Water Quality Study of Bays in Coastal Mississippi
Water Quality Report
Science and Ecosystem Support Division
United States Environmental Protection Agency - Region 4
Athens, GA 30605
Mississippi Department of Environmental Quality
2380 Highway 80 West
Jackson, Mississippi 39204
Project #05-0926
October 28, 2005
(Version: 05msbay-report.WebFinal.doc)
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Executive Summary
EPA's Region 4 Science & Ecosystem Support Division (SESD), in cooperation with
the Mississippi Department of Environmental Quality (MDEQ), conducted a water quality
study in the rivers and bays along the Mississippi coast following Hurricanes Katrina and
Rita. The study was completed during the period September 26-30, 2005. The study area
encompassed major bay systems on the Mississippi coast including Bangs Lake, Bayou
Casotte, the Pascagoula and West Pascagoula River systems, the Back Bay of Biloxi, St.
Louis Bay, and the Pearl River. The objective of this study was to provide sediment and
water quality data in each major bay system along the Mississippi Sound. Flow was also
measured at the seaward boundary of each system for estimating both conventional and toxic
pollutant loadings entering the Mississippi Sound at the time of the study. This study was
not designed to identify specific pollutant sources within each system or provide definitive
information on the potential long term effects of the hurricanes on human or ecological
health.
Findings from the EPA and MDEQ joint survey of coastal Mississippi following
Hurricanes Katrina and Rita showed few detectable priority pollutant type compounds in the
studied bays and rivers. In general, the pollutants present were detected in favorable
concentrations when compared to EPA's National Ambient Water Quality Criteria for surface
waters and the National Oceanic and Atmospheric Administration (NOAA) published effect
levels for sediment. Dissolved oxygen concentrations were determined to be above the
State's adopted minimum criteria at all but two of the thirty-nine surface water locations.
Bacteriological densities at the study locations were less than EPA's promulgated enterococci
criteria for coastal waters. Overall, the data collected by EPA shows that few water quality
criteria were exceeded during the study. An exception was algal growth results in Back Bay
of Biloxi and Bayou Casotte that exceeded 5 mg/1 (dry weight). Dioxin results for the five
sediment samples collected were all well below the EPA screening value for residential soils.
The results of this study may be used as the basis for future targeted water quality studies by
MDEQ and/or the EPA.
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Table of Contents
1.0 Introduction 1
2.0 Objectives 1
3.0 Study Area 1
4.0 Summary 8
5.0 Methods
5.1 Chemical Water Quality Sampling 8
5.2 Bacteriological Water Quality Sampling 9
5.3 Analytical Methods 9
5.4 In-Situ Monitoring 10
5.5 Sediment Sampling 10
5.6 Bay outlet loadings to MS Sound 11
6.0 Results
6.1 Chemical Water Quality Sampling 12
6.2 Bacteriological Water Quality Sampling 18
6.3 In-Situ Monitoring 19
6.4 Sediment Sampling 20
6.5 Bay outlet loadings to MS Sound 26
7.0 Data Management
7.1 Documentation/Records 30
7.2 Quality Assurance and Quality Control 30
7.3 Data Validation/Verification 32
8.0 Project Management 32
9.0 Project Schedule 33
10.0 References 34
Appendix A ASB Analytical Detection Limit Tables 35
Appendix B Chemical Surface Water Quality Data 47
Appendix C Chemical Sediment Data 60
Appendix D In-Situ Water Quality Profiles 78
Appendix E MQL and NAWQC Tables 104
Appendix F Sediment MQLs 109
Appendix G Quality Assurance/Quality Control Results 114
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LIST OF TABLES
1 - Sampling Station Location & Descriptions 2
2 - Water Quality Preservation Requirements 9
3 - Field Parameter Analytical Methods 10
4 - Sediment Sample Preservation Requirements 11
5 - Chemical Water Quality Data - Detected Concentrations-
Bangs Lake & Bayou Casotte 13
6 - Chemical Water Quality Data - Detected Concentrations
Pascagoula, Escatawpa,& West Pascagoula Rivers 14
7 - Chemical Water Quality Data - Detected Concentrations
Back Bay of Biloxi 15
8 - Chemical Water Quality Data - Detected Concentrations
St. Louis Bay, Bayou Caddy, Pearl River 16
9 - Unionized Ammonia Data 17
10 - Microbiological Analysis of Coastal Waters in Mississippi 18
11 - Summary of In-Situ Profiles 20
12 - Chemical Sediment Data - Detected Concentrations -
Bangs Lake & Bayou Casotte 22
13 - Chemical Sediment Data - Detected Concentrations -
Pascagoula, Escatawpa, & West Pascagoula Rivers 23
14 - Chemical Sediment Data - Detected Concentrations -
Back Bay of Biloxi 24
15 - Chemical Sediment Data - Detected Concentrations -
St. Louis Bay, Bayou Caddy, & Pearl River 25
16 - Sediment Dioxin Results Escatawpa & Pascagoula Rivers
and St. Louis Bay 26
17 - Bay Outlet Metal Maximum Loading 28
18 - Bay Outlet Nutrient Maximum Loading 28
19 - Bay Outlet Volatile Organic Maximum Loading 28
20 - AGPT Results for Bay Outlets in Coastal Mississippi 29
21 - Critical Project Deliverables 33
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LIST OF FIGURES
1 - Site Location Map - Gulf Coast Monitoring 3
2 - Sampling Stations: Bayou Casotte and Bangs Lake 3
3 - Sampling Stations: Pascagoula, Escatawpa, and
West Pascagoula Rivers 4
4- Sampling Stations: Back Bay of Biloxi 4
5 - Sampling Stations: St. Louis Bay, Bayou Caddy and
Pearl River 5
6- Picture of Mississippi Phosphate NPDES discharge 5
7 - Picture of Escatawpa River near shipyard 6
8 - Picture of Back Bay of Biloxi @ Hwy 90 bridge 6
9 - Picture of Back Bay of Biloxi @ Industrial canal 7
10 - Picture of St. Louis Bay near bay outlet 7
11 - Tidal curve - Back Bay of Biloxi 27
12 - Bays in Coastal Mississippi - Wind Data 27
13 - AGPT Results for Bay Outlets in Coastal Mississippi 29
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1.0 Introduction
Hurricane Katrina struck the U.S. Gulf Coast on August 29, 2005. USGS real-time
instruments in Gautier, MS recorded wind speeds as high as 140 miles per hour and rainfall of
approximately 2 feet. Several agencies including EPA, the Mississippi Department of
Environmental Quality (MDEQ), United States Geological Survey (USGS), United States Corps
of Engineers (USCOE), and Federal Emergency Management Agency (FEMA) have conducted
extensive investigations into all aspects of the storm damage. Water quality in the major bay
systems of the Mississippi Sound is currently of particular concern to MDEQ and US EPA,
Region 4.
The EPA Office of Research and Development has conducted a comprehensive water
quality monitoring/sampling of the Mississippi Sound. To complement that effort, the Region 4
Science & Ecosystem Support Division (SESD) conducted water quality monitoring and
sampling at the major bay outlets to the Mississippi Sound. Additionally, MDEQ requested that
this sampling include historic SESD/MDEQ sampling stations within each bay.
2.0 Objectives
The primary objective of this survey was to provide water quality and flow data during a
mid-ebb tide in each major bay system feeding Mississippi Sound for estimating both
conventional and toxic pollutant loadings entering the Sound at the time of the study. In concert
with this effort, water quality sampling, in-situ monitoring, and sediment sampling was
conducted at selected stations within each bay or riverine system to provide an estimate of
pollutant concentrations at the time of the study. The scope of this study was determined by
scientists and engineers with the MDEQ and EPA to provide preliminary data on these systems
within a reasonable timeframe. The detection limits for the analysis of water and sediments for
this study are included in Appendix A.
The sampling locations were selected based on the hydrodynamic characteristics of the
water bodies, the location of historic water quality sampling locations, and the general location
of potential releases from industrial/municipal sources. The data generated from this study
presents a preliminary picture of the levels of targeted pollutants in the systems, and will be
useful to the State of Mississippi and EPA as additional studies are planned to assess water,
sediment and fish/shellfish conditions in each of the four major bay systems included in the
study. The results of this study may be used to develop a targeted water quality monitoring
study. However, the study was not designed to identify specific pollutant sources within each
system or provide definitive information on the potential long term effects on water quality from
Hurricane Katrina.
3.0 Study Area
The study area (see Figure 1) encompassed four major bay systems on the Mississippi
coast including Bayou Casotte (including Bangs Lake), the Pascagoula/West Pascagoula River
systems, the Back Bay of Biloxi, and St. Louis Bay (including Bayou Caddy, and the Pearl
River). Tablel and Figures 2-5 show the water and sediment sampling locations within each
major bay system. Figures 6-10 show pictures taken of Bayou Casotte, Escatawpa River, Back
Bay of Biloxi, Industrial Canal, and St. Louis Bay taken during the survey.
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Table 1
Sampling Station Locations and Descriptions
Water Quality Study of Bays in Coastal Mississippi
Station
Description
Location
Latitude Longitude
Sample
Date Time
BL1-SW
Bangs Lake - Water @ 1.5 ft depth
30° 21.234
88°
28.000
9/27/2005
1315
BL1-SD
Bangs Lake - Sediment - bottom @ 3 ft depth
30° 21.234
88°
28.000
9/27/2005
1415
BC1-SW
Bayou Casotte - water @ 22.75 ft depth
30° 19.980
88°
30.797
9/27/2005
1134
BC1-SW-D
Bayou Casotte - water @ 22.75 ft depth (duplicate)
30° 19.980
88°
30.797
9/27/2005
1205
BC2-SW
Bayou Casotte - water @ 21.75 ft depth
30° 20.681
88°
30.508
9/27/2005
1333
BC2-SD
Bayou Casotte - Sediment - bottom @ 43.5 ft depth
30° 20.641
88°
30.547
9/27/2005
1130
BC3-SW
Bayou Casotte - water @ 22.5 ft depth
30° 21.001
88°
30.412
9/27/2005
1410
BC4-SW
Bayou Casotte - water @1 ft depth
30° 21.521
88°
30.268
9/27/2005
1450
BC4-SD
Bayou Casotte - Sediment - bottom @ 2.1 ft depth
30° 21.506
88°
30.275
9/27/2005
1240
WPR1-SW
West Pascagoula River - Water @ 13 ft depth
30° 22.751
88°
36.509
9/28/2005
1115
WPR1-SD
West Pascagoula River - Sediment -bottom 26 ft depth
30° 22.751
88°
36.509
9/28/2005
1150
PR1-SW
Pascagoula River - Water @ 20 ft depth
30° 22.047
88°
33.882
9/28/2005
1240
PR1-SD
Pascagoula River - Sediment-bottom 40 ft depth
30° 22.047
88°
33.882
9/28/2005
1320
PR2-SW
Pascagoula River - Water Composited from 5 & 15 ft depths
30° 26.387
88°
33.471
9/28/2005
1557
PR2-SD
Pascagoula River - Sediment-bottom 23 ft depth
30° 26.387
88°
33.471
9/28/2005
1545
ER1-SW
Escatawpa River - Water Composited from 5 &15 ft depths
30° 25.516
88°
32.861
9/28/2005
1420
ER1-SW-D
Escatawpa River - Water Composited from 5 &15 ft depths (duplicate)
30° 25.516
88°
32.861
9/28/2005
1425
ER1-SD
Escatawpa River - Sediment- bottom 23 ft depth
30° 25.517
88°
32.862
9/28/2005
1400
ER1-SD-D
Escatawpa River - Sediment- bottom 23 ft depth (duplicate)
30° 25.517
88°
32.862
9/28/2005
1430
ER2-SW
Escatawpa River - Water @ 10 ft depth
30° 25.312
88°
30.971
9/28/2005
1135
WPR2-SW
West Pascagoula River - Water @ 15 ft depth
30° 26.971
88°
37.573
9/28/2005
1420
BBB1-SW
Back Bay of Biloxi - Water @ 5.5 ft depth
30° 24.438
88° 50.816
9/29/2005
1312
BBB1-SW-D
Back Bay of Biloxi - Water @ 5.5 ft depth (duplicate)
30° 24.438
88° 50.816
9/29/2005
1340
BBB2-SW
Back Bay of Biloxi - Water @ 5.75 ft depth
30° 25.317
88° 53.760
9/29/2005
1032
BBB3-SW
Back Bay of Biloxi - Water @ 3.55 ft depth
30° 25.197
88° 55.868
9/29/2005
935
BBB3-SD
Back Bay of Biloxi - Sediment-bottom 7.1 ft depth
30° 25.195
88° 55.848
9/29/2005
945
BBB3-SD-D
Back Bay of Biloxi - Sediment-bottom 7.1 ft depth (duplicate)
30° 25.195
88° 55.848
9/29/2005
1005
BBB4-SW
Back Bay of Biloxi - Water @ 5 ft depth
30° 24.730
89° 00.665
9/29/2005
1300
BBB5-SW
Back Bay of Biloxi - Water @ 5 ft depth
30° 25.080
89° 00.416
9/29/2005
1140
BBB6-SW
Back Bay of Biloxi - Water @ 7 ft depth
30° 25.555
89° 03.461
9/29/2005
1025
BBB6-SD
Back Bay of Biloxi - Sediment-bottom 15 ft depth
30° 25.556
89° 03.448
9/29/2005
1120
BLC1-SW
Bayou Lacroix - water @ 4.5 ft depth
30° 20.467
CO!
24.493
9/30/2005
1000
JR1-SW
Jordan River - water @ 4.6 ft depth
30° 20.439
89°
21.649
9/30/2005
1047
WR1-SW
Wolf River - water @ 2 ft depth
30° 21.476
89°
16.398
9/30/2005
1445
BCD1-SW
Bayou Caddy - water @ 5 ft depth
30° 14.275
89°
25.841
9/30/2005
1015
SLB1-SW
St. Louis Bay - water @ 5.9 ft depth
30° 19.177
89°
18.407
9/30/2005
1230
SLB2-SW
St. Louis Bay - water @ 2.75 ft depth
30° 20.586
89°
17.588
9/30/2005
1430
SLB2-SD
St. Louis Bay - Sediment- bottom 5.7 ft depth
30° 20.586
89°
17.588
9/30/2005
1520
SLB3-SW
St. Louis Bay - water @ 3.75 ft depth
30° 20.593
89°
19.384
9/30/2005
1155
SLB3-SD
St. Louis Bay - Sediment- bottom 7.6 ft depth
30° 20.593
89°
19.384
9/30/2005
1230
SLB4-SW
St. Louis Bay - Water @ 2 ft depth
30° 21.345
89°
18.190
9/30/2005
1320
SLB5-SW
St. Louis Bay - Water @ 3 ft depth
30° 21.045
89°
20.400
9/30/2005
1240
SLB6-SW
St. Louis Bay - Water @ 3.4 ft depth
30° 21.733
89°
19.564
9/30/2005
1010
SLB6-SD
St. Louis Bay - Sediment- bottom 6.8 ft depth
30° 21.733
89°
19.564
9/30/2005
1040
SLB6-SD-D
St. Louis Bay - Sediment- bottom 6.8 ft depth (duplicate)
30° 21.733
89°
19.564
9/30/2005
1100
SLB7-SW
St. Louis Bay - Water @ 3 ft depth
30° 21.574
89°
21.221
9/30/2005
1126
PEARL1-SW
Pearl River - water composited from 3 and 9.5 ft depth
30° 14.140
89°
36.974
9/30/2005
1615
PEARL1-SD
Pearl River -Sediment - bottom @ 17 ft depth
30° 14.312
89°
36.860
9/29/2005
1645
2
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ad Bay | / /\
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3
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Station WPR2 L __
Figure 3, Sampling Stations - Pasiaaoula, Escalanpa, West Pascagoula Riveis
»
Station PR2
Escatawpa
Ford
\ Moss PoiniK
\\
u
w
i Station ER2
j®"!
Cautier
Station 1TR1 , —
*W\
Station EKI
i0j Pastagoulu
Station PR1
'#) In situ profiling, water quality sampling, sediment sampling
# In situ profiling, water quality sampling
©1393 EbL^xnu KUjpiii
^ii>
Figure 4, Sampling Stations Back Bay of Biloxi
.cum LiuA.r '
Lorraine
Station H B H5
\\
Gulfport-Bilo^ ^Regional Aupoit---'
| 1 1 lHandsboro
| Station BBBfi
„ Mississippi City
Station BE04
Station EBBS
Station BBB2
//
I1
If ¦
U D'iberville
Gulf]
Beau voir
o o
EdgeYsatei 1'diL
Station BBB1 -
Tfitoxi
® In situ profiling, water quality sampling, sediment sampling
£ In-situ profiling, water quality sampling
EbLonan M4^daj
4
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Figure 5, Sampling Stations - St. Louis Bay, Bayou Caddy, & Pearl River
Jones Mill
Station SLB4
Station SLB6
Station SLB7
'fo\f Riv&
Station WR1
Devils Swamj
Station BLC1
Station JR1
Station SLB5 fri—
-"p-] r \ i 1 Lv Station SLB3
/Bayside,Paik/<^'
Logtown
RfSi.
Station BCD1
Clermont Harbor
.Pearlington
Station Pearll
Ansley
Q_1 SW-Lb 1^' mi
n Station SLB2 [an
Henderson Pomt
Station SLB1
Lake shore ,g:i In_situ profiJing
A ~ In-situ profiling
water quality sampling, sediment samplin
water quality sampling
Figure 6, Mississippi Phosphate's NPDES discharge
5
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Figure 7, Escatawpa River near Shipyard
6
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7
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4.0 Summary
Results from the EPA and MDEQ joint survey of coastal Mississippi following Hurricane
Katrina and Rita showed few detectable priority pollutant compounds in the studied bays and
rivers. In general, the compounds present in surface waters were low in concentration compared
to EPA's National Ambient Water Quality Criteria (NAWQC) for priority toxic pollutants. The
compounds present in the sediment were generally lower than the levels which would be
expected to have adverse effects, based on values published by NOAA. Only two surface water
stations had dissolved oxygen concentrations below the minimum water quality criteria adopted
by the state of Mississippi. Bacteriological densities at the study locations were less than EPA's
promulgated enterococci criteria for coastal waters. Overall, the data collected by EPA shows
that few water quality criteria were exceeded during the study. An exception was high algal
growth results in the Back Bay of Biloxi and Bayou Casotte. Dioxin results for the five sediment
samples collected were all well below the EPA screening value for residential soils. The results
of this study may be used as the basis for future targeted water quality studies by MDEQ and/or
the EPA.
5.0 Methods
5.1 Chemical Water Quality Sampling
All surface water samples were collected according to the procedures described in the
Ecological Assessment Standard Operation Procedures and Quality Assurance Manual, January
2002 (EASOPQAM) and the Environmental Investigations Standard Operating Procedures and
Quality Assurance Manual, November, 2001 (EISOPQAM) (EPA 2002(a), EPA 2001). Water
quality samples were collected at each station shown on Table 1 and on Figures 2-5. Analyses
conducted on these samples included enterococci, Total Organic Carbon (TOC) and nutrients
scan, metals scan, routine volatile scan, routine semi-volatile scan, pesticide and PCB scan.
Appendix A contains a series of tables that list individual analytes for each of these scans. All
samples were collected after the completion of the in-situ profiling at each station. If the station
was stratified based on salinity, dissolved oxygen or temperature then the collection was
composited from the mid-depth point of each stratified layer as noted in Table 1. If stratification
was present, volatile organic compound (VOA) samples were collected from the upper layer.
The data that were critical to meeting the data quality objectives included flow measurements,
dissolved oxygen (DO), conductivity, enterococci, and the metals/organics scans.
Table 2 shows the required sample containers, preservation, and holding times for these
water quality samples. Containers were provided by SESD's Analytical Support Branch (ASB)
or obtained from the SESD Field Equipment Center. A second sample was collected each day at
a location selected by the project leader for volatile, semi-volatile and pesticide/PCB matrix
spike analyses. Following collection, samples were preserved as described in Table 2 and placed
in an iced cooler. Samples were transported to the command center at Keesler Air Force Base
(AFB) for processing. Samples were transported daily by MDEQ or EPA courier to the SESD
laboratory in Athens, Georgia.
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Table 2
Water Quality Sample Preservation Requirements
Analytical Group
Volume/Container
Preservative
Holding Time
TOC/nutrients
1 liter polyethylene
H2S04 to pH < 2,
Ice to 4° C
28 days
Metals
1 liter polyethylene
HNO3 to pH < 2,
Ice to 4° C
6 months
Hg is 28 days
Volatiles
40 ml glass vials (3)
with septum seal
HC1 to pH < 2,
Ice to 4° C
14 days
Semi-volatiles
1 liter amber glass
(2 bottles per station)
Ice to 4° C
7 days
Pesticides/PCBs
1 liter amber glass
(2 bottles per station)
Ice to 4° C
7 days
Enterococci
250 ml plastic
Ice to 4° C
6 hours
5.2 Bacteriological Water Quality Sampling
Bacteriological samples were collected for enterococcus analyses. Samples were
collected at each station as shown in Table 1 and Figures 2-5. Samples were collected by hand
dipping 100 ml or 250 ml wide mouth plastic bottles from the surface per EASOPQAM. Sample
collection personnel wore latex gloves and shoulder length plastic gloves during sample
collection and bottles remained capped prior to collection to avoid contamination. Following
sample collection, the bottles were recapped and sealed in whirl packs then placed on ice for
preservation. The samples were delivered by EPA personnel to the Ecological Assessment
Branch (EAB) Mobile Lab, located in Gulfport, MS within the 6 hour holding time.
5.3 Analytical Methods
All samples were analyzed by the SESD laboratory in Athens, Georgia with the exception
for dioxin/furan. Dioxin samples were analyzed by Paradigm Laboratories. All analyses
conducted by the SESD laboratory were in accordance with the Analytical Support Branch
Laboratory Operations and Quality Assurance Manual, dated November 17, 2004 which can be
accessed at: http://www.epa.gov/region4/sesd/asbsop/asbsop.html (EPA 2004). Refer to
Appendix A for a list of analytes, methods and minimum quantitation limits (MQLs) that were
used for this study. It should be noted that MQLs were matrix dependent and vary from sample
to sample depending on background material and other analyte concentrations. The MQLs
presented in these tables are those which can be achieved the majority of time in the matrix
listed. ASBs Standard Operating Procedures (SOPs) for the listed methods include quality
control procedures equal to or greater than the method specified levels.
Validation of the dioxin/furan data was conducted using the National Functional
Guidelines for Dioxin Data Review, OSWER540-R-02-003 (August 2002) and Region 4's Data
Validation Standard Operating Procedures for Dioxin Data Version 3.0 (May 2002) documents
(EPA 2002(c) and (d)). The dioxin/furan data consisted of a Level 4 - CLP type data package
that contains the C-O-Cs, instrument raw data, initial and/or continuing calibration data/curves,
9
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bench sheets/sample preparation information, QA/QC data/information, and case narrative
detailing any problems associated with these data.
5.4 In-Situ Monitoring
In-situ monitoring was conducted at all stations shown in Figures 2-5. Dissolved oxygen,
salinity, pH and temperature profiles were obtained using a manually deployed multi-parameter
water quality monitor. All monitoring equipment was calibrated in accordance with the
EASOPQAM and the manufacturer's specifications daily and end checked at the end of each
day. Data were recorded in designated data sheets. Calibration standards were obtained from
EAB stocks that are traceable and new reagents and buffers were used during the study.
Parameter measurements were obtained from surface to bottom at one foot increments in waters
up to 12 feet deep and at two foot increments in waters greater than 12 feet deep. In order to
maintain consistency, measurements made at two foot increments were taken at odd-numbered
depths. The results from the profiling were used to guide the water quality sampling effort (see
section 4.1 for discussion of stratified conditions).
Exact profiling locations were determined by Global Positioning System (GPS)
instrumentation by the profiling crew in the field. The latitude/longitude, date and time of each
profile were recorded in the field data book. Table 3 shows the analytical methods used for the
in-situ monitoring.
Table 3
Field Parameter Analytical Methods
In-situ and Field
Parameters
Units
Analytical
Method
Accuracy of
Primary Equipment
Dissolved Oxygen
mg/1
Membrane-electrode
+ 0.2 mg/1
(up to 20 mg/1)
Temperature
°C
Thermistor
+ 0.15 °C
Salinity
ppt
Conductivity probe
greater of
+ 1% of reading or
0.1 ppt
pH
su
pH electrode
+ 0.2 SU
Latitude/Longitude
decimal degrees
DGPS/GPS based on
NAD83
+ 10 m
(w/ selective
availability disabled)
5.5 Sediment Sampling
Sediment samples were collected at the stations shown in Table 1 and Figures 2-5
according to the procedures in the EASOPQAM and the EISOPQAM (EPA 2002(a) and EPA
2001). Sediment samples were collected using a Petite Ponar Dredge, then transferred into a
Pyrex pan for homogenization and distribution using stainless steel spoon into the appropriate
sample containers (Table 4). Samples for VOA analysis were collected prior to homogenization
using an Encore device. SESD lab analyses of sediment samples included enterococci, nutrient
series scan, metals scan, volatiles scan, semi-volatiles scan, pesticide and PCB scan. A contract
10
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laboratory (Paradigm) analyzed the sediment samples selected for dioxin. The specific analytes
included in these scans are included in Appendix A (excluding dioxin). Samples were
transported daily by MDEQ or EPA couriers to the SESD laboratory in Athens, Georgia.
Multiple dredges were utilized to minimize the need to decontaminate sampling equipment
between stations. As required, between stations and at the end of each sampling day, sampling
equipment was decontaminated in the field according to the procedures in the EASOPQAM.
Table 4
Sediment Sample Preservation Requirements
Analytical Group
Volume/Container
Preservative
Holding Time
Nutrients
8 oz. glass
Ice to 4° C
Not specified
Metals
8 oz. glass
Ice to 4° C
6 months
Volatiles
Encore Sampler
+ 2 oz. glass for %
moisture
Ice to 4° C
48 hours
Semi-volatiles
8 oz. glass
Ice to 4° C
7 days
Pesticides/PCBs
8 oz. glass
Ice to 4° C
7 days
Dioxin
8 oz. Glass
Ice to 4° C
365 days
Enterococci
WhirlPak
Ice to 4° C
24 hours
5.6 Bay Outlet Loading to MS Sound
In order to estimate maximum pollutant loadings entering Mississippi Sound at the time
of the study, tidal flow measurement and water quality sampling were conducted at each major
bay outlet during a mid-ebb tide. As shown on Figures 2-5, major bay outlets include Bayou
Casotte, Pascagoula River, West Pascagoula River, Bay St. Louis, Back Bay of Biloxi, and the
Pearl River.
Flow was measured in the cross-section via boat-mounted RD Instruments Rio Grande
Acoustic Doppler Current Profiler (ADCP). The ADCP was towed by boat across the
measurement transect acquiring depth, width, and velocity. The resulting data was fed in real
time to a laptop computer for flow calculation using the manufacturer's software. Resulting
flows are recorded in the field. A QA review of the data is performed prior to reporting of the
final results. The meter is factory calibrated and has a sensitivity of 0.003 fps.
Due to the tidal nature of the water bodies sampled, flow varied during the sampling
period. Therefore, two to four measurements were made during the sampling effort to provide
an average flow condition. In addition, flow measurements in Bayou Casotte were complicated
by southerly winds causing bi-directional flow. This wind effect was addressed during the QA
review of the data using United States Geological Survey (USGS) recommendations.
Concurrent with flow measurement, water quality samples were collected and analyzed
as described in Section 4.1. These samples were collected at mid point and mid depth of the
main hydraulic section. Time constraints associated with the sampling effort mandated the
change from the original plan to use quarter point sampling. In addition, a grab sample for Algal
11
-------
Growth Potential Test (AGPT) and enterococci analysis were collected in their appropriate
containers. The AGPT samples were immediately placed on ice, and transported to the SESD
laboratory in Athens, Georgia. The bacteriological samples were placed on ice and delivered by
EPA personnel to the EPA Mobile Lab, located in Gulfport, MS within the 6 hour holding time
In order to identify the sampling period associated with the tidal cycle, a Stevens Axsys
water level recorder was installed at the Keesler AFB boat ramp on Back Bay of Biloxi, (Figure
11).
6.0 Results
6.1 Chemical Water Quality Sampling
All contaminants detected in surface water are presented in Tables 5-9. All data, detect
and non-detect, are presented in Appendices B and C. Corresponding minimum quantitation
limits (MQLs) for these data based on background salt interferences can be found in Appendices
E and F. Appendix D contains the in-situ profiling results.
All surface water data was compared to "criteria maximum concentration" (CMC) values
and the "criteria continuous concentration" (CCC) values established in the 2002 National
Ambient Water Quality Criteria (NAWQC) for priority toxic pollutants (EPA 2002(b)). The
CMC values are estimates of the highest concentration of a contaminant in surface water to
which an aquatic community can be exposed to briefly without resulting in an unacceptable
effect. The CCC values are estimates of the highest concentration of a contaminant in surface
water to which an aquatic community can be exposed to indefinitely without resulting in an
unacceptable effect. CMC and CCC values are not available for all contaminants analyzed in
this investigation. Only those contaminants that have published CMC and CCC values were
evaluated for this assessment. Additional literature review is required to evaluate all other
detected contaminants.
Tables 5 through 9 show the concentrations of toxic pollutants in surface waters measured during
the study. There were no detected concentrations of these pollutants that exceeded the CMC
levels published in EPA's NAWQC. As shown in Tables 5, 6, and 7, samples collected from
several stations detected concentrations of selenium and arsenic that exceeded the CCC levels
published in EPA's NAWQC. The analysis of arsenic (As) and selenium (Se) in saline matrices is
problematic because of the combination of low analytical sensitivity of As and Se and the large
interferences produced by the background salts in the matrix. While the technique used for these
analyses (ICP-MS) is the most sensitive available for the analysis of As and Se, these two
analytes are in the analytical region of the ICP-MS that is most prone to interferences from saline
matrices and are the most difficult to correct, resulting in analytical results with an elevated level
of uncertainty. As shown in Table 9, there was one sample collected from Bayou Casotte at
station BC4 which exceeded the national recommended CCC for ammonia.
12
-------
Table 5
Chemical Water Quality Data-Detected Concentrations - Bangs Lake & Bayou Casotte
September 27-30, 2005
Metals Scan
2002
NAWQC
CMC CCC
BC1SW
9/27/2005
1134
BC2SW
9/27/2005
1333
BC3SW
9/27/2005
1410
BC4SW
9/27/2005
1450
BL1SW
9/27/2005
1315
Arsenic
7440-38-2
UG/L
69
36
45
J
42
J
41
J
48
AJ
36 J
Calcium
7440-70-2
MG/L
350
360
350
340
A
270
Magnesium
7439-95-4
MG/L
1100
1100
1100
1000
A
820
Manganese
7439-96-5
UG/L
U
U
U
U
120
Potassium
7440-09-7
MG/L
360
380
360
320
A
270
Selenium
7782-49-2
UG/L
290
71
150
J
140
J
130
J
150
AJ
110 J
Sodium
7440-23-5
MG/L
9200
9500
9200
8400
A
6800
Strontium
7440-24-6
UG/L
6100
6300
6100
5500
A
4600
PCB Scan
None detected
Pesticides Scan
None detected
Volatiles Scan
None detected
Extractables Scan
None detected
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.075
0.072
0.064
1.5
U
Nitrate-Nitrite Nitrogen
MG/L
0.06
0.066
0.095
0.055
U
Total Kjeldahl Nitrogen
MG/L
0.25
0.2
0.22
1.9
0.76
Total Organic Carbon
MG/L
1.4
12
1.4
2.2
17
Total Phosphorus
7723-14-0
MG/L
0.22
0.27
0.38
17
0.18
Shaded areas identify analyte detected is above the ambient water quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
13
-------
Table 6
Chemical Water quality Data- Detectable Concetrations - Pascagoula River, Escatawpa River, and West Pascagoula River
September 27-30, 2005
Metals Scan
2002
NAWQC
CMC CCC
ER1DSW
9/28/2005
1425
ER1SW
9/28/2005
1420
ER2SW
9/28/2005
1135
PR1SW
9/28/2005
1240
PR2SW
9/28/2005
1557
WPR1SW
9/28/2005
1115
WPR2SW
9/28/2005
1420
Arsenic
7440-38-2
UG/L
69 36
23
AJ
24
J
28
J
46
J
23
J
34
J
U
Barium
7440-39-3
UG/L
U
U
U
U
U
U
47
Calcium
7440-70-2
MG/L
170
A
180
190
330
160
260
28
Magnesium
7439-95-4
MG/L
520
A
560
590
1000
470
840
74
Manganese
7439-96-5
UG/L
160
AJ
140
240
u
270
98
340
Potassium
7440-09-7
MG/L
170
A
180
200
340
150
260
26
Selenium
7782-49-2
UG/L
290 71
77
AJ
80
J
89
J
150
J
72
J
110
J
U
Sodium
7440-23-5
MG/L
4400
A
4700
5000
8700
4000
6900
650
Strontium
7440-24-6
UG/L
2900
A
3100
3300
5600
2700
5200
450
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
Toluene
108-88-3
UG/L
0.064
J
0.072
J
U
u
U
U
U
Extractables Scan
None Detected
Miscellaneous Extractables
Benzenedicarboxylic Acid, Dihexyl Ester
UG/L
NR
NR
10
NJ
NR
NR
NR
NR
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.087
0.093
0.17
0.072
0.12
0.083
0.056
Nitrate-Nitrite Nitrogen
MG/L
U
U
U
0.056
0.062
U
0.079
Total Kjeldahl Nitrogen
MG/L
0.38
0.41
0.49
0.29
0.47
0.45
0.51
Total Organic Carbon
MG/L
4.2
4.2
4.1
1.6
4.2
2.5
7
Total Phosphorus
7723-14-0
MG/L
0.05
0.048
0.036
0.087
0.052
0.063
0.041
Shaded areas identify analyte detected is above the ambient water quality criteria
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
NR-Not Reported
14
-------
Table 7
Chemical Water Quality Data- Detectable Concentrations- Back Bay of Biloxi
September 27-30, 2005
Metals Scan
2002
NAWQC
CMC CCC
BBB1DSW
9/29/2005
1340
BBB1SW
9/29/2005
1312
BBB2SW
9/29/2005
1032
BBB3SW
9/29/2005
935
BBB4SW
9/29/2005
1300
BBB5SW
9/29/2005
1140
BBB6SW
9/29/2005
1025
Arsenic
7440-38-2
UG/L
69 36
26
AJ
25
J
19
J
14
J
8
J
9.1
J
6.4 J
Barium
7440-39-3
UG/L
U
U
U
46
44
46
40
Calcium
7440-70-2
MG/L
160
A
160
130
90
51
58
40
Iron
7439-89-6
MG/L
1000
U
U
U
U
0.55
0.56
0.56
Magnesium
7439-95-4
MG/L
480
A
500
390
270
140
170
98
Manganese
7439-96-5
UG/L
67
A
62
110
190
260
290
190
Potassium
7440-09-7
MG/L
160
A
160
120
88
46
55
33
Selenium
7782-49-2
UG/L
290 71
56
J
38
J
20
J
25
J
14 J
Sodium
7440-23-5
MG/L
3900
A
4000
3100
2200
1100
1400
800
Strontium
7440-24-6
UG/L
2800
A
2900
2300
1600
840
990
610
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
(m- and/or p-)Xylene
UG/L
U
U
0.068
J
U
U
U
U
Bromodichloromethane
75-27-4
UG/L
U
U
U
U
U
U
0.074 J
Chloroform
67-66-3
UG/L
U
U
U
U
U
U
0.092 J
Toluene
108-88-3
UG/L
U
0.13
J
0.2
J
U
U
0.09
J
U
Extractables Scan
None Detected
Classical Nutrients
Ammonia
7664-41-7
MG/L
U
U
0.12
0.15
0.13
0.18
0.39
Nitrate-Nitrite Nitrogen
MG/L
U
U
U
U
0.1
0.071
0.54
Total Kjeldahl Nitrogen
MG/L
0.68
0.68
0.72
1.2
0.77
0.97
0.97
Total Organic Carbon
MG/L
11
5.2
6
12
10
9.1
11
Total Phosphorus
7723-14-0
MG/L
0.04
0.04
0.041
0.046
0.049
0.033
0.14
Shaded areas identify analyte detected is above the ambient water quality criteria
iers
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
15
-------
Table 8
Chemical Water Quality Data- Detectable Concentrations- St. Louis Bay, Bayou Caddy, and Pearl River
Sptember 27-30, 2005
Metals Scan
2002
NAWQC
CMC CCC
BCD1DSW
9/30/2005
1015
BLC1SW
9/30/2005
945
JR1SW
9/30/2005
1047
PEARL 1SW
9/30/2005
1615
SLB1SW
9/30/2005
1230
SLB2SW
9/30/2005
1430
SLB3SW
9/30/2005
1155
SLB4SW
9/30/2005
1320
SLB5SW
9/30/2005
1240
SLB6SW
9/30/2005
1010
SLB7SW
9/30/2005
1126
WR1SW
9/30/2005
1445
Aluminum
7429-90-5
UG/L
1200 A
U
U
U
U
U
U
U
U
U
U
U
Arsenic
7440-38-2
UG/L
69 36
20 AJ
9.6
J
14
J
4.6
J
22
J
21
J
20
J
18
AJ
17
J
18
J
16
J
11 J
Barium
7440-39-3
UG/L
66 AJ
65
67
61
61
62
61
61
AJ
62
64
64
110
Calcium
7440-70-2
MG/L
160 A
70
110
40
180
160
170
140
A
140
130
130
160
Iron
7439-89-6
MG/L
1000
1.2 A
1
U
0.76
U
U
U
U
U
U
U
1.6
Magnesium
7439-95-4
MG/L
520 A
210
330
110
550
500
520
450
A
430
410
380
500
Manganese
7439-96-5
UG/L
130 A J
880
480
870
U
300
72
240
AJ
210
260
300
650
Potassium
7440-09-7
MG/L
160 A
66
100
38
170
160
160
140
A
130
130
120
160
Selenium
7782-49-2
UG/L
290 71
60 AJ
25
J
39
J
11
J
64
J
63
J
62
J
52
AJ
51
J
52
J
46
J
31 J
Sodium
7440-23-5
MG/L
4200 A
1700
2700
930
4500
4100
4200
3600
A
3500
3400
3100
4100
Strontium
7440-24-6
UG/L
2800 A
1100
1800
640
3000
2800
2800
2500
A
2400
2300
2100
2800
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
(m- and/or p-)Xylene
UG/L
U
U
U
0.32
J
U
U
U
U
U
U
U
U
1,2,4-Tri methyl benzene
95-63-6
UG/L
U
U
U
0.11
J
U
U
U
U
U
U
U
U
Benzene
71-43-2
UG/L
U
U
U
0.11
J
U
U
U
U
U
U
U
U
Ethyl Benzene
100-41-4
UG/L
U
U
U
0.1
J
U
U
U
U
U
U
U
U
o-Xylene
95-47-6
UG/L
U
U
U
0.12
J
U
U
U
U
U
U
U
U
Toluene
108-88-3
UG/L
U
0.16
J
U
0.74
J
U
U
U
U
0.057
J
U
U
U
Extractables Scan
None Detected
Miscellaneous Extractables
Benzenedicarboxylic Acid, Dihexyl Ester
UG/L
NR
NR
NR
NR
NR
NR
NR
NR
NR
10
NJ
NR
NR
Classical Nutrients
Ammonia
7664-41-7
MG/L
U
0.16
U
0.07
U
U
U
U
U
U
U
U
Total Kjeldahl Nitrogen
MG/L
0.81
0.99
0.99
0.73
0.55
0.68
0.71
0.67
0.65
0.76
0.72
0.71
Total Organic Carbon
MG/L
3.9
13
9.8
7.8
4.5
6.4
5.6
6.6
7.5
7.7
8.4
8.6
Total Phosphorus
7723-14-0
MG/L
0.059
0.032
0.033
0.062
0.03
0.036
0.026
0.031
0.026
0.026
0.025
0.029
Shaded areas identify anaiyte detected is above the ambient water quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-ldentification of anaiyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence anaiyte is present; anaiyte reported as tentative identification.
