Katrina Response Environmental Soil and Sediment Sampling Gulf Coast of Mississippi October, 2005


United States Environmental Protection Agency, Region 4

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Report
Katrina Response
Environmental Soil and Sediment Sampling
Gulf Coast of Mississippi
October, 2005

Science and Ecosystem Support Division
980 College Station Road
Athens, GA 30605

Mississippi Department of Environmental Quality
2380 Highway 80 West
Jackson, Mississippi 39204

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Title and Approval Sheet

Title: Report, Katrina Response Environmental Soil and
Sediment Sampling, Gulf Coast of Mississippi

Approvals:

Jl

Fred Sloa

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Sloan

Project Leader
Superfund and Air Section
Environmental Investi:

Date

nch

Scott Sudweeks

Chief

Technical SujjpdctSection

S uperfy&d'BLemedial

I't-f-Z tfos"

Date

ic^rl Support Branch

idall Chaffins"

^Acting Chief

3erfundiRemedial and Technical Support Branch

	:	im

Antujnio uumones

Chief

Environmental Investigations Branch

Date

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Executive Summary

On August 29, 2005, Hurricane Katrina made landfall along the Gulf coast of the
southeastern United States, causing unprecedented damage from eastern Louisiana to
near Mobile, Alabama, due to the high winds and storm surge. During the week of
October 3, 2005, the USE PA Region 4, Science and Ecosystem Support Division (SESD)
collected soil and sediment samples near facilities in the affected areas in Mississippi to
determine if flooding from the storm surge released hazardous constituents and materials.
The facilities being investigated were located in the storm surge impacted portions of
Hancock, Harrison and Jackson Counties in Mississippi. This investigation was
requested by the Mississippi Department of Environmental Quality (MDEQ) and the
USEPA, Region 4, Waste Management Division.

The locations of these sites are shown and identified in Figure 1 (Appendix A),
while Figures 2 through 7 show the facilities. Sample locations are shown in Figures 8
through 13, also included in Appendix A. The analytical data are presented in Section 6
and Appendix B of this report.

The analytical data presented in Section 6 and Appendix B of this report, was
evaluated by the Region 4 Waste Management Division, Technical Services Section
(TSS) to determine if there were any observable or attributable Post-Katrina impacts at
the investigated sites. Technical Services Section staff reviewed the data presented in
Section 6 and Appendix B. Evaluating the sampling data to determine if there was an
off-site impact from Hurricane Katrina posed a challenge, due to the scarcity of pre-
existing sampling data and supporting information that could be used for data
interpretation.

EPA's conclusions regarding the potential impact of the hurricane on these sites
are based on a comparison of post-hurricane data to available past sample data collected
during any facility investigations or routine monitoring activities. In addition, the results
were compared to EPA Region 9 Preliminary Remediation Goals (PRCs) to determine if
conditions at the sites might represent previously unrecognized risks to human health and
the environment. EPA Region 9 PRCs (available at:

http://vvvvvv.epa.gov/region9/vvaste/sfund/prg/index.html) are conservative risk-based
concentrations based on long-term exposures in either a residential or
commercial/industrial setting. They are considered by EPA to be protective for people
(including sensitive groups) over a lifetime. The PRCs are not clean up standards, but
used to assist EPA scientists and others in initial screening-level evaluations of
environmental measurements. The impact evaluations are presented in Section 7 of this
report.

The scope of the investigations at each site and the conclusions that were reached
regarding releases or impacts from Hurricane Katrina are presented in the following site
summaries. For the Risk Management Plan (RMP), Toxic Release Inventory (TRI) and
Tier II Emergency Planning and Community Right-to-Know Act (EPCRA) facilities,
PRCs based on an industrial/commercial exposure situation were utilized, except in the
case where samples were taken in the vicinity of residential development; in which case

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residential PRC soil screening values were used. The impact evaluations are presented in
Section 7 of this report.

The scope of the investigations at each site and the conclusions that were reached
regarding releases or impacts from Hurricane Katrina are presented in the following site
summaries:

DuPont DeLisle - Pass Christian. Mississippi

Three surface soil and two sediment samples were collected at five locations.
These samples were analyzed for volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), pesticides/PCBs, and metals. Low levels of metals, VOCs,
pesticides, and SVOCs were detected in samples. Samples were also collected for
dioxins. The dioxin data will be released in an addendum to this report when it is
available. No PCBs were reported.

From a comparison with sampling conducted pre-hurricane Katrina there is no
clear and consistent pattern of increased contamination levels that would clearly indicate
a potential release in the area of the DuPont DeLisle facility due to the effects of
Hurricane Katrina. None of the reported analytes exceeded risk-based soil screening
benchmarks for an industrial exposure scenario, or residential PRCs in the vicinity of
residential development northeast of the facility.

Chevron Pascagoula. First Chemical. Mississippi Phosphates - Pascagoula. Mississippi

Three surface soil and seven sediment samples were collected at ten locations.
These samples were analyzed for volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), pesticides/PCBs, metals, and radionuclides (samples BC2
and BC4 were collected as part of another investigation, no radionuclide analyses were
performed on these samples). Several metals were detected, along with low
concentrations of VOCs, pesticides, and SVOCs. No PCBs were reported in these
samples.

Several metals exceeded pre-hurricane concentrations, however these elevated
concentrations were detected in sediments in a ditch that is part of a solid waste
management unit on site property that was previously known to contain elevated metals
concentrations and were the site of previous industrial activity. EPA believes the
exceedances are not significant enough to clearly indicate an impact due to hurricane
Katrina in light of the likelihood of pre-existing metals contamination in surficial soil and
drainage ditch sediments. Maximum detected levels of the metals arsenic and chromium
exceeded PRCs, however were within a risk-range considered acceptable by EP A in
other regulatory contexts. It is unlikely that frequent and prolonged human contact with
sediments under water in drainage ditches would occur. There does not appear to be an
indication of a potential release in the area of the facilities due to the effects of Hurricane
Katrina.

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Omega Protein - Moss Point. Mississippi

Three sediment samples were collected at three locations. These samples were
analyzed for volatile organic compounds (VOCs), semi-volatile organic compounds
(SVOCs), pesticides/PCBs, and metals. Low concentrations of several metals were
detected, along with several reported low concentrations of SVOCs. One PCB was
reported. No VOCs were reported.

There is no indication of a potential release in the area of the Omega Protein facility due
to the effects of Hurricane Katrina. None of the reported analytes exceeded human health
benchmarks for exposed to contaminants in soil or sediment under a
commercial/industrial scenario.

Port Bienville Industrial Park (Polvchemie. Inc.) - Pearlington, Mississippi

Two surface soil and three sediment samples were collected at five locations.
These samples were analyzed for volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), pesticides/PCBs, and metals. Low levels of several metals
were detected, along with low levels of ten SVOCs, along with a few VOCs, and
pesticides. No PCBs were reported for these samples.

Arsenic and benzo(a)pyrene exceeded PRCs but fell within a risk range of 1 in
1,000,000 to 1 in 10,000 risk over background of an individual developing cancer over a
lifetime from long-term exposure to those concentrations, which EPA has found
acceptable in other regulatory and remedial contexts. None of the remaining analytes
detected in soil or sediment exceeded industrial PRC soil screening levels. There is no
indication of a potential release in the area of the Polychemie, Inc. facility, due to the
effects of Hurricane Katrina.

Ershigs Fiberglass, Inc. - Biloxi. Mississippi

Three surface soil and two sediment samples were collected at five locations.
These samples were analyzed for volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), pesticides/PCBs, and metals. Low concentrations of
several pesticides and SVOCs were reported. No VOCs or PCBs were reported.

Arsenic exceeded residential PRCs, however all detections were within a risk
range of 1 in 1,000,000 to 1 in 10,000 risk over background of an individual developing
cancer over a lifetime from long-term exposure to those concentrations, which EPA has
found acceptable in other regulatory and remedial contexts. None of the other analytes
exceeded residential PRC soil screening values. There does not appear to be indication of
a potential release in the area of Ershigs Fiberglass due to the effects of Hurricane
Katrina.

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Naval Construction Battalion Center - Gulfport. Mississippi

Five sediment samples were collected from the wetland north of this installation.
These samples were analyzed for dioxins only. At the request of MDEQ, an additional
four sediment samples were collected in November by SESD personnel from an outfall
that may have been contaminated from a pre-Katrina event. These samples were
analyzed for PCBs only. This data will be released in an addendum to this report when it
becomes available.

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Acronyms



AOC

Area of Concern

ASBLOQAM

Analytical Support Branch Laboratory Operations and Quality



Assurance Manual

bgs

below ground surface

CERCLA

Comprehensive Environmental Response, Compensation, and



Liability Act

CLP

Contract Laboratory Program

DAP

diammonium phosphate

DQO

Data Quality Objectives

EAB

Ecological Assessment Branch

EI

Environmental Indicator

EISOPQAM

Environmental Investigations Standard Operating Procedures and



Quality Assurance Manual

EPCRA

Emergency Planning and Community Right-to-Know Act

ESAT

Environmental Services Assistance Team

FCC

First Chemical Corporation

GPRA

Government Performance and Results Act

GPS

Global Positioning System

HSO

Health and Safety Officer

HSWA

Hazardous and Solid Waste Amendments

IDW

Investigation Derived Waste

MDEQ

Mississippi Department of Environmental Quality

MSDS

Material Safety Data Sheet

MS/MSD

Matrix Spike/Matrix Spike Duplicate

NAREL

National Air and Radiation Environmental Laboratory

NCBC

Naval Construction Battalion Center

osc

On-Scene Coordinator

OSWER

Office of Solid Waste and Emergency Response

PCBs

Polychlorinated Biphenyls

POTW

Publicly-Owned Treatment Works

QAPP

Quality Assurance Project Plan

QA/QC

Quality Assurance/Quality Control

RCRA

Resource Conservation and Recovery Act

RALs

removal action levels

RFA

RCRA Facility Assessment

RFI

RCRA Facility Investigation

RMP

Risk Management Plan

SESD

Science and Ecosystem Support Division

SOW

Statement Of Work

svoc

Semi-Volatile Organic Compound

SWMU

Solid Waste Management Unit

TCL/TAL

Target Compound List/Target Analyte List

TIC

Tentatively Identified Compound

UIC

Underground Injection Control

USAJF

United States Air Force

USEPA

United States Environmental Protection Agency

voc

Volatile Organic Compound

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Table of Contents

Title and Approval Sheet	ii

Executive Summary	iii

Acronyms	vii

1.0 INTRODUCTION	1

1.1	Report Outline	1

1.2	Background/Site Locations	2

1.3	Site Histories/Status Post Katrina	2

2.0 SAMPLING/DATA QUALITY OBJECTIVES	8

2.1 Data Quality Objectives	8

2.1.1	Problem Statement	8

2.1.2	Identify the Decision	8

2.1.3	Decision Inputs	9

2.1.4	Study Boundaries	9

2.1.5	Decision Rule	10

2.1.6	Error Limits	10

2.1.7	Optimize Sampling Design	10

3.0 INVESTIGATION MANAGEMENT PLAN	13

3.1	Field Project Responsibilities	13

3.2	Site Control and Access	13

3.3	Sample Collection and Handling Procedures	13

3.4	Sample Analysis and Validation	14

3.5	Chain of Custody	14

3.5.1	Sample Labels	15

3.5.2	Sample Custody Seals	15

3.5.3	Chain-of-Custody Record	15

3.6	Station and Sample Identification	15

3.7	Site Mapping	 16

3.8	Investigation Derived Waste (IDW)	16

3.9	Sample Containers	16

3.10	Investigation Schedule	16

4.0 SAMPLING DESIGN AND RATIONALE	 17

4.1	Sampling Design	17

4.2	Data Validation/Usability	 17

4.3	Data Management/Document Control	17

5.0 QUALITY ASSURANCE	 18

5.1	Organization and Responsibilities	18

5.2	Field QA/QC Samples	 18

5.2.1	Matrix Spike/Matrix Spike Duplicate	18

5.2.2	Population Variability - Duplicate Samples	18

5.2.3	Sample Handling - On-Site Splits	18

5.2.4	Trip Blanks	19

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6.0 INVESTIGATION RESULTS	20

6.1	DuPont - DeLisle	20

6.2	Chevron - Pascagoula, First Chemical, Mississippi Phosphates	21

6.3	Omega Protein	21

6.4	Port Bienville Industrial Park (Polychemie, Inc.)	21

6.5	Ershigs Fiberglass, Inc	21

6.6	Naval Construction Battalion Center	22

7.0 IMPACT EVALUATION	23

7.1	DuPont DeLisle - Pass Christian, Mississippi	24

7.1.1	Results	24

7.1.2	Discussion	24

7.1.3	Conclusion	25

7.2	Chevron Pascagoula, First Chemical, Mississippi Phosphate -
Pascagoula, Mississippi	25

7.2.1	Results	25

7.2.2	Discussion	26

7.2.3	Conclusion	27

7.3	Omega Protein - Moss Point, Mississippi	28

7.3.1	Results	28

7.3.2	Discussion	28

7.3.3	Conclusion	28

7.4	Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington,
Mississippi	28

7.4.1	Results	28

7.4.2	Discussion	29

7.4.3	Conclusion	29

7.5	Ershigs Fiberglass - Biloxi, Mississippi	30

7.5.1	Results	30

7.5.2	Discussion	30

7.5.3	Conclusion	30

7.6	Naval Construction Battalion Center - Gulfport, Mississsippi	31

8.0 REFERENCES	32

Appendix A	33

Appendix B	48

Appendix C	86

IX

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1.0 INTRODUCTION

On August 29, 2005, Hurricane Katrina made landfall along the Gulf coast of the
southeastern United States, causing unprecedented damage from eastern Louisiana to
near Mobile, Alabama, due to the high winds and storm surge. During the week of
October 3, 2005, the USEPA Region 4, Science and Ecosystem Support Division (SESD)
collected soil and sediment samples near facilities in the affected areas in Mississippi to
determine if flooding from the storm surge released hazardous constituents and materials.
The facilities being investigated are located in the storm surge impacted portions of
Hancock, Harrison and Jackson Counties in Mississippi. This investigation was
requested by the Mississippi Department of Environmental Quality (MDEQ) and the
USEPA, Region 4, Waste Management Division.

The Quality Assurance Project Plan Katrina Response Environmental Soil and
Sediment Sampling Gulf Coast of Mississippi (QAPP, 2005) for the collection of
environmental samples in the three county Gulf coastal area of Mississippi was
developed by the United States Environmental Protection Agency (US-EPA), Region 4,
in accordance with the EPA Guidance for Quality Assurance Project Plans (EPA QA/G-
5, 1998). The QAPP underwent external peer review by the Science Advisory Board,
whose comments were incorporated.

Soil and sediment samples were collected from RMP (Risk Management Plan),
Tier II, and TRI (Toxic Release Inventory) facilities in the three counties. In addition,
one facility. Naval Construction Battalion Center (NCBC) Gulfport, was selected because
the recent flooding may have re-contaminated a partially remediated site. All samples
were analyzed for metals (including mercury), volatile organic compounds and semi-
volatile organic compounds, including pesticides/PCBs (polychlorinated biphenyls), with
the exception of one site (NCBC Gulfport) where some samples were analyzed for
dioxins only, and others were analyzed for PCBs only. At the DuPont DeLisle facility,
samples were also analyzed for dioxin, in addition to the parameters listed above.

Samples from the Chevron Refinery - Pascagoula, First Chemical, and MS Phosphates
complex were analyzed using gamma spectroscopy in addition to the parameters listed
above. Split samples were offered to each facility.

Where knowledge of site specific analytes was available (such as the NCBC and
DuPont DeLisle), the analyte list was tailored for that situation. The analytical results
were evaluated to determine if these constituents are present in soils and sediments
adjacent to the facilities, indicating a possible release to the environment, which could
lead to a more thorough assessment.

1.1 Report Outline

Section 1 provides the introduction to the report and a brief summary of the sites
investigated. Section 2 provides the sampling data quality objectives used to develop the
Quality Assurance Project Plan (QAPP) for the investigation. Section 3 is the
investigation management plan detailing the field procedures used during the study.
Section 4 is the sampling design and rationale, including data validation procedures.

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Section 5 presents QA/QC procedures used during the investigation. Section 6 is a
summary of the sample data. Section 7 presents the results of the decision matrix used to
evaluate the sampling results. Section 8 is references. Appendix A contains the figures
referenced in the report. Appendix B contains data summary tables. Appendix C
contains the laboratory data sheets.

1.2	Background/Site Locations

Figure 1 (Appendix A) is an area map indicating the general locations of the
facilities investigated. Maps were also prepared showing the locations of the facilities
and the proposed sampling locations. See Figures 2-7 in Appendix A.

1.3	Site Histories/Status Post Katrina

These facilities were selected by the Waste Management Division because they
are located in areas of significant widespread damage, and are RMP, Tier II, or TRI
facilities. All have reported damage from the effects of Katrina. One additional facility
(NCBC) was included to assess the possibility of re-contamination of a wetland due to
the flooding. It should be noted that these facilities may be covered by more than one of
these definitions.

Risk Management Plan (RMP) Facilities:

Initial reports from these facilities indicated no visible releases of hazardous
constituents beyond their perimeters. However, due to the large amounts of chemicals
used and/or manufactured by these facilities, an off-site examination was deemed
necessary. The following information was obtained from the South Programs Section,
RCRA Programs Branch.

DuPont DeLisle - Pass Christian

The DuPont-DeLisle plant is a titanium dioxide manufacturing operation located
on Bay St. Louis, in the community of Pass Christian, Mississippi. The DuPont DeLisle
facility operates two identical production lines. Line 1 began production in September
1979, Line 2 production began in October of 1991. DuPont utilizes the Chloride
Ilmenite process to extract titanium from ore. A hazardous waste generated on site is a
mixture of ferrous and ferric chloride. This waste is characteristic for lead, chromium,
and is also considered corrosive. DuPont performs deep well injection onsite through a
Underground Injection Control (UIC) permit.

DuPont DeLisle has an operating RCRA Permit for onsite treatment and storage
units. The annual quantity of D002/D007/D008 wastes for tank treatment, storage and
UIC is listed as 1,500,000 tons per year. On April 13, 2005, DuPont submitted a Class 1
modification package for the RCRA Part B, which proposed the addition of two splitter
tanks which would improve the handling of the corrosive waste streams. The modified
permit was issued August 10, 2005, and will expire on August 9, 2014.

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Because MDEQ is not fully Hazardous and Solid Waste Amendment (HSWA)
authorized, the DeLisle plant is under EPA authority for corrective action through the
HSWA portion of the permit.

RCRA Facility Investigation (RFI) phase I and II have been conducted at the site,
and an approved Corrective Action Groundwater Monitoring Plan is in place to monitor
three areas (5 SWMlJs) for arsenic, barium, beryllium, manganese, lead, cis-1,2
dichloroethene, trans-1,2-dichloroethene, 1,1-dichloroethene, trichloroethene,
tetrachloroethene (PCE) and vinyl chloride:

Southeast Waste Management Area for Solid Waste Management Units
(SWMlJs) 14, 22 & 29;

West Waste Management Area for SWMlJs 8 & 28; and
PCE Containment Sump downgradient.

The class of chemicals known as dioxins and furans (polychlorinated
dibenzodioxins, and polychlorinated dibenzofurans, PCDD/PCDF) are present at the
DuPont-DeLisle facility.

EPA received first communication from DuPont on September 7, 2005. Prior to
that email communication, EPA was unable to establish phone or data contact with
DuPont-DeLisle. EPA has had follow-up contact with the Environmental Office at
DuPont-DeLisle on September 14, 2005. Much of the following information is derived
from these exchanges. MDEQ visited the site two days after the Hurricane along with
Florida Emergency Responders. The storm surged over the site's levee (~ 20 feet) and
the site was under 7 to 9 feet of water. There is significant mud and sediment from Bay
St. Louis spread across the site; DuPont reported that they did not believe there is any
process material in the sediments. All plant process ditches, sumps and trenches were
cleaned prior to the storm and all containment and structures faired well. DuPont has
been in contact with MDEQ on Solid Waste issues.

There was nearly 100% retention in the Waste Management area; one small
breech at WMU #11 of mostly storm water occurred; this was repaired. There have been
no known leaks/releases to the air or water.

Aerial imagery indicates a small area of housing immediately north of the facility.
This facility is located in Figure 2.

Chevron Refinery - Pascagoula

The Pascagoula Refinery was built in the early 1960"s and went into operation in
1963. The Facility is owned by Chevron U.S. A, Inc. and is operated by ChevronTexaco
Products Company, a division of Chevron U.S.A., Inc. The Refinery property consists of
approximately 3,000 acres. A total of 1,000 acres have been developed industrially. The
refinery is ChevronTexaco"s largest with a refining capacity of 325,000 barrels per day.
An expansion to 360,000 barrels per day was underway when Hurricane Katrina struck
the facility.

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The facility is completely surrounded by a hurricane dike that has closable gates.
The dike was not breeched, however, it was eroded in places and the facility was flooded.
This caused a loss of power at the facility which has now been restored. Power was lost
to the storm water pumping system and the wastewater treatment system [the units of the
wastewater treatment system are HSWA SWMUs], The wastewater treatment system
was restarted about 10 days after the storm. The oil shipping terminal is back in
operation, therefore, ChevronTexaco can distribute product which was stored in tanks or
arrives by ship. The RCRA regulated units are at one of the highest points in the facility
and were not flooded. The tank field was flooded, but there have been no observed
releases inside the facility.

The facility also had HSWA corrective action underway in August before the
hurricane struck. A removal action at the Wharf Revetment Area in the shipping terminal
was completed two days before the hurricane struck and the area was concreted over.

First report is that the new, concrete revetment, [as opposed to sandbags] held up well in
the storm, thus protecting the area that was excavated. Excavation of contaminated soil
in the tank field was completed just before the storm struck and the Oily Dirt Pile SWMU
80 was removed as well. A total of 38 roll off containers of removed soil were stored on
the East Hill [near the regulated units], one of the highest areas in the facility, and were
not affected by the storm surge. The HSWA corrective action scheduled at the North
Canal [part of the storm water system] had not yet begun, and will have to be delayed.
ChevronTexaco's large [140 acre, 200 million gallon] hurricane surge lagoon was
overtopped [incoming] by the storm surge, but the dike held and there was no apparent
release to the adjacent Grand Bay National Wildlife Refuge and the National Estuarine
Research Reserve [NERR], However, the large lagoon took on salt water from the surge,
which may affect the freshwater wildlife in the lagoon. The lagoon has been
characterized as an 'attractive nuisance" for wildlife and is the subject of an ongoing
Ecological Risk Assessment. Overall, the flooding was not as bad at the facility as
Hurricane George in 1998.

No adjacent housing areas were located on the aerial imagery. This facility is
located in Figure 3.

First Chemical Corporation - Pascagoula

First Chemical Corporation (FCC) has operated since 1967, manufacturing
numerous and sundry chemicals. A 1988 RFA identified approximately 30 SWMUs and
Areas of Concern (AOCs). The recently completed RCRA Facility Assessment (RFA)
expanded that number to greater than 65. FCC has conducted several investigations at
the facility over the years, with the most recent study being completed in 2004. First
Chemical was purchased in 2002 by DuPont, and it is operated as a wholly owned
subsidiary.

Shallow groundwater at the site (<15 ft bgs) has been impacted by various
contaminants; predominantly aniline, benzene, nitrobenzene, and toluene. The primary
sources of groundwater contamination are a former wastewater treatment pond (Pond 3)
and associated former effluent ditch. Miscellaneous leaks and minor releases have also

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contributed. The facility has monitoring and recovery systems in place, and they are
designing enhancements to the groundwater recovery system. The design should be
completed in early 2006, with installation possibly completed within 2006.

Hurricane Katrina Impacts

The facility did not suffer heavy damage, and there were no reported releases.
Two tanks were damaged, but the contents are being transferred to temporary storage
tanks. The facility will be out of operation for perhaps several weeks. A Publicly-
Owned Treatment Works (POTW) to which the facility pipes its partially treated effluent
was damaged, however, and it may be out of commission for "months". The facility will
require some means of disposing of its wastewater if the POTW is not online by the time
FCC is ready to go live.

No adjacent housing areas were located on the aerial imagery. This facility is
located in Figure 3.

Toxic Release Inventory (TRI) Facilities:

The following information is derived from the TRI website
(http://www.epa.gov/tri/): The Toxics Release Inventory (TRI) is a publicly available
EPA database that contains information on toxic chemical releases and other waste
management activities reported annually by certain covered industry groups as well as
federal facilities. This inventory was established under the Emergency Planning and
Community Right-to-Know Act of 1986 (EPCRA) and expanded by the Pollution
Prevention Act of 1990.

Information about these facilities is limited, but incidents are known to have
occurred due to the effects of Hurricane Katrina. Region 4 On-Scene Coordinators
(OSCs) have responded to incidents at the following facilities:

Omega Protein - Moss Point

No adjacent housing areas were located on the aerial imagery. This facility is
located in Figure 4.

Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington

No adjacent housing areas were located on the aerial imagery. This facility is
located in Figure 5.

Ershigs Fiberglass - Biloxi

Housing was noted to the northwest, west and south in the aerial imagery. This
facility is located in Figure 6.

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Tier II Facility:

The Emergency Planning and Community Right-to-Know Act of 1986 (EPCRA)
has a requirement for facilities exceeding the EPCRA Chemicals and Reporting
Thresholds specified in Sections 3 11/3 12 of the Act to submit a Tier II form. Tier II
forms require basic facility identification information, employee contact information for
both emergencies and non-emergencies, and information about chemicals stored or used
at the facility:

•	The chemical name or the common name as indicated on the Material Safety Data
Sheet (MSDS);

•	An estimate of the maximum amount of the chemical present at any time during
the preceding calendar year and the average daily amount;

•	A brief description of the manner of storage of the chemical;

•	The location of the chemical at the facility; and

•	An indication of whether the owner of the facility elects to withhold location
information from disclosure to the public,

Mississippi Phosphates - Pascagoula

Mississippi Phosphates Corporation is located at 601 Highway 611 Pascagoula,
MS and employs approximately 220 people. More than 900,000 tons of diammonium
phosphate (DAP) are produced at the complex each year. Nearly two-thirds of this
product is exported, mainly to China and India. Mississippi Phosphates Corporation is a
member of the Phosphate Chemical Export Association, Inc., (PhosChem) which handles
the export sales of the company's DAP. Its deep-water port facility on the Gulf of
Mexico allows Mississippi Phosphates to load ships for export directly from the plant
site. MS Phosphates imports phosphate rock from the country of Morocco.

Data from Region 4 OSCs indicates a leak of anhydrous ammonia from an above
ground storage tank. This is a large facility that had the potential to release hazardous
constituents beyond its" operational perimeter.

No adjacent housing areas were located on the aerial imagery. This facility is
located in Figure 3.

Naval Construction Battalion Center:

Naval Construction Battalion Center (NCBC) - Gulfport. NCBC Gulfport is
located in the western part of the City of Gulfport, in Harrison County, Mississippi,
approximately two miles north of the Gulf of Mexico. The off-base Area of Concern
(AOC) is located immediately downgradient (north) of Outfall 3.

The source area of dioxin contamination for the off-base AOC is the Herbicide
Orange Storage Area, designated as Site 8, at NCBC Gulfport. Between 1968 and 1977,
Site 8 was used by the United States Air Force (USAJF) as a storage area for drums
containing the herbicide Agent Orange, also known as Herbicide Orange, prior to being
shipped to Vietnam. Occasional spills and drum ruptures occurred during storage and

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handling of the Herbicide Orange. Dioxin migration has occurred primarily through
erosion of dioxin-contaminated soil and sediment from Site 8 and its transport
downstream via ditches and canals to a small wetland area at Turkey Creek. This
wetland was in the process of being cleaned up (80% completion) when Katrina occurred,
and there is a possibility that flooding may re-contaminated the remediated area.

Four sediment samples were collected by SESD in November from an outfall that
may have been contaminated with PCBs prior to the Katrina event.

Housing is located immediately adjacent to the wetland. This facility is located in
Figure 7.

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2.0 SAMPLING/DATA QUALITY OBJECTIVES

2.1 Data Quality Objectives

The Data Quality Objectives (DQO) process for Superfund was used in
developing the QAPP, in accordance with the Guidance for the DQO Process (EPA
QA/G-4, 2000). DQOs are useful in identifying the study objectives and decisions to be
made and the criteria by which the data will be assessed. These data are then used for
decision making.

DQOs were established prior to data collection and integrated with the project
planning process so that sufficient data of known quality are collected to support sound
decision making. DQOs are developed using an interactive approach to decision-making
based on detailed EPA guidance. The steps are:

• Problem statement

• Identify the decisions

• Identify the inputs into the decision

• Define the boundaries of the study

• Develop decision rules

• Specify tolerable limits on decision errors

• Optimize the design for obtaining data

2.1.1 Problem Statement

The initial step in the DQO process is to define the problem so that the focus of
the investigation will be clear. During the landfall of Hurricane Katrina, a massive storm
surge flooded extensive portions of Hancock, Harrison and Jackson Counties in the Gulf
Coast of Mississippi. Within this area are located many hazardous waste facilities. It
was not known what effect, if any, the storm surge had on these facilities and the
surrounding areas, with respect to release and dispersion of hazardous materials and
chemicals, particularly to residential settings and sediment. The facilities selected for this
investigation have had indications of a potential release to surrounding soils, or
conditions prior to Katrina make a release to surrounding soils or sediment possible. The
problem is identifying these potential releases to surrounding soils and sediments. It
must be strongly emphasized that this investigation is not intended to provide a
comprehensive assessment of potential releases beyond the operational perimeters of
these facilities. Rather, it is intended to provide a first look at these areas post-Katrina.

2.1.2 Identify the Decision

The purpose of this DQO step is to identify the decisions that must be supported
with the collected data. This helped to define the objectives of the field investigation.
The decision needed was to determine what areas of the Mississippi Gulf Coast, in
immediate proximity to the hazardous waste facilities, may be the site of a potential

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release of hazardous materials to surrounding soils and\or sediments. SESD prepared this
report detailing the results of the investigation to provide the supporting data for these
decisions.

2.1.3 Decision Inputs

This step is used to identify the information needed to support the decisions. The
primary inputs needed to support the decisions are surface soil and sediment samples.
Analytical results used in this decision making process were definitive laboratory data,
obtained from analysis by a contract laboratory obtained through the EPA's Contract
Laboratory Program (CLP lab). All samples were analyzed for metals (including
mercury), volatile organic compounds and semi-volatile organic compounds, including
pesticides and PCBs, with the exception of samples from NCBC Gulfport where samples
were analyzed for PCBs or dioxins only. Samples from the DuPont DeLisle facility were
analyzed for dioxins in addition to these parameters. Samples from the Chevron Refinery
- Pascagoula, First Chemical, and MS Phosphates complex were also analyzed using
gamma spectroscopy in addition to the parameters listed above.

Surface soil samples were composites comprised of soil from the 0" to 3" interval
at each aliquot location. The sample for volatile organic compounds was collected from
the centermost aliquot. Sediment samples were collected from ditches or other surface
water conveyances as grab samples in the vicinity of each site to determine if releases
occurred via these pathways.

2.1.4 Study Boundaries

The purpose of this step is to identify the boundaries of the study. The media of
interest was surface soils and sediments adjacent to the selected RMP, Tier II and TRI
facilities, as well as the wetland north of NCBC Gulfport. The study boundaries are
defined below.

Study Area - The study area was the portions of Hancock, Harrison and Jackson
counties flooded by the storm surge associated with Hurricane Katrina. Within the larger
study area are the selected facilities. For each of the identified sites, the area to be
investigated consisted of soils and/or sediments near the facility (but outside the
perimeter), including ditches or storm water conveyances that were present.

Sample Depth - Soil samples were collected from 0" to 3" below ground surface
depth. Samples collected from ditches were from a similar interval.

Temporal Boundaries -The field investigation was conducted the week of
October 3, 2005. All efforts were made to obtain the quickest possible turnaround times
on the analytical results (consistent with good laboratory practices) to expedite decision
making.

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Physical Boundaries - No sampling was conducted beneath any concrete or
asphalt paved areas or from under any structures. Also, no samples were collected in the
immediate vicinity of any downed power lines or under any unstable structures that may
have posed a collapse hazard to the sampling team. Several sample locations were
moved varying distances from the original proposed locations due to on-site conditions
(see Table 1 in Appendix B for a description and rationale of sample boundaries).

2.1.5 Decision Rule

The Technical Services Section in the Superfund Remedial and Technical
Services Branch has prepared a decision matrix to be used in determining if a potential
release has occurred (Appendix C). The results of this matrix evaluation are found in
Section 7.0 of this report.

2.1.6 Error Limits

Because of inherent variability introduced through sample collection, mixing,
storage, transportation, and analysis, it is important to specify the acceptable decision
error rates. Decision errors were reduced by using standard, published protocols for
sampling and analytical procedures. Sampling protocols followed the Environmental
Investigations Standard Operating Procedures and Quality Assurance Manual
(EISOPQAM) while analytical procedures followed the current CLP Statement of Work
(SOW), the regional SOW for dioxins, and the NAREL (National Air and Radiation
Environmental Laboratory) GAM-01 for gamma spectroscopy.

2.1.7 Optimize Sampling Design

The final step in the DQO process is the development of a sampling design that
takes into account data needs, key decisions, and environmental variables, such as
physical and site constraints, and how the spatial and temporal boundaries of the
contamination and population at risk will be identified. The work plan, as included in the
QAPP, was developed based on the integration of aerial imagery of the affected areas
(pre-Katrina) and the EPA facility registry. Due to the time-critical nature of the
investigation, a reconnaissance of each area was not practical or possible. As such, each
sample team approached each site with generic protocols for sampling. As stated in
Section 3.3, up to 5 samples were collected adjacent to each facility. Sediment samples
were also collected from ditches or other conveyances that left the property. It must be
noted that the proposed sample locations were selected using 1:24,000 topographic maps
and quarter-quad digital orthographic quads. These maps were the most current
available, but are still several years old. In addition, they may be inaccurate by as much
as 20' to 40'.

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Samples were collected on an authoritative basis, from areas deemed most likely
to be impacted. Specifically, soils were sampled adjacent to facility perimeters and
sediment samples from drainage pathways. Sampling locations are presented in Table 1
of Appendix B.

DuPont DeLisle. see Figure 8

Two grab sediment samples were collected from ditches draining the facility to
St. Louis Bay. Three additional composite surface soil samples were collected between
the facility and a residential area immediately north of the facility.

Chevron Refinery - Pascagoula. First Chemical Corporation, and Mississippi
Phosphates, see Figure 9

Because these selected facilities are adjacent to each other, sampling occurred
around these facilities as a unit. Grab sediment samples were collected from ditches
draining to Bayou Cassotte, Bangs Lake, and the Gulf of Mexico. In addition, composite
surface soil samples were collected north and south of the facility complex. Finally, this
report includes data from two sediment sampling stations established in Bayou Cassotte
by the Ecological Assessment Branch (EAB), Water Quality Studies of Bays in Coastal
Mississippi (EPA 2005), the week prior to this investigation.

Omega Protein, see Figure 10

Three grab sediment samples were collected from the north bank of the
Escatawpa River, two at the facility and one downgradient. No upland soil samples are
proposed for this facility because Morton International (which was not listed for sampling
in this effort) is immediately north. In addition, this report contains data from a sediment
sampling station established by EAB the week prior to this investigation in the Escatawpa
River downstream of Omega Protein.

Port Bienville Industrial Park (Polvchemie. Inc.). see Figure 11

Grab sediment samples were collected at the three indicated locations to
determine if a potential release to the waterway occurred as the storm surge receded.
Two composite surface soil samples were collected at the indicated locations to
determine if contaminants may have moved further inland from the facility on the rising
flood waters.

Ershigs Fiberglass, see Figure 12

Four composite surface soil samples were collected as shown, to determine if
contaminants may have been deposited between the facility and nearby housing. An
additional grab sediment sample was collected from a small inlet draining to Biloxi Bay.

1 1

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Naval Construction Battalion Center (NCBC) Gulfport. see Figure 13

Five grab sediment samples were collected as shown, to determine if the wetland
may have become re-contaminated during the storm surge. These samples were
recollected by SESD in November due to problems with the sample analysis. At the
same time four sediment samples were collected from an NCBC outfall that may have
been contaminated with PCBs from an earlier, non-Katrina related incident.

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3.0 INVESTIGATION MANAGEMENT PLAN

3.1 Field Project Responsibilities

The overall field investigation/sampling phase of the project and any field
decisions were the responsibility of the Field Project Leader who was responsible for the
following field activities:

• Ensure that all field activities were communicated and coordinated with the
Project Leader.

• Monitoring overall field project quality control.

• Coordinating field scheduling of work with other Section and Division
activities.

• Overseeing and managing field technical resources including non-sampling
field activities.

The site Health and Safety Officer (HSO) was responsible for monitoring the
health and safety of the sampling/investigative personnel. In addition to the Field Project
Officer and HSO, five other staff persons were involved in the field operations for the
investigation. All field investigators are required to have 40 hours of hazardous waste
site safety training, and specific knowledge and expertise of sample collection and safety
techniques in accordance with the Region 4 EP A Environmental Investigations Standard
Operating Procedures and Quality Assurance Manual (EISOPQAM), November 2001.

3.2 Site Control and Access

Access arrangements for RMP facilities were made by Lael Butler, Chief, South
Programs Section, RCRA Programs Branch. Access arrangements for TRI and Tier II
facilities were made by Fred Sloan. Access to the NCBC was arranged by Michelle
Thornton.

3.3 Sample Collection and Handling Procedures

All samples were collected, containerized, preserved, handled, and documented in
accordance with the EISOPQAM. A copy of the manual, in addition to the site-specific
Health and Safety Plan, was maintained by the field project leader for reference during all
phases of the field sampling activities.

The surface soil samples were collected as composite samples, with the number of
aliquots and pattern determined by the site conditions, using stainless steel hand augers.
The pattern size was appropriate to characterize the area in question. The central aliquot
location for each sample was located using GPS to at least one meter accuracy. Each
aliquot was comprised of the 0" to 3" below ground surface interval. All grass, roots and
other vegetative material, as well as small rocks or stones, were removed from the sample

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matrix during sample mixing, prior to containerization. It should be noted that sediment
deposited by the storm surge was present in the collected samples.

Sediment samples were collected using stainless steel scoops, stainless steel
spoons and/or stainless steel hand augers.

Soil samples were collected as described in Section 2.1.7, using hand augers,
spoons, or scoops as appropriate, and the aliquots were thoroughly mixed in glass pans.
Samples for volatile organic compound analyses were collected prior to mixing with
minimum disturbance from the central aliquot in Encore® sample containers using EPA
Method 5035. After mixing, the samples were placed in the appropriate containers and
placed on ice, as specified in Appendix A of the Region 4 EISOPQAM.

3.4	Sample Analysis and Validation

All samples were analyzed for metals, volatiles, semi-volatiles, pesticides and
PCBs, in accordance with the current Contract Laboratory Program Statement of Work,
again with the exception of the NCBC Gulfport facility where samples were analyzed for
dioxins or PCBs only. Samples from the DuPont DeLisle facility were analyzed for
dioxins in addition to these parameters. Samples from the Chevron Refinery -
Pascagoula, First Chemical, and MS Phosphates complex were also analyzed for
Radium-226 and radionuclides using gamma spectroscopy in addition to the parameters
listed above.

By using sampling procedures as outlined in the Region 4 EISOPQAM errors
introduced in the decision making process were minimized.

3.5	Chain of Custody

All chain-of-custody and record keeping procedures were in accordance with the
EISOPQAM. Chain-of-custody procedures are comprised of the following elements; 1)
maintaining sample custody and 2) documentation of samples for evidence.

As defined in the EISOPQAM, a sample or other physical evidence is in custody

if:

•	it is in the actual possession of an investigator;

•	it is in the view of an investigator, after being in their physical possession;

•	it was in the physical possession of an investigator and then it was secured to
prevent tampering; and/or

•	it is placed in a designated secure area.

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3.5.1	Sample Labels

Sample labels were prepared and affixed to each sample container sent to the CLP
laboratory. The labels were prepared using waterproof, non-erasable ink as specified in
Section 3 of the EISOPQAM.

3.5.2	Sample Custody Seals

The samples were sealed as soon as possible following collection as specified in
the EISOPQAM. The custody seal bears the date and the initials of the sample custodian
at the time it was sealed.

3.5.3 Chain-of-Custody Record

The field Chain-Of-Custody Record is used to record the custody of all samples
sent to the laboratory. All of these samples were accompanied by a Chain-Of-Custody
Record. The Chain-Of-Custody Record documents transfer of custody of samples from
the sampler/sample custodian to another person, the laboratory, or other organizational
elements. To simplify the Chain-of-Custody Record and eliminate potential litigation
problems, as few people as possible should have custody of the samples or physical
evidence during the investigation.

The Chain-Of-Custody Record also serves as a sample logging mechanism for the
laboratory sample custodian. A Chain-of-Custody Record was completed for all samples
collected for this investigation. A separate Chain-of-Custody Record was used for each
final destination or laboratory utilized during the investigation.

For samples split with a facility, a Receipt for Sample form was completed and

signed.

3.6 Station and Sample Identification

Sample identification numbers were assigned using the following format:

XXX##YYZ, where:

XXX is an identifier for the RMP, Tier 2, TRI, or NCBC facility

## indicates surface soil (SF) or sediment SD

YY indicates the sample location number, i.e., 01 for the facility location

Z identifies splits or duplicates: "S" is split; "D" is duplicate

A split sample is a sample comprised of two samples, the primary sample and the
designated split sample, that are collected from the same sample material that has been
homogenized in a glass pan prior to filling of the sample containers. Assuming a well
mixed sample, a split helps evaluate both the field and laboratory procedures. A

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duplicate sample is a co-located sample, usually collected less than six inches from the
primary sample at a location and is collected to show variability of the matrix sampled.

3.7	Site Mapping

The locations of all samples were logged using a GPS unit capable of one meter
accuracy, as specified in Section 2.1.7,

3.8	Investigation Derived Waste (IDW)

The following identifies types of non-hazardous IDW that were generated during
the investigation and their disposition:

• Gloves, paper towels, and other miscellaneous trash generated during the
investigation were bagged and placed in a dumpster for disposal at a Class D
landfill. It is not anticipated that this material will constitute a significant
threat to human health and the environment.

3.9	Sample Containers

Sample containers were obtained from the SESD Field Equipment Center in
Athens, Georgia. These containers complied with the requirements specified in
Appendix A of the EISOPQAM. Table 2 (Appendix B) lists the container types and
numbers used.

It should be noted that time constraints did not allow for the normal QA/QC
checks for these pre-cleaned sample containers as specified in the EISOPQAM.

3.10	Investigation Schedule

The field investigation began October 3, 2005, and ended October 7, 2005.
During the investigation SESD:

•	Collected soil and sediment samples from the identified properties within the
area affected by the Katrina storm surge.

•	Collected location data for sampling points using GPS techniques (Section
3.7).

•	Collected and properly disposed non-hazardous IDW.

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4.0

SAMPLING DESIGN AND RATIONALE

Surface soil and sediment samples were collected during this field investigation.

4.1 Sampling Design

Seven RMP, Tier II, and TRI facilities were selected for this investigation. In
addition, one superfund site that had the potential to re-contaminant a remediated portion
of the site was also selected. Three to eight sampling stations were selected for each site
(or complex of sites). These sampling stations were selected to provide preliminary
information on potential releases to soils and sediments beyond the perimeters of the
facilities.

4.2 Data Validation/Usability

Analyses for metals. Volatile Organic Compounds (VOCs), semivolatiles,
pesticides and PCBs were performed by CLP laboratories. This data was validated
according to the National Functional Guidelines for Organic Data Review, Office of
Solid Waste and Emergency Response (OSWER) 9240.1-05-A-P (October 1999), the
National Functional Guidelines for Inorganic Data Review, OSWER 9240.1-45 (October
2004) and Region 4's Data Validation Standard Operating Procedures for Contract
Laboratory Program Routine Analytical Services, Revision 2.0 (January 1999).

The dioxin/furan analyses were performed by a laboratory contracted to EPA.
Validation of the dioxin data will be performed by ESAT, using the National Functional
Guidelines for Dioxin Data Review, OSWER540-R-02-003 (August 2002) and Region
4's Data Validation Standard Operating Procedures for Dioxin Data Version 3.0 (May
2002) documents. The dioxin data will consist of a Level 4 - CLP type data package that
contains the Chain-of-Custody paperwork, instrument raw data, initial and/or continuing
calibration data/curves, bench sheets/sample preparation information, QA/QC
data/information, and case narrative detailing any problems associated with this data.

The gamma spectroscopy analyses were performed by the National Air and
Radiation Environmental Laboratory (NAREL), using method NAREL GAM-01.

Review and validation of all data (including screening data) from samples
collected during this investigation was completed in an expeditious manner, utilizing
quick turnaround times consistent with good laboratory practices.

4.3 Data Management/Document Control

Project files will be maintained in accordance to the EISOPQAM. The field
project leader will review the file at the conclusion of the project to ensure completeness.
Laboratory data was released to the Chief, Technical Services Section as it became
available.

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5.0 QUALITY ASSURANCE

Quality assurance (QA) procedures must begin in the planning stage and continue
through sample collection, analyses, reporting and final review. The methods that were
used to ensure data quality are discussed below.

5.1 Organization and Responsibilities

The field project leader has overall responsibility for field QA. Off-site
laboratory analyses for samples collected during the investigation were conducted by the
CLP. The precision, comparability and accuracy of sample analyses were addressed in
accordance with the Analytical Support Branch laboratory Operations and Quality
Assurance Manual (ASBLOQAM).

5.2 Field QA/QC Samples

5.2.1 Matrix Spike/Matrix Spike Duplicate

Samples for laboratory quality control analyses matrix spike/matrix spike
duplicate (MS/MSD), were designated as specified in the EISOPQAM. One MS/MSD
sample was designated for every 20 samples split to the CLP laboratory, two total for this
investigation.

5.2.2 Population Variability - Duplicate Samples

Co-located duplicate samples were collected to provide data for an assessment of
the variability of constituents within the designated areas. Following collection of the
initial sample that is to be duplicated, the sample was re-collected with clean equipment.
The letter 'D' was appended to the sample ID used for the primary sample at the
duplicated location for the duplicate containers being sent to the laboratory (see Section
3.6). One duplicate sample was collected per site or complex of sites. The data is located
in the Data Summary Tables in Appendix B. There is not enough data for a valid
statistical interpretation of this data, but examining the data indicates that some
heterogeneity is present in these samples. This is likely a result of the samples being to
some extent a mixture of pre-Katrina soil and sediment deposited post-Katrina. To
answer this definitively is beyond the scope of this investigation. However, as seen
below, the results of the split sampling indicate that this may be the case.

5.2.3 Sample Handling - On-Site Splits

Split samples were collected to assess sample handling variability. Following
collection and mixing of the sample that was to be split, the sample was apportioned into
two identical sets of sample containers. The letter 'S' was appended to the sample ID

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used for the primary sample to indicate the split sample being sent to the laboratory (see
Section 3.6). One split sample was to be collected per site, or complex of sites, two were
inadvertently not collected. The data is located in the Data Summary Tables in
Appendix B. As with the duplicate samples discussed above, there is not sufficient data
for a valid statistical interpretation of this data. However, examining the data indicates
that samples were properly mixed in the field, providing a homogenous sample for lab
analysis. Again, a definitive answer is beyond the scope of this investigation.

5.2.4 Trip Blanks

Four trip blanks were collected during this investigation. Trip blanks provide a
check on the handling of soil samples collected for volatile organic compounds (VOCs)
analyses. The results are shown in Table 8, Appendix B. Low levels (11 to 17 ug/kg) of
acetone were reported in three of the four blanks. Acetone is a common laboratory
contaminant.

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6.0 INVESTIGATION RESULTS

The field investigation teams noted a layer of what appeared to be newly
deposited sediment at the various sampling locations. This was apparently a result of the
Katrina storm surge, but a factual determination of this was beyond the scope of this
investigation. Visual estimates of the thickness of this layer of material ranged from 0"
to approximately 2", and was generally less than Vi". Where present, this material was
included in the samples collected.

The following sections summarize the results of analysis of samples collected at
the facilities or sites selected for the Post-Katrina soil/sediment investigation. Figures 8
through 13, contained in Appendix A of this document, show the locations of these
samples. The analytical data summary tables provided for each facility or site are
comprised of only the compounds or analytes that were detected (Appendix B). The
complete data, included in Appendix C of this report, contain the detected compounds as
well as those analyzed for but not detected, with the minimum quantitation limits for the
undetected compounds and analytes. Appendix C also contains analytical data for
tentatively identified compounds (TICs), unknown compounds, and petroleum products,
where these were detected.

The following is a list of data qualifiers used in the analytical data summary tables
accompanying the presentation of the investigation results.

U Anafyte not detected at or above reporting limit.

J Identification of anafyte is acceptable; reported value is an estimate.

N Presumptive evidence anafyte is present; anafyte reported as tentative
identification.

UJ Anafyte not detected at or above reporting limit. Reporting limit is an
estimate.

NJ Presumptive evidence anafyte is present; anafyte reported as tentative
identification. Reported value is an estimate.

R Presence or absence of anafyte can not be determinedfrom data due to
severe quality control problems. Data are rejected and considered
unusable.

A Anafyte analyzed in replicate. Reported value is "average " of replicates.

/2 constituents or metabolites of technical chlordane.

6.1 DuPont - DeLisle

Three surface soil and two sediment samples were collected at five locations, as
shown on Figure 8. These samples were analyzed for volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, metals, and
dioxins. Table 3 in Appendix B summarizes the results of analysis of these samples.
Appendix C contains the data sheets with all results, including tentatively identified
compounds (TICs) and quantitation limits for analytes that were not detected.

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A small diesel fuel spill was noted in the area of sample DU-SD-02 by the
sampling team.

6.2 Chevron - Pascagoula, First Chemical, Mississippi Phosphates

Three surface soil and seven sediment samples were collected at ten locations, as
shown on Figure 9. These samples were analyzed for volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, metals, and
radionuclides (samples BC2 and BC4 were collected as part of another investigation, no
radionuclide analyses were performed on these samples). Table 4 in Appendix B
summarizes the results of analysis of these samples. Appendix C contains the data
sheets with all results, including tentatively identified compounds (TICs) and quantitation
limits for analytes that were not detected.

6.3 Omega Protein

Three sediment samples were collected at three locations, as shown on Figure 10.
These samples were analyzed for volatile organic compounds (VOCs), semi-volatile
organic compounds (SVOCs), pesticides/PCBs, and metals. Table 5 in Appendix B
summarizes the results of analysis of these samples. Appendix C contains the data
sheets with all results, including tentatively identified compounds (TICs) and quantitation
limits for analytes that were not detected.

6.4 Port Bienville Industrial Park (Polychemie, Inc.)

Two surface soil and three sediment samples were collected at five locations, as
shown on Figure 11. These samples were analyzed for volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, and metals. Table

6 in Appendix B summarizes the results of analysis of these samples. Appendix C
contains the data sheets with all results, including tentatively identified compounds
(TICs) and quantitation limits for analytes that were not detected.

6.5 Ershigs Fiberglass, Inc.

Three surface soil and two sediment samples were collected at five locations, as
shown on Figure 12. These samples were analyzed for volatile organic compounds
(VOCs), semi-volatile organic compounds (SVOCs), pesticides/PCBs, and metals. Table

7 in Appendix B summarizes the results of analysis of these samples. Appendix C
contains the data sheets with all results, including tentatively identified compounds
(TICs) and quantitation limits for analytes that were not detected.

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6.6 Naval Construction Battalion Center

Five sediment samples were collected at the locations indicated on Figure 13.
These samples were analyzed for dioxins only. An additional four sediment samples
were collected in November from an outfall that may have been contaminated from a pre-
Katrina event. These samples were analyzed for PCBs only. This data will be released in
an addendum to this report when it is available.

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7.0 IMPACT EVALUATION

The Technical Services Section (TSS) of the Superfund Remedial and Technical
Services Branch has reviewed the data for these sites, in consultation with the Regional
programs. TSS has made a preliminary assessment regarding whether surface soil or
sediments may have been adversely impacted by the Katrina storm surge. In particular,
TSS was asked to evaluate whether there are any significant post-Katrina impacts from
potential releases of hazardous substances. The question is whether or not potential
releases of hazardous substances may have occurred or (in the case of NCBC) whether
known environmental contamination associated with the sites has been re-distributed. It
must be understood however, that a definitive attribution to sites cannot be made, nor can
this study determine if observed contaminants are present due to the effects of Katrina, or
were present prior to Katrina.

Evaluating the sampling data to determine if there was an off-site impact from
Hurricane Katrina posed a challenge due to the scarcity of pre-existing sampling data and
supporting information that could be used for data interpretation. EPA's conclusions
regarding the potential impact of the hurricane on these sites are based on a comparison
of post-hurricane data to available past sample data collected during facility
investigations or routine monitoring activities. In addition, the results were compared to
EPA Region 9 Preliminary Remediation Goals (PRCs) to determine if conditions at the
sites might represent previously unrecognized risks to human health and the environment.
EPA Region 9 PRCs (available at:

http://www.epa.gov/region9/waste/sfund/prg/index.html) are conservative risk-based
concentrations based on long-term exposures in either a residential or
commercial/industrial setting. They are considered by EPA to be protective for people
(including sensitive groups) over a lifetime. The PRCs are not clean up standards, but
used to assist EPA scientists and others in initial screening-level evaluations of
environmental measurements.

A typical background level for PAHs was based on a value of 45 mg/kg that EPA
Region 4 considers representative of anthropogenic urban background based on a
compilation of literature sources. For further comparison. Figure 14 (Appendix A)
shows urban background ranges of carcinogenic P AHs from a number of literature
sources.

Sediments were screened against soil benchmarks because no similar benchmarks
existed for sediments. Region 4 normally considers long-term human exposure to
sediments that are underwater to be minimal due to limited opportunity for frequent
contact of significant duration. Several samples contained unidentified organic

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compounds reported by the laboratory. Because the identities of the compounds are not
known, they could not be screened against levels protective of human health.

7.1 DuPont DeLisle - Pass Christian, Mississippi

The samples for dioxin analysis were recollected due to uncertainties with the
quality of the data from the original laboratory. This data will be issued as an addendum
when it becomes available.

7.1.1 Results

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead,
magnesium, manganese, nickel, potassium, vanadium, and zinc were detected in the soil
samples collected from the DuPont DeLisle facility from the dirt road and ditch. No
semi-volatile organic compounds or PCBs were detected in soils collected from the
DuPont DeLisle facility. Acetone was detected in several samples. Acetone is a
common laboratory contaminant, and detections of low levels such as this one are not
indicative of a release. Low levels of the pesticides DDD, alpha-chlordane, dieldrin,
endrin ketone, and methoxychlor were also in these samples.

Sediments

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead,
magnesium, manganese, nickel, potassium, selenium, sodium, thallium, vanadium, and
zinc were detected in sediments collected from the DuPont DeLisle facility. No PCBs
were detected in these samples. A few organic compounds were detected in sediments
collected from depositional areas outside the facility (see discussion below).

7.1.2 Discussion

No detected metals exceeded industrial PRCs. Samples in the vicinity of
residential development did not exceed residential soil screening values (PRCs). Facility
specific background data was available for the metals arsenic, lead, and chromium. The
detected concentrations of lead were slightly above the facility specific background value
(8.7 mg/kg) taken prior to hurricane Katrina. Of the three samples the maximum value for
lead in soil was 26 mg/kg. The maximum concentration was measured at sample location
DU-SF-04, lower than previously detected. The maximum detected concentration of lead
was below the preliminary remedial goal for industrial exposure of 800 mg/kg.

Concentrations of Metals Detected in Soils Compared to Site-Specific Background

Chemical

Maximum Detected

Site-Specific Background

Concentration, mg/kg

Prior to Katrina, mg/kg

Arsenic

1.5

7.4

Lead

26J

8.7

Chromium

1 1

36.5

-------
Sediments were screened against soil benchmarks because no similar benchmarks
exist for sediments. Region 4 normally considers long-term human exposure to sediments
that are underwater to be minimal. The sediments in question are in a depositional area.
They are not in an area where people are likely to come in contact with the sediments.

A few organic compounds were detected in sample DlJ-SD-02, which was
collected in a depositional area outside the facility. 1,1 -Biphenyl was detected at 1100
ug/kg, 2-methylnaphthalene was detected at 4100 ug/kg, naphthalene was detected at
1100 ug/kg, phenanthrene was detected at 1200 ug/kg, anthracene was detected at 110
ug/kg, and pyrene was detected at 130 ug/kg. None of the values were considered
elevated with respect to protection of human health. Three of the chemicals (1,1-
biphenyl, naphthalene, and 2-methylnaphthalene) are volatile chemicals that are not
expected to persist in the environment for long periods of time. These chemicals degrade
rapidly in the environment and are not of concern for long-term exposure to people. None
of the concentrations were greater than anthropogenic background EP A Region 4
considers typical of industrial/urban areas.

7.1.3 Conclusion

7.2 Chevron Pascagoula, First Chemical, Mississippi Phosphate -
Pascagoula, Mississippi

7.2.1 Results

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead,
magnesium, manganese, mercury, nickel, potassium, selenium, sodium, vanadium, and
zinc were detected in the soil samples. Low levels of pesticides heptachlor epoxide and
methoxychlor were also detected at in soil samples. No VOCs, SVOCs or PCBs were
reported. Samples were collected and analyzed for radionuclides. The primary
radionuclide of concern is Radium 226 (Ra 226).

Sediments

Aluminum, arsenic, barium, beryllium, calcium, chromium, cobalt, copper, iron,
lead, magnesium, manganese, nickel, potassium, selenium, sodium, vanadium, and zinc
were detected in sediment samples. Acetone and toluene were detected at low levels in

-------
two samples. Acetone and toluene are common laboratory contaminants, and detections
of low levels such as these are not indicative of a release. Low levels of the pesticides
DDE, gamma chlordane, heptachlor epoxide, and methoxychlor were also detected in
sediment samples. No PCBs were reported. Samples were collected and analyzed for
radionuclides. The primary radionuclide of concern is Ra226.

7.2.2 Discussion

There were no levels for Ra226 or any other radionuclide that exceeded expected
background levels. From the data reported there were no levels that indicated a potential
release of radioactive contamination.

Sediments were screened against industrial PRCs. Region 4 normally considers
long-term human exposure to sediments that are under water to be minimal. The
sediments in question are in ditches that serve the storm water drainage and outfall areas
of the sampled facilities. They are not in areas where people are likely to come in contact
with the sediments. The maximum detection of total chromium (95 mg/kg) at sample
CFM-SD-05 exceeded the industrial PRC (64 mg/kg) but was below the 1E-05 (1 in
100,000) risk level (640 mg/kg). The maximum detected level of arsenic at sample CFM-
SD-06 (10 mg/kg) was above the industrial PRC (1.6 mg/kg) but below the in 1E-05 risk
level (100 mg/kg). Both chromium and arsenic concentrations fell within a risk range of 1
in 1,000,000 to 1 in 10,000 risk over background of an individual developing cancer over
a lifetime from long-term exposure to those concentrations, which EPA has found
acceptable in other regulatory and remedial contexts. None of the remaining analytes
detected in soil or sediment exceeded industrial PRC soil screening levels.

Baseline data collected prior to hurricane Katrina was available, including recent
sediment data from Bayou Cassotte, sediment samples from the wetlands south of the
Chevron Pascagoula operational area, and recent sediment sampling data from outfall
areas of the Mississippi Phosphates Corp.

Facility specific background data was available for the metals aluminum, arsenic,
barium, beryllium, calcium, chromium, cobalt, iron, lead, magnesium, manganese, nickel,
potassium, selenium and vanadium. Sediment sampling from Bayou Cassotte also
included the metals antimony, cadmium, copper, silver, sodium, thallium, mercury and
zinc in addition to the facility-specific metals data. Sediment and soil data were
compared to relevant baseline data. Data that exceeded baseline sampling are shown
below:

-------
Metals Detected in Sediment/Soils Exceeding Site-Speci

ic Background

Chemical

Maximum detected
concentration,

mg/kg

Location

Site-Specific
Background Prior to
Katrina, mg/kg

Aluminum

16000

CFM-SD-06

8200 (Bayou Cassotte)

Beryllium

1.3

CFM-SD-06

1.1 (Chevron)

Calcium

43000

CFM-SD-06

7400 (Bayou Cassotte)

Chromium

CFM-SD-05

29 (Chevron)

Cobalt

CFM-SD-06

8.7 (Chevron)

Lead

CFM-SD-07

16 (Chevron)

Nickel

CFM-SD-05/08

15 (Chevron)

Vanadium

590

CFM-SD-05

86 (Chevron)

Detected concentrations of aluminum, beryllium, calcium, cobalt, lead and nickel
were above levels detected in Bayou Cassotte and the wetlands South of Chevron prior to
hurricane Katrina. However, these samples (CFM-SD-06 and CFM-SD-07) were taken
from a ditch that collects surface runoff drainage from the Chevron facility and an area to
the south that had a history of industrial activity. The area where samples CFM-SD-06,
CFM-SD-07 and CFM-SF-08 were located is currently in a solid waste management unit
(SWMU).

Prior to Chevron acquiring this area, it was formerly used by the HK Porter
Company to manufacture refractory brick. During industrial activities, surface soil
became contaminated with various metals including magnesium and calcium. Later, this
area became part of the Owens Corning Glass Plant. Given the past history of industrial
use in the area, and that the sample was obtained from a drainage ditch that collected
surface runoff from areas impacted by current and previous industrial activity, it is not
surprising to see elevated levels of metals. It is likely that these metals concentrations
were pre-existing in the area and questionable whether they resulted from the impact of
hurricane Katrina.

Detected concentrations of chromium, nickel, and vanadium were identified in
sample CFM-SD-05, which was collected from a drainage ditch southeast of the Chevron
operational area. This ditch is part of an existing SWMU and on Chevron property. The
SWMU that this ditch drains is a hurricane retention pond known to contain vanadium in
soil and sludge. This is the only location where vanadium has been previously detected in
any significant quantity. Nickel has been used as a crude oil cracking catalyst and can be
found in the soil at several SWMUs within the plant. Therefore, it is unsurprising to
encounter elevated levels of vanadium, nickel or other metals in this ditch, and is unlikely
to constitute a hurricane Katrina-related impact.

7.2.3 Conclusion

In spite of several metals exceeding local baseline sampling data, the exceedances
are not significant enough to clearly indicate an impact due to hurricane Katrina in light
of the likelihood of pre-existing metals contamination in surficial soil and drainage ditch
sediments. All detected analytes were within a risk-range considered acceptable by EPA
in other regulatory contexts. It is unlikely that frequent and prolonged human contact

-------
with sediments under water in drainage ditches would occur. There does not appear to be
an indication of a potential release in the area of the facilities due to the effects of
Hurricane Katrina.

7.3 Omega Protein - Moss Point, Mississippi

7.3.1 Results

Sediments

Aluminum, antimony, arsenic, barium, beryllium, calcium, chromium, cobalt,
copper, iron, lead, magnesium, manganese, nickel, potassium, sodium, thallium, mercury,
vanadium and zinc were detected in these samples. Low concentrations of several semi-
volatile organic compounds and low levels of pesticides were also detected. One PCB,
PCB-1260, was reported at a concentration of 21J ug/kg in sample OP-SD-02. No
volatile organic compounds were reported.

