NHEXAS PHASE I REGION 5 STUDY

List of Available Documents:
Protocols and SOPs


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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1. QUALITY SYSTEMS AND IMPLEMENTATION PLAN

SOP Number	Entry Title and Author

ID

RTI/5740/02-02QSIP 18440 "Quality Systems and Implementation Plan for Human

Exposure Assessment Study," Research Triangle Institute,
and Environmental and Occupational Health Sciences
Institute, E. Pellizzari, Principal Investigator, May 1995.

2. SAMPLE COLLECTION AND FIELD OPERATIONS PROTOCOLS AND SOPS

SOP Number

RTI/ACS-AP-209-001

RTI/ACS-AP-209-002

RTI/ACS-AP-209-003
RTI/ACS-AP-209-010
RTI/ACS-AP-209-011
RTI/ACS-AP-209-012

EOHSI-AP-209-020
EOHSI-AP-209-021

Entry
ID

16860

16879

16880

16882

16899

16919

16921

17948

Title and Author

"Procedure for Collection, Storage, and Shipment of Standing
Tap Water Samples for Metals By EPA Method 200.8,"
Research Triangle Institute, M. Roberds and K. Thomas, June
1994.

"Procedure for Collection, Storage, and Shipment of Flush
and Drinking Water or Drinking Water Samples for Metals by
EPA Method 200.8," Research Triangle Institute, M. Roberds
and K. Thomas, June 1994.

'Trocedure for Collection, Storage, and Shipment of Drinking
Water Samples for YOCs by EPA Method 524.2," Research
Triangle Institute, M. Roberds and K. Thomas, June 1994.

"Personal, Indoor and Outdoor Air Sampling Procedures for
Total Inspirable and PM10 Aerosols," Research Triangle
Institute, C. Rodes, June 1994.

"NHEXAS Filter Handling, Weighing and Archiving
Procedures for Aerosol Samples," Research Triangle Institute,
C. Rodes, June 1994.

'Trocedure for Collection, Storage, and Shipment of Samples
for Volatile Organic Compounds in Personal, Indoor,
Outdoor, and Occupational Air" Research Triangle Institute,
K. Thomas, June 1994.

"Dust Sampling Workplan," Environmental and
Occupational Health Sciences Institute, T. Wainman, June
1994.

"Soil/Street Sampling Workplan," Environmental and
Occupational Health Sciences Institute, T. Wainman, June
1994.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number	Entry

ID

RTI/ACS-AP-209-030	16959

EOHSI-AP-209-040	16979

RTI/ACS-AP-209-046	17019

RTI/ACS-AP-209-070	17079

RTI/ACS-AP-209-071	17080

RTI/ACS-AP-209-080	17099

RTI/ACS-AP-209-081	17119

RTI/ACS-AP-209-082	17120

RTI/ACS-AP-209-083	17139

RTI/ACS-AP-209-084	17159

RTI/ACS-AP-209-085	17160

RTI/ACS-AP-209-086	17161

RTI/ACS-AP-209-087	17179

RTI/ACS-AP-209-090	17180

RTI/ACS-AP-209-095	17181

Title and Author

"Procedure for Collection, Storage, and Shipment of
Duplicate Diet Food and Beverage Samples," Research
Triangle Institute, K. Thomas, June 1994.

"Human Biological Markers: Sample Collection and
Analyses," Environmental and Occupational Health Sciences
Institute, J. Waldman and Kent Thomas, June 1994.

"Procedure for Collection, Storage, and Shipment of Hair
Samples for Trace Metals," Research Triangle Institute, K.
Thomas, June 1994.

"Sample Coding, Labeling, and Tracking Procedures,"
Research Triangle Institute, K. Thomas, June 1994.

"Sample Custody Procedures," Research Triangle Institute,
K. Thomas, June 1994.

"NHEXAS Pilot Field Study Scripting and Logistics,"
Research Triangle Institute, Kent Thomas, June 1994.

"Field Sample Storage Procedures," Research Triangle
Institute, Kent Thomas, June 1994.

"Procedures for Field Checks of Equipment," Research
Triangle Institute, Kent Thomas and Charles Rodes, work in
progress.

"Sample Shipping Procedures," Research Triangle Institute,
Kent Thomas, June 1994.

"Field Vehicle Operations and Maintenance Procedures,"
Research Triangle Institute, Kent Thomas, work in progress.

"Field Staff Safety and Decorum," Research Triangle
Institute, Kent Thomas.

"Field Use of the Sample Collection and Custody Software,"
Research Triangle Institute, Kent Thomas, June 1994.

"Comprehensive Approach to Participant Training and
Minimization of Burden," Research Triangle Institute, Kent
Thomas and Harvey Zelon.

"Handling Quality Control Samples in the Field," Research
Triangle Institute, Kent Thomas, June 1994.

"Field Staff Training," Research Triangle Institute, Kent
Thomas, work in progress.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number

Entry
ID

Title and Author

NHX-SOP-190-002

16859 "Standard Operating Procedure for Handling Human Blood
and Other Body Fluids," Research Triangle Institute, C.
Sparacino, May 1991.

