Tetrachlorophenol
260
u
1 Cannot be separated from Diphenylamine
SOM01.1 (5/20
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories, Inc.:
Lab Code: DATAC Case No.: 3634 5; v Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Contract: EP-W-05-026
No. :
SDG No.: J8 6R0
Lab Sample ID: 7120009011
(g/mL)
Lab File ID: NAB05C11
Level: (LOW/MED) LOW
% Moisture: 36
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5Q0 (uL)
Injection Volume: 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y_
pH: 7 .1
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
I—1
o
260
JN
Po'lycyclic hydrocarbon
19.17
• 600
JNi
Polycyclic hydrocarbon
24.78
490
JN
i
E9667 96 2
Total Alkanes
N/A
550
J '
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26'
27
28
2 9
30
?EPA-designated Registry Number.
£>/t \ Iq-{-
SOM01.1 (
5/20?#)4
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories, Inc. ». Contract: EP-W-05-026
Lab Code: DATAC Case No.: 3-6345 y Mod. Ref No.: SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL i ¦ Lab Sample ID:''7120009012
Sample wt/vol: 30.0 (q/mL) q Lab File ID: NAB06C12
Level: (LOW/MED) LOW Extraction: (Type) SONC
% Moisture: 37 __ Decanted: (Y/N) N • Date Received: 04/30/2007
Concentrated Extract Volume: 5f00 (uL) Date Extracted: 05/01/2007
Injection Volume: 1. 0 . (uL) GPC Factor: 2 . 0 Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y pH: 7 . 8 Dilution Factor: 1. 0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7 ¦
Benzaldehyde
tJ-U
108-95-2
Phenol
270
u
:111-4 4-4
Bis(2-chloroethyl)ether
• 270
u
95-57-8
2-Chlorophenol
270
u
95-48-7
2-Methylphenol
270
u
108-60-1
2,21-Oxybis(1-chloropropane)
270
u
98-86-2
Acetophenone
45
J
106-44-5
4-Methylphenol
' 270
" u
621-64-7
N-Nitroso-di-n-propylamine
270
u
67-72-1
Hexachloroethane
270
u
98-95-3
Nitrobenzene
270
u
78-59-1
Isophorone
¦ 270
u
88-75-5
2-Nitrophenol
270
U -
105-67-9
2,4-Dimethylphenol
270
u
111-91-1
Bis(2-chloroethoxy)methane
270
U'
120-83-2
2,4-Dichlorophenol
270
u
91-20-3
Naphthalene
270
U
106-47-8
4-Chloroaniline ¦
270
u
87-68-3
Hexachlorobutadiene
270
u
105-60-2
Caprolactam
270
u
59-50-7
4-Chloro-3-methylphenol
270
u
91-57-6
2-Methylnaphthalene
270
u
77-47-4
Hexachlorocyclopentadiene
270
u
88-06-2
2,4,6-Trichlorophenol
270
u
95-95-4
2,4,5-Trichlorophenol
270
u
92-52-4
1,1'-Biphenyl
270
u
91-58-7
2-Chloronaphthalene
270
u
88-74-4
2-Nitroaniline
520
u
131-11-3
Dimethylphthalate
270
u
606-20-2
2,6-Dinitrotoluene
270
u
208-96-8
Acenaphthylene
¦270
u '
99-09-2
3-Nitroaniline
520
u
83-32-9
Acenaphthene
270
u
S-Ztl/Ol SOM01.1 (5/20?)§£
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories, Inc* ;
Lab Code: DATAC Case No.: 36345 >'
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Level: (LOW/MED) LOW
% Moisture: 37
Lab Sample ID: 7120009012
(g/mL)
Lab File ID: NAB06C12
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
f
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.8
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS' NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/kg
Q
51-28-5 -
2,4-Dinitrophenol
520
or
100-02-7
4-Nitrophenol
520
u
132-64-9
Dibenzofuran
270
u
121-14-2
2,4-Dinitrotoluene
270
u
84-66-2
Diethylphthalate
270
u
86-73-7
Fluorene
270
u
7005-72-3
4-Chlorophenyl-phenylether
270
u
100-01-6
4-Nitroaniline
520
¦¦ u
534-52-1
4,6-Dinitro-2-methylphenol
520
u
86-30-6
N-Nitrosodiphenylamine1
270
u
95-94-3
1,2,4,5-Tetrachlorobenzene
270
u
101-55-3
4,-Bromophenyl-ph'enyl ether
270
u
118-74-1
Hexachlorobenzene
270
¦. u
1912-24-9
Atrazine
270
u
87-86-5
Pentachlorophenol
520
u
CO
I—1 '
0
1
LO :
COj
Phenanthrene .
270
u
120-12-7
Anthracene
270
u
86-74-8
Carbazole
270
u
84-74-2
Di-n-butylphthalate
'270
u
206-44-0
Fluoranthene
270
u.
129-00-0
Pyrene
270
u
85-68-7
Butylbenzylphthalate
270
u
91-94-1
3, 3'.-Dichlorobenzidine
270
u
56-55-3 .
Benzo(a)anthracene
27 0
u
218-01-9
Chrysene
270
u
117-81-7
Bis(2-ethylhexyl)phthalate
23
J ¦
117-84-0
Di-n-octylphthalate
270
u
205-99-2
Benzo(b)fluoranthene
270
u
¦207-08-9
Benzo(k)fluoranthene
270
u
50-32-8
Benzo(a)pyrene
270
u
193-39-5
Inde.no (1, 2, 3-cd) pyrene
27.0
u
53-70-3
Dibenzo(a,h)anthracene
270
u
191-24-2
Benzo(g,h,i)perylene
270
u
58-90-2 '
2,3,4,6-Tetrachloropheriol
270
u
1 Cannot be separated from Diphenylamine
£—¦
Jm/cTZ
SOM01.1 (5/2025)6
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7120009012
(g/mL)
Lab File.ID: NAB06C12
Level: (LOW/MED) LOW
•% Moisture: 37
Extraction: (Type) SONC
Decanted: '(Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 5^)0
Injection Volume: 1. 0 (uL) GPC Factor: 2.0
. (uL) Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y_
pH: 7.8
Dilution Factor: 1.0
CONCENTRATION UNITS: (ug/L or u-g/kg) uq/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 . 01
460
JN
Polycyclic hydrocarbon
19.17
620
JN
Polycyclic hydrocarbon
24.77
640
JN .
'
¦
E9667 962
Total Alkanes
N/A
400
J
01
02
03
04
05
06
07
08
0-9
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26'
27
28
29
30
2EPA-designated Registry Number.
SOM01.1 (5/20 35)7
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inc; Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345 V Mod. Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
Lab Sample. ID: 7120009013
(g/mL) g_
Lab File ID: NAB07C13
Level: (LOW/MED) LOW
% Moisture: 32
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/3'0/2007'
Concentrated Extract Volume: 500 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/10/2007
GPC Cleanup: (Y/N) Y_
pH: 6^
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7
Benzaldehyde
'250
108-95-2 '
Phenol
250
U
111-44-4
Bis(2-chloroethyl)ether
250
U
95-57-8
2-Chlorophenol
250
u
95-48-7
2-Methylphenol
250
u
108-60-1
2,2'-Oxybis(1-chloropropane)
250
U'
98-86-2
Acetophenone
52
J-
106-44-5
. 4-Methylphenol
¦ 250
U
621-64-7
N-Nitroso-di-n-propylamine
250
¦ u
67-72-1
Hexachloroethane
250
u
98-95-3
Nitrobenzene
250
u
78-59-1
Isophorone
250
u
88-75-5 '
2-Nitrophenol
250
U'
105-67-9
2,4-Dimethylphenol
250
u
111-91-1
Bis(2-chloroethoxy)methane
250
u.
120-83-2
2,4-Dichlorophenol
250
u
91-20-3
Naphthalene
250
u
106-47-8
,4-Chloroaniline
250
u
87-68-3
Hexachlorobutadiene
250
u
105-60-2
Caprolactam
250
u
59-50-7-
4-Chloro-3-methylphenol
250
u
91-57-6
2-Methylnaphthalene
250
u
77-47-4
Hexachlorocyclopentadiene
250
u
88-06-2
2,4,6-Trichlorophenol
250
u
95-95-4.
2,4,5-Trichlorophenol
250
u
92-52-4
1,1'-Biphenyl
250
u
91-58-7 '
2-Chloronaphthalene
250
u
88-74-4
2-Nitroaniline .
490-
u
131-11-3
Dimethylphthalate
250
u
606-20-2
2, 6-Dinitrotoluene
250
u
208-96-8
Acenaphthylene
250
u
99-09-2
3-Nitroaniline
490
u
83-32-9
Acenaphthene
250
u
SOM01.1 ( 5/2o3§P
-------
.IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inci.
Lab Code: DATAC Case No.: 36345:
Mod.
Contract: EP-W-05-026
Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab 'Sample ID: 7120009013
(g/mL) g_
Lab File ID: NAB07C13
Level: (LOW/MED) LOW
% Moisture: 32 .
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/3Q/2007
Concentrated Extract Volume: 500.
(uL) Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2,0
pH: 6^8
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS 'NO.
COMPOUND - '
CONCENTRATION UNITS:
(uq/L or ug/kq) ug/kq
Q
51-28-5 "
2,4-Dinitrophenol-
490
UT
100-02-7
4-Nitrophenol
490
U
132-64-9
Dibenzofuran
250
U
' 121-14-2
2,4-Dinitrotoluene
250
U
84-66-2
Diethylphthalate
250
u
86-73-7.
Fluorene
250
u
7005-72-3
4-Chlorophenyl-phenylether
250
u
100-01-6
4-Nitroaniline
490
" u
534-52-1
4,6-Dinitro-2-methylphenol
490
u
8.6-30-6
N-Nitrosodiphenylamine1
250
u
95-94-3
1,2,4,5-Tetrachlorobenzene
250
u
101-55-3
4-Bromopheny.l-phenylether
250
u
118-74-1,
Hexachlorobenzene
'250
¦ u
1912-24-9
Atrazine
' 250
u
87-86-5
Pentachlorophenol
490
u
OO
1
i—1
0
1
LO
OO
Phenanthrene
12
¦ J
120-12-7
Anthracene -
250
u
86-74-8
Carbazole
250
u
84-74-2
Di-n-butylphthalate
¦ 250
u
206-44-0
Fluoranthene
¦21
J -
129-00-0
Pyrene
. 19
J
85-68-7
Butylbenzylphthalate
250
u
91-94-1
3,3'-Dichlorobenzidine
250
u
56-55-3
Benzo(a)anthracene
"2SQ9-r£
C? O
218-01-9
Chrysene
11
J
117-81-7
Bis (2-ethylhexyl)phthalate
49
. J
117-84-0
Di-n-octylphthalate
250
u
205-99-2
Benzo(b)fluoranthene
14
J
207-08-9
Benzo(k)fluoranthene
250
u
50-32-8
Benzo(a)pyrene
250
u
193-39-5
Indeno(1,2, 3-cd) pyrene
250
u
53-70-3
Dibenzo(a,h)anthracene
250
u
191-24-2
Benzo(g,h,i)perylene
250
u
58-90-2
2,3,4,6-Tetrachlorophenol
250
u
1 Cannot be separated from Diphenylamine
<£/<( /fefSOMOl.l (5/20
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY' IDENTIFIED COMPOUNDS'
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inc:
Lab Code: DATA.C Case No.: 36345:
. Contract: EP-W-05-026
Mod..Ref No.:
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL,
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 32
Lab Sample ID: 7120009013
(g/mL) g_
Lab File ID: NAB07C13
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
—r—
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1.0
GPC Cleanup: (Y/N)
(uL) GPC Factor: 2.0
pH: 6J3 ^
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
COMPOUND NAME
' RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.02
450
JN
2416-20-8
Heixadecenoic acid, Z-ll-
12. 63
320
JN
57-10-3
n-Hexadecanoic acid
12 .76
220
JN
Unknown oxyhydrocarbon
15. 98
14 0
JM
Unknown oxyhydrocarbon
16.30
130
JN
Unknown oxyhydrocarbon
16.86
120
JM
91-76-9
1,3,5-Triazine-2,4-diamine, 6-phenyl-
17.09
140
" JN
Unknown oxyhydrocarbon
17.58
100
JM
Polycyclic hydrocarbon
19.18
520
JM
Polycyclic hydrocarbon
24 . 54
110
JH
Polycyclic hydrocarbon
24.78
400
JM-
*
E9667 96 2
Total Alkanes
N/A
990
J '
01
02
03
04
05
•06
07'
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26'
27
28
29
30
!EPA-designated Registry Number.
SOM01.1 (5
/20??)1
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA'SHEET
EPA SAMPLE NO.
J86T5
Lab Name: DataChem Laboratories, Inc. ».
Lab Code: DATAC Case No.: 36345
Matrix: (SOIL/SED/WATER) SOIL J_
Sample wt/vol: 30. 0 (g/mL) 3
Level: (LOW/MED) LOW
% Moisture: 23
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R0
Lab Sample ID: 7120009014
Lab File ID: NAB08C14
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
(uL)
Date.Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup:¦(Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7.5
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kg) ug/kg
Q
100-52-7 '
Benzaldehyde
220
¦3 (J
108-95-2
Phenol
220
U
111-44-4
Bis(2-chloroethyl)ether
220
. U
95-57-8
2-Chlorophenol
220
u
95-48-7
2-Methylphenol
220
u
108-60-1
2,2'-Oxybis(1-chloropropane)
220
u
"98-8 6-2
Acetophenone
41
J
106-44-5
4-Methylphenol
220
u
6.21-64-7
N-Nitroso-di-n-propylamine
220
u
67-72-1
Hexachloroethane
220
u
98-95-3
Nitrobenzene
220
u
78-59-1
Isophorone
220
u
88-75-5
2-Nitrophenol
220
u
105-67-9
2,4-Dimethylphenol
220
u
111-91-1
Bis(2-chloroethoxy)methane
.220
u
120-83-2
2,4-Dichlorophenol
. 220
u
91-20-3
Naphthalene
220
u
106-47-8
4-Chloroaniline
220
. u
87-68-3
Hexachlorobutadiene
. 220
u
105-60-2
Caprolactam
. 220
u
59-50-7
4-Chloro-3-methylphenol
220
u
91-57-6
2-Methylnaphthalene
220
u
77-47-4
Hexachlorocyclopentadiene
220
u
88-06-2.
2,4,6-Trichlorophenol
220
u
95-95-4
2,4,5-Trichlorophenol
220
u
92-52-4
1,1'-Biphenyl
220
u
91-58-7
2-Chloronaphthalene ¦
220
u
88-74-4
2-Nitroaniline
430
u
131-11-3
Dimethylphthalate
220
u
606-20-2
2,6-Dinitrotoluene
220
u
208-96-8
Acenaphthylene
220
u
99-09-2
3-Nitroaniline
430
u
83-32-9 '
Acenaphthene
220
u
£¦/(< /£?
SOM01.1 (5/201
39j6
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T5
Lab¦ Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case'No.: 36345
Mod.
Contract: EP-W-05-026
Ref No.:
a_
SDG No.: J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7120009014
(g/mL) 3__
Lab File ID: NAB08C14
Level: (LOW/MED) LOW
% Moisture: 23
Extraction: (Type) SONC
Decanted: (Y/N) N_
Date Received: 04/30/2007
Concentrated Extract Volume: 5.00
(uL)
Date Extracted: 05/01/2007
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.5
Date Analyzed: 05/10/2007
Dilution Factor: l.'O
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kq) ug/kg
Q
51-28-5 '
2,4-Dinitrophenol
430
UJ
100-02-7
4-Nitrophenol .
430
U
:132-64-9
Dibenzofuran
220
u
121-14-2
2,4-Dinitrotoluene
220
u
84-66-2
Diethylphthalate
220
u
.86-73-7
Fluorene
220
u
7005-72-3
4-Chlorophenyl-phenylether
220
u
100-01-6
4-Nitroaniline
430
u
534-52-1
4,6-Dinitro-2-methylphenol
430
u
86-30-6
N-Nitrosodiphehylamine1
220
u
95-94-3
1,2,4,5-Tetrachlorobenzene
220
u
101-55-3
4-Bromophenyl-phenylether
220
u
118-74-1
Hexachlorobenzene
220
u '
1912-24-9
Atrazine
220
u
87-86-5
Pentachlorophenol
430
u
85-01-8
Phenanthrene .
220
u
120-12-7
Anthracene
220
u
86-74-8
Carbazole
220
u
84-74-2
Di-n-butylphthalate
.8.8
J
206-44-0
Fluoranthene
220
u ¦
129-00-0
Pyrene
220
u
85-68-7
Butylbenzylphthalate ' -
9.4
J
91-94-1
3,3'-Dichlorobenzidine
220
u
56-55-3
Benzo(a)anthracene
220
u
218-01-9
Chrysene
220
u
117-81-7
Bis(2-ethylhexyl)phthalate
20
J
117-84-0
Di-n-octylphthalate
220
u
205-99-2
Benzo(b)fluoranthene ¦
• 220
¦u
207-08-9'
Benzo(k)fluoranthene
220
u
50-32-8
Benzo(a)pyrene
220
u
193-39-5 .