7.3.2 Discussion

No pre-Katrina sampling data is available for the site, therefore there is
uncertainty about impact of the hurricane on the surrounding environment. Detected
analytes were compared to industrial PRC soil screening levels. Arsenic (2.2 mg/kg)
slightly exceeded the industrial PRC (1.6 mg/kg) at sampling point OP-SD-02, but was
below the 1E-05 risk level (16 mg/kg). Benzo(a)pyrene (1300 ug/kg) exceeded the
industrial PRC (210 ug/kg) at sample location OP-SD-01, but was below the 1E-05 risk
range. Both fell within a risk range of 1 in 1,000,000 to 1 in 10,000 risk over background
of an individual developing cancer over a lifetime from long-term exposure to those
concentrations, which EPA has found acceptable in other regulatory and remedial
contexts. None of the remaining analytes detected in soil or sediment exceeded industrial
PRC soil screening levels.

7.3.3 Conclusion

There is no clear indication of a release in the area of the Omega Protein facility
due to the effects of Hurricane Katrina. None of the reported analytes exceeded levels of
concern for exposure to contaminants in soil or sediment under a commercial/industrial
scenario.

7.4 Port Bienville Industrial Park (Polychemie, Inc.) - Pearlington, Mississippi
7.4.1 Results

Soils

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead,
magnesium, manganese, nickel, potassium, selenium, sodium, vanadium, and zinc were

-------
detected in the soil samples collected from the Polychemie, Inc. facility from the southern
portion of the site. No semi-volatile or volatile organic compounds were reported in
these samples. No PCBs were reported for these samples. Gamma chlordane was
detected in soil sample PO-SF-04 at 0.86J mg/kg.

Sediments

Aluminum, arsenic, barium, cadmium, calcium, chromium, cobalt, copper, iron,
lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were
detected in sediments collected from the Polychemie, Inc. facility. No pesticides or PCBs
were reported in these samples.

Several organic compounds were detected in sediments. One volatile organic
compound, acetone, was detected at 140 ug/kg in sample PO-SD-OID. Acetone is a
common laboratory contaminant, and detections of low levels such as this one are not
suggestive of a release. Ten PAH compounds were detected in Sample PO-SD-03. These
included benzo(a)anthracene, benzo(b)fluoranthene, benzo(ghi)perylene,
benzo(k)fluoranthene, benzo-a-pyrene, chrysene, fluoranthene, indeno (1,2,3-cd) pyrene,
phenanthrene, and pyrene. Levels of the PAHs ranged between 120 ug/kg for
benzo(ghi)perylene to 400 ug/kg for fluoranthene.

Unknown miscellaneous semi-volatile organic compounds were reported by the
CLP laboratory. The identities of the unknown compounds were not verified by the
laboratory.

7.4.2 Discussion

No facility specific background data was available for the metals detected in soils.
Arsenic detections exceeded the industrial PRC (1.6 mg/kg) at sample locations PO-SD-
01 and PO-SD-02 (18, 7.7 mg/kg), but were within a risk range of 1 in 1,000,000 to 1 in
10,000 risk over background of an individual developing cancer over a lifetime from
long-term exposure to those concentrations, which EPA has found acceptable in other
regulatory and remedial contexts. None of the other metals detected exceeded industrial
PRCs.

None of the concentrations of organic compounds exceeded industrial PRCs and
detected PAHs appear low relative to anthropogenic background typical of urban areas as
shown in Figure 14.

7.4.3 Conclusion

Because no background data are available for the site prior to Hurricane Katrina,
it is difficult to determine the impact of the hurricane on the surrounding environment
with certainty. However, none of the concentrations detected were at levels of concern in
regard to protection of human health. There is no indication of a potential release in the
area of the Polychemie, Inc. facility due to the effects of Hurricane Katrina.

-------
7.5 Ershigs Fiberglass - Biloxi, Mississippi

7.5.1	Results

Soils

Aluminum, arsenic, barium, cadmium, calcium, chromium, cobalt, copper, iron,
lead, magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were
reported in soil samples collected for this site. No volatile organic compounds, or PCBs
were detected in these samples. Low concentrations of six semi-volatile organic
compounds and six pesticides were reported.

Sediments

Aluminum, arsenic, barium, calcium, chromium, cobalt, copper, iron, lead,
magnesium, manganese, nickel, potassium, sodium, vanadium, and zinc were reported for
these samples. Twelve semi-volatile organic compounds and eight pesticides were
reported at low concentrations. No volatile organic compounds or PCBs were reported.

7.5.2	Discussion

Because no background data are available for the site prior to Hurricane Katrina,
it is difficult to determine the impact of the hurricane on the surrounding environment
with certainty. Although this facility is in an industrialized area, there is evidence of
residential development in the vicinity of the site. As an added precaution, detected
analytes were compared to residential PRCs.

Arsenic (1.3-14 mg/kg) was the only metal that exceeded residential PRCs (0.4
mg/kg), however all detections were within a risk range of 1 in 1,000,000 to 1 in 10,000
risk over background of an individual developing cancer over a lifetime from long-term
exposure to those concentrations, which EPA has found acceptable in other regulatory
and remedial contexts. The highest arsenic concentrations were taken in the vicinity of a
commercial parking lot, while those samples closer to residential areas were below the
1E-05 risk level. None of the other analytes exceeded residential PRC soil screening
values.

7.5.3	Conclusion

There does not appear to be indication of a potential release in the area of Ershigs
Fiberglass due to the effects of Hurricane Katrina. Styrene, one of the primary chemicals
stored and used on site, was not detected in the analysis. None of the detected analytes
were at levels of concern for excess human health risk from long term exposure.

30

-------
7.6 Naval Construction Battalion Center - Gulfport, Mississsippi

The data and discussion for NCBC will be issued as an addendum. Samples for
dioxin analysis were recollected due to uncertainties with the quality of the data from the
original laboratory. Four additional samples were collected from another portion of the
base for PCB analysis at the request of MDEQ, and will be included in the addendum.

31

-------
8.0 REFERENCES

1.	Comprehensive Environmental Response, Compensation, and Liability
Act of 1980 (CERCLA) and the Superfund Amendments and
Reauthorization Act of 1986 (SARA).

2.	U.S. EPA, EPAQA/G-4, Guidance for the Data Quality Objectives
Process, EPA/600/R-96/055, August 2000.

3.	U.S. EPA, EPAQA/G-5, EPA Guidance for Quality Assurance Project
Plans, EPA/600/R-98/018, February 1998.

4.	U.S. EPA, Region 4, Analytical Support Branch Operations and Quality
Control Manual Revision 1, (ASBLOQAM). July 2001.

5.	U.S. EPA, Region 4, Environmental Investigations Standard Operating
Procedures and Quality Assurance Manual (E1SOPQAM). November
2001. (http://vvvvvv.epa.gov/region4/sesd/sesdpub_guidance.html).

6.	USEPA Contract laboratory Program Statement of Work for Inorganic
Analysis, ILM05.3 March 2004.
http://vvvvvv.epa.gov/superfund/programs/clp/inorg.htm

7.	USEPA Contract laboratory Program Statement of Work for Inorganic
Analysis, OLM04.2, May, 1999.

http://vvvvvv.epa.gov/superfund/programs/clp/organic, htm

8.	USEPA Water Quality Studies of Bays in Waters of Mississippi, October,

2005.

9.	Quality Assurance Project Plan Katrina Response Environmental Soil and
Sediment Sampling Gulf Coast of Mississippi, September, 2005.

10.	Menzie et al. (1992) Exposure to Carcinogenic PAHs in the Environment.
Env Sci Technol 26, 1278-1284.

1 1. Saltiene et al. (2001) Contamination of Soil by Polycyclic Aromatic
Hydrocarbons in Some Urban Areas,
http: // preprint. chemvveb .com/envchem/0102001.

12.	Electric Power Research Institute (EPRI) (2000) Literature Review of
Polycyclic Aromatic Hydrocarbons TR-1 14755. This source provides
values for US and Japan background ranges, Michigan schools and
residences and Ohio residences.

13.	AT SDR, 2002 Toxicological Profile for Polycyclic Aromatic
Hydrocarbons. P. 262, Table 5-3.

32

-------
Appendix A
Figures

33

-------
U>
4^

-------
Ul

Figure 2
DuPont DeLisle Plant

DuPont DeLisle Plant

mmwrnrn

-------
Figure 3
Chevron, First Chemical
and MS Phosphates

'COUNTY AI ifKi



|pASCAGOUft4*

First Chemical Corporation

Substation

28 Ej.

m © © £jU*\

£00 fB*.;,

fa  ~ « l - • *

*»*"

fesr.

Mississippi Phosphates Corporation^

;t -\ AMI H'tf' f i

Chevron Pascagoula Refinery

Cfeariwgoi
,>:¦! Island /

-	j

y



Tenors

1 Miles

-------
! '' Omega Protein |

Figure 4
Omega Protein

Rtybert&on

Bounds Lake -¦¦¦if

y w u it t \



Mc /nn
Lake

MOSS POINT

ar.
-------
Figure 5
Polychemie, Inc

Comm Town
We^ Smfttr j,

AKviE

Polychemie Inc. - Pearlington, MS FacilityII

SgbMQtfon

2 Miles

-------
Figure 6
Ershigs Fiberglass, Inc

R hocfes" —
Point

Ershigs Fiberglass - Biloxi

NASHV'l

LCST"

% \ V S MILIT
^rfRESBBVAl

Oaybeacon

©Light

-------


... ...

i#fW8liV ti-V' '
:, ~

V- MSMff:

nmmsim-

Figure 7
NCBC Wetland

NCBC Wetland

Eversredi C«m ! ^

Gulfport

1 Miles

-------
-------
CFM-SF-02

CFM-SF-01

Hurricane Dike

Gulf Coast Monitoring
Study - Station BC4

CFM-SD-Q3

Gulf Coast Monitoring
Study - Station BC2

CFM-SD-04

CFM-SD-07

CFM-SD-06

1.2 Miles

G:/Katrina/EIB/Facilityjjata/Maps/review2,apr

Figure 9
Chevron, First Chemical
and MS Phosphates
Sampling Locations

-------
OP-SD-02

OP-SD-03

Figure 10
Omega Protein
Sampling Locations

OP-SD-01

2000

3000

4000

5000 Feet

-------
Figure 11
Polychemie, Inc.
Sampling Locations

PO-SD-01

PO-SD-02



PO-SF-04

PO-SD-03



4000 Feet

-------
Figure 12
Ershigs Fiberglass, Inc
Sampling Locations

ER-SD-04

500	1000 Feet

-------
NC-SD-01

G:/Katrina/EIB/Facility_data/Maps/review2i

Figure 13
NCBC Gulfport
Sampling Locations

NC-SD-02

-------
Figure 14: Comparison of background ranges of cPAHs from a variety of sources.

Menzie et al. US urban background
Saltiene et al, Int'l cities
Michigan Residences
Michigan Schools
Columbus OH residences
EPRI Japan background
EPRI US urban background
ATSDR Background Range
Eastern Magazine Area

0.1

10 100 1000 10000

47

-------
Appendix B
Data Summary Tables

48

-------
Table 1

Sample Rationale and Locations

Facility

Sample ID

Grab or
Composite

Location

Rationale

DuPont DeLisle

DU-SD-01

Grab (0"-
3")

Dirt road and canal southwest
of Site

Evaluate potential for hazardous constituents to have
drained from site via ditch.

DuPont DeLisle

DlJ-SD-02

Grab (0"-
3")

Dirt road at well south of site

Evaluate potential for hazardous constituents to have
drained from site via ditch.

DuPont DeLisle

DU-SF-03

3 point

composite

(0"-3")

South of swale along Kiln
DeLisle Rd.

Evaluate potential for hazardous constituents to have
moved North with storm surge.

DuPont DeLisle

DU-SF-04

3 point
composite

(0"-3")

South of swale along Kiln
DeLisle Rd.

Evaluate potential for hazardous constituents to have
moved North with storm surge.

DuPont DeLisle

DlJ-SF-05

4 point

composite

(0"-3")

South of swale along Kiln
DeLisle Rd.

Evaluate potential for hazardous constituents to have
moved North with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SF-01

3 point

linear

composite

(0"-3")

Bank of concrete drainage
structure

Evaluate potential for hazardous constituents to have
moved North with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SF-02

5 point
•Star-
composite
(0"-3")

Chevron Ditch, South of
complex

Evaluate potential for hazardous constituents to have
moved drained with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SD-04

Grab (0"-
3")

South of storm surge lagoon

Evaluate potential for hazardous constituents to have
moved North with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SD-05

Grab (0"-
3")

Wetlands southeast of complex

Evaluate potential for hazardous constituents to have
moved North with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SD-06

Grab (0"-
3")

Ditch south of complex

Evaluate potential for hazardous constituents to have
moved North with storm surge.

49

-------
Chevron, First
Chemical, MS
Phosphates

CFM-SD-07

Grab (0"-
3")

Ditch south of complex

Evaluate potential for hazardous constituents to have
moved North with storm surge.

Chevron, First
Chemical, MS
Phosphates

CFM-SF-08

5 point

•Star-

composite

(0"-3")

South of complex

Evaluate potential for hazardous constituents to have
moved South with storm surge.

Chevron, First
Chemical, MS
Phosphates

BC2

(Sediment)

Grab

Bayou Cassotte, West of MS
Phosphates

Evaluate potential for hazardous constituents to have
moved South with storm surge.

Chevron, First
Chemical, MS
Phosphates

BC4

(Sediment)

Grab

Bayou Cassotte, Southwest of
First Chemical

Evaluate potential for hazardous constituents to have
moved South with storm surge.

Omega Protein

OP-SD-01

Grab

Bank of Escatawpa River,
South of Site

Evaluate potential for hazardous constituents to have
drained South with storm surge.

Omega Protein

OP-SD-02

Grab

Bank of Escatawpa River,
South of Site

Evaluate potential for hazardous constituents to have
drained South with storm surge.

Omega Protein

OP-SD-03

Grab

Bank of Escatawpa River,
downstream of Site (power
line right-of-way)

Evaluate potential for hazardous constituents to have
moved downstream with storm surge.

Polychemie

PO-SD-01



Wetland North of Site

Evaluate potential for hazardous constituents to have
drained North with storm surge

Polychemie

PO-SD-02



Canal West of Site

Evaluate potential for hazardous constituents to have
drained West with storm surge

Polychemie

PO-SD-03

Grab

Canal at Sea Plane Rd.

Evaluate potential for hazardous constituents to have
moved downgradient with storm surge

Polychemie

PO-SF-04

5 point
linear
composite
near road

Southeast of Site

Evaluate potential for hazardous constituents to have
moved Southeast with storm surge

50

-------
Polychemie

PO-SF-05

5 point

linear

composite

between
fence and
road

Southwest of Site

Evaluate potential for hazardous constituents to have
moved Southwest with storm surge

Ershigs Fiberglass,

Inc.

ER-SF-01

5 point

composite

collected

around

perimeter

of

basketball
court

Northwest of Site

Evaluate potential for hazardous constituents to have
moved Northwest with storm surge









Ershigs Fiberglass,

Inc.

ER-SF-02

5 point

•Star-

composite

(0"-3")

Southwest of Site

Evaluate potential for hazardous constituents to have
moved West with storm surge

Ershigs Fiberglass,

Inc.

ER-SF-03

5 point

•Star-

composite

(0"-3")

South of Site

Evaluate potential for hazardous constituents to have
moved Southwest with storm surge

Ershigs Fiberglass,

Inc.

ER-SD-04

Grab (0"-
3")

South of Site, Canal on west
side of parking lot

Evaluate potential for hazardous constituents to have
moved South with storm surge

Ershigs Fiberglass,
Inc.

ER-SD-05

Grab (0"-
3")

Inlet southeast of Site

Evaluate potential for hazardous constituents to have
drained Southwest with storm surge

NCBC Gulfport

NC-SD-01

Grab (0"-
3")

Wetland North of NCBC

Evaluate potential for TCDD to have redoposited in
remediated portion of wetland due to storm surge

NCBC Gulfport

NC-SD-02

Grab (0"-
3")

Wetland North of NCBC

Evaluate potential for TCDD to have redoposited in
remediated portion of wetland due to storm surge

NCBC Gulfport

NC-SD-03

Grab (0"-
3")

sediment
trap

Wetland North of NCBC

Evaluate potential for TCDD to have redoposited in
remediated portion of wetland due to storm surge

51

-------
NCBC Gulfport

NC-SD-04

Grab (0"-

3")sedime
nt trap

Wetland North of NCBC

Evaluate potential for TCDD to have redoposited in
remediated portion of wetland due to storm surge

NCBC Gulfport

NC-SD-05

Grab (0"-
3")

sediment
trap

Wetland North of NCBC
(Edwards tract)

Evaluate potential for TCDD to have redoposited in
remediated portion of wetland due to storm surge

52

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Table 2
Sample Containers and I

olding Times

Analytes

Containers

Splits

Dups

Holding

Times

Metals

1 8oz. glass

1 8oz. glass

1 8oz. glass

180 days

VOCs

3 EnCore™

3 EnCore™

3 EnCore™

48 hours

Semi-Volatiles,
Pesticides, PCBs

1 8oz. glass

1 8oz. glass

1 8oz. glass

14 days

Dioxins

1 8oz. glass

1 8oz. glass

1 8oz. glass

30 days

Radium 226 and

gamma

Spectroscopy

1 Boz. glass

1 8oz. glass

1 8oz. glass

180 days

53

-------
Table 3

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
DuPont - DeLisle
Pass Christian, Mississippi
October, 2005



DUSD01



DUSD01D



DUSD02



DUSF03



DUSF04



DUSF05



1010



1105



1200



1405



1345



1320

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

55



58



24



11



12



12



Aluminum

MG/KG

12000



9000



4800



6500



5100



4000



Arsenic

MG/KG

53

J

35

J

1

R

1.4



1.5



1

R

Barium

MG/KG

140

J

87

J

400



27



17

J

15

J

Beryllium

MG/KG

2



1.3



0,22

UJ

0,12

UJ

0.1

UJ

0,04

UJ

Calcium

MG/KG

1500

J

1400

J

330

J

1100



230

J

540

J

Chromium

MG/KG

22

J

18

J

7.3

J

11

J

9.1

J

5.6

J

Cobalt

MG/KG

8.3

J

7.9

J

0.83

J

1.2

J

0.74

J

0.45

J

Copper

MG/KG

33

J

22

J

2.6

J

2.7

J

2

J

1.9

J

Iron

MG/KG

13000

J

13000

J

2900

J

9900

J

7900

J

4300

J

Lead

MG/KG

18

J

15

J

16

J

16

J

26

J

13

J

Magnesium

MG/KG

1100



1200



470

J

150

J

140

J

140

J

Manganese

MG/KG

96

J

130

J

12

J

380

J

180

J

36

J

Nickel

MG/KG

18

J

14

J

1.6

J

2.5

J

1.6

J

1.3

J

Potassium

MG/KG

1600



1200

J

240

J

88

J

82

J

85

J

Selenium

MG/KG

0.88

J

0,73

R



U

4

u

0,48

R

4

u

Sodium

MG/KG

1800



1900



630

J

110

UJ

110

UJ

96

UJ

Thallium

MG/KG

1.9

J

0,53

R

3.3

u

2... 8

u

2.8

U

2... 8

u

Vanadium

MG/KG

50



38



11



16



14



9.2



Zinc

MG/KG

56



49

J

15



21



14



11



U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered
unusable.

54

-------
Table 3 (Continued)

Data Summary Table - Semi-Volatiles
Post - Katrina Soil and Sediment Sampling
DuPont - DeLisle
Pass Christian, Mississippi
October, 2005



DUSD01



DUSD01D



DUSD02



DUSF03



DUSF04



DUSF05



1010



1105



1200



1405



1345



1320

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

50



50



24



14



12



10



1,1 -Biphenyl

UG/KG

660

U

660

U

1100



380

U

380

U

370

U

2-Methylnaphthalene

UG/KG

660

U

660

U

4100



380

u

380

u

370

u

Anthracene

UG/KG

660

U

660

U

110

J

380

u

380

u

370

u

Naphthalene

UG/KG

660

U

660

U

1100



380

u

380

u

370

u

Phenanthrene

UG/KG

660

U

660

U

1200



380

u

380

u

370

u

Pyrene

UG/KG

660

U

660

U

130

J

380

u

380

u

370

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

55

-------
Table 3 (Continued)

Data Summary Table - Pesticides/PCBs
Post - Katrina Soil and Sediment Sampling
DuPont - DeLisle
Pass Christian, Mississippi
October, 2005



DUSD01



DUSD01D



DUSD02



DUSF03



DUSF04



DUSF05



1010



1105



1200



1405



1345



1320

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

50



50



24



14



12



10



4,4'-DDD (p,p'-DDD)

UG/KG

6 6

UJ

6 6

UJ

4.3

UJ

3.3

UJ

0.8

J

3.7

UJ

alpha-Chlordane 12

UG/KG

4.7



4

N

2.2

U

1.7

U

1.1

NJ

1.9

U

Dieldrin

UG/KG

6 6

U

6 6

U

4.3

u

3.3

u

1

J

0.86

NJ

Endosulfan 1 (alpha)

UG/KG

3.4

u

1.1

J

2.2

u

1.7

u

1.9

U

1.9

U

Endrin

UG/KG

1.8

NJ

6 6

u

1

J

3.3

u

3.8

U

3.7

U

Endrin Ketone

UG/KG

6 6

u

6 6

u

4.3

u

3.3

u

3.8

u

1.7

NJ

Methoxychlor

UG/KG

34

u

34

u

22

u

5.7

J

19

u

19

U

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
/2-constituents or metabolites of technical chlordane

56

-------
Table 3 (Continued)

Data Summary Table - Volatile Organic Compounds
Post - Katrina Soil and Sediment Sampling
DuPont - DeLisle
Pass Christian, Mississippi
October, 2005



DUSD01



DUSD01D



DUSD02



DUSF03



DUSF04



DUSF05



1010



1105



1200



1405



1345



1320

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

56



55



24



14



12



10



Acetone

UG/KG

34

UJ

50

J

68

J

12

UJ

53

J

95

J

Benzene

UG/KG

34

U

38

U

24

J

12

U

11

U

12

U

Ethyl Benzene

UG/KG

34

u

38

U

230

J

12

U

11

u

12

U

Isopropylbenzene

UG/KG

34

u

38

u

140

J

12

U

11

u

12

u

Methylcyclohexane

UG/KG

34

u

38

u

140

J

12

U

11

u

12

u

Toluene

UG/KG

34

u

38

u

23

J

12

U

11

u

12

u

Total Xylenes

UG/KG

34

u

38

u

760

J

12

U

11

u

12

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

57

-------
Table 4

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005



CFMSF01



CFMSF02



CFMSF02S

CFMSD03



CFMSD04



CFMSD05



CFMSD05D



1055



1130



1130



1240



1345



1235



1245

10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005

% Moisture

%

9



22



22



58



25



77



80



Aluminum

MG/KG

7500



4000



4200



6800



4000



8900



8900



Arsenic

MG/KG

1.7



0.64

J

0.68

R

3.3



1.5

J

3.8

J

3.3

J

Barium

MG/KG

13

J

8

J

8.6

J

11

J

7.3

J

74

J

50

J

Beryllium

MG/KG

0.13

UJ

0.08

UJ

0.08

UJ

0.32

UJ

0.06

J

0.82

UJ

0.79

UJ

Calcium

MG/KG

9800



660



690



1200

J

3000



5100



5000



Chromium

MG/KG

9.2

J

4

J

4.2

J

14

J

5.6



95

J

80

J

Cobalt

MG/KG

0.69

J

0.34

J

0.38

J

1.8

J

0.66

J

4.1

J

2.7

J

Copper

MG/KG

3.6



2.6

J

2.7

J

6.8



2

J

33



30



Iron

MG/KG

5100

J

1300

J

1400

J

9200

J

5800



8500

J

6500

J

Lead

MG/KG

8.4

J

15

J

18

J

8

J

3



23

J

25

J

Magnesium

MG/KG

300

J

190

J

190

J

2400



610

J

4300



4400



Manganese

MG/KG

16

J

4.6

J

5.1

J

51

J

32

J

54

J

51

J

Nickel

MG/KG

3.6

J

1.2

J

1.4

J

5.9

J

2.5

J

64



47



Potassium

MG/KG

200

J

110

J

110

J

1400



240

J

1400

J

1500

J

Selenium

MG/KG

3.9

u

0.48

R

4.5

u

8.4

u

4.7

U

24



21



Sodium

MG/KG

470

J

520

J

530

J

9900



2800



22000



25000



Total Mercury

MG/KG

0.38



0.03

UJ

0.03

UJ

0.24

u

0.13

U

0.17

UJ

0.14

UJ

Vanadium

MG/KG

15



7.1



7.5



28



9.8



590



500



Zinc

MG/KG

18



16



16



30



9.5



150



130



U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered
unusable.

58

-------
Table 4 (Continued)

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005



CFMSD06



CFMSD07



CFMSF08



1145



1115



1035

10/6/2005



10/6/2005



10/6/2005

% Moisture

%

49



49



7



Aluminum

MG/KG

16000



11000



4300



Antimony

MG/KG

0.76

R

12

UJ

6.4

UJ

Arsenic

MG/KG

10



2.9



1.7



Barium

MG/KG

59



37

J

17

J

Beryllium

MG/KG

1.3



0.51

UJ

0,29

UJ

Cadmium

MG/KG

0,34

UJ

0.29

UJ

0,05

UJ

Calcium

MG/KG

43000



7700



15000



Chromium

MG/KG

60

J

28

J

16

J

Cobalt

MG/KG

14



2.5

J

2.2

J

Copper

MG/KG

15



20



23



Iron

MG/KG

21000

J

8600

J

4300

J

Lead

MG/KG

26

J

63

J

6.6

J

Magnesium

MG/KG

11000



3200



890



Manganese

MG/KG

890

J

93

J

45

J

Nickel

MG/KG

20



8.7



64



Potassium

MG/KG

2300



1300



220

J

Selenium

MG/KG

6 8

U

3.1

J

1.5

J

Sodium

MG/KG

8600



7700



300

J

Vanadium

MG/KG

41



60



240



Zinc

MG/KG

130



120



95



U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered
unusable.

59

-------
Table 4 (Continued)

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005



BC2SD



BC4DSD



BC4SD



1130



1300



1240

9/27/2005



9/27/2005



9/27/2005

% Moisture

%

60



41



49

A

Aluminum

MG/KG

8200



2600



3000



Arsenic

MG/KG

6.4



1.2



0.87



Barium

MG/KG

130



27



57



Beryllium

MG/KG

0.82



0.3



0.3



Cadmium

MG/KG

1.1



1.5



1.8



Calcium

MG/KG

7400



4900



4700



Chromium

MG/KG

21



7.2



9.7



Cobalt

MG/KG

4.6



0.59



0.66



Copper

MG/KG

20



4.7



5.5



Iron

MG/KG

17000



3400



3200



Lead

MG/KG

36



4.8



5.9



Magnesium

MG/KG

5100



1800



1700



Manganese

MG/KG

450



26



26



Nickel

MG/KG

8.4



2.4



2.7



Potassium

MG/KG

2300



510



450



Sodium

MG/KG

18000



8500



5900



Strontium

MG/KG

57



59



66



Titanium

MG/KG

17



12



14



Vanadium

MG/KG

24



6.1



7.3



Yttrium

MG/KG

12



2.7



2.5



Zinc

MG/KG

140



48



55



A-Analyte analyzed in replicate. Reported value is 'average' of replicates.

60

-------
Table 4 (Continued)

Data Summary Table - Semi-Volatile Organic Compounds
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005





BC2SD



BC4DSD



BC4SD







1130



1300



1240







9/27/2005



9/27/2005



9/27/2005



% Moisture

%

63.61



29.58



33.67



Fluoranthene

UG/KG

900

U

66

J

500

U

Pyrene

UG/KG

900

u

63

J

500

U

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

61

-------
Table 4 (Continued)

Data Summary Table - Pesticides/PCBs
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005



CFMSF01



CFMSF02



CFMSF02S



CFMSD03



CFMSD04



CFMSD05



1055



1130



1130



1240



1345



1235

10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005

% Moisture

%

9



23



21



54



25



77



gamma-Chlordane 12

UG/KG

1.9

U

2.2

U

2.2

U

3.7

U

2.3

U

3.8

NJ

Methoxychlor

UG/KG

19

U

22

U

5.3

NJ

37

U

23

U

74

U



CFMSD05D



CFMSD06



CFMSD07



CFMSF08



1245



1145



1115



1035

10/6/2005



10/6/2005



10/6/2005



10/6/2005

% Moisture

%

73



51



40



6



gamma-Chlordane 12

UG/KG

3.2

NJ

3.5

U

2.8

U



U

Methoxychlor

UG/KG

63

U

7.8

NJ

28

U

3.7

NJ

U-Analyte not detected at or above reporting limit.

NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
/2-constituents or metabolites of technical chlordane

-------
Table 4 (Continued)

Data Summary Table - VOCs
Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005





CFMSF01



CFMSF02



CFMSF02S



CFMSD03



CFMSD04



CFMSD05



CFMSD05D







1055



1130



1130



1240



1345



1235



1245







10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



10/6/2005



% Moisture

%

9



23



21



56



25



77



78



Acetone

UG/KG

11

U

13

U

13

U

35

IJ

13

U

180



81



Toluene

UG/KG

11

u

13

U

13

U

35

U

13

U

24

J

59

U





CFMSD06



CFMSD07



CFMSF08







1145



1115



1035







10/6/2005



10/6/2005



10/6/2005



% Moisture

%

51



40



6



Acetone

UG/KG

25

U

24

U



U

Toluene

UG/KG

25

U

24

U



u





BC2SD



BC4DSD



BC4SD







1130



1300



1240







9/27/2005



9/27/2005



9/27/2005



% Moisture

%

60



41



50



1,2,3-T richlorobenzene

UG/KG

1.8

J



U

6.5

U

Benzene

UG/KG

0.23

J

2.3

U

3.3

U

Carbon Disulfide

UG/KG

4.7

J

3.2



4.4



Isopropylbenzene

UG/KG

14



2.3

u

3.3

u

n-Butylbenzene

UG/KG

50

J



u

6.5

u

n-Propylbenzene

UG/KG

51

J

2.3

u

3.3

u

p-lsopropyltoluene

UG/KG

43

J

2.3

u

3.3

u

sec-Butylbenzene

UG/KG

30

J

2.3

u

3.3

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

63

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SF-01)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1.2e-01

PCI/GDRY

10/06/2005

Bi212

4.72e-01

2.3 e-01



PCI/GDRY

10/06/2005

Bi214 *

8.24e-01

6.6e-02



PCI/GDRY

10/06/2005

Co60

ND



2.7e-02

PCI/GDRY

10/06/2005

Csl37

4.5le-02

1.3e-02



PCI/GDRY

10/06/2005

1131

ND



4.9e-02

PCI/GDRY

10/06/2005

K40

7.19e-01

2.2e-01



PCI/GDRY

10/06/2005

Pb210

ND



3. le+00

PCI/GDRY

10/06/2005

Pb212

4.28e-01

4.3e-02



PCI/GDRY

10/06/2005

Pb214 *

8.75e-01

6.5e-02



PCI/GDRY

10/06/2005

Ra223

1.41 e-01

1.0e-01



PCI/GDRY

10/06/2005

Ra226 *

2.28e+00

4.1e-01



PCI/GDRY

10/06/2005

Ra228

4.61e-01

6.2e-02



PCI/GDRY

10/06/2005

T1208

1.34e-01

2. le-02



PCI/GDRY

10/06/2005

U235 *

1,42e-01

2.5e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2 a

MDC

Unit

Date





Uncertainty







Ra226

9.22e-01

1.5e-01

2.6e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SF-02)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1. le-01

PCI/GDRY

10/06/2005

Bi212

3.99e-01

2.2e-01



PCI/GDRY

10/06/2005

Bi214 *

5.10e-01

4.8e-02



PCI/GDRY

10/06/2005

Co60

ND



2.6e-02

PCI/GDRY

10/06/2005

Csl37

1.54e-01

2.0e-02



PCI/GDRY

10/06/2005

1131

ND



4.5e-02

PCI/GDRY

10/06/2005

K40

5.89e-01

2. le-01



PCI/GDRY

10/06/2005

Pb210

ND



2.8e+00

PCI/GDRY

10/06/2005

Pb212

4.64e-01

4.6e-02



PCI/GDRY

10/06/2005

Pb214 *

5.45e-01

4.9e-02



PCI/GDRY

10/06/2005

Ra223

1.00e-01

1.0e-01



PCI/GDRY

10/06/2005

Ra224

3.93e-01

3.6e-01



PCI/GDRY

10/06/2005

Ra226 *

1.20e+00

3.5e-01



PCI/GDRY

10/06/2005

Ra228

4.67e-01

6. le-02



PCI/GDRY

10/06/2005

T1208

1.36e-01

2. le-02



PCI/GDRY

10/06/2005

U235 *

7.54e-02

2.2e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

5.85e-01

1.0e-01

2.8e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SF-02S)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1.5e-01

PCI/GDRY

10/06/2005

Bi212

3.29e-01

2.4e-01



PCI/GDRY

10/06/2005

Bi214 *

5.06e-01

5.2e-02



PCI/GDRY

10/06/2005

Co60

ND



2.8e-02

PCI/GDRY

10/06/2005

Csl37

1.56e-01

2. le-02



PCI/GDRY

10/06/2005

1131

ND



5. le-02

PCI/GDRY

10/06/2005

K40

8.68e-01

2.2e-01



PCI/GDRY

10/06/2005

Pb210

ND



3. le+00

PCI/GDRY

10/06/2005

Pb212

4.58e-01

4.7e-02



PCI/GDRY

10/06/2005

Pb214 *

5.59e-01

5.2e-02



PCI/GDRY

10/06/2005

Ra223

1.3 le-01

9.8e-02



PCI/GDRY

10/06/2005

Ra226 *

1.13e+00

4. le-01



PCI/GDRY

10/06/2005

Ra228

4.77e-01

6.6e-02



PCI/GDRY

10/06/2005

T1208

1.33e-01

2.2e-02



PCI/GDRY

10/06/2005

U235 *

7.12e-02

2.6e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2 a

MDC

Unit

Date





Uncertainty







Ra226

6.70e-01

1.le-01

3.3e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-03)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1,6e-01

PCI/GDRY

10/06/2005

Be7

2.75e-01

1.5e-01



PCI/GDRY

10/06/2005

Bi212

3.5le-01

2.8e-01



PCI/GDRY

10/06/2005

Bi214 *

3.64e-01

6.0e-02



PCI/GDRY

10/06/2005

Co60

ND



5.6e-02

PCI/GDRY

10/06/2005

Csl37

2.39e-02

1.7e-02



PCI/GDRY

10/06/2005

1131

ND



5. le-02

PCI/GDRY

10/06/2005

K40

2.34e+00

4.2e-01



PCI/GDRY

10/06/2005

Pb210 *

8.85e-01

9.3e-01



PCI/GDRY

10/06/2005

Pb212

4.65e-01

4.8e-02



PCI/GDRY

10/06/2005

Pb214 *

4.35e-01

5.2e-02



PCI/GDRY

10/06/2005

Ra223

1.53e-01

7.5e-02



PCI/GDRY

10/06/2005

Ra224

3.97e-01

3.3e-01



PCI/GDRY

10/06/2005

Ra226 *

1.08e+00

4.0e-01



PCI/GDRY

10/06/2005

Ra228

3.74e-01

7.0e-02



PCI/GDRY

10/06/2005

Th234 *

6.77e-01

2.3e-01



PCI/GDRY

10/06/2005

T1208

1,42e-01

2.8e-02



PCI/GDRY

10/06/2005

U235 *

6.75e-02

2.5e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

4.90e-01

8.8e-02

2.7e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-04)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



8.7e-02

PCI/GDRY

10/06/2005

Be7

5.55e-02

5.8e-02



PCI/GDRY

10/06/2005

Bi212

4.60e-01

1.3e-01



PCI/GDRY

10/06/2005

Bi214 *

3.84e-01

3.3e-02



PCI/GDRY

10/06/2005

Co60

ND



2.0e-02

PCI/GDRY

10/06/2005

Csl37

ND



2.0e-02

PCI/GDRY

10/06/2005

1131

ND



2.5e-02

PCI/GDRY

10/06/2005

K40

1.11 e+00

1.6e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.2e+00

PCI/GDRY

10/06/2005

Pb212

4.38e-01

3.3e-02



PCI/GDRY

10/06/2005

Pb214 *

4.36e-01

3.3e-02



PCI/GDRY

10/06/2005

Ra224

4.03e-01

2.0e-01



PCI/GDRY

10/06/2005

Ra226 *

7.93e-01

1.9e-01



PCI/GDRY

10/06/2005

Ra228

4.13e-01

3.9e-02



PCI/GDRY

10/06/2005

T1208

1.29e-01

1.4e-02



PCI/GDRY

10/06/2005

U235 *

4.98e-02

1.2e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2 a

MDC

Unit

Date





Uncertainty







Ra226

5.77e-01

1.0e-01

3.5e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-05)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



6.3e-01

PCI/GDRY

10/06/2005

Bi212

4.59e-01

4.2e-01



PCI/GDRY

10/06/2005

Bi214 *

4.74e-01

9.8e-02



PCI/GDRY

10/06/2005

Co60

ND



7.8e-02

PCI/GDRY

10/06/2005

Csl37

4.28e-01

5.3e-02



PCI/GDRY

10/06/2005

1131

ND



3.2e-01

PCI/GDRY

10/06/2005

K40

2.32e+00

6.7e-01



PCI/GDRY

10/06/2005

Pb210

ND



9.4e+00

PCI/GDRY

10/06/2005

Pb212

4.93e-01

8. le-02



PCI/GDRY

10/06/2005

Pb214 *

5.59e-01

8.3e-02



PCI/GDRY

10/06/2005

Ra226 *

1.26e+00

7.6e-01



PCI/GDRY

10/06/2005

Ra228

3.98e-01

1.2e-01



PCI/GDRY

10/06/2005

Th234 *

1.04e+00

6. le-01



PCI/GDRY

10/06/2005

T1208

1.35e-01

4.9e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

7.35e-01

1.2e-01

1.9e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-05D)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte



Activity

± 2a

MDC

Unit

Date







Uncertainty







Ba 140



ND



2.4e-01

PCI/GDRY

10/06/2005

Bi212



6.80e-01

3.4e-01



PCI/GDRY

10/06/2005

Bi214

*

6.00e-01

1.0e-01



PCI/GDRY

10/06/2005

Co60



ND



6.le-02

PCI/GDRY

10/06/2005

Csl37



7.10e-01

6.2e-02



PCI/GDRY

10/06/2005

1131



ND



8.6e-02

PCI/GDRY

10/06/2005

K40



2.90e+00

5.4e-01



PCI/GDRY

10/06/2005

Pb210



ND



3.5e+00

PCI/GDRY

10/06/2005

Pb212



5.55e-01

7.3e-02



PCI/GDRY

10/06/2005

Pb214

*

7.32e-01

8.6e-02



PCI/GDRY

10/06/2005

Ra223



2.33e-01

1,4e-01



PCI/GDRY

10/06/2005

Ra226

*

1,66e+00

7.4e-01



PCI/GDRY

10/06/2005

Ra228



5.93e-01

1.2e-01



PCI/GDRY

10/06/2005

Th234

*

1.61e+00

5.3e-01



PCI/GDRY

10/06/2005

T1208



1.92e-01

4.4e-02



PCI/GDRY

10/06/2005

U235

*

1.13e-01

4.4e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte



Activity

± 2a

MDC

Unit

Date







Uncertainty







Ra226

7.42e-01

1.2e-01

1.7e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-06)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



2.0e-01

PCI/GDRY

10/06/2005

Be7

3.53e-01

1.7e-01



PCI/GDRY

10/06/2005

Bi212

1.17e+00

3.3e-01



PCI/GDRY

10/06/2005

Bi214 *

7.05e-01

7.6e-02



PCI/GDRY

10/06/2005

Co60

ND



4.5e-02

PCI/GDRY

10/06/2005

Csl37

5.36e-02

2. le-02



PCI/GDRY

10/06/2005

1131

ND



6.6e-02

PCI/GDRY

10/06/2005

K40

6.28e+00

6.0e-01



PCI/GDRY

10/06/2005

Pb210

ND



4.6e+00

PCI/GDRY

10/06/2005

Pb212

9.39e-01

7.8e-02



PCI/GDRY

10/06/2005

Pb214 *

7.85e-01

7.3e-02



PCI/GDRY

10/06/2005

Ra223

2.97e-01

l.le-01



PCI/GDRY

10/06/2005

Ra226 *

1,82e+00

5.8e-01



PCI/GDRY

10/06/2005

Ra228

1.00e+00

l.le-01



PCI/GDRY

10/06/2005

T1208

2.63e-01

3.6e-02



PCI/GDRY

10/06/2005

U235 *

1.14e-01

3.6e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

8.82e-01

1.4e-01

3. le-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SD-07)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1.8e-01

PCI/GDRY

10/06/2005

Be7

3.12e-01

1.7e-01



PCI/GDRY

10/06/2005

Bi212

5.62e-01

2.8e-01



PCI/GDRY

10/06/2005

Bi214 *

3.64e-01

5.8e-02



PCI/GDRY

10/06/2005

Co60

ND



4.le-02

PCI/GDRY

10/06/2005

Csl37

6.30e-01

4.8e-02



PCI/GDRY

10/06/2005

1131

ND



6.2e-02

PCI/GDRY

10/06/2005

K40

2.25e+00

3.4e-01



PCI/GDRY

10/06/2005

Pb210

ND



4.9e+00

PCI/GDRY

10/06/2005

Pb212

5.01e-01

5.4e-02



PCI/GDRY

10/06/2005

Pb214 *

4.04e-01

5.4e-02



PCI/GDRY

10/06/2005

Ra224

4.95e-01

3.8e-01



PCI/GDRY

10/06/2005

Ra226

ND



5.9e-01

PCI/GDRY

10/06/2005

Ra228

5.57e-01

8.0e-02



PCI/GDRY

10/06/2005

Th234 *

7.23e-01

3.6e-01



PCI/GDRY

10/06/2005

T1208

1,66e-01

2.8e-02



PCI/GDRY

10/06/2005

U235 *

8.07e-02

2.8e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

3.72e-01

6.9e-02

2.6e-02

PCI/GDRY

10/25/2005

-------
Table 4 (Continued)

Data Summary Table - Radionuclides (CFM-SF-08)

Post - Katrina Soil and Sediment Sampling
Chevron Refinery - Pascagoula, First Chemical, and Mississippi Phosphate

Pascagoula, Mississippi
October, 2005

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ba 140

ND



1.5e-01

PCI/GDRY

10/06/2005

Bi212

4.82e-01

2.9e-01



PCI/GDRY

10/06/2005

Bi214 *

4.57e-01

5.2e-02



PCI/GDRY

10/06/2005

Co60

ND



3.2e-02

PCI/GDRY

10/06/2005

Csl37

1.60e-02

1.3e-02



PCI/GDRY

10/06/2005

1131

ND



5.4e-02

PCI/GDRY

10/06/2005

K40

1.04e+00

2.8e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.4e+00

PCI/GDRY

10/06/2005

Pb212

4.38e-01

4.9e-02



PCI/GDRY

10/06/2005

Pb214 *

5.17e-01

5.3e-02



PCI/GDRY

10/06/2005

Ra223

1.14e-01

l.le-01



PCI/GDRY

10/06/2005

Ra226 *

8.91 e-01

4.5e-01



PCI/GDRY

10/06/2005

Ra228

4.66e-01

6.9e-02



PCI/GDRY

10/06/2005

T1208

1.38e-01

2.4e-02



PCI/GDRY

10/06/2005

U235 *

5.59e-02

2.8e-02



PCI/GDRY

10/06/2005

* An asterisk indicates a result whose value may be significantly over or underestimated.

Analyte

Activity

± 2a

MDC

Unit

Date





Uncertainty







Ra226

5.54e-01

9.7e-02

2.6e-02

PCI/GDRY

10/25/2005

-------
Table 5

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Omega Protein
Moss Point, Mississippi
October, 2005



OPSD01



OPSD02



OPSD02D



OPSD03



950



900



925



1020

10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

7



15



18



19



Aluminum

MG/KG

9500



5000



7800



4000



Antimony

MG/KG

0.45

J

1.6

J

7,4

UJ

7,4

UJ

Arsenic

MG/KG

1.2

J

3.6

J

2.2

J

1.6

J

Barium

MG/KG

260

J

81

J

18

J

15

J

Beryllium

MG/KG

0,04

UJ

0.05

J

0,08

UJ

0,03

UJ

Calcium

MG/KG

16000

J

970

J

2100

J

180

J

Chromium

MG/KG

10

J

39

J

10

J

8.5

J

Cobalt

MG/KG

3.3

J

4.1

J

1.1

J

0.41

J

Copper

MG/KG

45

J

46

J

6.5

J

13

J

Iron

MG/KG

8800

J

56000

J

10000

J

7700

J

Lead

MG/KG

80

J

130

J

8.8

J

17

J

Magnesium

MG/KG

1800



620



540

J

350

J

Manganese

MG/KG

54

J

350

J

46

J

8.9

J

Nickel

MG/KG

6.7

J

14

J

2.3

J

1.2

J

Potassium

MG/KG

270

J

260

J

240

J

290

J

Sodium

MG/KG

1400



1200



1100



1500



Thallium

MG/KG

0.47

R

0.54

J

3.1

u

3.1

u

Total Mercury

MG/KG

0,03

UJ

0,12

U

0,12

u

0.15



Vanadium

MG/KG

18



11



16



12



Zinc

MG/KG

220



980



44



11



U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered
unusable.

74

-------
Table 5 (Continued)

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Omega Protein
Moss Point, Mississippi
October, 2005



ER1DSD



ER1SD



1430



1400

9/28/2005



9/28/2005

% Moisture

%

23



20



Aluminum

MG/KG

180

A

210



Barium

MG/KG

1.7

A

1



Calcium

MG/KG

71

A

50



Iron

MG/KG

270

A

370



Lead

MG/KG

2.1

A

1.3



Magnesium

MG/KG

200

A

120



Manganese

MG/KG

1.7

A

2.5



Sodium

MG/KG

1300

A

540



Strontium

MG/KG

1.5

A

1.1



Titanium

MG/KG

2.6

AJ

2.8

J

Zinc

MG/KG

1.6

A

1.9



J-Identification of analyte is acceptable; reported value is an estimate.
A-Analyte analyzed in replicate. Reported value is 'average' of replicates.

-------
Table 5 (Continued)

Data Summary Table - Semi-Volatiles
Post - Katrina Soil and Sediment Sampling
Omega Protein
Moss Point, Mississippi
October, 2005



OPSD01



OPSD02



OPSD02D



OPSD03



950



900



925



1020

10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

6



14



19



14



Acenaphthylene

UG/KG

160

J

380

U

410

U

380

U

Acetophenone

UG/KG

300

J

91

J

410

u

8400



Anthracene

UG/KG

120

J

380

u

410

u

380

u

Benzaldehyde

UG/KG

350

UJ

380

UJ

410

UJ

1700

J

Benzo(a)Anthracene

UG/KG

1200



380

u

410

u

95

J

Benzo(b)Fluoranthene

UG/KG

1600



380

u

410

u

210

J

Benzo(ghi)Perylene

UG/KG

750

J

380

UJ

410

UJ

380

u

Benzo(k)Fluoranthene

UG/KG

890



380

u

410

u

130

J

Benzo-a-Pyrene

UG/KG

1300



380

u

410

u

380

u

Chrysene

UG/KG

1200



380

u

410

u

220

J

Dibenzo(a,h)Anthracene

UG/KG

360

J

380

UJ

410

UJ

380

u

Dimethyl Phthalate

UG/KG

350

u

570



410

u

380

u

Fluoranthene

UG/KG

1900



380

u

410

u

320

J

Indeno (1,2,3-cd) Pyrene

UG/KG

1100

J

380

UJ

410

UJ

87

J

Phenanthrene

UG/KG

140

J

380

u

410

u

380

u

Phenol

UG/KG

350

u

380

u

410

u

11000



Pyrene

UG/KG

2000



380

u

410

u

270

J

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

76

-------
Table 5 (Continued)

Data Summary Table - Pesticides/PCBs
Post - Katrina Soil and Sediment Sampling
Omega Protein
Moss Point, Mississippi
October, 2005



OPSD01



OPSD02



OPSD02D



OPSD03



950



900



925



1020

10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

6



14



19



14



4,4'-DDE (p,p'-DDE)

UG/KG

3.5

U

3.8

U

4 J

U

19

N

4,4'-DDT (p,p'-DDT)

UG/KG

1.4

J

3.8

U

4.1

U

12

N

alpha-Chlordane 12

UG/KG

1.7

NJ

2

u

2.1

u

2

U

Dieldrin

UG/KG

3.5

U

3.8

u

4.1

u

9.7



Endrin Ketone

UG/KG

3.5

U

3.8

u

2

NJ

2.7

NJ

gamma-Chlordane 12

UG/KG



u

2

u

2.1

u

5.8



Methoxychlor

UG/KG

8

NJ

20

u

21

u

20

U

PCB-1260 (Aroclor 1260)

UG/KG

35

u

21

J

41

u

38

U

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.

/2-constituents or metabolites of technical chlordane

77

-------
Table 6

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Polychemie, Inc.

Pearlington, Mississippi
October, 2005



POSD01



POSD01D



POSD02



POSD03



POSF04



POSF05



POSF05S



1225



1240



1320



1320



1250



1220



1220

10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005

% Moisture

%

80



79



64



26



14



13



14



Aluminum

MG/KG

15000



11000



9300



1900



2600



5400



5500



Arsenic

MG/KG

18

J

9

J

7.7

J

1

J

0.41

R

1.3

J

1.3

J

Barium

MG/KG

52

J

79

J

160

J

390

J

15

J

16

J

16

J

Cadmium

MG/KG

2., 5

U

2.3

U

1.4

U

0.92



0.58

U

0.57

U

0.58

U

Calcium

MG/KG

2300

J

2200

J

1900

J

11000

J

2000

J

320

J

380

J

Chromium

MG/KG

19

J

14

J

13

J

3.6

J

2.7

J

5.3

J

5.1

J

Cobalt

MG/KG

5.3

J

7.8

J

7.4

J

1.2

J

0.49

J

0.87

J

0.91

J

Copper

MG/KG

14

J

16

J

14

J

2.9

J

2

J

2.5

J

2.6

J

Iron

MG/KG

41000

J

23000

J

18000

J

3500

J

1900

J

5200

J

5000

J

Lead

MG/KG

26

J

17

J

14

J

8.8

J

6.6

J

6

J

6.5

J

Magnesium

MG/KG

3400



3400



3600



460

J

160

J

210

J

220

J

Manganese

MG/KG

190

J

260

J

380

J

160

J

21

J

160

J

170

J

Nickel

MG/KG

8.1

J

9.7

J

12

J

1.6

J

1.2

J

1.6

J

1.6

J

Potassium

MG/KG

1400

J

1500

J

1900



200

J

89

J

120

J

120

J

Selenium

MG/KG

17

u



u

98

u

4.7

U

4.1

u

0.27

R

0.58

J

Sodium

MG/KG

9600



9400



8100



830



530

J

440

J

590



Vanadium

MG/KG

38



28



25



4.3

J

4.6

J

9.8



9.7



Zinc

MG/KG

85



110



74



83



21



6.3

J

6.5

J

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered
unusable.

78

-------
Table 6 (Continued)

Data Summary Table - Semi-volatile Organic Compounds
Post - Katrina Soil and Sediment Sampling
Polychemie, Inc.

Pearlington, Mississippi
October, 2005



POSD01



POSD01D



POSD02



POSD03



POSF04



POSF05



POSF05S



1225



1240



1320



1320



1250



1220



1220

10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005

% Moisture

%

78



80



58



17



12



13



13



Benzo(a)Anthracene

UG/KG

1500

u

1700

u

790

U

220

J

380

U

380

U

380

U

Benzo(b)Fluoranthene

UG/KG

1500

u

1700

u

790

u

210

J

380

u

380

u

380

u

Benzo(ghi)Perylene

UG/KG

1500

UJ

1700

UJ

790

UJ

120

J

380

UJ

380

UJ

380

UJ

Benzo(k)Fluoranthene

UG/KG

1500

u

1700

u

790

u

230

J

380

u

380

u

380

u

Benzo-a-Pyrene

UG/KG

1500

u

1700

u

790

u

200

J

380

u

380

u

380

u

Chrysene

UG/KG

1500

u

1700

u

790

u

280

J

380

u

380

u

380

u

Fluoranthene

UG/KG

1500

u

1700

u

790

u

400



380

u

380

u

380

u

Indeno (1,2,3-cd) Pyrene

UG/KG

1500

u

1700

u

790

u

150

J

380

u

380

u

380

u

Phenanthrene

UG/KG

1500

u

1700

u

790

u

180

J

380

u

380

u

380

u

Pyrene

UG/KG

1500

u

1700

u

790

u

370

J

380

u

380

u

380

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

79

-------
Table 6 (Continued)

Data Summary Table - Pesticides/PCBs
Post - Katrina Soil and Sediment Sampling
Polychemie, Inc.

Pearlington, Mississippi
October, 2005





POSD01



POSD01D



POSD02



POSD03



POSF04



POSF05



POSF05S







1225



1240



1320



1320



1250



1220



1220







10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



% Moisture

%

78



80



58



17



12



13



13



gamma-Chlordane 12

UG/KG

7.7

U

8.5

IJ

4

U

2

U

0.86

J

2

U

2

U

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.
/2-constituents or metabolites of technical chlordane

80

-------
Table 6 (Continued)

Data Summary Table - Volatile Organic Compounds
Post - Katrina Soil and Sediment Sampling
Polychemie, Inc.

Pearlington, Mississippi
October, 2005



POSD01



POSD01D



POSD02



POSD03



POSF04



POSF05



POSF05S



1225



1240



1320



1320



1250



1220



1220

10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005



10/3/2005

% Moisture

%

78



80



58



17



12



13



13



Acetone

UG/KG

96

U

140



32

U

11

U

10

UJ

10

UJ

10

UJ

U-Analyte not detected at or above reporting limit.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

-------
Table 7

Data Summary Table - Metals
Post - Katrina Soil and Sediment Sampling
Ershigs Fiberglass
Biloxi, Mississippi
October, 2005



ERSF01



ERSF01S



ERSF02



ERSF03



ERSD04



ERSD04D



ERSD05



915



915



1010



1050



1115



1125



1145

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

45



38



9



20



49



29



52



Aluminum

MG/KG

4100



5300



2600



3000



15000



3500



4300



Antimony

MG/KG

OA

R

0.48

R

6 6

UJ

7.5

UJ

0.71

R

0.55

R

1.2

J

Arsenic

MG/KG

2.2

J

2.3

J

2.7

J

1.3

J

14

J

2.1

J

4.5

J

Barium

MG/KG

75

J

52

J

24

J

29

J

180

J

97

J

430

J

Cadmium

MG/KG

0.27

J

0,81

U

0.55

u

0.83

u

0.98

U

0.71

U

1.1

U

Calcium

MG/KG

19000

J

14000

J

1500

J

5900

J

3200

J

12000

J

2900

J

Chromium

MG/KG

8.1

J

8.7

J

3.9

J

5.9

J

16

J

8.3

J

9.2

J

Cobalt

MG/KG

1.5

J

1.4

J

0.47

J

0.83

J

2.5

J

1.3

J

2.2

J

Copper

MG/KG

48

J

32

J

11

J

9.9

J

39

J

18

J

120

J

Iron

MG/KG

6800

J

6500

J

2600

J

3300

J

11000

J

5400

J

8300

J

Lead

MG/KG

48

J

34

J

71

J

44

J

26

J

91

J

21

J

Magnesium

MG/KG

830

J

770

J

330

UJ

610

J

1700



2300



1700



Manganese

MG/KG

120

J

82

J

35

J

74

J

210

J

85

J

73

J

Nickel

MG/KG

4

J

3.9

J

1.4

J

4.8

J

5

J

2.6

J

3

J

Potassium

MG/KG

340

J

370

J

150

J

280

J

700

J

280

J

730

J

Sodium

MG/KG

1800



1400



730



900



2500



1300



4300



Vanadium

MG/KG

8.8

J

11



4.5

J

5.8

J

23



8.2



11

J

Zinc

MG/KG

1200



580



93



78



110



130



100



U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an
R-Presence or absence of analyte can not be determined from data due to
unusable.

estimate.

severe quality control problems.

Data are rejected and considered

82

-------
Table 7 (Continued)

Data Summary Table - Semi-Volatile Organic Compounds
Post - Katrina Soil and Sediment Sampling
Ershigs Fiberglass
Biloxi, Mississippi
October, 2005



ERSF01



ERSF01S



ERSF02



ERSF03



ERSD04



ERSD04D



ERSD05



915



915



1010



1050



1115



1125



1145

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

36



36



9



18



45



32



50



Acetophenone

UG/KG

170

J

520

U

360

U

400

U

300

J

490

U

660

U

Benzo(a)Anthracene

UG/KG

520

U

520

u

360

u

400

U

600

u

180

J

660

u

Benzo(b)Fluoranthene

UG/KG

520

u

520

u

360

u

87

J

600

u

280

J

660

u

Benzo(ghi)Perylene

UG/KG

520

UJ

520

UJ

360

UJ

400

UJ

600

UJ

250

J

660

UJ

Benzo(k)Fluoranthene

UG/KG

520

u

520

u

80

J

400

u

600

u

200

J

660

u

Benzo-a-Pyrene

UG/KG

520

u

520

u

360

u

400

u

600

u

230

J

660

u

bis(2-Ethylhexyl) Phthalate

UG/KG

860

u

1200

u

360

u

400

u

600

u

490

u

200

J

Chrysene

UG/KG

520

u

520

u

81

J

400

u

600

u

270

J

660

u

Fluoranthene

UG/KG

520

u

520

u

110

J

100

J

600

u

530



660

u

Indeno (1,2,3-cd) Pyrene

UG/KG

520

UJ

520

UJ

360

UJ

400

UJ

600

UJ

210

J

660

UJ

Phenanthrene

UG/KG

520

u

520

u

360

u

400

u

600

u

180

J

660

u

Pyrene

UG/KG

520

u

520

u

150

J

96

J

600

u

460

J

660

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

83

-------
Table 7 (Continued)

Data Summary Table - Pesticides/PCBs
Post - Katrina Soil and Sediment Sampling
Ershigs Fiberglass
Biloxi, Mississippi
October, 2005



ERSF01



ERSF01S



ERSF02



ERSF03



ERSD04



ERSD04D



ERSD05



915



915



1010



1050



1115



1125



1145

10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005



10/4/2005

% Moisture

%

36



36



9



18



45



32



50



4,4'-DDD (p,p'-DDD)

UG/KG

5., 2

UJ

5., 2

UJ

3.6

UJ

4

UJ

3.3

NJ

2

J

6 6

UJ

4,4'-DDE (p,p'-DDE)

UG/KG

5., 2

U

1.1

NJ

6.3



5.6



6.5



4.9

N

2

J

4,4'-DDT (p,p'-DDT)

UG/KG

5., 2

u

5., 2

U

6.2

N

9.9



12



3.9

J

2.7

J

Aldrin

UG/KG

2.7

u

2.7

U

1.9

U

0.91

NJ

15

N

2., 5

U

3.4

u

alpha-Chlordane 12

UG/KG

2., 7

u

3

u

17

U



IJ

24

N

8.4

N

6.5

u

Dieldrin

UG/KG

5., 2

u

1.3

J

7.2



9.4



12



7.1



4.6

NJ

Endosulfan Sulfate

UG/KG

5., 2

u

1.2

J

3.6

u

4

IJ

6

IJ

4.9

U

6 6

u

gamma-Chlordane 12

UG/KG

2.7

u

3.5

N

11

N

19

N

23

N

6 6

U

8.4



Methoxychlor

UG/KG

27

u

27

u

19

u

21

IJ

31

IJ

6.8

J

34

u

U-Analyte not detected at or above reporting limit.

J-Identification of analyte is acceptable; reported value is an estimate.

UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification.

NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
/2-constituents or metabolites of technical chlordane.

