TET1A TECH
July 28, 2016
Mr. Tom Mahler
On-Scene Coordinator
U.S. Environmental Protection Agency, Region 7
J1201 Renner Boulevard
Lenexa, Kansas 66219
Subject: Data Deliverable Package for June 2016 Sediment Sampling
West Lake Landfill Site, Bridgeton, Missouri
CIRCUS ID: M( >1)079900932
EPA Region 7, START 4, Contract No. EP-S7-13-06, Task Order No. 0134
Task Monitor: Tom Mahler, On-Scenc Coordinator
Dear Mr. Mahler:
Tetra Tech, Inc. is submitting electrically, on the enclosed CD, the Level 4 analytical laboratory report
and corresponding data validation report for the following sediment samples obtained from the West Lake
Landfill Site in Bridgeton. Missouri.
Sample Delivery Group Sample Name Date of Collection
J17814 AC-SED-4 06/10/2016
J17814 AC-SED-6 06/10/2016
J17814 AC-SED-7 06/10/2016
j 17814 AC-SED-8 06/10/2016
If you have any questions or comments, please contact Colin Willits at (816) 412-1785.
Sincerely,
J/ ^
Colin Willits
STA^T Project Manager
i ' I 1 ¦
- •' ^ v'
J^Ted Faile, PG, CH^M
START Program Manager
Enclosure
cc; Debra Dorsey, START Project Officer (cover letter only)
X9025.16.0134.000
415 Oa
Tel 816.412.1741 Fax 81
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Tetra Tech, Inc.
DATA VALIDATION REPORT
LEVEL IV
Site:
West Lake Landfill Site, Bridgeton, Missouri
Laboratory:
TestAmerica Laboratories, Inc. (Earth City, Missouri)
Data Reviewer:
Harry Ellis, Tetra Tech, Inc. (Tetra Tech)
Review Date
July 26, 2016
Sample Delivery Group (SDG): J17814
Sample Numbers:
AC-SED-4, AC-SED-6, AC-SED-7, and AC-SED-8
Matrix / Number of Samples: Four Sediment Samples
The data were qualified according to the U.S. Environmental Protection Agency (EPA) Region 7
documents entitled "Contract Laboratory Program National Functional Guidelines for Inorganic
Superfund Methods Data Review" (9355.0-131), August 2014. In addition, the Tetra Tech document
"Review of Data Packages from Subcontracted Laboratories" (February 2002) and the EPA and others
document "Multi-Agency Radiological Laboratory Analytical Protocols Manual" (July 2004) were used
along with other criteria specified in the applicable methods.
The review was intended to identify problems and quality control (QC) deficiencies that were readily
apparent from the summary data package. The following sections discuss any problems or deficiencies
that were found, and data qualifications applied because of non-compliant QC. The data review was
limited to the available field and laboratory QC information submitted with the project-specific data
package.
I, Harry Ellis, certify that all data validation criteria outlined in the above-referenced documents were
assessed, and any qualifications made to the data accorded with those documents.
26 July 2016
Certified by Harry Ellis, Chemist
Date
10319025160134
1
SDG J17814
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DATA VALIDATION QUALIFIERS
U — The analyte was not detected above the reported sample quantitation limit.
J — The analyte was positively identified; the associated numerical value is the approximate
concentration of the analyte in the sample.
UJ — The analyte was not detected above the reported sample quantitation limit, which is
estimated.
R — The sample results are rejected due to serious deficiencies in the ability to analyze the
sample and meet QC criteria. Presence or absence of the analyte cannot be verified.
10319025160134
2
SDG J17814
-------
DATA ASSESSMENT
Sample delivery group (SDG) J17814 included four (4) environmental sediment samples and no QC
samples. The samples were analyzed for thorium and uranium isotopes by alpha spectroscopy, using
DOE Method A-01 -R, and for radium-226 and other isotopes by gamma spectroscopy, using EPA
Method GA-01-R. The following summarizes the data validation that was performed.
ALPHA SPECTROSCOPY ANALYSES
I. Holding Time and Chain of Custody (COC) Requirements
The samples were received by the laboratory and analyzed within the established holding time of 6
months from sample collection to analysis. No data were qualified.
II. Matrix Spike/Matrix Spike Duplicate (MS/MSD)
MS/MSD analyses were not performed in these analyses. No qualifications were applied for this data
gap. LCS and duplicate analyses provided adequate confirmation of accuracy and precision.
III. Blanks
The laboratory (method) blanks yielded low activities for thorium-228, thorium 230, and uranium-238.
The field sample results for thorium-228 were less than 10 times the blank result, so they were qualified
as estimated, possibly biased high, and flagged "J". The activities of the other isotopes were more than
10 times the blank activities, so no further qualifications were applied.
IV. Laboratory Control Sample (LCS)
All percent recoveries and relative percent differences from the LCS analyses were within established
control limits. No qualifications were applied.
V. Tracers
The tracers (thorium-229 and uranium-232) yielded fully satisfactory recoveries from most samples.
However the thorium tracer in sample AC-SED-7 yielded a 136 percent recovery, well above the
laboratory limits of 30 to 110 percent. The thorium isotope results for sample AC-SED-7 were qualified
as estimated and flagged "J".
VI. Calibrations and other Quality Control measures
All calibrations (including initial, annual verification, monthly, and daily) were within their QC limits.
Monthly background checks were also within limits.
VI. Comments
None.
10319025160134
3
SDG J17814
-------
VII. Overall Assessment of Data
Overall data quality is acceptable, with no significant qualifications applied. All data are usable as
qualified for their intended purposes.
GAMMA SPECTROSCOPY ANALYSES
I. Holding Time and Chain of Custody (COC) Requirements
The samples were received by the laboratory and analyzed within the established holding time of 6
months from sample collection to analysis. The preferred 21-day ingrowth period was performed before
determination of the radium and other isotopes. No data were qualified.
II. Matrix Spike/Matrix Spike Duplicate (MS/MSD)
MS/MSD analyses were not performed in these analyses. No qualifications were applied for this data
gap. LCS and duplicate analyses provided adequate confirmation of accuracy and precision.
III. Blanks
The laboratory (method) blank yielded a low activity for thallium-208. The field sample results for that
isotope were less than 10 times the blank result, so they were qualified as estimated, possibly biased high,
and flagged "J".
IV. Laboratory Control Sample (LCS)
All percent recoveries from the LCS analyses were within established control limits. No qualifications
were applied.
V. Tracers
Tracers are not used in these radioanalytical methods.
VI. Calibrations and other Quality Control measures
All calibrations (including initial, annual verification, and daily) were within their QC limits. Monthly
background checks were also within limits.
VI. Comments
None.
VII. Overall Assessment of Data
Overall data quality is acceptable, with no qualifications applied. All data are usable as reported for their
intended purposes.
10319025160134
4
SDG J17814
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Tetf./ rnericci
THE LEADER IN ENVIRONMENTAL TESTING
ANALYTICAL REPORT
Job Number: 160-17814-1
Job Description: West Lake Landfill
For:
Tetra Tech EM Inc.
415 Oak Street
Kansas City, MO 64106
Attention: Ms. Emily Fisher
Erika K Gish, Project Manager II
13715 Rider Trail North, Earth City, MO, 63045
(314)298-8566
erika.gish@testamericainc.com
07/13/2016
Approved for release.
Erika K Gish
Project Manager II
7/13/2016 3:55 PM
The test results in this report meet NELAP requirements for parameters for which accreditation is required or available.
Any exceptions to the NELAP requirements are noted. Results pertain only to samples listed in this report. Pursuant to
NELAP, this report shall not be reproduced, except in full, without the written approval of the laboratory. This report is
confidential and is intended for the sole use of TestAmerica and its client. All questions regarding this report should be
directed to the TestAmerica Project Manager.
Louisiana Lab Certification ID (Non-Potable, Solid/Haz. Material): 106151
Florida Lab Certification ID (Drinking Water): E87689.
TestAmerica Laboratories, Inc.
TestAmerica St. Louis 13715 Rider Trail North, Earth City, MO 63045
Tel (314) 298-8566 Fax (314) 298-8757 www.testamericainc.com
Page 1 of 551
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Table of Contents
Cover Title Page 1
Data Summaries 4
Definitions 4
Case Narrative 5
Client Sample Results 7
Tracer/Carrier Summary 11
QC Sample Results 12
QC Association 15
Chronicle 16
Certification Summary 18
Method Summary 19
Sample Summary 20
Reagent Traceability 21
COAs 25
Radiochemistry Raw Data 136
Alpha Spectroscopy 136
Method A-01-R Th 1 37
Method A-01-R U 152
Daily Checks 1 65
Initial Calibrations 181
Initial Calibration Verifications 196
Monthly Calibration Verifications 213
Monthly Backgrounds 228
Run Logs 257
Gamma Spectroscopy 261
Method GA-01-R Ra-226 262
Page 2 of 551
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Table of Contents
Daily Checks 424
Initial Calibrations 433
Initial Calibration Verifications 462
Annual Calibration Verifications 490
Monthly Backgrounds 514
Run Logs 545
Pre-Preparation Data 548
Shipping and Receiving Documents 549
Client Chain of Custody 550
Sample Receipt Checklist 551
Page 3 of 551
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Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Definitions/Glossary
TestAmerica Job ID: 160-17814-1
Qualifiers
Rad
Qualifier Qualifier Description
U Result is less than the sample detection limit.
X Tracer is outside acceptance limits.
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CNF Contains no Free Liquid
DER Duplicate error ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL, RA, RE, IN Indicates a Dilution, Re-analysis, Re-extraction, or additional Initial metals/anion analysis of the sample
DLC Decision level concentration
MDA Minimum detectable activity
EDL Estimated Detection Limit
MDC Minimum detectable concentration
MDL Method Detection Limit
ML Minimum Level (Dioxin)
NC Not Calculated
ND Not detected at the reporting limit (or MDL or EDL if shown)
PQL Practical Quantitation Limit
QC Quality Control
RER Relative error ratio
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
Page 4 of 551
TestAmerica St. Louis
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CASE NARRATIVE
Client: Tetra Tech EM Inc.
Project: West Lake Landfill
Report Number: 160-17814-1
With the exceptions noted as flags or footnotes, standard analytical protocols were followed in the analysis of the samples and no
problems were encountered or anomalies observed. In addition all laboratory quality control samples were within established control
limits, with any exceptions noted below. Each sample was analyzed to achieve the lowest possible reporting limit within the constraints of
the method. In some cases, due to interference or analytes present at high concentrations, samples were diluted. For diluted samples,
the reporting limits are adjusted relative to the dilution required.
TestAmerica St. Louis attests to the validity of the laboratory data generated by TestAmerica facilities reported herein. All analyses
performed by TestAmerica facilities were done using established laboratory SOPs that incorporate QA/QC procedures described in the
application methods. TestAmerica's operations groups have reviewed the data for compliance with the laboratory QA/QC plan, and data
have been found to be compliant with laboratory protocols unless otherwise noted below.
The test results in this report meet all NELAP requirements for parameters for which accreditation is required or available. Any
exceptions to NELAP requirements are noted in this report. Pursuant to NELAP, this report may not be reproduced, except in full, without
the written approval of the laboratory.
Calculations are performed before rounding to avoid round-off errors in calculated results.
All holding times were met and proper preservation noted for the methods performed on these samples, unless otherwise detailed in the
individual sections below.
All solid sample results for Chemistry analyses are reported on an "as received" basis unless otherwise indicated by the presence of a %
solids value in the method header. All soil/sediment sample results for radiochemistry analyses are based upon sample as dried and
disaggregated with the exception of tritium, carbon-14, and iodine-129 by gamma spectroscopy unless requested as wet weight by the
client."
This laboratory report is confidential and is intended for the sole use of TestAmerica and its client.
RECEIPT
The samples were received on 6/10/2016 9:45 AM; the samples arrived in good condition, properly preserved. The temperature of the
cooler at receipt was 19.8° C.
ISOTOPIC THORIUM (ALPHA SPECTROMETRY)
Samples AC-SED-4 (160-17814-1), AC-SED-6 (160-17814-2), AC-SED-7 (160-17814-3) and AC-SED-8 (160-17814-4) were analyzed for
Isotopic Thorium (Alpha Spectrometry) in accordance with DOE A01R_Th. The samples were dried on 06/16/2016, prepared on
06/22/2016 and analyzed on 07/02/2016 and 07/07/2016.
The following sample has a Th-229 tracer recovery above the 110% QC limit; (160-17814-A-3-C: 136%). The LCS (laboratory control
sample) has an acceptable spike recovery demonstrating acceptable sample preparation and instrument performance. The samples
associated with the batch have been truncated to 100% to reduce any potential bias a high carrier recovery may have. The data have
been qualified and reported.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
ISOTOPIC URANIUM (ALPHA SPECTROMETRY)
Samples AC-SED-4 (160-17814-1), AC-SED-6 (160-17814-2), AC-SED-7 (160-17814-3) and AC-SED-8 (160-17814-4) were analyzed for
Isotopic Uranium (Alpha Spectrometry) in accordance with DOE. The samples were dried on 06/16/2016, prepared on 06/22/2016 and
analyzed on 07/02/2016.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
RADIUM-226 BY GAMMA SPEC (21 DAY INGROWTH)
Samples AC-SED-4 (160-17814-1), AC-SED-6 (160-17814-2), AC-SED-7 (160-17814-3) and AC-SED-8 (160-17814-4) were analyzed for
Radium-226 by gamma spec (21 day ingrowth) in accordance with EPA GA_01_R. The samples were dried on 06/16/2016, prepared on
06/20/2016 and analyzed on 07/11/2016.
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Page 5 of 551
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Page 6 of 551
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Client Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Client Sample IE);: AC-SED-4
Date Collected; 06/10/16 06:35
Date Received; 06/10/16 09:45
TestAmerica Job ID: 160-17814-1
1LJ- "\imple III"" '
Matrix; Solid
Method: A-01-R -
Isotopic Thorium (Alpha Spectrometry)
Count Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Thorium-228
1.01
0.146
0.169
0.0658
0.0254
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-230
3.56
0.268
0.401
0.0278
0.00635
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-232
1.04
0.144
0.169
0.0150
0.00632
pCi/g
06/22/16 10:35
07/02/16 15:17
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Thorium-229
88.8
30.110
06/22/16 10:35
07/02/16 15:17
Method: A-01-R -
Isotopic Uranium (Alpha Spectrometry)
Count Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Uranium-233/234
0.767
0.136
0.151
0.0478
0.0150
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-235/236
0.0517
0.0391
0.0393
0.0222
0.00933
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-238
0.805
0.138
0.154
0.0178
0.00748
pCi/g
06/22/16 10:35
07/02/16 15:31
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Uranium-232
73.4
30.110
06/22/16 10:35
07/02/16 15:31
Method: GA-01-R
- Radium-226 & Other Gamma Emitters (GS)
Count Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Actinium-227
0.349
U
0.741
0.742
1.65
0.782
pCi/g
06/20/16 08:50
07/11/16 07:46
Actinium 228
1.17
0.272
0.297
0.179
0.0566
pCi/g
06/20/16 08:50
07/11/16 07:46
Bismuth-212
0.743
U
2.03
2.03
3.45
1.62
pCi/g
06/20/16 08:50
07/11/16 07:46
Bismuth-214
1.14
0.273
0.298
0.220
0.0951
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-210
0.0417
u
2.66
2.66
3.93
1.87
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-212
0.881
0.157
0.194
0.142
0.0638
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-214
1.17
0.227
0.257
0.230
0.103
pCi/g
06/20/16 08:50
07/11/16 07:46
Potassium-40
13.5
2.36
2.74
1.14
0.438
pCi/g
06/20/16 08:50
07/11/16 07:46
Protactinium-231
-1.65
u
4.78
4.78
8.03
3.88
pCi/g
06/20/16 08:50
07/11/16 07:46
Radium-226
1.14
0.273
0.298
0.220
0.0951
pCi/g
06/20/16 08:50
07/11/16 07:46
Radium-228
1.17
0.272
0.297
0.179
0.0566
pCi/g
06/20/16 08:50
07/11/16 07:46
Thorium-232
1.17
0.272
0.297
0.179
0.0566
pCi/g
06/20/16 08:50
07/11/16 07:46
Thorium-234
2.37
1.73
1.75
2.20
1.03
pCi/g
06/20/16 08:50
07/11/16 07:46
Thallium-208
0.365
0.115
0.121
0.0879
0.0362
pCi/g
06/20/16 08:50
07/11/16 07:46
Uranium-235
-0.263
u
0.652
0.652
1.09
0.527
pCi/g
06/20/16 08:50
07/11/16 07:46
Uranium-238
2.37
1.73
Count
1.75
Total
2.20
1.03
pCi/g
06/20/16 08:50
07/11/16 07:46
Other Detected
Uncert.
Uncert.
Radionuclides
Result
Qualifier
(2cr+/-)
(2cr+/-)
MDC
DLC
Unit
Prepared
Analyzed
Other Detected
None
pCi/g
06/20/16 08:50
07/11/16 07:46
Dil Fac
T"
1
1
Dil Fac
1
Dil Fac
1"
1
1
Dil Fac
1
Dil Fac
Dil Fac
1
Radionuclide
Page 7 of 551
TestAmerica St. Louis
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Client Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Client Sample ID: AC-SED-6
Date Collected; 06/10/16 06:40
Date Received; 06/10/16 09:45
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
I J- "V«nipll- III" * i- •
Matrix; Solid
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Thorium-228
1.07
0.150
0.175
0.0545
0.0195
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-230
2.82
0.241
0.338
0.0339
0.00920
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-232
1.19
0.156
0.185
0.0154
0.00647
pCi/g
06/22/16 10:35
07/02/16 15:17
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Thorium-229
82.6
30-110
06/22/16 10:35
07/02/16 15:17
Method: A-01-R -
Isotopic Uranium (Alpha Spectrometry)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Uranium-233/234
0.657
0.123
0.134
0.0314
0.00719
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-235/236
0.0425
0.0347
0.0348
0.0212
0.00894
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-238
0.821
0.137
0.153
0.0314
0.00717
pCi/g
06/22/16 10:35
07/02/16 15:31
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Uranium-232
79.3
30-110
06/22/16 10:35
07/02/16 15:31
Method: GA-01-R
- Radium-226 & Other Gamma Emitters (GS)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Actinium-227
0.409
U
0.557
0.559
0.923
0.425
pCi/g
06/20/16 08:50
07/11/16 07:46
Actinium 228
0.783
0.229
0.242
0.262
0.110
pCi/g
06/20/16 08:50
07/11/16 07:46
Bismuth-212
0.312
U
1.14
1.14
1.96
0.912
pCi/g
06/20/16 08:50
07/11/16 07:46
Bismuth-214
0.958
0.195
0.219
0.159
0.0698
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-210
1.13
u
1.68
1.68
2.75
1.30
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-212
0.907
0.145
0.186
0.141
0.0648
pCi/g
06/20/16 08:50
07/11/16 07:46
Lead-214
1.21
0.231
0.263
0.191
0.0875
pCi/g
06/20/16 08:50
07/11/16 07:46
Potassium-40
17.0
2.11
2.73
1.01
0.420
pCi/g
06/20/16 08:50
07/11/16 07:46
Protactinium-231
-0.0000001
u
3.54
3.54
6.02
2.92
pCi/g
06/20/16 08:50
07/11/16 07:46
Radium-226
36
0.958
0.195
0.219
0.159
0.0698
pCi/g
06/20/16 08:50
07/11/16 07:46
Radium-228
0.783
0.229
0.242
0.262
0.110
pCi/g
06/20/16 08:50
07/11/16 07:46
Thorium-232
0.783
0.229
0.242
0.262
0.110
pCi/g
06/20/16 08:50
07/11/16 07:46
Thorium-234
0.834
u
0.741
0.746
2.12
1.00
pCi/g
06/20/16 08:50
07/11/16 07:46
Thallium-208
0.361
0.114
0.120
0.100
0.0447
pCi/g
06/20/16 08:50
07/11/16 07:46
Uranium-235
0.102
u
0.190
0.190
0.951
0.460
pCi/g
06/20/16 08:50
07/11/16 07:46
Uranium-238
0.834
u
0.741
0.746
2.12
1.00
pCi/g
06/20/16 08:50
07/11/16 07:46
Count
Total
Other Detected
Uncert.
Uncert.
Radionuclides
Result
Qualifier
(2cr+/-)
(2cr+/-)
MDC
DLC
Unit
Prepared
Analyzed
Other Detected
Radionuclide
None
pCi/g
Dil Fac
1"
1
1
Dil Fac
1
Dil Fac
T"
1
1
Dil Fac
1
Dil Fac
06/20/16 08:50 07/11/16 07:46
Dil Fac
1
Page 8 of 551
TestAmerica St. Louis
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Client Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Client Sample ID: AC-SED-7
Date Collected; 06/10/16 06:50
Date Received; 06/10/16 09:45
Method: A-01-R - Isotopic Thorium (Alpha Spectrometry)
I .'til- 1,1 .'timipl"" III' mi mi " ill-11 1
Matrix; Solid
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Thorium-228
0.728
0.119
0.134
0.0628
0.0245
pCi/g
06/22/16 10:35
07/07/16 13:10
Thorium-230
2.45
0.212
0.296
0.0300
0.00817
pCi/g
06/22/16 10:35
07/07/16 13:10
Thorium-232
0.656
0.109
0.123
0.0251
0.00575
pCi/g
06/22/16 10:35
07/07/16 13:10
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Thorium-229
136
X
30-110
06/22/16 10:35
07/07/16 13:10
Method: A-01-R -
Isotopic Uranium (Alpha Spectrometry)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Uranium-233/234
0.513
0.114
0.122
0.0410
0.0112
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-235/236
0.0311
0.0311
0.0312
0.0233
0.00982
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-238
0.789
0.140
0.155
0.0344
0.00787
pCi/g
06/22/16 10:35
07/02/16 15:31
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Uranium-232
67.5
30-110
06/22/16 10:35
07/02/16 15:31
Method: GA-01-R
- Radium-226 & Other Gamma Emitters (GS)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Actinium-227
0.600
U
1.27
1.27
2.13
1.03
pCi/g
06/20/16 08:50
07/11/16 08:45
Actinium 228
0.750
0.243
0.255
0.426
0.188
pCi/g
06/20/16 08:50
07/11/16 08:45
Bismuth-212
-0.813
U
1.72
1.73
2.69
1.27
pCi/g
06/20/16 08:50
07/11/16 08:45
Bismuth-214
1.07
0.247
0.271
0.194
0.0858
pCi/g
06/20/16 08:50
07/11/16 08:45
Lead-210
-1.56
u
1.73
1.74
5.63
2.73
pCi/g
06/20/16 08:50
07/11/16 08:45
Lead-212
0.759
0.134
0.166
0.128
0.0582
pCi/g
06/20/16 08:50
07/11/16 08:45
Lead-214
1.39
0.188
0.238
0.175
0.0785
pCi/g
06/20/16 08:50
07/11/16 08:45
Potassium-40
16.2
2.24
2.79
0.731
0.262
pCi/g
06/20/16 08:50
07/11/16 08:45
Protactinium-231
0.568
u
2.29
2.29
7.33
3.56
pCi/g
06/20/16 08:50
07/11/16 08:45
Radium-226
1.07
0.247
0.271
0.194
0.0858
pCi/g
06/20/16 08:50
07/11/16 08:45
Radium-228
0.750
0.243
0.255
0.426
0.188
pCi/g
06/20/16 08:50
07/11/16 08:45
Thorium-232
0.750
0.243
0.255
0.426
0.188
pCi/g
06/20/16 08:50
07/11/16 08:45
Thorium-234
0.970
u
0.746
0.752
2.06
0.971
pCi/g
06/20/16 08:50
07/11/16 08:45
Thallium-208
0.336
0.0884
0.0950
0.0672
0.0276
pCi/g
06/20/16 08:50
07/11/16 08:45
Uranium-235
-0.344
u
0.443
0.444
1.33
0.651
pCi/g
06/20/16 08:50
07/11/16 08:45
Uranium-238
0.970
u
0.746
0.752
2.06
0.971
pCi/g
06/20/16 08:50
07/11/16 08:45
Count
Total
Other Detected
Uncert.
Uncert.
Radionuclides
Result
Qualifier
(2cr+/-)
(2cr+/-)
MDC
DLC
Unit
Prepared
Analyzed
Other Detected
None
pCi/g
06/20/16 08:50
07/11/16 08:45
Dil Fac
1"
1
1
Dil Fac
1
Dil Fac
T"
1
1
Dil Fac
1
Dil Fac
Dil Fac
1
Radionuclide
Page 9 of 551
TestAmerica St. Louis
-------
Client Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Client Sample ID: AC-SED-8
Date Collected; 06/10/16 07:00
Date Received; 06/10/16 09:45
I .'til- 1,1 .'iitiripll"" III' ii" '-17-II i i
Matrix; Solid
Method: A-01-R -
Isotopic Thorium (Alpha Spectrometry)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Thorium-228
1.07
0.153
0.177
0.0652
0.0248
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-230
3.77
0.281
0.423
0.0157
0.00660
pCi/g
06/22/16 10:35
07/02/16 15:17
Thorium-232
1.11
0.152
0.178
0.0156
0.00656
pCi/g
06/22/16 10:35
07/02/16 15:17
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Thorium-229
89.2
30-110
06/22/16 10:35
07/02/16 15:17
Method: A-01-R -
Isotopic Uranium (Alpha Spectrometry)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Uranium-233/234
0.757
0.143
0.157
0.0533
0.0167
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-235/236
0.0330
0.0330
0.0331
0.0247
0.0104
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-238
0.826
0.148
0.163
0.0198
0.00835
pCi/g
06/22/16 10:35
07/02/16 15:31
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Uranium-232
68.8
30-110
06/22/16 10:35
07/02/16 15:31
Method: GA-01-R
- Radium-226 & Other Gamma Emitters (GS)
Count
Total
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Actinium-227
1.14
1.08
1.09
1.48
0.684
pCi/g
06/20/16 08:50
07/11/16 08:46
Actinium 228
0.921
0.314
0.327
0.355
0.137
pCi/g
06/20/16 08:50
07/11/16 08:46
Bismuth-212
-0.608
U
1.86
1.86
2.86
1.30
pCi/g
06/20/16 08:50
07/11/16 08:46
Bismuth-214
1.42
0.310
0.343
0.228
0.0959
pCi/g
06/20/16 08:50
07/11/16 08:46
Lead-210
3.66
2.62
2.66
3.47
1.62
pCi/g
06/20/16 08:50
07/11/16 08:46
Lead-212
1.04
0.194
0.236
0.183
0.0828
pCi/g
06/20/16 08:50
07/11/16 08:46
Lead-214
1.62
0.253
0.305
0.264
0.118
pCi/g
06/20/16 08:50
07/11/16 08:46
Potassium-40
17.0
2.95
3.43
1.41
0.541
pCi/g
06/20/16 08:50
07/11/16 08:46
Protactinium-231
-1.57
U
4.39
4.39
7.42
3.54
pCi/g
06/20/16 08:50
07/11/16 08:46
Radium-226
1.42
0.310
0.343
0.228
0.0959
pCi/g
06/20/16 08:50
07/11/16 08:46
Radium-228
0.921
0.314
0.327
0.355
0.137
pCi/g
06/20/16 08:50
07/11/16 08:46
Thorium-232
0.921
0.314
0.327
0.355
0.137
pCi/g
06/20/16 08:50
07/11/16 08:46
Thorium-234
-1.10
u
1.68
1.68
3.92
1.87
pCi/g
06/20/16 08:50
07/11/16 08:46
Thallium-208
0.398
0.105
0.113
0.0522
0.0165
pCi/g
06/20/16 08:50
07/11/16 08:46
Uranium-235
0.239
u
0.632
0.632
1.07
0.509
pCi/g
06/20/16 08:50
07/11/16 08:46
Uranium-238
-1.10
u
1.68
1.68
3.92
1.87
pCi/g
06/20/16 08:50
07/11/16 08:46
Count
Total
Other Detected
Uncert.
Uncert.
Radionuclides
Result
Qualifier
(2cr+/-)
(2cr+/-)
MDC
DLC
Unit
Prepared
Analyzed
Other Detected
None
pCi/g
06/20/16 08:50
07/11/16 08:46
Dil Fac
1"
1
1
Dil Fac
1
Dil Fac
T"
1
1
Dil Fac
1
Dil Fac
Dil Fac
1
Radionuclide
Page 10 of 551
TestAmerica St. Louis
-------
Tracer/Carrier Summary
Client: Tetra Tech EM Inc.
TestAmerica Job ID: 160-17814-1
Project/Site: West Lake Landfill
Method: A-01-R -
Isotopic Thorium (Alpha Spectrometry)
Matrix; Solid
Prep Type; Total/NA
—
Percent Yield (Acceptance Limits)
Th-229
Lab Sample ID
Client Sample ID
(30-110)
160-17814-1
AC-SED-4
88.8
160-17814-1 DU
AC-SED-4
88.9
160-17814-2
AC-SED-6
82.6
160-17814-3
AC-SED-7
136 X
160-17814-4
AC-SED-8
89.2
ICS 160-257492/2-A
Lab Control Sample
90.6
MB 160-257492/1-A
Method Blank
82.6
Tracer/Carrier Legend
Th-229 = Thorium-229
Method: A-01-R -
Isotopic Uranium (Alpha Spectrometry)
Matrix; Solid
Prep Type; Total/NA
—
Percent Yield (Acceptance Limits)
U-232
Lab Sample ID
Client Sample ID
(30-110)
160-17814-1
AC-SED-4
73.4
160-17814-1 DU
AC-SED-4
65.3
160-17814-2
AC-SED-6
79.3
160-17814-3
AC-SED-7
67.5
160-17814-4
AC-SED-8
68.8
ICS 160-257935/2-A
Lab Control Sample
79.9
MB 160-257935/1-A
Method Blank
71.3
Tracer/Carrier Legend
U-232 = Uranium-232
TestAmerica St. Louis
Page 11 of 551
-------
QC Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Meth ' ill I otopic Thorium (Alpha Spectrome-i ¦
Lab Sample ID: MB 160-257492/1-A
Matrix: Solid
Analysis Batch: 259078
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 257492
Count
Total
MB
MB
Uncert.
Uncert.
Analyte
Result
Qualifier
(2ct+/-)
(2ct+/-)
MDC
DLC
Unit
Prepared Analyzed Dil Fac
Thorium-228
0.1309
0.0590
0.0600
0.0620
0.0233
pCi/g
06/22/16 10:35 07/02/16 15:17 1
Thorium-230
0.1162
0.0488
0.0497
0.0154
0.00647
pCi/g
06/22/16 10:35 07/02/16 15:17 1
Thorium-232
0.002972
U
0.0110
0.0110
0.0282
0.00644
pCi/g
06/22/16 10:35 07/02/16 15:17 1
MB
MB
Tracer
%Yield
Qualifier
Limits
Prepared Analyzed Dil Fac
Thorium-229
82.6
30.110
06/22/16 10:35 07/02/16 15:17 1
Lab Sample ID: LCS 160-257492/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch
: 259080
Prep Batch: 257492
Total
Spike
LCS
LCS
Uncert.
% Rec.
Analyte
Added
Result
Qual
(2ct+/-)
MDC
DLC
Unit
% Rec Limits
Thorium-230
24.5
26.83
2.49
0.0307
0.0129
pCi/g
110 81.118
LCS LCS
Tracer %Yield Qualifier
Limits
Thorium-229
90.6
30.110
Lab Sample ID: 160-17814-1 DU
Client Sample ID: AC-SED-4
Matrix: Solid
Prep Type: Total/NA
Analysis Batch
: 259082
Prep Batch: 257492
Total
Sample Sample
DU
DU
Uncert.
RER
Analyte
Result Qual
Result
Qual
(2ct+/-)
MDC
DLC
Unit
RER Limit
Thorium-228
1.01
0.9640
0.165
0.0589
0.0217
pCi/g
0.14 1
Thorium-230
3.56
3.480
0.397
0.0286
0.00654
pCi/g
0.10 1
Thorium-232
1.04
0.9194
0.158
0.0285
0.00651
pCi/g
0.37 1
DU DU
Tracer %Yield Qualifier
Limits
Thorium-229
88.9
30.110
Lab Sample ID: MB 160-257935/1-A
Matrix: Solid
Analysis Batch: 259144
Analyte
MB
Result
MB
Qualifier
Count
Uncert.
(2ct+/-)
Total
Uncert.
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Uranium-233/234
0.03094
0.0277
0.0278
0.0186
0.00782
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-235/236
-0.006417
U
0.00908
0.00909
0.0506
0.0138
pCi/g
06/22/16 10:35
07/02/16 15:31
Uranium-238
0.006176
U
0.0124
0.0124
0.0185
0.00781
pCi/g
06/22/16 10:35
07/02/16 15:31
MB
MB
Tracer
%Yield
Qualifier
Limits
Prepared
Analyzed
Uranium-232
71.3
30-110
06/22/16 10:35
07/02/16 15:31
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 257935
Dil Fac
T"
1
1
Dil Fac
1
Page 12 of 551
TestAmerica St. Louis
-------
QC Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Meth ' ill I atopic Uranium (Alpha Spectrome m. i. itiriuecl)
Lab Sample ID: LCS 160-257935/2-A
Matrix: Solid
Analysis Batch: 259145
Analyte
Uranium-233/23
4
Uranium-238
Tracer
LCS LCS
%Yield Qualifier
Uranium-232
79.9
Spike
Added
637
6.51
Limits
30-110
Lab Sample ID: 160-17814-1 DU
Matrix: Solid
Analysis Batch: 259147
Analyte
Uranium-233/23
4
Uranium-235/23
6
Uranium-238
Tracer
Uranium-232
LCS LCS
Result Qual
6.283
6.600
Sample Sample
Result Qual
0.767
0.0517
0.805
DU DU
%Yield Qualifier Limits
65.3 30- 110
DU DU
Result Qual
0.7844
0.01978 U
0.8740
Total
Uncert.
(2ct+/-)
Total
Uncert.
(2ct+/-)
0.161
0.171
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Prep Batch: 257935
MDC
DLC Unit
0.0368 0.0683
% Rec.
% Rec Limits
0.651 0.0426 0.0126 pCi/g
0.678 0.0173 0.00728 pCi/g
99 84.120
101 82 -122
Client Sample ID: AC-SED-4
Prep Type: Total/NA
Prep Batch: 257935
MDC DLC Unit
0.0448 0.0122 pCi/g
RER
RER Limit
0.05 T"
0.0214 pCi/g
0.0376 0.00859 pCi/g
0.42
0.21
Lab Sample ID: MB 160-257060/1-A
Matrix: Solid
Analysis Batch: 259963
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 257060
Analyte
MB
Result
MB
Qualifier
Count
Uncert.
(2ct+/-)
Total
Uncert.
(2ct+/-)
MDC
DLC
Unit
Prepared
Analyzed
Actinium-227
0.2838
U
0.646
0.647
1.10
0.511
pC
/g
06/20/16 08:50
07/11/16 07:48
Actinium 228
0.08187
U
0.179
0.179
0.246
0.0968
pC
/g
06/20/16 08:50
07/11/16 07:48
Bismuth-212
-0.05294
u
0.795
0.795
1.87
0.853
pC
/g
06/20/16 08:50
07/11/16 07:48
Bismuth-214
0.08999
u
0.0680
0.0687
0.315
0.146
pC
/g
06/20/16 08:50
07/11/16 07:48
Lead-210
-0.6987
u
1.04
1.04
2.36
1.10
pC
/g
06/20/16 08:50
07/11/16 07:48
Lead-212
-0.09505
u
0.0534
0.0548
0.208
0.0981
pC
/g
06/20/16 08:50
07/11/16 07:48
Lead-214
0.04168
u
0.104
0.104
0.185
0.0834
pC
/g
06/20/16 08:50
07/11/16 07:48
Potassium-40
-0.1195
u
0.868
0.868
1.21
0.501
pC
/g
06/20/16 08:50
07/11/16 07:48
Protactinium-231
0.5009
u
1.33
1.34
3.17
1.48
pC
/g
06/20/16 08:50
07/11/16 07:48
Radium-226
0.08999
u
0.0680
0.0687
0.315
0.146
pC
/g
06/20/16 08:50
07/11/16 07:48
Radium-228
0.08187
u
0.179
0.179
0.246
0.0968
pC
/g
06/20/16 08:50
07/11/16 07:48
Thorium-232
0.08187
u
0.179
0.179
0.246
0.0968
pC
/g
06/20/16 08:50
07/11/16 07:48
Thorium-234
0.3719
u
0.986
0.987
1.46
0.672
pC
/g
06/20/16 08:50
07/11/16 07:48
Thallium-208
0.05460
0.0364
0.0368
0.0718
0.0298
pC
/g
06/20/16 08:50
07/11/16 07:48
Uranium-235
-0.001966
u
0.252
0.252
0.446
0.207
pC
/g
06/20/16 08:50
07/11/16 07:48
Uranium-238
0.3719
u
0.986
0.987
1.46
0.672
pC
/g
06/20/16 08:50
07/11/16 07:48
Dil Fac
TestAmerica St. Louis
Page 13 of 551
-------
QC Sample Results
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
TestAmerica Job ID: 160-17814-1
Count
Total
Other Detected
MB MB
Uncert.
Uncert.
Radionuclides
Result Qualifier
(2cr+/-)
(2cr+/-)
MDC
DLC
Unit
Prepared
Analyzed Dil Fac
Other Detected
None
pCi/g
06/20/16 08:50
07/11/16 07:48 1
Radionuclide
Lab Sample ID: LCS 160-257060/2-A
Client Sample ID: Lab Control Sample
Matrix: Solid
Prep Type: Total/NA
Analysis Batch
259965
Prep Batch: 257060
Total
Spike
LCS
LCS
Uncert.
% Rec.
Analyte
Added
Result
Qual
(2ct+/-)
MDC
DLC
Unit
% Rec
Limits
Americium-241
97.1
95.67
10.0
1.02
0.507
pCi/g
99
87.116
Cesium-137
29.6
28.64
3.06
0.254
0.122
pCi/g
97
87 -120
Cobalt-60
16.9
15.99
1.66
0.0831
0.0341
pCi/g
94
87.115
Lab Sample ID: 160-17814-1 DU
Client Sample ID: AC-SED-4
Matrix: Solid
Prep Type: Total/NA
Analysis Batch
259965
Prep Batch: 257060
Total
Sample
Sample
DU
DU
Uncert.
RER
Analyte
Result
Qual
Result
Qual
(2ct+/-)
MDC
DLC
Unit
RER Limit
Actinium-227
0.349
U
-0.4288
U
1.04
1.40
0.667
pCi/g
0.44 1
Actinium 228
1.17
0.8354
0.249
0.201
0.0782
pCi/g
0.61 1
Bismuth-212
0.743
U
0.4704
U
0.805
1.36
0.610
pCi/g
0.1 1
Bismuth-214
1.14
1.230
0.245
0.107
0.0436
pCi/g
0.16 1
Lead-210
0.0417
u
0.05687
u
2.06
3.51
1.68
pCi/g
0 1
Lead-212
0.881
0.8705
0.178
0.147
0.0686
pCi/g
0.03 1
Lead-214
1.17
1.133
0.217
0.165
0.0750
pCi/g
0.07 1
Potassium-40
13.5
14.87
2.64
1.03
0.424
pCi/g
0.26 1
Protactinium-231
-1.65
u
-1.029
u
3.40
5.70
2.77
pCi/g
0.08 1
Radium-226
1.14
1.230
0.245
0.107
0.0436
pCi/g
0.16 1
Radium-228
1.17
0.8354
0.249
0.201
0.0782
pCi/g
0.61 1
Thorium-232
1.17
0.8354
0.249
0.201
0.0782
pCi/g
0.61 1
Thorium-234
2.37
-0.02837
u
1.32
2.26
1.09
pCi/g
0.78 1
Thallium-208
0.365
0.2425
0.0812
0.0715
0.0306
pCi/g
0.61 1
Uranium-235
-0.263
u
-0.1956
u
0.343
1.02
0.495
pCi/g
0.07 1
Uranium-238
2.37
-0.02837
u
1.32
Total
2.26
1.09
pCi/g
0.78 1
Other Detected
Sample
Sample
DU
DU
Uncert.
RER
Radionuclides
Result
Qual
Result
Qual
(2cr+/-)
MDC
DLC
Unit
RER Limit
Other Detected
None
None
pCi/g
Radionuclide
Page 14 of 551
TestAmerica St. Louis
-------
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
QC Association Summary
TestAmerica Job ID: 160-17814-1
iii caa
Leach Batch: 256643
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
160-17814-1
AC-SED-4
Total/NA
Solid
Dry and Grind
160-17814-1 DU
AC-SED-4
Total/NA
Solid
Dry and Grind
160-17814-2
AC-SED-6
Total/NA
Solid
Dry and Grind
160-17814-3
AC-SED-7
Total/NA
Solid
Dry and Grind
160-17814-4
AC-SED-8
Total/NA
Solid
Dry and Grind
Prep Batch: 257060
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
160-17814-1
AC-SED-4
Total/NA
Solid
F
ll_Geo-21
256643
160-17814-1 DU
AC-SED-4
Total/NA
Solid
F
ll_Geo-21
256643
160-17814-2
AC-SED-6
Total/NA
Solid
F
ll_Geo-21
256643
160-17814-3
AC-SED-7
Total/NA
Solid
F
ll_Geo-21
256643
160-17814-4
AC-SED-8
Total/NA
Solid
F
ll_Geo-21
256643
ICS 160-257060/2-A
Lab Control Sample
Total/NA
Solid
F
ll_Geo-21
MB 160-257060/1-A
Method Blank
Total/NA
Solid
F
ll_Geo-21
Prep Batch: 257492
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
160-17814-1
AC-SED-4
Total/NA
Solid
ExtChrom
256643
160-17814-1 DU
AC-SED-4
Total/NA
Solid
ExtChrom
256643
160-17814-2
AC-SED-6
Total/NA
Solid
ExtChrom
256643
160-17814-3
AC-SED-7
Total/NA
Solid
ExtChrom
256643
160-17814-4
AC-SED-8
Total/NA
Solid
ExtChrom
256643
ICS 160-257492/2-A
Lab Control Sample
Total/NA
Solid
ExtChrom
MB 160-257492/1-A
Method Blank
Total/NA
Solid
ExtChrom
Prep Batch: 257935
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
160-17814-1
AC-SED-4
Total/NA
Solid
ExtChrom
256643
160-17814-1 DU
AC-SED-4
Total/NA
Solid
ExtChrom
256643
160-17814-2
AC-SED-6
Total/NA
Solid
ExtChrom
256643
160-17814-3
AC-SED-7
Total/NA
Solid
ExtChrom
256643
160-17814-4
AC-SED-8
Total/NA
Solid
ExtChrom
256643
ICS 160-257935/2-A
Lab Control Sample
Total/NA
Solid
ExtChrom
MB 160-257935/1-A
Method Blank
Total/NA
Solid
ExtChrom
Page 15 of 551
TestAmerica St. Louis
-------
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Lab Chronicle
TestAmerica Job ID: 160-17814-1
Client Sample ID: AC-SED-4
Date Collected; 06/10/16 06:35
Date Received; 06/10/16 09:45
I .ill" ''' .ilTiplle III "" ' III..
Matrix; Solid
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257492
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259081
07/02/16 15:17
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257935
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259146
07/02/16 15:31
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
Fill_Geo-21
257060
06/20/16 08:50
R1S
TALSL
Total/NA
Analysis
GA-01-R
1
259964
07/11/16 07:46
RTM
TALSL
Client Sample ID: AC-SED-6
Date Collected; 06/10/16 06:40
Date Received; 06/10/16 09:45
I .ill" '''.ilTiplle III"" ' III.."
Matrix; Solid
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257492
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259083
07/02/16 15:17
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257935
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259148
07/02/16 15:31
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
Fill_Geo-21
257060
06/20/16 08:50
R1S
TALSL
Total/NA
Analysis
GA-01-R
1
259962
07/11/16 07:46
RTM
TALSL
Client Sample ID: AC-SED-7
Date Collected; 06/10/16 06:50
Date Received; 06/10/16 09:45
I >il" ''' .'iirriplle III ¦ ' i.." '
Matrix; Solid
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257935
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259149
07/02/16 15:31
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
ExtChrom
257492
06/22/16 10:35
SCB
TALSL
Total/NA
Analysis
A-01-R
1
259665
07/07/16 13:10
ALD
TALSL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TALSL
Total/NA
Prep
Fill_Geo-21
257060
06/20/16 08:50
R1S
TALSL
Total/NA
Analysis
GA-01-R
1
259963
07/11/16 08:45
RTM
TALSL
Page 16 of 551
TestAmerica St. Louis
-------
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Lab Chronicle
TestAmerica Job ID: 160-17814-1
Client Sample ID: AC-SED-8
Date Collected; 06/10/16 07:00
Date Received; 06/10/16 09:45
I J- "V«nipll- III" * i i
Matrix; Solid
Laboratory References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566
Batch
Batch
Dilution
Batch
Prepared
Prep Type
Type
Method
Run Factor
Number
or Analyzed
Analyst
Lab
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TAL SL
Total/NA
Prep
ExtChrom
257492
06/22/16 10:35
SCB
TAL SL
Total/NA
Analysis
A-01-R
1
259085
07/02/16 15:17
ALD
TAL SL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TAL SL
Total/NA
Prep
ExtChrom
257935
06/22/16 10:35
SCB
TAL SL
Total/NA
Analysis
A-01-R
1
259150
07/02/16 15:31
ALD
TAL SL
Total/NA
Leach
Dry and Grind
256643
06/16/16 09:44
DRO
TAL SL
Total/NA
Prep
Fill_Geo-21
257060
06/20/16 08:50
R1S
TAL SL
Total/NA
Analysis
GA-01-R
1
259964
07/11/16 08:46
RTM
TAL SL
Page 17 of 551
TestAmerica St. Louis
-------
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Certification Summary
TestAmerica Job ID: 160-17814-1
Laboratory';: TestAmeri uiis
Unless otherwise noted, all analytes for this laboratory were covered under each certification below.
Authority Program EPA Region Certification ID Expiration Date
Louisiana NELAP 6 04080 06-30-17
The following analytes are included in this report, but certification is not offered by the governing authority:
Analysis Method
Prep Method
Matrix
Analyte
A-01-R
ExtChrom
Solid
Thorium-228
A-01-R
ExtChrom
Solid
Thorium-230
A-01-R
ExtChrom
Solid
Thorium-232
A-01-R
ExtChrom
Solid
Uranium-235/236
GA-01-R
Fi
l_Geo-21
Solid
Actinium 228
GA-01-R
Fi
l_Geo-21
Solid
Actinium-227
GA-01-R
Fi
l_Geo-21
Solid
Bismuth-212
GA-01-R
Fi
l_Geo-21
Solid
Bismuth-214
GA-01-R
Fi
l_Geo-21
Solid
Lead-210
GA-01-R
Fi
l_Geo-21
Solid
Lead-212
GA-01-R
Fi
l_Geo-21
Solid
Lead-214
GA-01-R
Fi
l_Geo-21
Solid
Potassium-40
GA-01-R
Fi
l_Geo-21
Solid
Protactinium-231
GA-01-R
Fi
l_Geo-21
Solid
Radium-226
GA-01-R
Fi
l_Geo-21
Solid
Radium-228
GA-01-R
Fi
l_Geo-21
Solid
Thallium-208
GA-01-R
Fi
l_Geo-21
Solid
Thorium-232
GA-01-R
Fi
l_Geo-21
Solid
Thorium-234
GA-01-R
Fi
l_Geo-21
Solid
Uranium-235
GA-01-R
Fi
I Geo-21
Solid
Uranium-238
Page 18 of 551
TestAmerica St. Louis
-------
Method Summary
Client: Tetra Tech EM Inc. TestAmerica Job ID: 160-17814-1
Project/Site: West Lake Landfill
Method Method Description Protocol Laboratory
A-01-R
Isotopic Thorium (Alpha Spectrometry)
DOE
TAL SL
A-01-R
Isotopic Uranium (Alpha Spectrometry)
DOE
TAL SL
GA-01-R
Radium-226 & Other Gamma Emitters (GS)
DOE
TAL SL
Protocol References:
DOE = U.S. Department of Energy
Laboratory References:
TAL SL = TestAmerica St. Louis, 13715 Rider Trail North, Earth City, MO 63045, TEL (314)298-8566
Page 19 of 551
TestAmerica St. Louis
-------
Client: Tetra Tech EM Inc.
Project/Site: West Lake Landfill
Sample Summary
TestAmerica Job ID: 160-17814-1
Lab Sample ID
Client Sample ID
Matrix
Collected
160-17814-1
AC-SED-4
Solid
06/10/16 06:35
160-17814-2
AC-SED-6
Solid
06/10/16 06:40
160-17814-3
AC-SED-7
Solid
06/10/16 06:50
160-17814-4
AC-SED-8
Solid
06/10/16 07:00
Received
Page 20 of 551
TestAmerica St. Louis
-------
Lab Name: TestAmerica St. Louis
REAGENT TRACEABILITY SUMMARY
Job No. : 160-17814-1
SDG No.:
Reagent ID
Exp
Date
Prep
Date
Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Analyte
Concentration
Reagent ID
Volume
Added
82232-334_00001
06/03/60
Eckert & Ziegler, Lot 82232-334
(Purchased Reagent)
Americium-2 41
7.281 Bg
Pu-239
7.137 Bg
Thorium-230
7.63 Bg
82233-334_00001
06/03/60
Eckert & Zigler, Lot 82233-334
(Purchased Reagent)
Americium-2 41
5.114 Bg
Pu-239
6.064 Bg
Thorium-230
4.95 Bg
82235-334_00001
06/04/60
Eckert & Ziegler, Lot 82235-334
(Purchased Reagent)
Americium-2 41
7.466 Bg
Pu-239
6.897 Bg
Thorium-230
7.167 Bg
82236-334_00001
06/02/60
Eckert & Ziegler, Lot 82236-334
(Purchased Reagent)
Americium-2 41
6.891 Bg
Pu-239
6.664 Bg
Thorium-230
7.107 Bg
82237-334_00003
06/01/60
Eckert & Ziegler, Lot 82237-334
(Purchased Reagent)
Americium-2 41
5.608 Bg
Pu-239
6.424 Bg
Thorium-230
5.856 Bg
82240-334_00001
06/08/60
Eckert & Ziegler, Lot 82240-334
(Purchased Reagent)
Americium-2 41
8.298 Bg
Pu-239
7.163 Bg
Thorium-230
6.304 Bg
82241-334_00001
06/08/60
Eckert & Ziegler, Lot 82241-334
(Purchased Reagent)
Americium-2 41
6.638 Bg
Pu-239
6.797 Bg
Thorium-230
6.629 Bg
82242-334_00001
06/08/60
Eckert & Ziegler, Lot 82242-334
(Purchased Reagent)
Americium-2 41
7.145 Bg
Pu-239
6.414 Bg
Thorium-230
6.583 Bg
82243-334_00001
06/09/60
Eckert & Ziegler, Lot 82243-334
(Purchased Reagent)
Americium-2 41
6.39 Bg
Pu-239
5.979 Bg
Thorium-230
5.856 Bg
82244-334_00001
06/09/60
Eckert & Zigler, Lot 82244-334
(Purchased Reagent)
Americium-2 41
6.897 Bg
Pu-239
6.717 Bg
Thorium-230
7.352 Bg
8224 6-334_00001
06/09/60
Eckert & Ziegler, Lot 82246-334
(Purchased Reagent)
Americium-2 41
6.002 Bg
Pu-239
5.353 Bg
Thorium-230
5.57 Bg
8224 7-334_00001
06/10/60
Eckert & Ziegler, Lot 82247-334
(Purchased Reagent)
Americium-2 41
6.291 Bg
Pu-239
5.746 Bg
Thorium-230
6.251 Bg
Source A 00001
04/01/59
02/23/11
water, Lot 79670-334
0. 9986
Source
Gamma Ampuole 00001
0.9986 g
Americium-2 41
9. 4429 Bg
Cd-109
132.909 Bg
Ce-139
4 . 4538 Bg
Cesium-137
3.7296 Bg
Co-57
2.9513 Bg
Cobalt-60
6.2002 Bg
Page 21 of 551
-------
REAGENT TRACEABILITY SUMMARY
Lab Name: TestAmerica St. Louis Job No.: 160-17814-1
SDG No.:
Reagent ID
Exp
Date
Prep
Date
Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Analyte
Concentration
Reagent ID
Volume
Added
Hg-203
9.6996 Bg
Sn-113
7.62 6 6 Bg
Y-88
12.712 Bg
.Gamma Ampuole 00001
04/07/59
Analytics, Lot 79670-334
(Purchased Reagent)
Americium-2 41
9442.9 Bg
Cd-109
132909 Bg
Ce-139
4 4 53.8 Bg
Cesium-137
3729.6 Bg
Co-57
2951.3 Bg
Cobalt-60
6200.2 Bg
Hg-203
9699.6 Bg
Sn-113
7 626.6 Bg
Y-88
12712 Bg
Source C 00001
04/01/59
02/23/12
water, Lot 79670-334
1. 0148 g
Gamma Ampuole 00001
1.0148 g
Americium-2 41
9442.9 Bg
Cd-109
132909 Bg
Ce-139
4 4 53.8 Bg
Cesium-137
3729.6 Bg
Co-57
2951.3 Bg
Cobalt-60
6200.2 Bg
Hg-203
9699.6 Bg
Sn-113
7 626.6 Bg
Y-88
12712 Bg
.Gamma Ampuole 00001
04/07/59
Analytics, Lot 79670-334
(Purchased Reagent)
Americium-2 41
9442.9 Bg
Cd-109
132909 Bg
Ce-139
4 4 53.8 Bg
Cesium-137
3729.6 Bg
Co-57
2951.3 Bg
Cobalt-60
6200.2 Bg
Hg-203
9699.6 Bg
Sn-113
7 626.6 Bg
Y-88
12712 Bg
Source D 00001
04/01/59
02/23/11
water, Lot 79670-334
0.9781 g
Gamma Ampuole 00001
0. 9781 g
Americium-2 41
9442.9 Bg
Cd-109
132909 Bg
Ce-139
4 4 53.8 Bg
Cesium-137
3729.6 Bg
Co-57
2951.3 Bg
Cobalt-60
6200.2 Bg
Hg-203
9699.6 Bg
Sn-113
7 626.6 Bg
Y-88
12712 Bg
.Gamma Ampuole 00001
04/07/59
Analytics, Lot 79670-334
(Purchased Reagent)
Americium-2 41
9442.9 Bg
Cd-109
132909 Bg
Ce-139
4 4 53.8 Bg
Cesium-137
3729.6 Bg
Co-57
2951.3 Bg
Cobalt-60
6200.2 Bg
Hg-203
9699.6 Bg
Sn-113
7 626.6 Bg
Page 22 of 551
-------
Lab Name: TestAmerica St. Louis
REAGENT TRACEABILITY SUMMARY
Job No. : 160-17814-1
SDG No.:
Reagent ID
Exp
Date
Prep
Date
Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Analyte
Concentration
Reagent ID
Volume
Added
Y-88
12712 Bq
Th-22 9_0 0020
08/05/16
07/16/15
0.1M HN03, Lot n/a
500 mL
Th-22 9 00017
15 mL
At-217
67 . 2296
dpm/mL
Thorium-22 9
67 . 2296
dpm/mL
.Th-22 9 00017
08/05/16
08/20/14
0.1M HN03, Lot n/a
100 mL
Th-22 9 00016
5.04 64 g
At-217
2240.99
dpm/mL
Thorium-22 9
2240.99
dpm/mL
. .Th-22 9 00016
08/06/64
Analytics, Lot 97790
(Purchased Reagent)
At-217
740.127 Bq/g
Thorium-22 9
740.127 Bq/g
TRM-2 00001
03/20/50
DOE, Lot TRM-2
(Purchased Reagent)
Lead-210
22.1 pCi/g
Radium-226
25.4 pCi/g
Thorium-230
24.5 pCi/g
Uranium-2 33/234
6.2 pCi/g
Uranium-238
6 pCi/g
Tuna Can LCS 00005
10/29/16
Analytics, Lot 74139-334
(Purchased Reagent)
Americium-2 41
219 dpm/g
Cesium-137
82.3 dpm/g
Cobalt-60
136 dpm/g
Tuna Can 00002
02/03/15
Eckert & Ziegler, Lot 81427-334
(Purchased Reagent)
Americium-2 41
1164 Bq
Cd-109
16 0 63 Bq
Ce-139
54 6 Bq
Cesium-137
4 65 Bq
Co-57
357 Bq
Cobalt-60
7 4 2 Bq
Hg-203
1208 Bq
Lead-210
15186 Bq
Sn-113
943 Bq
Y-88
1571 Bq
Tuna Can 00003
02/09/17
Eckert & Ziegler, Lot 90099
(Purchased Reagent)
Americium-2 41
1164 Bq
Cd-109
16373 Bq
Ce-139
54 9 Bq
Cesium-137
4 67 Bq
Co-57
362 Bq
Cobalt-60
7 35 Bq
Hg-203
1171 Bq
Lead-210
14 936 Bq
Sn-113
967 Bq
Y-88
1590 Bq
Tuna Can 00006
03/01/16
Eckert & Ziegler, Lot 83814-334
(Purchased Reagent)
Americium-2 41
1195 Bq
Cd-109
16353 Bq
Ce-139
543 Bq
Cesium-137
453 Bq
Co-57
354 Bq
Cobalt-60
7 4 5 Bq
Hg-203
1175 Bq
Page 23 of 551
-------
Lab Name: TestAmerica St. Louis
REAGENT TRACEABILITY SUMMARY
Job No. : 160-17814-1
SDG No.:
Reagent ID
Exp
Date
Prep
Date
Dilutant
Used
Reagent
Final
Volume
Parent Reagent
Analyte
Concentration
Reagent ID
Volume
Added
Lead-210
14606 Bq
Sn-113
961 Bq
Y-88
1568 Bq
U-232_00034
03/24/17
03/23/16
DI Water, Lot n/a
250 mL
U-232 00009
2 mL
Uranium-232
82 .2457
dpm/mL
.U-232 00009
03/24/17
08/29/11
1M HN03, Lot 0
100 mL
U-232 00003
5.1609 g
Uranium-232
10280.7
dpm/mL
..U-232 00003
08/25/61
Eckert & Ziegler, Lot 85539-334
(Purchased Reagent)
Uranium-232
332 0.07 Bq/g
UNAT 00012
05/05/17
04/28/15
1M HN03, Lot n/a
2 00 mL
UNAT Parent 00001
2 0 mL
Uranium-2 33/234
70.6912
dpm/mL
Uranium-235
3.37064
dpm/mL
Uranium-238
7 2.265 dpm/mL
.UNAT Parent 00001
05/05/17
05/03/13
1M HN03, Lot n/a
2 00 mL
UNAT Ampoule 00001
19.2509
g
Uranium-2 33/234
706.912
dpm/mL
Uranium-235
33.7064
dpm/mL
Uranium-238
7 22.65 dpm/mL
..UNAT Ampoule 00001
03/30/58
New Brunswick Lab, Lot CRM 145
(Purchased Reagent)
Uranium-2 33/234
7 344.2 dpm/g
Uranium-235
350.18 dpm/g
Uranium-238
7507.7 dpm/g
Page 24 of 551
-------
Reagent
82232-334 00001
Page 25 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404'352*8677
Fax 404*352-2837
www.analyticsinc.com
82232-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk:
Customer: Test America/St. Louis
P.O. No.: 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eclcert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
Reference Date: 3-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope Activity (Bq) (keV) years ua % U
Th-230
7.630E+00
4420-4800
7.540E+04
0.7
1.1
2.6
Pu-239
7.13TE+00
4950-5240
2.410E+04
0.7
1.1
2.6
Am-^241
7.281E+00
5280-5600
4.326E+02
0.7
1.1
2.6
Total
Activity
2.210E+01
3000-8000
0.4
1.1
2.3
^Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 26 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.48 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
OA Approved:
E. A. Taskaev, OA Manager Alternate
CAUf?'9'-<
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 27 of 551
-------
Reagent
82233-334 00001
Page 28 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82233-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer; Test America/St. Louis
P.O. No.: 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352*8677
Fax 404*352*2837
www.analytlcslnc.com
Reference Date;
3-Jun-2010
12:00 PM EST
Energy Range
Half-Life,
Uncertainty* Type (%)
Isotope
Activity (Bq)
(keV)
years
«A
«B
u
Th-230
4.950E+00
4420-4800
7.540E+04
0.8
1.1
2.7
Pu-239
6.064E+00
4950-5240
2.410E+04
0.7
1.1
2.6
Am-241
5,114E+00
5280-5600
4.326E+02
0.8
1.1
2.7
Total
Activity
1.616E+01
3000-8000
0.1
1.1
2.2
^Uncertainty: U - Relative expanded uncertainty, k = 2, See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tlbbitts Valencia, California 91355
Page 29 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x0.45 mm thick
stainless steel disk.
CAUTION; Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopic
Date: Q6-2
-------
Reagent
82235-334 00001
Page 31 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82235-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.: 2380182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404.352-8677
Fax 404-352*2837
www.arialyticsinc.com
Reference Date;
4-Jun-2010
12:00 PM EST
Energy Range
Half-Life,
Uncertainty* Type (%)
Isotope
Activity (Bq)
OceV)
years
%
u
Th-230
7.167E+00
4420-4800
7.840E+04
0.8
1.1
2.7
Pu-239
6.897E+00
4980-8240
2.410E+04
0.8
1.1
2.7
Am=241
7.466E+QQ
8280=8600-.
4.326E+02
0.8
1.1
2.7
Total
Activity
2.161E+01
3000-8000
0.8
1.1
2.4
¦^Uncertainty; U - Relativo expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
(y* sc jxr o.
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 32 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 10 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0,46 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon, coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, OA Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 33 of 551
-------
Reagent
82236-334 00001
Page 34 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82236-334
24,1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer; Test America/St. Louis
P.O. No,; 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eclcert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352"8677
Fax 404-352*2837
www.analyticsinc.com
Reference Date:
2-Jun-2010
12:00 PM EST
Energy Range
Half-Life,
Uncertainty* Type (%)
Isotope
Activity (Bq)
(keV)
years
Ua
uB
U
Th-230
7.107E+00
4420-4800
7.540E+04
0.7
1.1
2.6
Pu-239
6.664E+00
4950-B240
2.410E+04
0.8
1.1
2.7
Am-241
6.891E+00
.5280-5600
4.326E+02
0.7
1.1
2,6
Total
Activity
2.071E+01
3000-8000
0.4
1.1
2.3
Uncertainty: U - Relative expanded uncertainty, k - 2, See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tlbbitts Valencia, California 91355
Page 35 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area; 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.48 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, OA Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 36 of 551
-------
Reagent
82237-334 00003
Page 37 of 551
-------
• Eckert & Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82237-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.: 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4. IB, Revision 1, February, 1978, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352*8677
Fax 404-352-2837
www.analyticsinc.com
Reference Date:
l-Jun-2010
12:00 PM EST
Energy Range
Half-Life,
Uncertainty* Type (%)
Isotope
Activity (Bq)
CkeV)
years
Ua
Ub
U
Th-230
0.886E+OO
4420-4800
7.S40E+04
1.0
1.1
3.0
Pu-239
6.424E+00
4980-8240
2.410E+04
0.9
1.1
2.8
Am-241
5.608E+00
- —8280=5600
4.326E+02
1.0
1.1
3.0
Total
Activity
1.793E+01
3000-8000
0.6
1.1
2.5
~Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results,"
(Certificate continued on reverse side)
Mixed Aloha Certificate, Rev 1 9/28/2009
VI
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 9135S
Page 38 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30315
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.48 mm thick
stainless steel disk.
CAUTION; Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps), Store in the container provided when
not in use,
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, OA Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 39 of 551
-------
Reagent
82240-334 00001
Page 40 of 551
-------
¦J Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82240-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No,; 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector, Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziogler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4,18, Revision 1, February, 1979, and compliance with ANSI N42.22-1996,
"Traceability of Radioactive Sources to WIST," EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste, 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352»8677
Fax 404*352*2837
www.analytksinc.com
Reference Date;
8-Jun-2010
12:00 PM EST
Energy Range
Half-Life,
Uncertainty* Type (%)
Isotope
Activity (Bq)
(keV)
years
%
Ub
U
Th-230
6.3Q4E+00
4420-4800
7.540E+04
0,9
1.1
2.8
Pu-239
7.163E+00
4950-8240
2.410E+04
0.8
1.1
2.7
Am-241
8.298E+00
8280=6600,
4.326E+02
0.8
1.1
2.7
Total
Activity
2.182E+01
3000-8000
O.S
1.1
2.4
^Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 41 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.4S mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps), Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taslcaev, OA Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 42 of 551
-------
Reagent
82241-334 00001
Page 43 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82241-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.; 23SS182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 404*352*2837
www.arialytlcslnc.com
Reference Date: 8-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%}
Isotope
Activity (Bq)
fleeV)
years
UA
%
u
Th-230
6.629E+00
4420-4800
7.S40E+04
0.8
LI
2,7
Pu-239
6.797E+00
4950-8240
2.410E+04
0.8
1.1
2.7
Am-241
6.638E+00
6280,5600
4.326E+02
0.8
1.1
2.7
Total
Activity 2.011E+01 3000-8000 0.4 1.1 2.3
^Uncertainty; U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 91 355
Page 44 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 3031 £
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.4S mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, OA Manager Alternate
#CA
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 45 of 551
-------
Reagent
82242-334 00001
Page 46 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82242-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St, Louis
P.O. No.: 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 404-352-2837
www.analyticsinc.com
Reference Date: 8-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope Activity (Bq) (keV) years ufl uB U
Th-230
6.583E+00
4420-4800
7.540E+04
0.9
1.1
2.8
Pu-239
6.414E+00
49S0-B240
2.410E+04
0.9
1.1
2.8
Am=241
7.145E+00
5280-5600
4.326E+02
0.9
1.1
2.8
Total
Activity
2.018E+01
3000-8000
0.6
1.1
2.8
^Uncertainty: U - Relative expanded uncertainty, k — 2, See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.45 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source {i.e., use Teflon coated forceps), Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
Date: 0(f ~ 2.^ - "2 O f X^)
cal/o^
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 48 of 551
Page 2 of 2
-------
Reagent
82243-334 00001
Page 49 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82243-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No,; 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.18, Revision 1, February, 1979, and compliance with ANSI N42.22-1998,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste, 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352*8677
Fax 404*352*2837
www.analyticsinc.com
Reference Date: 9-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope Activity (Bq) (keV) years uB U
Th-230
5.856E+00
4420-4800
7.540E+04
0.8
i.i
2.7
Pu-239
8.979E+00
4950-5240
2.410E+04
0.8
i.i
2.7
Am-241
6.390E+00
5280=5600
4.326E+02
0.8
i.i
2.7
Total
Activity
1.827E+01
3000-8000
CO
d
i.i
2.3
^Uncertainty: U - Relative expanded uncertainty, k = 2, See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results,"
(Certificate continued on reverse side)
2493? Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments;
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.45 mm thick
stainless steel disk.
CAUTION": Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
QA Approved:
&eCAL/a^
Mixed Alpha Certificate, Rev 1 9/28/2009
°*. ygScrrrC/ ^
Page 51 of 551
Page 2 of 2
-------
Reagent
82244-334 00001
Page 52 of 551
-------
•Jf Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82244-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.; 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352«8677
Fax 404*352-2837
www.analytlcslnc.conn
Reference Date: 9-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope
Activity (Bq)
(keV)
years
%
u„
U
Th-230
7.352E+00
4420-4800
7.640E+04
0.8
1.1
2.7
Pu-239
6.717E+00
4950-5240
2.410E+04
0.9
1.1
2.8
Amr241
6.897E+00
5280-5600.
4.326E+02
0.9
1.1
2.8
Total
Activity 2.101E+01 3000-8000 0,6 1.1 2.5
~Uncertainty: U - Relative expanded uncertainty, k= 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 AvenueTibbltts Valencia, California 91355
Page 53 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments;
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.45 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by;
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, QA Manager Alternate
0frCAUs^
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 54 of 551
-------
Reagent
82246-334 00001
Page 55 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82246-334
24.1 mm Diameter x 0,68 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.: 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk, Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.16, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceability of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352»8677
Fax 404-352-2837
www.analyticsirsc.com
Reference Date: 9-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope Activity (Bq) (keV) years «a ug U
Th-230
5.S70E+00
4420-4800
7.540E+04
1.0
1.1
3.0
Pu-239
5.353E+00
4980-8240
2.410E+04
1.0
1.1
3.0
Am-241
6.002E+00 -
8280=6600
4.326E+02
1.0
1,1
3.0
Total
Activity
1.696E+Q1
3000-8000
0.7
1.1
2.6
Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
/
Page 1 of 2
Corporate Office
24937 Avenue Tlbbitts Valencia, California 91355
Page 56 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30315
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.45 mm thick
stainless steel disk.
CAUTION; Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopist
OA Approved:
E. A. Taskaev, OA Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 57 of 551
-------
Reagent
82247-334 00001
Page 58 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
82247-334
24.1 mm Diameter x 0.65 mm Thick Stainless Steel Disk
Customer: Test America/St. Louis
P.O. No.; 2355182, Item 1
This standard radionuclide source was prepared by electrodeposition onto a stainless steel disk. Total
alpha activity was determined with a ZnS scintillation detector. Radionuclide activities and impurities
were calculated from the total activity and the fraction of activity for each radionuclide determined by
alpha spectroscopy. Eckert & Ziegler Analytics (EZA) maintains traceabiiity to the National Institute of
Standards and Technology through a Measurements Assurance Program as described in USNRC
Regulatory Guide 4.15, Revision 1, February, 1979, and compliance with ANSI N42.22-1995,
"Traceabiiity of Radioactive Sources to NIST." EZA is accredited by the Health Physics Society (HPS) for
the production of NIST-traceable sources, and this source was produced in accordance with the HPS
accreditation requirements. Customers may report any concerns with the accreditation program to the
HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352-8677
Fax 404«352«2837
www.analyttcslric.com
Reference Date: 10-Jun-2010 12:00 PM EST
Energy Range Half-Life, Uncertainty* Type (%)
Isotope Activity (Bq) (keV) years »a "b U
Th-230
6.251E+00
4420-4800
7.540E+04
0.9
1.1
2.8
Pu-239
S.746E+00
49S0-S240
2.410E+04
0.9
1.1
2.8
- Am-241
6.291E+00
5280-5600
4.326E+02
0.9
1.1
2.8
Total
Activity
1.832E+01
3000-8000
0.6
1.1
2,0
Uncertainty: U - Relative expanded uncertainty, k — 2, See NIST Technical Note 1297, "Guidelines for Evaluating and
Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 1 of 2
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 59 of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Comments:
Diameter of active area: 19 mm. Disk mounted on customer supplied disk 31.8 mm diameter x 0.48 mm thick
stainless steel disk.
CAUTION: Active material deposited on the unmarked surface. Handle carefully to prevent scratching or
damaging the active surface of this source (i.e., use Teflon coated forceps). Store in the container provided when
not in use.
Source Calibrated by:
A. Chen, Spectroscopy
OA Approved:
E. A. Taskaev, Oil Manager Alternate
Mixed Alpha Certificate, Rev 1 9/28/2009
Page 2 of 2
Page 60 of 551
-------
Reagent
Gamma Ampuole 00001
Page 61 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 4Q4»352"2837
www.analyticsrnc.com
79670-334
5 mL Liquid in Flame Sealed Vial
Customer: TestAmerica St, Louis
P.O. No.: 230392B, Item 1
Calibration Date: 01 -Apr-2009
12:00 EST
Grams of Master Source: 0.028371
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains
traceability to the National Institute of Standards and Technology through a Measurements Assurance
Program as described in USNRC Regulatory Guide 4,15, Revision 1, February, 1979, and compliance
with ANSI N42.22-1995, "Traceability of Radioactive Sources to HIST."
Master Uncertainty, %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
•^ps/gram
tps
u*
%
U
Method
Am-241
S9.8
157860
3.390E+03
0.1
0.9
1.8
4rr LS
Cd-109
88.0
462.60
1.691E+05
4.798E+03
0.4
1.7
3.5
HPGe
Co-57
122.1
271.79
8.904E+04
2.526E+03
0.8
1.3
2.8
HPGe
Ce-139
168.9
137.6
1.256E+0S
3.S63E+03
0.4
1.1
2.3
HPGe
Hg-203
279.2
46.61
2.788E+0S
7.910E+03
0.3
1.1
2.3
HPGe
Sn-113
391.7
118.1
1.72SE+0S
4.894E+03
0.5
1.1
2.4
HPGe
Cs-137
661.7
10983
1.120E+0B
3.178E+03
0.7
1.2
2.8
HPGe
Y-88
898.0
106.6
4.205E+08
1.193E+04
0.8
1.1
2.7
HPGe
Co-60
1173.2
1925.4
2.184E+0S
6.196E+03
0.7
1.1
2.6
HPGe
Co-60
1332.6
1925.4
2.185E+0S
6.199E+03
0.7
1.1
2.6
HPGe
Y-88
1836.1
106.6
4.444E+0S
1.261E+04
0,7
1.1
2.6
HPGe
* Master Source refers to Analytics' 8-isotope.mixture which is calibrated quarterly.
Calibration Methods; 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer,
IC - Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297,
"Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results,"
Comments:
8.31740 grams 4M HC1 solution with approximately 30 microg/g each of Cd, Co, Ce, Hg, Sn, Cs, and Y carriers.
This standard will expire one year after the calibration date.
Source Prepared by:
W, Mao, Radiochemist
OA Approved: Date: jT-/3ngf
D, M. Montgoirfery, OA Manager
End of Certificate
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 62"of551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Reagent
Source A 00001
Page 63 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 4Q4»352"2837
www.analyticsrnc.com
79670-334
5 mL Liquid in Flame Sealed Vial
Customer: TestAmerica St, Louis
P.O. No.: 230392B, Item 1
Calibration Date: 01 -Apr-2009
12:00 EST
Grams of Master Source: 0.028371
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains
traceability to the National Institute of Standards and Technology through a Measurements Assurance
Program as described in USNRC Regulatory Guide 4,15, Revision 1, February, 1979, and compliance
with ANSI N42.22-1995, "Traceability of Radioactive Sources to HIST."
Master Uncertainty, %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
•^ps/gram
tps
u*
%
U
Method
Am-241
S9.8
157860
3.390E+03
0.1
0.9
1.8
4rr LS
Cd-109
88.0
462.60
1.691E+05
4.798E+03
0.4
1.7
3.5
HPGe
Co-57
122.1
271.79
8.904E+04
2.526E+03
0.8
1.3
2.8
HPGe
Ce-139
168.9
137.6
1.256E+0S
3.S63E+03
0.4
1.1
2.3
HPGe
Hg-203
279.2
46.61
2.788E+0S
7.910E+03
0.3
1.1
2.3
HPGe
Sn-113
391.7
118.1
1.72SE+0S
4.894E+03
0.5
1.1
2.4
HPGe
Cs-137
661.7
10983
1.120E+0B
3.178E+03
0.7
1.2
2.8
HPGe
Y-88
898.0
106.6
4.205E+0S
1.193E+04
0.8
1.1
2.7
HPGe
Co-60
1173.2
1925.4
2.184E+0S
6.196E+03
0.7
1.1
2.6
HPGe
Co-60
1332.6
1925.4
2.185E+05
6.199E+03
0.7
1.1
2.6
HPGe
Y-88
1836.1
106.6
4.444E+0S
1.261E+04
0,7
1.1
2.6
HPGe
* Master Source refers to Analytics' 8-isotope.mixture which is calibrated quarterly.
Calibration Methods; 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer,
IC - Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297,
"Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results,"
Comments:
8.31740 grams 4M HC1 solution with approximately 30 microg/g each of Cd, Co, Ce, Hg, Sn, Cs, and Y carriers.
This standard will expire one year after the calibration date.
Source Prepared by:
W, Mao, Radiochemist
OA Approved: Date: jT-/3ngf
D, M. Montgoirfery, OA Manager
End of Certificate
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 64"of551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Reagent
Source C 00001
Page 65 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 4Q4»352"2837
www.analyticsrnc.com
79670-334
5 mL Liquid in Flame Sealed Vial
Customer: TestAmerica St, Louis
P.O. No.: 230392B, Item 1
Calibration Date: 01 -Apr-2009
12:00 EST
Grams of Master Source: 0.028371
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains
traceability to the National Institute of Standards and Technology through a Measurements Assurance
Program as described in USNRC Regulatory Guide 4,15, Revision 1, February, 1979, and compliance
with ANSI N42.22-1995, "Traceability of Radioactive Sources to HIST."
Master Uncertainty, %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
•^ps/gram
tps
u*
%
U
Method
Am-241
S9.8
157860
3.390E+03
0.1
0.9
1.8
4rr LS
Cd-109
88.0
462.60
1.691E+05
4.798E+03
0.4
1.7
3.5
HPGe
Co-57
122.1
271.79
8.904E+04
2.526E+03
0.8
1.3
2.8
HPGe
Ce-139
168.9
137.6
1.256E+0S
3.S63E+03
0.4
1.1
2.3
HPGe
Hg-203
279.2
46.61
2.788E+0S
7.910E+03
0.3
1.1
2.3
HPGe
Sn-113
391.7
118.1
1.72SE+0S
4.894E+03
0.5
1.1
2.4
HPGe
Cs-137
661.7
10983
1.120E+0B
3.178E+03
0.7
1.2
2.8
HPGe
Y-88
898.0
106.6
4.205E+08
1.193E+04
0.8
1.1
2.7
HPGe
Co-60
1173.2
1925.4
2.184E+0S
6.196E+03
0.7
1.1
2.6
HPGe
Co-60
1332.6
1925.4
2.185E+05
6.199E+03
0.7
1.1
2.6
HPGe
Y-88
1836.1
106.6
4.444E+0S
1.261E+04
0,7
1.1
2.6
HPGe
* Master Source refers to Analytics' 8-isotope.mixture which is calibrated quarterly.
Calibration Methods; 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer,
IC - Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297,
"Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results,"
Comments:
8.31740 grams 4M HC1 solution with approximately 30 microg/g each of Cd, Co, Ce, Hg, Sn, Cs, and Y carriers.
This standard will expire one year after the calibration date.
Source Prepared by:
W, Mao, Radiochemist
OA Approved: Date: jT-/3ngf
D, M. Montgoirfery, OA Manager
End of Certificate
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 66"of551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Reagent
Source D 00001
Page 67 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 4Q4»352"2837
www.analyticsrnc.com
79670-334
5 mL Liquid in Flame Sealed Vial
Customer: TestAmerica St, Louis
P.O. No.: 230392B, Item 1
Calibration Date: 01 -Apr-2009
12:00 EST
Grams of Master Source: 0.028371
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given. Analytics maintains
traceability to the National Institute of Standards and Technology through a Measurements Assurance
Program as described in USNRC Regulatory Guide 4,15, Revision 1, February, 1979, and compliance
with ANSI N42.22-1995, "Traceability of Radioactive Sources to HIST."
Master Uncertainty, %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
•^ps/gram
tps
u*
%
U
Method
Am-241
S9.8
157860
3.390E+03
0.1
0.9
1.8
4rr LS
Cd-109
88.0
462.60
1.691E+05
4.798E+03
0.4
1.7
3.5
HPGe
Co-57
122.1
271.79
8.904E+04
2.526E+03
0.8
1.3
2.8
HPGe
Ce-139
168.9
137.6
1.256E+0S
3.S63E+03
0.4
1.1
2.3
HPGe
Hg-203
279.2
46.61
2.788E+0S
7.910E+03
0.3
1.1
2.3
HPGe
Sn-113
391.7
118.1
1.72SE+0S
4.894E+03
0.5
1.1
2.4
HPGe
Cs-137
661.7
10983
1.120E+0B
3.178E+03
0.7
1.2
2.8
HPGe
Y-88
898.0
106.6
4.205E+08
1.193E+04
0.8
1.1
2.7
HPGe
Co-60
1173.2
1925.4
2.184E+0S
6.196E+03
0.7
1.1
2.6
HPGe
Co-60
1332.6
1925.4
2.185E+05
6.199E+03
0.7
1.1
2.6
HPGe
Y-88
1836.1
106.6
4.444E+0S
1.261E+04
0,7
1.1
2.6
HPGe
* Master Source refers to Analytics' 8-isotope.mixture which is calibrated quarterly.
Calibration Methods; 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer,
IC - Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297,
"Guidelines for Evaluating and Expressing the Uncertainty of NIST Measurement Results,"
Comments:
8.31740 grams 4M HC1 solution with approximately 30 microg/g each of Cd, Co, Ce, Hg, Sn, Cs, and Y carriers.
This standard will expire one year after the calibration date.
Source Prepared by:
W, Mao, Radiochemist
OA Approved: Date: jT-/3ngf
D, M. Montgoirfery, OA Manager
End of Certificate
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Page 68"of 551
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Reagent
Th-229 00016
Page 69 of 551
-------
Eckert & Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404,352,8677
Fax 404-352-2837
www.analyticsinc.com
97790
Th-229 5 mL Liquid in Flame Sealed Vial
Customer:
P.O. No.:
TestAmerica - St. Louis
2573570, Item 1 Product Code: 8229
430569
ID: Th-229_00016
Exp:08/06/64 PrpdtSCB Opn:08/20/14
Th-229 Ampoule
This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert
& Ziegler Analytics, The master solution was calibrated by liquid scintillation counting. Radionuclide
calibration and purity were checked by germanium gamma-ray spectrometry, liquid scintillation counting,
and/or alpha spectrometry, as applicable. The nuclear decay rate and reference date for this source are
given below. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and
Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4.15,
Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST."
EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this
source was produced in accordance with the HPS accreditation requirements. Customers may report any
concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean,
VA 22101.
Isotope
Half-Life,
Days
Activity
(Bq)
Uncertainty* , %
Type
uA uB u
Reference Date
(12:00 PM EST)
Th-229
2.681E+06
3.761E+03
0.5
1.5 3.1
08/06/2014
Uncertainty: U - Relative expanded uncertainty, k = 2, See NIST Technical Note 1297, "Guidelines for Evaluating and Expressing
the Uncertainty of NIST Measurement Results."
Comments:
Impurities: a-impurities: Th-228 2.83E-01 Bq, Th-230 2.33E+01 Bq, Th-232 1.51E0 Bq; y-impurities (other than
decay products)<0.1%.
5.08156 g 0.5M HN03 solution. Carrier free.
Source Prepared by:
Z. Dimitrova, Radiochemist
QC Approved:
A. Chen, Spectroscopist
Date: Ofc>
24937 Avenue Tibbitts Valencia, California 91355 1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
°'c%
l U.S. DEPARTMENT OF COMMERCE
National Institute of Standards & Technology
Gaithersburg, MD 20899
^4T"ES 0^ ^
Certificate of Participation
Eckert & Ziegler Analytics
Atlanta, Georgia
is a participant for the period January 1,2014, through
December 31,2014, in a radioactivity measurements assurance
program conducted by the National Institute of Standards and
Technology, in cooperation with NRMAP Incorporated.
Continued participation is evidenced by dated Reports of
Traceability issued for particular radionuclides, which indicate
the deviation of the participant's reported value from that
measured by the National Institute of Standards and
Technology. The significance of these Reports is addressed
below.*
For the Director,
Michael P. Unterweger, Leader
Radioactivity Group
Physical Measurement Laboratory
* As guidance for the proper use of Reports of Traceability, it should be emphasized that the National Institute of
Standards and Technology is concerned only with fostering good measurements capability and consistency with the
national measurements system. The assurance of the proper application of that capability to the ultimate consumer
products is the responsibility of each manufacturer of these products and of the Federal regulatory agencies.
A continuing traceability program in radioactivity demonstrates, to the degree established by the periodic assays of
calibrated radioactivity samples, a continuing competence to maintain the methods and standards necessary for
accurate measurement. Such a program cannot, however, endorse each and every measurement nor the final
product, any more than a spot check can vouch for every unchecked item. Care should be taken, therefore, not to
imply such endorsement. The proper use of this Report is governed by section 200.114 of Title 15 of the Code of
Federal Regulations. These regulations may be met if Reports are quoted only in their entirety. Excerpts out of
context may be misleading.
Page 71 of 551
-------
1380 Seaboard Industrial Boulevard
Atlanta, Georgia 30318 USA
Phone (404) 352-8677 • Fax (404) 352-2837
Email: analvtics@ezaq.com (Tax EIN: 58-1406082)
Recommended Procedure for Opening the Flame Sealed Vial
• Eckert&Ziegler
Analytics
1) If the solution is to be diluted, it is recommended that the diluting
solution have a composition comparable to that of the standard.
2) Wear eye protection, gloves, and protective clothing and work over
a tray with absorbent paper in it. Work in a fume hood.
3) Shake the vial to wet the entire inside surface of the vial. Return
the vial to the upright position.
4) Check that all of the liquid has drained out of the neck of the vial.
If necessary, gently tap the neck to speed the process.
5) The Wheaton vials we use are pre-scored.
6) Lightly wet the scored line. This reduces the crack propagation
velocity and makes for a cleaner break.
7) Hold the vial upright and wrap with soft tissue, such as Chem
Wipes, around the tip of the vial and secure with tape (see
picture). Snap off the top of the vial by pressing the pre-scored
part of the neck away towards you while pulling the tip of the vial
away from you.
8) Transfer the solution from the vial using a pycnometer or pipet
with a dispenser handle. NEVER PIPETTE BY MOUTH.
9) Seal any unused solution in a flame sealed glass vial, if possible,
to minimize the evaporation loss.
K:\DATA\ANALYTTC\DOCS\QA\Recommended Procedure for Opening the Flame Sealed Vial 10-22-09.doc
Page 72 of 551
-------
Reagent
Th-229 00020
Page 73 of 551
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
Th-229
00020 |
Radionuclide:
True Value =
66.223 I
DPM/L org
| Th-229 |
Date Analyzed:
8/5/2015|
Replicates
#1
66.657
DPM/L
or
g
#2
65.249
DPM/L
or
g
#3
68.757
DPM/L
or
g
Mean = 66.88767
1 sigma = 1.765339 1.96 sigma = 3.460064
True Value minus 5% = 62.91185 (True Value - 5%)
True Value plus 5% = 69.53415 (True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value? Yes (Acceptance Criteria)
Precision:
1.96 sigma Value Within 10% of Mean Value? Yes (Acceptance Criteria)
Standard Reverification Acceptable? Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date: Rachel T. Mueller 8/11/2015
SOP Reference: STL-QA-0002, Current Revision
Page 74 of 551
-------
Alpha-Spectroscopy
Analysis Report
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 1
SampleType: Sample
Sample Collection Date:
Batch Name: Th-229_00020
AnalysisID: 650912
Tracer Name: Th-230_00025
Tracer Activity: 44.56 DPM/mL x (Vol,)0.30 mL = 13.37 DPM
Tracer Ref. Date: 8/8/2013 12:00:04PM
_______— —— Acquisition
Detector: AV115
Serial Number: 49-037E4
Acquisition Start Date: 8/5/2015 12:04:12PM
Live Time: 960.00 min.
Real Time: 960.02 min.
Background Date: 7/17/2015 12:56:42PM
Background Info: Sample: ICB;AV115; Det: AV115; Spectrum #1;
Jul-17-2015 12:56
Sample
Batch
Tracer
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
5:31:53PM 8/11/2015
Spectrum #1 Analysis #1
Sample Volume: O.IOOOmL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
Tracer Nuclide: Th-230
Tracer Recovery: 99.76%
Calibration Name: IC-9817;AV115-20150603
Calibration Date: 6/4/2015 1:31:22AM
Gain = 7.4575 keV/Ch
r- ~ , Offset = 3,366.95 keV
Energy Cal:
Quadratic = 0.0000 keV / Ch
Efficiency: 25.44% +/- 0.31% TPU(2 sigma)
520
480
440
400
360
| 320
" 280
240
200
160
120
80
40
0
3374 3674 3974 4274 4574 4874 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (ReV)
General Analysis — —
Analysis Method: Absolute ROI Analysis, Set Name = Th-230_Tracer Nuclide Library: Thorium
Decay Correction: 8/5/2015 12:01:32PM MDA Source: Background
MDA Constants: Ka = 1.65 , K|3 = 1.65
— Nuclide Summary (ROI) ~
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity
Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072,0
10.7
100.2
2
3.4586
-1.46
-0.060
DPM/mL
Th-230
4688.0
4,687.5
0.5
4448.3
4746.6
31.9
99.7
3250
2.0000
3248.00
133.370
DPM/mL
Th-229
4848.0
4,845.3
2.7
4746.6
5119.5
75.3
99.8
1624
3.0000
1621.00
66.657
DPM/mL
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
11.0
99.8
28
3.0000
25.15
1.035
DPM/mL
Th-232
I' f I
Th-230
Th-229
! %
JBk
m,±
Th-228
1—i—r
J\ s
1#
i I"" i1 "V i1—r
Page 75 of 551
-------
Alpha-Spectroscopy
Analysis Report
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 2
SampleType: Sample
Sample Collection Date:
Batch Name: Th-229_00020
AnalysisID: 650913
Sample
Batch
Tracer
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
5:33:35PM 8/11/2015
Spectrum #1 Analysis #1
Sample Volume : 0.1000mL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
Tracer Name: Th-230_00025
Tracer Activity: 44.56 DPM/mL x (Vol.)0.30 mL = 13.37 DPM
Tracer Ref. Date: 8/8/2013 12:00:04PM
— —— — ¦— Acquisition
Detector: AV116
Serial Number: 49-034G1
Acquisition Start Date: 8/5/2015 12:04:13PM
Live Time: 960.00 min.
Real Time: 960.02 min.
Background Date: 7/17/2015 12:56:44PM
Background Info: Sample: ICB;AV116; Det: AV116; Spectrum #1;
Jul-17-2015 12:56
Tracer Nuclide: Th-230
Tracer Recovery: 102.76%
Calibration Name: IC-9884;AV116-20150603
Calibration Date: 6/4/2015 1:31:31AM
Gain = 7.4575 keV/Ch
~ , Offset = 3,366.95 keV
Enerqy Cal:
Quadratic = 0.0000 keV / Ch
Efficiency: 24.86% +/- 0.36% TPU(2 sigma)
520
480
440 :
400
380
320
280 ;
240 ;
200 :
160
120 :
80 ;
40 :
0 -
Th-23:
Th-230
JL
Th-229
y
I"""?—1—*T-*r
3374 3674 3974 4274 4574 4874 5174 5474 5774 6074 6374 6674
Th-228
r "i "v
tap
if—t*
1±
I
i i r
6974 7274
7574
Energy (keV)
General Analysis •
Analysis Method: Absolute ROI Analysis, Set Name = Th-230_Tracer Nuclide Library: Thorium
Decay Correction: 8/5/2015 12:01:32PM MDA Source: Background
MDA Constants: Ka=1.65,K(3= 1.65
Nuclide Summary (ROI)'
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity
Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
44.6
100.2
4
1.0000
2.54
0.103
DPM/mL
Th-230
4688.0
4,687.5
0.5
4448.3
4731.7
40.1
99.7
3272
3.0000
3269.00
137.388
DPM/mL
Th-229
4848.0
4,845,3
2.7
4731.7
5119.5
69.1
99.8
1599
2.0000
1597.00
65.249
DPM/mL
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
.3
99.8
24
4.0000
19.94
0.815
DPM/mL
Page 76 of 551
-------
Alpha-Spectroscopy
Analysis Report
THE LEADER IN ENVIRONMENTAL TESTING
—< — > ¦ Sample
Sample Name: Verification 3
SampleType: Sample
Sample Collection Date: Batch
Batch Name: Th-229_00020
AnalysisID: 650914
____________ , : T^CSr
Tracer Name: Th-230_00025
Tracer Activity: 44.56 DPM/mL x (Vol.)0.30 mL = 13.37 DPM
Tracer Ref. Date: 8/8/2013 12:00:04PM
—:— —— Acquisition
Detector: AV117
Serial Number: 49-037X4
Acquisition Start Date: 8/5/2015 12:04:18PM
Live Time: 960.00 min.
Real Time: 960,02 min.
Background Date: 7/19/2015 5:26:41PM
Background Info: Sample: ICB;AV117; Det: AV117; Spectrum #1;
J ul-19-2015 17:26
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
5:34:26PM 8/11/2015
Spectrum #1 Analysis #1
Sample Volume : 0.1000mL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
Tracer Nuclide: Th-230
Tracer Recovery: 99.73%
Calibration Name: IC-9885;AV117-20150603
Calibration Date: 6/4/2015 1:31:41AM
Gain = 7.4575 keV/Ch
c ~ , Offset = 3,366.95 keV
Energy Cal:
Quadratic = 0.0000 keV / Ch
Efficiency: 24.89% +/- 0.37% TPU(2 sigma)
420
390
36G
330
300
270
g 240
21 0
1 80
1 50
120
90
GO
30
0
3374 3674 3974 4274 4574 4374 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV)
—_____ — — General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th-230_Tracer Nuclide Library: Thorium
Decay Correction: 8/5/2015 12:01:32PM MDA Source: Background
MDA Constants: Ka=1.65,K|3= 1.65
Nuclide Summary (ROI) '
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity
Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
10.2
100.2
7
1.0000
6.00
0.251
DPM/mL
Th-230
4688.0
4,687.5
0.5
4448.3
4731.7
46.3
99.7
3176
0.0000
3176.00
133.339
DPM/mL
Th-229
4848.0
4,845.3
2.7
4731.7
5119.5
78.5
99.8
1635
0.0000
1635.00
68.757
DPM/mL
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
258.3
99.8
16
2.0866
14.09
0.593
DPM/mL
Th-232
V-n-^—i" i—r
Th-230
Th-229
J %
Th-228
L ..
n—i
J\
tt-t
#
."U
I I I
Page 77 of 551
-------
Page 78 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
II IIIIIIII II
2 2 9
Reagent ID: Th-229_00020
Description:
No. of Bottles:
Storage Location:
Reagent Volume:
Creation Date:
Open Date:
Container(s):
Comment:
Th-229 Tracer
1
RAD Actinide STDs
500.000 mL
07/16/2015
684059
Expiration Date:
Laboratory:
Prepared By:
Solvent:
Solvent Lot:
12/24/2015
TestAmerica St, Louis
Bernsen, Sarah C
0.1 M HN03
n/a
Reagent Analyte Information
Analyte
Source ID
Source
Exp. Date
Source
Cone.
Source Cone.
Units
Final
Cone.
Final
Cone. Units
At-217
Th-229
Th-229_00017
Th-229_0Q017
08/06/2064 2240.98600
08/06/2064 2240.98600
dpm/mL 67.22958
dpm/mL 67.22958
dpm/mL
dpm/mL
Source Reagents
Vendor Vendor Volume Volum<
Reagent Description Type Expiration Vendor Lot # Cat Lot # Used Units
Th-229_00017 Th-229 Parent 08/06/64 15.00000 mL
07/16/2015 14:21
Page 79 of 551
Page 1 of 1
-------
Reagent
TRM-2 00001
Page 80 of 551
-------
Perry, Doug E
From; Salmi, Douglas R
Sent: March 20, 2000 10:48 AM
To: Perry, Doug E; Puissant, Pamela M
Subject: FW; SRMs for radiochemistry LCSs
Pam, Doug
FYl
—Original Message—
From: Minteer@aol.com [mailto:Minteer@aoI.coml
Sent: March 20,2000 10:36 AM
To: drsalmt@sandia.gov
Cc: dboume@doeal.gov; GLDechant@aol.com; Grandailb@quanterra.com
Subject: SRMs for radiochemistry LCSs
Doug:
As we discussed by telephone, please send approximately 500 grams each of
FEM-1, TRM-2, and NBHD to STL St, Louis. These are to be used by STL as
laboratory control samples. As with our other laboratories, STL will be
asked to provide summaries of the data obtained in quarterly progress
reports. This is not to assess their proficiency, but rather to help us
develop interlaboratory acceptance criteria. The known values (given below)
for PEM and TRM are good because the samples are well characterized. The
known values for NBHD result from a single analysis and hence should be taken
as estimates. AH the values below are in pCi/g,
PEM-1:
Parameter Result Std. Dev.
Pu-238 8.03 0.37
Pu-239 41.0 3.0
Am-241 32.5 1.1
Cs-137 73,5 0.9
U-2345.99 "0,2
U-235 0,27 0.04
U-238 18.1 0.5
» ¦
TRM-2
Parameter "Result Uncertainty
U-238 6,0 +/- 4.0
U-234 6.2 +/-4.0
Th-230 24.5 +/- 0.6
Ra-226 25.4 +/- 0.9
Pb-210 22.1 +/- 1.2
NBHD
Parameter Result Uncertainty
Am-241 1,47 +/- 0.28
Ra-226 67.3 +/. 5.5
U-234 174 none available
U-235 8.7 ¦
U-238 212 "
Cs-137 52.1 +/- 4 6
Pb-210 78.3 +/- 2.4
Pu-239/40 4.7 +/- 0.63
Pu-238 0.3 +/- 0.11
Th-230 83.4 +/- 6,5
1
Page 81 of 551
-------
Reagent
Tuna Can LCS 00005
Page 82 of 551
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
Tuna Can LCS 00005
(776670) |
Radionuclide:
True Value =
30.08
pCi/g
\ Gamma LCS Cs-1371
Date Analyzed:
10/25/2015
Replicates
#1
30
pCi/g
#2
29.42
pCi/g
#3
28.95
pCi/g
Mean =
29.45667
sigma =
0.525959
True Value minus 5% =
True Value plus 5% =
1.96 sigma = 1.030881
28.576
31.584
(True Value - 5%)
(True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value?
Precision:
1.96 sigma Value Within 10% of Mean Value?
Standard Reverification Acceptable?
Yes (Acceptance Criteria)
Yes (Acceptance Criteria)
Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date:
Jody Watson 10/29/15
SOP Reference: STL-QA-0002, Current Revision
Tuna Can LCS_00005 (776670)Cs-137 10/29/2015
Page 83 of 551
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
Tuna Can LCS_00005 (776670) |
Radionuclide:
True Value =
97.23
pCi/g
| Gamma LCS Am-2411
Date Analyzed:
10/25/2015
Replicates
#1
96.82
pCi/g
#2
97.14
pCi/g
#3
97.26
pCi/g
Mean =
97.07333
sigma =
0.22745
True Value minus 5% =
True Value plus 5% =
1.96 sigma = 0.445801
92.3685
102.0915
(True Value - 5%)
(True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value?
Precision:
1.96 sigma Value Within 10% of Mean Value?
Standard Reverification Acceptable?
Yes (Acceptance Criteria)
Yes (Acceptance Criteria)
Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date:
Jody Watson 10/29/15
SOP Reference: STL-QA-0002, Current Revision
Tuna Can LCS_00005 (776670)Am-241
Page 84 of 551
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
Tuna Can LCS_00005 (776670) T Radionuclide:
True Value
18.6
pCi/g 1 Gamma LCS Co-60
Date Analyzed:
10/25/2015
Replicates
#1
17.74
pCi/g
#2
18.7
pCi/g
#3
17.74
pCi/g
Mean =
18.06
1 sigma = 0.554256
True Value minus 5% =
True Value plus 5% =
1.96 sigma = 1.086342
17.67
19.53
(True Value - 5%)
(True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value?
Precision:
1.96 sigma Value Within 10% of Mean Value?
Standard Reverification Acceptable?
Yes (Acceptance Criteria)
Yes (Acceptance Criteria)
Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date:
Jody Watson 10/29/15
SOP Reference: STL-QA-0002, Current Revision
Tuna Can LCS_00005 (776670)Co-60 10/29/2015
Page 85 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Analysis Report for Gamma Spectroscopy
Batch: 217910 Operator:
SampID
LCS 160-217910-2-
WRKNO
LCS
Aliquot
341.90g
Sigma Instrument Detector
1.00 GammaVision GV01
CountDatcTime
10/25/15 16:00
CountDuration
30
Analvte
Cnmndii
Activitv
TotalUnc
CountUnc
MDA MLCC
Act/MDA
AC-228
11136
6.771 E-001pCi/g
2.800E-001
2.778E-001
1.003E+000 4.849E-001
0.68
AG-108M
10982
-6.779E-003pCi/g
1.235E-002
1.235E-002
2.560E-001 1.249E-001
-0.03
AG-110M
10973
8.663E-003pCi/g
1.112E-001
1.112E-001
3.788E-001 1.830E-001
0.02
AM-241
10818
9.682E+001 pCi/g
5.076E+000
7.243E-001
1.019E+000 5.045E-001
95.00
BA-133
10469
1.494E-002pCi/g
8.071 E-002
8.071 E-002
2.729E-001 1.325E-001
0.05
BA-140
10463
1.374E-001 pCi/g
2.240E-001
2.238E-001
7.542E-001 3.638E-001
0.18
BE-7
10435
O.OOOE+OOOpCI/g
3.925E-001
3.925E-001
2.266E+000 1.104E+000
0.00
BI-207
10195
-2.705E-003pCi/g
5.167E-002
5.167E-002
1.770E-001 8.502E-002
-0.02
BI-210M
10173
8.461 E-002pCi/g
9.172E-002
9.158E-002
3.052E-001 1.486E-001
0.28
BI-212
10160
5.691 E-002pCi/g
6.570E-001
6.570E-001
2.266E+000 1.080E+000
0.03
BI-214
10154
5.973E-001 pCi/g
1.858E-001
1.832E-001
3,511 E-001 1.678E-001
1.70
CD-109
9254
9.357E+000pCi/g
3.288E+000
3.246E+000
3.163E+000 1.546E+000
2.96
CD-113NI
17462
-1.418E+002pCi/g
7.297E+002
7.296E+002
2.462E+003 1.198E+003
-0.06
CE-139
9241
-3.471 E-002pCi/g
4.795E-002
4.783E-002
1.596E-001 7.801 E-002
-0.22
CE-141
9235
1.101E-001 pCi/g
6.681 E-002
6.657E-002
2.193E-001 1.068E-001
0.50
CE-144
9221
-1.962E-001 pCi/g
3.271 E-001
3.269E-001
1.092E+000 5.343E-001
-0.18
CF-249
9215
-9.471 E-002pCi/g
9.312E-002
9.299E-002
3.094E-001 1.508E-001
-0.31
CF-251
13690
9.783E-002pCi/g
2.187E-001
2.185E-001
7.329E-001 3.576E-001
0.13
CO-56
8704
-4.255E-002pCi/g
7.343E-002
7.340E-002
2.477E-001 1.193E-001
-0,17
CO-57
13694
3.299E-002pCi/g
4.336E-002
4.333E-002
1.444E-001 7.069E-002
0.23
CO-58
8698
-4.234E-003pCi/g
6.516E-002
6.516E-002
2.232E-001 1.072E-001
-0.02
CO-60
8692
1.774E+001 pCI/g
9.138E-001
2.049E-001
6.716E-002 2.728E-002
264.12
CR-51
8604
3.076E-001 pCi/g
4.401E-001
4.398E-001
1.475E+000 7.149E-001
0,21
CS-134
8553
2.831 E-002pCi/g
5.517E-002
5.515E-002
1.867E-001 8.973E-002
0.15
CS-136
8546
-1.109E-001 pCi/g
7.217E-002
7.189E-002
2.373E-001 1.142E-001
-0.47
CS-137
8539
3.000E+001 pCi/g
1.596E+000
3.338E-001
2.346E-001 1.129E-001
127.87
EU-152
7145
2.877E-001 pCi/g
2.421 E-001
2.417E-001
6.269E-001 3.045E-001
0,46
EU-154
7138
1.536E-001 pCi/g
1.711 E-001
1.709E-001
2.192E+000 1.058E+000
0.07
EU-155
7131
4.023E-002pCi/g
1.795E-001
1.795E-001
6.019E-001 2.949E-001
0.07
FE-59
7073
5.086E-002pCi/g
8.161 E-002
8.157E-002
4.958E-001 2.382E-001
0.10
GA-68
18005
-1,209E+000pCi/g
2.759E+000
2.758E+000
9.368E-+000 4.493E+000
-0.13
GD-153
6824
-3.997E-003pCi/g
1.316E-001
1.316E-001
4.420E-001 2.167E-001
-0.01
HF-181
6495
9.445E-002pCi/g
6.542E-002
6.524E-002
2.322E-001 1.124E-001
0.41
HG-203
6466
-3.305E-002pCi/g
5.989E-002
5.986E-002
2.006E-001 9.778E-002
-0.16
1-131
6380
6.854E-002pCi/g
6.647E-002
6.638E-002
2.080E-001 1.010E-001
0.33
IR-192
6303
-3.750E-002pCi/g
5,981 E-002
5.977E-002
2.001 E-001 9.748E-002
-0.19
K-40
6148
-1.766E-002pCi/g
3.281 E-001
3,281 E-001
1.273E+000 5.734E-001
-0.01
LA-140
6096
5.379E-002pCi/g
4.255E-002
4.246E-002
1.212E-001 5.304E-002
0.44
MN-54
5382
3.726E-002pCi/g
6.608E-002
6.605E-002
2.235E-001 1.073E-001
0.17
NA-22
5201
2.193E-002pCi/g
3.156E-002
3.154E-002
1.109E-001 4.933E-002
0.20
NB-94
5160
-7.036E-002pCi/g
5.947E-002
5.936E-002
1.977E-001 9.485E-002
-0.36
NB-95
5154
3.994E-002pCI/g
5.496E-002
5.493E-002
1.856E-001 8.861 E-002
0.22
ND-147
5083
-4.022E-002pCi/g
4.368E-001
4.368E-001
1.486E+000 7.183E-001
-0,03
NP-237
4757
-4.170E-001 pCi/g
3.829E-001
3,821 E-001
1.266E+000 6.228E-001
-0.33
NP-239
4751
-3.998E-004pCi/g
1.579E-001
1.579E-001
5.314E-001 2.601 E-001
0.00
PA-231
4541
1.362E+000pCI/g
8.851 E-001
8.820E-001
4.992E+000 2.420E+000
0.27
PA-233
4535
1.538E-001 pCI/g
1.053E-001
1.050E-001
4.596E-001 2.236E-001
0.33
PA-234
4528
-1.000E-001 pCi/g
2.035E-001
2.034E-001
6.804E-001 3.330E-001
-0.15
PA-234M
19453
-4.676E-001pCi/g
9.603E+000
9.603E+000
3.283E+001 1.580E+001
-0,01
PB-210
4467
8.549E+002pCi/g .
5.089E+001
8.359E+000
1.428E+O01 7.079E+000
59.88
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PB-212 4454 3.866E-001 pCi/g 1.254E-001 1.229E-001 3.210E-001 1.563E-001 1.20
PB-214 4448 3.785E-001 pCi/g 1.361E-001 1.347E-001 4.828E-001 2.350E-001 078
PM-144 19585 4.119E-002pCi/g 3.554E-002 3.548E-002 1.884E-001 9.023E-002 022
PM-146 2464 3.014E-002pCi/g 1.161E-001 1.161E-001 5.435E-001 2.596E-001 M6
RH-106 1882 -2.180E-001 pCi/g 1.994E-001 1.991E-001 2.012E+000 9.694E-001 OT
RU-103 1828 O.OOOE+OOOpCi/g 5.216E-002 5.216E-002 2.468E-001 1.200E-001 OOO
SB-124 ' 1784 4.494E-003pCi/g 5.524E-002 5.524E-002 1.889E-001 9.084E-002 002
SB-125 1777 2.356E-001 pCi/g 2.342E-001 2.338E-001 7.180E-001 3.497E-001 033
SC-46 1739 9.344E-002pCi/g 5.627E-002 5.606E-002 2.546E-001 1.226E-001 0J7
SN-113 1570 -5.143E-002pCi/g 9.312E-002 9.309E-002 3.121E-001 1.520E-001 =016
SN-126 17459 5.835E-002pCi/g 5.783E-001 5.783E-001 1.938E+000 9.517E-001 003
TA-182 1301 1.840E-003pCi/g 2.175E-001 2.175E-001 7.482E-001 3.582E-001 OOO
TC-99M 17412 2.645E-002pCi/g 4.239E-002 4.236E-002 1.415E-001 6.920E-002 019
TH-227 1058 2.617E+000pCi/g 1.856E+000 1.850E+000 6.105E+000 3.024E+000 043
TH-229 1046 9.577E-002pCi/g 1.073E-001 1.070E-001 3.470E+000 1.699E+000 003
TH-234 1027 7.930E-002pCi/g 7.788E-002 7.777E-002 5.067E+000 2.489E+000 002
TL-208 929 1.848E-001 pCi/g 8.785E-002 8.733E-002 2.310E-001 1.114E-001 080
U-235 281 8.439E-002pCi/g 1.008E-001 1.007E-001 9.972E-001 4.863E-001 008
• Y-88 74 -2.520E-002pCi/g 8.904E-002 8.903E-002 3.017E-001 1.458E-001 =008
ZN-65 31 -9.888E-002pCi/g 1.701E-001 1.700E-001 5.742E-001 2.762E-001 ^17
ZR-95 7 8.948E-002pCi/g 8.129E-002 8.116E-002 3.492E-001 1.669E-001 026
Sample ID WRKNO Analvte Activity StdAdded Recovery ZFactor
LCS160-217910~2-A ICS 160-217910-2-A CS-137 3.000E+001 pCI/g 3.008E+001 99.72% -0.0379
CO-60 1.774E+001 pCi/g 1.860E+001 95.37% -0.6506
AM-241 9.682E+001 pCI/g 9.723E+001 99.58% -0.0565
Sample Duplicate Information
Sample ID Pup Sample ID Analvte Samp Activity Pup Activity RPD RER PER Flag ZFactor
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-------
Blanks In formation
SamcID
WRKNO
Analvte
Activity
UncTotal
ZFactor
MB 160-217910~1-A
MB
AC-228
4.303E-002
4.671 E-002
0.9214
MB 160-217910-1-A
MB
AG-108M
5.251E-003
5.684E-003
0.9238
MB 160-217910~1-A
MB
AG-110M
-1.714E-002
2.621 E-002
-0.6542
MB 160-217910-1-A
MB
AM-241
-1.074E-002
2.656E-002
-0,4043
MB 160-217910-1-A
MB
BA-133
8.629E-003
1.742E-002
0.4954
MB 160-217910~1-A
MB
BA-140
1.558E-002
5.153E-002
0.3023
MB 160-217910~1-A
MB
BE-7
2.157E-003
9.785E-002
0.0220
MB 160-217910~1-A
MB
BI-207
1.116E-002
1.404E-002
0.7947
MB 160-217910~1-A
MB
BI-210M
1.161E-002
2.003E-002
0.5795
MB 160-217910~1-A
MB
BI-212
-6.519E-004
1.749E-001
-0.0037
MB 160-217910-1-A
MB
BI-214
-3.620E-002
1.629E-001
-0,2222
MB 160-217910~1-A
MB
CD-109
1.434E-001
1.674E-001
0,8566
MB 160-217910~1-A
MB
CD-113M
O.OOOE+OOO
1.045E+002
0,0000
MB 160-217910~1-A
MB
CE-139
1.578E-003
8.340E-003
0,1892
MB 160-217910~1-A
MB
CE-141
1.422E-002
1.284E-002
1,1075
MB 160-217910-1-A
MB
CE-144
4.109E-002
5.187E-002
0,7922
MB 160-217910~1-A
MB
CF-249
-5.027E-003
1.126E-002
-0.4467
MB 160-217910~1-A
MB
CF-251
4.859E-003
5.226E-002
0.0930
MB 160-217910~1-A
MB
CO-56
8.063E-003
1.466E-002
0.5492
MB 160-217910-1-A
MB
CO-57
O.OOOE+OOO
3.213E-003
0.0000
MB 160-217910-1-A
MB
CO-58
O.OOOE+OOO
1.250E-002
0.0000
MB 160-217910-1-A
MB
CO-60
-1.064E-002
2.053E-002
-0.5180
MB 160-217910-1-A
MB
CR-51
1.172E-001
6.390E-002
1.8350
MB 160-217910-1-A
MB
CS-134
9.670E-003
1,221 E-002
0.7837
MB 160-217910~1-A
MB
CS-136
3.486E-003
1.564E-002
0,2228
MB 160-217910-1 -A
MB
CS-137
9.350E-003
1.111 E-002
0,8412
MB 160-217910-1-A
MB
EU-152
2.175E-002
4.360E-002
0.4989
MB 160-217910~1-A
MB
EU-154
4.973E-002
3.892E-002
1.2779
MB 160-217910~1-A
MB
EU-155
1.249E-002
1.540E-002
0.8106
MB 160-217910~1-A
MB
FE-59
1.620E-002
2.388E-002
0.6781
MB 160-217910-1-A
MB
GA-68
O.OOOE+OOO
1.259E-001
0.0000
MB 160-217910-1-A
MB
GD-153
-7.436E-003
2.145E-002
-0,3466
MB 160-217910~1-A
MB
HF-181
3.207E-003
4.689E-003
0,6839
MB 160-217910~1-A
MB
HG-203
-1.192E-003
1.116E-002
-0,1067
MB 160-217910~1-A
MB
1-131
2.131 E-002
1.517E-002
1,4047
MB 160-217910~1-A
MB
IR-192
1.091E-003
6.973E-003
0.1565
MB 160-217910~1-A
MB
K-40
-4.508E-001
8.911E+000
-0.0506
MB 160-217910—1-A
MB
LA-140
O.OOOE+OOO
5.961 E-003
0.0000
MB 160-217910—1-A
MB
MN-54
-1.135E-002
1.784E-002
-0.6362
MB 160-217910~1-A
MB
NA-22
O.OOOE+OOO
4.741 E-003
0.0000
MB 160-217910~1-A
MB
NB-94
2.773E-004
1.092E-002
0.0254
MB 160-217910—1-A
MB
NB-95
7.816E-004
1.302E-002
0,0600
MB 160-217910—1-A
MB
ND-147
4.997E-002
8.625E-002
0,5794
MB 160-217910~1-A
MB
NP-237
1.411 E-002
3.697E-002
0,3816
MB 160-217910~1-A
MB
NP-239
1.903E-002
2.441 E-002
0.7798
MB 160-217910~1-A
MB
PA-231
5.945E-002
5.603E-002
1.0610
MB 160-217910~1-A
MB
PA-233
2.561 E-002
2.422E-002
1.0574
MB 160-217910~1-A
MB
PA-234
2.390E-002
2,381 E-002
1.0038
MB 160-217910—1-A
MB
PA-234M
-1.176E+000
2.117E+O00
-0.5557
MB 160-217910-1-A
MB
PB-210
O.OOOE+OOO
1.332E-001
0.0000
MB 160-217910~1-A
MB
PB-212
O.OOOE+OOO
1.627E-002
0,0000
MB 160-217910~1-A
MB
PB-214
5.054E-002
1.994E-002
2.5345
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Page 88 of 551
-------
MB 160-217910-1-A
MB
PM-144
7.657E-003
1.530E-002
0.5006
MB 160-217910~1-A
MB
PM-146
-3.061 E-002
4.827E-002
-0.6342
MB 160-217910-1-A
MB
RA-226
-8.578E-002
2.376E-001
-0.3610
MB 160-217910-1-A
MB
RH-106
-3.627E-003
1.343E-001
-0.0270
MB 160-217910-1-A
MB
RU-103
-4.735E-003
1.118E-002
-0.4237
MB 160-217910~1-A
MB
SB-124
4.616E-003
1.522E-002
0.3032
MB 160-217910-1-A
MB
SB-125
1.047E-002
2.186E-002
0.4787
MB 160-217910-1 -A
MB
SC-46
0.000E+000
7.139E-003
0.0000
MB 160-217910~1-A
MB
SN-113
6.694E-003
1.727E-002
0.3875
MB 160-217910~1-A
MB
SN-126
9.094E-003
7.322E-002
0.1242
MB 160-217910-1-A
MB
TA-182
9.043E-003
1.445E-002
0.6258
MB 160-217910-1-A
MB
TC-99M
-1.255E-003
8.033E-003
-0.1562
MB 160-217910~1-A
MB
TH-227
5.670E-003
1.499E-001
0,0378
MB 160-217910-1-A
MB
TH-229
-7.369E-002
1.885E-001
-0.3910
MB 160-217910-1-A
MB
TH-234
1.446E-002
1.018E-001
0.1420
MB 160-217910~1-A
MB
TL-208
1.346E-002
1.077E-002
1,2495
MB 160-217910~1-A
MB
U-235
7.507E-002
5.910E-002
1,2704
MB 160-217910~1-A
MB
Y-88
O.OOOE+OOO
3.838E-003
0.0000
MB 160-217910-1-A
MB
2N-65
-1.025E-002
3.666E-002
-0.2797
MB 160-217910—1-A
MB~
ZR-95
3.371 E-003
1.189E-002
0.2836
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Page 89 of 551
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TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Analysis Report for Gamma Spectroscopy
Batch: 218441 Operator:
SampID
WRKNO
Aliquot
Sigma Instrument Detector CountDateTime
CountDuration
LCS 160-218441-2-
LCS
341,90g
1.00 GammaVision
GV08 10/27/ 15 15:25 30
Analvte
Cmimcl#
Activitv
TotalUnc
CountUnc
MDA
MLCC
Aot/MDA
AC-228
11136
7.359E-002pCi/g
1.183E-001
1.183E-001
1.351E+000
6.534E-001
0.05
AG-108M
10982
-1.250E-001 pCi/g
9.830E-002
9.810E-002
3.249E-001
1.586E-001
-0.38
AG-110M
10973
-2.165E-001 pCi/g
1.350E-001
1.346E-001
4.435E-001
2,131 E-001
-0.49
AM-241
10818
9.714E+001pCi/g
5.131E+000
9.547E-001
1.461E+000
7.246E-001
66.50
BA-133
10469
-1.434E-001 pCI/g
1.166E-001
1.163E-001
3.856E-001
1.880E-001
-0.37
BA-140
10463
3.008E-001 pCl/g
3.866E-001
3.863E-001
8.898E-001
4.279E-001
0.34
BE-7
10435
1.764E-001 pCi/g
8.364E-001
8.364E-001
2.818E+000
1.373E+000
0.06
BI-207
10195
-3.983E-002pCi/g
7.303E-002
7.300E-002
2.465E-001
1.188E-001
-0.16
BI-210M
10173
4.829E-002pCi/g
6.207E-002
6,201 E-002
3.950E-001
1.928E-001
0,12
BI-212
10160
1.191E+000pCi/g
9.269E-001
9.248E-001
3.076E+000
1.467E+000
0,39
BI-214
10154
1.600E-001 pCi/g
1.464E-001
1.462E-001
4.902E-001
2.351 E-001
0.33
CD-109
9254
2.361 E+OOOpCi/g
4,441 E-K)00
4.439E+000
4.063E+000
1.992E+000
0.58
CD-113M
17462
-3.716E+001 pCi/g
9.021 E+002
9.021 E-KI02
3.049E+003
1.485E+003
-0.01
CE-139
9241
3.182E-002pCi/g
5.820E-002
5.812E-002
1.942E-001
9.506E-002
0.16
CE-141
9235
4.980E-002pCi/g
8.364E-002
8.361 E-002
2.795E-001
1.366E-001
0.18
CE-144
9221
2.569E-002pCi/g
4.004E-001
4.004E-001
1.345E+000
6.591 E-001
0.02
CF-249
9215
5.942E-002pCi/g
1.163E-001
1.162E-001
3.177E-001
1.540E-001
0.19
CF-251
13690
3.966E-001 pCi/g
2.757E-001
2.735E-001
9.033E-001
4.415E-001
0.44
CO-56
8704
8.557E-002pCI/g
8.063E-002
8.051 E-002
2.695E-001
1.287E-001
0.32
CO-57
13694
3.076E-002pCi/g
5.134E-002
5.131E-002
1.712E-001
8.393E-002
0.18
CO-58
8698
1.346E-002pCi/g
8.405E-002
8.405E-002
2.875E-001
1.379E-001
0.05
CO-60
8692
1.870E+001 pCi/g
1.007E+000
3.639E-001
1.870E-001
8.459E-002
100.02
CR-51
8604
-4.740E-001 pCi/g
6.167E-001
6.162E-001
2.059E+000
1.002E+000
-0,23
CS-134
8553
9.391 E-002pCi/g
6.368E-002
6.349E-002
1.526E-001
7.164E-002
0.62
CS-136
8546
3.304E-002pCI/g
3.799E-002
3.794E-002
3.085E-001
1.484 E-001
0.11
CS-137
8539
2.942E+001 pCi/g
1.582E+000
3.998E-001
3.497E-001
1,691E-001
84.15
EU-152
7145
1.912E-001 pCi/g
2.554E-001
2.552E-001
8.302E-001
4.042E-001
0.23
EU-154
7138
6.956E-002pCi/g
1.146E-001
1.146E-001
2.351 E-+000
1.125E+000
0.03
EU-1S5
7131
2.888E-002pCi/g
2.199E-001
2.199E-001
7.370E-001
3.618E-001
0.04
FE-59
7073
-1.833E-001 pCi/g
1.818E-001
1.815E-001
6.083E-001
2.908E-001
-0.30
GA-68
18005
4.764E+000pCi/g
2.454E+000
2.440E+000
7.914E+000
3.694E+000
0,60
GD-153
6824
7.978E-002pCi/g
1.552E-001
1.551 E-001
5.177E-001
2.540E-001
0.15
HF-181
6495
2.335E-002pCi/g
1.043E-001
1.043E-001
3.518E-001
1.712E-001
0.07
HG-203
6466
6.698E-003pCi/g
6.497E-002 1
6.497E-002
2.197E-001
1.068E-001
0.03
1-131
6380
-1.610E-002pCi/g
8.500E-002
8.500E-002
2.866E-001
1.396E-001
-0.06
IR-192
6303
1.018E-001 pCi/g
9.042E-002
9.022E-002
2.283E-001
1.111 E-001
0.45
K-40
6148
1.623E-001 pCi/g
3.950E-001
3.949E-001
1.502E+000
6.607E-001
0.11
LA-140
6096
6.191 E-003pCi/g
4.179E-002
4.179E-002
5.946E-002
1.880E-002
0.10
MN-54
5382
1.822E-002pCi/g
9.095E-002
9.094E-002
3.102E-001
1.491 E-001
0.06
NA-22
5201
1.507E-002pCi/g
4.555E-002
4.554E-002
1.637E-001
7.329E-002
0,09
NB-94
5160
6.019E-002pCr/g
3.912E-002
3.899E-002
2.572E-001
1.233E-001
0.23
NB-95
5154
2.541 E-002pCi/g
7.560E-002
7.559E-002
2.579E-001
1.234E-001
0.10
ND-147
5083
4.071 E-001pCI/g
4.877E-001
4,871E-001
1.636E+000
7.863E-001
0.25
NP-237
4757
O.OOOE+OOOpCi/g
4.510E-001
4.510E-001
1.509E+000
7.430E-001
0.00
NP-239
4751
-1.622E-002pCi/g
2,061 E-001
2.061 E-001
6.910E-001
3.393E-001
-0.02
PA-231
4541
-2.797E-001 pCi/g
6.016E-001
6.014E-001
7.388E+000
3.603E+000
-0.04
PA-233
4535
1.354E-001 pCi/g
2.200E-001
2.199E-001
5.917E-001
2.884E-001
0.23
PA-234
4528
2.370E-002pCi/g
7.301 E-002
7.300E-002
8.496E-001
4.166E-001
0.03
PA-234M
19453
2.685E+000pCi/g
3.731E+000
3.729E+000
3.935E+O01
1.884E+001
0.07
PB-210
4467
8.385E+002pCi/g
5.067E+001
1.196E+001
2.132E+001
1.059E+001
39.34
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-------
PB-212
4454
2.569E-001 pCi/g
1.484E-001
1.475E-001
4.865E-001
2.382E-001
0.53
PB-214
4448
-1.187E-001 pCi/g
2.062E-001
2.061E-001
4,941 E-001
2.392E-001
-0.24
PM-144
19585
-1.104E-002pCi/g
1.584E-002
1.583E-002
2.412E-001
1.154E-001
-0.05
PM-146
2464
1.016E-001 pCi/g
1.134E-001
1.133E-001
6.877E-001
3.278E-001
0.15
RH-106
1882
9.849E-001 pCi/g
7.318E-001
7.301 E-001
1.785E+000
8.453E-001
0.55
RU-103
1828
-7,826E-003pCI/g
8.182E-002
8.182E-002
2.777E-001
1.346E-001
-0.03
SB-124
1784
1.264E-001 pCi/g
7.595E-002
7.567E-002
1.582E-001
7.445E-002
0.80
SB-125
1777
2,237E-001pCi/g
1.965E-001
1.962E-001
9.608E-001
4.688E-001
0.23
SC-46
1739
6,651 E-002pCI/g
9.525E-002
9.519E-002
3.209E-001
1.541E-001
0,21
SN-113
1570
2.166E-002pCi/g
1.160E-001
1.160E-001
3.912E-001
1.906E-001
0.06
SN-126
17459
¦6.991 E+OOOpCi/g
1.044E+000
9.772E-001
3.085E+000
1.523E+000
-2.27
TA-182
1301
2.287E-001 pCi/g
2.419E-001
2.416E-001
9.149E-001
4.354E-001
0.25
TC-99M
17412
-3.499E-002pCi/g
5.302E-002
5.298E-002
1.767E-001
8.659E-002
-0,20
TH-227
1058
-3.701 E+001 pCi/g
4.063E+000
3.522E+000
1.124E+001
5.589E+000
-3.29
TH-229
1046
¦1.190E+0OOpCi/g
1.295E+000
1.291E+000
4.291 E+000
2.104E+000
-0.28
TH-234
1027
-5.199E+001pCi/g
5.252E+000
4.493E+000
1.365E+001
6.775E+000
-3.81
TL-208
929
1.496E-001 pCi/g
8.481 E-002
8.445E-002
2.772E-001
1.334E-001
0.54
U-235
281
-6.184E-002pCi/g
1.918E+001
1.918E+001
1.442E+000
7.072E-001
-0.04
Y-88
74
-1.169E-001 pCi/g
1.223E-001
1.221 E-001
4.080E-001
1.972E-001
-0.29
ZN-65
31
-6.060E-002pCi/g
2.169E-001
2.169E-001
7.398E-001
3.548E-001
-0.08
ZR-95 7 1.074E-001 pCi/g 1.365E-001 1.364E-001 4.600E-001 2.199E-001 0.23
Laboratory Control Sample Information
Sample ID
LCS 160-218441-2-A
WRKNO Analvte
LCS 160-218441 ~2-A CS-137
CO-60
AM-241
Activity
2.942E+001 pCi/g
1.870E+001 pCi/g
9.714E+001 pCI/g
StdAdded
3.008E+001
1.859E+001
9.723E+001
Recovery
97.82%
100.64%
99.92%
ZFactor
-0,2899
0.0836
-0.0112
Sample Duplicate Information
Sample ID
Pup Sample ID Analvte Samp Activity
Pup Activity
RPD
RER
PER Flag
ZFactor
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-------
Blanks Information
SamulD
WRKNO
Analvte
Activity
UncTotal
ZFactor
MB 160-218441~1-A
MB
AC-228
3.987E-002
4.560E-002
0.8743
MB 160-218441-1-A
MB
AQ-108M
5,451 E-003
8.527E-003
0,6393
MB 160-218441-1-A
MB
AG-110M
-1.473E-002
2.625E-002
-0.5612
MB 160-218441-1-A
MB
AM-241
-1.477E-002
2.928E-002
-0.5047
MB 160-21844M-A
MB
BA-133
3.407E-003
1.959E-002
0.1740
MB 160-218441-1-A
MB
BA-140
6.525E-002
6.139E-002
1.0630
MB 160-218441—1-A
MB
BE-7
O.OOOE+OOO
6.035E-002
0.0000
MB 160-218441-1-A
MB
BI-207
8.121E-003
1.544E-002
0.5258
MB 160-218441-1-A
MB
BI-210M
1.934E-002
1.581E-002
1.2233
MB 160-218441-1-A
MB
BI-212
O.OOOE+OOO
1.856E-001
0.0000
MB 160-218441-1-A
MB
BI-214
-1.133E-002
5.880E-002
-0.1926
MB 160-218441-1-A
MB
CD-109
9.453E-002
2.288E-001
0.4132
MB 160-218441-1-A
MB
CD-113M
-1.366E+002
2.218E+002
-0.6159
MB 160-218441-1-A
MB
CE-139
-3.140E-003
9.986E-003
-0.3145
MB 160-218441-1-A
MB
CE-141
-6.169E-003
1.570E-002
-0.3929
MB 160-218441-1-A
MB
CE-144
4.904E-003
4.662E-002
0,1052
MB 160-218441-1-A
MB
CF-249
8.754E-003
1.572E-002
0.5569
MB 160-218441-1-A
MB
CF-251
-2.594E-002
5.279E-002
-0.4914
MB 160-218441-1-A
MB
CO-56
-6.736E-003
1.135E-002
-0,5936
MB 160-218441-1-A
MB
CO-57
4.406E-003
9.298E-003
0.4738
MB 160-218441-1-A
MB
CO-58
1.276E-002
1.914E-002
0.6662
MB 160-218441-1-A
MB
CO-60
-3.371 E-003
2.082E-002
-0.1619
MB 160-218441-1-A
MB
CR-51
6.564E-002
1.182E-001
0.5552
MB 160-218441-1-A
MB
CS-134
-7.518E-004
1.083E-003
-0.6945
MB 160-218441-1-A
MB
CS-136
O.OOOE+OOO
5.399E-003
0.0000
MB 160-218441-1-A
MB
CS-137
1.650E-002
1.844E-002
0.8946
MB 160-218441-1-A
MB
EU-152
-8.619E-004
1.441 E-003
-0.5979
MB 160-218441-1-A
MB
EU-154
1.149E-001
1.445E-001
0.7954
MB 160-218441-1-A
MB
EU-155
-2.026E-002
3.719E-002
-0,5447
MB 160-218441-1-A
MB
FE-59
9.255E-003
1.826E-002
0.5070
MB 160-218441-1-A
MB
GA-68
O.OOOE+OOO
1.430E-001
0.0000
MB 160-218441-1-A
MB
GD-153
-2.088E-002
3.165E-002
-0.6598
MB 160-218441-1-A
MB
HF-181
-1.476E-003
1.865E-003
-0.7914
MB 160-218441-1-A
MB
HG-203
1.656E-002
9.732E-003
1.7013
MB 160-218441-1-A
MB
1-131
6.142E-003
2.344E-002
0,2620
MB 160-218441-1-A
MB
IR-192
3.418E-003
1.317E-002
0.2595
MB 160-218441-1-A
MB
K-40
-6.451 E-001
1.290E+001
-0.0500
MB 160-218441-1-A
MB
LA-140
2.528E-003
2.485E-002
0.1017
MB 160-218441-1-A .