Indeno(1,2,3-cd)pyrene
220
,u
53-70-3
Dibenzo(a,h)anthracene
220
u
191-24-2
Benzo(g,h,i)perylene
220
u
58-90-2
2, 3-, 4 ,-6-Tetrachlorophenol
220
U ¦¦
1Cannot be separated from Diphenylamine
K/n/rPf SOM01-1 <
5/2C&97
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86T5
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.:.J8 6R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 23
Lab Sample ID: 7120009014
(g/mL)
Lab File ID: NAB08C14
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 500
f
Injection Volume: 1. 0
(uL)
Date Extracted: 05/01/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.5
Date Analyzed: 05/10/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS•NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1, 2, 2-tetrachloro-
4.01
220
JN
Polycyclic hydrocarbon
19.17
260
JN
Polycyclic hydrocarbon
24 .76
230
JH
v
E9667 962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
2 6-
27
28
29
30
2EPA-designated Registry Number.
£>/tl /S~f SOM01.1 (5/20^^)8
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc.;.'. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345: y Mod. Ref No.
Matrix:' (SOIL/SED/WATER) SOIL j
SDG No.: J8 6R0
Lab Sample ID: 7120009015
Sample wt/vol: 3Q . 0
(g/mL) 2_
Lab File ID: NAF04C15
Level: (LOW/MED) LOW
% Moisture: 4 0
Extraction: (Type) SONC
•Decanted: (Y/N) N
Date Received: 04/30/2007
Concentrated Extract Volume: 5(j)0 (uL)
Injection Volume: 1. 0 (uL) GPC Factor: 2 . 0
Date Extracted: 05/01/2007
Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
pH: 7 . 4
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
2 SO
3- Li
108-95-2
Phenol
2JsC
*(J
111-44-4
Bis (2-chloroet-hyl) ether
280
U
95-57-8
2-Chlorophenol
280
¦u
95-48-7
2-Methylphenol
280
u
108-60-1
2, 2 '-Oxybis (1-chloropr.opane)
280
u
98-86-2
Acetophenone
48
J
106-4.4-5-
4-Methylphenol
280
" u
621-64-7
N-Nitroso-di-n-propylamine
280
u
67-72-1
Hexachloroethane
280
u
98-95-3
Nitrobenzene
280
u
78-59-1
Isophorone
280
u
88-75-5.
2-Nitrophenol
280
u
105-67-9
2,4-Dimethylphenol
280
u
111-91-1
Bis(2-chloroethoxy)methane
280
u
120-83-2
2,4-Dichlorophenol
280
u
91-20-3
Naphthalene ' '
280
u
106-47-8
4-Chloroaniline
.280
u
87-68-3
Hexachlorobutadiene
280
u
105-60-2
Caprolactam
280
u
59-50-7
4-Chioro-3-methylphenol
280
u
91-57-6
2-Methylnaphthalene
280
u
77-47-4
Hexachlorocyclopentadiene
280
u
88-06-2
2, 4, 6-Trichlorophenol.
280
u
95-95-4
2,4,5-Trichlorophenol
¦280
u
92-52-4
1,1'-Biphenyl
280
u
91-58-7
2-Chloronaphthalene
280
¦ u
88-74-4
2-Nitroaniline
550
u
131-11-3
Dimethylphthalate
280
u
606-20-2
2,6-Dinitrotoluene
280
u
208-96-8
Acenaphthylene
280
u
99-09-2 .
3-Nitroaniline
550
u
83-32-9
Acenaphthene
280.
u
SOM01.1 (
5/20$ 9)9
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 10
1200 Sixth Avenue
Seattle, WA 98101
June 4, 2007
MEMORANDUM
SUBJECT:
FROM:
TO:
CC:
The quality assurance (QA) review of six soil and two water samples collected from the above referenced site has
been completed. The samples were analyzed for SVOCs, Pesticides, and PCBs in accordance with the USEPA
Contract Laboratory Program (CLP) Statement of Work (SOW) for Multi-Concentration Organic Analysis
* (SOM01.1) by Datachem Laboratories, Inc. in Salt Lake City, Utah. The following samples were evaluated in
this validation report:
SPG: J86R1
J86R1 J86R2 J86R3 J86R4 J86R5 J86T6
J86T9 J86W1
DATA QUALIFICATIONS
, The following comments refer to the laboratory performance specification outlined in the Quality Assurance
Project Plan dated April, 2007, USEPA CLP SOW for Organic Analysis (SOM01.1, 05/2005), and applicable
criteria set forth in the USEPA CLP National Functional Guidelines for Organic Data Review (01/2005). Note
that some of the analytical data reported may be qualified based on the professional judgment of the data
reviewer.
The conclusions presented herein are based on the information provided for the review.
Holding Time - Acceptable
All of the samples met the extraction and analytical holding time criteria for SVOC,
Printed on Recycled Paper
W
PRO&
Data validation report for the Semi-Volatile Organics (SVOCs), Organochlorine Pesticides
(Pests) and Polychlorinated Biphenyls (PCBs) analysis of samples from the Drums NE Marine
Drive SI Site Case: 36345 SDG: J86R1
Raymond Wu, QA Chemist
Office of Environmental Assessment < *— t/Ot
Joanne Labaw, Site Assessment Manager
Office of Environmental Cleanup
Alexis Ande, Start-3 Site Assessment Project Leader
Techlaw, Inc.
-------
Data Validation Report
Drum NE Marine Drive SI
Case 36345 SDG I86R1
Page 3 of 5
Analytical Sequence - Acceptable
All of the standards, blanks, samples, and QC samples were analyzed in accordance with the SOW specified
analytical sequence. The retention times as monitored by the internal standards (SVOCs) and surrogates
(Pesticides) were within the specified RT windows. All of the sample analyses were within an acceptable 12 hour
QC period and were bracketed by a technically acceptable CCV check standards. None of the data was qualified
on this basis. ?
Surrogates/Deuterated Monitoring Compound Recoveries - Acceptable
Surrogates or deuterated monitoring compounds (DMCs) are known concentrations of isotope-labeled acid and
base/neutral or polynuclear hydrocarbon compounds added to the field and QC samples prior to extraction for
SVOC analyses to monitor the laboratory's performance and efficiency during sample processing, extraction and
analysis. The following is the list of DMCs/surrogates added to' all field and QC samples prior to sample
extraction:
DMCs (Water SVOCs)
Recovery
Limits (%)
DMCs (Water SVOCs)
Recovery
Limits (%)
Phenol-d-5 (PHL)
39-106
Dimethylphthalate-d6 (DMP)
47-114
Bis(2-chloroethyl)ether-d8 (BCE)
40-105
Acenapthylene-d8 (ACY)
41-107
2-chlorophenol-d4 (2CP)
41-106
4-Nitrophenol-d4 (4NP)
33-116
4-Methylphenol-d8 (4MP)
25-111
Fluorene-dlO (FLR)
42-111
Nitrobenzene-d4 (NBZ)
43-108
4,6-Dinitro-2-methylphenol-d2 (NMP)
22-104
2-Nitrophenol-d4 (2NP)
40-108
Anthracene-dlO (ANC)
44-110
2,4-Dichlorophenol-d3 (DCP)
37-105
Pyrene-dlO (PYR)
52-119
4-Chloroaniline-d4 (4CA)
1-145
Benzo(a)pyrene-dl2 (BAP)
32-121
DMCs (Soil SVOCs)
Recovery
Limits (%)
DMCs (Soil SVOCs)
Recovery
Limits (%)
Phenol-d5 (PHL)
17-103
Dimethylphthalate-d6 (DMP)
43-111
Bis(2-chloroethyl)ether-d8 (BCE)
12-98
Acenapthylene-d8 (ACY)
20-97
2-chlorophenol-d4 (2CP)
13-101
4-Nitrophenol-d4 (4NP)
16-166
4-Methylphenol-d8 (4MP)
8-100
Fluorene-dlO (FLR)
40-108
Nitrobenzene-d4 (NBZ)
16-103
4,6-Dinitro-2-methylphenol-d2 (NMP)
1-121
2-Nitrophenol-d4 (2NP)
16-104
Anthracene-dlO (ANC)
22-98
2,4-Dichlorophenol-d3 (DCP)
23-104
Pyrene-dlO (PYR)
51-120
-------
Data Validation Report
Dram NE Marine Drive SI
Case 36345 SDGJ86R1
Page 5 of 5
Tentatively Identified Compounds ¦
Chromatographic peaks in the samples' SVOC runs that are not target compounds, surrogates or internal
standards with areas > 10% of the nearest IS must be tentatively identified by the laboratory using a mass spectral
search of the NIST library.
Common laboratory artifacts and peaks that are found in both the sample and the blanks were crossed out by the
reviewer and flagged unusable, "R". The rest of the TICs identified by the lab on the Form I were qualified as
tentatively identified at estimated concentrations, "IN", with an unknown bias.
Laboratory Contact
The laboratory was not contacted for this review.
Overall Assessment
The total number of data points was 776. As the result of the data validation, data results were qualified as
follows: 2.6% of the total data points were qualified as non-detects, "U".
The data, as qualified, are acceptable and can be used for all purposes.
Data Qualifiers
U
The analyte was not detected at or above the reported result.
J
The analyte was positively identified. The associated numerical result is an
estimate.
UJ
The analyte was not detected at or above the reported estimated result. The
associated numerical value is an estimate of the quantitation limit of the analyte in
this sample.
R
The data are unusable for all purposes.
N
There is evidence the analyte is present in this sample.
JN
There is evidence that the analyte is present. The associated numerical result is an
estimate.
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6IO.
Lab Name: DataChem Laboratories, Inc.¦
Lab Code: DATAC Case No.: 36345-
_ Contract: EP-W-05-026
Mod. Ref No.':
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
(g/mL)
Level: (LOW/MED) LOW
% Moisture: 22
Decanted: (Y/N) N
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
GPC Cleanup: (Y/N) Y_
(uL). 'GPC Factor: 2.0
' pH: 8 .1 .
Lab Sample ID: 7117018001
Lab File ID: NZW08C01
Extraction: (Type) SONC
Date Received: 04/27/2007
Date Extracted: 04/29/2007
Date" Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
100-52-7
Benzaldehyde
33
J
108-95-2
Phenol
220
U
111-44-4
Bis(2-chloroethyl)ether
220
U
95-57-8
2-Chlorophenol
220
U
95-48-7
2-Methylphenol
220
u
108-60-1
2,2'-Oxybis(1-chloropropane)
220
u
98-8 6-2
Acetophenone
20
J
106-44-5
4-Methylphenol
220
u
621-64-7
N-Nitroso-di-n-propylamine
220
u
67-72-1
Hexachloroethane
220
u
98-95-3
Nitrobenzene
220
u
78-59-1
Isophorone
220
u
88-75-5
2-Nitrophenol
220
u
105-67-9
2,4-Dimethylphenol
220
u
111-91-1
Bis (2-chloroethoxy)methane
220
' u
120-83-2
2,4-Dichlorophenol
220
, u
91-20-3
Naphthalene
220
u
106-47-8
4-Chloroaniline
220
u
87-68-3
Hexachlorobutadiene
220
u
105-60-2
Caprolactam
220
u
59-50-7
4-Chloro-3-methylphenol
220
u
91-,57-6
2-Methylnaphthalene
220
u
77-47-4
Hexachlor'ocyclopentadiene
220
u
88-06-2.
2,4,6-Trichlorophenol
220
u
95-95-4
2,4,5-Trichlorophenol
220
u
92-52-4
1,1'-Biphenyl
220
u
91-58-7
2-Chloronaphthalene
220
u
88-74-4
2-Nitroaniline
420
u
131-11-3
Dimethylphthalate
220
u
606-20-2
2,6-Dinitrotoluene
220
, u
208-96-8
Acenaphthylene
. ' 220
u
99-09-2
3-Nitroaniline
420
u
83-32-9
Acenaphthene ¦
220
u .
(U—i
vi(5/2004)1
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS'ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R1
Lab Name: DataChem Laboratories, Inc.
Contract: EP-W-05-026
Lab Code: DATAC
Case No.: 36345;: Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
(g/mL) g__
Level: (LOW/MED) LOW
% Moisture: 22
Decanted: (Y/N) N
Concentrated Extract Volume: 500
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 8.1
Lab Sample ID: 7117018001
Lab File ID: NZW08C01
Extraction: (Type) SONC
Date Received: 04/27/2007
(uL) Date Extracted; 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.,
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
420
U
100-02-7
4-Nitrophenol
420
' U
132-64-9
Dibenzofuran '
220
U .
121-14-2
2,4-Dinitrotoluene
220
u
84-66-2
Diethylphthalate
220
u
86-73-7
Fluorene
220
¦ u
7005-72-3
4-Chlorophenyl-phenylether
220
u '
100-01-6 '
4-Nitroaniline
420
u
534-52-1
4,6-Dinitro-2-methylphenol
420
u
86-30-6
N-Nitrosodiphenylamine1
220
u
95-94-3
1,2,4,5-Tetrachlorobenzene
220
u
101-55-3
4-Bromophenyl-phenylether
220
u .
118-74-1
Hexachlorobenzene
220
u
1.912-24-9
Atrazine
220
u
87-86-5
Pentachlorophenol
420
u
85-01-8
Phenanthrene ,
220
u
120-12-7
Anthracene
220
. u
86-74-8
Carbazole
220
u
84-74-2
Di-n-butylphthalate
220
u
206-44-0
Fluoranthene
220
u
129-00-0
Pyrene
220
u
85-68-7
Butylbenzylphthalate
. . 220
u
91-94-1
3,3'-Dichlorobenzidine
220
u
56-55-3
Benzo(a)anthracene
220
u
218-01-9
Chrysene
220
u
117-81-7
Bis(2-ethylhexyl)phthalate
220
u
117-84-0
Di-n-octylphthalate
220
¦ u
205-99-2
Benzo (b). fluoranthene
220
u
207-08-9
Benzo(k)fluoranthene.
220
u
50-32-8
Benzo(a)pyrene
220
u
193-39-5'
Indeno(l,2,3-cd)pyrene
220
u
53-70-3
Dibenzo(a,h)anthracene
220
u
191-24-2
Benzo(g,h,i)perylene -
220
u
58-90-2
2,3,4,6-Tetrachlorophenol
220
u
1 Cannot be separated from Diphenylamine
S/3l/o:? SOM01.1 (5/20o4£
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
JO ©Rl
Lab Name: DataChem Laboratories', Inc.
Lab Code: DATAC Case No. : 36345 :: Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Contract: EP-W-05-02 6
No. :
SDG No.: J8 6R1
Lab Sample ID: 7117018001
(g/mL) 3
Lab File ID: NZW08C01
Level: (LOW/MED) LOW
% Moisture: 22
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
Date Extracted: 04/29/20.07
GPC Cleanup: (Y/N) Y_
(uL) 'GPC Factor: 2.0
pH: 8.1
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.02
590
JN
2050-95-5
1-Butanol, 3-methyl-, carbonate (2:1)
4.21
210
JN
Unknown aromatic
7 .18
270
jM
Polycyclic hydrocarbon
19.13
230
JNl
Polycyclic hydrocarbon
24 . 69
98
JM
i
E9667962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
!EPA-designated Registry Number.
SOM01.1 (5/200 4j3
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R2
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
(g/mL) q_
Level: (LOW/MED) LOW
% Moisture: 25
Decanted: (Y/N) N
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
GPC Cleanup: (Y/N) Y_
(uL) fGPC Factor: 2.0
pH: 8.2
Lab Sample ID: 7117018002
Lab File ID: NZW09C02
Extraction: (Type) SONC
Date Received: 04/27/2007
Date Extracted: 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or.ug/kg) ug/kg
Q
100-52-7
Benzaldehyde ,
32
J
108-95-2
Phenol ¦
230
U
111-44-4
Bis (2-chloroethyl)ether
230
U
95-57-8 ¦
2-Chlorophenol
230
U
95-48-7
2-Methylphenol
230
u
108-60-1
2,2'-Oxybis(1-chloropropane)
230
u
98-8 6-2
Acetophenone
19
J
106-44-5
4-Methylphenol
230
.. u
621-64-7
N-Nitroso-di-n-propylamine
2.30
' u
67-72-1
Hexachloroethane
230
u
98-95-3
Nitrobenzene
230
u
78-59-1
Isophorone
230
u
88-75-5
2-Nitrophenol
230
u
105-67-9
2,4-Dimethylphenol
230
u
111-91-1
Bisi2-chloroethoxy)methane
230
u
120-83-2
2,4-Dichlorophenol
230
u
91-20-3
Naphthalene
230
u
106-47-8
4-Chloroaniline
230
u
87-68-3
Hexachlorobutadiene
.230
u
105-60-2
Caprolactam
230
u
59-50-7
4-Chloro-3-me'thylphenol
230
u
91-57-6
2-Methylnaphthalene
230
¦ u
77-47-4
Hexachlorocyclopentadiene
230
u
88-06-2
2,4,6-Trichlorophenol
230
u
95-95-4
2,4,5-Trichlorophenol
230
u
92-52-4
1,1'-Biphenyl
230
u
91-58-7
2-Chloronaphthalene
' 230
u
88-74-4
2-Nitroaniline
440
u
131-11-3
Dimethylphthalate
230
¦ u
606-20-2
2, 6-Dinitro.toluene
230
u
208-96-8
Acenaphthylene
230
u
99-09-2
3-Nitroaniline
440
u
83-32-9
Acenaphthene
230'
u
¦jn/bi SOM01.1 (5/200 §)3
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R2
Lab Name: DataChem Laboratories, Inc. .
