East Helena

Zero-Valent Iron Permeable Reactive Barrier Treatment of Arsenic in Groundwater

ABSTRACT:

The East Helena site in Lewis and Clark
County, Montana operated for more than
100 years as a primary lead smelter. The
decades of smelting operations at the site
deposited lead, arsenic, copper, zinc,
cadmium, and some 15 other hazardous
substances into the soil, surface water,
and groundwater, A pilot-scale zero-valent
iron (ZVI) permeable reactive barrier (PRB)
was first installed at the site in 2005 to
treat arsenic contaminated groundwater.
On site, the PRB is located just west of the
slag pile, and situated down gradient
about 600 feet from the main contaminant
source. Preliminary evaluation of the
system indicates that arsenic
concentrations as high as 20 mg/L are
reduced to below 0.010 mg/L within the
barrier. This case study focuses on the
effectiveness to date of the pilot-scale ZVI
PRB in treating arsenic contaminated
groundwater.

Site Background

East Helena

CERCLIS ID: MTD006230346

The East Helena site is located in East Helena, Montana in
Lewis and Clark County. The site is the location of a primary
lead smelter that also recovered zinc and other metals. The
East Helena Smelter operated for more than 100 years from
the late 1880s through the early 21st century, ASARCO,
formerly the American Smelting and Refining Company,
purchased the 160 acre site from the Helena and Livingston
Lead Smelting Company in 1899. The decades of lead and
zinc smelting operations at the site deposited lead, arsenic,
copper, zinc, cadmium, and some 15 other hazardous
substances into the soil, surface water, and groundwater.
Smelting operations continued until 2001 when ASARCO
placed the smelter in "indefinite closed status." (U.S. EPA,
1999).

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East Helena Technology Case Study

Zero-Valent Iron Permeable Reactive Barrier

Source
Isolation

In 1984, the East Helena Smelter
was added to the National
Priorities List (NPL) because of
contaminated soils in East
Helena residential areas,
elevated blood lead-levels in
children, elevated metal levels in
air, and contaminated process
ponds over shallow groundwater
near the plant. Process ponds at
the site were identified as the
primary sources of groundwater
contamination which was
detected in the shallow aquifer
under the plant.	The

contamination extended into the
aquifer underlying the City of
Helena. Of the contaminants
detected in the groundwater,
arsenic is the most mobile in the
groundwater system and is
present in relatively high
concentrations (U.S. EPA, 1999).
This case study focuses on the
effectiveness to date of a pilot-
scale zero-valent iron (ZVI)
permeable reactive barrier (PRB)
Figure 1: East Helena arsenic plume.	in treating arsenic contaminated

groundwater.

Waste Stream Characteristics

East Helena was added to the NPL in 1984 partly due to contaminated process ponds located over
shallow groundwater. Due to the smelting operations at East Helena that occurred for over 100
years, groundwater at East Helena has high concentrations of arsenic existing in the redox state of
arsenite (As3+) and arsenate (As5+). The arsenic plume targeted by the PRB is roughly 450 feet wide
extending 2,100 feet downgradient from the primary source of subsurface contamination (Figure 1).
In the area surrounding the site, groundwater flow varies from about 0.5 to 3.0 ft/day. The average
pretreatment concentration of arsenic in the groundwater is 20 mg/L whereas the maximum
contaminant level (MCL) for arsenic is 0.010 mg/L (U.S. EPA, 2005).

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Treatment Technology

Construction on the ZVI PRB began at the East Helena
site in spring of 2005. The PRB remedial technology for
treatment of groundwater can be used for a wide
array of organic and inorganic contaminants.
However, in designing a PRB for treatment of arsenic iri
groundwater, finding the correct reactive media is a
major challenge. The reactive media must serve as
both a long-term sink for metals while at the same time
maintain permeability and hydraulic connectivity
between the contaminant plume and the reactive
treatment zone (Lien and Wilkin, 2005). In the past, ZVI
has proven an effective reactive media for arsenic in
groundwater.

Although ZVI is more commonly used to treat metals
and halogenated organic solvents, in the past six
years, a few studies have focused on using ZVI for
arsenic removal because ZVI has a high arsenic
removal capacity. Arsenic removal mechanisms by
ZVI include sorption onto corrosion products, co-
precipitation with iron sulfides and green rust (class of
iron oxide compounds), and precipitation as arsenic
sulfides. However, this technology is ultimately limited
because of the initial removal capacity and any
additional capacity that may come about after iron
metal corrodes in water (Lien and Wilkin, 2005).
Arsenic removal is a two-step reaction including the
initial rapid removal of arsenite followed by a slower
removal process that involves formation of smaller
capacity of ZVI is estimated to be 7.5 mg arsenic/g iron

Figure 2: Construction of the PRB trench at the
East Helena site.