MB
MN-54
-2.351 E-003
1.657E-002
-0.1419
MB 160-218441-1-A
MB
NA-22
O.OOOE+OOO
5.287E-003
0.0000
MB 160-218441-1-A
MB
NB-94
1.400E-003
7.442E-003
0,1881
MB 160-218441-1-A
MB
NB-95
-2,221 E-003
1.672E-002
-0.1328
MB 160-218441-1-A
MB
ND-147
2.932E-002
2.819E-002
1.0401
MB 160-218441-1-A
MB
NP-237
-1.201E-002
7.433E-002
-0.1615
MB 160-218441-1-A
MB
NP-239
4.366E-002
2.736E-002
1.5962
MB 160-218441-1-A
MB
PA-231
3.079E-001
2.831 E-001
1.0876
MB 160-218441-1-A
MB
PA-233
2.077E-002
3.041 E-002
0.6831
MB 160-218441-1-A
MB
PA-234
5.537E-002
5.645E-002
0.9808
MB 160-218441-1-A
MB
PA-234M
-7.028E-001
1.816E+000
-0.3870
MB 160-218441-1-A
MB
PB-210
4.463E-001
4.306E-001
1.0364
MB 160-218441-1-A
MB
PB-212
4.711 E-003
2.788E-002
0.1690
MB 160-218441-1-A
MB
PB-214
4.377E-002
3.189E-002
1.3727
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Page 92 of 551
-------
MB 160-218441-1-A
MB
PM-144
9.554E-004
6.357E-003
0.1503
MB 160-218441~1-A
MB
PM-146
-3.544E-002
4.841 E-002
-0.7319
MB 160-218441-1-A
MB
RH-106
4.655E-002
1.634E-001
0,2849
MB 160-218441~1-A
MB
RU-103
6.210E-003
1.531 E-002
0.4057
MB 160-218441-1-A
MB
SB-124
-1.006E-002
1.857E-002
-0.5418
MB 160-218441-1-A
MB
SB-125
1.305E-003
4.143E-003
0.3151
MB 160-218441-1-A
MB
SC-46
-1.594E-004
1.758E-002
-0,0091
MB 160-218441-1-A
MB
SN-113
3.684E-002
1.998E-002
1.8437
MB 160-218441-1-A '
MB
SN-126
2.933E-001
1.237E-001
2.3710
MB 160-218441-1-A
MB
TA-182
2.383E-002
4.528E-002
0,5262
MB 160-218441-1-A
MB
TC-99M
3.169E-003
8.389E-003
0.3778
MB 160-218441-1-A
MB
TH-227
2.179E-001
1.503E-001
1.4498
MB 160-218441-1-A
MB
TH-229
-9.602E-002
2.482E-001
-0,3868
MB 160-218441-1-A
MB
TH-234
-6.219E-001
8.472E-001
-0.7341
MB 160-218441-1-A
MB
TL-208
1.433E-002
2.289E-002
0.6260
MB 160-218441-1-A
MB
U-235
1.116E-001
8.413E-002
1,3268
MB 160-218441-1-A
MB
Y-88
O.OOOE+OOO
6.164E-003
0,0000
MB 160-218441-1-A
MB
ZN-65
O.OOOE+OOO
9.463E-003
0.0000
MB 160-218441-1-A
MB
ZR-95
-8.939E-004
1.210E-003
-0.7385
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-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
SampID WRKNO Aliquot Sigma Instrument Detector CountPateTime CountDuration
LCS 160-218442~2- LCS 341.90g 1.00 GammaVision GV09 10/27/15 14:09 30
Analvte
Cmimdlt
Activitv
TotalUnc
CountUnc
MDA
MLCC
Act/MDA
AC-228
11136
5.980E-001 pCI/g
2.506E-001
2.488E-001
1.014E+000
4.923E-001
0.59
AG-108M
10982
6.362E-006pCi/g
7.135E-002
7.135E-002
2.404E-001
1.175E-001
0.00
AG-110M
10973
-4.015E-003pCi/g
1.009E-001
1.009E-001
3.435E-001
1.661 E-001
-0.01
AM-241
10818
9.726E+001 pCI/g
5.101 E+000
7.368E-001
1.053E+000
5.222E-001
92.32
BA-133
10469
8.644E-004pCi/g
8.695E-002
8.695E-002
2.932E-001
1.432E-001
0.00
BA-140
10463
2.814E-001pCi/g
2.308E-001
2.303E-001
7.647E-001
3.708E-001
0.37
BE-7
10435
5.425E-001 pCi/g
6.400E-001
6.394E-001
2.131E+000
1.041E+000
0.25
BI-207
10195
-2.984E-002pCi/g
5.728E-002
5.726E-002
1.928E-001
9.338E-002
-0.15
BI-210M
10173
2.463E-002pCi/g
9.686E-002
9.684E-002
3.249E-001
1.590E-001
0.08
BI-212
10160
4.340E-001 pCi/g
7.169E-001
7.165E-001
2.420E+000
1.163E+000
0.18
BI-214
10154
8.273E-001 pCi/g
1.845E-001
1.794E-001
3.533E-001
1.700E-001
2.34
CD-109
9254
5,485E+000pCi/g
3.401E+000
3.387E+000
3.143E+000
1540E+000
1.75
CD-113M
17462
8.114E+000pCi/g
7.905E+002
7.905E+002
2.661 E+003
1.302E+003
0.00
CE-139
9241
-3.089E-002pCi/g
5.178E-002
5.170E-002
1.723E-001
8.460E-002
-0.18
CE-141
9235
-3.579E-003pCi/g
6.317E-002
6.317E-002
2.129E-001
1.040E-001
-0.02
CE-144
9221
1.068E-001 pCi/g
3.278E-001
3.277E-001
1.096E+000
5.379E-001
0.10
CF-249
9215
1.007E-001 pCi/g
1.004E-001
1.002E-001
2.876E-001
1.404E-001
0.35
CF-251
13690
-2.639E-001 pCi/g
2.511E-001
2.500E-001
8.293E-001
4.069E-001
-0.32
CO-56
8704
1.134E-001 pCi/g
8.881 E-002
8.861 E-002
2.341 E-001
1.131 E-001
0.48
CO-57
13694
5.717E-003pCi/g
4.406E-002
4.406E-002
1.476E-001
7.249E-002
0.04
CO-58
8698
5,129E-002pCi/g
6.155E-002
6.150E-002
2.064E-001
9.935E-002
0.25
CO-60
8692
1.774E+001 pCi/g
9.122E-001
1.984E-001
9.851 E-002
4.359E-002
180.05
CR-51
8604
-2.572E-002pCi/g
5.332E-001
5.332E-001
1.795E+000
8.779E-001
-0.01
CS-134
8553
5.920E-002pCi/g
4.059E-002
4.047E-002
2.764E-001
1.350E-001
0.21
CS-136
8546
4.051 E-002pCi/g
4.705E-002
4.700E-002
1.989E-001
9.561 E-002
0.20
CS-137
8539
2.895E+001 pCi/g
1.537E+000
3.066E-001
2.184E-001
1.053E-001
132.57
EU-152
7145
1.210E-001 pCi/g
1.140E-001
1.138E-001
6.662E-001
3.254E-001
0.18
EU-154
7138
1.536E-001 pCi/g
2.903E-001
2.902E-001
2.035E+000
9.844E-001
0.08
EU-155
7131
-2.215E-001 pCi/g
1.885E-001
1.881 E-001
6.227E-001
3.061 E-001
-0,36
FE-59
7073
-2.347E-001 pCI/g
1.656E-001
1.651 E-001
5.463E-001
2.646E-001
-0.43
GA-68
18005
-1.959E+000pCi/g
2.934E+000
2.932E+000
9.861 E+000
4.761 E+000
-0.20
GD-153
6824
1.074E-001 pCI/g
5.604E-002
5.566E-002
4.253E-001
2.089E-001
0.25
HF-181
6495
7.655E-003pCi/g
2.864E-002
2.863E-002
2.832E-001
1.384E-001
0.03
HG-203
6466
-5.635E-002pCi/g
6.273E-002
6.264E-002
2.084E-001
1.020E-001
-0.27
1-131
6380
7.130E-002pCi/g
8.246E-002
8.238E-002
2.211E-001
1.079E-001
0.32
IR-192
6303
6.154E-002pCi/g
5.067E-002
5.054E-002
2.010E-001
9.829E-002
0.31
K-40
6148
-1.447E-001 pCi/g
7.481E-001
7.481 E-001
1.284E+000
5.849E-001
-0.11
LA-140
6096
1.563E-002pCi/g
2.812E-002
2.811 E-002
1.016E-001
4.393E-002
0.15
MN-54
5382
-2.832E-002pCi/g
6.926E-002
6.925E-002
2.341E-001
1.131 E-001
-0.12
NA-22
5201
-2.471 E-002pCi/g
3.987E-002
3.985E-002
1.381 E-001
6.356E-002
-0.18
NB-94
5160
4.992E-002pCI/g
4.304E-002
4.296E-002
1.435E-001
6.826E-002
0.35
NB-95
5154
-8.541 E-002pCI/g
6.319E-002
6.303E-002
2.089E-001
1.008E-001
-0.41
ND-147
5083
-5.970E-002pCi/g
4.393E-001
4.392E-001
1.487E+000
7.219E-001
-0.04
NP-237
4757
-4.152E-001 pCi/g
3.778E-001
3.771 E-001
1.248E+000
6.152E-001
-0.33
NP-239
4751
1.422E-001 pCi/g
1.425E-001
1.422E-001
4.725E-001
2.313E-001
0,30
PA-231
4541
7.897E-001 pCi/g
5.588E-001
5.571 E-001
6.014E+000
2.942E+000
0.13
PA-233
4535
1.659E-001 pCi/g
1.174E-001
1.170E-001
4.817E-001
2.355E-001
0.34
PA-234
4528
7,379E-003pCI/g
1.848E-001
1.848E-001
6.212E-001
3.043E-001
0.01
PA-234M
19453
-3.849E+000pCi/g
1.050E+001
1.050E+001
3.544E+001
1.718E+001
-0.11
PB-210
4467
8.556E+002pCi/g
5.093E+001
8.354E+000
1.399E+001
6.939E+000
61.17
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Page 94 of 551
Analysis Report for Gamma Spectroscopy
Batch: 218442 Operator:
-------
PB-212
4454
4.747E-001 pCi/g
1.198E-001
1.158E-001
2.884E-001
1.405E-001
1.65
PB-214
4448
2.527E-001 pCi/g
1.397E-001
1.390E-001
4.865E-001
2.377E-001
0.52
PM-144
19585
5.467E-002pCi/g
5.088E-002
5.080E-002
1.697E-001
8.140E-002
0,32
PM-146
2464
-1.121 E-001pCI/g
1.694E-001
1.693E-001
5.705E-001
2.747E-001
-0.20
RH-106
1882
2.453E-001 pCi/g
5.500E-001
5.499E-001
1.858E+000
8.973E-001
0.13
RU-103
1828
3.179E-003pCi/g
6.795E-002
6.795E-002
2.296E-001
1.119E-001
0.01
SB-124
1784
6.871 E-002pCi/g
5.491 E-002
5.479E-002
1.820E-001
8.786E-002
0.38
SB-125
1777
7.725E-002pCi/g
1.204E-001
1.203E-001
7.192E-001
3.515E-001
0.11
SC-46
1739
6.865E-002pCI/g
3.773E-002
3.756E-002
2.744E-001
1.331E-001
0.25
SN-113
1570
-5.988E-002pCi/g
9.283E-002
9.278E-002
3.100E-001
1.515E-001
-0.19
SN-126
17459
4.728E-001 pCi/g
6.187E-001
6.182E-001
2.053E+000
1.011E+000
0.23
TA-182
1301
2.190E-001 pCi/g
1.744E-001
1.740E-001
6.078E-001
2.897E-001
0.36
TC-99M
17412
4.814E-002pCi/g
4.538E-002
4.530E-002
1.502E-001
7.375E-002
0.32
TH-227
1058
5.812E-001 pCi/g
8.496E-001
8.490E-001
7.338E+000
3.643E+000
0.08
TH-229
1046
3.346E-001 pCi/g
9.867E-001
9.864E-001
3.300E+000
1.619E+000
0.10
TH-234
1027
-3.012E+001 pCi/g
2.825E+000
2.346E+000
7.161E+000
3.541E+000
-4.21
TL-208
929
1.402E-001 pCi/g
7.085E-002
7.047E-002
2.180E-001
1.055E-001
0.64
U-235
281
1.225E-001 pCi/g
2.509E-001
2.508E-001
1.165E+000
5.718E-001
0.11
Y-88
74
-5.977E-002pCi/g
8.913E-002
8.908E-002
2.987E-001
1.449E-001
-0.20
ZN-65
31
1.053E-001 pCi/g
9,011 E-002
8.995E-002
3.017E-001
1.411E-001
0,35
ZR-95
7
3.603E-002pCi/g
1.120E-001
1.120E-001
3.799E-001
1.833E-001
0.09
Laboratory Control Sample Information
Sample ID
LCS160-218442-2-A
WRKNO
LCS 160-218442-2-A
Analvte
CS-137
CO-60
AM-241
Activity
2.895E+001 pCi/g
1.774E+001 pCi/g
9.726E+001 pCi/g
StdAdded
3.008E+001
1.859E+001
9.723E+001
Recovery
96.24%
95.42%
100.04%
ZFactor
-0.5100
-0.6439
0.0052
Sample Duplicate Information
Sample ID Pup Sample ID Analvte Samp Activity Pup Activity RPP RER PER Flag ZFactor
10/29/2015
2:42:37PM
Page 2 of 4 RadCapture, version 5.1.00, released 7/26/2012
Page 95 of 551
-------
Blanks Information
SamolD
WRKNO
Analyte
Activity
UncTotal
ZFactor
MB 160-218442-1-A
MB
AC-228
4.629E-002
5.406E-002
0.8562
MB 160-218442-1-A
MB
AG-108M
5.830E-003
1.413E-002
0.4125
MB 160-218442-1-A
MB
AG-110M
1.867E-002
2.797E-002
0.6674
MB 160-218442-1-A
MB
AM-241
4.337E-002
3.562E-002
1.2178
MB 160-218442~1-A
MB
BA-133
3.213E-003
1.707E-002
0.1882
MB 160-218442~1-A
MB
BA-140
7.074E-002
6.022E-002
1.1747
MB 160-218442~1-A
MB
BE-7
2.063E-003
1.089E-001
0.0189
MB 160-218442-1-A
MB
BI-207
-8.550E-003
1.554E-002
-0.5500
MB 160-218442~1-A
MB
BI-210M
-5.240E-005
2.134E-002
-0,0025
MB 160-218442-1-A
MB
BI-212
1.891 E-001
2.106E-001
0.8980
MB 160-218442~1-A
MB
BI-214
5.878E-002
4.257E-002
1.3807
MB 160-218442~1-A
MB
CD-109
-3.780E-002
2.773E-001
-0.1363
MB 160-218442~1-A
MB
CD-113M
-1.209E+002
2.006E+002
-0.6023
MB 160-218442~1-A
MB
CE-139
-2.638E-003
1.098E-002
-0.2403
MB 160-218442-1-A
MB
CE-141
O.OOOE+OOO
1.549E-002
0.0000
MB 160-218442-1-A
MB
CE-144
2.685E-004
7.314E-002
0.0037
MB 160-218442-1-A
MB
CF-249
1.313E-003
1.950E-002
0.0673
MB 160-218442-1-A
MB
CF-251
-3.857E-003
5.706E-002
-0.0676
MB 160-218442~1-A
MB
CO-56
1.232E-004
1.804E-004
0.6833
MB 160-218442—1 -A
MB
CO-57
2.443E-003
8.085E-003
0.3022
MB 160-218442—1-A
MB
CO-58
-1.180E-003
2.037E-002
-0.0579
MB 160-218442-1-A
MB
CO-60
6.900E-003
9.579E-003
0.7203
MB 160-218442-1-A
MB
CR-51
1.599E-003
1.074E-001
0.0149
MB 160-218442-1-A
MB
CS-134
3.207E-002
2.395E-002
1.3391
MB 160-218442~1-A
MB
CS-136
5.803E-003
1.781 E-002
0.3257
MB 160-218442~1-A
MB
CS-137
O.OOOE+OOO
1.138E-002
0.0000
MB 160-218442~1-A
MB
EU-152
-3.093E-005
4.932E-002
-0.0006
MB 160-218442-1 -A
MB
EU-154
-1.070E-001
1.707E-001
-0.6272
MB 160-218442-1-A
MB
EU-155
2.380E-002
1.887E-002
1.2612
MB 160-218442-1-A
MB
FE-59
O.OOOE+OOO
8.903E-003
0.0000
MB 160-218442~1-A
MB
GA-68
O.OOOE+OOO
1.515E-001
0.0000
MB 160-218442~1-A
MB
GD-153
O.OOOE+OOO
1.067E-002
0.0000
MB 160-218442~1-A
MB
HF-181
1.261E-002
1.480E-002
0.8522
MB 160-218442- 1-A
MB
HG-203
3.510E-003
1.144E-002
0.3067
MB 160-218442~1-A
MB
1-131
O.OOOE+OOO
6.680E-003
0.0000
MB 160-218442-1 -A
MB
IR-192
1.578E-003
1.452E-002
0,1086
MB 160-218442-1-A
MB
K-40
-2.137E-001
7.006E-001
-0.3050
MB 160-218442~1-A
MB
LA-140
O.OOOE+OOO
7.055E-003
0.0000
MB 160-218442-1-A
MB
MN-54
O.OOOE+OOO
5.770E-003
0.0000
MB 160-218442~1-A
MB
NA-22
-2.879E-004
1.602E-002
-0.0180
MB 160-218442~1-A
MB
NB-94
1.568E-003
1.741 E-002
0.0901
MB 160-218442-1-A
MB
NB-95
2.922E-003
1.554E-002
0.1880
MB 160-218442~1-A
MB
ND-147
7.112E-002
1.032E-001
0.6894
MB 160-218442-1-A
MB
NP-237
5.092E-003
7.332E-002
0.0695
MB 160-218442-1-A
MB
NP-239
1.565E-002
3.200E-002
0.4890
MB 160-218442~1-A
MB
PA-231
-1.854E-001
3.961 E-001
-0.4681
MB 160-218442~1-A
MB
PA-233
7.432E-003
1.916E-002
0.3879
MB 160-218442~1-A
MB
PA-234
1.231 E-002
3.411 E-002
0.3608
MB 160-218442-1-A
MB
PA-234M
O.OOOE+OOO
7.911 E-001
0.0000
MB 160-218442-1-A
MB
PB-210
3.880E-001
4.487E-001
0.8648
MB 160-218442—1 -A
MB
PB-212
-2.440E-002
9.674E-002
-0.2522
MB 160-218442-1 -A
MB
PB-214
-2.424E-002
8.010E-002
-0,3026
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Page 96 of 551
-------
MB 160-218442-1-A
MB
PM-144
2.715E-003
1.733E-002
0.1567
MB 160-218442-1-A
MB
PM-146
1.519E-002
1.570E-002
0.9676
MB 160-218442-1-A
MB
RH-106
-2.995E-002
1.833E-001
-0,1634
MB 160-218442~1-A
MB
RU-103
-5.540E-003
1.385E-002
-0,4000
MB 160-218442~1-A
MB
SB-124
3.566E-003
1.681 E-002
0.2121
MB 160-218442~1-A
MB
SB-125
-3.271 E-002
4.871 E-002
-0.6716
MB 160-218442~1-A
MB
SC-46
1.794E-002
1.459E-002
1.2302
MB 160-218442~1-A
MB
SN-113
5.033E-004
1.899E-002
0.0265
MB 160-218442~1 -A
MB
SN-126
2.542E-002
1.062E-001
0.2393
MB 160-218442~1-A
MB
TA-182
5,091 E-002
6.392E-002
0.7965
MB 160-218442~1-A
MB
TC-99M
4.412E-003
8.994E-003
0.4906
MB 160-218442~1-A
MB
TH-227
O.OOOE+OOO
6.308E-002
0.0000
MB 160-218442~1-A
MB
TH-229
1.425E-001
1.928E-001
0,7391
MB 160-218442~1-A
MB
TH-234
-5.703E-002
3.530E-001
-0.1616
MB 160-218442~1-A
MB
TL-208
-2.982E-003
2.496E-002
-0.1195
MB 160-218442~1 -A
MB
U-235
-6.134E-003
8.135E-003
-0.7541
MB 160-218442~1-A
MB
Y-88
1.099E-002
2.017E-002
0.5449
MB 160-218442~1-A
MB
ZN-65
O.OOOE+OOO
1.005E-002
0,0000
MB 160-218442~1-A
MB
ZR-95
-1.630E-002
3.169E-002
-0.5142
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Page 97 of 551
-------
l^ac'd ; IZ-ZU-OLp
ANALYTICS
An Isotope Products Laboratories Company
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404"352'8677
Fax 404"352*2837
www.analyticslnc.com
74139-334
1.0 Liter Sand in 1 Liter Wide Mouth HDPE "S" Bottle
Customer: Severn Trent Laboratories/Earth City, MO
P.O. No,: 2169877, Item 1
Calibration Date: Ol-Oct-2QQ6 12:00 EST Grams of Master Source: 0.01832
This standard radionuclide source was prepared using aliquots measured gravimetric ally from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given.' Analytics maintains
traceability to the National Institute of Standards and Technology through a Measurements Assurance
Program as described in USNRC Regulatory Guide 4.IB, Revision 1, February, 1979, and compliance
with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST."
Nuclide
Master Uncertainty, %
Gamma-Ray Half-Life, Source* This Source Type Calibration
Energy (keV) Pays Tps/gram Tps ufl uB U Method
Pb-210
Am-241
Cd-109
Co-67
Ce-139
Hg-203
Sn-113
Cs-137
Y-88
Co-60
Co-60
Y-88
46.S
59.5
88.0
122.1
168.9
279.2
391.7
661.7
898.0
1173.2
1332.5
1836.1
8145.9
157860
462.60
271.79
137.6
46.61
115.1
10983
106.60
1925.4
1925.4
100.6
189000
94570
133800
295300
185600
116700
453400
226900
227000
481200
3079.8
2034.3
2933.5
1467.8
2076.7
4583
2880.7
1811.3
7068
3522
3823
7469
0.33
0.33
0.S7
0.34
0.35
0.40
0.42
0.70
0.30
0.60
0.90
0.90
1.46
1.46
1.70
1.30
1.10
1.10
1.10
1.20
1.10
1.10
1.10
1.10
2.99
2.99
3.89
2.69
2.31
2.34
2.38
2.78
2.42
2.51
2.84
2.84
4rrLS
4n LS
HPGe
HPGe
HPGe
HPGe
HPGe
HPGe
HPGe
HPGe
HPGe
HPGe
* Master Source rsfera to Analytics1 8-isotope mixture which is calibrated quarterly,
Calibration Methods! 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer,
IC - Ionization Chamber. Uncertainty! U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines
for Evaluating and Expressing the Uncertainty of NIST Measurement Results."
Comments:
1880 grams of sand. NOTE: Homogeneity was checked by the addition of Tc-99 tracer to the solution used to
spike the sand. Ten 10-gram aliquots were removed after mixing and counted to measure the Tc-S9. The
standard deviation for the 10 measurements was 1,3% with a range of 4.8%. This demonstrates reasonable
homogeneity for this source material down to a 10-gram aliquot.
This standard will expire one year after the calibration date.
Source Prepared by:
QA Approved:
M. I. Taskaeva, Radiochemist
Date: 12 ~0£
D. M. Montgomery, OA Manager
End of Certificate
Corporate Office Laboratory
AvpniieTlhhlm Valonrla. California qi w Page 98 Of 551 1380 Seaboard Industrial Blvd. Atlanta, Georaia. 30318
-------
Reagent
Tuna Can 00002
Page 99 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
81427-334
1,0 Liter Sand, in 1 Liter HDPE Silgan Jar
Customer; TestAmerica/St. Louis, MO
P.O. No.: 2339090, Item 1
Reference Date; . 0L-Jan-2010 12:00 PM EST Grams of Master Source: 0.017570
This standard radionuclide source was prepared using aliquots measured gravimetxieally from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected. The
gamma-ray emission rates for the most intense gamma-ray lines are given. Eckert & Ziegler Analytics
(EZA) maintains traceability. to the National Institute of Standards and Technology through a
Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February,
1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to KIST." EZA is
accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this
source was produced in accordance with the HPS accreditation requirements. Customers may report any
concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402,
McLean, VA 22101.
Master
Uncertainty
, %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
Ypa/gram
Tps
%
uB
U
Method
Pb-210
48.8
8.120E+03
3.141E+03
0.1
2.1
4.1
4 IT LS
Am-241
59.5
LS80E+QS
2.034E+03
0.1
1.7
3.S
4n LS
Cd-109
88.0
4.626E+02
1.806E+0S
2.822E+03
0.4
2.3
4.7
HPGe
Co-S7
122.1
2.718E+02
8.471E+04
1.488E+03
0.8
2.0
4.1
HPGe
Ce-139
165.9
1.376E+02
1.209E+03
2.124E+03
0.4
1.9
3.9
HPGe
Hg-203
279.2
4.661E+01
2.728E+0S
4.790E+03
0.4
1.9
3.9
HPGe
Sn-113
391.7
1.151E+02
1.672E+0S
2.938E+03
0.5
1.9
3.9
HPGe
Cs-132
661.7
1.098E+04
1.096E+05
1.926E+03
0.6
1.9
4.0
HPGe
Y-88
898.0
1.066E+02
• 4.077E+05
7.163E+03
0.4
1.9
3.9
HPGe
Co-60
1173.2
1.925E+03
2.0S6E+08
3.611E+03
0.5
1.9
3.9
HPGe '
Co-60
1332.S
1.92SE+03
2.056E+05
3.612E+03
0.7
1.9
4.0
HPGe
Y-88
1836.1
1.066E+02
4.308E+0S
7.S69E+03
0.8
1.9
3.9
HPGe
* Master Source refers to Analytics1 8-isotope mixture which is calibrated quarterly.
Calibration Methods: 4tj LS - 4 pi Liquid Scintillation Counting, HPGa - High Purity Germanium Gamma-Ray Spectrometer, IG -
Ionization Chamber. Uncertainty; U - Relative expanded uncertainty, k = 2, See NIST Technical Note 1297, "Guidelines for
Evaluating and Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 404-352-2837
www.analyticsinc.com
MGS Certificate, Rev 2 09-28-2009
(»$. caus^
Page 1 of 2
*>A0^7 fiuent)
Corporate Office
> Tihhlf-tc Ualonria C alifnrnia 01 3 ^
Laboratory
1ISO Industrial Rlvd Atlanta
-------
Comments;
1050 grams of sand.
This standard will expire one year after the reference date.
Source Prepared by:
OA Approved;
W. Mao, Radiochemist
J. D. McCorvey, OA Manager Alternat
Dd\e:Xj / j I
0
i
cAue^
MGS Certificate, Rev 2 09-28-2009
Page 2 of 2
Page 101 of 551
-------
Reagent
Tuna Can 00003
Page 102 of 551
-------
Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tet 404-352-8677
Fax 404-352-2837
www.analyticslnc.com
90099
1.0 Liter Sand in 1 Liter Wide Mouth HDPE Silgan Jar
Customer: TestAmerica St. Louis / Earth City, MO
P.O. No.: 2454180, Item 1
Reference Date: 01-Jan-2012 12:00 PM EST Grams of Master Source: 0.017180
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Additional radionuclides were added gravimetrically from solutions calibrated by
gamma-ray spectrometry, ionization chamber, or liquid scintillation counting. Calibration and purity were
checked using a germanium gamma spectrometer system. At the time of calibration no interfering gamma-ray
emitting impurities were detected. The gamma-ray emission rates for the most intense gamma-ray lines arc
given. Eckert & Ziegler Analytics (EZA) maintains traceability to the National Institute of Standards and
Technology through a Measurements Assurance Program as described in USNRC Regulatory Guide 4. IS,
Revision 2, July 2007, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST."
EZA is accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this
source was produced in accordance with the HPS accreditation requirements. Customers may report any
concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean
VA 22101.
Master
Uncertainty* , %
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
yps/gram
TPs
Ufl
U
Method*
Pb-210
46.8
8.109E+03
3.094E+03
0.1
2.1
4.1
4rr LS
Am-241
89,5
1.880E+05
2.037E+03
0.1
1.7
3.8
4ttLS
Cd-109
88.0
4.626E+02
1.677E+0S
2.881E+03
0.5
2.3
4.7
HPGe
Co-57
122.1
2.718E+02
8.79SE+04
1.511E+03
0.4
2.0
4.1
HPGe
Ce-139
165.9
1.376E+02
1.245E+0S
2.139E+03
0.4
1.9
3.9
HPGe
Hg-203
279.2
4.661E+01
2.707E+0S
4.851E+03
0.3
1.9
3.8
HPGe
Sn-'l 13
¦ 391.7
1.151E+02
1.7SSE+05
3.0ISE+03
0.4
1.9
3.9
HPGe
Cs-137
661.7
1.098E+04
1.128E+05
1.938E+03
0.7
1.9
4.0
HPGe
Y-88
898.0
1.066E+02
4.228E-0S
7.264E+03
0.8
1.9
3.9
HPGe
Co-60
1173.2
1.925E+03
2.084E+0S
3.S80E+03
0.6
1.9
4.0
HPGe
Co-60
1332.8
1.925E+03
2.084E+05
3.881E+03
0.7
1.9
4.0
HPGe
Y-88
1836.1
1.066E+02
4.476E+0S
7.690E+03
0.7
1.9
4.0
HPGe
* Master Source refers to Analytics' 8-isotope mixture which is calibrated quarterly.
Calibration Methods: 4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Hay Spectrometer, IG -
Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines for
Evaluating and Expressing the Uncertainty of NIST Measurement Results,"
(Certificate continued on reverse side)
-------
Comments:
1550 grams of sand. Homogenous down to 10 grams aliquot,
This standard will expire one year after the reference date.
Source Prepared by
OA Approved:
Z. Dimitrova, Radiochemist
j.D. McCorvey, Counting Room Man! ger
Date: ^0 "3^. ^
MGS Certificate, Rev 3 04-08-2010
Pagd%
Page 2 of 2
-------
Reagent
Tuna Can 00006
Page 105 of 551
-------
• Eckert & Ziegler
Analytics
CERTIFICATE OF CALIBRATION
Standard Radionuclide Source
83814-334
1.0 Liter Sand in 1 Liter Wide Mouth HDPE Silgan Jar
Customer: Test America St. Louis
P.O. No,: 2395112, Item 1
Reference Dale: 01-Jan-2011 12:00 PM EST Grams of Master Source: 0.016927
This standard radionuclide source was prepared using aliquots measured gravimetrically from master
radionuclide solutions. Calibration and purity were checked using a germanium gamma spectrometer
system. At the time of calibration no interfering gamma-ray emitting impurities were detected, The
gamma-ray emission rates for the most intense gamma-ray lines are given. Eckert & Ziegler Analytics
(EZA) maintains traceability to the National Institute of Standards and Technology through a
Measurements Assurance Program as described in USNRC Regulatory Guide 4.15, Revision 1, February,
1979, and compliance with ANSI N42.22-1995, "Traceability of Radioactive Sources to NIST," EZA is
accredited by the Health Physics Society (HPS) for the production of NIST-traceable sources, and this
source was produced in accordance with the HPS accreditation requirements. Customers may report any
concerns with the accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402,
McLean, VA 22101.
Master
Uncertainty
Gamma-Ray
Half-Life,
Source*
This Source
Type
Calibration
Nuclide
Energy (keV)
Days
yps/gram
Yps
%
U
Method
Pb-210
46.5
8.120E+03
3.021E+03
0.1
2.1
4.1
4n LS
Am-241
59.5
1.580E+05
2.090E+03
0.1
1.7
3.5
4-n LS
Cd-109
88.0
4.626E+02
1.697E+05
2.873E+03
0.8
2.3^
4.9
HPGe
Co-57
122.1
2.718E-I-02
8.711E+04
1.478E+03
0.6
2.0~
4.1
HPGe
Ce-139
165,9
1.376E+02
1.247E+0S
2.111E+03
0.5
1.9
3.9
HPGe
Hg-203
279.2
4.661E+01
2.7S3E+Q6
4.660E+03
0.4
1.9
3.9
HPGe
Sn-113
391.7
1.181E+02
1.769E+05
2.994E+03
0.8
1.9
3.9
HPGe
Cs-137
661.7
1.098E+04
1.109E+05
1.877E+03
0.7
1.9
4.0
HPGe
Y-8S
' 898.0
1.066E+02
4.224E+0B
7.150E+03
0.5
1.0
3.9
HPGe
Co-60
1173.2
1.926E+Q3
2.142E+05
3.626E+03
o.e
1.9
4.0
HPGe
Co-60
1332.5
1.925E+03
2.143E+05
3.627E+03
0.6
1.9
4.0
HPGe
Y-8S
1836.1
1.066E+02'
4.472E+05
7.570E+03
0.5
1.9
3.9
HPGe
* Master Source refers to Analytics' 8-isotope mixture which is calibrated quarterly.
Calibration Methods :4rr LS - 4 pi Liquid Scintillation Counting, HPGe - High Purity Germanium Gamma-Ray Spectrometer, 1C
- Ionization Chamber. Uncertainty: U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297s"Guidelines for
Evaluating and Expressing the Uncertainty of NIST Measurement Results."
(Certificate continued on reverse side)
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404*352*8677
Fax 404-352-2837
www.analyticsinc.com
-------
1
Comments;
1580 grams of sand, Homogeneous down to 10 gram aliquot.
This standard will expire one year after the reference date.
Source Prepared by:
OA Approved:
Z. Dimitrova, Radiochemist
Date:
z(t I [ <\
J, D. McCorvey, OA Manager Alternate
^feCA UBn
/ '
O /w
& if
MGS Certificate, Rev 2 09-28-2009
Pag&-1
Page 2 of 2
-------
Reagent
U-232 00003
Page 108 of 551
-------
• Eckert&Ziegler
Analytics
CERTIFICATE OF CALIBRATION
" Standard Radionuclide Source
85539-334
8 mL Liquid in Flame Sealed Vial
Customer; Test America/Earth City, MO
P.O. No.: 2434448. Item 1
This standard radionuclide source was prepared gravimetrically from a master solution, calibrated by Eckert
& Zieglor Analytics. The master solution was calibrated by liquid scintillation counting. Radionuclide purity
and calibration were checked by germanium gamma-ray spectrometry and liquid scintillation counting. The
nuclear decay rate and reference date for this source are given below, Eckert & Ziegler Analytics (EZA)
maintains traceabiiity to the National Institute of Standards and Technology through a Measurements
Assurance Program as described in USMRC Regulatory Guide 4.18, Revision 1, February, 1919, and
compliance with ANSI N42.22-199S, "Traceabiiity of Radioactive Sources to NIST." EZA is accredited by the
Health Physics Society (HPS) for the production of NIST-traceable sources, and this source was produced in
accordance with the HPS accreditation requirements. Customers may report any concerns with the
accreditation program to the HPS Secretariat, 1313 Dolley Madison Blvd., Ste. 402, McLean, VA 22101.
1380 Seaboard Industrial Blvd.
Atlanta, Georgia 30318
Tel 404-352-8677
Fax 404-352*2837
www.a na lyticsi nc.com
Isotope
Half-Life,
Days
Activity
(Bq)
Uncertainty*, %
Type
% % U
Reference Date
(12:00 PM EST)
U-232
2.517E+04
1.725E+04
0.5
2.4 4.9
08/25/2011
^Uncertainty; U - Relative expanded uncertainty, k = 2. See NIST Technical Note 1297, "Guidelines tor Evaluating and Expressing
the Uncertainty of NIST Measurement Results."
Comments:
Impurities: U-232 daughters, y-impurities (other than decay products) <0.1 %.
Source Prepared by:
M. I. Taskaeva. Radiochemist
OA Approved:
Date:
J. D. McCorvey, OA Manager Alternate
Single Isotope Certificate, Rev 1 9/28/2009
Page 109 of 551
Corporate Office
24937 Avenue Tibbitts Valencia, California 91355
Laboratory
1380 Seaboard Industrial Blvd. Atlanta, Georgia, 30318
-------
Reagent
U-232 00034
Page 110 of 551
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
True Value =
Date Analyzed:
U-232_00034""""""|
78.54115[DPM/L org
3/24/20161
Radionuclide:
| U-232 |
Replicates
#1
75.703
DPM/L or g
#2
74.112
DPM/L or g
#3
77.034
DPM/L or g
Mean = 75.61633
1 sigma = 1.462927
True Value minus 5% =
True Value plus 5% =
1,96 sigma = 2.867336
74.61409
82.4682
(True Value - 5%)
(True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value?
Precision:
1.96 sigma Value Within 10% of Mean Value?
Standard Reverification Acceptable?
Yes (Acceptance Criteria)
Yes (Acceptance Criteria)
Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date:
Amanda Leigh Dick 03/29/2016
SOP Reference: STL-QA-0002, Current Revision
Page 111 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscof
Analysis Report
Sample Name: Verification 1
SampleType: Sample
Sample Collection Date:
Batch Name: U-232_00034
AnalysisiD: 671238
Tracer Name: UNAT Spike_00001
Tracer Activity: 72.27 DPIVl/mL x (Vol.)0.10 mL
Tracer Ref. Date: 3/30/2008 11:00:22AM
Sample
Batch
Tracer
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:47:39AM 3/29/2016
Spectrum #1 Analysis #1
Sample Volume : 0.1000mL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
7.23 DPM
Tracer Nuclide: U-238
Tracer Recovery: 104.90%
Acquisition
Detector: AV132
Serial Number: 49-16404
Acquisition Start Date: 3/24/2016 6:16:21PM
Live Time: 960.00 min.
Real Time: 960.02 min. ,
Background Date: 3/16/2016 3:25:06PM
Background Info: Sample: ICB;AV132; Det: AV132; Spectrum #1;
Mar-16-2016 15:25
Calibration Name: IC-9886;AV132-20150604
Calibration Date: 6/4/2015 6:23:37PM
Gain = 7.4575 keV/Ch
Enerqv Cal: Offset = 3,366.95 keV
Quadratic = 0.0000 keV/Ch2
Efficiency: 24.32% +/- 0.33% TPU(2 sigma)
200
180
160
140
<1
-
V
120 -
o
100 -
so -
60 -
40 -
20 -
0 -
U-238
; I
-i—r
U-235
LI-234
U-232
1
\
^6-
-t-°1—i 'T* i
J.~L
~ I I
i "r i i
3374 3674 3974 4274 4574 4374 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keY)
General Analysis ¦
Analysis Method: Absolute ROI Analysis, Set Name = U_Verify
Decay Correction: 3/24/2016 6:14:58PM
MDA Constants: Ka = 1.65 , K(3 = 1.65
Nuclide Library: Uranium
MDA Source: Background
Nuclide
Peak
Energy
keV
Peak
Expected
keV
Peak
Diff
keV
ROI
Start
keV
ROI
End
keV
Nuclide Summary (ROI)
FWHM
keV
B.R.
%
Gross
Counts
Bkgd
Counts
Net
Counts
Activity Units
U-238 4157.5 4,196.0 -38.5 3956.1 4261.9 87.0 100.0 1770 0.0000 1770.00
U-235 4381.2 4,396.0 -14.8 4269,3 4470.7 25.7 91.1 68 0.0000 68.00
U-234 4776.4 4,775.8 0.6 4530.3 4851.0 76.4 99.8 1603 0.0000 1603.00
U-232 5343.2 5,320.3 22.9 5097.1 5410.3 80.2 100.4 1862 0.0000 1862.00
75.809 DPM/mL
3.048 DPM/mL
65.578 DPM/mL
75.703 DPM/mL
Page 112 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
~
Ipha-Spectroscoi
Analysis Report
LI
Sample Name: Verification 2
SampleType: Sample
Sample Collection Date:
Batch Name: U-232_00034
AnalysisID: 671239
Sample
Batch
Tracer
Tracer Name: UNAT Spike_00001
Tracer Activity: 72.27 DPM/mL x (Vol.)0.10 mL = 7.23 DPM
Tracer Ref. Date: 3/30/2008 11:00:22AM
i Acquisition
Detector: AV133
Serial Number: 49-169B4
Acquisition Start Date: 3/24/2016 6:16:23PM
Live Time: 960.00 min.
Real Time: 960.02 min.
Background Date: 3/16/2016 3:25:08PM
Background Info: Sample: ICB;AV133; Det: AV133; Spectrum #1;
Mar-16-2016 15:25
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:47:27AM 3/29/2016
Spectrum #1 Analysis #1
Sample Volume : 0.1000mL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
Tracer Nuclide: U-238
Tracer Recovery: 93.31%
Calibration Name: IC-7107;AV133-20150607
Calibration Date: 6/8/2015 7:46:18PM
Gain = 7.4575 keV/Ch
Energy Cal: Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch
Efficiency: 25.35% +/- 0.29% TPU(2 sigma)
Energy (keV)
—— General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = U_Verify Nuclide Library: Uranium
Decay Correction: 3/24/2016 6:14:58PM MDA Source: Background
MDA Constants: Koc = 1.65 , K(3 = 1.65
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity
Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
44.2
100.0
1641
0.0000
1641.00
67.428
DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
93.5
91.1
64
0.0000
64.00
3.094
DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
84.5
99.8
1523
0.0000
1523.00
67.203
DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
87.0
100.4
1690
0.0000
1690.00
74.112
DPM/mL
Page 113 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 3
SampleType: Sample
Sample Collection Date:
•¦3 Name: U-232_00034
AnalysisID: 671240
Sample
Batch
Tracer
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:47:13AM 3/29/2016
Spectrum #1 Analysis #1
Sample Volume : O.IOOOmL
Aliquot: N/A Aliquot Fraction: N/A
Analyst: 60040
Tracer Name: UNAT Spike_00001
Tracer Activity: 72.27 DPM/mL x (Vol.)0.10 ml. = 7.23 DPM
Tracer Ref. Date: 3/30/2008 11:00:22AM
— Acquisition
Detector: AV134
Serial Number: 49-169C2
Acquisition Start Date: 3/24/2016 6:16:24PM
Live Time: 960.00 min.
Real Time: 960.02 min.
Background Date: 3/16/2016 3:25:10PM
Background Info: Sample: ICB;AV134; Det: AV134; Spectrum #1;
Mar-16-2016 15:25
Tracer Nuclide: U-238
Tracer Recovery: 93.15%
Calibration Name: IC-8874;AV134-20150607a
Calibration Date: 6/8/2015 7:46:39PM
Gain = 7.4575 keV/Ch
Enerqv Cal: Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 26.35% +/- 0.38% TPU(2 sigma)
200 -
180
160
140 -
«
¦E 120
zs
o
o
100 -
80 -
60 -
40
20
0 H
, , , , , p,,, | T,„| | | | |~ ^ 1111^,1,1111
3374 3674 3974 4274 4574 4674 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV)
U-23S
*4
U-235
U-234
i
i
M
General Analysis ¦
Analysis Method: Absolute ROI Analysis, Set Name = U_Verify
Decay Correction: 3/24/2016 6:14:58PM
MDA Constants: Koc = 1.65 , K(3 = 1.65
Nuclide Library: Uranium
MDA Source: Background
Peak
Peak
Peak
ROI
ROI
Nucnae nummary (ROI)
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity
Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
78.5
100.0
1703
0.0000
1703.00
67.317
DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
62.8
91.1
68
0.0000
68.00
3.167
DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
82.9
99.8
1632
0.0000
1632.00
69.391
DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
82.7
100.4
1825
2.0000
1823.00
77.034
DPM/mL
Page 114 of 551
-------
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603977.4
35.37889501
dpm
days
days
dpm
Uranium-232
82.245
8/25/2011
3/24/2016
1673
25165.725
0.954965614
78.54114693
Initial Activity:
Reference Date:
Current Date:
Elapsed Time:
Half Life:
Exponential Term:
| Corrected Activity:
-------
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Page 116 of 551
-------
TestAmerica
THE LEADER in environmental testing
Reagent ID: U-232 00034
Description:
No. of Bottles:
Storage Location:
Reagent Volume:
Creation Date:
Open Date:
Container(s):
Comment:
U-232 clean
1
RAD Actinide STDs
250.000 mL
03/23/2016
875270
3 4
Expiration Date:
Laboratory:
Prepared By:
Solvent:
Solvent Lot:
07/16/2016
TestAmerica St. Louis
Bernsen, Sarah C
Dl Water
n/a
Reagent Analyte Information
Analyte
U-232
Source ID
Source
Exp. Date
Source
Cone.
Source Cone.
Units
U-232 00009
08/06/2016 10280.70700
dpm/mL
Final
Cone.
82.24566
Final
Cone. Units
dpm/mL
Source Reagents
Vendor Vendor Volume Volum<
Reagent Description Type Expiration Vendor Lot# Cat Lot# Used Units
U-232_00009 U-232 Parent 08/06/16 2.00000 mL
03/23/2016 14:30
Page 117 of 551
Page 1 of 1
-------
Reagent
UNAT Ampoule 00001
Page 118 of 551
-------
New Brunswick Laboratory
U.S. Department of Energy
Certificate of Analysis
CRM 145
Uranyl (Normal) Nitrate Assay and Isotopic Solution
Uranium Mass Fraction: 0.0101356 g U/g solution ± 0.0000011 g U/g solution
[ 10.1356 mg U/g solution ± 0.0011 mg U/g solution ]
234-jj^238 235y^238^j
0.000052841 0.0072543
0.000000082 0.0000040
234U.
235u
238u
Atom Percent:
0.0052458
0.72017
99.27458
Atom Percent Uncertainty:
0.0000081
0.00039
0.00039
Weight Percent:
0.0051579
0.71114
99.28370
Weight Percent Uncertainty:
0.0000080
0.00038
0.00038
Relative Atomic Weight: 238.028918
Relative Atomic Weight Uncertainty: 0.000012
Note: 233U and 236U were not detected. The detection limit of uranium ratios for the technique used is 5 x 1 (T9.
This Certified Reference Material (CRM) is a uranium concentration and isotopic solution standard intended for use in
calibration of and/or quality control for uranium analysis methods. Each unit of CRM 145 consists of approximately
20-mL of uranyl nitrate solution in 1M nitric acid, contained in a sealed glass ampoule.
NOTE: The vial should be handled under proper radiologically-controlled conditions at all times.
The certified uranium content value is based on the mass of high-purity metal dissolved and diluted to a known solution radi3-oois
mass. The stated uranium concentration was calculated as the prepared value and verified experimentally by the NBL- ^JjSSpike
modified Davies and Gray titration. The certified uranium isotopic composition and atomic weight is based upon None
measurements performed on multiple samples by two different measurement techniques on a Thermal Ionization Mass t:xp(i^'a/1'o/2m'4'2°13
Spectrometer (TIMS), calibrated using CRM U030-A as primary comparator and CRM 129-A as a quality control Fxp(2): S/10/2014
sample. The isotopic values are shared with CRM 112-A, uranium (normal) metal standard which was the source of
uranium used to produce the solutions.
All uncertainties for the certified values are expressed as expanded uncertainties (U) where U = k*u0, where u0 is the
September 30, 2010
Argonne, Illinois www.nbl.doe.gov
Page 1 of2
(Revision of Certificate dated March 30, 2008)
Page 119 of 551
Atom Ratio:
Atom Ratio Uncertainty:
Jon Neuhoff, Director
New Brunswick Laboratory
127971
ID; UNAT_00008
Exp: 05/10/14 Prpd: SB Cri: 05/03/13
UNAT spike
-------
combined standard uncertainty and the coverage factor k = 2. Uncertainties were determined according to the JCGM
100:2008 Guide to the Expression of Uncertainty in Measurement. The coverage factor of 2 was chosen to provide an
approximate 95% level of confidence, The input quantities associated with the uranium content included uncertainties
due to weighing, CRM 112-A purity, and buoyancy factors. The input quantities associated with the uranium isotopic
composition included uncertainties from the certified value for CRM U030-A, measurement precision, and background
corrections associated with the analytical techniques.
The CRM was produced by dissolving uranium metal in a single batch and container, with extensive mixing of the
resultant solution followed by dispensation into individual bottles. Subsequent measurements of a random sampling of
the total lot produced did not indicate any inhomogeneity in uranium concentration or isotopic composition. The
minimum sample sizes taken from packaged units and measured were 30 mg U by titration and 1 |ig U by TIMS. The
NBL makes no recommendation as to the minimum sample size to be used to ensure concentration or isotopic
homogeneity.
Users are cautioned that once the vial is opened, the uranium concentration and/or isotopic composition of the material
may be affected by evaporative losses or environmental contamination. User's should take appropriate precautions to
safeguard the material before, during and after use to ensure valid certificate values.
Recommended Procedure for Ampoule Handling and Dispensing of Solution
1. The ampoule contains a strongly acidic solution of uranium. Appropriate precautions should be taken.
2. Before opening the ampoule, ensure that any dried uranium or condensed liquid in the neck or body of the
ampoule is re-dissolved into solution. This can be accomplished by inverting the ampoule repeatedly.
3. The glass ampoules are scored at the neck for ease of opening. However, glass burrs and fragments pose a cut
hazard to anyone opening the ampoules. Appropriate precautions should be taken.
4. Lightly moisten the scored line on the neck with distilled water to help ensure a clean break at the score.
5. Because of the narrow neck of the ampoule it may be difficult or impossible to pour the solution out. Here is
one possible method:
a. Obtain approximately 12-cm length of plastic capillary tubing (e.g. i.d. Of 0.1", o.d. of 0.16").
b. Insert one end of the capillary tubing fully into the ampoule
c. Fold the remaining length of tubing along the outside of the ampoule, ensuring that the tube is not
crimped and will allow the free flow of air through the tube and into the ampoule.
d. Holding the ampoule and tubing in one hand, and a beaker or dispensing bottle in another, invert the
ampoule over the container allowing the solution to drain into it.
e. The capillary tubing allows air to flow into the ampoule, eliminating the "airlock" created by the
narrow neck of the open ampoule,
6. The user should be wary of evaporative losses once the ampoule is opened, and prevent uranium
contamination of the sample. It is recommended that the entire solution be accurately weighed and aliquanted
as soon as possible after opening the sample. Precautions should be taken (clean glass/plastic ware, air
filtration, etc) to prevent uranium contamination of the CRM with subsequent perturbation of the isotopic
composition.
September 30, 2010 Jon Neuhoff, Director
Argonne, Illinois www.nbl.doe.gov New Brunswick Laboratory
Page 2 of 2
(Revision of Certificate dated March 30, 2008)
Page 120 of 551
-------
Reagent
UNAT 00012
Page 121 of 551
-------
St. Louis Radiological Standard Reverification Form
UNAT 00011
Radionuclide:
True Value
=
70.69 IDPM/L or g | U-234 |
Date Analyzed:
5/5/2016j
Replicates
#1
66.49
DPM/L org
#2
71.93
DPM/L or g
#3
67.79
DPM/L or g
Mean =
68.73667
1 sigma =
2.840868
1.96 sigma = 5.568102
True Value minus 5% =
True Value plus 5% =
67.1555
74.2245
(True Value - 5%)
(True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value?
Precision:
1.96 sigma Value Within 10% of Mean Value?
Standard Reverification Acceptable?
Yes (Acceptance Criteria)
Yes (Acceptance Criteria)
Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date:
Amanda Dick 05/09/2016
SOP Reference: STL-QA-0002, Current Revision
Page 122 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
WaI
pna-bpectrosc
Analysis Repo
Sample
Sample Name: Verification 1
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Type: Sample
Batch
Batch Name: UN AT 00011
Description:
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mLx (Vol.) 0.10 mL:
Tracer Ref. Date: 8/25/2011 12:03:08PM
Tracer
8.22 DPM
Acquisition
Detector: AV194 SN: 50-119J2
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.00 min.
Background Date: 4/22/2016 10:41:10AM
Bkgd Info: Sample: ICB;AV194; Det: AV194; Spectrum #1; 4/22/2016
10:41:10 AM
~
lestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:10:46AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 100.46%
Energy Calibration: IC-9520;AV194-20151017
Efficiency Calibration:IC-9520;AV194-20151017
Calibration Date: 10/18/2015 3:55:14PM
Energy Cal: Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.83% +/- 0.35% TPU(2 sigma)
240 -
220
200 -
180 -
180 -
w
"I 14 0 -
Q
(3
120 -
1» -
60 -
60 -
40 -
20 -
0 -
3374 3874 3974 4274 4574 4874 5174 5474 5774 6074 6374 ©874 ©974 7274 7574
Enerfly (feeV)
General Analysis —
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM Nuclide Library: Uranium
MDA Constants: Ka = 1.64 , K|3 = 1.64 MDA Source: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
77.8
100.0
1645
1.0000
1644.00
6.865E+001 DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
22.2
80.2
60
3,0000
57.00
2.968E+000 DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
74.8
99.8
1590
1.0000
1589.00
6.649E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
76.2
100.1
1892
8.0000
1884.00
8.262E+001 DPM/mL
4-H-
U-235
U-234
U-232
i'i—f™iMi^"i i—i 1 i1 f1
J,
i i r
~I I I I i
l I I 1 I
Page 123 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 2 Type: Sample
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Batch Name: UNAT_00011
Description:
Sample
Batch
Tracer
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mL x (Vol.) 0.10 ml. = 8.22 DPM
Tracer Ref. Date: 8/25/2011 12:03:08PM _ Acquisition
Detector: AV195 SN: 50-117AA2
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.00 min.
Background Date: 4722/2016 10:41:10AM
Bkgd Info: Sample: ICB;AV195; Det: AV195; Spectrum #1; 4/22/2016
10:41:10 AM
lestAmerica at. Louis
13715 Rider Trail North
Earth City, MO 63045
11:10:20AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 83.14%
Energy Calibration: IC-9792;AV195-20151017a
Efficiency Calibration:IC-9792;AV195-20151017a
Calibration Date: 10/18/2015 3:55:41PM
Enerqv Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.85% +/- 0.30% TPU(2 sigma)
200 -
160
140
¦fe 12ft
3
O
Q
60 -
40 ¦
20 -
U-23E
U-235
Kl
U-234
« U-232
-I rT
6674
i—i i i—r
7274 7574
0 H—r—r-i—r
3374 '3674
3974
4274 4574
r " r
4874
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM
MDAConstants: Ka=1.64,K(3= 1.64
f i i '"r"i
5174 5474
Energy flseV)
General Analysis
F" i ni
5774
i r i
©074
T I I
8374
¦T—i—r
6i74
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI)1
Nuclide
Peak
Energy
keV
Peak
Expected
keV
Peak
Diff
keV
ROI
Start
keV
ROI
End
keV
FWHM
keV
B.R.
%
Gross
Counts
Bkgd
Counts
Net
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
73.6
100.0
1490
0.0000
1490.00
7.223E+001 DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
78.5
80.2
77
0.0000
77.00
4.654E+000 DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
69.4
99.8
1484
3.0000
1481.00
7.193E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
73.2
100.1
1633
10.0000
1623.00
6.838E+001 DPM/mL
Page 124 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 3 Type: Sample
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Batch Name: UNAT_00011
Description:
Sample
Batch
Tracer
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mL x (Vol.) 0.10 mL = 8.22 DPM
Tracer Ref. Date: 8/25/2011 12:03:08PM .
Acquisition
Detector: AV197 SN: 50-117Z5
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.01 min.
Background Date: 4/25/2016 9:56:18AM
Bkgd Info: Sample: ICB;AV197; Det: AV197; Spectrum #1; 4/25/2016
9:56:18 AM
lestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:09:54AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 95.37%
Energy Calibration: IC-9794;AV197-20151017
Efficiency Calibration:IC-9794;AV197-20151017
Calibration Date: 10/18/2015 3:55:22PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.48% +/- 0.31% TPU(2 sigma)
220
200
181
160
« «D'
I isc
1130 -
80
60
«
20
U-23E
k
¦1
3374
-r~r—i' r'r,T""T"
3674 3974
U-235
A
U-234
4274
T I I
4574 4874
U-232
1—I
51:74
4.
5774
5474
Energy flsaV)
General Analysis
6074 6374
I f ' I
6674
6974
i—I—r
7274
t—i—r
7574
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM
MDA Constants: Ka = 1.64 , K|3 = 1.64
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI)
Nuclide
Peak
Energy
keV
Peak
Expected
keV
Peak
Diff
keV
ROI
Start
keV
ROI
End
keV
FWHM
keV
B.R.
%
Gross
Counts
Bkgd
Counts
Net
Counts
Activity Units
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
73.5
99.8
1519
3.0000
1516.00
6.779E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
78.8
100.1
1769
6.0000
1763.00
7.844E+001 DPM/mL
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
72.8
100.0
1655
0.0000
1655.00
7.385E+001 DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
62.5
80.2
77
0.0000
77.00
4.284E+000 DPM/mL
Page 125 of 551
-------
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TestAmerica
THE LEADER !N ENVIRONMENTAL TESTING
Reagent ID: UNAT 00011
U N A T
Description:
No. of Bottles:
Storage Location:
Reagent Volume:
Creation Date:
Open Date:
Container(s):
Comment:
Analyte
UNAT spike
1
RAD Actinide STDs
200.000 mL
04/28/2015
622074
1 1
Expiration Date:
Laboratory:
Prepared By:
Solvent:
Solvent Lot:
Reagent Analyte Information
05/20/2016
TestAmerica St. Louis
Bernsen, Sarah C
1M HN03
n/a
Source ID
Source
Exp. Date
Source
Cone.
Source Cone.
Units
Final
Cone.
Final
Cone. Units
U-234
U-235
U-238
UNAT Parent_00001
UNAT Parent_00001
UNAT Parent 00001
05/20/2016 706.91200
05/20/2016 33.70600
05/20/2016 722.65000
dpm/mL 70.69123
dpm/mL 3.37064
dpm/mL 72.26499
dpm/mL
dpm/mL
dpm/mL
Source Reagents
Vendor Vendor Volume Volum<
Reagent Description Type Expiration Vendor Lot# Cat Lot# Used Units
UNAT Parent_00001 UNAT Parent 05/20/16 20.00000 mL
05/02/2016 14:34
Page 127 of 551
Page 1 of 1
-------
Batch:
Uranium only via UTEVA
ST-RC-0238
*AII rinses should flow at 1 mL/minute (only 3M HN03 may be done at 3 mL/minute)
Page 128 of 551
Form: RAD-0060, Revised 09/17/13
-------
St. Louis Radiological Standard Reverification Form
Standard ID Number:
True Value =
Date Analyzed:
Replicates
#1
68.65
DPM/L
or
g
#2
72.23
DPM/L
or
g
#3
73.85
DPM/L
or
g
Mean = 71.57667
1 sigma = 2.660852 1.96 sigma = 5,21527
True Value minus 5% = 68.65166 (True Value - 5%)
True Value plus 5% = 75.87815 (True Value + 5%)
Accuracy:
Mean value within 5% of Certified (True) Value? Yes (Acceptance Criteria)
Precision:
1.96 sigma Value Within 10% of Mean Value? Yes (Acceptance Criteria)
Standard Reverification Acceptable? Yes
Note: Criteria for reverification of radiological standards is taken from the
DOE QSAS and LANL Statements of Work
Reviewed By/Date: Amanda Dick 05/09/2016
SOP Reference: STL-QA-0002, Current Revision
UN AT
_00011 |
Radionuclide:
72.2649
DPM/L org
| U-238 |
5/5/2016
Page 129 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 1
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Batch Name: UNAT 00011
Type: Sample
Sample
Description:
Batch
Tracer
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mL x (Vol.) 0.10 mL = 8.22 DPM
Tracer Ref. Date: 8/25/2011 12:03:08PM
Acquisition
Detector: AV194 SN: 50-119J2
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.00 min.
Background Date: 4/22/2016 10:41:10AM
Bkgd Info: Sample: ICB;AV194; Det: AV194; Spectrum #1; 4/22/2016
10:41:10 AM
lestAmerica at. Louis
13715 Rider Trail North
Earth City, MO 63045
11:10:46 AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 100.46%
Energy Calibration: IC-9520;AV194-20151017
Efficiency Calibration:IC-9520;AV194-20151017
Calibration Date: 10/18/2015 3:55:14PM
Energy Cal: Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.83% +/- 0.35% TPU(2 sigma)
240
220'
200
180
160
m
K 140
Q
U
120
m
80
6§
40
20
0
3374 3674 3974 4274 4574 4874 51i74 5474 5774 6074 6374 8B74 8974 7274 7574
Energy (teVJ
¦ General Analysis —— —
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM Nuclide Library: Uranium
MDAConstants: Ka=1.64,Kp= 1.64 MDASource: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Nuclide
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
77.8
100.0
1645
1.0000
1644.00
6.865E+001 DPIWmL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
22.2
80.2
60
3.0000
57.00
2.968E+000 DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
74.8
99.8
1590
1.0000
1589.00
6.649E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
76.2
100.1
1892
8.0000
1884.00
8.262E+001 DPM/mL
Page 130 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 2
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Batch Name: UNAT 00011
Type: Sample
Sample
Description:
Batch
Tracer
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mL x (Vol.) 0.10 mL = 8.22 DPM
Tracer Ref. Date: 8/25/2011 12:03:08PM
Acquisition
Detector: AV195 SN: 50-117AA2
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.00 min.
Background Date: 4722/2016 10:41:10AM
Bkgd Info: Sample: ICB;AV195; Det: AV195; Spectrum #1; 4/22/2016
10:41:10 AM
lestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:10:20AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 83.14%
Energy Calibration: IC-9792;AV195-20151017a
Efficiency Calibration:IC-9792;AV195-20151017a
Calibration Date: 10/18/2015 3:55:41PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.85% +/- 0.30% TPU(2 sigma)
2D0
181
16»
140
-£ 120
Z!
O
U-238
-1—r-T—f-T
3374 3674
U-235
U-234
T
i U-232
^ 1 I
f" i "i
f—r
3974 4274 4574 4374 c174 5474 5774 8074
Energy {JseV)
General Analysis
i i i i r
T I I I I I I [
8974 7274 7574
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM
MDAConstants: Ka=1.64,K(3= 1.64
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI)'
Peak
Peak
Peak
ROI
ROI
Nuclide
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
73.6
100.0
1490
0.0000
1490.00
7.223E+001 DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
78.5
80.2
77
0.0000
77.00
4.654E+000 DPM/mL
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
69.4
99.8
1484
3.0000
1481.00
7.193E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
73.2
100.1
1633
10.0000
1623.00
6.838E+001 DPM/mL
Page 131 of 551
-------
Type: Sample
Sample
Batch
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Verification 3
Spectrum #1 Analysis #1
Sample Collection Date:
Comment:
Batch Name: UNAT_00011
Description:
Tracer Name: U-232_00032
Tracer Activity: 82.25 DPM / mLx (Vol.) 0.10 mL :
Tracer Ref. Date: 8/25/2011 12:03:08PM
Detector: AV197 SN: 50-117Z5
Acquisition Start Date: 5/5/2016 10:51:35AM
Live Time: 960.00 min.
Real Time: 960.01 min.
Background Date: 4/25/2016 9:56:18AM
Bkgd Info: Sample: ICB;AV197; Det: AV197; Spectrum #1; 4/25/2016
9:56:18 AM
Tracer
8.22 DPM
Acquisition
lestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:09:54AM 5/9/2016
Sample Volume: 0.10
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: mL
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 95.37%
Energy Calibration: IC-9794;AV197-20151017
Efficiency Calibration:IC-9794;AV197-20151017
Calibration Date: 10/18/2015 3:55:22PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.48% +/- 0.31% TPU(2 sigma)
220
20®
180
1:60
| 120
100
80
80
20
0
3374 3674 3974 4274 4574 4874 5174 5474 5774 8074 6374 6674 6974 7274 7574
Energy flraV)
General Analysis
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:5/5/2016 10:49:41AM Nuclide Library: Uranium
MDAConstants: Ka=1.64,Kp= 1.64 MDASource: Background
Nuclide Summary (ROI) ————
Peak
Peak
Peak
ROI
ROI
Nuclide
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
73.5
99.8
1519
3.0000
1516.00
6.779E+001 DPM/mL
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
78.8
100.1
1769
6.0000
1763.00
7.844E+001 DPM/mL
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
72.8
100.0
1655
0.0000
1655.00
7.385E+001 DPM/mL
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
62.5
80.2
77
0.0000
77,00
4.284E+000 DPM/mL
U-235
h i i r
—IjrililiMt Hi
U-234
U-232
i I I
T-T
t—r—r
r i—i—p
Page 132 of 551
-------
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Page 133 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Reagent ID: UNAT_00011
Description:
No. of Bottles;
Storage Location:
Reagent Volume:
Creation Date:
Open Date:
Container(s):
Comment:
UNAT spike
1
RAD Actinide STDs
200.000 mL
04/28/2015
622074
Expiration Date:
Laboratory:
Prepared By:
Solvent:
Solvent Lot:
05/20/2016
TestAmerica St. Louis
Bernsen, Sarah C
1M HN03
n/a
Reagent Analyte Information
Analyte
Source ID
Source
Exp. Date
Source
Cone.
Source Cone.
Units
Final
Cone.
Final
Cone. Units
U-234
UNAT Parent_00001
05/20/2016
706.91200
dpm/mL
70.69123
dpm/mL
U-235
UNAT Parent_00001
05/20/2016
33,70600
dpm/mL
3.37064
dpm/mL
U-238
UNAT Parent_00001
05/20/2016
722.65000
dpm/mL
72.26499
dpm/mL
Source Reagents
D . . Vendor Vendor Volume Volum<
Reagent Description Type Expiration Vendor Lot # Cat Lot # Used Units
UNAT Parent_00001 UNAT Parent 05/20/16 20.00000 mL
05/02/2016 14:34
Page 134 of 551
Page 1 of 1
-------
Uranium only via UTEVA
Batch: ST-RC-0238
*AII rinses should flow at 1 mL/minute (only 3M HN03 may be done at 3 mL/minute)
Page 135 of 551
Form: RAD-0060, Revised 09/17/13
-------
ALPHA SPECTROSCOPY
Page 136 of 551
-------
Method A-01-R Th
Isotopic Thorium (Alpha
Spectrometry) by Method A-01-R
Page 137 of 551
-------
Prep Batch: 257492
Preparation, Extraction
Chromatography Resin Actinide
Separation
Page 138 of 551
-------
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257492
Lab ID: MB 160-257492/1 -A
Client ID:
Sigma: 2
Analyzed: 07/02/16 15:17
Detector: AV148
Dil Fac: 1
Decay Corrected: No
Yield Truncated: Yes
Is: 400
Analyte
MB Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
0.1309
0.0590
0.0600
pCi/g
0.0620
0.0233 259078
Thorium-230
0.1162
0.0488
0.0497
pCi/g
0.0154
0.00647 259078
Thorium-232
0.002972
0.0110
0.0110
U
pCi/g
0.0282
0.00644 259078
Tracer
MB Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
5.001
0.291
0.511
pCi/g
0.00756
6.06 82.6
30-110
Lab ID: LCS 160-257492/2-A
Analyzed
: 07/02/16
15:17
Decay Corrected: No
Client ID:
Detector:
AV150
Yi icated: Yes
Sigma: 2
Dil Fac:
1
Is: 400
Analyte
LCS Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-230
26.83
1.05
2.49
pCi/g
0.0307
0.0129 259080
Tracer
LCS Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
10.99
0.639
1.12
pCi/g
0.0203
12.1 90.6
30-110
Lab ID: 160-17314-1
Analyzed
: 07/02/16
15:17
Decay Corrected: No
Client ID: AC-SED-4
Detector:
AV151
Yi icated: Yes
Sigma: 2
Dil Fac:
1
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
1.01
0.146
0.169
pCi/g
0.0658
0.0254 259081
Thorium-230
3.56
0.268
0.401
pCi/g
0.0278
0.00635 259081
Thorium-232
1.04
0.144
0.169
pCi/g
0.0150
0.00632 259081
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
5.37
0.310
0.547
pCi/g
0.00798
6.05 88.8
30-110
Lab ID: 160-17 DU
Analyzed
: 07/02/16
15:17
Decay Corrected: No
Client ID: AC-SED-4
Detector:
AV152
Yi icated: Yes
Sigma: 2
Dil Fac:
1
Is: 400
Analyte
DU Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
0.9640
0.144
0.165
pCi/g
0.0589
0.0217 259082
Thorium-230
3.480
0.269
0.397
pCi/g
0.0286
0.00654 259082
Thorium-232
0.9194
0.138
0.158
pCi/g
0.0285
0.00651 259082
Page 1 of 3
TestAmerica St. Louis
Page 139 of 551
-------
Tracer
DU Result Count Unc Total Unc Qualifier Unit
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257492
Spike Added % Rec % Rec Limits
DLC
Thorium-229
5.378
0.315
0.551
pCi/g
0.0101
6.05 88.9
30-110
Lab ID:
Client ID:
Sigma:
160-17314-2
AC-SED-6
2
Analyzed
Detector:
Dil Fac:
: 07/02/16
AV153
1
15:17
Decay Corrected: No
Yi icated: Yes
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
1.07
0.150
0.175
pCi/g
0.0545
0.0195 259083
Thorium-230
2.82
0.241
0.338
pCi/g
0.0339
0.00920 259083
Thorium-232
1.19
0.156
0.185
pCi/g
0.0154
0.00647 259083
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
5.01
0.292
0.512
pCi/g
0.00760
6.07 82.6
30-110
Lab ID:
Client ID:
Sigma:
160-17314-3
AC-SED-7
2
Analyzed
Detector:
Dil Fac:
: 07/07/16
AV199
1
13:10
Decay Corrected: No
Yi icated: Yes
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
0.728
0.119
0.134
pCi/g
0.0628
0.0245 259665
Thorium-230
2.45
0.212
0.296
pCi/g
0.0300
0.00817 259665
Thorium-232
0.656
0.109
0.123
pCi/g
0.0251
0.00575 259665
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
8.24
0.388
0.793
X
pCi/g
0.00999
6.05 136
30-110
Lab ID:
Client ID:
Sigma:
160-17314-4
AC-SED-8
2
Analyzed
Detector:
Dil Fac:
: 07/02/16
AV155
1
15:17
Decay Corrected: No
Yi icated: Yes
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Thorium-228
1.07
0.153
0.177
pCi/g
0.0652
0.0248 259085
Thorium-230
3.77
0.281
0.423
pCi/g
0.0157
0.00660 259085
Thorium-232
1.11
0.152
0.178
pCi/g
0.0156
0.00656 259085
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Thorium-229
5.39
0.317
0.552
pCi/g
0.00211
6.04 89.2
30-110
Page 2 of 3
Page 140 of 551
TestAmerica St. Louis
-------
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257492
Quail ntrol Summary
Method Blank ID:
Analyte
Parent Result
Spike Added
MB Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER
RER Limit
Z Factor
MB 160-257492/1-A
Thorium-228
0.1309
pCi/g
4.361193
58
4.671035
MB 160-257492/1-A
Thorium-230
0.1162
pCi/g
MB 160-257492/1-A
Thorium-232
0.002972
U
pCi/g
.5383239
Lab Control Sample ID:
Analyte
Parent Result
Spike Added
LCS Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER
RER Limit
Z Factor
ICS 160-257492/2-A
Thorium-230
24.5
26.83
pCi/g
110
81-118
1.388087
6722
Duplicate ID:
Analyte
Parent Result
Spike Added
DU Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER
RER Limit
Z Factor
160-17814-1
160-17814-1
160-17814-1
Thorium-228
Thorium-230
Thorium-232
1.01
3.56
1.04
0.9640
3.480
0.9194
pCi/g
pCi/g
pCi/g
5
2
12
0.14
0.10
0.37
0.40
0.29
1.04
1
1
1
Glossary:
Ts = Count Duration, Sample
Page 3 of 3
Page 141 of 551
TestAmerica St. Louis
-------
ALPHA SPECTROSCOPY BATCH WORKSHEET
Lab Name: TestAmerica St. Louis Job No.: 160-17814-1
SDG No.:
Batch Number: 257492 Batch Start Date: 06/22/16 10:35 Batch Analyst: Bernsen, Sarah C
Batch Method: ExtChrom Batch End Date: 07/01/16 16:21
Lab Sample ID
Client Sample ID
Method Chain
Basis
InitialAmount
Th-229 00020
TRM-2 00001
AnalysisComment
MB 160-257492/1
ExtChrom,
A-01-R
1. 0 g
0.2 mL
LCS
160-257492/2
ExtChrom,
A-01-R
0.4989 g
0.2 mL
0.4989 g
TRM
160-17814-A-l-A
AC-SED-4
ExtChrom,
A-01-R
T
1. 0018 g
0.2 mL
160-17814-A-l-A
DU
AC-SED-4
ExtChrom,
A-01-R
T
1.0008 g
0.2 mL
160-17814-A-2-A
AC-SED-6
ExtChrom,
A-01-R
T
0.9986 g
0.2 mL
160-17814-A-3-A
AC-SED-7
ExtChrom,
A-01-R
T
1.0003 g
0.2 mL
160-17814-A-4-A
AC-SED-8
ExtChrom,
A-01-R
T
1.0033 g
0.2 mL
Batch Notes
Balance ID
27050421
Analyst ID - Column
nmn per scb
Column Date
7/1/16
Analyst ID - CoPrecipitation
scb
CoPrecipitation Date
7/1/16
Pipette ID
Radl04
Analyst ID - Reagent Drop Witness
rj s per scb
Analyst ID - Reagent Drop
scb
SOP Number
ST-RC-0 0 03, ST-RC-0004, ST-RC-0100, ST-RC-0242
Basis
Basis Description
T
Total/NA
The pound sign (#) in the amount added field denotes that the reagent was
this reagent.
A-01-R
used undiluted. All calculations are performed using the stated concentration for
Page 1 of 1
Page 142 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample
Sample Name: MB 160-257492/1-A
Spectrum #1 Analysis #1
: MB 160-257492/1-A
Sample Collection Date: 7/1/2016 4:42:00PM
Comment:
Batch Name: 257492
AnalysisResultsID: 170136
Description:
Type: Blank
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV148 SN: 50-05/R2
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.01 min.
Background Date: 6/24/2016 4:15:34PM
Bkgd Info: Sample: ICB;AV148; Det: AV148; Spectrum #1; 6/24/2016
4:15:34 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:57:22PM
7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 82.58%
Energy Calibration: IC-8874;AV148-20151016a
Efficiency Calibration:IC-8874;AV148-20151016a
Calibration Date: 10/16/2015 6:47:19PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 26.72% +/- 0.38% TPU(2 sigma)
SO
so
70
m 60
Zl
Q
° 50
40
30
20
10
0
3374 3674 3974 4274 4574 4S74 5174 5474 5774 ©074 6374 6674 6974 7274 7574
Energy ikeV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:38PM Nuclide Library: Thorium
MDA Constants: Ka = 1.64 , K(3 = 1.64 MDA Source: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
44.5
100.2
1
0.4167
0.58
2.972E-003 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
.3
99.7
23
0.0000
22.69
1.162E-001 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
98.6
99.6
1183
0.8333
1182.17
5.001 E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
75.0
99.8
31
5.4167
25.58
1.309E-001 pCi/g
Th-232
h—i—r1
Th-229
Th-230
V
Th-228
Page 143 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: LCS 160-257492/2-A
Spectrum #1 Analysis #1
: LCS 160-257492/2-A
Sample Collection Date: 7/1/2016 4:42:00PM
Comment:
Batch Name: 257492
AnalysisResultsID: 170138
Description:
Type: Control
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 mL= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV150 SN: 50-05/R4
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.01 min.
Background Date: 6/24/2016 4:15:33PM
Bkgd Info: Sample: ICB;AV150; Det: AV150; Spectrum #1; 6/24/2016
4:15:33 PM
9:57:52PM
7/2/2016
Sample Weight: 0.50
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 90.56%
Energy Calibration: IC-8876;AV150-20151016
Efficiency Calibration:IC-8876;AV150-20151016
Calibration Date: 10/16/2015 6:46:46PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.45% +/- 0.29% TPU(2 sigma)
390
360
330
300
270
on
240
h
_i
o
o
210
1S0
150
120
90
60
30
0
-r
I ¦! rj'r^*
Th-232
ill
1-
i i i i i rL'i—r'T V- l '-i
Th-228
a!
T
i-n r'
f
1 I I I I I I I I
3374 3674 3974 4274 4574 4S74 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV}
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:36PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Thorium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
66.1
100.2
136
0.4167
136.01
1.383E+000 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
40.2
99.7
2625
0.0000
2624.69
2.683E+001 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
87.0
99.6
1188
1.2500
1186.69
1.099E+001 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
51.6
99.8
135
5.4528
129.48
1.323E+000 pCi/g
Page 144 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-1-D Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-1-D
Sample Collection Date: 6/10/2016 6:35:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170137
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV151 SN: 50-05/R5
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:34PM
Bkgd Info: Sample: ICB;AV151; Det: AV151; Spectrum #1; 6/24/2016
4:15:34 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:57:39PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 89.05%
Energy Calibration: IC-8877;AV151-20151016
Efficiency Calibration:IC-8877;AV151-20151016
Calibration Date: 10/16/2015 6:46:50PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.28% +/- 0.31% TPU(2 sigma)
130 -
120 ¦
110 -
100 ¦
90 ¦
SO ¦
70 ¦
60 -
50
40
30
20
10 H
(f>
c
=i
o
o
Th-232
1-^
~i i i i i i i i ii i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i n
3374 3674 3974 4274 4574 4S74 5174 5474 5774 6074 6374 6674 6974 7274 7574
Th-230
Th-229
¦f
Energy (keV}
Gen eraI Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:35PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Thorium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
64.0
100.2
208
0.0000
208.00
1.037E+000 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
35.1
99.7
705
0.4167
704.77
3.530E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
84.3
99.6
1207
0.8333
1206.04
5.384E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
65.8
99.8
208
6.6667
201.33
1.008E+000 pCi/g
Page 145 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-1-D Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-1-D
Sample Collection Date: 6/10/2016 6:35:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170218
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV151 SN: 50-05/R5
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:34PM
Bkgd Info: Sample: ICB;AV151; Det: AV151; Spectrum #1; 6/24/2016
4:15:34 PM
8:33:30AM
7/5/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 88.76%
Energy Calibration: IC-8877;AV151-20151016
Efficiency Calibration:IC-8877;AV151-20151016
Calibration Date: 10/16/2015 6:46:50PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.28% +/- 0.31% TPU(2 sigma)
130 -
120 ¦
110 -
100 ¦
90 ¦
SO ¦
70 ¦
60 -
50
40
30
20
10 H
(f>
c
=i
o
o
Th-232
1-^
~i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i-
3374 3674 3974 4274 4574 4S74 5174 5474 5774 6074 6374 6674 6974 7274 7574
Th-230
Th-229
Th-228
¦f
Analysis Method: Absolute Interactive ROI Analysis
Decay Correction:7/2/2016 3:14:35PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Energy (keV}
Gen eraI Analysis
Nuclide Library: Thorium
MDA Source: Background
Manual Integration for
tailing. 07/05/2016 ALD
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-229
4848.0
4,845.3
2.7
4739.1
5119.5
84.3
99.6
1203
0.8333
1202.17
5.366E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
65.8
99.8
208
6.6667
201.33
1.011E+000 pCi/g
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
64.0
100.2
208
0.0000
208.00
1.040E+000 pCi/g
Th-230
4688.0
4,687.5
0.5
4448.3
4739.1
44.8
99.7
709
0.4167
708.58
3.561 E+000 pCi/g
Page 146 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-1-E DU Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-1-E DU
Sample Collection Date: 6/10/2016 6:35:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170140
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV152 SN: 50-05/R6
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.01 min.
Background Date: 6/26/2016 5:10:10PM
Bkgd Info: Sample: ICB;AV152; Det: AV152; Spectrum #4; 6/26/2016
5:10:10 PM
9:58:16PM
7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 88.88%
Energy Calibration: IC-9520;AV152-20151016
Efficiency Calibration:IC-9520;AV152-20151016
Calibration Date: 10/16/2015 6:46:53PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.54% +/- 0.35% TPU(2 sigma)
110 -
100 -
90 -
80 -
® 70 -
"E
8 60 -
50 -
40 -
30 -
20 -
10 -
0 -
3374 3674 3974 4274 4574 4574 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV}
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:35PM Nuclide Library: Thorium
MDA Constants: Ka = 1.64 , K(3 = 1.64 MDA Source: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
51.9
100.2
179
0.4167
178.58
9.194E-001 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
23.7
99.7
673
0.4167
672.65
3.480E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
81.7
99.6
1170
1.2500
1168.81
5.379E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
50.9
99.8
191
4.5833
186.42
9.640E-001 pCi/g
Th-232
k
J
I
A
rt i
Th-229
Th-23G |'|
A
Th-228
1 1 n1
.¦./¦Alt', All ,rr>', . A. . r,. A .
I I
I I
Page 147 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-2-C Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-2-C
Sample Collection Date: 6/10/2016 6:40:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170142
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV153 SN: 54-011 Y6
Acquisition Start Date: 7/2/2016 3:17:11PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:17PM
Bkgd Info: Sample: ICB;AV153; Det: AV153; Spectrum #1; 6/24/2016
4:15:17 PM
9:58:38PM
7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 82.59%
Energy Calibration: IC-9792;AV153-20151016
Efficiency Calibration:IC-9792;AV153-20151016
Calibration Date: 10/16/2015 6:46:57PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 26.60% +/- 0.31% TPU(2 sigma)
3374 3674 3974 4274 4574 4674 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV}
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:35PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Thorium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
61.9
100.2
231
0.0000
231.43
1.186E+000 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
30.2
99.7
549
0.8333
548.14
2.822E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
83.0
99.6
1178
0.8333
1177.14
5.009E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
70.4
99.8
212
3.7500
208.25
1.072E+000 pCi/g
Page 148 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-3-C Type: Sample
Spectrum #2 Analysis #1
: 160-17814-A-3-C
Sample Collection Date: 6/10/2016 6:50:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170665
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV199 SN: 50-117Z3
Acquisition Start Date: 7/7/2016 1:10:54PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:21PM
Bkgd Info: Sample: ICB;AV199; Det: AV199; Spectrum #1; 6/24/2016
4:15:21 PM
8:01:37PM
7/7/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 128.63%
Energy Calibration: IC-9817;AV199-20151017
Efficiency Calibration:IC-9817;AV199-20151017
Calibration Date: 10/18/2015 3:55:29PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.71% +/- 0.30% TPU(2 sigma)
Of)
"E
=i
o
o
Energy (keV}
Gen eraI Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:36PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Thorium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
60.4
100.2
145
0.4167
144.27
5.100E-001 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
53.9
99.7
637
0.8462
635.83
2.259E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
71.4
99.6
1704
0.8462
1703.15
7.788E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
52.3
99.8
167
7.5361
159.40
5.687E-001 pCi/g
Page 149 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-3-C Type: Sample
Spectrum #2 Analysis #1
: 160-17814-A-3-C
Sample Collection Date: 6/10/2016 6:50:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170687
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV199 SN: 50-117Z3
Acquisition Start Date: 7/7/2016 1:10:54PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:21PM
Bkgd Info: Sample: ICB;AV199; Det: AV199; Spectrum #1; 6/24/2016
4:15:21 PM
8:11:08AM
7/8/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 136.10%
Energy Calibration: IC-9817;AV199-20151017
Efficiency Calibration:IC-9817;AV199-20151017
Calibration Date: 10/18/2015 3:55:29PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.71% +/- 0.30% TPU(2 sigma)
Of)
"E
=i
o
o
140
130 ¦
120 -
110 -
100 ¦
90 ¦
SO
70 -
60 ¦
50 -
40
30 ¦
20 ¦
10
0
Analysis Method: Absolute Interactive ROI Analysis
Decay Correction:7/2/2016 3:14:36PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Energy (keV}
Gen eraI Analysis
Nuclide Library: Thorium
MDA Source: Background
Manual Integration for
tailing. 07/08/2016 ALD
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
60.4
100.2
145
0.4167
144.27
4.820E-001 pCi/g
Th-230
4552.7
4,687.5
-134.8
4448.3
4657.1
39.8
99.7
538
0.8333
537.17
1.804E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4657.1
5119.5
72.5
99.8
1806
1.2500
1804.75
8.240E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
52.3
99.8
167
7.5361
159.40
5.375E-001 pCi/g
Page 150 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
Sample
Sample Name: 160-17814-A-4-C Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-4-C
Sample Collection Date: 6/10/2016 7:00:00AM
Comment:
Batch Name: 257492
AnalysisResultsID: 170139
Description:
Batch
Tracer
Tracer Name: Th-229_00020
Tracer Activity: 67.23 DPM/mLx (Vol.) 0.20 ml_= 13.45 DPM
Tracer Ref. Date: 8/6/2014 1:28:22PM
Acquisition
Detector: AV155 SN: 50-05/111
Acquisition Start Date: 7/2/2016 3:17:12PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/26/2016 5:10:11PM
Bkgd Info: Sample: ICB;AV155; Det: AV155; Spectrum #4; 6/26/2016
5:10:11 PM
9:58:04PM
7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: Th-229
Tracer Recovery: 89.24%
Energy Calibration: IC-9794;AV155-20151016
Efficiency Calibration:IC-9794;AV155-20151016
Calibration Date: 10/16/2015 6:47:03PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.17% +/- 0.31% TPU(2 sigma)
110
Of)
"E
=i
o
o
100 -
90 -
SO -
70 ¦
60 -
50 ¦
40 -
30 ¦
20 -
10 ¦
Th-232
..>A- ---A
Energy (keV}
Gen eraI Analysis
Analysis Method: Absolute ROI Analysis, Set Name = Th2007_ROI
Decay Correction:7/2/2016 3:14:36PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Thorium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
Th-232
3999.0
4,010.0
-11.0
3743.0
4072.0
55.9
100.2
213
0.0000
213.00
1.106E+000 pCi/g
Th-230
4688.0
4,687.5
0.5
4446.0
4717.0
20.5
99.7
723
0.0000
723.22
3.775E+000 pCi/g
Th-229
4848.0
4,845.3
2.7
4717.0
5119.0
77.6
99.6
1156
0.0533
1155.79
5.387E+000 pCi/g
Th-228
5420.0
5,423.3
-3.3
5119.0
5493.0
47.9
99.8
212
5.8866
206.05
1.075E+000 pCi/g
Page 151 of 551
-------
Method A-01-R U
Isotopic Uranium (Alpha
Spectrometry) by Method A-01-R
Page 152 of 551
-------
Prep Batch: 257935
Preparation, Extraction
Chromatography Resin Actinide
Separation
Page 153 of 551
-------
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257935
Lab ID: MB 160-257935/1 -A
Client ID:
Sigma: 2
Analyzed: 07/02/16 15:31
Detector: AV235
Dil Fac: 1
Decay Corrected: No
Yield Truncated: No
Is: 400
Analyte
MB Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Uranium-233/234
0.03094
0.0277
0.0278
pCi/g
0.0186
0.00782
259144
Uranium-235/236
-0.006417
0.00908
0.00909
U
pCi/g
0.0506
0.0138
259144
Uranium-238
0.006176
0.0124
0.0124
U
pCi/g
0.0185
0.00781
259144
Tracer
MB Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added
% Rec % Rec Limits
Uranium-232
5.043
0.298
0.518
pCi/g
0.0124
7.41
71.3 30-110
Lab ID: LCS 160-257935/2-A
Client ID:
Sigma: 2
Analyzed: 07/02/16 15:31
Detector: AV236
Dil Fac: 1
Decay Corrected: No
Yield Truncated: No
Is: 400
Analyte LCS Result Count Unc Total Unc Qualifier Unit
Uranium-233/234 6.283 0.381 0.651 pCi/g
Uranium-238 6.600 0.390 0.678 pCi/g
Tracer LCS Result Count Unc Total Unc Qualifier Unit
Uranium-232 5.650 0.323 0.574 pCi/g
MDC
DLC Anly Batch
0.0426 0.0126 259145
0.0173 0.00728 259145
DLC Spike Added % Rec % Rec Limits
0.0101 7\4l 79.9 30-110
Lab ID: 160-17314-1
Client ID: AC-SED-4
Sigma: 2
Analyzed: 07/02/16 15:31
Detector: AV237
Dil Fac: 1
Decay Corrected: No
Yield Truncated: No
Ts: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Uranium-233/234
0.767
0.136
0.151
pCi/g
0.0478
0.0150 259146
Uranium-235/236
0.0517
0.0391
0.0393
pCi/g
0.0222
0.00933 259146
Uranium-238
0.805
0.138
0.154
pCi/g
0.0178
0.00748 259146
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec % Rec Limits
Uranium-232
5.18
0.300
0.529
pCi/g
0.0123
7.40 73.4 30-110
Lab ID: 160-17314-1 DU
Client ID: AC-SED-4
Sigma: 2
Analyzed: 07/02/16 15:31
Detector: AV238
Dil Fac: 1
Decay Corrected: No
Yield Truncated: No
Ts: 400
Analyte
DU Result Count Unc Total Unc Qualifier Unit
Uranium-233/234
Uranium-235/236
Uranium-238
0.7844
0.01978
0.8740
0.147
0.0367
0.155
0.161
0.0368 U
0.171
pCi/g
pCi/g
pCi/g
MDC
0.0448
0.0683
0.0376
DLC Anly Batch
259147
259147
259147
0.0122
0.0214
0.00859
Page 1 of 3
TestAmerica St. Louis
Page 154 of 551
-------
Tracer
DU Result Count Unc Total Unc Qualifier Unit
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257935
Spike Added % Rec % Rec Limits
DLC
Uranium-232
4.617
0.287
0.482
pCi/g
0.0112
7.40 65.3
30-110
Lab ID: 160-17814-2
Client ID: AC-SED-6
Sigma: 2
Analyzed
Detector:
Dil Fac:
: 07/02/16
AV239
1
15:31
Decay Corrected: No
Yi icated: No
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Uranium-233/234
0.657
0.123
0.134
pCi/g
0.0314
0.00719 259148
Uranium-235/236
0.0425
0.0347
0.0348
pCi/g
0.0212
0.00894 259148
Uranium-238
0.821
0.137
0.153
pCi/g
0.0314
0.00717 259148
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Uranium-232
5.62
0.318
0.569
pCi/g
0.00985
7.42 79.3
30-110
Lab ID:
Client ID: AC-SED-7
Sigma: 2
Analyzed
Detector:
Dil Fac:
: 07/02/16
AV240
1
15:31
Decay Corrected: No
Yi icated: No
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Uranium-233/234
0.513
0.114
0.122
pCi/g
0.0410
0.0112 259149
Uranium-235/236
0.0311
0.0311
0.0312
pCi/g
0.0233
0.00982 259149
Uranium-238
0.789
0.140
0.155
pCi/g
0.0344
0.00787 259149
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Uranium-232
4.77
0.284
0.491
pCi/g
0.00920
7.41 67.5
30-110
Lab ID:
Client ID: AC-SED-8
Sigma: 2
Analyzed
Detector:
Dil Fac:
: 07/02/16
AV241
1
15:31
Decay Corrected: No
Yi icated: No
Is: 400
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC Anly Batch
Uranium-233/234
0.757
0.143
0.157
pCi/g
0.0533
0.0167 259150
Uranium-235/236
0.0330
0.0330
0.0331
pCi/g
0.0247
0.0104 259150
Uranium-238
0.826
0.148
0.163
pCi/g
0.0198
0.00835 259150
Tracer
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Spike Added % Rec
% Rec Limits
Uranium-232
4.85
0.297
0.504
pCi/g
0.00574
7.39 68.8
30-110
Page 2 of 3
Page 155 of 551
TestAmerica St. Louis
-------
Alpha Spectroscopy Analysis Detail Report
Prep Batch: 257935
Quail ntrol Summary
Method Blank ID:
Analyte
Parent Result
Spike Added
MB Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER
RER Limit
Z Factor
MB 160-257935/1-A
Uranium-233/234
0.03094
pCi/g
2.226271
67
-1.411725
45
.9991191
7
MB 160-257935/1-A
Uranium-235/236
-0.006417
U
pCi/g
MB 160-257935/1-A
Uranium-238
0.006176
U
pCi/g
Lab Control Sample ID:
Analyte
Parent Result
Spike Added
LCS Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER
RER Limit
Z Factor
LCS 160-257935/2-A Uranium-233/234 6.37 6.283 pCi/g 99 84-120 -.1840500
64
LCS 160-257935/2-A Uranium-238 6.51 6.600 pCi/g 101 82-122 .1889105
392
Duplicate ID:
Analyte
Parent Result Spike Added
DU Result
Qualifier
Unit
% Rec % Rec Limits
RPD
RER
DER
RER Limit Z Factor
160-17814-1
Uranium-233/234
0.767
0.7844
pCi/g
2
0.05
0.15
1
160-17814-1
Uranium-235/236
0.0517
0.01978
U
pCi/g
89
0.42
1.19
1
160-17814-1
Uranium-238
0.805
0.8740
pCi/g
8
0.21
0.60
1
Glossary:
Ts = Count Duration, Sample
Page 3 of 3 TestAmerica St. Louis
Page 156 of 551
-------
ALPHA SPECTROSCOPY BATCH WORKSHEET
Lab Name: TestAmerica St. Louis Job No.: 160-17814-1
SDG No.:
Batch Number: 257935 Batch Start Date: 06/24/16 15:54 Batch Analyst: Bernsen, Sarah C
Batch Method: ExtChrom Batch End Date: 07/01/16 16:21
Lab Sample ID
Client Sample ID
Method Chain
Basis
InitialAmount
U-232 00034
UNAT 00012
MB 160-257935/1
ExtChrom,
A-01-R
1. 0 g
0.2 mL
LCS
160-257935/2
ExtChrom,
A-01-R
1. 0 g
0.2 mL
0.2 mL
160-17814-A-l-A
AC-SED-4
ExtChrom,
A-01-R
T
1. 0018 g
0.2 mL
160-17814-A-l-A
DU
AC-SED-4
ExtChrom,
A-01-R
T
1.0008 g
0.2 mL
160-17814-A-2-A
AC-SED-6
ExtChrom,
A-01-R
T
0.9986 g
0.2 mL
160-17814-A-3-A
AC-SED-7
ExtChrom,
A-01-R
T
1.0003 g
0.2 mL
160-17814-A-4-A
AC-SED-8
ExtChrom,
A-01-R
T
1.0033 g
0.2 mL
Batch Notes
Balance ID
27050421
Analyst ID - Column
nmn per scb
Column Date
7/1/16
Analyst ID - CoPrecipitation
scb
CoPrecipitation Date
7/1/16
Pipette ID
Radl04
Analyst ID - Reagent Drop Witness
rj s per scb
Analyst ID - Reagent Drop
scb
SOP Number
ST-RC-0 0 03, ST-RC-0004, ST-RC-0100, ST-RC-0242
Basis
Basis Description
T
Total/NA
The pound sign (#) in the amount added field denotes that the reagent was
this reagent.
A-01-R
used undiluted. All calculations are performed using the stated concentration for
Page 1 of 1
Page 157 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: MB 160-257935/1-A
Spectrum #1 Analysis #1
: MB 160-257935/1-A
Sample Collection Date: 7/1/2016 4:42:00PM
Comment:
Batch Name: 257935
AnalysisResultsID: 170198
Description:
Type: Blank
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV235 SN: 51-005Q5
Acquisition Start Date: 7/2/2016 3:31:33PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:28PM
Bkgd Info: Sample: ICB;AV235; Det: AV235; Spectrum #1; 6/24/2016
4:15:28 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:14:41PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 71.32%
Energy Calibration: IC-8877;AV235-20151018
Efficiency Calibration:IC-8877;AV235-20151018
Calibration Date: 10/19/2015 4:11:39PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.57% +/- 0.31% TPU(2 sigma)
Of)
"E
=i
o
o
150 -
140 ¦
130
120 H
110
100 ¦
90 -
SO ¦
70
60 ¦
50 -
40 ¦
30 -
20
10
0
U-238
U-235
U-234
I
U-232
I I I'' T I* I 11 ' fcH|l I ' I' I I 1 I I ' I I I 11 I I I 1 I I I
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:42PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Energy (keV}
Gen eraI Analysis
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
44.5
100.0
1
0.0000
1.00
6.176E-003 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
.0
80.2
0
0.8333
-0.83
-6.417E-003 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
96.6
99.8
5
0.0000
5.00
3.094E-002 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
65.2
100.1
1148
2.0833
1145.92
5.285E+000 pCi/g
Page 158 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: LCS 160-257935/2-A
Spectrum #1 Analysis #1
: LCS 160-257935/2-A
Sample Collection Date: 7/1/2016 4:42:00PM
Comment:
Batch Name: 257935
AnalysisResultsID: 170201
Description:
Type: Control
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV236 SN: 51-005P3
Acquisition Start Date: 7/2/2016 3:31:34PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:30PM
Bkgd Info: Sample: ICB;AV236; Det: AV236; Spectrum #1; 6/24/2016
4:15:30 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:15:41PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 79.90%
Energy Calibration: IC-9520;AV236-20151018
Efficiency Calibration:IC-9520;AV236-20151018
Calibration Date: 10/19/2015 4:11:44PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.47% +/- 0.34% TPU(2 sigma)
Of)
"E
=i
o
o
150 -
140 ¦
130
120 H
110
100 ¦
90 -
SO ¦
70
60 ¦
50 -
40 ¦
30 -
20
10
0
U-23S
U-235
U-234
U-232
d I
i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i i r~
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Energy (keV}
Gen eraI Analysis
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
79.7
100.0
1146
0.0000
1146.00
S.600E+000 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
61.4
80.2
41
0.4167
40.58
2.914E-001 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
75.6
99.8
1090
1.2500
1088.75
S.283E+000 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
81.9
100.1
1230
1.2500
1228.75
5.920E+000 pCi/g
Page 159 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-1-F Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-1-F
Sample Collection Date: 6/10/2016 6:35:00AM
Comment:
Batch Name: 257935
AnalysisResultsID: 170200
Description:
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV237 SN: 50-120DD7
Acquisition Start Date: 7/2/2016 3:31:34PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:29PM
Bkgd Info: Sample: ICB;AV237; Det: AV237; Spectrum #1; 6/24/2016
4:15:29 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:15:21PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 73.36%
Energy Calibration: IC-9792;AV237-20151018
Efficiency Calibration:IC-9792;AV237-20151018
Calibration Date: 10/19/2015 4:11:48PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.87% +/- 0.30% TPU(2 sigma)
160 -
150 -
140 ¦
130 -
120 ¦
110 -
100 -
r
n
90 ¦
O
80 -
70 -
60 ¦
50 -
40 ¦
30 ¦
20 -
10 ¦
0 -
\ I I I I l
U-235
iu-
T"T
U-234
)
U-232
I I I I I I I I I
T-
i i i i i i
i i i
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV}
General Analysis
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
60.5
100.0
136
0.0000
136.00
8.054E-001 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
18.3
80.2
7
0.0000
7.00
5.169E-002 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
89.5
99.8
131
1.6667
129.33
7.674E-001 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
74.3
100.1
1195
2.0833
1192.92
5.426E+000 pCi/g
Page 160 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-1-G DU Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-1 -G DU
Sample Collection Date: 6/10/2016 6:35:00AM
Comment:
Batch Name: 257935
AnalysisResultsID: 170202
Description:
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV238 SN: 51-005P7
Acquisition Start Date: 7/2/2016 3:31:34PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:30PM
Bkgd Info: Sample: ICB;AV238; Det: AV238; Spectrum #1; 6/24/2016
4:15:30 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:16:01PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 65.35%
Energy Calibration: IC-9793;AV238-20151018
Efficiency Calibration:IC-9793;AV238-20151018
Calibration Date: 10/19/2015 4:11:53PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.33% +/- 0.31% TPU(2 sigma)
130 -
120 -
110 -
100 -
90 -
¦§ SO -
=i
o
° 70 -
60 -
50 -
40 -
30 -
20 -
10 -
0 -
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV}
General Analysis
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM Nuclide Library: Uranium
MDA Constants: Ka = 1.64 , K(3 = 1.64 MDA Source: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
77.0
100.0
129
0.4167
128.58
8.740E-001 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
27.9
80.2
4
1.6667
2.33
1.978E-002 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
93.6
99.8
116
0.8333
115.17
7.844E-001 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
65.5
100.1
1042
1.6667
1040.33
4.838E+000 pCi/g
-I—r
U-23S
J
-A
U-235
—
U-234
/.if I
"i—r1
U-232
i
h—i—Lr
\ i
i i
Page 161 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-2-D Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-2-D
Sample Collection Date: 6/10/2016 6:40:00AM
Comment:
Batch Name: 257935
AnalysisResultsID: 170204
Description:
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV239 SN: 51-005EE1
Acquisition Start Date: 7/2/2016 3:31:34PM
Live Time: 400.00 min.
Real Time: 400.06 min.
Background Date: 6/24/2016 4:15:30PM
Bkgd Info: Sample: ICB;AV239; Det: AV239; Spectrum #1; 6/24/2016
4:15:30 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:16:43PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 79.35%
Energy Calibration: IC-9794;AV239-20151018
Efficiency Calibration:IC-9794;AV239-20151018
Calibration Date: 10/19/2015 4:11:57PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 25.04% +/- 0.32% TPU(2 sigma)
160 -
150 -
140 ¦
130 -
120 ¦
110 -
100 -
r
n
90 ¦
O
80 -
70 -
60 ¦
50 -
40 ¦
30 ¦
20 -
10 ¦
0 -
U-233
\ I I I I I
4=-
U-235
1t-
U-234
i U-232
I 'f*
1 I I I I
-f-
I I I I I I I I I
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV}
General Analysis
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
67.4
100.0
145
0.4167
144.58
8.205E-001 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
19.5
80.2
6
0.0000
6.00
4.246E-002 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
69.0
99.8
116
0.4167
115.58
6.573E-001 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
70.7
100.1
1250
1.2500
1248.75
5.887E+000 pCi/g
Page 162 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-3-D Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-3-D
Sample Collection Date: 6/10/2016 6:50:00AM
Comment:
Batch Name: 257935
AnalysisResultsID: 170197
Description:
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV240 SN: 51-005Q1
Acquisition Start Date: 7/2/2016 3:31:35PM
Live Time: 400.00 min.
Real Time: 400.00 min.
Background Date: 6/24/2016 4:15:30PM
Bkgd Info: Sample: ICB;AV240; Det: AV240; Spectrum #1; 6/24/2016
4:15:30 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:14:22PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 67.54%
Energy Calibration: IC-9795;AV240-20151018
Efficiency Calibration:IC-9795;AV240-20151018
Calibration Date: 10/19/2015 4:12:02PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 26.76% +/- 0.35% TPU(2 sigma)
130 -
120 -
110 -
100 -
90 -
¦§ SO -
=i
o
° 70 -
60 -
50 -
40 -
30 -
20 -
10 -
0 -
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV}
General Analysis
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM Nuclide Library: Uranium
MDA Constants: Ka = 1.64 , K(3 = 1.64 MDA Source: Background
Nuclide Summary (ROI)
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
63.8
100.0
127
0.4167
126.58
7.885E-001 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
70.8
80.2
4
0.0000
4.00
3.107E-002 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
61.0
99.8
83
0.8333
82.17
5.129E-001 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
78.0
100.1
1137
1.2500
1135.75
5.003E+000 pCi/g
U-23S
J
1 'Y' i
U-235
U-234
ML
1 U-232
I I
-i—r
i i
i i
Page 163 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Alpha-Spectroscopy
Analysis Report
Sample
Sample Name: 160-17814-A-4-D Type: Sample
Spectrum #1 Analysis #1
: 160-17814-A-4-D
Sample Collection Date: 6/10/2016 7:00:00AM
Comment:
Batch Name: 257935
AnalysisResultsID: 170205
Description:
Batch
Tracer
Tracer Name: U-232_00034
Tracer Activity: 82.25 DPM/mLx (Vol.) 0.20 ml_= 16.45 DPM
Tracer Ref. Date: 8/25/2011 4:14:20PM
Acquisition
Detector: AV241 SN: 50-005P1
Acquisition Start Date: 7/2/2016 3:31:35PM
Live Time: 400.00 min.
Real Time: 400.05 min.
Background Date: 6/24/2016 4:15:31PM
Bkgd Info: Sample: ICB;AV241; Det: AV241; Spectrum #1; 6/24/2016
4:15:31 PM
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:17:03PM 7/2/2016
Sample Weight: 1.00
First Stage Dilution: N/A
Aliquot: N/A Aliquot Fraction: N/A
Dilution 2: N/A
Lab Preparation:
Sample Units: g
Client Name: Undefined
Client Contact:
Analyst: 60040
Tracer Nuclide: U-232
Tracer Recovery: 68.76%
Energy Calibration: IC-9817;AV241-20151018
Efficiency Calibration:IC-9817;AV241 -20151018
Calibration Date: 10/19/2015 4:12:06PM
Energy Cal: Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Efficiency: 24.71% +/- 0.30% TPU(2 sigma)
Of)
"E
=i
o
o
140
130 ¦
120 -
110 -
100 ¦
90 ¦
SO
70 -
60 ¦
50 -
40
30 ¦
20 ¦
10
0
U-23S
J
1 I i i i I I I I I I I I I I I I I I I I I I I I I I I I I I i i r~
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
U-235
U-234
¦T-
I
U-232
H-
Analysis Method: ROI Analysis, Set Name = UROI
Decay Correction:7/2/2016 3:29:41PM
MDA Constants: Ka = 1.64 , K(3 = 1.64
Energy (keV}
Gen eraI Analysis
Nuclide Library: Uranium
MDA Source: Background
Nuclide Summary (ROI) 1
Peak
Peak
Peak
ROI
ROI
Energy
Expected
Diff
Start
End
FWHM
B.R.
Gross
Bkgd
Net
Nuclide
keV
keV
keV
keV
keV
keV
%
Counts
Counts
Counts
Activity Units
U-238
4157.5
4,196.0
-38.5
3956.1
4261.9
54.0
100.0
125
0.0000
125.00
8.259E-001 pCi/g
U-235
4381.2
4,396.0
-14.8
4269.3
4470.7
134.2
80.2
4
0.0000
4.00
3.295E-002 pCi/g
U-234
4776.4
4,775.8
0.6
4530.3
4851.0
64.3
99.8
116
1.6667
114.33
7.569E-001 pCi/g
U-232
5343.2
5,320.3
22.9
5097.1
5410.3
64.9
100.1
1068
0.4167
1067.58
5.078E+000 pCi/g
Page 164 of 551
-------
Daily Checks
Page 165 of 551
-------
Alpha Spectroscopy Daily Pulser Check
Analysis Date )2/16
Detector
Analysis Date
Gross Counts
FWHM (keV)
Pulser Center
Energy (keV)
Result
Criteria
P/F
Result
Criteria
P/F
Result
Criteria
P/F
Result
Criteria
P/F
AV148
07/02/16
12
40
6013
5686.2-6284.7
Pass
14.4
10-20
Pass
222.0
218.0-228.0
Pass
5023
4990.0-5070.0
Pass
AV150
07/02/16
11
53
6010
5623.0-6214.9
Pass
14.5
10-20
Pass
224.0
219.0-229.0
Pass
5038
4997.7-5077.7
Pass
AV151
07/02/16
11
53
5839
5640.3-6234.1
Pass
12.6
10-20
Pass
222.0
217.0-227.0
Pass
5022
4982.2-5062.2
Pass
AV152
07/02/16
11
53
5816
5683.1-6281.3
Pass
12.7
10-20
Pass
224.0
218.9-228.9
Pass
5038
4996.9-5076.9
Pass
AV153
07/02/16
11
53
5995
5694.3-6293.7
Pass
15.9
10-20
Pass
223.0
218.0-228.0
Pass
5030
4989.9-5069.9
Pass
AV155
07/02/16
11
53
5809
5702.4-6302.6
Pass
12.7
10-20
Pass
222.0
216.5-226.5
Pass
5023
4978.5-5058.5
Pass
AV235
07/02/16
11
53
6028
5703.8-6304.2
Pass
13.4
10-20
Pass
223.0
218.0-228.0
Pass
5030
4990.0-5070.0
Pass
AV236
07/02/16
11
53
6029
5514.1-6094.6
Pass
14.6
10-20
Pass
223.1
217.6-227.6
Pass
5030
4987.2-5067.2
Pass
AV237
07/02/16
11
53
6019
5531.5-6113.7
Pass
14.0
10-20
Pass
221.9
217.1-227.1
Pass
5022
4983.5-5063.5
Pass
AV238
07/02/16
11
53
5977
5718.5-6320.5
Pass
16.3
10-20
Pass
221.9
217.2-227.2
Pass
5022
4984.2-5064.2
Pass
AV239
07/02/16
11
53
5653
5505.4-6084.9
Pass
13.6
10-20
Pass
223.1
217.3-227.3
Pass
5031
4984.8-5064.8
Pass
AV240
07/02/16
11
53
6034
5521.1-6102.2
Pass
13.4
10-20
Pass
223.0
218.1-228.1
Pass
5030
4991.0-5071.0
Pass
AV241
07/02/16
11
53
5641
5544.0-6127.6
Pass
13.4
10-20
Pass
224.1
218.1-228.1
Pass
5038
4990.6-5070.6
Pass
Analysis
Date: 07/07/16
Gross Counts
FWHM (keV)
Pulser Center
Energy (keV)
Detector
Analysis Date
Result
Criteria
P/F
Result
Criteria
P/F
Result
Criteria
P/F
Result
Criteria
P/F
AV199
07/07/16
08:33
6003
5584.5-6172.3
Pass
19.0
10-20
Pass
217.9
214.0-224.0
Pass
4992
4959.9-5039.9
Pass
Page 1 of 1
Page 166 of 551
TestAmerica St. Louis
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV148
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:41:30PM 7/2/2016
Spectrum #6 Analysis #1
Batch Name: June2016a
Description:
Detector: AV148 , SN: 50-05/R2
Acquisition Start Date: 7/2/2016 12:40:23PM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-8874;AV148-20151016a
Calibration Date: 10/16/2015 6:47:19PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Mm -
320-0 -
290 C -
270C -
2 5 C C -
2200 -
m
"E
-i
2000 -
o
o
1SCC -
1600 -
1300 :
1100 -
900 -
700 -
400 :
200 -
0 -
-r""T—i—i—i—i—i—i—i—i—i—i—r
3374 3674 3974 4274 4574 4874 5174 5474 5774 6074
Energy (keV)
l—i—i—i—i—i—r
6374 6674 6974
-i—i—i—i—r
7274 7574
Analysis Method: Peak Fit Analysis
General Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser
5022.714 4998.249 5047.180
14.37
6,008.26
6,013.09
Page 167 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV150
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:08:26PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016a
Description:
Detector: AV150 , SN: 50-05/R4
Acquisition Start Date: 7/2/2016 11:53:36AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-8876;AV150-20151016
Calibration Date: 10/16/2015 6:46:46PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Mm -
320-0 -
290 C -
270C -
2 5 C C -
2200 -
m
"E
-i
2000 -
o
o
1SCC -
1600 -
1300 :
1100 -
900 -
700 -
400 :
200 -
0 -
-r-i—i—i—i—i—i—i—i—i—i—r
3374 3674 3974 4274 4574 4874 5174 5474 5774 6074
Energy (keVJ
i—i—|—|—|—r
6374 6674
n—i—i—i—i—i—r
6974 7274 7574
Analysis Method: Peak Fit Analysis
General Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser
5037.715 5013.004 5062.425
14.52
6,072.51
6,009.79
Page 168 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV151
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:08:22PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016a
Description:
Detector: AV151 , SN: 50-05/R5
Acquisition Start Date: 7/2/2016 11:53:36AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-8877;AV151-20151016
Calibration Date: 10/16/2015 6:46:50PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3400 -
3100 :
2SCO :
2?CC -
2300 -
m
"E
-i
2000 -
o
u
1700 -
1400 :
1100 :
800 :
600 -
300 -
—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3374 3674 3974 4274 4574 4874 5174 5474 5774 6074 6374 6674 §§74 7274 7574
Energy (keV)
Analysis Method: Peak Fit Analysis
General Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser
5022.238 5000.834 5043.643
12.57
5,499.22
5,839.15
Page 169 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV152
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:08:17PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016a
Description:
Detector: AV152 , SN: 50-05/R6
Acquisition Start Date: 7/2/2016 11:53:36AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9520;AV152-20151016
Calibration Date: 10/16/2015 6:46:53PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
;;cc -
21CC -
2900 -
2600 -
2400 -
m
2100 :
b
j
n
1900 -
o
-
1700 -
liOC -
120C -
900 :
7CC -
ECC -
200 -
0 -
1—i—i—i—m—i—i—i—i—i—i—i—r
3374 3674 3974 4274 4574 4874 5174 5474 5774
Energy (te¥)
i—i—r
6074 6374
6674 6974
7274 7574
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5037.761 5016.110 5059.412 12.72 5,466.19 5,815.85
Page 170 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV153
Comment:
Batch Name: June2016a
Description:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:08:30PM 7/2/2016
Spectrum #5 Analysis #1
Detector: AV153 , SN: 54-011 Y6
Acquisition Start Date: 7/2/2016 11:53:36AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9792;AV153-20151016
Calibration Date: 10/16/2015 6:46:57PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3000 -
2800 -
2600 -
2400 -
22CC -
20GC -
m
V
1 see -
u
_
u
o
1 cCC -
14GC -
12CC -
10CC -
BOG -
SCO -
ACC -
20*0 -
0 -
3374
3674
3974 4274
4574
4874
5174 5474
Energy (key)
5774
6074
6374 6674
6974
7274
7574
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5029.921 5002.799 5057.043 15.93 5,917.83 5,995.02
Page 171 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV155
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:08:43PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016a
Description:
Detector: AV155 , SN: 50-05/111
Acquisition Start Date: 7/2/2016 11:53:37AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9794;AV155-20151016
Calibration Date: 10/16/2015 6:47:03PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
"E
u
o
o
2374
3674
3974
4274 4574
TT—i—r
4874 5174
i—i—i—i—i—i—i—i—i—r
5474 5774 6074 6374
1—i—i—i—i—i—r
6974 7274 7574
Energy (keV)
Analysis Method: Peak Fit Analysis
General Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser
5022.849 5001.173 5044.524
12.73
5,468.82
5,809.36
Page 172 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV199
Comment:
Batch Name: June2016b
Description:
n
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:02:44AM 7/7/2016
Spectrum #8 Analysis #1
Detector: AV199 , SN: 50-117Z3
Acquisition Start Date: 7/7/2016 8:33:54AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9817;AV199-20151017
Calibration Date: 10/18/2015 3:55:29PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2400 -
2200 -
2000 -
1800 -
1600 -
id
"E
1400 -
n
u
1200 -
1000 -
800 -
600 -
400 -
200 -
3374
3674
3974
4274 4574
4874
5174 5474
Energy (key)
5774
©0-74
6374
i—i—i—i—i—i—i—i—i—r
6674 6974 7274 7574
Analysis Method: Peak Fit Analysis
General Analysis
Nuclide
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
keV keV keV keV Area Counts
Pulser
4991.619 4959.281
5023.956
19.00
5,520.73
6,002.99
Page 173 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV235
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:14:27PM 7/2/2016
Spectrum #6 Analysis #1
Batch Name: June2016c
Description:
Detector: AV235 , SN: 51-005Q5
Acquisition Start Date: 7/2/2016 11:53:57AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-8877;AV235-20151018
Calibration Date: 10/19/2015 4:11:39PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3600 -
saw -
30*00 -
270-0 :
2400 :
m
"E
2100 :
n
u
1800 -
1500 :
1200 :
900 :
600 1
300 :
1—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r-^i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5029.844 5007.090 5052.597 13.37 6,023.76 6,027.90
Page 174 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV236
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:14:10PM 7/2/2016
Spectrum #6 Analysis #1
Batch Name: June2016c
Description:
Detector: AV236 , SN: 51-005P3
Acquisition Start Date: 7/2/2016 11:53:57AM
Live Time: 1.00 min.
Real Time: 1.01 min.
Calibration Name: IC-9520;AV236-20151018
Calibration Date: 10/19/2015 4:11:44PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
?ooc -
28CC -
2600 -
2400 -
2200 -
2000 -
"E
-i
1SCC -
o
u
1600 -
1-GC -
1200 -
1000 -
800 -
600 -
400 -
200 -
1—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy CtceV)
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5030.458 5005.617 5055.300 14.59 5,745.83 6,029.00
Page 175 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV237
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:14:33PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016c
Description:
Detector: AV237 , SN: 50-120DD7
Acquisition Start Date: 7/2/2016 11:53:57AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9792;AV237-20151018
Calibration Date: 10/19/2015 4:11:48PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3000 -
2800 -
2600 -
2400 -
22CC -
20GC -
m
V
1 see -
u
_
u
o
1 cCC -
14GC -
12CC -
10CC -
BOG -
SGC -
ACC -
20*0 -
0 -
t—i—i—i—i—i—i—i—i—i—i—i—i—i—i——i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (TceV)
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5021.625 4997.865 5045.384 13.96 5,180.14 6,019.17
Page 176 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV238
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:11:10PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016c
Description:
Detector: AV238 , SN: 51-005P7
Acquisition Start Date: 7/2/2016 11:53:58AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9793;AV238-20151018
Calibration Date: 10/19/2015 4:11:53PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 8774 6974 7174
Energy (keV)
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5021.743 4994.078 5049.409 16.25 5,445.99 5,977.25
Page 177 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV239
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:11:17PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016c
Description:
Detector: AV239 , SN: 51-005EE1
Acquisition Start Date: 7/2/2016 11:53:58AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9794;AV239-20151018
Calibration Date: 10/19/2015 4:11:57PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3000 -
2800 -
2600 -
2400 -
22CC -
20GC -
m
V
1 see -
u
_
u
o
1 cCC -
14GC -
12CC -
10CC -
BOG -
SGC -
ACC -
20*0 -
0 -
—!—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5031.039 5007.929 5054.149 13.58 5,067.67 5,653.49
Page 178 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV240
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:11:23PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016c
Description:
Detector: AV240 , SN: 51-005Q1
Acquisition Start Date: 7/2/2016 11:53:58AM
Live Time: 1.00 min.
Real Time: 1.01 min.
Calibration Name: IC-9795;AV240-20151018
Calibration Date: 10/19/2015 4:12:02PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3400 -
1—i—i—i—i—i—i—i—i—i—i—i—i—r-*i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV}
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5029.834 5007.016 5052.652 13.41 5,956.47 6,033.76
Page 179 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: Pulser;AV241
Comment:
Sample
Batch
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
12:12:00PM 7/2/2016
Spectrum #5 Analysis #1
Batch Name: June2016c
Description:
Detector: AV241 , SN: 50-005P1
Acquisition Start Date: 7/2/2016 11:53:58AM
Live Time: 1.00 min.
Real Time: 1.00 min.