Lab Code: DATAC Case No.: 36345-
Matrix: (SOIL/SED/WATER) SOIL
: Contract: EP-W-05-Q26
Mod. Ref No.:
SDG No.: J8 6R1
Lab Sample ID: 7117018002
Sample yrt/vol: 30 . 0
(g/mL) g_
Lab File ID: NZW09C02
Level: (LOW/MED) LOW
% Moisture: 25
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
.Injection Volume: 1. 0
(uL)
Date Extracted: 04/29/2007
¦GPC Cleanup: (Y/N) Y_
(uL) fGPC Factor: 2.0
PH: 8.2
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
440
U
100-02-7
4-Nitrophenol
440
U
132-64-9
Dibenzofuran
230
U
121-14-2
2,4-Dinitrotoluene
230
u
84-66-2
Diethylphthalate
230
u
86-73-7
Fluorene
230
u
7005-72-3
4-Chlorophenyl-phenylether
230
u
100-01-6 ¦
4-Nitroaniline
440
.. u
534-52-1
4,6-Dinitro-2-methylphenol
440
u
86-30-6
N-Nitrosodiphenylamine1
230
u
95-94-3
1,2,4,5-Tetrachlorobenzene
230
u
.101-55-3
4-Bromophenyl-phenylether .
230
u
118-74-1
Hexachlorobenzene
230
u
1912-24-9
Atrazine
230
u
87-86-5
Pentachlorophenol
440
u
85-01-8
Phenanthrene
230
u
120-12-7
Anthracene
230
u
86-74-8
Carbazole
230
u
84-74-2
Di-n-butylphthalate
230
u
206-44-0
Fluoranthene
230
u
129-00-0
Pyrene
230
u
85-68-7
Butylbenzylphthalate
230
u
91-94-1
3,3'-Dichlorobenzidine
230
u
56-55-3
Benzo(a)anthracene
230
u
218-01-9
Chrysene '
230
u
117-81-7
Bis(2-ethylhexyl)phthalate
230
u
117-84-0
Di-n-octylphthalate
230
u
205-99-2
Benzo(b)fluoranthene
230
u
207-08-9
Benzo(k)fluoranthene
230
u
50-32-8
Benzo(a)pyrene
230
u
193-39-5
Indeno (.1, 2, 3-cd) pyrene
230
u
53-70-3"
Dibenzo(a,h)anthracene
230
u
191-24-2
Benzo(g,h,i)perylene
230
u
58-90-2
2,3,4,6-Tetrachlorophenol
230
u
^Cannot be separated from Diphenylamine
S/310
SOM01.1 (5/200§^
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED, COMPOUNDS
EPA SAMPLE NO.
J86R2
Lab Name: Dat.aChem Laboratories, Inc. ¦
Lab Code: DATAC Case No. : 36345 Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL ' ¦
Sample wt/vol: 30.0 (g/mL) q
Contract: EP-W-05-026
No. :
SDG No.: J8 6R1
Lab Sample ID: 7117018002
Lab File ID: NZW0 9C02
Level: (LOW/MED) LOW
% Moisture: 25
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
Date Extracted: 04/29/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 8.2
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
GAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4.02
480
JN
Unsaturated Hydrocarbon
4.21
210
JH
Unknown aromatic
7.18
180
JN
Polycyclic hydrocarbon
19.14
210
JN
Polycyclic hydrocarbon
24.70
95
JM
E9667962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14,
15
16
17
18
19
20
21
22
23
24
25
26
27'
28
29
30
*EPA-designated Registry Number.
&A3I/C-
SOM01.1 (5/200§P
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6R3
Lab Name: DataChem Laboratories, Inc.¦
Lab Code: DATAC Case No.: 36345:;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Level: (LOW/MED) LOW
% Moisture: 25
(g/mL)
Decanted: (Y/N) N
Concentrated Extract Volume: 500
K
Injection Volume.: 1-. 0
(uL)
GPC .Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 8.2
Lab Sample ID: 7117018003
Lab File ID: NZW10C03
Extraction: (Type) SONC
Date Received: 04/27/2007
Date Extracted: 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/kq
Q
100-52-7
Benzaldehyde
35
J
' 108-95-2
Phenol
230
U
111-44-4
Bis(2-chloroethyl)ether
230
u
95-57-8
2-Chlorophenol
• 230
u
95-48-7
2-Methylphenol
230
u
108-60-1
2,2'-Oxybis(1-chloropropane)
230
u
98-86-2 . :
Acetophenone.
19
J
106-44-5
4-Methylphenol
230
.. u
621-64-7
N-Nitroso-di-n-propylamine
, 230
u
67-72-1
Hexachloroethane
230
u
98-95-3
Nitrobenzene
230
u
78-59-1
Isophorone
230
u
88-75-5
2-Nitrophenol
230
u
105-67-9
2,4-Dimethylphenol
230
u
111-91-1
Bis(2-chloroethoxy)methane
230
u
120-83-2
2,4-Dichlorophenol
230
u
91-20-3
Naphthalene
230
u
106-47-8
4-Chloroaniline
230
u
87-68-3
Hexachlorobutadiene
230
u
105-60-2
Caprolactam
230
u
59-50-7
4-Chioro-3-methylphenol
230
u
91-57-6
2-Methylnaphthalene
230
u
77-47-4
Hexachlorocyclopentadiene
230
u
88-06-2
2,4,6-Trichlorophenol
230
u
95-95-4 .
2,4,5-Trichlorophenol
230
u
92-52-4
1,1'-Biphenyl
230
u.
91-58-7
2-Chloronaphthalene
' 230
u
88-74-4
2-Nitroaniline
440
u
131-11-3
Dimethylphthalate
230
u
606-20-2.
2,6-Dinitrotoluene
230
u
208-96-8
Acenaphthylene
230
u
99-09-2
3-Nitroaniline
440
u
83-32-9
Acenaphthene
230
u
Sfel/ol SOM01..1 (5/2.00§£
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6M3
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345;
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER). SOIL
Sample wt/vol: 30 . 0
Level: (LOW/MED) LOW
% Moisture: 25
(g/mL) q__
Decanted: (Y/N) N.
Concentrated Extract Volume: 500
Injection Volume: 1. 0
(uL)
GPC Cleanup: (Y/N). Y_
(uL) fGPC Factor: 2.0
pH: 8^2
Lab Sample ID: 7117018003
Lab File ID: NZW10C03
Extraction: (Type) SONC
Date Received: 04/27/2007
Date Extracted: 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/kg
Q
51-28-5 ¦
2,4-Dinitrophenol
440
U
100-02-7
4-Nitrophenol
440
U
132-64-9
Dibenzofuran
230
¦ u
121-14-2 •
2,4-Dinitrotoluene
230
u
84-66-2
Diethylphthalate
- 230
u
86-73-7
Fluorene
230
u
7005-72-3
4-Chlorophenyl-phenylether
23'0
u
100-01-6
4-Nitroaniline
440
.. u
534-52-1
4,6-Dinitro-2-methylphenol
440
u
86-30-6
N-Nitrosodiphenylamine1
230
. u
95-94-3
1,2,4,5-Tetrachlorobenzene
230
u
101-55-3
4-Bromophenyl-phenyl.ether
230
u
118-74-1
Hexa.chlorobenz.ene
230
u
1912-24-9
Atrazine ¦¦'.'•
230
u
87-86-5
Pentachlorophenol
440
u
85-01-8
Phenanthrene
230
u
120-12-7
Anthracene
230
u
86-74-8
Carbazole
230
u
• 84-74-2 '
Di-n-butylphthalate
230
u
206-44-0
Fluoranthene ¦
230
u
129-00-0
Pyrene
230
u
85-68-7
Butylbenzylphthalate
230
u
91-94-1
3,3'-Dichlorobenzidine
230
u
•56-55-3 -
Benzo(a)anthracene
230
u
218-01-9
Chrysene
230
u
117-81-7
Bis(2-ethylhexyl)phthalate
230
u
117-84-0
Di-n-octylphthalate
230
u
205-99-2
Benzo(b)fluoranthene
230
u .
207-08-9
Benzo(k)fluoranthene
230
u
50-32-8
Benzo(a)pyrene
230
u
193-39-5
Indeno(1,2,3-cd)pyrene
230
u
53-70-3
Dibenzo(a,h)anthracene
230
u
191-24-2
Benzo(g,h,i)perylene
230
u
58-90-2
2,3,4,6-Tetrachlorophenol
230
u
^Cannot be separated from Diphenylamine
S'/il/cy- SOM01.1 (5/20of>)6
-------
. IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED.COMPOUNDS
EPA SAMPLE NO.
J86R3
Lab Name: DataChem Laboratories, Inc.¦
Lab Code: DATAC Case No.: 36345• Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL ¦ ' -
Sample wt/vol : 30. 0 (g/mL) q
Contract: EP-W-05-026
No. :
SDG No.: J8 6R1
Lab Sample ID: 7117018003
Lab File ID: NZW10C03
Level: (LOW/MED) LOW
% Moisture: 25
Extraction: (Type), SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500 (uL)
Injection Volume: 1. 0 (uL) fGPC Factor: 2 . 0
Date Extracted: 04/29/2007
Date Analyzed: 05/03/2007
GPC Cleanup: (Y/N) Y_
pH: 8.2
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 . 02
480
JN
Unsaturated Hydrocarbon
4.21
2 60
JKj
Unknown aromatic .
7.18
410
J.\i
Polycyclic hydrocarbon
19.13
230
Jf4
Polycyclic hydrocarbon
24.70
110
. Jf\i
• - ¦
E9667 962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27'
28
29
30
2EPA-des±gnated Registry Number.
O
OM01.1 (5/2009)
i)7
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6R.4
Lab' Name: DataChem Laboratories, Inc. - Contract: EP-W.-05-026
Lab. Code: DAT AC Case No.: 36345 Mod.' Ref No.: ' ' SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL ' ¦ ' Lab Sample ID: 7117018004
Sample wt/vol: 30 . 0 (q/mL) q Lab File ID: NZW11C04
Level: (LOW/MED) LOW Extraction: (Type) SONC
% Moisture: 25 Decanted: (Y/N) N Date Received: 04/27/2007
Concentrated Extract Volume: 500 (uL) Date Extracted: 04/29/2007
Injection Volume: 1 ¦ 0 (uL) fGPC Factor: 2.0 Date Analyzed: 05/03/2007
GPC Cleanup: (Y/N) Y pH: 8 . 4 • Dilution Factor: 1. 0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kg) uq/kq
Q
100-52-7
Benzaldehyde
29
J
108-95-2
Phenol
230
U
111-44-4
Bis(2-chloroethyl)ether
230
u
95-57-8
2-Chlorophenol
230
u
95-48-7
2-Methylphenol
230
u
108-60-1
2, 2'-Oxybis(1-chloropropane)
230
u
98-86-2
Acetophenone
21
7 J .
106-44-5
4-Methylphenol
230
¦ U
621-64-7
N-Nitroso-di-n-propylamine
230
U
67-72-1
Hexachloroethane
230
U
98-95-3
Nitrobenzene
230
U
78-59-1
Isophorone
230
u
88-75-5
2-Nitrophenol
230
u
105-67-9
2,4-Dimethylphenol
230
u
111-91-1
Bis(2-chloroethoxy)methane
230
u
120-83-2
2,4-Dichlorophenol
230
u
91-20-3
Naphthalene
230
u
106-47-8
4-Chloroaniline
230
u
87-68-3
Hexachlorobutadiene
230
u
105-60-2
Caprolactam
230
u
59-50-7 '
4-Chloro-3-methylphenol
230
u
91-57-6
2-Methylnaphthalene
230
u
77-47-4
Hfexachlorocyclopentadiene
230
u
¦8 8-06-2
2,4,6-Trichlorophenol
'230
¦ u
95-95-4
2,4,5-Trichlorophenol
230
u
92-52-4
1,1'-Biphenyl
230
u
91-58-7
2-Chloronaphthalene
230
u
88-74-4
2-Nitroaniline
440
u
131-11-3
Dimethylphthalate
230
u
606-20-2
2,6-Drnitrotoluene
230
u
208-96-8
Acenaphthylene '
230
u
99-09-2
3-Nitroaniline
440
u
83-32-9
Acenaphthene
230
u
S/3l/o7 SOM01.1 (5/2 00? 7
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J8 6K.4
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345:
_ ¦ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
(g/mL)
Level: (LOW/MED) LOW
% Moisture: 25
Decanted: (Y/N) N_
Concentrated Extract Volume: 500
(C
Injection Volume: 1.0,
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: £^4
Lab Sample ID: 7117018004
Lab File ID: N.ZW11C04
Extraction: (Type) SONC
Date Received: 04/27/2007
(uL) Date Extracted: 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND .
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
51-28-5
2,4-Dinitrophenol
440
U
100-02-7
4-Nitrophenol
4 40
U
, 132-64-9
Dibenzofuran
230
u
121-14-2
2,4-Dinitrotoluene
230
u
84-66-2
Diethylphthalate
230
u
86-73-7
Fluorene
230
u
7005-72-3
4-Chlorophenyl-phenylether
230
u '
100-01-6
4-Nitroaniline
44 0
- u
534-52-1
4,6-Dinitro-2-methylphenol
440
u
.86-30-6
N-Nitrosodiphenylamine1
230
u
95-94-3
1,2,4,5-Tetrachlorobenzene
230
u
101-55-3
4-Bromophenyl-phenylether
230
u
118-74-1
Hexachlorobenzene
230
0
1912-24-9
Atrazine
230
u
87-86-5
Pentachlorophenol
440
u
85-01-8
Phenanthrene
230
u
120-12-7
Anthracene
230
u
86-74-8 .
Carbazole
230
u
84-74-2
Di-n-butylphthalate
230
u
206-44-0
Fluorahthene
230
u
129-00-0
Pyrene
230
u
85-68-7 .
Butylbenzylphthalate
230
u
91-94-1
3,3' -Dichl.orobenzidine
230
u
56-55-3
Benzo(a)anthracene •
" 230
u
218-01-9
Chrysene
230
u ;
117-81-7
Bis(2-ethylhexyl)phthalate
230 2ri
117-84-0 .
Di-n-octylphthalate
230
u
205-99-2 '¦
Benzo(b)fluoranthene
230
u
207-08-9
Benzo(k)fluoranthene
230
u
50-32-8
Benzo(a)pyrene
230
u
193-3 9-5
Indeno(1,2,3-cd)pyrene
230
u
53-70-3
Dibenzo(a,h)anthracene
230
u
191-24-2
Benzo(g,h,i)perylene
230
u
58-90-2
2,3,4,6-Tetraehlorophenol
230
u
1 Cannot be separated from Diphenylamine
5~/&l/c7 SOM01 ¦1 (5/200?^
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY, IDENTIFIED COMPOUNDS
EPA'SAMPLE NO.
J86R4
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7117018004
(g/mL)
Lab File ID: NZW11C04
Level: (LOW/MED) LOW
% Moisture: 25
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
. f1'
Injection Volume: 1. 0
(uL)
Date Extracted: 04/29/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 8^_4
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kg
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
354-21-2
Ethane, 1,2,2-trichloro-l,1-difluoro-
4 .02
350
JN
Unsaturated Hydrocarbon
4 .23
150
JW
¦
Unknown aromatic
7 .18
370
JM
Polycyclic hydrocarbon
19.14
220
JN
Polycyclic hydrocarbon
24 .70
120
JM
-
E9667962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
2EPA-designated Registry Number.
^ " '
r/3//<>7 SOM01.1 (5/2-00 IP
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
iij@ 6R5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 .0
Lab Sample ID: 7117018007
(g/mL) 2_
Level: (LOW/MED) LOW
% Moisture: 29
Lab File ID: NZW14C07
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
P
Injection Volume: 1. 0
(uL)
Date Extracted: 04/29/2007
GPC Cleanup: (Y/N). Y_
(uL) GPC Factor: 2.0
pH: 8_JL
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kg) uq/kq
Q
100-52-7
Benzaldehyde
34
J
108-95-2
Phenol
240
U
111-44-4
Bis(2-chloroethyl)ether
240
U
95-57-8
2-Chlorophenol
240
U
95-48-7
2-Methylphenol
240
U
108-60-1
2,21-Oxybis(1-chloropropane)
240
U
98-86-2
Acetophenone
17
J
106-44-5
4-Methylphenol
240
- u
621-64-7
N-Nitroso-di-n-propylamine
240
u
67-72-1
Hfexachloroethane
24 0
u
98-95-3
Nitrobenzene
240
u
78-59-1
Isophorone
240
u
88-75-5
2-Nitrophenol
* ' 240
u
105-67-9
2,4-Dimethylphenol
240
u
111-91-1
Bis(2-chloroethoxy)methane
240
u
120-83-2
2,4-Dichlorophenol '
240
u
91-20-3
Naphthalene
-240
u
106-47-8
4-Chloroaniline
¦240
u
87-68-3
Hexachlorobutadiene ' , .