84

-------
Table 8

Data Summary Table - Volatile Trip Blanks
Post - Katrina Soil and Sediment Sampling
Ershigs Fiberglass
Biloxi, Mississippi
October, 2005



POTB901



TB902



TB903



TB904

1521



1229



1426



1427

10/3/2005



10/4/2005



10/6/2005



10/6/2005

% Moisture

%

0



0



0



0

Acetone

UG/KG

11



14

UJ

17



14

IJJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate

85

-------
Appendix C
Laboratory Data Sheets

86

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9518 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF08/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ4
D No: 3AJ4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

350

U

UG/KG

Benzaldehyde

350

U

UG/KG

Dibenzofuran

350

U

UG/KG

Phenol

350

U

UG/KG

2,4-Dinitrotoluene

350

U

UG/KG

bis(2-Chloroethyl) Ether

350

U

UG/KG

Diethyl Phthalate

350

U

UG/KG

2-Chlorophenol

350

U

UG/KG

Fluorene

350

U

UG/KG

2-Methylphenol

350

U

UG/KG

4-Chlorophenyl Phenyl Ether

350

U

UG/KG

bis(2-Chloroisopropyl) Ether

880

U

UG/KG

4-Nitroaniline

350

U

UG/KG

Acetophenone

880

U

UG/KG

2-Methyl-4,6-Dinitrophenol

350

U

UG/KG

(3-and/or 4-)Methylphenol

350

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

350

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

350

U

UG/KG

Hexachloroethane

350

UJ

UG/KG

4-Bromophenyl Phenyl Ether

350

U

UG/KG

Nitrobenzene

350

UJ

UG/KG

Hexachlorobenzene (HCB)

350

U

UG/KG

Isophorone

350

U

UG/KG

Atrazine

350

U

UG/KG

2-Nitrophenol

880

U

UG/KG

Pentachlorophenol

350

U

UG/KG

2,4-Dimethylphenol

350

U

UG/KG

Phenanthrene

350

U

UG/KG

bis(2-Chloroethoxy)Methane

350

U

UG/KG

Anthracene

350

U

UG/KG

2,4-Dichlorophenol

350

U

UG/KG

Carbazole

350

U

UG/KG

Naphthalene

350

U

UG/KG

Di-n-Butylphthalate

350

U

UG/KG

4-Chloroaniline

350

U

UG/KG

Fluoranthene

350

U

UG/KG

Hexachlorobutadiene

350

U

UG/KG

Pyrene

350

U

UG/KG

Caprolactam

350

U

UG/KG

Benzyl Butyl Phthalate

350

U

UG/KG

4-Chloro-3-Methylphenol

350

U

UG/KG

3,3'-Dichlorobenzidine

350

U

UG/KG

2-Methylnaphthalene

350

U

UG/KG

Benzo(a)Anthracene

350

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

350

U

UG/KG

Chrysene

350

U

UG/KG

2,4,6-T richlorophenol

350

U

UG/KG

bis(2-Ethylhexyl) Phthalate

880

u

UG/KG

2,4,5-Trichlorophenol

350

U

UG/KG

Di-n-Octylphthalate

350

u

UG/KG

1,1 -Biphenyl

350

U

UG/KG

Benzo(b)Fluoranthene

350

u

UG/KG

2-Chloronaphthalene

350

U

UG/KG

Benzo(k)Fluoranthene

880

u

UG/KG

2-Nitroaniline

350

U

UG/KG

Benzo-a-Pyrene

350

u

UG/KG

Dimethyl Phthalate

350

u

UG/KG

Indeno (1,2,3-cd) Pyrene

350

u

UG/KG

2,6-Dinitrotoluene

350

u

UG/KG

Dibenzo(a,h)Anthracene

350

u

UG/KG

Acenaphthylene

350

u

UG/KG

Benzo(ghi)Perylene

880

u

UG/KG

3-Nitroaniline

6



%

% Moisture

350

u

UG/KG

Acenaphthene









880

u

UG/KG

2,4-Dinitrophenol









880

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9518 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF08/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ4
D No: 3AJ4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:35
Ending:

RESULTS UNITS

4200 J UG/KG
89 J UG/KG

ANALYTE

22 UNKNOWNS

SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9519 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD07/

Media: SEDIMENT

Case No: 34717
MD No: 3AJ5
D No: 3AJ5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

550

U

UG/KG

Benzaldehyde

550

U

UG/KG

Dibenzofuran

550

U

UG/KG

Phenol

550

U

UG/KG

2,4-Dinitrotoluene

550

U

UG/KG

bis(2-Chloroethyl) Ether

550

U

UG/KG

Diethyl Phthalate

550

U

UG/KG

2-Chlorophenol

550

U

UG/KG

Fluorene

550

U

UG/KG

2-Methylphenol

550

U

UG/KG

4-Chlorophenyl Phenyl Ether

550

U

UG/KG

bis(2-Chloroisopropyl) Ether

1400

U

UG/KG

4-Nitroaniline

550

U

UG/KG

Acetophenone

1400

U

UG/KG

2-Methyl-4,6-Dinitrophenol

550

U

UG/KG

(3-and/or 4-)Methylphenol

550

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

550

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

550

U

UG/KG

Hexachloroethane

550

UJ

UG/KG

4-Bromophenyl Phenyl Ether

550

U

UG/KG

Nitrobenzene

550

UJ

UG/KG

Hexachlorobenzene (HCB)

550

U

UG/KG

Isophorone

550

U

UG/KG

Atrazine

550

U

UG/KG

2-Nitrophenol

1400

U

UG/KG

Pentachlorophenol

550

U

UG/KG

2,4-Dimethylphenol

550

U

UG/KG

Phenanthrene

550

U

UG/KG

bis(2-Chloroethoxy)Methane

550

U

UG/KG

Anthracene

550

U

UG/KG

2,4-Dichlorophenol

550

U

UG/KG

Carbazole

550

U

UG/KG

Naphthalene

550

U

UG/KG

Di-n-Butylphthalate

550

U

UG/KG

4-Chloroaniline

550

U

UG/KG

Fluoranthene

550

U

UG/KG

Hexachlorobutadiene

550

U

UG/KG

Pyrene

550

U

UG/KG

Caprolactam

550

U

UG/KG

Benzyl Butyl Phthalate

550

u

UG/KG

4-Chloro-3-Methylphenol

550

U

UG/KG

3,3'-Dichlorobenzidine

550

u

UG/KG

2-Methylnaphthalene

550

U

UG/KG

Benzo(a)Anthracene

550

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

550

U

UG/KG

Chrysene

550

u

UG/KG

2,4,6-T richlorophenol

550

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1400

u

UG/KG

2,4,5-Trichlorophenol

550

U

UG/KG

Di-n-Octylphthalate

550

u

UG/KG

1,1 -Biphenyl

550

U

UG/KG

Benzo(b)Fluoranthene

550

u

UG/KG

2-Chloronaphthalene

550

U

UG/KG

Benzo(k)Fluoranthene

1400

u

UG/KG

2-Nitroaniline

550

U

UG/KG

Benzo-a-Pyrene

550

u

UG/KG

Dimethyl Phthalate

550

u

UG/KG

Indeno (1,2,3-cd) Pyrene

550

u

UG/KG

2,6-Dinitrotoluene

550

u

UG/KG

Dibenzo(a,h)Anthracene

550

u

UG/KG

Acenaphthylene

550

u

UG/KG

Benzo(ghi)Perylene

1400

u

UG/KG

3-Nitroaniline

40



%

% Moisture

550

u

UG/KG

Acenaphthene









1400

u

UG/KG

2,4-Dinitrophenol









1400

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9519 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD07/	MD No: 3AJ5	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ5	Org Contractor: LIBRTY

RESULTS

UNITS

8700

J

UG/KG

550

NJ

UG/KG

210

NJ

UG/KG

210

NJ

UG/KG

210

NJ

UG/KG

1000

NJ

UG/KG

1200

NJ

UG/KG

ANALYTE

24 UNKNOWNS

EUCALYPTOL

CARYOPHYLLENE

HEXADECANOIC ACID, METHYL ESTER
N-HEXADECANOIC ACID
STIGMASTEROL, 22,23-DIHYDRO-
STIGMAST-4-EN-3-ONE

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:15
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9520 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF02/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ6
D No: 3AJ6

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

430

U

UG/KG

Benzaldehyde

430

U

UG/KG

Dibenzofuran

430

U

UG/KG

Phenol

430

U

UG/KG

2,4-Dinitrotoluene

430

U

UG/KG

bis(2-Chloroethyl) Ether

430

U

UG/KG

Diethyl Phthalate

430

U

UG/KG

2-Chlorophenol

430

U

UG/KG

Fluorene

430

U

UG/KG

2-Methylphenol

430

U

UG/KG

4-Chlorophenyl Phenyl Ether

430

U

UG/KG

bis(2-Chloroisopropyl) Ether

1100

U

UG/KG

4-Nitroaniline

430

U

UG/KG

Acetophenone

1100

U

UG/KG

2-Methyl-4,6-Dinitrophenol

430

U

UG/KG

(3-and/or 4-)Methylphenol

430

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

430

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

430

U

UG/KG

Hexachloroethane

430

UJ

UG/KG

4-Bromophenyl Phenyl Ether

430

U

UG/KG

Nitrobenzene

430

UJ

UG/KG

Hexachlorobenzene (HCB)

430

U

UG/KG

Isophorone

430

U

UG/KG

Atrazine

430

U

UG/KG

2-Nitrophenol

1100

U

UG/KG

Pentachlorophenol

430

U

UG/KG

2,4-Dimethylphenol

430

U

UG/KG

Phenanthrene

430

U

UG/KG

bis(2-Chloroethoxy)Methane

430

U

UG/KG

Anthracene

430

U

UG/KG

2,4-Dichlorophenol

430

U

UG/KG

Carbazole

430

U

UG/KG

Naphthalene

430

U

UG/KG

Di-n-Butylphthalate

430

U

UG/KG

4-Chloroaniline

430

U

UG/KG

Fluoranthene

430

u

UG/KG

Hexachlorobutadiene

430

U

UG/KG

Pyrene

430

u

UG/KG

Caprolactam

430

U

UG/KG

Benzyl Butyl Phthalate

430

u

UG/KG

4-Chloro-3-Methylphenol

430

U

UG/KG

3,3'-Dichlorobenzidine

430

u

UG/KG

2-Methylnaphthalene

430

U

UG/KG

Benzo(a)Anthracene

430

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

430

U

UG/KG

Chrysene

430

u

UG/KG

2,4,6-T richlorophenol

430

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1100

u

UG/KG

2,4,5-Trichlorophenol

430

U

UG/KG

Di-n-Octylphthalate

430

u

UG/KG

1,1 -Biphenyl

430

U

UG/KG

Benzo(b)Fluoranthene

430

u

UG/KG

2-Chloronaphthalene

430

U

UG/KG

Benzo(k)Fluoranthene

1100

u

UG/KG

2-Nitroaniline

430

U

UG/KG

Benzo-a-Pyrene

430

u

UG/KG

Dimethyl Phthalate

430

u

UG/KG

Indeno (1,2,3-cd) Pyrene

430

u

UG/KG

2,6-Dinitrotoluene

430

u

UG/KG

Dibenzo(a,h)Anthracene

430

u

UG/KG

Acenaphthylene

430

u

UG/KG

Benzo(ghi)Perylene

1100

u

UG/KG

3-Nitroaniline

23



%

% Moisture

430

u

UG/KG

Acenaphthene









1100

u

UG/KG

2,4-Dinitrophenol









1100

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9520 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF02/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ6
D No: 3AJ6

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

RESULTS UNITS

1400

J

UG/KG

340

NJ

UG/KG

800

NJ

UG/KG

ANALYTE

8 UNKNOWNS

.GAMMA.-SITOSTEROL

A'-NEOGAMMACER-22(29)-EN-3-ONE

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9521 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF02S/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ7
D No: 3AJ7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

420

U

UG/KG

Benzaldehyde

420

U

UG/KG

Dibenzofuran

420

U

UG/KG

Phenol

420

U

UG/KG

2,4-Dinitrotoluene

420

U

UG/KG

bis(2-Chloroethyl) Ether

420

U

UG/KG

Diethyl Phthalate

420

U

UG/KG

2-Chlorophenol

420

U

UG/KG

Fluorene

420

U

UG/KG

2-Methylphenol

420

U

UG/KG

4-Chlorophenyl Phenyl Ether

420

U

UG/KG

bis(2-Chloroisopropyl) Ether

1100

U

UG/KG

4-Nitroaniline

420

U

UG/KG

Acetophenone

1100

U

UG/KG

2-Methyl-4,6-Dinitrophenol

420

U

UG/KG

(3-and/or 4-)Methylphenol

420

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

420

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

420

U

UG/KG

Hexachloroethane

420

UJ

UG/KG

4-Bromophenyl Phenyl Ether

420

U

UG/KG

Nitrobenzene

420

UJ

UG/KG

Hexachlorobenzene (HCB)

420

U

UG/KG

Isophorone

420

U

UG/KG

Atrazine

420

U

UG/KG

2-Nitrophenol

1100

U

UG/KG

Pentachlorophenol

420

U

UG/KG

2,4-Dimethylphenol

420

U

UG/KG

Phenanthrene

420

U

UG/KG

bis(2-Chloroethoxy)Methane

420

U

UG/KG

Anthracene

420

U

UG/KG

2,4-Dichlorophenol

420

U

UG/KG

Carbazole

420

U

UG/KG

Naphthalene

420

U

UG/KG

Di-n-Butylphthalate

420

U

UG/KG

4-Chloroaniline

420

U

UG/KG

Fluoranthene

420

u

UG/KG

Hexachlorobutadiene

420

U

UG/KG

Pyrene

420

u

UG/KG

Caprolactam

420

U

UG/KG

Benzyl Butyl Phthalate

420

u

UG/KG

4-Chloro-3-Methylphenol

420

U

UG/KG

3,3'-Dichlorobenzidine

420

u

UG/KG

2-Methylnaphthalene

420

U

UG/KG

Benzo(a)Anthracene

420

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

420

U

UG/KG

Chrysene

420

u

UG/KG

2,4,6-T richlorophenol

420

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1100

u

UG/KG

2,4,5-Trichlorophenol

420

U

UG/KG

Di-n-Octylphthalate

420

u

UG/KG

1,1 -Biphenyl

420

U

UG/KG

Benzo(b)Fluoranthene

420

u

UG/KG

2-Chloronaphthalene

420

U

UG/KG

Benzo(k)Fluoranthene

1100

u

UG/KG

2-Nitroaniline

420

U

UG/KG

Benzo-a-Pyrene

420

u

UG/KG

Dimethyl Phthalate

420

u

UG/KG

Indeno (1,2,3-cd) Pyrene

420

u

UG/KG

2,6-Dinitrotoluene

420

u

UG/KG

Dibenzo(a,h)Anthracene

420

u

UG/KG

Acenaphthylene

420

u

UG/KG

Benzo(ghi)Perylene

1100

u

UG/KG

3-Nitroaniline

21



%

% Moisture

420

u

UG/KG

Acenaphthene









1100

u

UG/KG

2,4-Dinitrophenol









1100

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/31/2005 12:29

Sample 9521 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF02S/	MD No: 3AJ7	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ7	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

5300 J

UG/KG

21 UNKNOWNS

100 NJ

UG/KG

SUBSTITUTED PHENANTHRENECARBOXYLIC ACID

770 NJ

UG/KG

.GAMMA.-SITOSTEROL

460 NJ

UG/KG

2,5 -HEXANEDIONE

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9522 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSF01 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ8
D No: 3AJ8

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:55
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

360

U

UG/KG

Benzaldehyde

360

U

UG/KG

Dibenzofuran

360

U

UG/KG

Phenol

360

U

UG/KG

2,4-Dinitrotoluene

360

U

UG/KG

bis(2-Chloroethyl) Ether

360

U

UG/KG

Diethyl Phthalate

360

U

UG/KG

2-Chlorophenol

360

U

UG/KG

Fluorene

360

U

UG/KG

2-Methylphenol

360

U

UG/KG

4-Chlorophenyl Phenyl Ether

360

U

UG/KG

bis(2-Chloroisopropyl) Ether

910

U

UG/KG

4-Nitroaniline

360

U

UG/KG

Acetophenone

910

U

UG/KG

2-Methyl-4,6-Dinitrophenol

360

U

UG/KG

(3-and/or 4-)Methylphenol

360

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

360

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

360

U

UG/KG

Hexachloroethane

360

UJ

UG/KG

4-Bromophenyl Phenyl Ether

360

U

UG/KG

Nitrobenzene

360

UJ

UG/KG

Hexachlorobenzene (HCB)

360

U

UG/KG

Isophorone

360

U

UG/KG

Atrazine

360

U

UG/KG

2-Nitrophenol

910

U

UG/KG

Pentachlorophenol

360

U

UG/KG

2,4-Dimethylphenol

360

U

UG/KG

Phenanthrene

360

U

UG/KG

bis(2-Chloroethoxy)Methane

360

U

UG/KG

Anthracene

360

U

UG/KG

2,4-Dichlorophenol

360

U

UG/KG

Carbazole

360

U

UG/KG

Naphthalene

360

U

UG/KG

Di-n-Butylphthalate

360

U

UG/KG

4-Chloroaniline

360

U

UG/KG

Fluoranthene

360

U

UG/KG

Hexachlorobutadiene

360

U

UG/KG

Pyrene

360

U

UG/KG

Caprolactam

360

U

UG/KG

Benzyl Butyl Phthalate

360

U

UG/KG

4-Chloro-3-Methylphenol

360

U

UG/KG

3,3'-Dichlorobenzidine

360

U

UG/KG

2-Methylnaphthalene

360

U

UG/KG

Benzo(a)Anthracene

360

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

360

U

UG/KG

Chrysene

360

u

UG/KG

2,4,6-T richlorophenol

360

U

UG/KG

bis(2-Ethylhexyl) Phthalate

910

u

UG/KG

2,4,5-Trichlorophenol

360

U

UG/KG

Di-n-Octylphthalate

360

u

UG/KG

1,1 -Biphenyl

360

U

UG/KG

Benzo(b)Fluoranthene

360

u

UG/KG

2-Chloronaphthalene

360

U

UG/KG

Benzo(k)Fluoranthene

910

u

UG/KG

2-Nitroaniline

360

U

UG/KG

Benzo-a-Pyrene

360

u

UG/KG

Dimethyl Phthalate

360

u

UG/KG

Indeno (1,2,3-cd) Pyrene

360

u

UG/KG

2,6-Dinitrotoluene

360

u

UG/KG

Dibenzo(a,h)Anthracene

360

u

UG/KG

Acenaphthylene

360

u

UG/KG

Benzo(ghi)Perylene

910

u

UG/KG

3-Nitroaniline

9



%

% Moisture

360

u

UG/KG

Acenaphthene









910

u

UG/KG

2,4-Dinitrophenol









910

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9522 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF01 /	MD No: 3AJ8	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ8	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

12 UNKNOWNS

1900

J

UG/KG

81

NJ

UG/KG

390

NJ

UG/KG

1-(10-METHYLANTHRACEN-9-YL)ETHANONE
1-NAPHTHALENECARBOXYLIC ACID, DECAHYDRO-

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:55
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9523 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD06/

Media: SEDIMENT

Case No: 34717
MD No: 3AJ9
D No: 3AJ9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

670

U

UG/KG

Benzaldehyde

670

U

UG/KG

Dibenzofuran

670

U

UG/KG

Phenol

670

U

UG/KG

2,4-Dinitrotoluene

670

U

UG/KG

bis(2-Chloroethyl) Ether

670

U

UG/KG

Diethyl Phthalate

670

U

UG/KG

2-Chlorophenol

670

U

UG/KG

Fluorene

670

U

UG/KG

2-Methylphenol

670

U

UG/KG

4-Chlorophenyl Phenyl Ether

670

U

UG/KG

bis(2-Chloroisopropyl) Ether

1700

U

UG/KG

4-Nitroaniline

670

U

UG/KG

Acetophenone

1700

U

UG/KG

2-Methyl-4,6-Dinitrophenol

670

U

UG/KG

(3-and/or 4-)Methylphenol

670

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

670

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

670

U

UG/KG

Hexachloroethane

670

UJ

UG/KG

4-Bromophenyl Phenyl Ether

670

U

UG/KG

Nitrobenzene

670

UJ

UG/KG

Hexachlorobenzene (HCB)

670

U

UG/KG

Isophorone

670

U

UG/KG

Atrazine

670

U

UG/KG

2-Nitrophenol

1700

U

UG/KG

Pentachlorophenol

670

U

UG/KG

2,4-Dimethylphenol

670

U

UG/KG

Phenanthrene

670

U

UG/KG

bis(2-Chloroethoxy)Methane

670

U

UG/KG

Anthracene

670

U

UG/KG

2,4-Dichlorophenol

670

U

UG/KG

Carbazole

670

U

UG/KG

Naphthalene

670

U

UG/KG

Di-n-Butylphthalate

670

U

UG/KG

4-Chloroaniline

670

U

UG/KG

Fluoranthene

670

U

UG/KG

Hexachlorobutadiene

670

U

UG/KG

Pyrene

670

U

UG/KG

Caprolactam

670

U

UG/KG

Benzyl Butyl Phthalate

670

u

UG/KG

4-Chloro-3-Methylphenol

670

U

UG/KG

3,3'-Dichlorobenzidine

670

u

UG/KG

2-Methylnaphthalene

670

U

UG/KG

Benzo(a)Anthracene

670

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

670

U

UG/KG

Chrysene

670

u

UG/KG

2,4,6-T richlorophenol

670

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1700

u

UG/KG

2,4,5-Trichlorophenol

670

U

UG/KG

Di-n-Octylphthalate

670

u

UG/KG

1,1 -Biphenyl

670

U

UG/KG

Benzo(b)Fluoranthene

670

u

UG/KG

2-Chloronaphthalene

670

U

UG/KG

Benzo(k)Fluoranthene

1700

u

UG/KG

2-Nitroaniline

670

U

UG/KG

Benzo-a-Pyrene

670

u

UG/KG

Dimethyl Phthalate

670

u

UG/KG

Indeno (1,2,3-cd) Pyrene

670

u

UG/KG

2,6-Dinitrotoluene

670

u

UG/KG

Dibenzo(a,h)Anthracene

670

u

UG/KG

Acenaphthylene

670

u

UG/KG

Benzo(ghi)Perylene

1700

u

UG/KG

3-Nitroaniline

51



%

% Moisture

670

u

UG/KG

Acenaphthene









1700

u

UG/KG

2,4-Dinitrophenol









1700

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9523 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD06/	MD No: 3AJ9	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ9	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

17 UNKNOWNS

15000

J

UG/KG

310

NJ

UG/KG

280

NJ

UG/KG

N-HEXADECANOIC ACID
SQUALENE

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:45
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9524 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD05/

Media: SEDIMENT

Case No: 34717
MD No: 3AK0
D No: 3AK0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1400

U

UG/KG

Benzaldehyde

1400

U

UG/KG

Dibenzofuran

1400

U

UG/KG

Phenol

1400

U

UG/KG

2,4-Dinitrotoluene

1400

U

UG/KG

bis(2-Chloroethyl) Ether

1400

U

UG/KG

Diethyl Phthalate

1400

U

UG/KG

2-Chlorophenol

1400

U

UG/KG

Fluorene

1400

U

UG/KG

2-Methylphenol

1400

U

UG/KG

4-Chlorophenyl Phenyl Ether

1400

U

UG/KG

bis(2-Chloroisopropyl) Ether

3600

U

UG/KG

4-Nitroaniline

1400

U

UG/KG

Acetophenone

3600

U

UG/KG

2-Methyl-4,6-Dinitrophenol

1400

U

UG/KG

(3-and/or 4-)Methylphenol

1400

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

1400

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

1400

U

UG/KG

Hexachloroethane

1400

UJ

UG/KG

4-Bromophenyl Phenyl Ether

1400

U

UG/KG

Nitrobenzene

1400

UJ

UG/KG

Hexachlorobenzene (HCB)

1400

U

UG/KG

Isophorone

1400

U

UG/KG

Atrazine

1400

U

UG/KG

2-Nitrophenol

3600

U

UG/KG

Pentachlorophenol

1400

U

UG/KG

2,4-Dimethylphenol

1400

U

UG/KG

Phenanthrene

1400

U

UG/KG

bis(2-Chloroethoxy)Methane

1400

U

UG/KG

Anthracene

1400

U

UG/KG

2,4-Dichlorophenol

1400

U

UG/KG

Carbazole

1400

U

UG/KG

Naphthalene

1400

U

UG/KG

Di-n-Butylphthalate

1400

U

UG/KG

4-Chloroaniline

1400

U

UG/KG

Fluoranthene

1400

U

UG/KG

Hexachlorobutadiene

1400

U

UG/KG

Pyrene

1400

U

UG/KG

Caprolactam

1400

U

UG/KG

Benzyl Butyl Phthalate

1400

u

UG/KG

4-Chloro-3-Methylphenol

1400

U

UG/KG

3,3'-Dichlorobenzidine

1400

u

UG/KG

2-Methylnaphthalene

1400

U

UG/KG

Benzo(a)Anthracene

1400

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

1400

U

UG/KG

Chrysene

1400

u

UG/KG

2,4,6-T richlorophenol

1400

U

UG/KG

bis(2-Ethylhexyl) Phthalate

3600

u

UG/KG

2,4,5-Trichlorophenol

1400

U

UG/KG

Di-n-Octylphthalate

1400

u

UG/KG

1,1 -Biphenyl

1400

U

UG/KG

Benzo(b)Fluoranthene

1400

u

UG/KG

2-Chloronaphthalene

1400

u

UG/KG

Benzo(k)Fluoranthene

3600

u

UG/KG

2-Nitroaniline

1400

u

UG/KG

Benzo-a-Pyrene

1400

u

UG/KG

Dimethyl Phthalate

1400

u

UG/KG

Indeno (1,2,3-cd) Pyrene

1400

u

UG/KG

2,6-Dinitrotoluene

1400

u

UG/KG

Dibenzo(a,h)Anthracene

1400

u

UG/KG

Acenaphthylene

1400

u

UG/KG

Benzo(ghi)Perylene

3600

u

UG/KG

3-Nitroaniline

77



%

% Moisture

1400

u

UG/KG

Acenaphthene









3600

u

UG/KG

2,4-Dinitrophenol









3600

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9524 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD05/

Media: SEDIMENT

Case No: 34717
MD No: 3AK0
D No: 3AK0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:35
Ending:

RESULTS

UNITS

ANALYTE

870 NJ

UG/KG

BICYCLO [3.1.1] HEPTANE, 6,6,DIMETHYL-2-METHYL-

74000 J

UG/KG

26 UNKNOWNS

1600 NJ

UG/KG

N-HEXADECANOIC ACID

5300 NJ

UG/KG

STIGMAST-4-EN-3-ONE

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9525 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD05D/

Media: SEDIMENT

Case No: 34717
MD No: 3AK1
D No: 3AK1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1200

U

UG/KG

Benzaldehyde

1200

U

UG/KG

Dibenzofuran

1200

U

UG/KG

Phenol

1200

U

UG/KG

2,4-Dinitrotoluene

1200

U

UG/KG

bis(2-Chloroethyl) Ether

1200

U

UG/KG

Diethyl Phthalate

1200

U

UG/KG

2-Chlorophenol

1200

U

UG/KG

Fluorene

1200

U

UG/KG

2-Methylphenol

1200

U

UG/KG

4-Chlorophenyl Phenyl Ether

1200

U

UG/KG

bis(2-Chloroisopropyl) Ether

3100

U

UG/KG

4-Nitroaniline

1200

U

UG/KG

Acetophenone

3100

U

UG/KG

2-Methyl-4,6-Dinitrophenol

1200

U

UG/KG

(3-and/or 4-)Methylphenol

1200

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

1200

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

1200

U

UG/KG

Hexachloroethane

1200

UJ

UG/KG

4-Bromophenyl Phenyl Ether

1200

U

UG/KG

Nitrobenzene

1200

UJ

UG/KG

Hexachlorobenzene (HCB)

1200

U

UG/KG

Isophorone

1200

U

UG/KG

Atrazine

1200

U

UG/KG

2-Nitrophenol

3100

U

UG/KG

Pentachlorophenol

1200

U

UG/KG

2,4-Dimethylphenol

1200

U

UG/KG

Phenanthrene

1200

U

UG/KG

bis(2-Chloroethoxy)Methane

1200

U

UG/KG

Anthracene

1200

U

UG/KG

2,4-Dichlorophenol

1200

U

UG/KG

Carbazole

1200

U

UG/KG

Naphthalene

1200

U

UG/KG

Di-n-Butylphthalate

1200

u

UG/KG

4-Chloroaniline

1200

U

UG/KG

Fluoranthene

1200

u

UG/KG

Hexachlorobutadiene

1200

U

UG/KG

Pyrene

1200

u

UG/KG

Caprolactam

1200

U

UG/KG

Benzyl Butyl Phthalate

1200

u

UG/KG

4-Chloro-3-Methylphenol

1200

U

UG/KG

3,3'-Dichlorobenzidine

1200

u

UG/KG

2-Methylnaphthalene

1200

U

UG/KG

Benzo(a)Anthracene

1200

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

1200

U

UG/KG

Chrysene

1200

u

UG/KG

2,4,6-T richlorophenol

1200

U

UG/KG

bis(2-Ethylhexyl) Phthalate

3100

u

UG/KG

2,4,5-Trichlorophenol

1200

U

UG/KG

Di-n-Octylphthalate

1200

u

UG/KG

1,1 -Biphenyl

1200

u

UG/KG

Benzo(b)Fluoranthene

1200

u

UG/KG

2-Chloronaphthalene

1200

u

UG/KG

Benzo(k)Fluoranthene

3100

u

UG/KG

2-Nitroaniline

1200

u

UG/KG

Benzo-a-Pyrene

1200

u

UG/KG

Dimethyl Phthalate

1200

u

UG/KG

Indeno (1,2,3-cd) Pyrene

1200

u

UG/KG

2,6-Dinitrotoluene

1200

u

UG/KG

Dibenzo(a,h)Anthracene

1200

u

UG/KG

Acenaphthylene

1200

u

UG/KG

Benzo(ghi)Perylene

3100

u

UG/KG

3-Nitroaniline

73



%

% Moisture

1200

u

UG/KG

Acenaphthene









3100

u

UG/KG

2,4-Dinitrophenol









3100

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9525 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD05D/	MD No: 3AK1	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AK1	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

28 UNKNOWNS

58000

J

UG/KG

1500

NJ

UG/KG

4400

NJ

UG/KG

15-ISOBUTYL-(13ALPHAH)-ISOCOPALANE
STIGMAST-4-EN-3-ONE

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:45
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9526 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD03/

Media: SEDIMENT

Case No: 34717
MD No: 3AK2
D No: 3AK2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

720

U

UG/KG

Benzaldehyde

720

U

UG/KG

Dibenzofuran

720

U

UG/KG

Phenol

720

U

UG/KG

2,4-Dinitrotoluene

720

U

UG/KG

bis(2-Chloroethyl) Ether

720

U

UG/KG

Diethyl Phthalate

720

U

UG/KG

2-Chlorophenol

720

U

UG/KG

Fluorene

720

U

UG/KG

2-Methylphenol

720

U

UG/KG

4-Chlorophenyl Phenyl Ether

720

U

UG/KG

bis(2-Chloroisopropyl) Ether

1800

U

UG/KG

4-Nitroaniline

720

U

UG/KG

Acetophenone

1800

U

UG/KG

2-Methyl-4,6-Dinitrophenol

720

U

UG/KG

(3-and/or 4-)Methylphenol

720

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

720

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

720

U

UG/KG

Hexachloroethane

720

UJ

UG/KG

4-Bromophenyl Phenyl Ether

720

U

UG/KG

Nitrobenzene

720

UJ

UG/KG

Hexachlorobenzene (HCB)

720

U

UG/KG

Isophorone

720

U

UG/KG

Atrazine

720

U

UG/KG

2-Nitrophenol

1800

U

UG/KG

Pentachlorophenol

720

U

UG/KG

2,4-Dimethylphenol

720

U

UG/KG

Phenanthrene

720

U

UG/KG

bis(2-Chloroethoxy)Methane

720

U

UG/KG

Anthracene

720

U

UG/KG

2,4-Dichlorophenol

720

U

UG/KG

Carbazole

720

U

UG/KG

Naphthalene

720

U

UG/KG

Di-n-Butylphthalate

720

U

UG/KG

4-Chloroaniline

720

U

UG/KG

Fluoranthene

720

U

UG/KG

Hexachlorobutadiene

720

U

UG/KG

Pyrene

720

U

UG/KG

Caprolactam

720

U

UG/KG

Benzyl Butyl Phthalate

720

u

UG/KG

4-Chloro-3-Methylphenol

720

U

UG/KG

3,3'-Dichlorobenzidine

720

u

UG/KG

2-Methylnaphthalene

720

U

UG/KG

Benzo(a)Anthracene

720

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

720

U

UG/KG

Chrysene

720

u

UG/KG

2,4,6-T richlorophenol

720

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1800

u

UG/KG

2,4,5-Trichlorophenol

720

U

UG/KG

Di-n-Octylphthalate

720

u

UG/KG

1,1 -Biphenyl

720

U

UG/KG

Benzo(b)Fluoranthene

720

u

UG/KG

2-Chloronaphthalene

720

U

UG/KG

Benzo(k)Fluoranthene

1800

u

UG/KG

2-Nitroaniline

720

U

UG/KG

Benzo-a-Pyrene

720

u

UG/KG

Dimethyl Phthalate

720

u

UG/KG

Indeno (1,2,3-cd) Pyrene

720

u

UG/KG

2,6-Dinitrotoluene

720

u

UG/KG

Dibenzo(a,h)Anthracene

720

u

UG/KG

Acenaphthylene

720

u

UG/KG

Benzo(ghi)Perylene

1800

u

UG/KG

3-Nitroaniline

54



%

% Moisture

720

u

UG/KG

Acenaphthene









1800

u

UG/KG

2,4-Dinitrophenol









1800

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:40
Ending:

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

10000

J

UG/KG

24 UNKNOWNS

540

NJ

UG/KG

HEXADECENOIC ACID, Z-

500

NJ

UG/KG

N-HEXADECANOIC ACID

630

NJ

UG/KG

1-EICOSENE

840

NJ

UG/KG

TESTOSTERONE

Sample 9526 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD03 /	MD No: 3AK2

Media: SEDIMENT	D No: 3AK2

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9527 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD04/

Media: SEDIMENT

Case No: 34717
MD No: 3AK5
D No: 3AK5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

440

U

UG/KG

Benzaldehyde

440

U

UG/KG

Dibenzofuran

440

U

UG/KG

Phenol

440

U

UG/KG

2,4-Dinitrotoluene

440

U

UG/KG

bis(2-Chloroethyl) Ether

440

U

UG/KG

Diethyl Phthalate

440

U

UG/KG

2-Chlorophenol

440

U

UG/KG

Fluorene

440

U

UG/KG

2-Methylphenol

440

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

440

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

1100

U

UG/KG

4-Nitroaniline

440

U

UG/KG

Acetophenone

1100

U

UG/KG

2-Methyl-4,6-Dinitrophenol

440

U

UG/KG

(3-and/or 4-)Methylphenol

440

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

440

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

440

UJ

UG/KG

Hexachloroethane

440

U

UG/KG

4-Bromophenyl Phenyl Ether

440

U

UG/KG

Nitrobenzene

440

UJ

UG/KG

Hexachlorobenzene (HCB)

440

U

UG/KG

Isophorone

440

U

UG/KG

Atrazine

440

U

UG/KG

2-Nitrophenol

1100

U

UG/KG

Pentachlorophenol

440

U

UG/KG

2,4-Dimethylphenol

440

U

UG/KG

Phenanthrene

440

U

UG/KG

bis(2-Chloroethoxy)Methane

440

U

UG/KG

Anthracene

440

U

UG/KG

2,4-Dichlorophenol

440

U

UG/KG

Carbazole

440

U

UG/KG

Naphthalene

440

U

UG/KG

Di-n-Butylphthalate

440

U

UG/KG

4-Chloroaniline

440

U

UG/KG

Fluoranthene

440

u

UG/KG

Hexachlorobutadiene

440

U

UG/KG

Pyrene

440

u

UG/KG

Caprolactam

440

U

UG/KG

Benzyl Butyl Phthalate

440

u

UG/KG

4-Chloro-3-Methylphenol

440

U

UG/KG

3,3'-Dichlorobenzidine

440

u

UG/KG

2-Methylnaphthalene

440

U

UG/KG

Benzo(a)Anthracene

440

u

UG/KG

Hexachlorocyclopentadiene (HCCP)

440

U

UG/KG

Chrysene

440

u

UG/KG

2,4,6-T richlorophenol

440

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1100

u

UG/KG

2,4,5-Trichlorophenol

440

U

UG/KG

Di-n-Octylphthalate

440

u

UG/KG

1,1 -Biphenyl

440

U

UG/KG

Benzo(b)Fluoranthene

440

u

UG/KG

2-Chloronaphthalene

440

U

UG/KG

Benzo(k)Fluoranthene

1100

UJ

UG/KG

2-Nitroaniline

440

U

UG/KG

Benzo-a-Pyrene

440

u

UG/KG

Dimethyl Phthalate

440

u

UG/KG

Indeno (1,2,3-cd) Pyrene

440

u

UG/KG

2,6-Dinitrotoluene

440

u

UG/KG

Dibenzo(a,h)Anthracene

440

u

UG/KG

Acenaphthylene

440

u

UG/KG

Benzo(ghi)Perylene

1100

u

UG/KG

3-Nitroaniline

25



%

% Moisture

440

u

UG/KG

Acenaphthene









1100

u

UG/KG

2,4-Dinitrophenol









1100

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9527 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD04/

Media: SEDIMENT

Case No: 34717
MD No: 3AK5
D No: 3AK5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

RESULTS UNITS

4100 J UG/KG

ANALYTE

17 UNKNOWNS

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9528 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AF9
D No: 3AF9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1500

U

UG/KG

Benzaldehyde

1500

U

UG/KG

Dibenzofuran

1500

U

UG/KG

Phenol

1500

U

UG/KG

2,4-Dinitrotoluene

1500

U

UG/KG

bis(2-Chloroethyl) Ether

1500

U

UG/KG

Diethyl Phthalate

1500

U

UG/KG

2-Chlorophenol

1500

U

UG/KG

Fluorene

1500

U

UG/KG

2-Methylphenol

1500

U

UG/KG

4-Chlorophenyl Phenyl Ether

1500

U

UG/KG

bis(2-Chloroisopropyl) Ether

3800

U

UG/KG

4-Nitroaniline

1500

U

UG/KG

Acetophenone

3800

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

1500

U

UG/KG

(3-and/or 4-)Methylphenol

1500

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

1500

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

1500

U

UG/KG

Hexachloroethane

1500

U

UG/KG

4-Bromophenyl Phenyl Ether

1500

U

UG/KG

Nitrobenzene

1500

U

UG/KG

Hexachlorobenzene (HCB)

1500

U

UG/KG

Isophorone

1500

U

UG/KG

Atrazine

1500

U

UG/KG

2-Nitrophenol

3800

U

UG/KG

Pentachlorophenol

1500

U

UG/KG

2,4-Dimethylphenol

1500

U

UG/KG

Phenanthrene

1500

U

UG/KG

bis(2-Chloroethoxy)Methane

1500

U

UG/KG

Anthracene

1500

U

UG/KG

2,4-Dichlorophenol

1500

U

UG/KG

Carbazole

1500

U

UG/KG

Naphthalene

1500

U

UG/KG

Di-n-Butylphthalate

1500

U

UG/KG

4-Chloroaniline

1500

U

UG/KG

Fluoranthene

1500

U

UG/KG

Hexachlorobutadiene

1500

U

UG/KG

Pyrene

1500

UR

UG/KG

Caprolactam

1500

U

UG/KG

Benzyl Butyl Phthalate

1500

U

UG/KG

4-Chloro-3-Methylphenol

1500

U

UG/KG

3,3'-Dichlorobenzidine

1500

U

UG/KG

2-Methylnaphthalene

1500

U

UG/KG

Benzo(a)Anthracene

1500

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

1500

U

UG/KG

Chrysene

1500

U

UG/KG

2,4,6-T richlorophenol

1500

U

UG/KG

bis(2-Ethylhexyl) Phthalate

3800

U

UG/KG

2,4,5-Trichlorophenol

1500

U

UG/KG

Di-n-Octylphthalate

1500

U

UG/KG

1,1 -Biphenyl

1500

u

UG/KG

Benzo(b)Fluoranthene

1500

u

UG/KG

2-Chloronaphthalene

1500

u

UG/KG

Benzo(k)Fluoranthene

3800

u

UG/KG

2-Nitroaniline

1500

u

UG/KG

Benzo-a-Pyrene

1500

u

UG/KG

Dimethyl Phthalate

1500

u

UG/KG

Indeno (1,2,3-cd) Pyrene

1500

u

UG/KG

2,6-Dinitrotoluene

1500

u

UG/KG

Dibenzo(a,h)Anthracene

1500

u

UG/KG

Acenaphthylene

1500

UJ

UG/KG

Benzo(ghi)Perylene

3800

u

UG/KG

3-Nitroaniline

78



%

% Moisture

1500

u

UG/KG

Acenaphthene









3800

UJ

UG/KG

2,4-Dinitrophenol









3800

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9528 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AF9
D No: 3AF9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:25
Ending:

RESULTS UNITS

20000 J UG/KG
N UG/KG

ANALYTE

19 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9529 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD01D/

Media: SEDIMENT

Case No: 34717
MD No: 3AG0
D No: 3AG0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1700

U

UG/KG

Benzaldehyde

1700

U

UG/KG

Dibenzofuran

1700

U

UG/KG

Phenol

1700

U

UG/KG

2,4-Dinitrotoluene

1700

U

UG/KG

bis(2-Chloroethyl) Ether

1700

U

UG/KG

Diethyl Phthalate

1700

U

UG/KG

2-Chlorophenol

1700

U

UG/KG

Fluorene

1700

U

UG/KG

2-Methylphenol

1700

U

UG/KG

4-Chlorophenyl Phenyl Ether

1700

U

UG/KG

bis(2-Chloroisopropyl) Ether

4200

U

UG/KG

4-Nitroaniline

1700

U

UG/KG

Acetophenone

4200

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

1700

U

UG/KG

(3-and/or 4-)Methylphenol

1700

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

1700

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

1700

U

UG/KG

Hexachloroethane

1700

U

UG/KG

4-Bromophenyl Phenyl Ether

1700

U

UG/KG

Nitrobenzene

1700

U

UG/KG

Hexachlorobenzene (HCB)

1700

U

UG/KG

Isophorone

1700

U

UG/KG

Atrazine

1700

U

UG/KG

2-Nitrophenol

4200

U

UG/KG

Pentachlorophenol

1700

U

UG/KG

2,4-Dimethylphenol

1700

U

UG/KG

Phenanthrene

1700

U

UG/KG

bis(2-Chloroethoxy)Methane

1700

U

UG/KG

Anthracene

1700

U

UG/KG

2,4-Dichlorophenol

1700

U

UG/KG

Carbazole

1700

U

UG/KG

Naphthalene

1700

U

UG/KG

Di-n-Butylphthalate

1700

U

UG/KG

4-Chloroaniline

1700

U

UG/KG

Fluoranthene

1700

U

UG/KG

Hexachlorobutadiene

1700

U

UG/KG

Pyrene

1700

UR

UG/KG

Caprolactam

1700

U

UG/KG

Benzyl Butyl Phthalate

1700

U

UG/KG

4-Chloro-3-Methylphenol

1700

U

UG/KG

3,3'-Dichlorobenzidine

1700

U

UG/KG

2-Methylnaphthalene

1700

U

UG/KG

Benzo(a)Anthracene

1700

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

1700

U

UG/KG

Chrysene

1700

U

UG/KG

2,4,6-T richlorophenol

1700

U

UG/KG

bis(2-Ethylhexyl) Phthalate

4200

U

UG/KG

2,4,5-Trichlorophenol

1700

u

UG/KG

Di-n-Octylphthalate

1700

U

UG/KG

1,1 -Biphenyl

1700

u

UG/KG

Benzo(b)Fluoranthene

1700

u

UG/KG

2-Chloronaphthalene

1700

u

UG/KG

Benzo(k)Fluoranthene

4200

u

UG/KG

2-Nitroaniline

1700

u

UG/KG

Benzo-a-Pyrene

1700

u

UG/KG

Dimethyl Phthalate

1700

u

UG/KG

Indeno (1,2,3-cd) Pyrene

1700

u

UG/KG

2,6-Dinitrotoluene

1700

u

UG/KG

Dibenzo(a,h)Anthracene

1700

u

UG/KG

Acenaphthylene

1700

UJ

UG/KG

Benzo(ghi)Perylene

4200

u

UG/KG

3-Nitroaniline

80



%

% Moisture

1700

u

UG/KG

Acenaphthene









4200

UJ

UG/KG

2,4-Dinitrophenol









4200

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9529 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD01D/

Media: SEDIMENT

Case No: 34717
MD No: 3AG0
D No: 3AG0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:40
Ending:

RESULTS UNITS

8900 J UG/KG
N UG/KG

ANALYTE

11 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9530 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG1
D No: 3AG1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

790

U

UG/KG

Benzaldehyde

790

U

UG/KG

Dibenzofuran

790

U

UG/KG

Phenol

790

U

UG/KG

2,4-Dinitrotoluene

790

U

UG/KG

bis(2-Chloroethyl) Ether

790

U

UG/KG

Diethyl Phthalate

790

U

UG/KG

2-Chlorophenol

790

U

UG/KG

Fluorene

790

U

UG/KG

2-Methylphenol

790

U

UG/KG

4-Chlorophenyl Phenyl Ether

790

U

UG/KG

bis(2-Chloroisopropyl) Ether

2000

U

UG/KG

4-Nitroaniline

170

J

UG/KG

Acetophenone

2000

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

790

U

UG/KG

(3-and/or 4-)Methylphenol

790

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

790

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

790

U

UG/KG

Hexachloroethane

790

U

UG/KG

4-Bromophenyl Phenyl Ether

790

U

UG/KG

Nitrobenzene

790

U

UG/KG

Hexachlorobenzene (HCB)

790

U

UG/KG

Isophorone

790

U

UG/KG

Atrazine

790

U

UG/KG

2-Nitrophenol

2000

U

UG/KG

Pentachlorophenol

790

U

UG/KG

2,4-Dimethylphenol

790

U

UG/KG

Phenanthrene

790

U

UG/KG

bis(2-Chloroethoxy)Methane

790

U

UG/KG

Anthracene

790

U

UG/KG

2,4-Dichlorophenol

790

U

UG/KG

Carbazole

790

U

UG/KG

Naphthalene

790

U

UG/KG

Di-n-Butylphthalate

790

U

UG/KG

4-Chloroaniline

790

U

UG/KG

Fluoranthene

790

U

UG/KG

Hexachlorobutadiene

790

U

UG/KG

Pyrene

790

UR

UG/KG

Caprolactam

790

U

UG/KG

Benzyl Butyl Phthalate

790

U

UG/KG

4-Chloro-3-Methylphenol

790

U

UG/KG

3,3'-Dichlorobenzidine

790

U

UG/KG

2-Methylnaphthalene

790

U

UG/KG

Benzo(a)Anthracene

790

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

790

U

UG/KG

Chrysene

790

U

UG/KG

2,4,6-T richlorophenol

790

U

UG/KG

bis(2-Ethylhexyl) Phthalate

2000

U

UG/KG

2,4,5-Trichlorophenol

790

U

UG/KG

Di-n-Octylphthalate

790

U

UG/KG

1,1 -Biphenyl

790

U

UG/KG

Benzo(b)Fluoranthene

790

u

UG/KG

2-Chloronaphthalene

790

U

UG/KG

Benzo(k)Fluoranthene

2000

u

UG/KG

2-Nitroaniline

790

U

UG/KG

Benzo-a-Pyrene

790

u

UG/KG

Dimethyl Phthalate

790

u

UG/KG

Indeno (1,2,3-cd) Pyrene

790

u

UG/KG

2,6-Dinitrotoluene

790

u

UG/KG

Dibenzo(a,h)Anthracene

790

u

UG/KG

Acenaphthylene

790

UJ

UG/KG

Benzo(ghi)Perylene

2000

u

UG/KG

3-Nitroaniline

58



%

% Moisture

790

u

UG/KG

Acenaphthene









2000

UJ

UG/KG

2,4-Dinitrophenol









2000

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9530 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG1
D No: 3AG1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

RESULTS UNITS

25000 J UG/KG
N UG/KG

ANALYTE

28 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9531 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD03 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG2
D No: 3AG2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

400

U

UG/KG

Benzaldehyde

400

U

UG/KG

Dibenzofuran

400

U

UG/KG

Phenol

400

U

UG/KG

2,4-Dinitrotoluene

400

U

UG/KG

bis(2-Chloroethyl) Ether

400

U

UG/KG

Diethyl Phthalate

400

U

UG/KG

2-Chlorophenol

400

U

UG/KG

Fluorene

400

U

UG/KG

2-Methylphenol

400

U

UG/KG

4-Chlorophenyl Phenyl Ether

400

U

UG/KG

bis(2-Chloroisopropyl) Ether

1000

U

UG/KG

4-Nitroaniline

400

U

UG/KG

Acetophenone

1000

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

400

u

UG/KG

(3-and/or 4-)Methylphenol

400

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

400

u

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

400

u

UG/KG

Hexachloroethane

400

U

UG/KG

4-Bromophenyl Phenyl Ether

400

u

UG/KG

Nitrobenzene

400

U

UG/KG

Hexachlorobenzene (HCB)

400

u

UG/KG

Isophorone

400

U

UG/KG

Atrazine

400

u

UG/KG

2-Nitrophenol

1000

U

UG/KG

Pentachlorophenol

400

u

UG/KG

2,4-Dimethylphenol

180

J

UG/KG

Phenanthrene

400

u

UG/KG

bis(2-Chloroethoxy)Methane

400

U

UG/KG

Anthracene

400

u

UG/KG

2,4-Dichlorophenol

400

U

UG/KG

Carbazole

400

u

UG/KG

Naphthalene

400

U

UG/KG

Di-n-Butylphthalate

400

u

UG/KG

4-Chloroaniline

400



UG/KG

Fluoranthene

400

u

UG/KG

Hexachlorobutadiene

370

J

UG/KG

Pyrene

400

UR

UG/KG

Caprolactam

400

U

UG/KG

Benzyl Butyl Phthalate

400

u

UG/KG

4-Chloro-3-Methylphenol

400

U

UG/KG

3,3'-Dichlorobenzidine

400

u

UG/KG

2-Methylnaphthalene

220

J

UG/KG

Benzo(a)Anthracene

400

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

280

J

UG/KG

Chrysene

400

u

UG/KG

2,4,6-T richlorophenol

400

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1000

u

UG/KG

2,4,5-Trichlorophenol

400

U

UG/KG

Di-n-Octylphthalate

400

u

UG/KG

1,1 -Biphenyl

210

J

UG/KG

Benzo(b)Fluoranthene

400

u

UG/KG

2-Chloronaphthalene

230

J

UG/KG

Benzo(k)Fluoranthene

1000

u

UG/KG

2-Nitroaniline

200

J

UG/KG

Benzo-a-Pyrene

400

u

UG/KG

Dimethyl Phthalate

150

J

UG/KG

Indeno (1,2,3-cd) Pyrene

400

u

UG/KG

2,6-Dinitrotoluene

400

U

UG/KG

Dibenzo(a,h)Anthracene

400

u

UG/KG

Acenaphthylene

120

J

UG/KG

Benzo(ghi)Perylene

1000

u

UG/KG

3-Nitroaniline

17



%

% Moisture

400

u

UG/KG

Acenaphthene









1000

UJ

UG/KG

2,4-Dinitrophenol









1000

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9531 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD03 /	MD No: 3AG2	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AG2	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

300

J

UG/KG

3 UNKNOWNS

190

NJ

UG/KG

UNKNOWN PAH



N

UG/KG

PETROLEUM PRODUCT

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9532 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF04 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG3
D No: 3AG3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

U

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

U

UG/KG

4-Chlorophenyl Phenyl Ether

380

U

UG/KG

bis(2-Chloroisopropyl) Ether

940

U

UG/KG

4-Nitroaniline

380

U

UG/KG

Acetophenone

940

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

U

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

U

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

U

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

940

U

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

UR

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

U

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

940

U

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

U

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

U

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

940

U

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

U

UG/KG

Dimethyl Phthalate

380

u

UG/KG

Indeno (1,2,3-cd) Pyrene

380

u

UG/KG

2,6-Dinitrotoluene

380

u

UG/KG

Dibenzo(a,h)Anthracene

380

u

UG/KG

Acenaphthylene

380

UJ

UG/KG

Benzo(ghi)Perylene

940

u

UG/KG

3-Nitroaniline

12



%

% Moisture

380

u

UG/KG

Acenaphthene









940

UJ

UG/KG

2,4-Dinitrophenol









940

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9532 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF04 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG3
D No: 3AG3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:50
Ending:

RESULTS UNITS

8400 J UG/KG
N UG/KG

ANALYTE

27 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9533 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF05 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG4
D No: 3AG4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

U

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

U

UG/KG

4-Chlorophenyl Phenyl Ether

380

U

UG/KG

bis(2-Chloroisopropyl) Ether

950

U

UG/KG

4-Nitroaniline

380

U

UG/KG

Acetophenone

950

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

U

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

U

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

U

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

950

U

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

UR

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

U

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

950

U

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

U

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

U

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

950

U

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

U

UG/KG

Dimethyl Phthalate

380

u

UG/KG

Indeno (1,2,3-cd) Pyrene

380

u

UG/KG

2,6-Dinitrotoluene

380

u

UG/KG

Dibenzo(a,h)Anthracene

380

u

UG/KG

Acenaphthylene

380

UJ

UG/KG

Benzo(ghi)Perylene

950

u

UG/KG

3-Nitroaniline

13



%

% Moisture

380

u

UG/KG

Acenaphthene









950

UJ

UG/KG

2,4-Dinitrophenol









950

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9533 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF05 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG4
D No: 3AG4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

RESULTS UNITS

21000 J UG/KG
N UG/KG

ANALYTE

20 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9534 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF05S /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG5
D No: 3AG5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

U

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

U

UG/KG

4-Chlorophenyl Phenyl Ether

380

U

UG/KG

bis(2-Chloroisopropyl) Ether

950

U

UG/KG

4-Nitroaniline

380

U

UG/KG

Acetophenone

950

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

U

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

U

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

U

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

950

U

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

UR

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

U

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

950

U

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

U

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

U

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

950

U

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

U

UG/KG

Dimethyl Phthalate

380

u

UG/KG

Indeno (1,2,3-cd) Pyrene

380

u

UG/KG

2,6-Dinitrotoluene

380

u

UG/KG

Dibenzo(a,h)Anthracene

380

u

UG/KG

Acenaphthylene

380

UJ

UG/KG

Benzo(ghi)Perylene

950

u

UG/KG

3-Nitroaniline

13



%

% Moisture

380

u

UG/KG

Acenaphthene









950

UJ

UG/KG

2,4-Dinitrophenol









950

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9534 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSF05S /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AG5
D No: 3AG5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

RESULTS UNITS

34000 J UG/KG
N UG/KG

ANALYTE

22 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9535 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG7
D No: 3AG7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

UJ

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

U

UG/KG

4-Chlorophenyl Phenyl Ether

380

U

UG/KG

bis(2-Chloroisopropyl) Ether

970

U

UG/KG

4-Nitroaniline

91

J

UG/KG

Acetophenone

970

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

U

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

U

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

UJ

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

970

UJ

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

UR

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

UJ

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

970

U

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

U

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

U

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

970

U

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

570



UG/KG

Dimethyl Phthalate

380

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

380

U

UG/KG

2,6-Dinitrotoluene

380

UJ

UG/KG

Dibenzo(a,h)Anthracene

380

U

UG/KG

Acenaphthylene

380

UJ

UG/KG

Benzo(ghi)Perylene

970

u

UG/KG

3-Nitroaniline

14



%

% Moisture

380

u

UG/KG

Acenaphthene









970

UJ

UG/KG

2,4-Dinitrophenol









970

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9535 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG7
D No: 3AG7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:00
Ending:

RESULTS UNITS

7300 J UG/KG
N UG/KG

ANALYTE

28 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9536 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD02D /

Media: SEDIMENT

Case No: 34717
MD No: 3AG8
D No: 3AG8

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

410

UJ

UG/KG

Benzaldehyde

410

U

UG/KG

Dibenzofuran

410

U

UG/KG

Phenol

410

U

UG/KG

2,4-Dinitrotoluene

410

U

UG/KG

bis(2-Chloroethyl) Ether

410

U

UG/KG

Diethyl Phthalate

410

U

UG/KG

2-Chlorophenol

410

U

UG/KG

Fluorene

410

U

UG/KG

2-Methylphenol

410

U

UG/KG

4-Chlorophenyl Phenyl Ether

410

U

UG/KG

bis(2-Chloroisopropyl) Ether

1000

U

UG/KG

4-Nitroaniline

410

U

UG/KG

Acetophenone

1000

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

410

U

UG/KG

(3-and/or 4-)Methylphenol

410

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

410

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

410

U

UG/KG

Hexachloroethane

410

U

UG/KG

4-Bromophenyl Phenyl Ether

410

U

UG/KG

Nitrobenzene

410

U

UG/KG

Hexachlorobenzene (HCB)

410

u

UG/KG

Isophorone

410

UJ

UG/KG

Atrazine

410

u

UG/KG

2-Nitrophenol

1000

UJ

UG/KG

Pentachlorophenol

410

u

UG/KG

2,4-Dimethylphenol

410

U

UG/KG

Phenanthrene

410

u

UG/KG

bis(2-Chloroethoxy)Methane

410

U

UG/KG

Anthracene

410

u

UG/KG

2,4-Dichlorophenol

410

U

UG/KG

Carbazole

410

u

UG/KG

Naphthalene

410

U

UG/KG

Di-n-Butylphthalate

410

u

UG/KG

4-Chloroaniline

410

U

UG/KG

Fluoranthene

410

u

UG/KG

Hexachlorobutadiene

410

U

UG/KG

Pyrene

410

UR

UG/KG

Caprolactam

410

U

UG/KG

Benzyl Butyl Phthalate

410

u

UG/KG

4-Chloro-3-Methylphenol

410

UJ

UG/KG

3,3'-Dichlorobenzidine

410

u

UG/KG

2-Methylnaphthalene

410

U

UG/KG

Benzo(a)Anthracene

410

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

410

U

UG/KG

Chrysene

410

u

UG/KG

2,4,6-T richlorophenol

410

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1000

u

UG/KG

2,4,5-Trichlorophenol

410

U

UG/KG

Di-n-Octylphthalate

410

u

UG/KG

1,1 -Biphenyl

410

U

UG/KG

Benzo(b)Fluoranthene

410

u

UG/KG

2-Chloronaphthalene

410

U

UG/KG

Benzo(k)Fluoranthene

1000

u

UG/KG

2-Nitroaniline

410

u

UG/KG

Benzo-a-Pyrene

410

u

UG/KG

Dimethyl Phthalate

410

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

410

u

UG/KG

2,6-Dinitrotoluene

410

UJ

UG/KG

Dibenzo(a,h)Anthracene

410

u

UG/KG

Acenaphthylene

410

UJ

UG/KG

Benzo(ghi)Perylene

1000

u

UG/KG

3-Nitroaniline

19



%

% Moisture

410

u

UG/KG

Acenaphthene









1000

UJ

UG/KG

2,4-Dinitrophenol









1000

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9536 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD02D /

Media: SEDIMENT

Case No: 34717
MD No: 3AG8
D No: 3AG8

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:25
Ending:

RESULTS UNITS

6200 J UG/KG
N UG/KG

ANALYTE

24 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9537 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG9
D No: 3AG9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

350

UJ

UG/KG

Benzaldehyde

350

U

UG/KG

Dibenzofuran

350

U

UG/KG

Phenol

350

U

UG/KG

2,4-Dinitrotoluene

350

U

UG/KG

bis(2-Chloroethyl) Ether

350

U

UG/KG

Diethyl Phthalate

350

U

UG/KG

2-Chlorophenol

350

U

UG/KG

Fluorene

350

U

UG/KG

2-Methylphenol

350

U

UG/KG

4-Chlorophenyl Phenyl Ether

350

U

UG/KG

bis(2-Chloroisopropyl) Ether

880

U

UG/KG

4-Nitroaniline

300

J

UG/KG

Acetophenone

880

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

350

U

UG/KG

(3-and/or 4-)Methylphenol

350

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

350

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

350

U

UG/KG

Hexachloroethane

350

U

UG/KG

4-Bromophenyl Phenyl Ether

350

U

UG/KG

Nitrobenzene

350

U

UG/KG

Hexachlorobenzene (HCB)

350

U

UG/KG

Isophorone

350

UJ

UG/KG

Atrazine

350

U

UG/KG

2-Nitrophenol

880

UJ

UG/KG

Pentachlorophenol

350

U

UG/KG

2,4-Dimethylphenol

140

J

UG/KG

Phenanthrene

350

U

UG/KG

bis(2-Chloroethoxy)Methane

120

J

UG/KG

Anthracene

350

U

UG/KG

2,4-Dichlorophenol

350

U

UG/KG

Carbazole

350

U

UG/KG

Naphthalene

350

U

UG/KG

Di-n-Butylphthalate

350

U

UG/KG

4-Chloroaniline

1900



UG/KG

Fluoranthene

350

U

UG/KG

Hexachlorobutadiene

2000



UG/KG

Pyrene

350

UR

UG/KG

Caprolactam

350

U

UG/KG

Benzyl Butyl Phthalate

350

U

UG/KG

4-Chloro-3-Methylphenol

350

UJ

UG/KG

3,3'-Dichlorobenzidine

350

U

UG/KG

2-Methylnaphthalene

1200



UG/KG

Benzo(a)Anthracene

350

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

1200



UG/KG

Chrysene

350

U

UG/KG

2,4,6-T richlorophenol

350

U

UG/KG

bis(2-Ethylhexyl) Phthalate

880

U

UG/KG

2,4,5-Trichlorophenol

350

U

UG/KG

Di-n-Octylphthalate

350

U

UG/KG

1,1 -Biphenyl

1600



UG/KG

Benzo(b)Fluoranthene

350

U

UG/KG

2-Chloronaphthalene

890



UG/KG

Benzo(k)Fluoranthene

880

U

UG/KG

2-Nitroaniline

1300



UG/KG

Benzo-a-Pyrene

350

U

UG/KG

Dimethyl Phthalate

1100

J

UG/KG

Indeno (1,2,3-cd) Pyrene

350

u

UG/KG

2,6-Dinitrotoluene

360

J

UG/KG

Dibenzo(a,h)Anthracene

160

J

UG/KG

Acenaphthylene

750

J

UG/KG

Benzo(ghi)Perylene

880

u

UG/KG

3-Nitroaniline

6



%

% Moisture

350

u

UG/KG

Acenaphthene









880

UJ

UG/KG

2,4-Dinitrophenol









880

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:50
Ending:

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

10000 J

UG/KG

22 UNKNOWNS

250 NJ

UG/KG

CYCLOPENTA(DEF) PHENANTHRENONE

550 NJ

UG/KG

11H-BENZO [B] FLUORENE

380 NJ

UG/KG

2 PYRENE, 1-METHYL-

470 NJ

UG/KG

BENZO [E] PYRENE

N

UG/KG

PETROLEUM PRODUCT

1100 NJ

UG/KG

UNKNOWN PAH

Sample 9537 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD01 /	MD No: 3AG9

Media: SEDIMENT	D No: 3AG9

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9538 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD03 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH0
D No: 3AH0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1700

J

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

11000



UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

U

UG/KG

4-Chlorophenyl Phenyl Ether

380

U

UG/KG

bis(2-Chloroisopropyl) Ether

970

U

UG/KG

4-Nitroaniline

8400



UG/KG

Acetophenone

970

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

U

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

U

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

UJ

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

970

UJ

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

320

J

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

270

J

UG/KG

Pyrene

380

UR

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

UJ

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

95

J

UG/KG

Benzo(a)Anthracene

380

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

220

J

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

970

U

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

U

UG/KG

1,1 -Biphenyl

210

J

UG/KG

Benzo(b)Fluoranthene

380

U

UG/KG

2-Chloronaphthalene

130

J

UG/KG

Benzo(k)Fluoranthene

970

U

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

U

UG/KG

Dimethyl Phthalate

87

J

UG/KG

Indeno (1,2,3-cd) Pyrene

380

U

UG/KG

2,6-Dinitrotoluene

380

U

UG/KG

Dibenzo(a,h)Anthracene

380

U

UG/KG

Acenaphthylene

380

U

UG/KG

Benzo(ghi)Perylene

970

u

UG/KG

3-Nitroaniline

14



%

% Moisture

380

u

UG/KG

Acenaphthene









970

UJ

UG/KG

2,4-Dinitrophenol









970

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:20
Ending:

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

98000

J

UG/KG

24 UNKNOWNS

550

NJ

UG/KG

2-BUTEN-1-ONE, 1,3-DIPHENYL-

480

NJ

UG/KG

6,7,8,9-BENZO[B]FLUORENE

6800

NJ

UG/KG

1,3-PROPANEDIONE, 1,3-DIPHENYL-

1700

NJ

UG/KG

1,3,5-TRIPHENYL-1,5-PENTANEDIONE

370

NJ

UG/KG

1,V:3',V ':3' ',1'' '-QUATERPHENYL



N

UG/KG

PETROLEUM PRODUCT

Sample 9538 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD03 /	MD No: 3AH0

Media: SEDIMENT	D No: 3AH0

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9539 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF01 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH1
D No: 3AH1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

520

UJ

UG/KG

Benzaldehyde

520

U

UG/KG

Dibenzofuran

520

U

UG/KG

Phenol

520

U

UG/KG

2,4-Dinitrotoluene

520

U

UG/KG

bis(2-Chloroethyl) Ether

520

U

UG/KG

Diethyl Phthalate

520

U

UG/KG

2-Chlorophenol

520

U

UG/KG

Fluorene

520

U

UG/KG

2-Methylphenol

520

U

UG/KG

4-Chlorophenyl Phenyl Ether

520

U

UG/KG

bis(2-Chloroisopropyl) Ether

1300

U

UG/KG

4-Nitroaniline

170

J

UG/KG

Acetophenone

1300

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

520

U

UG/KG

(3-and/or 4-)Methylphenol

520

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

520

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

520

U

UG/KG

Hexachloroethane

520

U

UG/KG

4-Bromophenyl Phenyl Ether

520

U

UG/KG

Nitrobenzene

520

U

UG/KG

Hexachlorobenzene (HCB)

520

U

UG/KG

Isophorone

520

UJ

UG/KG

Atrazine

520

U

UG/KG

2-Nitrophenol

1300

UJ

UG/KG

Pentachlorophenol

520

U

UG/KG

2,4-Dimethylphenol

520

U

UG/KG

Phenanthrene

520

U

UG/KG

bis(2-Chloroethoxy)Methane

520

U

UG/KG

Anthracene

520

U

UG/KG

2,4-Dichlorophenol

520

U

UG/KG

Carbazole

520

U

UG/KG

Naphthalene

520

U

UG/KG

Di-n-Butylphthalate

520

U

UG/KG

4-Chloroaniline

520

U

UG/KG

Fluoranthene

520

U

UG/KG

Hexachlorobutadiene

520

U

UG/KG

Pyrene

520

UR

UG/KG

Caprolactam

520

U

UG/KG

Benzyl Butyl Phthalate

520

U

UG/KG

4-Chloro-3-Methylphenol

520

UJ

UG/KG

3,3'-Dichlorobenzidine

520

U

UG/KG

2-Methylnaphthalene

520

U

UG/KG

Benzo(a)Anthracene

520

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

520

U

UG/KG

Chrysene

520

U

UG/KG

2,4,6-T richlorophenol

860

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1300

U

UG/KG

2,4,5-Trichlorophenol

520

U

UG/KG

Di-n-Octylphthalate

520

U

UG/KG

1,1 -Biphenyl

520

U

UG/KG

Benzo(b)Fluoranthene

520

U

UG/KG

2-Chloronaphthalene

520

U

UG/KG

Benzo(k)Fluoranthene

1300

u

UG/KG

2-Nitroaniline

520

U

UG/KG

Benzo-a-Pyrene

520

u

UG/KG

Dimethyl Phthalate

520

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

520

u

UG/KG

2,6-Dinitrotoluene

520

UJ

UG/KG

Dibenzo(a,h)Anthracene

520

u

UG/KG

Acenaphthylene

520

UJ

UG/KG

Benzo(ghi)Perylene

1300

u

UG/KG

3-Nitroaniline

36



%

% Moisture

520

u

UG/KG

Acenaphthene









1300

UJ

UG/KG

2,4-Dinitrophenol









1300

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9539 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF01 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH1
D No: 3AH1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

