NERL Research Abstract

EPA's National Exposure Research Laboratory
GPRA Goal 1 - Clean Air
APM # 443

Significant Research Findings

Atmospheric Chemistry of
Secondary Organic Aerosol Formation

Research The overall objective of this research is to determine the key chemical and
Approach physical processes that control the yield and chemical composition of the

secondary organic aerosol (SOA) component of particulate matter (PM2 5) from
atmospheric transformations of aromatic compounds, biogenic hydrocarbons,
and atmospherically relevant mixtures including synthetic automobile exhaust.
The SOA yield is the amount of organic aerosol produced per unit hydrocarbon
reacted—a critical parameter needed to develop cost-effective control strategies
for SOA formation. To generate this information, a smog chamber system was
developed for simulating SOA formation under near-ambient conditions. The
smog chamber was used to irradiate selected hydrocarbons in the presence of
nitrogen oxides to assess the impact of environmental parameters such as
relative humidity on the yield and chemical composition of SOA. The
hydrocarbon systems investigated to date include toluene,/^-xylene, 1,3,5-
trimethylbenzene, and synthetic automobile exhaust.

Results of the laboratory study clearly demonstrated that aromatic compounds
emitted into the atmosphere contribute to SOA formation through atmospheric
transformation to form oxidation products that are partially absorbed into the
organic films on pre-existing PM2 5. The SOA yields were found to be strongly
influenced by the total mass of organic compounds present on the aerosol, but
were not affected significantly by typical daytime relative humidity.
Furthermore, the laboratory results demonstrated that SOA compounds from
aromatic compounds are far less effective in taking up liquid water that
contributes to regional haze than sulfate and nitrate compounds commonly
found in PM2 5. The SOA chemical composition studies, which represent the
first investigation of this type, are consistent with the formation of multi-
functional oxygenated compounds. Finally, it was demonstrated that as much
as 75% of the SOA from synthetic automobile exhaust could be explained by
the aromatic content of the exhaust. These results and others obtained in the
study will serve as the foundation for building a chemical mechanism to be
used in an air quality model to predict the contribution of SOA formation to

Results
and

Implications

National Exposure Research Laboratory - September 2000


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ambient PM2 5 levels. These predictions will be used to target specific sources
of SOA for emission reductions.

Research The PM chemistry laboratory program was conducted by a team of NERL staff

Collaboration scientists along with support from ManTech Environmental Technology, Inc.

*tu1l1. . This research has been presented at several conferences and in the following
Publications	. , ,	.

articles and manuscripts.

Kleindienst, T.E., Smith, D.F., Li, W., Edney, E.O., Driscoll, D.J., Speer, R.E., Weathers, W.S.
Secondary organic aerosol formation from the oxidation of aromatic hydrocarbons in
the presence of dry submicron ammonium sulfate aerosol. Atmospheric Environment
33: 3669-3681, 1999.

Edney, E.O., Driscoll, D.J., Speer, R.E., Weathers, W.S., Kleindienst, T.E., Li, W., Smith, D.F.
Impact of aerosol liquid water on secondary aerosol yields of irradiated
toluene/propylene/NOx/ (NH4)2S04/air mixtures. Atmospheric Environment 34: 3907-
3919, 2000.

Edney, E.O., Driscoll, D.J., Weathers, W.S., Kleindienst, T.E., Conver, T.S., Mclver, C.D., Li,
W. Formation of polyketones in irradiated toluene/propylene/NOx/air mixtures.
Aerosol Science & Technology. Submitted.

Kleindienst, T.E., Li, W., Edney, E.O., Driscoll, D.J., Speer, R.E., Weathers, W.S., Tejada.
Secondary organic aerosol formation from the irradiation of simulated automobile
exhaust. Journal of Air & Waste Management Association. Submitted.

Although this research has led to a significant improvement in the
understanding of the SOA formation from aromatic compounds, additional
research is required to investigation other significant sources of SOA including
biogenic hydrocarbons. Experiments similar to those conducted for aromatic
compounds are underway for biogenic hydrocarbons. Laboratory studies are
planned to assess the impact of the organic composition of pre-existing PM2 5
on the SOA yields of aromatic and biogenic compounds. Furthermore, during
the summer of 2000, ambient PM2 5 samples will be collected and analyzed for
the presence of multifunctional oxygenates.

Questions and inquiries on NERL's PM chemistry research can be directed to:

Edward O. Edney, Ph.D.

U.S. Environmental Protection Agency

National Exposure Research Laboratory (MD-84)

Research Triangle Park, NC 27711

Phone: (919)541-3905

E-mail: edney.edward@epa.gov

Future
Research

National Exposure Research Laboratory - September 2000


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