Calibration Name: IC-9817;AV241-20151018
Calibration Date: 10/19/2015 4:12:06PM
Acquisition
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
?ooc -
28CC -
2600 -
2400 -
2200 -
2000 -
"E
-i
1SCC -
o
u
1600 -
1-GC -
1200 -
1000 -
800 -
600 -
400 -
200 -
3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (teV}
General Analysis
Analysis Method: Peak Fit Analysis
Nuclide Summary (Peak Search) ¦
Peak Start End
Energy Energy Energy FWHM Fit Gross
Nuclide keV keV keV keV Area Counts
Pulser 5038.108 5015.302 5060.914 13.40 5,242.35 5,640.97
Page 180 of 551
-------
Initial
Calibrations
Page 181 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:26:49PM 11/23/2015
Sample Name: IC-8874;AV148-20151016a
Description:
Detector: AV148
Certificate ID: 82233-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:47:19PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV148 , SN: 50-05/R2
Acquisition Start Date: 10/16/2015 4:27:06PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-8874;AV148-20151016:
Certification Date: 6/3/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.72% +/- 0.38% TPU(2 sigma)
34MM
2300
2cCC H
24CC
22CC ^
2CCC
I 1 see
Q
° icoe
1400
120C
100C
SCO
600
40#
200
0
Pu-230
Th-230
I
Am-241
_
i i i i i i i i i i i i r i rrT i i ¦ i i tttti tt i r i i i i f i i i i i i i i i i i i i i i i i i i i i
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.28
10,746.00
76.76
Pu-239
240
5,155.40
186
249
31.36
14,143.00
101.02
Am-241
284
5,485.70
249
303
32.16
11,206.00
80.04
Page 182 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
6:46:47PM 10/16/2015
Sample Name: IC-8876;AV150-20151016
Description:
Detector: AV150
Certificate ID: 82235-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:46:46PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV150 , SN: 50-05/R4
Acquisition Start Date: 10/16/2015 3:51:29PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-8876;AV150-20151016
Certification Date: 6/4/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.45% +/- 0.29% TPU(2 sigma)
2800
2600
2400
2200 H
200C
18CC
1SCC
1*0C -
1200 -
100C -
800 -
eco
40 C
200 4
Pu-239
I
Th-230
Am-241
0 H—i—i—i—i—i—i—i—i—i—i—r-i—fnn—i :i *T tt i i——i—r i—i—i—i—r-j—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—r
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.57
14,812.00
105.80
Pu-239
240
5,155.40
186
249
32.92
14,414.00
102.96
Am-241
284
5,485.70
249
303
34.04
14,906.00
106.47
Page 183 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
6:46:50PM 10/16/2015
Sample Name: IC-8877;AV151-20151016
Description:
Detector: AV151
Certificate ID: 82236-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:46:50PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV151 , SN: 50-05/R5
Acquisition Start Date: 10/16/2015 3:51:50PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-8877;AV151-20151016
Certification Date: 6/2/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.28% +/- 0.31% TPU(2 sigma)
320C
20CC H
28C0
2600
240-0 H
22CC
« 20CC
1 1 see
o
1?CC
1400
1200
100C
8CC -
ecc -
iOC
2CC
0
Th-230
a
i
Pu-239
a
J
M
Am-241
i—i—i—i—i—i—i—i—i—i—i—i——i IT i—rn—i—i "ft T "n i—it —i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—r
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.27
14,588.00
104.20
Pu-239
240
5,155.40
186
249
32.53
15,116.00
107.97
Am-241
284
5,485.70
249
303
33.58
14,215.00
101.54
Page 184 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:27:05PM 11/23/2015
Sample Name: IC-9520;AV152-20151016
Description:
Detector: AV152
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:46:53PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV152 , SN: 50-05/R6
Acquisition Start Date: 10/16/2015 3:52:05PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9520;AV152-20151016
2SCC -
2€GC
2400
2200 H
2000
1300 H
I 1600 -|
o
o
1400
1200 -|
1000
800
600
400
200
0
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.54% +/- 0.35% TPU(2 sigma)
Pu-239
Th-230
Am-241
1 1 1 1 1 1 1 1 1 1 1 1 I tT I I '1 1 nnprp-'| 1* | 1 1 f-| 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1—
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.71
11,699.00
83.56
Pu-239
240
5,155.40
186
249
33.73
13,727.00
98.05
Am-241
284
5,485.70
249
303
34.89
11,357.00
81.12
Page 185 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
6:46:57PM 10/16/2015
Sample Name: IC-9792;AV153-20151016
Description:
Detector: AV153
Certificate ID: 82240-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:46:57PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV153 , SN: 54-011 Y6
Acquisition Start Date: 10/16/2015 3:52:22PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9792;AV153-20151016
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.60% +/- 0.31% TPU(2 sigma)
320C
20CC H
28C0
2600
240-0 H
22CC
« 20CC
1 1 see
o
1?CC
1400
1200
100C
8CC -
ecc -
iOC
2CC
0
Pu-239
Am-241
Th-230
1 ! I I I I I I 1 ! 1 ! IT t f IT^T I I TT*"~T T-™! I I I I I I I I I I ! I ! I ! I ! I i I ! I I I I I T
1 21 41 61 81 111 141 171 201 2.M 261 2=1 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.79
13,953.00
99.66
Pu-239
240
5,155.40
186
249
34.07
16,216.00
115.83
Am-241
284
5,485.70
249
303
33.42
18,314.00
130.81
Page 186 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:27:13PM 11/23/2015
Sample Name: IC-9794;AV155-20151016
Description:
Detector: AV155
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/16/2015 6:47:03PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV155 , SN: 50-05/111
Acquisition Start Date: 10/16/2015 3:52:52PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9794;AV155-20151016
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.17% +/- 0.31% TPU(2 sigma)
2800
2600
2400
2200 H
20 OC
1800
12CC
KGC
12CC -
1000 -
300
600
400
200 ^
0
Am-241
Pu-239
Th-230
1—I—I—I—I—I—n—I—I—I—I -m* I ri'lT I l"ri——i—i—i—i——i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—1—|—i—i—i—r
1 21 41 61 81 111 141 171 201 221 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.44
13,390.00
95.64
Pu-239
240
5,155.40
186
249
30.32
13,163.00
94.02
Am-241
284
5,485.70
249
303
32.54
14,240.00
101.71
Page 187 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
3:55:30PM 10/18/2015
Sample Name: IC-9817;AV199-20151017
Description:
Detector: AV199
Certificate ID: 82244-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/18/2015 3:55:29PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV199 , SN: 50-117Z3
Acquisition Start Date: 10/17/2015 6:15:17PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9817;AV199-20151017
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.71% +/- 0.30% TPU(2 sigma)
34MM
2300
2cCC H
24CC
22CC ^
2CCC
I 1 see
Q
° icoe
1400
120C
100C
SCO
600
40#
200
0
Th-230
i—i—i—i—i—i—i—i—i—i—i—i——r TT i—m—i—rrTTTm—r i—i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—i
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
—r
Pu-239
Am-241
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.96
15,446.00
110.33
Pu-239
240
5,155.40
186
249
29.88
13,902.00
99.30
Am-241
284
5,485.70
249
303
29.92
14,059.00
100.42
Page 188 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:11:41PM 10/19/2015
Sample Name: IC-8877;AV235-20151018
Description:
Detector: AV235
Certificate ID: 82236-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:11:39PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV235 , SN: 51-005Q5
Acquisition Start Date: 10/18/2015 9:32:08PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-8877;AV235-20151018
Certification Date: 6/2/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.57% +/- 0.31% TPU(2 sigma)
34MM
2300
2cCC H
24CC
22CC ^
2CCC
I 1 see
Q
° icoe
1400
120C
100C
SCO
600
40#
200
0
Pu-239
Th-230
i—i—i—i—i—i—i—i—i—i—i—i——m—i—i "T i—it i r *r,Tii—i—i—r—i—i—i—i—r—i—i—i—i—i—i—i—i—i—i—i—i—i—i—
1 21 41 61 81 101 131 161 191 221 251 2J1 311 341 371 401 431 461 491
-r
Am-241
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.88
14,697.00
104.98
Pu-239
240
5,155.40
186
249
32.18
15,135.00
108.11
Am-241
284
5,485.70
249
303
30.94
14,563.00
104.02
Page 189 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:11:45PM 10/19/2015
Sample Name: IC-9520;AV236-20151018
Description:
Detector: AV236
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:11:44PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV236 , SN: 51-005P3
Acquisition Start Date: 10/18/2015 9:32:19PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9520;AV236-20151018
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.47% +/- 0.34% TPU(2 sigma)
20CG
ZBCC
2cCC -
2400 -
2200 -
2000
1300
15CC
140C -
12CG -
1CCC -
see
600
400
200 H
0
Pu-239
Th-230
Am-241
1 1 I [ 1 1 [ 1 I [ I i iTT I 1*1 I | -J | ! II I I " I 1 I II II III It II I
1 21 41 61 81 101 131 161 191 221 251 ¦ 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.26
11,521.00
82.29
Pu-239
240
5,155.40
186
249
31.34
13,821.00
98.72
Am-241
284
5,485.70
249
303
30.54
11,354.00
81.10
Page 190 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:11:50PM 10/19/2015
Sample Name: IC-9792;AV237-20151018
Description:
Detector: AV237
Certificate ID: 82240-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:11:48PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV237 , SN: 50-120DD7
Acquisition Start Date: 10/18/2015 9:32:32PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9792;AV237-20151018
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.87% +/- 0.30% TPU(2 sigma)
320C
20CC H
28C0
2600
240-0 H
22CC
« 20CC
1 1 see
o
1?CC
1400
1200
100C
8CC -
ecc -
iOC
2CC
0
Pu-239
Th-230
Am-241
i—i—i—i—i—i—i—i—i—i—i—i——i—i—i—i—r"i—i—rTT i T' i—i—i1 i—i—i—i—r-i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 lei 191 221 251 231 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.50
13,753.00
98.24
Pu-239
240
5,155.40
186
249
32.16
15,771.00
112.65
Am-241
284
5,485.70
249
303
32.48
17,661.00
126.15
Page 191 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:29:41PM 11/23/2015
Sample Name: IC-9793;AV238-20151018
Description:
Detector: AV238
Certificate ID: 82241-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:11:53PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV238 , SN: 51-005P7
Acquisition Start Date: 10/18/2015 9:32:47PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9793;AV238-20151018
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.33% +/- 0.31% TPU(2 sigma)
20CG
ZBCC
2cCC -
2400 -
2200 -
2000 -
1300
15CC
140C -
12CG -
1CCC -
see
600
400
200 H
0
Th-230
Pu-239
Am-241
i—i—i—i—i—i—i—i—i—i—i—i— i r11—i—m—i—f t r i r i—i—i1 i—i—i—i—tt—i—i—i—i—i—i—i—i—i—i—i—i—i—
1 21 41 61 81 101 131 161 191 221 251 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.36
13,900.00
99.29
Pu-239
240
5,155.40
186
249
32.15
14,628.00
104.49
Am-241
284
5,485.70
249
303
34.24
14,067.00
100.48
Page 192 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:11:59PM 10/19/2015
Sample Name: IC-9794;AV239-20151018
Description:
Detector: AV239
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:11:57PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV239 , SN: 51-005EE1
Acquisition Start Date: 10/18/2015 9:33:00PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9794;AV239-20151018
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.04% +/- 0.32% TPU(2 sigma)
2800
2600
2400
2200 H
20 OC
« 1800
1
£ 1SCC
o
KGC
12CC -
1000 -
300
600
400
200 ^
0
T
Th-230
Pu-239
Am-241
i—i—i—i—i—i—i—i—i—i—i—i——rfT i—1 "r i t i—r","i""T"i—i—i1 i—i—i—i—r-i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 161 191 221 251 2M 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.03
13,815.00
98.68
Pu-239
240
5,155.40
186
249
31.59
13,662.00
97.59
Am-241
284
5,485.70
249
303
31.15
14,789.00
105.64
Page 193 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:12:04PM 10/19/2015
Sample Name: IC-9795;AV240-20151018
Description:
Detector: AV240
Certificate ID: 82243-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:12:02PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV240 , SN: 51-005Q1
Acquisition Start Date: 10/18/2015 9:33:12PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9795;AV240-20151018
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.76% +/- 0.35% TPU(2 sigma)
20CG
ZBCC
2cCC -
2400 -
2200 -
2000
1300
15CC
140C -
12CG -
1CCC -
see
600
400
200 H
0
Th-230
Pu-239
Jl
Am-241
i—i—i—i—i—i—i—i—i—i—i—i—i—r-r—!—i—rn—r f~p'T r"i t
1 21 41 61 81 101 131 161 191 221 251
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
if i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—
311 341 371 401 431 461 491
Initial Calibration: Yes
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.66
13,193.00
94.24
Pu-239
240
5,155.40
186
249
30.85
13,452.00
96.09
Am-241
284
5,485.70
249
303
29.84
14,212.00
101.51
Page 194 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
4:12:08PM 10/19/2015
Sample Name: IC-9817;AV241-20151018
Description:
Detector: AV241
Certificate ID: 82244-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/19/2015 4:12:06PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV241 , SN: 50-005P1
Acquisition Start Date: 10/18/2015 9:33:21PM
Live Time: 140.00 min.
Real Time: 140.01 min.
Efficiency Calibration Name: IC-9817;AV241-20151018
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.71% +/- 0.30% TPU(2 sigma)
20CG
ZBCC
2cCC -
2400 -
2200 -
2000
1300
15CC
140C -
12CG -
1CCC -
see
600
400
200 H
0
Th-230
i
Pu-239
Am-241
i—i—i—i—i—i—i—i—i—i—i—i— 'i' T™ r i—f—f—i i imi i "f i—i—i 1 i—i—i—i—r—i—i—i—i—i—i—i—i—i—i—i—i—i—i—
1 21 41 61 81 101 131 161 191 221 251 251 311 341 371 401 431 461 491
channels.
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: Yes
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.42
15,200.00
108.57
Pu-239
240
5,155.40
186
249
31.91
14,189.00
101.35
Am-241
284
5,485.70
249
303
31.06
14,029.00
100.21
Page 195 of 551
-------
Initial
Calibration
Verifications
Page 196 of 551
-------
Alpha Spectroscopy Calibration Summary
Detector: AV148
Lab Sample ID
IC 160-223445/1
ICV 160-223563/1
CCV 160-258276/1
Detector: AV150
Lab Sample ID
IC 160-223447/1
ICV 160-223565/1
CCV 160-258278/1
Detectc
Lab Sample ID
IC 160-223448/1
ICV 160-223566/1
CCV 160-258279/1
Detector: AV152
Lab Sample ID
IC 160-223449/1
ICV 160-223567/1
CCV 160-258280/1
Detector: AV153
Lab Sample ID
IC 160-223450/1
ICV 160-223568/1
CCV 160-258281/1
Detector: AW155
Lab Sample ID
IC 160-223452/1
ICV 160-223570/1
CCV 160-258283/1
Detector: AV199
Lab Sample ID
IC 160-223496/1
ICV 160-223614/1
CCV 160-258308/1
Detector: AV235
Lab Sample ID
IC 160-223531/1
ICV 160-223650/1
CCV 160-258340/1
Analysis Date
10/16/15 16:27
10/26/15 19:10
06/27/16 10:48
Analysis Date
10/16/15 15:51
10/26/15 19:10
06/27/16 10:49
Analysis Date
10/16/15 15:51
10/26/15 19:11
06/27/16 10:49
Analysis Date
10/16/15 15:52
10/26/15 19:11
06/27/16 10:49
Analysis Date
10/16/15 15:52
10/26/15 19:11
06/27/16 10:50
Analysis Date
10/16/15 15:52
10/26/15 19:12
06/27/16 10:50
Analysis Date
10/17/15 18:15
11/01/15 14:25
06/27/16 13:50
Analysis Date
10/18/15 21:32
11/01/15 20:30
06/27/16 18:53
Reagent ID
82233-334_00001
82232-334_00001
82233-334 00001
Reagent ID
82235-334_00001
82247-334_00001
82235-334 00001
Reagent ID
82236-334_00001
82246-334_00001
82236-334 00001
Reagent ID
82237-334_00003
82242-334_00001
82237-334 00003
Reagent ID
82240-334_00001
82243-334_00001
82240-334 00001
Reagent ID
82242-334_00001
82237-334_00003
82242-334 00001
Reagent ID
82244-334_00001
82241-334_00001
82244-334 00001
Reagent ID
82236-334_00001
82246-334_00001
82236-334 00001
Efficiency
0.2672
0.2586
0.2679
Efficiency
0.2445
0.2449
0.2394
Efficiency
0.2528
0.2559
0.2486
Efficiency
0.2454
0.2417
0.2372
Efficiency
0.2660
0.2646
0.2605
Efficiency
0.2417
0.2427
0.2305
Efficiency
0.2471
0.2515
0.2420
Efficiency
0.2557
0.2578
0.2487
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Recovery
96.8
100.3
Recovery
Limits
95-105
95-105
Efficiency Recovery
Recovery Limits
100.1
97.9
95-105
95-105
Efficiency Recovery
Recovery Limits
101.3
98.4
95-105
95-105
Efficiency Recovery
Recovery Limits
98.5
96.7
95-105
95-105
Efficiency Recovery
Recovery Limits
99.5
97.9
95-105
95-105
Efficiency Recovery
Recovery Limits
100.4
95.4
95-105
95-105
Efficiency Recovery
Recovery Limits
101.8
97.9
95-105
95-105
Efficiency Recovery
Recovery Limits
100.8
97.3
95-105
95-105
Page 1 of 2 TestAmerica St. Louis
Page 197 of 551
-------
Alpha Spectroscopy Calibration Summary
Detectc 236
Lab Sample ID
IC 160-223532/1
ICV 160-223666/2
CCV 160-258356/1
Detectc '237
Lab Sample ID
IC 160-223533/1
ICV 160-223652/1
CCV 160-258342/1
Detectc '238
Lab Sample ID
IC 160-223534/1
ICV 160-223653/1
CCV 160-258343/1
Detectc 239
Lab Sample ID
IC 160-223535/1
ICV 160-223654/1
CCV 160-258357/1
Detector:
Lab Sample ID
IC 160-223536/1
ICV 160-223655/1
CCV 160-258358/1
Detector:
Lab Sample ID
IC 160-223537/1
ICV 160-223656/1
CCV 160-258359/1
Analysis Date
10/18/15 21:32
11/05/15 18:22
06/28/16 09:29
Analysis Date
10/18/15 21:32
11/01/15 20:31
06/27/16 18:53
Analysis Date
10/18/15 21:32
11/01/15 20:31
06/27/16 18:53
Analysis Date
10/18/15 21:33
11/01/15 20:31
06/28/16 08:13
Analysis Date
10/18/15 21:33
11/01/15 20:31
06/28/16 08:13
Analysis Date
10/18/15 21:33
11/01/15 20:32
06/28/16 08:21
Reagent ID
82237-334_00003
82242-334_00001
82237-334 00003
Reagent ID
82240-334_00001
82243-334_00001
82240-334 00001
Reagent ID
82241-334_00001
82244-334_00001
82241-334 00001
Reagent ID
82242-334_00001
82237-334_00003
82242-334 00001
Reagent ID
82243-334_00001
82240-334_00001
82243-334 00001
Reagent ID
82244-334_00001
82241-334_00001
82244-334 00001
Efficiency
0.2447
0.2437
0.2440
Efficiency
0.2587
0.2639
0.2562
Efficiency
0.2533
0.2451
0.2456
Efficiency
0.2504
0.2501
0.2417
Efficiency
0.2676
0.2611
0.2670
Efficiency
0.2471
0.2517
0.2417
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Limits
0.20-0.32
0.20-0.32
0.20-0.32
Efficiency
Recovery
99.6
99.7
Recovery
Limits
95-105
95-105
Efficiency Recovery
Recovery Limits
102.0
99.0
95-105
95-105
Efficiency Recovery
Recovery Limits
96.7
96.9
95-105
95-105
Efficiency Recovery
Recovery Limits
99.9
96.5
95-105
95-105
Efficiency Recovery
Recovery Limits
97.6
99.8
95-105
95-105
Efficiency Recovery
Recovery Limits
101.9
97.8
95-105
95-105
Page 2 of 2
Page 198 of 551
TestAmerica St. Louis
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:20:51PM 10/26/2015
Sample Name: ICV-7107;AV148-20151026
Description:
Detector: AV148
Certificate ID: 82232-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/26/2015 8:20:51PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV148 , SN: 50-05/R2
Acquisition Start Date: 10/26/2015 7:10:27PM
Live Time: 60.00 min.
Real Time: 60.01 min.
Efficiency Calibration Name: ICV-7107;AV148-20151021
Certification Date: 6/3/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.86% +/- 0.40% TPU(2 sigma)
liCC -
13CC -
12CC -
hoc -
10CC -
900 -
%
800 -
<"!
u
700 -
600 -
500 -
400 -
300 -
200 -
100 -
0 -
Pu-239
Th-230
i
I I I I I I I I ! I ! I f-p-ff-V | '|"i 'n'l I f
Am-241
f i i i f
t-i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 111 141 171 201 __1 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
33.29
7,000.00
116.67
Pu-239
240
5,155.40
186
249
31.50
6,783.00
113.05
Am-241
284
5,485.70
249
303
30.75
6,700.00
111.67
Page 199 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:30:17PM 11/23/2015
Sample Name: ICV-9886;AV150-20151026
Description:
Detector: AV150
Certificate ID: 82247-334
Prepared by: Analytics
Description:
Calibration
Source Info
Acquisition
Detector: AV150 , SN: 50-05/R4
Acquisition Start Date: 10/26/2015 7:10:54PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9886;AV150-2015102i
Analyst: 60040
Analysis Date: 10/26/2015 8:20:57PM
Calibration Type: Energy And Efficiency
Certification Date: 6/10/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.49% +/- 0.44% TPU(2 sigma)
1100 -I
1000 -
900 -
800 -
m
700 -
o
o
600 -
500 -
400 -
300 -
200 -
100 -
0 -
—r
Pu-230
Th-230
Am-241
1—I—I—I—I—I—n—I—I—I • I' r I 1 "*¦1 *1| ' yn , frm |- |—|l«j- I | 1 |« I—I—I—I—I—I—I—I—(—T—I—I—I—I—I—I—I—I—I—I—I—I—I—|—I—|—I
1 21 41 61 81 111 141 171 201 231 261 2i1 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.59
5,506.00
91.77
Pu-239
240
5,155.40
186
249
32.24
5,075.00
84.58
Am-241
284
5,485.70
249
303
31.73
5,498.00
91.63
Page 200 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:21:01PM 10/26/2015
Sample Name: ICV-9885;AV151 -20151026
Description:
Detector: AV151
Certificate ID: 82246-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/26/2015 8:21:00PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV151 , SN: 50-05/R5
Acquisition Start Date: 10/26/2015 7:11:09PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9885;AV151-20151021
1100
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.59% +/- 0.49% TPU(2 sigma)
1000
900
800
700
600
500 H
400
300 H
200
100 H
0
Th-230
1 1 1 1 1 1 1 1 1 1 1 1 r Tjrrjr- | 1 ¦ | »|—| 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 1 f
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
Pu-239
H
II
KnBjniimy.
Am-241
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.66
5,115.00
85.25
Pu-239
240
5,155.40
186
249
31.32
4,991.00
83.18
Am-241
284
5,485.70
249
303
31.95
5,449.00
90.82
Page 201 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:30:25PM 11/23/2015
Sample Name: ICV-9794;AV152-20151026
Description:
Detector: AV152
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/26/2015 8:21:03PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV152 , SN: 50-05/R6
Acquisition Start Date: 10/26/2015 7:11:27PM
Live Time: 60.00 min.
Real Time: 60.01 min.
Efficiency Calibration Name: ICV-9794;AV152-2015102i
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.17% +/- 0.41% TPU(2 sigma)
1100
1000 H
900
800
700
600
500
400
300
200
100 H
0
Pu-230
Am-241
Th-230
i—i—i—i—i—i—i—i—i—i—i—rrn—i—i—rm**n—r "r i—i—r—r—i—i—i—i v i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r-
1 21 41 61 SI 111 141 1?| 20-1 231 281 291 521 351 361 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
34.77
5,721.00
95.35
Pu-239
240
5,155.40
186
249
33.01
5,586.00
93.10
Am-241
284
5,485.70
249
303
31.64
6,169.00
102.82
Page 202 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:21:07PM 10/26/2015
Sample Name: ICV-9795;AV153-20151026
Description:
Detector: AV153
Certificate ID: 82243-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/26/2015 8:21:06PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV153 , SN: 54-011 Y6
Acquisition Start Date: 10/26/2015 7:11:41PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9795;AV153-2015102i
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.46% +/- 0.46% TPU(2 sigma)
1100
1000 H
900
800
700
600
500
400
300
200
100 H
0
1-
Pu-239
Th-230
Am-241
i—i—i—i—i—i—n—i—i—i—r |,nv""r7i—i—r*i—rT™r |~Tv1riTr"T i—P i—i—i—i r i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—r
1 21 41 61 81 111 141 171 201 2M 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.33
5,618.00
93.63
Pu-239
240
5,155.40
186
249
32.54
5,595.00
93.25
Am-241
284
5,485.70
249
303
32.83
6,103.00
101.72
Page 203 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:30:33PM 11/23/2015
Sample Name: ICV-9520;AV155-20151026
Description:
Detector: AV155
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 10/26/2015 8:21:13PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV155 , SN: 50-05/111
Acquisition Start Date: 10/26/2015 7:12:14PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9520;AV155-2015102i
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.27% +/- 0.45% TPU(2 sigma)
1300 -
1200 -
1100 -
1000 -
900 -
m
800 -
o
o
700 -
600 -
500 -
400 -
300 -
200 -
100 -
0 -
Am-241
F'u-239
Th-230
¦jp-^|rT|- | -[ I "TTI I
r»r
~ i i i i i i i i i i i
i—r i—i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
27.23
4,940.00
82.33
Pu-239
240
5,155.40
186
249
32.51
5,892.00
98.20
Am-241
284
5,485.70
249
303
33.96
4,770.00
79.50
Page 204 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:32:06PM 11/23/2015
Sample Name: ICV-9793;AV199-20151101
Description:
Detector: AV199
Certificate ID: 82241-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 3:56:07PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV199 , SN: 50-117Z3
Acquisition Start Date: 11/1/2015 2:25:56PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9793;AV199-2015110
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.15% +/- 0.42% TPU(2 sigma)
1 ilJtt -
1200 -
110-0 -
1000 -
900 -
m
800 -
o
u
700 -
600 -
500 -
400 -
300 -
200 -
100 -
0 -
1-
Pu-239
Th-230
Am-241
i—i—i—i—i—i—n—i—i—f—i— i "Tl i "i "i—i—i "I i—i "i™f i—i" P i—i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.93
5,988.00
99.80
Pu-239
240
5,155.40
186
249
30.79
6,118.00
101.97
Am-241
284
5,485.70
249
303
31.69
6,015.00
100.25
Page 205 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:16:22PM 11/1/2015
Sample Name: ICV-9885;AV235-20151101
Description:
Detector: AV235
Certificate ID: 82246-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:20PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV235 , SN: 51-005Q5
Acquisition Start Date: 11/1/2015 8:30:02PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9885;AV235-2015110
1100
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.78% +/- 0.49% TPU(2 sigma)
1000
900
800
700
600
500 H
400
300 H
200
100 ^
Pu-239
Th-230
Am-241
0 H—I—I—I—I—I—I—I—I—I—I ' I* I— TT I—I—| "1 1 p-p»( !—j—| f |—|—|—|—|—|—|—|—|—|—|—|—|—|—|—|—|—|—|-
1 21 41 61 81 101 131 161 191 221 251 281 311 341 371 401 431 461 491
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
32.30
5,105.00
85.08
Pu-239
240
5,155.40
186
249
33.27
4,989.00
83.15
Am-241
284
5,485.70
249
303
32.76
5,571.00
92.85
Page 206 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
2:05:18PM 11/7/2015
Sample Name: ICV-9794;AV236-20151105a
Description:
Detector: AV236
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/7/2015 2:05:17PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV236 , SN: 51-005P3
Acquisition Start Date: 11/5/2015 6:22:59PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9794;AV236-2015110!
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.37% +/- 0.42% TPU(2 sigma)
1100
1000 H
900
800
700
600
500
400
300
200
100 H
0
Pu-239
Th-230
Am-241
1—!—!—J—!—!—J—!—(—^—|" P™"!","!"" |—|—'| '"T "| ""I "TTT1 imp ,—|—| ' j" |—|—|—(—[—|—|—|—|—[—|—(—|—(—|—(—|—|—r
1 21 41 61 81 101 131 1c 1 191 221 251 2i1 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
32.30
5,696.00
94.93
Pu-239
240
5,155.40
186
249
34.39
5,670.00
94.50
Am-241
284
5,485.70
249
303
32.72
6,259.00
104.32
Page 207 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:33:25PM 11/23/2015
Sample Name: ICV-9795;AV237-20151101
Description:
Detector: AV237
Certificate ID: 82243-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:28PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV237 , SN: 50-120DD7
Acquisition Start Date: 11/1/2015 8:31:02PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9795;AV237-2015110
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.39% +/- 0.46% TPU(2 sigma)
1100
1000 H
900
800
700
600
500
400
300
200
100 H
0
T
Th-230
—r
Pu-239
i—i—i—n—i—i—i—i—i—r
~ I ! I
Arn-241
"n
I
\ i i r
1 21 41 61 81 101 131
191 221 251 2
channels.
— General Analysis
i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—i—
311 341 371 401 431 461 491
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.15
5,513.00
91.88
Pu-239
240
5,155.40
186
249
33.06
5,665.00
94.42
Am-241
284
5,485.70
249
303
30.78
6,092.00
101.53
Page 208 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:16:32PM 11/1/2015
Sample Name: ICV-9817;AV238-20151101
Description:
Detector: AV238
Certificate ID: 82244-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:31PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV238 , SN: 51-005P7
Acquisition Start Date: 11/1/2015 8:31:15PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9817;AV238-2015110
120-0
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.51% +/- 0.41% TPU(2 sigma)
11(H)
1000
900
800
700
600
500 H
400
300
200 H
100
Th-230
Pu-239
Atn-241
0 +—i—r—i—ri—m—! i i r f rfti—I T rrTT*T i '1 ""i"* i
1 21 41 61 81 101 131 161 191 221 251 1
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
I I I I I ! I I ! t I I I I I I I I I
311 341 371 401 431 461 491
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
33.17
6,400.00
106.67
Pu-239
240
5,155.40
186
249
35.28
6,070.00
101.17
Am-241
284
5,485.70
249
303
35.24
5,990.00
99.83
Page 209 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:16:36PM 11/1/2015
Sample Name: ICV-9520;AV239-20151101
Description:
Detector: AV239
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:35PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV239 , SN: 51-005EE1
Acquisition Start Date: 11/1/2015 8:31:32PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9520;AV239-2015110
liCC
13GG
12CC
hoc ^
10CC
900 A
I 800 -
o
o
700
600 H
500
400
300
200 H
100
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.01% +/- 0.46% TPU(2 sigma)
o 4™t
Pu-239
Th-230
Am-241
1—I—I—I—I—I—I—I—I—I— I TV I—I—I " [ I I I i
1 21 41 61 81 101 131 1c 1 191 221 251
t~T—I—I ' I—I—I—I—f—I—I—I—I—I—I—I—I—I—I—I—I—I—I—
311 341 371 401 431 461 491
channels.
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
27.94
5,117.00
85.28
Pu-239
240
5,155.40
186
249
29.59
6,071.00
101.18
Am-241
284
5,485.70
249
303
27.94
4,887.00
81.45
Page 210 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:16:40PM 11/1/2015
Sample Name: ICV-9792;AV240-20151101
Description:
Detector: AV240
Certificate ID: 82240-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:39PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV240 , SN: 51-005Q1
Acquisition Start Date: 11/1/2015 8:31:50PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9792;AV240-2015110
liCC
13GG
12CC
hoc ^
10CC
900 A
I 800 -
o
o
700
600 H
500
400
300
200 H
100
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.11% +/- 0.41% TPU(2 sigma)
o
Pu-239
Th-230
i—i—i—i—i—i—i—i—i—i—i—i— l—i11 i—i i i—i ,r,r r,r' i i1 'f "T*"!—i—i1 i—m—i—r-i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 161 191 221 251 251 311 341 371 401 431 461 491
channels
General Analysis
Am-241
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.15
5,861.00
97.68
Pu-239
240
5,155.40
186
249
32.46
6,691.00
111.52
Am-241
284
5,485.70
249
303
32.67
7,840.00
130.67
Page 211 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:33:33PM 11/23/2015
Sample Name: ICV-9793;AV241-20151101
Description:
Detector: AV241
Certificate ID: 82241-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 11/1/2015 11:16:43PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV241 , SN: 50-005P1
Acquisition Start Date: 11/1/2015 8:32:05PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: ICV-9793;AV241-2015110
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.17% +/- 0.42% TPU(2 sigma)
1 mo h
1200
1100
1000 H
900
I 800
8 700 -I
600
500
400
300 -
200 -
100
0 +-T-T
Th-230
Pu-239
Am-241
1
i—i—i—i—i—i—i—r— l' r"T i—f f i T~r*T i T"i—i—r*f—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 161 191 221 251 1: ' 311 341 371 401 431 461 491
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 0
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.18
5,997.00
99.95
Pu-239
240
5,155.40
186
249
30.06
6,143.00
102.38
Am-241
284
5,485.70
249
303
34.64
5,997.00
99.95
Page 212 of 551
-------
Monthly
Calibration
Verifications
Page 213 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:52:51AM 6/27/2016
Sample Name: CCV-8874;AV148-20160627
Description:
Detector: AV148
Certificate ID: 82233-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:52:50AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV148 , SN: 50-05/R2
Acquisition Start Date: 6/27/2016 10:48:12AM
Live Time: 60.00 min.
Real Time: 60.02 min.
Efficiency Calibration Name: CCV-8874;AV148-201606;
Certification Date: 6/3/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.79% +/- 0.50% TPU(2 sigma)
1300 -
1200 -
1100 -
1000 -
900 -
m
800 -
o
o
700 -
600 -
500 -
400 -
300 -
200 -
100 -
0 -
Pu-239
I
Th-230
-J
Am-241
1 r rt11 i—i i "i' i'™t i—i1 "V' i—i—I i—i—i—i—i—i—n—i—i—i—i—i—i—i—i—i—i—i—i—r
\ I I ! I ! I I 1 I 1 r
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.04
4,552.00
75.87
Pu-239
240
5,155.40
186
249
32.45
6,017.00
100.28
Am-241
284
5,485.70
249
303
32.21
4,950.00
82.50
Page 214 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:53:18 AM 6/27/2016
Sample Name: CCV-8876;AV150-20160627
Description:
Detector: AV150
Certificate ID: 82235-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:53:17AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV150 , SN: 50-05/R4
Acquisition Start Date: 6/27/2016 10:49:05AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-8876;AV150-201606;
120-0
Certification Date: 6/4/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 23.94% +/- 0.39% TPU(2 sigma)
11(H)
1000
900
800
700
600
500 H
400
300
200 H
100
0
r
Pu-239
Th-230
Am-241
i—i—i—i—i—i—r—i—i—i—rrrfi—i—i —i——i—i—i—i——i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—r
1 21 41 61 81 111 141 r' 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
32.32
6,372.00
106.20
Pu-239
240
5,155.40
186
249
34.61
5,965.00
99.42
Am-241
284
5,485.70
249
303
36.46
6,178.00
102.97
Page 215 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:53:31AM 6/27/2016
Sample Name: CCV-8877;AV151 -20160627
Description:
Detector: AV151
Certificate ID: 82236-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:53:30AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV151 , SN: 50-05/R5
Acquisition Start Date: 6/27/2016 10:49:25AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-8877;AV151 -201606;
Certification Date: 6/2/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.86% +/- 0.41% TPU(2 sigma)
120-0 -
1100 -
1000 -
900 -
800 -
m
N
700 -
n
u
600 -
500 -
400 -
300 -
200 -
100 -
0 -
i—i—i—i—i—i—n—i—t*t—r-f
Th-230
I
Pu-239
i f1 t 11 i i i i 'i rr i i' i i i i r i i i i f i i i i i i i i i i i i i i i i i
Am-241
'3
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.02
6,181.00
103.02
Pu-239
240
5,155.40
186
249
35.02
6,152.00
102.53
Am-241
284
5,485.70
249
303
31.25
6,123.00
102.05
Page 216 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:53:56AM 6/27/2016
Sample Name: CCV-9520;AV152-20160627
Description:
Detector: AV152
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:53:54AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV152 , SN: 50-05/R6
Acquisition Start Date: 6/27/2016 10:49:44AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9520;AV152-201606;
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 23.72% +/- 0.44% TPU(2 sigma)
1100
1000 H
900
800
700
600
500
400
300
200
100 H
0
Pu-239
Th-230
i
•"T I i V
Am-241
i—i—i—i—i—i—i—i—i—i—i—i——i—i—i—i—i—i—ill i—i ttt f i—i— i i "i—i—m—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—i—r~
1 21 41 61 81 111 141 171 201 231 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.54
4,771.00
79.52
Pu-239
240
5,155.40
186
249
34.92
5,725.00
95.42
Am-241
284
5,485.70
249
303
32.75
4,753.00
79.22
Page 217 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:54:09AM 6/27/2016
Sample Name: CCV-9792;AV153-20160627
Description:
Detector: AV153
Certificate ID: 82240-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:54:07AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV153 , SN: 54-011 Y6
Acquisition Start Date: 6/27/2016 10:50:05AM
Live Time: 60.00 min.
Real Time: 60.01 min.
Efficiency Calibration Name: CCV-9792;AV153-201606;
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.05% +/- 0.41% TPU(2 sigma)
1 mo h
1200
1100
1000 H
900
I 800
8 700 -I
600
500
400
300 -
200 -
100
0
Pu-239 Am-241
Th-230
i—i—i—i—i—i—n—i—i—i—i—rrrn—r"i—r r "( i—i t"t i—i—r i—i—i—i—r-1—n—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—i
1 21 41 61 81 111 141 171 201 221 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.30
5,884.00
98.07
Pu-239
240
5,155.40
186
249
33.65
6,740.00
112.33
Am-241
284
5,485.70
249
303
33.08
7,716.00
128.60
Page 218 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
11:54:31AM 6/27/2016
Sample Name: CCV-9794;AV155-20160627
Description:
Detector: AV155
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 11:54:30AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV155 , SN: 50-05/111
Acquisition Start Date: 6/27/2016 10:50:52AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9794;AV155-201606;
1100
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 23.05% +/- 0.40% TPU(2 sigma)
1000
900
800
700
600
500 H
400
300 H
200
100 H
0
Arn-241
Pu-230
Th-230
i—i—i—i—i—i—n—i—i—i * i'' y'T"*!—rTTtm—r ttt i—r i—i—i—i—n—n—i—i—i—i—i—i—i—i—i—i—i—i—i—n—i—i—i—r
1 21 41 61 81 111 141 171 201 2M 261 291 321 351 381 411 441 471 501 531 561
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.46
5,389.00
89.82
Pu-239
240
5,155.40
186
249
34.35
5,412.00
90.20
Am-241
284
5,485.70
249
303
32.27
5,863.00
97.72
Page 219 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
2:55:18PM 6/27/2016
Sample Name: CCV-9817;AV199-20160627
Description:
Detector: AV199
Certificate ID: 82244-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/27/2016 2:55:17PM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV199 , SN: 50-117Z3
Acquisition Start Date: 6/27/2016 1:50:21 PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9817;AV199-201606;
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.20% +/- 0.40% TPU(2 sigma)
120-0 -
1100 -
1000 -
900 -
800 -
m
N
700 -
n
u
600 -
500 -
400 -
300 -
200 -
100 -
0 -
Am-241
F'u-239
Th-230
__
1 i i i i i i i I I 1 I I I I I I I I I I I I I I I I I I I I I I I
;;i 291 321 351 381 411 441 471 501 531 561
1 21 41 61 81 111 141 171 201
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide Activity Summary
Peak ROI ROI Peak
Peak Energy Start End FWHM
Nuclide Channel keV Channel Channel keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.68
6,410.00
106.83
Pu-239
240
5,155.40
186
249
33.57
5,773.00
96.22
Am-241
284
5,485.70
249
303
34.41
6,034.00
100.57
Page 220 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
2:14:48PM 6/28/2016
Sample Name: CCV-8877;AV235-20160627
Description:
Detector: AV235
Certificate ID: 82236-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 7:40:39AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV235 , SN: 51-005Q5
Acquisition Start Date: 6/27/2016 6:53:04PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-8877;AV235-201606;
Certification Date: 6/2/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.87% +/- 0.41% TPU(2 sigma)
1 mo h
1200
1100
1000 H
900
I 800
8 700 -I
600
500
400
300 -
200 -
100
0
Pu-239
Th-230
Am-241
I
l—I—I—I—I—I—I—I—I—I—I—I——I—I—I—I—I—I T p-r | |' TT" I—I—I—1—1—I—I—I—I—I—I—I—I—I—I—I—I—I—I—I—I—r
1 21 41 61 81 101 131 HI 191 221 251 2S1 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
29.94
6,157.00
102.62
Pu-239
240
5,155.40
186
249
32.06
6,396.00
106.60
Am-241
284
5,485.70
249
303
33.98
5,953.00
99.22
Page 221 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
10:30:01AM 6/28/2016
Sample Name: CCV-9520;AV236-20160628a
Description:
Detector: AV236
Certificate ID: 82237-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 10:30:00AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV236 , SN: 51-005P3
Acquisition Start Date: 6/28/2016 9:29:55AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9520;AV236-201606;
1300
1200
1100
1000
900
Certification Date: 6/1/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.40% +/- 0.45% TPU(2 sigma)
| 800
600
500
400
300
200
100
0
Pu-239
Th-230
i—i—i—i—i—i—i—i—i—i—i—i— i "i' i—i—r~i—i ¦ r ¦Kv i—i' "i"" i—i—i i—i—i—i—r—i—i—i—i—i—i—i—i—i—i—i—i—i—i—
1 21 41 61 81 101 131 161 191 221 251 251 311 341 371 401 431 461 491
channels.
General Analysis
I
Am-241
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.76
5,069.00
84.48
Pu-239
240
5,155.40
186
249
31.90
5,772.00
96.20
Am-241
284
5,485.70
249
303
35.09
4,829.00
80.48
Page 222 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
7:40:50AM 6/28/2016
Sample Name: CCV-9792;AV237-20160627
Description:
Detector: AV237
Certificate ID: 82240-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 7:40:49AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV237 , SN: 50-120DD7
Acquisition Start Date: 6/27/2016 6:53:27PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9792;AV237-201606
liCC -
13GG
12CC
hoc ^
10CC
900 A
I 800 -
o
o
700
600 H
500
400
300
200 H
100
0
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 25.62% +/- 0.41% TPU(2 sigma)
T
t—i—i—i—i—i—i—r
—r
Pu-239
Th-230
i T i—i—r
1—l fT**i**
Am-241
¦y i i—r
1 21 41 61 81 101 131
-T—I 1—I 1—I—I 1—I 1—I 1—I—I 1—I 1—I—
191 221 251 281 311 341 371 401 431 461 491
channels.
- General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.73
5,783.00
96.38
Pu-239
240
5,155.40
186
249
31.02
6,637.00
110.62
Am-241
284
5,485.70
249
303
33.88
7,586.00
126.43
Page 223 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
7:40:55AM 6/28/2016
Sample Name: CCV-9793;AV238-20160627
Description:
Detector: AV238
Certificate ID: 82241-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 7:40:54AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV238 , SN: 51-005P7
Acquisition Start Date: 6/27/2016 6:53:44PM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9793;AV238-201606I
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.56% +/- 0.42% TPU(2 sigma)
1100
1000 H
900
800
700
600
500 H
400
300
200
100 ^
Am-241
Pu-239
Th-230
0 -I—i—i—i—i—i—i—i—i—i—i—i—i—pt"t' i—i—rn—r*i"-r—t—i *Y i—i—r—f—i—n—i t i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 1?1 191 221 251 2:1 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
32.03
5,702.00
95.03
Pu-239
240
5,155.40
186
249
36.54
6,170.00
102.83
Am-241
284
5,485.70
249
303
37.88
5,823.00
97.05
Page 224 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:16:48AM 6/28/2016
Sample Name: CCV-9794;AV239-20160628a
Description:
Detector: AV239
Certificate ID: 82242-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 9:16:47AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV239 , SN: 51-005EE1
Acquisition Start Date: 6/28/2016 8:13:35AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9794;AV239-201606I
120-0
11(H)
1000
900
800
| 700
o
o
600
500 H
400
300
200 H
100
0
Certification Date: 6/8/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.17% +/- 0.41% TPU(2 sigma)
I
Pu-239
Th-230
—i—i—i—i—i—i—i—i—i—mr
1 21 41 61 81 101 131
-r*r
t-
Am-241
191 221 251 :
channels
— General Analysis
r*T—r i I'ri i i it i j i i j i i i i i i i i i r-
311 341 371 401 431 461 491
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
28.30
5,694.00
94.90
Pu-239
240
5,155.40
186
249
30.59
5,613.00
93.55
Am-241
284
5,485.70
249
303
34.03
6,166.00
102.77
Page 225 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:16:55 AM 6/28/2016
Sample Name: CCV-9795;AV240-20160628a
Description:
Detector: AV240
Certificate ID: 82243-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 9:16:53AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV240 , SN: 51-005Q1
Acquisition Start Date: 6/28/2016 8:13:56AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9795;AV240-201606;
120-0
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 26.70% +/- 0.46% TPU(2 sigma)
11(H)
1000
900
800
700
600
500 H
400
300
200 H
100
Pu-239
Th-230
Am-241
0 H—i—i—i—r—i—i—i—i—i—i* i™ i— f™lm i—i—t*i—| —"f—n—i—i' i—i—i—m—i—i—i—i—i—i—i—i—i—i—i—i—i—r
1 21 41 61 81 101 131 1c 1 191 221 251 2c 1 311 341 371 401 431 461 491
channels
General Analysis
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
30.29
5,715.00
95.25
Pu-239
240
5,155.40
186
249
33.62
5,731.00
95.52
Am-241
284
5,485.70
249
303
35.41
6,024.00
100.40
Page 226 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Ipha-Spectroscopy
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:22:02AM 6/28/2016
Sample Name: CCV-9817;AV241 -20160628a
Description:
Detector: AV241
Certificate ID: 82244-334
Prepared by: Analytics
Description:
Calibration
Source Info
Analyst: 60040
Analysis Date: 6/28/2016 9:22:00AM
Calibration Type: Energy And Efficiency
Acquisition
Detector: AV241 , SN: 50-005P1
Acquisition Start Date: 6/28/2016 8:21:27AM
Live Time: 60.00 min.
Real Time: 60.00 min.
Efficiency Calibration Name: CCV-9817;AV241 -201606;
120-0
Certification Date: 6/9/2010 12:00:00PM
Energy Calibration Equation:
Gain = 7.4575 keV / Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV I Ch2
Efficiency: 24.17% +/- 0.40% TPU(2 sigma)
11(H)
1000
900
800
700
600
500 H
400
300
200 H
100
0
Th-230
1 !—f—j—! ^( j—j j , pr.p | «.[- i , -r j T(jn—p , , nny™ |—, (—p-, ,—, ,—,—,—, ,—, ,—| ,—,—t 1—| 1—| n
1 21 41 61 81 101 131 161 191 221 251 2=1 311 341 371 401 431 461 491
channels
General Analysis
Pu-239
Arn-241
Method: Manual (ROI)
Algorithm: Linear
Initial Calibration: No
Shelf: 1
Nuclide
Peak
Channel
Peak
Energy
keV
ROI
Start
Channel
ROI
End
Channel
Peak
FWHM
keV
Gross
Counts
Net Count
Rate
(cpm)
Th-230
177
4,687.50
132
186
31.44
6,421.00
107.02
Pu-239
240
5,155.40
186
249
33.75
5,817.00
96.95
Am-241
284
5,485.70
249
303
32.40
5,951.00
99.18
Page 227 of 551
-------
Monthly
Backgrounds
Page 228 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV148
Comment:
Batch Name: June2016
Description:
Detector: AV148 , SN: 50-05/R2
Acquisition Start Date: 6/24/2016 4:15:34PM
Live Time: 960.00 min.
Real Time: 960.49 min.
Calibration Name: IC-8874;AV148-20151016a
Calibration Date: 10/16/2015 6:47:19PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:23:50AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
7 ¦
6 -
(/)
3 -
Th-23U-238
J_L
U-235
T U-Np-2Po-209
ILi
Th-22S
PAPo-2 Cm-24641
? ri
Cm-24^
J J
in
Pu-236
I 1 1
ThCm-242
1
0
3374 3674 3974 4274 4E74 4S74 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV)
I I I I I I
l i r
i i I
i i i i i
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 162.00
Page 229 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertaintv
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
1.00
1.042E-003
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
0.00
0.000E+000
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
0.00
0.000E+000
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
0.00
0.000E+000
1.473E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
3.00
3.125E-003
2.083E-003
Am-243
5,231.34
5,052.36
5,305.92
3.00
3.125E-003
2.083E-003
U-232
5,253.71
5,059.82
5,402.86
7.00
7.292E-003
2.946E-003
Th-228
5,447.61
5,186.59
5,507.27
14.00
1.458E-002
4.034E-003
Po-210
5,276.09
5,231.34
5,291.00
1.00
1.042E-003
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
13.00
1.354E-002
3.898E-003
Am-241
5,484.90
5,298.46
5,604.22
16.00
1.667E-002
4.295E-003
Cm-245
5,417.78
5,395.41
5,447.61
9.00
9.375E-003
3.294E-003
Pu-236
5,760.83
5,611.67
5,887.60
55.00
5.729E-002
7.795E-003
Cm-244
5,775.74
5,641.51
5,902.52
54.00
5.625E-002
7.725E-003
Th-227
6,074.04
5,932.35
6,178.45
9.00
9.375E-003
3.294E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 230 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV150
Comment:
Batch Name: June2016
Description:
Detector: AV150 , SN: 50-05/R4
Acquisition Start Date: 6/24/2016 4:15:33PM
Live Time: 960.00 min.
Real Time: 960.01 min.
Calibration Name: IC-8876;AV150-20151016
Calibration Date: 10/16/2015 6:46:46PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:19:30 AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
6 -
5 ¦
m 4 -
"E
o
o
o
3
2 ¦
1 -
Th-23U-238
U-235
Po-209
1
T U-Np-237292
111
Pu-238
PAPo-2 Cm-24641
Cm-2«
ThCm-242
0
3374 3674 3974 4274 4E74 4874 5174 5474 5774 6074 6374 6674 6974
Energy (keV)
I I I I I I
I I I I I I r
7274 7574
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 82.00
Page 231 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
1.00
1.042E-003
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
1.00
1.042E-003
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
0.00
0.000E+000
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
0.00
0.000E+000
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
3.00
3.125E-003
2.083E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
2.00
2.083E-003
1.804E-003
Pu-239
5,179.14
4,970.33
5,238.80
2.00
2.083E-003
1.804E-003
Am-243
5,231.34
5,052.36
5,305.92
3.00
3.125E-003
2.083E-003
U-232
5,253.71
5,059.82
5,402.86
6.00
6.250E-003
2.756E-003
Th-228
5,447.61
5,186.59
5,507.27
13.00
1.354E-002
3.898E-003
Po-210
5,276.09
5,231.34
5,291.00
2.00
2.083E-003
1.804E-003
P u-238
5,469.98
5,268.63
5,552.01
14.00
1.458E-002
4.034E-003
Am-241
5,484.90
5,298.46
5,604.22
13.00
1.354E-002
3.898E-003
Cm-245
5,417.78
5,395.41
5,447.61
5.00
5.208E-003
2.552E-003
Pu-236
5,760.83
5,611.67
5,887.60
21.00
2.188E-002
4.886E-003
Cm-244
5,775.74
5,641.51
5,902.52
21.00
2.188E-002
4.886E-003
Th-227
6,074.04
5,932.35
6,178.45
6.00
6.250E-003
2.756E-003
Cm-242
6,148.62
6,118.79
6,178.45
5.00
5.208E-003
2.552E-003
Page 232 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV151
Comment:
Batch Name: June2016
Description:
Detector: AV151 , SN: 50-05/R5
Acquisition Start Date: 6/24/2016 4:15:34PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-8877;AV151-20151016
Calibration Date: 10/16/2015 6:46:50PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:19:29AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
6 -
5 ¦
m 4
"E
o
o
o
3
2 ¦
1 -
Th-23U-238
J_L
U-235
I (-'-a!. I "jL.S
m
Cm-246
Po-21CPu-238
T U-Np-2PO-209 PAU-232 Am-241
"111 "
Pu-236
J
II
Cm-2
Th-227
i
HCm-242
3374 3674 3974 4274 4574 4S74 5174 5474 5774 6074 6374 6674
i—i—i—i—r
7274 7574
6974
Energy (keV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 159.00
Page 233 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertaintv
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
1.00
1.042E-003
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
1.00
1.042E-003
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
1.00
1.042E-003
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
0.00
0.000E+000
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
1.00
1.042E-003
1.473E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
1.00
1.042E-003
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
4.00
4.167E-003
2.329E-003
U-232
5,253.71
5,059.82
5,402.86
7.00
7.292E-003
2.946E-003
Th-228
5,447.61
5,186.59
5,507.27
18.00
1.875E-002
4.541 E-003
Po-210
5,276.09
5,231.34
5,291.00
3.00
3.125E-003
2.083E-003
P u-238
5,469.98
5,268.63
5,552.01
18.00
1.875E-002
4.541 E-003
Am-241
5,484.90
5,298.46
5,604.22
18.00
1.875E-002
4.541 E-003
Cm-245
5,417.78
5,395.41
5,447.61
7.00
7.292E-003
2.946E-003
Pu-236
5,760.83
5,611.67
5,887.60
44.00
4.583E-002
6.988E-003
Cm-244
5,775.74
5,641.51
5,902.52
41.00
4.271 E-002
6.751 E-003
Th-227
6,074.04
5,932.35
6,178.45
5.00
5.208E-003
2.552E-003
Cm-242
6,148.62
6,118.79
6,178.45
1.00
1.042E-003
1.473E-003
Page 234 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV152
Comment:
Batch Name: June2016a
Description:
Detector: AV152 , SN: 50-05/R6
Acquisition Start Date: 6/26/2016 5:10:10PM
Live Time: 960.00 min.
Real Time: 960.03 min.
Calibration Name: IC-9520;AV152-20151016
Calibration Date: 10/16/2015 6:46:53PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:10:55 AM 6/27/2016
Spectrum #4 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Energy (keV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 131.00
Page 235 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
1.00
1.042E-003
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
2.00
2.083E-003
1.804E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
1.00
1.042E-003
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
4.00
4.167E-003
2.329E-003
Pu-242
4,903.21
4,679.48
4,947.95
3.00
3.125E-003
2.083E-003
Th-229
4,858.46
4,739.14
5,119.48
3.00
3.125E-003
2.083E-003
Np-237
4,783.89
4,768.97
4,806.26
3.00
3.125E-003
2.083E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
0.00
0.000E+000
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
3.00
3.125E-003
2.083E-003
U-232
5,253.71
5,059.82
5,402.86
6.00
6.250E-003
2.756E-003
Th-228
5,447.61
5,186.59
5,507.27
11.00
1.146E-002
3.608E-003
Po-210
5,276.09
5,231.34
5,291.00
3.00
3.125E-003
2.083E-003
P u-238
5,469.98
5,268.63
5,552.01
9.00
9.375E-003
3.294E-003
Am-241
5,484.90
5,298.46
5,604.22
8.00
8.333E-003
3.125E-003
Cm-245
5,417.78
5,395.41
5,447.61
4.00
4.167E-003
2.329E-003
Pu-236
5,760.83
5,611.67
5,887.60
40.00
4.167E-002
6.670E-003
Cm-244
5,775.74
5,641.51
5,902.52
40.00
4.167E-002
6.670E-003
Th-227
6,074.04
5,932.35
6,178.45
10.00
1.042E-002
3.455E-003
Cm-242
6,148.62
6,118.79
6,178.45
3.00
3.125E-003
2.083E-003
Page 236 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV153
Comment:
Batch Name: June2016
Description:
Detector: AV153 , SN: 54-011 Y6
Acquisition Start Date: 6/24/2016 4:15:17PM
Live Time: 960.00 min.
Real Time: 960.01 min.
Calibration Name: IC-9792;AV153-20151016
Calibration Date: 10/16/2015 6:46:57PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:19:47AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
11
10 -
9 -
s -
w 7 ¦
"E
8 6 H
5 H
4
3
2 ¦
1 -
0
Th-23U-238
u
U-235
Th-:Np-237
ii II
U-23TtP c-209
11
rm-24Cm-245
III ill
Pu-Po-21CIAm-241
Ujl II.
IC m-244
5774
Cm-242
llli
Th-227
3374 3674
i i i i
3974 4274
4574
4S74
E174 5474
Energy (keV)
6074
6374
6674
1 I I I I I I I
6974 7274 7574
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 155.00
Page 237 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
2.00
2.083E-003
1.804E-003
U-234
4,709.31
4,507.96
4,821.17
3.00
3.125E-003
2.083E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
1.00
1.042E-003
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
2.00
2.083E-003
1.804E-003
Am-243
5,231.34
5,052.36
5,305.92
2.00
2.083E-003
1.804E-003
U-232
5,253.71
5,059.82
5,402.86
6.00
6.250E-003
2.756E-003
Th-228
5,447.61
5,186.59
5,507.27
9.00
9.375E-003
3.294E-003
Po-210
5,276.09
5,231.34
5,291.00
1.00
1.042E-003
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
8.00
8.333E-003
3.125E-003
Am-241
5,484.90
5,298.46
5,604.22
9.00
9.375E-003
3.294E-003
Cm-245
5,417.78
5,395.41
5,447.61
3.00
3.125E-003
2.083E-003
Pu-236
5,760.83
5,611.67
5,887.60
52.00
5.417E-002
7.583E-003
Cm-244
5,775.74
5,641.51
5,902.52
51.00
5.313E-002
7.512E-003
Th-227
6,074.04
5,932.35
6,178.45
13.00
1.354E-002
3.898E-003
Cm-242
6,148.62
6,118.79
6,178.45
8.00
8.333E-003
3.125E-003
Page 238 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV155
Comment:
Batch Name: June2016a
Description:
Detector: AV155 , SN: 50-05/111
Acquisition Start Date: 6/26/2016 5:10:11PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9794;AV155-20151016
Calibration Date: 10/16/2015 6:47:03PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
9:10:37 AM 6/27/2016
Spectrum #4 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
7 ¦
6 -
(/)
3 -
Th-23U-238
J_L
U-235
T U-Np-2Po-209
ILi
I
Th-228
I
Cm-24^
j|
ThCm-242
0
3374 3674 3974 4274 4E74 4S74 5174 5474 5774 6074 6374 6674 6974 7274 7574
Energy (keV)
I I I I I I
1 I I I I I I
I I I I
I I I I I
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 150.00
Page 239 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
0.00
0.000E+000
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
0.00
0.000E+000
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
0.00
0.000E+000
1.473E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
2.00
2.083E-003
1.804E-003
Am-243
5,231.34
5,052.36
5,305.92
2.00
2.083E-003
1.804E-003
U-232
5,253.71
5,059.82
5,402.86
8.00
8.333E-003
3.125E-003
Th-228
5,447.61
5,186.59
5,507.27
15.00
1.563E-002
4.167E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
17.00
1.771E-002
4.419E-003
Am-241
5,484.90
5,298.46
5,604.22
17.00
1.771 E-002
4.419E-003
Cm-245
5,417.78
5,395.41
5,447.61
8.00
8.333E-003
3.125E-003
Pu-236
5,760.83
5,611.67
5,887.60
40.00
4.167E-002
6.670E-003
Cm-244
5,775.74
5,641.51
5,902.52
39.00
4.062E-002
6.588E-003
Th-227
6,074.04
5,932.35
6,178.45
15.00
1.563E-002
4.167E-003
Cm-242
6,148.62
6,118.79
6,178.45
7.00
7.292E-003
2.946E-003
Page 240 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV199
Comment:
Batch Name: June2016
Description:
Detector: AV199 , SN: 50-117Z3
Acquisition Start Date: 6/24/2016 4:15:21PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9817;AV199-20151017
Calibration Date: 10/18/2015 3:55:29PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:16:37 AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
6974 7274 7574
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 165.00
Page 241 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
1.00
1.042E-003
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
3.00
3.125E-003
2.083E-003
U-234
4,709.31
4,507.96
4,821.17
3.00
3.125E-003
2.083E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
1.00
1.042E-003
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
4.00
4.167E-003
2.329E-003
Am-243
5,231.34
5,052.36
5,305.92
4.00
4.167E-003
2.329E-003
U-232
5,253.71
5,059.82
5,402.86
10.00
1.042E-002
3.455E-003
Th-228
5,447.61
5,186.59
5,507.27
18.00
1.875E-002
4.541 E-003
Po-210
5,276.09
5,231.34
5,291.00
1.00
1.042E-003
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
17.00
1.771E-002
4.419E-003
Am-241
5,484.90
5,298.46
5,604.22
17.00
1.771 E-002
4.419E-003
Cm-245
5,417.78
5,395.41
5,447.61
8.00
8.333E-003
3.125E-003
Pu-236
5,760.83
5,611.67
5,887.60
59.00
6.146 E-002
8.069E-003
Cm-244
5,775.74
5,641.51
5,902.52
59.00
6.146 E-002
8.069E-003
Th-227
6,074.04
5,932.35
6,178.45
8.00
8.333E-003
3.125E-003
Cm-242
6,148.62
6,118.79
6,178.45
3.00
3.125E-003
2.083E-003
Page 242 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV235
Comment:
Batch Name: June2016
Description:
Detector: AV235 , SN: 51-005Q5
Acquisition Start Date: 6/24/2016 4:15:28PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-8877;AV235-20151018
Calibration Date: 10/19/2015 4:11:39PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:17:07 AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2 ¦
¦e
o
o
1 -
Th-23;U-238
J_L
U-235
TU-:Np-2;P O-209
m
P 0-210
P A U-232C m-24641
lillllltl.lll
Cm-244
ThCm-242
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
I I I I I I 1 I
I I I I I I I
I I I I I 1 I I I
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 34.00
Page 243 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
2.00
2.083E-003
1.804E-003
Th-230
4,679.48
4,403.55
4,746.60
0.00
0.000E+000
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
0.00
0.000E+000
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
1.00
1.042E-003
1.473E-003
Th-229
4,858.46
4,739.14
5,119.48
1.00
1.042E-003
1.473E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
0.00
0.000E+000
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
3.00
3.125E-003
2.083E-003
U-232
5,253.71
5,059.82
5,402.86
5.00
5.208E-003
2.552E-003
Th-228
5,447.61
5,186.59
5,507.27
9.00
9.375E-003
3.294E-003
Po-210
5,276.09
5,231.34
5,291.00
2.00
2.083E-003
1.804E-003
P u-238
5,469.98
5,268.63
5,552.01
10.00
1.042E-002
3.455E-003
Am-241
5,484.90
5,298.46
5,604.22
8.00
8.333E-003
3.125E-003
Cm-245
5,417.78
5,395.41
5,447.61
4.00
4.167E-003
2.329E-003
Pu-236
5,760.83
5,611.67
5,887.60
6.00
6.250E-003
2.756E-003
Cm-244
5,775.74
5,641.51
5,902.52
6.00
6.250E-003
2.756E-003
Th-227
6,074.04
5,932.35
6,178.45
4.00
4.167E-003
2.329E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 244 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV236
Comment:
Batch Name: June2016
Description:
Detector: AV236 , SN: 51-005P3
Acquisition Start Date: 6/24/2016 4:15:30PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9520;AV236-20151018
Calibration Date: 10/19/2015 4:11:44PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:17:11AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2 ¦
¦e
o
o
1 -
Th-23;U-238
J_L
I l l i
U-235
TU-:Np-2;P O-209
JliPL
Th-228
P A IP 0-2 C m-24641
ii
Cm-244
I I I
ThCm-242
I I I I
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 27.00
Page 245 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
1.00
1.042E-003
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
3.00
3.125E-003
2.083E-003
U-234
4,709.31
4,507.96
4,821.17
3.00
3.125E-003
2.083E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
0.00
0.000E+000
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
0.00
0.000E+000
1.473E-003
U-232
5,253.71
5,059.82
5,402.86
3.00
3.125E-003
2.083E-003
Th-228
5,447.61
5,186.59
5,507.27
6.00
6.250E-003
2.756E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
6.00
6.250E-003
2.756E-003
Am-241
5,484.90
5,298.46
5,604.22
6.00
6.250E-003
2.756E-003
Cm-245
5,417.78
5,395.41
5,447.61
3.00
3.125E-003
2.083E-003
Pu-236
5,760.83
5,611.67
5,887.60
5.00
5.208E-003
2.552E-003
Cm-244
5,775.74
5,641.51
5,902.52
3.00
3.125E-003
2.083E-003
Th-227
6,074.04
5,932.35
6,178.45
2.00
2.083E-003
1.804E-003
Cm-242
6,148.62
6,118.79
6,178.45
1.00
1.042E-003
1.473E-003
Page 246 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV237
Comment:
Batch Name: June2016
Description:
Detector: AV237 , SN: 50-120DD7
Acquisition Start Date: 6/24/2016 4:15:29PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9792;AV237-20151018
Calibration Date: 10/19/2015 4:11:48PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:17:21AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
3 ¦
¦E 2
o
o
Th-23;U-238
J_L
U-235
TU-:Np-2;P O-209
m
Cm-245
PAiPo-210IAm-241
I
Cm-244
ThCm-242
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
I I I I I I 1 I I
I I I
1 I I I I I
i i i i i r
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 36.00
Page 247 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
2.00
2.083E-003
1.804E-003
U-234
4,709.31
4,507.96
4,821.17
4.00
4.167E-003
2.329E-003
Pu-242
4,903.21
4,679.48
4,947.95
3.00
3.125E-003
2.083E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
2.00
2.083E-003
1.804E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
0.00
0.000E+000
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
0.00
0.000E+000
1.473E-003
U-232
5,253.71
5,059.82
5,402.86
5.00
5.208E-003
2.552E-003
Th-228
5,447.61
5,186.59
5,507.27
8.00
8.333E-003
3.125E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
8.00
8.333E-003
3.125E-003
Am-241
5,484.90
5,298.46
5,604.22
8.00
8.333E-003
3.125E-003
Cm-245
5,417.78
5,395.41
5,447.61
5.00
5.208E-003
2.552E-003
Pu-236
5,760.83
5,611.67
5,887.60
8.00
8.333E-003
3.125E-003
Cm-244
5,775.74
5,641.51
5,902.52
8.00
8.333E-003
3.125E-003
Th-227
6,074.04
5,932.35
6,178.45
2.00
2.083E-003
1.804E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 248 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV238
Comment:
Batch Name: June2016
Description:
Detector: AV238 , SN: 51-005P7
Acquisition Start Date: 6/24/2016 4:15:30PM
Live Time: 960.00 min.
Real Time: 960.22 min.
Calibration Name: IC-9793;AV238-20151018
Calibration Date: 10/19/2015 4:11:53PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:23:30AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2 ¦
¦e
o
o
1 -
Th-23;U-238
JILL
i i i i
U-235
U-234
Th-;Np-2;P O-209
m
P A IP 0-2 C m-24641
118
Cm-244
~ I
ThCm-242
u
i i i r
i i i
i i i i
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 21.00
Page 249 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
2.00
2.083E-003
1.804E-003
U-238
4,135.08
3,918.81
4,239.49
1.00
1.042E-003
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
4.00
4.167E-003
2.329E-003
Th-230
4,679.48
4,403.55
4,746.60
6.00
6.250E-003
2.756E-003
U-234
4,709.31
4,507.96
4,821.17
3.00
3.125E-003
2.083E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
1.00
1.042E-003
1.473E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
5.00
5.208E-003
2.552E-003
Am-243
5,231.34
5,052.36
5,305.92
4.00
4.167E-003
2.329E-003
U-232
5,253.71
5,059.82
5,402.86
4.00
4.167E-003
2.329E-003
Th-228
5,447.61
5,186.59
5,507.27
4.00
4.167E-003
2.329E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
0.00
0.000E+000
1.473E-003
Am-241
5,484.90
5,298.46
5,604.22
2.00
2.083E-003
1.804E-003
Cm-245
5,417.78
5,395.41
5,447.61
0.00
0.000E+000
1.473E-003
Pu-236
5,760.83
5,611.67
5,887.60
2.00
2.083E-003
1.804E-003
Cm-244
5,775.74
5,641.51
5,902.52
0.00
0.000E+000
1.473E-003
Th-227
6,074.04
5,932.35
6,178.45
0.00
0.000E+000
1.473E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 250 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV239
Comment:
Batch Name: June2016
Description:
Detector: AV239 , SN: 51-005EE1
Acquisition Start Date: 6/24/2016 4:15:30PM
Live Time: 960.00 min.
Real Time: 960.01 min.
Calibration Name: IC-9794;AV239-20151018
Calibration Date: 10/19/2015 4:11:57PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:17:44AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
Energy (keV)
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 19.00
Page 251 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
1.00
1.042E-003
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
0.00
0.000E+000
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
1.00
1.042E-003
1.473E-003
Pu-242
4,903.21
4,679.48
4,947.95
1.00
1.042E-003
1.473E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
1.00
1.042E-003
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
1.00
1.042E-003
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
0.00
0.000E+000
1.473E-003
U-232
5,253.71
5,059.82
5,402.86
3.00
3.125E-003
2.083E-003
Th-228
5,447.61
5,186.59
5,507.27
8.00
8.333E-003
3.125E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
8.00
8.333E-003
3.125E-003
Am-241
5,484.90
5,298.46
5,604.22
8.00
8.333E-003
3.125E-003
Cm-245
5,417.78
5,395.41
5,447.61
5.00
5.208E-003
2.552E-003
Pu-236
5,760.83
5,611.67
5,887.60
5.00
5.208E-003
2.552E-003
Cm-244
5,775.74
5,641.51
5,902.52
5.00
5.208E-003
2.552E-003
Th-227
6,074.04
5,932.35
6,178.45
0.00
0.000E+000
1.473E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 252 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV240
Comment:
Batch Name: June2016
Description:
Detector: AV240 , SN: 51-005Q1
Acquisition Start Date: 6/24/2016 4:15:30PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9795;AV240-20151018
Calibration Date: 10/19/2015 4:12:02PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:17:50 AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2 ¦
¦e
o
o
1 -
Th-23;U-238
J_L
U-235
Th-230
U-:Np-2;P O-209
it
P A IP 0-2 C m-24641
I
Cm-244
ThCm-242
u
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
I I I I I I 1 I I
I I I 1 I I I I I
I I I I I I I I
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 15.00
Page 253 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
1.00
1.042E-003
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
2.00
2.083E-003
1.804E-003
U-234
4,709.31
4,507.96
4,821.17
2.00
2.083E-003
1.804E-003
Pu-242
4,903.21
4,679.48
4,947.95
2.00
2.083E-003
1.804E-003
Th-229
4,858.46
4,739.14
5,119.48
2.00
2.083E-003
1.804E-003
Np-237
4,783.89
4,768.97
4,806.26
0.00
0.000E+000
1.473E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
1.00
1.042E-003
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
0.00
0.000E+000
1.473E-003
U-232
5,253.71
5,059.82
5,402.86
3.00
3.125E-003
2.083E-003
Th-228
5,447.61
5,186.59
5,507.27
4.00
4.167E-003
2.329E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
4.00
4.167E-003
2.329E-003
Am-241
5,484.90
5,298.46
5,604.22
4.00
4.167E-003
2.329E-003
Cm-245
5,417.78
5,395.41
5,447.61
4.00
4.167E-003
2.329E-003
Pu-236
5,760.83
5,611.67
5,887.60
1.00
1.042E-003
1.473E-003
Cm-244
5,775.74
5,641.51
5,902.52
1.00
1.042E-003
1.473E-003
Th-227
6,074.04
5,932.35
6,178.45
2.00
2.083E-003
1.804E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 254 of 551
-------
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
Sample Name: ICB;AV241
Comment:
Batch Name: June2016
Description:
Detector: AV241 , SN: 50-005P1
Acquisition Start Date: 6/24/2016 4:15:31PM
Live Time: 960.00 min.
Real Time: 960.00 min.
Calibration Name: IC-9817;AV241-20151018
Calibration Date: 10/19/2015 4:12:06PM
Alpha-Spectroscopy
Analysis Report
Sample
Batch
Acquisition
TestAmerica St. Louis
13715 Rider Trail North
Earth City, MO 63045
8:18:07 AM 6/25/2016
Spectrum #1 Analysis #1
Analyst: 60040
Energy Calibration Equation:
Gain = 7.4575 keV/Ch
Offset = 3,366.95 keV
Quadratic = 0.0000 keV / Ch2
2 ¦
¦e
o
o
1 -
Th-23;U-238
J_L
U-235
TU-:Np-2;P O-209
~ '*ih -ir i
P A IP 0-2 C m-24641
I iHI I HI II
Cm-244
ThCm-242
u
0
3374 3574 3774 3974 4174 4374 4574 4774 4974 5174 5374 5574 5774 5974 6174 6374 6574 6774 6974 7174
Energy (keV)
I I I I I I 1 I I
I I I I I I I
1 I I I I I I
General Analysis
Analysis Method: Absolute ROI Analysis, Set Name = 11/05_BackgroundFMWclide Library: Background ROI Library
Total Background Counts: 19.00
Page 255 of 551
-------
Nuclide Summary (ROI)
ReoionName
Peak Enerov
Start Enerov
End Enerov
GrossCounts
Count Rate
CR Uncertainty
(keV)
(keV)
(keV)
(CPM)
(CPM)
Th-232
3,985.93
3,754.75
4,053.05
0.00
0.000E+000
1.473E-003
U-238
4,135.08
3,918.81
4,239.49
0.00
0.000E+000
1.473E-003
U-235
4,358.81
4,261.86
4,463.21
0.00
0.000E+000
1.473E-003
Th-230
4,679.48
4,403.55
4,746.60
1.00
1.042E-003
1.473E-003
U-234
4,709.31
4,507.96
4,821.17
4.00
4.167E-003
2.329E-003
Pu-242
4,903.21
4,679.48
4,947.95
5.00
5.208E-003
2.552E-003
Th-229
4,858.46
4,739.14
5,119.48
5.00
5.208E-003
2.552E-003
Np-237
4,783.89
4,768.97
4,806.26
3.00
3.125E-003
2.083E-003
Po-209
4,918.12
4,903.21
4,933.04
0.00
0.000E+000
1.473E-003
Pu-239
5,179.14
4,970.33
5,238.80
0.00
0.000E+000
1.473E-003
Am-243
5,231.34
5,052.36
5,305.92
0.00
0.000E+000
1.473E-003
U-232
5,253.71
5,059.82
5,402.86
1.00
1.042E-003
1.473E-003
Th-228
5,447.61
5,186.59
5,507.27
2.00
2.083E-003
1.804E-003
Po-210
5,276.09
5,231.34
5,291.00
0.00
0.000E+000
1.473E-003
P u-238
5,469.98
5,268.63
5,552.01
2.00
2.083E-003
1.804E-003
Am-241
5,484.90
5,298.46
5,604.22
2.00
2.083E-003
1.804E-003
Cm-245
5,417.78
5,395.41
5,447.61
1.00
1.042E-003
1.473E-003
Pu-236
5,760.83
5,611.67
5,887.60
4.00
4.167E-003
2.329E-003
Cm-244
5,775.74
5,641.51
5,902.52
4.00
4.167E-003
2.329E-003
Th-227
6,074.04
5,932.35
6,178.45
0.00
0.000E+000
1.473E-003
Cm-242
6,148.62
6,118.79
6,178.45
0.00
0.000E+000
1.473E-003
Page 256 of 551
-------
Run Logs
Page 257 of 551
-------
Alpha Spectroscopy Run Log
Detector:
Analysis Date
10/16/15 16:27
Count
Minutes
140
Lab Sample ID
IC 160-223445/1
Client Sample ID
Analysis
Batch
223445
Prep
Batch
Method
Analyst
Initials
PS
10/26/15 19:10
60
ICV 160-223563/1
223563
PS
06/24/16 16:15
960
ICB 160-258037/1
258037
PS
06/27/16 10:48
60
CCV 160-258276/1
258276
PS
07/02/16 11:53
1
PULSER 160-259078/1
259078
07/02/16 12:40
1
PULSER 160-259078/2
259078
ALD
07/02/16 15:17
400
MB 160-257492/1-A
259078
257492
A-01-R
ALD
Detector: AV150
Analysis Date
10/16/15 15:51
Count
Minutes
140
Lab Sample ID
IC 160-223447/1
Client Sample ID
Analysis
Batch
223447
Prep
Batch
Method
Analyst
Initials
PS
10/26/15 19:10
60
ICV 160-223565/1
223565
PS
06/24/16 16:15
960
ICB 160-258039/1
258039
PS
06/27/16 10:49
60
CCV 160-258278/1
258278
PS
07/02/16 11:53
1
PULSER 160-259080/1
259080
ALD
07/02/16 15:17
400
LCS 160-257492/2-A
259080
257492
A-01-R
ALD
Detector: AV151
Analysis Date
10/16/15 15:51
Count
Minutes
140
Lab Sample ID
IC 160-223448/1
Client Sample ID
Analysis
Batch
223448
Prep
Batch
Method
Analyst
Initials
PS
10/26/15 19:11
60
ICV 160-223566/1
223566
PS
06/24/16 16:15
960
ICB 160-258040/1
258040
PS
06/27/16 10:49
60
CCV 160-258279/1
258279
PS
07/02/16 11:53
1
PULSER 160-259081/1
259081
ALD
07/02/16 15:17
400
160-17814-1
AC-SED-4
259081
257492
A-01-R
ALD
Detector: AV152
Analysis Date
10/16/15 15:52
Count
Minutes
140
Lab Sample ID
IC 160-223449/1
Client Sample ID
Analysis
Batch
223449
Prep
Batch
Method
Analyst
Initials
PS
10/26/15 19:11
60
ICV 160-223567/1
223567
PS
06/26/16 17:10
960
ICB 160-258131/1
258131
PS
06/27/16 10:49
60
CCV 160-258280/1
258280
PS
07/02/16 11:53
1
PULSER 160-259082/1
259082
ALD
07/02/16 15:17
400
160-17814-1 DU
AC-SED-4 DU
259082
257492
A-01-R
ALD
Detector: AV153
Analysis Date
10/16/15 15:52
Count
Minutes
140
Lab Sample ID
IC 160-223450/1
Client Sample ID
Analysis
Batch
223450
Prep
Batch
Method
Analyst
Initials
PS
10/26/15 19:11
60
ICV 160-223568/1
223568
PS
06/24/16 16:15
960
ICB 160-258042/1
258042
PS
06/27/16 10:50
60
CCV 160-258281/1
258281
PS
07/02/16 11:53
1
PULSER 160-259083/1
259083
ALD
07/02/16 15:17
400
160-17814-2
AC-SED-6
259083
257492
A-01-R
ALD
Detector: AW155
Analysis Date
Count
Minutes
Lab Sample ID
Client Sample ID
Analysis
Batch
Prep
Batch
Method
Analyst
Initials
10/16/15 15:52
140
IC 160-223452/1
223452
PS
Page 1 of 3
TestAmerica St. Louis
Page 258 of 551
-------
Alpha Spectroscopy Run Log
Detector: tiriuecl)
Analysis Date
10/26/15 19:12
Count
Minutes
60
Lab Sample ID
ICV 160-223570/1
Client Sample ID
Analysis
Batch
223570
Prep
Batch
Method
Analyst
Initials
PS
06/26/16 17:10
960
ICB 160-258132/1
258132
PS
06/27/16 10:50
60
CCV 160-258283/1
258283
PS
07/02/16 11:53
1
PULSER 160-259085/1
259085
ALD
07/02/16 15:17
400
160-17814-4
AC-SED-8
259085
257492
A-01-R
ALD
Detector: AV199
Analysis Date
10/17/15 18:15
Count
Minutes
140
Lab Sample ID
IC 160-223496/1
Client Sample ID
Analysis
Batch
223496
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 14:25
60
ICV 160-223614/1
223614
PS
06/24/16 16:15
960
ICB 160-258079/1
258079
PS
06/27/16 13:50
60
CCV 160-258308/1
258308
PS
07/07/16 08:33
1
PULSER 160-259665/1
259665
ALD
07/07/16 13:10
400
160-17814-3
AC-SED-7
259665
257492
A-01-R
ALD
Detector: AW235
Analysis Date
10/18/15 21:32
Count
Minutes
140
Lab Sample ID
IC 160-223531/1
Client Sample ID
Analysis
Batch
223531
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:30
60
ICV 160-223650/1
223650
PS
06/24/16 16:15
960
ICB 160-258114/1
258114
PS
06/27/16 18:53
60
CCV 160-258340/1
258340
PS
07/02/16 11:53
1
PULSER 160-259144/1
259144
ALD
07/02/16 15:31
nntnrtnr' A\/^
400
MB 160-257935/1-A
259144
257935
A-01-R
ALD
iiueiecioir., #4wi
Analysis Date
10/18/15 21:32
Count
Minutes
140
Lab Sample ID
IC 160-223532/1
Client Sample ID
Analysis
Batch
223532
Prep
Batch
Method
Analyst
Initials
PS
11/05/15 16:56
60
ICV 160-223666/1
223666
11/05/15 18:22
60
ICV 160-223666/2
223666
PS
06/24/16 16:15
960
ICB 160-258115/1
258115
PS
06/28/16 09:29
60
CCV 160-258356/1
258356
PS
07/02/16 11:53
1
PULSER 160-259145/1
259145
ALD
07/02/16 15:31
400
LCS 160-257935/2-A
259145
257935
A-01-R
ALD
Detector: AW237
Analysis Date
10/18/15 21:32
Count
Minutes
140
Lab Sample ID
IC 160-223533/1
Client Sample ID
Analysis
Batch
223533
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:31
60
ICV 160-223652/1
223652
PS
06/24/16 16:15
960
ICB 160-258116/1
258116
PS
06/27/16 18:53
60
CCV 160-258342/1
258342
PS
07/02/16 11:53
1
PULSER 160-259146/1
259146
ALD
07/02/16 15:31
nntortnr' A\/^
400
160-17814-1
AC-SED-4
259146
257935
A-01-R
ALD
UclctlUI . HVi
Analysis Date
10/18/15 21:32
Count
Minutes
140
Lab Sample ID
IC 160-223534/1
Client Sample ID
Analysis
Batch
223534
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:31
60
ICV 160-223653/1
223653
PS
Page 2 of 3
Page 259 of 551
TestAmerica St. Louis
-------
Alpha Spectroscopy Run Log
Detector: 238 (Continued)
Analysis Date
06/24/16 16:15
Count
Minutes
960
Lab Sample ID
ICB 160-258117/1
Client Sample ID
Analysis
Batch
258117
Prep
Batch
Method
Analyst
Initials
PS
06/27/16 18:53
60
CCV 160-258343/1
258343
PS
07/02/16 11:53
1
PULSER 160-259147/1
259147
ALD
07/02/16 15:31
400
160-17814-1 DU
AC-SED-4 DU
259147
257935
A-01-R
ALD
Detector: AV239
Analysis Date
10/18/15 21:33
Count
Minutes
140
Lab Sample ID
IC 160-223535/1
Client Sample ID
Analysis
Batch
223535
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:31
60
ICV 160-223654/1
223654
PS
06/24/16 16:15
960
ICB 160-258118/1
258118
PS
06/28/16 08:13
60
CCV 160-258357/1
258357
PS
07/02/16 11:53
1
PULSER 160-259148/1
259148
ALD
07/02/16 15:31
400
160-17814-2
AC-SED-6
259148
257935
A-01-R
ALD
Detector: AV240
Analysis Date
10/18/15 21:33
Count
Minutes
140
Lab Sample ID
IC 160-223536/1
Client Sample ID
Analysis
Batch
223536
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:31
60
ICV 160-223655/1
223655
PS
06/24/16 16:15
960
ICB 160-258119/1
258119
PS
06/28/16 08:13
60
CCV 160-258358/1
258358
PS
07/02/16 11:53
1
PULSER 160-259149/1
259149
ALD
07/02/16 15:31
400
160-17814-3
AC-SED-7
259149
257935
A-01-R
ALD
Detector: AV241
Analysis Date
10/18/15 21:33
Count
Minutes
140
Lab Sample ID
IC 160-223537/1
Client Sample ID
Analysis
Batch
223537
Prep
Batch
Method
Analyst
Initials
PS
11/01/15 20:32
60
ICV 160-223656/1
223656
PS
06/24/16 16:15
960
ICB 160-258120/1
258120
PS
06/28/16 08:21
60
CCV 160-258359/1
258359
PS
07/02/16 11:53
1
PULSER 160-259150/1
259150
ALD
07/02/16 15:31
400
160-17814-4
AC-SED-8
259150
257935
A-01-R
ALD
Page 3 of 3
Page 260 of 551
TestAmerica St. Louis
-------
GAMMA SPECTROSCOPY
Page 261 of 551
-------
Method GA-01-R
Ra-226
Radium-226 & Other Gamma Emitters
(GS) by Method GA-01-R
Page 262 of 551
-------
Prep Batch: 257060
Fill Geometry, 21-Day In-Growth
Page 263 of 551
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Lab ID: MB 160-257060/1 -A Analyzed: 07/11/16 07:43 Is: 30 Sigma: 2
Client ID: Detector: GV8 Decay Corrected: No
Analyte
MB Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
0.2838
0.646
0.647
U
pC
/g
1.10
0.511
259963
Radium-226
0.08999
0.0680
0.0687
U
pc
/g
0.315
0.146
259963
Radium-228
0.08187
0.179
0.179
u
pC
/g
0.246
0.0968
259963
Thorium-232
0.08187
0.179
0.179
u
pc
/g
0.246
0.0968
259963
Thorium-234
0.3719
0.986
0.987
u
pc
/g
1.46
0.672
259963
Thallium-208
0.05460
0.0364
0.0368
pc
/g
0.0718
0.0298
259963
Uranium-235
-0.001966
0.252
0.252
u
pc
/g
0.446
0.207
259963
Uranium-238
0.3719
0.986
0.987
u
pc
/g
1.46
0.672
259963
Actinium 228
0.08187
0.179
0.179
u
pc
/g
0.246
0.0968
259963
Bismuth-212
-0.05294
0.795
0.795
u
pc
/g
1.87
0.853
259963
Bismuth-214
0.08999
0.0680
0.0687
u
pc
/g
0.315
0.146
259963
Lead-210
-0.6987
1.04
1.04
u
pc
/g
2.36
1.10
259963
Lead-212
-0.09505
0.0534
0.0548
u
pc
/g
0.208
0.0981
259963
Lead-214
0.04168
0.104
0.104
u
pc
/g
0.185
0.0834
259963
Potassium-40
-0.1195
0.868
0.868
u
pc
/g
1.21
0.501
259963
Protactinium-231
0.5009
1.33
1.34
u
pc
/g
3.17
1.48
259963
Other Detected Radionuclides
MB Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Other Detected Radionuclide None pCi/g
Lab ID: LCS 160-257060/2-A Analyzed: Is: 30 Sigma: 2
Client ID: Detector: GV7 Decay Corrected: No
Analyte LCS Result Count Unc Total Unc Qualifier Unit MDC DLC Anly Batch
Americium-241 95.67 VA2 100 pCi/g T02 0.507 259965
Cesium-137 28.64 0.682 3.06 pCi/g 0.254 0.122 259965
Cobalt-60 15.99 0.423 1.66 pCi/g 0.0831 0.0341 259965
Lab ID: Analyzed: 07/11/16 07:46 Is: 30 Sigma: 2
Client ID: AC-SED-4 Detector: GV5 Decay Corrected: No
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
0.349
0.741
0.742
U
pCi/g
1.65
0.782
259964
Radium-226
1.14
0.273
0.298
pCi/g
0.220
0.0951
259964
Radium-228
1.17
0.272
0.297
pCi/g
0.179
0.0566
259964
Thorium-232
1.17
0.272
0.297
pCi/g
0.179
0.0566
259964
Thorium-234
2.37
1.73
1.75
pCi/g
2.20
1.03
259964
Page 1 of 6
Page 264 of 551
TestAmerica St. Louis
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Lab ID: Analyzed: 07/11/16 07:46 Is: 30 Sigma: 2
Client ID: AC-SED-4 Detector: GV5 Decay Corrected: No
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Thallium-208
0.365
0.115
0.121
¦Q I
o
/g
0.0879
0.0362
259964
Uranium-235
-0.263
0.652
0.652
U
pC
/g
1.09
0.527
259964
Uranium-238
2.37
1.73
1.75
pC
/g
2.20
1.03
259964
Actinium 228
1.17
0.272
0.297
pC
/g
0.179
0.0566
259964
Bismuth-212
0.743
2.03
2.03
U
pC
/g
3.45
1.62
259964
Bismuth-214
1.14
0.273
0.298
pC
/g
0.220
0.0951
259964
Lead-210
0.0417
2.66
2.66
u
pC
/g
3.93
1.87
259964
Lead-212
0.881
0.157
0.194
pC
/g
0.142
0.0638
259964
Lead-214
1.17
0.227
0.257
pC
/g
0.230
0.103
259964
Potassium-40
13.5
2.36
2.74
pC
/g
1.14
0.438
259964
Protactinium-231
-1.65
4.78
4.78
u
pC
/g
8.03
3.88
259964
Other Detected Radionuclides
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Other Detected Radionuclide None pCi/g
Lab ID: DU Analyzed: 07/11/16 03:47 Is: 30 Sigma: 2
Client ID: AC-SED-4 Detector: GV7 Decay Corrected: No
Analyte
DU Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
-0.4288
1.04
1.04
U
pC
/g
1.40
0.667
259965
Radium-226
1.230
0.209
0.245
pC
/g
0.107
0.0436
259965
Radium-228
0.8354
0.233
0.249
pC
/g
0.201
0.0782
259965
Thorium-232
0.8354
0.233
0.249
pC
/g
0.201
0.0782
259965
Thorium-234
-0.02837
1.32
1.32
U
pC
/g
2.26
1.09
259965
Thallium-208
0.2425
0.0773
0.0812
pC
/g
0.0715
0.0306
259965
Uranium-235
-0.1956
0.342
0.343
u
pC
/g
1.02
0.495
259965
Uranium-238
-0.02837
1.32
1.32
u
pC
/g
2.26
1.09
259965
Actinium 228
0.8354
0.233
0.249
pC
/g
0.201
0.0782
259965
Bismuth-212
0.4704
0.803
0.805
u
pC
/g
1.36
0.610
259965
Bismuth-214
1.230
0.209
0.245
pC
/g
0.107
0.0436
259965
Lead-210
0.05687
2.06
2.06
u
pC
/g
3.51
1.68
259965
Lead-212
0.8705
0.138
0.178
pC
/g
0.147
0.0686
259965
Lead-214
1.133
0.182
0.217
pC
/g
0.165
0.0750
259965
Potassium-40
14.87
2.15
2.64
pC
/g
1.03
0.424
259965
Protactinium-231
-1.029
3.40
3.40
u
pC
/g
5.70
2.77
259965
Other Detected Radionuclides
DU Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Other Detected Radionuclide None pCi/g
Page 2 of 6 TestAmerica St. Louis
Page 265 of 551
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Lab ID: 160-17314-2 Analyzed: 07/11/16 07:46 Is: 30 Sigma:
Client ID: AC-SED-6 Detector: GV3 Decay Corrected: No
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
0.409
0.557
0.559
U
pC
/g
0.923
0.425
259962
Radium-226
0.958
0.195
0.219
pc
/g
0.159
0.0698
259962
Radium-228
0.783
0.229
0.242
pC
/g
0.262
0.110
259962
Thorium-232
0.783
0.229
0.242
pc
/g
0.262
0.110
259962
Thorium-234
0.834
0.741
0.746
U
pc
/g
2.12
1.00
259962
Thallium-208
0.361
0.114
0.120
pc
/g
0.100
0.0447
259962
Uranium-235
0.102
0.190
0.190
u
pc
/g
0.951
0.460
259962
Uranium-238
0.834
0.741
0.746
u
pc
/g
2.12
1.00
259962
Actinium 228
0.783
0.229
0.242
pc
/g
0.262
0.110
259962
Bismuth-212
0.312
1.14
1.14
u
pc
/g
1.96
0.912
259962
Bismuth-214
0.958
0.195
0.219
pc
/g
0.159
0.0698
259962
Lead-210
1.13
1.68
1.68
u
pc
/g
2.75
1.30
259962
Lead-212
0.907
0.145
0.186
pc
/g
0.141
0.0648
259962
Lead-214
1.21
0.231
0.263
pc
/g
0.191
0.0875
259962
Potassium-40
17.0
2.11
2.73
pc
/g
1.01
0.420
259962
Protactinium-231
-0.00000013
3.54
3.54
u
pc
/g
6.02
2.92
259962
Other Detected Radionuclides
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Other Detected Radionuclide None pCi/g
Lab ID: 160-17314-3 Analyzed: 07/11/16 03:45 Is: 30 Sigma: 2
Client ID: AC-SED-7 Detector: GV8 Decay Corrected: No
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
0.600
1.27
1.27
U
¦Q I
o
/g
2.13
1.03
259963
Radium-226
1.07
0.247
0.271
pC
/g
0.194
0.0858
259963
Radium-228
0.750
0.243
0.255
pC
/g
0.426
0.188
259963
Thorium-232
0.750
0.243
0.255
pC
/g
0.426
0.188
259963
Thorium-234
0.970
0.746
0.752
U
pc
/g
2.06
0.971
259963
Thallium-208
0.336
0.0884
0.0950
pc
/g
0.0672
0.0276
259963
Uranium-235
-0.344
0.443
0.444
u
pc
/g
1.33
0.651
259963
Uranium-238
0.970
0.746
0.752
u
pc
/g
2.06
0.971
259963
Actinium 228
0.750
0.243
0.255
pc
/g
0.426
0.188
259963
Bismuth-212
-0.813
1.72
1.73
u
pc
/g
2.69
1.27
259963
Bismuth-214
1.07
0.247
0.271
pc
/g
0.194
0.0858
259963
Lead-210
-1.56
1.73
1.74
u
pc
/g
5.63
2.73
259963
Lead-212
0.759
0.134
0.166
pc
/g
0.128
0.0582
259963
Page 3 of 6
TestAmerica St. Louis
Page 266 of 551
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Lab ID: 160-17314-3 Analyzed: 07/11/16 03:45 Is: 30 Sigma:
Client ID: AC-SED-7 Detector: GV8 Decay Corrected: No
Analyte
Result Count Unc Total Unc Qualifier Unit
Lead-214
Potassium-40
Protactinium-231
1.39
16.2
0.568
Other Detected Radionuclides
Other Detected Radionuclide
MDC
0.188
2.24
2.29
Result
None
0.238 pCi/g
2.79 pCi/g
2.29 U pCi/g
Count Unc Total Unc Qualifier
0.175
0.731
7.33
Unit
pCi/g
DLC Anly Batch
0.0785 259963
0.262 259963
3.56 259963
DLC
Lab ID: 16 Analyzed: 07/11/16 03:46 Is: 30 Sigma: 2
Client ID: AC-SED-3 Detector: GV5 Decay Corrected: No
Analyte
Result
Count Unc
Total Unc
Qualifier
Unit
MDC
DLC
Anly Batch
Actinium-227
1.14
1.08
1.09
pC
/g
1.48
0.684
259964
Radium-226
1.42
0.310
0.343
pc
/g
0.228
0.0959
259964
Radium-228
0.921
0.314
0.327
pC
/g
0.355
0.137
259964
Thorium-232
0.921
0.314
0.327
pc
/g
0.355
0.137
259964
Thorium-234
-1.10
1.68
1.68
U
pc
/g
3.92
1.87
259964
Thallium-208
0.398
0.105
0.113
pc
/g
0.0522
0.0165
259964
Uranium-235
0.239
0.632
0.632
U
pc
/g
1.07
0.509
259964
Uranium-238
-1.10
1.68
1.68
u
pc
/g
3.92
1.87
259964
Actinium 228
0.921
0.314
0.327
pc
/g
0.355
0.137
259964
Bismuth-212
-0.608
1.86
1.86
u
pc
/g
2.86
1.30
259964
Bismuth-214
1.42
0.310
0.343
pc
/g
0.228
0.0959
259964
Lead-210
3.66
2.62
2.66
pc
/g
3.47
1.62
259964
Lead-212
1.04
0.194
0.236
pc
/g
0.183
0.0828
259964
Lead-214
1.62
0.253
0.305
pc
/g
0.264
0.118
259964
Potassium-40
17.0
2.95
3.43
pc
/g
1.41
0.541
259964
Protactinium-231
-1.57
4.39
4.39
u
pc
/g
7.42
3.54
259964
Other Detected Radionuclides
Result
Count Unc
Total Unc
Qualifier
Unit
DLC
Other Detected Radionuclide None pCi/g
Page 4 of 6
Page 267 of 551
TestAmerica St. Louis
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Quail ntrol Summary
Method Blank ID:
Analyte
Parent Result
Spike Added
MB Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER RER Limit Z Factor
MB 160-257060/1-A
Actinium-227
0.2838
U
pCi/g
.8776796
1
2.621098
74
.9162139
1
.9162139
1
.7536209
7
2.964314
69
-.0156251
MB 160-257060/1-A
Radium-226
0.08999
U
pCi/g
MB 160-257060/1-A
Radium-228
0.08187
u
pCi/g
MB 160-257060/1-A
Thorium-232
0.08187
u
pCi/g
MB 160-257060/1-A
Thorium-234
0.3719
u
pCi/g
MB 160-257060/1-A
Thallium-208
0.05460
pCi/g
MB 160-257060/1-A
Uranium-235
-0.001966
u
pCi/g
MB 160-257060/1-A
Uranium-238
0.3719
u
pCi/g
.7536209
7
.9162139
1
-.1332121
1
2.621098
74
-1.340117
96
-3.466679
77
.8046230
MB 160-257060/1-A
Actinium 228
0.08187
u
pCi/g
MB 160-257060/1-A
Bismuth-212
-0.05294
u
pCi/g
MB 160-257060/1-A
Bismuth-214
0.08999
u
pCi/g
MB 160-257060/1-A
Lead-210
-0.6987
u
pCi/g
MB 160-257060/1-A
Lead-212
-0.09505
u
pCi/g
MB 160-257060/1-A
Lead-214
0.04168
u
pCi/g
MB 160-257060/1-A
Potassium-40
-0.1195
u
pCi/g
-.2753985
MB 160-257060/1-A
Protactinium-231
0.5009
u
pCi/g
.7499269
4
Lab Control Sample ID:
Analyte
Parent Result
Spike Added
LCS Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER RER Limit Z Factor
ICS 160-257060/2-A
ICS 160-257060/2-A
ICS 160-257060/2-A
Americium-241
Cesium-137
Cobalt-60
97.1
29.6
16.9
95.67
28.64
15.99
pCi/g
pCi/g
pCi/g
99
97
94
87-116
87 -120
87-115
-.2029023
205
-.4349387
734
-.7816121
071
Duplicate ID:
Analyte
Parent Result
Spike Added
DU Result
Qualifier
Unit
% Rec
% Rec Limits
RPD
RER
DER RER Limit Z Factor
160-17814-1
Actinium-227
0.349
-0.4288
U
pCi/g
1944
0.44
1.22 1
160-17814-1
Radium-226
1.14
1.230
pCi/g
7
0.16
0.44 1
160-17814-1
Radium-228
1.17
0.8354
pCi/g
33
0.61
1.71 1
160-17814-1
Thorium-232
1.17
0.8354
pCi/g
33
0.61
1.71 1
160-17814-1
Thorium-234
2.37
-0.02837
u
pCi/g
205
0.78
2.19 1
160-17814-1
Thallium-208
0.365
0.2425
pCi/g
40
0.61
1.69 1
Page 5 of 6
TestAmerica St. Louis
Page 268 of 551
-------
Gamma Spectroscopy Analysis Detail Report
Prep Batch: 257060
Duplicate ID:
Analyte
Parent Result Spike Added
DU Result
Qualifier
Unit
% Rec % Rec Limits
RPD
RER
DER
160-17814-1
Uranium-235
-0.263
-0.1956
U
¦Q I
o
/g
29
0.07
0.18
160-17814-1
Uranium-238
2.37
-0.02837
U
pC
/g
205
0.78
2.19
160-17814-1
Actinium 228
1.17
0.8354
pC
/g
33
0.61
1.71
160-17814-1
Bismuth-212
0.743
0.4704
u
pC
/g
45
0.1
0.25
160-17814-1
Bismuth-214
1.14
1.230
pC
/g
7
0.16
0.44
160-17814-1
Lead-210
0.0417
0.05687
u
pC
/g
31
0
0.01
160-17814-1
Lead-212
0.881
0.8705
pC
/g
1
0.03
0.08
160-17814-1
Lead-214
1.17
1.133
pC
/g
3
0.07
0.20
160-17814-1
Potassium-40
13.5
14.87
pC
/g
10
0.26
0.73
160-17814-1
Protactinium-231
-1.65
-1.029
u
pC
/g
47
0.08
0.21
Glossary:
RER Limit Z Factor
Ts = Count Duration, Sample
Page 6 of 6
Page 269 of 551
TestAmerica St. Louis
-------
GAMMA SPECTROSCOPY BATCH WORKSHEET
Lab Name: TestAmerica St. Louis Job No.: 160-17814-1
SDG No.:
Batch Number: 257060 Batch Start Date: 06/20/16 08:50 Batch Analyst: Sloan, Robert 1
Batch Method: Fill Geo-21 Batch End Date: 06/20/16 10:00
Lab Sample ID
Client Sample ID
Method Chain
Basis
TareWeight
GrossWeight
InitialAmount
IngDecDatel
IngDecDate3
Geometry
MB 160-257060/1
Fill Geo-21,
GA-01-R
291.18 g
6/20/2016
7/11/2016
Tuna Can
LCS
160-257060/2
Fill Geo-21,
GA-01-R
341.9 g
6/20/2016
7/11/2016
Tuna Can
160-17814-A-l-A
AC-SED-4
Fill Geo-21,
GA-01-R
T
46.3 g
327 3 g
281 g
6/20/2016
7/11/2016
Tuna Can
160-17814-A-l-A
DU
AC-SED-4
Fill Geo-21,
GA-01-R
T
46.3 g
327 3 g
281 g
6/20/2016
7/11/2016
Tuna Can
160-17814-A-2-A
AC-SED-6
Fill Geo-21,
GA-01-R
T
4 6.8 g
325.0 g
278.2 g
6/20/2016
7/11/2016
Tuna Can
160-17814-A-3-A
AC-SED-7
Fill Geo-21,
GA-01-R
T
46.2 g
346.2 g
300 g
6/20/2016
7/11/2016
Tuna Can
160-17814-A-4-A
AC-SED-8
Fill Geo-21,
GA-01-R
T
46.3 g
273.7 g
227.4000 g
6/20/2016
7/11/2016
Tuna Can
Lab Sample ID
Client Sample ID
Method Chain
Basis
Tuna Can LCS
00005
MB 160-257060/1
Fill Geo-21,
GA-01-R
LCS
160-257060/2
Fill Geo-21,
GA-01-R
# g
160-17814-A-l-A
AC-SED-4
Fill Geo-21,
GA-01-R
T
160-17814-A-l-A
DU
AC-SED-4
Fill Geo-21,
GA-01-R
T
160-17814-A-2-A
AC-SED-6
Fill Geo-21,
GA-01-R
T
160-17814-A-3-A
AC-SED-7
Fill Geo-21,
GA-01-R
T
160-17814-A-4-A
AC-SED-8
Fill Geo-21,
GA-01-R
T
Batch Notes
Balance ID
1121432711
SOP Number
ST-RC-0003 ST-RC-0025
Basis
Basis Description
T
Total/NA
The pound sign (#) in the amount added field denotes that the reagent was used undiluted. All calculations are performed using the stated
this reagent.
GA-01-R
for
Page 1 of 1
Page 270 of 551
-------
Test America St. Louis Spectrum ID: 8_Gamma_2 016 0992
Sample Description: 257060_Gamma_MB 160-257060-1-A
Detector: Detector # 8
Batch ID: 257060
Work Order Number: Gamma
Lot Number: MB 160-257060~1-A
Decay to Time: 7/11/2016 07:48 Live Time: 1800 sec
Acquisition Time: 7/11/2016 07:48:49 Real Time: 1854 sec
Analysis Time: 7/11/2016 08:19 Dead Time: 2.89 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
8_Soil_TunaCan.Clb
8_Soil_TunaCan_90099_032 712
3/28/2012 10:35
2/28/2012 10:34
Client_Long_Revll.lib
8 2016-07-10 1451.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
5 . 569E-01
399 . 5
2 . 225E+00
2.225E+00
8.098E+00
NA-22
0.000E+00
1.#INF
8.011E-02
8.011E-02
5.904E-01
K-40
-1.288E+00
363 .1
4.676E+00
4.677E+00
1.3 08E+01
Sc-46
7 . 089E-03
8385 . 0
5.944E-01
5.944E-01
2.116E+00
CR-51
-2 .164E+00
75 . 8
1.639E+00
1.644E+00
7.776E+00
MN-54
1.302E-01
207 . 0
2.696E-01
2.697E-01
7.132E-01
FE-59
-6 . 863E-01
123 .2
8.456E-01
8.463E-01
2.222E+00
Co - 56
2.3 06E-01
124 . 1
2.863E-01
2.866E-01
7.373E-01
CO - 57
0.000E+00
1.#INF
4.951E-02
4.951E-02
5.372E-01
CO - 58
6.570E-01
28 . 9
1.897E-01
1.927E-01
4.035E-01
CO-6 0
-2.444E-01
133 .3
3.258E-01
3.260E-01
8.901E-01
ZN-65
0.000E+00
1.#INF
1.411E-01
1.411E-01
2.3 55E+00
NB-94
6.932E-02
39 . 5
2.735E-02
2.759E-02
8.362E-01
ZR-95
-9.970E-01
92 . 0
9.177E-01
9.191E-01
2.156E+00
NB-95
0.000E+00
1.#INF
5.202E-02
5.202E-02
1.069E+00
RU-103
-3 . 862E-01
103 .4
3.994E-01
3.999E-01
9.749E-01
RH-106
0.000E+00
1.#INF
4.3 96E-01
4.3 96E-01
1.553E+01
AG-108M
1. 53IE-01
149 . 8
2.293E-01
2.294E-01
5.927E-01
AG-110M
1.955E-01
80 . 5
1.574E-01
1.577E-01
2.902E+00
SN-113
2.068E-01
143 . 8
2.975E-01
2.977E-01
1.052E+00
SB-124
3.687E-01
114 . 6
4.226E-01
4.23 0E-01
1.429E+00
SB-125
9 .499E-01
61.2
5.813E-01
5.833E-01
1.3 07E+00
1-131
9 . 822E-02
103 . 0
1.012E-01
1.013E-01
7.388E-01
Gd-153
0.000E+00
1.#INF
8.961E-02
8.962E-02
3.365E+00
Ga-6 8
-7.408E+00
238 . 8
1.769E+01
1.770E+01
4.308E+01
Tc-99m
-1. 527E-02
1994.6
3.045E-01
3.045E-01
1.046E+00
BA-133
-1. 547E-02
131. 6
2.036E-02
2.038E-02
1.450E+00
CS-134
1. 220E-01
112 .1
1.368E-01
1.369E-01
1.544E+00
CS-137
-1.067E-01
324 . 9
3.467E-01
3.467E-01
1.3 03E+00
CE-139
1. 274E-01
130.2
1.659E-01
1.664E-01
5.738E-01
Ba-140
7 . 947E-01
177 . 8
1.413E+00
1.413E+00
2.621E+00
La-140
1. 138E-01
138 . 9
1.580E-01
1.581E-01
7.522E-01
CE-141
-3 . 561E-01
106 . 0
3.776E-01
3.780E-01
9.856E-01
(Page 1 of 20)
Page 271 of 551
-------
CE-144
-8 . 692E-01
247 . 8
2 . 154E+00
2.154E+00
7.3 51E+00
PM-144
-1.938E-01
204 . 6
3 . 965E-01
3.966E-01
9.759E-01
EU-152
1. 649E+00
33 .3
5 . 496E-01
5.563E-01
3.837E+00
EU-154
-2 . 553E+00
51. 9
1.326E+00
1.332E+00
9.340E+00
EU-155
0.000E+00
1.#INF
1.534E-01
1.534E-01
4.703E+00
HF-181
0 . 000E+00
1.#INF
1.078E-01
1.078E-01
1.103E+00
Ta-182
0.000E+00
1.#INF
2.055E-01
2.055E-01
3.429E+00
Hg-203
0 . 000E+00
1.#INF
1.686E-01
1.686E-01
8.726E-01
TL-208
5 . 882E-01
33 .3
1.961E-01
1.984E-01
7.739E-01
pm-146
7 . 430E-01
40 . 8
3.033E-01
3.058E-01
1.911E+00
y-88
-8 . 479E-02
755 . 1
6.403E-01
6.403E-01
1.074E+00
Cd-113m
7 . 295E+02
393 . 7
2.872E+03
2.872E+03
1.03 0E+04
Cd-109
-3 . 062E+00
261.2
7.997E+00
7.999E+00
2.711E+01
Cf-251
-3 . 778E-01
225 . 0
8.501E-01
8.507E-01
2.320E+00
Cf-249
2 . 844E-01
149 . 9
4.264E-01
4.266E-01
1.183E+00
Sn-126
-1.948E+00
139 . 7
2.722E+00
2.724E+00
9.246E+00
PB-210
-7 . 528E+00
74 . 4
5.600E+00
5.617E+00
2.540E+01
PB-212
-1. 024E+00
28 . 1
2.879E-01
2.954E-01
2.241E+00
PB-214
4 . 490E-01
124 .2
5.575E-01
5.580E-01
1.996E+00
BI-207
-1. 122E-01
249.2
2.795E-01
2.796E-01
9.498E-01
BI-212
-5 . 704E-01
750 . 7
4.282E+00
4.282E+00
2.016E+01
BI-214
9 . 695E-01
37 . 8
3.664E-01
3.699E-01
3.3 95E+00
BI-210M
-2 . 202E-01
170 . 9
3.763E-01
3.766E-01
1.316E+00
AC-228
8 . 820E-01
109 . 0
9.617E-01
9.627E-01
2.647E+00
TH -7.7.1
3.057E+00
113 . 8
3.479E+00
3.483E+00
1.184E+01
TH-229
3.000E+00
110 . 5
3.317E+00
3.326E+00
8.869E+00
TH-234
4.007E+00
132 . 6
5.313E+00
5.317E+00
1.576E+01
PA-2 31
5.3 96E+00
133 .2
7.190E+00
7.196E+00
3.419E+01
PA-233
3 .147E-01
188 . 5
5.933E-01
5.936E-01
3.142E+00
PA-2 3 4
-2 . 923E-01
143 . 5
4.194E-01
4.197E-01
4.158E+00
PA-234M
-3 . 424E+00
1387 . 0
4.749E+01
4.749E+01
1.767E+02
U-235
-2 . 119E-02
6399.9
1.3 56E+00
1.3 56E+00
4.806E+00
AM-2 41
-1.646E-01
426 .3
7.019E-01
7.019E-01
2.471E+00
Np-237
-1.401E+00
182 . 6
2.558E+00
2.559E+00
8.622E+00
Ir-192
5 . 413E-02
116 . 5
6.3 04E-02
6.312E-02
1.221E+00
Cs-136
-9 . 186E-02
106 . 8
9.806E-02
9.820E-02
1.344E+00
Np-239
-8 . 605E-01
143 .1
1.231E+00
1.232E+00
4.147E+00
Nd-147
3 . 833E+00
27 . 7
1.063E+00
1.086E+00
2.173E+00
Total 7.595E+02
Analyst: Amanda Dick
(Page 2 of 20)
Page 272 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 1
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
Sample description
257060 Gamma MB 160-257060-1-A
Spectrum Filename: C:\User\SPC\Det8\8_Gamma_20160992.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 7:48:49 AM
1800
1854
2.89 %
Detector system
Ge 8 SN/174
Calibration
Filename:
8 Soil TunaCan 90099 032712
8 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 10:34:41 AM
0.052 keV
0.250 keV/channel
5.282E-10 keV/channel^2
3/28/2012 10:35:20 AM
165.85 keV
Quadratic Uncertainty = 1.3 9
-1.098764E-01 + (-4.958544E-01*Log(E) )
( -2.572270E-02*Log(E)^2 )
Quadratic Uncertainty = 1.71
-2.525301E+01 + ( 9.3 982 53E+00*Log(E) )
( -1.000034E+00*Log(E)^2 )
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 37.55keV )
8000 ( 1999.97keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
(Page 3 of 20)
Page 273 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:19:58 AMPage 2
Spectrum name: 8_Gamma_2 016 0992.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 7:48:00 AM
8_2016 - 07 -10_1451.PBC
7/10/2016 2:51:27 PM
total peaks alloc. 3 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.0957
* * * * * g
U M M A
R Y 0
F P E
A K S I
Peak
Area
Uncert
FWHM
Corrctn
Energy
Factor
50 .14
10 .
. 113.81
1. 01
2.267E-02
59 . 54
-3 .
. 426.34
1. 02
2.881E-02
63 .40
9 .
. 132.59
0 . 62
3 . 099E-02
121.78
2 .
. 474.34
1. 07
4.148E-02
123.10
8 .
90.89
1. 07
4.138E-02
165 . 85
7 .
. 130.22
1. 10
3 . 629E-02
185.53
7 .
. 114.31
0 .67
3 .332E-02
193 . 51
8 .
. 110.55
1.13
3 . 226E-02
205.33
-3 .
. 367.79
1.13
3.083E-02
263.70
2 .
. 393.70
1.18
2 . 539E-02
295.09
6 .
. 163.52
1.20
2 . 324E-02
300.03
6 .
. 169.73
1.20
2 . 294E-02
300.07
6 .
. 179.40
1.20
2 . 293E-02
300.18
6 .
. 188.55
1.20
2 . 293E-02
N
r RAN
G E
* * * * *
Nuclide
Brnch.
Act.
Nuc
Energy
Ratio
Bq/Sampl
50 . 14
8 . 000
PBC
-------
ORTEC g v - i
TestAmerica Inc
(3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 3
Spectrum name: 8_Gamma_2 016 0992.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
302.65
6 .
197.03
1.21
2.278E-02
302.65
2 . 880
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 4
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
1063.66
-3 .
217.33
1. 71
8 .106E-03
1063.66
74 . 500
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
5
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
PA-2 3 4
525 . 00
131.29
124 .
-11.
-0.006
143 .49
1. 078s
HF-181
531. 92
133.02
136 .
-11.
-0 . 006
149.38
1.079s
CE-144
533.98
133.54
147 .
-7 .
-0.004
247.81
1.080s
HF-181
545.02
136 .30
154 .
0 .
0 . 000
1000 . 00
1.082s
CO - 57
545.72
136.47
163 .
-12 .
-0.007
154 .46
1.082s
CE-141
581. 59
145.44
43 .
-12 .
-0 . 007
106.03
1.089s
Ba-140
650.47
162.66
67 .
-12 .
-0.007
99 . 56
1.102s
U-235
653.35
163 .38
82 .
-8 .
-0.004
139.10
1.102s
CE-13 9
663 .24
165.85
34 .
7 .
0 . 004
130.22
1.104
Cf-251
706.23
176.60
22 .
-4 .
-0.002
225 . 00
1.112s
TH-229
773.87
193.51
18 .
8 .
0 . 004
110.55
1.125s
U-235
821.17
205.33
29 .
-3 .
-0.001
367 . 79
1.134
TH-229
843.24
210.85
40 .
-7 .
-0 . 004
180 . 89
1.138s
Cf-251
907 . 84
227.00
28 .
-4 .
-0.002
263.79
1.151s
PB-212
954 .37
238 . 63
94 .
-22 .
-0.012
28 .11
1.159s
PB-214
967 . 84
242.00
98 .
-13 .
-0.007
112 . 99
1.162s
EU-152
978.62
244 .69
107 .
-7 .
-0 . 004
208 .15
1.164s
TH-227
1024.81
256 .24
20 .
-2 .
-0.001
443 .47
1.172s
Cd-113m
1054.65
263.70
30 .
2 .
0 . 001
393.70
1.178s
BI-210M
1063.18
265.83
34 .
-5 .
-0.003
170 . 88
1.179
TL-208
1108.99
277.28
32 .
-5 .
-0.003
114.12
1.188s
Hg-203
1116 . 66
279.20
37 .
0 .
0 . 000
1000 . 00
1.189s
1-131
1137.05
284 .30
24 .
-8 .
-0.004
125 . 00
1.193s
PB-214
1180.22
295.09
44 .
6 .
0 . 003
163.52
1.201s
PB-212
1199.98
300.03
48 .
6 .
0 . 003
169.73
1.205s
PA-2 31
1200.14
300.07
53 .
6 .
0 . 003
179.40
1.205s
PA-233
1200 . 58
300.18
59 .
6 .
0 . 003
188.55
1.205s
PA-2 31
1210.46
302 .65
65 .
6 .
0 . 003
197.03
1.207s
BA-133
1211.27
302.85
71.
6 .
0 . 003
205.38
1.207s
Ba-140
1219.26
304.85
77 .
6 .
0 . 003
218 . 51
1.208s
Ir-192
1233 . 62
308.44
83 .
0 .
0 . 000
1000.00
1.211s
Ir-192
1265 . 82
316.49
71.
-3 .
-0.002
362.49
1.217s
CR-51
1280.20
320 . 08
35 .
-8 .
-0.005
75 . 77
1.219s
La-140
1314.91
328.76
32 .
6 .
0 . 003
138 . 85
1.226s
Cf-249
1333 . 63
333 .44
38 .
6 .
0 . 003
149.92
1.229s
AC-228
1353.15
338 .32
44 .
6 .
0 . 003
160 .14
1.233s
Cs-136
1362 .15
340 . 57
50 .
6 .
0 . 003
169 . 92
1.234s
EU-152
1377.01
344 .29
56 .
6 .
0 . 003
178.97
1.237s
HF-181
1383.19
345 . 83
138 .
-11.
-0.006
148 . 66
1.238s
PB-214
1407.60
351.93
28 .
4 .
0 . 002
186.91
1.243s
BA-133
1423 . 87
356.00
41.
-6 .
-0.003
164.60
1.245s
1-131
1457.81
364 .48
16 .
-4 .
-0.002
202.07
1.252
BA-133
1535.24
383 . 84
20 .
6 .
0 . 003
113.06
1.266s
Cf-249
1551.68
387 . 95
26 .
2 .
0 . 001
299.38
1.269s
SN-113
1566 . 64
391.69
18 .
4 .
0 . 002
143 . 85
1.271s
SB-125
1711.39
427.88
4 .
5 .
0 . 003
98 . 79
1.297s
AG-108M
1735.64
433.94
9 .
4 .
0 . 002
149.80
1.301s
pm-146
1815.41
453 . 88
14 .
-5 .
-0.003
135.31
1.315s
(Page 7 of 20)
Page 277 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
6
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
SB-125
1853 .36
463 .37
8 .
5 .
0 . 003
100.56
1.322s
Ir-192
1872.14
468.06
12 .
5 .
0 . 003
116 .47
1.325s
BE - 7
1910.28
477.60
21.
2 .
0 . 001
399 . 50
1.332s
HF-181
1927.89
482.00
23 .
0 .
0 . 000
1000.00
1.335s
La-140
1947.98
487.02
23 .
0 .
0 . 000
1000.00
1.339s
RU-103
1988.12
497.05
22 .
-10 .
-0.005
103 .42
1.346s
RH-106
2047.36
511.86
14 .
24 .
0 . 013
45 . 58
2 . 606s
Nd-147
2123.91
531.00
0 .
13 .
0 . 007
27 . 74
1.369s
Ba-140
2148.95
537.26
9 .
2 .
0 . 001
280.50
1.373s
CS-134
2252.86
563.24
18 .
-4 .
-0.002
161.84
1.391s
CS-134
2277.20
569.32
13 .
-2 .
-0.001
264.58
1.395s
BI-207
2278.73
569.70
19 .
-3 .
-0.002
249.21
1.396s
TL-208
2332.01
583.02
8 .
1.
0 . 001
394 . 86
1.405s
SB-125
2401.92
600.50
19 .
5 .
0 . 003
133.56
1.416s
SB-124
2410.85
602.73
42 .
7 .
0 . 004
141. 69
1.418s
CS-134
2418.76
604.71
49 .
0 .
0 . 000
1000 . 00
1.419s
BI-214
2437.17
609.31
52 .
-3 .
-0.002
173.68
1.422s
RU-103
2441.12
610.30
49 .
0 .
0 . 000
1000 . 00
1.423s
AG-108M
2457.05
614.28
49 .
0 .
0 . 000
1000.00
1.426s
PM-144
2472.18
618 . 06
49 .
0 .
0 . 000
1000 . 00
1.428s
RH-106
2487.60
621.92
49 .
0 .
0 . 000
1000.00
1.431s
SB-125
2543.49
635 . 89
11.
3 .
0 . 002
149.00
1.440s
1-131
2547.83
636.97
8 .
4 .
0 . 002
103.04
1.441s
AG-110M
2630.98
657.76
13 .
7 .
0 . 004
80 . 50
1.455s
CS-137
2646 . 58
661. 66
21.
-2 .
-0.001
324 . 88
1.457s
PM-144
2786.11
696.54
14 .
-4 .
-0 . 002
204 . 63
1.480s
NB-94
2810.46
702 . 63
9 .
-5 .
-0.003
129.00
1.484s
SB-124
2891.09
722.79
8 .
2 .
0 . 001
180.14
1.497s
AG-108M
2891.70
722.94
10 .
0 .
0 . 000
1000 . 00
1.498s
EU-154
2893.37
723 .36
25 .
-9 .
-0.005
84 . 94
1.498s
ZR-95
2896.74
724.20
29 .
-6 .
-0 . 003
137.80
1.498s
BI-212
2908.63
727.17
36 .
-1.
0 . 000
750 . 66
1. 500
pm-146
2942.83
735.72
0 .
6 .
0 . 003
40 . 82
1. 506s
pm-146
2988.59
747.16
5 .
2 .
0 . 001
207.02
1. 513s
ZR-95
3026.87
756.73
19 .
-11.
-0.006
92 . 04
1.519s
AG-110M
3055.73
763.94
12 .
-2 .
-0.001
222.69
1.524s
NB-95
3063.11
765 . 79
15 .
0 .
0 . 000
1000 . 00
1.525s
PA-234M
3065.60
766 .41
21.
-7 .
-0.004
96 .38
1. 526s
EU-152
3115.64
778.92
5 .
1.
0 . 001
354.44
1.534s
CS-134
3183.43
795 . 87
9 .
4 .
0 . 002
112.14
1.544s
CS-134
3207.77
801.95
4 .
0 .
0 . 000
1000 . 00
1. 548s
CO - 58
3243 . 06
810.78
0 .
12 .
0 . 007
28 . 87
1. 554
La-140
3263.04
815.77
12 .
0 .
0 . 000
1000 . 00
1.557s
Cs-136
3273.97
818.50
22 .
-5 .
-0.003
129.28
1.559s
MN-54
3339.36
834.85
5 .
2 .
0 . 001
207.02
1.569s
Co - 56
3387 . 05
846.77
5 .
4 .
0 . 002
124.14
1.577s
TL-208
3442 .23
860.56
0 .
9 .
0 . 005
33 .33
1. 585
NB-94
3484 .36
871.10
0 .
7 .
0 . 004
39.46
1. 592s
(Page 8 of 20)
Page 278 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 7
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
EU-154
3492 . 89
873 .23
13 .
-5 .
-0 . 003
51. 93
1. 593s
PA-2 3 4
3522.10
880.53
32 .
-10 .
-0.005
89 .19
1. 598s
PA-2 3 4
3532.94
883 .24
42 .
-9 .
-0.005
102.60
1.599s
AG-110M
3538.71
884 .68
51.
0 .
0 . 000
1000 . 00
1.600s
y-88
3592.14
898.04
9 .
-1.
-0.001
755.14
1.608s
AC-228
3644.26
911.07
5 .
3 .
0 . 002
147.99
1. 616s
AG-110M
3749.96
937.49
10 .
-5 .
-0.003
146.06
1. 633s
PA-2 3 4
3784.07
946.02
5 .
1.
0 . 001
501. 66
1.638s
EU-152
3856.43
964.11
6 .
0 .
0 . 000
734 . 85
1.649s
AC-228
3875.88
968.97
0 .
0 .
0 . 000
1000.00
1. 652s
EU-154
3985.31
996 .33
10 .
6 .
0 . 003
89.27
1. 668s
EU-154
4019.10
1004.77
8 .
2 .
0 . 001
397.46
1.673s
Cs-136
4192.29
1048.07
5 .
2 .
0 . 001
173.21
1.698s
RH-106
4201.45
1050.36
2 .
0 .
0 . 000
1000 . 00
1.700s
BI-207
4254.65
1063.66
3 .
-3 .
-0.002
217.33
1. 708s
Ga-6 8
4309.61
1077.40
10 .
-3 .
-0.002
238 . 82
1. 716
FE-59
4397.02
1099.25
11.
-6 .
-0.003
123 .22
1. 728s
EU-152
4448 . 32
1112.07
0 .
9 .
0 . 005
33 .33
1. 736s
ZN-65
4462 .20
1115.55
9 .
0 .
0 . 000
1000 . 00
1. 738s
Ta-182
4485 . 22
1121.30
9 .
0 .
0 . 000
1000.00
1. 741s
CO-6 0
4692.97
1173.24
4 .
1.
0 . 001
198.61
1.770s
Ta-182
4756.23
1189.05
0 .
0 .
0 . 000
1000 . 00
1.779s
Ta-182
4885.67
1221.41
0 .
0 .
0 . 000
1000.00
1.797s
Co - 56
4953.16
1238.28
0 .
0 .
0 . 000
1000 . 00
1.806s
NA-22
5098.16
1274.53
0 .
0 .
0 . 000
1000.00
1. 826s
EU-154
5098.22
1274.54
0 .
0 .
0 . 000
1000 . 00
1. 826s
FE-59
5166.43
1291.60
0 .
0 .
0 . 000
1000.00
1.835s
CO-6 0
5330.06
1332.50
3 .
-3 .
-0.002
133 .26
1.857s
AG-110M
5537.25
1384 .30
11.
-5 .
-0.003
165 . 68
1. 884
EU-152
5632.07
1408.00
0 .
0 .
0 . 000
1000.00
1. 896s
K-40
5843.40
1460.83
8 .
-2 .
-0.001
363 . 07
1. 923s
SB-124
6764.03
1690.98
0 .
0 .
0 . 000
1000 . 00
2.034s
BI-214
7058.07
1764 .49
0 .
7 .
0 . 004
37 . 80
2.067s
Co - 56
7085.51
1771.35
7 .