N J-Presumptive evidence anaiyte is present; anaiyte reported as tentative identification. Reported value is an estimate.
K-ldentification of anaiyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-Identification of anaiyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of anaiyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
16
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Table 9
Unionized Ammonia Data
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Station
Date
Time
Temp
Salinity
pH
Sample
NH3
N02-N03
TKN
TN
TP
TN:TP
UIA
UIA
Deg C
ppt
su
Depth -ft
mg/l
mg/l
mg/l
mg/l
mg/l
fraction
mg/l
BL1
9/27/2005
1315
29.57
23.54
7.47
1.5
0.05 u
0.05 u
0.76
0.81
0.18
4.5
0.021
0.001
BC1
9/27/2005
1134
28.36
29.2
7.86
22.5
0.075
0.06
0.25
0.31
0.21
1.5
0.044
0.003
BC2
9/27/2005
1333
28.34
29.1
7.78
22
0.072
0.066
0.2
0.266
0.54
0.5
0.037
0.003
BC3
9/27/2005
1410
28.38
29.4
7.77
23
0.064
0.095
0.22
0.315
0.38
0.8
0.036
0.002
BC4
9/28/2005
1450
30.35
25
7.81
1
1.5
0.055
1.9
1.955
17
0.1
0.046
0.069
ER1*
9/28/2005
1425
29.12
4.07
7.48
0.09
0.05 u
0.39
0.44
0.05
8.8
0.023
0.002
ER2
9/28/2005
1135
28.72
10.43
6.47
10
0.17
0.05 u
0.49
0.54
0.036
15.0
0.002
0.000
PR1
9/28/2005
1240
28.51
28.53
7.8
20
0.072
0.056
0.29
0.346
0.087
4.0
0.039
0.003
PR2*
9/28/2005
1557
28.94
2.86
7.02
0.12
0.062
0.47
0.532
0.052
10.2
0.008
0.001
WPR1
9/28/2005
1115
28.56
24.1
7.69
13
0.083
0.05 u
0.45
0.5
0.063
7.9
0.031
0.003
WPR2
9/29/2005
1420
28.99
7.2
6.66
15
0.056
0.079
0.51
0.589
0.041
14.4
0.003
0.000
BBB1
9/29/2005
1340
28.52
15.07
7.88
5
0.05 u
0.05 u
0.68
0.73
0.04
18.3
0.050
0.002
BBB2
9/29/2005
1032
28.04
12.76
7.49
6
0.12
0.05 u
0.72
0.77
0.041
18.8
0.020
0.002
BBB3
9/29/2005
1030
28.39
8.66
7.33
5
0.15
0.05 u
1.2
1.25
0.046
27.2
0.015
0.002
BBB4
9/29/2005
1300
28.49
4.32
7.03
5
0.13
0.1
0.77
0.87
0.049
17.8
0.008
0.001
BBB5
9/29/2005
1140
28.37
5.01
6.94
5
0.18
0.071
0.97
1.041
0.033
31.5
0.006
0.001
BBB6
9/30/2005
1025
28.9
3.2
6.9
7
0.39
0.54
0.97
1.51
0.14
10.8
0.006
0.002
SLB1
9/30/2005
1230
28.18
15.24
7.8
6
0.05 u
0.05 u
0.55
0.6
0.03
20.0
0.041
0.002
SLB2
9/30/2005
1430
28.98
13.82
7.87
3
0.05 u
0.05 u
0.68
0.73
0.036
20.3
0.051
0.003
SLB3
9/30/2005
1155
28.48
14.34
7.8
4
0.05 u
0.05 u
0.71
0.76
0.54
1.4
0.042
0.002
SLB4
9/30/2005
1320
28.62
12.55
7.67
2
0.05 u
0.05 u
0.67
0.72
0.031
23.2
0.032
0.002
SLB5
9/30/2005
1240
28.6
12.02
7.84
3
0.05 u
0.05 u
0.65
0.7
0.026
26.9
0.047
0.002
SLB6
9/30/2005
1010
27.97
11.57
7.63
3
0.05 u
0.05 u
0.76
0.81
0.026
31.2
0.028
0.001
SLB7
9/30/2005
1126
28.12
10.55
7.78
3
0.05 u
0.05 u
0.72
0.77
0.025
30.8
0.040
0.002
BCD1
9/30/2005
1015
28.84
14.27
7.35
5
0.05 u
0.05 u
0.72
0.77
0.061
12.6
0.016
0.001
BLC1
9/30/2005
945
28.75
6.5
6.88
5
0.16
0.05 u
0.99
1.04
0.032
32.5
0.006
0.001
WR1
9/30/2005
1445
29.7
7.41
7.11
2
0.05 u
0.05 u
0.71
0.76
0.029
26.2
0.010
0.001
JR1
9/30/2005
1047
27.81
9.15
7.49
5
0.05 u
0.05 u
0.99
1.04
0.093
11.2
0.020
0.001
Pearl"!*
9/30/2005
1615
30.15
2.22
6.91
0.07
0.05 u
0.73
0.78
0.062
12.6
0.007
0.000
* Sample was composited
EPA's recommended CCC amonia criteria for saltwater set at 0.035 mg/l
u - analyte not detected at or above reporting limit
j - identification of analyte is acceptable; reported value is an estimate
uj - analyte not detected at or above reporting limit. Reporting limit is an estimate
a - analyte analyzed in replicate. Reported value is an "average" of replicates
17
-------
6.2 Bacteriological Water Quality Sampling
The Federal Register Part 131-Water Quality Standards for bacteriological criteria sets
the designated bathing beach single sample maximum allowable density for marine waters at
104. This criteria is the most restrictive of the use classification criteria. None of the water
samples collected for Enterococci analysis exceeded this density during the study, table 10.
Table 10, Microbiological Analyses of Coastal Waters in Mississippi
Project # 05-0926
Water Quality Indicator: Enterococcus
ASTM Method using Enterolert
MDL: 10 cfu/100 ml for marine waters
Results derived from the MPN
Sample ID Date/Time (most probable number)
Bayou Casotte & Bangs Lake
BC1 water
9/27/05 12:30
10
BC1 water (duplicate)
9/27/05 12:30
10
BC2 water
9/27/05 12:50
<10
BC3 water
9/27/05 13:00
<10
BC4 water
9/27/05 13:15
30
BL1 water
9/27/05 14:45
<10
BC2 sediment
9/27/05 11:30
1000
BC4 sediment
9/27/05 12:40
2000
BC4 sediment (duplicate)
9/27/05 13:00
2000
BL1 sediment
9/27/05 14:45
1000
Pascagou
a, Escatawpa, West Pascagoula Rivers
PR1 water
9/28/05 13:15
96
WPR2 water
9/28/05 14:20
41
ER2 water
9/28/05 14:30
<10
ER1 water
9/28/05 14:00
10
WPR1 water
9/28/05 16:00
51
WPR1 sediment
9/28/05 11:50
5100
PR1 sediment
9/28/05 13:20
1000
ER1 sediment
9/28/05 14:00
1000
ER1 sediment (duplicate)
9/28/05 14:30
1000
PR2 sediment
9/28/05 15:30
4100
Back Bay of Biloxi
BBB6 water
9/29/05 10:05
<10
BBB5 water
9/29/05 10:20
10
BBB4 water
9/29/05 10:30
10
BBB3 water
9/29/05 10:45
<10
BBB2 water
9/29/05 11:00
<10
BBB1 water
9/29/05 11:15
<10
BBB1 water (duplicate)
9/29/05 11:15
<10
BBB3 sediment
9/29/05 09:45
13,000
18
-------
Table 10, Microbiological Analyses of Coastal Waters in Mississippi
Project # 05-0926
Water Quality Indicator: Enterococcus
ASTM Method using Enterolert
MDL: 10 cfu/100 ml for marine waters
Results derived from the MPN
Sample ID Date/Time (most probable number)
BBB3 sediment (duplicate)
9/29/05 10:05
11,900
BBB6 sediment
9/29/05 11:20
3000
St. Louis Bay, Bayou Caddy, Pearl River
BLC1 water
9/30/05 8:20
41
JR1 water
9/30/05 8:35
20
SLB7 water
9/30/05 8:42
20
SLB5 water
9/30/05 8:50
10
SLB6 water
9/30/05 8:58
<10
SLB3 water
9/30/05 9:03
10
SLB4 water
9/30/05 9:11
<10
SLB2 water
9/30/05 9:20
20
SLB1 water
9/30/05 9:28
<10
WR1 water
9/30/05 9:44
52
BC1 water
9/30/05 11:15
10
Pearl 1 water
9/30/05 16:50
10
Pearl 1 sediment
9/29/05 16:45
<1000
SLB6 sediment
9/30/05 10:40
13,000
SLB6 sediment (duplicate)
9/30/05 11:00
10,800
SLB3 sediment
9/30/05 12:30
7300
SLB2 sediment
9/30/05 15:20
3100
6.3 In-Situ Monitoring
The two parameters that have associative water quality criteria for the in-situ profiling are
dissolved oxygen and temperature. The MDEQ criteria for dissolved oxygen states that in
thermally stratified waters, such as lakes, estuaries, and impounded streams, dissolved oxygen
concentrations shall be maintained with an instantaneous minimum of not less than 4.0 mg/1 with
the exception of a portion of Escatawpa which is set at 3 mg/1 (MDEQ, 2003). State ambient
water quality criteria were met at all study stations with the exception of two noted in the profiles
in Appendix stations. Of these exceptions, one was station ER2 in Escatawpa River. This
station is located near the fish processing plant and the now closed IP pulp and paper mill. The
second station was station BLC1 described as at Bayou LaCroix, a tributary to St Louis Bay.
None of the study stations exceeded the criteria for temperature. All temperatures were less than
the maximum allowable temperature of 32.2 ° C. The specific profiles for this monitoring can be
found in Appendix D
The in-situ data showed that Bangs Lake, Bayou Casotte, Pascagoula River, Escatawpa
River, and West Pascagoula River systems were the most saline and lowest in dissolved oxygen,
19
-------
Table 11. In contrast, less salinity and higher average dissolved oxygen were observed within
the Back Bay of Biloxi and St. Louis Bay systems.
Table 11
Summary of In-Situ Profiles
Water Quality Study of Bays in Coastal Mississippi
System
Station
Date
Time
Depth
Dissolved Oxygen (mg/l)
Salinity (ppt)
T emperature (degree C)
(ft)
Max
Avg
Min
Max
Avg
Min
Max
Avg
Min
Bangs Lake
BL1
9/27/2005
1245
3
6.82
6.38
5.71
23.59
23.56
23.54
29.67
29.36
28.84
Bayou Casotte
BC1
9/27/2005
1110
43
5.64
4.61
3.69
30
28.97
27.2
28.74
28.42
28.33
Bayou Casotte
BC2
9/27/2005
1310
43
6.25
4.54
3.91
29.8
28.76
26.4
29.44
28.51
28.3
Bayou Casotte
BC3
9/27/2005
1505
43
6.79
4.32
3.25
29.8
28.91
25.7
29.55
28.49
28.3
Bayou Casotte
BC4
9/27/2005
1435
2
12.82
11.46
9.25
31.27
30.33
30.75
West Pascagoula River
WPR1
9/28/2005
-1045
26
6.77
5.35
4.81
25
20.45
5.63
28.77
28.55
28.22
West Pascagoula River
WPR2
9/28/2005
-1350
28
8.22
4.48
3.23
11.81
5.96
0.72
29.13
28.95
29.13
Pascagoula River
PR1
9/28/2005
- 1210
40
7.56
4.94
4.12
30.28
26.86
15.2
28.53
28.46
28.28
Pascagoula River
PR2
9/28/2005
-1530
23
6.33
4.1
2.94
26.46
14.26
2.21
28.97
28.65
28.06
Escatawpa River
ER1
9/28/2005
-1350
23
5.3
4.12
3.31
28.02
18.81
3.69
29.2
28.72
28.44
Escatawpa River
ER2
9/28/2005
-1105
19
3.35
2.54
2.25
21.45
13.62
1.8
28.84
28.63
28.32
Back Bay of Biloxi
BBB!
9/29/2005
1312
12
8.95
6.33
3.25
21.52
16.83
13.34
29.06
28.66
28.25
Back Bay of Biloxi
BBB2
9/29/2005
1025
11
7.35
6.25
5.27
15.28
12.25
8.59
28.58
28.15
27.99
Back Bay of Biloxi
BBB3
9/29/2005
935
7
6.92
6.24
4.97
11.59
8.83
7.8
28.78
27.31
20.1
Back Bay of Biloxi
BBB4
9/29/2005
1250
10
7.62
6.03
3.95
6.75
4.5
4.07
29.17
28.69
28.45
Back Bay of Biloxi
BBB5
9/29/2005
1130
9
7.33
5.46
3.75
8.83
5.7
4.13
29
28.58
28.36
Back Bay of Biloxi
BBB6
9/29/2005
1000
15
7.58
3.32
0.54
4.53
3.38
2.43
28.9
28.49
28.74
St. Louis Bay
SLB1
9/30/2005
1225
11
7.74
7.09
6.47
15.29
15.24
15.21
29.06
28.3
27.85
St. Louis Bay
SLB2
9/30/2005
-1400
6
8.9
8.03
6.77
14.65
14.04
13.77
29.06
28.73
27.98
St. Louis Bay
SLB3
9/30/2005
-1125
8
8.68
7.59
6.94
14.51
14.15
13.25
28.62
28.44
28.35
St. Louis Bay
SLB4
9/30/2005
1315
4
8.32
7.21
5.51
13.07
12.72
12.5
28.68
28.47
28.09
St. Louis Bay
SLB5
9/30/2005
1230
5
7.98
7.73
7.28
12.26
12.11
12.02
28.8
28.37
27.88
St. Louis Bay
SLB6
9/30/2005
-0940
7
6.56
5.91
3.06
12.83
11.9
11.55
28.24
28.04
27.97
St. Louis Bay
SLB7
9/30/2005
1125
5
7.71
7.34
6.38
11.15
10.74
10.53
28.45
28.07
27.76
Wolf River
WR1
9/30/2005
1435
4
7.75
7.49
7.21
9.02
8.03
7.06
29.7
29.4
29.07
Jordan River
Jr1
9/30/2005
1045
9
6.93
6.74
6.55
9.28
8.82
7.49
27.86
27.71
27.64
Bayou La Croix
BLC1
9/30/2005
945
9
5.03
4.04
3.63
7.72
6.31
5.12
28.83
28.58
28.24
Bayou Caddy
BCD1
9/30/2005
945
9
6.18
6.16
6.15
14.27
14.26
14.27
28.86
28.84
28.83
Pearl River
Pearl 1
9/30/2005
1545
17
7.01
3.9
1.88
4.26
3.34
2.15
30.32
29.46
29.01
6.4 Sediment Sampling
All sediment results were compared to Threshold Effects Levels (TEL) and Probable
Effect Levels (PEL) summarized in the NOAA Screening Quick References Tables (SQuiRT's)
[MacDonald (1994), Long (1991), Long (1995)]. The TELs represent concentrations below
which adverse effects are expected to rarely occur. PELs are concentrations above which
adverse effects are frequently expected. TELs and PELs are not available for every contaminant
analyzed in this study. Only those contaminants that have published TELs and PELs were
evaluated in this assessment. Additional literature reviews are required to evaluate all other
detected contaminants.
Only two sampling areas had sediment concentrations above the TELs, Bayou Casotte
and St. Louis Bay (Tables 12-15). Both sediment sampling locations in Bayou Casotte had
cadmium concentrations above the TEL of 0.68 ppm. Locations BC2SD and BC4SD had
cadmium concentrations of 1.1 and 1.8 ppm, respectively. One location, BC2SD, had zinc (140
ppm), lead (36 ppm) and copper (20 ppm) concentrations that exceeded their respective TELs.
Although these concentrations exceed the TELs, they do not exceed their respective PELs.
Bay St. Louis only had one exceedence of the TELs. Location SLB6SD had an arsenic
concentration of 9 ppm, which exceeds the arsenic TEL of 7.24 ppm. The arsenic PEL is 41.6
ppm. Although arsenic exceeds the TEL, it is well below the PEL.
20
-------
Five sediment samples were also collected from the Pascagoula/Escatawpa system (three
locations) and St Louis Bay (two locations) for dioxin analysis. The locations were based on
recommendations made by MDEQ. The analyses were conducted by an EPA contract laboratory.
The results for each sample collected are reported for individual compounds and summarized
into a toxic equivalent value (TEQ). The toxic equivalent value is computed for birds, fish and
mammals. A comparison was then made against the World Health Organization (WHO) low and
high risk screening values. Of the five stations sampled, four were found to have toxic
equivalent values higher than the low risk mammalian wildlife value as shown in Table 16.
However, none of the values exceeded the "effects value" of 25 ng/kg (TEQ) (EPA, 1993). All
of the concentrations measured were well below the EPA screening value for residential soils
(1,000 ng/kg); additionally, there are no known human health effects associated with this level of
dioxin in sediment (Personal Communication with Scott Sudweeks, Chief, Technical Services
Section, Region 4 Waste Management Division).
21
-------
Table 12
Chemical Sediment Data- Detectable Concentrations- Bangs Lake & Bayou Casotte
Septemebr 27-30, 2005
Metals Scan
TEL*
PEL**
BC2SD
9/27/2005
1130
BC4DSD
9/27/2005
1300
BC4SD
9/27/2005
1240
BL1SD
9/27/2005
1415
% Moisture
%
60
41
49
A
39
Aluminum
7429-90-5
MG/KG
8200
2600
3000
1800
A
Arsenic
7440-38-2
MG/KG
7.24
41.6
6.4
1.2
0.87
2.4
A
Barium
7440-39-3
MG/KG
130
27
57
6.6
A
Beryllium
7440-41-7
MG/KG
0.82
0.3
0.3
U
Cadmium
7440-43-9
MG/KG
0.68
4.2
1.1
1.5
1.8
U
Calcium
7440-70-2
MG/KG
7400
4900
4700
1000
A
Chromium
7440-47-3
MG/KG
52.3
81
21
7.2
9.7
4.5
A
Cobalt
7440-48-4
MG/KG
4.6
0.59
0.66
1.1
A
Copper
7440-50-8
MG/KG
18.7
108.2
20
4.7
5.5
1.9
A
Iron
7439-89-6
MG/KG
17000
3400
3200
4900
A
Lead
7439-92-1
MG/KG
30.2
112.2
36
4.8
5.9
4.1
A
Magnesium
7439-95-4
MG/KG
5100
1800
1700
1400
A
Manganese
7439-96-5
MG/KG
450
26
26
46
A
Nickel
7440-02-0
MG/KG
15.9
42.8
8.4
2.4
2.7
2
A
Potassium
7440-09-7
MG/KG
2300
510
450
630
A
Sodium
7440-23-5
MG/KG
18000
8500
5900
5300
AJ
Strontium
7440-24-6
MG/KG
57
59
66
10
A
Titanium
7440-32-6
MG/KG
17
12
14
7.6
AJ
Total Mercury
7439-97-6
MG/KG
0.13
0.7
0.078
U
U
U
Vanadium
7440-62-2
MG/KG
24
6.1
7.3
9.5
A
Yttrium
7440-65-5
MG/KG
12
2.7
2.5
2.4
A
Zinc
7440-66-6
MG/KG
124
271
140
48
55
14
A
PCB Scan
None Detected
Pesticides Scan
tone Detected
Volatiles Scan
% Moisture
%
60
41
50
39
1,2,3-Trichlorobenz<
87-61-6
UG/KG
1.8
J
U
U
U
Benzene
71-43-2
UG/KG
0.23
J
U
U
U
Carbon Disulfide
75-15-0
UG/KG
4.7
J
3.2
4.4
0.73
J
Isopropylbenzene
98-82-8
UG/KG
14
U
U
U
n-Butyl benzene
104-51-8
UG/KG
50
J
U
U
U
n-Propyl benzene
103-65-1
UG/KG
51
J
U
U
U
p-lsopropyltoluene
99-87-6
UG/KG
43
J
U
U
U
sec-Butyl benzene
135-98-8
UG/KG
30
J
U
U
U
Miscellaneous Volatiles
Petroleum Products
UG/KG
N
NR
NR
NR
Thiobism ethane
UG/KG
NR
200
NJ
NR
30
NJ
Extractables Scan
% Moisture
%
63.61
29.58
33.67
35.82
Fluoranthene
206-44-0
UG/KG
112.8
1493.5
U
66
J
U
U
Pyrene
129-00-0
UG/KG
152.7
1397.6
U
63
J
U
U
Classical Nutrients
Ammonia
7664-41-7
MG/KG
55
15
13
5.5
Total Kjeldahl Nitroc
MG/KG
1400
430
330
450
Total Organic Carbon
MG/KG
17000
U
U
U
Total Phosphorus
7723-14-0
MG/KG
1200
1800
2400
61
Shaded areas identify analyte detected is above sediment quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
22
-------
Table 13
Chemical Sediment Data- Detectable Concentrations-Pascagoula River, Escatawpa River, and West Pascagoula River
September 27-30, 2005
Metals Scan
TEL
PEL
ER1DSD
9/28/2005
1430
ER1SD
9/28/2005
1400
PR1SD
9/28/2005
1320
PR2SD
9/28/2005
1545
WPR1SD
9/28/2005
1150
% Moisture
%
23
20
69
16
34
Aluminum
7429-90-5
MG/KG
180
A
210
5600
3700
1800
Arsenic
7440-38-2
MG/KG
7.24
41.6
U
U
6.6
3.3
1.7
Barium
7440-39-3
MG/KG
1.7
A
1
24
19
5.4
Beryllium
7440-41-7
MG/KG
U
U
0.88
0.68
U
Cadmium
7440-43-9
MG/KG
0.68
4.2
U
U
0.38
0.28
U
Calcium
7440-70-2
MG/KG
71
A
50
2600
960
410
Chromium
7440-47-3
MG/KG
52.3
160.4
U
U
12
6.5
3.4
Cobalt
7440-48-4
MG/KG
U
U
5.6
7.7
2
Copper
7440-50-8
MG/KG
18.7
108.2
UJ
UJ
12
5.9
2.5
Iron
7439-89-6
MG/KG
270
A
370
16000
9900
4300
Lead
7439-92-1
MG/KG
30.24
112.8
2.1
A
1.3
16
8.1
3.8
Magnesium
7439-95-4
MG/KG
200
A
120
4500
2000
1200
Manganese
7439-96-5
MG/KG
1.7
A
2.5
270
130
38
Nickel
7440-02-0
MG/KG
15.9
42.8
U
U
6.1
3.9
1.9
Potassium
7440-09-7
MG/KG
U
U
1600
900
510
Selenium
7782-49-2
MG/KG
U
U
0.73
U
U
Sodium
7440-23-5
MG/KG
1300
A
540
20000
7300
5400
Strontium
7440-24-6
MG/KG
1.5
A
1.1
39
19
8.1
Titanium
7440-32-6
MG/KG
2.6
AJ
2.8
J
22
J
13
J
11
J
Total Mercury
7439-97-6
MG/KG
0.13
0.7
U
u
0.055
U
U
Vanadium
7440-62-2
MG/KG
UJ
UJ
25
14
6.3
Yttrium
7440-65-5
MG/KG
U
u
11
8
3.6
Zinc
7440-66-6
MG/KG
124
271
1.6
A
1.9
71
30
15
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
% Moisture
%
23
20
69
55
34
Benzene
71-43-2
UG/KG
U
u
U
0.18
J
U
Carbon Disulfide
75-15-0
UG/KG
U
u
4.4
J
1.4
J
UJ
Extractables Scan
None Detected
Classical Nutrients
Ammonia
7664-41-7
MG/KG
3.4
u
78
41
4
Total Kjeldahl Nitrogen
MG/KG
57
57
2200
1200
430
Total Organic Carbon
MG/KG
U
u
u
15000
U
Total Phosphorus
7723-14-0
MG/KG
U
u
330
180
86
Shaded areas identify analyte detected is above sediment quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-Identification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
23
-------
Table 14
Chemical Sediment Data - Detectable Concentrations- Back Bay of Biloxi
September 27-30, 2005
BBB3DSD
BBB3SD
BBB6SD
9/29/2005
9/29/2005
9/29/2005
Metals Scan
TEL PEL
1005
945
1120
% Moisture
%
69
66
62
Aluminum
7429-90-5
MG/KG
7000
7800
5800 A
Arsenic
7440-38-2
MG/KG
7.24 41.6
5.2
5.5
4.7 A
Barium
7440-39-3
MG/KG
14
16
22 A
Beryllium
7440-41-7
MG/KG
0.99
1.1
0.57 A
Cadmium
7440-43-9
MG/KG
0.68 4.2
0.42
0.46
0.31 A
Calcium
7440-70-2
MG/KG
1400
1400
1700 A
Chromium
7440-47-3
MG/KG
52.3 370
12
12
11 A
Cobalt
7440-48-4
MG/KG
5.9
6
3.4 A
Copper
7440-50-8
MG/KG
18.7 108.2
14 J
15 J
13 AJ
Iron
7439-89-6
MG/KG
14000 J
15000 J
12000 AJ
Lead
7439-92-1
MG/KG
30.24 112.18
18
20
16 A
Magnesium
7439-95-4
MG/KG
3200
3200
2200 A
Manganese
7439-96-5
MG/KG
140
140
93 A
Molybdenum
7439-98-7
MG/KG
U
0.61
0.72 A
Nickel
7440-02-0
MG/KG
15.9 42.8
5.9 J
6.2 J
UJ
Potassium
7440-09-7
MG/KG
1200
1300
840 A
Selenium
7782-49-2
MG/KG
1
1.2
0.57 A
Sodium
7440-23-5
MG/KG
6800
6000
5600 A
Strontium
7440-24-6
MG/KG
27
28
24 A
Titanium
7440-32-6
MG/KG
12
11
9 AJ
Total Mercury
7439-97-6
MG/KG
0.13 0.7
0.069
0.07 A
U
Vanadium
7440-62-2
MG/KG
16
17
16 A
Yttrium
7440-65-5
MG/KG
12
13
7.2 A
Zinc
7440-66-6
MG/KG
124 271
63
66
82 A
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
% Moisture
%
69
66
62
1,3,5-Tri methyl benzene
108-67-8
UG/KG
U
U
2 J
Isopropylbenzene
98-82-8
UG/KG
U
U
0.87 J
Methyl Ethyl Ketone
78-93-3
UG/KG
11 J
UJ
UJ
n-Butyl benzene
104-51-8
UG/KG
U
U
3.6 J
n-Propy I benzene
103-65-1
UG/KG
U
U
2.1 J
o-Xylene
95-47-6
UG/KG
U
U
0.39 J
p-lsopropyltoluene
99-87-6
UG/KG
U
U
2 J
sec-Butyl benzene
135-98-8
UG/KG
U
U
1.7 J
Extractables Scan
% Moisture
%
70
68.22
62.62
Fiuoranthene
206-44-0
UG/KG
112 1493
U
U
150 J
Pyrene
129-00-0
UG/KG
152.7 1397.6
U
U
120 J
Classical Nutrients
Ammonia
7664-41-7
MG/KG
52
77
91
Total Kjeldahl Nitrogen
MG/KG
2300
2400
1700
Total Organic Carbon
MG/KG
26000
28000
20000
Total Phosphorus
7723-14-0
MG/KG
300
330
430
Shaded areas identify analyte detected is above sediment quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-Identification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-Identification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
n ^/-vr,firrr,a/H Kw riOH/IQ I M u
-------
Table 15
Chemical Sediment Data - Detectable Concentrations- St Louis Bay, Bayou Caddy, and Pearl River
September 27-30, 2005
Metals Scan
TEL
PEL
PEARL1SD
9/29/2005
1645
SLB2SD
9/30/2005
1520
SLB3SD
9/30/2005
1230
SLB6DSD
9/30/2005
1100
SLB6SD
9/30/2005
1040
% Moisture
%
65
23
52
56
57
Aluminum
7429-90-5
MG/KG
5600
1200
A
4600
6600
6100
Arsenic
7440-38-2
MG/KG
7.24
41.6
3.4
1.5
A
4.4
8.9
9
Barium
7440-39-3
MG/KG
37
6.7
A
18
19
18
Beryllium
7440-41-7
MG/KG
0.86
U
0.51
0.77
0.72
Cadmium
7440-43-9
MG/KG
1.2
4.2
0.2
U
0.17
0.24
0.21
Calcium
7440-70-2
MG/KG
1800
1400
A
2600
4400
1700
Chromium
7440-47-3
MG/KG
52.3
160.4
10
2
A
6.6
10
9.4
Cobalt
7440-48-4
MG/KG
4.2
1.6
A
4.8
7.7
7.5
Copper
7440-50-8
MG/KG
18.7
108.2
9.6
J
1.5
A
5.2
6.7
6.2
Iron
7439-89-6
MG/KG
8800
J
3000
A
10000
16000
16000
Lead
7439-92-1
MG/KG
30.2
112.2
17
3.2
A
9.8
15
14
Magnesium
7439-95-4
MG/KG
3000
700
A
2600
3500
3300
Manganese
7439-96-5
MG/KG
160
78
A
210
260
240
Molybdenum
7439-98-7
MG/KG
0.99
U
U
U
U
Nickel
7440-02-0
MG/KG
15.9
42.8
8.3
J
1.5
A
5.4
8
7.6
Potassium
7440-09-7
MG/KG
1000
340
A
1200
1600
1500
Selenium
7782-49-2
MG/KG
0.66
U
U
U
U
Sodium
7440-23-5
MG/KG
3100
1600
A
5600
5900
5900
Strontium
7440-24-6
MG/KG
31
10
A
26
37
22
Titanium
7440-32-6
MG/KG
16
12
AJ
17
J
20
J
19
J
Vanadium
7440-62-2
MG/KG
17
3.5
A
13
19
18
Yttrium
7440-65-5
MG/KG
14
2.6
A
7.9
11
10
Zinc
7440-66-6
MG/KG
124
270
22
9.7
A
32
42
41
PCB Scan
None Detected
Pesticides Scan
None Detected
Volatiles Scan
% Moisture
%
66
23
52
56
57
1,3,5-T rim ethyl benzene
108-67-8
UG/KG
0.25
J
U
U
U
U
o-Xylene
95-47-6
UG/KG
0.21
J
U
U
u
u
p-lsopropyltoluene
99-87-6
UG/KG
3.4
J
U
U
u
u
Extractables Scan
% Moisture
%
67.8
23.22
54.05
55.91
57.75
Benzo(a)Anthracene
56-55-3
UG/KG
74.83
1600
U
58
J
U
u
u
Benzo(b)Fluoranthene
205-99-2
UG/KG
U
130
J
U
u
u
Benzo(ghi)Perylene
191-24-2
UG/KG
U
74
J
U
u
u
Benzo(k)Fluoranthene
207-08-9
UG/KG
U
120
J
U
u
u
Benzo-a-Pyrene
50-32-8
UG/KG
88
1600
U
130
J
U
u
u
Chrysene
218-01-9
UG/KG
107.8
2800
U
82
J
U
u
u
Dibenzo(a,h)Anthracene
53-70-3
UG/KG
6.22
134.61
U
47
J
U
u
u
Fluoranthene
206-44-0
UG/KG
112.8
1493.5
U
98
J
U
u
u
indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
U
84
J
U
u
u
Pyrene
129-00-0
UG/KG
152.7
1397.6
U
170
J
U
u
u
Classical Nutrients
Ammonia
7664-41-7
MG/KG
22
U
17
16
17
Total Kjeldahl Nitrogen
MG/KG
2500
270
940
1300
1200
Total Organic Carbon
MG/KG
58000
U
16000
14000
13000
Total Phosphorus
7723-14-0
MG/KG
100
65
160
170
160
Shaded areas identify analyte detected is above sediment quality criteria
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-Identification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
-------
Table 16
Sediment Dioxin Results
Pascagoula, Escatawpa, and St. Louis Bays
Septemebr 28&30, 2005
ER1DSD
ER1SD
PR1SD
PR2SD
SLB2SD
SLB6SD
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/30/2005
9/30/2005
Dioxin Scan
1430
1400
1320
1545
1520
1040
% Moisture
%
21
19
51
52
23
55
1,2,3,4,6,7,8-Heptachlorodibenzodioxin
35822-46-9
NG/KG
7
11
220
290
50
330
1,2,3,4,6,7,8-Heptachlorodibenzofuran
67562-39-4
NG/KG
CO
U
0.47 U
8.9
9
1.4 J
9.1
1,2,3,4,7,8,9-Heptachlorodibenzofuran
55673-89-7
NG/KG
1.1
J
0.15 U
0.8 J
0.7 U
0.15 J
1.1 U
1,2,3,4,7,8-Hexachlorodibenzodioxin
39227-28-6
NG/KG
1.9
U
0.24 J
2 J
1.9 J
0.56 J
3.9
1,2,3,4,7,8-Hexachlorodibenzofuran
70648-26-9
NG/KG
2.2
U
0.15 U
1.2 U
0.78 U
0.17 U
1 U
1,2,3,6,7,8-Hexachlorodibenzodioxin
57653-85-7
NG/KG
1.9
U
0.39 J
4.7
6.2
1.1 J
7.5
1,2,3,6,7,8-Hexachlorodibenzofuran
57117-44-9
NG/KG
11
U
0.14 U
0.58 U
0.56 U
0.17 U
1.1 U
1,2,3,7,8,9-Hexachlorodibenzodioxin
19408-74-3
NG/KG
2
U
0.72 J
8.9
12
2.3
16
1,2,3,7,8,9-Hexachlorodibenzofuran
72918-21-9
NG/KG
0.68
J
0.15 U
0.37 U
0.35 U
0.089 U
0.36 U
1,2,3,7,8-Pentachlorodibenzodioxin
40321-76-4
NG/KG
1.5
U
0.14 U
0.67 J
0.74 J
0.22 J
1.2 J
1,2,3,7,8-Pentachlorodibenzofuran
57117-41-6
NG/KG
1.5
U
0.16 U
0.4 U
0.25 U
0.1 U
0.4 U
2,3,4,6,7,8-Hexachlorodibenzofuran
60851-34-5
NG/KG
1.1
J
0.17 U
0.77 U
0.71 U
0.17 U
1.4 U
2,3,4,7,8-Pentachlorodibenzofuran
57117-31-4
NG/KG
1.4
U
0.2 U
0.77 U
0.43 U
0.15 U
0.58 U
2,3,7,8-Tetrachlorodibenzodioxin
1746-01-6
NG/KG
0.21
U
0.19 U
1.1
0.81 J
0.1 U
0.3 U
2,3,7,8-T etrachlorodibenzofuran
51207-31-9
NG/KG
1.1
U
1.6 U
12
2.4
0.16 U
0.53 U
Heptachlorodibenzodioxin (Total)
NG/KG
19
J
30 J
870 J
840 J
180 J
1200 J
Heptachlorodibenzofuran (Total)
38998-75-3
NG/KG
1.1
J
0.37 J
30 J
28 J
3.4 J
22 J
Hexachlorodibenzodioxin (Total)
34465-46-8
NG/KG
1.9
UJ
11 J
270 J
250 J
75 J
520 J
Hexachlorodibenzofuran (TotaI)
55684-94-1
NG/KG
22
J
0.33 J
13 J
11 J
1.6 J
11 J
Octachlorodibenzodioxin
3268-87-9
NG/KG
170
300
5000 J
10000 J
1100
5700 J
Octachlorodibenzofuran
39001-02-0
NG/KG
5.9
0.8 J
18
20
3.2 J
19
Pentachlorodibenzodioxin (Total)
36088-22-9
NG/KG
1.5
UJ
1.4 J
38 J
33 J
11 J
84 J
Pentachlorodibenzofuran (T ota I)
30402-15-4
NG/KG
9.1
J
0.21 J
4 J
4.1 J
0.57 J
6.1 J
Tetrachlorodibenzodioxin (Total)
41903-57-5
NG/KG
0.54
J
0.63 J
28 J
25 J
5.5 J
44 J
Tetrachlorodibenzofuran (Total)
55722-27-5
NG/KG
12
J
2.9 J
28 J
7.5 J
0.74 J
7.9 J
TEQ (Avian Toxic. Equiv. Value, From WHO TEQ (1998))
NG/KG
6.2 J
2.3 J
17 J
7.4 J
1.2 J
5.8 J
TEQ (Fish Toxic. Equiv. Value, From WHO TEQ (1998))
NG/KG
5.1
J
0.75 J
5 J
4.7 J
1 J
5.3 J
TEQ (Mammalian Toxic. Equiv. Value, From WHO TEQ (1998
i)) NG/KG
4.8 J
0.93 J
8 J
8.3 J
1.5 J
8.9 J
Shaded entries indicate exceedence of EPA screening values (below)
EPA Sediment Screening Values (USEPA1993) TEQ (NG/KG) Low Risk High Risk
Fish 60 100
Mammalian Wildlife 2.5* 25
Avian Wildlife 21 210
* The 2.5 mammalian screening value is based on effect value of 25 ng/kg (I* EPA (1993) with an applied safety factor or 10.
