NCP SUBPART J TECHNICAL NOTEBOOK
A COMPENDIUM TO THE NCP PRODUCT SCHEDULE

MARCH 2023
(03/01/2023)

FOREWORD

The U.S. Environmental Protection Agency's (EPA) Office of Emergency Management (OEM)
Regulations Implementation Division (RID) compiled the National Oil and Hazardous
Substances Pollution Contingency Plan (NCP) Product Schedule, as required by the Clean Water
Act, the Oil Pollution Act of 1990 (OPA 90), and the NCP. This NCP Product Schedule
Technical Notebook contains a compilation of product bulletins summarizing data requirements
and test results for those products listed on EPA's NCP Product Schedule. The Technical
Notebook presents information provided by the product manufacturer to include, but is not
limited to: contact information, worker health and safety, storage, application methods, toxicity
and effectiveness data, and physical properties. Updates to this Technical Notebook, such as the
addition of new products to the Schedule, or modifications and/or deletions of listed products,
are indicated in bold.

NCP Product Schedule Technical Notebook users can navigate to all product bulletins, including
aka's, by category type (i.e., Bioremediation Agents, Dispersants, Miscellaneous Oil Spill
Control Agents, Surface Collecting Agents, Surface Washing Agents) or alphabetically by
clicking on the product link in the Table of Contents; and scrolling through the Navigation Pane.

For additional information, please leave a message on EPA's NCP Subpart J Information Line at
(202) 260-2342.

Written requests may be mailed to:

Attention: NCP Product Schedule Manager
U.S. Environmental Protection Agency
1200 Pennsylvania Avenue NW
Mail Code: 5104-A, Room 1448K
William Jefferson Clinton North Building
Washington, DC 20460

Disclaimer: [Product Name] is on the U.S. Environmental Protection Agency's NCP Product
Schedule. This listing does NOT mean that EPA approves, recommends, licenses, certifies, or
authorizes the use of [Product Name] on an oil discharge. The listing means only that data have
been submitted to EPA as required by Subpart J of the National Oil and Hazardous Substances
Pollution Contingency Plan, Section 300.915. (Source: 40 CFR §300.920 (e))


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Currently Listed Number of NCP Product Schedule

Products Listed by Category

Product Category

Bioremediation Agents (B)

Dispersants (D)

Miscellaneous Oil Spill Control Agents (M)
Surface Collecting Agents (S)

Surface Washing Agents (SW)

Total Products

Number of Products

29
19
18
2

62
130

All changes and additions to the NCP Product Schedule Technical Notebook are indicated in bold
under the applicable product listing.

Changes to the Product Bulletins

Product Bulletin Changes Pending EPA
Verification:

Contact Information Could Not Be Verified
(last attempt dates noted on product bulletin):

CLEANGREEN® PLANET WASH (SW-44) to include
changes to listing letter date, product name, manufacturer
contact information, and distributor contact information;
and ABLUOL OSASA H/C (SW-75) new product
listing.

STEP ONE (B-43); SHAMANTRA GREEN (B-68); OIL
SOLUTIONS POWDER (M-25); SIMPLE GREEN®
(Water Based) (SW-15); PREMIER 99 (SW-12); and EO
ALL PURPOSE SOAP-LAVENDER (SW-50).

WMI-2000 (B-19); SYSTEM E.T. 20 (B-45); BET
BIOPETRO (B-48); LAND AND SEA RESTORATION
PRODUCT 001 (VELITE) (B-55); JE1058BS (B-58);
PRO-ACT (B-62); DUALZORB® (B-65); ERGOFIT
MICRO MIX AQUA (B-67); NEOS AB3000 (D-2);
MARE CLEAN 200 (D-3); JD-109 (D-6); JD-2000™
(D-7); BIODISPERS (D-9); SAF-RON GOLD (D-12);
ZI-400 (D-13); FFT-SOLUTION® (D-17); CIAGENT
(M-17); WASTE-SET #3200® (M-19); WASTE-SET
#3400® (M-20); RAPIDGRAB 2000™ (M-24);
ELASTOL (M-26); NORSOREX® APX (M-30); CAS
100© (M-31); THICKSLICK 6535 (S-5); SILTECH OP-
40 (S-6); CN-110 (SW-9); DE-SOLV-IT INDUSTRIAL
FORMULA (SW-11); NATURE'S WAY HS (SW-18);
PETROTECH 25 (SW-21); DO-ALL #18 (SW-24); BG-
CLEAN™ 401 (SW-32); E-SAFE© (SW-33); SHEEN-
MAGIC© (SW-34); PROCLEANS (SW-35); G-CLEAN
OSC-1809 (SW-39); GREEN BEAST™ OIL SPILL &
ODOR REMEDIATOR (SW-40); SOC-10 (SW-45);
ENVIRONMENTAL 1 CRUDE OIL CLEANER (SW-
47); SANDKLENE 950 (SW-48); DE-SOLV-IT CLEAN
AWAY APC SUPER CONCENTRATE (SW-49);
VERU-SOLVE™ MARINE 200 HP (SW-52); JEP-

li


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MARINE CLEAN (SW-52); ETHOS CLEAN (SW-58);
OSR-IO (SW-59); EPA OIL FIELD SOLUTION™ (SW-
61); and FORMULA 206-lx BIO-WASH™ (SW-66).

Note: Products are numbered as they are listed. Numbering may not be consecutive when products are
removed from the NCP Product Schedule. For example, Bioremediation Agents begin with B-19.

Products numbered B-l through B-18 were removed from the NCP Product Schedule.

Updated: 03/01/2023

111


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NCP PRODUCT SCHEDULE TECHNICAL NOTEBOOK
TABLE OF CONTENTS: LISTING BY PRODUCT CATEGORY

BIOREMEDIATION AGENTS: TECHNICAL NOTEBOOK BULLETINS	1

W VI1-2000	2

OPPENHEIMER FORMULA	5

MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL	8

VB591™, VB997™, BINUTRIX®	12

STEP ONE	16

SYSTEM E.T. 20	20

BET BIOPETRO	24

Oil. SPILL EATER II (OSE II)	27

LAND AND SEA RESTORATION PRODUCT 001 (VELITE)	32

S-200C	35

SPILLREMED (MARINE)®	39

JE1058BS	42

BIO WORLD BIOREMEDIATION TREATMENT PRODUCTS (BIOWORLD BHTP)	45

MUNOX SR®	49

SOU. RX	53

PRO-ACT	57

BIOREM-2000 OIL DIGESTER™	61

DRYLET™ MB BIO	65

DUALZORB®	68

REMEDIADE™	72

ERGOFIT MIC ROM IX AQUA	76

SHAM ANTRA GREEN	81

SUMP SAFE BIO-RECLAIM	85

WASTE AWAY®	89

ACT TERRA FIRM A	93

PETROCLEAN™	98

ECOBIOCLEAN® 100 COSW	102

SPILL GENIE™ 3T	107

GHG ORGANIC	Ill

DISPERSANTS: TECHNICAL NOTEBOOK BULLETINS	115

COREXIT™ EC9527A	116

NEOS AB3000	 120

MARE CLEAN 200	 123

COREXIT™ EC9500A	126

DISPERSIT SPC 1000™	130

JD-109	133

JD-2000™	136

NOKOMIS 3-F4	139

BIODISPERS	142

SEA BRAT #4	145

FINASOL® OSR 52	148

Categorical Table of Contents	iv	Categorical Table of Contents


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SAF-RON GOLD	152

Z1-400 	 155

NOKOMIS 3-AA	158

ACCELL CLEAN® DWD	162

FFT-SOLUTION®	166

MARINE D-BLUE CLEAN™	170

COREXIT™ EC9500B	173

CHIMEC CHIMSPERSE 6000	 177

MISCELLANEOUS OIL SPILL CONTROL AGENTS: TECHNICAL NOTEBOOK

BULLETINS	180

PES-51	181

CIAGENT	186

ZYME-FLOW	189

WASTE-SET #3200®	192

WASTE-SET #3400®	195

PX-700®	198

ALSOCUP	201

RAPIIXiRAB 2000™	204

Oil. SOLUTIONS POWDER	207

ELASTOL	210

OIL BOND®	213

AQUAFLEX® (Open-Cell Elastomeric Sorbents)	216

GELCO 200	219

NORSOREX® APX	223

CAS 100®	228

S-200 OILGONE®	231

HYDRO-BOND™	234

AQUAPAL® (Open-Cell polyolefin foam Sorbent)	237

SURFACE COLLECTING AGENTS: TECHNICAL NOTEBOOK BULLETINS 240

THICK SLICK 6535	241

SILTECH OP-40	244

SURFACE WASHING AGENTS: TECHNICAL NOTEBOOK BULLETINS	247

TOPS ALL #30 (aka, SUPERALL #38)	248

CN-110	251

COREXIT™ EC9580A	254

DE-SOLV-IT INDUSTRIAL FORMULA	257

PREMIER 99	260

SIMPLE GREEN®	263

AQUACLEAN	266

NATURE'S WAY HS	269

CYTOSOL	272

BIO SOLVE® PINK WATER"	276

Categorical Table of Contents	v	Categorical Table of Contents


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PETROTECH 25 	279

PI TRO-C I.HAN	282

DO-ALL #18	285

SC-1000™	288

GOLD CREW SW	291

N ALE-IT	294

1-500	297

i:\yiroci.i :\\	300

BG-CLEAN™ 401 	 303

E-SAFE®	306

SHEEN-MAGIC®	309

PROCLEANS	312

SPILLCLEAN	315

TXCHEM HE-1000™	319

NOKOMIS 5-W	322

G-CLEAN OSC-1809	 325

GREEN BEAST™ OIL SPILL & ODOR REMEDIATOR	328

TULXA	331

MARINE GREEN CLEAN™	334

MARINE GREEN CLEAN PLUS™	337

CLEANGREEN® PLANET WASH	340

SOC 10 (SURFACE OIL CLEANER)	343

BIOGRASS EXTRA®	346

ENVIRONMENTAL 1 CRUDE OIL CLEANER	349

SANDKLENE 950	 352

DE-SOLV-IT CLEAN AWAY APC SUPER CONCENTRATE	355

EO ALL PURPOSE SOAP-LAVENDER	358

DYNAMIC GREEN™	361

VERU-SOLVE™ MARINE 200 HP	364

NATURAMA G3 A-5	367

SAFEKLEEN	370

CORIBA 700 SR	373

CORIBA 713 SR	376

JEP-MARINE CLEAN	379

ETHOS CLEAN	382

OSR-10	385

ACCELL CLEAN® SWA	388

EPA Oil. FIELD SOLUTION™	391

PETROMAX PSC 3	394

GREEN TECHNOLOGIES SOLUTIONS-OIL RECOVERY (GTS-OR)	397

SIMPLE GREEN® 2013 Reformulation	400

NONTOX™ SURFACE WASHING AGENT	403

FORMULA 206-lx BIO-WASH™	406

RHAMNOWASH 10	409

ADP-7	412

Categorical Table of Contents	vi	Categorical Table of Contents


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WATER WORKS™ HEAVY DUTY DEGREASER CONCENTRATE	415

X4JH2000	418

TASMANIA C-CLENZ	421

GOLD CREW® TC	425

DE-OIL-IT INDUSTRIAL STRENGTH CONCENTRATE	428

ECOGREEN	431

ABLUOL OSASA H/C	434

Categorical Table of Contents

vii

Categorical Table of Contents


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NCP PRODUCT SCHEDULE TECHNICAL NOTEBOOK
ALPHABETICAL LIST OF ALL PRODUCT BULLETINS

ABLUOL OSASA II/C	434

ACCELL CLEAN® DWD	162

ACCELL CLEAN® SWA	388

ACT TERRA FIRM A	93

ADP-7	412

ALSOCUP	201

AQUACLEAN	266

AQUAFLEX® (Open-Cell Elastomeric Sorbents)	216

AQUAPAL® (Open-Cell polyolefin foam Sorbent)	237

BET BIOPETRO	24

BG-CLEAN™ 401 	 303

BIODISPERS	142

BIOGRASS EXTRA®	346

BIOREM-2000 OIL DIGESTER™	61

BIO SOLVE® PINK WATER"	276

BIO WORLD BIOREMEDIATION TREATMENT PRODUCTS (BIOWORLD BHTP)	45

CAS 100®	228

CIIIYIHC CHIMSPERSE 6000	 177

CIAGENT	186

CLEANGREEN® PLANET WASH	340

CN-110	251

COREXIT™ EC9500A	126

COREXIT™ EC9500B	173

COREXIT™ EC9527A	116

COREXIT™ EC9580A	254

CORIBA 700 SR	373

CORIBA 713 SR	376

CYTOSOL	272

DE-OIL-IT INDUSTRIAL STRENGTH CONCENTRATE	428

DE-SOLV-IT CLEAN AWAY APC SUPER CONCENTRATE	355

DE-SOLV-IT INDUSTRIAL FORMULA	257

DISPERSIT SPC 1000™	130

DO-ALL #18	285

DRYLET™ MB BIO	65

DUALZORB®	68

DYNAMIC GREEN™	361

ECOBIOCLEAN® 100 COSW	102

ECOGREEN	431

ELASTOL	210

i:\yiroci.i :\\	300

ENVIRONMENTAL 1 CRUDE Oil. CLEANER	349

Alphabetical Table of Contents	viii	Alphabetical Table of Contents


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IX) ALL PURPOSE SOAP-LAVENDER	358

EPA Oil. FIELD SOLUTION™	391

ERGOFIT MIC ROM IX AQUA	76

E-SAFE®	306

ETHOS CLEAN	382

1-500	297

FFT-SOLUTION®	166

FINASOL® OSR 52	148

FORMULA 206-lx BIO-WASH™	406

G-CLEAN OSC-1809	 325

GHG ORGANIC	Ill

GELCO 200	219

GOLD CREW SW	291

GOLD CREW® TC	425

GREEN BEAST™ OIL SPILL & ODOR REMEDIATOR	328

GREEN TECHNOLOGIES SOLUTIONS-OIL RECOVERY (GTS-OR)	397

HYDRO-BOND™	234

JD-109	133

JD-2000™	136

JE1058BS	42

JEP-MARINE CLEAN	379

LAND AND SEA RESTORATION PRODUCT 001 (VELITE)	32

MARE CLEAN 200	 123

MARINE D-BLUE CLEAN™	170

MARINE GREEN CLEAN™	334

MARINE GREEN CLEAN PLUS™	337

MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL	8

MUNOX SR®	49

N ALE-IT	294

NATURAMA G3 A-5	367

NATURE'S WAY HS	269

NEOS AB3000	 120

NOKOMIS 3-AA	158

NOKOMIS 3-F4	139

NOKOMIS 5-W	322

NONTOX™ SURFACE WASHING AGENT	403

NORSOREX® APX	223

OIL BOND®	213

OIL SOLUTIONS POWDER	207

OIL SPILL EATER II (OSE II)	27

OPPENHEIMER FORMULA	5

OSR-10	385

PES-51	181

PETRO-CLEAN	282

PETROCLEAN™	98

Alphabetical Table of Contents	ix	Alphabetical Table of Contents


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PETROMAX PSC 3	3

PETROTECH 25	2

PREMIER 99	2

PRO-ACT	

PROCLEANS	3

PX-700®	1

RAPIIXiRAB 2000™	2

REMEDIADE™	

RHAMNOWASH 10	4

S-200 OILGONE®	2

S-200C	

SAFE KLEEN	3

SAF-RON GOLD	1

SANDKLENE 950	3

SC-1000™	2

SEA BRAT #4	1

SHAM ANTRA GREEN	

SHEEN-MAGIC®	3

SILTECH OP-40	2

SIMPLE GREEN®	2

SIMPLE GREEN® 2013 Reformulation	4

SOC 10 (SURFACE OIL CLEANER)	3

SOIL RX	

SPILLCLEAN	3

SPILL GENIE™ 3T	1

SPILLREMED (MARINE)®	

STEP ONE	

SUMP SAFE BIO-RECLAIM	

SYSTEM E.T. 20	

TASMANIA C-CLENZ	4

THICK SLICK 6535	2

TOPS ALL #30 (aka, SUPERALL #38)	2

TULXA	3

TXCHEM HE-1000™	3

VB591™, VB997™, BINUTRIX®	

VERU-SOLVE™ MARINE 200 HP	3

WASTE AWAY®	

WASTE-SET #3200®	19

WASTE-SET #3400®	19

WATER WORKS™ HEAVY DUTY DEGREASER CONCENTRATE	41

X4JH2000	41

W VI1-2000	

Z1-400 	 155

ZYME-FLOW	189

Alphabetical Table of Contents

x

Alphabetical Table of Contents


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BIOREMEDIATION AGENTS:
TECHNICAL NOTEBOOK BULLETINS

Bioremediation Agents

1

Bioremediation Agents


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

9/07/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #B-19

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JUNE 18, 1990

REVISED LISTING DATE: JANUARY 11, 1996

"WMI-2000"

I.	NAME, BRAND, OR TRADEMARK
WMI-2000

Type of Product: Biological Additive

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
WMI International, Inc.	Mailing Address

2104 Brentwood Drive	WMI International, Inc.

Houston, TX 77019	P.O. Box 130583

Phone: updated information required	Houston, TX 77219

Mobile: updated information required	(Mr. Joseph F. Jennings, President)

Fax: updated information required

E-mail: updated information required

or teri @oxy genorchard. com

(Mr. Joseph F. Jennings, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
WMI International, Inc.	Mailing Address

2104 Brentwood Drive	WMI International, Inc.

Houston, TX 77019	P.O. Box 130583

Phone: updated information required	Houston, TX 77219

Mobile: updated information required	(Mr. Joseph F. Jennings, President)

Fax: updated information required

E-mail: updated information required

or teri @ oxy genor chard. com

(Mr. Joseph F. Jennings, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: WMI-2000 is non-flammable.

2.	Ventilation: Avoid breathing dust or aerosol due to possibility of sensitization. Use adequate
ventilation.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Minimize contact with
eyes, skin, and clothing. Wash hands thoroughly after handling culture.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 45°F - 90°F

Store in a cool, dry location. Keep partially-used containers tightly closed. Prolonged exposure

Bioremediation Agents

2

WMI-2000


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to high temperature and humidity, may lower activity of product.

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

The shelf life of WMI-2000 is 2 years if stored at ambient temperatures

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: The culture should be activated for 2 hours in water, when applicable.
Conditions for use vary depending on substrate concentration and type, pH, temperature,
availability of nutrients, oxygen content, and liquid medium (static or flowing).

2.	Concentration/Application Rate: Inoculation concentration is 5-9 billion spores per gram.

3.	Conditions for Use: Temperature requirements are between 35°F and 100°F. The optimum
dissolved oxygen content is 2 ppm at the sludge-to-water interface. Nitrogen and phosphorous
are key nutrients which promote cultural growth, and should be maintained at concentrations of
15-20 ppm and 2.5-5 ppm, respectively. The optimum pH range is between 7.0 and 8.0.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL
MEAN

RED%



3 REPS/PROD

ALKANES
(ppm)

28 DAYS

AROMATIC
S (ppm)

28 DAYS



CONTROL

2626.7

0

1850.0

0

0

NUTRIENT

2763.3

0

2030.0

0

WMI-2000

2453.3

0

1880.0

0



CONTROL

2246.7

0

1823.3

0

7

NUTRIENT

1920.0

0

1666.7

0



WMI-2000

1243.3

0

1456.7

0



CONTROL

2240.0

14.7

1866.7

-0.9

28

NUTRIENT

1210.0

56.2

1480.0

27.0

WMI-2000

973.3

60.3

1253.0

33.3

Bioremediation Agents

3

WMI-2000


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Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product (WMI-2000)

0%	25%	44%

b. Toxicity: NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentage in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additives:

Optimum pH: 7.0

Optimum temperature: 45°F - 90°F
Optimum salinity: Fresh water to sea water

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 6.0 - 8.0

Temperature: 40°F - 120°F
Salinity range: Fresh to sea water

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the following:

Salmonella - Negative

Fecal Coliform - Negative
Shigella - Negative

Staphylococcus Coagulase positive - Negative
Beta hemolytic Streptococcus - Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

4

WMI-2000


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TECHNICAL PRODUCT BULLETIN #B-36

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 17, 1991

REVISED LISTING DATE: OCTOBER 6, 1996

"OPPENHEIMER FORMULA"

(aka, THE OPPENHEIMER FORMULA I, MICROSORB SC)

I.	NAME, BRAND, OR TRADEMARK
OPPENHEIMER FORMULA

(aka, THE OPPENHEIMER FORMULA I, MICROSORB SC)

Type of Product: Biological Additive

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Oppenheimer Biotechnology, Inc.

P.O. Box 1490
Pflugerville, TX 78691-1490
Phone: (512) 474-1016
E-mail: ien.neve@obio.com
Website: www.obio.com
(Ms. Jen Neve)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Oppenheimer Biotechnology, Inc.

P.O. Box 1490
Pflugerville, TX 78691-1490
Phone: (512) 474-1016
E-mail: ien.neve@obio.com
Website: www.obio.com
(Ms. Jen Neve)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Special ventilation is not required. Treat product as an hygroscopic powder. In
closed spaces use dust protective measures.

3.	Skin and eye contact; protective clothing; treatment in case of contact: The application of the
dry powder requires the usual precautions of a dust irritant to membranes. The material is easily
removed by washing or flushing, and in confined areas or use, a protective mask and eye glasses
are recommended.

4.a.	Maximum storage temperature: 130°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 82°F

V.	SHELF LIFE

The shelf life of the product is approximately 5 year.

Bioremediation Agents

5

OPPENHEIMER FORMULA


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VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Optimal application is by powder seeding directly at the source of oil
contamination. Application over larger areas of water surface can be accomplished by aerial
powder dusting, spraying a water mixture of nutrients/formula over the oil area, or by dusting
with mechanical powder pumps.

2.	Concentration/Application Rate: The application rate at the source oil slick is 1 pound per
cubic yard of oil. In the open sea slick, the basic application rate is 10 pounds per acre, but this
may vary in different situations related to speed of clean up. In estuaries, a larger biomass is
recommended and may be at a rate of up to 100 pounds per acre, depending on the oil type and
concentration. Heavier oils may require a higher biomass than light oils.

3.	Conditions for Use: THE OPPENHEIMER FORMULA may be used in a wide range of
environmental conditions of temperature and salinities, ranging from fresh to 100 ppt salts. The
formula is especially valuable in grass flats, marshes and the open sea. It has also proved
effective in soil and fresh water oil clean up and municipal waste treatment, septic tanks and
grease traps.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28 DAYS

AROMATIC

28 DAYS





(ppm)



S (ppm)





CONTROL

29965.2

0

5620.5

0

0

NUTRIENT

31494.8

0

6660.2

0

OPPENHEIMER

31140.6

0

5528.2

0



CONTROL

30101.5

0

5610.1

0

7

NUTRIENT

8073.9

0

5086.6

0



OPPENHEIMER

5019.7

0

4338.9

0



CONTROL

28785.6

3.9

5512.7

1.9

28

NUTRIENT

706.2

97.8

4863.7

27.0

OPPENHEIMER

3396.8

89.1

3417.8

38.2

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product (Oppenheimer)

-6.4%	50.9%	10.4%

Bioremediation Agents

6

OPPENHEIMER FORMULA


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b. Toxicity:
NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentage in the composition:

Natural, ubiquitous, hydrocarbon-oxidizing, microorganisms for use in removing hydrocarbons
and organic materials from soils, fresh and salt waters by natural oxidative pathways.

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.6

Temperature: 82°F

Salinity: Fresh water to 20 percent salts
Optimal: 0.5 to 3.5%

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 5.5-11

Temperature: 32°F-140°F
Salinity: Fresh to 15%

4.	Special nutrient requirements: NA

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: <90/100 ml
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

7

OPPENHEIMER FORMULA


-------
TECHNICAL PRODUCT BULLETIN #B-41
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: DECEMBER 18, 1991
REVISED LISTING DATE: JANUARY 21, 1997
"MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL"

I.	NAME, BRAND, OR TRADEMARK
MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL
Type of Product: Biological Additive

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Verde Environmental, Inc.

9223 Eastex Freeway
Houston, TX 77093
Phone: (713) 691-6468
(800)626-6598
Fax: (713)691-2331
Website: www.micro-blaze.com
E-mail: bscogin@micro-blaze.com
(Mr. William L. Scogin)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Verde Environmental, Inc.

9223 Eastex Freeway
Houston, TX 77093
Phone: (713) 691-6468
(800)626-6598
Fax: (713)691-2331
Website: www.micro-blaze.com
E-mail: bscogin@micro-blaze.com
(Mr. William L. Scogin)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal room ventilation

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact.
Wear protective gloves, and wash hands with soap and water after handling the product. Wash
contaminated clothing and footwear before reuse.

4.	Optimum Storage Conditions:

4.a. Maximum storage temperature: 120°F

4.b. Minimum storage temperature: 35°F

4.c. Optimum storage range temperature: NA

4.d. Temperatures of phase separations and chemical changes: NA

Bioremediation Agents

8

MICRO-BLAZE® EMERGENCY
LIQUID SPILL CONTROL


-------
V.	SHELF LIFE

Minimum 10 years, with proper storage, in original containers. Freezing will not kill these
microbes; however, extreme heat (over 180°F) for long periods of time will kill the microbes.

VI.	RECOMMENDED APPLICATION PROCEDURE

MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL is a liquid formulation of several
microbial strains, surfactants, and nutrients designed to bioremediate organics and hydrocarbons
in soil and water as well as control odors.

1.	Application Method: Use normal spray equipment, fire or response equipment, eductor setups,
water trucks, etc. as methods of application. Mix MICRO-BLAZE® EMERGENCY LIQUID
SPILL CONTROL/water mixture with contaminated soils and liquids thoroughly for maximum
contact. Pick up treated contamination after volatile hazard has been negated per local
regulatory parameters.

For general bioremediation: For in-situ soils, mix MICRO-BLAZE® EMERGENCY LIQUID
SPILL CONTROL/water mixture can be tilled into the contaminated area. For shallower
contamination, areas can be over sprayed with normal spray equipment, eductor setups, water
trucks, etc. For deeper contamination, application can be applied through underground setups
using perforated piping per regulatory recommendations. For wastewater and other operational
by-product sludges and soils extracted from contaminated areas, a bioslurry or bioreactor can be
setup using MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL and water in the
process.

2.	Concentration/Application Rate: For more viscous or less hazardous contamination, apply
MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL at a 3% solution mixed with
water (3 parts MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL, 97 parts water).
When bioremediating soils, generally, per every 10 cubic yards of contaminated soils, use one
gallon of concentrate, diluted with water according to contamination type.

3.	Conditions for Use: Water Salinity: Can be mixed with any fresh, brackish or brine. However,
brine reduces the effectiveness by 10%.

Water Temperature: 35°F - 180°F
pH: 4 to 11.5

Temperature: 32°F - 120°F

Nutrient Requirements: Nutrients for microbes are included in product. However, for longer-
term bioremediation projects, additional applications of bio-catalyst may be added to boost
microbial activity.

Type and Ages of Pollutants: For use on organics and hydrocarbon-based materials. These
strains of bacteria provide the capability of biodegrading various straight chained, branched
chained, aromatic and polynuclear aromatic hydrocarbons found in diesel and other fuels. Age
of contamination is not a factor as much as its density. Tar-like substances may need to be cut
for timely remediation.

Bioremediation Agents

9

MICRO-BLAZE® EMERGENCY
LIQUID SPILL CONTROL


-------
VII. TOXICITY AND EFFECTIVENESS

Non-toxic, naturally-occurring spore-forming microorganisms common to soil and water. Non-
pathogenic, certified by count; will not mutate.

a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300,900) Federal Register September 15,
1994.

Microbiological Results - Average

Day 0 - 1.7 x 109 Day 7 - 8.43 x 108 Day 28 - 5.2xl07

The organisms in this product convert to a spore state (dormant) to survive an unfavorable
environment and will reactivate upon favorable conditions. Documentation available from
Verde Environmental.

Summary Data Table	

DAYS

28

PRODUCT

TOTAL

RED%

TOTAL

RED%



MEAN



MEAN



3 REP/PROD

ALKANES

28 DAYS

AROMATIC

28 DAYS



(ppm)



S (ppm)



CONTROL

31258.6

0

973

0

NUTRIENT

28251.8

0

976.6

0

PRODUCT

29548.9

0

1081.2

0

CONTROL

31401.73

0

990.5

0

NUTRIENT

20728.3

26.6

619.1

36.6

PRODUCT

12870.5

56.4

496.3

54.1

CONTROL

32465.8

0

925.7

0

NUTRIENT

1787.2

93.7

722.6

26.0

PRODUCT

1758.2

94.1

566.9

47.6

Alkanes showed significant reductions with aromatic components less dramatic but still
significant.

Results of Gravimetric Analysis:
Percentage ^

Control

o) Decrease in Weight of Oil on Day 28

Nutrient

Product (MICRO-BLAZE®^
12%

<1%	17.6%

CONCLUSIONS: The MICRO-BLAZE® EMERGENCY LIQUID SPILL CONTROL product
shows an initial rapid consumption of all measured hydrocarbons at seven (7) days. This rate
apparently slows over 28-day period in a closed environment which may be due to a change in
the environment of the flask due to the rapid degradation rates. Because of the high microbial
population at the end of the test, it is to be assumed that the quantity of metabolites might
account for the increased weight as determined by the gravimetric analysis.

Bioremediation Agents

10

MICRO-BLAZE® EMERGENCY
LIQUID SPILL CONTROL


-------
b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentage in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, salinity ranges for use of the additive:
pH: 7.5

Temperature: 45°F - 105°F
Salinity: 0-10%

3.	Minimum and maximum pH, temperature, salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: <5.9, >9.0
Temperature: <32°F, >180°F
Salinity: <0%, 10%

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Product is determined to be free of gram negative contamination.

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

11

MICRO-BLAZE® EMERGENCY
LIQUID SPILL CONTROL


-------
TECHNICAL PRODUCT BULLETIN #B-42

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JANUARY 3, 1992

REVISED LISTING DATE: FEBRUARY 5, 1997

UPDATED LISTING LETTER: OCTOBER 7, 2020

"VB591™, VB997™, BINUTRIX®"

I.	NAME, BRAND, OR TRADEMARK
VB591™, VB997™, BINUTRIX®

Type of Product: Biological Additive (patented, partial encapsulated oleophilic (oil-loving)
nutrient; a nutrient additive that contains no microorganisms)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
BioNutraTech Inc.

13647 Pemberwick Park Lane
Houston, TX 77070
Phone: (800) 567-5432
Phone: (281)354-5900
E-mail: shruza@bionutratech.com
Website: www.bionutratech.com
(Ms. Sandra L. Hruza)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
BioNutraTech Inc.

13647 Pemberwick Park Lane
Houston, TX 77070
Phone: (800) 567-5432
Phone: (281)354-5900
E-mail: shruza@bionutratech.com
Website: www.bionutratech.com
(Ms. Sandra L. Hruza)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal ventilation is adequate.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Normal precautions
and protective equipment for handling any type of powder, such as dust protectors and eye
shield. Avoid contact with eyes and do not take internally. Upon contact with eyes, flush with
water immediately for a minimum of 15 minutes. If redness or irritation continues, contact a
physician. Avoid breathing dust.

4.a.	Maximum storage temperature: >140°F
4.b. Minimum storage temperature: NA

4.c. Optimum storage temperature range: 50°F to 80°F
4.d. Temperature phase separations and chemical changes: NA

Bioremediation Agents

12

VB591™, VB997™, BINUTRIX®


-------
V.	SHELF LIFE

The shelf life is approximately three years if kept dry. Store in dry location and avoid contact
with moisture. Prolonged storage may result in the formation of soft clumps, which are easily
broken by mechanical disruption.

VI.	RECOMMENDED APPLICATION PROCEDURE

VB591™, VB997™, BINUTRIX® is a powder, and can be applied using conventional powder
spraying equipment. No pre-mixing or dilution is required.

1.	Application Method: Application for localized spills can be done using hand-held pressurized
dust blowers. For inland waterways, ship channels, marinas or coastal wetlands, large dust
blowers mounted on barges or ships can be employed to apply the product. Application by
aircraft using conventional dust spraying systems is recommended for treatment of large
uncontained spreading spills or spills in open waters or at sea.

2.	Concentration/Application Rate: Recommended initial application rate is 5 to 15 pounds of
VB591™, VB997™, BINUTRIX® per barrel of spilled oil. Follow-up applications at 48 to 72
hour intervals should be adjusted to allow for reduction in oil due to clean-up activities and
natural loss by evaporation, droplet formation and dispersion and microbial activity.

Applications should not exceed 250 pounds per acre per application.

3.	Conditions for Use: VB591™, VB997™, BINUTRIX® should be applied to spilled oil as soon
as possible following spillage to stimulate natural oil utilizing microbial populations to maximize
biodegradation activity. Application of VB591™, VB997™, BINUTRIX® to spilled oil does not
significantly alter the physical consistency of the spilled oil, and as such will not adversely affect
conventional cleanup activities, nor will conventional and removal activities adversely affect the
activity of VB591™, VB997™, BINUTRIX®. Dispose of waste in accordance with local, state,
and federal regulations. Information regarding use of VB591™, VB997™, BINUTRIX® in
conjunction with chemical dispersing agents is at present not available.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL
MEAN

RED%



3 REPS/PROD

ALKANES

(ppm)

28 DAYS

AROMATIC S
(ppm)

28 DAYS



CONTROL

31041.7

0

973.1

0

0

NUTRIENT

28251.8

0

976.6

0

VB591™,
VB997™,
BINUTRIX®

28813.8

0

932.8

0

Bioremediation Agents

13

VB591™, VB997™, BINUTRIX®


-------


CONTROL

31436.33

0

990.5

0

7

NUTRIENT

20728.3

26.6

619.1

36.6



VB591™,
VB997™,
BINUTRIX®

14637.4

49.2

733.1

21.4



CONTROL

32465.8

0

925.7

0

28

NUTRIENT

1787.2

93.7

722.6

26.0

VB591™,
VB997™,
BINUTRIX®

937.97

96.8

290.8

73.1

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

<1%	17.6%	18.0%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

VB591™, VB997™, BINUTRIX® is an oleophilic nutrient additive and contains no preserved
natural or mutated microorganisms of any type.

1.	Listing of all microorganisms by species and percentage in the composition: None

2.	Optimum pH, temperature, and salinity ranges for use of the additive: VB591™, VB997™,
BINUTRIX® may be used under any conditions where natural populations of oil-degrading
microbes are active.

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: NA

Temperature: NA
Salinity: NA

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: NA

Fecal coliform: NA
Shigella: NA

Staphylococcus coagulase positive: NA
Beta hemolytic Streptococci: NA

IX.	PHYSICAL PROPERTIES

NA

Bioremediation Agents

14

VB591™, VB997™, BINUTRIX®


-------
X. ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

15

VB591™, VB997™, BINUTRIX®


-------
LISTING CHANGES PENDING;
VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN #B-43

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 12, 1992

REVISED LISTING DATE: MARCH 21, 1997

"STEP ONE"

(aka, B&S INDUSTRIAL)

I. NAME, BRAND, OR TRADEMARK
STEP ONE

(aka, B&S INDUSTRIAL)

Type of Product: Biological Additive

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
B&S Research, Inc.

4345 Highway 21

Embarrass, MN 55732

Phone: (218) 984-3757

Fax: (218) 984-3212

E-mail: farmforprofit@frontier.com

(Mr. H. W. Lashmett)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
B&S Research, Inc.	Bioremediation International
4345 Highway 21 4345 Highway 21

Embarrass, MN 55732	Embarrass, MN 55732

Phone: (218) 984-3757	Phone: (218) 984-3757

Fax: (218) 984-3212	Fax: (218) 984-3212

E-mail: farmforprofit@frontier.com	E-mail: farmforprofit@frontier.com

(Mr. H. W. Lashmett)	(Mr. H. W. Lashmett)

Farm for Profit Research and Development

4345 Highway 21

Embarrass, MN 55732

Phone: (800) 232-7692

Fax: (218) 984-3212

E-mail: farmforprofit@frontier.com

(Mr. H. W. Lashmett)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: None

2.	Ventilation: Normal ventilation is adequate

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with

Bioremediation Agents

16

STEP-ONE


-------
skin, especially when there are open wounds. In case of skin contact, wash with soapy water.

The use of protective gloves is recommended. Avoid contact with eyes. In case of eye contact,

immediately flush eyes with plenty of water continuously for at least 15 minutes. Consult a

physician. The use of protective goggles is recommended. Avoid inhalation and ingestion. It is

recommended that workers wear dust mask and not eat or smoke while handling the product(s).

4.a. Maximum storage temperature: 90°F

4.b. Minimum storage temperature: -30°F

4.c. Optimum storage temperature range: 32°F to 70°F

4.d. Temperature phase separations and chemical changes: NA

V.	SHELF LIFE
Over 3 years

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Components of the product STEP ONE (BC101) and STEP ONE
(MSE2.5) are only sold together. B&S Research will make application recommendations based
on contamination and ppm of contamination at time of purchase order and employ specified
application methods (spray, plowing, agitation, etc.) appropriate for a particular situation.

2.	Concentration/Application Rate: Nominally, the STEP ONE water mixture can be used on
most hydrocarbons, including crude and refined petroleum products, pesticides, etc., on land,
fresh water or ocean water. Laboratory tests also indicate effectiveness in destruction of PCB's.
In certain circumstances, B&S Research, Inc. may require laboratory soil and water
contamination tests before the product may be used (see VI1. above).

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED %

TOTAL MEAN

RED %





MEAN









3 REPS/PROD.

ALKANES

28 DAYS

AROMATIC S

28 DAYS





(ppm)



(ppm)



0

CONTROL

29959.5



5391.8





NUTRIENT

29008.5



5163.0





STEP ONE

30477.8



5499.8



7

CONTROL

33471.3



5720.9





NUTRIENT

22723.7



5050.1





STEP ONE

24196.8



3110.2



28

CONTROL

30997.4

0.0 %

5388.9

0.0 %



NUTRIENT

1103.9

96.19%

4582.4

11.23%

Bioremediation Agents

17

STEP-ONE


-------
DAYS

PRODUCT

TOTAL
MEAN

RED %

TOTAL MEAN

RED %



3 REPS/PROD.

ALKANES
(ppm)

28 DAYS

AROMATIC S
(ppm)

28 DAYS



STEP ONE

17059.4

44.03%

2501.9

54.51%

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product (STEP ONE)

0%	19%	51%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6-8

Temperature: 70°F to 90°F

Salinity: Fresh or salt (ocean <110 ppm) water, land or dry surfaces

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: <5 or <9, (apply neutralizing agents — lime or P205
Temperature: <50°F or>135°F
Salinity: <0 or >110 ppm

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: -7°F

3.	Viscosity: 2.8 cSt @ 50°F
3.5 cSt @ 32°F

5.9 cSt @ -4°F

4.	Specific Gravity: 1.03 @ 59°F

5.	pH: 7.2 (1:2.5:80 BC101:MSE2.5:water mixture)

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: Noedal

8.	Solvents: None

Bioremediation Agents

18

STEP-ONE


-------
9.	Additives: Phosphoric acid as P205
3% emulsifier <.5% by weight

10.	Solubility: Infinite

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration

Arsenic	<0.0200

Cadmium	<0.0030

Chromium	0.0859

Copper	0.0177

Lead	0.0090

Mercury	0.0002

Nickel	<0.0080

Zinc	0.0602

Cyanide	0.2830

Chlorinated Hydrocarbons	<0.0050

Bioremediation Agents

19

STEP-ONE


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

8/09/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #B-45

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JANUARY 28, 1993

REVISED LISTING DATE: NOVEMBER 14, 1995

"SYSTEM E.T. 20"

I.	NAME, BRAND, OR TRADEMARK
SYSTEM E.T. 20

Type of Product: Biological Additive
(formerly MCW.B 20)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Environmental Restoration Services

9211 Lakewood Drive
Windsor, CA 95492
E-mail: ERS,BTI@gmail.com
Phone: (619) 253-0664
(Mr. John Chase)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Environmental Restoration Services

14384 Highland Valley Road
Escondido, CA 92025
E-mail: ERS,BTI@gmail.com
Phone: (619) 253-0664
(Mr. John Chase)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: SYSTEM E. T. 20 is non-flammable

2.	Ventilation: No special ventilation is required under normal use.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In its primary form, no
special handling or storage is required. Avoid excessive inhalation, and protect the nose and
mouth with a dust protection mask. Wear protective gloves, and wash hands with soap and water
after handling the product.

4.a.	Maximum storage temperature:

4.b. Minimum storage temperature:

4.c. Optimum storage temperature range: 4°C - 20°C (39°F - 68°F). Place in a dry area, shaded
from sunlight.

4.d. Temperatures of phase separations and chemical changes: NA

V. SHELF LIFE

2 years if maintained at 4°C (39°F).

Bioremediation Agents

20

SYSTEM E.T. 20


-------
VI.	RECOMMENDED APPLICATION PROCEDURE

SYSTEM E. T. 20 can be used on a broad range of hydrocarbon compounds (including PAH's)
found in open and closed water systems (salt or fresh) or in soil (beach, sands, or inland soil
types). SYSTEM E.T. 20 protocols can be used with indigenous and introduced bacteria.
SYSTEM E.T. 20 is an oleophilic, non-water soluble nutrient, which releases nitrogen and
phosphorous enzymatically, thus allowing SYSTEM E.T. 20 to be used in water and soil
applications including: conditions requiring fast degradation rates due to regulations, limited
space or cost; under conditions where weathered or heavy oils, sludges or PAH's exist that
require consistently high populations of hydrocarbon degrading bacteria to metabolize these long
or more complex carbon chains; tropical or sub-tropical conditions that support large,
indigenous, non-beneficial bacterial populations that would otherwise dilute the effectiveness of
standard bioaugmentation approaches; aqueous conditions in which soluble or time release
nutrient compounds would be washed away or diluted, i.e., beaches, frequent rains, floods,
streams, stream banks, estuaries and areas affected by tides; sensitive environmental conditions
that demand low or no toxicity; toxicity in soil or water during bioremediation may be stimulated
by adding broadly available nutrients which may activate disease carrying bacilli or pathogens;
controlled nutrient release to SYSTEM E. T. 20 bacteria prevents over-nitrification; conditions
requiring the elimination of oil discoloration caused by the presence of polar fractions; and
conditions where salt water conditions exist or where only salt water is available for bacteria
application.

1.	Application Methods:

Biopile	Land farm	Pump and Treat

Bioreactor	Bio slurry

In situ	Windrow

Topical application to discolored rocks or soil.

Topical application to beaches.

2.	Concentration/Application Rate: Concentration and rate of application will vary from site to
site depending upon the type of contaminant and the area contaminated. Contact QET for
specific information.

3.	Conditions for Use: Before applying SYSTEM E. T. 20, QET recommends that the site be
evaluated for its physical and chemical soil characteristics (i.e., pH, salinity, conductivity,
physical parameters, moisture content, hydrocarbon type and concentration, nitrogen content,
etc.), and toxicity of both the soil and the contaminant, by biological screening tests.

Basic biological requirements of SYSTEM E. T. 20, site conditions and SYSTEM E. T. 20
capabilities dictate the appropriate procedures for application of SYSTEM E. T. 20.

Biological requirements for SYSTEM E. T. 20 bacteria are nutrients, adequate oxygen supply,
hydrocarbon food source, neutral pH and a 15% minimum moisture level for soil remediation
applications.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

Bioremediation Agents

21

SYSTEM E.T. 20


-------
DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28 DAYS

AROMATIC

28 DAYS





(ppm)



S (ppm)





CONTROL

29959.5

0

5391.8

0

0

NUTRIENT

29008.5

0

5163.0

0

SYSTEM E.T. 20

30476.1

0

5311.3

0



CONTROL

33471.3

0

5720.9

0

7

NUTRIENT

22723.7

0

5050.1

0



SYSTEM E.T. 20

3837.1

0

2928.8

0



CONTROL

30997.4

0

5383.9

0.2

28

NUTRIENT

1103.9

96.2

4582.4

11.2

SYSTEM E.T. 20

261.9

99.1

1188.0

77.0

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product (SYSTEM E.T. 20)

0%	19%	18%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentage in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.5, (6.5 to 8.5)

Temperature: 4°C to 35°C (39°F to 95°F)

Salinity: Fresh to 2.5% (average ocean salt level)

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: <6.5 and >8.5

Temperature: <5°C and >35°C (<41°F and >95°F)

Salinity: >3%

4.	Special nutrient requirements: Recommendation is for a non-soluble nutrient. The specific
types of nutrients will be dependent on the site requirements.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Bioremediation Agents

22

SYSTEM E.T. 20


-------
Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

23

SYSTEM E.T. 20


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

5/18/2006
7/27/2022

TECHNICAL PRODUCT BULLETIN #B-48

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 10, 1993

REVISED LISTING DATE: AUGUST 31, 2000

"BET BIOPETRO"

I.	NAME, BRAND, OR TRADEMARK
BET BIOPETRO

Type of Product: Biological Additive
(formerly BET BIOPETRO HEAVY)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
BioEnviroTech

ADDRESS: updated information required
PHONE: updated information required
(Mr. Warren Butler)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
BioEnviroTech

ADDRESS: updated information required
PHONE: updated information required
(Mr. Warren Butler)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable

2.	Ventilation: Normal ventilation

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye and skin
contact. In case of eye contact, flush eyes with water or eyewash, and refrain from rubbing. For
skin contact, wash with mild soap and apply hand cream if itching or redness occurs. Avoid
inhalation. In case of inhalation, seek fresh air. Repeated inhalation has been associated with
respiratory allergy in some persons. Such allergic individuals should wear protective clothing
and eye goggles. In enclosed buildings, workers should wear single use nuisance dust masks
appropriate for fine particulate dust. In outdoor field applications, no dust mask is required.

4.a.	Maximum storage temperature: 105°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 50°F to 75°F

4.d. Temperatures of phase separations and chemical changes: NA

Bioremediation Agents

24

BET BIOPETRO


-------
V. SHELF LIFE

More than 3 years in unopened original shipping container, stored in cool dry area.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: BET BIOPETRO is a powder containing granules of bacterial product
formulated to provide performance in the bioremediation of heavy refined and crude
hydrocarbon contaminants in both soil and water environments.

Application procedure and treatment schedule will vary with specific environmental conditions
and bioremediation requirements. Contact BET for specific technical advice.

2.	Concentration/Application Rate: Dosage will vary with specific environmental conditions and
bioremediation requirements. Contact BET for specific technical advice.

3.	Conditions for Use: BET BIOPETRO should be used at temperatures in the range of 45°F to
100°F, pH range of 5.5 to 8.5, and dissolved oxygen level of 3 to 5 mg/1. The product is
effective in both salt and fresh waters. However, where extreme salinity is projected, testing and
evaluation of the bacteria in bioremediation are advised. BET BIOPETRO cultures exhibit some
resistance to toxic shocks from strong chemicals. Nonetheless, highly chlorinated compounds,
acids, caustics, disinfectants, germicides, and chlorine will render the cultures ineffective, just
like other bacteria. Where such chemicals are anticipated, testing and evaluation of the bacteria
in bioremediation are advised.

BET BIOPETRO cultures require supplemental nutrients for optimum performance (See section
VIII. 4).

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28 DAYS

AROMATIC S

28





(ppm)



(ppm)

DAYS



CONTROL

29965.2

0

5620.5

0

0

NUTRIENT

31494.8

0

6660.2

0

BET BIOPETRO

25914.5

0

5569.1

0



CONTROL

30101.5

0

5610.1

0

7

NUTRIENT

8073.9

0

5086.6

0



BET BIOPETRO

373.0

0

1220.0

0



CONTROL

28785.6

4.0

5512.7

2.0



NUTRIENT

706.2

98.0

4863.7

27.0

Bioremediation Agents

25

BET BIOPETRO


-------
DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28 DAYS

AROMATIC S

28

28



(ppm)



(ppm)

DAYS

BET BIOPETRO

350.3

99.0

1882.9

67.0

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product (BET BIOPETRO)

0%	51%	30%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentage in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive
pH: 6.6 to 7.4

Temperature: 70°F to 95°F
Salinity: Fresh to Salt water

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity.

pH: <5.5 and >8.5
Temperature: <45°F and >105°F
Salinity: Extreme salinity

4.	Special nutrient requirements: BioEnviroTech, Inc. recommends nutrient supplements for
optimum performance of the product in bioremediation application. The required nutrients are
dependent upon hydrocarbon contamination levels. Contact BET for specific nutrient dosing
requirements.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS OF HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

26

BET BIOPETRO


-------
TECHNICAL PRODUCT BULLETIN #B-53

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 26, 1996

REMOVAL DATE: AUGUST 16, 2005

RELISTING DATE: SEPTEMBER 18, 2009

"OIL SPILL EATER II (OSE II)"

I.	NAME, BRAND, OR TRADEMARK
OIL SPILL EATER II (OSE II)

Type of Product: Bioremediation Agent (Biological Enzyme Additive [previously listed as a
Nutrient Additive])

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
OSEI Corporation (Formerly Sky Blue Chems)

P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Website: www.osei.us

(Mr. Steven Pedigo, Chairman, CEO, Inventor)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
OSEI Corporation (Formerly Sky Blue Chems)

P.O. Box 515429
Dallas, TX 75251-5429
Phone: (972) 669-3390
E-mail: oseicorp@msn.com
Website: www.osei.us

(Mr. Steven Pedigo, Chairman, CEO, Inventor)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Water-based, non-flammable

2.	Ventilation: Needs no ventilation; aqueous-based product; does not emit hazardous vapors

3.	Skin and eye contact; protective clothing; treatment in case of contact: OSE II is not a primary
dermal irritant. Avoid eye contact, and wear goggles if possible for the spray to come in direct
contact with eyes. Facilities for quick and copious eye flushing should be provided and prompt
medical attention should be sought if exposure and irritation persists. Protective rubber gloves
are suggested during handling. Before mixing the product has a smell of fermentation. The
product does not give off any harmful vapors.

4.a.	Maximum storage temperature: 120°F

4.b. Minimum storage temperature: None; OSE II can freeze and thaw without adverse effects

4.c. Optimum storage temperature range: 72°F

4.d. Temperatures of phase separations and chemical changes: 120°F

Bioremediation Agents

27

OIL SPILL EATER II (OSE II)


-------
V.	SHELF LIFE

OSE II has a recommended shelf life of 5 years. After 5 years at optimum storage temperature,
there is an approximate 10% decrease per year in product capability.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method:

A.	Use surface spray apparatus, such as small hand held tanks, back pack, large mixing tanks
with mechanical pumping devices, vessels with booms for spraying wide paths, or spray
devices on airplanes or helicopters.

B.	OSE II can be applied by eductor systems from vessels, fire trucks, etc. Set the eductor
system to 2% and apply 1 gallon of mixed OSE II to each spilled gallon of hydrocarbon.

2.	Concentration/Application Rate:

General - OSE II generally takes 3 to 30 minutes to penetrate the molecular walls of
hydrocarbons. However, once you spray OSE II on the hydrocarbons, OSE II attaches itself and
will eventually engulf the hydrocarbons regardless of where the hydrocarbons may spread on the
surface of salt or fresh water. Additionally, once you spray OSE II, the hydrocarbons cannot
attach itself to the shoreline, rocks, or any equipment in its path. OSE II breaks down the
adhesion properties of hydrocarbons and causes hydrocarbons to float, thereby, eliminating
secondary contamination of the water column or any other areas, and holding the contaminated
area to the water's surface, the original contaminated area.

•	If OSE II is to be used on ocean spills or on intertidal zones OSE II should be mixed with
ocean water.

•	If OSE II is to be used on lakes, rivers, streams, ponds, or on land mix the product with water
from a lake, stream, or pond.

•	If you are performing a cleanup, make sure the water used to mix with OSE II, and the water
used to keep the area saturated, is the type of water normally associated with that area.

•	If you use fresh water in an area normally contacted with salt water or vice versa, the
different types of bacteria and competition could occur, not to mention the problems with
salinity for fresh water organisms.

[Note: Do not mix tap water with OSE II if possible: Chlorine in tap water slows bacterial
enhancement]

Spills on Water:

Dilute each gallon of OSE II with 50 gallons of fresh, brackish, or salt water - depending on the
water associated with the area that has been impacted by the spill. Apply OSE II at a ratio of 1
gallon mixed OSE II to each gallon of hydrocarbon spilled. Apply using hand held sprayers, tank
sprayers, booms from vessels, helicopters, or airplanes; by spraying the perimeter first then
working toward the middle of the spilled area. Next spray the entire surface of the spill. If the
spill is very heavy (more than 2 inches thick) it is recommended that OSE II be applied every
day until you have met a 1:1 ratio of OSE II and water mixture to spilled oil/hydrocarbons.

•	Use 1 gallon OSE II for every 50 gallons of hydrocarbons.

•	Use 1 drum of OSE II for every 2,750 gallons of hydrocarbons.

•	If you know gallons of hydrocarbons spilled, multiply gallons of hydrocarbons by 0.02 to get
amount of OSE II needed [gallons of hydrocarbons x 0.02 = gallons of OSE II],

•	If you know barrels of crude oil spilled, multiply barrels of crude oil by 0.015 toO get drums

Bioremediation Agents

28

OIL SPILL EATER II (OSE II)


-------
of OSEII needed [barrels of crude oil x 0.015 = drums of OSEII],

•	If you do not know gallons of hydrocarbons or barrels of crude oil, multiply size of spill by
0.0023 to get drums of OSE II needed or by 0.12 to get gallons of OSE II needed [(yards
long x yards wide x inches thick) x 0.0.0023 = drums of OSE II or (yards long x yards wide x
inches thick) x 0.015 = gallons of OSE II],

Intertidal Zone:

Mix each 55 gallon drum of OSE II with 2,750 gallons of fresh, brackish, or salt water. The
water used is determined by the type of water associated with the site. OSE II should be applied
as the tide recedes (if there is a tide) and once the tide comes in the application should cease until
the tide recedes again. Additional applications should only be warranted if spill has been allowed
time to percolate into the depths of the soil.

If there is no tide, but waves have pushed the spill into the intertidal zone, then there will be
direct access to the spill at all times. If possible use string or stakes to grid off the beach or
intertidal zone area, and then you can calculate how much premixed OSE II to apply to a given
area. If unable to grid off an area then calculate how much OSE II to apply and then determine
how much premixed OSE II will flow through a nozzle (gallons per minute) then let application
technician know how many gallons to apply in a given area and this can be determined by
applying product for a certain time period to get the correct amount of OSE II applied to gain the
1:1 ratio.

Note: If the intertidal zone is associated with the sea then mix OSE II with salt water. If the spill
area is in an area of brackish water then mix OSE II with brackish water. If the intertidal zone is
associated with fresh water such as lakes, rivers, streams, ponds, creeks, aquifers, or drinking
water wells then use fresh water to mix OSE II.

3. Conditions for Use:

•	OSE II can remediate hydrocarbon-based material including chlorinated hydrocarbons,
PCB's, dioxins, and some pesticides.

•	As the age of spilled hydrocarbons increases, the time necessary for bioremediation
increases. In general, fresh crude, gasoline of BTEX takes from 72 hours to 30 days to
completely bioremediate.

•	Variations of sea water salinity should have no effect, but as long as microbial life can exist,
then OSE II will be effective.

•	OSE II bioremediation slows somewhat at temperatures below 40°F. OSE II however, will
continue to work at any liquid water temperature that will sustain microbial life.

Bioremediation Agents

29

OIL SPILL EATER II (OSE II)


-------
VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Summary Data Table	

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

43,170

-

11,435

-

0

NUTRIENT

40,569

-

11,785

-



OSE II

41,730

-

12,155

-



CONTROL

39,250

9.1

10,355

9.4

7

NUTRIENT

34,815

14.2

9,898

16.0



OSE II

26,316

36.9

8,072

33.6



CONTROL

35,797

17.1

9,534

16.6

28

NUTRIENT

26,507

34.7

8,938

24.2



OSE II

4,273

89.8

1,268

89.6

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product

16.5%	52.0%	85.4%

b. Toxicity: NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of each component of the total formulation, other than enzymes, by chemical name
and percentage by weight: CONFIDENTIAL

2.	Enzyme Names: CONFIDENTIAL

3.	I.U.B.: CONFIDENTIAL

4.	Source of Enzymes: Fermentation process

5.	Units: No less than 1% and no more than 50% by weight

6.	Specific Gravity: 1.05

7.	Optimum Conditions:

a.	pH: 7.0

b.	Temperature: 72°F

c.	Salinity Ranges: Fresh water to salt water

d.	Maximum and Minimum pH: 3.5-8.0

e.	Maximum and Minimum Temperature: 28°F - 128°F

Bioremediation Agents

30

OIL SPILL EATER II (OSE II)


-------
f.	Maximum and Minimum Salinity Levels - Salinity level above that will support
microbial activity will adversely affect OSE II's performance

g.	Enzyme Shelf Life: Up to 5 years when properly stored

h.	Enzyme Optimal Storage Conditions: 72°F is optimal, enzyme range is freezing to
120°F, never leave OSE II in direct sunlight for more than a couple of hours

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

31

OIL SPILL EATER II (OSE II)


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN B-55
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: SEPTEMBER 10, 1999
"LAND AND SEA RESTORATION PRODUCT 001 (VELITE)"

I.	NAME, BRAND, OR TRADEMARK
LAND AND SEA RESTORATION PRODUCT 001 (VELITE)

Type of Product: Bioremediation Agent (Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Land and Sea Restoration LLC

ADDRESS: updated information required
PHONE: updated information required
(Mr. T. Shawn Parker)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Land and Sea Restoration LLC

ADDRESS: updated information required
PHONE: updated information required
(Mr. T. Shawn Parker)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Flash Point 250°C (482°F)

2.	Ventilation: Normal ventilation

3.	Skin and eye contact; protective clothing; treatment in case of contact: Protective clothing and
glasses. In case of eye contact, flush eyes with water or eyewash and refrain from rubbing. For
skin contact, wash with mild soap and apply cream if itching or redness occurs. Avoid
inhalation. In case of inhalation, seek fresh air. Wear protective clothing and eye goggles.
Workers should wear single use nuisance dust masks appropriate for fine particulate dust.

4.a.	Maximum storage temperature: 65°C (150°F)

4.b. Minimum storage temperature: 0°C (32°F)

4.c. Optimum storage temperature range: 0°C to 65°C (32 to 150°F)

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

More than 5 years in unopened original shipping container, store in a cool, dry place. Avoid
moisture prior to use.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: On water, spread over contaminated area at 1 to 3 ratios. On soil, blend
to depth equivalent to contamination level. On hard surfaces, spread over contaminated area.

4/02/2007
7/27/2022

Bioremediation Agents

32

LAND AND SEA RESTORATION
PRODUCT 001 (VELITE)


-------
Make sure the spill is completely absorbed. For best results agitate with broom. (Will not
damage cured asphalt if used as an absorbent for spills.) Remove and dispose of in accordance
with all state and federal laws, after absorption is complete.

2.	Concentration/Application Rate:

1 part 001 to 3 parts hydrocarbon.

3.	Conditions for Use:

NA

VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

13.8239

0

0.0443

0

0

001

13.5856

0

0.0509

0



CONTROL

14.3292

0

0.0473

0

7

001

10.1005

29.52

0.0437

0



CONTROL

14.4675

0

0.0401

0

28













001

8.2629

42.92

0.0273

31.92

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Product (001)

0%	25.18%

b. Toxicity: NA

VIII. MICROBIOLOGICAL ANALYSIS

1. Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2. Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6 to 8

Temperature: 25°C to 30°C (77°F to 86°F)

Salinity: Fresh to salt water

Bioremediation Agents

33

LAND AND SEA RESTORATION
PRODUCT 001 (VELITE)


-------
3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: NA

Temperature: NA
Salinity: NA

4.	Special nutrient requirements: The product "001" is a nutrient, therefore no nutrients are
required.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: <3
Shigella: Negative

Staphylococcus Coagulase positive: <10
Beta hemolytic Streptococci: 1,100

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 250°C (482°F)

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: NA

5.	pH: NA

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: NA

9.	Solubility in Water: NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

34

LAND AND SEA RESTORATION
PRODUCT 001 (VELITE)


-------
TECHNICAL PRODUCT BULLETIN B-56

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JULY 24, 2002

"S-200C"

I.	NAME, BRAND, OR TRADEMARK
S-200C

Type of Product: Bioremediation Agent (Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
RBL Environmental, LLC*

1311 Dorothy Avenue
Phoenixville, PA 19460
Phone: (610) 520-7665
E-mail: iim.lynn@iepusa.com
(Mr. James Lynn)

(*RBL Environmental, LLC is the manufacturer and marketer for International Environmental
Products)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
RBL Environmental, LLC

1311 Dorothy Avenue
Phoenixville, PA 19460
Phone: (610) 520-7665
E-mail: iim.lynn@iepusa.com
(Mr. James Lynn)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Ventilation of the work place is not necessary.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of contact with
skin or eyes, wash with plenty of water.

4.a.	Maximum storage temperature: 132°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 55°F - 85°F

4.d. Temperatures of phase separations and chemical changes: <32°F and >140°F

V.	SHELF LIFE

The recommended shelf life of S-200C is 10 years if kept in the unopened, original container.

Bioremediation Agents

35

S-200C


-------
VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: S-200C is a light amber liquid, and as such can be sprayed with
traditional liquid spraying equipment, such as pressurized sprayers or backpack sprayers.

2.	Concentration/Application Rate: The recommended application rate is approximately 10% by
of the S-200C as compared to the hydrocarbon being remediated. In other words, use 1 pound of
S-200C for every 10 pounds of hydrocarbon you are remediating. For applications on soil
contaminated below 1 foot, the soil is turned and the material is applied. This allows air to
circulate and thereby maintains an aerobic condition. On a surface application, the amount to use
is approximately 0.1 to 1 pound of S-200C for every square yard of surface area. The amount
sprayed is dependent on the amount of hydrocarbon on the surface you are spraying.

To remediate a sheen on water, the same application ratio for a surface application is used.

3.	Conditions for Use: S-200C is a bioremediation accelerator used for the remediation of
hydrocarbon spills or leaks. It is a non-intrusive, cost effective remedy for the cleanup of these
hydrocarbons. These hydrocarbons include but are not limited to gasoline, No. 2 up to No. 6
diesel fuel, jet fuels, kerosene, lubricating oils, hydraulic oils, and crude oils.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

27666

0

5600

0

0

S-200C

29333

0

5666

0



CONTROL

21333

0

4333

0

7

S-200C

11000

0

4400

0



CONTROL

18771

32

5597

0.05

28













S-200C

660

98

5073

10.4

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Product (001)

-18.57%	27.82%

Bioremediation Agents

36

S-200C


-------
b. Toxicity:
Material Tested
S-200C

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Mysidopsis bahia

Species

LC50 (ppm)
39.69 96-hr
21.33 48-hr
35.36 96-hr
35.36 48-hr
25.33 96-hr
17.67 48-hr
22.96 48-hr

No. 2 Fuel Oil

S-200C & No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:

S-200C is a nutrient bioremediation accelerator and does not contain bacterial cultures or
amendments. However, with the addition of S-200C, the microbiological data shows a continued
viability of microbial incubations over time.

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.0

Temperature: 86°F
Salinity: Fresh to salt water

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 4.5 - 10.0
Temperature: 50°F - 120°F
Salinity: 0% - 10%

4.	Special nutrient requirements: NA

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 40°F

3.	Viscosity: 100cp@70°F

4.	Specific Gravity: 0.996

5.	pH: 4.5

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: NA

9.	Solubility in Water: Dispersible

Bioremediation Agents

37

S-200C


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

S-200C does not contain any heavy metals, cyanide, or chlorinated hydrocarbons.

Bioremediation Agents

38

S-200C


-------
TECHNICAL PRODUCT BULLETIN B-57

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JANUARY 8, 2007

"SPILLREMED (MARINE)®"

(aka, AGROREMED, HYDROREMED, SPILLREMED (INDUSTRIAL), VAPORREMED)

I.	NAME, BRAND, OR TRADEMARK
SPILLREMED (MARINE)®

(aka, AGROREMED, HYDROREMED, SPILLREMED (INDUSTRIAL), VAPORREMED)
Type of Product: Bioremediation Agent (Biological Additive: Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Sarva Bio Remed, LLC

25 Marianne Drive, Suite 'B'

York, PA 17406
Phone: (717) 779-0040
Phone: (877) 717-2782
E-mail: sales@sarvabioremed.com
Website: www.sarvabioremed.com
(Mr. Satya Ganti)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Sarva Bio Remed, LLC

25 Marianne Drive, Suite 'B'

York, PA 17406
Phone: (717) 779-0040
Phone : (877) 717-2782
E-mail: sales@sarvabioremed.com
Website: www.sarvabioremed.com
(Mr. Satya Ganti)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: No special ventilation required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: On contact with
product, wash with plenty of water and for eye contact consult your physician. Use of gloves
and eye protection is recommended during field application to protect eyes from spray.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: Ambient

4.d. Temperatures of phase separations and chemical changes: <32°F and >100°F

Bioremediation Agents

39

SPILLREMED (MARINE)®


-------
V.	SHELF LIFE

The recommended shelf life is one year.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method:

SPILLREMED (MARINE)® is a ready to use liquid product. It can be sprayed undiluted over
the spill in open water conditions.

2.	Concentration/Application Rate:

SPILLREMED (MARINE)® is applied in a product to oil ratio of 1:10. Rate of application is
one gallon per 10 minutes.

3.	Conditions for Use:

SPILLREMED (MARINE)® is a marine salt formulation and is not effective in fresh water
conditions. Optimal effectiveness is in the salinity range of 10 to 35 ppt.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL
MEAN

RED%



3 REPS/PROD

ALKANES

(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS



CONTROL

48,963.31



13,467.59



0

NUTRIENT

SPILLREMED
(MARINE)®

CONTROL

46,963.33
52,063.18

47,606.78



13,779.24
14,143.06

11,262.98



7

NUTRIENT

SPILLREMED
(MARINE)®

40,853.28
43,236.67



11,329.01
11,076.99





CONTROL

45,467.28

7

12,560.37

7

28

NUTRIENT

7,210.06

98

9,927.87

28

SPILLREMED
(MARINE)®

1,310.09

97

7,442.71

47

Bioremediation Agents

40

SPILLREMED (MARINE)®


-------
Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control
6.00%

Nutrient
76%

Product

85%

b. Toxicity:

Material Tested
SPILLREMED (MARINE)®

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
392.30 96-hr
343.80 48-hr
40.50 96-hr
17.40 48-hr
37.50 96-hr
22.40 48-hr
8.00 96-hr
15.90 48-hr

No. 2 Fuel Oil

SPILLREMED (MARINE)®
& No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.6

Temperature: 55°F
Salinity: 30 ppt

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 6.5-6.9

Temperature: 40°F - 90°F
Salinity: 10 ppt - 35 ppt

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

41

SPILLREMED (MARINE)®


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/22/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN B-58

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: DECEMBER 3, 2007

"JE1058BS"

I.	NAME, BRAND, OR TRADEMARK
JE1058BS

Type of Product: Bioremediation Agent (Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Japan Energy Corporation

Business Development Department, Bio Research Center
3-17-35 Niizo-Minami
Toda-shi, Saitama 335-8502
Japan

Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Hisashi Saeki)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Japan Energy Corporation

Business Development Department, Bio Research Center
3-17-35 Niizo-Minami
Toda-shi, Saitama 335-8502
Japan

Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Hisashi Saeki)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Use adequate ventilation. Treat product as a hygroscopic powder.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
eyes and do not take internally. Upon contact with eyes, flush with plenty of fresh water. Avoid
breathing dust. Normal protective equipment for handling of powder, such as a dust mask and
eye shield can be used.

4.a.	Maximum storage temperature: 105°F
4.b. Minimum storage temperature: NA

4.c. Optimum storage temperature range: 0°F - 68°F

4.d. Temperatures of phase separations and chemical changes: NA

Bioremediation Agents

42

JE1058BS


-------
V.	SHELF LIFE

The shelf life of the product is approximately 2 years if stored in a cool dry area.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method:

JE1058BS contains biosurfactant and has an ability to stimulate the biodegradation of oil by
indigenous microorganisms. JE1058BS, which is a powder, can be applied using conventional
spraying equipment, for example a powder mist duster attached with boom type multi-hole head.

2.	Concentration/Application Rate:

JE1058BS is applied in a product:oil ratio of 1:10. No pre-mixing or dilution by water is
required.

3.	Conditions for Use:

JE1058BS may be used in a wide range of environmental conditions of temperature and salinities
where natural populations of oil-degrading microbes are active. The mechanical removal of as
much oil as possible should be done before the product is introduced to the slick.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

48,213



11,413



0

NUTRIENT

51,833



13,056





JE1058BS

52,280



13,211





CONTROL

48,030



11,108



7

NUTRIENT

33,423



11,755





JE1058BS

13,453



10,188





CONTROL

48,257

0

10,429

8.6

28

NUTRIENT

16,953

67.3

11,837

9.3



JE1058BS

3,854

92.6

8,061

39.0

Bioremediation Agents

43

JE1058BS


-------
Results of Gravimetric Analysis: DATA MISSING
Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

5.9%	60.0%	81.8%

b. Toxicity:

Material Tested	Species	LC50 (ppm)

JE1058BS	Menidia beryllina	91.70 96-hr

Mysidopsis bahia	72.09 48-hr

No. 2 Fuel Oil	Menidia beryllina	5.56 96-hr

Mysidopsis bahia	2.19 48-hr

JE1058BS &No. 2 Fuel Oil (1:10) Menidia beryllina	8.68 96-hr

Mysidopsis bahia	2.44 48-hr

Reference Toxicant (SLS)	Menidia beryllina	12.23 96-hr

Mysidopsis bahia	11.70 48-hr

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive: NA

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

Store in dry location and avoid contact with moisture

4.	Special nutrient requirements: NA

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX. PHYSICAL PROPERTIES

NA

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

44

JE1058BS


-------
TECHNICAL PRODUCT BULLETIN B-59

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 24, 2008

"BIOWORLD BIOREMEDIATION TREATMENT PRODUCTS (BIOWORLD BHTP)"

I.	NAME, BRAND, OR TRADEMARK

BIOWORLD BIOREMEDIATION TREATMENT PRODUCTS (BIOWORLD BHTP)

Type of Product: Bioremediation Agent (Microbiological Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
BioWorld USA, Inc.

6734B W Pershing Ave

Visalia, CA 93291

Phone: (559) 651-2042

Fax:(559)651-9041

E-mail: support@bioworldusa.com

Website: www.bioworldusa.com

(Ms. Diane R. Barnes)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
BioWorld USA, Inc.

6734B W Pershing Ave

Visalia, CA 93291

Phone: (559) 651-2042

Fax:(559)651-9041

E-mail: support@bioworldusa.com

Website: www.bioworldusa.com

(Mr. Donald E. Damschen)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-hazardous.

2.	Ventilation: Use adequate ventilation. Treat dry product as a hygroscopic powder and avoid
ventilation.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
eyes and do not take internally. Upon contact with eyes, flush with plenty of fresh water. Avoid
breathing dust. Normal protective equipment for handling of powder, such as a dust mask and
eye shield are recommended to be used. Wash hands and body contacted areas with soap and
water.

4.a.	Maximum storage temperature: 110°F

4.b. Minimum storage temperature: 34°F - containers may break if frozen
4.c. Optimum storage temperature range: 34°F - 90°F

4.d. Temperatures of phase separations and chemical changes: <32°F and > 140°F

Bioremediation Agents

45

(BIOWORLD BHTP)


-------
V.	SHELF LIFE

The recommended shelf life exceeds 3 years when stored properly in cool, dry place out of direct
sun light.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method:

BioWorld BHTP is a two part product 1) Bioremediation Enhancer liquid and 2) Hydrocarbon
Digesting Microbes in a dry form. Prior to use the microbes are rehydrated in 100°F water for
10 to 300 minutes.

Example for small volume applications - best results are obtained by applying Bioremediation
Enhancer first followed by the rehydrated Hydrocarbon Microbe solution in the same location.
Example for large volume applications - the two parts of BioWorld BHTP can be mixed with
additional water and applied together to spray over the perimeter and over the top of the spill.
Example for soil and groundwater applications - evenly apply to soils and mix with till or
discing equipment. Oxygen additions are periodically used in certain situations and can be
applied with mechanical generation and/or by using oxygen release compound products.

2.	Concentration/Application Rate:

BioWorld BHTP is applied at an approximate rate of 40 gallons Bioremediation Enhancer liquid
and 4 pounds Hydrocarbon Microbes per surface acre treated. Increased quantities and multiple
applications may be required to meet shorter cleanup time constraints and desired results.

3.	Conditions for Use:

BioWorld BHTP can be used in freshwater conditions, wetlands, rock or sand shorelines,
contaminated soil areas, salt marshes and salt water conditions (up to 60 ppt salinity).

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

61,234



9,395



0

NUTRIENT

64,803



8,873





BioWorld BHTP

63,192



9,220





CONTROL

57,907

5

7,290

22

7

NUTRIENT

49,747

14

5,956

18



BioWorld BHTP

41,480

28

4,405

40

Bioremediation Agents

46

(BIOWORLD BHTP)


-------
CONTROL

49,364 19

6,499

31

28 NUTRIENT

21,490 67

5,259

41

BioWorld BHTP

1,948 97

1,078

88

Results of Gravimetric Analysis:







Percentage (%) Decrease in Weight of Oil on Day 28





Control

Nutrient

Product



21%

64%

96%



b. Toxicity:







Material Tested

Species

LC50 (DDm)



BioWorld BHTP

Menidia beryllina

8,848.70 96-hr





Mysidopsis bahia

7,348.70 48-hr



No. 2 Fuel Oil

Menidia beryllina

4.50 96-hr





Mysidopsis bahia

3.21 48-hr



BioWorld BHTP &

Menidia beryllina

13.90 96-hr



No. 2 Fuel Oil (1:10)

Mysidopsis bahia

7.10 48-hr



Reference Toxicant (SLS)

Menidia beryllina

15.00 96-hr





Mysidopsis bahia

15.90 48-hr



VIII. MICROBIOLOGICAL ANALYSIS





1. Listing of all microorganisms by species and percentages

in the composition:



CONFIDENTIAL







2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6-8

Temperature: 80°F-100°F
Salinity: 0-1 for use of the additive

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 3-10

Temperature: 33°F-120°F
Salinity: >5

Use under any conditions where indigenous populations of oil-degrading microbes are/are not
present

4.	Special nutrient requirements: Some sites may benefit with various nutrients added depending
on project variables

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: <2
Shigella: Negative

Staphylococcus Coagulase positive: <10
Beta hemolytic Streptococci: <10

Bioremediation Agents

47

(BIOWORLD BHTP)


-------
IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

48

(BIOWORLD BHTP)


-------
TECHNICAL PRODUCT BULLETIN: B-60

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: OCTOBER 28, 2010

"MUNOX SR®"

I.	NAME, BRAND, OR TRADEMARK
MUNOX SR®

Type of Product: Bioremediation Agent (Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Osprey Biotechnics, a division of Phibro Animal Health Corporation

1845 57th Street

Sarasota, FL 34243

Phone: (941)351-2700

Fax: (941)351-0026

E-mail: troy.smith@pahc.com

(Mr. Troy Smith, Sr. VP Technical Operations

E-mail: thomas.baldeschwieler@pahc.com

(Mr. Thomas Baldeschwieler, Regulatory)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Osprey Biotechnics a division of Phibro Animal Health Corporation

1845 57th Street

Sarasota, FL 34243

Phone: (941)351-2700

Fax: (941)351-0026

E-mail: rafael.bortoleto@pahc.com

(Mr. Rafael Bortoleto, Sr. Director - Microbial Operations)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: No special ventilation is required under normal use.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special handling
necessary. In case of skin contact, wash with soap and water. In case of eye contact, flush with
water. In case of eye contact, flush with water. Wear protective gloves and wash hands with soap
and water after handling.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 35°F to 95°F. Store in a cool, dry location.
4.d. Temperatures of phase separations and chemical changes: <32°F and >212°F

V.	SHELF LIFE

MUNOX SR® is stable for over one year when stored at temperatures from 35°F to 95°F.