3. SAMPLE ANALYSIS PROTOCOLS AND SOPS

SOP Number

RTI/ACS-AP-209- 111

NHX-SOP-171-005

NHX-SOP-171-006

RTI/ACS-AP-209-112

NHX-SOP-184-001

NHX-SOP-184-002

EOHSI-AP-209-120

RTI/ACS-AP-209-121

RTI/ACS-AP-209-122
RTI/ACS-AP-209-123

Entry
ID

17182

16820

16839

17183

16840

16841

17184

17185

17186

17187

Title and Author

"Analysis of Teflon Filters Used in Personal Air Monitoring
Samplers for Lead, Arsenic, Cadmium, and Chromium,"
Research Triangle Institute, R. Fernando, June 1994.

"Standard Operating Procedure for the Calibration of Perkin
Elmer (PE) Model 5100 ZL Atomic Absorption
Spectrometer: Graphite Furnace," Research Triangle Institute,
M. Lang, Revision 0, February 1992.

"Standard Operating Procedure for Maintenance of Perkin
Elmer (PE) Model ZL5100 PC Atomic Absorption
Spectrometer, Research Triangle Institute, M. Lang, Revision
0, January 1992.

"Analysis of Volatile Organic Compounds from charcoal
Badges by Gas Chromatography/Mass Spectrometry,"
Research Triangle Institute, J. Keever, June 1994.

"Standard Operating Procedure for Maintenance of the
Hewlett-Packard 5988A GC/MS System," Research Triangle
Institute, J. Keever, October 1990.

"Standard Operating Procedure for Tuning of the HP-5988A
Mass Spectrometer," Research Triangle Institute, J. Keever,
October 1990.

"Analysis of Dust and Soil for Lead, Cadmium, and
Chromium" Environmental and Occupational Health
Sciences Institute, B. Buckley, March 1994.

"Analysis of Wipes Used in Lioy-Wiesel Surface Samplers for
Arsenic," Research Triangle Institute, R. Fernando, June
1994.

"Analysis of Carpet Dust for Arsenic," Research Triangle
Institute, R. Fernando, March 1994.

"Analysis of Soil Samples for Arsenic," Research Triangle
Institute, R. Fernando, March 1994.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number

EPA Compendium

FDA Compendium

CDC Compendium

Entry
ID

17360

17361

17322

Title and Author

"Compendium of Methods for Analysis of Metals and YOCs
in Water," U.S. Environmental Protection Agency,
Environmental Monitoring Systems Laboratory, 1991-1994.

"Compendium of Methods for Analysis of Trace Metals in
Dietary Samples Using Total Diet Study Procedures," Food
and Drug Administration, Total Diet Study Laboratory,
November 1993.

"Compendium of Method Summaries for Collection and
Analysis of Metals and YOCs in Blood and Urine," Centers
for Disease Control, National Center for Environmental
Health, Division of Environmental Health Laboratory
Sciences, July 1993.

4. SOPs FOR RTI TRACE METALS FACILITY

SOP Number

NHX/SOP-300-001

NHX/SOP-300-002

NHX/SOP-300-003

NHX/SOP-300-004

NHX/SOP-300-005

NHX/SOP-300-006

Entry
ID

17279

17280

17281

17282

17283

17284

Title and Author

"Standard Operating Procedure for Operation of PS
Analytical Hydride Generation Atomic Fluorescence
Spectrometer (HGAF)," Research Triangle Institute, R.
Fernando, June 1994.

"Standard Operating Procedure for Safety in the ACS
Inorganic Clean Lab Facility," Research Triangle Institute, R.
Fernando, June 1994.

"Standard Operating Procedure for Purification of Reagents
in the ACS Inorganic Clean Lab Facility for Trace/Ultratrace
Metal Analysis," Research Triangle Institute, R. Fernando,
June 1994.

"Standard Operating Procedure for Monitoring and
Maintenance of the Cleanliness of the ACS Inorganic Clean
Lab Facility," Research Triangle Institute, R. Fernando, June
1994.

"Standard Operating Procedure for the Maintenance of PSA
(Excalibur) Hydride Generation-Atomic Fluorescence
Spectrometer (HG-AFS)," Research Triangle Institute, R.
Fernando, June 1994.

"Standard Operating Procedure for the ACS Inorganic Class
100/10,000 Clean Lab Facility," Research Triangle Institute,
M. Lang, June 1994.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number

NHX/SOP-300-007

NHX/SOP-300-008
NHX/SOP-300-009

Entry
ID

17285

17286

17287

Title and Author

"Standard Operating Procedure for Cleaning Labware in the
ACS Inorganic Class 100/10,000 Clean Lab Facility,"
Research Triangle Institute, M. Lang, June 1994.

"Standard Operating Procedure for the Mettler AT 261
Analytical Balance," Research Triangle Institute, R. Fernando,
June 1994.

"Standard Operating Procedure for the Hydro 'PicosystemŽ
Plus' Ultrapure Water System," Research Triangle Institute, R.
Fernando, June 1994.