240
u
105-60-2
Caprolactam
24 0
u
59-50-7
.4-Chioro-3-methylphenol
240
u
91-57-6
2-Methylnaphthalene
240
U '
77-47-4
Hexachlorocyclopentadiene
240
u
88-06-2
2,4,6-Trichlorophenol
240
u
95-95-4
2,4,5-Trichlorophenol
¦ 240
u
92-52-4
1,1'-Biphenyl
240
u
91-58-7
2-Chloronaphthalene
240
u
88-74-4
2-Nitroaniline
460
u
131-11-3
Dimethylphthalate
240
u
606-20-2
2,6-Dinitrotoluene
240
U -
208-96-8
Acenaphthylene
240
u
99-09-2
3-Nitroaniline
460
u
83-32-9
Acenaphthene
240
u
*5l2>l(&l SOM01.1 (5/200iP
-------
¦IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R5
Lab Name: DataChem Laboratories, Inc.,
Lab Code: DATAC Case No.: 36345 '
Contract: EP-W-05-026
Mod. Ref No.:
SDG- No. : J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
Lab Sample ID: 7117018.007
(g/mL)
Lab File ID: NZW14C07
Level: (LOW/MED) LOW
% Moisture: 29
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
P
Injection Volume: 1. 0
(UL)
Date Extracted: 04/29/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: jKl .
Date Analyzed: 05/03/2007
Dilution Factor: l.'O
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
51-28-5
2,4-Dinitrophenol
4 60
U
100-02-7
4-Nitrophenol
460
U
132-64-9
Dibenzofuran
240
U
121-14-2
2,4-Dinitrotoluene
240
u
84-66-2
Diethylphthalate
240
¦ u
86-73-7
Fluorene
240
u
7005-72-3
4-Chlorophenyl-phenylether
240
u
100-01-6
4-Nitroaniline
460
- u
534-52-1
4,6-Dinitro-2-methylphenol
460
u
86-30-6
N-Nitrosodiphenylamine1
24 0
u
95-94-3
1, 2, 4, 5-TetraGhlor.obenzene
240
u '
101-55-3
4-Bromophenyl-phenylether
240
u
118-74-1
Hexachlorobenzene
240
u
1912-24-9
Atrazine
240
u
87-86-5
Pentachlorophenol
460
u
85-01-8
Phenanthrene
24 0
u
120-12-7
Anthracene
240
u
86-74-8
Carbazole
240
u
84-74-2
Di-n-butylphthalate
240
u
206-44-0
Fluoranthene '
24 0
u
129-00-0
Pyrene
240
¦ u
85-68-7
Butylbenzylphthalate
240
u
91-94-1
3,3'-Dichlorobenzidine
. 240
u
56-55-3
Benzo(a)anthracene
240
u
218-01-9
Chrysene
240
u
117-81-7
Bis(2-ethylhexyl)phthalate
240-3r9
117-84-0
Di-n-octylphthalate
240'
u
205-99-2
Benzo(b)fluoranthene
240
u
207-08-9
Benzo(k)fluoranthene
240
u
50-32-8
Benzo(a)pyrene
240
u
193-39-5
Indeno(1,2,3-cd)pyrene
240
u
53-70-3
Dibenzo(a,h)anthracene
240
u
191-24-2
Benzo(g,h,i)perylene
240
u
58-90-2
2,3,4,6-Tetrachlorophenol
'240
u
^Cannot be separated from Diphenylamine
S31 /.V^SOMO 1.1 (5/200^)1
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY. IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86R5
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345 Mod. Ref
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Contract: EP-W-05-026
No. :
SDG No.: J8 6R1
Lab Sample ID: 7117018007
(g/ioL)
Lab File ID: NZW14C07
Level: (LOW/MED) LOW
% Moisture: 29
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
p
Injection Volume: 1. 0
(uL) Date Extracted: 04/29/2007.
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 8.1
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane, 1,1,2,2-tetrachloro-
4 .03
360
JN
Unsaturated Hydrocarbon
4.22
200
JN
Unknown aromatic
7.19
260
JN
Polycyclic hydrocarbon
19.15
210
JN
Polycyclic hydrocarbon
24.74
' 100
JN
.
E9667962
Total Alkanes
N/A
01
02
03
04
05
06
07
08
09
10
11
12
13
¦ 14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
!EPA-designated Registry Number.
C:;;
S/3l/s1 SOM01.1- (5/20o9£
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
¦ J86X6
Lab Name: DataChem Laboratories, Inc.. .
Lab Code: DATAC Case No.: 36345':
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
Lab Sample ID: 7117018008
(g/mL)
Lab File ID: NZW15C08
Level: (LOW/MED) LOW
% Moisture: 29
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
f
Injection Volume: 1. 0
(uL) Date Extracted: 04/29/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: JMD
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO. .
COMPOUND .
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/kg
Q
100-52-7
Benzaldehyde
39
J
108-95-2
Phenol
24 0
U
111-44-4
Bis(2-ohloroethyl)ether
' - .. 240
U
95-57-8
2-Chlorophenol
240
u
95-48-7
2-Methylphenol
240
u
108-60-1
2,2'-Oxybis(1-chloropropane)
240
u
98-86-2
Acetophenone
20
. J
106-44-5
4-Methylphenol
240
" u
621-64-7
N-Nitroso-di-n-propylamine
240
u
67-72-1
Hexachloroethane
24 0
u
98-95-3
Nitrobenzene
240
u
78-59-1
Isophorone
240
u
88-75-5
2-Nitrophenol
24 0
u
105-67-9
2,4-Dimethylphenol .
240
- u
111-91-1
Bis(2-chloroethoxy)methane
240
u
120-83-2
2,4-Dichlorophenol
240
u
91-20-3
Naphthalene
240
u
106-47-8
4-Chloroaniline
240
u
87-68-3
Hexachlorobutadiene
240
u
105-60-2
Caprolactam
240
u
59-50-7
4-Chloro-3-methylphenol
240
u
91-57-6
2-Methylnaphthalene
240
u
77-47-4
Hexachlorocyclopentadiene
240
u
88-06-2
2,4,6-Trichlorophenol
240
u
95-95-4
2,4,5-Trichlorophenol
240
u
92-52-4 ¦
1,1'-Biphenyl
240
u
91-58-7
2-Chloronaphthalene
240
u
88-74-4
2-Nitroaniline
4 60
u
131-11-3
Dimethylphthalate
240
u
606-20-2
2,-6-Dinitrotoluene
240
. u
208-96-8
Acenaphthylene
240
u
99-09-2
3-Nitroaniline
460
u
83-32-9
Acenaphthene
240
u
^73//n soM°1-1 (
5/2ot$?
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T6
Lab Name: DataChem Laboratories, Inc.
Lab' Code: DATAC Case No.: 36345'-
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0
(g/mL) g__
Level: (LOW/MED) LOW
% Moisture: 2 9
Decanted: (Y/N) N
Concentrated Extract Volume: 500
Injection Volume: 1. 0
GPC Cleanup: (Y/N) Y
(uL)
(uL) GPC Factor: 2.0
pH: 8^_0
Lab Sample ID: 7117018008
Lab File ID: NZW15C08
Extraction: (Type) SONC
Date Received: 04/27/2007
Date Extralcted: 04/29/2007
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
51-28-5
2, 4-Dinitrophenol
460
U
.100-02-7
4-Nitrophenol
460
u
132-64-9
Dibenzofuran
240
u
121-14-2
2,4-Dinitrbtoluene
240
u
84-66-2
Diethylphthalate
240
•u
86-73-7
Fluorene
240
u
7005-72-3
4-Chlorophenyl-phenylether
240
u
100-01-6
4-Nitroaniline
460
¦¦ u
534-52-1
4, 6-Dinitro-2-meth.ylphenol
4.60
u
8,6-30-6
N-Nitrosodiphenylamine1
240
u
95-94-3
1,2,4,5-Tetrachlorobenzene
240
u
101-55-3
4-Bromophenyl-phenylether
240
u
118-74-1
Hexachlorobenzene
240
u
1912-24-9
Atrazine
240
u
87-86-5
Pentachlorophenol
460
u
85-01-8
Phenanthrene
, 240
u
120-12-7 .
Anthracene
240
u
86-74-8
Carbazole
24.0
u
84-74-2
Di-n-butylphthalate
240
u
206-44-0
Fluoranthene
240
u
129-00-0
Pyrene
' 240
u
85-68-7
Butylbenzylphthalate
240
u
91-94-1
3,3'-Dichlorobenzidine
240
u
56-55-3
Benzo(a)anthracene
240
u
218-01-9
Chrysene . '
240
u
117-81-7'
Bis (2-ethylhexyl)phthalate
240
u
117-84-0
Di-n-octylphthalate
240
u
205-99-2
Benzo(b)fluoranthene •
240
u
207-08-9
Benzo(k)fluoranthene ' .
240
u
50-32-8
Benzo(a)pyrene
240
u
193-39-5
Indeno(1,2,3-cd)pyrene
240
u
53-70-3
Dibenzo(a,h)anthracene
240
u
191-24-2
Benzo(g,h,i)perylene
240
u
58-90-2 -
2,3,4,6-Tetrachlorophenol
240
u
1 Cannot be separated from, Diphenylamine
A
SOM01.1 (5/200^94
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J8 6T6
Lab Name: DataChem Laboratories/ Inc.;
Lab Code: DATAC Case No,: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol': 30.0
Lab Sample ID: 7117018008
(g/mL)
Level: (LOW/MED) LOW
% Moisture: 29
Lab File ID: NZW15C08
Extraction: (Type) SONC
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 500
p
Injection Volume: 1.0
(uL)
Date Extracted: 04/29/2007
GPC Cleanup: (Y/N) Y
uL) GPC Factor: 2.0
pH: £^0
Date Analyzed: 05/03/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/kq
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
79-34-5
Ethane-, 1,1,2, 2-tetrachloro-
4.03
500
JN
Unsaturated Hydrocarbon
4 .22
200
JN
Unknown aromatic
7.20
340
JN
629-54-9
Hexadecanamide
14.17
130
JN
Unknown amide
15.06
1500
Jivl
Polycyclic hydrocarbon
19.15
260
'JN
Polycyclic hydrocarbon
24 . 74
¦ 170
JN
-
E9667962
Total Alkanes
N/A
4400
J
01
02
03
04
05
06
07
08
09
10
11
12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
?EPA-designated Registry•Number.
?r/3> l/d'l SOM01.1 (5/20$9)5
-------
ID - FORM I SV-1
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T9
Lab'Name: DataChem Laboratories, Inc.;
Lab Code: DA,TAC Case No.: 3 634 5j:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
(g/mL) mL
Level: (LOW/MED) LOW
% Moisture:
Decanted: (Y/N) N
Concentrated Extract Volume: 1000
i
Injection Volume: 1.0.
(uL)
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:.
PH:
Lab Sample ID: 7117018010
Lab File ID: YEJ04C10
Extraction: (Type) CONT
Date Received: 04/27/2007
Date Extracted: 04/30/2007
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/L
Q
100-52-7
Benzaldehyde
5.0
U
108-95-2
Phenol.
5.0
U
.111-44-4
Bis(2-chloroethyl)ether
5.0
U
95-57-5
2-Chlorophenol
5.0
u
95-48-7
2-Methylphenol
5.0
u
108-60-1
2,2'-Oxybis(1-chloropropane)
5.0
u
98-86-2
Acetophenone
5.0
U '
106-44-5
4-Methylphenol
5.0
U
621-64-7
N-Nitroso-di-n-propylamine
5.0
u
67-72-1
Hexachloroethane
5.0
u
98-95-3
Nitrobenzene
5.0
u
78-59-1
Isophorone
5.0
u
88-75-5
2-Nitrophenol '
5.0
u
105-67-9
2,4-Dimethylphenol
5.0
u
111-91-1
Bis(2-chloroethoxy)methane
5.0
u
120-83-2
2,4-Dichlorophenol
5.0
u
91-20-3
Naphthalene
5.0
u
106-47-8
4-Chloroanilirie
5.0
u
87-68-3
Hexachlorobutadiene
5.0
u
105-60-2
Caprolactam
5.0
. u
59-50-7
4-Chioro-3-methylphenol
5.0
u
91-57-6
2-Methylnaphthalene
5.0
u
77-47-4
Hexachlorocyclopentadiene
5.0
u
88-06-2
2,4,6-Trichlorophenol
5.0
u
95-95-4
'2, 4, 5-Trichlorophenol
5.0
u
92-52-4
1,1 '-Biphenyl ¦ /
¦ 5.0
u
91-58-7
2-Chloronaphthalene
5.0
u
88-74-4
2-Nitroaniline
10
u
131-11-3
Dimethylphthalate
5.0
u
606-20-2
2,6-Dinitrotoluene'
5.0
u
208-96-8.
Ac.enaphthylene
. 5.0
u
99-09-2 '
3-Nitroaniline
10
u
83-32-9
Acenaphthene
5.0
u
S~/3l/dl SQM01-1 (5/2o1d1P
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T9
Lab Name: DataChem Laboratories, Inc
Lab Code: DATAC
Case No.: 3634$
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
(g/mL) mL
Level: (LOW/MED) LOW
% Moisture:
Decanted: (Y/N) N
Contract: EP-W-05-026
Mod. Ref No.
SDG No.: J8 6R1
Concentrated Extract Volume: 1000
p
Injection Volume: 1. 0
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:
PH: ,
Lab Sample ID: 7117018010
Lab File ID: YEJ04C10
Extraction: (Type) CONT
Date Received: 04/27/2007
(uL) Date Extracted:' 04/30/2007
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/L
Q
51-28-5
2,4-Dinitrophenol
10
U
100-02-7
4-Nitrophenol
10
U
132-64-9
Dibenzofuran
5.0
U
121-14-2
2,4-Dinitrotoluene
5.0
U
84-66-2
Diethylphthalate
<3,0 9 • 7'9
cFU
86-73-7
Fluorene
5.0
u
7005-72-3
4-Chiorophenyl-phenylether
5.0
u
100-01-6
4-Nitroaniline
10
" u
534-52-1
4,6-Dinitro-2-methylphenol
10
u
86-30-6
N-Nitrosodiphenylamine1
5.0
u
95-94-3
1,2,4,5-Tetrachlorobenzene
5.0
u ¦
101-55-3
4-Bromophenyl-phenylether
5.0
u
118-74-1
Hexachlorobenzene
5.0
u
1912-24-9
Atrazine
5.0
u
87-86-5
Pentachlorophenol ;
10
u
85-01-8
•Phenanthrene
5.0
u
120-12-7
Anthracene
5.0
u
86-74-8
Carbazole
5.0
u
84-74-2
Di-n-butylphthalate
o 0 Ch-66
•
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J86T9
Lab Name: DataChem Laboratories, Inc.;
Lab Code: DATAC Case No.: 36345;; Mod. Ref
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
Contract: EP-W-05-026
No.:
SDG No.: J8 6R1
Lab Sample ID: 7117018010
(g/mL) mL
Lab File ID: YEJ04C10
Level: (LOW/MED) LOW
% Moisture:
Extraction: (Type) CONT
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 1000
f
Injection Volume: 1. 0
(uL)
Date Extracted: 04/30/2007
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:
PH:
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) ug/L
CAS NUMBER
COMPOUND NAME
RT
EST. CONC.
Q
'
E9667 962
Total Alkanes
N/A
01
02
03
04
05
0 6
07
08
09
10
-11
' 12
13
14
15
16
17
18
19
20
21
22
23
24
25
26
27
28
29
30
!EPA-designated Registry Number.
SOM01.1 ( 5/20"l)§^
-------
ID - FORM I SV-1
SEMI.VOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W1
Lab Name: DataChem Laboratories, Inc.-.
Lab Code: DATAC ' Case No.: 36345*.
Contract': EP-W-05-026
Mod. Ref No. :
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
(g/mL) mL
Level: (LOW/MED) LOW
% Moisture:
Decanted: (Y/N) N
Concentrated Extract Volume: 1000
Injection Volume: 1. 0
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:
PH:
(uL.)
Lab Sample ID: 7117018009
Lab File ID: YEJ03C09.
Extraction:, (Type) CONT
Date Received: 04/27/2007
Date Extracted: 04/30/2007
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND
¦CONCENTRATION UNITS:
(uq/L or uq/kg) ug/L
Q
100-52-7
Benzaldehyde
5.0
U
108-95-2
Phenol
5.0
U
' 111-44-4
Bis(2-chloroethyl)ether
5.0
U
95-57-8
2-Chlorophenol
5.0
u
95-48-7
2-Methylphenol
¦5.0
* u
108-60-1
2, 2'-Oxybis(1-chloropropane)
5.0
u
98-86-2
Acetophenone
5.0
u
106-44-5
4-Methylphenol
5.0
u
621-64-7
N-Nitroso-di-n-propylamine
5.0
u
67-72-1
Hexachloroethane
5.0
u
98-95-3
Nitrobenzene
5.0
u
78-59-1
Isop'horone
5.0
u
88-75-5
2-Nitrophenol
5.0
u
105-67-9
2,4-Dimethylphenol
5.0
u
111-91-1
Bis(2-chloroethoxy)methane
5.0
u
120-83-2
2,4-Dichlorophenol
5.0
u -
91-20-3
Naphthalene
5.0
u
106-47-8
4-Chloroaniline -
'5.0
U ¦
87-68-3
Hexachlorobutadiene
5.0
u
105-60-2
Caprolactam
5.0
U
59-50-7
4-Chloro-3-methylphenol
5.0
u
91-57-6
2-Methylnaphthalene
5.0
U
77-47-4
Hexachlorocyclopentadiene
5.0
U
88-06-2
2,4,6-Trichlorophenol
,5.0
u
95-95-4
2,'4, 5-Trichlorophenol
5.0
u
92-52-4
1,1'-Biphenyl
5.0
u
91-58-7
2-Chloronaphthalene
5.0
u
88-74-4
2-Nitroaniline
10
u
131-11-3
Dime'thylphthalate
5.0
u
606-20-2
2,6-Dinitrotoluene
. 5.0
u
208-96-8
Acenaphthylene
5.0
u
99-09-2
3-Nitroaniline
10
: U
83-32-9
Acenaphthene
5.0
u ¦
Thl/s? SOM01.1 (5/20t§?