Bioremediation Agents

49

MUNOX SR®


-------
VI. RECOMMENDED APPLICATION PROCEDURE

1.	Application Method:

MUNOX SR® is a consortium of robust organisms that tolerate the natural salinity of seawater
up to approximately 5% and water temperatures below 100°F. MUNOX SR® is effective on
fresh and weathered crude oil and refined products because the metabolic pathways of the
organisms are based on beta oxidation that is effective on a wide range of constituents of
petroleum including aromatic, aliphatic and polyaromatic compounds. MUNOX SR® is provided
with a microbial density of lxlO8 cfu/mL in stabilized liquid form or after the freeze-dried form
is hydrated. The target population for effective treatment is 2.5xl05 cfu/mL.

One unit consists of one 55-gallon drum of hydrated MUNOX SR® or the amount of freeze-dried
powder to mix with 55-gallons of water to formulate the equivalent hydrated microbial solution.
Based on this formulation and treatment ratio, one unit of MUNOX SR® will treat approximately
22,000 gallons of impacted water.

Apply using in situ, hand sprayer, pump, pressure washer, etc. Product is ready to use and does
not require dilution of additional formulation.

2.	Concentration/Application Rate:

Surface water: MUNOX SR® provides organisms that can be effective in the destruction and
removal of petroleum hydrocarbons in surface water. It is best applied in areas where vertical
water mixing is minimal in order to maintain high microbial density in the vicinity of floating
hydrocarbons and near the water surface where there is a maximal oxygen concentration..

Beach application: The best application on the beach is by mixing the microbes in the beach
between the tide marks. Assuming the contractor will be mixing the microbes to a depth of 12
inches and there is 30% porosity, 5 drums per acres will provide sufficient MUNOX SR®
microbes for treatment.

Marsh or wetland application: This application of MUNOX SR® provides the greatest value
because it is the treatment approach that will not cause more damage to the wetlands. The
microbes will be sprayed on the oiled wetland from a boat or aircraft so the vegetation is not
disturbed. The recommended volume of MUNOX SR® will provide enough microbes to degrade
a moderate oiling level to acceptable levels. This application rate will treat the oil in surface
water, attached to vegetation, and on the soil surface. Assuming the wetland is submerged to a
depth of six inches during high tide, an application rate of 8 units per acre will provide sufficient
microbes for treatment.

3.	Conditions for Use:

MUNOX SR® is formulated for the bioremediation and metabolism of a wide range of petroleum
hydrocarbons including crude oil and refined fuels. Because petroleum in all of its forms is made
up of a wide variety of components, the dosage and application of MUNOX SR® will depend on
the type of hydrocarbon, degree of weathering, and environmental conditions.

Heavy petroleum compounds such as crude oil and refined products, such as bunker fuel, with a
high proportion of complex aliphatics will require a high dosage than lighter petroleum
compounds such as gasoline. The dosage will be site specific and will be determined with the
assistance of CL Solutions at no cost to the U.S. EPA or the user.

Bioremediation Agents

50

MUNOX SR®


-------
MUNOX SR® will tolerate a wide range of environmental conditions; however, some conditions
may reduce the effectiveness of MUNOX SR®. MUNOX SR® is most effective at a neutral pH,
but can tolerate a pH range from 5 to 8.5. The salinity of water should be less than 5%. MUNOX
SR® will also be most effective at moderately high temperatures from 70°F to 100°F. MUNOX
SR® will tolerate low temperatures and will become dormant at freezing temperatures. However,
MUNOX SR® will not tolerate temperatures above 105°F.

VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

1,003

0

3,609

0

0

NUTRIENT

1,096

0

4,661

0



MUNOX SR®

806

0

4,063

0



CONTROL

1,039

0

3,932

0

7

NUTRIENT

815

0

3,172

0



MUNOX SR®

199

0

3,292

0



CONTROL

847

15.5

3,578

0.85

28

NUTRIENT

832

24

3,674

21.2



MUNOX SR®

41

94.9

996

75.5

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control	Nutrient	Product

0.2.	9.9%	14.3%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:

Bioremediation Agents

51

MUNOX SR®


-------
pH: 6-8

Temperature: 4°C-35°C

Salinity: Fresh water to salt water, <110 ppm

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: <6.0 and >8.0
Temperature: <4°C->35°C
Salinity: >110 ppm

4.	Special nutrient requirements: None required. In application, MUNOX SR® may be
supplemented with the following Nutrient Mix at a ratio up to 1:10.

Nutrient Mix Composition:

Soy Peptone - 2.2%

Yeast Extract - 2.2%

Dextrose - 0.2%

Sodium Nitrate - 0.2%

Di-potassium Phosphate - 0.2%

Sodium Thiosulfate - 0.01%

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative.

Fecal coliform: Negative.

Shigella: Negative.

Staphylococcus Coagulase positive: Negative.

Beta hemolytic Streptococci: Negative.

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

52

MUNOX SR®


-------
TECHNICAL PRODUCT BULLETIN: B-61

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 17, 2010

"SOIL RX"

(aka, BIO-REGEN HYDROCARBON)

I.	NAME, BRAND, OR TRADEMARK
SOIL RX

(aka, BIO-REGEN HYDROCARBON)

Type of Product: Bioremediation Agent (Microbiological Culture, Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
3 Tier Technologies LLC

Worldwide Headquarters
413 W 13th Street
Sanford, FL 32771
Phone: (877) 226-7498
Fax:(877)570-0072
E-mail: dburdette@3 tiertech.com
Website: www.3tiertech.com
(Daniel J. Burdette, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Direct Sales

3 Tier Technologies LLC
Worldwide Headquarters
413 W 13th Street
Phone: (877) 226-7498
Fax:(877)570-0072
E-mail: dburdette@3 ti ertech. com
Website: www.3tiertech.com
(Daniel J. Burdette, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal ventilation is adequate.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Ingestion: No effect if
ingested in small amounts. A single dose of this product is rarely toxic by ingestion. Irritation of
the mouth, pharynx, esophagus and stomach can develop. Give two glasses of water. Do not
induce vomiting. Contact physician if needed. Eyes: Avoid eye contact. This material may cause
eye irritation. Immediately flush with water for 15 minutes. Contact physician if needed. Skin:
Slight redness on hands and forearms if individual has a history of dermal allergic reactions.
Dermatitis and skin sensitization can develop after repeated and/or prolonged contact. Remove
contaminated clothing and footwear. Wash with soap and water.

Bioremediation Agents

53

SOIL RX


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Always consult a physician if needed. Respirators are not required for recommended uses.
Rubber gloves are not required, but recommended. Safety glasses are not required, but
recommended. Wash hands with soap and water after handling product. Wash contaminated
clothing and footwear before reuse.

4.a. Maximum storage temperature: 120°F

4.b. Minimum storage temperature: 34°F - do not allow product to freeze

4.c. Optimum storage temperature range: 45°F to 95°F.

4.d. Temperatures of phase separations and chemical changes: NA, stable.

V.	SHELF LIFE

Shelf life exceeds 2 years when properly stored in the unopened original container.

VI.	RECOMMENDED APPLICATION PROCEDURE

SOIL RX (aka, BIO-REGEN HYDROCARBON) is a concentrated liquid formulation of
activated humic acid, highly concentrated hydrocarbon-oxidizing bacteria, and a readily
biodegradable natural amino acid complex consisting of a nutrient-rich extract with a broad-
spectrum package of identifiable amino acids, surfactants, and other proteins. This product is
designed to digest organics and hydrocarbons in soil and water.

1.	Application Method: SOIL RX (aka, BIO-REGEN HYDROCARBON) is a liquid concentrate
that must be diluted prior to use. The product can be sprayed after dilution using standard spray
application equipment, including but not limited to hand sprayers, mechanical sprayers, water
trucks, fire or emergency response equipment, pressure washers, etc. Mix or saturate
concentrate/water mixture with contaminated soils thoroughly for maximum performance. For
shallow/surface contamination, drench affected areas with enough dilution to fully saturate the
soil using normal spray equipment and water trucks. For general contamination less than two
feet, contaminated soil may require tilling or excavation to properly mix concentrate/water
dilution into soils. For deeper contamination greater than two feet, product application can be
applied through boring the area and using perforated piping per regulatory recommendations or
excavate the material and treat while land farming or bio-piling. For contaminated water, such as
marshes, shoreline and open water with floating hydrocarbons, apply dilution directly to the
contaminated areas using appropriate spray equipment and water cannons.

2.	Concentration/Application Rate: SOIL RX (aka, BIO-REGEN HYDROCARBON) must be
diluted using 1 part concentrate to 10 parts clean water prior to use. Product can be diluted up to
100 parts water as directed for specific applications. Application rates are determined by level of
contamination, area of application, and speed required for cleanup. Specific application rates are
determined prior to sale by the manufacturer and the distributor. A normal application rate for
contaminated soil is on gallon 10:1 diluted product per cubic yard of soil. Normal application
rate for water applications is three gallons 10:1 diluted product per 1000 square feet of
contaminated surface area.

3.	Conditions for Use: SOIL RX (aka, BIO-REGEN HYDROCARBON) is safe for application
in ocean and fresh water, all soil types, and shoreline treatments.

Water Salinity: Product should be diluted with fresh, clean water. Use of brackish or brine water
may be used if fresh water is not available. It should be noted that the use of brine water may
slightly reduce product performance or increase overall remediation time.

Bioremediation Agents

54

SOIL RX


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Water Temperature: Water must be between 42° to 110°F for normal product performance.
pH: Optimum water pH ranges between 4 to 8.

Temperature: Temperatures are below 32° and above 120°F may decrease product performance.
Nutrient Requirements: None. Nutrients required are in the product.

Type and Age of Pollutants: For use on most organic based contaminants and hydrocarbon based
materials like gasoline, jet fuels, diesel fuels, grease, tar, motor oils, crude oils, solvents, etc. Age
of contamination is not a factor as much as level of contamination, depth of contamination, and
length of time required for the remediation process. For materials that have hardened and are tar-
like, additional procedures may be required for effective remediation.

VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

34908.9

0

6051.3

0

0

NUTRIENT

34863.3

0

6047.4

0



SOIL RX

34993.0

0

6069.0

0



CONTROL

35206.2

+0.08

5720.9

5.45

7

NUTRIENT

32894.1

5.64

5745.8

4.98



SOIL RX

24446.0

30.14

3219.2

46.96



CONTROL

34287.8

1.779

5892.7

2.621

28

NUTRIENT

32610.0

6.463

5205.1

13.928



SOIL RX

17597.0

49.713

1600.1

73.635

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

8.01%	7.43%	30.14%

b. Toxicity:

NA

Bioremediation Agents

55

SOIL RX


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VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 4-8

Temperature: 42°F-100°F
Salinity: NA

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 2-10

Temperature: 34°F-125°F
Salinity: NA

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

56

SOIL RX


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN: B-62
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: DECEMBER 15, 2010
"PRO-ACT"

(aka, OILCLEAN w/ACTIVATOR)

I.	NAME, BRAND, OR TRADEMARK
PRO-ACT

(aka, OILCLEAN w/ACTIVATOR)

Type of Product: Bioremediation Agent (Biological Additive: Microbiological Culture w/
Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Pro-Act Biotech a Unit of LLG.LLC

64 Church Street
Warren, RI 02885
Phone: (401)245-7004
Fax: (401)633-6270
E-mail: bill@proactbiotech.com
Website: www.oil-clean.net
(Mr. William Campion)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Pro-Act Biotech a Unit of LLG.LLC

64 Church Street
Warren, RI 02885
Phone: (401)245-7004
Fax: (401)633-6270
E-mail: bill@proactbiotech.com
Website: www.oil-clean.net
(Mr. William Campion)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing is required in the handling, storage and field application of this product. For skin and
eye contact, wear goggles. If eye or skin irritation occurs, flush with plenty of fresh water.

4.a.	Maximum storage temperature: 110°F, up to 5 days
4.b. Minimum storage temperature: 35°F, do not freeze
4.c. Optimum storage temperature range: 40°F to 90°F

2/04/2020
7/27/2022

Bioremediation Agents

57

PRO-ACT


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V.	SHELF LIFE
One year as packaged.

VI.	RECOMMENDED APPLICATION PROCEDURE

PRO-ACT (aka, OILCLEAN w/ACTIVATOR) consists of two parts: liquid microbes and
activator (i.e., nutrient additive). As part of the Product Schedule, training on the proper use of
PRO-ACT (aka, OILCLEAN w/ACTIVATOR) will be provided by Pro-Act Microbial, Inc.
certified personnel.

1.	Application Method: Site (water and/or soil) testing is highly recommended prior to product
application. The testing is designed to assess the nutrient status of the contaminated site. The
desired nitrogen and phosphorus concentrations are in the range of 0.5 to 2.5 mg N/L for
nitrogen and 0.05 to 0.3 mg P/L for phosphorus. If there are inadequate nutrients in the
water/soil, the activator portion will be needed to bring the nutrients in line with product
specification. The activator portion can be applied directly to the site for treatment or it can be
mixed in with the diluted liquid microbes first. Nutrient levels need to be maintained for optimal
microbial action. Thus, depending on the nature of water/soil and the results of on site
monitoring, activator may need to be applied more than once. It is recommended that physical
methods such as skimming should be employed to recover as much oil as possible. PRO-ACT
(aka, OILCLEAN w/ACTIVATOR) should be used to breakdown the residual oil after the
physical methods have been used.

2.	Concentration/Application Rate: Liquid microbes are to be diluted with the non-chlorinated,
non-ozonated water or with the water to be treated (1:10 liquid microbe/water ratio) and applied
with a sprayer, either pump or pneumatic. The amount of PRO-ACT (aka, OILCLEAN
w/ACTIVATOR) needed depends on the amount of oil to be treated. One gallon undiluted liquid
microbes can treat up to 1000 square feet, assuming there is less than Vi inch of oil on surface.
For example, one gallon undiluted liquid microbes is good for up to 5 gallons of spilled oil. A
second application of Pro-Act (aka OilClean w/Activator) is beneficial to speed up the
bioremediation process.

3.	Conditions for Use: Monitoring of dissolved oxygen levels is recommended. If needed, a
mechanical aeration device should be deployed to maintain DO levels above 3 mg/L. PRO-ACT
(aka, OILCLEAN w/ACTIVATOR) works with fresh oil as well as weathered oil. Oil toxicity
(especially from easily dissolved shorter chain hydrocarbons in the fresh oil) should not be a
problem as long as physical methods are used first following a spill. The product is ideal for salt
water, brackish water and fresh water, with no limitations as to usage within optimum
temperature range of 20 to 400°C.

Bioremediation Agents

58

PRO-ACT


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VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

41277

0

6100

0

0

NUTRIENT

41670

0

6140

0



PRO-ACT

43193

0

6460

0



CONTROL

41393

0

5705

0

7

NUTRIENT

26370

0

3640

0



PRO-ACT

302

0

1979

0



CONTROL

42451

-2.766

4546

25.475

28

NUTRIENT

3654

91.231

1968

67.948



PRO-ACT

59

99.863

378

94.149

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

12.624%	55.670%	65.516%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.0

Temperature: 30°C
Salinity: 0.2 to 4%

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: <6.0 or >9.0
Temperature: <15°C or >45°C

Bioremediation Agents

59

PRO-ACT


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Salinity: <0.02% or >5%

4.	Special nutrient requirements: PRO-ACT (aka, OILCLEAN w/ACTIVATOR)

5.	Test results regarding the determination of the presence of the following:
Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

60

PRO-ACT


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TECHNICAL PRODUCT BULLETIN: B-63

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: DECEMBER 15, 2010

"BIOREM-2000 OIL DIGESTER™"

I.	NAME, BRAND, OR TRADEMARK
BIOREM-2000 OIL DIGESTER™

Type of Product: Bioremediation Agent (Biological Additive: Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Clift Industries, Inc.

P.O. Box 471578
Charlotte, NC 28247
Customer Service:

Phone: (800) 996-9901
Product Management:

Phone: (704) 752-0031
Fax:(704)544-2532
E-mail: matt@cliftindustries.com
(Mr. Matt Barnhill)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Clift Industries, Inc.

P.O. Box 471578

Charlotte, NC 28247

Customer Service:

Phone: (800) 996-9901

Product Management:

Phone: (704) 752-0031

Fax:(704)544-2532

E-mail: matt@cliftindustries.com

(Mr. Matt Barnhill)

X-Cel Chemical Specialties

921 Rosewood Street

Jenison, MI 49428

Office: (616) 581-4324

Fax: (616) 777-0022

E-mail: 1 arry. hewitt@xcel chemi cal. com

(Mr. Larry Hewitt, Primary Contact)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing is required in the handling, storage and field application of this product. For skin and
eye contact, wear gloves and goggles.

4.a.	Maximum storage temperature: 140°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 85°F

Bioremediation Agents

61

BIOREM-2000 OIL DIGESTER™


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V.	SHELF LIFE

The shelf life of the product is two (2) years when stored within the storage temperature range in
the original container.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray from boats, aircraft, fire eductor systems on boats, helicopter
buckets, hand-held or backpack sprayers, or from hoses attached to small pumps, water trucks
and aerial spray, including typical spreading systems.

2.	Concentration/Application Rate:

Shoreline Treatment:

To treat beaches, coarse sand, rocks, rip rap, sea walls, cobble shorelines and rocky shores, oiled
pilings and piers use one (1) part BIOREM-2000 OIL DIGESTER™ diluted with five (5) parts
water. Use one (1) gallon per 1,500 square feet of contaminated area.

Treating Marine Vegetation/Wetlands:

Dilute one (1) part BIOREM-2000 OIL DIGESTER™ with five (5) parts water and apply with
non-pressure, non-impact spraying equipment onto reeds, grasses, trees, and rocks in marsh areas
and vegetated wetlands. Use one (1) gallon per 1,500 square feet of contaminated area.
For Treating Water:

Do no dilute BIOREM-2000 OIL DIGESTER™ and apply directly spraying onto the surface of
oil.

Small Applications:

BIOREM-2000 OIL DIGESTER™ may be applied with hand sprayers or portable pumps to
spray the product directly onto oiled surfaces. Dose rates will vary with the type and amount of
petroleum spilled, the extent of weathering, and other site-specific conditions, including
temperature, porosity of surface, and residence time available to let the product contact the oil.

3.	Conditions for Use: Effective at temperatures above 40°F.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS PRODUCT

TOTAL
MEAN

RED%

TOTAL
MEAN

RED%

3 REPS/PROD

ALKANES

(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS

CONTROL

0

NUTRIENT

43163

0

6001

0

36643

0

4813

0

Bioremediation Agents

62

BIOREM-2000 OIL DIGESTER™


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BIOREM-2000
OIL

DIGESTER™

36492

0

4634

0



CONTROL

39249

9.0

5067

15.5



NUTRIENT

2946

91.9

3832

20.0

7

BIOREM-2000
OIL

DIGESTER™

5390

85.2

4114

11.0



CONTROL

33961

21.0

3812

36.0



NUTRIENT

106

99.7

729

84.0

28

BIOREM-2000
OIL

DIGESTER™

64

99.8

1324

71.0

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

10.7%	68.9%	67.0%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.0

Temperature: 85°F
Salinity: <10%

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 3.0 or 11.5

Temperature: <35°F or>125°F
Salinity: >40%

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

Bioremediation Agents

63

BIOREM-2000 OIL DIGESTER™


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IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

64

BIOREM-2000 OIL DIGESTER™


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TECHNICAL PRODUCT BULLETIN: B-64

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: FEBRUARY 22, 2011

"DRYLET™ MB BIO"

I.	NAME, BRAND, OR TRADEMARK
DRYLET™ MB BIO

Type of Product: Bioremediation Agent (Biological Additive: Microbiological Culture)

(formerly DRYLET™ MB BIOREMEDIATION)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Dry let, Inc.

8300 FM 1960 West
Suite #450
Houston, TX 77070
Phone: (346) 980-9570
E-mail: sales@drylet.com
(Mr. Scott Conley)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Dry let, Inc.

8300 FM 1960 West
Suite #450
Houston, TX 77070
Phone: (346) 980-9570
E-mail: sales@drylet.com
(Mr. Scott Conley)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements. In closed spaces, uses dust protective measures.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing is required; however, goggles and dust mask are recommended. Applying dry powder
may cause irritation to membranes. If eye or skin irritation occurs, flush with plenty of water.

4.a.	Maximum storage temperature: 120°F continuous
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

V.	SHELF LIFE

Minimum 5 years, with proper storage, in original packaging. Freezing does not harm shelf life;
however, extreme heat (over 180°F) for long periods of time can shorten shelf life.

Bioremediation Agents

65

DRYLET™ MB BIO


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VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply DRYLET™ MB BIO directly to oil contamination. DRYLET™
MB BIO may be applied by the usual methods of aerial or manual broadcast spreading. For
smaller spills, manual broadcast will deliver the best results. Larger spills in open water, marsh,
wetlands, or estuary areas should be treated by aerial powder dusting or dusting with mechanical
powder pumps.

2.	Concentration/Application Rate: Apply DRYLET™ MB BIO directly on the spill. Apply 0.4
pounds of product per cubic yard of soil, or 50 pounds per acre of open water slick. In marsh,
wetlands, and estuaries application rates may be up to 75 pounds per acre depending on the oil
type and contamination level.

3.	Conditions for Use: Water salinity: can be used in fresh or salt water. pH: 4 to 11.5.
Temperature: 32°F - 120°F. Water Temperature: 35°F - 170°F. Nutrient Requirements:

Nutrients are included with the product. However, for longer term project, additional nutrients
may be added to increase microbial activity. Types and Ages of Contamination: For use on
organic and hydrocarbon-based contamination. Tar like contamination may require mechanically
breaking the structure to obtain timely results.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

60871

0

8729

0

0

NUTRIENT

61995

0

8170

0



PRODUCT

61459

0

8790

0



CONTROL

56197

0

6224

0

7

NUTRIENT

42501

0

4833

0



PRODUCT

12303

0

4140

0



CONTROL

27314

55.0

5030

42.4

28

NUTRIENT

47

99.9

533

93.5



PRODUCT

820

98.6

1305

85.1

Bioremediation Agents

66

DRYLET™ MB BIO


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Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control
0.30%

Nutrient
50.0%

Product
84.8%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6.0-8.0

Temperature: 85°F to 110°F
Salinity: 0.5-4.0

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 4.0 or 11.5
Temperature: 35°F or 180°F

Salinity: 0.5 or 5.0 (above 4.5 reduces effectiveness by half)

4.	Special nutrient requirements: None

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

67

DRYLET™ MB BIO


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/17/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN: B-65

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: MAY 18, 2011

"DUALZORB®"

(aka, TRAILZORB, WHITZORB)

I.	NAME, BRAND, OR TRADEMARK
DUALZORB®

(aka, TRAILZORB, WHITZORB)

Type of Product: Bioremediation Agent (Biological Additive: Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
LBI Renewable

P.O. Box 637
22 Plains Drive
Buffalo, WY 82834
CUSTOMER SERVICE:

Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Mr. Aaron Larsen)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

DUALZORB® and TRAILZORB:

LBI Renewable

P.O. Box 637

22 Plains Drive

Buffalo, WY 82834

CUSTOMER SERVICE:

Phone: updated information required

Fax: updated information required

E-mail: updated information required

(Mr. Aaron Larsen)

WHITZORB:

Whit more Manufacturing Co.
930 Whit more Drive
Rockwall, TX 75032
CUSTOMER SERVICE:

Phone: (972) 771-1000, ext. 241
Fax: (972) 722-4561
E-mail: mkellis@whitmores.com
(Ms. Mary Kathryn Ellis)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: DUALZORB® is classified as non-flammable by DOT regulations (49 CFR

173. 124)

2.	Ventilation: DUALZORB" is not volatile and does not require ventilation.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact due
to mechanical abrasion. In case of eye contact, immediately flush eyes with large amounts of
water until particles are evacuated. Goggles are recommended during use.

Bioremediation Agents

68

DUALZORB®


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4.a. Maximum storage temperature: 200°F continuous

4.b. Minimum storage temperature: NA

4.c. Optimum storage temperature range: 32°F to 100°F

4.d. Temperatures of phase separation and chemical changes: DUALZORB® should be stored

out of the weather and should not be exposed to direct sun light for extended periods of time.

V.	SHELF LIFE

Guaranteed shelf life of unopened product is 5 years if not exposed to weather or direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURE

DUALZORB® is a dehydrated product that must be hydrated for maximum effectiveness to
bioremediate hydrocarbons in soil and water. Hydration can be accomplished with fresh or sea
water. Additionally, it can be applied on a surface and hydrated with natural precipitation.

1.	Application Method: This product can be applied by hand, mechanical spreaders, portable
mixer or blown onto a surface using an air conveyor. Mix hydrated DualZorb® with oil
contaminated soil, sand, or rocks by either hand, shovel or till into the soil with power
equipment. DUALZORB® will absorb approximately 80% of the oil from soil and sand in the
first 2 hours of application, with, continued bioremediation of oil. The bioremediation effect of
this product is not affected by water salinity, temperature, or oil type and age. However, the oil
absorption capacity is reduced in the presence of salt water as it will also absorb salts. For hard
surface stains and cleanup, hydrated product can be rubbed by hand over the surface until it will
no longer absorb oil. Place the spent product in an approved, labeled container in accordance
with local, state, federal, international, or country specific regulations. Depending upon the
compound(s) absorbed, this product may be disposed in a landfill, incinerated, or land farmed.
This product has a heat value of 842 IBtu pound and an ash content of 0.35%. For in situ
applications, the hydrated DUALZORB® can be tilled into the contaminated soil.

2.	Concentration/Application Rate: DUALZORB* is packaged in a dehydrated form and expands
three times its original volume when retrydrated with either fresh or 1.5 times with salt water.

This product should be mixed on a 1:1 volume basis with hydration water. For every 1 gallon of
oil, 4 pounds of DUALZORB® is recommended. For in situ applications, 50 pounds of hydrated
DUALZORB* is recommended per cubic yard of soil.

3.	Conditions for Use: DUALZORB* is manufactured for land use and will absorb hydrocarbon,
waste oil, and fuel spills. DUALZORB® is not affected by cold water but may require additional
contact time.

VII.	TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Bioremediation Agents

69

DUALZORB®


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Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

255,568

0

10,816

0

0

NUTRIENT

255,414

0

10,821

0



PRODUCT

248,869

0

12,738

0



CONTROL

244,841

0

10,290

0

7

NUTRIENT

79,688

0

9,963

0



PRODUCT

14,254

0

11,168

0



CONTROL

215,169

15.8

7,908

26.9

28

NUTRIENT

2,407

99.1

9,393

13.2



PRODUCT

1,545

99.4

950

92.5

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

0.4%	15.4%	30.0%

b. Toxicity:
Materials Tested
DUALZORB

®

No. 2 Fuel Oil

DUALZORB® &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

1,414.21

96-hr

1,096.05

48-hr

7.08

96-hr

1.13

48-hr

8.43

96-hr

2.70

48-hr

12.25

96-hr

11.71

48-hr

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of all microorganisms by species and percentages in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6.5-7.5

Temperature: 60°F to 100°F
Salinity: 0-10%

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3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 5.5-9.0

Temperature: 45°F and 105°F
Salinity: 0-10%

4.	Special nutrient requirements: LBI Renewable recommends nutrient supplement s of
maximum performance for bioremediation or in-situ applications. Contact LBI Renewable for
project specific nutrient dosing.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX. PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 2.25 g/mL

5.	pH: NA

6.	Surface Washing Agents: NA

7.	Solvents: NA

8.	Additives: None

9.	Solubility: NA

X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS
Compound
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Zinc
Cyanide

Chlorinated Hydrocarbons

CYANIDE, AND CHLORINATED

Concentration (ppm)
0.185
0.185
0.500
0.537
<0.185
<0.00303
<0.463
9.35
<0.060
<0.024

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TECHNICAL PRODUCT BULLETIN: B-66

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 08, 2011

"REMEDIADE™"

(aka, SP 7010)

I. NAME, BRAND, OR TRADEMARK

REMEDIADE™

(aka, SP 7010)

Type of Product: Bioremediation Agent (Nutrient Additive)

II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
GrowMate International, LLC
17150 Butte Creek Drive, Suite 100

Houston, TX 77090

Phone: (281) 866-9042

Fax: (281)866-9714

E-mail: victor@growmateintl.com

Website: www.growmateintl.com

(Mr. Victor J. Cardenas)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

GrowMate International, LLC
17150 Butte Creek Drive, Suite 100
Houston, TX 77090
Phone: (281)866-9042
Fax: (281) 866-9714
E-mail: victor@growmateintl.com
Website: www.growmateintl.com
(Mr. Victor J. Cardenas)

VariChem International, Inc.
78330 Hi Way 35 North
Bay City, TX 77414
Phone: (979) 245-7278
Fax: (979) 245-0612
E-mail: Gordon@varichemusa.com
Website: www.varichemusa.com
(Mr. Gordon Winfrey)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: As defined by OSHA's
Hazard Communication Standard, this product is non-hazardous with no evidence of adverse
effects. Use safety glasses when handling for eye protection. Store in a cool dry place. Flush eyes
and wash skin if contacted. In the event of contact with skin, wash with water. In the event of
contact with eyes, rinse with water. In the event of contact with clothing or surfaces such as
floors or counter tops, rinse with water and dry. In the event of spilling onto land or water, no
handling or rinsing requirements are needed. No other safety or handling precautions need to be
adhered to in the event of contact or spills.

4.a.	Maximum storage temperature: 115°F continuous
4.b. Minimum storage temperature: 32°F

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4.c. Optimum storage temperature range: 40°F to 98°F

4.d. Temperatures of phase separation and chemical changes: NA

V.	SHELF LIFE

Shelf life of product unopened is 2 years. If the container has been opened, but uncontaminated
and is resealed properly, the shelf life is 1 year after initial opening.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product may be applied to any surface for removal of hydrocarbons. For
treatment of large areas, properly diluted product may be applied by spraying with a pressure
washer, portable fire pump or any other suitable pump with non-chlorinated fresh water or salt
water. Application can also be made with normal spray equipment via a 1" or larger hose and a
spray nozzle, similar to a fire nozzle. Eductor setups, water trucks as well as fire or other
emergency response equipment may be used. Aircraft application is also effective in covering
large areas or contaminated water.

2.	Concentration/Application Rate: For in-situ soils, till the REMEDIADE™/water mixture onto
the contaminated area. Soil treatment rate guidelines are 1 gallon of concentrate for 30 cubic
yards of soil for each 20,000 TPH contamination level. Example: 40,000 TPH level would be 2
gallons per 30 cubic yards. Clay soils may take more product and sandy soils may take less.

After the treatment rate is established, apply l/3rd of the product mixture on the first day, wait 5
to 7 days and apply the second l/3rd of the product mixture, wait another 5 to 7 days and apply
the final l/3rd of the product mixture. During each of the three applications apply '/2 of the
product mixture to the affected soil. Till or blade in this application before applying the second V2
of the product mixture. This will help the product get good coverage and disperse well into the
soil.

In the event of oil spills on water, treatment guidelines are 1 gallon of concentrate per 30 square
foot of surface area. After the treatment rate is established, apply l/3rd over the area and wait 5 to
7 days and apply the second treatment. Then wait 2 to 5 days and apply the third treatment. Light
gravity oils may take more. When spraying the product over oil, good agitation of the
contaminant with the product can only help. This helps add to surface contact and aids in the
bioremediation process. Salinity of the water will not make a difference in the effectiveness of
the product.

3.	Conditions for Use: Product must be mixed with non-chlorinated water, but it can be used with
fresh, salt or brackish water. Reapplication may be necessary in severely contaminated areas. Be
sure to apply the product on three separate days, allowing time in between the days, this helps
keep bacteria counts up at a more consistent level through the process. Adding all the product in
one treatment will only prove to waste product and slow the effectiveness of the overall
remediation process.

Bioremediation Agents

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REMEDIADE™


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VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL

RED%





MEAN



MEAN





3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

255,568

0

10,822

0

0

NUTRIENT

255,414

0

10,821

0



PRODUCT

245,168

0

10,816

0



CONTROL

244,841

0

10,920

0

7

NUTRIENT

215,169

0

9,963

0



PRODUCT

79,688

0

9,393

0



CONTROL

21,469

91.6

9,067

16.2

28

NUTRIENT

4,198

98.4

7,908

26.9



PRODUCT

2,404

99.0

607

94.4

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

0.0%	17.8%	36.0%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

The product is a nutrient additive and does not contain microbiological cultures or enzyme
additives.

1.	Listing of each component of the formulation by chemical name and percentage by weight:
CONFIDENTIAL

2.	Optimum storage conditions:

Temperature: 40°F to 98°F

IX.	PHYSICAL PROPERTIES

NA

Bioremediation Agents

74

REMEDIADE™


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X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

75

REMEDIADE™


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN: B-67
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: JULY 27, 2011
"ERGOFIT MICROMIX AQUA"

I.	NAME, BRAND, OR TRADEMARK
ERGOFIT MICROMIX AQUA
Type of Product: Bioremediation Agent (Microbiological Culture, Enzyme Additive, Nutrient
Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Evadine Technologies, LLC

217 Deborah Drive

New Braunfels, TX 78130

Phone: updated information required

E-mail: updated information required

(Mr. Warren Russell)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Evadine Technologies, LLC
217 Deborah Drive
New Braunfels, TX 78130
Phone: updated information required
E-mail: updated information required
(Mr. Warren Russell)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Water-based, Non-flammable

2.	Ventilation: Needs no ventilation; aqueous-based organic product; does not emit hazardous
vapors. Some CO2 may build up.

3.	Skin and eye contact; protective clothing; treatment in case of contact: ERGOFIT
MICROMIX AQUA is not a dermal irritant. Avoid eye contact, and wear goggles when using
product. Eyewash for quick and copious eye flushing should be available on site. Seek prompt
medical attention should contact occur and if irritation persists. Protective rubber gloves are
suggested during handling. ERGOFIT MICROMIX AQUA has a smell of fermentation and
yeast. The product does not give off harmful vapors. Long storage will cause build up of CO2 in
water vapor.

4.a.	Maximum storage temperature: 104°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 57°F to 97°F

4.d. Temperatures of phase separation and chemical changes: above 113°F

4/16/2017
7/27/2022

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V.	SHELF LIFE

ERGOFIT MICROMIX AQUA has a recommended shelf life of 5 years. After 5 years at
optimum storage in cool temperature there is an approximate 10% decrease per year in product
effectiveness. Shelter from direct sunlight or extreme cold or heat source. In the event of fire,
wash with water.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: ERGOFIT MICROMIX AQUA can be applied with any commercially
available spray apparatus, such as small hand held tanks, back packs, large mixing tanks with
mechanical pumping devices, vessels with booms for spraying wide paths, or liquid spray
devices on crop duster airplanes or helicopters. ERGOFIT MICROMIX AQUA can also be
applied by eductor systems from vessels, fire trucks, or any other outfitted vehicle.

2.	Concentration/Application Rate: ERGOFIT MICROMIX AQUA generally takes 5 to 50
minutes to penetrate the molecular walls of hydrocarbons. Warmer conditions favor faster
biological action whereas colder conditions may reduce the speed of decomposition. Once
ERGOFIT MICROMIX AQUA is applied to the targeted areas, the microbes will attach
themselves to the hydrocarbons and start to attack their carbon structure and metabolize into
natural organic substances from the humus family. Aquatic plants and animal life will feed on
this nutrient. Within hours odor will be negligent and changes will be noticeable in seven days,
depending on the temperature. ERGOFIT MICROMIX AQUA will also break down the
adhesive properties of the hydrocarbons, preventing oils from attaching to animals, vegetation,
rocks, and earth.

Dilution Rates: ERGOFIT MICROMIX AQUA should always be mixed with the native water of
the affected area. Note: Do not use city water that has been treated with chlorine with ERGOFIT
MICROMIX AQUA. This means that if you are treating an affected saltwater area, then
saltwater should be used as your base carrier for the product. Likewise if you are treating a lake
or river, then that carrier water would be the freshwater from that source. For general
applications and light oil films, dilute each gallon of ERGOFIT MICROMIX AQUA with source
water (e.g., fresh, brackish, or saltwater) at a ratio of 1:50. For oil mousse like formation in
intertidal zones, use a dilution of 1:30. If the spill is very heavy and the oil layer is thick (more
than 1 inch) it is recommended that ERGOFIT MICROMIX AQUA be applied at a lower ratio of
1:20. On land not involving water bodies, it is recommended that an organic absorbent be
applied prior to using ERGOFIT MICROMIX AQUA to treat oil spills to remediate the CI and
C35 Petroleum Hydrocarbons. This is to increase the contact surface area for ERGOFIT
MICROMIX AQUA to convert spills oil and absorbent to organic humus.

Application on Coastal Water: Apply the mixed solution using hand held sprayers, tank sprayers,
booms from vessels, helicopters, or airplanes. First, start by spraying the outer perimeter of the
spill and systematically work towards the middle of the affected area, making sure to cover the
entire surface area of the spill. Use 1.5 gallons of ERGOFIT MICROMIX AQUA concentrate for
every 1000 gallons of hydrocarbons spilled. Dilute it with 30 gallons of seawater per gallon of
concentrate for spraying. [To calculate gallons of ERGOFIT MICROMIX AQUA required,
multiply estimated gallons of hydrocarbons by 0.0015.] For denser hydrocarbons, like in the case
of crude oil, multiply barrels of crude oil by 42 to get gallons of crude and apply above ratios. If

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you do not know gallons of hydrocarbons or barrels of crude oil, estimate size of spill by (1000
square yards x 2 inch average thickness) to arrive at gallons of oil spilled. Use 10 kg/22 lbs of
ERGOFIT MICROMIX AQUA diluted to 50 gallons in water to cover this area. As a rule, 2
kg/4.4 lbs ERGOFIT MICROMIX AQUA is required per metric ton of oil spilled. Dilution
varies depending on oil thickness or simple sheen floating on water surface.

Application for Intertidal Zones: ERGOFIT MICROMIX AQUA should be applied at low tide,
when the affected areas are exposed to the elements, allowing the product to securely attach to
the hydrocarbons. Cease application if the tide rises and resume once the water level has receded
again. Continue application cycle until the entire affected area has been coated. The
recommended mix ratio is 1:30. In areas where a combination of high tide and waves have
pushed the contamination beyond the intertidal zone, oil rag layer looking like chocolate mousse,
cordon off the area and start spraying ERGOFIT MICROMIX AQUA diluted at a ratio of 1:20 in
water. The objective is to get an application rate of between 1 to 2 gallons of concentrated
ERGOFIT MICROMIX AQUA sprayed per 1000 gallons of hydrocarbons spilled.

3. Conditions for Use: ERGOFIT MICROMIX AQUA acts on all organic hydrocarbons on sea,
fresh water, and land. As the age of spilled hydrocarbons increases, so does the time necessary
for bioremediation. In general, fresh crude, gasoline of BTEX takes anywhere from 30 days to 12
months to completely bioremediate depending on weather conditions and density of spill.
However, the remediation process will be noticeable throughout the process. Variations in
seawater salinity, has no effect, as long as microbial life can exist, then ERGOFIT MICROMIX
AQUA will be effective in salt and brackish water with a maximum salinity of 4.9 percent.
ERGOFIT MICROMIX AQUA bioremediation slows somewhat at temperatures below 40°F.
However, it will continue to work in any water temperatures that will sustain microbial life.
Decreasing the amount of ERGOFIT MICROMIX AQUA per square yard from recommended
dosage rates lengthens the remediation time. When nitrogen and carbon is added to ERGOFIT
MICROMIX AQUA the initiation of bacterial-enzymatic activity is enhanced many fold to begin
bioremediation within 2 hours of application.

VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL MEAN

RED%



3 REPS/PROD

ALKANES

(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS

0

CONTROL

239,235

0

16,502

0

PRODUCT

239,686

0

17,431

0



CONTROL

217,023

9.30

10,942

33.70

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7

PRODUCT

17,819

92.6

9,606

44.90



CONTROL

188,379

21.3

8,989

45.50

28









PRODUCT

2,216

99.10

3,100

82.20

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Product

1.7%	45.6%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS
Microbiological Culture:

1.	Listing of all microorganisms by species and percentage in the composition:
CONFIDENTIAL

2.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6.5 to 7.5.

Temperature: 57°F to 97°F.

Salinity: The maximum permissible salinity is up to 4.9% sodium by solution

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: Lower than 4.5 or higher than 8.5 reduces the product efficiency by 50 percent.
Temperature: Lower than 32°F or higher than 104°F reduces the product efficiency by 50
percent.

Salinity: The maximum permissible salinity is up to 4.9% sodium by solution

4.	Special nutrient requirements: NA

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta Hemolytic Streptococci: Negative

Enzyme Additive:

1.	Listing of each component of the total formulation, other than enzymes, by chemical name
and percentage by weight: CONFIDENTIAL

2.	Enzyme Names: CONFIDENTIAL

3.	I.U.B.: CONFIDENTIAL

4.	Source of Enzymes: Plant or Fungi/Fermentation process

5.	Units: No less than 1% and no more than 50% by weight

6.	Specific Gravity: 1.00

7.	Optimum Conditions:

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a.	pH: 7.0

b.	Temperature: 72°F

c.	Salinity Ranges: Fresh water to salt water up to 4.9%

d.	Minimum and Maximum pH: 4.5 - 8.5

e.	Minimum and Maximum Temperature: 32°F - 104°F

f.	Minimum and Maximum Salinity Levels: Salinity level that will support microbial
activity will not adversely a ERGOFIT MICROMIX AQUA performance

g.	Enzyme Shelf Life: Up to 5 years when properly stored

h.	Enzyme Optimal Storage Conditions: 72°F is optimal, enzyme range is freezing to
104°F, never leave ERGOFIT MICROMIX AQUA in direct sunlight for more than a
couple of hours

Nutrient Additive:

1.	Listing of each component of the formulation by chemical name and percentage by weight:
CONFIDENTIAL

2.	Optimum storage conditions:

Temperature: 32°F to 104°F

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

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LISTING CHANGES PENDING;

VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN: B-68

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 8, 2011

"SHAMANTRA GREEN"

(aka, SHAMANTRA BIO)

I.	NAME, BRAND, OR TRADEMARK
SHAMANTRA GREEN

(aka, SHAMANTRA BIO)

Type of Product: Bioremediation Agent (Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Molecular Mediation LLC

C/- Molecular Mediation Pty Ltd
Level 3, Suite 405
152 Bunnerong Road
Eastgardens 2036
Australia

Phone: +612-9659-4553
E-mail: info@molecularmediation.com
E-mail: mark@molecularmediation.com
(Mr. Mark Pilgrim, Manager)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Molecular Mediation PTY LTD

Level 3, Suite 405
152 Bunnerong Road

Eastgardens 2036
Australia

Phone: +612-9659-4553
E-mail: info@molecularmediation.com
E-mail: mark@molecularmediation.com
(Mr. Mark Pilgrim, Manager)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required, however goggles are recommended. If eye or skin irritation occurs, flush
with plenty of fresh water.

4.a.	Maximum storage temperature: 200°F
4.b. Minimum storage temperature: None

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4.c. Optimum storage temperature range: 40°F to 140°F

4.d. Temperatures of phase separation and chemical changes: Stable

V.	SHELF LIFE

>3 years when stored in sealed silos, polydrums, poly bags or totes.

VI.	RECOMMENDED APPLICATION PROCEDURE
1. Application Method:

Recommended Uses and Product Description

Shamantra Green is recommended for use on water and near shoreline oil spills. Shamantra
Green is a natural product made using humic acid. The product has been processed to have a
strong affinity for collecting natural oils. The process makes applying and removing the product
to/from the environment easy and safe.

Water Applications

For small scale spills on fresh or salt water, Shamantra Green can be broadcast directly onto the
spill by hand or a hand held spreader. Agitation is not necessary when using Shamantra Green on
small scale spills. Shamantra Green can also be used in booms, sacks, and pillows.

For large spills on fresh or salt water, Shamantra Green can be deployed into the spill using an
air or water stream.

Shamantra Green will remove oils and other hazardous hydrocarbon based materials from both
salt and fresh water very effectively using an encapsulation process on the spilled oil. Once
encapsulated into the carbon matrix of Shamantra Green, the spilled oil will not leach out, even
under pressure. The humic acid then acts as a nutrient to stimulate microbial activity and enhance
the bioremediation of the spilled oil.

Any encapsulated residue can be removed from the water with hand vacuums, vacuum barges,
commercial nets, centrifuges, etc. Encapsulated materials can be sent to landfill or used as a fuel
source for generating heat ensuring that any material disposed of is in accordance with all
applicable federal, state, and local regulations.

Shoreline Applications

For spills on shorelines, Shamantra Green would be applied in the same manner and ratios as
with the water applications. The product can also be applied by sand-blasting equipment, fire
hoses or pneumatic spreading equipment. Agitation is not necessary for most applications.

To recover encapsulated oil or hazardous materials from spills on land, the encapsulated product
can be collected and removed efficiently and effectively using a variety of manual and
mechanical methods including picking up by hand, using brooms, rakes and shovels to remove
and pick up encapsulated petroleum waste product. Mechanical means include using hand held
vacuums, portable vacuum units, and vacuum vehicles.

Once the Shamantra Green has been saturated with oil or hazardous materials, it will not leach

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the contaminants, even under pressure, so any encapsulated materials can be disposed of
appropriately or used as a fuel source for generating heat ensuring that any material disposed of
is in accordance with all applicable federal, state, and local regulations.

Proper precautions, including testing as necessary to identify the characteristics of wastes
encapsulated by Shamantra Green should be taken to determine the safe and legally required
means of recovering, handling, storing, transporting, treating, recycling, or disposing of materials
on land in accordance with all applicable federal, state, and local regulations.

2.	Concentration/Application Rate:

Shamantra Green is usually applied at a ratio of 1:5-1:30 to waste by weight to remediate light,
medium, and heavy hydrocarbons. Shamantra Green can also be used very effectively on heavier
crudes including Bunker C using the aforementioned application ratios. The specific ratio will
depend on many factors including the composition of the waste, the ambient temperatures, pH of
the contaminated water and age of the waste spill. Optimum application ratios should be
determined on a case by case basis.

3.	Conditions for Use:

Shamantra Green initially behaves like a synthetic sorbent, then encapsulates the oil through a
chemical and physical process. Once encapsulated, the spilled oil is captured within the pore
matrix contained within the carbon structure.

Shamantra Green is effective in all environments and under a broad range of weather conditions.
Depending upon the age, viscosity, and composition of the spilled material, varying amounts of
Shamantra Green may be required to obtain complete remediation. Any encapsulated residue can
be recovered and disposed of in accordance with all applicable federal, state, and local
regulations.

VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL MEAN

RED%





MEAN









3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

43,457

0

6,451

0

0

NUTRIENT

43,047

0

6,263

0



PRODUCT

43,153

0

6,262

0

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CONTROL

40,943

0

5,283

0

7

NUTRIENT

214

0

2,389

0



PRODUCT

9,859

0

1,338

0



CONTROL

39,066

10.1

4,429

31.3

28

NUTRIENT

76

99.8

685

89.1



PRODUCT

122

99.7

297

95.3

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

14.4%	0.0%	25.4%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
Nutrient Additive:

No special requirements are required other than the product can be stored in dry conditions with
an optimum storage temperature of 40°F to 140°F and a maximum storage temperature of 200°F.

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

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TECHNICAL PRODUCT BULLETIN: B-69

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: OCTOBER 13, 2011

"SUMP SAFE BIO-RECLAIM"

I.	NAME, BRAND, OR TRADEMARK
SUMP SAFE BIO-RECLAIM

Type of Product: Bioremediation Agent (Biological Additive/Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

F4 Environmental, Inc.

P.O. BOX 2506
Stony Plain, Alberta, Canada
T7Z 1X9

Mobile: (780) 238-2741

E-mail: marlin@f4environmental.ca

(Mr. Marl in Rudolph)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Long Chain Reclaim

960 Boulder Blvd

Stony Plain, Alberta, Canada

T7Z 0E6

Phone: (780) 886-2024
Email: mmv shak@l creel aim. com
(Mr. Mike Myshak)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required, however goggles are recommended. If eye or skin irritation occurs, flush
with plenty of fresh water.

4.a.	Maximum storage temperature: 110°F maximum, must be used within 24 hours from
constitution

4.b. Minimum storage temperature: 45°F

4.c. Optimum storage temperature range: 60°F to 90°F

4.d. Temperatures of phase separation and chemical changes: Stable

V.	SHELF LIFE

The material must be used within 24-48 hours of constitution of the powdered bacteria portion in
water. The dry material must be kept at -20°C and is stable for two years at this temperature.
Once sent to the field, the material may be stored on ice for up to two weeks prior to constitution.

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VI. RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product may be applied by the usual methods. For smaller spills a drum
pump with sprayer may be used, mixing with fresh water typically. The concentrate is used at
25:1 dilution rate with water and is typically applied at a rate of 6 gallons per cubic meter of soil.
It is important that the soil be broken up into small clumps (rototilling is acceptable) to ensure
effective application. The soil is left and biodegradation is expected to complete in
approximately 12 weeks. Analysis using approved sampling procedures is performed to confirm
biodegradation.

For larger volume projects, any auger based soil homogenizer is employed to break up large
clumps of soil, which are dug out from the contaminated area using a standard hoe. The broken
up soil is taken up a conveyor and has the diluted concentrate (25:1) at a rate of 6 gallons per
cubic meter of soil. Piles up to 20 feet high may be formed. The soil is left and biodegradation is
expected to be complete in approximately 12-18 weeks. Analysis using approved sampling
procedures is performed to confirm biodegradation. Proper safety rules must be employed to
ensure that any holes dug out are not accessible to employees or unauthorized personnel.

For oil spills on open water, it is recommended that a 25:1 dilution of the product be applied via
spraying. In this way, the bacteria can contact the floating oil and immediately begin to form a
bio-film. The spray would also be applied on any soil contaminated on banks, etc. It is important
to ensure complete coverage of the water/oily surface and soil during spray application.
Degradation will be visible visually and can be confirmed by Fats, Oil and Grease (FOG)
analysis.

For smaller, contained volumes of oily water (typically emulsified, white water), it is
recommended that sufficient concentrate be added to the contaminated water such that it results
in a 2.5% concentration of the concentrate in the contaminated water. Preferably, aeration can be
performed, using even a small, fish tank aeration unit. Visual evidence of biodegradation should
be apparent within one week or less and can be confirmed by FOG analysis.

2.	Concentration/Application Rate: The concentrate is used at 25:1 dilution rate with water and is
typically applied at a rate of 6 gallons per cubic meter of soil.

3.	Conditions for Use: The product can be used in fresh or salt water and may be applied at
temperatures between 40°F and 120°F. However, the product is most effective when applied at
water temperatures between 70°F-90°F. Further, the product is effective on fresh spills or aged
hydrocarbons. Note for preparation of the product to be applied while in the field: all
components listed in the product are packaged as a complete unit and are applied as such. The
microbial portion of the product is supplied in bags which are either drum (55 gallon) or pail (5
gallon) sizes. Fresh water, if available, is added to fill the bag (bags are placed in pails or open
headed drums) to 55 gallon of 5 gallons respectively. Depending upon which of these are being
constituted with water, a high-density polyethylene (HDPE) bottle with the appropriate quantity
of surfactant is added into the container (bottles are labeled Bio-Reclaim Surfactant - Drum Size
(or Pail Size)). In the same way, HDPE containers with appropriate amounts of sodium nitrite are
added and are labeled Bio-Reclaim Salt - Drum Size (or Pail Size)).

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VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL MEAN

RED%





MEAN









3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

40770

0

5229

0

0

NUTRIENT

41329

0

5326

0



PRODUCT

40609

0

5384

0



CONTROL

37530

0

4824

0

7

NUTRIENT

21788

0

4634

0



PRODUCT

38354

0

5298

0



CONTROL

31456

22.8

3692

24.2

28

NUTRIENT

502

98.8

3052

42.7



PRODUCT

21356

47.4

3742

49.0

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

6.36%	33.00%	3.00%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition of
the additive: CONFIDENTIAL

3.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 6-8

Temperature: 90°F
Salinity: Not applicable

3. Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

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pH: 4.8-9

Temperature: 59°F - 104°F
Salinity: Not applicable

4.	Special nutrient requirements: A combination of 70 percent live active yeast mixed with 30
percent fine ground corn cob is used as a nutrient. In a 55 gallon drum of concentrate,
approximately 1.1 kg of this mix will be found (relative to the 1.1 kg, the actual bacteria
represent the negligible mass of several grams). There are no storage requirements for the
nutrient portion of the formula; however, as they are in a homogenous mixture with the bacteria,
they must be stored as described in Part V of this bulletin.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

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TECHNICAL PRODUCT BULLETIN: B-70

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: FEBRUARY 7, 2013

"WASTE AWAY®"

I.	NAME, BRAND, OR TRADEMARK
WASTE AWAY®

Type of Product: Bioremediation Agent (Biological Additive/Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
CXI (Chem-X International, LLC)

1100 East Sandy Lake Road

Coppell, Texas 75019

Phone: (972) 471-7775

Fax: (972)393-2011

E-mail: dhowardcxi@outlook.com

Website: www.cxinternational.com

(Mr. David Howard)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Prime-Dirt
20810 Avenue 332
Woodlake, California 93286
Phone: (555) 787-7278
Fax:(555) 787-8560
E-mail: iames@prime-dirt.com
Website: www.prime-dirt.com
(Mr. James Henderson)

Back-To-Nature Compost

P.O. Box 190

5407 Slaton Highway

Slaton, Texas 79364

Phone: (888) 282-2000

Phone: (806) 745-1170

E-mail: greg@backtonaturecompost.com or

bi @backtonaturecompost.com

Website: www.backtonaturecompost.com

(Mr. Greg Schilling)

Microbial Matrix

33935 Highway 99E, Suite B

Tangent, Oregon 97389

Phone: (541) 967-0554

E-mail: lrogers@microbialmatrix.com

Website: www.microbialmatrix.com

(Ms. Lynn Rogers)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however, gloves and goggles are recommended. If eye or skin irritation

Bioremediation Agents

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occurs, flush with plenty of fresh water. If ingested, may cause nausea or vomiting, seek medical
attention. Do not induce vomiting. In case of spills, disperse with water, treat like a surfactant or
soap spill.

4.a. Maximum storage temperature: 100°F continuous, 120°F up to 5 days

4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 50°F to 100°F

4.d. Temperatures of phase separation and chemical changes: Stable

V.	SHELF LIFE

Two years when product remains in sealed bottles, poly drums, or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product may be applied by any type of liquid delivery system (i.e., boom
sprayers, spray pumps). For smaller spills a drum pump with sprayer may be used, mixing with
fresh or salt water as required depending on the type and viscosity of oil being treated. Typically
containment is not necessary.

2.	Concentration/Application Rate:

a.	On heavy oils: use product directly on the spill, or up to approximately a 1:10 dilution ratio
(product:water). Lighter oils will require a 1:10 to 1:30 product to water ratio. Warmer waters
(greater than 78 °F) and/or good agitation during application will require less product.

b.	Lagoon application: 2 gallons per surface acre of lagoon or 16 ounces per 3,000 cubic feet.
Maintain daily at 50 percent initial application. Use spray applicator for even distribution.

c.	Shoreline application: 1 gallon per 10 cubic yards of contaminated soil applied at 3 percent
concentration. Maintain weekly with 50 percent initial application. Use spray applicator for even
distribution. Till soil after application or use gravity fed drip system.

3.	Conditions for Use: Effective in salt water or fresh water, with no limitations as to usage
within optimum temperature parameters (application may be made at or above 35°F, with
optimum above 48°F). Product may be used on any age crude and any type. Optimum salinity
range is from fresh water to salt water of 110 ppt.

Bioremediation Agents

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VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL MEAN

RED%



3 REPS/PROD

ALKANES
(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS



CONTROL

99715

0

11056

0

0

NUTRIENT

94558

0

10228

0



PRODUCT

98187

0

10270

0



CONTROL

54816

0

9690

0

7

NUTRIENT

48670

0

9329

0



PRODUCT

51534

0

6019

0



CONTROL

46847

53.0

6452

40.8

28

NUTRIENT

3581

96.2

6136

40.0



PRODUCT

776

99.2

4038

60.7

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	Product

6.41%	50.91%	49.95%

b. Toxicity:

Material Tested
WASTE AWAY®

No. 2 Fuel Oil

WASTE AWAY® & No. 2
Fuel Oil (1:10)

Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
552,762.06 96-hr
353,302.46 48-hr
10.22 96-hr

2.11	48-hr
12.54 96-hr

2.11	48-hr
11.87 96-hr
13.29 48-hr

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition of

Bioremediation Agents

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the additive: CONFIDENTIAL

3. Optimum pH, temperature, and salinity ranges for use of the additive:
pH: 7.5, range 6.0 to 8.0
Temperature: 72°F, range 60°F to 60°F
Salinity: 40 ppt, range 0 to 110 ppt

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 4.0-11.0
Temperature: 40°F - 125°F
Salinity: 0-110

4.	Special nutrient requirements: Not applicable

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

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TECHNICAL PRODUCT BULLETIN: B-71

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 7, 2014

"ACT TERRA FIRMA"

(aka, ACT-TF)

I.	NAME, BRAND, OR TRADEMARK
ACT TERRA FIRMA

(aka, ACT-TF)

Type of Product: Bioremediation Agent (Biological Additive/Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Franssen Enterprises, Inc.

511 N. McKinley Avenue
Fort Lupton, CO 80621
Phone: (303) 833-5393
Fax:(303)833-2872
E-mail: actcleaners@comcast.net
Website: www.actcleaners.com
(Mr. Todd Franssen)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
American Cleaning Technologies, Inc.

(ACT BioRemediation Products)

511 N. McKinley Avenue
Fort Lupton, CO 80621
Phone: (303) 833-5393
Phone: (866) 919-2872
Fax:(303)833-2872
E-mail: actcl eaner s@ comcast. net
Website: www.actcleaners.com
(Mr. Todd Franssen)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Standard industrial hygiene ventilation practices should be used to control human
exposures to this product. Respiratory protection equivalent to either N100 or the older HEPA
filter (APR with a DFM (purple) cartridge) will provide adequate protection.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Recommendations are
guidelines and may not apply to every situation. To prevent skin contact, standard work clothing
and standard work or latex gloves will provide adequate protection. To prevent eye contact,
standard safety glasses with side shields are recommended.

4.a.	Maximum storage temperature: 48°C continuous, 60°C up to 5 days
4.b. Minimum storage temperature: -45°C

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4.c. Optimum storage temperature range: 4°C to 38°C

4.d. Temperatures of phase separation and chemical changes: Stable

V.	SHELF LIFE

Store product in a dry area. If kept in a sealed container with desiccant bag the shelf life is 5
years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply ACT TERRA FIRMA directly to surfaces by broadcasting
product with a scoop or grass seed drop spreader. DO NOT add fertilizers or nutrients.

2.	Concentration/Application Rate:

Hard Surface with Limited Permeability (e.g., concrete, asphalt, stone, etc.): Apply a small
amount of ACT TERRA FIRMA with a scoop or grass seed drop spreader to the surface. Using a
soft bristle broom spread ACT TERRA FIRMA over the surface. If desired results are not
achieved within two weeks repeat application. DO NOT sweep or wash cleaner off. ACT
TERRA FIRMA will dissipate over time. One pound covers approximately 100 square feet. DO
NOT add fertilizers or nutrients. Prior to application, appropriate containment mechanisms
should be used deployed to prevent runoff of the product/oil mixture.

Permeable Surfaces (e.g.. packed sand, gravel, or soil; loose, bulk material that may be excavated
and stockpiled for treatment): Apply ACT TERRA FIRMA product directly to surfaces by
broadcasting product using a scoop or grass seed drop spreader over the contaminated area.
Check the contamination levels every 15 days, reapplying as needed. Tilling may be needed for
contamination 12 inches or deeper. One pound covers approximately 50 square feet. DO NOT
add fertilizers or nutrients. Prior to application, appropriate containment mechanisms should be
deployed to prevent runoff of the product/oil mixture.

Applications to Water: ACT TERRA FIRMA is recommended for use in conditions where the
water is not actively flowing. Apply to water surface at a rate of one pound over approximately a
200 square foot surface area. Using a scoop or a handheld broadcast spreader to ensure that ACT
TERRA FIRMA is dispersed evenly. DO NOT add fertilizers or nutrients.

Conditions for Use: Product usage is not affected by salinity. Water temperature range should be
-2°C to 46°C and can be used on frozen water in temperatures as low as -65°C. ACT TERRA
FIRMA is best used on contamination levels of 3% to 5% TPH. Contact Act BioRemediation
Products for usage on higher contamination levels.

Bioremediation Agents

94

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VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL MEAN

RED%



3 REPS/PROD

ALKANES
(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS



CONTROL

29,969

0

9,018

0

0

NUTRIENT

29,102

0

8,582

0



ACT TERRA
FIRMA

27,685

0

8,240

0



CONTROL

24,289

0

6,974

0

7

NUTRIENT

18,132

0

6,377

0



ACT TERRA
FIRMA

2,614

0

3,306

0



CONTROL

18,909

36.9

4,426

50.8

28

NUTRIENT

1,465

94.9

5,609

34.6

ACT TERRA
FIRMA

113

99.6

475

94.2

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28

Control
0.0%

Nutrient
17.0%

ACT Terra Firma
9.7%

b. Toxicity:

Material Tested
ACT TERRA FIRMA

No. 2 Fuel Oil

ACT TERRA FIRMA & No.
2 Fuel Oil (1:10)

Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
223.60 96-hr
74.10 48-hr
4.24 96-hr
1.99 48-hr
2.61 96-hr
1.19 48-hr
12.25 96-hr
12.27 48-hr

Bioremediation Agents

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VIII.	MICROBIOLOGICAL ANALYSIS

1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition of
the additive: CONFIDENTIAL

3.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: range 4.0 to 9.0

Temperature: range -20°C to 52°C

Salinity: Freshwater 0 to 500 ppm; Ocean Saltwater 35,000 ppm

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 3.0 and 13.0
Temperature: -50°C and 65°C
Salinity: Freshwater and 45,000 ppm

4.	Special nutrient requirements: Not applicable. DO NOT add fertilizers or nutrients.

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 0.8 g/cm3

5.	pH: 7.0-12.0

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: NA

8.	Additives: CONFIDENTIAL

9.	Solubility: <5% (estimated)

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.13

Barium	1.30

Cadmium	0.077

Chromium	0.17

Copper	NA

Lead	<0.25

Mercury	<0.00010

Selenium	0.67

Silver	<0.030

Bioremediation Agents	96 ACT TERRA FIRMA


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Zinc	NA

Cyanide	NA

Chlorinated Hydrocarbons	NA

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97

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TECHNICAL PRODUCT BULLETIN: B-72

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 2, 2018

"PETROCLEAN™"

I.	NAME, BRAND, OR TRADEMARK
PETROCLEAN™

Type of Product: Bioremediation Agent (Biological Additive/Microbiological Culture)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Green Earth Naturally, L L C.

2314 Ridgefield Street NE

Roanoke, V A 24102

Phone: (540) 362-5636

Fax:(540)362-9447

E-mail: chale@greenearthnaturally.com

Website: www.GreenEarthNaturally.com

(Mr. Carroll Hale III)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Green Earth Naturally, L L C.

2314 Ridgefield Street NE

Roanoke, V A 24102

Phone: (540) 362-5636

Fax:(540)362-9447

E-mail: chale@greenearthnaturally.com

Website: www. GreenEarthN aturally. com

(Mr. Carroll Hale III)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Use combination of general dilution ventilation and local exhaust ventilation to
keep exposure as low as possible.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Prevent skin and eye
contact by wearing appropriate personal protective equipment. If eye or skin irritation occurs,
flush with plenty of fresh water. Coveralls or other suitable protective garments should be worn
with suitable footwear for application and working conditions. Chemical safety goggles or
glasses and impervious gloves are recommended.

4.a.	Maximum storage temperature: below 120°F
4.b. Minimum storage temperature: above freezing

4.c. Optimum storage temperature range: 55°F to 100°F. Avoid storage in areas of extreme heat
or extreme cold. Store in tightly closed containers, and away from children.

4.d. Temperatures of phase separation and chemical changes: Stable

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V.	SHELF LIFE

Three to six months in sealed 1 gallon containers, 5 gallon buckets and 55 gallon drums or totes
(as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURE

PETROCLEAN™ is effective in bioremediating petroleum contaminated soils and is not
designed for use in open waters. There are no limitations to usage within optimum temperature
parameters.

1.	Application Method:

a.	Surficial spraying of PETROCLEAN™ may be applied by any type of liquid delivery
system.

i.	Soils and gravels can be treated with PETROCLEAN™ using a conventional yard
sprayer. Repetition may be needed.

ii.	PETROCLEAN™ can be applied to secondary containment areas, the key factor in
cleaning the contaminated substrate, whether gravel or soil, is residence time for the
microbes, moisture, and oxygen.

b.	Subsurface application can vary by location. Soil type becomes a contingent factor in
dilution rates and method of application. When bioremediating soils, cleaning the
contaminated substrate, whether gravel or soil, is affected by residence time for the
microbes, moisture, and oxygen.

i.	For in-situ soils, mix PETROCLEAN™ with water to the desired concentration and
dispense inoculated fluids in the subsurface, adjacent infrastructure, and the surface.

ii.	For ex-situ soils and longer term bioremediation projects, additional applications of
nutrients and oxygen releasing compounds may be required to maintain or boost
microbial activity.

2.	Concentration/Application Rate: Rates will vary based upon the type of soil and amount of
petroleum spilled, the extent of weathering, and other site-specific conditions, including soil
profiles, proximity to surface waters and wells. Heavy petroleum compounds such as crude
oil and bunker fuel, with a higher proportion of complex aliphatics, will require a higher
concentration of PETROCLEAN™ than lighter petroleum compounds such as gasoline.

a.	Hydrocarbon types: PETROCLEAN™ can be applied on any hydrocarbon compound
(including crude, diesel, gasoline, aviation fuel, bunker fuels, etc.) found in soils.

b.	Most frequent applications include any petroleum contamination around AST's and USTs
and containment pits requiring rehabilitation.

c.	Concentration Rate: on heavy oils, apply PETROCLEAN™ directly on the spill area
following absorption of free product, utilize a 1:10 dilution ratio (product to water).
Lighter oils will require a 1:30 (product to water) dilution ratio.

3. Conditions for Use: Bioremediation slows at temperatures below 40°F. No limitations as to
usage within optimum temperature parameters have been observed.

a.	Monitoring of dissolved oxygen levels is recommended. If needed, a mechanical aeration
device should be deployed or the use of Oxygen Releasing Compounds (ORC) should be
encouraged to maintain dissolved oxygen levels above 3 mg/L.

b.	Additional nutrients may be required to increase microbial activity over time if intrinsic
nutrients are depleted. The application of 10% nitrogen, 10% phosphorus, and 10%

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potassium fertilizer can be used in-situ or ex-situ as situations warrant to boost microbial
activity and enhance co-metabolic digestion of petroleum.

c.	Prevent spill run-off from entering surface water bodies.

d.	Eliminate all source of ignition.

e.	Dispose of used absorbent materials according to all local, regional, and federal
regulations.

II. TOXICITY AND EFFECTIVENESS
b. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL MEAN

RED%



3 REPS/PROD

ALKANES

(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS



CONTROL

57,032

0

12,547

0

0

NUTRIENT

55,231

0

12,458

0



PETROCLEAN™

58,148

0

12,141

0



CONTROL

55,126

0

12,091

0

7

NUTRIENT

47,951

0

11,599

0



PETROCLEAN™

34,095

0

8,640

0



CONTROL

50,608

11.2%

10,766

14.2%

28

NUTRIENT

34,291

37.9%

9,574

23.1%



PETROCLEAN™

14,854

74.4%

4,711

61.1%

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	PETROCLEAN™

7.83%	41.50%	60.93%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS

1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition of
the additive: CONFIDENTIAL

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3. Optimum pH, temperature, and salinity ranges for use of the additive:
pH: range 6.3 to 7.3
Temperature: range 55°F to 100°F
Salinity: 0 to 5%

3.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 6.0 and 8.0

Temperature: >32°F and <120°F
Salinity: no minimum and 10%

4.	Special nutrient requirements: NA

5.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

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TECHNICAL PRODUCT BULLETIN: B-73

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: MAY 21, 2019

"ECOBIOCLEAN® 100 COSW"

I.	NAME, BRAND, OR TRADEMARK
ECOBIOCLEAN® 100 COSW

Type of Product: Bioremediation Agent (Microbiological Culture, Enzyme Additive, Nutrient
Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

JACOR, LLC

1000 Brown Street, Suite 208
Wauconda, II. 60084
Phone: (847) 865-3189
Fax: (847) 865-3287

E-mail: info@ecobioclean.com or ianetangel@ecobioclean.com
Website: www.ecobioclean.com

(Dr. J an el Angel, CEO, Inventor)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

JACOR, LLC

1000 Brown Street, Suite 208
Wauconda, II. 60084
Phone: (847) 865-3189
Fax: (847) 865-3287

E-mail: info@ecobioclean.com or ianetangel@ecobioclean.com
Website: www.ecobioclean.com
(Dr. J an el Angel, CEO, Inventor)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Special ventilation is not required. Use standard industrial hygiene ventilation
practices. Use of a dust mask for respiratory protection in line with NIOSH standards such as
N100 (3M) quality or comparable products will provide adequate protection from non-oil-based
dust particles.

3.	Skin and eye contact; protective clothing; treatment in case of contact: To protect skin from
contact, standard work clothing and standard work or latex gloves will provide adequate
protection. In case of skin contact, wash with soap and water. To prevent eye contact, standard
safety glasses with side shields are recommended. In case of eye contact, flush with plenty of
water.

4.a.	Maximum storage temperature: 120°F (48°C) continuous up to 5 days.

4.b. Minimum storage temperature: 32°F (0.00 °C)

4.c. Optimum storage temperature range: 40°F (4.44°C) to 120°F (48°C).

Bioremediation Agents

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4.d. Temperatures of phase separation and chemical changes: Stable

V.	SHELF LIFE

Store product in a dry area. If kept in sealed container such as drums or totes (as delivered) at

temperatures below 100 °F, shelf life is 4-5 years.

VI.	RECOMMENDED APPLICATION PROCEDURE

4.	Application Method: ECOBIOCLEAN® 100 COSW is a multi-faceted bioremediation
product that may be applied directly in powder form or diluted with non-chlorinated water to
initiate degradation of crude oil (hydrocarbons) at the source of contamination such as on
shorelines, vegetation, or land. For powder treatment, apply directly to contamination site via
crop dusting implements, farm fertilizer apparatus, and planes for larger areas. For smaller
spills where powder form is desired, use fertilizer distributors, hand sprinklers, or other dry
nutrient delivery system. For liquid applications and after dilution, apply with any
commercially available spray apparatus, such as hand held tanks, back packs, and large
mixing tanks with pumping devices. In addition, ECOBIOCLEAN® 100 COSW may be
applied via educator systems from vessels, fire trucks, or any other appropriately outfitted
vehicle. Spraying/applying to the outer edges of contamination site first and then working
inward will help control spreading of spill.

5.	Concentration/Application Rate: Concentration rates will vary based upon the type of crude
oil spilled, the type of substrate and the amount of contamination spilled, the weathering
process, and environmental conditions. ECOBIOCLEAN® 100 COSW contains billions of
active hydrocarbon consuming microbes (MC) per gram along with a supporting proprietary
complex of nutrients (NA) and enzymes (EA), which together are bio-catalyzing elements
that stimulate bioremediation. ECOBIOCLEAN® 100 COSW may be applied to shorelines or
land in full strength powder form or diluted using native water supplies as required
depending upon the location of environmental contamination (do not use
municipal/chlorinated water for mixing). Product may be applied immediately after mixing
or within 12 hours via hoses or other spray devices or systems. Dilute 1:10 to 1:30(1 pound
product to 10-30 gallons native water) depending upon the type of contamination. For
example, heavy petroleum compounds such as crude oil or bunker fuel will require higher
dose of ECOBIOCLEAN® 100 COSW and lighter petroleum compounds will require less.
Nutrient additives are not necessary. Within minutes ECOBIOCLEAN® 100 COSW should
begin to penetrate the molecular walls initiating bioremediation. ECOBIOCLEAN® 100
COSW provides an inoculum that insures bacterial colonies consume hydrocarbons
throughout the remediation process. Within 3-7 days, there should be a noticeable reduction
of crude oil contamination and odor while population of microbial strains continue to
proliferate. Weathered oils may require longer treatment times. Diluted product can be
sprayed from a boat or aircraft to degrade surface oils on soil, beach/sand surface, or
vegetation. When dry application is preferred, such as in or around UST/AST and
containment pits, ECOBIOCLEAN® 100 COSW can be applied via powder distribution
implements as with seeding/fertilizing equipment or dry sprayers and then tilled for more
complete distribution of product to contaminant. Be certain to cover the entire contaminated
area for thorough treatment starting with perimeter and working to center. Product will
quickly begin to break the hydrocarbon structure into organic nutrient substances that aquatic

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and ground life can feed upon. In some circumstances (such as above) tilling of the ground is
advisable to insure higher oxygenation and that product is reaching offending chemical.
Within hours, odors should be greatly reduced, as may the hydrocarbon bonding properties
helping to prevent adhesion to vegetation, rocks, soil/earth, and wildlife. (Use only non-
chlorinated water for dilution.) Estimate area needing treatment. Use 1 pound of product
(dilute 1:10 to 1:25 product to gallons of water) per cubic yard of heavy crude oil spilled, or
10 pounds of product per acre of land depending upon the oil type, penetration depth and
concentration. Heavier oils may need greater biomass than lighter oils or fuels.
6. Conditions for Use: Product is effective in salt water or fresh water ecosystems including
marshlands, rocks, vegetation, sand, and soil (shorelines/land) with no limitations as to usage
within temperature parameters above 35°F and below 100°F. For greater immediate activity,
water temperature for optimal mixing is between 60-80°F, though you may mix with warmer
or colder non-chlorinated water between 45-105°F if need exists. Water salinity is not a
factor as ECOBIOCLEAN® 100 COSW works well with all forms of water. Weathered
crude/hydrocarbon contamination or tar-like substances may need to be agitated or tilled/cut
for shorter remediation time prior to or with application. For heavy oils use product directly
on the spill or up to approximately a 1:10 dilution ratio (1 pound product to 10 gallons of
water). Lighter oils would require a 1:10 to 1:30 product to water dilution ratio. In warmer
waters and in good agitation during application less product may be required.
ECOBIOCLEAN® 100 COSW will work more quickly when adequate oxygen levels exist at
contamination site but is viable wherever microbial life can be sustained.