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
6.5 Bay Outlet Loading to MS Sound
Loading measurements were made for the outlets from Bayou Casotte, Pascagoula River,
West Pascagoula River, Back Bay of Biloxi, St. Louis Bay and Pearl River (Tables 16-19). Flow
was measured using a boat mounted Doppler current meter. Every attempt was made to make
the loading measurements at mid-ebb tide. Samples for the respective water columns were
collected and analyzed from mid depth of the center of the main hydraulic conveyance outlet. A
tide chart recorder located at Keesler AFB on Back Bay of Biloxi depicts the estimated point of
sampling and flow measurement at each outlet, Figure 11. As such, the only outlet system that
accurately reflects the timing relative to the tidal stage is for Back Bay of Biloxi. The timing for
the other loading outlet measurements were estimates based on the tidal lag irrespective to the
effect of the wind, Figure 12.
26
-------
The results for the algal growth potential test (AGPT) at the bay & river outlets are found
in Table 19 and Figure 13. The AGPT numbers for all of the bay & river systems were low with
the exception of Bayou Casotte and Back Bay of Biloxi. The algal growth potential within
Bayou Casotte was exceptionally high. This result was likely tied to the nutrient enriched
discharge from Mississippi Phosphates to Bayou Casotte.
Figure 11, Tidal Curve - Back Bay of Biloxi
@ Keesler AFB
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9/26/2005
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10/01/2005
27
-------
Table 17
Bay Outlet Metal Loading
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Detectable Metals scan (mg/l) compounds
System
Station
Flow
Date
Time
Calcium
Iron
Magnesium
Potassium
Sodium
cfs
mg/l
ton/day
mg/l ton/day
mg/l
ton/day
mg/l
ton/day
mg/l
ton/day
Bayou Casotte
BC1
1591
9/27/2005
1134
350
1501
1100
4717
360
1544
9200
39454
Pascagoula River
PR1
17968
9/28/2005
1240
330
15982
1000
48432
340
16467
8700
421355
West Pascagoula River
WPR1
17618
9/28/2005
1115
260
12347
840
39890
260
12347
6900
327668
Back Bay of Biloxi
BBB1
36514
9/29/2005
1312
160
15747
490
48226
160
15747
3950
388763
St Louis Bay
SLB1
44835
9/30/2005
1230
180
21753
550
66467
170
20544
4500
543824
Pearl River
PearM
6500
9/30/2005
1615
40
701
0.76 13
110
1927
38
666
930
16294
Detectable Metals scan (ug/l) compounds
System
Station
Flow
Date
Time
Arsenic
Barium
Manganese
Selenium
Strontium
cfs
ug/l
ton/day
ug/l ton/day
ug/l
ton/day
ug/l
ton/day
ug/l
ton/day
Bayou Casotte
BC1
1591
9/27/2005
1134
45 J
0.2
150 J
0.6
6100
26.2
Pascagoula River
PR1
17968
9/28/2005
1240
46 J
2.2
150 J
7.3
5600
271.2
West Pascagoula River
WPR1
17618
9/28/2005
1115
34 J
1.6
98
4.7
110 J
5.2
5200
246.9
Back Bay of Biloxi
BBB1
36514
9/29/2005
1312
25 J
2.5
64
6.3
77 J
7.6
2850
280.5
St Louis Bay
SLB1
44835
9/30/2005
1230
22 J
2.7
61 7.4
64 J
7.7
3000
362.5
Pearl River
Pearl 1
6500
9/30/2005
1615
4.6 J
0.1
61 1.1
870
15.2
11 J
0.2
640
11.2
J
identification of analyte is acceptable; reported value is an estimate
Table 18
Bay Outlet Nutrient Loading
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Detectable Nutrient Compounds
System
Station
Flow
Date
Time
TOC
NH3
N02-N03
TKN
Total N
Total
P
cfs
mq/l
ton/dav
mq/l
ton/dav
mq/l
ton/dav
mq/l
ton/dav
mq/l
ton/dav
mq/l
ton/dav
Bayou Casotte
BC1
1591
9/27/2005
1205
1.40
6.0
0.08
0.3
0.06
0.2
0.25
1.1
0.31
1.3
0.22
0.9
Pascagoula River
PR1
17968
9/28/2005
1240
1.60
77.5
0.07
3.5
0.06
2.7
0.29
14.0
0.35
16.8
0.09
4.2
West Pascagoula River
WPR1
17618
9/28/2005
1115
2.50
118.7
0.08
3.9
0.05 u
2.4
0.45
21.4
0.50
23.7
0.06
3.0
Back Bay of Biloxi
BBB1
36514
9/29/2005
1340
8.10
797.2
0.05 u
4.9
0.05 u
4.9
0.68
66.9
0.73
71.8
0.04
3.9
St Louis Bay
SLB1
44835
9/30/2005
1230
4.50
543.8
0.05 u
6.0
0.05 u
6.0
0.55
66.5
0.60
72.5
0.03
3.6
Pearl River
PearM
6500
9/30/2005
1615
7.80
136.7
0.07
1.2
0.05 u
0.9
0.73
12.8
0.78
13.7
0.06
1.1
28
-------
Table 20
Algal Growth Potential Test - Mississippi Bay Outlet Results
September 27-30, 2005
AGPT- MSC, mq/L (Dry Weight)
Limiting
Station
Control
C+N
C+P C+N+P
Nutrient
Marine Test
BC1
55.1
107
56.3
N
Dunaliella
BL1
3.9
57.5
2.5
N
PR1
3.8
5.5
4.1
N
WPR1
4.1
6.9
4.8
N
BBB1
7.5
5.8
6.9
ND
SLB1
4.0
4.6
3.4
ND
FW Test
Pearl-1
0.80
7.1
1.1
N
Selenastrum
Excessive growth for marine waters is considered 5 mg/l (dry weight)
AGPT - Algal Growth Potential Test
MSC - Maximum Standing Crop
C+N - Control + 1.0 mg/L Nitrate-N
C+P - Control + 0.05 mg/L Phosphate-P
C+N+P - Control + 1.0 mg/L Nitrate-N + 0.05 mg/L Phosphate-P
FW - Freshwater AGPT using Selenastrum as test alga
ND - Not Determined
Fig. 13 MS Gulf Coast AGPT
Se pte m be r 27 - 30, 2005
107
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6.3
57.5
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3.85-54.1
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WPR1
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BBB1
SLB1
Ftearl-1
29
-------
7.0 Data Management
ASB performed data review and data verification. Data review is the in-house
examination process to ensure that the data were recorded, transmitted, and processed correctly.
ASB's data review procedures included review by the analyst generating the data (primary
analyst) and a second review by an analyst who was not directly responsible for performing the
analysis (secondary analysts). A final review was performed by the organic or inorganic
supervisor prior to reporting the data. ASB's detailed data review procedures are covered in
Section 5.5.7.7 of ASB's Quality Assurance Manual. Any departures from QAPP, method or
SOP specifications were noted in a narrative report sent to the data user/decision maker who then
evaluated the departures as to the overall effects on the project objectives. Limitations on the use
of the data were a result of the data validation process addressed in the project report.
7.1 Documentation and Records
Field log books were maintained according to the procedures in the EASOPQAM by
each sampling team for the duration of the field survey. Following completion of the field
surveys, the log books were placed in the project file by the project leader. Upon completion of
the final report, the log books and associated project records will be stored in the SESD Records
Center. Copies of the final report will be provided to MDEQ and EPA Region 4 Water
Management Division - Standards, Monitoring and TMDL Branch. A copy of the final report
will also be maintained in the SESD Records Center.
7.2 Quality Assurance and Quality Control
Sample handling variability can be a major source of error in sample collection
investigations. Some of that error was controlled by requiring that field investigators strictly
adhere to an approved sampling methodology, thereby helping ensure that samples are collected
correctly. However, other sources of error, such as cross contamination and storage and
transport conditions, do exist and cannot always be mitigated by using proper collection
methods. These other sources of error can be evaluated and monitored by collecting specific
quality control samples designed to detect positive or negative biases associated with sample
handling, storage, transport and spatial variability.
During this study, sampling activities were conducted according to strict protocols as
outlined in the methods section. In addition, field investigators collected specific quality control
samples for evaluating variability associated with sample handling and external contamination.
The following quality control samples were utilized during the study to assess the
sampling procedures used during field operations:
1. Water VOA Trip Blanks (VOA vials)
Water VOA trip blanks were utilized to determine if the water VOA samples were
contaminated during storage or transport while in the field. The trip blanks were
prepared in the laboratory prior to the sampling event. The trip blanks consisted of three
40 mL VOA vials. One trip blank was included with each shipment of VOA samples.
30
-------
2. Sediment VOA Trip Blanks (En Core® samplers)
Sediment VOA trip blanks were utilized to determine if the sediment VOA samples were
contaminated during storage or transport while in the field. Blank EnCore samplers were
prepared in the laboratory prior to the sampling event. One sediment trip blank was
included with each shipment of sediment samples.
3. Equipment Rinse Blanks
Equipment rinse blanks were used to assess the adequacy of field decontamination
procedures. The equipment decontaminated while in the field included the petite Ponar
sediment samplers and the vacuum head caps. One equipment rinse blank was collected
each day that decontamination of equipment occurred. The equipment rinse blank was
collected by capturing the analyte-free water which had been poured over/through the
sampling equipment as part of the decontamination process. The equipment rinse blank
was analyzed for the same suite of parameters as the sediment samples.
4. Preservative Blanks
Post study preservative blanks were collected to determine if contamination of
preservatives occurred during the sampling event. One preservative blank was collected
for each bottle of preservative used during the sampling event. One liter polyethylene
bottles filled with analyte-free water were provided by the laboratory prior to the
sampling event. At the completion of the sampling event, the preservative blanks were
prepared by preserving the bottles provided by the laboratory. The preservative blanks
were analyzed for the appropriate analytes based on the preservative used.
5. Temperature Blanks
Temperature blanks were prepared by filling containers with water and sealing. A
temperature blank was shipped with each cooler of samples requiring preservation by
cooling with ice to 4°C. The temperature blanks were measured at the time of receipt by
the laboratory.
6. Organic/Analyte Free Water System Blank
A blank water sample was prepared by collecting a water sample from the field
organic/analyte free water generating system at the end of the study. The purpose of this
sample was to measure positive bias associated with localized contamination of the water
generating system.
7. Duplicate Samples
Duplicate samples were collected at selected surface water and sediment sampling
locations as outlined in Table 1 to provide an initial estimate of the spatial variability of
pollutants in the water column and sediments.
The results from the quality control sampling can be found in Appendix G. The only
detectable concentrations were a low level of zinc and TOC in an equipment rinse blank, and a
negligible amount of toluene in the de-ionized water. All other quality control samples were
clean from any detectable compounds.
The project leader was responsible for all corrective actions that became necessary during
the field investigation.
31
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7.3 Data Validation/Verification
Data verification is the process for evaluating the completeness, correctness, and
compliance of a specific data set against the method, procedural, or contractual specifications.
ASB's analytical data is verified by the primary and secondary analyst against the procedural and
quality assurance requirements of the analytical methods which are utilized, and the ASB
internal standard operating procedure for the methods. Any data which did not meet the method
or QC requirements was either re-analyzed, or qualified to denote that method or QC criteria
were not met during the analysis. ASB's data verification procedures are described in detail in
Sections 5.7 - 5.10 of ASB's Quality Assurance Manual.
Data validation is an analyte- and sample-specific process that extends the evaluation of
data beyond data verification to determine the quality of a specific data set relative to the end
use. It focuses on the project's specifications, the needs of the decision makers/data users and
should note potentially unacceptable departures from the QA Project Plan. The data validation
for this project was performed by Region 4 SESD Quality Assurance Section (QAS) with
assistance from the Environmental Services Assistance Team (ESAT) data validators. Both
QAS and ESAT personnel are independent of the data generation process. In order to perform
the data review QAS/ESAT personnel was provided with copies of data packages generated
during the analytical process. The data packages included chain of custody reports, instrument
calibration curves, instrument raw data, sample preparation records, and quality control
information. The QAS/ESAT staff validated project data against the data quality objectives and
specifications described in the QAPP, the method requirements and ASB Standard Operating
Procedures.
8.0 Project Management
Data collection was managed through the Ecological Assessment Branch with guidance
from the Mississippi Department of Environmental Quality and Region 4 Water Management
Division. The project leader for EAB was Mark Koenig. Technical direction from MDEQ was
provided by Henry Folmar. Technical direction from EPA WMD was provided by Andrew
Bartlett, Chief of the Standards, Monitoring and TMDL Branch. The appropriate use of
historical EPA or MDEQ data for comparison to data generated from this study will be the
responsibility of the data user. The QAPP has undergone internal peer review by branch
scientists and the Quality Assurance Section. An external peer review by EPA's Science
Advisory Board was also completed. No oversight or audits in the field were scheduled for this
study. The data quality assessment (DQA) phase of this study consisted of a review of log books
and field data by the project leader to reconcile any problems with sample locations or
sampling/sample handling procedures. A review of the data and any associated data qualifiers
was part of the DQA process.
9.0 Project Schedule
Field work for this project was completed from Monday, September 26, 2005 through
Friday, September 30, 2005. Each geographic area (Figures 1-4) was sampled on separate days,
beginning with Bayou Casotte and moving westward through the study period. Sampling on the
Pearl River and Bayou Caddy system was conducted on the same day as the Bay St. Louis
sampling.
32
-------
Lab analyses were scheduled for completion within 14 days following receipt by the
Analytical Support Branch, or in the case of dioxin by the contract laboratory by October 21st.
The SESD laboratory needed only 11 days to complete the analytical work. The analytical data
were then subject to validation which was scheduled to add an additional 14 days before the final
data package was available to the Project Leader. The validated data was released before the
target date, (Table 21).
Table 21
Critical Project Deliverables
Deliverable
Assigned
Date Due
Date Completed
Produce Water Quality
Plan of Study
September 15, 2005
September 20, 2005
September 19, 2005
Water Quality Field
Study
September 26, 2005
October 3, 2005
October 1, 2005
Final Sample
Shipment
-
October 3, 2005
October 1, 2005
Sample Analysis
October 1, 2005
October 15, 2005
October 14, 2005
QA Data Review
October 14, 2005
October 28, 2005
October 21, 2005
Water Quality Data
Report
September 25, 2005
November 4, 2005
October 21, 2005
Final Report to SESD
Web Site
October 28, 2005
33
-------
10.0 References
EPA 2002a. Ecological Assessment Standard Operating Procedures and Quality Assurance
Manual, January 2002. Environmental Protection Agency, Region 4, Science and Ecosystem
Support Division, Ecological Assessment Branch, Athens, Georgia
EPA 2001. Environmental Investigation Standard Operating Procedures and Quality Assurance
Manual, November 2001. Environmental Protection Agency, Region 4, Science and Ecosystem
Support Division, Environmental Investigation Branch, Athens, Georgia
EPA 2004. Analytical Support Standard Operating Procedures and Quality Assurance Manual,
November 2004. Environmental Protection Agency, Region 4, Science and Ecosystem Support
Division, Analytical Support Branch, Athens, Georgia
EPA 2002b. United States Environmental Protection Agency - National Recommended Water
Quality Criteria: 2002, EPA-822-R-02-047, Office of Water, November 2002.
EPA 2002c. United States Environmental Protection Agency Region 4 Data Validation Standard
Operating Procedures for Chlorinated Dioxin, Version 3.0, Science and Ecosystem Support
Division, Office of Quality Assurance and Data Integration, May 2002.
USEPA 1993. Interim report on data and methods for assessment of 2, 3, 7, 8-
tetrachlorodibenzo-p-dioxin risks to aquatic life and associated wildlife. U.S. Environmental
Protection Agency, Office of Research and Development, EPA /600/ R-93/055.
EPA 2002d. United States Environmental Protection Agency National Guidelines for Dioxin
Data Review, OSWER 9240.1-37, EPA 540-R-02-003, Office of Emergency and Remedial
Response, August 2002.
MDEQ 2003. State of Mississippi Water Quality Criteria For Intrastate, Interstate and Coastal
Waters, Department of Environmental Quality, June 27, 2003
MacDonald Environmental Sciences, Ltd. Approach to the Assessment of Sediment Quality in
Florida Coastal Waters. Florida Department of Environmental Protection. November 1994.
Long, ER, and LG Morgan. 1991. The Potential for Biological Effects of Sediment-Sorbed
Contaminants Tested in the National Status and Trends Program. NOAA Technical
Memorandum NOS OMA 52.
Long, ER, DD MacDonald, SL Smith, and FD Calder. 1995. "Incidence of Adverse Biological
Effects with Ranges of Chemical Concentrations in Marine and Estuarine Sediments."
Environmental Management 19(1): 81-97.
34
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Appendix A
ASB Analytical Detection
Limit Tables
35
-------
Appendix A
ASB Analytical Tables
Table A1
Nutrients and Classicals Analyte List
Minimum Quantitation Limits by Matrices and Analytical Methods
ANALYTE
Water
Soil/Sed
Reference Analytical
mg/L
mg/kg
Method
(ppm)1
(ppm)
Ammonia
0.05
2.52
780-86-T (Equivalent to
EPA 350.1)
Nitrate+Nitrite
0.05
5
EPA 353.2
Phosphorus, Total
0.01
253
EPA 365.1
Kjeldahl Nitrogen
0.05
12.53
786-86T (Equivalent to
EPA 351.2)
Total Org. Carbon
1.0
10,000
EPA 415.1-water
ASB 107C-soils
MQLs may increase due to variability of interferences that make dilutions of
sample necessary. Sample sizes required for achieving the routine quantitation
limits listed above:
1 Units as specified unless otherwise noted
2 Calculated using 1.0 grams of sample (dry weight basis, % moisture will
increase MQLs).
3 Calculated using 0.2 grams of sample (dry weight basis, % moisture will
increase MQLs).
36
-------
Table A2
Metals Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
ANALYTE
Water
//g/L
(ppb)3
Saline
Water
Mg/L
(ppb)3
Soil/Sed
mg/kg
(ppm) h 3
Reference
Analytical
Method
Antimony
2.0
20
2.0
EPA 200.8
Arsenic
2.0
20
1.0
EPA 200.8
Aluminum
500
500
50
EPA 6010B
Barium
10
100
1.0
EPA 6010B
Beryllium
5.0
50
0.5
EPA 6010B
Cadmium
1.0
10
0.5
EPA 200.8
Calcium
500
5000
50
EPA 6010B
Cobalt
10
100
1.0
EPA 6010B
Chromium
10
100
1.0
EPA 6010B
Copper
10
100
1.0
EPA 6010B
Iron
250
2500
25
EPA 6010B
Lead
2.0
20
0.5
EPA 200.8
Magnesium
250
2500
25
EPA 6010B
Manganese
10
100
1.0
EPA 6010B
Mercury
0.2
0.4
0.05
EPA 245.1
Molybdenum
10
100
1.0
EPA 6010B
Nickel
20
200
2.0
EPA 6010B
Potassium
2000
20000
200
EPA 6010B
Selenium
5.0
50
4.0
EPA 200.8
Sodium
2000
20000
200
EPA 6010B
Strontium
10
100
1.0
EPA 601OB
Silver
10
100
1.0
EPA 601OB
Tin
25
250
2.5
EPA 601OB
Titanium
10
100
1.0
EPA 601OB
Thallium
1.0
10
0.5
EPA 200.8
Vanadium
10
100
1.0
EPA 601OB
Yttrium
10
100
1.0
EPA 601OB
37
-------
Table A2
Metals Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
ANALYTE
Water
Mg/L
(ppb)3
Saline
Water
li g/L
(ppb)3
Soil/Sed
mg/kg
(ppm) h 3
Reference
Analytical
Method
Zinc
10
100
1.0
EPA 6010B
1 Detection limits are based on 1.0 grams of sample (on dry weight basis,
% moisture will increase MQLs).
2 Detection limits are based on 5.0 grams of sample.
3 Units as specified unless otherwise noted
Table A3
Volatile Organics (VOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
(Encore® or
Tared Vial)
Reference
Analytical Method
acetone
25
25
EPA 8260B
acrylonitrile
NA
NA
EPA 8260B
benzene
1
1
EPA 8260B
bromobenzene
1
1
EPA 8260B
bromochloro methane
1
1
EPA 8260B
bromodichloromethane
1
1
EPA 8260B
bromoform
1
1
EPA 8260B
bromo methane
1
1
EPA 8260B
1,3-butadiene
NA
NA
EPA 8260B
butyl acrylate
NA
NA
EPA 8260B
n-butylbenzene
1
1
EPA 8260B
38
-------
Table A3
Volatile Organics (VOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
(Encore® or
Tared Vial)
Reference
Analytical Method
sec-butylbenzene
1
1
EPA 8260B
tert-butylbenzene
1
1
EPA 8260B
carbon tetrachloride
1
1
EPA 8260B
chlorodifluoromethane(R22)
NA
NA
EPA 8260B
carbon disulfide
2.5
1
EPA 8260B
chlorobenzene
1
1
EPA 8260B
chloroethane
1
1
EPA 8260B
chloroform
1
1
EPA 8260B
chloromethane
1
1
EPA 8260B
2-chloro-1,3-butadiene
(chloroprene)
NA
NA
EPA 8260B
o-chlorotoluene
1
1
EPA 8260B
p-chlorotoluene
1
1
EPA 8260B
cyclohexane
1
1
EPA 8260B
dibromochloromethane
1
1
EPA 8260B
1,2-dibromo-3 -chloropropane
1
1
EPA 8260B
1,2-dibromoethane
1
1
EPA 8260B
dibromo methane
1
1
EPA 8260B
1,2-dichlorobenzene
1
1
EPA 8260B
1,3 -dichlorobenzene
1
1
EPA 8260B
1,4-dichlorobenzene
1
1
EPA 8260B
dichlorodifluoromethane(R12)
1
1
EPA 8260B
1,1 -dichloroethene
1
1
EPA 8260B
cis-l,2-dichloroethene
1
1
EPA 8260B
trans-1,2-dichloroethene
1
1
EPA 8260B
1,1-dichloroethane
1
1
EPA 8260B
39
-------
Table A3
Volatile Organics (VOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
(Encore® or
Tared Vial)
Reference
Analytical Method
1,2-dichloroethane
1
1
EPA 8260B
1,2-dichloropropane
1
1
EPA 8260B
1,3 -dichloropropane
1
1
EPA 8260B
2,2-dichloropropane
1
1
EPA 8260B
1,1 -dichloropropene
1
1
EPA 8260B
cis-l,3-dichloropropene
1
1
EPA 8260B
dichlorotetrafluoroethane(Rl 14)
NA
NA
EPA 8260B
trans-1,3 -dichloropropene
1
5
EPA 8260B
ethyl acrylate
NA
NA
EPA 8260B
ethyl benzene
1
1
EPA 8260B
hexachlorobutadiene
1
1
EPA 8260B
hexane
NA
NA
EPA 8260B
isopropylbenzene
1
1
EPA 8260B
p-isopropyltoluene
1
1
EPA 8260B
methyl acetate
5
1
EPA 8260B
methyl cyclohexane
1
1
EPA 8260B
methyl methacrylate
NA
NA
EPA 8260B
methylene chloride
1
1
EPA 8260B
methyl butyl ketone
2.5
2.5
EPA 8260B
methyl ethyl ketone
12
2.5
EPA 8260B
methyl isobutyl ketone
2.5
2.5
EPA 8260B
methyl-t-butyl ether
1
1
EPA 8260B
n-propylbenzene
1
1
EPA 8260B
1,1,1,2-tetrachloroethane
1
1
EPA 8260B
1,1,2,2-tetrachloroethane
1
1
EPA 8260B
tetrachloroethene
1
1
EPA 8260B
40
-------
Table A3
Volatile Organics (VOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
(Encore® or
Tared Vial)
Reference
Analytical Method
toluene
1
1
EPA 8260B
1,2,3-trichlorobenzene
1
1
EPA 8260B
1,2,4-trichlorobenzene
1
1
EPA 8260B
1,1,1 -trichloroethane
1
1
EPA 8260B
1,1,2-trichloroethane
1
1
EPA 8260B
trichloroethene
1
1
EPA 8260B
trichlorofluoromethane(Rl 1)
1
1
EPA 8260B
1,2,3 -trichloropropane
1
1
EPA 8260B
trichlorotrifluoroethane(Rl 13)
1
1
EPA 8260B
1,2,4-trimethylbenzene
1
1
EPA 8260B
1,3,5 -trimethylbenzene
1
1
EPA 8260B
styrene
1
1
EPA 8260B
o-xylene
1
1
EPA 8260B
(m- and/or p-)xylene
2
2
EPA 8260B
vinyl chloride
1
1
EPA 8260B
MQLs may increase due to variability of interferences that make dilutions of
sample necessary. Sample sizes required for achieving the routine quantitation
limits listed above:
1 - Water- 5 mL from septum sealed vial.
2 - Routine Level Soil - 5 gram sample preserved with water or acid (dry weight
basis, % moisture will increase MQLs).
41
-------
Table A4
Semivolatile Organics (SemiVOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits Guidelines by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
Reference Analytical Method
(3- and/or 4-)Methylphenol
10.
330
EPA 8270D
l,l'-biphenyl
10.
330
EPA 8270D
1,2,4-Trichlorobenzene
10.
330
EPA 8270D
2-Nitrophenol
10.
330
EPA 8270D
2-Methyl-4,6-dinitrophenol
20.
670
EPA 8270D
2,3,4,6-Tetrachlorophenol
10
330
EPA 8270D
2,4-Dimethylphenol
10.
330
EPA 8270D
2,4-Dinitrotoluene
10.
330
EPA 8270D
2,4-Dinitrophenol
20.
670
EPA 8270D
2-Methylphenol
10.
330
EPA 8270D
2-Nitroaniline
10.
330
EPA 8270D
2-Chlorophenol
10.
330
EPA 8270D
2-Methylnaphthalene
10.
330
EPA 8270D
2,4,5-Trichlorophenol
10.
330
EPA 8270D
2-Chloronaphthalene
10.
330
EPA 8270D
2,6-Dinitrotoluene
10.
330
EPA 8270D
2,4-Dichlorophenol
10.
330
EPA 8270D
2,4,6-Trichlorophenol
10.
330
EPA 8270D
3,3 '-Dichlorobenzidine
10.
330
EPA 8270D
3-Nitroaniline
10.
330
EPA 8270D
4-Chlorophenylphenylether
10.
330
EPA 8270D
4-Chloroaniline
10.
330
EPA 8270D
4-Nitroaniline
10.
330
EPA 8270D
4-Nitrophenol
20.
670
EPA 8270D
4-Chloro-3 -methylphenol
10.
330
EPA 8270D
4-Bromophenylphenylether
10.
330
EPA 8270D
Acenaphthene
10.
330
EPA 8270D
42
-------
Table A4
Semivolatile Organics (SemiVOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits Guidelines by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
Reference Analytical Method
Acenaphthylene
10.
330
EPA 8270D
Acetophenone
10.
330
EPA 8270D
Anthracene
10.
330
EPA 8270D
Atrazine
10.
330
EPA 8270D
Benzo(a)anthracene
10.
330
EPA 8270D
Benzo(a)pyrene
10.
330
EPA 8270D
Benzo(b)fluoranthene
10.
330
EPA 8270D
Benzo(k)fluoranthene
10.
330
EPA 8270D
Benzo(g,h,i)perylene
10.
330
EPA 8270D
Benzaldehyde
10.
330
EPA 8270D
Benzyl Butyl Phthalate
10.
330
EPA 8270D
Bis(2-ethylhexyl)phthalate
10.
330
EPA 8270D
Bis(2-chloroethyl)ether
10.
330
EPA 8270D
Bis(chloroethoxy)methane
10.
330
EPA 8270D
Bis(chloroisopropyl)ether
10.
330
EPA 8270D
Caprolactam
10.
330
EPA 8270D
Carbazole
10.
330
EPA 8270D
Chrysene
10.
330
EPA 8270D
Di-n-butylpthalate
10.
330
EPA 8270D
Di-n-octylphthalate
10.
330
EPA 8270D
Dibenz(a,h)anthracene
10.
330
EPA 8270D
Dibenzofuran
10.
330
EPA 8270D
Diethyl phthalate
10.
330
EPA 8270D
Dimethyl Phthalate
10.
330
EPA 8270D
Fluoranthene
10.
330
EPA 8270D
Fluorene
10.
330
EPA 8270D
Hexachlorobenzene
10.
330
EPA 8270D
43
-------
Table A4
Semivolatile Organics (SemiVOAs) Target Analyte List, Analytical Methods and
Minimum Quantitation Limits Guidelines by Matrices
Water1
Mg/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
Reference Analytical Method
Hexachlorobutadiene
10.
330
EPA 8270D
Hexachlorocyclopentadiene
10.
330
EPA 8270D
Hexachloroethane
10.
330
EPA 8270D
Indeno( 1,2,3 ,c,d)pyrene
10.
330
EPA 8270D
Isophorone
10.
330
EPA 8270D
N-Nitrosodiphenylamine
10.
330
EPA 8270D
Naphthalene
10.
330
EPA 8270D
Nitrobenzene
10.
330
EPA 8270D
Nitroso-di-N-propylamine
10.
330
EPA 8270D
Pentachlorophenol
20.
670
EPA 8270D
Phenanthrene
10.
330
EPA 8270D
Phenol
10.
330
EPA 8270D
Pyrene
10.
330
EPA 8270D
MQLs may increase due to variability of interferences that make dilutions of sample
necessary. Sample sizes required for achieving the routine quantitation limits listed
above:
1 - All water -1000 ml, final extract volume 1 ml.
2 - Routine Level Soil - 30 grams: If the final volume is 1 ml the above limits apply.
If split with pesticide, and a final volume of 2 mis, the above detection levels are
doubled to 670/1300 ,ug/kg (dry weight basis, % moisture will increase MQLs).
44
-------
Table A5
Pesticide/PCB Target Analyte List
Minimum Quantitation Limits Guidelines by Matrices
Revised 06/26/03
Water1
^g/L
(PPb)
Soil/Sed2
Mg/kg
(PPb)
ANALYTE
Routine
Level
Routine
Level
Reference Analytical Method
Aldrin
0.50
20
EPA 8081A
Heptachlor
0.50
20
EPA 8081A
Hept. Epoxide
0.50
20
EPA 8081A
alpha-BHC
0.50
20
EPA 8081A
beta-BHC
0.50
20
EPA 8081A
gamma-BHC
0.50
20
EPA 8081A
delta-BHC
0.50
20
EPA 8081A
Endosulfan-1
0.50
20
EPA 8081A
Dieldrin
0.50
20
EPA 8081A
p,p'-DDT
0.50
20
EPA 8081A
p,p'-DDE
0.50
20
EPA 8081A
p,p'-DDD
0.50
20
EPA 8081A
Endrin
0.50
20
EPA 8081A
Endosulfan -II
0.50
20
EPA 8081A
Endosulfan- S04
0.50
20
EPA 8081A
Endrin Ketone
0.50
20
EPA 8081A
Methoxychlor
1.0
50
EPA 8081A
Tech. Chlordane
1.5
50
EPA 8081A
b-chlordene
0.50
20
EPA 8081A
g-chlordane
0.50
20
EPA 8081A
a-chlordane
0.50
20
EPA 8081A
chlordene
0.50
20
EPA 8081A
a-chlordene
0.50
20
EPA 8081A
oxychlordane
0.50
20
EPA 8081A
trans-no nachlor
0.50
20
EPA 8081A
cis-nonachlor
0.50
20
EPA 8081A
PCB(as Aroclors)
2.5
100
EPA 8082
45
-------
Table A5
Pesticide/PCB Target Analyte List
Minimum Quantitation Limits Guidelines by Matrices
Revised 06/26/03
Water1
Soil/Sed2
^g/L
Mg/kg
(PPb)
(PPb)
ANALYTE
Routine
Routine
Reference Analytical Method
Level
Level
Toxaphene
20
1000
EPA 8081A
MQLs may increase due to variability of interferences that make dilutions of sample
necessary. Sample sizes required for achieving the routine quantitation limits listed
above:
1 - All water -1000 ml, final extract volume 1 ml.
2 - Routine Level Soil - 30 grams: final extract volume 1 mis (dry weight basis - %
moisture will increase MQLs).