-------
IE - FORM I SV-2
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W1
Lab Name: DataChem Laboratories, Inc.;,
Lab Code: DATAC Case No.: 36345>.
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J8 6R1
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
Lab Sample ID: 7117018009
(g/mL) mL
Lab File ID: YEJ03C09
Level: (LOW/MED) LOW
% Moisture:
Extraction: (Type) CONT
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 1.000
r
Injection Volume: 1. Q-
(uL)
Date Extracted: 04/30/2007
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:
PH:
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CAS NO.
COMPOUND •
CONCENTRATION UNITS:
(uq/L or ug/kg) ug/L
Q
51-28-5
2,4-Dinitrophenol
10
u -
100-02-7
4-Nitrophenol
10
u
1 132-64-9
Dibenzofuran
5.0
u
121-14-2'
2,4-Dinitrotoluene
5.0
u
84-66-2
Diethylphthalate
e-r^T1
¦ J(J
86-73-7
Fluorene
5.0
u
7005-72-3
4-Chiorophenyl-phenylether
5.0
: u
100-01-6
4-Nitroaniline
10
" u
534-52-1
4,6-Dinitro-2-methylphenol
10
u
86-30-6
N-Nitrosodiphenylamine1
5-. 0
u
95-94-3
1,2,4,5-Tetrachlorobenzene
5.0
-U ,
.101-55-3
4-Bromophenyl-phenylether
5.0
U"
118-74-1
Hexachlorobenzene
5.0
u
1912-24-9
Atrazine
5.0
u
87-86-5
Pentachlorophenol
10
¦u
85-01-8
Phenanthrene
5.0
u
120-12-7
Anthracene
5.0
u
86-74-8
Carbazole ¦
5.0
u
84-74-2
Di-n-butylphthalate
S,Q 0-rdT
(J
206-44-0
Fluoranthene
5.0
u
129-00-0
Pyrene
5.0
¦ u
85-68-7
Butylbenzylphthalate
So
¦3 U
91-94-1
3,3'-Dichlorobenzidine
5.0
u
56-55-3
Benzo(a)anthracene \
5.0
u
218-01-9
Chrysene i
5.0
u
117-81-7
Bis(2^ethylhexyl)phthalate
S.0 <*-3$
'd- (J
117-84-0
Di-n-octylphthalate
5.0
u
205-99-2
Benzo(b)fluoranthene
5.0
u
207-08-9
Benzo(k)fluoranthene
5.0
u
50-32-8
Benzo(a)pyrene
5.0
' u
193-39-5
Indeno (1, 2,.3-cd) pyrene /
5.0
u
5,3-70-3
Dibenzo(a,h)anthracene ¦ ¦
5.0
u
191-24-2
Benzo(g,h,i)perylene
5.0
u
58-90-2
2,3,4,6-Tetrachlorophenol
5.0
u
1 Cannot be separated from Diphenylamine \
¦ ¦ _ -¦
fyJSl/fiJ S0M°1.1 (5/20MP
-------
IK - FORM I SV-TIC
SEMIVOLATILE ORGANICS ANALYSIS DATA SHEET
TENTATIVELY IDENTIFIED COMPOUNDS
EPA SAMPLE NO.
J8 6W1
Lab Name: DataChem Laboratories, Inc;.
Lab Code: DATAC Case No.: 36345 v Mod. Ref
Matrix: (SOIL/SED/WATER) WATER
Sample wt/vol: 1000
Contract: EP-W-05-026
No.:
SDG No.: J8 6R1
Lab Sample ID: 7117018009
(g/mL) mL
Lab File ID: YEJ03C09
Level: (LOW/MED) LOW
% Moisture:
Extraction: (Type) CONT
Decanted: (Y/N) N
Date Received: 04/27/2007
Concentrated Extract Volume: 1000
?
¦ Injection Volume: 1. 0
(uL)
Date Extracted: 04/30/2007
GPC Cleanup: (Y/N) N_
(uL) GPC Factor:
PH:
Date Analyzed: 05/01/2007
Dilution Factor: 1.0
CONCENTRATION UNITS:(ug/L or ug/kg) uq/L
CAS NUMBER
COMPOUND NAME
RT :
EST. CONC.
Q.
01
Column bleed product
6.34
6.1
02
Column bleed product
9.24
2.3
.jyfL.
03
04
05
06
07
08
09
10
11
12
'
13
1.4
15
16
17
18
19
20
21
22
23
24
25
2.6
27
28
'
29
30
E9667962
Total Alkanes
' N/A
2EPA-designated Registry Number.
iIcq- SOM01.1 (5/2ot)4)1
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026 ;
Lab Code: DATAC Case No. : 36345;: Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ' ¦ Lab Sample ID: 7120009001
Sample wt/vol: 3 0.0 (g/mL) q Lab File ID: 21070514A023,21070514B023
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/3 0/2007
Extraction: (Type) SONC . Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007 ^
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2.0 Dilution Factor: 1. 0 .
GPC Cleanup: (Y/N) Y pH: 7 .4 Sulfur Cleanup: (Y/N) N ,
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or uq/kq) uq/kq
Q
319-84-6
alpha-BHC
2.1
u
319-85-7
beta-BHC
2.1
u
319-86-8
delta-BHC
2.1
u
58-89-9
gamma-BHC (Lindane)
<2, |
ifp u
76-44-8
Heptachlor
2.1
u
309-00-2
Aldrin
¦ 2.1
u
1024-57-3
Heptachlor epoxide
2.1
u
959-98-8
Endosulfan I
2.1
u
60-57-1
Dieldrin
4.1
u
72-55-9
4,4'-DDE .
¦4, 1 8'.04-2
dFPU
72-20-8
Endrin
4.1
u
33213-65-9
Endosulfan II
4.1
u
72-54-8
4,4'-DDD
4.1
u
1031-07-8
Endosulfan sulfate
4.1
u
50-29-3
4,4'-DDT
4.1
u
72-43-5
Methoxychlor
.0.46
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde
,4.1
U '
5103-71-9
alpha-Chlordane
2.1
U
5103-74-2
gamma-Ch1ordane
2.1
u
8001-35-2
Toxaphene
210
. u
SOM01.1 (5/2 ®®7
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S5
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345: Mod. Ref No. : _______ SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ¦ Lab Sample ID: 7120009002
Sample wt/vol: 30.0 (g/mL) g Lab File ID: 21070514A024, 21070514B024
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2. 0 Dilution Factor: 1. 0 ,
GPC Cleanup: (Y/N) Y pH: 6^5 Sulfur Cleanup: (Y/N) N
CAS NO. ,
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.1
u
319-85-7
beta-BHC
2.1
u
319-86-8
delta-BHC
2.1
u
58-89-9
gamma-BHC (Lindane)
2A 0.0&4
¦JPCJ
76-44-8
Heptachlor
2.1
u
309-00-2
Aldrin
2.1
u
1024-57-3
Heptachlor epoxide
2.1
u
959-98-8
Endosulfan I
2.1
u
60-57-1
Dieldrin
0 .¦¦05-4
39 U
72-55-9
4,4'-DDE x
39 cj
72-20-8 ¦
Endrin
4.1
U
33213-65-9
Endosulfan II
4.1
u
72-54-8
4,4'-DDD
«4.| &-.-008
Ji'iJ
1031-07-8
Endosulfan sulfate
4.1
u
50-29-3
4,4'-DDT
¦s4i ( 0". 2 0
tfPU
72-43-5
Methoxychlor
0.27
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde
,4.1
u
5103-71-9
alpha-Chlordane
2.1
u
5103-74-2
gamma-Chlordane
2s | 0-r0^3
39U
8001-35-2
Toxaphene
210
u
SOM01.1 (5/2®®0
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories, Inc.,
Lab Code: DAT AG Case No.. : 3 6345:
Matrix: (SOIL/SED/WATER) SOIL ' i
Sample wt/vol: 30.0 (g/mL) q
% Moisture: 38 Decanted: (Y/N) N
_ Contract: EP-W-05-026
Mod. Ref No.: -
SDG No.: J86R0
Lab Sample ID: 7120009003
Lab File ID: 21070514A025,21070514B025
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2 007
Concentrated Extract Volume: 10000
f :
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 6^8
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q.
319-84-6
alpha-BHC
2.7
U
319-85-7
beta-BHC
2.7
u
319-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane)
2rf- 6-r-&W
jpU
76-44-8
Heptachlor
jf>(J
309-00-2
Aldrin ¦
2.7
u
1024-57-3
Heptachlor epoxide
2 .7
u
959-98-8
Endosulfan I
2.7
. u
60-57-1
Dieldrin
5.3
u
72-55-9
4,4'-DDE
5,3
d
72-20-8
Endrin
5.3
u
33213-65-9
Endosulfan II
S3
tJPU
72-54-8
4,4'-DDD
5.3
u
1031-07-8
Endosulfan sulfate
5.3
u
50-29-3
4,4'-DDT
S.3
dFPU
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5.3
u
7421-93-4
Endrin aldehyde
5.3
u
5103-71-9
alpha-Chlordane
2.7
u
5103-74-2
gamma-Chlordane
i?P u
8001-35-2
Toxaphene
270
u
SOM01.1 (5/2&S3
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026 .
Lab Code: DATAC Case No.: 36345; Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' Lab Sample ID: 7120009004
Sample wt/vol: 30.0 (g/mL) q__ Lab File ID: 21070514A026,21070514B026
% Moisture: 30 Decanted: (Y/N) N_ Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
P
Injection Volume: 2.0 (up GPC Factor: 2.0 Dilution Factor: 1.0 -
GPC Cleanup: (Y/N) Y pH: 6 . 9 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.4
U
319-85-7
beta-BHC ¦ .
2.4
u
319-86-8
delta-BHC
2.4
u
58-89-9
gamma-BHC (Lindane)
2.4
U
76-44-8
Heptachlor
2.4
u
309-00-2
Aldrin
2.4
u
1024-57-3
Heptachlor epoxide
2.4
u
959-98-8
Endosulfan I
2.4
u
60-57-1
Dieldrin
4.7
u
72-55-9
4,4'-DDE
4.7
u.
72-20-8
Endrin
4.7
u
33213-65-9
Endosulfan II
'4.7
u
72-54-8
4,4'-DDD
4.7
u
1031-07-8
Endosulfan sulfate
4.7
u
50-29-3
4,4'-DDT
4.7
u
72-43-5
Methoxychlor
24
u
53494-70-5
Endrin ketone
4.7
u
7421-93-4
Endrin aldehyde
,4.7
u
5103-71-9
alpha-Chlordane
2.4
u
5103-74-2
gamma-Chlordane
2.4 e-r&5-
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S8
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3 6345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30 . 0 (g/mL) q
% Moisture: 29 Decanted: (Y/N) N_
Lab Sample ID: 7120009005
Lab File ID: 21070514A027,21070514B027
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
f
Injection Volume: 2.0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
uL) GPC Factor: 2 . 0
pH: 5.3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) ug/kq
Q
319-84-6
alpha-BHC
2.4
u
319-85-7
beta-BHC
2,4
¦jp u
319-86-8
delta-BHC
2.4
u
58-89-9
gamma-BHC (Lindane)
2.4
U •
76-44-8
Heptachlor
2.4
u
309-00-2
Aldrin
2.4
u
1024-57-3
Heptachlor epoxide
0.12
J
959-98-8
Endosulfan I
2.4
u
60-57-1
Dieldrin
4.7
u
72-55-9
4,4'-DDE
.1.1
J
72-20-8
Endrin
4.7
u
33213-65-9
Endosulfan II
l-Q-r&W
•flil
72-54-8
4,41-DDD
4^=f 0-r«
JP u
1031-07-8
Endosulfan sulfate
4.7
u
50-29-3
4,4'-DDT
0-.30
t£p d
72-43-5
Methoxychlor
0.63
j
53494-70-5
Endrin ketone
4.7.
¦ u
7421-93-4
Endrin aldehyde
,4.7
u
5103-71-9
alpha-Chlordane
2.4
u
5103-74-2
gamma-Chlordane
2.4 o^e
i»U
8001-35-2
Toxaphene
240
u
SOM01.1 (5/2 6®9
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ; Lab Sample ID: 7120009006
Sample wt/vol: 30.0 (g/mL) g Lab File ID: 21070514A028,21070514B028
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/30/2007 ¦
Extraction: (Type) SONC Date Extracted: 05/01/2007 ___
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
f
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 6 . 5 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:¦
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.1
U
319-85-7
beta-BHC
2.1
¦ U
319-86-8
delta-BHC
2.1
u
58-89-9
gamma-BHC (Lindane)
2.1
u '
76-44-8
Heptachlor
2.1
u
309-00-2
Aldrin
¦2.1
u
1024-57-3
Heptachlor epoxide
2.1
u
959-98-8
Endosulfan I
2.1
u
60-57-1
Dieldrin
4.1
u
72-55-9
4,4'-DDE
4.1
u
72-20-8
Endrin
4.1
u
33213-65-9
Endosulfan II
4.1
u
72-54-8
4,4'-DDD
4.1
u
1031-07-8
Endosulfan, sulfate
4.1
u
50-29-3
4,4"-DDT
4.1
u
72-43-5
Methoxychlor
0.44
J
53494-70-5
Endrin ketone
4.1
u
7421-93-4
Endrin aldehyde, -
,4.1
u ¦
5103-71-9
alpha-Chlordane
2.1
u
5103-74-2
gamma-Chlordane
0.066
jf
8001-35-2
Toxaphene
210
u
6//o/a?
SOM01.1 (5/2 5(&2
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T0
Lab Name: DataChem Laboratories. Inc.,
Lab Code: DATAC Case No. : 3 6345::
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 40
Lab Sample ID: 7120009007
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A029,21070514B029
Date Received: 04/30/2007
Extraction: (Type) SQNC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
T
Injection Volume: 2 . 0
(uL)
Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 5.9
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) IL
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.8
U
319-85-7
beta-BHC
U
319-86-8
delta-BHC
2.8
U
58-89-9
gamma-BHC (Lindane)
2.8
u
76-44-8
Heptachlor
2.8
u
309-00-2
Aldrin
2.8
u
1024-57-3
Heptachlor epoxide
2.8
u
959-98-8
Endosulfan I
2.8
u
60-57-1
Dieldrin
57S&tM
U
72-55-9
4,4'-DDE
1.2
J/
72-20-8
Endrin
5.5
u
33213-65-9
Endosulfan II
0.42
J?'
72-54-8
4,4'-DDD
5^" 9.22
1031-07-8
Endosulfan sulfate .
0.34
J/
50-29-3
4,4'-DDT
S,S
-34PU
72-43-5
Methoxychlor
28
U
53494-70-5
Endrin ketone
5.5
U
7421-93-4
Endrin aldehyde
5.5
U
5103-71-9
alpha-Chlordane
2.8
U ¦
5103-74-2
gamma-Chlordane
2.8 6^4
' -
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 3 6345;;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 33
Lab Sample ID: 7120009010
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A032,21070514B032
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 .0
PH: 7.0
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ucr/kcr) ua/ka
Q
319-84-6
alpha-BHC
2.5
u
319-85-7
beta-BHC
2.5
u
319-86-8
delta-BHC
2.5
u
58-89-9
gamma-BHC (Lindane)
2.5
u
76-44-8
Heptachlor
2.5
u
309-00-2
Ald'rin
2.5
u
1024-57-3
Heptachlpr epoxide
2.5
u
959-98-8
Endosulfan I
2.5
u
60-57-1
Dieldrin
0.21
J/
72-55-9
4,4'-DDE
cjp U
72-20-8
Endrin
4.9
u
33213-65-9
Endosulfan II
4<\ Q-rQZZ
a^U
72-54-8
4,4'-DDD
Q-^
1031-07-8
Endosulfan sulfate
4.9
. u
50-29-3
4,4'-DDT
'9-r44
•tfp u
72-43-5
Methoxychlor
1.6
J?
53494-70-5
Endrin ketone
4.9
u
7421-93-4
Endrin aldehyde
,4.9
u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2¦
gamma-Chlordane
-32 (J
8001-35-2
Toxaphene '
250
U
SOM01.1 (5/2(S)t8
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T2
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345:
Contract: EP-W-05-026
Mod. Ref No. : .
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 36
Lab Sample ID: 7120009011
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A033,21070514B033
I?ate Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
f
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7 .1 .
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO,
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.6
U
319-85-7
beta-BHC
2.6
U
319-86-8
delta-BKC
2.6
U
58-89-9
gamma-BHC (Lindane)
2.6
U
76-44-8
Heptachlor
2.6
U
309-00-2
Aldrin
2.6
U
1024-57-3
Heptachlor epoxide
2.6
U
959-98-8
Endosulfan I
2.6
U
60-57-1
Dieldrin
0.18
J/
72-55-9
4,4'-DDE
S.I &T±i
ifPU
72-20-8
Endrin
5.1
u
33213-65-9
Endosulfan II
0.14
J
72-54-8
4,4'-DDD
5.1
u
1031-07-8
Endosulfan sulfate
5.1
u
50-29-3
4,4'-DDT
vS^I
jp u
72-43-5
Methoxychlor .