II. TOXICITY AND EFFECTIVENESS
c. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL MEAN

RED%





MEAN









3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

65064

0

7360

0

0

NUTRIENT

57799

0

6452

0



PRODUCT

59661

0

6731

0



CONTROL

60375

0

5788

0

7

NUTRIENT

47685

0

5309

0



PRODUCT

33684

0

3888

0



CONTROL

55425

14.80

5874

20.20

28













NUTRIENT

27944

57.10

4041

45.10

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PRODUCT	6479	90.00	1789	75.70

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	ECOBIOCLEAN® 100 COSW

8.90%	51.50%	60.93%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS
Microbiological Cultures:

1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition
of the additive: CONFIDENTIAL

3.	Optimum pH, temperature, and salinity ranges for use of the additive:
pH: range 6.5 to 7.5

Temperature: range 75°F to 85°F
Salinity: 0.5 to 15.0%

4.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity:

pH: 5.5 and 11.0
Temperature: 32°F and 120°F

Salinity: maximum permissible salinity is up to 20% by solution

5.	Special nutrient requirements: NA

6.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

Enzyme Additives:

1.	Listing of each component of the total formulation, other than enzymes, by chemical and
percentage by weight: CONFIDENTIAL

2.	Enzyme(s): CONFIDENTIAL

3.	International Union of Biochemistry (I.U.B.) number(s): CONFIDENTIAL

4.	Source of enzyme: CONFIDENTIAL

5.	Units: No less than 1% and no more than 25% by weight.

6.	Specific Activity: CONFIDENTIAL

7.	Optimum Conditions:
pH: 7.0

Temperature: CONFIDENTIAL

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Salinity ranges for use of the additive: CONFIDENTIAL

Minimum and maximum pH: 4.5 to 8.5

Minimum and maximum temperature: CONFIDENTIAL

Minimum and maximum salinity levels above or below which the effectiveness of the
additive is reduced to half its optimum capacity: CONFIDENTIAL

8.	Enzyme shelf life: Up to 5 years if unopened and stored properly

9.	Enzyme optimum storage conditions: Low moisture environment at temperatures between
40°F and 115°F

Nutrient Additives:

1.	Listing of each component of the total formulation by chemical name and percentage by
weight: CONFIDENTIAL

2.	Nutrient additive optimum storage conditions: Store product in sealed containers and dry area
at temperatures between 40°F and 120°F.

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

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TECHNICAL PRODUCT BULLETIN: B-74

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 6, 2020

"SPILL GENIE™ 3T"

(aka, SG3T)

I. NAME, BRAND, OR TRADEMARK
SPILL GENIE™ 3T
(aka, SG3T)

Type of Product: Bioremediation Agent (Biological Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Product Owner/Primary Contact:	Product Manufacturer:

Spill Genie, LLC	Seatex Corporation

401 East Jackson Street (SunTrust Financial 445 Texas Highway 36
Center), Suite 2340	Rosenberg, TX 77417

Tampa, FL 33602	Phone: (713) 357-5300

Phone: (352) 515-3861	E-mail: kaimes@seatexcorp.com

Fax: (813) 807-3036	Website: www.seatexcorp.com

E-mail: rstotts@spill-genie.com	(Mr. Kelly Aimes)

Website: www.sg3t.com
(Mr. Rick Stotts, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Spill Genie, LLC

401 East Jackson Street (SunTrust Financial Center), Suite 2340

Tampa, FL 33602

Phone: (352) 515-3861

Fax: (813) 807-3036

E-mail: rstotts@spill-genie.com

Website: www.sg3t.com

(Mr. Rick Stotts, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-Hazardous)

2.	Ventilation: Recommended, ventilator in confined areas.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wear eye protection
and impervious gloves. Wash face, hands and any exposed skin thoroughly after handling. If eye
contact, wash eyes thoroughly for 15 minutes; including upper and lower lids and seek medical
attention. For skin contact, irritation is possible, wash with soap and water for 15 minutes. If
irritation persists, seek medical attention.

4.a.	Maximum storage temperature: Below 95°F.

4.b. Minimum storage temperature: Above 32°F.

4.c. Optimum storage temperature range: 55°F to 90°F. Avoid storage in extreme heat and

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extreme cold.

4.d. Temperatures of phase separation and chemical changes: Stable within storage temperature
ranges.

V.	SHELF LIFE

One year in the original unopened container, as delivered, under optimum storage conditions. It
is not recommended to store in open containers. Unused product stored in a properly sealed or air
tight container will have a diminished shelf life of less than one year.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Surficial spraying of Spill Genie™ 3T may be applied by a
conventional liquid delivery system used in the bioremediation industry.

a.	Spill Genie™ 3T is designated for use on soils, sandy or gravel applications. In-situ
and situ application can vary based on soil and surface composition. Spill Genie™ 3T
is pre-mixed into water and sprayed directly onto the hydrocarbon contaminants on
soils, sandy or gravel areas. Spill Genie™ 3T should be applied using recommended
dilution rates and utilizing a conventional sprayer or water dispensing cannon
(recommend application above 35°F, with optimum above 48°F). Reapplication may
be required to achieve desired results.

b.	When bioremediating contaminated substrate, whether sand, gravel or soil, additional
applications of nutrients, oxygen releasing compounds and or aeration may be
required to maintain or boost microbial activity.

2.	Concentration/Application Rate:

a.	Typical dilution is 1 gallon of Spill Genie™ 3T with 9 gallons of water
(approximately 1:10 dilution ratio, product to water). For lighter hydrocarbons, a
dilution ratio of up to 1:30, product to water). Apply 0.5 gallons of stock solution of
Spill Genie™ 3T to one cubic yard of contaminated soil. Agitate to slurry by mixing
thoroughly with contaminated soil. Application rate may vary due to level of
hydrocarbon contamination or type and density of treatable substrate.

b.	Hydrocarbon types: Spill Genie™ 3T can be applied on hydrocarbon compounds
including, but not limited to, crude, diesel, gasoline, aviation fuel, light oils, and
bunker fuels.

c.	Aged or asphaltic contaminants may be more resistant to remediation efforts and may
require multiple applications.

d.	Application rates of Spill Genie™ 3T may vary widely based on unknown extent and
depth of contamination.

3.	Conditions for Use:

a.	Most frequent applications include petroleum contamination around ASTs and USTs
(Above and Underground Storage Tanks) and containment pits requiring
rehabilitation.

b.	Optimum application temperature of Spill Genie™ 3T is above 48°F.

c.	Aeration of treated medium is recommended as it will increase oxygen levels within
the treated area allowing microbial reproductions and remediation activity to thrive.

d.	Additional nutrients may be required to increase microbial activity over time if
intrinsic nutrients are depleted. An application of nitrogen, phosphorus, and

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potassium fertilizer can be used in-situ or situ to boost microbial activity and enhance
co-metabolic digestion of petroleum.

e.	After treatment, solid asphaltic residue should be collected, removed from the site and
disposed of in accordance with applicable local, state and federal regulations.
Collection process and disposal of any excess washing solution, should comply with
applicable local, state and federal regulations.

f.	Prevent spill run-off from entering surface and sub-surface water bodies.

g.	Expected results in TPH (Total Petroleum Hydrocarbon) reduction have been
observed between 7 and 28 days.

II. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL
MEAN

RED%

TOTAL MEAN

RED%



3 REPS/PROD

ALKANES

(ppm)

28

DAYS

AROMATIC S
(ppm)

28

DAYS



CONTROL

46495

0

14656

0

0

NUTRIENT

43232

0

14090

0



PRODUCT

45979

0

13652

0



CONTROL

43141

0

12848

0

7

NUTRIENT

40276

0

12538

0



PRODUCT

33679

0

10128

0



CONTROL

37497

19.3%

12332

15.9%

28

NUTRIENT

22732

47.4%

10686

24.2%



PRODUCT

14482

68.5%

7538

44.4%

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	SPILL GENIE™ 3T

14.5%	35.0%	57.0%

b. Toxicity:

NA

VIII. MICROBIOLOGICAL ANALYSIS
Microbiological Cultures:

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1.	Listing of each component of the total formulation, other than microorganisms, by chemical
name and percentage by weight: CONFIDENTIAL

2.	Listing of all microorganisms by species and percentages of each species in the composition
of the additive: CONFIDENTIAL

3.	Optimum pH, temperature, and salinity ranges for use of the additive: CONFIDENTIAL

4.	Minimum and maximum pH, temperature, and salinity levels below or above which the
effectiveness of the additive is reduced to half its optimum capacity: CONFIDENTIAL

5.	Special nutrient requirements: NA

6.	Test results regarding the determination of the presence of the following:

Salmonella: Negative

Fecal coliform: Negative
Shigella: Negative

Staphylococcus Coagulase positive: Negative
Beta hemolytic Streptococci: Negative

Enzyme Additives:

1.	Listing of each component of the total formulation, other than enzymes, by chemical and
percentage by weight: CONFIDENTIAL

2.	Enzyme(s): CONFIDENTIAL

3.	International Union of Biochemistry (I.U.B.) number(s): CONFIDENTIAL

4.	Source of enzyme: CONFIDENTIAL

5.	Units: CONFIDENTIAL.

6.	Specific Activity: CONFIDENTIAL

7.	Optimum Conditions: CONFIDENTIAL

8.	Enzyme shelf life: CONFIDENTIAL

9.	Enzyme optimum storage conditions: CONFIDENTIAL

Nutrient Additives: NA

IX.	PHYSICAL PROPERTIES

NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

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TECHNICAL PRODUCT BULLETIN: B-75

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 08, 2021

"GHG ORGANIC"

I.	NAME, BRAND, OR TRADEMARK
GHG ORGANIC

Type of Product: Bioremediation Agent (Nutrient Additive)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Bucheus Investments LLC
4320 NW 72nd Avenue
Miami, FL 33166

Phone: +56-9-79128229 (WhatsApp Phone Number)

Phone: (786) 521-0074 (Christian Alonso)

Phone: (786) 436-9498 (Rene Mendoza)

E-mail: asroiasl261@gmail.com

(Mr. Alberto Rojas P., CEO)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Bucheus Investments LLC
4320 NW 72nd Avenue
Miami, FL 33166

Phone: +56-9-79128229 (WhatsApp Phone Number)

Phone: (786) 521-0074 (Cristian Alonso)

Phone: (786) 436-9498 (Rene Mendoza)

E-mail: asroiasl261@gmail.com

(Mr. Alberto Rojas P., CEO)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Wearing masks with filter for fine dust under MESH 200 is recommended.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wear goggles for eye
protection, impervious gloves, and normal work clothing. Contact may cause mild irritation.
Wash face, hands, and any exposed skin thoroughly after handling. For eye contact, wash eyes
thoroughly with clean water until irritation disappears. For skin contact and in case of redness or
rash, wash the affected area with clean water until irritation disappears. If irritation persists, seek
medical attention.

4.a.	Maximum storage temperature: 140°F.

4.b. Minimum storage temperature: -10°F.

4.c. Optimum storage temperature range: -4°F to 104°F.

4.d. Temperatures of phase separation and chemical changes: Stable in powder form under all
conditions. GHG ORGANIC in its natural states does not agglomerate or bind due to moisture. It
does not require any type of additive to preserve its properties.

Bioremediation Agents

111

GHG ORGANIC


-------
V.	SHELF LIFE

Five years in open container; and four years in pressurized containers. Pressurized containers
include portable extinguisher with N2 gas at 25 pounds working pressure 100 psi with metal
anticorrosive valve made of 1/16-inch-thick carbon steel. Store in closed and dry places (e.g.,
containers, closed metal/wooden warehouses). Keep in manufacturers closed containers and store
in height according to the resistance that bagged containers or pallets indicate, not to have a
column with more than 2,000 pounds. Do not store volumes greater than 20,000 pounds in bulk
in closed warehouses less than 1,000 yards from the vicinity of swamps of stagnant waters.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: GHG ORGANIC is a homogenous powder that is applied directly to oil
contaminated solid surfaces (e.g., soil, sand, shorelines, and vegetation). Apply directly from
container, product should not be diluted in water or mixed with other substances or solvents.
Distribute GHG ORGANIC directly and uniformly on the spilled oil from containers (such as
buckets and maxi bags) on the solid surface. For remote areas, apply using pressurized
extinguishers with N2 gas (manual extinguishers from 2 pounds to 100 pounds) on solid
surfaces. Means of application:

a.	From all terrain trucks, distribute GHG ORGANIC using 50-yard x 1 inch rubber hose of
medium pressure (8 bar) coupled with:

i.	<5,000-pound tank mounted on pressurized pickup with N2 gas at 200 psi.

ii.	Compressed air 250 CFM and 8 bar working pressure mounted on a truck to pull
product directly from open containers using a VENTURI so that GHG ORGANIC is
projected onto the spilled oil on the solid surface.

b.	For difficult to access environments such as edges of islets and cliffs, recommend
distributing GHG ORGANIC:

i.	From boats using 50-yard x 1-inch-long rubber hoses of medium pressure (8 bar)
coupled to a compressed air compressor. 250 CFM and 8 bar working pressure is used
to pull product directly from open containers using a VENTURI.

ii.	From planes and helicopters, GHG ORGANIC is available in plastic tanks that
discharge the compound by gravity from gravitational sprinklers mounted on the
discharge pipes outside the equipment. The application rate of the compound will be
defined based on the surface affected by the spill.

2.	Concentration/Application Rate: Applied at a ratio of 2 pounds product per square yard of
oil; or 8,800 pounds of product per acre of oil.

3.	Conditions for Use: Time of bioremediation is dependent upon oil density and ambient
temperature. For light oils, bioremediation is 30 days. For heavy fuel oils, bioremediation is
90 days. A second application may be necessary in areas of accumulation. In case of oil
seepage to the subsoil due to old spills in permeable soils and to accelerate the
bioremediation process, the manufacturer recommends removing the contaminated soil and
mixing GHG ORGANIC using vibratory screens and industrial blending machines.

Bioremediation Agents

112

GHG ORGANIC


-------
VII. TOXICITY AND EFFECTIVENESS
a. Effectiveness:

Bioremediation Agent Effectiveness Test (40 CFR 300.900), Federal Register September 15,
1994:

Summary Data Table

DAYS

PRODUCT

TOTAL

RED%

TOTAL MEAN

RED%





MEAN









3 REPS/PROD

ALKANES

28

AROMATIC S

28





(ppm)

DAYS

(ppm)

DAYS



CONTROL

39682

0

5055

0

0

NUTRIENT

38370

0

5578

0



PRODUCT

38358

0

4699

0



CONTROL

38159

0

4797

0

7

NUTRIENT

36956

0

5575

0



PRODUCT

31488

0

4270

0



CONTROL

37517

5.5%

4871

3.6%

28

NUTRIENT

29986

21.8%

4822

13.5%



PRODUCT

13599

64.7%

3074

34.6%

Results of Gravimetric Analysis:

Percentage (%) Decrease in Weight of Oil on Day 28
Control	Nutrient	GHG ORGANIC

7.0%	15.1%	52.5%

b. Toxicity:

NA

VIII.	MICROBIOLOGICAL ANALYSIS

The product is a nutrient additive and does not contain microbiological cultures or enzyme
additives.

1.	Listing of each component of the formulation by chemical name and percentage by weight:
CONFIDENTIAL

2.	Optimum storage conditions:

Temperature: -4.0°F to 104°F

IX.	PHYSICAL PROPERTIES

NA

Bioremediation Agents

113

GHG ORGANIC


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

NA

Bioremediation Agents

114

GHG ORGANIC


-------
DISPERSANTS: TECHNICAL
NOTEBOOK BULLETINS

115


-------
TECHNICAL PRODUCT BULLETIN #D-1

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 10, 1978

REVISED LISTING DATE: DECEMBER 18, 1995

"COREXIT™ EC9527A"

I.	NAME, BRAND, OR TRADEMARK
COREXIT™ EC9527A

Type of Product: Dispersant
(formerly COREXIT 9527)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: COREXIT™ EC9527A is not classified as flammable by either DOT or IMO
regulations.

2.	Ventilation: Avoid prolonged breathing of vapors. Use with ventilation equal to unobstructed
outdoors in moderate breeze.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact. In
case of eye contact, immediately flush eyes with large amounts of water for at least 15 minutes.
Get prompt medical attention. Avoid contact with skin and clothing. In case of skin contact,
immediately flush with large amounts of water, and soap if available. Remove contaminated
clothing, including shoes, after flushing has begun. If irritation persists, seek medical attention.
For open systems where contact is likely, wear long sleeve shirt, chemical resistant gloves, and
chemical protective goggles.

4.a.	Maximum storage temperature: 170°F
4.b. Minimum storage temperature: -30°F

4.c. Optimum storage temperature range: 40°F to 100°F

Dispersants

116

COREXIT™ EC9527A


-------
4.d. Temperatures of phase separations and chemical changes: COREXIT™ EC9527A is not
adversely affected by changes in storage temperature unless evaporation is allowed to occur.

V.	SHELF LIFE

The shelf life of unopened drums of COREXIT™ EC9527A is unlimited. Containers should
always be capped when not in use to prevent contamination and evaporation of solvents.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: COREXIT™ EC9527A is most effectively applied by aircraft, however,
application with boat spray booms, boat fire monitors, and by hand held sprayers and back packs
has been successfully done on a number of spills and trials.

Aerial Spraying - Aircraft provide the most rapid method of applying dispersants to an oil spill
and a variety of aircraft can be used for spraying. For aerial spraying, COREXIT™ EC9527A is
applied undiluted. Typical application altitudes of 30 to 50 feet have been used, although higher
altitudes may be effective under certain conditions. Actual effective altitudes will depend on the
application equipment, weather and aircraft. Careful selection of spray nozzles is critical to
achieve desired dose levels, since droplet size must be controlled. Many nozzles used for
agricultural spraying are of low capacity and produce too fine a spray. A quarter-inch open pipe
may be all that is necessary if the aircraft travels at 120 mph (104 knots) or more, since the air
shear at these speeds will be sufficient to break the dispersant into the proper sized droplets.

Boat Spraying - COREXIT™ EC9527A may be applied by workboats equipped with spray
booms mounted ahead of the bow wake or as far forward as possible. The preferred and most
effective method of application from a workboat is to use a low-volume, low-pressure pump so
the chemical can be applied undiluted. Spray equipment designed to provide a five to ten
percent diluted dispersant solution to the spray booms can also be used. COREXIT™ EC9527A
should be applied as droplets, not fogged or atomized. Natural wave or boat wake action usually
provides adequate mixing energy to disperse the oil.

Recent tests have indicated that a fire monitor modified with a screen cap for droplet size may
also be useful for applying COREXIT™ EC9527A. Due to the increased volume output and the
greater reach of the fire monitor, significantly more area can be covered in a shorter period of
time.

System Calibration - Spray systems should be calibrated at temperatures anticipated to insure
successful application and dosage control.

2.	Concentration/Application Rate: A treatment rate of about 2 to 10 U.S. gallons per acre, or a
dispersant to oil ratio of 1:50 to 1: 10 is recommended. This rate varies depending on the type of
oil, degree of weathering, temperature, and thickness of the slick.

3.	Conditions for Use: As with all dispersants, timely application ensures the highest degree of
success. Early treatment with COREXIT™ EC9527A, even at reduced treat rates, can reduce the
"mousse" forming tendencies of the spilled oil. COREXIT™ EC9527A is useful on oil spills in
salt water.

Dispersants

117

COREXIT™ EC9527A


-------
VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50

(DDm)

COREXIT™ EC9527A

Menidia beryllina

14.57

96-hr



Mysidopsis bahia

24.14

48-hr

No. 2 Fuel Oil

Menidia beryllina

10.72

96-hr



Mysidopsis bahia

16.12

48-hr

COREXIT™ EC9527A &

Menidia beryllina

4.49

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

6.60

48-hr

Reference Toxicant (DSS)

Menidia beryllina

7.07

96-hr



Mysidopsis bahia

9.82

48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%)

Prudhoe Bay Crude	37.4

South Louisiana Crude	63.4

Average of Prudhoe Bay and South Louisiana Crudes	50.4

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 163°F

2.	Pour Point: < - 40°F

3.	Viscosity: 160 cSt at 32°F

4.	Specific Gravity: 0.98 - 1.02

5.	pH: 6.1

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: Water, Propylene Glycol, 2-Butoxyethanol

8.	Additives: CONFIDENTIAL

9.	Solubility: Complete

Dispersants

118

COREXIT™ EC9527A


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)
<0.005
<0.01
1.0
<0.2
<0.1
<0.003
<0.1
0.1
<0.01
<0.01

Dispersants

119

COREXIT™ EC9527A


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #D-2
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: APRIL 22, 1985
REVISED LISTING DATE: JANUARY 26, 1996
"NEOS AB3000"

I.	NAME, BRAND, OR TRADEMARK
NEOS AB3000

Type of Product: Dispersant (Hydrocarbon Solvent Based)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
NEOS Company Limited

Daisan Kendai Building
1-2, 3-chome Isobedori
Chuo-ku, Kobe, 651-0084 Japan
Phone: updated information required
E-mail: updated information required
(Mr. T. Ishii, Manager)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
NEOS Company Limited

Daisan Kendai Building

1-2, 3-chome Isobedori

Chuo-ku, Kobe, Japan

Phone: updated information required

E-mail: updated information required

(Mr. T. Ishii, Manager)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: NEOS AB3000 is flammable; keep away from open flame.

2.	Ventilation: Special ventilation is not required; however, natural ventilation is recommended.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Contact may cause skin
and eye irritation. Goggles and rubber clothing are recommended during application.

In case of contact with skin or eye, flush with copious amounts of fresh water. If severe, consult
a doctor.

4.a.	Maximum storage temperature: 158°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 50°F to 140°F

4.d. Temperatures of phase separations and chemical changes: Phase separation and chemical
changes do not appear between the temperature range of 32°F to 158°F.

V.	SHELF LIFE

3/18/2016
7/27/2022

Dispersants

120

NEOS AB3000


-------
The shelf life is five (5) years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray neat concentrate on the oil slick in atomized form by means of a
manual pump, or spray with a pump system incorporating an ejector system for drawing
concentrate from the drum or stock tank.

For aerial application, use a spray boom with pressure nozzles or rotating atomizers mounted on
helicopters or airplanes.

2.	Concentration/Application Rate: The application rate is 65 gallons of dispersant per ton of oil.
Five (5) to fifteen (15) parts of dispersant to suctioned water is recommended for ejector
systems.

For aerial application, 75 to 125 gallons per ton of oil is recommended.

3.	Conditions for Use: NEOS AB3000 can be used in salt water. It is effective with crude and
residual heavy oil. The dispersant is also effective at controlling volatile emissions from the oil.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (DDm)

NEOS AB3000

Menidia beryllina

91.1 96-hr



Mysidopsis bahia

33.0 48-hr

No. 2 Fuel Oil

Menidia beryllina

201.8 96-hr



Mysidopsis bahia

11.5 48-hr

NEOS AB3000 &

Menidia beryllina

57.0 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

25.0 48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.5 96-hr



Mysidopsis bahia

9.3 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH LOUISIANA

(S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%)

Prudhoe Bay Crude	19.7

South Louisiana Crude	89.8

Average of Prudhoe Bay and South Louisiana Crudes	54.8

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES
1. Flash Point: No flash point to 212°F

Dispersants

121

NEOS AB3000


-------
2.	Pour Point: Less than 32°F

3.	Viscosity: 30.7 cSt at 104°F

4.	Specific Gravity: 0.924 at 59°F

5.	pH: 8.0 (5wt % aq., at 77°F)

6.	Surface Active Agents: Nonionic and Cationic surfactants

7.	Solvents: Paraffin

8.	Additives: None

9.	Solubility: NA

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.1

Cadmium	<0.1

Chromium	0.26

Copper	<0.05

Lead	0.21

Mercury	<0.001

Nickel	0.076

Zinc	1.1

Cyanide	<0.05

Chlorinated Hydrocarbons	<0.10

Dispersants

122

NEOS AB3000


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/22/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #D-3

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: FEBRUARY 23, 1988

REVISED LISTING DATE: JANUARY 26, 1996

"MARE CLEAN 200"

I.	NAME, BRAND, OR TRADEMARK
MARE CLEAN 200

Type of Product: Dispersant (Solvent-Based)

(formerly MARE CLEAN 505)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Ichinen Chemicals Co., Ltd

Mita Twin Building, East Wing 8F
4-2-8 Shibaura, Minato-ku,

Tokyo, Japan 108-0023
Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Mr. Tsuyoshi Imai)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Ichinen Chemicals Co., Ltd

Mita Twin Building, East Wing 8F
4-2-8 Shibaura, Minato-ku
Tokyo, Japan 108-0023
Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Mr. Tsuyoshi Imai)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: The flash point is 212°F @ 20°F

2.	Ventilation: Is required. Use in closed room is not recommended.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Use protective goggles
to avoid eye contact. In case of eye contact, wash immediately with plenty of water and consult
with physician.

4.a.	Maximum storage temperature: 122°F
4.b. Minimum storage temperature: 21°F

4.c. Optimum storage temperature range: 32°F to 86°F

4.d. Temperatures of phase separations and chemical changes: Phase separation does not relate to
temperatures. Chemical changes may occur at temperatures above 194°F.

Dispersants

123

MARE CLEAN 505


-------
V.	SHELF LIFE

The shelf life of MARE CLEAN 200 is 10 years when stored indoors. (Container will
deteriorate before contents.)

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Sprinkle the dispersant on the oil spill, then 5-10 minutes later stir the
surface intensively. For convenience, MARE CLEAN 200 may be diluted with water if desired.

2.	Concentration/Application Rate: Use 53-66 gallons of MARE CLEAN 200 per ton of oil

3.	Conditions for Use: The performance of MARE CLEAN 200 is not affected by water salinity.
At temperatures below 40°F or in case of heavy crude oil spill, MARE CLEAN 200 should be
used without dilution. MARE CLEAN 200 is an effective dispersant for any liquid hydrocarbon.

VII.	TOXICITY AND EFFECTIVENESS
1. Toxicity:

Material Tested

Species

LC50 (DDm)

MARE CLEAN 200

Menidia beryllina

1996.00

96-hr



Mysidopsis bahia

938.00

48-hr

No. 2 Fuel Oil

Menidia beryllina

10.72

96-hr



Mysidopsis bahia

16.12

48-hr

MARE CLEAN 200 and

Menidia beryllina

42.00

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

9.84

48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.07

96-hr



Mysidopsis bahia

9.82

48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OILS

Oil	Effectiveness (%)

Prudhoe Bay Crude	63.97

South Louisiana Crude	84.14

Average of Prudhoe Bay and South Louisiana Crudes	74.06

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 212°F@ 20°F

2.	Pour Point: 14 @ 10°F

3.	Viscosity: 2.4 @ 5 cSt at 104°F

4.	Specific Gravity: 0.95 @ 0.03 at 77°F

5.	pH: 7.7 @ 1.0 (10% solution)

Dispersants

124

MARE CLEAN 505


-------
6.	Surface Active Agents: A mixture of sorbitan fatty acid esters, polysorbates, and
polyoxyethylene fatty acid esters.

7.	Solvents: Paraffinic hydrocarbons (CAS 74664-93-0)

8.	Additives: None

9.	Solubility: NA

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.50

Cadmium	<0.100

Chromium	<0.500

Copper	<0.250

Lead	<2.50

Mercury	<0.0200

Nickel	<0.250

Zinc	0.611

Cyanide	<0.01

Chlorinated Hydrocarbons	<0.10

Dispersants

125

MARE CLEAN 505


-------
TECHNICAL PRODUCT BULLETIN #D-4

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: APRIL 13, 1994

REVISED LISTING DATE: DECEMBER 18, 1995

"COREXIT™ EC9500A"

I.	NAME, BRAND, OR TRADEMARK
COREXIT™ EC9500A

Type of Product: Dispersant
(formerly COREXIT 9500)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-flammable; DOT - Non-hazardous.

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in moderate breeze.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact. In
case of eye contact, immediately flush eyes with large amounts of water for at least 15 minutes.
Get prompt medical attention. Avoid contact with skin and clothing. In case of skin contact,
immediately flush with large amounts of water, and soap if available. Remove contaminated
clothing, including shoes, after flushing has begun. If irritation persists, seek medical attention.
For open systems where contact is likely, wear long sleeve shirt, chemical resistant gloves, and
chemical protective goggles.

4.a.	Maximum storage temperature: 170°F
4.b. Minimum storage temperature: -30°F

4.c. Optimum storage temperature range: 40°F to 100°F

4.d. Temperatures of phase separations and chemical changes: None

Dispersants

126

COREXIT™ EC9500A


-------
V.	SHELF LIFE

The shelf life of unopened drums of COREXIT™ EC9500A is unlimited. Containers should
always be capped when not in use to prevent contamination and evaporation of solvents.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: COREXIT™ EC9500A contains the same surfactants present in
COREXIT™ EC9527A and a new improved oleophilic solvent delivery system.

Aerial Spraying - Aircraft provide the most rapid method of applying dispersants to an oil spill
and a variety of aircraft can be used for spraying. For aerial spraying, COREXIT™ EC9500A is
applied undiluted. Typical application altitudes of 30 to 50 feet have been used, although higher
altitudes may be effective under certain conditions. Actual effective altitudes will depend on the
application equipment, weather and aircraft. Careful selection of spray nozzles is critical to
achieve desired dose levels, since droplet size must be controlled. Many nozzles used for
agricultural spraying are of low capacity and produce too fine a spray. A quarter-inch open pipe
may be all that is necessary if the aircraft travels at 120 mph (104 knots) or more, since the air
shear at these speeds will be sufficient to break the dispersant into the proper sized droplets.

Boat Spraying - COREXIT™ EC9500A may also be applied by workboats equipped with spray
booms mounted ahead of the bow wake or as far forward as possible. The preferred and most
effective method of application from a workboat is to use a low-volume, low-pressure pump so
the chemical can be applied undiluted. Spray equipment designed to provide a five to ten
percent diluted dispersant solution to the spray booms can also be used. COREXIT™ EC9500A
should be applied as droplets, not fogged or atomized. Natural wave or boat wake action usually
provides adequate mixing energy to disperse the oil.

Recent tests have indicated that a fire monitor modified with a screen cap for droplet size control
may also be useful for applying COREXIT™ EC9500A. Due to the increased volume output
and the greater reach of the fire monitor, significantly more area can be covered in a shorter
period of time.

System Calibration - Spray systems should be calibrated at temperatures anticipated to insure
successful application and dosage control. Application at sub-freezing temperatures may require
larger nozzle, supply lines and orifices due to higher product viscosity.

2.	Concentration/Application Rate: A treatment rate of about 2 to 10 U.S. gallons per acre, or a
dispersant to oil ratio of 1:50 to 1:10 is recommended. This rate varies depending on the type of
oil, degree of weathering, temperature, and thickness of the slick.

3.	Conditions for Use: As with all dispersants, timely application ensures the highest degree of
success. Early treatment with COREXIT™ EC9500A, even at reduced treat rates, can also
counter the "mousse" forming tendencies of the spilled oil. COREXIT™ EC9500A is useful on
oil spills in salt water.

Dispersants

127

COREXIT™ EC9500A


-------
VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (ppm)

COREXIT™ EC9500A

Menidia beryllina

25.20 96-hr



Mysidopsis bahia

32.23 48-hr

No. 2 Fuel Oil

Menidia beryllina

10.72 96-hr



Mysidopsis bahia

16.12 48-hr

COREXIT™ EC9500A &

Menidia beryllina

2.61 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

3.40 48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.07 96-hr



Mysidopsis bahia

9.82 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OILS

Oil	Effectiveness (%)

Prudhoe Bay Crude	45.3

South Louisiana Crude	54.7

Average of Prudhoe Bay and South Louisiana Crudes	50.0

VIII.	MICROBIOLOGICAL PROPERTIES

NA

IX.	PHYSICAL PROPERTIES

1.	FlashPoint: 181.4°F

2.	Pour Point: <-71°F

3.	Viscosity: 22.5 cSt at 104°F

4.	Specific Gravity: 0.95 at 60°F

5.	pH: 6.2

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

9.	Additives: None

10.	Solubility: Miscible

Dispersants

128

COREXIT™ EC9500A


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.16

Cadmium	ND

Chromium	0.03

Copper	0.10

Lead	ND

Mercury	ND

Nickel	ND

Zinc	ND

Cyanide	ND

Chlorinated hydrocarbons	ND

Dispersants

129

COREXIT™ EC9500A


-------
TECHNICAL PRODUCT BULLETIN #D-5

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: APRIL 22, 1999

"DISPERSIT SPC 1000™"

(aka, SEACARE E.P.A. (ECOSPERSE™ POLLUTION ABATEMENT))

I.	NAME, BRAND, OR TRADEMARK
DISPERSIT SPC 1000™

(aka, SEACARE E.P.A. (ECOSPERSE™ POLLUTION ABATEMENT))

Type of Product: Dispersant (Water Based)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
U.S. Polychemical Corp.

584 Chestnut Ridge Road
Chestnut Ridge, NY 10977
Phone: (845) 356-5530
Fax: (845)356-6656
E-mail: bruceg@uspoly.com
(Mr. Bruce Gebhardt)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
U.S. Polychemical Corp.

584 Chestnut Ridge Road
Chestnut Ridge, NY 10977
Phone: (845) 356-5530
Fax: (845)356-6656
E-mail: bruceg@uspoly.com
(Mr. Bruce Gebhardt)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO: Non-flammable; DOT: Non-hazardous

2.	Ventilation: None normally required. Adequate to maintain fume levels below the TLV.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid prolonged
contact with skin and eyes. Flush eyes with plenty of water for at least 15 minutes. Get medical
attention. Wear long sleeve shirt, chemical resistant gloves, and chemical protective goggles in
case of exposure to mist.

4.a.	Maximum storage temperature: 180°F
4.b. Minimum storage temperature: -25°F

4.c. Optimum storage temperature range: 40°F to 140°F

4.d. Temperatures of phase separations and chemical changes: None

Dispersants

130

DISPERSIT SPC 1000™


-------
V.	SHELF LIFE

The shelf life of DISPERSIT SPC 1000™ is unlimited in unopened containers. Containers must
be kept closed when not in use to prevent contamination.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: The dispersant may be applied by any conventional methods such as 1)
aerial spraying and 2) boat spraying to accommodate weather conditions.

2.	Concentration/Application Rate: A dispersant to oil ratio ranging from 1 part dispersant to 50
parts oil to 1 part dispersant to 10 parts oil; or an application rate of about 2-10 gallons (7.6
liters- 37.9 liters) per acre (4840 square meters) is suggested. These rates will be dependent on
the type of oil, degree of weathering, temperature and extent of oil slick.

3.	Conditions for Use: Timely application ensures the highest degree of successful dispersion of
the oil spill.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

DISPERSIT SPC 1000™

Menidia beryllina

3.5 96-hr



Mysidopsis bahia

16.6 48-hr

No. 2 Fuel Oil

Menidia beryllina

11.6 96-hr



Mysidopsis bahia

11.7 48-hr

DISPERSIT SPC 1000™

Menidia beryllina

7.9 96-hr

& No. 2 Fuel Oil (1:10)

Mysidopsis bahia

8.2 48-hr

Reference Toxicant (SDS)

Menidia beryllina

6.3 96-hr



Mysidopsis bahia

11.7 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH LOUISIANA
(S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness

Prudhoe Bay Crude	40

South Louisiana Crude	105

Average of Prudhoe Bay and South Louisiana Crudes	73

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM D-56-87: 208°F

2.	Pour Point, ASTM D-97-87: <-20°C

3.	Viscosity, ASTM D-445-88: 144CPS, @ 68°F

4.	Specific Gravity, ASTM D-1298-85(90): 0.995, @ 68°F

5.	pH, ASTM D-1293-84(90): 10.0

6.	Surface Active Agents: Anionic and non-ionic, proprietary, surfactants

7.	Solvents: Proprietary, non-petroleum based

8.	Additives: None

Dispersants

131

DISPERSIT SPC 1000™


-------
9. Solubility in Water: Complete

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.00

Cadmium	<2.00

Chromium	<2.00

Copper	<2.00

Lead	<1.00

Mercury	<0.04

Nickel	<10.00

Zinc	<2.00

Cyanide	<2.00

Chlorinated Hydrocarbons	<5.00

Dispersants

132

DISPERSIT SPC 1000™


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #D-6
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: SEPTEMBER 20, 2000
"JD-109"

I.	NAME, BRAND, OR TRADEMARK
JD-109

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76571

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76571

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Nonflammable; DOT - Nonhazardous

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in a moderate breeze.

3.	Skin and eye contact, protective clothing, treatment in case of contact: Avoid skin and
clothing contact. If skin contact occurs, immediately wash with large amounts of soap and water
(if possible). Remove any contaminated clothing and shoes. Launder before reusing. If
irritation persists, seek medical assistance. For areas where contact is likely, wear long sleeve
shirt, chemical resistant gloves, and chemical resistant goggles.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: - 4°F

4.c. Optimum storage temperature range: 32°F to 90°F

4.d. Temperatures of phase separations and chemical changes: None

3/22/2016
7/27/2022

Dispersants

133

JD-109


-------
V.	SHELF LIFE

The shelf life of unopened drums of JD-109 in unlimited. Containers should be capped when not
being used to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: The most rapid and effective method of applying JD-109 to a oil spill is
by spraying. Temperature ranges for application should not drop below 32°F or exceed 120°F.

Aerial Spraying - Typical application altitudes of 30 to 50 feet are advised although higher
altitudes may be used if conditions warrant. Spray nozzle should be about Vi inches in diameter
flying at 104 knots or more to create enough water shear sufficient to break the dispersant into
proper sized droplets. A V2 inch diameter nozzle may be needed for temperatures below 50°F.

Boat Spraying - JD-109 can also be applied by workboats with spray booms mounted as far
forward as possible of the bow or wake. The most effective application from a workboat is a
low-volume, low-pressure pump.

2.	Concentration/Application Rate: A treatment rate of about 2 to 10 US gallons (7.6 to 37.9
liters) per acre (4,840 square meters) or a dispersant to oil ratio of 1:50 to 1:10 is recommended.
The rate may vary depending on the type of oil, degree of weathering, temperature and thickness
of slick.

3.	Conditions for Use: As with any oil related spill, timely application of a dispersant will ensure
the highest degree of success. Timely treatment with JD-109, even at low application rates, can
counter the "mousse" forming effect of the spilled oil.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

JD-109

No. 2 Fuel Oil

JD-109 & No. 2 Fuel Oil
(1:10)

Reference Toxicant (SRT)

LC50 (ppm)
1.90 96-hr
1.18 48-hr
96-hr
48-hr

9.35
3.13

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH LOUISIANA
(S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

on

Prudhoe Bay Crude
South Louisiana Crude

Average of Prudhoe Bay and South Louisiana Crudes

3.84 96-hr
3.51 48-hr
2.63 96-hr
8.06 48-hr

Effectiveness (°/
26
91
58.5

Dispersants

134

JD-109


-------
VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM D3278-89: 93°C

2.	Pour Point, ASTM D97-87: -19°C

3.	Viscosity, ASTM D445-88: 202.9 cSt

4.	Specific Gravity, ASTM D1298-85 (90): 1.02

5.	pH, ASTM D1293-84 (90): 9.45

6.	Surface Active Agents: Anionic and nonionic, proprietary, surfactants

7.	Solvents: Proprietary, ester based

8.	Additives: None

9.	Solubility in Water: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<10

Cadmium	<10

Chromium	<10

Copper	<10

Lead	<10

Mercury	<1

Nickel	<10

Zinc	<10

Cyanide	<0.5

Chlorinated Hydrocarbons	<1.4

Dispersants

135

JD-109


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

5/18/2006
7/27/2022

TECHNICAL PRODUCT BULLETIN #D-7

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 06, 2001

"JD-2000™"

I.	NAME, BRAND, OR TRADEMARK
JD-2000™

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76571

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76571

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-flammable. This product is not regulated by DOT when shipped
domestically by land.

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in a moderate breeze.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid skin and
clothing contact. If skin contact occurs, immediately wash with large amounts of soap and water
(if possible). Remove any contaminated clothing and shoes. Launder before reusing. If
irritation persists, seek medical assistance. For areas where contact is likely, wear long sleeve
shirt, chemical resistant gloves, and chemical resistant goggles.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: -30°F

4.c. Optimum storage temperature range: 30°F to 90°F

4.d. Temperatures of phase separations and chemical changes: None

Dispersants

136

JD-2000™


-------
V.	SHELF LIFE

The shelf life of unopened drums of JD-2000™ is unlimited. Containers should be capped when
not being used to prevent contamination and evaporation. Opened container should be used
within 1 year for optimal performance. Poly containers are recommended for storage near wet
environments, i.e., ships, harbors, ports, etc.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: JD-2000™ is free of phosphates, aromatic chlorinated solvents, branched
ethoxylated alcohols, and hydrotreated distillates. Optimum temperature for application is above
30°F.

Aerial Spraying - Typical application altitudes of 30 to 50 feet are advised although higher
altitudes may be used if conditions warrant. Spray nozzle should be about Vi inch in diameter
flying at 104 knots or more to create enough air shear sufficient to break the dispersant into
proper sized droplets. A V2 inch diameter nozzle may be needed for temperatures from 30°F to
30°F.

Boat Spraying - JD-2000™ can also be applied by workboats with spray booms mounted as far
forward as possible of the bow or wake. The most effective application from a workboat is a
low-volume, low-pressure pump.

2.	Concentration/Application Rate: JD-2000™ is an oil spill dispersant concentrate that may be
diluted by 5 to 10 percent with water if needed. A treatment rate of about 2 to 10 U.S. gallons
(7.6 to 37.9 liters) per acre (4,840 square meters) or a dispersant to oil ratio of 1:50 to 1:10 is
recommended. The rate may vary depending on the type of oil, degree of weathering,
temperature, and thickness of slick.

3.	Conditions for Use: As with any oil related spill, timely (preferably within 48 hours)
application of a dispersant will ensure the highest degree of success. Timely treatment with JD-
2000™, even at low application rates, can counter the "mousse" forming effect of the spilled oil.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (DDm)

JD-2000™

Menidia beryllina

407.00 96-hr



Mysidopsis bahia

90.50 48-hr

No. 2 Fuel Oil

Menidia beryllina

8.39 96-hr



Mysidopsis bahia

2.58 48-hr

JD-2000™ & No. 2 Fuel Oil

Menidia beryllina

3.59 96-hr

(1:10)

Mysidopsis bahia

2.19 48-hr

Reference Toxicant (SDS)

Menidia beryllina

2.22 96-hr



Mysidopsis bahia

10.50 48-hr

Dispersants

137

JD-2000™


-------
2. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH LOUISIANA
(S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%)

Prudhoe Bay Crude	60.4

South Louisiana Crude	77.8

Average of Prudhoe Bay and South Louisiana Crudes	69.1

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point (SW1010): 212°F

2.	Pour Point (ASTM D97): -36°F

3.	Viscosity (ASTM D445):65.2 cSt

4.	Specific Gravity 60/60 (ASTM D287): 0.99

5.	pH (EPA 150.1): 7.54

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: None

9.	Solubility in Water: Dispersible in fresh and salt water. Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.24

Cadmium	<0.10

Chromium	<0.10

Copper	<0.10

Lead	0.43

Mercury	<0.10

Nickel	<0.10

Zinc	0.11

Cyanide	<0.20

Chlorinated Hydrocarbons	<2.00

Dispersants

138

JD-2000™


-------
TECHNICAL PRODUCT BULLETIN #D-8

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 04, 2002

"NOKOMIS 3-F4"

I.	NAME, BRAND, OR TRADEMARK
NOKOMIS 3-F4

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax: (510) 782-2032

E-mail: marlensupply@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax: (510) 782-2032

E-mail: marlensupplv@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (water based)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of eye contact,
flush with water; in case of skin contact, wash with water; and if swallowed, drink water to dilute
and induce vomiting.

4.a.	Maximum storage temperature: 212°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 50°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

15 years or more if stored correctly in plastic drums.

Dispersants

139

NOKOMIS 3-F4


-------
VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Application of the product may be made directly from 33 and 35 gallon
drums (marketing sizes) by fitting the drum with a "T" connection and pumping fresh or salt
water across the junction, which will pull the dispersant from the drum into the water stream and
onto the oil spill.

2.	Concentration/Application Rate: For heavy concentrations of crude or Bunker C oil, apply the
product undiluted. Where lighter fractions of petroleum are involved, the product can be diluted
up to one part dispersant to 30 parts water.

3.	Conditions for Use: Effective in salt water, and can be used on water of any temperature.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

NOKOMIS 3-F4

Menidia beryllina

29.80 96-hr



Mysidopsis bahia

32.20 48-hr

No. 2 Fuel Oil

Menidia beryllina

100.00 96-hr



Mysidopsis bahia

72.70 48-hr

NOKOMIS 3-F4 &

Menidia beryllina

100.00 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

58.40 48-hr

Reference Toxicant (DSS)

Menidia beryllina

159.60 96-hr



Mysidopsis bahia

267.70 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH

LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness

Prudhoe Bay Crude	62.20

South Louisiana Crude	64.90

Average of Prudhoe Bay and South Louisiana Crudes	63.55

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: None

2.	Pour Point: 28°F

3.	Viscosity: 290 cps at 20°C (68°F)

4.	Specific Gravity: 1.0065g/cc at20°C (68°F)

5.	pH: 10.3 (at room temperature)

6.	Surface Active Agents: Confidential

7.	Solvents: None

8.	Additives: None

9.	Solubility: Completely water soluble

Dispersants

140

NOKOMIS 3-F4


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED

HYDROCARBONS

Compound

Concentration (ppm)
Arsenic	0.30

Cadmium	<5.00

Chromium	<10.00

Copper	<10.00

Lead	<10.00

Mercury	<0.05

Nickel	<10.00

Zinc	<10.00

Cyanide	<2.00

Chlorinated Hydrocarbons	<1.00

Dispersants

141

NOKOMIS 3-F4


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #D-9
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JUNE 28, 2002
"BIODISPERS"

I.	NAME, BRAND, OR TRADEMARK
BIODISPERS
Type of Product: Dispersant
(formerly PETROBIODISPERS)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Petrotech America Corporation

130 William Street, Suite 802

New York, NY 10038

Phone: (212)933-9071, ext. 7001

Fax:(877)226-4028

E-mail: Info@helpenvironmental.com

(Mr. Lawrence Gallo)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Petrotech America Corporation	Manufacturing Plant:

130 William Street, Suite 802	Clariant Corp.

New York, NY 1003 8	Charlotte, NC

Phone: (212)933-9071, ext. 7001

Fax: (877) 226-4028

E-mail: Info@helpenvironmental.com

(Mr. Lawrence Gallo)

H.E.L.P.	Environmental
926 3rd Avenue
Brooklyn, NY 11232

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

I.	Flammability: Non-flammable

2.	Ventilation: Use general ventilation to minimize exposure to vapor or mist.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Skin contact -
immediately flush with copious amounts of water. Remove and wash contaminated clothing and
shoes. If irritation persists, see a doctor. Eye contact - may cause eye irritation. In case of
contact, immediately flush eyes with plenty of water. If irritation persists, immediately see a
doctor. Hygienic practices - wear safety glasses. Wear gloves in accordance with routine
laboratory safety precautions.

7/19/2021
7/27/2022

Dispersants

142

BIODISPERS


-------
4.a. Maximum storage temperature: >70°C
4.b. Minimum storage temperature: -25°C
4.c. Optimum storage temperature range:

4.d. Temperatures of phase separations and chemical changes: No phase or chemical separation
observed.

V.	SHELF LIFE

The product has unlimited shelf life.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Recommended application is by aircraft, fireboat monitors or similar
apparatus.

2.	Concentration/Application Rate: Concentration varies with spilled material - Solvents at 5%,
light oils at 10%, medium oils at 10%, and heavy oils at 10%.

3.	Conditions for Use: Data is for water temperature of 40°F to 65°F. There are no known
application restrictions.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

BIODIPSERS

Menidia beryllina

13.46 96-hr



Mysidopsis bahia

78.90 48-hr

No. 2 Fuel Oil

Menidia beryllina

12.42 96-hr



Mysidopsis bahia

2.82 48-hr

BIODIPSERS &

Menidia beryllina

5.95 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.66 48-hr

Reference Toxicant (SDS)

Menidia beryllina

11.84 96-hr



Mysidopsis bahia

21.81 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH

LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%)

Prudhoe Bay Crude	51.0

South Louisiana Crude	63.0

Average of Prudhoe Bay and South Louisiana Crudes	57.0

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point, ASTM Method D56: 193°F

2.	Pour Point, ASTM Method D97: - 26°F

3.	Viscosity at 40°C, ASTM Method D445: Initial boil point 104.2°C, at 50 mL 109°C, at 70 mL
111°C, at 80 mL 113.7°C, final temperature 307.1°C)

4.	Specific Gravity: 0.965

Dispersants

143

BIODISPERS


-------
5.	pH: 7

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: Water

8.	Additives: None

9.	Solubility: Product is 100% soluble in water.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<2.50

Cadmium	<0.75

Chromium	<0.75

Copper	<0.50

Lead	<5.00

Nickel	<1.20

Zinc	<0.50

Cyanide	3.90*

Chlorinated Hydrocarbons	<5.00

*During the analysis of cyanide on sample #V202057-01 (Petrotech Dispersant) analyst

encountered interferences due to the matrix of sample. Soapy residue created a false positive for

cyanide. Sample showed no traces of cyanide. Value related to the soap film turbidity.

Dispersants

144

BIODISPERS


-------
TECHNICAL PRODUCT BULLETIN #D-10

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 26, 2002

"SEA BRAT #4"

I.	NAME, BRAND, OR TRADEMARK
SEA BRAT #4

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
B.R.A.T. Microbial Products Inc.

208 Cinnabar Bay Court
League City, TX 77573
Phone: (713) 724-9226
E-mail: alabastercorp@gmail.com
(Mr. John Sheffield)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
B.R.A.T. Microbial Products Inc.

208 Cinnabar Bay Court
League City, TX 77573
Phone: (713) 724-9226
E-mail: alabastercorp@gmail.com
(Mr. John Sheffield)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact:

Wear safety glasses or goggles, gloves, and rubber boots. Wash after each shift. Remove and
wash contaminated clothing before reuse. No respiratory protection is required. Local exhaust is
desirable. Mechanical exhaust is helpful in congested areas. Skin contact - flush with water.

Seek medical attention if irritation persists. Eye contact - flush with water using eye cup or
fountain for 15 minutes. Seek medical attention if irritation persists. Ingestion - seek medical
attention. Inhalation - no medical attention is required with inhalation.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 35°F
4.c. Optimum storage temperature range: NA

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

Indefinite when stored properly.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: Spray affected area with a high pressure pump. Always apply in

Dispersants

145

SEA BRAT #4


-------
compliance with federal, state, and local laws.

2.	Concentration/Application Rate: Dilution ratios of 1 part SEA BRAT #4 to 9 parts water for a
10 percent solution.

3.	Conditions for Use: May be applied to the coastal waters of the U.S. It is designed for
hydrocarbon spills on water temperatures between 50°F and 90°F. It is best applied with nozzle
pressure of between 80 psi and 100 psi, with a direct hard spray and continuously moving the
stream of water over the entire surface.

VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

SEA BRAT #4

Menidia beryllina

30.00 96-hr



Mysidopsis bahia

14.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

16.00 96-hr



Mysidopsis bahia

14.00 48-hr

SEA BRAT #4 &

Menidia beryllina

23.00 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

18.00 48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.14 96-hr



Mysidopsis bahia

0.98 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

VENDOR LAB REPORT:

Oil	Effectiveness (%)

Prudhoe Bay Crude	53.55

South Louisiana Crude	60.65

Average of Prudhoe Bay and South Louisiana Crudes	57.10

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point, ASTM Method D56: 200°F

2.	Pour Point, ASTM Method D97: 4°F

3.	Viscosity (furol seconds): 380 at 77°F

4.	Specific Gravity (g/cc): 0.994 at 70°F

5.	pH: 9.45

6.	Surface Active Agents: Surfactants

7.	Solvents: Propylene glycol

8.	Additives: None

9.	Solubility: Soluble in all ratios.

Dispersants

146

SEA BRAT #4


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)
<0.05
<0.05
<0.05
<0.05
<0.05
<0.0002
<0.05
0.215
<0.05
<0.05

Dispersants

147

SEA BRAT #4


-------
TECHNICAL PRODUCT BULLETIN #D-11

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JANUARY 30, 2003

"FINASOL® OSR 52"

(aka, SEACARE ECOSPERSE 52)

I.	NAME, BRAND, OR TRADEMARK
FINASOL® OSR 52

(aka, SEACARE ECOSPERSE 52)

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
TotalEnergies Fluids

24 cours Michelet La Defense 10
92069 Paris La Defense Cedex
France

Phone: 011-33-1-41-35-30-48
United States: (713) 297-4651
24-hour Emergency Number: (713) 297-1996
E-mail: beniamin.swoboda@totalenergi es.com
Website: www.specialfluids.totalenergies.com
(Mr. Benjamin Swoboda)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Importer/U.S. Distributor

TOTAL SPECIALTIES USA, INC.

1201 Louisiana Street, Suite 1800
Houston, TX 77002
Phone: (713)297-4651
Fax: (713)297-4689
E-mail: peter.egan@totalenergies.com
Website: www.specialfluids.totalenergies.com
(Mr. Peter Egan)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Keep well away from sources of ignition and heat. Avoid the accumulation of
static electricity. Provide grounding.

2.	Ventilation: Keep containers closed when not in use. Do not inhale vapors, fumes, or mists.
In case of inhalation, take the person into fresh air. Ensure adequate ventilation is provided if
there is any risk of vapors, mists, or aerosols forming. In the event of serious problems, call a
doctor or summon medical assistance urgently.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wear appropriate long
sleeve shirts, chemical resistant gloves and goggles. Avoid contact with skin and eyes. In case
of contact, wash immediately with plenty of water. Avoid contact with clothing. In case of

Dispersants

148

FINASOL® OSR 52


-------
contact, wash immediately and remove contaminated clothing. Prolonged and repeated contact

with the skin may cause skin disorders. In case of ingestion, do not induce vomiting to prevent

aspiration into the respiratory tract.

4.a. Maximum storage temperature: 65°C

4.b. Minimum storage temperature: -20°C

4.c. Optimum storage temperature range: 5 - 35°C

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

The shelf life of unopened drums of FINASOL® OSR 52 is potentially unlimited when the
containers remain capped and sealed to prevent contamination and evaporation of solvents, and
are stored in a place with stable temperatures and are unexposed to direct sunlight. After storage,
stir the product and assure uniformity before use. Testing of FINASOL® OSR 52 is
recommended every three years and then on a yearly basis to ensure it remains fit for its intended
usage.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: FINASOL® OSR 52 is applied effectively by aircraft or from boats. It
can also be applied by hand held sprayers as well as with backpack spray units. Spraying must
not give too fine or atomized droplets as in fog. It must be done as moderately coarse droplets,
with diameters in the range of 500 - 1000 m, whether application is by surface vessel, aircraft, or
land-based equipment.

2.	Concentration/Application Rate: Use FINASOL® OSR 52 from 1:5 to 1:50, according to the
nature of the oil, its state of weathering, temperature, thickness of the slick, and other
circumstances of the spill. A 1:10 ratio would correspond appreciatively to 26 gallons per ton of
oil.

Aerial spraying - FINASOL® OSR 52 is sprayed undiluted when applied from aircrafts, usually
between 30 and 50 feet altitude, or at higher altitude in poor weather conditions.

Boat spraying - FINASOL® OSR 52 is sprayed undiluted using a low-pressure system. Spraying
equipment providing 5 to 10% dilution of FINASOL® OSR 52 can also be used.

3.	Conditions for Use: Diluted application in low salinity water is not recommended. Use only
receptacles, joints, pipes, etc. which are resistant to hydrocarbons. Do not spray at high pressure
(> 3 bar). FINASOL® OSR 52 is designed to treat spills in salt water.

Dispersants

149

FINASOL® OSR 52


-------
VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species	LC50 (ppm)

Menidia beryllina	11.66 96-hr

Mysidopsis bahia	9.37 48-hr

Menidia beryllina	5.95 96-hr

Mysidopsis bahia	2.37 48-hr

Menidia beryllina	5.40 96-hr

Mysidopsis bahia	2.37 48-hr

Menidia beryllina	8.54 96-hr

Mysidopsis bahia	21.81 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL
VENDOR LAB REPORT:

FINASOL® OSR 52

No. 2 Fuel Oil

FINASOL® OSR 52 &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

on

Prudhoe Bay Crude
South Louisiana Crude

Average of Prudhoe Bay and South Louisiana Crudes

Effectiveness
32.50
71.60
52.10

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM Method D-3278-89: 110°C

2.	Pour Point, ASTM Method D-97-87: -27°C

3.	Viscosity, ASTM Method D-445-88: 58.5 cSt

4.	Specific Gravity, ASTM Method D-1298-85 (90): 1.01

5.	pH, ASTM Method D-1293-84 (90): 8.57

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Dispersible in water.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Antimony	<10.0

Arsenic	<10.0

Barium	<10.0

Cadmium	<10.0

Chromium	<10.0

Copper	<10.0

Lead	<10.0

Mercury	<1.0

Dispersants

150

FINASOL® OSR 52


-------
Nickel

Selenium

Silver

Zinc

Cyanide

Chlorinated Hydrocarbons

<10.0

<10.0

<10.0

<10.0

<0.4

<4.4

Dispersants

151

FINASOL® OSR 52


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #D-12
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JANUARY 03, 2005
"SAF-RON GOLD"

(aka, SF-GOLD DISPERSANT)

I.	NAME, BRAND, OR TRADEMARK
SAF-RON GOLD
(aka, SF-GOLD DISPERSANT)

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Sustainable Environmental Technologies Inc.

55 Ivan Allen Jr. Boulevard, Suite 850
Atlanta, GA 30308
Customer Service:

Phone: (404) 946-3585
24-hour Emergency Number:

Phone: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Bruce Richards)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Sustainable Environmental Technologies Inc.

55 Ivan Allen Jr. Boulevard, Suite 850
Atlanta, GA 30308
Customer Service:

Phone: (404) 946-3585
24-hour Emergency Number:

Phone: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Bruce Richards)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Special ventilation is not required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
required; however, goggles are recommended. Skin contact - if irritation occurs flush with
water; seek medical attention if irritation persists. Eye contact - flush with plenty of water; seek
medical attention if irritation persists.

3/18/2016
7/27/2022

Dispersants

152

SAF-RON GOLD


-------
4.a. Maximum storage temperature: 120°F

4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 40 - 120°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

The shelf life is unlimited in unopened containers.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Sprayer, Boat, Aircraft.

2.	Concentration/Application Rate: A dispersant to oil ratio ranging from 1:50 to 1:10 is
recommended. For heavy high-viscosity oils - 8 gallons of SAF-RON GOLD will disperse
approximately 70 gallons of crude oil or bunker C. Also for use with heavy high viscosity oils,
SAF-RON GOLD can be used as a concentrate or diluted at a dispersant to water ratio of 1:10.
For lighter oils, SAF-RON GOLD can be diluted at mixtures of 1:20 to 1:100. A recommended
dispersant to water ratio of 1:40 can be used for most spills. Ratios are dependent upon type of
oil and weather conditions.

3.	Conditions for Use: Any applicable condition determined by authorities for dispersant use.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

SAF-RON GOLD

Menidia beryllina

29.43 96-hr



Mysidopsis bahia

63.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

16.76 96-hr



Mysidopsis bahia

5.93 48-hr

SAF-RON GOLD

Menidia beryllina

9.25 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

3.04 48-hr

Reference Toxicant (SLS)

Menidia beryllina

15.94 96-hr



Mysidopsis bahia

9.83 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

VENDOR LAB REPORT:

Oil	Effectiveness (%)

Prudhoe Bay Crude	84.80

South Louisiana Crude	53.80

Average of Prudhoe Bay and South Louisiana Crudes	69.30

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point, ASTMD-56: >100°C

2.	Pour Point, ASTMD-97: -2.5°C

3.	Viscosity @40°C, ASTM Method D-445: 1.42 cSt

Dispersants

153

SAF-RON GOLD


-------
4.	Specific Gravity @60°F/60°F, ASTM Method D-287: 1.014

5.	pH: 8.8

6.	Surface Active Agents: Proprietary blend of surface-active agents.

7.	Solvents: None.

8.	Additives: None.

9.	Solubility: Fully water soluble.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.01

Cadmium	<0.005

Chromium	0.140

Copper	0.324

Lead	<0.005

Mercury	<0.020

Nickel	<0.005

Zinc	0.0671

Cyanide	<0.20

Chlorinated Hydrocarbons	<0.80

Dispersants

154

SAF-RON GOLD


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #D-13
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JUNE 16, 2005
"ZI-400"

(aka, ZI-400 OIL SPILL DISPERSANT)

I.	NAME, BRAND, OR TRADEMARK
ZI-400

(aka, ZI-400 OIL SPILL DISPERSANT)

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Z.I. Chemicals

340 S Lemon Avenue #5358
Walnut, CA 91789
Phone: updated information required
E-mail: updated information required
Website: www.zichemicals.com
(Ms. Annie Mack)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Z.I. Chemicals

340 S Lemon Avenue #5358
Walnut, CA 91789
Phone: updated information required
E-mail: updated information required
Website: www.zichemicals.com
(Ms. Annie Mack)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-Hazardous).

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however, goggles are recommended. If eye or skin irritation occurs, flush
with plenty of water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40 - 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Unlimited in sealed polydrums of totes (as delivered).

3/18/2019
7/27/2022

Dispersants

155

ZI-400


-------
VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: ZI-400 may be applied by the usual method of aerial or boat spraying.
For smaller spills a drum pump with sprayer may be used, mixing with water as required
depending on the type and viscosity of oil being treated.

2.	Concentration/Application Rate: On heavy oils use ZI-400 directly on the spill, or up to
approximately a 1:10 dilution ratio (product:water). Lighter oils will require a 1:10 to 1:30
product to water dilution ratio. Warmer waters (greater than 78°F) and/or good agitation during
application will require less product.

3.	Conditions for Use: No limitations as to usage within optimum temperature parameters
(application may be made at or above 35°F, with optimum above 48°F).

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

ZI-400

Menidia beryllina

31.76 96-hr



Mysidopsis bahia

20.96 48-hr

No. 2 Fuel Oil

Menidia beryllina

18.05 96-hr



Mysidopsis bahia

2.66 48-hr

ZI-400

Menidia beryllina

8.35 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.77 48-hr

Reference Toxicant (SLS)

Menidia beryllina

16.13 96-hr



Mysidopsis bahia

27.80 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

VENDOR LAB REPORT:

Oil	Effectiveness (%)

Prudhoe Bay Crude	50.10

South Louisiana Crude	89.80

Average of Prudhoe Bay and South Louisiana Crudes	69.90

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point, ASTM D-56: >93°C

2.	Pour Point, ASTMD-97: 12.6°F

3.	Viscosity, ASTM D-445: 18.80 cSt @ 40°C

4.	Specific Gravity, ASTM D-1298: 1.026 @ 60°F

5.	pH, ASTM D-1293: 10.9

6.	Surface Active Agents: Proprietary

7.	Solvents: Proprietary

8.	Additives: None.

9.	Solubility: Miscible in oil, water, and solvents.

Dispersants

156

ZI-400


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<10

<10

<10

<10

<10

<1

<10

<10

<0.5

<1.0

Dispersants

157

ZI-400


-------
TECHNICAL PRODUCT BULLETIN #D-14

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 31, 2008

"NOKOMIS 3-AA"

I.	NAME, BRAND, OR TRADEMARK
NOKOMIS 3-AA

Type of Product: Water-Based Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax:(510)782-2032

E-mail: marlensupply@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax:(510)782-2032

E-mail: marlensupplv@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (water based)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of eye contact,
flush with water; in case of skin contact, wash with water; and if swallowed, drink water to dilute
and induce vomiting.

4.a.	Maximum storage temperature: 160°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 32 - 140°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

In excess of 24 months or more if stored correctly in plastic drums.

Dispersants

158

NOKOMIS 3-AA


-------
VI. RECOMMENDED APPLICATION PROCEDURES

1.	Application Method:

Aerial applied dispersant - spray from an aircraft flying with a controllable speed at altitudes of
30 to 50 feet. Spray nozzles should be sized to cover an area using 5 gallons per surface acre.

Spray from boat: NOKOMIS 3-AA can be applied by ships of workboat with spray booms
mounted as far forward as possible. NOKOMIS 3-AA will generally be marketed in 55 gallon
plastic drums. Application of the products may be made directly from the drum. By using a
direct connection from pump to drum NOKOMIS 3-AA can be applied at full strength to the oil
spill. The determination of whether to use NOKOMIS 3-AA at full strength or diluted with
water must be determined by observations and evaluations made on-site at the oil spill.

Portable engine powered centrifugal water pumps are a satisfactory means of moving the
dispersant from the container to the spill's surface. Diesel-powered larger capacity pump may
also be used. If the spill is confined to a small area, a hand-pump connected directly to the 55
gallon drum can be used. Hose diameters and lengths will relate to capacities required for the
specific situation and distances from the pump to container and the spill. Fire hose has been
successfully used, and with hand pumps small diameter hose is adequate. Fog nozzles on the
dispersing end of the hose provide a fine spray of NOKOMIS 3-AA full strength or diluted as
appropriate. Any type of hose nozzle can be used, but preferable one with the ability to produce
a spray rather than a coarse stream.

2.	Concentration/Application Rate: NOKOMIS 3-AA may be applied to oil spills at full strength,
or diluted with sea water. Where large areas of water may be covered with heavy concentrations
of crude or Bunker C oil, it may be advantageous to apply NOKOMIS 3-AA at full strength.
Where lighter fractions of petroleum are involved it is possible that dilutions of up to one part
NOKOMIS 3-AA to 30 parts water may be applicable. Approximately 5 gallons of NOKOMIS
3-AA can be used for one surface acre of oil spill.

3.	Conditions for Use: Once NOKOMIS 3-AA is applied to the water's surface, to obtain the
most efficient emulsification of the oil it is necessary to agitate and mix dispersant, oil, and water
thoroughly. In open unconfined areas, the use of ship propellers has been determined a practical
way of accomplishing this purpose. By passing over the spill area on a grid system, the vessel's
propellers will churn the water, causing the needed mixing. For a large spill, two or more vessels
may be needed to apply the product and agitate the water. In and around piers and similar
confined areas it is necessary to apply the product from small boats, the shore, or pier itself.
Where it is impossible or impractical to supply agitation with propellers of a vessel it is
necessary to use pumps and a hose, applying salt water in the coarse stream and under sufficient
pressure to cause surface turbulences and subsequent mixing.

Dispersants

159

NOKOMIS 3-AA


-------
VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

NOKOMIS 3-AA

Menidia beryllina

34.22 96-hr



Mysidopsis bahia

20.16 48-hr

No. 2 Fuel Oil

Menidia beryllina

22.50 96-hr



Mysidopsis bahia

11.07 48-hr

NOKOMIS 3-AA &

Menidia beryllina

7.03 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

5.56 48-hr

Reference Toxicant (CUSO4)

Menidia beryllina

5.36 96-hr



Mysidopsis bahia

7.83 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH

LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%

Prudhoe Bay Crude	63.20

South Louisiana Crude	65.70

Average of Prudhoe Bay and South Louisiana Crudes	64.50

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: None

2.	Pour Point: 25 °F

3.	Viscosity: 72.3 sus at 100°F

4.	Specific Gravity: 1.031 at 60°F

5.	pH: 9.0

6.	Surface Active Agents: Confidential

7.	Solvents: Propylene glycol and Water

8.	Additives: None

9.	Solubility: Completely water soluble

Dispersants

160

NOKOMIS 3-AA


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<0.12

<0.25

<0.25

<0.25

<0.12

<0.0016

<0.25

<1.0

0.034
<0.10

Dispersants

161

NOKOMIS 3-AA


-------
TECHNICAL PRODUCT BULLETIN #D-16

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 18, 2011

"ACCELL CLEAN® DWD"

I.	NAME, BRAND, OR TRADEMARK
ACCELL CLEAN® DWD

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Advanced BioCatalytics Corporation

18010 Skypark Circle, #130
Irvine, California 92614-6456
Office Phone: (949) 771-0209
General E-mail: info@abiocat.com
Website: www.abiocat.com
Product Management:

Mobile: (949) 981-6510
E-mail: cpodella@abiocat.com
(Mr. Carl Podella)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Advanced BioCatalytics Corporation

18010 Skypark Circle, #130
Irvine, California 92614-6456
Office Phone: (949) 771-0209
General E-mail: info@abiocat.com
Website: www.abiocat.com
Product Management:

Mobile: (949) 981-6510
E-mail: cpodella@abiocat.com
(Mr. Carl Podella)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Combustible as defined by DOT and USCG.

2.	Ventilation: Use in well ventilated areas.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Protective clothing is
recommended. Avoid eye contact. In case of eye contact, immediately flush with large amounts
of water for at least 15 minutes. Get prompt medical attention. Avoid direct contact with skin and
clothing. In case of skin contact, immediately flush with large amounts of water. Remove
contaminated clothing, including shoes, after flushing has begun. If irritation persists, seek
medical attention. For open systems were contact is likely, wear long sleeve shirt, chemical
resistant gloves, and protective chemical goggles.

4.a.	Maximum storage temperature: 130°F/55°C

Dispersants

162

ACCELL CLEAN® DWD


-------
4.b. Minimum storage temperature: 30°F/-1°C

4.c. Optimum storage temperature range: 40°F to 100°F/4°C to 38°C

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

The shelf life of unopened drums of ACCELL CLEAN® DWD is unlimited. Containers should
always remain capped when not in use to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Aircrafts provide the most rapid method of applying dispersants to an oil
spill and a variety of aircraft can be used for spraying. For aerial spraying, ACCELL CLEAN®
DWD is applied undiluted. Typically application altitudes of 30 to 50 feet are recommended,
although higher altitudes may be effective under certain conditions. Actual effective altitudes
will depend on the application equipment, weather and aircraft. Careful selection of spray
nozzles is critical to achieve desired dose levels, since droplet size must be controlled. A quarter-
inch open pipe may be all that is necessary if the aircraft travels at 120 mph (104 knots) or more,
since the air shear at these speeds will be sufficient to break the dispersant into the proper sized
droplets. Agricultural spray delivery systems may not be suitable because of too fine of spray
and too little delivery of ACCELL CLEAN® DWD to the affected area.

Boat Spraying: ACCELL CLEAN® DWD may also be applied from boats equipped with spray
booms mounted ahead of the bow wake or as far forward as possible. The most effective method
of application from a boat is to apply ACCELL CLEAN® DWD using a low-volume, low-
pressure pump so the ACCELL CLEAN® DWD can be applied undiluted. ACCELL CLEAN®
DWD should not be fogged or atomized. Natural wave or boat wake action usually provides
adequate mixing energy to disperse the oil. Application at sub-freezing temperatures may require
larger nozzle, supply lines and orifices due to higher product viscosity.

2.	Concentration/Application Rate: A treatment rate of about 10 gallons per acre, or a dispersant
to oil ratio of 1:10 is optimal. The rate varies depending on the type of oil, degree of weathering,
temperatures, and thickness of the slick.

3.	Conditions for Use: For optimal results, ACCELL CLEAN® DWD early treatment of oil-
contaminated waters is beneficial. ACCELL CLEAN® DWD can be used on weathered oils.

Dispersants

163

ACCELL CLEAN® DWD


-------
VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:

Materials Tested
ACCELL CLEAN® DWD

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)

5.66	96-hr

2.07	48-hr

11.10	96-hr

1.68	48-hr

8.05	96-hr

1.32	48-hr

6.60	96-hr

30.80	48-hr

No. 2 Fuel Oil

ACCELL CLEAN® DWD
& No. 2 Fuel Oil (1:10)
Reference Toxicant (DDS)

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil

Effectiveness (%)

Prudhoe Bay Crude
South Louisiana Crude

Average of Prudhoe Bay and South Louisiana Crudes

58.70
96.03
77.37

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	FlashPoint: 130°F/55°C

2.	Pour Point: -20.2°F/-29°C

3.	Viscosity: 130 SUS @100°F

4.	Specific Gravity: 1.0329 @60°F

5.	pH: 5.8

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Miscible

Dispersants	164	ACCELL CLEAN® DWD


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	ND

Copper	ND

Lead	ND

Mercury	ND

Nickel	ND

Zinc	ND

Cyanide	ND

Chlorinated Hydrocarbons	ND

Dispersants

165

ACCELL CLEAN® DWD


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

7/23/2021
7/27/2022

TECHNICAL PRODUCT BULLETIN #D-17

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 01, 2011

"FFT-SOLUTION®"

I.	NAME, BRAND, OR TRADEMARK
FFT-SOLUTION®

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Fog Free Technologies, LLC

4365 Dorchester Road
Building 300, Suite 301
North Charleston, SC 29405
Product Management:

Office Phone: (843) 735-6626
Mobile: (478) 697-2588
E-mail: updated information required
Website: www.fogfreetechnologies.com
(Mr. William Knight)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Fog Free Technologies, LLC

4365 Dorchester Road
Building 300, Suite 301
North Charleston, SC 29405
Product Management:

Office Phone: (843) 735-6626
Mobile: (478) 697-2588
E-mail: updated information required
Website: www.fogfreetechnologies.com
(Mr. William Knight)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO: Non-Flammable, DOT: Non-Hazardous

2.	Ventilation: Lowest level of skin protection is acceptable, but no special ventilation is
required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Lowest level of skin
protection is acceptable. Avoid eye contact. In case of eye contact, immediately flush eyes with
large amounts of water for at least 15 minutes. Avoid contact with skin. In case of skin contact,
immediately flush with water and soap if available. For open systems where contact is likely,
wear long sleeve shirt, chemical resistant gloves and chemical goggles.