RESULTS UNITS

11000 J
N

UG/KG
UG/KG

ANALYTE

27 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9540 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF01S/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH2
D No: 3AH2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

520

UJ

UG/KG

Benzaldehyde

520

U

UG/KG

Dibenzofuran

520

U

UG/KG

Phenol

520

U

UG/KG

2,4-Dinitrotoluene

520

U

UG/KG

bis(2-Chloroethyl) Ether

520

U

UG/KG

Diethyl Phthalate

520

U

UG/KG

2-Chlorophenol

520

U

UG/KG

Fluorene

520

U

UG/KG

2-Methylphenol

520

U

UG/KG

4-Chlorophenyl Phenyl Ether

520

U

UG/KG

bis(2-Chloroisopropyl) Ether

1300

U

UG/KG

4-Nitroaniline

520

U

UG/KG

Acetophenone

1300

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

520

U

UG/KG

(3-and/or 4-)Methylphenol

520

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

520

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

520

U

UG/KG

Hexachloroethane

520

U

UG/KG

4-Bromophenyl Phenyl Ether

520

U

UG/KG

Nitrobenzene

520

U

UG/KG

Hexachlorobenzene (HCB)

520

U

UG/KG

Isophorone

520

UJ

UG/KG

Atrazine

520

U

UG/KG

2-Nitrophenol

1300

UJ

UG/KG

Pentachlorophenol

520

U

UG/KG

2,4-Dimethylphenol

520

U

UG/KG

Phenanthrene

520

U

UG/KG

bis(2-Chloroethoxy)Methane

520

U

UG/KG

Anthracene

520

U

UG/KG

2,4-Dichlorophenol

520

U

UG/KG

Carbazole

520

U

UG/KG

Naphthalene

520

U

UG/KG

Di-n-Butylphthalate

520

U

UG/KG

4-Chloroaniline

520

U

UG/KG

Fluoranthene

520

U

UG/KG

Hexachlorobutadiene

520

U

UG/KG

Pyrene

520

UR

UG/KG

Caprolactam

520

U

UG/KG

Benzyl Butyl Phthalate

520

U

UG/KG

4-Chloro-3-Methylphenol

520

UJ

UG/KG

3,3'-Dichlorobenzidine

520

U

UG/KG

2-Methylnaphthalene

520

U

UG/KG

Benzo(a)Anthracene

520

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

520

U

UG/KG

Chrysene

520

U

UG/KG

2,4,6-T richlorophenol

1200

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1300

U

UG/KG

2,4,5-Trichlorophenol

520

U

UG/KG

Di-n-Octylphthalate

520

U

UG/KG

1,1 -Biphenyl

520

U

UG/KG

Benzo(b)Fluoranthene

520

U

UG/KG

2-Chloronaphthalene

520

U

UG/KG

Benzo(k)Fluoranthene

1300

u

UG/KG

2-Nitroaniline

520

U

UG/KG

Benzo-a-Pyrene

520

u

UG/KG

Dimethyl Phthalate

520

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

520

u

UG/KG

2,6-Dinitrotoluene

520

UJ

UG/KG

Dibenzo(a,h)Anthracene

520

u

UG/KG

Acenaphthylene

520

UJ

UG/KG

Benzo(ghi)Perylene

1300

u

UG/KG

3-Nitroaniline

36



%

% Moisture

520

u

UG/KG

Acenaphthene









1300

UJ

UG/KG

2,4-Dinitrophenol









1300

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9540 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF01S/

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH2
D No: 3AH2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

RESULTS UNITS

20000 J UG/KG
N UG/KG

ANALYTE

28 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9541 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF02 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH3
D No: 3AH3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

360

UJ

UG/KG

Benzaldehyde

360

U

UG/KG

Dibenzofuran

360

U

UG/KG

Phenol

360

U

UG/KG

2,4-Dinitrotoluene

360

U

UG/KG

bis(2-Chloroethyl) Ether

360

U

UG/KG

Diethyl Phthalate

360

U

UG/KG

2-Chlorophenol

360

U

UG/KG

Fluorene

360

U

UG/KG

2-Methylphenol

360

U

UG/KG

4-Chlorophenyl Phenyl Ether

360

U

UG/KG

bis(2-Chloroisopropyl) Ether

910

U

UG/KG

4-Nitroaniline

360

U

UG/KG

Acetophenone

910

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

360

U

UG/KG

(3-and/or 4-)Methylphenol

360

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

360

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

360

U

UG/KG

Hexachloroethane

360

U

UG/KG

4-Bromophenyl Phenyl Ether

360

U

UG/KG

Nitrobenzene

360

U

UG/KG

Hexachlorobenzene (HCB)

360

U

UG/KG

Isophorone

360

UJ

UG/KG

Atrazine

360

U

UG/KG

2-Nitrophenol

910

UJ

UG/KG

Pentachlorophenol

360

U

UG/KG

2,4-Dimethylphenol

360

U

UG/KG

Phenanthrene

360

U

UG/KG

bis(2-Chloroethoxy)Methane

360

U

UG/KG

Anthracene

360

U

UG/KG

2,4-Dichlorophenol

360

U

UG/KG

Carbazole

360

U

UG/KG

Naphthalene

360

U

UG/KG

Di-n-Butylphthalate

360

U

UG/KG

4-Chloroaniline

110

J

UG/KG

Fluoranthene

360

U

UG/KG

Hexachlorobutadiene

150

J

UG/KG

Pyrene

360

UR

UG/KG

Caprolactam

360

U

UG/KG

Benzyl Butyl Phthalate

360

U

UG/KG

4-Chloro-3-Methylphenol

360

UJ

UG/KG

3,3'-Dichlorobenzidine

360

U

UG/KG

2-Methylnaphthalene

360

U

UG/KG

Benzo(a)Anthracene

360

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

81

J

UG/KG

Chrysene

360

U

UG/KG

2,4,6-T richlorophenol

360

U

UG/KG

bis(2-Ethylhexyl) Phthalate

910

U

UG/KG

2,4,5-Trichlorophenol

360

U

UG/KG

Di-n-Octylphthalate

360

U

UG/KG

1,1 -Biphenyl

360

U

UG/KG

Benzo(b)Fluoranthene

360

U

UG/KG

2-Chloronaphthalene

80

J

UG/KG

Benzo(k)Fluoranthene

910

U

UG/KG

2-Nitroaniline

360

U

UG/KG

Benzo-a-Pyrene

360

u

UG/KG

Dimethyl Phthalate

360

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

360

u

UG/KG

2,6-Dinitrotoluene

360

UJ

UG/KG

Dibenzo(a,h)Anthracene

360

u

UG/KG

Acenaphthylene

360

UJ

UG/KG

Benzo(ghi)Perylene

910

u

UG/KG

3-Nitroaniline

9



%

% Moisture

360

u

UG/KG

Acenaphthene









910

UJ

UG/KG

2,4-Dinitrophenol









910

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9541 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF02 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH3
D No: 3AH3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

RESULTS UNITS

12000 J UG/KG
N UG/KG

ANALYTE

24 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9542 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH4
D No: 3AH4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

400

UJ

UG/KG

Benzaldehyde

400

U

UG/KG

Dibenzofuran

400

U

UG/KG

Phenol

400

U

UG/KG

2,4-Dinitrotoluene

400

U

UG/KG

bis(2-Chloroethyl) Ether

400

U

UG/KG

Diethyl Phthalate

400

U

UG/KG

2-Chlorophenol

400

U

UG/KG

Fluorene

400

U

UG/KG

2-Methylphenol

400

U

UG/KG

4-Chlorophenyl Phenyl Ether

400

U

UG/KG

bis(2-Chloroisopropyl) Ether

1000

U

UG/KG

4-Nitroaniline

400

U

UG/KG

Acetophenone

1000

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

400

u

UG/KG

(3-and/or 4-)Methylphenol

400

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

400

u

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

400

u

UG/KG

Hexachloroethane

400

U

UG/KG

4-Bromophenyl Phenyl Ether

400

u

UG/KG

Nitrobenzene

400

U

UG/KG

Hexachlorobenzene (HCB)

400

u

UG/KG

Isophorone

400

UJ

UG/KG

Atrazine

400

u

UG/KG

2-Nitrophenol

1000

UJ

UG/KG

Pentachlorophenol

400

u

UG/KG

2,4-Dimethylphenol

400

U

UG/KG

Phenanthrene

400

u

UG/KG

bis(2-Chloroethoxy)Methane

400

U

UG/KG

Anthracene

400

u

UG/KG

2,4-Dichlorophenol

400

U

UG/KG

Carbazole

400

u

UG/KG

Naphthalene

400

U

UG/KG

Di-n-Butylphthalate

400

u

UG/KG

4-Chloroaniline

100

J

UG/KG

Fluoranthene

400

u

UG/KG

Hexachlorobutadiene

96

J

UG/KG

Pyrene

400

UR

UG/KG

Caprolactam

400

U

UG/KG

Benzyl Butyl Phthalate

400

u

UG/KG

4-Chloro-3-Methylphenol

400

UJ

UG/KG

3,3'-Dichlorobenzidine

400

u

UG/KG

2-Methylnaphthalene

400

U

UG/KG

Benzo(a)Anthracene

400

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

400

U

UG/KG

Chrysene

400

u

UG/KG

2,4,6-T richlorophenol

400

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1000

u

UG/KG

2,4,5-Trichlorophenol

400

U

UG/KG

Di-n-Octylphthalate

400

u

UG/KG

1,1 -Biphenyl

87

J

UG/KG

Benzo(b)Fluoranthene

400

u

UG/KG

2-Chloronaphthalene

400

U

UG/KG

Benzo(k)Fluoranthene

1000

u

UG/KG

2-Nitroaniline

400

U

UG/KG

Benzo-a-Pyrene

400

u

UG/KG

Dimethyl Phthalate

400

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

400

u

UG/KG

2,6-Dinitrotoluene

400

UJ

UG/KG

Dibenzo(a,h)Anthracene

400

u

UG/KG

Acenaphthylene

400

UJ

UG/KG

Benzo(ghi)Perylene

1000

u

UG/KG

3-Nitroaniline

18



%

% Moisture

400

u

UG/KG

Acenaphthene









1000

UJ

UG/KG

2,4-Dinitrophenol









1000

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9542 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH4
D No: 3AH4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:50
Ending:

RESULTS UNITS

15000 J UG/KG
N UG/KG

ANALYTE

28 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9543 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD04 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH5
D No: 3AH5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

600

UJ

UG/KG

Benzaldehyde

600

U

UG/KG

Dibenzofuran

600

U

UG/KG

Phenol

600

U

UG/KG

2,4-Dinitrotoluene

600

U

UG/KG

bis(2-Chloroethyl) Ether

600

U

UG/KG

Diethyl Phthalate

600

U

UG/KG

2-Chlorophenol

600

U

UG/KG

Fluorene

600

U

UG/KG

2-Methylphenol

600

U

UG/KG

4-Chlorophenyl Phenyl Ether

600

U

UG/KG

bis(2-Chloroisopropyl) Ether

1500

U

UG/KG

4-Nitroaniline

300

J

UG/KG

Acetophenone

1500

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

600

U

UG/KG

(3-and/or 4-)Methylphenol

600

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

600

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

600

U

UG/KG

Hexachloroethane

600

U

UG/KG

4-Bromophenyl Phenyl Ether

600

U

UG/KG

Nitrobenzene

600

U

UG/KG

Hexachlorobenzene (HCB)

600

U

UG/KG

Isophorone

600

UJ

UG/KG

Atrazine

600

U

UG/KG

2-Nitrophenol

1500

UJ

UG/KG

Pentachlorophenol

600

U

UG/KG

2,4-Dimethylphenol

600

U

UG/KG

Phenanthrene

600

U

UG/KG

bis(2-Chloroethoxy)Methane

600

U

UG/KG

Anthracene

600

U

UG/KG

2,4-Dichlorophenol

600

U

UG/KG

Carbazole

600

U

UG/KG

Naphthalene

600

U

UG/KG

Di-n-Butylphthalate

600

U

UG/KG

4-Chloroaniline

600

U

UG/KG

Fluoranthene

600

u

UG/KG

Hexachlorobutadiene

600

U

UG/KG

Pyrene

600

UR

UG/KG

Caprolactam

600

U

UG/KG

Benzyl Butyl Phthalate

600

U

UG/KG

4-Chloro-3-Methylphenol

600

UJ

UG/KG

3,3'-Dichlorobenzidine

600

U

UG/KG

2-Methylnaphthalene

600

U

UG/KG

Benzo(a)Anthracene

600

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

600

U

UG/KG

Chrysene

600

U

UG/KG

2,4,6-T richlorophenol

600

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1500

U

UG/KG

2,4,5-Trichlorophenol

600

U

UG/KG

Di-n-Octylphthalate

600

u

UG/KG

1,1 -Biphenyl

600

u

UG/KG

Benzo(b)Fluoranthene

600

u

UG/KG

2-Chloronaphthalene

600

u

UG/KG

Benzo(k)Fluoranthene

1500

u

UG/KG

2-Nitroaniline

600

u

UG/KG

Benzo-a-Pyrene

600

u

UG/KG

Dimethyl Phthalate

600

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

600

u

UG/KG

2,6-Dinitrotoluene

600

UJ

UG/KG

Dibenzo(a,h)Anthracene

600

u

UG/KG

Acenaphthylene

600

UJ

UG/KG

Benzo(ghi)Perylene

1500

u

UG/KG

3-Nitroaniline

45



%

% Moisture

600

u

UG/KG

Acenaphthene









1500

UJ

UG/KG

2,4-Dinitrophenol









1500

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9543 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD04 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH5
D No: 3AH5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:15
Ending:

RESULTS UNITS

13000 J
N

UG/KG
UG/KG

ANALYTE

28 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9544 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD04D /

Media: SEDIMENT

Case No: 34717
MD No: 3AH6
D No: 3AH6

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

490

UJ

UG/KG

Benzaldehyde

490

U

UG/KG

Dibenzofuran

490

U

UG/KG

Phenol

490

U

UG/KG

2,4-Dinitrotoluene

490

U

UG/KG

bis(2-Chloroethyl) Ether

490

U

UG/KG

Diethyl Phthalate

490

U

UG/KG

2-Chlorophenol

490

U

UG/KG

Fluorene

490

U

UG/KG

2-Methylphenol

490

U

UG/KG

4-Chlorophenyl Phenyl Ether

490

U

UG/KG

bis(2-Chloroisopropyl) Ether

1200

U

UG/KG

4-Nitroaniline

490

U

UG/KG

Acetophenone

1200

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

490

U

UG/KG

(3-and/or 4-)Methylphenol

490

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

490

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

490

U

UG/KG

Hexachloroethane

490

U

UG/KG

4-Bromophenyl Phenyl Ether

490

U

UG/KG

Nitrobenzene

490

U

UG/KG

Hexachlorobenzene (HCB)

490

U

UG/KG

Isophorone

490

UJ

UG/KG

Atrazine

490

U

UG/KG

2-Nitrophenol

1200

UJ

UG/KG

Pentachlorophenol

490

U

UG/KG

2,4-Dimethylphenol

180

J

UG/KG

Phenanthrene

490

U

UG/KG

bis(2-Chloroethoxy)Methane

490

U

UG/KG

Anthracene

490

U

UG/KG

2,4-Dichlorophenol

490

U

UG/KG

Carbazole

490

U

UG/KG

Naphthalene

490

U

UG/KG

Di-n-Butylphthalate

490

U

UG/KG

4-Chloroaniline

530



UG/KG

Fluoranthene

490

U

UG/KG

Hexachlorobutadiene

460

J

UG/KG

Pyrene

490

UR

UG/KG

Caprolactam

490

U

UG/KG

Benzyl Butyl Phthalate

490

U

UG/KG

4-Chloro-3-Methylphenol

490

UJ

UG/KG

3,3'-Dichlorobenzidine

490

U

UG/KG

2-Methylnaphthalene

180

J

UG/KG

Benzo(a)Anthracene

490

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

270

J

UG/KG

Chrysene

490

U

UG/KG

2,4,6-T richlorophenol

490

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1200

U

UG/KG

2,4,5-Trichlorophenol

490

U

UG/KG

Di-n-Octylphthalate

490

U

UG/KG

1,1 -Biphenyl

280

J

UG/KG

Benzo(b)Fluoranthene

490

U

UG/KG

2-Chloronaphthalene

200

J

UG/KG

Benzo(k)Fluoranthene

1200

u

UG/KG

2-Nitroaniline

230

J

UG/KG

Benzo-a-Pyrene

490

u

UG/KG

Dimethyl Phthalate

210

J

UG/KG

Indeno (1,2,3-cd) Pyrene

490

u

UG/KG

2,6-Dinitrotoluene

490

UJ

UG/KG

Dibenzo(a,h)Anthracene

490

u

UG/KG

Acenaphthylene

250

J

UG/KG

Benzo(ghi)Perylene

1200

u

UG/KG

3-Nitroaniline

32



%

% Moisture

490

u

UG/KG

Acenaphthene









1200

UJ

UG/KG

2,4-Dinitrophenol









1200

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9544 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSD04D /	MD No: 3AH6	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AH6	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

27 UNKNOWNS
PETROLEUM PRODUCT
BENZO [E] PYRENE

6900

J

UG/KG



N

UG/KG

250

NJ

UG/KG

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:25
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9545 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD05 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH7
D No: 3AH7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

660

UJ

UG/KG

Benzaldehyde

660

U

UG/KG

Dibenzofuran

660

U

UG/KG

Phenol

660

U

UG/KG

2,4-Dinitrotoluene

660

U

UG/KG

bis(2-Chloroethyl) Ether

660

U

UG/KG

Diethyl Phthalate

660

U

UG/KG

2-Chlorophenol

660

U

UG/KG

Fluorene

660

U

UG/KG

2-Methylphenol

660

U

UG/KG

4-Chlorophenyl Phenyl Ether

660

U

UG/KG

bis(2-Chloroisopropyl) Ether

1700

U

UG/KG

4-Nitroaniline

660

U

UG/KG

Acetophenone

1700

UJ

UG/KG

2-Methyl-4,6-Dinitrophenol

660

U

UG/KG

(3-and/or 4-)Methylphenol

660

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

660

U

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

660

U

UG/KG

Hexachloroethane

660

U

UG/KG

4-Bromophenyl Phenyl Ether

660

U

UG/KG

Nitrobenzene

660

U

UG/KG

Hexachlorobenzene (HCB)

660

U

UG/KG

Isophorone

660

UJ

UG/KG

Atrazine

660

U

UG/KG

2-Nitrophenol

1700

UJ

UG/KG

Pentachlorophenol

660

U

UG/KG

2,4-Dimethylphenol

660

U

UG/KG

Phenanthrene

660

U

UG/KG

bis(2-Chloroethoxy)Methane

660

U

UG/KG

Anthracene

660

U

UG/KG

2,4-Dichlorophenol

660

U

UG/KG

Carbazole

660

U

UG/KG

Naphthalene

660

U

UG/KG

Di-n-Butylphthalate

660

U

UG/KG

4-Chloroaniline

660

U

UG/KG

Fluoranthene

660

U

UG/KG

Hexachlorobutadiene

660

U

UG/KG

Pyrene

660

UR

UG/KG

Caprolactam

660

U

UG/KG

Benzyl Butyl Phthalate

660

U

UG/KG

4-Chloro-3-Methylphenol

660

U

UG/KG

3,3'-Dichlorobenzidine

660

U

UG/KG

2-Methylnaphthalene

660

U

UG/KG

Benzo(a)Anthracene

660

UJ

UG/KG

Hexachlorocyclopentadiene (HCCP)

660

U

UG/KG

Chrysene

660

U

UG/KG

2,4,6-T richlorophenol

200

J

UG/KG

bis(2-Ethylhexyl) Phthalate

1700

U

UG/KG

2,4,5-Trichlorophenol

660

U

UG/KG

Di-n-Octylphthalate

660

U

UG/KG

1,1 -Biphenyl

660

U

UG/KG

Benzo(b)Fluoranthene

660

U

UG/KG

2-Chloronaphthalene

660

U

UG/KG

Benzo(k)Fluoranthene

1700

u

UG/KG

2-Nitroaniline

660

U

UG/KG

Benzo-a-Pyrene

660

u

UG/KG

Dimethyl Phthalate

660

UJ

UG/KG

Indeno (1,2,3-cd) Pyrene

660

u

UG/KG

2,6-Dinitrotoluene

660

UJ

UG/KG

Dibenzo(a,h)Anthracene

660

u

UG/KG

Acenaphthylene

660

UJ

UG/KG

Benzo(ghi)Perylene

1700

u

UG/KG

3-Nitroaniline

50



%

% Moisture

660

u

UG/KG

Acenaphthene









1700

UJ

UG/KG

2,4-Dinitrophenol









1700

UJ

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9545 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD05 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH7
D No: 3AH7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:45
Ending:

RESULTS UNITS

14000 J
N

UG/KG
UG/KG

ANALYTE

26 UNKNOWNS
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9546 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH8
D No: 3AH8

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

660

U

UG/KG

Benzaldehyde

660

U

UG/KG

Dibenzofuran

660

U

UG/KG

Phenol

660

U

UG/KG

2,4-Dinitrotoluene

660

U

UG/KG

bis(2-Chloroethyl) Ether

660

U

UG/KG

Diethyl Phthalate

660

U

UG/KG

2-Chlorophenol

660

U

UG/KG

Fluorene

660

U

UG/KG

2-Methylphenol

660

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

660

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

1700

U

UG/KG

4-Nitroaniline

660

U

UG/KG

Acetophenone

1700

U

UG/KG

2-Methyl-4,6-Dinitrophenol

660

U

UG/KG

(3-and/or 4-)Methylphenol

660

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

660

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

660

UJ

UG/KG

Hexachloroethane

660

U

UG/KG

4-Bromophenyl Phenyl Ether

660

U

UG/KG

Nitrobenzene

660

UJ

UG/KG

Hexachlorobenzene (HCB)

660

U

UG/KG

Isophorone

660

U

UG/KG

Atrazine

660

U

UG/KG

2-Nitrophenol

1700

U

UG/KG

Pentachlorophenol

660

U

UG/KG

2,4-Dimethylphenol

660

U

UG/KG

Phenanthrene

660

U

UG/KG

bis(2-Chloroethoxy)Methane

660

U

UG/KG

Anthracene

660

U

UG/KG

2,4-Dichlorophenol

660

U

UG/KG

Carbazole

660

U

UG/KG

Naphthalene

660

U

UG/KG

Di-n-Butylphthalate

660

U

UG/KG

4-Chloroaniline

660

U

UG/KG

Fluoranthene

660

U

UG/KG

Hexachlorobutadiene

660

U

UG/KG

Pyrene

660

U

UG/KG

Caprolactam

660

U

UG/KG

Benzyl Butyl Phthalate

660

u

UG/KG

4-Chloro-3-Methylphenol

660

U

UG/KG

3,3'-Dichlorobenzidine

660

u

UG/KG

2-Methylnaphthalene

660

U

UG/KG

Benzo(a)Anthracene

660

u

UG/KG

Hexachlorocyclopentadiene (HCCP)

660

U

UG/KG

Chrysene

660

u

UG/KG

2,4,6-T richlorophenol

660

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1700

u

UG/KG

2,4,5-Trichlorophenol

660

U

UG/KG

Di-n-Octylphthalate

660

u

UG/KG

1,1 -Biphenyl

660

U

UG/KG

Benzo(b)Fluoranthene

660

u

UG/KG

2-Chloronaphthalene

660

U

UG/KG

Benzo(k)Fluoranthene

1700

UJ

UG/KG

2-Nitroaniline

660

U

UG/KG

Benzo-a-Pyrene

660

u

UG/KG

Dimethyl Phthalate

660

u

UG/KG

Indeno (1,2,3-cd) Pyrene

660

u

UG/KG

2,6-Dinitrotoluene

660

u

UG/KG

Dibenzo(a,h)Anthracene

660

u

UG/KG

Acenaphthylene

660

u

UG/KG

Benzo(ghi)Perylene

1700

u

UG/KG

3-Nitroaniline

50



%

% Moisture

660

u

UG/KG

Acenaphthene









1700

u

UG/KG

2,4-Dinitrophenol









1700

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9546 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD01 /	MD No: 3AH8	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AH8	Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

SUBSTITUTED NAPHTHALENE
1,1'-BIPHENYL, BIS( 1 -METHYLETHYL)-
27 UNKNOWNS

200

J

UG/KG

390

NJ

UG/KG

8900

J

UG/KG

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9547 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD01D/

Media: SEDIMENT

Case No: 34717
MD No: 3AH9
D No: 3AH9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

660

U

UG/KG

Benzaldehyde

660

U

UG/KG

Dibenzofuran

660

U

UG/KG

Phenol

660

U

UG/KG

2,4-Dinitrotoluene

660

U

UG/KG

bis(2-Chloroethyl) Ether

660

U

UG/KG

Diethyl Phthalate

660

U

UG/KG

2-Chlorophenol

660

U

UG/KG

Fluorene

660

U

UG/KG

2-Methylphenol

660

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

660

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

1700

U

UG/KG

4-Nitroaniline

660

U

UG/KG

Acetophenone

1700

U

UG/KG

2-Methyl-4,6-Dinitrophenol

660

U

UG/KG

(3-and/or 4-)Methylphenol

660

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

660

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

660

UJ

UG/KG

Hexachloroethane

660

U

UG/KG

4-Bromophenyl Phenyl Ether

660

U

UG/KG

Nitrobenzene

660

UJ

UG/KG

Hexachlorobenzene (HCB)

660

U

UG/KG

Isophorone

660

U

UG/KG

Atrazine

660

U

UG/KG

2-Nitrophenol

1700

U

UG/KG

Pentachlorophenol

660

U

UG/KG

2,4-Dimethylphenol

660

U

UG/KG

Phenanthrene

660

U

UG/KG

bis(2-Chloroethoxy)Methane

660

U

UG/KG

Anthracene

660

U

UG/KG

2,4-Dichlorophenol

660

U

UG/KG

Carbazole

660

U

UG/KG

Naphthalene

660

U

UG/KG

Di-n-Butylphthalate

660

U

UG/KG

4-Chloroaniline

660

U

UG/KG

Fluoranthene

660

U

UG/KG

Hexachlorobutadiene

660

U

UG/KG

Pyrene

660

U

UG/KG

Caprolactam

660

U

UG/KG

Benzyl Butyl Phthalate

660

u

UG/KG

4-Chloro-3-Methylphenol

660

U

UG/KG

3,3'-Dichlorobenzidine

660

u

UG/KG

2-Methylnaphthalene

660

U

UG/KG

Benzo(a)Anthracene

660

u

UG/KG

Hexachlorocyclopentadiene (HCCP)

660

U

UG/KG

Chrysene

660

u

UG/KG

2,4,6-T richlorophenol

660

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1700

u

UG/KG

2,4,5-Trichlorophenol

660

U

UG/KG

Di-n-Octylphthalate

660

u

UG/KG

1,1 -Biphenyl

660

U

UG/KG

Benzo(b)Fluoranthene

660

u

UG/KG

2-Chloronaphthalene

660

U

UG/KG

Benzo(k)Fluoranthene

1700

UJ

UG/KG

2-Nitroaniline

660

U

UG/KG

Benzo-a-Pyrene

660

u

UG/KG

Dimethyl Phthalate

660

u

UG/KG

Indeno (1,2,3-cd) Pyrene

660

u

UG/KG

2,6-Dinitrotoluene

660

u

UG/KG

Dibenzo(a,h)Anthracene

660

u

UG/KG

Acenaphthylene

660

u

UG/KG

Benzo(ghi)Perylene

1700

u

UG/KG

3-Nitroaniline

50



%

% Moisture

660

u

UG/KG

Acenaphthene









1700

u

UG/KG

2,4-Dinitrophenol









1700

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9547 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD01D /	MD No: 3AH9	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AH9	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

280

NJ

UG/KG

BICYCLO[3.1.1] HEPT-2-ENE, 2,6,6-TRIMETHYL-

240

NJ

UG/KG

BENZENE, 1 -METHYL-4-(1 -METHYLETHYL)-

490

NJ

UG/KG

1,1'-BIPHENYL, BIS( 1 -METHYLETHYL)-

200

J

UG/KG

UNKNOWN ALDEHYDE

600

NJ

UG/KG

ANDROSTAN-6-ONE, (5.ALPHA. )-

8400

J

UG/KG

24 UNKNOWNS

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:05
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9548 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AJ0
D No: 3AJ0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 12:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

430

U

UG/KG

Benzaldehyde

430

U

UG/KG

Dibenzofuran

430

U

UG/KG

Phenol

430

U

UG/KG

2,4-Dinitrotoluene

430

U

UG/KG

bis(2-Chloroethyl) Ether

430

U

UG/KG

Diethyl Phthalate

430

U

UG/KG

2-Chlorophenol

430

U

UG/KG

Fluorene

430

U

UG/KG

2-Methylphenol

430

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

430

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

1100

U

UG/KG

4-Nitroaniline

430

U

UG/KG

Acetophenone

1100

U

UG/KG

2-Methyl-4,6-Dinitrophenol

430

U

UG/KG

(3-and/or 4-)Methylphenol

430

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

430

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

430

UJ

UG/KG

Hexachloroethane

430

U

UG/KG

4-Bromophenyl Phenyl Ether

430

U

UG/KG

Nitrobenzene

430

UJ

UG/KG

Hexachlorobenzene (HCB)

430

U

UG/KG

Isophorone

430

U

UG/KG

Atrazine

430

U

UG/KG

2-Nitrophenol

1100

U

UG/KG

Pentachlorophenol

430

U

UG/KG

2,4-Dimethylphenol

1200



UG/KG

Phenanthrene

430

U

UG/KG

bis(2-Chloroethoxy)Methane

110

J

UG/KG

Anthracene

430

U

UG/KG

2,4-Dichlorophenol

430

U

UG/KG

Carbazole

1100



UG/KG

Naphthalene

430

U

UG/KG

Di-n-Butylphthalate

430

U

UG/KG

4-Chloroaniline

430

U

UG/KG

Fluoranthene

430

u

UG/KG

Hexachlorobutadiene

130

J

UG/KG

Pyrene

430

u

UG/KG

Caprolactam

430

U

UG/KG

Benzyl Butyl Phthalate

430

u

UG/KG

4-Chloro-3-Methylphenol

430

U

UG/KG

3,3'-Dichlorobenzidine

4100



UG/KG

2-Methylnaphthalene

430

U

UG/KG

Benzo(a)Anthracene

430

u

UG/KG

Hexachlorocyclopentadiene (HCCP)

430

U

UG/KG

Chrysene

430

u

UG/KG

2,4,6-T richlorophenol

430

U

UG/KG

bis(2-Ethylhexyl) Phthalate

1100

u

UG/KG

2,4,5-Trichlorophenol

430

U

UG/KG

Di-n-Octylphthalate

1100



UG/KG

1,1 -Biphenyl

430

U

UG/KG

Benzo(b)Fluoranthene

430

u

UG/KG

2-Chloronaphthalene

430

U

UG/KG

Benzo(k)Fluoranthene

1100

UJ

UG/KG

2-Nitroaniline

430

U

UG/KG

Benzo-a-Pyrene

430

u

UG/KG

Dimethyl Phthalate

430

U

UG/KG

Indeno (1,2,3-cd) Pyrene

430

u

UG/KG

2,6-Dinitrotoluene

430

U

UG/KG

Dibenzo(a,h)Anthracene

430

u

UG/KG

Acenaphthylene

430

U

UG/KG

Benzo(ghi)Perylene

1100

u

UG/KG

3-Nitroaniline

24



%

% Moisture

430

u

UG/KG

Acenaphthene









1100

u

UG/KG

2,4-Dinitrophenol









1100

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9548 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD02 /	MD No: 3AJ0	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ0	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

18000

J

UG/KG

27 UNKNOWNS

520

NJ

UG/KG

NAPHTHALENE,

200

NJ

UG/KG

NAPHTHALENE.

190

NJ

UG/KG

NAPHTHALENE.

530

NJ

UG/KG

NAPHTHALENE.

170

NJ

UG/KG

NAPHTHALENE,

210

NJ

UG/KG

NAPHTHALENE.

2400

NJ

UG/KG

DIBENZOTHIOP

1-METHYL-

1,2,3,4-TETRAHYDRO-5,6-DIMETHYL-

1.5-DIMETHYL-

2.6-DIMETHYL-

2-(1-METHYLETHYL)-
1,4,6-TRIMETHYL-
HENE, 4-METHYL-

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 12:00
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9549 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSF05 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ1
D No: 3AJ1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

370

U

UG/KG

Benzaldehyde

370

U

UG/KG

Dibenzofuran

370

U

UG/KG

Phenol

370

U

UG/KG

2,4-Dinitrotoluene

370

U

UG/KG

bis(2-Chloroethyl) Ether

370

U

UG/KG

Diethyl Phthalate

370

U

UG/KG

2-Chlorophenol

370

U

UG/KG

Fluorene

370

U

UG/KG

2-Methylphenol

370

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

370

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

920

U

UG/KG

4-Nitroaniline

370

U

UG/KG

Acetophenone

920

U

UG/KG

2-Methyl-4,6-Dinitrophenol

370

U

UG/KG

(3-and/or 4-)Methylphenol

370

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

370

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

370

UJ

UG/KG

Hexachloroethane

370

U

UG/KG

4-Bromophenyl Phenyl Ether

370

U

UG/KG

Nitrobenzene

370

UJ

UG/KG

Hexachlorobenzene (HCB)

370

U

UG/KG

Isophorone

370

U

UG/KG

Atrazine

370

U

UG/KG

2-Nitrophenol

920

U

UG/KG

Pentachlorophenol

370

U

UG/KG

2,4-Dimethylphenol

370

U

UG/KG

Phenanthrene

370

U

UG/KG

bis(2-Chloroethoxy)Methane

370

U

UG/KG

Anthracene

370

U

UG/KG

2,4-Dichlorophenol

370

U

UG/KG

Carbazole

370

U

UG/KG

Naphthalene

370

U

UG/KG

Di-n-Butylphthalate

370

U

UG/KG

4-Chloroaniline

370

U

UG/KG

Fluoranthene

370

U

UG/KG

Hexachlorobutadiene

370

U

UG/KG

Pyrene

370

U

UG/KG

Caprolactam

370

U

UG/KG

Benzyl Butyl Phthalate

370

U

UG/KG

4-Chloro-3-Methylphenol

370

U

UG/KG

3,3'-Dichlorobenzidine

370

U

UG/KG

2-Methylnaphthalene

370

U

UG/KG

Benzo(a)Anthracene

370

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

370

U

UG/KG

Chrysene

370

U

UG/KG

2,4,6-T richlorophenol

370

U

UG/KG

bis(2-Ethylhexyl) Phthalate

920

u

UG/KG

2,4,5-Trichlorophenol

370

U

UG/KG

Di-n-Octylphthalate

370

u

UG/KG

1,1 -Biphenyl

370

U

UG/KG

Benzo(b)Fluoranthene

370

u

UG/KG

2-Chloronaphthalene

370

U

UG/KG

Benzo(k)Fluoranthene

920

UJ

UG/KG

2-Nitroaniline

370

u

UG/KG

Benzo-a-Pyrene

370

u

UG/KG

Dimethyl Phthalate

370

u

UG/KG

Indeno (1,2,3-cd) Pyrene

370

u

UG/KG

2,6-Dinitrotoluene

370

u

UG/KG

Dibenzo(a,h)Anthracene

370

u

UG/KG

Acenaphthylene

370

u

UG/KG

Benzo(ghi)Perylene

920

u

UG/KG

3-Nitroaniline

10



%

% Moisture

370

u

UG/KG

Acenaphthene









920

u

UG/KG

2,4-Dinitrophenol









920

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/31/2005 12:29

Sample 9549 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF05 /	MD No: 3AJ1	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ1	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

330 NJ

UG/KG

CYCLOHEXENE, 1 -METHYL-4-(1 -METHYLETHENYLJ-

240 NJ

UG/KG

N-HEXADECANOIC ACID

24000 J

UG/KG

23 UNKNOWNS

700 NJ

UG/KG

.GAMMA.-SITOSTEROL

1200 NJ

UG/KG

STIGMAST-4-EN-3-ONE

1700 NJ

UG/KG

2 PHENANTHRENECARBOXYLIC ACIDS

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:20
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9550 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSF04 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ2
D No: 3AJ2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

U

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

380

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

940

U

UG/KG

4-Nitroaniline

380

U

UG/KG

Acetophenone

940

U

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

UJ

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

UJ

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

U

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

940

U

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

U

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

U

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

940

u

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

u

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

u

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

940

UJ

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

u

UG/KG

Dimethyl Phthalate

380

u

UG/KG

Indeno (1,2,3-cd) Pyrene

380

u

UG/KG

2,6-Dinitrotoluene

380

u

UG/KG

Dibenzo(a,h)Anthracene

380

u

UG/KG

Acenaphthylene

380

u

UG/KG

Benzo(ghi)Perylene

940

u

UG/KG

3-Nitroaniline

12



%

% Moisture

380

u

UG/KG

Acenaphthene









940

u

UG/KG

2,4-Dinitrophenol









940

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9550 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF04 /	MD No: 3AJ2	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ2	Org Contractor: LIBRTY

RESULTS

UNITS

10000

J

UG/KG

150

NJ

UG/KG

360

NJ

UG/KG

530

NJ

UG/KG

350

NJ

UG/KG

ANALYTE

25 UNKNOWNS

PHENANTHRENE, 1 -METHYL-7-( 1 -METHYLETHYL)-
SUBSTITUTED PHENANTHRENECARBOXYLIC ACID
.GAMMA.-SITOSTEROL
LONGIFOLENALDEHYDE

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:45
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9551 FY 2005 Project: 05-0928

Extractables Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ3
D No: 3AJ3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 14:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

380

U

UG/KG

Benzaldehyde

380

U

UG/KG

Dibenzofuran

380

U

UG/KG

Phenol

380

U

UG/KG

2,4-Dinitrotoluene

380

U

UG/KG

bis(2-Chloroethyl) Ether

380

U

UG/KG

Diethyl Phthalate

380

U

UG/KG

2-Chlorophenol

380

U

UG/KG

Fluorene

380

U

UG/KG

2-Methylphenol

380

UJ

UG/KG

4-Chlorophenyl Phenyl Ether

380

UJ

UG/KG

bis(2-Chloroisopropyl) Ether

970

U

UG/KG

4-Nitroaniline

380

U

UG/KG

Acetophenone

970

U

UG/KG

2-Methyl-4,6-Dinitrophenol

380

U

UG/KG

(3-and/or 4-)Methylphenol

380

U

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

380

UJ

UG/KG

n-Nitroso di-n-Propylamine



NA

UG/KG

1,2,4,5-Tetrachlorobenzene

380

UJ

UG/KG

Hexachloroethane

380

U

UG/KG

4-Bromophenyl Phenyl Ether

380

U

UG/KG

Nitrobenzene

380

UJ

UG/KG

Hexachlorobenzene (HCB)

380

U

UG/KG

Isophorone

380

U

UG/KG

Atrazine

380

U

UG/KG

2-Nitrophenol

970

U

UG/KG

Pentachlorophenol

380

U

UG/KG

2,4-Dimethylphenol

380

U

UG/KG

Phenanthrene

380

U

UG/KG

bis(2-Chloroethoxy)Methane

380

U

UG/KG

Anthracene

380

U

UG/KG

2,4-Dichlorophenol

380

U

UG/KG

Carbazole

380

U

UG/KG

Naphthalene

380

U

UG/KG

Di-n-Butylphthalate

380

U

UG/KG

4-Chloroaniline

380

U

UG/KG

Fluoranthene

380

U

UG/KG

Hexachlorobutadiene

380

U

UG/KG

Pyrene

380

U

UG/KG

Caprolactam

380

U

UG/KG

Benzyl Butyl Phthalate

380

U

UG/KG

4-Chloro-3-Methylphenol

380

U

UG/KG

3,3'-Dichlorobenzidine

380

U

UG/KG

2-Methylnaphthalene

380

U

UG/KG

Benzo(a)Anthracene

380

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

380

U

UG/KG

Chrysene

380

U

UG/KG

2,4,6-T richlorophenol

380

U

UG/KG

bis(2-Ethylhexyl) Phthalate

970

u

UG/KG

2,4,5-Trichlorophenol

380

U

UG/KG

Di-n-Octylphthalate

380

u

UG/KG

1,1 -Biphenyl

380

U

UG/KG

Benzo(b)Fluoranthene

380

u

UG/KG

2-Chloronaphthalene

380

U

UG/KG

Benzo(k)Fluoranthene

970

UJ

UG/KG

2-Nitroaniline

380

U

UG/KG

Benzo-a-Pyrene

380

u

UG/KG

Dimethyl Phthalate

380

u

UG/KG

Indeno (1,2,3-cd) Pyrene

380

u

UG/KG

2,6-Dinitrotoluene

380

u

UG/KG

Dibenzo(a,h)Anthracene

380

u

UG/KG

Acenaphthylene

380

u

UG/KG

Benzo(ghi)Perylene

970

u

UG/KG

3-Nitroaniline

14



%

% Moisture

380

u

UG/KG

Acenaphthene









970

u

UG/KG

2,4-Dinitrophenol









970

u

UG/KG

4-Nitrophenol









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9551 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ3
D No: 3AJ3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 14:05
Ending:

RESULTS UNITS

4000 J
930 NJ

UG/KG
UG/KG

ANALYTE

20 UNKNOWNS

SUBSTITUTED PHENANTHRENE CARBOXYLIC ACID

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9518 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 10:35

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSF08/

MD No: 3AJ4 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ4 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4300



MG/KG

Aluminum

6.4

UJ

MG/KG

Antimony

1.7



MG/KG

Arsenic

17

J

MG/KG

Barium

0.29

UJ

MG/KG

Beryllium

0.05

UJ

MG/KG

Cadmium

15000



MG/KG

Calcium

16

J

MG/KG

Chromium

2.2

J

MG/KG

Cobalt

23



MG/KG

Copper

4300

J

MG/KG

Iron

6.6

J

MG/KG

Lead

890



MG/KG

Magnesium

45

J

MG/KG

Manganese

0.11

U

MG/KG

Total Mercury

64



MG/KG

Nickel

220

J

MG/KG

Potassium

1.5

J

MG/KG

Selenium

1.1

U

MG/KG

Silver

300

J

MG/KG

Sodium

2.7

U

MG/KG

Thallium

240



MG/KG

Vanadium

95



MG/KG

Zinc



NA

MG/KG

Cyanide

7



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

11000



MG/KG

Aluminum

12

UJ

MG/KG

Antimony

2.9



MG/KG

Arsenic

37

J

MG/KG

Barium

0.51

UJ

MG/KG

Beryllium

0.29

UJ

MG/KG

Cadmium

7700



MG/KG

Calcium

28

J

MG/KG

Chromium

2.5

J

MG/KG

Cobalt

20



MG/KG

Copper

8600

J

MG/KG

Iron

63

J

MG/KG

Lead

3200



MG/KG

Magnesium

93

J

MG/KG

Manganese

0.07

UJ

MG/KG

Total Mercury

8.7



MG/KG

Nickel

1300



MG/KG

Potassium

3.1

J

MG/KG

Selenium

1.9

U

MG/KG

Silver

7700



MG/KG

Sodium

4.9

U

MG/KG

Thallium

60



MG/KG

Vanadium

120



MG/KG

Zinc



NA

MG/KG

Cyanide

49



%

% Moisture

Sample 9519 FY 2005 Project: 05-0928
Metals Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD07 /	MD No: 3AJ5

Media: SEDIMENT	D No: 3AJ5

Produced by: Goddard, Denise
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9520 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 11:30

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSF02/

MD No: 3AJ6 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ6 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4000



MG/KG

Aluminum

7.7

UJ

MG/KG

Antimony

0.64

J

MG/KG

Arsenic

8.0

J

MG/KG

Barium

0.08

UJ

MG/KG

Beryllium

0.07

UJ

MG/KG

Cadmium

660



MG/KG

Calcium

4.0

J

MG/KG

Chromium

0.34

J

MG/KG

Cobalt

2.6

J

MG/KG

Copper

1300

J

MG/KG

Iron

15

J

MG/KG

Lead

190

J

MG/KG

Magnesium

4.6

J

MG/KG

Manganese

0.03

UJ

MG/KG

Total Mercury

1.2

J

MG/KG

Nickel

110

J

MG/KG

Potassium

0.48

R

MG/KG

Selenium

1.3

U

MG/KG

Silver

520

J

MG/KG

Sodium

3.2

U

MG/KG

Thallium

7.1



MG/KG

Vanadium

16



MG/KG

Zinc



NA

MG/KG

Cyanide

22



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9521 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 11:30

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSF02S/

MD No: 3AJ7 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ7 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4200



MG/KG

Aluminum

7.7

UJ

MG/KG

Antimony

0.68

R

MG/KG

Arsenic

8.6

J

MG/KG

Barium

0.08

UJ

MG/KG

Beryllium

0.04

UJ

MG/KG

Cadmium

690



MG/KG

Calcium

4.2

J

MG/KG

Chromium

0.38

J

MG/KG

Cobalt

2.7

J

MG/KG

Copper

1400

J

MG/KG

Iron

18

J

MG/KG

Lead

190

J

MG/KG

Magnesium

5.1

J

MG/KG

Manganese

0.03

UJ

MG/KG

Total Mercury

1.4

J

MG/KG

Nickel

110

J

MG/KG

Potassium

4.5

U

MG/KG

Selenium

1.3

U

MG/KG

Silver

530

J

MG/KG

Sodium

3.2

U

MG/KG

Thallium

7.5



MG/KG

Vanadium

16



MG/KG

Zinc



NA

MG/KG

Cyanide

22



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9522 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 10:55

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSF01 /

MD No: 3AJ8 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ8 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

7500



MG/KG

Aluminum

0.24

R

MG/KG

Antimony

1.7



MG/KG

Arsenic

13

J

MG/KG

Barium

0.13

UJ

MG/KG

Beryllium

0.17

UJ

MG/KG

Cadmium

9800



MG/KG

Calcium

9.2

J

MG/KG

Chromium

0.69

J

MG/KG

Cobalt

3.6



MG/KG

Copper

5100

J

MG/KG

Iron

8.4

J

MG/KG

Lead

300

J

MG/KG

Magnesium

16

J

MG/KG

Manganese

0.38



MG/KG

Total Mercury

3.6

J

MG/KG

Nickel

200

J

MG/KG

Potassium

3.9

U

MG/KG

Selenium

1.1

U

MG/KG

Silver

470

J

MG/KG

Sodium

2.8

U

MG/KG

Thallium

15



MG/KG

Vanadium

18



MG/KG

Zinc



NA

MG/KG

Cyanide

9



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9523 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 11:45

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSD06/

MD No: 3AJ9 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AJ9 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

16000



MG/KG

Aluminum

0.76

R

MG/KG

Antimony

10



MG/KG

Arsenic

59



MG/KG

Barium

1.3



MG/KG

Beryllium

0.34

UJ

MG/KG

Cadmium

43000



MG/KG

Calcium

60

J

MG/KG

Chromium

14



MG/KG

Cobalt

15



MG/KG

Copper

21000

J

MG/KG

Iron

26

J

MG/KG

Lead

11000



MG/KG

Magnesium

890

J

MG/KG

Manganese

0.20

U

MG/KG

Total Mercury

20



MG/KG

Nickel

2300



MG/KG

Potassium

6.8

U

MG/KG

Selenium

2.0

U

MG/KG

Silver

8600



MG/KG

Sodium

0.72

R

MG/KG

Thallium

41



MG/KG

Vanadium

130



MG/KG

Zinc



NA

MG/KG

Cyanide

49



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9524 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 12:35

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSD05/

MD No: 3AK0 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AK0 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

8900



MG/KG

Aluminum

26

UJ

MG/KG

Antimony

3.8

J

MG/KG

Arsenic

74

J

MG/KG

Barium

0.82

UJ

MG/KG

Beryllium

2.2

U

MG/KG

Cadmium

5100



MG/KG

Calcium

95

J

MG/KG

Chromium

4.1

J

MG/KG

Cobalt

33



MG/KG

Copper

8500

J

MG/KG

Iron

23

J

MG/KG

Lead

4300



MG/KG

Magnesium

54

J

MG/KG

Manganese

0.17

UJ

MG/KG

Total Mercury

64



MG/KG

Nickel

1400

J

MG/KG

Potassium

24



MG/KG

Selenium

4.3

U

MG/KG

Silver

22000



MG/KG

Sodium

11

U

MG/KG

Thallium

590



MG/KG

Vanadium

150



MG/KG

Zinc



NA

MG/KG

Cyanide

77



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9525 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 12:45

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSD05D/

MD No: 3AK1 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AK1 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

8900



MG/KG

Aluminum

30

UJ

MG/KG

Antimony

3.3

J

MG/KG

Arsenic

50

J

MG/KG

Barium

0.79

UJ

MG/KG

Beryllium

2.5

U

MG/KG

Cadmium

5000



MG/KG

Calcium

80

J

MG/KG

Chromium

2.7

J

MG/KG

Cobalt

30



MG/KG

Copper

6500

J

MG/KG

Iron

25

J

MG/KG

Lead

4400



MG/KG

Magnesium

51

J

MG/KG

Manganese

0.14

UJ

MG/KG

Total Mercury

47



MG/KG

Nickel

1500

J

MG/KG

Potassium

21



MG/KG

Selenium

4.9

U

MG/KG

Silver

25000



MG/KG

Sodium

12

U

MG/KG

Thallium

500



MG/KG

Vanadium

130



MG/KG

Zinc



NA

MG/KG

Cyanide

80



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9526 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/06/2005 12:40

Program: SF

Case No: 34717

Ending:

Id/Station: CFMSD03/

MD No: 3AK2 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AK2 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

6800



MG/KG

Aluminum

14

UJ

MG/KG

Antimony

3.3



MG/KG

Arsenic

11

J

MG/KG

Barium

0.32

UJ

MG/KG

Beryllium

1.2

U

MG/KG

Cadmium

1200

J

MG/KG

Calcium

14

J

MG/KG

Chromium

1.8

J

MG/KG

Cobalt

6.8



MG/KG

Copper

9200

J

MG/KG

Iron

8.0

J

MG/KG

Lead

2400



MG/KG

Magnesium

51

J

MG/KG

Manganese

0.24

U

MG/KG

Total Mercury

5.9

J

MG/KG

Nickel

1400



MG/KG

Potassium

8.4

U

MG/KG

Selenium

2.4

U

MG/KG

Silver

9900



MG/KG

Sodium

6.0

U

MG/KG

Thallium

28



MG/KG

Vanadium

30



MG/KG

Zinc



NA

MG/KG

Cyanide

58



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

4000

MG/KG

Aluminum

0.49 R

MG/KG

Antimony

1.5 J

MG/KG

Arsenic

7.3 J

MG/KG

Barium

0.06 J

MG/KG

Beryllium

0.67 U

MG/KG

Cadmium

3000

MG/KG

Calcium

5.6

MG/KG

Chromium

0.66 J

MG/KG

Cobalt

2.0 J

MG/KG

Copper

5800

MG/KG

Iron

3.0

MG/KG

Lead

610 J

MG/KG

Magnesium

32 J

MG/KG

Manganese

0.13 U

MG/KG

Total Mercury

2.5 J

MG/KG

Nickel

240 J

MG/KG

Potassium

4.7 U

MG/KG

Selenium

1.3 U

MG/KG

Silver

2800

MG/KG

Sodium

3.3 U

MG/KG

Thallium

9.8

MG/KG

Vanadium

9.5

MG/KG

Zinc

NA

MG/KG

Cyanide

25

%

% Moisture

Sample 9527 FY 2005 Project: 05-0928
Metals Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD04 /	MD No: 3AK5

Media: SEDIMENT	D No: 3AK5

Produced by: Goddard, Denise
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9528 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 12:25

Program: SF

Case No: 34717

Ending:

Id/Station: POSD01 /

MD No: 3AF9 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AF9 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

15000



MG/KG

Aluminum

1.1

R

MG/KG

Antimony

18

J

MG/KG

Arsenic

52

J

MG/KG

Barium

0.97

UJ

MG/KG

Beryllium

2.5

U

MG/KG

Cadmium

2300

J

MG/KG

Calcium

19

J

MG/KG

Chromium

5.3

J

MG/KG

Cobalt

14

J

MG/KG

Copper

41000

J

MG/KG

Iron

26

J

MG/KG

Lead

3400



MG/KG

Magnesium

190

J

MG/KG

Manganese

0.50

U

MG/KG

Total Mercury

8.1

J

MG/KG

Nickel

1400

J

MG/KG

Potassium

17

U

MG/KG

Selenium

5.0

U

MG/KG

Silver

9600



MG/KG

Sodium

12

U

MG/KG

Thallium

38



MG/KG

Vanadium

85



MG/KG

Zinc



NA

MG/KG

Cyanide

80



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9529 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 12:40

Program: SF

Case No: 34717

Ending:

Id/Station: POSD01D/

MD No: 3AG0 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG0 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

11000



MG/KG

Aluminum

28

UJ

MG/KG

Antimony

9.0

J

MG/KG

Arsenic

79

J

MG/KG

Barium

0.84

UJ

MG/KG

Beryllium

2.3

U

MG/KG

Cadmium

2200

J

MG/KG

Calcium

14

J

MG/KG

Chromium

7.8

J

MG/KG

Cobalt

16

J

MG/KG

Copper

23000

J

MG/KG

Iron

17

J

MG/KG

Lead

3400



MG/KG

Magnesium

260

J

MG/KG

Manganese

0.47

U

MG/KG

Total Mercury

9.7

J

MG/KG

Nickel

1500

J

MG/KG

Potassium

16

U

MG/KG

Selenium

4.7

U

MG/KG

Silver

9400



MG/KG

Sodium

12

U

MG/KG

Thallium

28



MG/KG

Vanadium

110



MG/KG

Zinc



NA

MG/KG

Cyanide

79



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9530 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 13:20

Program: SF

Case No: 34717

Ending:

Id/Station: POSD02 /

MD No: 3AG1 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG1 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

9300



MG/KG

Aluminum

17

UJ

MG/KG

Antimony

7.7

J

MG/KG

Arsenic

160

J

MG/KG

Barium

0.74

UJ

MG/KG

Beryllium

1.4

U

MG/KG

Cadmium

1900

J

MG/KG

Calcium

13

J

MG/KG

Chromium

7.4

J

MG/KG

Cobalt

14

J

MG/KG

Copper

18000

J

MG/KG

Iron

14

J

MG/KG

Lead

3600



MG/KG

Magnesium

380

J

MG/KG

Manganese

0.09

UJ

MG/KG

Total Mercury

12

J

MG/KG

Nickel

1900



MG/KG

Potassium

9.8

U

MG/KG

Selenium

2.8

U

MG/KG

Silver

8100



MG/KG

Sodium

7.0

U

MG/KG

Thallium

25



MG/KG

Vanadium

74



MG/KG

Zinc



NA

MG/KG

Cyanide

64



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9531 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 13:20

Program: SF

Case No: 34717

Ending:

Id/Station: POSD03 /

MD No: 3AG2 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG2 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

1900



MG/KG

Aluminum

8.1

UJ

MG/KG

Antimony

1.0

J

MG/KG

Arsenic

390

J

MG/KG

Barium

0.15

UJ

MG/KG

Beryllium

0.92



MG/KG

Cadmium

11000

J

MG/KG

Calcium

3.6

J

MG/KG

Chromium

1.2

J

MG/KG

Cobalt

2.9

J

MG/KG

Copper

3500

J

MG/KG

Iron

8.8

J

MG/KG

Lead

460

J

MG/KG

Magnesium

160

J

MG/KG

Manganese

0.14

U

MG/KG

Total Mercury

1.6

J

MG/KG

Nickel

200

J

MG/KG

Potassium

4.7

U

MG/KG

Selenium

1.4

U

MG/KG

Silver

830



MG/KG

Sodium

3.4

U

MG/KG

Thallium

4.3

J

MG/KG

Vanadium

83



MG/KG

Zinc



NA

MG/KG

Cyanide

26



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9532 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 12:50

Program: SF

Case No: 34717

Ending:

Id/Station: POSF04 /

MD No: 3AG3 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AG3 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

2600



MG/KG

Aluminum

6.9

UJ

MG/KG

Antimony

0.41

R

MG/KG

Arsenic

15

J

MG/KG

Barium

0.03

UJ

MG/KG

Beryllium

0.58

U

MG/KG

Cadmium

2000

J

MG/KG

Calcium

2.7

J

MG/KG

Chromium

0.49

J

MG/KG

Cobalt

2.0

J

MG/KG

Copper

1900

J

MG/KG

Iron

6.6

J

MG/KG

Lead

160

J

MG/KG

Magnesium

21

J

MG/KG

Manganese

0.03

UJ

MG/KG

Total Mercury

1.2

J

MG/KG

Nickel

89

J

MG/KG

Potassium

4.1

U

MG/KG

Selenium

1.2

U

MG/KG

Silver

530

J

MG/KG

Sodium

2.9

U

MG/KG

Thallium

4.6

J

MG/KG

Vanadium

21



MG/KG

Zinc



NA

MG/KG

Cyanide

14



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9533 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 12:20

Program: SF

Case No: 34717

Ending:

Id/Station: POSF05 /

MD No: 3AG4 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AG4 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5400



MG/KG

Aluminum

6.9

UJ

MG/KG

Antimony

1.3

J

MG/KG

Arsenic

16

J

MG/KG

Barium

0.03

UJ

MG/KG

Beryllium

0.57

U

MG/KG

Cadmium

320

J

MG/KG

Calcium

5.3

J

MG/KG

Chromium

0.87

J

MG/KG

Cobalt

2.5

J

MG/KG

Copper

5200

J

MG/KG

Iron

6.0

J

MG/KG

Lead

210

J

MG/KG

Magnesium

160

J

MG/KG

Manganese

0.04

UJ

MG/KG

Total Mercury

1.6

J

MG/KG

Nickel

120

J

MG/KG

Potassium

0.27

R

MG/KG

Selenium

1.2

U

MG/KG

Silver

440

J

MG/KG

Sodium

2.9

U

MG/KG

Thallium

9.8



MG/KG

Vanadium

6.3

J

MG/KG

Zinc



NA

MG/KG

Cyanide

13



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9534 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/03/2005 12:20

Program: SF

Case No: 34717

Ending:

Id/Station: POSF05S /

MD No: 3AG5 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AG5 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5500



MG/KG

Aluminum

7.0

UJ

MG/KG

Antimony

1.3

J

MG/KG

Arsenic

16

J

MG/KG

Barium

0.04

UJ

MG/KG

Beryllium

0.58

U

MG/KG

Cadmium

380

J

MG/KG

Calcium

5.1

J

MG/KG

Chromium

0.91

J

MG/KG

Cobalt

2.6

J

MG/KG

Copper

5000

J

MG/KG

Iron

6.5

J

MG/KG

Lead

220

J

MG/KG

Magnesium

170

J

MG/KG

Manganese

0.05

UJ

MG/KG

Total Mercury

1.6

J

MG/KG

Nickel

120

J

MG/KG

Potassium

0.58

J

MG/KG

Selenium

1.2

U

MG/KG

Silver

590



MG/KG

Sodium

2.9

U

MG/KG

Thallium

9.7



MG/KG

Vanadium

6.5

J

MG/KG

Zinc



NA

MG/KG

Cyanide

14



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9535 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 09:00

Program: SF

Case No: 34717

Ending:

Id/Station: OPSD02 /

MD No: 3AG7 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG7 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5000



MG/KG

Aluminum

1.6

J

MG/KG

Antimony

3.6

J

MG/KG

Arsenic

81

J

MG/KG

Barium

0.05

J

MG/KG

Beryllium

0.58

U

MG/KG

Cadmium

970

J

MG/KG

Calcium

39

J

MG/KG

Chromium

4.1

J

MG/KG

Cobalt

46

J

MG/KG

Copper

56000

J

MG/KG

Iron

130

J

MG/KG

Lead

620



MG/KG

Magnesium

350

J

MG/KG

Manganese

0.12

U

MG/KG

Total Mercury

14

J

MG/KG

Nickel

260

J

MG/KG

Potassium

4.1

U

MG/KG

Selenium

1.2

U

MG/KG

Silver

1200



MG/KG

Sodium

0.54

J

MG/KG

Thallium

11



MG/KG

Vanadium

980



MG/KG

Zinc



NA

MG/KG

Cyanide

15



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9536 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 09:25

Program: SF

Case No: 34717

Ending:

Id/Station: OPSD02D /

MD No: 3AG8 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG8 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

7800



MG/KG

Aluminum

7.4

UJ

MG/KG

Antimony

2.2

J

MG/KG

Arsenic

18

J

MG/KG

Barium

0.08

UJ

MG/KG

Beryllium

0.61

U

MG/KG

Cadmium

2100

J

MG/KG

Calcium

10

J

MG/KG

Chromium

1.1

J

MG/KG

Cobalt

6.5

J

MG/KG

Copper

10000

J

MG/KG

Iron

8.8

J

MG/KG

Lead

540

J

MG/KG

Magnesium

46

J

MG/KG

Manganese

0.12

U

MG/KG

Total Mercury

2.3

J

MG/KG

Nickel

240

J

MG/KG

Potassium

0.47

R

MG/KG

Selenium

1.2

U

MG/KG

Silver

1100



MG/KG

Sodium

3.1

U

MG/KG

Thallium

16



MG/KG

Vanadium

44



MG/KG

Zinc



NA

MG/KG

Cyanide

18



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9537 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 09:50

Program: SF

Case No: 34717

Ending:

Id/Station: OPSD01 /

MD No: 3AG9 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AG9 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

9500



MG/KG

Aluminum

0.45

J

MG/KG

Antimony

1.2

J

MG/KG

Arsenic

260

J

MG/KG

Barium

0.04

UJ

MG/KG

Beryllium

0.54

U

MG/KG

Cadmium

16000

J

MG/KG

Calcium

10

J

MG/KG

Chromium

3.3

J

MG/KG

Cobalt

45

J

MG/KG

Copper

8800

J

MG/KG

Iron

80

J

MG/KG

Lead

1800



MG/KG

Magnesium

54

J

MG/KG

Manganese

0.03

UJ

MG/KG

Total Mercury

6.7

J

MG/KG

Nickel

270

J

MG/KG

Potassium

3.8

U

MG/KG

Selenium

1.1

U

MG/KG

Silver

1400



MG/KG

Sodium

0.47

R

MG/KG

Thallium

18



MG/KG

Vanadium

220



MG/KG

Zinc



NA

MG/KG

Cyanide

7



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9538 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 10:20

Program: SF

Case No: 34717

Ending:

Id/Station: OPSD03 /

MD No: 3AH0 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH0 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4000



