Final

2013 Salt Chuck Mine
Superfund Site
Field Data Report
Prince of Wales Island, Alaska

Prepared for

U.S. Environmental Protection Agency

EPA Region 10

* £* %
USB J

February 2014

CH2HJ1HILL®

1100 112th Avenue NE, Suite 500
Bellevue, WA 98004


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Contents

Section Page
Acronyms and Abbreviations	vii

1	Introduction	1-1

1.1	Background Information	1-1

1.1.1	Upland Area	1-1

1.1.2	Marine Area	1-2

1.2	Purpose of Investigation	1-2

1.3	Data Quality Objectives and Sampling Design	1-2

1.4	Report Organization	1-4

2	Field Activities	2-1

2.1	Surface Sediment Investigations	2-1

2.1.1	Summary of Sampling Activities	2-1

2.1.2	Field Observations and Measurements	2-2

2.1.3	Deviations from QAPP	2-2

2.2	Marine Tailings Investigation	2-3

2.2.1	Summary of Sampling Activities	2-3

2.2.2	Field Observations and Measurements	2-6

2.2.3	Deviations from QAPP	2-6

2.3	Upland Tailings Investigation	2-7

2.3.1	Summary of Tailings Delineation and Sampling Activities	2-7

2.3.2	Field Observations and Measurements	2-7

2.3.3	Deviations from QAPP	2-7

2.4	Porewater	2-7

2.4.1	Summary of Sampling Activities	2-8

2.4.2	Field Observations and Parameter Measurements	2-9

2.4.3	Deviations from QAPP	2-9

2.5	Surface Water	2-10

2.5.1	Summary of Sampling Activities	2-10

2.5.2	Field Observations and Parameter Measurements	2-11

2.5.3	Deviations from QAPP	2-11

2.6	Marine Biota	2-12

2.6.1	Summary of Sampling Activities	2-12

2.6.2	Field Observations and Measurements	2-13

2.6.3	Deviations from QAPP	2-13

2.7	Groundwater	2-13

2.7.1	Summary of Sampling Activities	2-13

2.7.2	Field Observations and Parameter Measurements	2-14

2.7.3	Deviations from QAPP	2-14

2.8	Quality Assurance Activities	2-14

2.8.1	Equipment Calibration	2-14

2.8.2	Field Documentation	2-15

2.8.3	Quality Control Samples	2-15

2.9	Equipment Decontamination	2-15

2.10	Containment and Disposal of Investigation-Derived Wastes	2-16

2.11	Sample Tracking and Shipping	2-16

2.11.1	Sample Designation	2-16

2.11.2	Sample Management and Tracking	2-17

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CONTENTS, CONTINUED

Section	Page

3	Analytical Data Quality	3-1

3.1	Data Validation	3-1

3.2	Data Management	3-1

3.3	Data Usability Assessment	3-2

4	Analytical Results	4-1

4.1	Surface Sediment	4-1

4.2	Sediment Borings	4-2

4.3	Upland Tailings	4-2

4.4	Porewater	4-2

4.5	Surface Water	4-3

4.6	Crab Tissue	4-3

4.7	2012 Bivalve Tissue Arsenic Speciation	4-3

4.8	Groundwater	4-3

5	References	5-1

Appendices

A	Field Forms and Boring Logs

B	Site Photographs

C	Deviation from the Field Sampling Plan

D	Chains of Custody Forms

E	Data Validation Reports

F	Data Quality Assessment Report

G	Technical Review of 2013 Bioassay Testing Conducted for Salt Chuck Mine Project

H	Arsenic Speciation Results for 2012 Bivalve Samples

Tables

1-1	2013 Field Investigation Chronology

2-1	Surface Marine Sediment Sample Information
2-2	Surface Marine Sediment Analyses

2-3	Short-Core and Test Pit Sample Information - Marine Sediment Core Investigation

2-4	Deep-Core Sample Information - Marine Sediment Core Investigation

2-5	Marine Sediment Core and Test Pit Analyses

2-6	Short-Core and Test Pit Sample Information - Upland Tailings Investigation

2-7	Upland Short-Core and Test Pit Sample Analyses

2-8	Marine Porewater Sample Information

2-9	Marine Porewater Analyses

2-10	Surface Water Sample Information


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CONTENTS, CONTINUED

Section	Page

2-11 Surface Water Analyses

2-12 Marine Biota Sample Information

2-13 Marine Biota Analyses

2-14 Groundwater Sample Information

2-15 Groundwater Analyses

2-16 Field Blank Samples

2-17 Field Blank Analyses

2-18	MS/MSD Samples

3-1	Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Surface
Sediment Samples

3-2 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Marine
Sediment Core and Test Pit Samples

3-3 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Modified SPLP
Sediment Samples

3-4 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Upland Core
and Test Pit Samples

3-5 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Porewater
Samples

3-6 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Surface Water
Samples

3-7 Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Crab Tissue
Samples

3-8	Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Groundwater
Samples

4-1	Surface Sediment Sample Results
4-2 Sediment Toxicity Bioassay Results
4-3 Agronomic Sediment Sample Results

4-4 Marine Sediment Core and Test Pit Sample Results - May 2013

4-5 Marine Sediment Core and Test Pit Sample Results - August 2013

4-6 Marine Sediment Core and Test Pit Sample Results - Modified SPLP Metals Analysis

4-7 Upland Core and Test Pit Sample Results

4-8 Porewater Sample Results

4-9 Surface Water Sample Results

4-10 Crab Tissue Sample Results

4-11 Groundwater Sample Results

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CONTENTS, CONTINUED

Section	Page

Figures

1-1	Site Location Map

2-1	2013 Surface Sediment and Sediment Toxicity Sample Locations
2-2 2013 Agronomic Surface Sediment Sample Locations

2-3 2013 Sediment Core and Test Pit Locations

2-4 2013 Upland Tailings Sample and Delineation Locations

2-5 2013 Porewater Sample Locations

2-6 2013 Surface Water Sample Locations

2-7 2013 Marine Biota Sample Locations

2-8 2013 Groundwater Sample Locations

VI

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Acronyms and Abbreviations

Hg/L

micrograms per liter

AVS

acid volatile sulfide

CLP

Contract Laboratory Program

cm

centimeter

DO

dissolved oxygen

DQO

data quality objective

DRO

diesel-range organic

EPA

U.S. Environmental Protection Agency

ERL

effects range low

ERM

effects range median

FD

field duplicate

Forest Service

U.S. Forest Service

FS

feasibility study

GPS

global positioning system

L/min

liters per minute

MDL

method detection limit

MEL

Manchester Environmental Laboratory

MHHW

Mean higher high water

mg/kg

milligrams per kilogram

mL

milliliter

MS/MSD

matrix spike/matrix spike duplicate

NAD83

North American Datum 1983

NAVD88

North American Vertical Datum 1988

NTCRA

non-time-critical removal action

PAH

polycyclic aromatic hydrocarbon

PPE

personal protective equipment

PVC

polyvinyl chloride

QAPP

Quality Assurance Project Plan

QC

Quality Control

Rl

remedial investigation

RRO

residual-range organic

RSCC

Regional Sample Control Coordinator

RSL

regional screening level

Site

Salt Chuck Mine Superfund Site

SEM

simultaneously extracted metals

SPLP

Synthetic Precipitation Leaching Procedure

TAL

target analyte list

TCL

target compound list

TNF

Tongass National Forest

UTM

Universal Transverse Mercator

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VII


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SECTION 1

Introduction

This report provides a summary of the sampling and analytical programs conducted in May and August 2013
at the Salt Chuck Mine Superfund Site (Salt Chuck Mine Site or Site) on Prince of Wales Island in the Tongass
National Forest, Alaska. The intent of this report is to provide an overview of results in relation to the data
quality objectives (DQOs) for the 2013 investigations. The 2013 data will be combined with data from
previous investigations to complete evaluations associated with the remedial investigation (Rl) and
feasibility study (FS) being conducted for the site by the U.S. Environmental Protection Agency (EPA).
Therefore, only limited interpretation of results is provided in this report. A more complete assessment of
the Rl results will be provided in the Rl Report in 2014.

Work presented in this report was conducted in accordance with the 2013 Remedial Investigation Quality
Assurance Project Plan (QAPP) dated May 14, 2013 (CH2M HILL, 2013a), and with the Modification to
Tailings Delineation Activities - Salt Chuck Mine technical memorandum (Modification Memo) dated
August 1, 2013 (CH2M HILL, 2013b).

1.1 Background Information

The Salt Chuck Mine Site is located approximately 4Vz miles south-southwest of Thorne Bay, Alaska, at the
northern end of Kasaan Bay, on Prince of Wales Island. The mine is located in the Tongass National Forest,
Outer Ketchikan County, within Township 72 South, Range 84 East, Sections 16 and 17, Copper River
Meridian, Alaska. Salt Chuck, from which the mine takes its name, is a shallow, restricted waterbody
bordering the mine site to the south and forms the northernmost arm of Kasaan Bay (Figure 1-1). The Salt
Chuck Mine Site is accessible by water or by road, the last Vz mile of which is newly constructed. A locked
gate restricts road access to the lower part of the Site. Thorne Bay (population 471) is the closest year-round
population, and is accessible from the Site by road. The Organized Village of Kasaan (Kasaan, population 49)
is the nearest community by water and is located 9 miles southeast of the Site on the eastern side of Kasaan
Bay.

The Site consists of an upland area comprising the mine, waste rock piles, and remnants of the former mill
and support facilities (Upland Area), and the intertidal area adjacent to the former mill and other portions of
Salt Chuck affected by releases from the former mill (Marine Area), as described below.

1.1.1 Upland Area

The Upland Area is managed by the U.S. Forest Service (Forest Service) and covers approximately 45 acres.
The mine is uphill and approximately Vz mile north of the former mill. The mine area includes the glory hole
and adits where ore was removed, a former railway for transporting ore to the former mill, a variety of
dilapidated structures, and numerous waste rock piles. The mine area is relatively steep and heavily
vegetated. The former mill was the subject of a non-time-critical removal action (NTCRA) conducted by the
Forest Service in 2011. Prior to the NTCRA, the mill site contained a large roller mill, workshops, bunkhouses,
aboveground storage tanks reportedly used to store fuel and possibly coal tar for use as a floatation agent in
ore processing, fuel drum caches, and other support facilities for the mining camp. The former mill was
constructed over and surrounded by tailings and waste rock piles. The structures, tanks, and fuel drum
cache were removed and exposed contaminated soil, tailings, and waste rocks were excavated to bedrock
during the NTCRA. The excavated areas were then backfilled, graded, covered and revegetated (North Wind
Group [North Wind], 2012).

The Upland Area is drained by a small unnamed stream (hereafter "Unnamed Stream") that originates
northeast of the site at Power Lake, cuts across the mine site, and exits the forest near the former mill site
into Salt Chuck. The Upland Area also includes a large tailings pond that formerly occupied the area where

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SECTION 1 INTRODUCTION

Unnamed Stream currently exits the forest and enters Salt Chuck. At high tide, seawater from Salt Chuck
inundates Unnamed Stream.

1.1.2	Marine Area

The Marine Area includes both the intertidal and subtidal zones of Salt Chuck. The intertidal zone is
generally defined by the area below mean higher high water (MHHW) at an elevation of 11.91 feet North
American Vertical Datum 1988 (NAVD88), and above mean lower low tide (minus [-] 3.84 feet NAVD88), but
also includes the elevated tailings pile adjacent to the former mill. Overall, the intertidal zone encompasses
approximately 97 acres south and east of the former mill, where tailings and/or other facility-related
releases may have occurred. The intertidal zone adjacent to the former mill includes the elevated spit and
beach composed of tailings from the mill. Accumulations of tailings are also evident where the tailings pond
was formerly located, along the shoreline of Unnamed Stream upstream of the tailings spit, and in the cove
on the east side of the former barge slip. The intertidal tailings are not contained in a manner that prevents
contaminants within the tailings from migrating into the waters of Salt Chuck. The tailings, outlying
sediment, and intertidal portion of Unnamed Stream and Lake Ellen Creek are exposed at low tide. Flow in
the intertidal zone is dominated by Lake Ellen Creek, which flows west to east past the former mill, then
turns sharply south and west to follow the western side of an unnamed island (hereafter "Unnamed Island")
in the middle of Salt Chuck. The intertidal zone is covered by seaweed, gravel, mollusk shell fragments, and
beach grasses, but areas south and east of the former mill site consist of mud flats mixed with tailings, with
little vegetation.

The subtidal zone occupies the remainder of Salt Chuck. While areas of the zone near the shore may be
exposed during low tide, the majority of the subtidal zone is permanently submerged.

1.1.3	Reference Area

Browns Bay is located approximately 2 miles from the Salt Chuck Mine Site, and is considered an area
unimpacted by mining activities. For the purposes of this investigation, Browns Bay is a used as a reference
area and is considered representative of marine background conditions in the area.

1.2	Purpose of Investigation

The purpose of the 2013 investigation was to collect additional sampling data for tailings in the Upland and
Marine Areas, sediment, surface water, porewater, groundwater, and marine biota at the Salt Chuck Mine
Site to support the RI/FS. The data collected in 2013 will be used in conjunction with data collected during
previous investigations to characterize the nature and extent of contamination associated with releases
from the Site, assess potential risks to human health and the environment, and develop remedial
alternatives.

1.3	Data Quality Objectives and Sampling Design

The systematic planning process and data quality objectives (DQOs) for the 2013 investigation were
documented in Appendix A of the QAPP. The overall objectives and associated problem statements are
listed below:

• Objective 1 - Refine Evaluation of Nature and Extent of Contamination Within, or Releases to, the
Intertidal Area and Assess Risk:

-	Problem Statement 1-1: The extent of contamination along the distal (southern) segment of the
thalweg of Lake Ellen Creek on the west side of Unnamed Island is not adequately defined to
characterize potential risks to human health or the environment and/or to support a remedial
decision.

-	Problem Statement 1-2: Existing Rl data suggest that seeps are releasing soluble copper and other
metal discharges into surface water within Lake Ellen Creek during low tide, potentially impacting

1-2

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SECTION 1 INTRODUCTION

aquatic life. The extent to which these releases originate from tailings present within the intertidal
areas near the former mill area and/or from upland groundwater sources is not adequately defined
to characterize potential risks to human health or the environment and/or to support a remedial
decision.

-	Problem Statement 1-3: Existing Rl data suggest that tailings in the cove east of the barge slip may
exhibit anomalous toxicity, bioaccumulation, and/or leaching characteristics. The importance or
impact of these differences is not fully understood to characterize potential risks to human health or
the environment and/or to support a remedial decision.

-	Problem Statement 1-4: Total chromium has been detected in tailings/sediment and may be mine-
related. However, it is unknown what portion of the total chromium occurs in the more toxic
hexavalent form. This is needed to adequately characterize potential risks to human health or the
environment and/or to support a remedial decision.

-	Problem Statement 1-5: The Organized Village of Kasaan has expressed concern about
contamination within the intertidal lands, particularly with subsistence concerns. Potential impacts
on the beneficial use of crab and shrimp harvesting are of particular concern, both from past
releases and from potential releases from any proposed remedial actions. This is needed to
adequately characterize potential risks to human health or the environment and/or to support a
remedial decision.

-	Problem Statement 1-6: Existing Rl data indicate that groundwater in the former mill area is affected
by releases of petroleum and by metals in tailings. The extent of groundwater contamination is
unknown and contaminant concentrations appear to have changed over time. More information is
needed to assess trends and understand potential discharges to nearby surface water in the
intertidal areas. This is needed to adequately characterize potential risks to the environment and/or
to support a remedial decision.

• Objective 2 - Sample Collection for Evaluation of Remedial Alternatives:

-	Problem Statement 2-1: The thickness and vertical profile of tailings within the intertidal areas are
uncertain. This information is needed to adequately support evaluation of remedial alternatives by
providing volume estimates, and information regarding waste classification and disposal methods.

-	Problem Statement 2-2: Existing Rl data indicate that surface sediment from the peninsula that is
circumvented by Lake Ellen Creek (at low tide) within Salt Chuck contains relatively lower
concentrations of mine-related metals. However, it is unknown whether this is due to historic
deposition of cleaner sediment from Lake Ellen Creek onto deeper contamination, or whether the
peninsula itself represents an erosional feature. If deeper contaminated sediment exists at this
location, the potential for future mobilization into the bay should be evaluated.

-	Problem Statement 2-3: The thickness and vertical and lateral profile of tailings within the tailing
piles along Unnamed Stream are uncertain. This information is needed to adequately support
evaluation of remedial alternatives by providing volume estimates, and information regarding waste
classification and disposal methods.

-	Problem Statement 2-4: The agronomic characteristics of intertidal sediment are unknown. This
information is needed to support evaluation of remedial alternatives.

The 2013 field effort was designed to fill data gaps associated with the problem statements listed above and
the elements of the sampling design are described generally in Section 2.2.4 and specifically in Section A. 7 of
the QAPP. However, work activities performed in May and August 2013 included some modifications to the
sampling designs described in the QAPP. The planned field investigation elements, including sample counts
and target analytical suites, are summarized and compared to actual sample counts in Table 1-1.

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SECTION 1 INTRODUCTION

In general, the field work consisted of the following activities:

•	Collected surface sediment (0 to 0.5 foot) samples in the intertidal and subtidal zones of Salt Chuck west
of Unnamed Island (Lake Ellen Creek thalweg-associated samples) and from background locations in
Browns Bay. Collected porewater samples from intertidal sediment and tailings in Salt Chuck and from
background locations in Browns Bay by burying an aquarium airstone under the sediment and applying
suction with a hand-operated syringe. Collected porewater samples from drive-points installed in
intertidal sediments and tailings in Salt Chuck at locations downgradient of the former mill and collapsed
buildings.

•	Collected grab surface water samples from intertidal tailings areas within Unnamed Creek, Lake Ellen
Creek, seepage inputs to Lake Ellen Creek, intertidal areas of Salt Chuck, and background locations in
Browns Bay. Collected time-series grab samples of surface water hourly during the period bounded by
two high tide cycles at a single location close to the confluence of the barge area seep and Lake Ellen
Creek downstream from tailings areas.

•	Collected crab at sample locations in Salt Chuck and from background locations in Browns Bay. As
described in Section 2.6, no shrimp were collected for analysis because only a few specimens were
caught despite extensive deployment of traps in Salt Chuck and Browns Bay. Collected continuous
sediment cores from numerous borings in the Marine Area for visual documentation of tailings
thickness. Sediment samples were collected for chemical analysis at regular intervals (0 to 0.5 foot, 0.5
to 1.0 foot, 1.0 to 2.0 feet, and so on) in a subset of the locations. The majority of the borings in the
intertidal area were advanced using a hand-held portable short-coring device. Shallow test pits were
also used to characterize sediment and tailings in portions of the area where short cores could not be
advanced. A direct-push drilling rig was to be used in the upland tailings piles and in the tailings spit area
where tailings were expected to be thicker (up to 15 feet). The short hand-held core sampling program
occurred in May 2013 and the sampling design for the direct-push core program, implemented in August
2013, was modified based on conditions encountered during the May event. As described in Section 2.2,
the modified direct-push sampling program included new and relocated direct-push tailings borings,
additional borings to delineate the extent of petroleum and coal tar in sediment near the barge slip, and
sampling of native sediment beneath the tailings.

•	Documented the lateral extent of visible upland tailings deposits in the large tailings pond where
Unnamed Stream exits the forest by hand-digging holes with a shovel (test pits) and by coring with a
hand-held portable short coring device. Upland tailings and soil samples were collected for chemical
analysis at a subset of the locations.

•	Collected groundwater samples from four existing monitoring wells (sampled in May 2013) and the
replacement monitoring well that was installed by the Forest Service in June 2013 (sampled in August
2013). As described in Section 2.6, the proposed two new monitoring wells were not installed.

The timeline for sample collection during the May and August events is detailed in Table 1-2.

1.4 Report Organization

The remaining sections of this document describe the field collection effort, sampling procedures used
during the May and August 2013 sampling events, and associated analytical results. Section 2 describes field
sampling activities by medium, including field observations and deviations or modifications from the QAPP.
Section 3 describes sample analyses, data validation, and data quality assessment results, and presents the
2013 analytical data by medium. Section 4 summarizes the completion of the 2013 investigations by
documenting attainment of the DQOs outlined in the QAPP and Modification Memo. Cited references are
listed in Section 5.

1-4

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SECTION 1 INTRODUCTION

Supporting information is provided in eight appendices:

•	Appendix A. Field Forms and Boring Logs

•	Appendix B. Field Sampling Photographs

•	Appendix C. Deviation from the Field Sampling Plan

•	Appendix D. Chains-of-Custody Forms

•	Appendix E. Data Validation Reports

•	Appendix F. Data Quality Assessment Report

•	Appendix G. Technical Review of 2013 Bioassay Testing Conducted for Salt Chuck Mine Project

•	Appendix H. Arsenic Speciation Results for 2012 Bivalve Samples

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SECTION 2

Field Activities

The 2013 field investigation was conducted in two parts. The initial sampling effort occurred between
May 22 and May 30, 2013, and consisted of all of the activities listed in Section 1, except for the direct-push
sediment core sampling in the Marine Area and groundwater monitoring of the replacement monitoring
well in the Upland Area, which occurred between August 26 and August 30, 2013. Because the focus of the
2013 sampling effort was to characterize conditions in the intertidal area, both sampling events were
scheduled to coincide with periods of prolonged low tides during daylight hours. The timeline for sample
collection during both events is detailed in Table 1-2.

2.1 Surface Sediment Investigations

This section summarizes the field methods and procedures that were used to collect surface sediment
samples for characterization of sediment conditions in Salt Chuck and Browns Bay, and for characterization
of agronomic properties in sediments in the vicinity of the tailings spit and near Lake Ellen Creek. The
agronomic properties were needed to support remedial alternative development for the feasibility study.
For sediment characterization, samples were analyzed for chemistry and sediment toxicity using two
bioassays (survival and growth using polychaetes Neanthes arenaceodentata, and survival and development
using the blue mussel Mytilus galloprovincialis).1 Surface sediment sample information is listed in Table 2-1
and sample locations are depicted on Figure 2-1 (Salt Chuck and Browns Bay sediment and bioassay
samples) and Figure 2-2 (Salt Chuck agronomic samples).

All surface sediment samples were collected from the sediment surface (0 to 0.5 foot). Samples were
obtained from locations exposed during low tide or were accessed by wading at low tide or by boat,
depending onsite access and the depth of water at the sample location. Samples obtained from locations
exposed during low tide were collected using a stainless-steel sampling spoon. Underwater samples were
collected using a Petite Ponar grab sampler.

2.1.1 Summary of Sampling Activities

Sample collection was conducted in accordance with sampling procedures detailed in the QAPP. The
procedures for sampling exposed surface sediment using a stainless-steel spoon consisted of the following:

1.	Locate the geographic position using global positioning system (GPS) and record this and other
parameters identified in the Surface Sediment Sample Collection Sheet. Photograph and describe each
location.

2.	Line a stainless-steel bowl with aluminum foil and arrange sample containers and sampling equipment
and exercise caution not to step on, or otherwise contaminate, the sample surface.

3.	Label each sample container properly and fill out appropriate chain-of-custody information.

4.	Using a new stainless-steel spoon, remove the organic layer on the surface of the selected sampling
point, if present. Insert the spoon into the sediment at the selected sampling point and slowly remove
the sample.

5.	Slowly decant excess water, if appropriate and necessary.

6.	For locations requiring acid volatile sulfide and simultaneously extracted metals (AVS/SEM) analysis,
transfer the unmixed sample into the appropriate container using a stainless-steel spoon. The AVS/SEM

-|

The results of exploratory testing in 2011 confirmed that polychaetes and bivalves are suitable bioassay test organisms for detecting toxicity in
sediments at the Site. Amphipods did not appear to be adequately sensitive enough for the types of contaminants found at the Site.

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SECTION 2 FIELD ACTIVITIES

container should be filled with sediment leaving no air space. Wipe outside of containers with paper
towel and place in iced cooler.

7.	Deposit the sample remaining after collection of undisturbed AVS/SEM aliquot into a stainless-steel
bowl lined with clean foil. Collect additional volume as needed for bioassay sample locations, field
duplicate (FD), and matrix spike/matrix spike duplicate (MS/MSD). Remove large organisms and pieces
of debris and record sample description on the Surface Sediment Sample Collection Sheet.

8.	Homogenize the sample in the foil-lined bowl using a stainless-steel spoon (or equivalent device) prior
to placement into sample containers. Transfer the sample into the appropriate containers using a
stainless-steel spoon (or equivalent device). Wipe outside of containers with paper towel and place in
iced cooler.

9.	Carefully remove used foil from the stainless-steel bowl and dispose of the used stainless-steel spoon
and foil in a garbage bag prior to moving to the next location to avoid need for decontamination.

The procedures for collecting underwater surface sediment samples were similar to those above, except
that a stainless-steel Petite Ponar grab sampler was used to bring the sediment to the surface. A Ponar grab
sampler has a jaw-type mechanism that is tripped from above in order to close the jaws and collect the
sample. The sampler is lowered slowly through the water to the sediment with the jaws in the open
position. As the sampler is retrieved, the jaws close and the isolated sediment is brought to the surface,
where overlying water is decanted before collecting the sediment sample.

Surface sediment samples were stored on ice under custody control before they were packaged and shipped
to the laboratories for analysis.

2.1.2	Field Observations and Measurements

Field observations recorded at the time of collection at each sample location are presented in Table 2-1.
Table 2-2 lists the target analytes and laboratories conducting the analyses for each sample. Copies of the
sampling records are provided in Appendix A-l. Photographs of the sampling effort are included in
Appendix B.

2.1.3	Deviations from QAPP

Deviations to the planned surface sediment sampling program included the following:

•	Sample volumes for bioassay, AVS/SEM, and grain size were mistakenly collected at locations 2013SC-
SS-139 and SS-141 and submitted for analysis. Samples were discarded by the laboratories without
analysis.

•	The FD for target analyte list (TAL) metals and mercury planned for 2013SC-SS-140 was moved to
2013SC-SS-141 because insufficient volume was recovered at 2013SC-SS-140.

•	The MS/MSD scheduled for 2013SC-SS-141 was not collected due to sufficient number of MS/MSD
volumes already submitted for sediment.

•	The Location ID for one background location was misidentified as 2013SC-SB-510 rather than
2013SC-SS-510.

•	Nine primary samples and one FD were collected for agronomic analysis, rather than the 10 primary
samples that were planned. In addition, all agronomic samples were analyzed for TAL metals and
mercury.

Copies of the alteration forms are provided in Appendix C.

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SECTION 2 FIELD ACTIVITIES

2.2 Marine Tailings Investigation

This section summarizes the field methods and procedures that were used to investigate the thickness of
tailings and evaluate the vertical distribution of contaminants in sediment in the intertidal portion of the
Site. Sediment short-core and test pit sample information for May 2013 are listed on Table 2-3 and sediment
deep-core sample information for August 2013 are listed on Table 2-4. Sediment core and test pit locations
are depicted on Figure 2-3. Two types of borings and hand-dug test pits were used to assess tailings
thickness and collect tailings and sediment samples. A generator-powered reciprocating hammer was used
to collect short (2 to 3 feet) sediment cores. An AMS Power Probe 9500, operated by North Wind Group,
was used to collect deeper (up to 20 feet) sediment cores. All sample locations were accessed by foot during
low tide.

2.2.1 Summary of Sampling Activities

Sample collection was conducted in accordance with sampling procedures detailed in the QAPP and in the
Technical Memorandum on Modifications to Tailings Delineation Activities (CH2M HILL, 2013c). The
procedures for sampling using the short-core, test-pit, and deep-core methods are described below. A video
showing the short-core sampling method is provided in Appendix B, Attachment Bl-13.

2.2.1.1 Short-Core Samples

The following procedure was used to advance borings and obtain each short-core sample:

1.	The geographic position for the core was located using GPS and recorded along with other parameters
identified in the Intertidal Tailing Core Log - Short Core. Photograph and describe each location.

2.	Set up the generator and reciprocating hammer.

3.	Attach the vibration head to a clean Lexan tube and insert a core catcher in tube.

4.	Raise the tube into a vertical position. Connect the reciprocating hammer to vibration head. Check
plumbness of the tube and turn on the hammer motor. Maintain light tension on the assembly to keep
the tube in place and allow it to slowly penetrate the sediments. Advance the tube until a depth of 3.5
feet or refusal is reached. Record the depth of penetration on the core log.

5.	Turn off the motor when the target penetration depth is reached or refusal occurs. Slowly withdraw the
core from the tailings.

6.	Mark the outside of the tube with the Location ID and indicate the top and bottom of the core. Tape
caps on the ends of the core.

7.	Use the same procedures to advance two to three additional cores in close proximity (within 5 feet) to
the original boring location to collect additional volume for an FD or MS/MSD sample.

8.	Transport the labeled core to a clean foil-covered table in the field laboratory. Extract the core from the
tube by tapping the core with a rubber mallet or by inserting a rod to push the core out. Examine the
core for lithology, presence of tailings, and other parameters identified in the core log. Describe tailings
according to color, grain size, and other distinguishing characteristics.

9.	Depending on location, collect samples of the core following lithologic description. Sample collection
procedures are listed below:

-	Arrange sample containers and sampling equipment.

-	Label each sample container properly and fill out Tailings Core Sample Information Sheet and
appropriate chain-of-custody information for each sample.

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-	Using a new stainless-steel spoon (or equivalent device), partition the core into separate intervals -
up to four intervals were sampled in each core: 0 to 0.5 foot, 0.5 to 1 foot, 1 to 2 feet, 2 to 3 feet.
Record Sample IDs for each interval and intervals with FDs and MS/MSDs on the core log.

-	Place the full length of each interval into separate foil-lined aluminum bowls or foil covered areas. If
an FD or MS/MSD was collected, add that same interval from the additional cores obtained at the
same location to the foil-lined bowl/area. Homogenize each sample interval (and additional volumes
for FDs and MS/MSDs, as appropriate) using a stainless-steel spoon or gloved hand (change gloves
between sample intervals) prior to placement into sample containers. Transfer the sample into the
appropriate containers using a stainless-steel spoon or gloved hand. Wipe the outside of the
containers with a paper towel and place in an iced cooler.

-	Dispose of the used foil and used stainless-steel spoons in a garbage bag to avoid need for
decontamination.

10. Decontaminate all reusable sampling equipment that contacts potentially contaminated sediment or
tailings between sample locations.2

Short-core sediment samples were stored on ice under custody control before they were packaged and

shipped to the laboratories for analysis.

2.2.1.2 Test Pit Samples

The following procedure was used to dig shallow test pits and obtain sediment samples in areas where short

cores could not be obtained due to the presence of dense or compacted material:

1.	Locate the geographic position for the test pit using GPS and record this and other parameters identified
in the Intertidal Tailing Core Log - Short Core. Photograph and describe the location.

2.	Use a decontaminated shovel to dig a test pit to expose subsurface sediment and tailings for
examination by the Field Geologist. Test pits were dug to depths of 2 to 3 feet; test pit size varied based
on the types of materials encountered. Larger pits were needed for wet or loose material; smaller pits
were used for dry and dense material.

3.	Examine the wall of the test pit for lithology, presence of tailings, and other parameters identified in the
core log. Describe the tailings according to color, grain size, and other distinguishing characteristics.

4.	Depending on location, collect samples of subsurface sediment or tailings following lithologic
description. Sample collection procedures are listed below:

-	Arrange sample containers and sampling equipment.

-	Label each sample container properly and fill out Tailings Core Sample Information Sheet and
appropriate chain-of-custody information for each sample.

-	Using a new stainless-steel spoon (or equivalent device), collect samples from separate intervals in
the test pit - up to four intervals were sampled in each pit: 0 to 0.5 foot, 0.5 to 1 foot, 1 to 2 feet, 2
to 3 feet. Record Sample IDs for each interval and intervals with FDs and MS/MSDs on the core log.

-	Place each sample interval (and additional volumes for FDs and MS/MSDs, as appropriate) in a
gallon-size resealable plastic bag for transport to the field laboratory. Homogenize the sample
interval on foil using a stainless-steel spoon or gloved hand (change gloves between sample
intervals) prior to placement into sample containers. Transfer the sample into the appropriate
containers using a stainless-steel spoon or gloved hand. Wipe the outside of the containers with a
paper towel and place in an iced cooler.

Reusable sampling equipment was limited to a few Lexan tubes, which were reused between tailings thickness only core locations.

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-	Dispose of used foil and used stainless-steel spoons in a garbage bag to avoid need for
decontamination.

5.	Allow the test pit to collapse or backfill to the surface.

6.	Decontaminate all reusable sampling equipment that contacts potentially contaminated sediment or
tailings between sample locations.3

Test pit sediment samples were stored on ice under custody control before they were packaged and shipped

to the laboratories for analysis.

2.2.1.3 Deep Cores

The following procedure was used to advance and obtain sediment samples from deep cores using a direct-

push rig:

1.	Locate the geographic position for the core using GPS and record this and other parameters identified in
the Direct Push Soil Boring Log. Photograph and describe each location.

2.	Stage the direct-push rig over the desired drilling location. Lower a sampling tool with polyvinyl chloride
(PVC) liner down the inside probe drive string to the end of the cutting shoe. Hydraulically push the
probe drive string and sampler down through the sample interval to obtain an undisturbed sample of
tailings/sediment. Once the probe drive string and sampler are fully advanced, withdraw the sampler
and center rods from the probe drive string and remove the recovered core in the PVC liner from the
sampler. After the tailings/sediment core is removed, lower another sampler with a PVC liner down the
inside of the probe drive string to the end of the cutting shoe to conduct continuous-core sampling to
the maximum depth of the tailings deposit.

3.	After core recovery, extract the PVC liner encasing the tailings/sediment core from the sample sheath
and cut open the PVC liner to expose the core. Examine the core for lithology, presence of tailings, and
other parameters identified in the log.

4.	Use the same procedures to advance two to three additional cores in close proximity (within 5 feet) to
the original boring location to collect additional volume for an FD or MS/MSD sample.

5.	Depending on location, collect samples of the core following lithologic description. Sample collection
procedures are listed below:

-	Arrange sample containers and sampling equipment.

-	Label each sample container properly and fill out Tailings Core Sample Information Sheet and
appropriate chain-of-custody information for each sample.

-	Using a new stainless-steel spoon (or equivalent device), partition the core into separate intervals -
up to 16 intervals were sampled in each core: 0 to 0.5 foot, 0.5 to 1 foot, 1 to 2 feet, 2 to 3 feet, and
so forth. Record Sample IDs for each interval and intervals with FDs and MS/MSDs on the log.

-	Place the full length of each interval into separate foil-lined aluminum bowls or foil covered areas. If
an FD or MS/MSD was collected, add that same interval from the additional cores obtained at the
same location to the foil-lined bowl/area. Homogenize each sample interval (and additional volumes
for FDs and MS/MSDs, as appropriate) using a stainless-steel spoon or gloved hand (change gloves
between sample intervals) prior to placement into sample containers. Transfer the sample into the
appropriate containers using a stainless-steel spoon or gloved hand. Wipe the outside of the
containers with a paper towel and place the container in an iced cooler.

D

Reusable sampling equipment was limited to a few Lexan tubes, which were reused between tailings thickness only core locations.

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Dispose of the used foil and used stainless-steel spoons in a garbage bag to avoid need for
decontamination.

Deep-core sediment samples were stored on ice under custody control before they were packaged and
shipped to the laboratories for analysis.

2.2.2	Field Observations and Measurements

The lithology, tailings thickness, and other field observations for each core and test pit are presented in
Tables 2-3 and 2-4. Table 2-5 lists the target analytes and laboratories conducting the analyses for each
sample. Deep-core tailings delineation samples were analyzed for metals. Deep-core PAH delineation boring
samples were analyzed for PAHs. The August 2013 samples were not analyzed for the other target analytical
suites from May because adequate data for these analytes were obtained from the short-core samples
collected in May 2013. Copies of the logs for cores and test pits are provided in Appendix A-2. Photographs
of the core and test pit sampling effort are provided in Appendix B.

2.2.3	Deviations from QAPP

Deviations to the May sediment coring and subsurface sediment sampling program include:

•	Hand-held coring equipment was not capable of penetrating very fine-grained, dense, clayey tailings,
which tended to occur at depths of 1.5 to 2 feet. Therefore, the majority of sample cores were restricted
to the upper 2 feet of tailings (only 6 cores reached depths greater than 2 feet). This resulted in the
collection of fewer samples than planned for laboratory analysis and reductions in the number of FD and
MS/MSD sample volumes.

•	Hand-dug test pits, rather than cores, were used to characterize subsurface conditions in key locations
where coring was unsuccessful.

•	Thirteen short cores/test pits and 10 tailings thickness short cores/test pits were added around the
margins of tailings deposits.

•	Some tailings thickness cores were converted to sample cores based on conditions encountered in the
field (presence or absence of tailings, creosote-like odor, grain size differences) or if shallow refusal was
encountered at a nearby sample core location.

•	Some scheduled FD locations and depths were moved to other locations/depths where greater sample
volume was available. Certain scheduled FDs were not collected because of the reduced number of
samples.

•	The number of short-core tailings thickness only locations (no samples) was reduced from 64 to 24
because of the depth limitation of short-core equipment and the proximity of other sampled core
locations.

•	The number of locations where Synthetic Precipitation Leaching Procedure (SPLP) metals analysis was
conducted increased from 7 to 12 locations because the appearance and texture of tailings in several
locations were different than those observed in borings where SPLP analysis was conducted.

•	One of the deep-core locations designated for chromium VI analysis (SB-019) in the QAPP was
eliminated from the modified deep-core program so the number of chromium VI samples was reduced
from 8 to 7.

Deviations to the August sediment deep coring and subsurface sampling program include:

•	One planned direct-push sediment core south of the tailings spit near Unnamed Stream (SB-302) was
not performed due to time constraints.

•	The full extent of petroleum- and coal-tar-impacted sediment in the vicinity of the barge slip could not
be determined due to time constraints.

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• Duplicate Contract Laboratory Program (CLP) sample identification numbers were mistakenly assigned
to two groups of samples submitted for polycyclic aromatic hydrocarbon (PAH) analysis at an EPA CLP
laboratory (Sample SB-322-02 was assigned the same CLP number as SB-313-04 and Sample SB-322-03
was assigned the same CLP number as SB-316-06). Although each sample bottle had a different Scribe
sample identification number, as well as different sampling dates and times, the CLP did not recognize
that the bottles were for separate samples and reported the results for only one sample in the group of
duplicated CLP sample IDs. The samples were discarded before the error was recognized. Consequently,
there is some uncertainty about which of the duplicate samples were analyzed for PAHs and which
samples have missing PAH results.

Copies of the alteration forms are provided in Appendix C.

2.3	Upland Tailings Investigation

This section summarizes the field methods and procedures that were used to investigate the extent and
thickness of tailings in upland portions of the Site that were formerly occupied by the tailings pond. Visual
observations of shallow test pits and short cores at 40 locations were used to delineate the extent of the
tailings. Samples were collected for laboratory analysis from 8 locations to confirm observed conditions (up
to 3 depth intervals were collected at each location). Visual observations are listed with sample information
in Table 2-6 and investigation locations are depicted on Figure 2-4. The upland tailings investigation was
conducted in May 2013.

2.3.1	Summary of Tailings Delineation and Sampling Activities

Tailings delineation was accomplished by walking through the upland portion of the Site near the former
tailings pond and digging test pits with a shovel or by driving Lexan tubes by hand into the upper foot of soil.
The soil was then examined for the presence of tailings (greenish gray sand, silt, or clay). The GPS
coordinates and observations at each location were recorded in field notes and observation logs. Soil
samples were collected using the same sampling procedures described in Section 2.2 for the intertidal
sediment. The soil samples were stored on ice under custody control before they were packaged and
shipped to the laboratories for analysis.

2.3.2	Field Observations and Measurements

The field observations for each upland core and test pit are presented in Table 2-6. Copies of the field forms
and core logs are provided in Appendix A-3.4 Photographs of the core and test pit sampling effort are
provided in Appendix B.

Table 2-7 lists the target analytes and laboratories conducting the analyses for each sample.

2.3.3	Deviations from QAPP

Deviations to the upland tailings investigation described in the QAPP included the use of a hand-driven
Lexan tube in addition to hand-dug test pits to conduct the visual observation of tailings investigation and to
collect samples for laboratory analysis.

2.4	Porewater

This section summarizes the field methods and procedures that were used to collect porewater samples in
the intertidal portion of Salt Chuck near the former mill and in the reference area at Browns Bay. Porewater
sample information is presented in Table 2-8 and sample locations are depicted on Figure 2-5. Two types of
devices were used to collect porewater samples, ceramic airstones and drive-point wells. The sampling
devices were installed during low tide and before sediment sampling or other intrusive activities occurred in
the vicinity of the former mill. Samples from buried airstones were collected during low tide 3 days (4 tide

4 Note that intertidal and deep-core field sampling forms and logs were used to record upland tailings observations.

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cycles) after airstone installation, when porewater was expected to be less than 2 feet below the surface.
Drive-point samples were collected 3 to 4 days after installation.

2.4.1 Summary of Sampling Activities

Sample collection was conducted in accordance with sampling procedures detailed in the QAPP. The
procedures for sampling using airstones and drive-point wells are described below.

2.4.1.1 Airstone Sample Collection

Airstone porewater samples were collected by suction through a cylindrically shaped, aquarium airstone
(e.g., 10 to 15 centimeters [cm] long and 1.5 cm wide) placed vertically in the sediment.

The procedure for airstone installation and sample collection is described below:

1.	Locate the geographic position for the sample location using GPS and enter coordinates on the
Porewater Collection Field Form.

2.	Use a pre-marked wood or plastic dowel of about 1 to VA inch diameter to make a hole by pushing or
tapping into the sediment to a depth of 2 feet below the sediment surface (adjust hole depths as
necessary based on field conditions). Place the airstone and connected tubing (pre-marked to 2 feet) in
the hole.5 After installation, compress the sediment surrounding the tube and hole by foot. Determine
airstone depth by measuring the remaining tubing above the sediment surface. Record depth on the
sample collection sheet. Clamp the end of the tube to prevent entry of sea water. Decontaminate the
hole-making device between holes.

3.	Allow installed airstones to equilibrate for 3 days (about 4 tide cycles) prior to sampling.

4.	Collect samples as follows:6

-	Arrange sample containers and sampling equipment and exercise caution not to step on or
otherwise disturb the sample tubing. Remove clamp on tubing.

-	Label each sample container (with preservative) properly, and fill out appropriate chain-of-custody
information.

-	Using a disposable hand-held 50 milliliter (mL) Luer-lock syringe, extract water by slow suction from
the buried airstone. Discard the first draw of 50 mL, then fill syringe again. Connect 0.45 micron
filter to syringe and transfer filtered water to pre-preserved sample containers (place acid in sample
container before transferring water to bottle). Continue collection until sufficient sample volume
(including volumes for FD and MS/MSD, if applicable) is collected. Discard filter(s).

-	Measure salinity of porewater using refractometer.7

-	Record sample description and salinity measurements on Porewater Collection Field Form.

-	Remove and discard airstone and tubing.

Airstone porewater samples were stored on ice under custody control before they were packaged and
shipped to the laboratories for analysis.

5 Installation of sampling probes occurred when the tide level was about 2 feet lower than the sediment surface to allow the subsurface water level
to be well below the positioning elevation of the sampling device (preventing the installation hole from prematurely collapsing due to overly wet
subsurface conditions).

® Porewater sampling proceeded from the higher to lower elevation direction as the tide fell.

^ It was not feasible to measure other water quality parameters using a Horiba water quality meter due to the limited volume of recovered water.

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2.4.1.2 Drive-point Well Sample Collection

Temporary drive point wells were used to collect porewater samples near the shoreline at the former mill.
The drive points consisted of a 2-inch diameter PVC slotted well screen (with PVC well point) that was
manually driven approximately 3 to 4 feet into the sediment/tailings using a slide hammer. A 0.75-inch-
diameter PVC well screen with pre-pack filter (and end cap) was then installed inside the outer screen.

1.	Locate the geographic position for the sample location using GPS and enter coordinates on the
Porewater Collection Field Form.

2.	Measure the water level within the drive-point well using a water level indicator. Record the
measurement on the Porewater Collection Field Form.

3.	Install an appropriate length of sample intake tubing in the drive-point well and connect tubing to the
battery-operated peristaltic pump. Set the tubing to discharge to a purge bucket.

4.	Use low-flow (less than 0.5 liters per minute [L/min]) methods to purge one full volume from the drive-
point well. Retain purge water and treat with activated charcoal prior to discharge onsite.

5.	Measure water quality parameters (conductivity, temperature, dissolved oxygen (DO), pH, salinity, and
turbidity) using a water quality meter and the procedures in the manufacturer's manual after one well
volume had been purged. Measure salinity using a refractometer to be consistent with measurement
equipment used at the airstone locations. Record these measurements and other observations on the
Porewater Collection Field Form.

6.	Drive-point well porewater samples were collected as follows:

-	Arrange sample containers.

-	Label each sample container (with preservative) properly, and fill out appropriate chain-of-custody
information.

-	Fill the sample containers. Continue collection until sufficient sample volume (including volumes for
FD and MS/MSD, if applicable) is collected. Collect sample aliquots for dissolved metals analysis into
unpreserved containers prior to filtering. Filter these aliquots using 0.45 micron filters attached to
syringes prior to transfer into pre-preserved sample containers.

-	Remove and discard sample tubing.

-	Decontaminate water level and water quality meter probes.

7.	Remove and discard the drive-point well.

Drive-point well porewater samples were stored on ice under custody control before they were packaged
and shipped to the laboratories for analysis.

2.4.2	Field Observations and Parameter Measurements

Information about each porewater sample is presented in Table 2-8. Table 2-9 lists the target analytes and
laboratories conducting the analyses for each sample. Copies of the sampling records are provided in
Appendix A-4. Photographs of the porewater sampling effort are provided in Appendix B.

2.4.3	Deviations from QAPP

Deviations to the planned porewater sampling program included the following:

•	2013SC-PW-001 (planned drive-point) was not installed due to proximity of other drive-points in the
vicinity of the barge and tailings spit.

•	Seven porewater sample locations were moved due to the presence of rocks and pilings, or to optimize
the sample location in an area of potential interest.

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•	2013SC-PW-016 was changed from a drive-point to an airstone location due to presence of rocks in the
area, and the target analytes for the location were reduced to dissolved TAL metals and dissolved
mercury only due to the limited volume of recoverable porewater.

•	The FD planned for 2013SC-PW092 was moved to 2013SC-PW-091 because of volume recovery issues.

•	Extra volumes for MS/MSD were not collected at 2013SC-PW-088 and 2013SC-PW-100 because
sufficient MS/MSD volumes for metals analysis had already been collected at other locations.

•	Three porewater samples were added at Browns Bay to characterize reference area porewater
conditions.

•	All installed porewater airstones were allowed to equilibrate for 3 days prior to sampling, rather than
the 2 days specified in the QAPP.

•	A field meter was not used to measure field parameters at airstone locations. Salinity was measured
using a hand-held refractometer.

•	Sample volumes submitted for laboratory analysis were 100 mL rather than 1,000 mL.

•	Dissolved mercury was analyzed for at all porewater sample locations.

Copies of the alteration forms are provided in Appendix C.

2.5 Surface Water

This section summarizes the field methods and procedures that were used to collect surface water samples
in the intertidal portion of Salt Chuck near the former mill and in the reference area at Browns Bay. Surface
water sample information is presented in Table 2-10 and sample locations are depicted on Figure 2-6.

The majority of samples were single grab samples collected during low tide at locations accessed by foot.
However, hourly grab samples were collected at one location (SW-108) to characterize temporal changes
during both low and higher tide levels. The higher tide samples (when foot access was precluded) were
obtained using a peristaltic pump connected to tubing secured at the sampling point during low tide.

2.5.1 Summary of Sampling Activities

The procedure for sample collection is described below:

1.	Locate the geographic position for the sample location using GPS and enter coordinates on the Surface
Water Collection Field Form.

2.	When possible, measure the water depth at the time of sampling using a tape measure and record the
measurement on the Surface Water Collection Field Form.

3.	Exercise caution not to disturb the sediment at or upcurrent of the sample location.

4.	Samples were collected as follows:8

-	Arrange sample containers and sampling equipment.

-	Label each sample container (with preservative) properly, and fill out appropriate chain-of-custody
information.

-	For one-time grab samples, with minimum surface disturbance, submerge an unpreserved sample
bottle (at least 500 mL) with the mouth of the container facing upstream and allow sample stream
to flow gently into the bottle. Obtain FDs and MS/MSDs from the same sampling equipment as the
parent samples.

o

Surface water sampling proceeded from downstream to upstream.

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-	For hourly grab samples, stake the end of a sampling tubing several inches above the bottom of Lake
Ellen Creek at Location SW-108 and run the other end to the bank and clamp off. At the appropriate
time, sample with a peristaltic pump and draw the initial flush of water and discard, then collect the
hourly grab sample. Begin hourly sampling at least 4 hours before low tide and continue with an
equal number of grabs after low tide, according to the tide table for that day (May 26, 2013).

-	For sample aliquots analyzed for dissolved metals concentrations, transfer the sample to the pre-
preserved sample container using a hand-held syringe and a 0.45 micron filter. Use a new filter for
each water sample location. Transfer aliquots analyzed for total metals and PAHs directly to sample
bottles (no filtration).

-	After sample aliquots are collected, measure field parameters (conductivity, pH, temperature,
salinity, and DO) using the water quality meter and the procedures in the manufacturer's manual.
Record sample description and water quality readings on the Surface Water Collection Field Form.
Decontaminate the water quality meter.

Surface water samples were stored on ice under custody control before they were packaged and shipped to

the laboratories for analysis.

2.5.2	Field Observations and Measurements

Information about each surface water sample is presented in Table 2-10. Table 2-11 lists the target analytes

and laboratories conducting the analyses for each sample. Copies of the sampling records are provided in

Appendix A-5. Photographs of the surface water sampling effort are provided in Appendix B.

2.5.3	Deviations from QAPP

Deviations to the planned surface water sampling program included the following:

•	All samples for laboratory analysis were collected as planned. However, locations scheduled for PAH
analysis were sampled on two dates (May 25 and May 26, 2013) due to concerns about holding times
caused by EPA furlough dates.

•	The time-series grab samples scheduled for location SW-105 were moved to SW-108 based on
conditions observed in the field (closer to the confluence of the barge area seep and Lake Ellen Creek).

•	The sample identification numbers for several time-series samples contain a typographical error (2013CS
instead of 2013SC).

•	The FD scheduled at background location 2013SC-SW-501 was moved to background location 2013SC-
SW-509.

•	The second sample location (2013SC-SW-601) for water to be used in the SPLP analyses of sediments
from cores was not obtained due to sample volume/shipment concerns.

•	Initial results for all surface water surface water samples from the Site and background locations had
method detection limits (MDLs) well above targeted levels, resulting in non-detects for most metals of
interest (for example, copper). The elevated MDLs were the result of the laboratory's standard practice
of diluting marine water samples by 20 to 40 times to protect their instrumentation. A sample plan
alteration form for reanalysis of the surface water samples was prepared and approved by EPA (see
Appendix C). Then the remaining volume from each sample was transferred to another laboratory with
the capability of analyzing marine water samples without dilution (ALS Environmental) and the analyses
were re-run successfully.

Copies of the alteration forms are provided in Appendix C.

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2.6 Marine Biota

This section summarizes the field methods and procedures that were used to collect marine biota samples in
the intertidal and subtidal portions of Salt Chuck and in the reference area at Browns Bay. Both crab and
shrimp samples were scheduled for collection. However, no shrimp were collected for analysis because only
a few specimens were caught despite extensive deployment of traps in Salt Chuck and Browns Bay. Only
Dungeness crab samples were collected (no other crab species were kept). Biota sample information
(number of individuals, weight, size, etc.) is presented in Table 2-12 and sample locations are depicted on
Figure 2-7.

2.6.1 Summary of Sampling Activities

The procedure for crab sample collection is described below:

1.	Set shellfish traps in accordance with standard sport fishery practice and baiting. The standard soak
time, defined as the time the pots are set until the time the pots are retrieved, was approximately
24 hours. Record GPS coordinates for trap on Shellfish Collection Field Form.

2.	After an appropriate time, retrieve traps and sort catches. Retain shellfish for tissue analyses equivalent
to the legal size and condition taken in the sport fishery. Male Dungeness crab less than the minimum
legal size (6% inches in shoulder width) and all female Dungeness crab were immediately returned to the
water unharmed, with some exceptions.9 Three crabs were retained for tissue compositing at each
successful sample location.

3.	Photograph catch and record species on Shellfish Collection Field Form.

4.	Place all crabs from a given location in a single plastic bucket with overlying water. Label the outside of
buckets and fill out appropriate chain-of-custody information.

5.	Once in port, freeze samples until tissue resection and processing can be done within one week.

6.	Remove sample buckets of whole crabs from the freezer at the start of each resection day, and thaw
just enough to allow processing.

7.	Dry and line the tissue processing area with clean paper cloth. Carefully rinse excess sediment off
outside of shellfish by running under tap water, and let drain for one minute. Record the sex of the crab
by inspection of the telson width, and the carapace width of each crab to the nearest millimeter. Record
carapace length of each shrimp to the nearest millimeter (1 mm) using a ruler. Carapace length is
defined as behind the eye stalk to the beginning of the abdomen. Measure total weight of the whole
crab to the nearest gram (1 g) using a bench scale. Record on the Shellfish Collection Field Form.

8.	For each sample location, pre-tare or weigh the empty tissue sample container on the scale.

9.	Using clean latex or nitrile gloves, remove muscle tissue from the claws and largest sections of legs.

Break individual crab leg sections from the body or cut from the body using pre-cleaned stainless-steel
scissors. Slit each section of the leg down the flat edge using scissors. Once muscle tissue is exposed, use
stainless-steel forceps or spatula to remove the muscle tissue from all the claw and leg cavities.

10.	For each species and location, collect the appropriate amount of tissue and place samples inside the
pre-labeled, pre-tared jar and weigh the sample container with the composite tissue sample on the scale
to ensure the minimum sample volume is met. Based on the total amount of tissue required for analysis,
and the number of individual animals per composite, keep approximately the same mass of tissue from
each animal until the total requirement is attained.

Q

In some cases, crabs below the legal size limit were kept, in accordance with a Fish Resource Permit CF-13-097 obtained from Alaska Department of
Fish and Game.

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11. Place the sample (inside the container) in a plastic bag, label, and place in the freezer.

Crab samples were stored frozen under custody control before they were packaged and shipped to the
laboratory for analysis.

2.6.2	Field Observations and Measurements

Information about each crab sample is presented in Table 2-12. Table 2-13 lists the target analytes and
laboratories conducting the analyses for each sample. Copies of the sampling records are provided in
Appendix A-6. Photographs of the crab sampling effort are provided in Appendix B.

2.6.3	Deviations from QAPP

Deviations to the planned marine biota sampling program included the following:

•	No shrimp were collected for analysis because only a few specimens were caught despite extensive
deployment of traps in Salt Chuck and Browns Bay.

•	The FD scheduled at Biota-138 (crab) was moved to Biota-148 (crab) due to larger volume of available
tissue.

•	No crabs were present at the planned location for Biota-130, so the sample location was moved about
100 feet to the west where the intertidal portion of Lake Ellen Creek channel was more pronounced.

•	No crabs were present at the planned location for Biota-107, so the sample location was moved to the
southwestern side of Unnamed Island.

•	The planned FD scheduled at Biota-150 (crab) was not collected because sufficient duplicates had
already been collected for biota.

•	Methylmercury was mistakenly included as a target analyte in several QAPP tables. This analyte should
not have been included because the risk assessment will assume that all mercury detected in tissue is
methylmercury.

Copies of the alteration forms are provided in Appendix C.

2.7 Groundwater

This section summarizes the field methods and procedures applicable to collection of groundwater samples
from monitoring wells at the Site. Monitoring wells GW-01 through GW-06 were installed by the Forest
Service as part of the NTCRA for the former mill. Monitoring well GW-05 was found to be damaged in 2012
and was abandoned by the Forest Service in early 2013. The well was replaced by the Forest Service in June
2013 and is renamed GW-05r. Groundwater sample information is presented in Table 2-14 and sample
locations are depicted on Figure 2-8.

2.7.1 Summary of Sampling Activities

The following procedures were used to collect groundwater samples:

1.	Locate the geographic position for the well using GPS and enter the coordinates on the Groundwater
Collection Field Form.

2.	Measure the water level within the well using a water level indicator. Record the measurement on the
Groundwater Collection Field Form.

3.	Install an appropriate length of sample intake tubing in the well and connect the tubing to the battery-
operated peristaltic pump. Set up the tubing to discharge to a purge bucket.

4.	Use low-flow (less than 0.5 L/min) methods to purge the well until field parameters (DO, oxygen
reduction potential, conductivity, pH, turbidity, and temperature) stabilize, until three well casing
volumes are purged, or until the well purges dry. Measure field parameters using a water quality meter

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SECTION 2 FIELD ACTIVITIES

and the procedures in the manufacturer's manual. Retain purge water and treat with activated charcoal
prior to discharge onsite.

5. Groundwater samples were collected as follows:

- Arrange sample containers.

Label each sample container (with preservative) properly, and fill out appropriate chain-of-custody
information.

Fill the sample containers. Continue collection until sufficient sample volume (including volumes for
FD and MS/MSD, if applicable) is collected. Collect sample aliquots for dissolved metals analysis into
unpreserved containers prior to filtering. Filter these aliquots using 0.45 micron filters attached to
syringes prior to transfer into pre-preserved sample containers.

Remove and discard sample tubing.

Record any odor, color, sheen, or other parameters identified in the Groundwater Sampling Sheet.
Decontaminate water level and water quality meter probes.

Groundwater samples were stored on ice under custody control before they were packaged and shipped to
the laboratories for analysis..

2.7.2	Field Observations and Parameter Measurements

Information about each groundwater sample is presented in Table 2-14. Table 2-15 lists the target analytes
and laboratories conducting the analyses for each sample. Copies of the sampling records are provided in
Appendix A-7. Photographs of the sampling effort are provided in Appendix B.

2.7.3	Deviations from QAPP

Deviations to the planned groundwater sampling program for May 2013, as previously described in CH2M
HILL (2013c), included the following:

•	Wells GW-05r, GW-07, and GW-08 were not sampled in May 2013 because the proposed wells were not
installed.

•	EPA decided not to install proposed wells GW-07 and GW-08 due to the proximity of existing monitoring
wells and intertidal area drive-point samples. The replacement well for GW-05 (GW-05r) was installed in
June 2013 and sampled in August 2013.

•	Well GW-02 was not sampled for diesel-range organics/residual-range organics (DRO/RRO) and PAH
analyses because of inadequate recovery (less than 1 liter per 2 hours).

•	Well GW-06 was sampled but the samples were discarded due to the presence of thick colloidal material
in the samples (including the filtered sample). The presence of this material suggests that the bentonite
seal has failed and the well is not suitable for sample collection.

Copies of the alteration forms are provided in Appendix C.

2.8 Quality Assurance Activities

This section describes the quality assurance activities conducted in support of the May and August 2013
field activities.

2.8.1 Equipment Calibration

Equipment calibration was conducted in accordance with the QAPP. Instruments used in the field included
the GPS and the multi-parameter water quality meter. The GPS was calibrated and/or checked by the
manufacturer and did not require any adjustment or calibration in the field. The multi-parameter water

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SECTION 2 FIELD ACTIVITIES

quality meter was calibrated each day prior to use and was verified at the end of each day's use. Any
instrument deviations from the calibration solution were recorded in the field notebook.

2.8.2	Field Documentation

All sampling and associated activities were documented on activity-specific field logs. Copies of the
completed logs are included in Appendix A. Daily field activities were documented through journal entries in
bound field logbooks, which were dedicated to each field team. All pertinent information about sampling
activities, site conditions, field methods used, general observations, and other pertinent technical
information were recorded in the field logbook.

2.8.3	Quality Control Samples

Quality Control (QC) samples were collected or prepared to assess the overall quality of the May and August
2013 project data. Field QC samples include FDs, equipment rinsate blanks, filter blanks, and temperature
blanks. Laboratory QC samples included method blanks and MS/MSDs.

2.8.3.1	Blind Field Duplicate Samples

Blind FD samples were collected to assess the homogeneity of samples collected in the field and the
precision of the sampling process. The FDs were prepared by collecting two aliquots of sample from the
sampling equipment and submitting them for analysis as separate samples. Note that aliquots of
sediment/tailings samples were homogenized prior to splitting into separate samples. FDs were collected
from at least 10 percent of the sampling locations, as listed in the media-specific tables described above.

2.8.3.2	Equipment Rinsate Blank

Equipment rinsate blanks are used to evaluate sampling device cleanliness and potential carryover of target
contaminants from equipment. Equipment rinsate blanks were collected from unused disposable sampling
equipment or, in the case of reusable sampling equipment, after decontamination of the equipment. The
rinsate blanks were created by pouring American Society of Testing and Materials Type II water (purchased
and certified from a commercial vendor) over or through the sampling device and collecting the rinsate in a
sample container for analysis. One equipment rinsate blank was collected for each type of disposable or
reusable sampling equipment used during the sampling event. Table 2-16 lists the associated equipment and
target analytes for each equipment rinsate blank.

2.8.3.3	Temperature Blanks

All coolers submitted to the laboratories contained a temperature blank.

2.8.3.4	Matrix Spike/Matrix Spike Duplicates Samples

MS/MSD analyses was performed in the laboratory to assess the accuracy of the analyses. These analyses
were performed according to the laboratory protocols at a frequency of once every 20 samples using extra
volumes of sample matrices collected in the field. The MS/MSD samples were designated as such on the
chain-of-custody form. Analyses were the same as those required by the parent sample. Individual sample
locations where MS/MSD volumes were collected and the total number of MS/MSD samples for each
sample group are listed in Table 2-17.

2.9 Equipment Decontamination

Sampling equipment decontamination was performed in accordance with the QAPP. Factory-wrapped
disposable equipment intended for one-time use was not decontaminated and was discarded after use.
Reusable equipment that came into contact with potentially contaminated samples was decontaminated
using the following procedure:

•	Prewash with site water.

•	Wash with solution of tap water and Alconox® soap and brush.

•	Rinse with site water.