Dispersants	166	FFT-SOLUTION®


-------
4.a. Maximum storage temperature: 170°F

4.b. Minimum storage temperature: 30°F

4.c. Optimum storage temperature range: 40°F to 105°F

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

The shelf life of unopened drums of FFT-Solution® is limited to 60 months. Storage should be in
a semi-controlled warehouse, out of direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Aerial Spraying - Aircraft provide the most rapid method of applying
dispersants to an oil spill and a variety of aircraft can be used for spraying. For aerial spraying,
FFT-Solution® is applied undiluted. Typical application altitudes of 30 to 50 feet have been used,
although higher altitudes may be effective under certain conditions. Actual effective altitudes
will depend upon application equipment, weather, and aircraft. Careful selection of spray nozzles
is critical to achieve desired dose levels, since droplet size must be controlled. Many nozzles
used for agricultural spraying are of low capacity and product fine a spray. A quarter-inch open
pipe may be all that is necessary if the aircraft travels at 120 mph (104 knots) or more, since the
air shear at these speeds will be sufficient to break the dispersant into the proper sized droplets.
Optimal temperatures for application are between 33°F and 105°F.

Boat Spraying - FFT-Solution® may also be applied by workboats equipped with spray booms
mounted on the stern of the vessel. (Mounting boom on the stern prevents any over spray from
making contact with boat operators.) The preferred and most effective method of application
from a workboat is to use a low-volume, low-pressure pump so the chemical can be applied
undiluted. Standard agriculture spray equipment is designed to make dosage adjustments or
provide different spray tips that effect dosage rates. Natural wave or boat wake action usually
provides adequate mixing energy to disperse the oil. A typical agriculture spray boom can be
mounted to the stern to get wide coverage. The booms on shrimp boats also can be retrofitted to
cover a much wider path during applications. The manufacturer also recommends that in lieu of
spray tips on the booms, spray tips be changed into solid tubing for injection of FFT-Solution® 3
to 5 feet below the water surface. This will get the thicker crude slicks injected faster and with
better results. FFT-Solution® should be applied as droplets, not fogged or atomized.

2.	Concentration/Application Rate: A treatment rate of about 2 to 10 U.S. gallons per acre, or
dispersant to oil ratio of 1:50 to 1:10 is recommended. This rate varies depending on the type of
oil, degree of weathering, temperature, and thickness of the slick.

3.	Conditions for Use: FFT-Solution® can be applied to weathered oil as well as light, medium,
or heavy oils. Early treatment even at reduced treatment rates, can also counter the foaming
tendencies of the spilled oil in turbulent waters. FFT-Solution® can be used on any type oil spills
in salt water.

Dispersants

167

FFT-SOLUTION®


-------
VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:
Materials Tested
FF T - S OLUTION®

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)

5.34	96-hr

2.72	48-hr

40.80	96-hr

5.19	48-hr

5.14	96-hr

2.75	48-hr

2.42	96-hr

6.97	48-hr

No. 2 Fuel Oil

FF T - S OLUTION®
& No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil

Effectiveness (%)

Prudhoe Bay Crude
South Louisiana Crude

Average of Prudhoe Bay and South Louisiana Crudes

49.97
48.87
49.42

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 170°F

2.	Pour Point: 23°F

3.	Viscosity: 450 SUS @100°F

4.	Specific Gravity: 1.0302 @60°F

5.	pH: 9.96

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: None

9.	Solubility: Product is 100% soluble in water

Dispersants	168	FFT-SOLUTION®


-------
X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	ND

Copper	ND

Lead	ND

Mercury	ND

Nickel	ND

Zinc	ND

Cyanide	ND

Chlorinated Hydrocarbons	ND

Dispersants

169

FFT-SOLUTION®


-------
TECHNICAL PRODUCT BULLETIN #D-18

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: APRIL 23, 2012

"MARINE D-BLUE CLEAN™"

I.	NAME, BRAND, OR TRADEMARK
MARINE D-BLUE CLEAN™

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail.com

Website: www.agstx.com

(Mrs. Linda Whiteley)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail.com

Website: www.agstx.com

(Mrs. Linda Whiteley)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: No special requirements. Drums and similar containers should be kept closed.
Store in steel or plastic containers.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of contact with
eyes, wash thoroughly with plenty of clean water. Seek medical attention if irritation develops.
Rubber protective gloves should be used if prolonged use of product is anticipated. Goggles,
long sleeve shirt, and rubber gloves are recommended during application.

4.a.	Maximum storage temperature: 170°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 40°F to 110°F

4.d. Temperatures of phase separations and chemical changes: Marine D-Blue Clean™ has a
pour point of 30°F and may cause chemical changes at temperatures >110°F.

Dispersants

170

MARINE D-BLUE CLEAN™


-------
V. SHELF LIFE

Marine D-Blue Clean™ has a shelf life of >2 years, if unopened. Cleaner older than 24 months
may still be viable. Ensure product is mixed well and then inspect to confirm the product is
suitable for application. The product will not lose effectiveness unless the temperatures in
>140°F.

VI. RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Sprayer, boat, aircraft. Marine D-Blue Clean™ is to be used to disperse
petroleum-based products in salt water. It may be applied by any conventional methods such as
aerial spraying or surface vessel spraying, to accommodate weather conditions. Marine D-Blue
Clean™ is to be applied undiluted, for aerial spraying. Timely application provides optimal
results. Spray concentrated on the oil slick in atomized form such as with a manual pump or a
pump system using moderately coarse droplets rather than a fine mist.

2.	Concentration/Application Rate: Marine D-Blue Clean™ can be applied with a variety of
spraying equipment, depending upon the type and scale of the water to be cleaned. For heavy
concentrations of crude oil spill or temperatures below 40°F, Marine D-Blue Clean™ should be
used without dilution in neat form. A dispersant to oil ratio up to 1 part dispersant to 20 parts of
oil is suggested. Dose rates may vary depending on type and amount of petroleum spilled, and
other site specific conditions such as weather, temperatures and extent of oil slick.

3.	Conditions for Use: The performance of Marine D-Blue Clean™ is not affected by water
salinity. Marine D-Blue Clean™ is useful on oil spills in salt water. It is effective with crude and
residual heavy oil spills.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50

(DDm)

MARINE D-BLUE CLEAN™

Menidia beryllina

18.00

96-hr



Mysidopsis bahia

56.00

48-hr

No. 2 Fuel Oil

Menidia beryllina

18.00

96-hr



Mysidopsis bahia

18.00

48-hr

MARINE D-BLUE CLEAN™ &

Menidia beryllina

32.00

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

18.00

48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.06

96-hr



Mysidopsis bahia

0.97

48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH

LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OIL

Oil	Effectiveness (%

Prudhoe Bay Crude	45.00

South Louisiana Crude	55.59

Average of Prudhoe Bay and South Louisiana Crudes	50.30

Dispersants

171

MARINE D-BLUE CLEAN™


-------
VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: 30°F

3.	Viscosity: 17.29 cSt @ 100°C

4.	Specific Gravity: 1.035 @70°F

5.	pH: 11.89

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: None

9.	Solubility: Completely soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.25

Cadmium	<0.005

Chromium	<0.08

Copper	<0.30

Lead	<0.015

Mercury	<0.0025

Nickel	<0.350

Zinc	<2.015

Cyanide	<0.050

Chlorinated Hydrocarbons	ND

Dispersants

172

MARINE D-BLUE CLEAN™


-------
TECHNICAL PRODUCT BULLETIN #D-19
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: AUGUST 1, 2013
"COREXIT™ EC9500B"

I.	NAME, BRAND, OR TRADEMARK
COREXIT™ EC9500B

Type of Product: Dispersant

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: DOT HazMat Classification - This product meets the criteria for classification
as a Class 3 combustible liquid (49 CFR §173.120(b)(1)). However, it does not contain
combustion, and, therefore, is not subject to the requirements for the Hazardous Materials
Regulations (49 CFR §173.120(b)(3)).

2.	Ventilation: Use with adequate ventilation equal to unobstructed outdoors in moderate breeze.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Do not get in eyes, on
skin, or on clothing. In case of eye contact, rinse immediately with plenty of water and seek
medical advice promptly. In case of skin contact, wash immediately with plenty of soap and
water. If irritation persists or symptoms develop, seek medical attention. If clothing is
contaminated, remove clothing and thoroughly wash the affected area. Do not take internally. In
the event of oral ingestion, do not induce vomiting (can cause chemical pneumonia if aspirated
into lungs). If conscious, wash out mouth and give water to drink. Get medical attention. If
inhaled, remove to fresh air, treat symptomatically. Get medical attention.

Dispersants

173

COREXIT™ EC9500B


-------
For open systems where contact is likely, wear Tyvek, chemical resistant gloves (e.g., nitrile),

and chemical splash goggles. Where concentrations in air may be high (e.g., confined area), the

use of a half face filter mask or air supplied breathing apparatus is recommended.

4.a. Maximum storage temperature: 170°F

4.b. Minimum storage temperature: 40°F

4.c. Optimum storage temperature range: 40°F to 100°F

4.d. Temperatures of phase separations and chemical changes: No phase changes or chemical
reactions are anticipated in the minimum to maximum storage range. Below 40°F, surfactant may
slowly precipitate out of the solution, but it will return back into solution when warmed.

V.	SHELF LIFE

The shelf life of unopened drums of COREXIT™ EC9500B is potentially unlimited when
containers remain capped and sealed to prevent contamination and evaporation of solvents.
Testing of COREXIT™ EC9500B is recommended every five years to ensure it remains fit for
its intended purpose.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: For aerial spraying, apply COREXIT™ EC9500B undiluted. Various
fixed-wing aircraft or helicopters can be used for spraying over a large area, from an altitude of
30 to 50 feet or even higher, depending on the application equipment and aircraft. Typical
application altitudes of 30 to 50 feet have been used, although higher altitudes may be effective
under certain conditions. Actual altitudes will depend on the application equipment, weather and
aircraft. Careful selection of spray nozzles is critical to achieve desired dose levels, since droplet
size must be controlled. Many nozzles used for agricultural spraying are of low capacity and
produce too fine a spray. Avoid nozzles that produce a mist or fog. No nozzle may be necessary
if the aircraft travels at 120 mph (104 knots) or more, since the air shear at these speeds will be
sufficient to break the chemical stream into appropriately-sized droplets.

For boat spraying (spray boom), COREXIT™ EC9500B may also be applied by workboats
equipped with spray booms mounted ahead of the bow wake or as far forward as possible. The
most effective method of application from a workboat could be the use of a low-volume, low-
pressure pump. Spray equipment designed to provide a diluted dispersant solution to the spray
booms can also be used. Dispersant concentrations in the 5 to 10 percent range are
recommended; lower concentrations may result in significant fall-off in effectiveness.
COREXIT™ EC9500B should be applied as droplets, not fogged or atomized. Natural wave or
boat wake action usually provides adequate mixing energy to disperse the oil. Water from a fire
hose can also be used for agitation of the treated slick.

For boat spraying (fire monitor), a slightly modified fire monitor may be useful for applying
dispersant concentrates such as COREXIT™ EC9500B from a boat. A screen cap is used on the
nozzle of the monitor to obtain a uniform spray pattern with the proper sized droplet. Due to the
volume output and the greater reach of the fire monitor, significantly more area can be covered
in a shorter period of time than using conventional spray booms.

Dispersants

174

COREXIT™ EC9500B


-------
System Calibration - To facilitate successful application and dosage control, calibrate spray
systems at the temperatures anticipated. Application at sub-freezing temperatures may require
larger nozzle, supply lines and orifices due to higher product viscosity.

2.	Concentration/Application Rate: A treatment rate of about 2 to 10 U.S. gallons per acre, or a
dispersant to oil ratio of 1:50 to 1:10 is recommended; lower concentrations may also be used.
This rate varies depending on the type of oil, degree of weathering, temperature, and thickness of
the slick.

3.	Conditions for Use: COREXIT™ EC9500B can be used on oil spills in salt waters and at any
water temperature. The product can be used on most oils, weathered spills, and "chocolate
mousse" (water-oil emulsions). Viscous oil may require higher dosage rates.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (ppm)

COREXIT™ EC9500B

Menidia beryllina

29.13 96-hr



Mysidopsis bahia

10.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

7.54 96-hr



Mysidopsis bahia

2.51 48-hr

COREXIT™ EC9500B & No. 2 Fuel Oil (1:10)

Menidia beryllina

4.46 96-hr



Mysidopsis bahia

2.13 48-hr

Reference Toxicant (SLS)

Menidia beryllina

12.19 96-hr



Mysidopsis bahia

10.53 48-hr

b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH
LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OILS

Oil	Effectiveness (%)

Prudhoe Bay Crude	57.0

South Louisiana Crude	50.9

Average of Prudhoe Bay and South Louisiana Crudes	53.9

VIII.	MICROBIOLOGICAL PROPERTIES

NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 164°F

2.	Pour Point: -44.0°F

3.	Viscosity: 21.78 cSt at 40°C

4.	Specific Gravity: 0.9626 at 15°C

5.	pH: 6.29

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

Dispersants

175

COREXIT™ EC9500B


-------
9.	Additives: None

10.	Solubility: Miscible

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0108

Cadmium	<0.0020

Chromium	<0.0060

Copper	<0.0060

Lead	<0.0040

Mercury	<1.0000 (ug/L)

Nickel	<0.0100

Zinc	<0.0060

Cyanide	<0.0100
Chlorinated hydrocarbons 1.7600

Dispersants

176

COREXIT™ EC9500B


-------
TECHNICAL PRODUCT BULLETIN #D-20
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: NOVEMBER 06, 2019
"CHIMEC CHIMSPERSE 6000"

I. NAME, BRAND, OR TRADEMARK
CHIMEC CHIMSPERSE 6000
Type of Product: Dispersant

II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

CHIMEC S.p.A.

Via deH'informatica 5

00071 Pomezia (RM), Italy

Phone: +39-06-91825291

Fax: +39-06-91825225

E-mail: fnanchi@chimec.it

(Mr. Francesco Nanchi, Deputy and

Special Prosecutor for Manufacturing,

Shipping, Safety, and Environment)

CHIMEC Technical Manager and Primary Contact:
Phone: +39-06-91825258
Fax: +39-06-91825262
E-mail: mmantarro@chimec.it
(Mrs. Milena Mantarro)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

CHIMEC Technical Manager and Primary Contact:
Phone: +39-06-91825258
Fax: +39-06-91825262
E-mail: mmantarro@chimec.it
(Mrs. Milena Mantarro)

CHIMEC S.p.A.

Via deirinformatica 5
00071 Pomezia (RM), Italy
Phone: +39-06-918251
Fax: +39-06-9194170
E-mail: mortolani@chimec.it
(Mrs. Maria Angela Ortolani,
Chairperson and Legal Representative)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable.

2.	Ventilation: None under normal conditions. If exposure levels are exceeded or irritation is
experienced, wear approved respiratory protection. In case of inadequate ventilation, oxygen
deficient atmosphere, or where exposure levels are not known, wear approved respiratory
protection (e.g., a mask fit for organic vapors (Al)). If inhaled, go into open air and ventilate
suspected area. Obtain medical attention if breathing difficulty persists.

3.	Skin and eye contact; protective clothing; treatment in case of contact: For skin protection,
wear latex or neoprene gloves, and clothing with chemically resistant materials and fabric (e.g.,
trivalent suit). For eye and face protection, wear chemical safety glasses; or face shield with
safety glasses. General first aid measures include never give anything by mouth to an
unconscious person. If feeling unwell, see medical advice. After skin contact, remove

Dispersants

177

CHIMEC CHIMSPERSE 6000


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contaminated clothing and drench affected area with water for at least 15 minutes. Obtain
medical attention if irritation develops or persists. In case of eye contact, immediately rinse with
water for at least 15 minutes. Remove contact lenses, if present and easy to do. Continue rinsing.
Get immediate medical advice/attention. If ingested, rinse mouth. DO NOT induce vomiting and
obtain medical attention.

4.a. Maximum storage temperature: 104°F (40°C) continuous
4.b. Minimum storage temperature: -4°F (-20°C)

4.c. Optimum storage temperature range: 32°F (0°C) to 80°F (27°C)

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

The shelf life of opened containers is 12 months. If sealed as delivered, shelf life of closed
containers is 24 months. Shelf life may be extended to 48 months after analytical checks.
According to internal procedures for dispersant products, after 24 months the Chimec Quality
Control department checks analytical parameters based on technical specifications before
extending shelf life to 48 months.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: CHIMEC CHIMSPERSE 6000 may be applied by the usual methods
(e.g., NIMBUS package, the Modular Aerial Spray System (MASS) package, or the Aerial
Dispersant Delivery System (ADDS) package). The preferred and most effective method of
application from a workboat is to use a low-volume, low-pressure pump.

2.	Concentration/Application Rate: CHIMEC CHIMSPERSE 6000 is preferably used undiluted.
A typical treatment rate is 10 to 15 L/acre or a DOR (dispersant to oil ratio) of 1:50 to 1:10.
However, the treatment rate can vary depending on the type or oil, degree of weathering,
temperature, and thickness of oil slick. For heavy oils, a 1:10 dilution ratio (product: water) is
recommended. Lighter oils will require a 1:10 to 1:30 (product:water) dilution ratio. Warmer
waters (greater than 78°F) and/or good agitation during application will require less product.

3.	Conditions for Use: CHIMEC CHIMSPERSE 6000 can be used in salt water, with no
limitations as to usage if within optimum temperature parameters (application may be made at or
above 35°F, with optimum above 48°F).

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested
CHIMSPERSE 6000

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)

2.51	96-hr

3.43	48-hr
4.48	96-hr
3.26	48-hr
3.01	96-hr
1.88	48-hr
1.86	96-hr

9.44	48-hr

No. 2 Fuel Oil

CHIMSPERSE 6000 & No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

Dispersants

178

CHIMEC CHIMSPERSE 6000


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b. Effectiveness:

SWIRLING FLASK DISPERSANT EFFECTIVENESS TEST WITH SOUTH

LOUISIANA (S/L) AND PRUDHOE BAY (P/B) CRUDE OILS

Oil	Effectiveness (%

Prudhoe Bay Crude	48.30

South Louisiana Crude	58.50

Average of Prudhoe Bay and South Louisiana Crudes	53.40

VIII. MICROBIOLOGICAL PROPERTIES

NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >100°F

2.	Pour Point: -28°C

3.	Viscosity: 26.8 cSt at 40°C

4.	Specific Gravity: 0.9987 at 60°F

5.	pH: 7.3

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

9.	Additives: None

10.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	1.24

Cadmium	<0.122

Chromium	0.254

Copper	<0.272

Lead	<0.118

Mercury	<0.0132

Nickel	0.778

Zinc	5.24

Cyanide	1.75

Chlorinated hydrocarbons	<1.80

Dispersants

179

CHIMEC CHIMSPERSE 6000


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MISCELLANEOUS OIL SPILL CONTROL AGENTS:
TECHNICAL NOTEBOOK BULLETINS

Miscellaneous Oil Spill Control Agents

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Miscellaneous Oil Spill Control Agents


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TECHNICAL PRODUCT BULLETIN #M-12

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 31, 1992

REVISED LISTING DATE: SEPTEMBER 13, 1995

"PES-51"

I.	NAME, BRAND, OR TRADEMARK
PES-51

Type of Product: Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Practical Environmental Solutions (Formerly known as Petroleum Environmental Services)
P.O. Box 12563

San Antonio, Texas 78212
Phone: (210) 493-7172
Mobile Phone: (210) 875-4011
Fax: (210) 493-7172
E-mail: simsbi@aol.com
Website: www.pes51.com
(Mr. Bill Sims)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Practical Environmental Solutions (Formerly known as Petroleum Environmental Services)
P.O. Box 12563

San Antonio, Texas 78212
Phone: (210) 493-7172
Mobile Phone: (210) 875-4011
Fax: (210) 493-7172
E-mail: simsbi@aol.com
Website: www.pes51.com
(Mr. Bill Sims)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: 124°F

2.	Ventilation: Handle product in a normal well ventilated place.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Although PES-51 is
expected not to pose any specific health hazard, the following precautions are recommended due
to possible irritation from the biological by-produc2ts contained in the product: Avoid contact
with skin, eyes, and clothing. Avoid prolonged or repeated contact with skin, breathing mist, and
do not take internally. Keep product away from heat, sparks, and flames, and store in a cool, dry,
well ventilated place, away from incompatible materials. Vent container in warm weather to
relieve pressure. Do not cut, grind, weld, or drill on or near product containers. Handle empty
containers just as would the full ones.

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4.a. Maximum storage temperature: NA.

4.b. Minimum storage temperature: NA
4.c. Optimum storage temperature range: NA

4.d. Temperatures of phase separations and chemical changes: Not applicable, butPES-51
freezes at -142°F.

V.	SHELF LIFE

6 years (unopened drum), 1 year (opened drum).

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: The following PES-51 application methods are applicable for the full
range of PES-51 industrial uses, including shoreline and surface treatment, tank cleaning and
equipment decontamination. The selection of the method(s) will be dependent on the level and
extent of hydrocarbon contamination, type of oil, and its degree of weathering/emulsion and the
nature and type of surface to be treated or cleaned. Equipment availability, logistics and
manpower requirements should also be considered. Application methods may be combined, if
necessary. In addition, for shoreline cleaning, the treatment area will be boomed and contained
prior to PES-51 usage. For equipment decontamination, the use of portable de-con pools or
secondary containment liners are recommended.

PORTABLE EQUIPMENT

Hand Held Spraying - Spray PES-51 on the contaminated area using a Chapin Steel Sprayer
#1729 (or equivalent), 2.5 gallons capacity, or the AU 8000 MicroNair sprayer. After
application, allow 3 to 5 minutes for soaking without allowing evaporation of PES-51 (weather
dependent). When saturation is attained, hydrocarbon will be seen running off the impacted
surface. Rinse the treated surface with available water (fresh or sea water) from the pump until
no hydrocarbon remains. The water should be used at ambient temperature. Depending on level
and extent of contamination, a pressure washer may also be used for rinsing (ambient may be
used). Collect the effluent hydrocarbons with absorbent booms and pads, and squeeze off the oil
contaminants from the booms and pads for reuse as process oil.

Airless Sprayer - Depending on the level and extent of the hydrocarbon contamination and the
nature of the impacted surface, an airless type sprayer may be used for direct product application.
Common types of airless sprayers are: Airlessco, Graeco or equivalents. These airless sprayers
can have single or multi-hose attachments and can include wand extensions as required.

Application rate and pressure will vary depending on the equipment type and site specific
conditions. After spraying with PES-51, allow to soak for 3 to 5 minutes (weather dependent)
avoiding evaporation, rinse/flush surfaces with pumps, fire hoses, deluge headers or pressure
washers (ambient).

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Pressure Washer with Syphon Feed System - Depending on the level and extent of the
hydrocarbon contamination and the nature of the impacted surface proposed for treatment, a
pressure washer may be used for direct product application. In most applications, hot water
(greater than 120°F) is not necessary. Common types of pressure washers are: Hotsy and
Lambda, or equivalents. These pressure washers have a variable rate "detergent syphon feed"
system for PES-51 application and can have single or multi-hose attachments which can include
wand extensions. Application rate and pressure will vary depending on equipment type and site
specific conditions.

After spraying with PES-51, allow to soak for 3 to 5 minutes (weather dependent) avoiding
evaporation, rinse/flush surfaces with pumps, fire hoses, deluge headers or pressure washers
(ambient).

Air Knife (Modified for PES-51 Application) - PES has developed a patent-pending modified air
knife system for product application. This method was developed primarily for rocky, cobble,
bedrock type shorelines with both surface subsurface oil. The modified air knife delivers the
PES-51 in both a liquid stream (125 psi) or as an aerosol. Compressed air is used to dilate
subsurface sediments and allow for distribution of the PES-51. The air knife method is also
applicable for surface treatment of impacted rocks, bulkheads, seawalls, rip-rap jetties, etc.

After spraying with PES-51, allow to soak for 3 to 5 minutes (weather dependent) avoiding
evaporation, rinse/flush surfaces with pumps, fire hoses, deluge headers or pressure washers
(ambient). For subsurface treatment, continue flushing with large quantities of low-pressure
seawater at ambient temperatures.

MOBILE EQUIPMENT

Boat Spraying - The recommended application rate is 1 to 5 gallons per 200 sq. ft., from a boat
with speed of 1 to 3 knots, depending on the sea conditions and oil film thickness on the rocks.
For a boat with a mounted AU-8110 MicroNair sprayer (or equivalent sprayer) and a spray swath
of about 20 feet, traveling at approximately two knots, 25 acres/hr will be treated.

After spraying, rinse PES-51 off the rocks with a hard, coarse spray of sea water. Standard size
pumps with fire hoses or deluge headers may be used. Higher pressure rinses may be required if
oil is thick and weathered. The shoreline may also be sprayed from the beach side, which will
force the oil into the containment boom.

Helicopter Deployed Spraying - Aerial spraying can be utilized for shore treatments and
pretreatment with the AU 5000 atomizer (MicroNair) or equivalent sprayer.

The recommended aerial application of PES-51 is 14 to 23 liters/minute. The AU 5000 (or
equivalent) can be used with fixed-wing aircraft and helicopters operating at speeds of 90 MPH
(145 km/hr) and more. The smaller AU 7000 sprayer (or equivalent) is recommended for use at
airspeeds below 90 MPH. After spraying, the hydrocarbons can be rinsed off the shore rocks as
described above with hand held pumps, deluge headers or boat spraying.

Vehicular Spraying - The recommended vehicular spraying is 50 to 150 ft2/gallon depending on
climatic conditions. A MicroNair vehicle-mounted sprayer is recommended. This unit is a self-

Miscellaneous Oil Spill Control Agents

183

PES-51


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contained sprayer kit that combines the AU 8000 sprayhead (or equivalent) with a powerful 4-
stroke engine and a 60 liter chemical tank to give complete product coverage. After spraying,
the hydrocarbons can then be rinsed off the shore rocks as described above with hand held
pumps, deluge headers or boat spraying.

2.	Concentration/Application Rate: The product comes already mixed, and ready for use.
For specific application, see rate of application as indicated above.

3.	Conditions for Use: Water temperature and salinity do not affect the product performance.
PES-51 is effective against hydrocarbons only, and the age of the hydrocarbon is not relevant.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

PES-51

Menidia beryllina

137.00 96-hr



Mysidopsis bahia

54.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

200.00 96-hr



Mysidopsis bahia

11.50 48-hr

PES-51 &

Menidia beryllina

435.00 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

14.50 48-hr

Reference Toxicant (DSS)

Menidia beryllina

2.20 96-hr



Mysidopsis bahia

9.80 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 124°F

2.	Pour Point: -50°F at 30 min.

3.	Viscosity: 30 cSt at 28°C

4.	Specific Gravity: 0.840 at 25°C

5.	pH: 6.7

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

9.	Additives: CONFIDENTIAL

10.	Solubility: NA

Miscellaneous Oil Spill Control Agents

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PES-51


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X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<

0.005

<

0.01

<

0.05

<

0.05

<

0.05

<

0.005

<

0.01

<

0.05

<

1.00

<

0.01

Miscellaneous Oil Spill Control Agents

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PES-51


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #M-17
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: FEBRUARY 25, 1994
REVISED LISTING DATE: JUNE 14, 1995
"CIAGENT"

I.	NAME, BRAND, OR TRADEMARK
CIAGENT

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier
(formerly CI AGENT, CHEAP INSURANCE, & PETRO-CAPTURE)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
CIAGENT Solutions, LLC

11760 Commonwealth Dr.

Louisville, KY 40299
Phone: updated information required
Fax: updated information required
E-mail: dan@ciagent.com
(Mr. Dan Parker)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
CIAGENT Solutions, LLC

11760 Commonwealth Dr.

Louisville, KY 40299
Phone: updated information required
Fax: updated information required
E-mail: dan@ciagent.com
(Mr. Dan Parker)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Flammable solid at >210°F.

2.	Ventilation: Normal ventilation is adequate.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Product may cause
slight eye irritation if in contact with eyes. Use protective eye goggles when handling the
product. In case of eye contact, flush eyes with water. In an enclosed environment, workers
should wear a dust mask for personal comfort. In case of a confined space fire, do not enter
without full bunker gear and positive pressure NIOSH approved self-contained breathing
apparatus. Maintain fire watch at 450°F.

4.a.	Maximum storage temperature: 190°F
4.b. Minimum storage temperature: None

4.c. Optimum storage temperature range: 50°F - 80°F

3/17/2016
7/27/2022

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4.d. Temperatures of phase separations and chemical changes: None. Avoid contact with strong
oxidizing agents due to possible oxidation reaction with the product.

V.	SHELF LIFE

> 5 years, if stored in cool dry area, away from direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: For small scale spills on water (salt or fresh), CIAGENT can be
broadcast directly onto the spill, spreading a thin layer from the outer edge into the middle of the
spill. Agitation is not necessary. The product is also available in oil absorbent, water repellant
booms and pillows. For large spills on water (fresh or salt), CIAGENT may be deployed with an
air or water stream directed at the leading edge of the spill. Because of its fine particulate nature,
static buildup may occur if the product is applied in dry form at a high rate of delivery.
Dispensing material should be properly grounded to prevent this. The product is relatively non-
abrasive and should not harm machinery or pumping systems. Agitation is not necessary.

The polymer has a specific gravity of less than one and will tend to separate and move to the
surface when mixed with water. Therefore, in the case of water carrying media, the product
should be introduced "just in time" as the media is sprayed, or agitation will be needed to keep
the product suspended. The product will remove oils and other hazardous hydrocarbon based
materials from fresh or salt water. CIAGENT may be used in a flow-through filter to remediate
contaminated water. CIAGENT encapsulates and solidifies the oil, while continuing to float
even after saturation. The solidified oil or hazardous material may be removed from water using
a vacuum pump or fish net. The material should be put into appropriate containers and disposed
of in accordance with federal, state and local regulations. For spills on land, the product would
be applied in the same manner as in the water-based spill situation. Agitation is not necessary.
To recover solidified oil or hazardous materials from spills on land, the spent material may be
collected and swept up using an industrial vacuum cleaner, broom, or shovel. The material
should be put into appropriate containers and disposed of in accordance with federal, state and
local regulations.

2.	Concentration/Application Rate: In general, a 10% to 30% by weight application is required to
solidify light, medium, and heavy oils. Solidification may occur faster if additional CIAGENT is
applied.

3.	Conditions for Use: CIAGENT is equally effective in fresh or salt water, and under any
weather conditions; however, colder temperatures may slow the solidification process. The
product is most effective on water temperatures between 32°F and 120°F. Depending on the age
and/or viscosity of the material, varying amounts of CIAGENT may be required to obtain
complete solidification. The recovered solidified oil or hazardous materials may be landfilled,
incinerated, used as a secondary fuel, or otherwise disposed of according to federal, state and
local regulations.

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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (ppm)

CIAGENT

Menidia beryllina

2227.00 96-hr



Mysidopsis bahia

2617.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

4.36 96-hr



Mysidopsis bahia

1.45 48-hr

CIAGENT &

Menidia beryllina

5.93 96-hr

No. 2 Fuel (1:10)

Mysidopsis bahia

1.73 48-hr

Reference Toxicant (DSS)

Menidia beryllina

3.68 96-hr



Mysidopsis bahia

6.82 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

IX. PHYSICAL PROPERTIES AND COMPONENTS

1.	Flash Point: No flash observed at 210DF.

2.	Pour Point: Not applicable; solid samples

3.	Viscosity: Not applicable; solid samples

4.	Specific Gravity: 0.94 g/cm3

5.	pH: 7.81

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: None

8.	Solvents: None

9.	Additives: None

10.	Solubility: Negligible

X. ANALYSIS FOR HEAVY METALS AND CHLORINATED HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.0

Cadmium	<2.5

Chromium	<2.0

Copper	<2.5

Lead	<5.0

Mercury	<0.050

Nickel	<5.0

Zinc	<2.5

Cyanide	<0.50

Chlorinated Hydrocarbons	ND

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CIAGENT


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TECHNICAL PRODUCT BULLETIN #M-18

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 29, 1994

REVISED LISTING DATE: MARCH 12, 1997

"ZYME-FLOW"

(aka, ZYME-TREAT, MARI-ZYME, UNITED 658 PETRO-ZYME)

I.	NAME, BRAND, OR TRADEMARK
ZYME-FLOW

(aka, ZYME-TREAT, MARI-ZYME, UNITED 658 PETRO-ZYME)Type of Product:
Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
United Laboratories, Inc.

320 37th Avenue
St. Charles, IL 60174

Phone: (630) 377-0900 x7408 or (800) 323-2594
Fax: (630) 377-0960
E-mail: nsherrel@unitedlabsine.com
(Ms. Nancy Sherrel)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
United Laboratories, Inc.

320 37th Avenue
St. Charles, IL 60174

Phone: (630) 377-0900 x7408 or (800) 323-2594
Fax: (630) 377-0960
E-mail: nsherrel @unitedl ab sine. com
(Ms. Nancy Sherrel)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: No mechanical ventilation required

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact due
to possible mild eye irritation. In case of eye contact, flush eyes with water. Protective clothing
is normally not required.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 0°F - 120°F

4.d. Temperatures of phase separations and chemical changes: > 3 freeze-thaw cycles.

V.	SHELF LIFE
1 year minimum.

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VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: United's ZYME-FLOW is a chemically designed product that will make
heavy crudes more pumpable, and break the adhesion between oils and soil, rock or sand.
ZYME-FLOW can be applied where the contaminated soil or sand is temporarily removed and
placed into a device that can provide mechanical agitation (e.g., a cement mixer or a
fractionating tank). Unagitated tanks may also be used, but more time will be required to
achieve the goal.

Add ZYME-FLOW solution to the tank. As agitation continues, oils with a specific gravity of
less than one will float, while oils with a specific gravity of greater than one will settle.
The floating or settled oil can then be removed from the soil or sand. As ZYME-FLOW will not
emulsify oils, the recovered oils are almost anhydrous, and the water can be collected and reused.
Another method is to physically isolate a small area that is to be cleaned with damming collars,
sand bags or other means on the sides and a none permeable layer on the bottom (if possible).
Then wash the contaminated area with ZYME-FLOW solution using a pressurized water stream.
Keep the area super-saturated with water for several hours to allow oil residues to float to the
surface for collection.

ZYME-FLOW can be used to wash the inside or outside of a ship or barge that has been
contaminated with oil, using a high pressure sprayer. Bilges of a ship, or barge can also be
cleaned using a 1% ZYME-FLOW solution, and allowing the natural movement of the ship to
provide the agitation.

2.	Concentration/Application Rate: The exact dilution of ZYME-FLOW will vary between 50:1
and 200:1 depending on temperature, viscosity and type of petroleum product.

3.	Conditions for Use: ZYME-FLOW is effective in all non-frozen waters with greater efficacy
as the temperature increases. The product efficiency is not affected by salinity, but it will be
affected by tar sand.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

ZYME-FLOW

Menidia beryllina

35.00 96-hr



Mysidopsis bahia

26.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

6.90 96-hr



Mysidopsis bahia

3.70 48-hr

ZYME-FLOW &

Menidia beryllina

8.70 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.60 48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.07 96-hr



Mysidopsis Bahia

18.60 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this

bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

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ZYME-FLOW


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IX. PHYSICAL PROPERTIES

1.	Flash Point: None

2.	Pour Point: 32°F

3.	Viscosity: <10 cps

4.	Specific Gravity: 0.99

5.	pH: 7.0 - 8.0

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: NA

9.	Additives: CONFIDENTIAL

10.	Solubility: Soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.005

Cadmium	0.002

Chromium	0.002

Copper	0.020

Lead	0.007

Mercury	0.0004

Nickel	0.070

Zinc	0.040

Cyanide	0.300

Chlorinated Hydrocarbons	<1.00

Miscellaneous Oil Spill Control Agents

191

ZYME-FLOW


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

11/03/2008
7/27/2022

TECHNICAL PRODUCT BULLETIN #M-19

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 22, 1996

"WASTE-SET #3200®"

I.	NAME, BRAND, OR TRADEMARK
WASTE-SET #3200®

Type of Product: Miscellaneous Oil Spill Control Agent - Oil Spill Solidifying Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Environmental & Fire Technology, LLC

Address: updated information required
Phone: updated information required
(Mr. Cal Blystra)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Environmental & Fire Technology, LLC

Address: updated information required
Phone: updated information required
(Mr. Cal Blystra)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Product will not burn unless preheated. Avoid elevated temperatures (>200°F)
for extended periods (>5 days).

Product has a tendency to accumulate a static charge during transport, which is a potential fire
hazard if used near flammables.

2.	Ventilation: Avoid generating dust clouds.

3.	Skin and eye contact; protective clothing; treatment in case of contact: May cause mild
mechanical irritation to eyes, skin and respiratory tract. Dust may cause coughing and watery
eyes. Pre-existing eye, skin and respiratory disorders may be aggravated by this product. Wear
NIOSH-approved respirator to prevent overexposure. Refer to transitional occupational
exposure limits established by OSHA in 29CFR 1910.1000. Flush eyes with water; wash skin
with soap and water; if molten, treat as for burns. Remove person(s) to fresh air if excessive
amounts of dust have been inhaled. Protective gloves and safety glasses should be worn.

If material is released or spilled, sweep up or vacuum and place in an approved container.

4.a.	Maximum storage temperature: 200°F
4.b. Minimum storage temperature: None

4.c. Optimum storage temperature range: <200°F

4.d. Temperatures of phase separations and chemical changes: >450°F

Miscellaneous Oil Spill Control Agents

192

WASTE-SET #3200


-------
V. SHELF LIFE
Unlimited.

VI. RECOMMENDED APPLICATION PROCEDURE
1 .Application Method:

Spills on Water - For spills on water, surround the spill with WASTE-SET® 3200 to prevent
migration. Reinforce containment line with a boom or sweep if necessary. WASTE-SET® and
the resulting reacted material will float.

If the interior of the diked spill is not to be reclaimed, fill in the remaining surface area of the
spill by broadcasting additional WASTE-SET® 3200 evenly over the spill until the WASTE-
SET® no longer reacts with the spill. Alternatively, the product may be introduced under the
surface of the spill to rise and react with oils in the suspension layer.

WASTE-SET® can then be swept or netted from the surface of the water.

Spills on Hard Surfaces - For spills on hard surfaces, apply WASTE-SET 3200® heavily to
perimeter of spill to prevent migration. After surrounding the spill, reinforcement of the
containment line thus formed with a boom or sweep may be advisable depending on the volume
and flow rate.

If the interior of the diked spill is not to be reclaimed, fill in the remaining surface of the spilled
material by evenly distributing additional WASTE-SET 3200® until the WASTE-SET® no
longer reacts with the spill and remains white and on the surface.

Disposal - Dispose of reacted material in accordance with local, state, and federal regulation.
Under the EPA Toxicity Characteristic Leaching Procedures (TCLP), WASTE-SET
encapsulated material may be eligible for disposal in landfills. Incineration results in extremely
low ash content. Dependent upon the nature of the encapsulated material, it may also be
disposed of by incorporation into synthetic surfaces such as asphalt.

WASTE-SET® will effectively "encapsulate" crude oil and petroleum-based products, such as
gasoline, kerosene, and diesel fuel; in addition to the various following liquid and vapor-phase
contaminants:

Aliphatic hydrocarbons	Esters

Aromatic hydrocarbons	Ethers

Chlorinated hydrocarbons	Ketones

Alcohols	Other hydrocarbons

2.	Concentration/Application Rate: One pound WASTE-SET® per five pounds of oil (May vary
with viscosity and temperature).

3.	Conditions for Use: No limitations.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested	Species	LC50 (ppm)

WASTE-SET 3200®	Menidia beryllina	>10000.0 96-hr

Miscellaneous Oil Spill Control Agents

193

WASTE-SET #3200


-------
Mysidopsis bahia	5431.0 48-hr

No. 2 Fuel Oil	Menidia beryllina	274.0 96-hr

Mysidopsis bahia	29.0 48-hr

WASTE-SET 3200® &	Menidia beryllina	552.0 96-hr

No. 2 Fuel Oil	Mysidopsis bahia	58.0 48-hr

Reference Toxicant (SDS)	Menidia beryllina	1.8 96-hr

Mysidopsis bahia	4.9 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: No flash observed at 310°F

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 0.94

5.	pH: NA

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: NA

8.	Solvents: None

9.	Additives: None

10.	Solubility: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.44

Copper	0.98

Lead	0.08

Mercury	ND

Nickel	0.38

Zinc	3.1

Cyanide	ND

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

194

WASTE-SET #3200


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

11/03/2008
7/27/2022

TECHNICAL PRODUCT BULLETIN #M-20

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 22, 1996

"WASTE-SET #3400®"

I.	NAME, BRAND, OR TRADEMARK
WASTE-SET #3400®

Type of Product: Miscellaneous Oil Spill Control Agent - Oil Spill Solidifying Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Environmental & Fire Technology, LLC

Address: updated information required
Phone: updated information required
(Mr. Cal Blystra)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Environmental & Fire Technology, LLC

Address: updated information required
Phone: updated information required
(Mr. Cal Blystra)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Product will not burn unless preheated. Avoid elevated temperatures (>200°F)
for extended periods (>5 days). Product has a tendency to accumulate a static charge during
transport, which is a potential fire hazard if used near flammables.

2.	Ventilation: Avoid generating dust clouds.

3.	Skin and eye contact; protective clothing; treatment in case of contact: May cause mild
mechanical irritation to eyes, skin and respiratory tract. Dust may cause coughing and watery
eyes. Pre-existing eye, skin and respiratory disorders may be aggravated by this product. Wear
NIOSH-approved respirator to prevent overexposure. Refer to transitional occupational
exposure limits established by OSHA in 29CFR 1910.1000. Flush eyes with water; wash skin
with soap and water; if molten, treat as for burns. Remove person(s) to fresh air if excessive
amounts of dust have been inhaled. Protective gloves and safety glasses should be worn.

If material is released or spilled, sweep up or vacuum and place in an approved container.

4.a.	Maximum storage temperature: 200°F
4.b. Minimum storage temperature: None

4.c. Optimum storage temperature range: <200°F

4.d. Temperatures of phase separations and chemical changes: >450°F

Miscellaneous Oil Spill Control Agents

195

WASTE-SET #3400


-------
V. SHELF LIFE
Unlimited.

VI. RECOMMENDED APPLICATION PROCEDURE
1. Application Method:

Spills on Water - For spills on water, surround the spill with WASTE-SET® 3400 to prevent
migration. Reinforce containment line with a boom or sweep if necessary. WASTE-SET® and
the resulting reacted material will float. If the interior of the diked spill is not to be reclaimed,
fill in the remaining surface area of the spill by broadcasting additional WASTE-SET 3400®
evenly over the spill until the WASTE-SET® no longer reacts with the spill. Alternatively, the
product may be introduced under the surface of the spill to rise and react with oils in the
suspension layer. WASTE-SET® can then be swept or netted from the surface of the water.

Spills on Hard Surfaces - For spills on hard surfaces, apply WASTE-SET® 3400 heavily to
perimeter of spill to prevent migration. After surrounding the spill, reinforcement of the
containment line thus formed with a boom or sweep may be advisable depending on the volume
and flow rate. If the interior of the diked spill is not to be reclaimed, fill in the remaining surface
of the spilled material by evenly distributing additional WASTE-SET® 3400 until the WASTE-
SET® no longer reacts with the spill and remains white and on the surface.

Disposal - Dispose of reacted material in accordance with local, state, and federal regulation.
Under the EPA Toxicity Characteristic Leaching Procedures (TCLP), WASTE-SET®
encapsulated material may be eligible for disposal in landfills. Incineration results in extremely
low ash content. Dependent upon the nature of the encapsulated material, it may also be
disposed of by incorporation into synthetic surfaces such as asphalt.

WASTE-SET® will effectively "encapsulate" crude oil and petroleum-based products, such as
gasoline, kerosene, and diesel fuel; in addition to the various following liquid and vapor-phase
contaminants:

Aliphatic hydrocarbons	Esters

Aromatic hydrocarbons	Ethers

Chlorinated hydrocarbons	Ketones

Alcohols	Other hydrocarbons

2.	Concentration/Application Rate: One pound WASTE-SET® per five pounds of oil (May vary
with viscosity and temperature).

3.	Conditions for Use: No limitations.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested Species	LC50 (ppm)

WASTE-SET 3400® Menidia beryllina	>10000.0 96-hr

Mysidopsis bahia	>10000.0 48-hr

No. 2 Fuel Oil Menidia beryllina	274.0 96-hr

Mysidopsis bahia	29.0 48-hr

Miscellaneous Oil Spill Control Agents

196

WASTE-SET #3400


-------
WASTE-SET 3400® &	Menidia beryllina	442.0 96-hr

No. 2 Fuel Oil	Mysidopsis bahia	36.0 48-hr

Reference Toxicant (SDS)	Menidia beryllina	1.8 96-hr

Mysidopsis bahia	4.9 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: No flash observed at 350°F

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 0.91

5.	pH: NA

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: NA

8.	Solvents: None

9.	Additives: None

10.	Solubility: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.41

Copper	0.97

Lead	0.08

Mercury	ND

Nickel	3.3

Zinc	4.0

Cyanide	ND

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

197

WASTE-SET #3400


-------
TECHNICAL PRODUCT BULLETIN #M-22

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: FEBRUARY 27, 1998

REVISED LISTING DATE: OCTOBER 5, 1998

"PX-700®"

I.	NAME, BRAND, OR TRADEMARK
PX-700®

Type of Product: Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Enviro-Tech

715 NE 19th Place #22
Cape Coral, FL 33909
Phone: (239) 673-8280
Fax: (239) 424-8408
E-mail: info@px700.com
Website: www.px700.com
(Mr. Charlie Jones)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Enviro-Tech

715 NE 19th Place #22
Cape Coral, FL 33909
Phone: (239) 673-8280
Fax: (239) 424-8408
E-mail: info@px700.com
Website: www.px700.com
(Mr. Charlie Jones)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Not flammable; no special precautions necessary.

2.	Ventilation: None required; no vapor emissions at normal temperatures, summer and winter.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Product contains a
surfactant; avoid prolonged skin contact. Mild eye irritant; in case of eye contact, flush with
copious amounts of water. No protective clothing required. Contact treatment is to flush with
water. Product is acidic (pH 3.5-4.0). Eye protection is recommended as a precaution against
splashing.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 30°F

4.c. Optimum storage temperature range: 65°F - 85°F

4.d. Temperatures of phase separations and chemical changes: Separation may occur after 3
months. Separation will not affect product performance.

Miscellaneous Oil Spill Control Agents

198

PX-700™


-------
V.	SHELF LIFE
Two years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: To remove oily sheen from areas surrounding an oil spill, spray
undiluted PX-700® directly over area at an application rate of one gallon for every 900 to 1200
square feet of surface area. Dilute PX-700® 25:1 for cleaning equipment and other surfaces.
Either spray or immerse equipment, as applicable. Dilute PX-700® 50:1 for immersing wildlife
to remove oil.

2.	Concentration/Application Rate: At normal temperatures product is free flowing and applied
full strength to remove oily sheen from aquatic environments, soils, and wastewater.

3.	Conditions for Use: Water salinity, water temperature, types and ages of pollutants. Do not
allow product to freeze, as separation may occur. Product may work more slowly at low
temperatures. At full strength or diluted with fresh water, product will have a specific gravity
lower than sea water and should float. Use of PX-700® should aid skimming and other
conventional oil recovery operations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (DDm)

PX-700®

Menidia beryllina

380.00 96-hr



Mysidopsis bahia

297.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

7.07 96-hr



Mysidopsis bahia

1.89 48-hr

PX-700®

Menidia beryllina

5.65 96-hr

& No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.77 48-hr

Reference Toxicant (DDS)

Menidia beryllina

6.16 96-hr



Mysidopsis bahia

23.00 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness
NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: Not flammable

2.	Pour Point: 30°F

3.	Viscosity: Equivalent to water

4.	Specific Gravity: 1.0

5.	pH: 3.5 to 4.0 standard units

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

Miscellaneous Oil Spill Control Agents

199

PX-700™


-------
7.	Surface Active Agents: Less than 5% Cocamide

8.	Solvents: None

9.	Additives: Citric acid for pH control

10.	Solubility: 100% soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.47

Cadmium	ND

Chromium	ND

Copper	0.14

Lead	ND

Mercury	ND

Nickel	ND

Zinc	0.77

Cyanide	ND

Chlorinated Hydrocarbons	CONFIDENTIAL

Miscellaneous Oil Spill Control Agents

200

PX-700™


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TECHNICAL PRODUCT BULLETIN #M-23

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 23, 1998

"ALSOCUP"

I.	NAME, BRAND, OR TRADEMARK
ALSOCUP

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
REVCOM Associates

1550 Rimpau Avenue #53
Corona, CA 92881
Phone: (951)737-0104
E-mail: revcom@sbcglobal.net
(Mr. Dave Naylor, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
REVCOM Associates

1550 Rimpau Avenue #53
Corona, CA 92881
Phone: (951)737-0104
E-mail: revcom@sbcglobal.net
(Mr. Dave Naylor, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: NA

2.	Ventilation: NA

3.	Skin and eye contact; protective clothing; treatment in case of contact: ALSOCUP is
practically non-irritating to the eyes and is non-irritating to the skin. Safety glasses and
protective clothing should be worn when applying the material. The product is not expected to
cause irritation to the nose, throat, or respiratory tract.

4.a.	Maximum storage temperature: 163°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 0°F to 163°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

ALSOCUP has a shelf life of five years.

Miscellaneous Oil Spill Control Agents

201

ALSOCUP


-------
VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: ALSOCUP is used to collect petroleum-based products spilled on water
or land. When ALSOCUP comes into contact with a petroleum product it chemically bonds and
traps the petroleum. Once captured, spilled product cannot be released from ALSOCUP.
ALSOCUP does not absorb water and will not sink. The product can be collected by skimming
with pumps or mechanical devices.

2.	Concentration/Application Rate: ALSOCUP is used by applying one pound of product to
each 10 pounds of spilled petroleum products.

3.	Conditions for Use: Water temperature does not appear to affect the ability of ALSOCUP to
collect petroleum products. Heavy seas may prevent containment of an oil spill, and the product
would lose efficiency if the oil product dispersed. Booms and dams that contain the petroleum
product into an area are most effective when using ALSOCUP. In water the motion of the sea
will mix the product with oil. On land a mechanical means is necessary to combine the oil with
ALSOCUP. ALSOCUP will collect petroleum products at any stage; however, it is most
effective early in the spill before dispersion.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

ALSOCUP is a non-toxic substance. The product is generally considered to have a low order of
acute oral toxicity.

Material Tested

Species

LC50

(DDm)

ALSOCUP

Menidia beryllina

>100

96-hr



Mysidopsis bahia

>100

48-hr

No. 2 Fuel Oil

Menidia beryllina

8.1

96-hr



Mysidopsis bahia

3.9

48-hr

ALSOCUP & No. 2 Fuel Oil (1:10)

Menidia beryllina

14.0

96-hr



Mysidopsis bahia

10.0

48-hr

Reference Toxicant (DSS)

Menidia beryllina

NA





Mysidopsis bahia

NA



VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: NA

5.	pH: NA

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: NA

9.	Solubility in Water: NA

Miscellaneous Oil Spill Control Agents

202

ALSOCUP


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.0211

0.090

0.456

0.445

0.454

0.00492

0.474

0.433

ND

NA

Miscellaneous Oil Spill Control Agents

203

ALSOCUP


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

5/18/2006
7/27/2022

TECHNICAL PRODUCT BULLETIN #M-24

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JANUARY 26, 2001

"RAPIDGRAB 2000™"

I.	NAME, BRAND, OR TRADEMARK
RAPIDGRAB 2000™

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76517

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
GlobeMark Resources Ltd.

1312 Mill Creek Drive

Sal ado, TX 76517

Mobile: (254) 231-2251

E-mail: fiddler656@gmail.com

Website: www.globemarkresources.com

(Ms. Joannie Docter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-flammable; DOT - Non-hazardous

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in a moderate breeze.

3.	Skin and eye contact; protective covering; treatment in case of contact: Avoid skin and
clothing contact. If skin contact occurs, immediately wash with large amounts of water and soap
(if possible). Remove any contaminated clothing or shoes. Launder before reusing. If irritation
persists, seek medical assistance. For areas where contact is likely, wear long sleeve shirt,
chemical resistant gloves, and chemical resistant goggles.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 32°F to 90°F

4.d. Temperatures of phase separations and chemical changes: None

Miscellaneous Oil Spill Control Agents

204

RAPIDGRAB 2000™


-------
V.	SHELF LIFE

The shelf life of unopened drums of RAPIDGRAB 2000™ is unlimited. Containers should be
capped when not being used to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: RAPIDGRAB 2000™ is a non-ionic liquid formulation that may be
effectively applied by mist spraying onto floating oil slicks and sheens that are often found in
harbors and at sea as the result of oil leakage and spills from ships. It instantly reduces and
confines floating oils by the oleophitic synergistic effect of contraction and congealment into a
physical state that greatly simplifies cleanup operations. Oil slicks and sheens may be reduced
by up to 1,000 percent or more. The broad temperature range for RAPIDGRAB 2000™ sprays
are from 32°F to 120°F.

Aerial Spraying - Typical application altitudes of 30 to 50 feet are advised although higher
altitudes may be used if condition warrant. Spray nozzle should be about Vi inches in diameter at
104 knots or more to create enough air shear sufficient to break the RAPIDGRAB 2000™ into
proper sized droplets. A '/2-inch diameter nozzle may be needed for temperatures below 50°F.

Boat Spraying - Mist sprays may be applied from shipboard by power "foggers."

2.	Concentration/Application Rate: RAPIDGRAB 2000™ should be mist sprayed full strength
on surface oil until sufficient herding results are achieved. Results will vary depending on oil
type, temperature, wave action, and viscosity.

3.	Conditions for Use: RAPIDGRAB 2000™ is designed to be used after oil has been contained
by booms or other similar apparatus. Timely treatment with RAPIDGRAB 2000™, even at low
application rates, can help to contain the sheen/spreading effect of the oil slick.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity
Material Tested
RAPIDGRAB 2000™

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
5.13 96-hr
2.29 48-hr
9.34 96-hr
3.12 48-hr
4.07 96-hr
2.60 48-hr
2.97 96-hr
6.71 48-hr

No. 2 Fuel Oil

RAPIDGRAB 2000™ &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SRTT)

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Miscellaneous Oil Spill Control Agents

205

RAPIDGRAB 2000™


-------
IX. PHYSICAL PROPERTIES

1.	FlashPoint: 110°C

2.	Pour Point: 30°F

3.	Viscosity: 20.2

4.	Specific Gravity: 0.84

5.	pH: 6.95

6.	Surface Active Agents: Oleophitic surfactant

7.	Solvents: Proprietary formulation oleophitic surfactants

8.	Additives: None

9.	Solubility in Water: Miscible in oil and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	ND

Copper	ND

Lead	ND

Mercury	<0.1

Nickel	ND

Zinc	ND

Cyanide	2.8

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

206

RAPIDGRAB 2000™


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LISTING CHANGES PENDING;

VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN #M-25

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 9, 2006

"OIL SOLUTIONS POWDER"

(aka, AQUA N-CAP™ POLYMER)

I.	NAME, BRAND, OR TRADEMARK
OIL SOLUTIONS POWDER

(aka, AQUA N-CAP™ POLYMER)

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Oil Solutions International

35 Mill Street

Amityville, NY 11701

Phone: (631)608-8889

Fax: (631)789-1676

E-mail: 4oilgreen@gmail.com

Website: www.cleaningupoil.com

(Mr. Dennis J. Traina, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Oil Solutions International

35 Mill Street

Amityville, NY 11701

Phone: (631)608-8889

Fax: (631)789-1676

E-mail: 4oilgreen@gmail.com

Website: www.cleaningupoil.com

(Mr. Dennis J. Traina, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Work in a well-ventilated area. Avoid excessive inhalation of dust.

3.	Skin and eye contact; protective covering; treatment in case of contact: Skin contact - No
recommendation is made specifying the need for personal protective clothing to prevent skin
contact. Person(s) should wash daily at the end of each work shift. Exposed areas should be
thoroughly washed with water. Eye contact - Product may cause irritation as any normal dust.
Wear appropriate eye protection, compliant with ANSI Standard Z87.1, to prevent eye contact.
If eye irritation or redness is experienced, promptly wash eyes with large amounts of water, for at
least 15 minutes, occasionally lifting the lower and upper lids. Should eye irritation persist, seek

Miscellaneous Oil Spill Control Agents

207

OIL SOLUTIONS POWDER


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medical attention immediately. Contact lenses should not be worn when working with this
product. Inhalation - Wear appropriate respiratory protection, compliant with OSHA standard 29
CFR 1910.134, to prevent inhalation. If a respiratory disorder is observed, remove person(s)
from the work area immediately. Should respiratory disorder persist, seek medical attention
immediately. Ingestion - Rinse mouth with water and seek medical attention immediately.
4.a. Maximum storage temperature: 185°F
4.b. Minimum storage temperature: NA
4.c. Optimum storage temperature range: 185°F

4.d. Temperatures of phase separations and chemical changes: None. Polymer may accumulate
static charge during transport, handling, and processing. Static charge can be a potential fire
hazard in the presence of volatile or flammable materials or in high airborne dust conditions.

V.	SHELF LIFE
Not limited.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply OIL SOLUTIONS POWDER along the outer edges of spill area
to prevent spill migration. Proceed by applying product onto remaining spill area, until a light
white excess of product is observed. OIL SOLUTIONS POWDER may be broadcast onto the
spill by hand or with a mechanical blower. Lighter hydrocarbons and synthetic oils will clump
into a soft cluster like material easily recoverable with a net or other means as appropriate.

2.	Concentration/Application Rate: Apply OIL SOLUTIONS POWDER at a rate of 0.5 to 2 lbs
per gallon of spilled hydrocarbon. Depending on the type of hydrocarbon and recovery
operations employed, more or less product may be used to achieve recoverable solid mat/residue.
Allow approximately 30-60 minutes of contact time, product will form an elastic or rubber-like
mat material. Mat like material may be removed whole or segmented as appropriate.

3.	Conditions for Use: OIL SOLUTIONS POWDER differs from traditional sorbents in that it
initially behaves like a synthetic sorbent, then as a solidifier as the molecular microencapsulating
process occurs. Once encapsulated, the spilled oil is captured within the polymer matrix. OIL
SOLUTIONS POWDER is designed to cleanup a wide variety of crude oil, refined hydrocarbon
products (i.e., fuels, oils, hydraulic fluids), and synthetic fluids spilled on water and surfaces.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (ppm)

OIL SOLUTIONS POWDER

Menidia beryllina

484,000

96-hr



Mysidopsis bahia

104,000

48-hr

No. 2 Fuel Oil

Menidia beryllina

15.80

96-hr



Mysidopsis bahia

1.45

48-hr

OIL SOLUTIONS POWDER &

Menidia beryllina

22.50

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.13

48-hr

Reference Toxicant (SRTT)

Menidia beryllina

3.65

96-hr



Mysidopsis bahia

9.55

48-hr

Miscellaneous Oil Spill Control Agents 208

OIL SOLUTIONS POWDER


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b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: 230°F

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 0.91

5.	pH: 4.08

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: None

9.	Solubility in Water: Negligible

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.0

Cadmium	<0.05

Chromium	<0.325

Copper	17.25

Lead	<0.08

Mercury	0.02

Nickel	<0.225

Zinc	<0.45

Cyanide	<0.1

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

209

OIL SOLUTIONS POWDER


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

7/23/2021
7/27/2022

TECHNICAL PRODUCT BULLETIN #M-26

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 30, 2008

"ELASTOL"

(aka, SEPARATE, LIQUID ELASTOL)

I.	NAME, BRAND, OR TRADEMARK
ELASTOL

(aka, SEPARATE, LIQUID ELASTOL)

Type of Product: Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Action Additives, Inc.

205 Industrial Road

P.O. Box 965

Ducktown, TN 37326

Phone: updated information required

(Mr. Tim Kaylor)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Design Engineering Systems Analysis

P.O. Box 293

Alexandria, VA 22313

Phone: (703)4613912

E-mail: escambos@actionadditivesinc.com

(Mr. Ernest T. Scambos)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Autoignition temperature for product is 392°F. Product is combustible in liquid
form and can form combustible mixtures and possibly explosive mixtures above the flash point.
Use water spray to cool fire exposed surfaces and to protect personnel. Isolate "fuel" supple
from fire. Use foam, dry chemical, or water spray to extinguish fire. Avoid spraying water
directly into storage containers due to danger of boil over. Product is volatile and gives off
invisible vapors. Either the liquid or vapor may settle in low areas or travel some distance along
the ground or surface to ignition source where they may ignite.

2.	Ventilation: Product is moderately volatile. Ensure proper ventilation. Avoid formation and
inhalation of spray mist and vapors. Do not wear contaminated clothing. Keep away from fire
and heated objects. Avoid formation of aerosols. Avoid squirting and use dosage pump when
transferring.

3.	Skin and eye contact; protective covering; treatment in case of contact: Protection depends on
use and condition of work environment. Ensure good personal hygiene, wash hands regularly

Miscellaneous Oil Spill Control Agents

210

ELASTOL


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with soap and water. Avoid contact with skin and eyes and inhalation of fumes/aerosols. All

new protective gear must be of CE standard. There must be an eye rinsing kit available at the

work place. Where there is danger of inhalation, use mask with brown filter. If the product is

sprayed and there is a risk of aerosol formation, use mask with combination filter A2-P2. When

used regularly, measuring routines for solvent measurement should be implemented. Level of

contamination should be kept as low as possible.

4.a. Maximum storage temperature: ~160°F

4.b. Minimum storage temperature: -100°F

4.c. Optimum storage temperature range: 40-70°F

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

At least 5 years when stored at temperatures below 150°F.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: ELASTOL can be applied to the surface of an oil/water separator tank or
added to a waste stream before it enters a separation tank. ELASTOL floats on water, dissolving
when it comes in contact with petroleum products (e.g., gasoline, diesel, jet fuel, fuel oil, crude,
etc.). It remains effective for long periods, but naturally degrades when exposed to the
atmosphere over longer periods. ELASTOL treated oil may increase the performance of
containment and recovery equipment:

•	Containment booms - may have higher current and tow speed capability

•	Mechanical skimming equipment - may be improved 2 to 10 times its normal recovery
rates

•	Drum skimmers - may recover little or no water with the oil

When applied early to a spill, ELASTOL may reduce emulsification and dispersion of oil. In
addition, it may reduce the penetration of oil into porous soils and sandy beaches.

2.	Concentration/Application Rate: ELASTOL can be used at very low concentrations from 100-
1,500 ppm (0.01% to 0.15%). The amount of ELASTOL to be used is dependent upon the
viscosity of the oil being removed. For example, one gallon of ELASTOL will remove:

•	13 gallons of gasoline

•	34 gallons of diesel

•	84 gallons of medium oil

•	150 gallons of heavy oil

3.	Conditions for Use: ELASTOL may be used on fresh or salt water (under warm or cold
temperatures). Prompt application may maximize effectiveness. The older the pollutants the
few light oil elements remain in the oil, which may reduce the effectiveness of recovery.

Miscellaneous Oil Spill Control Agents

211

ELASTOL


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

ELASTOL

No. 2 Fuel Oil

ELASTOL &

No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
1,333 96-hr

94
5.4

3.3
8.2
3.7

7.4
10.7

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 176°F

2.	Pour Point: -71°F

3.	Viscosity: 3.46 cSt @ 77°F

4.	Specific Gravity: 0.83@t 60°F

5.	pH: 6.8-7.0

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	ND

Copper	ND

Lead	ND

Mercury	ND

Nickel	ND

Zinc	1.4

Cyanide	ND

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

212

ELASTOL


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TECHNICAL PRODUCT BULLETIN #M-27

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 03, 2010

"OIL BOND®"

I.	NAME, BRAND, OR TRADEMARK
OIL BOND®

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Solidification Products International, Inc.

P.O. Box 35

524 Forrest Road

Northford, CT 06472

Phone: (203) 484-9494

Toll Free: (800) 758-3634

Fax:(203)484-9492

E-mail: dgannon@oilbarriers.com

(Ms. Donna Gannon)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Solidification Products International, Inc.

P.O. Box 35

524 Forrest Road

Northford, CT 06472

Phone: (203) 484-9494

Toll Free: (800) 758-3634

Fax:(203)484-9492

E-mail: dgannon@oilbarriers.com

(Ms. Donna Gannon)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Not classified as flammable, but will burn. Maintain a fire watch if OIL
BOND® is heated above 450°F.

2.	Ventilation: Normal ventilation is adequate. For confined space entry or lack of exhaust in a
contained area, avoid generating dust. Dust in excessive concentration can result in an explosive
mixture in air. Wear approved NIOSH respirator with particulate pre-filter for dust.

3.	Skin and eye contact; protective covering; treatment in case of contact: Product dust may be
mildly irritating to eyes and respiratory tract. Wear approved standard issue work clothes, gloves,
dust mask, and dust tight goggles as needed. In case of contact with eyes, flush with water. If
prolonged skin contact, wash with soap and water. For inhalation of dust, remove to fresh air.

4.a.	Maximum storage temperature: 180°F
4.b. Minimum storage temperature: None

Miscellaneous Oil Spill Control Agents

213

OIL BOND®


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4.c. Optimum storage temperature range: Ambient. Avoid elevated temperatures >200°F for
extended periods of time.

4.d. Temperatures of phase separations and chemical changes: >450°F chance of auto-
combustion. Avoid strong oxidizing agents.

V.	SHELF LIFE

5 years. Store OIL BOND® in cool, dry area away from direct sunlight to prolong shelf life.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: OIL BOND® will absorb and solidify hydrocarbon spills on freshwater
and saltwater or land applications. For small spills, OIL BOND® may be broadcast by hand, and
booms and pillows may be used to ring the spill. For large spills, OIL BOND® may be
distributed by equipment with an air or water stream. Ground all dispensing equipment if
deploying dry OIL BOND® at a high rate of speed to prevent static discharge. Introduce OIL
BOND® with dispensing water spray just before final discharge to allow mixing of OIL BOND®
with the water stream. Allow OIL BOND® contact time with the spilled fuel or hydrocarbon
waste for 10 minutes to 1 hour before collection to allow absorption and solidification. Lighter
fuels require less solidification time than heavier viscosity fuels such as No. 6 fuel oil or heavy
crude. OIL BOND® is non-toxic and biologically inactive, and will remain floating on the
surface of the water before and after solidification.

Collect solidified materials with a net or vacuum equipment from the surface of the water. For
land spills shovel, sweep, or vacuum solidified material. Place the solidified debris in approved,
labeled, and sealed containers as required by local, state, federal, international, or country-
specific regulations.

Depending on the inherent nature of the spilled liquid that was solidified, disposal options
include landfilling, incineration, waste to energy incineration, or use as a secondary fuel.

2.	Concentration/Application Rate: OIL BOND® should be applied at a rate of 15% to 30% by
weight to a spilled hydrocarbon liquid. Lighter viscosity hydrocarbon waste and oils require less
OIL BOND® than heavier fuels. Conditions for use on spills may be highly variable, degraded
product or extremely heavy viscosity fuels may require additional OIL BOND® to obtain
complete solidification.

3.	Conditions for Use: OIL BOND® may be used on any hydrocarbon waste, oil or fuel on
freshwater, saltwater, or land applications. During rough weather with high winds or seas a
conventional containment collection boom is recommended to corral the spill allowing easier
retrieval and contact time with OIL BOND®. Cold water temperatures may require longer
contact time to fully solidify a spill.

Miscellaneous Oil Spill Control Agents

214

OIL BOND®


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

OIL BOND®

No. 2 Fuel Oil

OIL BOND® &

No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
>10000 96-hr
>10000 48-hr

3.0

7.1
3.8
9.6
8.0
11.3

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: NA, solid product

3.	Viscosity: NA, solid product

4.	Specific Gravity: 0.21

5.	pH: 8.8

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: Pigment/Antioxidant

9.	Solubility in Water: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.6

Cadmium	<0.32

Chromium	<0.32

Copper	0.71

Lead	<0.32

Mercury	<0.07

Nickel	0.97

Zinc	0.32

Cyanide	<0.50

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

215

OIL BOND®


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TECHNICAL PRODUCT BULLETIN #M-28

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 17, 2010

"AQUAFLEX®"

I.	NAME, BRAND, OR TRADEMARK
AQUAFLEX® (OPEN-CELL ELASTOMERIC SORBENTS)

Type of Product: Miscellaneous Oil Spill Control Agent
(formerly OPFLEX®^

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
AquaFlex Holdings LLC

P.O. Box 355

West Hyannisport, MA 02672
Phone: (508) 345-6520
Fax: (508) 425-2990
E-mail: ssmith@aflx.com
Website: www.aqflx.com
(Mr. Scott Smith)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
AquaFlex Holdings LLC

P.O. Box 355

West Hyannisport, MA 02672
Phone: (508) 345-6520
Fax: (508) 425-2990
E-mail: ssmith@aflx.com
Website: www.aqflx.com
(Mr. Scott Smith)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements. No special handling is required.

3.	Skin and eye contact; protective covering; treatment in case of contact: No special equipment
or clothing required. If eye or skin irritation occurs, flush with plenty of fresh water.

4.a.	Maximum storage temperature: 120°F continuous
4.b. Minimum storage temperature: No minimum

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

Miscellaneous Oil Spill Control Agents

216

AQUAFLEX®


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V.	SHELF LIFE

Shelf life is unlimited when stored in plastic bags.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Example - AquaFlex foam is fabricated into 40 6-foot strips that are in mesh netting. These
booms can be connected end-to-end and positioned behind containment booms to absorb oil that
has breached the containment.

2.	Example - AquaFlex foam is fabricated into 1/4" x 16" x 18" pads that can be deployed by
placing on an oil patch to absorb the oil from the water surface.

3.	Example - AquaFlex foam can be cut into small cubes such as 1 cubes and contained in a net
or mesh tube to create a very high surface area absorbent boom.

4.	Example - AquaFlex foam can be fabricated into mega pads of 1/4" x 1 foot x 6 foot sections
to be connected on the back of a containment boom system to absorb oil which flows over the
boom, especially in marsh areas.

5.	Example - AquaFlex foam can be fabricated into multiple mops that are strung between
support posts at the shoreline to remove oil from the surf.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

AQUAFLEX®

No. 2 Fuel Oil

AQUAFLEX® &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
>35640 96-hr
8630 48-hr

3.35

2.24

5.49

1.67

12.19

10.53

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: NA, solid product

3.	Viscosity: NA, solid product

4.	Specific Gravity: 0.0415 g/mL

5.	pH: NA

6.	Surface Active Agents: NA

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

Miscellaneous Oil Spill Control Agents

217

AQUAFLEX®


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9. Solubility in Water: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.179 (brl)

Cadmium	<0.089 (brl)

Chromium	<0.268 (brl)

Copper	1.74

Lead	0.286

Mercury	<0.0031 (brl)

Nickel	<0.446 (brl)

Zinc	139

Cyanide	0.498

Chlorinated Hydrocarbons	<2.43 (brl)

Miscellaneous Oil Spill Control Agents

218

AQUAFLEX®


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TECHNICAL PRODUCT BULLETIN #M-29

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 17, 2010

"GELCO 200"

I.	NAME, BRAND, OR TRADEMARK
GELCO 200

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
UESS, Ltd.

Box 6088

Drayton Valley, AB, Canada
T7A 1R6

Phone: (780) 621-6870
E-mail: hugh.morrison@telus.net
(Mr. Hugh Morrison)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
UESS, Ltd.

Box 6088

Drayton Valley, AB, Canada
T7A 1R6

Phone: (780) 621-6870
E-mail: hugh.morrison@telus.net
(Mr. Hugh Morrison)

*Currently only one distributor, which serves as a point of contact.

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: >150°F

2.	Ventilation: Store in well-ventilated location. Where local exhaust ventilation is not practical
and odors are detected, use a negative pressure half face respirator with a cartridge designed to
protect against organic vapors and dust if also present, a particulate pre-filter should be used. For
high airborne dust concentrations, use a cartridge to be used against nuisance dust.

3.	Skin and eye contact; protective covering; treatment in case of contact: Use cloth gloves if
desired. Dust-tight mono-glasses and standard issue work-wear. In case of contact with eyes or
skin, flush with water.

4.a.	Maximum storage temperature: 200°F
4.b. Minimum storage temperature: None

4.c. Optimum storage temperature range: 40-90°F

4.d. Temperatures of phase separations and chemical changes: Begins to oxidize exothermically
at high temperatures (230°F).

4.e. Store in a cool, dry location. Away from direct sunlight or sources of intense heat.

Miscellaneous Oil Spill Control Agents

219

GELCO 200


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4.f. Maintain fire watch if material temperature reaches 536°F (280°C).

4.g. Product may accumulate static charge during processing, handling, and transport.
Earth/ground all equipment used in handling and applying this product.

4.h. Avoid contact with strong oxidizing agents.

4.i. Do not stack Flexible Intermediate Bulk Containers or palletized bags.

V.	SHELF LIFE

>10 years when stored in dry, cool area out of sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: For small scale spills on water (fresh or salt), GELCO 200 can be
broadcast directly onto the spill by hand or small hand held spreader from the outer edge back
into the middle of the spill. Agitation is not necessary for GELCO 200 to be effective. The
product can also be used and is available in booms, socks, and pillows.

For large spills on water (fresh or salt), GELCO 200 may be deployed with an air or water
stream directed at the leading edge of the spill. Dispensing equipment should be properly
grounded to prevent static electricity build-up if pumping GELCO 200 in dry form at high rates
of delivery. If used with a water carrying media, product will require agitation to keep product
suspended if there is a delay or travel time associated between batching and delivering product
upon spill.