46
-------
Appendix B
Chemical Surface Water
Quality Data
47
-------
Bayou Casotte Surfacewater All Data
BC1D
9/27/2005
1205
BC1SW
9/27/2005
1134
BC2SW
9/27/2005
1333
BC3SW
9/27/2005
1410
BC4SW
9/27/2005
1450
BL1SW
9/27/2005
1315
Metals Scan
Aluminum
7429-90-5
UG/L
2000 U
2000 U
2000 U
2000
U
2000 U
2000 U
Antimony
7440-36-0
UG/L
5 U
5 U
5 U
5
U
5 U
5 U
Arsenic
7440-38-2
UG/L
46 J
45 J
42 J
41
J
48 AJ
36 J
Barium
7440-39-3
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Beryllium
7440-41-7
UG/L
60 U
60 U
60 U
60
U
60 U
45 U
Cadmium
7440-43-9
UG/L
37 U
37 U
37 U
37
U
37 UJ
37 U
Calcium
7440-70-2
MG/L
350
350
360
350
340 A
270
Chromium
7440-47-3
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Cobalt
7440-48-4
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Copper
7440-50-8
UG/L
400 U
400 U
400 U
400
U
400 U
300 U
Iron
7439-89-6
MG/L
2 U
2 U
2 U
2
U
2 U
2 U
Lead
7439-92-1
UG/L
5 U
5 U
5 U
5
U
5 U
5 U
Magnesium
7439-95-4
MG/L
1100
1100
1100
1100
1000 A
820
Manganese
7439-96-5
UG/L
100 U
100 U
100 U
100
U
100 U
120
Molybdenum
7439-98-7
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Nickel
7440-02-0
UG/L
200 U
200 U
200 U
200
U
200 U
150 U
Potassium
7440-09-7
MG/L
350
360
380
360
320 A
270
Selenium
7782-49-2
UG/L
150 J
150 J
140 J
130
J
150 AJ
110 J
Silver
7440-22-4
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Sodium
7440-23-5
MG/L
9000
9200
9500
9200
8400 A
6800
Strontium
7440-24-6
UG/L
5900
6100
6300
6100
5500 A
4600
Thallium
7440-28-0
UG/L
5 U
5 U
5 U
5
U
5 U
5 U
Tin
7440-31-5
UG/L
NA
NA
NA
NA
NA
NA
Titanium
7440-32-6
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Total Mercury
7439-97-6
UG/L
0.2 U
0.2 U
0.2 U
0.2
U
0.2 U
0.2 U
Vanadium
7440-62-2
UG/L
100 U
100 U
100 U
100
U
100 U
75 U
Yttrium
7440-65-5
UG/L
60 U
60 U
60 U
60
U
60 U
45 U
Zinc
7440-66-6
UG/L
200 U
200 U
200 U
200
U
200 U
150 U
PCB Scan
PCB-1016 (Aroclor 1016)
12674-11-2
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1221 (Aroclor 1221)
11104-28-2
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1232 (Aroclor 1232)
11141-16-5
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1242 (Aroclor 1242)
53469-21-9
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1248 (Aroclor 1248)
12672-29-6
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1254 (Aroclor 1254)
11097-69-1
UG/L
2 U
2 U
2 U
2
U
2 U
2 U
PCB-1260 (Aroclor 1260)
11096-82-5
UG/L
2 U
2 U
2 U
2
u
2 U
2 U
Pesticides Scan
4,4'-DDD (p.p'-DDD)
72-54-8
UG/L
0.25 U
0.26 U
0.25 U
0.26
u
0.25 U
0.25 U
4,4'-DDE (p.p'-DDE)
72-55-9
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/L
0.25 U
0.26 U
0.25 U
0.26
u
0.25 U
0.25 U
Aldrin
309-00-2
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
alpha-BHC
319-84-6
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
alpha-Chlordane 12
5103-71-9
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
beta-BHC
319-85-7
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Chlordene 12
3734-48-3
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
cis-Nonachlor 12
5103-73-1
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
delta-BHC
319-86-8
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Dieldrin
60-57-1
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Endosulfan 1 (alpha)
959-98-8
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Endosulfan II (beta)
33213-65-9
UG/L
0.25 U
0.26 U
0.25 U
0.26
u
0.25 U
0.25 U
Endosulfan Sulfate
1031-07-8
UG/L
0.25 U
0.26 U
0.5 U
0.26
u
0.25 U
0.25 U
Endrin
72-20-8
UG/L
0.25 U
0.26 U
0.25 U
0.26
u
0.25 U
0.25 U
Endrin Ketone
53494-70-5
UG/L
0.25 U
0.25 U
0.5 U
0.26
u
0.25 U
0.25 U
gamma-BHC (Lindane)
58-89-9
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
gamma-Chlordane 12
5566-34-7
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Heptachlor
76-44-8
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Heptachlor Epoxide
1024-57-3
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
Methoxychlor
72-43-5
UG/L
0.51 U
0.51 U
0.5 U
0.51
u
0.5 U
0.5 U
Toxaphene
8001-35-2
UG/L
10 U
10 U
10 U
10
u
10 U
10 U
trans-Nonachlor 12
39765-80-5
UG/L
0.1 U
0.1 U
0.1 U
0.1
u
0.1 U
0.1 U
48
-------
Bayou Casotte Surfacewater All Data
BC1D
9/27/2005
1205
BC1SW
9/27/2005
1134
BC2SW
9/27/2005
1333
BC3SW
9/27/2005
1410
BC4SW
9/27/2005
1450
BL1SW
9/27/2005
1315
1,1,2-Trichloroethane
79-00-5
UG/L
1 U
1 u
1 u
1 u
1 u
1,1-Dichloroethane
75-34-3
UG/L
1 U
1 u
1 u
1 u
1 u
1,1 -Dichloroethene (1,1 -Dichloroethylene)
75-35-4
UG/L
1 U
1 u
1 u
1 u
1 u
1,1-Dichloropropene
563-58-6
UG/L
1 U
1 u
1 u
1 u
1 u
1,2,3-Trichlorobenzene
87-61-6
UG/L
1 U
1 u
1 u
1 u
1 u
1,2,3-Trichloropropane
96-18-4
UG/L
1 U
1 u
1 u
1 u
1 u
1,2,4-Trichlorobenzene
120-82-1
UG/L
1 U
1 u
1 u
1 u
1 u
1,2,4-Trimethylbenzene
95-63-6
UG/L
1 U
1 u
1 u
1 u
1 u
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/L
2 U
2 U
2 U
2 U
2 U
1,2-Dibromoethane (EDB)
106-93-4
UG/L
1 U
1 u
1 u
1 u
1 u
1,2-Dichlorobenzene
95-50-1
UG/L
1 U
1 u
1 u
1 u
1 u
1,2-Dichloroethane
107-06-2
UG/L
1 U
1 u
1 u
1 u
1 u
1,2-Dichloropropane
78-87-5
UG/L
1 U
1 u
1 u
1 u
1 u
1,3,5-Trimethylbenzene
108-67-8
UG/L
1 U
1 u
1 u
1 u
1 u
1,3-Dichlorobenzene
541-73-1
UG/L
1 U
1 u
1 u
1 u
1 u
1,3-Dichloropropane
142-28-9
UG/L
1 U
1 u
1 u
1 u
1 u
1,4-Dichlorobenzene
106-46-7
UG/L
1 U
1 u
1 u
1 u
1 u
2,2-Dichloropropane
590-20-7
UG/L
1 U
1 u
1 u
1 u
1 u
Acetone
67-64-1
UG/L
2 U
2 U
2 U
2 U
2 U
Benzene
71-43-2
UG/L
1 U
1 u
1 u
1 u
1 u
Bromobenzene
108-86-1
UG/L
1 U
1 u
1 u
1 u
1 u
Bromochloromethane
74-97-5
UG/L
1 U
1 u
1 u
1 u
1 u
Bromodichloromethane
75-27-4
UG/L
1 U
1 u
1 u
1 u
1 u
Bromoform
75-25-2
UG/L
1 U
1 u
1 u
1 u
1 u
Bromomethane
74-83-9
UG/L
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
Carbon Disulfide
75-15-0
UG/L
1 U
1 u
1 u
1 u
1 u
Carbon Tetrachloride
56-23-5
UG/L
1 U
1 u
1 u
1 u
1 u
Chlorobenzene
108-90-7
UG/L
1 U
1 u
1 u
1 u
1 u
Chloroethane
75-00-3
UG/L
1 U
1 u
1 u
1 u
1 u
Chloroform
67-66-3
UG/L
1 U
1 u
1 u
1 u
1 u
Chloromethane
74-87-3
UG/L
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
cis-1,2-Dichloroethene
156-59-2
UG/L
1 u
1 u
1 u
1 u
1 u
cis-1,3-Dichloropropene
10061-01-5
UG/L
1 u
1 u
1 u
1 u
1 u
Cyclohexane
110-82-7
UG/L
1 u
1 u
1 u
1 u
1 u
Dibromochloromethane
124-48-1
UG/L
1 u
1 u
1 u
1 u
1 u
Dibromomethane
74-95-3
UG/L
1 u
1 u
1 u
1 u
1 u
Dichlorodifluoromethane
75-71-8
UG/L
1 u
1 u
1 u
1 u
1 u
Ethyl Benzene
100-41-4
UG/L
1 u
1 u
1 u
1 u
1 u
Hexachloro-1,3-Butadiene
87-68-3
UG/L
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
Isopropylbenzene
98-82-8
UG/L
1 u
1 u
1 u
1 u
1 u
Methyl Acetate
79-20-9
UG/L
1 u
1 u
1 u
1 u
1 u
Methyl Butyl Ketone
591-78-6
UG/L
2 U
2 U
2 U
2 U
2 U
Methyl Ethyl Ketone
78-93-3
UG/L
5 U
5 U
5 U
5 U
5 U
Methyl Isobutyl Ketone
108-10-1
UG/L
1 U
1 u
1 u
1 u
1 u
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/L
1 U
1 u
1 u
1 u
1 u
Methylcyclohexane
108-87-2
UG/L
1 U
1 u
1 u
1 u
1 u
Methylene Chloride
75-09-2
UG/L
1 u
1 u
1 u
1 u
1 u
n-Butylbenzene
104-51-8
UG/L
1 u
1 u
1 u
1 u
1 u
n-Propylbenzene
103-65-1
UG/L
1 u
1 u
1 u
1 u
1 u
o-Chlorotoluene
95-49-8
UG/L
1 u
1 u
1 u
1 u
1 u
o-Xylene
95-47-6
UG/L
1 u
1 u
1 u
1 u
1 u
p-Chlorotoluene
106-43-4
UG/L
1 u
1 u
1 u
1 u
1 u
p-lsopropyltoluene
99-87-6
UG/L
1 u
1 u
1 u
1 u
1 u
sec-Butylbenzene
135-98-8
UG/L
1 u
1 u
1 u
1 u
1 u
Styrene
100-42-5
UG/L
1 u
1 u
1 u
1 u
1 u
tert-Butylbenzene
98-06-6
UG/L
1 u
1 u
1 u
1 u
1 u
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/L
1 u
1 u
1 u
1 u
1 u
Toluene
108-88-3
UG/L
1 u
1 u
1 u
1 u
1 u
49
-------
Bayou Casotte Surfacewater All Data
BC1D
BC1SW
BC2SW
BC3SW
BC4SW
BL1SW
9/27/2005
9/27/2005
9/27/2005
9/27/2005
9/27/2005
9/27/2005
1205
1134
1333
1410
1450
1315
Extractables Scan
(3-and/or 4-)Methylphenol
UG/L
11 U
10 U
10 U
10 u
9.9 U
10 U
1,1 -Biphenyl
92-52-4
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
1,2,4-Trichlorobenzene
120-82-1
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,4,5-Trichlorophenol
95-95-4
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,4,6-Trichlorophenol
88-06-2
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,4-Dichlorophenol
120-83-2
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,4-Dimethylphenol
105-67-9
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 U
2,4-Din itrophenol
51-28-5
UG/L
23 U
20 U
20 U
20 U
20 U
20 U
2,4-Dinitrotoluene
121-14-2
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2,6-Dinitrotoluene
606-20-2
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2-Chloronaphthalene
91-58-7
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 U
2-Chlorophenol
95-57-8
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 U
2-Methyl-4,6-Dinitro phenol
534-52-1
UG/L
23 U
20 U
20 U
20 U
20 U
20 U
2-Methylnaphthalene
91-57-6
UG/L
11 U
10 U
10 u
10 u
9.9 U
10 U
2-Methylphenol
95-48-7
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 U
2-Nitroaniline
88-74-4
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 U
2-N itrophenol
88-75-5
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
3,3'-Dichlorobenzidine
91-94-1
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
3-Nitroaniline
99-09-2
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-Bromophenyl Phenyl Ether
101-55-3
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-Chloro-3-Methylphenol
59-50-7
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-Chloroaniline
106-47-8
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-Nitroaniline
100-01-6
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
4-N itrophenol
100-02-7
UG/L
23 U
20 U
20 U
20 U
20 U
20 U
Acenaphthene
83-32-9
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Acenaphthylene
208-96-8
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Acetophenone
98-86-2
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Anthracene
120-12-7
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Atrazine
1912-24-9
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzaldehyde
100-52-7
UG/L
11 UJ
10 UJ
10 UJ
10 UJ
9.9 UJ
10 UJ
Benzo(a)Anthracene
56-55-3
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzo(b)Fluoranthene
205-99-2
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzo(ghi)Perylene
191-24-2
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzo(k)Fluoranthene
207-08-9
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzo-a-Pyrene
50-32-8
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
Benzyl Butyl Phthalate
85-68-7
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
bis(2-Chloroethoxy)Methane
111-91-1
UG/L
11 U
10 u
10 u
10 u
9.9 U
10 u
bis(2-Chloroethyl) Ether
111-44-4
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
bis(2-Chloroisopropyl) Ether
108-60-1
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Caprolactam
105-60-2
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Carbazole
86-74-8
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Chrysene
218-01-9
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Dibenzo(a,h)Anthracene
53-70-3
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Dibenzofuran
132-64-9
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Diethyl Phthalate
84-66-2
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Dimethyl Phthalate
131-11-3
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Di-n-Butylphthalate
84-74-2
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Di-n-Octyl phthalate
117-84-0
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Fluoranthene
206-44-0
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Fluorene
86-73-7
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Hexachlorobenzene (HCB)
118-74-1
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Hexachloro butadiene
87-68-3
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
Hexachloroethane
67-72-1
UG/L
11 u
10 u
10 u
10 u
9.9 U
10 u
50
-------
Bayou Casotte Surfacewater All Data
BC1D BC1SW BC2SW BC3SW BC4SW BL1SW
9/27/2005 9/27/2005 9/27/2005 9/27/2005 9/27/2005 9/27/2005
1205 1134 1333 1410 1450 1315
Pentachlorophenol
87-86-5
UG/L
23 U
20 U
20 U
20 U
20 U
20 U
Phenanthrene
85-01-8
UG/L
11 U
10 U
10 U
10 U
9.9 U
10 U
Phenol
108-95-2
UG/L
11 U
10 U
10 U
10 U
9.9 U
10 U
Pyrene
129-00-0
UG/L
11 U
10 U
10 U
10 U
9.9 U
10 U
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.05 U
0.075
0.072
0.064
1.5
0.05 U
Nitrate-Nitrite Nitrogen
MG/L
0.055
0.06
0.066
0.095
0.055
0.05 U
Total Kjeldahl Nitrogen
MG/L
0.25
0.25
0.2
0.22
1.9
0.76
Total Organic Carbon
MG/L
1.4
1.4
12
1.4
2.2
17
Total Phosphorus
7723-14-0
MG/L
0.23
0.22
0.27
0.38
17
0.18
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
51
-------
Pascagoula River, West Pascagoula River, Escatawpa River Surface Water All Data
ER1DSW
ER1SW
ER2SW
PR1SW
PR2SW
WPR1SW
WPR2SW
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/28/2005
1425
1420
1135
1240
1557
1115
1420
Metals Scan
Aluminum
7429-90-5
UG/L
2000 U
2000 U
2000 U
2000 U
2000 U
750 U
2000 U
Antimony
7440-36-0
UG/L
5 U
5 U
5 U
5 U
5 U
5 U
5 U
Arsenic
7440-38-2
UG/L
23 AJ
24 J
28 J
46 J
23 J
34 J
5 U
Barium
7440-39-3
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
47
Beryllium
7440-41-7
UG/L
30 U
30 U
30 U
60 U
30 U
45 U
6 U
Cadmium
7440-43-9
UG/L
38 U
38 U
38 U
38 U
38 U
38 U
38 U
Calcium
7440-70-2
MG/L
170 A
180
190
330
160
260
28
Chromium
7440-47-3
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Cobalt
7440-48-4
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Copper
7440-50-8
UG/L
200 U
200 U
200 U
400 U
200 U
300 U
40 U
Iron
7439-89-6
MG/L
2 U
2 U
2 U
2 U
2 U
1.5 U
2 U
Lead
7439-92-1
UG/L
5 U
5 U
5 U
5 U
5 U
5 U
5 U
Magnesium
7439-95-4
MG/L
520 A
560
590
1000
470
840
74
Manganese
7439-96-5
UG/L
160 AJ
140
240
100 U
270
98
340
Molybdenum
7439-98-7
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Nickel
7440-02-0
UG/L
100 U
100 U
100 U
200 U
100 U
150 U
20 U
Potassium
7440-09-7
MG/L
170 A
180
200
340
150
260
26
Selenium
7782-49-2
UG/L
77 AJ
80 J
89 J
150 J
72 J
110 J
10 U
Silver
7440-22-4
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Sodium
7440-23-5
MG/L
4400 A
4700
5000
8700
4000
6900
650
Strontium
7440-24-6
UG/L
2900 A
3100
3300
5600
2700
5200
450
Thallium
7440-28-0
UG/L
5 U
5 U
5 U
5 U
5 U
5 U
5 U
Tin
7440-31-5
UG/L
NA
NA
NA
NA
NA
NA
NA
Titanium
7440-32-6
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Total Mercury
7439-97-6
UG/L
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
0.2 U
Vanadium
7440-62-2
UG/L
50 U
50 U
50 U
100 U
50 U
75 U
10 U
Yttrium
7440-65-5
UG/L
30 U
30 U
30 U
60 U
30 U
45 U
6 U
Zinc
7440-66-6
UG/L
100 U
100 U
100 U
200 U
100 U
150 U
20 U
PCB Scan
PCB-1016 (Aroclor 1016)
12674-11-2
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1221 (Aroclor 1221)
11104-28-2
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1232 (Aroclor 1232)
11141-16-5
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1242 (Aroclor 1242)
53469-21-9
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1248 (Aroclor 1248)
12672-29-6
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1254 (Aroclor 1254)
11097-69-1
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
PCB-1260 (Aroclor 1260)
11096-82-5
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
Pesticides Scan
4,4'-DDD (p,p'-DDD)
72-54-8
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
4,4'-DDE (p.p'-DDE)
72-55-9
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Aldrin
309-00-2
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
alpha-BHC
319-84-6
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
alpha-Chlordane /2
5103-71-9
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
beta-BHC
319-85-7
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Chlordene /2
3734-48-3
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
cis-Nonachlor /2
5103-73-1
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
delta-BHC
319-86-8
UG/L
0.1 U
0.19 U
0.1 U
0.21 U
0.1 U
0.1 U
0.1 U
Dieldrin
60-57-1
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Endosulfan I (alpha)
959-98-8
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Endosulfan II (beta)
33213-65-9
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Endosulfan Sulfate
1031-07-8
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Endrin
72-20-8
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Endrin Ketone
53494-70-5
UG/L
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
gamma-BHC (Lindane)
58-89-9
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
gamma-Chlordane /2
5566-34-7
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.11 U
0.1 U
0.1 U
Heptachlor
76-44-8
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Heptachlor Epoxide
1024-57-3
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Methoxychlor
72-43-5
UG/L
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
Toxaphene
8001-35-2
UG/L
10 U
10 U
10 U
10 U
10 U
10 U
10 U
trans-Nonachlor /2
39765-80-5
UG/L
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
0.1 U
Volatiles Scan
(m- and/or p-)Xylene
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
1,1,1,2-Tetrachloroethane
630-20-6
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1,1-Trichloroethane
71-55-6
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1,2-Trichloroethane
79-00-5
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1-Dichloroethane
75-34-3
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1-Dichloroethene
75-35-4
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,1-Dichloropropene
563-58-6
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,2,3-Trichlorobenzene
87-61-6
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1,2,3-Trichloropropane
96-18-4
UG/L
1 U
1 U
1 U
1 U
1 U
1 U
1 U
52
-------
Pascagoula River, West Pascagoula River,Escatawpa River Surface Water All Data
ER1DSW ER1SW ER2SW PR1SW PR2SW WPR1SW WPR2SW
9/28/2005 9/28/2005 9/28/2005 9/28/2005 9/28/2005 9/28/2005 9/28/2005
1425 1420 1135 1240 1557 1115 1420
1,2-Dichloropropane
78-87-5
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 UJ
1,3,5-T rimethylbenzene
108-67-8
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
1,3-Dichlorobenzene
541-73-1
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
1,3-Dichloropropane
142-28-9
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
1,4-Dichlorobenzene
106-46-7
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
2,2-Dichloropropane
590-20-7
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Acetone
67-64-1
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
Benzene
71-43-2
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Bromobenzene
108-86-1
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Bromochloromethane
74-97-5
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Bromodichloromethane
75-27-4
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Bromoform
75-25-2
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Bromomethane
74-83-9
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Carbon Disulfide
75-15-0
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Carbon Tetrachloride
56-23-5
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Chlorobenzene
108-90-7
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Chloroethane
75-00-3
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Chloroform
67-66-3
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Chloromethane
74-87-3
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
cis-1,2-Dichloroethene
156-59-2
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
cis-1,3-Dichloropropene
10061-01-5
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Cyclohexane
110-82-7
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Dibromochloromethane
124-48-1
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Dibromomethane
74-95-3
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Dichlorodifluoromethane
75-71-8
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Ethyl Benzene
100-41-4
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Hexachloro-1,3-Butadiene
87-68-3
UG/L
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
1 UJ
Isopropylbenzene
98-82-8
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Methyl Acetate
79-20-9
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Methyl Butyl Ketone
591-78-6
UG/L
2 U
2 U
2 U
2 U
2 U
2 U
2 U
Methyl Ethyl Ketone
78-93-3
UG/L
5 U
5 U
5 U
5 U
5 U
5 U
5 U
Methyl Isobutyl Ketone
108-10-1
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Methylcyclohexane
108-87-2
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Methylene Chloride
75-09-2
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
n-Butylbenzene
104-51-8
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
n-Propylbenzene
103-65-1
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
o-Chlorotoluene
95-49-8
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
o-Xylene
95-47-6
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
p-Chlorotoluene
106-43-4
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
p-lsopropyltoluene
99-87-6
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
sec-Butylbenzene
135-98-8
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Styrene
100-42-5
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
tert-Butylbenzene
98-06-6
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/L
1 u
1 u
1 u
1 u
1 u
1 u
1 u
Toluene
108-88-3
UG/L
0.064 J
0.072 J
1 u
1 u
1 u
1 u
1 u
trans-1,2-Dichloroethene
156-60-5
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
trans-1,3-Dichloropropene
10061-02-6
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Trichloroethene (Trichloroethylene)
79-01-6
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Trichlorofluoromethane (Freon11)
75-69-4
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Vinyl Chloride
75-01-4
UG/L
1 U
1 u
1 u
1 u
1 u
1 u
1 u
Extractables Scan
(3-and/or 4-)Methylphenol
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1,1-Biphenyl
92-52-4
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
1,2,4-T richlorobenzene
120-82-1
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,3,4,6-Tetrachlorophenol
58-90-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,4,5-Trichlorophenol
95-95-4
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,4,6-Trichlorophenol
88-06-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,4-Dichlorophenol
120-83-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,4-Dimethyl phenol
105-67-9
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,4-Dinitrophenol
51-28-5
UG/L
20 U
20 U
20 U
20 U
20 U
20 U
20 U
2,4-Dinitrotoluene
121-14-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2,6-Dinitrotoluene
606-20-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Chloronaphthalene
91-58-7
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Chlorophenol
95-57-8
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/L
20 U
20 U
20 U
20 U
20 U
20 U
20 U
2-Methylnaphthalene
91-57-6
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Methylphenol
95-48-7
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Nitroaniline
88-74-4
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
2-Nitrophenol
88-75-5
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3,3'-Dichloro benzidine
91-94-1
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
3-Nitroaniline
99-09-2
UG/L
10 u
10 u
10 u
10 u
10 u
10 u
10 u
53
-------
Pascagoula River, West Pascagoula River,Escatawpa River Surface Water All Data
ER1DSW ER1SW ER2SW PR1SW
9/28/2005 9/28/2005 9/28/2005 9/28/2005
1425 1420 1135 1240
PR2SW
9/28/2005
1557
WPR1SW
9/28/2005
1115
WPR2SW
9/28/2005
1420
Acenaphthene
83-32-9
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Acenaphthylene
208-96-8
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Acetophenone
98-86-2
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Anthracene
120-12-7
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Atrazine
1912-24-9
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Benzaldehyde
100-52-7
UG/L
10
UJ
10 UJ
10 UJ
10
UJ
10
UJ
10
UJ
10 UJ
Benzo(a) Anthracene
56-55-3
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Benzo(b)Fluoranthene
205-99-2
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Benzo(ghi)Perylene
191-24-2
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 U
Benzo(k)Fluoranthene
207-08-9
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
Benzo-a-Pyrene
50-32-8
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
Benzyl Butyl Phthalate
85-68-7
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
bis(2-Chloroethoxy)Methane
111-91-1
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
bis(2-Chloroethyl) Ether
111-44-4
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
bis(2-Chloroisopropyl) Ether
108-60-1
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/L
10
U
10 u
10 u
10
U
10
U
10
U
10 u
Caprolactam
105-60-2
UG/L
10
U
10 u
10 u
10
u
10
U
10
U
10 u
Carbazole
86-74-8
UG/L
10
u
10 u
10 u
10
u
10
U
10
U
10 u
Chrysene
218-01-9
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Dibenzo(a.h) Anthracene
53-70-3
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Dibenzofuran
132-64-9
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Diethyl Phthalate
84-66-2
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Dimethyl Phthalate
131-11-3
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Di-n-Butyl phthalate
84-74-2
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Di-n-Octylphthalate
117-84-0
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Fluoranthene
206-44-0
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Fluorene
86-73-7
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Hexachlorobenzene (HCB)
118-74-1
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Hexachlorobutadiene
87-68-3
UG/L
10
UJ
10 UJ
10 UJ
10
UJ
10
UJ
10
UJ
10 UJ
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Hexachloroethane
67-72-1
UG/L
10
UJ
10 UJ
10 UJ
10
UJ
10
UJ
10
UJ
10 UJ
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Isophorone
78-59-1
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Naphthalene
91-20-3
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Nitrobenzene
98-95-3
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
n-Nitroso di-n-Propylamine
621-64-7
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
n-Nitrosodiphenylamine/Diphenylamine
122-39-4
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Pentachlorophenol
87-86-5
UG/L
20
u
20 U
20 U
20
u
20
u
20
u
20 U
Phenanthrene
85-01-8
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Phenol
108-95-2
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Pyrene
129-00-0
UG/L
10
u
10 u
10 u
10
u
10
u
10
u
10 u
Miscellaneous Extractables
Benzenedicarboxylic Acid, Dihexyl Ester
UG/L
NR
NR
10 NJ
NR
NR
NR
NR
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.087
0.093
0.17
0.072
0.12
0.083
0.056
Nitrate-Nitrite Nitrogen
MG/L
0.05
u
0.05 U
0.05 U
0.056
0.062
0.05
u
0.079
Total Kjeldahl Nitrogen
MG/L
0.38
0.41
0.49
0.29
0.47
0.45
0.51
Total Organic Carbon
MG/L
4.2
4.2
4.1
1.6
4.2
2.5
7
Total Phosphorus
7723-14-0
MG/L
0.05
0.048
0.036
0.087
0.052
0.063
0.041
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
54
-------
Back Bay Biloxi All Data
BBB1DSW
9/29/2005
1340
BBB1SW
9/29/2005
1312
BBB2SW
9/29/2005
1032
BBB3SW
9/29/2005
935
BBB4SW
9/29/2005
1300
BBB5SW
9/29/2005
1140
BBB6SW
9/29/2005
1025
Metals Scan
Aluminum
7429-90-5
UG/L
500 U
1200 U
1200
U
600
U
360
U
360
U
240 U
Antimony
7440-36-0
UG/L
2.5 U
2.5 U
2.5
U
2.5
U
2.5
U
2.5
U
2.5 U
Arsenic
7440-38-2
UG/L
26 AJ
25 J
19
J
14
J
8
J
9.1
J
6.4 J
Barium
7440-39-3
UG/L
50 U
50 U
50
U
46
44
46
40
Beryllium
7440-41-7
UG/L
30 U
30 U
30
U
15
U
9
U
9
U
6 U
Cadmium
7440-43-9
UG/L
14 U
14 U
14
U
14
U
14
U
14
U
14 U
Calcium
7440-70-2
MG/L
160 A
160
130
90
51
58
40
Chromium
7440-47-3
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Cobalt
7440-48-4
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Copper
7440-50-8
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Iron
7439-89-6
MG/L
1 U
1 U
1
U
0.5
U
0.55
0.56
0.56
Lead
7439-92-1
UG/L
2.5 U
2.5 U
2.5
U
2.5
U
2.5
U
2.5
U
2.5 U
Magnesium
7439-95-4
MG/L
480 A
500
390
270
140
170
98
Manganese
7439-96-5
UG/L
67 A
62
110
190
260
290
190
Molybdenum
7439-98-7
UG/L
200 U
200 U
200
U
100
U
60
U
60
U
40 U
Nickel
7440-02-0
UG/L
100 U
100 U
100
U
50
U
30
U
30
U
20 U
Potassium
7440-09-7
MG/L
160 A
160
120
88
46
55
33
Selenium
7782-49-2
UG/L
78 AJ
77 J
56
J
38
J
20
J
25
J
14 J
Silver
7440-22-4
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Sodium
7440-23-5
MG/L
3900 A
4000
3100
2200
1100
1400
800
Strontium
7440-24-6
UG/L
2800 A
2900
2300
1600
840
990
610
Thallium
7440-28-0
UG/L
2.5 U
2.5 U
2.5
U
2.5
U
2.5
U
2.5
U
2.5 U
Tin
7440-31-5
UG/L
NA
NA
NA
NA
NA
NA
NA
Titanium
7440-32-6
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Total Mercury
7439-97-6
UG/L
0.2 U
0.2 U
0.2
U
0.2
U
0.2
U
0.2
U
0.2 U
Vanadium
7440-62-2
UG/L
50 U
50 U
50
U
25
U
15
U
15
U
10 U
Yttrium
7440-65-5
UG/L
30 U
30 U
30
U
15
U
9
U
9
U
6 U
Zinc
7440-66-6
UG/L
100 U
100 U
100
U
50
U
30
U
30
U
20 U
PCB Scan
PCB-1016 (Aroclor 1016)
12674-11-2
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1221 (Aroclor 1221)
11104-28-2
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1232 (Aroclor 1232)
11141-16-5
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1242 (Aroclor 1242)
53469-21-9
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1248 (Aroclor 1248)
12672-29-6
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1254 (Aroclor 1254)
11097-69-1
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
PCB-1260 (Aroclor 1260)
11096-82-5
UG/L
2 U
2 U
2
U
2
U
2
U
2
U
2 U
Pesticides Scan
4,4'-DDD (p.p'-DDD)
72-54-8
UG/L
0.25 U
0.25 U
0.26
u
0.26
U
0.25
U
0.5
UJ
0.24 U
4,4'-DDE (p.p'-DDE)
72-55-9
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/L
0.25 U
0.25 U
0.26
u
0.26
u
0.25
u
0.5
UJ
0.24 U
Aldrin
309-00-2
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
alpha-BHC
319-84-6
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
alpha-Chlordane 12
5103-71-9
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
beta-BHC
319-85-7
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Chlordene 12
3734-48-3
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
cis-Nonachlor 12
5103-73-1
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
delta-BHC
319-86-8
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Dieldrin
60-57-1
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Endosulfan 1 (alpha)
959-98-8
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Endosulfan II (beta)
33213-65-9
UG/L
0.25 U
0.25 U
0.26
u
0.26
u
0.25
u
0.5
UJ
0.24 U
Endosulfan Sulfate
1031-07-8
UG/L
0.25 U
0.25 U
0.26
u
0.26
u
0.25
u
0.5
UJ
0.24 U
Endrin
72-20-8
UG/L
0.25 U
0.25 U
0.26
u
0.26
u
0.25
u
0.5
UJ
0.24 U
Endrin Ketone
53494-70-5
UG/L
0.25 U
0.25 U
0.26
u
0.26
u
0.25
u
0.5
UJ
0.24 U
gamma-BHC (Lindane)
58-89-9
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
gamma-Chlordane 12
5566-34-7
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Heptachlor
76-44-8
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Heptachlor Epoxide
1024-57-3
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Methoxychlor
72-43-5
UG/L
0.5 U
0.5 U
0.51
u
0.51
u
0.5
u
0.5
UJ
0.48 U
Toxaphene
8001-35-2
UG/L
10 U
10 U
10
u
10
u
10
u
10
UR
9.7 U
trans-Nonachlor 12
39765-80-5
UG/L
0.1 U
0.1 U
0.1
u
0.1
u
0.1
u
0.5
UJ
0.097 U
Volatiles Scan
(m- and/or p-)Xylene
UG/L
2 U
2 U
0.068
J
2
u
2
u
2
u
2 U
1,1,1,2-Tetrachloroethane
630-20-6
UG/L
1 U
1 U
1
u
1
u
1
u
1
u
1 U
1,1,1-Trichloroethane
71-55-6
UG/L
1 U
1 U
1
u
1
u
1
u
1
u
1 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/L
1 U
1 U
1
u
1
u
1
u
1
u
1 U
1,1,2-T richloro-1,2,2-T rifluoroethane
76-13-1
UG/L
1 U
1 U
1
u
1
u
1
u
1
u
1 U
55
-------
Back Bay Biloxi All Data
BBB1DSW BBB1SW BBB2SW BBB3SW BBB4SW BBB5SW BBB6SW
9/29/2005 9/29/2005 9/29/2005 9/29/2005 9/29/2005 9/29/2005 9/29/2005
1340 1312 1032 935 1300 1140 1025
1,2,4-T richlorobenzene
120-82-1
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,2,4-T rimethylbenzene
95-63-6
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/L
2
U
2
U
2 U
2
u
2
U
2 U
2
U
1,2-Dibromoethane (EDB)
106-93-4
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,2-Dichlorobenzene
95-50-1
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,2-Dichloroethane
107-06-2
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,2-Dichloropropane
78-87-5
UG/L
1
U
1
U
1 u
1
u
1
U
1 UJ
1
U
1,3,5-T rimethylbenzene
108-67-8
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,3-Dichlorobenzene
541-73-1
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,3-Dichloropropane
142-28-9
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
1,4-Dichlorobenzene
106-46-7
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
2,2-Dichloropropane
590-20-7
UG/L
1
U
1
U
1 u
1
u
1
U
1 UJ
1
U
Acetone
67-64-1
UG/L
2
U
2
U
2 U
2
u
2
U
2 U
2
U
Benzene
71-43-2
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
Bromobenzene
108-86-1
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
Bromochloromethane
74-97-5
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
1
U
Bromodichloromethane
75-27-4
UG/L
1
U
1
U
1 u
1
u
1
U
1 u
0.074
J
Bromoform
75-25-2
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Bromomethane
74-83-9
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Carbon Disulfide
