ENVIRONMENTAL LABORATORY ADVISORY BOARD MEETING

Monthly Teleconference: 202-991-0477/7939251# March 21, 2018; 1:00 - 3:00 p.m. EST

MEETING SUMMARY

The U.S. Environmental Protection Agency's (EPA) Environmental Laboratory Advisory Board
(ELAB or Board) teleconference meeting was held on March 21, 2018. The agenda for this
meeting is provided as Attachment A, a list of meeting participants is provided as Attachment
B, and action items are included as Attachment C. The official certification of the minutes by the
Chair or Vice-Chair and the Designated Federal Officer is included as Attachment D.

ROLL CALL/ INTRODUCTION

Dr. Tom O'Farrell started the recording at 12:56pm. Dr. Delaney noted that this is the 1st post-
Kristen meeting so Dr. O'Farrell and he will be taking notes together. Dr. Mike Delaney, Chair
of ELAB, welcomed the members and guests to the meeting. He took roll of the members
present and attending by teleconference.

APPROVAL OF THE PRIOR MINUTES

Dr. Delaney asked whether any members had comments about the Board's February 2018
minutes; Dr. Delaney had comments about the cyanide methodology 2mi paragraph referring to
the wastewater Methods Update Rule. That paragraph should state communicating with
Adrian Hanley and Lemuel Walker and not with Mr. Hautman. Dr. Dallas Wait moved to
approve the minutes; Dr. Leibovitz seconded the motion. The Board unanimously approved the
February minutes.

OPENING REMARKS AND UPDATES FROM THE DFO

Dr. Tom O'Farrell thanked everyone for attending and congratulated Mr. Michael Floumoy and
Mike Delaney on their new positions and wished them the best of luck. Kristen is no longer
with us; we now have Thomas Cawiezell, who is a contractor at the EPA, writing up the
minutes with the meeting recording. As Lara said we are in a recruiting year so if you know
anyone who would be interested in joining the board please let Dr. O'Farrell know so we can
begin the onboarding process. The ELAB is looking to add 6 new people to the board.

Dr. O'Farrell is going to check with Ms. Lara Phelps and review the requirements for new
members to join the ELAB board. There will be a Federal Register notice (FRN) requesting
nominations, but EPA is considering broadening the requirements for expertise. Until this FRN
goes out we can refer to the FRN from 2 years ago if you have interested candidates, or are


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interested in nominating people. The FRN will be posted in April or May and Dr. O'Farrell will
send out the FRN from 2 years ago to reference until this FRN goes out.

According to the charter, ELAB formally reports to the EPA Administrator, the Science Advisor,
or the FEM. We want to try to reestablish the process according to the charter. In the future we
should be formatting letters or reports for EPA so they are addressed to the EPA Science
Advisor, Dr. Jennifer Orme-Zavaleta. Dr. O'Farrell will work on getting everyone the correct
contact information. Each letter or document should be addressed to Dr. Orme-Zavaleta,
reviewed and approved by the Board and sent to Dr. O'Farrell to be processed. Dr. O'Farrell
will decide who the most appropriate person in the program offices is to get the letter or report
in addition to the Science Advisor.

TASK GROUP UPDATES ON CURRENT TOPICS

The Board possesses broad expertise and works on a variety of topics identified by ELAB
members, the Agency or the environmental laboratory community. The Board addresses these
topics through temporary Task Groups. The Task Group leaders or their representatives
provided a report of current topics/activities.

Cyanide Methodology

Dr. Leibovitz sent the ELAB Cyanide Methodology letter back to EPA since our last meeting,
responding to the EPA letter. This effort is on hold pending EPAs response. The wastewater
Methods Update Rule (MUR) on the Clean Water Act question and answer site on cyanide
hasn't been updated since 2004 and is no longer correct. Mr. Adrian Han ley and Mr. Lemuel
Walker have been working on site updates and will go live with it when it has been approved.
EPA is working on the next MUR and said they would like any submissions by May 30th in
order to be considered. They have also updated the FAQs on the 600 series methods. Dr.
Leibovitz will reach out to Richard Burrows and see if ELAB should have a task group to
develop a proposal that EPA further revise and improve Methods 608.3, 624.1 and 625.1 during
the next MUR cycle.