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SECTION 2 FIELD ACTIVITIES

•	Rinse the brush with site water to remove any visible dirt.

•	Rewash with solution of tap water and Alconox® soap and brush.

•	Rinse with site water.

•	Double rinse with distilled water.

•	Repeat as necessary.

•	Cover (no contact) all decontaminated items with clean aluminum foil.

2.10	Containment and Disposal of Investigation-Derived
Wastes

Waste generated during fieldwork included personal protective equipment (PPE), disposable items (such as
stainless-steel spoons), excess sediment samples, and decontamination wash water. Disposal of these
wastes is described below:

•	All general refuse (such as PPE, gloves, paper towels, and plastic sheeting) that would not likely contain
hazardous material was disposed of as municipal waste.

•	Excess surface sediment or tailings, porewater, and surface water were left at the sampling locations
where they were collected.

•	Excess tailings or sediment from test pits and sediment cores were placed in and near the core or pit
location and tamped by foot to compact the sediment. Excess groundwater purge water was treated
using activated carbon prior to discharge onsite.

•	Equipment decontamination occurred in the exclusion zone within the intertidal area and all liquids and
solids were left onsite near the sampling locations where they were generated.

2.11	Sample Tracking and Shipping

This section describes the methods that were used to document data and sample collection during the 2013
investigation effort at the Salt Chuck Mine Site.

2.11.1 Sample Designation

A sample numbering scheme was developed that allows each sample to be uniquely identified and provides
a means of tracking the sample from collection through analysis. The numbering scheme indicates the
location and sample type and depth or species, if appropriate. The unique sample numbers were entered in
the field notebook, field tracking sheets, chain-of-custody forms, and other records documenting sampling
activities. The following sample number convention was used for normal and field duplicate samples:

Location Prefix - Medium - Location ID - Depth or Species

Explanation:

Location Prefix: 2013SC
Medium:	SW = surface water

PW = porewater

SS = surface sediment (for Lake Ellen Creek thalweg, Browns Bay, and
agronomic samples only)

BIOTA = crab

SB = boring (for short cores, test pits, and direct-push borings)

GW = groundwater
Location:	001 through 400 (Salt Chuck locations, three digits)

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SECTION 2 FIELD ACTIVITIES

Depth:
Biota:

500 through 550 (Browns Bay [reference] locations)
Depth below top of sediment (top of interval, two digits)
Crab

Location numbers were assigned by location. FDs were assigned numbers that match the parent sample,
except a "9" was inserted at the beginning of the location number. MS/MSDs were labeled with the same
Sample ID as the parent sample, with MS or MSD added at the end of the number.

Sample identification for the equipment blanks was as follows:

Location Prefix: 2013SC

Medium:	EB = equipment blank

Date:	Date of collection (month, date, year [8 digits])

2.11.2 Sample Management and Tracking

Chain-of-custody procedures were used to maintain and document sample collection and possession after
sample packaging. Scribe software was used for project data management and completing chain-of-custody
documentation. All Scribe project information, sample information, and documentation (labels/traffic
report-chain of custody) were completed according to the Region 10 Regional Sample Control Coordinator
(RSCC) sampling guidelines. A separate unique traffic report/chain of custody was created for each cooler
shipped, documenting the specific contents and location of the associated cooler. Copies of the traffic
report/chain of custody, Scribe XML (*.xml), and Excel (*.xls) were submitted to CLP and the RSCC in
accordance with the instructions for sample shipping and documentation per CLP/RSCC requirements. The
laboratory copy was sent to the CLP and subcontracted labs, while the regional copy was be sent to
Manchester Environmental Laboratory (MEL). Copies of the chains of custody are included in Appendix D.

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SECTION 3

Analytical Data Quality

Samples collected during the 2013 sampling event were packaged and shipped under chain-of-custody
protocol to the following laboratories for analysis:

•	A4 Scientific (metals and mercury)

•	KAP Technologies (PAHs)

•	CH2M HILL Applied Sciences Laboratory (AVS/SEM, DRO, RRO, bulk density, grain size)

•	MEL (hexavalent chromium, lipids, arsenic speciation, SPLP metals, total organic carbon). MEL also
performed an arsenic speciation analysis on archived (frozen) samples of bivalves collected in 2012.

•	Northwestern Aquatic Sciences (sediment toxicity bioassays)

•	A & L Western Agricultural Laboratories (agronomic sediment analyses)

•	ALS Environmental (marine surface water analyses)

For the most part, laboratory analyses and data reporting for each laboratory were consistent with the
procedures defined in the QAPP. However, two data quality issues were identified when the initial sediment
toxicity bioassay and marine surface water data were reported, as summarized below:

•	Bioassay - Initial bioassay results for two surface sediment samples from Salt Chuck (SS-140, and SS-9140
[FD for SS-140]) and from the background location (SS-510) showed unexpected bioassay responses for
the bivalve test. Further analysis at the laboratory identified relatively high levels of ammonia in these
samples, possibly representing a confounding influence on the test results. This may have occurred due
to inadvertent storage at elevated temperatures. Additional volumes of sediment for these samples that
were stored in refrigeration at A4 Scientific (metals laboratory) were transferred to Northwestern
Aquatic Sciences and the bioassays were re-run.

•	Surface water - Initial results for all surface water surface water samples from the Site and background
locations had method detection limits (MDLs) well above targeted levels, resulting in non-detects for
most metals of interest (for example, copper). The elevated MDLs were the result of the laboratory's
standard practice of diluting marine water samples by 20 to 40 times to protect their instrumentation. A
sample plan alteration form for reanalysis of the surface water samples was prepared and approved by
EPA (see Appendix C). Then the remaining volume from each sample was transferred to another
laboratory with the capability of analyzing marine water samples without dilution (ALS Environmental)
and the analyses were re-run successfully.

3.1	Data Validation

The analytical chemistry data packages were reviewed and validated according to the protocols identified in
the QAPP. Data from the EPA MEL laboratory were validated by the EPA Office of Environmental
Assessment. Chemistry data from other laboratories were validated by CH2M HILL. The validation reports
for each laboratory are provided in Appendix E. The Data Quality Assessment Report summarizing the
findings of the 2013 validation reports is provided in Appendix F. Sediment toxicity bioassay results were
also reviewed for technical quality and usability by CH2M HILL, as provided in Appendix G.

3.2	Data Management

Following validation, the data with assigned validation codes were then uploaded to the Site database
maintained by CH2M HILL. Sample location data, as determined in the field using GPS equipment and/or
relative position to known structures or features, were linked to the analytical data in the Site geographic

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SECTION 3 ANALYTICAL DATA QUALITY

information system database. The data were then reviewed for completeness (i.e., were all samples and
target analytes accounted for and did all samples have accurate locations?). Any discrepancies were
resolved through consultation with the field team, laboratory personnel, and the project chemist.

For the most part, the data received from the validators were uploaded to the CH2M HILL database without
modification. However, because analytical results for crab tissue samples were reported by the laboratory as
dry weight concentrations and the screening levels used to identify possible contaminants in tissue are
based on wet weight concentrations, the dry weight results for each sample were converted to wet weight
values using the measured moisture content of each specific sample according to the following formula:

Wet weight concentration = Dry weight concentration x (1 - percent moisture/100)

In addition, concentrations of low molecular weight PAHs and high molecular weight PAHs were calculated
for samples using the detected concentrations of individual PAH constituents, and these values were
entered as separate results for each sample. No other conversions or adjustments were made in the
database.

3.3 Data Usability Assessment

Data collected during the 2013 investigations were reviewed and validated in accordance with the QAPP.
Data validation findings are discussed in the Data Quality Assessment Report presented in Appendix F. The
results of the data quality review indicate that all data, as qualified, are usable for their intended purpose.
Also, all data associated with sediment toxicity bioassay testing were found to be of suitable quality and
acceptable for making management decisions (Appendix G).

The 2013 analytical data were evaluated for usability in the context of the DQOs for the overall Rl for the
Salt Chuck Mine Site. The first step in the evaluation process was a determination of whether data from
2013 were appropriate for use in evaluating the nature and extent of contamination and assessing risk.
Although target analyte and sample coverage are important, the key consideration in determining the
usability of the dataset was whether the MDLs for the 2013 sample results were adequate to detect the
target analytes at concentrations consistent with the screening levels for the Site; that is, whether the MDLs
were low enough to conclude that target analytes are not present at levels that might pose potential risk
(assuming the conservative exposure scenarios of the screening levels) if an analyte was not detected.

To accomplish the usability evaluations, data for each sample group were consolidated into summary
statistics tables that list the following for each analyte:

•	Number of samples analyzed

•	Number of detects

•	Frequency of detection

•	Minimum and maximum detected values

•	Minimum and maximum MDLs for non-detects

•	Screening level10

•	Number of detect results with concentrations greater than the screening level

•	Number of non-detect results with MDLs greater than the screening level (non-detect MDL
exceedances)

10

The screening levels are used only as means of characterizing the nature and extent of contamination; they are not intended to necessarily infer
the existence of unacceptable risk.

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SECTION 3 ANALYTICAL DATA QUALITY

These summaries are provided in Tables 3-1 through 3-8. Only analytes and media with screening levels are
listed in the tables. Full listings of analytical results by sample group are presented in Section 4 of this report.

Only two analytes (cobalt and silver) in the SPLP metals results for sediment boring samples and three
analytes (chromium, cobalt, and iron) in the total metals results for upland tailings samples had non-detect
MDLs in excess of their screening levels. The MDLs for these analytes were less than 10 times the screening
levels and most of these metals are not expected to influence the nature and extent of contamination or risk
assessment evaluations (note that the upland screening level used for chromium is based on the more toxic
hexavalent chromium form and all results for hexavalent chromium were non-detect). Therefore, these
results do not adversely affect the usability of the 2013 data and do not merit further evaluation.

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SECTION 4

Analytical Results

This section summarizes the 2013 results in the context of the primary DQOs for the 2013 field investigation.
The intent is not to provide detailed analysis and interpretation of data, but to provide a brief overview of
results in relation to the DQOs and screening levels identified in the QAPP to assess the completeness of the
dataset. Note that the screening levels are used only as means of characterizing the nature and extent of
contamination; they are not intended to necessarily infer the existence of unacceptable risk. The risk
assessment to be conducted as part of the Rl will provide site-specific estimates of cumulative risk intended
for management decision making.

The following summaries are supported by tables wherein the analytical results for each sample group are
compared to risk-based screening levels and other criteria that were identified in the QAPP. These tables are
organized by location, medium, and sample identification number. FD and normal results are presented as
separate samples. Sample results with detected exceedances of the listed screening level are indicated by
bold font; ND results with MDLs in excess of the screening levels are indicated by italics.

A variety of media and locations were sampled to complete the nature and extent of contamination
evaluations and assess potential risks. The sample groups included:

•	Surface sediment in or near the distal (southern) segment of the thalweg of Lake Ellen Creek on the west
side of Unnamed Island

•	Surface and subsurface tailings and sediment in the intertidal area south and east of the former mill

•	Porewater in the intertidal area south and east of the former mill

•	Marine surface water in Lake Ellen Creek, Unnamed Stream, Salt Chuck, and Browns Bay

•	Crab in Salt Chuck and Browns Bay

•	Upland tailings in the vicinity of the former tailings pond near the former mill

•	Groundwater in the vicinity of the former mill.

4.1 Surface Sediment

The analytical results for the surface sediment samples collected in Salt Chuck are presented in Table 4-1.
Concentrations of copper in eight of the nine thalweg-associated samples exceeded both the effects range
low (ERL) value (34 milligrams per kilogram [mg/kg]) and effects range median (ERM) value (270 mg/kg) for
copper. The ninth sample (SS-143) exceeded only the ERL value. Copper concentrations in most of the
surface sediment samples collected for agronomic purposes south of the tailings spit and on the west side of
Unnamed Stream (SS-181 through -189) were also above the ERL and ERM values. The Browns Bay sample
did not exceed either criterion. In addition, concentrations of cobalt, manganese, selenium, and vanadium in
several surface sediment samples exceeded their apparent effects threshold (AET) values, which are used as
screening levels for analytes without an ERL or ERM.

The sediment toxicity bioassay results for the surface sediment samples collected in Salt Chuck are
presented in Table 4-2. Of the three Salt Chuck sediment samples tested, the sample collected at SS-146 was
found to result in reduced polychaete growth (but not reduced survival) when compared to the control
sediment results; but this sediment sample was not statistically different when compared to the reference
area sediment (SS-510). Moreover, no toxicity to bivalves was seen at location SS-146. Therefore, the
toxicity result (reduced polychaete growth) at location SS-146 is considered questionable. The bivalve test
results at one station (SS-140) indicated significant toxicity (when compared to both control and reference
area sediments) where larval development was significantly reduced (but larval survival was not reduced).

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SECTION 4 ANALYTICAL RESULTS

The agronomic results for the surface sediment samples collected south of the tailings spit and on the west
side of Unnamed Stream are presented in Table 4-3. The mercury and metals data for the agronomic sample
locations are presented in Table 4-1.

4.2	Sediment Cores and Test Pits

The analytical results for tailings and sediment samples collected in the intertidal area south and east of the
former mill are provided in Tables 4-4 and 4-5 (May and August, respectively). Concentrations of copper in
most of the samples collected from locations and intervals where tailings were identified exceeded both the
ERL and ERM values. Copper concentrations in native gravel beneath tailings and in areas without visible
tailings were slightly above the ERL value and well below the ERM value. Concentrations of mercury in
excess of the ERL value (0.15 mg/kg) occurred in about 13 percent of the samples, but only five results were
above the ERM value (0.71 mg/kg). There is no apparent pattern to the mercury exceedances. Elevated
concentrations of arsenic, nickel, and zinc also occurred in several samples, but the reported concentrations
are only slightly above the ERL values and no pattern for the exceedances was identified. The concentration
of silver in one sample (SB-021, 0 to 0.5 feet) exceeded both the ERL and ERM. In addition, concentrations of
cobalt, manganese, selenium, and vanadium in several sediment samples exceeded their AET values, which
are used as screening levels for analytes without an ERL or ERM.

Modified SPLP metals analysis was conducted on 31 samples of tailings from the intertidal areas south and
east of the former mill. Sea water from Browns Bay (sample location SW-600 in Figure 2-6) was used to
conduct the leaching portion of the test.11 The SPLP metals results for the samples are compared to surface
water screening levels in Table 4-6. Concentrations of copper in SPLP leachate from 19 of the 31 samples
exceeded the screening level of 3.1 micrograms per liter (ng/L). The SPLP leachate with the highest copper
concentrations occurred in samples collected west of the former mill (SB-021, 472 ng/L) and barge slip (SB-
033, 121 ng/L) (see Figure 2-3). Scattered exceedances of the screening levels for cobalt, iron, manganese,
and zinc were also reported in the SPLP leachate samples.

Hexavalent chromium was not detected in any of the sediment samples analyzed for the metal. These
results will be used to better characterize the type of chromium present in sediment and soil at the Site and
assess its potential impacts on human health. This information will be presented in the upcoming Rl Report.

Although staining and petroleum odors were noted in several intertidal borings near the former mill and
barge slip, elevated PAH concentrations were only reported in a few samples collected at SB-306 and
SB-089, with all reported concentrations below their respective ERMs.

4.3	Upland Tailings

The analytical results for tailings samples collected in the Upland Area are presented in Table 4-7. The only
chemicals with concentrations that exceeded the regional screening levels (RSL) for residential soil were
chromium, cobalt, and iron. Chromium (reported as total chromium) was detected in 8 soil samples and all
reported concentrations exceeded the EPA residential RSL for chromium (0.29 mg/kg), which is based on the
more toxic hexavalent form of the metal. However, hexavalent chromium was not detected in any of the
three upland tailings samples analyzed for the metal. The cobalt and iron exceedances occur in a single
sample (SB-179, 0 to 0.5 feet).

4.4	Porewater

The analytical results for porewater samples collected in the intertidal area south and east of the former mill
and Browns Bay are listed in Table 4-8. Concentrations of dissolved copper in 22 of the 50 samples exceeded
the screening level of 3.1 ng/L. The highest porewater concentration (664 ng/L) was reported in PW-027
located just south of the former mill, on the east side of the barge slip. Elevated concentrations of dissolved

1 1

The metals results for SW-600 are presented in Table 4-9.

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SECTION 4 ANALYTICAL RESULTS

barium, iron, manganese, and zinc were also reported in numerous porewater samples from the Site.
Dissolved mercury was detected in 6 porewater samples, but all concentrations were below the screening
level. No screening level exceedances were identified for the background porewater samples.

Although staining and petroleum odors were noted in several intertidal borings near the former mill and
barge slip, only a few PAHs were detected in porewater samples collected from these areas and all detects
were below their respective screening levels.

4.5	Surface Water

The analytical results for surface water samples collected in the intertidal area along the shoreline of the
former mill, Lake Ellen Creek, Unnamed Stream, and Browns Bay are listed in Table 4-9. Concentrations of
dissolved copper in 7 of the 30 samples exceeded the screening level of 3.1 ng/L. The highest surface water
concentration (22.5 ng/L) was reported in SW-029 located at the head of the seep that originates at the
barge slip. Similarly elevated concentrations were also reported in the normal and FD samples collected at
SW-084 located along Unnamed Stream near its confluence with Lake Ellen Creek. Elevated concentrations
of iron were also reported in these samples. No screening level exceedances were identified for dissolved or
total mercury. No screening level exceedances were identified for the hourly grab samples collected at SW-
105 or the background surface water samples collected at Browns Bay. None of the time-series grab samples
from SW-108 had concentrations exceeding screening levels.

Although staining and petroleum odors were noted in several intertidal borings near the former mill and
barge slip, only a few PAHs were detected in the surface water samples collected from these areas and all
detects were below their respective screening levels.

4.6	Crab Tissue

The analytical results for crab tissue samples collected in Salt Chuck and Browns Bay are listed in Table 4-10.
Concentrations of total arsenic in all of the crab tissue samples, including those from the background
location at Browns Bay, exceeded the screening level for tissue. The arsenic speciation results for crab (also
presented in Table 4-10) will be used to better characterize the type of arsenic present in crab and its
potential impacts on human health. This information will be presented and interpreted in the upcoming Rl
Report.

4.7	2012 Bivalve Tissue Arsenic Speciation

The arsenic speciation results for the bivalve tissue samples collected in 2012 and analyzed in 2013 are listed
in Appendix H. The arsenic speciation results will be used to better characterize the type of arsenic present
in clams and its potential impacts on human health. This information will be presented and interpreted in
the upcoming Rl Report.

4.8	Groundwater

The analytical results for groundwater samples collected in the vicinity of the former mill are listed in
Table 4-11. The results are similar to those reported for 2012, with concentrations of DRO, naphthalene, and
several total and dissolved metals, including copper, exceeding their respective screening levels. The sample
from GW-03 had the highest concentrations of DRO and dissolved metals, while the samples (primary and
field duplicate) from GW-01 had the highest concentrations of naphthalene.

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SECTION 5

References

Alaska Department of Environmental Conservation. Revised as of October 1, 2011. Alaska Administrative
Code, Title 18, Chapter 75: Oil and Other Hazardous Substances Pollution Control.

Alaska Department of Environmental Conservation. August 2008. Guidelines for Data Reporting, Data
Reduction, and Treatment of Non-detect Values. Technical Memorandum 08-001.

Buchman, M.F. 2008. NOAA Screening Quick Reference Tables. NOAA OR&R Report 08-1, National Oceanic
and Atmospheric Administration, Office of Response and Restoration Division, Seattle, Washington, 34
pages. Available at http://response.restoration.noaa.gov/sites/default/files/SQuiRTs.pdf.

CH2M HILL. 2013a. Remedial Investigation Quality Assurance Project Plan Salt Chuck Mine Remedial
Investigation, Tongass National Forest, Alaska. Prepared for U.S. Environmental Protection Agency
Region 10. May 14.

CH2M HILL. 2013b. Modification to Tailings Delineation Activities - Salt Chuck Mine. Prepared for U.S.
Environmental Protection Agency Region 10. August 1.

CH2M HILL. 2013c. Modification to Groundwater Plume Delineation Activities - Salt Chuck Mine. Prepared
for U.S. Environmental Protection Agency. July 8.

Long, E.R., D.D. MacDonald, S.L. Smith, and F.D. Calder. 1995. "Incidence of Adverse Biological Effects within
Ranges of Chemical Concentrations in Marine and Estuarine Sediments." Environmental Management.
19(l):81-97.

North Wind Group (North Wind). 2012. Final Completion Report Non-Time-Critical Removal Action, Salt
Chuck Mine Mill, Prince of Wales Island, Alaska. May 2012.

U.S. Environmental Protection Agency (EPA). 1986. Quality Criteria for Water. EPA 440/5-85-001.

U.S. Environmental Protection Agency, Office of Water Regulations and Standards, Washington, DC.
May 1.

U.S. Environmental Protection Agency (EPA). 2004. National Recommended Water Quality Criteria.
U.S. Environmental Protection Agency, Washington, DC.

U.S. Environmental Protection Agency (EPA). 2011. Regional Screening Level Fish Ingestion Summary Table.
Available at http://www.epa.gov/reg3hscd/risk/human/index.htm. June.

U.S. Environmental Protection Agency (EPA). 2012. Regional Screening Levels for Chemical Contaminants at
SuperfundSites. Available at http://www.epa.gov/region9/superfund/prg/.

ES022414063908SEA/SEA1405 50001

5-1


-------
Tables


-------
TABLE 1-1

Comparison of Planned and Actual Field Activities

2013 Salt Chuck Mine Superfund Site Field Doto Report

Medium/Location

Analytes

Planned

Actual

Reason for Changes

Marine Surface Sediment (Lake Ellen Creek Thalweg Area)

AVS/SEM Metals

5

5

2 samples mistakenly submitted for grain size analysis

Bioassay (polychaetes, bivalves)

5

5

Grain Size

5

7

Mercury

10

10

TAL Metals

10

10

Marine Surface Sediment (Agronomic)

Mercury

0

10



TAL Metals

0

10

Agronomic

10

10

Marine Tailings and Sediment

Total Organic Carbon

42

37

QAPP assumed 4 samples per short core location and 15 samples per deep core location for the May 2013 field event (total of
132 samples for metals analysis). Most May 2013 cores were less than 2 feet deep and the deep borings were not attempted in
May. Certain visual short-core locations were omitted due to time constraints. New/modified deep cores and 141 additional
samples were added to the sampling program as part of the Tailings Delineation Modification Memo. However, several of the
planned deep borings were omitted or were shorter. Consequently, fewer sediment samples were collected for metals analysis
during the May and August field events. Also, the number of borings and samples associated with the PAH delineation effort was
not specified in the Modification Memo, so these account for the differences in the number of borings and PAH samples.

Chromium VI

8

7

TAL Metals

273

191

Mercury

273

191

SPLP Metals

36

31

PAHs

36

50

Grain Size

42

37

Bulk Density

42

34

Visual Borings and Test Pits

Short-core - 64
Deep-core -5/0*

Short-core - 32

Test Pit - 4
Deep-core -12
Total - 48

Sampled Borings and Test Pits

Short-core - 22
Deep-core -2/8*

Short-core - 34

Test Pit -1
Deep-core -11
Total - 46

Upland Tailings and Soil

TAL Metals

74

16

QAPP assumed 4 samples per short core location and 15 samples per deep core location. Most cores were less than 2 feet deep.
Therefore, fewer samples were collected for total metals analysis. The additional hexavalent chromium analysis is a field
duplicate added for quality assurance purposes. Also, the number of borings associated with the upland tailings delineation
effort was not specified in the QAPP, so these account for the differences in the number of borings.

Mercury

74

16

Chromium VI

2

3

Visual Borings and Test Pits

Short-core - 2

Short-core -1
Test pit - 31
Total-32

Sampled Borings and Test Pits

Short-core - 4

Short-core - 5
Test pit - 3
Total - 8

Porewater

Dissolved TAL Metals

48

50

3 background porewater samples collected at Browns Bay, 1 drive-point location with metals and PAH analysis not installed due
to proximity of other porewater sample locations, obtained sufficient volume for dissolved mercury analysis at airstone locations

Dissolved Mercury

8

50

PAHs

8

7

Marine Surface Water

Total TAL Metals

6

4

Hourly samples at one location were counted as single sample in QAPP. Surface water samples to be used in SPLP leaching were
mistakenly counted as field samples in QAPP.

Total Mercury

6

4

Dissolved TAL Metals

23

30

Dissolved Mercury

23

30

PAHs

6

6

Crab Tissue

Lipids

17

16

Methylmercury was mistakenly included in several QAPP tables, this analyte should not have been included because the risk
assessment will assume that all mercury detected in tissue is methylmercury. One field duplicate sample was not collected.

TAL Metals

17

16

Mercury

17

16

Methylmercury

17

0

Arsenic Speciation

17

16

Shrimp Tissue

Lipids

16

0

Insufficient shrimp present in Salt Chuck

TAL Metals

16

0

Mercury

16

0

Methylmercury

16

0

Arsenic Speciation

16

0

Groundwater

Total TAL Metals

9

7

2 new wells not installed (GW-07 and GW-08), limited groundwater recovery, compromised well (GW-06)

Dissolved TAL Metals

9

7

PAHs

9

6

DRO/RRO

9

6

* Number of deep cores listed in Tailings Delineation Modification Memorandum
Notes:

AVS/SEM = acid volatile sulfide/simultaneously extracted metals

DRO = diesel range organics

PAHs = polycyclic aromatic hydrocarbons

RRO = residual range organics

SPLP = synthetic precipitation leaching procedure

TAL = target analyte list

PAGE 10F 1


-------
TABLE 1-2

2013 Field Investigation Chronology

2013 Salt Chuck Mine Superfund Site Field Data Report



May 2013 Event

Task

22-May

23-May

24-May

25-May

26-May

27-May

28-May

29-May

30-May

Surface Sediment Investigations

Thalweg-associated



















Reference area



















Agronomic



















Intertidal Tailings Investigation

Short cores/test pits



















Deep cores



















Upland Tailings Investigation

Short cores/test pits



















Biota

Site



















Reference Area



















Porewater Investigation

Airstones



















Drive points



















Reference airstones



















Surface Water Investigation

Grabs



















Hourly grabs



















Groundwater Investigation

GW-01 - GW-04, GW-06



















GW-05r



















August 2013 Event

27-Aug

28-Aug

29-Aug

30-Aug

































































































































PAGE 1 OF 1


-------
TABLE 2-1

Surface Marine Sediment Sample Information

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

Elevation
(feet NAVD88)

Latitude

Longitude

Date

Time

Water
Depth (feet)

Tide

Description

Comments

Deviations

SS-139

2013SC-SS-139

--

55.618125

-132.553951

5/24/2013

6:45 AM

NA*

Low

Not recorded



Mistakenly submitted for bioassay and AVS/SEM
analyses - discarded by lab

SS-140

2013SC-SS-140



55.618245

-132.552901

5/24/2013

6:20 AM

NA*

Low

Not recorded

Field duplicate 2013SC-SS-9140
(bioassay, AVS/SEM, grain size)



SS-141

2013SC-SS-141

--

55.617305

-132.552781

5/24/2013

7:26 AM

NA*

Low

Not recorded

Field duplicate 2013SC-SS-9141 (metals)
and MS/MSD

Mistakenly submitted for bioassay and AVS/SEM
analyses - discarded by lab

SS-143

2013SC-SS-143



55.616355

-132.554141

5/29/2013

5:10 PM

15

High

Black; very fine sand and
clay; shells; eel grass

Collected with Ponar



SS-144

2013SC-SS-144



55.616385

-132.552401

5/29/2013

5:05 PM

20

High

Black; very fine sand and
silt; shells; woody debris

Collected with Ponar



SS-145

2013SC-SS-145



55.616385

-132.551341

5/29/2013

5:00 PM

19

High

Dark grey to black; very
fine sand; eel grass

Collected with Ponar



SS-146

2013SC-SS-146



55.615415

-132.553661

5/29/2013

5:20 PM

36

High

Black; very fine sand
with clay

Collected with Ponar



SS-147

2013SC-SS-147

--

55.615785

-132.550831

5/29/2013

5:30 PM

27

High

Black; very fine sand
with clay; clam shells

Collected with Ponar



SS-510

2013SC-SB-510



55.587705

-132.546961

5/27/2013

9:00 AM

NA*

Low

Numerous shells on top
layer

Reference bioassay

Sample ID mistakenly uses SB instead of SS.

SS-181

2013SC-SS-181

11.9

55.625693

-132.557298

5/29/2013

5:06 PM

NA*

Low

Not recorded -
agronomic



Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-182

2013SC-SS-182

11.3

55.625567

-132.557532

5/29/2013

5:11 PM

NA*

Low

Not recorded -
agronomic



Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-183

2013SC-SS-183

12.9

55.625602

-132.557708

5/29/2013

5:15 PM

NA*

Low

Not recorded -
agronomic

Field duplicate 2013SC-SS-9183

Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-184

2013SC-SS-184

13.1

55.625741

-132.557375

5/29/2013

5:25 PM

NA*

Low

Not recorded -
agronomic



Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-185

2013SC-SS-185

11.2

55.625434

-132.557208

5/30/2013

8:30 AM

NA*

Low

Not recorded -
agronomic

Adjacent to rock jetty.

Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-186

2013SC-SS-186

10.7

55.625338

-132.557171

5/30/2013

8:55 AM

NA*

Low

Not recorded -
agronomic

Adjacent to rock jetty.

Analyzed fortotal metals and mercury in addition to
agronomic properties

SS-187

2013SC-SS-187

12.5

55.624805

-132.558383

5/30/2013

9:18 AM

NA*

Low

Not recorded -
agronomic

In grass west of unnamed stream

Analyzed for total metals and mercury in addition to
agronomic properties

SS-188

2013SC-SS-188

10.9

55.624896

-132.55835

5/30/2013

9:50 AM

NA*

Low

Not recorded -
agronomic

In grass west of unnamed stream

Analyzed for total metals and mercury in addition to
agronomic properties

SS-189

2013SC-SS-189

9.6

55.624817

-132.558216

5/30/2013

10:15 AM

NA*

Low

Not recorded -
agronomic

In grass west of unnamed stream

Analyzed for total metals and mercury in addition to
agronomic properties

— Sample location outside of area surveyed for elevation
* Location accessed during low tide (no water depth measurement)
Notes:

AVS/SEM = acid volatile sulfides/simultaneously extracted metals
MS/MSD = matrix spike/matrix spike duplicate

PAGE 1 OF 1


-------
TABLE 2-2

Surface Marine Sediment Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report











Analytical Suite and Laboratory











Grain Size





AVS/SEM

Bioassay

Agronomic





Sample

Depth



(Applied Sciences

Mercury

TAL Metals a

(Applied Sciences

(Northwest

(A&L Western

Location

Activity ID

Type

(feet)

Sample Date

Laboratory)

(A4 Scientific)

(A4 Scientific)

Laboratory)

Aquatic Sciences)

Agricultural Labs)

SS-139

2013SC-SS-139-00-20130529

N

LO

o
o

5/29/2013

X

X

X







SS-140

2013SC-SS-140-00-20130529

N

LO

o
o

5/29/2013

X

X

X

X

X



SS-140

2013SC-SS-9140-00-20130529 FD

FD

LO

o
o

5/29/2013

X





X

X



SS-141

2013SC-SS-141-00-201305 29

N

LO

o
o

5/29/2013

X

X

X







SS-141

2013SC-SS-9141-00-20130529 FD

FD

LO

o
o

5/29/2013



X

X







SS-143

2013SC-SS-143-00-20130529

N

LO

o
o

5/29/2013



X

X







SS-144

2013SC-SS-144-00-20130529

N

LO

o
o

5/29/2013



X

X







SS-145

2013SC-SS-145-00-20130529

N

LO

o
o

5/29/2013

X

X

X

X

X



SS-146

2013SC-SS-146-00-20130529

N

LO

o
o

5/29/2013

X

X

X

X

X



SS-147

2013SC-SS-147-00-20130529

N

LO

o
o

5/29/2013



X

X







SS-181

2013SC-SS-181-00-201305 29

N

LO

o
o

5/29/2013



X

X





X

SS-182

2013SC-SS-182-00-20130529

N

LO

o
o

5/29/2013



X

X





X

SS-183

2013SC-SS-183-00-20130529

N

LO

o
o

5/29/2013



X

X





X

SS-183

2013SC-SS-9183-00-20130529 FD

FD

LO

o
o

5/29/2013



X

X





X

SS-184

2013SC-SS-184-00-20130529

N

LO

o
o

5/29/2013



X

X





X

SS-185

2013SC-SS-185-00-20130530

N

LO

o
o

5/30/2013



X

X





X

SS-186

2013SC-SS-186-00-20130530

N

LO

o
o

5/30/2013



X

X





X

SS-187

2013SC-SS-187-00-20130530

N

LO

o
o

5/30/2013



X

X





X

SS-188

2013SC-SS-188-00-20130530

N

LO

o
o

5/30/2013



X

X





X

SS-189

2013SC-SS-189-00-20130530

N

LO

o
o

5/30/2013



X

X





X

SS-510

2013SC-SB-510-00-20130527

N

LO

o
o

5/27/2013

X

X

X

X

X



Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium, silver, thallium, vanadium, zinc
AVS/SEM = acid volatile sulfides/simultaneously extracted metals
N = normal
FD = field duplicate

PAGE 1 OF 1


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-004

Test pit

10.9

55.626065

-132.557311

5/28/2013

7:00 AM

12

12

2013SC-SB-004-00 +
MS/MSD

0" to 6" - very fine SAND, dark
greenish gray with red oxidation,
dense, moist

2013SC-SB-004-0.5
2013SC-SB-9004-0.5

6' to 12" - wet, dark greenish gray
veryfine SAND with ~10%Silt, red
oxidation layers, dense









Drilled three attempts with hand
vibracore. Too rocky to get sample via
core; collected with shovel.

0.5' -1.0' interval had hydrocarbon
odor



SB-013

Short-core

8.0

55.625855

-132.556571

5/28/2013

9:25AM

25

14.25

2013SC-SB-013-00

0" to 8" - dark gray very fine to
fins SAND, micaceous, dense,
moist

2013SC-SB-013-0.5

8" to 10" - grayish green veryfins
SAND, very dense, moist

No sample

10" to 14" - dark gray to black fine
SAND, dense, moist. Refusal in
loose wet sand





0" to 10" - petroleum odor; tailings.
10" -14" - strong petroleum odor,
orange-colored water in bags and on
surface of sample pile. No odor, not
petroleum

Moved ~10 ft from planned
location

SB-018

Short-core

12.2

55.625745

-132.557261

5/27/2013

10:06 AM

27.5

11.25

2013SC-SB-018-00

0" to 11.25" - very fine grained
SAND (SP), trace Silt/Clay, olive
gray with some mica flakes, wet

2013SC-SB-018-0.5
+MS/MSD

0" to 11.25" - veryfine grained
SAND (SP), trace Silt/Clay, olive
gray with some mica flakes, wet

No sample

Same as previous, more Silt from
1.2'to 1.4'





Tailings



SB-020

Short-core

8.2

55.626028

-132.558003

5/23/2013

12:27 PM

42

27

No sample

0" to 1.5" -fine to medium
SAND, moist, iron oxide stain,
loose

1.5" to 17" - silty CLAY with very
fine Sand, grey with light grey
laminations, wet, interbedded
Sand at 6", 9" 12" and 16", hard

No sample

1.5" to 17" - silty CLAY with very
fine Sand, grey with light grey
laminations, wet, interbedded
Sand at 6", 9" 12" and 16", hard

No sample

1.5" to 17" - silty CLAY with very
fine Sand, grey with light grey
laminations, wet, interbedded
Sand at 6", 9" 12" and 16", hard
17" to 21" - fine and medium
SAND, black, loose, wet,
micaceous.

21" to 24" - same as above with
increased fine content

No sample

24" to 27" - veryfine SAND,
micaceous, grey, wet

no debris



SB-021

Test pit

10.2

55.626225

-132.558151

5/28/2013

8:00 AM

18

18

2013SC-SB-021-00

0" to 5" - root mat with
vegetation, very little soil, mainly
consisting of brown silty Sand
with some subangular Gravel

2013SC-SB-021-0.5

5" to 12" - black to brown coarse
SAND (tailings) with orange Silt
(iron oxide staining)

No sample

12" to 18" - saturated GRAVEL
with some coarse Sand, very wet
and difficult to dig; gravel
diameter 1" to 2"





collected and logged via test pit; hit
refusal on 4 attempts drilling



SB-031

Short-core

7.4

55.625825

-132.558021

5/28/2013

8:30 AM

21

19

2013SC-SB-031-00,
2013SC-SB-9031-00

Oto 5 in. = black to rusty orange
very fine SAND, root mass, some
mica

2013SC-SB-031-0.5

5 to 8 in. = fine SAND, micaceous,
dark gray, loose, moist

2013SC-SB-031-01

8" to 18" - dense gray clay, wet
18" - 21" - dark gray fine grained
SAND, loose, moist





0' - 5" - tailings w/roots/vegetation
5" - 8" -tailings, no odor
18". 21" - tailings, petroleum odor
when homogenized



SB-032

Short-core

5.7

55.625615

-132.556421

5/27/2013

11:19 AM

25.5

13.5

2013SC-SB-032-00

0" to 13.5" - very fine grained
SAND, little Silt, trace wood, dark
grayish black to olive gray with
mica flakes at ~1 ft bgs, wet, light
gray clay-like material at ~1 foot

2013SC-SB-032-0.5

0" to 13.5" - veryfine grained
SAND, little Silt, trace wood, dark
grayish black to olive gray with
mica flakes at ~1 ft bgs, wet, light
gray clay-like material at ~1 foot









0' to 13.5" - likely tailings; sulfur odor



SB-033

Short-core

7.1

55.625515

-132.556881

5/27/2013

10:48 AM

19

12

2013SC-SB-033-00

0" to 5" - grayish black and black
very fine SAND, 5% mica, moist,
dense

2013SC-SB-033-0.5

5" to 10" - laminated gray and
black v.f. SAND and CLAY layers,
very dense, moist
10" -12" - greenish gray v.f. SAND,
moist, dense









0" -12" - tailings

0" -10" - possible HC or creosote odor



SB-036

Short-core

9.8

55.626223

-132.558455

5/28/2013

12:45 PM

36

25.5

No sample

0" to 10" - clayey soil and dense
root mat. Oxidized with black
organic decay. Wet.

No sample

10" -14" - fine SAND with 15-20%
fines. Dark gray to olive. Wet

No sample

14" to 15" - Poorly graded fine
SAND, trace fines, brown, wet.
15" - 25.5" - fine SAND with trace
fines, grey, poorly graded SAND,
wet, with globs of light grey Silty
Clay, globs have thin laminations.
Globs randomly located in
interval.

No sample



0" to 15" - roots and decaying
vegetation



SB-043

Short-core

10.5

55.625395

-132.557361

5/27/2013

9:50 AM

32.5

26.4

2013SC-SB-043-00

0" to 18" - very fine grained
SAND with thin Clay/Silt
laminations, olive gray, wet, light
gray laminations

2013SC-SB-043-0.5

0" to 18" - very fine grained SAND
with thin Clay/Silt laminations,
olive gray, wet, light gray
laminations

2013SC-SB-043-01

18" to 26.4"-fine SAND, dark
grayish black with some mica
flakes, wet





0" - 26.4" - Tailings



SB-052

Short-core

10.2

55.625675

-132.555561

5/28/2013

9:45 AM

26.4

22

2013SC-SB-052-00

0" - 22" - fine SAND, trace fines,
poorly graded, wet, olive with
black bands of very fine sand,
degraded vegetation at 6"

2013SC-SB-052-0.5

see 0" to 6" cell

2013SC-SB-052-01

see 0" to 6" cell

No sample







SB-059

Short-core

9.6

55.625135

-132.557051

5/27/2013

8:30 AM

36

25

2013SC-SB-059-00

0" to 14" - greenish gray v.f. to f.
SAND, ~5% mica, moist, dense,
1/4" band of black sand at 11"

2013SC-SB-059-0.5

see 0" to 6" cell

2013SC-SB-059-01

14" to 16" - gray brown SILT and

v.f. SAND bands, moist, very dense

16" to 18" - greenish gray v.f.

SAND, moist, very dense

18" to 20" - gray brown laminated

SILT and v.f. SAND, moist, very

dense

21" to 25" - greenish gray, v.f.
SAND, 5% mica, loose, wet

No sample

see 12" to 24" cell

0" to 14" tailings, no odor

0.5' to 2' - possible naphthalene odor



SB-061

Short-core

8.4

55.625125

-132.557801

5/27/2013

8:58 AM

18

12.25

2013SC-SB-061-00

Very fine grained SAND, some
Silt/Clay, olive green with mica
flakes, wet, Clay/Silt laminations
are light gray

2013SC-SB-061-0.5

Veryfine grained SAND, some
Silt/Clay, olive green with mica
flakes, wet, Clay/Silt laminations
are light gray









tailings



PAGE 1 OF 6


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-062

Short-core

8.5

55.625365

-132.555501

5/28/2013

11:15AM

42

27.5

2013SC-SB-062-00

0" to 9" tailings material, grayish
brown, fine SAND, dense, moist

2013SC-SB-062-0.5

9" to 27.5" laminated very fine
greenish gray and light gray, very
dense, SILT

2013SC-SB-062-01

9" to 27.5" laminated very fine
greenish gray and light gray, very
dense, SILT









SB-078

Short-core

8.9

55.625235

-132.554881

5/28/2013

10:05 AM

42

29.5

2013SC-SB-078-00

0' to 9" - fine SAND with trace
fines, wet, brown to olive, poorly
graded

2013SC-SB-078-0.5

9" - 29.5" -fine SAND with SILT,
gray Clay lenses throughout with
thin laminations, wet, brown

2013SC-SB-078-01

9" - 29.5" -fine SAND with SILT,
gray Clay lenses throughout with
thin laminations, wet, brown

No sample







SB-079

Short-core

3.9

55.624915

-132.555311

5/28/2013

11:00 AM

32

22.5

2013SC-SB-079-00

0' to 3' - SILT with trace fine
Sand, wet, dark brown, soft.
3" to 12" - very fine SAND with
trace Silt, poorly graded, dense,
dark brown, wet

2013SC-SB-079-0.5

see 0" to 6" cell

2013SC-SB-079-01

12" to 19" - CLAY, gray with thin
laminations, wet, soft
20" to 22.5" - fine SAND with trace
fines, olive

No sample







SB-082

Short-core

7.5

55.625315

-132.554401

5/28/2013

10:15AM

24

17

2013SC-SB-082-00

0" to 6" - very fine black SAND,
micaceous, well rooted

2013SC-SB-082-0.5

6" to 12" - very dense gray and
black laminated very fine and fine
SAND, decaying organic matter,
some Gravel in interval

2013SC-SB-082-01

12" to 17" -1 to 1.5 feet of very
wet, very fine SAND and CLAY,
sulfur odor; below 17" - Gravel,
moist

No sample



0"to6"_ strong sulfur odor



SB-089

Short-core

6.1

55.624775

-132.554641

5/28/2013

10:30 AM

42

29.75

2013SC-SB-089-00

0" to 10" - dark gray to black fine
SAND with red inclusion, slight
petroleum odor

2013SC-SB-089-0.5

10" to 29.75" - dark gray very
dense, very fine SAND, petroleum
odor, very wet 15" to 16"

2013SC-SB-089-01

see 6" to 12" cell

No sample







SB-109

Short-core



55.623674

-132.553773

5/23/2013

3:45 PM

24

14.4

No sample

0" to 6" - gray, dense, SILT with
Gravel and organic debris

No sample

6" to 12" - gray SAND with Gravel
and red Silt

No sample

12" -14.4" - gray GRAVEL with
gray Sand and some Silt

No sample



No odor; red silt in 6" to 12" interval is
rust color

No sample per change to
sampling plan at SB-127

SB-110

Short-core



55.623721

-132.553034

5/23/2013

3:30 PM

14

12

No sample

0" to 2" - coarse brown to red
SAND with angular GRAVEL,
some Silt

2" to 6" - brown, coarse SAND
with red SILT and smooth poorly
sorted Gravel

No sample

6" to 12" - GRAVEL with fine brown
Sand and Silt

No sample



No sample



No odor

2" to 6" - fine Silt is a red, rust color
6" to 12" - very little rust colored Silt
in this interval



SB-Ill

Short-core



55.623815

-132.552621

5/23/2013

7:00 AM

36

18

2013SC-SB-111-00

0"to 18" - Sandy SILT to silty
SAND (ML/SM), Sand is fine to
coarse, little fine angularto
subrounded Gravel, trace shells,
trace plant material, wet, grayish
black

2013SC-SB-111-0.5

See 0" to 6" cell

2013SC-SB-111-01

See 0" to 6" cell









SB-112

Short-core



55.624022

-132.552132

5/22/2013

3:00 PM

18

9

No sample

0" to 9" - brown to black fine SILT
with angular Gravel and woody
debris

No sample

see 0" to 6" cell

No sample



No sample



subsurface portion of core had strong
marine decay odor



SB-114

Short-core



55.622648

-132.556454

5/24/2013

8:30 AM

6

6

No sample

Brown SILT with Gravel, 50% Silt
and 50% Gravel, angular gravel

















SB-115

Short-core



55.623485

-132.552761

5/22/2013

6:36 AM

36

21

2013SC-SB-115-00
2013SC-SB-9115-00

0"to 15.6" -siltyfineto medium
SAND (SM), little fine to coarse
Gravel (subrounded) coarsening
downward, few laminations (Silt)
near surface, grayish black, wet,
trace shell fragments

2013SC-SB-115-0.5

See 0" to 6" cell

2013SC-SB-115-01

15.6" to 21" - Silty fine to coarse
GRAVEL (GM), abundant shell
fragments, little fine Sand, wet,
dark grayish brown. Gravel is
subangularto angular

2013SC-SB-115-1.5



Ocean-like odor from sample; non-
sulfur



SB-116

Short-core



55.624219

-132.551554

5/22/2013

2:34 PM

6

6

No sample

0" to 1" -GRAVEL with well
graded Sand, Gravel up to 1",
angularto subangular, organics,
brown, wet, soft.

1" to 6" - SILT with GRAVEL,
brown. Gravel upto 1/2"
subrounded to sub angular, wet,
soft.













0" to 1" - algae cover and some
seaweed

1" to 6" - woody debris



SB-117

Short-core



55.622695

-132.554951

5/24/2013

6:40 AM

36

15.6

2013SC-SB-117-00

0" to 15.6" - fine to coarse
angular to subangular Silty
GRAVEL (GM), some fine to
coarse Sand, little Silt, wet,
grayish brown with some red-
brown oxidation, olive gray 1.1'
to 1.3', trace roots, possible fine
grained tailings from 1.1' to 1.3'

2013SC-SB-117-0.5

See 0" to 6" cell

2013SC-SB-117-01

See 0" to 6" cell









SB-118

Short-core



55.623581

-132.552279

5/22/2013

7:04 AM

42

22

No sample

0" to 2" - very fine SAND with
SILT, olive to dark brown, wet,
loose

2" to 4" - SILT with very fine
SAND, laminated gray to light
gray, wet, soft

4" to 6" - well graded SAND, fine
to coarse, trace Gravel, 10%.
15% fines, wet, dark brown,
loose.

No sample

6" to 18" - Same as above. Brown
color grades with increased Gravel
beginning at 16". Gravel 1/2"
rounded, wet.

No sample

18" to 14" - GRAVEL with coarse
SAND and trace fines, wet, loose,
up to 1/2" subrounded to
rounded.

14" - 22" - Same as above with
shell hash, dark gray

No sample







PAGE 2 OF 6


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-119

Short-core



55.624075

-132.551487

5/22/2013

2:59 PM

27

14

No sample

0" to 4" - SILT with trace very
fine Sand, wet, soft, dark brown.
4" to 8" - SILT, increased density,
wet, dark brown

No sample

8" to 10" - medium SAND with
GRAVEL, trace coarse Sand, trace
fines, loose, wet, subrounded
Gravel to 1/2".

No sample

10" to 14" - GRAVEL with SAND,
well graded. Silt (15%), wet, loose,
medium brown.

No sample







SB-120

Short-core



55.622526

-132.555662

5/24/2013

Jot recorde

14

14

No sample

Surface covered with small rocks
and Gravel. To 6"-Thin clay soil
with vegetation

No sample

6" to 14" - small angular Gravel,
reddish brown.













SB-121

Short-core



55.624165

-132.551141

5/23/2013

9:15AM

36

24

2013SC-SB-121-00

0" to 6" - black Clayey Sandy
GRAVEL, Gravel is subangular,
same color as sand, not plastic,
wet, poorly soil

2013SC-SB-121-0.5

6" to 10" - dark black very wet
Sandy SILT, some white shell (sand
sized), clams.

10" to 12" - two-inch subangular
rock, one-inch subangular rock.

2013SC-SB-121-01

12" to 24" - light gray SAND with
GRAVEL, light particles are shell
hash, likely bivalves. Gravel is
subangular 1/2" to 2" size range,
wet, soil is cohesive



No recovery

0" to 6" - Gravel ranges to 1" diameter
12" to 24" - over 50% shell pieces



SB-123

Short-core



55.623845

-132.551261

5/23/2013

6:00 AM

36

30

2013SC-SB-123-00 +
MS/MSD

2013SC-SB-9123-00

0" to 30" - SILT (ML), trace fine to
medium Sand below 2 feet bgs,
thinly bedded/laminated Silt,
trace organics (wood, plant
fibers), grayish black, wet, non-
plastic

2013SC-SB-123-0.5

See 0" to 6" cell

2013SC-SB-123-01

See 0" to 6" cell

2013SC-SB-123-02

See 0" to 6" cell (24" to 30")





SB-124

Short-core

*

55.623144

-132.552059

5/22/2013

7:15AM

12

12

No sample

Dark gray SILT

No sample

Gray SILT with some fine Sand
(<10%), stiff

No sample

GRAVEL with fine SAND, shell
fragments

No sample



Info from Attempt 2 at this location
No odor



SB-125

Short-core



55.623944

-132.550755

5/22/2013

9:10AM

24

12

No sample

0" to 2" - SILT with trace very
fine Sand, wet, soft, dark brown
2" to 5"-SILT with CLAY, light
brown to dark brown with thin
laminations, wet, soft.

No sample

5" to 12" - Sandy GRAVEL, well
graded Sand, mostly fine Gravel,
subangular to subrounded, brown,
wet, black band between 5" and 6"













SB-126

Short-core



55.624012

-132.55046

5/23/2013

Jot recorde

0

0

No sample

Three sample attempts but
hitting rock and were unable to
collect.

















SB-127

Short-core



55.623295

-132.551531

5/22/2013

6:45 AM

36

18

2013SC-SB-127-00

0" to 12" - SILT (ML), some very
fine Sand, trace shells, trace
organics, dark gray to black, wet,
non-plastic, few thin laminations
in Silt zones, trace organics/plant
matter

2013SC-SB-127-0.5

See 0" to 6" cell

2013SC-SB-127-01

12" to 18" - Silty fine to medium
SAND, some shell fragments, little
fine subrounded Gravel, wet, dark
gray to black - possibly tailings









SB-128

Short-core



55.62345

-132.551033

5/23/2013

7:05 AM

42

29.5

No sample

0" to 3" - SILT with CLAY, wet,
soft, black

3" to 4" SILT, gray, soft, wet
4" to 8"-fine SAND with SILT,
gray, wet, loose.

No sample

8" to 21" - same as 4" to 8" with
increased Silt content, gray

No sample

8" to 21" - same as 4" to 8" with
increased Silt content, gray
21" to 29.5" Sandy SILT, very fine
Sand, soft, wet, dark brown

No sample

21" to 29.5" Sandy SILT, very
fine Sand, soft, wet, dark
brown





SB-129

Short-core



55.623585

-132.550591

5/23/2013

6:08 AM

36

25.2

2013SC-SB-129-00
+MS/MSD
2013SC-SB-9129-00

0" to 25.2"-SILT (ML), little fine
Sand throughout from about 1.5'
bgs and below, trace shell
fragments from 1.2' bgs and
below, trace fine subangular
Gravel and trace plant
fibers/wood below 1.2', wet,
grayish black, thinly laminated
Silt

2013SC-SB-129-0.5

See 0" to 6" cell

2013SC-SB-129-01

See 0" to 6" cell

See 0" to 6" cell







SB-131

Short-core



55.623704

-132.550152

5/23/2013

8:47 AM

36

15

No sample

0" to 3" - SILT with trace very
fine Sand, dark brown, wet
3" to 5" SILT with CLAY, light to
dark gray with thin laminations,
soft, wet

No sample

5" to 15" - Sandy GRAVEL, well
graded Sand, Gravel up to 1/2 inch,
subangularto subrounded, wet,
loose, black and iron oxide bands
between 6" and 8'













SB-132

Short-core



55.622902

-132.551065

5/22/2013

7:41 AM

39

25

No sample

0" to 1.5" - SILT, dark gray, wet,
soft

2" to 20" - very fine SAND with
trace fines (10%fines), grayish
brown, moist, wet at 17"

No sample

2" to 20" - very fine SAND with
trace fines (10%fines), grayish
brown, moist, wet at 17"

No sample

2" to 20" - very fine SAND with
trace fines (10%fines), grayish
brown, moist, wet at 17"
20" to 25" - very fine SAND with
SILT, iron oxide staining in bands,
soft, v.f. Sand is grayish brown

No sample







SB-133

Short-core



55.623065

-132.550461

5/22/2013

6:00 PM

36

30

2013SC-SB-133-00

0" to 30"-SILT (ML), little very
fine Sand and possible fine
tailings, thin laminations within
Silt, trace organics/plant matter,
one coarse angular Gravel, wet,
dark gray to dark olive gray

2013SC-SB-133-0.5

See 0" to 6" cell

2013SC-SB-133-01
2013SC-SB-9133-01

See 0" to 6" cell

2013SC-SB-133-02

See 0" to 6" cell





SB-134

Short-core



55.623209

-132.550017

5/23/2013

7:29 AM

42

26.5

No sample

0" to 13" - SILT with very fine
SAND, soft, wet, dark gray to
light gray, thin laminations
throughout

No sample

see 0" to 6" cell

No sample

13" to 26.5" - SILT, dark gray to
black, organics at 22", soft, wet.

No sample



clam shells in sample intervals



PAGE 3 OF 6


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-135

Short-core



55.623313

-132.549725

5/23/2013

7:57 AM

42

16

No sample

0" to 3" - SILT with trace very
fine Sand, black, soft, wet
3" to 7.5" - SILT with CLAY, light
to dark gray, thin laminations
between 5" and 7.5", wet, soft.

No sample

7.5" to 16" - Gravelly SAND, well
graded Sand, black to dark brown,
medium size Gravel, angularto sub
rounded, up to 1/2 inch, wet, loose

No sample

7.5" to 16" - Gravelly SAND, well
graded Sand, black to dark brown,
medium size Gravel, angularto
sub rounded, upto 1/2 inch, wet,
loose

No sample



shell hash at 16"



SB-136

Short-core



55.622814

-132.549818

5/22/2013

7:40 AM

42

30

No sample

0" to 12". light brown SILT with
some fines (<5%)

No sample

see 0" to 6" cell

No sample

12" to 24". dark brown SILT with
some fines, very loose, layer felt
soft while drilling

No sample

24" to 30" - brown to black
very stiff SILT with no fines





SB-137

Short-core



55.623001

-132.549389

5/22/2013

8:41AM

36

18

No sample

0" to 9" - brown stiff Clayey SILT;
slight earthy odor

No sample

0" to 9" - brown stiff Clayey SILT;
slight earthy odor
9 to 18"-fine GRAVEL, angular with
>15% Silt, no Sand

No sample

0" to 9" - brown stiff Clayey SILT;
slight earthy odor
9 to 18"-fine GRAVEL, angular
with >15% Silt, no Sand

No sample







SB-157

Short-core

4.0

55.624185

-132.555191

5/25/2013

11:35AM

42

27.5

2013SC-SB-157-00

0" to 18" - very fine SAND (SP),
with trace Silt, thinly laminated,
likely tailings (sand with mica)
from 0' to 0.6' bgs, some
oxidation from 0' to 0.3', olive
green to dark grayish black ~0.1
ft thick laminated layers of
smooth clay-like material from
1.4' to 1.5' (light gray), wet

2013SC-SB-157-0.5

0" to 18" - very fine SAND (SP),
with trace Silt, thinly laminated,
likely tailings (sand with mica)from
0' to 0.6' bgs, some oxidation from
0' to 0.3', olive green to dark
grayish black ~0.1 ft thick
laminated layers of smooth clay-
like material from 1.4' to 1.5' (light
gray), wet

2013SC-SB-157-01

18" to 27.5" - dark grayish brown
fine to coarse SAND (SW), some
Silt, little fine to coarse subangular
Gravel, trace shell fragments, wet

2013SC-SB-157-1.8



smooth clay-like layer has no odor,
dries quickly when smeared



SB-158

Short-core

2.6

55.623998

-132.55574

5/25/2013

11:28 AM

12

12

No sample

0" to 6" - dark gray, very fine,
micaceous SAND (100%), upper
three inches very fine lamination

No sample

6" to 10"-SAND and SILT
(80%/20%)

10" to 12" - SAND, GRAVEL, SILT
bed









Test pit - shovel dug
Shells, woody debris, top 6"



SB-159

Short-core

3.0

55.623808

-132.55642

5/25/2013

11:06 AM

12

12

No sample

0" to 3" - black, very fine SAND
(90%), Silt (10%), micaceous,
moist

3" to 7" - gray-brown fine SAND
(100%), rusty mottling, mica
(5%), moist

No sample

7" to 12" - Black, very fine SAND
(80%), Silt (20%)

No sample

12" - Sandy GRAVEL, Gravel (50%),
Sand (30%), Silt (20%), subangular
Gravel up to 2" dia.. Sand is
medium to coarse, dark gray, wet

No sample



Test pit - shovel dug

woody debris and shells throughout
sample intervals



SB-162

Short-core

6.0

55.624704

-132.556495

5/25/2013

1:15 PM

36

26

No sample

0" to 3" - laminated green gray
v.f. SAND with red inclusions,
moist, gray and yellow
laminations

3" to 12" - gray green v.f. SAND,
very dense, moist

No sample

3" to 12" - gray green v.f. SAND,
very dense, moist

No sample

12" to 19" - gray green v.f. SAND
with black mottles, micaceous,
light gray clay, rip up clasts at base
19" to 26" - light green gray SILT or
CLAY, gel-like consistency, wet

No sample

26" to 27" - black micaceous
v.f. SAND

Tailings; all intervals

19" to 26" - paste-like odor, very
different than tailings (retained for
possible analysis)



SB-163

Short-core

4.2

55.624357

-132.556158

5/26/2013

12:40 PM

36

18

No sample

0" to 9" - very fine SAND and
SILT, with mica flakes, thin
laminations of clay-like material,
olive gray to grayish black, wet,
clay-like laminations are light
gray

No sample

9" to 12" - fine to medium SAND
and SILT, some fine subangular
Gravel, dark grayish black, trace
shell fragments, possible tailings
mixed with sand and gravel, wet

No sample

12" to 18" - fine to coarse GRAVEL
and fine to coarse SAND, some
Silt, olive gray, wet

No sample



Soil core contains suspected tailings
from 0' to ~1'



SB-164

Short-core

8.8

55.625069

-132.556841

5/25/2013

12:55 PM

36

23

No sample

0" to 23" - dark gray green
micaceous v.f. SAND, moist, v.
dense, bioturbated (worm
castings, vent holes), few shells,
laminated section and rip up
clasts of gray clay at 21"

No sample

see 0" to 6" cell

No sample

see 0" to 6" cell

No sample



tailings, biological activity



SB-165

Short-core

8.5

55.624885

-132.557469

5/25/2013

1:00 PM

36

27

No sample

0" to 7" - light brown gray v.f.
SAND with bioturbation, some
mica

No sample

7" to 25" - dark gray v.f. SAND,
micaceous, dense, moist

No sample

7" to 25" - dark gray v.f. SAND,
micaceous, dense, moist

No sample

25' to 27" - same as 7" to
15" but very wet

Bioturbation may be worm-related
7" to 27" - tailings



SB-176

Test pit

7.6

55.625737

-132.558198

5/30/2013

8:00 AM

6

6

2013SC-SB-176-00

0" to 6" - brown, fine SAND













New sample location, 6" depth, spoon
dug

New sampling location in
removal area by unnamed
creek, south oftailings

SB-177

Test pit

12.0

55.626011

-132.558546

5/30/2013

8:34 AM

6

6

2013SC-SB-177-00

0" to 6" - brown, fine SAND
(tailings)













New sample location, 6" depth,
spoon dug

New sampling location in
removal area, south of SB-
176

SB-191

Short-core



55.623275

-132.552541

5/23/2013

7:45 AM

36

24

2013SC-SB-191-00

0" to 2" - dark gray brown Clayey
SILT with black mottling, 50% Silt
somewhat plastic and cohesive
2" to 4" - dark gray Gravelly
SAND, moist, not particularly
cohesive

4" to 8" - dark brown Silty SAND,
some mica present, moist, not
cohesive

2013SC-SB-191-0.5

4" to 8" - dark brown Silty SAND,
some mica present, moist, not
cohesive

8" to 20" - Dark gray to black Silty
SAND, abundant mica (20%),
suspected possible tailings

2013SC-SB-191-01

8" to 20" - Dark gray to black Silty
SAND, abundant mica (20%),
suspected possible tailings
20" to 24" - Sandy GRAVEL, dark
gray to black with subangular
Gravel (1/2" -1" diameter)





4" to 8" - wood debris and less than
5% shell

8" to 20" - woody debris and 5% shell
hash

20" - 24" - wood debris

New location in potential
depositional area

PAGE 4 OF 6


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-192

Short-core



55.623075

-132.552291

5/23/2013

8:00 AM

36

28

2013SC-SB-192-00

0" to 4" - dark gray to black very
fine SAND, possibly tailings, mica
content high

4" to 12' -dark gray Clayey
SAND and GRAVEL, sand is fine
grained, gravel is subangular
1/2" to 1" dia., moist to wet

2013SC-SB-192-0.5

4" to 12'. dark gray Clayey SAND
and GRAVEL, sand is fine grained,
gravel is subangular 1/2" to 1" dia.,
moist to wet

2013SC-SB-192-1

12" to 22" - coarse SAND and
GRAVEL, gravel 1/2"-1",
subangular

22" to 28". light gray Silty SAND
and GRAVEL, light colored material
is shell hash

2013SC-SB-192-02

22" to 28" - light gray Silty
SAND and GRAVEL, light
colored material is shell hash
28" - dark gray Silty SAND
and GRAVEL

0" to 4" - no wood debris, shell hash
<5% in last inch, distinct decaying
marine odor

New location in potential
depositional area

SB-193

Short-core



55.623182

-132.552225

5/23/2013

9:34 AM

36

22.5

No sample

0" to 2". 0% Gravel, 10% Sand,
90% fines, brown SILT with
brown fine Sand
2" to 18" - very fine black SAND,
100% sand, very loose

No sample

2" to 18" - very fine black SAND,
100% sand, very loose

No sample

18" - 30" - 50% GRAVEL, 50%
SAND, well sorted angular Gravel
with brown coarse Sand

No sample



no odor, marine deposits (0" to 2")

no odor, interval very loose, drilling
easy, suspected tailings-like material
(2" to 18") -sloughing was observed
around tube; sloughed 3" at this
interval only

similar to nearby creek bed (18" to
30")

New location in potential
deposit ional area

SB-194

Short-core



55.623329

-132.552274

5/23/2013

8:40 AM

12

12

No sample

2" to 12" -100% SAND, black fine
sand, loosely deposited













suspected tailings



SB-195

Short-core



55.622852

-132.552425

5/24/2013

6:50 AM

7

7

No sample

0" to 2" - Silty SAND with Gravel,
5% Gravel, 60% Clay, 35% fine
Sand, dark grayish brown, light
colored shells

2" to 6" - fine SAND with Gravel,
10% Gravel, fines, dark gray,
mica, possible tailings













Refusal at 7"



SB-196b

Short-core



55.622385

-132.552091

5/24/2013

7:15 AM

36

12

2013SC-SB-196-00

0" to 12" - fine to coarse Silty
SAND (SM), some fine
subangular Gravel, trace shell
fragments, grayish black, wet,
trace roots

2013SC-SB-196-0.5

0" to 12" - fine to coarse Silty
SAND, some fine subangular
Gravel, trace shell fragments,
grayish black, wet, trace roots









Log for 196a was a trial boring, log for
196b is log of record and sampled
borehole



SB-197

Short-core



55.622125

-132.551621

5/24/2013

7:20 AM

36

25.2

2013SC-SB-197-00

0" to 25.2" - predominantly fine
SAND (SP), some Silt, trace fine
angular Gravel, wet, grayish
black, little oxidation (red-
orange) from 0' to 1', trace shells
at 2.1'

2013SC-SB-197-0.5

0" to 25.2" - predominantly fine
SAND, some Silt, trace fine angular
Gravel, wet, grayish black, little
oxidation (red-orange) from 0' to
1', trace shells at 2.1'

2013SC-SB-197-01

0" to 25.2" - predominantly fine
SAND, some Silt, trace fine angular
Gravel, wet, grayish black, little
oxidation (red-orange) from 0' to
1', trace shells at 2.1'









SB-198

Short-core



55.622486

-132.551099

5/24/2013

7:45 AM

16

16

No sample

0" to 2"-fine SAND and SILT,
dark brown, wet, shell debris
2" to 10" - black, fine SAND, wet,
possibly tailings, <5% Gravel

No sample

2" to 10" - black, fine SAND, wet,
possibly tailings, <5% Gravel

No sample

10" to 16"-SAND and SHELLS
(bivalves) with Gravel, 50% Sand,
40% shell debris, 10% angular
Gravel

No sample







SB-199

Short-core



55.623635

-132.554591

5/24/2013

8:15 AM

36

19.2

2013SC-SB-199-00

0" to 19.2" - Silty fine to coarse
SAND (SM), little fine to coarse
subangular Gravel, trace shell
fragments, possible fine grained
tailings from 0.4' to 0.8',
brownish gray with some
oxidation, olive green from 0.4'
to 0.8'

2013SC-SB-199-0.5

0" to 19.2" - Silty fine to coarse
SAND (SM), little fine to coarse
subangular Gravel, trace shell
fragments, possible fine grained
tailings from 0.4' to 0.8', brownish
gray with some oxidation, olive
green from 0.4' to 0.8'

2013SC-SB-199-01

0" to 19.2" - Silty fine to coarse
SAND (SM), little fine to coarse
subangular Gravel, trace shell
fragments, possible fine grained
tailings from 0.4' to 0.8', brownish
gray with some oxidation, olive
green from 0.4' to 0.8'









SB-200

Short-core



55.623136

-132.556189

5/24/2013

8:45 AM

13

13

No sample

0" to 2". SILT

2" to 5". Silty SAND and Gravel,
65% fine Sand, 35% Gravel

No sample

5" to 8" - 60% Gravel, 30% Sand,
10% Silt, red brown, Sandy GRAVEL
8" to 12". gray brown coarse
SAND and GRAVEL









5" to 8" - very easily penetrated
No odor from soil core



SB-201

Short-core



55.623372

-132.555851

5/24/2013

9:00 AM

36

7

No sample

0" to 2 - brown Silty SAND with
Gravel

2 - 4" - brown to red Silty SAND
with some Gravel
4" - 6" - saturated 1 to 1.5-inch
Gravel

No sample

6 - 7" - saturated Gravel with Sand;
remainder of core lost









Based on nearby test pit, suspect that
lost core (7 to 36 ") consists of coarse
brown Sand with Gravel and some
fines (<10%)



SB-202

Test pit



55.623595

-132.555531

5/24/2013

9:15 AM

12

12

2013SC-SB-202-00
2013SC-SB-9202-00

0" to 6" - fine to coarse SAND,
some fine to coarse subangular
Gravel, little Silt, dark brownish
gray with some oxidation, wet

2013SC-SB-202-0.5

6" to 12" - fine to coarse SAND,
same as above, no oxidation, trace
angular Cobbles, wet









hand dug with shovel



SB-205

Short-core



55.623171

-132.552046

5/23/2013

9:34 AM

30

18.5

No sample

0" to 6" - fine SAND, dark gray
with thin laminations, moist

No sample

6" to 10" - fine SAND with trace
fines, micaceous, dark gray, wet
10" to 14" - same as above with
increased SILT/CLAY content

No sample

14" to 18.5" - Silty CLAY, dark gray,
wet, moderate stiff.