MG/KG

Aluminum

7.4

UJ

MG/KG

Antimony

1.6

J

MG/KG

Arsenic

15

J

MG/KG

Barium

0.03

UJ

MG/KG

Beryllium

0.62

U

MG/KG

Cadmium

180

J

MG/KG

Calcium

8.5

J

MG/KG

Chromium

0.41

J

MG/KG

Cobalt

13

J

MG/KG

Copper

7700

J

MG/KG

Iron

17

J

MG/KG

Lead

350

J

MG/KG

Magnesium

8.9

J

MG/KG

Manganese

0.15



MG/KG

Total Mercury

1.2

J

MG/KG

Nickel

290

J

MG/KG

Potassium

4.3

U

MG/KG

Selenium

1.2

U

MG/KG

Silver

1500



MG/KG

Sodium

3.1

U

MG/KG

Thallium

12



MG/KG

Vanadium

11



MG/KG

Zinc



NA

MG/KG

Cyanide

19



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9539 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 09:15

Program: SF

Case No: 34717

Ending:

Id/Station: ERSF01 /

MD No: 3AH1 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AH1 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4100



MG/KG

Aluminum

0.40

R

MG/KG

Antimony

2.2

J

MG/KG

Arsenic

75

J

MG/KG

Barium

0.17

UJ

MG/KG

Beryllium

0.27

J

MG/KG

Cadmium

19000

J

MG/KG

Calcium

8.1

J

MG/KG

Chromium

1.5

J

MG/KG

Cobalt

48

J

MG/KG

Copper

6800

J

MG/KG

Iron

48

J

MG/KG

Lead

830

J

MG/KG

Magnesium

120

J

MG/KG

Manganese

0.07

UJ

MG/KG

Total Mercury

4.0

J

MG/KG

Nickel

340

J

MG/KG

Potassium

6.4

U

MG/KG

Selenium

1.8

U

MG/KG

Silver

1800



MG/KG

Sodium

4.6

U

MG/KG

Thallium

8.8

J

MG/KG

Vanadium

1200



MG/KG

Zinc



NA

MG/KG

Cyanide

45



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9540 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 09:15

Program: SF

Case No: 34717

Ending:

Id/Station: ERSF01S/

MD No: 3AH2 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AH2 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5300



MG/KG

Aluminum

0.48

R

MG/KG

Antimony

2.3

J

MG/KG

Arsenic

52

J

MG/KG

Barium

0.15

UJ

MG/KG

Beryllium

0.81

U

MG/KG

Cadmium

14000

J

MG/KG

Calcium

8.7

J

MG/KG

Chromium

1.4

J

MG/KG

Cobalt

32

J

MG/KG

Copper

6500

J

MG/KG

Iron

34

J

MG/KG

Lead

770

J

MG/KG

Magnesium

82

J

MG/KG

Manganese

0.07

UJ

MG/KG

Total Mercury

3.9

J

MG/KG

Nickel

370

J

MG/KG

Potassium

5.6

U

MG/KG

Selenium

1.6

U

MG/KG

Silver

1400



MG/KG

Sodium

4.0

U

MG/KG

Thallium

11



MG/KG

Vanadium

580



MG/KG

Zinc



NA

MG/KG

Cyanide

38



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9541 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 10:10

Program: SF

Case No: 34717

Ending:

Id/Station: ERSF02 /

MD No: 3AH3 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AH3 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

2600



MG/KG

Aluminum

6.6

UJ

MG/KG

Antimony

2.7

J

MG/KG

Arsenic

24

J

MG/KG

Barium

0.06

UJ

MG/KG

Beryllium

0.55

U

MG/KG

Cadmium

1500

J

MG/KG

Calcium

3.9

J

MG/KG

Chromium

0.47

J

MG/KG

Cobalt

11

J

MG/KG

Copper

2600

J

MG/KG

Iron

71

J

MG/KG

Lead

330

UJ

MG/KG

Magnesium

35

J

MG/KG

Manganese

0.13



MG/KG

Total Mercury

1.4

J

MG/KG

Nickel

150

J

MG/KG

Potassium

0.24

R

MG/KG

Selenium

1.1

U

MG/KG

Silver

730



MG/KG

Sodium

2.8

U

MG/KG

Thallium

4.5

J

MG/KG

Vanadium

93



MG/KG

Zinc



NA

MG/KG

Cyanide

9



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9542 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 10:50

Program: SF

Case No: 34717

Ending:

Id/Station: ERSF03 /

MD No: 3AH4 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AH4 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

3000



MG/KG

Aluminum

7.5

UJ

MG/KG

Antimony

1.3

J

MG/KG

Arsenic

29

J

MG/KG

Barium

0.08

UJ

MG/KG

Beryllium

0.63

U

MG/KG

Cadmium

5900

J

MG/KG

Calcium

5.9

J

MG/KG

Chromium

0.83

J

MG/KG

Cobalt

9.9

J

MG/KG

Copper

3300

J

MG/KG

Iron

44

J

MG/KG

Lead

610

J

MG/KG

Magnesium

74

J

MG/KG

Manganese

0.07

UJ

MG/KG

Total Mercury

4.8

J

MG/KG

Nickel

o

00
CM

J

MG/KG

Potassium

4.4

U

MG/KG

Selenium

1.3

U

MG/KG

Silver

900



MG/KG

Sodium

3.1

U

MG/KG

Thallium

5.8

J

MG/KG

Vanadium

78



MG/KG

Zinc



NA

MG/KG

Cyanide

20



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9543 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 11:15

Program: SF

Case No: 34717

Ending:

Id/Station: ERSD04 /

MD No: 3AH5 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH5 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

15000



MG/KG

Aluminum

0.71

R

MG/KG

Antimony

14

J

MG/KG

Arsenic

180

J

MG/KG

Barium

0.31

UJ

MG/KG

Beryllium

0.98

U

MG/KG

Cadmium

3200

J

MG/KG

Calcium

16

J

MG/KG

Chromium

2.5

J

MG/KG

Cobalt

39

J

MG/KG

Copper

11000

J

MG/KG

Iron

26

J

MG/KG

Lead

1700



MG/KG

Magnesium

210

J

MG/KG

Manganese

0.08

UJ

MG/KG

Total Mercury

5.0

J

MG/KG

Nickel

700

J

MG/KG

Potassium

6.8

U

MG/KG

Selenium

2.0

U

MG/KG

Silver

2500



MG/KG

Sodium

4.9

U

MG/KG

Thallium

23



MG/KG

Vanadium

110



MG/KG

Zinc



NA

MG/KG

Cyanide

49



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9544 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 11:25

Program: SF

Case No: 34717

Ending:

Id/Station: ERSD04D /

MD No: 3AH6 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH6 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

3500



MG/KG

Aluminum

0.55

R

MG/KG

Antimony

2.1

J

MG/KG

Arsenic

97

J

MG/KG

Barium

0.14

UJ

MG/KG

Beryllium

0.71

U

MG/KG

Cadmium

12000

J

MG/KG

Calcium

8.3

J

MG/KG

Chromium

1.3

J

MG/KG

Cobalt

18

J

MG/KG

Copper

5400

J

MG/KG

Iron

91

J

MG/KG

Lead

2300



MG/KG

Magnesium

85

J

MG/KG

Manganese

0.12

UJ

MG/KG

Total Mercury

2.6

J

MG/KG

Nickel

o

00
CM

J

MG/KG

Potassium

5.0

U

MG/KG

Selenium

1.4

U

MG/KG

Silver

1300



MG/KG

Sodium

0.35

R

MG/KG

Thallium

8.2



MG/KG

Vanadium

130



MG/KG

Zinc



NA

MG/KG

Cyanide

29



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9545 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 11:45

Program: SF

Case No: 34717

Ending:

Id/Station: ERSD05 /

MD No: 3AH7 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH7 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4300



MG/KG

Aluminum

1.2

J

MG/KG

Antimony

4.5

J

MG/KG

Arsenic

430

J

MG/KG

Barium

0.30

UJ

MG/KG

Beryllium

1.1

U

MG/KG

Cadmium

2900

J

MG/KG

Calcium

9.2

J

MG/KG

Chromium

2.2

J

MG/KG

Cobalt

120

J

MG/KG

Copper

8300

J

MG/KG

Iron

21

J

MG/KG

Lead

1700



MG/KG

Magnesium

73

J

MG/KG

Manganese

0.05

UJ

MG/KG

Total Mercury

3.0

J

MG/KG

Nickel

730

J

MG/KG

Potassium

7.4

U

MG/KG

Selenium

2.1

U

MG/KG

Silver

4300



MG/KG

Sodium

5.3

U

MG/KG

Thallium

11

J

MG/KG

Vanadium

100



MG/KG

Zinc



NA

MG/KG

Cyanide

52



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9546 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 10:10

Program: SF

Case No: 34717

Ending:

Id/Station: DUSD01 /

MD No: 3AH8 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH8 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

12000



MG/KG

Aluminum

1.1

R

MG/KG

Antimony

53

J

MG/KG

Arsenic

140

J

MG/KG

Barium

2.0



MG/KG

Beryllium

1.1

U

MG/KG

Cadmium

1500

J

MG/KG

Calcium

22

J

MG/KG

Chromium

8.3

J

MG/KG

Cobalt

33

J

MG/KG

Copper

13000

J

MG/KG

Iron

18

J

MG/KG

Lead

1100



MG/KG

Magnesium

96

J

MG/KG

Manganese

0.13

UJ

MG/KG

Total Mercury

18

J

MG/KG

Nickel

1600



MG/KG

Potassium

0.88

J

MG/KG

Selenium

2.2

U

MG/KG

Silver

1800



MG/KG

Sodium

1.9

J

MG/KG

Thallium

50



MG/KG

Vanadium

56



MG/KG

Zinc



NA

MG/KG

Cyanide

55



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9547 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 11:05

Program: SF

Case No: 34717

Ending:

Id/Station: DUSD01D/

MD No: 3AH9 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AH9 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

9000



MG/KG

Aluminum

0.59

R

MG/KG

Antimony

35

J

MG/KG

Arsenic

87

J

MG/KG

Barium

1.3



MG/KG

Beryllium

1.2

U

MG/KG

Cadmium

1400

J

MG/KG

Calcium

18

J

MG/KG

Chromium

7.9

J

MG/KG

Cobalt

22

J

MG/KG

Copper

13000

J

MG/KG

Iron

15

J

MG/KG

Lead

1200



MG/KG

Magnesium

130

J

MG/KG

Manganese

0.15

UJ

MG/KG

Total Mercury

14

J

MG/KG

Nickel

1200

J

MG/KG

Potassium

0.73

R

MG/KG

Selenium

2.4

U

MG/KG

Silver

1900



MG/KG

Sodium

0.53

R

MG/KG

Thallium

38



MG/KG

Vanadium

49

J

MG/KG

Zinc



NA

MG/KG

Cyanide

58



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9548 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 12:00

Program: SF

Case No: 34717

Ending:

Id/Station: DUSD02 /

MD No: 3AJ0 Inorg Contractor: LIBRTY

Media: SEDIMENT

D No: 3AJ0 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4800



MG/KG

Aluminum

7.9

UJ

MG/KG

Antimony

1.0

R

MG/KG

Arsenic

400



MG/KG

Barium

0.22

UJ

MG/KG

Beryllium

0.65

U

MG/KG

Cadmium

330

J

MG/KG

Calcium

7.3

J

MG/KG

Chromium

0.83

J

MG/KG

Cobalt

2.6

J

MG/KG

Copper

2900

J

MG/KG

Iron

16

J

MG/KG

Lead

470

J

MG/KG

Magnesium

12

J

MG/KG

Manganese

0.13

U

MG/KG

Total Mercury

1.6

J

MG/KG

Nickel

240

J

MG/KG

Potassium

4.6

U

MG/KG

Selenium

1.3

U

MG/KG

Silver

630

J

MG/KG

Sodium

3.3

U

MG/KG

Thallium

11



MG/KG

Vanadium

15



MG/KG

Zinc



NA

MG/KG

Cyanide

24



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9549 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 13:20

Program: SF

Case No: 34717

Ending:

Id/Station: DUSF05 /

MD No: 3AJ1 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ1 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4000



MG/KG

Aluminum

6.8

UJ

MG/KG

Antimony

1.0

R

MG/KG

Arsenic

15

J

MG/KG

Barium

0.04

UJ

MG/KG

Beryllium

0.57

U

MG/KG

Cadmium

540

J

MG/KG

Calcium

5.6

J

MG/KG

Chromium

0.45

J

MG/KG

Cobalt

1.9

J

MG/KG

Copper

4300

J

MG/KG

Iron

13

J

MG/KG

Lead

140

J

MG/KG

Magnesium

36

J

MG/KG

Manganese

0.03

UJ

MG/KG

Total Mercury

1.3

J

MG/KG

Nickel

85

J

MG/KG

Potassium

4.0

U

MG/KG

Selenium

1.1

U

MG/KG

Silver

96

UJ

MG/KG

Sodium

2.8

U

MG/KG

Thallium

9.2



MG/KG

Vanadium

11



MG/KG

Zinc



NA

MG/KG

Cyanide

12



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9550 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 13:45

Program: SF

Case No: 34717

Ending:

Id/Station: DUSF04 /

MD No: 3AJ2 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ2 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5100



MG/KG

Aluminum

0.28

R

MG/KG

Antimony

1.5



MG/KG

Arsenic

17

J

MG/KG

Barium

0.10

UJ

MG/KG

Beryllium

0.57

U

MG/KG

Cadmium

230

J

MG/KG

Calcium

9.1

J

MG/KG

Chromium

0.74

J

MG/KG

Cobalt

2.0

J

MG/KG

Copper

7900

J

MG/KG

Iron

26

J

MG/KG

Lead

140

J

MG/KG

Magnesium

180

J

MG/KG

Manganese

0.04

UJ

MG/KG

Total Mercury

1.6

J

MG/KG

Nickel

82

J

MG/KG

Potassium

0.48

R

MG/KG

Selenium

1.1

U

MG/KG

Silver

110

UJ

MG/KG

Sodium

2.8

U

MG/KG

Thallium

14



MG/KG

Vanadium

14



MG/KG

Zinc



NA

MG/KG

Cyanide

12



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/28/2005 14:33

Sample 9551 FY 2005 Project:

05-0928

Produced by: Goddard, Denise

Metals Scan



Requestor:



Project Leader: FSLOAN

Facility: Hurricane Katrina Response



Beginning: 10/04/2005 14:05

Program: SF

Case No: 34717

Ending:

Id/Station: DUSF03 /

MD No: 3AJ3 Inorg Contractor: LIBRTY

Media: SURFACE SOIL

D No: 3AJ3 Org Contractor: LIBRTY

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

6500



MG/KG

Aluminum

0.24

R

MG/KG

Antimony

1.4



MG/KG

Arsenic

27



MG/KG

Barium

0.12

UJ

MG/KG

Beryllium

0.56

U

MG/KG

Cadmium

1100



MG/KG

Calcium

11

J

MG/KG

Chromium

1.2

J

MG/KG

Cobalt

2.7

J

MG/KG

Copper

9900

J

MG/KG

Iron

16

J

MG/KG

Lead

150

J

MG/KG

Magnesium

380

J

MG/KG

Manganese

0.11

U

MG/KG

Total Mercury

2.5

J

MG/KG

Nickel

88

J

MG/KG

Potassium

4.0

U

MG/KG

Selenium

1.1

U

MG/KG

Silver

110

UJ

MG/KG

Sodium

2.8

U

MG/KG

Thallium

16



MG/KG

Vanadium

21



MG/KG

Zinc



NA

MG/KG

Cyanide

11



%

% Moisture

Cyanide Analysis Not Requested

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.8

UJ

UG/KG

alpha-BHC

1.8

U

UG/KG

beta-BHC

1.8

U

UG/KG

delta-BHC

1.8

UJ

UG/KG

gamma-BHC (Lindane)

1.8

U

UG/KG

Heptachlor

1.8

U

UG/KG

Aldrin

1.8

U

UG/KG

Heptachlor Epoxide

1.8

U

UG/KG

Endosulfan I (alpha)

3.5

U

UG/KG

Dieldrin

3.5

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.5

U

UG/KG

Endrin

3.5

U

UG/KG

Endosulfan II (beta)

3.5

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.5

U

UG/KG

Endosulfan Sulfate

3.5

U

UG/KG

4,4'-DDT (p, p'-DDT)

3.7

NJ

UG/KG

Methoxychlor

3.5

U

UG/KG

Endrin Ketone

3.5

U

UG/KG

Endrin Aldehyde

1.8

U

UG/KG

alpha-Chlordane /2

1.8

U

UG/KG

gamma-Chlordane /2

180

U

UG/KG

Toxaphene

35

U

UG/KG

PCB-1016 (Aroclor 1016)

71

U

UG/KG

PCB-1221 (Aroclor 1221)

35

U

UG/KG

PCB-1232 (Aroclor 1232)

35

U

UG/KG

PCB-1242 (Aroclor 1242)

35

U

UG/KG

PCB-1248 (Aroclor 1248)

35

U

UG/KG

PCB-1254 (Aroclor 1254)

35

U

UG/KG

PCB-1260 (Aroclor 1260)

6



%

% Moisture

Sample 9518 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF08 /	MD No: 3AJ4

Media: SURFACE SOIL	D No: 3AJ4

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.8

UJ

UG/KG

alpha-BHC

2.8

U

UG/KG

beta-BHC

2.8

U

UG/KG

delta-BHC

2.8

UJ

UG/KG

gamma-BHC (Lindane)

2.8

U

UG/KG

Heptachlor

2.8

U

UG/KG

Aldrin

2.8

U

UG/KG

Heptachlor Epoxide

2.8

U

UG/KG

Endosulfan I (alpha)

5.5

U

UG/KG

Dieldrin

5.5

U

UG/KG

4,4'-DDE (p,p'-DDE)

5.5

U

UG/KG

Endrin

5.5

U

UG/KG

Endosulfan II (beta)

5.5

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

5.5

U

UG/KG

Endosulfan Sulfate

5.5

U

UG/KG

4,4'-DDT (p, p'-DDT)

28

U

UG/KG

Methoxychlor

5.5

U

UG/KG

Endrin Ketone

5.5

U

UG/KG

Endrin Aldehyde

2.8

U

UG/KG

alpha-Chlordane /2

2.8

U

UG/KG

gamma-Chlordane /2

280

U

UG/KG

Toxaphene

55

U

UG/KG

PCB-1016 (Aroclor 1016)

110

U

UG/KG

PCB-1221 (Aroclor 1221)

55

U

UG/KG

PCB-1232 (Aroclor 1232)

55

U

UG/KG

PCB-1242 (Aroclor 1242)

55

U

UG/KG

PCB-1248 (Aroclor 1248)

55

u

UG/KG

PCB-1254 (Aroclor 1254)

55

u

UG/KG

PCB-1260 (Aroclor 1260)

40



%

% Moisture

Sample 9519 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD07 /	MD No: 3AJ5

Media: SEDIMENT	D No: 3AJ5

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.2

UJ

UG/KG

alpha-BHC

2.2

U

UG/KG

beta-BHC

2.2

U

UG/KG

delta-BHC

2.2

UJ

UG/KG

gamma-BHC (Lindane)

2.2

U

UG/KG

Heptachlor

2.2

U

UG/KG

Aldrin

2.2

U

UG/KG

Heptachlor Epoxide

2.2

U

UG/KG

Endosulfan 1 (alpha)

4.3

U

UG/KG

Dieldrin

4.3

U

UG/KG

4,4'-DDE (p,p'-DDE)

4.3

U

UG/KG

Endrin

4.3

U

UG/KG

Endosulfan II (beta)

4.3

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.3

U

UG/KG

Endosulfan Sulfate

4.3

U

UG/KG

4,4'-DDT (p, p'-DDT)

22

U

UG/KG

Methoxychlor

4.3

U

UG/KG

Endrin Ketone

4.3

U

UG/KG

Endrin Aldehyde

2.2

U

UG/KG

alpha-Chlordane /2

2.2

U

UG/KG

gamma-Chlordane /2

220

U

UG/KG

Toxaphene

43

U

UG/KG

PCB-1016 (Aroclor 1016)

87

U

UG/KG

PCB-1221 (Aroclor 1221)

43

U

UG/KG

PCB-1232 (Aroclor 1232)

43

U

UG/KG

PCB-1242 (Aroclor 1242)

43

U

UG/KG

PCB-1248 (Aroclor 1248)

43

U

UG/KG

PCB-1254 (Aroclor 1254)

43

u

UG/KG

PCB-1260 (Aroclor 1260)

23



%

% Moisture

Sample 9520 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF02 /	MD No: 3AJ6

Media: SURFACE SOIL	D No: 3AJ6

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.2

UJ

UG/KG

alpha-BHC

2.2

U

UG/KG

beta-BHC

2.2

U

UG/KG

delta-BHC

2.2

UJ

UG/KG

gamma-BHC (Lindane)

2.2

U

UG/KG

Heptachlor

2.2

U

UG/KG

Aldrin

2.2

U

UG/KG

Heptachlor Epoxide

2.2

U

UG/KG

Endosulfan I (alpha)

4.2

U

UG/KG

Dieldrin

4.2

U

UG/KG

4,4'-DDE (p,p'-DDE)

4.2

U

UG/KG

Endrin

4.2

U

UG/KG

Endosulfan II (beta)

4.2

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.2

U

UG/KG

Endosulfan Sulfate

4.2

U

UG/KG

4,4'-DDT (p, p'-DDT)

5.3

NJ

UG/KG

Methoxychlor

4.2

U

UG/KG

Endrin Ketone

4.2

U

UG/KG

Endrin Aldehyde

2.2

U

UG/KG

alpha-Chlordane /2

2.2

U

UG/KG

gamma-Chlordane /2

220

U

UG/KG

Toxaphene

42

U

UG/KG

PCB-1016 (Aroclor 1016)

85

U

UG/KG

PCB-1221 (Aroclor 1221)

42

U

UG/KG

PCB-1232 (Aroclor 1232)

42

U

UG/KG

PCB-1242 (Aroclor 1242)

42

U

UG/KG

PCB-1248 (Aroclor 1248)

42

U

UG/KG

PCB-1254 (Aroclor 1254)

42

U

UG/KG

PCB-1260 (Aroclor 1260)

21



%

% Moisture

Sample 9521 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF02S /	MD No: 3AJ7

Media: SURFACE SOIL	D No: 3AJ7

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.9

UJ

UG/KG

alpha-BHC

1.8

U

UG/KG

beta-BHC

1.9

U

UG/KG

delta-BHC

1.9

UJ

UG/KG

gamma-BHC (Lindane)

1.9

U

UG/KG

Heptachlor

1.9

U

UG/KG

Aldrin

1.9

U

UG/KG

Heptachlor Epoxide

1.9

U

UG/KG

Endosulfan I (alpha)

3.6

U

UG/KG

Dieldrin

3.6

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.6

U

UG/KG

Endrin

3.6

U

UG/KG

Endosulfan II (beta)

3.6

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.6

U

UG/KG

Endosulfan Sulfate

3.6

U

UG/KG

4,4'-DDT (p, p'-DDT)

19

U

UG/KG

Methoxychlor

3.6

U

UG/KG

Endrin Ketone

3.6

U

UG/KG

Endrin Aldehyde

1.9

U

UG/KG

alpha-Chlordane /2

1.9

U

UG/KG

gamma-Chlordane /2

190

U

UG/KG

Toxaphene

36

U

UG/KG

PCB-1016 (Aroclor 1016)

74

U

UG/KG

PCB-1221 (Aroclor 1221)

36

U

UG/KG

PCB-1232 (Aroclor 1232)

36

U

UG/KG

PCB-1242 (Aroclor 1242)

36

U

UG/KG

PCB-1248 (Aroclor 1248)

36

U

UG/KG

PCB-1254 (Aroclor 1254)

36

u

UG/KG

PCB-1260 (Aroclor 1260)

9



%

% Moisture

Sample 9522 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF01 /	MD No: 3AJ8

Media: SURFACE SOIL	D No: 3AJ8

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:55
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.5

UJ

UG/KG

alpha-BHC

3.5

U

UG/KG

beta-BHC

3.5

U

UG/KG

delta-BHC

3.5

UJ

UG/KG

gamma-BHC (Lindane)

3.5

U

UG/KG

Heptachlor

3.5

U

UG/KG

Aldrin

3.5

U

UG/KG

Heptachlor Epoxide

3.5

U

UG/KG

Endosulfan I (alpha)

6.7

U

UG/KG

Dieldrin

6.7

U

UG/KG

4,4'-DDE (p,p'-DDE)

6.7

U

UG/KG

Endrin

6.7

U

UG/KG

Endosulfan II (beta)

6.7

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

6.7

U

UG/KG

Endosulfan Sulfate

6.7

U

UG/KG

4,4'-DDT (p, p'-DDT)

7.8

NJ

UG/KG

Methoxychlor

6.7

U

UG/KG

Endrin Ketone

6.7

U

UG/KG

Endrin Aldehyde

3.5

U

UG/KG

alpha-Chlordane /2

3.5

U

UG/KG

gamma-Chlordane /2

350

U

UG/KG

Toxaphene

67

U

UG/KG

PCB-1016 (Aroclor 1016)

140

U

UG/KG

PCB-1221 (Aroclor 1221)

67

U

UG/KG

PCB-1232 (Aroclor 1232)

67

U

UG/KG

PCB-1242 (Aroclor 1242)

67

U

UG/KG

PCB-1248 (Aroclor 1248)

67

U

UG/KG

PCB-1254 (Aroclor 1254)

67

U

UG/KG

PCB-1260 (Aroclor 1260)

51



%

% Moisture

Sample 9523 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD06 /	MD No: 3AJ9

Media: SEDIMENT	D No: 3AJ9

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

7.4

UJ

UG/KG

alpha-BHC

7.4

U

UG/KG

beta-BHC

7.4

U

UG/KG

delta-BHC

7.4

UJ

UG/KG

gamma-BHC (Lindane)

7.4

U

UG/KG

Heptachlor

7.4

U

UG/KG

Aldrin

7.4

U

UG/KG

Heptachlor Epoxide

7.4

U

UG/KG

Endosulfan I (alpha)

14

U

UG/KG

Dieldrin

14

U

UG/KG

4,4'-DDE (p,p'-DDE)

14

U

UG/KG

Endrin

14

U

UG/KG

Endosulfan II (beta)

14

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

14

U

UG/KG

Endosulfan Sulfate

14

U

UG/KG

4,4'-DDT (p, p'-DDT)

74

U

UG/KG

Methoxychlor

14

U

UG/KG

Endrin Ketone

14

U

UG/KG

Endrin Aldehyde

7.4

U

UG/KG

alpha-Chlordane /2

3.8

NJ

UG/KG

gamma-Chlordane /2

740

U

UG/KG

Toxaphene

140

U

UG/KG

PCB-1016 (Aroclor 1016)

290

U

UG/KG

PCB-1221 (Aroclor 1221)

140

U

UG/KG

PCB-1232 (Aroclor 1232)

140

U

UG/KG

PCB-1242 (Aroclor 1242)

140

U

UG/KG

PCB-1248 (Aroclor 1248)

140

U

UG/KG

PCB-1254 (Aroclor 1254)

140

U

UG/KG

PCB-1260 (Aroclor 1260)

77



%

% Moisture

Sample 9524 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD05 /	MD No: 3AK0

Media: SEDIMENT	D No: 3AK0

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

6.3

UJ

UG/KG

alpha-BHC

6.3

U

UG/KG

beta-BHC

6.3

U

UG/KG

delta-BHC

6.3

UJ

UG/KG

gamma-BHC (Lindane)

6.3

U

UG/KG

Heptachlor

6.3

U

UG/KG

Aldrin

6.3

U

UG/KG

Heptachlor Epoxide

6.3

U

UG/KG

Endosulfan I (alpha)

12

U

UG/KG

Dieldrin

12

U

UG/KG

4,4'-DDE (p,p'-DDE)

12

U

UG/KG

Endrin

12

U

UG/KG

Endosulfan II (beta)

12

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

12

U

UG/KG

Endosulfan Sulfate

12

U

UG/KG

4,4'-DDT (p, p'-DDT)

63

U

UG/KG

Methoxychlor

12

U

UG/KG

Endrin Ketone

12

U

UG/KG

Endrin Aldehyde

6.3

U

UG/KG

alpha-Chlordane /2

3.2

NJ

UG/KG

gamma-Chlordane /2

630

U

UG/KG

Toxaphene

120

U

UG/KG

PCB-1016 (Aroclor 1016)

250

U

UG/KG

PCB-1221 (Aroclor 1221)

120

U

UG/KG

PCB-1232 (Aroclor 1232)

120

U

UG/KG

PCB-1242 (Aroclor 1242)

120

U

UG/KG

PCB-1248 (Aroclor 1248)

120

U

UG/KG

PCB-1254 (Aroclor 1254)

120

U

UG/KG

PCB-1260 (Aroclor 1260)

73



%

% Moisture

Sample 9525 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD05D /	MD No: 3AK1

Media: SEDIMENT	D No: 3AK1

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.7

UJ

UG/KG

alpha-BHC

3.7

U

UG/KG

beta-BHC

3.7

U

UG/KG

delta-BHC

3.7

UJ

UG/KG

gamma-BHC (Lindane)

3.7

U

UG/KG

Heptachlor

3.7

U

UG/KG

Aldrin

3.7

U

UG/KG

Heptachlor Epoxide

3.7

U

UG/KG

Endosulfan I (alpha)

7.2

U

UG/KG

Dieldrin

7.2

U

UG/KG

4,4'-DDE (p,p'-DDE)

7.2

U

UG/KG

Endrin

7.2

U

UG/KG

Endosulfan II (beta)

7.2

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

7.2

U

UG/KG

Endosulfan Sulfate

7.2

U

UG/KG

4,4'-DDT (p, p'-DDT)

37

U

UG/KG

Methoxychlor

7.2

U

UG/KG

Endrin Ketone

7.2

U

UG/KG

Endrin Aldehyde

3.7

U

UG/KG

alpha-Chlordane /2

3.7

U

UG/KG

gamma-Chlordane /2

370

U

UG/KG

Toxaphene

72

U

UG/KG

PCB-1016 (Aroclor 1016)

150

U

UG/KG

PCB-1221 (Aroclor 1221)

72

U

UG/KG

PCB-1232 (Aroclor 1232)

72

U

UG/KG

PCB-1242 (Aroclor 1242)

72

U

UG/KG

PCB-1248 (Aroclor 1248)

72

U

UG/KG

PCB-1254 (Aroclor 1254)

72

u

UG/KG

PCB-1260 (Aroclor 1260)

54



%

% Moisture

Sample 9526 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD03 /	MD No: 3AK2

Media: SEDIMENT	D No: 3AK2

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.3

UJ

UG/KG

alpha-BHC

2.3

U

UG/KG

beta-BHC

2.3

U

UG/KG

delta-BHC

2.3

UJ

UG/KG

gamma-BHC (Lindane)

2.3

U

UG/KG

Heptachlor

2.3

U

UG/KG

Aldrin

2.3

U

UG/KG

Heptachlor Epoxide

2.3

U

UG/KG

Endosulfan 1 (alpha)

4.4

U

UG/KG

Dieldrin

4.4

U

UG/KG

4,4'-DDE (p,p'-DDE)

4.4

U

UG/KG

Endrin

4.4

U

UG/KG

Endosulfan II (beta)

4.4

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.4

U

UG/KG

Endosulfan Sulfate

4.4

U

UG/KG

4,4'-DDT (p, p'-DDT)

23

U

UG/KG

Methoxychlor

4.4

U

UG/KG

Endrin Ketone

4.4

U

UG/KG

Endrin Aldehyde

2.3

U

UG/KG

alpha-Chlordane /2

2.3

U

UG/KG

gamma-Chlordane /2

230

U

UG/KG

Toxaphene

44

U

UG/KG

PCB-1016 (Aroclor 1016)

89

U

UG/KG

PCB-1221 (Aroclor 1221)

44

U

UG/KG

PCB-1232 (Aroclor 1232)

44

U

UG/KG

PCB-1242 (Aroclor 1242)

44

U

UG/KG

PCB-1248 (Aroclor 1248)

44

U

UG/KG

PCB-1254 (Aroclor 1254)

44

u

UG/KG

PCB-1260 (Aroclor 1260)

25



%

% Moisture

Sample 9527 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD04 /	MD No: 3AK5

Media: SEDIMENT	D No: 3AK5

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

7.7

UJ

UG/KG

alpha-BHC

7.7

U

UG/KG

beta-BHC

7.7

U

UG/KG

delta-BHC

7.7

UJ

UG/KG

gamma-BHC (Lindane)

7.7

U

UG/KG

Heptachlor

7.7

U

UG/KG

Aldrin

7.7

U

UG/KG

Heptachlor Epoxide

7.7

U

UG/KG

Endosulfan I (alpha)

15

U

UG/KG

Dieldrin

15

U

UG/KG

4,4'-DDE (p,p'-DDE)

15

U

UG/KG

Endrin

15

U

UG/KG

Endosulfan II (beta)

15

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

15

U

UG/KG

Endosulfan Sulfate

15

U

UG/KG

4,4'-DDT (p, p'-DDT)

77

U

UG/KG

Methoxychlor

15

U

UG/KG

Endrin Ketone

15

U

UG/KG

Endrin Aldehyde

7.7

U

UG/KG

alpha-Chlordane /2

7.7

U

UG/KG

gamma-Chlordane /2

770

U

UG/KG

Toxaphene

150

U

UG/KG

PCB-1016 (Aroclor 1016)

300

U

UG/KG

PCB-1221 (Aroclor 1221)

150

u

UG/KG

PCB-1232 (Aroclor 1232)

150

u

UG/KG

PCB-1242 (Aroclor 1242)

150

u

UG/KG

PCB-1248 (Aroclor 1248)

150

u

UG/KG

PCB-1254 (Aroclor 1254)

150

u

UG/KG

PCB-1260 (Aroclor 1260)

78



%

% Moisture

Sample 9528 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD01 /	MD No: 3AF9

Media: SEDIMENT	D No: 3AF9

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

8.5

UJ

UG/KG

alpha-BHC

8.5

U

UG/KG

beta-BHC

8.5

U

UG/KG

delta-BHC

8.5

UJ

UG/KG

gamma-BHC (Lindane)

8.5

U

UG/KG

Heptachlor

8.5

U

UG/KG

Aldrin

8.5

U

UG/KG

Heptachlor Epoxide

8.5

U

UG/KG

Endosulfan I (alpha)

17

U

UG/KG

Dieldrin

17

U

UG/KG

4,4'-DDE (p,p'-DDE)

17

U

UG/KG

Endrin

17

U

UG/KG

Endosulfan II (beta)

17

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

17

U

UG/KG

Endosulfan Sulfate

17

U

UG/KG

4,4'-DDT (p, p'-DDT)

85

U

UG/KG

Methoxychlor

17

U

UG/KG

Endrin Ketone

17

U

UG/KG

Endrin Aldehyde

8.5

U

UG/KG

alpha-Chlordane /2

8.5

U

UG/KG

gamma-Chlordane /2

850

U

UG/KG

Toxaphene

170

U

UG/KG

PCB-1016 (Aroclor 1016)

340

U

UG/KG

PCB-1221 (Aroclor 1221)

170

u

UG/KG

PCB-1232 (Aroclor 1232)

170

u

UG/KG

PCB-1242 (Aroclor 1242)

170

u

UG/KG

PCB-1248 (Aroclor 1248)

170

u

UG/KG

PCB-1254 (Aroclor 1254)

170

u

UG/KG

PCB-1260 (Aroclor 1260)

80



%

% Moisture

Sample 9529 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD01D /	MD No: 3AG0

Media: SEDIMENT	D No: 3AG0

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

4.0

UJ

UG/KG

alpha-BHC

4.0

U

UG/KG

beta-BHC

4.0

U

UG/KG

delta-BHC

4.0

UJ

UG/KG

gamma-BHC (Lindane)

4.0

U

UG/KG

Heptachlor

4.0

U

UG/KG

Aldrin

4.0

U

UG/KG

Heptachlor Epoxide

4.0

U

UG/KG

Endosulfan I (alpha)

7.9

U

UG/KG

Dieldrin

7.9

U

UG/KG

4,4'-DDE (p,p'-DDE)

7.9

U

UG/KG

Endrin

7.9

U

UG/KG

Endosulfan II (beta)

7.9

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

7.9

U

UG/KG

Endosulfan Sulfate

7.9

U

UG/KG

4,4'-DDT (p, p'-DDT)

40

U

UG/KG

Methoxychlor

7.9

U

UG/KG

Endrin Ketone

7.9

U

UG/KG

Endrin Aldehyde

4.0

U

UG/KG

alpha-Chlordane /2

4.0

U

UG/KG

gamma-Chlordane /2

400

U

UG/KG

Toxaphene

79

U

UG/KG

PCB-1016 (Aroclor 1016)

160

U

UG/KG

PCB-1221 (Aroclor 1221)

79

U

UG/KG

PCB-1232 (Aroclor 1232)

79

U

UG/KG

PCB-1242 (Aroclor 1242)

79

U

UG/KG

PCB-1248 (Aroclor 1248)

79

u

UG/KG

PCB-1254 (Aroclor 1254)

79

u

UG/KG

PCB-1260 (Aroclor 1260)

58



%

% Moisture

Sample 9530 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD02 /	MD No: 3AG1

Media: SEDIMENT	D No: 3AG1

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.0

UJ

UG/KG

alpha-BHC

2.0

U

UG/KG

beta-BHC

2.0

U

UG/KG

delta-BHC

2.0

UJ

UG/KG

gamma-BHC (Lindane)

2.0

U

UG/KG

Heptachlor

2.0

U

UG/KG

Aldrin

2.0

U

UG/KG

Heptachlor Epoxide

2.0

U

UG/KG

Endosulfan I (alpha)

4.0

U

UG/KG

Dieldrin

4.0

U

UG/KG

4,4'-DDE (p,p'-DDE)

4.0

U

UG/KG

Endrin

4.0

U

UG/KG

Endosulfan II (beta)

4.0

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.0

U

UG/KG

Endosulfan Sulfate

4.0

U

UG/KG

4,4'-DDT (p, p'-DDT)

20

U

UG/KG

Methoxychlor

4.0

U

UG/KG

Endrin Ketone

4.0

U

UG/KG

Endrin Aldehyde

2.0

U

UG/KG

alpha-Chlordane /2

2.0

U

UG/KG

gamma-Chlordane /2

200

U

UG/KG

Toxaphene

40

U

UG/KG

PCB-1016 (Aroclor 1016)

81

u

UG/KG

PCB-1221 (Aroclor 1221)

40

u

UG/KG

PCB-1232 (Aroclor 1232)

40

u

UG/KG

PCB-1242 (Aroclor 1242)

40

u

UG/KG

PCB-1248 (Aroclor 1248)

40

u

UG/KG

PCB-1254 (Aroclor 1254)

40

u

UG/KG

PCB-1260 (Aroclor 1260)

17



%

% Moisture

Sample 9531 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD03 /	MD No: 3AG2

Media: SEDIMENT	D No: 3AG2

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.9

UJ

UG/KG

alpha-BHC

1.9

U

UG/KG

beta-BHC

1.9

U

UG/KG

delta-BHC

1.9

UJ

UG/KG

gamma-BHC (Lindane)

1.9

U

UG/KG

Heptachlor

1.9

U

UG/KG

Aldrin

2.5

U

UG/KG

Heptachlor Epoxide

1.9

U

UG/KG

Endosulfan I (alpha)

3.8

U

UG/KG

Dieldrin

3.8

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.8

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

3.8

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

3.8

U

UG/KG

4,4'-DDT (p, p'-DDT)

19

U

UG/KG

Methoxychlor

3.8

U

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

1.9

U

UG/KG

alpha-Chlordane 12

0.86

J

UG/KG

gamma-Chlordane 12

190

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

76

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

38

U

UG/KG

PCB-1260 (Aroclor 1260)

12



%

% Moisture

Sample 9532 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF04 /	MD No: 3AG3

Media: SURFACE SOIL	D No: 3AG3

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.0

UJ

UG/KG

alpha-BHC

2.0

U

UG/KG

beta-BHC

2.0

U

UG/KG

delta-BHC

2.0

UJ

UG/KG

gamma-BHC (Lindane)

2.0

U

UG/KG

Heptachlor

2.0

U

UG/KG

Aldrin

2.0

U

UG/KG

Heptachlor Epoxide

2.0

U

UG/KG

Endosulfan I (alpha)

3.8

U

UG/KG

Dieldrin

3.8

U

UG/KG

4,4'-DDE (p,p'-DDE)

3.8

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

3.8

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

3.8

U

UG/KG

4,4'-DDT (p, p'-DDT)

20

U

UG/KG

Methoxychlor

3.8

U

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

2.0

U

UG/KG

alpha-Chlordane /2

2.0

U

UG/KG

gamma-Chlordane /2

200

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

77

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

38

u

UG/KG

PCB-1260 (Aroclor 1260)

13



%

% Moisture

Sample 9533 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF05 /	MD No: 3AG4

Media: SURFACE SOIL	D No: 3AG4

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.0

UJ

UG/KG

alpha-BHC

2.0

U

UG/KG

beta-BHC

2.0

U

UG/KG

delta-BHC

2.0

UJ

UG/KG

gamma-BHC (Lindane)

2.0

U

UG/KG

Heptachlor

2.0

U

UG/KG

Aldrin

2.0

U

UG/KG

Heptachlor Epoxide

2.0

U

UG/KG

Endosulfan I (alpha)

3.8

U

UG/KG

Dieldrin

3.8

U

UG/KG

4,4'-DDE (p,p'-DDE)

3.8

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

3.8

U

UG/KG

4,4'-DDD (p,p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

3.8

U

UG/KG

4,4'-DDT (p, p'-DDT)

20

U

UG/KG

Methoxychlor

3.8

U

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

2.0

U

UG/KG

alpha-Chlordane /2

2.0

U

UG/KG

gamma-Chlordane /2

200

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

77

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

38

u

UG/KG

PCB-1260 (Aroclor 1260)

13



%

% Moisture

Sample 9534 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF05S /	MD No: 3AG5

Media: SURFACE SOIL	D No: 3AG5

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.0

UJ

UG/KG

alpha-BHC

2.0

U

UG/KG

beta-BHC

2.0

U

UG/KG

delta-BHC

2.0

UJ

UG/KG

gamma-BHC (Lindane)

2.0

U

UG/KG

Heptachlor

2.0

U

UG/KG

Aldrin

2.0

U

UG/KG

Heptachlor Epoxide

2.0

U

UG/KG

Endosulfan I (alpha)

3.8

U

UG/KG

Dieldrin

3.8

U

UG/KG

4,4'-DDE (p,p'-DDE)

3.8

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

3.8

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

3.8

U

UG/KG

4,4'-DDT (p, p'-DDT)

20

U

UG/KG

Methoxychlor

3.8

U

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

2.0

U

UG/KG

alpha-Chlordane /2

2.0

U

UG/KG

gamma-Chlordane /2

200

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

78

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

21

J

UG/KG

PCB-1260 (Aroclor 1260)

14



%

% Moisture

Sample 9535 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD02 /	MD No: 3AG7

Media: SEDIMENT	D No: 3AG7

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.1

UJ

UG/KG

alpha-BHC

2.1

U

UG/KG

beta-BHC

2.1

U

UG/KG

delta-BHC

2.1

UJ

UG/KG

gamma-BHC (Lindane)

2.1

U

UG/KG

Heptachlor

2.1

U

UG/KG

Aldrin

2.1

U

UG/KG

Heptachlor Epoxide

2.1

U

UG/KG

Endosulfan I (alpha)

4.1

U

UG/KG

Dieldrin

4.1

U

UG/KG

4,4'-DDE (p,p'-DDE)

4.1

U

UG/KG

Endrin

4.1

U

UG/KG

Endosulfan II (beta)

4.1

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.1

U

UG/KG

Endosulfan Sulfate

4.1

U

UG/KG

4,4'-DDT (p, p'-DDT)

21

U

UG/KG

Methoxychlor

2.0

NJ

UG/KG

Endrin Ketone

4.1

U

UG/KG

Endrin Aldehyde

2.1

U

UG/KG

alpha-Chlordane /2

2.1

U

UG/KG

gamma-Chlordane /2

210

U

UG/KG

Toxaphene

41

U

UG/KG

PCB-1016 (Aroclor 1016)

83

U

UG/KG

PCB-1221 (Aroclor 1221)

41

U

UG/KG

PCB-1232 (Aroclor 1232)

41

U

UG/KG

PCB-1242 (Aroclor 1242)

41

U

UG/KG

PCB-1248 (Aroclor 1248)

41

U

UG/KG

PCB-1254 (Aroclor 1254)

41

U

UG/KG

PCB-1260 (Aroclor 1260)

19



%

% Moisture

Sample 9536 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD02D /	MD No: 3AG8

Media: SEDIMENT	D No: 3AG8

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.8

UJ

UG/KG

alpha-BHC

1.8

U

UG/KG

beta-BHC

1.8

U

UG/KG

delta-BHC

1.8

UJ

UG/KG

gamma-BHC (Lindane)

1.8

U

UG/KG

Heptachlor

1.8

U

UG/KG

Aldrin

1.8

U

UG/KG

Heptachlor Epoxide

1.8

U

UG/KG

Endosulfan I (alpha)

3.5

U

UG/KG

Dieldrin

3.5

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.5

U

UG/KG

Endrin

3.5

U

UG/KG

Endosulfan II (beta)

3.5

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.5

U

UG/KG

Endosulfan Sulfate

1.4

J

UG/KG

4,4'-DDT (p, p'-DDT)

8.0

NJ

UG/KG

Methoxychlor

3.5

U

UG/KG

Endrin Ketone

3.5

U

UG/KG

Endrin Aldehyde

1.7

NJ

UG/KG

alpha-Chlordane /2

1.8

U

UG/KG

gamma-Chlordane /2

180

U

UG/KG

Toxaphene

35

U

UG/KG

PCB-1016 (Aroclor 1016)

71

U

UG/KG

PCB-1221 (Aroclor 1221)

35

U

UG/KG

PCB-1232 (Aroclor 1232)

35

U

UG/KG

PCB-1242 (Aroclor 1242)

35

U

UG/KG

PCB-1248 (Aroclor 1248)

35

U

UG/KG

PCB-1254 (Aroclor 1254)

35

U

UG/KG

PCB-1260 (Aroclor 1260)

6



%

% Moisture

Sample 9537 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD01 /	MD No: 3AG9

Media: SEDIMENT	D No: 3AG9

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.0

UJ

UG/KG

alpha-BHC

2.0

U

UG/KG

beta-BHC

2.0

U

UG/KG

delta-BHC

2.0

UJ

UG/KG

gamma-BHC (Lindane)

2.0

U

UG/KG

Heptachlor

2.0

U

UG/KG

Aldrin

8.3

U

UG/KG

Heptachlor Epoxide

2.0

U

UG/KG

Endosulfan I (alpha)

9.7



UG/KG

Dieldrin

19

N

UG/KG

4,4'-DDE (p,p'-DDE)

3.9

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

3.8

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

12

N

UG/KG

4,4'-DDT (p, p'-DDT)

20

U

UG/KG

Methoxychlor

2.7

NJ

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

2.0

U

UG/KG

alpha-Chlordane /2

5.8



UG/KG

gamma-Chlordane /2

200

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

78

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

38

U

UG/KG

PCB-1260 (Aroclor 1260)

14



%

% Moisture

Sample 9538 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD03 /	MD No: 3AH0

Media: SEDIMENT	D No: 3AH0

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.7

UJ

UG/KG

alpha-BHC

2.7

U

UG/KG

beta-BHC

2.7

U

UG/KG

delta-BHC

2.7

UJ

UG/KG

gamma-BHC (Lindane)

2.7

U

UG/KG

Heptachlor

2.7

U

UG/KG

Aldrin

2.7

U

UG/KG

Heptachlor Epoxide

2.7

U

UG/KG

Endosulfan I (alpha)

5.2

U

UG/KG

Dieldrin

5.2

U

UG/KG

4,4'-DDE (p,p'-DDE)

5.2

U

UG/KG

Endrin

5.2

U

UG/KG

Endosulfan II (beta)

5.2

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

5.2

U

UG/KG

Endosulfan Sulfate

5.2

U

UG/KG

4,4'-DDT (p, p'-DDT)

27

U

UG/KG

Methoxychlor

5.2

U

UG/KG

Endrin Ketone

5.2

U

UG/KG

Endrin Aldehyde

2.7

U

UG/KG

alpha-Chlordane /2

2.7

U

UG/KG

gamma-Chlordane /2

270

U

UG/KG

Toxaphene

52

U

UG/KG

PCB-1016 (Aroclor 1016)

100

U

UG/KG

PCB-1221 (Aroclor 1221)

52

U

UG/KG

PCB-1232 (Aroclor 1232)

52

U

UG/KG

PCB-1242 (Aroclor 1242)

52

U

UG/KG

PCB-1248 (Aroclor 1248)

52

U

UG/KG

PCB-1254 (Aroclor 1254)

52

u

UG/KG

PCB-1260 (Aroclor 1260)

36



%

% Moisture

Sample 9539 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF01 /	MD No: 3AH1

Media: SURFACE SOIL	D No: 3AH1

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.7

UJ

UG/KG

alpha-BHC

2.7

U

UG/KG

beta-BHC

2.7

U

UG/KG

delta-BHC

2.7

UJ

UG/KG

gamma-BHC (Lindane)

2.7

U

UG/KG

Heptachlor

2.7

U

UG/KG

Aldrin

2.7

U

UG/KG

Heptachlor Epoxide

2.7

U

UG/KG

Endosulfan I (alpha)

1.3

J

UG/KG

Dieldrin

1.1

NJ

UG/KG

4,4'-DDE (p,p'-DDE)

5.2

U

UG/KG

Endrin

5.2

U

UG/KG

Endosulfan II (beta)

5.2

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

1.2

J

UG/KG

Endosulfan Sulfate

5.2

U

UG/KG

4,4'-DDT (p, p'-DDT)

27

U

UG/KG

Methoxychlor

5.2

U

UG/KG

Endrin Ketone

5.2

U

UG/KG

Endrin Aldehyde

3.0

U

UG/KG

alpha-Chlordane /2

3.5

N

UG/KG

gamma-Chlordane /2

270

U

UG/KG

Toxaphene

52

U

UG/KG

PCB-1016 (Aroclor 1016)

100

U

UG/KG

PCB-1221 (Aroclor 1221)

52

U

UG/KG

PCB-1232 (Aroclor 1232)

52

U

UG/KG

PCB-1242 (Aroclor 1242)

52

U

UG/KG

PCB-1248 (Aroclor 1248)

52

U

UG/KG

PCB-1254 (Aroclor 1254)

52

U

UG/KG

PCB-1260 (Aroclor 1260)

36



%

% Moisture

Sample 9540 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF01S /	MD No: 3AH2

Media: SURFACE SOIL	D No: 3AH2

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.9

UJ

UG/KG

alpha-BHC

1.9

U

UG/KG

beta-BHC

1.9

U

UG/KG

delta-BHC

1.9

UJ

UG/KG

gamma-BHC (Lindane)

1.9

U

UG/KG

Heptachlor

1.9

U

UG/KG

Aldrin

5.0

U

UG/KG

Heptachlor Epoxide

1.9

U

UG/KG

Endosulfan I (alpha)

7.2



UG/KG

Dieldrin

6.3



UG/KG

4,4'-DDE (p.p'-DDE)

3.6

U

UG/KG

Endrin

3.6

U

UG/KG

Endosulfan II (beta)

3.6

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.6

U

UG/KG

Endosulfan Sulfate

6.2

N

UG/KG

4,4'-DDT (p, p'-DDT)

19

U

UG/KG

Methoxychlor

3.6

U

UG/KG

Endrin Ketone

3.6

U

UG/KG

Endrin Aldehyde

17

U

UG/KG

alpha-Chlordane 12

11

N

UG/KG

gamma-Chlordane 12

190

U

UG/KG

Toxaphene

36

U

UG/KG

PCB-1016 (Aroclor 1016)

74

U

UG/KG

PCB-1221 (Aroclor 1221)

36

U

UG/KG

PCB-1232 (Aroclor 1232)

36

U

UG/KG

PCB-1242 (Aroclor 1242)

36

U

UG/KG

PCB-1248 (Aroclor 1248)

36

U

UG/KG

PCB-1254 (Aroclor 1254)

36

U

UG/KG

PCB-1260 (Aroclor 1260)

9



%

% Moisture

Sample 9541 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF02 /	MD No: 3AH3

Media: SURFACE SOIL	D No: 3AH3

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

2.1

UJ

UG/KG

alpha-BHC

2.1

U

UG/KG

beta-BHC

2.1

U

UG/KG

delta-BHC

2.1

UJ

UG/KG

gamma-BHC (Lindane)

2.1

U

UG/KG

Heptachlor

0.91

NJ

UG/KG

Aldrin

2.9

U

UG/KG

Heptachlor Epoxide

2.1

U

UG/KG

Endosulfan I (alpha)

9.4



UG/KG

Dieldrin

5.6



UG/KG

4,4'-DDE (p,p'-DDE)

4.0

U

UG/KG

Endrin

4.0

U

UG/KG

Endosulfan II (beta)

4.0

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.0

U

UG/KG

Endosulfan Sulfate

9.9



UG/KG

4,4'-DDT (p, p'-DDT)

21

U

UG/KG

Methoxychlor

4.0

U

UG/KG

Endrin Ketone

4.0

U

UG/KG

Endrin Aldehyde

18

U

UG/KG

alpha-Chlordane /2

19

N

UG/KG

gamma-Chlordane /2

210

U

UG/KG

Toxaphene

40

U

UG/KG

PCB-1016 (Aroclor 1016)

82

U

UG/KG

PCB-1221 (Aroclor 1221)

40

U

UG/KG

PCB-1232 (Aroclor 1232)

40

U

UG/KG

PCB-1242 (Aroclor 1242)

40

U

UG/KG

PCB-1248 (Aroclor 1248)

40

U

UG/KG

PCB-1254 (Aroclor 1254)

40

U

UG/KG

PCB-1260 (Aroclor 1260)

18



%

% Moisture

Sample 9542 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF03 /	MD No: 3AH4

Media: SURFACE SOIL	D No: 3AH4

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.1

UJ

UG/KG

alpha-BHC

3.1

U

UG/KG

beta-BHC

3.1

U

UG/KG

delta-BHC

3.1

UJ

UG/KG

gamma-BHC (Lindane)

3.1

U

UG/KG

Heptachlor

15

N

UG/KG

Aldrin

3.1

U

UG/KG

Heptachlor Epoxide

3.1

U

UG/KG

Endosulfan I (alpha)

12



UG/KG

Dieldrin

6.5



UG/KG

4,4'-DDE (p,p'-DDE)

6.0

U

UG/KG

Endrin

6.0

U

UG/KG

Endosulfan II (beta)

3.3

NJ

UG/KG

4,4'-DDD (p,p'-DDD)

6.0

U

UG/KG

Endosulfan Sulfate

12



UG/KG

4,4'-DDT (p, p'-DDT)

31

U

UG/KG

Methoxychlor

6.0

U

UG/KG

Endrin Ketone

6.0

U

UG/KG

Endrin Aldehyde

24

N

UG/KG

alpha-Chlordane /2

23

N

UG/KG

gamma-Chlordane /2

310

U

UG/KG

Toxaphene

60

U

UG/KG

PCB-1016 (Aroclor 1016)

120

U

UG/KG

PCB-1221 (Aroclor 1221)

60

U

UG/KG

PCB-1232 (Aroclor 1232)

60

U

UG/KG

PCB-1242 (Aroclor 1242)

60

U

UG/KG

PCB-1248 (Aroclor 1248)

60

U

UG/KG

PCB-1254 (Aroclor 1254)

60

U

UG/KG

PCB-1260 (Aroclor 1260)

45



%

% Moisture

Sample 9543 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSD04 /	MD No: 3AH5

Media: SEDIMENT	D No: 3AH5

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.5

UJ

UG/KG

alpha-BHC

2.5

U

UG/KG

beta-BHC

2.5

U

UG/KG

delta-BHC

2.5

UJ

UG/KG

gamma-BHC (Lindane)

2.5

U

UG/KG

Heptachlor

2.5

U

UG/KG

Aldrin

2.5

U

UG/KG

Heptachlor Epoxide

2.5

U

UG/KG

Endosulfan I (alpha)

7.1



UG/KG

Dieldrin

4.9

N

UG/KG

4,4'-DDE (p,p'-DDE)

4.9

U

UG/KG

Endrin

4.9

U

UG/KG

Endosulfan II (beta)

2.0

J

UG/KG

4,4'-DDD (p,p'-DDD)

4.9

U

UG/KG

Endosulfan Sulfate

3.9

J

UG/KG

4,4'-DDT (p, p'-DDT)

6.8

J

UG/KG

Methoxychlor

2.3

U

UG/KG

Endrin Ketone

4.9

U

UG/KG

Endrin Aldehyde

8.4

N

UG/KG

alpha-Chlordane /2

6.6

U

UG/KG

gamma-Chlordane /2

250

U

UG/KG

Toxaphene

49

U

UG/KG

PCB-1016 (Aroclor 1016)

99

U

UG/KG

PCB-1221 (Aroclor 1221)

49

U

UG/KG

PCB-1232 (Aroclor 1232)

49

U

UG/KG

PCB-1242 (Aroclor 1242)

49

U

UG/KG

PCB-1248 (Aroclor 1248)

49

U

UG/KG

PCB-1254 (Aroclor 1254)

49

U

UG/KG

PCB-1260 (Aroclor 1260)

32



%

% Moisture

Sample 9544 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSD04D /	MD No: 3AH6

Media: SEDIMENT	D No: 3AH6

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.4

UJ

UG/KG

alpha-BHC

3.4

U

UG/KG

beta-BHC

3.4

U

UG/KG

delta-BHC

3.4

UJ

UG/KG

gamma-BHC (Lindane)

3.4

U

UG/KG

Heptachlor

3.4

U

UG/KG

Aldrin

3.4

U

UG/KG

Heptachlor Epoxide

3.4

U

UG/KG

Endosulfan I (alpha)

4.6

NJ

UG/KG

Dieldrin

2.0

J

UG/KG

4,4'-DDE (p,p'-DDE)

6.6

U

UG/KG

Endrin

6.6

U

UG/KG

Endosulfan II (beta)

6.6

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

6.6

U

UG/KG

Endosulfan Sulfate

2.7

J

UG/KG

4,4'-DDT (p, p'-DDT)

34

U

UG/KG

Methoxychlor

6.6

U

UG/KG

Endrin Ketone

6.6

U

UG/KG

Endrin Aldehyde

6.5

U

UG/KG

alpha-Chlordane /2

8.4



UG/KG

gamma-Chlordane /2

340

U

UG/KG

Toxaphene

66

U

UG/KG

PCB-1016 (Aroclor 1016)

130

U

UG/KG

PCB-1221 (Aroclor 1221)

66

U

UG/KG

PCB-1232 (Aroclor 1232)

66

U

UG/KG

PCB-1242 (Aroclor 1242)

66

U

UG/KG

PCB-1248 (Aroclor 1248)

66

U

UG/KG

PCB-1254 (Aroclor 1254)

66

U

UG/KG

PCB-1260 (Aroclor 1260)

50



%

% Moisture

Sample 9545 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSD05 /	MD No: 3AH7

Media: SEDIMENT	D No: 3AH7

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.4

UJ

UG/KG

alpha-BHC

3.4

U

UG/KG

beta-BHC

3.4

U

UG/KG

delta-BHC

3.4

UJ

UG/KG

gamma-BHC (Lindane)

3.4

U

UG/KG

Heptachlor

3.4

U

UG/KG

Aldrin

3.4

U

UG/KG

Heptachlor Epoxide

3.4

U

UG/KG

Endosulfan I (alpha)

6.6

U

UG/KG

Dieldrin

6.6

U

UG/KG

4,4'-DDE (p,p'-DDE)

1.8

NJ

UG/KG

Endrin

6.6

U

UG/KG

Endosulfan II (beta)

6.6

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

6.6

U

UG/KG

Endosulfan Sulfate

6.6

U

UG/KG

4,4'-DDT (p, p'-DDT)

34

U

UG/KG

Methoxychlor

6.6

U

UG/KG

Endrin Ketone

6.6

U

UG/KG

Endrin Aldehyde

4.7



UG/KG

alpha-Chlordane /2

3.4

U

UG/KG

gamma-Chlordane /2

340

U

UG/KG

Toxaphene

66

U

UG/KG

PCB-1016 (Aroclor 1016)

130

U

UG/KG

PCB-1221 (Aroclor 1221)

66

U

UG/KG

PCB-1232 (Aroclor 1232)

66

U

UG/KG

PCB-1242 (Aroclor 1242)

66

U

UG/KG

PCB-1248 (Aroclor 1248)

66

U

UG/KG

PCB-1254 (Aroclor 1254)

66

U

UG/KG

PCB-1260 (Aroclor 1260)

50



%

% Moisture

Sample 9546 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD01 /	MD No: 3AH8

Media: SEDIMENT	D No: 3AH8

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

3.4

UJ

UG/KG

alpha-BHC

3.4

U

UG/KG

beta-BHC

3.4

U

UG/KG

delta-BHC

3.4

UJ

UG/KG

gamma-BHC (Lindane)

3.4

U

UG/KG

Heptachlor

3.4

U

UG/KG

Aldrin

3.4

U

UG/KG

Heptachlor Epoxide

1.1

J

UG/KG

Endosulfan I (alpha)

6.6

U

UG/KG

Dieldrin

6.6

U

UG/KG

4,4'-DDE (p,p'-DDE)

6.6

U

UG/KG

Endrin

6.6

U

UG/KG

Endosulfan II (beta)

6.6

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

6.6

U

UG/KG

Endosulfan Sulfate

6.6

U

UG/KG

4,4'-DDT (p, p'-DDT)

34

U

UG/KG

Methoxychlor

6.6

U

UG/KG

Endrin Ketone

6.6

U

UG/KG

Endrin Aldehyde

4.0

N

UG/KG

alpha-Chlordane /2

3.4

U

UG/KG

gamma-Chlordane /2

340

U

UG/KG

Toxaphene

66

U

UG/KG

PCB-1016 (Aroclor 1016)

130

U

UG/KG

PCB-1221 (Aroclor 1221)

66

U

UG/KG

PCB-1232 (Aroclor 1232)

66

U

UG/KG

PCB-1242 (Aroclor 1242)

66

U

UG/KG

PCB-1248 (Aroclor 1248)

66

U

UG/KG

PCB-1254 (Aroclor 1254)

66

U

UG/KG

PCB-1260 (Aroclor 1260)

50



%

% Moisture

Sample 9547 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD01D /	MD No: 3AH9

Media: SEDIMENT	D No: 3AH9

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

2.2

UJ

UG/KG

alpha-BHC

2.2

U

UG/KG

beta-BHC

2.2

U

UG/KG

delta-BHC

2.2

UJ

UG/KG

gamma-BHC (Lindane)

2.2

U

UG/KG

Heptachlor

2.2

U

UG/KG

Aldrin

2.2

U

UG/KG

Heptachlor Epoxide

2.2

U

UG/KG

Endosulfan I (alpha)

4.3

U

UG/KG

Dieldrin

4.3

U

UG/KG

4,4'-DDE (p,p'-DDE)

1.0

J

UG/KG

Endrin

4.3

U

UG/KG

Endosulfan II (beta)

4.3

UJ

UG/KG

4,4'-DDD (p,p'-DDD)

4.3

U

UG/KG

Endosulfan Sulfate

4.3

U

UG/KG

4,4'-DDT (p, p'-DDT)

22

U

UG/KG

Methoxychlor

4.3

U

UG/KG

Endrin Ketone

4.3

U

UG/KG

Endrin Aldehyde

2.2

U

UG/KG

alpha-Chlordane /2

2.2

U

UG/KG

gamma-Chlordane /2

220

U

UG/KG

Toxaphene

43

U

UG/KG

PCB-1016 (Aroclor 1016)

88

U

UG/KG

PCB-1221 (Aroclor 1221)