Selected Ion Monitoring (SIM)

The SIM task group met to discuss the EPA's response for the minimum criteria arid determine
how comprehensive the Board's response should be. This meeting included five members from
ELAB and four external subject matter experts. Dr. Delaney will propose to task the group to
revise the minimum SIM criteria.

EPA's letter contained 8 pages of comments and clarifications plus a reprint of EPA research on
SIM gas chromatography (GC)/mass spectrometry (MS) for air toxics analysis (Pleil et al. 1990.


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Journal of the Air & Waste Management Association 41(3):287-293.) EPA discussed the
minimum criteria at a FEM meeting and solicited comments from subject-matter experts. Staff
from EPA's Office of Air and Radiation, Office of Land and Emergency Management, Office of
Resource and Conservation Recovery, OW'sOffice of Science and Technology, National
Exposure Research Laboratory, NRMRL, and Region 7 provided input. Generally, EPA was
"very supportive of having some minimum criteria for SIM methods" but noted that its
programs have differing needs. The Agency asked ELAB to "provide a revision to the minimum
criteria."

In its feedback, EPA provided a number of editorial suggestions, as well as 7 pages of technical
suggestions about background/definitions, personnel, method flexibility, type of MS, MS tuning
criteria, number of scans per peak and scan descriptors, SIM acquisition parameters, sensitivity,
retention time windows, identification and identification verification criteria, automated peak
detection, and other criteria that have not been mentioned.

The SIM task group will address EPA's comments in the revised minimum criteria document,
though not point by point.

User-Generated Library Acceptance Criteria

Dr. Brian Buckley sent a draft letter earlier today regarding the topic discussed last month to
suspend the tuning criteria. This effort was recommended at the end of last meeting. Dr.
Buckley requests that the Board please read and make comments and send to him. The Board
will then vote on the final draft. Unless EPA will suspend the requirement of calibration, none
of the criteria matter in terms of using user-based libraries. The effects of not allowing the
suspension is people must detune instruments, which reduces sensitivity. The Board has
considered going to the FEM to discuss and think about considering all programs that use
GC/MS. Ms. Phelps suggested allowing flexibility in some EPA methods. The Board has
suggested removing the word suspend from the letter and using words such as flexibility more.
The Board suggested meeting again with Ms. Phelps via teleconference to get her opinion on
methods. This will give the Board a way to express ideas and methods, and to talk about how
many methods are not flexible enough. This is an opportunity to provide more sensitivity and
selectivity and take advantage of newer technology. Dr. O'FarrelI expressed that this cannot be
a formal meeting, so there cannot be a quorum of members. Dr. Buckley suggested the next
steps to take place would be to set up a task group to meet with Ms. Phelps. He will draft a
letter to her.

Addressing emerging contaminants

In the Absence of Ms. Sharon Mertens, no update was provided.


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Acrolein and Acrylonitrile

Dr. Mahesh Pujari explained that he would like to submit a letter with the current data to EPA
regarding the analysis requirements and pH preservation for acrolein and acrylonitrile, asking
whether the Board supported submitting another letter to EPA. EPA had not incorporated the
recommended changes into the revised MUR because submitted data was not in sample matrix
and it was in deionized water. Dr. Pujari will work on getting more data to EPA, suggesting
that this change is very much needed. Dr. Leibovitz heard back from Dr. O'Farrell about the
use of commercial laboratory data to support this position, and EPA has concerns about conflict
of interest between contracted and industry labs. Dr. O'Farrell talked to people in General
Council and they recommended not using commercial laboratories. Dr. O'Farrell will write up
an explanation from General Council as to why EPA doesn't want to use commercial
laboratories. Dr. Richard Burrows (TestAmerica, Inc.) explained in the previous meeting that
they have plenty on data that they would share to help ELAB's positions. Dr. Pujari will write
up another letter to EPA stating science is science and urge them to consider taking data from
other sources.

Drinking Water Program Adoption of Recent Approved Methods
In the absence of Ms. Deb Waller, no update was provided.