No sample



No debris



PAGE 5 OF 6


-------
TABLE 2-3

Short-core and Test Pit Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report	

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Advanced
(inches)

Core Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(Oto 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24+ inches)

Comments

Deviations

SB-207

Test pit

1.7

55.62394

-132.554563

5/25/2013

11:45AM

10.8

10.8

No sample

0" to 2.4". black fine SAND,
tailings

2.4" to 10.8" -black fine SAND
(tailings) with blobs of light gray
viscous Clay (gel-like)

No sample

10.8" - coarse SAND and GRAVEL,
wet









hand dug with shovel

Top 2 " - decayed marine odor

Gel-like material has no odor, dries
quickly when smeared



SB-208

Test pit

5.9

55.62514

-132.558005

5/27/2013

9:18 AM

24

24

No sample

0"to 10" -Tailings

No sample

10" to 14" - Light Clay

No sample

14" to 24" - Tailings

No sample

24" (bottom) - Light Grey
Clayey layer

Hand dug with shovel



SB-209

Test pit

6.7

55.625275

-132.558091

5/27/2013

9:20 AM

24

24

2013SC-SB-209-00

Dark gray silt, tailings with plastic
and debris

No sample

Dark gray silt, tailings with plastic
and debris

2013SC-SB-209-01

Same as above, 1-inch gray clay
layer at 13"

2013SC-SB-209-02

24 to 30" laminated gray
clay

30" sand (tailings) and gravel

Test pit on bank of unnamed stream

Added based on appearance
of stream bank

SB-220b

Short-core

9.5

55.625908

-132.557563

5/27/2013

2:10 PM

20.5

13.5

No sample

0" to 7.5" - fine SAND, trace Silt,
0" - 2" - brown, 2" - 7.5" - dark
grey. Poorly graded, wet. Clay
lens at 3", light grey.

No sample

7.5" to 9.5" - CLAY, light grey, wet,
thin laminations

9.5" to 11" - fine SAND, trace fines,
dark grey

No sample

11" to 13.5" - fine to medium
SAND, increased fine Sand content
at 13", dark grey, thin, light grey
Clay layer at 12.5"

No sample



Tailings; no debris

Duplicate location ID -this is
unsampled core

SB-222

Test pit

6.5

55.625161

-132.558251

5/30/2013

9:45 AM

6

6

2013SC-SB-222-00

black to dark brown SAND













Spoon sampled

added based on upland
tailings delineation

SB-223

Test pit

6.8

55.624708

-132.557969

5/30/2013

9:50 AM

6

6

2013SC-SB-223-00

brown to dark brown SAND













Spoon sampled

added based on upland
tailings delineation

Notes:

0 Number at the end of each Sample ID indicates the top of the sample interval. The first two intervals are 0.5 ft thick (0 to 0.5 ft and 0.5 to 1 ft), remaining intervals are 1 ft thick
MS/MSD = matrix spike/matrix spike duplicate

PAGE 6 OF 6


-------
TABLE 2-4

Deep Core Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Intervals
(feet)

Core
Recovered
(feet)

Sample IDa
(0 to 4 feet)

Sample Description
(0 to 4 feet)

Sample IDa
(4 to 8 feet)

Sample Description
(4 to 8 feet)

Sample IDa
(8 to 12 feet)

Sample Description
(8 to 12 feet)

Sample IDa
(12 to 16 feet)

Sample Description
(12 to 16 feet)

Sample IDa
(16 to 20 feet)

Sample Description
(16 to 20 feet)

Comments

Deviations

SB-301

Direct Push

8.414288

55.625936

-132.557955

8/30/2013

09:15 AM
Field

duplicates at
09:30 AM

0' to 2'
2' to 4'
4' to 7'

1.872.0'
1.272.0'
1.8'/3.0'

2013SC-SB-301-00

2013SC-SB-301-0.5

2013SC-SB-9301-.05

2013SC-SB-301-01

2013SC-SB-301-02

2013SC-SB-301-03

0" to 4": black CLAY

6": banded orange and

brown fine SAND

1' to 1.5': gray, laminated

SILT and CLAY with bands of

Sand

1.5' to 4': dark gray,
micaceous, SAND, dense,
moist

-per driller, loss is from
bottom of core, very wet
tailings

2013SC-SB-301-04

GRAVEL with SAND, gray
brown, 1-1/5" rounded rocks
and angular Gravel, wet 4 - 7
feet. Possible petroleum stain
and odor at top of gravel layer.













No odor

Refusal at 7 feet bgs
Native gravel at 4 feet bgs



SB-303

Direct Push

14.179021

55.625703

-132.557553

8/28/2013

10:45 AM
Field

duplicates at
11:00 AM

0' to 4'
4' to 8'
8' to 12'
12' to 16'
16' to 20'

3.2'/4.0'
3.0'/4.0'
4.0'/4.0'
2.0'/4.0'
2.4'/4.0'

2013SC-SB-303-00
2013SC-SB-303-0.5
2013SC-SB-303-01
2013SC-SB-303-02
2013SC-SB-303-03
2013-SC-SB-9303-03

0' to 3.2': very fine to fine
SAND (SP), olive green with
some oxidation banding,
moist, trace mica flakes
throughout, trace wood in
top 2 feet - tailings- trace
Silt

2013SC-SB-303-04
2013SC-SB-303-05
2013SC-SB-303-06
2013SC-SB-303-07

4' to 4.8': grayish brown very
fine SAND (SP), trace Silt, trace
Silt/Clay laminations, wet,
some oxidation
4.8' to 5.5': Silty very fine
SAND to SILT (SM/ML), wet,
gray, some light gray Silt
laminations throughout
5.5' to 6.0': dark green, very
fine to fine SAND (SP), trace
Silt, wet, trace mica (dark
green to black in places)
6' to 7': same as 5.5' to 6' with
few light gray Clay/Silt
laminations

2013-SC-SB-303-08

2013-SC-SB-303-09

2013SC-SB-9309-09

2013SC-SB-303-10

2013SC-SB-303-11

8' to 9.6': very fine
to fine SAND (SP),
some Silt, wet,
greenish gray to
dark gray, mica
flakes throughout
9.6'to 10.6':
SILT/CLAY (ML), wet,
medium gray, trace
fine dark gray Sand
10.6' to 12': dark
gray to black very
fine to fine SAND
(SP), trace light gray
Clay/Silt

laminations, wet

2013SC-SB-303-12
2013SC-SB-303-13
2013SC-SB-303-14
2013SC-SB-303-15

silty fine to coarse
SAND (SM), some
fine to medium
subangular Gravel,
wet, brown and
grayish brown, trace
shells, trace metallic
mica-like flakes from
13.9' to 14' (gold
colored)

-begin native
formation-

None

Silty fine to coarse SAND
(SM) and fine to coarse
subangular Gravel, wet,
grayish brown

Bottom of borehole at 20 feet
bgs

No odor



SB-304

Direct Push

10.539925

55.625432

-132.557437

8/28/2013

08:57 AM
Field

duplicates at
09:05 AM

0' to 4'
4' to 8'
8' to 12'
12' to 16'
16'to 20'

2.2'/4.0'
2.8'/4.0'
1.2'/4.0
1.3'/4.0'
0.5'/4.0'

2013SC-SB-304-00

2013SC-SB-9304-00

2013SC-SB-304-0.5

2013SC-SB-304-01

2013SC-SB-304-02

2013-SC-SB-304-03

0' to 0.8': very fine SAND
with some Silt (SP), wet,
greenish gray - tailings,
trace mica

0.8' to 1.4': SILT (ML),
laminated gray to light
grayish white, wet, trace
Clay

1.4' to 2.2': very fine to fine
SAND (SP), trace Silt, wet,
greenish gray with trace
mica - tailings, increased
Silt from 2.0' to 2.2' (same
as 0.8' to 1.4' interval): no
petroleum or naphthalene
odor

2013SC-SB-304-04 +
MS/MSD

2013SC-SB-304-05
2013SC-SB-304-06
2013SC-SB-304-07

4' to 6.8': very fine to fine
SAND (SP), some Silt, Silt/Clay
interbeds throughout ~1"
thick beds, sand is greenish
gray with trace mica, Silt/Clay
layers are light gray to gray,
wet: no petroleum or
naphthalene odor

2013SC-SB-304-08
2013SC-SB-304-09
2013SC-SB-304-10
2013SC-SB-304-11
2013SC-SB-9304-11

8' to 8.4': very fine
SAND (SP), trace Silt,
wet, dark greenish
gray - tailings
8.4' to 8.8': dark
brown Silty fine to
coarse SAND and
fine subangular
GRAVEL, wet, trace
shells (SM)
8.8' to 9.2': light
gray Shell Hash with
fine SAND with Silt,
trace coarse
subangular Gravel

2013SC-SB-304-12
2013SC-SB-304-13

fine to coarse SAND
(SW), some fine
subangular Gravel,
wet, dark gray, little
Silt - native material

None

Same as 12' to 16' interval

Bottom of borehole at 20 feet
bgs

No odor

Native material ~ 9 feet bgs



SB-305

Direct Push

9.36182

55.625098

-132.557307

8/27/2013

2:00 PM
Field

duplicates at
2:30 PM

0' to 2'
2'to 6'
6' to 10'
10'to 12'

1.5'/2.0'
3.5'/4.0'
3.9'/4.0'
0.5'/2.0'

2013SC-SB-305-00
2013SC-SB-305-0.5 +
MS/MSD

2013SC-SB-305-01
2013SC-SB-305-02
2013SC-SB-305-03
2013SC-SB-9305-03

0' to 2': very fine SAND (SP)
with trace Silt, greenish gray
with trace mica flecks, trace
medium gray Silt, wet,
tailings

2' to 4': very fine SAND with
trace Silt as above (SP), wet,
tailings, increasing Silt from
3.4' to 4', trace light gray
Silt

2013SC-SB-305-04
2013SC-SB-305-05
2013SC-SB-305-06
2013SC-SB-305-07

4' to 4.6': coarser (medium)
SAND, with trace Silt, and
trace mica, wet greenish gray
(olivine colored)

4.6' to 5.5': SILT with trace
Clay (ML), gray with a slight
greenish hue, wet, trace light
gray Clay

5.5' to 6': no recovery

6' to 7.4': greenish gray very
fine to fine SAND (SP) with
trace Silt, wet, trace mica
flakes, tailings
7.4' to 8.4': light to medium
gray SILT (ML), trace Clay,
trace black organics, trace
tailings - green fine sand-, low
plasticity, wet

2013SC-SB-305-08
2013SC-SB-305-09
2013SC-SB-9305-09
2013SC-SB-305-10

8.4' to 9.9': fine to
coarse SAND (SW),
trace fine
subangular Gravel,
medium brown,
trace Silt, wet, shell
hash from 9.5' to
9.9' - native material

10' to 10.5': light
gray shell hash, shell
particles and trace
Silt, wet, trace very
fine Sand









Bottom of tailings at ~8.4 feet
No odor

Bottom of hole at 12 feet bgs



PAGE 1 OF 3


-------
TABLE 2-4

Deep Core Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Intervals
(feet)

Core
Recovered
(feet)

Sample IDa
(0 to 4 feet)

Sample Description
(0 to 4 feet)

Sample IDa
(4 to 8 feet)

Sample Description
(4 to 8 feet)

Sample IDa
(8 to 12 feet)

Sample Description
(8 to 12 feet)

Sample IDa
(12 to 16 feet)

Sample Description
(12 to 16 feet)

Sample IDa
(16 to 20 feet)

Sample Description
(16 to 20 feet)

Comments

Deviations

SB-306

Direct Push
(PAH

delineation)

8.205701

55.625863

-132.556602

8/29/2013

09:15 AM
Field

duplicates at
09:40 AM

0' to 4'
4' to 6'
6' to 8'
8' to 12'

2.174.0'
1.372.0'
0.972.01
2.574.01

2013SC-SB-306-00

2013SC-SB-306-0.5

2013SC-SB-9306-0.5

2013SC-SB-306-01

2013SC-SB-306-02

2013SC-SB-306-03

0' to 1.7': dark olive green
to black, very fine SAND
(SP), little Silt, wet, trace
organics, soft
1.7' to 2.1': Silty fine to
coarse SAND and fine
subangular Gravel (SM),
medium gray, wet, loose;
petroleum odor from 0 to 4
ft.

2013SC-SB-306-04
2013SC-SB-306-05
2013SC-SB-306-06
2013SC-SB-306-07 +
MS/MSD for PAH only

4' to 5.3': brownish gray fine
to coarse SAND and SILT (SM),
slightly dense, wet; petroleum
odor.

6' to 6.9': Same as above -
native material

None

8' to 10.5': brownish
gray to olive gray
Silty fine to coarse
SAND with some
Gravel (fine to
coarse subangular)
grading to mostly
Gravel at ~9.8' bgs,
wet, loose (SM/GM)









Petroleum like odor from 0' to 4'
interval

No noticeable odor through rest
of core

PAH sample from native material
at 7' to 8'

Bottom of borehole at 12 feet
bgs



SB-307

Direct Push

9.258244

55.62543

-132.555388

8/29/2013

10:30 AM
Field

duplicates at
11:00 AM

0' to 4'
4' to 8'
8' to 10'

2.074.01
4.074.01
1.672.0'

2013SC-SB-307-00

2013SC-SB-307-0.5

2013SC-SB-307-01

2013SC-SB-9307-01

2013SC-SB-307-02

2013SC-SB-307-03

0' to 2': olive gray very fine
to fine SAND, trace Silt, wet,
loose, trace mica flakes (SP)

2013SC-SB-307-04
2013SC-SB-307-05
2013SC-SB-307-06
2013SC-SB-307-07

4' to 6.5': olive gray very fine
SAND, some Silt (SP/SM), wet,
trace mica, becoming siltier
toward 6.5 feet
6.5' to 7.4': gray to light gray
thinly laminated SILT/CLAY
(ML/CL), soft to medium stiff,
wet

7.4' to 8.0': dark gray to black
very fine to fine SAND (SP),
trace Silt < 5%, trace mica
flakes; black staining with
"piney" odor 7 to 9 ft.

2013SC-SB-307-08
2013SC-SB-307-8.5
2013SC-SB-307-09

8' to 9.6': fine to
coarse SAND and
SILT (SM), some fine
to coarse subangular
Gravel, gravel
increases from 8.7'
to 9.6', color
changes from
black/dark gray at 8'
to 8.4' to dark
grayish brown from
8.4' to 9' then light
gray from 9' to 9.6',
trace organics from
8' to 9', shell
fragments
throughout,
abundant shells
from 9' to 9.6', wet,
medium dense;
black staining with
"piney" odor to 8 ft
-native material at
~9' bgs









No noticeable odor

Bottom of borehole at 12 feet
bgs; sampled and logged to 10
feet bgs



SB-308

Direct Push

11.879741

55.625642

-132.55527

8/29/2013

1:15 PM
Field

duplicates at
1:30 PM

0' to 4'
4' to 8'
8'to 9.5'

2.6'/4.0'
2.0'/4.0'
1.5'/1.5'

2013SC-SB-308-00

2013SC-SB-308-0.5

2013SC-SB-9308-0.5

2013SC-SB-308-01

2013SC-SB-308-02

2013SC-SB-308-03

very fine to fine SAND (SP),
moist to wet, loose to
medium dense,
greenish/olive gray, trace
mica, trace Silt

2013SC-SB-308-04
2013SC-SB-308-05
2013SC-SB-308-06
2013SC-SB-308-07

fine to medium fine SAND
(SP), trace mica, trace Silt, wet,
medium dense, olive gray to
dark olive gray, light to
medium gray at 6 feet bgs

2013SC-SB-308-08

+MS/MSD

2013SC-SB-308-09

8' to 9.5': brownish
gray Silty fine to
coarse SAND (SM),
some fine to coarse
subangular to
subrounded Gravel,
wet, loose
-native formation-









No noticeable odor

Bottom of borehole at 9.5 feet
bgs on rock



SB-309

Direct Push
(PAH

delineation)

7.868355

55.625674

-132.557014

8/28/2013



0' to 4'
4' to 8'



None

0 to 2 ft: black stained,
moderate chemical odor,
not distinctly petroleum or
naphthalene, 2 - 4 ft
tailings, no odor

None

tailings, gravel at 8 feet

















SB-310

Direct Push
(PAH

delineation)

7.158964

55.625543

-132.556935

8/28/2013



0' to 4'



None

0 to 2 ft: black stained,
moderate chemical odor,
not distinctly petroleum or
naphthalene, 2 - 4 ft
tailings, no odor





















SB-311

Direct Push
(PAH

delineation)

7.258086

55.625382

-132.55669

8/28/2013



0' to 4'



None

0 to 2.5 ft degraded organic
(fishy) odor; 2.5 ft degraded
petroleum odor





















SB-312

Direct Push
(PAH

delineation)

6.472287

55.62526

-132.55644

8/28/2013



0' to 4'



None

0 to 3.5 feet tailings, no
petroleum or naphthalene
odor. 3.5 to 4 feet dark
staining and petroleum
odor.





















SB-313

Direct Push
(PAH

delineation)

6.334189

55.625113

-132.556338

8/28/2013

2:40 PM

0' to 4'
4' to 8'

2.0'/4.0'
1.2'/4.0'

2013SC-SB-313-02
2013SC-SB-313-03

0' to 1.5': very fine SAND
(SP), some Silt, wet, olive
green with light gray Silt
laminations - few
laminations;

1.5' to 2.0': dark green to
black very fine to fine SAND
(SP), trace Silt, trace mica,
wet (coarser than 0' to
1.5'); no petroleum or
naphthalene odor

2013SC-SB-313-04 (no
results, CLP lab ID
issue)

4' to 4.2': SILT and decayed
organics (ML), light gray to
black, soft, wet; no petroleum
or naphthalene odor
4.2' to 5.2': dark brown silty
fine to coarse SAND (SM), wet,
some fine subangular Gravel,
trace shell fragments and
organics. Likely native
material. Possible petroleum
odor at 4 to 5 ft













Bottom of PAH delineation
boring at 8 feet bgs.

No odor

Duplicated CLP
sample ID issue. See
text.

PAGE 2 OF 3


-------
TABLE 2-4

Deep Core Sample Information - Marine Sediment Core Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Core Intervals
(feet)

Core
Recovered
(feet)

Sample IDa
(0 to 4 feet)

Sample Description
(0 to 4 feet)

Sample IDa
(4 to 8 feet)

Sample Description
(4 to 8 feet)

Sample IDa
(8 to 12 feet)

Sample Description
(8 to 12 feet)

Sample IDa
(12 to 16 feet)

Sample Description
(12 to 16 feet)

Sample IDa
(16 to 20 feet)

Sample Description
(16 to 20 feet)

Comments

Deviations

SB-314

Direct Push
(PAH

delineation)

9.043253

55.625417

-132.556991

8/28/2013





0' to 4'
4' to 8'

None

Tailings, no petroleum or
naphthalene odor

None

Tailings; strong petroleum
odor at 5 to 6 ft.

















SB-315

Direct Push
(PAH

delineation)

11.066621

55.62549

-132.557208

8/28/2013





0' to 4'
4' to 8'

None

Tailings, no petroleum or
naphthalene odor

None

Tailings; strong petroleum
odor at 6 to 8 ft.

















SB-316

Direct Push
(PAH

delineation)

10.970952

55.625453

-132.557323

8/28/2013

4:30 PM

0' to 4'
4' to 8'

2.074.0'
3.674.0'

None

0' to 1.3': medium to light
gray SILT/CLAY, some
oxidized laminations, trace
very fine Sand, wet, soft
(ML/CL)

1.3' to 2.0': very fine to fine
SAND (SP), trace Silt, wet,
dark olive green, trace mica;
no petroleum or
naphthalene odor

2013SC-SB-316-06 +
MS/MSD

2013SC-SB-316-07

4' to 7': light gray, wet, soft
SILT (ML), little possible Clay,
trace fine Sand 6.4' to 6.6'
7' to 7.6': very fine to fine dark
olive green to black SAND (SP),
trace Silt, wet, trace light gray
Silt laminations at 7.5' to 7.6';
possible petroleum odor at 7 -
8 ft.













Bottom of PAH delineation
borehole at 8 feet bgs.

No noticeable odor

Duplicated CLP
sample ID issue. See
text.

SB-317

Direct Push
(PAH

delineation)

5.570826

55.625397

-132.556198

8/29/2013



0' to 4'
4' to 8'



None

Black stained tailings with
clayey beds, slight
petroleum odor

None

Gravel; strong petroleum odor
and dark staining

















SB-318

Direct Push
(PAH

delineation)

5.672883

55.625284

-132.555767

8/29/2013



0' to 4'
4' to 8'



None

Black stained tailings at 3 to
4 ft; petroleum odor.

None

Soft clay to 5 ft; petroleum
odor. Gravel 5 to 8 ft
petroleum odor.

















SB-319

Direct Push
(PAH

delineation)

4.973153

55.625063

-132.55545

8/29/2013

4:00 PM

0' to 4'
4' to 8'

1.8'/4.0'
2.1'/4.0'

None

very fine to fine SAND (SP),
little Silt in think
laminations, olive green to
dark gray, wet,
soft/medium dense, silt
laminations are light gray;
no petroleum or
naphthalene odor

2013SC-SB-319-04

4' to 5': Silty fine to coarse
SAND and fine subangular
GRAVEL (SM), trace organics
and shells, wet, medium
dense, black stained with
petroleum odor.

5' to 6.1': organic
soil/decomposed wood,
brown, soft, wet, some shells
and wood debris.

Likely native material 5' to 6.1'













Petroleum like odor from 4' to 8'
sample interval

Bottom of borehole at 8 feet bgs



SB-320

Direct Push
(PAH

delineation)

4.74279

55.624838

-132.555072

8/29/2013



0' to 4'
4' to 8'



None

Tailings and woody debris;
no petroleum or
naphthalene odor

None

Clay with silt, gray, petroleum
odor

















SB-321

Direct Push
(PAH

delineation)

8.63726

55.625733

-132.556123

8/29/2013



0' to 4'
4' to 8'



None

Tailings, no petroleum or
naphthalene odor

None

Tailings to 4.5 feet; no
petroleum or naphthalene
odor; Gravel 4.5 to 8 feet,
black stained with petroleum
odor 4.5 to 5 feet; no stain or
odor 5 to 7 feet.

















SB-322

Direct Push
(PAH

delineation)

11.637403

55.626135

-132.55744

8/30/2013

11:00 AM

0' to 4'
4' to 6'

not recorded

2013SC-SB-322-02
(no results, CLP lab
ID issue)

2013SC-SB-322-03

0' to 3': fine SAND, dark
gray, micaceous, moist
-tailings; no petroleum or
naphthalene odor.
3 to 4 feet GRAVEL, black
stained with petroleum
odor.

2013SC-SB-322-04

4 to 6 ft GRAVEL, mottled
orange and gray with black
staining and petroleum odor,
rounded pebbles and angular
gravel, moist













Chemical and petroleum odor
from 3' to 6.5'

Refusal at 6.5 feet bgs

Duplicated CLP
sample ID issue. See
text.

SB-323

Direct Push
(PAH

delineation)

9.949631

55.626023

-132.557466

8/30/2013



0' to 4'
4' to 6.5'



None

Tailings to 4 ft; slight
petroleum odor at 3.75
feet.

None

4-6.5 feet GRAVEL, dark
stained with sweet chemical
odor. Refusal at 6.5 feet.

















SB-324

Direct Push
(PAH

delineation)

8.762872

55.626073

-132.557674

8/30/2013



0' to 4'
4' to 5'



None

Tailings to 2.5 ft; Black
stained gravel 3- 4 feet with
degraded petroleum odor

None

Gravel and sand; mottled
orange and gray, slight
petroleum odor.

















Notes:

0 Number at the end of each Sample ID indicates the top of the sample interval. The first two intervals are 0.5 ft thick (0 to 0.5 ft and 0.5 to 1 ft), remaining intervals are 1 ft thick
PAHs = polycyclic aromatic hydrocarbons
MS/MSD = matrix spike/matrix spike duplicate

PAGE 3 OF 3


-------
TABLE 2-5

Marine Sediment Core and Test Pit Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Activity ID

Sample
Type

Depth
(feet)

Sample Date

Analytical Suite and Laboratory

Cr-VI
(Manchester
Environmental
Laboratory)

Mercury
(A4 Scientific)

TAL Metals3
(A4 Scientific)

Modified SPLPb
(Manchester
Environmental
Laboratory)

PAHs
(KAP
Technologies)

Total Organic

Carbon
(Manchester
Environmental
Laboratory)

Bulk Density
(Applied Sciences
Laboratory)

Grain Size
(Applied Sciences
Laboratory)

SB-004

2013SC-SB-004-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-004

2013SC-SB-004-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-004

2013SC-SB-9004-0.5-20130528FD

FD

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-013

2013SC-SB-013-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-013

2013SC-SB-013-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-018

2013SC-SB-018-00-20130527

N

LO

o
o

5/27/2013



X

X











SB-018

2013SC-SB-018-0.5-20130527

N

0.5 - 1

5/27/2013



X

X











SB-021

2013SC-SB-021-00-20130528

N

LO

o
o

5/28/2013



X

X



X

X





SB-021

2013SC-SB-021-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-031

2013SC-SB-031-00-20130528

N

LO

o
o

5/28/2013



X

X











SB-031

2013SC-SB-9031-00-20130528FD

FD

LO

o
o

5/28/2013



X

X











SB-031

2013SC-SB-031-0.5-20130528

N

0.5 - 1

5/28/2013



X

X











SB-031

2013SC-SB-031-01-20130528

N

1 - 2

5/28/2013



X

X











SB-032

2013SC-SB-032-00-20130527

N

LO

o
o

5/27/2013



X

X

X

X

X

X

X

SB-032

2013SC-SB-032-0.5-20130527

N

0.5 - 1

5/27/2013



X

X

X

X

X

X

X

SB-033

2013SC-SB-033-00-20130527

N

LO

o
o

5/27/2013



X

X

X

X

X

X

X

SB-033

2013SC-SB-033-0.5-20130527

N

0.5 - 1

5/27/2013



X

X

X

X

X

X

X

SB-043

2013SC-SB-043-00-20130527

N

LO

o
o

5/27/2013



X

X











SB-043

2013SC-SB-043-0.5-20130527

N

0.5 - 1

5/27/2013



X

X











SB-043

2013SC-SB-043-01-20130527

N

1 - 2

5/27/2013



X

X











SB-052

2013SC-SB-052-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-052

2013SC-SB-052-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-052

2013SC-SB-052-01-20130528

N

1 - 2

5/28/2013



X

X

X

X







SB-059

2013SC-SB-059-00-20130527

N

LO

o
o

5/27/2013

X

X

X

X

X

X

X

X

SB-059

2013SC-SB-059-0.5-20130527

N

0.5 - 1

5/27/2013



X

X

X

X

X



X

SB-059

2013SC-SB-059-01-20130527

N

1 - 2

5/27/2013



X

X

X

X

X



X

SB-061

2013SC-SB-061-00-20130527

N

LO

o
o

5/27/2013

X

X

X





X

X

X

SB-061

2013SC-SB-061-0.5-20130527

N

0.5 - 1

5/27/2013



X

X











SB-062

2013SC-SB-062-00-20130528

N

LO

o
o

5/28/2013

X

X

X

X

X

X

X

X

SB-062

2013SC-SB-062-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-062

2013SC-SB-062-01-20130528

N

1 - 2

5/28/2013



X

X

X

X

X

X

X

SB-078

2013SC-SB-078-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-078

2013SC-SB-078-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-078

2013SC-SB-078-01-20130528

N

1 - 2

5/28/2013



X

X

X

X

X

X

X

SB-079

2013SC-SB-079-00-20130528

N

LO

o
o

5/28/2013

X

X

X

X

X

X

X

X

SB-079

2013SC-SB-079-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-079

2013SC-SB-079-01-20130528

N

1 - 2

5/28/2013



X

X

X

X

X

X

X

SB-082

2013SC-SB-082-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-082

2013SC-SB-082-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-082

2013SC-SB-082-01-20130528

N

1 - 2

5/28/2013



X

X

X

X

X

X

X

SB-089

2013SC-SB-089-00-20130528

N

LO

o
o

5/28/2013



X

X

X

X

X

X

X

SB-089

2013SC-SB-089-0.5-20130528

N

0.5 - 1

5/28/2013



X

X

X

X

X

X

X

SB-089

2013SC-SB-089-01-20130528

N

1 - 2

5/28/2013



X

X

X

X

X

X

X

SB-Ill

2013SC-SB-111-00-20130523

N

LO

o
o

5/23/2013



X

X











SB-Ill

2013SC-SB-111-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-Ill

2013SC-SB-111-01-20130523

N

1 - 2

5/23/2013



X

X











SB-115

2013SC-SB-115-00-20130522

N

LO

o
o

5/22/2013

X

X

X





X

X

X

PAGE 1 OF 5


-------
TABLE 2-5

Marine Sediment Core and Test Pit Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Activity ID

Sample
Type

Depth
(feet)

Sample Date

Analytical Suite and Laboratory

Cr-VI
(Manchester
Environmental
Laboratory)

Mercury
(A4 Scientific)

TAL Metals3
(A4 Scientific)

Modified SPLPb
(Manchester
Environmental
Laboratory)

PAHs
(KAP
Technologies)

Total Organic

Carbon
(Manchester
Environmental
Laboratory)

Bulk Density
(Applied Sciences
Laboratory)

Grain Size
(Applied Sciences
Laboratory)

SB-115

2013SC-SB-9115-00-20130522FD

FD

LO

o
o

5/22/2013

X

X

X











SB-115

2013SC-SB-115-0.5-20130522

N

0.5 - 1

5/22/2013



X

X











SB-115

2013SC-SB-115-01-20130522

N

1 - 2

5/22/2013



X

X











SB-115

2013SC-SB-115-02-20130522

N

2 - 3

5/22/2013



X

X











SB-117

2013SC-SB-117-00-20130524

N

0 - 0.5

5/24/2013



X

X











SB-117

2013SC-SB-117-0.5-20130524

N

0.5 - 1

5/24/2013



X

X











SB-117

2013SC-SB-117-01-20130524

N

1 - 2

5/24/2013



X

X











SB-121

2013SC-SB-121-00-20130523

N

0 - 0.5

5/23/2013



X

X











SB-121

2013SC-SB-121-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-121

2013SC-SB-121-01-20130523

N

1 - 2

5/23/2013



X

X











SB-123

2013SC-SB-123-00-20130523

N

0 - 0.5

5/23/2013



X

X











SB-123

2013SC-SB-9123-00-20130523FD

FD

0 - 0.5

5/23/2013



X

X











SB-123

2013SC-SB-123-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-123

2013SC-SB-123-01-20130523

N

1 - 2

5/23/2013



X

X











SB-123

2013SC-SB-123-02-20130523

N

2 - 2.5

5/23/2013



X

X











SB-127

2013SC-SB-127-00-20130522

N

0 - 0.5

5/22/2013



X

X











SB-127

2013SC-SB-127-0.5-20130522

N

0.5 - 1

5/22/2013



X

X











SB-127

2013SC-SB-127-01-20130522

N

1 - 1.5

5/22/2013



X

X











SB-129

2013SC-SB-129-00-20130523

N

0 - 0.5

5/23/2013

X

X

X





X

X

X

SB-129

2013SC-SB-9129-00-20130523FD

FD

0 - 0.5

5/23/2013



X

X





X

X

X

SB-129

2013SC-SB-129-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-129

2013SC-SB-129-01-20130523

N

1 - 2

5/23/2013



X

X











SB-133

2013SC-SB-133-00-20130522

N

LO

o
o

5/22/2013



X

X











SB-133

2013SC-SB-133-0.5-20130522

N

0.5 - 1

5/22/2013



X

X











SB-133

2013SC-SB-133-01-20130522

N

1 - 2

5/22/2013



X

X











SB-133

2013SC-SB-9133-01-20130522FD

FD

1 - 2

5/22/2013



X

X











SB-133

2013SC-SB-133-02-20130522

N

2 - 3

5/22/2013



X

X











SB-157

2013SC-SB-157-00-20130525

N

LO

o
o

5/25/2013



X

X











SB-157

2013SC-SB-157-0.5-20130525

N

0.5 - 1

5/25/2013



X

X











SB-157

2013SC-SB-157-01-20130525

N

1 - 2

5/25/2013



X

X











SB-157

2013SC-SB-157-02-20130525

N

2 - 2.3

5/25/2013



X

X











SB-176

2013SC-SB-176-00-20130530

N

LO

o
o

5/30/2013



X

X











SB-177

2013SC-SB-177-0.5-20130530

N

0.5 - 1

5/30/2013



X

X











SB-191

2013SC-SB-191-00-20130523

N

LO

o
o

5/23/2013



X

X











SB-191

2013SC-SB-191-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-191

2013SC-SB-191-01-20130523

N

1 - 2

5/23/2013



X

X











SB-192

2013SC-SB-192-00-20130523

N

LO

o
o

5/23/2013



X

X





X

X

X

SB-192

2013SC-SB-192-0.5-20130523

N

0.5 - 1

5/23/2013



X

X











SB-192

2013SC-SB-192-01-20130523

N

1 - 2

5/23/2013



X

X











SB-192

2013SC-SB-192-02-20130523

N

2 - 2.4

5/23/2013



X

X











SB-196

2013SC-SB-196-00-20130524

N

LO

o
o

5/24/2013



X

X











SB-196

2013SC-SB-196-0.5-20130524

N

0.5 - 1

5/24/2013



X

X











SB-197

2013SC-SB-197-00-20130524

N

LO

o
o

5/24/2013



X

X











SB-197

2013SC-SB-197-0.5-20130524

N

0.5 - 1

5/24/2013



X

X











SB-197

2013SC-SB-197-01-20130524

N

1 - 2

5/24/2013



X

X











SB-199

2013SC-SB-199-00-20130524

N

LO

o
o

5/24/2013



X

X











SB-199

2013SC-SB-199-0.5-20130524

N

0.5 - 1

5/24/2013



X

X











PAGE 2 OF 5


-------
TABLE 2-5

Marine Sediment Core and Test Pit Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Activity ID

Sample
Type

Depth
(feet)

Sample Date

Analytical Suite and Laboratory

Cr-VI
(Manchester
Environmental
Laboratory)

Mercury
(A4 Scientific)

TAL Metals a
(A4 Scientific)

Modified SPLPb
(Manchester
Environmental
Laboratory)

PAHs
(KAP
Technologies)

Total Organic

Carbon
(Manchester
Environmental
Laboratory)

Bulk Density
(Applied Sciences
Laboratory)

Grain Size
(Applied Sciences
Laboratory)

SB-199

2013SC-SB-199-01-20130524

N

1 - 2

5/24/2013



X

X











SB-202

2013SC-SB-202-00-20130524

N

0 - 0.5

5/24/2013



X

X





X

X

X

SB-202

2013SC-SB-9202-00-20130524FD

FD

0 - 0.5

5/24/2013



X

X











SB-202

2013SC-SB-202-0.5-20130524

N

0.5 - 1

5/24/2013



X

X











SB-209

2013SC-SB-209-00-20130527

N

0 - 0.5

5/27/2013



X

X



X







SB-209

2013SC-SB-209-01-20130527

N

1 - 1.5

5/27/2013



X

X



X







SB-209

2013SC-SB-209-02-20130527

N

2 - 2.5

5/27/2013



X

X



X





X

SB-222

2013SC-SB-222-00-20130530

N

0 - 0.5

5/30/2013



X

X











SB-223

2013SC-SB-223-0.5-20130530

N

0.5 - 1

5/30/2013



X

X











SB-301

2013SC-SB-301-00-20130830

N

0 - 0.5

8/30/2013



X

X











SB-301

2013SC-SB-301-0.5-20130830

N

0.5 - 1

8/30/2013



X

X











SB-301

2013SC-SB-9301-0.5-20130830FD

FD

0.5 - 1

8/30/2013



X

X











SB-301

2013SC-SB-301-01-20130830

N

1 - 2

8/30/2013



X

X











SB-301

2013SC-SB-301-02-20130830

N

2 - 3

8/30/2013



X

X











SB-301

2013SC-SB-301-03-20130830

N

3 - 4

8/30/2013



X

X











SB-301

2013SC-SB-301-04-20130830

N

4 - 5

8/30/2013



X

X











SB-303

2013SC-SB-303-00-20130828

N

0 - 0.5

8/28/2013



X

X











SB-303

2013SC-SB-303-0.5-20130828

N

0.5 - 1

8/28/2013



X

X











SB-303

2013SC-SB-303-01-20130828

N

1 - 2

8/28/2013



X

X











SB-303

2013SC-SB-303-02-20130828

N

2 - 3

8/28/2013



X

X











SB-303

2013SC-SB-303-03-20130828

N

3 - 4

8/28/2013



X

X











SB-303

2013SC-SB-9303-03-20130828FD

FD

3 - 4

8/28/2013



X

X











SB-303

2013SC-SB-303-04-20130828

N

4 - 5

8/28/2013



X

X











SB-303

2013SC-SB-303-05-20130828

N

5 - 6

8/28/2013



X

X











SB-303

2013SC-SB-303-06-20130828

N

6 - 7

8/28/2013



X

X











SB-303

2013SC-SB-303-07-20130828

N

7 - 8

8/28/2013



X

X











SB-303

2013SC-SB-303-08-20130828

N

8 - 9

8/28/2013



X

X











SB-303

2013SC-SB-303-09-20130828

N

9 - 10

8/28/2013



X

X











SB-303

2013SC-SB-9303-09-20130828

FD

9 - 10

8/28/2013



X

X











SB-303

2013SC-SB-303-10-20130828

N

10 - 11

8/28/2013



X

X











SB-303

2013SC-SB-303-11-20130828

N

11 - 12

8/28/2013



X

X











SB-303

2013SC-SB-303-12-20130828

N

12 - 13

8/28/2013



X

X











SB-303

2013SC-SB-303-13-20130828

N

13 - 14

8/28/2013



X

X











SB-303

2013SC-SB-303-14-20130828

N

14 - 15

8/28/2013



X

X











SB-303

2013SC-SB-303-15-20130828

N

15 - 16

8/28/2013



X

X











SB-304

2013SC-SB-304-00-20130828

N

0 - 0.5

8/28/2013



X

X











SB-304

2013SC-SB-9304-00-20130828FD

FD

0 - 0.5

8/28/2013



X

X











SB-304

2013SC-SB-304-0.5-20130828

N

0.5 - 1

8/28/2013



X

X











SB-304

2013SC-SB-304-01-20130828

N

1 - 2

8/28/2013



X

X











SB-304

2013SC-SB-304-02-20130828

N

2 - 3

8/28/2013



X

X











SB-304

2013SC-SB-304-03-20130828

N

3 - 4

8/28/2013



X

X











SB-304

2013SC-SB-304-04-20130828

N

4 - 5

8/28/2013



X

X











SB-304

2013SC-SB-304-05-20130828

N

5 - 6

8/28/2013



X

X











SB-304

2013SC-SB-304-06-20130828

N

6 - 7

8/28/2013



X

X











SB-304

2013SC-SB-304-07-20130828

N

7 - 8

8/28/2013



X

X











SB-304

2013SC-SB-304-08-20130828

N

8 - 9

8/28/2013



X

X











SB-304

2013SC-SB-304-09-20130828

N

9 - 10

8/28/2013



X

X











PAGE 3 OF 5


-------
TABLE 2-5

Marine Sediment Core and Test Pit Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Activity ID

Sample
Type

Depth
(feet)

Sample Date

Analytical Suite and Laboratory

Cr-VI
(Manchester
Environmental
Laboratory)

Mercury
(A4 Scientific)

TAL Metals a
(A4 Scientific)

Modified SPLPb
(Manchester
Environmental
Laboratory)

PAHs
(KAP
Technologies)

Total Organic

Carbon
(Manchester
Environmental
Laboratory)

Bulk Density
(Applied Sciences
Laboratory)

Grain Size
(Applied Sciences
Laboratory)

SB-304

2013SC-SB-304-10-20130828

N

10 - 11

8/28/2013



X

X











SB-304

2013SC-SB-304-11-20130828

N

11 - 12

8/28/2013



X

X











SB-304

2013SC-SB-9304-11-20130828FD

FD

11 - 12

8/28/2013



X

X











SB-304

2013SC-SB-304-12-20130828

N

12 - 13

8/28/2013



X

X











SB-304

2013SC-SB-304-13-20130828

N

13 - 14

8/28/2013



X

X











SB-305

2013SC-SB-305-00-20130827

N

0 - 0.5

8/27/2013



X

X











SB-305

2013SC-SB-305-0.5-20130827

N

0.5 - 1

8/27/2013



X

X











SB-305

2013SC-SB-305-01-20130827

N

1 - 2

8/27/2013



X

X











SB-305

2013SC-SB-305-02-20130827

N

2 - 3

8/27/2013



X

X











SB-305

2013SC-SB-305-03-20130827

N

3 - 4

8/27/2013



X

X











SB-305

2013SC-SB-9305-03-20130827FD

FD

3 - 4

8/27/2013



X

X











SB-305

2013SC-SB-305-04-20130827

N

4 - 5

8/27/2013



X

X











SB-305

2013SC-SB-305-05-20130827

N

5 - 6

8/27/2013



X

X











SB-305

2013SC-SB-305-06-20130827

N

6 - 7

8/27/2013



X

X











SB-305

2013SC-SB-305-07-20130827

N

7 - 8

8/27/2013



X

X











SB-305

2013SC-SB-305-08-20130827

N

8 - 9

8/27/2013



X

X











SB-305

2013SC-SB-305-09-20130827

N

9 - 10

8/27/2013



X

X











SB-305

2013SC-SB-9305-09-20130827FD

FD

9 - 10

8/27/2013



X

X











SB-305

2013SC-SB-305-10-20130827

N

10 - 10.5

8/27/2013



X

X











SB-306

2013SC-SB-306-00-20130829

N

0 - 0.5

8/29/2013



X

X



X







SB-306

2013SC-SB-306-0.5-20130829

N

0.5 - 1

8/29/2013



X

X



X







SB-306

2013SC-SB-306-20130829FD

FD

0.5 - 1

8/29/2013









X







SB-306

2013SC-SB-306-01-20130829

N

1 - 2

8/29/2013



X

X



X







SB-306

2013SC-SB-306-02-20130829

N

2 - 3

8/29/2013









X







SB-306

2013SC-SB-306-03-20130829

N

3 - 4

8/29/2013









X







SB-306

2013SC-SB-306-04-20130829

N

4 - 5

8/29/2013



X

X











SB-306

2013SC-SB-306-05-20130829

N

5 - 6

8/29/2013



X

X











SB-306

2013SC-SB-306-06-20130829

N

6 - 7

8/29/2013



X

X











SB-306

2013SC-SB-306-07-20130829

N

7 - 8

8/29/2013



X

X



X







SB-307

2013SC-SB-307-00-20130829

N

0 - 0.5

8/29/2013



X

X











SB-307

2013SC-SB-307-0.5-20130829

N

0.5 - 1

8/29/2013



X

X











SB-307

2013SC-SB-307-01-20130829

N

1 - 2

8/29/2013



X

X











SB-307

2013SC-SB-9307-01-20130829FD

FD

1 - 2

8/29/2013



X

X











SB-307

2013SC-SB-307-02-20130829

N

2 - 3

8/29/2013



X

X











SB-307

2013SC-SB-307-03-20130829

N

3 - 4

8/29/2013



X

X











SB-307

2013SC-SB-307-04-20130829

N

4 - 5

8/29/2013



X

X











SB-307

2013SC-SB-307-05-20130829

N

5 - 6

8/29/2013



X

X











SB-307

2013SC-SB-307-06-20130829

N

6 - 7

8/29/2013



X

X











SB-307

2013SC-SB-307-07-20130829

N

7 - 8

8/29/2013



X

X











SB-307

2013SC-SB-307-08-20130829

N

8 - 9

8/29/2013



X

X











SB-307

2013SC-SB-307-8.5-20130829

N

8.5 - 9

8/29/2013









X







SB-307

2013SC-SB-307-09-20130829

N

9 - 10

8/29/2013



X

X











SB-308

2013SC-SB-308-00-20130829

N

0 - 0.5

8/29/2013



X

X











SB-308

2013SC-SB-308-0.5-20130829

N

0.5 - 1

8/29/2013



X

X











SB-308

2013SC-SB-9308-0.5-20130829FD

FD

0.5 - 1

8/29/2013



X

X











SB-308

2013SC-SB-308-01-20130829

N

1 - 2

8/29/2013



X

X











SB-308

2013SC-SB-308-02-20130829

N

2 - 3

8/29/2013



X

X











PAGE 4 OF 5


-------
TABLE 2-5

Marine Sediment Core and Test Pit Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report











Analytical Suite and Laboratory





















Total Organic















Cr-VI





Modified SPLPb



Carbon















(Manchester





(Manchester

PAHs

(Manchester

Bulk Density

Grain Size





Sample

Depth



Environmental

Mercury

TAL Metals a

Environmental

(KAP

Environmental

(Applied Sciences

(Applied Sciences

Location

Activity ID

Type

(feet)

Sample Date

Laboratory)

(A4 Scientific)

(A4 Scientific)

Laboratory)

Technologies)

Laboratory)

Laboratory)

Laboratory)

SB-308

2013SC-SB-308-03-20130829

N

3 - 4

8/29/2013



X

X











SB-308

2013SC-SB-308-04-20130829

N

4 - 5

8/29/2013



X

X











SB-308

2013SC-SB-308-05-20130829

N

5 - 6

8/29/2013



X

X











SB-308

2013SC-SB-308-06-20130829

N

6 - 7

8/29/2013



X

X











SB-308

2013SC-SB-308-07-20130829

N

7 - 8

8/29/2013



X

X











SB-308

2013SC-SB-308-08-20130829

N

8 - 9

8/29/2013



X

X











SB-308

2013SC-SB-308-09-20130829

N

9 - 9.5

8/29/2013



X

X











SB-313

2013SC-SB-313-02-20130828

N

2 - 3

8/28/2013









X







SB-313

2013SC-SB-313-03-20130828

N

3 - 4

8/28/2013









X







SB-316

2013SC-SB-316-07-20130828

N

7 - 7

8/28/2013









X







SB-316

2013SC-SB-316-07-20130828

N

7 - 8

8/28/2013









X







SB-319

2013SC-SB-319-04-20130829

N

4 - 5

8/29/2013









X







SB-322

2013SC-SB-322-02-20130830

N

2 - 2.5

8/30/2013









X







SB-316

2013SC-SB-316-06-20130828

N

6 - 7

8/30/2013









X







SB-322

2013SC-SB-322-04-20130830

N

4 - 5

8/30/2013









X







Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium, silver, thallium, vanadium, zinc

bSeawater collected at SW-600 in Browns Bay was used for sediment leaching

Cr VI = hexavalent chromium

PAHs = polycyclic aromatic hydrocarbons

SPLP = synthetic precipitation leaching procedure

N = normal

FD = field duplicate

PAGE 5 OF 5


-------
TABLE 2-6

Short-core and Test Pit Sample Information - Upland Tailings Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Depth

Core
Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(0 to 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24 + inches)

Comments

Deviations

SB-041

Short-core

13.5

55.626415

-132.558551

5/25/2013

11:15 AM

17

12

2013SC-SB-041-00 +MS/MSD
2013SC-SB-9041-00

0" to 12" - very fine SAND with
mica, trace Silt, trace
organics/plant fibers, wet, most
likely tailings, olive green

2013SC-SB-041-0.5

0" to 12" - very fine SAND with
mica, trace Silt, trace
organics/plant fibers, wet,
most likely tailings, olive green













SB-047

Short-core

14.1

55.626467

-132.558739

5/25/2013

11:30 AM

12

12

No sample

0" to 12" - coarse brown SAND
w/high levels of mica, some
wood and organic debris
throughout the interval,
saturated at bottom (8" to 12");
no clear interface between
tailings or sediment

No sample

see 0" to 6" cell

No sample



No sample



1st attempt, refusal at 6"; 2nd
attempt, refusal at 12".

After completing drilling, 4" of
standing water in drill hole.



SB-053

Test pit

12.7

55.626365

-132.558821

5/25/2013

12:45 PM

24

24

2013SC-SB-053-00 +MS/MSD
2013SC-SB-9053-00

0" to 6" - very fine SAND (very
likely tailings) fine mica flakes
throughout, trace Silt, some
wood pieces throughout, wet,
dark gray to olive gray

2013SC-SB-053-0.5

6" to 12" - same as 0" to 6"
with abundant wood debris,
wet

2013SC-SB-053-01

12" to 24" - very fine SAND
with mica flakes (tailings),
wood pieces, and roots
throughout, wet, olive green,
increased Silt





vibracore refusal at 9"; hand dug
to 2 feet



SB-173

Short-core

14.3

55.626445

-132.558631

5/25/2013

12:00 PM

19.2

19.2

2013SC-SB-173-00

0" to 19.2" - very fine SAND
with mica, olive green, wet,
trace Silt, most likely tailings,
trace oxidized Silt/Clay at 1.5'
bgs and decomposed plant
matter from 1.5' to 1.6' (tailings
on top of forest floor material)

2013SC-SB-173-0.5

0" to 19.2" - very fine SAND
with mica, olive green, wet,
trace Silt, most likely tailings,
trace oxidized Silt/Clay at 1.5'
bgs and decomposed plant
matter from 1.5' to 1.6'
(tailings on top of forest floor
material)

2013SC-SB-173-01

0" to 19.2" - very fine SAND
with mica, olive green, wet,
trace Silt, most likely tailings,
trace oxidized Silt/Clay at 1.5'
bgs and decomposed plant
matter from 1.5' to 1.6'
(tailings on top of forest floor
material)





Drill 19" before hitting refusal

Moved sample
location 10 feet south
of planned due to
dense vegetation

SB-178

Short-core







5/30/2013

8:50 AM

18

12

No sample

0" to 2" - vegetation, bark, pine
needles in top 2"

2013SC-SB-178-0.5

6" to 12" - gray to greenish gray
SAND with some fines.









Drove core from 0.5 feet to 1.0
feet using a tube.

Location added as part
of upland tailings
investigation.

SB-179

Short-core



55.626971

-132.559483

5/30/2013

9:05 AM

12

12

No sample

No description

2013SC-SB-179-0.5

6" to 12" - gray to yellowish,
stiff CLAY with no Sand. Same
material was observed 50 ft
upstream of unnamed creek









Sample collected inside
unnamed creek

Sample added as part
of upland tailings
delineation

SB-180

Short-core

28.7

55.626878

-132.558766

5/30/2013

9:17 AM

12

12

No sample

No description

2013SC-SB-180-0.5

6" to 12" - gray to greenish
gray fine SAND (tailings)











Sample added as part
of upland tailings
investigation

SB-220 a

Test pit



55.625673

-132.559407

5/30/2013

9:25 AM

6

6

2013SC-SB-220-00

50% Fines, 50% Silt, brown to
dark gray













Spoon sampled

Sample added as part
of upland tailings
delineation
(unrecognized
duplicate location ID)

SB-221

Test pit



55.625999

-132.558951

5/30/2013

9:40 AM

6

6

2013SC-SB-221-00

75% Sand, 25% fines













Spoon sampled

Sample added as part
of upland tailings
delineation

UT-01

Test pit

20.7

55.626318

-132.557665

5/30/2013



12

12

No sample

1" duff, 5" tailings (green sand)

No sample

Tailings (green sand)













UT-02

Test pit

21.6

55.626332

-132.557733

5/30/2013



12

12

No sample

3" duff, 3" tailings (green sand)

No sample

Tailings (green sand)













UT-03

Test pit

18.1

55.626393

-132.558111

5/30/2013



10

10

No sample

2" duff, 4" tailings (green sand)

No sample

Tailings (green sand)













UT-04

Test pit

17.3

55.626375

-132.558119

5/30/2013



12

12

No sample

3" duff, 3" tailings (green sand)

No sample

Tailings (green sand)













UT-05

Test pit

27.9

55.626499

-132.558027

5/30/2013



6

6

No sample

6" duff and roots, no tailings

















UT-06

Test pit

19.3

55.626511

-132.558412

5/30/2013



8

8

No sample

1" duff, 5" tailings (green sand)

No sample

Tailings (green sand)













UT-07

Test pit

19.8

55.626517

-132.55838

5/30/2013



15

15

No sample

4" duff, 2" tailings (green sand)

No sample

Tailings (green sand)

No sample

Tailings (green sand)









UT-08

Test pit

22.2

55.626538

-132.558349

5/30/2013



10

10

No sample

5" duff, 1" tailings (green sand)

No sample

Tailings (green sand)













UT-09

Test pit

23.0

55.626631

-132.558506

5/30/2013



4

4

No sample

4" tailings (green sand)

















UT-10

Test pit

18.5

55.626588

-132.558639

5/30/2013



6

6

No sample

1" duff, 5" tailings (green sand)

















UT-11

Test pit

20.3

55.626679

-132.558697

5/30/2013



6

6

No sample

1" duff, 5" tailings (green sand)

















UT-12

Test pit

18.9

55.626656

-132.558732

5/30/2013



11

11

No sample

3" duff, 3" tailings (green sand)

No sample

Tailings (green sand)













UT-13

Test pit

19.6

55.626726

-132.558848

5/30/2013



17

17

No sample

5" duff, 1" tailings (green silty
clay and sand)

No sample

Tailings (green silty clay and sai

No sample

Tailings (green silty clay and sand)







UT-14

Test pit

19.4

55.626766

-132.558974

5/30/2013



13

13

No sample

Brown sandy silt - high organic
content

No sample

6 -10" brown sandy silt, 10 -
13" tailings (green silty and
clayey sand)

No sample











UT-15

Test pit

14.2

55.62657

-132.558888

5/30/2013



36

36

No sample

Cut bank, tailings (green silty san

No sample

Cut bank, tailings (green silty sa

No sample

Cut bank, tailings (green silty sa

No sample

Cut bank, tailings (green silty sand)



UT-16

Test pit

*

55.626918

-132.559033

5/30/2013



14

14

No sample

Black silty sand, no tailings

No sample

Black silty sand, no tailings

No sample

Black silty sand, no tailings









UT-18

Test pit

*

55.626746

-132.559198

5/30/2013



36

36

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings
(green silty sand)

Extends 30 feet upstream



UT-19

Test pit

*

55.626531

-132.559187

5/30/2013



36

36

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings (green silty
sand)

No sample

Cut bank, tailings
(green silty sand)

Extends 30 feet upstream



UT-20

Test pit



55.626589

-132.559306

5/30/2013



21

21

No sample

Black silty sand, organic, no
tailings

No sample

Black silty sand, organic, no
tailings

No sample

Black silty sand, organic, no
tailings to 20"; tailings (green
silty sand) at 20 to 21"









UT-21

Test pit

*

55.626528

-132.559261

5/30/2013



11

11

No sample

1" duff, 5" tailings (green silty sa

No sample

Tailings (green silty sand)













UT-22

Test pit

*

55.626455

-132.55931

5/30/2013



7

7

No sample

1" duff, 5" tailings (green silty sa

No sample

Tailings (green silty sand)













UT-23

Test pit

*

55.626345

-132.559502

5/30/2013



7

7

No sample

Brown organic silty sand

No sample

Brown organic silty sand













UT-24

Test pit

*

55.626402

-132.559189

5/30/2013



6

6

No sample

1" duff, 5" tailings (green silty sand)















PAGE 1 OF 2


-------
TABLE 2-6

Short-core and Test Pit Sample Information - Upland Tailings Investigation

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Type

Elevation

(feet
NAVD88)

Latitude

Longitude

Date

Time

Depth

Core
Recovered
(inches)

Sample IDa
(0 to 6 inches)

Sample Description
(0 to 6 inches)

Sample IDa
(6 to 12 inches)

Sample Description
(6 to 12 inches)

Sample IDa
(12 to 24 inches)

Sample Description
(12 to 24 inches)

Sample IDa
(24+ inches)

Sample Description
(24 + inches)

Comments

Deviations

UT-25

Test pit

*

55.626266

-132.559159

5/30/2013



5

5

No sample

1" duff, 4" tailings (green silty sand)















Ut-26

Test pit

*

55.626181

-132.559273

5/30/2013



12

12

No sample

Brown organic silty sand

No sample

Brown organic silty sand









Boggy low point



UT-27

Test pit

*

55.626164

-132.55911

5/30/2013



12

12

No sample

Brown organic silty sand

No sample

Brown organic silty sand













UT-28

Test pit



55.626116

-132.559185

5/30/2013



18

18

No sample

Duff

No sample

6 - 7" duff, 7-10" tailings
(green silty sand), 10 -12"
brown organic silty sand

No sample

Brown organic silty sand









UT-29

Test pit

*

55.626153

-132.559055

5/30/2013



8

8

No sample

2" duff, 4" tailings (green silty sa

No sample

Tailings (green silty sand)













UT-30

Test pit

*

55.625869

-132.559323

5/30/2013



7

7

No sample

2" duff, 4" tailings (green silty sa

No sample

Tailings (green silty sand)













UT-32

Test pit

13.7

55.625951

-132.558966

5/30/2013



9

9

No sample

1" duff, 5" tailings (green silty sa

No sample

Tailings (green silty sand)













UT-33

Test pit

14.0

55.625623

-132.558751

5/30/2013



9

9

No sample

Duff

No sample

Duff













Notes:

0 Number at the end of each Sample ID indicates the top of the sample interval. The first two intervals are 0.5 ft thick (0 to 0.5 ft and 0.5 to 1 ft), remaining intervals are 1 ft thick
MS/MSD = matrix spike/matrix spike duplicate

PAGE 2 OF 2


-------
TABLE 2-7

Upland Short Core and Test Pit Sample Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Activity ID

Sample
Type

Depth
(feet)

Sample Date

Analytical Suite and Laboratory

Cr-VI
(Manchester
Environmental
Laboratory)

Mercury
(A4 Scientific)

TAL Metals a
(A4 Scientific)

SB-041

2013SC-SB-041-00-20130525

N

LD

O
O

5/25/2013

X

X

X

SB-041

2013SC-SB-9041-00-20130525FD

FD

LD

o
o

5/25/2013

X

X

X

SB-041

2013SC-SB-041-0.5-20130525

N

0.5 - 1

5/25/2013



X

X

SB-053

2013SC-SB-053-00-20130525

N

LD

o
o

5/25/2013

X

X

X

SB-053

2013SC-SB-9053-00-20130525FD

FD

LD

o
o

5/25/2013



X

X

SB-053

2013SC-SB-053-0.5-20130525

N

0.5 - 1

5/25/2013



X

X

SB-053

2013SC-SB-053-01-20130525

N

1 - 2

5/25/2013



X

X

SB-173

2013SC-SB-173-00-20130525

N

LD

o
o

5/25/2013



X

X

SB-173

2013SC-SB-173-0.5-20130525

N

0.5 - 1

5/25/2013



X

X

SB-173

2013SC-SB-173-01-20130525

N

1 - 1.6

5/25/2013



X

X

SB-173

2013SC-SB-9173-01-20130525FD

FD

1 - 2

5/25/2013



X

X

SB-178

2013SC-SB-178-0.5-20130530

N

0.5 - 1

5/30/2013



X

X

SB-179

2013SC-SB-179-00-20130530

N

LD

o
o

5/30/2013



X

X

SB-180

2013SC-SB-180-0.5-20130530

N

0.5 - 1

5/30/2013



X

X

SB-220a

2013SC-SB-220-00-20130530

N

LD

o
o

5/30/2013



X

X

SB-221

2013SC-SB-221-00-20130530

N

LD

o
o

5/30/2013



X

X

Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium, silver,

thallium, vanadium, zinc.