GELCO 200 will remove oils and other hazardous hydrocarbon based materials from both salt
and fresh water. GELCO 200 encapsulates and solidifies the oil, and remains buoyant even after
total saturation. The solidified products can be removed from the water with hand vacs, vacuum
barges, commercial fishing nets, and conveyors. Solidified materials should be placed into
appropriate containers and disposed of in accordance with all applicable federal, state, and local
regulations.

Land Application

For spills on land, the product would be applied in the same manner. The product can also be
applied by sand-blasting equipment/hopper or pneumatic air seeders. Agitation is not necessary
in most scenarios. Some fine agitation may be necessary to remove contaminated materials from
native grasses and marsh areas.

Many factors are taken into consideration before determining the best method(s) of application.
They include weather, geography, access, land use, and habitat of affected spill area.

When removing contaminants from land, it should be a priority to minimize the volume of land
taken to preserve the integrity of the land and to minimize the volume of waste requiring
disposal.

To recover solidified oil or hazardous materials from spills on land, the solidified product can be
collected and removed efficiently and effectively using a variety of manual and mechanical

Miscellaneous Oil Spill Control Agents

220

GELCO 200


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means.

Manual methods include picking up by hand, using brooms, rakes, shovels, and squeegees to
remove and pick up solidified petroleum waste product.

Mechanical means include using hand held vacuums, portable vac units, vac-trucks, or
commercial shop vacs. Once the spilled product is solidified by GELCO 200, it will not leach.
GELCO 200 is extremely hydrophobic and will not take on water, which may help to keep the
volume of waste produced down, depending on the characterization of any non-solidified oil and
water remaining in the area treated. Pressure flushing the solidified product or raw into a
containment area where it can be solidified - a boomed area, containment dike, bell hole, etc. for
removal by vacuum - is also a very practical method for removal.

Land spill cleanup of solidified oil/product

Collection and disposal of materials generated from application to oil spilled on land involve
greater variation in waste composition, and appropriate disposal techniques have to be selected
for the particular circumstances. Proper precautions, including testing as necessary to identify the
characteristics of wastes generated from the application of GELCO 200, should be taken to
determine the safe and legally required means of recovering, handling, storing, transporting,
treating, recycling, or disposing of materials produced from the application of GELCO 200 to oil
spilled on land.

All materials should be placed into appropriate containers, characterized by knowledge or testing
as to waste type, and handled, stored, transported, treated, or disposed of in accordance with all
applicable federal, state, and local regulations. Professional advice should be obtained where
needed.

2.	Concentration/Application Rate: GELCO 200 is usually applied at a ratio of 5-20% of
GELCO 200 to waste by weight to solidify light, medium, and heavy hydrocarbons.

Solidification typically occurs 1-3 minutes for most oils. GELCO 200 has been used effectively
on heavier crudes including Bunker C within the application rates noted above.

3.	Conditions for Use: GECLO 200 is effective in all environments and under a broad range of
weather conditions. The product is most effective on water temperatures between 32°F and
120°F. Depending upon the age and/or viscosity of the material, varying amounts of GELCO
200 may be required to obtain complete solidification. The recovered solidified product can be
disposed of in landfills, incinerated, or disposed of in accordance with all applicable federal,
state, and local regulations. Some products can be recovered from the solidified mass through a
heat process that would allow the solidified product to release itself from the GELCO 200.

UESS, Ltd. has had TCLP tests completed on several occasions and have not had any field
instances of product being released in our methods of recovery and disposal to date due to
pressure related issues.

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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

GELCO 200

No. 2 Fuel Oil

GELCO 200 &

No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
>10000 96-hr

>1000

9.26

6.58

3.15

3.51

8.03

14.5

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >150°F

2.	Pour Point: NA, solid product

3.	Viscosity: NA, solid product

4.	Specific Gravity: 0.25 g/cm3 at 4°C

5.	pH: 4.75

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.577

Cadmium	<0.289

Chromium	<0.577

Copper	<0.577

Lead	<0.577

Mercury	<0.100

Nickel	5.91

Zinc	0.788

Cyanide	ND

Chlorinated Hydrocarbons	ND

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GELCO 200


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LAST COMMUNICATION WITH MANUFACTURER:

1/10/2017

LAST ATTEMPT:	7/27/2022

TECHNICAL PRODUCT BULLETIN #M-30

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 26, 2012

"NORSOREX® APX"

I.	NAME, BRAND, OR TRADEMARK
NORSOREX® APX

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
D-NOV GmbH

Perfektastrasse 86
A-1230 Vienna
Austria, Europe

Office: updated information required
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Gerhard Karall, COO)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
D-NOV GmbH

Perfektastrasse 86
A-1230 Vienna
Austria, Europe
D-NOV GmbH
Perfektastrasse 86
A-1230 Vienna
Austria, Europe

Office: updated information required
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Gerhard Karall, COO)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: >174°F

2.	Ventilation: Dust explosions are possible while handling organic powders at high

Miscellaneous Oil Spill Control Agents

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NORSOREX® APX


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concentrations; therefore, provide proper air ventilation with fresh air or other methods to avoid
dust formation. General dust limits (DE-TRGS 900): 3 mg/m3 (respirable dust fraction), 10
mg/m3 (inhalable dust fraction), short-term exposure value (TRGS 900, 2.3) - excess factor 4.
For short-term exposure wear dust masks.

3.	Skin and eye contact; protective covering; treatment in case of contact: Avoid contact to skin
and eyes. Do not breathe dust. Wear protective goggles, gloves, and clothing. Following skin
contact, wash with plenty of water and pH-neutral soap. Obtain medical attention if irradiation
symptoms persist. Following eye contact, remove contact lenses immediately and rinse with
plenty of water (also under the eyelids) for at least 15 minutes. Obtain medical attention.
Following ingestion, remove all of product from the respiratory system and wash oral cavity.
Drink 200-300 ml of water. Do not induce vomiting without medical advice. Obtain medical
attention.

4.a.	Maximum storage temperature: 45°C/113°F
4.b. Minimum storage temperature: -5°C/23°F

4.c. Optimum storage temperature range: -5°C to 30°C/23°F to 86°F

4.d. Temperatures of phase separations and chemical changes: The material composition does
not change with the temperature (no phase separation). Chemical changes occur at temperatures
>45°C/113°F with oxygen. The material changes from white to yellow and the absorption
behavior decreases.

V.	SHELF LIFE

Shelf life is 3 years from date of production. Keep material stored in original containers in a
dark, dry area until use. The product should be used within 6 months after opening the original
container.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: NORSOREX® APX is a special polymer with very high affinity for
hydrocarbons and, since it is hydrophobic, it is also insoluble in water. NORSOREX® APX can
be used in free powder or pad form (sealed bags containing the powder). NORSOREX® APX
powder can bond to a variety of liquid hydrocarbons in two stages. First, due to the fast
absorption process further oil spreading is prevented (forming of a gel). Second, the oil solidifies
to a non-leaching inert, firm cohesive "rubber-like" mass within a few hours, which can be easily
collected and burned, disposed of or used for other purposes (e.g., rubber industry in a full green
recycle process). It is a combination of an adsorption and absorption process.

Use NORSOREX® APX powder or pads by estimating the hydrocarbon quantity and checking
with the application chart to individuate the necessary quantity. The suggestion to optimize the
usage is to keep ratio values of NORSOREX® APX to hydrocarbon as close as possible to the
application chart. If possible, use pretests to test the process. Deploy NORSOREX® APX in the
environment where there is hydrocarbon to be removed or recovered. NORSOREX® APX can be
applied by hand or through mechanical spreading. According to the desired performance, wait
the necessary reaction time. Reaction takes place within minutes and it reaches 80 percent of its
efficiency after only a few hours. Maximum efficiency (100 percent) can be reached in less than
24 hours. Once NORSOREX® APX has reacted, it is possible to recover the hydrocarbon in solid

Miscellaneous Oil Spill Control Agents

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NORSOREX® APX


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form.

2. Concentration/Application Rate:

Type of Hydrocarbon (HC)

kgHc/kgAP

X

kgAPx/kgH
c

kgAPx/m3H
c

Lhc/Lap

X

Lapx/Lh
c

Benzene

23.0

0.043

38.1

9.189

0.109

Toluene

18.0

0.056

48.2

7.267

0.138

Hexane

4.2

0.238

155.9

2.245

0.445

Heptane

5.0

0.200

135.9

2.575

0.388

Cyclorhexane

6.8

0.147

114.6

3.055

0.327

Di chl orom ethane/Methyl ene
chloride

18.0

0.056

73.9

4.737

0.211

Chloroform

26.0

0.038

57.0

6.136

0.163

T ri chl oroethane/T ri chl oroethy 1 en
e

31.8

0.031

45.9

7.623

0.131

Tetrachl oroethene/Tri chl oroethy 1
ene

31.0

0.032

52.3

6.689

0.149

1,2-Dichlorobenze

27.4

0.036

47.4

7.377

0.136

Pyralene 60 (60% PCB/40%TCB)

36.4

0.027

39.3

8.909

0.112

Pyralene 78 (78% PCB/22%
TCB)

28.8

0.035

52.4

6.675

0.150

Diethyl glycol

2.7

0.370

3.11.1

1.125

0.889

Diocytlphthalate

2.8

0.357

353.9

0.990

1.010

Heavy Crude Oil A

12.0

0.083

75.0

4.667

0.214

Heavy Crude Oil B

9.0

0.111

88.9

3.938

0.254

Light Crude Oil

9.5

0.105

88.4

3.958

0.253

Kerosene

10.2

0.098

79.4

4.407

0.227

Diesel

10.0

0.100

82.3

4.253

0.235

Aromatic Process Oils

8.3

0.120

120.5

2.905

0.344

Naphthenic Process Oils

8.3

0.120

108.4

3.228

0.310

Paraffinic Process Oils

4.0

0.250

217.5

1.609

0.621

Refrigerator Oils

10.7

0.093

81.3

4.305

0.232

Turbine Oils

4.3

0.233

209.3

1.672

0.598

Machine Oils

4.5

0.222

200.0

1.750

0.571

Motor Oils

3.8

0.263

228.9

1.529

0.654

Vegetable Oils

2.7

0.370

337.0

1.038

0.963

HC - Hydrocarbon
APX - NORSOREX® APX
kgxx - Kilogram of xx
M3xx - Cubic meters of xx
Lxx - Liter of xx

kgAPX./m3HC - Kilograms of NORSOREX® APX per cubic

Bulk density of NORSOREX®
APX powder: 0.35 g/cm3
The results are tested at room
temperature (23°C/73°F) and
most substrates show an
improvement of 10 until 15% at

Miscellaneous Oil Spill Control Agents

225

NORSOREX® APX


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Type of Hydrocarbon (HC)

kgHc/kgAP

X

kgAPx/kgH
c

kgAPx/m3H
c

Lhc/Lap

X

Lapx/Lh
c

meter of hydrocarbon

40°C. The best performance is
achieved at 60°C with an
improvement of about 30%. At
higher temperatures the effect of
improvement falls and over
100°C significant.

3. Conditions for Use:

To recover the solidified NORSOREX® APX from the environment, mechanically collect the
material and transport it to the nearest designated disposal location. NORSOREX® APX has the
capability of 3.5 bar of pressure before it will start leaking. Do not discharge into drains, surface
waters, or ground waters. NORSOREX® APX is not biodegradable. The resulting "rubber-like"
material could still be hazardous so extreme caution should be exercised when handling these
materials. Very polar substances such as organic acids, alcohols or glycols show a reduced
absorption efficiency of the product. The water temperature has an influence on the reaction
time. Cold water slows down the solidification process. The ages of pollutants only have an
influence on the absorption performance if their viscosity or polarity are increased to the typical
values for the "fresh" pollutant.

Avoid damage to NORSOREX® APX pads if the application environment is characterized by
rough water. This will ensure the easiest deployment and recovery procedure. If allowed by
current regulations and if properly contained, the free powder form is recommended to optimize
the contact interface between NORSOREX® APX and the liquid hydrocarbon.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

NORSOREX® APX
No. 2 Fuel Oil

NORSOREX® APX & No. 2
Fuel Oil (1:10)

Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
>100,000.00 96-hr
>100,000.00 48-hr
15.10 96-hr
2.41 48-hr
39.80 96-hr
3.06 48-hr
2.01 96-hr
6.63 48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

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NORSOREX® APX


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IX. PHYSICAL PROPERTIES

1.	Flash Point: 174°F

2.	Pour Point: NA

3.	Viscosity: NA

4.	Specific Gravity: 0.91047 at 60°F

5.	pH: 7.10

6.	Surface Active Agents: Polynorbornene

7.	Solvents: NA

8.	Additives: Phenolic antioxidant, flow agent

9.	Solubility in Water: Insoluble in water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.40

Copper	0.14

Lead	ND

Mercury	0.011

Nickel	ND

Zinc	55.40

Cyanide	0.222

Chlorinated Hydrocarbons	ND

Miscellaneous Oil Spill Control Agents

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NORSOREX® APX


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #M-31
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: NOVEMBER 9, 2015
"CAS 100®"

I.	NAME, BRAND, OR TRADEMARK
CAS 100®

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Tradewinds Environmental Safety Services SA de CV

Calle 1 "E" No. 245 por 30 y 36
Col. Campestre
Merida, Mexico C.P 97120
Phone: updated information required
E-mail: updated information required
(Mr. Michael Harper)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
EPC Evolved Products, Inc.

5889 Greenwood Plaza Boulevard, Suite 201
Greenwood Village, CO 80111
Phone: 720-496-0023
E-mail: dave.washington@epces.com
(Mr. Dave Washington)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable

2.	Ventilation: Work in well ventilated area. Avoid excessive inhalation of fine particles.

3.	Skin and eye contact; protective covering; treatment in case of contact: Avoid contact to eyes.
Do not breathe in particles. Wear protective goggles, gloves and clothing. Following skin
contact, wash with plenty of soap and water. Remove exposed or contaminated clothing, taking
care not to contaminate the eyes. Please seek medical attention if adverse effects continue after
flushing. Following eye contact, remove contact lenses (if necessary) and rinse with gently
running water for at least 15 minutes. Obtain medical attention. Following ingestion, call
physician or poison control center for most current information. If professional advice is not
available, do not induce vomiting. Drink large quantities of water. Following inhalation, move to
fresh air location. Seek medical attention if adverse symptoms continue after removal to fresh
air.

4.a.	Maximum storage temperature: 140°F

3/10/2016
7/27/2022

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CAS 100®


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4.b. Minimum storage temperature: -40°F

4.c. Optimum storage temperature range: -40°F to 140°F

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

The shelf life of CAS 100® is 1 year from date of production if stored in a dry dark location.

Keep material stored in original containers in a dark, dry area until use. If the product is exposed
to UV rays consistently, it will degrade over time.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: In powder form, apply CAS 100® along the outer edges of spill area to
prevent migration. Continue to apply CAS 100® inside spill area until the area is saturated with
product. Depending on type of hydrocarbon, the resulting oil/CAS 100® mixture can be rolled up
like a carpet or clumps of the solid can be removed with a net. In pad form, booms can be used to
prevent migration of oil spill. Pads can be used to clean up the spill area by placing them on the
oil spill itself. Once the pad is saturated, it can be easily removed by simply picking up the pad.

2.	Concentration/Application Rate: CAS 100® is used by applying 1 pound of product to each 10
pounds of spilled hydrocarbon. The contact time varies from just a few seconds to several hours
depending upon the quantity of the spill. Hydrocarbon viscosities decrease as temperatures
increase causing an increase in the time required for the gelling process of hydrocarbon to CAS
100®.

3.	Conditions for Use: CAS 100® can be used on any concentration of water salinity and water
temperature. There is no restriction of the types of ages of the hydrocarbon being processed.
Depending upon the types of the hydrocarbon, the resulting CAS 100®/oil mixture can be in the
form of a carpet, rubber ball or crumb like material. CAS 100® has a fast gelling characteristic,
which prevents the hydrocarbon from spreading further. Once the hydrocarbon comes in contact
with CAS 100®, the result is a non-leaching solid within a few minutes (or hours) depending on
the size of the spill. The resulting solid should be collected at the spill site and disposed of
according to federal, state and local regulations. Collecting the solid at the spill site will prevent
the resulting CAS 100®/oil mixture from reaching open water.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity
Material Tested
CAS 100®

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
>1000 96-hr
>1000 48-hr
4.81 96-hr

1.93	48-hr

5.94	96-hr
1.41 48-hr
8.84 96-hr
23.00 48-hr

No. 2 Fuel Oil

CAS 100® & No. 2 Fuel Oil Menidia beryllina

(1:10)

Reference Toxicant (SDS)

Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

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229

CAS 100®


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b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS

NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: NA (solid material)

3.	Viscosity: NA (solid material)

4.	Specific Gravity: 0.51

5.	pH: 6.94

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: NA

9.	Solubility in Water: Insoluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<2.0

Cadmium	<0.5

Chromium	<1.0

Copper	<2.5

Lead	<2.0

Mercury	<0.029

Nickel	<4.0

Zinc	<5.0

Cyanide	<0.22

Chlorinated Hydrocarbons	ND

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CAS 100®


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TECHNICAL PRODUCT BULLETIN #M-32

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 21, 2016

"S-200 OILGONE®"

I.	NAME, BRAND, OR TRADEMARK
S-200 OILGONE®

Type of Product: Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
RBL Environmental, LLC*

1311 Dorothy Avenue
Phoenixville, PA 19460
Phone: (610) 520-7665
E-mail: iim.lynn@iepusa.com
(Mr. James Lynn)

(*RBL Environmental, LLC is the manufacturer and marketer for International Environmental
Products)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
RBL Environmental, LLC

1311 Dorothy Avenue
Phoenixville, PA 19460
Phone: (610) 520-7665
E-mail: iim.lynn@iepusa.com
(Mr. James Lynn)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable

2.	Ventilation: Ensure good ventilation. This can be achieved by local suction and or general air
extraction. If this is insufficient to maintain the concentration under Workplace Exposure Limits
(WEL), suitable breathing protection should be worn. Applies only if maximum permissible
exposure values are listed below. Respiration protection normally not necessary. If Occupational
Exposure Standards (OES) or Maximum Exposure Limits (MELs) are exceeded, use appropriate
air purifying respirator with filter.

EXPOSURE CONTROL/PERSONAL PROTECTION
Exposure limit values: Not applicable
Name	WEL-TWA	WEL-STEL	Content

2-(2-butoxyethoxy)-ethanol	10 ppm	15 ppm	1-5%

Butyl carbitol®	(67.5 mg/m3)	(101.2 mg/m3)

(WEL, EC)	(WEL, EC)

WEL-TWA: Workplace Exposure Limit-Time-Weighted Average; WEL-STEL: Workplace Exposure Limit-Short-Term
Exposure Limit; EC: European Commission

3.	Skin and eye contact; protective covering; treatment in case of contact: General hygiene

Miscellaneous Oil Spill Control Agents

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S-200 OILGONE®


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measures for the handling of chemicals are applicable. Wash hands before breaks and at end of
shift. Keep away from food, drink and animal feeding supplies. Skin Protection: wear protective
work garments (e.g., safety shoes, long-sleeves). Wear chemical resistant protective gloves; or if
applicable, gloves made of protective neoprene or butyl rubber. Protective hand cream is
recommended. Eye Protection: wear tight fitting protective goggles with side protection.
4.a. Maximum storage temperature: 132°F
4.b. Minimum storage temperature: 32°F
4.c. Optimum storage temperature range: 55°F to 85°F

4.d. Temperatures of phase separations and chemical changes: <0°F and >212°F. Phase
separation will be eliminated when returning to ambient temperatures.

V. SHELF LIFE

Recommended shelf life is 10 years if product is kept in the unopened, original container.

VI. RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: S-200 OILGONE® is a water like liquid and can be sprayed with
traditional liquid spraying equipment, such as pressurized sprayers or backpack sprayers. Apply
product directly to the hydrocarbon.

2.	Concentration/Application Rate: The recommended application rate for spraying on the spill is
approximately 1:1 by weight of the product as compared to the hydrocarbon being agglomerated.
For example, use 1 gallon of product for every 1 gallon of hydrocarbon to be treated. For sheens,
apply 1 gallon of product for every 8 square yards of surface area.

3.	Conditions for Use: S-200 OILGONE® is a hydrocarbon coagulator used for the cleanup of
hydrocarbon spills on water. These hydrocarbons include, but are not limited to, gasoline, No. 2
to No. 6 Fuel Oil, jet fuels, kerosene, lubricating oils, hydraulic oils and crude oils. Once applied,
the hydrocarbon will agglomerate with S-200 OILGONE® and remain on the water's surface. To
prevent the hydrocarbon or agglomeration from reaching open water during application, use
traditional booms to contain the spill. The agglomeration will form gel like balls, eliminating the
sheen and allowing for the product:oil mixture to be removed from the water's surface using
traditional skimming tools. The resulting gel like balls should be collected at the spill site and
disposed of according to federal, state and local regulations. S-200 OILGONE® can be used in
salt, brackish or fresh water. The product can be applied at any ambient temperature on any
hydrocarbon pollutant whether fresh or weathered. The size of the gel balls will be dependent on
the quantity (not type) of hydrocarbon spilled.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested
S-200 OILGONE®

No. 2 Fuel Oil

S-200 OILGONE® & No. 2
Fuel Oil (1:10)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
326.22 96-hr
47.29 48-hr
21.11 96-hr
2.56 48-hr
15.83 96-hr
2.46 48-hr

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S-200 OILGONE®


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LC50 (ppm)
3.47 96-hr
4.91 48-hr

b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Material Tested	Species

Reference Toxicant (SDS) Menidia beryllina

Mysidopsis bahia

IX. PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 29 °F

3.	Viscosity: 6.9 cst@40°C

4.	Specific Gravity: 0.9796

5.	pH: 7.01

6.	Surface Active Agents: Confidential

7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility in Water: Miscible

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.5

Cadmium	<0.25

Chromium	<0.25

Copper	<0.5

Lead	<0.6

Mercury	<0.0025

Nickel	<0.5

Zinc	0.54

Cyanide	<0.025

Chlorinated Hydrocarbons	<0.1

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S-200


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TECHNICAL PRODUCT BULLETIN #M-33

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 22, 2016

"HYDRO-BOND™"

I.	NAME, BRAND, OR TRADEMARK
HYDRO-BOND™

Type of Product: Miscellaneous Oil Spill Control Agent - Solidifier

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Oil Spill Solutions, LLC

153 Foster Street

Center, TX 75935

Phone: (936) 598-6595

Fax: (936) 598-6338

E-mail: fred@,fredwulf.com

Website: www.oilspillsolutionsllc.com

(Mr. Fred Wulf)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Oil Spill Solutions, LLC

153 Foster Street

Center, TX 75935

Phone: (936) 598-6595

Fax: (936) 598-6338

E-mail: fred@,fredwulf.com

Website: www.oilspillsolutionsllc.com

(Mr. Fred Wulf)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable (DOT: Non-Hazardous)

2.	Ventilation: Personal protective equipment should be used when applying Hydro-Bond™.
Recommended equipment would include safety glasses or goggles, disposable respirators,
nuisance dust mask or procedural mask, disposable gloves and long sleeves. Odors/vapors may
produce mild and temporary discomfort to the respiratory tract resulting in wheezing, tightness in
the chest, shortness of breath and coughing. Although they may be present in low amounts, dust
and small pieces of material may aggravate bronchitis, asthma, and emphysema if inhaled.

3.	Skin and eye contact; protective covering; treatment in case of contact: Hydro-Bond™ in
contact with the skin may result in irritation (redness, itching) or other effects with some
individuals. In case of skin contact wash exposed skin thoroughly with soap and water. As some
are sensitive or allergic to natural rubber (Latex), if irritation develops and is prolonged and/or
sore, consult a physician. Hydro-Bond™ material is abrasive if it enters the eye, which can cause
irritation to sever damage if left untreated. In case of eye contact flush eyes with plenty of water

Miscellaneous Oil Spill Control Agents

234

HYDRO-BOND™


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for at least 15 minutes. Avoid rubbing the eye. If experiencing prolonged irritation or soreness,
seek medical attention. In the event that Hydro-Bond™ is ingested there may be irritation of
mucus membranes of mouth, throat, esophagus and stomach along with nausea may occur.
Abrasion to the mouth, esophagus, stomach and intestinal tract may occur. If inhaled, in
emergency situations, use proper respiratory protection and immediately remove the affected
person from the exposure. Keep at rest. Administer artificial respiration if breathing has stopped.
Seek medical attention. If swallowed do not induce vomiting. Rinse mouth well with water.
Never give anything by mouth to an unconscious person. Seek medical attention. Repeated
unprotected exposure to Hydro-Bond™ may result in sensitization to susceptible individuals.
General advice: If negative symptoms develop while handling the product, move out of the area
to prevent further exposure. Consult a physician as a precautionary measure if symptoms develop
after being subjected to unprotected exposure of the material. If eye or skin irritation occurs flush
with plenty of fresh water.

4.a. Maximum storage temperature: 120°F continuous, 140°F up to 5 days

4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Unlimited in sealed poly drums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product is best used in contained systems such as barriers, socks, mats,
blankets, etc. Containment systems should be fully deployed before the application of Hydro-
Bond™ to better facilitate rapid and complete recovery. For smaller spills a drum pump with
sprayer and large orifice may be used to apply the Hydro-Bond™ material, mixing with salt or
fresh water, depending on the spill being in salt or fresh water, as required depending on the type
and viscosity of oil being treated. Aged hydrocarbon pollutants will tend to be more concentrated
and more viscous; this may require additional quantities of Hydro-Bond™ to be applied. A
higher viscosity hydrocarbon spill will require higher concentrations of Hydro-Bond™ and
longer dwell times to ensure maximum absorption.

2.	Concentration/Application Rate: In contained spills, product may be applied directly to water-
borne spills on a 1:18 ratio by weight or a 1:1 ratio by volume. On heavy oils use Product
directly on the spill with a 1:1 ratio by volume of spilled contaminant.

3.	Conditions for Use: Effective in salt water or fresh water, with no limitation as to usage within
optimum temperature parameters (application may be made at or above 30°F). In applications
wherein the salinity of the water is higher in content, application of Hydro-Bond™ should be
targeted more accurately to the spill concentrations as the hydrocarbon pollutant will be
concentrated closer to the surface and effort should be made to ensure that the exposed pollutant
is covered to the greatest extent possible. After treatment with Hydro-Bond™, residue should be
collected by means of surface skimmers, vacuum pumps, skimming booms, etc. and removed
from the site. The specific collection process and methodologies should be determined by on-site
coordinator based on practices of the area and available equipment. Collected residue should be
disposed of in accordance with local, state, and federal regulations.

Miscellaneous Oil Spill Control Agents

235

HYDRO-BOND™


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (ppm)

HYDRO-BOND™

Menidia beryllina

6544.77 96-hr



Mysidopsis bahia

5000.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

41.81 96-hr



Mysidopsis bahia

5.88 48-hr

HYDRO-BOND™ & No. 2

Menidia beryllina

19.93 96-hr

Fuel Oil (1:10)

Mysidopsis bahia

1.93 48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.52 96-hr



Mysidopsis bahia

5.47 48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: N/A

3.	Viscosity: N/A

4.	Specific Gravity: 0.9524 @60°F

5.	pH: N/A

6.	Surface Active Agents: N/A

7.	Solvents: N/A

8.	Additives: None

9.	Solubility in Water: Not soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<2.0

Cadmium	<1.0

Chromium	6.07

Copper	69.0

Lead	53.5

Mercury	<0.020

Nickel	2.16

Zinc	4140

Cyanide	<0.118

Chlorinated Hydrocarbons	<80 (ug)

Miscellaneous Oil Spill Control Agents

236

HYDRO-BOND™


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TECHNICAL PRODUCT BULLETIN #M-34

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: APRIL 16, 2021

"AQUAPAL®"

I.	NAME, BRAND, OR TRADEMARK

AQUAPAL® (OPEN-CELL POLYOLEFIN FOAM SORBENT)

Type of Product: Miscellaneous Oil Spill Control Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Palziv North America

7966 NC 56 Highway
Louisburg, NC 27549
Phone: (508) 345-6520
Fax: (919) 496-2523
E-mail: ssmith@aqflx.com
Website: www.palzivna.com
(Mr. Scott Smith)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Palziv North America

7966 NC 56 Highway
Louisburg, NC 27549
Phone: (919) 497-0010
Fax: (919) 496-2523
E-mail: tlehnartz@palzivna.com
Website: www.palzivna.com
(Mr. Tom Lehnartz)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous).

2.	Ventilation: No special requirements. No special handling is required.

3.	Skin and eye contact; protective covering; treatment in case of contact: No special equipment
or clothing required; however, at all times, from deployment to reuse to disposal of AquaPal®, it
is recommended that deployment personnel wear appropriate personal protective equipment
including, but not limited to, impervious gloves, goggles, face masks/shields (as necessary that
be dependent upon local air quality testing), and Tyvek suits. If eye or skin irritation occurs,
flush with plenty of fresh water. Depending upon the type of spill and specific oil spilled, there
may be supplemental safety requirement at the spill site. It is strongly recommended that
deployment personnel follow all health and safety recommendations established for the spill site.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days.

4.b. Minimum storage temperature: No minimum

4.c. Optimum storage temperature range: 40°F to 120°F

Surface Collecting Agents

237

Surface Collecting Agents


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4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Shelf life is unlimited when stored in plastic bags.

VI.	RECOMMENDED APPLICATION PROCEDURE
Mechanism of Action:

AquaPal® is an open-cell foam manufactured in continuous rolls from polymers that are naturally
oleophilic (and thus water repellant/hydrophobic). AquaPal® is deployed in roll form and/or
fabricated into various configurations (e.g., eelgrass, pads, netted booms). When placed in an
environment of oil and water, AquaPal® attracts oil and repels water. The open-cell structure
provides capillaries for the oil to fill, and oil travels into the foam structure by capillary action.
AquaPal® should be removed from the spill environment when the products are saturated with
oil; and the oil should be disposed of according to federal, state, and local regulations.

The following are examples of various product configurations of AquaPal®:

•	Example - AquaPal® foam rolls with thickness of 1/4 - 3/8 inches, widths of 20 to 60 inches,
and lengths of 2 - 100 feet can be deployed directly on an oil patch/slick to absorb the oil
from the water surface.

•	Example - AquaPal® foam is fabricated into 10-foot strips to make round, netted booms.
These booms can be connected end-to-end and positioned in front and/or behind containment
booms to absorb oil that has breached the containment.

•	Example - AquaPal® foam is fabricated into 3/8-inch-thick x 1/2-inch-wide x 6-inch-long
pads that can be deployed by placing on an oil patch to absorb the oil from the water surface.

•	Example - AquaPal® foam can be cut into small strips such as 3/8-inch-thick x 1/2-inch-wide
x 6 inches long and contained in a net or mesh bag to create a high surface area oil absorbent
filter bag.

•	Example - AquaPal® foam can be fabricated into eelgrass configurations of 5-foot sections
with a rope and carabiner clips at each end with eelgrass blades of 3/8-inch-thick x 3/4-
inches wide x 18 inches long to be connected on the back of a containment boom systems to
absorb oil which flows over or under the boom, especially in marsh areas and other sensitive
ecosystems.

Surface Collecting Agents

238

Surface Collecting Agents


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

AQUAPAL®

No. 2 Fuel Oil

AQUAPAL® &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

3134.10	96-hr

>17040.00	48-hr

18.84	96-hr

3.40	48-hr

17.76	96-hr

3.56	48-hr

3.56	96-hr

7.02	48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >212°F

2.	Pour Point: NA, solid product

3.	Viscosity: NA, solid product

4.	Specific Gravity (ASTM D-792): 0.386 g/mL

5.	pH: NA

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Not soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<3.86 (mg/L)

Cadmium	<0.725 (mg/L)

Chromium	<1.70 (mg/L)
Copper 1.90 (mg/L)

Lead	<1.21 (mg/L)

Mercury	<0.0036 (mg/L)
Nickel 0.954 (mg/L)

Zinc	16.3 (mg/L)
Cyanide 0.02 (mg/L)

Chlorinated Hydrocarbons	<5.00 (mg/L)

Surface Collecting Agents

239

Surface Collecting Agents


-------
SURFACE COLLECTING AGENTS:
TECHNICAL NOTEBOOK BULLETINS

Surface Collecting Agents

240

Surface Collecting Agents


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/14/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #S-5

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 29, 2012

"THICKSLICK 6535"

I.	NAME, BRAND, OR TRADEMARK
THICKSLICK 6535

Type of Product: Surface Collecting Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Desmi, Inc.

1119 Cavalier Boulevard
Chesapeake, VA 23323
Phone: updated information required
E-mail: pla@desmi.com
Website: http ://www.desmi.com
(Mr. Peter Lane)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Desmi, Inc.

1119 Cavalier Boulevard
Chesapeake, VA 23323
Phone: updated information required
Phone: (716) 662-0632
E-mail: pla@desmi.com
Website: http://www.desmi.com
(Mr. Peter Lane)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-Flammable; DOT - Non-Hazardous

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in a moderate breeze

3.	Skin and eye contact; protective covering; treatment in case of contact: May produce eye
irritation in some persons and produce eye damage 24 hours or more after instillation. May cause
skin irritation after prolonged or repeated exposure. Avoid skin and clothing contact. If skin
contact occurs, immediately wash with large amounts of soap and water (if possible). Remove
any contaminated clothing and shoes. Launder before reusing. If irritation persists, seek medical
assistance. For areas where contact is likely, wear long sleeve shirt, chemical resistant gloves,
and chemical resistant goggles.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: -40°F

4.c. Optimum storage temperature range: 59°F to 77°F

Surface Collecting Agents

241

THICKSLICK 6535


-------
4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

Minimum of three years in unopened container.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray on water around the perimeter of an oil slick using a pressurized
backpack sprayer or aerial applicator.

2.	Concentration/Application Rate: 6.4 U.S. gallons/mile (or 15L/km).

3.	Conditions for Use: THICKSLICK 6535 is designed to aid in situ burning of free oil in calm
water with drift ice where fire boom would be ineffective. When sprayed on the water around the
perimeter of an oil slick, THICKSLICK 6535 will concentrate the oil to a thickness suitable for
igniting a burn. It works in all water temperatures and salinities and works best with fluid
petroleum that has not weathered significantly.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

THICKSLICK 6535
No. 2 Fuel Oil

THICKSLICK 6535 & No. 2
Fuel Oil (1:10)

Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
138 96-hr
286 48-hr
37.6 96-hr
2.43 48-hr
5.91 96-hr
1.53 48-hr
3.02 96-hr
8.23 48-hr

b. Effectiveness:
NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >180°F

2.	Pour Point: 21.2 °F

3.	Viscosity: 118 SUS at 100 °F

4.	Specific Gravity: 0.9745 at 60°F

5.	pH: 6.45

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: None

9.	Solubility in Water: Partly miscible

Surface Collecting Agents

242

THICKSLICK 6535


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X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE, AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Surface Collecting Agents

243

THICKSLICK 6535


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/14/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #S-6

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 29, 2012

"SILTECH OP-40"

I.	NAME, BRAND, OR TRADEMARK
SILTECH OP-40

Type of Product: Surface Collecting Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Desmi, Inc.

1119 Cavalier Boulevard
Chesapeake, VA 23323
Phone: updated information required
E-mail: pla@desmi.com
Website: http ://www.desmi.com
(Mr. Peter Lane)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Desmi, Inc.

1119 Cavalier Boulevard
Chesapeake, VA 23323
Phone: updated information required
E-mail: pla@desmi.com
Website: http://www.desmi.com
(Mr. Peter Lane)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-Flammable; DOT - Non-Hazardous

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in a moderate breeze

3.	Skin and eye contact; protective covering; treatment in case of contact: May produce eye
irritation in some persons and produce eye damage 24 hours or more after instillation. May cause
skin irritation after prolonged or repeated exposure. Avoid skin and clothing contact. If skin
contact occurs, immediately wash with large amounts of soap and water (if possible). Remove
any contaminated clothing and shoes. Launder before reusing. If irritation persists, seek medical
assistance. For areas where contact is likely, wear long sleeve shirt, chemical resistant gloves,
and chemical resistant goggles.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: -40°F

4.c. Optimum storage temperature range: 59°F to 77°F

4.d. Temperatures of phase separations and chemical changes: None

Surface Collecting Agents

244

SILTECH OP-40


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V. SHELF LIFE

Minimum of three years in unopened container.

VI. RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray on water around the perimeter of an oil slick using a pressurized
backpack sprayer or aerial applicator.

2.	Concentration/Application Rate: 6.4 U.S. gallons/mile (or 15L/km).

3.	Conditions for Use: SILTECH OP-40 is designed to aid in situ burning of free oil in calm
water with drift ice where fire boom would be ineffective. When sprayed on the water around the
perimeter of an oil slick, SILTECH OP-40 will concentrate the oil to a thickness suitable for
igniting a burn. It works in all water temperatures and salinities and works best with fluid
petroleum that has not weathered significantly.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

SILTECH OP-40

No. 2 Fuel Oil

SILTECH OP-40 & No. 2
Fuel Oil (1:10)

Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

3.33
6.83
40.50
6.43
9.70
3.27
2.33
8.68

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >180°F

2.	Pour Point: -74.2 °F

3.	Viscosity: 53 SUS at 100 °F

4.	Specific Gravity: 0.98816 at 60°F

5.	pH: 8.03

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: None

9.	Solubility in Water: Partly miscible

Surface Collecting Agents

245

SILTECH OP-40


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X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE, AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

ND

ND

ND

ND

ND

ND

ND

ND

ND

ND

Surface Collecting Agents

246

SILTECH OP-40


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SURFACE WASHING AGENTS:
TECHNICAL NOTEBOOK BULLETINS

Surface Washing Agents

247

Surface Washing Agents


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TECHNICAL PRODUCT BULLETIN #SW-2

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JANUARY 7, 1985

REVISED LISTING DATE: AUGUST 21, 1995

"TOPSALL #30"

(aka, SUPERALL #38)

I. NAME, BRAND, OR TRADEMARK
TOPSALL #30 (AKA, SUPERALL #38)

Type of Product: Surface Washing Agent (Oil and Petroleum Cleaning Agent)
(formerly #D-20)

II. NAME, ADDRESS, AND TELEPHONE

TOPSALL #30

Stutton North Corporation

P.O. Box 724

Mandeville, LA 70470

Phone: (985) 626-3900

Fax:(985)674-0476

(Mr. David Anton)

NUMBER OF MANUFACTURER/CONTACT
SUPERALL #38
Superall Products LLP
P.O. Box 2954
Spring, TX 77383
Phone: (281)351-4800
Fax: (281) 351-4855
E-mail: info@superall.com
Website: www.superall.com
(Mr. Sammy Roberts II)

III. NAME, ADDRESS, AND TELEPHONE

TOPSALL #30

Stutton North Corporation

P.O. Box 724

Mandeville, LA 70470

Phone: (985) 626-3900

Fax:(985) 674-0476

(Mr. David Anton)

NUMBER OF PRIMARY DISTRIBUTORS
SUPERALL #38
Superall Environmental LLC
P.O. Box 2954
Spring, TX 77383
Phone: (281)351-4800
Fax: (281) 351-4855
E-mail: info@superall.com
Website: www.superall.com
(Mr. Sammy Roberts II)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: TOPSALL #30 (aka, SUPERALL #38) is non-flammable.

2.	Ventilation: Normal type household ventilation is adequate for handling and storage.

3.	Skin and eye contact; protective clothing; treatment in case of contact:

In case of contact with eyes, wash thoroughly with large amounts of water. If irritation persists,
seek medical attention. Use protective gloves for manual cleaning.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 20°F

Surface Washing Agents

248

TOPSALL #30


-------
4.c. Optimum storage temperature range: 40°F to 100°F

4.d. Temperatures of phase separations and chemical changes: TOPSALL #30 (aka, SUPERALL
#38) has a pour point of 20°F and a boiling point of 212°F.

V.	SHELF LIFE

TOPSALL #30 (aka, SUPERALL #38) has a shelf life of not less than two years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: For general use, apply by spray, mop, etc. Agitate severe spots and rinse
thoroughly for a residue-free surface.

2.	Concentration/Application Rate: Normal cleaning (rigs and platforms, bilges, decks, waterline
scum, shop machinery and equipment) use 1 part TOPSALL #30 (aka, SUPERALL #38) to up to
20 parts water.

Heavy cleaning (degassing tanks and barges, engine rooms and soot, oil stained concrete,
petroleum based drilling muds) use 1 part TOPSALL #30 (aka, SUPERALL #38) to up to 15
parts water.

Severe cleaning (Black magic, Bunker C, crude oil, holding tanks, grease traps) use 1 part
TOPSALL #30 (aka, SUPERALL #38) to up to 5 parts water.

Steam cleaning use 1 part TOPSALL #30 (aka, SUPERALL #38) to up to 50 parts of water.
Pressure wash use 1 part TOPSALL #30 (aka, SUPERALL #38) to up to 30 parts water.
DO NOT USE UNDILUTED ON COMPOSITION FLOORS, WATER BASED PAINTED
SURFACES, OR ALUMINUM.

3.	Conditions for Use: Recommended for cleaning petroleum fractions from decks, platforms,
bilges, rigs, and other seagoing equipment, as noted above.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested Species	LC50 (ppm)

TOPSALL #30 Menidia beryllina	156.60 96-hr

(aka, SUPERALL #38) Mysidopsis bahia	115.80 48-hr

No. 2 Fuel Oil Menidia beryllina	6.40 96-hr

Mysidopsis bahia	1.30 48-hr

TOPSALL #30 Menidia beryllina	4.60 96-hr

(aka, SUPERALL #38) & Mysidopsis bahia	5.00 48-hr
No. 2 Fuel Oil (1:10)

Reference Toxicant (DSS) Menidia beryllina	1.60 96-hr

Mysidopsis bahia	10.00 48-hr
NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

Surface Washing Agents

249

TOPSALL #30


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b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 20°F

3.	Viscosity: 30.53 SUS at 100°F

4.	Specific Gravity: 1.06 at 70°F

5.	pH: 12.6

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility: Miscible with water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.05

Cadmium	<0.002

Chromium	0.031

Copper	0.25

Lead	0.02

Mercury	<0.01

Nickel	<0.01

Zinc	0.25

Cyanide	<0.1

Chlorinated Hydrocarbons	<0.1

Surface Washing Agents

250

TOPSALL #30


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

11/03/2008
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-9

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MAY 25, 1989

REVISED LISTING DATE: APRIL 16, 1996

"CN-110"

I.	NAME, BRAND, OR TRADEMARK
CN-110

Type of Product: Surface Washing Agent
(formerly D-37)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Chemex, Inc.

107-B Balboa Drive
Broussard, LA 70518
Phone: updated information required
E-mail: updated information required
(Contact: updated information required)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Chemex, Inc.

107-B Balboa Drive
Broussard, LA 70518
Phone: updated information required
E-mail: updated information required
(Contact: updated information required)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: None needed.

3.	Skin and eye contact; protective clothing; treatment in case of contact: As in handling any
industrial chemical, the standard precautions of wearing chemical-resistant gloves and eye
protection are recommended.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: -40°F

4.c. Optimum storage temperature range: 70°F-80°F

4.d. Temperatures of phase separations and chemical changes: Product does not lose
effectiveness between temperatures of -40°F through 120°F, although it will become hazy if the
temperature is sustained at less than 30°F over a 24-hour period.

Surface Washing Agents

251

CN-110


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V.	SHELF LIFE:

CN-110 has a shelf life of 2 years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: There are no application restrictions. The preferred application method
is by spraying and/or applying the product over the pollutant (primarily oil of any viscosity) on
the stained area. Immediately, the product begins to work on breaking the physical bond
between the oil and the object desired to be cleaned. The full effect of CN-110 on hard, porous
and most non-porous materials usually takes a minimum of 30 minutes with a maximum
retention time of 60 minutes. Then the freed oil is sprayed off with available water. The oil is
then safely and effectively skimmed without dispersed oil remaining in the affected waters.

If "herding" or "corralling" a slick is desired, CN-110 can also be applied without the increased
toxicities by dispersing minute particles of oil into the affected water stream.

2.	Concentration/Application Rate: Application concentration for cleaning shorelines is
approximately 1 gallon per 75-100 square feet of affected area. Depending on depths of
shorelines, this amount will give a residual of much less than 1 ppm of CN-110 in the affected
waters. This residual should be lower than the toxicity of the spilled oil.

If "herding" is desired, the application concentration should be in its original state while either
spraying CN-110 around the slick or dropping small amounts from a plane. The resulting
residual concentration in this case should be the same as shoreline cleaning or less.

If it is desired that CN-110 be added to a high-pressure cleaning system or steam, the dilution
rate should be no lower than 10%. This will lower the CN-110 residual in the affected waters to
the parts per billion range.

3.	Conditions for Use: Preferably fresh water, at temperature of 32°F.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (DDm)

CN-110

Menidia beryllina

52,233.00 96-hr



Mysidopsis bahia

12,262.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

1.90 96-hr



Mysidopsis bahia

0.90 48-hr

CN-110

Menidia beryllina

7.40 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.19 48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.80 96-hr



Mysidopsis bahia

5.90 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this

bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

Surface Washing Agents

252

CN-110


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VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: None

2.	Pour Point: 30°F

3.	Viscosity: 45.7 cSt at 78°F

4.	Specific Gravity: 1.025

5.	pH: 11.4

6.	Surface Active Agents: Trace amounts of a sulfonated compound

7.	Solvents: None

8.	Additives: Complex silicate solution

9.	Solubility: NA

X. ANALYSIS FOR HEAVY METALS,

HYDROCARBONS

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons
* Duplicate Analyses

CYANIDES, AND CHLORINATED

Concentration (ppm)
<0.22
<0.088
0.109/0.131*
0.238/0.234*
<0.275
<0.0001
<0.11

<0.374/<0.369*

0.25
ND

Surface Washing Agents

253

CN-110


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TECHNICAL PRODUCT BULLETIN #SW-10

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 21, 1989

REVISED LISTING DATE: SEPTEMBER 27, 1995

"COREXIT™ EC9580A"

I.	NAME, BRAND, OR TRADEMARK
COREXIT™ EC9580A

Type of Product: Surface Washing Agent (hydrocarbon based)

(formerly COREXIT 9580 SHORELINE CLEANER; D-38)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Corexit Environmental Solutions LLC

11177 South Stadium Drive
Sugar Land, TX 77478
Product Management:

Phone: (281)632-8827
E-mail: corexitinfo@corexit.com
(Mr. Huw Jones)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO nonflammable; DOT combustible

2.	Ventilation: Use with ventilation equal to unobstructed outdoors in moderate breeze.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
eyes, skin and clothing. Wash skin with soap and water. Flush eyes with plenty of water until
irritation subsides. Remove to fresh air.

4.a.	Maximum storage temperature: 170°F
4.b. Minimum storage temperature: -30°F

4.c. Optimum storage temperature range: 40°F-100°F

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

The shelf life of unopened drums of COREXIT™ EC9580A is unlimited.

Surface Washing Agents

254

OREXIT™ EC9580A


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VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: COREXIT™ EC9580A contains a balanced formula of specifically
selected biodegradable surfactants in a de-aromatized hydrocarbon solvent system. COREXIT™
EC9580A has a very low degree of toxicity to marine and shoreline organisms.

Shorelines, Mangroves, and Seagrasses - COREXIT™ EC9580A is sprayed directly on the oiled
rocky shorelines, mangroves or seagrasses full strength as supplied. After a soak time of zero to
thirty minutes, rinse the cleaner and the oil released from the shoreline surface into the water
where it can be readily recovered by conventional means such as skimmers or absorbents. The
soak time may vary with temperature, oil density and degree of weathering.

2.	Concentration/Application Rate: The recommended dosage is approximately 1 gallon per 100
square feet but this can vary depending on the amount of weathering and oiling. The product
should be applied full strength as supplied. Since it is hydrocarbon-based, the product should not
be diluted with water during application as this will greatly reduce effectiveness.

3.	Conditions for Use: COREXIT™ EC9580A is useful on shorelines in fresh or salt water. It is
effective on all types of oil including heavily weathered and emulsified oil ("chocolate mousse")
containing up to 50 percent water.

VII.	TOXICITY AND EFFECTIVENESS

~.	Toxicity:

Material Tested Species	LC50 (ppm)

COREXIT™ EC9580A Menidia beryllina	86.88 96-hr

Mysidopsis bahia	31.96 48-hr

No. 2 Fuel Oil Menidia beryllina	10.72 96-hr

Mysidopsis bahia	16.12 48-hr

COREXIT™ EC9580A & Menidia beryllina	13.20 96-hr

No.2 Fuel Oil (1:10) Mysidopsis bahia	9.06 48-hr

Reference Toxicant (DSS) Menidia beryllina	7.02 96-hr

Mysidopsis bahia	9.82 48-hr
NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 174°F

2.	Pour Point: -65°F

3.	Viscosity: 8 cSt at 104°F, 28 cSt at 32°F

4.	Specific Gravity: 0.810 at 60°F

5.	pH: Not Applicable

~.	Surface Active Agents: CONFIDENTIAL

Surface Washing Agents

255

OREXIT™ EC9580A


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7.	Solvents: De-aromatized Hydrocarbon

8.	Additives: None

9.	Solubility: Not Applicable

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.06

Cadmium	<0.002

Chromium	0.003

Copper	<0.001

Lead	<0.009

Mercury	<0.0002

Nickel	0.01

Zinc	0.041

Cyanide	<0.05

Chlorinated Hydrocarbons	ND

Surface Washing Agents

256

OREXIT™ EC9580A


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-11
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JUNE 26, 1989
REMOVAL DATE: SEPTEMBER 15, 1994
RELISTING DATE: JULY 07, 2010
"DE-SOLV-IT INDUSTRIAL FORMULA"

I.	NAME, BRAND, OR TRADEMARK
DE-SOL V-IT INDUSTRIAL FORMULA
Type of Product: Surface Washing Agent
(formerly D-40)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Orange-Sol Blending and Packaging

1400 N Fiesta Boulevard

Gilbert, AZ 85233

Phone: (800) 877-7771

Fax: (480) 497-0444

E-mail: updated information required

Website: www.orange-sol.com

(Mr. Albert Farnsworth or

Mr. Jack Farnsworth at (480) 319-0141)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Bell Tech

Master Distributor

P.O. Box 2198

Valdez, AK 99686

Phone: (907) 602-0111

Fax: (907) 835-4535

E-mail: bellenterprise@cvinternet.net

(Mr. Randy Bell)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Not regulated unless shipped by land in a package
having a capacity of 3,500 gallons or more). Combustible Class IIIA per OSHA, 29 CFR
1910.106

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
of clothing required; however, goggles are recommended where splash is potential. If eye or skin

3/03/2016
7/27/2022

Surface Washing Agents

257

PREMIER 99


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irritation occurs, flush with ample fresh water.

4.a. Maximum storage temperature: 120°F continuous, 140°F up to 5 days

4.b. Minimum storage temperature: -20°F

4.c. Optimum storage temperature range: 0°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Two (2) years in sealed polydrums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: DE-SOLV-IT (DSI) is to be used in neat form. DSI works just as well
with fresh or salt water. This product works well with all types of oils. Product can be used on
oil-contaminated beaches.

2.	Concentration/Application Rate: Use DSI directly on the contaminated area, or up to
approximately a 1:10 dilution ratio (product:water). Lighter oils will require a 1:10 to 1:30
product to water dilution ratio. Warmer waters (greater than 78°F) and/or good agitation during
application will require less product. Response personnel can determine best method to collect
clean up residue. Clean up residue should be collected and disposed of in accordance to local,
state, and federal regulations.

3.	Conditions for Use: Effective in salt or fresh water, with no limitations as to usage within
optimum temperature parameters (application may be made at or above 35°F, with optimum
above 48°F).

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

DE-SOLV-IT

Menidia beryllina

37.71 96-hr



Mysidopsis bahia

4.57 48-hr

No. 2 Fuel Oil

Menidia beryllina

3.76 96-hr



Mysidopsis bahia

2.04 48-hr

DE-SOLV-IT &

Menidia beryllina

9.40 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.68 48-hr

Reference Toxicant (SLS)

Menidia beryllina

12.25 96-hr



Mysidopsis bahia

11.71 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 145°F

2.	Pour Point: -84°F

3.	Viscosity: 1.8 cSt @ 40°C

Surface Washing Agents

258

PREMIER 99


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4.	Specific Gravity: 1.8345 @60°F

5.	pH: 6.6

6.	Surface Active Agents: Nonionic PROPRIETARY Surfactants

7.	Solvents: PROPRIETARY

8.	Additives: None

9.	Solubility: Miscible in oil and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.010

Cadmium	<0.005

Chromium	<0.015

Copper	<0.015

Lead	<0.010

Mercury	<1 |ig/L

Nickel	<0.025

Zinc	0.0.15

Cyanide	<0.010

Chlorinated Hydrocarbons	<6.00

Surface Washing Agents

259

PREMIER 99


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LISTING CHANGES PENDING;

VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN #SW-12

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 11, 1989

REVISED LISTING DATE: NOVEMBER 2, 1995

"PREMIER 99"

I.	NAME, BRAND, OR TRADEMARK
PREMIER 99

Type of Product: Surface Washing Agent (Water Based)

(formerly D-41)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Gold Coast Chemical Products

2357 Stirling Road
Dania Beach, FL 33312
Phone: (954) 893-0044
Fax: (954) 893-8884

E-mail: noslime@goldcoastchemical.com
(Mr. Eli Finkelberg or Ms. Maria Morris)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Gold Coast Chemical Products

2357 Stirling Road
Dania Beach, FL 33312
Phone: (954) 893-0044
Fax:(954) 893-8884

E-mail: noslime@goldcoastchemical.com
(Mr. Eli Finkelberg or Ms. Maria Morris)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: None

2.	Ventilation: Adequate ventilation is needed if in closed environment.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Skin and eye contact:
Detergents will defat skin and eyes. May cause irritation. Protective clothing: Use protective
gloves for manual cleaning and splash goggles. Treatment in case of contact: If splashed on
skin, wash with copious amounts of water. If ingested, drink diluted vinegar or lemon juice. Get
medical attention.

4.a.	Maximum storage temperature: 125°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 0°F - 75°F

Surface Washing Agents

260

PREMIER 99


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Avoid freezing the product. If material freezes and separation is experienced, it should be
warmed and mixed together.

4.d. Temperatures of phase separations and chemical changes: No separation expected down to
20°F.

V.	SHELF LIFE

Unopened material - at least 5 years is expected.

Opened material - at least 2 years is expected.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply by spray, mop, or pressure washer, etc. Agitate severe spots.
Rinse thoroughly for residue free surface.

2.	Concentration/Application Rate:

Normal Cleaning - 1 part PREMIER 99 to up to 20 parts water.

Heavy Cleaning - 1 part PREMIER 99 to up to 15 parts water.

Severe Cleaning - 1 part PREMIER 99 to up to 5 parts water.

Steam Cleaning - 1 part PREMIER 99 to up to 50 parts water.

Pressure Wash - 1 part PREMIER 99 to up to 30 parts water.

3. Conditions for Use: Water salinity, water temperature, types and ages of pollutants are not

determined.





VII. TOXICITY AND EFFECTIVENESS





a. Toxicity:





Material Tested

Species

LC50 (ppm)

PREMIER 99

Menidia beryllina

565.70 96-hr



Mysidopsis bahia

94.70 48-hr

No. 2 Fuel Oil

Menidia beryllina

10.20 96-hr



Mysidopsis bahia

2.10 48-hr

PREMIER 99 &

Menidia beryllina

8.20 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.50 48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.55 96-hr



Mysidopsis bahia

7.96 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this

bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES
1. Flash Point: 160°F

Surface Washing Agents

261

PREMIER 99


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2.	Pour Point: NA

3.	Viscosity: 15 cps

4.	Specific Gravity: 1.01

5.	pH: 10- 11.5

6.	Surface Active Agents: Active 8000* - Purity Chemical <10%

7.	Solvents: <5%

8.	Additives: <5%

9.	Solubility: Complete in Water

*NOTE: Particular chemical composition of Active 8000 is considered by Purity Chemical as a
trade secret. More detailed information can be given by Purity Chemical - Mr. Jim Palmer, 1800
NW 70th Avenue, Miami, FL 33126, 1-800-654-0235, FAX (305) 592-2601.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	< 0.01

Cadmium	< 0.0005

Chromium	<0.1

Copper	<0.1

Lead	< 0.005

Mercury	<0.001

Nickel	< 0.5

Zinc	<0.1

Cyanide	< 0.005

Chlorinated Hydrocarbons	ND

Surface Washing Agents

262

PREMIER 99


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LISTING CHANGES PENDING;

VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN #SW-15

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: APRIL 23,1990

REVISED LISTING DATE: AUGUST 30, 1995

"SIMPLE GREEN®"

I.	NAME, BRAND, OR TRADEMARK
SIMPLE GREEN®

Type of Product: Surface Washing Agent (Water Based)

(formerly D-46)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Sunshine Makers, Inc.

15922 Pacific Coast Highway

Huntington Beach, CA 92649

Phone: (800) 228-0709

Phone: (562) 795-6000

Fax: (562) 592-3830

E-mail: LLorincz@simplegreen.com

(Ms. Laura Lorincz)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Sunshine Makers, Inc.

15922 Pacific Coast Highway

Huntington Beach, CA 92649

Phone: (800) 228-0709

Phone: (562) 795-6000

Fax: (562) 592-3830

E-mail: LLorincz@simplegreen.com

(Ms. Laura Lorincz)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Not required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: SIMPLE GREEN® is
safe for use on skin and will not cause irritation in the majority of users. Avoid contact with eyes,
irritation may result. Wear splash goggles or full face-shield and have eye washing equipment
available in areas where potential is high for eye contact. No special precautions or additional
protective equipment are required during handling or use. SIMPLE GREEN® is provided with a
Material Safety Data Sheet (No. 1002).

Surface Washing Agents

263

SIMPLE GREEN®


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4.a. Maximum storage temperature: 140°F

4.b. Minimum storage temperature: 34°F

4.c. Optimum storage temperature range: >32°F and <140°F

4.d. Temperatures of phase separations and chemical changes: SIMPLE GREEN® is stable and
phase separation will not occur at temperatures within the above storage range.

V.	SHELF LIFE

SIMPLE GREEN® has an unlimited shelf life.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray on oily surface.

2.	Concentration/Application Rate: For open water, spray concentrated product directly on
surface of oil at a ratio of 4 parts of oil to 1 part of SIMPLE GREEN®. Site conditions may
warrant alternative procedures to maintain effectiveness.

3.	Conditions for Use: Equally effective in fresh water, estuarine, and marine environments at all
temperatures. SIMPLE GREEN® contains no known EPA Priority Pollutants.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (DDm)

SIMPLE GREEN®

Menidia beryllina

27.90 96-hr



Mysidopsis bahia

77.60 48-hr

No. 2 Fuel Oil

Menidia beryllina

6.50 96-hr



Mysidopsis bahia

3.70 48-hr

SIMPLE GREEN® &

Menidia beryllina

8.30 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

4.40 48-hr

Reference Toxicant (DSS)

Menidia beryllina

7.80 96-hr



Mysidopsis bahia

21.20 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.

VIII.	MICROBIOLOGICAL ANALYSIS

SIMPLE GREEN® contains no microorganisms, enzymes, or biological material.

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: None

3.	Viscosity: 2.0 Centistokes at 78°F

4.	Specific Gravity: 1.0257 g/ml at 72°F

5.	pH: 9.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

Surface Washing Agents

264

SIMPLE GREEN®


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8.	Additives: CONFIDENTIAL

9.	Solubility: Infinitely miscible.

(Increasing salt concentrations in marine ecosystems will lead to complexes with SIMPLE
GREEN® that may become visible at ratios above one part SIMPLE GREEN® to 99 parts
seawater.)

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<5.0000

Cadmium	<0.0233

Chromium	0.1150

Copper	<0.7500

Lead	0.0776

Mercury	<0.0125

Nickel	<2.3000

Zinc	<4.4000

Cyanide	<1.0000

Chlorinated Hydrocarbons	<1.0

Surface Washing Agents

265

SIMPLE GREEN®


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TECHNICAL PRODUCT BULLETIN #SW-16

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 8, 1991

REVISED LISTING DATE: JUNE 14, 1995

"AQUACLEAN"

I.	NAME, BRAND, OR TRADEMARK
AQUACLEAN

Type of Product: Surface Washing Agent
(formerly D-52)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Madison Chemical Company, Inc.

3141 Clifty Drive

Madison, IN 47250

Phone: (812) 273-6000

Fax:(812) 273-6002

E-mail: steve.preece@madchem.com

(Dr. Steve Preece)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Madison Chemical Company, Inc.

3141 Clifty Drive

Madison, IN 47250

Phone: (812) 273-6000

Fax:(812)273-6002

E-mail: steve.preece@madchem.com

(Dr. Steve Preece)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Handle in a well-ventilated space. Local exhaust is recommended if TLV's are
exceeded.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye and skin
contact. In case of such contact, immediately flush with large amount of cool water for at least
15 minutes, and call a physician. Wear protective eye goggles, impermeable protective gloves,
and protective clothing when handling the product. Wash contaminated protective equipment
(including clothing, shoes, eye goggles, gloves, etc.) thoroughly in soap and water, rinse
repeatedly in clean water and dry before reuse. Avoid ingestion, breathing dusts, mists, or fumes.
In case of ingestion, induce vomiting, give water and call a physician. In case of inhalation,
move the affected person to fresh air, and call a physician.

4.a.	Maximum storage temperature: 140°F

Surface Washing Agents

266

AQUACLEAN


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4.b. Minimum storage temperature: 50°F

4.c. Optimum storage temperature range: >50°F to <104°F

4.d. Temperatures of phase separations and chemical changes: <50°F, >104°F

V.	SHELF LIFE

18 months if stored between 50°F and 104°F, and away from acids.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: AQUACLEAN may be introduced with a pressure spray to cover the
affected area, after the appropriate dilution or concentration is prepared. After application,
agitate spill area with water using a solid stream flow.

For manual cleaning with AQUACLEAN, follow instructions in the product data sheet provided
by the manufacturer.

2.	Concentration/Application Rate: For small spills, dilute 3 to 1 with water and apply as above.
For large spills, prepare a 33% solution of AQUACLEAN and apply through a foam eductor at
6% setting with approximately 90 gallons per minute flow at the nozzle.

For spills on shorelines and beaches, dilute AQUACLEAN 50% with fresh water and apply
using a pressure spray to cover the entire contaminated area. Then rinse with fresh water.

3.	Conditions for Use: Water temperature should be above 41°F.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material tested

Species

LC50 (ppm)

AQUACLEAN

Menidia beryllina

70.7 96-hr



Mysidopsis bahia

32.7 48-hr

No. 2 Fuel Oil

Menidia beryllina

4.4 96-hr



Mysidopsis bahia

1.8 48-hr

AQUACLEAN and

Menidia beryllina

6.5 96-hr

No. 2 Fuel (1:10)

Mysidopsis bahia

2.1 48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.4 96-hr



Mysidopsis bahia

4.9 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

267

AQUACLEAN


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IX. PHYSICAL PROPERTIES

1.	Flash Point: None detected

2.	Pour Point: -20°F

3.	Viscosity: 16.5 cP at 25°C (77°F)

4.	Specific Gravity: 1.06 at 25°C (77°F)

5.	pH: 11.8 (at full strength)

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: Anionic and nonionic synthetic surfactants.

8.	Solvents: CONFIDENTIAL

9.	Additives: CONFIDENTIAL

10.	Solubility: Completely soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	1.10

Cadmium	0.16

Chromium	0.20

Copper	0.66

Lead	1.83

Mercury	<0.01

Nickel	0.80

Zinc	0.29

Cyanide	0.06

Chlorinated hydrocarbons	4.20

Surface Washing Agents

268

AQUACLEAN


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

6/10/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-18

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: OCTOBER 23, 1996

"NATURE'S WAY HS" (There is only one listing and no "aka 's "for this product.)

I.	NAME, BRAND, OR TRADEMARK
NATURE'S WAY HS

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Integra Environmental, Ltd.

5825 Central crest
Houston, TX 77092
Phone: updated information required
Fax: updated information required
Email: updated information required
Website: updated information required
(Ms. Cathy Kaiser)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Integra Environmental, Ltd.

5825 Central crest
Houston, TX 77092
Phone: updated information required
Fax: updated information required
Email: updated information required
Website: updated information required
(Ms. Cathy Kaiser)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: No special precautions are required, but in case of inhalation, move person to
fresh air.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Flush contaminated
skin with plenty of water for at least 15 minutes. Consult a physician if irritation develops.
Protective gloves are recommended for extended or prolonged contact, (e.g., immersing hands).
Tight fitting safety goggles are recommended for handling product in concentrated form,
especially if contacts are worn.

4.a.	Maximum storage temperature: 130°F

Surface Washing Agents

269

NATURE'S WAY HS


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4.b. Minimum storage temperature: 32°F
4.c. Optimum storage temperature: 90°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

NATURE'S WAY HS has a five year shelf life.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: NATURE'S WAY HS may be applied by spraying, pouring, dispensing
equipment, or by manual or automatic scrubber machines. Do not mix the product with any
other cleaner nor allow any other cleaners to contact surfaces where HS is being used. Hot water
should never be used.

2.	Concentration/Application Rate: Apply NATURE'S WAY HS full strength (undiluted) to
surface area with sprayer, concentrating on areas with heaviest contamination first. To speed
clean-up of shorelines and beaches, pressure spray into cracks and crevices prior to scrubbing.
Agitate and scrub well using power brushes, hand brushes, brooms or mops. If possible, allow
the scrubbed solution to remain on the surface for at least 15 minutes. If allowed to soak
overnight, the next morning the treated surface must be re-wet with water, reagitated, and rinsed.
Additional product will not be necessary at that time.

3.	Conditions for Use: For heavily contaminated surfaces, NATURE'S WAY HS should always
be used full strength. For moderate accumulations HS may be diluted to as little as 2 oz. per
gallon of cool water for cleaning light contamination. For average contamination, a dilution of
12 oz. per gallon is recommended (1 part NATURE'S WAY HS to 10 parts water). For light use,
4 to 6 oz. of product per gallon water will be sufficient.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (DDm)

NATURE'S WAY HS

Menidia beryllina

152.14 96-hr



Mysidopsis bahia

193.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

3.15 96-hr



Mysidopsis bahia

0.96 48-hr

NATURE'S WAY HS

Menidia beryllina

3.91 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.07 48-hr

Reference Toxicant (DSS)

Menidia beryllina

96-hr



Mysidopsis bahia

5.71 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this

bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
a. Effectiveness:

NA

Surface Washing Agents

270

NATURE'S WAY HS


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VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: Flowable at all temperatures above freezing

3.	Viscosity: <100 CPS

4.	Specific Gravity: 1.01

5.	pH: 8-9.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: NA

X. ANALYSIS FOR HEAVY METALS AND CHLORINATED HYDROCARBONS

ComDOund

Concentration (dditi)

Arsenic

<0.003

Cadmium

<0.005

Chromium

<0.010

Copper

0.020

Lead

<0.002

Mercury

<0.0002

Nickel

<0.030

Zinc

0.260

Cyanide

<0.020

Chlorinated Hydrocarbons

ND

Surface Washing Agents

271

NATURE'S WAY HS


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TECHNICAL PRODUCT BULLETIN #SW-19

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JANUARY 30, 1997

"CYTOSOL"

I. NAME, BRAND, OR TRADEMARK
CYTOSOL

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
CytoCulture International, Inc.

122 Martina Street

Point Richmond, CA 94801-3829

Phone: (510) 233-0102

Fax: (510) 233-3777

Emergency Mobile: (510) 233-0102

E-mail First Response: rvwedel@gmail.com

E-mail: cytoculture@gmail.com

Website: www.cvtosolbiosolvent.com

Website: www.cvtoculture.com

(Dr. Randall von Wedel)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
CytoCulture International, Inc.	Foss Environmental, Inc.

122 Martina Street	7440 West Marginal

Point Richmond, CA 94801-3829	Seattle, WA 98108-4141

Phone: (510) 233-0102	Phone: (206) 768-1450

Fax: (510) 233-3777	Fax: (206) 767-3460

Emergency Mobile: (510) 233-0102	(Mr. Larry Pintler)

E-mail First Response: rvwedel@gmail.com

E-mail: cvtoculture@ gm ail. com

Website: www.cvtosolbiosolvent.com

Website: www.cvtoculture.com

(Dr. Randall von Wedel)

Advanced Cleanup Technologies, Inc.

20928 Lamberton Avenue

Carson, CA 90810

Phone: (800) 334-2284

Fax: (310) 763-9076

(Mr. Walt Dorn)

Surface Washing Agents

272

CYTOSOL


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IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable. However, keep the product away from heat and avoid contact
with strong oxidizing agents. Ensure proper disposal of product-saturated absorbents, rags, and
combustible materials to avoid the possibility of spontaneous combustion.

2.	Ventilation: Product is not volatile. However, in the event of aerosol inhalation, immediately
move victim to fresh air. If victim has stopped breathing, give artificial respiration, preferably
by mouth to mouth. Get medical attention immediately.

3.	Skin and eye contact; protective clothing; treatment in case of contact: The CYTOSOL
contains no volatile hydrocarbons or petroleum constituents. However, as a precautionary
measure, wear gloves and safety glasses meeting the specifications of ANSI Standard Z87.1.
Avoid breathing aerosols. Avoid prolonged contact with skin.

4.a.	Maximum storage temperature: 110°F
4.b. Minimum storage temperature: 39°F
4.c. Optimum storage temperature: 55°F

4.d. Temperatures of phase separations and chemical changes: Avoid freezing. At temperatures
below the cloud point (43°F), the product may become cloudy, but will return to normal upon
warming, with no effect on performance. Store product in airtight containers, if possible,
without excessive exposure to moisture.

V.	SHELF LIFE

Closed container: 10 years in a dry environment.

Open container: 1 year in a warm, humid environment.

The product does not deteriorate appreciably over time, but will grow bacteria if water
condensation accumulates in the container.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: The CYTOSOL is applied to oiled shorelines to extract and recover
weathered petroleum by flotation with passive water deluges from header pipes or manual
spraying. Remaining residual hydrocarbons are biodegraded, either passively by intrinsic
bioremediation, or aggressively by enhancing the process with controlled amounts of nutrients
and/or acclimated cultures of bacteria cultured from the site, when approved by local, state and
federal agencies.

The CYTOSOL process is most suitable for the treatment of heavily oiled shorelines that do not
respond well to conventional treatments, or that are considered too sensitive for
mechanical/pressure wash strategies. Prior to the application of CYTOSOL, collection booms,
oil skimmers, sorbent pads, or other appropriate containment and collection mechanisms must be
deployed and operational.

2.	Concentration/Application Rate: CYTOSOL may be applied with a variety of spraying or
washing equipment, depending upon the scale and type of shoreline to be cleaned. The product
is to be used only neat and undiluted, for direct application to spilled oil. For large beach areas,
CYTOSOL can be sprayed from water trucks or work boats equipped with pumps, hoses, and

Surface Washing Agents

273

CYTOSOL


-------
nozzles to deliver the product as an aerial spray. In smaller applications, CYTOSOL may be
applied with hand sprayers or portable pumps to spray the product directly onto oiled surfaces.
Dose rates will vary with the type and amount of petroleum spilled, the extent of weathering, and
other site specific conditions, including temperature, porosity of shoreline, and residence time
available to let the product contact the oil. In general, the ratio of applied CYTOSOL to crude
oil is between 0.5:1 and 1:1. The quantity of CYTOSOL applied should be approximately
equivalent to the quantity of petroleum accumulated on the shoreline, or as required to dissolve
and remove weathered oil. After application, the product should be allowed to penetrate and
dissolve the weathered petroleum for at least one hour, preferably longer. Cold weather
applications will require more contact time before initiating recovery. In tidal areas, it is
advisable to apply the CYTOSOL as the tide is ebbing (receding) to maximize contact time.
Trapped oil may continue to be released for several days, requiring that containment devices be
left in place.

3. Conditions for Use: The following shoreline types are appropriate for the use of CYTOSOL:
Coarse sand beaches where petroleum has penetrated into sand; marsh areas and vegetated
wetlands where oil has coated plants and become trapped; concrete bulkheads, rip rap and piers
that may have trapped oil; oiled pilings; gravel or cobble shorelines and rocky shores, where oil
has become trapped in pockets; and, public beaches, fisheries, hatcheries, river banks, and other
sensitive or high impact sites. The CYTOSOL has been fielded tested successfully for removing
oil from mussel beds and intertidal zones, pilings and concrete rip rap. The CYTOSOL also
proved effective in facilitating the removal of oil from the banks and vegetation along an oiled
creek.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity

Material Tested

Species

LC50 (DDm)

CYTOSOL

Menidia beryllina

738.0 96-hr



Mysidopsis bahia

124.0 48-hr

No. 2 Fuel Oil

Menidia beryllina

38.9 96-hr



Mysidopsis bahia

5.9 48-hr

CYTOSOL &

Menidia beryllina

24.3 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

7.0 48-hr

Reference Toxicant (DSS)

Menidia beryllina

13.8 96-hr



Mysidopsis bahia

22.2 48-hr

NOTE: This toxicity data was derived with the EPA protocols for dispersants using a blender to
emulsify the product into the water for testing organisms. The CYTOSOL emulsion created
microdroplets of product which may have had direct physical effects on the test larvae. Since the
solubility of the product in water is so low (14 ppm or less), it is probable that the observed
effects on the test organisms was caused by larvae having direct contact with droplets of product
rather than by a true chemical toxicity from the trace amount of dissolved product. In practice,
the CYTOSOL would not be emulsified to any great extent during application. See Section VI of
this bulletin for information regarding the manufacturer's recommendations for concentrations
and application rates for field use.