75-15-0
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Carbon T etrachloride
56-23-5
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Chlorobenzene
108-90-7
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Chloroethane
75-00-3
UG/L
1
u
1
U
1 u
1
u
1
U
1 u
1
U
Chloroform
67-66-3
UG/L
1
u
1
U
1 u
1
u
1
u
1 u
0.092
J
Chloromethane
74-87-3
UG/L
1
u
1
U
1 u
1
u
1
u
1 u
1
U
cis-1,2-Dichloroethene
156-59-2
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
U
cis-1,3-Dichloropropene
10061-01-5
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
U
Cyclohexane
110-82-7
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
U
Dibromochloromethane
124-48-1
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
U
Dibromomethane
74-95-3
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Dichlorodifluoromethane
75-71-8
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Ethyl Benzene
100-41-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Hexachloro-1,3-Butadiene
87-68-3
UG/L
1
UJ
1
UJ
1 UJ
1
UJ
1
UJ
1 UJ
1
UJ
Isopropylbenzene
98-82-8
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Methyl Acetate
79-20-9
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Methyl Butyl Ketone
591-78-6
UG/L
2
u
2
u
2 U
2
u
2
u
2 U
2
u
Methyl Ethyl Ketone
78-93-3
UG/L
5
u
5
u
5 U
5
u
5
u
5 U
5
u
Methyl Isobutyl Ketone
108-10-1
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 UJ
1
u
Methylcyclohexane
108-87-2
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Methylene Chloride
75-09-2
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
n-Butylbenzene
104-51-8
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
n-Propylbenzene
103-65-1
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
o-Chlorotoluene
95-49-8
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
o-Xylene
95-47-6
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
p-Chlorotoluene
106-43-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
p-lsopropyltoluene
99-87-6
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
sec-Butylbenzene
135-98-8
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Styrene
100-42-5
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
tert-Butylbenzene
98-06-6
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Toluene
108-88-3
UG/L
1
u
0.13
J
0.2 J
1
u
1
u
0.09 J
1
u
trans-1,2-Dichloroethene
156-60-5
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
trans-1,3-Dichloropropene
10061-02-6
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Trichloroethene (Trichloroethylene)
79-01-6
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Trichlorofluoromethane (Freon11)
75-69-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Vinyl Chloride
75-01-4
UG/L
1
u
1
u
1 u
1
u
1
u
1 u
1
u
Extractables Scan
(3-and/or 4-)Methylphenol
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
1,1-Biphenyl
92-52-4
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
1,2,4-T richlorobenzene
120-82-1
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
2,3,4,6-Tetrachlorophenol
58-90-2
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
2,4,5-Trichlorophenol
95-95-4
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
2,4,6-Trichlorophenol
88-06-2
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
2,4-Dichlorophenol
120-83-2
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
2,4-Dimethylphenol
105-67-9
UG/L
10
u
9.6
u
10 u
10
u
9.7
u
9.6 U
9.7
u
56
-------
Back Bay Biloxi All Data
BBB1DSW
9/29/2005
1340
BBB1SW
9/29/2005
1312
BBB2SW
9/29/2005
1032
BBB3SW
9/29/2005
935
BBB4SW
9/29/2005
1300
BBB5SW
9/29/2005
1140
BBB6SW
9/29/2005
1025
2-Methylnaphthalene
91-57-6
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
2-Methylphenol
95-48-7
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
2-Nitroaniline
88-74-4
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
2-Nitrophenol
88-75-5
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
3,3'-Dichlorobenzidine
91-94-1
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
UR
9.7 U
3-Nitroaniline
99-09-2
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/L
10
U
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Chloro-3-Methylphenol
59-50-7
UG/L
10
u
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Chloroaniline
106-47-8
UG/L
10
u
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/L
10
u
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Nitroaniline
100-01-6
UG/L
10
u
9.6 U
10
U
10
U
9.7
U
9.6
U
9.7 U
4-Nitrophenol
100-02-7
UG/L
10
u
9.6 U
10
u
10
U
9.7
U
9.6
U
9.7 U
Acenaphthene
83-32-9
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Acenaphthylene
208-96-8
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Acetophenone
98-86-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Anthracene
120-12-7
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Atrazine
1912-24-9
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzaldehyde
100-52-7
UG/L
10
UJ
9.6 UJ
10
UJ
10
UJ
9.7
UJ
9.6
UJ
9.7 UJ
Benzo(a)Anthracene
56-55-3
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzo(b)Fluoranthene
205-99-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzo(ghi)Perylene
191-24-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzo(k)Fluoranthene
207-08-9
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzo-a-Pyrene
50-32-8
UG/L
10
u
9.6 U
10
u
10
u
9.7
U
9.6
U
9.7 U
Benzyl Butyl Phthalate
85-68-7
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
U
9.7 U
bis(2-Chloroethoxy)Methane
111-91-1
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
U
9.7 U
bis(2-Chloroethyl) Ether
111-44-4
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
bis(2-Chloroisopropyl) Ether
108-60-1
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Caprolactam
105-60-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Carbazole
86-74-8
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Chrysene
218-01-9
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Dibenzo(a,h)Anthracene
53-70-3
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Dibenzofuran
132-64-9
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Diethyl Phthalate
84-66-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Dimethyl Phthalate
131-11-3
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Di-n-Butylphthalate
84-74-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Di-n-Octylphthalate
117-84-0
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Fluoranthene
206-44-0
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Fluorene
86-73-7
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Hexachlorobenzene (HCB)
118-74-1
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Hexachlorobutadiene
87-68-3
UG/L
10
UJ
9.6 UJ
10
UJ
10
UJ
9.7
UJ
9.6
UJ
9.7 UJ
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Hexachloroethane
67-72-1
UG/L
10
UJ
9.6 UJ
10
UJ
10
UJ
9.7
UJ
9.6
UJ
9.7 UJ
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Isophorone
78-59-1
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Naphthalene
91-20-3
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Nitrobenzene
98-95-3
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
n-Nitroso di-n-Propylamine
621-64-7
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
n-Nitrosodiphenylamine/Diphenylamine
122-39-4
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Pentachlorophenol
87-86-5
UG/L
20
u
19 U
21
u
21
u
19
u
19
u
19 U
Phenanthrene
85-01-8
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Phenol
108-95-2
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Pyrene
129-00-0
UG/L
10
u
9.6 U
10
u
10
u
9.7
u
9.6
u
9.7 U
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.05
u
0.05 U
0.12
0.15
0.13
0.18
0.39
Nitrate-Nitrite Nitrogen
MG/L
0.05
u
0.05 U
0.05
u
0.05
u
0.1
0.071
0.54
Total Kjeldahl Nitrogen
MG/L
0.68
0.68
0.72
1.2
0.77
0.97
0.97
Total Organic Carbon
MG/L
11
5.2
6
12
10
9.1
11
Total Phosphorus
7723-14-0
MG/L
0.04
0.04
0.041
0.046
0.049
0.033
0.14
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
57
-------
Bay St Louis Surface Water All Data
BCD1SW
9/30/2005
1015
BLC1SW
9/30/2005
JR1SW PEARL1SW
9/30/2005 9/30/2005
1047 1615
SLB1SW
9/30/2005
1230
SLB2SW
9/30/2005
1430
SLB3SW
9/30/2005
1155
SLB4SW
9/30/2005
1320
SLB5SW
9/30/2005
1240
SLB6SW
9/30/2005
1010
SLB7SW
9/30/2005
1126
WR1SW
9/30/2005
1445
Metals Scan
Aluminum
Antimony
Arsenic
Barium
Beryllium
Cadmium
Calcium
Chromium
Cobalt
Copper
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Strontium
Thallium
Tin
T Itanium
Total Mercury
Vanadium
Yttrium
7429-90-5 UG/L
7440-36-0 UG/L
7440-38-2 UG/L
7440-39-3 UG/L
7440-41-7 UG/L
7440-43-9 UG/L
7440-70-2 MG/L
7440-47-3 UG/L
7440-48-4 UG/L
7440-50-8 UG/L
7439-89-6 MG/L
7439-92-1 UG/L
7439-95-4 MG/L
7439-96-5 UG/L
7439-98-7 UG/L
7440-02-0 UG/L
7440-09-7 MG/L
7782-49-2 UG/L
7440-22-4 UG/L
7440-23-5 MG/L
7440-24-6 UG/L
7440-28-0 UG/L
7440-31-5 UG/L
7440-32-6 UG/L
7439-97-6 UG/L
7440-62-2 UG/L
7440-65-5 UG/L
7440-66-6 UG/L
1100
2 5 U
20 J
67
30 U
12 U
160
50 U
50 U
50 U
50 U
100 U
160
61 J
50 U
4300
2800
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
9 6 J
65
30 U
12 U
70
50 U
50 U
50 U
100 U
66
25 J
50 U
1700
1100
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
30 U
12 U
110
50 U
50 U
50 U
50 U
100 U
100
39 J
50 U
2700
1800
2 5 U
50 U
0 2 U
50 U
30 U
100 U
200 U
2 5 U
4 6 J
40
10 U
10 U
10 U
0 76
2 5 U
110
870
10 U
20 U
10 U
0 2 U
10 U
1000 U
2 5 U
22 J
61
30 U
12 U
180
50 U
50 U
50 U
50 U
50 U
100 U
170
64 J
50 U
4500
3000
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
21 J
62
30 U
12 U
160
50 U
50 U
50 U
50 U
100 U
160
63 J
50 U
4100
2800
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
20 J
61
30 U
12 U
170
50 U
50 U
50 U
50 U
100 U
160
62 J
50 U
4200
2800
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
18 AJ
61 AJ
30 U
12 U
140 A
50 U
50 U
50 U
1 U
2 5 U
450 A
240 AJ
50 U
100 U
140 A
52 AJ
50 U
3600 A
2500 A
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
17 J
62
30 U
12 U
140
50 U
50 U
50 U
50 U
100 U
130
51 J
50 U
3500
2400
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
18 J
64
30 U
12 U
130
50 U
50 U
50 U
50 U
100 U
130
52 J
50 U
3400
2300
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
16 J
64
30 U
12 U
130
50 U
50 U
50 U
50 U
100 U
120
46 J
50 U
3100
2100
2 5 U
50 U
0 2 U
50 U
30 U
100 U
1000 U
2 5 U
30 U
12 U
160
50 U
50 U
50 U
50 U
100 U
160
31 J
50 U
4100
2800
2 5 U
50 U
0 2 U
50 U
30 U
100 U
PCB Scan
PCB-1016 (Aroc
PCB-1221 (Aroc
PCB-1232 (Aroc
PCB-1242 (Aroc
PCB-1248 (Aroc
PCB-1254 (Aroc
PCB-1260 (Aroc
-1016)
-1221)
- 1232)
-1242)
-1248)
-1254)
- 1260)
12674-1 1-2 UG/L
1 1104-28-2 UG/L
11141-16-5 UG/L
53469-21-9 UG/L
12672-29-6 UG/L
1 1097-69-1 UG/L
1 1096-82-5 UG/L
Pesticides Scan
44-DDD (p.p'-DDD)
44-DDE (p.p'-DDE)
44-DDT (p.p'-DDT)
Aldrin
alpha-BHC
alpha-Chlordane /2
beta-BHC
Chlordene /2
cis-Nonachlor /2
delta-BHC
Dieldnn
Endosulfan I (alpha)
Endosulfan II (beta)
Endosulfan Sulfate
Endrin Ketone
gamma-BHC (Lindane)
gamma-Chlordane /2
Heptachlor
Heptachlor Epoxide
Methoxychlor
T oxaphene
trans-Nonachlor /2
Volatiles Scan
(m- and/or p-)Xylene
1,1,1,2-Tetrachloroethane
1.1.1-Trichloroethane
1,1,2,2-Tetrachloroethane
1.1.2-T nchloro-1,2,2-Trifluoroethane
1.1.2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1.1-Dichloropropene
1.2.3-Trichlorobenzene
1,2,3-Trichloropropane
1,24-Trichlorobenzene
1,24-Trimethylbenzene
1.2-Dibromo-3-Chloropropane (DBCP)
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1.2-Dichloropropane
1,3,5-Trimethylbenzene
1.3-Dichlorobenzene
1,3-Dichloropropane
1 4-Dichlorobenzene
2,2-Dichloropropane
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromom ethane
Carbon Disulfide
Carbon Tetrachloride
Chlorobenzene
Chloroethane
UG/L
UG/L
1 UG/L
72-54-8 UG/L
72-55-9 UG/L
50-29-3 UG/L
309-00-2 UG/L
319-84-6 UG/L
5103-71-9 UG/L
319-85-7 UG/L
3734-48-3 UG/L
5103-73-1
319-86-8
60-57-1
959-98-8 UG/L
33213-65-9 UG/L
1031-07-8 UG/L
72-20-8 UG/L
53494-70-5 UG/L
58-89-9 UG/L
5566-34-7 UG/L
76-44-8 UG/L
1024-57-3 UG/L
72-43-5 UG/L
8001-35-2 UG/L
39765-80-5 UG/L
UG/L
630-20-6 UG/L
71-55-6 UG/L
79-34-5 UG/L
76-13-1 UG/L
79-00-5 UG/L
75-34-3 UG/L
75-35-4 UG/L
563-58-6 UG/L
87-61-6 UG/L
96-18-4 UG/L
120-82-1 UG/L
95-63-6 UG/L
96-12-8 UG/L
106-93-4 UG/L
1 UG/L
95-50-1
107-06-2 UG/L
78-87-5 UG/L
108-67-8 UG/L
541-73-1 UG/L
142-28-9 UG/L
106-46-7 UG/L
590-20-7 UG/L
67-64-1 UG/L
71-43-2 UG/L
108-86-1 UG/L
74-97-5 UG/L
75-27-4 UG/L
75-25-2 UG/L
74-83-9 UG/L
75-15-0 UG/L
56-23-5 UG/L
108-90-7 UG/L
75-00-3 UG/L
0 24 U
0 097 U
0 24 U
0 097 U
0 097 U
0 097 U
0 097 U
0 097 U
0 097 U
0 097 U
0 097 U
0 097 U
0 24 U
0 24 U
0 24 U
0 24 U
0 097 U
0 097 U
0 097 U
0 097 U
0 48 U
9 7 U
0 097 U
0 25 U
0 1 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 25 U
0 25 U
0 25 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 5 U
10 U
0 1 U
0 26 U
0 1 U
0 26 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 u
0 1 u
0 26 U
0 26 U
0 26 U
0 26 U
0 1 U
0 1 U
0 1 U
0 1 U
0 52 U
10 U
0 1 U
0 25 U
0 1 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 u
0 25 U
0 25 U
0 25 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 5 U
10 U
0 1 U
0 25 U
0 1 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 u
0 1 u
0 25 U
0 25 U
0 25 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 51 U
10 U
0 1 U
0 25 U
0 098 U
0 25 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 25 U
0 25 U
0 25 U
0 25 U
0 098 U
0 098 U
0 098 U
0 098 U
0 49 U
9 8 U
0 098 U
0 25 U
0 099 U
0 25 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 25 U
0 25 U
0 25 U
0 25 U
0 099 U
0 099 U
0 099 U
0 099 U
0 49 U
9 9 U
0 099 U
0 25 U
0 1 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 25 U
0 25 U
0 25 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 5 U
10 U
0 1 U
0 24 U
0 098 U
0 24 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 24 U
0 24 U
0 24 U
0 24 U
0 098 U
0 098 U
0 098 U
0 098 U
0 49 U
9 8 U
0 098 U
0 24 U
0 098 U
0 24 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 098 U
0 24 U
0 24 U
0 24 U
0 24 U
0 098 U
0 098 U
0 098 U
0 098 U
049 U
9 8 U
0 098 U
0 25 U
0 1 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 1 U
0 11 U
0 25 U
0 25 U
0 25 U
0 25 U
0 1 U
0 1 U
0 1 U
0 1 U
0 51 U
10 U
0 1 U
0 25 U
0 099 U
0 25 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 099 U
0 25 U
0 25 U
0 25 U
0 25 U
0 099 U
0 099 U
0 099 U
0 099 U
0 5 U
9 9 U
0 099 U
58
-------
1 u
1 u
1 u
1 UJ
1 u
1 u
2 U
5 U
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1 U
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
1 u
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
19 U
9 6 U
9 6 U
9 6 U
9 6 U
19 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 UJ
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
9 6 U
19 U
9 6 U
BCD1SW
9/30/2005
1015
BLC1SW
9/30/2005
JR1SW PEARL1SW SLB1SW
9/30/2005 9/30/2005 9/30/2005
1047 1615 1230
SLB2SW
9/30/2005
1430
SLB3SW
9/30/2005
1155
SLB4SW SLB5SW
9/30/2005 9/30/2005
1320 1240
74-95-3 UG/L
75-71-8 UG/L
100^1^1 UG/L
87-68-3 UG/L
98-82-8 UG/L
79-20-9
591-78-6
UG/L
UG/L
78-93-3 UG/L
1634-04-4 UG/L
108-87-2 UG/L
75-09-2 UG/L
104-51-8 UG/L
103-65-1 UG/L
95-49-8 UG/L
95-4 7-6 UG/L
106-43-4 UG/L
99-87-6 UG/L
135-98-8 UG/L
100-42-5 UG/L
98-06-6 UG/L
127-18-4 UG/L
108-88-3 UG/L
156-60-5 UG/L
10061-02-6 UG/L
79-01-6 UG/L
75-69-4 UG/L
75-01-4 UG/L
UG/L
92-5 2-4 UG/L
120-82-1 UG/L
58-90-2 UG/L
95-95-4 UG/L
88-06-2 UG/L
120-83-2 UG/L
105-67-9 UG/L
51-28-5 UG/L
121-14-2 UG/L
606-20-2 UG/L
91-58-7 UG/L
95-57-8 UG/L
534-52-1 UG/L
91-57-6 UG/L
95-48-7 UG/L
88-74-4 UG/L
88-75-5 UG/L
91-94-1 UG/L
99-09-2 UG/L
101-55-3 UG/L
59-50-7 UG/L
106-47-8 UG/L
7005-72-3 UG/L
100-01-6 UG/L
100-02-7 UG/L
83-32-9 UG/L
208-96-8 UG/L
98-86-2 UG/L
120-12-7 UG/L
1912-24-9 UG/L
100-52-7 UG/L
56-55-3 UG/L
205-99-2 UG/L
191-24-2 UG/L
207-08-9 UG/L
50-32-8 UG/L
85-68-7 UG/L
1-91-
UG/L
111-44-4 UG/L
108-60-1 UG/L
117-81-7 UG/L
105-60-2 UG/L
86-74-8 UG/L
218-01-9 UG/L
53-70-3 UG/L
132-64-9 UG/L
84-66-2 UG/L
131-11-3 UG/L
84-74-2 UG/L
117-84-0 UG/L
206-44-0 UG/L
86-73-7 UG/L
118-74-1 UG/L
87-68-3 UG/L
77-47-4 UG/L
67-72-1 UG/L
193-39-5 UG/L
78-59-1 UG/L
91-20-3 UG/L
98-95-3 UG/L
621-64-7 UG/L
122-39-4 UG/L
87-86-5 UG/L
85-01-8 UG/L
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
19 U
97 U
97 U
97 U
97 U
19 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
9 7 UJ
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
97 U
19 U
97 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 UJ
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
20 U
10 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
20 U
98 U
98 U
98 U
98 U
20 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 UJ
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
98 U
20 U
98 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
20 U
9 9 U
9 9 U
9 9 U
9 9 U
20 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 UJ
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
9 9 U
20 U
9 9 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 UJ
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
9 8 U
20 U
9 8 U
20 U
10 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
19 U
9 5 U
9 5 U
9 5 U
9 5 U
19 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 UJ
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
9 5 U
19 U
9 5 U
59
-------
Appendix C
Chemical Sediment Data
60
-------
Bayou Casotte Sediment All Data
Metals Scan
BC2SD
9/27/2005
1130
BC4DSD
9/27/2005
1300
BC4SD
9/27/2005
1240
BL1SD
9/27/2005
1415
% Moisture
%
60
41
49 A
39
Aluminum
7429-90-5
MG/KG
8200
2600
3000
1800 A
Antimony
7440-36-0
MG/KG
0.5
U
0.5 U
0.5 U
0.5 UJ
Arsenic
7440-38-2
MG/KG
6.4
1.2
0.87
2.4 A
Barium
7440-39-3
MG/KG
130
27
57
6.6 A
Beryllium
7440-41-7
MG/KG
0.82
0.3
0.3
0.3 U
Cadmium
7440-43-9
MG/KG
1.1
1.5
1.8
0.25 U
Calcium
7440-70-2
MG/KG
7400
4900
4700
1000 A
Chromium
7440-47-3
MG/KG
21
7.2
9.7
4.5 A
Cobalt
7440-48-4
MG/KG
4.6
0.59
0.66
1.1 A
Copper
7440-50-8
MG/KG
20
4.7
5.5
1.9 A
Iron
7439-89-6
MG/KG
17000
3400
3200
4900 A
Lead
7439-92-1
MG/KG
36
4.8
5.9
4.1 A
Magnesium
7439-95-4
MG/KG
5100
1800
1700
1400 A
Manganese
7439-96-5
MG/KG
450
26
26
46 A
Molybdenum
7439-98-7
MG/KG
1.6
U
1.6 U
1.6 U
1.6 U
Nickel
7440-02-0
MG/KG
8.4
2.4
2.7
2 A
Potassium
7440-09-7
MG/KG
2300
510
450
630 A
Selenium
7782-49-2
MG/KG
1
U
1 U
1 U
1 U
Silver
7440-22-4
MG/KG
0.5
U
0.5 U
0.5 U
0.5 U
Sodium
7440-23-5
MG/KG
18000
8500
5900
5300 AJ
Strontium
7440-24-6
MG/KG
57
59
66
10 A
Thallium
7440-28-0
MG/KG
0.5
U
0.5 U
0.5 U
0.5 U
Tin
7440-31-5
MG/KG
NA
NA
NA
NA
Titanium
7440-32-6
MG/KG
17
12
14
7.6 AJ
Total Mercury
7439-97-6
MG/KG
0.078
0.044 U
0.044 U
0.044 U
Vanadium
7440-62-2
MG/KG
24
6.1
7.3
9.5 A
Yttrium
7440-65-5
MG/KG
12
2.7
2.5
2.4 A
Zinc
7440-66-6
MG/KG
140
48
55
14 A
PCB Scan
% Moisture
%
64
30
34
36
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100
UJ
100 U
100 U
100 U
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100
UJ
100 U
100 U
100 U
Pesticides Scan
% Moisture
%
64
30
34
36
4,4'-DDD (p.p'-DDD)
72-54-8
UG/KG
27
U
14 U
15 U
15 U
4,4'-DDE (p.p'-DDE)
72-55-9
UG/KG
11
U
5.7 U
6 U
6.1 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/KG
41
U
14 U
15 U
15 U
Aldrin
309-00-2
UG/KG
11
U
5.7 U
6 U
6.1 U
alpha-BHC
319-84-6
UG/KG
11
U
5.7 U
6 U
6.1 U
alpha-Chlordane 12
5103-71-9
UG/KG
11
U
5.7 U
6 U
6.1 U
beta-BHC
319-85-7
UG/KG
28
U
5.7 U
6 U
6.1 U
Chlordene 12
3734-48-3
UG/KG
11
U
5.7 U
6 U
6.1 U
cis-Nonachlor 12
5103-73-1
UG/KG
11
U
5.7 U
6 U
6.1 U
delta-BHC
319-86-8
UG/KG
11
U
5.7 U
6 U
6.1 U
Dieldrin
60-57-1
UG/KG
11
U
5.7 U
6 U
6.1 U
Endosulfan 1 (alpha)
959-98-8
UG/KG
11
U
5.7 U
6 U
6.1 U
Endosulfan II (beta)
33213-65-9
UG/KG
27
U
14 U
15 U
15 U
Endosulfan Sulfate
1031-07-8
UG/KG
27
U
14 U
15 U
15 U
Endrin
72-20-8
UG/KG
27
u
14 U
15 U
15 U
Endrin Ketone
53494-70-5
UG/KG
35
u
18 U
19 U
15 U
gamma-BHC (Lindane)
58-89-9
UG/KG
11
u
5.7 U
6 U
6.1 U
gamma-Chlordane 12
5566-34-7
UG/KG
11
u
5.7 U
6 U
6.1 U
Heptachlor
76-44-8
UG/KG
11
u
6.8 U
6.8 U
8.8 U
Heptachlor Epoxide
1024-57-3
UG/KG
11
u
5.7 U
6 U
6.1 U
Methoxychlor
72-43-5
UG/KG
54
u
28 U
30 U
30 U
Toxaphene
8001-35-2
UG/KG
1080
u
570 U
600 U
610 U
61
-------
Bayou Casotte Sediment All Data
BC2SD BC4DSD BC4SD BL1SD
Metals Scan
9/27/2005
1130
9/27/2005
1300
9/27/2005
1240
9/27/2005
1415
1,1,1-Trichloroethane
71-55-6
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)
76-13-1
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1,2-Trichloroethane
79-00-5
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1-Dichloroethane
75-34-3
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1-Dichloroethene (1,1-Dichloroethylene)
75-35-4
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,1-Dichloropropene
563-58-6
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,2,3-T richlorobenzene
87-61-6
UG/KG
1.8
J
4.6
U
6.5
U
3.7 U
1,2,3-T richloropropane
96-18-4
UG/KG
7.7
U
4.6
U
6.5
U
3.7 U
1,2,4-T richlorobenzene
120-82-1
UG/KG
7.7
U
4.6
U
6.5
U
3.7 U
1,2,4-T ri methyl benzene
95-63-6
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
19
U
11
U
16
U
9.3 U
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,2-Dichlorobenzene
95-50-1
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,2-Dichloroethane
107-06-2
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,2-Dichloropropane
78-87-5
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,3,5-Tri methyl benzene
108-67-8
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,3-Dichlorobenzene
541-73-1
UG/KG
7.7
U
4.6
U
6.5
U
3.7 U
1,3-Dichloropropane
142-28-9
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
1,4-Dichlorobenzene
106-46-7
UG/KG
7.7
U
4.6
U
6.5
U
3.7 U
2,2-Dichloropropane
590-20-7
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
Acetone
67-64-1
UG/KG
39
U
23
U
33
U
19 U
Benzene
71-43-2
UG/KG
0.23
J
2.3
U
3.3
U
1.9 U
Bromobenzene
108-86-1
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
Bromochloromethane
74-97-5
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
Bromodichloromethane
75-27-4
UG/KG
3.9
U
2.3
U
3.3
U
1.9 U
Bromoform
75-25-2
UG/KG
19
U
11
U
16
U
9.3 U
Bromomethane
74-83-9
UG/KG
3.9
U
2.3
u
3.3
U
1.9 U
Carbon Disulfide
75-15-0
UG/KG
4.7
J
3.2
4.4
0.73 J
Carbon Tetrachloride
56-23-5
UG/KG
3.9
U
2.3
u
3.3
u
1.9 U
Chlorobenzene
108-90-7
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Chloroethane
75-00-3
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Chloroform
67-66-3
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Chloromethane
74-87-3
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
cis-1,2-Dichloroethene
156-59-2
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
cis-1,3-Dichloropropene
10061-01-5
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Cyclohexane
110-82-7
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Dibromochloromethane
124-48-1
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Dibromomethane
74-95-3
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Dichlorodifluoromethane
75-71-8
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Ethyl Benzene
100-41-4
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
3.9
u
2.3
u
CO
CO
u
1.9 U
Isopropyl benzene
98-82-8
UG/KG
14
2.3
u
CO
CO
u
1.9 U
Methyl Acetate
79-20-9
UG/KG
3.9
u
2.3
u
CO
CO
u
1.9 U
Methyl Butyl Ketone
591-78-6
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Methyl Ethyl Ketone
78-93-3
UG/KG
7.7
u
4.6
u
6.5
u
3.7 U
Methyl Isobutyl Ketone
108-10-1
UG/KG
3.9
u
2.3
u
CO
CO
u
1.9 U
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/KG
3.9
u
2.3
u
CO
CO
u
1.9 U
Methylcyclohexane
108-87-2
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Methylene Chloride
75-09-2
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
n-Butyl benzene
104-51-8
UG/KG
50
J
4.6
u
6.5
u
3.7 U
n-Propylbenzene
103-65-1
UG/KG
51
J
2.3
u
3.3
u
1.9 U
o-Chlorotoluene
95-49-8
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
o-Xylene
95-47-6
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
p-Chlorotoluene
106-43-4
UG/KG
7.7
u
4.6
u
6.5
u
3.7 U
p-lsopropyltoluene
99-87-6
UG/KG
43
J
2.3
u
3.3
u
1.9 U
sec-Butyl benzene
135-98-8
UG/KG
30
J
2.3
u
3.3
u
1.9 U
Styrene
100-42-5
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
tert-Butylbenzene
98-06-6
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Toluene
108-88-3
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
trans-1,2-Dichloroethene
156-60-5
UG/KG
19
u
11
u
16
u
9.3 U
trans-1,3-Dichloropropene
10061-02-6
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
3.9
u
2.3
u
3.3
u
1.9 U
62
-------
Bayou Casotte Sediment All Data
BC2SD BC4DSD BC4SD BL1SD
Metals Scan
9/27/2005
1130
9/27/2005
1300
9/27/2005
1240
9/27/2005
1415
Extractables Scan
% Moisture
%
63.61
29.58
33.67
35.82
(3-and/or 4-)Methylphenol
UG/KG
900
U
460
U
500
U
510 U
1,1-Biphenyl
92-52-4
UG/KG
900
U
460
U
500
U
510 U
1,2,4-T richlorobenzene
120-82-1
UG/KG
900
U
460
U
500
U
510 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
900
U
460
U
500
U
510 U
2,4,5-Trichlorophenol
95-95-4
UG/KG
900
U
460
U
500
U
510 U
2,4,6-Trichlorophenol
88-06-2
UG/KG
900
U
460
U
500
U
510 U
2,4-Dichlorophenol
120-83-2
UG/KG
900
U
460
U
500
U
510 U
2,4-Dimethylphenol
105-67-9
UG/KG
900
U
460
U
500
U
510 U
2,4-Dinitrophenol
51-28-5
UG/KG
1800
UJ
930
UJ
990
UJ
1000 UJ
2,4-Dinitrotoluene
121-14-2
UG/KG
900
U
460
U
500
U
510 U
2,6-Dinitrotoluene
606-20-2
UG/KG
900
U
460
U
500
U
510 U
2-Chloronaphthalene
91-58-7
UG/KG
900
U
460
U
500
U
510 U
2-Chlorophenol
95-57-8
UG/KG
900
U
460
U
500
U
510 U
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
1800
U
930
U
990
U
1000 U
2-Methylnaphthalene
91-57-6
UG/KG
900
U
460
U
500
U
510 U
2-Methylphenol
95-48-7
UG/KG
900
U
460
U
500
U
510 U
2-Nitroaniline
88-74-4
UG/KG
900
U
460
U
500
U
510 U
2-Nitrophenol
88-75-5
UG/KG
900
u
460
U
500
u
510 U
3,3'-Dichlorobenzidine
91-94-1
UG/KG
900
u
460
U
500
u
510 U
3-Nitroaniline
99-09-2
UG/KG
900
u
460
U
500
u
510 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
900
u
460
U
500
u
510 U
4-Chloro-3-Methylphenol
59-50-7
UG/KG
900
u
460
U
500
u
510 U
4-Chloroaniline
106-47-8
UG/KG
900
u
460
U
500
u
510 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
900
u
460
U
500
u
510 U
4-Nitroaniline
100-01-6
UG/KG
900
u
460
u
500
u
510 U
4-Nitrophenol
100-02-7
UG/KG
1800
u
930
u
990
u
1000 U
Acenaphthene
83-32-9
UG/KG
900
u
460
u
500
u
510 U
Acenaphthylene
208-96-8
UG/KG
900
u
460
u
500
u
510 U
Acetophenone
98-86-2
UG/KG
900
u
460
u
500
u
510 U
Anthracene
120-12-7
UG/KG
900
u
460
u
500
u
510 U
Atrazine
1912-24-9
UG/KG
900
u
460
u
500
u
510 U
Benzaldehyde
100-52-7
UG/KG
900
UJ
460
UJ
500
UJ
510 UJ
Benzo(a)A nth race ne
56-55-3
UG/KG
900
u
460
u
500
u
510 U
Benzo(b)Fluoranthene
205-99-2
UG/KG
900
u
460
u
500
u
510 U
Benzo(ghi)Perylene
191-24-2
UG/KG
900
u
460
u
500
u
510 U
Benzo(k)Fluoranthene
207-08-9
UG/KG
900
u
460
u
500
u
510 U
Benzo-a-Pyrene
50-32-8
UG/KG
900
u
460
u
500
u
510 U
Benzyl Butyl Phthalate
85-68-7
UG/KG
900
u
460
u
500
u
510 U
bis(2-Chloroethoxy)Methane
111-91-1
UG/KG
900
u
460
u
500
u
510 U
bis(2-Chloroethyl) Ether
111-44-4
UG/KG
900
u
460
u
500
u
510 U
bis(2-Chloroisopropyl) Ether
108-60-1
UG/KG
900
u
460
u
500
u
510 U
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/KG
900
u
460
u
500
u
510 U
Caprolactam
105-60-2
UG/KG
900
u
460
u
500
u
510 U
Carbazole
86-74-8
UG/KG
900
u
460
u
500
u
510 U
Chrysene
218-01-9
UG/KG
900
u
460
u
500
u
510 U
Dibenzo(a,h)Anthracene
53-70-3
UG/KG
900
u
460
u
500
u
510 U
Dibenzofuran
132-64-9
UG/KG
900
u
460
u
500
u
510 U
Diethyl Phthalate
84-66-2
UG/KG
900
u
460
u
500
u
510 U
Dimethyl Phthalate
131-11-3
UG/KG
900
u
460
u
500
u
510 U
Di-n-Butylphthalate
84-74-2
UG/KG
900
u
460
u
500
u
510 U
Di-n-Octylphthalate
117-84-0
UG/KG
900
u
460
u
500
u
510 U
Fluoranthene
206-44-0
UG/KG
900
u
66
J
500
u
510 U
Fluorene
86-73-7
UG/KG
900
u
460
u
500
u
510 U
Hexachlorobenzene (HCB)
118-74-1
UG/KG
900
u
460
u
500
u
510 U
Hexachlorobutadiene
87-68-3
UG/KG
900
u
460
u
500
u
510 U
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/KG
900
u
460
u
500
u
510 UJ
Hexachloroethane
67-72-1
UG/KG
900
u
460
u
500
u
510 U
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
900
u
460
u
500
u
510 U
Isophorone
78-59-1
UG/KG
900
u
460
u
500
u
510 U
Naphthalene
91-20-3
UG/KG
900
u
460
u
500
u
510 U
Nitrobenzene
98-95-3
UG/KG
900
u
460
u
500
u
510 U
63
-------
Bayou Casotte Sediment All Data
Metals Scan
BC2SD
9/27/2005
1130
BC4DSD
9/27/2005
1300
BC4SD
9/27/2005
1240
BL1SD
9/27/2005
1415
Classical Nutrients
Ammonia
7664-41-7
MG/KG
55
15
13
5.5
Nitrate-Nitrite Nitrogen
MG/KG
2.5 UJ
1.6
UJ
1.9 UJ
1.6
UJ
Total Kjeldahl Nitrogen
MG/KG
1400
430
330
450
Total Organic Carbon
MG/KG
17000
9800
U
9800 U
9400
U
Total Phosphorus
7723-14-0
MG/KG
1200
1800
2400
61
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
64
-------
Pascagoula Sediment All Data
ER1DSD
ER1SD
PR1SD
PR2SD
WPR1SD
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/28/2005
Metals Scan
1430
1400
1320
1545
1150
% Moisture
%
23
20
69
16
34
Aluminum
7429-90-5
MG/KG
180 A
210
5600
3700
1800
Antimony
7440-36-0
MG/KG
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Arsenic
7440-38-2
MG/KG
0.25 U
0.25 U
6.6
3.3
1.7
Barium
7440-39-3
MG/KG
1.7 A
1
24
19
5.4
Beryllium
7440-41-7
MG/KG
0.3 U
0.3 U
0.88
0.68
0.3 U
Cadmium
7440-43-9
MG/KG
0.12 U
0.12 U
0.38
0.28
0.12 U
Calcium
7440-70-2
MG/KG
71 A
50
2600
960
410
Chromium
7440-47-3
MG/KG
0.5 U
0.5 U
12
6.5
3.4
Cobalt
7440-48-4
MG/KG
0.5 U
0.5 U
5.6
7.7
2
Copper
7440-50-8
MG/KG
2 UJ
2 UJ
12
5.9
2.5
Iron
7439-89-6
MG/KG
270 A
370
16000
9900
4300
Lead
7439-92-1
MG/KG
2.1 A
1.3
16
8.1
3.8
Magnesium
7439-95-4
MG/KG
200 A
120
4500
2000
1200
Manganese
7439-96-5
MG/KG
1.7 A
2.5
270
130
38
Molybdenum
7439-98-7
MG/KG
5.2 U
5.2 U
5.2 U
5.2 U
5.2 U
Nickel
7440-02-0
MG/KG
0.99 U
1 U
6.1
3.9
1.9
Potassium
7440-09-7
MG/KG
99 U
100 U
1600
900
510
Selenium
7782-49-2
MG/KG
0.5 U
0.5 U
0.73
0.5 U
0.5 U
Silver
7440-22-4
MG/KG
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
Sodium
7440-23-5
MG/KG
1300 A
540
20000
7300
5400
Strontium
7440-24-6
MG/KG
1.5 A
1.1
39
19
8.1
Thallium
7440-28-0
MG/KG
0.25 U
0.25 U
0.25 U
0.25 U
0.25 U
Tin
7440-31-5
MG/KG
NA
NA
NA
NA
NA
Titanium
7440-32-6
MG/KG
2.6 AJ
2.8 J
22 J
13 J
11 J
Total Mercury
7439-97-6
MG/KG
0.045 U
0.044 U
0.055
0.043 U
0.042 U
Vanadium
7440-62-2
MG/KG
2 UJ
2 UJ
25
14
6.3
Yttrium
7440-65-5
MG/KG
0.3 U
0.3 U
11
8
3.6
Zinc
7440-66-6
MG/KG
1.6 A
1.9
71
30
15
PCB Scan
% Moisture
%
21
20
31
54
30
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100 U
100 U
100 UJ
100 UJ
100 U
Pesticides Scan
% Moisture
%
21
20
31
54
30
4,4'-DDD (p.p'-DDD)
72-54-8
UG/KG
10 U
10 U
12 U
18 U
12 U
4,4'-DDE (p, p'-DDE)
72-55-9
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/KG
10 U
10 U
12 U
18 U
12 U
Aldrin
309-00-2
UG/KG
4.1 U
4.1 U
4.8 U
9.8 U
6 U
alpha-BHC
319-84-6
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
alpha-Chlordane 12
5103-71-9
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
beta-BHC
319-85-7
UG/KG
4.1 U
4.1 U
4.8 U
23 U
8.7 U
Chlordene 12
3734-48-3
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
cis-Nonachlor 12
5103-73-1
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
delta-BHC
319-86-8
UG/KG
4.1 U
4.1 U
8.1 U
12 U
7.6 U
Dieldrin
60-57-1
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
Endosulfan 1 (alpha)
959-98-8
UG/KG
4.1 U
4.1 U
5.4 U
8.3 U
5.4 U
Endosulfan II (beta)
33213-65-9
UG/KG
10 U
10 U
12 U
18 U
12 U
Endosulfan Sulfate
1031-07-8
UG/KG
10 U
10 U
12 U
18 U
12 U
Endrin
72-20-8
UG/KG
10 U
10 U
12 U
18 U
12 U
Endrin Ketone
53494-70-5
UG/KG
10 U
10 U
12 U
18 U
15 U
gamma-BHC (Lindane)
58-89-9
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
gamma-Chlordane 12
5566-34-7
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
Heptachlor
76-44-8
UG/KG
4.1 U
4.1 U
6.2 U
7.3 U
5 U
Heptachlor Epoxide
1024-57-3
UG/KG
4.1 U
4.1 U
4.8 U
7.1 U
4.6 U
Methoxychlor
72-43-5
UG/KG
23 U
21 U
24 U
36 U
23 U
Toxaphene
8001-35-2
UG/KG
410 U
410 U
480 U
710 U
460 U
65
-------
Pascagoula Sediment All Data
ER1DSD ER1SD PR1SD PR2SD WPR1SD
Metals Scan
9/28/2005
1430
9/28/2005
1400
9/28/2005
1320
9/28/2005
1545
9/28/2005
1150
1,1,1-Trichloroethane
71-55-6
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)
76-13-1
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1,2-Trichloroethane
79-00-5
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1-Dichloroethane
75-34-3
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1-Dichloroethene (1,1-Dichloroethylene)
75-35-4
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,1-Dichloropropene
563-58-6
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,2,3-T richlorobenzene
87-61-6
UG/KG
2.4 U
2.5 U
10
U
6
U
3.4 U
1,2,3-Trichloropropane
96-18-4
UG/KG
2.4 U
2.5 U
10
U
6
U
3.4 U
1,2,4-T richlorobenzene
120-82-1
UG/KG
2.4 U
2.5 U
10
U
6
U
3.4 U
1,2,4-T rimethylbenzene
95-63-6
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
5.9 U
6.3 U
26
U
15
U
8.6 U
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,2-Dichlorobenzene
95-50-1
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,2-Dichloroethane
107-06-2
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,2-Dichloropropane
78-87-5
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,3,5-T rimethylbenzene
108-67-8
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,3-Dichlorobenzene
541-73-1
UG/KG
2.4 U