0 .
0 . 000
1000 . 00
2.070s
y-88
7344 .36
1836.06
0 .
0 .
0 . 000
1000.00
2 . 098s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE-7 C 5.5694E-01 5.31E+01
477.60 5.569E-01 ?( 8.098E+00 3.99E+02 1.05E+01 G
(Page 9 of 20]
Page 279 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 8
TestAmerica Inc
Nuclide Ave activity
K-40 N -1.2879E+00
Sc-46 F 7.0894E-03
Spectrum name: 8_Gamma_2 016 0992.Anl
Energy Activity Code Peak MDA Comments
4.66E+11
1460.83-1.288E+00 ?(P 1.308E+01 3.63E+02 1.07E+01 G
889.28 7 . 089E-03
1120.55-3.493E-02
8.3 8E+01
(P 2.116E+00 8.39E+03 1.00E+02 G
P 1.223E+00 1.43E+03 1.00E+02 G
CR-51
-2.1636E+00
2.77E+01
320.08-2.164E+00 ?(P 7.776E+00 7.58E+01 9.94E+00 G
MN-54
1. 3025E-01
834.85 1.302E-01 ?(
3.12E+02
7.132E-01 2.07E+02 1.00E+02 G
FE-59
-6 . 8625E-01
4 . 45E+01
1099.25-6.863E-01 ?(P 2.222E+00 1.23E+02 5.65E+01 G
1291.60 0.000E+00 + 1.382E+00 1.00E+03 4.32E+01 G
Co - 56
2 . 3064E-01
7 . 73E+01
846.77 2.306E-01 ?(P 7.373E-01 1.24E+02 9.99E+01 G
1238.28 0.000E+00 - 8.711E-01 1.00E+03 6.61E+01 G
1037.84-7.401E-02 % P 6.313E+00 3.95E+03 1.41E+01 G
1771.35 0.000E+00 - 1.036E+01 1.00E+03 1.55E+01 A
CO - 58
6 . 5697E-01
'10.78 6.570E-01 ?(
7.09E+01
4.035E-01 2.89E+01 9.95E+01 G
CO-6 0
-2 . 4444E-01
1332 . 50-2.444E-01 ?(P
1173.24 1.113E-01 + P
1.93E+03
.901E-01 1.33E+02 1.00E+02 G
.535E-01 1.99E+02 9.99E+01 G
NB-94
6 . 9317E-02
702.63-2.632E-01 ?(
7.41E+06
.362E-01 1.29E+02 9.79E+01 G
'71.10 3.952E-01 ?(P 4.268E-01 3.95E+01 9.99E+01 G
ZR-95
¦9.9699E-01
756.73-9.970E-01 ?(
724.20-6.524E-01 +
6 . 40E+01
2.156E+00 9.20E+01 5.45E+01 G
3.129E+00 1.38E+02 4.42E+01 G
RU-103
-3 . 8620E-01
497.05-3.862E-01 ?(
610.30 0.000E+00 +
3.93E+01
9.749E-01 1.03E+02 9.09E+01 G
2.641E+01 1.00E+03 5.75E+00 GA
AG-108M
1.5307E-01
1.53E+05
433.94 1.53IE-01 ?(P 5.927E-01 1.50E+02 9.05E+01 G
722.94 0.000E+00 - 9.500E-01 1.00E+03 9.08E+01 G
614.28 0.000E+00 - 1.699E+00 1.00E+03 8.98E+01 G
(Page 10 of 20)
Page 280 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:19:58 AMPage 9
Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
AG-110M
1. 9547E-01
2.50E+02
SN-113 F 2 . 0682E-01
SB-124 F 3 .6875E-01
SB-125 I 9.4994E-01
1-131 I 9.8216E-02
Ga-6 8 C -7.4080E+00
Tc-99m I -1.5265E-02
BA-133 F -1.5475E-02
884 .68
0.000E+00
? (
2.902E+00
1.00E+03
7 .
27E+01
G
657.76
3.456E-01
? (
9.427E-01
8.05E+01
9 .
46E+01
G
937.49
-8.957E-01
+
3.125E+00
1.46E+02
3 .
44E+01
G
1384 .30
-1.652E+00
&
6.348E+00
1.66E+02
2 .
43E+01
G
763.94
-5.425E-01
+
4.435E+00
2.23E+02
2 .
23E+01
G
1.15E+02
391.69
2.068E-01
? (
1.052E+00
1.44E+02
6 .
40E+01
G
6.02E+01
602.73
2.919E-01
& (
1.429E+00
1.42E+02
9 .
83E+01
G
1690.98
0.000E+00
-
1.579E+00
1.00E+03
4 .
78E+01
G
722.79
1.068E+00
? (
7.143E+00
1.80E+02
1.
08E+01
G
1.01E+03
427.88
4.899E-01
? (
1.3 07E+00
9.88E+01
2 .
96E+01
G
600 . 50
1.169E+00
? (
5.488E+00
1.34E+02
1.
79E+01
G
635.89
1.310E+00
? (
7.048E+00
1.49E+02
1.
13E+01
G
463 .37
1.487E+00
&( P
5.221E+00
1.01E+02
1.
05E+01
G
8.02E+00
364 .48
-1.384E-01
? (
7.388E-01
2.02E+02
8 .
17E+01
G
284 .30
-3.025E+00
+
9.657E+00
1.25E+02
6 .
14E+00
G
636.97
2.795E+00
? (
1.012E+01
1.03E+02
7 .
17E+00
G
4 . 71E
-02
1077.40
-7 . 408E+00
? (
4.308E+01
2.3 9E+02
3 .
3 0E+00
G
2 . 51E
-01
140 . 51
-1. 527E-02
& (
1.046E+00
1.99E+03
8 .
93E+01
G
3.85E+03
356.00
-2 . 534E-01
? (
1.450E+00
1.65E+02
6 .
20E+01
G
302 . 85
7.898E-01
& (
5.598E+00
2.05E+02
1.
83E+01
G
383.84 1.964E+00 ?
80 . 99-5.123E-01 +
7.693E+00 1.13E+02 8.94E+00 GA
1.435E+00 1.07E+02 3.41E+01 GA
CS-134 I 1.2196E-01
604.71 0.000E+00 ?(
795.87 2.612E-01 ?(
569. 32-5.278E-01 +
801.95 0.000E+00 -
563 . 24-1.886E+00 + P
7.54E+02
1.544E+00 1.00E+03 9.76E+01 G
1.03 8E+00 1.12E+02 8.55E+01 G
5.149E+00 2.65E+02 1.54E+01 G
7.588E+00 1.00E+03 8.69E+00 G
1.081E+01 1.62E+02 8.35E+00 G
(Page 11 of 20)
Page 281 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 10
TestAmerica Inc
Nuclide Ave activity
CS-137 I -1.0672E-01
CE-139
Ba-140
La-140
1.2741E-01
7 . 9471E-01
1.1375E-01
CE-141 I -3 . 5614E-01
CE-144 I -8 . 6920E-01
PM-144 C -1.93 76E-01
Spectrum name: 8_Gamma_20160992.Anl
Energy Activity Code Peak MDA Comments
1.10E+04
661.66-1.067E-01 &(P 1.303E+00 3.25E+02 8.52E+01 G
165.85 1.274E-01 ?(
1.38E+02
5.738E-01 1.30E+02 7.99E+01 G
1.28E+01
537.26 3.519E-01 ?(P 2.621E+00 2.81E+02 2.44E+01 G
1.013E+01 9.96E+01 6.22E+00 G
2.496E+01 2.19E+02 4.29E+00 G
162 . 66-3.011E+00 +
304 . 85 3.312E+00 ?(
1.28E+01
1596.21-2.655E-02 %(P 7.522E-01 2.15E+03 9.54E+01 G
1.967E+00 1.00E+03 4.55E+01 G
3.729E+00 1.39E+02 2.03E+01 G
4.433E+00 1.00E+03 2.33E+01 G
487.02 0.000E+00 +
328.76 7.73 IE-01 ?(
815.77 0.000E+00 -
3.25E+01
145.44-3.561E-01 ?( 9.856E-01 1.06E+02 4.82E+01 G
2.85E+02
133.54-8.692E-01 &( 7.351E+00 2.48E+02 1.11E+01 G
3.63E+02
696.54-1.938E-01 ?( 9.759E-01 2.05E+02 9.90E+01 G
618.06 0.000E+00 + 1.548E+00 1.00E+03 9.91E+01 G
EU-152 F 1.6488E+00
4.94E+03
344 .29
1112.07
121.78
778.92
964.11
244.69-
1408.00
200E-01
696E+00
373E-02
425E-01
158E-01
947E+00
? (
? (
? (
0.000E+00
3
3
1
5
6
1
3
837E+00
846E+00
576E+00
199E+00
297E+00
388E+01
062E+00
79E+02
33E+01
74E+02
54E+02
35E+02
08E+02
00E+03
65E+01 G
36E+01 G
86E+01 G
29E+01 G
46E+01 G
58E+00 G
10E+01 GA
EU-154 I -2.5534E+00
TL-208 N 5.8824E-01
3 . 14E+03
873 .23
-2 . 553E+00
? (P
9 .340E+00
5.19E+01
1.23E+01
G
123.10
2 . 742E-01
+
8 .484E-01
9.09E+01
4.08E+01
G
1274.54
0.000E+00
+
1. 677E+00
1.00E+03
3.52E+01
G
723 .36
-2.208E+00
+
6 . 347E+00
8.49E+01
2.02E+01
G
1004.77
5.916E-01
+
5 . 869E+00
3.97E+02
1.80E+01
G
996 .33
3.546E+00
Sc.
1.089E+01
8.93E+01
1.06E+01
G
6.98E+02
583.02
6.490E-02
? (P
7.739E-01
3.95E+02
8.45E+01
G
277.28-1.980E+00 + P 1.056E+01 1.14E+02 6.31E+00 G
(Page 12 of 20)
Page 282 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 11
TestAmerica Inc
Nuclide Ave activity
Energy
Spectrum name: 8_Gamma_2 016 0992.Anl
Activity Code Peak MDA Comments
860.56 4.149E+00 ?( 3.397E+00 3.33E+01 1.24E+01 G
pm-146
7 .4303E-01
747.16 3.489E-01 ?(
735.72 1. 33 9E+00 ?(
2.02E+03
1.911E+00 2.07E+02 3.40E+01
1.644E+00 4.08E+01 2.25E+01
453.88-2.507E-01 + P 1.040E+00 1.35E+02 6.50E+01
y-
¦8 . 4788E-02
1.07E+02
898 . 04-8.479E-02 ?(P 1.074E+00 7.55E+02 9.37E+01 G
1836.06 0.000E+00 + 8.180E-01 1.00E+03 9.92E+01 G
Cd-113m
7 .2951E+02
263.70 7.295E+02
5.33E+03
1.030E+04 3.94E+02 6.00E-03
K
Cd-109
-3.0620E+00
. 04-3.062E+00 ?(
4.53E+02
2.711E+01 2.61E+02 3.79E+00
G
Cf-251
-3 . 7782E-01
176 . 60-3.778E-01 ?(
227.00-1.236E+00 +
3.28E+05
2.320E+00 2.25E+02 1.70E+01 G
8.460E+00 2.64E+02 6.30E+00 GA
Cf-249
2 . 8438E-01
387.95 1.101E-01 ?(
333.44 1. 026E+00 &(
1. 28E+05
1.183E+00 2.99E+02 6.60E+01 G
5.339E+00 1.50E+02 1.55E+01 G
Sn-126
¦1. 9480E+00
87 . 57-4.869E-01 +
64.28-1.948E+00 ?(
86 . 94-2.026E+00 +
3.65E+07
2.7 83E+00 1.69E+02 3.75E+01 GA
9.246E+00 1.40E+02 9.70E+00 G
1.188E+01 1.74E+02 9.04E+00 GA
PB-210
N
¦7.5278E+00
8.14E+03
46 . 54-7.528E+00 ?(P 2.540E+01 7.44E+01 4.25E+00
G
PB-212
N
¦1.0240E+00
6.98E+02
238 . 63-1.024E+00 ?(P 2.241E+00 2.81E+01 4.33E+01 G
300.03 4.374E+00 + 2.574E+01 1.70E+02 3.28E+00 GA
PB-214
N
4 . 4901E-01
5 . 84E+05
351.93 3.040E-01 ?(P 1.996E+00 1.87E+02 3.76E+01 G
4.150E+00 1.64E+02 1.93E+01 G
1.344E+01 1.13E+02 7.43E+00 GA
295.09 7.315E-01 &(
242 . 00-3.518E+00 &
BI-207
¦1.1218E-01
1.18E+04
569 . 70-1.122E-01 ?(P 9.498E-01 2.49E+02 9.77E+01 G
1063.66-2.833E-01 + P 1.002E+00 2.17E+02 7.45E+01 G
(Page 13 of 20)
Page 283 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:19:58 AMPage 12
Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
BI-212 N
-5.7036E-01
6.98E+02
727.17-5.704E-01
&( P
2.016E+01
7.51E+02 7.55E+00
G
785 . 42-1.381E+00
o.
"o
7.019E+01
1.95E+03 1.28E+00
GA
BI-214 N
9.6949E-01
5.84E+05
609.31-3.213E-01
? (P
3.3 95E+00
1.74E+02 4.61E+01
G
1120.29-2.312E-01
% p
8.096E+00
1.41E+03 1.51E+01
G
1764.49 4.833E+00
? (
5.088E+00
3.78E+01 1.54E+01
G
BI-210M T
-2.2024E-01
1.10E+09
265.83-2.202E-01
& (
1.316E+00
1.71E+02 5.00E+01
G
304.90-3.342E-07
o.
"o
3.957E+00
3.38E+08 2.80E+01
G
AC-228 N
8.8204E-01
2.10E+03
911.07 6.906E-01
? (
2.647E+00
1.48E+02 2.90E+01
G
968.97 0.000E+00
-
2.672E+00
1.00E+03 1.75E+01
G
338.32 1.344E+00
? (
7.463E+00
1.60E+02 1.20E+01
G
93.35 0.000E+00
-
1.838E+01
1.00E+03 5.56E+00
XA
TH-227 N
3.0574E+00
7.95E+03
50.14 3.057E+00
& (
1.184E+01
1.14E+02 8.00E+00
G
256.24-6.114E-01
-
7.199E+00
4.43E+02 7.00E+00
G
TH-229 N
3.0004E+00
2.68E+06
193.51 3 . 000E+00
? (
8.869E+00
1.11E+02 4.40E+00
G
210.85-4.306E+00
Sc.
1.980E+01
1.81E+02 2.99E+00
G
TH-234 N
4.0068E+00
1.63E+12
63.29 4.007E+00
(P
1.576E+01
1.33E+02 3.81E+00
G
92 . 59-1.515E+01
+ P
1.972E+01
2.30E+01 5.58E+00
G
PA-231 N
5 .3963E+00
1.20E+07
302.65 5.024E+00
& (
3.419E+01
1.97E+02 2.88E+00
G
300.07 5.833E+00
? (
3.623E+01
1.79E+02 2.46E+00
G
PA-233 C
3 .1469E-01
7.82E+08
312.01-2.986E-02
% (P
3.142E+00
1.48E+03 3.60E+01
G
300.18 2 . 315E+00
? (
1.510E+01
1.89E+02 6.20E+00
G
PA-2 3 4 N
-2.923 IE-01
1.63E+12
131.29-8.545E-01
? (
4.158E+00
1.43E+02 1.80E+01
G
946.02 4.629E-01
? (
6.078E+00
5.02E+02 1.34E+01
G
569.47-2.475E-01
o,
"o
1.042E+01
1.12E+03 8.20E+00
G
883 . 24-5 . 718E+00
+
1.998E+01
1.03E+02 9.60E+00
G
880.53-9.359E+00
+
2.828E+01
8.92E+01 6.00E+00
GA
(Page 14 of 20)
Page 284 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:19:58 AMPage 13
Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PA-234M N
-3 .4240E+00
1001.00-3.424E+00
766.41-1.198E+02 + P
1. 63E+12
(P 1.767E+02 1.39E+03 8.37E-01 G
4.2 92E+02 9.64E+01 2.94E-01 G
U-235
N
-2.1186E-02
143 . 79-2.119E-02
205.33-9.518E-01 + P
163 .38-2.387E+00 + P
2.57E+11
(P 4.806E+00 6.40E+03 1.10E+01 G
9.947E+00 3.68E+02 5.01E+00 G
1.372E+01 1.39E+02 5.08E+00 G
AM-241 T -1.6463E-01
1.58E+05
59.54-1.646E-01 ?(P 2.471E+00 4.26E+02 3.59E+01 G
Np-237 F -1.4008E+00
2.14E+06
86.49-1.401E+00 ?( 8.622E+00 1.83E+02 1.31E+01 G
Ir-192 F 5.4126E-02
7 . 40E+01
316.49-9.676E-02 ?( 1.221E+00 3.62E+02 8.70E+01 G
468.06 3.079E-01 *( 1.264E+00 1.16E+02 5.18E+01 G
308.44 0.000E+00 - 3.522E+00 1.00E+03 3.18E+01 G
Cs-136
¦9 .1859E-02
818 . 50-2.975E-01 ?(
1048.07 1.692E-01 +
340.57 3.465E-01 ?(
1.30E+01
1.344E+00 1.29E+02 1.00E+02 G
1.111E+00 1.73E+02 8.00E+01 G
2.039E+00 1.70E+02 4.69E+01 G
Np-239
¦8 . 6048E-01
103.70 0.000E+00 +
106 .13-8.605E-01 ?(
99.50 0.000E+00 +
2.36E+00
4.161E+00 1.00E+03 2.40E+01 X
4.147E+00 1.43E+02 2.27E+01 G
6.7 02E+00 1.00E+03 1.50E+01 X
Nd-147
3 . 8331E+00
531. 00 3 . 833E+00 ?(
91.10-4.625E-08 %
1.11E+01
2.173E+00 2.77E+01 1.30E+01 G
3.642E+00 2.30E+09 2.83E+01 G
( - This peak used in the nuclide activity average.
Peak is too wide, but only one peak in library.
Peak is part of a multiplet and this area went
negative during deconvolution.
Peak is too narrow.
Peak is too wide at FW25M, but ok at FWHM.
Peak fails sensitivity test.
Peak identified, but first peak of this nuclide
failed one or more qualification tests.
Peak activity higher than counting uncertainty range.
Peak activity lower than counting uncertainty range.
Peak outside analysis energy range.
(Page 15 of 20)
Page 285 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 14
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** £)
I S C A R D
ED ISO
TOPE P
E A K S
***********
Nuclide
Centroid
Background
Net Area
Intensity
Uncert
Activity
Energy
Counts
Counts
Cts/Sec
1 Sigma %
PB-210
46 . 54
61.
-12 .
-0.006
74 .39
-7.528E+00
TH -7.7.1
50 .14
60 .
10 .
0 . 006
113 . 81
3.057E+00
AM-2 41
59 . 54
86 .
-3 .
-0 . 002
426 .34
-1.646E-01
Sn-126
64 .28
106 .
-11.
-0.006
139.74
-1.948E+00
BA-133
80 . 99
44 .
-12 .
-0.007
107.37
-5.123E-01
Np-237
86 .49
279 .
-13 .
-0.007
182.62
-1.401E+00
EU-155
86 . 54
266 .
-13 .
-0.007
178.38
-5.976E-01
Sn-126
86 . 94
253 .
-13 .
-0.007
173.98
-2.026E+00
Sn-126
87 . 57
239 .
-13 .
-0.007
169.47
-4.869E-01
Cd-109
88 . 04
233 .
-8 .
-0.005
261.18
-3.062E+00
Np-239
106.13
214 .
-15 .
-0.008
143.06
-8.605E-01
EU-152
121.78
44 .
2 .
0 . 001
474 . 34
9.373E-02
EU-154
123.10
24 .
8 .
0 . 005
90 . 89
2.742E-01
PA-2 3 4
131.29
124 .
-11.
-0.006
143 .49
-8.545E-01
HF-181
133.02
136 .
-11.
-0.006
149.38
-3 . 574E-01
CE-144
133.54
147 .
-7 .
-0.004
247 . 81
-8 . 692E-01
CO - 57
136.47
163 .
-12 .
-0.007
154 . 46
-1.547E+00
CE-141
145.44
43 .
-12 .
-0.007
106.03
-3 . 561E-01
Ba-140
162.66
67 .
-12 .
-0.007
99 . 56
-3 . 011E+00
U-235
163 .38
82 .
-8 .
-0 . 004
139.10
-2 .387E+00
CE-13 9
165.85
34 .
7 .
0 . 004
130.22
1. 274E-01
Cf-251
176.60
22 .
-4 .
-0 . 002
225.00
-3 . 778E-01
TH-229
193.51
18 .
8 .
0 . 004
110.55
3.000E+00
U-235
205.33
29 .
-3 .
-0.001
367 . 79
-9.518E-01
TH-229
210 . 85
40 .
-7 .
-0 . 004
180 . 89
-4.3 06E+00
Cf-251
227.00
28 .
-4 .
-0.002
263.79
-1.236E+00
PB-214
242.00
98 .
-13 .
-0.007
112 . 99
-3 . 518E+00
EU-152
244 .69
107 .
-7 .
-0.004
208.15
-1.947E+00
TH-771
256.24
20 .
-2 .
-0.001
443 .47
-6 . 114E-01
Cd-113m
263.70
30 .
2 .
0 . 001
393.70
7 . 295E+02
(Page 16 of 20)
Page 286 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 15
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide
Channel
Energy Background Net
area 1
Cnts/sec
Uncert FWHM
BI-210M
265 . 83
34
-5 .
-0 . 003
170 . 88
-2 .202E-01
TL-208
277 .28
32
-5 .
-0.003
114.12
-1.980E+00 P
1-131
284 .30
24
-8 .
-0 . 004
125.00
-3.025E+00
PB-214
295.09
44
6 .
0 . 003
163.52
7.315E-01
PA-2 31
300.07
53
6 .
0 . 003
179.40
5.833E+00
PA-233
300.18
59
6 .
0 . 003
188.55
2.315E+00
PA-2 31
302.65
65
6 .
0 . 003
197.03
5.024E+00
BA-133
302.85
71
6 .
0 . 003
205.38
7.898E-01
Ba-140
304.85
77
6 .
0 . 003
218.51
3.312E+00
Ir-192
316.49
71
-3 .
-0 . 002
362 .49
-9.676E-02
CR-51
320.08
35
-8 .
-0.005
75 . 77
-2.164E+00 P
La-140
328.76
32
6 .
0 . 003
138 . 85
7.73 IE-01
Cf-249
333.44
38
6 .
0 . 003
149.92
1.026E+00
AC-228
338 .32
44
6 .
0 . 003
160 .14
1.344E+00
Cs-136
340.57
50
6 .
0 . 003
169 . 92
3.465E-01
EU-152
344 .29
56
6 .
0 . 003
178.97
6.200E-01
HF-181
345.83
138
-11.
-0.006
148 . 66
-2.049E+00
PB-214
351.93
28
4 .
0 . 002
186.91
3.040E-01 P
BA-133
356.00
41
-6 .
-0 . 003
164.60
-2 . 534E-01
1-131
364 .48
16
-4 .
-0.002
202.07
-1.384E-01
BA-133
383 . 84
20
6 .
0 . 003
113.06
1. 964E+00 P
Cf-249
387 . 95
26
2 .
0 . 001
299.38
1.101E-01
SN-113
391.69
18
4 .
0 . 002
143 . 85
2.068E-01
SB-125
427 . 88
4
5 .
0 . 003
98 . 79
4.899E-01
AG-108M
433.94
9
4 .
0 . 002
149 . 80
1.53 IE-01 P
pm-146
453 . 88
14
-5 .
-0 . 003
135.31
-2.507E-01 P
SB-125
463 .37
8
5 .
0 . 003
100.56
1.487E+00 P
Ir-192
468.06
12
5 .
0 . 003
116 .47
3.079E-01
BE - 7
477 .60
21
2 .
0 . 001
399 . 50
5.569E-01
RU-103
497.05
22
-10 .
-0.005
103 .42
-3.862E-01
RH-106
511. 86
14
24 .
0 . 013
45 . 58
4.464E+00
Ba-140
537.26
9
2 .
0 . 001
280.50
3.519E-01 P
CS-134
563.24
18
-4 .
-0 . 002
161.84
-1.886E+00 P
CS-134
569.32
13
-2 .
-0.001
264.58
-5.278E-01
BI-207
569.70
19
-3 .
-0.002
249.21
-1.122E-01 P
TL-208
583.02
8
1.
0 . 001
394 . 86
6.490E-02 P
SB-125
600 . 50
19
5 .
0 . 003
133.56
1.169E+00
SB-124
602.73
42
7 .
0 . 004
141. 69
2.919E-01
BI-214
609.31
52
-3 .
-0 . 002
173 .68
-3.213E-01 P
SB-125
635 . 89
11
3 .
0 . 002
149 . 00
1.310E+00
1-131
636 . 97
8
4 .
0 . 002
103.04
2.795E+00
AG-110M
657.76
13
7 .
0 . 004
80 . 50
3.456E-01
CS-137
661. 66
21
-2 .
-0.001
324 . 88
-1.067E-01 P
PM-144
696 . 54
14
-4 .
-0 . 002
204 . 63
-1.938E-01
NB-94
702 . 63
9
-5 .
-0.003
129 . 00
-2.632E-01
SB-124
722.79
8
2 .
0 . 001
180.14
1.068E+00
EU-154
723 .36
25
-9 .
-0.005
84 . 94
-2.208E+00
ZR-95
724.20
29
-6 .
-0 . 003
137.80
-6.524E-01
(Page 17 of 20)
Page 287 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:19:58 AMPage 16
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
Nuclide
Channel
Energy Background Net
area 1
Cnts/sec
Uncert FWHM
BI-212
727.17
36
-1.
0 . 000
750.66
-5 . 704E-01 P
pm-146
735.72
0
6 .
0 . 003
40 . 82
1.33 9E+00
pm-146
747 .16
5
2 .
0 . 001
207.02
3.489E-01
ZR-95
756.73
19
-11.
-0.006
92 . 04
-9.970E-01
AG-110M
763.94
12
-2 .
-0.001
222.69
-5.425E-01
PA-234M
766.41
21
-7 .
-0.004
96 .38
-1.198E+02 P
EU-152
778.92
5
1.
0 . 001
354.44
5.425E-01
CS-134
795.87
9
4 .
0 . 002
112.14
2.612E-01
Cs-136
818.50
22
-5 .
-0 . 003
129.28
-2.975E-01
MN-54
834.85
5
2 .
0 . 001
207.02
1.302E-01
Co - 56
846.77
5
4 .
0 . 002
124.14
2.306E-01 P
TL-208
860.56
0
9 .
0 . 005
33 .33
4.149E+00
NB-94
871.10
0
7 .
0 . 004
39.46
3.952E-01 P
EU-154
873 .23
13
-5 .
-0 . 003
51. 93
-2 . 553E+00 P
PA-2 3 4
880.53
32
-10 .
-0.005
89 .19
- 9.3 59E+00
PA-2 3 4
883 .24
42
-9 .
-0.005
102.60
-5.718E+00
y-88
898.04
9
-1.
-0.001
755 . 14
-8.479E-02 P
AC-228
911.07
5
3 .
0 . 002
147 . 99
6.906E-01
AG-110M
937.49
10
-5 .
-0 . 003
146.06
-8.957E-01
PA-2 3 4
946.02
5
1.
0 . 001
501. 66
4.629E-01
EU-152
964.11
6
0 .
0 . 000
734 . 85
2.158E-01
EU-154
996.33
10
6 .
0 . 003
89.27
3.546E+00
EU-154
1004.77
8
2 .
0 . 001
397.46
5.916E-01
Cs-136
1048.07
5
2 .
0 . 001
173.21
1.692E-01
BI-207
1063.66
3
-3 .
-0 . 002
217.33
-2.833E-01 P
Ga-6 8
1077.40
10
-3 .
-0.002
238 . 82
-7.408E+00
FE-59
1099.25
11
-6 .
-0.003
123 .22
-6.863E-01 P
EU-152
1112.07
0
9 .
0 . 005
33 .33
4.696E+00
CO-6 0
1173.24
4
1.
0 . 001
198.61
1.113E-01 P
CO-6 0
1332.50
3
-3 .
-0 . 002
133 .26
-2 . 444E-01 P
AG-110M
1384.30
11
-5 .
-0.003
165 . 68
-1. 652E+00
K-40
1460.83
8
-2 .
-0.001
363.07
-1.288E+00 P
BI-214
1764.49
0
7 .
0 . 004
37 . 80
4.833E+00
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#A
5 . 5694E-01
5.5694E-01
3.995E+02 %
8.10E+00
NA-22
#A
0.0000E+00
0.0000E+00
1.000E+03 %
5.90E-01
K-40
#A
-1.2879E+00
-1.2879E+00
3.631E+02 %
1.31E+01
Sc-46
#A
7 . 0894E-03
7.0894E-03
8.385E+03%
2.12E+00
CR-51
#A
-2 .1636E+00
-2.1636E+00
7.577E+01%
7.78E+00
MN-54
#A
1. 3025E-01
1.3025E-01
2.070E+02%
7.13E-01
FE-59
#A
-6 . 8624E-01
-6.8625E-01
1.232E+02 %
2.22E+00
(Page 18 of 20)
Page 288 of 551
-------
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TestAmerica Inc Spectrum name: 8_Gamma_2 016 0992.Anl
Co - 56
#A
2 . 3064E-01
2 . 3064E-01
1.241E+02 %
7.37E-01
CO - 57
#A
0.0000E+00
0.0000E+00
1.000E+03 %
5.37E-01
CO - 58
#
6.5697E-01
6.5697E-01
2.887E+01%
4.03E-01
CO-6 0
#A
-2 . 4444E-01
-2.4444E-01
1.333E+02 %
8.90E-01
ZN-65
#A
0.0000E+00
0.0000E+00
1.000E+03 %
2.3 5E+00
NB-94
#A
6.9317E-02
6.9317E-02
3.946E+01%
8.36E-01
ZR-95
#A
-9.9698E-01
-9.9699E-01
9.204E+01%
2.16E+00
NB-95
#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.07E+00
RU-103
#A
-3.8620E-01
-3.8620E-01
1.034E+02 %
9.75E-01
RH-106
#A
0.0000E+00
0.0000E+00
7.071E+02 %
1.55E+01
AG-108M#A
1.5307E-01
1.5307E-01
1.498E+02%
5.93E-01
AG-110M#A
1. 9547E-01
1.9547E-01
8.050E+01%
2.90E+00
SN-113
#A
2 . 0682E-01
2.0682E-01
1.43 8E+02 %
1.05E+00
SB-124
#A
3.6875E-01
3.6875E-01
1.146E+02 %
1.43E+00
SB-125
#A
9.4994E-01
9.4994E-01
6.119E+01%
1.31E+00
1-131
#A
9 . 8211E-02
9.8216E-02
1.03 0E+02 %
7.39E-01
Gd-153
#A
0.0000E+00
0.0000E+00
7.071E+02 %
3.3 7E+00
Ga-6 8
#A
-7 . 3464E+00
-7.4080E+00
2.3 8 8E+02 %
4.31E+01
Tc-99m
#A
-1.5241E-02
-1.5265E-02
1.995E+03 %
1.05E+00
BA-133
#A
-1.5475E-02
-1.5475E-02
1.316E+02 %
1.45E+00
CS-134
#A
1.2196E-01
1.2196E-01
1.121E+02 %
1.54E+00
CS-137
#A
-1.0672E-01
-1.0672E-01
3.24 9E+02 %
1.30E+00
CE-139
#A
1. 2741E-01
1.2741E-01
1.3 02E+02 %
5.74E-01
Ba-140
#A
7 . 9468E-01
7.9471E-01
1.778E+02%
2.62E+00
La-140
#A
1. 1375E-01
1.1375E-01
1.389E+02%
7.52E-01
CE-141
#A
-3 . 5613E-01
-3.5614E-01
1.060E+02%
9.86E-01
CE-144
#A
-8 . 6920E-01
-8.6920E-01
2.478E+02%
7.35E+00
PM-144
#A
-1.9376E-01
-1.9376E-01
2.046E+02 %
9.76E-01
EU-152
#A
1. 6488E+00
1.6488E+00
3.333E+01%
3.84E+00
EU-154
#A
-2 . 5534E+00
-2.5534E+00
5 .193E+01%
9.34E+00
EU-155
#A
0.0000E+00
0.0000E+00
1. 000E+03 %
4.70E+00
HF-181
#A
0.0000E+00
0.0000E+00
7.071E+02 %
1.10E+00
Ta-182
#A
0.0000E+00
0.0000E+00
5.774E+02 %
3.43E+00
Hg-203
#A
0.0000E+00
0.0000E+00
1.000E+03 %
8.73E-01
TL-208
#A
5 . 8824E-01
5.8824E-01
3 .333E+01%
7.74E-01
pm-146
#A
7 .4303E-01
7.4303E-01
4.082E+01%
1.91E+00
y-88
#A
-8 . 4788E-02
-8.4788E-02
7.551E+02 %
1.07E+00
Cd-113m#A
7 . 2951E+02
7.2951E+02
3.93 7E+02 %
1.03E+04
Cd-109
#A
-3 . 0620E+00
-3.0620E+00
2.612E+02%
2.71E+01
Cf-251
#A
-3 . 7782E-01
-3.7782E-01
2.250E+02%
2.32E+00
Cf-249
#A
2 . 8438E-01
2.8438E-01
1.499E+02%
1.18E+00
Sn-126
#A
-1.9480E+00
-1.9480E+00
1.3 97E+02 %
9.25E+00
PB-210
#A
-7.5278E+00
-7.5278E+00
7.439E+01%
2.54E+01
PB-212
#A
-1.0240E+00
-1.0240E+00
2.811E+01%
2.24E+00
PB-214
#A
4 . 4901E-01
4.4901E-01
1.242E+02 %
2.00E+00
BI-207
#A
-1.1218E-01
-1.1218E-01
2.492E+02%
9.50E-01
BI-212
#A
-5.7036E-01
-5.7036E-01
7.507E+02 %
2.02E+01
BI-214
#A
9 . 6949E-01
9.6949E-01
3.780E+01%
3.40E+00
BI-210M#A
-2 . 2024E-01
-2.2024E-01
1.709E+02%
1.32E+00
(Page 19 of 20)
Page 289 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 8:
19:58 AMPage 18
TestAmerica
Inc
Spectrum
name: 8 Gamma
20160992.Anl
AC-228
#A
8 . 8204E-01
8 . 8204E-01
1.090E+02 %
2.65E+00
TH -7.7.1
#A
3 . 0574E+00
3.0574E+00
1.13 8E+02 %
1.18E+01
TH-229
#A
3 . 0004E+00
3.0004E+00
1.105E+02 %
8.87E+00
TH-234
A
4.0068E+00
4.0068E+00
1. 326E+02%
1.58E+01
PA-2 31
#A
5.3 963E+00
5.3 963E+00
1.332E+02 %
3.42E+01
PA-233
#A
3 .1469E-01
3.1469E-01
1.8 8 5E+02 %
3.14E+00
PA-2 3 4
#A
-2.923 IE-01
-2.923 IE-01
1.43 5E+02 %
4.16E+00
PA-234M#A
-3.4240E+00
-3.4240E+00
1.387E+03%
1.77E+02
U-235
#A
-2.1186E-02
-2.1186E-02
6.400E+03 %
4.81E+00
AM-2 41
#A
-1.6463E-01
-1.6463E-01
4.263E+02 %
2.47E+00
Np-237
#A
-1.4008E+00
-1.4008E+00
1.826E+02 %
8.62E+00
Ir-192
#A
5 . 4126E-02
5.4126E-02
1.16 5E+02 %
1.22E+00
Cs-136
#A
-9 . 1856E-02
-9.1859E-02
1.068E+02%
1.34E+00
Np-239
#A
-8 . 6034E-01
-8.6048E-01
1.431E+02 %
4.15E+00
Nd-147
#
3 . 8330E+00
3.8331E+00
2.774E+01%
2.17E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.5 to 2000.0 keV) 0.000E+00 Bq/Sample
Total Decayed Activity ( 37.5 to 2000.0 keV) 0.0000000E+00 Bq/Sample
(Page 2 0 of 20)
Page 290 of 551
-------
257060_Gamma_MB 160-257060~1-A. 8_Gamma_20160992.spc.
1.0e4n
1.0e3-
Tl
£B
CQ
fte2
cn
cn
CO CO
CN CN
I CO C C CO I o
iOT c CO't
~ "r-
hco <^r
cc>
. C CN CN w .
Qj :r' ro l .t—
<
o
Td"
^r
¦*7
CN
(0
_l
CD
500 1000 1500 2000 2500 3000 3500 4000
Channels
4500
5000
5500
6000
6500
7000
7500
8000
-------
Test America St. Louis Spectrum ID: 7_Gamma_20161686
Sample Description: 2 5706 0_Gamma_LCS 160-257060-2-A
Detector: Detector # 7
Batch ID: 257060
Work Order Number: Gamma
Lot Number: LCS 160-257060~2-A
Decay to Time: 7/11/2016 07:47 Live Time: 1800 sec
Acquisition Time: 7/11/2016 07:47:36 Real Time: 1838 sec
Analysis Time: 7/11/2016 08:18 Dead Time: 2.07 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
7_Soil_TunaCan.Clb
7_TunaCan_90099_032 712
3/16/2012 11:45
2/23/2012 08:40
Client_Long_Revll.lib
7 2016-07-10 0612.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
-1.345E+01
103 . 0
1.385E+01
1.387E+01
4.594E+01
NA-22
8 . 951E-02
673 . 6
6 . 030E-01
6.03 0E-01
2.152E+00
K-40
8.870E+00
33 . 9
3.009E+00
3.043E+00
7.23 0E+00
Sc-46
5.393E-01
318 .4
1.717E+00
1.718E+00
5.765E+00
CR-51
-2 . 573E+00
599 . 0
1.541E+01
1.541E+01
5.128E+01
MN-54
1.715E+00
83 . 7
1.436E+00
1.438E+00
3.217E+00
FE-59
6.920E-01
535.4
3.706E+00
3.706E+00
7.858E+00
Co - 56
4.986E-01
177 . 1
8.832E-01
8.836E-01
3.774E+00
CO - 57
0.000E+00
1.#INF
3.960E-01
3.960E-01
2.164E+00
CO - 58
1. 698E+00
83 . 9
1.425E+00
1.427E+00
4.727E+00
CO-6 0
2 . 023E+02
1.3
2.674E+00
1.050E+01
1.051E+00
ZN-65
0.000E+00
1.#INF
1.448E+00
1.448E+00
1.187E+01
NB-94
-1.203E-01
1026 .3
1.23 5E+00
1.23 5E+00
2.817E+00
ZR-95
2 . 441E+00
87.3
2.132E+00
2.136E+00
4.795E+00
NB-95
8.424E-01
122 . 8
1.035E+00
1.036E+00
3.467E+00
RU-103
1. 327E+00
95.3
1.264E+00
1.266E+00
2.935E+00
RH-106
2.976E+01
50 . 7
1.509E+01
1.517E+01
3.186E+01
AG-108M
1.055E-01
1276.7
1.346E+00
1.346E+00
3.279E+00
AG-110M
1. 666E+00
32 . 9
5.473E-01
5.539E-01
7.419E+00
SN-113
2 . 393E-01
793 . 8
1.900E+00
1.900E+00
6.3 52E+00
SB-124
-7.880E-01
139 . 7
1.101E+00
1.102E+00
5.735E+00
SB-125
4 . 121E+00
95 . 5
3.936E+00
3.942E+00
9.494E+00
1-131
1. 524E+00
105 . 6
1.610E+00
1.612E+00
2.962E+00
Gd-153
-1.998E+00
143 . 6
2.870E+00
2.872E+00
9.508E+00
Ga-6 8
3.000E+01
227 . 9
6.835E+01
6.837E+01
1.448E+02
Tc-99m
-6 . 605E-01
121. 5
8.026E-01
8.035E-01
2.661E+00
BA-133
1. 584E+00
95 . 1
1.506E+00
1.508E+00
4.997E+00
CS-134
1.979E+00
83 . 6
1.653E+00
1.656E+00
5.736E+00
CS-137
3 . 623E+02
1.2
4.313E+00
1.933E+01
3.208E+00
CE-139
7 . 294E-01
101. 9
7.436E-01
7.469E-01
2.466E+00
Ba-140
-5.921E+00
101. 7
6.020E+00
6.028E+00
1.261E+01
La-140
1.058E+00
33 .3
3.528E-01
3.572E-01
6.371E-01
CE-141
1.152E+00
157 . 5
1.815E+00
1.816E+00
6.016E+00
(Page 1 of 21)
Page 292 of 551
-------
CE-144
3 . 020E+00
189 . 5
5.723E+00
5.725E+00
1.903E+01
PM-144
-3 . 956E-01
134 .3
5.312E-01
5.316E-01
3.073E+00
EU-152
3 . 963E+00
74 . 2
2.940E+00
2.947E+00
1.23 0E+01
EU-154
5.43 8E+00
182 .4
9.919E+00
9.923E+00
3.33 8E+01
EU-155
9.627E-01
174 . 6
1.681E+00
1.681E+00
1.3 56E+01
HF-181
4.705E-01
114 . 0
5.362E-01
5.368E-01
6.163E+00
Ta-182
-7.201E+00
79 . 1
5.693E+00
5.705E+00
1.886E+01
Hg-203
7.744E-02
1123 . 5
8.700E-01
8.700E-01
2.922E+00
TL-208
5.187E+00
23 . 9
1.241E+00
1.270E+00
2.517E+00
pm-146
1.310E+00
139 . 5
1.828E+00
1.829E+00
8.566E+00
y-88
2.069E+00
\o
00
1.788E+00
1.792E+00
3.868E+00
Cd-113m
-1. 427E+04
107 . 1
1.529E+04
1.532E+04
5.070E+04
Cd-109
1.717E+01
130 . 7
2.244E+01
2.246E+01
7.433E+01
Cf-251
-3.709E+00
90.4
3.3 53E+00
3.369E+00
1.111E+01
Cf-249
1.801E+00
96 . 9
1. 746E+00
1.748E+00
5.564E+00
Sn-126
-1. 860E+00
478 .2
8.894E+00
8.894E+00
2.964E+01
PB-210
1. 033E+04
1. 0
1.049E+02
6.156E+02
1.831E+02
PB-212
6 . 940E+00
26 . 6
1.846E+00
1.900E+00
4.250E+00
PB-214
2.346E+00
94 . 7
2.221E+00
2.225E+00
7.444E+00
BI-207
1.303E-02
00
00
1.154E-02
1.156E-02
3.052E+00
BI-212
-1.510E+01
104 . 6
1.579E+01
1.581E+01
5.264E+01
BI-214
6.942E+00
23 . 6
1.639E+00
1.678E+00
3.965E+00
BI-210M
-1. 736E+00
43 .3
7.523E-01
7.593E-01
5.969E+00
AC-228
8.558E-01
00
o
3.493E-01
3.520E-01
1.482E+01
TH -7.7.1
-3.273E+01
190 . 9
6.248E+01
6.251E+01
2.063E+02
TH-229
3 . 647E+00
96 .1
3.505E+00
3.517E+00
4.319E+01
TH-234
-3 . 097E+01
234 .4
7.260E+01
7.262E+01
7.253E+01
PA-2 31
-3 .327E+01
157 .1
5.225E+01
5.228E+01
1.733E+02
PA-233
2 . 683E+00
155.3
4.167E+00
4.170E+00
1.3 82E+01
PA-2 3 4
7.870E+00
00
00
\o
5.414E+00
5.429E+00
1.132E+01
PA-234M
-6.157E+01
358 .1
2.205E+02
2.205E+02
8.3 50E+02
U-235
5.056E+00
160 . 5
8.116E+00
8.120E+00
2.691E+01
AM-2 41
1.210E+03
0 . 7
8.995E+00
6.345E+01
1.294E+01
Np-237
0.000E+00
1.#INF
7.012E+00
7.012E+00
2.33 0E+01
Ir-192
1. 061E+00
147 . 1
1.560E+00
1.561E+00
5.747E+00
Cs-136
1. 617E+00
CM
\o
00
1.394E+00
1.3 97E+00
4.629E+00
Np-239
2 . 531E+00
139 . 9
3.541E+00
3.544E+00
1.173E+01
Nd-147
1.557E+00
131.4
2.045E+00
2.047E+00
2.124E+01
Total 1.22 8E+04
Analyst: Amanda Dick
(Page 2 of 21)
Page 293 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 1
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Sample description
257060 Gamma LCS 160-257060-2-A
Spectrum Filename: C:\User\SPC\Det7\7_Gamma_20161686.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 7:47:36 AM
1800
1838
2 . 07 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
7 TunaCan 90099 032712
7 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/23/2012 8:40:56 AM
0.117 keV
0.250 keV/channel
3.508E-09 keV/channel^2
3/16/2012 11:45:14 AM
165.85 keV
Quadratic
6 . 716580E-01
( -2 . 065917E
Quadratic
-2 . 689695E+01
Uncertainty = 0.8 7
+ (-6 .166540E-01*Log(E) )
02*Log(E)^2 )
Uncertainty = 1.4 8
+ ( 1. 019544E+01*Log(E) )
( -1.081671E+00*Log(E) 2
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 3 7.61keV )
8000 ( 2000.13keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00*
1.0000E+00
Reg. Guide 4.16 Method
1.0000E+00)
(Page 3 of 21)
Page 294 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:18:38 AMPage 2
Spectrum name: 7_Gamma_2 01616 86.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 7:47:00 AM
7_2 016-07-10_0612.PBC
7/10/2016 6:12:03 AM
total peaks alloc. 25 cutoff: 5.00E+01 !
Energy Calibration
Normalized diff: 0.1233
* * * * * g
U M
M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq/Sampl
46 . 57
19620.
1. 02
0 . 94
2.486E-02
46 . 54
4 .250
1
. 033E+04
PB210
59 . 56
2i
3945 .
0 . 74
0 . 95
3.703E-02
59 . 54
35.900
1
.210E+03
AM241
77 . 04
217 .
21.29
1.21
4 . 884E-02
86 . 55
0 .
. 539.99
0 . 88
5 . 279E-02
86 .49
13 .100
PBC
-------
ORTEC g v - i (3263) Env32 G800W064
TestAmerica
Inc
Spectrum nar
pk energy
area
uncert
f whm
corr
227.00
6 .
798.92
1. 03
3.757E-02
238 . 60
195 .
26 .60
0 . 92
3.602E-02
242 . 00
7 .
782.07
1. 04
3 . 560E-02
256 .24
9 .
533.46
1. 06
3.3 92E-02
269.97
77 .
35 . 06
0 . 56
3.245E-02
277.80
52 .
50.24
0.48
3.167E-02
295.09
24 .
195.83
1.10
3.009E-02
306.93
69 .
33 .44
1.11
2.910E-02
310.53
70 .
38.25
1.12
2.882E-02
312.01
50 .
155.31
1.12
2.869E-02
316.32
28 .
270.59
1.12
2 . 834E-02
317.33
50 .
50 . 70
1.12
2 . 826E-02
318.58
8 .
318.20
1.12
2 . 816E-02
333 .44
47 .
96 . 92
1. 14
2.711E-02
338.74
62 .
40 . 81
1.45
2.677E-02
345 . 83
15 .
331.17
1. 15
2.627E-02
351.93
42 .
94 .67
1. 16
2.588E-02
356.00
45 .
95 .10
1. 16
2.562E-02
364.48
36 .
125.61
1. 17
2.511E-02
375.44
16 .
97 . 63
0 . 44
2.448E-02
387.95
22 .
218.04
1. 19
2 . 380E-02
390.58
7 .
793 . 82
1.20
2 . 360E-02
427.88
48 .
95 . 53
1.23
2 . 186E-02
453.88
33 .
139.47
1.26
2 . 077E-02
468 . 64
33 .
147.09
1.27
2 . 022E-02
487.02
44 .
119.49
1.29
1. 954E-02
497.05
42 .
95.29
1.30
1.919E-02
511. 86
84 .
74 . 63
2 . 56
1.870E-02
563 .24
18 .
187.55
1.36
1.720E-02
569.47
40 .
69 . 06
1.37
1.704E-02
583.62
132 .
23 . 93
2 .10
1.669E-02
609.55
92 .
23 .61
1.23
1. 605E-02
618.06
21.
134 .27
1.42
1. 585E-02
621.92
34 .
79 .19
1.42
1. 576E-02
636.97
16 .
169.86
1.43
1. 543E-02
661.79
8293 .
1.19
1.49
1. 492E-02
747.16
10 .
309.03
1. 53
1. 340E-02
756.73
32 .
87.34
1. 54
1. 325E-02
765.79
20 .
122.83
1. 55
1. 3HE-02
778.92
15 .
199.67
1. 56
1. 291E-02
785 . 42
14 .
216.40
1. 57
1. 281E-02
801.95
38 .
83 . 55
1. 58
1. 258E-02
810.78
38 .
00
00
ro
00
1. 59
1.246E-02
815.77
11.
283 . 87
1. 59
1.239E-02
818.50
36 .
86 .21
1.60
1.235E-02
7/11/2016 8:18:38 AMPage
7 Gamma 20161686.Anl
nuclide
brnch.
act.
nuc
227.00
6 .300
PBC
-------
ORTEC g v - i
TestAmerica Inc
(3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 4
Spectrum name: 7_Gamma_2 01616 86.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
834 . 85
37 .
83 .69
1.61
1.213E-02
834.85
99.980
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 5
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
M - Peak is close to a library peak.
This section based
on library:
Client
Long Revll.
lib
************** J
D
E N T I
F I
ED P
E A K S
U M M A
Y **************
Nuclide
Peak
Centroid
Background
Net Area
Intensity Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec
1 Sigma %
keV
PB-210
185.84
46 . 57
5484 .
19620.
10 . 900
1. 02
0 . 941s
TH-227
200.12
50 .14
32600.
-134 .
-0.074
190.89
0 . 840
AM-2 41
237.80
59 . 56
4335 .
28945.
16.081
0 . 74
0 . 947
TH-234
252.71
63 .29
1778 .
-85 .
-0.047
234.44
0 . 854s
Sn-126
256.68
64 .28
2001.
-13 .
-0.007
478 .20
0 . 856s
BA-133
323.52
80 . 99
1474 .
-58 .
-0 . 032
342.73
0.874s
Np-237
345.53
86 .49
3801.
0 .
0 . 000
539 . 99
0.88OA
EU-155
345 . 74
86 . 54
3511.
48 .
0 . 027
174 . 57
0.880s
Sn-126
347.33
86 . 94
3559 .
0 .
0 . 000
1000.00
0 . 880
Sn-126
349 . 85
87 . 57
3548 .
11.
0 . 006
425 . 92
0.88ID
Cd-109
351.73
88 . 04
3295 .
62 .
0 . 035
130 . 66
0.8 81A
Nd-147
363.97
91.10
3358 .
63 .
0 . 035
131.39
0.885s
TH-234
369.93
92 . 59
3327 .
35 .
0 . 019
233.10
0.886s
AC-228
372.97
93 .35
3482 .
63 .
0 . 035
133 .40
0 . 887
Gd-153
389.57
97 . 50
3668 .
-60 .
-0.033
143.62
0 . 892
Np-239
397.57
99 . 50
3728 .
-60 .
-0 . 033
144.43
0 . 894s
Gd-153
412.38
103.20
3788 .
-59 .
-0 . 033
148.26
0 . 898s
Np-239
414.38
103.70
3847 .
0 .
0 . 000
1000 . 00
0.898s
Np-239
424.10
106.13
3302 .
58 .
0 . 032
139 . 89
0.901s
EU-152
486 .69
121.78
1515 .
48 .
0 . 027
115.58
0.918s
CO - 57
487 . 83
122.06
1563 .
0 .
0 . 000
1000.00
0 . 918s
PA-2 3 4
524.77
131.29
1820 .
54 .
0 . 030
112.57
0 . 928s
HF-181
531. 68
133.02
1874 .
54 .
0 . 030
113.97
0 . 930
CE-144
533.74
133.54
1928 .
33 .
0 . 018
189.51
0.930s
CO - 57
545.48
136.47
1998 .
0 .
0 . 000
1000.00
0.933s
Tc-99m
561.63
140.51
2202 .
-55 .
-0.031
121.51
0 . 938
U-235
574.73
143.79
3535 .
53 .
0 . 029
160 . 54
0 . 941
CE-141
581.35
145.44
3373 .
52 .
0 . 029
157.48
0 . 943s
Ba-140
650.24
162.66
1498 .
-53 .
-0.030
103 .44
0 . 961s
U-235
653.11
163 .38
1541.
-2 .
-0.001
916.93
0 . 962s
CE-13 9
663.01
165.85
1337 .
51.
0 . 028
101. 95
0 . 965s
Cf-251
706.00
176.60
1104 .
-53 .
-0.029
90.40
0 . 976
TH-229
773 . 64
193.51
957 .
-35 .
-0.019
166 .22
0 . 994s
U-235
820.94
205.33
816 .
-29 .
-0.016
73 .32
1. 007
TH-229
843.01
210.85
1231.
52 .
0 . 029
96 .48
1. 012
(Page 7 of 21)
Page 298 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 6
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Cf-251
907 . 62
227.00
730 .
6 .
0 . 004
798.92
1. 029s
PB-212
954.03
238 . 60
626 .
195 .
0 .108
26 .60
0 . 924
PB-214
967.61
242.00
1495 .
7 .
0 . 004
782.07
1. 045s
EU-152
978.39
244 .69
1898 .
-37 .
-0.021
167.33
1. 048
TH -7.7.1
1024.59
256.24
627 .
9 .
0 . 005
533.46
1. 060
Cd-113m
1054.43
263.70
1468 .
-51.
-0.028
107.14
1. 067s
BI-210M
1062.96
265.83
1393 .
-51.
-0.029
43 .33
1.070s
TL-208
1108.77
277.28
737 .
-51.
-0.029
75 . 98
1. 081
1-131
1136 . 83
284 .30
628 .
-19 .
-0.010
118.95
1.089s
PB-214
1180.00
295.09
628 .
24 .
0 . 013
195 . 83
1.100s
PB-212
1199.76
300.03
3308 .
-51.
-0.028
29 .44
1.105s
PA-2 31
1199.92
300.07
3257 .
-51.
-0.028
159 . 91
1.105
PA-233
1200.36
300.18
3206 .
-51.
-0.028
158.67
1.105
PA-2 31
1210.24
302 .65
3155 .
-51.
-0.028
157.06
1.107s
BA-133
1211.05
302.85
3104 .
-51.
-0.028
155.76
1.108s
Ba-140
1219.04
304.85
3054 .
-51.
-0.028
154 .21
1.110
BI-210M
1219.23
304.90
3109 .
-51.
-0.028
155.59
1.110
Ir-192
1233 .41
308.44
3193 .
-51.
-0.028
157.15
1.113s
PA-233
1247.69
312 . 01
2976 .
50 .
0 . 028
155.31
1.117s
Ir-192
1265.61
316.49
2935 .
28 .
0 . 016
270.59
1.122
CR-51
1279.99
320 . 08
2990 .
-13 .
-0.007
598.95
1.125s
La-140
1314.69
328.76
962 .
-51.
-0 . 028
87 . 76
1.134s
Cf-249
1333 .41
333 .44
1014 .
47 .
0 . 026
96 . 92
1.139s
AC-228
1354.61
338.74
216 .
62 .
0 . 034
40 . 81
1.452s
Cs-136
1361.93
340 . 57
1032 .
-10 .
-0.005
471.00
1.146s
EU-152
1376.80
344 .29
1064 .
-20 .
-0 . Oil
233 .65
1.150s
HF-181
1382 . 97
345 . 83
1185 .
15 .
0 . 008
331.17
1.151s
PB-214
1407.39
351.93
751.
42 .
0 . 023
94 .67
1.157s
BA-133
1423 . 66
356.00
907 .
45 .
0 . 025
95 .10
1.162s
1-131
1457.59
364 .48
524 .
36 .
0 . 020
125.61
1.170s
BA-133
1535.03
383 . 84
1416 .
-50 .
-0.028
108.18
1.189s
Cf-249
1551.47
387 . 95
1100 .
22 .
0 . 012
218.04
1.193
SN-113
1566.43
391.69
1330 .
7 .
0 . 004
793.82
1.197s
SB-125
1711.18
427.88
536 .
48 .
0 . 027
95 . 53
1.233s
pm-146
1815.20
453 . 88
544 .
33 .
0 . 018
139.47
1.258s
SB-125
1853.15
463 .37
1087 .
-25 .
-0.014
191.28
1.268s
Ir-192
1871.93
468.06
1185 .
33 .
0 . 019
147.09
1.272s
BE - 7
1910.07
477.60
1333 .
-51.
-0.028
102 . 99
1.282s
HF-181
1927.68
482.00
1384 .
-7 .
-0.004
712.71
1.286s
La-140
1947.77
487 . 02
1339 .
44 .
0 . 024
119.49
1.291s
RU-103
1987.91
497.05
368 .
42 .
0 . 023
95.29
1.301s
RH-106
2047.15
511.86
587 .
84 .
0 . 046
74 . 63
2.565s
Nd-147
2123.70
531.00
351.
0 .
0 . 000
1000 . 00
1.333s
Ba-140
2148.74
537.26
429 .
-47 .
-0.026
101.68
1.339s
CS-134
2252.65
563.24
278 .
18 .
0 . 010
187.55
1.364s
CS-134
2276.99
569.32
351.
-43 .
-0.024
63 .69
1.369s
PA-2 3 4
2277.59
569.47
353 .
40 .
0 . 022
69 . 06
1.370s
BI-207
2278.51
569.70
363 .
-31.
-0.017
88 .60
1.370s
(Page 8 of 21)
Page 299 of 551
-------
ORTEC g v -
i (3263)
Env32 G800W064
7/11/2016 8:18:
:3 8 AMPage
7
TestAmerica Inc
Spectrum name: 7
Gamma 20161686.Anl
Nuclide
Channel
Energy
Background Net
area
Cnts/sec
Uncert
FWHM
TL-208
2334 .19
583.62
172 .
132 .
0 . 073
23 . 93
2 . 096s
SB-125
2401. 71
600.50
1241.
-38 .
-0.021
82 .23
1.399s
SB-124
2410.64
602.73
1204 .
-23 .
-0.013
139.74
1.401
CS-134
2418.55
604.71
1181.
0 .
0 . 000
1000 . 00
1.403s
BI-214
2437.91
609.55
116 .
92 .
0 . 051
23 .61
1.228
PM-144
2471.96
618 . 06
387 .
21.
0 . 012
134 .27
1.415s
RH-106
2487.38
621.92
349 .
34 .
0 . 019
79 .19
1.419s
SB-125
2543.28
635 . 89
332 .
-25 .
-0.014
88 . 70
1.432s
1-131
2547.62
636.97
339 .
16 .
0 . 009
169.86
1.433s
AG-110M
2630.77
657.76
8686 .
-13 .
-0.007
170.40
1.452
CS-137
2646 . 87
661. 79
230 .
8293 .
4 .607
1.19
1.488
PM-144
2785.90
696.54
262 .
-39 .
-0.022
253.10
1.487s
SB-124
2890.87
722 . 79
360 .
-16 .
-0.009
169.56
1.511s
AG-108M
2891.48
722.94
376 .
0 .
0 . 000
1000 . 00
1.511s
EU-154
2893.15
723 .36
375 .
-6 .
-0.004
434.43
1.511s
ZR-95
2896.52
724.20
382 .
0 .
0 . 000
1000 . 00
1.512s
BI-212
2908.41
727.17
420 .
-28 .
-0.016
104.59
1. 515
pm-146
2988.37
747.16
210 .
10 .
0 . 006
309.03
1. 533s
ZR-95
3026.65
756.73
163 .
32 .
0 . 018
87.34
1. 541s
AG-110M
3055.51
763.94
262 .
-25 .
-0.014
392.89
1. 548
NB-95
3062.89
765 . 79
287 .
20 .
0 . 011
122 . 83
1. 549s
PA-234M
3065.38
766 .41
325 .
-37 .
-0.021
70 . 55
1.550s
EU-152
3115.41
778.92
196 .
15 .
0 . 008
199.67
1. 561
BI-212
3141.41
785.42
191.
14 .
0 . 008
216.40
1. 567s
CS-134
3183.20
795 . 87
468 .
-34 .
-0.019
90.25
1. 576s
CS-134
3207.54
801. 95
485 .
38 .
0 . 021
83 . 55
1.581s
CO - 58
3242 . 84
810.78
486 .
38 .
0 . 021
83 . 88
1. 589
La-140
3262 . 82
815.77
524 .
11.
0 . 006
283 . 87
1. 593s
Cs-136
3273.74
818.50
462 .
36 .
0 . 020
86 .21
1. 596s
MN-54
3339.13
834.85
210 .
37 .
0 . 021
83 .69
1.610s
Co - 56
3386.82
846.77
285 .
-9 .
-0.005
414.37
1.620s
TL-208
3442.00
860.56
275 .
7 .
0 . 004
530 . 87
1. 632
NB-94
3484 .13
871.10
306 .
-7 .
-0.004
355.42
1. 641
EU-154
3492.66
873 .23
319 .
14 .
0 . 008
182.39
1. 643s
PA-2 3 4
3521.86
880.53
626 .
-43 .
-0.024
83 .14
1. 649s
PA-2 3 4
3532.70
883 .24
595 .
-10 .
-0.005
356.64
1. 652s
AG-110M
3538.47
884 .68
548 .
19 .
0 . 010
177.26
1.653
Sc-46
3556.86
889.28
622 .
11.
0 . 006
318 .45
1. 657s
y-88
3591.90
898.04
235 .
40 .
0 . 022
86 . 44
1. 664s
AC-228
3644 . 02
911.07
326 .
-19 .
-0.010
99 .65
1. 675s
AG-110M
3749.71
937.49
385 .
-52 .
-0 . 029
36 .24
1.697
PA-2 3 4
3783.82
946.02
320 .
25 .
0 . 014
158.58
1. 704s
EU-152
3856.18
964.11
553 .
37 .
0 . 020
92 . 01
1. 719
AC-228
3875.62
968.97
581.
9 .
0 . 005
387.71
1. 724
EU-154
3985.06
996 .33
761.
-45 .
-0.025
88 . 71
1. 746s
PA-234M
4003.73
1001.00
742 .
-10 .
-0.005
358.08
1.750s
EU-154
4018.84
1004.77
932 .
-49 .
-0 . 027
89 . 02
1. 753s
Co - 56
4151.10
1037.84
195 .
17 .
0 . 009
187.32
1.780s
(Page 9 of 21)
Page 300 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 8
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Cs-136
4192 . 02
1048.07
261.
-18 .
-0 . 010
126 . 87
1. 788s
RH-106
4201.18
1050.36
292 .
39 .
0 . 022
63 .41
1.790s
BI-207
4254.38
1063.66
214 .
18 .
0 . 010
184.19
1.801s
Ga-6 8
4309.34
1077.40
213 .
15 .
0 . 008
227.86
1.812s
FE-59
4396.74
1099.25
245 .
7 .
0 . 004
535.44
1.829s
EU-152
4448.04
1112.07
425 .
20 .
0 . 011
146.01
1. 839
ZN-65
4461.92
1115.55
445 .
0 .
0 . 000
1000 . 00
1. 842s
Sc-46
4481.94
1120.55
445 .
9 .
0 . 005
318.46
1.846A
Ta-182
4484 . 94
1121.30
532 .
-42 .
-0 . 023
79 . 06
1. 846
CO-6 0
4693.50
1173.44
65 .
3255 .
1. 809
1. 86
1. 918
Ta-182
4755.93
1189.05
80 .
5 .
0 . 003
426.18
1.899s
Co - 56
4952.84
1238.28
48 .
6 .
0 . 003
275.00
1.936s
NA-22
5097 . 84
1274.53
40 .
1.
0 . 001
673.61
1.963s
EU-154
5097 . 89
1274.54
41.
0 .
0 . 000
1000 . 00
1.963s
FE-59
5166.10
1291.60
28 .
-2 .
-0.001
538 . 99
1.975s
CO-6 0
5330.42
1332.68
7 .
2889 .
1.605
1. 88
2 .145
AG-110M
5536.89
1384 .30
0 .
10 .
0 . 005
32 . 86
2 . 042
EU-152
5631. 70
1408.00
28 .
-16 .
-0.009
81. 91
2.059s
K-40
5843.01
1460.83
3 .
12 .
0 . 007
33 . 92
2.095s
La-140
6384.49
1596.21
0 .
9 .
0 . 005
33 .33
2.185s
SB-124
6763.55
1690.98
18 .
-8 .
-0.004
132 . 88
2,245s
BI-214
7057.56
1764.49
1.
27 .
0 . 015
19 .60
2,290s
Co - 56
7084.99
1771.35
39 .
-8 .
-0.004
116.06
2,294s
y-88
7343 . 81
1836.06
19 .
-8 .
-0.004
139.85
2,332s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***^
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE-7 C -1.3450E+01 5.31E+01
477.60-1.345E+01 ( 4.594E+01 1.03E+02 1.05E+01 G
NA-22 C 8.9511E-02 9.50E+02
1274.53 8.951E-02 ?( 2.152E+00 6.74E+02 9.99E+01 G
K-40 N 8.8704E+00 4.66E+11
1460.83 8.870E+00 ?(P 7.230E+00 3.39E+01 1.07E+01 G
Sc-46 F 5.3927E-01 8.38E+01
889.28 5.393E-01 ?( 5.765E+00 3.18E+02 1.00E+02 G
1120.55 5.393E-01 } 6.029E+00 3.18E+02 1.00E+02 G
(Page 10 of 21)
Page 301 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 9
TestAmerica Inc
Nuclide Ave activity
CR-51 F -2.573 5E+00
MN-54
1. 7152E+00
Spectrum name: 7_Gamma_2 01616 86.Anl
Energy Activity Code Peak MDA Comments
320.08-2.573E+00 &(
2.77E+01
5.128E+01 5.99E+02 9.94E+00 G
3.12E+02
834.85 1.715E+00 &(P 3.217E+00 8.37E+01 1.00E+02 G
FE-59
6 . 9204E-01
1099.25 6.920E-01 ?(
1291.60-3.668E-01 +
4.45E+01
7.858E+00 5.35E+02 5.65E+01 G
4.325E+00 5.39E+02 4.32E+01 G
Co - 56
4.9858E-01
7.73E+01
846.77-4.021E-01 ( 3.774E+00 4.14E+02 9.99E+01 G
1238.28 5.736E-01 &(P 3.468E+00 2.75E+02 6.61E+01 G
1037.84 6.518E+00 ?(P 2.674E+01 1.87E+02 1.41E+01 G
1771.35-4.676E+00 + 1.862E+01 1.16E+02 1.55E+01 A
CO - 58
1. 6983E+00
810.78 1.698E+00 (
7.09E+01
4.727E+00 8.39E+01 9.95E+01 G
CO-6 0
2 . 0233E+02
1332.50 2.019E+02 (
1.93E+03
1.051E+00 1.88E+00 1.00E+02 G
1173.24 2.028E+02 (P 2.502E+00 1.86E+00 9.99E+01 G
NB-94
¦1. 2031E-01
702.63-1.203E-01 %(
871.10-3.333E-01 +
7 .41E+06
2.817E+00 1.03E+03 9.79E+01 G
4.010E+00 3.55E+02 9.99E+01 G
ZR-95
2 . 4414E+00
756.73 2.441E+00 ?(
724.20 0.000E+00 -
6.40E+01
4.7 95E+00 8.73E+01 5.45E+01 G
8.564E+00 1.00E+03 4.42E+01 G
NB-95
. 4241E-01
765.79 8.424E-01 & (
6.40E+01
3.467E+00 1.23E+02 9.98E+01 G
RU-103
1.3270E+00
497.05 1.327E+00 (
610.30 2.300E-06 &
3.93E+01
2.935E+00 9.53E+01 9.09E+01 G
9.817E+01 1.27E+09 5.75E+00 GA
RH-106
2.9759E+01
621.92 1.213E+01 (
1050.36 1. 42 0E+02 ?(
511.86 1. 242E+01
3.74E+02
3.186E+01 7.92E+01 9.93E+00 G
2.969E+02 6.34E+01 1.56E+00 G
1.716E+01 7.46E+01 2.00E+01 GA
AG-108M
1. 0546E-01
1.53E+05
433.94 1.055E-01 %(P 3.279E+00 1.28E+03 9.05E+01 G
722.94 0.000E+00 - 4.126E+00 1.00E+03 9.08E+01 G
614.28-1.480E-07 % 6.319E+00 1.27E+09 8.98E+01 G
(Page 11 of 21)
Page 302 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:18:38 AMPage 10
Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
AG-110M
1. 6657E+00
2.50E+02
884.68 1.250E+00
(P
7 . 419E+00
1.77E+02
7.27E+01
G
657.16-5.027E-01
+
P
1. 710E+01
1.7 0E+02
9.46E+01
G
937. 49-7.666E+00
+
P
1.3 92E+01
3.62E+01
3.44E+01
G
1384.30 2 . 909E+00
(P
2 . 195E+00
3.29E+01
2.43E+01
G
763 . 94-4.771E+00
+
P
1. 484E+01
3.93E+02
2.23E+01
G
SN-113 F 2.3 932E-01
1.15E+02
391.69 2.393E-01 &(P 6.352E+00 7.94E+02 6.40E+01 G
SB-124 F -7.8802E-01
602 .13-1.
1690.98-1.456E+00 +
722 . 79-5.959E+00 +
6.02E+01
0E-01 ?(P 5.735E+00 1.40E+02 9.83E+01 G
4.091E+00 1.33E+02 4.78E+01 G
3.3 94E+01 1.70E+02 1.08E+01 G
SB-125 I 4 . 1206E+00
427.88 4.121E+00 & (
600.50-7.333E+00 & P
635 . 89-7.838E+00 + P
463 . 37-6.442E+00 + P
1. 01E+03
9.494E+00 9.55E+01 2.96E+01 G
3.192E+01 8.22E+01 1.79E+01 G
2.7 83E+01 8.87E+01 1.13E+01 G
4.066E+01 1.91E+02 1.05E+01 G
1-131 I 1.5241E+00
364.48 9.749E-01 ?(
284 . 30-5.463E+00 + P
636.97 7.782E+00 ?(
8.02E+00
2.962E+00 1.26E+02 8.17E+01 G
3.481E+01 1.19E+02 6.14E+00 G
4.443E+01 1.70E+02 7.17E+00 G
Gd-153 F -1.9980E+00
97.50-1.998E+00 (
103.20-2.672E+00 +
2.42E+02
9.508E+00 1.44E+02 3.00E+01 G
1.312E+01 1.48E+02 2.18E+01 G
Ga-6 8 C 2.9998E+01
1077.40 3.000E+01 ?(
4.71E-02
1.448E+02 2.28E+02 3.30E+00 G
Tc-99m I -6.6055E-01
140 . 51-6.605E-01 &(
2.51E-01
2.661E+00 1.22E+02 8.93E+01 G
BA-133 F 1.583 9E+00
356.00 1.584E+00 ?(
302.85-5.231E+00 &
383.84-1.284E+01 +
80.99-1.872E+00 & P
3.85E+03
4.997E+00 9.51E+01 6.20E+01 G
2.7 02E+01 1.56E+02 1.83E+01 G
4.607E+01 1.08E+02 8.94E+00 GA
5.845E+00 3.43E+02 3.41E+01 GA
CS-134 I 1.9785E+00
604.71 0.000E+00 ?(
795.87-1.769E+00 +
569.32-9.084E+00 +
801.95 1.931E+01 ?(
7.54E+02
5.736E+00 1.00E+03 9.76E+01 G
5.307E+00 9.03E+01 8.55E+01 G
1.908E+01 6.37E+01 1.54E+01 G
5.354E+01 8.36E+01 8.69E+00 G
(Page 12 of 21)
Page 303 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 11
TestAmerica Inc
Nuclide Ave activity
CS-137
3.622 9E+02
Spectrum name: 7_Gamma_2 01616 86.Anl
Energy Activity Code Peak MDA Comments
563.24 7.069E+00 ?(P 3.109E+01 1.88E+02 8.35E+00 G
1.10E+04
661.66 3.623E+02 (P 3.208E+00 1.19E+00 8.52E+01 G
CE-139
7 .2943E-01
165.85 7.294E-01 ?(
1.38E+02
2.466E+00 1.02E+02 7.99E+01 G
Ba-140
¦5 . 9209E+00
1.28E+01
537.26-5.921E+00 &(P 1.261E+01 1.02E+02 2.44E+01 G
162.66-9.843E+00 + 3.375E+01 1.03E+02 6.22E+00 G
304.85-2.252E+01 + 1.152E+02 1.54E+02 4.29E+00 G
La-140 I 1.0585E+00
1596.21 7.780E-01 ?(
487.02 2.729E+00 &
328 . 76-5.052E+00 -
815.77 2.208E+00 ?(
1.28E+01
6.371E-01 3.33E+01 9.54E+01 G
1.083E+01 1.19E+02 4.55E+01 G
1.469E+01 8.78E+01 2.03E+01 G
2.106E+01 2.84E+02 2.33E+01 G
CE-141 I 1.1523E+00
145.44 1.152E+00 ?(
3.25E+01
6.016E+00 1.57E+02 4.82E+01 G
CE-144 I 3 . 0200E+00
133.54 3.020E+00 ?(
2.85E+02
1.903E+01 1.90E+02 1.11E+01 G
PM-144 C -3 . 9565E-01
3.63E+02
696.54-1.535E+00 &(P 3.073E+00 2.53E+02 9.90E+01 G
618.06 7.427E-01 ?( 3.338E+00 1.34E+02 9.91E+01 G
EU-152 F 3.9627E+00
4.94E+03
344 .29-
1112.07
121.78
778.92
964.11
244.69-
1408.00-
577E+00
774E+00
664E+00
988E+00
311E+01
690E+00
599E+00
? (
(
Sc. (
+
+
1
4
6
2
4
4
9
23 0E+01
290E+01
381E+00
260E+01
006E+01
276E+01
626E+00
34E+02
46E+02
16E+02
00E+02
20E+01
67E+02
19E+01
65E+01 G
36E+01 G
86E+01 G
29E+01 G
46E+01 G
58E+00 G
10E+01 GA
EU-154 I 5.43 83E+00
3.14E+03
'73 .23 5.43 8E+00 ?( 3.338E+01 1.82E+02 1.23E+01 G
123 .10-6.218E-02 %
1274.54 0.000E+00 -
723 .36-1.262E+00 -
1004.77-1.475E+01 +
996.33-2.258E+01 &
4.172E+00 3.20E+03 4.08E+01 G
6.206E+00 1.00E+03 3.52E+01 G
1.853E+01 4.34E+02 2.02E+01 G
4.3 53E+01 8.90E+01 1.80E+01 G
6.644E+01 8.87E+01 1.06E+01 G
(Page 13 of 21)
Page 304 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 12
TestAmerica Inc
Nuclide Ave activity
EU-155 I 9.6270E-01
Spectrum name: 7_Gamma_2 01616 86.Anl
Energy Activity Code Peak MDA Comments
1.81E+03
105.31-3.343E-02 %(P 1.356E+01 1.14E+04 2.12E+01 G
86.54 1.651E+00 & ( 9.555E+00 1.75E+02 3.07E+01 G
HF-181
4 . 7049E-01
482 . 00-2.587E-01 ?(
133.02 1.270E+00 ?(
4.24E+01
6.163E+00 7.13E+02 8.05E+01 G
4.7 98E+00 1.14E+02 4.33E+01 G
345.83 2.070E+00 ?(P 2.289E+01 3.31E+02 1.51E+01 G
136.30 6.434E-01
3.699E+01 1.72E+03 5.85E+00 G
Ta-182
¦7 .2014E+00
1.14E+02
1121.30-7.201E+00 ?( 1.886E+01 7.91E+01 3.49E+01 G
1221.41 4.974E-02 % P 9.189E+00 8.37E+03 2.70E+01 G
1189.05 1.867E+00 + P 1.728E+01 4.26E+02 1.62E+01 G
Hg-203
7 . 7437E-02
279.20 7.744E-02 %(
4.66E+01
2.922E+00 1.12E+03 8.15E+01 G
TL-208
N
5.1870E+00
6.98E+02
583.02 5.187E+00 * (P 2.517E+00 2.39E+01 8.45E+01 G
3.587E+01 7.60E+01 6.31E+00 G
P 3.030E+01 5.31E+02 1.24E+01 G
277.28-1.427E+01
860.56 2.608E+00
pm-146
1.3104E+00
747.16 1.220E+00 & (
735.72 3.030E-01 %
453.88 1. 3 58E+00 &(
2.02E+03
8.566E+00 3.09E+02 3.40E+01 G
1.263E+01 1.83E+03 2.25E+01 G
4.584E+00 1.39E+02 6.50E+01 G
y-
2.0689E+00
898.04 2.069E+00 * (
1836.06-7.569E-01 -
1.07E+02
3.868E+00 8.64E+01 9.37E+01 G
2.178E+00 1.40E+02 9.92E+01 G
Cd-113m
Cd-109
Cf-251
¦1.4268E+04
1. 7173E+01
-3 . 7086E+00
263 . 70-1.427E+04 ?(
.04 1.717E+01 }(
176.60-3.709E+00 ?(
227.00 1.487E+00 +
5.33E+03
5.070E+04 1.07E+02 6.00E-03 K
4.53E+02
Derived Ave Activity
7.433E+01 1.31E+02 3.79E+00 G
3.28E+05
1.111E+01 9.04E+01 1.70E+01 G
3.019E+01 7.99E+02 6.30E+00 GA
Cf-249
1. 8012E+00
387.95 7 . 648E-01 &(
333.44 6.212E+00 &(
1.28E+05
5.564E+00 2.18E+02 6.60E+01 G
1.997E+01 9.69E+01 1.55E+01 G
(Page 14 of 21)
Page 305 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 13
TestAmerica Inc
Nuclide Ave activity
Sn-126
PB-210
N
¦1. 8599E+00
1.033 0E+04
Spectrum name: 7_Gamma_2 01616 86.Anl
Energy Activity Code Peak MDA Comments
87.57 3.115E-01 }
64.28-1.860E+00 & (
86.94 0 . 000E+00 }
3 . 65E+07
7.814E+00 4.26E+02 3.75E+01 GA
2.964E+01 4.78E+02 9.70E+00 G
3.259E+01 1.00E+03 9.04E+00 GA
8.14E+03
46.54 1.033E+04 @(P 1.831E+02 1.02E+00 4.25E+00 G
PB-212
N
6 . 9398E+00
6.98E+02
238.63 6.940E+00 (P 4.250E+00 2.66E+01 4.33E+01 G
300.03-2.927E+01 - P 1.546E+02 2.94E+01 3.28E+00 GA
PB-214
N
2 . 3462E+00
5 . 84E+05
351.93 2 . 370E+00 (P 7.444E+00 9.47E+01 3.76E+01 G
295.09 2.300E+00 (P 1.143E+01 1.96E+02 1.93E+01 G
242.00 1.470E+00 ? 3.842E+01 7.82E+02 7.43E+00 GA
BI-207
1. 3029E-02
569 . 70-1.036E+00 ?(
1.18E+04
3.052E+00 8.86E+01 9.77E+01 G
1063.66 1.389E+00 &(P 5.414E+00 1.84E+02 7.45E+01 G
BI-212
N
¦1.5101E+01
727 . 17-1.510E+01 (
785.42 4.629E+01 ?
6.98E+02
5.264E+01 1.05E+02 7.55E+00 G
2.275E+02 2.16E+02 1.28E+00 GA
BI-214
N
6 . 9422E+00
609.31 6 . 942E+00
1120.29 0.000E+00 }
5.84E+05
(P 3.965E+00 2.36E+01 4.61E+01 G
3.913E+01 1.60E+03 1.51E+01 G
1764.49 1.607E+01 + P 4.329E+00 1.96E+01 1.54E+01 G
BI-210M
¦1. 7361E+00
1.10E+09
265.83-1.736E+00 ?(P 5.969E+00 4.33E+01 5.00E+01 G
304.90-3.451E+00 + 1.780E+01 1.56E+02 2.80E+01 G
AC-228 N 8.5576E-01 2.10E+03
911.07-3.218E+00 ?(P 1.482E+01 9.97E+01 2.90E+01 G
968.97 2.646E+00 & P 3.448E+01 3.88E+02 1.75E+01 G
338.32 1.069E+01 (P 1.231E+01 4.08E+01 1.20E+01 G
93.35 1.148E+01 5.072E+01 1.33E+02 5.56E+00 XA
TH-227
N
-3 . 2733E+01
50.14-3.273E+01 (
7.95E+03
2.063E+02 1.91E+02 8.00E+00 G
256.24 2.059E+00 + P 2.794E+01 5.33E+02 7.00E+00 G
TH-229
N
3 . 6472E+00
193 . 51-1.029E+01 (
210.85 2.416E+01 &(
2.68E+06
4.319E+01 1.66E+02 4.40E+00 G
7.727E+01 9.65E+01 2.99E+00 G
(Page 15 of 21)
Page 306 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:18:38 AMPage 14
Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
TH-234
N
-3 . 0966E+01
1.63E+12
63 .29-3.097E+01
(P
7 . 253E+01
2.34E+02 3.81E+00
G
92.59 6.404E+00
+ P
4 . 954E+01
2.33E+02 5.58E+00
G
PA-2 31
N
-3 .3268E+01
1.20E+07
302.65-3.327E+01
& (
1. 733E+02
1.57E+02 2.88E+00
G
300.07-3.858E+01
+
2.045E+02
1.60E+02 2.46E+00
G
PA-233
C
2 . 6832E+00
7.82E+08
312.01 2.683E+00
& (
1.3 82E+01
1.55E+02 3.60E+01
G
300.18-1.531E+01
+
8.055E+01
1.59E+02 6.20E+00
G
PA-2 3 4
N
7 . 8698E+00
1.63E+12
131.29 3.033E+00
(
1.132E+01
1.13E+02 1.80E+01
G
946.02 9 . 555E+00
? (
3.2 90E+01
1.59E+02 1.34E+01
G
569.47 1. 573E+01
? (
3.592E+01
6.91E+01 8.20E+00
G
883 . 24-4.873E+00
8c
5.839E+01
3.57E+02 9.60E+00
G
880.53-3.464E+01
+
9.548E+01
8.31E+01 6.00E+00
GA
PA-234M
N
-6 .1574E+01
1.63E+12
1001.00-6.157E+01
&(p
8.3 50E+02
3.58E+02 8.37E-01
G
766 . 41-5.362E+02
8c
1.2 51E+03
7.05E+01 2.94E-01
G
U-235
N
5.0557E+00
2.57E+11
143.79 5.056E+00
&(p
2.691E+01
1.61E+02 1.10E+01
G
205.33-7.754E+00
+ p
3.685E+01
7.33E+01 5.01E+00
G
163.38-5.155E-01
& p
4.207E+01
9.17E+02 5.08E+00
G
AM-241 T 1.2102E+03
59.54 1. 210E+03 (
1.58E+05
1.2 94E+01 7.43E-01 3.59E+01 G
Ir-192 F 1.0607E+00
316.49 6.392E-01 &(
468.06 1. 769E+00 ?(
308 .44-3.083E+00 &
7.40E+01
5.747E+00 2.71E+02 8.70E+01 G
8.661E+00 1.47E+02 5.18E+01 G
1.607E+01 1.57E+02 3.18E+01 G
Cs-136 F 1.6172E+00
818.50 1.617E+00 &(
1048.07-1.287E+00 -
340.57-4.302E-01 &
1.30E+01
4.629E+00 8.62E+01 1.00E+02 G
5.480E+00 1.27E+02 8.00E+01 G
6.7 82E+00 4.71E+02 4.69E+01 G
Np-239 T 2.5310E+00
103.70 0.000E+00 -
106.13 2.531E+00 ?(
99 . 50-3.985E+00 +
2.36E+00
1.201E+01 1.00E+03 2.40E+01 X
1.173E+01 1.40E+02 2.27E+01 G
1.907E+01 1.44E+02 1.50E+01 X
(Page 16 of 21)
Page 307 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 15
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
Nd-147 1.5565E+00 1.11E+01
531.00 0.000E+00 *( 2.124E+01 1.00E+03 1.30E+01 G
91.10 2.272E+00 ?( 9.887E+00 1.31E+02 2.83E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
TH-227
50 . 14
32600.
-134 .
-0 . 074
190 . 89
-3.273E+01
TH-234
63 .29
1778 .
-85 .
-0 . 047
234 .44
-3.097E+01
P
BA-133
cn
en
o
00
1474 .
-58 .
-0 . 032
342.73
-1.872E+00
P
EU-155
86 . 54
3511.
48 .
0 . 027
174.57
1.651E+00
Nd-147
91.10
3358 .
63 .
0 . 035
131.39
2.272E+00
TH-234
92 . 59
3327 .
35 .
0 . 019
233.10
6.404E+00
P
Gd-153
97 . 50
3668 .
-60 .
-0 . 033
143.62
-1.998E+00
Np-239
99 . 50
3728 .
-60 .
-0 . 033
144.43
-3.985E+00
Gd-153
103.20
3788 .
-59 .
-0 . 033
148.26
-2.672E+00
Np-239
106.13
3302 .
58 .
0 . 032
139.89
2.531E+00
PA-2 3 4
131.29
1820 .
54 .
0 . 030
112.57
3.033E+00
(Page 17 of 21)
Page 308 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 16
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
HF-181
133.02
1874
54 .
0 . 030
113.97
1.270E+00
CE-144
133.54
1928
33 .
0 . 018
189.51
3 . 020E+00
Tc-99m
140.51
2202
-55 .
-0.031
121. 51
-6 . 605E-01
CE-141
145.44
3373
52 .
0 . 029
157 .48
1.152E+00
Ba-140
162.66
1498
-53 .
-0.030
103 .44
-9.843E+00
CE-13 9
165.85
1337
51.
0 . 028
101.95
7 . 294E-01
Cf-251
176.60
1104
-53 .
-0.029
90.40
-3 . 709E+00
TH-229
193.51
957
-35 .
-0.019
166 .22
-1.029E+01
TH-229
210 . 85
1231
52 .
0 . 029
96 .48
2 . 416E+01
Cf-251
227.00
730
6 .
0 . 004
798.92
1. 487E+00
PB-214
242.00
1495
7 .
0 . 004
782.07
1. 470E+00
TH-227
256 .24
627
9 .
0 . 005
533.46
2.059E+00
P
Cd-113m
263.70
1468
-51.
-0.028
107.14
-1.427E+04
BI-210M
265 . 83
1393
-51.
-0.029
43 .33
-1.736E+00
P
1-131
284 .30
628
-19 .
-0.010
118.95
- 5.463E+00
P
PB-214
295.09
628
24 .
0 . 013
195 . 83
2.3 00E+00
P
PA-2 31
300.07
3257
-51.
-0.028
159 . 91
-3.858E+01
PA-233
300.18
3206
-51.
-0.028
158 .67
-1.531E+01
PA-2 31
302.65
3155
-51.
-0.028
157.06
-3.327E+01
BA-133
302.85
3104
-51.
-0.028
155.76
- 5.231E+00
Ba-140
304.85
3054
-51.
-0.028
154 .21
-2.252E+01
BI-210M
304.90
3109
-51.
-0.028
155.59
-3.451E+00
PA-233
312.01
2976
50 .
0 . 028
155.31
2.683E+00
CR-51
320.08
2990
-13 .
-0.007
598.95
-2.573E+00
Cf-249
333.44
1014
47 .
0 . 026
96 . 92
6.212E+00
Cs-136
340 . 57
1032
-10 .
-0.005
471.00
-4.3 02E-01
HF-181
345.83
1185
15 .
0 . 008
331.17
2.070E+00
P
PB-214
351.93
751
42 .
0 . 023
94 .67
2.370E+00
P
BA-133
356.00
907
45 .
0 . 025
95 .10
1.584E+00
1-131
364 .48
524
36 .
0 . 020
125.61
9.749E-01
BA-133
383 . 84
1416
-50 .
-0.028
108.18
-1.284E+01
Cf-249
387 . 95
1100
22 .
0 . 012
218.04
7.648E-01
SB-125
427.88
536
48 .
0 . 027
95 . 53
4.121E+00
pm-146
453.88
544
33 .
0 . 018
139.47
1.3 58E+00
SB-125
463 .37
1087
-25 .
-0 . 014
191.28
-6.442E+00
P
BE - 7
477.60
1333
-51.
-0 . 028
102 . 99
-1.345E+01
HF-181
482.00
1384
-7 .
-0.004
712 . 71
-2 . 587E-01
RU-103
497.05
368
42 .
0 . 023
95.29
1. 327E+00
RH-106
511. 86
587
84 .
0 . 046
74 . 63
1.242E+01
Ba-140
537.26
429
-47 .
-0 . 026
101.68
-5.921E+00
P
CS-134
563.24
278
18 .
0 . 010
187.55
7.069E+00
P
CS-134
569.32
351
-43 .
-0 . 024
63 .69
-9.084E+00
PA-2 3 4
569.47
353
40 .
0 . 022
69 . 06
1.573E+01
BI-207
569.70
363
-31.
-0.017
o
00
00
-1.036E+00
SB-125
600 . 50
1241
-38 .
-0 . 021
ro
CM
CM
00
-7 .333E+00
P
SB-124
602.73
1204
-23 .
-0.013
139.74
-7.880E-01
P
PM-144
618.06
387
21.
0 . 012
134 .27
7.427E-01
RH-106
621. 92
349
34 .
0 . 019
79 . 19
1.213E+01
(Page 18 of 21)
Page 309 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 17
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
Nuclide
Channel Energy Background Net
area i
Cnts/sec
Uncert FWHM
SB-125
635.89
332 .
-25 .
-0 . 014
88 . 70
-7.838E+00
P
1-131
636.97
339 .
16 .
0 . 009
169 . 86
7.782E+00
AG-110M
657.76
8686 .
-13 .
-0.007
170.40
-5.027E-01
P
PM-144
696 . 54
262 .
-39 .
-0 . 022
253.10
-1.535E+00
P
SB-124
722 . 79
360 .
-16 .
-0.009
169.56
-5.959E+00
EU-154
723 .36
375 .
-6 .
-0.004
434.43
-1.262E+00
BI-212
727.17
420 .
-28 .
-0.016
104.59
-1.510E+01
pm-146
747 . 16
210 .
10 .
0 . 006
309.03
1.220E+00
ZR-95
756.73
163 .
32 .
0 . 018
87.34
2.441E+00
AG-110M
763.94
262 .
-25 .
-0 . 014
392.89
-4.771E+00
P
NB-95
765 . 79
287 .
20 .
0 . 011
122.83
8.424E-01
PA-234M
766.41
325 .
-37 .
-0.021
70 . 55
- 5.3 62E+02
BI-212
785 . 42
191.
14 .
0 . 008
216.40
4.629E+01
CS-134
795.87
468 .
-34 .
-0.019
90.25
-1.769E+00
CS-134
801. 95
485 .
38 .
0 . 021
83 . 55
1.931E+01
CO - 58
810.78
486 .
38 .
0 . 021
83 . 88
1.698E+00
Cs-136
818.50
462 .
36 .
0 . 020
86 .21
1.617E+00
MN-54
834.85
210 .
37 .
0 . 021
83 .69
1.715E+00
P
Co - 56
846.77
285 .
-9 .
-0.005
414.37
-4.021E-01
NB-94
871.10
306 .
-7 .
-0 . 004
355.42
-3.333E-01
EU-154
873 .23
319 .
14 .
0 . 008
182.39
5.43 8E+00
PA-2 3 4
880.53
626 .
-43 .
-0 . 024
83 .14
-3.464E+01
PA-2 3 4
883 .24
595 .
-10 .
-0.005
356.64
-4.873E+00
AG-110M
884 .68
548 .
19 .
0 . 010
177.26
1.250E+00
P
y-88
898.04
235 .
40 .
0 . 022
86 . 44
2.069E+00
AG-110M
937.49
385 .
-52 .
-0.029
36 .24
-7.666E+00
P
PA-2 3 4
946.02
320 .
25 .
0 . 014
158.58
9.555E+00
EU-154
996.33
761.
-45 .
-0.025
88 . 71
-2.258E+01
PA-234M
1001.00
742 .
-10 .
-0.005
358.08
-6.157E+01
P
EU-154
1004.77
932 .
-49 .
-0 . 027
89 . 02
-1.475E+01
Co - 56
1037.84
195 .
17 .
0 . 009
187.32
6.518E+00
P
Cs-136
1048.07
261.
-18 .
-0.010
126 . 87
-1.287E+00
RH-106
1050.36
292 .
39 .
0 . 022
63 .41
1.42 0E+02
BI-207
1063.66
214 .
18 .
0 . 010
184.19
1.389E+00
P
Ga-6 8
1077.40
213 .
15 .
0 . 008
227.86
3.000E+01
FE-59
1099.25
245 .
7 .
0 . 004
535.44
6.920E-01
Ta-182
1121.30
532 .
-42 .
-0 . 023
79 . 06
-7.201E+00
Ta-182
1189.05
80 .
5 .
0 . 003
426.18
1.867E+00
P
Co - 56
1238.28
48 .
6 .
0 . 003
275.00
5.736E-01
P
NA-22
1274.53
40 .
1.
0 . 001
673.61
8.951E-02
FE-59
1291.60
28 .
-2 .
-0.001
538.99
-3.668E-01
AG-110M
1384.30
0 .
10 .
0 . 005
32 . 86
2.909E+00
P
SB-124
1690.98
18 .
-8 .
-0 . 004
132 . 88
-1.456E+00
Co - 56
1771.35
39 .
-8 .
-0.004
116.06
-4.676E+00
y-88
1836.06
19 .
-8 .
-0.004
139.85
-7.569E-01
P - Peakbackground
subtraction
(Page 19 of 21)
Page 310 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:18:38 AMPage 18
TestAmerica Inc Spectrum name: 7_Gamma_2 01616 86.Anl
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#A
-1. 3450E+01
-1.3450E+01
1.03 0E+02 %
4.59E+01
NA-22
#A
8 . 9511E-02
8.9511E-02
6.73 6E+02 %
2.15E+00
K-40
#
8 . 8704E+00
8.8704E+00
3.392E+01%
7.23E+00
Sc-46
#A
5 . 3927E-01
5.3927E-01
3.184E+02 %
5.76E+00
CR-51
#A
-2 . 5735E+00
-2.573 5E+00
5.990E+02 %
5.13E+01
MN-54
#A
1. 7152E+00
1.7152E+00
8.369E+01%
3.22E+00
FE-59
#A
6 . 9204E-01
6.9204E-01
5.3 54E+02 %
7.86E+00
Co - 56
#A
4.9858E-01
4.9858E-01
1.771E+02 %
3.77E+00
CO - 57
#A
0.0000E+00
0.0000E+00
7.071E+02 %
2.16E+00
CO - 58
#A
1.6983E+00
1.6983E+00
8.388E+01%
4.73E+00
CO-6 0
2 . 0233E+02
2.0233E+02
1.321E+00%
1.05E+00
ZN-65
#A
0.0000E+00
0.0000E+00
1. 000E+03 %
1.19E+01
NB-94
#A
-1.2031E-01
-1.2031E-01
1.026E+03 %
2.82E+00
ZR-95
#A
2 . 4414E+00
2.4414E+00
8.734E+01%
4.79E+00
NB-95
#A
8 . 4241E-01
8.4241E-01
1.22 8E+02 %
3.47E+00
RU-103
#A
1. 3270E+00
1.3270E+00
9 . 529E+01%
2.93E+00
RH-106
#A
2.9759E+01
2.9759E+01
5 . 072E+01%
3.19E+01
AG-108M#A
1.0546E-01
1.0546E-01
1.277E+03%
3.28E+00
AG-110M#A
1. 6657E+00
1.6657E+00
3.286E+01%
7.42E+00
SN-113
A
2 . 3932E-01
2.3 932E-01
7.93 8E+02 %
6.3 5E+00
SB-124
#A
-7.8802E-01
-7.8802E-01
1.3 97E+02 %
5.74E+00
SB-125
#A
4 . 1206E+00
4.1206E+00
9.553E+01%
9.49E+00
1-131
#A
1. 5240E+00
1.5241E+00
1.056E+02 %
2.96E+00
Gd-153
#A
-1.9980E+00
-1.9980E+00
1.43 6E+02 %
9.51E+00
Ga-6 8
#A
2.9814E+01
2.9998E+01
2.279E+02%
1.45E+02
Tc-99m
#A
-6.5979E-01
-6.6055E-01
1.215E+02%
2.66E+00
BA-133
#A
1.583 9E+00
1.583 9E+00
9.510E+01%
5.00E+00
CS-134
#A
1.9785E+00
1.9785E+00
8.355E+01%
5.74E+00
CS-137
3.622 9E+02
3.622 9E+02
1.191E+00%
3.21E+00
CE-139
#A
7.2943E-01
7.2943E-01
1.019E+02 %
2.47E+00
Ba-140
#A
-5.9207E+00
-5.9209E+00
1.017E+02 %
1.26E+01
La-140
#
1.0585E+00
1.0585E+00
3.333E+01%
6.3 7E-01
CE-141
#A
1.1523E+00
1.1523E+00
1.575E+02%
6.02E+00
CE-144
#A
3.0199E+00
3.0200E+00
1.895E+02%
1.90E+01
PM-144
#A
-3.9564E-01
-3.9565E-01
1.343E+02 %
3.07E+00
EU-152
A
3 . 9627E+00
3.9627E+00
7 . 419E+01%
1.23E+01
EU-154
#A
5 .4383E+00
5.43 83E+00
1.824E+02 %
3.34E+01
EU-155
#A
9 . 6270E-01
9.6270E-01
1.746E+02 %
1.36E+01
HF-181
#A
4 . 7049E-01
4.7049E-01
1.14 0E+02 %
6.16E+00
Ta-182
#A
-7 . 2014E+00
-7.2014E+00
7.906E+01%
1.89E+01
Hg-203
#A
7 . 7436E-02
7.7437E-02
1.123E+03 %
2.92E+00
TL-208
5.1870E+00
5.1870E+00
2.393E+01%
2.52E+00
pm-146
#A
1.3104E+00
1.3104E+00
1.3 95E+02 %
8.57E+00
(Page 2 0 of 21)
Page 311 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 8:
18:38 AMPage 19
TestAmerica
Inc
Spectrum
name: 7 Gamma
20161686.Anl
y-88
#A
2.0688E+00
2.0689E+00
8.644E+01%
3.87E+00
Cd-113m#A
-1.4268E+04
-1.4268E+04
1.071E+02 %
5.07E+04
Cd-109
#A
1. 7173E+01
1.7173E+01
1.3 07E+02 %
7.43E+01
Cf-251
#A
-3 . 7086E+00
-3.7086E+00
9.040E+01%
1.11E+01
Cf-249
#A
1. 8012E+00
1.8012E+00
9.692E+01%
5.56E+00
Sn-126
A
-1.8599E+00
-1. 8599E+00
4.782E+02 %
2.96E+01
PB-210
#
1.033 0E+04
1.033 0E+04
1.016E+00%
1.83E+02
PB-212
6 . 9398E+00
6.93 98E+00
2.660E+01%
4.25E+00
PB-214
#A
2 . 3462E+00
2.3462E+00
9.467E+01%
7.44E+00
BI-207
#A
1.3029E-02
1.3029E-02
8.860E+01%
3.05E+00
BI-212
#A
-1.5101E+01
-1.5101E+01
1.046E+02 %
5.26E+01
BI-214
6 . 9422E+00
6.9422E+00
2 .361E+01%
3.97E+00
BI-210M#A
-1. 7361E+00
-1.7361E+00
4.333E+01%
5.97E+00
AC-228
A
8.5576E-01
8.5576E-01
4.081E+01%
1.48E+01
TH-227
#A
-3.2733E+01
-3.2733E+01
1.909E+02 %
2.06E+02
TH-229
#A
3 . 6472E+00
3.6472E+00
9.610E+01%
4.32E+01
TH-234
#A
-3 . 0966E+01
-3.0966E+01
2.344E+02 %
7.25E+01
PA-2 31
#A
-3 .3268E+01
-3.3268E+01
1.571E+02 %
1.73E+02
PA-233
#A
2 . 6832E+00
2.6832E+00
1. 553E+02%
1.38E+01
PA-2 3 4
#A
7 . 8698E+00
7.8698E+00
6 . 879E+01%
1.13E+01
PA-234M#A
-6 .1574E+01
-6.1574E+01
3.581E+02%
8.3 5E+02
U-235
#A
5.0557E+00
5.0557E+00
1.605E+02%
2.69E+01
AM-2 41
1.2102E+03
1.2102E+03
7.433E-01%
1.29E+01
Np-237
#A
0.0000E+00
0.0000E+00
1.000E+03 %
2.33E+01
Ir-192
A
1.0607E+00
1.0607E+00
1.471E+02%
5.75E+00
Cs-136
#A
1. 6172E+00
1.6172E+00
8.621E+01%
4.63E+00
Np-239
#A
2 . 5306E+00
2.5310E+00
1.3 99E+02 %
1.17E+01
Nd-147
#A
1. 5565E+00
1.5565E+00
1.314E+02 %
2.12E+01
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.1 keV) 1.212E+04 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.1 keV) 1.2123812E+04 Bq/Sample
(Page 21 of 21)
Page 312 of 551
-------
257060_Gamma_LCS 160-257060-2-A. 7_Gamma_20161686.spc.
1.0e6n
1.0e5-
Channels
-------
Test America St. Louis Spectrum ID: 5_Gamma_2 0161261
Sample Description: 257060_Gamma_160-17814-A-l-B
Detector: Detector # 5
Batch ID: 257060
Work Order Number: Gamma
Lot Number: 160-17814-A-l-B
Decay to Time: 7/11/2016 07:46 Live Time: 1800 sec
Acquisition Time: 7/11/2016 07:46:20 Real Time: 1807 sec
Analysis Time: 7/11/2016 08:17 Dead Time: 0.38 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
5_Soil_TunaCan.Clb
5_Soil_TunaCan_90099_032612
3/27/2012 17:20
2/28/2012 19:35
Client_Long_Revll.lib
5 2016-07-10 0601.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
3.3 77E+00
132 .4
4 . 470E+00
4.474E+00
1.532E+01
NA-22
3.23 7E-02
1396 .4
4.520E-01
4.520E-01
1.741E+00
K-40
1.401E+02
8 . 8
1.229E+01
1.423E+01
1.187E+01
Sc-46
-6.455E-01
110 . 6
7.136E-01
7.144E-01
2.436E+00
CR-51
3.783E+00
126 .3
4.779E+00
4.783E+00
1.617E+01
MN-54
-3.511E-01
172 . 7
6.065E-01
6.068E-01
1.572E+00
FE-59
8.193E-01
91. 7
7.513E-01
7.524E-01
3.216E+00
Co - 56
1.286E+00
37 . 8
4.864E-01
4.908E-01
1.167E+00
CO - 57
2.878E-01
142 . 4
4.097E-01
4.100E-01
9.817E-01
CO - 58
1.257E-01
469 . 7
5.902E-01
5.903E-01
2.101E+00
CO-6 0
6 . 530E-01
48 . 7
3.181E-01
3.197E-01
1.387E+00
ZN-65
-1.528E+00
142 .3
2.174E+00
2.175E+00
7.426E+00
NB-94
6 . 013E-02
742 . 7
4.466E-01
4.466E-01
1.173E+00
ZR-95
-6.895E-01
220 . 8
1. 523E+00
1.523E+00
2.825E+00
NB-95
-1.198E+00
77 . 9
9.33 IE-01
9.352E-01
3.109E+00
RU-103
-1.455E-01
297 . 5
4.328E-01
4.329E-01
1.142E+00
RH-106
-5.542E+00
195 . 0
1.080E+01
1.081E+01
3.659E+01
AG-108M
3.915E-01
102 . 8
4.027E-01
4.032E-01
1.025E+00
AG-110M
6.240E-01
35.4
2.206E-01
2.229E-01
2.936E+00
SN-113
4.207E-01
151. 0
6.3 54E-01
6.358E-01
2.182E+00
SB-124
5 . 060E-01
40 . 8
2.066E-01
2.082E-01
3.43 7E+00
SB-125
8 .418E-01
72 .2
6.075E-01
6.090E-01
3.621E+00
1-131
1.089E+00
47 . 8
5.207E-01
5.237E-01
8.566E-01
Gd-153
3.511E-01
146 . 0
5.127E-01
5.132E-01
2.693E+00
Ga-6 8
2 . 679E+01
33 .3
8.929E+00
9.054E+00
2.194E+01
Tc-99m
-3 . 253E-01
126 . 0
4.098E-01
4.102E-01
1.376E+00
BA-133
-4 . 483E-02
2365.3
1.060E+00
1.060E+00
3.636E+00
CS-134
1.878E-01
184 .3
3.462E-01
3.463E-01
3.469E+00
CS-137
-2.638E-01
224 . 0
5.909E-01
5.911E-01
2.162E+00
CE-139
0.000E+00
1.#INF
2.034E-01
2.034E-01
1.150E+00
Ba-140
1.547E+00
105 . 1
1.625E+00
1.627E+00
4.198E+00
La-140
1. 930E-02
104 . 1
2.009E-02
2.012E-02
1.697E+00
CE-141
-6 . 945E-01
127 . 7
8.867E-01
8.874E-01
2.970E+00
(Page 1 of 21)
Page 314 of 551
-------
CE-144
-2 . 653E+00
136
PM-144
-5 .130E-01
103
EU-152
-1.051E-01
97
EU-154
4.971E+00
84
EU-155
2 . 124E-01
735
HF-181
3 . 698E-01
135
Ta-182
1.785E+00
77
Hg-203
3.349E-02
1126
TL-208
3.797E+00
15
pm-146
1.153E-02
104
y-88
-5 . 104E-01
112
Cd-113m
2.747E+03
175
Cd-109
-8 . 434E+00
148
Cf-251
9.887E-01
168
Cf-249
2.3 07E-03
508
Sn-126
-3 . 845E+00
123
PB-210
4 . 340E-01
3187
PB-212
9.155E+00
8
PB-214
1.214E+01
9
BI-207
3.871E-01
93
BI-212
7.727E+00
136
BI-214
1.190E+01
11
BI-210M
-7.091E-01
99
AC-228
1.212E+01
11
TH -7.7.1
3 . 627E+00
106
TH-229
2.910E+00
105
TH-234
2.467E+01
36
PA-2 31
-1.719E+01
144
PA-233
-1.035E+00
205
PA-2 3 4
2 . 739E-01
104
PA-234M
8 . 482E+01
92
U-235
-2 . 733E+00
124
AM-2 41
-1.490E+00
73
Np-237
-2 . 350E+00
165
Ir-192
1. 292E-01
81
Cs-136
1.791E-01
128
Np-239
9.352E-01
152
Nd-147
-2.150E+00
177
Total 3 .114E+03
Analyst: Amanda Dick
3 . 620E+00
3.622E+00
1.214E+01
5.326E-01
5.333E-01
1.441E+00
1. 026E-01
1.028E-01
7.571E+00
4 . 204E+00
4.212E+00
1.422E+01
1. 562E+00
1.563E+00
5.326E+00
4.999E-01
5.003E-01
2.245E+00
1.381E+00
1.384E+00
6.415E+00
3.774E-01
3.774E-01
1.33 0E+00
5.964E-01
6.281E-01
9.136E-01
1.199E-02
1.200E-02
4.040E+00
5.717E-01
5.723E-01
1.584E+00
4.823E+03
4.826E+03
1.665E+04
1.253E+01
1.254E+01
4.195E+01
1.668E+00
1.671E+00
4.581E+00
1.172E-02
1.172E-02
2.770E+00
4.751E+00
4.755E+00
1.594E+01
1.3 83E+01
1.3 84E+01
4.085E+01
8.178E-01
1.010E+00
1.477E+00
1.178E+00
1.336E+00
2.388E+00
3.632E-01
3.637E-01
1.164E+00
1.054E+01
1.055E+01
3.590E+01
1.419E+00
1.548E+00
2.284E+00
7.052E-01
7.065E-01
2.377E+00
1.412E+00
1.542E+00
1.860E+00
3.854E+00
3.859E+00
1.720E+01
3.057E+00
3.066E+00
1.682E+01
9.010E+00
9.102E+00
2.288E+01
2.485E+01
2.486E+01
8.345E+01
2.125E+00
2.125E+00
7.159E+00
2.863E-01
2.867E-01
6.990E+00
7.857E+01
7.869E+01
2.751E+02
3.388E+00
3.3 91E+00
1.137E+01
1.092E+00
1.095E+00
3.441E+00
3.887E+00
3.890E+00
1.3 02E+01
1.051E-01
1.053E-01
1.872E+00
2.294E-01
2.296E-01
2.185E+00
1.422E+00
1.423E+00
4.794E+00
3.814E+00
3.816E+00
9.806E+00
2 of 21)
4
8
7
6
5
2
4
9
7
0
0
6
5
8
1
6
8
9
7
8
4
9
5
7
3
0
5
5
2
6
6
0
3
4
3
1
0
4
Page
Page 315 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 1
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Sample description
257060 Gamma 160-17814-A-l-B
Spectrum Filename: C:\User\SPC\Det5\5_Gamma_20161261.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 7:46:20 AM
1800
1807
0.38 %
5
Detector system
Ge 5 SN/157
Calibration
Filename:
5 Soil TunaCan 90099 032612
5 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 7:35:48 PM
0.158 keV
0.250 keV/channel
3.911E-08 keV/channel^2
3/27/2012 5:20:37
165.85 keV
Quadratic
6 .466115E-01
( -4 .117504E
Quadratic
-2 . 462251E+01
( -9 . 664422E
PM
Uncertainty = 0.8 7
+ ( - 7 . 83 04 54E-01*Log(E) )
03 *Log(E)^2 )
Uncertainty = 1.43
+ ( 9 . 075211E+00*Log(E) )
01*Log(E)^2 )
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 37.62keV )
8000 ( 2000.81keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00*
1.0000E+00
Reg. Guide 4.16 Method
1.0000E+00)
(Page 3 of 21)
Page 316 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:17:14 AMPage 2
Spectrum name: 5_Gamma_2 0161261.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 7:46:00 AM
5_2 016-07-10_06 01.PBC
7/10/2016 6:01:50 AM
total peaks alloc. 24 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.1321
* * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq/Sampl
46 . 57
13 .
82.93
0 .60
1.790E-02
46 . 54
4 .250
PBC
-------
ORTEC g v - i
TestAmerica Inc
(3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 3
Spectrum name: 5_Gamma_2 0161261.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
238 . 70
157 .
10 . 98
0 . 84
2.319E-02
238 . 63
43 .300
8.685E+00
PB212
242.03
45 .
24 . 62
0 . 98
2.293E-02
242.00
7.430
1.481E+01
PB214
256.24
7 .
163.70
1. 00
2 .186E-02
256.24
7 . 000
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 4
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
964 .11
6 .
149.20
1.61
7.239E-03
964.11
14 .605
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
5
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Np-237
345 . 63
86 .49
486 .
-19 .
-0 . 011
165.42
0 . 825
EU-155
345.84
86 . 54
467 .
-19 .
-0.011
162 .21
0 . 825
Sn-126
347 .43
86 . 94
448 .
-19 .
-0.011
158 . 89
0 . 825
Sn-126
349.95
87 . 57
429 .
-16 .
-0.009
183 .45
0 . 826
Cd-109
351.83
88 . 04
428 .
-20 .
-0 . 011
148.53
0 . 826s
Nd-147
364 . 08
91.10
408 .
-10 .
-0.005
294 . 70
0 . 829
TH-234
370.05
92 . 59
93 .
28 .
0 . 016
52 . 58
0.83 ID
AC-228
373.09
93 .35
334 .
18 .
0 . 010
148 . 78
0.832s
Np-239
397.71
99 . 50
81.
7 .
0 . 004
231.90
0.838s
Gd-153
412.52
103.20
169 .
13 .
0 . 007
146.02
0.842s
Np-239
414.52
103.70
182 .
0 .
0 . 000
1000 . 00
0 . 842
EU-155
420.98
105.31
231.
3 .
0 . 002
735 . 50
0 . 844s
Np-239
424 .25
106.13
214 .
14 .
0 . 008
152 . 01
0 . 845s
EU-152
486.88
121.78
116 .
6 .
0 . 003
257.12
0 . 861
CO - 57
488 . 03
122.06
122 .
0 .
0 . 000
1000.00
0 . 861s
EU-154
492.18
123.10
120 .
-11.
-0.006
202 .41
0 . 862s
PA-2 3 4
524 . 99
131.29
271.
-18 .
-0.010
128 . 57
0.871s
HF-181
531. 91
133.02
290 .
-18 .
-0 . 010
132 .46
0.872s
CE-144
533.97
133.54
308 .
-18 .
-0 . 010
136 .41
0 . 873
HF-181
545.02
136 .30
327 .
-19 .
-0 . 010
139 . 89
0 . 876s
CO - 57
545.72
136.47
293 .
17 .
0 . 010
142 .38
0.876s
Tc-99m
561.88
140.51
229 .
-17 .
-0.010
125 . 98
0.880s
U-235
574.99
143.79
245 .
-18 .
-0 . 010
123.96
0 . 883
CE-141
581. 61
145.44
322 .
-20 .
-0.Oil
127.68
0.885s
U-235
653.42
163 .38
122 .
0 .
0 . 000
1000 . 00
0 . 903s
CE-13 9
663 .32
165 . 85
Ill.
0 .
0 . 000
1000.00
0.905s
Cf-251
706.34
176.60
70 .
9 .
0 . 005
168.75
0.916s
TH-229
774.03
193.51
53 .
-4 .
-0.002
303.72
0 . 933s
U-235
821.35
205.33
65 .
-6 .
-0.003
389.36
0.945s
TH-229
843.44
210.85
64 .
14 .
0 . 008
105 . 03
0.950s
PB-212
954.64
238 . 63
27 .
165 .
0 . 092
8 . 93
0.978D
PB-214
968.10
242.00
40 .
45 .
0 . 025
24 . 62
0.981D
EU-152
978.89
244 .69
365 .
-15 .
-0.009
178 .34
0.984s
TH-227
1025.11
256.24
41.
7 .
0 . 004
163.70
0.995s
Cd-113m
1054.97
263.70
59 .
6 .
0 . 004
175.59
1. 002
BI-210M
1063.50
265.83
84 .
-14 .
-0.008
99.46
1.005s
TL-208
1109.33
277.28
62 .
3 .
0 . 002
375.65
1. 016
1-131
1137.41
284 .30
40 .
12 .
0 . 006
105.96
1. 022s
PB-214
1181.48
295.31
24 .
75 .
0 . 041
15 . 96
0 . 988
PB-212
1201.48
300.31
24 .
9 .
0 . 005
100.36
1. 824s
PA-2 31
1200.53
300.07
277 .
-17 .
-0.009
141. 08
1. 038s
PA-233
1200.97
300.18
275 .
-17 .
-0 . 009
140.74
1. 038s
PA-2 31
1210.86
302.65
292 .
-17 .
-0.009
144.54
1. 040s
BA-133
1211.66
302.85
309 .
-17 .
-0.009
148.53
1. 040s
Ba-140
1219.66
304.85
326 .
-17 .
-0.009
152.17
1. 042s
BI-210M
1219.85
304.90
343 .
-17 .
-0.009
155.98
1. 042s
Ir-192
1234.03
308.44
242 .
14 .
0 . 008
163.90
1. 046s
PA-233
1248 .32
312.01
321.
-12 .
-0.007
205.21
1. 049s
(Page 7 of 21)
Page 320 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 6
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Ir-192
1266 .25
316.49
120 .
-16 .
-0 . 009
100.31
1. 053s
CR-51
1280 . 63
320.08
115 .
12 .
0 . 007
126 .32
1.057s
La-140
1315.35
328.76
40 .
4 .
0 . 002
328 .22
1.065s
Cf-249
1334.08
333 .44
33 .
2 .
0 . 001
541. 99
1. 070
AC-228
1354.53
338 . 55
16 .
58 .
0 . 032
19 .15
1.448s
Cs-136
1362 . 62
340.57
159 .
-12 .
-0.007
146.37
1.077s
EU-152
1377.49
344 .29
161.
-15 .
-0.008
126.02
1.080s
HF-181
1383 . 66
345 . 83
Ill.
11.
0 . 006
135.17
1.082s
PB-214
1407.97
351.90
28 .
144 .
0 . 080
11. 06
0 . 920
1-131
1458.32
364.48
15 .
17 .
0 . 010
47 . 81
1.099s
BA-133
1535.78
383 . 84
95 .
-12 .
-0.007
115 . 74
1.117
Cf-249
1552.22
387 . 95
107 .
-2 .
-0 . 001
859.56
1.121s
SN-113
1567.19
391.69
59 .
7 .
0 . 004
151.02
1.125
SB-125
1711.99
427.88
28 .
-2 .
-0.001
469.00
1.158s
AG-108M
1736.25
433.94
20 .
9 .
0 . 005
102 . 84
1.164s
pm-146
1816.05
453 . 88
12 .
7 .
0 . 004
104.00
1.182s
SB-125
1854.01
463 .37
57 .
-4 .
-0.002
251.74
1.191s
Ir-192
1872.79
468.06
55 .
7 .
0 . 004
150.39
1.195s
BE - 7
1910.94
477.59
57 .
8 .
0 . 005
132 .36
1.204s
La-140
1948.65
487 . 02
16 .
8 .
0 . 004
104.08
1.212s
RU-103
1988.80
497.05
20 .
-3 .
-0.002
297 . 52
1.221s
RH-106
2048.06
511.86
47 .
36 .
0 . 020
50 . 72
2 ,485s
Nd-147
2124.62
531.00
28 .
-6 .
-0.003
177 . 43
1.252s
Ba-140
2149.67
537.26
17 .
8 .
0 . 004
105.07
1.258
CS-134
2253.60
563.24
20 .
-3 .
-0.002
297.52
1.280s
CS-134
2277.94
569.32
16 .
3 .
0 . 002
197.20
1.286s
PA-2 3 4
2278.54
569.47
20 .
-1.
0 . 000
948 .68
1.286s
BI-207
2279.47
569.70
19 .
0 .
0 . 000
1000 . 00
1.286s
TL-208
2333 . 87
583 .30
7 .
63 .
0 . 035
15 . 71
1.170
SB-125
2402.69
600.50
185 .
-5 .
-0.003
363.58
1.313s
SB-124
2411.61
602.73
180 .
0 .
0 . 000
1000 . 00
1.315s
CS-134
2419.53
604.71
180 .
0 .
0 . 000
1000.00
1.317s
BI-214
2438.42
609.43
14 .
105 .
0 . 058
11. 92
0.811s
RU-103
2441. 89
610.30
180 .
0 .
0 . 000
1000 . 00
1.322s
AG-108M
2457.82
614.28
180 .
0 .
0 . 000
1000.00
1.325s
PM-144
2472.94
618 . 06
180 .
0 .
0 . 000
1000 . 00
1.328s
RH-106
2488 .37
621.92
198 .
-10 .
-0.006
194.95
1.332s
SB-125
2544.26
635 . 89
13 .
8 .
0 . 004
72 .16
1.344s
1-131
2548.61
636.97
29 .
2 .
0 . 001
344.84
1.345s
AG-110M
2631.76
657.76
26 .
9 .
0 . 005
82 . 76
1.362s
CS-137
2647.36
661. 66
42 .
-4 .
-0.002
224.00
1.366s
PM-144
2786.90
696.54
22 .
-9 .
-0.005
103 . 82
1.395s
NB-94
2811.25
702 . 63
13 .
1.
0 . 001
742.74
1.400s
SB-124
2891.88
722.79
50 .
-13 .
-0.007
81.68
1.417s
AG-108M
2892.48
722.94
63 .
-8 .
-0 . 005
142 . 64
1.417s
EU-154
2894.16
723 .36
71.
0 .
0 . 000
1000.00
1.418s
ZR-95
2897.53
724.20
72 .
-10 .
-0.005
126 .27
1.418s
BI-212
2909.41
727.17
81.
10 .
0 . 005
136 .40
1.421s
(Page 8 of 21)
Page 321 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
7
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
pm-146
2943 .61
735 . 72
13 .
-3 .
-0 . 002
378.74
1.428s
pm-146
2989.37
747.16
17 .
-4 .
-0.002
297.94
1.437s
ZR-95
3027.65
756.73
22 .
-6 .
-0.003
220.85
1.445s
AG-110M
3056.50
763.94
80 .
-20 .
-0.011
68 . 58
1.451s
NB-95
3063.89
765.79
99 .
-19 .
-0.010
77 . 90
1.453s
PA-234M
3066.38
766 .41
91.
15 .
0 . 008
92 . 63
1.453s
EU-152
3116.41
778.92
28 .
-12 .
-0.007
94 .44
1.463s
BI-212
3142.41
785.42
19 .
-3 .
-0 . 001
349.11
1.468s
CS-134
3184.19
795 . 87
14 .
0 .
0 . 000
1000 . 00
1.477s
CS-134
3208.53
801. 95
9 .
4 .
0 . 002
184 .30
1.482s
CO - 58
3243.82
810.78
38 .
2 .
0 . 001
469.67
1.489s
La-140
3263.80
815.77
40 .
0 .
0 . 000
1000 . 00
1.493s
Cs-136
3274.72
818.50
41.
-1.
-0.001
687.39
1.495s
MN-54
3340.10
834.85
19 .
-5 .
-0 . 003
172.74
1.508s
Co - 56
3387.78
846.77
9 .
7 .
0 . 004
104 . 64
1. 518s
TL-208
3442.95
860.56
9 .
8 .
0 . 004
93 . 64
1.529s
NB-94
3485 . 08
871.10
30 .
-4 .
-0.002
254.12
1.537s
EU-154
3493.61
873 .23
22 .
9 .
0 . 005
84 . 56
1.539s
PA-2 3 4
3522.80
880.53
31.
-3 .
-0.002
268 . 74
1. 544s
PA-2 3 4
3533.64
883 .24
34 .
0 .
0 . 000
1000.00
1.547s
AG-110M
3539.41
884 .68
34 .
0 .
0 . 000
1000.00
1.547s
Sc-46
3557.79
889.28
45 .
-9 .
-0.005
110.55
1.551s
y-88
3592.83
898.04
15 .
-7 .
-0 . 004
112 . 01
1.558s
AC-228
3645.15
911.12
1.
46 .
0 . 026
15 . 01
1.604
AG-110M
3750.60
937.49
9 .
1.
0 . 000
979 . 80
1.589s
PA-2 3 4
3784.70
946.02
14 .
5 .
0 . 003
164.92
1.595s
EU-152
3857.05
964.11
32 .
6 .
0 . 003
149.20
1.609
AC-228
3878.75
969.54
3 .
24 .
0 . 013
25 . 11
3 .183s
EU-154
3985.88
996 .33
30 .
-2 .
-0.001
527.05
1. 633s
PA-234M
4004.55
1001.00
32 .
0 .
0 . 000
1000.00
1. 636s
EU-154
4019.65
1004.77
55 .
-13 .
-0.007
86 . 85
1. 639s
Co - 56
4151.87
1037.84
10 .
2 .
0 . 001
408.26
1. 664s
Cs-136
4192.77
1048.07
18 .
5 .
0 . 003
128 . 06
1. 671s
RH-106
4201.93
1050.36
31.
-5 .
-0.003
163.71
1. 673s
BI-207
4255.11
1063.66
10 .
8 .
0 . 004
93 . 82
1. 682s
Ga-6 8
4310.04
1077.40
0 .
9 .
0 . 005
33 .33
1. 692s
FE-59
4397.41
1099.25
16 .
2 .
0 . 001
389.82
1. 708s
EU-152
4448.68
1112.07
89 .
-13 .
-0.007
103 . 81
1.717s
ZN-65
4462 . 56
1115.55
76 .
-9 .
-0 . 005
142 .28
1.720s
BI-214
4481.51
1120.29
6 .
32 .
0 . 018
20.65
1.723D
Sc-46
4482.57
1120.55
67 .
0 .
0 . 000
1000 . 00
1. 723s
Ta-182
4485.56
1121.30
24 .
6 .
0 . 003
123 .42
1. 724s
CO-6 0
4693.21
1173.24
6 .
13 .
0 . 007
48 . 70
1.760s
Ta-182
4756.42
1189.05
30 .
-10 .
-0.006
124 . 50
1.771s
Ta-182
4885 . 79
1221.41
5 .
6 .
0 . 003
93 .30
1. 793s
Co - 56
4953.23
1238.28
6 .
18 .
0 . 010
37 . 82
1. 804
EU-154
5098.19
1274.54
11.
0 .
0 . 000
1000 . 00
1. 828s
FE-59
5166 .35
1291.60
5 .
6 .
0 . 004
91. 70
1. 840s
(Page 9 of 21)
Page 322 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 8
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
CO-6 0
5329 . 85
1332.50
6 .
1.
0 . 001
397.16
1. 866s
AG-110M
5536.88
1384 .30
0 .
8 .
0 . 004
35.36
1.899s
K-40
5843.24
1460.95
4 .
137 .
0 . 076
8 . 77
2 .185
La-140
6383.73
1596.21
6 .
-4 .
-0.002
160.96
2 . 024s
SB-124
6762.39
1690.98
0 .
6 .
0 . 003
40 . 82
2 . 076s
BI-214
7056.06
1764 .49
27 .
1.
0 . 001
672.51
2.114s
Co - 56
7083.46
1771.35
14 .
7 .