Surface Washing Agents

274

CYTOSOL


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b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: 360°F

2.	Pour Point: 10°F

3.	Viscosity: 4.15 CST @ 104°F

4.	Specific Gravity: 0.8877 @ 60°F

5.	pH: Neutral

6.	Surface Active Agents: None

7.	Solvents: No Petroleum Distillates

8.	Additives: CONFIDENTIAL

9.	Solubility: 14 ppm in fresh water, 7 ppm in sea water

X. ANALYSIS FOR HEAVY METALS AND CHLORINATED HYDROCARBONS

Compound

Concentration

Arsenic

ND

Cadmium

ND

Chromium

ND

Copper

ND

Lead

ND

Mercury

ND

Nickel

ND

Zinc

ND

Cyanide

ND

Chlorinated Hydrocarbons

ND

Surface Washing Agents

275

CYTOSOL


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TECHNICAL PRODUCT BULLETIN #SW-20
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: MARCH 21, 1997
"BIOSOLVE® PINKWATER®"

I.	NAME, BRAND, OR TRADEMARK
BIOSOLVE® PINKWATER®

Type of Product: Surface Washing Agent

(formerly BIOSOLVE® HYDROCARBON MITIGATION™ AGENT)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
The BioSolve® Company

24 Victory Lane
Dracut, MA 01826

Phone: (781) 482-7900 or (800) 225-3909
Fax: (781)482-7909
Website: www.biosolve.com
E-mail: info@biosolve.com
(Mr. Stephen Hosmer)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
The BioSolve® Company

24 Victory Lane
Dracut, MA 01826

Phone: (781) 482-7900 or (800) 225-3909
Fax: (781)482-7909
Website: www.biosolve.com
E-mail: info@biosolve.com
(Mr. Stephen Hosmer)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal

3.Skin and eye contact; protective clothing; treatment in case of contact: Flush contaminated
eyes thoroughly with water for 15 minutes, and get medical attention. Remove contaminated
clothing, wash exposed area with soap and water, wash clothing before reuse. Get medical
attention if irritation develops. Get medical attention for ingestion. No medical attention is
necessary with inhalation. There are no special storage requirements or special handling
precautions; use good normal hygiene.

4.a. Maximum storage temperature: 120°F (50°C)

4.b. Minimum storage temperature: 35°F (1.5°C)

4.c. Optimum storage temperature: 60°F (15°C)

Surface Washing Agents

276

BIOSOLVE® PINKWATER®


-------
4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

BIOSOLVE® has a 10+ year shelf life if unopened.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Dilute or use eductors to specified rate and apply through fire hose,
power washers, steam powered units, or chemical boom sprayers with nozzles that produce a
shearing action. Special nozzles to apply the solution as droplets are not necessary. For
shoreline cleanup involving heavy or weathered crude, presoak to a 6% solution may be
necessary.

2.	Concentration/Application Rate: BIOSOLVE® is a highly concentrated product and must be
diluted with water before use. Dilution ratios vary depending on site specific conditions.
Dilution ratio's normally run at 6%, 3%, or 1%. For heavy, mousse, or weathered oil, a 3% to
6% solution should be applied. For light or refined products, apply at 2% to 3%. For sheens,
apply at .5 to 1%. Since testing shows that BIOSOLVE® quickly emulsifies weathered crude, it
is not critical to apply immediately after a spill occurs; impact considerations can be fully
considered prior to action taken.

Surface Washing Applications: BIOSOLVE® applied through power washers in light dilution is
very effective in attaining the removal of oils from rock, cobblestone, shorelines, and sea walls.
In marsh or wetland applications, BIOSOLVE® prevents the oil from clinging to grasses and
mangroves.

Rigs and Platforms: BIOSOLVE® is used to inert undersea pipelines before plugging and
abandonment, degas tanks and platforms during work over operations, and to wash drill cuttings
to remove oils and prevent sheens on surface waters.

3.	Conditions for Use: May be used with salt or fresh water. Temperature is not relevant.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (DDm)

BIOSOLVE®

Menidia beryllina

6.4 96-hr



Mysidopsis bahia

3.6 48-hr

No. 2 Fuel Oil

Menidia beryllina

5.6 96-hr



Mysidopsis bahia

2.7 48-hr

BIOSOLVE® &

Menidia beryllina

7.4 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

1.3 48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.2 96-hr



Mysidopsis bahia

13.4 48-hr

NOTE: This toxicity data was derived using the concentrated product. See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and

Surface Washing Agents

277

BIOSOLVE® PINKWATER®


-------
application rates for field use.
b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES
(Liquid concentrate)

1.	Flash Point: NA, Water based >200°F (93.3°C)

2.	Pour Point: 32.9°F (0.5°C)

3.	Viscosity: 77.5 Centistrokes (concentrate), 490 centipoise (concentrate), 15 centipoise at 6%,
at 60.08°F or 15.6°C

4.	Specific Gravity: 1.025 at 60°F or 15.5°C

5.	pH: 9.37 +/- 0.5

6.	Chemical Name and Percentage by Weight of the Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

9.	Additives: CONFIDENTIAL

10.	Solubility: Complete-true solution formed with water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.2

Cadmium	<0.18

Chromium	<0.5

Copper	<0.6

Lead	<0.2

Mercury	<0.07

Nickel	<0.6

Silver	<0.4

Zinc	0.51

Cyanide	<0.01

Chlorinated Hydrocarbons	<0.5

Surface Washing Agents

278

BIO SOLVE® PINKWATER®


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-21
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: MARCH 2, 1998
"PETROTECH 25"

I.	NAME, BRAND, OR TRADEMARK
PETROTECH 25

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Petrotech America Corporation

130 William Street, Suite 802

New York, NY 10038

Phone: (212)933-9071, ext. 7001

Fax: (877) 226-4028

E-mail: Info@helpenvironmental.com

(Mr. Lawrence Gallo)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Petrotech America Corporation	Manufacturing Plant:

130 William Street, Suite 802	Clariant Corp.

New York, NY 1003 8	Charlotte, NC

Phone: (212)933-9071, ext. 7001

Fax: (877) 226-4028

E-mail: Info@helpenvironmental.com

(Mr. Lawrence Gallo)

H.E.L.P.	Environmental
926 3rd Avenue
Brooklyn, NY 11232

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

I.	Flammability: Non-flammable.

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special handling is
required beyond that prescribed under the general OSHA rules for non-hazardous, non-
flammable and noncorrosive liquids. This is not to suggest that contact with eyes and skin is
totally without risk for allergy. Contact with eyes and skin is to be avoided, as suggested under
OSHA procedures.

4.a.	Maximum storage temperature: +45°C

7/19/2021
7/27/2022

Surface Washing Agents

279

PETROTECH 25


-------
4.b. Minimum storage temperature: -5°C (can be stored below its freezing point without
detectable loss of performance provided that it is warmed to within liquid range prior to
application.)

4.c. Optimum storage temperature: >-5°C and <+45°C

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

PETROTECH 25 has an unlimited shelf-life when maintained in the factory sealed containers
and stored within the prescribed temperature limits. Climatic factors such as humidity have no
effect on closed container storage although the product is hygroscopic and will absorb water if
left for long periods in open containers.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: It is recommended that the surface washing agent PETROTECH 25 be
applied to contaminated surfaces in one of three ways: (a) a mixture of ten parts PETROTECH
25 to ninety parts water, either fresh or saltwater, should be discharged over the surface by
commercial pressure washer, hot or cold; (b) the same mixture discharged on the surface using
standard firefighting apparatus preferably at a nozzle pressure of 100 PSI plus; or (3)
PETROTECH 25 in concentrated form can be applied to the surface and manually or
mechanically brushed and then water applied.

2.	Concentration/Application Rate: Generally, PETROTECH 25 is applied neat in its factory
supplied concentrate form. However, for lighter oils where educting or proportioning equipment
is available, an aqueous solution of PETROTECH 25 between 3 and 10 percent may be used.
Broadly speaking, PETROTECH 25 has no solvent action. For any given oil spill of a specific
nature, the application rate is unaffected by neat or diluted application as long as the concentrate
to oil ratio remains the same. Applications of diluted PETROTECH 25 in the 6 - 10 percent
range via firefighting equipment can be used on automobile and aviation gasoline's together with
the lighter oils such as diesel and all jet fuels.

The dosage of PETROTECH 25 to be used depends upon two factors: 1) The nature of the oil,
and 2) The energy used in its application to the contaminated substrate.

3.	Conditions for Use: May be used with salt or fresh water. Temperature is not relevant.

Surface Washing Agents

280

PETROTECH 25


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

PETROTECH 25

Menidia beryllina

601.0 96-hr



Mysidopsis bahia

350.0 48-hr

No. 2 Fuel Oil

Menidia beryllina

2.8 96-hr



Mysidopsis bahia

1.8 48-hr

PETROTECH 25 & No. 2 Fuel Oil

Menidia beryllina

3.4 96-hr

(1:10)

Mysidopsis bahia

1.0 48-hr

Reference Toxicant (DSS)

Menidia beryllina

7.9 96-hr



Mysidopsis bahia

19.8 48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES
(Liquid concentrate)

1.	Flash Point: None

2.	Pour Point: 0°C

3.	Viscosity: 700 CP

4.	Specific Gravity: 1.03

5.	pH: 7.5

6.	Chemical Name and Percentage by Weight of Total Formulation: CONFIDENTIAL

7.	Surface Active Agents: CONFIDENTIAL

8.	Solvents: CONFIDENTIAL

9.	Additives: CONFIDENTIAL

10.	Solubility: 100%

X. ANALYSIS FOR HEAVY METALS AND CHLORINATED HYDROCARBONS

Compound

Concentration (ppm)

Arsenic

<0.10

Cadmium

<0.08

Chromium

<0.10

Copper

<0.26

Lead

0.047

Mercury

<0.0005

Nickel

<0.40

Zinc

0.256

Cyanide

0.70

Chlorinated Hydrocarbons

ND

Surface Washing Agents

281

PETROTECH 25


-------
TECHNICAL PRODUCT BULLETIN #SW-23

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: MARCH 1, 1999

"PETRO-CLEAN"

I.	NAME, BRAND, OR TRADEMARK
PETRO-CLEAN

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
B.R.A.T. Microbial Products Inc.

208 Cinnabar Bay Court
League City, TX 77573
Phone: (713) 724-9226
E-mail: alabastercorp@gmail.com
(Mr. John Sheffield)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
B.R.A.T. Microbial Products Inc.

208 Cinnabar Bay Court
League City, TX 77573
Phone: (713) 724-9226
E-mail: alabastercorp@gmail.com
(Mr. John Sheffield)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal

3.	Skin and eye contact: Protective clothing; treatment in case of contact. Eyes-flush with water
using eye cup of fountain for 15 minutes. Seek medical attention if irritation persists. Wash
contaminated clothing and footwear before reuse. Ingestion - seek medical attention. Inhalation
- no medical attention is required.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 35°F
4.c. Optimum storage temperature range:

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

Indefinite when stored properly.

Surface Washing Agents

282

PETRO-CLEAN


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VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: PETRO-CLEAN is applied through power washers or even garden type
sprayers in light dilution is very effective in removing petrochemical hydrocarbons from rocks,
shorelines, sea walls, bridges, and highways. In wetland applications, PETRO-CLEAN prevents
hydrocarbons from attaching to grasses, trees, rocks, etc.

2.	Concentration/Application Rate: Dilute or use eductors to specified rate and apply through fire
hose, power washers, or sprayers to contaminated area. PETRO-CLEAN is a highly
concentrated product and must be diluted before use. Dilution ratios vary depending on the
specific conditions of the contaminated site. Normal recommended dilutions are from 0.5% to
6%. On heavy or weathered crude, pre-soaking with 6% may be necessary. For light or refined
products, apply as 3% to 6% solution. For sheens on water apply a 0.5% to 1.0% solution.

3.	Conditions for Use: May be used with salt or fresh water

VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity
Material Tested
PETRO-CLEAN

No. 2 Fuel Oil

PETRO-CLEAN &

No. 2 Fuel Oil (1:10)

Reference Toxicant (DSS)

b.	Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: > 200°F

2.	Pour Point: -17°F

3.	Viscosity: 1.26@75°F

4.	Specific Gravity: 0.99 @ 75°F

5.	pH: 8.05 (10% solution, s.u.)

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: 100 percent

Species	LC50 (ppm)

Menidia beryllina	100 96-hr

Mysidopsis bahia	110 48-hr

Menidia beryllina	110 96-hr

Mysidopsis bahia	110 48-hr

Menidia beryllina	115 96-hr

Mysidopsis bahia	105 48-hr

Menidia beryllina	1.14 96-hr

Mysidopsis bahia	0.98 48-hr

Surface Washing Agents

283

PETRO-CLEAN


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X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<0.10

<0.10

<0.01

<0.01

<0.002

<0.01

<0.01

<0.01

<2.0

<1.0

Surface Washing Agents

284

PETRO-CLEAN


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

8/17/2012
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-24

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JULY 14, 2000

"DO-ALL #18"

I.	NAME, BRAND, OR TRADEMARK
DO-ALL #18

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Radcob Solutions, Inc.

4800 North State Road 7, Suite #105
Lauderdale Lakes, FL 33319
Phone: (954) 249-2178
Fax: (954) 640-7080
Email: updated information required
Website: updated information required
(Mr. Adam Goldberg)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Radcob Solutions, Inc.

4800 North State Road 7, Suite #105
Lauderdale Lakes, FL 33319
Phone: (954) 249-2178
Fax: (954) 640-7080
Email: updated information required
Website: updated information required
(Mr. Adam Goldberg)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: DO-ALL #18 is water based, contains no solvents and is non-flammable.

2.	Ventilation: Normal room ventilation.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
skin, eyes, and clothing. Wear safety glasses or goggles and protective gloves when handling.
In case of eye contact, flush immediately with water for at least 15 minutes. If persistent
irritation occurs, call a physician. For skin contact, wash thoroughly with soap and water.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 100°F

Surface Washing Agents

285

DO-ALL# 18


-------
4.d. Temperatures of phase separations and chemical changes: DO-ALL #18 has a pour point of
32°F and phase separation occurs at 105°F.

V.	SHELF LIFE

DO-ALL #18 has a shelf life of at least two (2) years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: May be diluted with fresh or salt water. For general use, apply by spray,
mop, etc. Agitate severe spots, rinse thoroughly for residue-free surface.

2.	Concentration/Application Rate: To clean oil from beaches, rocks, and piers as a shore-line
cleaner, first use a pre-treatment or soaking, using one (1) part DO-ALL #18 diluted with three
(3) parts of water. Allow 30 to 45 minutes to soften viscous oil deposits (soak time may vary
with temperature, oil density, and degree of weathering). After the soaking period, dilute one (1)
part of DO-ALL #18 with 15 parts of water and apply with a high pressure water hose (50 - 100
PSI). Oil released can then be removed by vacuuming, skimmers, or absorbents.

For normal cleaning of shop machinery, bilges, decks, waterline scum, rigs, and platforms, dilute
one (1) part DO-ALL #18 with up to 20 parts of water.

For heavy cleaning and degreasing of tanks, barges, engine rooms and soot, oil stained concrete,
and petroleum based drilling muds, dilute one (1) part DO-ALL #18 with up to 15 parts of water.
For severe cleaning of holding tanks, grease traps, black magic, crude oil, and Bunker C, dilute
one (1) part DO-ALL #18 with up to five (5) parts of water.

For steam cleaning, dilute one (1) part of DO-ALL #18 with up to 50 parts of water.

For pressure washing, dilute one (1) part DO-ALL #18 with up to 30 parts of water.

DO NOT USE UNDILUTED ON COMPOSITION FLOORS, WATER-BASED PAINTED
SURFACES, OR ALUMINUM,

3.	Conditions for Use: Recommended for cleaning petroleum fractions from beaches, rocks,
piers, bilges, decks, waterline scum, rigs, platforms, tanks, barges, engine rooms, machinery,
holding tanks, and grease traps.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity
Material Tested
DO-ALL #18

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
66.10 96-hr
288.00 48-hr

No. 2 Fuel Oil

9.10 96-hr
0.65 48-hr
9.38 96-hr
0.57 48-hr
6.36 96-hr
16.53 48-hr

DO-ALL #18 & No. 2 Fuel Oil
(1:10)

Reference Toxicant (SDS)

Surface Washing Agents

286

DO-ALL# 18


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b. Effectiveness:
NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: 32°F

3.	Viscosity: 1.8 @ 68°F

4.	Specific Gravity: 1.07 @ 68°F

5.	pH:13.1

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Soluble with water.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND (<0.02)

Cadmium	ND (<0.02)

Chromium	ND (<0.02)

Copper	0.33

Lead	ND (<0.02)

Mercury	ND (<0.00)

Nickel	ND (<0.10)

Zinc	0.28

Cyanide	0.26

Chlorinated Hydrocarbons	ND (<0.30)

Surface Washing Agents

287

DO-ALL# 18


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TECHNICAL PRODUCT BULLETIN #SW-25

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JULY 9, 2001

"SC-1000®"

I.	NAME, BRAND, OR TRADEMARK
SC-1000®

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
GEMTEK® Products

4640 East Elwood Street

Phoenix, AZ 85040

Emergency Number: (602) 265-8586

Phone: (800)331-7022

Fax:(602)265-7241

E-mail: sarahkristoff@gemtek.com

(Ms. Sarah S. Kristoff)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
GEMTEK® Products

4640 East Elwood Street

Phoenix, AZ 85040

Emergency Number: (602) 265-8586

Phone: (800)331-7022

Fax:(602)265-7241

E-mail: sarahkristoff@gemtek.com

(Ms. Sarah S. Kristoff)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: General room ventilation is satisfactory.

3.Skin and eye contact; protective clothing; treatment in case of contact: Non-irritating, no first

aid needed. May be an eye irritant. Do not spray into eyes; safety glasses are recommended. If

irritation does occur, rinse thoroughly with water.

4.a. Maximum storage temperature: None.

4.b. Minimum storage temperature: Room temperature.

4.c. Optimum storage temperature range: 70°F to 90°F

4.d. Temperatures of phase separations and chemical changes: Low temperature can cause
handling problems; viscosity of material will increase. The product is an organic compound and
it will not typically stratify. The cloud point is 54°F. At 212°F it will boil and at somewhat less
(around 130°F) water vapor will form. Repeat freeze/thaw/boiling cycles over a 30-day period

Surface Washing Agents

288

SC-1000™


-------
has not demonstrated noticeable break down of the product.

V.	SHELF LIFE
Minimum of 5 years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: SC-1000® is a highly concentrated cleaning compound capable of a
multitude of cleaning applications with dilutions ranging from full strength to far in excess of

1:350. Depending on the specific factors in the cleaning environment, the desired cleaning speed
with the least amount of SC-1000® can be determined. When diluting, it is recommended that
SC-1000® be added to premeasured water to minimize foaming in the solution.

2.	Concentration/Application Rate: Beach Waterfront, Rocky Soils, Break Water Structures, and
Pier Facilities: For beach sands or light rocky soils, burning or creating a temporary shallow
wash tank is most successful. Fill one-half of the tank with contaminated beach sand, then add a
solution of SC-1000® and clean water (ocean or fresh) to cover the sand. Gentle agitation will
release the oil to the surface of the tank where it can be collected. For rocky surfaces spray with
a 20 percent solution of SC-1000® using a horizontal eductor sprayer, spraying side-to-side,
allowing the soil to dwell for several minutes before spraying top-to-bottom with clean ocean or
fresh water to rinse oil into perimeter oil booms, blankets or impermeable sheeting.

Washing Marine Vegetation - Use a non-pressure/impact spraying equipment to dispense a 0.01
percent SC-1000® solution and allow to stand for 5-10 minutes before a final rinsing with fresh
or ocean water. Washing Marine Equipment - For wet oils and bunker crude, use SC-1000™ at
20 percent solution (preferably warmer than 80°F) and spray or wipe. Apply directly to
equipment, allow to dwell for 1-2 minutes and then spray rinse with fresh or ocean water. For
hardened oils, fuels, and viscous lubricants, apply SC-1000® blended with SC-Supersolve™ (a
non-toxic, low aromatic, water miscible solvent) at the ratio of 80/20 then dilute with water to a
50 percent solution, spray or wipe onto surface, let stand for 1-2 minutes before rinsing.

Heavy Cleaning Examples - Dilution full strength 1:5; diesel engines, auto parts, baked on oil or
lube grease, dried oil/enamel, latex paints, thick food syrups, insect smears, dried animal or
vegetable fats, hard resins, thick dust-laden oily dirt, asphalt and grass or plant stains.

Average Cleaning Examples - Dilution 1:5 up to 1:20; automotive work counters and tools, food
and beverage processing equipment, oily or food-laden floors, manufacturing work areas, vehicle
maintenance, shipping containers, utility equipment, and parts washers. General Maintenance
Examples - 1:20 up to 1:100; vehicle washing, general janitorial for

offices/schools/hospitals/recreation and related equipment, pressure sprayers, food preparation
and storage, painted/plastic laminate surfaces, sports equipment, general cleaning, immersion
tanks, and ultrasonics.

3.	Conditions for Use: SC-1000® may be used on any surface that is compatible with water. The
product may tarnish some soft aluminum surfaces if not adequately diluted and rinsed with
water.

Surface Washing Agents

289

SC-1000™


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VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity

Material Tested	Species	LC50 (ppm)

SC-1000®	Menidia beryllina	26.40 96-hr

Mysidopsis bahia	15.20 48-hr

No. 2 Fuel Oil	Menidia beryllina	8.85 96-hr

Mysidopsis bahia	1.57 48-hr

SC-1000® & No. 2 Fuel Oil	Menidia beryllina	4.72 96-hr

Mysidopsis bahia	2.13 48-hr

Reference Toxicant (SDS)	Menidia beryllina	2.22 96-hr

Mysidopsis bahia	10.5 48-hr

b.	Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 25°F

3.	Viscosity: <10 cps @ 25°C

4.	Specific Gravity: 1.009

5.	pH: 10.2 - 10.5

6.	Surface Active Agents: CONFIDENTIAL.

7.	Solvents: None.

8.	Additives: CONFIDENTIAL.

9.	Solubility in Water: Soluble in water.

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	1.33

Cadmium	ND

Chromium	ND

Copper	0.100

Lead	ND

Mercury	ND

Nickel	ND

Zinc	0.20

Cyanide	ND

Chlorinated Hydrocarbons	ND

Surface Washing Agents

290

SC-1000™


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TECHNICAL PRODUCT BULLETIN #SW-26

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: AUGUST 06, 2001

"GOLD CREW SW"

I. NAME, BRAND, OR TRADEMARK
GOLD CREW SW

Type of Product: Surface Washing Agent

II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Gold Crew Products & Services, LLC
P.O. Box 12032
Orange, CA 92869
Phone: (714)288-8781
Mobile: (714)318-5997
E-mail: ifigueira@goldcrew.net
E-mail: ifigueira@ecschem.com
(Mr. Jim Figueira)

ECS

5713 Wollochet Drive NW, Suite B
Gig Harbor, WA 98332
Phone: (253) 263-8040
E-mail: egrubbs@ecschem.com
Website: www.ecschem.com
(Mr. Ed Grubbs)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Gold Crew Products & Services, LLC
P.O. Box 12032
Orange, CA 92869
Phone: (714)288-8781
Mobile: (714)318-5997
E-mail: i fi gueira@ gol dcrew. net
E-mail: ifigueira@ecschem.com
(Mr. Jim Figueira)

ECS

5713 Wollochet Drive NW, Suite B
Gig Harbor, WA 98332
Phone: (253) 263-8040
E-mail: egrubbs@ecschem.com
Website: www.ecschem.com
(Mr. Ed Grubbs)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Extensive testing
indicates that GOLD CREW SW is non-hazardous and non-toxic to humans; however, good
hygiene practices should always be followed as outlined below:

Eyes- flush with water; get medical attention if required; Skin - remove contaminated clothing,
wash exposed area, and wash clothing before use. If irritation develops get medical attention;
Ingestion - get medical attention if required; Inhalation - none considered necessary.

4.a.	Maximum storage temperature: When above 120°F, keep container closed and stored in a
cool dark place. Evaporation may change product's characteristics.

4.b. Minimum storage temperature: Product will freeze below 25°F. No phase separation will
occur. If frozen, thaw, and stir well.

Surface Washing Agents

291

GOLD CREW SW


-------
4.c. Optimum storage temperature range: 25°F to 120°F

4.d. Temperatures of phase separations and chemical changes: No separation at any temperature
between 32-120°F. No tendency to "layer out" or separate, standing for 30 days. No separation
of layering after freezing.

V.	SHELF LIFE

20 years (unopened).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply through hand pump sprayer and allow to soak.

2.	Concentration/Application Rate: As a presoak dilute 20 parts water to 1 part SW. For crude
oil, allow about 1 hour. For medium distillates, allow 30 minutes. For light distillates, allow 15
minutes. Time may vary depending on weather conditions. After allowing the solution to
presoak, wash the area in the following manner: Apply through a power washer or through a
steam powered unit at 1 percent, 3 percent, or 5 percent depending on oil viscosity and
temperature.

3.	Conditions for Use: Equally effective with salt or fresh water.

VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested
GOLD CREW SW

No. 2 Fuel Oil

GOLD CREW SW &

No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

b.	Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >200

2.	Pour Point: 25°F

3.	Viscosity: 33.87 CST

4.	Specific Gravity: 1.035

5.	pH: 9.76 +/- 0.01

6.	Surface Active Agents: CONFIDENTIAL.

7.	Solvents: None.

Species

LC50

ism.)

Menidia beryllina

13.80

96-hr

Mysidopsis bahia

20.40

48-hr

Menidia beryllina

6.75

96-hr

Mysidopsis bahia

2.82

48-hr

Menidia beryllina

6.34

96-hr

Mysidopsis bahia

2.70

48-hr

Menidia beryllina

2.22

96-hr

Mysidopsis bahia

9.52

48-hr

Surface Washing Agents

292

GOLD CREW SW


-------
8.	Additives: CONFIDENTIAL.

9.	Solubility in Water: Complete.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.0

Cadmium	<0.10

Chromium	<1.0

Copper	<1.0

Lead	<0.5

Mercury	<0.02

Nickel	<1.0

Zinc	0.44

Cyanide	ND

Chlorinated Hydrocarbons	ND

Surface Washing Agents

293

GOLD CREW SW


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TECHNICAL PRODUCT BULLETIN #SW-28

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 05, 2001

"NALE-IT"

I.	NAME, BRAND, OR TRADEMARK
NALE-IT

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
SPL Control LLC

P.O. Box 627
Elmore City, OK 73433
Phone: (580) 788-2187
E-mail: splcontrol@aol.com
(Mr. Tom Luster)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
SPL Control LLC

P.O. Box 627
Elmore City, OK 73433
Phone: (580) 788-2187
E-mail: splcontrol@aol.com
(Mr. Tom Luster)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Workers should be in well ventilated areas; if in a confined area, use a respirator.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Workers should wear
protective goggles or safety glasses. Prolonged contact with skin may result in dryness.

4.a.	Maximum storage temperature: NA
4.b. Minimum storage temperature: >32°F

4.c. Optimum storage temperature range: 40°F to 200°F

4.d. Temperatures of phase separations and chemical changes: No phase separation or hazardous
polymerization will occur.

V.	SHELF LIFE
Indefinite.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: NALE-IT may be applied using a pressure sprayer.

2.	Concentration/Application Rate: For pit closures, surface hydrocarbon spills, compressor

Surface Washing Agents

294

NALE-IT


-------
stations, pipeline and flow line leaks, well head and tank farm leaks, and highway spills,
(petroleum products) mix 1 part NALE-IT with 20 parts water.

3. Conditions for Use: Equally effective with fresh or salt water.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

NALE-IT

No. 2 Fuel Oil

NALE-IT & No. 2 Fuel Oil
(1:10)

Reference Toxicant (SDS)

b. Effectiveness:

NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 30°F

3.	Viscosity: 1.18

4.	Specific Gravity: 1.02

5.	pH: 6.8-7.2

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Soluble in fresh and sat water.

LC50 (ppm)

273.30	96-hr

69.00	48-hr

6.93	96-hr

2.29	48-hr

3.82	96-hr

1.84	48-hr
2.60 96-hr

8.56	48-hr

Surface Washing Agents

295

NALE-IT


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.82

ND

ND

0.173

ND

ND

ND

0.18

ND

ND

Surface Washing Agents

296

NALE-IT


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TECHNICAL PRODUCT BULLETIN #SW-30

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JULY 24, 2002

"F-500"

I.	NAME, BRAND, OR TRADEMARK
F-500

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Hazard Control Technologies, Inc.

150 Walter Way
Fayetteville, GA 30214
Phone: (770)719-5112
Fax: (770)719-5117
E-mail: egriffin@hct-world.com
(Ms. Esther Griffin)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Hazard Control Technologies, Inc.

150 Walter Way
Fayetteville, GA 30214
Phone: (770)719-5112
Fax: (770)719-5117
E-mail: egriffin@hct-world.com
(Ms. Esther Griffin)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Local exhaust - no special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Eye contact - may
cause eye irritation, flush with water. Wear splash proof protection goggles or full-face shield.
If irritation persists contact a physician. Skin contact - may cause mild irritation, flush with
water. Wear rubber and vinyl gloves and apron. Product has been tested and found to be non-
skin sensitizing per OECD 406. Ingestion - may cause gastrointestinal irritation. Drink plenty
of water to dilute. Do not induce vomiting. If irritation persists contact a physician. Inhalation
- elevated temperature vapors may cause irritation to respiratory tract. Remove to fresh air.

4.a.	Maximum storage temperature: 130°F
4.b. Minimum storage temperature: 17°F

4.c. Optimum storage temperature range: 35°F - 130°F

4.d. Temperatures of phase separations and chemical changes: NA

Surface Washing Agents

297

F-500


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V.	SHELF LIFE

The shelf life is 15 years when stored between 35°F - 130°F in unopened containers.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Standard fire apparatus spray nozzle with agitation onto and into spill.

2.	Concentration/Application Rate: 1 part F-500:8 parts hydrocarbon:32 parts water (fresh or
salt).

3.	Conditions for Use: Water temperature: 33°F - 211°F. Effective on both polar and non-polar
hydrocarbons

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

F-500

No. 2 Fuel Oil

F-500 & No. 2 Fuel Oil
(1:10)

Reference Toxicant (DSS)

b. Effectiveness:

NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
<10.00 96-hr
32.00 48-hr
56.00 96-hr
100.00 48-hr
<10.00 96-hr
32.00 48-hr
1.14 96-hr
0.98 48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: -17°F

3.	Viscosity: 54-56 centistokes @ 72°F

4.	Specific Gravity: 0.99 g/cc @ 72°F

5.	pH: 7.00

6.	Surface Active Agents: PROPRIETARY/CONFIDENTIAL

7.	Solvents: None

8.	Additives: None

9.	Solubility in Water: Complete

Surface Washing Agents

298

F-500


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<0.03

<0.01

<0.01

<0.05

<0.025

<0.005

<0.02

<0.07

<0.02

<0.10

Surface Washing Agents

299

F-500


-------
TECHNICAL PRODUCT BULLETIN #SW-31

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: OCTOBER 27, 2003

"ENVIROCLEAN"

I.	NAME, BRAND, OR TRADEMARK
ENVIROCLEAN

Type of Product: Surface Washing Agent
(formerly ENVIRO CLEAN 165)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Blind Gate Holdings, LLC

14 Largo Woods Place

The Woodlands, TX 77382

Phone: (281)216-6363

E-mail: igibson@evergreenchems.com

E-mail: mgibson@ever greenchems.com

Website: www, ever greenchem s. com

(Mr. Jonathan Gibson)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Evergreen Chemical Solutions, LLC

6700 Woodlands Parkway, Suite 230-250

Spring, TX 77382

Phone: 281-216-6363

E-mail: igibson@evergreenchems.com

Website: www, ever greenchem s. com

(Mr. Jonathan Gibson)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Use good normal
hygiene and avoid contact with skin and eyes. Gloves and goggles are recommended for field
application and product handling. If contact with eyes flush with water for 15 minutes and seek
medical attention. For contact with skin, wash area with soap and water. May cause redness,
edema, and drying of skin. Seek medical attention if irritation develops. In case of ingestion,
seek medical attention. Not considered an inhalation risk.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 28°F

4.c. Optimum storage temperature range: 30°F - 120°F

4.d. Temperatures of phase separations and chemical changes: Temperature fluctuations will not

Surface Washing Agents

300

ENVIROCLEAN


-------
cause separation or deterioration of product. Product blend is stable and will not undergo phase
separation of ingredients or stratification of contents over time.

V.	SHELF LIFE
Unlimited if unopened.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Dilute product with water prior to use. Apply product via manual
pressure applicator (i.e., hand pump), or other delivery equipment, to impacted surfaces. Allow
product to soak prior to rinse/recovery if heavily saturated with oil. On hard surfaces, product
may be applied and agitated with a brush or other physical means prior to recovery of effluent.
Product may also be pre-mixed and used in a batch tank or through an eduction/metering system
for flushing and recovery operations.

2.	Concentration/Application Rate: ENVIROCLEAN is a concentrated product and must be
diluted prior to use. Concentrations vary based upon type of oil and degree of surface saturation.
For light ends (i.e., gas condensate/gasoline) a 1% - 2% solution may be used to flush area to
containment. (A higher concentration solution of 6% should be used if flammable vapor
presents an explosion hazard.) For lighter oils (i.e., No. 2 Fuel Oil) a 3% solution may be used to
flush impacted areas to containment. For heavy ends (i.e., crude oil/No. 6 Fuel Oil) a 6%
solution of ENVIROCLEAN should be applied and allowed to soak into containment/substrate
for up to an hour to allow for release of oil. The surface should then be flushed to containment
with a 1% - 3% solution of ENVIROCLEAN. Product may be used as noted above through any
pressure or steam equipment. The use of a "hot" unit is recommended when oils are at low
temperature or have been weathered.

3.	Conditions for Use: ENVIROCLEAN may be diluted with hard, soft, brackish, salt, or most
waters of sufficient quality for operations.

Surface Washing Agents

301

ENVIROCLEAN


-------
VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

ENVIROCLEAN

Menidia beryllina

27.80 96-hr



Mysidopsis bahia

22.60 48 hr

No. 2 Fuel Oil

Menidia beryllina

8.77 96-hr



Mysidopsis bahia

1.53 48-hr

ENVIROCLEAN&





No. 2 Fuel Oil (1:10)

Menidia beryllina

8.13 96-hr



Mysidopsis bahia

1.76 48 hr

Reference Toxicant (DSS)

Menidia beryllina

1.83 96-hr



Mysidopsis bahia

3.37 48 hr

b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: 28.8°F

3.	Viscosity: 9 Centipose

4.	Specific Gravity: 1.028

5.	pH: 8.63

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Complete

X.	ANALYSIS FOR HEAVY METALS, CYANIDE,
HYDROCARBONS

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

AND CHLORINATED

Concentration (ppm)

<0.002

<0.001

<0.005

<0.002

<0.005

<0.0002

<0.005

<0.002

<0.1

<0.05

Surface Washing Agents

302

ENVIROCLEAN


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LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-32
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JULY 21, 2006
"BG-CLEAN™ 401"

I.	NAME, BRAND, OR TRADEMARK
BG-CLEAN™ 401

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Amiran BioChemicals, LLC

7221 South 10th Street
Oak Creek, WI 53154
Phone: updated information required
Fax: updated information required
(Dr. Mohsen Amiran)

Phone: updated information required
Fax: updated information required
E-mail: updated information required
(Mr. Sherwin Amiran)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Amiran BioChemicals, LLC

7221 South 10th Street
Oak Creek, WI 53154
Phone: updated information required
Fax: updated information required
(Dr. Mohsen Amiran)

BioCenter, Inc.

P.O. Box 170498
Milwaukee, WI 53217
Phone: (414) 768-7100
Fax: (414)768-7106
E-mail: skelling@aol.com
(Mr. Scott Kelling)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1. Flammability: BG-CLEAN™ 401 is not classified as flammable by either USDOT or IMO
regulations.

3/09/2016
7/27/2022

Surface Washing Agents

303

BG-CLEAN™ 401


-------
2.	Ventilation: Avoid prolonged breathing of vapors.

3.	Skin and eye contact; protective clothing; treatment in case of contact:

BG-CLEAN™ 401 is an organic compound with a slightly alkaline pH. No extraordinary
precautions are required during handling. Avoid unnecessary contact with skin or eyes. No
special protective clothing is required. Body areas exposed to BG-CLEAN™ 401 may be
flushed with water to clean off the chemical.

4.a.	Maximum storage temperature: 180°F
4.b. Minimum storage temperature: -25°F
4.c. Optimum storage temperature range: 68°F

4.d. Temperatures of phase separations and chemical changes: BG-CLEAN™ 401 is not
adversely affected by changes in storage temperature unless evaporation is allowed to occur.
Phase separation does not occur when the product is stored in below freezing conditions. BG-
CLEAN™ 401 is ready for use as soon as it is rewarmed to approximately 34-40°F. Product will
expand when frozen.

V.	SHELF LIFE

The shelf life of unopened containers of BG-CLEAN™ 401 is unlimited. Containers should
always be capped when not in use to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: BG-CLEAN™ 401 is applied by one of two methods. 1) For situations
where cleanup starts shortly after contamination and the oil has not yet weathered, use a high
pressure spray. BG-CLEAN™ 401 is proportioned into a stream of water and sprayed directly
on the surface to be cleaned at a rate of 60-70 gpm. 2) For difficult cleaning situations such as
weathered crude oil on a rocky beach, a three step procedure should be used. First presoak the
contaminated area by proportioning BG-CLEAN™ 401 into a low pressure stream of water at a
rate of about 20 gpm. Allow the spray to soak for 15-30 minutes. Then proportion BG-
CLEAN™ 401 into a high pressure water stream and apply at a rate of 60-70 gpm. Selection of
the best procedure depends on site conditions. BG-CLEAN™ 401 effectiveness is increased
when applied with water heated to between 100°F and 180°F. As ambient temperature
decreases, the benefits of applying heated spray increase.

The efficiency of BG-CLEAN™ 401 depends directly on mixing of the BG-CLEAN™ 401
molecules with the hydrocarbon molecules. Given good mixing, BG-CLEAN™ 401 can be used
on all hydrocarbons except asphalt.

2.	Concentration/Application Rate: Dilute BG-CLEAN™ 401 water. The amount of spray
required varies with the amount of oil. Concentrations ranging from 5:1 to 100:1 have been
found useful depending on hydrocarbon concentrations and viscosity. During application, adjust
the concentration of BG-CLEAN™ 401 to suit the cleaning effect desired.

3.	Conditions for Use: BG-CLEAN™ 401 is recommended as a cleaner for piers, seawalls,
pilings, ship's hulls, and rocky beaches. It can be used on metal, wood, and plastics. BG-
CLEAN™ 401 is also highly useful for cleaning contaminated solids such as soil. This includes
a range from normal soil aggregate to 100% sand. Two conditions are required for maximum
cleaning; thorough mixing of BG-CLEAN™ 401 with the oil and an adequate concentration of

Surface Washing Agents

304

BG-CLEAN™ 401


-------
BG-CLEAN™ 401.

VII. TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested
BG-CLEAN™ 401

No. 2 Fuel Oil

BG-CLEAN™ 401
No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

b.	Effectiveness:

NA

Species

LC50 (ppm)

Menidia beryllina

787.

.00

96-hr

Mysidopsis bahia

477.

.00

48-hr

Menidia beryllina

16.

.90

96-hr

Mysidopsis bahia

2.

.92

48-hr

Menidia beryllina

13.

.10

96-hr

Mysidopsis bahia

2.

.86

48-hr

Menidia beryllina

3.

.93

96-hr

Mysidopsis bahia

8.

.80

48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM D-93: >76.6°C (>170°F)

2.	Pour Point, ASTM D-97: -4°C

3.	Viscosity, ASTMD-88: 24 SUS@ 100°F

4.	Specific Gravity, ASTM D-1298: 1.00604 @ 60°F

5.	pH: 8.227

6.	Surface Active Agents: Proprietary

7.	Solvents: Proprietary

8.	Additives: Proprietary

9.	Solubility: Miscible in water.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.118

Cadmium	<0.020

Chromium	<0.125

Copper	0.049

Lead	0.166

Mercury	<0.02

Nickel	<0.125

Zinc	0.280

Cyanide	0.002

Chlorinated Hydrocarbons	ND

Surface Washing Agents

305

BG-CLEAN™ 401


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

7/15/2021
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-33

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 27, 2006

"E-SAFE®"

I.	NAME, BRAND, OR TRADEMARK
E-SAFE®

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
PLUTUS Environmental Technologies, Inc.

3138 Hatcher Mountain Road
300 John L Marshall Drive
Sevierville, TN 37862-8323
Phone: (865)214-0350
E-mail: plutusceo@mail.com
(Mr. James Hatcher)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
PLUTUS Environmental Technologies, Inc.

3138 Hatcher Mountain Road
300 John L Marshall Drive
Sevierville, TN 37862-8323
Phone: (865)214-0350
E-mail: plutusceo@mail.com
(Mr. James Hatcher)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable until >170°F

2.	Ventilation: Handle in a well-ventilated space. Local exhaust is recommended if TLV's are
exceeded.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye and
(sensitive) skin contact. In case of contact, immediately flush with large amount of cool water of
at least 5 minutes. Wear protective eye goggles when using any chemicals. Impermeable
protective gloves are recommended for sensitive skin types. Protective clothing is not required.
Rinse contaminated clothing, shoes, goggles, and gloves in simple tap water to remove any
chemical residue. Avoid ingestion, breathing dusts, mists, or fumes. In case of ingestion drink
several glasses of water. Do not induce vomiting. In case of inhalation, move affected person to
fresh air.

4.a.	Maximum storage temperature: 160°F

Surface Washing Agents

306

E-SAFE®


-------
4.b. Minimum storage temperature: -15°F

4.c. Optimum storage temperature range: 40°F - 110°F

4.d. Temperatures of phase separations and chemical changes: No phase separations will occur.
Continued exposure to direct sunlight may cause a change in color, but performance is not
affected.

V.	SHELF LIFE

Unlimited if left in unopened containers stored at 40°F - 110°F and away from direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: E-SAFE® may be introduced with a pressure spray to cover the affected
area. The contaminated area should be thoroughly moistened. Following the spray application
the treated area should be soaked with water to facilitate penetration. Heavy soil such as clay
will be cleaned by E-SAFE®, but tilling or aerating the soil will rapidly shorten penetration time.
Sand or loam ay require heavy dosage with E-SAFE® because hydrocarbon migration is so rapid
in these soil types. Treatment of fouled beach areas should have E-SAFE® sprayed on all
contaminated surfaces. Any remaining hydrocarbons may then be effectively vacuumed or
wiped away from the treated surfaces. Incidental wave action or rainfall will enhance coverage
and penetration by E-SAFE®.

2.	Concentration/Application Rate: E-SAFE® should be applied full strength. Beginning
treatment for hydrocarbon contaminated surface is one gallon of E-SAFE® per 100 square foot of
surface area. This dosage is recommended when the ambient temperature is 72°F and humidity
is moderate. Higher temperature or lower humidity will increase the need for repeated
applications or a higher volume of E-SAFE® per application.

3.	Conditions for Use: E-SAFE® works on all soil types and weather conditions that allow
hydrocarbon penetration. E-SAFE® follows the same path, channel, or gradient as the
contaminant. When visible detection reveals that E-SAFE® has been absorbed by, or has
penetrated the soil, water should be applied to the site. E-SAFE® is soluble in water and also
breaks the surface tension of the transporting water molecules.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:
Material Tested
E-SAFE®

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)

329.00	96-hr

257.00	48-hr

5.45	96-hr

10.20	48-hr

8.77	96-hr

14.20	48-hr

8.07	96-hr

16.00	48-hr

No. 2 Fuel Oil

E-SAFE®

No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

b. Effectiveness:
NA

Surface Washing Agents

307

E-SAFE®


-------
VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM D-93: >170°F

2.	Pour Point, ASTM D-97: -27°C

3.	Viscosity, ASTMD-88: 11SFS@ 100°F

4.	Specific Gravity, ASTM D-1298: 1.0118 @ 60°F

5.	pH: 8.04

6.	Surface Active Agents: Confidential

7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility: Soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.005

Cadmium	<0.0008

Chromium	<0.025

Copper	0.061

Lead	0.082

Mercury	<0.007

Nickel	<0.003

Zinc	0.214

Cyanide	0.200

Chlorinated Hydrocarbons	ND

Surface Washing Agents

308

E-SAFE®


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

7/15/2021
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-34

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 27, 2006

"SHEEN-MAGIC®"

I.	NAME, BRAND, OR TRADEMARK
SHEEN-MAGIC®

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
PLUTUS Environmental Technologies, Inc.

3138 Hatcher Mountain Road
300 John L Marshall Drive
Sevierville, TN 37862-8323
Phone: (865)214-0350
E-mail: plutusceo@mail.com
(Mr. James Hatcher)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
PLUTUS Environmental Technologies, Inc.

3138 Hatcher Mountain Road
300 John L Marshall Drive
Sevierville, TN 37862-8323
Phone: (865)214-0350
E-mail: plutusceo@mail.com
(Mr. James Hatcher)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable until >170°F

2.	Ventilation: Handle in a well-ventilated space. Local exhaust is recommended if TLV's are
exceeded.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye and
(sensitive) skin contact. In case of contact, immediately flush with large amount of cool water of
at least 5 minutes. Wear protective eye goggles when using any chemicals. Impermeable
protective gloves are recommended for sensitive skin types. Protective clothing is not required.
Rinse contaminated clothing, shoes, goggles, and gloves in simple tap water to remove any
chemical residue. Avoid ingestion, breathing dusts, mists, or fumes. In case of ingestion drink
several glasses of water. Do not induce vomiting. In case of inhalation, move affected person to
fresh air.

4.a.	Maximum storage temperature: 160°F

Surface Washing Agents

309

SHEEN-MAGIC®


-------
4.b. Minimum storage temperature: -8°F

4.c. Optimum storage temperature range: 40°F - 110°F

4.d. Temperatures of phase separations and chemical changes: No phase separations will occur.

V.	SHELF LIFE

Unlimited if left in unopened containers stored at 40°F - 110°F and away from direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: SHEEN-MAGIC® recommended treatment is light misting of
contaminated surface. Heavier hydrocarbons such as crude oil should be boomed or vacuumed
away as much as possible before application of the SHEENMAGIC®. Treatment of fouled beach
areas should have SHEEN-MAGIC® sprayed on all contaminated surfaces. Incidental wave
action or rainfall will enhance coverage and penetration by SHEEN-MAGIC®. Any remaining
hydrocarbons may then be effectively vacuumed or wiped away from the treated surfaces.

Aerial application should be delivered at height and air speed that will create air shear necessary
to deliver droplets as per nozzle manufacturer's recommendations. Mist spray from surface
vehicles may be delivered from power fogger units. Hand sprayers are generally used for small
treatment areas.

2.	Concentration/Application Rate: One ounce per 50 square yards of surface is the normal
treatment for diesel spills. Heavier hydrocarbon sheens may require additional treatment to
remove the contaminant.

3.	Conditions for Use: SHEEN-MAGIC® works in all weather conditions that allow hydrocarbon
penetration. SHEEN-MAGIC® should be used as soon as the temperature and weather
conditions allow delivery to the spill area. Heavier concentrations may be required when the
temperature/humidity will cause rapid evaporation of the spray.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

SHEEN-MAGIC®

Menidia beryllina

183.00 96-hr



Mysidopsis bahia

161.00 48-hr

No. 2 Fuel Oil

Menidia beryllina

4.57 96-hr



Mysidopsis bahia

3.04 48-hr

SHEEN-MAGIC®

Menidia beryllina

7.82 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

5.75 48-hr

Reference Toxicant (SDS)

Menidia beryllina

11.70 96-hr



Mysidopsis bahia

5.36 48-hr

b. Effectiveness:

NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

310

SHEEN-MAGIC®


-------
IX. PHYSICAL PROPERTIES

1.	Flash Point, ASTM D-93: >170°F

2.	Pour Point, ASTM D-97: -22°C

3.	Viscosity, ASTMD-88: 11SFS@ 100°F

4.	Specific Gravity, ASTM D-1298: 1.0127 @ 60°F

5.	pH: 8.10

6.	Surface Active Agents: Confidential

7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility: Soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.005

Cadmium	<0.0008

Chromium	0.026

Copper	0.023

Lead	0.085

Mercury	<0.007

Nickel	<0.003

Zinc	0.231

Cyanide	0.200

Chlorinated Hydrocarbons	ND

Surface Washing Agents

311

SHEEN-


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-35
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
LISTING DATE: JUNE 16, 2008
"PROCLEANS"

I.	NAME, BRAND, OR TRADEMARK
PROCLEANS

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Eximco International, Inc.

5250 Gulfton, #2-B
Houston, TX 77081
Phone: updated information required
E-mail: updated information required
(Mr. Nat Brown)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Eximco International, Inc.

5250 Gulfton, #2-B

Houston, TX 77081

Phone: updated information required

E-mail: updated information required

E-mail:

(Mr. Nat Brown)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Flush contaminated
eyes thoroughly with water for 15 minutes, and get medical attention. Remove contaminated
clothing, wash exposed area with soap and water, and wash clothing before use. Get medical
attention if irritation develops. Get medical attention if ingested. No medical attention is
necessary if inhaled.

4.a.	Maximum storage temperature: 130°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 50°F to 100°F

4.d. Temperatures of phase separations and chemical changes: NA

3/16/2016
7/27/2022

Surface Washing Agents

312

PROCLEANS


-------
V.	SHELF LIFE

Approximately 2 years at recommended temperatures if unopened.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Apply specified dilute solution using fire hoses or heated pressure
washers onto the contaminated solid surface of the spill.

2.	Concentration/Application Rate: Use ten parts water to one part product. Dilution rates may
be adjusted to suit different job conditions. Apply 10 to 15 gallons of diluted PROCLEANS to
one cubic yard of contamination.

3.	Conditions for Use: May be used with fresh or salt water. Warmer temperatures may improve
results. Most effective if used on solid surfaces such as shoreline beaches and rocks
contaminated with light and medium weight crude oils and refined petroleum products.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

PROCLEANS

Menidia beryllina

83.73 96-hr



Mysidopsis bahia

83.98 48-hr

No. 2 Fuel Oil

Menidia beryllina

7.41 96-hr



Mysidopsis bahia

11.68 48-hr

PROCLEANS &

Menidia beryllina

4.78 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

11.68 48-hr

Reference Toxicant (CuS04)

Menidia beryllina

0.73 96-hr



Mysidopsis bahia

0.77 48-hr

b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >186°F

2.	Pour Point: 34.6°F

3.	Viscosity: 2.41 cST @ 104°F

4.	Specific Gravity: 1.01 @ 25°C

5.	pH: 6.8

6.	Surface Active Agents: Anionic and nonionic

7.	Solvents: None.

8.	Additives: None

9.	Solubility in Water: NA

Surface Washing Agents

313

PROCLEANS


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.690

ND

ND

ND

ND

ND

ND

0.738

ND

ND

Surface Washing Agents

314

PROCLEANS


-------
TECHNICAL PRODUCT BULLETIN #SW-36

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 30, 2009

"SPILLCLEAN"

SPILLCLEAN ["Concentrate"]

(aka, FIREMAN'S BRAND SPILLCLEAN)

I.	NAME, BRAND, OR TRADEMARK
SPILLCLEAN

SPILLCLEAN ["Concentrate"] = 30% Active Ingredients and 70% Water
(aka, FIREMAN'S BRAND SPILLCLEAN)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Super Sat Ventures, Inc.

S96 W34577 Jericho Drive
Eagle, WI 53119
Phone: (414) 840-9223
E-mail: dwk@ssvinc.com
(Mr. Daniel W. Klein)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Super Sat Ventures, Inc.

S96 W34577 Jericho Drive
Eagle, WI 53119
Phone: (414) 840-9223
E-mail: dwk@ssvinc.com
(Mr. Daniel W. Klein)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: >210°F

2.	Ventilation: General room ventilation is expected to be satisfactory.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Product may cause
mild skin irritation. Wear impervious gloves, safety goggles, and full cover clothes. Eye wash
and safety shower should be accessible. If eye contact, flush immediately with water for at least
15 minutes. If skin contact, wash with soap and water. If swallowed, give two glasses of water
(do not induce vomiting). Seek medical attention for eye and skin contact and ingestion.

4.a.	Maximum storage temperature: <210°F
4.b. Minimum storage temperature: >32°F

4.c. Optimum storage temperature range: 50°F - 70°F

4.d. Temperatures of phase separations and chemical changes: <32°F and >210°F

Surface Washing Agents

315	SPILLCLEAN [CONCENTRATE]


-------
V.	SHELF LIFE

3 years. Avoid extreme heat and store in a dry, cool area.

VI.	RECOMMENDED APPLICATION PROCEDURES
Please note:

SPILLCLEAN comes in two forms "Concentrate" and "Original Formula." SPILLCLEAN
["Concentrate"] is 30% Active Ingredients and 70% Water while SPILLCLEAN ["Original
Formula"] is 10% Active Ingredients and 90% Water.

SPILLCLEAN ["Concentrate"] and SPILLCLEAN ["Original Formula"] are for on land and
surface use only. They should not be used around or near bodies of water when there is a
reasonable chance of mixing in with water. Once the contaminant/SPILLCLEAN
["Concentrate"] solution mixes with the body of water, "control" of the contaminant will be lost
since SPILLCLEAN is water soluble.

SPILLCLEAN is a formula designed to solubilize and emulsify oil and oil-type products such as
motor oil, gasoline, diesel fuel, and transmission fluid. When such products are accidentally
spilled and need to be cleaned up from hard surfaces such as streets and driveways,
SPILLCLEAN is an effective material to use. Being a surfactant-type material, SPILLCLEAN
allows the spilled contaminant to be emulsified and then lifted and separated from the hard
surface. The resulting spill/contaminant can then be picked up, vacuumed up, or flushed with
water, all in accordance with federal, state, and local regulations.

1. Application Method: SPILLCLEAN ["Concentrate"] 30% Active Ingredients and 70% Water
- squeeze product directly around outside perimeter of oil/gasoline/antifreeze spill using squeeze
bottle container. This process is designed to "contain" the contaminant and keep if from
migrating down a hard surface like a city street, parking lot, or garage floor. SPILLCLEAN
["Concentrate"] is more viscous than oil/gasoline, and will "hold" the contaminant in place.

Once the contaminant is contained, the user can apply SPILLCLEAN ["Original Formula"] over
the "body" of the contaminant if the spill is large (over 2 gallons). If the spill is small (less than
2 gallons), the user can apply either SPILLCLEAN ["Concentrate"] or SPILLCLEAN ["Original
Formula"] to the "body" of the contaminant spill. Using a broom or broom-like applicator,
sweep SPILLCLEAN in with the contaminant until thoroughly blended in place. The original
bright red color of SPILLCLEAN ["Concentrate"] and SPILLCLEAN ["Original Formula"] will
dissipate when it is thoroughly mixed with the contaminant.

SPILLCLEAN ["Original Formula"] 10%) Active Ingredients and 90%) Water - apply over the
"body" of the contaminant if the spill is large (over 2 gallons). If the spill is small (less than 2
gallons), the user can apply SPILLCLEAN ["Concentrate"] or SPILLCLEAN ["Original
Formula"] to the "body" of the contaminant spill. SPILLCLEAN ["Original Formula"] is
designed to "attach" to a contaminant and remove it from a hard surface like a city street, parking
lot, or garage floor. It is recommended to be used on any size contaminant spill, large or small.
This product is designed to penetrate into the surface pores and molecularly "attach" with the
contaminant, thus making the contaminant "water soluble." The contaminant can be removed

Surface Washing Agents

316	SPILLCLEAN [CONCENTRATE]


-------
from the pores (of the asphalt, concrete, epoxy surface, etc.) with a 60psi water supply. The user
can then dispose of the resulting mixture according to regulations. This product can be applied
using a vast number of different applicators, especially with regard to firefighting equipment.
Using a broom or broom-like applicator, sweep SPILLCLEAN in with the contaminant until
thoroughly blended in place. The original bright red color of SPILLCLEAN ["Concentrate"] and
SPILLCLEAN ["Original Formula"] will dissipate when it is thoroughly mixed with the
contaminant.

When SPILLCLEAN'S bright red color has dissipated (upon mixing) with the contaminant, it
can be wiped clean with a rag or wet-vacuumed, collected, and disposed of according to EPA,
federal, state, and local regulations. Additionally, a dry sorbent may be applied to the resulting
SPILLCLEAN/contaminant/water mixture, shoveled up and disposed of according to applicable
regulations.

2.	Concentration/Application Rate: For Surface and Land Application Only:

SPILLCLEAN ["Concentrate"] 30% Active Ingredients and 70% Water - for spills less than 2
gallons squeeze a one-half inch ribbon of straight product around the perimeter of the
oil/gasoline spill, followed by an "X" pattern over the body of the spill. For spills greater than 2
gallons squeeze a one-half inch ribbon of straight product around the perimeter of the
oil/gasoline spill. The general purpose of SPILLCLEAN ["Concentrate"] is to "contain" the
contaminant from migrating, and therefore should not be diluted with water during application.

SPILLCLEAN ["Original Formula"] 10% Active Ingredients and 90% Water - concentration
rate is based on equipment used and disposal method. Typical usage will be (0 to 100 parts
water) plus 1 part SPILLCLEAN ["Original Formula"] all applied to 1 part contaminant
(oil/gasoline spill).

The resulting mixture of SPILLCLEAN and oil must be disposed of in accordance with EPA,
federal, state, and local agencies that regulate disposal of contaminant. The resulting
SPILLCLEAN contaminant mixture should be wet-vacuumed up and placed in a proper
container and disposed.

3.	Conditions for Use:

Water Salinity: Water soluble, not applicable for use on water
Water Temperature: >32°F and <120°F

Types of Pollutants: Automobile motor oil, gasoline, diesel fuel, and transmission fluid
Ages of Pollutants: 0 to 20 years old

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested	Species	LC50 (ppm)

SPILLCLEAN ["Concentrate"]	Menidia beryllina	24.30 96-hr

Mysidopsis bahia	10.00 48-hr

Surface Washing Agents

317	SPILLCLEAN [CONCENTRATE]


-------
No. 2 Fuel Oil

SPILLCLEAN ["Concentrate"] &
No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

6.60 96-hr
2.20 48-hr
3.30 96-hr
1.30 48-hr
8.90 96-hr
10.70 48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: SPILLCLEAN ["Concentrate"] = >210°F

2.	Pour Point: SPILLCLEAN ["Concentrate"] = 27.0°F

3.	Viscosity: SPILLCLEAN ["Concentrate"] = 6400cPs@25°C

4.	Specific Gravity: SPILLCLEAN ["Concentrate"] = 1.030

5.	pH: SPILLCLEAN ["Concentrate"] = 7.20

6.	Surface Active Agents: Confidential

7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility: Water soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS
Compound
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Zinc
Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.02

<0.007

<0.01

<0.01

<0.02

<0.00003

<0.01

<0.01

0.137

<0.01

Surface Washing Agents

318	SPILLCLEAN [CONCENTRATE]


-------
TECHNICAL PRODUCT BULLETIN #SW-37

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MARCH 15, 2010

"TXCHEM HE-1000™"

I.	NAME, BRAND, OR TRADEMARK
TXCHEM HE-1000™

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Texas EnviroChem, Inc.

17890 Airfield Lane
Pearland, TX 77581
Phone: (713) 806-4099
(Mr. Pete Franks)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Texas EnviroChem, Inc.

17890 Airfield Lane
Pearland, TX 77581
Phone: (713) 806-4099
(Mr. Pete Franks)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Not flammable

2.	Ventilation: Recommended, respirator in confined area

3.	Skin and eye contact; protective clothing; treatment in case of contact:

Wear rubber gloves and eye protection. If eye contact, wash eyes thoroughly for 15 minutes;
including upper and lowers lids, and seek medical attention. For skin contact, irritation is
possible, wash with soap and water for 15 minutes. If irritation persists, seek medical attention.

4.a.	Maximum storage temperature: 95°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 75°F

4.d. Temperatures of phase separations and chemical changes: No phase changes have been
observed.

V.	SHELF LIFE

One year in a sealed container.

VI.	RECOMMENDED APPLICATION PROCEDURES

1. Application Method: TXCHEM HE-1000™ is applied by pressure sprayer, heated pressure
washer, fire hoses or mixing on or into hydrocarbon contaminated media.

Surface Washing Agents

319

TXCHEM HE-1000™


-------
2.	Concentration/Application Rate: TXCHEM HE-1000™ should be diluted to a one (1) part
concentrated chemical to ten (10) parts water solution. Apply ten to fifteen gallons of diluted
solution to one cubic yard of contaminated media. Agitate to slurry. Dilution rate may change
due to level of hydrocarbon contamination. Please see manufacturer's instructions for additional
application dilutions. Excess washing solution should be disposed of according to local, state,
and federal regulations.

3.	Conditions for Use: Pollutants should be of hydrocarbon in nature. Greater results occur at
ambient temperatures greater than 50°F. Fresh or salt water can be used with no performance
change.

VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

TXCHEM HE-1000™

Menidia beryllina

91.33 96-hr



Mysidopsis bahia

65.52 48-hr

No. 2 Fuel Oil

Menidia beryllina

5.84 96-hr



Mysidopsis bahia

2.17 48-hr

TXCHEM HE-1000™ &

Menidia beryllina

7.07 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.11 48-hr

Reference Toxicant (SLS)

Menidia beryllina

15.27 96-hr



Mysidopsis bahia

12.84 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >210°F

2.	Pour Point: 23.0°F

3.	Viscosity: 1.99cSt

4.	Specific Gravity: 0.999

5.	pH: 7.20

6.	Surface Active Agents: Confidential

7.	Solvents: NA

8.	Additives: Confidential

9.	Solubility: NA

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED

HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.0366

Surface Washing Agents	320 TXCHEM HE-1000™


-------
Copper	0.0402

Lead	0.0189

Mercury	ND

Nickel	0.0125

Zinc	0.29

Cyanide	<0.05

Chlorinated Hydrocarbons	ND

Surface Washing Agents

321

TXCHEM HE-1000™


-------
TECHNICAL PRODUCT BULLETIN #SW-38

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MAY 11, 2010

"NOKOMIS 5-W"

I.	NAME, BRAND, OR TRADEMARK
NOKOMIS 5-W

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax: (510) 782-2032

E-mail: marlensupply@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Mar-Len Supply, Inc.

23159 Kidder Street

Hayward, CA 94545

Phone: (510) 782-3555

Fax:(510)782-2032

E-mail: marlensupplv@vahoo.com

(Mrs. Shirley Winter or Mr. Curt Winter)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (water based)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of eye contact,
flush with water; in case of skin contact, wash with water; and, if swallowed drink water to dilute
and induce vomiting.

4.a.	Maximum storage temperature: 212°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 50°F

4.d. Temperatures of phase separations and chemical changes: NA

V.	SHELF LIFE

15 years or more if stored correctly in plastic drums.

VI.	RECOMMENDED APPLICATION PROCEDURES

1. Application Method: NOKOMIS 5-W is a concentrated liquid, non-hazardous cleaner. Can be

Surface Washing Agents

322

NOKOMIS 5-W


-------
used full strength or diluted with fresh or salt water. NOKOMIS 5-W is marketed in plastic
containers.

2.	Concentration/Application Rate: Dilution ratios are determined by the individual cleaning
application. For washing equipment contaminated with soluble crude and/or bunker fuel oil use a
5:1 cleaning solution. Spray or brush onto surface, agitate with a stiff bristle brush, and rinse
with fresh or salt water. For pressure washing, pre-spray surface with concentrate and allow to
dwell on surface one to ten minutes (depending on age of oil). For shoreline areas and beaches
with rocky, breakwaters contain the area of beach sand and gravel by creating a sand bather
around a small contaminated area. Spray contaminated area with a 10:1 solution. Add salt or
freshwater, agitate surface to help release oil from sand. Allow time for oil to surface and recover
oil. To clean larger tidal rock surfaces, apply 5:1 or 20 percent mixture of NOKOMIS 5-W.

Spray solution onto rocks with a garden type pump sprayer. Agitate with a stiff bristle brush.
Allow to dwell on surface until surface looks soluble. Contain with a boom or use oil absorbent
pads to recover oil.

3.	Conditions for Use: Fresh or salt water can be used.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

NOKOMIS 5-W

No. 2 Fuel Oil

NOKOMIS 5-W
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

b. Effectiveness: NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

10.46
21.52
4.25
2.11
3.07
2.24
13.01
9.05

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: None

2.	Pour Point: 28°F

3.	Viscosity: 31.00 cps

4.	Specific Gravity: 1.0065 g/cc

5.	pH: 10.4

6.	Surface Active Agents: Confidential

7.	Solvents: None

8.	Additives: None

9.	Solubility: Completely water soluble

Surface Washing Agents

323

NOKOMIS 5-W


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.037

<0.050

<0.050

<0.050

<0.025

<0.0064

<0.050

1.7

0.042

<0.500

Surface Washing Agents

324

NOKOMIS 5-W


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-39
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JULY 02, 2010
"G-CLEAN OSC-1809"

I.	NAME, BRAND, OR TRADEMARK
G-CLEAN OSC-1809
(aka, OIL SPILL CLEANUP)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Green Earth Technologies

1136 Celebration Boulevard
Celebration, FL 34347
Phone: (330) 540-4220
Fax: (815)331-0931
E-mail: mlukco@getg.com
E-mail: iloch@getg.com
Website: www.getg.com
(Mr. Michael Lukco)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Green Earth Technologies

1136 Celebration Boulevard
Celebration, FL 34347
Phone: (330) 540-4220
Fax: (815)331-0931
E-mail: mlukco@getg.com
E-mail: iloch@getg.com
Website: www.getg.com
(Mr. Michael Lukco)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: As defined by OSHA's
Hazard Communication Standard, this product is non-hazardous with no evidence of adverse
effects. No personal protection or exposure controls.

4.a.	Maximum storage temperature: 140°F continuous up to 5 days
4.b. Minimum storage temperature: 35°F

8/23/2012
7/27/2022

Surface Washing Agents

325

G-CLEAN OSC 1809


-------
4.c. Optimum storage temperature range: 50°F to 98°F

4.d. Temperatures of phase separations and chemical changes: May begin freezing at or below
25°F as product begins to thaw. Mix product with agitator until product becomes homogenous.

V.	SHELF LIFE

Five to ten years in sealed polydrums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied to any surface for removal of oils. Select proper
dilution depending on product types and material surface prior to application. For treatment of
large areas, properly diluted product may be applied by spraying with a pressure washer, portable
fire pump or any other suitable pump with seawater or freshwater suction that is equipped with a
chemical inductor or feed pump. For smaller areas, properly diluted product may be applied with
scrubber, mop, cloth or damp sponge. Apply liberally, adjusting dilution on site as necessary.

2.	Concentration/Application Rate: For heavily weathered oil on rocks, a diluted solution of 3
parts water to 1 part product is recommended. For heavily weathered oil on beaches/sand, a
diluted solution of 5 parts water to 1 part product is ideal. For tar balls, no dilution is necessary
and it is suggested to apply directly at full strength. For removing oil from vegetation, a diluted
solution of 10/20 parts water to 1 part product is preferred. Product may be diluted with either
salt water or fresh water. Warmer waters (greater than 78°F) and/or good agitation during
application will require less product.

3.	Conditions for Use: Best results are obtained by allowing diluted solution to soak for at least
30 minutes to soften the oil deposits. Reapplication may be necessary in severely contaminated
areas. A sorbent boom or vacuum suction equipment should be positioned to collect the washed
off effluent. When proper containment equipment is in place and a soaking period of at least 30
minutes has been achieved, a diluted solution of 20 parts water and 1 part product should be
applied at mid-pressure (approximately 100 PSI). Adjust the pressure and angle of the hose
sprayer to achieve optimum results, adjusting dilution as necessary on site. Product and effluent
should be vacuumed up or absorbed in absorbent boom and disposed of according to EPA
guidelines.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

G-CLEAN OSC-1809

Menidia beryllina

11.49 96-hr



Mysidopsis bahia

7.32 48-hr

No. 2 Fuel Oil

Menidia beryllina

2.51 96-hr



Mysidopsis bahia

2.24 48-hr

G-CLEAN OSC-1809 &

Menidia beryllina

6.05 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.51 48-hr

Reference Toxicant (SLS)

Menidia beryllina

12.25 96-hr



Mysidopsis bahia

11.71 48-hr

Surface Washing Agents

326

G-CLEAN OSC 1809


-------
b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS

NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: -16°F

3.	Viscosity: 60.77 at40°C

4.	Specific Gravity: 1.029 @60°F

5.	pH: 11.3

6.	Surface Active Agents: Nonionic, Surfactants, PROPRIETARY

7.	Solvents: Plant-based, PROPRIETARY

8.	Additives: None

9.	Solubility: Completely water soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.004

Cadmium	<0.002

Chromium	2.004

Copper	0.068

Lead	<0.004

Mercury	<1 |ig/L
Nickel 0.0132
Zinc 0.0136

Cyanide	<0.25

Chlorinated Hydrocarbons	<5.00

Surface Washing Agents

327

G-CLEAN OSC 1809


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

3/16/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-40

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 06, 2010

"GREEN BEAST™ OIL SPILL & ODOR REMEDIATOR"

(aka, GREEN BEAST WASHING AGENT; ALL PURPOSE CLEANER & REMEDIATOR)

I.	NAME, BRAND, OR TRADEMARK

GREEN BEAST™ OIL SPILL & ODOR REMEDIATOR

(aka, GREEN BEAST WASHING AGENT; ALL PURPOSE CLEANER & REMEDIATOR)
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
BioFusion Corporation

310 Godwin Avenue
Ridgewood, NJ 07450
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. David Gubb)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Brightside Products, LLC	MSC Industrial Supply Company, Inc.
310 Godwin Avenue 75 Maxess Road

Ridgewood, NJ 07450	Melville, NY 11747

Phone: updated information required	Phone: (800) 645-7270

Fax: updated information required	Website: www.mscdirect.com

E-mail: updated information required
(Mr. David Gubb)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however, goggles are recommended. If eye or skin irritation occurs, flush
with plenty of water.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 113°F

4.d. Temperatures of phase separations and chemical changes: Stable

Surface Washing Agents

328

GREEN BEAST™ OIL SPILL
& ODOR REMEDIATOR


-------
V.	SHELF LIFE

Unlimited in sealed polydrums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: The diluted composition of the present formulation is preferably applied
to a surface to be cleaned under pressure (i.e., power washing), but will work well poured
directly onto the contaminated area. It is advantageous to apply the diluted final composition at
high pressure, above 500 psi, but it is not required.

2.	Concentration/Application Rate: For treating hydrocarbons on beaches, rocks, and hard
surfaces the final composition is diluted 1:15 with fresh or sea water and is applied to the
hydrocarbons at a rate of about 4 gallons for 1000 square feet of contaminated area. For spills
which are of heavy consistency, the diluted mixture is preferably applied at a rate of about 1.3
gallons for 1000 square feet of contaminated area and the diluted final composition is preferably
applied over a period of three consecutive days. Residue should be collected and disposed of in
accordance with local, state, and federal practices and laws.

3.	Conditions for Use: The composition of the present formulation is diluted into water,
preferably at a temperature of about 38°F to about 60°F. While the composition is active below
about 38°F, the activity is slightly reduced. The composition is also active at temperatures above
about 60°F; however, at these elevated temperatures the composition is less stable and is
denatured at a greater rate than at lower temperatures. Preferably, the diluted compositions of the
present formulation are used immediately after the dilution into about 38°F to 60°F water.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Product
No. 2 Fuel Oil
Product &

No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

b. Effectiveness: NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

29.18
30.42
2.51
2.24
7.15
2.24
12.25
11.71

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >85°C

2.	Pour Point: +26°F

Surface Washing Agents

329

GREEN BEAST™ OIL SPILL
& ODOR REMEDI AT OR


-------
3.	Viscosity: 3.87 at40°C

4.	Specific Gravity: 0.9986 @60°F

5.	pH: 4.5

6.	Surface Active Agents: Anionic andNonionic, PROPRIETARY SURFACTANTS

7.	Solvents: None

8.	Additives: Nutrient and Protein Package, PROPRIETARY

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0088

Cadmium	<0.002

Chromium	0.1752

Copper	0.0360

Lead	<0.004

Mercury	<1 |ig/L

Nickel	<0.010

Zinc	0.0840

Cyanide	<0.010

Chlorinated Hydrocarbons	<5.00

Surface Washing Agents

330

GREEN BEAST™ OIL SPILL
& ODOR REMEDI AT OR


-------
TECHNICAL PRODUCT BULLETIN #SW-41

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 13, 2010

"TULXA"

I.	NAME, BRAND, OR TRADEMARK
TULXA

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Grupo Arthuriana S.A. de C.V.

Cuernavaca No. 43

Colonia Condesa, Delegacion Cuauhtemoc
Mexico, Distrito Federal C.P. 06140
Phone: 01 52 (55) 52 41 11 90
Fax: 01 52 (55) 53 61 13 54

E-mail: sgarcia@arthuriana. com.mx. sgarcia@onsite.com.mx or bescorcia@arthuriana.com.mx.

bescorcia@onsite.com.mx

Website: www.grupoarthuriana.com.mx

(Ms. Susana Garcia Ballesteros)

(Ms. Bertha Escorcia Rodriguez)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Grupo Arthuriana S.A. de C.V.

Cuernavaca No. 43

Colonia Condesa, Delegacion Cuauhtemoc
Mexico, Distri to Federal C.P. 06140
Phone: 01 52 (55) 52 41 11 90
Fax: 01 52 (55) 53 61 13 54

E-mail: sgarcia@arthuriana.com.mx, sgarcia@onsite.com.mx or bescorcia@arthuriana.com.mx,

bescorcia@onsite.com.mx

Website: www.grupoarthuriana.com.mx

(Ms. Susana Garcia Ballesteros)

(Ms. Bertha Escorcia Rodriguez)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Wear protective mask.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
eyes, in case of contact rinse with fresh water. Do not ingest. If swallowed do not induce
vomiting and contact a doctor immediately. Use normal protective equipment for handling
powder, such as a mask or eye shield. If eye or skin irritation occurs, flush with plenty of fresh

Surface Washing Agents

331

TULXA


-------
water.

4.a. Maximum storage temperature: 104°F or40°C

4.b. Minimum storage temperature: 52°F or20°C

4.c. Optimum storage temperature range: 77°F or 25°C and 95°F or 35°C

4.d. Temperatures of phase separations and chemical changes: >104°F or 40°C

V.	SHELF LIFE

Two years if stored in dry, fresh environment.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Tulxa can be applied using conventional spraying equipment using low
to moderate pressure. Tulxa can be applied directly to any surfaces coated with oil (e.g., beaches,
rocks, plants).

2.	Concentration/Application Rate: Tulxa can be diluted with fresh water up to a ratio of 1:200.
Higher concentration of Tulxa may be required for weathered oils. Optimum concentration
should be determined on site based on the type and age of the oil being removed. The product is
fully miscible with water with minimal mixing.