2.5 U
10
U
6
U
3.4 U
1,3-Dichloropropane
142-28-9
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
1,4-Dichlorobenzene
106-46-7
UG/KG
2.4 U
2.5 U
10
U
6
U
3.4 U
2,2-Dichloropropane
590-20-7
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
Acetone
67-64-1
UG/KG
12 U
12 U
70
U
30
U
17 U
Benzene
71-43-2
UG/KG
1.2 U
1.2 U
5.3
U
0.18
J
1.7 U
Bromobenzene
108-86-1
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
Bromochloromethane
74-97-5
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
Bromodichloromethane
75-27-4
UG/KG
1.2 U
1.2 U
5.3
U
3
U
1.7 U
Bromoform
75-25-2
UG/KG
5.9 U
6.3 U
26
U
15
U
8.6 U
Bromomethane
74-83-9
UG/KG
1.2 U
1.2 U
5.3
u
3
U
1.7 UJ
Carbon Disulfide
75-15-0
UG/KG
1.2 U
1.2 U
4.4
J
1.4
J
1.7 UJ
Carbon Tetrachloride
56-23-5
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Chlorobenzene
108-90-7
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Chloroethane
75-00-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Chloroform
67-66-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Chloromethane
74-87-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
cis-1,2-Dichloroethene
156-59-2
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
cis-1,3-Dichloropropene
10061-01-5
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Cyclohexane
110-82-7
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Dibromochloromethane
124-48-1
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Dibromomethane
74-95-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Dichlorodifluoromethane
75-71-8
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 UJ
Ethyl Benzene
100-41-4
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Isopropylbenzene
98-82-8
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Methyl Acetate
79-20-9
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 UJ
Methyl Butyl Ketone
591-78-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Methyl Ethyl Ketone
78-93-3
UG/KG
2.4 U
2.5 U
21
u
6
u
3.8 UJ
Methyl Isobutyl Ketone
108-10-1
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Methylcyclohexane
108-87-2
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Methylene Chloride
75-09-2
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
n-Butylbenzene
104-51-8
UG/KG
2.4 U
2.5 U
10
u
6
u
3.4 U
n-Propyl benzene
103-65-1
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
o-Chlorotoluene
95-49-8
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
o-Xylene
95-47-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
p-Chlorotoluene
106-43-4
UG/KG
2.4 U
2.5 U
10
u
6
u
3.4 U
p-lsopropyltoluene
99-87-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
sec-Butyl benzene
135-98-8
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Styrene
100-42-5
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
tert-Butylbenzene
98-06-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Toluene
108-88-3
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
trans-1,2-Dichloroethene
156-60-5
UG/KG
5.9 U
6.3 U
26
u
15
u
8.6 U
trans-1,3-Dichloropropene
10061-02-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
1.2 U
1.2 U
5.3
u
3
u
1.7 U
66
-------
Pascagoula Sediment All Data
ER1DSD ER1SD PR1SD PR2SD WPR1SD
Metals Scan
9/28/2005
1430
9/28/2005
1400
9/28/2005
1320
9/28/2005
1545
9/28/2005
1150
1,1-Biphenyl
92-52-4
UG/KG
400
U
410
U
440
U
710
U
450 U
1,2,4-Trichlorobenzene
120-82-1
UG/KG
400
U
410
U
440
U
710
U
450 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
400
U
410
U
440
U
710
U
450 U
2,4,5-Trichlorophenol
95-95-4
UG/KG
400
U
410
U
440
U
710
U
450 U
2,4,6-Trichlorophenol
88-06-2
UG/KG
400
U
410
U
440
U
710
U
450 U
2,4-Dichlorophenol
120-83-2
UG/KG
400
U
410
U
440
U
710
U
450 U
2,4-Dimethylphenol
105-67-9
UG/KG
400
U
410
U
440
U
710
U
450 U
2,4-Dinitrophenol
51-28-5
UG/KG
790
UJ
820
UJ
890
UJ
1400
UR
900 UJ
2,4-Dinitrotoluene
121-14-2
UG/KG
400
U
410
U
440
U
710
U
450 U
2,6-Dinitrotoluene
606-20-2
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Chloronaphthalene
91-58-7
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Chlorophenol
95-57-8
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
790
U
820
U
890
U
1400
UJ
900 U
2-Methylnaphthalene
91-57-6
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Methylphenol
95-48-7
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Nitroaniline
88-74-4
UG/KG
400
U
410
U
440
U
710
U
450 U
2-Nitrophenol
88-75-5
UG/KG
400
U
410
U
440
U
710
UJ
450 U
3,3'-Dichlorobenzidine
91-94-1
UG/KG
400
U
410
U
440
U
710
U
450 U
3-Nitroaniline
99-09-2
UG/KG
400
u
410
U
440
U
710
U
450 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
400
u
410
U
440
U
710
U
450 U
4-Chloro-3-Methylphenol
59-50-7
UG/KG
400
u
410
U
440
U
710
U
450 U
4-Chloroaniline
106-47-8
UG/KG
400
u
410
U
440
U
710
U
450 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
400
u
410
u
440
U
710
U
450 U
4-Nitroaniline
100-01-6
UG/KG
400
u
410
u
440
U
710
u
450 U
4-Nitrophenol
100-02-7
UG/KG
790
u
820
u
890
u
1400
u
900 U
Acenaphthene
83-32-9
UG/KG
400
u
410
u
440
u
710
u
450 U
Acenaphthylene
208-96-8
UG/KG
400
u
410
u
440
u
710
u
450 U
Acetophenone
98-86-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Anthracene
120-12-7
UG/KG
400
u
410
u
440
u
710
u
450 U
Atrazine
1912-24-9
UG/KG
400
UJ
410
UJ
440
UJ
710
UJ
450 UJ
Benzaldehyde
100-52-7
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzo(a)Anthracene
56-55-3
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzo(b)Fluoranthene
205-99-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzo(ghi)Perylene
191-24-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzo(k)Fluoranthene
207-08-9
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzo-a-Pyrene
50-32-8
UG/KG
400
u
410
u
440
u
710
u
450 U
Benzyl Butyl Phthalate
85-68-7
UG/KG
400
u
410
u
440
u
710
u
450 U
bis(2-Chloroethoxy (Methane
111-91-1
UG/KG
400
u
410
u
440
u
710
u
450 U
bis(2-Chloroethyl) Ether
111-44-4
UG/KG
400
u
410
u
440
u
710
u
450 U
bis(2-Chloroisopropyl) Ether
108-60-1
UG/KG
400
u
410
u
440
u
710
u
450 U
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/KG
400
u
410
u
440
u
710
u
450 U
Caprolactam
105-60-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Carbazole
86-74-8
UG/KG
400
UJ
410
UJ
440
UJ
710
UJ
450 UJ
Chrysene
218-01-9
UG/KG
400
u
410
u
440
u
710
u
450 U
Dibenzo(a,h)Anthracene
53-70-3
UG/KG
400
u
410
u
440
u
710
u
450 U
Dibenzofuran
132-64-9
UG/KG
400
u
410
u
440
u
710
u
450 U
Diethyl Phthalate
84-66-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Dimethyl Phthalate
131-11-3
UG/KG
400
UJ
410
UJ
440
UJ
710
UJ
450 UJ
Di-n-Butylphthalate
84-74-2
UG/KG
400
u
410
u
440
u
710
u
450 U
Di-n-Octyl phthalate
117-84-0
UG/KG
400
u
410
u
440
u
710
u
450 U
Fluoranthene
206-44-0
UG/KG
400
u
410
u
440
u
710
u
450 U
Fluorene
86-73-7
UG/KG
400
u
410
u
440
u
710
u
450 U
Hexachlorobenzene (HCB)
118-74-1
UG/KG
400
u
410
u
440
u
710
u
450 U
Hexachlorobutadiene
87-68-3
UG/KG
400
u
410
u
440
u
710
u
450 U
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/KG
400
u
410
u
440
u
710
UJ
450 U
Hexachloroethane
67-72-1
UG/KG
400
u
410
u
440
u
710
u
450 U
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
400
u
410
u
440
u
710
u
450 U
Isophorone
78-59-1
UG/KG
400
u
410
u
440
u
710
u
450 U
Naphthalene
91-20-3
UG/KG
400
u
410
u
440
u
710
u
450 U
Nitrobenzene
98-95-3
UG/KG
400
u
410
u
440
u
710
u
450 U
n-Nitroso di-n-Propylamine
621-64-7
UG/KG
400
u
410
u
440
u
710
u
450 U
n-Nitrosodiphenylamine/Diphenyl amine
122-39-4
UG/KG
400
u
410
u
440
u
710
u
450 U
Pentachlorophenol
87-86-5
UG/KG
790
u
820
u
890
u
1400
u
900 U
Phenanthrene
85-01-8
UG/KG
400
u
410
u
440
u
710
u
450 U
67
-------
Pascagoula Sediment All Data
Metals Scan
ER1DSD
9/28/2005
1430
ER1SD
9/28/2005
1400
PR1SD
9/28/2005
1320
PR2SD
9/28/2005
1545
WPR1SD
9/28/2005
1150
Total Kjeldahl Nitrogen
Total Organic Carbon
Total Phosphorus
MG/KG
MG/KG
7723-14-0 MG/KG
57
8700 U
26 U
57
8600 U
26 U
2200
39000 U
330
1200
15000
180
430
9500 U
86
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
68
-------
Back Bay Biloxi Sediment All Data
Metals Scan
BBB3DSD
9/29/2005
1005
BBB3SD
9/29/2005
945
BBB6SD
9/29/2005
1120
% Moisture
%
69
66
62
Aluminum
7429-90-5
MG/KG
7000
7800
5800
A
Antimony
7440-36-0
MG/KG
0.25
U
0.25
U
0.25
UJ
Arsenic
7440-38-2
MG/KG
5.2
5.5
4.7
A
Barium
7440-39-3
MG/KG
14
16
22
A
Beryllium
7440-41-7
MG/KG
0.99
1.1
0.57
A
Cadmium
7440-43-9
MG/KG
0.42
0.46
0.31
A
Calcium
7440-70-2
MG/KG
1400
1400
1700
A
Chromium
7440-47-3
MG/KG
12
12
11
A
Cobalt
7440-48-4
MG/KG
5.9
6
3.4
A
Copper
7440-50-8
MG/KG
14
J
15
J
13
AJ
Iron
7439-89-6
MG/KG
14000
J
15000
J
12000
AJ
Lead
7439-92-1
MG/KG
18
20
16
A
Magnesium
7439-95-4
MG/KG
3200
3200
2200
A
Manganese
7439-96-5
MG/KG
140
140
93
A
Molybdenum
7439-98-7
MG/KG
0.5
U
0.61
0.72
A
Nickel
7440-02-0
MG/KG
5.9
J
6.2
J
4
UJ
Potassium
7440-09-7
MG/KG
1200
1300
840
A
Selenium
7782-49-2
MG/KG
1
1.2
0.57
A
Silver
7440-22-4
MG/KG
0.5
U
0.5
U
0.5
U
Sodium
7440-23-5
MG/KG
6800
6000
5600
A
Strontium
7440-24-6
MG/KG
27
28
24
A
Thallium
7440-28-0
MG/KG
0.25
U
0.25
U
0.25
U
Tin
7440-31-5
MG/KG
NA
NA
NA
Titanium
7440-32-6
MG/KG
12
11
9
AJ
Total Mercury
7439-97-6
MG/KG
0.069
0.07
A
0.045
U
Vanadium
7440-62-2
MG/KG
16
17
16
A
Yttrium
7440-65-5
MG/KG
12
13
7.2
A
Zinc
7440-66-6
MG/KG
63
66
82
A
PCB Scan
% Moisture
%
70
68
63
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100
UJ
100
UJ
100
UJ
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100
UJ
100
UJ
100
UJ
Pesticides Scan
% Moisture
%
70
68
63
4,4'-DDD (p.p'-DDD)
72-54-8
UG/KG
28
U
26
UJ
20
UJ
4,4'-DDE (p.p'-DDE)
72-55-9
UG/KG
11
U
10
UJ
7.9
UJ
4,4'-DDT (p.p'-DDT)
50-29-3
UG/KG
40
U
37
UJ
20
UJ
Aldrin
309-00-2
UG/KG
15
U
14
UJ
10
UJ
alpha-BHC
319-84-6
UG/KG
11
U
10
UJ
7.9
UJ
alpha-Chlordane 12
5103-71-9
UG/KG
11
U
10
UJ
7.9
UJ
beta-BHC
319-85-7
UG/KG
11
U
26
UJ
24
UJ
Chlordene 12
3734-48-3
UG/KG
11
U
10
UJ
7.9
UJ
cis-Nonachlor 12
5103-73-1
UG/KG
11
U
10
UJ
7.9
UJ
delta-BHC
319-86-8
UG/KG
20
U
18
UJ
13
UJ
Dieldrin
60-57-1
UG/KG
12
U
10
UJ
7.9
UJ
Endosulfan 1 (alpha)
959-98-8
UG/KG
18
U
10
UJ
8.3
UJ
Endosulfan II (beta)
33213-65-9
UG/KG
28
U
26
UJ
20
UJ
Endosulfan Sulfate
1031-07-8
UG/KG
28
U
26
UJ
20
UJ
Endrin
72-20-8
UG/KG
28
U
26
UJ
20
UJ
Endrin Ketone
53494-70-5
UG/KG
28
U
26
UJ
20
UJ
gamma-BHC (Lindane)
58-89-9
UG/KG
11
u
10
UJ
7.9
UJ
69
-------
Back Bay Biloxi Sediment All Data
Metals Scan
BBB3DSD
9/29/2005
1005
BBB3SD
9/29/2005
945
BBB6SD
9/29/2005
1120
Volatiles Scan
% Moisture
%
69
66
62
(m- and/or p-)Xylene
UG/KG
14
U
8.7
u
8.7 U
1,1,1,2-Tetrachloroethane
630-20-6
UG/KG
6.8
U
4.3
U
4.3 U
1,1,1 -T richloroethane
71-55-6
UG/KG
6.8
U
4.3
U
4.3 U
1,1,2,2-T etrachloroethane
79-34-5
UG/KG
6.8
U
4.3
U
4.3 U
1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)
76-13-1
UG/KG
6.8
U
4.3
U
4.3 U
1,1,2-Trichloroethane
79-00-5
UG/KG
6.8
U
4.3
U
4.3 U
1,1-Dichloroethane
75-34-3
UG/KG
6.8
U
4.3
U
4.3 U
1,1 -Dichloroethene (1,1 -Dichloroethylene)
75-35-4
UG/KG
6.8
U
4.3
U
4.3 U
1,1-Dichloropropene
563-58-6
UG/KG
6.8
U
4.3
U
4.3 U
1,2,3-T richloro benzene
87-61-6
UG/KG
14
U
8.7
U
8.7 U
1,2,3-Trichloro propane
96-18-4
UG/KG
14
U
8.7
U
8.7 U
1,2,4-T richlorobenzene
120-82-1
UG/KG
14
U
8.7
U
8.7 U
1,2,4-Trimethyl benzene
95-63-6
UG/KG
6.8
U
4.3
U
4.3 U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
34
U
22
U
22 U
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
6.8
U
4.3
U
4.3 U
1,2-Dichlorobenzene
95-50-1
UG/KG
6.8
U
4.3
U
4.3 U
1,2-Dichloroethane
107-06-2
UG/KG
6.8
U
4.3
U
4.3 U
1,2-Dichloropropane
78-87-5
UG/KG
6.8
U
4.3
U
4.3 U
1,3,5-T rimethylbenzene
108-67-8
UG/KG
6.8
U
4.3
U
2 J
1,3-Dichlorobenzene
541-73-1
UG/KG
14
U
8.7
U
8.7 U
1,3-Dichloropropane
142-28-9
UG/KG
6.8
U
4.3
U
4.3 U
1,4-Dichlorobenzene
106-46-7
UG/KG
14
U
8.7
U
8.7 U
2,2-Dichloropropane
590-20-7
UG/KG
6.8
U
4.3
U
4.3 U
Acetone
67-64-1
UG/KG
68
U
40
u
43 U
Benzene
71-43-2
UG/KG
6.8
U
4.3
u
4.3 U
Bromobenzene
108-86-1
UG/KG
6.8
U
4.3
u
4.3 U
Bromochloromethane
74-97-5
UG/KG
6.8
U
4.3
u
4.3 U
Bromodichloromethane
75-27-4
UG/KG
6.8
u
4.3
u
4.3 U
Bromoform
75-25-2
UG/KG
34
u
22
u
22 U
Bromomethane
74-83-9
UG/KG
6.8
UJ
4.3
UJ
4.3 UJ
Carbon Disulfide
75-15-0
UG/KG
6.8
u
4.3
UJ
4.3 U
Carbon Tetrachloride
56-23-5
UG/KG
6.8
u
CO
u
4.3 U
Chloro benzene
108-90-7
UG/KG
6.8
u
CO
u
4.3 U
Chloroethane
75-00-3
UG/KG
6.8
u
CO
u
4.3 U
Chloroform
67-66-3
UG/KG
6.8
u
CO
u
4.3 U
Chloro methane
74-87-3
UG/KG
6.8
u
CO
u
4.3 U
cis-1,2-Dichloroethene
156-59-2
UG/KG
6.8
u
CO
u
4.3 U
cis-1,3-Dichloropropene
10061-01-5
UG/KG
6.8
u
CO
u
4.3 U
Cyclohexane
110-82-7
UG/KG
6.8
u
CO
u
4.3 U
Di bromochloromethane
124-48-1
UG/KG
6.8
u
CO
u
4.3 U
Di bromomethane
74-95-3
UG/KG
6.8
u
CO
u
4.3 U
Dichlorodifluoromethane
75-71-8
UG/KG
6.8
UJ
CO
UJ
4.3 UJ
Ethyl Benzene
100-41-4
UG/KG
6.8
u
CO
u
4.3 U
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
6.8
u
CO
u
4.3 U
Isopropylbenzene
98-82-8
UG/KG
6.8
u
CO
u
0.87 J
Methyl Acetate
79-20-9
UG/KG
6.8
UJ
CO
UJ
4.3 UJ
Methyl Butyl Ketone
591-78-6
UG/KG
6.8
u
CO
u
4.3 U
Methyl Ethyl Ketone
78-93-3
UG/KG
11
J
9.7
UJ
8.7 UJ
Methyl Isobutyl Ketone
108-10-1
UG/KG
6.8
u
CO
u
4.3 U
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/KG
6.8
u
CO
u
4.3 U
Methylcyclohexane
108-87-2
UG/KG
6.8
u
CO
u
4.3 U
Methylene Chloride
75-09-2
UG/KG
6.8
u
CO
u
4.3 U
n-Butyl benzene
104-51-8
UG/KG
14
u
8.7
u
3.6 J
n-Propylbenzene
103-65-1
UG/KG
6.8
u
CO
u
2.1 J
o-Chlorotoluene
95-49-8
UG/KG
6.8
u
CO
u
4.3 U
o-Xylene
95-47-6
UG/KG
6.8
u
CO
u
0.39 J
70
-------
Back Bay Biloxi Sediment All Data
Metals Scan
BBB3DSD
9/29/2005
1005
BBB3SD
9/29/2005
945
BBB6SD
9/29/2005
1120
Toluene
108-88-3
UG/KG
6.8
u
4.3
u
4.3 U
trans-1,2-Dichloroethene
156-60-5
UG/KG
34
u
22
u
22 U
trans-1,3-Dichloropropene
10061-02-6
UG/KG
6.8
u
4.3
u
4.3 U
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
6.8
u
4.3
u
4.3 U
Trichlorofluoromethane (Freon11)
75-69-4
UG/KG
6.8
u
4.3
u
4.3 U
Vinyl Chloride
75-01-4
UG/KG
6.8
u
4.3
u
4.3 U
Extractables Scan
% Moisture
%
70
68.22
62.62
(3-and/or 4-)Methylphenol
UG/KG
1100
u
1000
u
850 U
1,1 -Biphenyl
92-52-4
UG/KG
1100
u
1000
u
850 U
1,2,4-Trichlorobenzene
120-82-1
UG/KG
1100
u
1000
u
850 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
1100
u
1000
u
850 U
2,4,5-Trichlorophenol
95-95-4
UG/KG
1100
u
1000
u
850 U
2,4,6-Trichlorophenol
88-06-2
UG/KG
1100
u
1000
u
850 U
2,4-Dichlorophenol
120-83-2
UG/KG
1100
u
1000
u
850 U
2,4-Dimethylphenol
105-67-9
UG/KG
1100
u
1000
u
850 U
2,4-Dinitrophenol
51-28-5
UG/KG
2200
UJ
2000
UJ
1700 UJ
2,4-Dinitrotoluene
121-14-2
UG/KG
1100
u
1000
u
850 U
2,6-Dinitrotoluene
606-20-2
UG/KG
1100
u
1000
u
850 U
2-Chloronaphthalene
91-58-7
UG/KG
1100
u
1000
u
850 U
2-Chlorophenol
95-57-8
UG/KG
1100
u
1000
u
850 U
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
2200
u
2000
u
1700 U
2-Methylnaphthalene
91-57-6
UG/KG
1100
u
1000
u
850 U
2-Methylphenol
95-48-7
UG/KG
1100
u
1000
u
850 U
2-Nitroaniline
88-74-4
UG/KG
1100
u
1000
u
850 U
2-Nitrophenol
88-75-5
UG/KG
1100
u
1000
u
850 U
3,3'-Dichlorobenzidine
91-94-1
UG/KG
1100
u
1000
u
850 U
3-Nitroaniline
99-09-2
UG/KG
1100
u
1000
u
850 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
1100
u
1000
u
850 U
4-Chloro-3-Methylphenol
59-50-7
UG/KG
1100
u
1000
u
850 U
4-Chloroaniline
106-47-8
UG/KG
1100
u
1000
u
850 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
1100
u
1000
u
850 U
4-Nitroaniline
100-01-6
UG/KG
1100
u
1000
u
850 U
4-Nitrophenol
100-02-7
UG/KG
2200
u
2000
u
1700 U
Acenaphthene
83-32-9
UG/KG
1100
u
1000
u
850 U
Acenaphthylene
208-96-8
UG/KG
1100
u
1000
u
850 U
Acetophenone
98-86-2
UG/KG
1100
u
1000
u
850 U
Anthracene
120-12-7
UG/KG
1100
u
1000
u
850 U
Atrazine
1912-24-9
UG/KG
1100
UJ
1000
UJ
850 UJ
Benzaldehyde
100-52-7
UG/KG
1100
u
1000
u
850 U
Be nzo(a) Anthracene
56-55-3
UG/KG
1100
u
1000
u
850 U
Benzo(b)Fluoranthene
205-99-2
UG/KG
1100
u
1000
u
850 U
Benzo(ghi)Perylene
191-24-2
UG/KG
1100
u
1000
u
850 U
Benzo(k)Fluoranthene
207-08-9
UG/KG
1100
u
1000
u
850 U
Benzo-a-Pyrene
50-32-8
UG/KG
1100
u
1000
u
850 U
Benzyl Butyl Phthalate
85-68-7
UG/KG
1100
u
1000
u
850 U
bis(2-Chloroethoxy)Methane
111-91-1
UG/KG
1100
u
1000
u
850 U
bis(2-Chloroethyl) Ether
111-44-4
UG/KG
1100
u
1000
u
850 U
bis(2-Chloroisopropyl) Ether
108-60-1
UG/KG
1100
u
1000
u
850 U
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/KG
1100
u
1000
u
850 U
Caprolactam
105-60-2
UG/KG
1100
u
1000
u
850 U
Carbazole
86-74-8
UG/KG
1100
UJ
1000
UJ
850 UJ
Chrysene
218-01-9
UG/KG
1100
u
1000
u
850 U
Dibenzo(a.h) Anthracene
53-70-3
UG/KG
1100
u
1000
u
850 U
Dibenzofuran
132-64-9
UG/KG
1100
u
1000
u
850 U
Diethyl Phthalate
84-66-2
UG/KG
1100
u
1000
u
850 U
Dimethyl Phthalate
131-11-3
UG/KG
1100
UJ
1000
UJ
850 UJ
Di-n-Butylphthalate
84-74-2
UG/KG
1100
u
1000
u
850 U
71
-------
Back Bay Biloxi Sediment All Data
Metals Scan
9/29/2005
1005
9/29/2005
945
9/29/2005
1120
Hexachloroethane
67-72-1
UG/KG
1100
U
1000
U
850
U
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
1100
U
1000
U
850
U
Isophorone
78-59-1
UG/KG
1100
U
1000
U
850
U
Naphthalene
91-20-3
UG/KG
1100
U
1000
U
850
U
Nitrobenzene
98-95-3
UG/KG
1100
U
1000
U
850
U
n-Nitroso di-n-Propylamine
621-64-7
UG/KG
1100
U
1000
U
850
U
n-Nitrosodiphenylamine/Diphenylamine
122-39-4
UG/KG
1100
U
1000
U
850
U
Pentachlorophenol
87-86-5
UG/KG
2200
U
2000
U
1700
U
Phenanthrene
85-01-8
UG/KG
1100
U
1000
U
850
U
Phenol
108-95-2
UG/KG
1100
U
1000
U
850
U
Pyrene
129-00-0
UG/KG
1100
U
1000
U
120
J
Classical Nutrients
Ammonia
7664-41-7
MG/KG
52
77
91
Nitrate-Nitrite Nitrogen
MG/KG
3.1
UJ
2.8
UJ
5.1
UJ
Total Kjeldahl Nitrogen
MG/KG
2300
2400
1700
Total Organic Carbon
MG/KG
26000
28000
20000
Total Phosphorus
7723-14-0
MG/KG
300
330
430
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is 'average' of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
72
-------
Bay St Louis Sediment All Data
Metals Scan
PEARL1SD
9/29/2005
1645
SLB2SD
9/30/2005
1520
SLB3SD
9/30/2005
1230
SLB6DSD
9/30/2005
1100
SLB6SD
9/30/2005
1040
% Moisture
%
65
23
52
56
57
Aluminum
7429-90-5
MG/KG
5600
1200 A
4600
6600
6100
Antimony
7440-36-0
MG/KG
0.25 U
0.25 U
0.25 U
0.25
U
0.25 U
Arsenic
7440-38-2
MG/KG
3.4
1.5 A
4.4
8.9
9
Barium
7440-39-3
MG/KG
37
6.7 A
18
19
18
Beryllium
7440-41-7
MG/KG
0.86
0.3 U
0.51
0.77
0.72
Cadmium
7440-43-9
MG/KG
0.2
0.12 U
0.17
0.24
0.21
Calcium
7440-70-2
MG/KG
1800
1400 A
2600
4400
1700
Chromium
7440-47-3
MG/KG
10
2 A
6.6
10
9.4
Cobalt
7440-48-4
MG/KG
4.2
1.6 A
4.8
7.7
7.5
Copper
7440-50-8
MG/KG
9.6 J
1.5 A
5.2
6.7
6.2
Iron
7439-89-6
MG/KG
8800 J
3000 A
10000
16000
16000
Lead
7439-92-1
MG/KG
17
3.2 A
9.8
15
14
Magnesium
7439-95-4
MG/KG
3000
700 A
2600
3500
3300
Manganese
7439-96-5
MG/KG
160
78 A
210
260
240
Molybdenum
7439-98-7
MG/KG
0.99
0.5 U
0.5 U
0.5
U
0.5 U
Nickel
7440-02-0
MG/KG
8.3 J
1.5 A
5.4
8
7.6
Potassium
7440-09-7
MG/KG
1000
340 A
1200
1600
1500
Selenium
7782-49-2
MG/KG
0.66
0.5 U
0.5 U
0.5
U
0.5 U
Silver
7440-22-4
MG/KG
0.5 U
0.5 U
0.5 U
0.5
U
0.5 U
Sodium
7440-23-5
MG/KG
3100
1600 A
5600
5900
5900
Strontium
7440-24-6
MG/KG
31
10 A
26
37
22
Thallium
7440-28-0
MG/KG
0.25 U
0.25 U
0.25 U
0.25
U
0.25 U
Tin
7440-31-5
MG/KG
NA
NA
NA
NA
NA
Titanium
7440-32-6
MG/KG
16
12 AJ
17 J
20
J
19 J
Total Mercury
7439-97-6
MG/KG
0.046 U
0.046 U
0.046 U
0.047
U
0.049 U
Vanadium
7440-62-2
MG/KG
17
3.5 A
13
19
18
Yttrium
7440-65-5
MG/KG
14
2.6 A
7.9
11
10
Zinc
7440-66-6
MG/KG
22
9.7 A
32
42
41
PCB Scan
% Moisture
%
68
23
54
36
58
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100 UJ
100 U
100 UJ
100
UJ
100 UJ
Pesticides Scan
% Moisture
%
68
23
54
56
58
4,4'-DDD (p.p'-DDD)
72-54-8
UG/KG
24 UJ
9.9 U
18 U
18
U
19 U
4,4'-DDE (p.p'-DDE)
72-55-9
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/KG
34 UJ
9.9 U
18 U
18
U
19 U
Aldrin
309-00-2
UG/KG
9.7 UJ
4 U
7 U
9.3
U
9.7 U
alpha-BHC
319-84-6
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
alpha-Chlordane 12
5103-71-9
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
beta-BHC
319-85-7
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
Chlordene 12
3734-48-3
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
cis-Nonachlor 12
5103-73-1
UG/KG
9.7 UJ
4 U
7 U
7.2
U
7.8 U
delta-BHC
319-86-8
UG/KG
14 UJ
6.4 U
11 U
11
U
7.8 U
Dieldrin
60-57-1
UG/KG
9.7 UJ
4 U
7.9 U
7.2
U
7.8 U
Endosulfan 1 (alpha)
959-98-8
UG/KG
9.7 UJ
4 U
7.9 U
8.2
U
7.8 U
Endosulfan II (beta)
33213-65-9
UG/KG
24 UJ
9.9 U
18 U
18
U
19 U
Endosulfan Sulfate
1031-07-8
UG/KG
24 UJ
9.9 U
18 U
18
U
19 U
Endrin
72-20-8
UG/KG
24 UJ
9.9 U
18 U
18
U
19 U
Endrin Ketone
53494-70-5
UG/KG
24 UJ
9.9 U
18 U
18
u
25 U
gamma-BHC (Lindane)
58-89-9
UG/KG
9.7 UJ
4 U
7 U
7.2
u
7.8 U
gamma-Chlordane 12
5566-34-7
UG/KG
9.7 UJ
4 U
7 U
7.2
u
7.8 U
Heptachlor
76-44-8
UG/KG
10 UJ
4 U
7 U
7.2
u
7.8 U
Heptachlor Epoxide
1024-57-3
UG/KG
9.7 UJ
4 U
7 U
7.2
u
7.8 U
Methoxychlor
72-43-5
UG/KG
49 UJ
20 U
35 U
36
u
39 U
Toxaphene
8001-35-2
UG/KG
970 UJ
400 U
700 U
720
u
780 U
trans-Nonachlor 12
39765-80-5
UG/KG
9.7 UJ
4 U
7 U
7.2
u
7.8 U
73
-------
Bay St Louis Sediment All Data
Metals Scan
PEARL1SD
9/29/2005
1645
SLB2SD
9/30/2005
1520
SLB3SD
9/30/2005
1230
SLB6DSD
9/30/2005
1100
SLB6SD
9/30/2005
1040
1,1,1-Trichloroethane
71-55-6
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)
76-13-1
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1,2-Trichloroethane
79-00-5
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1-Dichloroethane
75-34-3
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1-Dichloroethene (1,1-Dichloroethylene)
75-35-4
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,1-Dichloropropene
563-58-6
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,2,3-Trichlorobenzene
87-61-6
UG/KG
8.3
U
2.8
U
5.4
U
6.5
U
6.8 U
1,2,3-Trichloropropane
96-18-4
UG/KG
8.3
U
2.8
U
5.4
U
6.5
U
6.8 U
1,2,4-Trichlorobenzene
120-82-1
UG/KG
8.3
U
2.8
U
5.4
U
6.5
U
6.8 U
1,2,4-Trimethylbenzene
95-63-6
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
21
U
7
U
14
U
16
U
17 U
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,2-Dichlorobenzene
95-50-1
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,2-Dichloroethane
107-06-2
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,2-Dichloropropane
78-87-5
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,3,5-Trimethylbenzene
108-67-8
UG/KG
0.25
J
1.4
U
2.7
U
3.2
U
3.4 U
1,3-Dichlorobenzene
541-73-1
UG/KG
8.3
U
2.8
U
5.4
U
6.5
U
6.8 U
1,3-Dichloropropane
142-28-9
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
1,4-Dichlorobenzene
106-46-7
UG/KG
8.3
U
2.8
U
5.4
U
6.5
U
6.8 U
2,2-Dichloropropane
590-20-7
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
Acetone
67-64-1
UG/KG
42
U
14
U
27
U
32
U
34 U
Benzene
71-43-2
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
Bromobenzene
108-86-1
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
Bromochloromethane
74-97-5
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
Bromodichloromethane
75-27-4
UG/KG
4.2
U
1.4
U
2.7
U
3.2
U
3.4 U
Bromoform
75-25-2
UG/KG
21
U
7
U
14
U
16
U
17 U
Bromomethane
74-83-9
UG/KG
4.2
UJ
1.4
UJ
2.7
UJ
3.2
UJ
3.4 UJ
Carbon Disulfide
75-15-0
UG/KG
5
UJ
1.4
UJ
2.7
UJ
3.2
UJ
3.4 UJ
Carbon Tetrachloride
56-23-5
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Chlorobenzene
108-90-7
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Chloroethane
75-00-3
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Chloroform
67-66-3
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Chloromethane
74-87-3
UG/KG
4.2
u
1.4
UJ
2.7
u
3.2
u
3.4 U
cis-1,2-Dichloroethene
156-59-2
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
cis-1,3-Dichloropropene
10061-01-5
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Cyclohexane
110-82-7
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Dibromochloromethane
124-48-1
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Dibromomethane
74-95-3
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Dichlorodifluoromethane
75-71-8
UG/KG
4.2
UJ
1.4
UJ
2.7
UJ
3.2
UJ
3.4 UJ
Ethyl Benzene
100-41-4
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Isopropylbenzene
98-82-8
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Methyl Acetate
79-20-9
UG/KG
4.2
UJ
1.4
UJ
2.7
UJ
3.2
UJ
3.4 UJ
Methyl Butyl Ketone
591-78-6
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Methyl Ethyl Ketone
78-93-3
UG/KG
8.3
UJ
2.8
UJ
5.4
UJ
6.5
UJ
6.8 UJ
Methyl Isobutyl Ketone
108-10-1
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Methylcyclohexane
108-87-2
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Methylene Chloride
75-09-2
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
n-Butylbenzene
104-51-8
UG/KG
8.3
u
2.8
u
5.4
u
6.5
u
6.8 U
n-Propylbenzene
103-65-1
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
o-Chlorotoluene
95-49-8
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
o-Xylene
95-47-6
UG/KG
0.21
J
1.4
u
2.7
u
3.2
u
3.4 U
p-Chlorotoluene
106-43-4
UG/KG
8.3
u
2.8
u
5.4
u
6.5
u
6.8 U
p-lsopropyltoluene
99-87-6
UG/KG
3.4
J
1.4
u
2.7
u
3.2
u
3.4 U
sec-Butylbenzene
135-98-8
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Styrene
100-42-5
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
tert-Butylbenzene
98-06-6
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Toluene
108-88-3
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
trans-1,2-Dichloroethene
156-60-5
UG/KG
21
u
7
u
14
u
16
u
17 U
trans-1,3-Dichloropropene
10061-02-6
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
Trichlorofluoromethane (Freon 11)
75-69-4
UG/KG
4.2
u
1.4
u
2.7
u
3.2
u
3.4 U
74
-------
Bay St Louis Sediment All Data
Metals Scan
PEARL1SD
9/29/2005
1645
SLB2SD
9/30/2005
1520
SLB3SD
9/30/2005
1230
SLB6DSD
9/30/2005
1100
SLB6SD
9/30/2005
1040
1,1-Bi phenyl
92-52-4
UG/KG
980
U
430
U
700
U
740
U
740 U
1,2,4-T richlorobenzene
120-82-1
UG/KG
980
U
430
U
700
U
740
U
740 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
980
U
430
U
700
U
740
U
740 U
2,4,5-T richlorophenol
95-95-4
UG/KG
980
U
430
U
700
U
740
U
740 U
2,4,6-T richlorophenol
88-06-2
UG/KG
980
U
430
U
700
U
740
U
740 U
2,4-Dichlorophenol
120-83-2
UG/KG
980
U
430
U
700
U
740
U
740 U
2,4-Dimethylphenol
105-67-9
UG/KG
980
U
430
U
700
U
740
U
740 U
2,4-Dinitrophenol
51-28-5
UG/KG
2000
UJ
860
UJ
1400
UJ
1500
UJ
1500 UJ
2,4-Dinitrotoluene
121-14-2
UG/KG
980
U
430
U
700
U
740
U
740 U
2,6-Dinitrotoluene
606-20-2
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Chloronaphthalene
91-58-7
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Chlorophenol
95-57-8
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
2000
U
860
U
1400
U
1500
U
1500 U
2-Methylnaphthalene
91-57-6
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Methylphenol
95-48-7
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Nitroaniline
88-74-4
UG/KG
980
U
430
U
700
U
740
U
740 U
2-Nitrophenol
88-75-5
UG/KG
980
U
430
U
700
U
740
U
740 U
3,3'-Dichlorobenzidine
91 -94-1
UG/KG
980
U
430
U
700
u
740
U
740 U
3-Nitroaniline
99-09-2
UG/KG
980
U
430
U
700
u
740
U
740 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
980
U
430
U
700
u
740
U
740 U
4-Chloro-3-Methylphenol
59-50-7
UG/KG
980
U
430
U
700
u
740
U
740 U
4-Chloroaniline
106-47-8
UG/KG
980
U
430
U
700
u
740
U
740 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
980
U
430
U
700
u
740
U
740 U
4-Nitroaniline
100-01-6
UG/KG
980
u
430
U
700
u
740
u
740 U
4-Nitrophenol
100-02-7
UG/KG
2000
u
860
u
1400
u
1500
u
1500 U
Acenaphthene
83-32-9
UG/KG
980
u
430
u
700
u
740
u
740 U
Acenaphthylene
208-96-8
UG/KG
980
u
430
u
700
u
740
u
740 U
Acetophenone
98-86-2
UG/KG
980
u
430
u
700
u
740
u
740 U
Anthracene
120-12-7
UG/KG
980
u
430
u
700
u
740
u
740 U
Atrazine
1912-24-9
UG/KG
980
UJ
430
u
700
u
740
u
740 U
Benzaldehyde
100-52-7
UG/KG
980
u
430
UJ
700
UJ
740
UJ
740 UJ
Benzo(a) Anthracene
56-55-3
UG/KG
980
u
58
J
700
u
740
u
740 U
Benzo(b)Fluoranthene
205-99-2
UG/KG
980
u
130
J
700
u
740
u
740 U
Benzo(ghi)Perylene
191-24-2
UG/KG
980
u
74
J
700
u
740
u
740 U
Benzo(k)Fluoranthene
207-08-9
UG/KG
980
u
120
J
700
u
740
u
740 U
Benzo-a-Pyrene
50-32-8
UG/KG
980
u
130
J
700
u
740
u
740 U
Benzyl Butyl Phthalate
85-68-7
UG/KG
980
u
430
u
700
u
740
u
740 U
bis(2-Chloroethoxy)Methane
111-91-1
UG/KG
980
u
430
u
700
u
740
u
740 U
bis(2-Chloroethyl) Ether
111-44-4
UG/KG
980
u
430
u
700
u
740
u
740 U
bis(2-Chloroisopropyl) Ether
108-60-1
UG/KG
980
u
430
u
700
u
740
u
740 U
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/KG
980
u
430
u
700
u
740
u
740 U
Caprolactam
105-60-2
UG/KG
980
u
430
u
700
u
740
u
740 U
Carbazole
86-74-8
UG/KG
980
UJ
430
u
700
u
740
u
740 U
Chrysene
218-01-9
UG/KG
980
u
82
J
700
u
740
u
740 U
D i be nz o(a, h) A nt h racen e
53-70-3
UG/KG
980
u
47
J
700
u
740
u
740 U
Dibenzofuran
132-64-9
UG/KG
980
u
430
u
700
u
740
u
740 U
Diethyl Phthalate
84-66-2
UG/KG
980
u
430
u
700
u
740
u
740 U
Dimethyl Phthalate
131-11-3
UG/KG
980
UJ
430
u
700
u
740
u
740 U
Di-n-Butylphthalate
84-74-2
UG/KG
980
u
430
u
700
u
740
u
740 U
Di-n-Octylphthalate
117-84-0
UG/KG
980
u
430
u
700
u
740
u
740 U
Fluoranthene
206-44-0
UG/KG
980
u
98
J
700
u
740
u
740 U
Fluorene
86-73-7
UG/KG
980
u
430
u
700
u
740
u
740 U
Hexachlorobenzene (HCB)
118-74-1
UG/KG
980
u
430
u
700
u
740
u
740 U
Hexachlorobutadiene
87-68-3
UG/KG
980
u
430
u
700
u
740
u
740 U
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/KG
980
u
430
u
700
u
740
u
740 U
Hexachloroethane
67-72-1
UG/KG
980
u
430
u
700
u
740
u
740 U
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
980
u
84
J
700
u
740
u
740 U
Isophorone
78-59-1
UG/KG
980
u
430
u
700
u
740
u
740 U
Naphthalene
91-20-3
UG/KG
980
u
430
u
700
u
740
u
740 U
Nitrobenzene
98-95-3
UG/KG
980
u
430
u
700
u
740
u
740 U
n-Nitroso di-n-Propylamine
621-64-7
UG/KG
980
u
430
u
700
u
740
u
740 U
n-Nitrosodiphenylamine/Diphenylamine
122-39-4
UG/KG
980
u
430
u
700
u
740
u
740 U
Pentachlorophenol
87-86-5
UG/KG
2000
u
860
u
1400
u
1500
u
1500 U
Phenanthrene
85-01-8
UG/KG
980
u
430
u
700
u
740
u
740 U
Phenol
108-95-2
UG/KG
980
u
430
u
700
u
740
u
740 U
75
-------
Bay St Louis Sediment All Data
Metals Scan
PEARL1SD
9/29/2005
1645
SLB2SD
9/30/2005
1520
SLB3SD
9/30/2005
1230
SLB6DSD
9/30/2005
1100
SLB6SD
9/30/2005
1040
Total Kjeldahl Nitrogen
Total Organic Carbon
Total Phosphorus
MG/KG
MG/KG
7723-14-0 MG/KG
2500
58000
100
270
9500 U
65
940
16000
160
1300
14000
170
1200
13000
160
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
76
-------
Table 16
Sediment Dioxin Results
Pascagoula, Escatawpa, and St. Louis Bays
Septemebr 28&30, 2005
ER1DSD
ER1SD
PR1SD
PR2SD
SLB2SD
SLB6SD
9/28/2005
9/28/2005
9/28/2005
9/28/2005
9/30/2005
9/30/2005
Dioxin Scan
1430
1400
1320
1545
1520
1040
% Moisture
%
21
19
51
52
23
55
1,2,3,4,6,7,8-Heptachlorodibenzodioxin
35822-46-9
NG/KG
7
11
220
290
50
330
1,2,3,4,6,7,8-Heptachlorodibenzofuran
67562-39-4
NG/KG
8.4 U
0.47 U
8.9
9
1.4 J
9.1
1,2,3,4,7,8,9-Heptachlorodibenzofuran
55673-89-7
NG/KG
1.1 J
0.15 U
0.8 J
0.7 U
0.15 J
1.1 U
1,2,3,4,7,8-Hexachlorodibenzodioxin
39227-28-6
NG/KG
1.9 U
0.24 J
2 J
1.9 J
0.56 J
3.9
1,2,3,4,7,8-Hexachlorodibenzofuran
70648-26-9
NG/KG
2.2 U
0.15 U
1.2 U
0.78 U
0.17 U
1 U
1,2,3,6,7,8-Hexachlorodibenzodioxin
57653-85-7
NG/KG
1.9 U
0.39 J
4.7
6.2
1.1 J
7.5
1,2,3,6,7,8-Hexachlorodibenzofuran
57117-44-9
NG/KG
11 U
0.14 U
0.58 U
0.56 U
0.17 U
1.1 U
1,2,3,7,8,9-Hexachlorodibenzodioxin
19408-74-3
NG/KG
2 U
0.72 J
8.9
12
2.3
16
1,2,3,7,8,9-Hexachlorodibenzofuran
72918-21-9
NG/KG
0.68 J
0.15 U
0.37 U
0.35 U
0.089 U
0.36 U
1,2,3,7,8-Pentachlorodibenzodioxin
40321-76-4
NG/KG
1.5 U
0.14 U
0.67 J
0.74 J
0.22 J
1.2 J
1,2,3,7,8-Pentachlorodibenzofuran
57117-41-6
NG/KG
1.5 U
0.16 U
0.4 U
0.25 U
0.1 U
0.4 U
2,3,4,6,7,8-Hexachlorodibenzofuran
60851-34-5
NG/KG
1.1 J
0.17 U
0.77 U
0.71 U
0.17 U
1.4 U
2,3,4,7,8-Pentachlorodibenzofuran
57117-31-4
NG/KG
1.4 U
0.2 U
0.77 U
0.43 U
0.15 U
0.58 U
2,3,7,8-Tetrachlorodibenzodioxin
1746-01-6
NG/KG
0.21 U
0.19 U
1.1
0.81 J
0.1 U
0.3 U
2,3,7,8-Tetrachlorodibenzofuran
51207-31-9
NG/KG
1.1 U
1.6 U
12
2.4
0.16 U
0.53 U
Heptachlorodibenzodioxin (Total)
NG/KG
19 J
30 J
870 J
840 J
180 J
1200 J
Heptachlorodibenzofuran (Total)
38998-75-3
NG/KG
1.1 J
0.37 J
30 J
28 J
3.4 J
22 J
Hexachlorodibenzodioxin (Total)
34465-46-8
NG/KG
1.9 UJ
11 J
270 J
250 J
75 J
520 J
Hexachlorodibenzofuran (Total)
55684-94-1
NG/KG
22 J
0.33 J
13 J
11 J
1.6 J
11 J
Octachlorodibenzodioxin
3268-87-9
NG/KG
170
300
5000 J
10000 J
1100
5700 J
Octac h lorod i be nzof u ra n
39001-02-0
NG/KG
5.9
0.8 J
18
20
3.2 J
19
Pentachlorodibenzodioxin (Total)
36088-22-9
NG/KG
1.5 UJ
1.4 J
38 J
33 J
11 J
84 J
Pentachlorodibenzofuran (Total)
30402-15-4
NG/KG
9.1 J
0.21 J
4 J
4.1 J
0.57 J
6.1 J
Tetrachlorodibenzodioxin (Total)
41903-57-5
NG/KG
0.54 J
0.63 J
28 J
25 J
5.5 J
44 J
Tetrachlorodibenzofuran (Total)
55722-27-5
NG/KG
12 J
2.9 J
28 J
7.5 J
0.74 J
7.9 J
TEQ (Avian Toxic. Equiv. Value, From WHO TEQ-98)
NG/KG
6.2 J
2.3 J
17 J
7.4 J
1.2 J
5.8 J
TEQ (Fish Toxic. Equiv. Value, From WHO TEQ-98)
NG/KG
5.1 J
0.75 J
5 J
1 J
5.3 J
TEQ (Mammalian Toxic. Equiv. Value, From WHO TEQ-98)
NG/KG
4.8
0.93 J
8
8.3
1.5 J
8.9
Shaded entries indicate exceedence of EPA screening values (below)
EPA Sediment Screening Values Low Risk High Risk
Fish 60 100
Mammalian Wildlife 2.5 25
Avian Wildlife 21 210
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
77
-------
Appendix D
In-Situ Water Quality Profiles
78
-------
Banss Lake & Bayou Casotte
Table
Bangs Lake - Station BL1
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
DO.