43

U

UG/KG

PCB-1232 (Aroclor 1232)

43

U

UG/KG

PCB-1242 (Aroclor 1242)

43

U

UG/KG

PCB-1248 (Aroclor 1248)

43

U

UG/KG

PCB-1254 (Aroclor 1254)

43

U

UG/KG

PCB-1260 (Aroclor 1260)

24



%

% Moisture

Sample 9548 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD02 /	MD No: 3AJ0

Media: SEDIMENT	D No: 3AJ0

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 12:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

1.9

UJ

UG/KG

alpha-BHC

1.9

U

UG/KG

beta-BHC

1.9

U

UG/KG

delta-BHC

1.9

UJ

UG/KG

gamma-BHC (Lindane)

1.9

U

UG/KG

Heptachlor

1.9

U

UG/KG

Aldrin

13

U

UG/KG

Heptachlor Epoxide

1.9

U

UG/KG

Endosulfan I (alpha)

0.86

NJ

UG/KG

Dieldrin

3.7

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.7

U

UG/KG

Endrin

3.7

U

UG/KG

Endosulfan II (beta)

3.7

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.7

U

UG/KG

Endosulfan Sulfate

3.7

U

UG/KG

4,4'-DDT (p, p'-DDT)

19

U

UG/KG

Methoxychlor

1.7

NJ

UG/KG

Endrin Ketone

3.7

U

UG/KG

Endrin Aldehyde

1.9

U

UG/KG

alpha-Chlordane 12

1.9

U

UG/KG

gamma-Chlordane 12

190

U

UG/KG

Toxaphene

37

U

UG/KG

PCB-1016 (Aroclor 1016)

74

U

UG/KG

PCB-1221 (Aroclor 1221)

37

U

UG/KG

PCB-1232 (Aroclor 1232)

37

U

UG/KG

PCB-1242 (Aroclor 1242)

37

U

UG/KG

PCB-1248 (Aroclor 1248)

37

U

UG/KG

PCB-1254 (Aroclor 1254)

37

U

UG/KG

PCB-1260 (Aroclor 1260)

10



%

% Moisture

Sample 9549 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF05 /	MD No: 3AJ1

Media: SURFACE SOIL	D No: 3AJ1

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS UNITS ANALYTE

1.9

UJ

UG/KG

alpha-BHC

1.9

U

UG/KG

beta-BHC

1.9

U

UG/KG

delta-BHC

1.9

UJ

UG/KG

gamma-BHC (Lindane)

1.9

U

UG/KG

Heptachlor

1.9

U

UG/KG

Aldrin

1.9

U

UG/KG

Heptachlor Epoxide

1.9

U

UG/KG

Endosulfan I (alpha)

1.0

J

UG/KG

Dieldrin

3.8

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.8

U

UG/KG

Endrin

3.8

U

UG/KG

Endosulfan II (beta)

0.80

J

UG/KG

4,4'-DDD (p.p'-DDD)

3.8

U

UG/KG

Endosulfan Sulfate

3.8

U

UG/KG

4,4'-DDT (p, p'-DDT)

19

U

UG/KG

Methoxychlor

3.8

U

UG/KG

Endrin Ketone

3.8

U

UG/KG

Endrin Aldehyde

1.1

NJ

UG/KG

alpha-Chlordane 12

1.9

U

UG/KG

gamma-Chlordane 12

190

U

UG/KG

Toxaphene

38

U

UG/KG

PCB-1016 (Aroclor 1016)

76

U

UG/KG

PCB-1221 (Aroclor 1221)

38

U

UG/KG

PCB-1232 (Aroclor 1232)

38

U

UG/KG

PCB-1242 (Aroclor 1242)

38

U

UG/KG

PCB-1248 (Aroclor 1248)

38

U

UG/KG

PCB-1254 (Aroclor 1254)

38

U

UG/KG

PCB-1260 (Aroclor 1260)

12



%

% Moisture

Sample 9550 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF04 /	MD No: 3AJ2

Media: SURFACE SOIL	D No: 3AJ2

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

1.7

UJ

UG/KG

alpha-BHC

1.7

U

UG/KG

beta-BHC

1.7

U

UG/KG

delta-BHC

1.7

UJ

UG/KG

gamma-BHC (Lindane)

1.7

U

UG/KG

Heptachlor

1.7

U

UG/KG

Aldrin

1.7

U

UG/KG

Heptachlor Epoxide

1.7

U

UG/KG

Endosulfan I (alpha)

3.3

U

UG/KG

Dieldrin

3.3

U

UG/KG

4,4'-DDE (p.p'-DDE)

3.3

U

UG/KG

Endrin

3.3

U

UG/KG

Endosulfan II (beta)

3.3

UJ

UG/KG

4,4'-DDD (p.p'-DDD)

3.3

U

UG/KG

Endosulfan Sulfate

3.3

U

UG/KG

4,4'-DDT (p, p'-DDT)

5.7

J

UG/KG

Methoxychlor

3.3

U

UG/KG

Endrin Ketone

3.3

U

UG/KG

Endrin Aldehyde

1.7

U

UG/KG

alpha-Chlordane /2

1.7

U

UG/KG

gamma-Chlordane /2

170

U

UG/KG

Toxaphene

33

U

UG/KG

PCB-1016 (Aroclor 1016)

67

U

UG/KG

PCB-1221 (Aroclor 1221)

33

U

UG/KG

PCB-1232 (Aroclor 1232)

33

U

UG/KG

PCB-1242 (Aroclor 1242)

33

U

UG/KG

PCB-1248 (Aroclor 1248)

33

U

UG/KG

PCB-1254 (Aroclor 1254)

33

U

UG/KG

PCB-1260 (Aroclor 1260)

14



%

% Moisture

Sample 9551 FY 2005 Project: 05-0928
Pesticides & Aroclors Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF03 /	MD No: 3AJ3

Media: SURFACE SOIL	D No: 3AJ3

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 14:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9518 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF08/	MD No: 3AJ4	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ4	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

16

U

UG/KG

Dichlorodifluoromethane

16

U

UG/KG

Dibromochloromethane

16

U

UG/KG

Chloromethane

16

U

UG/KG

1,2-Dibromoethane (EDB)

16

U

UG/KG

Vinyl Chloride

16

U

UG/KG

Chlorobenzene

16

U

UG/KG

Bromomethane

16

U

UG/KG

Ethyl Benzene

16

UJ

UG/KG

Chloroethane

16

U

UG/KG

Total Xylenes

16

U

UG/KG

Trichlorofluoromethane (Freon11)

16

U

UG/KG

Styrene

16

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

16

U

UG/KG

Bromoform

16

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

16

U

UG/KG

Isopropylbenzene

16

U

UG/KG

Acetone

16

U

UG/KG

1,1,2,2-Tetrachloroethane

16

U

UG/KG

Carbon Disulfide

16

U

UG/KG

1,3-Dichlorobenzene

16

U

UG/KG

Methyl Acetate

16

U

UG/KG

1,4-Dichlorobenzene

16

U

UG/KG

Methylene Chloride

16

U

UG/KG

1,2-Dichlorobenzene

16

U

UG/KG

trans-1,2-Dichloroethene

16

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

16

U

UG/KG

Methyl T-Butyl Ether (MTBE)

16

U

UG/KG

1,2,4-T richlorobenzene

16

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

16

U

UG/KG

cis-1,2-Dichloroethene

6



%

% Moisture

16

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









16

U

UG/KG

Chloroform









16

U

UG/KG

1,1,1-Trichloroethane









16

U

UG/KG

Cyclohexane









16

U

UG/KG

Carbon Tetrachloride









16

U

UG/KG

Benzene









16

U

UG/KG

1,2-Dichloroethane









16

U

UG/KG

Trichloroethene (Trichloroethylene)









16

U

UG/KG

Methylcyclohexane









16

U

UG/KG

1,2-Dichloropropane









16

U

UG/KG

Bromodichloromethane









16

U

UG/KG

cis-1,3-Dichloropropene









16

U

UG/KG

Methyl Isobutyl Ketone









16

U

UG/KG

Toluene









16

U

UG/KG

trans-1,3-Dichloropropene









16

U

UG/KG

1,1,2-Trichloroethane









16

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









16

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9519 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD07/	MD No: 3AJ5	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ5	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

24

U

UG/KG

Dichlorodifluoromethane

24

U

UG/KG

Dibromochloromethane

24

U

UG/KG

Chloromethane

24

U

UG/KG

1,2-Dibromoethane (EDB)

24

U

UG/KG

Vinyl Chloride

24

U

UG/KG

Chlorobenzene

24

U

UG/KG

Bromomethane

24

U

UG/KG

Ethyl Benzene

24

UJ

UG/KG

Chloroethane

24

U

UG/KG

Total Xylenes

24

U

UG/KG

Trichlorofluoromethane (Freon11)

24

U

UG/KG

Styrene

24

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

24

U

UG/KG

Bromoform

24

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

24

U

UG/KG

Isopropylbenzene

24

U

UG/KG

Acetone

24

U

UG/KG

1,1,2,2-Tetrachloroethane

24

U

UG/KG

Carbon Disulfide

24

U

UG/KG

1,3-Dichlorobenzene

24

U

UG/KG

Methyl Acetate

24

U

UG/KG

1,4-Dichlorobenzene

24

U

UG/KG

Methylene Chloride

24

U

UG/KG

1,2-Dichlorobenzene

24

U

UG/KG

trans-1,2-Dichloroethene

24

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

24

U

UG/KG

Methyl T-Butyl Ether (MTBE)

24

U

UG/KG

1,2,4-T richlorobenzene

24

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

24

U

UG/KG

cis-1,2-Dichloroethene

40



%

% Moisture

24

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









24

U

UG/KG

Chloroform









24

U

UG/KG

1,1,1-Trichloroethane









24

U

UG/KG

Cyclohexane









24

U

UG/KG

Carbon Tetrachloride









24

U

UG/KG

Benzene









24

U

UG/KG

1,2-Dichloroethane









24

U

UG/KG

Trichloroethene (Trichloroethylene)









24

U

UG/KG

Methylcyclohexane









24

U

UG/KG

1,2-Dichloropropane









24

U

UG/KG

Bromodichloromethane









24

U

UG/KG

cis-1,3-Dichloropropene









24

U

UG/KG

Methyl Isobutyl Ketone









24

U

UG/KG

Toluene









24

U

UG/KG

trans-1,3-Dichloropropene









24

U

UG/KG

1,1,2-Trichloroethane









24

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









24

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9520 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF02/	MD No: 3AJ6	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ6	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

13

U

UG/KG

Dichlorodifluoromethane

13

U

UG/KG

Dibromochloromethane

13

U

UG/KG

Chloromethane

13

U

UG/KG

1,2-Dibromoethane (EDB)

13

U

UG/KG

Vinyl Chloride

13

U

UG/KG

Chlorobenzene

13

U

UG/KG

Bromomethane

13

U

UG/KG

Ethyl Benzene

13

UJ

UG/KG

Chloroethane

13

U

UG/KG

Total Xylenes

13

U

UG/KG

Trichlorofluoromethane (Freon11)

13

U

UG/KG

Styrene

13

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

13

U

UG/KG

Bromoform

13

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

13

U

UG/KG

Isopropylbenzene

13

U

UG/KG

Acetone

13

U

UG/KG

1,1,2,2-Tetrachloroethane

13

U

UG/KG

Carbon Disulfide

13

U

UG/KG

1,3-Dichlorobenzene

13

U

UG/KG

Methyl Acetate

13

U

UG/KG

1,4-Dichlorobenzene

13

U

UG/KG

Methylene Chloride

13

U

UG/KG

1,2-Dichlorobenzene

13

U

UG/KG

trans-1,2-Dichloroethene

13

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

13

U

UG/KG

Methyl T-Butyl Ether (MTBE)

13

U

UG/KG

1,2,4-T richlorobenzene

13

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

13

U

UG/KG

cis-1,2-Dichloroethene

23



%

% Moisture

13

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









13

U

UG/KG

Chloroform









13

U

UG/KG

1,1,1-Trichloroethane









13

U

UG/KG

Cyclohexane









13

U

UG/KG

Carbon Tetrachloride









13

U

UG/KG

Benzene









13

U

UG/KG

1,2-Dichloroethane









13

U

UG/KG

Trichloroethene (Trichloroethylene)









13

U

UG/KG

Methylcyclohexane









13

U

UG/KG

1,2-Dichloropropane









13

U

UG/KG

Bromodichloromethane









13

U

UG/KG

cis-1,3-Dichloropropene









13

U

UG/KG

Methyl Isobutyl Ketone









13

U

UG/KG

Toluene









13

U

UG/KG

trans-1,3-Dichloropropene









13

U

UG/KG

1,1,2-Trichloroethane









13

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









13

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9521 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF02S/	MD No: 3AJ7	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ7	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

13

U

UG/KG

Dichlorodifluoromethane

13

U

UG/KG

Dibromochloromethane

13

U

UG/KG

Chloromethane

13

U

UG/KG

1,2-Dibromoethane (EDB)

13

U

UG/KG

Vinyl Chloride

13

U

UG/KG

Chlorobenzene

13

U

UG/KG

Bromomethane

13

U

UG/KG

Ethyl Benzene

13

UJ

UG/KG

Chloroethane

13

U

UG/KG

Total Xylenes

13

U

UG/KG

Trichlorofluoromethane (Freon11)

13

U

UG/KG

Styrene

13

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

13

U

UG/KG

Bromoform

13

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

13

U

UG/KG

Isopropylbenzene

13

U

UG/KG

Acetone

13

U

UG/KG

1,1,2,2-Tetrachloroethane

13

U

UG/KG

Carbon Disulfide

13

U

UG/KG

1,3-Dichlorobenzene

13

U

UG/KG

Methyl Acetate

13

U

UG/KG

1,4-Dichlorobenzene

13

U

UG/KG

Methylene Chloride

13

U

UG/KG

1,2-Dichlorobenzene

13

U

UG/KG

trans-1,2-Dichloroethene

13

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

13

U

UG/KG

Methyl T-Butyl Ether (MTBE)

13

U

UG/KG

1,2,4-T richlorobenzene

13

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

13

U

UG/KG

cis-1,2-Dichloroethene

21



%

% Moisture

13

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









13

U

UG/KG

Chloroform









13

U

UG/KG

1,1,1-Trichloroethane









13

U

UG/KG

Cyclohexane









13

U

UG/KG

Carbon Tetrachloride









13

U

UG/KG

Benzene









13

U

UG/KG

1,2-Dichloroethane









13

U

UG/KG

Trichloroethene (Trichloroethylene)









13

U

UG/KG

Methylcyclohexane









13

U

UG/KG

1,2-Dichloropropane









13

U

UG/KG

Bromodichloromethane









13

U

UG/KG

cis-1,3-Dichloropropene









13

U

UG/KG

Methyl Isobutyl Ketone









13

U

UG/KG

Toluene









13

U

UG/KG

trans-1,3-Dichloropropene









13

U

UG/KG

1,1,2-Trichloroethane









13

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









13

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9522 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSF01 /	MD No: 3AJ8	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ8	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

u

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

UJ

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

u

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

u

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

9



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 10:55
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9523 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD06/	MD No: 3AJ9	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ9	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

25

U

UG/KG

Dichlorodifluoromethane

25

U

UG/KG

Dibromochloromethane

25

U

UG/KG

Chloromethane

25

U

UG/KG

1,2-Dibromoethane (EDB)

25

U

UG/KG

Vinyl Chloride

25

U

UG/KG

Chlorobenzene

25

U

UG/KG

Bromomethane

25

U

UG/KG

Ethyl Benzene

25

UJ

UG/KG

Chloroethane

25

U

UG/KG

Total Xylenes

25

U

UG/KG

Trichlorofluoromethane (Freon11)

25

U

UG/KG

Styrene

25

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

25

U

UG/KG

Bromoform

25

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

25

U

UG/KG

Isopropylbenzene

25

U

UG/KG

Acetone

25

U

UG/KG

1,1,2,2-Tetrachloroethane

25

U

UG/KG

Carbon Disulfide

25

U

UG/KG

1,3-Dichlorobenzene

25

U

UG/KG

Methyl Acetate

25

U

UG/KG

1,4-Dichlorobenzene

25

U

UG/KG

Methylene Chloride

25

U

UG/KG

1,2-Dichlorobenzene

25

U

UG/KG

trans-1,2-Dichloroethene

25

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

25

U

UG/KG

Methyl T-Butyl Ether (MTBE)

25

U

UG/KG

1,2,4-T richlorobenzene

25

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

25

U

UG/KG

cis-1,2-Dichloroethene

51



%

% Moisture

25

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









25

U

UG/KG

Chloroform









25

U

UG/KG

1,1,1-Trichloroethane









25

U

UG/KG

Cyclohexane









25

U

UG/KG

Carbon Tetrachloride









25

U

UG/KG

Benzene









25

U

UG/KG

1,2-Dichloroethane









25

U

UG/KG

Trichloroethene (Trichloroethylene)









25

U

UG/KG

Methylcyclohexane









25

U

UG/KG

1,2-Dichloropropane









25

U

UG/KG

Bromodichloromethane









25

U

UG/KG

cis-1,3-Dichloropropene









25

U

UG/KG

Methyl Isobutyl Ketone









25

U

UG/KG

Toluene









25

U

UG/KG

trans-1,3-Dichloropropene









25

U

UG/KG

1,1,2-Trichloroethane









25

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









25

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9523 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD06/

Media: SEDIMENT

Case No: 34717
MD No: 3AJ9
D No: 3AJ9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 11:45
Ending:

RESULTS UNITS

50 NJ UG/KG

ANALYTE

DIMETHYL SULFIDE

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9524 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD05/	MD No: 3AK0	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AK0	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

67

U

UG/KG

Dichlorodifluoromethane

67

U

UG/KG

Dibromochloromethane

67

U

UG/KG

Chloromethane

67

U

UG/KG

1,2-Dibromoethane (EDB)

67

U

UG/KG

Vinyl Chloride

67

U

UG/KG

Chlorobenzene

67

U

UG/KG

Bromomethane

67

U

UG/KG

Ethyl Benzene

67

UJ

UG/KG

Chloroethane

67

U

UG/KG

Total Xylenes

67

U

UG/KG

Trichlorofluoromethane (Freon11)

67

U

UG/KG

Styrene

67

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

67

U

UG/KG

Bromoform

67

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

67

U

UG/KG

Isopropylbenzene

180



UG/KG

Acetone

67

U

UG/KG

1,1,2,2-Tetrachloroethane

67

U

UG/KG

Carbon Disulfide

67

U

UG/KG

1,3-Dichlorobenzene

67

U

UG/KG

Methyl Acetate

67

U

UG/KG

1,4-Dichlorobenzene

67

U

UG/KG

Methylene Chloride

67

U

UG/KG

1,2-Dichlorobenzene

67

U

UG/KG

trans-1,2-Dichloroethene

67

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

67

U

UG/KG

Methyl T-Butyl Ether (MTBE)

67

U

UG/KG

1,2,4-T richlorobenzene

67

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

67

U

UG/KG

cis-1,2-Dichloroethene

77



%

% Moisture

67

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









67

U

UG/KG

Chloroform









67

U

UG/KG

1,1,1-Trichloroethane









67

U

UG/KG

Cyclohexane









67

U

UG/KG

Carbon Tetrachloride









67

U

UG/KG

Benzene









67

U

UG/KG

1,2-Dichloroethane









67

U

UG/KG

Trichloroethene (Trichloroethylene)









67

U

UG/KG

Methylcyclohexane









67

U

UG/KG

1,2-Dichloropropane









67

U

UG/KG

Bromodichloromethane









67

U

UG/KG

cis-1,3-Dichloropropene









67

U

UG/KG

Methyl Isobutyl Ketone









24

J

UG/KG

Toluene









67

U

UG/KG

trans-1,3-Dichloropropene









67

U

UG/KG

1,1,2-Trichloroethane









67

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









67

U

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:35
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9524 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD05/

Media: SEDIMENT

Case No: 34717
MD No: 3AK0
D No: 3AK0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:35
Ending:

RESULTS

UNITS

ANALYTE

120 NJ

UG/KG

(1 R)-2,6,6-TRIMETHYLBICYCLO[3,1,1] HEPT-2-ENE

57 NJ

UG/KG

CAMPHENE

130 NJ

UG/KG

BENZENE, 1 -METHYL-3-(1 -METHYLETHYL)-

N

UG/KG

PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9525 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD05D/	MD No: 3AK1	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AK1	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

59

U

UG/KG

Dichlorodifluoromethane

59

U

UG/KG

Dibromochloromethane

59

U

UG/KG

Chloromethane

59

U

UG/KG

1,2-Dibromoethane (EDB)

59

U

UG/KG

Vinyl Chloride

59

U

UG/KG

Chlorobenzene

59

U

UG/KG

Bromomethane

59

U

UG/KG

Ethyl Benzene

59

UJ

UG/KG

Chloroethane

59

U

UG/KG

Total Xylenes

59

U

UG/KG

Trichlorofluoromethane (Freon11)

59

U

UG/KG

Styrene

59

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

59

U

UG/KG

Bromoform

59

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

59

U

UG/KG

Isopropylbenzene

81



UG/KG

Acetone

59

U

UG/KG

1,1,2,2-Tetrachloroethane

59

U

UG/KG

Carbon Disulfide

59

U

UG/KG

1,3-Dichlorobenzene

59

U

UG/KG

Methyl Acetate

59

U

UG/KG

1,4-Dichlorobenzene

59

U

UG/KG

Methylene Chloride

59

U

UG/KG

1,2-Dichlorobenzene

59

U

UG/KG

trans-1,2-Dichloroethene

59

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

59

U

UG/KG

Methyl T-Butyl Ether (MTBE)

59

U

UG/KG

1,2,4-T richlorobenzene

59

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

59

U

UG/KG

cis-1,2-Dichloroethene

78



%

% Moisture

59

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









59

U

UG/KG

Chloroform









59

U

UG/KG

1,1,1-Trichloroethane









59

U

UG/KG

Cyclohexane









59

U

UG/KG

Carbon Tetrachloride









59

U

UG/KG

Benzene









59

U

UG/KG

1,2-Dichloroethane









59

U

UG/KG

Trichloroethene (Trichloroethylene)









59

U

UG/KG

Methylcyclohexane









59

U

UG/KG

1,2-Dichloropropane









59

U

UG/KG

Bromodichloromethane









59

U

UG/KG

cis-1,3-Dichloropropene









59

U

UG/KG

Methyl Isobutyl Ketone









59

U

UG/KG

Toluene









59

U

UG/KG

trans-1,3-Dichloropropene









59

U

UG/KG

1,1,2-Trichloroethane









59

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









59

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9526 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD03/	MD No: 3AK2	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AK2	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

35

U

UG/KG

Dichlorodifluoromethane

35

U

UG/KG

Dibromochloromethane

35

U

UG/KG

Chloromethane

35

U

UG/KG

1,2-Dibromoethane (EDB)

35

U

UG/KG

Vinyl Chloride

35

U

UG/KG

Chlorobenzene

35

U

UG/KG

Bromomethane

35

U

UG/KG

Ethyl Benzene

35

UJ

UG/KG

Chloroethane

35

U

UG/KG

Total Xylenes

35

U

UG/KG

Trichlorofluoromethane (Freon11)

35

U

UG/KG

Styrene

35

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

35

U

UG/KG

Bromoform

35

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

35

U

UG/KG

Isopropylbenzene

35

U

UG/KG

Acetone

35

U

UG/KG

1,1,2,2-Tetrachloroethane

35

U

UG/KG

Carbon Disulfide

35

U

UG/KG

1,3-Dichlorobenzene

35

U

UG/KG

Methyl Acetate

35

U

UG/KG

1,4-Dichlorobenzene

35

U

UG/KG

Methylene Chloride

35

U

UG/KG

1,2-Dichlorobenzene

35

U

UG/KG

trans-1,2-Dichloroethene

35

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

35

U

UG/KG

Methyl T-Butyl Ether (MTBE)

35

U

UG/KG

1,2,4-T richlorobenzene

35

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

35

U

UG/KG

cis-1,2-Dichloroethene

56



%

% Moisture

35

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









35

U

UG/KG

Chloroform









35

U

UG/KG

1,1,1-Trichloroethane









35

U

UG/KG

Cyclohexane









35

U

UG/KG

Carbon Tetrachloride









35

U

UG/KG

Benzene









35

U

UG/KG

1,2-Dichloroethane









35

U

UG/KG

Trichloroethene (Trichloroethylene)









35

U

UG/KG

Methylcyclohexane









35

U

UG/KG

1,2-Dichloropropane









35

U

UG/KG

Bromodichloromethane









35

U

UG/KG

cis-1,3-Dichloropropene









35

U

UG/KG

Methyl Isobutyl Ketone









35

U

UG/KG

Toluene









35

U

UG/KG

trans-1,3-Dichloropropene









35

U

UG/KG

1,1,2-Trichloroethane









35

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









35

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9527 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: CFMSD04/	MD No: 3AK5	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AK5	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

13

U

UG/KG

Dichlorodifluoromethane

13

U

UG/KG

Dibromochloromethane

13

U

UG/KG

Chloromethane

13

U

UG/KG

1,2-Dibromoethane (EDB)

13

U

UG/KG

Vinyl Chloride

13

U

UG/KG

Chlorobenzene

13

U

UG/KG

Bromomethane

13

U

UG/KG

Ethyl Benzene

13

UJ

UG/KG

Chloroethane

13

U

UG/KG

Total Xylenes

13

U

UG/KG

Trichlorofluoromethane (Freon11)

13

U

UG/KG

Styrene

13

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

13

U

UG/KG

Bromoform

13

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

13

U

UG/KG

Isopropylbenzene

13

U

UG/KG

Acetone

13

U

UG/KG

1,1,2,2-Tetrachloroethane

13

U

UG/KG

Carbon Disulfide

13

U

UG/KG

1,3-Dichlorobenzene

13

U

UG/KG

Methyl Acetate

13

U

UG/KG

1,4-Dichlorobenzene

13

U

UG/KG

Methylene Chloride

13

U

UG/KG

1,2-Dichlorobenzene

13

U

UG/KG

trans-1,2-Dichloroethene

13

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

13

U

UG/KG

Methyl T-Butyl Ether (MTBE)

13

U

UG/KG

1,2,4-T richlorobenzene

13

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

13

U

UG/KG

cis-1,2-Dichloroethene

25



%

% Moisture

13

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









13

U

UG/KG

Chloroform









13

U

UG/KG

1,1,1-Trichloroethane









13

U

UG/KG

Cyclohexane









13

U

UG/KG

Carbon Tetrachloride









13

U

UG/KG

Benzene









13

U

UG/KG

1,2-Dichloroethane









13

U

UG/KG

Trichloroethene (Trichloroethylene)









13

U

UG/KG

Methylcyclohexane









13

U

UG/KG

1,2-Dichloropropane









13

U

UG/KG

Bromodichloromethane









13

U

UG/KG

cis-1,3-Dichloropropene









13

U

UG/KG

Methyl Isobutyl Ketone









13

U

UG/KG

Toluene









13

U

UG/KG

trans-1,3-Dichloropropene









13

U

UG/KG

1,1,2-Trichloroethane









13

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









13

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9527 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: CFMSD04/

Media: SEDIMENT

Case No: 34717
MD No: 3AK5
D No: 3AK5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/06/2005 13:45
Ending:

RESULTS

21 J

UNITS

UG/KG

ANALYTE

1 UNKNOWN

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9528 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AF9
D No: 3AF9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

96

U

UG/KG

Dichlorodifluoromethane

96

U

UG/KG

Dibromochloromethane

96

U

UG/KG

Chloromethane

96

U

UG/KG

1,2-Dibromoethane (EDB)

96

U

UG/KG

Vinyl Chloride

96

U

UG/KG

Chlorobenzene

96

U

UG/KG

Bromomethane

96

U

UG/KG

Ethyl Benzene

96

UJ

UG/KG

Chloroethane

96

U

UG/KG

Total Xylenes

96

U

UG/KG

Trichlorofluoromethane (Freon11)

96

U

UG/KG

Styrene

96

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

96

U

UG/KG

Bromoform

96

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

96

U

UG/KG

Isopropylbenzene

96

U

UG/KG

Acetone

96

U

UG/KG

1,1,2,2-Tetrachloroethane

96

U

UG/KG

Carbon Disulfide

96

U

UG/KG

1,3-Dichlorobenzene

96

U

UG/KG

Methyl Acetate

96

U

UG/KG

1,4-Dichlorobenzene

96

U

UG/KG

Methylene Chloride

96

U

UG/KG

1,2-Dichlorobenzene

96

U

UG/KG

trans-1,2-Dichloroethene

96

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

96

U

UG/KG

Methyl T-Butyl Ether (MTBE)

96

U

UG/KG

1,2,4-T richlorobenzene

96

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

96

U

UG/KG

cis-1,2-Dichloroethene

78



%

% Moisture

96

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









96

U

UG/KG

Chloroform









96

U

UG/KG

1,1,1-Trichloroethane









96

U

UG/KG

Cyclohexane









96

U

UG/KG

Carbon Tetrachloride









96

U

UG/KG

Benzene









96

U

UG/KG

1,2-Dichloroethane









96

U

UG/KG

Trichloroethene (Trichloroethylene)









96

U

UG/KG

Methylcyclohexane









96

U

UG/KG

1,2-Dichloropropane









96

U

UG/KG

Bromodichloromethane









96

U

UG/KG

cis-1,3-Dichloropropene









96

U

UG/KG

Methyl Isobutyl Ketone









96

U

UG/KG

Toluene









96

U

UG/KG

trans-1,3-Dichloropropene









96

U

UG/KG

1,1,2-Trichloroethane









96

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









96

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9529 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSD01D /	MD No: 3AG0	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AG0	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

110

u

UG/KG

Dichlorodifluoromethane

110

u

UG/KG

Dibromochloromethane

110

u

UG/KG

Chloromethane

110

u

UG/KG

1,2-Dibromoethane (EDB)

110

u

UG/KG

Vinyl Chloride

110

u

UG/KG

Chlorobenzene

110

u

UG/KG

Bromomethane

110

u

UG/KG

Ethyl Benzene

110

UJ

UG/KG

Chloroethane

110

u

UG/KG

Total Xylenes

110

u

UG/KG

Trichlorofluoromethane (Freon11)

110

u

UG/KG

Styrene

110

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

110

u

UG/KG

Bromoform

110

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

110

u

UG/KG

Isopropylbenzene

140



UG/KG

Acetone

110

u

UG/KG

1,1,2,2-Tetrachloroethane

110

u

UG/KG

Carbon Disulfide

110

u

UG/KG

1,3-Dichlorobenzene

110

u

UG/KG

Methyl Acetate

110

u

UG/KG

1,4-Dichlorobenzene

110

u

UG/KG

Methylene Chloride

110

u

UG/KG

1,2-Dichlorobenzene

110

u

UG/KG

trans-1,2-Dichloroethene

110

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

110

u

UG/KG

Methyl T-Butyl Ether (MTBE)

110

u

UG/KG

1,2,4-T richlorobenzene

110

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

110

u

UG/KG

cis-1,2-Dichloroethene

80



%

% Moisture

110

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









110

u

UG/KG

Chloroform









110

u

UG/KG

1,1,1-Trichloroethane









110

u

UG/KG

Cyclohexane









110

u

UG/KG

Carbon Tetrachloride









110

u

UG/KG

Benzene









110

u

UG/KG

1,2-Dichloroethane









110

u

UG/KG

Trichloroethene (Trichloroethylene)









110

u

UG/KG

Methylcyclohexane









110

u

UG/KG

1,2-Dichloropropane









110

u

UG/KG

Bromodichloromethane









110

u

UG/KG

cis-1,3-Dichloropropene









110

u

UG/KG

Methyl Isobutyl Ketone









110

u

UG/KG

Toluene









110

u

UG/KG

trans-1,3-Dichloropropene









110

u

UG/KG

1,1,2-Trichloroethane









110

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









110

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9530 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG1
D No: 3AG1

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

32

U

UG/KG

Dichlorodifluoromethane

32

U

UG/KG

Dibromochloromethane

32

U

UG/KG

Chloromethane

32

U

UG/KG

1,2-Dibromoethane (EDB)

32

U

UG/KG

Vinyl Chloride

32

U

UG/KG

Chlorobenzene

32

U

UG/KG

Bromomethane

32

U

UG/KG

Ethyl Benzene

32

UJ

UG/KG

Chloroethane

32

U

UG/KG

Total Xylenes

32

U

UG/KG

Trichlorofluoromethane (Freon11)

32

U

UG/KG

Styrene

32

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

32

U

UG/KG

Bromoform

32

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

32

U

UG/KG

Isopropylbenzene

32

U

UG/KG

Acetone

32

U

UG/KG

1,1,2,2-Tetrachloroethane

32

U

UG/KG

Carbon Disulfide

32

U

UG/KG

1,3-Dichlorobenzene

32

U

UG/KG

Methyl Acetate

32

U

UG/KG

1,4-Dichlorobenzene

32

U

UG/KG

Methylene Chloride

32

U

UG/KG

1,2-Dichlorobenzene

32

U

UG/KG

trans-1,2-Dichloroethene

32

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

32

U

UG/KG

Methyl T-Butyl Ether (MTBE)

32

U

UG/KG

1,2,4-T richlorobenzene

32

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

32

U

UG/KG

cis-1,2-Dichloroethene

58



%

% Moisture

32

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









32

U

UG/KG

Chloroform









32

U

UG/KG

1,1,1-Trichloroethane









32

U

UG/KG

Cyclohexane









32

U

UG/KG

Carbon Tetrachloride









32

U

UG/KG

Benzene









32

U

UG/KG

1,2-Dichloroethane









32

U

UG/KG

Trichloroethene (Trichloroethylene)









32

U

UG/KG

Methylcyclohexane









32

U

UG/KG

1,2-Dichloropropane









32

U

UG/KG

Bromodichloromethane









32

U

UG/KG

cis-1,3-Dichloropropene









32

U

UG/KG

Methyl Isobutyl Ketone









32

U

UG/KG

Toluene









32

U

UG/KG

trans-1,3-Dichloropropene









32

U

UG/KG

1,1,2-Trichloroethane









32

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









32

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9531 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: POSD03 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG2
D No: 3AG2

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

u

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

UJ

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

u

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

u

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

17



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9532 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF04 /	MD No: 3AG3	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AG3	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

10

u

UG/KG

Dichlorodifluoromethane

10

u

UG/KG

Dibromochloromethane

10

u

UG/KG

Chloromethane

10

u

UG/KG

1,2-Dibromoethane (EDB)

10

u

UG/KG

Vinyl Chloride

10

u

UG/KG

Chlorobenzene

10

u

UG/KG

Bromomethane

10

u

UG/KG

Ethyl Benzene

10

UJ

UG/KG

Chloroethane

10

u

UG/KG

Total Xylenes

10

u

UG/KG

Trichlorofluoromethane (Freon11)

10

u

UG/KG

Styrene

10

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

10

u

UG/KG

Bromoform

10

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

10

u

UG/KG

Isopropylbenzene

10

UJ

UG/KG

Acetone

10

u

UG/KG

1,1,2,2-Tetrachloroethane

10

u

UG/KG

Carbon Disulfide

10

u

UG/KG

1,3-Dichlorobenzene

10

UJ

UG/KG

Methyl Acetate

10

u

UG/KG

1,4-Dichlorobenzene

10

u

UG/KG

Methylene Chloride

10

u

UG/KG

1,2-Dichlorobenzene

10

u

UG/KG

trans-1,2-Dichloroethene

10

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

10

u

UG/KG

Methyl T-Butyl Ether (MTBE)

10

u

UG/KG

1,2,4-T richlorobenzene

10

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

10

u

UG/KG

cis-1,2-Dichloroethene

12



%

% Moisture

10

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









10

u

UG/KG

Chloroform









10

u

UG/KG

1,1,1-Trichloroethane









10

u

UG/KG

Cyclohexane









10

u

UG/KG

Carbon Tetrachloride









10

u

UG/KG

Benzene









10

u

UG/KG

1,2-Dichloroethane









10

u

UG/KG

Trichloroethene (Trichloroethylene)









10

u

UG/KG

Methylcyclohexane









10

u

UG/KG

1,2-Dichloropropane









10

u

UG/KG

Bromodichloromethane









10

u

UG/KG

cis-1,3-Dichloropropene









10

u

UG/KG

Methyl Isobutyl Ketone









10

u

UG/KG

Toluene









10

u

UG/KG

trans-1,3-Dichloropropene









10

u

UG/KG

1,1,2-Trichloroethane









10

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









10

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9533 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF05 /	MD No: 3AG4	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AG4	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

10

u

UG/KG

Dichlorodifluoromethane

10

u

UG/KG

Dibromochloromethane

10

u

UG/KG

Chloromethane

10

u

UG/KG

1,2-Dibromoethane (EDB)

10

u

UG/KG

Vinyl Chloride

10

u

UG/KG

Chlorobenzene

10

u

UG/KG

Bromomethane

10

u

UG/KG

Ethyl Benzene

10

UJ

UG/KG

Chloroethane

10

u

UG/KG

Total Xylenes

10

u

UG/KG

Trichlorofluoromethane (Freon11)

10

u

UG/KG

Styrene

10

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

10

u

UG/KG

Bromoform

10

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

10

u

UG/KG

Isopropylbenzene

10

UJ

UG/KG

Acetone

10

u

UG/KG

1,1,2,2-Tetrachloroethane

10

u

UG/KG

Carbon Disulfide

10

u

UG/KG

1,3-Dichlorobenzene

10

UJ

UG/KG

Methyl Acetate

10

u

UG/KG

1,4-Dichlorobenzene

10

u

UG/KG

Methylene Chloride

10

u

UG/KG

1,2-Dichlorobenzene

10

u

UG/KG

trans-1,2-Dichloroethene

10

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

10

u

UG/KG

Methyl T-Butyl Ether (MTBE)

10

u

UG/KG

1,2,4-T richlorobenzene

10

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

10

u

UG/KG

cis-1,2-Dichloroethene

13



%

% Moisture

10

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









10

u

UG/KG

Chloroform









10

u

UG/KG

1,1,1-Trichloroethane









10

u

UG/KG

Cyclohexane









10

u

UG/KG

Carbon Tetrachloride









10

u

UG/KG

Benzene









10

u

UG/KG

1,2-Dichloroethane









10

u

UG/KG

Trichloroethene (Trichloroethylene)









10

u

UG/KG

Methylcyclohexane









10

u

UG/KG

1,2-Dichloropropane









10

u

UG/KG

Bromodichloromethane









10

u

UG/KG

cis-1,3-Dichloropropene









10

u

UG/KG

Methyl Isobutyl Ketone









10

u

UG/KG

Toluene









10

u

UG/KG

trans-1,3-Dichloropropene









10

u

UG/KG

1,1,2-Trichloroethane









10

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









10

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9534 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: POSF05S /	MD No: 3AG5	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AG5	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

10

u

UG/KG

Dichlorodifluoromethane

10

u

UG/KG

Dibromochloromethane

10

u

UG/KG

Chloromethane

10

u

UG/KG

1,2-Dibromoethane (EDB)

10

u

UG/KG

Vinyl Chloride

10

u

UG/KG

Chlorobenzene

10

u

UG/KG

Bromomethane

10

u

UG/KG

Ethyl Benzene

10

UJ

UG/KG

Chloroethane

10

u

UG/KG

Total Xylenes

10

u

UG/KG

Trichlorofluoromethane (Freon11)

10

u

UG/KG

Styrene

10

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

10

u

UG/KG

Bromoform

10

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

10

u

UG/KG

Isopropylbenzene

10

UJ

UG/KG

Acetone

10

u

UG/KG

1,1,2,2-Tetrachloroethane

10

u

UG/KG

Carbon Disulfide

10

u

UG/KG

1,3-Dichlorobenzene

10

UJ

UG/KG

Methyl Acetate

10

u

UG/KG

1,4-Dichlorobenzene

10

u

UG/KG

Methylene Chloride

10

u

UG/KG

1,2-Dichlorobenzene

10

u

UG/KG

trans-1,2-Dichloroethene

10

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

10

u

UG/KG

Methyl T-Butyl Ether (MTBE)

10

u

UG/KG

1,2,4-T richlorobenzene

10

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

10

u

UG/KG

cis-1,2-Dichloroethene

13



%

% Moisture

10

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









10

u

UG/KG

Chloroform









10

u

UG/KG

1,1,1-Trichloroethane









10

u

UG/KG

Cyclohexane









10

u

UG/KG

Carbon Tetrachloride









10

u

UG/KG

Benzene









10

u

UG/KG

1,2-Dichloroethane









10

u

UG/KG

Trichloroethene (Trichloroethylene)









10

u

UG/KG

Methylcyclohexane









10

u

UG/KG

1,2-Dichloropropane









10

u

UG/KG

Bromodichloromethane









10

u

UG/KG

cis-1,3-Dichloropropene









10

u

UG/KG

Methyl Isobutyl Ketone









10

u

UG/KG

Toluene









10

u

UG/KG

trans-1,3-Dichloropropene









10

u

UG/KG

1,1,2-Trichloroethane









10

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









10

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/03/2005 12:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9535 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG7
D No: 3AG7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

10

u

UG/KG

Dichlorodifluoromethane

10

u

UG/KG

Dibromochloromethane

10

u

UG/KG

Chloromethane

10

u

UG/KG

1,2-Dibromoethane (EDB)

10

u

UG/KG

Vinyl Chloride

10

u

UG/KG

Chlorobenzene

10

UJ

UG/KG

Bromomethane

10

u

UG/KG

Ethyl Benzene

10

u

UG/KG

Chloroethane

10

u

UG/KG

Total Xylenes

10

u

UG/KG

Trichlorofluoromethane (Freon11)

10

u

UG/KG

Styrene

10

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

10

u

UG/KG

Bromoform

10

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

10

u

UG/KG

Isopropylbenzene

10

UJ

UG/KG

Acetone

10

u

UG/KG

1,1,2,2-Tetrachloroethane

10

u

UG/KG

Carbon Disulfide

10

u

UG/KG

1,3-Dichlorobenzene

10

u

UG/KG

Methyl Acetate

10

u

UG/KG

1,4-Dichlorobenzene

10

UJ

UG/KG

Methylene Chloride

10

u

UG/KG

1,2-Dichlorobenzene

10

u

UG/KG

trans-1,2-Dichloroethene

10

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

10

u

UG/KG

Methyl T-Butyl Ether (MTBE)

10

u

UG/KG

1,2,4-T richlorobenzene

10

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

10

u

UG/KG

cis-1,2-Dichloroethene

14



%

% Moisture

10

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









10

u

UG/KG

Chloroform









10

u

UG/KG

1,1,1-Trichloroethane









10

u

UG/KG

Cyclohexane









10

u

UG/KG

Carbon Tetrachloride









10

u

UG/KG

Benzene









10

u

UG/KG

1,2-Dichloroethane









10

u

UG/KG

Trichloroethene (Trichloroethylene)









10

u

UG/KG

Methylcyclohexane









10

u

UG/KG

1,2-Dichloropropane









10

u

UG/KG

Bromodichloromethane









10

u

UG/KG

cis-1,3-Dichloropropene









10

u

UG/KG

Methyl Isobutyl Ketone









10

u

UG/KG

Toluene









10

u

UG/KG

trans-1,3-Dichloropropene









10

u

UG/KG

1,1,2-Trichloroethane









10

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









10

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9536 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: OPSD02D /	MD No: 3AG8	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AG8	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

UJ

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

u

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

UJ

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

UJ

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

19



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9537 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AG9
D No: 3AG9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

10

u

UG/KG

Dichlorodifluoromethane

10

u

UG/KG

Dibromochloromethane

10

u

UG/KG

Chloromethane

10

u

UG/KG

1,2-Dibromoethane (EDB)

10

u

UG/KG

Vinyl Chloride

10

u

UG/KG

Chlorobenzene

10

UJ

UG/KG

Bromomethane

10

u

UG/KG

Ethyl Benzene

10

u

UG/KG

Chloroethane

10

u

UG/KG

Total Xylenes

10

u

UG/KG

Trichlorofluoromethane (Freon11)

10

u

UG/KG

Styrene

10

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

10

u

UG/KG

Bromoform

10

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

10

u

UG/KG

Isopropylbenzene

10

UJ

UG/KG

Acetone

10

u

UG/KG

1,1,2,2-Tetrachloroethane

10

u

UG/KG

Carbon Disulfide

10

u

UG/KG

1,3-Dichlorobenzene

10

u

UG/KG

Methyl Acetate

10

u

UG/KG

1,4-Dichlorobenzene

10

UJ

UG/KG

Methylene Chloride

10

u

UG/KG

1,2-Dichlorobenzene

10

u

UG/KG

trans-1,2-Dichloroethene

10

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

10

u

UG/KG

Methyl T-Butyl Ether (MTBE)

10

u

UG/KG

1,2,4-T richlorobenzene

10

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

10

u

UG/KG

cis-1,2-Dichloroethene

6



%

% Moisture

10

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









10

u

UG/KG

Chloroform









10

u

UG/KG

1,1,1-Trichloroethane









10

u

UG/KG

Cyclohexane









10

u

UG/KG

Carbon Tetrachloride









10

u

UG/KG

Benzene









10

u

UG/KG

1,2-Dichloroethane









10

u

UG/KG

Trichloroethene (Trichloroethylene)









10

u

UG/KG

Methylcyclohexane









10

u

UG/KG

1,2-Dichloropropane









10

u

UG/KG

Bromodichloromethane









10

u

UG/KG

cis-1,3-Dichloropropene









10

u

UG/KG

Methyl Isobutyl Ketone









10

u

UG/KG

Toluene









10

u

UG/KG

trans-1,3-Dichloropropene









10

u

UG/KG

1,1,2-Trichloroethane









10

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









10

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9538 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: OPSD03 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH0
D No: 3AH0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

UJ

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

u

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

UJ

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

UJ

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

14



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9539 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF01 /	MD No: 3AH1	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AH1	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

16

! U

UG/KG

Dichlorodifluoromethane

18

U

UG/KG

Dibromochloromethane

16

! U

UG/KG

Chloromethane

18

U

UG/KG

1,2-Dibromoethane (EDB)

16

! U

UG/KG

Vinyl Chloride

18

U

UG/KG

Chlorobenzene

16

! UJ

UG/KG

Bromomethane

18

U

UG/KG

Ethyl Benzene

16

! U

UG/KG

Chloroethane

18

U

UG/KG

Total Xylenes

16

! U

UG/KG

Trichlorofluoromethane (Freon11)

18

U

UG/KG

Styrene

16

! U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

18

U

UG/KG

Bromoform

16

! U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

18

U

UG/KG

Isopropylbenzene

16

! UJ

UG/KG

Acetone

18

U

UG/KG

1,1,2,2-Tetrachloroethane

16

! U

UG/KG

Carbon Disulfide

18

U

UG/KG

1,3-Dichlorobenzene

16

! U

UG/KG

Methyl Acetate

18

U

UG/KG

1,4-Dichlorobenzene

16

! UJ

UG/KG

Methylene Chloride

18

U

UG/KG

1,2-Dichlorobenzene

16

! U

UG/KG

trans-1,2-Dichloroethene

18

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

16

! U

UG/KG

Methyl T-Butyl Ether (MTBE)

18

U

UG/KG

1,2,4-T richlorobenzene

16

! U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

16

! U

UG/KG

cis-1,2-Dichloroethene

36



%

% Moisture

16

! U
NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









16

! U

UG/KG

Chloroform









16

! U

UG/KG

1,1,1-Trichloroethane









16

! U

UG/KG

Cyclohexane









16

! U

UG/KG

Carbon Tetrachloride









16

! U

UG/KG

Benzene









16

! U

UG/KG

1,2-Dichloroethane









16

! U

UG/KG

Trichloroethene (Trichloroethylene)









16

! U

UG/KG

Methylcyclohexane









16

! U

UG/KG

1,2-Dichloropropane









16

! U

UG/KG

Bromodichloromethane









16

! U

UG/KG

cis-1,3-Dichloropropene









16

! U

UG/KG

Methyl Isobutyl Ketone









16

! U

UG/KG

Toluene









16

! U

UG/KG

trans-1,3-Dichloropropene









16

! U

UG/KG

1,1,2-Trichloroethane









16

! U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









16

! U

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9540 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF01S /	MD No: 3AH2	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AH2	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

15

U

UG/KG

Dichlorodifluoromethane

15

U

UG/KG

Dibromochloromethane

15

U

UG/KG

Chloromethane

15

U

UG/KG

1,2-Dibromoethane (EDB)

15

U

UG/KG

Vinyl Chloride

15

U

UG/KG

Chlorobenzene

15

UJ

UG/KG

Bromomethane

15

U

UG/KG

Ethyl Benzene

15

U

UG/KG

Chloroethane

15

U

UG/KG

Total Xylenes

15

U

UG/KG

Trichlorofluoromethane (Freon11)

15

U

UG/KG

Styrene

15

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

15

U

UG/KG

Bromoform

15

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

15

U

UG/KG

Isopropylbenzene

15

UJ

UG/KG

Acetone

15

U

UG/KG

1,1,2,2-Tetrachloroethane

15

U

UG/KG

Carbon Disulfide

15

U

UG/KG

1,3-Dichlorobenzene

15

U

UG/KG

Methyl Acetate

15

U

UG/KG

1,4-Dichlorobenzene

15

UJ

UG/KG

Methylene Chloride

15

U

UG/KG

1,2-Dichlorobenzene

15

U

UG/KG

trans-1,2-Dichloroethene

15

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

15

U

UG/KG

Methyl T-Butyl Ether (MTBE)

15

U

UG/KG

1,2,4-T richlorobenzene

15

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

15

U

UG/KG

cis-1,2-Dichloroethene

36



%

% Moisture

15

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









15

U

UG/KG

Chloroform









15

U

UG/KG

1,1,1-Trichloroethane









15

U

UG/KG

Cyclohexane









15

U

UG/KG

Carbon Tetrachloride









15

U

UG/KG

Benzene









15

U

UG/KG

1,2-Dichloroethane









15

U

UG/KG

Trichloroethene (Trichloroethylene)









15

U

UG/KG

Methylcyclohexane









15

U

UG/KG

1,2-Dichloropropane









15

U

UG/KG

Bromodichloromethane









15

U

UG/KG

cis-1,3-Dichloropropene









15

U

UG/KG

Methyl Isobutyl Ketone









15

U

UG/KG

Toluene









15

U

UG/KG

trans-1,3-Dichloropropene









15

U

UG/KG

1,1,2-Trichloroethane









15

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









15

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 09:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9541 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF02 /	MD No: 3AH3	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AH3	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

UJ

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

u

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

UJ

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

UJ

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

9



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9542 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSF03 /	MD No: 3AH4	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AH4	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

UJ

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

u

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

11

UJ

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

UJ

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

18



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:50
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9542 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AH4
D No: 3AH4

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:50
Ending:

RESULTS UNITS

41 J
N

UG/KG
UG/KG

ANALYTE

UNKNOWN

PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9543 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD04 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH5
D No: 3AH5

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:15
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

22

U

UG/KG

Dichlorodifluoromethane

22

U

UG/KG

Dibromochloromethane

22

U

UG/KG

Chloromethane

22

U

UG/KG

1,2-Dibromoethane (EDB)

22

U

UG/KG

Vinyl Chloride

22

U

UG/KG

Chlorobenzene

22

UJ

UG/KG

Bromomethane

22

U

UG/KG

Ethyl Benzene

22

U

UG/KG

Chloroethane

22

U

UG/KG

Total Xylenes

22

U

UG/KG

Trichlorofluoromethane (Freon11)

22

U

UG/KG

Styrene

22

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

22

U

UG/KG

Bromoform

22

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

22

U

UG/KG

Isopropylbenzene

22

UJ

UG/KG

Acetone

22

U

UG/KG

1,1,2,2-Tetrachloroethane

22

U

UG/KG

Carbon Disulfide

22

U

UG/KG

1,3-Dichlorobenzene

22

U

UG/KG

Methyl Acetate

22

U

UG/KG

1,4-Dichlorobenzene

22

UJ

UG/KG

Methylene Chloride

22

U

UG/KG

1,2-Dichlorobenzene

22

U

UG/KG

trans-1,2-Dichloroethene

22

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

22

U

UG/KG

Methyl T-Butyl Ether (MTBE)

22

U

UG/KG

1,2,4-T richlorobenzene

22

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

22

U

UG/KG

cis-1,2-Dichloroethene

45



%

% Moisture

22

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









22

U

UG/KG

Chloroform









22

U

UG/KG

1,1,1-Trichloroethane









22

U

UG/KG

Cyclohexane









22

U

UG/KG

Carbon Tetrachloride









22

U

UG/KG

Benzene









22

U

UG/KG

1,2-Dichloroethane









22

U

UG/KG

Trichloroethene (Trichloroethylene)









22

U

UG/KG

Methylcyclohexane









22

U

UG/KG

1,2-Dichloropropane









22

U

UG/KG

Bromodichloromethane









22

U

UG/KG

cis-1,3-Dichloropropene









22

U

UG/KG

Methyl Isobutyl Ketone









22

U

UG/KG

Toluene









22

U

UG/KG

trans-1,3-Dichloropropene









22

U

UG/KG

1,1,2-Trichloroethane









22

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









22

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9544 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: ERSD04D /	MD No: 3AH6	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AH6	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

16

U

UG/KG

Dichlorodifluoromethane

16

U

UG/KG

Dibromochloromethane

16

U

UG/KG

Chloromethane

16

U

UG/KG

1,2-Dibromoethane (EDB)

16

U

UG/KG

Vinyl Chloride

16

U

UG/KG

Chlorobenzene

16

UJ

UG/KG

Bromomethane

16

U

UG/KG

Ethyl Benzene

16

U

UG/KG

Chloroethane

16

U

UG/KG

Total Xylenes

16

U

UG/KG

Trichlorofluoromethane (Freon11)

16

U

UG/KG

Styrene

16

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

16

U

UG/KG

Bromoform

16

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

16

U

UG/KG

Isopropylbenzene

16

UJ

UG/KG

Acetone

16

U

UG/KG

1,1,2,2-Tetrachloroethane

16

U

UG/KG

Carbon Disulfide

16

U

UG/KG

1,3-Dichlorobenzene

16

U

UG/KG

Methyl Acetate

16

U

UG/KG

1,4-Dichlorobenzene

16

UJ

UG/KG

Methylene Chloride

16

U

UG/KG

1,2-Dichlorobenzene

16

U

UG/KG

trans-1,2-Dichloroethene

16

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

16

U

UG/KG

Methyl T-Butyl Ether (MTBE)

16

U

UG/KG

1,2,4-T richlorobenzene

16

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

16

U

UG/KG

cis-1,2-Dichloroethene

32



%

% Moisture

16

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









16

U

UG/KG

Chloroform









16

U

UG/KG

1,1,1-Trichloroethane









16

U

UG/KG

Cyclohexane









16

U

UG/KG

Carbon Tetrachloride









16

U

UG/KG

Benzene









16

U

UG/KG

1,2-Dichloroethane









16

U

UG/KG

Trichloroethene (Trichloroethylene)









16

U

UG/KG

Methylcyclohexane









16

U

UG/KG

1,2-Dichloropropane









16

U

UG/KG

Bromodichloromethane









16

U

UG/KG

cis-1,3-Dichloropropene









16

U

UG/KG

Methyl Isobutyl Ketone









16

U

UG/KG

Toluene









16

U

UG/KG

trans-1,3-Dichloropropene









16

U

UG/KG

1,1,2-Trichloroethane









16

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









16

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:25
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9545 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: ERSD05 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH7
D No: 3AH7

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

21

U

UG/KG

Dichlorodifluoromethane

21

U

UG/KG

Dibromochloromethane

21

U

UG/KG

Chloromethane

21

U

UG/KG

1,2-Dibromoethane (EDB)

21

U

UG/KG

Vinyl Chloride

21

U

UG/KG

Chlorobenzene

21

UJ

UG/KG

Bromomethane

21

U

UG/KG

Ethyl Benzene

21

U

UG/KG

Chloroethane

21

U

UG/KG

Total Xylenes

21

U

UG/KG

Trichlorofluoromethane (Freon11)

21

U

UG/KG

Styrene

21

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

21

U

UG/KG

Bromoform

21

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

21

U

UG/KG

Isopropylbenzene

21

UJ

UG/KG

Acetone

21

U

UG/KG

1,1,2,2-Tetrachloroethane

21

U

UG/KG

Carbon Disulfide

21

U

UG/KG

1,3-Dichlorobenzene

21

U

UG/KG

Methyl Acetate

21

U

UG/KG

1,4-Dichlorobenzene

21

UJ

UG/KG

Methylene Chloride

21

U

UG/KG

1,2-Dichlorobenzene

21

U

UG/KG

trans-1,2-Dichloroethene

21

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

21

U

UG/KG

Methyl T-Butyl Ether (MTBE)

21

U

UG/KG

1,2,4-T richlorobenzene

21

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

21

U

UG/KG

cis-1,2-Dichloroethene

51



%

% Moisture

21

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









21

U

UG/KG

Chloroform









21

U

UG/KG

1,1,1-Trichloroethane









21

U

UG/KG

Cyclohexane









21

U

UG/KG

Carbon Tetrachloride









21

U

UG/KG

Benzene









21

U

UG/KG

1,2-Dichloroethane









21

U

UG/KG

Trichloroethene (Trichloroethylene)









21

U

UG/KG

Methylcyclohexane









21

U

UG/KG

1,2-Dichloropropane









21

U

UG/KG

Bromodichloromethane









21

U

UG/KG

cis-1,3-Dichloropropene









21

U

UG/KG

Methyl Isobutyl Ketone









21

U

UG/KG

Toluene









21

U

UG/KG

trans-1,3-Dichloropropene









21

U

UG/KG

1,1,2-Trichloroethane









21

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









21

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9546 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD01 /

Media: SEDIMENT

Case No: 34717
MD No: 3AH8
D No: 3AH8

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 10:10
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

34

U

UG/KG

Dichlorodifluoromethane

34

U

UG/KG

Dibromochloromethane

34

U

UG/KG

Chloromethane

34

U

UG/KG

1,2-Dibromoethane (EDB)

34

U

UG/KG

Vinyl Chloride

34

U

UG/KG

Chlorobenzene

34

UJ

UG/KG

Bromomethane

34

U

UG/KG

Ethyl Benzene

34

U

UG/KG

Chloroethane

34

U

UG/KG

Total Xylenes

34

U

UG/KG

Trichlorofluoromethane (Freon11)

34

U

UG/KG

Styrene

34

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

34

U

UG/KG

Bromoform

34

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

34

U

UG/KG

Isopropylbenzene

34

UJ

UG/KG

Acetone

34

U

UG/KG

1,1,2,2-Tetrachloroethane

34

U

UG/KG

Carbon Disulfide

34

U

UG/KG

1,3-Dichlorobenzene

34

U

UG/KG

Methyl Acetate

34

U

UG/KG

1,4-Dichlorobenzene

34

UJ

UG/KG

Methylene Chloride

34

U

UG/KG

1,2-Dichlorobenzene

34

U

UG/KG

trans-1,2-Dichloroethene

34

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

34

U

UG/KG

Methyl T-Butyl Ether (MTBE)

34

U

UG/KG

1,2,4-T richlorobenzene

34

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

34

U

UG/KG

cis-1,2-Dichloroethene

56



%

% Moisture

34

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









34

U

UG/KG

Chloroform









34

U

UG/KG

1,1,1-Trichloroethane









34

U

UG/KG

Cyclohexane









34

U

UG/KG

Carbon Tetrachloride









34

U

UG/KG

Benzene









34

U

UG/KG

1,2-Dichloroethane









34

U

UG/KG

Trichloroethene (Trichloroethylene)









34

U

UG/KG

Methylcyclohexane









34

U

UG/KG

1,2-Dichloropropane









34

U

UG/KG

Bromodichloromethane









34

U

UG/KG

cis-1,3-Dichloropropene









34

U

UG/KG

Methyl Isobutyl Ketone









34

U

UG/KG

Toluene









34

U

UG/KG

trans-1,3-Dichloropropene









34

U

UG/KG

1,1,2-Trichloroethane









34

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









34

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9547 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD01D /	MD No: 3AH9	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AH9	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

38

U

UG/KG

Dichlorodifluoromethane

38

U

UG/KG

Dibromochloromethane

38

UJ

UG/KG

Chloromethane

38

U

UG/KG

1,2-Dibromoethane (EDB)

38

U

UG/KG

Vinyl Chloride

38

U

UG/KG

Chlorobenzene

38

U

UG/KG

Bromomethane

38

U

UG/KG

Ethyl Benzene

38

UJ

UG/KG

Chloroethane

38

U

UG/KG

Total Xylenes

38

U

UG/KG

Trichlorofluoromethane (Freon11)

38

U

UG/KG

Styrene

38

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

38

U

UG/KG

Bromoform

38

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

38

U

UG/KG

Isopropylbenzene

50

J

UG/KG

Acetone

38

U

UG/KG

1,1,2,2-Tetrachloroethane

38

U

UG/KG

Carbon Disulfide

38

U

UG/KG

1,3-Dichlorobenzene

38

U

UG/KG

Methyl Acetate

38

U

UG/KG

1,4-Dichlorobenzene

38

U

UG/KG

Methylene Chloride

38

U

UG/KG

1,2-Dichlorobenzene

38

U

UG/KG

trans-1,2-Dichloroethene

38

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

38

U

UG/KG

Methyl T-Butyl Ether (MTBE)

38

U

UG/KG

1,2,4-T richlorobenzene

38

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

38

U

UG/KG

cis-1,2-Dichloroethene

55



%

% Moisture

38

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









38

U

UG/KG

Chloroform









38

U

UG/KG

1,1,1-Trichloroethane









38

U

UG/KG

Cyclohexane









38

U

UG/KG

Carbon Tetrachloride









38

U

UG/KG

Benzene









38

U

UG/KG

1,2-Dichloroethane









38

U

UG/KG

Trichloroethene (Trichloroethylene)









38

U

UG/KG

Methylcyclohexane









38

U

UG/KG

1,2-Dichloropropane









38

U

UG/KG

Bromodichloromethane









38

U

UG/KG

cis-1,3-Dichloropropene









38

U

UG/KG

Methyl Isobutyl Ketone









38

U

UG/KG

Toluene









38

U

UG/KG

trans-1,3-Dichloropropene









38

U

UG/KG

1,1,2-Trichloroethane









38

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









38

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9547 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD01D/

Media: SEDIMENT

Case No: 34717
MD No: 3AH9
D No: 3AH9

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 11:05
Ending:

RESULTS UNITS

36 NJ UG/KG
N UG/KG

ANALYTE

BENZENE, 1 -METHYL-3-(1 -METHYLETHYL)-
PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9548 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSD02 /

Media: SEDIMENT

Case No: 34717
MD No: 3AJ0
D No: 3AJ0

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 12:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

66

UJ

UG/KG

Dichlorodifluoromethane

66

U

UG/KG

Dibromochloromethane

66

UJ

UG/KG

Chloromethane

66

U

UG/KG

1,2-Dibromoethane (EDB)

66

UJ

UG/KG

Vinyl Chloride

66

U

UG/KG

Chlorobenzene

66

UJ

UG/KG

Bromomethane

230

J

UG/KG

Ethyl Benzene

66

UJ

UG/KG

Chloroethane

760

J

UG/KG

Total Xylenes

66

UJ

UG/KG

Trichlorofluoromethane (Freon11)

66

U

UG/KG

Styrene

66

UJ

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

66

U

UG/KG

Bromoform

66

UJ

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

140

J

UG/KG

Isopropylbenzene

68

J

UG/KG

Acetone

66

U

UG/KG

1,1,2,2-Tetrachloroethane

66

UJ

UG/KG

Carbon Disulfide

66

U

UG/KG

1,3-Dichlorobenzene

66

UJ

UG/KG

Methyl Acetate

66

U

UG/KG

1,4-Dichlorobenzene

66

UJ

UG/KG

Methylene Chloride

66

U

UG/KG

1,2-Dichlorobenzene

66

UJ

UG/KG

trans-1,2-Dichloroethene

66

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

66

UJ

UG/KG

Methyl T-Butyl Ether (MTBE)