3.	Conditions for Use: It is recommended to do a test to measure the amount of oils removed and
check the time and dilution at which the fats are separated. The product should completely
separate the oils in 25 minutes. Although, it may be necessary to let the mixture stay in contact
with surface for a longer period of time depending on the type and age of the oil. Residue should
be collected and disposed of in accordance with local, state, and federal practices and laws.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

TULXA

Menidia beryllina

16.50 96-hr



Mysidopsis bahia

11.33 48-hr

No. 2 Fuel Oil

Menidia beryllina

4.94 96-hr



Mysidopsis bahia

1.31 48-hr

TULXA&

Menidia beryllina

6.08 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.24 48-hr

Reference Toxicant (SLS)

Menidia beryllina

12.19 96-hr



Mysidopsis bahia

10.53 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >185°F

2.	Pour Point: 22°F

3.	Viscosity: 30.77 cSt @ 40°C

Surface Washing Agents

332

TULXA


-------
4.	Specific Gravity: 1.0263 @60°F

5.	pH: 5.0

6.	Surface Active Agents: NA

7.	Solvents: NA

8.	Additives: None

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.002

Cadmium	<0.001
Chromium 0.4436
Copper 0.0034

Lead	<0.002

Mercury	<1 |ig/L

Nickel	<0.005
Zinc 0.0278

Cyanide	<0.013

Chlorinated Hydrocarbons	<1.00

Surface Washing Agents

333

TULXA


-------
TECHNICAL PRODUCT BULLETIN #SW-42

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 28, 2010

"MARINE GREEN CLEAN™"

I.	NAME, BRAND, OR TRADEMARK
MARINE GREEN CLEAN™

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail.com

Website: www.agstx.com

(Mrs. Linda Whiteley)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail.com

Website: www.agstx.com

(Mrs. Linda Whiteley)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Respiratory protection is not considered necessary for normal use. If exposure to
vapors or mists is possible, such as is a fire emergency, NIOSH approved respiratory protection
for organic vapors should be used. Mechanical ventilation is not normally required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of contact with
eyes, wash thoroughly with plenty of clean water. Seek medical attention if irritation develops.
Rubber protective gloves should be used if prolonged use of product is anticipated.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 33°F to 100°F

4.d. Temperatures of phase separations and chemical changes: >100°F

Surface Washing Agents

334

MARINE GREEN CLEAN™


-------
V.	SHELF LIFE

Shelf life is > 2 years. The product may lose its effectiveness at temperatures >140°F. Make sure
bulk containers are properly vented. Drums and similar containers should be kept closed. Store in
steel or plastic containers.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: For general use, apply product by spray, mop, or with standard steam
and pressure wash cleaning equipment. It can also be applied using a foam generator, or any
convenient sprayer. Product can be used as is or by using heat and pressure or mechanical
scrubbing. Rinse thoroughly with fresh water for a residue-free surface. In direct applications,
foaming will be most effective as it will allow more contact time for the product to work. In a
typical foam cleaning application operation the surface to be cleaned will be thoroughly covered
with foam and allowed to stand for several minutes. The foam is rinsed away with clean water
using a hot pressure of low pressure washer. Product can be applied with a variety of spraying or
washing equipment, depending upon the type and scale of the shoreline or beach to be cleaned.
For large areas such as beaches, the product can be sprayed from water trucks or other vehicles
equipped with pumps, hoses, and nozzles to aerially deliver cleaner. On smaller oily surfaces, the
product can be applied with hand sprayers or portable pumps may be used to spray directly onto
oily surfaces. Dose rates may vary depending on type and amount of petroleum spilled, and other
site conditions such as water, temperatures, and porosity of shoreline. Cold weather applications
will require more contact time before initiating recovery. The treated product can be removed by
several means including but not limited to: sorbent pads, oil skimmers, collection booms, use of
vacuum trucks, berm collecting, drumming, frac tanks, or other appropriate containment and
collection mechanism.

2.	Concentration/Application Rate: For spills on shorelines and beaches, the product can be used
undiluted up to 14% dilution with fresh water. After application, the product should be allowed
to penetrate and dissolve the oily surface for up to 30 minutes, longer is preferable - if possible,
to maximize contact time. For light cleaning, use up to 1:50 parts product to water. For heavy
cleaning, use up to 1:14 parts product to water.

3.	Conditions for Use: Product can be used in fresh or salt water, sand beaches, gravel, cobble,
coarse sand and rocky shores, public beaches, and other sensitive or high impact sites.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50

(DDm)

MARINE GREEN CLEAN™

Menidia beryllina

46.00

96-hr



Mysidopsis bahia

89.00

48-hr

No. 2 Fuel Oil

Menidia beryllina

18.00

96-hr



Mysidopsis bahia

22.00

48-hr

MARINE GREEN CLEAN™ &

Menidia beryllina

34.00

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

45.00

48-hr

Reference Toxicant (DSS)

Menidia beryllina

1.06

96-hr



Mysidopsis bahia

0.97

48-hr

Surface Washing Agents

335

MARINE GREEN CLEAN™


-------
b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS

NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: 30°F

3.	Viscosity: 77.2 cSt @ 25°C

4.	Specific Gravity: 1.032 @70°F

5.	pH: 11-12.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: None

9.	Solubility: Completely soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.648

Cadmium	0.030

Chromium	0.143

Copper	0.154

Lead	<0.025

Mercury	<0.013

Nickel	0.357

Zinc	2.540

Cyanide	<0.02

Chlorinated Hydrocarbons	ND

Surface Washing Agents

336

MARINE GREEN CLEAN™


-------
TECHNICAL PRODUCT BULLETIN #SW-43

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 28, 2010

"MARINE GREEN CLEAN PLUS™"

I.	NAME, BRAND, OR TRADEMARK
MARINE GREEN CLEAN PLUS™

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail. com

Website: www.agstx.com

(Mrs. Linda Whiteley)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
AGS Solutions, Inc.

5647 Nunn Street

Houston, TX 77087

Phone: (713) 645-4933

Fax: (713)645-4903

E-mail: agssolutionsinc@gmail. com

Website: www.agstx.com

(Mrs. Linda Whiteley)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Respiratory protection is not considered necessary for normal use. If exposure to
vapors or mists is possible, such as is a fire emergency, NIOSH approved respiratory protection
for organic vapors should be used. Mechanical ventilation is not normally required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of contact with
eyes, wash thoroughly with plenty of clean water. Seek medical attention if irritation develops.
Rubber protective gloves should be used if prolonged use of product is anticipated.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 0°F

4.c. Optimum storage temperature range: 33°F to 100°F

4.d. Temperatures of phase separations and chemical changes: >100°F

Surface Washing Agents

337

MARINE GREEN PLUS™


-------
V.	SHELF LIFE

Shelf life is > 2 years. The product will not lose its effectiveness unless the temperatures is
>140°F. Make sure bulk containers are properly vented. Drums and similar containers should be
kept closed. Store in steel or plastic containers.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: For general use, apply product by spray, mop, or with standard steam
and pressure wash cleaning equipment. It can also be applied using a foam generator, or any
convenient sprayer. Product can be used as is or by using heat and pressure or mechanical
scrubbing. Rinse thoroughly with fresh water for a residue-free surface. In direct applications,
foaming will be most effective as it will allow more contact time for the product to work. In a
typical foam cleaning application operation the surface to be cleaned will be thoroughly covered
with foam and allowed to stand for several minutes. The foam is rinsed away with clean water
using a hot pressure of low pressure washer. Product can be applied with a variety of spraying or
washing equipment, depending upon the type and scale of the shoreline or beach to be cleaned.
For large areas such as beaches, the product can be sprayed from water trucks or other vehicles
equipped with pumps, hoses, and nozzles to aerially deliver cleaner. On smaller oily surfaces, the
product can be applied with hand sprayers or portable pumps may be used to spray directly onto
oily surfaces. Dose rates may vary depending on type and amount of petroleum spilled, and other
site conditions such as water, temperatures, and porosity of shoreline. Cold weather applications
will require more contact time before initiating recovery. The treated product can be removed by
several means including but not limited to: sorbent pads, oil skimmers, collection booms, use of
vacuum trucks, berm collecting, drumming, frac tanks, or other appropriate containment and
collection mechanism.

2.	Concentration/Application Rate: For spills on shorelines and beaches, the product can be used
undiluted up to 14% dilution with fresh water. After application, the product should be allowed
to penetrate and dissolve the oily surface for up to 30 minutes, longer is preferable - if possible,
to maximize contact time. For light cleaning, use up to 1:200 parts product to water. For heavy
cleaning, use up to 1:14 parts product to water.

3.	Conditions for Use: Product can be used in fresh or salt water, sand beaches, gravel, cobble,
coarse sand and rocky shores, public beaches, and other sensitive or high impact sites.

Surface Washing Agents

338

MARINE GREEN PLUS™


-------
VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested

MARINE GREEN CLEAN PLUS™
No. 2 Fuel Oil

MARINE GREEN CLEAN PLUS™
& No. 2 Fuel Oil (1:10)

Reference Toxicant (DSS)

b.	Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: NA

2.	Pour Point: 28°F

3.	Viscosity: 80.2 cSt @ 25°C

4.	Specific Gravity: 8.6 @70°F

5.	pH: 11-12.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Completely soluble

X.	ANALYSIS FOR HEAVY METALS,
HYDROCARBONS
Compound
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Zinc
Cyanide

Chlorinated Hydrocarbons

Species

LC50

(DDm)

Menidia beryllina

28

.00

96-hr

Mysidopsis bahia

53

.00

48-hr

Menidia beryllina

18

.00

96-hr

Mysidopsis bahia

23

.00

48-hr

Menidia beryllina

30

.00

96-hr

Mysidopsis bahia

32

.00

48-hr

Menidia beryllina

1

.06

96-hr

Mysidopsis bahia

0

.97

48-hr

AND CHLORINATED

Concentration (ppm)

0.827

0.025

0.078

0.062

<0.025

<0.013

0.220

1.990

<0.02

ND

CYANIDE,

Surface Washing Agents

339

MARINE GREEN PLUS™


-------
BULLETIN UPDATES IN BOLD

TECHNICAL PRODUCT BULLETIN #SW-44

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 5, 2010

UPDATED LISTING LETTER DATE: MARCH 1, 2023

"CLEANGREEN® PLANET WASH"

I.	NAME, BRAND, OR TRADEMARK
CLEANGREEN® PLANET WASH

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
U.S. AG, LLC

P.O. Box 368
Hogansville, GA 30230

Phone: (706) 637-1111
E-mail: carl@unitedstatesag.com
Website: www.unitedstatesag.com
(Mr. Carl Schneider)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
U.S. AG, LLC

7054 Lone Oak Road
Hogansville, GA 30230

Phone: (706) 637-1111
E-mail: carl@unitedstatesag.com
Website: www.unitedstatesag.com
(Mr. Carl Schneider)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required, however, goggles are recommended. If eye or skin irritation occurs, flush
with plenty of fresh water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

Surface Washing Agents

340	CLEANGREEN® PLANET WASH


-------
V.	SHELF LIFE

5 years in sealed polydrums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied to any oil coated surface, such as beaches,
equipment, rocks, etc. A variety of pumps or sprayers may be used for direct application to
contaminates, back-pack, drum pumps, pick-up sprayers, etc.

2.	Concentration/Application Rate: Where ever higher oil concentrations occur use
approximately a 1:10 dilution ratio (product:water). Lightly soiled areas will require a 1:10 to
1:30 ratio.

3.	Conditions for Use: Residue from surface washing should be collected and disposed of
according to local, state, and federal regulations. The collection of residue can be determined on
a site by site basis based on best practices of the area.

VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested

CLEANGREEN® PLANET WASH
No. 2 Fuel Oil

CLEANGREEN® PLANET WASH &

No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

b.	Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +25°F

3.	Viscosity: 3.72 @40°C

4.	Specific Gravity: 1.0691 @70°F

5.	pH: 9.9

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Miscible in oil, water, and solvents

Species	LC50 (ppm)

Menidia beryllina	136.10 96-hr

Mysidopsis bahia	70.70 48-hr

Menidia beryllina	3.35 96-hr

Mysidopsis bahia	2.24 48-hr

Menidia beryllina	4.73 96-hr

Mysidopsis bahia	2.24 48-hr

Menidia beryllina	12.25 96-hr

Mysidopsis bahia	10.53 48-hr

Surface Washing Agents

341	CLEANGREEN® PLANET WASH


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.0265

<0.005

0.0985

<0.0150

<0.0100

0.0005

<0.0250

0.2455

<0.300

<5.0

Surface Washing Agents

342	CLEANGREEN® PLANET WASH


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

8/05/2010
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-45

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 5, 2010

"SOC-10"

I.	NAME, BRAND, OR TRADEMARK
SOC 10 (SURFACE OIL CLEANER)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Oil Treatment International AG

Seestrasse 5
CH-6300 Zug
Switzerland

Phone: updated information required
Fax: updated information required
(Mr. Paul Schuler, CEO)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Eco-Oil Treatment Technologies Corporation

18 Poppy Hills
Laguna Niguel, CA 92677
Phone: (949) 903-40336 (24-Hour)

E-mail: EcoOilTreatment@gmail.com
(Mr. William Azzalino)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (water based)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: In case of eye contact,
flush with water. In case of skin contact, wash with water. If swallowed, drink water to dilute
and induce vomiting.

4.a.	Maximum storage temperature: 60°C
4.b. Minimum storage temperature: 0°C

4.c. Optimum storage temperature range: 10°C to 30°C

4.d. Temperatures of phase separations and chemical changes: 85°C

V.	SHELF LIFE

2 years or more if stored correctly in plastic drums and at recommended temperatures.

Surface Washing Agents

343

SOC 10


-------
VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied by manual or mechanical means including but
not limited to: hand operated spraying flask, spraying equipment and jet spraying equipment.
Application mixture, once applied, should be washed with water or any suitable type for desired
end result after about 3 minutes. Application mixture can be applied without further action or
may be scrubbed, rubbed, or abraded as desired until diluted hydrocarbons have been removed
from soil, sand, or rocks.

2.	Concentration/Application Rate: Product should be applied at a 1:12 product to water ratio:
1:12(1 oz of SOC 10 concentrated: 11 oz water or 1 ml SOC 10 concentrated to 11 ml water).

3.	Conditions for Use: Product may be used in fresh, river, brackish, or salt water of any
temperature above 35°F. Optimum temperature for normal contamination is 25°C for heavy or
aged oil. Product is suitable for use on crude oils and petroleum products that retain the majority
of their VOCs including oil slicks, oil sheens, oil emulsions, and oil spills. It is not suitable for
use on tar balls or other tar masses, or tar sands. For in-situ washing of sands, soils, and
vegetation, a lined recovery trench may be built down slope to recover any residue. As washing
occurs, pump residue from trench and dispose according to federal, state, and local regulations.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

SOC 10

Menidia beryllina

20,007 96-hr



Mysidopsis bahia

9,639 48-hr

No. 2 Fuel Oil

Menidia beryllina

3.76 96-hr



Mysidopsis bahia

2.04 48-hr

SOC 10 &

Menidia beryllina

6.31 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.24 48-hr

Reference Toxicant (SLS)

Menidia beryllina

12.19 96-hr



Mysidopsis bahia

10.53 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	FlashPoint: 122°F

2.	Pour Point: 29°F

3.	Viscosity: 1.261 cps @40°C

4.	Specific Gravity: 0.9970 g/cc @60°F

5.	pH: 7.3

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: None

9.	Solubility: Completely water soluble

Surface Washing Agents

344

SOC 10


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Concentration (ppm)

Arsenic

<0.050

Cadmium

<0.035

Chromium

<0.025

Copper

<0.050

Lead

<0.060

Mercury

0.0005

Nickel

<0.050

Zinc

0.052

Cyanide

<0.150

Chlorinated Hydrocarbons

<1.0

Surface Washing Agents

345

SOC 10


-------
TECHNICAL PRODUCT BULLETIN #SW-46
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: AUGUST 17, 2010
"BIOGRASS EXTRA®"

I.	NAME, BRAND, OR TRADEMARK
BIOGRASS EXTRA®

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Quimica del Desierto, S. De R.L. de C.V.

Madrid 2001-A
Col. Mirador

Chihuahua City, Chihuahua, Mexico C.P. 31205
Phone: +52-1-614-110-2650
E-mail: erich.wolf@biograssextra.com
Website: www.biograssextra.com
(Ing. Erich Wolf)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
HRD Ecological Equations LLC

1417 Palma Plaza
Austin, Texas, 78703
Phone: (512) 789-4881
E-mail: info@biograssextra.com
(Mr. Howard Reed)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous).

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however goggles are recommended. In case of eye irritation, flush with
plenty of fresh water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Mix well before use if outside the
60-85°F range.

Surface Washing Agents

346

BIOGRASS EXTRA®


-------
V.	SHELF LIFE
Two years minimum.

VI.	RECOMMENDED APPLICATION PROCEDURES

Recommended application procedures depending on concentration of contaminants, water
salinity levels, water temperature, and the type and age of the contaminant.

There are two means of application: power spraying or direct application.

a.	Application via power spraying: Use of a power washer to spray the contaminated surface.
The action may be improved by warming the product during use.

b.	Application via direct application: Remove contaminated soil, sand, etc. into a container.
Irrigate the affected ground with the product and let it soak in. Agitate the mixture of
water/product/ground and add additional water to float the contaminant off of the surface. A
layer of product-contaminant will form which may be physically separated from the soil. The oil
in this layer may be separated by dehydration or pumping to prepare the contaminant for disposal
or reclamation. The clean soil or sand may be returned to its original environment.

The residue should be removed and disposed of as required by local, state, or federal regulations.
The on-site coordinator can determine the best way to recover the residue based on the spill type,
surface, and environment of the area.

Concentrations: The concentration of the BIOGRASS® EXTRA product to be used depends on
the density of the contaminant. Normally the product is used in a one-to-one proportion with the
contaminant.

VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested
BIOGRASS® EXTRA

No. 2 Fuel Oil

BIOGRASS® EXTRA &

No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

b.	Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

Species

LC50 (DDm)

Menidia beryllina

548.66

96-hr

Mysidopsis bahia

703.43

48-hr

Menidia beryllina

2.51

96-hr

Mysidopsis bahia

2.24

48-hr

Menidia beryllina

2.54

96-hr

Mysidopsis bahia

2.24

48-hr

Menidia beryllina

12.25

96-hr

Mysidopsis bahia

11.71

48-hr

Surface Washing Agents

347

BIOGRASS EXTRA®


-------
IX. PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: 21.0°F

3.	Viscosity: 1.37 cSt @40°C

4.	Specific Gravity: 1.0253 @60°F

5.	pH: 7.1

6.	Surface Active Agents: Anionic and nonionic, proprietary, surfactants

7.	Solvents: Water

8.	Additives: Sodium phosphate dibasic, sodium chloride

9.	Solubility: Miscible in water and some solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0702

Cadmium	0.0024

Chromium	0.0174

Copper	0.0158

Lead	0.0086

Mercury	<0.001

Nickel	0.0580

Zinc	0.3092

Cyanide	<0.010

Chlorinated Hydrocarbons	<1.0

Surface Washing Agents

348

BIOGRASSEXTRA®


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-47
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: AUGUST 25, 2010
"ENVIRONMENTAL 1 CRUDE OIL CLEANER"

I.	NAME, BRAND, OR TRADEMARK
ENVIRONMENTAL 1 CRUDE OIL CLEANER
(aka, ENVIRONMENTAL 1 WASHING AGENT)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Environmental 1, LLC

P.O. Box 9

Jackson, TN 38302

Phone: (615) 269-0506

Fax: (615)269-0025

E-mail: info@environmental-one.com

E-mail: mfb@environmental-one.com

Website: www.environmental-one.com

(Ms. Mary Frances Blankenship, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Environmental 1, LLC

P.O. Box 9

Jackson, TN 38302

Phone: (615) 269-0506

Fax: (615)269-0025

E-mail: info@environmental-one.com

E-mail: mfb@environmental-one.com

Website: www.environmental-one.com

(Ms. Mary Frances Blankenship, President)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable, no hazards or restrictions

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however goggles are recommended if used with a pressure washer. If eye or
skin irritation occurs, flush with plenty of fresh water.

4.a.	Maximum storage temperature: 140°F
4.b. Minimum storage temperature: 35°F

4/04/2016
7/27/2022

Surface Washing Agents

349

ENVIRONMENTAL 1
CRUDE OIL CLEANER


-------
4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Unlimited in sealed polydrums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

ENVIRONMENTAL 1 CRUDE OIL CLEANER cleans oil from solid surfaces such as beaches,
rocks, machines, buildings, tools, and other hard surfaces.

1.	Spray ENVIRONMENTAL 1 CRUDE OIL CLEANER on oil surface to be cleaned with a
drum pump sprayer or for smaller jobs use a hand pump sprayer.

2.	On areas of heavy oil accumulation use product directly on the spill, or for areas of lighter
accumulation use a 1:10 to 1:30 dilution ratio (product:water).

3.	The oil and cleaner form a loose emulsion that can be rinsed away. Oil displaced from hard
surfaces can be skimmed from the rinse water, absorbed with an oil absorbent, or removed
via commercial waste removal.

4.	May be used with fresh or salt water in normal climatic temperatures.

VII.	TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested

ENVIRONMENTAL 1 CRUDE
OIL CLEANER
No. 2 Fuel Oil

ENVIRONMENTAL 1 CRUDE
OIL CLEANER & No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

b.	Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +26.0°F

3.	Viscosity: 3.34 cSt @ 40°C

4.	Specific Gravity: 1.01 @ 15°C

5.	pH: 6.2

6.	Surface Active Agents: Anionic, nonionic, zwitterionic surfactants

7.	Solvents: None

8.	Additives: Preservative

Species

LC50

(DDm)

Menidia beryllina

22.68

96-hr

Mysidopsis bahia

16.27

48-hr

Menidia beryllina

2.24

96-hr

Mysidopsis bahia

0.99

48-hr

Menidia beryllina

2.19

96-hr

Mysidopsis bahia

0.43

48-hr

Menidia beryllina

12.25

96-hr

Mysidopsis bahia

11.71

48-hr

Surface Washing Agents

350

ENVIRONMENTAL 1
CRUDE OIL CLEANER


-------
9. Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0021

Cadmium	<0.0010

Chromium	<0.0030

Copper	<0.0030

Lead	<0.0020

Mercury	<0.0005

Nickel	<0.0050

Zinc	<0.0030

Cyanide	<0.010

Chlorinated Hydrocarbons	<5.00

Surface Washing Agents

351

ENVIRONMENTAL 1
CRUDE OIL CLEANER


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-48
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: OCTOBER 4, 2010
"SANDKLENE 950"

I.	NAME, BRAND, OR TRADEMARK
SANDKLENE 950

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
MDEChem, Inc.

923 10th Street PMB 101
Floresville, TX 78114
Phone: updated information required
E-mail: updated information required
Website: www.mdechem.com
(Mr. Paul Sack)

III.	NAME, ADDRESS, AND
Imperial Petroleum, Inc.

101 NW 1st Street #213
Evansville, IN 47708
Phone: (812)867-1433
E-mail: Jwilsonx 1 @aol.com
(Mr. Jeff Wilson)

Archer Petroleum Corp.

490-580 Hornby St.

Vancouver, Canada V6C 3B6
604-683-7588
(Mr. Colin Bowkett)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Normal

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wear chemically
impervious gloves. No other special equipment or clothing is required; however, goggles are
recommended. If eye or skin irritation occurs, flush with plenty of water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

3/16/2016
7/27/2022

TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Mailing Address:

Imperial Petroleum, Inc.

P.O. Box 1006
Evansville, IN 47706
(Mr. Jeff Wilson)

Surface Washing Agents

352

SANDKLENE 950


-------
4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Unlimited in sealed drums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: SANDKLENE 950 is most effective in enclosed systems using
centrifuges, shearing devices, or similar high speed equipment to process material. Under these
conditions, SANDKLENE 950 and water are recycled continuously. In smaller applications on
solid surfaces, SANDKLENE 950 may be applied with sprayers using water diluted product
directly onto solid oil coated surfaces.

2.	Concentration/Application Rate: Oil contaminated sands are placed in an enclosed chamber
with a solution of SANDKLENE 950 and water. The concentration of SANDKLENE 950 in
water ranges from about 0.15% to about 1.0%. The total volume of solution is 350 gallons per 3
cubic yards of contaminated sand. The mixture is agitated at an elevated temperature in the range
of 100°F to 150°F. The actual treatment rate will vary within the recommended range, depending
upon the nature of sand, the nature of the oil, and the percentage of oil content.

3.	Conditions for Use: The water and oil parts are separated from the sand. The water part is
continuously recycled, the oil is recovered, and the sand can be disposed according to federal,
state, and local regulations. Dose rates and SANDKLENE 950 concentrations will vary with the
type and amount of petroleum present, the extent of weathering, and other site specific
conditions, including temperature and time available to let the solution contact the oil.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (DDm)

SANDKLENE 950

Menidia beryllina

1768.73 96-hr



Mysidopsis bahia

1263.78 48-hr

No. 2 Fuel Oil

Menidia beryllina

8.95 96-hr



Mysidopsis bahia

2.41 48-hr

SANDKLENE 950&

Menidia beryllina

4.48 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.24 48-hr

Reference Toxicant (DLS)

Menidia beryllina

12.25 96-hr



Mysidopsis bahia

11.71 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +10°F

3.	Viscosity: 3.69 cSt @ 40°C

Surface Washing Agents

353

SANDKLENE 950


-------
4.	Specific Gravity: 1.2806 @60°F

5.	pH: 9.4

6.	Surface Active Agents: None

7.	Solvents: None

8.	Additives: None

9.	Solubility: Completely soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.540

Cadmium	<0.209

Chromium	1.100

Copper	<0.205

Lead	<0.494

Mercury	0.0009

Nickel	<0.274

Zinc	<0.204

Cyanide	<1.150

Chlorinated Hydrocarbons	<0.100

Surface Washing Agents

354

SANDKLENE 950


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-49
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: NOVEMBER 10, 2010
"DE-SOLV-IT CLEAN AWAY APC SUPER CONCENTRATE"

I.	NAME, BRAND, OR TRADEMARK
DE-SOL V-IT CLEAN AWAY APC SUPER CONCENTRATE
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Orange-Sol Blending and Packaging

1400 N Fiesta Boulevard

Gilbert, AZ 85233

Phone: (800) 877-7771

Fax: (480) 497-0444

E-mail: updated information required

Website: www.orange-sol.com

(Mr. Albert Farnsworth or

Mr. Jack Farnsworth at (480) 319-0141)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Bell Tech

Master Distributor

P.O. Box 2198

Valdez, AK 99686

Phone: (907) 602-0111

Fax: (907) 835-4535

E-mail: bellenterprise@cvinternet.net

(Mr. Randy Bell)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-combustible

2.	Ventilation: No special requirements

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
of clothing required; however, goggles are recommended where splash is potential. If eye or skin
irritation occurs, flush with ample fresh water.

4.a.	Maximum storage temperature: 210°F
4.b. Minimum storage temperature: 34°F

4.c. Optimum storage temperature range: 55°F to 90°F

3/03/2016
7/27/2022

Surface Washing Agents

355

DE-SOL V-IT CLEAN AWAY
APC SUPER CONCENTRATE


-------
4.d. Temperatures of phase separations and chemical changes: There are no known phase
separations, chemical changes, or other altercations that will change the effectiveness of the
product.

V.	SHELF LIFE

Two (2) years in sealed drums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: DE-SOLV-IT CLEAN AWAY APC SUPER CONCENTRATE can be
used on all oil coated surfaces including sand and rocks through a detergency mechanism.
Product should be used with handheld sprayers or for larger applications applied with truck
mounted sprayers. Remove contamination with DE-SOLV-IT CLEAN AWAY APC SUPER
CONCENTRATE, followed by a rinse.

2.	Concentration/Application Rate: For oil spill removal and heavy duty cleaning, dilute product
with water using a 1:1 ratio.

3.	Conditions for Use: DE-SOLV-IT CLEAN AWAY APC SUPER CONCENTRATE can be
used in salt or fresh water, with no limitations as to usage within the optimum temperature
parameters (application may be made at or above 35°F, with optimum above 48°F). Cleaning of
oil soaked areas should be done in a contained area and residue should be collected. For sand or
vegetation cleaning, a berm may be constructed down slope that will collect the residue for
disposal. All disposal residues should be done according to federal, state, and local regulations.
In general, the technique used for collection of the oil/soap residue should be determined by the
onsite contractor based on the environment of the area to be cleaned and the equipment and
materials available for collection. Cleanup residue should be collected and disposed of in
accordance with local, state, and federal regulations.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

DE-SOLV-IT CLEAN
AWAY APC SUPER
CONCENTRATE
No. 2 Fuel Oil

DE-SOLV-IT CLEAN
AWAY APC SUPER
CONCENTRATE &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
20.95 96-hr
30.95 48-hr

4.07 96-hr
0.86 48-hr
6.42 96-hr
0.69 48-hr

12.04 96-hr
8.19 48-hr

b. Effectiveness: NA

Surface Washing Agents

356

DE-SOLV-IT CLEAN AWAY
APC SUPER CONCENTRATE


-------
VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +20°F

3.	Viscosity: 3.1 cSt @ 40°C

4.	Specific Gravity: 1.024 @60°F

5.	pH: 9.03

6.	Surface Active Agents: PROPRIETARY

7.	Solvents: PROPRIETARY

8.	Additives: Yes

9.	Solubility: 100 percent

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.0

Cadmium	<0.5

Chromium	<0.5

Copper	<2.0

Lead	<1.0

Mercury	<0.005

Nickel	<1.0

Zinc	<2.5

Cyanide	0.08

Chlorinated Hydrocarbons	<0.05

Surface Washing Agents

357

DE-SOLV-IT CLEAN AWAY
APC SUPER CONCENTRATE


-------
LISTING CHANGES PENDING;

VERIFICATION BY MANUFACTURER AND EPA REQUIRED

TECHNICAL PRODUCT BULLETIN #SW-50

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: NOVEMBER 17, 2010

"EO ALL PURPOSE SOAP-LAVENDER"

I.	NAME, BRAND, OR TRADEMARK
EO ALL PURPOSE SOAP-LAVENDER
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
EO Products/Small World Trading Company

90 Windward Way
San Rafael, CA 94901
Phone: (415) 945-1900
Fax: (415)945-7117

E-mail: kimberly@eoproducts.com or sam@eoproducts.com

Website: www.eoproducts.com

(Ms. Kimberly Luce or Mr. Sam Borri)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
EO Products/Small World Trading Company

90 Windward Way

San Rafael, CA 94901

Phone: (415) 945-1900

Fax:(415) 945-7117

E-mail: kimberly@eoproducts.com or

sam@eoproducts.com

Website: www.eoproducts.com

(Ms. Kimberly Luce or Mr. Sam Borri)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Normal

3.	Skin and eye contact; protective clothing; treatment in case of contact: Rinse thoroughly after
use. Avoid eye contact. In case of such contact, immediately flush with large amounts of cool
water for at least 15 minutes. Consult a physician if irritation develops. Protective gloves are
recommended for extended or prolonged contact (e.g., immersing hands). Wear safety glasses if
the method of use presents the likelihood of eye contact. Do not ingest. In case of ingestion,
consult a physician.

4.a.	Maximum storage temperature: 45°C

Surface Washing Agents

358

EO ALL PURPOSE
SOAP LAVENDER


-------
4.b. Minimum storage temperature: 4°C

4.c. Optimum storage temperature range: 22°C to 30°C

4.d. Temperatures of phase separations and chemical changes: Phase separation may occur at
<15°C (but will restore to original condition at optimum temperature).

V.	SHELF LIFE

Three (3) years (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: EO ALL PURPOSE SOAP may be applied by pouring, spraying (when
diluted 1:4), dispensing equipment, or by scrubbing machines.

2.	Concentration/Application Rate: Apply EO ALL PURPOSE SOAP full strength (undiluted) to
surface area by pouring or with dispensing equipment concentrating on areas with heaviest
contamination first. Apply diluted (1:4 dilution rate) EO ALL PURPOSE SOAP with sprayer.
Agitate and scrub well. Rinse thoroughly. For heavily contaminated surfaces, EO ALL
PURPOSE SOAP should always be used full strength (undiluted). For average to light
contamination, EO ALL PURPOSE SOAP may be diluted from 2x-10x with water.

3.	Conditions for Use: During cleaning, contain the oil soaked area and collect residue. For sand
and vegetation cleaning, a berm may be constructed down slope that will collect the residue for
disposal. All disposal of residue should be done according to federal, state, and local regulations.
In general, the technique used for the collection of the oil/soap residue should be determined by
the on-site contractor based on the environment of the area to be cleaned, and equipment and
materials available for collection.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

EO ALL PURPOSE

Menidia beryllina

21.33 96-hr

SOAP

Mysidopsis bahia

83.65 48-hr

No. 2 Fuel Oil

Menidia beryllina

8.95 96-hr



Mysidopsis bahia

2.41 48-hr

EO ALL PURPOSE

Menidia beryllina

3.14 96-hr

SOAP & No. 2 Fuel Oil

Mysidopsis bahia

2.37 48-hr

(1:10)





Reference Toxicant

Menidia beryllina

12.04 96-hr

(SLS)

Mysidopsis bahia

8.19 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES
1. Flash Point: >93°C

Surface Washing Agents

359

EO ALL PURPOSE
SOAP LAVENDER


-------
2.	Pour Point: +24°F

3.	Viscosity: 349.5 cSt @ 40°C

4.	Specific Gravity: 1.0208 @60°F

5.	pH: 5.88

6.	Surface Active Agents: PROPRIETARY

7.	Solvents: PROPRIETARY

8.	Additives: PROPRIETARY

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS
Compound
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Zinc
Cyanide

Chlorinated Hydrocarbons

CYANIDE, AND CHLORINATED

Concentration (ppm)

<0.540

<0.209

0.202

<0.205

<0.494

<0.000388

5.99

<0.204

<1.15

<2.0

Surface Washing Agents

360

EO ALL PURPOSE
SOAP LAVENDER


-------
TECHNICAL PRODUCT BULLETIN #SW-51
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: DECEMBER 7, 2010
"DYNAMIC GREEN™"

I.	NAME, BRAND, OR TRADEMARK
DYNAMIC GREEN™

Type of Product: Surface Washing Agent (Water-based)

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Wechem, Inc.

5734 Susitna Drive
Harahan, LA 70123
Phone: (800) 426-0512
Phone: (504) 733-1152
Fax:(504)733-2218

E-mail: mwisecarver@ wechem.com or lhernandez@wechem.com
Website: www.wechem.com
(Mr. Mike Wisecarver)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Wechem, Inc.

5734 Susitna Drive
Harahan, LA 70123
Phone: (800) 426-0512
Phone: (504) 733-1152
Fax:(504)733-2218

E-mail: mwisecarver@wechem.com or lhernandez@wechem.com
Website: www.wechem.com
(Mr. Mike Wisecarver)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Not required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wear protective gloves
that are chemical resistant, rubber. In case of skin contact, wash with soap and water. If irritation
develops seek medical attention. Wear safety glasses/goggles for eye protection. In case of eye
contact flush with water for 15 minutes. If irritation develops seek medical attention.

4.a.	Maximum storage temperature: 140°F
4.b. Minimum storage temperature: 34°F

4.c. Optimum storage temperature range: >50°F and <100°F

4.d. Temperatures of phase separations and chemical changes: <35°F and >100°F.

Surface Washing Agents

361

DYNAMIC GREEN™


-------
V.	SHELF LIFE

DYNAMIC GREEN™ has a shelf life of 6-10 years in sealed poly drums or totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied to any surface for removal of oils. The product
can be applied through power washers, garden type sprayers, fire pump or any other portable
pump with seawater or freshwater suction that is equipped with a chemical inductor or feed
pump. For smaller areas properly diluted DYNAMIC GREEN™ may be applied with sponge,
mop, scrub brush or cloth. Apply liberally, adjusting dilution on site if necessary.

2.	Concentration/Application Rate: For heavily weathered oil on rocks, a diluted solution of 4
parts water to 1 part product is recommended. For heavily weathered oil on beaches/sand a
diluted solution of 7 parts water to 1 part product is effective. For removing oil from vegetation,
a diluted solution of 10/20 parts water to 1 part product is preferred. Product is effective in fresh
or salt water.

3.	Conditions for Use: Allow diluted product to soak for 20-30 minutes to soften and lift oil from
surface. Reapplication may be necessary for severely contaminated areas. Vacuum suction
equipment and sorbent boom or pads should be used to collect the washed effluent. When proper
containment equipment is in place and a soak time of 20 minutes has been achieved, a diluted
solution of 20 parts water to 1 part product should be applied through a pressure washer or
flushing device to remove oils. Product and oil should be vacuumed up or absorbed with
absorbent boom and disposed of according to EPA guidelines.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested
DYNAMIC GREEN™

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
106.00 96-hr
66.60 48-hr
13.00 96-hr
3.16 48-hr
6.85 96-hr
3.30 48-hr

No. 2 Fuel Oil

EO ALL PURPOSE
SOAP & No. 2 Fuel
Oil (1:10)

Reference Toxicant

Menidia beryllina
Mysidopsis bahia

2.67 96-hr
9.14 48-hr

(SDS)

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

362

DYNAMIC GREEN™


-------
IX. PHYSICAL PROPERTIES

1.	Flash Point: >200°F

2.	Pour Point: -16°F

3.	Viscosity: <10 cSt @ 78°F

4.	Specific Gravity: 1.01 @77°F

5.	pH: 7.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Infinitely miscible

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.25

Cadmium	<0.25

Chromium	<0.25

Copper	<0.25

Lead	<0.25

Mercury	<2.00

Nickel	<0.25

Zinc	<0.25

Cyanide	<0.50

Chlorinated Hydrocarbons	ND

Surface Washing Agents

363

DYNAMIC GREEN™


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

8/29/2012
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-52
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: DECEMBER 9, 2010
"VERU-SOLVE™ MARINE 200 HP"

I.	NAME, BRAND, OR TRADEMARK
VERU-SOLVE™ MARINE 200 HP
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
VeruTEK® Technologies

65 West Dudley Town Road, Suite 100
Bloomfield, CT 06002
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Ms. Bethany McAvoy)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
VeruTEK® Technologies

65 West Dudley Town Road, Suite 100
Bloomfield, CT 06002
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Ms. Bethany McAvoy)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Use in a well ventilated area.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Prevent eye contact,
wear safety glasses or goggles. If eye contact occurs remove contact lenses at once. Flush with
water for at least 15 minutes. If irritation persists seek medical attention. Prevent skin contact,
nitrile gloves are recommended. Boots, aprons, or bodysuits should be worn as necessary.
Contact with product may cause slight redness. Prolonged or repeated exposure may cause
drying of skin. If skin contact occurs wash affected area with copious amounts of soap and water.
Respiratory protection is not normally required. If adequate ventilation is unavailable use
NIOSH approved air-purifying respirator with organic vapor cartridge or canister. The product is
not likely toxic. If ingestion occurs DO NOT induce vomiting. Rinse mouth thoroughly with

Surface Washing Agents

364	VERU-SOLVE™ MARINE 200 HP


-------
water. Offer water to drink. DO NOT administer anything by mouth to an unconscious person.
4.a. Maximum storage temperature: Should not exceed 110°F (43.3°C)

4.b. Minimum storage temperature: Above 41°F (5°C)

4.c. Optimum storage temperature range: Between 41°F and 110°F (5°C to 43.3°C)
4.d. Temperatures of phase separations and chemical changes: Stable. There is no known
temperature within the maximum and minimum storage temperature that would cause phase
separation, chemical changes, or other known alterations to the effectiveness of the product.

V.	SHELF LIFE

Indefinite, product will not degrade over time.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: VERU-SOLVE™ MARINE 200 HP is an aqueous based liquid without
solids that can be readily applied through standard spray equipment. VERU-SOLVE™ MARINE
200 HP is suited for treating oil shorelines, sensitive environments, and for treating access
limited areas. VERU-SOLVE™ MARINE 200 HP may be applied directly to oil on shoreline,
beaches, rocks, or marsh surfaces by agricultural or standard sprayers attached to all terrain
vehicles (ATVs), or workboats equipped with spray booms. The preferred and most effective
method of application is to use a low-volume, low-pressure pump.

2.	Concentration/Application Rate: The product can be applied undiluted to the spilled oil.
VERU-SOLVE™ MARINE 200 HP should be applied as droplets, not fogged or atomized.
System Calibration - Spray systems should be calibrated to insure accurate application rates for
successful application and dosage control.

3.	Conditions for Use: VERU-SOLVE™ MARINE 200 HP is sprayed directly on oil coated
materials; and can be used on fresh or aged oil or oil combinations. Application may be limited
at sub-freezing temperatures (<31 °F) without inclusion of antifreeze additives. VERU-SOLVE™
MARINE 200 HP can be applied at temperatures above freezing without notable changes in
viscosity with increasing temperature. Application is not affected by increasing salinity. VERU-
SOLVE™ MARINE 200 HP can be used at temperatures above freezing and at temperatures
above 70°F. VERU-SOLVE™ MARINE 200 HP will separate the oil and water from the sand or
soiled surface. Cleaning of oil soaked surfaces should be done in a contained area and residue
should be collected. For sand or vegetation cleaning, a berm may be constructed down slope that
will collect the residue for disposal. Oil that has separated from sand or vegetation may be
recovered from the substrate and collected for disposal. All disposal of residue should be done in
accordance with federal, state, and local regulations. In general, the technique used for the
collection of the oil/product residue should be determined by the On-Scene Coordinator based on
the environment of the area to be cleaned, equipment and materials available for collection, and
disposal regulations.

Surface Washing Agents

365	VERU-SOLVE™ MARINE 200 HP


-------
VII. TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested

Species

LC50 (ppm)

VERU-SOLVE™

Menidia beryllina

418.32 96-hr

MARINE 200 HP

Mysidopsis bahia

76.98 48-hr

No. 2 Fuel Oil

Menidia beryllina

13.36 96-hr



Mysidopsis bahia

1.94 48-hr

VERU-SOLVE™

Menidia beryllina

10.67 96-hr

MARINE 200 HP & No.

Mysidopsis bahia

2.51 48-hr

2 Fuel Oil (1:10)





Reference Toxicant

Menidia beryllina

13.36 96-hr

(SLS)

Mysidopsis bahia

12.08 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +18°F

3.	Viscosity: 1.77391 cSt @ 40°C

4.	Specific Gravity: 1.017 @60°F

5.	pH: 7.01

6.	Surface Active Agents: PROPRIETARY

7.	Solvents: None

8.	Additives: None

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS
Compound
Arsenic
Cadmium
Chromium
Copper
Lead
Mercury
Nickel
Zinc
Cyanide

Chlorinated Hydrocarbons

CYANIDE, AND CHLORINATED

Concentration (ppm)

0.0025

<0.0010

0.0326

0.0093

<0.0020

0.00109

0.0077

0.0165

<0.010

<0.025

Surface Washing Agents

366	VERU-SOLVE™ MARINE 200 HP


-------
TECHNICAL PRODUCT BULLETIN #SW-53
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JANUARY 26, 2011
"NATURAMA G3 A-5"

I. NAME, BRAND, OR TRADEMARK

NATURAMA G3 A-5

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Green Life Development, Inc.	Merlin-Tao Ltd.

5112 W. Charleston Boulevard, Suite C	65 Yigal Alon Street POB 91

Las Vegas, NV 89146	Tel Aviv, Israel 67443

Mobile: (702) 355-5102	Phone: 972-3-562-8020

Fax: (702) 448-6977	Fax: 972-3-562-8021

E-mail: david@greenlifedevelopment.com	E-mail: asaf@merlin-tao.com

Website: www.greenlifedevelopment.com	Website: www.merlin-tao.com

(Mr. David A. Levy)	(Mr. Asaf Yaari, CEO)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Green Life Development, Inc.

5112 W. Charleston Boulevard, Suite C
Las Vegas, NV 89146
Mobile: (702)355-5102
Fax: (702) 448-6977

E-mail: david@greenlifedevelopment.com
Website: www.greenlifedevelopment.com
(Mr. David A. Levy)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing is required; however, goggles are recommended. If eye or skin irritation occurs, flush
with plenty of water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V. SHELF LIFE

NATURAMA G3 A-5 has unlimited shelf life in sealed poly drums.

Surface Washing Agents

367

NATURAMA G3 A-5


-------
VI. RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied by any method (e.g., drum pump, pressurized
spray applicator, brush, or aqueous wash tank), depending on the surface; and type and viscosity
of the oil/contamination to be treated.

2.	Concentration/Application Rate: The dilution ratio depends on the amount and type of
contamination to be removed. For light contamination areas a 1:6 dilution ratio (product to
fresh/salt water) with a 2-3 minutes wait. For heavier/thick/burnt contamination, the exact ratio
should be determined by the field coordinator but a general starting point of 20-25% should
remove most contamination (grease, burnt oil, diesel, tar, etc.) after a contact time of 10-15
minutes before rinsing with water/steam.

3.	Conditions for Use: Cleanup residue must be collected and should be disposed of in
accordance with local, state, and federal regulations. Where possible, the product/oil mixture can
be recovered and processed using an oil separator system or a stagnant tank. A circulating wash
tank fitted with an oil separator or filter system extends the life of NATURAMA G3 A-5 by
weeks, greatly impacting the waste reduction.

VII. TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested Species	LC50 (ppm)

NATURAMA G3 A-5 Menidia beryllina	577.68 96-hr

Mysidopsis bahia	482.97 48-hr

No. 2 Fuel Oil Menidia beryllina	2.39 96-hr

Mysidopsis bahia	0.32 48-hr

NATURAMA G3 A-5 & Menidia beryllina	3.68 96-hr

No. 2 Fuel Oil (1:10) Mysidopsis bahia	2.24 48-hr

Reference Toxicant (SLS) Menidia beryllina	12.25 96-hr

Mysidopsis bahia	12.08 48-hr

b.	Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >93°C

2.	Pour Point: +28°F

3.	Viscosity: 1.3628 cSt @ 40°C

4.	Specific Gravity: 1.006 @60°F

5.	pH: 8.39

6.	Surface Active Agents: PROPRIETARY

7.	Solvents: PROPRIETARY

8.	Additives: None

9.	Solubility: Miscible in oil, water, and solvents

Surface Washing Agents

368

NATURAMA G3 A-5


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.0092

<0.002

0.0262

<0.006

0.0062

0.0005

<0.01

<0.0166

0.014

<26.30

Surface Washing Agents

369

NATURAMA G3 A-5


-------
TECHNICAL PRODUCT BULLETIN #SW-54

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: FEBRUARY 25, 2011

"SAFE KLEEN"

I.	NAME, BRAND, OR TRADEMARK
SAFE KLEEN

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Anti Slip Solutions Ltd

Beauchamp House
402/403 Stourpout Road
Kidderminster, Worcestershire
DY12 1AB, UK
Phone: 44 (0) 345-222-5613
E-mail: info@safe-grip.co.uk
(Mr. Dan Bayliss)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
V4 Distributing

507 West Bird Avenue
Nampa, ID 83686
Phone: (208) 571-8596
E-mail: info@v4distributing.com
(Mr. Todd Vitek)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO Non-flammable (DOT: Non-hazardous)

2.	Ventilation: Provide adequate ventilation.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Chemical eye goggles
should be worn. In case of contact with eyes, rinse immediately with plenty of clean water for at
least 15 minutes and seek medical advice. PVC or rubber gloves are recommended. Use
protective clothing. Remove contaminated clothing and wash with soap and water.

4.a.	Maximum storage temperature: 130°F
4.b. Minimum storage temperature: 40°F

4.c. Optimum storage temperature range: >40°F to <130°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Five years if stored in tightly closed containers under dry conditions within temperature range.

Surface Washing Agents

370

SAFE-KLEEN


-------
VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: For general use apply the product by spray, brush, mop, or standard
pressure washing equipment.

2.	Concentration/Application Rate: SAFE KLEEN is a concentrated liquid that can be used either
as supplied or diluted with hot or cold, fresh or salt water. For small spills dilute 1:3 (product to
water) and apply as described. For larger spills prepare a solution of SAFE KLEEN diluted with
50 percent water and apply as described. Concentrations may be adjusted to take account of
temperatures, types and age of oil/contaminant and other local site conditions. Surface contact
time will also be dependent on temperature. For low temperatures and conditions of heavy
contamination extend the contact time, where possible agitation of the product during application
time will assist the efficiency of the cleaning. Thoroughly rinse with water.

3.	Conditions for Use: Response personnel can determine the best method to collect residue,
which can include, but is not limited to, oil skimmers, collecting booms, vacuum equipment,
absorbent materials, and other appropriate containment and collecting mechanisms. The cleanup
residue should be collected and disposed of in accordance with local, state, and federal
regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

Species

LC50 (DDm)

SAFE KLEEN

Menidia beryllina

170.00

96-hr



Mysidopsis bahia

258.00

48-hr

No. 2 Fuel Oil

Menidia beryllina

3.30

96-hr



Mysidopsis bahia

6.20

48-hr

SAFE KLEEN &

Menidia beryllina

2.60

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

6.50

48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.60

96-hr



Mysidopsis bahia

16.90

48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: NA; water-based product

2.	Pour Point: NA; water-based product

3.	Viscosity: 2.33 cSt @ 40°C

4.	Specific Gravity: 1.060 @68°F

5.	pH: 11.5-13.0

6.	Surface Active Agents: PROPRIETARY

7.	Solvents: None

8.	Additives: PROPRIETARY

9.	Solubility: Totally soluble

Surface Washing Agents

371

SAFE-KLEEN


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE, AND CHLORINATED

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

<0.31

<0.16

<0.16

<0.16

<0.16

<0.025

<0.16

<0.16

ND

ND

Surface Washing Agents

372

SAFE-KLEEN


-------
TECHNICAL PRODUCT BULLETIN #SW-55
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: FEBRUARY 25, 2011
"CORIBA 700 SR"

(aka, CORIBA 700 ER, CORIBA 700 OS)

I.	NAME, BRAND, OR TRADEMARK
CORIBA 700 SR

(aka, CORIBA 700 ER, CORIBA 700 OS)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Coriba Technologies, LLC

5708 Cadron Creek
North Little Rock, AR 72116
Phone: (501) 834-2972
E-mail: ronrios@bellsouth.net
(Mr. Harvey G. Cobb)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
MLU Services

573 Hawthorne Avenue
Athens, GA 30606
Phone: (706) 569-7300
Fax: (706) 425-0300
(Mr. Billy Ulm)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal (contains ammonia)

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact due
to possible mild eye irritation. In case of eye contact, flush eyes with water for at least 15
minutes. In the case of skin contact, flush with water for at least 15 minutes. If irritation occurs
and persists, obtain medical attention. Protective clothing is not normally required.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 33°F

4.c. Optimum storage temperature range: 33°F - 100°F

4.d. Temperatures of phase separations and chemical changes: Does not separate.

V.	SHELF LIFE

Two years unopened minimum.

Surface Washing Agents

373

CORIBA 700 SR


-------
VI. RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: CORIBA 700 SR is covered by U.S. Patent #7678201 (issued on March
16, 2010). The process is designed to remove and recover oil from sand. The product does not
react with or alter the oil. Contaminated sand is transferred into a standard sand washer filled
with 700 SR. The product is an aqueous solution that, upon contact, reduces the interfacial
tension between the oil and the sand. The oil no longer adheres to the sand and is free to float to
the surface of the processor and is removed with an auger. The cleaned sand is dried in a
centrifuge and the collected liquid is recycled back to the processor. The product has a high
vapor pressure and evaporates from the sand leaving no residue or contamination. The separated
oil is transferred to a conical vertical tower where it concentrates at the surface and is siphoned
off to be used as a fuel or sent to a refinery for further processing. The process solution that
collects in the conical tower is recycled back to the processor. The clean, dry sand can be
disposed as appropriate. Any sand that collects in the bottom of the conical tower is sent back
through the processor. The process can be set up on a beach, waste treatment facility or on a
barge for treating sensitive areas like barrier islands. The process chemical is not designed to
come into contact with any body of water. There process is not designed to treat contaminated
water. The process does not consume the process chemical. Any chemical that remains after the
sand has been cleaned can be returned to the manufacturer or sent to an appropriate waste
treatment facility.

2.	Concentration/Application Rate: CORIBA 700 SR is used at full strength. It is delivered in
aqueous solution. The application rate is 200 gallons/ton of oil-contaminated sand.

3.	Conditions for Use: CORIBA 700 SR can be applied to contaminated sand as long as the sand
mixture is not frozen.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

CORIBA 700 SR

No. 2 Fuel Oil

CORIBA 700 SR &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

1470.00	96-hr

3810.00	48-hr

11.10	96-hr

3.29	48-hr

22.80	96-hr

3.58	48-hr

5.70	96-hr

9.04	48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

374

CORIBA 700 SR


-------
IX. PHYSICAL PROPERTIES

1.	Flash Point: 102°F

2.	Pour Point: 200°F

3.	Viscosity: 1.0 cps

4.	Specific Gravity: 0.981

5.	pH: 11.4

6.	Surface Active Agents: None

7.	Solvents: None

8.	Additives: PROPRIETARY

9.	Solubility: Miscible with water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.05

Cadmium	<0.002

Chromium	0.031

Copper	0.25

Lead	0.02

Mercury	<0.01

Nickel	<0.01

Zinc	0.25

Cyanide	<0.1

Chlorinated Hydrocarbons	<0.1

Surface Washing Agents

375

CORIBA 700 SR


-------
TECHNICAL PRODUCT BULLETIN #SW-56
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: FEBRUARY 25, 2011
"CORIBA 713 SR"

(aka, CORIBA 713 ER, CORIBA 713 OS)

I.	NAME, BRAND, OR TRADEMARK
CORIBA 713 SR

(aka, CORIBA 713 ER, CORIBA 713 OS)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Coriba Technologies, LLC

5708 Cadron Creek
North Little Rock, AR 72116
Phone: (501) 834-2972
E-mail: ronrios@bellsouth.net
(Mr. Harvey G. Cobb)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
MLU Services

573 Hawthorne Avenue
Athens, GA 30606
Phone: (706) 569-7300
Fax: (706) 425-0300
(Mr. Billy Ulm)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal (contains ammonia)

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid eye contact due
to possible mild eye irritation. Use chemical safety goggles and/or full face shield where
splashing is possible. In case of eye contact, flush eyes with water for at least 15 minutes. Wear
impervious protective clothing, including boots, gloves, lab coat, apron or coveralls, as
appropriate, to prevent skin contact. In the case of skin contact, flush with water for at least 15
minutes. If irritation occurs and persists, obtain medical attention. Protective clothing is not
normally required.

4.a.	Maximum storage temperature: 100°F
4.b. Minimum storage temperature: 33°F

4.c. Optimum storage temperature range: 33°F - 100°F

4.d. Temperatures of phase separations and chemical changes: Does not separate.

Surface Washing Agents

376

CORIBA 713 SR


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V.	SHELF LIFE

Two years unopened minimum.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: CORIBA 713 SR is covered by U.S. Patent #7678201 (issued on March
16, 2010). The process is designed to remove and recover oil from sand. The product does not
react with or alter the oil. Contaminated sand is transferred into a standard sand washer filled
with 713 SR. The product is an aqueous solution that, upon contact, reduces the interfacial
tension between the oil and the sand. The oil no longer adheres to the sand and is free to float to
the surface of the processor and is removed with an auger. The cleaned sand is dried in a
centrifuge and the collected liquid is recycled back to the processor. The product has a high
vapor pressure and evaporates from the sand leaving no residue or contamination. The separated
oil is transferred to a conical vertical tower where it concentrates at the surface and is siphoned
off to be used as a fuel or sent to a refinery for further processing. The process solution that
collects in the conical tower is recycled back to the processor. The clean, dry sand can be
disposed as appropriate. Any sand that collects in the bottom of the conical tower is sent back
through the processor. The process can be set up on a beach, waste treatment facility or on a
barge for treating sensitive areas like barrier islands. The process chemical is not designed to
come into contact with any body of water. There process is not designed to treat contaminated
water. The process does not consume the process chemical. Any chemical that remains after the
sand has been cleaned can be returned to the manufacturer or sent to an appropriate waste
treatment facility.

2.	Concentration/Application Rate: CORIBA 713 SR is used at full strength. It is delivered in
aqueous solution. The application rate is 200 gallons/ton of oil-contaminated sand.

3.	Conditions for Use: CORIBA 713 SR can be applied to contaminated sand as long as the sand
mixture is not frozen. The process is effective at ambient temperature.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

CORIBA 713 SR

No. 2 Fuel Oil

CORIBA 713 SR &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

1070.00
2350.00
11.10
3.29
9.55
4.04
5.70
9.04

96-hr
48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

377

CORIBA 713 SR


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IX. PHYSICAL PROPERTIES

1.	Flash Point: 212°F

2.	Pour Point: 220°F

3.	Viscosity: 1.0 cps

4.	Specific Gravity: 0.997

5.	pH: 11.0

6.	Surface Active Agents: None

7.	Solvents: None

8.	Additives: PROPRIETARY

9.	Solubility: Miscible with water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.05

Cadmium	<0.002

Chromium	0.031

Copper	0.25

Lead	0.02

Mercury	<0.01

Nickel	<0.01

Zinc	0.25

Cyanide	<0.1

Chlorinated Hydrocarbons	<0.1

Surface Washing Agents

378

CORIBA 713 SR


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LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

7/19/2021
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-57

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: MAY 11, 2011

"JEP-MARINE CLEAN"

(aka, ECOVOOM-MARINE)

I.	NAME, BRAND, OR TRADEMARK
JEP-MARINE CLEAN

(aka, ECOVOOM-MARINE)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Nuance Solutions*

900 E. 103rd Street, Suite D
Chicago, IL 60628
Phone: (800) 621-8553
Fax:(800)621-1276
(Mr. Neil Houtsma)

(*Nuance Solutions is the manufacturer for Jubilee Environmental Products, product owner)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Jubilee Environmental Products

406 S. Boulder, Suite 820

Tulsa, OK 74103

Phone: (918) 277-1113

Fax: (918) 296-3997

E-mail: iubilinc@aol.com

Sales and Inquiries:

Phone: (918) 277-1113

Fax: (918) 296-3997

E-mail: iubilinc@aol.com

(Mr. Thomas J. Rhein, President)

Restored Cleaner LLC

2475 Fairfield Avenue

Bridgeport, CT 06605

Phone: (203) 335-9555

Fax:(203)335-9550

E-mail: info@restoredcleaner.com

Sales and Inquiries:

Phone: (203) 335-9555

Fax:(203)335-9550

E-mail: info@restoredcleaner.com

(Mr. Col ton Amster)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Respiratory protection
not required under normal conditions. Protect against generated mists using protective clothing
in order to minimize contact (i.e., boots, apron, face shield). Use safety glasses/goggles during
handling and application to prevent eye contact. Wear rubber/PVC gloves to prevent skin

Surface Washing Agents

379

JEP-MARINE CLEAN


-------
contact.

4.a. Maximum storage temperature: 90°F
4.b. Minimum storage temperature: 40°F

4.c. Optimum storage temperature range: 40 - 90°F; product freezes at 32°F
4.d. Temperatures of phase separations and chemical changes: 120°F

V. SHELF LIFE

In unopened containers, shelf life is minimum 2 years.

VI. RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be diluted with fresh or salt water, and may be applied to
any type of surfaces that have been coated with oil or other petroleum-based substances resulting
from a spill (e.g., beaches, rocks). Manual pump sprayers should be used to presoak the
contaminated areas, and pressure washers should be used to agitate the contaminated areas after
a presoak has been applied.

2.	Concentration/Application Rate: Shoreline Cleaning - presoak the surface needing to be
cleaned, using a manual pump sprayer, with a dilution rate of one (1) part to three (3) parts water
for approximately 10 to 15 minutes, without letting the product dry or evaporate. After the
contaminated areas have been presoaking for the allotted time, run a dilution rate of one (1) part
product to fifteen (15) parts water, through a pressure washer directly onto the contaminant.

3.	Conditions for Use: Option temperature range for use is 45 to 212°F. When the contaminants
have been released, they can be removed using sorbent pads, suction booms or skimmers, and
hauled away and disposed of according to local, state, and federal law. It is recommended that
for older or crustier contaminants higher pressure and stronger dilutions be used.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

JEP-MARINE CLEAN

No. 2 Fuel Oil

JEP-MARINE CLEAN &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
88.40 96-hr

153.90
2.70
1.63
3.58
2.32
8.84
14.90

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES
1. Flash Point: >100°C

Surface Washing Agents

380

JEP-MARINE CLEAN


-------
2.	Pour Point: -14°C

3.	Viscosity: 1.1 cSt

4.	Specific Gravity: 1.041

5.	pH: 11.2

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: Water

8.	Additives: CONFIDENTIAL

9.	Solubility: Miscible with water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.004
Cadmium 0.084
Chromium 0.082
Copper 0.138

Lead	<0.025

Mercury	<0.0012

Nickel	<0.025
Zinc 0.219
Cyanide 0.01

Chlorinated Hydrocarbons	<0.01

Surface Washing Agents

381

JEP-MARINE CLEAN


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

9/27/2012
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-58

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JUNE 28, 2011

"ETHOS CLEAN"

I.	NAME, BRAND, OR TRADEMARK
ETHOS CLEAN

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
MAG7 Venture Group, LLC, DBA MAG7 Technologies

1 Lepage Place, Suite 100
Syracuse, NY 13206
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Greg Goodell or Mr. Trevor Quig)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
MAG7 Venture Group, LLC, DBA MAG7 Technologies

1 Lepage Place, Suite 100
Syracuse, NY 13206
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Greg Goodell or Mr. Trevor Quig)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Move subject to fresh air. If breathing is difficult, obtain medical help.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wash affected skin area
with water. Consult physician of irritation persists. Skin irritation will not occur with most users.
Flush eyes with a large amount of water for at least 15 minutes. Consult physician if irritation
persists. Wear safety glasses and neoprene or rubber gloves during application.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: NA. Phase separation will not

Surface Washing Agents

382

ETHOS CLEAN


-------
occur within the storage range. Product should be stored out of direct sunlight unless it is in an
Ultraviolet (UV) light resistant container.

V.	SHELF LIFE

2 years in a sealed (unopened) container (tote, drum, pail) as delivered. 1 year in an opened
container).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Apply ETHOS CLEAN to oil or contaminant with sprayer, pressure
washer, mop, sponge, brush, or rags. Application times will depend on the level of contaminant
with a minimum of 30 minutes recommended soak time. The required soak time to remove oil
will vary with oil density and degree of weathering. ETHOS CLEAN separates the oil from the
physical surface to allow the oil to be sprayed off with a water rinse. ETHOS CLEAN should be
mixed into soil applications to increase the effectiveness and reduce the application time.

2.	Concentration/Application Rate: Pure concentrate can be used for heavy contamination.
Dilution ratios for most applications range from 2 to 1 (parts water to parts ETHOS CLEAN) to
10 to 1 (parts water to parts ETHOS CLEAN). Dilution ratios are dependent on the
contamination level and application with heavier crude oil spills requiring a lower dilution ratio.
Dilutions up to 50 to 1 (parts water to parts ETHOS CLEAN) can be used for lighter
contaminations and cleaning. Rinse with water after usage for residue free surface. Surface
cleaning typically requires 5 to 1 or 10 to 1 dilution ratio. These dilution ratios will require 1
gallon of ETHOS CLEAN per 250 square feet of surface area. These dilution ratios can be used
in many applications including shorelines, rocks, and beaches.

3.	Conditions for Use: Salt or fresh water (temperature ranges from 35°F to 120°F). Oil or
contaminant can be skimmed from the water or rinsed and captured into collection containers
and disposed of per local, state, and federal regulations.

Dilution	Intended Use

2:1	Heavy contamination such as oil spills

5:1	Direct application to heavily soiled areas

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

ETHOS CLEAN

No. 2 Fuel Oil

ETHOS CLEAN &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)

3960.00

96-hr

4510.00

48-hr

26.30

96-hr

4.86

48-hr

25.00

96-hr

5.00

48-hr

2.23

96-hr

7.93

48-hr

b. Effectiveness: NA

Surface Washing Agents

383

ETHOS CLEAN


-------
VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 142°F

2.	Pour Point: 30°F

3.	Viscosity: 32 SUS @60°F

4.	Specific Gravity: 1.1664 @60°F

5.	pH: 11.6

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Complete in water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound

Concentration (ppm)

Arsenic

ND

Cadmium

0.0813

Chromium

0.240

Copper

0.201

Lead

14.5

Mercury

5.0 (ppb)

Nickel

2.12

Zinc

ND

Cyanide

ND

Chlorinated Hydrocarbons

ND

Surface Washing Agents

384

ETHOS CLEAN


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

9/27/2012
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-59

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JUNE 28, 2011

"OSR-10"

I.	NAME, BRAND, OR TRADEMARK
OSR-10

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
MAG7 Venture Group, LLC, DBA MAG7 Technologies

1 Lepage Place, Suite 100
Syracuse, NY 13206
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Greg Goodell or Mr. Trevor Quig)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
MAG7 Venture Group, LLC, DBA MAG7 Technologies

1 Lepage Place, Suite 100
Syracuse, NY 13206
Phone: updated information required
Fax: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Greg Goodell or Mr. Trevor Quig)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Move subject to fresh air. If breathing is difficult, obtain medical help.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Wash affected skin area
with water. Consult physician of irritation persists. Skin irritation will not occur with most users.
Flush eyes with a large amount of water for at least 15 minutes. Consult physician if irritation
persists. Wear safety glasses and neoprene or rubber gloves during application.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: NA. Phase separation will not

Surface Washing Agents

385

OSR-10


-------
occur within the storage range. Product should be stored out of direct sunlight unless it is in an
Ultraviolet (UV) light resistant container.

V.	SHELF LIFE

2 years in a sealed (unopened) container (tote, drum, pail) as delivered. 1 year in an opened
container).

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Apply OSR-IO to oil or contaminant with sprayer, pressure washer, mop,
sponge, or brush. Application times will depend on the level of contaminant with a minimum of
10 minutes recommended soak time. The required soak time to remove oil will vary with oil
density and degree of weathering. OSR-IO separates the oil from the physical surface to allow
the oil to be sprayed off with a water rinse. OSR-IO should be mixed into soil applications and
agitated to increase the effectiveness and reduce the application time.

2.	Concentration/Application Rate: Dilution ratios for most applications range from 2 to 1 (parts
water to parts OSR-IO) to 15 to 1 (parts water to parts OSR-IO). Dilution ratios are dependent on
the contamination level and application with heavier crude oil spills requiring a lower dilution
ratio. Rinse with water after usage for residue free surface. Surface cleaning typically requires 5
to 1 or 10 to 1 dilution ratio. These dilution ratios will require 1 gallon of OSR-IO per 300 square
feet of surface area. These dilution ratios can be used in many applications including shorelines,
rocks, and beaches.

3.	Conditions for Use: Salt or fresh water (temperature ranges from 35°F to 120°F). Oil or
contaminant can be skimmed from the water or rinsed and captured into collection containers
and disposed of per local, state, and federal regulations.

Dilution	Intended Use

2:1	Heavy/severe contamination such as oil spills

5:1 to 10:1	Moderate contamination

15:1 to 30:1	Light contamination

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

Species

LC50 (ppm)



OSR-10

Menidia beryllina

385.00

96-hr



Mysidopsis bahia

399.00

48-hr

No. 2 Fuel Oil

Menidia beryllina

26.30

96-hr



Mysidopsis bahia

4.86

48-hr

OSR-10 &

Menidia beryllina

16.00

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

4.77

48-hr

Reference Toxicant (SDS)

Menidia beryllina

2.23

96-hr



Mysidopsis bahia

7.93

48-hr

b. Effectiveness: NA

Surface Washing Agents

386

OSR-10


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VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: 143°F

2.	Pour Point: 20°F

3.	Viscosity: 37 SUS @60°F

4.	Specific Gravity: 1.1672 @60°F

5.	pH: 11.5

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Complete in water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.209

Copper	0.150

Lead	7.57

Mercury	6.8 (ppb)

Nickel	1.20

Zinc	ND

Cyanide	ND

Chlorinated Hydrocarbons	ND

Surface Washing Agents

387

OSR-10


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TECHNICAL PRODUCT BULLETIN #SW-60

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 13, 2011

"ACCELL CLEAN® SWA"

I.	NAME, BRAND, OR TRADEMARK
ACCELL CLEAN® SWA

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Advanced BioCatalytics Corporation

18010 Skypark Circle, #130
Irvine, California 92614-6456
Office Phone: (949) 771-0209
General E-mail: info@abiocat.com
Website: www.abiocat.com
Product Management:

Mobile: (949) 981-6510
E-mail: cpodella@abiocat.com
(Mr. Carl Podella)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Advanced BioCatalytics Corporation

18010 Skypark Circle, #130
Irvine, California 92614-6456
Office Phone: (949) 771-0209
General E-mail: info@abiocat.com
Website: www.abiocat.com
Product Management:

Mobile: (949) 981-6510
E-mail: cpodella@abiocat.com
(Mr. Carl Podella)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Use in well-ventilated area.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Protective clothing is
recommended. Avoid eye contact. In case of eye contact, immediately flush with large amounts
of water for at least 15 minutes. Get prompt medical attention. Avoid direct contact with skin and
clothing. In case of skin contact, immediately flush with large amounts of water. Remove
contaminated clothing, including shoes, after flushing has begun. If irritation persists, seek
medical attention. For open systems were contact is likely, wear long sleeve shirt, chemical
resistant gloves, and protective chemical goggles.

Surface Washing Agents

388

ACCELL CLEAN® SWA


-------
4.a. Maximum storage temperature: 130°F/55°C

4.b. Minimum storage temperature: 30°F/-1°C

4.c. Optimum storage temperature range: 40°F to 100°F/4°C to 38°C

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

The shelf life of unopened drums of ACCELL CLEAN® SWA is unlimited. Containers should
always remain capped when not in use to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Spray ACCELL CLEAN® SWA onto oil-contaminated shorelines,
mangroves, or seagrasses full strength as applied. Allow to soak for 15-30 minutes. Rocks may
be scrubbed with a stiff bristle brush where appropriate. Rinse with fresh or salt water as
appropriate. For weathered crude oil on sand, transfer oil-contaminated sand to sand washing
equipment. Agitate sand/ACCELL CLEAN® SWA solution. ACCELL CLEAN® SWA will lift
the oil from the sand due to its low interfacial tension. Remove water from sand by centrifuge.

2.	Concentration/Application Rate: Recommended application rate is 1 gallon per 100 square
feet, dependent on the amount of oil and the degree of weathering. For weathered crude oil from
sand, prepare a cleaning solution of 0.25%-2.0% ACCELL CLEAN® SWA using fresh or salt
water.

3.	Conditions for Use: Collect the oil/product residue from the water's surface using skimmers,
absorbent pads, or other conventional means. Dispose of used, clean up residue in accordance
with local, state, and federal regulations. Dispose of clean sand as appropriate and ACCELL
CLEAN® SWA solution can be recycled after centrifuge.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

Species

LC50

(ppm)

ACCELL CLEAN® SWA

Menidia beryllina

24.12

96-hr



Mysidopsis bahia

59.46

48-hr

No. 2 Fuel Oil

Menidia beryllina

17.13

96-hr



Mysidopsis bahia

2.92

48-hr

ACCELL CLEAN® SWA &

Menidia beryllina

12.25

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.25

48-hr

Reference Toxicant (DDS)

Menidia beryllina

10.00

96-hr



Mysidopsis bahia

29.00

48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES
1. Flash Point: >180°F/82°C

Surface Washing Agents

389

ACCELL CLEAN® SWA


-------
2.	Pour Point: 10°F/-12°C

3.	Viscosity: 68 SUS @60°F

4.	Specific Gravity: 1.0141 @60°F

5.	pH: 8.12

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: CONFIDENTIAL

8.	Additives: CONFIDENTIAL

9.	Solubility: Soluble in fresh or seawater

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<1.00

Cadmium	<0.50

Chromium	<1.00

Copper	<2.50

Lead	<1.00

Mercury	<0.020

Nickel	<4.00

Zinc	<6.00

Cyanide	<1.00

Chlorinated Hydrocarbons	ND

Surface Washing Agents

390

ACCELL CLEAN® SWA


-------
LAST COMMUNICATION WITH MANUFACTURER:
LAST ATTEMPT:

10/19/2016
7/27/2022

TECHNICAL PRODUCT BULLETIN #SW-61

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: OCTOBER 13, 2011

"EPA OIL FIELD SOLUTION™"

(aka, HYDRO-CLEAN™, GLOBAL ENVIRONMENTAL CLEANER™, AW AN PRA OIL
FIELD SOLUTION™)

I.	NAME, BRAND, OR TRADEMARK
EPA OIL FIELD SOLUTION™

(aka, HYDRO-CLEAN™, GLOBAL ENVIRONMENTAL CLEANER™, AW AN PRA OIL

FIELD SOLUTION™)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Environmental Protection Associates, Inc.

2578 Enterprise Road, Suite 141
Orange City, FL 32763
Phone: updated information required
E-mail: updated information required
Website: updated information required
(Mr. Nathan Hall)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
International Green Building Group, Inc.	AW AN International General Trading
10800 Main Street, Suite 150 P.O. Box 75352

Fairfax, VA 22030	Kingdom of Bahrain

Phone: (202) 300-8324	Phone: 973-173-111-28

E-mail: info@internationalgreenbuildinggroup.com Fax: 973-172-950-05
Website: updated information required	E-mail: iames@awanpra.com

Website: www.awangroups.com
Website: updated information required
(Mr. James Gard)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however goggles are recommended. If eye or skin irritation occurs, flush
with plenty of fresh water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

Surface Washing Agents

391

EPA OIL FIELD SOLUTION™


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4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

Unlimited in sealed polydrums or totes (as delivered). Avoid direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: Product may be applied to surfaces for removal of oils. Select proper
dilution depending on material surface prior to application. For treatment of large areas, properly
diluted product may be applied by spraying with a pressure washer, portable fire pump, or any
other suitable pump with seawater or freshwater suction that is equipped with a chemical
inductor or feed pump. For smaller areas, properly diluted product may be applied with scrubber,
mop, cloth or damp sponge. Apply liberally, adjusting dilution on site as necessary. For
shorelines, mangroves, and seagrasses product is sprayed directly on the oiled rocky surfaces full
strength as supplied. After a soak time of zero to 30 minutes, the cleaner and oil released from
the shoreline surface can be collected and disposed. The soak time may vary with temperature,
oil density, and degree of weathering.

2.	Concentration/Application Rate: For heavily weathered oil on rocks, a diluted solution of 3
parts water to 1 part product is recommended. For heavily weathered oil on beaches/sand, a
diluted solution of 5 parts water to 1 part product is ideal. For removing oil from vegetation, a
diluted solution of 10-20 parts water to 1 part product is preferred. Product may be diluted with
either salt or fresh water. Warmer water (greater than 78°F) and/or good agitation during
application will require less of the product.