0.77
J/
53494-70-5
Endrin ketone
5.1
.. u
7421-93-4
Endrin aldehyde
5.1
u
5103-71-9
alpha-Chlordane
2.6
u
5103-74-2
gamma-Chlordane
2^0-riQ-
8001-35-2
Toxaphene
260
u
& A z/d -i
SOM01.1 (5/2 5©1
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories., Inc.
Lab Code: DATAC Case No. : 36345
Contract: EP-W-05-026
Mod. Ref No. :
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' -
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 37 Decanted: (Y/N) N_
Lab Sample ID: 7120009012
Lab File ID: 21070514A034,21070514B034
Date. Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
' f1'
Injection Volume: 2.0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.8
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kcr) ua/kg
Q
319-84-6
alpha-BHC
2.7
U
319-85-7
beta-BHC
2.7
U
319-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane).
2V7- 0.057
Wli
76-44-8
Heptachlor
2.7
u
309-00-2
Aldrin
2.7
u
1024-57-3
Heptachlor epoxide
2.7
u
959-98-8
Endosulfan I
2.7
u
60-57-1
Dieldrin
5.2
u
72-55-9
4,4'-DDE
5.2
u
72-20-8
Endrin
5.2
u
33213-65-9
Endosulfan II
5.2
u
72-54-8
4,4'-DDD
5.2
u
1031-07-8
Endosulfan sulfate
5.2
u
50-29-3
4,4'-DDT
5.2
u
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5.2
u
7421-93-4
Endrin aldehyde
5.2
u
51.03-71-9
alpha-Chlordane
2.7
u
5103-74-2
gamma-Chlordane
2, T 0rir9-
iff-(J
8001-35-2
Toxaphene
270
u
SOM01.1 (5/2(864
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inc., Contract: EP-W-05-026 .
Lab Code: DATAC Case No. : 3 6345 Mod. Ref No. :* SDG No. : J86R0 L
Matrix: (SOIL/SED/WATER) SOIL ; Lab Sample ID: 7120009013
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 21070514A035,21070514B035
% Moisture: 32 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC ^ . Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL)' Date Analyzed: 05/15/2007
?
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 6 . 8 Sulfur Cleanup: (Y/N) N ¦
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.5
u
319-85-7
beta-BHC
2.5
u
319-86-8
delta-BHC
2.5
u
58-89-9
gairima-BHC (Lindane)
2.5
u
76-44-8
Heptachlor
2.5
u
309-00-2
Aldrin
2.5
u
1024-57-3
Heptachlor epoxide
' 2.5
¦ u
959-98-8
Endosulfan I .
2.5
u
60-57-1
Dieldrin
4.9
u
72-55-9
4,4'-DDE
-4,^ e-r^8
J£)(j
72-20-8
Endrin
4.9
U
33213-65-9
Endosulfan II
4.9
u .
72-54-8
4,4'-DDD
•ijfU
1031-07-8
Endosulfan sulfate
4.9
u
50-29-3
4,4'-DDT
4.9
u
72-43-5
Methoxychlor
0.61
j i
53494-70-5
Endrin ketone
4.9
u
7421-93-4
Endrin aldehyde
,4.9
u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2
gamma-Chlordane
2
8001-35-2
Toxaphene
250
u
SOM01.1 (5/2
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345::
Contract: EP-W-05-02'6
Mod. Ref No.:
SDG NO.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' :
Sample wt/vol: 30 . 0 (g/mL) g
% Moisture: 23 - Decanted: (Y/N) N_
Lab Sample ID: 7120009014
Lab File ID: 21070514A03 6,21070514B03 6
Date Received: 04/30/2007
Extraction: (Type)' SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
f
Injection Volume: 2 . 0
(uL)
Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
PH: 7.5
' Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.2
u
319-85-7
beta-BHC
2.2
u
319-86-8
delta-BHC
2.2
u
58-89-9
gamma^-BHC (Lindane)
2.2
u
76-44-8
Heptachlor
2.2
u .
309-00-2
Aldrin
2.2
u
1024-57-3
Heptachlor epoxide
2.2
u
959-98-8
Endosulfan I
2.2
u
60-57-1
Dieldrin
0.054
J/
72-55-9
4,4'-DDE
-4A
ifP-U
72-20-8
Endrin
4.3
u
33213-65-9
Endosulfan II
4.3
u
72-54-8
4,4'-DDD '
0.14
J
1031-07-8
Endosulfan sulfate
4.3
u
50-29-3
4,4'-DDT
tfPU
72-43-5
Methoxychlar
2Z 9-^5
53494-70-5
Endrin ketone
4.3
•u.
7421-93-4
Endrin aldehyde
,4.3
u
5103-71-9
alpha-Chlordane
2.2
u
5103-74-2
gamma-Chlordane
0.062
jf
8001-35-2
Toxaphene
220
u
SOM01.1 (5/2®6Q
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3 6345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 40
Lab Sample ID: 7120009015
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 21070514A037,21070514B037
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2.0
(uL) Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7Jk
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.8
u
319-85-7
beta-BHC
2.8
u
319-86-8
delta-BHC
2.8
u
58-89-9 :
gamma-BHC (Lindane)
ZgerWf
: &pU
76-44-8
Heptachlor
2.8
u
309-00-2
Aldrin
2.8
u
1024-57-3
Heptachlor epoxide
2,3
- jpU
959-98-8
Endosulfan I
2,% ***
¦tJP O
60-57-1
Dieldrin
5.5
u
72-55-9
4,4'-DDE
1.3
Jjf
72-20-8
Endrin
0.30
J
33213-65-9
Endosulfan II
S,S" Q-T&9-
jp U
72-54-8
4,4'-DDD
5.5
. u
1031-07-8
Endosulfan sulfate
5.5
u
50-29-3
4,4'-DDT
2.8
J
72-43-5
Methoxychlor
28
u
53494-7,0-5
Endrin ketone
.5.5
u
7421-93-4
Endrin aldehyde
.5.5
u
5103-71-9
alpha-Chlordane
2.8
u
5103-74-2
gamma-Chlordane -
2.8
u.
8001-35-2
Toxaphene
280
u
SOM01.1 (5/2®6S
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T8
Lab Name; DataChem.Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345 Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ' Lab Sample ID: 7120009016 .
Sample wt/vol: 30.0 . (g/mL) g Lab File ID: 21070514A038, 21070514B038
% Moisture: 3J Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
f
Injection Volume: 2.0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 6 .1 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kq) uq/kq
Q
319-84-6
alpha-BHC
2.8
u
319-85-7
beta-BHC
0.37
J
319-86-8
delta-BHC
2.8
u
58-89-9
gamma-BHC (Lindane)
2.8
u
76-44-8
Heptachlor
2.8
u
309-00-2
Aldrin
2.8
u
1024-57-3
Heptachlor epoxide '
2.8
u
959-98-8
Endosulfan I
2.8
u
60-57-1
Dieldrin
0.39
J
72-55-9
4,4'-DDE
1.1
• J
72-20-8
Endrin
5.4
u
33213-65-9
Endosulfan II
,5,4 0 -0 61
jp u
72-54-8
4,4'-DDD
,5,4- 0-r^5-
•<3HP (J
1031-07-8
Endosulfan sulfate
5.4
U
50-29-3
4,4'-DDT
5,4 0^9
JP u
72-43-5
Methoxychlor
9.% ^
53494-70-5
Endrin ketone
5.4
u
7421-93-4
Endrin aldehyde
,5.4
U
5103-71-9
alpha-Chlordane
2.8
u
5103-74-2
gamma-Chlordane
2.S-
.W'U
8001-35-2
Toxaphene
280
u
e, //Jl/c?
SOM01.1 (5/2S6©
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W4
Lab Name: DataChem Laboratories, Inc.; Contract: EP-W-05-026
Lab Code: DATAC Case No. : 3 6345^ Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER)* SOIL ' ' • Lab Sample ID: 7120009017
Sample wt/vol: 30.0 (q/mL) q Lab File ID: 21070514A039,21070514B039
% Moisture: 32 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: ^.0000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 7.8 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
319-84-6
alpha-BHC
2.5
u
319-85-7
beta-BHC
2.5
u
319-36-8
delta-BHC
2.5
u
58-89-9
gamma-BHC (Lindane)
2.5
u
00
1
1
vo
Heptachlor
2.5
u
309-00-2
Aldrin
2.5
u
1024-57-3
Heptachlor epoxide
2.5
u
959-98-8
Endosulfan I
2.5
u
60-57-1
Dieldrin
4.8
u
72-55-9
4,4'-DDE
4.8
u
72-20-8
Endrin
4.8
u
33213-65-9
Endosulfan II
4.8
u
72-54-8
4,4'-DDD
4.8
u
1031-07-8
Endosulfan sulfate
4.8
u
50-29-3
4,4'-DDT
' 4.8
u
72-43-5
Methoxychlor
0.44
J/
53494-70-5
Endrin ketone
4.8
u
7421-93-4
Endrin aldehyde
4.8
u
5103-71-9
alpha-Chlordane
2.5
u
5103-74-2
gamma-Chlordane
2(5"
¦cFP-U
8001-35-2
Toxaphene
250
u
somoi.i (5/2<£bG9
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
tr-
EPA SAMPLENO.
J86W5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345:
Contract: - EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ;
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 36 Decanted: (Y/N) N_
Lab Sample ID: 7120009018
Lab File ID: 21070514A040,21070514B040
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated,Extract Volume: 10000
Injection Volume: 2 . 0
(uL)
Date Analyzed: 05/15/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
PH: 7.3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
[
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kg) ug/kg
Q
319-84-6
alpha-BHC-
2.7
u
319-85-7
beta-BHC
2.7
u
319-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane)
2.7
u
76-44-8
Heptachlor .
2.7
u
309-00-2
Aldrin
(?p u
1024-57-3
Heptachlor epoxide
2.7
u
959-98-8
Endosulfan I
2.7
u
60-57-1
Dieldrin
5.2
u
72-55-9'
4,4'-DDE
5.2
u
72-20-8
Endrin
. 5.2
u
33213-65-9
Endosulfan II ¦
5.2
u
72-54-8
4,4'-DDD
5.2
u
1031-07-8
Endosulfan sulfate
5.2
u.
50-29-3
4,4'-DDT
5.2
u
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5.2
u
7421-93-4
Endrin aldehyde
,5.2
u
5103-71-9
alpha-Chlordane
2.7
u
5103-74-2
gamma-Chlordane
2.7
u
8001-35-2
Toxaphene
,270
u
SOM01.1 (5/2 SobZ
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
Po&r
EPA SAMPLE NO.
J86W5RX
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345;
Contract: EP-W-05-026
Mod. Ref No. :
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' -
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 36 Decanted: (Y/N) N
Lab Sample ID: 7120009018RX
Lab File ID: 21070517A020,21070517B020
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/14/2007
Concentrated Extract Volume: 10000
¦ • f'
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/18/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2. 0
pH: 7.3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
319-84-6
alpha-BHC
2.7
U
319-85-7
beta-BHC
2.7
u
313-86-8
delta-BHC
2.7
u
58-89-9
gamma-BHC (Lindane)
. 2.7
u
76-44-8
Heptachlor
2.7
u
309-00-2
Aldrin
2.7
u
1024-57-3
Heptachlor epoxide
.2.7
u
959-98-8
Endosulfan I
2.7
u
60-57-1
Dieldrin
5.2
u
72-55-9
4,4'-DDE
5.2
u
72-20-8
Endrin
5.2
u
33213-65-9
Endosulfan II
5.2
u.
72-54-8
4,4'-DDD
5 .2
u
1031-07-8
Endosulfan sulfate
5.2
u
50-29-3
4,4'-DDT
5.2
u
72-43-5
Methoxychlor
27
u
53494-70-5
Endrin ketone
5.2
u
7421-93-4
Endrin aldehyde
.5-2
u
5103-71-9
alpha-Chlordane
2.7
u
5103-74-2
gamma-Chlordane
0.066
J
8001-35-2
Toxaphene
270
u
SOM01.1 (5/2(8)15
-------
1G - FORM I PEST
PESTICIDE ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W6
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345;: Mod. Ref No.: SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' - Lab Sample ID: 7120009019
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 21070514A041,21070514B041
% Moisture: 36 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/15/2007
Injection Volume: 2 . 0 (uL) GPC Factor: 2.0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 7.3 Sulfur Cleanup: (Y/N) N
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kq) ug/kg
Q
319-84-6
alpha-BHC
2.6
U
319-85-7
beta-BHC
2.6
u
319-86-8
delta-BHC
2.6
u
58-89-9
gamma-BHC (Lindane)
2 .t> -©^-0^
76-44-8
Heptachlor
2.6
u
309-00-2
Aldrin
2.6
u
1024-57-3
Heptachlor epoxide
2.6
u
959-98-8
Endosulfan I
2.6
¦u
60-57-1
Dieldrin
5.1
u
72-55-9
4,4'-DDE
5.1
u
72-20-8
Endrin
• 5.1
.u
33213-65-9
Endosulfan II
5.1
u
72-54-8
4,4'-DDD
5.1
u
1031-07-8
Endosulfan sulfate
5.1
u
50-29-3
4,4'-DDT
5.1
u
72-43-5
Methoxychlor
0.3.7
J/
53494-70-5
Endrin ketone
5 .1
u
7421-93-4
Endrin aldehyde
,5.1
u
5103-71-9
alpha-Chlordane
2.6
u
5103-74-2
gamma-Chlordane
2.6
u
8001-35-2 .
Toxaphene
260
u
SOM01.1 ( 5/2(35)18
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86R0
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
(g/mL) g_
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0 .
% Moisture: 19 Decanted
Extraction: (Type) SONC
Lab Sample ID: 7120009001
(Y/N) N_
Lab File ID: 20070515A038,20070515B038
Date Received: 04/30/2007
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
. f
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/16/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2 . 0
pH: 7_J .
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
41
U
11104-28-2
Aroclor-1221
41
• u
11141-16-5
Aroclor-1232
41
u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-1262'
41
u
11100-14-4
Aroclor-1268
41
u
SOM01.1 (5/2(82$
-------
1H - FORM I ARO
AROCLOR QRGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S5
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No. : 36345;: Mod. Ref No. : SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL ' ' Lab Sample ID: 7120009002
Sample wt/vol: 30.0 (g/mL) q Lab File ID: 20070515A039,20070515B039
% Moisture: 19 Decanted: (Y/N) N Date Received: 04/30/2007 ^
Extraction: (Type) SONC Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/16/2007
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 6_J> Sulfur Cleanup: (Y/N) N
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
41
u
11104-28-2
Aroclor-1221
41
u •
11141-16-5
Aroclor-1232
41
. u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-12.62
41
u
11100-14-4
Aroclor-1268
41
u
6//z/o-7
SOM01.1 (5/2(g
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S6
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3 6345;;
Matrix: (SOIL/SED/WATER) SOIL ' - .
Sample wt/vol: 30.0 ,(g/mL) q
% Moisture: 38 Decanted: (Y/N) N_
__ Contract: EP-W-05-026
Mod. Ref No.:
SDG No. : J86R0
Extraction: (Type) SONC
Concentrated Extract Volume: 10000
f
Injection Volume: 2.0 (uL) GPC Factor: 2 .0
GPC Cleanup: (Y/N) Y_ pH: 6.8
Acid Cleanup: (Y/N) Y
Lab Sample ID: 7120009003
Lab File ID: 20070515A040.20070515B040
Date Received: 04/30/2007 ; ' -
Date Extracted: 05/01/2007
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
53
U
11104-28-2
Aroclor-1221
53
u
11141-16-5
Aroclor-1232
53
u
53469-21-9
Aroclor-1242
53
u
12672-29-6
Aroclor-1248
53
u
11097-69-1
Aroclor-1-254
53
u
11096-82-5
Aroclor-1260
53
u
37324-23-5
Aroclor-1262
53
u
11100-14-4
Aroclor-1268
53
u
£> /(z/o'-f-
SOM01.1 (5/2
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S7
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345:
. Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' -
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 30 Decanted: (Y/N) N_
Lab Sample ID: 7120009004
Lab File ID: 20070515A045,20070515B045
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
f
Injection Volume: 2 . 0 (uL) GPC Factor : 2 . 0
GPC Cleanup: (Y/N) Y pH: 6^9
Acid Cleanup: (Y/N) Y
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
47
u
11104-28-2
Aroclor-1221
47
u
11141-16-5
Aroclor-1232
47
u
53469-21-9
Aroclor-1242
47
u ,
12672-29-6
Aroclor-1248
.47
u
11097-69-1
Aroclor-1254
47
u
11096-82-5
Aroclor-1260
47
u
37324-23-5
Aroclor-1262
47
u
11100-14-4
Aroclor-1268
47
u
SOM01.1 (5/ 28®3
-------
1H - FORM I ARO
AROGLOR ORGANICS ANALYSIS DATA SHEET
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026 ,
Lab Code: DATAC. Case No. : 36345 Mod. Ref No. : SDG No. : J86R0 ¦
Matrix: (SOIL/SED/WATER) SOIL ' . Lab Sample ID: 7120009005
Sample wt/vol: 30.0 (g/mL) g_ Lab'File ID: 20070515A046, 20070515B046
% Moisture: 29 Decanted: (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC Date Extracted: 05/01/200.7
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/16/2007 .