Inactive Topics

1.	Whole Effluent Toxicity PT Standards

Dr. Henry Leibovitz had no updates on this topic. Before the next meeting he will reach out to
Ms. Lynn Bradley about TNI meeting minutes. He will follow-up with updates during next
month's ELAB meeting.

2.	Drinking Water Certification

In the Absence of Ms. Sharon Mertens, no update was provided

3.	In-line/On-line

Mr. Flournoy had no update, waiting to hear back from EPA. Dr. O'Farrell will reach out to Mr.
Lemuel Walker about if there have been any more meetings on in-line/on-line monitoring.

4.	Interagency data quality task force

Dr. Leibovitz indicated no meeting on this topic has happened between EPA and DOD
members on the task force. Ms. Phelps mentioned that this is still something they want to do,
it's just a matter of getting meetings scheduled. The Board asked that Dr. O'Farrell reach out


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and see if anything has been any scheduled or will be scheduled. Dr. Wait and Dr. Leibovitz
have asked to be included on these meetings if that were possible.

NEW TOPICS/ISSUES FOR CONSIDERATION

Dr. Richard Burrows commented in the February meeting saying ELAB isn't doing what labs
and industry want us to do. Dr. Burrows has requested that the Board consider establishing a
group to develop a proposal that EPA further revise and improve methods 608.3, 624.1 and
625.1 during the next MUR cycle. Dr. Leibovitz will follow-up with Dr. Burrows to obtain
further information.

Please read the draft that Dr. Buckley wants to send to EPA asking about whether they would
be willing to suspend the current tuning requirement to allow us to consider validation criteria
for user generated library spectra. Dr. Delaney would like to finalize it and vote to send it at the
April meeting.

WRAP-UP/SUMMARY OF ACTION ITEMS

Dr. O'Farrell reviewed the action items identified during the meeting, which are included in
attachment C. The next ELAB meeting is scheduled for the 18th of April. Dr. O'Farrell noted
more rounds of edits to the minutes may need to take place.

CLOSING REMARKS/ADJOURNMENT

Dr. Buckley moved to adjourn the meeting, the motion was seconded. The Board unanimously
voted to adjourn the meeting at 2:14 pm.


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Attachment A

ENVIRONMENTAL LABPORATORY ADVISORY BOARD (ELAB)

Face-to-Face Meeting/Teleconference: 202-991-0477 / 793-9251#

Date i I hue 3/21 /2018 I 1:00-3:00PM EST I	¦	• Mike Delaney

Item

Call Meeting to Order

Introduction of Board Members/Roll Call
Approval of Minutes for Previous Meeting(s)

Opening Remarks and Updates from DFO

Updates on Current Topics

A.	Cyanide Methodology — Delaney

B.	Selecting Ion Monitoring — Delaney

C.	User-generated Library Acceptance Criteria — Buckley

D.	Addressing Emerging Contaminants — Mertens

E.	Acrolein and Acrylonitrile Preservation and pH — Pujari

F.	Improving PCB congener method option — Pujari

G.	Drinking Water Program Adoption of Recent Approved
Methods — Waller

Inactive Topics awaiting feedback/input	Board

A.	Whole Effluent Toxicity proficiency study standards —

Leibovitz

B.	Drinking Water Certification Officer's Training Course —

Mertens

C.	In-Line/On-Line Monitoring — Flournoy

D.	Interagency Data Quality Task Force/Data Quality
Objective Process — Leibovitz

New Topics/Issues for Consideration	Delaney

Wrap-Up/Summary of Action Items	O'Farrel 1/Cawiezel 1 /Delaney

Owner

Delaney
Board

Delaney

O'Farrell

Board

Closing Remarks/Adjou rnment

O'Farrell/Delaney


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Attachment B
PARTICIPANTS LIST

Board Members Attendance
(Y/N)

Name

Affiliation







N

Dr. Michael (Mike) Delaney
(Chair)

Massachusetts Water Resources
Authority (MVVRA)

Representing: MWRA I

Y

Mr. Michael Floumoy (Vice-
Chair)

Eurofins Environment Testing
USA

Representing: American Council
of Independent Laboratories

Y

Dr. Thomas OTarrell (DFO)

U.S. Environmental Protection
Agency

Representing: CPA !