3.	Conditions for Use: Best results are obtained by allowing diluted solution to soak for at least
30 minutes to soften the oil deposits. Reapplication may be necessary in severely contaminated
areas. A sorbent boom or vacuum suction equipment should be positioned to collect the washed
off effluent. When proper containment equipment is in place and a soaking period of at least 30
minutes has been achieved, a diluted solution of 20 parts water and 1 part product should be
applied at mid-pressure (approximately 100 PSI). Adjust pressure and angle of the hose sprayer
to achieve optimum results, adjusting the dilution as necessary on site. Product and effluent
should be vacuumed up or absorbed in absorbent boom and disposed of according to local, state,
and federal regulations. EPA Oil Field Solution™ is useful on shorelines using fresh or salt
water. It can be used on all types of oil including heavily weathered and emulsified ("chocolate
mousse") containing up to 50 percent water.

Surface Washing Agents

392

EPA OIL FIELD SOLUTION™


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

EPA OIL FIELD SOLUTION™
No. 2 Fuel Oil

EPA OIL FIELD SOLUTION™ &
No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
113.76 96-hr

114.60
3.00
1.41
2.94
1.12
12.25
12.06

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >95°F

2.	Pour Point: -2°F

3.	Viscosity: 1.137368 SUS @40°F

4.	Specific Gravity: 1.11 @60°F

5.	pH: 13.4

6.	Surface Active Agents: Nonionic, proprietary, surfactants

7.	Solvents: Proprietary

8.	Additives: None

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.200

Cadmium	<0.0600

Chromium	<0.300

Copper	<0.300

Lead	<0.200

Mercury	<1.00 (ug/1)

Nickel	<0.500
Zinc 2.31

Cyanide	<0.0100

Chlorinated Hydrocarbons	<250 (ug/1)

Surface Washing Agents

393

EPA OIL FIELD SOLUTION™


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TECHNICAL PRODUCT BULLETIN #SW-62
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: MARCH 5, 2012
"PETROMAX PSC 3"

(aka, PETROMAX SOIL CLEANING AND WASHING AGENT)

I.	NAME, BRAND, OR TRADEMARK
PETROMAX PSC 3

(aka, PETROMAX SOIL CLEANING AND WASHING AGENT)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Alfaluz S.A.

Potosi 1517
Carrasco, Montevideo
Uruguay

Phone: 598-2-604-1006
Unites States: (305) 600-4927
Fax: (508)256-8318
E-mail: svonbergen@alfaluz.net
Website: www.alfaluz.net
(Mr. Scot von Bergen)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Alfaluz Inc.

1875 Post Oak Park Drive, Suite 523

Houston, Texas 77027

Phone: (832) 272-1816

Fax: (508) 256-8138

E-mail: mvonbergen@alfaluz.net

(Mrs. Marina von Bergen)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-hazardous)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: No special equipment
or clothing required; however, goggles are recommended. If eye or skin irritation occurs, flush
with plenty of fresh water.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days
4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 40°F to 120°F

4.d. Temperatures of phase separations and chemical changes: Stable

Surface Washing Agents

394

PETROMAX PSC 3


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V.	SHELF LIFE

Unlimited when stored in unopened, sealed 5 gallon containers, 55 gallon drums, poly drums, and
totes.

VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: PETROMAX PSC 3's mechanism of action is to reverse the charge of
the particles (sand) holding the hydrocarbons, in such a way that the hydrocarbons and the
particles reject each other thus allowing the hydrocarbons to be easily separated, removed, and
collected. This is because the separated hydrocarbons maintain their globular integrity and are
not dispersed nor solubilized into the water column.

PETROMAX PSC 3 is applied via hydroblaster directly to the contaminated sand/soil and as it
becomes fluidized it is sucked through a four inch hose into a mobile containment tank set up for
the purpose at the job site. The contaminated material is cleaned through a three phase separation
process:

a)	Solids Recovery: Once in the containment tank, the cleaned sand and soil particles
precipitate immediately to the bottom, from which they are extracted via a slew-valve to
secondary containment. Any entrained water within this containment is further recovered
for reuse according to local, state, and federal regulations.

b)	Oil Recovery: During this process the hydrocarbons float to the surface of the tank and
are removed by skimming. These removed hydrocarbons are collected and are sent to a
refinery for processing.

c)	PETROMAX PSC 3/Water Recovery: This leaves only the used PETROMAX PSC
3/water solution in the tank, which can be reused or disposed of according to local, state,
and federal regulations. The remaining water may contain some light particles in
suspension. These particles are easily precipitated into cake residues which are then
collected. The cake residues typically contain a water content below 10%. They can be
dried in open air pits with plastic protection underneath or in 15 yard roll-off containers.
Any contaminated water should be collected and sent to a standard water treatment
facility.

2.	Concentration/Application Rate: PETROMAX PSC 3 should be applied via hydroblaster lance
with minimum 3200 psi pressure and 4-15 gallons per minute flow depending on material to be
treated. For smaller spills, a smaller hydroblaster sprayer may be used, mixing fresh or salt water
according to availability, and depending on the oil composition and viscosity in the contaminated
sand and soil being treated. For large scale soil remediation and cleaning or soils and sands
contaminated with heavy crude, direct PETROMAX PSC 3 directly on the spill (contaminated)
material using a hydroblaster lance at a minimum pressure of 3500 psi, with a dilution ratio of
approximately 1:10 (product:water). Lighter oil soil contamination will require a 1:20 to 1:30
product to water dilution ratio with pressures at 2800 psi minimum. Warmer water (greater than
70°F) may require less PETROMAX PSC 3.

3.	Conditions for Use: A sorbent boom should be positioned during use to contain any runoff and
the collected material should be disposed of according to local, state, and federal regulations.

Surface Washing Agents

395

PETROMAX PSC 3


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VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

PETROMAX PSC 3

No. 2 Fuel Oil

PETROMAX PSC 3 &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SLS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
20332.19 96-hr
13460.87
1.90

1.68
1.99
1.00
12.25
12.35

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >185°F

2.	Pour Point: +22°F

3.	Viscosity: 1.5 est @40°C

4.	Specific Gravity: 1.08 @60°F

5.	pH: 13.23

6.	Surface Active Agents: Anionic, proprietary

7.	Solvents: None

8.	Additives: Proprietary

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.121

Cadmium	0.332

Chromium	0.067

Copper	<0.100

Lead	0.197

Mercury	<0.50 (ug/1)

Nickel	<0.100

Zinc	<0.100

Cyanide	<0.010

Chlorinated Hydrocarbons	<5.00 (ug/1)

Surface Washing Agents

396

PETROMAX PSC 3


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TECHNICAL PRODUCT BULLETIN #SW-63

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 12, 2012

"GREEN TECHNOLOGIES SOLUTIONS-OIL RECOVERY (GTS-OR)"

I.	NAME, BRAND, OR TRADEMARK

GREEN TECHNOLOGIES SOLUTIONS-OIL RECOVERY (GTS-OR)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
International Technologies and Services, Inc.

29258 Palos Verdes Drive East

Rancho Palos Verdes, CA 90275

Phone: (310) 749-4487

E-mail: pilarladvbug@itsenvironmental.com

Website: www.ITSEnvironmental.com

(Ms. Pilar Ortega)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
International Technologies and Services, Inc.

29258 Palos Verdes Drive East

Rancho Palos Verdes, CA 90275

Phone: (310) 749-4487

E-mail: pilarladybug@itsenvironmental.com

Website: www.ITSEnvironmental.com

(Ms. Pilar Ortega)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Handle in well ventilated space.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Product may cause
minor irritation, so avoid eye and skin contact by wearing protective goggles, impermeable
protective gloves, and protective clothing while handling the product. Wash contaminated
clothing with soap and water, and dry prior to reuse. In case of contact, flush with large amounts
of water for at least 15 minutes. Product may harmful if inhaled. In case of inhalation, move
affected person to fresh air, and call a physician. Product may be harmful if swallowed. In case
of ingestion, induce vomiting, give water, and call a physician.

4.a.	Maximum storage temperature: 120°F
4.b. Minimum storage temperature: 30°F

4.c. Optimum storage temperature range: >50°F to <100°F

4.d. Temperatures of phase separations and chemical changes: None

V.	SHELF LIFE

One year minimum when stored between 50°F and 100°F.

Surface Washing Agents

397 GREEN TECHNOLOGIES SOLUTIONS-
OIL RECOVERY (GTS-OR)


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VI.	RECOMMENDED APPLICATION PROCEDURES

1.	Application Method: GTS-OR may clean oil from beaches, rocks, riprap, pilings, and
seawalls. GTS-OR application method can be adjusted depending on the scale and type of area to
be cleaned. For large areas, GTS-OR can be sprayed from water trucks or water boats equipped
with pumps, hoses, and nozzles to deliver the product as an aerial spray. The pump should be
equipped with a chemical inductor or feed pump. In smaller applications, GTS-OR can be
applied directly onto oiled surfaces using a pressure washer, steam powered unit, fire hose, or
chemical boom sprayer with nozzles at mid-pressure (i.e., approximately 100 PSI) that produce a
shearing action. For small applications, the product may be applied with mops, cloth, or damp
sponges. For application in tidally influenced areas and to maximize contact time, GTS-OR
should be applied during ebb tide (i.e., receding). Oil trapped between rocks or in crevices may
be released over several days, requiring containment devises to be left in place.

2.	Concentration/Application Rate: For heavily weathered oil on rocks, a diluted solution of 15
parts water to 1 part product is recommended. For heavily weathered oil on beaches/sand, a
diluted solution of 10 parts water to 1 part product is ideal. For lightly-to-moderately oiled
shorelines, mangroves, and seagrasses, the product should be sprayed directly to the affected
surface at a 1:20 dilution ratio; a 1:10 dilution ratio is preferred for heavily oiled areas.

3.	Conditions for Use: GTS-OR may be used in freshwater, estuarine, and marine environments.
In all applications, the product may be diluted with either salt or fresh water, and the mixture
should be allowed to penetrate and dissolve weathered petroleum for at least 30 minutes. Cold
weather applications will require more contact time. Reapplication may be necessary for heavily
oiled areas. The product may be used on both lighter oils (e.g., No. 2 Fuel Oil) and heavy ends
(e.g., crude oil, No. 6 Fuel Oil). Prior to application, booms, oil skimmers, or other appropriate
containment and collection mechanism should be deployed and operational. Collected product
and oil mixture should be disposed of according to local, state, and federal regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Materials Tested

Species

LC50

(ppm)

GTS-OR

Menidia beryllina

3930

96-hr



Mysidopsis bahia

916

48-hr

No. 2 Fuel Oil

Menidia beryllina

8.16

96-hr



Mysidopsis bahia

4.47

48-hr

GTS-OR &

Menidia beryllina

5.77

96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.18

48-hr

Reference Toxicant (SDS)

Menidia beryllina

1.24

96-hr



Mysidopsis bahia

4.77

48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

Surface Washing Agents

398 GREEN TECHNOLOGIES SOLUTIONS-
OIL RECOVERY (GTS-OR)


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IX. PHYSICAL PROPERTIES

1.	FlashPoint: 171°F

2.	Pour Point: 35°F

3.	Viscosity: 8.5 cSt @40°C

4.	Specific Gravity: 1.009 @60°F

5.	pH: 9.0

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility: Soluble in water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

Concentration (ppm)

0.0084

<0.004

0.00064

0.180

0.00025

<0.00010

0.0012

0.017

<0.200

<2.5

Surface Washing Agents

399 GREEN TECHNOLOGIES SOLUTIONS-
OIL RECOVERY (GTS-OR)


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TECHNICAL PRODUCT BULLETIN #SW-64

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: JULY 9, 2013

"SIMPLE GREEN® 2013 Reformulation"

I.	NAME, BRAND, OR TRADEMARK
SIMPLE GREEN® 2013 REFORMULATION
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Sunshine Makers, Inc.

15922 Pacific Coast Highway

Huntington Beach, CA 92649

Phone: (800) 228-0709

Phone: (562) 795-6000

Fax: (562) 592-3830

E-mail: LLorincz@simplegreen.com

(Ms. Laura Lorincz)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Sunshine Makers, Inc.

15922 Pacific Coast Highway

Huntington Beach, CA 92649

Phone: (800) 228-0709

Phone: (562) 795-6000

Fax: (562) 592-3830

E-mail: LLorincz@simplegreen.com

(Ms. Laura Lorincz)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Not expected to cause respiratory irritation. However, use in well ventilated areas.
If adverse effect occurs, move to fresh air.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Not expected to cause
eye irritation. However, use protective glasses if splashing or spray-back is likely. If adverse
effect occurs, flush eyes with water. Not expected to cause skin irritation. However, dermally
sensitive users may experience dry skin and should use protective gloves. If adverse effect
occurs, rinse skin with water. General hygiene considerations include washing hands thoroughly
after handling and before eating or drinking. Ensure adequate ventilation. Keep out of reach of
children. If ingested, drink plenty of water to dilute.

4.a.	Maximum storage temperature: 109°F
4.b. Minimum storage temperature: 41°F

Surface Washing Agents

400

SIMPLE GREEN®
2013 REFORMULATION


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4.c. Optimum storage temperature range: 42°F to 108°F

4.d. Temperatures of phase separations and chemical changes: SIMPLE GREEN® is stable and
phase separation will not occur at temperatures within the maximum and minimum storage
temperatures. If separation occurs, mix the product for reconstitution.

V.	SHELF LIFE

SIMPLE GREEN® has a 5-year shelf life. Keep away from heat, sparks, open flame and direct
sunlight. Do not pierce any part of the container. Keep container tightly closed. Keep in a cool
dry area. Avoid prolonged exposure to direct sunlight. Do not store at temperatures above 109°F
(42.7°C).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Spray or apply on oily surfaces (e.g., beaches, rocks, shorelines, pilings,
etc.).

2.	Concentration/Application Rate:

a)	Mix SIMPLE GREEN® in clean water at recommended concentration for strength of surface
being cleaned:

Degree that Surface is Covered in Oil	Concentration of Simple Green®

HEAVY - fresh, thick, viscous oil; porous surfaces Full strength to 25%

MEDIUM - weathered, thinner coats of oil; non- 25% to 10%

porous surfaces - use pressure washer equipment

LIGHT - very light oil film; non-porous surfaces Less than 10%

b)	Apply SIMPLE GREEN® or diluted solution of Simple Green® to oiled surface via sponge,
mop, coarse spray, foaming applicator, or pressure washer.

c)	Whenever possible, allow several minutes (5-10) of contact time to loosen oil. Do not allow
product to dry on the surface or it will be difficult to remove.

d)	Wash and scrub as necessary.

e)	Rinse cleansed surfaces with clean water. Whenever possible, rinse should enter a
pretreatment system (e.g., clarifier, oil/water separator, municipal sanitary sewer) before
repurposing.

3.	Conditions for Use: SIMPLE GREEN® can be used in freshwater, estuarine, and marine
environments at all temperatures. Prior to application, booms, oil skimmers, or other appropriate
containment and collection mechanism should be deployed and operational. Collected product
and oil mixture should be disposed of according to local, state, and federal regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested Species	LC50 (ppm)

SIMPLE GREEN® Menidia beryllina	735.00 96-hr

Mysidopsis bahia	541.00 48-hr

No. 2 Fuel Oil Menidia beryllina	26.40 96-hr

Mysidopsis bahia	3.37 48-hr

Surface Washing Agents

401

SIMPLE GREEN®
2013 REFORMULATION


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SIMPLE GREEN® & No. 2 Fuel Oil (1:10) Menidia beryllina	28.50 96-hr

Mysidopsis bahia	5.05 48-hr

Reference Toxicant (DSS) Menidia beryllina	1.69 96-hr

Mysidopsis bahia	6.60 48-hr

NOTE: This toxicity data was derived using the concentrated product.	See Section VI of this
bulletin for information regarding the manufacturer's recommendations for concentrations and
application rates for field use.
b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS

SIMPLE GREEN® contains no microorganisms, enzymes, or biological material.

IX.	PHYSICAL PROPERTIES

1.	Flash Point (ASTM 92): 98°C

No Flash Point seen at or below 212°F (ASTM 93)

2.	Pour Point: 0°C

3.	Viscosity: <2.0 mm2/s at 40°C

4.	Specific Gravity: 1.0283 g/ml at 60°F

5.	pH: 9.0

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility: 100% soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0031

Cadmium	<0.0005

Chromium	0.013

Copper	<0.0025

Lead	<0.0005

Mercury	0.0016

Nickel	0.0054

Zinc	0.016

Cyanide	<0.08

Chlorinated Hydrocarbons	<5

Surface Washing Agents

402

SIMPLE GREEN®
2013 REFORMULATION


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TECHNICAL PRODUCT BULLETIN #SW-65
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: JANUARY 23, 2014
"NONTOX™ SURFACE WASHING AGENT"

I. NAME, BRAND, OR TRADEMARK
NONTOX™ SURFACE WASHING AGENT
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Bio-Organic Catalyst, Inc. (wholly owned subsidiary of Neozyme International, Inc.)

711 West 17th Street, Suite E-6
Costa Mesa, CA 92627
Phone: (949) 515-1301
Phone: (800) 982-8676
Fax: (949)515-1314
E-mail: parker@bio-organic.com
Website: www.bio-organic.com
(Mr. Parker Dale, President)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Government Logistics Solutions	Rolling Hills Construction and Demolition
3540 Chaneyville Road Recycling Center

Owings, MD 20736	6990 Rolling Hills Road

Phone: (410) 286-0098	Pensacola, FL 32505

Fax: (301) 812-2878	Phone: (850) 477-2687

(Mr. Charles M. Baker, Retired USAF (SMSgt (Mr. John Levitan - Mobile (850) 497-2724)

sel), President)	(Mr. Scott Miller - Mobile (850) 723-5715)

(Kelly Davis - (240) 691-3946)	(Mr. Charlie Davidson - Mobile (850) 776-2852)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: >93°C

2.	Ventilation: None required. No respiratory protection required.

3.	Skin and eye contact; protective clothing; treatment in case of contact: The use of protective
eyewear and rubber gloves is recommended under good manufacturing practices.

4.a.	Maximum storage temperature: 55°C
4.b. Minimum storage temperature: 2°C

4.c. Optimum storage temperature range: 25°C to 40°C

4.d. Temperatures of phase separations and chemical changes: No phase separations or chemical
changes observed under optimum storage temperatures.

Surface Washing Agents

403

NONTOX™
SURFACE WASHING AGENT


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V.	SHELF LIFE

A minimum of two (2) years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: For general use apply the product by spray, mop or with standard steam
and pressure wash cleaning equipment. It can also be applied using a foam generator or any
convenient sprayer. Product can be used as is or by using heat and pressure or mechanical
scrubbing. Rinse thoroughly with salt or fresh water for a residue-free surface. For direct
applications foaming will be most effective as it will allow more contact time for the product to
work. In a foam-cleaning application operation, the surface to be cleaned will be thoroughly
covered with foam and allowed to stand for several minutes. The foam is rinsed away with clean
water using a high pressure washer. The product can be applied with a variety of spraying or
washing equipment, depending on the type and scale of the shoreline or beach to be cleaned. For
large areas, such as beaches, the product can be sprayed from water trucks or other vehicles
equipped with pumps, hoses and nozzles to aerially deliver the product. On smaller oily surfaces,
the product can be applied with hand sprayers or portable pumps may be used to spray directly
onto the contaminated areas.

2.	Concentration/Application Rate: For spills on shorelines and beaches, the product can be used
at a dilution of 1:17 parts product to water using salt or fresh water. After application, the
product should be allowed to penetrate and dissolve the oily surface for up to 30 minutes. Longer
is preferable to maximize contact time. For light cleaning use a ratio up to 1:50 parts product to
water. For heavy cleaning use a ratio up to 1:17 parts product to water. Dose rates may vary
depending on type and amount of petroleum spilled, and other site conditions such as water,
temperatures and porosity of shoreline. Cold weather applications will require more contact time
before initiating recovery.

3.	Conditions for Use: The product can be used on sand beaches, gravel, cobble, and coarse sand
and rocky shores. Water salinity should not negatively impact product use. Water temperatures
below 2°C may impact application. Aged or highly viscous concentrations of hydrocarbons my
require presoaking prior to removal. The treated product can be collected and removed by
several means including, but not limited to, sorbent pads, oil skimmers, collection booms, or
other appropriate containment and collection mechanism. All oily water mixtures should follow
disposal procedures in accordance with current local, state and federal regulations.

Surface Washing Agents

404

NONTOX™
SURFACE WASHING AGENT


-------
VII. TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested

NONTOX™ SURFACE WASHING AGENT
No. 2 Fuel Oil

NONTOX™ SURFACE WASHING AGENT
& No. 2 Fuel Oil (1:10)

Reference Toxicant (SLS)

b.	Effectiveness: NA

Species

LC50 (ppm)

Menidia beryllina

203.

.04

96-hr

Mysidopsis bahia

316.

.23

48-hr

Menidia beryllina

2.

.51

96-hr

Mysidopsis bahia

2.

.24

48-hr

Menidia beryllina

3.

.29

96-hr

Mysidopsis bahia

2.

.19

48-hr

Menidia beryllina

12.

.25

96-hr

Mysidopsis bahia

12.

.08

48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES
2.Flash Point (ASTM 92): >93°C

2.	Pour Point: 2.22°C

3.	Viscosity: 2.3373 cST @ 40°C

4.	Specific Gravity: 1.005 at 68°F

5.	pH: 3.46

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: None

8.	Additives: CONFIDENTIAL

9.	Solubility: 100% soluble

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.0100

Cadmium	<0.0050

Chromium	0.1515

Copper	0.1530

Lead	<0.0100

Mercury	<0.5000 ug/L

Nickel	<0.0250

Zinc	4.781

Cyanide	<0.0100

Chlorinated Hydrocarbons	<2.50

Surface Washing Agents

405

NONTOX™
SURFACE WASHING AGENT


-------
LAST COMMUNICATION WITH MANUFACTURER:

LAST ATTEMPT:

TECHNICAL PRODUCT BULLETIN #SW-66
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: MAY 7, 2015
"FORMULA 206-lx BIO-WASH™"

(aka, CAST OFF™, FORMULA 206-lx)

I.	NAME, BRAND, OR TRADEMARK
FORMULA 206-IX BIO-WASH™

(aka, CAST OFF™, FORMULA 206-lx)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Natural Soap Formulas, Inc.

3200 S Andrews Avenue, Suite 113
Fort Lauderdale, FL 33316
Phone: updated information required
E-mail: updated information required
(Ms. Kaylin D'Aire)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Natural Soap Formulas, Inc.

3200 S Andrews Avenue, Suite 113
Fort Lauderdale, FL 33316
Phone: updated information required
E-mail: updated information required
(Ms. Kaylin D'Aire)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable (DOT: Non-Hazardous)

2.	Ventilation: Normal ventilation is adequate. No respiratory protection is required. If
respiratory irritation or distress occurs, remove exposed person to fresh air. Seek medical
attention if respiratory irritation or distress continues.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Protective eyewear is
advisable for operator's comfort. If eye irritation occurs, flush eyes with water. After initial
flushing, removal any contact lenses and continue flushing for 1 minute. Please seek medical
attention, if eye irritation symptoms persist or if there are additional concerns. Wash hands after
handling. If ingested, drink 2-4 glasses of water and allow the product to pass through the
digestive system naturally. Ingesting large amounts may cause gastrointestinal distress due to
emulsification of grease and oil in the digestive tract. Please seek medical attention, if symptoms
persist of if there additional concerns.

3/16/2016
7/27/2022

Surface Washing Agents

406

FORMULA 206-IX BIO-WASH™


-------
4.a. Maximum storage temperature: 120°F continuous, 130°F up to 5 days

4.b. Minimum storage temperature: 30°F

4.c. Optimum storage temperature range: 40°F to 110°F

4.d. Temperatures of phase separations and chemical changes: Stable

V.	SHELF LIFE

5 years in sealed poly drums or IBC totes (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: FORMULA 206-lx BIO-WASH™ may be applied to hard surfaces
including beaches, shorelines, and rocks; specifically to aid in the removal of oil and oil
saturated soiling. Product may be applied by spray, high pressure wash, mop, scrub brush, cloth
or sponge. Once applied to target surface, allow for a 5 to 30 minute dwell time, the product may
be agitated using suitable physical methods (i.e., scrubbing to increase effectiveness). For large
areas such as shorelines, product can be applied by vehicle or boat; spraying from fire eduction
systems or boom system, hand-held or backpack sprayers, garden type sprayers, or from hoses
attached to small pumps through power washers, fire pump or other portable pump with suction
that is equipped with a chemical inductor or feed pump. After application, the removal of oil or
oil saturated soiling can be done by rinsing with water where practicable followed by removal
with physical methods, such as sorbent pads, mop or vacuum application to prevent
contamination to open water. Ensure boom containment continues to be in place during
oil/product removal procedures.

2.	Concentration/Application Rate: FORMULA 206-lx BIO-WASH™ is typically diluted with
using tap-water at ambient temperature; and can be diluted with sea water or any other suitable
field expedient water source. The product is not affected by salinity or hard water dilution. Apply
using a typical dilution ratio of 1:10 in the first instance. Product dilution varies with the severity
of the contamination, contaminant viscosity, area of application and porosity, and nature of the
surface to be decontaminated. A dilution ratio ranging from 1:5 to 1:200 is recommended for this
product, there is no specific application rate; however, for large area application, 15 to 50 U.S.
gallons per acre can be considered optimal. During application, the rate and concentration of the
product can be adjusted to suit the cleaning effect desired.

3.	Conditions for Use: FORMULA 206-lx BIO-WASH™ is most effective on hydrocarbon and
bio-organic soiling on hard surfaces including beaches, shorelines, and rocks. A sorbent boom or
other containment equipment should be positioned prior and remain in place during product use
to collect runoff from application and removal operations. Collect and contain runoff from
oil/product mixture and dispose of such material in accordance with local, state, and federal
regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Surface Washing Agents

407

FORMULA 206-IX BIO-WASH™


-------
Material Tested Species	LC50 (ppm)

FORMULA 206-lx BIO-WASH™ Menidia beryllina	157.00 96-hr

Mysidopsis bahia	123.00 48-hr

No. 2 Fuel Oil Menidia beryllina	3.60 96-hr

Mysidopsis bahia	5.80 48-hr

FORMULA 206-lx BIO-WASH™ & Menidia beryllina	3.90 96-hr

No. 2 Fuel Oil (1:10) Mysidopsis bahia	4.10 48-hr

Reference Toxicant (SDS) Menidia beryllina	10.00 96-hr

Mysidopsis bahia	19.00 48-hr

b. Effectiveness: NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

3. Flash Point (ASTM 93): 130°F

2.	Pour Point (D2500): 30°F

3.	Viscosity (ASTMD88): 26 SUS @ 100°F

4.	Specific Gravity (ASTM D1217): 1.0137 g/ml at 60°F

5.	pH (EPA 9040C): 10.6

6.	Surface Active Agents: Natural fatty acid soaps

7.	Solvents: Hydrofurfuryl Alcohol

8.	Additives: NA

9.	Solubility: Miscible in oil, water, and solvents

X.	ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	ND

Cadmium	ND

Chromium	0.0173

Copper	0.115

Lead	ND

Mercury	ND

Nickel	0.160

Zinc	0.556

Cyanide	ND

Chlorinated Hydrocarbons	ND

Surface Washing Agents

408

FORMULA 206-IX BIO-WASH™


-------
TECHNICAL PRODUCT BULLETIN #SW-67
USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION
ORIGINAL LISTING DATE: AUGUST 3, 2015
"RHAMNOWASH 10"

I.	NAME, BRAND, OR TRADEMARK
RHAMNOWASH 10

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Rhamnolipid, Inc.

511 West Bay Street, Suite 350

Tampa, FL 33606

Phone: (917) 576-7381

Direct: (704) 564-6445

E-mail: greccosg@rhamnolipid.com

Website: http://www.rhamnolipid.com

(Mr. Samuel G. Grecco)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Rhamnolipid Companies, Inc.

511 West Bay Street, Suite 350

Tampa, FL 33606

Phone: (917) 576-7381

Direct: (704) 564-6445

E-mail: kdesanto@rhamnolipid.com

Website: http://www.rhamnolipid.com

(Mr. Keith DeSanto)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO, Non-flammable; DOT, Non-Hazardous

2.	Ventilation: Inhalation causes irritation. Use in properly ventilated areas, with approved
respiratory mask and goggles. Avoid creating mist where possible. If inhaled, allow plenty of
fresh air and loosen clothing around neck. Contact physician immediately.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Exposure to skin can
cause irritation if person has a history of dermal allergic reaction. Limit exposure and use rubber
gloves. Wash with soap and water. If product comes in contact with the eyes, excess redness and
swelling of the conjunctiva may occur. Causes moderate to severe irritation, which is
experienced as discomfort or pain, excessive blinking and tear production, with marked
excessive redness and swelling. Corneal injury may occur. Immediately flush with water for at
least 15 minutes. DO NOT remove contact lenses, if worn. Obtain medical attention without
delay, preferably from an ophthalmologist. To avoid eye contact, wear goggles or a face shield.

Surface Washing Agents

409

RHAMNOWASH 10


-------
Ingestion of product can lead to nausea or diarrhea. If ingested, give two glasses of water to

dilute product. DO NOT induce vomiting. Contact physician immediately. Treat as you would

any chemical or biological material. Always wash hands thoroughly after use. Follow product

sheets and SDS instructions.

4.a. Maximum storage temperature: 105°F

4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: 35°F to 75°F

4.d. Temperatures of phase separations and chemical changes: Phase separation may occur over
time, but mild agitation will reconstitute mixture.

V.	SHELF LIFE

The shelf life of unopened containers (i.e., drums, totes, etc.) of RHAMNOWASH 10 exceeds
five (5) years. Containers should always be capped when not in use to prevent spillage and/or
contamination.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: RHAMNOWASH 10 can remove oil (e.g., crude, different grades of fuel
oil, gasoline, and other petrochemicals) from soil, shorelines, sandy beaches, mangroves, or sea
grasses. The product may be applied by hand or using mechanical sprayers, pressure washers, or
mechanical soil washing equipment. After a soak time of approximately 30 minutes to 3 to 4
hours (depending on the nature of the spill repeat as necessary), the residual mixture may be
recovered using conventional methods. Actual cleaning time will likely depend on the
environmental conditions, chemistry of the spilled oil, and the cleaning method employed.

2.	Concentration/Application Rate: On heavy oils, use RHAMNOWASH 10 (neat) directly on
the spill, or use a 1:100 dilution ratio (product: water) depending on the nature of the oil (e.g.,
crude vs refined) and environmental conditions (e.g., warm vs cold water). Lighter oils may need
a 1:100 to 1:1000 dilution ratios depending on the oil's specific gravity and environmental
conditions. RHAMNOWASH 10 maintains its surfactant properties at high levels of dilution,
and works best when diluted with water (can use either saltwater or freshwater).

3.	Conditions for Use: RHAMNOWASH 10 can be applied on oiled surfaces and shorelines in
both freshwater and saltwater. Water temperatures less than 65°F may require higher dilution
rates. Sorbent booms, oil skimmers, or other containment equipment should be positioned prior
to and remain in place during product use to collect runoff from application and removal
operations. Collect and contain runoff from oil/product mixture and dispose of such material in
accordance with local, state, and federal regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested	Species	LC50 (ppm)

RHAMNOWASH 10	Menidia beryllina	76.64 96-hr

Mysidopsis bahia	164.61 48-hr

Surface Washing Agents

410

RHAMNOWASH 10


-------
No. 2 Fuel Oil

Menidia beryllina

10.85 96-hr



Mysidopsis bahia

2.27 48-hr

RHAMNOWASH 10 &

Menidia beryllina

13.70 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.15 48-hr

Reference Toxicant (SDS)

Menidia beryllina

7.52 96-hr



Mysidopsis bahia

5.47 48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >100°C

2.	Pour Point (ASTM D-97): 2.6°C

3.	Viscosity (ASTM D-445): 2.02 est @ 40°C

4.	Specific Gravity (ASTM D1298): 1.009 at 60°F

5.	pH (ASTM D-1293): 6.5

6.	Surface Active Agents: Anionic and nonionic, proprietary surfactants

7.	Solvents: None

8.	Additives: None

9.	Solubility: Miscible

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.250

Cadmium	<0.099

Chromium	<0.250

Copper	<0.740

Lead	<0.200

Mercury	<0.0033

Nickel	<0.200

Zinc	<5.000

Cyanide	<2.500

Chlorinated Hydrocarbons	<5.000

Surface Washing Agents

411

RHAMNOWASH 10


-------
TECHNICAL PRODUCT BULLETIN #SW-68

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: AUGUST 22, 2016

"ADP-7"

I.	NAME, BRAND, OR TRADEMARK
ADP-7

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Petro-Green, Inc.	Mailing Address

3952 Candlenut Lane	Petro-Green, Inc.

Dallas, TX 75244	P.O. Box 814665

Phone: updated information required	Dallas, TX 75381

E-mail: adp7@petro-green. com	(Mr. Michael Paddock)

E-mail: michael.paddock@petro-green.com
Website: www.petro-green.com
(Mr. Michael Paddock)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Petro-Green, Inc.	Mailing Address

3952 Candlenut Lane	Petro-Green, Inc.

Dallas, TX 75244	P.O. Box 814665

Phone: updated information required	Dallas, TX 75381

E-mail: adp7@petro-green. com	(Mr. Michael Paddock)

E-mail: michael,paddock@petro-green.com
Website: www.petro-green.com
(Mr. Michael Paddock)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable (DOT: Non-Hazardous)

2.	Ventilation: In most instances there will be no special requirements. However, if exposure
limits are exceeded or irritation is experienced, NIOSH/MSHA approved respiratory protection
should be worn. Positive pressure supplied air respirators may be required for high airborne
contaminant concentrations.

3.	Skin and eye contact; protective clothing; treatment in case of contact: First Aid: Skin/Body
Contact - Wash off immediately with soap and water while removing all contaminated clothing
and shoes. Wash all before reuse. Consult physician if irritation persists. Eyes - Immediately
flush with plenty of water. After initial flushing, remove contact lenses if present and continue
flushing for at least 15 minutes. If symptoms persist contact physician. Ingestion - Rinse mouth.
Drink plenty of water. Do NOT induce vomiting. If symptoms persist contact physician.

Surface Washing Agents

412

ADP-7


-------
Inhalation - Move to fresh air. If breathing is irregular or stopped administer artificial
respiration. Call physician.

4.a. Maximum storage temperature: 120°F continuous, 140°F up to 5 days

4.b. Minimum storage temperature: 26°F

4.c. Optimum storage temperature range: 40°F to 110°F

4.d. Temperatures of phase separations and chemical changes: Stable within storage temperature
range.

V.	SHELF LIFE

Unlimited in sealed poly drums (as delivered).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: For spills on soils, sandy or rocky areas: ADP-7 can be pre-mixed into
water, or educed into a water flow, to be sprayed directly onto the oil spill.

2.	Concentration/Application Rate: For spills on land: Typical dilution is one gallon of ADP-7
diluted with 42 gallons of water (approximately 2.4% concentration). Higher water temperatures
(over 78°F) and/or good agitation during application will allow you to reduce the concentration
strength. Aged or asphaltic spills may be more resistant to removal. Heating the solution to
150°F in a hot water washing rig, or a common oil field "hot oiler" truck will increase
effectiveness.

3.	Conditions for Use: ADP-7 is effective in salt water or fresh water, with no limitations as to
usage within optimum temperature parameters (application may be made at or above 35°F, with
optimum above 48°F). A sorbent boom or other containment equipment should be positioned
prior to product application and should remain in place during product use to collect runoff from
application and removal operations. The oil/product residue should be collected and removed
from the site. Collection process should be determined by onsite coordinator based on practices
of the area. Residue should be disposed of according to local, state and federal regulations.

VII.	TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

Species

LC50 (ppm)

ADP-7

Menidia beryllina

20.28 96-hr



Mysidopsis bahia

22.36 48-hr

No. 2 Fuel Oil

Menidia beryllina

17.46 96-hr



Mysidopsis bahia

5.30 48-hr

ADP-7 &

Menidia beryllina

14.10 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

3.24 48-hr

Reference Toxicant (SDS)

Menidia beryllina

3.42 96-hr



Mysidopsis bahia

7.81 48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS

Surface Washing Agents

413

ADP-7


-------
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >212°F

2.	Pour Point (ASTM D-97): 21°F

3.	Viscosity (ASTM D-445): 81.4 est @ 40°C

4.	Specific Gravity (ASTM D-287): 1.0985 at 60°F

5.	pH (ASTM D-1293): 9.9

6.	Surface Active Agents: Anionic and nonionic

7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility: Miscible in oil, water, and solvents

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.485

Cadmium	<0.243

Chromium	<0.243

Copper	<0.485

Lead	<0.585

Mercury	<3.26 |ig/L

Nickel	<0.485

Zinc	<0.485

Cyanide	<0.115

Chlorinated Hydrocarbons	<2.00

Surface Washing Agents

414

ADP-7


-------
TECHNICAL PRODUCT BULLETIN #SW-69

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

ORIGINAL LISTING DATE: SEPTEMBER 7, 2016

"WATER WORKS™ HEAVY DUTY DEGREASER CONCENTRATE"

(aka, HEAVY DUTY DEGREASER CONCENTRATE)

I.	NAME, BRAND, OR TRADEMARK

WATER WORKS™ HEAVY DUTY DEGREASER CONCENTRATE
(aka, HEAVY DUTY DEGREASER CONCENTRATE)

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
KetecaUSA, Inc.

4280 W. Opportunity Way
Phoenix, AZ 85086
Phone: (602) 278-7789
Fax: (602)535-1305
E-mail: sales@ketecausa.com
E-mail: kparks@ketecausa.com
Web site: www.ketecawaterworks.com
(Ms. Kathy Parks)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
KetecaUSA, Inc.

4280 W. Opportunity Way
Phoenix, AZ 85086
Phone: (602) 278-7789
Fax: (602)535-1305
E-mail: sales@ketecausa.com
E-mail: kparks@ketecausa.com
Web site: www.ketecawaterworks.com
(Ms. Kathy Parks)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-Flammable (DOT: Non-Hazardous)

2.	Ventilation: No special requirements.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Avoid contact with
eyes, slight irritation may result. Wear splash goggles or full face-shield and have eye washing
equipment available in areas where potential is high for eye contact. Skin contact will not cause
irritation in the majority of users. If eye or skin irritation occurs, flush with plenty of fresh water.
No special precautions or additional protective equipment are required during handling or use.

Surface Washing Agents

415	WATER WORKS™ HEAVY DUTY

DEGREASER CONCENTRATE


-------
Water Works™ Heavy Duty Degreaser Concentrate is provided with a Safety Data Sheet.
4.a. Maximum storage temperature: 100°F continuous, 110°F up to 5 days, keep away from
direct sun light.

4.b. Minimum storage temperature: 35°F

4.c. Optimum storage temperature range: >32°F to <100°F

4.d. Temperatures of phase separations and chemical changes: Stable and phase separation will
not occur at temperatures within the storage temperature range.

V.	SHELF LIFE

12 months from date of manufacturer in unopened original packaging (as delivered). Containers
should always remain closed when not in use to prevent contamination and evaporation.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product may be applied to rocks, shoreline, and beaches for removal of
oil. Select proper dilution depending on product types and contaminated material surface prior to
application. For treatment of large areas, properly diluted product may be applied by spraying
with a pressure washer, portable fire pump or any other suitable pump with seawater or
freshwater suction that is equipped with a chemical inductor or feed pump. For smaller areas,
properly diluted product may be applied with scrubber, mop, cloth or damp sponge. Apply
liberally, adjusting dilution on site as necessary.

2.	Concentration/Application Rate: For heavily weathered oil on rocks, applying concentrated or
diluted solution at 5 parts water to 1 part product is recommended. For heavily weathered oil on
beaches/sand, a diluted solution of 2 parts water to 1 part product is ideal. For tar balls, no
dilution is necessary and applying product at full strength is recommended. For removing oil
from vegetation, a diluted solution of 10-20 parts water to 1 part product is preferred. Product
may be diluted with either saltwater or freshwater. Warmer waters (greater than 78°F) and/or
good agitation during application will require less product.

3.	Conditions for Use: Can be used in freshwater, estuarine, and marine environments at all
temperatures. Prior to application, booms, oil skimmers, or other appropriate containment and
collection mechanism should be deployed and operational. Collected product and oil mixture
should be disposed of according to local, state, and federal regulations.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

WATER WORKS™ HEAVY DUTY
DEGREASER CONCENTRATE

No. 2 Fuel Oil

WATER WORKS™ HEAVY DUTY
DEGREASER CONCENTRATE &

Species

Menidia beryllina

Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina

LC50 (ppm)
68.70 96-hr

91.70 48-hr
11.53 96-hr
2.10 48-hr
14.60 96-hr

Surface Washing Agents

416	WATER WORKS™ HEAVY DUTY

DEGREASER CONCENTRATE


-------
2.27 48-hr
7.68 96-hr
5.27 48-hr

b. Effectiveness: NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

No. 2 Fuel Oil (1:10)	Mysidopsis bahia

Reference Toxicant (SDS)	Menidia beryllina

Mysidopsis bahia

IX. PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >212°F

2.	Pour Point (ASTM D-97): 26°F

3.	Viscosity (ASTM D-445): 2.66 est @ 40°C

4.	Specific Gravity (ASTM D-1298): 1.0728 at 60°F

5.	pH (ASTM D-1293): 9.4

6.	Surface Active Agents: Proprietary surfactants

7.	Solvents: None

8.	Additives: None

9.	Solubility: Soluble in water

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.001

Cadmium	<0.001

Chromium	<0.005

Copper	<0.01

Lead	0.0163

Mercury	<0.0002

Nickel	0.0167

Zinc	0.025

Cyanide	0.21

Chlorinated Hydrocarbons	6.22

Surface Washing Agents

417	WATER WORKS™ HEAVY DUTY

DEGREASER CONCENTRATE


-------
TECHNICAL PRODUCT BULLETIN #SW-70

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: MARCH 05, 2019

"X4JH2000"

I.	NAME, BRAND, OR TRADEMARK
X4JH2000

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
X4 Environmental Inc.

14702 Jersey Shore Drive

Houston, TX 77047

Phone: (281) 846-6003

E-mail: benlux.tam@x4environmental.com

(TszFung Benlux Tam)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
X4 Environmental Inc.

14702 Jersey Shore Drive

Houston, TX 77047

Phone: (281) 846-6003

E-mail: benlux.tam@x4environmental.com

(TszFung Benlux Tam)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable

2.	Ventilation: Recommend using a respirator in confined areas.

3.	Skin and eye contact; protective covering; treatment in case of contact: Wear rubber gloves
and eye protection. In case of eye contact, wash eyes thoroughly for 15 minutes including upper
and lower lids; and seek medical attention. In case of skin contact, irritation is possible; wash
with soap and water for 15 minutes. If irritation persists, seek medical attention.

4.a.	Maximum storage temperature: 95°F
4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 75°F

4.d. Temperatures of phase separations and chemical changes: No phase changes have been
observed.

V.	SHELF LIFE

One year in a sealed container; and six months for an opened container.

VI.	RECOMMENDED APPLICATION PROCEDURE

1. Application Method: X4JH2000 is applied by spraying apparatus or mixing on or into media

Surface Washing Agents

418

X4JH2000


-------
using excavator and 2-inch discharge hose, fire nozzle, or water pump; and water trucks.

2.	Concentration/Application Rate: X4JH2000 is a water-based chemical. Use a ratio of 1 to 1.5
U.S. gallons of X4JH2000 to 10 parts water (i.e., tap, salt or fresh water) per cubic yard of
contaminated media.

3.	Conditions for Use: Ambient temperature should be above 50°F. Water salinity and age of
hydrocarbon pollutants are not a condition of use. Prior to application, use oil spill absorbent,
boom and/or pad to prevent X4JH2000 from run off into ditches, creeks, and waterways.
Place collected booms, pads, and absorbents in black 55-gallon poly-bags, use duct tape to
seal, and then place bags in hazardous waste container for disposal. Collected containment
materials should be disposed of according to local, state, and federal regulations.

VII. TOXICITY AND EFFECTIVENESS

a. Toxicity

Material Tested

Species

LC50 (DDm)

X4JH2000

Menidia beryllina

145.89 96-hr



Mysidopsis bahia

40.26 48-hr

No. 2 Fuel Oil

Menidia beryllina

18.82 96-hr



Mysidopsis bahia

1.49 48-hr

X4JH2000 &

Menidia beryllina

18.59 96-hr

No. 2 Fuel Oil (1:10)

Mysidopsis bahia

2.07 48-hr

Reference Toxicant (SLS)

Menidia beryllina

4.64 96-hr



Mysidopsis bahia

8.42 48-hr

b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >220°F

2.	Pour Point (ASTM D-57): +28°F

3.	Viscosity (ASTM D-445): 4.99cSt at 40°C

4.	Specific Gravity (ASTM D-1298): 1.06 at 60°F

5.	pH (ASTM D-1293): 4.69

6.	Surface Active Agents: HS Code 340211 anionic organic surface-active agents

7.	Solvents: Not applicable

8.	Additives: Not applicable

9.	Solubility in Water: Not applicable

Surface Washing Agents

419

X4JH2000


-------
X. ANALYSIS FOR HEAVY METALS,
HYDROCARBONS

CYANIDE,

AND CHLORINATED

Compound

Concentration (ppm)

Arsenic

<0.050

Cadmium

<0.025

Chromium

<0.050

Copper

<0.100

Lead

<0.050

Mercury

<0.010

Nickel

<0.050

Zinc

0.461

Cyanide

<0.025

Chlorinated Hydrocarbons

<1.000

Surface Washing Agents

420

X4JH2000


-------
TECHNICAL PRODUCT BULLETIN #SW-71

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: JUNE 30, 2020

"TASMANIA C-CLENZ"

I. NAME, BRAND, OR TRADEMARK

TASMANIA C-CLENZ

Type of Product: Surface Washing Agent

II. NAME, ADDRESS, AND TELEPHONE
Head Office Physical Address
Tasmania Limited
104 Forest Drive

La Lucia, 4051, Durban, South Africa
(Mr. John Webster, CEO)

vtBER OF MANUFACTURER/CONTACT
Headquarter's Office Postal Address
Tasmania Limited
P.O. 242

Umhlanga Rocks, 4320, Durban, South Africa
(Mr. John Webster, CEO)

Product Management

Office: (+27) 562-9490

Mobile: (+27) 82-775-6555

U.S. Number: (904) 352-7195

E-mail: iohn.webster@tasmanialimited.com

Website: www.tasmanialimited.com

(Mr. John Webster, CEO)

U.S. Postal Address
Tasmania Limited
1958 East Peachtree Street
Nashville, AR 71852
Phone: (936) 777-4270
E-mail: moxxyoil@gmail.com
(Mr. Jeff Parker)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Skyfirm SA (Pty) Ltd	Sam Jariri

Nicol Grove Office Park	6314 Washington Blvd

William Nicol Drive	Arlington, VA 22205

Johannesburg, 2191, South Africa	Office: (202) 664-9250

Mobile: (+27) 76-280-0624	E-mail: sam.iariri@tasmanialimited.com

E-mail- martin@skyfirmsa.com	(Mr. Sam Jariri)

(Mr. Martin Schnuir)

Tasmania Limited
6 Lauderdale, 50 Chartwell Drive
Umhlanga Rocks, 4015, South Africa
Mobile: (+27) 71-419-1421
E-mail: russ@tasmanialimited.com
(Mr. Russell Parsons)

Surface Washing Agents

421

TASMANIA C-CLENZ


-------
IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: IMO - Non-flammable; DOT - Non-hazardous.

2.	Ventilation: Handle in well ventilated space, local exhaust is recommended if threshold limit
values are exceeded. If used in a confined area, wear a respirator. If used outdoors, no special
equipment is needed.

3.	Skin and eye contact; protective covering; treatment in case of contact: Use good normal
hygiene and avoid contact with skin and eyes. Wear rubber or vinyl gloves when applying the
product. Impermeable protective gloves are recommended for sensitive skin types. If contact is
made, wash with soap and water. Contact may cause redness, edema and drying of skin. Seek
medical attention if irritation develops. Wear protective eye goggles at all times. If in contact
with eyes, flush with water for 15 minutes and seek medical attention. Rinse contaminated
clothing, shoes, goggles and gloves in simple tap water to remove any chemical residue. In case
of ingestion, give water and call a doctor or medical professional. Remove to fresh air.

4.a.	Maximum storage temperature: 160°F
4.b. Minimum storage temperature: -25°F

4.c. Optimum storage temperature range: 60-90°F

4.d. Temperatures of phase separations and chemical changes: Temperature fluctuations will not
cause separation or deterioration of the product. There are no chemical changes to the product at
either the maximum or minimum temperature, the product is stable and will not undergo phase
separation of ingredients or stratification of contents over time.

V.	SHELF LIFE

The shelf life of an unopened TASMANIA C-CLENZ drum is 3 years. In case of opened drums,
shelf life is 2 years. Keep product away from direct sunlight.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: TASMANIA C-CLENZ is for land use only. There are no application
restrictions. The preferred application method is to apply the product over pollutant or
stained area with a hand sprayer, pressure sprayer or a heated pressure spray unit. For the
first application of TASMANIA C-CLENZ to shoreline contamination, use cold water/low
pressure washing (<50 PSI) to remove any liquid oil that has adhered to the substrate, pooled
on the surface or become trapped in vegetation. The average soak time of light oil
contamination is 15-30 minutes. The average soak time of heavy oil contamination is 30-45
minutes, which allows the viscous oil deposits to soften. The actual soak time may vary with
temperature, oil density and degree of weathering. The product starts to work on breaking the
physical bond between the oil and the surface to be cleaned. In the case of heavy oil on the
rocks or oil displaced into crevices, use warm water and moderate to high pressure washing
with a temperature of 90°F and 100 PSI. When accessible or applicable, a work boat with
mounted spray booms can be used to spray the product on the shoreline. Personnel can also
apply the product with a hand sprayer or pressure sprayer.

2.	Concentration/Application Rate: For heavily contaminated oil on rocks, use a full strength
solution (non-diluted). For heavily weathered oil on beaches and rocks, a dilution of 5 parts
water and 1 part product is ideal. For light contamination on the rocks, beaches and sand, a

Surface Washing Agents

422

TASMANIA C-CLENZ


-------
dilution of 10 parts water and one part product is used. Product can be diluted with either
fresh or salt water. For removing oil from vegetation, a diluted solution of 15 parts water and
one part product is preferred. Application rate is 1 gallon of product per square foot of
surface area.

3. Conditions for Use: Used for cleaning petroleum fractions from shoreline, beaches and rocks.
The water temperature can vary from 30-140°F. Best results are obtained by allowing either
the non-diluted of diluted product to soak for 15-45 minutes depending on the severity of the
pollutant on the area and whether the oil is weathered or is heavy oil. Adjust the pressure
angle of the sprayer for optimal results. TASMANIA C-CLENZ can be used for
contamination with all types of oil including heavily weathered and emulsified to light oil
fractions, only the dilution amount will be adjusted. In the case of high temperatures above
75°F, use full strength TASMANIA C-CLENZ as the temperature and humidity will cause
rapid evaporation of the spray. Greater results occur at ambient temperatures greater than
50°F. The salinity of the water has no effect on the performance of the product. Prior to
application, use booms to prevent the product and oil mixture from entering open water. The
product and oil mixture can be removed by either vacuum, skimmers or oil absorbents being
applied in the boomed off area. The product and oil mixture, along with containment
materials, should be disposed of according to local, state, and federal regulations.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity
Material Tested

TASMANIA C-CLENZ

No. 2 Fuel Oil

TASMANIA C-CLENZ &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
141.16 96-hr

34.27
6.17
2.11
5.24
1.93
3.47
8.75

48-hr
96-hr
48-hr
96-hr
48-hr
96-hr
48-hr

b. Effectiveness:
NA

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point (ASTM D-56): >100°C

2.	Pour Point (ASTM D-97): +26°C

3.	Viscosity (ASTM D-445): 2.299cSt at 60°F

4.	Specific Gravity (ASTM D-287): 0.9678 at 60°F

5.	pH: 7.0

6.	Surface Active Agents: Confidential

Surface Washing Agents

423

TASMANIA C-CLENZ


-------
7.	Solvents: Confidential

8.	Additives: Confidential

9.	Solubility in Water: 100%

X. ANALYSIS FOR HEAVY METALS,

HYDROCARBONS

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

CYANIDE, AND CHLORINATED

Concentration (ppm)

0.275

0.122

0.0406

0.272

0.154

0.0132

0.0154

0.195

0.00198

0.00050

Surface Washing Agents

424

TASMANIA C-CLENZ


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TECHNICAL PRODUCT BULLETIN #SW-72

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: MAY 17, 2021

"GOLD CREW® TC"

I. NAME, BRAND, OR TRADEMARK
GOLD CREW® TC

(aka, TRAFFIC COLLISION, SPILL CLEANUP AGENT)
Type of Product: Surface Washing Agent

II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Gold Crew Products & Services, LLC

P.O. Box 2039

Orange, CA 92869

Mobile: (714)318-5997

E-mail: ifigueira@goldcrew.net

E-mail: ifigueira@ecschem.com

(Mr. Jim Figueira)

ECS

5713 Wollochet Drive NW, Suite B
Gig Harbor, WA 98332
Phone: (253) 263-8040
E-mail: egrubbs@ecschem.com
Website: www.ecschem.com
(Mr. Ed Grubbs)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
ECS

5713 Wollochet Drive NW, Suite B
Gig Harbor, WA 98332
Phone: (253) 263-8040
E-mail: egrubbs@ecschem.com
Website: www.ecschem.com
(Mr. Ed Grubbs)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Normal.

3.	Skin and eye contact; protective clothing; treatment in case of contact: Good hygiene practices
should always be followed. Wear impervious gloves for solutions or where contact is repeated.
Avoid contact with eyes, skin, and clothing. Handle in accordance with good industrial hygiene
and safety practices. For eye contact, flush with water and get medical attention if required. For
skin contact, remove contaminated clothing and wash exposed area, and wash clothing before
next use. If irritation develops get medical attention. If ingested, get medical attention.

4.a.	Maximum storage temperature: When above 120°F, keep container closed and stored in a
cool dark place. Evaporation may change product's characteristics.

4.b. Minimum storage temperature: Product will freeze below 25°F. No phase separation will
occur. If frozen, thaw, and stir well.

4.c. Optimum storage temperature range: 25°F to 120°F. Use normal storage conditions, but
store away from incompatible materials.

Surface Washing Agents

425

GOLD CREW® TC


-------
4.d. Temperatures of phase separations and chemical changes: No separation at any temperature
between 32-120°F. No tendency to "layer out" or separate, standing for 30 days. No separation
of layering after freezing.

V.	SHELF LIFE

2 years (unopened); and 1 year (opened).

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Gold Crew® TC's mechanism of action desorbs or strips the hydrocarbon
off the surface of the solid through surface tension reduction enhanced with physical agitation.
The action is not a chemical reaction.

2.	Concentration/Application Rate: For small hard surface area, active wash: Apply undiluted
through hand pump sprayer. Apply to cover immediate work area. Use scrub brush to agitate.
Use appropriate sorbent material to pick up and contain. For releasing from hard surface using
presoak and/or power wash action: Boom off immediate work area. Use undiluted as presoak.
Apply to cover the focused work area. Work on a test area first to determine site specific
application. For crude oil, allow up to a 20-minute presoak. For medium distillates, allow 10 (±)
minutes. For light distillates, allow 5 minutes. Times may vary depending on weather
conditions/oil viscosity and site-specific conditions. After determining and applying the solution
for presoak, wash down the area in the following manner: Gold Crew® TC should be used
through a power washer or through a steam powered unit at 1 to 5 percent eduction rate to
decrease the water's surface tension and enhance power washing effectiveness. Wash to boomed
containment area and remove by absorbent or skimmer. Dispose of waste material according to
federal, state, and local regulations. For power wash with no presoak, used undiluted through
power washer for crude and heavy oils. For lighter distillate's dilute 50:50 with water. Follow
containment and recovery methods.

3.	Conditions for Use: Equally effective with salt or fresh water. Product will freeze in very low
temperature but when thawed, will not affect performance.

VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

GOLD CREW® TC

No. 2 Fuel Oil

GOLD CREW® TC &
No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

b. Effectiveness:

NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
630.00 96-hr
503.00 48-hr
8.77 96-hr
3.00 48-hr
5.65 96-hr
4.25 48-hr
1.90 96-hr
9.03 48-hr

Surface Washing Agents

426

GOLD CREW® TC


-------
VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >200

2.	Pour Point: 32°F

3.	Viscosity: 1.52 est @ 71°F (22°C); 1.213 est @ 104°F (40°C)

4.	Specific Gravity: 1.002

5.	pH: 8.78 (±0.01)

6.	Surface Active Agents: CONFIDENTIAL.

7.	Solvents: None.

8.	Additives: CONFIDENTIAL.

9.	Solubility in Water: Complete.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	0.0343

Cadmium	<0.0020

Chromium	<0.0050

Copper	0.0166

Lead	<0.0060

Mercury	<0.0008

Nickel	<0.0050

Zinc	<0.0200

Cyanide	<0.0050

Chlorinated Hydrocarbons	ND

Surface Washing Agents

427

GOLD CREW® TC


-------
TECHNICAL PRODUCT BULLETIN #SW-73

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: SEPTEMBER 29, 2021

"DE-OIL-IT INDUSTRIAL STRENGTH CONCENTRATE"

I.	NAME, BRAND, OR TRADEMARK

DE-OIL-IT INDUSTRIAL STRENGTH CONCENTRATE
Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Greenworld Innovations Corp.

3813 Highgate Drive
Valrico, FL 33594
Phone: (407) 574-3898
Fax: (813)413-6073
E-mail: info@gwi.world
Website: www.deoilit.com

(Mr. Ron McCarthy, CEO, or Mr. Danny Schillaci, COO)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Greenworld Innovations Corp.

3813 Highgate Drive
Valrico, FL 33594
Phone: (407) 574-3898
Fax: (813)413-6073
E-mail: info@gwi.world
Website: www.deoilit.com

(Mr. Ron McCarthy, CEO, or Mr. Danny Schillaci, COO)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: No mechanical ventilation required; fresh air supply recommended for inside
confined spaces.

3.	Skin and eye contact; protective clothing; treatment in case of contact: May cause eye
irritation, manufacturer recommends use of goggles during application. In case of eye contact,
flush with plenty of water. After initial flushing, remove any contact lenses and continue flushing
for at least 15 minutes. For skin contact, wash exposed skin with soap and water. If redness,
itching or a burning sensation develops get medical attention.

4.a.	Maximum storage temperature: 120°F continuous, 140°F up to 5 days.

4.b. Minimum storage temperature: 35°F.

4.c. Optimum storage temperature range: 40°F to 120°F.

4.d. Temperatures of phase separations and chemical changes: Stable; however, avoid freezing

Surface Washing Agents

428

DE-OIL-IT INDUSTRIAL
STRENGTH CONCENTRATE


-------
application solution (concentrated product diluted with water) to avoid possible separation.

V.	SHELF LIFE

The shelf life of unopened containers is unlimited. Containers should remain capped when not in
use to prevent contamination or evaporation. Activated concentrate (i.e., product diluted with
water) has unlimited shelf life if kept capped.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Product is to be used in diluted form and works just as well with fresh or
salt water. This product works well with all types of oils contaminating shorelines, beaches, and
rocks. Dilute to 30:1 (this is the application solution comprised of 30 parts water and one part
product), spray on surface areas, and allow to soak time for 15 minutes before rinsing with water.
For stubborn oil cleanup, after soaking scrub with brush before rinsing. Spraying means using
mechanical methods such as a pump that can deliver 30 psi or greater. Rinsing is best performed
with a pressure washer if available. Prior to application, use booms to prevent the product and oil
mixture from entering open water. Water run-off can be collected by a vacuum apparatus as
surface tension of the treated oil is reduced making pick up efforts easier (should not stick to
vacuuming). The product and oil mixture, along with containment materials, should be disposed
of according to local, state, and federal regulations.

2.	Concentration/Application Rate: The volume of an application solution for shoreline cleanup
means adding water (30 parts) to product (one part) and is dependent on size of cleanup area. In
general the calculation of application solution (water plus product) volume in gallons is (Length
x Width)*(0.08) - scale is in feet. As an example, a boundary of contaminated shoreline
measuring 50 feet x 12 feet, would be 600 square feet. Then 600 square feet * 0.08 = 48 gallons,
at 30:1 dilution ratio this would be 1.5 gallons of product and 46.5 gallons of water. Water does
not need to be filtered and can be salt or fresh.

3.	Conditions for Use: Outside air temperature of 50°F to 125°F is optimal; otherwise, there is no
specific restrictions outside this range other than avoid freezing of application solution. Water
temperature for activating the application solution produces optimal performance between 95°F
to 125°F; otherwise, there is no specific restrictions outside this range other than avoid freezing
application solution. Water source for application solution can be fresh, or a non-potable source
such as natural sources (i.e., lakes, ocean). Ambient water temperature at source of oil spill
should be above 35°F. Do no freeze product, possible separation could occur. Manufacturer
resting time of dilution application solution includes:

•	When creating a diluted application solution according to a selected dilution ratio, the
combined solution of water and product needs to rest.

•	Resting time of 30 minutes to one hour stabilizing at ambient temperature to which you
are to apply the application solution is optimal.

Surface Washing Agents

429

DE-OIL-IT INDUSTRIAL
STRENGTH CONCENTRATE


-------
VII. TOXICITY AND EFFECTIVENESS
a. Toxicity:

Material Tested

DE-OIL-IT INDUSTRIAL
STRENGTH CONCENTRATE
No. 2 Fuel Oil

PRODUCT &

No. 2 Fuel Oil (1:10)

Reference Toxicant (DSS)

b. Effectiveness:

NA

Species

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

LC50 (ppm)
144.59 96-hr
76.64 48-hr
10.55 96-hr
3.90 48-hr

4.65
4.13
3.98
8.36

96-hr
48-hr
96-hr
48-hr

VIII. MICROBIOLOGICAL ANALYSIS
NA

IX. PHYSICAL PROPERTIES

1.	Flash Point: >212°F

2.	Pour Point: 26°F

3.	Viscosity: 1.505 cSt @ 40°C

4.	Specific Gravity: 1.1959 @ 60°F

5.	pH: 12.9

6.	Surface Active Agents: Anionic and nonionic surfactants, proprietary

7.	Solvents: CONFIDENTIAL.

8.	Additives: CONFIDENTIAL.

9.	Solubility in Water: High solubility in water.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.050

Cadmium	<0.025

Chromium	<0.015

Copper	<0.050

Lead	<0.050

Mercury	<1.00 ug/L

Nickel	<0.050
Zinc 0.249
Cyanide 0.0774

Chlorinated Hydrocarbons	<0.005

Surface Washing Agents

430

DE-OIL-IT INDUSTRIAL
STRENGTH CONCENTRATE


-------
TECHNICAL PRODUCT BULLETIN #SW-74

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: NOVEMBER 17, 2021

"ECOGREEN"

I. NAME, BRAND, OR TRADEMARK
ECOGREEN

Type of Product: Surface Washing Agent

II. NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT

Rose Rock Products, LLC

P.O. Box 721926

Oklahoma City, OK 73172

Phone: (405) 883-1095

E-mail: Ken.Murphy@RoseRockEnv.com

Website: www.RoseRockEnv.com

(Mr. Ken Murphy, CEO)

III. NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS

Rose Rock Products, LLC	EcoTec, LLC

P.O. Box 721926	3 Nancy Court, Suite 4

Oklahoma City, OK 73172	Wappingers Falls, NY 12590

Phone: (405) 883-1095	Phone: (845) 897-0003

E-mail: Ken.Murphy@RoseRockEnv.com	E-mail: WJordan@EcoTecLLC.com

Website: www.RoseRockEnv.com	Website: www.EcoTecLLC.com

(Mr. Ken Murphy, CEO)	(Mr. Wyatt Jordan)

IV. SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Always keep exposure below permissible exposure limits. In general, dilution
ventilation is a satisfactory health hazard control for this substance. However, if conditions of
use create discomfort to the worker, a local exhaust system should be considered.

3.	Skin and eye contact; protective clothing; treatment in case of contact: As prescribed in the
OSHA Standard for Personal Protective Equipment (29 CFR 1910.132), employers must perform
a Hazard Assessment for all workplaces to determine the need for, and selection of, proper
protective equipment for each task performed. For skin and eye contact, use good normal
hygiene and avoid contact with skin and eyes. For prolonged or repeated handling, use
impervious gloves. Gloves should be tested to determine suitability for prolonged contact. Use of
impervious apron and boots are recommended. Wear face shield, safety glasses, or chemical
goggles are recommended for field application and product handling. If contact with eyes, flush
with water for 15 minutes and see medical attention if irritation develops. For contact with skin,
wash area with soap and water. May cause redness and drying of skin. Seek medical attention if

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irritation develops. In case of ingestion, seek medical attention. Not considered an inhalation
risk.

4.a. Maximum storage temperature: 120°F.

4.b. Minimum storage temperature: Freeze temperature is 32°F. No deterioration in performance
is expected as a result of freezing. Thaw product and mix thoroughly prior to use.

4.c. Optimum storage temperature range: 35°F to 120°F.

4.d. Temperatures of phase separations and chemical changes: Temperature fluctuations will not
cause separation or deterioration of product. Product blend is stable and will not undergo phase
separation of ingredients or stratification of contents over time.

V.	SHELF LIFE

Unlimited shelf life (unopened), product should be used within 12 months of opening.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: Dilute product with water prior to use. Apply diluted product via manual
pressure applicator (i.e., hand pump), or other delivery equipment, to impacted surfaces. Allow
product to soak prior to rinse/recovery if heavily saturated with oil. On hard surfaces, product
may be applied and agitated with a brush or other physical means prior to recovery of effluent.
Product may also by pre-mixed and used in a batch tank or through an eduction/metering system
for flushing and recovery operations. Any common pressure washer, either hot or cold, will be
effective for proper application at recommended dilutions of ECOGREEN. Proper containment
contingencies should be deployed prior to application of ECOGREEN solution to stranded oils
on impacted substrates to ensure adequate recovery of treated oils.

2.	Concentration/Application Rate: ECOGREEN is a concentrated product and must be diluted
prior to use. Concentrations vary based upon type of oil and degree of surface saturation. For
Light Ends (i.e., gas condensate/gasoline) a 1% to 2% solution may be used to flush area to
containment. Note: A higher concentration solution of 5% to 6% should be used if flammable
vapor presents an explosion hazard. For Lighter Oils (i.e., Diesel Fuel, #2 Fuel Oil) a 3%
solution may be used to flush impacted areas to containment. For Heavy Ends (i.e., Crude Oil,
#6 Fuel Oil) a 6% solution of ECOGREEN should be applied and allowed to soak into
containment/substrate for up to an hour to allow for release of oil. The surface should then be
flushed to containment with a 1% to 3% solution of ECOGREEN. Product may be used as noted
above through any pressure or steam equipment. The use of a "hot" unit is recommended when
oils are at low temperature or have been weathered.

3.	Conditions for Use: ECOGREEN may be diluted with hard, soft, brackish, salt, or most waters
of sufficient quality for operations. Upon proper application as noted above, all treated fluids
should be flushed and/or directed to proper containment and recovery. Affected shorelines and
other surfaces should be isolated with containment booms and/or sorbent materials prior to
treatment to avoid release of treated fluids to open waters. Diversion of swales and temporary
catchment sumps may be used for vacuum recovery of treated effluents. All recovered fluids
should be disposed of in accordance with all federal, state, and local regulations.

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VII. TOXICITY AND EFFECTIVENESS

a.	Toxicity:

Material Tested
ECOGREEN (neat)

No. 2 Fuel Oil

ECOGREEN & No. 2 Fuel Oil (1:10)
Reference Toxicant (SDS)

b.	Effectiveness:

NA

Species

LC50 (ppm)

Menidia beryllina

111.00

96-hr

Mysidopsis bahia

104.00

48-hr

Menidia beryllina

11.30

96-hr

Mysidopsis bahia

1.74

48-hr

Menidia beryllina

5.73

96-hr

Mysidopsis bahia

1.84

48-hr

Menidia beryllina

1.76

96-hr

Mysidopsis bahia

4.24

48-hr

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: >230°F

2.	Pour Point: 32.0°F

3.	Viscosity: 4.403 cSt @ 104°F

4.	Specific Gravity: 1.015 @ 60°F

5.	pH: 8.3

6.	Surface Active Agents: CONFIDENTIAL.

7.	Solvents: CONFIDENTIAL.

8.	Additives: CONFIDENTIAL.

9.	Solubility in Water: Complete.

X. ANALYSIS FOR HEAVY METALS, CYANIDE, AND CHLORINATED
HYDROCARBONS

Compound	Concentration (ppm)

Arsenic	<0.500

Cadmium	<0.100

Chromium	<0.250

Copper	<0.500

Lead	<0.300

Mercury	<0.151

Nickel	<0.250

Zinc	<1.250

Cyanide	<1.000

Chlorinated Hydrocarbons	All < Method Quantification Limit

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NEW PRODUCT LISTING

TECHNICAL PRODUCT BULLETIN #SW-75

USEPA, OEM REGULATIONS IMPLEMENTATION DIVISION

LISTING DATE: FEBRUARY 16, 2023

"ABLUOL OSASA H/C"

I.	NAME, BRAND, OR TRADEMARK
ABLUOL OSASA H/C

Type of Product: Surface Washing Agent

II.	NAME, ADDRESS, AND TELEPHONE NUMBER OF MANUFACTURER/CONTACT
Taiwan Surfactant Corporation

8F1., No. 11, Sec. 1

Chung Shan North Road

Taipei, 104, Taiwan

Phone: 886-2-25410022

E-mail: twsa@twsa.com.tw

Website: https://www.taiwan-surfactant.com/

(Mr. Lun Hsieh)

III.	NAME, ADDRESS, AND TELEPHONE NUMBER OF PRIMARY DISTRIBUTORS
Taiwan Surfactant Corporation

8F1., No. 11, Sec. 1

Chung Shan North Road

Taipei, 104, Taiwan

Phone: 886-2-25410022

E-mail: twsa@twsa.com.tw

Website: https://www.taiwan-surfactant.com/

(Mr. Lun Hsieh)

IV.	SPECIAL HANDLING AND WORKER PRECAUTIONS FOR STORAGE AND FIELD
APPLICATION

1.	Flammability: Non-flammable.

2.	Ventilation: Normal ventilation, use of a respirator in confined areas is recommended.

3.	Skin and eye contact; protective clothing; treatment in case of contact: As in handling any
industrial chemical, the standard precautions of wearing chemical-resistant gloves and eye
protection are recommended. Additional precautions include using non-sparking tools and
avoiding exposure to aerosol vapor.

4.a.	Maximum storage temperature: 212°F.

4.b. Minimum storage temperature: 32°F

4.c. Optimum storage temperature range: 68°F.

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4.d. Temperatures of phase separations and chemical changes: May begin freezing below 25°F as
product begins to get turbid. Stir until product becomes homogenous. No chemical changes.

V.	SHELF LIFE

Two years (unopened). After confirming there is no contamination in opened barrels, opened
barrels will have a shelf life of two years.

VI.	RECOMMENDED APPLICATION PROCEDURE

1.	Application Method: ABLUOL OSASA H/C is water-based formulation. The product is used
to remove oil from hard surfaces such as shorelines, rock, and sand. Prior to application of
ABLUOL OSASA H/C, collection booms, oil skimmers, sorbent pads, or other appropriate
containment and collection mechanism must be deployed and operational. Apply diluted product
via manual pressure washer, spraying tools, or hand pumps.

2.	Concentration/Application Rate: ABLUOL OSASA H/C is a highly concentrated product and
must be diluted with water (salt or fresh) before use. Dilution ratios vary depending on the
specific conditions of the contaminated site. The dilution ratio is approximately 1:80 to 1:100
(product: water). The application ratio of this diluted product to oil is approximately 1:10. For
shorelines and rock, ABLUOL OSASA H/C is to be used in approximately a 1:80 to 1:100
dilution ratio (product:water). ABLUOL OSASA H/C is sprayed directly on the oiled rocky
shorelines or rock. A dilution of ABLUOL OSASA H/C with warm waters (up to 176°F or
80°C) during application will enhance its washing effect on shorelines and rocks. After applying
the diluted ABLUOL OSASA H/C by hand or spraying tools, soaking for approximately 10
minutes, the washing work can be started. Application of pressure washer will accelerate the
washing process. For use on sand, ABLUOL OSASA H/C is to be used in approximately a 1:80
to 1:100 dilution ratio (product:water) under stirring. Oil will separate from sand and float on the
surface of spray water for timely collection or adsorption.

3.	Conditions for Use: Do not mix the product with any other cleaner or allow other cleaners to
contact surfaces while using ABLUOL OSASA H/C. ABLUOL OSASA H/C does not contain
petroleum distillates. The product works well with all types of oils and with salt or fresh water.
Use booms or other containments prior application of ABLUOL OSASA H/C to prevent the
product/oil mixture from reaching open water. Collect, remove, and dispose of product/oil
mixture from site according to federal, state, and local regulations.

VII.	TOXICITY AND EFFECTIVENESS

a. Toxicity:

Material Tested
ABLUOL OSASA H/C

Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia
Menidia beryllina
Mysidopsis bahia

Species

LC50 (ppm)
19.80 96-hr
28.10 48-hr
6.22 96-hr
1.41 48-hr
3.33 96-hr
1.32 48-hr
1.69 96-hr
4.64 48-hr

No. 2 Fuel Oil

ABLUOL OSASA H/C No. 2 Fuel Oil (1:10)

Reference Toxicant (SDS)

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b. Effectiveness:

NA

VIII.	MICROBIOLOGICAL ANALYSIS
NA

IX.	PHYSICAL PROPERTIES

1.	Flash Point: No flash

2.	Pour Point: -21°C

3.	Viscosity: 161 cSt @ 40°C

4.	Specific Gravity: 1.102 @ 60°F

5.	pH: 4.93

6.	Surface Active Agents: CONFIDENTIAL

7.	Solvents: Water

8.	Additives: CONFIDENTIAL

9.	Solubility in Water: Soluble in fresh and salt water.

AND CHLORINATED

Concentration (ppm)
<0.50
<0.10
<0.25
<0.50
<0.30
<0.0136
<0.25
<1.25
<1.00

Non Detect

X. ANALYSIS FOR HEAVY METALS, CYANIDE,

HYDROCARBONS

Compound

Arsenic

Cadmium

Chromium

Copper

Lead

Mercury

Nickel

Zinc

Cyanide

Chlorinated Hydrocarbons

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