Cr VI = hexavalent chromium

N = normal

FD = field duplicate

PAGE 1 OF 1


-------
TABLE 2-8

Marine Porewater Sample Information

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

Elevation
(feet NAVDSS)

Latitude

Longitude

Date

Time

Location Type
(airstone or
drive point)

Airstone Sample
Depth (inches)

Drive-point
Sample Depth
(feet)

Conductivity
(ms/cm)

Temperature
(deg. C)

DO
(mg/L)

pH

Salinity
(units as
indicated)8

Turbidity
(NTU)

Comments

Deviations

PW-001

None





























No sample

Not installed . other
samples in close proximity

PW-002

2013SC-PW-002

10.0

55.626075

-132.557391

5/28/2013

7:15 AM

Drive-point

NA

3

88.6

13.39

6.42

7.52

>4.0%

0.00





PW-003

2013SC-PW-003

11.6

55.626012

-132.557277

5/28/2013

8:05 AM

Drive-point

NA

3.5

>99.9

13.84

5.22

7.30

>4.0%

2.50

Collected field duplicate 2013SC-PW-9003;
conductivity out of range



PW-006

2013SC-PW-006

12.0

55.626174

-132.557538

5/28/2013

6:50 AM

Drive-point

NA

3

79.9

13.47

7.05

6.38

> 4.0 %

0.30





PW-008

2013SC-PW-008

11.3

55.625875

-132.557111

5/27/2013

1:40 PM

Drive-point

NA

3.5

>99.9

16.78

6.76

7.45

26 ppt

0.00

Turbidity value flashing 0.0; conductivity out
of range



PW-014

2013SC-PW-014

7.6

55.625835

-132.556671

5/27/2013

11:25 AM

Drive-point

NA

3

70.9

15.94

6.65

7.57

16 ppt

0.00

Turbidity value flashing 0.0; MS/MSD
collected



PW-016

2013SC-PW-016

8.7

55.625835

-132.556351

5/26/2013

7:28 AM

Airstone

19.5

NA

-

-

-

-

8 ppt







PW-017

2013SC-PW-017

8.6

55.625765

-132.557001

5/26/2013

7:55 AM

Airstone

23

NA

»

-

»

»

17 ppt







PW-022

2013SC-PW-022

11.0

55.625615

-132.557271

5/26/2013

6:44 AM

Airstone

23

NA

-

-

-

-

27 ppt







PW-027

2013SC-PW-027

CO
CO

55.625755

-132.556151

5/26/2013

7:35 AM

Airstone

18

NA

»

»

»

»

3 ppt







PW-030

2013SC-PW-030

6.2

55.625575

-132.556821

5/26/2013

8:23 AM

Airstone

19.5

NA

-

-

-

-

11 ppt







PW-037

2013SC-PW-037

10.7

55.625485

-132.557641

5/26/2013

6:36 AM

Airstone

21.5

NA

-

»

-

»

29 ppt







PW-042

2013SC-PW-042

8.1

55.625615

-132.555911

5/26/2013

7:41AM

Airstone

23.5

NA

-

-

-

-

12 ppt







PW-045

2013SC-PW-045

10.4

55.625415

-132.558001

5/26/2013

6:27 AM

Airstone

23

NA

-

»

-

»

33 ppt







PW-055

2013SC-PW-055

7.1

55.625235

-132.556511

5/26/2013

8:31AM

Airstone

24

NA

-

-

-

-

26 ppt



Collected field duplicate 2013SC-PW-9055



PW-056

2013SC-PW-056

CO
CO

55.625465

-132.555661

5/26/2013

7:48 AM

Airstone

24

NA

»

-

»

»

25 ppt







PW-064

2013SC-PW-064

4.6

55.625135

-132.556031

5/26/2013

6:45 AM

Airstone

22

NA

-

-

-

-

29 ppt







PW-065

2013SC-PW-065

5.6

55.625235

-132.555691

5/26/2013

6:55 AM

Airstone

24

NA

-

»

-

»

19 ppt







PW-066

2013SC-PW-066

6.3

55.625045

-132.556331

5/26/2013

8:47 AM

Airstone

21.5

NA

-

-

-

-

18 ppt







PW-068

2013SC-PW-068

8.5

55.625325

-132.555411

5/26/2013

7:00 AM

Airstone

21

NA

-

»

-

»

19 ppt







PW-069

2013SC-PW-069

7.5

55.624965

-132.556581

5/26/2013

6:30 AM

Airstone

23

NA

-

-

-

-

27 ppt







PW-071

2013SC-PW-071

8.0

55.624855

-132.556951

5/26/2013

6:20 AM

Airstone

23

NA

-

-

-

-

26 ppt



Collected field duplicate 2013SC-PW-9071



PW-073

2013SC-PW-073

5.0

55.624845

-132.556151

5/26/2013

8:56 AM

Airstone

23.5

NA

-

-

-

-

20 ppt







PW-074

2013SC-PW-074

8.2

55.625175

-132.555161

5/26/2013

7:10 AM

Airstone

24

NA

»

»

-

»

25 ppt







PW-076

2013SC-PW-076

8.1

55.624745

-132.557301

5/26/2013

6:11AM

Airstone

24

NA

-

-

-

-

30 ppt



MS/MSD collected



PW-080

2013SC-PW-080

8.2

55.625025

-132.554911

5/26/2013

7:20 AM

Airstone

23.5

NA

-

»

-

»

28 ppt







PW-081

2013SC-PW-081

4.3

55.624635

-132.555951

5/26/2013

9:10 AM

Airstone

18.5

NA

-

-

-

-

26 ppt







PW-086

2013SC-PW-086

4.0

55.624475

-132.555811

5/26/2013

9:20 AM

Airstone

24

NA

-

»

-

»

25 ppt







PW-088

2013SC-PW-088

7.1

55.624855

-132.554621

5/26/2013

7:30 AM

Airstone

24

NA

-

-

-

-

25 ppt







PW-090

2013SC-PW-090

3.0

55.624535

-132.555061

5/26/2013

8:05 AM

Airstone

19

NA









22 ppt



Placed 100 mL in clear glass jar to settle out
fines (airstone may have failed) sample
filtering postponed until fines settled out



PW-091

2013SC-PW-091

4.1

55.624405

-132.555471

5/26/2013

9:20 AM

Airstone

23

NA

-

-

-

-

27 ppt



Collected field duplicate 2013SC-PW-9091



PW-092

2013SC-PW-092

4.1

55.624635

-132.554731

5/26/2013

8:13 AM

Airstone

17

NA

"

~

"

"

NR



Took ~ 1 hr to pull and filter 100 mL

Field duplicate moved to
different location

PW-094

2013SC-PW-094

4.0

55.624265

-132.555931

5/26/2013

9:40 AM

Airstone

20

NA

-

-

-

-

29 ppt







PW-096

2013SC-PW-096

7.0

55.624745

-132.554491

5/26/2013

7:35 AM

Airstone

23.5

NA

-

»

-

»

22 ppt







PW-097

2013SC-PW-097

4.0

55.624175

-132.556241

5/26/2013

9:41AM

Airstone

22

NA

-

-

-

-

29 ppt







PW-100

2013 SC-PW-100

4.3

55.624085

-132.557031

5/26/2013

9:48 AM

Airstone

23

NA

-

-

-

-

25 ppt







PW-101

2013SC-PW-101

4.9

55.624095

-132.557501

5/26/2013

9:55 AM

Airstone

21.5

NA

-

-

-

-

25 ppt







PW-102

2013SC-PW-102

4.0

55.624075

-132.556561

5/26/2013

9:50 AM

Airstone

24

NA

-

»

-

»

29 ppt







PW-103

2013 SC-PW-103

3.8

55.624195

-132.555541

5/26/2013

9:31AM

Airstone

18

NA

-

-

-

-

24 ppt







PW-169

2013 SC-PW-169

8.4

55.625945

-132.557951

5/26/2013

7:08 AM

Airstone

20

NA

-

»

-

»

19 ppt







PW-170

2013 SC-PW-170

7.3

55.625835

-132.557951

5/26/2013

7:16 AM

Airstone

18

NA

-

-

-

-

23 ppt







PW-171

2013 SC-PW-171

7.8

55.626105

-132.558121

5/26/2013

6:55 AM

Airstone

16.5

NA

-

»

-

»

19 ppt







PW-174

2013 SC-PW-174

9.3

55.625734

-132.555858

5/27/2013

10:15 AM

Drive-point

NA

4.25

63.3

15.45

7.93

6.16

11 ppt

0.00

Turbidity readings flashing 0.0



PW-175

2013SC-PW-175

11.3

55.625637

-132.555355

5/27/2013

9:06 AM

Drive-point

NA

5

99.9

14.9

5.57

7.24

28 ppt

0.00

Turbidity and conductivity values flashing;
malfunction and out of range



PW-511

2013SC-PW-511

*

55.587645

-132.546961

5/29/2013

10:25 AM

Airstone

NR

NA

-

-

-

-

30 ppt







PW-512

2013SC-PW-512

*

55.587955

-132.547291

5/29/2013

10:40 AM

Airstone

NR

NA

»

»

-

»

28 ppt







PW-513

2013SC-PW-513

*

55.589225

-132.547611

5/29/2013

10:50 AM

Airstone

NR

NA

-

»

-

»

30 ppt







Notes:

a Salinity measured using Horriba (%) in selected drive-point samples, salinity measured using refractometer (ppt) in selected drive-point samples and in airstone samples.

- not measured at airstone locations due to limited volume

* Sample location outside of area surveyed for elevation

ppt = parts per thousand

NR = not recorded

NA = not applicable

MS/MSD = matrix spike/matrix spike duplicate

PAGE 1 OF 1


-------
TABLE 2-9

Marine Porewater Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Sample
Type

Activity ID

Sample Date

Depth (feet)

Analytical Suite and Laboratory

Dissolved
Mercury
(A4 Scientific)

Dissolved TAL

Metals8
(A4 Scientific)

PAHs
(KAP Technologies)

PW-002

N

2013SC-PW-002-20130528

5/28/2013

0-3

X

X

X

PW-003

N

2013SC-PW-003-20130528

5/28/2013

0-3

X

X

X

PW-003

FD

2013SC-PW-9003-20130528FD

5/28/2013

0-3

X

X

X

PW-006

N

2013SC-PW-006-20130528

5/28/2013

0-3

X

X



PW-008

N

2013SC-PW-008-20130527

5/27/2013

0-3

X

X

X

PW-014

N

2013SC-PW-014-20130527

5/27/2013

0-2

X

X

X

PW-016

N

2013SC-PW-016-20130526

5/26/2013

0-2

X

X



PW-017

N

2013SC-PW-017-20130526

5/26/2013

0-2

X

X



PW-022

N

2013SC-PW-022-20130526

5/26/2013

0-2

X

X



PW-027

N

2013SC-PW-027-20130526

5/26/2013

0-2

X

X



PW-030

N

2013SC-PW-030-20130526

5/26/2013

0-2

X

X



PW-037

N

2013SC-PW-037-20130526

5/26/2013

0-2

X

X



PW-042

N

2013SC-PW-042-20130526

5/26/2013

0-2

X

X



PW-045

N

2013SC-PW-045-20130526

5/26/2013

0-2

X

X



PW-055

N

2013SC-PW-055-20130526

5/26/2013

0-2

X

X



PW-055

FD

2013SC-PW-9055-20130526FD

5/26/2013

0-2

X

X



PW-056

N

2013SC-PW-056-20130526

5/26/2013

0-2

X

X



PW-064

N

2013SC-PW-064-20130526

5/26/2013

0-2

X

X



PW-065

N

2013SC-PW-065-20130526

5/26/2013

0-2

X

X



PW-066

N

2013SC-PW-066-20130526

5/26/2013

0-2

X

X



PW-068

N

2013SC-PW-068-20130526

5/26/2013

0-2

X

X



PW-069

N

2013SC-PW-069-20130526

5/26/2013

0-2

X

X



PW-071

N

2013SC-PW-071-20130526

5/26/2013

0-2

X

X



PW-071

FD

2013SC-PW-9071-20130526FD

5/26/2013

0-2

X

X



PW-073

N

2013SC-PW-073-20130526

5/26/2013

0-2

X

X



PW-074

N

2013SC-PW-074-20130526

5/26/2013

0-2

X

X



PW-076

N

2013SC-PW-076-20130526

5/26/2013

0-2

X

X



PW-080

N

2013SC-PW-080-20130526

5/26/2013

0-2

X

X



PW-081

N

2013SC-PW-081-201305 26

5/26/2013

0-2

X

X



PW-086

N

2013SC-PW-086-20130526

5/26/2013

0-2

X

X



PW-088

N

2013SC-PW-088-20130526

5/26/2013

0-2

X

X



PW-090

N

2013SC-PW-090-20130526

5/26/2013

0-2

X

X



PW-091

N

2013SC-PW-091-20130526

5/26/2013

0-2

X

X



PW-091

FD

2013SC-PW-9091-20130526FD

5/26/2013

0-2

X

X



PW-092

N

2013SC-PW-092-20130526

5/26/2013

0-2

X

X



PW-094

N

2013SC-PW-094-20130526

5/26/2013

0-2

X

X



PW-096

N

2013SC-PW-096-20130526

5/26/2013

0-2

X

X



PW-097

N

2013SC-PW-097-20130526

5/26/2013

0-2

X

X



PW-100

N

2013SC-PW-100-20130526

5/26/2013

0-2

X

X



PW-101

N

2013SC-PW-101-20130526

5/26/2013

0-2

X

X



PW-102

N

2013SC-PW-102-20130526

5/26/2013

0-2

X

X



PW-103

N

2013SC-PW-103-20130526

5/26/2013

0-2

X

X



PW-169

N

2013SC-PW-169-20130526

5/26/2013

0-2

X

X



PW-170

N

2013SC-PW-170-20130526

5/26/2013

0-2

X

X



PW-171

N

2013SC-PW-171-20130526

5/26/2013

0-2

X

X



PW-174

N

2013SC-PW-174-20130527

5/27/2013

0-3

X

X

X

PW-175

N

2013SC-PW-175-20130527

5/27/2013

0-3

X

X

X

PW-511

N

2013SC-PW-511-20130529

5/29/2013

0-2

X

X



PW-512

N

2013SC-PW-512-20130529

5/29/2013

0-2

X

X



PW-513

N

2013SC-PW-513-20130529

5/29/2013

0-2

X

X



Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel,
selenium, silver, thallium, vanadium, zinc
N = normal
FD = field duplicate

PAHs = polycyclic aromatic hydrocarbons

PAGE 1 OF 1


-------
TABLE 2-10

Surface Water Sample Information

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

Elevation
(feet NAVDSS)

Latitude

Longitude

Date

Time

Conductivity
(ms/cm)

Temperature
(deg. C)

DO
(mg/L)

pH

Salinity
(units as
indicated)8

Turbidity
(NTU)

Comments

Deviations

SW-015

2013SC-SW-015

6.9

55.626025

-132.557781

5/25/2013

9:00 AM

1.33

NR

10.9

6.99

0.10%

48.0

parameters measured one day later on 5/26/13 at 13:00
during sample processing; DO measurement not
representative

Diss. Metals collected 5.25.13; PAH
sample collected on 5/26/13

SW-029

2013SC-SW-029

5.1

55.625625

-132.556521

5/25/2013

9:00 AM

91.1

16.5

6.48

8.58

> 4.0%

2.2

Fine sand with silt at bottom. Sample collected at outlet
of seepage zone. Sculpin.



SW-075

2013SC-SW-075

3.7

55.624945

-132.555731

5/25/2013

8:45 AM

98.1

17.35

6.52

8.45

> 4.0%

2.7

Silt with fine sand on bottom, seaweed (10% cover),
marine life - hermit crab, shrimp/sculpin (difficult to see -
moved quickly)



SW-084

2013SC-SW-084

4.5

55.624435

-132.557641

5/25/2013

8:45 AM

8.75

13.48

10.86

8.51

0.50%

5.0





SW-085

2013SC-SW-085

6.0

55.625105

-132.554341

5/25/2013

8:35 AM

369.7

12.83

9.07

7.71

2.30%

3.9

Fine sand with silt on bottom. Algae and seaweed (~40%
cover)



SW-098

2013SC-SW-098

7.2

55.624625

-132.554541

5/25/2013

8:25 AM

51.5

12.14

9.87

8.02

3.30%

NR

Turbidity meter not working. Fine sand and silt. Cut bank
on right side of stream (looking downstream). Seaweed.



SW-099

2013SC-SW-099

2.5

55.624385

-132.555091

5/25/2013

8:10 AM

86.3

12.03

7.76

8.06

> 4.0%

116.0

High turb. reading but no visual indication of high
turbidity. Fine sand with silt on bottom. Algal mat on
upland banks.



SW-104

2013SC-SW-104

3.0

55.623935

-132.558501

5/25/2013

8:30 AM

41.3

11.71

10.7

8.35

2.70%

2.7





SW-105

2013SC-SW-105

1.1

55.623815

-132.555701

5/25/2013

8:15 AM

57.1

11.14

9.44

8.16

3.70%

2.6





SW-106

2013SC-SW-106

*

55.625055

-132.561231

5/25/2013

9:40 AM

21.5

14.7

11.56

8.9

1.30%

0.0

Gravel and coarse sand; riverbed.



SW-108

2013SC-SW-108

*

55.623455

-132.554301

5/25/2013

8:00 AM

62.4

10.88

8.68

7.98

4%

2.1





SW-108

2013SC-SW-108-0400

*

55.623455

-132.554301

5/26/2013

4:00 AM

~

~

~

~

~

~

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-0500

*

55.623455

-132.554301

5/26/2013

5:00 AM

~

~

~

~

~

~

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-0600

*

55.623455

-132.554301

5/26/2013

6:00 AM

~

"

~

"

~

"

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-0700

*

55.623455

-132.554301

5/26/2013

7:00 AM

~

"

~

"

~

"

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-0800

*

55.623455

-132.554301

5/26/2013

8:00 AM

~

"

~

"

~

"

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-0900

*

55.623455

-132.554301

5/26/2013

9:00 AM

"

"

"

"

"

"

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-1000

*

55.623455

-132.554301

5/26/2013

10:00 AM

~

~

~

~

~

~

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-1100

*

55.623455

-132.554301

5/26/2013

11:00 AM

~

~

~

~

~

~

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-108

2013SC-SW-108-1200

*

55.623455

-132.554301

5/26/2013

12:00 PM

~

"

~

"

~

"

Collected samples at every hour from 04:00 AM to 12:00
PM for full tide cycle



SW-113

2013SC-SW-113

*

55.623205

-132.552921

5/25/2013

7:50 AM

>99.9

10.78

7.12

7.84

>4.0%

3.0

Live crab in water, gravelly bottomed, seaweed (~60 %
cover)

Moved location ~25 feet downstream
to be in flow

SW-501

2013SC-SW-501

*

55.598455

-132.549681

5/28/2013

1:00 PM

-

»

-

»

30 ppt

»





SW-503

2013SC-SW-503

*

55.596695

-132.545041

5/28/2013

1:25 PM

-

-

-

-

30 ppt

-





SW-505

2013SC-SW-505

*

55.594125

-132.549861

5/28/2013

1:20 PM

-

-

-

-

30 ppt

-





SW-507

2013SC-SW-507

*

55.593735

-132.541491

5/28/2013

1:30 PM









29 ppt







SW-509

2013SC-SW-509

*

55.590685

-132.548551

5/28/2013

1:10 PM

»

-

»

-

29 ppt

-

Field duplicate 2013SC-SW-9509



SW-600

2013SC-SW-600

*

55.592795

-132.550791

5/29/2013

11:10 AM

»

-

»

-

30 ppt

-





Notes:

a Salinity measured using Horriba (%) in on-site surface water samples, salinity measured using refractometer (ppt) in background surface water locations
ppt = parts per thousand
- = not measured

* Sample location outside of area surveyed for elevation

mS/cm = millisiemens per centimeter

NTU = nephelometric turbidity unit

mg/L = milligrams per liter

deg. C = degrees Celcius

mV = millivolt

% = percent

PAGE 1 OF 1


-------
TABLE 2-11

Surface Water Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report









Analytical Suite and Laboratory















Dissolved

Dissolved TAL Metals8



Sample





PAHs

Total TAL Metalsa

Total Mercury

Mercury

(A4 Scientific and ALS

Location

Type

Activity ID

Sample Date

(KAP Technologies)

(A4 Scientific)

(A4 Scientific)

(A4 Scientific)

Environmental)

SW-015

N

2013SC-SW-015-20130525

5/25/2013

X





X

X

SW-029

N

2013SC-SW-0 29-201305 25

5/25/2013

X





X

X

SW-075

N

2013SC-SW-075-20130525

5/25/2013

X





X

X

SW-0S4

N

2013SC-SW-084-20130525

5/25/2013

X





X

X

SW-0S4

FD

2013SC-SW-9084-20130525FD

5/25/2013

X





X

X

SW-0S5

N

2013SC-SW-085-20130525

5/25/2013







X

X

SW-09S

N

2013SC-SW-098-20130525

5/25/2013







X

X

SW-099

N

2013SC-SW-099-20130525

5/25/2013

X





X

X

SW-104

N

2013SC-SW-104-20130525

5/25/2013



X

X

X

X

SW-105

N

2013SC-SW-105-20130525

5/25/2013



X

X

X

X

SW-106

N

2013SC-SW-106-20130525

5/25/2013



X

X

X

X

SW-106

FD

2013SC-SW-9106-201305 25 FD

5/25/2013



X

X

X

X

SW-108

N

2013SC-SW-108-0800-20130525

5/25/2013







X

X

SW-108

N

2013CS-SW-108-0400-20130526

5/26/2013







X

X

SW-108

N

2013CS-SW-108-0500-20130526

5/26/2013







X

X

SW-108

N

2013CS-SW-108-0700-201305 26

5/26/2013







X

X

SW-108

N

2013CS-SW-108-0800-20130526

5/26/2013







X

X

SW-108

N

2013CS-SW-108-09 00-201305 26

5/26/2013







X

X

SW-108

N

2013CS-SW-108-1000-20130526

5/26/2013







X

X

SW-108

N

2013CS-SW-108-1100-20130526

5/26/2013







X

X

SW-108

N

2013CS-SW-108-1200-20130526

5/26/2013







X

X

SW-108

N

2013SC-SW-108-0600-20130526

5/26/2013







X

X

SW-108

FD

2013SC-SW-9108-0700-20130526FC

5/26/2013







X

X

SW-113

N

2013SC-SW-113-201305 25

5/25/2013







X

X

SW-501

N

2013SC-SW-501-20130528

5/28/2013







X

X

SW-503

N

2013SC-SW-503-20130528

5/28/2013







X

X

SW-505

N

2013SC-SW-505-20130528

5/28/2013







X

X

SW-507

N

2013SC-SW-507-20130528

5/28/2013







X

X

SW-509

N

2013SC-SW-509-20130528

5/28/2013







X

X

SW-509

FD

2013SC-SW-9509-20130528FD

5/28/2013







X

X

Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTALmetals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium,
silver, thallium, vanadium, zinc

b Reanalyzed surface water samples for chromium, cobalt, copper, iron, lead, nickel, selenium, silver, thallium, and vanadium
N = normal environmental sample
FD = field duplicate

PAHs = polycyclic aromatic hydrocarbons

PAGE 1 OF 1


-------
TABLE 2-12

Marine Biota Sample Information

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

Elevation
(feet NAVDSS)

Latitude

Longitude

Date

Time

Species

Specimen 1
Size

Specimen 1
Weight

Specimen 2
Size

Specimen 2
Weight

Specimen 3
Size

Specimen 3
Weight

Total
Weight
Submitted

Comments

Deviations

2013-SC-Biota-107

2013-SC-Biota-107-Crab

*

55.623635

-132.550651

5/28/2013

3:00 PM

Dungeness
Crab

7.0 inches

828 grams

6.75 inches

764 grams

7.0 inches

972 grams

105 grams



Trap left 2 days at original location but no crabs.
Moved location to match where crab are in
deeper water

2013-SC-Biota -130

2013-SC-Biota-130-Crab

*

55.622735

-132.551921

5/24/2013

7:15 AM

Dungeness
Crab

6.625 inches

764 grams

6.5 inches

635 grams

6.625 inches

753 grams

105 grams

Relocated map location to Lake Ellen
Cr north of Unnamed Island centered
with island just off (N) of largest
boulder



2013-SC-Biota-138

2013-SC-Biota-138-Crab

*

55.618755

-132.552911

5/22/2013

6:30 AM

Dungeness
Crab

7.0 inches

854 grams

6.5 inches

666 grams

6.75 inches

814 grams

120 grams





2013-SC-Biota-142

2013-SC-Biota-142-Crab

*

55.6193

-132.544809

5/23/2013

7:30 AM

Dungeness
Crab

6.75 inches

790 grams

6.5 inches

750 grams

6.875 inches

834 grams

102 grams





2013-SC-Biota-148

2013-SC-Biota-148-Crab

*

55.612985

-132.549471

5/27/2013

3:30 PM

Dungeness
Crab

6.5 inches

689 grams

6.25 inches

625 grams

6.25 inches

614 grams

99 grams

Collected a field duplicate; 2013-SC-
Biota-9148 at 13:35

Moved location to match crab

2013-SC-Biota-148

2013-SC-Biota-9148-Crab

*

55.612985

-132.549471

5/27/2013

1:35 PM

Dungeness
Crab

6.5 inches

796 grams

7.0 inches

1006 grams

6.375 inches

699 grams

108 grams

Duplicate of 148



2013-SC-Biota-149

2013-SC-Biota-149-Crab

*

55.613085

-132.548051

5/28/2013

2:49 PM

Dungeness
Crab

6.75 inches

886 grams

6.625 inches

883 grams

6.625 inches

933 grams

123 grams





2013-SC-Biota-150

2013-SC-Biota-150-Crab

*

55.610365

-132.551718

5/27/2013

3:55 PM

Dungeness
Crab

6.25 inches

608 grams

6.25 inches

596 grams

6.625 inches

759 grams

100 grams





2013SC-Biota-151

2013SC-Biota-151-Crab

*

55.609915

-132.546621

5/28/2013

3:28 PM

Dungeness
Crab

7.0 inches

917 grams

7.0 inches

990 grams

6.625 inches

858 grams

106 grams





2013SC-Biota-152

2013SC-Biota-152-Crab

*

55.616985

-132.553081

5/28/2013

3:20 PM

Dungeness
Crab

6.75 inches

909 grams

6.875 inches

871 grams

6.875 inches

827 grams

118 grams



Location moved to match where crab are

2013SC-Biota-153

2013SC-Biota-153-Crab

*

55.606145

-132.550691

5/27/2013

4:05 PM

Dungeness
Crab

6.75 inches

889 grams

6.5 inches

779 grams

6.875 inches

949 grams

100 grams





2013SC-Biota-500

2013SC-Biota-500-Crab

*

55.591775

-132.553171

5/29/2013

11:20 AM

Dungeness
Crab

7.0 inches

968 grams

6.625 inches

883 grams

7.0 inches

982 grams

120 grams





2013SC-Biota-502

2013SC-Biota-502-Crab

*

55.592745

-132.554331

5/29/2013

11:30 AM

Dungeness
Crab

7.25 inches

1090 grams

7.0 inches

966 grams

7.5 inches

1159 grams

123 grams





2013SC-Biota-504

2013SC-Biota-504-Crab

*

55.596985

-132.554161

5/29/2013

11:40 AM

Dungeness
Crab

6.75 inches

789 grams

7.0 inches

953 grams

7.0 inches

902 grams

121 grams





2013SC-Biota-506

2013SC-Biota-506-Crab

*

55.590285

-132.546901

5/29/2013

11:55 AM

Dungeness
Crab

6.5 inches

717 grams

7.0 inches

961 grams

6.75 inches

814 grams

NR*





2013SC-Biota-508

2013SC-Biota-508-Crab

*

55.589485

-132.545681

5/29/2013

12:00 PM

Dungeness
Crab

6.875 inches

785 grams

6.5 inches

830 grams

6.125 inches

681 grams

127 grams





Notes:

NR = not recorded - assumed to be > 100 grams
* Sample location outside of area surveyed for elevation

PAGE 1 OF 1


-------
TABLE 2-13
Marine Biota Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Sample
Type

Activity ID

Sample Date

Analytical Suite and Laboratory

Mercury
(A4 Scientific)

TAL Metals a
(A4 Scientific)

Arsenic Speciation
(Manchester Environmental Lab)

Lipids

(Manchester Environmental Lab)

BIOTA-107

N

2013SC-Biota-107-CR-20130525

5/25/2013

X

X

X

X

BIOTA-130

N

2013SC-Biota-130-CR-20130524

5/24/2013

X

X

X

X

BIOTA-138

N

2013SC-Biota-138-CR-20130522

5/22/2013

X

X

X

X

BIOTA-142

N

2013SC-Biota-142-CR-20130523

5/23/2013

X

X

X

X

BIOTA-148

N

2013SC-Biota-148-CR-20130527

5/27/2013

X

X

X

X

BIOTA-148

FD

2013SC-Biota-9148-CR-20130527FD

5/27/2013

X

X

X

X

BIOTA-149

N

2013SC-Biota-149-CR-20130528

5/28/2013

X

X

X

X

BIOTA-150

N

2013SC-Biota-150-CR-20130527

5/27/2013

X

X

X

X

BIOTA-151

N

2013SC-Biota-151-CR-20130528

5/28/2013

X

X

X

X

BIOTA-152

N

2013SC-Biota-152-CR-20130528

5/28/2013

X

X

X

X

BIOTA-153

N

2013SC-Biota-153-CR-20130527

5/27/2013

X

X

X

X

BIOTA-500

N

2013SC-Biota-500-CR-20130529

5/29/2013

X

X

X

X

BIOTA-502

N

2013SC-Biota-502-CR-20130529

5/29/2013

X

X

X

X

BIOTA-504

N

2013SC-Biota-504-CR-20130529

5/29/2013

X

X

X

X

BIOTA-506

N

2013SC-Biota-506-CR-20130529

5/29/2013

X

X

X

X

BIOTA-508

N

2013SC-Biota-508-CR-20130528

5/28/2013

X

X

X

X

Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium, silver, thallium, vanadium, zinc
N = normal environmental sample
FD = field duplicate

PAGE 1 OF 1


-------
TABLE 2-14

Groundwater Sample Information

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

Elevation
(feet NAVDSS)

Latitude

Longitude

Date

Time

Depth to

GW
(feet)

Total well depth
(feet)

Volume Purged

PH

Conductivity
(ms/cm)

Turbidity
(NTU)

DO
(mg/L)

Temperature
(deg. C)

ORP
(mV)

Salinity

(%)

Comments

Deviations

GW-01

2013SC-GW-01

24.6

55.626065

-132.555981

5/25/2013

11:55 AM

6.12

12.1

4,100 mL

5.67

0.14

15.7

0

10.28

89

0

Field Duplicate at 12:05; DO sensor may
have malfunctioned



GW-02

2013SC-GW-02

20.0

55.626075

-132.556981

5/26/2013

10:40 AM

5.65

8.33

0.4 gallons

5.18

0.226

62.9

4.79

9.28

213

0

Purged well dry 6 times during sampling
attempt. Only filled Metals bottles

Dissolved and total metals
analyses only due to
volume limitations

GW-03

2013SC-GW-03

20.1

55.626105

-132.556981

5/25/2013

11:20 AM

5.34

9.58

1.10 gallons

6.37

0.528

0

2

9.26

38

0

Turbidity flashing 0.0, slight sheen on purge
water



GW-04

2013SC-GW-04

23.0

55.626235

-132.556981

5/26/2013

10:10 AM

6.01

8.1

1,770 mL

6.64

0.419

519

0

10.14

-70

0

Fuel odor from purge water; DO sensor may
have malfunctioned; turbidity readings
jumping +/-12.0



GW-06

2013SC-GW-06

35.0

55.62642

-132.557266

5/26/2013

2:40 PM

3.8

4.92

1000 mL

5.34

0.91

-5

1.88

12.26

218

0

Turbidity flashing; colloidal material settling
in sample bottle

Sample not submitted due
to colloidal material

GW-05r

2013SC-GW-05







8/30/2013

11:15 AM

5.1

6.96

1.5 gallons

6.26

no readings

27.4

3.62

13.85

-26

not measured

No conductivity readings, sensor would not
calibrate. MS/MSD collected for metals and
DRO/RRO only. Field duplicate collected at
11:45

Water clear with slight petroleum odor.







































Notes:

mS/cm = millisiemens per centimeter
NTU = nephelometric turbidity unit
mg/L= milligrams per liter
deg. C = degrees Celsius
mV = millivolt
% = percent

PAGE 1 OF 1


-------
TABLE 2-15

Groundwater Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Location

Sample
Type

Activity ID

Sample Date

Analytical Suite and Laboratory

DRO/RRO
(Applied Sciences Laboratory)

Dissolved Mercury
(A4 Scientific)

Total Mercury
(A4 Scientific)

Dissolved TAL
Metals8 (A4
Scientific)

Total TAL Metals8
(A4 Scientific)

PAHs
(KAP Technologies)

GW-01

N

2013SC-GW-01-20130525

5/25/2013

X

X

X

X

X

X

GW-01

FD

2013SC-GW-901-201305 25FD

5/25/2013

X

X

X

X

X

X

GW-02

N

2013SC-GW-0 2-20130526

5/26/2013



X

X

X

X



GW-03

N

2013SC-GW-03-20130525

5/25/2013

X

X

X

X

X

X

GW-04

N

2013SC-GW-04-20130526

5/26/2013

X

X

X

X

X

X

GW-05R

N

2013SC-GW-05-20130830

8/30/2013

X

X

X

X

X

X

GW-05R

FD

2013SC-GW-905-20130830FD

8/30/2013

X

X

X

X

X

X

Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead, manganese, magnesium, nickel, selenium, silver, thallium, vanadium, zinc
N = normal environmental sample
FD = field duplicate

PAGE 1 OF 1


-------
TABLE 2-16

Equipment Rinsate Blank Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

QA/QC Type

Date

Time

Description

EB-05222013

2013SC-EB-05222013

Field Blank

5/22/2013

7:30 PM

Equipment blank for unused airstone and tubing - applicable to
porewater samples collected using airstones

EB-05282013

2013SC-EB-05282013

Field Blank

5/28/2013

4:00 PM

Equipment blank for unused pre-packed well screen - applicable
to porewater samples collected using drive-points

EB-05302013A

2013SC-EB-05302013A

Field Blank

5/30/2013

2:00 PM

Equipment blank for decontaminated Ponar used to collect
surface sediment samples - applicable to surface sediment
samples in thalweg

EB-05302013B

2013SC-EB-05302013B

Field Blank

5/30/2013

2:10 PM

Equipment blank for unused sample core tube and core catcher -
applicable to sediment boring samples

EB01_083013

2013SC-EB01-083013

Field Blank

8/30/2013

3:10 PM

Decontaminated direct-push sampling tube - applicable to all
sediment core samples

PAGE 1 OF 1


-------
TABLE 2-17

Equipment Rinsate Blank Analyses

2013 Salt Chuck Mine Superfund Site Field Data Report

Activity ID

Sample Date

Analytical Suite and Laboratory

Dissolved Metalsa
(A4 Scientific)

Total Metalsa
(A4 Scientific)

PAHs
(KAP Technologies)

2013SC-EB-05222013

5/22/2013

X





2013SC-EB-05282013

5/28/2013

X



X

2013SC-EB-05302013A

5/30/2013



X



2013SC-EB-05302013B

5/30/2013



X

X

2013SC-EB01-20130830

8/30/2013



X

X

Notes:

1 Activity ID is a combination of the sample ID, date sampled and sample type if field duplicate.

aTAL metals include aluminum, antimony, arsenic, barium, beryllium, cadmium, cobalt, chromium (total), copper, iron, lead,
manganese, magnesium, nickel, selenium, silver, thallium, vanadium, zinc

PAGE 1 OF 1


-------
TABLE 2-18
MS/MSD Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Location ID

Sample ID

QA/QC Type

Date

Time

Medium

Analyses

SB-004

2013SC-SB-004-00

MS/MSD

5/28/2013

7:00

Sediment

TOC, Metals, PAHs

SB-018

2013SC-SB-018-0.5

MS/MSD

5/27/2013

10:06

Sediment

Metals

SB-041

2013SC-SB-041-00

MS/MSD

5/25/2013

11:15

Sediment

Metals

SB-053

2013SC-SB-053-00

MS/MSD

5/25/2013

12:45

Sediment

Metals

SB-059

2013SC-SB-059-00

MS/MSD

5/27/2013

8:30

Sediment

TOC, CrVI, Metals, PAHs

SB-123

2013SC-SB-123-00

MS/MSD

5/23/2013

6:00

Sediment

Metals

SB-129

2013SC-SB-129-00

MS/MSD

5/23/2013

6:08

Sediment

TOC, Metals, PAHs

SB-301

2013SC-SB-301-01

MS/MSD

8/30/2013

9:15

Sediment

Metals

SB-303

2013SC-SB-303-12

MS/MSD

8/28/2013

10:45

Sediment

Metals

SB-304

2013SC-SB-304-04

MS/MSD

8/28/2013

08:57

Sediment

Metals

SB-305

2013SC-SB-305-0.5

MS/MSD

8/27/2013

14:00

Sediment

Metals

SB-306

2013SC-SB-306-07

MS/MSD

8/29/2013

9:15 AM

Sediment

Metals, PAHs

SB-308

2013SC-SB-308-08

MS/MSD

8/29/2013

1:15 PM

Sediment

Metals

SB-316

2013SC-SB-316-06

MS/MSD

8/28/2013

4:30 PM

Sediment

PAHs

BIOTA-149

2013SC-BIOTA-149-CR

MS/MSD

5/28/2013

2:49 PM

Tissue

Metals

BIOTA-152

2013SC-BIOTA-152-CR

MS/MSD

5/28/2013

3:20 PM

Tissue

Metals

BIOTA-506

2013SC-BIOTA-506-CR

MS/MSD

5/29/2013

11:55 AM

Tissue

Metals, Arsenic Speciation

GW-01

2013SC-GW-01

MS/MSD

5/25/2013

11:55 AM

Water

Total Metals

GW-05R

2013SC-GW-05R

MS/MSD

8/30/2013

11:15 AM

Water

Total and Dissolved Metals, DRO/RRO

PW-076

2013SC-PW-076

MS/MSD

5/26/2013

6:11AM

Water

Dissolved metals

SW-015

2013SC-SW-015

MS/MSD

5/25/2013

9:00 AM

Water

Dissolved metals

SW-099

2013SC-SW-099

MS/MSD

5/25/2013

8:10 AM

Water

Dissolved metals, PAHs

SW-106

2013SC-SW-106

MS/MSD

5/25/2013

9:40 AM

Water

Total and Dissolved metals

SW-501

2013SC-SW-501

MS/MSD

5/28/2013

1:00 PM

Water

Dissolved metals

SW-509

2013SC-SW-509

MS/MSD

5/28/2013

1:10 PM

Water

Dissolved metals

SW-600

2013SC-SW-600

MS/MSD

5/29/2013

11:10 AM

Water

Total metals

EB01 083013

2013SC-EB01-083013

MS/MSD

8/30/2013

3:10 PM

Water

Total Metals, PAHs

Notes:

PAHs = polycyclic aromatic hydrocarbons

DRO = diesel-range organics

RRO = residual-range organics

N = normal

FD = field duplicate

PAGE 1 OF 1


-------
TABLE 3-1

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Surface Sediment Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Group

Analyte3

Units

Number of
Detects

Number of
Samples

Frequency of
Detection

Nondetect Range
(MDL)

Detect Range

Screening Level lb

Screening Level 2C

Min

Max

Min

Max

Screening
Level

# Detects
Exceeding
Screening
Level

# Nondetects
Exceeding Screening
Level

Screening
Level

# Detects
Exceeding
Screening
Level

# Nondetects
Exceeding
Screening Level

Mercury

Mercury

mg/Kg

19

20

95%

0.0064

0.0064

0.023

0.16

0.15

1

-

0.71

-

-

TAL Metals

Aluminum

mg/Kg

20

20

100%

-

-

6,010

16,500

-

-

-

18,000

-

-

TAL Metals

Antimony

mg/Kg

-

20

0

0.32

0.75

-

-

-

-

-

9.3

-

-

TAL Metals

Arsenic

mg/Kg

2

20

10%

0.22

0.5

6.6

7.2

8.2

-

-

70

-

-

TAL Metals

Barium

mg/Kg

-

20

0

1.9

4.5

-

-

-

-

-

48

-

-

TAL Metals

Cadmium

mg/Kg

-

20

0

0.18

0.43

-

-

1.2

-

-

9.6

-

-

TAL Metals

Chromium

mg/Kg

7

20

35%

0.31

0.73

1.5

10

81

-

-

370

-

-

TAL Metals

Cobalt

mg/Kg

18

20

90%

0.21

0.37

7.5

30.8

-

-

-

10

14

-

TAL Metals

Copper

mg/Kg

20

20

100%

-

-

13.5

4,260

34

19

-

270

16

-

TAL Metals

Iron

mg/Kg

20

20

100%

-

-

13,400

63,100

-

-

-

22,000,000

-

-

TAL Metals

Lead

mg/Kg

2

20

10%

0.21

0.48

9

15

46.7

-

-

218

-

-

TAL Metals

Manganese

mg/Kg

20

20

100%

-

-

170

773

-

-

-

260

7

-

TAL Metals

Nickel

mg/Kg

16

20

80%

0

1

5.2

0,015

20.9

-

-

51.6

-

-

TAL Metals

Selenium

mg/Kg

3

20

15%

1.2

2.8

1.2

1.5

-

-

-

1

3

17

TAL Metals

Silver

mg/Kg

-

20

0

0.15

0.35

-

-

1

-

-

3.7

-

-

TAL Metals

Vanadium

mg/Kg

20

20

100%

-

-

29

135

-

-

-

57

8

-

TAL Metals

Zinc

mg/Kg

20

20

100%

-

-

22.3

60.6

150

-

-

410

-

-

Notes:

aOnly analytes with screening levels are listed

bScreening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

cScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

TAL = target analyte list
MDL = method detection limit
mg/kg = milligram per kilogram
# = number

PAGE 1 OF 1


-------
TABLE 3-2

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Marine Sediment Core and Test Pit Samples

2013 Salt Chuck Mine Superfund Site Field Data Report













Nondetect Range

























(MDL)

Detect Range



Screening Level lb



Screening Level 2C























# Detects

# Nondetects



# Detects

# Nondetects







Number of

Number of

Frequency of









Screening

Exceeding

Exceeding Screening



Exceeding

Exceeding

Group

Analyte9

Units

Detects

Samples

Detection

Min

Max

Min

Max

Level

Screening Level

Level

Screening Level

Screening Level

Screening Level

Mercury

Mercury

mg/kg

171

191

90%

0.0064

0.0077

0.0068

2.2

0.15

29

-

0.71

4

-

TAL Metals

Aluminum

mg/kg

191

191

100%

-

-

3,900

18,000

-

-

-

18,000

-

-

TAL Metals

Antimony

mg/kg

--

191

0%

0.034

0.49

--

--

--

--

--

9.3

--

--

TAL Metals

Arsenic

mg/kg

34

191

18%

0.11

0.33

0.69

9.5

8.2

3

--

70

--

--

TAL Metals

Barium

mg/kg

35

191

18%

0.2

2.9

2.8

36.1

--

--

--

48

--

--

TAL Metals

Cadmium

mg/kg

2

191

1%

0.019

0.28

0.79

1.2

1.2

--

--

9.6

--

--

TAL Metals

Chromium

mg/kg

83

191

43%

0.035

0.44

1

43.5

81

--

--

370

--

--

TAL Metals

Cobalt

mg/kg

185

191

97%

0.2

0.25

3

30.8

--

--

--

10

135

--

TAL Metals

Copper

mg/kg

189

191

99%

0.59

0.68

7.6

5,760

34

170

--

270

143

--

TAL Metals

Iron

mg/kg

191

191

100%

--

--

10,800

118,000

--

--

--

22,000,000

--

--

TAL Metals

Lead

mg/kg

51

191

27%

0.1

0.31

0.62

29.5

46.7

--

--

218

--

--

TAL Metals

Manganese

mg/kg

190

191

99%

0.16

0.16

117

555

--

--

--

260

82

--

TAL Metals

Nickel

mg/kg

180

191

94%

0.22

0.26

4.4

27.4

20.9

2

--

51.6

--

--

TAL Metals

Selenium

mg/kg

38

191

20%

0.12

1.8

0.26

5.8

--

--

--

1

21

96

TAL Metals

Silver

mg/kg

6

191

3%

0.016

0.23

0.64

6.7

1

1

--

3.7

1

--

TAL Metals

Vanadium

mg/kg

187

191

98%

0.44

0.91

17.8

159

--

--

--

57

91

--

TAL Metals

Zinc

mg/kg

191

191

100%

-

-

15.6

249

150

1

-

410

-

-

TCLPAHs

2-Methylnaphthalene

ug/kg

1

50

2%

1.7

1.7

4

4

70

--

--

670

--

--

TCLPAHs

Acenaphthene

ug/kg

4

50

8%

1.7

1.7

5.3

64

16

2

--

500

--

--

TCL PAHs

Acenaphthylene

ug/kg

31

50

62%

1.7

1.7

4.3

52

44

1

--

640

--

--

TCL PAHs

Anthracene

ug/kg

19

50

38%

1.7

1.7

3.9

67

85.3

--

--

1,100

--

--

TCL PAHs

Benz(a)anthracene

ug/kg

42

50

84%

1.7

1.7

5.7

350

261

1

--

1,600

--

--

TCL PAHs

Benzo(a)pyrene

ug/kg

42

50

84%

1.7

1.7

4.9

240

430

--

--

1,600

--

--

TCL PAHs

Chrysene

ug/kg

42

50

84%

1.7

1.7

4.5

220

384

--

--

2,800

--

--

TCL PAHs

Dibenz(a,h (anthracene

ug/kg

16

50

32%

1.7

1.7

3.4

28

63.4

--

--

260

--

--

TCL PAHs

Fluoranthene

ug/kg

46

50

92%

1.7

1.7

3.7

650

600

1

--

5,100

--

--

TCL PAHs

Fluorene

ug/kg

4

50

8%

1.7

1.7

4.7

11

19

--

--

540

--

--

TCL PAHs

HPAH

ug/kg

50

50

100%

--

--

9.7

2,608

1,700

1

--

9,600

--

--

TCL PAHs

LPAH

ug/kg

39

50

78%

1.7

1.7

4.3

184.2

552

--

--

3,160

--

--

TCL PAHs

Naphthalene

ug/kg

5

50

10%

1.7

1.7

4.2

12

160

--

--

2,100

--

--

TCL PAHs

Phenanthrene

ug/kg

27

50

54%

1.7

1.7

3.8

49

240

--

--

1,500

--

--

TCL PAHs

Pyrene

ug/kg

46

50

92%

1.7

1.7

5.1

580

665

--

--

2,600

--

--

TCL PAHs

TPAH

ug/kg

50

50

100%

-

-

9.7

2,706

4,022

-

-

44,792

-

-

Notes:

aOnly analytes with screening levels are listed

bScreening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

MDL = method detection limit

mg/kg = milligram per kilogram

TAL = target analyte list

# = number

ug/Kg = micrograms per kilogram

PAGE 10F 1


-------
TABLE 3-3

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Modified SPLP Sediment Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Group

Analyte8

Units

Number of
Detects

Number of
Samples

Frequency of
Detection

Nondetect Range (MDL)

Detect Range

Screening Levelb

Min

Max

Min

Max

Screening Level

ff Detects
Exceeding
Screening Level

# Nondetects

Exceeding
Screening Level

Modified SPLP

Antimony

ug/L

--

31

0

S.S

8.8

--

--

500

--

--

Modified SPLP

Arsenic

ug/L

--

31

0

2.5

2.5

--

--

36

--

--

Modified SPLP

Barium

ug/L

31

31

100%

--

--

40

190

200

--

--

Modified SPLP

Beryllium

ug/L

--

31

0

2

2

--

--

100

--

--

Modified SPLP

Cadmium

ug/L

--

31

0

1.4

1.5

--

--

8.8

--

--

Modified SPLP

Chromium

ug/L

--

31

0

6.8

6.8

--

--

27.4

--

--

Modified SPLP

Cobalt

ug/L

3

31

10%

8.6

8.6

2.7

54

1

3

28

Modified SPLP

Copper

ug/L

19

31

61%

2.1

2.1

14

472

3.1

19

--

Modified SPLP

Iron

ug/L

3

31

10%

7.8

7.8

160

5,170

50

3

--

Modified SPLP

Lead

ug/L

--

31

0

1.9

2

--

--

8.1

--

--

Modified SPLP

Manganese

ug/L

11

31

35%

7.2

7.3

32

160

100

1

--

Modified SPLP

Mercury

ug/L

--

31

0

0.0088

0.0088

--

--

0.94

--

--

Modified SPLP

Nickel

ug/L

--

31

0

1.3

1.3

--

--

8.2

--

--

Modified SPLP

Selenium

ug/L

--

31

0

2.3

2.3

--

--

71

--

--

Modified SPLP

Silver

ug/L

--

31

0

1.2

1.2

--

--

0.95

--

31

Modified SPLP

Thallium

ug/L

--

31

0

0.94

0.95

--

--

17

--

--

Modified SPLP

Vanadium

ug/L

4

31

13%

2

2

7.2

31

50

--

--

Modified SPLP

Zinc

ug/L

30

31

97%

1.7

1.7

16

95

81

6

--

Notes:

a Only analytes with screening levels are listed

b Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of preference:
a = Marine chronic
b = Marine acute

ug/L = micrograms per liter

SPLP = synthetic precipitation leaching procedure

MDL = method detection limit

# = number

PAGE 1 OF 1


-------
TABLE 3-4

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Upland Core and Test Pit Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Group

Analyte3

Units

Number of
Detects

Number of
Samples

Frequency of
Detection

Nondetect Range
(MDL)

Detect Range

Screening Levelb

Min

Max

Min

Max

Screening
Level

# Detects
Exceeding
Screening
Level

# Nondetects
Exceeding
Screening Level

Chrome VI

Chromium(VI)

mg/kg

-

3

0%

0.031

0.14

-

-

0.29

-

-

Mercury

Aluminum

mg/kg

16

16

100%

-

-

5,410

32,600

77,000

-

-

TAL Metals

Antimony

mg/kg

-

16

0%

0

0

-

-

31

-

-

TAL Metals

Arsenic

mg/kg

-

16

0%

0.22

0.30

-

-

0.39

-

-

TAL Metals

Barium

mg/kg

-

16

0%

1.90

2.70

-

-

15,000

-

-

TAL Metals

Beryllium

mg/kg

-

16

0%

0.3

0.4

-

-

160

-

-

TAL Metals

Cadmium

mg/kg

-

16

0%

0.18

0.26

-

-

70

-

-

TAL Metals

Chromium

mg/kg

8

16

50%

0.31

0.44

0.36

0.93

0.29

8

8

TAL Metals

Cobalt

mg/kg

16

16

100%

-

-

11.3

42.5

23

1

-

TAL Metals

Copper

mg/kg

16

16

100%

-

-

84.9

2,270

3,100

-

-

TAL Metals

Iron

mg/kg

16

16

100%

-

-

27,900

56,500

55,000

1

-

TAL Metals

Lead

mg/kg

1

16

6%

0

0

16.5

16.5

400

-

-

TAL Metals

Manganese

mg/kg

16

16

100%

-

-

187

824

1,800

-

-

TAL Metals

Mercury

mg/kg

16

16

100%

-

-

0.032

1

10

-

-

TAL Metals

Nickel

mg/kg

12

16

75%

0.25

0.32

4.9

17.4

1,500

-

-

TAL Metals

Selenium

mg/kg

-

16

0%

1.2

1.7

-

-

390

-

-

TAL Metals

Silver

mg/kg

-

16

0%

0.15

0.21

-

-

390

-

-

TAL Metals

Thallium

mg/kg

-

16

0%

0.16

0.23

-

-

0.78

-

-

TAL Metals

Vanadium

mg/kg

16

16

100%

-

-

41.4

201

390

-

-

TAL Metals

Zinc

mg/kg

16

16

100%

-

-

21.6

83.2

23,000

-

-

Notes:

aOnly analytes with screening levels are listed
b Screening Level = Residential Soil RSLs (EPA, 2013)

MDL = method detection limit
mg/kg = milligram per kilogram
TAL = target analyte list
# = number

PAGE 1 OF 1


-------
TABLE 3-5

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Porewater Sample*

2013 Salt Chuck Mine Superfund Site Field Data Report













Nondetect Range





















(MDL)

Detect Range



Screening Levelb























# Detects

# Nondetects







Number of

Number of

Frequency of











Exceeding

Exceeding

Group

Analyte3

Units

Detects

Samples

Detection

Min

Max

Min

Max

Screening Level

Screening Level

Screening Level

Hg_Dissolved

Mercury

ug/L

6

50

12%

0.034

0.034

0.034

0.047

0.94

-

-

TAL Metals_Diss

Antimony

ug/L

--

50

0

0.085

1.7

--

--

500

--

--

TAL Metals_Diss

Arsenic

ug/L

--

50

0

0.079

1.6

--

--

36

--

--

TAL Metals_Diss

Barium

ug/L

14

50

28%

5.6

5.6

201

425

200

14

--

TAL Metals_Diss

Beryllium

ug/L

--

50

0

0.051

1

--

--

100

--

--

TAL Metals_Diss

Cadmium

ug/L

--

50

0

0.069

1.4

--

--

8.8

--

--

TAL Metals_Diss

Chromium

ug/L

--

50

0

0.11

2.2

--

--

27.4

--

--

TAL Metals_Diss

Cobalt

ug/L

--

50

0

0.038

0.76

--

--

1

--

--

TAL Metals_Diss

Copper

ug/L

22

50

44%

0.98

0.98

48.2

664

3.1

22

--

TAL Metals_Diss

Iron

ug/L

22

50

44%

25.6

25.6

85.7

34,400

50

22

--

TAL Metals_Diss

Lead

ug/L

--

50

0

0.021

0.42

--

--

8.1

--

--

TAL Metals_Diss

Manganese

ug/L

36

50

72%

4

4

13.9

590

100

16

--

TAL Metals_Diss

Nickel

ug/L

--

50

0

0.049

0.98

--

--

8.2

--

--

TAL Metals_Diss

Selenium

ug/L

3

50

6%

30

30

2.6

49.3

71

--

--

TAL Metals_Diss

Silver

ug/L

--

50

0

0.033

0.66

--

--

0.95

--

--

TAL Metals_Diss

Thallium

ug/L

--

50

0

0.036

0.72

--

--

17

--

--

TAL Metals_Diss

Vanadium

ug/L

--

50

0

0.15

3

--

--

50

--

--

TAL Metals Diss

Zinc

ug/L

37

50

74%

12

12

42.3

240

81

14

-

TCLPAHs

2-Methyl naphthalene

ug/L

--

7

0

0.1

0.1

--

--

300

--

--

TCLPAHs

Acenaphthene

ug/L

--

7

0

0.05

0.05

--

--

40

--

--

TCLPAHs

Acenaphthylene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Anthracene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Benz(a)anthracene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Benzo(a)pyrene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Benzo(b)fluoranthene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Benzo(ghi)perylene

ug/L

1

7

14%

0.05

0.05

0.13

0.13

300

--

--

TCLPAHs

Benzo(k)fluoranthene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Chrysene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Dibenz(a,h)anthracene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Fluoranthene

ug/L

1

7

14%

0.05

0.05

0.13

0.13

11

--

--

TCLPAHs

Fluorene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

HPAH

ug/L

2

7

29%

0.05

0.05

0.13

0.31

300

--

--

TCLPAHs

lndeno(l,2,3-cd)pyrene

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

LPAH

ug/L

--

7

0

0.05

0.05

--

--

300

--

--

TCLPAHs

Naphthalene

ug/L

--

7

0

0.05

0.05

--

--

1.4

--

--

TCLPAHs

Phenanthrene

ug/L

--

7

0

0.05

0.05

--

--

4.6

--

--

TCLPAHs

Pyrene

ug/L

1

7

14%

0.05

0.05

0.18

0.18

300

--

--

TCLPAHs

TPAH

ug/L

2

7

29%

0.1

0.1

0.13

0.31

300

--

--

Notes:

a Only analytes with screening levels are listed

bScreening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of preference:

a = Marine chronic
b = Marine acute

ug/L = micrograms per liter
MDL = method detection limit
TAL = target analyte list
Diss = dissolved

PAHs = polycylclic aromatic hydrocarbons
# = number

PAGE 1 OF 1


-------
TABLE 3-6

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Surface Water Samples

2013 Salt Chuck Mine Superfund Site Field Data Report				













Nondetect Range



















(MDL)

Detect Range



Screening Level























# Detects

# Nondetects







Number of

Number of

Frequency of









Screening

Exceeding

Exceeding

Group

Analyte3

Units

Detects

Samples

Detection

Min

Max

Min

Max

Level

Screening Level

Screening Level

TAL Metals_Diss

Antimony

ug/L



30

0%

0.85

1.7

--



500





TAL Metals_Diss

Arsenic

ug/L

3

30

10%

0.79

1.6

11.2

48.5

36

2



TAL Metals_Diss

Barium

ug/L

1

30

3%

2.8

5.6

6.2

6.2

200





TAL Metals_Diss

Beryllium

ug/L



30

0%

0.51

1

--



100





TAL Metals_Diss

Cadmium

ug/L

29

30

97%

0.004

0.004

0.017

0.086

8.8





TAL Metals_Diss

Chromium

ug/L

27

30

90%

0.13

0.18

0.14

0.22

27.4





TAL Metals_Diss

Cobalt

ug/L

30

30

100%

--

--

0.028

0.362

1





TAL Metals_Diss

Copper

ug/L

30

30

100%

--

--

0.287

22.5

3.1

7



TAL Metals_Diss

Iron

ug/L

25

30

83%

3

3

3.9

311

50

7



TAL Metals_Diss

Lead

ug/L

21

30

70%

0.005

0.008

0.006

0.065

8.1





TAL Metals_Diss

Manganese

ug/L

19

30

63%

4

4

4

80.8

100





TAL Metals_Diss

Mercury

ug/L

25

30

83%

0.034

0.034

0.034

0.093

0.94





TAL Metals_Diss

Nickel

ug/L

30

30

100%





0.146

0.717

8.2





TAL Metals_Diss

Selenium

ug/L

3

30

10%

0.2

0.2

0.21

0.34

71





TAL Metals_Diss

Silver

ug/L

12

30

40%

0.001

0.002

0.023

0.038

0.95





TAL Metals_Diss

Thallium

ug/L

29

30

97%

0.002

0.002

0.003

0.019

17





TAL Metals_Diss

Vanadium

ug/L

30

30

100%





1

3.7

50





TAL Metals Diss

Zinc

ug/L



30

0%

6

12





81





TAL Metals_Total

Antimony

ug/L



4

0%

1.7

1.7





500





TAL Metals_Total

Arsenic

ug/L

2

4

50%

1.6

1.6

27.7

35.2

36





TAL Metals_Total

Barium

ug/L

--

4

0%

5.6

5.6

--

--

200





TAL Metals_Total

Beryllium

ug/L

--

4

0%

1

1





100





TAL Metals_Total

Cadmium

ug/L

4

4

100%





0.023

0.055

8.8





TAL Metals_Total

Chromium

ug/L

4

4

100%





0.19

0.3

27.4





TAL Metals_Total

Cobalt

ug/L

4

4

100%





0.049

0.127

1





TAL Metals_Total

Copper

ug/L

4

4

100%





1.58

4.89

3.1

1



TAL Metals_Total

Iron

ug/L

4

4

100%





44.5

403

50

3



TAL Metals_Total

Lead

ug/L

4

4

100%





0.007

0.058

8.1





TAL Metals_Total

Manganese

ug/L

4

4

100%





4.5

13.4

100





TAL Metals_Total

Mercury

ug/L

1

4

25%

0.034

0.034

0.056

0.056

0.94





TAL Metals_Total

Nickel

ug/L

4

4

100%





0.143

0.312

8.2





TAL Metals_Total

Selenium

ug/L

1

4

25%

0.2

0.2

0.22

0.22

71





TAL Metals_Total

Silver

ug/L



4

0%

0.001

0.002





0.95





TAL Metals_Total

Thallium

ug/L

4

4

100%





0.005

0.008

17





TAL Metals_Total

Vanadium

ug/L

4

4

100%





1.3

3.5

50





TAL Metals Total

Zinc

ug/L

-

4

0%

12

12





81





TCLPAHs

2-Methylnaphthalene

ug/L



6

0%

0.1

0.1





300





TCLPAHs

Acenaphthene

ug/L



6

0%

0.05

0.05





40





TCLPAHs

Acenaphthylene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Anthracene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Benz(a)anthracene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Benzo(a)pyrene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Benzo(b)fluora nthene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Benzo(ghi)perylene

ug/L

2

6

33%

0.05

0.05

0.11

0.18

300





TCL PAHs

Benzo(k)fluora nthene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Chrysene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Dibenz(a,h)anthracene

ug/L



6

0%

0.05

0.05





300





TCLPAHs

Fluora nthene

ug/L



6

0%

0.05

0.05





11





TCL PAHs

Fluorene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

HPAH

ug/L

2

6

33%

0.05

0.05

0.11

0.18

300





TCL PAHs

lndeno(l,2,3-cd)pyrene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

LPAH

ug/L



6

0%

0.05

0.05





300





TCL PAHs

Naphthalene

ug/L



6

0%

0.05

0.05





1.4





TCL PAHs

Phenanthrene

ug/L



6

0%

0.05

0.05





4.6





TCL PAHs

Pyrene

ug/L



6

0%

0.05

0.05





300





TCL PAHs

TPAH

ug/L

2

6

33%

0.1

0.1

0.11

0.18

300





Notes:

aOnly analytes with screening levels are listed

b Screening Level = AWQ.C listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of preference:

a = Marine chronic
b = Marine acute

ug/L = micrograms per liter
MDL = method detection limit
TAL = target analyte list
Diss = dissolved

PAHs = polycylclic aromatic hydrocarbons
# = number

PAGE 1 OF 1


-------
TABLE 3-7

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Crab Tissue Samples

2013 Salt Chuck Mine Superfund Site Field Data Report

Group

Analyte3

Units

Number of
Detects

Number of
Samples

Frequency of
Detection

Nondetect Range
(MDL)

Detect Range

Screening Levelb

Min

Max

Min

Max

Screening
Level

# Detects
Exceeding
Screening
Level

# Nondetects
Exceeding
Screening Level

Mercury

Mercury

mg/Kg ww

16

16

100%

-

-

0.004

0.010

0.14

-

-

TAL Metals

Aluminum

mg/Kg ww

1

16

6%

1.26

2.02

4.81

4.81

1400

-

-

TAL Metals

Antimony

mg/Kg ww

0

16

0%

0.002

0.003

-

-

0.54

-

-

TAL Metals

Arsenic

mg/Kg ww

16

16

100%

-

-

2.87

6.72

0.0021

16

-

TAL Metals

Barium

mg/Kg ww

0

16

0%

0.116

0.184

-

-

270

-

-

TAL Metals

Beryllium

mg/kg ww



16

0%

0.126

0.202

-

-

2.7

-

-

TAL Metals

Cadmium

mg/Kg ww

1

16

6%

0.001

0.002

0.008

0.008

1.4

-

-

TAL Metals

Chromium

mg/Kg ww

7

16

44%

0.012

0.018

0.047

0.131

2000

-

-

TAL Metals

Cobalt

mg/kg ww

8

16

50%

0.001

0.001

0.00429

0.00823

0.41

-

-

TAL Metals

Copper

mg/Kg ww

16

16

100%

-

-

1.88

3.92

54

-

-

TAL Metals

Iron

mg/kg ww

3

16

19%

0.413

0.626

2.86

14.3

950

-

-

TAL Metals

Manganese

mg/Kg ww

16

16

100%

-

-

0.110

1.110

190

-

-

TAL Metals

Nickel

mg/Kg ww

5

16

31%

0.006

0.008

0.045

0.168

27

-

-

TAL Metals

Selenium

mg/Kg ww

16

16

100%

-

-

0.220

0.412

6.8

-

-

TAL Metals

Silver

mg/Kg ww

16

16

100%

-

-

0.015

0.092

6.8

-

-

TAL Metals

Thallium

mg/Kg ww

0

16

0%

0.001

0.001

-

-

0.014

-

-

TAL Metals

Vanadium

mg/Kg ww

3

16

19%

0.001

0.002

0.006

0.007

6.8

-

-

TAL Metals

Zinc

mg/Kg ww

16

16

100%

-

-

24.1

41.6

410

-

-

Notes:

aOnly analytes with screening levels are listed

b Lower of the two (carcinogenic vs. noncancer) fish tissue screening levels (EPA 2013).