0 . 004
79 . 73
2.117s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***^
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE-7 C 3.3 774E+00
NA-22 C 3.2367E-02
K-40 N 1.4012E+02
Sc-46 F -6 .4551E-01
477.60 3.377E+00 ?( 1.532E+01
1274.53 3.237E-02 %( 1.741E+00
1460.83 1.401E+02 (P 1.187E+01
889
1120
28-6
55 0
455E-01
000E+00
?( 2.436E+00
+ 3.558E+00
5.31E+01
1.32E+02 1.05E+01 G
9.50E+02
1.40E+03 9.99E+01 G
4.66E+11
8.77E+00 1.07E+01 G
8.3 8E+01
1.11E+02 1.00E+02 G
1.00E+03 1.00E+02 G
CR-51
MN-54
FE-59
Co - 56
3 . 7828E+00
-3 . 5111E-01
8 .1932E-01
1.2859E+00
320.08 3.783E+00 &( 1.617E+01
834 . 85-3.511E-01 ?(P 1.572E+00
1099
1291
846
1238
1037
1771
25 3
60 1
77 4
28 2
84 1
35 6
400E-01
446E+00
591E-01
596E+00
007E+00
083E+00
? (P 3.216E+00
?(P 3.066E+00
?( 1.167E+00
(P 2.010E+00
?(P 1.019E+01
? 1.641E+01
2.77E+01
1.26E+02 9.94E+00 G
3.12E+02
1.73E+02 1.00E+02 G
4.45E+01
3.90E+02 5.65E+01 G
9.17E+01 4.32E+01 G
7.73E+01
1.05E+02 9.99E+01 G
3.78E+01 6.61E+01 G
4.08E+02 1.41E+01 G
7.97E+01 1.55E+01 A
(Page 10 of 21)
Page 323 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 9
TestAmerica Inc
Nuclide Ave activity
CO-57 C 2.8776E-01
CO - 58
CO-6 0
ZN-65
NB-94
ZR-95
NB-95
RU-103
RH-106
AG-108M
AG-110M
1. 2567E-01
6 . 5304E-01
¦1. 5277E+00
6 . 0127E-02
-6 . 8951E-01
¦1.1979E+00
¦1.4548E-01
¦5.5415E+00
3 . 9154E-01
6.23 97E-01
Spectrum name: 5_Gamma_2 0161261.Anl
Energy Activity Code Peak MDA Comments
2.72E+02
122.06
0.000E+00
? (
9 . 817E-01
1.00E+03 8.
56E+01
G
136 .47
2.594E+00
? (
1. 240E+01
1.42E+02 1.
07E+01
G
7.09E+01
810.78
1.257E-01
? (P
2 . 101E+00
4.70E+02 9.
95E+01
G
1.93E+03
1332.50
1.381E-01
? (P
1.3 87E+00
3.97E+02 1.
00E+02
G
1173.24
1.168E+00
? (P
1.289E+00
4.87E+01 9.
99E+01
G
2.44E+02
1115.55
-1.528E+00
? (
7.426E+00
1.42E+02 5.
06E+01
G
7.41E+06
702 . 63
6.013E-02
& (
1.173E+00
7.43E+02 9.
79E+01
G
871.10
-2.491E-01
& P
1.978E+00
2.54E+02 9.
99E+01
G
6.40E+01
756.73
-6.895E-01
? (P
2.825E+00
2.21E+02 5.
45E+01
G
724 .20
-1.345E+00
+
5.7 84E+00
1.26E+02 4.
42E+01
G
6.40E+01
765.79
-1.198E+00
? (
3.109E+00
7.79E+01 9.
98E+01
G
3.93E+01
497.05
-1.455E-01
? (
1.142E+00
2.98E+02 9.
09E+01
G
610.30
0.000E+00
+
5.936E+01
1.00E+03 5.
75E+00
GJ
3.74E+02
621.92
-5.542E+00
? (
3.659E+01
1.95E+02 9.
93E+00
G
1050.36
-2.643E+01
+
1.515E+02
1.64E+02 1.
56E+00
G
511.86
8.207E+00
¦?
7.802E+00
5.07E+01 2.
00E+01
GJ
1.53E+05
433.94
3.915E-01
& (
1.025E+00
1.03E+02 9.
05E+01
G
722.94
-5.396E-01
+
2.638E+00
1.43E+02 9.
08E+01
G
614.28
0.000E+00
-
3.819E+00
1.00E+03 8.
98E+01
G
2.50E+02
884.68
0.000E+00
? (
2.936E+00
1.00E+03 7.
27E+01
G
657.76
5.576E-01
? (
1.558E+00
8.28E+01 9.
46E+01
G
937.49
1.454E-01
? (
3.697E+00
9.80E+02 3.
44E+01
G
1384 .30
3.426E+00
Sc. (
3.157E+00
3.54E+01 2.
43E+01
G
763.94
-5 . 537E+00
+
1.2 58E+01
6.86E+01 2.
23E+01
G
(Page 11 of 21)
Page 324 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 10
TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide Ave activity
SN-113 F 4.2075E-01
Energy
Activity Code Peak MDA Comments
1.15E+02
391.69 4.207E-01 &(P 2.182E+00 1.51E+02 6.40E+01 G
SB-124
5.0598E-01
602.73 0.000E+00 ?(
1690.98 1. 546E+00 ?(
722 . 79-7.268E+00 +
6.02E+01
3.437E+00 1.00E+03 9.83E+01 G
1.899E+00 4.08E+01 4.78E+01 G
1.991E+01 8.17E+01 1.08E+01 G
SB-125 I 8.4183E-01
1.01E+03
427 . 88-3.168E-01 &(P 3.621E+00 4.69E+02 2.96E+01 G
600 . 50-1.541E+00 + 1.912E+01 3.64E+02 1.79E+01 G
635.89 3.874E+00 ( 9.342E+00 7.22E+01 1.13E+01 G
463.37-1.721E+00 + 1.509E+01 2.52E+02 1.05E+01 G
1-131 I 1.0891E+00
364.48 7.223E-01 ?(
284.30 5.263E+00 &(
636.97 1.695E+00 ?(
8.02E+00
8.566E-01 4.78E+01 8.17E+01 G
1.457E+01 1.06E+02 6.14E+00 G
2.095E+01 3.45E+02 7.17E+00 G
Gd-153 F 3.5112E-01
97 . 50-5.177E-02 %(
103.20 9.055E-01 &(
2.42E+02
2.693E+00 1.50E+03 3.00E+01 G
4.468E+00 1.46E+02 2.18E+01 G
Ga-6 8 C 2.6787E+01
1077.40 2.679E+01 (
4.71E-02
2.194E+01 3.33E+01 3.30E+00 G
Tc-99m I -3 .2527E-01
140.51-3.253E-01 (
2.51E-01
1.376E+00 1.26E+02 8.93E+01 G
BA-133 F -4.4833E-02
356 . 00-4.483E-02 %(
302.85-2.703E+00 +
383 . 84-4.885E+00 &
80.99 8.188E-02 %
3 . 85E+03
3.636E+00 2.37E+03 6.20E+01 G
1.348E+01 1.49E+02 1.83E+01 G
1.913E+01 1.16E+02 8.94E+00 GA
2.874E+00 1.28E+03 3.41E+01 GA
CS-134 I 1.8783E-01
7 . 54E+02
604.71
0.000E+00
? (
3 .469E+00
1.00E+03
9.76E+01
G
795.87
0.000E+00
Sc. (
1. 539E+00
1.00E+03
8.55E+01
G
569.32
9.63 0E-01
? (
6 . 853E+00
1.97E+02
1.54E+01
G
801.95
2.775E+00
? (
1. 2 82E+01
1.84E+02
8.69E+00
G
563 .24
-1.758E+00
+
1.3 80E+01
2.98E+02
8.3 5E+00
G
CS-137 I -2.6381E-01
1.10E+04
661. 66-2.638E-01 ?(P 2.162E+00 2.24E+02 8.52E+01 G
(Page 12 of 21)
Page 325 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:17:14 AMPage 11
Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
Ba-140
1. 5466E+00
1.28E+01
537.26 1.547E+00 ?(P 4.198E+00 1.05E+02 2.44E+01 G
162 . 66-2.869E-01
8c
1. 549E+01
1.56E+03 6.22E+00
G
304 . 85-1.163E+01
8c
5 . 944E+01
1.52E+02 4.29E+00
G
La-140
I
1. 9305E-02
1.28E+01
1596.21-4.509E-01
? (
1. 697E+00
1.61E+02 9.54E+01
G
487.02 7.620E-01
? (
2 . 034E+00
1.04E+02 4.55E+01
G
328.76 5.644E-01
? (
4.973E+00
3.28E+02 2.03E+01
G
815.77 0.000E+00
-
9.222E+00
1.00E+03 2.33E+01
G
CE-141
I
-6 . 9450E-01
3.25E+01
145 . 44-6.945E-01
& (
2.970E+00
1.28E+02 4.82E+01
G
CE-144
I
-2 . 6535E+00
2.85E+02
133 . 54-2.653E+00
(
1.214E+01
1.36E+02 1.11E+01
G
PM-144
C
-5 . 1301E-01
3.63E+02
696 . 54-5.130E-01
? (p
1.441E+00
1.04E+02 9.90E+01
G
618.06 0.000E+00
+
3.481E+00
1.00E+03 9.91E+01
G
EU-152
F
-1.0511E-01
4.94E+03
344 . 29-1. 782E+00
& (
7.571E+00
1.26E+02 2.65E+01
G
1112.07-8.462E+00
+
2.964E+01
1.04E+02 1.36E+01
G
121.78 3 . 255E-01
+
2.869E+00
2.57E+02 2.86E+01
G
778.92-6.179E+00
+
1.357E+01
9.44E+01 1.29E+01
G
964.11 2.93 8E+00
? (
1.528E+01
1.49E+02 1.46E+01
G
244 . 69-4.938E+00
+
2.959E+01
1.78E+02 7.58E+00
G
1408.00 1. 675E-01
o.
"o
9.008E+00
2.23E+03 2.10E+01
GA
EU-154
I
4 . 9714E+00
3.14E+03
873.23 4.971E+00
? (P
1.422E+01
8.46E+01 1.23E+01
G
123.10-4.074E-01
- p
2.045E+00
2.02E+02 4.08E+01
G
1274.54 0 . 000E+00
-
5.010E+00
1.00E+03 3.52E+01
G
723.36 0.000E+00
Sc.
1.255E+01
1.00E+03 2.02E+01
G
1004.11-5.620E+00
-
1.642E+01
8.68E+01 1.80E+01
G
996.33-1.116E+00
-
2.117E+01
5.27E+02 1.06E+01
G
EU-155
I
2 . 1244E-01
1.81E+03
105.31 2 . 124E-01
? (P
5.326E+00
7.36E+02 2.12E+01
G
86 . 54-1.003E+00
+
5.448E+00
1.62E+02 3.07E+01
G
HF-181
F
3 . 6982E-01
4.24E+01
482 . 00-1.779E-02
%(
2.245E+00
3.59E+03 8.05E+01
G
133 .02-6.782E-01
&
3.014E+00
1.32E+02 4.33E+01
G
345.83 2.440E+00
? (
1.119E+01
1.35E+02 1.51E+01
G
136.30-5.088E+00
+
2.3 87E+01
1.40E+02 5.85E+00
G
(Page 13 of 21)
Page 326 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:17:14 AMPage 12
TestAmerica Inc
Nuclide Ave activity
Ta-182 F 1.7854E+00
Spectrum name: 5_Gamma_2 0161261.Anl
Energy Activity Code Peak MDA Comments
1121.30 1.495E+00 ?(
1221.41 2.160E+00 ?(
1189.05-5.650E+00 +
1.14E+02
6.415E+00 1.23E+02 3.49E+01 G
4.672E+00 9.33E+01 2.70E+01 G
1.595E+01 1.24E+02 1.62E+01 G
Hg-203
3 . 3492E-02
279.20 3.349E-02
4.66E+01
1.330E+00 1.13E+03 8.15E+01
G
TL-208
pm-146
N
3.7971E+00
1.1528E-02
583.02 3.735E+00 (
277.28 1. 290E+00 -
860.56 4.221E+00 & (
6.98E+02
9.136E-01 1.57E+01 8.45E+01
1.694E+01 3.76E+02 6.31E+00
9.519E+00 9.36E+01 1.24E+01
2.02E+03
747 . 16-8.078E-01 ?(P 4.040E+00 2.98E+02 3.40E+01
735 . 72-9.466E-01 + P 5.389E+00 3.79E+02 2.25E+01
453.88 4.401E-01 & ( 1.185E+00 1.04E+02 6.50E+01
y-
¦5.1039E-01
1.07E+02
898 . 04-5.104E-01 ?(P 1.584E+00 1.12E+02 9.37E+01 G
1836.06-4.150E-02 % P 9.809E-01 2.40E+03 9.92E+01 G
Cd-113m
Cd-109
2.7466E+03
¦8 .4343E+00
263.70 2.747E+03 & (
88 . 04-8.434E+00 ?(
5.33E+03
1.665E+04 1.76E+02 6.00E-03 K
4.53E+02
4.195E+01 1.49E+02 3.79E+00 G
Cf-251
9.8870E-01
176.60 9.887E-01 (
227.00-1.216E-01 %
3.28E+05
4.581E+00 1.69E+02 1.70E+01 G
1.340E+01 3.90E+03 6.30E+00 GA
Cf-249
2 . 3066E-03
387.95-9.296E-02 ?(
333.44 4.077E-01 & (
1.28E+05
2.770E+00 8.60E+02 6.60E+01 G
6.009E+00 5.42E+02 1.55E+01 G
Sn-126
-3 . 8447E+00
87.57-6.914E-01 +
64 .28-3.845E+00 (
86 . 94-3.399E+00 +
3.65E+07
4.257E+00 1.83E+02 3.75E+01 GA
1.594E+01 1.24E+02 9.70E+00 G
1.809E+01 1.59E+02 9.04E+00 GA
PB-210
N
4 . 3400E-01
8.14E+03
46.54 4.340E-01 %(P 4.085E+01 3.19E+03 4.25E+00
G
PB-212
N
9.1551E+00
238.63 9.155E+00
300.03 8 . 094E+00
6.98E+02
1.477E+00 8.93E+00 4.33E+01 G
2.248E+01 1.00E+02 3.28E+00 GA
(Page 14 of 21)
Page 327 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:17:14 AMPage 13
Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PB-214
N
1. 2137E+01
351.93 1. 271E+01
295.09 1.103E+01
242.00 1. 481E+01
5.84E+05
(P 2.388E+00 1.11E+01 3.76E+01 G
(P 3.814E+00 1.60E+01 1.93E+01 G
P 1.045E+01 2.46E+01 7.43E+00 GA
BI-207 C 3 . 8712E-01
569.70 0 . 000E+00 &(
1063.66 8 . 950E-01 ?(
1.18E+04
1.164E+00 1.00E+03 9.77E+01 G
1.952E+00 9.38E+01 7.45E+01 G
BI-212 N 7.7269E+00
6.98E+02
727.17 7.727E+00 ?(P 3.590E+01 1.36E+02 7.55E+00 G
785.42-1.346E+01 + 1.153E+02 3.49E+02 1.28E+00 GA
BI-214 N 1.1903E+01
609.31 1.190E+01
1120.29 1.869E+01 + P
1764.49 9 . 154E-01 - P
5.84E+05
(P 2.284E+00 1.19E+01 4.61E+01 G
8.052E+00 2.07E+01 1.51E+01 G
2.228E+01 6.73E+02 1.54E+01 G
BI-210M T -7 . 0906E-01
265 . 83-7.091E-01 ?(
304 . 90-1.783E+00 &
1.10E+09
2.3 77E+00 9.95E+01 5.00E+01 G
9.335E+00 1.56E+02 2.80E+01 G
AC-228 N 1.2118E+01
911.07 1. 165E+01
968.97 1.057E+01
338.32 1.550E+01
93.35 4.973E+00
2.10E+03
(P 1.860E+00 1.50E+01 2.90E+01 G
(P 4.7 90E+00 2.51E+01 1.75E+01 G
( 5.663E+00 1.92E+01 1.20E+01 G
2.483E+01 1.49E+02 5.56E+00 XA
TH-227 N 3.6268E+00
7.95E+03
50.14 4.429E+00 ?(P 1.720E+01 1.36E+02 8.00E+00 G
256.24 2.710E+00 ?(P 1.175E+01 1.64E+02 7.00E+00 G
TH-229 N 2.9102E+00
193.51-1.984E+00 ?(
2.68E+06
1.682E+01 3.04E+02 4.40E+00 G
210.85 1.011E+01 ?(P 2.887E+01 1.05E+02 2.99E+00 G
TH-234 N 2.4674E+01
63.29 2 . 467E+01
92.59 7 . 920E+00
1.63E+12
(P 2.288E+01 3.65E+01 3.81E+00 G
P 1.346E+01 5.26E+01 5.58E+00 G
PA-231 N -1.7189E+01
302.65-1.719E+01 ?(
300.07-1.994E+01 +
1.20E+07
8.345E+01 1.45E+02 2.88E+00 G
9.448E+01 1.41E+02 2.46E+00 G
PA-233 C -1.03 53E+00
312 . 01-1.035E+00 &(
300 .18-7.912E+00 +
7.82E+08
7.159E+00 2.05E+02 3.60E+01 G
3.741E+01 1.41E+02 6.20E+00 G
(Page 15 of 21)
Page 328 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:17:14 AMPage 14
Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PA-2 3 4
N
2.7385E-01
131.29-1.620E+00 ?(
946.02 2.818E+00 ?(
569.47-4.015E-01 &
883.24 0.000E+00 -
880 . 53-3.556E+00 +
1.63E+12
6.990E+00 1.29E+02 1.80E+01 G
1.136E+01 1.65E+02 1.34E+01 G
1.408E+01 9.49E+02 8.20E+00 G
2.219E+01 1.00E+03 9.60E+00 G
3.397E+01 2.69E+02 6.00E+00 GA
PA-234M N
8 .4823E+01
1001.00 0.000E+00 ?(
766 .41 3 . 263E+02 ?(
1.63E+12
2.7 51E+02 1.00E+03 8.37E-01 G
1.015E+03 9.26E+01 2.94E-01 G
U-235
N
-2 . 7331E+00
143 . 79-2.733E+00 (
205. 33-2.356E+00 + P
163.38 0.000E+00 +
2.57E+11
1.13 7E+01 1.24E+02 1.10E+01 G
1.696E+01 3.89E+02 5.01E+00 G
1.910E+01 1.00E+03 5.08E+00 G
AM-2 41
Np-237
¦1.4896E+00
-2 . 3501E+00
59 . 54-1.490E+00 ?(P 3.441E+00
86.49-2.350E+00 ?( 1.302E+01
1.58E+05
7.33E+01 3.59E+01 G
2.14E+06
1.65E+02 1.31E+01 G
Ir-192
1.2915E-01
316.49-5.555E-01 ?( 1.872E+00
468.06 5.806E-01 ?( 3.007E+00
308.44 1.270E+00 & ( 7.019E+00
7.40E+01
1.00E+02 8.70E+01 G
1.50E+02 5.18E+01 G
1.64E+02 3.18E+01 G
Cs-136
1. 7912E-01
818.50-8.919E-02 ?( 2.185E+00
1048.07 5.145E-01 & ( 2.313E+00
340 . 57-8.520E-01 + 4.217E+00
1.30E+01
6.87E+02 1.00E+02 G
1.28E+02 8.00E+01 G
1.46E+02 4.69E+01 G
Np-239
9 . 3521E-01
103.70 0.000E+00 & 4.201E+00
106.13 9.352E-01 ( 4.794E+00
99.50 7 . 218E-01 & 4.604E+00
2.36E+00
1.00E+03 2.40E+01 X
1.52E+02 2.27E+01 G
2.32E+02 1.50E+01 X
Nd-147
-2 .1498E+00
531. 00-2.150E+00 ?( 9.806E+00
91.10-5.455E-01 + 5.418E+00
( - This peak used in the nuclide activity average.
Peak is too wide, but only one peak in library.
Peak is part of a multiplet and this area went
negative during deconvolution.
Peak is too narrow.
1.11E+01
1.77E+02 1.30E+01 G
2.95E+02 2.83E+01 G
(Page 16 of 21)
Page 329 of 551
-------
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TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
TH-227
50 . 14
102 .
13 .
0 . 007
135 . 53
4.429E+00
AM-2 41
59 . 54
132 .
-24 .
-0 . 014
73 .32
-1.490E+00
Sn-126
64 .28
252 .
-19 .
-0.010
123.56
-3.845E+00
Np-237
86 .49
486 .
-19 .
-0.011
165.42
-2.3 50E+00
EU-155
86 . 54
467 .
-19 .
-0.011
162.21
-1.003E+00
Sn-126
86 . 94
448 .
-19 .
-0.011
158 . 89
-3.3 99E+00
Sn-126
87 . 57
429 .
-16 .
-0.009
183 .45
-6.914E-01
Cd-109
o
00
00
428 .
-20 .
-0.011
148.53
-8.434E+00
Nd-147
91.10
408 .
-10 .
-0.005
294.70
-5.455E-01
Np-239
99 . 50
81.
7 .
0 . 004
231.90
7.218E-01
Gd-153
103.20
169 .
13 .
0 . 007
146.02
9.055E-01
EU-155
105.31
231.
3 .
0 . 002
735.50
2.124E-01
Np-239
106.13
214 .
14 .
0 . 008
152.01
9.352E-01
EU-152
121.78
116 .
6 .
0 . 003
257.12
3.255E-01
EU-154
123.10
120 .
-11.
-0.006
202.41
-4.074E-01
PA-2 3 4
131.29
271.
-18 .
-0.010
128.57
-1.620E+00
HF-181
133.02
290 .
-18 .
-0.010
132 .46
-6.782E-01
CE-144
133.54
308 .
-18 .
-0.010
136 .41
-2.653E+00
HF-181
136.30
327 .
-19 .
-0.010
139 . 89
-5.088E+00
CO - 57
136.47
293 .
17 .
0 . 010
142 .38
2.594E+00
Tc-99m
140.51
229 .
-17 .
-0.010
125 . 98
-3 . 253E-01
U-235
143.79
245 .
-18 .
-0.010
123.96
-2 . 733E+00
CE-141
145.44
322 .
-20 .
-0.Oil
127.68
-6 . 945E-01
(Page 17 of 21)
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TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
Cf-251
176 .60
70
9 .
0 . 005
168.75
9.887E-01
TH-229
193 . 51
53
-4 .
-0 . 002
303 . 72
-1.984E+00
U-235
205.33
65
-6 .
-0.003
389.36
-2.3 56E+00
P
TH-229
210.85
64
14 .
0 . 008
105 . 03
1.011E+01
P
EU-152
244.69
365
-15 .
-0.009
178 .34
-4 . 938E+00
TH-227
256.24
41
7 .
0 . 004
163.70
2.710E+00
P
Cd-113m
263.70
59
6 .
0 . 004
175.59
2.747E+03
BI-210M
265 . 83
84
-14 .
-0.008
99.46
-7.091E-01
PA-2 31
300 . 07
277
-17 .
-0.009
141. 08
-1.994E+01
PA-233
300 .18
275
-17 .
-0.009
140.74
-7.912E+00
PA-2 31
302.65
292
-17 .
-0.009
144.54
-1.719E+01
BA-133
302.85
309
-17 .
-0.009
148.53
-2.703E+00
Ba-140
304.85
326
-17 .
-0.009
152.17
-1.163E+01
BI-210M
304.90
343
-17 .
-0.009
155.98
-1.783E+00
Ir-192
308.44
242
14 .
0 . 008
163.90
1.270E+00
PA-233
312.01
321
-12 .
-0.007
205.21
-1.035E+00
Ir-192
316.49
120
-16 .
-0.009
100.31
-5.555E-01
CR-51
320 . 08
115
12 .
0 . 007
126 .32
3.783E+00
La-140
328.76
40
4 .
0 . 002
328 .22
5.644E-01
Cf-249
333.44
33
2 .
0 . 001
541.99
4.077E-01
Cs-136
340 . 57
159
-12 .
-0.007
146 .37
-8.520E-01
EU-152
344 .29
161
-15 .
-0.008
126.02
-1.782E+00
HF-181
345.83
111
11.
0 . 006
135.17
2.440E+00
BA-133
383 . 84
95
-12 .
-0.007
115.74
-4.885E+00
Cf-249
387 . 95
107
-2 .
-0.001
859.56
-9.296E-02
SN-113
391.69
59
7 .
0 . 004
151.02
4.207E-01
P
SB-125
427 . 88
28
-2 .
-0.001
469 . 00
-3.168E-01
P
AG-108M
433.94
20
9 .
0 . 005
102 . 84
3.915E-01
pm-146
453 . 88
12
7 .
0 . 004
104.00
4.401E-01
SB-125
463 .37
57
-4 .
-0 . 002
251. 74
-1.721E+00
Ir-192
468.06
55
7 .
0 . 004
150.39
5.806E-01
La-140
487 . 02
16
8 .
0 . 004
104.08
7.620E-01
RU-103
497.05
20
-3 .
-0 . 002
297.52
-1.455E-01
RH-106
511. 86
47
36 .
0 . 020
50 . 72
8.207E+00
Nd-147
531.00
28
-6 .
-0 . 003
177.43
-2.150E+00
Ba-140
537.26
17
8 .
0 . 004
105.07
1.547E+00
P
CS-134
563.24
20
-3 .
-0 . 002
297.52
-1.758E+00
CS-134
569.32
16
3 .
0 . 002
197.20
9.63 0E-01
PA-2 3 4
569.47
20
-1.
0 . 000
948 .68
-4.015E-01
SB-125
600 . 50
185
-5 .
-0 . 003
363 . 58
-1.541E+00
RH-106
621. 92
198
-10 .
-0.006
194.95
-5.542E+00
SB-125
635 . 89
13
8 .
0 . 004
72 .16
3.874E+00
AG-110M
657.76
26
9 .
0 . 005
82 . 76
5.576E-01
CS-137
661. 66
42
-4 .
-0 . 002
224.00
-2.638E-01
P
PM-144
696 . 54
22
-9 .
-0.005
103 . 82
-5.13 0E-01
P
NB-94
702 . 63
13
1.
0 . 001
742.74
6.013E-02
SB-124
722.79
50
-13 .
-0.007
81.68
-7.268E+00
AG-108M
722.94
63
-8 .
-0.005
142 . 64
-5.396E-01
(Page 18 of 21)
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TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
ZR-95
724 .20
72
-10 .
-0.005
126.27
-1.345E+00
BI-212
727.17
81
10 .
0 . 005
136 .40
7 . 727E+00 P
pm-146
735 . 72
13
-3 .
-0 . 002
378 . 74
-9.466E-01 P
pm-146
747 . 16
17
-4 .
-0.002
297 . 94
-8.078E-01 P
ZR-95
756.73
22
-6 .
-0.003
220 . 85
-6.895E-01 P
AG-110M
763.94
80
-20 .
-0.011
68 . 58
-5.537E+00
NB-95
765 . 79
99
-19 .
-0.010
77 . 90
-1.198E+00
PA-234M
766.41
91
15 .
0 . 008
92 . 63
3.263E+02
EU-152
778.92
28
-12 .
-0.007
94 . 44
-6.179E+00
BI-212
785 . 42
19
-3 .
-0.001
349 .11
-1.346E+01
CS-134
801.95
9
4 .
0 . 002
184 .30
2.775E+00
CO - 58
810.78
38
2 .
0 . 001
469 . 67
1.257E-01 P
Cs-136
818.50
41
-1.
-0.001
687.39
-8.919E-02
MN-54
834.85
19
-5 .
-0 . 003
172.74
-3.511E-01 P
NB-94
871.10
30
-4 .
-0.002
254.12
-2.491E-01 P
EU-154
873 .23
22
9 .
0 . 005
84 . 56
4.971E+00 P
PA-2 3 4
880.53
31
-3 .
-0 . 002
268 . 74
-3.556E+00
Sc-46
889.28
45
-9 .
-0.005
110 . 55
-6.455E-01
y-88
898.04
15
-7 .
-0.004
112 . 01
- 5.104E-01 P
AG-110M
937.49
9
1.
0 . 000
979 . 80
1.454E-01
PA-2 3 4
946.02
14
5 .
0 . 003
164.92
2.818E+00
EU-152
964.11
32
6 .
0 . 003
149.20
2.938E+00
EU-154
996.33
30
-2 .
-0.001
527.05
-1.116E+00
EU-154
1004.77
55
-13 .
-0.007
86 . 85
-5.620E+00
Cs-136
1048.07
18
5 .
0 . 003
128 . 06
5.145E-01
RH-106
1050.36
31
-5 .
-0 . 003
163.71
-2.643E+01
BI-207
1063.66
10
8 .
0 . 004
93 . 82
8.950E-01
FE-59
1099.25
16
2 .
0 . 001
389.82
3.400E-01 P
EU-152
1112.07
89
-13 .
-0.007
103 . 81
-8.462E+00
ZN-65
1115.55
76
-9 .
-0.005
142 .28
-1.528E+00
CO-6 0
1173.24
6
13 .
0 . 007
48 . 70
1.168E+00 P
FE-59
1291.60
5
6 .
0 . 004
91. 70
1.446E+00 P
CO-6 0
1332.50
6
1.
0 . 001
397.16
1.381E-01 P
AG-110M
1384.30
0
8 .
0 . 004
35.36
3.426E+00
La-140
1596.21
6
-4 .
-0 . 002
160 . 96
-4.509E-01
SB-124
1690.98
0
6 .
0 . 003
40 . 82
1.546E+00
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE-7 #A 3.3 774E+00
NA-22 #A 3.2367E-02
K-40 1.4012E+02
Sc-46 #A -6.4551E-01
3.3774E+00
3 . 2367E-02
1. 4012E+02
-6 . 4551E-01
1. 324E+02'
1. 3 96E+03'
8.769E+00!
1.106E+02'
1. 53E+01
1. 74E+00
1.19E+01
2.44E+00
(Page 19 of 21)
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-------
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TestAmerica Inc Spectrum name: 5_Gamma_2 0161261.Anl
CR-51
#A
3 . 7828E+00
3 . 7828E+00
1.263E+02 %
1.62E+01
MN-54
#A
-3 . 5111E-01
-3 . 5111E-01
1.72 7E+02 %
1.57E+00
FE-59
#A
8 .1932E-01
8 .1932E-01
9.170E+01%
3.22E+00
Co - 56
C
1.2859E+00
1.2859E+00
3.782E+01%
1.17E+00
CO - 57
#A
2.8776E-01
2.8776E-01
1.424E+02 %
9.82E-01
CO - 58
#A
1.2567E-01
1.2567E-01
4.697E+02%
2.10E+00
CO-6 0
#A
6 . 5304E-01
6.5304E-01
4.870E+01%
1.39E+00
ZN-65
#A
-1. 5277E+00
-1.5277E+00
1.423E+02 %
7.43E+00
NB-94
#A
6 . 0127E-02
6.0127E-02
7.42 7E+02 %
1.17E+00
ZR-95
#A
-6.8951E-01
-6.8951E-01
2.208E+02%
2.83E+00
NB-95
#A
-1.1979E+00
-1.1979E+00
7.790E+01%
3.11E+00
RU-103
#A
-1.4548E-01
-1.4548E-01
2.975E+02%
1.14E+00
RH-106
#A
-5.5415E+00
-5.5415E+00
1.950E+02 %
3.66E+01
AG-108M#A
3 . 9154E-01
3.9154E-01
1.02 8E+02 %
1.02E+00
AG-110M#A
6.23 97E-01
6.23 97E-01
3.536E+01%
2.94E+00
SN-113
#A
4.2075E-01
4.2075E-01
1.510E+02 %
2.18E+00
SB-124
#A
5.0598E-01
5.0598E-01
4.082E+01%
3.44E+00
SB-125
#A
8.4183E-01
8.4183E-01
7.216E+01%
3.62E+00
1-131
#
1.0891E+00
1.0891E+00
4.781E+01%
8.57E-01
Gd-153
#A
3.5112E-01
3.5112E-01
1.460E+02%
2.69E+00
Ga-6 8
#
2.6696E+01
2.6787E+01
3.333E+01%
2.19E+01
Tc-99m
#A
-3.2507E-01
-3.2527E-01
1.260E+02%
1.38E+00
BA-133
#A
-4.4833E-02
-4.4833E-02
2.36 5E+03 %
3.64E+00
CS-134
#A
1.8783E-01
1.8783E-01
1.843E+02 %
3.47E+00
CS-137
#A
-2.6381E-01
-2.6381E-01
2.24 0E+02 %
2.16E+00
CE-139
#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.15E+00
Ba-140
#A
1.5465E+00
1.5466E+00
1. 051E+02%
4.20E+00
La-140
#A
1. 9305E-02
1.9305E-02
1.041E+02 %
1.70E+00
CE-141
#A
-6 . 9450E-01
-6.9450E-01
1.277E+02%
2.97E+00
CE-144
#A
-2 . 6535E+00
-2.6535E+00
1.3 64E+02 %
1.21E+01
PM-144
#A
-5 . 1301E-01
-5.1301E-01
1.03 8E+02 %
1.44E+00
EU-152
#A
-1.0511E-01
-1.0511E-01
9.765E+01%
7.57E+00
EU-154
#A
4.9714E+00
4.9714E+00
8.456E+01%
1.42E+01
EU-155
#A
2 . 1244E-01
2.1244E-01
7.3 55E+02 %
5.33E+00
HF-181
#A
3 . 6982E-01
3.6982E-01
1.3 52E+02 %
2.25E+00
Ta-182
#A
1. 7854E+00
1.7854E+00
7.736E+01%
6.42E+00
Hg-203
#A
3 . 3492E-02
3.3492E-02
1.12 7E+03 %
1.33E+00
TL-208
3.7971E+00
3.7971E+00
1.571E+01%
9.14E-01
pm-146
#A
1.1528E-02
1.1528E-02
1.04 0E+02 %
4.04E+00
y-88
#A
-5 . 1039E-01
-5.1039E-01
1.12 0E+02 %
1.58E+00
Cd-113m#A
2 . 7466E+03
2.7466E+03
1.756E+02 %
1.67E+04
Cd-109
#A
-8 .4343E+00
-8.4343E+00
1.485E+02%
4.20E+01
Cf-251
#A
9.8870E-01
9.8870E-01
1.688E+02%
4.58E+00
Cf-249
#A
2.3 066E-03
2.3 066E-03
5.081E+02%
2.77E+00
Sn-126
#A
-3 . 8447E+00
-3.8447E+00
1.23 6E+02 %
1.59E+01
PB-210
#A
4 .3400E-01
4.3400E-01
3.188E+03 %
4.09E+01
PB-212
#
9.1551E+00
9.1551E+00
8.932E+00%
1.48E+00
PB-214
1.2137E+01
1.2137E+01
9.708E+00%
2.3 9E+00
BI-207
#A
3 . 8712E-01
3.8712E-01
9.382E+01%
1.16E+00
(Page 2 0 of 21)
Page 333 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 8:
17:14 AMPage 19
TestAmerica
Inc
Spectrum
name: 5 Gamma
20161261.Anl
BI-212
#A
7 . 7269E+00
7.7269E+00
1.3 64E+02 %
3.59E+01
BI-214
1.1903E+01
1.1903E+01
1.192E+01%
2.28E+00
BI-210M#A
-7.0906E-01
-7.0906E-01
9.946E+01%
2.3 8E+00
AC-228
1. 2118E+01
1. 2118E+01
1.166E+01%
1.86E+00
TH-227
#A
3.6268E+00
3.6268E+00
1.063E+02 %
1.72E+01
TH-229
#A
2.9102E+00
2.9102E+00
1.050E+02 %
1.68E+01
TH-234
#
2 . 4674E+01
2.4674E+01
3 . 652E+01%
2.29E+01
PA-2 31
#A
-1.7189E+01
-1.7189E+01
1.44 5E+02 %
8.3 5E+01
PA-233
#A
-1.03 53E+00
-1.03 53E+00
2.052E+02 %
7.16E+00
PA-2 3 4
#A
2.7385E-01
2.7385E-01
1.046E+02 %
6.99E+00
PA-234M#A
8 .4823E+01
8.4823E+01
9.263E+01%
2.75E+02
U-235
#A
-2 . 7331E+00
-2.7331E+00
1.24 0E+02 %
1.14E+01
AM-2 41
#A
-1.4896E+00
-1.4896E+00
7 . 332E+01%
3.44E+00
Np-237
#A
-2 . 3501E+00
-2.3 501E+00
1.654E+02%
1.30E+01
Ir-192
#A
1. 2915E-01
1. 2915E-01
8.134E+01%
1.87E+00
Cs-136
#A
1.7911E-01
1. 7912E-01
1.281E+02 %
2.19E+00
Np-239
#A
9.3 515E-01
9.3521E-01
1.52 0E+02 %
4.79E+00
Nd-147
#A
-2 . 1498E+00
-2.1498E+00
1.774E+02 %
9.81E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.8 keV) 2.139E+02 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.8 keV) 2.1390179E+02 Bq/Sample
(Page 21 of 21)
Page 334 of 551
-------
257060_Gamma_160-17814-A-1 -B. 5_Gamma_20161261 .spc.
1.0e4n
1.0e3-
500 1000 1500 2000 2500 3000 3500 4000 4500 5000 5500 6000 6500 7000 7500 8000
Channels
-------
Test America St. Louis Spectrum ID: 7_Gamma_20161687
Sample Description: 257060_Gamma_160-17814-A-l-C DU
Detector: Detector # 7
Batch ID: 257060
Work Order Number: Gamma
Lot Number: 160-17814-A-l-C DU
Decay to Time: 7/11/2016 08:47 Live Time: 1800 sec
Acquisition Time: 7/11/2016 08:47:27 Real Time: 1832 sec
Analysis Time: 7/11/2016 09:18 Dead Time: 1.73 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
7_Soil_TunaCan.Clb
7_TunaCan_90099_032 712
3/16/2012 11:45
2/23/2012 08:40
Client_Long_Revll.lib
7 2016-07-10 0612.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
-3 . 928E+00
105.3
4 . 135E+00
4.140E+00
1.3 92E+01
NA-22
4 .252E-01
66 .4
2 . 822E-01
2.83 0E-01
9.266E-01
K-40
1.546E+02
7.2
1.120E+01
1.3 71E+01
1.074E+01
Sc-46
-4 . 834E-01
105 . 0
5.074E-01
5.080E-01
1.725E+00
CR-51
0.000E+00
1.#INF
7.964E-01
7.964E-01
1.910E+01
MN-54
-1.924E-02
3509.6
6.753E-01
6.753E-01
1.157E+00
FE-59
1. 038E-01
914 . 7
9.495E-01
9.495E-01
2.216E+00
Co - 56
2 . 461E-01
83 . 8
2.063E-01
2.067E-01
1.170E+00
CO - 57
1.107E-01
121.2
1.341E-01
1.342E-01
8.414E-01
CO - 58
-6.068E-01
84 . 1
5.104E-01
5.113E-01
1.713E+00
CO-6 0
4.426E-01
96 . 7
4.280E-01
4.286E-01
9.647E-01
ZN-65
7.521E-01
160 .1
1.204E+00
1.205E+00
4.164E+00
NB-94
-6.581E-01
91. 7
6.034E-01
6.044E-01
1.385E+00
ZR-95
-4.107E-01
196 . 9
8.089E-01
8.092E-01
1.942E+00
NB-95
6.451E-01
88.2
5.692E-01
5.701E-01
1.909E+00
RU-103
-1.062E-02
3377.1
3.585E-01
3.585E-01
9.037E-01
RH-106
-5.536E+00
156 .2
8.649E+00
8.654E+00
2.908E+01
AG-108M
3.038E-01
69.3
2.106E-01
2.111E-01
5.415E-01
AG-110M
3.484E-01
134 . 9
4.701E-01
4.705E-01
1.644E+00
SN-113
-3.247E-01
222 .2
7.215E-01
7.217E-01
1.742E+00
SB-124
-1.864E-01
51. 0
9.515E-02
9.564E-02
3.103E+00
SB-125
1.017E+00
94 . 5
9.611E-01
9.625E-01
2.763E+00
1-131
7.357E-01
51. 7
3.803E-01
3.822E-01
7.411E-01
Gd-153
-4.115E-01
162 . 7
6.698E-01
6.702E-01
1.817E+00
Ga-6 8
6 . 804E+00
229.3
1.560E+01
1.561E+01
3.660E+01
Tc-99m
-1.562E-01
180 . 9
2.825E-01
2.827E-01
9.526E-01
BA-133
-3 . 727E-01
224 . 6
8.3 71E-01
8.3 73E-01
2.827E+00
CS-134
-3 . 250E-01
112 . 7
3.664E-01
3.668E-01
3.058E+00
CS-137
-3 .108E-01
205 . 7
6.3 92E-01
6.3 94E-01
1.465E+00
CE-139
-6 . 762E-02
382 .3
2.585E-01
2.586E-01
8.842E-01
Ba-140
6 .333E-01
109 . 6
6.939E-01
6.947E-01
3.379E+00
La-140
-4 . 025E-01
77 . 8
3.133E-01
3.140E-01
1.943E+00
CE-141
3.886E-01
163 . 5
6.3 54E-01
6.3 57E-01
2.131E+00
(Page 1 of 21)
Page 336 of 551
-------
CE-144
0.000E+00
1.#INF
5.027E-01
5.027E-01
7.388E+00
PM-144
6 .299E-02
160 .1
1.008E-01
1.009E-01
1.232E+00
EU-152
6 .391E-01
89 . 6
5.725E-01
5.734E-01
5.278E+00
EU-154
1.481E+00
81. 8
1.211E+00
1.213E+00
9.361E+00
EU-155
7 . 894E-01
108 .4
8.556E-01
8.567E-01
2.872E+00
HF-181
3.500E-01
113 . 8
3.985E-01
3.989E-01
1.3 56E+00
Ta-182
8 . 091E-02
86 .3
6.981E-02
6.993E-02
7.212E+00
Hg-203
2 . 821E-01
96 .4
2.720E-01
2.725E-01
9.171E-01
TL-208
2 . 521E+00
15 . 9
4.016E-01
4.224E-01
7.433E-01
pm-146
1.095E+00
66 .2
7.254E-01
7.276E-01
2.067E+00
y-88
1.565E-01
289 . 6
4.532E-01
4.533E-01
1.083E+00
Cd-113m
3.595E+03
93 . 6
3.366E+03
3.3 74E+03
1.135E+04
Cd-109
0.000E+00
1.#INF
9.450E+00
9.450E+00
3.189E+01
Cf-251
-1.551E+00
107 . 7
1.671E+00
1.676E+00
4.270E+00
Cf-249
2 . 379E-01
187 . 6
4.464E-01
4.466E-01
1.535E+00
Sn-126
1.383E+00
248 . 5
3.436E+00
3.43 7E+00
9.3 05E+00
PB-210
5 . 913E-01
1807 . 7
1.069E+01
1.069E+01
3.646E+01
PB-212
9.051E+00
7 . 9
7.162E-01
9.251E-01
1.524E+00
PB-214
1.178E+01
8 . 0
9.451E-01
1.126E+00
1.714E+00
BI-207
2 . 765E-01
96 .1
2.657E-01
2.661E-01
9.703E-01
BI-212
4.890E+00
85.4
4.177E+00
4.185E+00
1.414E+01
BI-214
1.279E+01
8 . 5
1.085E+00
1.272E+00
1.111E+00
BI-210M
3 . 344E-01
128 . 0
4.279E-01
4.284E-01
1.456E+00
AC-228
8.685E+00
14 . 0
1.214E+00
1.292E+00
2.089E+00
TH -7.7.1
-4.459E+00
121. 1
5.401E+00
5.406E+00
1.454E+01
TH-229
1. 677E+00
276 . 6
4.640E+00
4.642E+00
1.282E+01
TH-234
-2 . 949E-01
2330.7
6.874E+00
6.874E+00
2.3 55E+01
PA-2 31
-1.070E+01
165 . 0
1.765E+01
1.766E+01
5.929E+01
PA-233
0 . 000E+00
1.#INF
3.100E-01
3.100E-01
5.159E+00
PA-2 3 4
2.826E-01
79 . 4
2.243E-01
2.247E-01
4.315E+00
PA-234M
-9 . 082E+01
56 .3
5.115E+01
5.135E+01
2.364E+02
U-235
-2 . 034E+00
87 . 4
1.778E+00
1.781E+00
1.056E+01
AM-2 41
8 .293E-01
112 .2
9.301E-01
9 . 3HE-01
2.500E+00
Np-237
0.000E+00
1.#INF
2.982E+00
2 . 982E+00
9.982E+00
Ir-192
2.145E-01
101.2
2.170E-01
2 . 173E-01
2.160E+00
Cs-136
4 . 423E-01
126 .3
5.585E-01
5.591E-01
1.903E+00
Np-239
-8 . 375E-01
111. 9
9.371E-01
9.384E-01
3.141E+00
Nd-147
-1.189E-01
192 . 1
2.284E-01
2.285E-01
8.23 0E+00
Total 3 . 824E+03
Analyst: Amanda Dick
(Page 2 of 21)
Page 337 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 1
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
Sample description
257060 Gamma 160-17814-A-l-C DU
Spectrum Filename: C:\User\SPC\Det7\7_Gamma_20161687.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 8:47:27 AM
1800
1832
1.73 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
7 TunaCan 90099 032712
7 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/23/2012 8:40:56 AM
0.117 keV
0.250 keV/channel
3.508E-09 keV/channel^2
3/16/2012 11:45:14 AM
165.85 keV
Quadratic
6 . 716580E-01
( -2 . 065917E
Quadratic
-2 . 689695E+01
Uncertainty = 0.8 7
+ (-6 .166540E-01*Log(E) )
02*Log(E)^2 )
Uncertainty = 1.4 8
+ ( 1. 019544E+01*Log(E) )
( -1.081671E+00*Log(E) 2
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 3 7.61keV )
8000 ( 2000.13keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00*
1.0000E+00
Reg. Guide 4.16 Method
1.0000E+00)
(Page 3 of 21)
Page 338 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:18:15 AMPage 2
Spectrum name: 7_Gamma_20161687.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 8:47:00 AM
7_2 016-07-10_0612.PBC
7/10/2016 6:12:03 AM
total peaks alloc. 20 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.1722
* * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq/Sampl
59 . 54
20 .
. 112.15
0 . 85
3.701E-02
59 . 54
35.900
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 3
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
242.06
51.
26 . 94
1. 04
3.560E-02
242.00
7.430
1. 067E+01
PB214
244 .69
17 .
185.43
1. 05
3.526E-02
244.69
7 . 580
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 4
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
871.10
8 .
70 .18
1. 64
1.168E-02
871.10
99 . 890
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 5
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
************** J
D E N T I
F I E D PEA
K
S U M M A
Y **************
Nuclide
Peak
Centroid
Background Net
Area
Intensity Uncert
FWHM
Channel
Energy
Counts Counts
Cts/Sec
1 Sigma %
keV
TH-227
200.12
50 .14
148 .
-18 .
-0 . 010
121.13
0 . 840s
AM-2 41
237.70
59 . 54
150 .
20 .
0 . 011
112.15
0 . 850
Sn-126
256.68
64 .28
186 .
10 .
0 . 005
248 . 50
0 . 856
BA-133
323.52
80 . 99
208 .
-25 .
-0.014
76 . 50
0 . 874s
Np-237
345.53
86 .49
680 .
0 .
0 . 000
213 . 98
0.88OA
EU-155
345 . 74
86 . 54
675 .
-24 .
-0.013
156 .39
0.880s
Sn-126
347.33
86 . 94
576 .
12 .
0 . 007
157.97
0.8 8 0D
Sn-126
349.85
87 . 57
576 .
31.
0 . 017
61.60
0.88ID
Cd-109
351.73
88 . 04
590 .
0 .
0 . 000
1000 . 00
0.8 81A
Nd-147
363.97
91.10
614 .
12 .
0 . 007
289 . 72
0.885s
TH-234
369 . 93
92 . 59
652 .
-26 .
-0.014
75 . 91
0.886s
AC-228
372.97
93 .35
578 .
24 .
0 . 013
143 . 80
0.887s
Gd-153
389.57
97 . 50
123 .
-12 .
-0.007
162.75
0 . 892s
Np-239
397.57
99 . 50
362 .
-17 .
-0 . 009
161. 66
0 . 894
Np-239
414.38
103.70
222 .
16 .
0 . 009
134.05
0 . 898s
EU-155
420.83
105.31
161.
17 .
0 . 009
108 .38
0 . 900
Np-239
424.10
106.13
224 .
-19 .
-0.011
111.89
0 . 901
EU-152
486 .69
121.78
205 .
-20 .
-0 . 011
101. 53
0 . 918s
CO - 57
487 . 83
122.06
225 .
-9 .
-0.005
250.21
0.918s
EU-154
491.98
123.10
221.
-14 .
-0.008
134 .31
0.919s
PA-2 3 4
524.77
131.29
253 .
-20 .
-0.011
116.78
0.928s
HF-181
531.68
133.02
272 .
-6 .
-0 . 003
378.25
0.930s
CE-144
533.74
133.54
279 .
0 .
0 . 000
1000 . 00
0.930s
HF-181
544.79
136 .30
279 .
0 .
0 . 000
1000.00
0 . 933s
CO - 57
545.48
136.47
246 .
19 .
0 . 010
121.17
0.933s
Tc-99m
561.63
140.51
270 .
-13 .
-0.007
180 . 89
0 . 938
U-235
574.73
143.79
528 .
-21.
-0 . 012
87.43
0 . 941s
CE-141
581.35
145.44
408 .
18 .
0 . 010
163.52
0 . 943s
Ba-140
650.24
162.66
127 .
15 .
0 . 008
109 . 57
0 . 961s
U-235
653.11
163 .38
141.
-18 .
-0.010
103.72
0 . 962s
CE-13 9
663.01
165.85
162 .
-5 .
-0 . 003
382 .28
0 . 965s
Cf-251
706.00
176 .60
154 .
-22 .
-0.012
107 .68
0 . 976s
TH-229
773 . 64
193.51
77 .
6 .
0 . 003
276 . 64
0.994s
TH-229
843.01
210.85
92 .
3 .
0 . 002
540.14
1.012s
Cf-251
907 . 62
227.00
81.
-8 .
-0.004
222.12
1.029s
PB-212
954.15
238 . 63
74 .
254 .
0 .141
7 . 91
1.04ID
PB-214
967 . 61
242.00
68 .
51.
0 . 028
26 . 94
1.045D
EU-152
978.39
244 .69
471.
17 .
0 . 009
185.43
1.048s
TH-227
1024.59
256 .24
77 .
-8 .
-0.005
245.49
1.060s
Cd-113m
1054.43
263.70
66 .
13 .
0 . 007
93 . 64
1.067s
BI-210M
1062.96
265.83
75 .
10 .
0 . 005
127 . 96
1.070s
TL-208
1108.77
277.28
60.
15 .
0 . 008
79 . 85
1.081s
Hg-203
1116.44
279.20
73 .
13 .
0 . 007
96 .41
1. 083
1-131
1136.83
284 .30
52 .
9 .
0 . 005
154.72
1.089s
(Page 7 of 21)
Page 342 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 6
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
PB-214
1180 . 66
295.26
34 .
117 .
0 . 065
13 .11
0 . 992s
PB-212
1199.76
300 . 03
314 .
0 .
0 . 000
883.18
1.105D
PA-2 31
1199.92
300.07
315 .
-16 .
-0.009
155.96
1. 105
PA-233
1200.36
300 .18
339 .
-16 .
-0 . 009
161. 60
1. 105
PA-2 31
1210.24
302 .65
355 .
-16 .
-0.009
164.98
1.107s
BA-133
1211.05
302.85
371.
-16 .
-0.009
168.61
1.108s
Ba-140
1219.04
304.85
388 .
-12 .
-0.007
225.54
1.110s
BI-210M
1219.23
304.90
400 .
0 .
0 . 000
1000 . 00
1.110s
Ir-192
1233 .41
308 .44
400 .
0 .
0 . 000
1000.00
1.113s
PA-233
1247.69
312.01
400 .
0 .
0 . 000
1000 . 00
1.117s
Ir-192
1265.61
316 .49
400 .
0 .
0 . 000
1000.00
1.122s
CR-51
1279.99
320.08
400 .
0 .
0 . 000
1000 . 00
1.125
La-140
1314.69
328 . 76
88 .
14 .
0 . 008
100.83
1.134
Cf-249
1333 .41
333 .44
130 .
-16 .
-0.009
101.78
1.139s
AC-228
1353.87
338 . 55
26 .
58 .
0 . 032
22 .37
1. 083
Cs-136
1361.93
340.57
203 .
-16 .
-0.009
128.79
1.146s
EU-152
1376.80
344 .29
187 .
-16 .
-0 . 009
123.43
1.150s
HF-181
1382 . 97
345.83
164 .
-16 .
-0.009
81. 92
1.151s
PB-214
1407.80
352.04
34 .
212 .
0 .118
9.24
1.451s
BA-133
1423 . 66
356 . 00
282 .
-11.
-0.006
224.61
1.162s
1-131
1457.59
364 .48
28 .
22 .
0 . 012
51.69
1.170s
BA-133
1535.03
383 . 84
65 .
11.
0 . 006
108.77
1.189s
Cf-249
1551.47
387 . 95
76 .
7 .
0 . 004
187.63
1.193s
SN-113
1566.43
391.69
92 .
-9 .
-0.005
222.24
1.197s
SB-125
1711.18
427.88
40 .
4 .
0 . 002
313.58
1.233s
AG-108M
1735.43
433.94
12 .
7 .
0 . 004
102.41
1.239s
pm-146
1815.20
453 . 88
32 .
0 .
0 . 000
1000.00
1.258
SB-125
1853.15
463 .37
51.
11.
0 . 006
94 . 53
1.268s
Ir-192
1871.93
468.06
55 .
11.
0 . 006
101.16
1.272s
BE - 7
1910.07
477.60
114 .
-15 .
-0.008
105.29
1.282
HF-181
1927.68
482.00
60.
10 .
0 . 006
113 . 85
1.286s
La-140
1947.77
487 . 02
87 .
6 .
0 . 003
220.04
1.291s
RH-106
2047.15
511.86
60 .
27 .
0 . 015
76 .31
2 . 565
Nd-147
2123.70
531.00
48 .
-6 .
-0.003
252.22
1.333s
CS-134
2252.65
563.24
39 .
-5 .
-0.003
195.40
1.364s
CS-134
2276.99
569.32
26 .
5 .
0 . 003
151.00
1.369s
PA-2 3 4
2277.59
569.47
32 .
-1.
-0.001
806.23
1.370
BI-207
2278.51
569.70
32 .
0 .
0 . 000
1000 . 00
1.370
TL-208
2333 .20
583 .37
12 .
64 .
0 . 036
15 . 93
1.440
SB-125
2401.71
600.50
357 .
-15 .
-0.009
66 .32
1.399s
SB-124
2410.64
602.73
342 .
-17 .
-0 . 009
62 .36
1.401s
CS-134
2418.55
604.71
326 .
-15 .
-0.009
167.44
1.403s
BI-214
2437.63
609.48
7 .
170 .
0 . 095
8.49
1.610
RU-103
2440 . 91
610.30
310 .
-15 .
-0.009
162.93
1.408s
AG-108M
2456.84
614.28
295 .
-16 .
-0 . 009
158.50
1.412s
PM-144
2471.96
618 . 06
165 .
10 .
0 . 005
187.32
1.415s
RH-106
2487 . 38
621.92
289 .
-16 .
-0.009
156 .25
1.419s
SB-125
2543.28
635 . 89
37 .
-11.
-0.006
130.14
1.432s
(Page 8 of 21)
Page 343 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
7
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
1-131
2547 . 62
636 . 97
62 .
-14 .
-0 . 007
86 . 75
1.433s
AG-110M
2630 . 77
657.76
36 .
-2 .
-0.001
722 .48
1.452s
CS-137
2646 .36
661.66
44 .
-7 .
-0.004
205.67
1.455s
PM-144
2785.90
696.54
38 .
-6 .
-0.003
259.61
1.487
NB-94
2810.25
702 . 63
47 .
-16 .
-0.009
91.69
1.493s
SB-124
2890.87
722.79
22 .
9 .
0 . 005
80 . 84
1.511s
AG-108M
2891.48
722.94
32 .
9 .
0 . 005
93 .45
1.511s
EU-154
2893.15
723 .36
41.
3 .
0 . 002
278.64
1.511s
ZR-95
2896.52
724.20
92 .
-18 .
-0.010
77 . 88
1.512s
BI-212
2908.41
727.17
26 .
9 .
0 . 005
85.41
1.515s
pm-146
2942.61
735.72
9 .
7 .
0 . 004
93 . 97
1. 523s
pm-146
2988.37
747.16
9 .
8 .
0 . 004
93 .40
1. 533s
ZR-95
3026.65
756.73
23 .
-5 .
-0.003
196.95
1.541s
AG-110M
3055.51
763.94
97 .
-23 .
-0.013
64 . 09
1. 548s
NB-95
3062.89
765 . 79
82 .
15 .
0 . 008
88 .23
1.549s
PA-234M
3065.38
766 .41
69.
-2 .
-0.001
707.39
1.550s
EU-152
3115.41
778.92
14 .
0 .
0 . 000
1000 . 00
1.561s
BI-212
3141.41
785.42
5 .
6 .
0 . 003
92 . 71
1.567s
CS-134
3183.20
795 . 87
34 .
2 .
0 . 001
418.33
1. 576s
CO - 58
3242 . 84
810.78
58 .
-14 .
-0.008
84 .11
1.589s
La-140
3262 . 82
815.77
72 .
-9 .
-0.005
130.44
1.593s
Cs-136
3273.74
818.50
72 .
10 .
0 . 005
126 .27
1. 596s
Co - 56
3386 . 82
846.77
23 .
-7 .
-0.004
144.53
1.620s
TL-208
3442.00
860.56
20 .
4 .
0 . 002
258 .49
1.632s
NB-94
3484 .13
871.10
12 .
8 .
0 . 004
70 . 18
1.641s
EU-154
3492.66
873 .23
21.
1.
0 . 001
704.60
1. 643s
PA-2 3 4
3521.86
880.53
10 .
6 .
0 . 003
88 . 00
1. 649s
PA-2 3 4
3532.70
883 .24
16 .
6 .
0 . 003
107 . 52
1. 652s
AG-110M
3538.47
884 .68
22 .
5 .
0 . 003
134.93
1. 653s
Sc-46
3556.86
889.28
50 .
-10 .
-0.006
104.97
1. 657s
y-88
3591.90
898.04
15 .
3 .
0 . 002
289 . 64
1. 664s
AC-228
3645.22
911.37
4 .
48 .
0 . 027
16 . 76
0 . 906s
AG-110M
3749.71
937.49
40 .
-17 .
-0.009
47 . 95
1.697
PA-2 3 4
3783.82
946.02
30 .
-4 .
-0 . 002
305.16
1. 704s
EU-152
3856.18
964.11
50 .
0 .
0 . 000
1000 . 00
1.719s
AC-228
3875.62
968.97
26 .
9 .
0 . 005
85.28
1.724s
EU-154
3985.06
996 .33
20 .
9 .
0 . 005
81. 75
1.746s
PA-234M
4003.73
1001.00
53 .
-14 .
-0.008
56 .31
1.750s
EU-154
4018.84
1004.77
58 .
-5 .
-0.003
207.86
1. 753s
Co - 56
4151.10
1037.84
25 .
-7 .
-0 . 004
107 . 52
1.780s
Cs-136
4192.02
1048.07
11.
1.
0 . 001
563 .47
1.788s
RH-106
4201.18
1050.36
15 .
-2 .
-0.001
282 . 84
1. 790
BI-207
4254.38
1063.66
11.
8 .
0 . 005
96 . 07
1.801s
Ga-6 8
4309.34
1077.40
11.
3 .
0 . 002
229.35
1.812s
FE-59
4396.74
1099.25
16 .
1.
0 . 001
914.69
1.829s
EU-152
4448.04
1112.07
43 .
6 .
0 . 004
150.27
1.839s
ZN-65
4461.92
1115.55
49 .
6 .
0 . 004
160.11
1. 842s
BI-214
4480 . 88
1120.29
33 .
6 .
0 . 004
132 .40
1. 845
(Page 9 of 21)
Page 344 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 8
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Sc-46
4481. 94
1120.55
39 .
6 .
0 . 004
143 .68
1. 846
Ta-182
4484 . 94
1121.30
72 .
-12 .
-0.006
107.03
1. 846s
CO-6 0
4692.68
1173.24
27 .
-2 .
-0.001
355.65
1.886s
Ta-182
4755.93
1189.05
22 .
2 .
0 . 001
431.15
1.899s
Ta-182
4885.37
1221.41
11.
9 .
0 . 005
86 .28
1.923s
Co - 56
4952.84
1238 .28
16 .
11.
0 . 006
84 . 92
1. 936s
NA-22
5097 . 84
1274.53
6 .
6 .
0 . 004
66 .37
1. 963s
EU-154
5097 . 89
1274.54
12 .
0 .
0 . 000
1000 . 00
1. 963s
FE-59
5166.10
1291.60
23 .
-8 .
-0.004
150.05
1.975s
CO-6 0
5329.71
1332.50
6 .
6 .
0 . 004
96 .69
2.005s
AG-110M
5536.89
1384 .30
12 .
-5 .
-0.003
213.71
2 . 042s
EU-152
5631. 70
1408.00
0 .
11.
0 . 006
30 .15
2.059s
K-40
5843.72
1461.01
7 .
217 .
0 .121
7 .25
1. 911
La-140
6384.49
1596 .21
18 .
-9 .
-0.005
118.63
2.185s
SB-124
6763.55
1690.98
0 .
0 .
0 . 000
1000 . 00
2,245s
BI-214
7057.56
1764.49
11.
7 .
0 . 004
73 .30
2,290s
Co - 56
7084.99
1771.35
19 .
8 .
0 . 004
84 .65
2,294s
y-88
7343 . 81
1836.06
6 .
-5 .
-0.003
124.92
2,332s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***¦>
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE - 7
C -3 . 9276E+00
5.31E+01
477.60-3.928E+00 ( 1.392E+01 1.05E+02 1.05E+01 G
NA-22 C 4 .2518E-01
9.50E+02
1274.53 4.252E-01 ?( 9.266E-01 6.64E+01 9.99E+01 G
K-40
N 1.54 56E+02
4.66E+11
1460.83 1.546E+02 (P 1.074E+01 7.25E+00 1.07E+01 G
Sc-46 F -4 . 8338E-01
8.3 8E+01
889.28-4.834E-01 ?( 1.725E+00 1.05E+02 1.00E+02 G
1120.55 3.830E-01 + 1.905E+00 1.44E+02 1.00E+02 G
MN-54 C -1.9242E-02
3.12E+02
834.85-1.924E-02 %(P 1.157E+00 3.51E+03 1.00E+02 G
FE-59 F 1.0381E-01
4.45E+01
1099.25 1.038E-01 ?( 2.216E+00 9.15E+02 5.65E+01 G
1291.60-1.205E+00 + 3.914E+00 1.50E+02 4.32E+01 G
(Page 10 of 21)
Page 345 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 9
TestAmerica Inc
Nuclide Ave activity
Co-56 C 2.4614E-01
Spectrum name: 7_Gamma_20161687.Anl
Energy Activity Code Peak MDA Comments
7.73E+01
846.77-3.402E-01 ?( 1.170E+00 1.45E+02 9.99E+01 G
1238.28 1.133E+00 ?(P 2.123E+00 8.49E+01 6.61E+01 G
1037.84-2.939E+00 + P 1.033E+01 1.08E+02 1.41E+01 G
1771.35 4.676E+00 ? 1.344E+01 8.47E+01 1.55E+01 A
CO - 57
1.1068E-01
122.06-9.918E-02 *(
136.47 1.793E+00 (
2.72E+02
8.414E-01 2.50E+02 8.56E+01 G
7.287E+00 1.21E+02 1.07E+01 G
CO - 58
-6 . 0678E-01
!10.78-6.068E-01 ?(
7.09E+01
1.713E+00 8.41E+01 9.95E+01 G
CO-6 0
4 . 4262E-01
1332.50 4.426E-01 ?(
1173 . 24-1.424E-01
1.93E+03
9.647E-01 9.67E+01 1.00E+02 G
P 1.685E+00 3.56E+02 9.99E+01 G
ZN-65
7 . 5209E-01
1115.55 7.521E-01 ?(
2.44E+02
4.164E+00 1.60E+02 5.06E+01 G
NB-94
-6 . 5814E-01
702 . 63-6.581E-01 ?(
871.10 3.841E-01 +
7.41E+06
1.385E+00 9.17E+01 9.79E+01 G
8.976E-01 7.02E+01 9.99E+01 G
ZR-95
-4 . 1071E-01
756 . 73-4.107E-01 ?(
724 . 20-1.664E+00 +
6.40E+01
1.942E+00 1.97E+02 5.45E+01 G
4.319E+00 7.79E+01 4.42E+01 G
NB-95
6 . 4506E-01
765.79 6.451E-01 &(
6.40E+01
1.909E+00 8.82E+01 9.98E+01 G
RU-103
¦1. 0616E-02
497 . 05-1.062E-02 %(
610.30-9.331E+00 +
3.93E+01
9.037E-01 3.38E+03 9.09E+01 G
5.112E+01 1.63E+02 5.75E+00 GA
RH-106
¦5.53 56E+00
621. 92-5.536E+00 &(
1050.36-7.216E+00 +
511.86 3.973E+00
3 . 74E+02
2.908E+01 1.56E+02 9.93E+00 G
7.489E+01 2.83E+02 1.56E+00 G
5.763E+00 7.63E+01 2.00E+01 GA
AG-108M
3 . 0378E-01
1.53E+05
433.94 2.038E-01 ?(P 5.415E-01 1.02E+02 9.05E+01 G
1.281E+00 9.35E+01 9.08E+01 G
3.210E+00 1.59E+02 8.98E+01 G
722.94 4.033E-01 ?(
614.28-6.022E-01 +
(Page 11 of 21)
Page 346 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:18:15 AMPage 10
Spectrum name: 7_Gamma_20161687.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
AG-110M
3 .4844E-01
2.50E+02
884.68 3 .484E-01
? (P
1.644E+00
1.35E+02 7.27E+01
G
657 .76-7.882E-02
- P
1.2 00E+00
7.22E+02 9.46E+01
G
937 . 49-2.478E+00
+ P
4.762E+00
4.80E+01 3.44E+01
G
1384.30-1.360E+00
+ P
5.528E+00
2.14E+02 2.43E+01
G
763 . 94-4.363E+00
+ P
9.233E+00
6.41E+01 2.23E+01
G
SN-113
F
-3 .2466E-01
1.15E+02
391.69-3.247E-01
? (P
1.742E+00
2.22E+02 6.40E+01
G
SB-124
F
-1. 8640E-01
6.02E+01
602.73-5.797E-01
? (P
3.103E+00
6.24E+01 9.83E+01
G
1690.98 0 . 000E+00
+
1.341E+00
1.00E+03 4.78E+01
G
722.79 3 .389E+00
? (
9.242E+00
8.08E+01 1.08E+01
G
SB-125
I
1. 0167E+00
1.01E+03
427.88 3.434E-01
? (
2.763E+00
3.14E+02 2.96E+01
G
600 . 50-2.949E+00
+ P
1.735E+01
6.63E+01 1.79E+01
G
635 . 89-3.548E+00
+ P
9.889E+00
1.30E+02 1.13E+01
G
463.37 2 . 920E+00
(P
9.326E+00
9.45E+01 1.05E+01
G
1-131
I
7 . 3570E-01
8.02E+00
364.48 5.958E-01
& (
7.411E-01
5.17E+01 8.17E+01
G
284.30 2.598E+00
(P
1.059E+01
1.55E+02 6.14E+00
G
636 . 97-6.778E+00
&
1.976E+01
8.68E+01 7.17E+00
G
Gd-153
F
-4 . 1154E-01
2.42E+02
97 . 50-4.115E-01
? (
1.817E+00
1.63E+02 3.00E+01
G
103 .20-4.323E-08
o.
"o
4.155E+00
2.83E+09 2.18E+01
G
Ga-6 8
C
6 . 8037E+00
4.71E-02
1077.40 6 . 804E+00
? (
3.660E+01
2.29E+02 3.30E+00
G
Tc-99m
I
-1. 5619E-01
2.51E-01
140 . 51-1.562E-01
& (
9.526E-01
1.81E+02 8.93E+01
G
BA-133 F -3.7269E-01
356.00-3.727E-01 ?(
302.85-1.683E+00 +
383.84 2.831E+00 ?
80.99-7.968E-01 + P
3.85E+03
2.827E+00 2.25E+02 6.20E+01 G
9.526E+00 1.69E+02 1.83E+01 G
1.045E+01 1.09E+02 8.94E+00 GA
2.247E+00 7.65E+01 3.41E+01 GA
CS-134 I -3 .2499E-01
604.71-5.432E-01 ?(
795.87 1.026E-01 +
569.32 1.060E+00 ?(
801.95 3.388E-01 %
7.54E+02
3.058E+00 1.67E+02 9.76E+01 G
1.533E+00 4.18E+02 8.55E+01 G
5.612E+00 1.51E+02 1.54E+01 G
1.585E+01 1.30E+03 8.69E+00 G
(Page 12 of 21)
Page 347 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Nuclide Ave activity
Env32 G800W064 7/11/2016 9:18:15 AMPage 11
Spectrum name: 7_Gamma_20161687.Anl
Energy Activity Code Peak MDA Comments
563 .24-2.085E+00 + P 1.236E+01 1.95E+02 8.35E+00 G
CS-137 I -3 .1079E-01
1.10E+04
661.66-3.108E-01 ?(P 1.465E+00 2.06E+02 8.52E+01 G
CE-139 F -6.7616E-02
165 . 85-6.762E-02 ?(
1.38E+02
8.842E-01 3.82E+02 7.99E+01 G
Ba-140 I 6.3331E-01
1.28E+01
537.26 9.181E-02 & (P 3.379E+00 1.45E+03 2.44E+01 G
162.66 2.757E+00 ?( 1.017E+01 1.10E+02 6.22E+00 G
304.85-5.506E+00 & 4.180E+01 2.26E+02 4.29E+00 G
La-140 I -4 . 0246E-01
1596.21-7.780E-01 ?(
487.02 3.822E-01 +
328.76 1. 362E+00 &(
815.77-1.824E+00 +
1.28E+01
1.943E+00 1.19E+02 9.54E+01 G
2.893E+00 2.20E+02 4.55E+01 G
4.631E+00 1.01E+02 2.03E+01 G
8.114E+00 1.30E+02 2.33E+01 G
CE-141 I 3.8858E-01
145.44 3 . 886E-01 & (
3.25E+01
2.131E+00 1.64E+02 4.82E+01 G
PM-144 C 6 . 2990E-02
3.63E+02
696.54-2.223E-01 ?(P 1.232E+00 2.60E+02 9.90E+01 G
618.06 3.480E-01 ?( 2.213E+00 1.87E+02 9.91E+01 G
EU-152 F 6.3915E-01
4.94E+03
344.29-1.271E+00 & ( 5.278E+00 1.
1112.07 2.777E+00 ?( 1.444E+01 1.
121. 78-7.082E-01 & 2.407E+00 1.
778.92 0.000E+00 - 6.700E+00 1.
964.11 0.000E+00 & 1.272E+01 1.
244.69 3.469E+00 ?( 2.157E+01 1.
1408.00 3.848E+00 ? 2.578E+00 3.
23E+02
50E+02
02E+02
00E+03
00E+03
85E+02
02E+01
65E+01 G
36E+01 G
86E+01 G
29E+01 G
46E+01 G
58E+00 G
10E+01 GA
EU-154 I 1.4809E+00
3.14E+03
'73 .23 3.618E-01 ?( 9.361E+00 7.05E+02 1.23E+01 G
123 .10-3.340E-01 + P
1274.54 0.000E+00 -
723.36 6.581E-01 ?(
1004.77-1.596E+00 +
996.33 4.346E+00 ?(
1.7 51E+00 1.34E+02 4.08E+01 G
3.594E+00 1.00E+03 3.52E+01 G
6.463E+00 2.79E+02 2.02E+01 G
1.150E+01 2.08E+02 1.80E+01 G
1.2 01E+01 8.18E+01 1.06E+01 G
EU-155 I 7.8942E-01
105.31 7 . 894E-01
86 . 54-8.119E-01
1.81E+03
(P 2.872E+00 1.08E+02 2.12E+01 G
4.241E+00 1.56E+02 3.07E+01 G
(Page 13 of 21)
Page 348 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 12
TestAmerica Inc
Nuclide Ave activity
HF-181 F 3.5001E-01
Spectrum name: 7_Gamma_20161687.Anl
Energy Activity Code Peak MDA Comments
482.00 3.500E-01 ?(
133.02-1.457E-01 -
345.83-2.211E+00 + P
136.30 0.000E+00 -
4.24E+01
1.3 56E+00 1.14E+02 8.05E+01 G
1.869E+00 3.78E+02 4.33E+01 G
8.767E+00 8.19E+01 1.51E+01 G
1.412E+01 1.00E+03 5.85E+00 G
Ta-182
Hg-203
8 . 0910E-02
2 . 8212E-01
1.14E+02
1121.30-1.990E+00 ?( 7.212E+00 1.07E+02 3.49E+01
1221.41 2.230E+00 ?(P 4.307E+00 8.63E+01 2.70E+01
1189.05 9.593E-01 &(P 9.461E+00 4.31E+02 1.62E+01
279.20 2.821E-01 (
4.66E+01
9.171E-01 9.64E+01 8.15E+01
G
TL-208
N
2 . 5208E+00
583.02 2.521E+00
277.28 4.047E+00 +
860.56 1.472E+00 -
6.98E+02
(P 7.433E-01 1.59E+01 8.45E+01 G
1.081E+01 7.99E+01 6.31E+00 G
P 8.942E+00 2.58E+02 1.24E+01 G
pm-146
1.0950E+00
747.16 9.190E-01 ?(
735.72 1.361E+00 ?(
453.88 0 . 000E+00 -
2.02E+03
2.067E+00 9.34E+01 3.40E+01 G
3.081E+00 9.40E+01 2.25E+01 G
1.196E+00 1.00E+03 6.50E+01 G
y-
1. 5649E-01
898.04 1.565E-01 ?(
1836 . 06-5.046E-01 +
1.07E+02
1.083E+00 2.90E+02 9.37E+01 G
1.366E+00 1.25E+02 9.92E+01 G
Cd-113m
Cf-251
3 . 5953E+03
¦1.5514E+00
263.70 3.595E+03 ?(
176.60-1.551E+00 &(
227 . 00-1.800E+00 +
5.33E+03
1.135E+04 9.36E+01 6.00E-03 K
3.28E+05
4.270E+00 1.08E+02 1.70E+01 G
1.046E+01 2.22E+02 6.30E+00 GA
Cf-249
2 . 3793E-01
387.95 2.379E-01 ?(
333 . 44-2.157E+00 +
1.28E+05
1.535E+00 1.88E+02 6.60E+01 G
7.3 75E+00 1.02E+02 1.55E+01 G
Sn-126
PB-210
N
1.3828E+00
5 . 9127E-01
87.57 8 . 714E-01 }
64.28 1. 3 83E+00 ?(
86.94 1.3 83E+00 }
46.54 5.913E-01
3.65E+07
3.195E+00 6.16E+01 3.75E+01
9.3 05E+00 2.48E+02 9.70E+00
1.329E+01 1.58E+02 9.04E+00
8.14E+03
(P 3.646E+01 1.81E+03 4.25E+00
GA
G
GA
G
(Page 14 of 21)
Page 349 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:18:15 AMPage 13
Spectrum name: 7_Gamma_20161687.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PB-212
N
9.0507E+00
238.63 9.051E+00
6 . 98E+02
(P 1.524E+00 7.91E+00 4.33E+01 G
300.03 0.000E+00 } P 4.870E+01 8.83E+02 3.28E+00 GA
PB-214
N
1. 1783E+01
5 . 84E+05
351.93 1.208E+01 *(P 1.714E+00 9.24E+00 3 . 76E+01 G
295.09 1.120E+01 (P 2.857E+00 1.31E+01 1.93E+01 G
242.00 1.067E+01 8.654E+00 2.69E+01 7.43E+00 GA
BI-207
2 . 7654E-01
569.70 0.000E+00 &(
1.18E+04
9.703E-01 1.00E+03 9.77E+01 G
1063.66 6.394E-01 ?(P 1.396E+00 9.61E+01 7.45E+01 G
BI-212
N
4 . 8903E+00
727.17 4.890E+00 ?(
785.42 1.883E+01 ?
6.98E+02
1.414E+01 8.54E+01 7.55E+00 G
4.327E+01 9.27E+01 1.28E+00 GA
BI-214
N
1. 2787E+01
609.31 1.279E+01
1120.29 2.535E+00
1764.49 4 . 293E+00
5.84E+05
(P 1.111E+00 8.49E+00 4.61E+01 G
1.163E+01 1.32E+02 1.51E+01 G
P 1.053E+01 7.33E+01 1.54E+01 G
BI-210M
3 .3443E-01
1.10E+09
265.83 3.344E-01 *(P 1.456E+00 1.28E+02 5.00E+01 G
304.90 0.000E+00 & 6.504E+00 1.00E+03 2.80E+01 G
AC-22J
N
8 . 6852E+00
911.07 8 .164E+00
968.97 2.761E+00 -
338.32 9.943E+00
93.35 4.364E+00 &
2.10E+03
(P 2.089E+00 1.68E+01 2.90E+01 G
P 7.957E+00 8.53E+01 1.75E+01 G
(P 4.610E+00 2.24E+01 1.20E+01 G
2.096E+01 1.44E+02 5.56E+00 XA
TH-227
N
-4 . 4586E+00
50 . 14-4.459E+00 & (
7.95E+03
1.454E+01 1.21E+02 8.00E+00 G
256.24-1.919E+00 + P 1.022E+01 2.45E+02 7.00E+00 G
TH-229
N
1. 6775E+00
193.51 1. 764E+00 ?(
210.85 1.550E+00 ?(
2.68E+06
1.282E+01 2.77E+02 4.40E+00 G
2.200E+01 5.40E+02 2.99E+00 G
TH-234
N
-2.9493E-01
63 .29-2.949E-01
1.63E+12
(P 2.355E+01 2.33E+03 3.81E+00 G
92.59-4.714E+00 + P 2.221E+01 7.59E+01 5.58E+00 G
PA-2 31
N
¦1.0700E+01
302.65-1.070E+01 ?(
300.07-1.241E+01 &
1.20E+07
5.929E+01 1.65E+02 2.88E+00 G
6.501E+01 1.56E+02 2.46E+00 G
(Page 15 of 21)
Page 350 of 551
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ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:18:15 AMPage 14
Spectrum name: 7_Gamma_20161687.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PA-2 3 4
N
2.8257E-01
1.63E+12
131.29-1.103E+00
? (
4.315E+00
1.17E+02 1.80E+01
G
946.02-1.529E+00
+
1.079E+01
3.05E+02 1.34E+01
G
569.47-3.977E-01
&
1.156E+01
8.06E+02 8.20E+00
G
883.24 2.880E+00
? (
1.076E+01
1.08E+02 9.60E+00
G
880.53 4 . 683E+00
7
1.416E+01
8.80E+01 6.00E+00
GA
PA-234M N
-9.0823E+01
1.63E+12
1001.00-9.082E+01
? (P
2.364E+02
5.63E+01 8.37E-01
G
766 .41-2.405E+01
&
5.962E+02
7.07E+02 2.94E-01
G
U-235 N
-2 . 0338E+00
2.57E+11
143 . 79-2.034E+00
? (P
1.056E+01
8.74E+01 1.10E+01
G
205.33-4.269E-01
% P
1.270E+01
1.18E+03 5.01E+00
G
163 .38-4 . 046E+00
+ P
1.316E+01
1.04E+02 5.08E+00
G
AM-241 T
8 .2927E-01
1.58E+05
59.54 8 . 293E-01
(
2.500E+00
1.12E+02 3.59E+01
G
Ir-192 F
2 . 1448E-01
7.40E+01
316.49 0 . 000E+00
& (
2.160E+00
1.00E+03 8.70E+01
G
468.06 5 . 752E-01
? (
1.973E+00
1.01E+02 5.18E+01
G
308.44 0.000E+00
-
5.792E+00
1.00E+03 3.18E+01
G
Cs-136 F
4.423 IE-01
1.30E+01
818.50 4.423E-01
? (
1.903E+00
1.26E+02 1.00E+02
G
1048.07 9.362E-02
-
1.2 59E+00
5.63E+02 8.00E+01
G
340 . 57-7.092E-01
+
3.073E+00
1.29E+02 4.69E+01
G
Np-239 T
-8.3753E-01
2.36E+00
103.70 6 . 584E-01
Sc.
2.969E+00
1.34E+02 2.40E+01
X
106.13-8.375E-01
(
3.141E+00
1.12E+02 2.27E+01
G
99.50-1.117E+00
+
6.064E+00
1.62E+02 1.50E+01
X
Nd-147
-1.1893E-01
1.11E+01
531.00-1.337E+00
? (
8.23 0E+00
2.52E+02 1.30E+01
G
91.10 4.406E-01 ?( 4.284E+00 2.90E+02 2.83E+01 G
( - This peak used in the nuclide activity average.
Peak is too wide, but only one peak in library.
Peak is part of a multiplet and this area went
negative during deconvolution.
Peak is too narrow.
Peak is too wide at FW25M, but ok at FWHM.
Peak fails sensitivity test.
Peak identified, but first peak of this nuclide
(Page 16 of 21)
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 15
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** £)
I S C A R D
ED ISO
TOPE P
E A K S
*************'
Nuclide
Centroid
Background
Net Area
Intensity
Uncert
Activity
Energy
Counts
Counts
Cts/Sec
1 Sigma %
TH-227
50 .14
148 .
-18 .
-0.010
121.13
-4 .459E+00
AM-2 41
59 . 54
150 .
20 .
0 . 011
112.15
8 .293E-01
BA-133
80 . 99
208 .
-25 .
-0 . 014
76 . 50
-7.968E-01
P
EU-155
86 . 54
675 .
-24 .
-0 . 013
156.39
-8.119E-01
Nd-147
91.10
614 .
12 .
0 . 007
289.72
4.406E-01
TH-234
92 . 59
652 .
-26 .
-0 . 014
75 . 91
-4.714E+00
P
Gd-153
97 . 50
123 .
-12 .
-0.007
162.75
-4.115E-01
EU-155
105.31
161.
17 .
0 . 009
108.38
7.894E-01
P
EU-152
121. 78
205 .
-20 .
-0.011
101.53
-7.082E-01
CO - 57
122.06
225 .
-9 .
-0.005
250.21
-9.918E-02
EU-154
123.10
221.
-14 .
-0.008
134 .31
-3.340E-01
P
PA-2 3 4
131.29
253 .
-20 .
-0.011
116.78
-1.103E+00
HF-181
133.02
272 .
-6 .
-0 . 003
378.25
-1.457E-01
CO - 57
136.47
246 .
19 .
0 . 010
121.17
1.793E+00
Tc-99m
140.51
270 .
-13 .
-0.007
180 . 89
-1.562E-01
U-235
143.79
528 .
-21.
-0 . 012
87.43
-2.034E+00
P
CE-141
145.44
408 .
18 .
0 . 010
163.52
3.886E-01
Ba-140
162.66
127 .
15 .
0 . 008
109.57
2.757E+00
U-235
163.38
141.
-18 .
-0.010
103.72
-4.046E+00
P
CE-139
165.85
162 .
-5 .
-0 . 003
382.28
-6.762E-02
Cf-251
176.60
154 .
-22 .
-0.012
107 .68
-1.551E+00
TH-229
193.51
77 .
6 .
0 . 003
276.64
1.764E+00
TH-229
210 . 85
92 .
3 .
0 . 002
540.14
1.550E+00
Cf-251
227.00
81.
-8 .
-0 . 004
222.12
-1.800E+00
EU-152
244 .69
471.
17 .
0 . 009
185.43
3.469E+00
TH-227
256.24
77 .
-8 .
-0.005
245 . 49
-1.919E+00
P
(Page 17 of 21)
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 16
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
BI-210M
265.83
75
10 .
0 . 005
127.96
3.344E-01
P
Hg-203
279.20
73
13 .
0 . 007
96 .41
2.821E-01
1-131
284 .30
52
9 .
0 . 005
154.72
2.598E+00
P
PA-2 31
300.07
315
-16 .
-0.009
155.96
-1.241E+01
PA-233
300.18
339
-16 .
-0.009
161. 60
-4.924E+00
PA-2 31
302.65
355
-16 .
-0.009
164.98
-1.070E+01
BA-133
302.85
371
-16 .
-0.009
168.61
-1.683E+00
Ba-140
304.85
388
-12 .
-0.007
225.54
-5.506E+00
La-140
328 . 76
88
14 .
0 . 008
100 . 83
1.362E+00
Cf-249
333.44
130
-16 .
-0.009
101.78
-2.157E+00
Cs-136
340 . 57
203
-16 .
-0.009
128.79
-7 . 092E-01
EU-152
344 .29
187
-16 .
-0.009
123.43
-1.271E+00
HF-181
345.83
164
-16 .
-0.009
81. 92
-2 . 211E+00
P
BA-133
356.00
282
-11.
-0.006
224.61
-3 . 727E-01
1-131
364 .48
28
22 .
0 . 012
51.69
5.958E-01
BA-133
383 . 84
65
11.
0 . 006
108.77
2.831E+00
Cf-249
387 . 95
76
7 .
0 . 004
187.63
2.379E-01
SN-113
391.69
92
-9 .
-0.005
222.24
-3.247E-01
P
SB-125
427 . 88
40
4 .
0 . 002
313.58
3.434E-01
AG-108M
433.94
12
7 .
0 . 004
102 .41
2.038E-01
P
SB-125
463 .37
51
11.
0 . 006
94 . 53
2.920E+00
P
Ir-192
468.06
55
11.
0 . 006
101.16
5.752E-01
BE - 7
477 .60
114
-15 .
-0.008
105.29
-3.928E+00
HF-181
482 . 00
60
10 .
0 . 006
113 . 85
3.500E-01
La-140
487.02
87
6 .
0 . 003
220 . 04
3.822E-01
RH-106
511. 86
60
27 .
0 . 015
76 .31
3.973E+00
Nd-147
531.00
48
-6 .
-0 . 003
252.22
-1.33 7E+00
CS-134
563.24
39
-5 .
-0.003
195.40
-2.085E+00
P
CS-134
569.32
26
5 .
0 . 003
151.00
1.060E+00
PA-2 3 4
569.47
32
-1.
-0.001
806.23
-3.977E-01
SB-125
600 . 50
357
-15 .
-0.009
66 .32
-2 . 949E+00
P
SB-124
602.73
342
-17 .
-0.009
62 .36
-5.797E-01
P
CS-134
604.71
326
-15 .
-0.009
167.44
-5.432E-01
RU-103
610.30
310
-15 .
-0.009
162.93
- 9.331E+00
AG-108M
614.28
295
-16 .
-0.009
158.50
-6.022E-01
PM-144
618.06
165
10 .
0 . 005
187.32
3.480E-01
RH-106
621. 92
289
-16 .
-0.009
156 .25
-5.536E+00
SB-125
635 . 89
37
-11.
-0.006
130.14
-3 . 548E+00
P
1-131
636.97
62
-14 .
-0.007
86 . 75
-6.778E+00
AG-110M
657.76
36
-2 .
-0.001
722 .48
-7.882E-02
P
CS-137
661. 66
44
-7 .
-0.004
205.67
-3.108E-01
P
PM-144
696 . 54
38
-6 .
-0.003
259.61
-2.223E-01
P
NB-94
702 . 63
47
-16 .
-0.009
91.69
-6.581E-01
SB-124
722.79
22
9 .
0 . 005
80 . 84
3.389E+00
AG-108M
722.94
32
9 .
0 . 005
93 .45
4.033E-01
EU-154
723.36
41
3 .
0 . 002
278.64
6.581E-01
ZR-95
724.20
92
-18 .
-0.010
77 . 88
-1.664E+00
BI-212
727.17
26
9 .
0 . 005
85.41
4.890E+00
(Page 18 of 21)
Page 353 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 17
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
Nuclide
Channel
Energy Background Net
area 1
Cnts/sec
Uncert FWHM
pm-146
735.72
9
7 .
0 . 004
93 . 97
1.361E+00
pm-146
747.16
9
8 .
0 . 004
93 .40
9.190E-01
ZR-95
756.73
23
-5 .
-0 . 003
196.95
-4.107E-01
AG-110M
763.94
97
-23 .
-0 . 013
64 . 09
-4.363E+00 P
NB-95
765.79
82
15 .
0 . 008
88 .23
6.451E-01
PA-234M
766.41
69
-2 .
-0.001
707.39
-2 . 405E+01
BI-212
785 . 42
5
6 .
0 . 003
92 . 71
1.883E+01
CS-134
795.87
34
2 .
0 . 001
418.33
1. 026E-01
CO - 58
810.78
58
-14 .
-0.008
84 .11
-6.068E-01
La-140
815.77
72
-9 .
-0.005
130.44
-1.824E+00
Cs-136
818.50
72
10 .
0 . 005
126 .27
4.423E-01
Co - 56
846.77
23
-7 .
-0 . 004
144.53
-3.402E-01
NB-94
871.10
12
8 .
0 . 004
70 . 18
3.841E-01
EU-154
873 .23
21
1.
0 . 001
704.60
3.618E-01
PA-2 3 4
880.53
10
6 .
0 . 003
88 . 00
4.683E+00
PA-2 3 4
883 .24
16
6 .
0 . 003
107 . 52
2.880E+00
AG-110M
884 .68
22
5 .
0 . 003
134.93
3.484E-01 P
Sc-46
889.28
50
-10 .
-0.006
104.97
-4.834E-01
y-88
898.04
15
3 .
0 . 002
289 . 64
1.565E-01
AG-110M
937.49
40
-17 .
-0.009
47 . 95
-2.478E+00 P
PA-2 3 4
946.02
30
-4 .
-0 . 002
305.16
-1.529E+00
EU-154
996.33
20
9 .
0 . 005
81. 75
4.346E+00
PA-234M
1001.00
53
-14 .
-0.008
56 .31
- 9.082E+01 P
EU-154
1004.77
58
-5 .
-0.003
207.86
-1.596E+00
Co - 56
1037.84
25
-7 .
-0.004
107 . 52
-2.93 9E+00 P
Cs-136
1048.07
11
1.
0 . 001
563 .47
9.362E-02
RH-106
1050.36
15
-2 .
-0.001
282 . 84
-7 .216E+00
BI-207
1063.66
11
8 .
0 . 005
96 . 07
6.394E-01 P
Ga-6 8
1077.40
11
3 .
0 . 002
229.35
6 . 804E+00
FE-59
1099.25
16
1.
0 . 001
914.69
1. 038E-01
EU-152
1112.07
43
6 .
0 . 004
150.27
2.777E+00
ZN-65
1115.55
49
6 .
0 . 004
160 .11
7.521E-01
Sc-46
1120.55
39
6 .
0 . 004
143 .68
3.83 0E-01
CO-6 0
1173.24
27
-2 .
-0.001
355 .65
-1.424E-01 P
Co - 56
1238.28
16
11.
0 . 006
84 . 92
1.133E+00 P
NA-22
1274.53
6
6 .
0 . 004
66 .37
4.252E-01
FE-59
1291.60
23
-8 .
-0 . 004
150.05
-1.205E+00
CO-6 0
1332.50
6
6 .
0 . 004
96 .69
4.426E-01
AG-110M
1384.30
12
-5 .
-0 . 003
213.71
-1.360E+00 P
EU-152
1408.00
0
11.
0 . 006
30 .15
3 . 848E+00
La-140
1596.21
18
-9 .
-0.005
118.63
-7.780E-01
Co - 56
1771.35
19
8 .
0 . 004
84 .65
4.676E+00
y-88
1836.06
6
-5 .
-0 . 003
124.92
-5.046E-01
P - Peakbackground subtraction
(Page 19 of 21)
Page 354 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:18:15 AMPage 18
TestAmerica Inc Spectrum name: 7_Gamma_20161687.Anl
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#A
-3 . 9276E+00
-3 . 9276E+00
1.053E+02 %
1.39E+01
NA-22
#A
4 . 2518E-01
4 . 2518E-01
6.637E+01%
9.27E-01
K-40
1.54 56E+02
1.54 56E+02
7.245E+00%
1.07E+01
Sc-46
#A
-4.8338E-01
-4 . 8338E-01
1.050E+02 %
1.73E+00
CR-51
#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.91E+01
MN-54
#A
-1. 9242E-02
-1.9242E-02
3.510E+03 %
1.16E+00
FE-59
#A
1. 0381E-01
1.0381E-01
9.14 7E+02 %
2.22E+00
Co - 56
#A
2 . 4614E-01
2.4614E-01
8.381E+01%
1.17E+00
CO - 57
#A
1.1068E-01
1.1068E-01
1.212E+02 %
8.41E-01
CO - 58
#A
-6.0678E-01
-6.0678E-01
8.411E+01%
1.71E+00
CO-6 0
#A
4 . 4262E-01
4.4262E-01
9.669E+01%
9.65E-01
ZN-65
#A
7 . 5209E-01
7.5209E-01
1.601E+02%
4.16E+00
NB-94
#A
-6 . 5814E-01
-6.5814E-01
9.169E+01%
1.39E+00
ZR-95
#A
-4 . 1071E-01
-4.1071E-01
1.969E+02%
1.94E+00
NB-95
#A
6 . 4506E-01
6.4506E-01
8.823E+01%
1.91E+00
RU-103
#A
-1.0616E-02
-1.0616E-02
3.3 77E+03 %
9.04E-01
RH-106
#A
-5.53 55E+00
-5.53 56E+00
1.562E+02 %
2.91E+01
AG-108M#A
3 . 0378E-01
3.0378E-01
6.932E+01%
5.41E-01
AG-110M#A
3 . 4844E-01
3.4844E-01
1.349E+02%
1.64E+00
SN-113
#A
-3 . 2466E-01
-3.2466E-01
2.222E+02 %
1.74E+00
SB-124
#A
-1. 8640E-01
-1.8640E-01
5.105E+01%
3.10E+00
SB-125
#A
1. 0167E+00
1. 0167E+00
9.453E+01%
2.76E+00
1-131
#A
7 .3568E-01
7 . 3570E-01
5.169E+01%
7.41E-01
Gd-153
#A
-4 . 1154E-01
-4 . 1154E-01
1.62 7E+02 %
1.82E+00
Ga-6 8
#A
6 . 7725E+00
6 . 8037E+00
2.2 93E+02 %
3.66E+01
Tc-99m
#A
-1. 5606E-01
-1.5619E-01
1.809E+02%
9.53E-01
BA-133
#A
-3 . 7269E-01
-3.7269E-01
2.246E+02 %
2.83E+00
CS-134
#A
-3 .2499E-01
-3.2499E-01
1.12 7E+02 %
3.06E+00
CS-137
#A
-3 .1079E-01
-3 .1079E-01
2.057E+02 %
1.47E+00
CE-139
#A
-6 . 7616E-02
-6 . 7616E-02
3.823E+02 %
8.84E-01
Ba-140
#A
6 .333 0E-01
6 .3331E-01
1.096E+02 %
3.3 8E+00
La-140
#A
-4 . 0246E-01
-4 . 0246E-01
7.785E+01%
1.94E+00
CE-141
#A
3.8858E-01
3.8858E-01
1.63 5E+02 %
2.13E+00
CE-144
#A
0.0000E+00
0.0000E+00
1.000E+03 %
7.39E+00
PM-144
#A
6 .2990E-02
6.2990E-02
1.601E+02%
1.23E+00
EU-152
#A
6 .3915E-01
6.3915E-01
8.957E+01%
5.28E+00
EU-154
#A
1.4809E+00
1.4809E+00
8.175E+01%
9.36E+00
EU-155
#A
7 . 8942E-01
7.8942E-01
1.084E+02 %
2.87E+00
HF-181
#A
3.5001E-01
3.5001E-01
1.13 8E+02 %
1.36E+00
Ta-182
#A
8 . 0910E-02
8.0910E-02
8.628E+01%
7.21E+00
Hg-203
#A
2 . 8212E-01
2.8212E-01
9.641E+01%
9.17E-01
TL-208
2 . 5208E+00
2.5208E+00
1.593E+01%
7.43E-01
pm-146
#A
1.0950E+00
1.0950E+00
6.624E+01%
2.07E+00
(Page 2 0 of 21)
Page 355 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 9:
18:15 AMPage 19
TestAmerica
Inc
Spectrum
name: 7 Gamma
20161687.Anl
y-88
#A
1. 5648E-01
1.5649E-01
2.896E+02%
1.08E+00
Cd-113m#A
3 . 5953E+03
3 . 5953E+03
9.364E+01%
1.13E+04
Cd-109
#A
0.0000E+00
0.0000E+00
1.000E+03 %
3.19E+01
Cf-251
#A
-1.5514E+00
-1.5514E+00
1.077E+02 %
4.27E+00
Cf-249
#A
2 .3793E-01
2.3793E-01
1.876E+02%
1.54E+00
Sn-126
#A
1.3828E+00
1.3828E+00
2 . 485E+02%
9.30E+00
PB-210
#A
5 . 9127E-01
5.9127E-01
1.808E+03 %
3.65E+01
PB-212
9.0507E+00
9.0507E+00
7.913E+00%
1.52E+00
PB-214
1.1783E+01
1.1783E+01
8.021E+00%
1.71E+00
BI-207
#A
2 . 7654E-01
2.7654E-01
9.607E+01%
9.70E-01
BI-212
#A
4 . 8903E+00
4.8903E+00
8.541E+01%
1.41E+01
BI-214
1. 2787E+01
1.2787E+01
8.486E+00%
1.11E+00
BI-210M#A
3 .3443E-01
3.3443E-01
1.28 0E+02 %
1.46E+00
AC-228
8 . 6852E+00
8.6852E+00
1.397E+01%
2.09E+00
TH-227
#A
-4 . 4586E+00
-4.4586E+00
1.211E+02%
1.45E+01
TH-229
#A
1. 6775E+00
1.6775E+00
2.766E+02 %
1.28E+01
TH-234
#A
-2 . 9493E-01
-2.9493E-01
2.331E+03 %
2.3 5E+01
PA-2 31
#A
-1.0700E+01
-1.0700E+01
1.650E+02%
5.93E+01
PA-233
#A
0.0000E+00
0.0000E+00
1. 000E+03 %
5.16E+00
PA-2 3 4
#A
2 . 8257E-01
2.8257E-01
7 . 937E+01%
4.32E+00
PA-234M#A
-9 . 0823E+01
-9.0823E+01
5.631E+01%
2.3 6E+02
U-235
#A
-2 . 0338E+00
-2.033 8E+00
8.743E+01%
1.06E+01
AM-2 41
#A
8 .2927E-01
8.2927E-01
1.122E+02 %
2.50E+00
Np-237
#A
0.0000E+00
0.0000E+00
1.000E+03 %
9.98E+00
Ir-192
#A
2 . 1448E-01
2.1448E-01
1.012E+02 %
2.16E+00
Cs-136
#A
4.423 0E-01
4.423 IE-01
1.263E+02 %
1.90E+00
Np-239
A
-8.3745E-01
-8.3753E-01
1.119E+02 %
3.14E+00
Nd-147
#A
-1.1893E-01
-1.1893E-01
1.921E+02 %
8.23E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.1 keV) 1.994E+02 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.1 keV) 1.9938333E+02 Bq/Sample
(Page 21 of 21)
Page 356 of 551
-------
257060_Gamma_160-17814-A-1-C DU. 7_Gamma_20161687.spc.
1.0e4-
1.0e3-
1.0e0-
500 1000 1500 2000 2500 3000 3500 4000
Channels
4500
5000
5500
6000
6500
7000
7500
8000
-------
Test America St. Louis Spectrum ID: 3_Gamma_2 0161196
Sample Description: 257060_Gamma_160-17814-A-2-B
Detector: Detector # 3
Batch ID: 257060
Work Order Number: Gamma
Lot Number: 160-17814-A-2-B
Decay to Time: 7/11/2016 07:46 Live Time: 1800 sec
Acquisition Time: 7/11/2016 07:46:36 Real Time: 1802 sec
Analysis Time: 7/11/2016 08:16 Dead Time: 0.11 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
3_Soil_TunaCan.Clb
3_Soil_TunaCan_90099_032 712
3/28/2012 11:26
2/28/2012 19:25
Client_Long_Revll.lib
3 2016-07-10 0602.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
-4 . 672E+00
104 . 6
4.887E+00
4.893E+00
1.641E+01
NA-22
-2.23 0E-01
190 . 9
4.256E-01
4.258E-01
1.514E+00
K-40
1. 745E+02
6.2
1.085E+01
1.405E+01
1.037E+01
Sc-46
3 . 720E-01
110 . 0
4.091E-01
4.095E-01
1.402E+00
CR-51
-3 . 933E+00
26 .3
1.036E+00
1.057E+00
1.93 0E+01
MN-54
-3 . 595E-01
138 . 0
4.961E-01
4.964E-01
1.126E+00
FE-59
-6 . 267E-02
85 . 8
5.379E-02
5.388E-02
2.789E+00
Co - 56
1. 744E-01
108 . 0
1.883E-01
1.885E-01
1.122E+00
CO - 57
1.798E-01
141. 0
2.536E-01
2.537E-01
9.321E-01
CO - 58
3.458E-01
129 . 9
4.492E-01
4.496E-01
1.541E+00
CO-6 0
3.129E-01
86 . 9
2.720E-01
2.725E-01
1.162E+00
ZN-65
-1.835E+00
89 . 7
1.646E+00
1.648E+00
5.513E+00
NB-94
6.087E-01
29.3
1.784E-01
1.811E-01
7.948E-01
ZR-95
-1.249E-01
731. 6
9.140E-01
9.140E-01
2.200E+00
NB-95
-2.559E-02
2099.0
5.372E-01
5.372E-01
1.879E+00
RU-103
-1.454E-01
255 . 9
3.721E-01
3.722E-01
9.080E-01
RH-106
3.963E+00
97 . 8
3.875E+00
3.881E+00
1.310E+01
AG-108M
1.402E-01
91. 9
1.289E-01
1.291E-01
1.014E+00
AG-110M
4.030E-02
408 . 8
1.647E-01
1.648E-01
2.3 55E+00
SN-113
4.940E-01
117 .1
5.785E-01
5.790E-01
1.955E+00
SB-124
-6.179E-02
64 . 0
3.953E-02
3.966E-02
2.975E+00
SB-125
3.3 55E+00
29.3
9.816E-01
9.965E-01
2.140E+00
1-131
4.917E-01
111. 5
5.481E-01
5.487E-01
9.127E-01
Gd-153
-7.983E-01
146 . 8
1.172E+00
1.173E+00
3.926E+00
Ga-6 8
1.3 86E+01
107 . 8
1.493E+01
1.495E+01
3.388E+01
Tc-99m
-2.902E-01
121. 0
3.511E-01
3.515E-01
1.177E+00
BA-133
-4 . 744E-01
192 .4
9.13 0E-01
9.133E-01
3.079E+00
CS-134
4 . 228E-01
61.3
2.593E-01
2.602E-01
2.929E+00
CS-137
2.168E-01
175 . 5
3.804E-01
3.806E-01
1.33 0E+00
CE-139
-5.848E-02
521.3
3.049E-01
3.050E-01
1.047E+00
Ba-140
-3 .100E-01
629 . 0
1.950E+00
1.950E+00
3.464E+00
La-140
7.570E-01
32 . 1
2.427E-01
2.460E-01
5.602E-01
CE-141
4.907E-01
123 .3
6.051E-01
6.056E-01
2.031E+00
(Page 1 of 21)
Page 358 of 551
-------
CE-144
-2 .257E+00
131.1
2.958E+00
2.960E+00
9.908E+00
PM-144
3.758E-01
100 . 6
3.779E-01
3.784E-01
8.954E-01
EU-152
2 . 046E+00
31. 7
6.481E-01
6.569E-01
5.713E+00
EU-154
9 . 565E-01
88.4
8.454E-01
8.468E-01
9.724E+00
EU-155
-7.669E-02
1294 . 6
9.929E-01
9.929E-01
5.742E+00
HF-181
-1.655E-01
81. 6
1.350E-01
1.353E-01
2.274E+00
Ta-182
-1.577E-01
1220.7
1.925E+00
1.925E+00
6.748E+00
Hg-203
1.797E-02
2353.3
4.23 0E-01
4.23 0E-01
1.119E+00
TL-208
3.719E+00
15 . 8
5.890E-01
6.198E-01
1.029E+00
pm-146
-1.905E+00
69 . 8
1.331E+00
1.334E+00
3.925E+00
y-88
4.018E-01
92 . 7
3.723E-01
3.729E-01
8.647E-01
Cd-113m
-1.437E+03
324 . 7
4.666E+03
4.667E+03
1.608E+04
Cd-109
0.000E+00
1.#INF
3.014E+00
3.014E+00
3.576E+01
Cf-251
2 . 865E-01
470 . 6
1.349E+00
1.349E+00
3.740E+00
Cf-249
0.000E+00
1.#INF
1.075E-01
1.075E-01
2.067E+00
Sn-126
-4 . 015E+00
104 . 9
4.213E+00
4.219E+00
1.407E+01
PB-210
1.163E+01
74 . 2
8.635E+00
8.662E+00
2.831E+01
PB-212
9.33 7E+00
8 . 0
7.455E-01
9.595E-01
1.447E+00
PB-214
1.242E+01
9 . 6
1.188E+00
1.3 52E+00
1.971E+00
BI-207
-2.497E-01
207 . 9
5.191E-01
5.193E-01
1.056E+00
BI-212
3 . 210E+00
182 .2
5.849E+00
5.851E+00
2.019E+01
BI-214
9 . 864E+00
10.2
1.005E+00
1.128E+00
1.641E+00
BI-210M
5 . 292E-01
100 . 0
5.293E-01
5.302E-01
1.782E+00
AC-228
8.058E+00
14 . 6
1.178E+00
1.247E+00
2.699E+00
TH -7.7.1
4.206E+00
68.2
2.868E+00
2.877E+00
9.505E+00
TH-229
9 . 649E+00
56 . 5
5.451E+00
5.505E+00
1.43 9E+01
TH-234
8.589E+00
44 . 4
3.815E+00
3.841E+00
2.180E+01
PA-2 31
-1.396E-06
1305466607.6
1.822E+01
1.822E+01
6.202E+01
PA-233
-1.014E+00
151. 5
1.536E+00
1.537E+00
5.157E+00
PA-2 3 4
-5.144E-01
123 . 5
6.3 53E-01
6.3 59E-01
5.702E+00
PA-234M
4.33 0E+01
89 . 5
3.877E+01
3.883E+01
1.939E+02
U-235
1.049E+00
93 . 0
9.757E-01
9.772E-01
9.785E+00
AM-2 41
-1.005E+00
122 . 7
1.234E+00
1.23 5E+00
3.310E+00
Np-237
2.094E+00
151.4
3.171E+00
3.173E+00
1.061E+01
Ir-192
3 . 682E-01
155 . 9
5.740E-01
5.744E-01
1.932E+00
Cs-136
2 . 435E-01
39 . 1
9.518E-02
9.620E-02
1.868E+00
Np-239
7.957E-01
152 .4
1.213E+00
1.214E+00
4.083E+00
Nd-147
1.048E+00
281. 5
2.949E+00
2.950E+00
7.290E+00
Total 3 .349E+02
Analyst: Amanda Dick
(Page 2 of 21)
Page 359 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 1
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
Sample description
257060 Gamma 160-17814-A-2-B
Spectrum Filename: C:\User\SPC\Det3\3_Gamma_20161196.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 7:46:36 AM
1800
1802
0.11 %
3
Detector system
Ge 3 SN/131
Calibration
Filename:
3 Soil TunaCan 90099 032712
3 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 7:25:37 PM
0.122 keV
0.250 keV/channel
3.421E-08 keV/channel^2
3/28/2012 11:26:55 AM
165.85 keV
Quadratic Uncertainty = 0.64
-6.102019E-01 + (-3.6422 82E-01*Log(E) )
( -2.895398E-02*Log(E)^2 )
Quadratic Uncertainty = 1.29
-2.525141E+01 + ( 9.446449E+00*Log(E) )
( -1.005974E+00*Log(E)^2 )
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 37.59keV )
8000 ( 2000.59keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
(Page 3 of 21)
Page 360 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:16:55 AMPage 2
Spectrum name: 3_Gamma_2 0161196.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 7:46:00 AM
3_2 016-07-10_06 02.PBC
7/10/2016 6:02:16 AM
total peaks alloc. 26 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.1355
* * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Energy
Factor
Energy
Ratio
Bq/Sampl
46 . 55
20 .
74.25
0 . 82
2.214E-02
46 . 54
4 .250
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 3
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
295.09
85 .
18 .65
0 . 77
2.683E-02
295.09
19.300
9 .142E+00
PB214
316.49
15 .
155 . 89
1. 09
2.556E-02
316.49
87 . 040
PBC
00
1.49
1.408E-02
722.79
10 . 810
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 4
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
969.38
-4 .
250 . 07
1. 71
1.129E-02
968.97
17.460
PBC
I-1
I-1
1. 99
9.048E-03
1291.60
43 .200
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
5
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
AC-228
373 .21
93 .35
421.
21.
0 . 012
140.54
0 . 867s
Gd-153
389.83
97 . 50
406 .
-20 .
-0 . 011
146 . 78
0 . 871
Np-239
397.83
99 . 50
426 .
-18 .
-0.010
160 . 68
0 . 873s
Gd-153
412.64
103.20
444 .
0 .
0 . 000
1000 . 00
0.877s
Np-239
414.64
103.70
444 .
0 .
0 . 000
1000.00
0.878s
Np-239
424.37
106.13
254 .
15 .
0 . 008
152.45
0.880s
EU-152
487 . 00
121.78
163 .
-18 .
-0.010
100.69
0.896s
CO - 57
488.14
122.06
182 .
-3 .
-0 . 002
664.08
0.897s
EU-154
492.30
123.10
138 .
17 .
0 . 009
103 .49
0 . 898s
PA-2 3 4
525.11
131.29
293 .
-20 .
-0.011
123.52
0.906s
HF-181
532.03
133.02
313 .
-20 .
-0 . 011
127.26
0.908s
CE-144
534.09
133.54
333 .
-20 .
-0.011
131.06
0.909s
HF-181
545.14
136 .30
353 .
-17 .
-0.010
154.43
0.911s
CO - 57
545.83
136.47
262 .
16 .
0 . 009
141.03
0.912s
Tc-99m
561.99
140.51
272 .
-20 .
-0.011
120.96
0 . 916
U-235
575.10
143.79
295 .
-10 .
-0.006
169.03
0.919s
CE-141
581.73
145.44
241.
18 .
0 . 010
123 .31
0.921s
Ba-140
650 .65
162.66
190 .
-17 .
-0.009
117.21
0.939s
U-235
653.53
163 .38
145 .
15 .
0 . 008
118.52
0.939s
CE-13 9
663.43
165.85
149 .
-3 .
-0.002
521.34
0 . 942s
Cf-251
706.45
176 .60
77 .
3 .
0 . 002
470 . 64
0 . 953s
TH-229
774.13
193.51
67 .
27 .
0 . 015
56 .49
0.970s
U-235
821.46
205.33
82 .
9 .
0 . 005
187.78
0.982s
TH-229
843.54
210.85
103 .
-5 .
-0.003
408 . 83
0.988s
Cf-251
908.18
227.00
88 .
-9 .
-0.005
197.83
1.004s
PB-212
954.74
238 . 63
48 .
226 .
0 .126
7 . 98
1.016D
PB-214
968.20
242.00
54 .
50 .
0 . 028
25 . 00
1.02 0D
TH-227
1025.21
256 .24
99 .
-18 .
-0.010
106.07
1. 034
Cd-113m
1055.07
263.70
104 .
-4 .
-0 . 002
324.70
1. 041s
BI-210M
1063.60
265.83
87 .
14 .
0 . 008
100 . 02
1. 044s
1-131
1137.51
284 .30
95 .
-19 .
-0.010
99 .65
1. 062s
PB-214
1180.71
295.09
42 .
85 .
0 . 047
18 .65
0.770s
PB-212
1200 .47
300.03
305 .
-15 .
-0.009
161.70
1. 078
PA-2 31
1200.63
300.07
306 .
-4 .
-0 . 002
589.58
1. 078
Ba-140
1219.75
304 . 85
282 .
-17 .
-0.009
143.20
1. 083s
BI-210M
1219.94
304.90
288 .
-17 .
-0.009
144 .47
1. 083s
Ir-192
1234.12
308.44
305 .
-17 .
-0.009
148.05
1.086s
PA-233
1248.42
312.01
321.
-17 .
-0.009
151.51
1.090s
Ir-192
1266.34
316 .49
257 .
15 .
0 . 008
155 . 89
1.094s
CR-51
1280.73
320.08
332 .
-18 .
-0.010
26 .34
1.098s
Cf-249
1334.18
333 .44
66 .
-4 .
-0 . 002
383 .24
1.Ills
AC-228
1353.97
338 .39
25 .
56 .
0 . 031
21.43
0.841s
Cs-136
1362.71
340 . 57
180 .
-16 .
-0.009
124 . 42
1.119s
EU-152
1377.58
344.29
182 .
-17 .
-0 . 009
117.93
1.122s
HF-181
1383.75
345.83
149 .
15 .
0 . 008
120.72
1.124s
PB-214
1408.59
352 . 03
39 .
199 .
0 . Ill
9 . 56
1.384s
BA-133
1424.46
356.00
282 .
-12 .
-0.007
192 .43
1.134
1-131
1458.41
364 .48
37 .
9 .
0 . 005
136.11
1.142s
(Page 7 of 21)
Page 364 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
6
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
BA-133
1535 . 87
383 . 84
114 .
-9 .
-0 . 005
171.05
1.162s
Cf-249
1552.32
387 . 95
123 .
0 .
0 . 000
1000.00
1.165s
SN-113
1567.28
391.69
101.
13 .
0 . 007
117.10
1.169s
SB-125
1712.08
427.88
20 .
9 .
0 . 005
98 . 99
1.205s
AG-108M
1736.34
433.94
44 .
-7 .
-0.004
197 . 75
1.211s
SB-125
1854.10
463 .37
44 .
38 .
0 . 021
29.26
1.240s
Ir-192
1872.88
468.06
96 .
-12 .
-0.007
116.95
1.244s
BE - 7
1911.04
477.60
148 .
-17 .
-0 . 009
104.59
1.254s
HF-181
1928.65
482.00
164 .
-17 .
-0.009
109.74
1.258
La-140
1948.75
487 . 02
189 .
-17 .
-0.009
116 . 80
1.263s
RU-103
1988.90
497.05
28 .
-4 .
-0.002
255.92
1.273s
RH-106
2048.16
511.86
87 .
28 .
0 . 015
50 . 85
2 . 537
Nd-147
2124.72
531.00
35 .
4 .
0 . 002
281.48
1.306
Ba-140
2149.77
537.26
26 .
-2 .
-0.001
628.98
1.312s
CS-134
2253.70
563.24
26 .
11.
0 . 006
96 .11
1.337s
CS-134
2278.04
569.32
22 .
6 .
0 . 003
129.21
1.342s
PA-2 3 4
2278.64
569.47
28 .
0 .
0 . 000
1000 . 00
1.343s
BI-207
2279.57
569.70
37 .
-7 .
-0.004
207.91
1.343s
TL-208
2334 .29
583 .38
25 .
93 .
0 . 052
15 . 84
1.277
SB-125
2402.79
600.50
326 .
-16 .
-0.009
93 . 50
1.372s
SB-124
2411.71
602.73
310 .
-15 .
-0.008
98 .24
1.374s
CS-134
2419.63
604.71
295 .
-15 .
-0.008
162.50
1.376s
BI-214
2438.90
609.53
17 .
130 .
0 . 072
10 .18
1.448
RU-103
2441. 99
610.30
280 .
-14 .
-0.008
175.17
1.382s
PM-144
2473.05
618.06
61.
-13 .
-0.007
103.04
1.389s
RH-106
2488.47
621.92
54 .
11.
0 . 006
97 . 80
1.392s
SB-125
2544.37
635 . 89
48 .
-10 .
-0.005
106.00
1.406s
1-131
2548.71
636.97
56 .
6 .
0 . 003
176.53
1.407s
AG-110M
2631.87
657.76
27 .
2 .
0 . 001
408.79
1.427s
CS-137
2647.47
661. 66
36 .
5 .
0 . 003
175 . 50
1.430s
PM-144
2787.02
696.54
19 .
10 .
0 . 005
100.56
1.463s
NB-94
2811.37
702 . 63
14 .
9 .
0 . 005
95 . 83
1.469
SB-124
2892.00
722.79
39 .
12 .
0 . 006
81. 98
1.488s
AG-108M
2892.61
722.94
51.
12 .
0 . 006
91. 91
1.488s
EU-154
2894.28
723 .36
62 .
4 .
0 . 002
306.18
1.488s
BI-212
2909.54
727.17
59 .
6 .
0 . 003
182.22
1.492s
pm-146
2989.50
747.16
42 .
-16 .
-0.009
69 . 84
1. 510
ZR-95
3027.78
756.73
33 .
-2 .
-0 . 001
731.57
1.519s
AG-110M
3056.63
763.94
70 .
-18 .
-0.010
68.47
1.526s
PA-234M
3066.51
766.41
51.
12 .
0 . 007
89 . 55
1.528s
EU-152
3116.54
778.92
19 .
4 .
0 . 002
216.89
1.540s
BI-212
3142.54
785.42
0 .
19 .
0 . 011
22 . 94
1. 546s
CS-134
3184.33
795 . 87
60 .
-8 .
-0.004
149 . 96
1. 556s
CS-134
3208.67
801. 95
52 .
12 .
0 . 007
88 . 54
1.561s
CO - 58
3243 . 96
810.78
50 .
8 .
0 . 004
129.90
1.569s
La-140
3263.94
815.77
77 .
-14 .
-0.008
89 . 57
1.574s
Cs-136
3274.86
818.50
75 .
-4 .
-0.002
285.77
1. 576s
MN-54
3340.25
834.85
24 .
-8 .
-0 . 005
137.98
1.591s
(Page 8 of 21)
Page 365 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
7
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Co - 56
3387.93
846.77
23 .
-1.
-0 . 001
832.06
1.602
TL-208
3443.11
860.56
29 .
-1.
0 . 000
680.15
1. 615s
NB-94
3485.23
871.10
6 .
19 .
0 . 011
29.30
1. 625
PA-2 3 4
3522.96
880.53
41.
11.
0 . 006
85.40
1. 633s
PA-2 3 4
3533.80
883 .24
53 .
2 .
0 . 001
448.82
1. 636s
AG-110M
3539.58
884 .68
55 .
0 .
0 . 000
1000 . 00
1. 637s
Sc-46
3557.96
889.28
35 .
8 .
0 . 004
109.98
1. 641s
y-88
3593.00
898.04
10 .
8 .
0 . 005
92 .67
1. 649s
AC-228
3646.33
911.37
9 .
43 .
0 . 024
19 . 87
1. 959
AG-110M
3750.78
937.49
35 .
-5 .
-0.003
263.94
1.685s
PA-2 3 4
3784.89
946.02
25 .
-5 .
-0.003
224 .35
1.692s
EU-152
3857.23
964.11
22 .
27 .
0 . 015
31.67
1.709s
AC-228
3876.67
968.97
56 .
-4 .
-0.002
250.07
1. 713
EU-154
3986.08
996 .33
30 .
10 .
0 . 005
88.38
1.737s
PA-234M
4004.75
1001.00
40 .
0 .
0 . 000
1000 . 00
1.742s
EU-154
4019.86
1004.77
52 .
-9 .
-0.005
116.22
1.745s
Co - 56
4152.08
1037.84
5 .
5 .
0 . 003
108.01
1.774s
Cs-136
4192.99
1048.07
5 .
12 .
0 . 007
39 . 09
1.783s
RH-106
4202.15
1050.36
44 .
-14 .
-0.008
73 .11
1.785s
BI-207
4255.33
1063.66
22 .
-3 .
-0.002
352 . 86
1.797s
Ga-6 8
4310.28
1077.40
11.
7 .
0 . 004
107.76
1.809s
FE-59
4397.65
1099.25
32 .
-9 .
-0.005
146.71
1.828s
EU-152
4448.93
1112.07
124 .
-17 .
-0 . 009
96 .18
1.839s
ZN-65
4462 . 81
1115.55
107 .
-17 .
-0.009
89.67
1. 842s
BI-214
4481.94
1120.33
1.
47 .
0 . 026
14 . 88
1.438
Sc-46
4482 . 82
1120.55
80 .
-9 .
-0.005
142 .32
1. 847s
CO-6 0
4693.48
1173.24
11.
9 .
0 . 005
86 . 92
1. 892s
Ta-182
4756.71
1189.05
27 .
-2 .
-0.001
708.52
1. 906
Ta-182
4886.09
1221.41
32 .
-6 .
-0 . 003
218 .16
1. 934
Co - 56
4953.53
1238.28
37 .
-3 .
-0.002
420.24
1. 948s
NA-22
5098.46
1274.53
23 .
-4 .
-0.002
190 . 91
1.979s
FE-59
5166.69
1291.60
6 .
7 .
0 . 004
89 .11
1. 993s
CO-6 0
5330.21
1332.50
11.
2 .
0 . 001
512 . 62
2.028s
AG-110M
5537.27
1384 .30
17 .
-4 .
-0.002
246.86
2.071s
EU-152
5632.02
1408.00
17 .
-6 .
-0.003
166 .25
2.090s
K-40
5843.87
1461.00
9 .
275 .
0 .153
6 .22
2 .284
La-140
6384.26
1596.21
0 .
10 .
0 . 006
32 . 06
2 .242s
SB-124
6763.00
1690.98
13 .
-5 .
-0.003
194.96
2 ,317s
BI-214
7056.73
1764.49
13 .
20 .
0 . 011
35 . 01
2 .373
Co - 56
7084.14
1771.35
46 .
-9 .
-0.005
111.67
2 ,379s
y-88
7342.69
1836.06
6 .
-1.
-0 . 001
490.41
2 ,428s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
(Page 9 of 21)
Page 366 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:16:55 AMPage
Spectrum name: 3_Gamma_2 0161196.Anl
***** SUMMARY
- Nuclide - Average
Name Code Activity
Bq/Sample
OF LIBRARY PEAK USAGE ***^
Peak
Energy Activity Code MDA Value
keV Bq/Sample Bq/Sample COMMENTS
BE-7 C -4 . 6721E+00
NA-22 C -2.2296E-01
K-40 N 1. 7453E+02
477 . 60-4.672E+00 & ( 1
1274 . 53-2.230E-01 ?( 1
1460.83 1.74 5E+02 (P 1
5.31E+01
641E+01 1.05E+02 1.05E+01 G
9.50E+02
514E+00 1.91E+02 9.99E+01 G
4.66E+11
037E+01 6.22E+00 1.07E+01 G
Sc-46 F 3 .7196E-01
8.3 8E+01
889.28 3.720E-01 ?( 1.402E+00 1.10E+02 1.00E+02 G
1120.55-5.031E-01 + 2.444E+00 1.42E+02 1.00E+02 G
CR-51
MN-54
-3.9334E+00
-3 . 5953E-01
320 . 08-3.933E+00 ?(P 1
834 . 85-3 . 595E-01 ?(P 1
2.77E+01
930E+01 2.63E+01 9.94E+00 G
3.12E+02
126E+00 1.38E+02 1.00E+02 G
FE-59
-6 . 2670E-02
4 . 45E+01
1099.25-8.633E-01 ?( 2.789E+00 1.47E+02 5.65E+01 G
1291.60 9 . 844E-01 ?( 1.962E+00 8.91E+01 4.32E+01 G
Co - 56
1. 7437E-01
846
1238
1037
1771
77-6
28-2
84 1
35-4
042E-02
998E-01
835E+00
579E+00
? (P 1
+ 2
? ( 4
7 . 73E+01
122E+00 8.32E+02 9.99E+01 G
805E+00 4.20E+02 6.61E+01 G
819E+00 1.08E+02 1.41E+01 G
746E+01 1.12E+02 1.55E+01 A
CO-57 C 1.7980E-01
2.72E+02
122.06-4.100E-02 &( 9.321E-01 6.64E+02 8.56E+01 G
136.47 1.949E+00 & ( 9.240E+00 1.41E+02 1.07E+01 G
CO-58 C 3 .4579E-01
810.78 3.458E-01 ?( 1
7.09E+01
541E+00 1.30E+02 9.95E+01 G
CO-6 0 F 3 .1295E-01
1.93E+03
1332.50 9.840E-02 ?(P 1.162E+00 5.13E+02 1.00E+02 G
1173.24 5.277E-01 ?(P 1.025E+00 8.69E+01 9.99E+01 G
(Page 10 of 21)
Page 367 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 9
TestAmerica Inc
Nuclide Ave activity
ZN-65 F -1.83 51E+00
NB-94
ZR-95
6 . 0867E-01
¦1.2493E-01
NB-95 I -2.5591E-02
RU-103 I -1.4541E-01
RH-106 I 3.9625E+00
AG-108M C 1.4023E-01
AG-110M F 4.0300E-02
Spectrum name: 3_Gamma_2 0161196.Anl
Energy Activity Code Peak MDA Comments
2.44E+02
1115.55-1.835E+00
? (
5.513E+00
8.97E+01 5.