5. GENERAL LABORATORY SOPS

SOP Number

Entry
ID

Title and Author

NHX-SOP-120-001

16679 "Standard Operating Procedure for Proper Use and

Maintenance of Laboratory Notebooks," Research Triangle
Institute, R. Handy and G. McNeill, Revision 2, August 1990.

NHX-SOP-120-002

NHX-SOP-120-003

NHX-SOP-150-001

NHX-SOP-160-001

NHX-SOP-160-002

NHX-SOP-160-005

16680 "Standard Operating Procedure for Proper Use and

Maintenance of Instrument Log Notebooks," Research
Triangle Institute, D. Smith, Revision 1, September 1990.

16699 "Standard Operating Procedure for Proper Use and

Maintenance of Chemical Log Notebooks," Research Triangle
Institute, D. Smith, Revision 1, August 1990.

16719 "Standard Operating Procedure for Cleaning

Glassware/Plasticware," Research Triangle Institute, R.
Handy, Revision 1, August 1990.

16739	"Standard Operating Procedure for Calibration of a Mettler
PL1200 Balance," Research Triangle Institute, D. Smith,
Revision 2, August 1990.

16740	"Standard Operating Procedure for Calibration of a Mettler
M5 Analytical Balance," Research Triangle Institute, D.

Smith, Revision 2, August 1990.

16741	"Standard Operating Procedure for Cahn 29 Electrobalance,"
Research Triangle Institute, G. McNeill and R. Reges,

Revision 2, October 1992.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number	Entry

ID

NHX-SOP-160-008	16759

NHX-SOP-160-009	16779

NHX-SOP-163-001	16799

NHX-SOP-163-003	16819

6. QUALITY ASSURANCE SOPS

SOP Number	Entry

ID

NHX-SOP-lOO-OOl	16599

NHX-SOP-100-002	16600

NHX-SOP-100-003	16601

NHX-SOP-110-002	16619

NHX-SOP-810-002	17299

NHX-SOP-815-001	17301

NHX-SOP-815-002	17300

NHX-SOP-815-003	17319

Title and Author

"Standard Operating Procedure for Mettler AE 163 and AE
240 Electronic Balance," Research Triangle Institute, C.
Sparacino, Revision 1, May 1992.

"Standard Operating Procedure for Mettler AE 160
Electronic Balance," Research Triangle Institute, C.

Sparacino, November 1990.

"Refrigerators and Freezers," Research Triangle Institute,
C. Sparacino, November 1990.

"Standard Operating Procedure for Drying Ovens," Research
Triangle Institute, C. Sparacino, November 1990.

Title and Author

"Standard Operating Procedure for Preparation of a Standard
Operating Procedure," Research Triangle Institute, D. Smith,
June 1994.

"Standard Operating Procedure for Revising Standard
Operating Procedures," Research Triangle Institute, D. Smith,
June 1994.

"Standard Operating Procedure for Preparation of a
Protocol," Research Triangle Institute, D. Smith, June 1994.

"Standard Operating Procedure for RTI/EOHSI Quality
Assurance Officer," Research Triangle Institute, D. Smith,
June 1994.

"Standard Operating Procedure for Preparation and Handling
of Performance Evaluation Samples," Research Triangle
Institute, D. Smith, June 1994.

"Standard Operating Procedure for Conducting Systems
Audits," Research Triangle Institute, D. Smith, June 1994.

"Standard Operating Procedure for Conducting Laboratory
Notebook Inspections," Research Triangle Institute, D.

Smith, Revision 1, August, 1990.

"Standard Operating Procedure for Conducting Instrument
Log Notebook Inspections," Research Triangle Institute, D.
Smith, Revision 1, August 1990.


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NHEXAS PHASE I REGION 5 STUDY-List of Available Documents

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SOP Number

NHX-SOP-815-004
NHX-SOP-820-001

Entry
ID

17320

17321

Title and Author

"Training File Inspections," Research Triangle Institute, D.
Smith, June 1994.

"Standard Operating Procedure for Certification of Standard
Weights," Research Triangle Institute, G. McNeill, September
1993.

7. SURVEY OPERATIONS PROCEDURES

SOP Number

EOHSI-AP-209-300

EOHSI-AP-209-301

Entry
ID

17197

17198

RTI/CSUR-AP-209-302 17220

Title and Author

"NHEXAS Time/Activity Diary Collection Protocol,"
Environmental and Occupational Health Sciences Institute,
N. Freeman, July 1994.

"NHEXAS Time/Activity Diary Processing and Analysis
Protocol," Environmental and Occupational Health Sciences
Institute, N. Freeman, July 1994.

"Field Interviewer Manual," Research Triangle Institute,
Survey Research Division, February 1996.

8. DATABASE MANAGEMENT

SOP Number

RTI/ACS-AP-209-400

Entry
ID

17262

Title and Author

"Procedure for Receipt, Processing, and Assembly of
Analytical Results and Questionnaire Data into a Database,"
Research Triangle Institute, L.C. Michael, June 1994.

9. DATA ANALYSIS

SOP Number

EOHSI-AP-209-600

Entry
ID

17939

Title and Author

"Exposure and Dose Assessment Modeling and Evaluation,"
Environmental and Occupational Health Sciences Institute, P.
Georgopoulos, March 1994.


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