MDL = method detection limit

mg/kg ww = milligram per kilogram wet weight

TAL = target analyte list

# = number

PAGE 1 OF 1


-------
TABLE 3-8

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Groundwater

2013 Salt Chuck Mine Superfund Site Field Data Report













Nondetect Range





















(MDL)

Detect Range



Screening Levelb'c























# Detects

























Exceeding

# Nondetects







Number of

Number of

Frequency of









Screening

Screening

Exceeding

Group

Analyte3

Units

Detects

Samples

Detection

Min

Max

Min

Max

Level

Level

Screening Level

DRO/RRO

Diesel range organics

ug/L

4

6

67%

16.4

17.2

112

1,640

1,500

1

-

DRO/RRO

Oil Range Organics

ug/L

6

6

100%

-

-

35.4

562

1,100

-

-

Hg_Tot

Mercury

ug/L

4

7

57%

0.034

0.034

0.16

0.23

0.94

-

-

Hg_Diss

Mercury

ug/L

4

7

57%

0.034

0.034

0.083

0.15

0.94

-

-

TAL Metals

Antimony

ug/L

-

7

0%

0.085

0.085

-

-

500

-

-

TAL Metals

Arsenic

ug/L

7

7

100%

-

-

0.6

11.2

36

-

-

TAL Metals

Barium

ug/L

7

7

100%

-

-

1.6

21.8

200

-

-

TAL Metals

Beryllium

ug/L

-

7

0%

0.051

0.051

-

-

100

-

-

TAL Metals

Cadmium

ug/L

3

7

43%

0.069

0.069

0.071

0.21

8.8

-

-

TAL Metals

Chromium

ug/L

5

7

71%

0.11

0.11

0.17

5.1

27.4

-

-

TAL Metals

Cobalt

ug/L

7

7

100%

-

-

1.1

6.9

1

7

-

TAL Metals

Copper

ug/L

5

7

71%

0.049

0.049

6.7

282

3.1

5

-

TAL Metals

Iron

ug/L

7

7

100%

-

-

979

9,280

50

7

-

TAL Metals

Lead

ug/L

2

7

29%

0.021

0.021

3.1

3.7

8.1

-

-

TAL Metals

Manganese

ug/L

7

7

100%

-

-

143

2,460

100

7

-

TAL Metals

Nickel

ug/L

5

7

71%

0.049

0.049

0.18

4.4

8.2

-

-

TAL Metals

Selenium

ug/L

-

7

0%

1.5

1.5

-

-

71

-

-

TAL Metals

Silver

ug/L

-

7

0%

0.033

0.033

-

-

0.95

-

-

TAL Metals

Thallium

ug/L

-

7

0%

0.036

0.036

-

-

17

-

-

TAL Metals

Vanadium

ug/L

7

7

100%

-

-

0.98

22.4

50

-

-

TAL Metals

Zinc

ug/L

7

7

100%

-

-

0.89

980

81

2

-

TAL Metals_Diss

Antimony

ug/L

-

7

0%

0.085

0.085

-

-

500

-

-

TAL Metals_Diss

Arsenic

ug/L

7

7

100%

-

-

0.55

10.6

36

-

-

TAL Metals_Diss

Barium

ug/L

7

7

100%

-

-

1.5

9.3

200

-

-

TAL Metals_Diss

Beryllium

ug/L

-

7

0%

0.051

0.051

-

-

100

-

-

TAL Metals_Diss

Cadmium

ug/L

1

7

14%

0.069

0.069

0.4

0.4

8.8

-

-

TAL Metals_Diss

Chromium

ug/L

5

7

71%

0.11

0.11

0.13

1.4

27.4

-

-

TAL Metals_Diss

Cobalt

ug/L

7

7

100%

-

-

1

2.8

1

6

-

TAL Metals_Diss

Copper

ug/L

2

7

29%

0.049

0.049

44.2

176

3.1

2

-

TAL Metals_Diss

Iron

ug/L

7

7

100%

-

-

808

6,560

50

7

-

TAL Metals_Diss

Lead

ug/L

-

7

0%

0.021

0.021

-

-

8.1

-

-

TAL Metals_Diss

Manganese

ug/L

7

7

100%

-

-

161

2,100

100

7

-

TAL Metals_Diss

Nickel

ug/L

5

7

71%

0.049

0.049

0.17

4.4

8.2

-

-

TAL Metals_Diss

Selenium

ug/L

-

7

0%

1.5

1.5

-

-

71

-

-

TAL Metals_Diss

Silver

ug/L

-

7

0%

0.033

0.033

-

-

0.95

-

-

TAL Metals_Diss

Thallium

ug/L

-

7

0%

0.036

0.036

-

-

17

-

-

TAL Metals_Diss

Vanadium

ug/L

7

7

100%

-

-

0.64

4.2

50

-

-

TAL Metals_Diss

Zinc

ug/L

6

7

86%

0.6

0.6

0.89

823

81

1

-

PAGE 1 OF 2


-------
TABLE 3-8

Comparison of Summarized Detect and Non-Detect MDL Results to Screening Levels - Groundwater

2013 Salt Chuck Mine Superfund Site Field Data Report

Group

Analyte3

Units

Number of
Detects

Number of
Samples

Frequency of
Detection

Nondetect Range
(MDL)

Detect Range

Screening Levelb,c

Min

Max

Min

Max

Screening
Level

# Detects
Exceeding
Screening
Level

# Nondetects
Exceeding
Screening Level

TCLPAHs

2-Methylnaphthalene

ug/L

2

6

33%

0.1

0.1

2.3

2.6

300

-

-

TCLPAHs

Acenaphthene

ug/L

6

6

100%

-

-

0.27

8.9

40

-

-

TCL PAHs

Acenaphthylene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Anthracene

ug/L

2

6

33%

0.05

0.05

0.29

0.34

300

-

-

TCL PAHs

Benz(a)anthracene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Benzo(a)pyrene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Benzo(b)fluoranthene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Benzo(ghi)perylene

ug/L

3

6

50%

0.05

0.05

0.15

0.15

300

-

-

TCL PAHs

Benzo(k)fluoranthene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Chrysene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Dibenz(a,h)anthracene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Fluoranthene

ug/L

3

6

50%

0.05

0.05

0.1

0.4

11

-

-

TCL PAHs

Fluorene

ug/L

6

6

100%

-

-

0.091

5.8

300

-

-

TCL PAHs

lndeno(l,2,3-cd)pyrene

ug/L

-

6

0%

0.05

0.05

-

-

300

-

-

TCL PAHs

Naphthalene

ug/L

4

6

67%

0.05

0.05

0.16

18

1.4

2

-

TCL PAHs

Phenanthrene

ug/L

2

6

33%

0.05

0.05

2.2

2.5

4.6

-

-

TCL PAHs

Pyrene

ug/L

3

6

50%

0.05

0.05

0.13

0.29

300

-

-

Notes:

a Only analytes with screening levels are listed

bScreening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of preference:
a = Marine chronic
b = Marine acute
cScreening Level for Petroleum = 18 AAC 75 Table C values
AAC = Alaska Administrative Code
ug/L = micrograms per liter
MDL = method detection limit
TAL = target analyte list
Diss = dissolved

PAHs = polycylclic aromatic hydrocarbons
# = number

PAGE 2 OF 2


-------
TABLE 4-1

Surface Sediment Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SS-139

SS-140

SS-140

SS-141

SS-141

SS-143

SS-144

SS-145

SS-146

SS-147

SS-181

SS-182

SS-183

SS-183

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











2013SC-SS-139-
00-20130529

2013SC-SS-140-
00-20130529

2013SC-SS-9140-
00-20130529FD

2013SC-SS-141-00
20130529

2013SC-SS-9141-
00-20130529FD

2013SC-SS-143-
00-20130529

2013SC-SS-144-
00-20130529

2013SC-SS-145-
00-20130529

2013SC-SS-146-00
20130529

2013SC-SS-147-
00-20130529

2013SC-SS-181-
00-20130529

2013SC-SS-182-
00-20130529

2013SC-SS-183-
00-20130529

2013SC-SS-9183-
00-20130529FD

Sample Type:











N

N

FD

N

FD

N

N

N

N

N

N

N

N

FD

Date Sampled:











05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

Depth (feet):











0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5









Screening Level





























ChemGroup



Analyte

Units

ERLa

ERMb





























AVS/SEM

AVS



umol/g

NE

NE



0.90

0.62









4.9

0.50











AVS/SEM

Cadmium

ug/L

NE

NE



9.67

6.84









8.64

18











AVS/SEM

Copper



ug/L

NE

NE



5,350

4,640









4,700

6,970











AVS/SEM

Lead



ug/L

NE

NE



44.1

28.4









48.7

85.6











AVS/SEM

Nickel



ug/L

NE

NE



51.2

51.3









45.2

118











AVS/SEM

Zinc



ug/L

NE

NE



449

328









328

840











AVS/SEM

Acid Volatile Sulfides

mg/Kg

NE

NE



28.7

19.8









158

16











AVS/SEM

Simultaneously Extracted Metals

umol/g

NE

NE



1.8

1.4









1.7

1.7











AVS/SEM

Simultaneously extracted metals/acid volatile sulfides

umol/g

NE

NE



2.0

2.2









0.34

3.3











Hg

Mercury

mg/Kg

0.15

0.71

0.059 J

0.037 J



0.049 J

0.046 J

0.055 J

0.064 J

0.096 J

0.12 J

0.07 J

0.044 J

0.12

0.068 J

0.065 J

TAL Metals

Aluminum

mg/Kg

NE

18,000

7,960

11,200



7,810

7,070

9,340

7,910

8,570

8,970

8,880

8,160

6,450

6,010

6,210

TAL Metals

Antimony

mg/Kg

NE

9.3

0.62 U

0.47 U



0.41 U

0.41 U

0.54 U

0.56 U

0.75 U

0.58 U

0.55 U

0.35 U

0.35 U

0.32 U

0.33 U

TAL Metals

Arsenic



mg/Kg

8.2

70

0.41 U

0.31 U



0.27 U

0.27 U

0.36 U

0.37 U

0.5 U

0.39 U

0.37 U

0.23 U

0.23 U

0.22 U

0.22 U

TAL Metals

Barium



mg/Kg

NE

48

3.7 U

2.8 U



2.5 U

2.4 U

3.3 U

3.3 U

4.5 U

3.5 U

3.3 U

2.1 U

2.1 U

1.9 U

2 U

TAL Metals

Beryllium



mg/Kg

NE

NE

0.47 U

0.36 U



0.31 U

0.31 U

0.42 U

0.43 U

0.58 U

0.45 U

0.42 U

0.27 U

0.27 U

0.25 U

0.25 U

TAL Metals

Cadmium

mg/Kg

1.2

9.6

0.35 U

0.26 U



0.23 U

0.23 U

0.31 U

0.31 U

0.43 U

0.33 U

0.31 U

0.2 U

0.2 U

0.18 U

0.18 U

TAL Metals

Calcium



mg/Kg

NE

NE

13,700

34,300



7,140

6,390

22,400

17,000

33,000

25,200

21,100

4,120

9,930

3,790

4,100

TAL Metals

Chromium

mg/Kg

81

370

0.6 U

10 J



2.8 J

0.39 U

0.53 U

0.54 U

0.73 U

0.57 U

0.53 U

0.33 U

0.34 U

0.31 U

0.31 U

TAL Metals

Cobalt



mg/Kg

NE

10

11.2 J

11.8



15.3

13 J

9.3 J

12.7 J

13.6 J

0.37 UJ

10 J

13.7 J

12.7 J

12.4 J

12.6 J

TAL Metals

Copper



mg/Kg

34

270

328 J

309 J



697 J

558 J

215 J

838 J

606 J

288 J

422 J

1,230 J

3,010 J

3,900 J

4,260 J

TAL Metals

Iron



mg/Kg

NE

22,000,000

25,900 J

31,500



30,000

27,500 J

25,000 J

27,800 J

34,700 J

25,100 J

29,700 J

40,800 J

37,400 J

41,600 J

44,200 J

TAL Metals

Lead



mg/Kg

46.7

218

0.39 U

0.29 UJ



0.26 UJ

0.26 U

0.35 U

0.35 U

0.48 U

0.37 U

0.35 U

0.22 U

0.22 U

0.21 U

0.21 U

TAL Metals

Magnesium

mg/Kg

NE

NE

9,420

11,900



9,420

8,330

9,130

9,640

10,100

9,060

9,280

9,290

7,760

7,020

7,270

TAL Metals

Manganese

mg/Kg

NE

260

212 J

261 J



249 J

221 J

249 J

226 J

255 J

244 J

233 J

241 J

271 J

243 J

251 J

TAL Metals

Nickel



mg/Kg

20.9

51.6

0.43 U

11



8.3

7

9.5

0.39 U

0.53 U

10.2

0.39 U

7.3

6.6

8.4

8.5

TAL Metals

Potassium

mg/Kg

NE

NE

1,330

935



858

737

1,150

1,150

1,530

1,220

1,120

53.1 U

53.6 U

49.2 U

49.9 U

TAL Metals

Selenium



mg/Kg

NE

1

2.3 U

1.7 U



1.5 U

1.5 U

2 U

2 U

2.8 U

2.1 U

2 U

1.3 U

1.3 J

1.2 J

1.5 J

TAL Metals

Silver



mg/Kg

1

3.7

0.29 U

0.22 U



0.19 U

0.19 U

0.25 U

0.26 U

0.35 U

0.27 U

0.26 U

0.16 U

0.16 U

0.15 U

0.15 U

TAL Metals

Sodium



mg/Kg

NE

NE

12,500

4,590



4,290

4,240

9,160

9,970

16,900

11,500

9,360

2,070

2,080

1,210

1,240

TAL Metals

Thallium



mg/Kg

NE

NE

0.31 U

0.23 U



0.2 U

0.2 U

0.27 U

0.28 U

0.38 U

0.29 U

0.28 U

0.17 U

0.17 U

0.16 U

0.16 U

TAL Metals

Vanadium

mg/Kg

NE

57

55.3 J

67.5 J



64.5 J

54.8 J

54.2 J

54 J

74.8 J

50.4 J

51.5 J

60.7 J

63.5 J

57 J

55.8 J

TAL Metals

Zinc



mg/Kg

150

410

30.4

45.8



33.5

28.1

37.7

30.7

38.7

36.7

34.6

27.2

23.7

22.3

22.6

Grain Size

Particle s

ze, 1 inch (25.40mm)

g

NE

NE

0

0

0

0







0

0











Grain Size

Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE

0

0

0

0







0

0











Grain Size

Particle s

ze, 2 inch, (50.80mm)

g

NE

NE

0

0

0

0







0

0











Grain Size

Particle s

ze, 3 inch, (76.20mm)

g

NE

NE

0

0

0

0







0

0











Grain Size

Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE

0

9.4

0

0







0

0











Grain Size

Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE

0

95

48

0







0

0











Grain Size

Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE

1.0

1.0

1.0

1.0







1.0

1.0











Grain Size

Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE

1.1

56

63

0







0

0











Grain Size

Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE

4.6

60

72

0.60







1.9

1.8











Grain Size

Particle s

ze, Sieve No. 140, 150 mesh, (0.106mm)

g

NE

NE

62

95

69

186







12

104











Grain Size

Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE

3.3

50

55

1.1







1.2

3.0











Grain Size

Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE

98

59

37

89







17

48











Grain Size

Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE

4.2

36

33

3.2







1.4

3.5











Grain Size

Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE

7.1

30

25

15







2.1

8.2











Grain Size

Sample Weight

g

NE

NE

385.4

578.4

473.7

408.1







167

314











Notes:

ug/L = micrograms per liter	BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

mg/L = milligrams per liter	Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

mg/Kg = milligrams per kilogram
g = grams

FD = field duplicate sample
N = normal sample

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

a Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

PAGE 1 OF 2


-------
TABLE 4-1

Surface Sediment Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SS-184

SS-185

SS-186

SS-187

SS-188

SS-189

SS-510

Area











Site

Site

Site

Site

Site

Site

Background

Activity ID:











2013SC-SS-184-00-
20130529

2013SC-SS-185-
00-20130530

2013SC-SS-186-
00-20130530

2013SC-SS-187-
00-20130530

2013SC-SS-188-
00-20130530

2013SC-SS-189-
00-20130530

2013SC-SB-510-00
20130527

Sample Type:











N

N

N

N

N

N

N

Date Sampled:











05/29/13

05/30/13

05/30/13

05/30/13

05/30/13

05/30/13

05/27/13

Depth (feet):











0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5









Screening Level















ChemGroup



Analyte

Units

ERLa

ERMb















AVS/SEM

AVS



umol/g

NE

NE













-3.20E-03

AVS/SEM

Cadmium

ug/L

NE

NE













9.68

AVS/SEM

Copper



ug/L

NE

NE













578

AVS/SEM

Lead



ug/L

NE

NE













87.2

AVS/SEM

Nickel



ug/L

NE

NE













89.4

AVS/SEM

Zinc



ug/L

NE

NE













552

AVS/SEM

Acid Volatile Sulfides

mg/Kg

NE

NE













0.854

AVS/SEM

Simultaneously Extracted Metals

umol/g

NE

NE













0.21

AVS/SEM

Simultaneously extracted metals/acid volatile sulfides

umol/g

NE

NE













1

Hg

Mercury

mg/Kg

0.15

0.71

0.062 J

0.16

0.094 J

0.023 J

0.05 J

0.053 J

0.0064 U

TAL Metals

Aluminum

mg/Kg

NE

18,000

6,610

16,500

9,230

9,140

6,820

9,420

7,680

TAL Metals

Antimony

mg/Kg

NE

9.3

0.34 U

0.38 U

0.34 U

0.38 U

0.42 U

0.38 U

0.33 U

TAL Metals

Arsenic



mg/Kg

8.2

70

0.22 U

0.25 U

0.23 U

6.6

7.2

0.25 U

0.22 U

TAL Metals

Barium



mg/Kg

NE

48

2 U

2.3 U

2.1 U

2.3 U

2.5 U

2.3 U

2 U

TAL Metals

Beryllium



mg/Kg

NE

NE

0.26 U

0.29 U

0.26 U

0.29 U

0.32 U

0.29 U

0.25 U

TAL Metals

Cadmium

mg/Kg

1.2

9.6

0.19 U

0.21 U

0.2 U

0.21 U

0.24 U

0.21 U

0.19 U

TAL Metals

Calcium



mg/Kg

NE

NE

2,280

23,200

16,000

4,840

2,640

3,980

22,500

TAL Metals

Chromium

mg/Kg

81

370

0.32 U

2.2 J

1.5 J

9.1 J

6.9 J

0.36 U

4.9 J

TAL Metals

Cobalt



mg/Kg

NE

10

12.9 J

30.8

15.6

7.5

8.9

15 J

0.21 U

TAL Metals

Copper



mg/Kg

34

270

1,570 J

2,000 J

1,570 J

172 J

168 J

495 J

13.5 J

TAL Metals

Iron



mg/Kg

NE

22,000,000

26,900 J

63,100

46,500

17,900

20,100

29,700 J

13,400

TAL Metals

Lead



mg/Kg

46.7

218

0.21 U

0.24 UJ

0.22 UJ

9.2 J

14.5 J

0.24 U

0.21 UJ

TAL Metals

Magnesium

mg/Kg

NE

NE

7,760

19,300

11,300

7,830

6,970

9,200

6,910

TAL Metals

Manganese

mg/Kg

NE

260

222 J

558 J

282 J

370 J

281 J

773 J

170 J

TAL Metals

Nickel



mg/Kg

20.9

51.6

7.4

14.9

8.5

6.6

5.5 J

8.7

5.2 J

TAL Metals

Potassium

mg/Kg

NE

NE

50.4 U

951

665

669

579 J

657

462 J

TAL Metals

Selenium



mg/Kg

NE

1

1.2 U

1.4 U

1.3 U

1.4 U

1.5 U

1.4 U

1.2 U

TAL Metals

Silver



mg/Kg

1

3.7

0.16 U

0.18 U

0.16 U

0.18 U

0.19 U

0.18 U

0.15 U

TAL Metals

Sodium



mg/Kg

NE

NE

1,390

2,610

1,860

5,460

4,760

3,050

2,230

TAL Metals

Thallium



mg/Kg

NE

NE

0.17 U

0.19 U

0.17 U

0.19 U

0.21 U

0.19 U

0.16 U

TAL Metals

Vanadium

mg/Kg

NE

57

51.4 J

135 J

71.5 J

40.7 J

50.9 J

68.7 J

29.4 J

TAL Metals

Zinc



mg/Kg

150

410

26

60.6

28.6

32.9

22.6

38.4

23.5

Grain Size

Particle s

ze, 1 inch (25.40mm)

g

NE

NE













0

Grain Size

Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE













0

Grain Size

Particle s

ze, 2 inch, (50.80mm)

g

NE

NE













0

Grain Size

Particle s

ze, 3 inch, (76.20mm)

g

NE

NE













0

Grain Size

Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE













10

Grain Size

Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE













94

Grain Size

Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE













1.0

Grain Size

Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE













141

Grain Size

Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE













77

Grain Size

Particle s

ze, Sieve No. 140, 150 mesh, (0.106mm)

g

NE

NE













15

Grain Size

Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE













47

Grain Size

Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE













3.1

Grain Size

Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE













25

Grain Size

Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE













14

Grain Size

Sample Weight

g

NE

NE













438.9

Notes:

ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

FD = field duplicate sample
N = normal sample

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

a Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL)

PAGE 2 OF 2


-------
TABLE 4-2

Sediment Toxicity Bioassay Results

2013 Salt Chuck Mine Superfund Site Field Data Report









Sample

Polychaete

Bivalve







Sample

Depth

Neanthes

Mytilus

Sample Description

Location

Area

Date

(feet)

arenaceodentata

galloprovincialis

13214112 (NAS #4424G/4534G)

SS-510

Background

05/27/13

0-0.5





13214126 (NAS #4425G)

SS-145

Site

05/29/13

0-0.5





13214127 (NAS #4426G)

SS-146

Site

05/29/13

0-0.5

••a,b
U



13214130 (NAS #4428G)

SS-140

Site

05/29/13

0-0.5



"C

U

13214133 (NAS #4430G)

SS-140 FD

Site

05/29/13

0-0.5



•• c
U

Notes:

Metals results for these samples are listed in Table 4-1

li = Significant effect seen when compared with the control sediment and/or reference area results.
a Statistically significant effect when compared to laboratory control but not reference area sediment.
b Statistically significant reduced growth, but no effect on survival.
c Statistically significant reduced larval development, but no effect on survival.

PAGE 1 OF 1


-------
TABLE 4-3

Agronomic Sediment Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:





SS-1S1

SS-182

SS-183

SS-183

SS-184

SS-185

SS-186

SS-187

SS-188

SS-189

Area





Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:





2013SC-SS-181-
20131529

2013SC-SS-182-
20131529

2013SC-SS-183-
20131529

2013SC-SS-9183-
20131529

2013SC-SS-184-
20131529

2013SC-SS-185-
20131530

2013SC-SS-186-
20131530

2013SC-SS-187-
20131530

2013SC-SS-188-
20131530

2013SC-SS-189-
20131530

Sample Type:





N

N

N

FD

N

N

N

N

N

N

Date Sampled:





05/29/13

05/29/13

05/29/13

05/29/13

05/29/13

05/30/13

05/30/13

05/30/13

05/30/13

05/30/13

Depth (feet):





0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

0-0.5

Soil Texture:





Loamy Sand

Sand

Sand

Sand

Sand

Loam

Loam

Loamy Sand

Loamy Sand

Loam

ChemGroup

Analyte

Units



Physical Characteristics

Sand

%

74

86

86

90

92

48

52

78

74

48

Physical Characteristics

Silt

%

20

8

6

4

2

40

38

14

16

40

Physical Characteristics

Clay

%

6

6

8

6

6

12

10

8

10

12

Nitrogen

Kjeldahl nitrogen

mg/kg

40 U

40 U

40 U

40 U

40 U

40 U

40 U

370

201

40 U

Soil Analysis

Boron

mg/kg

2.3

2.1

1.9

1.7

1.3

3.3

3.5

20.3

10.6

9.5

Soil Analysis

Calcium

mg/kg

633

1515

717

697

208

2054

2157

1362

848

690

Soil Analysis

Copper

mg/kg

216.0

283.0

293.0

277.0

210.0

244.0

282.0

126.0

60.5

191.0

Soil Analysis

Iron

mg/kg

13

13

25

22

8

2

9

60

99

15

Soil Analysis

Magnesium

mg/kg

279

268

201

228

266

299

278

1877

1223

905

Soil Analysis

Manganese

mg/kg

1

1

1

1

1

1

1

5

15

2

Soil Analysis

Nitrogen

mg/kg

3

5

5

51

79

8

7

22

9

12

Soil Analysis

Organic Matter

%

0.4

0.3

0.4

0.4

0.3

0.4

0.3

14.8

6.6

3.0

Soil Analysis

Phosphorus

mg/kg

8

9

6

7

4

2

3

22

19

13

Soil Analysis

Phosphorus, Weak Bray

mg/kg

19

8

12

13

23

2

1

20

21

9

Soil Analysis

Potassium

mg/kg

81

69

62

63

76

94

83

410

294

260

Soil Analysis

Sodium

mg/kg

1,313

1,191

1,016

1,151

1,381

1,429

1,310

9,614

7,632

3,092

Soil Analysis

Sulfur

mg/kg

122

118

85

97

119

135

125

479

385

280

Soil Analysis

Zinc

mg/kg

0.5

0.3

0.3

0.4

0.4

0.5

0.5

2.8

1.1

0.7

Cation Saturation

Calcium

%

27.8

50.0

36.5

33.1

11.0

53.5

56.8

10.4

8.0

13.8

Cation Saturation

Magnesium

%

20.2

14.6

16.9

17.8

23.2

12.8

12.1

23.7

19.0

29.8

Cation Saturation

Potassium

%

1.8

1.2

1.6

1.5

2.1

1.3

1.1

1.6

1.4

2.7

Cation Saturation

Sodium

%

50.2

34.3

45.0

47.6

63.8

32.4

30.1

64.3

62.6

53.8

Soil Salinity

Bicarbonate

meq/L

1.8

2.1

1.7

1.9

1.3

1.9

1.7

1.9

4.0

2.7

Soil Salinity

Boron

mg/kg

1.6

1.7

1.4

1.5

1.1

1.5

1.3

2.0

2.3

2.6

Soil Salinity

Calcium

meq/L

5.3

6.4

3.8

4.1

3.7

7

5.2

3.2

7.4

7.9

Soil Salinity

Carbonate

meq/L

0

0

0

0

0

0

0

0

0

0

Soil Salinity

Chloride

meq/L

110

150

72.5

91.5

81.5

136.5

92.5

82.0

211.4

212.9

Soil Salinity

EC

dS/m

13.5

12.4

10.5

7.4

8.5

14.0

15.9

23.4

25.5

20.1

Soil Salinity

ESP

none

34.7

37.2

19.7

32.2

19.1

38.0

18.5

20.0

41.0

42.0

Soil Salinity

Magnesium

meq/L

17.0

21.1

13.2

14.6

13.7

20.1

13.4

10.8

24.9

28.0

Soil Salinity

PH

none

7.7

8.1

8.1

8.0

7.5

8.1

8.3

7.0

6.4

7.1

Soil Salinity

SAR

none

36.8

41.1

17.5

33.0

16.8

42.4

16.2

17.8

47.9

50.0

Soil Salinity

Saturation

%

30.1

27.9

31.0

29.9

31.6

35.1

30.3

101.7

77.4

39.8

Soil Salinity

Sodium

meq/L

123.1

152.4

51.1

101.0

49.6

156.2

49.5

47.1

192.9

211.9

Notes:

Metals results for these samples are listed in Table 4-1
J = The analyte was positively identified; the quantitation is an estimation.
meq/L = milliequivalents per liter
mg/kg = milligrams per kilogram

U = The analyte was analyzed for, but not detected at the method reporting limit shown

PAGE 1 OF 1


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:













SB-004

SB-004

SB-004

SB-013

SB-013

SB-018

SB-018

SB-021

SB-021

SB-031

SB-031

SB-031

SB-031

SB-032

SB-032

SB-033

SB-033

SB-043

SB-043

SB-043

SB-052

SB-052

Area













Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:













2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-













004-0_5-

004-00-

9004-0_5-

013-0_5-

013-00-

018-0_5-

018-00-

021-0_5-

021-00-

031-0_5-

031-00-

031-01-

9031-00-

032-0_5-

032-00-

033-0_5-

033-00-

043-0_5-

043-00-

043-01-

052-0_5-

052-00-















20130528

20130528

20130528FD

20130528

20130528

20130527

20130527

20130528

20130528

20130528

20130528

20130528

20130528FD

20130527

20130527

20130527

20130527

20130527

20130527

20130527

20130528

20130528

Sample Type:













N

N

FD

N

N

N

N

N

N

N

N

N

FD

N

N

N

N

N

N

N

N

N

Date Sampled:













05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/28/13

05/28/13

Depth (feet):













0.5 -1

0-0.5

0.5 -1

0.5 -1

0-0.5

0.5 -1

0-0.5

0.5 -1

0-0.5

0.5 -1

0-0.5

1-2

0-0.5

0.5 -1

0-0.5

0.5 -1

0-0.5

0.5-1

0-0.5

1-2

0.5 -1

0-0.5











Screening Level













































ChemGroup





Analyte

Units

ERLa

ERMb













































Metals, Chrome VI



Chromiur

n VI

mg/Kg

NE

NE













































Metals, Hg



Mercury



mg/Kg

0.15

0.71

0.11 J

0.076 J

0.13

0.4

0.12

0.17

0.064 J

0.052 J

0.17

0.11 J

0.091 J

0.21

0.15

0.1 J

0.068 J

0.14

0.12 J

0.13

0.11 J

0.13

0.19

0.063 J

TAL Metals



Aluminun

i

mg/Kg

NE

18,000

7,310

6,940

7,280

5,410

5,370

7,240

9,580

6,830

7,620

7,980

7,630

15,000

8,020

6,300

6,620

9,320

9,050

12,200

12,500

8,110

4,190

4,170

TAL Metals



Antimony

mg/Kg

NE

9.3

0.36 U

0.36 U

0.35 U

0.35 U

0.36 U

0.36 U

0.34 U

0.36 U

0.41 U

0.35 U

0.41 U

0.36 U

0.42 U

0.41 U

0.39 U

0.34 U

0.46 U

0.36 U

0.34 U

0.34 U

0.35 U

0.34 U

TAL Metals



Arsenic



mg/Kg

8.2

70

0.24 U

0.24 U

0.23 U

0.23 U

0.24 U

0.24 U

0.23 U

6.5

0.27 U

0.23 U

0.28 U

0.24 U

0.28 U

0.28 U

0.26 U

0.23 U

0.3 U

0.24 U

0.23 U

0.22 U

0.23 U

0.23 U

TAL Metals



Barium



mg/Kg

NE

48

2.1 U

2.2 U

2.1 U

2.1 U

2.1 U

2.2 U

14.6 J

2.2 U

2.4 U

2.1 U

2.5 U

2.2 U

2.5 U

18.4 J

7.2 J

2 U

2.7 U

11.1 J

12.1 J

17.1 J

2.1 U

2.1 U

TAL Metals



Beryllium



mg/Kg

NE

NE

0.27 U

0.28 U

0.27 U

0.26 U

0.27 U

0.28 U

0.26 U

0.28 U

0.31 U

0.27 U

0.32 U

0.28 U

0.32 U

0.32 U

0.3 U

0.26 U

0.35 U

0.28 U

0.26 U

0.26 U

0.27 U

0.26 U

TAL Metals



Cadmium



mg/Kg

1.2

9.6

0.2 U

0.21 U

0.2 U

0.2 U

0.2 U

0.2 U

0.19 U

0.2 U

0.23 U

0.2 U

0.23 U

0.21 U

0.24 U

0.23 U

0.22 U

0.19 U

0.26 U

0.2 U

0.2 U

0.19 U

0.2 U

0.2 U

TAL Metals



Calcium



mg/Kg

NE

NE

3,350

3,270

3,250

2,500

2,620

3,940 J

5,080 J

2,650

3,160

5,860

3,590

14,700

3,890

2,810 J

2,900 J

13,300

4,710

18,200 J

17,200 J

14,500 J

1,960

1,850

TAL Metals



Chromiur

n

mg/Kg

81

370

0.34 U

0.35 U

0.34 U

1.2 J

1.3 J

1.5 J

2 J

1.1 J

1.1 J

1.7 J

2.5 J

1.9 J

2.5 J

2.3 J

2 J

0.33 U

0.44 U

2.5 J

1.5 J

1.3 J

0.34 U

0.33 U

TAL Metals



Cobalt



mg/Kg

NE

10

13.5 J

13 J

14.3 J

12.5

12.5

16.1

16.8

17.6

14.8

25

16.8

30.8

17.9

12.6

11.3

22.1 J

17.3 J

18.5

17.6

19.6

10.5 J

10.1 J

TAL Metals



Copper



mg/Kg

34

270

3,870 J

2,620 J

3,830 J

4,060

2,600

5,010

1,710

5,760

690

1,070 J

1,220 J

1,170 J

1,350 J

658

636

3,610 J

946 J

1,040

913

1,470

745 J

1,520 J

TAL Metals



Iron



mg/Kg

NE

22,000,000

29,200

32,000 J

31,600

118,000 J

109,000 J

27,200 J

46,000 J

63,700 J

55,400 J

31,400

49,400

59,900

55,000

31,000 J

35,900 J

42,400

52,900

56,600 J

53,000 J

45,000 J

48,600

33,200

TAL Metals



Lead



mg/Kg

46.7

218

0.23 U

0.23 U

6.3

0.22 U

7.3

0.23 U

3.8 J

0.23 U

7

0.22 UJ

15.2 J

0.23 UJ

0.26 UJ

14

9.6

0.22 U

0.29 U

0.72 J

0.65 J

0.64 J

29.5

0.22 U

TAL Metals



Magnesium

mg/Kg

NE

NE

8,140

7,800

8,130

6,370

6,270

7,670

10,400

7,520

8,520

10,200

8,940

18,700

9,440

7,540

7,860

10,600

10,400

13,600

13,500

9,750

5,140

5,140

TAL Metals



Manganese

mg/Kg

NE

260

219 J

207 J

229 J

180 J

183 J

293

277

228 J

223 J

406 J

237 J

509 J

247 J

209

178

395 J

265 J

336

317

352

184 J

166 J

TAL Metals



Nickel



mg/Kg

20.9

51.6

7.4

7.1

7.7

6

5.9

8.8

8.8

7.8

6.2 J

11.3

9.1

13.8

10.2

6.5 J

5.9 J

11.3

9.3

10.5

8.6

10.3

0.24 U

0.24 U

TAL Metals



Potassiur

n

mg/Kg

NE

NE

511 J

55.5 U

432 J

311 J

353 J

584 J

704

587 J

480 J

770

681 J

1,360

675 J

733

578 J

621

763

887

989

740

346 J

347 J

TAL Metals



Selenium



mg/Kg

NE

1

1.4 J

1.3 U

1.4 J

3.5 J

2.7 J

1.5 J

1.2 U

5.8 J

1.5 U

1.3 U

1.5 U

1.3 U

1.5 U

1.5 U

1.4 U

2.2 J

1.7 U

1.5 J

1.3 U

1.2 U

1.3 U

1.3 U

TAL Metals



Silver



mg/Kg

1

3.7

0.17 U

0.17 U

0.16 U

0.16 U

0.17 U

0.17 U

0.16 U

6.7

0.19 U

0.16 U

0.19 U

0.17 U

0.19 U

0.19 U

0.18 U

0.16 U

0.21 U

0.17 U

0.16 U

0.16 U

0.16 U

0.16 U

TAL Metals



Sodium



mg/Kg

NE

NE

937

1,970

806

1,480

1,880

895

1,550

96.7 J

188 J

1,210

3,550

1,720

3,400

3,190

2,860

1,820

3,060

1,970

2,020

847

2,320

1,810

TAL Metals



Thallium



mg/Kg

NE

NE

0.18 U

0.18 U

0.17 U

0.17 U

0.18 U

0.18 U

0.17 U

0.18 U

0.2 U

0.18 U

0.21 U

0.18 U

0.21 U

0.21 U

0.19 U

0.17 U

0.23 U

0.18 U

0.17 U

0.17 U

0.17 U

0.17 U

TAL Metals



Vanadiurr



mg/Kg

NE

57

58.5 J

61.1 J

62.6 J

88.9

78

65.7

77

76.5

80.6

123 J

114 J

159 J

122 J

59.7

49.6

108 J

87.7 J

94.5

84.7

101

53.7 J

50.6 J

TAL Metals



Zinc



mg/Kg

150

410

56

43.1

72.3

25.6

25.6

30.5

60

32.9

30.1

46.3

34.4

56.2

36.1

35

24.7

42

37.6

33.9

33

35.2

24.4

20.9

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

32

12

10

14

37





16

10









15

6.6

46

7.5







56

8.5

TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

26

14

14

24

22





6.6

8.8









15

8

110

8.1







46

9.4

TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

21

9.7

13

19

17





6.2

6.9









13

5.8

80

6.5







37

7.8

TCL PAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

25

20

18

28

18





12

16









16

9.7

71

13







41

9.5

TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

15

7.6

7.5

11

12





4.5

5.5









8.7

4.3 J

62

5







31

4.9

TCL PAHs

HPAH

Chrysene



ug/Kg

384

2,800

23

9.9

8.4

9.1

29





6.8

9.1









12

4.9

39

6.2







44

5.9

TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

4 J

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U









1.7 U

1.7 U

10

1.7 U







8.6

1.7 U

TCL PAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

65

13

9.5

9.5

46





35

12









41

7.8

66

12







78

9.7

TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

18

10

11

14

16





4.4

7.3









9.5

5

55

6.6







34

6.9

TCL PAHs

HPAH

Pyrene



ug/Kg

665

2,600

59

19

15

11

49





32

16









34

11

110

17







86

11

TCL PAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

288

115.2

106.4

139.6

246





123.5

91.6









164.2

63.1

649

81.9







461.6

73.6

TCL PAHs

LPAH

Acenaphthene

ug/Kg

16

500

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U









5.3

1.7 U

1.7 U

1.7 U







1.7 U

1.7 U

TCL PAHs

LPAH

Acenaphthylene

ug/Kg

44

640

6.6

7

5.3

4.9

7.9





1.7 U

6.3









1.7 U

1.7 U

23

4.5







16

1.7 U

TCL PAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

7.5

1.7 U

1.7 U

1.7 U

6.5





1.7 U

1.7 U









1.7 U

1.7 U

8.6

1.7 U







8.2

1.7 U

TCL PAHs

LPAH

Fluorene



ug/Kg

19

540

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U









1.7 U

1.7 U

1.7 U

1.7 U







1.7 U

1.7 U

TCL PAHs

LPAH

Naphthalene

ug/Kg

160

2,100

4.2 J

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U









1.7 U

1.7 U

1.7 U

1.7 U







1.7 U

1.7 U

TCL PAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

23

8.2

4.5

6.8

7.4





5.2

9.7









6.7

1.7 U

10

4.3







17

1.7 U

TCL PAHs

LPAH

Total LPAH

ug/kg

552

3,160

41.3

15.2

9.8

11.7

21.8





5.2

16









12

1.7 U

41.6

8.8







41.2

1.7 U

TCL PAHs

TPAH

Total PAH

ug/kg

4,022

44,792

329.3

130.4

116.2

151.3

267.8





128.7

107.6









176.2

63.1

690.6

90.7







502.8

73.6

TCL PAHs



2-Methylnaphthalene

ug/Kg

70

670

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U









1.7 U

1.7 U

1.7 U

1.7 U







1.7 U

1.7 U

Genchem, TOC



Organic carbon

mg/Kg

NE

NE

910 J

520 J

980 J

550 J

1,800 J





1,100 J

5,500 J









7,600 J

5,500 J

1,100 J

3,000 J







870 J

230 J

Genchem



Total solids

%

NE

NE

83.7

82.4

81.6

84.6

81.8





81.1

72.5









71.1

74.2

82.1

79.4







82.8

85.7

BulkDensity



Bulk Density

g/cm3

NE

NE

2.22

2.29

2.17

2.44

2.30





2.29











2.00

2.00

2.19

2.10







2.39

2.39

Grain Size



Particle s

ze, 1 inch (25.40mm)

g

NE

NE

0.00

0.00

0.00

0.00

0.00





0.00











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE

0.00

0.00

0.00

0.00

0.00





0.00











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, 2 inch, (50.80mm)

g

NE

NE

0.00

0.00

0.00

0.00

0.00





0.00











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, 3 inch, (76.20mm)

g

NE

NE

0.00

0.00

0.00

0.00

0.00





0.00











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE

0.00

0.00

0.00

0.00

0.00





0.00











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE

10.30

0.00

5.60

0.00

0.00





5.90











0.00

0.00

0.00

0.00







0.00

0.00

Grain Size



Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE

1.00

1.00

1.00

1.00

1.00





1.00











1.00

1.00

1.01

1.00







1.00

1.00

Grain Size



Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE

1.00

1.00

1.00

1.00

1.00





1.00











1.00

1.00

1.01

1.00







1.00

1.00

Grain Size



Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE

1.00

1.00

1.00

1.00

1.00





1.00











1.00

1.00

1.01

1.01







1.00

1.00

Grain Size



Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE

1.00

1.00

1.00

1.00

1.00





1.00











1.01

1.00

1.01

1.01







1.00

1.00

Grain Size



Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE

1.01

1.01

1.01



1.01





1.01











1.01

1.01

1.02

1.01







1.00



Grain Size



Particle s

ze, Hydrometer (.041 mm)

mg/L

NE

NE







1.01



































1.00

Grain Size



Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE

1.00

1.00

1.00

1.00

1.00





1.00











1.00

1.00

1.00

1.00







1.00

1.00

Grain Size



Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE

0.10

0.00

0.30

0.00

0.30





0.00











0.00

0.00

0.00

0.50







0.50

0.40

Grain Size



Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE

1.40

0.80

1.70

0.00

0.30





3.40











0.40

0.00

0.00

0.50







3.10

1.70

Grain Size



Particle s

ze, Sieve No. 140,150 mesh, (0.106mm)

g

NE

NE

170.50

194.63

143.90

244.92

201.65





169.54











163.26

174.64

24.29

135.23







261.17

271.40

Grain Size



Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE

2.71

2.00

1.04

0.82

0.35





6.33











0.77

0.72

0.00

0.75







2.34

2.34

Grain Size



Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE

78.87

77.53

71.43

62.56

59.18





75.92











63.68

69.86

46.27

100.02







57.30

60.83

Grain Size



Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE

10.44

9.59

6.56

11.04

5.32





25.31











9.65

7.56

0.58

1.87







15.20

13.26

Grain Size



Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE

36.73

42.76

28.99

65.42

42.17





63.26











42.84

38.17

1.16

10.49







72.11

70.97

Grain Size



Sample Weight

g

NE

NE

456.80

462.80

404.10

473.90

408.50





496.00











445.40

414.10

414.10

434.40







455.00



Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAH
LPAH = low molecular weight PAH
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

FD = field duplicate sample
N - normal sample

PAGE 1 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:



SB-004

SB-004

SB-004

SB-013

SB-013

SB-018

SB-018

SB-021

SB-021

SB-031

SB-031

SB-031

SB-031

SB-032

SB-032

SB-033

SB-033

SB-043

SB-043

SB-043

SB-052

SB-052

Area



Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:



2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-



004-0 5-

004-00-

9004-0 5-

013-0 5-

013-00-

018-0 5-

018-00-

021-0 5-

021-00-

031-0 5-

031-00-

031-01-

9031-00-

032-0 5-

032-00-

033-0 5-

033-00-

043-0 5-

043-00-

043-01-

052-0 5-

052-00-





20130528

20130528

20130528FD

20130528

20130528

20130527

20130527

20130528

20130528

20130528

20130528

20130528

20130528FD

20130527

20130527

20130527

20130527

20130527

20130527

20130527

20130528

20130528

Sample Type:



N

N

FD

N

N

N

N

N

N

N

N

N

FD

N

N

N

N

N

N

N

N

N

Date Sampled:



05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/28/13

05/28/13

Depth (feet):



0.5 -1

o
o

0.5 -1

0.5 -1

o
o

0.5 -1

o
o

0.5 -1

o
o

0.5 -1

o
o

1-2

o
o

0.5 -1

o
o

0.5 -1

o
o

0.5-1

o
o

1-2

0.5-1

o
o

ChemGroup



Analyte

Units

Screening Level



ERLa | ERMb

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics - onolyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 2 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:













SB-052

SB-059

SB-059

SB-059

SB-061

SB-061

SB-062

SB-062

SB-062

SB-078

SB-078

SB-078

SB-079

SB-079

SB-079

SB-082

SB-082

SB-082

SB-089

SB-089

SB-089

SB-Ill

SB-Ill

SB-Ill

Area













Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:













2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-













052-01-

059-0_5-

059-00-

059-01-

061-0_5-

061-00-

062-0_5-

062-00-

062-01-

078-0_5-

078-00-

078-01-

079-0_5-

079-00-

079-01-

082-0_5-

082-00-

082-01-

089-0_5-

089-00-

089-01-

lll-0_5-

111-00-

111-01-















20130528

20130527

20130527

20130527

20130527

20130527

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130523

20130523

20130523

Sample Type:













N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:













05/28/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/23/13

05/23/13

05/23/13

Depth (feet):













1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5-1

0-0.5

1-2

0.5-1

0-0.5

1-2

0.5 -1

0-0.5

1-2











Screening Level

















































ChemGroup





Analyte

Units

ERLa

ERMb

















































Metals, Chrome VI



Chromiur

n VI

mg/Kg

NE

NE





0.031 UJ





0.032 UJ



0.031 UJ











0.033 UJ





















Metals, Hg



Mercury



mg/Kg

0.15

0.71

0.049 J

1.1

0.083 J

0.076 J

0.056 J

0.042 J

0.11 J

0.11 J

0.16

0.06 J

0.04 J

0.052 J

0.074 J

0.45

0.088 J

0.14

0.12 J

0.056 J

0.17

0.27

0.23

0.043 J

0.042 J

0.019 J

TAL Metals



Aluminun

i

mg/Kg

NE

18,000

4,190

4,670

6,330

3,900

10,300

6,540

5,630

5,430

5,250

7,700

7,440

7,410

6,670

8,150

9,620

11,600

8,590

8,810

7,770

12,100

12,500

8,410

9,550

8,460

TAL Metals



Antimony

mg/Kg

NE

9.3

0.35 U

0.34 U

0.36 U

0.35 U

0.36 U

0.35 U

0.34 U

0.34 U

0.31 U

0.36 U

0.35 U

0.36 U

0.38 U

0.36 U

0.36 U

0.39 U

0.49 U

0.41 U

0.38 U

0.42 U

0.36 U

0.036 U

0.036 U

0.034 U

TAL Metals



Arsenic



mg/Kg

8.2

70

0.23 U

0.23 U

0.24 U

0.23 U

0.24 U

0.23 U

0.23 U

0.22 U

0.21 U

0.24 U

0.23 U

0.24 U

0.25 U

0.24 U

0.24 U

0.26 U

0.33 U

0.27 U

0.25 U

0.28 U

0.24 U

3.2 J

2.1 J

1.8 J

TAL Metals



Barium



mg/Kg

NE

48

2.1 U

2.1 U

12.4 J

2.1 U

2.1 U

5.3 J

2.1 U

2 U

1.9 U

2.1 U

2.1 U

2.2 U

9.6 J

2.2 U

2.2 U

13 J

2.9 U

4.4 J

2.3 U

2.5 U

2.1 U

0.22 U

0.22 U

6.8

TAL Metals



Beryllium



mg/Kg

NE

NE

0.27 U

0.26 U

0.28 U

0.27 U

0.27 U

0.27 U

0.26 U

0.26 U

0.24 U

0.27 U

0.27 U

0.28 U

0.29 U

0.28 U

0.28 U

0.3 U

0.37 U

0.31 U

0.29 U

0.32 U

0.27 U

0.028 U

0.028 U

0.026 U

TAL Metals



Cadmium



mg/Kg

1.2

9.6

0.2 U

0.19 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.19 U

0.18 U

0.2 U

0.2 U

0.21 U

0.22 U

0.21 U

0.21 U

0.22 U

0.28 U

0.23 U

0.21 U

0.24 U

0.2 U

0.021 U

0.021 U

0.019 U

TAL Metals



Calcium



mg/Kg

NE

NE

1,730

4,430

3,280

3,840

12,100

3,990 J

6,380

6,020

6,030

7,270

6,450

7,160

3,570 J

4,120

7,560

5,560 J

5,280

3,720 J

5,710

6,400

13,800

3,610 J

5,670 J

3,050 J

TAL Metals



Chromiur

n

mg/Kg

81

370

0.34 U

0.33 U

1.1 J

0.34 U

2 J

1 J

0.33 U

0.32 U

0.3 U

0.35 U

0.34 U

2.3 J

2.1 J

2.1 J

2.5 J

2.7 J

2.8 J

6.7 J

7.7 J

3 J

5.3 J

4.9 J

4.8 J

4.3 J

TAL Metals



Cobalt



mg/Kg

NE

10

10.1 J

12 J

13.3 J

10.7 J

18.6

11.3

12.9 J

11.5 J

10.9 J

15.1

14

13.8

11.3

14.8

16.9

19.8

15.2

9.4

19.9

20.3

25.3

5.3 J

4.6 J

3.2 J

TAL Metals



Copper



mg/Kg

34

270

494 J

1,370 J

748 J

1,450 J

1,690

870

674 J

555 J

616 J

642 J

721 J

635 J

380

576

1,310

876

606

222

805 J

823 J

706 J

105 J

79.8 J

12.5 J

TAL Metals



Iron



mg/Kg

NE

22,000,000

38,500

32,300

43,000

46,900

59,500 J

30,100 J

29,700

27,600

26,000

39,500

39,000

38,300

28,100 J

42,200 J

57,900 J

49,300 J

61,000 J

30,100 J

44,900

57,900

59,900

18,200

26,200

15,600

TAL Metals



Lead



mg/Kg

46.7

218

8.7

0.22 U

1.6 J

0.22 U

0.23 U

0.62 J

0.22 U

0.21 U

0.2 U

0.23 UJ

0.22 UJ

0.23 UJ

1.8 J

0.23 U

0.23 U

2.8 J

0.31 U

2 J

0.24 UJ

0.27 UJ

0.23 UJ

1.5

1.2

1.6

TAL Metals



Magnesium

mg/Kg

NE

NE

5,120

5,820

7,680

4,760

11,700

7,840

6,850

6,800

6,390

9,150

8,520

8,790

8,080

8,990

10,600

13,300

10,200

8,760

9,400

13,800

14,700

7,000

8,280

6,980

TAL Metals



Manganese

mg/Kg

NE

260

163 J

199 J

222 J

172 J

309 J

200

220 J

198 J

187 J

243 J

230 J

225 J

181

232 J

272 J

317

239 J

243

300 J

314 J

421 J

205 J

177 J

195 J

TAL Metals



Nickel



mg/Kg

20.9

51.6

6

5.8

6.2

6.1

10

6.4

6.1

0.24 U

0.22 U

7.4

7.7

6.7

5.9 J

7.4

8.6

9.6

8.2

8

13.6

9.9

14.1

5.1 J

4.8 J

4.4 J

TAL Metals



Potassiur

n

mg/Kg

NE

NE

313 J

500 J

604

330 J

563 J

513 J

523 J

688

496 J

637

567 J

627

798

681

722

991

831

683 J

713

884

1,060

617

636

532 J

TAL Metals



Selenium



mg/Kg

NE

1

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.2 U

1.2 U

1.3 U

1.3 U

1.3 U

1.4 U

1.3 U

1.3 U

1.4 U

1.8 U

1.5 U

1.4 U

1.5 U

1.3 U

0.13 UJ

0.13 UJ

0.12 UJ

TAL Metals



Silver



mg/Kg

1

3.7

0.16 U

0.16 U

0.17 U

0.16 U

0.17 U

0.16 U

0.16 U

0.16 U

0.15 U

0.17 U

0.16 U

0.17 U

0.18 U

0.17 U

0.17 U

0.18 U

0.23 U

0.19 U

0.18 U

0.2 U

0.17 U

0.017 U

0.017 U

0.016 U

TAL Metals



Sodium



mg/Kg

NE

NE

953

1,930

2,220

1,600

1,930

2,300

1,430

2,080

1,560

1,700

1,950

2,120

3,290

3,180

2,040

1,590

5,470

2,710

2,710

1,930

1,950

2,330

2,540

1,720

TAL Metals



Thallium



mg/Kg

NE

NE

0.18 U

0.17 U

0.18 U

0.18 U

0.18 U

0.18 U

0.17 U

0.17 U

0.16 U

0.18 U

0.17 U

0.18 U

0.19 U

0.18 U

0.18 U

0.2 U

0.24 U

0.2 U

0.19 U

0.21 U

0.18 U

0.018 U

0.018 U

0.017 U

TAL Metals



Vanadiurr



mg/Kg

NE

57

55.2 J

63.1 J

64.2 J

85.1 J

89.2

49.3

63.9 J

52.1 J

52.7 J

71.1 J

62.6 J

63.6 J

45.9

61.4

76.4

107

79.7

54.6

123 J

113 J

129 J

28.3 J

26.2 J

23.5 J

TAL Metals



Zinc



mg/Kg

150

410

21

23.5

24.9

18.4

34.9

21.5

23.9

21

20.3

27

25.8

24.4

23.6

31.2

35.6

40.1

31.9

29.5

35.5

40.6

45.2

22.3 J

17.5 J

20.4 J

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

7.2

8.7

7

17





5.7

1.7 U

16

26

27

28

9.1

8.8

24

100

7.7

8

62

10

350







TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

11

11

23

23





13

4.9

19

38

36

37

12

12

31

89

12

10

56

13

240







TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

10

8.6

18

18





11

1.7 U

16

34

38

30

10

8.7

22

83 J

10

6.6

41

9.6

180







TCL PAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

15

16

36

31





44

18

29

40

34

62

15

17

29

79

16

13

41

14

130







TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

5.4

5.2

9.4

9.2





4.3

1.7 U

7.9

15

18

14

6.1

6.5

16

41

6

4.7

26

7.1

120







TCL PAHs

HPAH

Chrysene



ug/Kg

384

2,800

5.3

6.2

6.9

12





5

1.7 U

11

15

17

18

10

7.4

18

69

5.9

5.7

39

9.1

220







TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

6.3

6.5

5.9

1.7 U

1.7 U

5

10

1.7 U

1.7 U

6.3

1.7 U

28







TCL PAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

7.3

6

5.9

12





4.3

1.7 U

14

18

18

19

9.6

11

65

160

9

22

42

12

650







TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

9.3

11

20

21





31

12

23

36

36

35

8.8

9

19

53

9.5

6.4

34

9.5

110







TCL PAHs

HPAH

Pyrene



ug/Kg

665

2,600

9.7

9.8

13

17





5.1

1.7 U

14

21

23

22

41

42

71

170

13

26

82

14

580







TCL PAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

80.2

82.5

139.2

160.2





123.4

34.9

149.9

249.3

253.5

270.9

121.6

122.4

300

854

89.1

102.4

429.3

98.3

2,608







TCL PAHs

LPAH

Acenaphthene

ug/Kg

16

500

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U







TCL PAHs

LPAH

Acenaphthylene

ug/Kg

44

640

1.7 U

5.9

8.3

15





6

4.3

5.6

19

12

22

7.4

5.7

17

27

1.7 U

1.7 U

21

9.1

52







TCL PAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

3.9 J

1.7 U

1.7 U

4.9

13

1.7 U

1.7 U

4.2 J

1.7 U

26







TCL PAHs

LPAH

Fluorene



ug/Kg

19

540

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

5.1







TCL PAHs

LPAH

Naphthalene

ug/Kg

160

2,100

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

4.3







TCL PAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

1.7 U

1.7 U

6.7

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

8.1

4.5

20

1.7 U

5

1.7 U

1.7 U

11







TCL PAHs

LPAH

Total LPAH

ug/kg

552

3,160

1.7 U

5.9

15

15





6

4.3

5.6

19

12

25.9

7.4

13.8

26.4

60

1.7 U

5

25.2

9.1

98.4







TCL PAHs

TPAH

Total PAH

ug/kg

4,022

44,792

80.2

88.4

154.2

175.2





129.4

39.2

155.5

268.3

265.5

296.8

129

136.2

326.4

914

89.1

107.4

454.5

107.4

2,706







TCL PAHs



2-Methylnaphthalene

ug/Kg

70

670

1.7 U

1.7 U

1.7 U

1.7 U





1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U







Genchem, TOC



Organic carbon

mg/Kg

NE

NE



200 J

490 J

190 J



560 J

200 J

240 J

150 J

170 J

240 J

240 J

4,400 J

3,700 J

2,600 J

7,200 J

15,000 J

15,000 J

4,000 J

6,900 J

670 J







Genchem



Total solids

%

NE

NE



84.8

83.9

84.9



81.9

85.1

84.1

83.2

84.3

83

83.7

76.6

79.6

78.5

73.4

63.4

75.9

77.8

77

82.7







BulkDensity



Bulk Density

g/cm3

NE

NE





2.28





2.20

2.33

2.22

2.27

2.24

2.28

2.24

2.11

2.19

2.22

1.93

1.59

1.92

2.08

2.08

2.31







Grain Size



Particle s

ze, 1 inch (25.40mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00







Grain Size



Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00







Grain Size



Particle s

ze, 2 inch, (50.80mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00







Grain Size



Particle s

ze, 3 inch, (76.20mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00







Grain Size



Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

8.30

0.00

0.00

0.00







Grain Size



Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE



0.00

0.00

0.00



0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

3.30

0.00

72.30

0.00

0.00

0.00







Grain Size



Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE



1.00

1.00

1.00



1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.01

1.00

1.01

1.00

1.00

1.01







Grain Size



Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE



1.00

1.00

1.00



1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.01

1.01

1.01

1.01

1.01

1.00

1.01







Grain Size



Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE



1.00

1.00

1.01



1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.01

1.01

1.01

1.01

1.01

1.00

1.01







Grain Size



Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE



1.00

1.01

1.01



1.00

1.01

1.01

1.00

1.01

1.00

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.02







Grain Size



Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE



1.01

1.01

1.01



1.00

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.01

1.02

1.01

1.01

1.02

1.01

1.02







Grain Size



Particle s

ze, Hydrometer (.041 mm)

mg/L

NE

NE

















































Grain Size



Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE



1.00

1.00

1.00



1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.00

1.01







Grain Size



Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE



0.00

0.10

0.00



0.80

0.00

0.00

0.00

0.90

0.00

0.00

0.00

0.00

0.00

3.70

0.00

45.60

0.00

0.00

0.00







Grain Size



Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE



0.00

0.20

0.00



0.60

0.00

0.00

0.00

0.00

0.00

0.30

0.60

0.50

1.50

1.90

0.00

53.30

0.00

0.00

0.00







Grain Size



Particle s

ze, Sieve No. 140,150 mesh, (0.106mm)

g

NE

NE



261.85

192.71

198.50



242.75

146.08

182.27

181.30

139.42

213.19

152.14

160.66

174.44

170.39

84.15

125.18

49.77

122.29

247.46

19.45







Grain Size



Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE



0.00

0.00

0.00



0.40

0.61

0.38

0.00

0.00

0.00

0.00

0.74

0.37

1.56

1.98

0.28

29.22

0.68

0.67

0.00







Grain Size



Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE



75.88

86.70

92.28



129.01

56.98

81.76

72.40

93.62

101.07

88.25

74.26

66.84

59.91

27.23

43.69

15.05

56.70

61.03

37.28







Grain Size



Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE



1.97

1.18

2.05



0.80

2.42

3.00

3.59

0.34

1.58

1.06

5.51

5.51

9.34

2.97

2.52

21.43

2.05

6.04

0.54







Grain Size



Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE



35.39

16.95

20.10



8.84

21.82

25.50

29.32

5.39

16.19

11.65

32.72

38.93

41.24

15.84

20.72

20.72

21.18

52.98

2.16







Grain Size



Sample Weight

g

NE

NE



454.90

454.30

473.70



466.00

435.20

432.80

434.40

389.20

455.60

406.60

426.70

424.30

451.20

356.40

322.90

383.00

527.40

525.10

416.00







Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAH
LPAH = low molecular weight PAH
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