66

U

UG/KG

1,2,4-T richlorobenzene

66

UJ

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

66

UJ

UG/KG

cis-1,2-Dichloroethene

24



%

% Moisture

66

UJ
NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









66

UJ

UG/KG

Chloroform









66

U

UG/KG

1,1,1-Trichloroethane









66

U

UG/KG

Cyclohexane









66

U

UG/KG

Carbon Tetrachloride









24

J

UG/KG

Benzene









66

UJ

UG/KG

1,2-Dichloroethane









66

U

UG/KG

Trichloroethene (Trichloroethylene)









140

J

UG/KG

Methylcyclohexane









66

UJ

UG/KG

1,2-Dichloropropane









66

UJ

UG/KG

Bromodichloromethane









66

UJ

UG/KG

cis-1,3-Dichloropropene









66

U

UG/KG

Methyl Isobutyl Ketone









23

J

UG/KG

Toluene









66

U

UG/KG

trans-1,3-Dichloropropene









66

U

UG/KG

1,1,2-Trichloroethane









66

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









66

U

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9548 FY 2005 Project: 05-0928
MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSD02 /	MD No: 3AJ0	Inorg Contractor: LIBRTY

Media: SEDIMENT	D No: 3AJ0	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

22000

NJ

UG/KG

6 SUBSTITUTED BENZENES

37000

J

UG/KG

12 UNKNOWNS

3300

NJ

UG/KG

BENZENE, 1-ETHYL-2.3-DIMETHYL

3200

NJ

UG/KG

BENZENE, 1 -METHYL-2-(1 -METHYLETHYL)-

2700

NJ

UG/KG

BENZENE, 1,4-DIETHYL-

2000

NJ

UG/KG

1H-INDENE, 2,3-DIHYDRO-4,7-DIMETHYL-

2900

NJ

UG/KG

BENZENE, 1-ETHYL-2,4,5-TRIMETHYL-

4900

NJ

UG/KG

1 H-INDENE, 2.3-DIHYDRO-1,2-DIMETHYL-

2200

NJ

UG/KG

1 H-INDENE, 2.3-DIHYDRO-1,1-DIMETHYL-

2000

NJ

UG/KG

NAPHTHALENE, 1,2,3,4-TETRAHYDRO-5-METHYL-

2100

NJ

UG/KG

1 H-INDENE, 2.3-DIHYDRO-1,1,5-TRIMETHYL-

4000

NJ

UG/KG

BENZOCYCLOHEPTATRIENE

3200

NJ

UG/KG

NAPHTHALENE, 1-METHYL-

2000

NJ

UG/KG

BENZENE, 1,3,5-TRIMETHYL-2-(1-METHYLETHYL)-



N

UG/KG

PETROLEUM PRODUCT

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 12:00
Ending:

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9549 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF05 /	MD No: 3AJ1	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ1	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

12

U

UG/KG

Dichlorodifluoromethane

12

U

UG/KG

Dibromochloromethane

12

UJ

UG/KG

Chloromethane

12

U

UG/KG

1,2-Dibromoethane (EDB)

12

U

UG/KG

Vinyl Chloride

12

U

UG/KG

Chlorobenzene

12

U

UG/KG

Bromomethane

12

U

UG/KG

Ethyl Benzene

12

UJ

UG/KG

Chloroethane

12

U

UG/KG

Total Xylenes

12

U

UG/KG

Trichlorofluoromethane (Freon11)

12

U

UG/KG

Styrene

12

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

12

U

UG/KG

Bromoform

12

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

12

U

UG/KG

Isopropylbenzene

95

J

UG/KG

Acetone

12

U

UG/KG

1,1,2,2-Tetrachloroethane

12

U

UG/KG

Carbon Disulfide

12

U

UG/KG

1,3-Dichlorobenzene

12

U

UG/KG

Methyl Acetate

12

U

UG/KG

1,4-Dichlorobenzene

12

U

UG/KG

Methylene Chloride

12

U

UG/KG

1,2-Dichlorobenzene

12

U

UG/KG

trans-1,2-Dichloroethene

12

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

12

U

UG/KG

Methyl T-Butyl Ether (MTBE)

12

U

UG/KG

1,2,4-T richlorobenzene

12

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

12

U

UG/KG

cis-1,2-Dichloroethene

10



%

% Moisture

12

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









12

U

UG/KG

Chloroform









12

U

UG/KG

1,1,1-Trichloroethane









12

U

UG/KG

Cyclohexane









12

U

UG/KG

Carbon Tetrachloride









12

U

UG/KG

Benzene









12

U

UG/KG

1,2-Dichloroethane









12

U

UG/KG

Trichloroethene (Trichloroethylene)









12

U

UG/KG

Methylcyclohexane









12

U

UG/KG

1,2-Dichloropropane









12

U

UG/KG

Bromodichloromethane









12

U

UG/KG

cis-1,3-Dichloropropene









12

U

UG/KG

Methyl Isobutyl Ketone









12

U

UG/KG

Toluene









12

U

UG/KG

trans-1,3-Dichloropropene









12

U

UG/KG

1,1,2-Trichloroethane









12

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









12

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:20
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9550 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF04 /	MD No: 3AJ2	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ2	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

U

UG/KG

Dibromochloromethane

11

UJ

UG/KG

Chloromethane

11

U

UG/KG

1,2-Dibromoethane (EDB)

11

U

UG/KG

Vinyl Chloride

11

U

UG/KG

Chlorobenzene

11

U

UG/KG

Bromomethane

11

U

UG/KG

Ethyl Benzene

11

UJ

UG/KG

Chloroethane

11

U

UG/KG

Total Xylenes

11

U

UG/KG

Trichlorofluoromethane (Freon11)

11

U

UG/KG

Styrene

11

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

U

UG/KG

Bromoform

11

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

U

UG/KG

Isopropylbenzene

53

J

UG/KG

Acetone

11

U

UG/KG

1,1,2,2-Tetrachloroethane

11

U

UG/KG

Carbon Disulfide

11

U

UG/KG

1,3-Dichlorobenzene

11

U

UG/KG

Methyl Acetate

11

U

UG/KG

1,4-Dichlorobenzene

11

U

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

U

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

U

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

U

UG/KG

cis-1,2-Dichloroethene

12



%

% Moisture

11

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

U

UG/KG

Carbon Tetrachloride









11

U

UG/KG

Benzene









11

U

UG/KG

1,2-Dichloroethane









11

U

UG/KG

Trichloroethene (Trichloroethylene)









11

U

UG/KG

Methylcyclohexane









11

U

UG/KG

1,2-Dichloropropane









11

U

UG/KG

Bromodichloromethane









11

U

UG/KG

cis-1,3-Dichloropropene









11

U

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 13:45
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9551 FY 2005 Project: 05-0928
Volatiles Scan

Facility: Hurricane Katrina Response

Program: SF	Case No: 34717

Id/Station: DUSF03 /	MD No: 3AJ3	Inorg Contractor: LIBRTY

Media: SURFACE SOIL	D No: 3AJ3	Org Contractor: LIBRTY

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

12

U

UG/KG

Dichlorodifluoromethane

12

U

UG/KG

Dibromochloromethane

12

U

UG/KG

Chloromethane

12

U

UG/KG

1,2-Dibromoethane (EDB)

12

U

UG/KG

Vinyl Chloride

12

U

UG/KG

Chlorobenzene

12

UJ

UG/KG

Bromomethane

12

U

UG/KG

Ethyl Benzene

12

U

UG/KG

Chloroethane

12

U

UG/KG

Total Xylenes

12

U

UG/KG

Trichlorofluoromethane (Freon11)

12

U

UG/KG

Styrene

12

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

12

U

UG/KG

Bromoform

12

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

12

U

UG/KG

Isopropylbenzene

12

UJ

UG/KG

Acetone

12

U

UG/KG

1,1,2,2-Tetrachloroethane

12

U

UG/KG

Carbon Disulfide

12

U

UG/KG

1,3-Dichlorobenzene

12

U

UG/KG

Methyl Acetate

12

U

UG/KG

1,4-Dichlorobenzene

12

UJ

UG/KG

Methylene Chloride

12

U

UG/KG

1,2-Dichlorobenzene

12

U

UG/KG

trans-1,2-Dichloroethene

12

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

12

U

UG/KG

Methyl T-Butyl Ether (MTBE)

12

U

UG/KG

1,2,4-T richlorobenzene

12

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

12

U

UG/KG

cis-1,2-Dichloroethene

14



%

% Moisture

12

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









12

U

UG/KG

Chloroform









12

U

UG/KG

1,1,1-Trichloroethane









12

U

UG/KG

Cyclohexane









12

U

UG/KG

Carbon Tetrachloride









12

U

UG/KG

Benzene









12

U

UG/KG

1,2-Dichloroethane









12

U

UG/KG

Trichloroethene (Trichloroethylene)









12

U

UG/KG

Methylcyclohexane









12

U

UG/KG

1,2-Dichloropropane









12

U

UG/KG

Bromodichloromethane









12

U

UG/KG

cis-1,3-Dichloropropene









12

U

UG/KG

Methyl Isobutyl Ketone









12

U

UG/KG

Toluene









12

U

UG/KG

trans-1,3-Dichloropropene









12

U

UG/KG

1,1,2-Trichloroethane









12

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









12

u

UG/KG

Methyl Butyl Ketone









Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 14:05
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9551 FY 2005 Project: 05-0928

MISCELLANEOUS COMPOUNDS

Facility: Hurricane Katrina Response
Program: SF
Id/Station: DUSF03 /

Media: SURFACE SOIL

Case No: 34717
MD No: 3AJ3
D No: 3AJ3

Inorg Contractor: LIBRTY
Org Contractor: LIBRTY

Produced by: Appleby, Charlie
Requestor:

Project Leader: FSLOAN
Beginning: 10/04/2005 14:05
Ending:

RESULTS UNITS

6 J UG/KG
N UG/KG

ANALYTE

UNKNOWN

PETROLEUM PRODUCT

Data Reported as Identified by CLP Lab - IDs Not Verified

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9552 FY 2005 Project:	05-0928 Produced by: Appleby, Charlie

,, . ~	Requestor:

Vo ati es Scan

Project Leader: FSLOAN

Facility: Hurricane Katrina Response	Beginning: 10/06/2005 14:26

Program: SF	Case No: 34717 Ending:

Id/Station: TB903/

Media: TRIP BLANK-SOIL	D No: 3AK3 Org Contractor: LI BRTY	DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

12

U

UG/KG

Dichlorodifluoromethane

12

U

UG/KG

Dibromochloromethane

12

U

UG/KG

Chloromethane

12

U

UG/KG

1,2-Dibromoethane (EDB)

12

U

UG/KG

Vinyl Chloride

12

U

UG/KG

Chlorobenzene

12

U

UG/KG

Bromomethane

12

U

UG/KG

Ethyl Benzene

12

UJ

UG/KG

Chloroethane

12

U

UG/KG

Total Xylenes

12

U

UG/KG

Trichlorofluoromethane (Freon11)

12

U

UG/KG

Styrene

12

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

12

U

UG/KG

Bromoform

12

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

12

U

UG/KG

Isopropylbenzene

17



UG/KG

Acetone

12

U

UG/KG

1,1,2,2-Tetrachloroethane

12

U

UG/KG

Carbon Disulfide

12

U

UG/KG

1,3-Dichlorobenzene

12

U

UG/KG

Methyl Acetate

12

U

UG/KG

1,4-Dichlorobenzene

12

U

UG/KG

Methylene Chloride

12

U

UG/KG

1,2-Dichlorobenzene

12

U

UG/KG

trans-1,2-Dichloroethene

12

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

12

U

UG/KG

Methyl T-Butyl Ether (MTBE)

12

U

UG/KG

1,2,4-T richlorobenzene

12

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

12

U

UG/KG

cis-1,2-Dichloroethene

0



%

% Moisture

12

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









12

U

UG/KG

Chloroform









12

U

UG/KG

1,1,1-Trichloroethane









12

U

UG/KG

Cyclohexane









12

U

UG/KG

Carbon Tetrachloride









12

U

UG/KG

Benzene









12

U

UG/KG

1,2-Dichloroethane









12

U

UG/KG

Trichloroethene (Trichloroethylene)









12

U

UG/KG

Methylcyclohexane









12

U

UG/KG

1,2-Dichloropropane









12

U

UG/KG

Bromodichloromethane









12

U

UG/KG

cis-1,3-Dichloropropene









12

U

UG/KG

Methyl Isobutyl Ketone









12

U

UG/KG

Toluene









12

U

UG/KG

trans-1,3-Dichloropropene









12

U

UG/KG

1,1,2-Trichloroethane









12

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









12

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9553 FY 2005 Project: 05-0928	Produced by: Appleby, Charlie

,, . ~	Requestor:

Vo ati es Scan

Project Leader: FSLOAN

Facility: Hurricane Katrina Response	Beginning: 10/06/2005 14:27

Program: SF	Case No: 34717 Ending:

Id/Station: TB904 /

Media: TRIP BLANK-SOIL	D No: 3AK4 Org Contractor: LI BRTY	DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

13

U

UG/KG

Dichlorodifluoromethane

13

U

UG/KG

Dibromochloromethane

13

U

UG/KG

Chloromethane

13

U

UG/KG

1,2-Dibromoethane (EDB)

13

U

UG/KG

Vinyl Chloride

13

U

UG/KG

Chlorobenzene

13

U

UG/KG

Bromomethane

13

U

UG/KG

Ethyl Benzene

13

UJ

UG/KG

Chloroethane

13

U

UG/KG

Total Xylenes

13

U

UG/KG

Trichlorofluoromethane (Freon11)

13

U

UG/KG

Styrene

13

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

13

U

UG/KG

Bromoform

13

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

13

U

UG/KG

Isopropylbenzene

14



UG/KG

Acetone

13

U

UG/KG

1,1,2,2-Tetrachloroethane

13

U

UG/KG

Carbon Disulfide

13

U

UG/KG

1,3-Dichlorobenzene

13

U

UG/KG

Methyl Acetate

13

U

UG/KG

1,4-Dichlorobenzene

13

U

UG/KG

Methylene Chloride

13

U

UG/KG

1,2-Dichlorobenzene

13

U

UG/KG

trans-1,2-Dichloroethene

13

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

13

U

UG/KG

Methyl T-Butyl Ether (MTBE)

13

U

UG/KG

1,2,4-T richlorobenzene

13

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

13

U

UG/KG

cis-1,2-Dichloroethene

0



%

% Moisture

13

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









13

U

UG/KG

Chloroform









13

U

UG/KG

1,1,1-Trichloroethane









13

U

UG/KG

Cyclohexane









13

U

UG/KG

Carbon Tetrachloride









13

U

UG/KG

Benzene









13

U

UG/KG

1,2-Dichloroethane









13

U

UG/KG

Trichloroethene (Trichloroethylene)









13

U

UG/KG

Methylcyclohexane









13

U

UG/KG

1,2-Dichloropropane









13

U

UG/KG

Bromodichloromethane









13

U

UG/KG

cis-1,3-Dichloropropene









13

U

UG/KG

Methyl Isobutyl Ketone









13

U

UG/KG

Toluene









13

U

UG/KG

trans-1,3-Dichloropropene









13

U

UG/KG

1,1,2-Trichloroethane









13

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









13

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9554 FY 2005 Project:	05-0928 Produced by: Appleby, Charlie

,, . ~	Requestor:

Vo ati es Scan

Project Leader: FSLOAN

Facility: Hurricane Katrina Response	Beginning: 10/03/2005 15:21

Program: SF	Case No: 34717 Ending:

Id/Station: POTB901 /

Media: TRIP BLANK-SOIL	D No: 3AF8 Org Contractor: LI BRTY	DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Dichlorodifluoromethane

11

u

UG/KG

Dibromochloromethane

11

u

UG/KG

Chloromethane

11

u

UG/KG

1,2-Dibromoethane (EDB)

11

u

UG/KG

Vinyl Chloride

11

u

UG/KG

Chlorobenzene

11

u

UG/KG

Bromomethane

11

u

UG/KG

Ethyl Benzene

11

UJ

UG/KG

Chloroethane

11

u

UG/KG

Total Xylenes

11

u

UG/KG

Trichlorofluoromethane (Freon11)

11

u

UG/KG

Styrene

11

u

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

11

u

UG/KG

Bromoform

11

u

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

11

u

UG/KG

Isopropylbenzene

11



UG/KG

Acetone

11

u

UG/KG

1,1,2,2-Tetrachloroethane

11

u

UG/KG

Carbon Disulfide

11

u

UG/KG

1,3-Dichlorobenzene

11

u

UG/KG

Methyl Acetate

11

u

UG/KG

1,4-Dichlorobenzene

11

u

UG/KG

Methylene Chloride

11

u

UG/KG

1,2-Dichlorobenzene

11

u

UG/KG

trans-1,2-Dichloroethene

11

u

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

11

u

UG/KG

Methyl T-Butyl Ether (MTBE)

11

u

UG/KG

1,2,4-T richlorobenzene

11

u

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

11

u

UG/KG

cis-1,2-Dichloroethene

0



%

% Moisture

11

u

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









11

U

UG/KG

Chloroform









11

U

UG/KG

1,1,1-Trichloroethane









11

U

UG/KG

Cyclohexane









11

u

UG/KG

Carbon Tetrachloride









11

u

UG/KG

Benzene









11

u

UG/KG

1,2-Dichloroethane









11

u

UG/KG

Trichloroethene (Trichloroethylene)









11

u

UG/KG

Methylcyclohexane









11

u

UG/KG

1,2-Dichloropropane









11

u

UG/KG

Bromodichloromethane









11

u

UG/KG

cis-1,3-Dichloropropene









11

u

UG/KG

Methyl Isobutyl Ketone









11

u

UG/KG

Toluene









11

u

UG/KG

trans-1,3-Dichloropropene









11

u

UG/KG

1,1,2-Trichloroethane









11

u

UG/KG

Tetrachloroethene (Tetrachloroethylene)









11

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/31/2005 12:29

Sample 9555 FY 2005 Project:	05-0928 Produced by: Appleby, Charlie

,, . ~	Requestor:

Vo ati es Scan

Project Leader: FSLOAN

Facility: Hurricane Katrina Response	Beginning: 10/04/2005 12:29

Program: SF	Case No: 34717 Ending:

Id/Station: TB902/

Media: TRIP BLANK-SOIL	D No: 3AG6 Org Contractor: LI BRTY	DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

14

U

UG/KG

Dichlorodifluoromethane

14

U

UG/KG

Dibromochloromethane

14

U

UG/KG

Chloromethane

14

U

UG/KG

1,2-Dibromoethane (EDB)

14

U

UG/KG

Vinyl Chloride

14

U

UG/KG

Chlorobenzene

14

UJ

UG/KG

Bromomethane

14

U

UG/KG

Ethyl Benzene

14

U

UG/KG

Chloroethane

14

U

UG/KG

Total Xylenes

14

U

UG/KG

Trichlorofluoromethane (Freon11)

14

U

UG/KG

Styrene

14

U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

14

U

UG/KG

Bromoform

14

U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

14

U

UG/KG

Isopropylbenzene

14

UJ

UG/KG

Acetone

14

U

UG/KG

1,1,2,2-Tetrachloroethane

14

U

UG/KG

Carbon Disulfide

14

U

UG/KG

1,3-Dichlorobenzene

14

U

UG/KG

Methyl Acetate

14

U

UG/KG

1,4-Dichlorobenzene

14

UJ

UG/KG

Methylene Chloride

14

U

UG/KG

1,2-Dichlorobenzene

14

U

UG/KG

trans-1,2-Dichloroethene

14

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

14

U

UG/KG

Methyl T-Butyl Ether (MTBE)

14

U

UG/KG

1,2,4-T richlorobenzene

14

U

UG/KG

1,1-Dichloroethane



NA

UG/KG

1,2,3-Trichlorobenzene

14

U

UG/KG

cis-1,2-Dichloroethene

0



%

% Moisture

14

U

NA

UG/KG
UG/KG

Methyl Ethyl Ketone
Bromochloromethane









14

U

UG/KG

Chloroform









14

U

UG/KG

1,1,1-Trichloroethane









14

U

UG/KG

Cyclohexane









14

U

UG/KG

Carbon Tetrachloride









14

U

UG/KG

Benzene









14

U

UG/KG

1,2-Dichloroethane









14

U

UG/KG

Trichloroethene (Trichloroethylene)









14

U

UG/KG

Methylcyclohexane









14

U

UG/KG

1,2-Dichloropropane









14

U

UG/KG

Bromodichloromethane









14

U

UG/KG

cis-1,3-Dichloropropene









14

U

UG/KG

Methyl Isobutyl Ketone









14

U

UG/KG

Toluene









14

U

UG/KG

trans-1,3-Dichloropropene









14

U

UG/KG

1,1,2-Trichloroethane









14

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)









14

u

UG/KG

Methyl Butyl Ketone









U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 11:25

Sample 9397 FY 2005 Project: 05-0926
Extractables Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC2SD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

900

U

UG/KG

bis(2-Chloroethyl) Ether

900

U

UG/KG

Anthracene

900

UJ

UG/KG

Benzaldehyde

900

U

UG/KG

Carbazole

900

U

UG/KG

Hexachloroethane

900

U

UG/KG

Di-n-Butylphthalate

900

U

UG/KG

bis(2-Chloroisopropyl) Ether

900

U

UG/KG

Fluoranthene

900

U

UG/KG

n-Nitroso di-n-Propylamine

900

U

UG/KG

Pyrene

900

U

UG/KG

Acetophenone

900

U

UG/KG

Benzyl Butyl Phthalate

900

U

UG/KG

Nitrobenzene

900

U

UG/KG

bis(2-Ethylhexyl) Phthalate

900

U

UG/KG

Hexachlorobutadiene

900

U

UG/KG

Benzo(a)Anthracene

900

U

UG/KG

Caprolactam

900

U

UG/KG

Chrysene

900

U

UG/KG

2-Methylnaphthalene

900

U

UG/KG

3,3'-Dichlorobenzidine

900

U

UG/KG

1,2,4-T richlorobenzene

900

U

UG/KG

Di-n-Octylphthalate

900

U

UG/KG

Naphthalene

900

U

UG/KG

Benzo(b)Fluoranthene

900

U

UG/KG

4-Chloroaniline

900

U

UG/KG

Benzo(k)Fluoranthene

900

U

UG/KG

bis(2-Chloroethoxy)Methane

900

U

UG/KG

Benzo-a-Pyrene

900

U

UG/KG

Isophorone

900

U

UG/KG

Indeno (1,2,3-cd) Pyrene

900

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

900

U

UG/KG

Dibenzo(a,h)Anthracene

900

U

UG/KG

1,1 -Biphenyl

900

U

UG/KG

Benzo(ghi)Perylene

900

u

UG/KG

2-Chloronaphthalene

900

U

UG/KG

2-Chlorophenol

900

u

UG/KG

2-Nitroaniline

900

U

UG/KG

2-Methylphenol

900

u

UG/KG

Acenaphthylene

900

U

UG/KG

(3-and/or 4-)Methylphenol

900

u

UG/KG

Acenaphthene

900

u

UG/KG

2-Nitrophenol

900

u

UG/KG

Dimethyl Phthalate

900

u

UG/KG

Phenol

900

u

UG/KG

Dibenzofuran

900

u

UG/KG

2,4-Dimethylphenol

900

u

UG/KG

2,4-Dinitrotoluene

900

u

UG/KG

2,4-Dichlorophenol

900

u

UG/KG

2,6-Dinitrotoluene

900

u

UG/KG

2,4,6-T richlorophenol

900

u

UG/KG

3-Nitroaniline

900

u

UG/KG

2,4,5-Trichlorophenol

900

u

UG/KG

4-Chlorophenyl Phenyl Ether

900

u

UG/KG

4-Chloro-3-Methylphenol

900

u

UG/KG

4-Nitroaniline

1800

UJ

UG/KG

2,4-Dinitrophenol

900

u

UG/KG

Fluorene

1800

u

UG/KG

2-Methyl-4,6-Dinitrophenol

900

u

UG/KG

Diethyl Phthalate

1800

u

UG/KG

Pentachlorophenol

900

u

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

1800

u

UG/KG

4-Nitrophenol

900

u

UG/KG

Hexachlorobenzene (HCB)

900

u

UG/KG

2,3,4,6-Tetrachlorophenol

900

u

UG/KG

Atrazine

63.61



%

% Moisture

900

u

UG/KG

4-Bromophenyl Phenyl Ether









900

u

UG/KG

Phenanthrene









Produced by: Muse, Janet
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

J- due to RSD >20% on ICAL for Benzaldehyde
J-qualified due to QC Limits Exceeded for 2,4-Dinitrophenol

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 11:25

Sample 9400 FY 2005 Project: 05-0926
Extractables Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4DSD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

460

U

UG/KG

bis(2-Chloroethyl) Ether

460

U

UG/KG

Anthracene

460

UJ

UG/KG

Benzaldehyde

460

U

UG/KG

Carbazole

460

U

UG/KG

Hexachloroethane

460

U

UG/KG

Di-n-Butylphthalate

460

U

UG/KG

bis(2-Chloroisopropyl) Ether

66

J

UG/KG

Fluoranthene

460

U

UG/KG

n-Nitroso di-n-Propylamine

63

J

UG/KG

Pyrene

460

U

UG/KG

Acetophenone

460

U

UG/KG

Benzyl Butyl Phthalate

460

U

UG/KG

Nitrobenzene

460

U

UG/KG

bis(2-Ethylhexyl) Phthalate

460

U

UG/KG

Hexachlorobutadiene

460

U

UG/KG

Benzo(a)Anthracene

460

U

UG/KG

Caprolactam

460

U

UG/KG

Chrysene

460

U

UG/KG

2-Methylnaphthalene

460

U

UG/KG

3,3'-Dichlorobenzidine

460

U

UG/KG

1,2,4-T richlorobenzene

460

U

UG/KG

Di-n-Octylphthalate

460

U

UG/KG

Naphthalene

460

U

UG/KG

Benzo(b)Fluoranthene

460

U

UG/KG

4-Chloroaniline

460

U

UG/KG

Benzo(k)Fluoranthene

460

U

UG/KG

bis(2-Chloroethoxy)Methane

460

U

UG/KG

Benzo-a-Pyrene

460

U

UG/KG

Isophorone

460

U

UG/KG

Indeno (1,2,3-cd) Pyrene

460

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

460

U

UG/KG

Dibenzo(a,h)Anthracene

460

U

UG/KG

1,1 -Biphenyl

460

U

UG/KG

Benzo(ghi)Perylene

460

U

UG/KG

2-Chloronaphthalene

460

U

UG/KG

2-Chlorophenol

460

U

UG/KG

2-Nitroaniline

460

U

UG/KG

2-Methylphenol

460

U

UG/KG

Acenaphthylene

460

U

UG/KG

(3-and/or 4-)Methylphenol

460

U

UG/KG

Acenaphthene

460

U

UG/KG

2-Nitrophenol

460

U

UG/KG

Dimethyl Phthalate

460

U

UG/KG

Phenol

460

U

UG/KG

Dibenzofuran

460

U

UG/KG

2,4-Dimethylphenol

460

U

UG/KG

2,4-Dinitrotoluene

460

U

UG/KG

2,4-Dichlorophenol

460

u

UG/KG

2,6-Dinitrotoluene

460

U

UG/KG

2,4,6-T richlorophenol

460

u

UG/KG

3-Nitroaniline

460

U

UG/KG

2,4,5-Trichlorophenol

460

u

UG/KG

4-Chlorophenyl Phenyl Ether

460

U

UG/KG

4-Chloro-3-Methylphenol

460

u

UG/KG

4-Nitroaniline

930

UJ

UG/KG

2,4-Dinitrophenol

460

u

UG/KG

Fluorene

930

u

UG/KG

2-Methyl-4,6-Dinitrophenol

460

u

UG/KG

Diethyl Phthalate

930

u

UG/KG

Pentachlorophenol

460

u

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

930

u

UG/KG

4-Nitrophenol

460

u

UG/KG

Hexachlorobenzene (HCB)

460

u

UG/KG

2,3,4,6-Tetrachlorophenol

460

u

UG/KG

Atrazine

29.58



%

% Moisture

460

u

UG/KG

4-Bromophenyl Phenyl Ether









460

u

UG/KG

Phenanthrene









Produced by: Muse, Janet
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 13:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

J- due to RSD >20% on ICAL for Benzaldehyde	J-qualified due to QC Limits Exceeded for 2,4-Dinitrophenol

J-qualified: value 
-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 11:25

Sample 9401 FY 2005 Project: 05-0926
Extractables Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4SD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

500

U

UG/KG

bis(2-Chloroethyl) Ether

500

U

UG/KG

Anthracene

500

UJ

UG/KG

Benzaldehyde

500

U

UG/KG

Carbazole

500

U

UG/KG

Hexachloroethane

500

U

UG/KG

Di-n-Butylphthalate

500

U

UG/KG

bis(2-Chloroisopropyl) Ether

500

U

UG/KG

Fluoranthene

500

U

UG/KG

n-Nitroso di-n-Propylamine

500

U

UG/KG

Pyrene

500

U

UG/KG

Acetophenone

500

U

UG/KG

Benzyl Butyl Phthalate

500

U

UG/KG

Nitrobenzene

500

U

UG/KG

bis(2-Ethylhexyl) Phthalate

500

U

UG/KG

Hexachlorobutadiene

500

U

UG/KG

Benzo(a)Anthracene

500

U

UG/KG

Caprolactam

500

U

UG/KG

Chrysene

500

U

UG/KG

2-Methylnaphthalene

500

U

UG/KG

3,3'-Dichlorobenzidine

500

U

UG/KG

1,2,4-T richlorobenzene

500

U

UG/KG

Di-n-Octylphthalate

500

U

UG/KG

Naphthalene

500

U

UG/KG

Benzo(b)Fluoranthene

500

U

UG/KG

4-Chloroaniline

500

U

UG/KG

Benzo(k)Fluoranthene

500

U

UG/KG

bis(2-Chloroethoxy)Methane

500

U

UG/KG

Benzo-a-Pyrene

500

U

UG/KG

Isophorone

500

U

UG/KG

Indeno (1,2,3-cd) Pyrene

500

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

500

U

UG/KG

Dibenzo(a,h)Anthracene

500

U

UG/KG

1,1 -Biphenyl

500

U

UG/KG

Benzo(ghi)Perylene

500

u

UG/KG

2-Chloronaphthalene

500

U

UG/KG

2-Chlorophenol

500

u

UG/KG

2-Nitroaniline

500

U

UG/KG

2-Methylphenol

500

u

UG/KG

Acenaphthylene

500

U

UG/KG

(3-and/or 4-)Methylphenol

500

u

UG/KG

Acenaphthene

500

U

UG/KG

2-Nitrophenol

500

u

UG/KG

Dimethyl Phthalate

500

U

UG/KG

Phenol

500

u

UG/KG

Dibenzofuran

500

U

UG/KG

2,4-Dimethylphenol

500

u

UG/KG

2,4-Dinitrotoluene

500

u

UG/KG

2,4-Dichlorophenol

500

u

UG/KG

2,6-Dinitrotoluene

500

u

UG/KG

2,4,6-T richlorophenol

500

u

UG/KG

3-Nitroaniline

500

u

UG/KG

2,4,5-Trichlorophenol

500

u

UG/KG

4-Chlorophenyl Phenyl Ether

500

u

UG/KG

4-Chloro-3-Methylphenol

500

u

UG/KG

4-Nitroaniline

990

UJ

UG/KG

2,4-Dinitrophenol

500

u

UG/KG

Fluorene

990

u

UG/KG

2-Methyl-4,6-Dinitrophenol

500

u

UG/KG

Diethyl Phthalate

990

u

UG/KG

Pentachlorophenol

500

u

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

990

u

UG/KG

4-Nitrophenol

500

u

UG/KG

Hexachlorobenzene (HCB)

500

u

UG/KG

2,3,4,6-Tetrachlorophenol

500

u

UG/KG

Atrazine

33.67



%

% Moisture

500

u

UG/KG

4-Bromophenyl Phenyl Ether









500

u

UG/KG

Phenanthrene









Produced by: Muse, Janet
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

J- due to RSD >20% on ICAL for Benzaldehyde
J-qualified due to QC Limits Exceeded for 2,4-Dinitrophenol

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/04/2005 09:54

Sample 9443 FY 2005 Project: 05-0926
Extractables Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1 DSD/

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

400

U

UG/KG

bis(2-Chloroethyl) Ether

400

U

UG/KG

Anthracene

400

U

UG/KG

Benzaldehyde

400

UJ

UG/KG

Carbazole

400

U

UG/KG

Hexachloroethane

400

U

UG/KG

Di-n-Butylphthalate

400

U

UG/KG

bis(2-Chloroisopropyl) Ether

400

U

UG/KG

Fluoranthene

400

U

UG/KG

n-Nitroso di-n-Propylamine

400

U

UG/KG

Pyrene

400

U

UG/KG

Acetophenone

400

U

UG/KG

Benzyl Butyl Phthalate

400

U

UG/KG

Nitrobenzene

400

U

UG/KG

bis(2-Ethylhexyl) Phthalate

400

U

UG/KG

Hexachlorobutadiene

400

U

UG/KG

Benzo(a)Anthracene

400

U

UG/KG

Caprolactam

400

U

UG/KG

Chrysene

400

U

UG/KG

2-Methylnaphthalene

400

U

UG/KG

3,3'-Dichlorobenzidine

400

U

UG/KG

1,2,4-T richlorobenzene

400

U

UG/KG

Di-n-Octylphthalate

400

U

UG/KG

Naphthalene

400

U

UG/KG

Benzo(b)Fluoranthene

400

U

UG/KG

4-Chloroaniline

400

U

UG/KG

Benzo(k)Fluoranthene

400

U

UG/KG

bis(2-Chloroethoxy)Methane

400

U

UG/KG

Benzo-a-Pyrene

400

U

UG/KG

Isophorone

400

U

UG/KG

Indeno (1,2,3-cd) Pyrene

400

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

400

U

UG/KG

Dibenzo(a,h)Anthracene

400

U

UG/KG

1,1 -Biphenyl

400

U

UG/KG

Benzo(ghi)Perylene

400

u

UG/KG

2-Chloronaphthalene

400

U

UG/KG

2-Chlorophenol

400

u

UG/KG

2-Nitroaniline

400

U

UG/KG

2-Methylphenol

400

u

UG/KG

Acenaphthylene

400

U

UG/KG

(3-and/or 4-)Methylphenol

400

u

UG/KG

Acenaphthene

400

U

UG/KG

2-Nitrophenol

400

UJ

UG/KG

Dimethyl Phthalate

400

U

UG/KG

Phenol

400

u

UG/KG

Dibenzofuran

400

u

UG/KG

2,4-Dimethylphenol

400

u

UG/KG

2,4-Dinitrotoluene

400

u

UG/KG

2,4-Dichlorophenol

400

u

UG/KG

2,6-Dinitrotoluene

400

u

UG/KG

2,4,6-T richlorophenol

400

u

UG/KG

3-Nitroaniline

400

u

UG/KG

2,4,5-Trichlorophenol

400

u

UG/KG

4-Chlorophenyl Phenyl Ether

400

u

UG/KG

4-Chloro-3-Methylphenol

400

u

UG/KG

4-Nitroaniline

790

UJ

UG/KG

2,4-Dinitrophenol

400

u

UG/KG

Fluorene

790

u

UG/KG

2-Methyl-4,6-Dinitrophenol

400

u

UG/KG

Diethyl Phthalate

790

u

UG/KG

Pentachlorophenol

400

u

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

790

u

UG/KG

4-Nitrophenol

400

u

UG/KG

Hexachlorobenzene (HCB)

400

u

UG/KG

2,3,4,6-Tetrachlorophenol

400

UJ

UG/KG

Atrazine

20.62



%

% Moisture

400

u

UG/KG

4-Bromophenyl Phenyl Ether









400

u

UG/KG

Phenanthrene









Produced by: Revell, Dennis
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

J-qualified for low recovery in CCV for Dimethylphthalate, Atrazine, Carbazole
J-qualified due to QC Limits Exceeded for 2,4-Dinitrophenol

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
EXTRACTABLES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/04/2005 09:54

Sample 9445 FY 2005 Project: 05-0926
Extractables Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1SD/

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

410

U

UG/KG

bis(2-Chloroethyl) Ether

410

U

UG/KG

Anthracene

410

U

UG/KG

Benzaldehyde

410

UJ

UG/KG

Carbazole

410

U

UG/KG

Hexachloroethane

410

U

UG/KG

Di-n-Butylphthalate

410

U

UG/KG

bis(2-Chloroisopropyl) Ether

410

U

UG/KG

Fluoranthene

410

U

UG/KG

n-Nitroso di-n-Propylamine

410

U

UG/KG

Pyrene

410

U

UG/KG

Acetophenone

410

U

UG/KG

Benzyl Butyl Phthalate

410

U

UG/KG

Nitrobenzene

410

U

UG/KG

bis(2-Ethylhexyl) Phthalate

410

U

UG/KG

Hexachlorobutadiene

410

U

UG/KG

Benzo(a)Anthracene

410

U

UG/KG

Caprolactam

410

U

UG/KG

Chrysene

410

U

UG/KG

2-Methylnaphthalene

410

U

UG/KG

3,3'-Dichlorobenzidine

410

U

UG/KG

1,2,4-T richlorobenzene

410

U

UG/KG

Di-n-Octylphthalate

410

U

UG/KG

Naphthalene

410

U

UG/KG

Benzo(b)Fluoranthene

410

U

UG/KG

4-Chloroaniline

410

U

UG/KG

Benzo(k)Fluoranthene

410

U

UG/KG

bis(2-Chloroethoxy)Methane

410

U

UG/KG

Benzo-a-Pyrene

410

U

UG/KG

Isophorone

410

U

UG/KG

Indeno (1,2,3-cd) Pyrene

410

U

UG/KG

Hexachlorocyclopentadiene (HCCP)

410

U

UG/KG

Dibenzo(a,h)Anthracene

410

U

UG/KG

1,1 -Biphenyl

410

U

UG/KG

Benzo(ghi)Perylene

410

U

UG/KG

2-Chloronaphthalene

410

U

UG/KG

2-Chlorophenol

410

U

UG/KG

2-Nitroaniline

410

U

UG/KG

2-Methylphenol

410

U

UG/KG

Acenaphthylene

410

U

UG/KG

(3-and/or 4-)Methylphenol

410

U

UG/KG

Acenaphthene

410

U

UG/KG

2-Nitrophenol

410

UJ

UG/KG

Dimethyl Phthalate

410

U

UG/KG

Phenol

410

u

UG/KG

Dibenzofuran

410

U

UG/KG

2,4-Dimethylphenol

410

u

UG/KG

2,4-Dinitrotoluene

410

U

UG/KG

2,4-Dichlorophenol

410

u

UG/KG

2,6-Dinitrotoluene

410

u

UG/KG

2,4,6-T richlorophenol

410

u

UG/KG

3-Nitroaniline

410

u

UG/KG

2,4,5-Trichlorophenol

410

u

UG/KG

4-Chlorophenyl Phenyl Ether

410

u

UG/KG

4-Chloro-3-Methylphenol

410

u

UG/KG

4-Nitroaniline

820

UJ

UG/KG

2,4-Dinitrophenol

410

u

UG/KG

Fluorene

820

u

UG/KG

2-Methyl-4,6-Dinitrophenol

410

u

UG/KG

Diethyl Phthalate

820

u

UG/KG

Pentachlorophenol

410

u

UG/KG

n-Nitrosodiphenylamine/Diphenylamine

820

u

UG/KG

4-Nitrophenol

410

u

UG/KG

Hexachlorobenzene (HCB)

410

u

UG/KG

2,3,4,6-Tetrachlorophenol

410

UJ

UG/KG

Atrazine

19.98



%

% Moisture

410

u

UG/KG

4-Bromophenyl Phenyl Ether









410

u

UG/KG

Phenanthrene









Produced by: Revell, Dennis
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

J-qualified for low recovery in CCV for Dimethylphthalate, Atrazine, Carbazole
J-qualified due to QC Limits Exceeded for 2,4-Dinitrophenol

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/14/2005 19:26

Sample 9397 FY 2005 Project: 05-0926

Produced by: Scifres, Jenny

Metals Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/27/2005 11:30

Program: WQU

Ending:

Id/Station: BC2SD /

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

0.50 U

MG/KG

Silver

6.4

MG/KG

Arsenic

130

MG/KG

Barium

0.82

MG/KG

Beryllium

1.1

MG/KG

Cadmium

4.6

MG/KG

Cobalt

21

MG/KG

Chromium

20

MG/KG

Copper

1.6 U

MG/KG

Molybdenum

8.4

MG/KG

Nickel

36

MG/KG

Lead

0.50 U

MG/KG

Antimony

1.0 U

MG/KG

Selenium

NA

MG/KG

Tin

57

MG/KG

Strontium

17

MG/KG

Titanium

0.50 U

MG/KG

Thallium

24

MG/KG

Vanadium

12

MG/KG

Yttrium

140

MG/KG

Zinc

0.078

MG/KG

Total Mercury

8200

MG/KG

Aluminum

450

MG/KG

Manganese

7400

MG/KG

Calcium

5100

MG/KG

Magnesium

17000

MG/KG

Iron

18000

MG/KG

Sodium

2300

MG/KG

Potassium

60

%

% Moisture

Per Cent Moisture Determined at 60 Degrees Celsius.

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/14/2005 19:26

Sample 9400 FY 2005 Project: 05-0926
Metals Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4DSD /

Media: SEDIMENT

Produced by: Scifres, Jenny
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 13:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

0.50 U

MG/KG

Silver

1.2

MG/KG

Arsenic

27

MG/KG

Barium

0.30

MG/KG

Beryllium

1.5

MG/KG

Cadmium

0.59

MG/KG

Cobalt

7.2

MG/KG

Chromium

4.7

MG/KG

Copper

1.6 U

MG/KG

Molybdenum

2.4

MG/KG

Nickel

4.8

MG/KG

Lead

0.50 U

MG/KG

Antimony

1.0 U

MG/KG

Selenium

NA

MG/KG

Tin

59

MG/KG

Strontium

12

MG/KG

Titanium

0.50 U

MG/KG

Thallium

6.1

MG/KG

Vanadium

2.7

MG/KG

Yttrium

48

MG/KG

Zinc

0.044 U

MG/KG

Total Mercury

2600

MG/KG

Aluminum

26

MG/KG

Manganese

4900

MG/KG

Calcium

1800

MG/KG

Magnesium

3400

MG/KG

Iron

8500

MG/KG

Sodium

510

MG/KG

Potassium

41

%

% Moisture

Per Cent Moisture Determined at 60 Degrees Celsius.

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/14/2005 19:26

Sample 9401 FY 2005 Project: 05-0926
Metals Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4SD /

Media: SEDIMENT

Produced by: Scifres, Jenny
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

0.50 U

MG/KG

Silver

0.87

MG/KG

Arsenic

57

MG/KG

Barium

0.30

MG/KG

Beryllium

1.8

MG/KG

Cadmium

0.66

MG/KG

Cobalt

9.7

MG/KG

Chromium

5.5

MG/KG

Copper

1.6 U

MG/KG

Molybdenum

2.7

MG/KG

Nickel

5.9

MG/KG

Lead

0.50 U

MG/KG

Antimony

1.0 U

MG/KG

Selenium

NA

MG/KG

Tin

66

MG/KG

Strontium

14

MG/KG

Titanium

0.50 U

MG/KG

Thallium

7.3

MG/KG

Vanadium

2.5

MG/KG

Yttrium

55

MG/KG

Zinc

0.044 U

MG/KG

Total Mercury

3000

MG/KG

Aluminum

26

MG/KG

Manganese

4700

MG/KG

Calcium

1700

MG/KG

Magnesium

3200

MG/KG

Iron

5900

MG/KG

Sodium

450

MG/KG

Potassium

49 A

%

% Moisture

Per Cent Moisture Determined at 60 Degrees Celsius.

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/14/2005 19:26

Sample 9443 FY 2005 Project: 05-0926
Metals Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1 DSD/

Media: SEDIMENT

Produced by: Scifres, Jenny
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

0.50

U

MG/KG

Silver

0.25

U

MG/KG

Arsenic

1.7

A

MG/KG

Barium

0.30

U

MG/KG

Beryllium

0.12

U

MG/KG

Cadmium

0.50

U

MG/KG

Cobalt

0.50

U

MG/KG

Chromium

2.0

UJ

MG/KG

Copper

5.2

U

MG/KG

Molybdenum

0.99

U

MG/KG

Nickel

2.1

A

MG/KG

Lead

0.25

U

MG/KG

Antimony

0.50

U

MG/KG

Selenium



NA

MG/KG

Tin

1.5

A

MG/KG

Strontium

2.6

AJ

MG/KG

Titanium

0.25

U

MG/KG

Thallium

2.0

UJ

MG/KG

Vanadium

0.30

U

MG/KG

Yttrium

1.6

A

MG/KG

Zinc

0.045

U

MG/KG

Total Mercury

180

A

MG/KG

Aluminum

1.7

A

MG/KG

Manganese

71

A

MG/KG

Calcium

200

A

MG/KG

Magnesium

270

A

MG/KG

Iron

1300

A

MG/KG

Sodium

99

U

MG/KG

Potassium

23



%

% Moisture

Per Cent Moisture Determined at 60 Degrees Celsius.	Quantitation limit estimated for Cu and V

LCS Precision outside Method Acceptance Criteria for Ti.

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
METALS SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/14/2005 19:26

Sample 9445 FY 2005 Project: 05-0926
Metals Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1SD/

Media: SEDIMENT

Produced by: Scifres, Jenny
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

0.50

U

MG/KG

Silver

0.25

U

MG/KG

Arsenic

1.0



MG/KG

Barium

0.30

U

MG/KG

Beryllium

0.12

U

MG/KG

Cadmium

0.50

U

MG/KG

Cobalt

0.50

U

MG/KG

Chromium

2.0

UJ

MG/KG

Copper

5.2

U

MG/KG

Molybdenum

1.0

U

MG/KG

Nickel

1.3



MG/KG

Lead

0.25

U

MG/KG

Antimony

0.50

U

MG/KG

Selenium



NA

MG/KG

Tin

1.1



MG/KG

Strontium

2.8

J

MG/KG

Titanium

0.25

U

MG/KG

Thallium

2.0

UJ

MG/KG

Vanadium

0.30

U

MG/KG

Yttrium

1.9



MG/KG

Zinc

0.044

U

MG/KG

Total Mercury

210



MG/KG

Aluminum

2.5



MG/KG

Manganese

50



MG/KG

Calcium

120



MG/KG

Magnesium

370



MG/KG

Iron

540



MG/KG

Sodium

100

U

MG/KG

Potassium

20



%

% Moisture

Per Cent Moisture Determined at 60 Degrees Celsius.	Quantitation limit estimated for Cu and V

LCS Precision outside Method Acceptance Criteria for Ti.

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/04/2005 20:57

Sample 9397 FY 2005 Project: 05-0926
Pesticides Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC2SD /

Media: SEDIMENT

Produced by: Revells, Lavon
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

11

U

UG/KG

Aldrin

11

U

UG/KG

Heptachlor

11

U

UG/KG

Heptachlor Epoxide

11

U

UG/KG

alpha-BHC

00
CM

U

UG/KG

beta-BHC

11

U

UG/KG

gamma-BHC (Lindane)

11

U

UG/KG

delta-BHC

11

U

UG/KG

Endosulfan I (alpha)

11

U

UG/KG

Dieldrin

41

U

UG/KG

4,4'-DDT (p,p'-DDT)

11

U

UG/KG

4,4'-DDE (p,p'-DDE)

27

U

UG/KG

4,4'-DDD (p.p'-DDD)

27

U

UG/KG

Endrin

27

U

UG/KG

Endosulfan II (beta)

27

U

UG/KG

Endosulfan Sulfate

1080

U

UG/KG

Toxaphene

11

U

UG/KG

Chlordene /2

11

U

UG/KG

gamma-Chlordane /2

11

U

UG/KG

trans-Nonachlor /2

11

U

UG/KG

alpha-Chlordane /2

11

U

UG/KG

cis-Nonachlor /2

54

U

UG/KG

Methoxychlor

35

U

UG/KG

Endrin Ketone

64



%

% Moisture

P.P-DDT reported MQL raised above requested MQL because of Matrix interference
Other pesticide results above requested MQL due to low sample dry weight

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/06/2005 14:05

Sample 9397 FY 2005 Project: 05-0926

Produced by: Revells, Lavon

PCB Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/27/2005 11:30

Program: WQU

Ending:

Id/Station: BC2SD /

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE





100

UJ

UG/KG

PCB-1242

(Aroclor

1242)

100

UJ

UG/KG

PCB-1254

(Aroclor

1254)

100

UJ

UG/KG

PCB-1221

(Aroclor

1221)

100

UJ

UG/KG

PCB-1232

(Aroclor

1232)

100

UJ

UG/KG

PCB-1248

(Aroclor

1248)

100

UJ

UG/KG

PCB-1260

(Aroclor

1260)

100

UJ

UG/KG

PCB-1016

(Aroclor

1016)

64



%

% Moisture



QC limits for surrogate exceeded

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/04/2005 20:57

Sample 9400 FY 2005 Project: 05-0926
Pesticides Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4DSD /

Media: SEDIMENT

Produced by: Revells, Lavon
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 13:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

5.7

U

UG/KG

Aldrin

6.8

U

UG/KG

Heptachlor

5.7

U

UG/KG

Heptachlor Epoxide

5.7

U

UG/KG

alpha-BHC

5.7

U

UG/KG

beta-BHC

5.7

U

UG/KG

gamma-BHC (Lindane)

5.7

U

UG/KG

delta-BHC

5.7

U

UG/KG

Endosulfan I (alpha)

5.7

U

UG/KG

Dieldrin

14

U

UG/KG

4,4'-DDT (p,p'-DDT)

5.7

U

UG/KG

4,4'-DDE (p,p'-DDE)

14

U

UG/KG

4,4'-DDD (p.p'-DDD)

14

U

UG/KG

Endrin

14

U

UG/KG

Endosulfan II (beta)

14

U

UG/KG

Endosulfan Sulfate

570

U

UG/KG

Toxaphene

5.7

U

UG/KG

Chlordene /2

5.7

U

UG/KG

gamma-Chlordane /2

5.7

U

UG/KG

trans-Nonachlor /2

5.7

U

UG/KG

alpha-Chlordane /2

5.7

U

UG/KG

cis-Nonachlor /2

28

U

UG/KG

Methoxychlor

18

U

UG/KG

Endrin Ketone

30



%

% Moisture

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/06/2005 14:05

Sample 9400 FY 2005 Project: 05-0926

Produced by: Revells, Lavon

PCB Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/27/2005 13:00

Program: WQU

Ending:

Id/Station: BC4DSD /

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE





100

u

UG/KG

PCB-1242

(Aroclor

1242)

100

u

UG/KG

PCB-1254

(Aroclor

1254)

100

u

UG/KG

PCB-1221

(Aroclor

1221)

100

u

UG/KG

PCB-1232

(Aroclor

1232)

100

u

UG/KG

PCB-1248

(Aroclor

1248)

100

u

UG/KG

PCB-1260

(Aroclor

1260)

100

u

UG/KG

PCB-1016

(Aroclor

1016)

30



%

% Moisture



U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/04/2005 20:57

Sample 9401 FY 2005 Project: 05-0926
Pesticides Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4SD /

Media: SEDIMENT

Produced by: Revells, Lavon
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

6.0

U

UG/KG

Aldrin

6.8

U

UG/KG

Heptachlor

6.0

U

UG/KG

Heptachlor Epoxide

6.0

U

UG/KG

alpha-BHC

6.0

U

UG/KG

beta-BHC

6.0

U

UG/KG

gamma-BHC (Lindane)

6.0

U

UG/KG

delta-BHC

6.0

U

UG/KG

Endosulfan I (alpha)

6.0

U

UG/KG

Dieldrin

15

U

UG/KG

4,4'-DDT (p,p'-DDT)

6.0

U

UG/KG

4,4'-DDE (p,p'-DDE)

15

U

UG/KG

4,4'-DDD (p.p'-DDD)

15

U

UG/KG

Endrin

15

U

UG/KG

Endosulfan II (beta)

15

U

UG/KG

Endosulfan Sulfate

600

U

UG/KG

Toxaphene

6.0

U

UG/KG

Chlordene /2

6.0

U

UG/KG

gamma-Chlordane /2

6.0

U

UG/KG

trans-Nonachlor /2

6.0

U

UG/KG

alpha-Chlordane /2

6.0

U

UG/KG

cis-Nonachlor /2

30

U

UG/KG

Methoxychlor

19

U

UG/KG

Endrin Ketone

34



%

% Moisture

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/06/2005 14:05

Sample 9401 FY 2005 Project: 05-0926

Produced by: Revells, Lavon

PCB Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/27/2005 12:40

Program: WQU

Ending:

Id/Station: BC4SD /

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE





100

U

UG/KG

PCB-1242

(Aroclor

1242)

100

U

UG/KG

PCB-1254

(Aroclor

1254)

100

U

UG/KG

PCB-1221

(Aroclor

1221)

100

U

UG/KG

PCB-1232

(Aroclor

1232)

100

U

UG/KG

PCB-1248

(Aroclor

1248)

100

u

UG/KG

PCB-1260

(Aroclor

1260)

100

u

UG/KG

PCB-1016

(Aroclor

1016)

34



%

% Moisture



U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/07/2005 17:22

Sample 9443 FY 2005 Project: 05-0926

Produced by: Revells, Lavon

PCB Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/28/2005 14:30

Program: WQU

Ending:

Id/Station: ER1 DSD/

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE





100

u

UG/KG

PCB-1242

(Aroclor

1242)

100

u

UG/KG

PCB-1254

(Aroclor

1254)

100

u

UG/KG

PCB-1221

(Aroclor

1221)

100

u

UG/KG

PCB-1232

(Aroclor

1232)

100

u

UG/KG

PCB-1248

(Aroclor

1248)

100

u

UG/KG

PCB-1260

(Aroclor

1260)

100

u

UG/KG

PCB-1016

(Aroclor

1016)

21



%

% Moisture



U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/10/2005 11:30

Sample 9443 FY 2005 Project: 05-0926
Pesticides Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1 DSD/

Media: SEDIMENT

Produced by: Revells, Lavon
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4.1

U

UG/KG

Aldrin

4.1

U

UG/KG

Heptachlor

4.1

U

UG/KG

Heptachlor Epoxide

4.1

U

UG/KG

alpha-BHC

4.1

U

UG/KG

beta-BHC

4.1

U

UG/KG

gamma-BHC (Lindane)

4.1

U

UG/KG

delta-BHC

4.1

U

UG/KG

Endosulfan I (alpha)

4.1

U

UG/KG

Dieldrin

10

U

UG/KG

4,4'-DDT (p,p'-DDT)

4.1

U

UG/KG

4,4'-DDE (p,p'-DDE)

10

U

UG/KG

4,4'-DDD (p.p'-DDD)

10

U

UG/KG

Endrin

10

U

UG/KG

Endosulfan II (beta)

10

U

UG/KG

Endosulfan Sulfate

410

U

UG/KG

Toxaphene

4.1

U

UG/KG

Chlordene /2

4.1

U

UG/KG

gamma-Chlordane /2

4.1

U

UG/KG

trans-Nonachlor /2

4.1

U

UG/KG

alpha-Chlordane /2

4.1

U

UG/KG

cis-Nonachlor /2

23

U

UG/KG

Methoxychlor

10

U

UG/KG

Endrin Ketone

21



%

% Moisture

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS	EPA - REGION IV SESD, ATHENS, GA	Production Date: 10/07/2005 17:22

Sample 9445 FY 2005 Project: 05-0926

Produced by: Revells, Lavon

PCB Scan

Requestor: MDEQ

Project Leader: MKOENIG

Facility: Mississippi Gulf Coast Monitoring Study

Beginning: 09/28/2005 14:00

Program: WQU

Ending:

Id/Station: ER1SD/

Media: SEDIMENT

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE





100

u

UG/KG

PCB-1242

(Aroclor

1242)

100

u

UG/KG

PCB-1254

(Aroclor

1254)

100

u

UG/KG

PCB-1221

(Aroclor

1221)

100

u

UG/KG

PCB-1232

(Aroclor

1232)

100

u

UG/KG

PCB-1248

(Aroclor

1248)

100

u

UG/KG

PCB-1260

(Aroclor

1260)

100

u

UG/KG

PCB-1016

(Aroclor

1016)

20



%

% Moisture



U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
PESTICIDES/PCB SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/10/2005 11:30

Sample 9445 FY 2005 Project: 05-0926
Pesticides Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1SD/

Media: SEDIMENT

Produced by: Revells, Lavon
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

RESULTS

UNITS

ANALYTE

4.1

U

UG/KG

Aldrin

4.1

U

UG/KG

Heptachlor

4.1

U

UG/KG

Heptachlor Epoxide

4.1

U

UG/KG

alpha-BHC

4.1

U

UG/KG

beta-BHC

4.1

U

UG/KG

gamma-BHC (Lindane)

4.1

U

UG/KG

delta-BHC

4.1

U

UG/KG

Endosulfan I (alpha)

4.1

U

UG/KG

Dieldrin

10

U

UG/KG

4,4'-DDT (p,p'-DDT)

4.1

U

UG/KG

4,4'-DDE (p,p'-DDE)

10

U

UG/KG

4,4'-DDD (p.p'-DDD)

10

U

UG/KG

Endrin

10

U

UG/KG

Endosulfan II (beta)

10

U

UG/KG

Endosulfan Sulfate

410

U

UG/KG

Toxaphene

4.1

U

UG/KG

Chlordene /2

4.1

U

UG/KG

gamma-Chlordane /2

4.1

U

UG/KG

trans-Nonachlor /2

4.1

U

UG/KG

alpha-Chlordane /2

4.1

U

UG/KG

cis-Nonachlor /2

21

U

UG/KG

Methoxychlor

10

U

UG/KG

Endrin Ketone

20



%

% Moisture

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane	rage 1 OT 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/13/2005 14:12

Sample 9397 FY 2005 Project: 05-0926
Volatiles Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC2SD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

3.9 U

UG/KG

Dichlorodifluoromethane

3.9

U

UG/KG

cis-1,3-Dichloropropene

3.9 U

UG/KG

Chloromethane

19

U

UG/KG

Bromoform

3.9 U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

3.9

U

UG/KG

Bromobenzene

3.9 U

UG/KG

Methyl T-Butyl Ether (MTBE)

3.9

U

UG/KG

1,1,2,2-Tetrachloroethane

3.9 U

UG/KG

Bromomethane

3.9

U

UG/KG

Tetrachloroethene (Tetrachloroethylene)

3.9 U

UG/KG

Cyclohexane

3.9

U

UG/KG

1,3-Dichloropropane

3.9 U

UG/KG

Vinyl Chloride

3.9

U

UG/KG

Methyl Butyl Ketone

3.9 U

UG/KG

Chloroethane

3.9

U

UG/KG

Toluene

3.9 U

UG/KG

Trichlorofluoromethane (Freon 11)

3.9

U

UG/KG

Chlorobenzene

3.9 U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

3.9

U

UG/KG

1,1,1,2-Tetrachloroethane

3.9 U

UG/KG

Methylene Chloride

3.9

U

UG/KG

Ethyl Benzene

39 U

UG/KG

Acetone

7.7

U

UG/KG

(m- and/or p-)Xylene

4.7 J

UG/KG

Carbon Disulfide

3.9

U

UG/KG

o-Xylene

3.9 U

UG/KG

Methyl Acetate

3.9

U

UG/KG

Styrene

3.9 U

UG/KG

1,1-Dichloroethane

7.7

U

UG/KG

1,2,3-Trichloropropane

3.9 U

UG/KG

cis-1,2-Dichloroethene

3.9

U

UG/KG

o-Chlorotoluene

3.9 U

UG/KG

2,2-Dichloropropane

7.7

U

UG/KG

p-Chlorotoluene

7.7 U

UG/KG

Methyl Ethyl Ketone

7.7

U

UG/KG

1,3-Dichlorobenzene

3.9 U

UG/KG

Bromochloromethane

7.7

U

UG/KG

1,4-Dichlorobenzene

19 U

UG/KG

trans-1,2-Dichloroethene

3.9

U

UG/KG

1,2-Dichlorobenzene

3.9 U

UG/KG

Chloroform

3.9

U

UG/KG

1,2-Dibromoethane (EDB)

3.9 U

UG/KG

1,2-Dichloroethane

14



UG/KG

Isopropylbenzene

3.9 U

UG/KG

1,1,1-Trichloroethane

51

J

UG/KG

n-Propylbenzene

3.9 U

UG/KG

1,1-Dichloropropene

3.9

U

UG/KG

1,3,5-Trimethylbenzene

3.9 U

UG/KG

Carbon Tetrachloride

3.9

U

UG/KG

tert-Butylbenzene

3.9 U

UG/KG

Bromodichloromethane

3.9

U

UG/KG

1,2,4-T rimethylbenzene

3.9 U

UG/KG

Methyl Isobutyl Ketone

30

J

UG/KG

sec-Butylbenzene

3.9 U

UG/KG

1,2-Dichloropropane

43

J

UG/KG

p-lsopropyltoluene

3.9 U

UG/KG

Methylcyclohexane

50

J

UG/KG

n-Butylbenzene

3.9 U

UG/KG

Dibromomethane

19

U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

3.9 U

UG/KG

trans-1,3-Dichloropropene

7.7

U

UG/KG

1,2,4-T richlorobenzene

3.9 U

UG/KG

Trichloroethene (Trichloroethylene)

3.9

u

UG/KG

Hexachloro-1,3-Butadiene

0.23 J

UG/KG

Benzene

1.8

J

UG/KG

1,2,3-Trichlorobenzene

3.9 U

UG/KG

Dibromochloromethane

60



%

% Moisture

3.9 U

UG/KG

1,1,2-Trichloroethane









Produced by: Hale, Same
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 11:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

Benzene and 1,2,3-trichlorobenzene results >MDL but 
-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 12:45

Sample 9397 FY 2005 Project: 05-0926

MISCELLANEOUS COMPOUNDS

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC2SD /

Media: SEDIMENT

RESULTS UNITS ANALYTE

N UG/KG Petroleum Products

Produced by: Hale, Sallie
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 11:30
Ending:

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/13/2005 14:12

Sample 9400 FY 2005 Project: 05-0926
Volatiles Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4DSD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

2.3 U

UG/KG

Dichlorodifluoromethane

2.3 U

UG/KG

cis-1,3-Dichloropropene

2.3 U

UG/KG

Chloromethane

11 U

UG/KG

Bromoform

2.3 U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

2.3 U

UG/KG

Bromobenzene

2.3 U

UG/KG

Methyl T-Butyl Ether (MTBE)

2.3 U

UG/KG

1,1,2,2-Tetrachloroethane

2.3 U

UG/KG

Bromomethane

2.3 U

UG/KG

Tetrachloroethene (Tetrachloroethylene)

2.3 U

UG/KG

Cyclohexane

2.3 U

UG/KG

1,3-Dichloropropane

2.3 U

UG/KG

Vinyl Chloride

2.3 U

UG/KG

Methyl Butyl Ketone

2.3 U

UG/KG

Chloroethane

2.3 U

UG/KG

Toluene

2.3 U

UG/KG

Trichlorofluoromethane (Freon 11)