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0 Dilution Factor: 1. 0
GPC Cleanup: (Y/N) Y pH: 5 .3 Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y^
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ug/kq) ug/kq
Q
12674-11-2
Aroclor-1016
47
U
11104-28-2
Aroclor-1221
47
u
11141-16-5
Aroclor-1232
47
u
53469-21-9
Aroclor-1242
47
u
12672-29-6
Aroclor-1248
47
u
11097-69-1
Aroclor-1254
' 47
u
11096-82-5
Aroclor-1260
.47
u
37324-23-5
Aroclor-1262
47
u
11100-14-4
Aroclor-1268
47
u
SOM01.1 (5/2®C$8
EPA SAMPLE NO.
J86S8
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86S9
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 19
Lab Sample ID: 7120009006
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 2 0070515A047,2 0070515B047
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
(uL)
Concentrated Extract Volume: 10000
- ; ' f
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH: 6^5
Acid. Cleanup: (Y/N) Y
Date Analyzed: 05/16/2007
Dilution Factor: 1. 0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kq) ug/kg
Q
12 674-11-2
Aroclor-1016
41
U
11104-28-2
Aroclor-1221
41
u
11141-16-5
Aroclor-1232
41
u
53469-21-9
Aroclor-1242
41
u
12672-29-6
Aroclor-1248
41
u
11097-69-1
Aroclor-1254
41
u '
11096-82-5
Aroclor-1260
41
u
37324-23-5
Aroclor-1262
41
u
11100-14-4
Aroclor-1268
41
. u
£>/l2-/o3
SOM01.1 (5/^J^)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T0
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026
Lab Code: DATAC Case No.: 36345^ Mod. Ref No.: " SDG No.: J86R0
Matrix: (SOIL/SED./WATER) SOIL ' ' Lab Sample ID: 7120009007
Sample wt/vol: 30 .0 (g/mL) g Lab File ID: 20070515A048, 20070515B048
% Moisture: 40 Decanted:. (Y/N) N Date Received: 04/30/2007
Extraction: (Type) SONC ' Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/16/2007 '
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0
GPC Cleanup: (Y/N) Y pH: 5_J3 Sulfur Cleanup: (Y/N) N '
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
55
U
11104-28-2
Aroclor-1221
55
U
11141-16-5
Aroclor-1232
55
u
53469-21-9
Aroclor-1242
55
u
12672-29-6
Aroclor-1248
55
u
11097-69-1
Aroclor-1254
55
u
11096-82-5
¦ Aroclor-1260
55
u
37324-23-5
Aroclor-1262
55
u
11100-14-4
Aroclor-1268
55
u
SOM01.1 (5/®4>4)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T1
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 36345.
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' '¦
Sample wt/vol: 30.0 (g/mL) q
% Moisture: 33 • Decanted: (Y/N) N_
Lab Sample ID: 7120009010
Lab File ID: 20070515A051,20070515B051
Date Received: 04/30/2007 __
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extra!ct Volume: 10000
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH: 7.0
Acid Cleanup: (Y/N) Y
(uL) Date Analyzed: 05/16/2007
Dilution Factor: 1. 0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
49
U
11104-28-2
Aroclor-1221
49
u
11141-16-5
Aroclor-1232
49
u .
53469-21-9
Aroclor-1242
49
u
12672-29-6
Aroclor-1248
49
u
11097-69-1
Aroclor-1254
49.
u
11096-82-5
Aroclor-1260
49
u
37324-23-5
Aroclor-1262
49
u
11100-14-4
Aroclor-1268
49
u
SOM01.1 (5/$fk|^)
-------
1H - FORM I ARO
AROGLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO,
J86T2
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3 6345.
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' '¦
Sample wt/vol: 30.0 (g/mL) q
% Moisture: 36 Decanted: (Y/N) N_
Lab Sample ID: 7120009011
Lab File ID: 20070515A052,20070515B052
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/20Q7
(uL)
Concentrated Extract Volume: 10000
f
Injection Volume: 2.0 (uL) GPC Factor: 2 .0
GPC Cleanup: (Y/N) Y pH: 1_A¦.
Acid Cleanup: (Y/N) Y
Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(uq/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
51
u
11104-28-2
Aroclor-1221
51
u
11141-16-5 .
Aroclor-1232
51
u
53469-21-9
Aroclor-1242
51
u
12672-29-6
Aroclor-1248
51
u
11097-69-1.
Aroclor-1254
51
u
11096-82-5
Aroclor-1260
51
u
37324-23-5
Aroclor-1262
51
u
11100-14-4
Aroclor-1268
51
u
SOM01.1
(5/®80)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T3
Lab Name: DataChem Laboratories, Inc. Contract: EP-W-05-026 '
Lab Code: DATAC Case No. : 36345: Mod. Ref No. : __ SDG No. : J86R0 -
Matrix: (SOIL/SED/WATER) SOIL ' ' Lab Sample ID: 7120009012
Sample wt/vol: 30.0 (g/mL) g ¦ Lab File ID: 2007Q515A053 , 20070515B053
% Moisture: 37 Decanted: (Y/N) N . Date Received: 04/30/2007 ^
Extraction: (Type) SONC ; Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000 (uL) Date Analyzed: 05/16/2007
f
Injection Volume: 2.0 (uL) GPC Factor: 2.0 Dilution Factor: 1.0 '¦
GPC Cleanup: (Y/N) Y pH: 7.8 Sulfur Cleanup: (Y/N) N ; :
Acid Cleanup: (Y/N) Y
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ucr/L or uq/kg) ug/kg
Q
12 674-11-2 .
Aroclor-1016
52
/
U.
11104-28-2
Aroclor-1221
52
U
11141-16-5
Aroclor-1232
52
U
53469-21-9
Aroclor-1242
52
U
12672-29-6
Aroclor-1248 '
52
U
11097-69-1
Aroclor-1254 .
52
U
11096-82-5
Aroclor-1260
52
U
37324-23-5
Aroclor-1262
52
U
11100-14-4
Aroclor-1268
52
U
£>/'-2-/^7
SOM01.1 (5/^|)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T4
Lab Name: DataChem Laboratories, Inc.
Lab Code: DAT AC Case No.: 36345;
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 32
Lab Sample ID: 7120009013
(g/mL) g_
Decanted: (Y/N) N
Lab File ID: 2 007 0515A054,20070515B054
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2 007
Concentrated Extract Volume: 10000
Injection Volume: 2 .0 (uL) GPC Factor:
GPC Cleanup: (Y/N) Y_ pH: 6^8.
(uL)
2.0
Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
49
U
11104-28-2
Aroclor-1221
49
U
11141-16-5
Aroclor-1232
49
u
53469-21-9
Aroclor-1242
49.
u
12672-29-6
Aroclor-1248
.49
u
11097-69-1
Aroclor-1254
49
u
11096-82-5
Aroclor-1260
49
u
37324-23-5
Aroclor-1262
49
. u
11100-14-4
Aroclor-1268
49
u
£>/I ^fo!
SOM01.1 {5/ffflf)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Gase No.: 36345.
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' '¦
Sample wt/vol: 30.0 (g/mL) g
% Moisture: 23 Decanted: (Y/N) N
Extraction: (Type) SONC
Concentrated Extract Volume: 10000
Injection Volume: 2 .0 (uL) GPC Factor: 2 . 0
GPC Cleanup: (Y/N) Y pH: 7J5
Acid Cleanup: (Y/N) Y
Lab Sample ID: 7120009014
Lab File ID: 2 0070515A055,2 0070515B055
Date Received: 04/30/2007
Date Extracted: 05/01/2007
(uL) Date Analyzed.: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kg) ug/kg
Q
12674-11-2
Aroclor-1016
43
U
11104-28-2 '
Aro.cl.or-1221
.43
U
11141-16-5
Aroclor-1232
43
U
53469-21-9
Aroclor-1242
43
U
12672-29-6
Aroclor-1248
43
U
11097-69-1
Aroclor-1254
43.
U
11096-82-5
Aroclor-1260
" 43
U
37324-23-5
Aroclor-1262
43
U
11100-14-4
Aroclor-1268
43
U
SOM01.1 (5/$p00)
-------
1H - FORM I ARO . .
AROCLOR ORGANICS ANALYSIS DATA SHEET
IZl&fLr. ten
EPA SAMPLE NO.
J86T7
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL (
Sample wt/vol: 30.0 (g/mL) g ;
% Moisture: 40 Decanted: (Y/N) N_
Lab Sample ID: 7120009015
Lab File ID: 2 0070515A056,20070515B056
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0 (uL) GPC Factor:
GPC Cleanup: (Y/N) Y pH: 7.4
Acid Cleanup: (Y/N) Y
(uL)
2.0
Date Analyzed: 05/16/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.'
COMPOUND
CONCENTRATION.UNITS:
(ucr/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
55
U
11104-28-2
Aroclor-1221
55
u
11141-16-5
Aroclor-1232
55
u
53469-21-9
Aroclor-1242
55
u
12672-29-6
Aroclor-1248
55
u
11097-69-1
Aroclor-1254
3 0-
JS
11096-82-5
Aroclor-1260
55
u
37324-23-5
Aroclor-1262
55
u
11100-14-4
Aroclor-1268
55
u
SOM01.1 (5/$p03)
-------
1H - FORM I ARO
AROCLOR ORGAN-ICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T7RE
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345;
Matrix
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
SOIL/SED/WATER) SOIL
Sample wt/vol: 30. 0
% Moisture: 40 Decanted: (Y/N) N
Lab Sample ID: 7120009015RE
(g/mL) g_
Lab File ID: 20070515A072,20070515B072
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
f
Injection Volume: 2 . 0 (uL) GPC Factor: 2 . 0
GPC.Cleanup: (Y/N) Y_ pH: 7^4
Acid Cleanup: (Y/N) Y
(uL) Date Analyzed: 05/17/2007
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/kg) ug/kg
Q
12674-11-2
Aroclor-1016
U
11104-28-2
Aroclor-1221
u
11141-16-5
Aroclor-1232
u
53469-21-9
Aroclor-1242 •
u
12672-29-6
Aroclor-1248
u
11097-69-1
Aroclor-1254
33
J
11096-82-5
Aroclor-1260
u
37324-23-5
Aroclor-1262
u
11100-14-4
Aroclor-1268
u
£//:
SOM01.1 (5/^p7l§)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86T8
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL ' -
Sample wt/vol: 30". 0 (g/mL) g
% Moisture: 39 Decanted: (Y/N) N_
Lab Sample ID: 7120009016
Lab File ID: 2 0070515A057,20070515B057
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2.0
GPC Cleanup: (Y/N) Y_
Acid Cleanup: (Y/N) Y_
(uL) Date Analyzed: 05/16/2007
(uL) GPC Factor: 2.0
pH: 6.1
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ug/kg) ug/kg
. Q
12674-11-2
Aroclor-1016
54
U
11104-28-2
Aroclor-1221
54
U
11141-16-5
Aroclor-1232
54
U
53469-21-9
Aroclor-1242
54
U
12672-29-6
Aroclor-1248
54
U
11097-69-1
Aroclor-1254
54
u'
11096-82-5
Aroclor-1260
54
u
37324-23-5
Aroclor-1262
54
u
11100-14-4
Aroclor-1268 .
54
u
SOM01.1 (5/$pJ)g)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W4
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No.: 36345:
Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOI L/SED/'WATER) SOIL
Sample wt/vol: 3 0 . 0
% Moisture: 32
Lab Sample ID: 7120009017
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 20070515A058,20070515B058
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0
(uL) Date Analyzed: 05/16/2007
GPC Cleanup: (Y/N) Y_
(uL) GPC Factor: 2.0
pH: 7.8
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
Acid Cleanup: (Y/N) Y_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ua/L or ucr/kq) ua/kq
Q
12674-11-2.
Aroclor-1016
48
U
11104-28-2
Aroclor-1221
. 48
U
11141-16-5
Aroclor-1232
48
U
53469-21-9
Aroclor-1242
48
U
12672-29-6
Aroclor-1248 .
48
U
11097-69-1
Aroclor-1254
48
u
11096-82-5
Aroclor-1260
48
U
37324-23-5
Aroclor-1262
48
U
11100-14-4
Aroclor-1268
48
U
SOM01.1 (5/ mv
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC . Case No. : 36345
_ Contract: EP-W-05-026
Mod. Ref No.:
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 36
Lab Sample ID: 7120009018
(g/mL) g_
Decanted: (Y/N) N_
Lab File ID: 2 0070515A059,20070515B059
Date Received: 04/30/2007 : '
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0
GPC Cleanup: (Y/N)Y_
Acid Cleanup: (Y/N) Y
(uL)
Date Analyzed: 05/16/2007
(uL) GPC Factor: 2 . 0
pH: 7^3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND .
CONCENTRATION UNITS:
(ua/L or uq/kq) uq/kq
Q
12674-11-2
Aroclor-1016
52
u
11104-28-2
Aroclor-1221.
52
u
11141-16-5
Aroclor-1232
52
u
53469-21-9
Aroclor-1242
52
u
12672-29-6
Aroclor-1248
52
u
11097-69-1
Aroclor-1254
52
u
11096-82-5
Aroclor-1260
52
u
37324-23-5
Aroclor-1262
52
u
11100-14-4
Aroclor-1268
52
u
'2./D 7
SOM01.1 (5/^p@4)
-------
^iPoPT F&W JStUJS
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W5RX
Lab Name: DataChem Laboratories, Inc.
Lab Code: DATAC Case No. : 3 6345;
Contract: EP-W-05-026
Mod. Ref No. :
SDG No.: J86R0
Matrix: (SOIL/SED/WATER) SOIL :
Sample iwt/vol: 30.0 (g/mL) g
% Moisture: 36 Decanted: (Y/N) N_
Lab Sample ID: 7120009018RX
Lab File ID: 2 0070517A021,20070517B021
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/14/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
Acid Cleanup: (Y/N) Y
(uL)
Date Analyzed: 05/18/2007
(uL) GPC Factor: 2 . 0
pH: 7.3
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N) N_
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or ug/ka) ug/kg
Q
12674-11-2
Aroclor-1016
.52
u
11104-28-2
Aroclor-1221
52
u
11141-16-5
Aroclor-1232
52
u
53469-21-9
Aroclor-1242
52
u
12672-29-6
Aroclor-1248
52
u
11097-69-1
Aroclor-1254
52
u
11096-82-5
Aroclor-1260
52
u
37324-23-5
Aroclor-1262
52
u
11100-14-4
Aroclor-1268
52
u
SOM01.1 (5/^g)g^)
-------
1H - FORM I ARO
AROCLOR ORGANICS ANALYSIS DATA SHEET
EPA SAMPLE NO.
J86W6
Lab Name: DataChem Laboratories; Inc.
Lab Code: DAT AC Case No.: 36345
Contract: EP-W-05-026
Mod. Ref No. :
SDG No. : J86R0
Matrix: (SOIL/SED/WATER) SOIL
Sample wt/vol: 30.0
% Moisture: 3 6
Lab Sample ID: 7120009019
(g/mL) g_
Decanted: (Y/N) N,
Lab File ID: 20070515A060,20070515B060
Date Received: 04/30/2007
Extraction: (Type) SONC
Date Extracted: 05/01/2007
Concentrated Extract Volume: 10000
Injection Volume: 2 . 0
GPC Cleanup: (Y/N) Y_
Acid Cleanup: (Y/N) Y_
(uL) Date Analyzed: 05/17/2007
(uL) GPC Factor: 2 . 0
pH: 1^1
Dilution Factor: 1.0
Sulfur Cleanup: (Y/N)
CAS NO.
COMPOUND
CONCENTRATION UNITS:
(ug/L or uq/kcr) uq/kq
Q
.12674-11-2
Aroclor-1016
51
U
11104-28-2
Aroclor-1221
51
u
11141-16-5
Aroclor-1232
51
u •
53469-21-9
Aroclor-1242 .
51
u
12672-29-6
Aroclor-1248
51
u
11097-69-1
Aroclor-1254
51.
u
11096-82-5
Aroclor-1260
51
u
37324-23-5
Aroclor-1262
51
u
11100-14-4
Aroclor-1268
51
u
6/j:2-/0J
SOM01.1 (5/^)g)
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 10 LABORATORY
7411 Beach Dr. East
Port Orchard, Washington 98366
QUALITY ASSURANCE MEMORANDUM
FOR GRAIN SIZE ANALYSES
Date:
October 15, 2007
To:
Joanne Labaw, SAM
Office of Environmental Cleanup, USEPA Region 10
From:
Chris Pace, Chemist
Office of Environmental Assessment, USEPA Region 10 Laboratory
Subject: Quality Assurance Review for the Grain Size Analysis of Samples from the Drums Marine Dr
NE project
Project Code: TEC-895A
Account Code: 08T10P302DD2C10ZZLA00
The following is a quality assurance review of the data for grain size analysis of 2 sediment samples from the
above referenced site. The analyses were performed by EPA Region 10 Laboratory ESAT contractor using
Manchester Environmental Laboratory guidelines and ASTM D 421 - 85 (Standard Practice for Dry
Preparation of Soil Samples for Particle Size Analysis and Determination of Soil Constants).