pH
CONDUCTIVITY SALINITY TEMPERAT
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
9/27/2005
1245
1
6.82
7.47
37344
23.54
29.67
2
6.62
7.47
37345
23.56
29.57
3
5.71
7.31
37385
23.59
28.84
MAX
6.82
7.47
37385
23.59
29.67
MIN
5.71
7.31
37344
23.54
28.84
AVG
6.38
7.42
37358
23.56
29.36
Instantaneous minimum dissolved oxygen concentration less than 4.0 mg
79
-------
DATE
TIME
9/27/2005 1110
DEPTH D.O.
(ft) (mg/1)
pH CONDUCTIVITYSALINITY*TEMPERATURE
(us/cm) (ppt) (°C)
Surf
5.64
7.73
45478
27.2
28.74
1
5.49
7.76
45545
27.2
28.72
3
5.11
7.81
46549
28.1
28.43
5
5.01
7.83
46764
28.2
28.40
7
4.93
7.84
47007
28.4
28.37
9
4.82
7.84
47388
28.7
28.34
11
4.82
7.85
47499
28.8
28.33
13
4.75
7.85
47581
28.8
28.33
15
4.75
7.85
47689
28.9
28.33
17
4.68
7.85
47831
29.0
28.33
19
4.59
7.85
47978
29.1
28.34
21
4.58
7.85
48035
29.1
28.35
23
4.58
7.85
48173
29.2
28.36
25
4.58
7.86
48193
29.2
28.36
27
4.57
7.85
48214
29.2
28.37
29
4.55
7.85
48226
29.2
28.37
31
4.47
7.85
48307
29.3
28.37
33
4.37
7.85
48542
29.4
28.40
35
4.36
7.85
48604
29.5
28.42
37
4.01
7.82
48898
29.6
28.44
39
3.69
7.81
49201
29.2
28.47
41
3.90
7.84
49302
29.9
28.49
43
4.14
7.88
49479
30.0
28.50
45
4.29
7.90
49554
30.0
28.51
MAX
5.64
7.90
49554
30.00
28.74
MIN
3.69
7.73
45478
27.20
28.33
AVG
4.61
7.84
47918
28.97
28.42
* Note: Salinity was calculated post-field study using conductivity and temperature measurem
Instantaneous minimum dissolved oxygen concentration less than 4.0 ms
80
-------
Table
Bayou Casotte - Station BC2
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/27/2005 1310
MAX
MIN
AVG
Surf
6.25
7.09
44877
26.4
29.44
1
6.03
7.14
45009
26.5
29.4
3
5.74
7.46
45625
27.1
28.97
5
5.31
7.73
46254
27.8
28.62
7
5.11
7.75
46670
28.1
28.52
9
4.61
7.77
46907
28.4
28.3
11
4.31
7.74
47369
28.7
28.32
13
4.23
7.75
47359
28.7
28.32
15
4.16
7.75
47816
29.0
28.34
17
4.23
7.77
47892
29.0
28.34
19
4.27
7.77
47908
29.0
28.34
21
4.32
7.78
47950
29.1
28.34
23
4.34
7.79
47996
29.1
28.35
25
4.37
7.79
48053
29.1
28.35
27
4.37
7.80
48133
29.2
28.36
29
4.41
7.81
48269
29.3
28.38
31
4.27
7.79
48360
29.3
28.38
33
4.25
7.81
48649
29.5
28.42
35
4.10
7.80
48687
29.5
28.42
37
3.95
7.79
48775
29.6
28.43
39
3.91
7.79
48796
29.6
28.44
41
3.93
7.80
48884
29.6
28.45
43
3.97
7.83
49199
29.8
28.46
6.25
7.83
49199
29.80
29.44
3.91
7.09
44877
26.40
28.30
4.54
7.71
47628
28.76
28.51
Instantaneous minimum dissolved oxygen concentration less than 4.0 mg
81
-------
Table
Bayou Casotte - Station BC3
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
9/28/2005 1505
MAX
MIN
AVG
DEPTH
D.O.
pH
CONDUCTIVITY SALINITY TEMPERAT
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
Surf
6.64
7.04
43938
25.7
29.55
1
6.79
7.24
44843
26.5
29.20
3
5.44
7.71
46499
28.0
28.55
5
5.06
7.79
46631
28.1
28.41
7
4.77
7.75
46781
28.2
28.40
9
4.56
7.78
47283
28.6
28.30
11
4.49
7.79
47597
28.8
28.31
13
4.47
7.79
47754
28.9
28.32
15
4.08
7.76
48005
29.1
28.35
17
4.06
7.76
48165
29.2
28.36
19
3.98
7.76
48303
29.3
28.37
21
3.98
7.77
48367
29.3
28.37
23
4.00
7.77
48416
29.4
28.38
25
4.01
7.78
48428
29.4
28.38
27
4.01
7.78
48430
29.4
28.39
29
4.02
7.78
48430
29.4
28.39
31
4.03
7.79
48433
29.4
28.39
33
3.61
7.74
48694
29.5
28.42
35
3.25
7.73
48866
29.6
28.44
37
3.39
7.77
48989
29.7
28.46
39
3.60
7.79
49102
29.8
28.47
41
3.70
7.79
49145
29.8
28.48
43
3.32
7.75
49204
29.8
28.49
6.79
7.79
49204
29.80
29.55
3.25
7.04
43938
25.70
28.30
4.32
7.71
47839
28.91
28.49
Instantaneous minimum dissolved oxygen concentration less than 4.0 ms
82
-------
Bayou Casotte - Station BC4
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/27/2005 1435
Surf
1
2
12.30
12.82
9.25
7.81
7.80
7.78
39913
40189
41304
31.27
30.65
30.33
MAX
MIN
AVG
12.82
9.25
11.46
7.81
7.78
7.80
41304
39913
40469
31.27
30.33
30.75
Instantaneous minimum ilissokoil owuen concentration less than 4 <> i
83
-------
Pascagoula, Escatawpa & West Pascagoula Rivers
Table
West Pascagoula River - Station WPR1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/28/2005
4045
MAX
MIN
AVG
SURF
6.77
7.00
10153
5.63
28.22
1
6.51
6.97
10476
5.84
28.25
3
5.92
7.16
20347
12.28
28.77
5
5.26
7.52
31242
19.35
28.71
7
5.47
7.64
33896
21.15
28.77
9
4.94
7.64
35729
22.40
28.57
11
4.81
7.67
37732
23.85
28.55
13
4.82
7.69
38102
24.10
28.56
15
4.96
7.71
38100
24.10
28.54
17
5.38
7.76
38353
24.28
28.71
19
5.26
7.76
38608
24.46
28.69
21
5.08
7.74
38662
24.49
28.50
23
5.03
7.74
39098
24.81
28.46
25
5.03
7.75
39336
24.97
28.47
Bottom
5.03
7.75
39375
25.00
28.47
6.77
7.76
39375
25.00
28.77
4.81
6.97
10153
5.63
28.22
5.35
7.57
32614
20.45
28.55
Instantaneous minimum dissolved oxygen concentration less than 4.0 mg
84
-------
Table
West Pascagoula River - Station WPR2
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
DO.
pH
CONDUCTIVITY SALINITY TEMPERATURE
9/28/2005 -1350
MAX
MIN
AVG
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
SURF
8.22
7.35
1430
0.72
28.74
1
6.01
6.89
1531
0.77
28.80
3
5.85
6.80
1588
0.79
28.77
5
5.69
6.74
1674
0.84
28.75
7
5.58
6.72
1763
0.87
28.79
9
5.40
6.71
2319
1.58
28.85
11
4.33
6.69
5517
3.04
28.84
13
3.70
6.61
7417
6.45
29.03
15
3.51
6.66
13280
7.20
28.99
17
3.45
6.74
14165
9.09
29.06
19
3.39
6.74
16280
9.55
29.08
21
3.38
6.74
16979
9.99
29.09
23
3.36
6.75
17780
10.32
29.09
25
3.35
6.76
17866
10.56
29.11
27
3.26
6.79
20119
11.81
29.13
BOTTOM
3.23
6.82
19837
11.73
29.13
8.22
7.35
20119
11.81
29.13
3.23
6.61
1430
0.72
28.74
4.48
6.78
9972
5.96
28.95
Instantaneous minimum dissolved oxygen concentration less than 4.0 ms
85
-------
Table
Pascagoula River - Station PR1
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
9/28/2005 -1210
MAX
MIN
AVG
DEPTH
DO.
pH
CONDUCTIVITY SALINITY TEMPERAT
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
Surf
7.56
7.61
24965
15.20
28.28
1
7.31
7.64
26584
16.50
28.28
3
7.19
7.71
29431
18.03
28.31
5
5.94
7.77
38226
23.78
28.40
7
5.27
7.78
39988
25.51
28.44
9
4.87
7.78
42443
27.25
28.49
11
4.57
7.79
43171
27.65
28.50
13
4.51
7.79
43774
28.15
28.50
15
4.50
7.81
44027
28.29
28.50
17
4.47
7.80
44265
28.50
28.53
19
4.41
7.80
44541
28.64
28.50
21
4.40
7.80
44353
28.53
28.51
23
4.39
7.81
44800
28.86
28.50
25
4.35
7.82
44830
28.86
28.49
27
4.46
7.82
44864
28.89
28.49
29
4.37
7.82
44891
28.90
28.50
31
4.39
7.82
45136
29.05
28.48
33
4.47
7.84
45874
29.70
28.48
35
4.46
7.85
46229
29.91
28.48
37
4.42
7.85
46570
30.11
28.48
39
4.28
7.85
46707
30.25
28.49
BOTTOM
4.12
7.83
46778
30.28
28.49
7.56
7.85
46778
30.28
28.53
4.12
7.61
24965
15.20
28.28
4.94
7.79
41929
26.86
28.46
Instantaneous minimum dissolved oxygen concentration less than 4.0 r
86
-------
Table
Pascagoula River - Station PR2
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
DO.
(ft) (mg/1)
pH CONDUCTIVITY SALINITY TEMPERATURE
(|is/cm) (ppt) (°C)
9/28/2005 -1530
MAX
MIN
AVG
1
6.33
6.82
4024
2.21
28.06
3
5.92
6.67
4697
2.58
28.97
5
5.70
6.59
5152
2.86
28.94
7
5.11
6.52
6641
3.81
28.87
9
4.99
6.53
7683
4.53
28.88
11
3.13
6.52
20642
12.25
28.75
13
2.94
6.84
34559
21.99
28.67
15
2.97
7.02
35910
22.59
28.58
17
2.95
7.09
36329
22.88
28.58
19
2.99
7.14
37239
23.47
28.57
21
3.16
7.27
40147
25.52
28.51
23
3.01
7.33
41553
26.46
28.47
6.33
7.33
41553
26.46
28.97
2.94
6.52
4024
2.21
28.06
4.10
6.86
22881
14.26
28.65
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
87
-------
Table
Escatawpa River - Station ER1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY S ALINITYTEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/28/2005 -1350 1
5.30
6.28
6774
3.69
29.20
3
5.06
6.22
6921
3.74
29.15
5
4.93
6.21
7644
4.07
29.12
7
4.04
6.26
10302
5.85
29.03
9
3.31
6.80
28466
18.51
28.75
11
3.39
7.18
37473
23.66
28.58
13
3.84
7.41
42149
27.01
28.52
15
3.90
7.48
42660
27.34
28.47
17
3.94
7.52
43356
27.88
28.45
19
3.94
7.54
43609
28.00
28.44
21
3.92
7.55
43556
27.97
28.44
23
3.89
7.55
43627
28.02
28.44
MAX
5.30
7.55
43627
28.02
29.20
MIN
3.31
6.21
6774
3.69
28.44
AVG
4.12
7.00
29711
18.81
28.72
Instantaneous minimum dissolved oxygen concentration less than 3.0 r
88
-------
Table
Escatawpa River - Station ER2
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/28/2005 -1105
MAX
MIN
AVG
1
3.35
5.85
3560
1.80
28.32
3
3.01
5.89
5662
3.12
28.51
5
2.35
6.09
12342
6.78
28.83
7
2.39
6.20
17742
10.43
28.84
9
2.25
6.47
23367
14.29
28.77
11
2.36
6.60
27184
16.83
28.69
13
2.32
6.71
31549
19.62
28.62
15
2.39
6.83
32866
20.44
28.59
17
2.48
6.93
34314
21.45
28.57
19
2.45
6.96
34271
21.42
28.57
3.35
6.96
34314
21.45
28.84
2.25
5.85
3560
1.80
28.32
2.54
6.45
22286
13.62
28.63
Instantaneous minimum dissolved oxygen concentration less than 3.0 n
89
-------
Back Bay of Biloxi
Table
Back Bay of Biloxi - Station BBB1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/29/2005 1312
MAX
MIN
AVG
SURF
8.95
8.08
23790
13.34
28.96
1
8.74
8.05
23919
14.47
28.82
2
8.59
8.03
23965
14.46
29.06
3
8.51
8.01
24072
14.52
28.97
4
8.34
7.99
24205
14.62
28.81
5
7.53
7.88
24980
15.07
28.52
6
6.52
7.75
26154
15.95
28.25
7
5.67
7.65
27829
16.76
28.41
8
4.54
7.50
30069
18.64
28.53
9
4.26
7.47
30700
18.96
28.55
10
4.01
7.45
30813
19.05
28.55
11
3.40
7.42
34376
21.47
28.60
BOTTOM
3.25
7.43
34376
21.52
28.61
8.95
8.08
34376
21.52
29.06
3.25
7.42
23790
13.34
28.25
6.33
7.75
27634
16.83
28.66
Instantaneous minimum dissoked o.wuen concentration less than 4 <> n
90
-------
Table
Back Bay of Biloxi - Station BBB2
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/29/2005 1025
MAX
MIN
AVG
SURF
7.35
7.61
14860
8.59
28.58
1
7.34
7.60
15909
9.21
28.27
2
7.30
7.62
17292
10.15
28.17
3
6.66
7.53
18792
11.1
28.01
4
6.28
7.47
19517
11.53
28.09
5
6.21
7.49
20057
11.93
28.08
6
6.06
7.49
21590
12.76
28.04
7
5.84
7.50
22650
13.61
27.99
8
5.65
7.51
23097
13.91
28.08
9
5.60
7.52
23316
14.07
28.12
10
5.43
7.52
24553
14.85
28.17
11
5.27
7.52
25079
15.28
28.25
7.35
7.62
25079
15.28
28.58
5.27
7.47
14860
8.59
27.99
6.25
7.53
20559
12.25
28.15
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
91
-------
Table
Back Bay of Biloxi - Station BBB3
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/29/2005 935
MAX
MIN
AVG
SURF
6.92
7.46
13602
7.81
28.14
1
6.88
7.46
13585
7.80
28.14
2
6.87
7.46
13617
7.82
28.11
3
6.74
7.44
13697
7.87
20.10
4
6.28
7.37
14320
8.26
28.09
5
6.03
7.33
14697
8.66
28.39
6
5.19
7.25
18916
10.86
28.73
7
4.97
7.26
19604
11.59
28.78
6.92
7.46
19604
11.59
28.78
4.97
7.25
13585
7.80
20.10
6.24
7.38
15255
8.83
27.31
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
92
-------
Table
Back Bay of Biloxi - Station BBB4
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O.
(ft) (mg/1)
pH CONDUCTIVITY SALINITY TEMPERATURE
(lis/cm) (ppt) (°C)
9/29/2005 1250 1
7.62
7.24
7429
4.07
29.17
2
7.18
7.19
7447
4.08
28.94
3
7.04
7.16
7494
4.11
28.92
4
6.79
7.11
7512
4.12
28.83
5
5.82
7.03
7825
4.32
28.49
6
5.61
7.00
7889
4.35
28.48
7
5.53
6.99
7937
4.37
28.46
8
5.46
6.98
7962
4.38
28.45
9
5.30
6.96
8054
4.45
28.46
10
3.95
6.81
11839
6.75
28.68
MAX
7.62
7.24
11839
6.75
29.17
MIN
3.95
6.81
7429
4.07
28.45
AVG
6.03
7.05
8139
4.50
28.69
Instantaneous minimum dissolved oxygen concentration less than 4.0 m
93
-------
Table
Back Bay of Biloxi - Station BBB5
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/29/2005 1130 1
7.33
7.16
7535
4.13
29.00
2
6.46
7.08
7652
4.20
28.51
3
5.98
7.01
8093
4.43
28.41
4
5.61
6.95
8647
4.81
28.36
5
5.44
6.94
8964
5.01
28.37
6
5.31
6.91
9482
5.30
28.36
7
4.95
6.87
10936
6.18
28.48
8
4.30
6.84
13967
8.37
28.81
9
3.75
6.86
15217
8.83
28.93
MAX
7.33
7.16
15217
8.83
29.00
MIN
3.75
6.84
7535
4.13
28.36
AVG
5.46
6.96
10055
5.70
28.58
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
Table
Back Bay of Biloxi -
Station BBB6
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
D.O.
PH
CONDUCTIVITY SALINITY
TEMPERAT
(ft)
(mg/l)
([JS/cm)
(PPt)
(°C)
9/29/2005
1000
1
7.58
7.52
4565
2.43
28.77
3
6.11
7.30
4664
2.46
28.49
5
4.06
7.08
5392
2.87
28.76
7
2.63
6.90
5927
3.20
28.90
9
2.23
6.84
6515
3.53
28.88
11
1.98
6.77
7096
3.87
28.83
13
1.41
6.74
7512
4.11
28.74
15
0.54
6.67
7830
4.58
28.51
MAX
7.58
7.52
7830
4.58
28.90
MIN
0.54
6.67
4565
2.43
28.49
AVG
3.32
6.98
6188
3.38
28.74
Instantaneous minimum dissolved oxygen concentration less than 4.0 mg/l
94
-------
Table
Bayou Lacroix - Station BLC1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 945
MAX
MIN
AVG
SURF
5.03
7.02
9190
5.12
28.29
1
4.52
6.93
9195
5.12
28.24
2
4.41
6.90
9930
5.22
28.27
3
4.07
6.88
9568
5.36
28.38
4
3.84
6.91
10416
5.85
28.54
5
3.83
6.88
11466
6.50
28.75
6
3.78
6.91
12567
7.15
28.83
7
3.73
6.92
12456
7.41
28.83
8
3.64
6.93
13265
7.60
28.81
9
3.56
6.93
13457
7.72
28.81
5.03
7.02
13457
7.72
28.83
3.56
6.88
9190
5.12
28.24
4.04
6.92
11151
6.31
28.58
Instantaneous minimum dissolved oxygen concentration less than 4.0 ms
95
-------
St. Louis Bay, Bayou Caddy, & Pearl River
Table
Bayou Caddy - Station BCD1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 -0945 1
6.15
7.35
23684
14.27
28.83
2
6.18
7.34
23689
14.27
28.84
3
6.16
7.35
23691
14.27
28.84
4
6.15
7.36
23688
14.27
28.84
5
6.16
7.35
23693
14.27
28.84
6
6.16
7.35
23682
14.27
28.84
7
6.16
7.36
23684
14.27
28.85
8
6.17
7.36
23679
14.27
28.86
9
6.15
7.36
23672
14.26
28.86
MAX
6.18
7.36
23693
14.27
28.86
MIN
6.15
7.34
23672
14.26
28.83
AVG
6.16
7.35
23685
14.27
28.84
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
96
-------
Table
Jordan River - Station JR1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1045
MAX
MIN
AVG
SURF
6.93
7.44
14454
8.35
27.64
1
6.70
7.43
14564
8.40
27.67
2
6.80
7.44
15138
8.77
27.65
3
6.81
7.46
15332
8.91
27.77
4
6.84
7.49
15540
7.49
27.86
5
6.83
7.49
15728
9.15
27.81
6
6.69
7.47
15892
9.25
27.72
7
6.66
7.47
15954
9.28
27.66
8
6.59
7.46
15931
9.28
27.65
9
6.55
7.46
15932
9.28
27.65
6.93
7.49
15954
9.28
27.86
6.55
7.43
14454
7.49
27.64
6.74
7.46
15447
8.82
27.71
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
97
-------
Table
St. Louis Bay - Station SLB1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1225
MAX
MIN
AVG
SURF
7.73
7.95
25194
15.27
29.05
1
7.74
7.95
25199
15.27
29.06
2
7.74
7.95
25211
15.29
28.94
3
7.40
7.87
25117
15.23
28.31
4
7.19
7.84
25118
15.23
28.30
5
7.10
7.82
25127
15.24
28.22
6
6.96
7.80
25136
15.24
28.18
7
6.90
7.78
25112
15.23
28.01
8
6.78
7.75
25098
15.22
27.92
9
6.57
7.71
25082
15.21
27.86
10
6.47
7.70
25080
15.21
27.85
11
6.47
7.70
25080
15.21
27.85
7.74
7.95
25211
15.29
29.06
6.47
7.70
25080
15.21
27.85
7.09
7.82
25130
15.24
28.30
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
98
-------
Table
St. Louis Bay - Station SLB2
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
DO.
pH
CONDUCTIVITY SALINITY TEMPERAT
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
9/30/2005
-1400
SURF
8.90
7.87
22931
13.77
29.03
1
8.58
7.88
22949
13.78
29.03
2
8.43
7.88
22953
13.78
29.06
3
8.40
7.87
22994
13.82
28.98
4
8.32
7.86
23034
13.82
28.99
5
6.79
7.57
24234
14.64
28.01
BOTTOM
6.77
7.55
24240
14.65
27.98
MAX
8.90
7.88
24240
14.65
29.06
MIN
6.77
7.55
22931
13.77
27.98
AVG
8.03
7.78
23334
14.04
28.73
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
99
-------
Table
St. Louis Bay - Station SLB3
Water Quality Study of Bays in Coastal Mississippi
DATE
TIME
DEPTH
D.O.