Y

Dr. Kim Anderson

Oregon State University
Representing: Academia—Oregon
State University

Y

Dr. Brian Buckley

Rutgers Environmental and
Occupational Health Sciences
Institute

Representing: Academia and

La boratory—R ut jiers

Y

Ms. Patricia (Patty) Carvajal

San Antonio River Authority

Representing:

Watershed/Restoration

Y

Dr. Deyuan (Kitty) Kong

Chevron Energy Technology
Company

Representiim: Chevron

N

Mr. Jeff Loewe

NiSource, Inc.
Representing: Industry—
NiSource. Inc.

Y

Dr. 1 lenrv Leibovilz

Rhode Island State 1 lealth
Laboratories

Representing: Association of
Public 1 lealth Laboratories

N

Mr. Brad Meadows

Babcock Laboratories, Inc.

Representing: Commercial
Laboratory— Babcock
Laboratories, Inc.

N

Ms. Sharon Merteiis

Milwaukee Metropolitan Sewerage
District

Representing: The NELAC

Institute

Y

Dr. Mahesh Pujari

City of Los Angeles
Representing: National

Association of Clean Water
A uendes

Y

Mr. Elan Rieser

Con Edison - Representing: Utility
Water Act Group








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Y

Dr. A. Dallas Wait

Gradient

Representing: Consumer Products
Indnstrv

N

Ms. Debra (Deb) Waller

New Jersey Department of





Environmental Protection





(NJDEP)





Representing: State Government—





NJDEP

PARTICIPANTS LIST (CON'T)

Contractors and Guests
Attendance (Y/N)

Name

Affiliation

N

Mr. Thomas Cawiezell
(Contractor)

Oak Ridge Associated
Universities at EPA

Y

Mr. Travis Bartholomew (Guest)

Texas Commission on

Environmental Quality

Y

Ms. Francois Chauvin (Guest)

New York City Department of
Environmental Protection


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Attachment C

Action Items

1.	Tom O'Farrell - Ask Lara Phelps if ELAB User-Generated Library Acceptance Criteria
task group can meet with her to talk about the issue of adding flexibility to EPA
methods. Possible engagement with FEM on this topic.

2.	Tom O'Farrell - Provide ELAB members with a summary of the Office of General
Council's determination on whether commercial labs can provide data on acrolein and
acrylonitrile.

3.	The Selected Ion Monitoring task group will meet to discuss the latest version of their
response letter to EPA.

4.	ELAB Members - Review the next draft of the Mass Spectral Library letter. Provide
feedback to Brian Buckley with the goal of final discussion at the next ELAB meeting.

5.	Mahesh Pujari - Invite Adrian Hanley to next ELAB meeting to discuss PCB congener
method options.

6.	Tom O'Farrell - Ask Lemuel Walker (EPA, OW) if there have been any further meetings
on In-Line/On-Line Monitoring.

7.	Henry Leibovitz - Ask Richard Burrows if ELAB should have a task group on EPA 600
Series methods.

8.	Henry Leibovitz - Ask Lynn Bradley if there was any additional discussion of whole
effluent toxicity in the latest TNI meetings.

9.	Tom O'Farrell - Ask Lara Phelps if there have been any further meetings of the
Interagency Data Quality Task Group.

10.	Tom O'Farrell - Ask Lara Phelps if stakeholders need to send supporting letters for
ELAB members being renewed for another term on ELAB.

11.	Tom O'Farrell - Send 2016 Federal Register Notice for recruiting new members of ELAB
to ELAB members.


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Attachment D

I hereby certify that this is the final version of the minutes for the Environmental
Advisory Board Meeting held on March 21, 2018.

H Recoverable Signature

}\U. UoJ f'

Dr. Michael Delaney
Chair

Sianed bvc Delarvev, Mike

X	¦ 0^7,

Or. Thomas O'Parrel!

Desionated Federal Officer


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