Photo courtesy of Rick Wilkin, EPA

amounts of arsenate. The overall removal
(Lien and Wilkin, 2005).

A trench measuring 30 feet long, 46 feet deep and 6 feet wide was constructed perpendicular to the
plume. The trench was filled with 175 tons of ZVI and coarse bedding sand (U.S. EPA, 2005). On site,
the PRB is located just west of the slag pile, and situated down gradient about 600 feet from the
contaminant source.

Performance of System

Using data from a network of monitoring wells, including over two dozen wells within the trench, the
first round of monitoring data was collected in June 2005. Preliminary evaluation of the system
indicates that arsenic concentrations as high as 20 mg/L are reduced to below 0.010 mg/L within the
barrier. Once construction impacts on the treatment system subside and the normal ground water
flow is re-established, researchers expect reductions in the arsenic concentrations downstream from
the PRB (U.S. EPA, 2005). At present, it is too early to determine if the treatment is successful as there
are still many uncertainties. Full-scale implementation of the treatment system will be determined
after two years of evaluating the success of the pilot system.

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Lessons Learned

A pilot-scale PRB was constructed at the East Helena site in the spring of 2005. Prior to installation, the
unique hydrogeology of the site and the composition of the aquifer materials created some doubt as
to whether installation of the PRB was possible at all. The challenging hydrogeology came from the
presence of a few boulders in the subsurface. Large excavation equipment was brought in to
remove the boulders.

In constructing PRBs, consideration must be given to the nature of the groundwater flow rate and the
contaminant concentration. In this case, the barrier was designed to involve wider dimensions to
account for the high arsenic concentrations and flow rate.

In addition, the biopolymer slurry used
to hold the trench open was a success.

Although it is still too early to determine
the success of the system, the
researchers are hopeful the PRB will be
able to control the arsenic plume and
off-site migration. Ultimately, treatment
of the arsenic contamination must
involve source control and the PRB can
only serve as part of the remedy.

Currently, source control at the site
includes pump and treat,
isolation/containment, and in situ
treatment while additional plume
control includes pump and treat, air
sparging, and monitored natural
attenuation. By itself, the PRB cannot
control the high arsenic concentration
and groundwater flow rates.

Cost

For the existing pilot-scale PRB system, Region VIII estimates a construction cost of $325,000 (U.S. EPA,
2005). There are no additional operation and maintenance costs associated with the PRB.

Key Dates

(U.S. EPA 1999, 2005)

1888

Smelter operations begin at East Helena.

1899

ASARCO purchases the smelter from the Helena
and Livingston Lead Smelting Company.

1969

Environmental investigations begin at the site.

1984

East Helena Smelter site is listed on the NPL.

2001

East Helena ASARCO Incorporated Smelter placed
in "indefinite closed status."

2003

NRMRL conducted batch and column studies on
simulated ground water to assess the effectiveness
of ZVI for arsenic remediation.

2005

Installation of the pilot-scale PRB is completed in
five days.

A two-year evaluation begins on the PRB to
determine long-term success of reducing arsenic
concentrations.

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EPA Contacts

Linda Jacobson

Remedial Project Manager

U.S. Environmental Protection Agency Region VIII

Phone: (303) 312-6503

Email: Jacobson.linda@epa.gov

Rick Wilkin

Project Manager

U.S. Environmental Protection Agency
National Risk Management Research Laboratory
Office of Research and Development
Phone: (580) 436-8874
Email: wilkin.rick@epa.gov

References

U.S. EPA. 1999. Five-Year Review East Helena Supertund Site. URL:
http://www.epa.gov/superfund/sites/fivevear/f99-08003.pdf.

U.S. EPA. 2005. "Zero-Valent Iron PRB Application Expands to Arsenic Removal." Technology News and Trends.
URL: http://clu-in.ora/products/newsltrs/tnandt/view.cfm?issue=1105.cfm#1.

Lien, H-L and Wilkin, R.T. 2005. "High-level arsenite removal from groundwater by zero-valent iron."
Chemosphere. 59(3): 377-86.

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