pH
CONDUCTIVITY SALINITY TEMPERAT
(ft)
(mg/1)
(|is/cm)
(PPt)
(°C)
9/30/2005
-1125
SURF
8.68
7.90
22115
13.25
28.62
1
8.18
7.89
22562
13.58
28.42
2
7.87
7.85
23442
14.05
28.43
3
7.77
7.83
23709
14.30
28.49
4
7.57
7.80
23785
14.34
28.48
5
7.23
7.75
23853
14.39
28.44
6
7.13
7.74
23898
14.42
28.35
7
6.98
7.72
24035
14.51
28.35
BOTTOM
6.94
7.72
24038
14.51
28.35
MAX
8.68
7.9
24038
14.51
28.62
MIN
6.94
7.72
22115
13.25
28.35
AVG
7.59
7.80
23493
14.15
28.44
Instantaneous minimum dissolved oxygen concentration less than 4.0 m
Table
St. Louis Bay - Station SLB4
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1315
MAX
MIN
AVG
1
8.32
7.69
20978
12.50
28.68
2
7.97
7.67
21019
12.55
28.62
3
7.05
7.52
21407
12.77
28.48
4
5.51
7.33
21814
13.07
28.09
8.32
7.69
21814
13.07
28.68
5.51
7.33
20978
12.50
28.09
7.21
7.55
21305
12.72
28.47
Instantaneous minimum dissolved oxygen concentration less than 4.0 ms
100
-------
Table
St. Louis Bay - Station SLB5
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1230
MAX
MIN
AVG
1
7.98
7.86
20344
12.09
28.80
2
7.94
7.86
20297
12.06
28.61
3
7.86
7.84
20243
12.02
28.60
4
7.58
7.81
20326
12.10
27.95
5
7.28
7.75
20593
12.26
27.88
7.98
7.86
20593
12.26
28.80
7.28
7.75
20243
12.02
27.88
7.73
7.82
20361
12.11
28.37
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
Table
St. Louis Bay - Station SLB6
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005
-0940 SURF
6.56
7.61
19505
11.55
28.00
1
6.54
7.62
19519
11.56
27.99
2
6.55
7.63
19511
11.56
27.98
3
6.50
7.62
19532
11.57
27.97
4
6.39
7.59
19596
11.63
27.98
5
6.11
7.50
19978
11.88
27.99
6
4.79
7.32
21082
12.59
28.19
BOTTOM
3.86
7.20
21482
12.83
28.24
MAX
6.56
7.63
21482
12.83
28.24
MIN
3.86
7.20
19505
11.55
27.97
AVG
5.91
7.51
20026
11.90
28.04
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
101
-------
Table
St. Louis Bay - Station SLB7
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITYTEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1125
MAX
MIN
AVG
SURF
7.69
7.86
17914
10.53
28.45
1
7.71
7.86
17924
10.54
28.42
2
7.66
7.85
17928
10.55
28.12
3
7.39
7.78
18169
10.68
27.83
4
7.20
7.74
18629
11.01
27.81
5
6.38
7.58
18860
11.15
27.76
7.71
7.86
18860
11.15
28.45
6.38
7.58
17914
10.53
27.76
7.34
7.78
18237
10.74
28.07
Instantaneous minimum dissolved oxygen concentration less than 4.0 r
Table
Wolf River - Station WR1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1435
MAX
MIN
AVG
1
7.65
7.14
12172
7.06
29.58
2
7.75
7.11
12875
7.41
29.70
3
7.36
7.08
14160
8.63
29.26
4
7.21
7.12
15848
9.02
29.07
7.49
7.11
13764
8.03
29.40
7.21
7.08
12172
7.06
29.07
7.49
7.11
13764
8.03
29.40
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
102
-------
Table
Pearl River - Station Pearl 1
Water Quality Study of Bays in Coastal Mississippi
DATE TIME DEPTH D.O. pH CONDUCTIVITY SALINITY TEMPERATURE
(ft) (mg/1) (|is/cm) (ppt) (°C)
9/30/2005 1545
MAX
MIN
AVG
SURF
7.01
6.96
4096
2.15
30.32
1
6.91
6.95
4118
2.17
30.27
3
6.40
6.91
4265
2.22
30.15
5
5.95
6.79
5108
2.70
29.16
7
2.45
6.56
6715
3.65
29.01
9
2.26
6.57
6809
3.74
29.04
11
2.14
6.57
7445
4.07
29.14
13
2.00
6.57
7680
4.21
29.17
15
1.95
6.57
7739
4.25
29.18
17
1.88
6.57
7759
4.26
29.18
7.01
6.96
7759
4.26
30.32
1.88
6.56
4096
2.15
29.01
3.90
6.70
6173
3.34
29.46
Instantaneous minimum dissolved oxygen concentration less than 4.0 n
103
-------
Appendix E
Minimum Quantitation Limits and National
Ambient Water Quality Criteria
104
-------
Minimum Quantitation Limits and National Ambient Water Quality Criteria
Endosulfan II (beta)
Endosulfan Sulfate
Endrin
Endrin Ketone
gamma-BHC (Lindane)
gamma-Chlordane /2
Heptachlor
Heptachlor Epoxide
Methoxychlor
Toxaphene
trans-Nonachlor /2
Volatiles Scan
(m- and/or p-)Xylene
1,1,1,2-Tetrachloroethane
1.1.1-Trichloroethane
1,1,2,2-Tetrachloroethane
1.1.2-Trichloro-1,2,2-Trifluoroethane
1.1.2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1.1-Dichloropropene
1.2.3-Trichlorobenzene
1.2.3-Trichloropropane
1.2.4-Trichlorobenzene
1.2.4-Trimethylbenzene
1.2-Dibromo-3-Chloropropane (DBCP)
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1.2-Dichloropropane
1.3.5-Trimethylbenzene
1.3-Dichlorobenzene
1.3-Dichloropropane
1.4-Dichlorobenzene
2,2-Dichloropropane
Acetone
Benzene
Bromobenzene
Bromochloromethane
Bromodichloromethane
Bromoform
Bromomethane
Carbon Disulfide
ASB
Method MQL
Analytical MQL
MQL Range
Min Max
2002 NAWQC
CMC CCC
(acute) (Chronic)
33213-65-9
1031-07-8
72-20-8
53494-70-5
58-89-9
5566-34-7
76-44-8
1024-57-3
72-43-5
8001-35-2
39765-80-5
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
UG/L
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
1
20
0.5
0.24
0.24
0.24
0.24
0.097
0.097
0.097
0.097
0.48
9.7
0.097
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.5
0.52
10
0.5
0.034
0.037
0.16
0.053
0.053
0.21
0.0087
0.0023
0.0036
0.0036
0.0002
UG/L
630-20-6 UG/L 1
71-55-6 UG/L 1
79-34-5 UG/L 1
76-13-1 UG/L 1
79-00-5 UG/L 1
75-34-3 UG/L 1
75-35-4 UG/L 1
563-58-6 UG/L 1
87-61-6 UG/L 1
96-18-4 UG/L 1
120-82-1 UG/L 1
95-63-6 UG/L 1
96-12-8 UG/L 1
106-93-4 UG/L 1
95-50-1 UG/L 1
107-06-2 UG/L 1
78-87-5 UG/L 1
108-67-8 UG/L 1
541-73-1 UG/L 1
142-28-9 UG/L 1
106-46-7 UG/L 1
590-20-7 UG/L 1
67-64-1 UG/L 25
71-43-2 UG/L 1
108-86-1 UG/L 1
74-97-5 UG/L 1
75-27-4 UG/L 1
75-25-2 UG/L 1
74-83-9 UG/L 1
75-15-0 UG/L 2.5
0.068 2
0.11
0.11
0.074
105
-------
Minimum Quantitation Limits and National Ambient Water Quality Criteria
ASB Analytical MQL 2002 NAWQC
Method MQL MQL Range CMC CCC
Min Max (acute) (Chronic)
cis-1,2-Dichloroethene
156-59-2
UG/L
1
1 1
cis-1,3-Dichloropropene
10061-01-5
UG/L
1
1 1
Cyclohexane
110-82-7
UG/L
1
1 1
Dibromochloromethane
124-48-1
UG/L
1
1 1
Dibromomethane
74-95-3
UG/L
1
1 1
Dichlorodifluoromethane
75-71-8
UG/L
1
1 1
Ethyl Benzene
100-41-4
UG/L
1
0.1 1
Hexachloro-1,3-Butadiene
87-68-3
UG/L
1
1 1
Isopropylbenzene
98-82-8
UG/L
1
1 1
Methyl Acetate
79-20-9
UG/L
5
1 1
Methyl Butyl Ketone
591-78-6
UG/L
2.5
Methyl Ethyl Ketone
78-93-3
UG/L
12
Methyl Isobutyl Ketone
108-10-1
UG/L
2.2
1 1
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/L
1
1 1
Methylcyclohexane
108-87-2
UG/L
1
1 1
Methylene Chloride
75-09-2
UG/L
1
1 1
n-Butylbenzene
104-51-8
UG/L
1
1 1
n-Propylbenzene
103-65-1
UG/L
1
1 1
o-Chlorotoluene
95-49-8
UG/L
1
1 1
o-Xylene
95-47-6
UG/L
2
0.12 1
p-Chlorotoluene
106-43-4
UG/L
1
1 1
p-lsopropyltoluene
99-87-6
UG/L
1
1 1
sec-Butylbenzene
135-98-8
UG/L
1
1 1
Styrene
100-42-5
UG/L
1
1 1
tert-Butylbenzene
98-06-6
UG/L
1
1 1
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/L
1
1 1
Toluene
108-88-3
UG/L
1
0.057 1
trans-1,2-Dichloroethene
156-60-5
UG/L
1
1 1
trans-1,3-Dichloropropene
10061-02-6
UG/L
1
1 1
Trichloroethene (Trichloroethylene)
79-01-6
UG/L
1
1 1
Trichlorofluoromethane (Freon11)
75-69-4
UG/L
1
1 1
Vinyl Chloride
75-01-4
UG/L
1
1 1
Extractables Scan
(3-and/or 4-)Methylphenol
UG/L
10
9.5 11
1,1-Biphenyl
92-52-4
UG/L
10
9.5 11
1,2,4-Trichlorobenzene
120-82-1
UG/L
10
9.5 11
2,3,4,6-Tetrachlorophenol
58-90-2
UG/L
10
9.5 11
2,4,5-Trichlorophenol
95-95-4
UG/L
10
9.5 11
2,4,6-Trichlorophenol
88-06-2
UG/L
10
9.5 11
2,4-Dichlorophenol
120-83-2
UG/L
10
9.5 11
2,4-Dimethylphenol
105-67-9
UG/L
10
9.5 11
2,4-Dinitrophenol
51-28-5
UG/L
20
19 23
2,4-Dinitrotoluene
121-14-2
UG/L
10
9.5 11
106
-------
Minimum Quantitation Limits and National Ambient Water Quality Criteria
ASB Analytical MQL 2002 NAWQC
Method MQL MQL Range CMC CCC
Min Max (acute) (Chronic)
2-Methyl phenol
95-48-7
UG/L
10
9.5 11
2-Nitroaniline
88-74-4
UG/L
10
9.5 11
2-Nitrophenol
88-75-5
UG/L
10
9.5 11
3,3'-Dichloro benzidine
91-94-1
UG/L
10
9.5 11
3-Nitroaniline
99-09-2
UG/L
10
9.5 11
4-Bromophenyl Phenyl Ether
101-55-3
UG/L
10
9.5 11
4-Chloro-3-Methyl phenol
59-50-7
UG/L
10
9.5 11
4-Chloroaniline
106-47-8
UG/L
10
9.5 11
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/L
10
9.5 11
4-Nitroaniline
100-01-6
UG/L
10
9.5 11
4-Nitrophenol
100-02-7
UG/L
20
9.5 23
Acenaphthene
83-32-9
UG/L
10
9.5 11
Acenaphthylene
208-96-8
UG/L
10
9.5 11
Acetophenone
98-86-2
UG/L
10
9.5 11
Anthracene
120-12-7
UG/L
10
9.5 11
Atrazine
1912-24-9
UG/L
10
9.5 11
Benzaldehyde
100-52-7
UG/L
10
9.5 11
Benzo(a)Anthracene
56-55-3
UG/L
10
9.5 11
Benzo(b)Fluoranthene
205-99-2
UG/L
10
9.5 11
Benzo(ghi)Perylene
191-24-2
UG/L
10
9.5 11
Benzo(k)Fluoranthene
207-08-9
UG/L
10
9.5 11
Benzo-a-Pyrene
50-32-8
UG/L
10
9.5 11
Benzyl Butyl Phthalate
85-68-7
UG/L
10
9.5 11
bis(2-Chloroethoxy)Methane
111-91-1
UG/L
10
9.5 11
bis(2-Chloroethyl) Ether
111-44-4
UG/L
10
9.5 11
bis(2-Chloroisopropyl) Ether
108-60-1
UG/L
10
9.5 11
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/L
10
9.5 11
Caprolactam
105-60-2
UG/L
10
9.5 11
Carbazole
86-74-8
UG/L
10
9.5 11
Chrysene
218-01-9
UG/L
10
9.5 11
Dibenzo(a,h)Anthracene
53-70-3
UG/L
10
9.5 11
Dibenzofuran
132-64-9
UG/L
10
9.5 11
Diethyl Phthalate
84-66-2
UG/L
10
9.5 11
Dimethyl Phthalate
131-11-3
UG/L
10
9.5 11
Di-n-Butylphthalate
84-74-2
UG/L
10
9.5 11
Di- n-Octyl phtha late
117-84-0
UG/L
10
9.5 11
Fluoranthene
206-44-0
UG/L
10
9.5 11
Fluorene
86-73-7
UG/L
10
9.5 11
Hexachlorobenzene (HCB)
118-74-1
UG/L
10
9.5 11
Hexachlorobutadiene
87-68-3
UG/L
10
9.5 11
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/L
10
9.5 11
Hexachloroethane
67-72-1
UG/L
10
9.5 11
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/L
10
9.5 11
Isophorone
78-59-1
UG/L
10
9.5 11
107
-------
Minimum Quantitation Limits and National Ambient Water Quality Criteria
ASB Analytical MQL 2002 NAWQC
Method MQL MQL Range CMC CCC
Min Max (acute) (Chronic)
Phenanthrene
85-01-8 UG/L
10
9.5
11
Phenol
108-95-2 UG/L
10
9.5
11
Pyrene
129-00-0 UG/L
10
9.5
11
Classical Nutrients
Ammonia
7664-41-7
MG/L
0.05
0.05
Nitrate-Nitrite Nitrogen
MG/L
0.05
0.05
Total Kjeldahl Nitrogen
MG/L
0.05
Total Organic Carbon
MG/L
1
Total Phosphorus
7723-14-0
MG/L
0.01
CMC - Criteria Maximum Concentration,
CCC - Criterion Continuous Concentration
108
-------
Appendix F
Sediment Minimum Quantitation Limits
109
-------
Sediment MQLs
Metals Scan
ASB
Method
MQL
Analytical MQL
Min Max
TEL
PEL
Aluminum
7429-90-5
MG/KG
50
180
8200
Antimony
7440-36-0
MG/KG
2
0.25
0.5
Arsenic
7440-38-2
MG/KG
1
0.25
7.24
41.6
Barium
7440-39-3
MG/KG
1
1
Beryllium
7440-41-7
MG/KG
0.5
0.3
Cadmium
7440-43-9
MG/KG
0.5
0.12
0.25
0.68
4.2
Calcium
7440-70-2
MG/KG
50
Chromium
7440-47-3
MG/KG
1
0.5
52.3
160.4
Cobalt
7440-48-4
MG/KG
1
0.5
Copper
7440-50-8
MG/KG
1
2
18.7
108.2
Iron
7439-89-6
MG/KG
25
Lead
7439-92-1
MG/KG
0.5
30.2
112.2
Magnesium
7439-95-4
MG/KG
25
Manganese
7439-96-5
MG/KG
1
Molybdenum
7439-98-7
MG/KG
1
0.5
5.2
Nickel
7440-02-0
MG/KG
2
0.99
4
15.9
42.8
Potassium
7440-09-7
MG/KG
200
99
100
Selenium
7782-49-2
MG/KG
4
0.5
1
Silver
7440-22-4
MG/KG
1
0.5
0.5
0.7
1.7
Sodium
7440-23-5
MG/KG
200
Strontium
7440-24-6
MG/KG
1
Thallium
7440-28-0
MG/KG
0.5
0.25
0.5
Tin
7440-31-5
MG/KG
2.5
0
0
Titanium
7440-32-6
MG/KG
1
2.6
22
Total Mercury
7439-97-6
MG/KG
0.05
0.042
0.049
0.13
0.7
Vanadium
7440-62-2
MG/KG
1
2
Yttrium
7440-65-5
MG/KG
1
0.3
14
Zinc
7440-66-6
MG/KG
1
124
271
PCB Scan
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100
100
100
21.6
188.8
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100
100
100
21.6
188.8
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100
100
100
21.6
188.8
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100
100
100
21.6
188.8
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100
100
100
21.6
188.8
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100
100
100
21.6
188.8
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100
100
100
21.6
188.8
Pesticides Scan
4,4'-DDD (p,p'-DDD)
72-54-8
UG/KG
20
9.9
28
1.2
7.8
4,4'-DDE (p,p'-DDE)
72-55-9
UG/KG
20
4
11
2.1
374.2
4,4'-DDT (p,p'-DDT)
50-29-3
UG/KG
20
9.9
41
1.2
4.8
Aldrin
309-00-2
UG/KG
20
4
15
alpha-BHC
319-84-6
UG/KG
20
4
11
alpha-Chlordane 12
5103-71-9
UG/KG
20
4
11
2.3
4.8
beta-BHC
319-85-7
UG/KG
20
4
28
Chlordene 12
3734-48-3
UG/KG
20
4
11
cis-Nonachlor 12
5103-73-1
UG/KG
20
4
11
delta-BHC
319-86-8
UG/KG
20
4.1
20
Dieldrin
60-57-1
UG/KG
20
4
12
0.7
4.3
Endosulfan 1 (alpha)
959-98-8
UG/KG
20
4
18
Endosulfan II (beta)
33213-65-9
UG/KG
20
9.9
28
Endosulfan Sulfate
1031-07-8
UG/KG
20
9.9
28
110
-------
Sediment MQLs
Metals Scan
ASB
Method
MQL
Analytical MQL
Min Max
Heptachlor
76-44-8
UG/KG
20
4
22
Heptachlor Epoxide
1024-57-3
UG/KG
20
4
13
Methoxychlor
72-43-5
UG/KG
50
20
55
Toxaphene
8001-35-2
UG/KG
20
400
1110
trans-Nonachlor /2
39765-80-5
UG/KG
20
4
11
Volatiles Scan
(m- and/or p-)Xylene
UG/KG
2
2.4
14
1,1,1,2-Tetrachloroethane
630-20-6
UG/KG
1
1.2
6.8
1,1,1-Trichloroethane
71-55-6
UG/KG
1
1.2
6.8
1,1,2,2-Tetrachloroethane
79-34-5
UG/KG
1
1.2
6.8
1,1,2-Trichloro-1,2,2-Trifluoroethane
76-13-1
UG/KG
1
1.2
6.8
1,1,2-Trichloroethane
79-00-5
UG/KG
1
1.2
6.8
1,1-Dichloroethane
75-34-3
UG/KG
1
1.2
6.8
1,1-Dichloroethene
75-35-4
UG/KG
1
1.2
6.8
1,1-Dichloropropene
563-58-6
UG/KG
1
1.2
6.8
1,2,3-Trichloro benzene
87-61-6
UG/KG
1
1.8
14
1,2,3-Trichloropropane
96-18-4
UG/KG
1
2.4
14
1,2,4-Trichloro benzene
120-82-1
UG/KG
1
2.4
14
1,2,4-Trimethylbenzene
95-63-6
UG/KG
1
1.2
6.8
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
1
5.9
34
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
1
1.2
6.8
1,2-Dichlorobenzene
95-50-1
UG/KG
1
1.2
6.8
1,2-Dichloroethane
107-06-2
UG/KG
1
1.2
6.8
1,2-Dichloropropane
78-87-5
UG/KG
1
1.2
6.8
1,3,5-Trimethylbenzene
108-67-8
UG/KG
1
0.25
6.8
1,3-Dichlorobenzene
541-73-1
UG/KG
1
2.4
14
1,3-Dichloropropane
142-28-9
UG/KG
1
1.2
6.8
1,4-Dichlorobenzene
106-46-7
UG/KG
1
2.4
14
2,2-Dichloropropane
590-20-7
UG/KG
1
1.2
6.8
Acetone
67-64-1
UG/KG
1
12
70
Benzene
71-43-2
UG/KG
1
1.2
6.8
Bromobenzene
108-86-1
UG/KG
1
1.2
6.8
Bromochloromethane
74-97-5
UG/KG
1
1.2
6.8
Bromodichloromethane
75-27-4
UG/KG
1
1.2
6.8
Bromoform
75-25-2
UG/KG
1
5.9
34
Bromomethane
74-83-9
UG/KG
1
1.2
6.8
Carbon Disulfide
75-15-0
UG/KG
2.5
1.2
6.8
Carbon Tetrachloride
56-23-5
UG/KG
1
1.2
6.8
Chlorobenzene
108-90-7
UG/KG
1
1.2
6.8
Chloroethane
75-00-3
UG/KG
1
1.2
6.8
Chloroform
67-66-3
UG/KG
1
1.2
6.8
Chloromethane
74-87-3
UG/KG
1
1.2
6.8
cis-1,2-Dichloroethene
156-59-2
UG/KG
1
1.2
6.8
cis-1,3-Dichloropropene
10061-01-5
UG/KG
1
1.2
6.8
Cyclohexane
110-82-7
UG/KG
1
1.2
6.8
Dibromochloromethane
124-48-1
UG/KG
1
1.2
6.8
Dibromomethane
74-95-3
UG/KG
1
1.2
6.8
Dichlorodifluoromethane
75-71-8
UG/KG
1
1.2
6.8
Ethyl Benzene
100-41-4
UG/KG
1
1.2
6.8
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
1
1.2
6.8
Isopropylbenzene
98-82-8
UG/KG
1
1.2
14
Methyl Acetate
79-20-9
UG/KG
1
1.2
6.8
111
-------
Sediment MQLs
Metals Scan
ASB
Method
MQL
Analytical MQL
Min Max
Methylcyclohexane
108-87-2
UG/KG
1
1.2
6.8
Methylene Chloride
75-09-2
UG/KG
1
1.2
6.8
n-Butylbenzene
104-51-8
UG/KG
1
2.4
14
n-Propylbenzene
103-65-1
UG/KG
1
1.2
6.8
o-Chlorotoluene
95-49-8
UG/KG
1
1.2
6.8
o-Xylene
95-47-6
UG/KG
1
0.21
6.8
p-Chlorotoluene
106-43-4
UG/KG
1
2.4
14
p-lsopropyltoluene
99-87-6
UG/KG
1
1.2
43
sec-Butylbenzene
135-98-8
UG/KG
1
1.2
6.8
Styrene
100-42-5
UG/KG
1
1.2
6.8
tert-Butylbenzene
98-06-6
UG/KG
1
1.2
6.8
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/KG
1
1.2
6.8
Toluene
108-88-3
UG/KG
1
1.2
6.8
trans-1,2-Dichloroethene
156-60-5
UG/KG
1
5.9
34
trans-1,3-Dichloropropene
10061-02-6
UG/KG
1
1.2
6.8
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
1
1.2
6.8
Trichlorofluoromethane (Freon 11)
75-69-4
UG/KG
1
1.2
6.8
Vinyl Chloride
75-01-4
UG/KG
1
1.2
6.8
Extractables Scan
(3-and/or 4-)Methylphenol
UG/KG
330
400
1100
1,1 -Biphenyl
92-52-4
UG/KG
330
400
1100
1,2,4-Trichlorobenzene
120-82-1
UG/KG
330
400
1100
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
330
400
1100
2,4,5-Trichlorophenol
95-95-4
UG/KG
330
400
1100
2,4,6-Trichlorophenol
88-06-2
UG/KG
330
400
1100
2,4-Dichlorophenol
120-83-2
UG/KG
330
400
1100
2,4-Dimethylphenol
105-67-9
UG/KG
330
400
1100
2,4-Dinitrophenol
51-28-5
UG/KG
670
790
2200
2,4-Dinitrotoluene
121-14-2
UG/KG
330
400
1100
2,6-Dinitrotoluene
606-20-2
UG/KG
330
400
1100
2-Chloronaphthalene
91-58-7
UG/KG
330
400
1100
2-Chlorophenol
95-57-8
UG/KG
330
400
1100
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
670
790
2200
2-Methylnaphthalene
91-57-6
UG/KG
330
400
1100
2-Methylphenol
95-48-7
UG/KG
330
400
1100
2-Nitroaniline
88-74-4
UG/KG
330
400
1100
2-Nitrophenol
88-75-5
UG/KG
330
400
1100
3,3'-Dichlorobenzidine
91-94-1
UG/KG
330
400
1100
3-Nitroaniline
99-09-2
UG/KG
330
400
1100
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
330
400
1100
4-Chloro-3-Methylphenol
59-50-7
UG/KG
330
400
1100
4-Chloroaniline
106-47-8
UG/KG
330
400
1100
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
330
400
1100
4-Nitroaniline
100-01-6
UG/KG
330
400
1100
4-Nitrophenol
100-02-7
UG/KG
670
790
2200
Acenaphthene
83-32-9
UG/KG
330
400
1100
Acenaphthylene
208-96-8
UG/KG
330
400
1100
Acetophenone
98-86-2
UG/KG
330
400
1100
Anthracene
120-12-7
UG/KG
330
400
1100
Atrazine
1912-24-9
UG/KG
330
400
1100
Benzaldehyde
100-52-7
UG/KG
330
400
1100
Benzo(a)Anthracene
56-55-3
UG/KG
330
400
1100
112
-------
Sediment MQLs
Metals Scan
ASB
Method
MQL
Analytical MQL
Min Max
TEL
PEL
Benzyl Butyl Phthalate
85-68-7
UG/KG
330
400
1100
bis(2-Chloroethoxy)Methane
111-91-1
UG/KG
330
400
1100
bis(2-Chloroethyl) Ether
111-44-4
UG/KG
330
400
1100
bis(2-Chloroisopropyl) Ether
108-60-1
UG/KG
330
400
1100
bis(2-Ethylhexyl) Phthalate
117-81-7
UG/KG
330
400
1100
Caprolactam
105-60-2
UG/KG
330
400
1100
Carbazole
86-74-8
UG/KG
330
400
1100
Chrysene
218-01-9
UG/KG
330
400
1100
107.8
846
Dibenzo(a,h)Anthracene
53-70-3
UG/KG
330
400
1100
6.2
134.6
Dibenzofuran
132-64-9
UG/KG
330
400
1100
Diethyl Phthalate
84-66-2
UG/KG
330
400
1100
Dimethyl Phthalate
131-11-3
UG/KG
330
400
1100
Di-n-Butylphthalate
84-74-2
UG/KG
330
400
1100
Di-n-Octylphthalate
117-84-0
UG/KG
330
400
1100
Fluoranthene
206-44-0
UG/KG
330
400
1100
112.8
1493.5
Fluorene
86-73-7
UG/KG
330
400
1100
21.2
144.4
Hexachlorobenzene (HCB)
118-74-1
UG/KG
330
400
1100
Hexachlorobutadiene
87-68-3
UG/KG
330
400
1100
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/KG
330
400
1100
Hexachloroethane
67-72-1
UG/KG
330
400
1100
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
330
400
1100
Isophorone
78-59-1
UG/KG
330
400
1100
Naphthalene
91-20-3
UG/KG
330
400
1100
34.6
390.6
Nitrobenzene
98-95-3
UG/KG
330
400
1100
n-Nitroso di-n-Propylamine
621-64-7
UG/KG
330
400
1100
n-Nitrosodiphenylamine/Diphenylamine
122-39-4
UG/KG
330
400
1100
Pentachlorophenol
87-86-5
UG/KG
670
790
2200
Phenanthrene
85-01-8
UG/KG
330
400
1100
86.7
543.5
Phenol
108-95-2
UG/KG
330
400
1100
Pyrene
129-00-0
UG/KG
330
400
1100
152.7
1397.6
Classical Nutrients
Ammonia
7664-41 -7
MG/KG
2.5
3
91
Nitrate-Nitrite Nitrogen
MG/KG
12.5
1.2
6.4
Total Kjeldahl Nitrogen
MG/KG
12.5
Total Organic Carbon
MG/KG
8600
39000
Total Phosphorus
7723-14-0
MG/KG
25
26
TEL - Threshold Effects Level
PEL - Probable Effects Level
113
-------
Appendix G
Quality Assurance/Quality
Control Results
114
-------
Quality Control Sample Results
Metals Scan
QCDI1 QCPB1SW QCPB2SW QCRB1WSW QCRB2WSW QCTB2WSW QCTB3WSW QCTB4SW QCTRIPBLK
Deionized H20 Preservative Preservative Equipment Rinse Equipment Rinse Trip Trip Trip Trip
Blank Blank Blank Blank Blank Blank Blank Blank Blank
9/28/2005 9/30/2005 9/30/2005 9/28/2005 9/29/2005 9/28/2005 9/29/2005 9/30/2005 9/27/2005
1849 1730 1845 1841 1600 1805 1450 1645
7440-66-6 UG/L
U
18
24
PCB Scan
Pesticides Scan
None Detected
None Detected
Volatiles Scan
Toluene 108-88-3 UG/L
Extractables Scan
None Detected
Classical Nutrients
Total Organic Carbon MG/L
Data Qualifiers
U-Analyte not detected at or above reporting limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites of technical chlordane
NR-Not Reported
115
-------
Table 19
Quality Control/Quality Assurance Duplicate Sample Results
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Results of Duplicate Sampling
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
BBB3DSD
BBB3SD
BC4DSD
BC4SD
ER1DSD
ER1SD
SLB6DSD
SLB6SD
9/29/2005
9/29/2005
9/27/2005
9/27/2005
9/28/2005
9/28/2005
9/30/2005
9/30/2005
Metals Scan
1005
945
1300
1240
1430
1400
1100
1040
% Moisture
%
69
66
41
49 A
23
20
56
57
Aluminum
7429-90-5
MG/KG
7000
7800
2600
3000
180 A
210
6600
6100
Antimony
7440-36-0
MG/KG
0.25 U
0.25 U
0.5 U
0.5 U
0.25 U
0.25 U
0.25 U
0.25 U
Arsenic
7440-38-2
MG/KG
5.2
5.5
1.2
0.87
0.25 U
0.25 U
8.9
9
Barium
7440-39-3
MG/KG
14
16
27
57
1.7 A
1
19
18
Beryllium
7440-41-7
MG/KG
0.99
1.1
0.3
0.3
0.3 U
0.3 U
0.77
0.72
Cadmium
7440-43-9
MG/KG
0.42
0.46
1.5
1.8
0.12 U
0.12 U
0.24
0.21
Calcium
7440-70-2
MG/KG
1400
1400
4900
4700
71 A
50
4400
1700
Chromium
7440-47-3
MG/KG
12
12
7.2
9.7
0.5 U
0.5 U
10
9.4
Cobalt
7440-48-4
MG/KG
5.9
6
0.59
0.66
0.5 U
0.5 U
7.7
7.5
Copper
7440-50-8
MG/KG
14 J
15 J
4.7
5.5
2 UJ
2 UJ
6.7
6.2
Iron
7439-89-6
MG/KG
14000 J
15000 J
3400
3200
270 A
370
16000
16000
Lead
7439-92-1
MG/KG
18
20
4.8
5.9
2.1 A
1.3
15
14
Magnesium
7439-95-4
MG/KG
3200
3200
1800
1700
200 A
120
3500
3300
Manganese
7439-96-5
MG/KG
140
140
26
26
1.7 A
2.5
260
240
Molybdenum
7439-98-7
MG/KG
0.5 U
0.61
1.6 U
1.6 U
5.2 U
5.2 U
0.5 U
0.5 U
Nickel
7440-02-0
MG/KG
5.9 J
6.2 J
2.4
2.7
0.99 U
1 U
8
7.6
Potassium
7440-09-7
MG/KG
1200
1300
510
450
99 U
100 U
1600
1500
Selenium
7782-49-2
MG/KG
1
1.2
1 U
1 U
0.5 U
0.5 U
0.5 U
0.5 U
Silver
7440-22-4
MG/KG
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
0.5 U
Sodium
7440-23-5
MG/KG
6800
6000
8500
5900
1300 A
540
5900
5900
Strontium
7440-24-6
MG/KG
27
28
59
66
1.5 A
1.1
37
22
Thallium
7440-28-0
MG/KG
0.25 U
0.25 U
0.5 U
0.5 U
0.25 U
0.25 U
0.25 U
0.25 U
Tin
7440-31-5
MG/KG
NA
NA
NA
NA
NA
NA
NA
NA
Titanium
7440-32-6
MG/KG
12
11
12
14
2.6 AJ
2.8 J
20 J
19 J
Total Mercury
7439-97-6
MG/KG
0.069
0.07 A
0.044 U
0.044 U
0.045 U
0.044 U
0.047 U
0.049 U
Vanadium
7440-62-2
MG/KG
16
17
6.1
7.3
2 UJ
2 UJ
19
18
Yttrium
7440-65-5
MG/KG
12
13
2.7
2.5
0.3 U
0.3 U
11
10
Zinc
7440-66-6
MG/KG
63
66
48
55
1.6 A
1.9
42
41
PCB Scan
% Moisture
%
70
68
30
34
21
20
36
58
PCB-1016 (Aroclor 1016)
12674-11-2
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1221 (Aroclor 1221)
11104-28-2
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1232 (Aroclor 1232)
11141-16-5
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1242 (Aroclor 1242)
53469-21-9
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1248 (Aroclor 1248)
12672-29-6
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1254 (Aroclor 1254)
11097-69-1
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
PCB-1260 (Aroclor 1260)
11096-82-5
UG/KG
100 UJ
100 UJ
100 U
100 U
100 U
100 U
100 UJ
100 UJ
Pesticides Scan
% Moisture
%
70
68
30
34
21
20
56
58
4,4'-DDD (p,p'-DDD)
72-54-8
UG/KG
28 U
26 UJ
14 U
15 U
10 U
10 U
18 U
19 U
4,4'-DDE (p,p'-DDE)
72-55-9
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
4,4'-DDT (p.p'-DDT)
50-29-3
UG/KG
40 U
37 UJ
14 U
15 U
10 U
10 U
18 U
19 U
Aldrin
309-00-2
UG/KG
15 U
14 UJ
5.7 U
6 U
4.1 U
4.1 U
9.3 U
9.7 U
alpha-BHC
319-84-6
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
alpha-Chlordane 12
5103-71-9
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
beta-BHC
319-85-7
UG/KG
11 U
26 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
Chlordene 12
3734-48-3
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
cis-Nonachlor 12
5103-73-1
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
delta-BHC
319-86-8
UG/KG
20 U
18 UJ
5.7 U
6 U
4.1 U
4.1 U
11 U
7.8 U
Dieldrin
60-57-1
UG/KG
12 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
Endosulfan 1 (alpha)
959-98-8
UG/KG
18 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
8.2 U
7.8 U
Endosulfan II (beta)
33213-65-9
UG/KG
28 U
26 UJ
14 U
15 U
10 U
10 U
18 U
19 U
Endosulfan Sulfate
1031-07-8
UG/KG
28 U
26 UJ
14 U
15 U
10 U
10 U
18 U
19 U
Endrin
72-20-8
UG/KG
28 U
26 UJ
14 U
15 U
10 U
10 U
18 U
19 U
Endrin Ketone
53494-70-5
UG/KG
28 U
26 UJ
18 U
19 U
10 U
10 U
18 U
25 U
gamma-BHC (Lindane)
58-89-9
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
gamma-Chlordane 12
5566-34-7
UG/KG
11 U
11 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
Heptachlor
76-44-8
UG/KG
22 U
11 UJ
6.8 U
6.8 U
4.1 U
4.1 U
7.2 U
7.8 U
Heptachlor Epoxide
1024-57-3
UG/KG
13 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
Methoxychlor
72-43-5
UG/KG
55 U
52 UJ
28 U
30 U
23 U
21 U
36 U
39 U
Toxaphene
8001-35-2
UG/KG
1110 U
1000 UJ
570 U
600 U
410 U
410 U
720 U
780 U
trans-Nonachlor 12
39765-80-5
UG/KG
11 U
10 UJ
5.7 U
6 U
4.1 U
4.1 U
7.2 U
7.8 U
Volatiles Scan
% Moisture
%
69
66
41
50
23
20
56
57
(m- and/or p-)Xylene
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
1,1,1,2-Tetrachloroethane
630-20-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1,1-Trichloroethane
71-55-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1,2,2-Tetrachloroethane
79-34-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1,2-Trichloro-1,2,2-Trifluoroethane (Freon 113)
76-13-1
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1,2-Trichloroethane
79-00-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1-Dichloroethane
75-34-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1-Dichloroethene (1,1-Dichloroethylene)
75-35-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,1-Dichloropropene
563-58-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,2,3-Trichlorobenzene
87-61-6
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
1,2,3-Trichloropropane
96-18-4
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
1,2,4-Trichlorobenzene
120-82-1
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
1,2,4-Trimethylbenzene
95-63-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
1,2-Dibromo-3-Chloropropane (DBCP)
96-12-8
UG/KG
34 U
22 U
11 U
16 U
5.9 U
6.3 U
16 U
17 U
1,2-Dibromoethane (EDB)
106-93-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
116
-------
Table 19
Quality Control/Quality Assurance Duplicate Sample Results
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Results of Duplicate Sampling
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
BBB3DSD
BBB3SD
BC4DSD
BC4SD
ER1DSD
ER1SD
SLB6DSD
SLB6SD
9/29/2005
9/29/2005
9/27/2005
9/27/2005
9/28/2005
9/28/2005
9/30/2005
9/30/2005
Metals Scan
1005
945
1300
1240
1430
1400
1100
1040
Bromochloromethane
74-97-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Bromodichloromethane
75-27-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Bromoform
75-25-2
UG/KG
34 U
22 U
11 U
16 U
5.9 U
6.3 U
16 U
17 U
Bromomethane
74-83-9
UG/KG
6.8 UJ
4.3 UJ
2.3 U
3.3 U
1.2 U
1.2 U
3.2 UJ
3.4 UJ
Carbon Disulfide
75-15-0
UG/KG
6.8 U
4.3 UJ
3.2
4.4
1.2 U
1.2 U
3.2 UJ
3.4 UJ
Carbon Tetrachloride
56-23-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Chlorobenzene
108-90-7
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Chloroethane
75-00-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Chloroform
67-66-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Chloromethane
74-87-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
cis-1,2-Dichloroethene
156-59-2
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
cis-1,3-Dichloropropene
10061-01-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Cyclohexane
110-82-7
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Dibromochloromethane
124-48-1
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Dibromomethane
74-95-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Dichlorodifluoromethane
75-71-8
UG/KG
6.8 UJ
4.3 UJ
2.3 U
3.3 U
1.2 U
1.2 U
3.2 UJ
3.4 UJ
Ethyl Benzene
100-41-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Hexachloro-1,3-Butadiene
87-68-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Isopropylbenzene
98-82-8
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Methyl Acetate
79-20-9
UG/KG
6.8 UJ
4.3 UJ
2.3 U
3.3 U
1.2 U
1.2 U
3.2 UJ
3.4 UJ
Methyl Butyl Ketone
591-78-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Methyl Ethyl Ketone
78-93-3
UG/KG
11 J
9.7 UJ
4.6 U
6.5 U
2.4 U
2.5 U
6.5 UJ
6.8 UJ
Methyl Isobutyl Ketone
108-10-1
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Methyl T-Butyl Ether (MTBE)
1634-04-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Methylcyclohexane
108-87-2
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Methylene Chloride
75-09-2
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
n-Butylbenzene
104-51-8
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
n-Propylbenzene
103-65-1
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
o-Chlorotoluene
95-49-8
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
o-Xylene
95-47-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
p-Chlorotoluene
106-43-4
UG/KG
14 U
8.7 U
4.6 U
6.5 U
2.4 U
2.5 U
6.5 U
6.8 U
p-lsopropyltoluene
99-87-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
sec-Butylbenzene
135-98-8
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Styrene
100-42-5
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
tert-Butylbenzene
98-06-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Tetrachloroethene (Tetrachloroethylene)
127-18-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Toluene
108-88-3
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
trans-1,2-Dichloroethene
156-60-5
UG/KG
34 U
22 U
11 U
16 U
5.9 U
6.3 U
16 U
17 U
trans-1,3-Dichloropropene
10061-02-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Trichloroethene (Trichloroethylene)
79-01-6
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Trichlorofluoromethane (Freon11)
75-69-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Vinyl Chloride
75-01-4
UG/KG
6.8 U
4.3 U
2.3 U
3.3 U
1.2 U
1.2 U
3.2 U
3.4 U
Miscellaneous Volatiles
Thiobismethane
UG/KG
NR
NR
200 NJ
NR
NR
NR
NR
NR
Extractables Scan
% Moisture
%
70
68.22
29.58
33.67
20.62
19.98
55.91
57.75
(3-and/or 4-)Methylphenol
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
1,1 -Biphenyl
92-52-4
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
1,2,4-Trichlorobenzene
120-82-1
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
2,3,4,6-Tetrachlorophenol
58-90-2
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
2,4,5-Trichlorophenol
95-95-4
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
2,4,6-Trichlorophenol
88-06-2
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
2,4-Dichlorophenol
120-83-2
UG/KG
1100 U
1000 U
460 U
500 U
400 U
410 U
740 U
740 U
2,4-Dimethylphenol
105-67-9
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2,4-Dinitrophenol
51-28-5
UG/KG
2200 UJ
2000 UJ
930 UJ
990 UJ
790 UJ
820 UJ
1500 UJ
1500 UJ
2,4-Dinitrotoluene
121-14-2
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2,6-Dinitrotoluene
606-20-2
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Chloronaphthalene
91-58-7
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Chlorophenol
95-57-8
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Methyl-4,6-Dinitrophenol
534-52-1
UG/KG
2200 U
2000 U
930 U
990 U
790 U
820 U
1500 U
1500 U
2-Methylnaphthalene
91-57-6
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Methylphenol
95-48-7
UG/KG
1100 U
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Nitroaniline
88-74-4
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
2-Nitrophenol
88-75-5
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
3,3'-Dichlorobenzidine
91-94-1
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
3-Nitroaniline
99-09-2
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Bromophenyl Phenyl Ether
101-55-3
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Chloro-3-Methylphenol
59-50-7
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Chloroaniline
106-47-8
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Chlorophenyl Phenyl Ether
7005-72-3
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Nitroaniline
100-01-6
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
4-Nitrophenol
100-02-7
UG/KG
2200 U
2000 U
930 U
990 U
790 U
820 U
1500 U
1500 U
Acenaphthene
83-32-9
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Acenaphthylene
208-96-8
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Acetophenone
98-86-2
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Anthracene
120-12-7
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Atrazine
1912-24-9
UG/KG
1100 UJ
1000 UJ
460 U
500 U
400 UJ
410 UJ
740 U
740 U
Benzaldehyde
100-52-7
UG/KG
1100 u
1000 u
460 UJ
500 UJ
400 U
410 U
740 UJ
740 UJ
Benzo(a (Anthracene
56-55-3
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Benzo(b)Fluoranthene
205-99-2
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
Benzo(ghi)Perylene
191-24-2
UG/KG
1100 u
1000 u
460 U
500 U
400 U
410 U
740 U
740 U
117
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Table 19
Quality Control/Quality Assurance Duplicate Sample Results
Water Quality Study of Bays in Coastal Mississippi
September 27-30, 2005
Results of Duplicate Sampling
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
Duplicate
Sample
BBB3DSD
BBB3SD
BC4DSD
BC4SD
ER1 DSD
ER1SD
SLB6DSD
SLB6SD
9/29/2005
9/29/2005
9/27/2005
9/27/2005
9/28/2005
9/28/2005
9/30/2005
9/30/2005
Metals Scan
1005
945
1300
1240
1430
1400
1100
1040
Dibenzofuran
132-64-9
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Diethyl Phthalate
84-66-2
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Dimethyl Phthalate
131-11-3
UG/KG
1100
UJ
1000
UJ
460
U
500 U
400
UJ
410 UJ
740 U
740 U
Di-n-Butylphthalate
84-74-2
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Di-n-Octylphthalate
117-84-0
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Fluoranthene
206-44-0
UG/KG
1100
U
1000
U
66
J
500 U
400
U
410 U
740 U
740 U
Fluorene
86-73-7
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Hexachlorobenzene (HCB)
118-74-1
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Hexachlorobutadiene
87-68-3
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Hexachlorocyclopentadiene (HCCP)
77-47-4
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Hexachloroethane
67-72-1
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Indeno (1,2,3-cd) Pyrene
193-39-5
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Isophorone
78-59-1
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Naphthalene
91-20-3
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Nitrobenzene
98-95-3
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
n-Nitroso di-n-Propylamine
621-64-7
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
n-Nitrosodiphenylamine/Diphenyl amine
122-39-4
UG/KG
1100
U
1000
U
460
U
500 U
400
U
410 U
740 U
740 U
Pentachlorophenol
87-86-5
UG/KG
2200
u
2000
u
930
U
990 U
790
U
820 U
1500 U
1500 U
Phenanthrene
85-01-8
UG/KG
1100
u
1000
u
460
U
500 U
400
U
410 U
740 U
740 U
Phenol
108-95-2
UG/KG
1100
u
1000
u
460
U
500 U
400
U
410 U
740 U
740 U
Pyrene
129-00-0
UG/KG
1100
u
1000
u
63
J
500 U
400
U
410 U
740 U
740 U
Classical Nutrients
Ammonia
7664-41-7
MG/KG
52
77
15
13
3.4
3 U
16
17
Nitrate-Nitrite Nitrogen
MG/KG
3.1
UJ
2.8
UJ
1.6
UJ
1.9 UJ
1.3
UJ
1.2 UJ
2.2 UJ
2.3 UJ
Total Kjeldahl Nitrogen
MG/KG
2300
2400
430
330
57
57
1300
1200
Total Organic Carbon
MG/KG
26000
28000
9800
U
9800 U
8700
U
8600 U
14000
13000
Total Phosphorus
7723-14-0
MG/KG
300
330
1800
2400
26
u
26 U
170
160
Data Qualifiers
U-Analyte not detected at or above reporting limit. The number is the minimum quantitation limit.
J-ldentification of analyte is acceptable; reported value is an estimate.
UJ-Analyte not detected at or above reporting limit. Reporting limit is an estimate.
N-Presumptive evidence analyte is present; analyte reported as tentative identification.
NJ-Presumptive evidence analyte is present; analyte reported as tentative identification. Reported value is an estimate.
K-ldentification of analyte is acceptable; reported value may be biased high. Actual value expected to be less than the reported value.
L-ldentification of analyte is acceptable; reported value may be biased low. Actual value expected to be greater than reported value.
NA-Not Analyzed. | NAI-Not Analyzed due to Interferences. | A-Analyte analyzed in replicate. Reported value is'average'of replicates.
R-Presence or absence of analyte can not be determined from data due to severe quality control problems. Data are rejected and considered unusable.
C-confirmed by GCMS | /1-when no value is reported, see chlordane constituents | /2-constituents or metabolites oftechnical chlordane
NR-Not Reported
118
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