The original laboratory request was to select one representative sample for grain size analysis. However, after
a thorough visual check of all 33 samples, approximately half were clay/silt samples and the other half were
coarse sand/small gravel samples (see Results section). The decision was to do 2 grain size fractions using the
following representative samples:
07174003 07174036
Should questions arise regarding the data, contact Chris Pace at the Region 10 Laboratory, phone number
(360) 871 - 8703.
-------
Data Review
Drums NE Grain Size
Page 2 of 2
1. Sample Transport and Receipt
Upon sample receipt, no conditions were noted that would impact data quality.
2. Sample Preparation
Samples were prepared according to the method and summarized below.
Each sediment sample came in an 8 oz glass container and the preparation involved: (1) Transferring each
sediment sample into drying trays and mixing the separated water back into the sediment of each sample. (2)
Recording the total wet weight minus tray tare. (3) Air drying each sample for approximately two days until
dry weights were within 1%. (4) Recording the total dry weight minus the tray tare. (5) Sieving 4 fractions
(3/8, 10, 30, and 170) for each sample using a Roto-tapper under a lab hood. (6) Weighing each sieved
fraction. (7) Recording the percentage of each fraction to the original total dry weight of whole sample.
3. Results
Grain Size
Sample#
Sample#
07174003
07174036
>3/8" Fraction (greater than 9.4 mm - Large Gravel)
0%
0%
<3/8" but >10 Fraction (between 2.0 mm and 9.5 mm - Gravel)
3%
3%
<10 but >30 Fraction (between 0.59 mm and 2.0 mm - Coarse
Sand)
18%
24%
<30 but >170 Fraction (between 0.088 mm and 0.59 mm - Fine to
Medium Sand)
78%
33%
<170 Fraction (less than 0.088 mm - Clay and Silt)
0%
39%
4. Representative Samples
Sample 07174003 was a mostly coarse sand/small gravel sample that was similar to the following samples:
07174000, 07174002, 07174004, 07174005, 07174006, 07174007, 07174008, 07174011, 07174014,
07174015, 07174016, 07174024 and 07174027.
Sample 07174036 was a mostly clay/silt sample that was similar to the following samples:
07174009, 07174010, 07174012, 07174013, 07174017, 07174018, 07174019, 07174020, 07174021,
07174022, 07174023, 07174025, 07174026, 07174028, 07174029, 07174034, 07174035, and 07174037.
-------
APPENDIX D
SAMPLE ALTERATION FORMS
-------
Sample Plan Alteration Form
Project Name and TDD Number:
])rumS - AJE DtTi'ufi
TDD (*>&--01- Op PC,
Material to be Sampled:
^c^rv^o'l: -Trom { Ke Cc>ju fiigp
Measurement Parameter:
'ioicA grcjriYiu rsrhnn^, j^-PaffYUry
Standard Procedure for Field Collection and Laboratory Analysis (cite reference):
u). ll fbr ben's &.»i fi ) yC'3 k)A<, &fvd<*'cJ
Special Equipment, Materials, or Personnel Required: , . •; I /
•ftrt-tTg'y A SQ ^\cip0llu^ I pi fa LJQS (; k W tH) T
Fpft may gj SOC?^.
o
jxkL /pL-, Date: O^h
Initiator's Name:
Project Manager: ^ Date:
QA Officer: . "L-- ¦ ''-t- / ' >''' i—, Date: ' ''
-------
Sample Plan Alteration Form
Project Name and TDD Number: ^
r>ru-onS - AJE Marine DfivAi
Tt>D CiC-o-?- 0006
Material to be Sampled: J\ C \ 1 ^ ' i ^
S-"cVitt\evrf Ln(? VQlUnibiQi ly'lc5^
r: SV'OC^t TkI I Cil)r% "PCBs, TT)£. 0K"/ctJs)
Measurement Parameter, uvvjy^ i c Nl i i^iw i v'ja>
\ O'ir-oj c.u~Carh o nS /\ fVAPvC ^ j
Standard Procedure for Field Collection and Laboratory Analysis (cite reference): X
Cc-WecT ^ Seniles Cb^b-Siyoi ^ly-IO^D-^J
fT^UcuJ
Reason for Change in Field Procedure or Analysis Variation: . I t 41
Co I tecX* A four extra So nop K t? beif^rCiSSics's
"Hmp -exff ni: CcrA urni ncr('or") CD^fo-Sb-?/j jrWD-Sb-B"f)
Variation from Field or Analytical Procedure: .
Sq.iwp>\e *b^AS)~$\>-30 (J ity
btc k ye^ocV ScitvipJe to c <• iIpc t<^c!( 0/i'i Hp d v ^ ir? r< ^
Special Equipment, Materials, or Personnel Required:
f\o ne
Initiator's Name: 1 LUVy^-^——s Date: ) j^C) JC)~~f'
Project Manager: Date: I/W6?
QA Officer: ~ji'i-l''—- Date: 3 ^ L
3 3j ty,c. celK.'/<-<) i'i 1 cWjnj/ffain
-tV(w {Ke Whesf U<^
-------
Sample Plan Alteration Form
Project Name and TDD Number:
nOftp.of Pfi
TbtiC&-0=»-OOOft
Material to be Sampled: \ p / /' I I £» •
gerh'mionr TQCV^ ~Lhe Lol^nnblcx K'C'en
Measurement Parameter:
leasurement Parameter: j rc^ c'L(C'f--> ¦ I V I,
^ArV"Tb-/:At carbon's "fr Oyr'cmy
Standard Procedure for Field Collection and Laboratory Analysis (cite reference): .
*TK^ S&rKblg loCcct^d)ns ulll ke. cW|eirmiV?aA "Tr.'mb'-o&
Variation from Field or Analytical Procedure: x ,
TtNs.ceckA I and ho O'Mt)~~ 3^ STo^pl? lecst'on
Uy>te> *vm»ipc\ t&inc Kg (rPMk'pQ t)^"j IK t' r ?f\ el ¦ W f^s
C CjA' ff<-<> • ;t''crV i'CA b«~' '1^) ) "A- STftRV-3 0-t*rr»i*'i hetkjhcl^ (?CCS
kTXO ,M1 * « a TVO V. l^_OM T \ < 11 • /L-'CTj ^ 1 1 I -Si -» « M «\ * \J~ »'»*'• ' 'H*C* l^'
Special Equipment, Materials, or Personnel Required: , i , , i -
C-X>\lsO-hv , GArM)K/ '^CC j G-q, ^,x hftocAhgH (nOC
Initiator's Name:
Project Manager:
. .)x M
i^C-tx ( {X\y Date: SJloM
C7
Date: J_
QA Officer: '/ i-/ ^ -/i t Date: ^ ^"' °^
-------
Sample Plan Alteration Form
Project Name and TDD Number: "X
Or u m - l\j E c'r 10 f- Uf1
Q T-hp ( c ' U ^ D\ C\ |v t tx (
Measurement Parameter: ^V'oc^ Tes/icicifS, PcBs.Tftl- Mo.isx
nt>-St)-Q^ ire "fyMb-S^-n LJ<»rD~"^G> -^S .
^.v^plcs Cc|l?C"tf5c\ "Tt r £(>"«v O^'icVt'n^ t '»&> cArUiin^, CTe-thicX' SOl^T5
Reason for Change in Field Procedure or Analysis Variation: i *
t>u^ ~£o U'U) VV^ibi'li^y -Cor -(.We FPf^ ^-> 4ci<
Special Equipment, Materials, or Personnel Required:
pome
Initiator's Name: Date: Ao/o?
Project Manager: ^ Date:
•7 /
QA Officer: /// ^/7 Date: ^ ^ °
y / J ^ w '
5 /Wo?-
-------
APPENDIX E
EPA DIVE REPORT
-------
UNITED STATES ENVIRONMENTAL PROTECTION AGENCY
REGION 10
1200 Sixth Avenue
Seattle, Washington 98101
DIVE REPORT - May 8, 2007
From: Rob Pedersen, Unit Diving Officer, Dates of dive: April 24-26, 2007
Divemaster
To: Keven McDermott, Dive Team Sponsor, Unit Manager, IEU
Bill Riley, OEA Director
Project: Columbia River drums
Requested by: Superfund program
Purpose: Scientific Investigation/Sampling
Location: Location: Approx. N45 34.914 W122 33.582 110-112 RM, south channel, just downstream of 1-205
bridge, between Lemon Island (part of Government Island Complex) and mainland Oregon, near Portland airport.
Scientific Objectives: We supported the Superfund program investigation to characterize the extent of
sediment contamination (metals, hydrocarbons - see Dive Plan for background details) in and around an area of
discarded drums. Scores of decaying drums and the presence of hazardous substances was documented by
ODEQ. Divers collected sediments cores: downstream of, amongst, and upstream of the drum depot. Analysis
results from core and grab samples (the latter were collected prior to diving at background stations by petite
Ponar) will be published under separate cover by TechLaw for Superfund.
Dive observations: Figure 1 depicts the general area of the drums (see the Dive Plan for a map showing the
proposed sampling area). Figures 2 and 3 give more detail in areas where dives were clustered. Table 1 lists the
GPS waypoint data; this locational information can be used with the data report, when available. Divers
estimated there were dozens of drums in conditions ranging from highly decomposed to intact but rusted.
Previous reports were of scores or hundreds of drums.
Afternoon on April 24. The first dive was done in mid-channel based on the previously reported GPS location
(see Fig. 1, "DRUMS")- High current limited the possible sweep range to a total sweep angle of 45 degrees
(diver swimming left and right on the tether). No drums were found. The bottom at about 20" consists of shifting
sand. The second dive was conducted closer to shore in less current and where the bottom consisted more of clay,
and silty-sand (seep angle of about 60-90 degrees). Sweeping away from shore to 13" deep, the diver noted a
steep drop-off to 20-25". A variety of metal garbage was noted, but no drums.
April 25. With the assistance of the Portland Fire Department dive team, two dives were made upstream of the
GPS flagging ("DRUMS"). No drums were located, only other metal debris. Two cores were obtained on the
second dive of the day. A core's diameter was four inches, one end was capped pre-dive, and numbered. The
diver reported the sample number and where the core was taken. The diver also gave descriptions of the substrate
type and waste debris found. The core were carried in a goodie bag. Two full cores in the bag made diver
movement difficult on the tether, in current.
Based on a site picture (using landmarks on Lemon Island) the operation moved downstream and closer to shore.
In the first area searched - downstream of waypoints 143-145, many drums were found (a few in clusters ranging
to singles, most in an advanced state of decay). On dive #5, a core sample was obtained by a drum, 10 meters out
on the tether line. Several more cores were taken around drums farther out on the tether (to about 37 meters).
Dives and coring proceeded from downstream to upstream. Due to poor visibility (until just off the bottom, 2-3"
depending on if the sun was out), an accurate drum count was not possible.
April 26. To further characterize the study zone, diving and sampling was planned for downstream of the
previous day's work and moving upstream to the lower boundary of dive number eight. The diver estimated one
to two dozen drums were in this area. On dive number nine, two cores were taken near drums. An intact drum
was noted at about 16 meters on the tether with other open/broken drums on dive #10; a core was obtained. A
-------
media event occurred during dives 11 and 12 (waypoints 148 and 149). Many drums were located and cores were
taken including two cores from inside of two drums (full of silt and sand). One intact drum had a bulging end.
Dives 13-15, waypoints 150-152 proceeded upstream. At 150, two drums were noted and cores obtained
(difficult to sample here given the mostly clay-like bottom). Two cores were taken at 151 and 152 each, but no
drums were seen. The final diving was for one of the upstream "background" samples for methods comparison to
the Ponar grab sampling. Station 153 was more off-shore than most of the sampling to obtain a core of a sandy-
silt substrate. Site 154 was in a clay-sand substrate. Although referred to as "clay" for description purposes, the
material was unlikely taie clay due to current and the type of material that could settle out.
Figure 1. Approximate drum deposition area. Yellow ovals demarcate the area of located drums.
2
-------
Figure 2. GPS locations of anchor points for dive surveys and core sampling.
-\™——
*%Jo
- 6 O 5
X>-
\ A
|0148j
jmm
EbT 13
^ ^01521 I u
J0142I
jDRUMSl H
^\N0141|
V\\
_ \ja
1 \ pile
1®
Fixed
Bridge
I 800 ft^
GPS Map Detail
Table 1. Locational data for anchor points and dives.
N45 34.914 W122 33.582 "DRUMS" (GPS location reported by Sheriff Dept. and ODEQ).
0139
0140
0141
0142
0143
0144
0145
0146
0147
0148
0149
0150
0151
0152
0153
0154
24-APR-
24-APR-
25-APR-
25-APR-
25-APR-
25-APR-
25-APR-
25-APR-
26-APR-
26-APR-
26-APR-
26-APR-
26-APR-
26-APR-
26-APR-
26-APR-
07 15:04
07 16:20
07 10:39
07 11:54
07 13:16
07 16:08
07 16:45
07 16:46
07 09:41
07 11:14
07 11:57
07 12:58
07 14:04
07 15:04
07 15:46
07 16:14
N45 35.050
N45 34.917
N45 34.882
N45 34.938
N45 35.228
N45 35.223
N45 35.219
N45 35.219
N45 35.381
N45 35.362
N45 35.339
N45 35.324
N45 35.295
N45 35.256
N45 34.804
N45 34.801
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
W122
33.600
33.578
33.472
33.559
34.120
34.097
34.118
34.118
34.483
34.434
34.388
34.330
34.285
34.210
33.339
33.352
7 ft
13 ft
2 ft
6 ft
4 ft
-8 ft
5 ft
8 ft
10 ft
10 ft
17 ft
15 ft
7 ft
9 ft
9 ft
11 ft
3
-------
Figure 2. Detail of anchor/dive locations.
Figure 3. Initial search area and final core (upstream background) locations.
BHD
14
\
JDRUMS
\
\
rF3
\
\
o \
W\
\ \
2
-
\
ffl™
17
200 ft
\ \ \
overzoom
Personnel:
Divers: Tim Siwiec (TS), Sean Sheldrake (SS), Rob Pedersen (RP)
Boat Operator: Curt Black, Dave Terpening
Dive Details: see Summary Table, below.
4
-------
Hazards: Diver entanglement in debris, potential for suit/body puncture. Rapid ascent due to current/tethering.
Injury potential exiting water in high current (for mid-channel dive).
Exposures: Sediment - heavy metals and hazardous hydrocarbons (see Dive Plan). Water - unknown
contaminants in site-related water discharging from outfalls.
Diver/Equipment Issues - Assignments (in bold):
-SS with a bad cold and sinus issues - self treated with meds.
-RP's Viking exhaust valve (left arm) leaked; cleaned in sink that PM and orally blew through the valve; no
further problems. Divers need to periodically remove and clean these valves especially diving in sandv/siltv
conditions.
-Need to check for spare clip-rings ("carabineers") in cooler/DM kit.
-AGA clean, reassemble (RP, done).
-Hang/dry tether, stow (SS, done).
-Recharge batteries (SS, done).
-Fill tanks, leaving ones needing hydro (TS, done/in progress).
A hole in the starboard side of the Monitor (occurred while trailering) the first morning of diving caused the
divers to use the samplers' boat the Wooldridge. Samples were processed on shore at the boat ramp. The
Monitor was repaired by that afternoon and was used for the rest of the dive operations.
First Aid Supplies Expended: none
Decontamination: Freshwater rinse.
Table 2 - Dive Summaries:
Date/dive
event
Divers
Max
Depth/ft
Bottom
Time/min
Comments
Dive 1
5/24
RP
22
35
Anchor 1, waypoint 139,
midchannel.
Dive 2
5/24
RP
20
41
Anchor 2, WP140
midchannel, E of anch. 1.
Dive 3
5/25
TS
18
34
Anchor 3, WP141
L bank, near/upstream
GPS flag.
Dive 4
5/25
TS
25
30
Anchor 4, WP142
L bk, deeper bet. 2 & 3,
2 core samples.
Dive 5
5/25
SS
13
7
Anchor 5, WP143
L bk, dwnstr. per picture,
core at drum, 10m out.
Dive 6
5/25
SS
13
22
Anchor 6, WP143(same)
L bk, 4 cores in lg. drum
area, 2 trips, ~37m out.
Dive 7/8
(same dive)
5/25
SS
12
37
Anchor 7&8, WP144
&145, L bk, uptr., no
samples.
5
-------
Dive 9
5/26
RP
13
37
Anchor 9, WP147
L bk, dwnstr. or 5/25,
drums, 2 cores.
Dive 10
5/26
RP
13
7
Same loc., return to
sample in drum, 16m
out. Lots of drums.
Dive 11
5/26
RP
11
24
Anchor 11, WP148
L bk, cores in/around
drums (1 in drum).
Dive 12
5/26
RP
13
27
Anchor 12, WP149
L bk, 2 cores.
Dive 13
5/26
TS
14
30
Anchor 13, WP150
L bk, contupstr, 2 drums
& 2 cores.
Dive 14
5/26
TS
14
29
Anchor 14, WP151
L bk, no drums, 2
samples.
Dive 15
5/26
TS
14
16
Anchor 15, WP152
L bk, less sweeping, no
drums, 2 cores.
Dive 16/17
(same dive)
5/26
TS
8
31
Anchor 16&17, WP153
& 154 uprstr.2 bkground
cores, towards channel,
more sand, then L bk,
Site charge account code: 07T 10N 302DD2C 10ZZQB00.
6
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