FD = field duplicate sample
N - normal sample

PAGE 3 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:



SB-052

SB-059

SB-059

SB-059

SB-061

SB-061

SB-062

SB-062

SB-062

SB-078

SB-078

SB-078

SB-079

SB-079

SB-079

SB-082

SB-082

SB-082

SB-089

SB-089

SB-089

SB-Ill

SB-Ill

SB-Ill

Area



Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:



2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-



052-01-

059-0 5-

059-00-

059-01-

061-0 5-

061-00-

062-0 5-

062-00-

062-01-

078-0 5-

078-00-

078-01-

079-0 5-

079-00-

079-01-

082-0 5-

082-00-

082-01-

089-0 5-

089-00-

089-01-

111-0 5-

111-00-

111-01-





20130528

20130527

20130527

20130527

20130527

20130527

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130528

20130523

20130523

20130523

Sample Type:



N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:



05/28/13

05/27/13

05/27/13

05/27/13

05/27/13

05/27/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/23/13

05/23/13

05/23/13

Depth (feet):



1-2

0.5 -1

o
o

1-2

0.5 -1

o
o

0.5 -1

o
o

1-2

0.5 -1

o
o

1-2

0.5 -1

o
o

1-2

0.5-1

o
o

1-2

0.5 -1

o
o

1-2

0.5 -1

o
o

1-2

ChemGroup



Analyte

Units

Screening Level



ERLa | ERMb

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics - onolyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 4 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:













SB-115

SB-115

SB-115

SB-115

SB-115

SB-117

SB-117

SB-117

SB-121

SB-121

SB-121

SB-123

SB-123

SB-123

SB-123

SB-123

SB-127

SB-127

SB-127

SB-129

SB-129

SB-129

SB-129

SB-133

Area













Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:













2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-













115-0_5-

115-00-

115-01-

115-02-

9115-00-

117-0_5-

117-00-

117-01-

121-0_5-

121-00-

121-01-

123-0_5-

123-00-

123-01-

123-02-

9123-00-

127-0_5-

127-00-

127-01-

129-0_5-

129-00-

129-01-

9129-00-

133-0_5-















20130522

20130522

20130522

20130522

20130522FD

20130524

20130524

20130524

20130523

20130523

20130523

20130523

20130523

20130523

20130523

20130523FD

20130522

20130522

20130522

20130523

20130523

20130523

20130523FD

20130522

Sample Type:













N

N

N

N

FD

N

N

N

N

N

N

N

N

N

N

FD

N

N

N

N

N

N

FD

N

Date Sampled:













05/22/13

05/22/13

05/22/13

05/22/13

05/22/13

05/24/13

05/24/13

05/24/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/22/13

05/22/13

05/22/13

05/23/13

05/23/13

05/23/13

05/23/13

05/22/13

Depth (feet):













0.5 -1

0-0.5

1-2

2-3

0-0.5

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

2-3

0-0.5

0.5-1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0-0.5

0.5 -1











Screening Level

















































ChemGroup





Analyte

Units

ERLa

ERMb

















































Metals, Chrome VI



Chromiur

n VI

mg/Kg

NE

NE



0.14 U





0.14 U































0.16 U







Metals, Hg



Mercury



mg/Kg

0.15

0.71

0.02 J

0.035 J

0.021 J

0.018 J

0.046 J

0.015 J

0.032 J

0.012 J

0.019 J

0.03 J

0.024 J

0.25

0.23

0.14

0.037 J

0.15

0.09 J

0.074 J

0.061 J

0.2

0.082 J

0.054 J

0.096 J

0.077 J

TAL Metals



Aluminun

i

mg/Kg

NE

18,000

8,810

9,920

10,500

7,030

10,000

10,100

11,100

12,300

9,450

8,860

7,570

11,300

13,500

17,400

9,230

14,300

7,840

8,930

7,730

16,700

11,200

11,800

10,700

12,700

TAL Metals



Antimony

mg/Kg

NE

9.3

0.034 U

0.035 U

0.035 U

0.065 U

0.035 U

0.37 U

0.36 U

0.35 U

0.35 U

0.035 U

0.039 U

0.038 U

0.042 U

0.39 U

0.041 U

0.035 U

0.37 U

0.038 U

0.035 U

0.39 U

0.2 U

0.43 U

0.4 U

0.37 U

TAL Metals



Arsenic



mg/Kg

8.2

70

2.8 J

2.1 J

8.8 J

3.2 J

2.2 J

9

0.24 U

0.23 U

0.23 U

2.4 J

1 J

1.5 J

1.6 J

0.26 U

2.4 J

1.6 J

0.25 U

1.7 J

0.69 J

0.26 U

0.27 U

0.29 U

0.27 U

0.25 U

TAL Metals



Barium



mg/Kg

NE

48

0.2 U

7.7

0.21 U

0.39 U

9.2

2.2 U

2.2 U

2.1 U

2.1 U

0.21 U

36.1

16.6

18.4

2.3 U

10.7

14.9

2.2 U

9.6

8.2

2.3 U

1.2 U

2.6 U

2.4 U

2.2 U

TAL Metals



Beryllium



mg/Kg

NE

NE

0.026 U

0.027 U

0.027 U

0.049 U

0.027 U

0.29 U

0.28 U

0.27 U

0.27 U

0.027 U

0.03 U

0.029 U

0.032 U

0.3 U

0.031 U

0.027 U

0.29 U

0.029 U

0.027 U

0.3 U

0.31 U

0.33 U

0.31 U

0.28 U

TAL Metals



Cadmium



mg/Kg

1.2

9.6

0.019 U

0.02 U

1.2

0.037 U

0.02 U

0.21 U

0.2 U

0.2 U

0.2 U

0.02 U

0.022 U

0.022 U

0.024 U

0.22 U

0.79

0.02 U

0.21 U

0.022 U

0.02 U

0.22 U

0.11 U

0.24 U

0.23 U

0.21 U

TAL Metals



Calcium



mg/Kg

NE

NE

14,700 J

5,090 J

23,500 J

153,000 J

5,060 J

3,910 J

4,280 J

4,160 J

18,600 J

4,190 J

164,000 J

10,600 J

17,700 J

14,600 J

5,140 J

12,200 J

8,580 J

4,970 J

6,490 J

15,900 J

8,990 J

9,170 J

6,950 J

12,100 J

TAL Metals



Chromiur

n

mg/Kg

81

370

4.1 J

4.7 J

5.9 J

7.7 J

3.6 J

0.36 U

12.5

11.8

0.34 U

4.6 J

5.5 J

1.6 J

1.7 J

0.37 U

5.5 J

1.5 J

0.36 U

1.6 J

1.3 J

40.5

0.39 U

0.42 U

43.5

0.36 U

TAL Metals



Cobalt



mg/Kg

NE

10

3.7 J

5.5 J

4.6 J

3.6 J

6.1 J

0.24 UJ

8.3 J

6.5 J

10.2 J

7.6 J

3 J

12.7 J

13.1 J

28.6 J

4.9 J

11.2 J

23.1 J

9.1 J

8.2 J

25.9 J

19.9 J

21.8 J

20.4 J

21.5 J

TAL Metals



Copper



mg/Kg

34

270

15.7 J

524 J

15.3 J

10.4 J

232 J

40.3 J

125 J

20 J

101 J

61.9 J

7.6 J

901 J

1,190 J

1,570 J

530 J

699 J

1,970 J

918 J

2,050 J

1,190 J

1,030 J

1,400 J

828 J

1,040 J

TAL Metals



Iron



mg/Kg

NE

22,000,000

16,700

20,900

21,200

13,000

21,100

18,900

22,800

20,700

22,400

18,500

13,900

59,900

65,200

60,000

20,100

68,700

46,100

31,400

24,800

69,800

54,400

29,500

51,900

53,000

TAL Metals



Lead



mg/Kg

46.7

218

1.2

1.4

1.2

1.2

1.4

0.24 U

0.23 U

0.22 U

0.22 U

1.5

0.81

1.9

1.9

0.25 U

1.8

1.6

0.24 U

1.3

0.86

0.24 U

0.13 U

0.27 U

0.25 U

0.23 U

TAL Metals



Magnesium

mg/Kg

NE

NE

7,640

8,840

9,010

6,520

8,870

8,060

9,160

9,850

8,570

7,410

6,440

12,700

14,900

18,600

7,360

15,700

8,620

9,440

8,280

18,600

11,600

10,300

11,400

13,000

TAL Metals



Manganese

mg/Kg

NE

260

196 J

223 J

230 J

164 J

125 J

344 J

381 J

281 J

268 J

224 J

178 J

280 J

270 J

445 J

198 J

244 J

361 J

185 J

189 J

415 J

305 J

407 J

310 J

331 J

TAL Metals



Nickel



mg/Kg

20.9

51.6

4.9 J

5.6 J

7.7 J

6.8 J

5.3 J

0.26 U

10.1

8.1

10.2

7.7 J

4.6 J

6.8 J

7 J

13.7

6.5 J

6 J

12.1

5.3 J

4.7 J

27.4

10.4

14.7

25.7

11.2

TAL Metals



Potassiur

n

mg/Kg

NE

NE

604

661

559 J

418 J

581 J

688

762

728

595

531 J

467 J

1,040

1,300

1,640

735

1,210

529 J

782

540 J

1,490

984

1,080

961

1,130

TAL Metals



Selenium



mg/Kg

NE

1

0.12 UJ

0.38 J

0.3 J

0.24 UJ

0.26 J

1.4 U

1.3 U

1.3 U

1.3 U

0.13 UJ

0.14 UJ

0.58 J

0.48 J

1.4 U

0.68 J

0.44 J

1.8 J

0.35 J

1.1 J

1.4 U

1.5 U

1.6 U

1.5 U

1.4 U

TAL Metals



Silver



mg/Kg

1

3.7

0.016 U

0.016 U

0.017 U

0.03 U

0.016 U

0.17 U

0.17 U

0.16 U

0.16 U

0.017 U

0.018 U

0.83

0.75

0.18 U

0.019 U

0.64

0.17 U

0.018 U

0.94

0.18 U

0.094 U

0.2 U

0.19 U

0.17 U

TAL Metals



Sodium



mg/Kg

NE

NE

1,950

2,500

2,540

3,190

2,010

3,850

4,650

2,930

1,090

706

2,190

2,310

3,670

2,690

1,270

3,720

2,420

3,370

1,950

3,040

3,710

2,630

4,070

3,050

TAL Metals



Thallium



mg/Kg

NE

NE

0.017 U

0.017 U

0.018 U

0.032 U

0.017 U

0.19 U

0.18 U

0.17 U

0.18 U

0.018 U

0.019 U

0.019 U

0.021 U

0.19 U

0.02 U

0.017 U

0.19 U

0.019 U

0.018 U

0.19 U

0.1 U

0.21 U

0.2 U

0.18 U

TAL Metals



Vanadiurr



mg/Kg

NE

57

27.5 J

30 J

29.7 J

22.9 J

33.9 J

42.3 J

56.1 J

43.4 J

47.7 J

31.3 J

17.8 J

64.2 J

62.9 J

135 J

30.2 J

52.8 J

111 J

41.6 J

35.1 J

130 J

95.4 J

116 J

93.8 J

96.8 J

TAL Metals



Zinc



mg/Kg

150

410

21.7 J

24.2 J

26.5 J

23.6 J

25.8 J

38.5 J

35.4 J

35.1 J

39.2 J

25.4 J

18.1 J

27.9 J

29.1 J

52.8 J

24.6 J

24.3 J

42.9 J

22.5 J

18.8 J

113 J

40.5 J

52 J

105 J

41.9 J

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

















































TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

















































TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Chrysene



ug/Kg

384

2,800

















































TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

















































TCL PAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

















































TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Pyrene



ug/Kg

665

2,600

















































TCL PAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

















































TCL PAHs

LPAH

Acenaphthene

ug/Kg

16

500

















































TCL PAHs

LPAH

Acenaphthylene

ug/Kg

44

640

















































TCL PAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

















































TCL PAHs

LPAH

Fluorene



ug/Kg

19

540

















































TCL PAHs

LPAH

Naphthalene

ug/Kg

160

2,100

















































TCL PAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

















































TCL PAHs

LPAH

Total LPAH

ug/kg

552

3,160

















































TCL PAHs

TPAH

Total PAH

ug/kg

4,022

44,792

















































TCL PAHs



2-Methylnaphthalene

ug/Kg

70

670

















































Genchem, TOC



Organic carbon

mg/Kg

NE

NE



3,300





































6,300



7,160



Genchem



Total solids

%

NE

NE



79.8





































72.3



72.1



BulkDensity



Bulk Density

g/cm3

NE

NE



2.15





































1.87



1.97



Grain Size



Particle s

ze, 1 inch (25.40mm)

g

NE

NE



0.00





































0.00



0.00



Grain Size



Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE



0.00





































0.00



0.00



Grain Size



Particle s

ze, 2 inch, (50.80mm)

g

NE

NE



0.00





































0.00



0.00



Grain Size



Particle s

ze, 3 inch, (76.20mm)

g

NE

NE



0.00





































0.00



0.00



Grain Size



Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE



0.00





































0.00



0.00



Grain Size



Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE



0.00





































0.00



1.50



Grain Size



Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE



1.00





































1.00



1.00



Grain Size



Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE



1.00





































1.00



1.00



Grain Size



Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE



1.00





































1.01



1.01



Grain Size



Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE



1.01





































1.01



1.01



Grain Size



Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE



1.01





































1.01



1.01



Grain Size



Particle s

ze, Hydrometer (.041 mm)

mg/L

NE

NE

















































Grain Size



Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE



1.00





































1.00



1.00



Grain Size



Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE



20.50





































0.00



0.90



Grain Size



Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE



35.40





































1.20



1.30



Grain Size



Particle s

ze, Sieve No. 140,150 mesh, (0.106mm)

g

NE

NE



105.51





































44.85



46.22



Grain Size



Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE



43.64





































0.64



1.14



Grain Size



Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE



71.64





































80.09



71.33



Grain Size



Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE



24.10





































1.92



1.71



Grain Size



Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE



26.70





































3.20



3.99



Grain Size



Sample Weight

g

NE

NE



490.30





































432.40



404.30



Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAH
LPAH = low molecular weight PAH
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

FD = field duplicate sample
N - normal sample

PAGE 5 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:



SB-115

SB-115

SB-115

SB-115

SB-115

SB-117

SB-117

SB-117

SB-121

SB-121

SB-121

SB-123

SB-123

SB-123

SB-123

SB-123

SB-127

SB-127

SB-127

SB-129

SB-129

SB-129

SB-129

SB-133

Area



Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:



2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-



115-0 5-

115-00-

115-01-

115-02-

9115-00-

117-0 5-

117-00-

117-01-

121-0 5-

121-00-

121-01-

123-0 5-

123-00-

123-01-

123-02-

9123-00-

127-0 5-

127-00-

127-01-

129-0 5-

129-00-

129-01-

9129-00-

133-0 5-





20130522

20130522

20130522

20130522

20130522FD

20130524

20130524

20130524

20130523

20130523

20130523

20130523

20130523

20130523

20130523

20130523FD

20130522

20130522

20130522

20130523

20130523

20130523

20130523FD

20130522

Sample Type:



N

N

N

N

FD

N

N

N

N

N

N

N

N

N

N

FD

N

N

N

N

N

N

FD

N

Date Sampled:



05/22/13

05/22/13

05/22/13

05/22/13

05/22/13

05/24/13

05/24/13

05/24/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/22/13

05/22/13

05/22/13

05/23/13

05/23/13

05/23/13

05/23/13

05/22/13

Depth (feet):



0.5 -1

o
o

1-2

2-3

o
o

0.5 -1

o
o

1-2

0.5 -1

o
o

1-2

0.5 -1

o
o

1-2

2-3

o
o

0.5-1

o
o

1-2

0.5 -1

o
o

1-2

o
o

0.5 -1

ChemGroup



Analyte

Units

Screening Level



ERLa | ERMb

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics - onolyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 6 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:













SB-133

SB-133

SB-133

SB-133

SB-157

SB-157

SB-157

SB-157

SB-176

SB-177

SB-191

SB-191

SB-191

SB-192

SB-192

SB-192

SB-192

SB-196

SB-196

SB-197

SB-197

SB-197

SB-199

SB-199

Area













Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:













2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-













133-00-

133-01-

133-02-

9133-01-

157-0_5-

157-00-

157-01-

157-02-

176-00-

177-0_5-

191-0_5-

191-00-

191-01-

192-0_5-

192-00-

192-01-

192-02-

196-0_5-

196-00-

197-0_5-

197-00-

197-01-

199-0_5-

199-00-















20130522

20130522

20130522

20130522FD

20130525

20130525

20130525

20130525

20130530

20130530

20130523

20130523

20130523

20130523

20130523

20130523

20130523

20130524

20130524

20130524

20130524

20130524

20130524

20130524

Sample Type:













N

N

N

FD

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:













05/22/13

05/22/13

05/22/13

05/22/13

05/25/13

05/25/13

05/25/13

05/25/13

05/30/13

05/30/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

Depth (feet):













0-0.5

1-2

2-3

1-2

0.5 -1

0-0.5

1-2

2-3

0-0.5

0.5 -1

0.5 -1

0-0.5

1-2

0.5-1

0-0.5

1-2

2-2.4

0.5-1

0-0.5

0.5-1

0-0.5

1-2

0.5 -1

0-0.5











Screening Level

















































ChemGroup





Analyte

Units

ERLa

ERMb

















































Metals, Chrome VI



Chromiur

n VI

mg/Kg

NE

NE

















































Metals, Hg



Mercury



mg/Kg

0.15

0.71

0.098 J

0.1 J

0.099 J

0.25

0.073 J

0.088 J

0.14

0.0067 U

0.059 J

0.096 J

0.11 J

0.073 J

2.2

0.034 J

0.18

0.028 J

0.028 J

0.026 J

0.083 J

0.0075 U

0.035 J

0.0075 U

0.02 J

0.024 J

TAL Metals



Aluminun

i

mg/Kg

NE

18,000

9,120

9,230

12,400

10,200

8,970

11,000

13,800

10,400

7,130

5,680

7,150

7,320

8,040

11,400

6,920

10,400

10,800

9,960

10,000

11,400

11,400

10,300

11,800

11,500

TAL Metals



Antimony

mg/Kg

NE

9.3

0.039 U

0.36 U

0.36 U

0.37 U

0.36 U

0.37 U

0.38 U

0.34 U

0.35 U

0.33 U

0.036 U

0.037 U

0.037 U

0.18 U

0.18 U

0.17 U

0.18 U

0.33 U

0.36 U

0.39 U

0.37 U

0.38 U

0.38 U

0.35 U

TAL Metals



Arsenic



mg/Kg

8.2

70

1.6 J

0.24 U

0.24 U

0.25 U

0.24 U

0.24 U

0.25 U

0.23 U

0.23 U

0.22 U

1.4 J

1.9 J

2.2 J

0.12 U

0.25 U

0.22 U

0.24 U

0.22 U

0.24 U

0.26 U

0.25 U

0.26 U

0.25 U

0.23 U

TAL Metals



Barium



mg/Kg

NE

48

13.3

2.1 U

2.2 U

2.2 U

2.1 U

2.2 U

2.3 U

2 U

2.1 U

2 U

12.9

9

7.4

1.1 U

1.1 U

1 U

1.1 U

2 U

2.2 U

2.3 U

2.2 U

3.8 J

6.4 J

5.2 J

TAL Metals



Beryllium



mg/Kg

NE

NE

0.03 U

0.27 U

0.28 U

0.28 U

0.27 U

0.28 U

0.29 U

0.26 U

0.27 U

0.25 U

0.028 U

0.028 U

0.028 U

0.14 U

0.28 U

0.26 U

0.28 U

0.25 U

0.28 U

0.3 U

0.28 U

0.29 U

0.29 U

0.27 U

TAL Metals



Cadmium



mg/Kg

1.2

9.6

0.022 U

0.2 U

0.2 U

0.21 U

0.2 U

0.21 U

0.21 U

0.19 U

0.2 U

0.18 U

0.021 U

0.021 U

0.021 U

0.1 U

0.1 U

0.095 U

0.1 U

0.19 U

0.2 U

0.22 U

0.21 U

0.22 U

0.22 U

0.2 U

TAL Metals



Calcium



mg/Kg

NE

NE

6,300 J

10,500 J

11,500 J

11,100 J

8,760

5,500

19,700

12,600

3,080

2,240

5,760 J

3,730 J

6,030 J

6,640 J

4,880 J

3,210 J

24,700 J

11,300 J

24,400 J

4,250 J

4,740 J

4,130 J

34,100 J

4,020 J

TAL Metals



Chromiur

n

mg/Kg

81

370

1.6 J

0.35 U

0.35 U

0.36 U

1.5 J

2.1 J

2 J

9.5 J

0.34 U

0.31 U

0.035 U

1.3 J

1.7 J

0.17 U

0.36 U

0.32 U

0.35 U

0.32 U

0.35 U

10.9 J

7.9 J

8.6 J

7.8 J

7.7 J

TAL Metals



Cobalt



mg/Kg

NE

10

9.7 J

21.5 J

24.9 J

20.5 J

18.1

13.7

17.5

6.4

13.8 J

13.5 J

10.2 J

9.1 J

7.5 J

4 J

7.5 J

0.21 UJ

0.23 UJ

9.2 J

13.2 J

0.25 U

7.5

4.8 J

7.9

9.4

TAL Metals



Copper



mg/Kg

34

270

454 J

993 J

777 J

1,130 J

1,750

797

874

82.2

2,170 J

651 J

1,290 J

692 J

739 J

82.2 J

447 J

0.59 UJ

12.6 J

831 J

383 J

28.3

174

0.68 U

255

199

TAL Metals



Iron



mg/Kg

NE

22,000,000

34,900

53,000

49,600

45,300

53,700 J

55,400 J

49,800 J

21,100 J

34,400

35,700

21,600

27,700

22,300

22,500

27,300

18,300

19,300

30,800

25,800

18,900 J

24,600 J

19,300 J

22,600 J

26,900 J

TAL Metals



Lead



mg/Kg

46.7

218

1.3

0.23 U

0.23 U

0.23 U

0.23 U

0.23 U

0.24 U

0.21 U

0.22 U

0.21 U

1.2

1.3

1

0.11 U

0.12 U

0.11 U

0.11 U

0.21 U

0.23 U

0.25 U

0.23 U

0.91 J

1.5 J

1.7 J

TAL Metals



Magnesium

mg/Kg

NE

NE

10,200

10,200

14,200

11,500

10,300

11,700

15,800

8,900

8,290

7,040

8,210

7,850

8,890

8,960

7,810

9,150

9,180

9,860

9,970

10,100

10,700

9,340

10,500

11,400

TAL Metals



Manganese

mg/Kg

NE

260

198 J

342 J

406 J

332 J

289 J

215 J

308 J

268 J

226 J

216 J

208 J

186 J

299 J

132 J

117 J

152 J

160 J

218 J

277 J

259

248

211

240

319

TAL Metals



Nickel



mg/Kg

20.9

51.6

5.5 J

10.1

11.6

9.6

8.8

7.1

8.5

8.1

7.2

6.1

5.4 J

4.9 J

5 J

6.9

0.26 U

0.23 U

8.3

6.6

10.3

9.1

7.9

9.1

9.4

8.5

TAL Metals



Potassiur

n

mg/Kg

NE

NE

942

806

1,390

950

863

905

1,240

613

518 J

546

810

900

837

878

618

665

643

526 J

755

770

776

677

742

618

TAL Metals



Selenium



mg/Kg

NE

1

0.26 J

1.3 U

1.3 U

1.3 U

1.5 J

1.3 U

1.4 U

1.2 U

1.3 U

1.2 U

0.83 J

0.4 J

0.39 J

0.65 U

1.4 U

1.2 U

1.3 U

1.2 U

1.3 U

1.4 U

1.4 U

1.4 U

1.4 U

1.3 U

TAL Metals



Silver



mg/Kg

1

3.7

0.018 U

0.17 U

0.17 U

0.17 U

0.17 U

0.17 U

0.18 U

0.16 U

0.16 U

0.15 U

0.97

0.017 U

0.017 U

0.083 U

0.086 U

0.078 U

0.084 U

0.15 U

0.17 U

0.18 U

0.17 U

0.18 U

0.18 U

0.16 U

TAL Metals



Sodium



mg/Kg

NE

NE

4,800

2,560

2,700

2,750

2,120

2,070

2,440

1,510

2,040

1,090

2,530

4,020

2,130

2,810

2,190

1,760

1,670

1,420

2,260

3,280

3,170

3,040

3,160

2,110

TAL Metals



Thallium



mg/Kg

NE

NE

0.02 U

0.18 U

0.18 U

0.18 U

0.18 U

0.18 U

0.19 U

0.17 U

0.17 U

0.16 U

0.018 U

0.019 U

0.018 U

0.089 U

0.092 U

0.084 U

0.09 U

0.17 U

0.18 U

0.19 U

0.18 U

0.59 J

0.19 U

0.18 U

TAL Metals



Vanadiurr



mg/Kg

NE

57

41.3 J

100 J

121 J

90.1 J

77.4

60.6

80.2

42.7

57.4 J

62.8 J

42.5 J

40.5 J

37.6 J

20.1 J

33.1 J

0.85 UJ

0.91 UJ

47.4 J

51.3 J

45.9

47

34.3

47.4

48.5

TAL Metals



Zinc



mg/Kg

150

410

23.4 J

39.5 J

48.4 J

37.8 J

36.7

27.8

34.5

33.8

26.8

25

24.5 J

23.3 J

21 J

18.8 J

15.6 J

17.5 J

19.4 J

28 J

36.7 J

31.6

41.4

30

32

32.5

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

















































TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

















































TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Chrysene



ug/Kg

384

2,800

















































TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

















































TCL PAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

















































TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

















































TCL PAHs

HPAH

Pyrene



ug/Kg

665

2,600

















































TCL PAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

















































TCL PAHs

LPAH

Acenaphthene

ug/Kg

16

500

















































TCL PAHs

LPAH

Acenaphthylene

ug/Kg

44

640

















































TCL PAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

















































TCL PAHs

LPAH

Fluorene



ug/Kg

19

540

















































TCL PAHs

LPAH

Naphthalene

ug/Kg

160

2,100

















































TCL PAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

















































TCL PAHs

LPAH

Total LPAH

ug/kg

552

3,160

















































TCL PAHs

TPAH

Total PAH

ug/kg

4,022

44,792

















































TCL PAHs



2-Methylnaphthalene

ug/Kg

70

670

















































Genchem, TOC



Organic carbon

mg/Kg

NE

NE





























2,750



















Genchem



Total solids

%

NE

NE





























79



















BulkDensity



Bulk Density

g/cm3

NE

NE





























1.94



















Grain Size



Particle s

ze, 1 inch (25.40mm)

g

NE

NE





























0.00



















Grain Size



Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE





























0.00



















Grain Size



Particle s

ze, 2 inch, (50.80mm)

g

NE

NE





























0.00



















Grain Size



Particle s

ze, 3 inch, (76.20mm)

g

NE

NE





























0.00



















Grain Size



Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE





























0.00



















Grain Size



Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE





























2.40



















Grain Size



Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Hydrometer (.041 mm)

mg/L

NE

NE

















































Grain Size



Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE





























1.00



















Grain Size



Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE





























1.30



















Grain Size



Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE





























1.80



















Grain Size



Particle s

ze, Sieve No. 140,150 mesh, (0.106mm)

g

NE

NE





























358.27



















Grain Size



Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE





























1.42



















Grain Size



Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE





























95.00



















Grain Size



Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE





























5.20



















Grain Size



Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE





























30.72



















Grain Size



Sample Weight

g

NE

NE





























558.50



















Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAH
LPAH = low molecular weight PAH
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

FD = field duplicate sample
N - normal sample

PAGE 7 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:



SB-133

SB-133

SB-133

SB-133

SB-157

SB-157

SB-157

SB-157

SB-176

SB-177

SB-191

SB-191

SB-191

SB-192

SB-192

SB-192

SB-192

SB-196

SB-196

SB-197

SB-197

SB-197

SB-199

SB-199

Area



Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:



2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-



133-00-

133-01-

133-02-

9133-01-

157-0 5-

157-00-

157-01-

157-02-

176-00-

177-0 5-

191-0 5-

191-00-

191-01-

192-0 5-

192-00-

192-01-

192-02-

196-0 5-

196-00-

197-0 5-

197-00-

197-01-

199-0 5-

199-00-





20130522

20130522

20130522

20130522FD

20130525

20130525

20130525

20130525

20130530

20130530

20130523

20130523

20130523

20130523

20130523

20130523

20130523

20130524

20130524

20130524

20130524

20130524

20130524

20130524

Sample Type:



N

N

N

FD

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:



05/22/13

05/22/13

05/22/13

05/22/13

05/25/13

05/25/13

05/25/13

05/25/13

05/30/13

05/30/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/23/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

05/24/13

Depth (feet):



o
o

1-2

2-3

1-2

0.5 -1

o
o

1-2

2-3

o
o

0.5 -1

0.5 -1

o
o

1-2

0.5-1

o
o

1-2

2-2.4

0.5-1

o
o

0.5-1

o
o

1-2

0.5 -1

o
o

ChemGroup



Analyte

Units

Screening Level



ERLa | ERMb

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics - onolyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 8 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:













SB-199

SB-202

SB-202

SB-202

SB-209

SB-209

SB-209

SB-222

SB-223

Area













Site

Site

Site

Site

Site

Site

Site

Site

Site















2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

Activity ID:













199-01-

202-00-

9202-00-

202-0_5-

209-00-

209-01-

209-02-

222-00-

223-0_5-















20130524

20130524

20130524FD

20130524

20130527

20130527

20130527

20130530

20130530

Sample Type:













N

N

FD

N

N

N

N

N

N

Date Sampled:













05/24/13

05/24/13

05/24/13

05/24/13

05/27/13

05/27/13

05/27/13

05/30/13

05/30/13

Depth (feet):













1-2

0-0.5

0-0.5

0.5 -1

0-0.5

1 -1.5

2-2.5

0-0.5

0.5 -1











Screening Level



















ChemGroup





Analyte

Units

ERLa

ERMb



















Metals, Chrome VI



Chromiur

n VI

mg/Kg

NE

NE



















Metals, Hg



Mercury



mg/Kg

0.15

0.71

0.007 U

0.0067 U

0.0068 U

0.0065 U

0.097 J

0.081 J

0.26

0.095 J

0.08 J

TAL Metals



Aluminun

i

mg/Kg

NE

18,000

9,290

10,800

12,200

10,400

7,850

5,570

13,800

6,980

10,500

TAL Metals



Antimony

mg/Kg

NE

9.3

0.35 U

0.34 U

0.33 U

0.34 U

0.39 U

0.35 U

0.36 U

0.36 U

0.41 U

TAL Metals



Arsenic



mg/Kg

8.2

70

0.23 U

0.23 U

0.22 U

0.23 U

0.26 U

0.23 U

0.24 U

0.24 U

0.27 U

TAL Metals



Barium



mg/Kg

NE

48

8.8 J

4.4 J

3.8 J

2.8 J

2.3 U

2.1 U

2.1 U

2.2 U

2.5 U

TAL Metals



Beryllium



mg/Kg

NE

NE

0.26 U

0.26 U

0.25 U

0.26 U

0.3 U

0.27 U

0.27 U

0.28 U

0.31 U

TAL Metals



Cadmium



mg/Kg

1.2

9.6

0.2 U

0.19 U

0.19 U

0.19 U

0.22 U

0.2 U

0.2 U

0.21 U

0.23 U

TAL Metals



Calcium



mg/Kg

NE

NE

43,100 J

3,850 J

3,600 J

3,250 J

3,770

5,610

15,800

3,160

9,800

TAL Metals



Chromiur

n

mg/Kg

81

370

9 J

8.1 J

8.3 J

7.3 J

0.38 U

0.34 U

0.34 U

0.35 U

0.4 U

TAL Metals



Cobalt



mg/Kg

NE

10

6.8

5.4 J

5.6

5.9

14.1 J

12.6 J

26.1 J

14.1 J

12.4 J

TAL Metals



Copper



mg/Kg

34

270

43.8

28

37.9

15.8

942 J

1,410 J

687 J

719 J

909 J

TAL Metals



Iron



mg/Kg

NE

22,000,000

16,200 J

21,400 J

27,600 J

18,200 J

42,600

27,900

53,300

42,900

34,300 J

TAL Metals



Lead



mg/Kg

46.7

218

1.1 J

1.3 J

1.3 J

1.2 J

0.25 U

0.22 U

0.23 U

0.23 U

0.26 U

TAL Metals



Magnesium

mg/Kg

NE

NE

7,290

9,900

11,000

10,100

8,990

7,030

16,600

8,020

22,400

TAL Metals



Manganese

mg/Kg

NE

260

227

301

279

257

212 J

203 J

455 J

211 J

335 J

TAL Metals



Nickel



mg/Kg

20.9

51.6

8.1

6.2

7.3

6.3

8.4

5.9

12.4

7

9.2

TAL Metals



Potassiur

n

mg/Kg

NE

NE

522 J

597

643

502 J

634 J

520 J

1,390

479 J

715

TAL Metals



Selenium



mg/Kg

NE

1

1.3 U

1.2 U

1.2 U

1.3 U

1.4 U

1.3 J

1.3 U

1.3 U

1.5 U

TAL Metals



Silver



mg/Kg

1

3.7

0.16 U

0.16 U

0.15 U

0.16 U

0.18 U

0.16 U

0.17 U

0.17 U

0.19 U

TAL Metals



Sodium



mg/Kg

NE

NE

2,630

1,640

1,900

1,660

3,100

1,660

2,160

1,510

4,320

TAL Metals



Thallium



mg/Kg

NE

NE

0.24 J

0.17 U

0.17 U

0.17 U

0.2 U

0.18 U

0.18 U

0.18 U

0.2 U

TAL Metals



Vanadiurr



mg/Kg

NE

57

44.5

38.2

38.4

38

88.9 J

53.9 J

128 J

72.1 J

60.2 J

TAL Metals



Zinc



mg/Kg

150

410

30

27.9

27.6

27.3

27.3

24.2

48.7

29.2

35.4

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600









6.2

1.7 U

82





TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600









1.7 U

1.7 U

73





TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE









5.6

4.9

53 J





TCL PAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE









9.9

12

31





TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE









1.7 U

1.7 U

31





TCL PAHs

HPAH

Chrysene



ug/Kg

384

2,800









4.5

1.7 U

41





TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260









1.7 U

1.7 U

6.5





TCL PAHs

HPAH

Fluoranthene

ug/Kg

600

5,100









9.1

1.7 U

66





TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE









4.5

6.3

31





TCL PAHs

HPAH

Pyrene



ug/Kg

665

2,600









11

1.7 U

67





TCL PAHs

HPAH

Total HPAH

ug/kg

1,700

9,600









50.8

23.2

481.5





TCL PAHs

LPAH

Acenaphthene

ug/Kg

16

500









1.7 U

1.7 U

1.7 U





TCL PAHs

LPAH

Acenaphthylene

ug/Kg

44

640









1.7 U

1.7 U

6.1





TCL PAHs

LPAH

Anthracene

ug/Kg

85.3

1,100









1.7 U

1.7 U

6.2





TCL PAHs

LPAH

Fluorene



ug/Kg

19

540









1.7 U

1.7 U

1.7 U





TCL PAHs

LPAH

Naphthalene

ug/Kg

160

2,100









1.7 U

1.7 U

1.7 U





TCL PAHs

LPAH

Phenanthrene

ug/Kg

240

1,500









4.8

1.7 U

3.8 J





TCL PAHs

LPAH

Total LPAH

ug/kg

552

3,160









4.8

1.7 U

16.1





TCL PAHs

TPAH

Total PAH

ug/kg

4,022

44,792









55.6

23.2

497.6





TCL PAHs



2-Methylnaphthalene

ug/Kg

70

670









1.7 U

1.7 U

1.7 U





Genchem, TOC



Organic carbon

mg/Kg

NE

NE



6,170















Genchem



Total solids

%

NE

NE



86.7















BulkDensity



Bulk Density

g/cm3

NE

NE



2.14















Grain Size



Particle s

ze, 1 inch (25.40mm)

g

NE

NE



0.00









0.00





Grain Size



Particle s

ze, 1.5 inch (38.1mm)

g

NE

NE



0.00









0.00





Grain Size



Particle s

ze, 2 inch, (50.80mm)

g

NE

NE



0.00









0.00





Grain Size



Particle s

ze, 3 inch, (76.20mm)

g

NE

NE



0.00









0.00





Grain Size



Particle s

ze, 3/4 inch (19.05mm)

g

NE

NE



0.00









0.00





Grain Size



Particle s

ze, 3/8 inch (9.525mm)

g

NE

NE



85.70









0.00





Grain Size



Particle s

ze, Hydrometer (.008 mm)

mg/L

NE

NE



1.00









1.01





Grain Size



Particle s

ze, Hydrometer (.011 mm)

mg/L

NE

NE



1.00









1.01





Grain Size



Particle s

ze, Hydrometer (.015 mm)

mg/L

NE

NE



1.00









1.01





Grain Size



Particle s

ze, Hydrometer (.026 mm)

mg/L

NE

NE



1.00









1.02





Grain Size



Particle s

ze, Hydrometer (.040 mm)

mg/L

NE

NE



1.00









1.02





Grain Size



Particle s

ze, Hydrometer (.041 mm)

mg/L

NE

NE



















Grain Size



Particle s

ze, Hydrometer (0.004mm)

mg/L

NE

NE



1.00









1.01





Grain Size



Particle s

ze, Sieve No. 04, 4 mesh, (4.75mm)

g

NE

NE



92.70









0.00





Grain Size



Particle s

ze, Sieve No. 10, 9 mesh, (2.00mm)

g

NE

NE



132.20









0.00





Grain Size



Particle s

ze, Sieve No. 140,150 mesh, (0.106mm)

g

NE

NE



64.40









60.98





Grain Size



Particle s

ze, Sieve No. 20, 20 mesh, (0.850mm)

g

NE

NE



125.85









1.30





Grain Size



Particle s

ze, Sieve No. 200, 200 mesh, (0.075mm)

g

NE

NE



12.06









47.35





Grain Size



Particle s

ze, Sieve No. 40, 35 mesh, (0.425mm)

g

NE

NE



61.46









5.84





Grain Size



Particle s

ze, Sieve No. 60, 60 mesh, (0.250mm)

g

NE

NE



47.64









12.97





Grain Size



Sample Weight

g

NE

NE



656.40









498.20





Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAH
LPAH = low molecular weight PAH
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown

FD = field duplicate sample
N - normal sample

PAGE 9 OF 10


-------
TABLE 4-4

Marine Sediment Core and Test Pit Sample Results - May 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:

SB-199

SB-202

SB-202

SB-202

SB-209

SB-209

SB-209

SB-222

SB-223

Area

Site

Site

Site

Site

Site

Site

Site

Site

Site



2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

2013SC-SB-

Activity ID:

199-01-

202-00-

9202-00-

202-0 5-

209-00-

209-01-

209-02-

222-00-

223-0 5-



20130524

20130524

20130524FD

20130524

20130527

20130527

20130527

20130530

20130530

Sample Type:

N

N

FD

N

N

N

N

N

N

Date Sampled:

05/24/13

05/24/13

05/24/13

05/24/13

05/27/13

05/27/13

05/27/13

05/30/13

05/30/13

Depth (feet):

1-2

o
o

o
o

0.5 -1

o
o

1 -1.5

2-2.5

o
o

0.5 -1









Screening Level



















ChemGroup



Analyte

Units

ERLa | ERMb



















Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)
b Screening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics - onolyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 10 OF 10


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-301

SB-301

SB-301

SB-301

SB-301

SB-301

SB-301

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130830

20130830

20130830FD

20130830

20130830

20130830

20130830

20130828

20130828

20130828

20130828

20130828

20130828FD

20130828

20130828

20130828

Sample Type:











N

N

FD

N

N

N

N

N

N

N

N

N

FD

N

N

N

Date Sampled:











08/30/13

08/30/13

08/30/13

08/30/13

08/30/13

08/30/13

08/30/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

Depth (feet):











o
o

0.5-1

0.5-1

1-1.5

2-2.5

3-4

4-5

o
o

0.5-1

1-1.5

2-2.5

3-4

3-4

4-5

5-6

6-7









Screening Level

































ChemGroup



Analyte

Units

ERLa

ERMb

































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.083 J

0.073 J

0.066 J

0.11 J

0.024 J

0.0072 U

0.0093 J

0.095 J

0.32

0.082 J

0.063 J

0.089 J

0.071 J

0.14

0.061 J

0.096 J

TAL Metals



Aluminum

mg/Kg

NE

18,000

8,340 J

8,260 J

4,270 J

9,890

7,350 J

7,470 J

8,150 J

6,340

6,250

7,020 J

8,940

9,710

9,060

8,160

10,400

5,340

TAL Metals



Antimony

mg/Kg

NE

9.3

0.22 U

0.17 U

0.18 U

0.17 U

0.18 U

0.18 U

0.16 U

0.18 U

0.16 U

0.16 U

0.16 U

0.16 U

0.16 U

0.17 U

0.18 U

0.17 U

TAL Metals



Arsenic

mg/Kg

8.2

70

0.15 U

0.11 U

0.12 U

0.12 U

0.12 U

0.12 U

0.11 U

0.12 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.12 U

0.12 U

TAL Metals



Barium

mg/Kg

NE

48

1.3 U

1 U

1.1 U

1 U

1.1 U

1.1 U

0.96 U

1.1 U

0.96 U

0.95 U

0.99 U

0.95 U

0.96 U

1 U

1.1 U

1 U

TAL Metals



Beryllium

mg/Kg

NE

NE

0.17 U

0.13 U

0.13 U

0.13 U

0.14 U

0.13 U

0.12 U

0.13 U

0.12 U

0.12 U

0.13 U

0.12 U

0.12 U

0.13 U

0.14 U

0.13 U

TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.12 U

0.096 U

0.099 U

0.098 U

0.1 U

0.1 U

0.091 U

0.099 U

0.091 U

0.09 U

0.093 U

0.09 U

0.09 U

0.097 U

0.1 U

0.098 U

TAL Metals



Calcium

mg/Kg

NE

NE

3,920 J

5,110 J

2,770 J

8,520

5,890 J

6,220 J

2,790 J

3,540

2,660

3,450 J

11,600

12,100

11,500

8,530

21,500

5,130

TAL Metals



Chromium

mg/Kg

81

370

0.21 UJ

0.16 UJ

0.17 UJ

0.17 UJ

0.17 UJ

0.17 UJ

7.9 J

0.17 UJ

0.15 UJ

0.15 UJ

0.16 UJ

0.15 UJ

0.15 UJ

0.17 UJ

0.17 UJ

0.17 UJ

TAL Metals



Cobalt

mg/Kg

NE

10

15.9 J

14.3 J

14.8 J

18.1 J

12.9 J

15.3 J

8.8 J

10.6 J

11.1 J

12 J

13.6 J

13.1 J

14.2 J

14.1 J

13.9 J

11.6 J

TAL Metals



Copper

mg/Kg

34

270

1,340 J

851 J

1,030 J

1,370 J

1,330 J

691 J

55.5 J

1,820 J

1,680 J

3,140 J

2,590 J

2,700 J

2,890 J

5,120 J

981 J

4,090 J

TAL Metals



Iron

mg/Kg

NE

22,000,000

42,500 J

49,100

19,600 J

69,900 J

29,200 J

26,000 J

16,400 J

25,100 J

21,600 J

23,700 J

25,400 J

26,000 J

26,800 J

29,200 J

54,100 J

32,600 J

TAL Metals



Lead

mg/Kg

46.7

218

4.3

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

3.5

0.11 U

0.1 U

0.1 U

0.1 U

0.1 U

0.1 U

0.11 U

0.11 U

0.11 U

TAL Metals



Magnesium

mg/Kg

NE

NE

9,500 J

10,300 J

5,270 J

12,300

9,120 J

9,190 J

7,330 J

7,760

7,620

7,790 J

10,300

10,200

10,000

9,670

12,900

6,970

TAL Metals



Manganese

mg/Kg

NE

260

235 J

239 J

252 J

312 J

229 J

273 J

304 J

186 J

194 J

233 J

287 J

269 J

281 J

252 J

309 J

207 J

TAL Metals



Nickel

mg/Kg

20.9

51.6

10.1 J

7 J

7.3 J

8.8 J

6.1 J

7.4 J

11.2 J

6.4 J

6.7 J

8.7 J

8.4 J

6.9 J

7.4 J

9.3 J

7.3 J

6 J

TAL Metals



Potassium

mg/Kg

NE

NE

742

949

529 J

951

1,160

1,230

240 J

292 J

286 J

408 J

468 J

550

454 J

377 J

662

314 J

TAL Metals



Selenium

mg/Kg

NE

1

0.8 U

0.62 U

0.64 U

0.64 U

0.65 U

0.64 U

0.59 U

0.64 U

0.59 U

0.58 U

0.69 J

1.3 J

1.2 J

3 J

0.65 U

2.8 J

TAL Metals



Silver

mg/Kg

1

3.7

0.1 U

0.079 U

0.082 U

0.081 U

0.083 U

0.082 U

0.075 U

0.082 U

0.075 U

0.074 U

0.077 U

0.074 U

0.074 U

0.08 U

0.083 U

0.081 U

TAL Metals



Sodium

mg/Kg

NE

NE

4,230 J

1,990 J

758 J

1,520

1,680 J

1,440 J

278 J

99.4 J

116 J

239 J

726

466 J

526 J

397 J

252 J

186 J

TAL Metals



Thallium

mg/Kg

NE

NE

0.11 U

0.085 U

0.088 U

0.087 U

0.089 U

0.088 U

0.08 U

0.088 U

0.08 U

0.079 U

0.082 U

0.08 U

0.08 U

0.086 U

0.089 U

0.086 U

TAL Metals



Vanadium

mg/Kg

NE

57

143 J

60.3 J

65.7 J

105 J

52.9 J

57.7 J

34.8 J

42.1 J

41.4 J

45.7 J

53.2 J

56.3 J

64.1 J

54 J

78.8 J

53.7 J

TAL Metals



Zinc

mg/Kg

150

410

35.5 J

26.9 J

28.1 J

32.2 J

24 J

28.6 J

32.5 J

20.8 J

22.7 J

25 J

26.2 J

24.8 J

26.7 J

25.9 J

25.7 J

21.8 J

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

































TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

































TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800

































TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

































TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

































TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600

































TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

































TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500

































TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640

































TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

































TCLPAHs

LPAH

Fluorene

ug/Kg

19

540

































TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100

































TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

































TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160

































TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792

































TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670

































Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 1 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-303

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828

20130828FD

01-20130828

20130828

20130828

Sample Type:











N

N

N

FD

N

N

N

N

N

N

N

N

FD

N

N

N

Date Sampled:











08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

Depth (feet):











7-8

8-9

9-10

9-10

10-11

11-12

12-13

13-14

14-15

15-16

0.5-1

o
o

o
o

1-1.5

2-2.5

3-4









Screening Level

































ChemGroup



Analyte

Units

ERLa

ERMb

































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.075 J

0.05 J

0.15

0.15

0.38

0.078 J

0.008 J

0.0066 U

0.015 J

0.0065 U

0.3 J

0.34 J

0.084 J

0.13 J

0.084 J

0.1 J

TAL Metals



Aluminum

mg/Kg

NE

18,000

7,300

7,900

16,300

13,100

17,600

7,330

8,490 J

6,480

12,900

10,300

9,180 J

12,400 J

9,220 J

9,070 J

12,300 J

8,510 J

TAL Metals



Antimony

mg/Kg

NE

9.3

0.17 U

0.17 U

0.18 U

0.18 U

0.2 U

0.18 U

0.17 U

0.16 U

0.16 U

0.16 U

0.18 U

0.18 U

0.19 U

0.18 U

0.17 U

0.18 U

TAL Metals



Arsenic

mg/Kg

8.2

70

0.11 U

0.11 U

0.12 U

0.12 U

0.13 U

0.12 U

3

0.21 U

3.5

2.8

0.23 U

0.24 U

0.25 U

0.24 U

0.23 U

0.24 U

TAL Metals



Barium

mg/Kg

NE

48

1 U

1 U

1.1 U

1.1 U

1.2 U

1.1 U

1 U

26.9

0.96 U

0.96 U

1.1 U

1.1 U

1.1 U

1.1 U

1 U

1.1 U

TAL Metals



Beryllium

mg/Kg

NE

NE

0.13 U

0.13 U

0.14 U

0.14 U

0.15 U

0.13 U

0.13 U

0.25 U

0.12 U

0.12 U

0.27 U

0.27 U

0.28 U

0.27 U

0.27 U

0.27 U

TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.097 U

0.096 U

0.1 U

0.1 U

0.11 U

0.099 U

0.095 U

0.091 U

0.091 U

0.091 U

0.1 U

0.1 U

0.11 U

0.1 U

0.099 U

0.1 U

TAL Metals



Calcium

mg/Kg

NE

NE

7,530

8,470

18,200

16,200

19,500

6,980

87,900 J

164,000

5,690

8,270

10,800 J

12,900 J

9,240 J

12,600 J

21,700 J

8,480 J

TAL Metals



Chromium

mg/Kg

81

370

0.17 UJ

0.16 UJ

0.17 UJ

0.18 UJ

0.19 UJ

0.17 UJ

9.1 J

0.31 U

9.2

8.2

0.34 U

0.34 U

0.36 U

0.34 U

0.34 U

0.34 U

TAL Metals



Cobalt

mg/Kg

NE

10

16.2 J

15.7 J

23 J

23 J

29.2 J

14.8 J

6.7 J

0.2 UJ

8.2 J

9.4 J

16

16.4

15.7

16.1

14.6

15.2

TAL Metals



Copper

mg/Kg

34

270

1,070 J

891 J

917 J

916 J

2,600 J

2,090 J

470 J

16.2

33.2

43.5

1,110

784

847

1,330

1,390

2,220

TAL Metals



Iron

mg/Kg

NE

22,000,000

24,200 J

27,100 J

50,500 J

55,300 J

68,900

31,500 J

17,800 J

15,000 J

24,900 J

22,200 J

29,500 J

34,500 J

30,800 J

28,400 J

44,200 J

31,000 J

TAL Metals



Lead

mg/Kg

46.7

218

0.11 U

0.11 U

0.11 U

0.12 U

0.12 U

0.11 U

0.11 U

0.1 U

2.8

3.5

0.11 U

0.11 U

0.12 U

0.11 U

0.11 U

0.11 U

TAL Metals



Magnesium

mg/Kg

NE

NE

8,690

9,350

18,700

15,400

20,700

8,460

7,320 J

5,770

10,500

8,880

10,200 J

14,900 J

11,500 J

11,400 J

15,500 J

10,800 J

TAL Metals



Manganese

mg/Kg

NE

260

293 J

290 J

445 J

449 J

555 J

256 J

236 J

194

285

369

315 J

312 J

307 J

328 J

320 J

280 J

TAL Metals



Nickel

mg/Kg

20.9

51.6

9.7 J

8.6 J

13.5 J

13.1 J

13.9 J

7.9 J

6.9 J

0.22 U

10.9

11.2

7.9

7.6

7.9

9

8.3

8.2

TAL Metals



Potassium

mg/Kg

NE

NE

898

779

1,150

1,030

1,390

754

638

322 J

368 J

2,100

635

992

891

715

812

882

TAL Metals



Selenium

mg/Kg

NE

1

0.63 U

0.62 U

0.66 U

0.67 U

0.93 J

0.93 J

0.62 U

1.2 U

0.59 U

0.59 U

1.3 U

1.3 U

1.4 U

1.3 U

1.3 U

1.3 U

TAL Metals



Silver

mg/Kg

1

3.7

0.08 U

0.079 U

0.084 U

0.085 U

0.092 U

0.082 U

0.079 U

0.075 U

0.075 U

0.075 U

0.082 U

0.083 U

0.087 U

0.082 U

0.081 U

0.083 U

TAL Metals



Sodium

mg/Kg

NE

NE

322 J

365 J

572 J

526 J

858

321 J

1,460 J

2,360

554

564

1,730

2,220

2,240

2,230

2,040

1,880

TAL Metals



Thallium

mg/Kg

NE

NE

0.086 U

0.085 U

0.09 U

0.091 U

0.098 U

0.088 U

0.084 U

0.08 U

0.08 U

0.08 U

0.088 U

0.089 U

0.093 U

0.088 U

0.087 U

0.088 U

TAL Metals



Vanadium

mg/Kg

NE

57

81.8 J

81.8 J

118 J

124 J

143 J

53.4 J

36.7 J

0.81 UJ

50.2 J

37.2 J

64.7

68.3

68

68.6

64

60.4

TAL Metals



Zinc

mg/Kg

150

410

29.9 J

28.9 J

43.1 J

42.6 J

55.8 J

25.8 J

31.8 J

22.2

38.9

47.7

30.4

31.9

30

29.8

27.7

28.6

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

































TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

































TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800

































TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

































TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

































TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600

































TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

































TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500

































TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640

































TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

































TCLPAHs

LPAH

Fluorene

ug/Kg

19

540

































TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100

































TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

































TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160

































TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792

































TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670

































Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 2 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-304

SB-305

SB-305

SB-305

SB-305

SB-305

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130828

20130828

20130828

20130828

20130828

20130828

10-20130828

20130828

20130828FD

20130828

20130828

20130827

20130827

20130827

20130827

20130827

Sample Type:











N

N

N

N

N

N

N

N

FD

N

N

N

N

N

N

N

Date Sampled:











08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/28/13

08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

Depth (feet):











4-5

5-6

6-7

7-8

8-9

9-10

10-11

11-12

11-12

12-13

13-14

o
o

0.5-1

1-1.5

2-2.5

3-4









Screening Level

































ChemGroup



Analyte

Units

ERLa

ERMb

































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.15

0.11 J

0.082 J

0.044 J

0.074 J

0.0072 U

0.0076 J

0.0068 U

0.0067 U

0.0076 U

0.0068 U

0.11 J

0.036 J

0.1 J

0.18

0.041 J

TAL Metals



Aluminum

mg/Kg

NE

18,000

11,500

12,600

11,900

7,110

8,980

8,430

9,350

8,460

8,610

13,700

12,500

5,270

5,220

5,790

5,600

5,970

TAL Metals



Antimony

mg/Kg

NE

9.3

0.19 U

0.18 U

0.18 U

0.18 U

0.17 U

0.18 U

0.17 U

0.17 U

0.17 U

0.18 U

0.17 U

0.17 U

0.18 U

0.18 U

0.18 U

0.18 U

TAL Metals



Arsenic

mg/Kg

8.2

70

0.12 U

0.23 U

0.12 U

0.12 U

0.12 U

9.5

4.4

0.11 U

3.1

4.8

0.11 U

0.11 U

0.12 U

0.12 U

0.12 U

0.12 U

TAL Metals



Barium

mg/Kg

NE

48

1.1 U

1.1 U

1.1 U

1.1 U

1 U

1.1 U

1 U

1 U

1 U

1.1 U

1 U

1 U

1.1 U

1.1 U

1.1 U

1.1 U

TAL Metals



Beryllium

mg/Kg

NE

NE

0.14 U

0.27 U

0.14 U

0.14 U

0.13 U

0.14 U

0.13 U

0.13 U

0.13 U

0.14 U

0.13 U

0.13 U

0.14 U

0.14 U

0.14 U

0.14 U

TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.11 U

0.1 U

0.1 U

0.1 U

0.098 U

0.1 U

0.098 U

0.096 U

0.095 U

0.1 U

0.096 U

0.097 U

0.1 U

0.1 U

0.1 U

0.1 U

TAL Metals



Calcium

mg/Kg

NE

NE

12,600

17,900

16,000

9,360

5,690

6,810

39,400

75,800

69,500

23,900

4,270

4,220

5,210

5,480

5,170

6,240

TAL Metals



Chromium

mg/Kg

81

370

0.18 UJ

0.34 UJ

0.17 UJ

0.17 UJ

0.17 UJ

7.6 J

7.8 J

8.7 J

7.1 J

8.5 J

8.1 J

0.17 U

0.17 U

0.17 U

0.18 U

0.17 U

TAL Metals



Cobalt

mg/Kg

NE

10

17.2 J

14 J

14.9 J

11.3 J

11.3 J

7.2 J

5.2 J

4.6 J

4.3 J

9 J

8.1 J

11.6 J

10.5 J

10.3 J

12.6 J

12.3 J

TAL Metals



Copper

mg/Kg

34

270

872

1,960

1,080

2,140

4,160

46.5

31.7 J

18.9

15.4

103 J

39.5 J

1,330

1,020

1,080

1,100

903

TAL Metals



Iron

mg/Kg

NE

22,000,000

53,900

65,400

57,600

20,600

33,600

17,300

17,500 J

15,000

15,400

25,000 J

24,700 J

34,400 J

32,500 J

33,300 J

59,800 J

60,600 J

TAL Metals



Lead

mg/Kg

46.7

218

0.12 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.12 U

5.8

0.11 U

0.11 U

0.11 U

0.12 U

0.11 U

TAL Metals



Magnesium

mg/Kg

NE

NE

13,400

13,900

14,800

9,140

10,200

8,120

8,500

8,240

8,250

12,800

12,300

6,330

6,090

7,200

6,790

6,810

TAL Metals



Manganese

mg/Kg

NE

260

333 J

293 J

306 J

213 J

236 J

279 J

253 J

226 J

237 J

309 J

293 J

194

182

174

215

207

TAL Metals



Nickel

mg/Kg

20.9

51.6

8.4 J

7.8 J

9.1 J

5.7 J

7.5 J

9.8 J

7.6 J

7 J

5.7 J

10.6 J

10.3 J

6.2

5.6

5.6

7.6

7.2

TAL Metals



Potassium

mg/Kg

NE

NE

889

757

1,040

630

752

548 J

557 J

523 J

435 J

495 J

390 J

543 J

661

578 J

512 J

521 J

TAL Metals



Selenium

mg/Kg

NE

1

0.69 U

1.3 U

0.66 U

0.87 J

2.4 J

0.65 U

0.63 U

0.62 U

0.61 U

0.67 U

0.62 U

0.63 U

0.65 U

0.65 U

0.67 U

0.66 U

TAL Metals



Silver

mg/Kg

1

3.7

0.087 U

0.082 U

0.084 U

0.084 U

0.081 U

0.083 U

0.08 U

0.079 U

0.078 U

0.086 U

0.079 U

0.08 U

0.083 U

0.083 U

0.085 U

0.084 U

TAL Metals



Sodium

mg/Kg

NE

NE

2,030

1,990

2,070

1,950

1,910

1,810

1,940

1,670

1,730

1,470

874

1,490

1,500

1,790

2,580

2,400

TAL Metals



Thallium

mg/Kg

NE

NE

0.094 U

0.088 U

0.09 U

0.09 U

0.087 U

0.088 U

0.086 U

0.085 U

0.084 U

0.092 U

0.085 U

0.086 U

0.089 U

0.089 U

0.091 U

0.09 U

TAL Metals



Vanadium

mg/Kg

NE

57

91.3

61.4

81.7

47.2

44.6

41.4

34.3 J

33.5

32.5

44.3 J

44.1 J

56.3 J

49.1 J

56.2 J

98.6 J

102 J

TAL Metals



Zinc

mg/Kg

150

410

36.2 J

26.9 J

28.5 J

20.8 J

26.7 J

32.3 J

26.8 J

24.4 J

26.2 J

37 J

32.8 J

22.6

20.9

19.9

24.6

22.7

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

































TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

































TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800

































TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

































TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

































TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

































TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600

































TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

































TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500

































TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640

































TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

































TCLPAHs

LPAH

Fluorene

ug/Kg

19

540

































TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100

































TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

































TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160

































TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792

































TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670

































Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 3 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-305