06E+01
G
7.41E+06
702.63 3.490E-01
? (
7.948E-01
9.58E+01 9.
79E+01
G
871.10 8.632E-01
(
6.417E-01
2.93E+01 9.
99E+01
G
6.40E+01
756.73-1.249E-01
? (
2.200E+00
7.32E+02 5.
45E+01
G
724 . 20-2.460E-02
% P
3 . 637E+00
3.57E+03 4.
42E+01
G
6.40E+01
765.79-2.559E-02
%(
1. 879E+00
2.10E+03 9.
98E+01
G
3.93E+01
497.05-1.454E-01
? (P
9.080E-01
2.56E+02 9.
09E+01
G
610.30-8.271E+00
+
4.881E+01
1.75E+02 5.
75E+00
GJ
3.74E+02
621.92 3 . 963E+00
? (P
1.310E+01
9.78E+01 9.
93E+00
G
1050.36-4.654E+01
&
1.134E+02
7.31E+01 1.
56E+00
G
511.86 4 .269E+00
7.053E+00
5.08E+01 2.
00E+01
GJ
1.53E+05
433 . 94-2.234E-01
&( P
1.014E+00
1.98E+02 9.
05E+01
G
722.94 5 . 024E-01
? (
1.559E+00
9.19E+01 9.
08E+01
G
614.28 2.969E-07
o.
"o
3.063E+00
3.02E+08 8.
98E+01
G
2.50E+02
884.68 0.000E+00
? (
2.3 55E+00
1.00E+03 7.
27E+01
G
657.76 7.125E-02
& (
1.049E+00
4.09E+02 9.
46E+01
G
937.49-6.982E-01
+
4.228E+00
2.64E+02 3.
44E+01
G
1384.30-1.067E+00
+
5.850E+00
2.47E+02 2.
43E+01
G
763 . 94-3.392E+00
+
7.695E+00
6.85E+01 2.
23E+01
G
SN-113 F 4 . 9399E-01
SB-124 F -6 . 1789E-02
SB-125 I 3 . 3553E+00
1.15E+02
391.69 4.940E-01 ?(P 1.955E+00 1.17E+02 6.40E+01 G
602. 73-5.329E-01
1690.98-7.412E-01 +
722 .79 4.221E+00 ?(
6.02E+01
(P 2.975E+00 9.82E+01 9.83E+01 G
3.065E+00 1.95E+02 4.78E+01 G
1.163E+01 8.20E+01 1.08E+01 G
427.88 8.515E-01 ?(
600.50-3.064E+00 + P
635 . 89-3.066E+00 &
1.01E+03
2.140E+00 9.90E+01 2.96E+01 G
1.6 72E+01 9.35E+01 1.79E+01 G
1.106E+01 1.06E+02 1.13E+01 G
(Page 11 of 21)
Page 368 of 551
-------
ORTEC g v -
TestAmerica Inc
i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 10
Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide Ave activity
Energy Activity Code Peak MDA Comments
463.37 1.043E+01 (P 9.112E+00 2.93E+01 1.05E+01 G
1-131
4.9175E-01
364.48 2.638E-01
8 . 02E+00
(P 9.127E-01 1.36E+02 8.17E+01 G
284 .30-6.192E+00
+
1.584E+01
9.97E+01 6.14E+00
G
636.97 3.089E+00
? (
1.885E+01
1.77E+02 7.17E+00
G
Gd-153
F
-7 . 9834E-01
2.42E+02
97 . 50-7.983E-01
& (
3.926E+00
1.47E+02 3.00E+01
G
103.20 0 . 000E+00
+
5.587E+00
1.00E+03 2.18E+01
G
Ga-6 8
C
1. 3857E+01
4.71E-02
1077.40 1.3 86E+01
? (
3.3 88E+01
1.08E+02 3.30E+00
G
Tc-99m
I
-2 . 9024E-01
2.51E-01
140 . 51-2.902E-01
(
1.177E+00
1.21E+02 8.93E+01
G
BA-133
F
-4 . 7443E-01
3.85E+03
356 . 00-4.744E-01
& (
3.079E+00
1.92E+02 6.20E+01
G
302 . 85-1.534E-01
o.
"o
9.662E+00
1.85E+03 1.83E+01
G
383 . 84-2.506E+00
8c
1.461E+01
1.71E+02 8.94E+00
g;
80.99 1.368E-01
+ p
2.416E+00
6.47E+02 3.41E+01
g;
CS-134
I
4 . 2282E-01
7.54E+02
604.71-5.359E-01
? (
2.929E+00
1.62E+02 9.76E+01
G
795.87-3.718E-01
+
1.916E+00
1.50E+02 8.55E+01
G
569.32 1.183E+00
? (
5.336E+00
1.29E+02 1.54E+01
G
801.95 5.955E+00
? (
1.776E+01
8.85E+01 8.69E+00
G
563.24 4.474E+00
? (
1.040E+01
9.61E+01 8.35E+00
G
CS-137
I
2 . 1676E-01
1.10E+04
661.66 2.168E-01
? (
1.330E+00
1.75E+02 8.52E+01
G
CE-139
F
-5 . 8485E-02
1.38E+02
165 . 85-5.848E-02
? (
1.047E+00
5.21E+02 7.99E+01
G
Ba-140
I
-3 . 1002E-01
1.28E+01
537.26-3.100E-01
? (P
3.464E+00
6.29E+02 2.44E+01
G
162 . 66-3 . 851E+00
+
1.516E+01
1.17E+02 6.22E+00
G
304.85-8.316E+00
&
4.001E+01
1.43E+02 4.29E+00
G
La-140
I
7 . 5699E-01
1.28E+01
1596.21 7 . 570E-01
? (P
5.602E-01
3.21E+01 9.54E+01
G
487 . 02-1.104E+00
-
4.331E+00
1.17E+02 4.55E+01
G
328.76 3.953E-02
% p
4.289E+00
4.03E+03 2.03E+01
G
815.77-2.686E+00
-
8.081E+00
8.96E+01 2.33E+01
G
(Page 12 of 21)
Page 369 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 11
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
CE-141 I 4.9066E-01 3.25E+01
145.44 4 . 907E-01
? (
2.031E+00
1.23E+02 4.82E+01
G
CE-144
I
-2 . 2566E+00
2.85E+02
133 . 54-2.257E+00
? (
9.908E+00
1.31E+02 1.11E+01
G
PM-144
C
3 . 7582E-01
3.63E+02
696.54 3 . 758E-01
? (P
8.954E-01
1.01E+02 9.90E+01
G
618 . 06-4.599E-01
+ P
1.3 86E+00
1.03E+02 9.91E+01
G
EU-152
F
2 . 0463E+00
4.94E+03
344 . 29-1.441E+00
? (
5.713E+00
1.18E+02 2.65E+01
G
1112 . 07-6.778E+00
+
2.187E+01
9.62E+01 1.36E+01
G
121. 78-7.855E-01
&
2.651E+00
1.01E+02 2.86E+01
G
778.92 1.3 97E+00
? (
7.364E+00
2.17E+02 1.29E+01
G
964.11 8 . 949E+00
& (
8.3 00E+00
3.17E+01 1.46E+01
G
244.69 5 . 582E-01
o.
"o
2.433E+01
1.29E+03 7.58E+00
G
1408 . 00-1.876E+00
+
6.856E+00
1.66E+02 2.10E+01
GA
EU-154
I
9 . 5653E-01
3.14E+03
873.23-1.853E-01
%(
9.724E+00
1.44E+03 1.23E+01
G
123.10 4 . 942E-01
? (
1.718E+00
1.03E+02 4.08E+01
G
1274.54-1.151E-01
o.
"o
4.650E+00
1.11E+03 3.52E+01
G
723.36 7.222E-01
? (
7.7 09E+00
3.06E+02 2.02E+01
G
1004.11-2. 575E+00
+
1.021E+01
1.16E+02 1.80E+01
G
996.33 4.504E+00
? (
1.349E+01
8.84E+01 1.06E+01
G
EU-155
I
-7.6692E-02
1.81E+03
105.31-7.669E-02
% (P
5.742E+00
1.29E+03 2.12E+01
G
86 . 54-9.677E-01
+
4.595E+00
1.42E+02 3.07E+01
G
HF-181
F
-1.6553E-01
4.24E+01
482 . 00-6.168E-01
(
2.274E+00
1.10E+02 8.05E+01
G
133 . 02-5.767E-01
+
2.459E+00
1.27E+02 4.33E+01
G
345.83 2 . 245E+00
? (
9.134E+00
1.21E+02 1.51E+01
G
136 .30-3 . 761E+00
+
1.949E+01
1.54E+02 5.85E+00
G
Ta-182
F
-1.5768E-01
1.14E+02
1121.30-1.577E-01
%(
6.748E+00
1.22E+03 3.49E+01
G
1221.41-1.307E+00
+
6.330E+00
2.18E+02 2.70E+01
G
1189.05-5.924E-01
+
9.517E+00
7.09E+02 1.62E+01
G
Hg-203
F
1.7973E-02
4.66E+01
279.20 1.797E-02
% (P
1.119E+00
2.35E+03 8.15E+01
G
(Page 13 of 21)
Page 370 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 12
TestAmerica Inc
Nuclide Ave activity
TL-208
N
3.7188E+00
Spectrum name: 3_Gamma_2 0161196.Anl
Energy Activity Code Peak MDA Comments
6.98E+02
583.02 3.719E+00 (P 1.029E+00 1.58E+01 8.45E+01 G
277.28-3.919E-01 % P 1.664E+01 1.11E+03 6.31E+00 G
860.56-2.867E-01 - P 1.003E+01 6.80E+02 1.24E+01 G
pm-146
¦1.9054E+00
2.02E+03
747.16-1.905E+00 ?(P 3.925E+00 6.98E+01 3.40E+01 G
735.72-1.777E-01 % 4.862E+00 1.13E+03 2.25E+01 G
453.88-4.317E-02 % 1.451E+00 1.30E+03 6.50E+01 G
y-
4.0180E-01
898.04 4.018E-01 & (
1836.06-1.145E-01
1.07E+02
.647E-01 9.27E+01 9.37E+01 G
P 1.185E+00 4.90E+02 9.92E+01 G
Cd-113m
¦1.4369E+03
263. 70-1.437E+03 ?(
5.33E+03
1.608E+04 3.25E+02 6.00E-03
K
Cf-251
2 . 8654E-01
176 .60 2.865E-01 ?(
227.00-2.471E+00 +
3.28E+05
3.740E+00 4.71E+02 1.70E+01 G
1.275E+01 1.98E+02 6.30E+00 GA
Sn-126
-4 . 0153E+00
87.57 0.000E+00 +
64 . 28-4.015E+00 (
86 . 94-1.577E+00 +
3.65E+07
3.622E+00 1.00E+03 3.75E+01 GA
1.407E+01 1.05E+02 9.70E+00 G
1.524E+01 2.88E+02 9.04E+00 GA
PB-210
N
1. 1629E+01
46.54 1.163E+01
8.14E+03
(P 2.831E+01 7.42E+01 4.25E+00
G
PB-212
N
9 .3366E+00
238.63 9 . 33 7E+00
300.03-9.871E+00
6.98E+02
(P 1.447E+00 7.98E+00 4.33E+01 G
5.367E+01 1.62E+02 3.28E+00 GA
PB-214
N
1. 2421E+01
351.93 1. 242E+01
295.09 9.142E+00
242.00 1. 221E+01
5.84E+05
(P 1.971E+00 9.56E+00 3.76E+01 G
P 3.522E+00 1.87E+01 1.93E+01 G
8.966E+00 2.50E+01 7.43E+00 GA
BI-207
-2 . 4967E-01
569 . 70-2.497E-01
1.18E+04
(P 1.056E+00 2.08E+02 9.77E+01
1063.66-2.119E-01 + P 1.742E+00 3.53E+02 7.45E+01
BI-212
N
3 .2098E+00
6.98E+02
727.17 3.210E+00 (P 2.019E+01 1.82E+02 7.55E+00 G
785.42 6.231E+01 & 2.417E+01 2.29E+01 1.28E+00 GA
(Page 14 of 21)
Page 371 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 8:16:55 AMPage 13
Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
BI-214
N
9 . 8644E+00
5 . 84E+05
609.31
9.827E+00
(P
1. 641E+00
1.02E+01 4.61E+01
G
1120.29
1.717E+01
+ P
2.684E+00
1.49E+01 1.51E+01
G
1764.49
9.978E+00
? (P
1. 009E+01
3.50E+01 1.54E+01
G
BI-210M
T
5.2919E-01
1.10E+09
265.83
5.292E-01
&( P
1. 7 82E+00
1.00E+02 5.00E+01
G
304.90
-1.274E+00
8c
6 .184E+00
1.44E+02 2.80E+01
G
AC-228
N
8.0581E+00
2.10E+03
911.07
6.966E+00
(p
2 . 699E+00
1.99E+01 2.90E+01
G
968.97
-1.178E+00
- p
1. 061E+01
2.50E+02 1.75E+01
G
338 .32
1.070E+01
(p
4 . 898E+00
2.14E+01 1.20E+01
G
93 .35
4.636E+00
-
2.181E+01
1.41E+02 5.56E+00
XA
TH-227
N
4.2060E+00
7.95E+03
50 .14
4.206E+00
(
9.505E+00
6.82E+01 8.00E+00
G
256 .24
-4.831E+00
-
1.317E+01
1.06E+02 7.00E+00
G
TH-229
N
9.6487E+00
2.68E+06
193 . 51
9.649E+00
* (
1.43 9E+01
5.65E+01 4.40E+00
G
210 . 85
-2.568E+00
&
2.747E+01
4.09E+02 2.99E+00
G
TH-234
N
8.5889E+00
1.63E+12
63 .29
1.207E+01
(p
2.180E+01
6.37E+01 3.81E+00
G
92 . 59
6.214E+00
(p
1.2 56E+01
6.19E+01 5.58E+00
G
PA-2 31
N
-1.3 956E-06
1.20E+07
302.65
-1.396E-06
%(
6.2 02E+01
1.31E+09 2.88E+00
G
300.07
-3 . 584E+00
+
7.170E+01
5.90E+02 2.46E+00
G
PA-233
C
-1.0136E+00
7.82E+08
312.01
-1. 014E+00
& (
5.157E+00
1.52E+02 3.60E+01
G
300.18
6.446E-07
o.
"o
2.864E+01
1.31E+09 6.20E+00
G
PA-2 3 4
N
-5.1436E-01
1.63E+12
131.29
-1.378E+00
? (
5.702E+00
1.24E+02 1.80E+01
G
946.02
-1. 803E+00
+
9.3 78E+00
2.24E+02 1.34E+01
G
569.47
0.000E+00
+
1.104E+01
1.00E+03 8.20E+00
G
883.24
1.105E+00
Sc. (
1.745E+01
4.49E+02 9.60E+00
G
880.53
8.658E+00
¦?
2.4 91E+01
8.54E+01 6.00E+00
GA
PA-234M N 4 .3298E+01
1001.00 0.000E+00 ?(
766.41 1.666E+02 ?(
1.63E+12
1.939E+02 1.00E+03 8.37E-01 G
5.03 0E+02 8.95E+01 2.94E-01 G
(Page 15 of 21)
Page 372 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 14
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
U-235 N 1.0489E+00 2.57E+11
143.79-1.237E+00 (P 9.785E+00 1.69E+02 1.10E+01 G
205.33 2.948E+00 ?(P 1.448E+01 1.88E+02 5.01E+00 G
163.38 4.107E+00 &(P 1.639E+01 1.19E+02 5.08E+00 G
AM-241 T -1.0051E+00
1.58E+05
59.54-1.005E+00 ?( 3.310E+00 1.23E+02 3.59E+01 G
Np-237 F 2.0943E+00
2.14E+06
86.49 2.094E+00 &( 1.061E+01 1.51E+02 1.31E+01 G
Ir-192 F 3 .6821E-01
316.49 3 . 682E-01 &(
468 . 06-6.786E-01 +
308.44-1.136E+00 +
7.40E+01
1.932E+00 1.56E+02 8.70E+01 G
2.686E+00 1.17E+02 5.18E+01 G
5.651E+00 1.48E+02 3.18E+01 G
Cs-136 F 2.43 52E-01 1.30E+01
818.50-1.886E-01 &( 1.868E+00 2.86E+02 1.00E+02 G
1048.07 7.837E-01 ?( 8.575E-01 3.91E+01 8.00E+01 G
340.57-7.593E-01 + 3.180E+00 1.24E+02 4.69E+01 G
Np-239
7.9575E-01
103.70 0.000E+00 -
106 .13 7.957E-01 *(
99.50-1.485E+00 +
2.36E+00
5.072E+00 1.00E+03 2.40E+01 X
4.083E+00 1.52E+02 2.27E+01 G
8.000E+00 1.61E+02 1.50E+01 X
Nd-147
1. 0478E+00
531.00 1.048E+00 ?(
91.10 0.000E+00 -
1.11E+01
7.290E+00 2.81E+02 1.30E+01 G
4.723E+00 1.00E+03 2.83E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
(Page 16 of 21)
Page 373 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 15
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** £)
I S C A R D
ED ISO
TOPE P
E A K S
***********
Nuclide
Centroid
Background
Net Area
Intensity
Uncert
Activity
Energy
Counts
Counts
Cts/Sec
1 Sigma %
AM-2 41
59 . 54
197 .
-21.
-0.011
122.74
-1.005E+00
Sn-126
64 .28
314 .
-24 .
-0.014
104.93
-4.015E+00
BA-133
80 . 99
164 .
4 .
0 . 002
647.35
1.368E-01
EU-155
86 . 54
540 .
-23 .
-0 . 013
142 .10
-9 . 677E-01
Sn-126
86 . 94
516 .
-11.
-0.006
287.53
-1.577E+00
Gd-153
97 . 50
406 .
-20 .
-0.011
146.78
-7.983E-01
Np-239
99 . 50
426 .
-18 .
-0.010
160 . 68
-1.485E+00
Np-239
106.13
254 .
15 .
0 . 008
152 .45
7.957E-01
EU-152
121.78
163 .
-18 .
-0.010
100 .69
-7.855E-01
CO - 57
122.06
182 .
-3 .
-0 . 002
664.08
-4.100E-02
EU-154
123.10
138 .
17 .
0 . 009
103.49
4.942E-01
PA-2 3 4
131.29
293 .
-20 .
-0.011
123.52
-1.378E+00
HF-181
133.02
313 .
-20 .
-0.011
127.26
-5.767E-01
CE-144
133.54
333 .
-20 .
-0.011
131.06
-2.257E+00
HF-181
136.30
353 .
-17 .
-0.010
154.43
-3.761E+00
CO - 57
136.47
262 .
16 .
0 . 009
141.03
1.949E+00
Tc-99m
140.51
272 .
-20 .
-0.011
120.96
-2.902E-01
U-235
143.79
295 .
-10 .
-0.006
169.03
-1.23 7E+00
CE-141
145.44
241.
18 .
0 . 010
123 .31
4.907E-01
Ba-140
162.66
190 .
-17 .
-0.009
117.21
-3.851E+00
U-235
163.38
145 .
15 .
0 . 008
118.52
4.107E+00
CE-13 9
165.85
149 .
-3 .
-0 . 002
521.34
-5.848E-02
Cf-251
176.60
77 .
3 .
0 . 002
470.64
2.865E-01
TH-229
193.51
67 .
27 .
0 . 015
56 .49
9.649E+00
U-235
205.33
82 .
9 .
0 . 005
187.78
2.948E+00
TH-229
210 . 85
103 .
-5 .
-0 . 003
408.83
-2.568E+00
Cf-251
227.00
88 .
-9 .
-0.005
197.83
-2.471E+00
Cd-113m
263.70
104 .
-4 .
-0.002
324.70
-1.437E+03
BI-210M
265 . 83
87 .
14 .
0 . 008
100 . 02
5.292E-01
1-131
284 .30
95 .
-19 .
-0.010
99 .65
-6.192E+00
PA-2 31
300.07
306 .
-4 .
-0 . 002
589.58
-3.584E+00
Ba-140
304.85
282 .
-17 .
-0.009
143.20
- 8.316E+00
BI-210M
304.90
288 .
-17 .
-0.009
144 .47
-1.274E+00
(Page 17 of 21)
Page 374 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 16
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
Ir-192
308 .44
305
-17 .
-0.009
148.05
-1.136E+00
PA-233
312 . 01
321
-17 .
-0.009
151.51
-1.014E+00
Ir-192
316.49
257
15 .
0 . 008
155 . 89
3 . 682E-01
CR-51
320 . 08
332
-18 .
-0.010
26 .34
-3 . 933E+00
P
Cf-249
333.44
66
-4 .
-0.002
383 .24
-5.815E-01
Cs-136
340 . 57
180
-16 .
-0.009
124 . 42
-7.593E-01
EU-152
344 .29
182
-17 .
-0.009
117.93
-1.441E+00
HF-181
345.83
149
15 .
0 . 008
120.72
2.245E+00
BA-133
356.00
282
-12 .
-0.007
192 .43
-4 . 744E-01
1-131
364 .48
37
9 .
0 . 005
136.11
2 . 638E-01
P
BA-133
383 . 84
114
-9 .
-0.005
171.05
-2 . 506E+00
SN-113
391.69
101
13 .
0 . 007
117.10
4 . 940E-01
P
AG-108M
433.94
44
-7 .
-0 . 004
197.75
-2 . 234E-01
P
Ir-192
468.06
96
-12 .
-0.007
116.95
-6.786E-01
BE - 7
477 .60
148
-17 .
-0.009
104.59
-4.672E+00
HF-181
482 . 00
164
-17 .
-0.009
109.74
-6.168E-01
RU-103
497.05
28
-4 .
-0.002
255.92
-1.454E-01
P
RH-106
511. 86
87
28 .
0 . 015
50 . 85
4.269E+00
Nd-147
531.00
35
4 .
0 . 002
281.48
1.048E+00
Ba-140
537.26
26
-2 .
-0.001
628 . 98
-3 .100E-01
P
CS-134
563.24
26
11.
0 . 006
96 .11
4 . 474E+00
CS-134
569.32
22
6 .
0 . 003
129.21
1.183E+00
BI-207
569.70
37
-7 .
-0 . 004
207.91
-2 . 497E-01
P
SB-124
602.73
310
-15 .
-0.008
98 .24
-5 . 329E-01
P
CS-134
604.71
295
-15 .
-0.008
162.50
-5.359E-01
RU-103
610.30
280
-14 .
-0.008
175.17
-8 . 271E+00
PM-144
618.06
61
-13 .
-0.007
103.04
-4 . 599E-01
P
RH-106
621.92
54
11.
0 . 006
97 . 80
3 . 963E+00
P
1-131
636.97
56
6 .
0 . 003
176.53
3.089E+00
AG-110M
657.76
27
2 .
0 . 001
408.79
7.125E-02
PM-144
696.54
19
10 .
0 . 005
100.56
3.758E-01
P
NB-94
702.63
14
9 .
0 . 005
95 . 83
3.490E-01
SB-124
722.79
39
12 .
0 . 006
81. 98
4.221E+00
AG-108M
722.94
51
12 .
0 . 006
91. 91
5.024E-01
EU-154
723 .36
62
4 .
0 . 002
306.18
7.222E-01
BI-212
727.17
59
6 .
0 . 003
182.22
3.210E+00
P
pm-146
747.16
42
-16 .
-0.009
69 . 84
-1.905E+00
P
ZR-95
756.73
33
-2 .
-0.001
731.57
-1.249E-01
AG-110M
763.94
70
-18 .
-0.010
68.47
-3.3 92E+00
PA-234M
766.41
51
12 .
0 . 007
89 . 55
1.666E+02
EU-152
778.92
19
4 .
0 . 002
216.89
1.3 97E+00
BI-212
785 . 42
0
19 .
0 . 011
22 . 94
6.231E+01
CS-134
795.87
60
-8 .
-0 . 004
149 . 96
-3.718E-01
CS-134
801. 95
52
12 .
0 . 007
88 . 54
5.955E+00
CO - 58
810.78
50
8 .
0 . 004
129 . 90
3.458E-01
Cs-136
818.50
75
-4 .
-0 . 002
285.77
-1.886E-01
MN-54
834.85
24
-8 .
-0.005
137.98
-3.595E-01
P
Co - 56
846.77
23
-1.
-0.001
832.06
-6.042E-02
P
(Page 18 of 21)
Page 375 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 17
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
Nuclide
Channel
Energy Background Net
area 1
Cnts/sec
Uncert FWHM
NB-94
871.10
6
19 .
0 . 011
29.30
8 . 632E-01
PA-2 3 4
880 . 53
41
11.
0 . 006
85.40
8 . 658E+00
PA-2 3 4
883 .24
53
2 .
0 . 001
448.82
1.105E+00
Sc-46
889.28
35
8 .
0 . 004
109.98
3.720E-01
y-88
898.04
10
8 .
0 . 005
92 .67
4.018E-01
AG-110M
937.49
35
-5 .
-0 . 003
263.94
-6.982E-01
PA-2 3 4
946.02
25
-5 .
-0.003
224 .35
-1.803E+00
EU-152
964.11
22
27 .
0 . 015
31.67
8.949E+00
EU-154
996.33
30
10 .
0 . 005
88.38
4.504E+00
EU-154
1004.77
52
-9 .
-0.005
116.22
-2.575E+00
Co - 56
1037.84
5
5 .
0 . 003
108.01
1.835E+00
Cs-136
1048.07
5
12 .
0 . 007
39 . 09
7.837E-01
RH-106
1050.36
44
-14 .
-0.008
73 .11
-4.654E+01
BI-207
1063.66
22
-3 .
-0.002
352 . 86
-2.119E-01 P
Ga-6 8
1077.40
11
7 .
0 . 004
107.76
1.3 86E+01
FE-59
1099.25
32
-9 .
-0.005
146.71
-8.633E-01
EU-152
1112.07
124
-17 .
-0.009
96 .18
-6.778E+00
ZN-65
1115.55
107
-17 .
-0.009
89.67
-1.835E+00
Sc-46
1120.55
80
-9 .
-0.005
142 .32
-5.03 IE-01
CO-6 0
1173.24
11
9 .
0 . 005
86 . 92
5.277E-01 P
Ta-182
1189.05
27
-2 .
-0.001
708.52
-5.924E-01
Ta-182
1221.41
32
-6 .
-0 . 003
218 .16
-1.3 07E+00
Co - 56
1238 .28
37
-3 .
-0.002
420 . 24
-2.998E-01
NA-22
1274.53
23
-4 .
-0.002
190 . 91
-2.23 0E-01
FE-59
1291.60
6
7 .
0 . 004
89 .11
9.844E-01
CO-6 0
1332.50
11
2 .
0 . 001
512 . 62
9.840E-02 P
AG-110M
1384.30
17
-4 .
-0 . 002
246 . 86
-1.067E+00
EU-152
1408.00
17
-6 .
-0.003
166 .25
-1.876E+00
SB-124
1690.98
13
-5 .
-0.003
194.96
-7.412E-01
Co - 56
1771.35
46
-9 .
-0.005
111 .67
-4.579E+00
y-88
1836.06
6
-1.
-0.001
490 .41
-1.145E-01 P
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#A
-4 . 6720E+00
-4.6721E+00
1.046E+02 %
1.64E+01
NA-22
#A
-2 . 2296E-01
-2.2296E-01
1.909E+02 %
1.51E+00
K-40
1.74 53E+02
1.74 53E+02
6.218E+00%
1.04E+01
Sc-46
#A
3.7196E-01
3.7196E-01
1.100E+02 %
1.40E+00
CR-51
#A
-3.9334E+00
-3.9334E+00
2.634E+01%
1.93E+01
MN-54
#A
-3 . 5953E-01
-3.5953E-01
1.380E+02%
1.13E+00
FE-59
#A
-6 .2669E-02
-6.2670E-02
8.583E+01%
2.79E+00
Co - 56
#A
1. 7437E-01
1.7437E-01
1.080E+02%
1.12E+00
CO - 57
#A
1.7980E-01
1.7980E-01
1.410E+02%
9.32E-01
(Page 19 of 21)
Page 376 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 18
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
CO - 58
#A
3 . 4579E-01
3.4579E-01
1.299E+02%
1.54E+00
CO-6 0
#A
3 . 1295E-01
3.1295E-01
8.692E+01%
1.16E+00
ZN-65
#A
-1. 8351E+00
-1.83 51E+00
8.967E+01%
5.51E+00
NB-94
#A
6 . 0867E-01
6.0867E-01
2.930E+01%
7.95E-01
ZR-95
#A
-1. 2493E-01
-1.2493E-01
7.316E+02 %
2.20E+00
NB-95
#A
-2 . 5591E-02
-2.5591E-02
2.099E+03 %
1.88E+00
RU-103
#A
-1. 4541E-01
-1.4541E-01
2.559E+02 %
9.08E-01
RH-106
#A
3 . 9625E+00
3.9625E+00
9.780E+01%
1.31E+01
AG-108M#A
1. 4023E-01
1.4023E-01
9.191E+01%
1.01E+00
AG-110M#A
4 . 0300E-02
4.0300E-02
4.088E+02%
2.3 5E+00
SN-113
#A
4 . 9399E-01
4.9399E-01
1.171E+02 %
1.96E+00
SB-124
#A
-6 .1789E-02
-6.1789E-02
6.397E+01%
2.97E+00
SB-125
#c
3 .3553E+00
3.3 553E+00
2.926E+01%
2.14E+00
1-131
#A
4 . 9173E-01
4.9175E-01
1.115E+02 %
9.13E-01
Gd-153
#A
-7 . 9834E-01
-7.9834E-01
1.468E+02%
3.93E+00
Ga-6 8
#A
1. 3772E+01
1.3857E+01
1.078E+02%
3.3 9E+01
Tc-99m
#A
-2 . 8991E-01
-2.9024E-01
1.210E+02%
1.18E+00
BA-133
#A
-4 . 7443E-01
-4.7443E-01
1.924E+02 %
3.08E+00
CS-134
#A
4 . 2282E-01
4.2282E-01
6.133E+01%
2.93E+00
CS-137
#A
2 . 1676E-01
2.1676E-01
1.755E+02%
1.33E+00
CE-139
#A
-5 . 8485E-02
-5.8485E-02
5.213E+02 %
1.05E+00
Ba-140
#A
-3 . 1001E-01
-3.1002E-01
6.290E+02%
3.46E+00
La-140
#
7 . 5697E-01
7.5699E-01
3.206E+01%
5.60E-01
CE-141
#A
4.9066E-01
4.9066E-01
1.233E+02 %
2.03E+00
CE-144
#A
-2.2565E+00
-2.2566E+00
1.311E+02 %
9.91E+00
PM-144
#A
3 . 7582E-01
3.7582E-01
1.006E+02 %
8.95E-01
EU-152
#A
2 . 0463E+00
2.0463E+00
3.167E+01%
5.71E+00
EU-154
#A
9 . 5653E-01
9.5653E-01
8.838E+01%
9.72E+00
EU-155
#A
-7 . 6692E-02
-7.6692E-02
1.295E+03 %
5.74E+00
HF-181
#A
-1. 6553E-01
-1.6553E-01
8.157E+01%
2.27E+00
Ta-182
#A
-1.5768E-01
-1.5768E-01
1.221E+03 %
6.75E+00
Hg-203
#A
1. 7973E-02
1.7973E-02
2.3 53E+03 %
1.12E+00
TL-208
3.7188E+00
3.7188E+00
1.584E+01%
1.03E+00
pm-146
#A
-1.9054E+00
-1.9054E+00
6.984E+01%
3.93E+00
y-88
#A
4.0179E-01
4.0180E-01
9.267E+01%
8.65E-01
Cd-113m#A
-1.4369E+03
-1.4369E+03
3.24 7E+02 %
1.61E+04
Cd-109
#A
0.0000E+00
0.0000E+00
1.000E+03 %
3.58E+01
Cf-251
#A
2.8654E-01
2.8654E-01
4.706E+02 %
3.74E+00
Cf-249
#A
0.0000E+00
0.0000E+00
1.000E+03 %
2.07E+00
Sn-126
#A
-4.0153E+00
-4.0153E+00
1.04 9E+02 %
1.41E+01
PB-210
A
1.1629E+01
1.1629E+01
7.425E+01%
2.83E+01
PB-212
9.3366E+00
9 .3366E+00
7.985E+00%
1.45E+00
PB-214
1.2421E+01
1.2421E+01
9.565E+00%
1.97E+00
BI-207
#A
-2 . 4967E-01
-2.4967E-01
2.079E+02%
1.06E+00
BI-212
#A
3 .2098E+00
3.2098E+00
1.822E+02 %
2.02E+01
BI-214
9 . 8644E+00
9.8644E+00
1.018E+01%
1.64E+00
BI-210M#A
5 . 2919E-01
5 . 2919E-01
1.000E+02 %
1.78E+00
AC-228
8.0581E+00
8.0581E+00
1.461E+01%
2.70E+00
TH -7.7.1
A
4.2060E+00
4.2060E+00
6.818E+01%
9.50E+00
(Page 2 0 of 21)
Page 377 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 8:16:55 AMPage 19
TestAmerica Inc Spectrum name: 3_Gamma_2 0161196.Anl
TH-229
#A
9 . 6487E+00
9.6487E+00
5.649E+01%
1.44E+01
TH-234
A
8.5889E+00
8.5889E+00
4.442E+01%
2.18E+01
PA-2 31
#A
-1.3 956E-06
-1.3 956E-06
1.305E+09%
6.20E+01
PA-233
#A
-1.0136E+00
-1.0136E+00
1.515E+02 %
5.16E+00
PA-2 3 4
#A
-5.1436E-01
-5.1436E-01
1.23 5E+02 %
5.7 0E+00
PA-234M#A
4.3298E+01
4.3298E+01
8.955E+01%
1.94E+02
U-235
#A
1.0489E+00
1.0489E+00
9.302E+01%
9.78E+00
AM-2 41
#A
-1.0051E+00
-1.0051E+00
1.22 7E+02 %
3.31E+00
Np-237
#A
2.0943E+00
2.0943E+00
1.514E+02 %
1.06E+01
Ir-192
#A
3 . 6820E-01
3.6821E-01
1.559E+02 %
1.93E+00
Cs-136
#A
2.43 51E-01
2.4352E-01
3 . 909E+01%
1.87E+00
Np-239
#A
7.9565E-01
7.9575E-01
1.524E+02 %
4.08E+00
Nd-147
#A
1.0478E+00
1.0478E+00
2.815E+02%
7.29E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.6 keV) 2.265E+02 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.6 keV) 2.2651714E+02 Bq/Sample
(Page 21 of 21)
Page 378 of 551
-------
257060_Gamma_160-17814-A-2-B. 3_Gamma_20161196.spc.
1.0e4n
1.0e3-
1000
1500
2000
2500 3000 3500 4000 4500 5000
Channels
5500
6000
6500
7000
7500
8000
-------
Test America St. Louis Spectrum ID: 8_Gamma_2 016 0993
Sample Description: 2 5706 0_Gamma_16 0-17814-A-3-B
Detector: Detector # 8
Batch ID: 257060
Work Order Number: Gamma
Lot Number: 16 0-17814-A-3-B
Decay to Time: 7/11/2016 08:45 Live Time: 1800 sec
Acquisition Time: 7/11/2016 08:45:21 Real Time: 1854 sec
Analysis Time: 7/11/2016 09:17 Dead Time: 2.92 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
8_Soil_TunaCan.Clb
8_Soil_TunaCan_90099_032 712
3/28/2012 10:35
2/28/2012 10:34
Client_Long_Revll.lib
8 2016-07-10 1451.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
9 .476E-01
288.3
2 . 732E+00
2.732E+00
9.714E+00
NA-22
5.085E-01
65 . 0
3 . 304E-01
3.314E-01
1.079E+00
K-40
1.797E+02
6 . 9
1. 245E+01
1.548E+01
8.115E+00
Sc-46
3.967E-01
126 . 9
5 . 035E-01
5.039E-01
2.204E+00
CR-51
3.577E+00
104 .3
3 . 732E+00
3.737E+00
1.258E+01
MN-54
3.045E-01
94 .3
2.871E-01
2.875E-01
7.132E-01
FE-59
5.614E-01
196 .4
1.102E+00
1.103E+00
2.627E+00
Co - 56
1.011E+00
44 . 6
4.510E-01
4.540E-01
1.147E+00
CO - 57
-2.736E-02
94 . 9
2.595E-02
2.599E-02
1.167E+00
CO - 58
-5.915E-01
87 . 5
5.179E-01
5.188E-01
1.748E+00
CO-6 0
1.152E-01
220 . 7
2.541E-01
2.542E-01
1.656E+00
ZN-65
-5 . 123E-01
305.3
1.564E+00
1.564E+00
5.459E+00
NB-94
1. 623E-01
192 .1
3.118E-01
3.119E-01
1.244E+00
ZR-95
3.145E-02
2755 . 0
8.666E-01
8.666E-01
2.156E+00
NB-95
0.000E+00
1.#INF
2.326E-01
2.326E-01
1.595E+00
RU-103
1.864E-01
245.3
4.574E-01
4.575E-01
1.134E+00
RH-106
3 .487E+00
101. 0
3.522E+00
3.526E+00
3.23 9E+01
AG-108M
-5.421E-01
120 . 7
6.544E-01
6.549E-01
1.255E+00
AG-110M
1.496E-01
43 .2
6.455E-02
6.500E-02
2.842E+00
SN-113
5.850E-01
118 . 1
6.907E-01
6.913E-01
2.336E+00
SB-124
0.000E+00
1.#INF
1.500E-01
1.500E-01
3.210E+00
SB-125
1. 065E+00
92 . 6
9.859E-01
9.874E-01
3.332E+00
1-131
3 . 012E-01
96 .2
2.896E-01
2.900E-01
7.388E-01
Gd-153
-1.226E+00
162 . 5
1.992E+00
1.993E+00
6.639E+00
Ga-6 8
4.915E+00
354 . 7
1.744E+01
1.744E+01
4.288E+01
Tc-99m
2.875E-01
157 . 8
4.538E-01
4.541E-01
1.522E+00
BA-133
-6.707E-01
164 . 5
1.103E+00
1.104E+00
3.712E+00
CS-134
5.061E-01
79.3
4.013E-01
4.022E-01
3.240E+00
CS-137
-9.384E-01
83 .3
7.821E-01
7.836E-01
1.983E+00
CE-139
-3 . 822E-01
92 . 6
3.540E-01
3.558E-01
1.184E+00
Ba-140
9 . 039E-01
132 .1
1.194E+00
1.195E+00
3.108E+00
La-140
1. 864E-01
120.2
2.23 9E-01
2.241E-01
7.522E-01
CE-141
-7.033E-01
146 . 1
1.027E+00
1.028E+00
3.432E+00
(Page 1 of 21)
Page 380 of 551
-------
CE-144
2.186E+00
147 . 4
3.222E+00
3.224E+00
1.082E+01
PM-144
1.13 0E-01
398 .2
4.501E-01
4.501E-01
1.107E+00
EU-152
2.180E+00
92 . 0
2.006E+00
2.009E+00
6.278E+00
EU-154
8.582E-01
82 .2
7.054E-01
7.068E-01
1.3 01E+01
EU-155
-1.723E+00
170.3
2.935E+00
2.936E+00
9.779E+00
HF-181
7.882E-01
68 .1
5.370E-01
5.385E-01
1.329E+00
Ta-182
2.918E+00
47 . 0
1.3 71E+00
1.379E+00
6.447E+00
Hg-203
-4 . 929E-01
ro
00
4.122E-01
4.13 IE-01
1.378E+00
TL-208
3 . 731E+00
13 .1
4.906E-01
5.274E-01
7.462E-01
pm-146
-4.985E-02
3079.0
1.535E+00
1.535E+00
3.772E+00
y-88
1.052E-01
398 .2
4.191E-01
4.191E-01
1.074E+00
Cd-113m
-6 . 511E+03
87 . 8
5.719E+03
5.735E+03
1.914E+04
Cd-109
-9.978E+00
168 . 7
1.683E+01
1.684E+01
5.611E+01
Cf-251
1. 322E+00
111. 8
1.478E+00
1.483E+00
3.832E+00
Cf-249
-5 . 745E-01
130 . 0
7.471E-01
7.476E-01
2.526E+00
Sn-126
1. 828E+00
270 . 6
4.945E+00
4.946E+00
1.668E+01
PB-210
-1. 735E+01
55 . 5
9.629E+00
9.682E+00
6.244E+01
PB-212
8 . 427E+00
8 . 8
7.429E-01
9.214E-01
1.419E+00
PB-214
1. 548E+01
6 . 7
1.044E+00
1.318E+00
1.941E+00
BI-207
-1.191E-01
347 . 9
4.144E-01
4.144E-01
1.223E+00
BI-212
-9.020E+00
106 .1
9.570E+00
9.581E+00
2.991E+01
BI-214
1.186E+01
11. 6
1.369E+00
1.501E+00
2.158E+00
BI-210M
-8.471E-01
88 . 5
7.496E-01
7.513E-01
2.506E+00
AC-228
8.324E+00
16 .2
1.3 50E+00
1.416E+00
4.733E+00
TH -7.7.1
6 . 663E+00
105 . 9
7.059E+00
7.069E+00
2.361E+01
TH-229
2 . 539E+00
102 .4
2.601E+00
2.608E+00
1.887E+01
TH-234
1.076E+01
38.4
4.138E+00
4.176E+00
2.284E+01
PA-2 31
6 .302E+00
201.4
1.269E+01
1.269E+01
8.142E+01
PA-233
1.955E-01
735 . 0
1.437E+00
1.437E+00
6.676E+00
PA-2 3 4
1. 815E+00
90 .1
1.636E+00
1.638E+00
6.385E+00
PA-234M
-8 . 245E+01
68 . 7
5.667E+01
5.683E+01
3.472E+02
U-235
-3 . 823E+00
64 .3
2.458E+00
2.466E+00
1.481E+01
AM-2 41
-1.981E+00
42 .2
8.364E-01
8.427E-01
4.833E+00
Np-237
-2.577E+00
184 . 0
4.742E+00
4.745E+00
1.582E+01
Ir-192
-4.756E-01
120 . 0
5.706E-01
5.713E-01
1.919E+00
Cs-136
6.516E-01
62 .3
4.058E-01
4.076E-01
1.861E+00
Np-239
1.506E+00
172 . 7
2.600E+00
2.602E+00
8.670E+00
Nd-147
0.000E+00
1.#INF
1.319E+00
1.319E+00
7.805E+00
Total 2 . 905E+02
Analyst: Amanda Dick
(Page 2 of 21)
Page 381 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 1
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
Sample description
257060 Gamma 160-17814-A-3-B
Spectrum Filename: C:\User\SPC\Det8\8_Gamma_20160993.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016
1800
1854
2 . 92 %
8:45:21 AM
Detector system
Ge 8 SN/174
Calibration
Filename:
8 Soil TunaCan 90099 032712
8 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 10:34:41 AM
0.052 keV
0.250 keV/channel
5.282E-10 keV/channel^2
3/28/2012 10:35:20 AM
165.85 keV
Quadratic Uncertainty = 1.3 9
-1.098764E-01 + (-4.958544E-01*Log(E) )
( -2.572270E-02*Log(E)^2 )
Quadratic Uncertainty = 1.71
-2.525301E+01 + ( 9.3 982 53E+00*Log(E) )
( -1.000034E+00*Log(E)^2 )
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 37.55keV )
8000 ( 1999.97keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
(Page 3 of 21)
Page 382 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:04 AMPage 2
Spectrum name: 8_Gamma_2 016 0993.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 8:45:00 AM
8_2016 - 07 -10_1451.PBC
7/10/2016 2:51:27 PM
total peaks alloc. 22 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.0881
* * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Energy
Factor
Energy
Ratio
Bq/Sampl
50 .14
22 .
. 105.94
1. 01
2.267E-02
50 . 14
8 . 000
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 3
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
140.51
18 .
157 . 81
1. 08
3 . 945E-02
140.51
89.300
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 4
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
766.41
7 .
89.20
1. 53
1.070E-02
765.79
99 . 790
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 5
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based
on library:
Client
Long Revll.
lib
************** J
D
E N T I
F I
ED P
E A K S
U M M A R
Y" **************
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec
1 Sigma %
keV
PB-210
185.96
46 . 54
399 .
-27 .
-0 . 015
55 . 50
1. 012s
TH -7.7.1
200.37
50 .14
255 .
22 .
0 . 012
105 . 94
1. 015
AM-2 41
237.95
59 . 54
351.
-37 .
-0.020
42 .22
1. 022s
TH-234
252.71
63 .23
96 .
20 .
0 . 011
83 .61
0 . 708s
Sn-126
256.93
64 .28
364 .
10 .
0 . 006
270.55
1. 026
BA-133
323.77
80 . 99
741.
-22 .
-0.012
176.13
1.039s
Np-237
345 . 77
86 .49
968 .
-24 .
-0.013
184.02
1. 043
EU-155
345.98
86 . 54
1119 .
-27 .
-0.015
175.32
1. 043
Sn-126
347 . 57
86 . 94
1092 .
-27 .
-0.015
173.14
1. 044
Sn-126
350.09
87 . 57
1065 .
-27 .
-0.015
170.94
1. 044
Cd-109
351.97
88 . 04
1037 .
-27 .
-0.015
168.71
1. 044
Nd-147
364.21
91.10
1010 .
-27 .
-0 . 015
166.15
1. 047s
TH-234
370.17
92 . 59
146 .
48 .
0 . 027
38.45
1. 048D
AC-228
373.21
93 .35
957 .
-27 .
-0.015
161.49
1. 049s
Gd-153
389.81
97 . 50
975 .
-27 .
-0 . 015
162 .45
1. 052s
Np-239
397.81
99 . 50
1002 .
-27 .
-0.015
164.45
1. 053s
Gd-153
412.62
103.20
1029 .
-27 .
-0.015
166.19
1. 056s
Np-239
414 . 62
103.70
1057 .
-27 .
-0.015
168 .31
1.057s
EU-155
421.07
105.31
1084 .
-28 .
-0.015
170 .27
1. 058
Np-239
424 . 34
106.13
976 .
26 .
0 . 014
172 .69
1. 058s
EU-152
486 . 92
121.78
214 .
-23 .
-0.013
91.49
1.071s
CO - 57
488.06
122.06
238 .
-20 .
-0.011
109 . 92
1.071s
EU-154
492.22
123.10
210 .
10 .
0 . 006
207.36
1.072s
PA-2 3 4
525.00
131.29
304 .
6 .
0 . 003
405.17
1. 078
HF-181
531.92
133.02
310 .
18 .
0 . 010
143.58
1.079s
CE-144
533.98
133.54
328 .
18 .
0 . 010
147.43
1.080s
HF-181
545.02
136 .30
346 .
18 .
0 . 010
150.94
1.082s
CO - 57
545.72
136.47
363 .
18 .
0 . 010
154.63
1.082s
Tc-99m
561. 86
140.51
381.
18 .
0 . 010
157 . 81
1.085s
U-235
574.97
143.79
569 .
-29 .
-0.016
64 .29
1. 087
CE-141
581. 59
145.44
584 .
-24 .
-0.013
146.08
1.089s
Ba-140
650.47
162.66
142 .
3 .
0 . 002
534 . 83
1.102s
U-235
653.35
163 .38
148 .
-3 .
-0.002
587.07
1.102s
CE-13 9
663 .24
165.85
161.
-20 .
-0.011
92 .60
1.104s
Cf-251
706.23
176 .60
66 .
14 .
0 . 008
111. 80
1.112s
TH-229
773.87
193.51
95 .
-8 .
-0.005
221. 92
1.125s
(Page 7 of 21)
Page 386 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 6
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
TH-229
843.24
210.85
84 .
18 .
0 . 010
102 .44
1.138s
Cf-251
907 . 84
227 . 00
76 .
5 .
0 . 003
344 .29
1.151s
PB-212
954.37
238 . 63
35 .
180 .
0 .100
8 . 81
1.159D
PB-214
967.84
242.00
36 .
57 .
0 . 032
19 . 94
1.162D
TH -7.7.1
1024.81
256.24
68 .
-14 .
-0.008
118.38
1.172s
Cd-113m
1054.65
263.70
114 .
-18 .
-0.010
87 . 84
1.178s
BI-210M
1063.18
265 . 83
135 .
-19 .
-0 . Oil
88.48
1.179s
TL-208
1110.57
277.68
10 .
17 .
0 . 010
38.45
1. 095
Hg-203
1116.66
279.20
99 .
-18 .
-0.010
83 . 62
1.189s
1-131
1137.05
284 .30
60.
-9 .
-0 . 005
171. 77
1.193s
PB-214
1180.22
295.09
22 .
125 .
0 . 069
10.42
1.201D
PB-212
1199.98
300.03
26 .
27 .
0 . 015
33 . 52
1.205D
PA-2 31
1200.14
300.07
384 .
14 .
0 . 008
201.36
1.205s
PA-233
1200 . 58
300 .18
398 .
4 .
0 . 002
734.96
1.205s
PA-2 31
1210.46
302.65
402 .
0 .
0 . 000
1000 . 00
1.207s
BA-133
1211.27
302 . 85
402 .
0 .
0 . 000
1000.00
1.207
Ba-140
1219.26
304.85
402 .
0 .
0 . 000
1000 . 00
1.208s
BI-210M
1219.45
304.90
402 .
0 .
0 . 000
1000.00
1.208s
Ir-192
1233 . 62
308.44
402 .
0 .
0 . 000
1000 . 00
1.211
Ir-192
1265 . 82
316.49
185 .
-16 .
-0.009
119.97
1.217s
CR-51
1280.20
320.08
99 .
14 .
0 . 008
104 .32
1.219s
La-140
1314.91
328 . 76
240 .
-15 .
-0.008
150 . 53
1.226s
Cf-249
1333 . 63
333 .44
225 .
-15 .
-0.008
145.55
1.229s
AC-228
1353.15
338 .32
216 .
15 .
0 . 008
142 .25
1.233
Cs-136
1362 .15
340 . 57
201.
15 .
0 . 008
137.26
1.234s
EU-152
1377.01
344 .29
160 .
14 .
0 . 008
128.04
1.237s
HF-181
1383.19
345 . 83
168 .
14 .
0 . 008
137.26
1.238s
PB-214
1407.85
351.99
26 .
212 .
0 .118
8 . 57
1.243
BA-133
1423 . 87
356.00
297 .
-15 .
-0.008
164.51
1.245s
1-131
1457.81
364 .48
16 .
9 .
0 . 005
96 .16
1.252s
BA-133
1535.24
383 . 84
116 .
-16 .
-0.009
117.31
1.266s
Cf-249
1551.68
387 . 95
131.
-13 .
-0 . 007
130 . 03
1.269s
SN-113
1566 . 64
391.69
103 .
13 .
0 . 007
118.07
1.271s
SB-125
1711.39
427.88
36 .
0 .
0 . 000
1000.00
1.297s
AG-108M
1735.64
433.94
48 .
-15 .
-0.008
120.70
1.301s
SB-125
1853.36
463 .37
48 .
11.
0 . 006
92 . 56
1.322s
Ir-192
1872.14
468.06
64 .
-3 .
-0.002
413 . 86
1.325s
BE - 7
1910.28
477.60
32 .
3 .
0 . 002
288.30
1.332s
HF-181
1927.89
482.00
35 .
8 .
0 . 004
109.65
1.335
La-140
1947.98
487 . 02
43 .
8 .
0 . 004
120 .16
1.339s
RU-103
1988.12
497.05
30 .
5 .
0 . 003
245.31
1.346s
RH-106
2047.36
511.86
70 .
16 .
0 . 009
138 . 96
2 .606
Nd-147
2123.91
531.00
26 .
0 .
0 . 000
1000 . 00
1.369s
Ba-140
2148.95
537.26
13 .
6 .
0 . 003
132.10
1.373s
CS-134
2252.86
563.24
22 .
3 .
0 . 002
352.79
1.391s
CS-134
2277.20
569.32
26 .
4 .
0 . 002
187.08
1.395s
PA-2 3 4
2277.80
569.47
22 .
8 .
0 . 004
90 .14
1.395s
BI-207
2278.73
569.70
33 .
-3 .
-0.002
347.91
1.396s
(Page 8 of 21)
Page 387 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
7
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
TL-208
2332.00
583.02
7 .
77 .
0 . 043
13 .15
0 . 958s
SB-125
2401.92
600.50
239 .
-4 .
-0 . 002
527 .18
1.416s
SB-124
2410.85
602.73
235 .
0 .
0 . 000
1000 . 00
1.418s
CS-134
2418.76
604.71
235 .
0 .
0 . 000
1000.00
1.419s
BI-214
2437.16
609.31
19 .
121.
0 . 067
11. 55
1.394
RU-103
2441.12
610.30
235 .
0 .
0 . 000
1000 . 00
1.423s
AG-108M
2457.05
614.28
235 .
0 .
0 . 000
1000.00
1.426s
PM-144
2472.18
618 . 06
235 .
0 .
0 . 000
1000 . 00
1.428s
RH-106
2487.60
621.92
232 .
0 .
0 . 000
1000.00
1.431s
SB-125
2543.49
635 . 89
17 .
4 .
0 . 002
168.86
1.440
AG-110M
2630.98
657.76
6 .
11.
0 . 006
43 .16
1.455s
CS-137
2646 . 58
661.66
53 .
-17 .
-0.010
83 .34
1.457s
PM-144
2786.11
696.54
19 .
2 .
0 . 001
398.21
1.480s
NB-94
2810.46
702 . 63
23 .
3 .
0 . 001
389.11
1.484s
SB-124
2891.09
722.79
54 .
-14 .
-0.008
79 . 90
1.497s
EU-154
2893.37
723 .36
68 .
0 .
0 . 000
1000 . 00
1.498s
ZR-95
2896.74
724 .20
68 .
0 .
0 . 000
1000.00
1.498s
BI-212
2908.63
727 . 17
84 .
-14 .
-0.008
106.10
1. 500
pm-146
2942.83
735 . 72
37 .
-12 .
-0.007
108 . 88
1. 506s
AG-110M
3055.73
763.94
31.
5 .
0 . 003
158.23
1.524s
NB-95
3063.11
765 . 79
36 .
0 .
0 . 000
1000 . 00
1. 525
PA-234M
3065.60
766 .41
18 .
7 .
0 . 004
89.20
1. 526s
EU-152
3115.64
778.92
23 .
-7 .
-0.004
144.53
1. 534
BI-212
3141.64
785.42
28 .
-6 .
-0.003
191.49
1. 538s
CS-134
3183.43
795 . 87
14 .
8 .
0 . 004
79.30
1. 544
CS-134
3207.77
801. 95
25 .
8 .
0 . 004
100 .15
1. 548s
CO - 58
3243 . 06
810.78
39 .
-11.
-0.006
87 . 54
1. 554s
La-140
3263.04
815.77
50 .
-5 .
-0.003
226.07
1.557s
Cs-136
3273.97
818.50
45 .
9 .
0 . 005
106.03
1.559s
MN-54
3339.36
834.85
5 .
5 .
0 . 003
94 .29
1.569s
TL-208
3442 .23
860.56
9 .
8 .
0 . 004
91. 92
1.585s
NB-94
3484 .36
871.10
19 .
3 .
0 . 002
192 . 05
1.592s
EU-154
3492.89
873 .23
28 .
-6 .
-0.004
100.43
1.593s
PA-2 3 4
3522.10
880.53
21.
8 .
0 . 004
90.49
1.598s
PA-2 3 4
3532.94
883 .24
52 .
-12 .
-0.007
86 . 81
1.599s
AG-110M
3538.71
884 .68
49 .
-9 .
-0 . 005
119 . 92
1.600s
Sc-46
3557.10
889.28
56 .
4 .
0 . 002
283 .11
1. 603s
y-88
3592.14
898.04
9 .
2 .
0 . 001
398.22
1. 608s
AC-228
3644.26
911.07
19 .
24 .
0 . 014
42 . 77
1. 616s
AG-110M
3749.96
937.49
25 .
-7 .
-0.004
161. 52
1. 633s
PA-2 3 4
3784.07
946.02
15 .
5 .
0 . 003
176.07
1. 638s
EU-152
3856.43
964.11
53 .
8 .
0 . 005
132.17
1. 649s
AC-228
3875.45
968.86
0 .
38 .
0 . 021
16 .22
1.333
EU-154
3985.31
996 .33
63 .
-14 .
-0.008
83 .36
1. 668s
PA-234M
4003.99
1001.00
81.
-11.
-0.006
68 . 73
1. 671s
EU-154
4019.10
1004.77
74 .
10 .
0 . 005
130.17
1.673
Co - 56
4151.36
1037.84
5 .
5 .
0 . 003
111.96
1. 693s
Cs-136
4192.29
1048.07
13 .
8 .
0 . 005
69 . 50
1. 698s
(Page 9 of 21)
Page 388 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 8
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
RH-106
4201.45
1050.36
15 .
6 .
0 . 003
100.98
1.700s
BI-207
4254 .65
1063.66
18 .
-7 .
-0 . 004
85.22
1.708s
Ga-6 8
4309.61
1077.40
10 .
2 .
0 . 001
354.73
1.716s
FE-59
4397.02
1099.25
16 .
4 .
0 . 002
196 .36
1.728s
EU-152
4448 .32
1112.07
70 .
-10 .
-0.006
117.43
1. 736s
ZN-65
4462.20
1115.55
60.
-4 .
-0.002
305.28
1. 738s
BI-214
4481. 17
1120.29
39 .
10 .
0 . 006
93 . 98
1.740s
Sc-46
4482.22
1120.55
47 .
8 .
0 . 004
126.94
1.740s
Ta-182
4485 . 22
1121.30
38 .
10 .
0 . 006
88 . 56
1.741s
CO-6 0
4692.97
1173.24
9 .
3 .
0 . 001
220.66
1.770s
Ta-182
4756.23
1189.05
15 .
1.
0 . 001
857.32
1.779s
Ta-182
4885.67
1221.41
5 .
14 .
0 . 008
46 . 98
1.797s
Co - 56
4953.16
1238.28
11.
19 .
0 . 011
44 . 63
1.806s
NA-22
5098.16
1274.53
5 .
6 .
0 . 004
64 . 98
1. 826s
AG-110M
5537.25
1384 .30
16 .
-7 .
-0.004
135.27
1.884s
EU-152
5632 . 07
1408.00
5 .
2 .
0 . 001
324 .35
1.896s
K-40
5844.43
1461.09
2 .
213 .
0 .118
6 . 93
1.357s
SB-124
6764.03
1690.98
11.
-6 .
-0.004
130.84
2 . 034s
BI-214
7058.07
1764.49
8 .
20 .
0 . 011
30.32
2 . 067
Co - 56
7085.51
1771.35
20 .
0 .
0 . 000
1000 . 00
2.070s
y-88
7344 .36
1836.06
0 .
0 .
0 . 000
1000.00
2.098s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***¦>
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE-7 C 9.4760E-01 5.31E+01
477.60 9.476E-01 ?( 9.714E+00 2.88E+02 1.05E+01 G
NA-22 C 5.0854E-01 9.50E+02
1274.53 5.085E-01 ?( 1.079E+00 6.50E+01 9.99E+01 G
K-40 N 1.7973E+02 4.66E+11
1460.83 1.797E+02 (P 8.115E+00 6.93E+00 1.07E+01 G
Sc-46 F 3.9666E-01 8.38E+01
889.28 2.230E-01 ?(P 2.204E+00 2.83E+02 1.00E+02 G
1120.55 5.704E-01 ?( 2.485E+00 1.27E+02 1.00E+02 G
CR-51 F 3.5774E+00 2.77E+01
320.08 3.577E+00 &(P 1.258E+01 1.04E+02 9.94E+00 G
(Page 10 of 21)
Page 389 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 9
TestAmerica Inc
Nuclide Ave activity
MN-54 C 3 . 0450E-01
FE-59
5 . 6143E-01
Spectrum name: 8_Gamma_2 016 0993.Anl
Energy Activity Code Peak MDA Comments
834 .85 3.045E-01 ?(
3.12E+02
7.132E-01 9.43E+01 1.00E+02 G
4.45E+01
1099.25 5.614E-01 &(P 2.627E+00 1.96E+02 5.65E+01 G
1291.60-1.250E-01 % 3.361E+00 1.12E+03 4.32E+01 G
Co - 56
1.0107E+00
7.73E+01
846.77-1.427E-02 &(P 1.147E+00 2.63E+03 9.99E+01 G
1238.28 2.285E+00 ?( 2.119E+00 4.46E+01 6.61E+01 G
1037.84 2.301E+00 ?(P 6.313E+00 1.12E+02 1.41E+01 G
1771.35 0.000E+00
1.617E+01 1.00E+03 1.55E+01 A
CO - 57
-2 . 7359E-02
122 . 06-3.171E-01 ?(
136 .47 2.295E+00 ?(
2.72E+02
1.167E+00 1.10E+02 8.56E+01 G
1.191E+01 1.55E+02 1.07E+01 G
CO - 58
CO-6 0
¦5 . 9154E-01
1.1517E-01
110.78-5.915E-01 ?(
7.09E+01
1.748E+00 8.75E+01 9.95E+01 G
1.93E+03
1332.50 3.294E-02 %(P 1.656E+00 1.98E+03 1.00E+02 G
1173.24 1.975E-01 ?(P 1.216E+00 2.21E+02 9.99E+01 G
ZN-65
¦5.1232E-01
1115 . 55-5.123E-01 ?(
2.44E+02
5.459E+00 3.05E+02 5.06E+01 G
NB-94
1. 6233E-01
702.63 1.316E-01 ?(
7.41E+06
1.244E+00 3.89E+02 9.79E+01 G
'71.10 1.925E-01 &(P 1.323E+00 1.92E+02 9.99E+01 G
ZR-95
3 . 1455E-02
756.73 3.145E-02 %(
724.20 0.000E+00 &
6.40E+01
2.156E+00 2.75E+03 5.45E+01 G
4.626E+00 1.00E+03 4.42E+01 G
RU-103
1. 8644E-01
497.05 1.864E-01 ?(
610.30 0.000E+00 -
3.93E+01
1.134E+00 2.45E+02 9.09E+01 G
5.542E+01 1.00E+03 5.75E+00 GA
RH-106
3.4873E+00
621.92 0.000E+00 ?(
1050.36 2.569E+01 ?(
511.86 2.976E+00
3.74E+02
3.239E+01 1.00E+03 9.93E+00 G
8.983E+01 1.01E+02 1.56E+00 G
7.7 55E+00 1.39E+02 2.00E+01 GA
AG-108M
¦5 . 4211E-01
1.53E+05
433.94-5.421E-01 ?(P 1.255E+00 1.21E+02 9.05E+01 G
722.94-4.860E-02 % 2.231E+00 1.31E+03 9.08E+01 G
(Page 11 of 21)
Page 390 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Nuclide Ave activity
Env32 G800W064 7/11/2016 9:17:04 AMPage 10
Spectrum name: 8_Gamma_2 016 0993.Anl
Energy Activity Code Peak MDA Comments
614.28 0.000E+00 + 3.566E+00 1.00E+03 8.98E+01 G
AG-110M F 1.4956E-01
2.50E+02
884 . 68-6.925E-01
? (
2.842E+00
1.20E+02
7.27E+01
G
657.76 5 . 487E-01
Sc. (
6.976E-01
4.32E+01
9.46E+01
G
937.49-1.254E+00
+
4.660E+00
1.62E+02
3.44E+01
G
1384 . 30-2.478E+00
+
7.559E+00
1.35E+02
2.43E+01
G
763.94 1.201E+00
? (
6.646E+00
1.58E+02
2.23E+01
G
SN-113 F 5.8498E-01
391.69 5.850E-01 &(
1. 15E+02
2.336E+00 1.18E+02 6.40E+01 G
SB-125 I 1.0651E+00
427.88 0.000E+00 (
600.50-9.893E-01 +
635.89 1.441E+00 & (
1.01E+03
3.332E+00 1.00E+03 2.96E+01 G
1.776E+01 5.27E+02 1.79E+01 G
8.6 92E+00 1.69E+02 1.13E+01 G
463.37 3.670E+00 &(P 1.147E+01 9.26E+01 1.05E+01 G
1-131 I 3 .0116E-01
364.48 3.012E-01 &(
284 .30-3.403E+00 +
636.97 4.140E-01 %
8.02E+00
7.388E-01 9.62E+01 8.17E+01 G
1.467E+01 1.72E+02 6.14E+00 G
1.596E+01 1.05E+03 7.17E+00 G
Gd-153 F -1.2262E+00
97.50-1.226E+00 &(
103.20-1.677E+00 +
2.42E+02
6.639E+00 1.62E+02 3.00E+01 G
9.289E+00 1.66E+02 2.18E+01 G
Ga-6 8 C 4.9154E+00
1077 .40 4.915E+00 ?(
4.71E-02
4.288E+01 3.55E+02 3.30E+00 G
Tc-99m I 2.8754E-01
140.51 2.875E-01 ?(
2.51E-01
1.522E+00 1.58E+02 8.93E+01 G
BA-133 F -6.7070E-01
356 . 00-6.707E-01 ?(
302.85 0.000E+00 +
383 . 84-5 .111E+00 + P
80.99-9.401E-01 +
3.85E+03
3.712E+00 1.65E+02 6.20E+01 G
1.280E+01 1.00E+03 1.83E+01 G
1.745E+01 1.17E+02 8.94E+00 GA
5.531E+00 1.76E+02 3.41E+01 GA
CS-134 I 5.0606E-01
7.54E+02
604.71
0.000E+00
? (
3 . 240E+00
1.00E+03
9.76E+01
G
795 . 87
4.760E-01
& (
1. 276E+00
7.93E+01
8.55E+01
G
569.32
1.056E+00
(
6.985E+00
1.87E+02
1.54E+01
G
801.95
4.727E+00
? (
1.622E+01
1.00E+02
8.69E+00
G
563 .24
1.326E+00
? (P
1.189E+01
3.53E+02
8.3 5E+00
G
(Page 12 of 21)
Page 391 of 551
-------
ORTEC g v -
TestAmerica Inc
i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 11
Spectrum name: 8_Gamma_2 016 0993.Anl
Nuclide
Ave
activity
Energy
Activity
Code Peak MDA Comments
CS-137
I -
9 .3844E-01
1.10E+04
661. 66
-9.384E-01
? (P
1. 983E+00
8.33E+01 8.52E+01
G
CE-139
F -
3 . 8222E-01
1.38E+02
165 . 85
-3.822E-01
? (
1.184E+00
9.26E+01 7.99E+01
G
Ba-140
I
9 . 0395E-01
1.28E+01
537.26
9.337E-01
&( P
3 .108E+00
1.32E+02 2.44E+01
G
162.66
7.872E-01
? (
1. 447E+01
5.35E+02 6.22E+00
G
304.85
0.000E+00
-
5 . 497E+01
1.00E+03 4.29E+00
G
La-140
I
1. 8636E-01
1.28E+01
1596.21
-2.655E-02
% (P
7 . 522E-01
5.68E+03 9.54E+01
G
487.02
6 .328E-01
? (
2 . 608E+00
1.20E+02 4.55E+01
G
328.76
-1.894E+00
&
9 . 599E+00
1.51E+02 2.03E+01
G
815.77
-1. 065E+00
+
8.3 95E+00
2.26E+02 2.33E+01
G
CE-141
I -
7 . 033IE-01
3.25E+01
145.44
-7 . 033E-01
? (
3.432E+00
1.46E+02 4.82E+01
G
CE-144
I
2.1857E+00
2.85E+02
133.54
2.186E+00
? (
1.082E+01
1.47E+02 1.11E+01
G
PM-144
C
1.1303E-01
3.63E+02
696.54
1.13 0E-01
? (
1.107E+00
3.98E+02 9.90E+01
G
618.06
0.000E+00
&
3.249E+00
1.00E+03 9.91E+01
G
EU-152
F
2.1804E+00
4.94E+03
344.29
1.454E+00
? (
6.278E+00
1.28E+02 2.65E+01
G
1112.07
-5.454E+00
+
2.177E+01
1.17E+02 1.36E+01
G
121.78
-1.089E+00
+
3.326E+00
9.15E+01 2.86E+01
G
778.92
-2.984E+00
+
1.026E+01
1.45E+02 1.29E+01
G
964.11
3.498E+00
? (
1.586E+01
1.32E+02 1.46E+01
G
244.69
2.167E-01
o.
"o
2.442E+01
3.32E+03 7.58E+00
G
1408.00
6.925E-01
7
5.597E+00
3.24E+02 2.10E+01
GA
EU-154
I
8.5815E-01
3.14E+03
873.23
-3.026E+00
? (P
1.3 01E+01
1.00E+02 1.23E+01
G
123.10
3.291E-01
+
2.312E+00
2.07E+02 4.08E+01
G
1274.54
7.240E-02
o.
"o
4.240E+00
1.53E+03 3.52E+01
G
723 .36
0.000E+00
+
1.009E+01
1.00E+03 2.02E+01
G
1004.77
3.504E+00
& (
1.555E+01
1.30E+02 1.80E+01
G
996 .33
-8.686E+00
+
2.428E+01
8.34E+01 1.06E+01
G
EU-155
I -
1.723 5E+00
1.81E+03
105.31
-1.723E+00
? (
9.779E+00
1.70E+02 2.12E+01
G
86 . 54-1.240E+00 +
7.246E+00 1.75E+02 3.07E+01 G
(Page 13 of 21)
Page 392 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 12
TestAmerica Inc
Nuclide Ave activity
HF-181 F 7. 8817E-01
Spectrum name: 8_Gamma_2 016 0993.Anl
Energy Activity Code Peak MDA Comments
482.00 3.537E-01 ?(
133.02 5.588E-01 ?(
345.83 2.449E+00 & (
136.30 4.187E+00 ?(
4.24E+01
1.329E+00 1.10E+02 8.05E+01 G
2.693E+00 1.44E+02 4.33E+01 G
1.134E+01 1.37E+02 1.51E+01 G
2.121E+01 1.51E+02 5.85E+00 G
Ta-182
2.9181E+00
1121.30 2.154E+00 ? (
1221.41 3.906E+00 ? (
1189.05 4.655E-01 &
1.14E+02
6.447E+00 8.86E+01 3.49E+01 G
3.850E+00 4.70E+01 2.70E+01 G
9.662E+00 8.57E+02 1.62E+01 G
Hg-203
-4.9293E-01
279.20-4.929E-01 ?(
4.66E+01
1.378E+00 8.36E+01 8.15E+01
G
TL-208
pm-146
N
3 . 7314E+00
-4 . 9850E-02
583.02 3 . 760E+00
6.98E+02
(P 7.462E-01 1.31E+01 8.45E+01
277.28 6.257E+00 + P 6.201E+00 3.84E+01 6.31E+00
860.56 3.534E+00 ?( 7.812E+00 9.19E+01 1.24E+01
747 . 16-4.985E-02 %(
735 . 72-2.751E+00 +
2.02E+03
3.772E+00 3.08E+03 3.40E+01
6.957E+00 1.09E+02 2.25E+01
453.88 4.338E-02 & P 1.491E+00 1.36E+03 6.50E+01
y-
1. 0524E-01
1.07E+02
898.04 1.052E-01 ?(P 1.074E+00 3.98E+02 9.37E+01 G
1836.06 0.000E+00 - 8.180E-01 1.00E+03 9.92E+01 G
Cd-113m
Cd-109
Cf-251
-6 . 5112E+03
¦9.9784E+00
1.3224E+00
263 . 70-6.511E+03 ?(
88 . 04-9.978E+00 ?(
176.60 1. 322E+00 ?(
227.00 1.546E+00 &
5.33E+03
1.914E+04 8.78E+01 6.00E-03
4.53E+02
5.611E+01 1.69E+02 3.79E+00
3.28E+05
3.832E+00 1.12E+02 1.70E+01
1.340E+01 3.44E+02 6.30E+00
K
G
G
GA
Cf-249
¦5.7452E-01
387.95-5.745E-01 ?(
333 . 44-2.514E+00 +
1.28E+05
2.526E+00 1.30E+02 6.60E+01 G
1.232E+01 1.46E+02 1.55E+01 G
Sn-126
1. 8278E+00
87.57-1.011E+00 +
64.28 1.828E+00 (
86 . 94-4.204E+00 +
3.65E+07
5.7 57E+00 1.71E+02 3.75E+01 GA
1.668E+01 2.71E+02 9.70E+00 G
2.426E+01 1.73E+02 9.04E+00 GA
(Page 14 of 21)
Page 393 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 13
TestAmerica Inc
Nuclide Ave activity
PB-210 N -1. 7348E+01
PB-212 N 8 .4274E+00
Spectrum name: 8_Gamma_2 016 0993.Anl
Energy Activity Code Peak MDA Comments
8.14E+03
46.54-1.735E+01 (P 6.244E+01 5.55E+01 4.25E+00 G
6.98E+02
238.63 8.427E+00 (P 1.419E+00 8.81E+00 4.33E+01 G
300.03 1.963E+01 + 1.969E+01 3.35E+01 3.28E+00 GA
PB-214
N
1. 5479E+01
5 . 84E+05
351.93 1.549E+01 (P 1.941E+00 8.57E+00 3.76E+01 G
295.09 1.546E+01 ( 3.053E+00 1.04E+01 1.93E+01 G
242.00 1.569E+01 8.452E+00 1.99E+01 7.43E+00 GA
BI-207
¦1. 1910E-01
1.18E+04
569. 70-1.191E-01 &(P 1.223E+00 3.48E+02 9.77E+01 G
1063 . 66-6.513E-01 + P 2.072E+00 8.52E+01 7.45E+01 G
BI-212
N
¦9.0196E+00
6.98E+02
727.17-9.020E+00 ?(P 2.991E+01 1.06E+02 7.55E+00 G
785.42-2.485E+01 + 1.134E+02 1.91E+02 1.28E+00 GA
BI-214
N
1.1855E+01
5.84E+05
609.31 1.124E+01 (P 2.158E+00 1.16E+01 4.61E+01 G
1120.29 4.741E+00 - P 1.510E+01 9.40E+01 1.51E+01 G
1764.49 1.369E+01 ?( 1.106E+01 3.03E+01 1.54E+01 G
BI-210M T
¦8 . 4715E-01
265.83-8.471E-01 ?(
304.90 0.000E+00 +
1.10E+09
2.506E+00 8.85E+01 5.00E+01 G
8.423E+00 1.00E+03 2.80E+01 G
AC-228
N
8.3243E+00
911.07 5.041E+00 ?(
968.97 1.378E+01 (
338.32 3 . 293E+00 -
93.35-6.675E+00 -
2.10E+03
4.733E+00 4.28E+01 2.90E+01 G
2.6 72E+00 1.62E+01 1.75E+01 G
1.578E+01 1.42E+02 1.20E+01 G
3.593E+01 1.61E+02 5.56E+00 XA
TH-227
N
6 . 6634E+00
50.14 6.663E+00 &(
256 . 24-4.280E+00 -
7.95E+03
2.361E+01 1.06E+02 8.00E+00 G
1.258E+01 1.18E+02 7.00E+00 G
TH-229
TH-234
N 2 . 5386E+00
N 1.0762E+01
193.51-3.261E+00 &(
210.85 1.107E+01 &(
2.68E+06
1.887E+01 2.22E+02 4.40E+00 G
2.794E+01 1.02E+02 2.99E+00 G
1.63E+12
63.29 9.270E+00 (P 2.284E+01 8.36E+01 3.81E+00 G
92.59 1.178E+01 (P 1.441E+01 3.84E+01 5.58E+00 G
(Page 15 of 21)
Page 394 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Nuclide Ave activity
PA-231 N 6.3 015E+00
Env32 G800W064 7/11/2016 9:17:04 AMPage 14
Spectrum name: 8_Gamma_2 016 0993.Anl
Energy
Activity Code Peak MDA Comments
302.65 0.000E+00 ?(
300.07 1. 368E+01 @(
1.20E+07
8.142E+01 1.00E+03 2.88E+00 G
9.262E+01 2.01E+02 2.46E+00 G
PA-233
1. 9553E-01
312 . 01-2.986E-02
300.18 1.504E+00
7.82E+08
(P 6.676E+00 1.57E+03 3.60E+01 G
( 3.740E+01 7.35E+02 6.20E+00 G
PA-2 3 4
N
1.8147E+00
131.29 4.651E-01 & (
946.02 2.314E+00 ?(
569.47 3.960E+00 (
883.24-7.580E+00 +
880.53 7.642E+00 ?
1.63E+12
6.385E+00 4.05E+02 1.80E+01 G
9.6 09E+00 1.76E+02 1.34E+01 G
1.216E+01 9.01E+01 8.20E+00 G
2.214E+01 8.68E+01 9.60E+00 G
2.358E+01 9.05E+01 6.00E+00 GA
PA-234M N
¦8 . 2452E+01
1. 63E+12
1001.00-8.245E+01 &(P 3.472E+02 6.87E+01 8.37E-01 G
766.41 1.305E+02 + P 3.967E+02 8.92E+01 2.94E-01 G
U-235
N
-3 . 8235E+00
143 . 79-3.823E+00
205.33 6.070E-01 % P
163.38-9.965E-01 + P
2.57E+11
(P 1.481E+01 6.43E+01 1.10E+01 G
1.664E+01 1.03E+03 5.01E+00 G
1.816E+01 5.87E+02 5.08E+00 G
AM-241 T -1.9812E+00
Np-237 F -2.5771E+00
1.58E+05
59.54-1.981E+00 ?(P 4.833E+00 4.22E+01 3.59E+01 G
2.14E+06
86 .49-2.577E+00 &( 1.582E+01 1.84E+02 1.31E+01 G
Ir-192 F -4.7561E-01
316.49-4.756E-01 ?(
468 . 06-1.843E-01 +
308.44 0.000E+00 +
7.40E+01
1.919E+00 1.20E+02 8.70E+01 G
2.668E+00 4.14E+02 5.18E+01 G
7.497E+00 1.00E+03 3.18E+01 G
Cs-136
6 . 5162E-01
Np-239
1.5057E+00
818.50 5.152E-01 ?(
1048.07 7.065E-01 ?(
340.57 8 . 488E-01 ?(
103.70-1.523E+00 +
106.13 1.506E+00 ?(
99 . 50-2.445E+00 +
1.30E+01
1.861E+00 1.06E+02 1.00E+02 G
1.632E+00 6.95E+01 8.00E+01 G
3.925E+00 1.37E+02 4.69E+01 G
2.36E+00
8.543E+00 1.68E+02 2.40E+01 X
8.670E+00 1.73E+02 2.27E+01 G
1.340E+01 1.64E+02 1.50E+01 X
( - This peak used in the nuclide activity average.
(Page 16 of 21)
Page 395 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 15
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** £)
I S C A R D
ED ISO
TOPE P
E A K S
***********
Nuclide
Centroid
Background
Net Area
Intensity
Uncert
Activity
Energy
Counts
Counts
Cts/Sec
1 Sigma %
PB-210
46 . 54
399 .
-27 .
-0.015
55 . 50
-1.735E+01
TH-227
50 .14
255 .
22 .
0 . 012
105 . 94
6 . 663E+00
AM-2 41
59 . 54
351.
-37 .
-0.020
42 .22
-1.981E+00
BA-133
80 . 99
741.
-22 .
-0 . 012
176.13
-9.401E-01
Np-237
86 .49
968 .
-24 .
-0.013
184.02
-2.577E+00
EU-155
86 . 54
1119 .
-27 .
-0.015
175.32
-1.240E+00
Cd-109
88 . 04
1037 .
-27 .
-0.015
168.71
-9.978E+00
Nd-147
91.10
1010 .
-27 .
-0.015
166.15
-1.321E+00
Gd-153
97 . 50
975 .
-27 .
-0.015
162 .45
-1.226E+00
Np-239
99 . 50
1002 .
-27 .
-0.015
164.45
-2.445E+00
Gd-153
103.20
1029 .
-27 .
-0.015
166.19
-1.677E+00
Np-239
103 . 70
1057 .
-27 .
-0.015
168 .31
-1.523E+00
EU-155
105.31
1084 .
-28 .
-0.015
170 .27
-1.723E+00
Np-239
106.13
976 .
26 .
0 . 014
172 .69
1.506E+00
EU-152
121.78
214 .
-23 .
-0 . 013
91.49
-1.089E+00
CO - 57
122.06
238 .
-20 .
-0.011
109 . 92
-3.171E-01
EU-154
123.10
210 .
10 .
0 . 006
207.36
3.291E-01
PA-2 3 4
131.29
304 .
6 .
0 . 003
405.17
4.651E-01
HF-181
133.02
310 .
18 .
0 . 010
143.58
5.588E-01
(Page 17 of 21)
Page 396 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:04 AMPage 16
Spectrum name: 8_Gamma_2 016 0993.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
CE-144
133.54
328
18 .
0 . 010
147.43
HF-181
136 .30
346
18 .
0 . 010
150.94
CO - 57
136.47
363
18 .
0 . 010
154 . 63
Tc-99m
140.51
381
18 .
0 . 010
157 . 81
U-235
143.79
569
-29 .
-0.016
64 .29
CE-141
145.44
584
-24 .
-0.013
146.08
Ba-140
162.66
142
3 .
0 . 002
534.83
U-235
163.38
148
-3 .
-0 . 002
587.07
CE-13 9
165.85
161
-20 .
-0.011
92 .60
Cf-251
176.60
66
14 .
0 . 008
111. 80
TH-229
193.51
95
-8 .
-0.005
221. 92
TH-229
210 . 85
84
18 .
0 . 010
102 . 44
Cf-251
227.00
76
5 .
0 . 003
344 .29
TH -7.7.1
256.24
68
-14 .
-0.008
118.38
Cd-113m
263.70
114
-18 .
-0.010
87 . 84
BI-210M
265 . 83
135
-19 .
-0.011
88.48
Hg-203
279.20
99
-18 .
-0.010
CM
\o
ro
00
1-131
284 .30
60
-9 .
-0.005
171.77
PA-2 31
300.07
384
14 .
0 . 008
201.36
PA-233
300.18
398
4 .
0 . 002
734.96
Ir-192
316.49
185
-16 .
-0.009
119.97
CR-51
320.08
99
14 .
0 . 008
104 .32
La-140
328.76
240
-15 .
-0.008
150.53
Cf-249
333.44
225
-15 .
-0.008
145.55
Cs-136
340 . 57
201
15 .
0 . 008
137.26
EU-152
344 .29
160
14 .
0 . 008
128.04
HF-181
345.83
168
14 .
0 . 008
137.26
BA-133
356.00
297
-15 .
-0.008
164.51
1-131
364 .48
16
9 .
0 . 005
96 .16
BA-133
383 . 84
116
-16 .
-0.009
117.31
Cf-249
387 . 95
131
-13 .
-0.007
130.03
SN-113
391.69
103
13 .
0 . 007
118.07
AG-108M
433.94
48
-15 .
-0.008
120.70
SB-125
463 .37
48
11.
0 . 006
92 . 56
Ir-192
468.06
64
-3 .
-0 . 002
413 . 86
BE - 7
477 .60
32
3 .
0 . 002
288.30
HF-181
482 . 00
35
8 .
0 . 004
109 .65
La-140
487.02
43
8 .
0 . 004
120.16
RU-103
497.05
30
5 .
0 . 003
245.31
RH-106
511. 86
70
16 .
0 . 009
138 . 96
Ba-140
537.26
13
6 .
0 . 003
132 .10
CS-134
563.24
22
3 .
0 . 002
352.79
CS-134
569.32
26
4 .
0 . 002
187.08
PA-2 3 4
569.47
22
8 .
0 . 004
90 .14
BI-207
569.70
33
-3 .
-0 . 002
347 . 91
SB-125
600 . 50
239
-4 .
-0.002
527 . 18
SB-125
635.89
17
4 .
0 . 002
168.86
AG-110M
657.76
6
11.
0 . 006
43 .16
4 .
2 .
2 .
-3 .
-7 .
7 .
1.
-3 .
1.
1.
-4 .
-6 .
-3 .
1.
1.
Uncert FWHM
2.186E+00
. 187E+00
. 295E+00
. 875E-01
. 823E+00 P
. 033E-01
. 872E-01
-9.965E-01 P
-3 . 822E-01
. 322E+00
. 261E+00
. 107E+01
. 546E+00
. 280E+00
. 511E+03
-8.471E-01
-4.929E-01
. 403E+00
. 368E+01
. 504E+00
-4 . 756E-01
3.577E+00 P
-1.894E+00
-2.514E+00
8.488E-01
. 454E+00
. 449E+00
-6.707E-01
3.012E-01
111E+00 P
745E-01
850E-01
-5.421E-01 P
3.670E+00 P
. 843E-01
. 476E-01
. 537E-01
. 328E-01
. 864E-01
. 976E+00
. 337E-01 P
. 326E+00 P
. 056E+00
. 960E+00
-1.191E-01 P
-9.893E-01
. 441E+00
. 487E-01
1.
2 .
¦5 .
¦5 .
5 .
-1.
9 .
3 .
6 .
1.
2 .
9 .
1.
1.
3 .
1.
5 .
(Page 18 of 21)
Page 397 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 17
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
Nuclide
Channel
Energy Background Net
area 1
Cnts/sec
Uncert FWHM
CS-137
661. 66
53
-17 .
-0.010
83 .34
-9.384E-01 P
PM-144
696 . 54
19
2 .
0 . 001
398.21
1.13 0E-01
NB-94
702 . 63
23
3 .
0 . 001
389 .11
1.316E-01
SB-124
722.79
54
-14 .
-0.008
79 . 90
-6.302E+00
BI-212
727.17
84
-14 .
-0.008
106.10
-9.020E+00 P
pm-146
735 . 72
37
-12 .
-0.007
108 . 88
-2 . 751E+00
AG-110M
763.94
31
5 .
0 . 003
158.23
1. 201E+00
PA-234M
766.41
18
7 .
0 . 004
89.20
1.3 05E+02 P
EU-152
778.92
23
-7 .
-0 . 004
144.53
-2 . 984E+00
BI-212
785 . 42
28
-6 .
-0.003
191.49
-2 . 485E+01
CS-134
795.87
14
8 .
0 . 004
79.30
4 . 760E-01
CS-134
801. 95
25
8 .
0 . 004
100.15
4 . 727E+00
CO - 58
810.78
39
-11.
-0.006
87 . 54
-5.915E-01
La-140
815.77
50
-5 .
-0.003
226.07
-1.065E+00
Cs-136
818.50
45
9 .
0 . 005
106.03
5.152E-01
MN-54
834.85
5
5 .
0 . 003
94 .29
3.045E-01
NB-94
871.10
19
3 .
0 . 002
192 . 05
1.925E-01 P
EU-154
873 .23
28
-6 .
-0 . 004
100.43
-3.026E+00 P
PA-2 3 4
880.53
21
8 .
0 . 004
90.49
7.642E+00
PA-2 3 4
883 .24
52
-12 .
-0.007
86 . 81
-7.580E+00
AG-110M
884 .68
49
-9 .
-0.005
119 . 92
-6.925E-01
Sc-46
889.28
56
4 .
0 . 002
283.11
2.23 0E-01 P
y-88
898.04
9
2 .
0 . 001
398 .22
1.052E-01 P
AG-110M
937.49
25
-7 .
-0 . 004
161.52
-1.254E+00
PA-2 3 4
946.02
15
5 .
0 . 003
176.07
2.314E+00
EU-152
964.11
53
8 .
0 . 005
132.17
3.498E+00
EU-154
996.33
63
-14 .
-0.008
83 .36
-8.686E+00
PA-234M
1001.00
81
-11.
-0.006
68 . 73
-8.245E+01 P
EU-154
1004.77
74
10 .
0 . 005
130.17
3.504E+00
Co - 56
1037.84
5
5 .
0 . 003
111.96
2.3 01E+00 P
Cs-136
1048.07
13
8 .
0 . 005
69 . 50
7.065E-01
RH-106
1050.36
15
6 .
0 . 003
100.98
2.569E+01
BI-207
1063.66
18
-7 .
-0 . 004
85.22
-6.513E-01 P
Ga-6 8
1077.40
10
2 .
0 . 001
354.73
4.915E+00
FE-59
1099.25
16
4 .
0 . 002
196.36
5.614E-01 P
EU-152
1112.07
70
-10 .
-0.006
117.43
-5.454E+00
ZN-65
1115.55
60
-4 .
-0.002
305.28
-5.123E-01
Sc-46
1120.55
47
8 .
0 . 004
126.94
5.704E-01
Co - 56
1238.28
11
19 .
0 . 011
44 . 63
2.285E+00
NA-22
1274.53
5
6 .
0 . 004
64 . 98
5.085E-01
AG-110M
1384 .30
16
-7 .
-0 . 004
135.27
-2.478E+00
EU-152
1408.00
5
2 .
0 . 001
324.35
6.925E-01
SB-124
1690.98
11
-6 .
-0 . 004
130.84
-1.3 57E+00
P - Peakbackground subtraction
(Page 19 of 21)
Page 398 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:04 AMPage 18
TestAmerica Inc Spectrum name: 8_Gamma_2 016 0993.Anl
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#A
9 . 4760E-01
9.4760E-01
2.883E+02%
9.71E+00
NA-22
#A
5 . 0854E-01
5.0854E-01
6.498E+01%
1.08E+00
K-40
1. 7973E+02
1.7973E+02
6.929E+00%
8.12E+00
Sc-46
#A
3.9666E-01
3.9666E-01
1.269E+02%
2.20E+00
CR-51
#A
3.5774E+00
3.5774E+00
1.043E+02 %
1.26E+01
MN-54
#A
3 . 0450E-01
3.0450E-01
9.429E+01%
7.13E-01
FE-59
#A
5 . 6143E-01
5.6143E-01
1.964E+02 %
2.63E+00
Co - 56
#A
1.0107E+00
1.0107E+00
4.463E+01%
1.15E+00
CO - 57
#A
-2.7359E-02
-2.7359E-02
9.486E+01%
1.17E+00
CO - 58
#A
-5 . 9154E-01
-5.9154E-01
8.754E+01%
1.75E+00
CO-6 0
#A
1.1517E-01
1.1517E-01
2.207E+02%
1.66E+00
ZN-65
#A
-5 . 1232E-01
-5.1232E-01
3.053E+02 %
5.46E+00
NB-94
#A
1. 6233E-01
1.6233E-01
1.921E+02 %
1.24E+00
ZR-95
#A
3 . 1455E-02
3.1455E-02
2.755E+03 %
2.16E+00
NB-95
#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.60E+00
RU-103
#A
1. 8644E-01
1.8644E-01
2.453E+02%
1.13E+00
RH-106
#A
3 .4873E+00
3.4873E+00
1.010E+02 %
3.24E+01
AG-108M#A
-5.4211E-01
-5.4211E-01
1.207E+02%
1.25E+00
AG-110M#A
1. 4956E-01
1.4956E-01
4.316E+01%
2.84E+00
SN-113
#A
5 . 8498E-01
5.8498E-01
1.181E+02%
2.34E+00
SB-124
#A
0.0000E+00
0.0000E+00
1.000E+03 %
3.21E+00
SB-125
#A
1.0651E+00
1.0651E+00
9.256E+01%
3.33E+00
1-131
#A
3.0116E-01
3.0116E-01
9.616E+01%
7.39E-01
Gd-153
#A
-1.2262E+00
-1.2262E+00
1.62 5E+02 %
6.64E+00
Ga-6 8
#A
4.8978E+00
4.9154E+00
3.54 7E+02 %
4.29E+01
Tc-99m
#A
2 . 8735E-01
2.8754E-01
1.578E+02%
1.52E+00
BA-133
#A
-6.7070E-01
-6.7070E-01
1.64 5E+02 %
3.71E+00
CS-134
#A
5.0606E-01
5.0606E-01
7.930E+01%
3.24E+00
CS-137
#A
-9 . 3844E-01
- 9.3 844E-01
8.334E+01%
1.98E+00
CE-139
#A
-3 . 8222E-01
-3.8222E-01
9 .260E+01%
1.18E+00
Ba-140
#A
9 . 0393E-01
9.0395E-01
1.321E+02%
3.11E+00
La-140
#A
1. 8636E-01
1.8636E-01
1. 2 02E+02 %
7.52E-01
CE-141
#A
-7.033 IE-01
-7.033 IE-01
1. 461E+02%
3.43E+00
CE-144
#A
2.1857E+00
2.1857E+00
1.474E+02%
1.08E+01
PM-144
#A
1.1303E-01
1.1303E-01
3.982E+02 %
1.11E+00
EU-152
#A
2.1804E+00
2.1804E+00
9.201E+01%
6.28E+00
EU-154
#A
8.5815E-01
8.5815E-01
8.220E+01%
1.30E+01
EU-155
#A
-1.723 5E+00
-1.723 5E+00
1.703E+02 %
9.78E+00
HF-181
#A
7.8817E-01
7.8817E-01
6.813E+01%
1.33E+00
Ta-182
#A
2.9181E+00
2.9181E+00
4.698E+01%
6.45E+00
Hg-203
#A
-4.9293E-01
-4.9293E-01
8.362E+01%
1.38E+00
TL-208
3.7314E+00
3.7314E+00
1.315E+01%
7.46E-01
pm-146
#A
-4.9850E-02
-4.9850E-02
3 . 079E+03 %
3.77E+00
(Page 2 0 of 21)
Page 399 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 9:
17:04 AMPage 19
TestAmerica
Inc
Spectrum
name: 8 Gamma
20160993.Anl
y-88
#A
1. 0524E-01
1. 0524E-01
3.982E+02 %
1.07E+00
Cd-113m#A
-6 . 5112E+03
-6 . 5112E+03
8.784E+01%
1.91E+04
Cd-109
#A
-9.9784E+00
-9 . 9784E+00
1.687E+02%
5.61E+01
Cf-251
#A
1. 3224E+00
1. 3224E+00
1.118E+02 %
3.83E+00
Cf-249
#A
-5 . 7452E-01
-5 . 7452E-01
1.3 00E+02 %
2.53E+00
Sn-126
A
1. 8278E+00
1.8278E+00
2.706E+02 %
1.67E+01
PB-210
#A
-1. 7348E+01
-1.7348E+01
5.550E+01%
6.24E+01
PB-212
8 . 4274E+00
8.4274E+00
8.815E+00%
1.42E+00
PB-214
1. 5479E+01
1.5479E+01
6.747E+00%
1.94E+00
BI-207
#A
-1.1910E-01
-1.1910E-01
3.479E+02%
1.22E+00
BI-212
#A
-9 . 0195E+00
-9 . 0196E+00
1. 061E+02%
2.99E+01
BI-214
1.1855E+01
1.1855E+01
1. 155E+01%
2.16E+00
BI-210M#A
-8.4715E-01
-8.4715E-01
8.848E+01%
2.51E+00
AC-228
8.3243E+00
8.3243E+00
1.622E+01%
4.73E+00
TH-227
#A
6.6634E+00
6.6634E+00
1.059E+02 %
2.36E+01
TH-229
#A
2.53 86E+00
2.53 86E+00
1.024E+02 %
1.89E+01
TH-234
A
1.0762E+01
1.0762E+01
3.845E+01%
2.28E+01
PA-2 31
#A
6.3 015E+00
6.3 015E+00
2.014E+02 %
8.14E+01
PA-233
#A
1. 9553E-01
1.9553E-01
7.3 50E+02 %
6.68E+00
PA-2 3 4
#A
1. 8147E+00
1.8147E+00
9 . 014E+01%
6.3 8E+00
PA-234M#A
-8 . 2452E+01
-8.2452E+01
6 . 873E+01%
3.47E+02
U-235
#A
-3 . 8235E+00
-3.823 5E+00
6.429E+01%
1.48E+01
AM-2 41
#A
-1.9812E+00
-1.9812E+00
4.222E+01%
4.83E+00
Np-237
#A
-2 . 5771E+00
-2.5771E+00
1.84 0E+02 %
1.58E+01
Ir-192
#A
-4 . 7561E-01
-4.7561E-01
1.200E+02%
1.92E+00
Cs-136
#A
6 . 5161E-01
6.5162E-01
6.228E+01%
1.86E+00
Np-239
#A
1.5056E+00
1.5057E+00
1.72 7E+02 %
8.67E+00
Nd-147
#A
0 . 0000E+00
0.0000E+00
1.000E+03 %
7.81E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.5 to 2000.0 keV) 2.275E+02 Bq/Sample
Total Decayed Activity ( 37.5 to 2000.0 keV) 2.2754265E+02 Bq/Sample
(Page 21 of 21)
Page 400 of 551
-------
257060_Gamma_160-17814-A-3-B. 8_Gamma_20160993.spc.
1.0e4-
1.0e3-
Tl
£B
CQ
ffce2-
cn
en
1.0e1
1.0e0
O) =3
< LU
fll
o
CM
C\i
m
500
1000
1500
2000
2500
3000
3500 4000
Channels
4500
5000
5500
6000
6500
7000
7500
8000
-------
Test America St. Louis Spectrum ID: 5_Gamma_2 0161262
Sample Description: 257060_Gamma_160-17814-A-4-B
Detector: Detector # 5
Batch ID: 257060
Work Order Number: Gamma
Lot Number: 160-17814-A-4-B
Decay to Time: 7/11/2016 08:45 Live Time: 1800 sec
Acquisition Time: 7/11/2016 08:46:11 Real Time: 1808 sec
Analysis Time: 7/11/2016 09:17 Dead Time: 0.44 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
5_Soil_TunaCan.Clb
5_Soil_TunaCan_90099_032612
3/27/2012 17:20
2/28/2012 19:35
Client_Long_Revll.lib
5 2016-07-10 0601.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bq/Sample % Bq/Sample Bq/Sample Bq/Sample
BE - 7
1.162E+01
25 . 5
2 . 960E+00
3.019E+00
7.731E+00
NA-22
-3 . 884E-01
150 . 0
5.826E-01
5.829E-01
2.073E+00
K-40
1. 432E+02
8 . 7
1.241E+01
1.441E+01
1.187E+01
Sc-46
-6 . 797E-02
87 . 4
5.939E-02
5.950E-02
2.886E+00
CR-51
-4 . 521E+00
105 . 0
4.748E+00
4.754E+00
1.599E+01
MN-54
2 . 611E-01
132 . 7
3.466E-01
3.468E-01
9.045E-01
FE-59
7.809E-01
41. 5
3.23 7E-01
3.261E-01
2.107E+00
Co - 56
8.457E-01
68 . 6
5.798E-01
5.814E-01
1.167E+00
CO - 57
2.046E-01
128 . 5
2.63 0E-01
2.632E-01
8.922E-01
CO - 58
-7.801E-01
41. 4
3.228E-01
3.253E-01
2.345E+00
CO-6 0
-4.329E-01
61.4
2.659E-01
2.668E-01
2.169E+00
ZN-65
0.000E+00
1.#INF
5.422E-01
5.422E-01
5.942E+00
NB-94
-6 . 013E-02
742 . 7
4.466E-01
4.466E-01
1.173E+00
ZR-95
-1.035E+00
53 .2
5.506E-01
5.533E-01
3.482E+00
NB-95
4 . 620E-01
149 . 4
6.902E-01
6.906E-01
2.375E+00
RU-103
-9.699E-02
443 . 5
4.301E-01
4.301E-01
1.142E+00
RH-106
2.057E+00
115.4
2.374E+00
2.376E+00
3.23 9E+01
AG-108M
3 .387E-01
140 . 1
4.747E-01
4.750E-01
8.202E-01
AG-110M
4 . 753E-01
40 . 8
1.940E-01
1.956E-01
3.620E+00
SN-113
3 . 094E-01
172 . 7
5.345E-01
5.347E-01
1.857E+00
SB-124
6.799E-01
126 . 6
8.610E-01
8.617E-01
3.3 95E+00
SB-125
1.3 55E+00
75 . 9
1.029E+00
1.031E+00
3.621E+00
1-131
8 . 692E-01
47 . 1
4.097E-01
4.122E-01
1.024E+00
Gd-153
-8 . 248E-01
100.4
8.282E-01
8.297E-01
2.783E+00
Ga-6 8
3 . 003E+00
702 . 4
2.109E+01
2.109E+01
5.23 8E+01
Tc-99m
2.511E-01
138 . 1
3.467E-01
3.470E-01
1.171E+00
BA-133
-6.125E-01
184 .3
1.129E+00
1.129E+00
3.818E+00
CS-134
7.685E-01
35 . 7
2.745E-01
2.774E-01
3.500E+00
CS-137
2.817E-01
225 . 5
6.351E-01
6.3 53E-01
2.212E+00
CE-139
2.882E-01
113 .2
3.264E-01
3.276E-01
1.103E+00
Ba-140
5 . 276E-02
2907.2
1.534E+00
1.534E+00
4.198E+00
La-140
-3 . 123E-01
78 . 9
2.465E-01
2.471E-01
2.262E+00
CE-141
4 . 367E-01
134 . 8
5.887E-01
5.891E-01
1.990E+00
(Page 1 of 21)
Page 402 of 551
-------
CE-144
1. 833E+00
132 . 8
2.43 5E+00
2.436E+00
8.232E+00
PM-144
-3 .359E-01
170.3
5.722E-01
5.725E-01
1.441E+00
EU-152
1.077E+00
107 . 5
1.158E+00
1.159E+00
5.813E+00
EU-154
-8.245E-02
100 . 8
8.310E-02
8.321E-02
1.680E+01
EU-155
-1. 218E+00
88 . 7
1.080E+00
1.082E+00
5.958E+00
HF-181
3 . 202E-01
122 .3
3.915E-01
3.918E-01
1.63 0E+00
Ta-182
1.776E+00
88.3
1.568E+00
1.570E+00
6.605E+00
Hg-203
-4.742E-01
93 . 8
4.445E-01
4.454E-01
1.495E+00
TL-208
3.346E+00
13 .2
4.43 IE-01
4.759E-01
4.3 92E-01
pm-146
6 . 322E-01
89.4
5.655E-01
5.664E-01
2.282E+00
y-88
4.049E-03
12561.2
5.086E-01
5.086E-01
1.343E+00
Cd-113m
0.000E+00
1.#INF
3.187E+03
3.187E+03
1.518E+04
Cd-109
0 . 000E+00
1.#INF
1.115E+01
1.115E+01
3.788E+01
Cf-251
2 . 527E+00
53 .2
1.344E+00
1.363E+00
3.535E+00
Cf-249
4 . 237E-01
124 .2
5.262E-01
5.267E-01
1.808E+00
Sn-126
1. 714E+00
221. 5
3.798E+00
3.799E+00
1.292E+01
PB-210
3.079E+01
35 . 8
1.103E+01
1.118E+01
2.921E+01
PB-212
8.762E+00
9.3
8.146E-01
9.924E-01
1.543E+00
PB-214
1.366E+01
7 . 8
1.066E+00
1.281E+00
2.218E+00
BI-207
3.196E-01
00
o
I-1
2.560E-01
2.565E-01
8.692E-01
BI-212
-5 .111E+00
152 . 8
7.809E+00
7.813E+00
2.410E+01
BI-214
1.198E+01
10 . 9
1.3 03E+00
1.444E+00
1.921E+00
BI-210M
-2 . 881E-01
230.3
6.637E-01
6.639E-01
2.291E+00
AC-228
7 . 746E+00
17 . 0
1.319E+00
1.377E+00
2.988E+00
TH -7.7.1
9 . 607E+00
47 . 2
4.539E+00
4.569E+00
1.244E+01
TH-229
3 . 528E+00
159.3
5.618E+00
5.625E+00
1.822E+01
TH-234
-9.241E+00
76 .3
7.050E+00
7.067E+00
3.297E+01
PA-2 31
-1. 321E+01
139 . 8
1.847E+01
1.848E+01
6.23 9E+01
PA-233
9.098E-01
150.2
1.366E+00
1.367E+00
4.635E+00
PA-2 3 4
-1. 573E-01
129 . 6
2.039E-01
2.041E-01
5.676E+00
PA-234M
6 . 322E+01
82 . 6
5.220E+01
5.23 0E+01
2.865E+02
U-235
2 . 014E+00
132 . 0
2.657E+00
2.659E+00
8.974E+00
AM-2 41
-1. 064E+00
79.2
8.423E-01
8.441E-01
3.289E+00
Np-237
0.000E+00
1.#INF
3.895E+00
3.895E+00
1.3 04E+01
Ir-192
-4.595E-01
102 .2
4.695E-01
4.703E-01
1.584E+00
Cs-136
5.575E-01
63 . 5
3.541E-01
3.556E-01
1.705E+00
Np-239
-1.033E+00
146 . 7
1.515E+00
1.516E+00
5.099E+00
Nd-147
-3 . 583E+00
108 .3
3.881E+00
3.887E+00
9.807E+00
Total 3 . 3 53E+02
Analyst: Amanda Dick
(Page 2 of 21)
Page 403 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 1
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
Sample description
257060 Gamma 160-17814-A-4-B
Spectrum Filename: C:\User\SPC\Det5\5_Gamma_20161262.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
7/11/2016 8:46:11 AM
1800
1808
0.44 %
5
Detector system
Ge 5 SN/157
Calibration
Filename:
5 Soil TunaCan 90099 032612
5 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 7:35:48 PM
0.158 keV
0.250 keV/channel
3.911E-08 keV/channel^2
3/27/2012 5:20:37
165.85 keV
Quadratic
6 .466115E-01
( -4 .117504E
Quadratic
-2 . 462251E+01
( -9 . 664422E
PM
Uncertainty = 0.8 7
+ ( - 7 . 83 04 54E-01*Log(E) )
03 *Log(E)^2 )
Uncertainty = 1.43
+ ( 9 . 075211E+00*Log(E) )
01*Log(E)^2 )
Client_Long_Revll.lib
0 . 500
Library based
Env32 G800W064
150 ( 37.62keV )
8000 ( 2000.81keV )
1000.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+00/( 1.0000E+00*
1.0000E+00
Reg. Guide 4.16 Method
1.0000E+00)
(Page 3 of 21)
Page 404 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:07 AMPage 2
Spectrum name: 5_Gamma_2 0161262.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4 . 0000000E+00
0.000%
3
12.000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
7/11/2016 8:45:00 AM
5_2 016-07-10_06 01.PBC
7/10/2016 6:01:50 AM
total peaks alloc. 22 cutoff: 5.00E+01 '
Energy Calibration
Normalized diff: 0.1816
* * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq/Sampl
46 . 75
58 .
24.80
0 . 76
1.801E-02
46 . 54
4 .250
3.079E+01
PB210
50 .14
28 .
47.24
0 . 79
2.012E-02
50 . 14
8 . 000
PBC
-------
ORTEC g v - i
TestAmerica Inc
(3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 3
Spectrum name: 5_Gamma_2 0161262.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
143.70
13 .
131. 97
0 . 88
3.3 71E-02
143.79
10 . 960
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 4
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
pk energy
area
uncert
f whm
corr
nuclide
brnch.
act.
nuc
765.79
7 .
149.41
1.45
8 . 781E-03
765.79
99 . 790
PBC
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 5
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
This section based
on library:
Client
Long Revll.
lib
************** J
D
E N T I
F I
ED P
E A K S
U M M A
Y **************
Nuclide
Peak
Centroid
Background
Net Area
Intensity Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec
1 Sigma %
keV
PB-210
186.53
46 . 75
64 .
42 .
0 . 023
35 . 82
0 . 761
TH-227
200.11
50 .14
51.
28 .
0 . 015
47 .24
0.787s
AM-2 41
237.72
59 . 54
120 .
-17 .
-0.010
79 .17
0.797s
TH-234
252.74
63 .29
158 .
-17 .
-0 . 010
76 .30
0 . 801
Sn-126
256.71
64 .28
163 .
8 .
0 . 005
221.53
0 . 802s
BA-133
323 .61
80 . 99
187 .
-21.
-0.012
116.04
0.819s
Np-237
345 . 63
86 .49
488 .
0 .
0 . 000
165 . 72
0.825A
EU-155
345 . 84
86 . 54
371.
8 .
0 . 004
341. 89
0 . 825
Sn-126
347 . 43
86 . 94
379 .
10 .
0 . 005
151. 03
0 . 825D
Sn-126
349.95
87 . 57
329 .
27 .
0 . 015
49 . 53
0.826D
Cd-109
351.83
88 . 04
347 .
0 .
0 . 000
1000 . 00
0.826A
Nd-147
364 . 08
91.10
364 .
15 .
0 . 008
180.25
0.829s
TH-234
370.05
92 . 59
98 .
21.
0 . 011
72 .29
0.83 ID
AC-228
373.09
93 .35
402 .
-15 .
-0.008
187.96
0 . 832
Gd-153
389.70
97 . 50
120 .
-16 .
-0.009
100.41
0 . 836s
Np-239
397.71
99 . 50
123 .
14 .
0 . 008
115.41
0 . 838s
Gd-153
412.52
103.20
122 .
6 .
0 . 004
243.98
0 . 842
Np-239
414.52
103.70
108 .
11.
0 . 006
134 . 87
0 . 842s
EU-155
420.98
105.31
291.
-17 .
-0.009
88 .67
0 . 844s
Np-239
424 .25
106.13
243 .
-15 .
-0.008
146 . 70
0 . 845s
EU-152
486.88
121.78
87 .
13 .
0 . 007
107 . 53
0 . 861s
CO - 57
488 . 03
122.06
100 .
11.
0 . 006
128.54
0 . 861s
EU-154
492.18
123.10
125 .
-16 .
-0.009
94 . 52
0 . 862s
PA-2 3 4
524 . 99
131.29
176 .
-13 .
-0 . 007
146.96
0 . 871
HF-181
531. 91
133.02
150 .
14 .
0 . 008
130.33
0 . 872s
CE-144
533.97
133.54
137 .
13 .
0 . 007
132 . 81
0 . 873s
Tc-99m
561.88
140.51
163 .
13 .
0 . 007
138.12
0.880s
U-235
574.99
143.79
150 .
13 .
0 . 007
131. 97
0 . 883
CE-141
581.61
145.44
140 .
13 .
0 . 007
134 . 80
0.885s
Ba-140
650.54
162.66
132 .
-11.
-0.006
150.76
0.902s
U-235
653.42
163 .38
143 .
0 .
0 . 000
1000.00
0 . 903
CE-13 9
663 .32
165.85
102 .
13 .
0 . 007
113 .25
0.905s
Cf-251
706.34
176.60
40 .
23 .
0 . 013
53 .19
0.916s
TH-229
774.03
193.51
63 .
3 .
0 . 001
534 . 59
0.933s
U-235
821.35
205.33
71.
-9 .
-0.005
163.62
0 . 945
TH-229
843.44
210.85
70 .
10 .
0 . 005
159.25
0.950s
Cf-251
908.08
227.00
57 .
-8 .
-0.004
178 . 42
0.966s
PB-212
954.64
238 . 63
29 .
158 .
0 . 088
9.30
0.978D
PB-214
968.10
242.00
44 .
46 .
0 . 025
25.34
0.981D
EU-152
978.89
244 .69
338 .
-14 .
-0.008
186.16
0.984s
TH-227
1025.11
256 .24
44 .
5 .
0 . 003
263.21
0.995s
(Page 7 of 21)
Page 408 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
6
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
Cd-113m
1054 . 97
263.70
48 .
0 .
0 . 000
1000.00
1. 002s
BI-210M
1063.50
265 . 83
78 .
-6 .
-0 . 003
230.34
1.005s
TL-208
1109.33
277.28
46 .
-1.
-0.001
964 .37
1.016s
Hg-203
1117.00
279.20
81.
-14 .
-0.008
93 . 75
1.017s
PB-214
1182.11
295.47
13 .
101.
0 . 056
11. 84
0.893s
PB-212
1201.88
300.41
6 .
24 .
0 . 014
27.41
1.867s
PA-2 31
1200.53
300.07
183 .
-13 .
-0.007
149.45
1. 038s
PA-233
1200.97
300.18
170 .
-13 .
-0 . 007
144 . 22
1.038s
PA-2 31
1210.86
302 .65
160 .
-13 .
-0.007
139.77
1. 040
BA-133
1211.66
302.85
173 .
-12 .
-0.006
163.02
1. 040
Ba-140
1219.66
304.85
184 .
0 .
0 . 000
1000 . 00
1. 042s
BI-210M
1219.85
304.90
184 .
0 .
0 . 000
1000.00
1. 042s
Ir-192
1234.03
308 .44
184 .
0 .
0 . 000
1000 . 00
1. 046s
PA-233
1248 .32
312.01
130 .
11.
0 . 006
150.18
1. 049s
Ir-192
1266 .25
316 .49
84 .
-13 .
-0.007
102.18
1. 053s
CR-51
1280.63
320.08
112 .
-15 .
-0.008
105.01
1.057s
Cf-249
1334.08
333 .44
40 .
-1.
-0.001
895.30
1.070s
AC-228
1353.75
338 .35
10 .
28 .
0 . 016
26 .41
1. 062
Cs-136
1362 . 62
340 . 57
83 .
9 .
0 . 005
144 .30
1.077s
EU-152
1377.49
344.29
92 .
9 .
0 . 005
151.22
1.080s
HF-181
1383 . 66
345.83
121.
-11.
-0.006
141.23
1.082s
PB-214
1408.36
352 . 00
23 .
148 .
0 . 082
H1
o
I-1
00
1. 083
BA-133
1424 .36
356.00
214 .
-11.
-0.006
184 .34
1.091s
1-131
1458.32
364 .48
22 .
21.
0 . 012
47 . 14
1.099s
BA-133
1535.78
383 . 84
37 .
6 .
0 . 004
140.66
1.117s
Cf-249
1552.22
387 . 95
43 .
8 .
0 . 004
124 .21
1.121s
SN-113
1567.19
391.69
42 .
5 .
0 . 003
172 . 75
1.125s
SB-125
1711.99
427.88
28 .
-6 .
-0.004
148 .61
1.158s
AG-108M
1736.25
433.94
12 .
5 .
0 . 003
142.83
1.164s
pm-146
1816.05
453 . 88
12 .
7 .
0 . 004
102 .35
1.182s
SB-125
1854.01
463 .37
43 .
10 .
0 . 006
96 . 66
1.191
Ir-192
1872.79
468.06
67 .
-10 .
-0.006
115 .10
1.195s
BE - 7
1910.94
477.59
12 .
29 .
0 . 016
25.48
1.204s
HF-181
1928.56
482 . 00
36 .
4 .
0 . 002
206.90
1.208s
La-140
1948.65
487 . 02
32 .
-12 .
-0.007
97.28
1.212s
RU-103
1988.80
497.05
20 .
-2 .
-0 . 001
443 .47
1.221s
RH-106
2048.06
511.86
33 .
56 .
0 . 031
29.65
2,485s
Nd-147
2124.62
531.00
28 .
-10 .
-0.006
108 .32
1.252s
CS-134
2253.60
563.24
20 .
-2 .
-0.001
443 .47
1.280s
CS-134
2277.94
569.32
25 .
-2 .
-0 . 001
360.56
1.286s
PA-2 3 4
2278.54
569.47
24 .
3 .
0 . 002
213.54
1.286s
BI-207
2279.47
569.70
10 .
6 .
0 . 004
cn
o
o
00
1.286s
TL-208
2334.02
583 .34
0 .
57 .
0 . 032
13 .25
0.791s
SB-125
2402.69
600.50
168 .
8 .
0 . 004
234.15
1.313s
SB-124
2411.61
602.73
175 .
8 .
0 . 004
239.14
1.315s
BI-214
2438.42
609.43
9 .
106 .
0 . 059
H1
o
00
00
1. 544
RU-103
2441. 89
610.30
168 .
8 .
0 . 004
233.13
1.322s
AG-108M
2457.82
614.28
176 .
8 .
0 . 004
241.15
1.325s
(Page 8 of 21)
Page 409 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
7
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
PM-144
2472 . 94
618.06
184 .
0 .
0 . 000
1000.00
1.328s
RH-106
2488 .37
621.92
154 .
-3 .
-0 . 002
621.92
1.332s
SB-125
2544.26
635 . 89
10 .
7 .
0 . 004
77 . 09
1.344s
1-131
2548.61
636.97
17 .
1.
0 . 001
557.69
1.345s
AG-110M
2631.76
657.76
50 .
-12 .
-0.006
90 . 77
1.362s
CS-137
2647.36
661. 66
44 .
4 .
0 . 002
225.48
1.366
PM-144
2786.90
696.54
22 .
-6 .
-0.003
170.34
1.395s
NB-94
2811.25
702 . 63
13 .
-1.
-0.001
742.74
1.400s
SB-124
2891.88
722.79
22 .
6 .
0 . 003
126 . 62
1.417
AG-108M
2892.48
722.94
27 .
0 .
0 . 000
1000.00
1.417
EU-154
2894.16
723 .36
27 .
0 .
0 . 000
1000.00
1.418
ZR-95
2897.53
724.20
27 .
0 .
0 . 000
1000.00
1.418s
BI-212
2909.41
727.17
34 .
-6 .
-0.004
152.77
1.421s
pm-146
2943.61
735.72
18 .
4 .
0 . 002
210.42
1.428s
pm-146
2989.37
747.16
4 .
4 .
0 . 002
131.31
1.437s
ZR-95
3027.65
756.73
35 .
-9 .
-0.005
53 .23
1.445s
AG-110M
3056.50
763.94
53 .
-16 .
-0 . 009
69.41
1.451s
NB-95
3063.89
765 . 79
56 .
7 .
0 . 004
149.41
1.453s
PA-234M
3066.38
766 .41
38 .
11.
0 . 006
82 . 56
1.453s
BI-212
3142.41
785.42
33 .
-14 .
-0.008
93 . 80
1.468s
CS-134
3184.19
795 . 87
5 .
17 .
0 . 010
35 . 72
1.477s
CS-134
3208.53
801. 95
9 .
5 .
0 . 003
146.39
1.482s
CO - 58
3243.82
810.78
48 .
-12 .
-0.006
41.38
1.489s
La-140
3263.80
815.77
29 .
7 .
0 . 004
109.40
1.493s
Cs-136
3274.72
818.50
24 .
7 .
0 . 004
101. 03
1.495s
MN-54
3340.10
834.85
5 .
4 .
0 . 002
132.73
1.508s
Co - 56
3387.78
846.77
9 .
7 .
0 . 004
94 .25
1. 518s
TL-208
3442.95
860.56
19 .
5 .
0 . 003
177 . 22
1.529s
NB-94
3485 . 08
871.10
14 .
-7 .
-0.004
70 . 52
1.537s
EU-154
3493.61
873 .23
32 .
-5 .
-0.003
100 . 80
1.539s
PA-2 3 4
3522.80
880.53
41.
-11.
-0.006
90 . 01
1. 544s
PA-2 3 4
3533.64
883 .24
52 .
-2 .
-0.001
644.06
1.547s
AG-110M
3539.41
884 .68
54 .
0 .
0 . 000
1000 . 00
1.547s
Sc-46
3557.79
889.28
65 .
-9 .
-0.005
128.54
1.551s
AC-228
3645.50
911.21
4 .
31.
0 . 017
21. 53
1.051s
AG-110M
3750.60
937.49
14 .
0 .
0 . 000
1000 . 00
1.589s
PA-2 3 4
3784.70
946.02
9 .
-1.
-0.001
493.71
1.595s
AC-228
3876.48
968.97
19 .
11.
0 . 006
88 .23
1.612s
EU-154
3985.88
996 .33
30 .
4 .
0 . 002
179 . 85
1. 633s
PA-234M
4004.55
1001.00
35 .
0 .
0 . 000
1000 . 00
1.636s
Co - 56
4151.87
1037.84
5 .
6 .
0 . 003
99 . 59
1. 664s
Cs-136
4192.77
1048.07
6 .
6 .
0 . 003
72 . 66
1.671s
RH-106
4201.93
1050.36
12 .
5 .
0 . 003
115.37
1. 673s
BI-207
4255.11
1063.66
15 .
-2 .
-0.001
431. 57
1.682s
Ga-6 8
4310.04
1077.40
10 .
1.
0 . 001
702 .38
1. 692s
FE-59
4397.41
1099.25
6 .
2 .
0 . 001
236 .19
1. 708s
EU-152
4448.68
1112.07
44 .
3 .
0 . 002
337.94
1.717s
ZN-65
4462 . 56
1115.55
47 .
0 .
0 . 000
1000 . 00
1.720s
(Page 9 of 21)
Page 410 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 8
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide
Channel
Energy
Background
Net area
Cnts/sec
Uncert
FWHM
BI-214
4481. 51
1120.29
19 .
3 .
0 . 002
217.07
1. 723s
Sc-46
4482.57
1120.55
22 .
6 .
0 . 003
118.42
1. 723s
Ta-182
4485.56
1121.30
26 .
6 .
0 . 003
127 . 06
1. 724s
CO-6 0
4693.21
1173.24
16 .
5 .
0 . 003
182.44
1. 760s
Ta-182
4756.42
1189.05
10 .
4 .
0 . 002
180 . 85
1.771s
Ta-182
4885 . 79
1221.41
11.
5 .
0 . 003
145.77
1. 793
Co - 56
4953.23
1238 .28
22 .
-3 .
-0.002
311. 56
1. 804s
NA-22
5098.13
1274.53
16 .
-4 .
-0.002
150 . 00
1. 828s
EU-154
5098.19
1274.54
20 .
0 .
0 . 000
1000.00
1. 828s
FE-59
5166 .35
1291.60
0 .
6 .
0 . 003
41.45
1. 840s
CO-6 0
5329 . 85
1332.50
16 .
-4 .
-0.002
61.42
1. 866s
AG-110M
5536.88
1384 .30
0 .
6 .
0 . 003
40 . 82
1.899s
EU-152
5631.62
1408.00
5 .
3 .
0 . 001
206.16
1.914s
K-40
5843.70
1461.07
4 .
140 .
0 . 078
8 .67
1.501s
La-140
6383.73
1596 .21
11.
-7 .
-0.004
113 . 82
2 . 024s
SB-124
6762.39
1690.98
0 .
0 .
0 . 000
1000 . 00
2 . 076s
BI-214
7056.06
1764.49
2 .
20 .
0 . 011
24 . 44
2.114s
Co - 56
7083.46
1771.35
32 .
-7 .
-0.004
115.70
2.117s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***¦>
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
BE - 7
C 1.1618E+01
5.31E+01
477.60 1.162E+01 ?( 7.731E+00 2.55E+01 1.05E+01 G
NA-22 C -3.8841E-01
9.50E+02
1274.53-3.884E-01 ?( 2.073E+00 1.50E+02 9.99E+01 G
K-40
N 1.4318E+02
4.66E+11
1460.83 1.432E+02 (P 1.187E+01 8.67E+00 1.07E+01 G
Sc-46 F -6.7969E-02
8.3 8E+01
889.28-6.575E-01 ?( 2.886E+00 1.29E+02 1.00E+02 G
1120.55 5.215E-01 ?( 2.146E+00 1.18E+02 1.00E+02 G
CR-51 F -4.5213E+00
2.77E+01
320.08-4.521E+00 ?( 1.599E+01 1.05E+02 9.94E+00 G
MN-54 C 2.6112E-01
3.12E+02
834.85 2.611E-01 ?(P 9.045E-01 1.33E+02 1.00E+02 G
(Page 10 of 21)
Page 411 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 9
TestAmerica Inc
Nuclide Ave activity
FE-59 F 7.8085E-01
Co - 56
8 .4569E-01
Spectrum name: 5_Gamma_2 0161262 .Anl
Energy Activity Code Peak MDA Comments
4.45E+01
1099.25 3.400E-01 ?(P 2.107E+00 2.36E+02 5.65E+01 G
1291.60 1.357E+00 ?(P 1.674E+00 4.15E+01 4.32E+01 G
7.73E+01
846.77 5.139E-01 &( 1.167E+00 9.43E+01 9.99E+01 G
1238.28-4.145E-01 - P 3.514E+00 3.12E+02 6.61E+01 G
1037.84 3.192E+00 ?(P 7.739E+00 9.96E+01 1.41E+01 G
1771.35-6.083E+00 + 2.422E+01 1.16E+02 1.55E+01 A
CO - 57
2 . 0461E-01
122.06 2 . 046E-01
136 . 47-1.435E-07
2.72E+02
8.922E-01 1.29E+02 8.56E+01 G
8.997E+00 1.82E+09 1.07E+01 G
CO - 58
CO-6 0
¦7.8012E-01
-4 .3290E-01
7.09E+01
810.78-7.801E-01 ?(P 2.345E+00 4.14E+01 9.95E+01 G
1.93E+03
1332 . 50-4.329E-01 ?(P 2.169E+00 6.14E+01 1.00E+02 G
1173.24 4.436E-01 + P 1.940E+00 1.82E+02 9.99E+01 G
NB-94
-6 . 0127E-02
702 . 63-6.013E-02 ?(
7.41E+06
1.173E+00 7.43E+02 9.79E+01 G
171.10-5.196E-01 + P 1.437E+00 7.05E+01 9.99E+01 G
ZR-95
¦1.0346E+00
6.40E+01
756.73-1.035E+00 ?(P 3.482E+00 5.32E+01 5.45E+01 G
724.20 0.000E+00 + 3.682E+00 1.00E+03 4.42E+01 G
NB-95
RU-103
4 . 6196E-01
¦9 . 6988E-02
765 . 79 4 . 620E-01 ?(
497 . 05-9.699E-02 ?(
610.30 7.243E+00 ?
6 .40E+01
2.375E+00 1.49E+02 9.98E+01 G
3 . 93E+01
1.142E+00 4.43E+02 9.09E+01 G
5.746E+01 2.33E+02 5.75E+00 GA
RH-106
2.0574E+00
621. 92-1.517E+00 ?(
1050.36 2.481E+01 ?(
511.86 1.257E+01 ?