2.3 U

UG/KG

Chlorobenzene

2.3 U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

2.3 U

UG/KG

1,1,1,2-Tetrachloroethane

2.3 U

UG/KG

Methylene Chloride

2.3 U

UG/KG

Ethyl Benzene

23 U

UG/KG

Acetone

4.6 U

UG/KG

(m- and/or p-)Xylene

3.2

UG/KG

Carbon Disulfide

2.3 U

UG/KG

o-Xylene

2.3 U

UG/KG

Methyl Acetate

2.3 U

UG/KG

Styrene

2.3 U

UG/KG

1,1-Dichloroethane

4.6 U

UG/KG

1,2,3-Trichloropropane

2.3 U

UG/KG

cis-1,2-Dichloroethene

2.3 U

UG/KG

o-Chlorotoluene

2.3 U

UG/KG

2,2-Dichloropropane

4.6 U

UG/KG

p-Chlorotoluene

4.6 U

UG/KG

Methyl Ethyl Ketone

4.6 U

UG/KG

1,3-Dichlorobenzene

2.3 U

UG/KG

Bromochloromethane

4.6 U

UG/KG

1,4-Dichlorobenzene

11 U

UG/KG

trans-1,2-Dichloroethene

2.3 U

UG/KG

1,2-Dichlorobenzene

2.3 U

UG/KG

Chloroform

2.3 U

UG/KG

1,2-Dibromoethane (EDB)

2.3 U

UG/KG

1,2-Dichloroethane

2.3 U

UG/KG

Isopropylbenzene

2.3 U

UG/KG

1,1,1-Trichloroethane

2.3 U

UG/KG

n-Propylbenzene

2.3 U

UG/KG

1,1-Dichloropropene

2.3 U

UG/KG

1,3,5-Trimethylbenzene

2.3 U

UG/KG

Carbon Tetrachloride

2.3 U

UG/KG

tert-Butylbenzene

2.3 U

UG/KG

Bromodichloromethane

2.3 U

UG/KG

1,2,4-T rimethylbenzene

2.3 U

UG/KG

Methyl Isobutyl Ketone

2.3 U

UG/KG

sec-Butylbenzene

2.3 U

UG/KG

1,2-Dichloropropane

2.3 U

UG/KG

p-lsopropyltoluene

2.3 U

UG/KG

Methylcyclohexane

4.6 U

UG/KG

n-Butylbenzene

2.3 U

UG/KG

Dibromomethane

11 U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

2.3 U

UG/KG

trans-1,3-Dichloropropene

4.6 U

UG/KG

1,2,4-T richlorobenzene

2.3 U

UG/KG

Trichloroethene (Trichloroethylene)

2.3 U

UG/KG

Hexachloro-1,3-Butadiene

2.3 U

UG/KG

Benzene

4.6 U

UG/KG

1,2,3-Trichlorobenzene

2.3 U

UG/KG

Dibromochloromethane

41

%

% Moisture

2.3 U

UG/KG

1,1,2-Trichloroethane







Produced by: Hale, Same
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 13:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 12:45

Sample 9400 FY 2005 Project: 05-0926

MISCELLANEOUS COMPOUNDS

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4DSD /

Media: SEDIMENT

RESULTS UNITS ANALYTE

200 NJ UG/KG Thiobismethane

Produced by: Hale, Sallie
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 13:00
Ending:

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/13/2005 14:12

Sample 9401 FY 2005 Project: 05-0926
Volatiles Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: BC4SD /

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

3.3 U

UG/KG

Dichlorodifluoromethane

3.3 U

UG/KG

cis-1,3-Dichloropropene

3.3 U

UG/KG

Chloromethane

16 U

UG/KG

Bromoform

3.3 U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

3.3 U

UG/KG

Bromobenzene

3.3 U

UG/KG

Methyl T-Butyl Ether (MTBE)

3.3 U

UG/KG

1,1,2,2-Tetrachloroethane

3.3 U

UG/KG

Bromomethane

3.3 U

UG/KG

Tetrachloroethene (Tetrachloroethylene)

3.3 U

UG/KG

Cyclohexane

3.3 U

UG/KG

1,3-Dichloropropane

3.3 U

UG/KG

Vinyl Chloride

3.3 U

UG/KG

Methyl Butyl Ketone

3.3 U

UG/KG

Chloroethane

3.3 U

UG/KG

Toluene

3.3 U

UG/KG

Trichlorofluoromethane (Freon 11)

3.3 U

UG/KG

Chlorobenzene

3.3 U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

3.3 U

UG/KG

1,1,1,2-Tetrachloroethane

3.3 U

UG/KG

Methylene Chloride

3.3 U

UG/KG

Ethyl Benzene

33 U

UG/KG

Acetone

6.5 U

UG/KG

(m- and/or p-)Xylene

4.4

UG/KG

Carbon Disulfide

3.3 U

UG/KG

o-Xylene

3.3 U

UG/KG

Methyl Acetate

3.3 U

UG/KG

Styrene

3.3 U

UG/KG

1,1-Dichloroethane

6.5 U

UG/KG

1,2,3-Trichloropropane

3.3 U

UG/KG

cis-1,2-Dichloroethene

3.3 U

UG/KG

o-Chlorotoluene

3.3 U

UG/KG

2,2-Dichloropropane

6.5 U

UG/KG

p-Chlorotoluene

6.5 U

UG/KG

Methyl Ethyl Ketone

6.5 U

UG/KG

1,3-Dichlorobenzene

3.3 U

UG/KG

Bromochloromethane

6.5 U

UG/KG

1,4-Dichlorobenzene

16 U

UG/KG

trans-1,2-Dichloroethene

3.3 U

UG/KG

1,2-Dichlorobenzene

3.3 U

UG/KG

Chloroform

3.3 U

UG/KG

1,2-Dibromoethane (EDB)

3.3 U

UG/KG

1,2-Dichloroethane

3.3 U

UG/KG

Isopropylbenzene

3.3 U

UG/KG

1,1,1-Trichloroethane

3.3 U

UG/KG

n-Propylbenzene

3.3 U

UG/KG

1,1-Dichloropropene

3.3 U

UG/KG

1,3,5-Trimethylbenzene

3.3 U

UG/KG

Carbon Tetrachloride

3.3 U

UG/KG

tert-Butylbenzene

3.3 U

UG/KG

Bromodichloromethane

3.3 U

UG/KG

1,2,4-T rimethylbenzene

3.3 U

UG/KG

Methyl Isobutyl Ketone

3.3 U

UG/KG

sec-Butylbenzene

3.3 U

UG/KG

1,2-Dichloropropane

3.3 U

UG/KG

p-lsopropyltoluene

3.3 U

UG/KG

Methylcyclohexane

6.5 U

UG/KG

n-Butylbenzene

3.3 U

UG/KG

Dibromomethane

16 U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

3.3 U

UG/KG

trans-1,3-Dichloropropene

6.5 U

UG/KG

1,2,4-T richlorobenzene

3.3 U

UG/KG

Trichloroethene (Trichloroethylene)

3.3 U

UG/KG

Hexachloro-1,3-Butadiene

3.3 U

UG/KG

Benzene

6.5 U

UG/KG

1,2,3-Trichlorobenzene

3.3 U

UG/KG

Dibromochloromethane

50

%

% Moisture

3.3 U

UG/KG

1,1,2-Trichloroethane







Produced by: Hale, Same
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/27/2005 12:40
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/13/2005 14:12

Sample 9443 FY 2005 Project: 05-0926
Volatiles Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1 DSD/

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1.2 U

UG/KG

Dichlorodifluoromethane

1.2 U

UG/KG

cis-1,3-Dichloropropene

1.2 U

UG/KG

Chloromethane

5.9 U

UG/KG

Bromoform

1.2 U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

1.2 U

UG/KG

Bromobenzene

1.2 U

UG/KG

Methyl T-Butyl Ether (MTBE)

1.2 U

UG/KG

1,1,2,2-Tetrachloroethane

1.2 U

UG/KG

Bromomethane

1.2 U

UG/KG

Tetrachloroethene (Tetrachloroethylene)

1.2 U

UG/KG

Cyclohexane

1.2 U

UG/KG

1,3-Dichloropropane

1.2 U

UG/KG

Vinyl Chloride

1.2 U

UG/KG

Methyl Butyl Ketone

1.2 U

UG/KG

Chloroethane

1.2 U

UG/KG

Toluene

1.2 U

UG/KG

Trichlorofluoromethane (Freon 11)

1.2 U

UG/KG

Chlorobenzene

1.2 U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

1.2 U

UG/KG

1,1,1,2-Tetrachloroethane

1.2 U

UG/KG

Methylene Chloride

1.2 U

UG/KG

Ethyl Benzene

12 U

UG/KG

Acetone

2.4 U

UG/KG

(m- and/or p-)Xylene

1.2 U

UG/KG

Carbon Disulfide

1.2 U

UG/KG

o-Xylene

1.2 U

UG/KG

Methyl Acetate

1.2 U

UG/KG

Styrene

1.2 U

UG/KG

1,1-Dichloroethane

2.4 U

UG/KG

1,2,3-Trichloropropane

1.2 U

UG/KG

cis-1,2-Dichloroethene

1.2 U

UG/KG

o-Chlorotoluene

1.2 U

UG/KG

2,2-Dichloropropane

2.4 U

UG/KG

p-Chlorotoluene

2.4 U

UG/KG

Methyl Ethyl Ketone

2.4 U

UG/KG

1,3-Dichlorobenzene

1.2 U

UG/KG

Bromochloromethane

2.4 U

UG/KG

1,4-Dichlorobenzene

5.9 U

UG/KG

trans-1,2-Dichloroethene

1.2 U

UG/KG

1,2-Dichlorobenzene

1.2 U

UG/KG

Chloroform

1.2 U

UG/KG

1,2-Dibromoethane (EDB)

1.2 U

UG/KG

1,2-Dichloroethane

1.2 U

UG/KG

Isopropylbenzene

1.2 U

UG/KG

1,1,1-Trichloroethane

1.2 U

UG/KG

n-Propylbenzene

1.2 U

UG/KG

1,1-Dichloropropene

1.2 U

UG/KG

1,3,5-Trimethylbenzene

1.2 U

UG/KG

Carbon Tetrachloride

1.2 U

UG/KG

tert-Butylbenzene

1.2 U

UG/KG

Bromodichloromethane

1.2 U

UG/KG

1,2,4-T rimethylbenzene

1.2 U

UG/KG

Methyl Isobutyl Ketone

1.2 U

UG/KG

sec-Butylbenzene

1.2 U

UG/KG

1,2-Dichloropropane

1.2 U

UG/KG

p-lsopropyltoluene

1.2 U

UG/KG

Methylcyclohexane

2.4 U

UG/KG

n-Butylbenzene

1.2 U

UG/KG

Dibromomethane

5.9 U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

1.2 U

UG/KG

trans-1,3-Dichloropropene

2.4 U

UG/KG

1,2,4-T richlorobenzene

1.2 U

UG/KG

Trichloroethene (Trichloroethylene)

1.2 U

UG/KG

Hexachloro-1,3-Butadiene

1.2 U

UG/KG

Benzene

2.4 U

UG/KG

1,2,3-Trichlorobenzene

1.2 U

UG/KG

Dibromochloromethane

23

%

% Moisture

1.2 U

UG/KG

1,1,2-Trichloroethane







Produced by: Hale, Same
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:30
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
VOLATILES SAMPLE ANALYSIS

EPA - REGION IV SESD, ATHENS, GA

Production Date: 10/07/2005 12:45

Sample 9445 FY 2005 Project: 05-0926
Volatiles Scan

Facility: Mississippi Gulf Coast Monitoring Study
Program: WQU
Id/Station: ER1SD/

Media: SEDIMENT

RESULTS

UNITS

ANALYTE

RESULTS

UNITS

ANALYTE

1.2 U

UG/KG

Dichlorodifluoromethane

1.2 U

UG/KG

cis-1,3-Dichloropropene

1.2 U

UG/KG

Chloromethane

6.3 U

UG/KG

Bromoform

1.2 U

UG/KG

1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)

1.2 U

UG/KG

Bromobenzene

1.2 U

UG/KG

Methyl T-Butyl Ether (MTBE)

1.2 U

UG/KG

1,1,2,2-Tetrachloroethane

1.2 U

UG/KG

Bromomethane

1.2 U

UG/KG

Tetrachloroethene (Tetrachloroethylene)

1.2 U

UG/KG

Cyclohexane

1.2 U

UG/KG

1,3-Dichloropropane

1.2 U

UG/KG

Vinyl Chloride

1.2 U

UG/KG

Methyl Butyl Ketone

1.2 U

UG/KG

Chloroethane

1.2 U

UG/KG

Toluene

1.2 U

UG/KG

Trichlorofluoromethane (Freon 11)

1.2 U

UG/KG

Chlorobenzene

1.2 U

UG/KG

1,1-Dichloroethene (1,1-Dichloroethylene)

1.2 U

UG/KG

1,1,1,2-Tetrachloroethane

1.2 U

UG/KG

Methylene Chloride

1.2 U

UG/KG

Ethyl Benzene

12 U

UG/KG

Acetone

2.5 U

UG/KG

(m- and/or p-)Xylene

1.2 U

UG/KG

Carbon Disulfide

1.2 U

UG/KG

o-Xylene

1.2 U

UG/KG

Methyl Acetate

1.2 U

UG/KG

Styrene

1.2 U

UG/KG

1,1-Dichloroethane

2.5 U

UG/KG

1,2,3-Trichloropropane

1.2 U

UG/KG

cis-1,2-Dichloroethene

1.2 U

UG/KG

o-Chlorotoluene

1.2 U

UG/KG

2,2-Dichloropropane

2.5 U

UG/KG

p-Chlorotoluene

2.5 U

UG/KG

Methyl Ethyl Ketone

2.5 U

UG/KG

1,3-Dichlorobenzene

1.2 U

UG/KG

Bromochloromethane

2.5 U

UG/KG

1,4-Dichlorobenzene

6.3 U

UG/KG

trans-1,2-Dichloroethene

1.2 U

UG/KG

1,2-Dichlorobenzene

1.2 U

UG/KG

Chloroform

1.2 U

UG/KG

1,2-Dibromoethane (EDB)

1.2 U

UG/KG

1,2-Dichloroethane

1.2 U

UG/KG

Isopropylbenzene

1.2 U

UG/KG

1,1,1-Trichloroethane

1.2 U

UG/KG

n-Propylbenzene

1.2 U

UG/KG

1,1-Dichloropropene

1.2 U

UG/KG

1,3,5-Trimethylbenzene

1.2 U

UG/KG

Carbon Tetrachloride

1.2 U

UG/KG

tert-Butylbenzene

1.2 U

UG/KG

Bromodichloromethane

1.2 U

UG/KG

1,2,4-T rimethylbenzene

1.2 U

UG/KG

Methyl Isobutyl Ketone

1.2 U

UG/KG

sec-Butylbenzene

1.2 U

UG/KG

1,2-Dichloropropane

1.2 U

UG/KG

p-lsopropyltoluene

1.2 U

UG/KG

Methylcyclohexane

2.5 U

UG/KG

n-Butylbenzene

1.2 U

UG/KG

Dibromomethane

6.3 U

UG/KG

1,2-Dibromo-3-Chloropropane (DBCP)

1.2 U

UG/KG

trans-1,3-Dichloropropene

2.5 U

UG/KG

1,2,4-T richlorobenzene

1.2 U

UG/KG

Trichloroethene (Trichloroethylene)

1.2 U

UG/KG

Hexachloro-1,3-Butadiene

1.2 U

UG/KG

Benzene

2.5 U

UG/KG

1,2,3-Trichlorobenzene

1.2 U

UG/KG

Dibromochloromethane

20

%

% Moisture

1.2 U

UG/KG

1,1,2-Trichloroethane







Produced by: Hale, Same
Requestor: MDEQ
Project Leader: MKOENIG
Beginning: 09/28/2005 14:00
Ending:

DATA REPORTED ON DRY WEIGHT BASIS

U-Analyte not detected at or above reporting limit. | J-ldentification of analyte is acceptable; reported value is an estimate. | UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.

N-Presumptive evidence analyte is present; analyte reported as tentative identification. | NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.

K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.

L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.

NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is "average" of replicates.

R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.

Page 1 of 1

-------
Data Package Checklist

(Initials do not signify approval)

Reviewer

MASB QA Officer
NAREL QA Coordinator
MASB Chief

Initials	Date

Project: KATRINA RESPONSE-MS

SDG Number: #0500067

Date due:

Analysis: NAREL RA-04

Type of Package:

~ Data Summary Package

~ Complete Package

Y N N/A

Comments

~	~	~	All samples in the SDG are reported

~	~	~	All results are the ones intended

~	~	~	Printed results match the raw data

~	~	~	Error report forms are attached

~	~	~	SDG Form is attached

~	~	~	Analyst's checklist is attached

~	~	~	Original prep batch forms are attached

~	~	~	All supporting data sheets are attached

~	~	~	All raw data sheets appear to be correct

~	~	~	All handwritten notes are initialed and dated

~	~	~	Package is arranged correctly

~	~	~	Package appears to be complete

Were holding times met?	~ Yes ~ No ~ N/A

Were all QC results acceptable? ~ Yes ~ No
Are there any exceptions to report? ~ Yes ~ No

Prepared by:

Q AO Review

Y	N	N/A

~	~	~	All QC failures are noted

~	~	~	Raw data look reasonable

~	~	~	All exceptions have been noted

Note: If changes to the case
narrative are suggested, please
provide the necessary language.

Comments:

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

REPORT OF SAMPLE DELIV ERY GROUP #0500067

Project:	KATRINA RESPONSE-MS

Analysis Procedure: Radium-226 in Environmental Matrices
Date Reported:	11/17/2005

SAMPLES

NAREL
Sample #

Client Sample ID

Type

Matrix

Date

Collected

Date
Received

A5.04976C

CFMSD03

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04977D

CFMSD04

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04978E

CFMSD05

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04979F

CFMSD05D

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04980Y

CFMSD06

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04981Z

CFMSD07

SAM

SEDIMENT

10/06/2005

10/07/2005

EXCEPTIONS

1.	Packaging and Shipping - No problems were observed.

2.	Documentation - No problems were observed.

3.	Sample Preparation - No problems were encountered.

4.	Analysis - No problems were encountered.

5.	Holding Times - All holding times were met.

QUALITY CONTROL

1.	QC samples - All QC analysis results met NAREL acceptance criteria except the matrix spike result.

2.	Instruments - Response and background checks for all instruments used in these analyses met NAREL
acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as
noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and
Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the
following signatures.

Mary F. Wisdom	Date

Quality Assurance Coordinator

John Griggs. Ph.D.	Date

Chief. Monitoring and Analytical Services Branch

-------
GENERAL INFORMATION

SAMPLE TYPES

BLD	Blind sample

FBK	Field blank

SAM	Normal sample

ANALYSIS QC TYPES

ANA	Normal analysis

DUP	Laboratory duplicate

LCS	Laboratory control sample (blank spike)

MS	Matrix spike

MSD	Matrix spike duplicate

RBK	Reagent blank

QUALITY INDICATORS

RPD	Relative Percent Difference

%R	Percent Recovery

Z	Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3
standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control
limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard
deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value
by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the
combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the
native sample activity is subtracted from each measured value and the net concentrations arc then converted to total
activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of
measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD. between duplicate results and the "percent recovery." or %R,
for spiked analyses, but docs not use these values for evaluation.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

ANALYSIS SUMMARY

Analysis Procedure: NAREL RA-04

Title:	Radium-226 in Environmental Matrices

NAREL Sample #

QC
Type

Preparation Procedure

Date

Completed

Prep
Batch #

QC

Batch #

A5.04976C



NAREL RA-01

11/10/2005

0010184F

0003928W

A5.04976C

DUP

NAREL RA-01

11/10/2005

0010184F

0003928W

A5.04977D



NAREL RA-01

11/10/2005

0010184F

0003928W

A5.04977D

MS

NAREL RA-01

11/10/2005

0010184F

0003928W

A5.04977D

MSD

NAREL RA-01

11/10/2005

0010184F

0003928W

A5.04978E



NAREL RA-01

11/17/2005

0010197L

0003928W

A5.04979F



NAREL RA-01

11/17/2005

0010197L

0003928W

A5.04980Y



NAREL RA-01

11/17/2005

0010197L

0003928W

A5.04981Z



NAREL RA-01

11/17/2005

0010197L

0003928W

RBK-00496346B *

RBK

NAREL RA-01

11/10/2005

0010184F

0003928W

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

PREPARATION METHOD(S) USED

Procedure ID

Title

NAREL RA-01

Preparing Solid Samples for Ra-226 and Ra-228 Analysis

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04976C

SEDIMENT

SAM

4.935e-01 GASH
44.22 %

92.00 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4E

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2a Uncertainty

MDC

Unit

Date

Ra226

4.90e-01

8.8e-02

2.7e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04976C

SEDIMENT

SAM

5.034e-01 GASH
44.22 %

92.00 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
DUP

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4F

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2a Uncertainty

MDC

Unit

Date

Ra226

6.06e-01

l.le-01

3.9e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04977D

SEDIMENT

SAM

4.977e-01 GASH
75.62 %

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4G

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2a Uncertainty

MDC

Unit

Date

Ra226

5.77e-01

1.0e-01

3.5e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04977D

SEDIMENT

SAM

4.977e-01 GASH
75.62 %

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
MS

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4I

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

2.31e+01

3.5e+00

2.7e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04977D

SEDIMENT

SAM

4.977e-01 GASH
75.62 %

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
MSD

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4K

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

3.25e+01

4.8e+00

3.4e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04978E

SEDIMENT

SAM

4.937e-01 GASH
22.28 %

56.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010197L

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4D

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2a Uncertainty

MDC

Unit

Date

Ra226

7.35e-01

1.2e-01

1.9e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04979F

SEDIMENT

SAM

4.973e-01 GASH
23.14%

66.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010197L

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4E

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

7.42e-() 1

1.2e-01

1.7e-()2

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04980Y

SEDIMENT
SAM

4.974e-01 GASH
50.08 %

82.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010197L

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4G

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2a Uncertainty

MDC

Unit

Date

Ra226

8.82e-01

1.4e-01

3.1e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04981Z

SEDIMENT

SAM

4.981e-01 GASH
59.53 %

85.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010197L

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4I

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

3.72e-01

6.9e-02

2.6e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

QC Sample #: RBK-00496346B

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003928W
0010184F

NAREL RA-01
NAREL RA-04
CHD
RBK

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/09/2005 18:25

1000.0

LC4M

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

3.83e-02

1.3e-02

1.4e-02

PCI

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

QC BATCH SUMMARY

QC batch#:	0003928W

Preparation procedure: NAREL RA-01
Analysis procedure: NAREL RA-04

NAREL Sample #

QC
Type

Yield (%)

± 2a Uncertainty (%)

Analyst

A5.04976C



N/A



CHD

A5.04976C

DUP

N/A



CHD

A5.04977D



N/A



CHD

A5.04977D

MS

N/A



CHD

A5.04977D

MSD

N/A



CHD

A5.04978E



N/A



CHD

A5.04979F



N/A



CHD

A5.04980Y



N/A



CHD

A5.04981Z



N/A



CHD

RBK-00496346B *

RBK

N/A



CHD

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL
Sample #

QC
Type

Aliquot Si/c

Completion
Date

Prep Batch

A5.04976C



4.94e-01 GASH

11/10/2005

0010184F

A5.04976C

DUP

5.03e-01 GASH

11/10/2005

0010184F

A5.04977D



4.98e-01 GASH

11/10/2005

0010184F

A5.04977D

MS

4.98e-01 GASH

11/10/2005

0010184F

A5.04977D

MSD

4.98e-01 GASH

11/10/2005

0010184F

A5.04978E



4.94e-01 GASH

11/17/2005

0010197L

A5.04979F



4.97e-01 GASH

11/17/2005

0010197L

A5.04980Y



4.97e-01 GASH

11/17/2005

0010197L

A5.04981Z



4.98e-01 GASH

11/17/2005

0010197L

RBK-00496346B *

RBK

1.00e+00 SAMP

11/10/2005

0010184F

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500067

DETECTOR REPORT

The following were used for samples in the SDG

LC4D	1 1/16/2005 18:15 00495553C A5.04978E

LC4E	1 1/09/2005 18:25 00495547E A5.04976C

LC4E	1 1/16/2005 18:15 00495556F A5.04979F

LC4F	11/09/2005 18:25 00496343Y A5.04976C

LC4G	1 1/09/2005 18:25 00495550Z A5.04977D

LC4G	1 1/16/2005 18:15 00495559J A5.04980Y

LC4I	1 1/09/2005 18:25 00496344Z A5.04977D

LC4I	1 1/16/2005 18:15 00495563E A5.04981Z

LC4K	11/09/2005 18:25 00496345A A5.04977D

The following were used for other samples in the QC batches

LC4M 11/09/2005 18:25 00496346B

-------
Data Package Checklist

(Initials do not signify approval)

Reviewer

MASB QA Officer
NAREL QA Coordinator
MASB Chief

Initials	Date

Project: KATRINA RESPONSE-MS

SDG Number: #0500068

Date due:

Analysis: NAREL RA-04

Type of Package:

~ Data Summary Package

~ Complete Package

Y N N/A

Comments

~	~	~	All samples in the SDG are reported

~	~	~	All results are the ones intended

~	~	~	Printed results match the raw data

~	~	~	Error report forms are attached

~	~	~	SDG Form is attached

~	~	~	Analyst's checklist is attached

~	~	~	Original prep batch forms are attached

~	~	~	All supporting data sheets are attached

~	~	~	All raw data sheets appear to be correct

~	~	~	All handwritten notes are initialed and dated

~	~	~	Package is arranged correctly

~	~	~	Package appears to be complete

Were holding times met?	~ Yes ~ No ~ N/A

Were all QC results acceptable? ~ Yes ~ No
Are there any exceptions to report? ~ Yes ~ No

Prepared by:

Q AO Review

Y	N	N/A

~	~	~	All QC failures are noted

~	~	~	Raw data look reasonable

~	~	~	All exceptions have been noted

Note: If changes to the case
narrative are suggested, please
provide the necessary language.

Comments:

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES

REPORT OF SAMPLE DELIV ERY GROUP #0500068

Project:	KATRINA RESPONSE-MS

Analysis Procedure: Radium-226 in Environmental Matrices
Date Reported:	11/17/2005

SAMPLES

NAREL
Sample #

Client Sample ID

Type

Matrix

Date

Collected

Date
Received

A5.04982A

CFMSF01

SAM

SOIL

10/06/2005

10/07/2005

A5.04983B

CFMSF02

SAM

SOIL

10/06/2005

10/07/2005

A5.04984C

CFMSF02S

SAM

SOIL

10/06/2005

10/07/2005

A5.04985D

CFMSF08

SAM

SOIL

10/06/2005

10/07/2005

EXCEPTIONS

1.	Packaging and Shipping - No problems were observed.

2.	Documentation - No problems were observed.

3.	Sample Preparation - No problems were encountered.

4.	Analysis - No problems were encountered.

5.	Holding Times - All holding times were met.

QUALITY CONTROL

1.	QC samples - All QC analysis results met NAREL acceptance criteria.

2.	Instruments - Response and background checks for all instruments used in these analyses met NAREL
acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as
noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and
Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the
following signatures.

Mary F. Wisdom	Date

Quality Assurance Coordinator

John Griggs. Ph.D.	Date

Chief. Monitoring and Analytical Services Branch

-------
GENERAL INFORMATION

SAMPLE TYPES

BLD	Blind sample

FBK	Field blank

SAM	Normal sample

ANALYSIS QC TYPES

ANA	Normal analysis

DUP	Laboratory duplicate

LCS	Laboratory control sample (blank spike)

MS	Matrix spike

MSD	Matrix spike duplicate

RBK	Reagent blank

QUALITY INDICATORS

RPD	Relative Percent Difference

%R	Percent Recovery

Z	Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3
standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control
limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard
deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value
by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the
combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the
native sample activity is subtracted from each measured value and the net concentrations arc then converted to total
activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of
measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD. between duplicate results and the "percent recovery." or %R,
for spiked analyses, but docs not use these values for evaluation.

-------
(Blank page)

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

ANALYSIS SUMMARY

Analysis Procedure: NAREL RA-04

Title:	Radium-226 in Environmental Matrices

NAREL Sample #

QC
Type

Preparation Procedure

Date

Completed

Prep
Batch #

QC

Batch #

A5.04982A



NAREL RA-01

11/15/2005

0010188k

0003929X

A5.04982A

MS

NAREL RA-01

11/15/2005

0010188k

0003929X

A5.04982A

MSD

NAREL RA-01

11/15/2005

0010188k

0003929X

A5.04983B



NAREL RA-01

11/15/2005

0010188k

0003929X

A5.04983B

DUP

NAREL RA-01

11/15/2005

0010188k

0003929X

A5.04984C



NAREL RA-01

11/17/2005

0010198M

0003929X

A5.04985D



NAREL RA-01

11/17/2005

0010198M

0003929X

RBK-00496350X *

RBK

NAREL RA-01

11/15/2005

0010188k

0003929X

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

PREPARATION METHOD(S) USED

Procedure ID

Title

NAREL RA-01

Preparing Solid Samples for Ra-226 and Ra-228 Analysis

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04982A
SOIL

SAM

5.022e-01 GASH
91.12%

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4E

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

9.22e-01

1.5e-01

2.6e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04982A
SOIL

SAM

4.981e-01 GASH
91.12%

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
MS

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4F

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

3.68e+01

5.5e+00

3.6e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04982A
SOIL

SAM

5.022e-01 GASH
91.12%

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
MSD

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4G

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

3.09e+01

4.6e+00

3.2e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04983B
SOIL

SAM

4.931e-01 GASH
77.88 %

95.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4I

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

5.85e-01

1.0e-01

2.8e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04983B
SOIL

SAM

4.982e-01 GASH
77.88 %

95.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
DUP

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4K

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

6.92e-01

1.2e-01

3.2e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04984C
SOIL

SAM

5.005e-01 GASH
77.37 %

95.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X
0010198M

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4K

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

6.70e-01

l.le-01

3.3e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04985D
SOIL

SAM

4.960e-01 GASH
93.22 %

97.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X
0010198M

NAREL RA-01
NAREL RA-04
CHD
ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/16/2005 18:15

1000.0

LC4M

CHD

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

5.54e-01

9.7e-02

2.6e-02

PCI/GDRY

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

QC Sample #: RBK-00496350X

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003929X

0010188K
NAREL RA-01
NAREL RA-04
CHD
RBK

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

11/14/2005 18:30

1000.0

LC4M

DPG

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Ra226

7.54e-02

1.7e-02

1.4e-02

PCI

10/25/2005

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

QC BATCH SUMMARY

QC batch#:	0003929X

Preparation procedure: NAREL RA-01
Analysis procedure: NAREL RA-04

NAREL Sample #

QC
Type

Yield (%)

± 2a Uncertainty (%)

Analyst

A5.04982A



N/A



CHD

A5.04982A

MS

N/A



CHD

A5.04982A

MSD

N/A



CHD

A5.04983B



N/A



CHD

A5.04983B

DUP

N/A



CHD

A5.04984C



N/A



CHD

A5.04985D



N/A



CHD

RBK-00496350X *

RBK

N/A



CHD

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL
Sample #

QC
Type

Aliquot Si/c

Completion
Date

Prep Batch

A5.04982A



5.02e-01 GASH

11/15/2005

0010188k

A5.04982A

MS

4.98e-01 GASH

11/15/2005

0010188k

A5.04982A

MSD

5.02e-01 GASH

11/15/2005

0010188k

A5.04983B



4.93e-01 GASH

11/15/2005

0010188k

A5.04983B

DUP

4.98e-01 GASH

11/15/2005

0010188k

A5.04984C



5.01e-01 GASH

11/17/2005

0010198M

A5.04985D



4.96e-01 GASH

11/17/2005

0010198M

RBK-00496350X *

RBK

1.00e+00 SAMP

11/15/2005

0010188k

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

RA226 ANALYSES
SDG #0500068

DETECTOR REPORT

The following were used for samples in the SDG

LC4E	1 1/14/2005 18:30 00495566H A5.04982A

LC4F	1 1/14/2005 18:30 00496347C A5.04982A

LC4G	1 1/14/2005 18:30 00496348D A5.04982A

LC4I	1 1/14/2005 18:30 00495569L A5.04983 B

LC4K	1 1/14/2005 18:30 00496349E A5.04983 B

LC4K	1 1/16/2005 18:15 00495572F A5.04984C

LC4M	1 1/16/2005 18:15 00495575J A5.04985D

The following were used for other samples in the QC batches

LC4M 11/14/2005 18:30 00496350X

-------
Data Package Checklist

(Initials do not signify approval)

Reviewer

MASB QA Officer
NAREL QA Coordinator
MASB Chief

Initials	Date

Project: KATRINA RESPONSE-MS

SDG Number: #0500067

Date due:

Analysis: NAREL GAM-01

Type of Package:

~ Data Summary Package

~ Complete Package

Y N N/A

Comments

~	~	~	All samples in the SDG are reported

~	~	~	All results are the ones intended

~	~	~	Printed results match the raw data

~	~	~	Error report forms are attached

~	~	~	SDG Form is attached

~	~	~	Analyst's checklist is attached

~	~	~	Original prep batch forms are attached

~	~	~	All supporting data sheets are attached

~	~	~	All raw data sheets appear to be correct

~	~	~	All handwritten notes are initialed and dated

~	~	~	Package is arranged correctly

~	~	~	Package appears to be complete

Were holding times met?	~ Yes ~ No ~ N/A

Were all QC results acceptable? ~ Yes ~ No
Are there any exceptions to report? ~ Yes ~ No

Prepared by:

Q AO Review

Y	N	N/A

~	~	~	All QC failures are noted

~	~	~	Raw data look reasonable

~	~	~	All exceptions have been noted

Note: If changes to the case
narrative are suggested, please
provide the necessary language.

Comments:

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

REPORT OF SAMPLE DELIV ERY GROUP #0500067

Project:	KATRINA RESPONSE-MS

Analysis Procedure: Gamma Spectrometry
Date Reported:	10/27/2005

SAMPLES

NAREL
Sample #

Client Sample ID

Type

Matrix

Date

Collected

Date
Received

A5.04976C

CFMSD03

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04977D

CFMSD04

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04978E

CFMSD05

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04979F

CFMSD05D

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04980Y

CFMSD06

SAM

SEDIMENT

10/06/2005

10/07/2005

A5.04981Z

CFMSD07

SAM

SEDIMENT

10/06/2005

10/07/2005

EXCEPTIONS

1.	Packaging and Shipping - No problems were observed.

2.	Documentation - No problems were observed.

3.	Sample Preparation - No problems were encountered.

4.	Analysis - NAREL sample A5.04978 was originally counted on a detector that failed its daily QC. The
sample was recounted on a different detector. The results of the recount arc reported in this data package.

5.	Holding Times - All holding times were met.

QUALITY CONTROL

1.	QC samples - All QC analysis results met NAREL acceptance criteria.

2.	Instruments - Response and background checks for all instruments used in these analyses met NAREL
acceptance criteria.

-------
CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as
noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and
Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the
following signatures.

Mary F. Wisdom	Date

Quality Assurance Coordinator

John Griggs. Ph.D.	Date

Chief. Monitoring and Analytical Services Branch

-------
GENERAL INFORMATION

SAMPLE TYPES

BLD	Blind sample

FBK	Field blank

SAM	Normal sample

ANALYSIS QC TYPES

ANA	Normal analysis

DUP	Laboratory duplicate

LCS	Laboratory control sample (blank spike)

MS	Matrix spike

MSD	Matrix spike duplicate

RBK	Reagent blank

QUALITY INDICATORS

RPD	Relative Percent Difference

%R	Percent Recovery

Z	Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3
standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control
limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard
deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value
by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the
combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the
native sample activity is subtracted from each measured value and the net concentrations arc then converted to total
activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of
measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD. between duplicate results and the "percent recovery." or %R,
for spiked analyses, but docs not use these values for evaluation.

-------
-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

ANALYSIS SUMMARY

Analysis Procedure: NAREL GAM-01
Title:	Gamma Spectrometry

NAREL Sample #

QC
Type

Preparation Procedure

Date

Completed

Prep
Batch #

QC

Batch #

A5.04976C



N/A

10/13/2005

0010113P

0003916R

A5.04977D



N/A

10/13/2005

0010113P

0003916R

A5.04978E



N/A

10/27/2005

0010151W

0003916R

A5.04979F



N/A

10/13/2005

0010113P

0003916R

A5.04980Y



N/A

10/13/2005

0010113P

0003916R

A5.04980Y

DUP

N/A

10/14/2005

0010113P

0003916R

A5.04981Z



N/A

10/13/2005

0010113P

0003916R

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04976C

SEDIMENT

SAM

1.150e+02 GDRY
44.22 %

92.00 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/12/2005 15:21

1000.0

GE02

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



1.6e-01

PCI/GDRY

10/06/2005

Be7

2.75e-01

1.5e-01



PCI/GDRY

10/06/2005

Bi212

3.51e-01

2.8e-01



PCI/GDRY

10/06/2005

Bi214 *

3.64e-01

6.0e-02



PCI/GDRY

10/06/2005

Co60

ND



5.6e-02

PCI/GDRY

10/06/2005

Csl37

2.39e-02

1.7e-()2



PCI/GDRY

10/06/2005

1131

ND



5.1e-02

PCI/GDRY

10/06/2005

K40

2.34e+00

4.2e-01



PCI/GDRY

10/06/2005

Pb210 *

8.85e-01

9.3e-01



PCI/GDRY

10/06/2005

Pb212

4.65e-01

4.8e-02



PCI/GDRY

10/06/2005

Pb214 *

4.35e-01

5.2e-02



PCI/GDRY

10/06/2005

Ra223

1.53e-01

7.5e-02



PCI/GDRY

10/06/2005

Ra224

3.97e-01

3.3e-01



PCI/GDRY

10/06/2005

Ra226 *

1.08e+00

4.0e-01



PCI/GDRY

10/06/2005

Ra228

3.74e-01

7.0e-02



PCI/GDRY

10/06/2005

Th234 *

6.77e-01

2.3e-01



PCI/GDRY

10/06/2005

T1208

1.42e-01

2.8e-02



PCI/GDRY

10/06/2005

U235 *

6.75e-02

2.5e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04977D

SEDIMENT

SAM

2.440e+02 GDRY

75.62 %

96.80 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/12/2005 15:22

1000.0

GE04

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



8.7e-02

PCI/GDRY

10/06/2005

Be7

5.55e-02

5.8e-02



PCI/GDRY

10/06/2005

Bi212

4.60e-01

1.3e-01



PCI/GDRY

10/06/2005

Bi214 *

3.84e-01

3.3e-02



PCI/GDRY

10/06/2005

Co60

ND



2.0e-02

PCI/GDRY

10/06/2005

Csl37

ND



2.0e-02

PCI/GDRY

10/06/2005

1131

ND



2.5e-02

PCI/GDRY

10/06/2005

K40

l.lle+00

1.6e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.2e+00

PCI/GDRY

10/06/2005

Pb212

4.38e-01

3.3e-02



PCI/GDRY

10/06/2005

Pb214 *

4.36e-01

3.3e-02



PCI/GDRY

10/06/2005

Ra224

4.03e-01

2.0e-01



PCI/GDRY

10/06/2005

Ra226 *

7.93e-01

1.9e-01



PCI/GDRY

10/06/2005

Ra228

4.13e-01

3.9e-02



PCI/GDRY

10/06/2005

T1208

1.29e-01

1.4e-02



PCI/GDRY

10/06/2005

U235 *

4.98e-02

1.2e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04978E

SEDIMENT

SAM

1.340e+01 GASH
22.28 %

56.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010151W
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/26/2005 14:15

1000.0

GE04

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



6.3e-01

PCI/GDRY

10/06/2005

Bi212

4.59e-01

4.2e-01



PCI/GDRY

10/06/2005

Bi214 *

4.74e-01

9.8e-02



PCI/GDRY

10/06/2005

Co60

ND



7.8e-02

PCI/GDRY

10/06/2005

Csl37

4.28e-01

5.3e-02



PCI/GDRY

10/06/2005

1131

ND



3.2e-01

PCI/GDRY

10/06/2005

K40

2.32e+00

6.7e-01



PCI/GDRY

10/06/2005

Pb210

ND



9.4e+00

PCI/GDRY

10/06/2005

Pb212

4.93e-01

8.1e-02



PCI/GDRY

10/06/2005

Pb214 *

5.59e-01

8.3e-02



PCI/GDRY

10/06/2005

Ra226 *

1.26e+00

7.6e-01



PCI/GDRY

10/06/2005

Ra228

3.98e-01

1.2e-01



PCI/GDRY

10/06/2005

Th234 *

1.04e+00

6.1e-01



PCI/GDRY

10/06/2005

T1208

1.35e-01

4.9e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04979F

SEDIMENT

SAM

4.060e+01 GDRY
23.14%

66.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/12/2005 15:23

1000.0

GE06

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



2.4e-01

PCI/GDRY

10/06/2005

Bi212

6.80e-01

3.4e-01



PCI/GDRY

10/06/2005

Bi214 *

6.00e-01

1.0e-01



PCI/GDRY

10/06/2005

Co60

ND



6.1e-02

PCI/GDRY

10/06/2005

Csl37

7.10e-01

6.2e-02



PCI/GDRY

10/06/2005

1131

ND



8.6e-02

PCI/GDRY

10/06/2005

K40

2.90e+00

5.4e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.5e+00

PCI/GDRY

10/06/2005

Pb212

5.55e-01

7.3e-02



PCI/GDRY

10/06/2005

Pb214 *

7.32e-01

8.6e-02



PCI/GDRY

10/06/2005

Ra223

2.33e-01

1.4e-01



PCI/GDRY

10/06/2005

Ra226 *

1.66e+00

7.4e-01



PCI/GDRY

10/06/2005

Ra228

5.93e-01

1.2e-01



PCI/GDRY

10/06/2005

Th234 *

1.61e+00

5.3e-01



PCI/GDRY

10/06/2005

T1208

1.92e-01

4.4e-02



PCI/GDRY

10/06/2005

U235 *

1.13e-01

4.4e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04980Y

SEDIMENT
SAM

7.390e+01 GDRY
50.08 %

82.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/12/2005 15:23

1000.0

GE07

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



2.0e-01

PCI/GDRY

10/06/2005

Be7

3.53e-01

1.7e-01



PCI/GDRY

10/06/2005

Bi212

1.17e+00

3.3e-01



PCI/GDRY

10/06/2005

Bi214 *

7.05e-01

7.6e-02



PCI/GDRY

10/06/2005

Co60

ND



4.5e-02

PCI/GDRY

10/06/2005

Csl37

5.36e-02

2. le-02



PCI/GDRY

10/06/2005

1131

ND



6.6e-02

PCI/GDRY

10/06/2005

K40

6.28e+00

6.0e-01



PCI/GDRY

10/06/2005

Pb210

ND



4.6e+00

PCI/GDRY

10/06/2005

Pb212

9.39e-01

7.8e-02



PCI/GDRY

10/06/2005

Pb214 *

7.85e-01

7.3e-02



PCI/GDRY

10/06/2005

Ra223

2.97e-01

l.le-01



PCI/GDRY

10/06/2005

Ra226 *

1.82e+00

5.8e-01



PCI/GDRY

10/06/2005

Ra228

1.00e+00

l.le-01



PCI/GDRY

10/06/2005

T1208

2.63e-01

3.6e-02



PCI/GDRY

10/06/2005

U235 *

1.14e-01

3.6e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04980Y

SEDIMENT
SAM

7.390e+01 GDRY
50.08 %

82.40 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

DUP

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/13/2005 12:52

1000.0

GE02

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



2.7e-()l

PCI/GDRY

10/06/2005

Be7

1.50C-01

1.5e-01



PCI/GDRY

10/06/2005

Bi212

9.95e-01

3.8e-01



PCI/GDRY

10/06/2005

Bi214 *

6.45e-01

9. le-02



PCI/GDRY

10/06/2005

Co60

ND



7.8e-02

PCI/GDRY

10/06/2005

Csl37

4.26e-02

3.0e-02



PCI/GDRY

10/06/2005

1131

ND



7.3e-02

PCI/GDRY

10/06/2005

K40

5.81e+00

7.7e-()l



PCI/GDRY

10/06/2005

Pb210

ND



2.0e+00

PCI/GDRY

10/06/2005

Pb212

9.68e-01

8.3e-02



PCI/GDRY

10/06/2005

Pb214 *

7.5 le-01

7.8e-02



PCI/GDRY

10/06/2005

Ra223

3.24e-01

1.4e-01



PCI/GDRY

10/06/2005

Ra224

8.66e-01

5.4e-01



PCI/GDRY

10/06/2005

Ra226 *

1.89e+00

5.5e-01



PCI/GDRY

10/06/2005

Ra228

8.66e-01

1.2e-01



PCI/GDRY

10/06/2005

Th234 *

1.55e+00

3.9e-01



PCI/GDRY

10/06/2005

T1208

3.00e-01

4.4e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04981Z

SEDIMENT

SAM

7.540e+01 GDRY
59.53 %

85.20 %

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003916R
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/12/2005 15:22

1000.0

GE09

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



1.8e-01

PCI/GDRY

10/06/2005

Be7

3.12e-01

1.7e-01



PCI/GDRY

10/06/2005

Bi212

5.62e-01

2.8e-01



PCI/GDRY

10/06/2005

Bi214 *

3.64e-01

5.8e-02



PCI/GDRY

10/06/2005

Co60

ND



4. le-02

PCI/GDRY

10/06/2005

Csl37

6.30e-01

4.8e-02



PCI/GDRY

10/06/2005

1131

ND



6.2e-02

PCI/GDRY

10/06/2005

K40

2.25e+(K)

3.4e-01



PCI/GDRY

10/06/2005

Pb210

ND



4.9e+00

PCI/GDRY

10/06/2005

Pb212

5.0 le-01

5.4e-02



PCI/GDRY

10/06/2005

Pb214 *

4.04e-01

5.4e-02



PCI/GDRY

10/06/2005

Ra224

4.95e-01

3.8e-01



PCI/GDRY

10/06/2005

Ra226

ND



5.9e-01

PCI/GDRY

10/06/2005

Ra228

5.57e-01

8.0e-02



PCI/GDRY

10/06/2005

Th234 *

7.23e-01

3.6e-01



PCI/GDRY

10/06/2005

T1208

1.66e-01

2.8e-02



PCI/GDRY

10/06/2005

U235 *

8.07e-02

2.8e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

QC BATCH SUMMARY

QC batch#:	0003916R

Preparation procedure: N/A
Analysis procedure: NAREL GAM-01

NAREL Sample #

QC
Type

Yield (%)

± 2a Uncertainty (%)

Analyst

A5.04976C



N/A



DPS

A5.04977D



N/A



DPS

A5.04978E



N/A



DPS

A5.04979F



N/A



DPS

A5.04980Y



N/A



DPS

A5.04980Y

DUP

N/A



DPS

A5.04981Z



N/A



DPS

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL
Sample #

QC
Type

Aliquot Si/c

Completion
Date

Prep Batch

A5.04976C



1.15e+02 GDRY

10/13/2005

0010113P

A5.04977D



2.44e+02 GDRY

10/13/2005

0010113P

A5.04978E



1.34e+01 GASH

10/27/2005

0010151W

A5.04979F



4.06e+01 GDRY

10/13/2005

0010113P

A5.04980Y



7.39e+01 GDRY

10/13/2005

0010113P

A5.04980Y

DUP

7.39e+01 GDRY

10/14/2005

0010113P

A5.04981Z



7.54e+01 GDRY

10/13/2005

0010113P

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500067

DETECTOR REPORT

The following were used for samples in the SDG

GE02	10/12/2005 15:21 00495545C A5.04976C

GE02	10/13/2005 12:52 00495560B A5.04980Y

GE04	10/12/2005 15:22 00495548F A5.04977D

GE04	10/26/2005 14:15 004963SOD A5.04978E

GE06	10/12/2005 15:23 00495554D A5.04979F

GE07	10/12/2005 15:23 00495557G A5.04980Y

GE09	10/12/2005 15:22 00495561C A5.04981Z

The following were used for other samples in the QC batches

None found

-------
Data Package Checklist

(Initials do not signify approval)

Reviewer

MASB QA Officer
NAREL QA Coordinator
MASB Chief

Initials	Date

Project: KATRINA RESPONSE-MS

SDG Number: #0500068

Date due:

Analysis: NAREL GAM-01

Type of Package:

~ Data Summary Package

~ Complete Package

Y N N/A

Comments

~	~	~	All samples in the SDG are reported

~	~	~	All results are the ones intended

~	~	~	Printed results match the raw data

~	~	~	Error report forms are attached

~	~	~	SDG Form is attached

~	~	~	Analyst's checklist is attached

~	~	~	Original prep batch forms are attached

~	~	~	All supporting data sheets are attached

~	~	~	All raw data sheets appear to be correct

~	~	~	All handwritten notes are initialed and dated

~	~	~	Package is arranged correctly

~	~	~	Package appears to be complete

Were holding times met?	~ Yes ~ No ~ N/A

Were all QC results acceptable? ~ Yes ~ No
Are there any exceptions to report? ~ Yes ~ No

Prepared by:

Q AO Review

Y	N	N/A

~	~	~	All QC failures are noted

~	~	~	Raw data look reasonable

~	~	~	All exceptions have been noted

Note: If changes to the case
narrative are suggested, please
provide the necessary language.

Comments:

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES

REPORT OF SAMPLE DELIV ERY GROUP #0500068

Project:	KATRINA RESPONSE-MS

Analysis Procedure: Gamma Spectrometry
Date Reported:	10/19/2005

SAMPLES

NAREL
Sample #

Client Sample ID

Type

Matrix

Date

Collected

Date
Received

A5.04982A

CFMSF01

SAM

SOIL

10/06/2005

10/07/2005

A5.04983B

CFMSF02

SAM

SOIL

10/06/2005

10/07/2005

A5.04984C

CFMSF02S

SAM

SOIL

10/06/2005

10/07/2005

A5.04985D

CFMSF08

SAM

SOIL

10/06/2005

10/07/2005

EXCEPTIONS

1.	Packaging and Shipping - No problems were observed.

2.	Documentation - No problems were observed.

3.	Sample Preparation - No problems were encountered.

4.	Analysis - No problems were encountered.

5.	Holding Times - All holding times were met.

QUALITY CONTROL

1.	QC samples - All QC analysis results met NAREL acceptance criteria.

2.	Instruments - Response and background checks for all instruments used in these analyses met NAREL
acceptance criteria.

CERTIFICATION

I certify that this data report complies with the terms and conditions of the Quality Assurance Project Plan, except as
noted above. Release of the data contained in this report has been authorized by the Chief of the Monitoring and
Analytical Services Branch and the NAREL Quality Assurance Coordinator, or their designees, as verified by the
following signatures.

Mary F. Wisdom	Date

Quality Assurance Coordinator

John Griggs. Ph.D.	Date

Chief. Monitoring and Analytical Services Branch

-------
GENERAL INFORMATION

SAMPLE TYPES

BLD	Blind sample

FBK	Field blank

SAM	Normal sample

ANALYSIS QC TYPES

ANA	Normal analysis

DUP	Laboratory duplicate

LCS	Laboratory control sample (blank spike)

MS	Matrix spike

MSD	Matrix spike duplicate

RBK	Reagent blank

QUALITY INDICATORS

RPD	Relative Percent Difference

%R	Percent Recovery

Z	Number of standard deviations by which a QC measurement differs from the expected value

EVALUATION OF QC ANALYSES

A reagent blank result is considered unacceptable if it is more than 3 standard deviations below zero or more than 3
standard deviations above a predetermined upper control limit. For some analyses NAREL has set the upper control
limit at zero. For others the control limit is a small positive number.

NAREL evaluates the results of duplicate and spike analyses using "Z scores." A Z score is the number of standard
deviations by which the QC result differs from its ideal value. The score is considered acceptable if its absolute value

is not greater than 3.

The Z score for a spiked sample is computed by dividing the difference between the measured value and the target value
by the combined standard uncertainty of the difference.

The Z score for a duplicate analysis is computed by dividing the difference between the two measured values by the
combined standard uncertainty of the difference. When the precision of paired MS/MSD analyses is evaluated, the
native sample activity is subtracted from each measured value and the net concentrations arc then converted to total
activities before the Z score is computed.

Each standard uncertainty used to compute a Z score includes an additional fixed term to represent sources of
measurement error other than counting error. This additional term is not used in the evaluation of reagent blanks.

NAREL reports the "relative percent difference," or RPD. between duplicate results and the "percent recovery." or %R,
for spiked analyses, but docs not use these values for evaluation.

-------
GENERAL INFORMATION (CONTINUED)

GAMMA ANALYSIS

The reporting format lists the gamma emitters in alphabetical order. The activity and 2-sigma uncertainty for
radionuclides measured by gamma spectroscopy are reported only if the nuclide is detected. Nuclides that arc not
detected do not appear in the report, with the exception of Ba-140. Co-60, Cs-137,1-131, K-40, Ra-226 and Ra-228.
If one of these seven nuclides is undetected. NAREL reports it as "Not Detected" or "ND", and provides a sample-
specific estimate of the MDC.

Due to potential spectral interferences and other possible problems associated with the determination of the activity
of certain radionuclides, the activities for Bi-214, Pb-214. Th-234, Pa-234m, Ra-226, Th-231, and U-235 arc subject
to greater possible uncertainty than other commonly reported radionuclides. It should be noted that this potential
uncertainty is not included in the two-sigma counting uncertainty which is reported with each activity. Although in
this report we do provide the calculated activities for these radionuclides, we recommend that the results be used only
as a qualitative means of indicating the presence of these radionuclides and not as a quantitative measure of their
concentration. The results for these nuclides arc not used in the evaluation of quality control samples. Furthermore,
because of mutual interference between Ra-226 and U-235, NAREL's gamma analysis software tends to overestimate
the amounts of these nuclides whenever both arc present in a sample. Lower estimates for Ra-226 activities can be
obtained from the reported activities of its decay products. Pb-214 and Bi-214, which arc likely to be somewhat less
than the Ra-226 activity because of the potential escape of radon gas.

NAREL's gamma spectroscopy software corrects activities and MDCs for decay between collection and analysis, but
only up to a limit of ten half-lives. So. if the decay time for a sample is more than ten half-lives of a radionuclide, that
nuclide will almost always be undetected and the reported MDC will be meaningless. This is usually a problem only
for short-lived radionuclides, such as 1-131 and Ba-140. when there is a long delay between collection and analysis.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

ANALYSIS SUMMARY

Analysis Procedure: NAREL GAM-01
Title:	Gamma Spectrometry

NAREL Sample #

QC
Type

Preparation Procedure

Date

Completed

Prep
Batch #

QC

Batch #

A5.04982A



N/A

10/13/2005

0010113P

0003917T

A5.04983B



N/A

10/14/2005

0010113P

0003917T

A5.04984C



N/A

10/14/2005

0010113P

0003917T

A5.04985D



N/A

10/14/2005

0010113P

0003917T

A5.04985D

DUP

N/A

10/18/2005

0010113P

0003917T

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04982A
SOIL

SAM

1.510e+02 GDRY

91.12%

N/A

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003917T
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/13/2005 12:47

500.0

GE13

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



1.2e-01

PCI/GDRY

10/06/2005

Bi212

4.72e-01

2.3e-01



PCI/GDRY

10/06/2005

Bi214 *

8.24e-01

6.6e-02



PCI/GDRY

10/06/2005

Co60

ND



2.7e-02

PCI/GDRY

10/06/2005

Csl37

4.5 le-02

1.3e-02



PCI/GDRY

10/06/2005

1131

ND



4.9e-02

PCI/GDRY

10/06/2005

K40

7.19C-01

2.2e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.1e+00

PCI/GDRY

10/06/2005

Pb212

4.28e-01

4.3e-02



PCI/GDRY

10/06/2005

Pb214 *

8.75e-01

6.5e-02



PCI/GDRY

10/06/2005

Ra223

1.4 le-01

1.0e-01



PCI/GDRY

10/06/2005

Ra226 *

2.28e+00

4.le-01



PCI/GDRY

10/06/2005

Ra228

4.6 le-01

6.2e-02



PCI/GDRY

10/06/2005

T1208

1.34e-01

2. le-02



PCI/GDRY

10/06/2005

U235 *

1.42e-01

2.5e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04983B
SOIL

SAM

1.560e+02 GDRY

77.88 %

N/A

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003917T
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/13/2005 21:09

500.0

GE13

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



l.le-01

PCI/GDRY

10/06/2005

Bi212

3.99e-01

2.2e-01



PCI/GDRY

10/06/2005

Bi214 *

5.10C-01

4.8e-02



PCI/GDRY

10/06/2005

Co60

ND



2.6e-02

PCI/GDRY

10/06/2005

Csl37

1.54e-01

2.0e-02



PCI/GDRY

10/06/2005

1131

ND



4.5e-02

PCI/GDRY

10/06/2005

K40

5.89e-01

2.1e-01



PCI/GDRY

10/06/2005

Pb210

ND



2.8e+00

PCI/GDRY

10/06/2005

Pb212

4.64e-01

4.6e-02



PCI/GDRY

10/06/2005

Pb214 *

5.45e-01

4.9e-02



PCI/GDRY

10/06/2005

Ra223

1.00e-01

1.0e-01



PCI/GDRY

10/06/2005

Ra224

3.93e-01

3.6e-01



PCI/GDRY

10/06/2005

Ra226 *

1.20e+00

3.5e-01



PCI/GDRY

10/06/2005

Ra228

4.67e-01

6. le-02



PCI/GDRY

10/06/2005

T1208

1.36e-01

2. le-02



PCI/GDRY

10/06/2005

U235 *

7.54e-02

2.2e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04984C
SOIL

SAM

1.380e+02 GDRY

77.37 %

N/A

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003917T
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/14/2005 05:32

500.0

GE13

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



1.5e-01

PCI/GDRY

10/06/2005

Bi212

3.29e-01

2.4e-01



PCI/GDRY

10/06/2005

Bi214 *

5.06e-01

5.2e-02



PCI/GDRY

10/06/2005

Co60

ND



2.8e-02

PCI/GDRY

10/06/2005

Csl37

1.56e-01

2. le-02



PCI/GDRY

10/06/2005

1131

ND



5. le-02

PCI/GDRY

10/06/2005

K40

8.68e-01

2.2e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.1e+00

PCI/GDRY

10/06/2005

Pb212

4.58e-01

4.7e-02



PCI/GDRY

10/06/2005

Pb214 *

5.59e-01

5.2e-02



PCI/GDRY

10/06/2005

Ra223

1.3 le-01

9.8e-02



PCI/GDRY

10/06/2005

Ra226 *

1.13e+00

4.le-01



PCI/GDRY

10/06/2005

Ra228

4.77e-01

6.6e-02



PCI/GDRY

10/06/2005

T1208

1.33e-01

2.2e-02



PCI/GDRY

10/06/2005

U235 *

7.12e-02

2.6e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04985D
SOIL

SAM

1.230e+02 GDRY

93.22 %

N/A

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003917T
0010113P
N/A

NAREL GAM-01

DPS

ANA

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/14/2005 13:55

500.0

GE13

NSS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



1.5e-01

PCI/GDRY

10/06/2005

Bi212

4.82e-01

2.9e-01



PCI/GDRY

10/06/2005

Bi214 *

4.57e-01

5.2e-02



PCI/GDRY

10/06/2005

Co60

ND



3.2e-02

PCI/GDRY

10/06/2005

Csl37

1.60e-02

1.3e-02



PCI/GDRY

10/06/2005

1131

ND



5.4e-02

PCI/GDRY

10/06/2005

K40

1.04e+00

2.8e-01



PCI/GDRY

10/06/2005

Pb210

ND



3.4e+00

PCI/GDRY

10/06/2005

Pb212

4.38e-01

4.9e-02



PCI/GDRY

10/06/2005

Pb214 *

5.17e-01

5.3e-02



PCI/GDRY

10/06/2005

Ra223

1.14e-01

l.le-01



PCI/GDRY

10/06/2005

Ra226 *

8.91e-01

4.5e-01



PCI/GDRY

10/06/2005

Ra228

4.66e-01

6.9e-02



PCI/GDRY

10/06/2005

T1208

1.38e-01

2.4e-()2



PCI/GDRY

10/06/2005

U235 *

5.59e-02

2.8e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

SAMPLE ANALYSIS REPORT

Sample #:

Matrix:

Sample type:
Amount analyzed:

Dry/wet weight:
Ash/dry weight:

A5.04985D
SOIL

SAM

1.230e+02 GDRY

93.22 %

N/A

QC batch #:

Prep batch #:

Prep procedure:
Analysis procedure:
Analyst:

QC type:

0003917T
0010113P
N/A

NAREL GAM-01

DPS

DUP

COUNTING INFORMATION

Date and time

Duration (mill)

Detector ID

Operator

10/17/2005 15:10

1000.0

GE02

DPS

ANALYTICAL RESULTS

Analyte

Activity

± 2o Uncertainty

MDC

Unit

Date

Bal40

ND



2.2e-01

PCI/GDRY

10/06/2005

Be7

2.12e-01

1.4e-01



PCI/GDRY

10/06/2005

Bi212

2.79e-01

2.6e-01



PCI/GDRY

10/06/2005

Bi214 *

4.26e-01

6.3e-02



PCI/GDRY

10/06/2005

Co60

ND



4.8e-02

PCI/GDRY

10/06/2005

Csl37

ND



4.2e-02

PCI/GDRY

10/06/2005

1131

ND



7. le-02

PCI/GDRY

10/06/2005

K40

1.16e+00

3.6e-01



PCI/GDRY

10/06/2005

Pb210

ND



1.4e+00

PCI/GDRY

10/06/2005

Pb212

4.06e-01

4.4e-02



PCI/GDRY

10/06/2005

Pb214 *

5.25e-01

5.5e-02



PCI/GDRY

10/06/2005

Ra223

1.06e-01

7.6e-02



PCI/GDRY

10/06/2005

Ra226 *

1.07e+00

3.7e-01



PCI/GDRY

10/06/2005

Ra228

4.67e-01

7.2e-02



PCI/GDRY

10/06/2005

Th234 *

5.20e-01

2.6e-01



PCI/GDRY

10/06/2005

T1208

1.37e-01

2.7e-02



PCI/GDRY

10/06/2005

U235 *

6.74e-02

2.3e-02



PCI/GDRY

10/06/2005

* Ail asterisk indicates a result whose value may be significantly over or underestimated.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

QC BATCH SUMMARY

QC batch#:	0003917T

Preparation procedure: N/A
Analysis procedure: NAREL GAM-01

NAREL Sample #

QC
Type

Yield (%)

± 2a Uncertainty (%)

Analyst

A5.04982A



N/A



DPS

A5.04983B



N/A



DPS

A5.04984C



N/A



DPS

A5.04985D



N/A



DPS

A5.04985D

DUP

N/A



DPS

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

PREPARATION BATCH SUMMARY

SAMPLES ANALYZED

NAREL
Sample #

QC
Type

Aliquot Si/c

Completion
Date

Prep Batch

A5.04982A
A5.04983B
A5.04984C
A5.04985D
A5.04985D

DUP

1.51e+02 GDRY
1.56e+02 GDRY
1.38e+02 GDRY
1.23e+02 GDRY
1.23e+02 GDRY

10/13/2005
10/14/2005
10/14/2005
10/14/2005
10/18/2005

0010113P
0010113P
0010113P
0010113P
0010113P

* Samples marked with an asterisk are not in this sample delivery group but were analyzed with it for QC purposes.

-------
U.S. ENVIRONMENTAL PROTECTION AGENCY
NATIONAL AIR AND RADIATION ENVIRONMENTAL LABORATORY

GAMMA ANALYSES
SDG #0500068

DETECTOR REPORT

The following were used for samples in the SDG

GE02	10/17/2005 15:10	00495576K A5.04985D

GE13	10/13/2005 12:47	00495564F A5.04982A

GE13	10/13/2005 21:09	00495567J A5.04983 B

GE13	10/14/2005 05:32	00495570D A5.04984C

GE13	10/14/2005 13:55	00495573G A5.04985D

The following were used for other samples in the QC batches

None found

-------