SB-305

SB-305

SB-305

SB-305

SB-305

SB-305

SB-305

SB-305

SB-306

SB-306

SB-306

SB-306

SB-306

SB-306

SB-306

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130827FD

20130827

20130827

20130827

20130827

20130827

20130827

20130827FD

20130827

20130829

20130829

20130829FD

20130829

20130829

20130829

20130829

Sample Type:











FD

N

N

N

N

N

N

FD

N

N

N

FD

N

N

N

N

Date Sampled:











08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

08/27/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

Depth (feet):











3-4

4-5

5-6

6-7

7-8

8-9

9-10

9-10

10-11

0.5-1

o
o

0.5-1

1-1.5

2-2.5

3-4

4-5









Screening Level

































ChemGroup



Analyte

Units

ERLa

ERMb

































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.043 J

0.086 J

0.052 J

0.35

0.55

0.084 J

0.0064 U

0.0068 U

0.0077 U

0.064 J

0.14



0.96





0.021 J

TAL Metals



Aluminum

mg/Kg

NE

18,000

6,650

6,820

16,500

7,820

9,750

11,100

10,100

9,950

6,110

5,810

6,440



8,170





18,000

TAL Metals



Antimony

mg/Kg

NE

9.3

0.18 U

0.18 U

0.2 U

0.17 U

0.18 U

0.19 U

0.16 U

0.17 U

0.19 U

0.17 U

0.18 U



0.19 U





0.17 U

TAL Metals



Arsenic

mg/Kg

8.2

70

0.24 U

0.12 U

0.13 U

0.23 U

0.12 U

0.12 U

6.1

0.22 U

4.1

0.11 U

0.12 U



0.12 U





3.4

TAL Metals



Barium

mg/Kg

NE

48

1.1 U

1.1 U

1.2 U

1 U

1.1 U

1.1 U

0.95 U

1 U

35

1 U

1.1 U



1.1 U





1 U

TAL Metals



Beryllium

mg/Kg

NE

NE

0.28 U

0.13 U

0.15 U

0.27 U

0.14 U

0.14 U

0.24 U

0.26 U

0.15 U

0.13 U

0.14 U



0.14 U





0.13 U

TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.1 U

0.1 U

0.11 U

0.098 U

0.1 U

0.11 U

0.09 U

0.095 U

0.11 U

0.097 U

0.1 U



0.11 U





0.098 U

TAL Metals



Calcium

mg/Kg

NE

NE

6,130

6,770

17,000

8,350

10,400

6,390

23,300 J

41,900 J

190,000

2,690

7,370



3,860





3,390

TAL Metals



Chromium

mg/Kg

81

370

0.35 U

0.17 U

0.19 U

0.33 U

0.17 U

0.18 U

11.1

13.3

8.9

0.17 UJ

0.18 UJ



0.18 UJ





10.3 J

TAL Metals



Cobalt

mg/Kg

NE

10

11.5 J

13.6 J

25 J

14.3 J

19.8 J

12.4 J

5.8 J

0.21 UJ

4 J

11.2 J

11.2 J



12.7 J





7.5 J

TAL Metals



Copper

mg/Kg

34

270

1,100

1,700

1,570

1,430

1,380

1,820

19.7

16

12.1

2,080

2,980



1,970





55.2

TAL Metals



Iron

mg/Kg

NE

22,000,000

69,000 J

62,000 J

68,600 J

23,700 J

44,200 J

30,300 J

18,200 J

17,500 J

11,600 J

55,200

101,000



77,300





32,400

TAL Metals



Lead

mg/Kg

46.7

218

0.12 U

0.11 U

0.13 U

0.11 U

0.11 U

0.12 U

0.1 U

0.11 U

0.12 U

0.11 U

16.4



7.2





0.11 U

TAL Metals



Magnesium

mg/Kg

NE

NE

7,840

8,150

19,300

9,890

12,000

11,000

9,170

8,590

5,940

7,180

7,710



10,100





14,300

TAL Metals



Manganese

mg/Kg

NE

260

206

238

426

263

340

295

281

267

180

182 J

196 J



219 J





305 J

TAL Metals



Nickel

mg/Kg

20.9

51.6

8.1

8.1

13.4

7.7

10.5

9.9

9.5

9.8

7.1

5.8 J

6.4 J



6.9 J





9.9 J

TAL Metals



Potassium

mg/Kg

NE

NE

722

656

1,440

781

1,010

801

495 J

546 J

461 J

346 J

452 J



608 J





580 J

TAL Metals



Selenium

mg/Kg

NE

1

1.3 U

0.65 U

0.73 U

1.3 U

0.66 U

0.68 U

1.2 U

1.2 U

0.71 U

1.3 J

3 J



1.1 J





0.64 U

TAL Metals



Silver

mg/Kg

1

3.7

0.086 U

0.082 U

0.093 U

0.081 U

0.084 U

0.087 U

0.074 U

0.078 U

0.09 U

0.08 U

0.086 U



0.087 U





0.081 U

TAL Metals



Sodium

mg/Kg

NE

NE

2,560

2,190

2,990

1,640

2,280

2,140

1,560 J

2,400 J

4,140

1,600

2,010



2,470





1,680

TAL Metals



Thallium

mg/Kg

NE

NE

0.092 U

0.088 U

0.099 U

0.087 U

0.09 U

0.093 U

0.079 U

0.084 U

0.097 U

0.086 U

0.092 U



0.093 U





0.087 U

TAL Metals



Vanadium

mg/Kg

NE

57

95.3 J

90.3 J

136 J

52.4 J

108 J

61.6 J

40.1 J

36.7 J

24.4 J

78.1

59.2



61.8





43.9

TAL Metals



Zinc

mg/Kg

150

410

19.2

26.3

56

31.6

42.4

37.6

33.6

34.3

23.9

21.1 J

30.5 J



249 J





40.1 J

TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600



















31

43

110

140

90

33



TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600



















27

48 J

81 J

58 J

43

25



TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE



















18

30

53

51

36

19



TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE



















18

33

34

39

31 J

22



TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE



















14

26

34

1.7 UJ

33 J

15



TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800



















15

35

30

68

38 J

19



TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260



















3.4 J

1.7 U

7.9

9.3

7.3 J

3.8



TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100



















33

65

280

410

290

20



TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE



















14

26

33

38

28 J

16



TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600



















43

69

340

410

290

17



TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600



















216.4

375

1002.9

1223.3

886.3

189.8



TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500



















1.7 U

1.7 U

1.7 U

24

64

6.5



TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640



















4.9

9.3

6.1

6.8

6.1 J

1.7 U



TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100



















5

67

12

30

47

9.7



TCLPAHs

LPAH

Fluorene

ug/Kg

19

540



















1.7 U

1.7 U

1.7 U

4.7

11 J

1.7 U



TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100



















1.7 U

1.7 U

1.7 U

12

7.1 J

5



TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500



















13

20

7.3

8.9

49

4.1



TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160



















22.9

96.3

25.4

86.4

184.2

25.3



TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792



















239.3

471.3

1,028

1,314

1,071

215.1



TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670



















1.7 U

1.7 U

1.7 U

4 J

1.7 UJ

1.7 U



Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 4 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-306

SB-306

SB-306

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

SB-307

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130829

20130829

20130829

20130829

20130829

20130829

20130829FD

20130829

20130829

20130829

20130829

20130829

20130829

20130829

20130829

20130829

Sample Type:











N

N

N

N

N

N

FD

N

N

N

N

N

N

N

N

N

Date Sampled:











08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

Depth (feet):











5-6

6-7

7-8

o
o

0.5-1

1-1.5

1-1.5

2-2.5

3-4

4-5

5-6

6-7

7-8

8-9

9-10

8.5-9









Screening Level

































ChemGroup



Analyte

Units

ERLa

ERMb

































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.016 J

0.0066 U

0.0065 U

0.059 J

0.096 J

0.076 J

0.11 J

0.07 J

0.074 J

0.054 J

0.066 J

0.23 J

0.46 J

0.0076 J

0.0068 J



TAL Metals



Aluminum

mg/Kg

NE

18,000

13,200

12,300

13,600

6,920 J

7,280 J

6,770 J

7,340 J

6,010 J

7,130 J

6,740 J

7,570 J

12,800 J

11,800 J

11,700 J

5,940 J



TAL Metals



Antimony

mg/Kg

NE

9.3

0.17 U

0.16 U

0.16 U

0.17 U

0.17 U

0.17 U

0.17 U

0.17 U

0.17 U

0.18 U

0.18 U

0.18 U

0.18 U

0.17 U

0.17 U



TAL Metals



Arsenic

mg/Kg

8.2

70

3.6

0.11 U

2.9

0.22 U

0.23 U

0.23 U

0.23 U

0.23 U

0.23 U

0.24 U

0.24 U

0.24 U

0.24 U

0.23 U

0.11 U



TAL Metals



Barium

mg/Kg

NE

48

1 U

0.98 U

0.94 U

1 U

1 U

1 U

1 U

1 U

1 U

1.1 U

1.1 U

1.1 U

1.1 U

1 U

28.7



TAL Metals



Beryllium

mg/Kg

NE

NE

0.13 U

0.12 U

0.12 U

0.26 U

0.26 U

0.26 U

0.26 U

0.27 U

0.27 U

0.27 U

0.27 U

0.28 U

0.28 U

0.26 U

0.13 U



TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.096 U

0.092 U

0.089 U

0.095 U

0.098 U

0.097 U

0.098 U

0.098 U

0.098 U

0.1 U

0.1 U

0.1 U

0.1 U

0.097 U

0.094 U



TAL Metals



Calcium

mg/Kg

NE

NE

4,030

3,580

4,390

6,850 J

7,860 J

7,010 J

7,360 J

6,760 J

7,590 J

8,840 J

8,990 J

14,100 J

13,000 J

7,750 J

206,000 J



TAL Metals



Chromium

mg/Kg

81

370

CO
CO

7.9

9.4

0.33 U

0.33 U

0.33 U

0.33 U

0.34 U

0.34 U

0.34 U

0.34 U

0.35 U

0.35 U

0.33 U

5.7



TAL Metals



Cobalt

mg/Kg

NE

10

7.5 J

6.9 J

7.1 J

10.8

13.4

11.3

11.3

11.7

10.8

10.4

15.2

17.8

15.9

6.8

3.7



TAL Metals



Copper

mg/Kg

34

270

42.3

38.8

34

1,250

816

712

874

1,130

1,360

369

542

1,000

4,910

74.7

40.4



TAL Metals



Iron

mg/Kg

NE

22,000,000

23,100 J

23,100 J

24,800 J

32,500 J

25,800 J

43,300 J

27,600 J

28,500 J

31,700 J

46,600 J

47,100 J

65,600 J

45,800 J

20,200 J

10,800 J



TAL Metals



Lead

mg/Kg

46.7

218

0.11 U

0.1 U

0.1 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.1 U



TAL Metals



Magnesium

mg/Kg

NE

NE

10,700

10,400

11,000

8,730 J

9,230 J

8,400 J

9,300 J

7,540 J

8,860 J

8,530 J

9,480 J

15,100 J

14,800 J

12,500 J

6,500 J



TAL Metals



Manganese

mg/Kg

NE

260

252

258

262

214 J

253 J

217 J

213 J

224 J

215 J

210 J

295 J

340 J

321 J

300 J

181 J



TAL Metals



Nickel

mg/Kg

20.9

51.6

11.7

11.1

12.4

0.24 U

7

5.8

5.8

6.1

0.24 U

0.25 U

7.5

9.4

8.1

12.9

4.6



TAL Metals



Potassium

mg/Kg

NE

NE

499 J

348 J

392 J

622

757

570 J

719

439 J

509 J

531 J

665

994

844

464 J

388 J



TAL Metals



Selenium

mg/Kg

NE

1

0.62 U

0.6 U

0.58 U

1.2 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

0.61 U



TAL Metals



Silver

mg/Kg

1

3.7

0.079 U

0.076 U

0.073 U

0.079 U

0.081 U

0.08 U

0.08 U

0.081 U

0.081 U

0.082 U

0.083 U

0.084 U

0.085 U

0.08 U

0.077 U



TAL Metals



Sodium

mg/Kg

NE

NE

1,190

987

726

1,650

1,470

1,750

1,860

2,080

2,380

2,920

2,540

2,650

2,260

1,060

2,770



TAL Metals



Thallium

mg/Kg

NE

NE

0.084 U

0.081 U

0.079 U

0.084 U

0.086 U

0.086 U

0.086 U

0.087 U

0.087 U

0.088 U

0.089 U

0.09 U

0.091 U

0.085 U

0.083 U



TAL Metals



Vanadium

mg/Kg

NE

57

38.8 J

37.6 J

40.8 J

43.6

51.8

47.6

48.2

54.2

45.1

55.1

76.1

92.4

70.6

38.7

22.6



TAL Metals



Zinc

mg/Kg

150

410

35.1

29.2

34.3

20

24.8

21

21.3

22.3

20.2

18.6

27.4

35.7

42.6

34.9

19.9



TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600





1.7 U

























1.7 U

TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600





1.7 U

























1.7 U

TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE





1.7 U

























1.7 U

TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE





9.7

























3.9

TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE





1.7 U

























1.7 U

TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800





1.7 U

























1.7 U

TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260





1.7 U

























1.7 U

TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100





1.7 U

























36

TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE





1.7 U

























1.7 U

TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600





1.7 U

























14

TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600





9.7

























53.9

TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500





1.7 U

























1.7 U

TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640





1.7 U

























1.7 U

TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100





1.7 U

























1.7 U

TCLPAHs

LPAH

Fluorene

ug/Kg

19

540





1.7 U

























1.7 U

TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100





1.7 U

























1.7 U

TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500





1.7 U

























1.7 U

TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160





1.7 U

























1.7 U

TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792





9.7

























53.9

TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670





1.7 U

























1.7 U

Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 5 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-308

SB-313

SB-313

SB-316

SB-316

SB-319

Area











Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:











20130829

20130829

20130829FD

20130829

20130829

20130829

20130829

20130829

20130829

20130829

20130829

20130829

20130828

20130828

20130830

20130828

20130829

Sample Type:











N

N

FD

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:











08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/29/13

08/28/13

08/28/13

08/30/13

08/28/13

08/29/13

Depth (feet):











o
o

0.5-1

0.5-1

1-1.5

2-2.5

3-4

4-5

5-6

6-7

7-8

8-9

9-10

2-2.5

3-4

3-4

7-8

4-5









Screening Level



































ChemGroup



Analyte

Units

ERLa

ERMb



































Metals, Hg



Mercury

mg/Kg

0.15

0.71

0.061 J

0.11

0.12

0.11 J

0.14

0.056 J

0.082 J

0.038 J

0.052 J

1.7

0.0098 J

0.0077 J











TAL Metals



Aluminum

mg/Kg

NE

18,000

6,700

7,020

7,350

6,380

6,260

6,310

6,410

6,850

6,730

5,930

10,900 J

13,400 J











TAL Metals



Antimony

mg/Kg

NE

9.3

0.16 U

0.16 U

0.16 U

0.17 U

0.17 U

0.17 U

0.18 U

0.17 U

0.18 U

0.17 U

0.18 U

0.18 U











TAL Metals



Arsenic

mg/Kg

8.2

70

0.11 U

0.11 U

0.11 U

0.11 U

0.12 U

0.12 U

0.12 U

0.12 U

0.12 U

0.11 U

0.24 U

0.23 U











TAL Metals



Barium

mg/Kg

NE

48

0.96 U

0.96 U

0.97 U

1 U

1 U

1 U

1.1 U

1 U

1.1 U

1 U

1.1 U

1.1 U











TAL Metals



Beryllium

mg/Kg

NE

NE

0.12 U

0.12 U

0.12 U

0.13 U

0.13 U

0.13 U

0.13 U

0.13 U

0.14 U

0.13 U

0.28 U

0.27 U











TAL Metals



Cadmium

mg/Kg

1.2

9.6

0.091 U

0.091 U

0.092 U

0.095 U

0.099 U

0.099 U

0.1 U

0.099 U

0.1 U

0.097 U

0.1 U

0.1 U











TAL Metals



Calcium

mg/Kg

NE

NE

4,430

6,180

6,530

5,900

5,850

3,910

2,880

2,860

2,790

2,540

3,090 J

3,460 J











TAL Metals



Chromium

mg/Kg

81

370

0.16 UJ

0.16 UJ

0.16 UJ

0.16 UJ

0.17 UJ

0.17 UJ

0.17 UJ

0.17 UJ

0.17 UJ

0.17 UJ

0.35 U

12.1











TAL Metals



Cobalt

mg/Kg

NE

10

11.6 J

12.5 J

13.1 J

12.6 J

10.7 J

17.6 J

10 J

10.8 J

10.5 J

10.4 J

12.3

11.9











TAL Metals



Copper

mg/Kg

34

270

1,920

1,490

1,390

1,470

1,140

2,350

307

327

570 J

1,960 J

53.4

36.9











TAL Metals



Iron

mg/Kg

NE

22,000,000

54,700

54,500

58,200

56,000

47,400

57,500

61,600

46,500

23,900 J

20,900 J

20,600 J

22,700 J











TAL Metals



Lead

mg/Kg

46.7

218

0.1 U

0.1 U

0.1 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U

0.11 U











TAL Metals



Magnesium

mg/Kg

NE

NE

8,260

8,770

9,220

7,810

7,980

8,000

8,010

8,510

8,400

7,510

8,760 J

10,800 J











TAL Metals



Manganese

mg/Kg

NE

260

219 J

233 J

241 J

223 J

198 J

315 J

176 J

0.16 UJ

175 J

168 J

295 J

283 J











TAL Metals



Nickel

mg/Kg

20.9

51.6

5.8 J

6 J

6.2 J

6.5 J

5.6 J

9.4 J

5 J

5.4 J

5.2 J

5.1 J

15.6

12











TAL Metals



Potassium

mg/Kg

NE

NE

495 J

562

645

504 J

440 J

400 J

409 J

469 J

611

419 J

390 J

591 J











TAL Metals



Selenium

mg/Kg

NE

1

0.59 U

0.59 U

0.59 U

0.62 U

0.64 U

0.77 J

0.64 U

0.64 U

0.65 U

1.2 J

1.3 U

1.3 U











TAL Metals



Silver

mg/Kg

1

3.7

0.075 U

0.075 U

0.075 U

0.078 U

0.082 U

0.081 U

0.082 U

0.082 U

0.082 U

0.08 U

0.084 U

0.082 U











TAL Metals



Sodium

mg/Kg

NE

NE

835

945

906

1,220

1,310

1,290

1,200

1,440

1,300

1,130

886

836











TAL Metals



Thallium

mg/Kg

NE

NE

0.08 U

0.08 U

0.081 U

0.084 U

0.087 U

0.087 U

0.088 U

0.087 U

0.088 U

0.085 U

0.09 U

0.088 U











TAL Metals



Vanadium

mg/Kg

NE

57

54.3

55.2

56.5

57.7

47.3

91.2

49.2

0.44 U

49.8 J

42.2 J

40.3

44.2











TAL Metals



Zinc

mg/Kg

150

410

21.2 J

22.8 J

23.9 J

23 J

20.7 J

35.6 J

21.7 J

23.6 J

22.3 J

23.6 J

48.5

70











TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

























1.7 U

10

1.7 U

42

1.7 U

TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

























1.7 U

16

1.7 U

14

1.7 U

TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

























1.7 U

11

1.7 U

10

1.7 U

TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

























7.7

14

6.3

8

4.4

TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

























1.7 U

7

1.7 U

9

1.7 U

TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800

























1.7 U

8.5

1.7 U

21

1.7 U

TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

























1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

























3.7 J

24

5.5

310

36

TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

























3.8 J

8

1.7 U

4.3

1.7 U

TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600

























6.5

39

6

310

26

TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

























21.7

137.5

17.8

728.3

66.4

TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500

























1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640

























1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

























1.7 U

1.7 U

4.3

51

1.7 U

TCLPAHs

LPAH

Fluorene

ug/Kg

19

540

























1.7 U

1.7 U

5.4

1.7 U

1.7 U

TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100

























1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

























1.7 U

1.7 U

1.7 U

13

1.7 U

TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160

























1.7 U

1.7 U

9.7

64

1.7 U

TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792

























21.7

137.5

27.5

792.3

66.4

TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670

























1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 6 OF 7


-------
TABLE 4-5

Marine Sediment Core and Test Pit Sample Results - August 2013

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:











SB-322

SB-322

Area











Site

Site

Activity ID:











20130830

20130830

Sample Type:











N

N

Date Sampled:











08/30/13

08/30/13

Depth (feet):











2-2.5

4-5









Screening Level





ChemGroup



Analyte

Units

ERLa

ERMb





Metals, Hg



Mercury

mg/Kg

0.15

0.71





TAL Metals



Aluminum

mg/Kg

NE

18,000





TAL Metals



Antimony

mg/Kg

NE

9.3





TAL Metals



Arsenic

mg/Kg

8.2

70





TAL Metals



Barium

mg/Kg

NE

48





TAL Metals



Beryllium

mg/Kg

NE

NE





TAL Metals



Cadmium

mg/Kg

1.2

9.6





TAL Metals



Calcium

mg/Kg

NE

NE





TAL Metals



Chromium

mg/Kg

81

370





TAL Metals



Cobalt

mg/Kg

NE

10





TAL Metals



Copper

mg/Kg

34

270





TAL Metals



Iron

mg/Kg

NE

22,000,000





TAL Metals



Lead

mg/Kg

46.7

218





TAL Metals



Magnesium

mg/Kg

NE

NE





TAL Metals



Manganese

mg/Kg

NE

260





TAL Metals



Nickel

mg/Kg

20.9

51.6





TAL Metals



Potassium

mg/Kg

NE

NE





TAL Metals



Selenium

mg/Kg

NE

1





TAL Metals



Silver

mg/Kg

1

3.7





TAL Metals



Sodium

mg/Kg

NE

NE





TAL Metals



Thallium

mg/Kg

NE

NE





TAL Metals



Vanadium

mg/Kg

NE

57





TAL Metals



Zinc

mg/Kg

150

410





TCLPAHs

HPAH

Benz(a)anthracene

ug/Kg

261

1,600

36

1.7 U

TCLPAHs

HPAH

Benzo(a)pyrene

ug/Kg

430

1,600

15

1.7 U

TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/Kg

NE

NE

13

3.1 J

TCLPAHs

HPAH

Benzo(ghi)perylene

ug/Kg

NE

NE

12

8.9

TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/Kg

NE

NE

11

1.7 U

TCLPAHs

HPAH

Chrysene

ug/Kg

384

2,800

22

1.7 U

TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/Kg

63.4

260

1.7 U

1.7 U

TCLPAHs

HPAH

Fluoranthene

ug/Kg

600

5,100

250

1.7 U

TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/Kg

NE

NE

6.8

1.7 U

TCLPAHs

HPAH

Pyrene

ug/Kg

665

2,600

250

1.7 U

TCLPAHs

HPAH

Total HPAH

ug/kg

1,700

9,600

615.8

12

TCLPAHs

LPAH

Acenaphthene

ug/Kg

16

500

1.7 U

1.7 U

TCLPAHs

LPAH

Acenaphthylene

ug/Kg

44

640

1.7 U

1.7 U

TCLPAHs

LPAH

Anthracene

ug/Kg

85.3

1,100

4.1

1.7 U

TCLPAHs

LPAH

Fluorene

ug/Kg

19

540

1.7 U

1.7 U

TCLPAHs

LPAH

Naphthalene

ug/Kg

160

2,100

1.7 U

1.7 U

TCLPAHs

LPAH

Phenanthrene

ug/Kg

240

1,500

3.8 J

1.7 U

TCLPAHs

LPAH

Total LPAH

ug/kg

552

3,160

7.9

1.7 U

TCLPAHs

TPAH

Total PAH

ug/kg

4,022

44,792

623.7

12

TCLPAHs



2-Methylnaphthalene

ug/Kg

70

670

1.7 U

1.7 U

Notes:

PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-
ug/L = micrograms per liter
mg/L = milligrams per liter
mg/Kg = milligrams per kilogram
g= grams

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method detection limit showi

FD = field duplicate sample
N = normal sample

Screening Level = Marine sediment ERL value listed in NOAA SQuiRT (Buchman, 2008)

bScreening Level = Marine sediment ERM value (AET, if no ERM) listed in NOAA SQuiRT (Buchman, 2008)

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds minimum screening level (ERL if available, ERM if no ERL)

Italics = analyte not detected but method detection limit exceeds the minimum screening level (ERL if available, ERM if no ERL)

PAGE 7 OF 7


-------
TABLE 4-6

Marine Sediment Core and Test Pit Sample Results - Modified SPLP Metals Analysis

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SB-004

SB-004

SB-004

SB-013

SB-013

SB-021

SB-032

SB-032

SB-033

SB-033

SB-052

Area







Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:







0_5-20130528

20130528

20130528FD

20130528

00-20130528

20130528

0_5-20130527

20130527

20130527

20130527

20130528

Sample Type:







N

N

FD

N

N

N

N

N

N

N

N

Date Sampled:







05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/27/13

05/27/13

05/28/13

Depth (feet):







0.5 -1

0-0.5

0.5 -1

0.5 -1

0-0.5

0.5 -1

0.5 -1

0-0.5

0.5 -1

0-0.5

0.5 -1



Analyte

Units

Screening Level3



Modified SPLP

Aluminum

ug/L

NE

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

Modified SPLP

Antimony

ug/L

500

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

Modified SPLP

Arsenic

ug/L

36

2.5 UJ

2.5 U

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 U

Modified SPLP

Barium

ug/L

200

120 J

40 J

170 J

130 J

110 J

160 J

140 J

63 J

95 J

150 J

160 J

Modified SPLP

Beryllium

ug/L

100

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

Modified SPLP

Cadmium

ug/L

8.8

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.5 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

Modified SPLP

Calcium

ug/L

NE

305,000

313,000

305,000

308,000

302,000

296,000

312,000

310,000

315,000

317,000

326,000

Modified SPLP

Chromium

ug/L

27.4

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

Modified SPLP

Cobalt

ug/L

1

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

54

8.6 U

8.6 U

8.6 U

2.9

8.6 U

Modified SPLP

Copper

ug/L

3.1

104

138

167

30

51

472

2.1 U

2.1 U

2.1 U

121

42

Modified SPLP

Iron

ug/L

50

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

160

2,410

7.8 U

7.8 U

7.8 U

Modified SPLP

Lead

ug/L

8.1

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

2 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

Modified SPLP

Magnesium

ug/L

NE

1,060,000

1,070,000

1,060,000

1,060,000

1,060,000

1.03E+06

1,060,000

1,050,000

1,050,000

1,060,000

1,060,000

Modified SPLP

Manganese

ug/L

100

7.2 U

7.2 U

7.2 U

7.2 U

7.2 U

7.3 U

32

7.2 U

160

51

7.2 U

Modified SPLP

Mercury

ug/L

0.94

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

Modified SPLP

Nickel

ug/L

8.2

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

Modified SPLP

Potassium

ug/L

NE

404,000

412,000

407,000

407,000

423,000

414,000

397,000

404,000

405,000

411,000

374,000

Modified SPLP

Selenium

ug/L

71

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

Modified SPLP

Silver

ug/L

0.95

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

Modified SPLP

Sodium

ug/L

NE

9,100,000 J

9,220,000

9,200,000 J

9,300,000 J

9,400,000 J

9.20E+06 J

9,100,000 J

9,100,000 J

9,100,000 J

9,200,000 J

8,870,000

Modified SPLP

Thallium

ug/L

17

0.94 U

0.94 UJ

0.94 U

0.94 U

0.94 U

0.95 U

0.94 U

0.94 U

0.94 U

0.94 U

0.94 UJ

Modified SPLP

Vanadium

ug/L

50

2 U

2 U

2 U

2 U

2 U

31

2 U

2 U

2 U

2 U

2 U

Modified SPLP

Zinc

ug/L

81

44 J

1.7 U

80.5 J

50 J

39 J

83.4 J

50 J

16 J

35 J

89.5 J

64.5 J

Notes:

ug/L = micrograms per liter

J = The analyte was positively identified; the quantitation is an estimation.

U =The analyte was analyzed for, but not detected at the method detection limit shown
FD = field duplicate sample
N = normal sample

a Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of
preference:

a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 1 OF 3


-------
TABLE 4-6

Marine Sediment Core and Test Pit Sample Results - Modified SPLP Metals Analysis

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SB-052

SB-052

SB-059

SB-059

SB-059

SB-062

SB-062

SB-062

SB-078

SB-078

SB-078

SB-079

SB-079

SB-079

Area







Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:







20130528

20130528

0_5-20130527

20130527

20130527

20130528

20130528

20130528

0_5-20130528

20130528

20130528

20130528

20130528

20130528

Sample Type:







N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:







05/28/13

05/28/13

05/27/13

05/27/13

05/27/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

Depth (feet):







0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2

0.5 -1

0-0.5

1-2



Analyte

Units

Screening Level3



Modified SPLP

Aluminum

ug/L

NE

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

25 U

Modified SPLP

Antimony

ug/L

500

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

Modified SPLP

Arsenic

ug/L

36

2.5 U

2.5 U

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 UJ

2.5 U

2.5 UJ

2.5 U

2.5 UJ

2.5 UJ

Modified SPLP

Barium

ug/L

200

150 J

130 J

130 J

190 J

120 J

150 J

130 J

180 J

130 J

110 J

170 J

110 J

110 J

180 J

Modified SPLP

Beryllium

ug/L

100

2 U

2 U

2 U

2 U

2 U

2 U

2 UJ

2 U

2 U

2 U

2 UJ

2 U

2 UJ

2 UJ

Modified SPLP

Cadmium

ug/L

8.8

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

Modified SPLP

Calcium

ug/L

NE

326,000

318,000

311,000

311,000

311,000

308,000

303,000

312,000

307,000

327,000

309,000

326,000

291,000

280,000

Modified SPLP

Chromium

ug/L

27.4

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

Modified SPLP

Cobalt

ug/L

1

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

8.6 U

Modified SPLP

Copper

ug/L

3.1

36

32

45

21

31

21

32

14

21

28

20

2.1 U

2.1 U

2.1 U

Modified SPLP

Iron

ug/L

50

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

7.8 U

Modified SPLP

Lead

ug/L

8.1

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

Modified SPLP

Magnesium

ug/L

NE

1,060,000

1,050,000

1,060,000

1,030,000

1,050,000

1,060,000

1,060,000

1,040,000

1,050,000

1,080,000

1,040,000

1,070,000

1,020,000

980,000

Modified SPLP

Manganese

ug/L

100

7.2 U

49

7.2 U

7.2 U

7.2 U

7.2 U

7.2 U

50

7.2 U

7.2 U

7.2 U

7.2 U

7.2 U

7.2 U

Modified SPLP

Mercury

ug/L

0.94

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

Modified SPLP

Nickel

ug/L

8.2

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

Modified SPLP

Potassium

ug/L

NE

374,000

373,000

401,000

379,000

397,000

400,000

415,000

381,000

401,000

391,000

388,000

403,000

414,000

399,000

Modified SPLP

Selenium

ug/L

71

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

Modified SPLP

Silver

ug/L

0.95

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

Modified SPLP

Sodium

ug/L

NE

8,840,000

8,790,000

9,200,000 J

8,800,000 J

9,100,000 J

9,200,000 J

9,300,000 J

9,000,000 J

9,200,000 J

9,080,000

9,000,000 J

9,130,000

9,100,000 J

8,800,000 J

Modified SPLP

Thallium

ug/L

17

0.94 UJ

0.94 UJ

0.94 U

0.94 U

0.94 U

0.94 U

0.94 U

0.94 U

0.94 U

0.94 UJ

0.94 U

0.94 UJ

0.94 U

0.94 U

Modified SPLP

Vanadium

ug/L

50

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

2 U

Modified SPLP

Zinc

ug/L

81

63.8 J

61 J

62 J

84.8 J

56 J

66.3 J

56 J

83.8 J

51 J

39 J

79.5 J

41 J

49 J

95 J

Notes:

ug/L = micrograms per liter

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown
FD = field duplicate sample
N = normal sample

a Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of
preference:

a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 2 OF 3


-------
TABLE 4-6

Marine Sediment Core and Test Pit Sample Results - Modified SPLP Metals Analysis

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SB-082

SB-082

SB-082

SB-089

SB-089

SB-089

Area







Site

Site

Site

Site

Site

Site

Activity ID:







20130528

20130528

20130528

0_5-20130528

20130528

20130528

Sample Type:







N

N

N

N

N

N

Date Sampled:







05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

05/28/13

Depth (feet):







0.5 -1

o

o
In

1-2

0.5 -1

o

o
In

1-2



Analyte

Units

Screening Level3



Modified SPLP

Aluminum

ug/L

NE

25 U

25 U

25 U

25 U

25 U

25 U

Modified SPLP

Antimony

ug/L

500

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

8.8 U

Modified SPLP

Arsenic

ug/L

36

2.5 U

2.5 U

2.5 U

2.5 U

2.5 U

2.5 UJ

Modified SPLP

Barium

ug/L

200

160 J

160 J

130 J

130 J

150 J

120 J

Modified SPLP

Beryllium

ug/L

100

2 U

2 U

2 U

2 U

2 U

2 UJ

Modified SPLP

Cadmium

ug/L

8.8

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

Modified SPLP

Calcium

ug/L

NE

319,000

314,000

328,000

330,000

327,000

316,000

Modified SPLP

Chromium

ug/L

27.4

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

6.8 U

Modified SPLP

Cobalt

ug/L

1

8.6 U

8.6 U

2.7

8.6 U

8.6 U

8.6 U

Modified SPLP

Copper

ug/L

3.1

2.1 U

2.1 U

2.1 U

2.1 U

2.1 U

2.1 U

Modified SPLP

Iron

ug/L

50

7.8 U

5,170

7.8 U

7.8 U

7.8 U

7.8 U

Modified SPLP

Lead

ug/L

8.1

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

1.9 U

Modified SPLP

Magnesium

ug/L

NE

1,080,000

1,060,000

1,050,000

1,060,000

1,060,000

1,060,000

Modified SPLP

Manganese

ug/L

100

43

80

36

61

51

89

Modified SPLP

Mercury

ug/L

0.94

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

0.0088 U

Modified SPLP

Nickel

ug/L

8.2

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

1.3 U

Modified SPLP

Potassium

ug/L

NE

416,000

414,000

380,000

381,000

379,000

392,000

Modified SPLP

Selenium

ug/L

71

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

2.3 U

Modified SPLP

Silver

ug/L

0.95

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

1.2 U

Modified SPLP

Sodium

ug/L

NE

9,260,000

9,170,000

8,920,000

8,950,000

8,860,000

9,100,000 J

Modified SPLP

Thallium

ug/L

17

0.94 UJ

0.94 UJ

0.94 UJ

0.94 UJ

0.94 UJ

0.94 U

Modified SPLP

Vanadium

ug/L

50

14

2 U

7.2

2 U

15

2 U

Modified SPLP

Zinc

ug/L

81

83.8 J

66.3 J

52 J

63 J

77.3 J

38 J

Notes:

ug/L = micrograms per liter

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown
FD = field duplicate sample
N = normal sample

a Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of
preference:

a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 3 OF 3


-------
TABLE 4-7

Upland Core and Test Pit Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SB-041

SB-041

SB-041

SB-053

SB-053

SB-053

SB-053

SB-173

SB-173

SB-173

SB-173

Area







Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:







20130525

20130525

20130525FD

20130525

20130525

20130525

20130525FD

20130525

20130525

20130525

20130525FD

Sample Type:







N

N

FD

N

N

N

FD

N

N

N

FD

Date Sampled:







05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

Depth (feet):







0.5 -1

0-0.5

0-0.5

0.5 -1

0-0.5

1 - 2

0-0.5

0.5 -1

0-0.5

1 - 2

1 - 2







Screening























ChemGroup

Analyte

Units

Level8























Metals, Chrome VI

Chromium VI

mg/Kg

0.29



0.14 U

0.14 U



0.031 U













Metals, Hg

Mercury

mg/Kg

10

0.11

0.19

0.13

0.032 J

0.037 J

0.075 J

0.062 J

0.034 J

0.063 J

0.052 J

0.14

TAL Metals

Aluminum

mg/Kg

77,000

7,100

6,460

7,540

7,450

6,610

6,480

6,040

7,410

6,760

7,760

8,440

TAL Metals

Antimony

mg/Kg

31

0.34 U

0.34 U

0.34 U

0.39 U

0.37 U

0.37 U

0.35 U

0.34 U

0.35 U

0.36 U

0.37 U

TAL Metals

Arsenic

mg/Kg

0.39

0.23 U

0.23 U

0.23 U

0.26 U

0.25 U

0.25 U

0.23 U

0.23 U

0.23 U

0.24 U

0.25 U

TAL Metals

Barium

mg/Kg

15,000

2.1 U

2.1 U

2.1 U

2.4 U

2.2 U

2.2 U

2.1 U

2.1 U

2.1 U

2.2 U

2.2 U

TAL Metals

Beryllium

mg/Kg

160

0.26 U

0.26 U

0.26 U

0.3 U

0.28 U

0.28 U

0.27 U

0.26 U

0.27 U

0.28 U

0.29 U

TAL Metals

Cadmium

mg/Kg

70

0.19 U

0.19 U

0.2 U

0.22 U

0.21 U

0.21 U

0.2 U

0.19 U

0.2 U

0.21 U

0.21 U

TAL Metals

Calcium

mg/Kg

NE

2,970

2,810

3,310

3,410

2,860

3,120

2,640

3,070

2,820

3,340

3,620

TAL Metals

Chromium

mg/Kg

0.29

0.61 J

0.36 J

0.43 J

0.79 J

0.36 U

0.36 U

0.34 U

0.46 J

0.61 J

0.86 J

0.93 J

TAL Metals

Cobalt

mg/Kg

23

12

11.3

12.2

13.2

11.5

13.5

12.8

12.7

12.6

12.8

14.5

TAL Metals

Copper

mg/Kg

3,100

918

825

998

912

750 J

875 J

730 J

790

801

582

703

TAL Metals

Iron

mg/Kg

55,000

39,700 J

32,400 J

35,500 J

39,300 J

32,100

42,000

40,200

27,900 J

52,800 J

28,400 J

30,600 J

TAL Metals

Lead

mg/Kg

400

0.22 U

0.22 U

0.22 U

0.25 U

0.23 UJ

0.24 UJ

0.22 UJ

0.22 U

0.22 U

0.23 U

0.24 U

TAL Metals

Magnesium

mg/Kg

NE

8,160

7,950

9,100

8,490

7,610

7,450

7,080

9,180

8,140

9,270

9,680

TAL Metals

Manganese

mg/Kg

1,800

196 J

187 J

208 J

218 J

187 J

211 J

205 J

274 J

202 J

291 J

277 J

TAL Metals

Nickel

mg/Kg

1,500

5.3 J

4.9 J

5.3 J

5.7 J

0.26 U

0.26 U

0.25 U

5.3 J

5.5 J

5.7 J

6.6

TAL Metals

Potassium

mg/Kg

NE

342 J

283 J

335 J

60.2 U

498 J

419 J

360 J

254 J

252 J

270 J

301 J

TAL Metals

Selenium

mg/Kg

390

1.3 U

1.3 U

1.3 U

1.4 U

1.4 U

1.4 U

1.3 U

1.3 U

1.3 U

1.3 U

1.4 U

TAL Metals

Silver

mg/Kg

390

0.16 U

0.16 U

0.16 U

0.18 U

0.17 U

0.17 U

0.16 U

0.16 U

0.16 U

0.17 U

0.17 U

TAL Metals

Sodium

mg/Kg

NE

42.1 J

342 J

413 J

775

1,030

783

900

41.6 J

129 J

43.7 J

55.7 J

TAL Metals

Thallium

mg/Kg

0.78

0.17 U

0.17 U

0.17 U

0.2 U

0.18 U

0.19 U

0.18 U

0.17 U

0.17 U

0.18 U

0.19 U

TAL Metals

Vanadium

mg/Kg

390

47.1

41.4

46.4

54.4

47.6 J

57.9 J

52.3 J

44.7

53.7

44.6

52.6

TAL Metals

Zinc

mg/Kg

23,000

22.8

21.6

23.2

24.4

22

25.7

24.8

23.4

23.7

24.6

28.4

Notes:

mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown
FD = field duplicate sample
N = normal sample

Screening Level = Residential Soil RSLs (EPA, 2013)

NE = not established

BOLD = detected result exceeds the soil screening level

Italics = analyte not detected but method detection limit exceeds the soil screening leve,

PAGE 1 OF 2


-------
TABLE 4-7

Upland Core and Test Pit Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SB-178

SB-179

SB-180

SB-220a

SB-221

Area







Site

Site

Site

Site

Site

Activity ID:







20130530

20130530

20130530

20130530

20130530

Sample Type:







N

N

N

N

N

Date Sampled:







05/30/13

05/30/13

05/30/13

05/30/13

05/30/13

Depth (feet):







0.5 -1

0-0.5

0.5 -1

0-0.5

0-0.5







Screening











ChemGroup

Analyte

Units

Level8











Metals, Chrome VI

Chromium VI

mg/Kg

0.29











Metals, Hg

Mercury

mg/Kg

10

0.097 J

1

0.088 J

0.16

0.066 J

TAL Metals

Aluminum

mg/Kg

77,000

9,660

32,600

5,410

6,490

8,200

TAL Metals

Antimony

mg/Kg

31

0.34 U

0.46 U

0.32 U

0.37 U

0.46 U

TAL Metals

Arsenic

mg/Kg

0.39

0.23 U

0.3 U

0.22 U

0.24 U

0.3 U

TAL Metals

Barium

mg/Kg

15,000

2.1 U

2.7 U

1.9 U

2.2 U

2.7 U

TAL Metals

Beryllium

mg/Kg

160

0.26 U

0.35 U

0.25 U

0.28 U

0.35 U

TAL Metals

Cadmium

mg/Kg

70

0.19 U

0.26 U

0.18 U

0.21 U

0.26 U

TAL Metals

Calcium

mg/Kg

NE

3,920

26,800

2,410

3,060

3,510

TAL Metals

Chromium

mg/Kg

0.29

0.33 U

0.44 U

0.31 U

0.35 U

0.44 U

TAL Metals

Cobalt

mg/Kg

23

16.8 J

42.5 J

12.6 J

12.2 J

17.8 J

TAL Metals

Copper

mg/Kg

3,100

429 J

2,270 J

1,410 J

111 J

84.9 J

TAL Metals

Iron

mg/Kg

55,000

37,500 J

56,500

35,500 J

40,500 J

51,400 J

TAL Metals

Lead

mg/Kg

400

0.22 U

0.29 U

0.21 U

16.5

0.29 U

TAL Metals

Magnesium

mg/Kg

NE

11,400

35,500

6,440

7,120

9,340

TAL Metals

Manganese

mg/Kg

1,800

289 J

824 J

199 J

203 J

304 J

TAL Metals

Nickel

mg/Kg

1,500

11.8

17.4

5.7

7.4

0.32 U

TAL Metals

Potassium

mg/Kg

NE

52.5 U

1,410

49.2 U

56 U

70.6 U

TAL Metals

Selenium

mg/Kg

390

1.3 U

1.7 U

1.2 U

1.3 U

1.7 U

TAL Metals

Silver

mg/Kg

390

0.16 U

0.21 U

0.15 U

0.17 U

0.21 U

TAL Metals

Sodium

mg/Kg

NE

138 J

319 J

42.9 J

102 J

317 J

TAL Metals

Thallium

mg/Kg

0.78

0.17 U

0.23 U

0.16 U

0.18 U

0.23 U

TAL Metals

Vanadium

mg/Kg

390

67.5 J

201 J

54.7 J

55.7 J

87.2 J

TAL Metals

Zinc

mg/Kg

23,000

34.5

83.2

22.1

28.3

32.4

Notes:

mg/Kg = milligrams per kilogram
g = grams

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method detection limit shown
FD = field duplicate sample
N = normal sample

Screening Level = Residential Soil RSLs (EPA, 2013)

NE = not established

BOLD = detected result exceeds the soil screening level

Italics = analyte not detected but method detection limit exceeds the soil screening leve,

PAGE 2 OF 2


-------
TABLE 4-8

Pore Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









PW-002

PW-003

PW-003

PW-006

PW-008

PW-014

PW-016

PW-017

PW-022

PW-027

PW-030

PW-037

PW-042

PW-045

PW-055

PW-055

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:









2013SC-PW-002-

2013SC-PW-003-

2013SC-PW-9003-

2013SC-PW-006-

2013SC-PW-008-

2013SC-PW-014-

2013SC-PW-016-

2013SC-PW-017-

2013SC-PW-022-

2013SC-PW-027-

2013SC-PW-030-

2013SC-PW-037-

2013SC-PW-042-

2013SC-PW-045-

2013SC-PW-055-

2013SC-PW-9055-

Sample Type:









N

N

FD

N

N

N

N

N

N

N

N

N

N

N

N

FD

Date Sampled:









05/28/13

05/28/13

05/28/13

05/28/13

05/27/13

05/27/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

Depth (feet):









0-3

0-3

0-3

0-3

0-3

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2









Screening

































ChemGroup



Analyte

Units

Level3

































Hg_Diss



Mercury

ug/L

0.94

0.034 J

0.044 J

0.034 J

0.034 U

0.041 J

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

TAL Metals_Diss



Aluminum

ug/L

NE

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

42.6 J

26.1 U

78.7 J

34.3 J

26.1 U

29.9 J

26.1 U

45.9 J

31.3 J

TAL Metals_Diss



Antimony

ug/L

500

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

0.085 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TAL Metals_Diss



Arsenic

ug/L

36

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

0.079 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

TAL Metals_Diss



Barium

ug/L

200

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

281 J

5.6 U

425 J

5.6 UJ

221 J

5.6 UJ

5.6 U

5.6 UJ

5.6 UJ

TAL Metals_Diss



Beryllium

ug/L

100

0.51 U

1 U

0.51 U

0.51 U

1 U

0.51 U

1 U

1 U

1 U

0.051 U

1 U

1 U

1 U

1 U

1 U

1 U

TAL Metals_Diss



Cadmium

ug/L

CO
CO

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

0.069 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

TAL Metals_Diss



Calcium

ug/L

NE

212,000

309,000

332,000

252,000

329,000

189,000

127,000

207,000 J

368,000

10,200 J

198,000 J

350,000

185,000 J

402,000

343,000 J

356,000 J

TAL Metals_Diss



Chromium

ug/L

27.4

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

0.11 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

TAL Metals_Diss



Cobalt

ug/L

1

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.038 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

TAL Metals_Diss



Copper

ug/L

3.1

616

256

268

545

145

0.98 U

0.98 U

0.98 UJ

0.98 U

664 J

0.98 UJ

92.1

0.98 UJ

66.2

73.2 J

82.4 J

TAL Metals_Diss



Iron

ug/L

50

25.6 U

25.6 U

25.6 U

25.6 U

25.6 U

952

34,400

25.6 U

25.6 U

85.7 J

824

25.6 U

1,810

25.6 U

25.6 U

25.6 U

TAL Metals_Diss



Lead

ug/L

8.1

0.21 U

0.42 U

0.42 U

0.21 U

0.42 U

0.21 U

0.42 U

0.42 U

0.42 U

0.021 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

TAL Metals_Diss



Magnesium

ug/L

NE

578,000

931,000

992,000

720,000

1.04E+06

519,000

351,000

566,000

1.08E+06

25,100

514,000

1.05E+06

438,000

1.25E+06

920,000

1,070,000

TAL Metals_Diss



Manganese

ug/L

100

156

125

124

33.6

65.7

168

68.1

4 U

4 U

13.9

173

4 U

63

4 U

4 U

4 U

TAL Metals_Diss



Nickel

ug/L

8.2

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.049 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

TAL Metals_Diss



Potassium

ug/L

NE

182,000

283,000

308,000

230,000

305,000

193,000

111,000

188,000

362,000

21,400

189,000

338,000

167,000

393,000

321,000

325,000

TAL Metals_Diss



Selenium

ug/L

71

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

36.3 J

2.6 J

30 U

30 U

30 U

30 U

30 U

30 U

TAL Metals_Diss



Silver

ug/L

0.95

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.033 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

TAL Metals_Diss



Sodium

ug/L

NE

4,860,000

7,910,000

8,550,000

6,180,000

8,820,000

1,190,000

1,330,000

4,640,000

9,290,000

469,000

4,410,000

8,770,000

3,990,000

10,400,000

7,440,000

8,840,000

TAL Metals_Diss



Thallium

ug/L

17

0.36 U

0.72 U

0.72 U

0.36 U

0.72 U

0.36 U

0.72 U

0.72 U

0.72 U

0.036 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

TAL Metals_Diss



Vanadium

ug/L

50

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

0.15 U

3 U

3 U

3 U

3 U

3 U

3 U

TAL Metals_Diss



Zinc

ug/L

81

240

185

190

53

12 U

12 U

96 J

59.3 J

79.9 J

157 J

87.4 J

70.4 J

66.7 J

70 J

65.8 J

66.9 J

TCLPAHs



2-Methylnaphthalene

ug/L

300

0.1 u

0.1 U

0.1 u



0.1 U

0.1 U





















TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Benzo(a)pyrene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Benzo(ghi)perylene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Chrysene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Fluoranthene

ug/L

11

0.05 U

0.05 U

0.05 U



0.05 U

0.13





















TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

HPAH

Pyrene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.18





















TCLPAHs

HPAH

Total HPAH

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.31





















TCLPAHs

LPAH

Acenaphthene

ug/L

40

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Acenaphthylene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Anthracene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Fluorene

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Naphthalene

ug/L

1.4

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Phenanthrene

ug/L

4.6

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

LPAH

Total LPAH

ug/L

300

0.05 U

0.05 U

0.05 U



0.05 U

0.05 U





















TCLPAHs

TPAH

Total PAH

ug/L

15

0.1 U

0.1 U

0.1 U



0.1 U

0.31





















Notes:

ug/L = micrograms per liter
PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method reporting limit shown

Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following
order of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 1 OF 3


-------
TABLE 4-8

Pore Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









PW-056

PW-064

PW-065

PW-066

PW-068

PW-069

PW-071

PW-071

PW-073

PW-074

PW-076

PW-080

PW-081

PW-086

PW-088

PW-091

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:









2013SC-PW-056-

2013SC-PW-064-

2013SC-PW-065-

2013SC-PW-066-

2013SC-PW-068-

2013SC-PW-069-

2013SC-PW-071-

2013SC-PW-9071-

2013SC-PW-073-

2013SC-PW-074-

2013SC-PW-076-

2013SC-PW-080-

2013SC-PW-081-

2013SC-PW-086-

2013SC-PW-088-

2013SC-PW-091-

Sample Type:









N

N

N

N

N

N

N

FD

N

N

N

N

N

N

N

N

Date Sampled:









05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

Depth (feet):









0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2









Screening

































ChemGroup



Analyte

Units

Level3

































Hg_Diss



Mercury

ug/L

0.94

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

TAL Metals_Diss



Aluminum

ug/L

NE

39.1 J

32.1 J

33.2 J

26.1 U

33.4 J

29.9 J

26.1 U

26.1 U

26.1 U

38.5 J

56.9 J

45 J

26.1 U

26.1 U

26.4 J

26.1 U

TAL Metals_Diss



Antimony

ug/L

500

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TAL Metals_Diss



Arsenic

ug/L

36

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

TAL Metals_Diss



Barium

ug/L

200

340 J

5.6 UJ

5.6 UJ

5.6 U

5.6 UJ

5.6 UJ

301 J

5.6 U

206 J

5.6 UJ

350 J

5.6 UJ

5.6 U

5.6 U

201 J

207 J

TAL Metals_Diss



Beryllium

ug/L

100

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

TAL Metals_Diss



Cadmium

ug/L

CO
CO

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

TAL Metals_Diss



Calcium

ug/L

NE

330,000 J

214,000 J

244,000 J

235,000

238,000 J

310,000 J

333,000

331,000

283,000 J

285,000 J

343,000 J

331,000 J

356,000

352,000

288,000 J

342,000

TAL Metals_Diss



Chromium

ug/L

27.4

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

TAL Metals_Diss



Cobalt

ug/L

1

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

TAL Metals_Diss



Copper

ug/L

3.1

159 J

0.98 UJ

0.98 UJ

93.4

239 J

48.2 J

119

99.2

0.98 UJ

144 J

74.7 J

126 J

0.98 U

0.98 U

0.98 UJ

0.98 U

TAL Metals_Diss



Iron

ug/L

50

25.6 U

25.6 U

131

25.6 U

25.6 U

25.6 U

25.6 U

25.6 U

592

25.6 U

25.6 U

25.6 U

692

211

1,940

1,690

TAL Metals_Diss



Lead

ug/L

8.1

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

TAL Metals_Diss



Magnesium

ug/L

NE

922,000

639,000

633,000

605,000

616,000

953,000

911,000

902,000

766,000

910,000

1.11E+06

940,000

1.04E+06

1.05E+06

840,000

961,000

TAL Metals_Diss



Manganese

ug/L

100

209

77.5

27

39

224

4 U

4 U

4 U

74.1

4 U

4 U

4 U

98.9

90.5

126

120

TAL Metals_Diss



Nickel

ug/L

8.2

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

TAL Metals_Diss



Potassium

ug/L

NE

303,000

214,000

233,000

214,000

215,000

297,000

291,000

287,000

260,000

285,000

346,000

310,000

315,000

314,000

270,000

301,000

TAL Metals_Diss



Selenium

ug/L

71

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

TAL Metals_Diss



Silver

ug/L

0.95

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

TAL Metals_Diss



Sodium

ug/L

NE

7,460,000

5,310,000

5,490,000

5,110,000

5,200,000

7,520,000

7,330,000

7,210,000

6,380,000

7,390,000

8,890,000

7,590,000

8,260,000

8,280,000

6,780,000

7,670,000

TAL Metals_Diss



Thallium

ug/L

17

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

TAL Metals_Diss



Vanadium

ug/L

50

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

TAL Metals_Diss



Zinc

ug/L

81

95.8 J

67.3 J

57.1 J

12 U

12 U

63.1 J

117 J

12 U

66.3 J

45.2 J

123 J

57.2 J

12 U

71 J

69.3 J

79.8 J

TCLPAHs



2-Methylnaphthalene

ug/L

300

































TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300

































TCLPAHs

HPAH

Benzo(a)pyrene

ug/L

300

































TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/L

300

































TCLPAHs

HPAH

Benzo(ghi)perylene

ug/L

300

































TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/L

300

































TCLPAHs

HPAH

Chrysene

ug/L

300

































TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300

































TCLPAHs

HPAH

Fluoranthene

ug/L

11

































TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300

































TCLPAHs

HPAH

Pyrene

ug/L

300

































TCLPAHs

HPAH

Total HPAH

ug/L

300

































TCLPAHs

LPAH

Acenaphthene

ug/L

40

































TCLPAHs

LPAH

Acenaphthylene

ug/L

300

































TCLPAHs

LPAH

Anthracene

ug/L

300

































TCLPAHs

LPAH

Fluorene

ug/L

300

































TCLPAHs

LPAH

Naphthalene

ug/L

1.4

































TCLPAHs

LPAH

Phenanthrene

ug/L

4.6

































TCLPAHs

LPAH

Total LPAH

ug/L

300

































TCLPAHs

TPAH

Total PAH

ug/L

15































Notes:

ug/L = micrograms per liter
PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method reporting limit shown

Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following
order of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 2 OF 3


-------
TABLE 4-8

Pore Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









PW-091

PW-092

PW-094

PW-096

PW-097

PW-100

PW-101

PW-102

PW-103

PW-169

PW-170

PW-171

PW-174

PW-175

PW-511

PW-512

PW-513

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Background

Background

Background

Activity ID:









2013SC-PW-9091-

2013SC-PW-092-

2013SC-PW-094-

2013SC-PW-096-

2013SC-PW-097-

2013SC-PW-100-

2013SC-PW-101-

2013SC-PW-102-

2013SC-PW-103-

2013SC-PW-169-

2013SC-PW-170-

2013SC-PW-171-

2013SC-PW-174-

2013SC-PW-175-

2013SC-PW-511-

2013SC-PW-512-

2013SC-PW-513-

Sample Type:









FD

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

N

Date Sampled:









05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/27/13

05/27/13

05/29/13

05/29/13

05/29/13

Depth (feet):









0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-2

0-3

0-3

0-2

0-2

0-2









Screening



































ChemGroup



Analyte

Units

Level3



































Hg_Diss



Mercury

ug/L

0.94

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.034 U

0.047 J

0.035 J

0.034 U

0.034 U

0.034 U

TAL Metals_Diss



Aluminum

ug/L

NE

26.1 U

31.4 J

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

39.7 J

35.8 J

40.1 J

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

TAL Metals_Diss



Antimony

ug/L

500

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TAL Metals_Diss



Arsenic

ug/L

36

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

TAL Metals_Diss



Barium

ug/L

200

5.6 U

222 J

205 J

217 J

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 UJ

220 J

5.6 UJ

5.6 U

5.6 U

5.6 U

5.6 U

234 J

TAL Metals_Diss



Beryllium

ug/L

100

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

0.51 U

1 U

1 U

1 U

TAL Metals_Diss



Cadmium

ug/L

CO
CO

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

1.4 U

TAL Metals_Diss



Calcium

ug/L

NE

359,000

318,000 J

402,000

277,000

359,000

332,000

342,000

371,000

327,000

255,000 J

330,000 J

229,000 J

123,000

333,000

413,000

368,000

365,000

TAL Metals_Diss



Chromium

ug/L

27.4

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

2.2 U

TAL Metals_Diss



Cobalt

ug/L

1

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

0.76 U

TAL Metals_Diss



Copper

ug/L

3.1

0.98 U

0.98 UJ

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 UJ

0.98 UJ

659 J

318

83.8

0.98 U

0.98 U

0.98 U

TAL Metals_Diss



Iron

ug/L

50

1,890

25.6 U

1,180

25.6 U

121

998

689

355

883

2,330

316

25.6 U

1,530

25.6 U

25.6 U

841

25.6 U

TAL Metals_Diss



Lead

ug/L

8.1

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

0.42 U

TAL Metals_Diss



Magnesium

ug/L

NE

1.02E+06

833,000

1.11E+06

747,000

984,000

910,000

935,000

1.02E+06

868,000

700,000

848,000

708,000

333,000

979,000

1,230,000

1,060,000

1,100,000

TAL Metals_Diss



Manganese

ug/L

100

116

82.3

56.2

236

76.6

90.7

117

76.3

83.5

352

590

4 U

94.5

26.7

213

39.1

4 U

TAL Metals_Diss



Nickel

ug/L

8.2

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

0.98 U

TAL Metals_Diss



Potassium

ug/L

NE

312,000

287,000

351,000

253,000

317,000

290,000

290,000

327,000

288,000

220,000

261,000

220,000

106,000

324,000

393,000

347,000

334,000

TAL Metals_Diss



Selenium

ug/L

71

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

30 U

49.3 J

30 U

30 U

30 U

30 U

30 U

30 U

TAL Metals_Diss



Silver

ug/L

0.95

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

0.66 U

TAL Metals_Diss



Sodium

ug/L

NE

8,080,000

6,890,000

8,630,000

6,160,000

7,820,000

7,430,000

7,470,000

8,110,000

7,020,000

5,770,000

6,760,000

5,640,000

2,960,000

8,190,000

10,700,000

8,940,000

9,260,000

TAL Metals_Diss



Thallium

ug/L

17

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

0.72 U

TAL Metals_Diss



Vanadium

ug/L

50

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

3 U

TAL Metals_Diss



Zinc

ug/L

81

12 U

71.3 J

81.2 J

59 J

12 U

12 U

12 U

70.6 J

12 U

74.7 J

81.8 J

101 J

143

12 U

81.2

70.8

42.3

TCLPAHs



2-Methylnaphthalene

ug/L

300

























0.1 U

0.1 U







TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Benzo(a)pyrene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Benzo(b)fluoranthene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Benzo(ghi)perylene

ug/L

300

























0.05 U

0.13







TCLPAHs

HPAH

Benzo(k)fluoranthene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Chrysene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Fluoranthene

ug/L

11

























0.05 U

0.05 U







TCLPAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Pyrene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

HPAH

Total HPAH

ug/L

300

























0.05 U

0.13







TCLPAHs

LPAH

Acenaphthene

ug/L

40

























0.05 U

0.05 U







TCLPAHs

LPAH

Acenaphthylene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

LPAH

Anthracene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

LPAH

Fluorene

ug/L

300

























0.05 U

0.05 U







TCLPAHs

LPAH

Naphthalene

ug/L

1.4

























0.05 U

0.05 U







TCLPAHs

LPAH

Phenanthrene

ug/L

4.6

























0.05 U

0.05 U







TCLPAHs

LPAH

Total LPAH

ug/L

300

























0.05 U

0.05 U







TCLPAHs

TPAH

Total PAH

ug/L

15

























0.1 U

0.13







Notes:

ug/L = micrograms per liter
PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimatior
U = The analyte was analyzed for, but not detected at the method reporting limit shown

Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following
order of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administratior
SQuiRT = Screening Quick Reference Table:

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 3 OF 3


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









SW-015

SW-029

SW-075

SW-084

SW-084

SW-085

SW-098

SW-099

SW-104

SW-105

SW-106

SW-106

SW-108

SW-108

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Activity ID:









2013SC-SW-015-

2013SC-SW-029-

2013SC-SW-075-

2013SC-SW-084-

2013SC-SW-9084-

2013SC-SW-085-

2013SC-SW-098-

2013SC-SW-099-

2013SC-SW-104-

2013SC-SW-105-

2013SC-SW-106-

2013SC-SW-9106-

2013CS-SW-108-

2013CS-SW-108-

Sample Type:









N

N

N

N

FD

N

N

N

N

N

N

FD

N

N

Date Sampled:









05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/25/13

05/26/13

05/26/13









Screening





























ChemGroup



Analyte

Units

Level8





























Hg Dissolved



Mercury

ug/L

0.94

0.05 J

0.054 J

0.049 J

0.042 J

0.042 J

0.035 J

0.038 J

0.052 J

0.034 J

0.034 U

0.038 J

0.04 J

0.034 U

0.037 J

TAL Metals_Diss



Aluminum

ug/L

NE

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

TAL Metals_Diss



Antimony

ug/L

500

0.85 U

1.7 U

1.7 U

1.7 U

1.7 U

0.85 U

0.85 U

1.7 U

0.85 U

1.7 U

0.85 U

0.85 U

1.7 U

1.7 U

TAL Metals_Diss



Arsenic

ug/L

36

0.79 U

1.6 U

1.6 U

1.6 U

1.6 U

0.79 U

0.79 U

1.6 U

11.2

36.2

0.79 U

0.79 U

1.6 U

1.6 U

TAL Metals_Diss



Barium

ug/L

200

2.8 U

5.6 U

5.6 U

5.6 U

5.6 U

2.8 U

2.8 U

5.6 U

2.8 U

5.6 U

2.8 U

2.8 U

5.6 U

5.6 U

TAL Metals_Diss



Beryllium

ug/L

100

0.51 U

1 U

1 U

1 U

1 U

0.51 U

0.51 U

1 U

0.51 U

1 U

0.51 U

0.51 U

1 U

1 U

TAL Metals_Diss



Cadmium

ug/L

CO
CO

0.004 U

0.054

0.06

0.03

0.032 J

0.03 J

0.036

0.052

0.039

0.059

0.024 J

0.017 J

0.07

0.068

TAL Metals_Diss



Calcium

ug/L

NE

11,800

270,000

287,000

54,100

57,700

94,900

139,000

257,000

177,000

254,000

96,700

98,100

337,000

348,000

TAL Metals_Diss



Chromium

ug/L

27.4

0.18 U

0.19 J

0.19 J

0.21 J

0.21 J

0.16 J

0.17 J

0.18 U

0.16 J

0.19 J

0.22 J

0.13 U

0.17 J

0.18 J

TAL Metals_Diss



Cobalt

ug/L

1

0.032 J

0.074

0.092

0.138

0.144

0.362

0.186

0.092

0.044

0.038

0.121

0.029

0.028 J

0.033 J

TAL Metals_Diss



Copper

ug/L

3.1

1.54

22.5

14.9

22.2

20.9

10.S

9.98

6.57

1.95

1.62

1.81

1.41

0.739

1.03

TAL Metals_Diss



Iron

ug/L

50

311

21

20.3

246

202

93.S

58.5

44.2

45.6

16.1 J

52.5

109

3 U

3.9 J

TAL Metals_Diss



Lead

ug/L

8.1

0.009 J

0.019 J

0.011 J

0.065

0.043

0.008 J

0.009 J

0.008 U

0.007 J

0.014 J

0.008 U

0.006 J

0.006 J

0.007 J

TAL Metals_Diss



Magnesium

ug/L

NE

19,800

778,000

845,000

138,000

148,000

257,000

390,000

752,000

440,000

888,000 J

275,000

275,000

1.06E+06

1.11E+06

TAL Metals_Diss



Manganese

ug/L

100

33.7

20.6

18.9 J

36.9

34.9

80.8

62

34.5

8.9 J

4.5 J

6.3 J

6.1 J

4 U

4 U

TAL Metals_Diss



Nickel

ug/L

8.2

0.717

0.462

0.521

0.258 J

0.281 J

0.447

0.425

0.286 J

0.284 J

0.302

0.308 J

0.344

0.471

0.308 J

TAL Metals_Diss



Potassium

ug/L

NE

7,200

278,000

296,000

46,000

49,300

94,300

148,000

260,000

171,000

253,000

94,500

93,200

324,000

335,000

TAL Metals_Diss



Selenium

ug/L

71

0.2 U

0.2 U

0.2 U

0.34 J

0.22 J

0.2 U

0.2 U

0.2 U

0.2 U

0.21 J

0.2 U

0.2 U

0.2 U

0.2 U

TAL Metals_Diss



Silver

ug/L

0.95

0.002 U

0.002 UJ

0.002 UJ

0.001 UJ

0.002 UJ

0.002 U

0.002 U

0.037 J

0.027 J

0.001 UJ

0.002 UJ

0.028 J

0.001 U

0.031 J

TAL Metals_Diss



Sodium

ug/L

NE

177,000

6,770,000

7,440,000

1,210,000

1,270,000

2,450,000

3,440,000

6,520,000

4,000,000

7,520,000

2,350,000

2,480,000

8,810,000

9,170,000

TAL Metals_Diss



Thallium

ug/L

17

0.002 U

0.007 J

0.007 J

0.019 J

0.007 J

0.003 J

0.004 J

0.004 J

0.006 J

0.01 J

0.007 J

0.019 J

0.014 J

0.012 J

TAL Metals_Diss



Vanadium

ug/L

50

1 J

3.5 J

2.9 J

1.5 J

1.2 J

1.4 J

2.2 J

3.2 J

2.6 J

2.6 J

1.5 J

1.9 J

2.8 J

3 J

TAL Metals Diss



Zinc

ug/L

81

6 U

12 U

12 U

12 U

12 U

6 U

6 U

12 U

6 U

12 U

6 U

6 U

12 U

12 U

Hg



Mercury

ug/L

0.94

















0.034 U

0.056 J

0.034 U

0.034 U





TAL Metals



Aluminum

ug/L

NE

















26.1 U

26.1 U

26.1 U

26.1 U





TAL Metals



Antimony

ug/L

500

















1.7 U

1.7 U

1.7 U

1.7 U





TAL Metals



Arsenic

ug/L

36

















27.7

35.2

1.6 U

1.6 U





TAL Metals



Barium

ug/L

200

















5.6 U

5.6 U

5.6 U

5.6 U





TAL Metals



Beryllium

ug/L

100

















1 U

1 U

1 U

1 U





TAL Metals



Cadmium

ug/L

CO
CO

















0.052

0.055

0.026 J

0.023 J





TAL Metals



Calcium

ug/L

NE

















192,000

239,000

95,700

90,900





TAL Metals



Chromium

ug/L

27.4

















0.3

0.2 J

0.19 J

0.2 J





TAL Metals



Cobalt

ug/L

1

















0.127

0.05

0.049

0.049





TAL Metals



Copper

ug/L

3.1

















4.89

1.73

1.58

1.73





TAL Metals



Iron

ug/L

50

















403

44.5

114

120





TAL Metals



Lead

ug/L

8.1

















0.058

0.007 J

0.008 J

0.01 J





TAL Metals



Magnesium

ug/L

NE

















660,000

869,000

303,000

291,000





TAL Metals



Manganese

ug/L

100

















13.4 J

4.5 J

6.3 J

6.5 J





TAL Metals



Nickel

ug/L

8.2

















0.312

0.308

0.151 J

0.143 J





TAL Metals



Potassium

ug/L

NE

















187,000

238,000

89,700

84,900





TAL Metals



Selenium

ug/L

71

















0.2 U

0.2 U

0.2 U

0.22 J





TAL Metals



Silver

ug/L

0.95

















0.001 U

0.001 UJ

0.002 UJ

0.001 UJ





TAL Metals



Sodium

ug/L

NE

















5.68E+06

6.87E+06

2.63E+06

2.47E+06





TAL Metals



Thallium

ug/L

17

















0.006 J

0.008 J

0.005 J

0.007 J





TAL Metals



Vanadium

ug/L

50

















3.5 J

2.7 J

1.9 J

1.3 J





TAL Metals



Zinc

ug/L

81

















12 U

12 U

12 U

12 U





TCLPAHs



2-Methyl naphthalene

ug/L

300

0.1 U

0.1 U

0.1 U

0.1 U

0.1 U





0.1 U













TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Benzo(a)pyrene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Benzo(ghi)perylene

ug/L

300

0.11

0.05 U

0.18

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Chrysene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Pyrene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

HPAH

Total HPAH

ug/L

300

0.11

0.05 U

0.18

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Acenaphthene

ug/L

40

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Acenaphthylene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Anthracene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Fluoranthene

ug/L

11

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Fluorene

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Naphthalene

ug/L

1.4

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Phenanthrene

ug/L

4.6

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

LPAH

Total LPAH

ug/L

300

0.05 U

0.05 U

0.05 U

0.05 U

0.05 U





0.05 U













TCL PAHs

TPAH

Total PAH

ug/L

300

0.11

0.1 U

0.18

0.1 U

0.1 U





0.1 U













Notes:

ug/L = micrograms per liter

PAGE 1 OF 6


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:

Area

Activity ID:
Sample Type:
Date Sampled:

SW-015
Site

2013SC-SW-015-
N

05/25/13

SW-029
Site

2013SC-SW-029-
N

05/25/13

SW-075
Site

2013SC-SW-075-
N

05/25/13

SW-084
Site

2013SC-SW-084-
N

05/25/13

SW-084
Site

2013SC-SW-9084-
FD

05/25/13

SW-085
Site

2013SC-SW-085-
N

05/25/13

SW-098
Site

2013SC-SW-098-
N

05/25/13

SW-099
Site

2013SC-SW-099-
N

05/25/13

SW-104
Site

2013SC-SW-104-
N

05/25/13

SW-105
Site

2013SC-SW-105-
N

05/25/13

SW-106
Site

2013SC-SW-106-
N

05/25/13

SW-106
Site

2013SC-SW-9106-
FD

05/25/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

ChemGroup



Analyte

Units

Screening
Level8







PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimation
U = The analyte was analyzed for, but not detected at the method detection limit showr

aScreening Level = AWQC listed in NOAASQuiRT (Buchman, 2008) selected in the following order
of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening lev>

** SPLP water results are not include in Table 3-6

PAGE 2 OF 6


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









SW-108

SW-108

SW-108

SW-108

SW-108

SW-108

SW-108

SW-108

SW-108

SW-113

SW-501

SW-503

SW-505

SW-507

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Background

Background

Background

Background

Activity ID:









2013CS-SW-108-

2013CS-SW-108-

2013CS-SW-108-

2013CS-SW-108-

2013CS-SW-108-

2013CS-SW-108-

2013SC-SW-108-

2013SC-SW-108-

2013SC-SW-9108-

2013SC-SW-113-

2013SC-SW-501-

2013SC-SW-503-

2013SC-SW-505-

2013SC-SW-507-

Sample Type:









N

N

N

N

N

N

N

N

FD

N

N

N

N

N

Date Sampled:









05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/26/13

05/25/13

05/26/13

05/25/13

05/28/13

05/28/13

05/28/13

05/28/13









Screening





























ChemGroup



Analyte

Units

Level8





























Hg Dissolved



Mercury

ug/L

0.94

0.041 J

0.042 J

0.04 J

0.041 J

0.043 J

0.047 J

0.042 J

0.046 J

0.036 J

0.038 J

0.034 U

0.093 J

0.082 J

0.034 U

TAL Metals_Diss



Aluminum

ug/L

NE

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

27.3 J

35.3 J

28.9 J

26.1 U

TAL Metals_Diss



Antimony

ug/L

500

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

1.7 U

TAL Metals_Diss



Arsenic

ug/L

36

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

1.6 U

TAL Metals_Diss



Barium

ug/L

200

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

5.6 U

TAL Metals_Diss



Beryllium

ug/L

100

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

1 U

0.51 U

1 U

1 U

1 U

1 U

TAL Metals_Diss



Cadmium

ug/L

CO
CO

0.064

0.056

0.04

0.028 J

0.024 J

0.018 J

0.073

0.064

0.062

0.073

0.086

0.069

0.067

0.067

TAL Metals_Diss



Calcium

ug/L

NE

334,000

309,000

249,000

196,000

160,000

127,000

334,000

290,000

310,000

311,000

370,000

384,000

374,000

367,000

TAL Metals_Diss



Chromium

ug/L

27.4

0.17 J

0.17 J

0.15 J

0.19 J

0.16 J

0.14 J

0.2 J

0.16 J

0.17 J

0.17 J

0.21 J

0.22 J

0.21 J

0.22 J

TAL Metals_Diss



Cobalt

ug/L

1

0.046

0.041

0.039

0.037

0.029

0.028

0.055

0.042

0.042

0.055

0.055

0.042

0.033

0.03

TAL Metals_Diss



Copper

ug/L

3.1

1.34

1.68

2.08

2.51

2.75

2.96

1.53

2.42

1.39

2.52

0.343

0.287

0.366

0.311

TAL Metals_Diss



Iron

ug/L

50

9.2 J

13.3 J

19.5 J

27.1

25.8

27.2

9.5 J

13.8 J

8.8 J

12.6 J

5.7 J

3 U

3 U

3 U

TAL Metals_Diss



Lead

ug/L

8.1

0.005 U

0.005 U

0.006 U

0.006 U

0.009 J

0.005 U

0.008 J

0.006 J

0.005 U

0.007 U

0.026 J

0.019 J

0.02 J

0.019 J

TAL Metals_Diss



Magnesium

ug/L

NE

1.06E+06

975,000

782,000

582,000

475,000

368,000

1,070,000

635,000

923,000

965,000

1,100,000

1,240,000

1,170,000

1,100,000

TAL Metals_Diss



Manganese

ug/L

100

4.8 J

4.8 J

4 J

4 U

4 U

4 U

6.9 J

6.2 J

5.3 J

9.6 J

4 U

4 U

4 U

4 U

TAL Metals_Diss



Nickel

ug/L

8.2

0.241 J

0.262

0.186 J

0.146 J

0.257 J

0.158 J

0.39

0.344

0.238 J

0.322 J

0.26 J

0.274 J

0.302

0.295

TAL Metals_Diss



Potassium

ug/L

NE

326,000

297,000

242,000

189,000

157,000

123,000

334,000

282,000

296,000

307,000

341,000

349,000

339,000

331,000

TAL Metals_Diss



Selenium

ug/L

71

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

0.2 U

TAL Metals_Diss



Silver

ug/L

0.95

0.023 J

0.024 J

0.025 J

0.001 UJ

0.001 UJ

0.001 UJ

0.001 U

0.026 J

0.024 J

0.031 J

0.002 UJ

0.001 UJ

0.001 UJ

0.001 UJ

TAL Metals_Diss



Sodium

ug/L

NE

8,730,000

8,090,000

6,590,000

4,980,000

4,040,000

3,010,000

8,840,000

5,280,000

7,730,000

8,330,000

8,680,000

9,690,000

9,220,000

8,670,000

TAL Metals_Diss



Thallium

ug/L

17

0.009 J

0.009 J

0.008 J

0.007 J

0.006 J

0.005 J

0.01 J

0.008 J

0.009 J

0.008 J

0.01 J

0.009 J

0.009 J

0.009 J

TAL Metals_Diss



Vanadium

ug/L

50

3.6 J

2.8 J

2.7 J

2.8 J

2.7 J

3.2 J

3.2 J

2.3 J

3.3 J

2.6 J

3.7 J

2.6 J

3.4 J

3.4 J

TAL Metals Diss



Zinc

ug/L

81

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

12 U

Hg



Mercury

ug/L

0.94





























TAL Metals



Aluminum

ug/L

NE





























TAL Metals



Antimony

ug/L

500





























TAL Metals



Arsenic

ug/L

36





























TAL Metals



Barium

ug/L

200





























TAL Metals



Beryllium

ug/L

100





























TAL Metals



Cadmium

ug/L

CO
CO





























TAL Metals



Calcium

ug/L

NE





























TAL Metals



Chromium

ug/L

27.4





























TAL Metals



Cobalt

ug/L

1





























TAL Metals



Copper

ug/L

3.1





























TAL Metals



Iron

ug/L

50





























TAL Metals



Lead

ug/L

8.1





























TAL Metals



Magnesium

ug/L

NE





























TAL Metals



Manganese

ug/L

100





























TAL Metals



Nickel

ug/L

8.2





























TAL Metals



Potassium

ug/L

NE





























TAL Metals



Selenium

ug/L

71





























TAL Metals



Silver

ug/L

0.95





























TAL Metals



Sodium

ug/L

NE





























TAL Metals



Thallium

ug/L

17





























TAL Metals



Vanadium

ug/L

50





























TAL Metals



Zinc

ug/L

81





























TCLPAHs



2-Methyl naphthalene

ug/L

300





























TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300





























TCL PAHs

HPAH

Benzo(a)pyrene

ug/L

300





























TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/L

300





























TCL PAHs

HPAH

Benzo(ghi)perylene

ug/L

300





























TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/L

300





























TCL PAHs

HPAH

Chrysene

ug/L

300





























TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300





























TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300





























TCL PAHs

HPAH

Pyrene

ug/L

300





























TCL PAHs

HPAH

Total HPAH

ug/L

300





























TCL PAHs

LPAH

Acenaphthene

ug/L

40





























TCL PAHs

LPAH

Acenaphthylene

ug/L

300





























TCL PAHs

LPAH

Anthracene

ug/L

300





























TCL PAHs

LPAH

Fluoranthene

ug/L

11





























TCL PAHs

LPAH

Fluorene

ug/L

300





























TCL PAHs

LPAH

Naphthalene

ug/L

1.4





























TCL PAHs

LPAH

Phenanthrene

ug/L

4.6





























TCL PAHs

LPAH

Total LPAH

ug/L

300





























TCL PAHs

TPAH

Total PAH

ug/L

300





























Notes:

ug/L = micrograms per liter

PAGE 3 OF 6


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:

Area

Activity ID:
Sample Type:
Date Sampled:

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013CS-SW-108-
N

05/26/13

SW-108
Site

2013SC-SW-108-
N

05/26/13

SW-108
Site

2013SC-SW-108-
N

05/25/13

SW-108
Site

2013SC-SW-9108-
FD

05/26/13

SW-113
Site

2013SC-SW-113-
N

05/25/13

SW-501

Background
2013SC-SW-501-
N

05/28/13

SW-503

Background
2013SC-SW-503-
N

05/28/13

SW-505

Background
2013SC-SW-505-
N

05/28/13

SW-507

Background
2013SC-SW-507-
N

05/28/13

ChemGroup



Analyte

Units

Screening
Level8



PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimation
U = The analyte was analyzed for, but not detected at the method detection limit showr

aScreening Level = AWQC listed in NOAASQuiRT (Buchman, 2008) selected in the following order
of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening lev>

** SPLP water results are not include in Table 3-6

PAGE 4 OF 6


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









SW-509

SW-509

SW-600**

Area









Background

Background

Modified SPLP water

Activity ID:









2013SC-SW-509-

2013SC-SW-9509-

2013SC-SW-600

Sample Type:









N

FD

N

Date Sampled:









05/28/13

05/28/13

05/29/13









Screening







ChemGroup



Analyte

Units

Level8







Hg Dissolved



Mercury

ug/L

0.94

0.034 U

0.036 J



TAL Metals_Diss



Aluminum

ug/L

NE

36.9 J

26.1 U



TAL Metals_Diss



Antimony

ug/L

500

1.7 U

1.7 U



TAL Metals_Diss



Arsenic

ug/L

36

1.6 U

4S.5



TAL Metals_Diss



Barium

ug/L

200

5.6 U

6.2 J



TAL Metals_Diss



Beryllium

ug/L

100

1 U

1 U



TAL Metals_Diss



Cadmium

ug/L

CO
CO

0.063

0.074



TAL Metals_Diss



Calcium

ug/L

NE

385,000

349,000



TAL Metals_Diss



Chromium

ug/L

27.4

0.2 J

0.21 J



TAL Metals_Diss



Cobalt

ug/L

1

0.037

0.029 J



TAL Metals_Diss



Copper

ug/L

3.1

0.412

0.334



TAL Metals_Diss



Iron

ug/L

50

3 U

5.1 J



TAL Metals_Diss



Lead

ug/L

8.1

0.043

0.059



TAL Metals_Diss



Magnesium

ug/L

NE

1,160,000

1,300,000 J



TAL Metals_Diss



Manganese

ug/L

100

4 U

4 U



TAL Metals_Diss



Nickel

ug/L

8.2

0.315 J

0.283 J



TAL Metals_Diss



Potassium

ug/L

NE

348,000

357,000



TAL Metals_Diss



Selenium

ug/L

71

0.2 U

0.2 U



TAL Metals_Diss



Silver

ug/L

0.95

0.031 J

0.038 J



TAL Metals_Diss



Sodium

ug/L

NE

9,140,000

10,800,000



TAL Metals_Diss



Thallium

ug/L

17

0.009 J

0.01 J



TAL Metals_Diss



Vanadium

ug/L

50

2.1 J

3.5 J



TAL Metals Diss



Zinc

ug/L

81

12 U

12 U



Hg



Mercury

ug/L

0.94





0.0811 J

TAL Metals



Aluminum

ug/L

NE





25 U

TAL Metals



Antimony

ug/L

500





8.8 U

TAL Metals



Arsenic

ug/L

36





2.5 U

TAL Metals



Barium

ug/L

200





5.2 U

TAL Metals



Beryllium

ug/L

100





2 U

TAL Metals



Cadmium

ug/L

CO
CO





1.4 U

TAL Metals



Calcium

ug/L

NE





351000

TAL Metals



Chromium

ug/L

27.4





6.8 U

TAL Metals



Cobalt

ug/L

1





8.6 U

TAL Metals



Copper

ug/L

3.1





2.1 U

TAL Metals



Iron

ug/L

50





65

TAL Metals



Lead

ug/L

8.1





1.9 U

TAL Metals



Magnesium

ug/L

NE





1110000

TAL Metals



Manganese

ug/L

100





7.2 U

TAL Metals



Nickel

ug/L

8.2





1.3 U

TAL Metals



Potassium

ug/L

NE





380000

TAL Metals



Selenium

ug/L

71





2.3 U

TAL Metals



Silver

ug/L

0.95





1.2 U

TAL Metals



Sodium

ug/L

NE





8910000

TAL Metals



Thallium

ug/L

17





0.94 U

TAL Metals



Vanadium

ug/L

50





2 U

TAL Metals



Zinc

ug/L

81





1.7 U

TCLPAHs



2-Methyl naphthalene

ug/L

300







TCLPAHs

HPAH

Benz(a)anthracene

ug/L

300







TCL PAHs

HPAH

Benzo(a)pyrene

ug/L

300







TCL PAHs

HPAH

Benzo(b)fluoranthene

ug/L

300







TCL PAHs

HPAH

Benzo(ghi)perylene

ug/L

300







TCL PAHs

HPAH

Benzo(k)fluoranthene

ug/L

300







TCL PAHs

HPAH

Chrysene

ug/L

300







TCL PAHs

HPAH

Dibenz(a,h)anthracene

ug/L

300







TCL PAHs

HPAH

lndeno(l,2,3-cd)pyrene

ug/L

300







TCL PAHs

HPAH

Pyrene

ug/L

300







TCL PAHs

HPAH

Total HPAH

ug/L

300







TCL PAHs

LPAH

Acenaphthene

ug/L

40







TCL PAHs

LPAH

Acenaphthylene

ug/L

300







TCL PAHs

LPAH

Anthracene

ug/L

300







TCL PAHs

LPAH

Fluoranthene

ug/L

11







TCL PAHs

LPAH

Fluorene

ug/L

300







TCL PAHs

LPAH

Naphthalene

ug/L

1.4







TCL PAHs

LPAH

Phenanthrene

ug/L

4.6







TCL PAHs

LPAH

Total LPAH

ug/L

300







TCL PAHs

TPAH

Total PAH

ug/L

300







Notes:

ug/L = micrograms per liter

PAGE 5 OF 6


-------
TABLE 4-9

Surface Water Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:







SW-509

SW-509

SW-600**

Area

Activity ID:
Sample Type:
Date Sampled:







Background
2013SC-SW-509-
N

05/28/13

Background
2013SC-SW-9509-
FD

05/28/13

Modified SPLP water

2013SC-SW-600
N

05/29/13

ChemGroup



Analyte

Units

Screening
Level8





PAH = polycyclic aromatic hydrocarbon
HPAH = high molecular weight PAI-
LPAH = low molecular weight PAI-

J = The analyte was positively identified; the quantitation is an estimation
U = The analyte was analyzed for, but not detected at the method detection limit showr

aScreening Level = AWQC listed in NOAASQuiRT (Buchman, 2008) selected in the following order
of preference:
a = Marine chronic
b = Marine acute

NE = not established

NOAA = National Oceanic and Atmospheric Administration
SQuiRT = Screening Quick Reference Tables

BOLD = detected result exceeds the screening level

Italics = analyte not detected but method detection limit exceeds the screening lev>

** SPLP water results are not include in Table 3-6

PAGE 6 OF 6


-------
TABLE 4-10

Crab Tissue Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Report

Location:









BIOTA-107

BIOTA-130

BIOTA-138

BIOTA-142

BIOTA-148

BIOTA-148

BIOTA-149

BIOTA-150

BIOTA-151

BIOTA-152

BIOTA-153

BIOTA-500

BIOTA-502

BIOTA-504

BIOTA-506

BIOTA-508

Area









Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Site

Background

Background

Background

Background

Background

Activity ID:









2013SC-Biota-107-CR

2013SC-Biota-130-CR

2013SC-Biota-138-CR

2013SC-Biota-142-CR

2013SC-Biota-148-CR

2013SC-Biota-9148-

2013SC-Biota-149-CR

2013SC-Biota-150-CR

2013SC-Biota-151-CR

2013SC-Biota-152-CR

2013SC-Biota-153-CR

2013SC-Biota-500-CR

2013SC-Biota-502-CR

2013SC-Biota-504-CR

2013SC-Biota-506-CR

2013SC-Biota-508-CR-

Sample Type:









N

N

N

N

N

FD

N

N

N

N

N

N

N

N

N

N

Date Sampled:









05/25/13

05/24/13

05/22/13

05/23/13

05/27/13

05/27/13

05/28/13

05/27/13

05/28/13

05/28/13

05/27/13

05/29/13

05/29/13

05/29/13

05/29/13

05/28/13









Screening

































ChemGroup

Analyte

Units

Level3

































Arsenic Speciat

on

Inorganic Arsenic (As+3 & As+5)

ng/g dw

NE

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

Arsenic Speciat

on

ASB + Cation

ng/g dw

NE

20,100 J

25,200 J

23,300 J

17,900 J

20,500 J

17,800 J

19,300 J

15,900 J

22,300 J

35,800 J

18,200 J

27,700 J

35,700 J

33,400 J

21,500 J

18,200 J

Arsenic Speciat

on

Dimethylarsinic Acid

ng/g dw

NE

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

Arsenic Speciat

on

Monomethylarsonic Acid

ng/g dw

NE

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

120 U

Arsenic Speciat

on

Unknown Arsenic Species

ng/g dw

NE

1,010 J

1,120 J

840 J

1,270 J

911 J

945 J

1,140 J

994 J

1,250 J

1,160 J

1,380 J

1,290 J

932 J

1,010 J

1,060 J

1,150 J

Arsenic Speciat

on

Total Arsenic

ng/g dw

NE

21,110

26,320

24,140

19,170

21,411

18,745

20,440

16,894

23,550

36,960

19,580

28,990

36,632

34,410

22,560

19,350

Lipids



Moisture content

%

NE

81.2

83.2

83.5

79.6

79.9

79.7

79.7

83.1

80.2

82.2

81.1

79.8

80.4

81.6

79.2

80.4

Lipids



Lipids

%

NE

0.3

0.68

0.42

0.59

0.69

0.64

0.19

0.21

0.32

0.1

0.23

0.28

0.7

0.56

0.91

0.65

Hg

Mercury

mg/Kg ww

0.14

0.008272

0.007308

0.007227

0.0095472

0.0088641

0.0068208

0.0084854

0.0063882

0.0070686

0.0064614

0.0081081

0.0072922

0.0050176

0.0042504

0.0058032

0.0069384

TAL Metals



Aluminum

mg/Kg ww

1,400

1.7 U

1.3 U

1.3 U

1.6 U

1.6 U

1.5 U

1.6 U

1.4 U

1.6 U

4.8

1.5 U

2.0 U

1.6 U

1.5 U

1.6 U

1.5 U

TAL Metals



Antimony

mg/Kg ww

0.54

0.0023 U

0.0016 U

0.0016 U

0.0020 U

0.0020 U

0.0019 U

0.0020 U

0.0017 U

0.0020 U

0.0018 U

0.0019 U

0.0026 U

0.0020 U

0.0018 U

0.0020 U

0.0018 U

TAL Metals



Arsenic

mg/Kg ww

0.0021

3.9

4.2

4.0

3.8

4.0

3.8

4.1

2.9

4.7

6.3

3.7

5.8

6.7

6.1

4.4

3.7

TAL Metals



Barium

mg/Kg ww

270

0.16 U

0.12 U

0.12 U

0.15 U

0.15 U

0.14 U

0.15 U

0.12 U

0.14 U

0.13 U

0.14 U

0.18 U

0.14 U

0.13 U

0.15 U

0.14 U

TAL Metals



Beryllium

mg/Kg ww

2.7

0.17 U

0.13 U

0.13 U

0.16 U

0.16 U

0.15 U

0.16 U

0.14 U

0.16 U

0.14 U

0.15 U

0.20 U

0.16 U

0.15 U

0.16 U

0.15 U

TAL Metals



Cadmium

mg/Kg ww

1.4

0.0017 U

0.0012 U

0.0012 U

0.0015 U

0.0015 U

0.0014 U

0.0015 U

0.0013 U

0.0015 U

0.0013 U

0.0014 U

0.0019 U

0.0015 U

0.0075

0.0015 U

0.0014 U

TAL Metals



Chromium

mg/Kg ww

2,000

0.016 U

0.047 J

0.064 J

0.015 UJ

0.014 UJ

0.059

0.097

0.012 U

0.091

0.013 U

0.013 U

0.018 U

0.13 J

0.013 UJ

0.087 J

0.013 UJ

TAL Metals



Coba It

mg/Kg ww

0.41

0.0010 U

0.0044

0.0043

0.0049

0.0009447 U

0.0008932 U

0.0009541 U

0.0007943 U

0.0009306 U

0.0045

0.0008694 U

0.0065

0.0082

0.0057

0.0052

0.0008624 U

TAL Metals



Copper

mg/Kg ww

54

2.5

2.4

2.9

3.9

2.1

2.2

3.3

2.8

3.1

3.6

2.8

1.9

3.2

2.8

3.2

2.2

TAL Metals



Iron

mg/Kg ww

950

0.55 U

2.9

0.41 U

0.51 U

0.50 U

0.47 U

0.51 U

0.42 U

0.50 U

3.4

0.47 U

0.63 U

14

0.44 U

0.50 U

0.45 U

TAL Metals



Lead

mg/Kg ww

NE

0.041 U

0.030 U

0.031 U

0.039 U

0.038 U

0.037 U

0.039 U

0.032 U

0.038 U

0.034 U

0.036 U

0.048 U

0.037 U

0.035 U

0.040 U

0.035 U

TAL Metals



Magnesium

mg/Kg ww

NE

273

267

243

290

302

272

305

262

277

290

282

281

274

280

266

276

TAL Metals



Manganese

mg/Kg ww

190

0.11

0.14

0.12

1.1

0.13

0.14

0.15

0.11

0.13

0.12

0.23

0.12

0.12

0.12

0.27

0.11

TAL Metals



Nickel

mg/Kg ww

27

0.0073 U

0.17 J

0.045 J

0.0067 UJ

0.0066 UJ

0.0063 U

0.061

0.0056 U

0.0065 U

0.0059 U

0.0062 U

0.0083 U

0.082 J

0.0059 UJ

0.046 J

0.0061 UJ

TAL Metals



Selenium

mg/Kg ww

6.8

0.26

0.25

0.23

0.27

0.22

0.22

0.26

0.22

0.30

0.23

0.25

0.30

0.41

0.29

0.31

0.24

TAL Metals



Silver

mg/Kg ww

6.8

0.021 J

0.015 J

0.040 J

0.041 J

0.022 J

0.028 J

0.035 J

0.025 J

0.044 J

0.036 J

0.043 J

0.075 J

0.092 J

0.086 J

0.087 J

0.049 J

TAL Metals



Thallium

mg/Kg ww

0.014

0.0010 U

0.0007224 U

0.0007425 U

0.0009384 U

0.0009246 U

0.0008729 U

0.0009338 U

0.0007774 U

0.0009108 U

0.0008010 U

0.0008505 U

0.0012 U

0.0009016 U

0.000828 U

0.000936 U

0.0008428 U

TAL Metals



Vanadium

mg/Kg ww

6.8

0.0014 U

0.0055

0.0010 U

0.0013 U

0.0012 U

0.0012 U

0.0013 U

0.0010 U

0.0012 U

0.0073

0.0060

0.0016 U

0.0012 U

0.0011 U

0.0013 U

0.0011 U

TAL Metals



Zinc

mg/Kg ww

410

39

26

24

29

30

39

41

33

42

36

39

40

40

35

37

33

Notes:

mg/kg ww = milligrams per kilogram wet weight
ng/g dw = nanograms per gram dry weight

J = The analyte was positively identified; the quantitation is an estimation.

U = The analyte was analyzed for, but not detected at the method reporting limit shown

FD = field duplicate sample
N = normal sample

Screening Level = Lower of the two (carcinogenic vs. noncancer) fish tissue screening levels (EPA, 2013).
NE = not established

BOLD = detected result exceeds screening level

Italics = analyte not detected but method detection limit exceeds the screening level

PAGE 1 OF 1


-------
TABLE 4-11

Groundwater Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Repor

Location:







GW-01

GW-01

GW-02

GW-03

GW-04

GW-05R

GW-05R

Activity ID:







2013SC-GW-01-20130525

2013SC-GW-901-20130525FD

2013SC-GW-02-20130526

2013SC-GW-03-20130525

2013SC-GW-04-20130526

2013SC-GW-05-20130830

2013SC-GW-905-20130830FD

Sample Type:







N

FD

N

N

N

N

FD

Date Sampled:







5/25/2013

5/25/2013

5/26/2013

5/25/2013

5/26/2013

8/30/2013

8/30/2013







Screening















ChemGroup

Analyte

Units

Level3" b















DRO/RRO

Diesel range organics

ug/L

1,500

17.2 UJ

16.4 UJ



1,640

1,020

112 J

179 J

DRO/RRO

Residual Range Organics

ug/L

1,100

44.3 J

35.4 J



399 J

562

99.1 J

387 J

Hg

Mercury

ug/L

0.94

0.23

0.18 J

0.034 U

0.16 J

0.23

0.034 U

0.034 U

Hg_Diss

Mercury

ug/L

0.94

0.13 J

0.15 J

0.034 U

0.083 J

0.15 J

0.034 U

0.034 U

TAL Metals

Aluminum

ug/L

NE

26.1 U

26.1 U

498

431

3,460

600

703

TAL Metals

Antimony

ug/L

500

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

TAL Metals

Arsenic

ug/L

36

0.64 J

0.6 J

0.79 J

2.2

11.2

3.7

3.4

TAL Metals

Barium

ug/L

200

1.6 J

2.7 J

10.4

8.5 J

21.8

9.6 J

9.1 J

TAL Metals

Beryllium

ug/L

100

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

TAL Metals

Cadmium

ug/L

CO
CO

0.069 U

0.069 U

0.071 J

0.21 J

0.15 J

0.069 U

0.069 U

TAL Metals

Calcium

ug/L

NE

7,850

7,670

6,230

21,200

36,500

29,200

31,100

TAL Metals

Chromium

ug/L

27.4

0.17 J

0.17 J

2.2

0.81 J

5.1

0.11 U

0.11 U

TAL Metals

Cobalt

ug/L

1

2.9

3

1.7

1.1

6.9

2.4 J

2.4 J

TAL Metals

Copper

ug/L

3.1

0.049 U

0.049 U

S4.3

2S2

239

7.6 J

6.7 J

TAL Metals

Iron

ug/L

50

1,230

1,180

979

9,280

9,030

3,240

3,550

TAL Metals

Lead

ug/L

8.1

0.021 U

0.021 U

3.1

0.021 U

3.7

0.021 U

0.021 U

TAL Metals

Magnesium

ug/L

NE

1,820 J

1,880 J

1,590 J

1,980 J

3,330 J

2,050 J

2,140 J

TAL Metals

Manganese

ug/L

100

419 J

434 J

143 J

2S3 J

1,390 J

2,460

2,180

TAL Metals

Nickel

ug/L

8.2

0.23 J

0.18 J

4.4

1.1

4.4

0.049 U

0.049 U

TAL Metals

Potassium

ug/L

NE

337 J

402 J

884 J

884 J

1,600 J

700 J

715 J

TAL Metals

Selenium

ug/L

71

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

TAL Metals

Silver

ug/L

0.95

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

TAL Metals

Sodium

ug/L

NE

226 U

226 U

226 U

7,360

7,220

4,820 J

4,970 J

TAL Metals

Thallium

ug/L

17

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

TAL Metals

Vanadium

ug/L

50

0.99 J

0.98 J

3.7 J

3.4 J

22.4

2.7 J

2.3 J

TAL Metals

Zinc

ug/L

81

1.5 J

0.89 J

9S0

44.9

145

4.1

3.3

TAL Metals_Diss

Aluminum

ug/L

NE

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

26.1 U

TAL Metals_Diss

Antimony

ug/L

500

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

0.085 U

TAL Metals_Diss

Arsenic

ug/L

36

0.55 J

0.61 J

0.66 J

1.8

10.6

3.2

2.9

TAL Metals_Diss

Barium

ug/L

200

1.5 J

1.5 J

9.3 J

8.8 J

4.1 J

7.2 J

8.1 J

TAL Metals_Diss

Beryllium

ug/L

100

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

0.051 U

TAL Metals_Diss

Cadmium

ug/L

CO
CO

0.069 U

0.069 U

0.069 U

0.4 J

0.069 U

0.069 U

0.069 U

TAL Metals_Diss

Calcium

ug/L

NE

7,530

8,300

6,340

20,000

34,800

29,200

30,600

TAL Metals_Diss

Chromium

ug/L

27.4

0.13 J

0.15 J

1.4 J

0.36 J

0.38 J

0.11 U

0.11 U

TAL Metals_Diss

Cobalt

ug/L

1

2.7

2.S

1.7

1 J

1.5

2.1 J

2 J

TAL Metals_Diss

Copper

ug/L

3.1

0.049 U

0.049 U

44.2

176

0.049 U

0.049 U

0.049 U

TAL Metals_Diss

Iron

ug/L

50

1,060

1,160

SOS

5,380

6,560

2,620 J

2,640 J

TAL Metals_Diss

Lead

ug/L

8.1

0.021 U

0.021 U

0.021 U

0.021 U

0.021 U

0.021 U

0.021 U

TAL Metals_Diss

Magnesium

ug/L

NE

1,830 J

1,990 J

1,640 J

1,860 J

3,000 J

2,060 J

2,180 J

TAL Metals_Diss

Manganese

ug/L

100

400 J

421 J

161 J

23S J

1,270 J

2,000

2,100

TAL Metals_Diss

Nickel

ug/L

8.2

0.27 J

0.17 J

4.4

0.9 J

0.24 J

0.049 U

0.049 U

TAL Metals_Diss

Potassium

ug/L

NE

465 J

422 J

880 J

935 J

1,960 J

777 J

714 J

TAL Metals_Diss

Selenium

ug/L

71

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

1.5 U

TAL Metals_Diss

Silver

ug/L

0.95

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

0.033 U

TAL Metals_Diss

Sodium

ug/L

NE

5,240

5,070

2,810 J

7,900

10,200

4,660 J

4,950 J

TAL Metals_Diss

Thallium

ug/L

17

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

0.036 U

TAL Metals_Diss

Vanadium

ug/L

50

0.85 J

0.86 J

1.6 J

2.2 J

4.2 J

0.64 J

1.1 J

TAL Metals Diss

Zinc

ug/L

81

1.2 J

0.89 J

S23

55.8

14.6

3.8

0.6 U

TCLPAHs

2-Methyl naphthalene

ug/L

300

2.3

2.6



0.1 U

0.1 U

0.1 U

0.1 U

TCLPAHs

Acenaphthene

ug/L

40

8

8.9



0.27

1.3

1

0.94

TCL PAHs

Acenaphthylene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Anthracene

ug/L

300

0.34

0.29



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Benz(a)anthracene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Benzo(a)pyrene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Benzo(b)fluoranthene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Benzo(ghi)perylene

ug/L

300

0.15

0.05 U



0.15

0.15

0.05 U

0.05 U

TCL PAHs

Benzo(k)fluoranthene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Chrysene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Dibenz(a,h)anthracene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Fluoranthene

ug/L

11

0.4

0.32



0.1

0.05 U

0.05 U

0.05 U

TCL PAHs

Fluorene

ug/L

300

5.1

5.8



0.49

0.5

0.11

0.091 J

TCL PAHs

lndeno(l,2,3-cd)pyrene

ug/L

300

0.05 U

0.05 U



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Naphthalene

ug/L

1.4

17

IS



0.18

0.16

0.05 U

0.05 U

TCL PAHs

Phenanthrene

ug/L

4.6

2.2

2.5



0.05 U

0.05 U

0.05 U

0.05 U

TCL PAHs

Pyrene

ug/L

300

0.29

0.28



0.13

0.05 U

0.05 U

0.05 U

Notes:

PAH = polycyclic aromatic hydrocarbon

DRO = diesel range organics

RRO = residual range organics

ug/L = micrograms per liter

FD = field duplicate sample

N = normal sample

J = The analyte was positively identified; the quantitation is an estimation
U = The analyte was analyzed for, but not detected at the method detection limit showr

PAGE 1 OF 2


-------
TABLE 4-11

Groundwater Sample Results

2013 Salt Chuck Mine Superfund Site Field Data Repor

Location: GW-01
Activity ID: 2013SC-GW-01-20130525

Sample Type: N
Date Sampled: 5/25/2013

GW-01

2013SC-GW-901-20130525FD
FD

5/25/2013

GW-02

2013SC-GW-02-20130526
N

5/26/2013

GW-03

2013SC-GW-03-20130525
N

5/25/2013

GW-04

2013SC-GW-04-20130526
N

5/26/2013

GW-05R

2013SC-GW-05-20130830
N

8/30/2013

GW-05R

2013SC-GW-905-20130830FD
FD

8/30/2013

ChemGroup

Analyte

Units

Screening

Level31 b



b Screening Level = AWQC listed in NOAA SQuiRT (Buchman, 2008) selected in the following order of preference:
a = Marine chronic
b = Marine acute
bScreening Level for Petroleum = 18 AAC 75 Table C values

NE = not established

AAC = Alaska Administrative Code
Diss = dissolved

NOAA = National Oceanic and Atmospheric Administration

SQuiRT = Screening Quick Reference Tables

MDL = method detection limit

PAHs = polycyclic aromatic hydrocarbons

TAL = target analyte list

BOLD = detected result exceeds screening level

Italics = analyte not detected but method detection limit exceeds the associated screening le\

PAGE 2 OF 2


-------
Figures


-------

-------
Unnamed Island

if

¦

>
\

SS-140

SS-1391— SS-141

V

r

SS-147

SS-145

Salt	C

SS-144

SS-143

\

V

SS-146

Bioassay and Sediment Chemistry Sample Locations

• Bioassay and Chemistry Sample Location
G Chemistry-onty Sample Location
O Reference Bioassay Sample Location
Internal Boundaries
—1 Approximate Marine Area Boundary (MHHW)

Topography and Bathymetry
Upland Topographic Contours
(100 ft contour tine)

Notes:

(1) Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,
UTM Zone 8N, Meters. Pixel size 1 meter.

0
L

375
	I	

750 Feet

Figure 2-1
2013 Surface Sediment
And Sediment Toxicty
Sample Locations

Salt Chuck Mine, Alaska

	£Em


-------
Former Mi

Salt	C

~



i\

s*»

Agronomic Sample Location

Agronomic and Metals Analyses
Internal Boundaries

¦¦ 1 Approximate Marine Area Boundary (MHHW)
Topography and Bathymetry

	Major Elevation Contour (feet NAVD88)

	Minor Elevation Contour (feet NAVD88)

Upland Features

	Upland Stream

	Wooden Barge

I 1 Former Structure

Intertidal Zone Features
Piling Structure
Rock Jetty
NTCRA Features

Tailings and Contaminated
O Soil Removal Area

(Backfilled and Covered)
Rock Outcrop

100
	I	

200 Feet

Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,

LTTM Zone 8N, Meters. Pixel size 1 meter.

(2)	Historical mine and mill features (torn

Focused Upland Engineering Evaluation/Cost Analysis (EE/CA)

Final Report Salt Chuck Mine Report (URS, March 2010)

(3)	Marine bathymetry and structures near former mill from
2013 EPA Survey Data

(4)	Excavation area and topography at former mill from Final Completion
Report Non-Time -Critical Removal Action Salt Chuck Mine Mill
Prince of Wales Island, Alaska, North Wind for USFS, May 2012

Figure 2-2
2013 Agronomic
Surface Sediment
Sample Locations

Salt Chuck Mine, Alaska

	SEPA


-------


SB-116

SB-112

Former Mill

SB-109

A^SB-126

SB-131

^SB-135

SB-137

SB-121



SB-125

V

SB-134

V

SB-129



SB-136

¦ SB-123



SB-133



SB-128

SB-119



SB-127



SB-132

SB-111

^-SB-118

1-©

SB-194



<— SB-205
SB-124

•SB-192



SB-198

SB-115 _

SB-191 -i



SB-197

SB-195



SB-196

SB-199

Salt	C

^SB-158

\	V^SB-202



SB-117

SB-201



SB-120



SB-114



>
V

Sediment Core Locations
Deep core with samples
Shallow core w ith sampfes
Deep core, no sample
Shallow core, no sample
lest pit wih samples
Test pit no sample

Sample Analyzed for Chromium VI

Interna] Boundaries

Approxin ate Marine Area Boundary (MHHW)
Approximate Upland Area Boundary
Topography and Bathymetry

	Major Elevation Contour (feet NAVD88)

	Mnor Elevation Contour (feet NAVD3S)

Upland Features

	 Upland Stream

	Wooden Barge

| Forrrwr Structure

intertidai Zone Features

# Piling Structure

Rock Jetty
NTCRA Features

	Taiings and Contaminated

j | Soil Removal Area

{Backfilled and Cowered)
Rock Outcrop

Sample Analyzed for Chromium VI and SPLP Metals

Sample Analyzed for SPLP meiate

200
	I	

Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,

HTM Zone 8N, Meters. Pixel size 1 meter.

(2)	Historical mine and mill features from

Focused Upland Engineering Evaluation/Cost Analysis (EE/CA)

Final Report Salt Chuck Mine Report (URS, March 2010)

(3)	Marine bathymetry and structures near former mill from
2013 EPA Survey Data

(4)	Excavation area and topography at former mill from Final Completion
Report Non-Time -Critical Removal Action Salt Chuck Mine Mill

Prince of Wales Island, Alaska, North Wind for USFS, May 2012

Figure 2-3
2013 Sediment Core and
Test Pit Locations

Salt Chuck Mine, Alaska

A I



¦N 1/30/2014 6:11:09 PM


-------
UT-08

UT-06

UT-07

SB-180

UT28

UT23

M Q

>.



Salt

Chuck



Upland Tailings Locations, Test Pits and Short Cores Topography and Bathymetry

NTCRA Features

5

V Tailings observed
No tailings observed
Tailings observed, sample collected
No tailings observed, sample collected
Internal Boundaries

Approximate Upland Area Boundary
Approximate Marine Area Boundary (MHHW)

	Major Elevation Contour {feet NAVD88} 	 Tailings and Contaminated

	Mir or Elevation Contour {feet N AVD88) I	1 ®?'! ^™val

(Backfilled and Covered)

Upland Features

I Former Structure
Intertidal Zone Features

• Piling Structure

100
	I	

200 Feet

Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,

UTM Zone 8N, Meters Pixel size 1 meter.

(2)	Historical mine and mill features from

Focused Upland Engineering Evaluation/Cost Analysis (EE/CA)

Final Report Salt Chuck Mine Report (URS, March 2010)

(3)	Marine bathymetry and structures near former mill from
2013 EPA Survey Data

(4)	Excavation area and topography at former mill from Final Completion
Report Non-Time -Critical Removal Action Salt Chuck Mine Mill

Prince of Wales Island, Alaska, North Wind for USFS, May 2012

Figure 2-4
2013 Upland Tailings Sample
and Delineation Locations

Salt Chuck Mine, Alaska

	6Em


-------
Browns
Bay

Gosti Island

PW-513

PW-511

PW-512



2013 Porewater Sample Locations

o Airstone Sample Location (Reference Area)
0 Airstone Sample Location (Site)
~ Drive-point Sample Location
Internal Boundaries
— Approximate Upland Area Boundary
™ ¦ Approximate Marine Area Boundary (MHHW)
Topography and Bathymetry

	Major Elevation Contour (feet NAVD88)

	Mnor Elevation Contour (feet NAVD88)

Upland Features

	Upland Stream

	Wooden Barge

I I Former Structure
Intertidal Zone Features
¦ Piling Structure
—Rock Jetty

NTCRA Features

	Tailings and Contaminated

~ Soil Removal Area

(Backfilled and Covered)
Rock Outcrop

o
L

200
	I	

400 Feet
_J

Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,

UTM Zone 8N, Meters. Pixel size 1 meter.

(2)	Historical mine and mill features from

Focused Upland Engineering Evaluation/Cost Analysts (EE/CA)

Final Report Salt Chuck Mine Report (URS, March 2010)

(3)	Marine bathymetry and structures near former mill from
2013 EPA Survey Data

(4)	Excavation area and topography at former mill from Final Completion
Report Non-Time -Critical Removal Action Salt Chuck Mine Mill

Prince of Wales Island, Alaska, North Wind for USFS, May 2012

KHEIDEMAN 1/30/:

Figure 2-5
2013 Porewater
Sample Locations

Salt Chuck Mine, Alaska

	6ER&

PW-088

PW-092

PW-068

PW-017

PW-076

PW-Q08

PW-003

PW-006


-------
X

vSW-503 \

SW-507

SW-501



Browns vsw-505

SW-085 -

> ^

S/

Bay

v

\

Gosti Island

SW-509



SW-113

V





SW-108

SW-099

SW-105

SW-600

$

D

a

a

£

Salt	C

~;

%•%

Sail

Chuck

2013 Surface water Sample Locations

Grab Sample Location
Hourly Grab Sample Location
A Reference Area Grab Sample Location
§ Water used for SPLP Analysis

Internal Boundaries

Approximate Upland Area Boundary
i Approximate Marine Area Boundary (MHHW)

Topography and Battiymetry	Intertidal Zone Features

	Major Elevation Contour (feet NAVDflS) • Piling Structoire

	Minor Elevation Contour (feet NAVD88)	Rock Jetty

Upland Features

	Upland Stream

	Wooden Barge

I I Former Structure

NTCRA Features

Tailings and Contaminated
' | Soil Removal Area

(Backfilled and Covered)
Rock Outcrop

200

400 Feet

Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,

HTM Zone 8N, Meters. Pixel size 1 meter.

(2)	Historical mine and mill features from

Focused Upland Engineering Evaluation/Cost Analysis (EE/CA)

Final Report Salt Chuck Mine Report (URS, March 2010)

(3)	Marine bathymetry and structures near former mill from
2013 EPA Survey Data

(4)	Excavation area and topography at former mill from Final Completion
Report Non-Time -Critical Removal Action Salt Chuck Mine Mill
Prince of Wales Island, Alaska, North Wind for USFS, May 2012

KHEIDEMAN 1/30/2014 12:09:25

Figure 2-6
2013 Surface Water
Sample Locations

Salt Chuck Mine, Alaska

	&ER*


-------
r

*£> T-

Browns
Bay

tC,

>5&

Biota-142

Biota-508

Biota-504

Biota-502

- Biota-506
Biota-500



*v.a

Biota-130



V - TO* i .

Biota-149



Biota-107

Biota-148

Biota-152

Biota-151





Biota-150



Biota-153



I Biota (Dungeness Crab) Sample Locations

O Reference Area Sample Location
C Site Sample Location
Internal Boundaries
— Approximate Marine Area Boundary (MHHW)
Topography and Bathymetry
Upland Topographic Contours
{100 ft contour line)

Notes:

(1) Aerial photography courtesy US Census
Bureau; approximate date 2006. NAD83,
UTM Zone 8N, Meters. Pixel size 1 meter

750 Feet

Figure 2-7
2013 Marine Biota
Sample Locations

Salt Chuck Mine, Alaska

	£ER&


-------
GW-06

Sampled, but not submitted
for analysis due to colloidal
material in samples.



Farjtur



kill Chile*, Hill



~



% *•



\\







Cfctrck

&

Ataoder. Barge
Ut«rl
-------
Appendix H

Arsenic Speciation Results for 2012 Bivalve

Samples


-------
From: Keeley, Karen [mailto:Keeley.Karen@epa.gov1
Sent: Monday, July 01, 2013 3:34 PM

To: Hamade, Ali K (HSS) (ali.hamade@alaska.gov); Cooper, Stacey B (HSS)

Cc: Kissinger, Lon; Duncan, Bruce; Townley, Paul J/SEA; Shelton, Dennis/CVO;

Mandy.M.Michalsen@usace.army.mil; Anne Marie Palmieri (annemarie.palmieri@alaska.gov); Wilcox,
Michael -FS; Goulet, Joe

Subject: Salt Chuck Mine Superfund Site - Arsenic Speciation in Clam Tissue
Ali and Stacey,

Please find attached the results of the arsenic speciation in ten samples of freeze-dried clam
tissues collected in 2012 (analyzed in 2013) for the Salt Chuck Mine Superfund Site. In
evaluating the data, please be sure to read the relevant notes below the table. As a reminder,
the sampled clam species are butter clam (BC), littleneck (LN) and the softshell clam, Mya
arenaria (SC). Station locations are depicted in the attached figures.

The results indicate that the percentage of the nontoxic organic form of arsenic ranged from
about 70% to >99%, with an average for all species tested of 89%. This is consistent with the
default of 90% that is sometimes used in risk assessments. You will notice however, that the
results are species-specific, with the softshell clam (Mya arenaria ) showing the highest
percentages of inorganic forms of arsenic. Given this outcome, when evaluating risks for clam
consumption, it appears that softshell clams should not be lumped together with other clams
(e.g., hardshell clams). This effect observed in the softshell clam has also been observed in
other areas (see below) and by EPA at other Region 10 sediment cleanup sites [e.g., Lower
Duwamish Waterway Superfund site; Harbor Island (East Waterway) Superfund Site] and likely
reflects inherent biological differences for this species. EPA is funding a research project on this
issue (see below). Please also note that none of the bivalve samples were depurated to remove
sediment from their gut contents prior to analysis; this can also affect softshell clams more
since they tend to live in muddier sediments.

EPA does not at this time believe that arsenic is associated with mine-related releases at Salt
Chuck Mine. The reasons are as follows: 1) During the 2011 and 2012 Rl sampling, a total of
136 sediment samples were analyzed for arsenic, only 2 of which had concentrations over 10
mg/kg and the maximum being 13.2 mg/kg. These levels appear consistent with naturally-
occurring levels. 2) There is no spatial association between concentrations of arsenic and
copper (copper is a definitive signature of mine-related releases at this site). This holds true for
both chemical concentrations in sediment and in bivalve tissues, where tissue samples with the
highest copper concentrations often have some of the lowest arsenic concentrations. 3) Arsenic
concentrations in sediments measured in Salt Chuck Bay are consistent with levels measured in
Browns Bay, which is a nearby area that has been identified as a 'reference area' - an area that
does not appear to be contaminated by mining activity. Most importantly, there appears to be
no direct association between sediment arsenic concentrations and co-located bivalve tissue
concentrations of arsenic. Given this observation, one can surmise that any remedy that would

H-l


-------
affect sediment would not be expected to have an effect on arsenic concentrations in clam
tissues.

Short background summary of EPA-funded study on Mya (for the Lower Duwamish Waterway
Site):

Mya arenaria has been reported previously to have the potential for high inorganic
arsenic accumulation. An investigation of an arsenic-contaminated marine site in Seal
Harbour, Nova Scotia, Canada, revealed that clams contained mostly inorganic arsenic
(Koch et al. 2007). In contrast, clams from a less contaminated area had inorganic
arsenic averaging 8.2% of total concentration. The higher concentrations and
proportions of inorganic arsenic in clams from the contaminated areas, compared with
control samples, appear to reflect the elevated inorganic arsenic present in the sediment
and water surrounding the organisms, which are the likeliest arsenic exposure routes
(Koch et al. 2007). It is not possible to generalize patterns of uptake and transformation
across invertebrates. However, the poor relationship between arsenic concentrations in
polychaetes and in sediments has been reported by Waring et al. (2005). Overall, no
significant correlation was observed, suggesting a limited utility of such relationships to
predict and interpret concentrations in polychaetes across different sites. The lack of a
strong relationship between body residues and sediment concentration is
understandable considering that sediments do not necessarily represent the main source
of arsenic for all polychaetes, that various species can interact differently with
suspended matter, surface and inner sediments, and that arsenic speciation in sediments
and tissues is controlled by different factors which can influence both bioavailability and
bioaccumulation rate (Fattorine et al. 2005). Overall, studies of arsenic concentrations in
polychaetes appear to confirm the hypothesis of the importance of species-specific
peculiarities, i.e. physiological features and/or ecological characteristics, affect arsenic
uptake and metabolism.

Please let us know if you would like to discuss these data, and we would be glad to set up a call.

Sincerely,

Karen Keeley | Superfund Remedial Project Manager
U.S. Environmental Protection Agency | Region 10

Office of

1200 6th ¦	:	11 | Seattle, WA 98101

p: 206,5!

H-2


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Table A
Arsenic Speciation Results3

Project Name: Salt Chuck Mine
Project Code: SFP-011B

1

Sample
Number

2

Sample
Description

3

Total
Arsenic in
tissue
(ng/g)

4

Total
Arsenic in
extract
(ng/g)

5

Extraction
Efficiency
(%)

Arsenic Species

7

Sum of All
Species
(ng/g)

8

Chromato-
graphic
Recovery
(%)

9

Overall
Speciation
Recovery
(%)

10

Inorganic %
of Total Asb

11

Organic % of
Total As

Inorganic
As (As+3 &
As+5)

AsB + Cation
species
(ng/g) * t

MMA
(ng/g)

DMA
(ng/g)

UIIKNUWN

arsenic
species
(ng/g) t



N1-12314509

SCTISS-329-LN

23700

17900

76

152

4230

130 U

1250

9590

15222

85

64

0.64%

99.36%

COMP-12314547

SCTISS-316-SC

17300

10200

59

5310

1610

120 U

483

2070

9473

93

55

30.69%

69.31%

COMP-12314552

SCTISS-329-BC

28100

19000

68

140 U

2920

140 U

1960

10800

15680

83

56

0.50%

99.50%

COMP-12314552DU

SCTISS-329-BC

28100

19400

69

140 U

2860

140 U

1950

10600

15410

79

55

0.50%

99.50%

COMP-12314552S1

SCTISS-329-BC

NA

NA

NA

98%

105%

104%

95%

NA

NA

NA

NA





COMP-12314552S2

SCTISS-329-BC

NA

NA

NA

101%

104%

104%

90%

NA

NA

NA

NA





N2-12314557

SCTISS-335-BC

28300

20700

73

191

3040

140 U

1780

11600

16611

80

59

0.67%

99.33%

COMP-12314558

SCTISS-336-SC

11000

7900

72

930

1850

54 U

638

3510

6928

88

63

8.45%

91.55%

N1-12314559

SCTISS-337-SC

12100

9230

76

1920

2750

57 U

517

3360

8547

93

71

15.87%

84.13%

COMP-12314563

SCTISS-312-SC

21300

10000

47

5890

1580

130 U

302

1740

9512

95

45

27.65%

72.35%

N1-12314565

SCTISS-336-LN

27800

20300

73

140 U

4200

140 U

1480

11100

16780

83

60

0.50%

99.50%

N1-12314714

SCTISS-335-SC

11200

7580

68

853

1580

54 U

717

3500

6650

88

59

7.62%

92.38%

COMP-12314717

SCTISS-311-SC

15300

9060

59

3990

2010

110 U

422

1930

8352

92

55

26.08%

73.92%

IT043013AL1

Spike blank

8000

8080

101

101%

112%

100%

96%

NA

NA

NA

NA





IT043013ACO

Dorm II

18000

15900

88

260 U

15400

260 U

301

260 UJ

15701

99

87





IT043013BCO

CRM Tuna

4800

3930

82

59 U

3640

59 U

148

59 UJ

3788

96

79





IT043013ABL

Blank

NA

NA

NA

58 U

58 UJ

58 U

58 U

58 UJ

NA

NA

NA





Average 89.17%

All results reported on a Dry Weight basis	t All AsB + Cation and Unknown Arsenic Species results are qualified 'J', (estimated, qualifiers not shown in table)

U - The analyte was not detected at or above the reported value.

J - The identification of the analyte is acceptable; the reported value is an estimate.

JL - The identification of the analyte is acceptable; the repored value is an estimate and may be biased low. The actual value is expected to be greater than the reported value.

NA- Not Applicable/Not Found

* - Only AsB in Spike added AsB only.

a. The bivalve samples were not depurated to remove sediment from their gut contents prior to analysis.

PAGE 1 OF 1


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Notes:

(1)	Aerial photography courtesy US Census
Bureau; approximate date 2006, NAD83,
UTM Zone 8N, Meters. Pixel size 1 meter

(2)	Source Documents: Figures 2-2 and 2-3,
URS, Salt Chuck Mine Report, March 2010.
Features: C-Series, D-Series, Mean High
Tide, Stream, with modifications based on
site observations from 2012 Rl investigation.

(3)	TNF = Tongass National Forest

DRAFT

Figure 4
Salt Chuck Bay
Intertidal Sample Locations

Salt Chuck Mine, Alaska

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Bay

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