3.74E+02
3.239E+01 6.22E+02 9.93E+00 G
1.008E+02 1.15E+02 1.56E+00 G
6.689E+00 2.96E+01 2.00E+01 GA
AG-108M
3 .3871E-01
433.94 2.175E-01 ?(
722.94 0.000E+00 -
614.28 4.607E-01 ?(
1.53E+05
8.202E-01 1.43E+02 9.05E+01 G
1.787E+00 1.00E+03 9.08E+01 G
3.780E+00 2.41E+02 8.98E+01 G
(Page 11 of 21)
Page 412 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:07 AMPage 10
Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
AG-110M
4 . 7531E-01
2.50E+02
884.68 0 . 000E+00
? (
3 . 620E+00
1.00E+03
7.27E+01
G
657 .16-6.829E-01
+
2.092E+00
9.08E+01
9.46E+01
G
937.49 0.000E+00
? (
4.3 95E+00
1.00E+03
3.44E+01
G
1384.30 2 . 570E+00
? (
3.157E+00
4.08E+01
2.43E+01
G
763 . 94-4.521E+00
+
1.041E+01
6.94E+01
2.23E+01
G
SN-113 F 3 . 0942E-01
1.15E+02
391.69 3.094E-01 &(P 1.857E+00 1.73E+02 6.40E+01 G
SB-124 F 6.7995E-01
602.73 4.174E-01 ?(
1690.98 0.000E+00 -
722 .79 3.067E+00 ?(
6.02E+01
3.395E+00 2.39E+02 9.83E+01 G
1.899E+00 1.00E+03 4.78E+01 G
1.3 56E+01 1.27E+02 1.08E+01 G
SB-125 I 1. 3552E+00
1.01E+03
427.88-8.425E-01 ?(P 3.621E+00 1.49E+02 2.96E+01 G
600.50 2.286E+00 ?( 1.821E+01 2.34E+02 1.79E+01 G
635.89 3.163E+00 ?( 8.234E+00 7.71E+01 1.13E+01 G
463.37 4.028E+00 ( 1.321E+01 9.67E+01 1.05E+01 G
1-131 I 8.6918E-01
364.48 8.751E-01 ?(
284.30 4.511E-01 &
636.97 8.017E-01 ?(
8.02E+00
1.024E+00 4.71E+01 8.17E+01 G
1.330E+01 1.08E+03 6.14E+00 G
1.656E+01 5.58E+02 7.17E+00 G
Gd-153 F -8.2480E-01
97.50-8.248E-01 ?(
103.20 4.587E-01 &
2.42E+02
2.7 83E+00 1.00E+02 3.00E+01 G
3.831E+00 2.44E+02 2.18E+01 G
Ga-6 8 C 3.0026E+00
1077.40 3.003E+00 ?(
4.71E-02
5.238E+01 7.02E+02 3.30E+00 G
Tc-99m I 2.5105E-01
140.51 2.511E-01
2.51E-01
1.171E+00 1.38E+02 8.93E+01 G
BA-133 F -6.1245E-01
356 . 00-6.125E-01 ?(
302.85-1.846E+00 +
383.84 2.523E+00 &
80 . 99-1.048E+00 +
3 . 85E+03
3.818E+00 1.84E+02 6.20E+01 G
1.018E+01 1.63E+02 1.83E+01 G
1.230E+01 1.41E+02 8.94E+00 GA
3.261E+00 1.16E+02 3.41E+01 GA
CS-134 I 7.6850E-01
604.71 3 . 570E-02 %(
795.87 1. 324E+00 ?(
569.32-6.420E-01 +
801.95 3.531E+00 &(
7.54E+02
3.500E+00 2.86E+03 9.76E+01 G
9.761E-01 3.57E+01 8.55E+01 G
8.349E+00 3.61E+02 1.54E+01 G
1.282E+01 1.46E+02 8.69E+00 G
(Page 12 of 21)
Page 413 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:07 AMPage 11
Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
563 .24
-1.172E+00
+
1.3 80E+01
4.43E+02 8.35E+00
G
CS-137
I
2 . 8169E-01
1.10E+04
661. 66
2.817E-01
? (P
2.212E+00
2.25E+02 8.52E+01
G
CE-139
F
2 . 8823E-01
1.38E+02
165 . 85
2.882E-01
@ (
1.103E+00
1.13E+02 7.99E+01
G
Ba-140
I
5 . 2763E-02
1.28E+01
537.26
5.276E-02
% (P
4.198E+00
2.91E+03 2.44E+01
G
162.66
-3.156E+00
+
1.614E+01
1.51E+02 6.22E+00
G
304.85
0.000E+00
Sc.
4.514E+01
1.00E+03 4.29E+00
G
La-140
I
-3 . 1232E-01
1.28E+01
1596.21
-9.018E-01
? (
2.262E+00
1.14E+02 9.54E+01
G
487.02
-1.136E+00
+
2.769E+00
9.73E+01 4.55E+01
G
328.76
5.13 IE-02
o.
"o
5.37 0E+00
3.88E+03 2.03E+01
G
815.77
2.103E+00
? (
7.915E+00
1.09E+02 2.33E+01
G
CE-141
I
4 .3669E-01
3.25E+01
145.44
4.367E-01
& (
1.990E+00
1.35E+02 4.82E+01
G
CE-144
I
1. 8331E+00
2.85E+02
133.54
1.833E+00
& (
8.232E+00
1.33E+02 1.11E+01
G
PM-144
C
-3 . 3592E-01
3.63E+02
696.54
-3.359E-01
? (P
1.441E+00
1.70E+02 9.90E+01
G
618.06
0.000E+00
+
3.517E+00
1.00E+03 9.91E+01
G
EU-152
F
1.0770E+00
4.94E+03
344.29
1.127E+00
? (
5.813E+00
1.51E+02 2.65E+01
G
1112.07
1. 792E+00
? (
2.136E+01
3.38E+02 1.36E+01
G
121.78
6 . 893E-01
? (
2.505E+00
1.08E+02 2.86E+01
G
778.92
-3.3 06E-01
o.
"o
1.133E+01
1.38E+03 1.29E+01
G
964.11
1.752E-01
o.
"o
1.868E+01
3.00E+03 1.46E+01
G
244.69
-4.553E+00
+
2.852E+01
1.86E+02 7.58E+00
G
1408.00
1.340E+00
7
6.769E+00
2.06E+02 2.10E+01
GA
EU-154
I
-8 . 2445E-02
3.14E+03
873.23
-3.047E+00
? (P
1.680E+01
1.01E+02 1.23E+01
G
123.10
-6.053E-01
+ p
2.090E+00
9.45E+01 4.08E+01
G
1274.54
0.000E+00
+
6.494E+00
1.00E+03 3.52E+01
G
723 .36
0.000E+00
+
8.031E+00
1.00E+03 2.02E+01
G
1004.77
2.206E-01
o.
"o
1.3 62E+01
1.71E+03 1.80E+01
G
996 .33
3.349E+00
& (
2.117E+01
1.80E+02 1.06E+01
G
(Page 13 of 21)
Page 414 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Nuclide Ave activity
EU-155 I -1.2180E+00
Env32 G800W064 7/11/2016 9:17:07 AMPage 12
Spectrum name: 5_Gamma_2 0161262.Anl
Energy
Activity Code Peak MDA Comments
105.31-1.218E+00 @
86.54 4.219E-01 &
1.81E+03
(P 5.958E+00 8.87E+01 2.12E+01 G
4.870E+00 3.42E+02 3.07E+01 G
HF-181 F 3.2019E-01
482 . 00 2.242E-01 ?(
133.02 4 . 986E-01 &(
345.83-2.440E+00 +
136.30 2.619E-07 %
4.24E+01
1.630E+00 2.07E+02 8.05E+01 G
2.194E+00 1.30E+02 4.33E+01 G
1.169E+01 1.41E+02 1.51E+01 G
1.642E+01 1.82E+09 5.85E+00 G
Ta-182 F 1. 7764E+00
Hg-203 F -4.7416E-01
1121.30 1.495E+00 ?(
1221.41 1.849E+00 (
1189.05 2.260E+00 ?(
279.20-4.742E-01 ?(
1.14E+02
6.605E+00 1.27E+02 3.49E+01 G
6.217E+00 1.46E+02 2.70E+01 G
9.8 58E+00 1.81E+02 1.62E+01 G
4.66E+01
1.495E+00 9.38E+01 8.15E+01 G
TL-208 N 3 .3456E+00
pm-146 C 6.3224E-01
583.02 3.397E+00 (
277.28-4.299E-01 -
860.56 2 . 996E+00 &(
6 . 98E+02
4.392E-01 1.32E+01 8.45E+01 G
1.475E+01 9.64E+02 6.31E+00 G
1.2 83E+01 1.77E+02 1.24E+01 G
2.02E+03
747.16 6.504E-01 ?(P 2.282E+00 1.31E+02 3.40E+01 G
735.72 1.138E+00 ?(P 6.085E+00 2.10E+02 2.25E+01 G
453.88 4.477E-01 ?( 1.185E+00 1.02E+02 6.50E+01 G
y-
F 4 . 0488E-03
898.04 4.049E-03
1836 . 06-4.150E-02
1.07E+02
(P 1.343E+00 1.26E+04 9.37E+01 G
P 9.809E-01 1.60E+03 9.92E+01 G
Cf-251 T 2.5267E+00
176.60 2 . 527E+00
227 . 00-2.797E+00
3.28E+05
3.535E+00 5.32E+01 1.70E+01 G
1.379E+01 1.78E+02 6.30E+00 GA
Cf-249 T 4 . 2367E-01
387.95 4.237E-01 ?(
333 . 44-2.718E-01 &
1.28E+05
1.808E+00 1.24E+02 6.60E+01 G
6.585E+00 8.95E+02 1.55E+01 G
Sn-126
1. 7143E+00
87.57 1.165E+00 }
64.28 1.714E+00 ?(
86.94 1.714E+00 }
3.65E+07
3.744E+00 4.95E+01 3.75E+01 GA
1.292E+01 2.22E+02 9.70E+00 G
1.668E+01 1.51E+02 9.04E+00 GA
(Page 14 of 21)
Page 415 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 13
TestAmerica Inc
Nuclide Ave activity
PB-210 N 3 . 0795E+01
Spectrum name: 5_Gamma_2 0161262.Anl
Energy Activity Code Peak MDA Comments
8.14E+03
46.54 3.079E+01 (P 2.921E+01 3.58E+01 4.25E+00 G
PB-212 N 8.7621E+00
238.63 8 . 762E+00 (
300.03 2.163E+01 +
6.98E+02
1.543E+00 9.30E+00 4.33E+01 G
1.288E+01 2.74E+01 3.28E+00 GA
PB-214 N 1.3660E+01
5.84E+05
351.93 1.298E+01 (P 2.218E+00 1.02E+01 3.76E+01 G
295.09 1.497E+01 @(P 2.871E+00 1.18E+01 1.93E+01 G
242.00 1.493E+01 P 1.099E+01 2.53E+01 7.43E+00 GA
BI-207
3 . 1962E-01
569 . 70 3 .196E-01 ?(
1063.66-2.238E-01 -
1.18E+04
8.692E-01 8.01E+01 9.77E+01 G
2.322E+00 4.32E+02 7.45E+01 G
BI-212
N
¦5 . 1114E+00
6.98E+02
727 . 17-5.111E+00 ?(P 2.410E+01 1.53E+02 7.55E+00 G
785.42-6.819E+01 + 1.481E+02 9.38E+01 1.28E+00 GA
BI-214
N
1.1979E+01
5.84E+05
609.31 1.198E+01 (P 1.921E+00 1.09E+01 4.61E+01 G
1120.29 1.723E+00 - P 1.332E+01 2.17E+02 1.51E+01 G
1764.49 1.667E+01 + P 7.566E+00 2.44E+01 1.54E+01 G
BI-210M T
-2 . 8815E-01
265.83-2.881E-01 &(
304.90 0.000E+00 &
1.10E+09
2.291E+00 2.30E+02 5.00E+01 G
6.916E+00 1.00E+03 2.80E+01 G
AC-228
N
7 . 7456E+00
911.07 7.864E+00
968.97 4.924E+00
338.32 7 .460E+00
93 .35-4.303E+00
2 .10E+03
(P 2.988E+00 2.15E+01 2.90E+01 G
P 1.017E+01 8.82E+01 1.75E+01 G
( 4.648E+00 2.64E+01 1.20E+01 G
2.717E+01 1.88E+02 5.56E+00 XA
TH-227
N
9 . 6073E+00
7.95E+03
50.14 9.607E+00 *(P 1.244E+01 4.72E+01 8.00E+00 G
256.24 1.742E+00 - P 1.223E+01 2.63E+02 7.00E+00 G
TH-229
TH-234
N 3 . 5277E+00
N -9 . 2407E+00
193.51 1. 221E+00 ?(
2.68E+06
1.822E+01 5.35E+02 4.40E+00 G
210.85 6.923E+00 ?(P 3.024E+01 1.59E+02 2.99E+00 G
1.63E+12
63.29-9.241E+00 ?(P 3.297E+01 7.63E+01 3.81E+00 G
92.59 5.788E+00 + P 1.378E+01 7.23E+01 5.58E+00 G
(Page 15 of 21)
Page 416 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:07 AMPage 14
Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide Ave activity Energy Activity Code Peak MDA Comments
PA-231 N
-1.3213E+01
1.20E+07
302.65-1.321E+01
? (
6.23 9E+01
1.40E+02 2.88E+00
G
300 . 07-1.532E+01
+
7.735E+01
1.49E+02 2.46E+00
G
PA-233 C
9.0976E-01
7.82E+08
312.01 9 . 098E-01
? (
4.635E+00
1.50E+02 3.60E+01
G
300 .18-6.082E+00
+
2.963E+01
1.44E+02 6.20E+00
G
PA-2 3 4 N
-1. 573IE-01
1.63E+12
131.29-1.143E+00
? (
5.676E+00
1.47E+02 1.80E+01
G
946 . 02-7.516E-01
+
9.552E+00
4.94E+02 1.34E+01
G
569.47 2.007E+00
? (
1.528E+01
2.14E+02 8.20E+00
G
883.24-1.186E+00
&
2.699E+01
6.44E+02 9.60E+00
G
880.53-1.273E+01
+
3.872E+01
9.00E+01 6.00E+00
GA
PA-234M N
6 . 3224E+01
1.63E+12
1001.00 0.000E+00
? (
2.865E+02
1.00E+03 8.37E-01
G
766.41 2.432E+02
? (
6.756E+02
8.26E+01 2.94E-01
G
U-235 N
2 . 0137E+00
2.57E+11
143.79 2.014E+00
? (
8.974E+00
1.32E+02 1.10E+01
G
205.33-3.904E+00
+ p
1.775E+01
1.64E+02 5.01E+00
G
163.38 0.000E+00
-
2.060E+01
1.00E+03 5.08E+00
G
AM-241 T
-1.063 9E+00
1.58E+05
59 . 54-1.064E+00
? (p
3.289E+00
7.92E+01 3.59E+01
G
Ir-192 F
-4.5950E-01
7.40E+01
316.49-4.595E-01
? (
1.584E+00
1.02E+02 8.70E+01
G
468 . 06-8.489E-01
+
3.321E+00
1.15E+02 5.18E+01
G
308.44 0 . 000E+00
&
6.158E+00
1.00E+03 3.18E+01
G
Cs-136 F
5.5751E-01
1.30E+01
818.50 4.918E-01
? (
1.705E+00
1.01E+02 1.00E+02
G
1048.07 5.976E-01
& (
1.4 53E+00
7.27E+01 8.00E+01
G
340.57 6 .293E-01
? (
3.099E+00
1.44E+02 4.69E+01
G
Np-239 T
-1. 0327E+00
2.36E+00
103.70 7 . 155E-01
7
3.274E+00
1.35E+02 2.40E+01
X
106.13-1.033E+00
& (
5.099E+00
1.47E+02 2.27E+01
G
99.50 1.442E+00
7
5.615E+00
1.15E+02 1.50E+01
X
Nd-147
-3 . 5832E+00
1.11E+01
531. 00-3.583E+00
& (
9.807E+00
1.08E+02 1.30E+01
G
91.10 8 . 462E-01
+
5.126E+00
1.80E+02 2.83E+01
G
(Page 16 of 21)
Page 417 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 15
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
S -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** £)
I S C A R D
ED IS
0 T 0 P E P
E A K S
*************'
Nuclide
Centroid
Background
Net Area
Intensity
Uncert
Activity
Energy
Counts
Counts
Cts/Sec
1 Sigma %
TH-227
50 .14
51.
28 .
0.015
47 .24
9 . 607E+00
P
AM-2 41
59 . 54
120 .
-17 .
-0.010
79 .17
-1.064E+00
P
BA-133
80 . 99
187 .
-21.
-0.012
116.04
-1.048E+00
EU-155
86 . 54
371.
8 .
0.004
341. 89
4 . 219E-01
Nd-147
91.10
364 .
15 .
0.008
180.25
8 . 462E-01
Gd-153
97 . 50
120 .
-16 .
-0.009
100.41
-8 . 248E-01
Np-239
99 . 50
123 .
14 .
0.008
115.41
1.442E+00
Gd-153
103.20
122 .
6 .
0.004
243.98
4.587E-01
Np-239
103 . 70
108 .
11.
0.006
134.87
7.155E-01
EU-155
105.31
291.
-17 .
-0.009
88 .67
-1.218E+00
P
Np-239
106.13
243 .
-15 .
-0.008
146 . 70
-1.033E+00
EU-152
121.78
87 .
13 .
0.007
107.53
6.893E-01
CO - 57
122.06
100 .
11.
0.006
128.54
2.046E-01
EU-154
123.10
125 .
-16 .
-0.009
94 . 52
-6.053E-01
P
PA-2 3 4
131.29
176 .
-13 .
-0.007
146.96
-1.143E+00
HF-181
133.02
150 .
14 .
0.008
130.33
4.986E-01
CE-144
133.54
137 .
13 .
0.007
132 . 81
1.833E+00
Tc-99m
140.51
163 .
13 .
0.007
138.12
2.511E-01
(Page 17 of 21)
Page 418 of 551
-------
ORTEC g v - i (3263!
TestAmerica Inc
Env32 G800W064 7/11/2016 9:17:07 AMPage 16
Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
CE-141
145 .44
140
13 .
0 . 007
134 . 80
Ba-140
162.66
132
-11.
-0.006
150.76
CE-139
165.85
102
13 .
0 . 007
113 .25
Cf-251
176.60
40
23 .
0 . 013
53 .19
TH-229
193.51
63
3 .
0 . 001
534 . 59
TH-229
210 . 85
70
10 .
0 . 005
159.25
Cf-251
227.00
57
-8 .
-0 . 004
178.42
EU-152
244 .69
338
-14 .
-0.008
186.16
TH -7.7.1
256.24
44
5 .
0 . 003
263.21
BI-210M
265.83
78
-6 .
-0 . 003
230.34
Hg-203
279.20
81
-14 .
-0.008
93 . 75
PA-2 31
300.07
183
-13 .
-0.007
149.45
PA-233
300.18
170
-13 .
-0.007
144 . 22
PA-2 31
302.65
160
-13 .
-0.007
139 . 77
BA-133
302.85
173
-12 .
-0.006
163.02
PA-233
312.01
130
11.
0 . 006
150.18
Ir-192
316.49
84
-13 .
-0.007
102.18
CR-51
320 . 08
112
-15 .
-0.008
105 . 01
Cf-249
333.44
40
-1.
-0.001
895.30
Cs-136
340 . 57
83
9 .
0 . 005
144 .30
EU-152
344 .29
92
9 .
0 . 005
151.22
HF-181
345.83
121
-11.
-0.006
141.23
BA-133
356.00
214
-11.
-0.006
184 .34
1-131
364 .48
22
21.
0 . 012
47 . 14
BA-133
383 . 84
37
6 .
0 . 004
140 . 66
Cf-249
387 . 95
43
8 .
0 . 004
124 .21
SN-113
391.69
42
5 .
0 . 003
172 . 75
SB-125
427 . 88
28
-6 .
-0 . 004
148 .61
AG-108M
433.94
12
5 .
0 . 003
142.83
pm-146
453 . 88
12
7 .
0 . 004
102 .35
SB-125
463 .37
43
10 .
0 . 006
96 . 66
Ir-192
468.06
67
-10 .
-0.006
115.10
HF-181
482 . 00
36
4 .
0 . 002
206 . 90
La-140
487 . 02
32
-12 .
-0.007
97.28
RU-103
497.05
20
-2 .
-0.001
443 .47
RH-106
511. 86
33
56 .
0 . 031
29.65
Nd-147
531.00
28
-10 .
-0.006
108 .32
CS-134
563.24
20
-2 .
-0.001
443 .47
CS-134
569.32
25
-2 .
-0.001
360.56
PA-2 3 4
569.47
24
3 .
0 . 002
213.54
BI-207
569.70
10
6 .
0 . 004
00
o
o
SB-125
600 . 50
168
8 .
0 . 004
234.15
SB-124
602.73
175
8 .
0 . 004
239.14
RU-103
610.30
168
8 .
0 . 004
233.13
AG-108M
614.28
176
8 .
0 . 004
241.15
RH-106
621. 92
154
-3 .
-0 . 002
621.92
SB-125
635 . 89
10
7 .
0 . 004
77 . 09
1-131
636.97
17
1.
0 . 001
557.69
Uncert FWHM
4 .367E-01
. 156E+00
. 882E-01
. 527E+00
. 221E+00
. 923E+00 P
. 797E+00
-4.553E+00
1.742E+00 P
881E-01
742E-01
-1.532E+01
-6.082E+00
. 321E+01
. 846E+00
. 098E-01
-4.595E-01
-4.521E+00
. 718E-01
. 293E-01
. 127E+00
. 440E+00
. 125E-01
. 751E-01
. 523E+00
. 237E-01
. 094E-01 P
. 425E-01 P
. 175E-01
. 477E-01
. 028E+00
. 489E-01
. 242E-01
. 136E+00
. 699E-02
. 257E+01
. 583E+00
. 172E+00
. 420E-01
. 007E+00
. 196E-01
. 286E+00
. 174E-01
. 243E+00
. 607E-01
. 517E+00
. 163E+00
. 017E-01
-3 .
2 .
2 .
1.
6 .
-2 .
-2
-4
¦1.
¦1.
9 .
-2 .
6 .
1.
-2 .
-6 .
8 .
2 .
4 .
3 .
-8 .
2 .
4 .
4 .
-8 .
2 .
-1.
-9 .
1.
-3 .
-1.
-6 .
2 .
3 .
2 .
4 .
7 .
4 .
-1.
3 .
(Page 18 of 21)
Page 419 of 551
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ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 17
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
Nuclide
Channel
Energy Background Net
area i
Cnts/sec
Uncert FWHM
AG-110M
657.76
50
-12 .
-0.006
90 . 77
-6 . 829E-01
PM-144
696.54
22
-6 .
-0.003
170.34
-3.359E-01 P
NB-94
702 . 63
13
-1.
-0.001
742.74
-6 . 013E-02
SB-124
722.79
22
6 .
0 . 003
126 . 62
3 . 067E+00
BI-212
727.17
34
-6 .
-0 . 004
152.77
- 5.111E+00 P
pm-146
735 . 72
18
4 .
0 . 002
210.42
1.13 8E+00 P
pm-146
747 . 16
4
4 .
0 . 002
131.31
6.504E-01 P
ZR-95
756.73
35
-9 .
-0.005
53 .23
-1.03 5E+00 P
AG-110M
763.94
53
-16 .
-0.009
69.41
-4.521E+00
NB-95
765 . 79
56
7 .
0 . 004
149.41
4.620E-01
PA-234M
766.41
38
11.
0 . 006
82 . 56
2.432E+02
BI-212
785 . 42
33
-14 .
-0.008
93 . 80
-6.819E+01
CS-134
795.87
5
17 .
0 . 010
35 . 72
1.324E+00
CS-134
801. 95
9
5 .
0 . 003
146.39
3.531E+00
CO - 58
810.78
48
-12 .
-0.006
41.38
-7.801E-01 P
La-140
815.77
29
7 .
0 . 004
109.40
2.103E+00
Cs-136
818.50
24
7 .
0 . 004
101. 03
4.918E-01
MN-54
834.85
5
4 .
0 . 002
132.73
2.611E-01 P
Co - 56
846.77
9
7 .
0 . 004
94 .25
5.139E-01
NB-94
871.10
14
-7 .
-0 . 004
70 . 52
- 5.196E-01 P
EU-154
873 .23
32
-5 .
-0.003
100 . 80
-3.047E+00 P
PA-2 3 4
880.53
41
-11.
-0.006
90 . 01
-1.273E+01
PA-2 3 4
883 .24
52
-2 .
-0.001
644.06
-1.186E+00
Sc-46
889.28
65
-9 .
-0.005
128.54
-6.575E-01
PA-2 3 4
946.02
9
-1.
-0.001
493.71
-7.516E-01
EU-154
996.33
30
4 .
0 . 002
179 . 85
3.349E+00
Co - 56
1037.84
5
6 .
0 . 003
99 . 59
3.192E+00 P
Cs-136
1048.07
6
6 .
0 . 003
72 . 66
5.976E-01
RH-106
1050.36
12
5 .
0 . 003
115.37
2.481E+01
BI-207
1063.66
15
-2 .
-0.001
431.57
-2.23 8E-01
Ga-6 8
1077.40
10
1.
0 . 001
702 .38
3.003E+00
FE-59
1099.25
6
2 .
0 . 001
236.19
3.400E-01 P
EU-152
1112.07
44
3 .
0 . 002
337 . 94
1.792E+00
Sc-46
1120.55
22
6 .
0 . 003
118.42
5.215E-01
CO-6 0
1173.24
16
5 .
0 . 003
182.44
4.436E-01 P
Co - 56
1238.28
22
-3 .
-0 . 002
311.56
-4.145E-01 P
NA-22
1274.53
16
-4 .
-0.002
150.00
-3.884E-01
FE-59
1291.60
0
6 .
0 . 003
41.45
1.3 57E+00 P
CO-6 0
1332.50
16
-4 .
-0 . 002
61.42
-4.329E-01 P
AG-110M
1384.30
0
6 .
0 . 003
40 . 82
2.570E+00
EU-152
1408.00
5
3 .
0 . 001
206.16
1.340E+00
La-140
1596.21
11
-7 .
-0 . 004
113 . 82
-9.018E-01
Co - 56
1771.35
32
-7 .
-0.004
115.70
-6.083E+00
P - Peakbackground subtraction
(Page 19 of 21)
Page 420 of 551
-------
ORTEC g v - i (3263) Env32 G800W064 7/11/2016 9:17:07 AMPage 18
TestAmerica Inc Spectrum name: 5_Gamma_2 0161262.Anl
***** SUMMARY OF NUCLIDES IN SAMPLE *****
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting MDA
Bq/Sample Bq/Sample Bq/Sample
BE - 7
#
1. 1618E+01
1. 1618E+01
2.548E+01%
7.73E+00
NA-22
#A
-3 . 8840E-01
-3 . 8841E-01
1.500E+02 %
2.07E+00
K-40
1. 4318E+02
1. 4318E+02
8.670E+00%
1.19E+01
Sc-46
#A
-6 . 7968E-02
-6 . 7969E-02
8.738E+01%
2.89E+00
CR-51
#A
-4 . 5212E+00
-4 . 5213E+00
1.050E+02 %
1.60E+01
MN-54
#A
2 . 6112E-01
2 . 6112E-01
1.327E+02%
9.05E-01
FE-59
#A
7 . 8084E-01
7.8085E-01
4.145E+01%
2.11E+00
Co - 56
#A
8 .4568E-01
8.4569E-01
6.856E+01%
1.17E+00
CO - 57
#A
2 . 0461E-01
2.0461E-01
1.285E+02%
8.92E-01
CO - 58
#A
-7.8012E-01
-7.8012E-01
4.138E+01%
2.3 5E+00
CO-6 0
#A
-4 . 3290E-01
-4.3290E-01
6.142E+01%
2.17E+00
ZN-65
#A
0.0000E+00
0.0000E+00
1.000E+03 %
5.94E+00
NB-94
#A
-6 . 0127E-02
-6.0127E-02
7.42 7E+02 %
1.17E+00
ZR-95
#A
-1. 0346E+00
-1.0346E+00
5.323E+01%
3.48E+00
NB-95
#A
4 . 6196E-01
4.6196E-01
1. 494E+02%
2.3 8E+00
RU-103
#A
-9 . 6987E-02
-9.6988E-02
4.43 5E+02 %
1.14E+00
RH-106
#A
2 . 0573E+00
2.0574E+00
1.154E+02 %
3.24E+01
AG-108M#A
3 .3871E-01
3.3871E-01
1.401E+02%
8.20E-01
AG-110M#A
4 . 7530E-01
4.7531E-01
4.082E+01%
3.62E+00
SN-113
#A
3 . 0941E-01
3.0942E-01
1.72 7E+02 %
1.86E+00
SB-124
#A
6 . 7994E-01
6.7995E-01
1.266E+02 %
3.40E+00
SB-125
#A
1. 3552E+00
1.3 552E+00
7.591E+01%
3.62E+00
1-131
#A
8 . 6912E-01
8.6918E-01
4.714E+01%
1.02E+00
Gd-153
#A
-8 . 2480E-01
-8.2480E-01
1.004E+02 %
2.78E+00
Ga-6 8
#A
2 . 9665E+00
3.0026E+00
7.024E+02 %
5.24E+01
Tc-99m
#A
2 . 5048E-01
2.5105E-01
1.381E+02%
1.17E+00
BA-133
#A
-6 . 1245E-01
-6.1245E-01
1.843E+02 %
3.82E+00
CS-134
#A
7.6850E-01
7.6850E-01
3.572E+01%
3.50E+00
CS-137
#A
2 . 8169E-01
2.8169E-01
2.255E+02%
2.21E+00
CE-139
#A
2 . 8823E-01
2.8823E-01
1.132E+02 %
1.10E+00
Ba-140
#A
5 . 2760E-02
5.2763E-02
2.907E+03 %
4.20E+00
La-140
#A
-3.123 0E-01
-3.1232E-01
7.894E+01%
2.26E+00
CE-141
#A
4.3668E-01
4.3669E-01
1.348E+02%
1.99E+00
CE-144
#A
1. 8331E+00
1.8331E+00
1.328E+02%
8.23E+00
PM-144
#A
-3 . 3592E-01
-3.3 592E-01
1.703E+02 %
1.44E+00
EU-152
#A
1.0770E+00
1.0770E+00
1.075E+02%
5.81E+00
EU-154
#A
-8.2445E-02
-8.2445E-02
1.008E+02 %
1.68E+01
EU-155
#A
-1.2180E+00
-1.2180E+00
8.867E+01%
5.96E+00
HF-181
#A
3 .2018E-01
3.2019E-01
1.223E+02 %
1.63E+00
Ta-182
A
1. 7764E+00
1.7764E+00
8.826E+01%
6.60E+00
Hg-203
#A
-4 . 7415E-01
-4.7416E-01
9.375E+01%
1.50E+00
TL-208
3 .3456E+00
3.3456E+00
1.325E+01%
4.3 9E-01
pm-146
#A
6.3224E-01
6 . 3224E-01
8.944E+01%
2.28E+00
(Page 2 0 of 21)
Page 421 of 551
-------
ORTEC g
v - i (3263)
Env32 G800W064
7/11/2016 9:
17:07 AMPage 19
TestAmerica
Inc
Spectrum
name: 5 Gamma
20161262.Anl
y-88
#A
4 . 0488E-03
4 . 0488E-03
1.256E+04%
1.34E+00
Cd-113m#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.52E+04
Cd-109
#A
0.0000E+00
0.0000E+00
1.000E+03 %
3.79E+01
Cf-251
#A
2 . 5267E+00
2.5267E+00
5.319E+01%
3.54E+00
Cf-249
#A
4 . 2367E-01
4.2367E-01
1.242E+02 %
1.81E+00
Sn-126
#A
1. 7143E+00
1.7143E+00
2.215E+02%
1.29E+01
PB-210
3.0795E+01
3.0795E+01
3.582E+01%
2.92E+01
PB-212
8.7621E+00
8.7621E+00
9 . 297E+00%
1.54E+00
PB-214
1.3660E+01
1.3660E+01
7 . 807E+00%
2.22E+00
BI-207
#A
3 .1962E-01
3.1962E-01
8 . 009E+01%
8.69E-01
BI-212
#A
-5 .1114E+00
-5.1114E+00
1.52 8E+02 %
2.41E+01
BI-214
1.1979E+01
1.1979E+01
1.088E+01%
1.92E+00
BI-210M#A
-2.8815E-01
-2.8815E-01
2.3 03E+02 %
2.29E+00
AC-228
7 . 7456E+00
7.7456E+00
1.703E+01%
2.99E+00
TH-227
#A
9 . 6073E+00
9.6073E+00
4.724E+01%
1.24E+01
TH-229
#A
3 . 5277E+00
3.5277E+00
1.593E+02 %
1.82E+01
TH-234
#A
-9.2407E+00
-9.2407E+00
7.630E+01%
3.3 0E+01
PA-2 31
#A
-1.3213E+01
-1.3213E+01
1.3 98E+02 %
6.24E+01
PA-233
#A
9.0976E-01
9.0976E-01
1.502E+02 %
4.64E+00
PA-2 3 4
#A
-1. 573IE-01
-1.573 IE-01
1.2 96E+02 %
5.68E+00
PA-234M#A
6 . 3224E+01
6 . 3224E+01
8 . 256E+01%
2.87E+02
U-235
#A
2 . 0137E+00
2 . 0137E+00
1.320E+02%
8.97E+00
AM-2 41
#A
-1.063 9E+00
-1.063 9E+00
7 . 917E+01%
3.29E+00
Np-237
#A
0.0000E+00
0.0000E+00
1.000E+03 %
1.30E+01
Ir-192
#A
-4.5949E-01
-4.5950E-01
1.022E+02 %
1.58E+00
Cs-136
#A
5 . 5748E-01
5.5751E-01
6.352E+01%
1.71E+00
Np-239
#A
-1.0325E+00
-1.0327E+00
1.467E+02%
5.10E+00
Nd-147
#A
-3.583 0E+00
-3.5832E+00
1.083E+02 %
9.81E+00
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.8 keV) 2.195E+02 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.8 keV) 2.1946523E+02 Bq/Sample
(Page 21 of 21)
Page 422 of 551
-------
257060_Gamma_160-17814-A-4-B. 5_Gamma_20161262.spc.
1.0e4-
1.0e3-
00
CN
CN
1 .OeO-
CO
CN
CO -
O
CN
<1,
O-O)
LO
O
D) =5
< I '
csi
m
o
O
500
1000
1500
2000
2500
3000 3500 4000
Channels
4500
5000
5500
6000
6500
7000
7500
8000
-------
Daily Checks
Page 424 of 551
-------
Test America
St. Louis
Quality Control Check
Spectrum: 3_20160711001_QCAsLeft
Description: Quality control Check (QC Source 'C') Post Stabilization
Acquired: 7/11/2016 12:40:31 AM
Detector: Detector # 3
Quality Control Evaluation Criteria:
1) Notify Supervisor if 'AS FOUND' parameters exceed Tolerance or Control Limits.
2) Place out of service if 'AS LEFT' parameters exceed Tolerance or Control Limits.
Target
L_Ctrl
L_Tol
Measured
H_Tol
H_Ctrl
Results
QA-6 0
Channel
238 . 00
236.00
237.00
238.00
239.00
240.00
PASS
Energy
59 . 54
59 . 04
59.29
59 . 57
59 . 79
o
o
PASS
FWHM
0 . 81
0 . 00
0 . 00
0 . 82
1. 91
2 . 01
PASS
ActivityDiff
647 . 00
-5 . 00
-4 . 00
-1. 67
4 . 00
5 . 00
PASS
QA-662
FWHM
1.46
0 . 00
0 . 00
1. 44
3 .16
3 .26
PASS
ActivityDiff
606.50
-5 . 00
-4 . 00
-3 . 12
4 . 00
5 . 00
PASS
Q A -13 3 2
Channel
5330 . 00
5327.00
5328 . 00
5331.10
5332.00
5333.00
PASS
Energy
1332 . 51
1331. 76
1332.01
1332.72
1333.01
1333 .26
PASS
FWHM
2 . 07
0 . 00
0 . 00
1. 98
4 .27
4.37
PASS
ActivityDiff
1183.00
-5 . 00
-4 . 00
-2 .27
4 . 00
5 . 00
PASS
Analyst: Aaron Schroder Reviewer: Amanda Dick
Page 425 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 3_20160711002_BG
Description: Background Contamination Check
Acquired: 7/11/2016 6:34:49 AM
Detector: Detector # 3
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 2.34 2.18 2.23 2.40 2.44 2.49 PASS
Analyst: Amanda Dick Reviewer: Amanda Dick
Page 426 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 5_20160711001_BG
Description: Background Contamination Check
Acquired: 7/11/2016 12:15:17 AM
Detector: Detector # 5
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.45 1.30 1.35 1.40 1.55 1.60 PASS
Analyst: Aaron Schroder Reviewer: Amanda Dick
Page 427 of 551
-------
Test America
St. Louis
Quality Control Check
Spectrum: 5_20160711002_QCAsLeft
Description: Quality control Check (QC Source 'A') Post Stabilization
Acquired: 7/11/2016 6:58:06 AM
Detector: Detector # 5
Quality Control Evaluation Criteria:
1) Notify Supervisor if 'AS FOUND' parameters exceed Tolerance or Control Limits.
2) Place out of service if 'AS LEFT' parameters exceed Tolerance or Control Limits.
Target
L_Ctrl
L_Tol
Measured
H_Tol
H_Ctrl
Results
QA-6 0
Channel
238 . 00
236.00
237.00
237.90
239.00
240.00
PASS
Energy
59 . 54
59 . 04
59.29
59 . 59
59 . 79
o
o
PASS
FWHM
0 . 74
0 . 00
0 . 00
0 . 74
1. 84
1. 94
PASS
ActivityDiff
636 .60
-5 . 00
-4 . 00
0 . 01
4 . 00
5 . 00
PASS
QA-662
FWHM
1.36
0 . 00
0 . 00
1.38
3 . 06
3 .16
PASS
ActivityDiff
596.80
-5 . 00
-4 . 00
-1.77
4 . 00
5 . 00
PASS
Q A -13 3 2
Channel
5330.00
5327.00
5328 . 00
5330.70
5332.00
5333.00
PASS
Energy
1332.51
1331. 76
1332.01
1332.73
1333.01
1333 .26
PASS
FWHM
1. 90
0 . 00
0 . 00
1. 83
4 .10
4.20
PASS
ActivityDiff
1164.20
-5 . 00
-4 . 00
-3 . 19
4 . 00
5 . 00
PASS
Analyst: Amanda Dick Reviewer: Amanda Dick
Page 428 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 7_20160711001_BG
Description: Background Contamination Check
Acquired: 7/11/2016 12:16:14 AM
Detector: Detector # 7
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.30 1.16 1.21 1.28 1.40 1.45 PASS
Analyst: Aaron Schroder Reviewer: Amanda Dick
Page 429 of 551
-------
Test America
St. Louis
Quality Control Check
Spectrum: 7_20160711002_QCAsLeft
Description: Quality control Check (QC Source 'C') Post Stabilization
Acquired: 7/11/2016 6:57:05 AM
Detector: Detector # 7
Quality Control Evaluation Criteria:
1) Notify Supervisor if 'AS FOUND' parameters exceed Tolerance or Control Limits.
2) Place out of service if 'AS LEFT' parameters exceed Tolerance or Control Limits.
Target
L_Ctrl
L_Tol
Measured
H_Tol
H_Ctrl
Results
QA-6 0
Channel
238 . 00
236.00
237.00
237.90
239.00
240.00
PASS
Energy
59 . 58
59 . 04
59.29
59 . 59
59 . 79
o
o
PASS
FWHM
0 . 84
0 . 00
0 . 00
0 . 96
1. 94
2 . 04
PASS
ActivityDiff
647 . 00
-5 . 00
-4 . 00
0 .47
4 . 00
5 . 00
PASS
QA-662
FWHM
1.45
0 . 00
0 . 00
1.49
3 .15
3.25
PASS
ActivityDiff
606.50
-5 . 00
-4 . 00
-0 . 33
4 . 00
5 . 00
PASS
Q A -13 3 2
Channel
5330 . 00
5327.00
5328 . 00
5330.60
5332.00
5333.00
PASS
Energy
1332 . 51
1331. 76
1332.01
1332.72
1333.01
1333 .26
PASS
FWHM
1. 98
0 . 00
0 . 00
2 . 02
4 .18
4.28
PASS
ActivityDiff
1183.00
-5 . 00
-4 . 00
-1. 07
4 . 00
5 . 00
PASS
Analyst: Amanda Dick Reviewer: Amanda Dick
Page 430 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 8_20160711001_BG
Description: Background Contamination Check
Acquired: 7/11/2016 12:17:39 AM
Detector: Detector # 8
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.56 1.39 1.45 1.61 1.68 1.74 PASS
Analyst: Aaron Schroder Reviewer: Amanda Dick
Page 431 of 551
-------
Test America
St. Louis
Quality Control Check
Spectrum: 8_20160711002_QCAsLeft
Description: Quality control Check (QC Source 'D') Post Stabilization
Acquired: 7/11/2016 6:56:31 AM
Detector: Detector # 8
Quality Control Evaluation Criteria:
1) Notify Supervisor if 'AS FOUND' parameters exceed Tolerance or Control Limits.
2) Place out of service if 'AS LEFT' parameters exceed Tolerance or Control Limits.
Target
L_Ctrl
L_Tol
Measured
H_Tol
H_Ctrl
Results
QA-6 0
Channel
238 . 00
236.00
237.00
237.80
239.00
240.00
PASS
Energy
59 . 54
59 . 04
59.29
59 . 52
59 . 79
o
o
PASS
FWHM
1.10
0 . 00
0 . 00
0 . 86
2.20
2.30
PASS
ActivityDiff
650.60
-5 . 00
-4 . 00
-1.48
4 . 00
5 . 00
PASS
QA-662
FWHM
1. 53
0 . 00
0 . 00
1.37
3 .23
3 .33
PASS
ActivityDiff
609.90
-5 . 00
-4 . 00
0 .47
4 . 00
5 . 00
PASS
Q A -13 3 2
Channel
5330.00
5327.00
5328 . 00
5331.30
5332.00
5333.00
PASS
Energy
1332 . 51
1331. 76
1332.01
1332.82
1333.01
1333 .26
PASS
FWHM
1. 90
0 . 00
0 . 00
1. 79
4 .10
4.20
PASS
ActivityDiff
1189.70
-5 . 00
-4 . 00
-0 . 43
4 . 00
5 . 00
PASS
Analyst: Amanda Dick Reviewer: Amanda Dick
Page 432 of 551
-------
Initial
Calibrations
Page 433 of 551
-------
Ge03 90099 solidcert2012TALS.xls
Gamma Verification per Geometry
Detector: Ge3
Geometry: Tunacan
Reference date 1/1/2012
Calibration Standard: 90099
Standard volume g / vial 1550
Standard volume transferred in g / geometry 317.8
lab ID# of cal standard 6699
Isotope
Certified Activity
gammas/sec
Geometry
Activity
qammas/sec
y abundance
Bq/sample
Count
Results
%recovery
Pb-210
3094
634
0.0425
14926
15038
100.7
Am-241
2037
418
0.3590
1163
1231.1
105.8
Cd-109
2881
591
0.0361
16363
16045
98.1
Co-57
1511
310
0.8560
362
348.66
96.3
Ce-139
2139
439
0.7990
549
542.18
98.8
Hg-203
4651
954
0.8146
1171
1190.9
101.7
Sn-113
3015
618
0.6400
966
974.14
100.9
Cs-137
1938
397
0.8510
467
465.73
99.7
Y-88
7264
1489
0.9370
1589
1562.9
98.3
Co-60
3580
734
0.9997
734
732.25
99.7
Co-60
3581
734
0.9999
734
726.4
98.9
Y-88
7690
1577
0.9920
1589
1616.3
101.7
Reviewed By: Jody Watson
Date: 3/28/2012
SOP: ST-RD-0102 current rev
CalVerif_tuna can
Page 434 of 551
-------
Calibration Data from file: 3_Soil_TunaCan.Clb
Energy Calibration Date; 3/28/2012 Time: 11:26:42 AM
Efficiency Calibration Date: 3/28/2012 Time: 11:26:55 AM
Calibration Description:
3 Soil TunaCan 90099 032712
Energy Calibration Fit
Energy = 0.1475 +0.249738*Channel +3.68165e-008*Channel**2
FWHM (ch) = 3.1011 +0.001004*Channel -1.23886e-008*Channel**2
Energy/FWHM Table
Channel Energy(keV) Fit(keV)
Delta FWHM(keV) Fit(keV)
Delta
185.95
46 .54
46 . 59
-0.10%
Csl
CO
o
0 . 82
0.35%
237.88
59 . 54
59 . 56
-0.03%
0 . 81
0 . 83
-2 .35%
351.51
88.03
87 . 94
0 . 11%
0 . 85
0 . 86
-1.11%
487.69
122 . 06
121. 95
0 . 09%
0 . 89
0 . 90
-0.30%
663.54
165 . 85
165.87
-0.01%
0 . 96
0 . 94
1.71%
1117.25
279.17
279.21
-0.02%
1. 06
1 . 05
1.21%
1567.81
391.69
391.78
-0 . 02%
1. 16
1 . 16
-0.08%
2647.99
661.66
661.71
-0.01%
1 .42
1 .42
-0.09%
3593 .39
898 . 02
898.03
-0.00%
1 . 68
1. 64
2 .32%
4693.77
1173 .24
1173.17
0 . 01%
1. 85
/
1. 89
-1.87%
5330.55
1332.50
1332.44
0 . 00%
2 . 01
2 . 03
-0.79%
7343 .39
1836 .01
1836.06
-0.00% /
2 . 47
2 .45
0 .53%
/
Efficiency Calibration Fit
Knee Energy =
Above the Knee:
Ln(Eff) = -0
Below the Knee:
Ln(Eff) = -25
165.85 keV
Quadratic Uncertainty = 0.6409 %
.6102 -0 . 364228*Ln(Eng) -0.028954* (Ln(Eng))**2
Quadratic Uncertainty = 1.2945 %
.2514 +9.446449*Ln(Eng) -1.00597* (Ln(Eng))**2
Efficiency Table
Energy
Efficiency
Fit
Delta
46 . 54
2 . 1302E-002
2.2144E-002
-3 . 95%
59 . 54
3 . 3461E-002
3.182 3E- 0 02
4 . 89%
88 . 03
4.3165E-002
4.4041E-002
-2.03%
122.06
4 . 3938E-002
4.5635E-002
-3 . 86%
165.85
-- Knee
11
II
II
II
II
II
11
II
II
165.85
3.9111E-002
3.963 0E-002
-1.33%
279.17
2.8374E-002
2.7881E-002
1 . 74%
391.69
2.2192E-002
2.1995E-002
0 . 89%
661.66
1.5033E-002
1.5039E-002
-0 . 04%
898.02
1.1768E-002
1.1963E-002
-1.66%
1173.24
9.7156E-003
9.7485E-003
-0 . 34%
1332.50
8.7374E-003
8.8303E-003
-1. 06%
1836 . 01
6.9703E-003
6.854 6E-0 03
1. 66%
/
Calibration Certificate Table
Isotope
Energy
Pet
Halflife
Pb-210
46 . 54
4 .25
8.15E+003
Am-241
59 . 54
35 . 70
1. 58E + 005
Cd-109
88 . 03
3 . 61
4.63E+002
Co-5 7
122.06
85 . 60
2.72E+002
Ce-139
165.85
79. 90
1.38E+002
Hg-203
279.17
81 . 50
4.66E+001
Sn-113
391.69
64 . 00
1.15E + 0 02
Cs -13 7
661.66
85 .21
1.10E+004
Y-88
898.02
93 . 70
1.07E+002
Co-6 0
1173.24
99 . 90
1.93E+003
Co - 6 0
1332.50
99 . 98
1.93E+003
Y-88
1836.01
99.20
1.07E+002
Activity
GPS Error
Date & Time
14918.00
1170.90
16371.00
362.15
549.44
1170.60
965.63
465.91
1589.10
734.73
734.15
1589.70
634.00
4 . 10%
1/1/2012
11:00 : 00
AM
418.00
3 . 50%
1/1/2012
11:00:00
AM
591.00
4 . 70%
1/1/2012
11: 00 : 00
AM
310.00
4 . 10%
1/1/2012
11:00:00
AM
439.00
3 . 90%
1/1/2012
11:00:00
AM
954.00
3 . 80%
1/1/2012
11: 00 : 00
AM
618 . 00
3 . 90%
1/1/2012
11: 00 : 00
AM
397 . 00
4 . 00%
1/1/2012
11: 00 : 00
AM
1489 . 00
3 . 90%
1/1/2012
11 : 00 : 00
AM
734 . 00
4 . 00%
1/1/2012
11 : 00:00
AM
734 . 00
4 . 00%
1/1/2012
11: 00:00
AM
1577 . 00
4 . 00%
1/1/2012
11:00:00
AM
Page 435 of 551
-------
ORTEC g V - i (1087) Env32 G53W4.25 3/28/2012 11:31:04 AM
TestAmerica Spectrum name: 3_TunaCan_20120996.Anl
Sample description
3 TunaCan 90099 32712
Spectrum Filename: C:\User\SPC\Det3\3_TunaCan_20120996.Anl
Acquisition information
Start time:
Live time;
Real time:
Dead time:
Detector ID:
3/27/2012 6:49:29 PM
3600
3659
1.62 %
3
Detector system
Ge 3 SN/131
Calibration
Filename:
3 Soil TunaCan 90099 032712
3 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/28/2012 11:26:42 AM
0.14 7 keV
0.250 keV/channel
3 . 682E-08 keV/channelA2
3/28/2012 11:26:55 AM
165.85 keV
Quadratic
-6.102019E-01
( -2.895398E
Quadratic
-2.52 5141E+01
Uncertainty = 0.64
+ (-3 .642282E-01*Log(E) )
02 *Log (E)a2 )
Uncertainty = 1.29
+ ( 9.446449E+0 0*Log(E) )
( -1.0 05974E+0 0*Log(E) 2 )
DET EnerqyStandardMix & Pb.Lib
0 .500
Library based
Env3 2 G53W4.25
150 ( 3 7.61keV )
iOOO ( 2 000.41keV )
10.000%
3
1.0000E+00
1.00 0 0E + 0 0/( 1.0000E + 00* 1.0000E + 00)
1.0000E+00
Reg. Guide 4.16 Method
Page 436 of 551
-------
ORTEC g V - i (1087) Env3 2 G53W4.25 3/28/2012 11:31:04 AM
TestAmerica Spectrum name: 3_TunaCan_20120996.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor: 2.000
Min. step backg. energy 0.000
Multiplet shift channel 2.000
Corrections Status
Decay correct to date: YES
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
4.0 0 0 0 0 0 0E + 0 0
4.0 0 0 0 0 0 0E + 0 0
0.000%
average of three points,
12.000
Comments
1/1/2012 11:00:00 AM
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0476
* * * * * CJ
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq
46 . 59
50574.
0 . 65
0 . 82
2 . 218E-02
46 . 54
4 .250
1.504E+04
Pb210
59 . 56
50333.
0 . 68
0 . 81
3 . 183E-02
59 . 54
35 .700
1.231E+03
AM241
o
00
o
[>
1766 .
9.08
0 . 85
3.816E-02
72 . 87
3614 .
4 . 56
0 . 85
3.911E-02
74 . 96
1613 .
9 . 70
0 . 85
3.999E-02
87 . 94
80693.
0 . 50
0 . 85
4.4 02E-02
88 . 03
3 .610
1.605E+04
CD109
121. 95
39343.
0 . 74
0 . 89
4.564E-02
122.06
85.600
3.487E+02
C057
136 .41
4721.
3 . 34
0 . 95
4.398E-02
165 . 87
40014.
0 . 68
0 . 96
3.963E-02
165.85
79 . 900
5.422E+02
Cel3 9
255.13
1516 .
9.66
0 . 98
2.966E-02
279.21
26998.
0.85
1 . 06
2.788E-02
279.17
81.500
1.191E+03
Hg2 03
391.78
29352.
0 . 72
1 . 16
2.199E-02
391.69
64.000
9.741E+02
SN113
661.71
21369.
0 . 89
1 .42
1.504E-02
661.66
85.210
4.657E+02
CS137
898 . 02
35979.
0 . 66
1. 68
1.196E-02
898.02
93 .700
1.563E+03
Y898
1173 . 16
24887.
0 . 79
1.85
9.749E-03
1173.24
99.900
7.323E+02
Coll73
1332 . 44
22381.
0 . 80
2 . 01
8.83 IE-03
1332.50
99.982
7.264E+02
Col332
1836 . 03
22571.
0 . 73
2.47
6.855E-03
1836.01
99.200
1.616E+03
Y1836
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
282.89
291.19
299.57
545 . 58
70.78
72 . 85
74 . 94
136.41
11968.
11762 .
11439.
6353 ,
1765. 4 . 626E + 04 9.08 0.845
3610. 9 .232E + 04 4.56 0.847
1606. 4 . 017E + 04 9.74 0.849
4721. 1.073E+05 3.34 0.952
D
D
D
Page 437 of 551
-------
ORTEC g V - i (1087) Env32 G53W4.25 3/28/2012 11:31:04 AM
TestAmerica Spectrum name: 3_TunaCan_20120996.Anl
Channel Energy Background Net area Eff*Area Uncert FWHM Suspected
1020.86 255.13 4778. 1516. 5.109E+04 9.66 0.975 - S
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EnergyStandardMix & Pb.Lib
D E N T I
F I E D P
E A K
S U M M A R
Y ft************
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
Pb-210
185.95
4 6 . 5 9
15712 .
50574 .
14.048
0 . 65
0 . 824
AM-241
237.88
59 . 56
16997 .
50333 .
13.981
0 . 68
0 . 815
CD -10 9
351.51
87 . 94
18663 .
80693.
22 .415
0 . 50
0 . 853
CO-5 7
487.69
121.95
10697.
39343 .
10 . 929
0 . 74
0 . 893
Ce-139
663.54
165.87
7740 .
40014 . '
11.115
0 . 68
0 . 956
Hg-2 03
1117 .25
279.21
5084 .
26998 .
7 .499
0 . 85
1 . 064
SN-113
1567 .81
391.78
3251.
29352 .
8 . 153
0 . 72
1. 160
CS-137
2647.99
661.71
2996 .
21369.
5 . 936
0 . 8 9
1.417
Y-898
3593 .36
898.02
2796 .
35979.
9 . 994
0 . 66
1. 677
Co-1173
4693.73
1173.16
1727 .
24887 .
6 . 913
0 . 79
1. 854
Co-13 32
5330.55
1332.44
1300 .
22381.
6.217
0 . 80
2 . 010
Y-1836
7343.2 9
1836.03
413 .
22571.
6 .270
0 . 73
2 .474
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OP LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq keV Bq Bq COMMENTS
Pb-210 N 1 .5038E + 04 8.15E+03
46.54 1.504E+04 ( 1.745E+02 6.50E-01 4.25E+00 G
AM-241 1 .2311E+03 1.58E+05
59.54 1.231E+03 ( 1.493E+01 6.75E-01 3.57E+01 G
CD-109 1.6045E + 04 4.63E+02
88.03 1.605E+04 ( 1.271E+02 4.98E-01 3.61E+00 G
CO-57 3 .4 866E+02 2.72E+02
122.06 3.487E+02 ( 4.295E+00 7.36E-01 8.56E+01 G
Page 438 of 551
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ORTEC g v - i (1087) Env32 G53W4.25 3/28/2012 11:31:04 AM
Spectrum name: 3_TunaCan_20120996.Anl
TestAmerica
Nuclide Ave activity
Energy Activity Code Peak MDA Comments
Ce-139
Hg-203
SN-113
CS-137
Y-898
Co-1173
Co-13 3 2
Y-183 6
5.4218E+02
1.1909E+03
9 . 7414E+02
4 . 6573E + 02
1. 5629E + 03
7 . 3225E+02
7 . 2640E+02
1. 6163E+03
165.85 5.422E+02
279.17 1.191E+03
391.69 9.741E+02
661.66 4.657E+02
398.02 1.563E+03
1173.24 7.323E+02
1332.50 7.264E+02
1836.01 1.616E+03
1.38E+02
5.592E + 00 6.78E-01 7.99E + 01 G
4.66E+01
1.478E+01 8.48E-01 8.15E+01 G
1.15E+02
8.908E+00 7.23E-01 6.40E+01 G
1.10E+04
5.618E + 0 0 8.92E-01 8.52E + 01 G
1.07E+02
1.082E+01 6.55E-01 9.37E+01 G
1.93E+03
5.778E+00 7.93E-01 9.99E+01 G
1.93E+03
5 . 541E + 00 8.01E-01 1.00E + 02 G
1.07E+02
6.976E+00 7.29E-01 9.92E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T - Thermal Neutron Activation G
F - Fast Neutron Activation X
I - Fission Product P
N - Naturally Occurring Isotope S
Gamma Ray
X-Ray
Positron Decay
Single-Escape
Page 439 of 551
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ORTEC g v - i (1087) Env32
TestAmerica
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
4.25 3/28/2012 11:31:04 AM
rum name: 3_TunaCan_20120996.Anl
D - Double-Escape
K - Key Line
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
* * * *
SUMMARY
OF N U C L I
D E S IN
SAMPLE
rt * * it rt
Time of Count
Time Corrected
Uncertainty
1 Sigma
Nuclide
Activity
Bq
Activity
Bq
Counting
MDA
Pb-210
1,4 92 7E + 04
1. 5038E+04
6.504E-01%
1.74E+02
AM-241
1.2307E+03
1. 2311E + 03
6.752E-01%
1.49E+01
CD-10 9
1.4098E+04
1.604 5E + 04
4.981E-01%
1.27E+02
CO-57
2.7 97 6E+02
3.4 866E + 02
7.363E-01%
4.30E+00
Ce-139
3.5103E+02
5.4218E+02
6.778E-01%
5.59E+00
Hg-203
3.3004E+02
1.1909E+03
8.4 8 0E-01%
1.48E+01
SN-113
5.7 92 0E+02
9.7414E+02
7.232E-01%
8.91E+00
CS-137
4.632 0E + 02
4.6573E+02
8.922E-01%
5.62E+00
Y-898
8.9159E+02
1.5 62 9E+03
6.551E-01%
1.08E+01
Co-1173
7.0984E+02
7.3225E+02
7.934E-01%
5.78E+00
Co-13 32
7.0417E+02
7.2640E+02
8.009E-01%
5.54E+00
Y-183 6
9.2 2 05E + 02
1.6163E+03
7.286E-01%
6.98E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 77.1 to 2000.4 keV) 3.549E+04 Bq
Total Decayed Activity ( 77.1 to 2000.4 keV) 4.0473316E+04 Bq
Analyzed by:
Admin
Reviewed by: .
Supervisor
Laboratory: TestAmerica
Page 440 of 551
-------
Ge05 90099 solidcert2012.xls
Gamma Verification per Geometry
Detector: Ge5
Geometry:
Reference date
Calibration Standard:
Standard volume g / vial
Standard volume transferred in g / geometry
lab ID# of cal standard
Tunacan
1/1/2012
90099
1550
317.8
Rad12-0007
Isotope
Certified Activity
gammas/sec
Geometry
Activity
aammas/sec
y abundance
Bq/sample
Count
Results
%recovery
Pb-210
3094
634
0.0425
14926
14353
96.2
Am-241
2037
418
0.3590
1163
1230.2
105.7
Cd-109
2881
591
0.0361
16363
16101
98.4
Co-57
1511
310
0.8560
362
347.72
96.1
Ce-139
2139
439
0.7990
549
538.4
98.1
Hg-203
4651
954
0,8146
1171
1208.4
103.2
Sn-113
3015
618
0.6400
966
972.07
100.6
Cs-137
1938
397
0.8510
467
462.35
99.0
Y-88
7264
1489
0.9370
1589
1559.3
98.1
Co-60
3580
734
0.9997
734
722.51
98.4
Co-60
3581
734
0.9999
734
739.67
100.7
Y-88
7690
1577
0.9920
1589
1613.8
101.5
Reviewed By: Jody Watson
Date: 3/27/2012
SOP: ST-RD-0102 current rev
CalVerif_tuna can
Page 441 of 551
-------
Calibration Data from file: 5_Soil_TunaCan.Clb
Energy Calibration Date: 3/27/2012 Time: 5:20:02 PM
Efficiency Calibration Date: 3/27/2012 Time: 5:20:37 PM
Calibration Description:
5 Soil TunaCan 90099 032612
Energy Calibration Fit
Energy = 0.1351 +0.24983l*Channel +2.72022e-008*Channel**2
FWHM (ch) = 2.8138 +0,001050*Channel -2.57606e-008*Channel**2
Energy/FWHM Table-
Channel Energy(keV) Fit(keV)
Delta FWHM(keV) Fit(keV)
Delta
186.01
46 . 54
46 . 61
-0 . 15%
0 . 74
0 . 75
-1 . 17%
237.86
59 . 54
59 .56
-0 . 04%
0 . 74
0 .77
-4.07%
351.46
88 . 03
87 . 95
0 . 10%
0 . 80
0.79
1.28%
487.52
122.06
121 . 94
0 . 10%
0 . 85
0 . 83
2 . 66%
663.26
165 . 85
165.85
0.00%
0 . 88
0 . 87
0 . 98%
1116.90
279.17
279 .20
-0.01%
0 . 97
0 . 99
-2.35%
1567 .36
391.69
391.78
-0.02%
1 . 12
1 . 10
1 . 78%
2647 . 45
661.66
661.74
-0,01%
1.38
1.35
1 . 91%
3592.51
898,02
898.01
0.00%
1 . 55
1.56
-1.11%
4692.96
1173 . 24
1173.18
0 . 00%
1 . 77
, 1.79
-1 . 18%
5329.72
1332.50
1332 .44
0 . 00%
1.93 i
1. 92
0.31%
7342.77
1836.01
1836 . 05
-0.00%
v/
2 .29
2.29
0 . 24%
~
Efficiency Calibration Fit
Knee Energy = 165.85 keV
Above the Knee: Quadratic Uncertainty = 0.8682 %
Ln(Eff) = 0.6466 -0.783045*Ln(Eng) -0.0041175*(Ln(Eng))**2
Below the Knee: Quadratic Uncertainty = 1.4296 %
Ln(Eff) = -24.6225 +9.075211*Ln(Eng) -0 . 966442*(Ln(Eng) )**2
Efficiency Table
Energy
Efficiency
Fit
Delta
46 . 54
1.7205E-002
1. 7882E-002
-3 . 93%
59.54
2.6619E-002
2 . 5335E-002
4.82%
88.03
3.4045E-002
3 . 4617E-002
-1. 68%
122 . 06
3.43 94E-002
3 . 5819E-002
-4 , 15%
165.85
TT n
165.85
3 . 0704E-002
3.133 IE-002
-2 . 04%
279.17
2.1030E-002
2.0365E-002
3 . 17%
391.69
1.5475E-002
1.5370E-002
0 . 68%
661 . 66
9.8486E-003
9.9244E-003
-0.77%
898.02
7.5404E-003
7.6837E-003
-1.90%
1173 . 24
6.0360E-003
6.13 8IE- 0 03
-1.69%
1332.50
5.5560E-003
5.5144E-003
0.75%
1836.01
4.2722E-003
4.2078E-003
1.51%
J
Calibration Certificate Table
Isotope
Energy
Pet
Halflife
Activity
GPS
Error
Date & '
Time
Pb-210
46 .54
4 . 2 5
8.15E+0d3
14918.00
634.00
4 .10%
1/1/2012
11 : 00:00
AM
Am-241
59 . 54
35.70
1.58E+005
1170.90
418.00
3 .50%
1/1/2012
11:00: 00
AM
Cd-109
88 . 03
3 . 61
4.63E+002
16371.00
591.00
4.70%
1/1/2012
11:00: 00
AM
Co-5 7
122.06
85 . 60
2.72E+002
362.15
310.00
4 . 10%
1/1/2012
11:00: 00
AM
Ce-139
¦ 165.85
79 . 90
1.38E+002
549.44
439.00
3 . 90%
1/1/2012
11:00:00
AM
Hg-2 03
279.17
81.50
4,66E+001
1170.60
954.00
3.80%
1/1/2012
11:00:00
AM
Sn-113
391.69
64 . 00
1,15E+002
965.63
618.00
3 . 90%
1/1/2012
11:00:00
AM
Cs-13 7
661.66
85.21
1.10E+004
465.91
397.00
4 . 00%
1/1/2012
11:00 : 00
AM
Y-88
898.02
93 . 70
1.07E+002
1589.10
1489.00
3 . 90%
1/1/2012
11:00:00
AM
Co-60
1173.24
99 . 90
1.93E+003
734.73
734.00
4 . 00%
1/1/2012
11 : 00:00
AM
Co-60
1332 . 50
99 . 98
1.93E+003
734.15
734 . 00
4 . 00%
1/1/2012
11:00:00
AM
Y-88
1836.01
99.20
1.07E+002
1589 . 70
1577.00
4.00%
1/1/2012
11:00:00
AM
Page 442 of 551
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ORTEC g v - i (1087) Env32 G53W4.25 3/27/2012 5:22:03 PM
TestAmerica Spectrum name: 5_TunaCan_2 012 0 810.Anl
Sample description
5 TunaCan 90099 032612
Spectrum Filename; C:\User\SPC\Det5\5__TunaCan_20120810.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/26/2012 3:05:42 PM
3600
3652
1.44 %
5
Detector system
Ge 5 SN/157
Calibration
Filename:
5 Soil TunaCan 90099 032612
5 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Ef f):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine;
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/27/2012 5:20:02 PM
0.135 keV
0.250 keV/channel
2.720E-08 keV/channela2
PM
3/27/2012 5:20:37
165.85 keV
Quadratic Uncertainty = 0.87
6.4 6 6115E- 01 + (-7 . 8 3 0 4 5 4 E- 01* Log(E) )
( -4.117504E-03*Log(E)*2 )
Quadratic Uncertainty = 1.43
-2.462251E+01 + ( 9.075211E+00*Log(E) )
( -9.664422E-01*Log(E)A2 )
DET EnergyStandardMix & Pb.Lib
0 . 500
Library based
Env32 G53W4.25
150 ( 3 7.61keV )
5000 ( 2000.5 3keV )
10.000%
3
1.0000E+00
1 . 0000E + 00/ ( 1.0000E + 00* 1.0000E + 00)
1.OOOOE+OO
Reg. Guide 4.16 Method
Page 443 of 551
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ORTEC g v
TestAmerica
i (1087) Env3 2 G53W4.25 3/27/2012 5:22:03 PM
Spectrum name: 5__TunaCan_2 012 0 810 . Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0 0 0 0 0 0 0E+0 0
4.0 0 0 0 0 0 0E + 0 0
0 . 000%
average of three points,
12.000
2.000
0.000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
1/1/2012 11:00:00 AM
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0527
t * * -k * CJ
U M M A
R Y 0
F P E
A K S I
N RAN
G E
•k * * * rt
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act .
Nuc
Energy
Factor
Energy
Ratio
Bq
46.61
38986.
0 . 74
0 . 74
1. 793E-02
46.54
4.250
1 . 435E + 04
Pb210
59.56
40041.
0 . 74
0 . 74
2 . 535E-02
59 . 54
35.700
1.23 0E + 03
AM241
70.85
1493 .
9 .22
0 . 78
3 . 019E-02
72 . 87
2354 .
5 . 96
0 . 78
3.089E-02
87 , 95
63754.
0 . 53
0 . 80
3.460E-02
88.03
3 . 610
1.610E+04
CD109
121.94
30888.
0 . 76
0 . 85
3,583E-02
122 . 06
85 . 600
3.477E+02
C057
13 6.41
3768 ,
3.80
0 . 89
3.457E-02
165 . 85
31597.
0 . 74
0 . 88
3.066E-02
165.85
79.900
5.384E+02
Cel39
279.20
20358.
0 . 87
0 . 97
2.036E-Q2
279.17
81 .500
1.208E+03
Hg2 03
391.78
20611.
0 . 93
1 . 12
1.53 7E- 02
391.69
64 . 000
9.721E+02
SN113
661 . 74
14000.
1 . 10
1.38
9.923E-03
661 . 6 6
85.210
4.623E+02
CS137
898.01
23228.
0 . 82
1 , 55
7.684E-03
898.02
93 . 700
1,559E+03
Y898
1173.18
15468.
0 . 93
1 . 77
6.138E-03
1173.24
99.900
7.225E+02
Coll73
1332.44
14238.
0 . 98
1. 93
5.515E-03
1332.50
99.982
7.397E+02
Col3 3 2
1836.04
13938.
0 . 87
2.30
4.208E-03
1836 .01
99.200
1.614E+03
Y1836
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
291.16 72.88 8722 . 2253. 7.295E + 04 7.09 0.801 - ' '
545.44 136.41 5274. 3768. 1.090E+05 3.80 0.888
Page 444 of 551
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ORTEC g v - i (1087) Env32 G53W4.25 3/27/2012 5:22:03 PM
TestAmerica Spectrum name: 5_TunaCan__20120810 . Anl
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EnergyStandardMix & Pb.Lib
************** J
D E N T I
F I E D P
E A K
S U M M A R
Y *************
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
Pb-210
186.01
46 . 61
12895.
38986.
10.829
0.74
0 . 743
AM-241
2 3 7.86
59.56
13293.
40041.
11.122
0 . 74
0 . 735
CD-10 9
351.46
87 . 95
12894.
63754 .
17.710
0 . 53
0.805
CO-57
487.52
121.94
6935 .
30888.
8.580
0 . 76
0 . 852
Ce-139
663 .26
165.85
5616 .
31597 .
8 . 777
0 . 74
0.883
Hg-203
1116.90
279.20
2848 .
20358 .
5 , 655
0 . 87
0 . 966
SN-113
1567.36
391.78
3046 .
20611.
5.725
0 . 93
1 . 119
CS-13 7
2647 . 45
661 . 74
1982 .
14000 .
3.889
1 . 10
1.380
Y-898
3592 .51
898 . 01
1944 .
2322 8.
6.452
0 . 82
1 . 547
Co-1173
4692.96
1173.18
847 .
15468.
4.297
0 , 93
1 . 774
Co-1332
5329 . 75
1332.44
693 .
14238.
3 . 955
0 . 98
1. 927
Y-1836
7342.72
1836.04
102 .
13938.
3 . 872
0 . 87
2 . 295
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq keV Bq Bq COMMENTS
Pb-210 N 1.4353E+04 8.15E+03
46.54 1 .435E+04 ( 1.958E + 02 7.44E-01 4.25E + 00 G
AM-241 1.2302E+03 1 . 58E + 05
59.54 1.230E+03 ( 1.659E+01 7.44E-01 3.57E+01 G
CD-10 9 1.6101E + 04 4.63E+02
88.03 1 . 610E + 04 ( 1.343E + 02 5.28E-01 3.61E + 00 G
CO-57 3.4772E+02 2.72E+02
122.06 3 .477E+02 ( 4.399E + 00 7.60E-01 8.56E + 01 G
Page 445 of 551
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ORTEC g v
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i (1087) Env32 G53W4.25 3/27/2012 5:22:03 PM
Spectrum name: 5_TunaCan_20120810.Anl
Nuclide Ave activity
Ce-139 5.3 84 0E + 02
Energy
Activity Code Peak MDA Comments
Hg-2 03
SN-113
CS-13 7
Y-898
Co-1173
Co -13 3 2
Y-18 3 6
1.2084E+03
9.7207E+02
4.62 3 5E + 02
1.5593E+03
7.2251E+02
7.3967E+02
1,613 8E + 03
165.85 5 . 3 84E + 02
279.17 1.20 8E + 0 3
391.69 9.721E+02
661.66 4 , 623E + 02
898.02 1.559E+03
1173.24 7.225E+02
1332.50 7 . 3 97E + 02
1836.01 1. 614E + 03
1,38E+02
5.9 97E + 0 0 7.36E-01 7.99E + 01 G
4.66E+01
1.492E+01 8.69E-01 8.15E+01 G
1.15E+02
1.22 6E + 01 9.3 IE- 01 6.40E + 01 G
1.10E+04
6.941E+00 1.10E+00 8.52E+01 G
1.07E+02
1.397E+01 8.19E-01 9.37E+01 G
1.93E+03
6.463E+00 9.30E-01 9.99E+01 G
1.93E+03
6.515E + 00 9.82E-01 1.00E + 02 G
1.07E+02
5.77 6E + 0 0 8.71E-01 9.92E + 01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW2 5M, but ok at PWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
Page 446 of 551
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ORTEC g v - i (1087) Env32 G53W4.25 3/27/2012 5:22:03 PM
TestAmerica Spectrum name: 5_TunaCan_2 012 0810.Anl
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
D - Double-Escape
K - Key Line
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
Peakbackground subtraction
Nuclide
SUMMARY
Time of Count
Activity
OP NUCLIDES IN
Time Corrected Uncertainty
Activity Counting
SAMPLE
1 S igma
MDA
Bq
Bq
210
1.42 5 0E + 04
1.4353E+04
7.43 9E- 01%
1.96E+02
241
1.2 2 97E + 03
1.23 02E + 03
7.442E-Q1%
1.66E+01
109
1.4172E+04
1.6101E+04
5.277E-01%
1.34E+02
57
2.7 9 8 3E + 02
3.4772E+02
7.604E-01%
4.4 0E+0 0
139
3.5 0 61E+02
5.3840E+02
7 . 359E-01%
6.00E+00
203
3.4071E+02
1.2084E+03
8.687E-01%
1.49E+01
113
5.82 0 0E + 02
9.7207E+02
9.315E-01%
1.23E+01
137
4.5987E+02
4.6235E+02
1,0 97E+0 0%
6.94E+00
98
8.962 0E + 02
1.5 5 93E+0 3
8.189E-01%
1,40E+01
1173
7.0069E+02
7.2 2 51E + 0 2
9.300E~01%
6.46E+00
1332
7.1733E+02
7.3967E+02
9.82 IE-01%
6.52E+00
836
9.2756E+02
1.6138E+03
8.71IE-01%
5.78E+00
Pb-
AM-
CD-
C0-
Ce-
Hg-
SN-
CS-
Y-E
Co-
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
s u M M A R
Total Activity ( 37.6 to 2000.5 keV)
Total Decayed Activity ( 37.6 to 2000.5
Analyzed by:
Y
3.4 91E+04 Bq
keV) 3.984 8164E+04
Bq
Admin
Reviewed by:
Supervisor
Laboratory: TestAmerica
Page 447 of 551
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Ge07 90099 solidcert2012TALS.xls
Gamma Verification per Geometry
Detector: Ge7
Geometry: Tunacan
Reference date 1/1/2012
Calibration Standard: 90099
Standard volume g / vial 1550
Standard volume transferred in g / geometry 317.8
lab ID# of cal standard 6699
Isotope
Certified Activity
gammas/sec
Geometry
Activity
aammas/sec
yabundance
Bq/sample
Count
Results
%recovery
Pb-210
3094
634
0.0425
14926
14726
98.7
Am-241
2037
418
0.3590
1163
1241.6
106.7
Cd-109
2881
591
0.0361
16363
15976
97.6
Co-57
1511
310
0.8560
362
346.77
95.8
Ce-139
2139
439
0.7990
549
539.48
98.3
Hq-203
4651
954
0.8146
1171
1199.2
102.4
Sn-113
3015
618
0.6400
966
976.76
101.1
Cs-137
1938
397
0.8510
467
467.66
100.2
Y-88
7264
1489
0.9370
1589
1567.3
98.6
Co-60
3580
734
0.9997
734
726.23
98.9
Co-60
3581
734
0.9999
734
719.64
98.0
Y-88
7690
1577
0.9920
1589
1635.7
102.9
Reviewed By: Jody Watson
Date: 3/16/2012
SOP: ST-RD-0102 current rev CalVerif_tuna can (2)
Page 448 of 551
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Calibration Data from file: 7__Soil_TunaCan. Clb
Energy Calibration Date: 3/16/2012 Time: 11:44:50 AM
Efficiency Calibration Date: 3/16/2012 Time: 11:45:14 AM
Calibration Description:
7 TunaCan 90099 030512
Energy Calibration Fit
Energy = 0.1533 +0.249954*Channel +6.71576e-009*Channel**2
FWHM (ch) = 3.2969 +0.001030*Channel -2.25091e-008*Channel**2
Energy/FWHM Table
Channel Energy(keV) Fit(keV) Delta FWHM(keV) Fit(keV) Delta
185.73
46.54
46.58
-0.08%
0.86
0.87
-1.80
237.72
59.54
59. 57
-0.06%
0.8 6
0.88
-3.29
351.56
88.03
88 . 03
0.00%
0.91
0. 91
-0 .17
487.42
122.06
121.99
0.06%
0.97
0. 95
2 . 36
662.55
165.85
165.76
0.05%
1. 00
0. 99
1.26
1116.52
279.17
279.24
-0.03%
1.13
1.10
1.85
1566.54
391.69
391.73
-0.01%
1. 21
1.21
-0.23
2646.25
661.66
661.64
0.00%
1.47
1.47
0 . 54
3591.85
898.02
898.04
-0.00%
1. 66
1. 68
-1.15
4692.53
1173.24
1173.22
0.00%
1. 92
1. 91
0 . 69
5329.58
1332.50
1332.49
0.00%
2 . 02
2.04
-0 . 87
7343.37
1836.01
1836.02
-0.00%
2 .42
2 .41
0.28
Efficiency Calibration Fit
Knee Energy = 165.85 keV
Above the Knee: Quadratic Uncertainty = 0.8690 %
Ln(Eff) = 0.6717 -0.616654*Ln(Eng) -0.0206592*(Ln(Eng))**2
Below the Knee: Quadratic Uncertainty = 1.4845 %
Ln(Eff) = -26.8969 + 10 .195443*Ln(Eng) -1.08167*(Ln(Eng))**2
Efficiency Table
Energy
Efficiency
Fit
Delta
46. 54
2.3732E-002
2.4829E-002
-4 . 62%
59.54
3.9252E-002
3. 7016E-002
5.70%
88.03
5.1999E-002
5. 3285E-002
-2.47%
122.06
5.367 9E-002
5.6057E-002
-4.43%
165.85
T '
i\ii6S
165.85
4.7932E-002
4.8811E-002
-1.83%
279.17
3.2 322E-002
3.1541E-002
2.42%
391.69
2. 3837E-002
2.3601E-002
0.99%
661. 66
1.4947E-002
1.4 924E-002
0.15%
898.02
1.1205E.-002
1.1367E-002
-1.45%
1173.24
8.8255E-003
8.9287E-003
-1.17%
1332.50
7.7 833E-003
7.9508E-003
-2.15%
1836.01
6. 0876E-003
5.9192E-003
2.77%
Calibration Certificate Table
Isotope
Energy
Pet
Halflife
Activity
GPS
Error
Date & 1
Time
Pb-210
46. 54
4 . 25
8 .15E+003
14941.00
635.00
4 .10%
1/1/2012
11:00:00
AM
Am-241
59. 54
35.70
1.58E+005
1170.90
418.00
3.50%
1/1/2012
11:00:00
AM
Cd-109
88.03
3. 61
4.63E+002
16371.00
591.00
4.70%
1/1/2012
11:00:00
AM
Co-57
122.06
85. 60
2.72E+002
362.15
310.00
4 .10%
1/1/2012
11:00:00
AM
Ce-139
165.85
79. 90
1.38E+002
549.44
439.00
3. 90%
1/1/2012
11:00:00
AM
Hg-203
279.17
81.50
4.66E+001
1170.60
954 . 00
3.80%
1/1/2012
11:00:00
AM
Sn-113
391.69
64 . 00
1.15E+002
967.19
619.00
3. 90%
1/1/2012
11:00:00
AM
Cs-137
661.66
85.21
1.10E+004
4 67.08
398.00
4 . 00%
1/1/2012
11:00:00
AM
Y-88
898.02
93. 70
1.07E+002
1590.20
1490.00
3. 90%
1/1/2012
11:00:00
AM
Co-60
1173.24
99.90
1.93E+003
734.73
734.00
4.00%
1/1/2012
11:00:00
AM
Co-60
1332.50
99. 98
1.93E+003
735.15
735.00
4.00%
1/1/2012
11:00:00
AM
Y-88
1836.01
99. 20
1.07E+002
1590.70
1578 . 00
4.00%
1/1/2012
11:00:00
AM
Page 449 of 551
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TestAmerica Spectrum name: 7_TunaCan_20120388.An!
Sample description
7 TunaCan 90099 030512
Spectrum Filename: C:\User\SPC\Det7\7_TunaCan_20120388.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/5/2012 2:07:36 PM
3600
3721
3.25 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
7 TunaCan 90099 032712
7 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
3/16/2012 11:44:50 AM
0.153 keV
0.250 keV/channel
6.716E-09 keV/channelA2
3/16/2012 11:45:14 AM
165.85 keV
Quadratic Uncertainty = 0.87 %
6.716580E-01 + (-6.166540E-01*Log(E) ) +
( -2.065917E-02*Log(E)A2 )
Quadratic Uncertainty = 1.48 %
-2.689695E+01 + ( 1.019544E+01*Log(E) ) +
( -1.081671E+00*Log(E)A2 )
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
DET_EnergyStandardMix & Pb.Lib
0.500
Library based
Env32 G53W4.25
150 ( 37.65keV )
8000 ( 2000.21keV )
10 . 000%
3
1.0000E+00
1.0000E+00/(
1.0000E+00
Reg. Guide 4,
1.0000E+00* 1. 0000E+00) =
16 Method
Page 450 of 551
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TestAmerica Spectrum name: 7_TunaCan_20120388.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4 . 0000000E+00
4.0000000E+00
0.000%
average of three points,
12.000
2.000
0.000
2.000
Corrections Status
Decay correct to date: YES
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
1/1/2012 11:00:00 AM
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0324
***** SUMMARY OF PEAKS IN
Peak Area Uncert FWHM Corrctn
Energy Factor
RANGE
Nuclide Brnch.
Energy Ratio
Act.
Nuc
46. 63
53946.
0.53
0.87
2 . 487E-02
46.54
4 .250
1.428E+04
Pb210
59.57
59050.
0. 65
0.86
3.7 04E-02
59.54
35.700
1.242E+03
AM241
70.74
2770.
6.58
0. 90
4.527E-02
72. 95
4536.
4.27
0. 90
4.661E-02
88 . 03
100494.
0.43
0. 91
5.328E-02
88.03
3. 610
1.598E+04
CD109
121.99
50865.
0.71
0. 97
5.606E-02
122 .06
85.600
3.4 68E+02
C057
136.41
6524.
3.77
0. 93
5.411E-02
165.76
54838.
0.57
1.00
4.7 67E-02
165.85
79.900
5.395E+02
Cel39
255.13
1772.
7.37
1.21
3.404E-02
279.24
42776.
0.59
1.13
3.153E-02
279.17
81.500
1.199E+03
Hg203
391.73
36096.
0. 66
1.21
2.360E-02
391.69
64.000
9.7 68E+02
SN113
661.68
21323.
0.77
1.47
1.4 92E-02
661.66
85.210
4.677E+02
CS137
898.03
39603.
0. 63
1. 66
1.137E-02
898.02
93.700
1.567E+03
Y898
1173.21
22788.
0.85
1. 92
8.929E-03
1173.24
99.900
7.2 62E+02
Coll7 3
1332.49
20124.
0.85
2 . 02
7.951E-03
1332.50
99.982
7.196E+02
Col332
1836.00
22787.
0.70
2 .43
5.919E-03
1836.01
99.200
1.636E+03
Y1836
************ UNIDENTIFIED
Peak Centroid Background Net Area
Channel Energy Counts Counts
PEAK SUMMARY * ***********
Efficiency Uncert FWHM Suspected
* Area 1 Sigma % keV Nuclide
282 .41
291.25
545.11
1020.07
70.73
72.94
136.41
255 .13
15146.
16305.
12980.
4580 .
2828. 6.248E+04 6.43 0.896
4682. 1.005E+05 4.12 0.899
6524. 1.206E+05 3.77 0.932
1772. 5.204E+04 7.37 1.209
Page 451 of 551
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TestAmerica Spectrum name: 7_TunaCan_20120388.Anl
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EnergyStandardMix & Pb.Lib
************** IDENTIFIED PEAK SUMMARY **************
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
Pb-210
185.73
46.58
19825.
55636.
15.454
0. 65
0.856
AM-241
237.72
59.57
21942.
59050.
16.403
0. 65
0.857
CD-109
351.56
88 . 03
21396.
100494.
27.915
0.43
0 . 912
CO-57
487.42
121.99
16859.
50865.
14.129
0.71
0. 971
Ce-139
662.55
165.76
9893.
54838.
15.233
0.57
1.005
Hg-203
1116.52
279.24
5111.
42776.
11.882
0.59
1.126
SN-113
1566.54
391.73
4106.
36096.
10.027
0. 66
1.211
CS-137
2646.33
661.66
2922.
21323.
5. 923
0.77
1. 4 66D
Y-898
3591.84
898.03
3210.
39603.
11.001
0. 63
1. 659
Co-1173
4692.50
1173.21
1804 .
22788.
6.330
0.85
1. 924
Co-1332
5329.58
1332.49
1286.
20124 .
5 .590
0.85
2 . 020
Y-1836
7343.30
1836.00
283.
22787 .
6.330
0.70
2. 426
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY
- Nuclide - Average
Name Code Activity
Bq
Pb-210 N 1.472 6E+04
AM-241
1. 2416E+03
OF LIBRARY PEAK USAGE *****
Peak
Energy Activity Code MDA Value
keV Bq Bq COMMENTS
8 .15E+03
46.54 1.473E+04 ( 1.744E+02 6.52E-01 4.25E+00 G
1.58E+05
59.54 1.242E+03 ( 1.457E+01 6.49E-01 3.57E+01 G
CD-109
CO-5 7
1.597 6E+04
3.4677E+02
.03 1.598E+04 (
4.63E+02
1.088E+02 4.29E-01 3.61E+00 G
2.72E+02
122.06 3.468E+02 ( 4.144E+00 7.08E-01 8.56E+01 G
Page 452 of 551
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ORTEC g v
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i (1087) Env32 G53W4.25 2/28/2014 11:43:43 AM
Spectrum name: 7_TunaCan_2012038 8.Anl
Nuclide Ave activity
Ce-139 5. 3948E+02
Energy
Activity Code Peak MDA Comments
Hg-203
SN-113
CS-137
Y-898
Co-1173
Co-1332
Y-1836
1.1992E+03
9.7 676E+02
4.67 66E+02
1.5673E+03
7.2623E+02
7.1964E+02
1.6357E+03
165.85 5.395E+02
279.17 1.199E+03
391.69 9.768E+02
661.66 4.677E+02
898.02 1.5 67E+03
1173.24 7.262E+02
1332.50 7.196E+02
1836.01 1.636E+03
1.38E+02
4.586E+00 5.65E-01 7.99E+01 G
4.66E+01
9.415E+00 5.92E-01 8.15E+01 G
1.15E+02
8.153E+00 6.55E-01 6.40E+01 G
1.10E+04
5.584E+00 7.73E-01 8.52E+01 G
1.07E+02
1.056E+01 6.2 9E-01 9.37E+01 G
1.93E+03
6.394E+00 8.53E-01 9.99E+01 G
1.93E+03
6.072E+00 8.54E-01 1.00E+02 G
1.07E+02
5.819E+00 7.02E-01 9.92E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
0 - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
Page 453 of 551
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ORTEC g v - i (1087) Env32
TestAmerica
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
'4.25 2/28/2014 11:43:43 AM
rum name: 7_TunaCan_20120388.Anl
D - Double-Escape
K - Key Line
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
•k -k -k -k -k
SUMMARY
OF N U C L I
D E S IN
SAMPLE
¦k -k -k -k -k
Time of Count
Time Corrected
Uncertainty
1 Sigma
Nuclide
Activity
Activity
Counting
MDA
Bq
Bq
Pb-210
1. 4646E+04
1. 4726E+04
6. 521E-01%
1. 74E+02
AM-241
1.2413E+03
1.2416E+03
6. 489E-01%
1. 46E+01
CD-109
1.4512E+04
1.5 976E+04
4 .292E-01%
1. 09E+02
CO-57
2.9445E+02
3 . 4677E+02
7.07 6E-01%
4.14E+00
Ce-139
3.9059E+02
5 .3948E+02
5.652E-01%
4.59E+00
Hg-203
4.6224E+02
1.1992E+03
5.917E-01%
9. 42E+00
SN-113
6.6381E+02
9.767 6E+02
6.552E-01%
8.15E+00
CS-137
4.6577E+02
4.67 66E+02
7 .730E-01%
5.58E+00
Y-898
1.032 9E+03
1.5673E+03
6.291E-01%
1.06E+01
Co-1173
7.0966E+02
7.2623E+02
0.534E-01%
6.39E+00
Co-1332
7.0321E+02
7.1964E+02
8.542E-01%
6.07E+00
Y-1836
1.0780E+03
1.6357E+03
7.017E-01%
5.82E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
SUMMARY
Total Activity ( 701.8 to 2000.2 keV) 3.620E+04 Bq
Total Decayed Activity ( 701.8 to 2000.2 keV) 4 . 0121711E+04 Bq
Analyzed by: _
Admin
Reviewed by:
Supervisor
Laboratory: TestAmerica
Page 454 of 551
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Ge08 90099 solidcert2012TALS.xls
Gamma Verification per Geometry
Detector: Ge8
Geometry: Tunacan
Reference date 1/1/2012
Calibration Standard: 90099
Standard volume g / vial 1550
Standard volume transferred in g / geometry 317.8
lab ID# of cal standard 6699
Isotope
Certified Activity
gammas/sec
Geometry
Activity
aammas/sec
y abundance
Bq/sample
Count
Results
%recovery
Pb-210
3094
634
0.0425
14926
14960
100.2
Am-241
2037
418
0.3590
1163
1240.5
106.6
Cd-109
2881
591
0.0361
16363
16066
98.2
Co-57
1511
310
0.8560
362
345.12
95.4
Ce-139
2139
439
0.7990
549
536.34
97.7
Hg-203
4651
954
0.8146
1171
1218.2
104.1
Sn-113
3015
618
0.6400
966
967.15
100.1
Cs-137
1938
397
0.8510
467
465.86
99.8
Y-88
7264
1489
0.9370
1589
1552.1
97.6
Co-60
3580
734
0.9997
734
724.48
98.7
Co-60
3581
734
0.9999
734
729.98
99.4
Y-88
7690
1577
0.9920
1589
1627.2
102.4
Reviewed By: Jody Watson
Date: 3/28/2012
SOP: ST-RD-0102 current rev
CalVerifJuna can
Page 455 of 551
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Calibration Data from file: 8_Soil_TunaCan.Clb
Energy Calibration Date: 3/28/2012 Time: 10:35:07 AM
Efficiency Calibration Date: 3/28/2012 Time: 10:35:20 AM
Calibration Description:
8 Soil TunaCan 90099 032712
Energy Calibration Fit
Energy = 0.0505 +0.250025*Channel +8.06699e-010*Channel**2
FWHM (ch) = 3.6351 +0.000832*Channel -2 . 49195e-008*Channel**2
Energy/FWHM Table
Channel Energy(keV) Fit(keV) Delta FWHM(keV) Fit(keV) Delta
185.74
46 .54
46 .49
0.11%
0 . 94
0 . 95
-0.61%
237 . 86
59.54
59 . 52
0 . 03%
0 . 95
0 . 96
-1.36%
351.89
88 . 03
88 . 03
-0.00%
0 . 97
0.98
-1. 63%
488.04
122 .06
122.07
-0.01%
1. 01
1. 01
0 . 12%
663 .26
165 . 85
165.88
-0.02%
1. 07
1. 04
2 . 17%
1116.59
279.17
279.23
-0.02%
1. 15
1.13
1.73%
1566.40
391.69
391.69
-0.00%
1.22
1.22
0.24%
2645.92
661.66
661.60
0 . 01%
1.39
1 .42
-1.95%
3591.62
898 .02
898.05
-0 . 00%
1. 61
1.58
2 . 16%
4692.17
1173 .24
1173 .23
0.00%
1. 74
1 . 75
-0.61%
5329.14
1332 .50
1332 .49
0.00%
1. 82
1 . 84
-1.05%
7342.97
1836.01
1836.02
-0.00%
2 . 11
2 .10
0 .42%
Efficiency
Calibration
Fit
Knee Energy = 165.
85 keV
Above the
Knee: Quadratic
Uncertainty =
1 .3942
%
Ln(Eff) = -0.1099 -0.495854*Ln(Eng) -0.0257227*(Ln(Eng))**2
Below the Knee: Quadratic Uncertainty = 1.7131 %
Ln(Eff) = -25.2530 +9.398253*Ln(Eng) -1.00003 *(Ln(Eng))**2
Efficiency Table
Energy Efficiency Fit Delta
46 . 54
1.9170E-0 02
2.0055E-002
-4.62%
59 . 54
3.052 6E-0 02
2.8813E-002
5 . 61%
88 . 03
3.9175E-0 02
3.9918E-002
-1.90%
122 . 06
3.9509E-002
4.1457E-002
-4.93%
165.85
165.85
3.5429E-002
3.62 91E-0 02
-2.43%
279.17
2.5270E-002
2.4275E-002
3 . 94%
391.69
1.85 82E-0 02
1.8550E-002
0 . 17%
661.66
1.2089E-002
1.2090E-002
-0.01%
898 . 02
9.1435E-003
9.3604E-003
-2 .37%
1173 . 24
7.34 87E-0 03
7.4527E-003
-1 .42%
1332.50
6.6398E-003
6.67 7 6E- 0 03
-0.57%
1836.01
5.1654E-003
5.0457E-003
2 . 32%
Calibration Certificate Table
Isotope
Energy
Pet
Halflife
Activity
GPS
Error
Date & 1
Time
Pb-210
46.54
4.25
8.15E+003
14918.00
634 .00
4.10%
1/1/2012
11:00:00
AM
Am-241
59 . 54
35,70
1.58E+005
1170.90
418.00
3 . 50%
1/1/2012
11:00:00
AM
Cd-109
88 . 03
3 . 61
4.63E+002
16371.00
591 .00
4 . 70%
1/1/2012
11:00:00
AM
Co-5 7
122.06
85 . 60
2.72E+002
362.15
310.00
4 . 10%
1/1/2012
11:00:00
AM
Ce-139
165.85
79.90
1.38E+002
549.44
439.00
3 . 90%
1/1/2012
11 : 00:00
AM
Hg-203
279.17
81.50
4.66E+001
1170.60
954.00
3 . 80%
1/1/2012
11:00:00
AM
Sn-113
391 . 69
64 . 00
1.15E+002
965.63
618.00
3 . 90%
1/1/2012
11:00:00
AM
Cs-13 7
661.66
85.21
1.10E+004
465.91
397.00
4 . 00%
1/1/2012
11:00: 00
AM
Y-88
898.02
93 . 70
1.07E+002
1589.10
1489.00
3 . 90%
1/1/2012
11:00: 00
AM
Co-60
1173.24
99 . 90
1.93E+003
734.73
734 . 00
4 . 00%
1/1/2012
11:00: 00
AM
Co-6 0
1332.50
99 . 98
1.93E+003
734.15
734.00
4 . 00%
1/1/2012
11:00: 00
AM
Y-88
1836.01
99.20
1.07E+002
1589.70
1577.00
4 . 00%
1/1/2012
11:00: 00
AM
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TestAmerica Spectrum name: 8_TunaCan_2 012 0 67 6.Anl
Sample description
8 TunaCan 90099 032712
Spectrum Filename: C:\User\SPC\Det8\8_TunaCan_20120676.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/27/2012 10: 58:29 AM
3600
3655
1.49 %
Detector system
Ge 8 SN/174
Calibration
Filename:
8 Soil TunaCan 90099 032712
8 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
3/28/2012 10:35:07 AM
0.050 keV
0.250 keV/channel
8.067E-10 keV/channelA2
3/28/2012 10:35:20 AM
165.85 keV
Quadratic Uncertainty = 1.39
-1.098764E-01 + (-4.958544E-0l*Log(E) )
( -2.572270E-02* Log(E)A 2 )
Quadratic Uncertainty = 1.71
-2.52 53 01E + 01 + ( 9.3 9 825 3E+0 0*Log(E) )
( -1.000034E+00*Log(E)a2 )
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
DET_EnergyStandardMix & Pb.Lib
0.500
Library based
Env32 G53W4.25
150 ( 37.55keV )
iOOO ( 2000.30keV )
10 . 000%
3
1.0000E+00
1.00 0 0E + 0 0/( 1.OOOOE + OO* 1.0000E + 00)
1.OOOOE+OO
Reg. Guide 4.16 Method
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Spectrum name: 8_TunaCan_2 012 067 6.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4 . 0000000E+00
4.0 0 0 0 0 0 0E + 0 0
0.000%
average of three points.
12 . 000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
1/1/2012 11:00:00 AM
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0205
• * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
rt * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
Bq
46 . 54
43426.
0 . 60
0 . 95
2.002E-02
46 . 54
4.250
1.426E+04
Pb210
59 . 52
45918.
0 . 77
0 . 95
2.880E-02
59 . 54
35 . 700
1.240E+03
AM241
72 . 86
2434 .
6 . 68
0 . 97
3.542E-02
88 . 03
73269.
0 . 53
0 . 97
3.992E-02
88 . 03
3 . 610
1.607E+04
CD109
122 . 07
35407.
0 . 77
1. 01
4 . 146E-02
122.06
85.600
3.451E+02
C057
136.51
4312 .
4 . 44
1. 06
3.999E-02
165.88
36308.
0 . 76
1. 07
3.62 9E-02
165.85
79.900
5.363E+02
Cel39
279.23
24162.
0 . 88
1. 15
2.427E-02
279.17
81.500
1.218E+03
Hg2 03
391.69
24625.
0 . 77
1 . 22
1.855E-02
391.69
64.000
9.671E+02
SN113
661.60
17184.
1 . 10
1.39
1.209E-02
661.66
85.210
4.659E+02
CS137
898.05
28015.
0 . 71
1.61
9.360E-03
898.02
93.700
1.552E+03
Y898
1173 .23
18826.
0 . 79
1.74
7.453E-03
1173.24
99.900
7.245E+02
Coll73
1332.49
17010.
0 . 84
1. 82
6.678E-03
1332.50
99.982
7.300E+02
Col332
1836.02
16762.
0 . 79
2 . 11
5.046E-03
1836.01
99.200
1.627E+03
Y1836
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
291.19 72.85 12003. 2434. 6 . 872E + 04 ' 6.68 0.969 : £T
545.78 136.51 8432. 4312. 1.078E+05 4.44 1.059 -
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TestAmerica Spectrum name: 8_TunaCan_20120676.Anl
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EnergyStandardMix & Pb.Lib
************** IDENTIFIED PEAK SUMMARY **************
Nuclide Peak Centroid Background Net Area Intensity Uncert FWHM
Channel Energy Counts Counts Cts/Sec 1 Sigma % keV
Pb-210
185.74
46.49
17505.
45568.
12 . 658
0 . 76
0 . 942
AM-2 41
237.86
59 . 52
18397.
45918.
12 . 755
0 .77
0 . 945
CD-109
351.89
88 . 03
17370.
73269.
20 . 353
0 . 53
0 . 966
CO-5 7
488.04
122.07
9639.
35407.
9 . 835
0 . 77
1.010
Ce-139
663.26
165.88
8356 .
36308.
10 . 085
0 . 76
1. 067
Hg-203
1116.59
279.23
4382 .
24162.
6 . 712
0 . 88
1. 153
SN-113
1566.40
3 91.69
2677 .
24625 .
6 . 840
0 . 77
1. 223
CS-137
2645.92
661.60
3145 .
17184.
4 . 773
1.10
1.389
Y-898
3591.62
898.05
1881.
28015 .
7 .782
0 . 71
1 . 611
Co-1173
4692.17
1173 .23
650 .
18826.
5.229
0 . 79
1. 738
Co-1332
5329.14
1332 .49
576 .
17010 .
4 . 725
0 . 84
1. 822
Y- 183 6
7342.97
1836.02
Ill.
16762.
4 . 656
0 . 79
2 . 110
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***¦>
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bg keV Bq Bq COMMENTS
Pb-210 N 1.4960E+04 8.15E+03
46.54 1.496E+04 ( 2.033E+02 7.55E-01 4.25E+00 G
AM-241 1.24 05E + 0 3 1.58E + 05
59.54 1. 240E + 03 ( 1.715E + 01 7.72E-01 3 . 57E + 01 G
CD-109 1.6 0 66E+04 4.63E + 02
88.03 1.607E + 04 ( 1.353E + 02 5.26E-01 3.61E + 00 G
CO-57 3.4512E+02 2.72E+02
122.06 3.451E+02 ( 4.486E+00 7.68E-01 8.56E+01 G
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TestAmerica
Nuclide Ave activity
Spectrum name: 8_TunaCan_2 012 0676.Anl
Energy Activity Code Peak MDA Comments
Ce-139
Hg-203
SN-113
CS-13 7
Y-898
Co-1173
Co-1332
Y-1836
5 . 3634E + 02
1 . 2182E+03
9.6715E+02
4 . 6586E + 02
1. 5521E + 03
7 . 2448E+02
7 . 2998E+02
1. 6272E + 03
165.85 5 . 3 63E + 02
279.17 1. 218E + 03
391.69 9.671E+02
661.66 4.659E+02
898.02 1.552E+03
1173.24 7 . 245E + 02
1332.50 7 . 300E+02
1.38E+02
6.333E+00 7.56E-01 7.99E+01 G
1.569E+01
4.66E+01
3IE-01 8 . 15E + 01 G
1836.01 1.627E+03
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW2 5M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
1.15E+02
9.575E+00 7.73E-01 6.40E+01 G
1.10E+04
7.158E+00 1.10E+00 8.52E+01 G
1. 07E + 0.2
1.135E+01 7.10E-01 9.37E+01 G
1.93E+03
4.676E+00 7.93E-01 9.99E+01 G
1.93E+03
4 . 916E + 00 8.45E-01 1.00E + 02 G
1.07E+02
5.029E+00 7.91E-01 9.92E+01 G
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
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Spectrum name: 8_TunaCan_2012067 6.Anl
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
D - Double-Escape
K - Key Line
A - Not in Average
C - Coincidence Peak
*************** d J s c A R D E D I S 0 T 0 P E P E A K S ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
* * * * *
SUMMARY
OF N U C L I
D E S IN
SAMPLE
*****
Time of Count
Time Corrected
Uncertainty
1 Sigma
Nuclide
Activity
Activity
Counting
MDA
Bq
Bq
Pb-210
1. 4851E + 04
1.4960E+04
7.555E-01%
2 . 03E+02
AM-241
1.2400E+03
1.2405E+03
7.719E-01%
1.71E+01
CD-109
1.4124E+04
1.6066E+04
5.2 60E-01%
1.35E+02
CO - 5 7
2.7715E+02
3.4512E+02
7.6 8 IE-01%
4.49E+00
Ce-139
3.4782E+02
5.3634E+02
7.558E-01%
6.33E+00
Hg-2 03
3.3925E+02
1.2182E+03
8.812E- 01%
1.57E+01
SN-113
5.7617E+02
9.6715E+02
7.72 9E- 01%
9.58E+00
CS-13 7
4.6334E+02
4.6586E+02
1.105E+00%
7.16E + 0 0
Y-898
8.8728E+02
1.5521E+03
7.104E-01%
1.13E+01
Co-1173
7.023 9E+02
7.2448E+02
7.93 IE-01%
4.6 8E + 0 0
Co-13 32
7.0772E+02
7.2998E+02
8.450E-01%
4 . 92E+00
Y-1836
9.3024E+02
1.6272E+03
7.905E-01%
5.03E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
s U M M A R Y
Total Activity ( 82.3 to 2000.3 keV) 3.545E+04 Bq
Total Decayed Activity ( 82.3 to 2000.3 keV) 4.0432598E+04 Bq
Analyzed by:
Admin
Reviewed by:
Supervisor
Laboratory: TestAmerica
Page 461 of 551
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Initial
Calibration
Verifications
Page 462 of 551
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Ge03 90099 solidcert 2012
2nd Source Verification
Detector: Ge3
Geometry: Tunacan
Reference date 1/1/2010
Source: 81427-334
Standard volume g / vial 1550
Standard volume transferred in g / geometry 318.5
lab ID# of cal standard Rad10-0006
Isotope
Certified Activity
gammas/sec
Geometry
Activity
yabundance
Bq/sample
Count
Results
% recovery
Am-241
2034
418
0.359
1164
1165
100.1
Cs-137
1926
396
0.851
465
443.73
95.4
Co-60
3611
742
0.99974
742
700.09
94.3
Co-60
3612
742
0.999856
742
704.11
94.9
Reviewed By: Jody Watson
Date: 3/27/2012
SOP: ST-RD-0102 current rev
2nd source tuna can
Page 463 of 551
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3_TunaCan2nd_20120999
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Spectrum name: 3_TunaCan2nd_20120999.Anl
Sample description
3_TunaCan_81427-334_2ndsource_032712
Spectrum Filename: C:\User\SPC\Det3\3_TunaCan2nd_20120999.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/27/2012 10:50:55 PM
3600
3624
0.65 %
3
Detector system
Ge 3 SN/131
Cali brati on
Fi 1ename:
3_Soil_TunaCan_90099_032712
3_Soil_TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gai n:
Quadrati c:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/28/2012 11:26:42 AM
0.147 kev
0.250 keV/channel
3.682E-08 keV/channelA2
3/28/2012 11:26:55 AM
165.85 kev
Quadratic Uncertainty = 0.64 %
-6.102019E-01 + (-3 . 642282E-01"'Log(E) ) +
( -2.895398E-02"Log(E)A2 )
Quadratic Uncertainty = 1.29 %
-2.525141E+01 + ( 9.446449E+00*Log(E) ) +
( -1.005974E+00*Log (E) A2 )
DET_EnergyStandardMix & Pb.Lib
0.500
Library based
Env32 G53W4.25
150 ( 37.61keV )
8000 ( 2000.41keV )
1000.000%
3
1.0000E+00
1.0000E+00/C 1.0000E+00* 1.0000E+00) =
1.0000E+00
Reg. Guide 4.16 Method
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Spectrum name: 3_TunaCan2nd_20120999.Anl
Page 1
Page 464 of 551
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3_TunaCan2nd_20120999
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4.0000000E+00
0.000%
average of three points.
12.000
2.000
0.000
2.000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
total peaks alloc. 11 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0561
Comments
1/1/2010 11:00:00 AM
3_2012-02-26_0244.PBC
2/26/2012 2:44:46 AM
SUMMARY
O F
PEAKS
I N
RANGE
Peak
Area
Uncert
FWHM
Corrctn
Nucli de
Brnch.
Act.
Energy
Factor
Energy
Rati o
Bq/Sampl
36.57
684.
13.49
0.86
1.380E-02
46.58
46359.
0.64
0.82
2.218E-02
46.54
4.250
1.465E+04
49.41
474.
26.39
0.62
2.446E-02
55.13
148.
69.87
0.50
2.879E-02
59.56
47477.
0.63
0.80
3.183E-02
59.54
35.700
1.165E+03
63.23
116.
55.13
0.52
3.413E-02
74.81
347.
24.83
0.85
3.992E-02
77.26
173.
50.89
0.85
4.088E-02
87.94
26078.
0.87
0.86
4.402E-02
88.03
3.610
1.549E+04
121.96
6006.
2.27
0.93
4.564E-02
122.06
85.600
3.426E+02
136.40
688.
9.11
0.98
4.398E-02
157.37
39.
92.20
0.44
4.044E-02
165.86
1056.
7.85
0.99
3.963E-02
165.85
79.900
5.658E+02
210.61
83.
58.19
0.66
3.379E-02
272.61
73.
46.14
0.59
2.834E-02
332.61
124.
44.81
0.91
2.468E-02
391.78
370.
17.84
1.12
2.199E-02
391.69
64.000
9.986E+02
621.40
108.
40.97
0.41
1.575E-02
661.73
19442.
0.81
1.44
1.504E-02
661.66
85.210
4.437E+02
719.67
90.
45.03
0.66
1.413E-02
813.20
114.
49.57
0.70
1.289E-02
898.03
310.
14.07
1.64
1.196E-02
898.02
93.700
1.553E+03
901.05
12.
303.83
1.64
1.193E-02
974.92
130.
55.88
0.66
1.124E-02
1145.48
114.
31.99
0.24
9.931E-03
1173.20
18293.
0.84
1.86
9.749E-03
1173.24
99.900
7.001E+02
1332.46
16679.
0.82
1.95
8.830E-03
1332.50
99.982
7.041E+02
1836.29
148.
9.58
2.45
6.855E-03
1836.01
99.200
1.225E+03
UNIDENTIFIED
PEAK
Page 2
SUMMARY
Page 465 of 551
-------
3_TunaCan2nd_20120999
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
145.86 36.57
197.25 49.41
220.16 55.13
252.57 63.23
2766. 684.
5697. 474.
4834. 148.
1834. 116.
4.960E+04 13.49
1.939E+04 26.39
5.123E+03 69.87
3.399E+03 55.13
0.858 - s
0.620 - sM
0.497 - sc
0.521 - s
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TestAmerica Spectrum name: 3_TunaCan2nd_20120999.Anl
Channel
Energy Background
Net area
Eff-'Area
Uncert
FWHM Suspected
298.78
74.77
3800.
394.
9.858E+03
26.85
0.961 -
308.61
77.22
3690.
220.
5.394E+03
46.86
0.670 -
545.54
136.40
1213.
688.
1.563E+04
9.11
0.979 -
629.48
157.37
627.
39.
9.644E+02
92.20
0.441 - c
842.63
210.61
900.
83.
2.456E+03
58.19
0.661 - s
1090.83
272.61
495.
73.
2.587E+03
46.14
0.594 - s
1330.98
332.61
884.
124.
5.010E+03
44.81
0.910 -
2486.71
621.40
501.
108.
6.835E+03
40.97
0.412 - s
2879.89
719.67
427.
90.
6.393E+03
45.03
0.665 - s
3254.07
813.20
660.
114.
8.842E+03
49.57
0.696 - s
3605.81
901.13
695.
12.
1.042E+03
301.14
1.640 - sc
3900.95
974.92
936.
130.
1.157E+04
55.88
0.655 - s
4583.05
1145.48
294.
114.
1.153E+04
31.99
0.244 - s
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
M - Peak is close to a library peak.
This section based on library: DET_EnergyStandardMix & Pb.Lib
****** T
D E N T I
F I E D P
E A K
S U M M A R
Y *******
Nucli de
Peak
Centroi d
Background
Net Area
Intensi ty
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec
1 Sigma %
keV
Pb-210
185.92
46.58
11142.
46316.
12.866
0.64
0.818
AM-241
237.87
59.56
10162.
47477.
13.188
0.63
0.799
CD-109
351.53
87.94
5716.
26078.
7.244
0.87
0.855
CO-5 7
487.71
121.96
2782.
6006.
1.668
2.27
0.932
Ce-139
663.45
165.85
1658.
1078.
0.300
7.99
0.995s
SN-113
1567.82
391.78
1043.
370.
0.103
17.84
1.118
CS-137
2648.06
661.73
971.
19442.
5.401
0.81
1.437
Y-898
3593.36
898.02
795.
310.
0.086
14.06
1.637D
Co-1173
4693.90
1173.20
663.
18293.
5.081
0.84
1.858
Co-1332
5330.66
1332.46
231.
16679.
4.633
0.82
1.949
Y-1836
7344.33
1836.29
27.
148.
0.041
9.58
2.454
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
~
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TestAmerica Spectrum name: 3_TunaCan2nd_20120999.Anl
Page 3
Page 466 of 551
-------
-A--A--A--A--A- SUMMARY
- Nuclide - Average
Name Code Activity
Bq/Sample
0 F
3_TunaCan2nd_20120999
LIBRARY PEAK USAGE ***'
Peak
Energy Activity Code MDA Value
kev Bq/Sample Bq/Sample COMMENTS
Pb-210
AM-241
CD-109
CO-5 7
Ce-139
Hg-203
SN-113
CS-137
Y-898
Co-1173
Co-1332
Y-1836
1.4654E+04
1.1650E+03
1.5485E+04
3.4265E+02
5.7768E+02
1.3708E-02
9.9863E+02
4.4373E+02
1.5527E+03
7.0009E+02
7.0411E+02
1.2247E+03
46.54 1.465E+04
59.54 1.165E+03
88.03 1.549E+04
122.06 3.426E+02
165.85 5.777E+02 *
279.17 1.371E-02 %
391.69 9.986E+02
661.66 4.437E+02
898.02 1.553E+03
1173.24 7.001E+02
1332.50 7.041E+02
1836.01 1.225E+03 ?
8.15E+03
P 1.565E+02 6.36E-01 4.25E+00 G
1.58E+05
1.159E+01 6.31E-01 3.57E+01 G
4.63E+02
2.108E+02 8.73E-01 3.61E+00 G
2.72E+02
1.418E+01 2.27E+00 8.56E+01 G
1.38E+02
1.031E+02 7.99E+00 7.99E+01 G
4.66E+01
2.387E+00 5.21E+03 8.15E+01 G
1.15E+02
4.131E+02 1.78E+01 6.40E+01 G
1.10E+04
3.375E+00 8.12E-01 8.52E+01 G
1.07E+02
6.719E+02 1.41E+01 9.37E+01 G
1.93E+03
4.695E+00 8.38E-01 9.99E+01 G
1.93E+03
3.104E+00 8.16E-01 1.00E+02 G
1.07E+02
2.214E+02 9.58E+00 9.92E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
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Spectrum name: 3_TunaCan2nd_20120999.Anl
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
Page 4
Page 467 of 551
-------
to be found directly.
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
3_TunaCan2nd_20120999
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
D - Double-Escape
K - Key Li ne
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS **********
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting
Bq/Sample Bq/Sample
MDA
Bq/Sample
Pb-210
1.3671E+04
1.4654E+04
6.370E-01%
1.56E+02
AM-241
1.1608E+03
1.1650E+03
6.312E-01%
1.16E+01
CD-109
4.5562E+03
1.5485E+04
8.727E-01%
2.llE+02
CO-5 7
4.2711E+01
3.4265E+02
2.266E+00%
1.42E+01
Ce-139 #
9.4613E+00
5.7768E+02
7.994E+00%
1.03E+02
Hg-203 #A
1.3708E-02 >12 Halflives
5.2116E+03%
2.3868E+00
SN-113
7.3077E+00
9.9863E+02
1.784E+01%
4.13E+02
CS-137
4.2144E+02
4.4373E+02
8.123E-01%
3.38E+00
Y-898
7.6802E+00
1.5527E+03
1.406E+01%
6.72E+02
Co-1173
5.2177E+02
7.0009E+02
8.377E-01%
4.70E+00
Co-1332
5.2477E+02
7.0411E+02
8.16lE-01%
3.10E+00
Y-1836 #
6.0578E+00
1.2247E+03
9.579E+00%
2.21E+02
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,25 3/28/2012
11:28:58 AM
Page 6
TestAmeri ca
Spectrum name: 3_TunaCan2nd_20120999.Anl
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
SUMMARY
Total Activity ( 974.7 to 2000.4 keV) 2.093E+04 Bq/Sample
Total Decayed Activity ( 974.7 to 2000.4 keV) 3.7848984E+04 Bq/Sample
Page 5
Page 468 of 551
-------
Ge05 90099 solidcert 2012
2nd Source Verification
Detector: Ge5
Geometry: Tunacan
Reference date 1/1/2010
Source: 81427-334
Standard volume g / vial 1550
Standard volume transferred in g / geometry 318.5
lab ID# of cal standard 6665
Isotope
Certified Activity
gammas/sec
Geometry
Activity
yabundance
Bq/sample
Count
Results
% recovery
Am-241
2034
418
0.359
1164
1160.9
99.7
Cs-137
1926
396
0.851
465
442.36
95.1
Co-60
3611
742
0.99974
742
700.21
94.3
Co-60
3612
742
0.999856
742
701.86
94.6
Reviewed By: Jody Watson
Date: 3/27/2012
SOP: ST-RD-0102 current rev
2nd source tuna can
Page 469 of 551
-------
5_TunaCan2nd_20120813
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Spectrum name: 5_TunaCan2nd_20120813.Anl
Sample description
5_TunaCan2nd_Radl0_032712
Spectrum Filename: C:\User\SPC\Det5\5_TunaCan2nd_20120813.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/27/2012 10:12:05 AM
7200
7250
0.69 %
5
Detector system
Ge 5 SN/157
Cali brati on
Fi 1ename:
5_Soil_TunaCan_90099_032612
5_Soil_TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gai n:
Quadrati c:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/27/2012 5:20:02 PM
0.135 kev
0.250 keV/channel
2.720E-08 keV/channelA2
PM
3/27/2012 5:20:37
165.85 kev
Quadratic Uncertainty = 0.87 %
6.466115E-01 + (-7. 830454E-01"'Log(E) ) +
( -4.117504E-03"'Log(E) A2 )
Quadratic Uncertainty = 1.43 %
-2.462251E+01 + ( 9.07521lE+00*Log(E) ) +
( -9. 664422 E-01"'Log (E) A2 )
DET_EnergyStandardMix & Pb.Lib
0.500
Library based
Env32 G53W4.25
150 ( 37.61keV )
8000 ( 2000.53keV )
1000.000%
3
1.0000E+00
1.0000E+00/C 1.0000E+00"
1.0000E+00
Reg. Guide 4.16 Method
1.0000E+00) =
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Spectrum name: 5_TunaCan2nd_20120813.Anl
Page 1
Page 470 of 551
-------
5_TunaCan2nd_20120813
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4.0000000E+00
0.000%
average of three points.
12.000
2.000
0.000
2.000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
1/1/2010 11:00:00 AM
5_2012-02-26_0305.PBC
2/26/2012 3:05:30 AM
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff:
33.1557
r**** SUMMARY OF PEAKS I
Peak Area Uncert FWHM Corrctn
Energy Factor
N RANGE
Nuclide Brnch.
Energy Ratio
Act. Nuc
Bq/Sampl
36.81
46.61
49.73
59.57
87.94
96.44
99.01
105.59
121.94
129.89
136.43
165.86
238.72
247.25
259.02
260.46
322.65
351.63
391.95
407.02
412.80
420.83
510.72
542.81
583.30
661.70
762.61
796.90
886.67
897.77
932.49
1005.
72616.
1326.
75329.
40851.
148.
160.
109.
9225.
126.
1263.
1574.
327.
57.
93.
98.
45.
256.
494.
43.
202.
123.
188.
148.
161.
25605.
129.
151.
129.
428.
230.
12.08
0.49
15.18
0.49
0.68
47.31
48.52
69.79
1.66
62.97
7.42
6.14
27.04
84.47
60.17
58.62
91.14
27.79
16.33
90.43
35.90
52.91
44.32
28.69
33.50
0.71
36.06
38.71
46.77
19.21
35.52
0.62
0.73
0.68
0.74
0.80
0.80
0.81
0.52
0.84
0.30
0.90
0.84
0.86
0.31
0.97
0.97
0.46
1.06
1.15
0.56
0.77
0.72
0.50
0.36
0.69
1.39
0.79
0.30
0.30
1.38
0.82
1.151E-02
1.792E-02
1.987E-02
2.535E-02
3.460E-02
3.568E-02
3.589E-02
3.619E-02
3.583E-02
3.522E-02
3.457E-02
3.133E-02
2.319E-02
2.252E-02
2.167E-02
2.157E-02
1.806E-02
1.681E-02
1.536E-02
1.489E-02
1.471E-02
1.448E-02
1.232E-02
1.171E-02
1.103E-02
9.924E-03
8.812E-03
8.493E-03
7.766E-03
7.686E-03
7.445E-03
Page 2
46.54 4.250 1.421E+04 Pb210
59.54 35.700
88.03 3.610
1.161E+03 AM241
1.542E+04 CD109
122.06 85.600 3.348E+02 C057
165.85 79.900 5.319E+02 Cel39
391.69 64.000 9.501E+02 SN113
661.66 85.210 4.424E+02 CS137
898.02 93.700 1.665E+03 Y898
Page 471 of 551
-------
1008.65 104. 56.29
1173.15 23044. 0.73
1332.39 20769. 0.71
1836.05 245. 7.47
5_TunaCan2nd_20120813
0.28 6.970E-03
1.79 6.138E-03 1173.24
1.87 5.515E-03 1332.50
1.56 4.208E-03 1836.01
99.900 7.002E+02 Coll73
99.982 7.019E+02 Col332
99.200 1.642E+03 Y1836
************ UNIDENTIFIED PEAK
Peak Centroid Background Net Area Efficiency
Channel Energy Counts Counts * Area
SUMMARY
Uncert FWHM Suspected
1 Sigma % keV Nuclide
146.78
198.52
385.40
395.68
36.81
49.73
96.42
98.99
4847.
12365.
1874.
2103.
1005. 8.731E+04 12.08 0.625
1326. 6.673E+04 15.18 0.681
90. 2.532E+03 71.31 0.588
121. 3.381E+03 58.44 0.394
s
sc
s
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Spectrum name: 5_TunaCan2nd_20120813.Anl
Channel
Energy Background
Net area
Eff-'Area
Uncert
FWHM Suspected
422.09
105.59
2271.
109.
3.012E+03
69.79
0.518 -
sc
519.32
129.89
2194.
126.
3.592E+03
62.97
0.298 -
s
545.51
136.43
23 77.
1263.
3.654E+04
7.42
0.900 -
s
954.90
238.72
2247.
327.
1.410E+04
27.04
0.863 -
SM
989.00
247.25
1031.
57.
2.516E+03
84.47
0.312 -
sc
1036.13
259.01
1532.
93.
4.309E+03
60.17
0.968 -
D
1041.90
260.46
1588.
98.
4.525E+03
58.62
0.970 -
D
1290.76
322.65
744.
45.
2.473E+03
91.14
0.455 -
c
1406.70
351.63
1442.
256.
1.523E+04
27.79
1.058 -
s
1628.36
407.02
667.
43.
2.866E+03
90.43
0.562 -
sc
1651.47
412.80
1438.
202.
1.370E+04
35.90
0.775 -
s
1683.60
420.83
1291.
123.
8.472E+03
52.91
0.720 -
s
2043.25
510.72
1553.
188.
1.523E+04
44.32
0.503 -
s
2171.67
542.81
587.
148.
1.267E+04
28.69
0.362 -
s
2333.63
583.30
785.
161.
1.460E+04
33.50
0.694 -
s
3050.97
762.61
614.
129.
1.468E+04
36.06
0.794 -
s
3188.11
796.90
856.
151.
1.782E+04
38.71
0.295 -
s
3547.15
886.67
963.
129.
1.665E+04
46.77
0.296 -
s
3730.41
932.49
1438.
230.
3.096E+04
35.52
0.818 -
s
4035.01
1008.65
864.
104.
1.490E+04
56.29
0.275 -
s
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
M - Peak is close to a library peak.
This section based on library: DET_EnergyStandardMix & Pb.Lib
************** I D E N T I
Nuclide Peak Centroid
Channel Energy
FIED PEAK S
Background Net Area
Counts Counts
U M M A R Y ************
Intensity Uncert FWHM
Cts/Sec 1 Sigma % keV
Pb-210
186.01
46.61
16470.
72552.
10.077
0.49
0.733
AM-241
237.88
59.57
15419.
75329.
10.462
0.49
0.735
CD-109
351.46
87.94
8772.
40851.
5.674
0.68
0.804
CO-5 7
487.54
121.94
3880.
9225.
1.281
1.66
0.838
Ce-139
663.30
165.86
2329.
1574.
0.219
6.14
0.840
SN-113
1568.04
391.95
1640.
494.
0.069
16.33
1.153
CS-137
2647.28
661.70
1362.
25582.
3.553
0.71
1.394
Y-898
3591.55
897.77
1410.
428.
0.060
19.21
1.376
Page 3
Page 472 of 551
-------
Co-1173 4692.83 1173.15
Co-1332 5329.55 1332.39
Y-1836 7342.76 1836.05
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
5_TunaCan2nd_20120813
788. 23044. 3.201
98. 20769. 2.885
15. 245. 0.034
0.73 1.786
0.71 1.870
7.47 1.556s
~
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TestAmerica Spectrum name: 5_TunaCan2nd_20120813.Anl
•••••••••••••••••••• SUMMARY
- Nuclide - Average
Name Code Activity
Bq/Sample
OF LIBRARY PEAK USAGE ***'
Peak
Energy Activity Code MDA Value
kev Bq/Sample Bq/Sample COMMENTS
Pb-210 N 1.4212E+04
AM-241 1.1609E+03
CD-109
CO-5 7
Ce-139
Hg-203
SN-113
CS-137
Y-898
Co-1173
Co-1332
Y-1836
1.5419E+04
3.3478E+02
5.3191E+02
-6.5193E-03
9.5011E+02
4.4236E+02
1.6655E+03
7.0021E+02
7.0186E+02
1.6424E+03
46.54 1.421E+04
59.54 1.161E+03
88.03 1.542E+04
122.06 3.348E+02
165.85 5.319E+02
279.17-6.519E-03 %
391.69 9.501E+02
661.66 4.424E+02
898.02 1.665E+03
1173.24 7.002E+02
1332.50 7.019E+02
1836.01 1.642E+03
P 1.177E+02
8.959E+00
1.658E+02
1.063E+01
7.689E+01
1.788E+00
3.682E+02
P 3.020E+00
6.908E+02
4.056E+00
1.651E+00
1.392E+02
8.15E+03
4.91E-01 4.25E+00 G
1.58E+05
4.87E-01 3.57E+01 G
4.63E+02
6.81E-01 3.61E+00 G
2.72E+02
1.66E+00 8.56E+01 G
1.38E+02
6.14E+00 7.99E+01 G
4.66E+01
8.22E+03 8.15E+01 G
1.15E+02
1.63E+01 6.40E+01 G
1.10E+04
7.12E-01 8.52E+01 G
1.07E+02
1.92E+01 9.37E+01 G
1.93E+03
7.32E-01 9.99E+01 G
1.93E+03
7.07E-01 1.00E+02 G
1.07E+02
7.47E+00 9.92E+01 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
Page 4
Page 473 of 551
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5_TunaCan2nd_20120813
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TestAmerica Spectrum name: 5_TunaCan2nd_20120813.Anl
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
D - Double-Escape
K - Key Li ne
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS **********
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting
Bq/Sample Bq/Sample
MDA
Bq/Sample
Pb-210
1.3259E+04
1.4212E+04
4.918E-01%
1.18E+02
AM-241
1.1568E+03
1.1609E+03
4.867E-01%
8.96E+00
CD-109
4.5403E+03
1.5419E+04
6.810E-01%
1.66E+02
CO-5 7
4.1787E+01
3.3478E+02
1. 660E+00%
1.06E+01
Ce-139
8.7347E+00
5.3191E+02
6.138E+00%
7.69E+01
Hg-203 #A
-6.5193E-03
>12 Halflives
8.2197E+03% 1.7882E+00
SN-113
6.9747E+00
9.5011E+02
1.633E+01%
3.68E+02
CS-137
4.2015E+02
4.4236E+02
7.122E-01%
3.02E+00
Y-898
8.2662E+00
1.6655E+03
1.92lE+01%
6.91E+02
Co-1173
5.2196E+02
7.0021E+02
7.316E-01%
4.06E+00
Co-1332
5.2320E+02
7.0186E+02
7.069E-01%
1.65E+00
Y-1836
8.1520E+00
1.6424E+03
7.47lE+00%
1.39E+02
ORTEC g V
TestAmeri ca
i (3263) Env32 G53W4.25 3/28/2012 7:35:49 AM Page 6
Spectrum name: 5_TunaCan2nd_20120813.Anl
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
Page 5
Page 474 of 551
-------
5_TunaCan2nd_20120813
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
SUMMARY
Total Activity ( 279.0 to 2000.5 keV) 2.050E+04 Bq/Sample
Total Decayed Activity ( 279.0 to 2000.5 keV) 3.7761527E+04 Bq/Sample
Page 6
Page 475 of 551
-------
Ge07 90099 solidcert2012TALS.xls
2nd Source Verification
Detector:
Ge7
Geometry:
Tunacan
Reference date
1/1/2010
Source:
81427-334
Standard volume g / vial
1550
Standard volume transferred in g / geometry
318.5
lab ID# of cal standard
6665
Isotope
Certified Activity
gammas/sec
Geometry
Activity
yabundance
Bq/sample
Count
Results
%recovery
Am-241
2034
418
0.359
1164
1150.4
98.8
Cs-137
1926
396
0.851
465
440.47
94.7
Co-60
3611
742
0.99974
742
681.72
91.9
Co-60
3612
742
0.999856
742
692.1
93.2
Reviewed By: Jody Watson
Date: 3/27/2012
SOP: ST-RD-0102 current rev
2nd source tuna can
Page 476 of 551
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TestAmerica Spectrum name: 7_TunaCan2ndSource_20120479.Anl
Sample description
7 TunaCan2ndSource 81427-334 032712
Spectrum Filename: C:\User\SPC\Det7\7_TunaCan2ndSource_20120479.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/27/2012 3:25:25 PM
3600
3684
2.28 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
7 TunaCan 90099 032712
7 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
3/16/2012 11:44:50 AM
0.153 keV
0.250 keV/channel
6.716E-09 keV/channela2
3/16/2012 11:45:14 AM
165.85 keV
Quadratic Uncertainty = 0.87 %
6 . 716580E- 01 + ( - 6.166540E-01*Log(E) ) +
( -2 . 065917E-02*Log(E)a2 )
Quadratic Uncertainty = 1.48 %
-2.689695E+01 + ( 1.019544E+01*Log(E) ) +
( -1.081671E+00*Log(E)A2 )
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
DET EnergyStandardMix & Pb.Lib
0 .500
Library based
Env3 2
150 (
S000 (
G53W4.25
3 7.65keV )
2000.21keV )
1000.000%
3
OOOOE+OO
0000E + 00/ (
OOOOE+OO
1.0000E+00* 1.0000E+00) =
Reg. Guide 4.16 Method
Page 477 of 551
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Spectrum name: 7 TunaCan2ndSource 20120479.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0 0 0 0 0 0 0E+0 0
4.OOOOOOOE+OO
0.000%
average of three points.
12 .000
2.000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Comments
1/1/2010 11:00:00 AM
7_2 012-02-2 6_03 2 7.PBC
2/26/2012 3:27:47 AM
Absorption (Internal)
Geometry correction:
Random summing:
NO
NO
NO
total peaks alloc. 11 cutoff:
Energy Calibration
Normalized diff:
5.00E+01%
0.0270
***** SUMMARY OF PEAKS IN RANGE *****
Peak Area Uncert FWHM Corrctn Nuclide Brnch. Act, Nuc
Energy Factor Energy Ratio Bg/Sampl
36 . 65
788 .
12 .78
0 . 82
1.4 87E-02
40.49
109.
96 . 90
0 . 59
1. 869E-02
46 . 62
49142.
0 . 63
0 . 84
2 . 491E-02
46 . 54
4 .250
1.386E+04
Pb210
49 . 64
876 .
18 . 72
0 . 86
2.792E-02
59.61
54530.
0 .58
0 . 87
3 . 707E-02
59 . 54
35 . 700
1.150E+03
AM241
76 . 99
260 .
38.90
1. 03
4 . 881E-02
88 . 06
31019.
0 . 77
0 . 89
5.32 9E-02
88 . 03
3 . 610
1.522E+04
CD109
122 . 04
6834 .
2 . 04
0 . 94
5.606E-02
122.06
85 . 600
3.171E+02
C057
136.41
810 .
9.51
1 . 00
5 . 4HE- 02
165.84
1193 .
6.45
0 . 96
4.765E-02
165.85
79.900
5.180E+02
Cel39
185.66
92 .
57 .01
0 . 73
4 . 445E-02
213.19
122 .
50 .56
0 . 75
3 .960E-02
272.80
146.
47.29
0.28
3 .217E-02
391.67
372 .
19 . 60
1. 11
2 . 360E-02
391.69
64.000
9.332E+02
SN113
442.91
47.
93 . 72
0.45
2 .122E-02
483.77
95 .
38.10
0 . 62
1. 965E-02
524.63
67.
65 . 12
0 . 73
1. 83IE-02
604.78
31.
59.37
0 .27
1.616E-02
628.99
32 .
94.37
0 . 58
1.561E-02
661.67
19152.
0 . 86
1. 47
1.492E-02
661.66
85.210
4.405E+02
CS137
898.03
322 .
23.. 53
1. 90
1.137E-02
898.02
93.700
1.694E+03
Y898
910.18
180 .
33 . 99
0 . 85
1.123E-02
963 .79
49 .
71.39
0 . 69
1.067E-02
1173 .23
16317.
0 . 86
1. 89
8.929E-03
1173.24
99.900
6.817E+02
Coll73
1332 .49
14763.
0 . 85
2 . 04
7.95 IE-03
1332.50
99.982
6.921E+02
Col332
1836.09
186 .
9 . 19
1.40
5.919E-03
1836.01
99.200
1.780E+03
Y1836
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
146.00 36.65
161.37 40.49
197.99 49.64
3116 .
4419 .
8222 .
788. 5.300E+04 12.78 0.819
109. 5.831E+03 96.90 0.587
8 7Bags 418 $££64 18.72 0.855
c
SM
-------
307.39 76.99 3728. 260. 5.319E+03 38.90 1.033
Page 479 of 551
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TestAmerica Spectrum name: 7_TunaCan2ndSource_2 012 04 7 9.Anl
Channel
Energy Background
Net area
Eff*Area
Uncert
FWHM
Suspected
545.11
136 . 41
1706 .
810.
1.497E+04
9 .51
1. 002
-
742.15
185.66
1076 .
92 .
2 . 081E + 03
57 . 01
0 . 725
s
852 .30
213.19
1296 .
122 .
3.077E+03
50 . 56
0 . 748
s
1090 . 74
272.80
1320 .
146 .
4.539E+03
47.29
0.283
s
1771.26
442.91
710 .
47 .
2.215E+03
93 . 72
0 . 453
sc
1934.71
483.77
486 .
95 .
4.835E+03
38.10
0 . 616
s
2098.18
524.63
583 .
67 .
3.669E+03
65 . 12
0 . 732
s
2418.80
604.78
172 .
31.
1.939E+03
59.37
0 . 268
s
2515.62
628.99
330 .
32 .
2.050E+03
94 .37
0 . 581
sc
3640.41
910.18
855 .
180 .
1.603E+04
33 . 99
0 . 852
s
3854.87
963.79
447 .
49 .
4.625E+03
71.39
0 . 695
s
s - Peak fails shape tests.
D - Peak area deconvoluted.
Li - Peak written from unknown list.
C - Area < Critical level.
M - Peak is close to a library peak.
This section based on library: DET_EnergyStandardMix & Pb.Lib
rt rt * * * rt * rt * * ft rt if -k J
D E N T I
F I E D P
E A K
S U M M A R
Y *** *** ********
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
Pb-210
185.90
46 . 62
12530 .
49107.
13 . 641
0 . 63
0 . 840
AM-241
237 . 87
59.61
10985 .
54530 .
15 . 147
0 .58
0 . 871
CD-10 9
351.70
88 . 06
6100 .
31019.
8 . 616
0 . 77
0 . 892
CO-57
487 . 62
122.04
3 040.
6834 .
1. 898
2. 04
0 . 937
Ce-139
662 .88
165.84
1495 .
1193 .
0.331
6.45
0 . 956
Hg-203
1114 .79
278 . 81
2119 .
-42 .
-0.012
155.58
1. 105s
SN-113
1566.31
391.67
1236 .
372 .
0 . 103
19.60
1. 107
CS-13 7
2646 . 35
661.67
1156.
19152.
5.320
0 . 86
1.474
Y-898
3591.81
898 . 03
1084 .
322 .
0.089
2 3.53
1.897
Co-1173
4692.59
1173.23
493 .
16317.
4 . 532
0 . 86
1.893
Co-1332
5329.55
1332 .49
127 .
14763.
4 . 101
0 . 85
2 . 038
Y-1836
7343.66
1836 . 09
16 .
186.
0 . 052
9.19
1.399s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
Page 480 of 551
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TestAmerica Spectrum name: 7_TunaCan2ndSource_20120479.Anl
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
Bq/Sample keV Bq/Sample Bq/Sample COMMENTS
Pb-210 N 1 . 3857E + 04
AM-2 4 X
CD-10 9
CO-5 7
Ce-139
SN-113
CS-13 7
Y-898
Co-1173
Co-13 3 2
Y-1836
1.1504E + 03
1 . 5217E + 04
3.1712E+02
5 . 1801E+02
Hg-203 -4 . 544IE-01
9 . 3315E+02
4 . 4047E + 02
1. 6944E + 03
6 . 8172E+02
6.9210E+02
1.7801E+03
46.54 1.3 8 6E + 04
59,54 1.150E+03
5 8.03 1.522E+04
122.06 3.171E+02
165.85 5.180E+02
279.17-4.544E-01 ?
391.69 9 . 332E + 02
661.66 4 . 405E + 02
898.02 1.694E+03
1173.24 6 . 817E + 02
1332.50 6 . 921E+02
1836.01 1 . 7 8 0E + 03
8.15E+03
P 1.480E+02 6.34E-01 4.25E+00 G
1.036E+01 5
1.7 99E+02 7
1.205E+01 2
7 . 941E + 01 6
2.347E+00 1
4 . 17 8E + 02 1
3.706E+00
I . 216E + 02 2
4 . 43 6E + 0 0
2.586E+00 8
2 . 065E + 02 9
1.58E+05
.8IE-01 3.57E+01 G
4.63E+02
.73E-01 3.61E+00 G
2.72E+02
.04E+00 8.56E+01 G
1.38E+02
.45E+00 7.99E+01 G
4.66E+01
. 56E+02 8.15E+01 G
1.15E+02
.96E+01 6.40E+01 G
1.10E+04
, 56E-01 8 . 52E + 01 G
1.07E+02
.3 5E+01 9.37E + 01 G
1.93E+03
, 58E-01 9.99E + 01 G
1.93E+03
.49E-01 1.00E+02 G
1.07E+02
,19E+00 9.92E+01 G
This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
Page 481 of 551
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TestAmerica Spectrum name: 7_TunaCan2ndSource_20120479.Anl
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T ¦
- Thermal Neutron Activation
G -
Gamma Ray
F ¦
- Fast Neutron Activation
X -
X-Ray
I •
- Fission Product
P -
Positron Decay
N ¦
- Naturally Occurring Isotope
S -
Single-Escape
P ¦
- Photon Reaction
D -
Double-Escape
C -
- Charged Particle Reaction
K -
Key Line
M -
- No MDA Calculation
A -
Not in Average
R -
- Coincidence Corrected
C -
Coincidence Peak
H -
- Halflife limit exceeded
*************** £) j g c a R D E D I S
Nuclide Centroid Background Net Area
Energy Counts Counts
OTOPE PEAKS ***************
Intensity Uncert Activity
Cts/Sec 1 Sigma %
Hg-203 278.81 2119.
P - Peakbackground subtraction
-42 .
-0.012
155 . 5S
0 . OOOE + OO
***** SUMMARY OF NUCLIDES IN
Time of Count Time Corrected Uncertainty
Nuclide Activity Activity Counting
Bq/Sample Bq/Sample
S A M P L
1 Sigma
MDA
Bq/Sample
Pb-210
1.2 92 7E + 04
1.3857E+04
6.344E-01%
1.48E+02
AM-241
1.1462E+03
1.1504E+03
5.808E-01%
1.04E+01
CD-10 9
4.4794E+03
1.5217E+04
7.72 7E-01%
1.80E+02
CO - 5 7
3.9561E+01
3.1712E+02
2.043E+00%
1.20E+01
Ce-139
8.4971E+00
5.1801E+02
6.453E+00%
7.94E+01
Hg-2 03 #A
-4 . 544 IE - 01
>12 Halflives
1.5558E+02%
2.34 74E+0 0
SN-113
6.8413E+00
9.3 315E + 02
1.960E+01%
4.18E+02
CS-137
4.1835E+02
4.4047E+02
8.557E-01%
3.71E+00
Y-898
8.3979E+00
1.6944E+03
2.353E+01%
8.22E+02
Co-1173
5.0814E+02
6.8172E+02
8.5 8IE-01%
4.44E+00
Co-13 3 2
5.15 8 8E + 02
6.9210E+02
8.485E-01%
2.5 9E + 0 0
Y-1836
8.8227E+00
1.7 8 01E+03
9.190E+00%
2.07E+02
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TestAmerica Spectrum name: 7_TunaCan2ndSource_20120479.Anl
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
.C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 37.6 to 2000.2 keV) 2.007E+04 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.2 keV) 3.7281199E+04 Bq/Sample
Analyzed by:
Admin
Reviewed by:
Supervisor
Laboratory: TestAmerica
Page 483 of 551
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Ge08 90099 solidcert 2012
2nd Source Verification
Detector: Ge8
Geometry: Tunacan
Reference date 1/1/2010
Source: 81427-334
Standard volume g / vial 1550
Standard volume transferred in g / geometry 318.5
lab ID# of cal standard 6665
Isotope
Certified Activity
gammas/sec
Geometry
Activity
yabundance
Bq/sample
Count
Results
% recovery
Am-241
2034
418
0.359
1164
1175.4
101.0
Cs-137
1926
396
0.851
465
446.61
96.0
Co-60
3611
742
0.99974
742
697.22
93.9
Co-60
3612
742
0.999856
742
691.92
93.2
Reviewed By: Jody Watson
Date: 3/29/2012
SOP: ST-RD-0102 current rev
2nd source tuna can
Page 484 of 551
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8_TunaCan2nd_20120697
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Spectrum name: 8_TunaCan2nd_20120697.Anl
Sample description
8_TunaCan_81427-334_2ndsource_032912
Spectrum Filename: C:\User\SPC\Det8\8_TunaCan2nd_20120697.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
3/29/2012 1:58:04 AM
3600
3622
0.61 %
8
Detector system
Ge 8 SN/174
Cali brati on
Fi 1ename:
8_Soil_TunaCan_90099_032712
8_Soil_TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gai n:
Quadrati c:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/28/2012 10:35:07 AM
0.050 keV
0.250 keV/channel
8.067E-10 keV/channelA2
3/28/2012 10:35:20 AM
165.85 keV
Quadratic Uncertainty = 1.39 %
-1.098764E-01 + (-4.958544E-01*Log(E) ) +
( -2 . 572270E-02"'Log (E) A2 )
Quadratic Uncertainty = 1.71 %
-2.525301E+01 + ( 9.398253E+00*Log(E) ) +
( -1.000034E+00*Log(E)A2 )
DET_EnergyStandardMix & Pb.Lib
0.500
Library based
Env32 G53W4.25
150 ( 37.55keV )
8000 ( 2000.30keV )
1000.000%
3
1.0000E+00
1.0000E+00/C 1.0000E+00* 1.0000E+00) =
1.0000E+00
Reg. Guide 4.16 Method
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Page 1
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8_TunaCan2nd_20120697
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4.0000000E+00
4.0000000E+00
0.000%
average of three points.
12.000
2.000
0.000
2.000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: YES
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
total peaks alloc. 12 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 27.9595
Comments
1/1/2010 11:00:00 AM
8_2012-03-02_0402.PBC
3/2/2012 4:02:11 AM
SUMMARY
O F
PEAKS
I N
RANGE
Peak
Area
Uncert
FWHM
Corrctn
Nucli de
Brnch.
Act.
NUC
Energy
Factor
Energy
Rati o
Bq/Sampl
36.61
594.
17.47
1.15
1.254E-02
46.53
38495.
0.62
0.95
2.001E-02
46.54
4.250
1.345E+04
Pb210
49.81
542.
25.92
1.04
2.243E-02
59.48
43371.
0.71
0.98
2.878E-02
59.54
35.700
1.175E+03
AM241
84.86
327.
26.82
0.98
3.922E-02
88.03
22911.
0.76
0.98
3.992E-02
88.03
3.610
1.504E+04
CD109
122.06
5318.
2.55
1.03
4.146E-02
122.06
85.600
3.349E+02
C057
136.54
691.
14.03
0.89
3.998E-02
165.93
1033.
8.62
1.19
3.628E-02
165.85
79.900
6.077E+02
Cel39
177.05
71.
70.08
0.69
3.453E-02
185.74
128.
40.98
0.85
3.329E-02
227.93
52.
65.04
0.45
2.844E-02
270.79
87.
50.41
0.41
2.486E-02
278.94
44.
131.33
1.13
2.428E-02
279.17
81.500
HL>Cutoff
Hg203
302.52
63.
54.81
0.69
2.279E-02
370.09
35.
84.23
0.41
1.941E-02
391.61
316.
17.91
0.81
1.855E-02
391.69
64.000
1.016E+03
SN113
409.22
93.
50.95
0.41
1.791E-02
428.24
88.
46.51
0.39
1.726E-02
564.57
72.
45.26
0.57
1.378E-02
591.73
73.
42.60
0.61
1.326E-02
661.62
15734.
0.88
1.38
1.209E-02
661.66
85.210
4.466E+02
CS137
720.39
41.
72.89
0.46
1.126E-02
831.73
36.
50.61
0.44
9.986E-03
897.91
396.
17.93
1.52
9.360E-03
898.02
93.700
2.554E+03
Y898
1092.31
69.
44.41
0.50
7.924E-03
1173.30
13922.
0.92
1.73
7.452E-03
1173.24
99.900
6.972E+02
C01173
1332.56
12390.
0.92
1.75
6.677E-03
1332.50
99.982
6.919E+02
C01332
1836.18
152.
9.00
1.63
5.046E-03
1836.01
99.200
1.724E+03
Y1836
Page 2
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8_TunaCan2nd_20120697
************ UNIDENTIFIED PEAK SUMMARY *********
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
146.23
199.01
339.16
36.61
49.81
84.85
3218.
6400.
3491.
594. 4.742E+04
542. 2.416E+04
236. 6.026E+03
17.47 1.147
25.92 1.039
42.58 0.697
s
SM
SM
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Channel Energy Background Net area Eff-'Area Uncert FWHM Suspected
545.91 136.54 2178. 691. 1.728E+04 14.03 0.888 -
707.94 177.05 893. 71. 2.046E+03 70.08 0.693 - sM
742.68 185.74 978. 128. 3.835E+03 40.98 0.847 - sM
911.43 227.93 546. 52. 1.829E+03 65.04 0.445 - sc
1082.86 270.79 683. 87. 3.486E+03 50.41 0.413 - sM
1209.76 302.52 484. 63. 2.765E+03 54.81 0.692 - s
1480.00 370.09 385. 35. 1.803E+03 84.23 0.412 - sc
1636.49 409.22 685. 93. 5.212E+03 50.95 0.407 - s
1712.56 428.24 565. 88. 5.117E+03 46.51 0.393 - s
2257.86 564.57 330. 72. 5.224E+03 45.26 0.565 - s
2366.45 591.73 298. 73. 5.505E+03 42.60 0.613 - s
2881.06 720.39 284. 41. 3.640E+03 72.89 0.464 - s
3326.37 831.73 148. 36. 3.605E+03 50.61 0.439 - s
4368.55 1092.31 290. 69. 8.708E+03 44.41 0.495 - s
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
M - Peak is close to a library peak.
This section based on library: DET_EnergyStandardMix & Pb.Lib
****** z
D E N T I
F I E D P
E A K
S U M M A R
Y *******
Nucli de
Peak
Centroi d
Background
Net Area
Intensi ty
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec
1 Sigma %
keV
Pb-210
185.71
46.48
12173.
40702.
11.306
0.74
0.992
AM-241
237.70
59.48
10649.
43371.
12.047
0.71
0.984
CD-109
351.85
88.02
4506.
23196.
6.443
0.88
1.056
CO-5 7
487.99
122.06
2908.
5318.
1.477
2.55
1.026
Ce-139
663.47
165.93
1722.
1033.
0.287
8.62
1.189s
Hg-203
1115.46
278.94
1642.
44.
0.012
131.33
1.133
SN-113
1566.07
391.61
822.
316.
0.088
17.91
0.806s
CS-137
2646.01
661.62
665.
15731.
4.370
0.88
1.379
Y-898
3591.03
897.91
871.
396.
0.110
17.93
1.524
Co-1173
4692.46
1173.30
374.
13922.
3.867
0.92
1.726
Co-1332
5329.42
1332.56
82.
12390.
3.442
0.92
1.753
Y-1836
7343.62
1836.18
6.
152.
0.042
9.00
1.626s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
~
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8_TunaCan2nd_20120697
L I
-A--A--A--A--A- SUMMARY OF
- Nuclide - Average
Name Code Activity Energy
Bq/Sample keV
BRARY PEAK USAGE
Peak
Activity Code MDA Value
Bq/Sample Bq/Sample
COMMENTS
Pb-210
AM-241
CD-109
CO-5 7
Ce-1B9
Hg-20B
SN-113
CS-1B7
Y-898
Co-1173
Co-1332
Y-1836
1.4221E+04
1.1754E+03
1.5223E+04
3.3494E+02
6.0766E+02
6.1671E-01
1.0157E+03
4.4661E+02
2.5543E+03
6.9722E+02
6.9192E+02
1.7236E+03
46.54 1.422E+04
59.54 1.175E+03
88.03 1.522E+04
122.06 3.349E+02
165.85 6.077E+02
279.17 6.167E-01
391.69 1.016E+03
661.66 4.466E+02
898.02 2.554E+03
1173.24 6.972E+02
1332.50 6.919E+02
1836.01 1.724E+03
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
8.15E+03
1.806E+02 7.43E-01 4.25E+00 G
1.58E+05
1.311E+01 7.10E-01 3.57E+01 G
4.63E+02
2.071E+02 8.83E-01 3.61E+00 G
2.72E+02
1.600E+01 2.55E+00 8.56E+01 G
1.38E+02
1.153E+02 8.62E+00 7.99E+01 G
4.66E+01
2.689E+00 1.31E+02 8.15E+01 G
1.15E+02
4.390E+02 1.79E+01 6.40E+01 G
1.10E+04
P 3.489E+00 8.85E-01 8.52E+01 G
1.07E+02
9.046E+02 1.79E+01 9.37E+01 G
1.93E+03
4.649E+00 9.19E-01 9.99E+01 G
1.93E+03
2.515E+00 9.18E-01 1.00E+02 G
1.07E+02
1.542E+02 9.00E+00 9.92E+01 G
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Spectrum name: 8_TunaCan2nd_20120697.Anl
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
Page 4
Page 488 of 551
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8_TunaCan2nd_20120697
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes:
T - Thermal Neutron Activation
F - Fast Neutron Activation
I - Fission Product
N - Naturally Occurring Isotope
P - Photon Reaction
C - Charged Particle Reaction
M - No MDA Calculation
R - Coincidence Corrected
H - Halflife limit exceeded
Peak Codes:
G - Gamma Ray
X - X-Ray
P - Positron Decay
S - Single-Escape
D - Double-Escape
K - Key Li ne
A - Not in Average
C - Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS **********
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN SAMPLE
Time of Count Time Corrected Uncertainty 1 Sigma
Nuclide Activity Activity Counting
Bq/Sample Bq/Sample
MDA
Bq/Sample
Pb-210
1.3265E+04
1.4221E+04
7.429E-01%
1.81E+02
AM-241
1.1712E+03
1.1754E+03
7.10lE-01%
1.31E+01
CD-109
4.4713E+03
1.5223E+04
8.832E-01%
2.07E+02
CO-5 7
4.1631E+01
3.3494E+02
2.55lE+00%
1.60E+01
Ce-139 #
9.8959E+00
6.0766E+02
8.616E+00%
1.15E+02
Hg-203 A
6.1671E-01 >12 Halflives
1.3133E+02% 2.6892E+00
SN-113
7.3819E+00
1.0157E+03
1.79lE+01%
4.39E+02
CS-137
4.2415E+02
4.4661E+02
8.848E-01%
3.49E+00
Y-898
1.2542E+01
2.5543E+03
1.793E+01%
9.05E+02
Co-1173
5.1942E+02
6.9722E+02
9.185E-01%
4.65E+00
Co-1332
5.1548E+02
6.9192E+02
9.176E-01%
2.52E+00
Y-1836
8.4633E+00
1.7236E+03
8.997E+00%
1.54E+02
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TestAmeri ca
Spectrum name: 8_TunaCan2nd_20120697.Anl
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
SUMMARY
Total Activity ( 37.6 to 2000.3 keV) 2.045E+04 Bq/Sample
Total Decayed Activity ( 37.6 to 2000.3 keV) 3.8690848E+04 Bq/Sample
Page 5
Page 489 of 551
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Annual Calibration
Verifications
Page 490 of 551
-------
Analysis Report for Gamma Spectroscopy
Batch: 229576 Operator:
Snmnll)
WRKNO
Aliquot
Siema Instrument Detector CountDatc lime
CountDuration
LCS 160-229576-2-
LCS
341.90g
1.00 GammaVision
GV03 1 / 19 / 16 7:22
30
Analvte
Cnwnd#
Activity
TotalUnc
CountUnc
MDA
MUX
Act/MDA
AC-228
11136
4.965E-001 pCI/g
2.941 E-001
2.930E-001
1.062E+000
5.136E-001
0.47
0.2941
AG-108M
10982
-4.175E"002pCi/g
6.792E-002
6.789E-002
2.277E-001
1.106E-001
-0.18
0.0679
AG-110M
10973
-3.575E-003pCi/g
2.188E-002
2.188E-002
4.448E-001
2.156E-001
-0.01
0.0219
AM-241
10818
9.980E+001 pCi/g
5.238E+000
7.784E-001
1.133E+000
5.611E-001
88.11
5.2375
BA-133
10469
5,873E-0O2pCi/g
9.186E-002
9.180E-002
3.075E-001
1.497E-001
0,19
0.0919
BA-14D
10463
4.O18E-0O3pCi/g
3.844E-003
3.839E-003
7.823E-001
3.772E-001
0.01
0.0038
BE-7
10435
-8.382E-002pCi/g
6.487E-001
6.487E-001
2.192E+000
1.066E+000
-0.04
0.6487
BI-207
10195
7.936E-O02pCi/g
5.743E-002
5.729E-002
1.898E-001
9.128E-002
0,42
0.0574
BI-210M
10173
6.234E-002pCi/g
1.031 E-001
1.031 E-001
3.449E-001
1.683E-001
0,18
0.1031
Bl-212
10160
1.346E+000pCi/g
8.174E-001
8.144E-001
2.681 E-+000
1.284E+000
0,50
0.8174
BI-214
10154
3.248E-001 pCi/g
1.433E-001
1.423E-001
4.660E-001
2.249E-001
0.70
0.1433
CD-109
9254
2.731 E+OOOpCi/g
2.382E+000
2.378E+000
3.514E+000
1.721E+000
0.78
2.3824
CD-113M
17462
8.379E-001 pCL'g
8.360E+002
8.360E+002
2.823E+003
1.377E+003
0.00
835.9792
CE-139
9241
3.194E-002pCi/g
4.967E-002
4.958E-002
1.656E-001
8.094E-002
0.19
0,0497
CE-141
9235
-9.276E-002pCI/g
8.336E-002
8.322E-002
2.761E-001
1.351 E-001
-0.34
0.0834
CE-144
9221
4.148E-001pCI/g
3.518E-001
3.512E-001
1.164E+000
5.698E-001
0.36
0.3518
CF-249
9215
3.609E-002pCi/g
7.851 E-002
7.848E-002
3.006E-001
1.462E-001
0.12
0.0785
CF-251
13690
-9.337E-0O2pCi/g
2.422E-001
2.421 E-001
8.119E-001
3.967E-001
-0.12
0.2422
CO-56
8704
5.712E-0O3pCi/g
1.869E-002
1.869E-002
2.580E-001
1.242E-001
0.02
0.0187
CO-57
13694
1.046E-002pCi/g
4.413E-002
4.413E-002
1.564E-001
7.667E-002
0.07
0.0441
CO-58
8698
2.582E-002pCi/g
6.995E-002
6.994E-002
2.376E-001
1.142E-001
0.11
0,0700
CO-60
8692
1.791E+001 pCi/g
9.248E-001
2.166E-001
3.666E-002
1.159E-002
488.51
0.9248
CR-51
8604
-5.434E-002pCi/g
5.663E-001
5.663E-001
1.911E+000
9.317E-001
-0,03
0.5663
CS-134
8553
8.527E-0O2pCi/g
5.497E-002
5.479E-002
2.246E-001
1.085E-001
0,38
0.0550
CS-136
8546
6.970E-002pCi/g
6.544E-002
6.532E-002
2.257E-001
1.082E-001
0,31
0,0654
CS-137
8539
2.987E+001 pCi/g
1.592E+000
3.439E-001
2.525E-001
1.216E-001
118.28
1.5915
EU-152
7145
4.783E-001 pCi/g
2.253E-001
2.239E-001
5.623E-001
2.718E-001
0.85
0.2253
EU-154
7138
1.944E-001 pCi/g
3.227E-001
3.226E-001
2.414E+000
1.167E+000
0.08
0.3227
EU-155
7131
4.818E-002pCi/g
1.507E-001
1.507E-001
5.063E-001
2.471 E-001
0.10
0.1507
FE-59
7073
1.976E-001 pCi/g
1.432E-001
1.428E-001
4.736E-001
2.265E-001
0.42
0.1432
GA-68
18005
5.250E+000pCi/g
2.726E+000
2.710E+000
8.844E+000
4.219E+000
0.59
2.7260
GD-153
6824
1.212E-001pCi/g
8.816E-002
8.785E-002
4.318E-001
2.115E-001
0.28
0.0882
HF-181
6495
8.831 E-002pCi/g
8.376E-002
8.363E-002
2.320E-001
1.121 E-001
0.38
0.0838
HG-203
6466
7.767E-002pCi/g
5.465E-002
5.447E-002
1.522E-001
7.346E-002
0.51
0.0546
1-131
6380
3.072E-003pCi/g
6.170E-002
6.170E-002
2.094E-001
1.016E-001
0.01
0,0617
IR-192
6303
3.665E-002pCi/g
6.296E-002
6.292E-002
2.108E-001
1.027E-001
0.17
0.0630
K-40
6148
-2.504E-001 pCi/g
9.590E-001
9.589E-001
1.437E+000
6.508E-001
-0,17
0.9590
LA-140
6096
7.503E-002pCi/g
7.767E-002
7.757E-002
1.S00E-001
8.688E-002
0.39
0.0777
MN-54
5382
-6.356E-002pCi/g
7.748E-002
7.741 E-002
2.597E-001
1.252E-001
-0.24
0.0775
NA-22
5201
2.684E-003pCi/g
3.144E-002
3.144E-002
1.160E-001
5.146E-002
0.02
0.0314
NB-94
5160
7.491 E-0O3pCi/g
1.036E-002
1.035E-002
1.803E-001
8.592E-002
0,04
0.0104
NB-95
5154
5.861 E-003pCi/g
6.671 E-002
6.671 E-002
2.282E-001
1.097E-001
0.03
0.0667
ND-147
5083
-5.976E-001 pCi/g
5.313E-001
5.302E-001
1.763E+000
8.557E-001
-0.34
0.5313
NP-237
4757
-6.326E-001 pCi/g
3.879E-001
3.863E-001
1.273E+000
6.261 E-001
-0.50
0.3879
NP-239
4751
1.659E-001 pCi/g
1.170E-001
1.165E-001
3.854E-001
1.870E-001
0.43
0,1170
PA-231
4541
2.101E-001 pCi/g
1.792E+000
1.792E+000
6.049E+000
2.946E+000
0,03
1.7916
PA-233
4535
8.968E-002pCi/g
1.522E-001
1.521 E-001
5.093E-001
2.482E-001
0,18
0.1522
PA-234
4528
2.653E-001 pCi/g
1.500E-001
1.494E-001
7.114E-001
3.483E-001
0.37
0.1500
PA-234M
19453
-2.813E-001 pCi/g
1.067E+001
1.067E+001
3.643E+001
1.757E+001
-0.01
10.6698
PB-210
4467
9,199E+002pCi/g
5.477E+001
9.060E+000
1.538E+001
7.626E+000
59.82
54.7700
2/29/2016 6:13:49PM Page 1 of 4 RadCapture, version 5.1.91, released 2/24/2016
Page 491 of 551
TestAmerica
THE LEADER IN ENVIRONMENTAL TESTING
-------
PB-212
4454
6.332E-001 pCi/g
1.510E-001
1.453E-001
3.483E-001
1.697E-001
1.82
0.1510
PB-214
4448
5.128E-001pCI/g
1.570E-001
1.547E-001
4.982E-001
2.424E-001
1.03
0,1570
PM-144
19585
2.182E-002pCi/g
2.495E-002
2.492E-002
1.999E-001
9.579E-002
0.11
0,0249
PM-146
2464
2.659E-002pCi/g
2.213E-002
2.209E-002
5.997E-001
2,871 E-001
0.04
0,0221
RH-106
1882
8.7O5E-O03pCi/g
4.824E-001
4.824E-001
1.665E+000
7.944E-001
0.01
0.4824
RU-103
1828
-2.228E-002pCi/g
7.147E-002
7.146E-002
2.412E-001
1.171 E-001
-0.09
0.0715
SB-124
1784
1.479E-002pCi/g
6.348E-002
6.347E-002
2.156E-001
1.040E-001
0.07
0.0635
SB-125
1777
6.246E-002pCi/g
8.163E-002
8.157E-002
8.005E-001
3.905E-001
0.08
0.0816
SC-46
1739
4.902E-002pCi/g
5.829E-002
5.824E-002
2.659E-001
1.280E-001
0.18
0.0583
SN-113
1570
-6.202E-002pCi/g
9.565E-002
9.560E-002
3.201 E-001
1.558E-001
-0.19
0,0956
SN-126
17459
2.876E-001 pCi/g
5.839E-001
5.837E-001
1.948E+000
9.564E-001
0.15
0.5839
TA-182
1301
9.507E-002pCi/g
7.136E-002
7.120E-002
7.354E-001
3.508E-001
0,13
0.0714
TC-99M
17412
-4.559E-004pCi/g
4.481 E-002
4.481 E-002
1.508E-001
7.382E-002
0,00
0.0448
TH-227
1058
3.043E+O00pCi/g
1.854E+000
1.846E+000
6.083E+000
3.012E+000
0.50
1.8537
TH-229
1046
4.315E-O02pCi/g
8,927 E-002
8.920E-002
3.602E+000
1.763E+000
0.01
0,0893
TH-234
1027
4.427E-001 pCi/g
8.093E-001
8.090E-001
5.471 E+000
2.690E+000
0.08
0.8093
TL-208
929
2.014E-001 pCi/g
1.080E-001
1.075E-001
2.276E-001
1.095E-001
0.88
0.1080
U-235
281
7.771 E-002pCI/g
2.597E-001
2.597E-001
1.183E+000
5.786E-001
0,07
0.2597
Y-88
74
7.631 E-003pCi/g
1.276E-002
1.276E-002
2.917E-001
1.406E-001
0.03
0.0128
ZN-65
31
2.900E-001 pCi/g
1.832E-001
1.827E-001
6.023E-001
2.895E-001
0.48
0,1832
ZR-95
7
5.699E-0O2pCi/g
8.566E-002
8.560E-002
2.916E-001
1.378E-001
0.20
0.0857
Laboratory Control Sample Information
Sample II)
LCS 160-229576-2-A
WRKNO Analvte
LCS 160-229576-2-A CS-137
CO-60
AM-241
Activity.
2.987E+001 pCi/g
1.791E+001 pCi/g
9.980E+001 pCi/g
StdAdded
2.992E+001
1.803E+001
9.719E+001
Recovery
99.83%
99.31%
102.69%
ZFactor
-0,0229
-0.0954
0.3571
Sample Duplicate Information
Sample ID Dun Sample ID Analvte Samp Activity Pup Activity RI'D RER PER Flag ZFactor
2/29/2016
6:13:49PM
Page 2 of 4 RadCapture, version 5.1.91, released 2/24/2016
Page 492 of 551
-------
ACV TOP 2016
Gamma Detector 3
Cs-137
Co-60
Am-241
Detector
Recovery
Recovery
Recovery
3
99.83%
99.31%
102.69%
Standard ID
Tuna Can LCS
Tuna Can LCS_00005 #776670
Cert #74139-334 Ref. date 10/1/2006
Known Activity:
Cs-137 29.92 pCi/g
Co-60 18.03 pCi/g
Am-241 97.19 pCi/g
Recovered Activity:
Cs-137 29.87 pCi/g
Co-60 17.91 pCi/g
Am-241 99.8 pCi/g
Original count ID: LCS 160-229576-2-A
1st review: Qi/Lj&T
2nd review 3/////?
SOP:ST-RD-0102 current rev. Gamma Det3 AVCTOP 2016.xls
Page 493 of 551
Printed: 3/1/2016
-------
Test America St. Louis
Spectrum ID: 3_Gamma_20160098
Sample Description: 229576_Gamma_LCS 160-229576~2-A
Detector: Ge 3 SN/131
Batch ID: 229576
Work Order Number: Gamma
Lot Number: LCS 160-229576-2-A
Decay to Time: 1/19/2016 07:22 Live Time: 1800 sec
Acquisition Time: 1/19/2016 07:22:44 Real Time: 1808 sec
Analysis Time: 1/19/2016 07:53 Dead Time: 0.44 %
Analysis Quantity: 1.000E+00 Sample
Efficiency Cal File
Efficiency Cal Desc
Efficiency Cal Date
Energy Cal Date
Library
Bkgd Correction File
3_Soil_TunaCan.Clb
3_Soil_TunaCan_90 099_03 2 712
3/28/2012 11:26
2/28/2012 19:25
Client_Long_Revll.lib
3 2016-01-10 0555.PBC
1-Sigma 1-Sigma 1-Sigma Minimum
Counting Counting Total Detectable
Nuclide Activity Uncert Uncert Uncert Activity
Bg/Sample % Bq/Sample Bq/Sample Bq/Sample
BE- 7
-1.060E+00
NA-22
3.3 95E-02
K-40
-3.167E+00
Sc-46
6.201E-01
CR-51
-6.874E-01
MN-54
-8.041E-01
FE-59
2.500E+00
Co-56
7.226E-02
CO-57
1.323E-01
CO - 58
3.266E-01
CO-60
2.266E+02
ZN-65
3.668E+00
NB-94
9.476E-02
ZR-95
7.209E-01
NB-95
7.414E-02
RU-103
-2.818E-01
RH-10 6
1.101E-01
AG-10 8M
-5.2 81E-01
AG-110M
-4.523E-02
SN-113
- 7.845E-01
SB-124
1.872E-01
SB-125
7.901E-01
1-131
3.887E-02
Gd-153
1.534E+00
Ga-68
6.641E+01
Tc-99m
-5.768E-03
BA-133
7.429E-01
CS-134
1.079E+00
CS-137
3.779E+02
CE-139
4.041E-01
Ba-140
5.082E-02
La-140
9.492E-01
CE-141
-1.174E+00
CE-144
5.247E+00
PM-144
2 . 760E-01
EU-152
6 . 050E+00
EU-154
2 . 459E+00
EU-155
6.095E-01
HF-181
1.117E+00
Ta-182
1.203E+00
Hg-203
9 . 826E-01
TL-208
2.547E+00
pm-146
3.364E-01
773 .9
8 .206E+00
1172 . 0
3 . 978E-01
383 . 0
1.213E+01
118 .8
7 . 368E-01
1042 . 0
7 .164E+00
121 .8
9 . 7 9 3 E - 01
72 .3
1. 807E+00
327 .2
2 . 365E-01
422 .0
5 . 583E-01
270 .9
8.848E-01
1.2
2 . 740E+00
63 .0
2 . 311E+00
138 .2
1. 310E-01
150 .2
1. 083E+00
1138 . 0
8 .439E-01
320 .7
9 . 040E-01
5542 . 0
6 .103E+00
162 .6
8.58 8E-01
612 .0
2.768E-01
154 .1
1.209E+00
429 .0
8.029E-01
130 .6
1.032E+00
2008 . 0
7.805E-01
72 .5
1.111E+00
51.6
3.428E+01
9829 . 0
5.669E-01
156 .3
1.161E+00
64 .3
6.931E-01
1.2
4.350E+00
155 .2
6.272E-01
95 .5
4.856E-02
103 .4
9.813E-01
89 .7
1.053E+00
84 .7
4.442E+00
114 .2
3.152E-01
46 . 8
2 . 832E+00
166 . 0
4 . 081E+00
312 .7
1. 906E+00
94 .7
1. 058E+00
74 .9
9.007E-01
70 .1
6.890E-01
53 .4
1.360E+00
83 • Page 4Sft-(7f3$P|- 01
8.206E+00
2 . 773E+01
3 . 978E-01
1.467E+00
1.213E+01
1. 818E+01
7.374E-01
3 . 363E+00
7.164E+00
2.417E+01
9.801E-01
3.286E+00
1.811E+00
5.991E+00
2.3 65E-01
3 . 263E+0 0
5 . 583E-01
1. 978E+00
8.849E-01
3 . 006E+00
1.170E+01
4.63 8E-01
2.318E+00
7.619E+00
1.310E-01
2.281E+0 0
1. 084E+00
3.688E+00
8.43 9E-01
2.887E+00
9.041E-01
3 . 051E+00
6.103E+00
2 .106E+01
8 . 592E-01
2 . 881E+00
2.768E-01
5 . 626E+00
1.210E+00
4.049E+00
8 . 03 0E-01
2.727E+00
1.033E+00
1.013E+01
7.805E-01
2.649E+00
1.115E+00
5.462E+00
3.448E+01
1.119E+02
5.669E-01
1.908E+00
1.162E+00
3.890E+00
6.954E-01
2 . 841E+00
2.013E+01
3 .195E+00
6 .283E-01
2.095E+00
4.863E-02
9.896E+00
9.826E-01
2.4 04E+0 0
1.055E+00
3.492E+00
4.451E+00
1.472E+01
3.156E-01
2.529E+00
2.850E+00
7.114E+00
4.082E+00
3.054E+01
1.906E+00
6.405E+00
1. 060E+00
2.935E+00
9.027E-01
9.303E+00
6.913E-01
1.925E+00
1.366E+00
2.879E+00
2.800E-01
7.587E+00
-------
y-88
9.654E-02
167.2
1.614E-01
1.615E-01
3.691E+00
Cd-113m
1.060E+01
99770.0
1.058E+04
1.05 8E+04
3.571E+04
Cd-109
3.455E+01
87 .1
3.008E+01
3.014E+01
4.445E+01
Cf-251
-1.181E+00
259.3
3.063E+00
3.065E+00
1.027E+01
Cf-249
4.565E-01
217.5
9.928E-01
9.93 IE-01
3.803E+00
Sn-126
3.638E+00
203 . 0
7.3 84E+00
7.387E+00
2.464E+01
PB-210
1.164E+04
1. 0
1.146E+02
6.929E+02
1.945E+02
PB-212
8.010E+00
23 . 0
1.838E+00
1.910E+00
4.406E+00
PB-214
6 .487E+00
30.2
1.957E+00
1.986E+00
6.302E+00
BI-207
1.004E+00
72 .2
7.247E-01
7.266E-01
2.4 01E+00
BI-212
1.703E+01
60 . 5
1.03 0E+01
1.034E+01
3.391E+01
BI-214
4.109E+00
43 . 8
1.800E+00
1.813E+0 0
5.895E+00
BI-210M
7.886E-01
165 .4
1.304E+00
1.305E+00
4.363E+00
AC-228
6.281E+00
59.0
3.707E+00
3.721E+00
1.343E+01
TH-227
3.850E+01
60.7
2.336E+01
2.345E+01
7.695E+01
TH-229
5.458E-01
206.7
1.128E+00
1.129E+00
4.557E+01
TH-234
5.601E+00
182 . 7
1.023E+01
1.024E+01
6.921E+01
PA-231
2.657E+00
852 . 9
2.266E+01
2.266E+01
7.652E+01
PA-233
1.135E+00
169.6
1.924E+00
1.925E+00
6.443E+00
PA-234'
3.357E+00
56.3
1.890E+00
1.898E+00
8.999E+00
PA-234M
-3.559E+00
3793.0
1.350E+02
1.350E+02
4.6 08E+02
U-235
9.830E-01
334 .2
3.285E+00
3 .285E+00
1.496E+01
AM-241
1.263E+03
0 . 8
9.848E+00
6.626E+01
1.433E+01
Np-237
-8.003E+00
61.1
4.887E+00
4.908E+00
1.610E+01
Ir-192
4.636E-01
171.7
7.960E-01
7.964E-01
2.666E+00
Cs-136
8.817E-01
93 .7
8.263E-01
8.278E-01
2.856E+00
Np-239
2.099E+00
70 .2
1.474E+00
1.480E+00
4.876E+00
Nd-147
-7.560E+00
88 . 7
6.708E+00
6.722E+00
2.230E+01
Total 1.375E+04
Analyst: kody Saulters
Page 495 of 551
-------
TestAmerica
rt TING
ANNUAL CALIBRATION VERIFICATION
Detector ID:
Detector# 5
~
SpectrumID:
5_20160128006_EffVe rif
*
Analysis Description:
ACVTop-776670;T unaCan2006
Calibration:
5_Soil_T unaCan_90099_032612
Detector:
Ge 5 S N/157
Verification Date:
Source Assay Date/Time:
2016-01-28 10:21
2006-10-01 11:00
U
03
(Q
CD
CD
a>
Isotope
Gamma
Energy
(kev)
Source Emission Rate (GPS)
(Assay)
Observed Activity
(GPS)
(Actual)
Percent Difference
(%)
Assav-Actual
Assay
o
Am-241
59.54
449
4.57E+02
-1.7%
cn
cn
Cs-137
661.66
400
3.97E+02
0.7%
Co-1332
1332.5
777
7.71 E+02
0.8%
Comments:
Perform Jody Watson 1/28/16 Reviev Rachel Mueller 1/28/16_
C:\User\CRpt\5_20160128006_EffVerif.xls
SOP: ST-RD-0102 current rev 5_EfficiencyVerification.xls Printed 1/28/2016
-------
Test America St. Louis
Spectrum ID: 5_20160128006_EffVerif
Sample Description: ACVTop-776670;TunaCan2006
Detector: Ge 5 SN/157
Source Date: 10/1/2006 11:00
Acquired: 1/28/2016 10:21:33
Analyzed: 2/4/2016 10:52
Analyst: Jody Watson
Efficiency: 5_Soil_TunaCan_90099_032612
Library: DET_EfficiencyVerification.lib
Nuclide
Activity
uCi/Source
Uncertainty
AM-2 41
CS-137
Co-1332
4 . 566E+02
3.974E+02
7.707E+02
0.45
0 . 71
1. 09
Total
1. 625E+03
Page 497 of 551
-------
ORTEC g v - i (1087) Env32 G53W4.25 2/4/2016 10:52:45 AMPage 1
TestAmerica Spectrum name: 5_20160128006_EffVerif.Anl
Sample description
ACVTop-776670;TunaCan2 006
Spectrum Filename: C:\User\SPC\Det5\5_20160128006_EffVerif.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
1/28/2016 10:21:33 AM
7200
7242
0.59 %
5
Detector system
Ge 5 SN/157
Calibration
Filename:
5 Soil TunaCan 90099 032612
5 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/28/2012 7:35:48 PM
0.158 keV
0.250 keV/channel
3.911E-08 keV/channel^2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
3/27/2012 5:20:37
165.85 keV
Quadratic
6 .466115E-01
( -4 .117504E
Quadratic
-2 . 462251E+01
( -9 . 664422E
PM
Uncertainty = 0.8 7
+ ( - 7 . 83 04 54E-01*Log(E) )
03 *Log(E)^2 )
Uncertainty = 1.43
+ ( 9 . 075211E+00*Log(E) )
01*Log(E)^2 )
DET_EfficiencyVerification.lib
0 . 500
Library based
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
Env32 G53W4.2 5
150 ( 37.62keV )
'000 ( 2000.81keV )
10.000%
3
1.0000E+00
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
Page 498 of 551
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Env32 G53W4.25 2/4/2016 10:52:45 AMPage 2
Spectrum name: 5_20160128006_EffVerif.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4 . 0000000E+00
4.0000000E+00
0 . 000%
average of three points.
12 . 000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
10/1/2006 11:00:00 AM
total peaks alloc. 3 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0281
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Energy
Factor
Energy
Ratio
uCi/Sour
46 . 59
62614.
0 . 54
0 . 73
1.791E-02
59 . 55
82059.
0.45
0 . 73
2.534E-02
59 . 54
100 . 000
4 . 566E+02
87 . 79
1068 .
8 . 88
0 . 81
3 .458E-02
661.63
22901.
0 . 71
1.29
9 . 925E-03
661.66
100 . 000
3.973E+02
1173.12
9966 .
1.10
1. 75
6.139E-03
1332 .41
8977 .
1. 09
1. 90
5.515E-03
1332.50
100 . 000
7 . 707E+02
Nuc
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
185.88 46.59 15162. 62614. 3.496E+06 0.54 0.733 -
350.82 87.79 2502. 1068. 3.087E+04 8.88 0.809 - s
4692.76 1173.12 266. 9966. 1.624E+06 1.10 1.754 -
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EfficiencyVerification.lib
Page 499 of 551
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TestAmerica Spectrum name: 5_20160128006_EffVerif.Anl
************** IDENTIFIED PEAK SUMMARY **************
Nuclide Peak Centroid Background Net Area Intensity Uncert FWHM
Channel Energy Counts Counts Cts/Sec 1 Sigma % keV
AM-241 237.79 59.55 13086. 82059. 11.397 0.45 0.731
CS-137 2647.26 661.63 612. 22901. 3.181 0.71 1.293
Co-1332 5329.50 1332.41 77. 8977. 1.247 1.09 1.898
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***^
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
uCi/Source keV uCi/Source uCi/Source COMMENTS
AM-241 4.5663E+02 1.58E+05
59.54 4.566E+02 ( 2.981E+00 4.47E-01 1.00E+02 G
CS-137 3.973 5E+02 1.10E+04
661.66 3.973E+02 ( 2.047E+00 7.08E-01 1.00E+02 G
Co-1332 7.706 8E+02 1.93E+03
1332.50 7.707E+02 ( 3.743E+00 1.09E+00 1.00E+02 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T - Thermal Neutron Activation G - Gamma Ray
F - Fast Neutron Activation X - X-Ray
I - Fission Product P - Positron Decay
Page 500 of 551
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Spectrum name: 5_20160128006_EffVerif.Anl
N - Naturally Occurring Isotope S
P - Photon Reaction D
C - Charged Particle Reaction K
M - No MDA Calculation A
R - Coincidence Corrected C
H - Halflife limit exceeded
Single-Escape
Double-Escape
Key Line
Not in Average
Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN
Time of Count Time Corrected Uncertainty
Nuclide Activity Activity Counting
uCi/Source uCi/Source
S A M P L
1 Sigma
MDA
AM-241 4.4986E+02 4.5663E+02 4.468E-01% 2.98E+00
CS-137 3.2 04 9E+02 3.9735E+02 7.077E-01% 2.05E+00
Co-1332 2.2610E+02 7.7068E+02 1.091E+00% 3.74E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.8 keV) 9.965E+02 uCi/Source
Total Decayed Activity ( 37.6 to 2000.8 keV) 1.6246621E+03 uCi/Source
Page 501 of 551
-------
TestAmerica
rt TING
ANNUAL CALIBRATION VERIFICATION
Detector ID:
Detector# 7
SpectrumID:
7_20160123003_EffVe rif
*
Analysis Description:
ACVTop-776670;T unaCan2006
Calibration:
7_T unaCan_90099_032712
Detector:
Ge 7 S N/154
Verification Date:
Source Assay Date/Time:
2016-01-23 19:25
2006-10-01 11:00
U
03
(Q
CD
cn
o
ro
Isotope
Gamma
Energy
(kev)
Source Emission Rate (GPS)
(Assay)
Observed Activity
(GPS)
(Actual)
Percent Difference
(%)
Assav-Actual
Assay
o
Am-241
59.54
449
4.38E+02
2.5%
cn
cn
Cs-137
661.66
400
3.86E+02
3.6%
Co-1332
1332.5
777
7.19E+02
7.5%
Comments:
Perform Kody Saulters 2/4/16 Reviev Jody Watson 2/4/16_
C:\User\CRpt\7_20160123003_EffVerif.xls
SOP: ST-RD-0102 current rev 7_EfficiencyVerification.xls Printed 2/4/2016
-------
Test America St. Louis
Spectrum ID: 7_20160123003_EffVerif
Sample Description: ACVTop-776670;TunaCan2006
Detector: Ge 7 SN/154
Source Date: 10/1/2006 11:00
Acquired: 1/23/2016 19:25:53
Analyzed: 2/4/2016 10:49
Analyst: Jody Watson
Efficiency: 7_TunaCan_90099_032 712
Library: DET_EfficiencyVerification.lib
Nuclide
Activity
uCi/Source
Uncertainty
AM-2 41
CS-137
Co-1332
4 .380E+02
3.857E+02
7 .189E+02
0.38
0 . 59
0 . 94
Total
1.543E+03
Page 503 of 551
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TestAmerica Spectrum name: 7_20160123003_EffVerif.Anl
Sample description
ACVTop-776670;TunaCan2 006
Spectrum Filename: C:\User\SPC\Det7\7_20160123003_EffVerif.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
1/23/2016 7:25:53 PM
7200
7361
2.18 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
7 TunaCan 90099 032712
7 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/23/2012 8:40:56 AM
0.117 keV
0.250 keV/channel
3.508E-09 keV/channel^2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
3/16/2012 11:45:14 AM
165.85 keV
Quadratic
6 . 716580E-01
( -2 . 065917E
Quadratic
-2 . 689695E+01
Uncertainty = 0.8 7
+ (-6 .166540E-01*Log(E) )
02*Log(E)^2 )
Uncertainty = 1.4 8
+ ( 1. 019544E+01*Log(E) )
( -1.081671E+00*Log(E) 2
DET_EfficiencyVerification.lib
0 . 500
Library based
Env32 G53W4.2 5
150 ( 3 7.61keV )
'000 ( 2000.12keV )
10.000%
3
1.0000E+00
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
Page 504 of 551
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Env32 G53W4.25 2/4/2016 10:49:24 AMPage 2
Spectrum name: 7_20160123003_EffVerif.Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4 . 0000000E+00
4.0000000E+00
0 . 000%
average of three points.
12 . 000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
10/1/2006 11:00:00 AM
total peaks alloc. 3 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0434
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Energy
Factor
Energy
Ratio
uCi/Sour
36 . 52
1402 .
9.33
1. 11
1.474E-02
46 .60
75982.
0.45
0 . 84
2.485E-02
59 . 55
114994.
0.38
0 . 89
3 . 702E-02
59 . 54
100 . 000
4 .380E+02
87 . 94
1428 .
8 .44
0 . 97
5 . 326E-02
661.74
33440.
0 . 59
1.49
1.492E-02
661.66
100 . 000
3 . 857E+02
1173.38
13650.
0 . 99
1. 95
8.928E-03
1332 . 63
12093.
0 . 94
1. 99
7.950E-03
1332.50
100 . 000
7.189E+02
Nuc
************ U
Peak Centroid
Channel Energy
IDENTIFIED
Background Net Area
Counts Counts
PEAK
Efficiency
* Area
SUM
Uncert
1 Sigma '
MAR
FWHM
keV
************
Suspected
Nuclide
145.62 36.52 4964
185.78 46.56 20640
351.31 87.94 3932
4693.26 1173.38 567
1402. 9.512E+04 9.33 1.111
82430. 3.318E+06 0.48 0.912
1428. 2.6 82E+04 8.44 0.972
13650. 1.52 9E+06 0.99 1.950
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list
C - Area < Critical level.
This section based on library: DET_EfficiencyVerification.lib
Page 505 of 551
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TestAmerica Spectrum name: 7_20160123003_EffVerif.Anl
************** IDENTIFIED PEAK SUMMARY **************
Nuclide Peak Centroid Background Net Area Intensity Uncert FWHM
Channel Energy Counts Counts Cts/Sec 1 Sigma % keV
AM-241 237.75 59.55 18759 . 114994 . 15.971 0.38 0.895
CS-137 2646.69 661.74 882. 33440. 4.644 0.59 1.494
Co-1332 5330.24 1332.63 117. 12093. 1.680 0.94 1.990
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***^
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
uCi/Source keV uCi/Source uCi/Source COMMENTS
AM-241 4.3 796E+02 1.58E+05
59.54 4.380E+02 ( 2.441E+00 3.82E-01 1.00E+02 G
CS-137 3.8573E+02 1.10E+04
661.66 3.857E+02 ( 1.628E+00 5.85E-01 1.00E+02 G
Co-1332 7.1885E+02 1.93E+03
1332.50 7.189E+02 ( 3.157E+00 9.42E-01 1.00E+02 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T - Thermal Neutron Activation G - Gamma Ray
F - Fast Neutron Activation X - X-Ray
I - Fission Product P - Positron Decay
Page 506 of 551
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Spectrum name: 7_20160123003_EffVerif.Anl
N - Naturally Occurring Isotope S
P - Photon Reaction D
C - Charged Particle Reaction K
M - No MDA Calculation A
R - Coincidence Corrected C
H - Halflife limit exceeded
Single-Escape
Double-Escape
Key Line
Not in Average
Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN
Time of Count Time Corrected Uncertainty
Nuclide Activity Activity Counting
uCi/Source uCi/Source
S A M P L
1 Sigma
MDA
AM-241 4.314 7E+02 4.3796E+02 3.822E-01% 2.44E+00
CS-137 3.1121E+02 3.8573E+02 5.852E-01% 1.63E+00
Co-1332 2.1125E+02 7.1885E+02 9.418E-01% 3.16E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.6 to 2000.1 keV) 9.539E+02 uCi/Source
Total Decayed Activity ( 37.6 to 2000.1 keV) 1.5425436E+03 uCi/Source
Page 507 of 551
-------
TestAmerica
rt TING
ANNUAL CALIBRATION VERIFICATION
Detector ID:
Detector# 8
~
SpectrumID:
8_20160128004_EffVe rif
*
Analysis Description:
ACVTop-776670;T unaCan2006
Calibration:
8_Soil_TunaCan_90099_032712
Detector:
Ge 8 SN/174
Verification Date:
Source Assay Date/Time:
2016-01-28 18:34
2006-10-01 11:00
U
03
(Q
CD
cn
o
CO
Isotope
Gamma
Energy
(kev)
Source Emission Rate (GPS)
(Assay)
Observed Activity
(GPS)
(Actual)
Percent Difference
(%)
Assav-Actual
Assay
o
Am-241
59.54
449
4.79E+02
-6.7%
cn
cn
Cs-137
661.66
400
3.90E+02
2.5%
Co-1332
1332.5
777
7.56E+02
2.7%
Comments:
Perform Aaron Schroder 1 /28/16 Reviev Jody Watson 1 /29/16_
C:\User\CRpt\8_20160128004_EffVerif.xls
SOP: ST-RD-0102 current rev 8_EfficiencyVerification.xls Printed 1/29/2016
-------
Test America St. Louis
Spectrum ID: 8_20160128004_EffVerif
Sample Description: ACVTop-776670;TunaCan2006
Detector: Ge 8 SN/174
Source Date: 10/1/2006 11:00
Acquired: 1/28/2016 18:34:05
Analyzed: 2/4/2016 10:51
Analyst: Jody Watson
Efficiency: 8_Soil_TunaCan_90099_032 712
Library: DET_EfficiencyVerification.lib
Nuclide
Activity
uCi/Source
Uncertainty
AM-2 41
CS-137
Co-1332
4.789E+02
3 . 899E+02
7.564E+02
0.41
0 . 64
0 . 99
Total
1. 625E+03
Page 509 of 551
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ORTEC g v - i (1087) Env32 G53W4.25 2/4/2016 10:51:02 AMPage 1
TestAmerica Spectrum name: 8_20160128004_EffVerif.Anl
Sample description
ACVTop-776670;TunaCan2 006
Spectrum Filename: C:\User\SPC\Det8\8_20160128004_EffVerif.Anl
Acquisition information
Start time:
Live time:
Real time:
Dead time:
Detector ID:
1/28/2016 6:34:05 PM
7200
7434
3 .15 %
Detector system
Ge 8 SN/174
Calibration
Filename:
8 Soil TunaCan 90099 032712
8 Soil TunaCan.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Log(Eff):
Below the Knee:
Log(Eff):
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
2/28/2012 10:34:41 AM
0.052 keV
0.250 keV/channel
5.282E-10 keV/channel^2
3/28/2012 10:35:20 AM
165.85 keV
Quadratic Uncertainty = 1.3 9
-1.098764E-01 + (-4.958544E-01*Log(E) )
( -2.572270E-02*Log(E)^2 )
Quadratic Uncertainty = 1.71
-2.525301E+01 + ( 9.3 982 53E+00*Log(E) )
( -1.000034E+00*Log(E)^2 )
DET_EfficiencyVerification.lib
0 . 500
Library based
Env32 G53W4.2 5
150 ( 37.55keV )
'000 ( 1999.96keV )
10.000%
3
1.0000E+00
1.0000E+00/( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
Page 510 of 551
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Env32 G53W4.25 2/4/2016 10:51:02 AMPage 2
Spectrum name: 8_20160128004_EffVerif .Anl
Random error:
Systematic error:
Fraction Limit:
Background width:
Half lives decay limit:
Activity range factor:
Min. step backg. energy
Multiplet shift channel
4 . 0000000E+00
4.0000000E+00
0 . 000%
average of three points.
12 . 000
2 . 000
0 . 000
2 . 000
Corrections Status
Decay correct to date: YES
Decay during acquisition: YES
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
10/1/2006 11:00:00 AM
total peaks alloc. 3 cutoff: 5.00E+01%
Energy Calibration
Normalized diff: 0.0632
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E
* * * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Energy
Factor
Energy
Ratio
uCi/Sour
46 . 57
74004.
0 .44
1. 01
2.005E-02
59 . 58
102880.
0.35
1. 02
2.881E-02
59 . 54
100 . 000
5 . 034E+02
cn
o
00
00
1218 .
9 . 96
0 . 76
3 . 993E-02
661.54
27378.
0 . 64
1.34
1. 209E-02
661.66
100 . 000
3.899E+02
1173.07
11810.
1. 00
1. 56
7.454E-03
1332 .31
10667.
0 . 99
1. 75
6.678E-03
1332.50
100 . 000
7 . 564E+02
Nuc
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
185.94 46.53 19029. 71370. 3.560E+06 0.54 0.847 -
352.16 88.09 3683. 1218. 3.051E+04 9.96 0.764 - s
4692.32 1173.07 306. 11810. 1.584E+06 1.00 1.561 -
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_EfficiencyVerification.lib
Page 511 of 551
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TestAmerica Spectrum name: 8_20160128004_EffVerif.Anl
************** IDENTIFIED PEAK SUMMARY **************
Nuclide Peak Centroid Background Net Area Intensity Uncert FWHM
Channel Energy Counts Counts Cts/Sec 1 Sigma % keV
AM-241 237.97 59 . 54 15110 . 97876 . 13 . 594 0 .41 0 . 867D
CS-137 2646.10 661.54 638. 27378. 3.802 0.64 1.335
Co-1332 5329.28 1332.31 68. 10667. 1.482 0.99 1.753
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE ***^
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
uCi/Source keV uCi/Source uCi/Source COMMENTS
AM-241 4.788 9E+02 1.58E+05
59.54 4.789E+02 ( 2.816E+00 4.13E-01 1.00E+02 G
CS-137 3.8993E+02 1.10E+04
661.66 3.899E+02 ( 1.714E+00 6.40E-01 1.00E+02 G
Co-1332 7.563 5E+02 1.93E+03
1332.50 7.564E+02 ( 2.913E+00 9.90E-01 1.00E+02 G
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T - Thermal Neutron Activation G - Gamma Ray
F - Fast Neutron Activation X - X-Ray
I - Fission Product P - Positron Decay
Page 512 of 551
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ORTEC g v - i (1087]
TestAmerica
Env32 G53W4.25 2/4/2016 10:51:02 AMPage 4
Spectrum name: 8_20160128004_EffVerif .Anl
N - Naturally Occurring Isotope S
P - Photon Reaction D
C - Charged Particle Reaction K
M - No MDA Calculation A
R - Coincidence Corrected C
H - Halflife limit exceeded
Single-Escape
Double-Escape
Key Line
Not in Average
Coincidence Peak
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
***** SUMMARY OF NUCLIDES IN
Time of Count Time Corrected Uncertainty
Nuclide Activity Activity Counting
uCi/Source uCi/Source
S A M P L
1 Sigma
MDA
AM-241 4.7179E+02 4.7889E+02 4.129E-01% 2.82E+00
CS-137 3.1450E+02 3.8993E+02 6.397E-01% 1.71E+00
Co-1332 2.2187E+02 7.5635E+02 9.900E-01% 2.91E+00
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
g u M m a R Y
Total Activity ( 37.5 to 2000.0 keV) 1.008E+03 uCi/Source
Total Decayed Activity ( 37.5 to 2000.0 keV) 1.6251797E+03 uCi/Source
Page 513 of 551
-------
Monthly
Backgrounds
Page 514 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 3_20160709004_BGLong
Description: Background Long PBC Count
Acquired: 7/9/2016 5:59:54 PM
Detector: Detector # 3
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 2.34 2.18 2.23 2.41 2.44 2.49 PASS
Analyst: Aaron Schroder Reviewer:
(Page 1 of 8)
Page 515 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:02:14 AMPage 1
TestAmerica Inc Spectrum name: 3_20160709004_BGLong.Anl
Sample description
Background Long PBC Count
Spectrum Filename: C:\User\SPC\Det3\3_2 016 07 09 004_BGLong.Anl
Acquisition information
Start time:
Live time:
Real time
Dead time:
Detector ID:
7/9/2016 5:59:54 PM
43200
43267
0.15 %
3
Detector system
Ge 3 SN/131
Calibration
Filename:
Ge3 QC
3 QC.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/28/2012 7:25:37 PM
0.122 keV
0.250 kev/channel
3.421E-08 keV/channelA2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Below the Knee:
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
Random error:
Systematic error:
Fraction Limit:
Background width:
1/6/2011 8:38:10 AM
0.0 0 keV
Interpolative Uncertainty = 0.00
Interpolative Uncertainty = 0.00
DET_Long Background PBC.lib
0.500
Library based
Env32 G800W064
150 ( 37.59keV )
3 0 0 0 ( 2 0 0 0.5 9keV )
30.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+ 00 / ( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
4.0000000E+00
4.0000000E+00
0 .000%
3
(Page 2 of 8)
Page 516 of 551
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ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 6:02:14 AMPage 2
Spectrum name: 3_20160709004_BGLong.Anl
Half lives decay limit: 12.000
Activity range factor: 2.000
Min. step backg. energy 0.000
Multiplet shift channel 2.000
Corrections
Decay
Status
correct to date: NO
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
total peaks alloc. 20 cutoff: 5.00E+01 °
Energy Calibration
Normalized diff: 0.1910
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E *
* * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
DPS
46.38
479 .
10.48
0 . 75
6.66 0E- 02
46 . 54
4.250
3 . 910E+00
PB210
63 .27
429 .
13.93
0 . 93
9.450E-02
63.29
3.810
2.759E+00
TH234
72 . 78
270 .
15.78
0 . 85
1.103E-01
74.90
671.
6 . 93
0 . 85
1.138E-01
84 . 64
352 .
11.44
0 . 86
1.299E-01
87.41
149 .
23.22
0 . 86
1.345E-01
86 . 54
30.700
8 . 454E-02
EU155
92 . 55
716 .
7.38
1. 15
1.357E-01
92 . 59
5 . 584
2 .186E+00
TH234
93 .35
5 . 561
2 .194E+00
AC2 2 8
185.82
443 .
12.25
1. 33
1.149E-01
185.72
54 . 000
1 . 654E-01
U235
185.99
3.280
2 . 724E+00
Ra2 2 6
198.40
113 .
27.70
1. 07
1.116E-01
238.78
276 .
16 . 02
0 . 85
1.010E-01
238 . 63
43 . 300
1.460E-01
PB212
351.90
253 .
17 .34
0 . 82
7.143E-02
351.93
37.600
2.184E-01
PB214
511. 23
1640 .
4.45
2 .38
5.106E-02
511. 86
20.000
3.723E+00
RH106
569.77
93 .
27.84
1.21
4.619E-02
569.70
97 . 740
4.769E-02
BI207
569.32
15.380
3.029E-01
CS134
569.47
8.200
5.682E-01
PA234
583 .29
127 .
26.74
1. 48
4.508E-02
583.02
84 . 500
7.718E-02
TL208
609.64
273 .
16 .41
1.26
4.286E-02
609.31
46.090
3.197E-01
BI214
610.30
5.750
2.568E+00
RU103
802.76
113 .
25.23
0 . 96
3.217E-02
801.95
8.690
9.3 74E-01
CS134
911.97
123 .
21 . 82
2 . 12
2.760E-02
911.16
29.000
3.567E-01
AC2 2 8
969.92
108 .
23 .35
1. 96
2.638E-02
968.97
17.460
5.445E-01
AC2 2 8
461.25
206 .
9 .85
2 . 00
1.865E-02
1460.83
10.670
2.3 97E+ 00
K4 0
764.82
114 .
14 . 92
1.29
1.571E-02
1764.49
15.400
1.094E+00
BI214
(Page 3 of 8)
Page 517 of 551
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ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:02:14 AMPage 3
TestAmerica Inc Spectrum name: 3_20160709004_BGLong.Anl
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
290.86
72 . 77
772 .
270 .
2 . 447E+03
15 .78
0.846 -
D
299.35
74 . 89
746 .
671 .
5 . 895E+03
6 . 93
0.848 -
D
338.35
84 .61
636 .
352 .
2 . 711E+03
11 .44
0.858 -
SD
349 . 42
87 .37
526 .
149 .
1. 110E+03
23 .22
0.861 -
SD
793.71
198 .40
325 .
113 .
1. 013E+03
27.70
1.072
M
2045.62
511 .23
472 .
1640 .
3 . 213E+04
4.45
2.383 -
S
3211.90
802 . 76
146 .
113 .
3 . 523E+03
25.23
0.960 -
SM
S -
- Peak
fails shape tests.
D -
- Peak
area deconvoluted.
L -
- Peak
written from unknown list.
C -
- Area
< Critical level.
M -
- Peak
is close to a library peak
This section based on library: DET_Long Background PBC.lib
********
****** J
D E N T I
FIED PEAK
S U M M A R
Y *******
******'
Nuclide
Peak
Centroid
Background Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts Counts
Cts/Sec 1
Sigma %
keV
PB-210
185.41
46 .44
720. 488.
0. 011
11.67
0 . 747s
TH-2 34
252.78
63 .27
822. 429.
0.010
13 . 93
0 . 934
TH-2 34
370 . 02
92 .55
592. 716.
0 . 017
7.38
1.154S
Ra-2 2 6
743 .36
185 . 82
602. 443.
0.010
12 .25
1. 333s
PB-212
955 . 34
238 .78
480. 276.
0 . 006
16 . 02
0.847s
PB-214
1408.04
351.90
387. 253.
0 . 006
17 .34
0.818s
BI-207
2279.86
569 .77
165. 93.
0 . 002
27.84
1.207
TL-208
2333.95
583 .29
220. 127.
0 . 003
26.74
1. 482
BI-214
2439 . 37
609.64
325. 273.
0 . 006
16 .41
1,262s
AC-228
3648.70
911.97
113. 123.
0 . 003
21 . 82
2 . 125S
AC-228
3880.48
969.92
100. 108.
0 . 003
23 .35
1. 965s
K-40
5844.86
1461.25
44. 206.
0 . 005
9 .85
2 . 001
BI-214
7058.06
1764.82
25. 114.
0 . 003
14 . 92
1,292s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
(Page 4 of 8)
Page 518 of 551
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ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:02:14 AMPage 4
TestAmerica Inc Spectrum name: 3_20160709004_BGLong.Anl
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
DPS keV DPS DPS COMMENTS
K-40 N 2.3967E+00
1460.83 2.397E+00 (
4 . 66E + 11
3.912E-01 9.85E+00 1.07E+01 G
TL-208 N 7.7183E-02
583 . 02 7.718E-02 ? (
277.28 0.000E+00 %
860.56 0.000E+00 %
6.98E+02
4.365E-02 2.67E+01 8.45E+01 G
2.333E-01 9.24E+01 6.31E+00 G
2.202E-01 5.83E+01 1.24E+01 G
PB-210 N 3.9836E+00
46.54 3.984E+00 * (
8.14E+03
1.042E+00 1.17E+01 4.25E+00 G
PB-212 N 1.4598E-01
238.63 1.460E-01 (
300.03 0.000E+00 %
6.98E+02
5.543E-02 1.60E+01 4.33E+01 G
4.884E-01 1.00E+03 3.28E+00 GA
PB-214 N 2.1836E-01
351. 93 2.184E-01 @(
295.09 0.000E+00 %
242.00 0.000E+00
5.84E+05
8.132E-02 1.73E+01 3.76E+01 G
8.175E-02 3.30E+01 1.93E+01 G
3.034E-01 0.00E+00 7.43E+00 GA
BI-207 C 4.7689E-02
569.70 4.769E-02
1063.66 0.000E+00
1.18E+04
3.208E-02 2.78E+01 9.77E+01 G
4.771E-02 7.91E+01 7.45E+01 G
BI-214 N 3.1972E-01
609.31 3.197E-01 *
1120.29 0.000E+00 %
1764.49 1.094E+00 +
5.84E+05
1.016E-01 1.64E+01 4.61E+01 G
2.655E-01 6.54E+01 1.51E+01 G
2.474E-01 1.49E+01 1.54E+01 G
AC-22 8 N 4.2724E-01
911.16 3.567E-01 (
968.97 5.445E-01 &(
338.32 0.000E+00 %
93.35 0.000E+00 ?
2 .10E+03
1.509E-01 2.18E+01 2.90E+01 G
2.474E-01 2.34E+01 1.75E+01 G
1.508E-01 1.15E+02 1.20E+01 G
4.656E-01 0.00E+00 5.56E+00 XA
TH-234 N 2.4183E+00
63.29 2.759E+00 (
92.59 2.186E+00 * (
1.63E+12
8.759E-01 1.39E+01 3.81E+00 G
3.548E-01 7.38E+00 5.58E+00 G
Ra-226
2.7242E+00
185.99 2.724E+00 * (
5.84E+05
7.190E-01 1.23E+01 3.28E+00 G
(Page 5 of 8)
Page 519 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:02:14 AMPage 5
TestAmerica Inc Spectrum name: 3_20160709004_BGLong.Anl
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
s -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** DISCARDED isotope peaks
Nuclide Centroid Background Net Area Intensity Uncert
Energy Counts Counts Cts/Sec 1 Sigma °
***************
Activity
Peakbackground subtraction
*****
S
U M M A R Y
OF N U C L
IDES
IN SAMP
Time of Count
Uncertainty
1 Sigma
Nuclide
Activity
DPS
Counting
MDA
BE - 7
<
1 .2370E-01
NA-2 2
<
4.4140E-02
K-40
2.3967E+00
9.8453E+00%
3 . 912E-01
Sc-46
<
1.4285E-02
CR-51
<
1.5062E-01
MN-54
<
2.7766E-02
FE-59
<
6.3268E-02
Co - 5 6
<
3.1237E-02
CO-5 7
<
1.9432E-02
CO-5 8
<
1.6041E-02
(Page 6 of 8)
Page 520 of 551
-------
ORTEC g v -
TestAmerica Inc
(1087) Env3 2 G800W064 7/10/2016 6:02:14 AMPage 6
Spectrum name: 3_20160709004_BGLong.Anl
CO - 6 0
<
3.4318E-02
ZN-65
<
6.7449E-02
NB - 94
<
3.2012E-02
ZR-95
<
5.1760E-02
NB-95
<
4.1117E- 02
RU-103
<
2.3130E-02
RH-106
<
2.5637E-01
AG-108M
! <
2.1504E-02
AG-110 M
! <
4.5685E-02
SN-113
<
2.8881E-02
SB-124
<
3.0233E-02
SB-125
<
6.0431E-02
1-131
<
1.9339E-02
BA-133
<
3.1899E-02
CS-134
<
3.4978E-02
CS-137
<
3.1819E-02
CE-13 9
<
2.5584E-02
Ba-140
<
8.7595E-02
La-140
<
4.0205E-02
CE-141
<
3.4373E-02
CE-144
<
1.3285E-01
PM-144
<
3.1250E-02
EU-152
<
4.5080E-02
EU-154
<
3.6596E-01
EU-155
<
5.3244E-02
HF-181
<
3.2442E-02
Ta-182
<
1 .4126E-01
Hg-203
<
1.7435E-02
TL-208
#
7.7183E-02
pm-146
<
7.6590E-02
y- 88
<
3.9449E-02
PB-210
#
3.9836E+00
PB-212
#
1.4598E-01
PB-214
#
2 .1836E-01
BI-207
4.7689E-02
BI-212
<
3.4799E-01
BI-214
#
3.1972E-01
BI-210M
! <
2.8015E-02
RA-224
<
5.7204E-01
AC-228
4.2724E-01
TH-2 2 7
<
1.1264E-01
TH-229
<
3.0603E-01
TH-2 34
2 . 4183E+ 0 0
PA-2 31
<
3 . 9748E-01
PA-2 3 3
<
4.4257E-02
PA-2 3 4
<
1.0423E-01
PA-234M
! <
5.2 04 9E+ 0 0
Ra-2 2 6
#
2.7242E+ 0 0
U-235
<
1.1006E-01
2.6745E+ Oli
1.16 6 9E+ 011
1.6 024E+ 011
1.73 3 6E+ 011
2.7 843 E+ Oli
1.64 07E+ Oli
1.5 9 7 9E+ 011
7.3813E+00^
1. 2252E+ 011
4.365E-02
1.042E+00
5.543E-02
8.132E-02
3.208E-02
1.016E-01
1.509E-01
8.759E-01
7.190E-01
(Page 7 of 8)
Page 521 of 551
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ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:02:14 AMPage 7
TestAmerica Inc Spectrum name: 3_20160709004_BGLong.Anl
AM-241 < 7.1454E-02
Np-2 3 7 < 1.8030E-01
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 37.6 to 2000.6 keV) 1.276E+01 DPS
(Page 8 of 8)
Page 522 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 5_20160709002_BGLong
Description: Background Long PBC Count
Acquired: 7/9/2016 5:58:11 PM
Detector: Detector # 5
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.45 1.30 1.35 1.41 1.55 1.60 PASS
Analyst: Aaron Schroder Reviewer:
(Page 1 of 7)
Page 523 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:01:48 AMPage 1
TestAmerica Inc Spectrum name: 5_20160709002_BGLong.Anl
Sample description
Background Long PBC Count
Spectrum Filename: C:\User\SPC\Det5\5_2 016 07 09 002_BGLong.Anl
Acquisition information
Start time:
Live time:
Real time
Dead time:
Detector ID:
7/9/2016 5:58:11 PM
43200
43365
0.38 %
5
Detector system
Ge 5 SN/157
Calibration
Filename:
Ge5 QC
5 QC.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/28/2012 7:35:48 PM
0.158 keV
0.250 kev/channel
3.911E-08 keV/channelA2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Below the Knee:
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
Random error:
Systematic error:
Fraction Limit:
Background width:
1/6/2011 8:03:22 AM
0.0 0 keV
Interpolative Uncertainty = 0.00
Interpolative Uncertainty = 0.00
DET_Long Background PBC.lib
0.500
Library based
Env32 G800W064
150 ( 37.62keV )
3 0 0 0 ( 2000.81keV )
30.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+ 00 / ( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
4.0000000E+00
4.0000000E+00
0 .000%
3
(Page 2 of 7)
Page 524 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 6:01:48 AMPage 2
Spectrum name: 5_20160709002_BGLong.Anl
Half lives decay limit: 12.000
Activity range factor: 2.000
Min. step backg. energy 0.000
Multiplet shift channel 2.000
Corrections
Decay
Status
correct to date: NO
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
total peaks alloc. 13 cutoff: 5.00E+01 °
Energy Calibration
Normalized diff: 0.1104
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E *
* * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
DPS
46 . 59
389 .
9 . 06
0 . 82
5 . 682E-02
46 . 54
4.250
3 . 733E+00
PB210
59 . 44
154 .
23.18
0 . 81
7 . 407E-02
59 . 54
35.900
1 .338E-01
AM2 41
63 .28
374 .
10.23
0 . 79
7 . 922E-02
63.29
3.810
2 . 872E+00
TH234
74.89
115 .
24.92
0 . 81
9 . 469E-02
77.28
124 .
21.97
0 . 82
9 . 789E-02
92 . 54
527 .
8.35
1. 05
1. 129E-01
92 . 59
5 . 584
1 . 935E+00
TH234
93 .35
5 . 561
1 . 941E+00
AC2 2 8
185.89
267 .
10.95
1. 03
9 . 603E-02
185.72
54 . 000
1 .191E-01
U235
185.99
3.280
1 . 961E+00
Ra2 2 6
295.22
104 .
23.54
0 . 82
6.95 0E- 02
295.09
19.300
1 . 791E-01
PB214
351.67
200 .
15.51
1. 32
5.58 0E- 02
351. 93
37.600
2.213 E-01
PB214
511.09
1010 .
6.10
2 . 45
3.835E-02
511.86
20.000
3.052E+00
RH106
609.20
152 .
21.54
1. 14
3.200E-02
609.31
46.090
2.386E-01
BI214
610.30
5.750
1.916E+00
RU103
662 .36
125 .
18.15
1. 06
2.86 0E- 02
661.66
85.210
1.187E-01
CS137
1120 . 29
72 .
28.87
0 . 51
1.646E-02
1120 . 29
15.100
6.704E-01
BI214
1120.55
99 . 987
1.013E-01
Sc4 6
1460 . 97
88 .
16.39
1. 90
1.300E-02
1460.83
10.670
1.469E+00
K4 0
1764.21
46 .
26.11
5 . 54
1.105E-02
1764.49
15.400
6.188E-01
BI214
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
29 9719 7478 0 3547 ri5~T77l6E+03 24792 07813 - SD~
(Page 3 of 7)
Page 525 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 6:01:48 AMPage 3
Spectrum name: 5_20160709002_BGLong.Anl
Channel Energy Background
308.75 77.19 306.
2044.98 511.09 322.
Net area
124.
Ef f *Area
1. 262E+03
1010. 2 . 633E+04
Uncert
21. 97
6.10
FWHM
0 .815
2 . 452
Suspected
SD
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library:
DET Long
Background
. PBC.lib
********
****** J
D E N T I
F I
ED P
E A K S
U M M A R
Y *******
******'
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
PB-210
185.89
46.59
284 .
389 .
0.009
9 . 06
0 . 820
AM-2 41
237.34
59.44
336 .
154 .
0 . 004
23 .18
0.811s
TH-2 34
252 . 71
63 .28
312 .
374 .
0.009
10.23
0.794s
TH-2 34
369.85
92 . 54
384 .
527 .
0 . 012
8.35
1.046s
Ra-2 2 6
743.51
185.89
207 .
267 .
0 . 006
10 . 95
1. 033
PB-214
1181.13
295.22
174 .
104 .
0 . 002
23 . 54
0 . 822
PB-214
1407.02
351.67
184 .
200 .
0 . 005
15 .51
1,317s
BI-214
2437.50
609.20
184 .
152 .
0 . 004
21 . 54
1. 137s
CS-137
2650.15
662.36
90 .
125 .
0 . 003
18 .15
1.060
BI-214
4481.54
1120.29
60 .
72 .
0 . 002
28 .87
0.506s
K-40
5843 .30
1460 . 97
24 .
88 .
0 . 002
16 .39
1. 897
BI-214
7054.95
1764.21
16 .
46 .
0 . 001
26 .11
5 . 540s
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
DPS keV DPS DPS COMMENTS
K-40 N 1.4688E+00 4.66E+11
1460.83 1.469E+00 ( 4.263E-01 1.64E+01 1.07E+01 G
CS-137 I 1.1872E-01 1.10E+04
661.66 1.187E-01 &( 4.456E-02 1.82E+01 8.52E+01 G
PB-210 N 3.7332E+00 8.14E+03
46.54 3.733E+00 ( 7.797E-01 9.06E+00 4.25E+00 G
(Page 4 of 7)
Page 526 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
PB-214
N
Env3 2 G800W064 7/10/2016 6:01:48 AMPage 4
Spectrum name: 5_20160709002_BGLong.Anl
Nuclide Ave activity Energy
Activity Code Peak MDA Comments
2.0698E-01
351.93 2.213E-01
295.09 1.791E-01
242.00 0.000E+00
5.84E+05
7.275E-02 1.55E+01 3.76E+01 G
1.108E-01 2.35E+01 1.93E+01 G
1.915E-01 9.52E+01 7.43E+00 GA
BI-214
N
2.3861E-01
609.31 2.386E-01 @(
1120.29 6.704E-01 +
1764.49 6.188E-01 +
5.84E+05
1.035E-01 2.15E+01 4.61E+01 G
3.613E-01 2.89E+01 1.51E+01 G
2.864E-01 2.61E+01 1.54E+01 G
TH-234
N
2.8717E+00
63.29 2.872E+00 * (
92.59 1.935E+00 -
1.63E+12
6.525E-01 1.02E+01 3.81E+00 G
3.452E-01 8.35E+00 5.58E+00 G
Ra-226
1.9614E+00
185.99 1.961E+00 (
5.84E+05
5.130E-01 1.10E+01 3.28E+00 G
AM - 2 41
1.3383E-01
59.54 1.338E-01 * (
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
1. 58E+05
7.659E-02 2.32E+01 3.59E+01 G
Nuclide Codes:
Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
s -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
(Page 5 of 7)
Page 527 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:01:48 AMPage 5
TestAmerica Inc Spectrum name: 5_20160709002_BGLong.Anl
R - Coincidence Corrected C - Coincidence Peak
H - Halflife limit exceeded
*************** DISCARDED isotope peaks
Nuclide Centroid Background Net Area Intensity Uncert
Energy Counts Counts Cts/Sec 1 Sigma °
***************
Activity
Peakbackground subtraction
*****
Nuclide
SUMMARY
Time of Count
Activity
DPS
OF N U C L
Uncertainty
Counting
IDES
1 Sigma
IN SAMPLE *****
MDA
BE - 7
<
2.3676E-01
NA-2 2
<
2.4128E-02
K-40
1.4688E+00
Sc-46
<
4.9825E-02
CR-51
<
1.6048E-01
MN-54
<
2.8526E-02
FE-59
<
5.4692E-02
Co - 5 6
<
3.2515E-02
CO-5 7
<
1.0937E-02
CO-5 8
<
2.9115E-02
CO - 6 0
<
4.2786E-02
ZN-65
<
1 .1980E-01
NB - 94
<
3.2682E-02
ZR-95
<
5.2342E-02
NB-95
<
3.8417E-02
RU-103
<
2.2589E-02
RH-106
<
2.7272E-01
AG-108M
<
2.1208E-02
AG-110 M
<
8.1898E-02
SN-113
<
2.8203E-02
SB-124
<
3.6502E-02
SB-125
<
6.3264E-02
1-131
<
2.2298E-02
BA-133
<
4.1125E-02
CS-134
<
3.2597E-02
CS-137
1.1872E-01
CE-13 9
<
2.2437E-02
Ba-140
<
8.7346E-02
La-140
<
4.3283E-02
CE-141
<
3.5837E-02
CE-144
<
1.6512E-01
PM-144
<
3.2987E-02
EU-152
<
7.1907E-02
EU-154
<
2.3309E-01
EU-155
<
5.0521E-02
1.63 8 9E+ 011
4.263E-01
1.8155E+ 011
4.456E-02
(Page 6 of 7)
Page 528 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:01:48 AMPage 6
TestAmerica Inc Spectrum name: 5_20160709002_BGLong.Anl
HF-181
<
2.0479E-02
Ta-182
<
2.2686E-01
Hg-203
<
2.0146E-02
TL-208
<
3.0257E-02
pm-146
<
8.0361E-02
y- 88
<
3.6587E-02
PB-210
3.7332E+00
9.0560E+00%
7.797E-01
PB-212
<
3.1920E-02
PB-214
2.0698E-01
1.4094E+01%
7.275E-02
BI-207
<
4.3497E-02
BI-212
<
3 . 7812E-01
BI-214
#
2.3 86 IE - 01
2.1540E+01%
1.035E-01
BI-210M
! <
2.8222E-02
RA-224
<
5.3272E-01
AC-228
<
1.1590E-01
TH-2 2 7
<
1 . 7073E-01
TH-229
<
3 . 0616E-01
TH-2 34
#
2.8717E+00
1.0232E+01%
6.525E-01
PA-2 31
<
5.2395E-01
PA-2 3 3
<
4.8273E-02
PA-2 3 4
<
7.6306E-02
PA-2 3 4 M
! <
3.9131E+00
Ra-2 2 6
1.9 614E+ 0 0
1.0951E+01%
5.13 0E-01
U-235
<
9.8216E-02
AM-2 41
#
1.3383E-01
2.3177E+01%
7.659E-02
Np-2 3 7
<
1.3313E-01
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 37.6 to 2000.8 keV) 1.073E+01 DPS
(Page 7 of 7)
Page 529 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 7_20160709002_BGLong
Description: Background Long PBC Count
Acquired: 7/9/2016 5:58:58 PM
Detector: Detector # 7
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.30 1.16 1.21 1.29 1.40 1.45 PASS
Analyst: Aaron Schroder Reviewer:
(Page 1 of 7)
Page 530 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:12:02 AMPage 1
TestAmerica Inc Spectrum name: 7_20160709002_BGLong.Anl
Sample description
Background Long PBC Count
Spectrum Filename: C:\User\SPC\Det7\7_2 016 07 09 002_BGLong.Anl
Acquisition information
Start time:
Live time:
Real time
Dead time:
Detector ID:
7/9/2016 5:58:58 PM
43200
43957
1.72 %
7
Detector system
Ge 7 SN/154
Calibration
Filename:
Ge7 QC
7 QC.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/23/2012 8:40:56 AM
0.117 kev
0.250 kev/channel
3.508E-09 keV/channelA2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Below the Knee:
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
Random error:
Systematic error:
Fraction Limit:
Background width:
1/6/2011 8:06:10 AM
0.0 0 kev
Interpolative Uncertainty = 0.00
Interpolative Uncertainty = 0.00
DET_Long Background PBC.lib
0.500
Library based
Env32 G800W064
150 ( 37.61keV )
3 0 0 0 ( 2000.13keV )
30.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+ 00 / ( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
4.0000000E+00
4.0000000E+00
0 .000%
3
(Page 2 of 7)
Page 531 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 6:12:02 AMPage 2
Spectrum name: 7_20160709002_BGLong.Anl
Half lives decay limit: 12.000
Activity range factor: 2.000
Min. step backg. energy 0.000
Multiplet shift channel 2.000
Corrections
Decay
Status
correct to date: NO
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
total peaks alloc. 10 cutoff: 5.00E+01 %
Energy Calibration
Normalized diff: 0.0864
***** g
U M M A
R Y 0
F P E
A K S I
N RAN
G E *
* * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
DPS
O
LO
414 .
10.25
1 . 08
8.10 IE - 02
46 . 54
4.250
2 . 782E+00
PB210
63.39
487 .
9.34
0 . 88
1.23 IE - 01
63.29
3.810
2 . 408E+00
TH234
92 . 66
620 .
7.31
1. 12
1.86 IE - 01
92 . 59
5 . 584
1 .381E+00
TH234
93 .35
5 . 561
1 .385E+00
AC2 2 8
185.53
293 .
13.08
1. 00
1.634E-01
185.72
54 . 000
7 . 691E-02
U235
185.99
3.280
1 . 267E+00
Ra2 2 6
238.69
196 .
18.55
1. 10
1.417E-01
238.63
43 . 300
7.4 07E-02
PB212
294.98
Ill.
27.43
2 . 76
1.186E-01
295.09
19.300
1.122E-01
PB214
351.83
96 .
28.46
0 . 65
9.546E-02
351.93
37.600
6.215E-02
PB214
511.07
989 .
6 .78
2 .38
6.487E-02
511. 86
20.000
1.767E+00
RH106
1460.76
61.
21.24
1. 84
1.997E-02
1460.83
10.670
6.646E-01
K4 0
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
^04 3799 51170 7 35l7 9 89~i752 5E+04 67^8 2379 1 S
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_Long Background PBC.lib
(Page 3 of 7)
Page 532 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:12:02 AMPage 3
TestAmerica Inc Spectrum name: 7_20160709002_BGLong.Anl
********
****** J
D E N T I
F I E D P
E A
K
S U M M A R
Y *******
******'
Nuclide
Peak
Centroid
Background
Net
Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
PB-210
185.53
46.50
363 .
414 .
0.010
10.25
1 . 078s
TH-234
253 .12
63 .39
396 .
487 .
0 . 011
9.34
0 . 883s
TH-234
370.20
92 .66
374 .
620 .
0 . 014
7.31
1.119s
Ra-226
741.72
185 . 53
294 .
293 .
0 . 007
13 . 08
0.998s
PB-212
954.40
238 .69
295 .
196 .
0 . 005
18 .55
1.098s
PB-214
1179.55
294 . 98
204 .
Ill .
0 . 003
27.43
2.762s
PB-214
1406.99
351.83
179 .
96 .
0 . 002
28.46
0.653s
K-40
5842.73
1460 .76
21.
61 .
0 . 001
21.24
1. 842
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
DPS keV DPS DPS COMMENTS
K-40
N 6.6461E-01
PB-210 N 2.7819E+00
PB-212 N 7.4073E-02
PB-214 N 7.9136E-02
TH-234 N 2.4085E+00
Ra-226
1460.83 6.646E-01 ?( 2.606E-01
46.54 2.782E+00 *( 6.140E-01
238.63 7.407E-02 *( 3.120E-02
300.03 0.000E+00 % 2.660E-01
351.93 6.215E-02 ( 4.194E-02
295.09 1.122E-01 *( 7.003E-02
242.00 0.000E+00 ? 1.404E-01
63.29 2.408E+00 *( 4.720E-01
92.59 1.381E+00 - 2.068E-01
1.2670E+00
185.99 1.267E+00 *( 3.572E-01
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
4 . 66E + 11
2.12E+01 1.07E+01 G
8.14E+03
1.03E+01 4.25E+00 G
6.98E+02
1.85E+01 4.33E+01 G
8.80E+01 3.28E+00 GA
5 . 84E+05
2.85E+01 3.76E+01 G
2.74E+01 1.93E+01 G
0.00E+00 7.43E+00 GA
1.63E+12
9.34E+00 3.81E+00 G
7.31E+00 5.58E+00 G
5.84E+05
1.31E+01 3.28E+00 G
(Page 4 of 7)
Page 533 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:12:02 AMPage 4
TestAmerica Inc Spectrum name: 7_20160709002_BGLong.Anl
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
Nuclide Codes: Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
s -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** DISCARDED isotope peaks
Nuclide Centroid Background Net Area Intensity Uncert
Energy Counts Counts Cts/Sec 1 Sigma °
***************
Activity
Peakbackground subtraction
***** SUMMARY
Time of Count
Nuclide Activity
DPS
OF NUCLIDES
Uncertainty 1 Sigma
Counting
IN SAMPLE *****
MDA
BE - 7
<
1 . 6047E-01
NA-2 2
<
3.1555E-02
K-40
#
6.6461E-01
Sc-46
<
2.0866E-02
CR-51
<
8.7029E-02
MN-54
<
2.0301E-02
FE-59
<
4.3559E-02
Co - 5 6
<
2.0763E-02
CO-5 7
<
8.3165E-03
CO-5 8
<
2.4327E-02
CO - 6 0
<
2.7031E-02
ZN-65
<
5.2883E-02
NB - 94
<
1.6936E-02
2.12 41E+ 01i
2.606E-01
(Page 5 of 7)
Page 534 of 551
-------
ORTEC g v -
TestAmerica Inc
(1087) Env3 2 G800W064 7/10/2016 6:12:02 AMPage 5
Spectrum name: 7_20160709002_BGLong.Anl
ZR-95
<
3.1670E-02
NB-95
<
2.7458E-02
RU-103
<
1.5059E-02
RH-106
<
1.8400E-01
AG-108M
<
1.1924E-02
AG-110 M
<
2.5931E-02
SN-113
<
1.6662E-02
SB-124
<
1.5448E-02
SB-125
<
3.5797E-02
1-131
<
1.2488E-02
BA-133
<
2.6024E-02
CS-134
<
1.8576E-02
CS-137
<
1.8852E-02
CE-13 9
<
8.6236E-03
Ba-140
<
5.4914E-02
La-140
<
3.4319E-02
CE-141
<
1.6035E-02
CE-144
<
6.3422E-02
PM-144
<
1.9340E-02
EU-152
<
3.6340E-02
EU-154
<
1.6467E-01
EU-155
<
2.9252E-02
HF-181
<
7.9311E-03
Ta-182
<
1.1886E-01
Hg-203
<
7.3087E-03
TL-208
<
2.1832E-02
pm-146
<
4.7400E-02
y- 88
<
2.5513E-02
PB-210 #
2.7819E+00
PB-212 #
7.4073E-02
PB-214
7.9136E-02
BI-207
<
2.6280E-02
BI-212
<
2.8809E-01
BI-214
<
4.0953E-02
BI-210M
<
1.5268E-02
RA-224
<
2 . 4955E-01
AC-228
<
8.9822E-02
TH-2 2 7
<
7.8294E-02
TH-229
<
1.7009E-01
TH-2 34 #
2.4085E+00
PA-2 31
<
2.8418E-01
PA-2 3 3
<
2.4264E-02
PA-2 3 4
<
4.3918E-02
PA-2 3 4 M
<
3.0174E+ 0 0
Ra-2 2 6 #
1 . 2670E+00
U-235
<
6.4124E-02
AM-2 41
<
5.4748E-02
Np-2 3 7
<
7.8646E-02
1. 0253E+ 011
1.8546E+ 011
1. 9762E+ 011
6.14 0E-01
3.12 0E-02
4.194E-02
9.3446E+ 0 01
1.3081E+01^
4.72 0E-01
3.572E-01
(Page 6 of 7)
Page 535 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 6:12:02 AMPage 6
TestAmerica Inc Spectrum name: 7_20160709002_BGLong.Anl
# - All peaks for activity calculation had bad shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 37.6 to 2000.1 keV) 7.275E+00 DPS
(Page 7 of 7)
Page 536 of 551
-------
Test America
St. Louis
Background Check
Spectrum: 8_20160709002_BGLong
Description: Background Long PBC Count
Acquired: 7/9/2016 6:00:08 PM
Detector: Detector # 8
Background Evaluation Criteria:
1) Place instrument out of service if Countrate exceeds Control Limits.
2) Investigate high countrate and take corrective action as necessary if Countrate
exceeds Tolerance Limits.
Target L_Ctrl L_Tol Measured H_Tol H_Ctrl Results
Bkgd
Countrate 1.56 1.39 1.45 1.59 1.68 1.74 PASS
Analyst: Aaron Schroder Reviewer:
(Page 1 of 8)
Page 537 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 2:51:26 PMPage 1
TestAmerica Inc Spectrum name: 8_20160709002_BGLong.Anl
Sample description
Background Long PBC Count
Spectrum Filename: C:\User\SPC\Det8\8_2 016 07 09 002_BGLong.Anl
Acquisition information
Start time:
Live time:
Real time
Dead time:
Detector ID:
7/9/2016 6:00:08 PM
72000
74127
2.87 %
Detector system
Ge 8 SN/174
Calibration
Filename:
Ge8 QC
8 QC.Clb
Energy Calibration
Created:
Zero offset:
Gain:
Quadratic:
2/28/2012 10:34:41 AM
0.052 keV
0.250 kev/channel
5.282E-10 keV/channelA2
Efficiency Calibration
Created:
Knee Energy:
Above the Knee:
Below the Knee:
Library Files
Main analysis library:
Library Match Width:
Peak stripping:
Analysis parameters
Analysis engine:
Start channel:
Stop channel:
Peak rejection level:
Peak search sensitivity:
Sample Size:
Activity scaling factor:
Detection limit method:
Random error:
Systematic error:
Fraction Limit:
Background width:
1/6/2011 8:07:20 AM
0.0 0 keV
Interpolative Uncertainty = 0.00
Interpolative Uncertainty = 0.00
DET_Long Background PBC.lib
0.500
Library based
Env32 G800W064
150 ( 37.55keV )
3 0 0 0 ( 19 9 9.9 7keV )
30.000%
3
1.0000E+00 + /- 0.000E+00%
1.0000E+ 00 / ( 1.0000E+00* 1.0000E+00)
1.0000E+00
Reg. Guide 4.16 Method
4.0000000E+00
4.0000000E+00
0 .000%
3
(Page 2 of 8)
Page 538 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 2:51:26 PMPage 2
Spectrum name: 8_20160709002_BGLong.Anl
Half lives decay limit: 12.000
Activity range factor: 2.000
Min. step backg. energy 0.000
Multiplet shift channel 2.000
Corrections
Decay
Status
correct to date: NO
Decay during acquisition: NO
Decay during collection: NO
True coincidence correction: NO
Peaked background correction: NO
Absorption (Internal): NO
Geometry correction: NO
Random summing: NO
Comments
total peaks alloc. 19 cutoff: 5.00E+01 %
Energy Calibration
Normalized diff: 0.1316
• * * * * g
U M M A
R Y 0
F P E
A K S I
N RAN
G E *
* * * *
Peak
Area
Uncert
FWHM
Corrctn
Nuclide
Brnch.
Act.
Nuc
Energy
Factor
Energy
Ratio
DPS
59.50
444 .
9.34
1 . 02
8 . 677E-02
59 . 54
35.900
1 . 974E-01
AM2 41
63 .31
1140 .
4.34
1 . 03
9 . 238E-02
63.29
3.810
4 . 496E+00
TH234
76 . 96
162 .
26.05
0 . 81
1. 126E-01
84 . 23
215 .
28.15
1. 11
1. 233E-01
92 . 62
2014 .
3.79
1. 02
1.295E-01
92 . 59
5 . 584
3 . 868E+00
TH234
93 .35
5 . 561
3 . 881E+00
AC2 2 8
140.03
112 .
29.81
1. 08
1.263E-01
143.80
244 .
15.05
1. 09
1.248E-01
143.79
10.960
2 . 477E-01
U235
185.76
1060 .
6.27
0 . 99
1.108E-01
185.72
54 . 000
2 . 462E-01
U235
185.99
3.280
4 . 056E+00
Ra2 2 6
238.45
366 .
14.63
1.21
9.644E-02
238.63
43 . 300
1 .219E-01
PB212
351. 72
127 .
23.79
1. 53
6.558E-02
351. 93
37.600
7 .154E-02
PB214
569.68
88 .
27.87
1. 24
4.064E-02
569.70
97 . 740
3 . 077E-02
BI207
569.32
15.380
1 . 954E-01
CS134
569.47
8.200
3 . 666E-01
PA234
583 .38
142 .
26.31
1. 13
3.958E-02
583.02
84 . 500
5 . 910E-02
TL208
608.95
138 .
26.16
1. 08
3.75 0E- 02
609.31
46.090
1 .109E-01
BI214
610.30
5.750
8 . 908E-01
RU103
661.82
282 .
13.58
1.35
3.333E-02
661.66
85.210
1 .378E-01
CS137
1000.87
152 .
24.47
0 . 97
2.158E-02
1001.00
0 . 837
1 .172E+01
PA2 34M
1063.06
123 .
20.84
0 . 86
2.040E-02
1063.66
74 . 500
1 .126E-01
BI207
1173 . 32
140 .
14.76
1. 88
1.834E-02
1173 . 24
99.900
1 . 064E-01
CO6 0
1332.46
118 .
19.74
1. 09
1.637E-02
1332.50
99.980
9.969E-02
CO6 0
1461.49
88 .
22.50
1. 95
1.543E-02
1460.83
10.670
7.3 97E-01
K4 0
(Page 3 of 8)
Page 539 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
Env3 2 G800W064 7/10/2016 2:51:26 PMPage 3
Spectrum name: 8_20160709002_BGLong.Anl
************ UNIDENTIFIED PEAK SUMMARY ************
Peak Centroid Background Net Area Efficiency Uncert FWHM Suspected
Channel Energy Counts Counts * Area 1 Sigma % keV Nuclide
307.63
76 . 96
570 .
162 .
1. 437E+03
26 . 05
0.806 -
336 . 73
CO
CO
CO
V£>
CO
215 .
1. 742E+03
28 .15
1.109 -
559.61
139.92
498 .
116 .
9 . 201E+02
28.70
1.085 -
SD
s - Peak fails shape tests.
D - Peak area deconvoluted.
L - Peak written from unknown list.
C - Area < Critical level.
This section based on library: DET_Long Background PBC.lib
********
****** J
D E N T I
F I E D P
E A K
S U M M A R
Y *******
*******
Nuclide
Peak
Centroid
Background
Net Area
Intensity
Uncert
FWHM
Channel
Energy
Counts
Counts
Cts/Sec 1
Sigma %
keV
AM-2 41
237.95
59 . 54
684 .
440 .
0 . 006
9 .66
1.02 2D
TH-2 34
252.96
63 .29
653 .
1140 .
0 . 016
4.34
1.025D
TH-2 34
370.31
92 . 62
954 .
2014 .
0 . 028
3.79
1. 022
U-235
574.97
143 .79
551.
244 .
0 . 003
15 . 03
1. 087D
U-235
742.71
185 . 72
Ill.
1068 .
0 . 015
4.30
0 . 993D
PB-212
953.63
238.45
602 .
366 .
0 . 005
14 . 63
1.213
PB-214
1406.73
351.72
262 .
127 .
0 . 002
23.79
1. 525s
BI-207
2278.64
569 .68
154 .
88 .
0 . 001
27.87
1.235
TL-208
2333.44
583 .38
261.
142 .
0 . 002
26.31
1. 130
BI-214
2435 . 72
608.95
259 .
138 .
0 . 002
26 .16
1. 082s
CS-137
2647 . 23
661 . 82
229 .
282 .
0 . 004
13 .58
1.349
PA-2 3 4 M
4003.48
1000 .87
173 .
152 .
0 . 002
24.47
0 . 972s
BI-207
4252 .26
1063.06
92 .
123 .
0 . 002
20.84
0.859s
CO - 6 0
4693 . 32
1173.32
67 .
140 .
0 . 002
14 .76
1.877
CO - 6 0
5329.89
1332.46
16.
118 .
0 . 002
19.74
1.094s
K-40
5846.04
1461.49
58 .
88 .
0 . 001
22.50
1. 954
s - Peak fails shape tests.
D - Peak area deconvoluted.
A Derived peak area.
(Page 4 of 8)
Page 540 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 2:51:26 PMPage 4
TestAmerica Inc Spectrum name: 8_20160709002_BGLong.Anl
***** SUMMARY OF LIBRARY PEAK USAGE *****
- Nuclide - Average Peak
Name Code Activity Energy Activity Code MDA Value
DPS keV DPS DPS COMMENTS
K-40 N 7.3972E-01
1460.83 7.397E-01 (
4 . 66E + 11
3.232E-01 2.25E+01 1.07E+01 G
CO-60 F 1.03 04E-01
1332 .50 9.969E-02 ? (
1173.24 1.064E-01 (
1.93E+03
3.688E-02 1.97E+01 1.00E+02 G
3.090E-02 1.48E+01 9.99E+01 G
CS-137 I 1.3778E-01
661.66 1.378E-01 (
1.10E+04
3.581E-02 1.36E+01 8.52E+01 G
TL-208 N 5.9103E-02
583.02 5.910E-02 (
277.28 0.000E+00 &
860.56 0.000E+00 &
6.98E+02
3.237E-02 2.63E+01 8.45E+01 G
1.491E-01 8.55E+01 6.31E+00 G
1.972E-01 1.00E+03 1.24E+01 G
PB-212 N 1.2191E-01
238.63 1.219E-01
300.03 0.000E+00
6.98E+02
3.894E-02 1.46E+01 4.33E+01 G
4.687E-01 0.00E+00 3.28E+00 GA
PB-214 N 7.1536E-02
351.93 7.154E-02 (
295.09 0.000E+00 ?
242.00 0.000E+00
5.84E+05
4.401E-02 2.38E+01 3.76E+01 G
7.784E-02 0.00E+00 1.93E+01 G
1.969E-01 0.00E+00 7.43E+00 GA
BI-207 C 3.0770E-02
569.70 3.077E-02 ? (
1063.66 1.126E-01 +
1.18E+04
2.117E-02 2.79E+01 9.77E+01 G
4.329E-02 2.08E+01 7.45E+01 G
BI-214 N 1.1091E-01
609.31 1.109E-01 * (
1120.29 0.000E+00 &
1764.49 0.000E+00 &
5.84E+05
6.245E-02 2.62E+01 4.61E+01 G
1.712E-01 6.22E+01 1.51E+01 G
2.098E-01 1.00E+03 1.54E+01 G
TH-234 N 4.4954E+00
63.29 4.495E+00 (
92.59 3.868E+00 -
1.63E+12
4.802E-01 4.34E+00 3.81E+00 G
2.817E-01 3.79E+00 5.58E+00 G
PA-234M N 1.1715E+ 01
1001.00 1.172E+01 (
766.41 0.000E+00 &
1.63E+12
4.918E+00 2.45E+01 8.37E-01 G
7.156E+00 2.83E+02 2.94E-01 G
(Page 5 of 8)
Page 541 of 551
-------
ORTEC g v - i (1087;
TestAmerica Inc
U-235
N
Env3 2 G800W064 7/10/2016 2:51:26 PMPage 5
Spectrum name: 8_20160709002_BGLong.Anl
Nuclide Ave activity Energy
Activity Code Peak MDA Comments
2.4788E-01
185.72 2.479E-01 } 3.078E-02
143.79 2.479E-01 ?( 1.138E-01
205.33 0.000E+00 % 1.808E-01
163.38 0.000E+00 % 1.676E-01
2.57E+11
4.30E+00 5.40E+01 GA
1.50E+01 1.10E+01 G
4.18E+01 5.01E+00 G
3.70E+01 5.08E+00 G
AM - 2 41
1.9608E-01
59.54 1.961E-01 (
( - This peak used in the nuclide activity average.
* - Peak is too wide, but only one peak in library.
! - Peak is part of a multiplet and this area went
negative during deconvolution.
? - Peak is too narrow.
@ - Peak is too wide at FW25M, but ok at FWHM.
% - Peak fails sensitivity test.
$ - Peak identified, but first peak of this nuclide
failed one or more qualification tests.
+ - Peak activity higher than counting uncertainty range.
- - Peak activity lower than counting uncertainty range.
= - Peak outside analysis energy range.
& - Calculated peak centroid is not close enough to the
library energy centroid for positive identification.
P - Peakbackground subtraction
} - Peak is too close to another for the activity
to be found directly.
1. 58E+05
5.547E-02 9.66E+00 3.59E+01 G
Nuclide Codes:
Peak Codes:
T -
- Thermal Neutron Activation
G -
- Gamma Ray
F -
- Fast Neutron Activation
X -
- X-Ray
I -
- Fission Product
P -
- Positron Decay
N -
- Naturally Occurring Isotope
s -
- Single-Escape
P -
- Photon Reaction
D -
- Double-Escape
C -
- Charged Particle Reaction
K -
- Key Line
M -
- No MDA Calculation
A -
- Not in Average
R -
- Coincidence Corrected
C -
- Coincidence Peak
H -
- Halflife limit exceeded
*************** DISCARDED ISOTOPE PEAKS ***************
Nuclide Centroid Background Net Area Intensity Uncert Activity
Energy Counts Counts Cts/Sec 1 Sigma %
P - Peakbackground subtraction
(Page 6 of 8)
Page 542 of 551
-------
ORTEC g v -
TestAmerica Inc
(1087) Env3 2 G800W064 7/10/2016 2:51:26 PMPage 6
Spectrum name: 8_20160709002_BGLong.Anl
***** SUMMARY
Time of Count
Nuclide Activity
DPS
OF NUCLIDES
Uncertainty 1 Sigma
Counting
IN SAMPLE *****
MDA
BE - 7
<
2.210 IE - 01
NA-2 2
<
2.3975E-02
K-40
7.3972E-01
Sc-46
<
2.0326E-02
CR-51
<
9.9497E-02
MN-54
<
2.1634E-02
FE-59
<
4.0328E-02
Co - 5 6
<
2.0169E-02
CO-5 7
<
1.3309E-02
CO-5 8
<
2.1116E-02
CO - 6 0
1.0304E-01
ZN-65
<
8.6349E-02
NB - 94
<
1.9827E-02
ZR-95
<
3.3544E-02
NB-95
<
3.6005E-02
RU-103
<
1.6960E-02
RH-106
<
1.1141E-01
AG-108M
<
1.6134E-02
AG-110 M
<
3.0125E-02
SN-113
<
2.3283E-02
SB-124
<
2.5934E-02
SB-125
<
5.1466E-02
1-131
<
1.6253E-02
BA-133
<
3.4489E-02
CS-134
<
1.1525E-02
CS-137
1.3778E-01
CE-13 9
<
1.0629E-02
Ba-140
<
6.6494E-02
La-140
<
2.3499E-02
CE-141
<
1.6675E-02
CE-144
<
5.3313E-02
PM-144
<
2.1845E-02
EU-152
<
4.3126E-02
EU-154
<
1.6647E-01
EU-155
<
3.9910E-02
HF-181
<
2.3894E-02
Ta-182
<
1.1464E-01
Hg-203
<
1.9366E-02
TL-208
5.9103E-02
pm-146
<
6.0638E-02
y- 88
<
2.7289E-02
PB-210
<
3.9808E-01
PB-212
1.2191E-01
2.24 9 9E+ 011
3.232E-01
1.23 2 7E+ 011
3.688E-02
1.3585E+01'
3.581E-02
2.63 09E+ 011
1.4632 E+ 011
3.237E-02
3.894E-02
(Page 7 of 8)
Page 543 of 551
-------
ORTEC g v - i (1087) Env32 G800W064 7/10/2016 2:51:26 PMPage 7
TestAmerica Inc Spectrum name: 8_20160709002_BGLong.Anl
PB-214
7.1536E-02
2.3792E+01%
4.401E-02
BI-207 #
3.0770E-02
2.7866E+01%
2.117E-02
BI-212
<
2 . 6010E-01
BI-214 #
1.1091E-01
2.6162E+01%
6.245E-02
BI-210M
<
1.8412E-02
RA-224
<
3.8410E-01
AC-228
<
9.4185E-02
TH-2 2 7
<
7.6651E-02
TH-229
<
2.1018E-01
TH-2 34
4.4954E+00
4.3383E+00%
4.802E-01
PA-2 31
<
4.7624E-01
PA-2 3 3
<
2.6774E-02
PA-2 3 4
<
7.3572E-02
PA-2 3 4 M
1.1715E+01
2 . 4472E+ 01 %
4.918E+00
U-235
2 . 4788E-01
1.5032E+01%
1.138E-01
AM-2 41
1.9608E-01
9.6560E+00%
5.547E-02
Np-2 3 7
<
1.0103E-01
# - All
peaks for activity calculation had bad
shape.
* - Activity omitted from total
& - Activity omitted from total and all peaks had bad shape.
< - MDA value printed.
A - Activity printed, but activity < MDA.
B - Activity < MDA and failed test.
C - Area < Critical level.
F - Failed fraction or key line test.
H - Halflife limit exceeded
S U M M A R Y
Total Activity ( 37.5 to 2000.0 keV) 1.803E+01 DPS
(Page 8 of 8)
Page 544 of 551
-------
Run Logs
Page 545 of 551
-------
Gamma Spectroscopy Run Log
Detector: GV3
Analysis Date
03/27/12 18:49
Count
Minutes
Lab Sample ID
IC 160-11762/1
Client Sample ID
Analysis
Batch
11762
Prep
Batch
Method
Analyst
Initials
JLW
03/27/12 22:50
ICV 160-11762/2
11762
JLW
01/19/16 07:22
ACVTOP 160-238517/1
238517
JLW
07/09/16 17:59
ICB 160-259819/1
259819
RTM
07/11/16 00:16
CCV 160-259962/1
259962
07/11/16 00:40
CCV 160-259962/2
259962
RTM
07/11/16 06:34
CCB 160-259962/3
259962
RTM
07/11/16 07:46
30
160-17814-2
AC-SED-6
259962
257060
GA-01-R
RTM
07/11/16 08:44
30
ZZZZZ
259962
07/11/16 09:25
30
ZZZZZ
259962
07/11/16 18:56
30
ZZZZZ
259962
07/11/16 19:29
30
ZZZZZ
259962
Detector: GV5
Analysis Date
03/26/12 15:05
Count
Minutes
Lab Sample ID
IC 160-12297/1
Client Sample ID
Analysis
Batch
12297
Prep
Batch
Method
Analyst
Initials
JLW
03/27/12 10:12
ICV 160-12297/2
12297
JLW
01/28/16 10:21
ACVTOP 160-236240/1
236240
PS
07/09/16 17:58
ICB 160-259822/1
259822
RTM
07/11/16 00:15
CCB 160-259964/1
259964
RTM
07/11/16 06:36
CCV 160-259964/2
259964
07/11/16 06:58
CCV 160-259964/3
259964
RTM
07/11/16 07:46
30
160-17814-1
AC-SED-4
259964
257060
GA-01-R
RTM
07/11/16 08:46
30
160-17814-4
AC-SED-8
259964
257060
GA-01-R
RTM
07/11/16 09:27
30
ZZZZZ
259964
07/11/16 18:56
30
ZZZZZ
259964
Detector: GV7
Analysis Date
03/27/12 08:10
Count
Minutes
Lab Sample ID
IC 160-12302/1
Client Sample ID
Analysis
Batch
12302
Prep
Batch
Method
Analyst
Initials
JLW
03/27/12 15:25
ICV 160-12302/2
12302
JLW
01/23/16 19:25
ACVTOP 160-236241/1
236241
PS
07/09/16 17:58
ICB 160-259823/1
259823
RTM
07/11/16 00:16
CCB 160-259965/1
259965
RTM
07/11/16 06:34
CCV 160-259965/2
259965
07/11/16 06:57
CCV 160-259965/3
259965
RTM
07/11/16 07:47
30
LCS 160-257060/2-A
259965
257060
GA-01-R
RTM
07/11/16 08:47
30
160-17814-1 DU
AC-SED-4 DU
259965
257060
GA-01-R
RTM
07/11/16 09:26
30
ZZZZZ
259965
07/11/16 10:25
60
ZZZZZ
259965
07/11/16 13:38
30
ZZZZZ
259965
07/11/16 18:57
30
ZZZZZ
259965
07/11/16 23:28
60
ZZZZZ
259965
Count Analysis Prep Analyst
Analysis Date Minutes Lab Sample ID Client Sample ID Batch Batch Method Initials
03/27/12 10:58 IC 160-12311/1 12311 JLW
03/29/12 01:58 ICV160-12311/2 12311 JLW
01/28/16 18:34 ACVTOP 160-236248/1 236248 PS
07/09/16 18:00 ICB 160-259824/1 259824 RTM
Page 1 of 2 TestAmerica St. Louis
Page 546 of 551
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Gamma Spectroscopy Run Log
Detector: GV8 (Continued)
Analysis Date
07/11/16 00:17
07/11/16 06:34
Count
Minutes Lab Sample ID
CCB 160-259963/1
CCV 160-259963/2
Client Sample ID
Analysis
Batch
259963
259963
Prep
Batch
Method
Analyst
Initials
RTM
07/11/16 06:56
07/11/16 07:48
07/11/16 08:45
CCV 160-259963/3
30 MB 160-257060/1-A
30 160-17814-3
AC-SED-7
259963
259963
259963
257060
257060
GA-01-R
GA-01-R
RTM
RTM
RTM
07/11/16 09:28
07/11/16 13:39
07/11/16 18:59
30 ZZZZZ
30 ZZZZZ
ZZZZZ
259963
259963
259963
07/11/16 19:31
30 ZZZZZ
259963
Page 2 of 2
Page 547 of 551
TestAmerica St. Louis
-------
Radiological
Page 548 of 551
-------
Shipping and
Documents
Page 549 of 551
-------
CHAIN OF CUSTODY RECORD
ENVIRONMENTAL PROTECTION AGENCY REGION VII
PC# WOS35JI
ACTIVITY LEADER(Print)
NAME OF SURVEY OR ACTIVITY
DATELOF GOLLECTlOi
3EC
im
CONTENTS
SAMPLE
NUMBER
OF SHIPMENT *-J IUL^W.7,^
: TYPE OF CONTAINERS - ¦ i—nmw
jfikz££hA,
foe-see-y~
CUBITAINER
BOTTLE
BOTTLE
BOTTLE
VOA SET
(2 VIALS EA)
NUMBERS OF CONTAINERS PER SAMPLE NUMBER
IML
ML
§m.
I Mb
onotfer
SAMPLED MEDIA
other
r«gjA e
RECEmNGUBOKATORV
REMARK&OTHER INFORMATION
(condition ol samples upon receipt,
other sample numbers, etc)
!py>v&Qip*&
Ti*A£ Ml o
mt <9b£o
f(to£ OWO
MmM i&$MLCmLvPfMa
XsoToAu \J
X5°T®f>ib rk
160-17814 Chain of Custody
DESCRIPTION OF SHIPMENT
MODE OF SHIPMENT
PIECEfS) CONSISTING OF.
I ICE CHEST(S): OTHER __
BOX(ES)
COMMERCIAL CARRIER:.
COURIER
^.SAMPLER CONVEYED
(SHIPPING DOCUMENT NUMBER)
PERSONNEL CUSTODY RECORD
F(E LIN QUISLED BY
LER)
"| SEALED
UNSEALED
RELINQUISHED BY
z
^SEALED
UNSEALED j"*
DATE
TIME
TIME
RECEIVED BY
L.U OT a
t#*r
"1 SEALED UNSEALED f
RECEIVED BY
"1 SEALED
UNSEALED
REASON FOR CHANGE OF CUSTODY
REASON FOR CHANGE OF CUSTODY
RELINQUISHED BY
DATE
TIME
RECEIVED BY
REASON FOR CHANGETSFCUSToSy"
"IsEALED
UNSEALED^
3
SEALED
ie bbU Ot bb'l
UNSEALED f"
7-EPA-9262( Revised 5/85)
•U.S. GPO: 2002-756-917/40053
-------
Login Sample Receipt Checklist
Client: Tetra Tech EM Inc. Job Number: 160-17814-1
Login Number: 17814 List Source: TestAmerica St. Louis
List Number: 1
Creator: Daniels, Brian J
Question Answer Comment
Radioactivity wasn't checked or is
------- |