THIRD FIVE-YEAR REVIEW REPORT FOR
NEWTON COUNTY WELLS SUPERFUND SITE
NEWTON COUNTY, MISSOURI

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Prepared by

U.S. Environmental Protection Agency
Region 7
Lenexa, Kansas

Digitally signed by ROBERT

ROBERT JURGENS jurgens

Date: 2024.03.29 14:30:23 -05'00'

Robert D. Jurgens, Director

Superfund and Emergency Management Division


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Table of Contents

LIST OF ABBREVIATIONS & ACRONYMS	iii

I.	INTRODUCTION	1

Site Background	1

FIVE-YEAR REVIEW SUMMARY FORM	2

II.	RESPONSE ACTION SUMMARY	3

Basis for Taking Action	3

Response Actions	3

Remedial Action Objectives	4

Remedy Components Selected in the ROD	4

Cleanup Levels	5

Status of Implementation	5

IC Summary Table	5

Systems Operations/Operation & Maintenance	6

III.	PROGRESS SINCE THE LAST REVIEW	6

IV.	FIVE-YEAR REVIEW PROCESS	8

Community Notification, Involvement & Site Interviews	8

Data Review	8

Sitewide Groundwater Sampling	9

Residential Wells	10

Vapor Intrusion	10

Site Inspection	11

V.	TECHNICAL ASSESSMENT	11

QUESTION A: Is the remedy functioning as intended by the decision documents?	11

QUESTION B: Are the exposure assumptions, toxicity data, cleanup levels and Remedial Action

Objectives (RAOs) used at the time of the remedy selection still valid?	13

QUESTION C: Has any other information come to light that could call into question the
protectiveness of the remedy?	15

VI.	ISSUES/RECOMMENDATIONS	15

OTHER FINDINGS	16

VII.	PROTECTIVENESS STATEMENT	16

VIII.	NEXT REVIEW	16

APPENDIX A- REFERENCE LIST

APPENDIX B - MAPS & FIGURES
APPENDIX C - SITE INSPECTION
APPENDIX D- REPORTS

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LIST OF ABBREVIATIONS & ACRONYMS

cis-DCE

cis-l,2-dichloroethene

COC

Contaminant of Concern

CSR

Code of State Regulations

MoDNR

Missouri Department of Natural Resources

EPA

U.S. Environmental Protection Agency

FYR

Five-Year Review

ICs

Institutional Controls

ISCO

In-situ chemical oxidation

MCL

Maximum Contaminant Level

MDHSS

Missouri Department of Health and Senior Services

NPL

National Priorities List

NCWS

Newton County Wells Superfund Site

O&M

Operation & Maintenance

OU

Operable Unit

M-g/L

micrograms per liter

PFAS

Per/Polyfluoroalkyl Substances

PRP

Potentially Responsible Party

ppb

parts per billion

RAO

Remedial Action Objectives

RfC

Acute Reference Concentration

RI/FS

Remedial Investigation/Feasibility Study

RML

Regional Removal Management Levels

ROD

Record of Decision

TBC

To Be Considered(s)

TCE

Trichloroethene

trans-DCE

trans-l,2-dichloroethene

VC

Vinyl Chloride

VI

Vapor Intrusion

VISL

Vapor Intrusion Screening Level

VOC

Volatile Organic Compounds

UU/UE

Unlimited use and unrestricted exposure

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I. INTRODUCTION

The purpose of a Five-Year Review is to evaluate the implementation and performance of a remedy to
determine whether the remedy is and will continue to be protective of human health and the
environment. The methods, findings and conclusions of reviews are documented in FYRs such as this
one. In addition, FYRs identify issues found during the review, if any, and document recommendations
to address them.

The Missouri Department of Natural Resources (MoDNR) is the lead agency; however, the U.S.
Environmental Protection Agency is preparing this FYR pursuant to the Comprehensive Environmental
Response, Compensation, and Liability Act Section 121, consistent with the National Oil and Hazardous
Substances Pollution Contingency Plan (NCP 40 CFR Section 300.430(f)(4)(ii)), and considering EPA
policy.

This is the third FYR for the Newton County Wells Superfund site (NCWS). The approval of the second
FYR, signed on April 4, 2019, was the triggering action for this policy review. The third FYR is being
conducted as a matter of policy where hazardous substances, pollutants or contaminants on site
remain above levels that allow for unlimited use and unrestricted exposure (UU/UE). The site consists
of one operable unit (OU1) and is the subject of this FYR report.

David Wennerstrom, EPA Region 7 Remedial Project Manager, led the NCWS FYR. Participants included
Catherine Chiccine, EPA counsel; Jessica Kidwell, EPA Hydrologist; Elizabeth Cole, EPA Human Health
Risk Assessor; Keke Gibb, EPA Ecological Risk Assessor; Nicolas Graddy, MoDNR Remedial Project
Manager; Bryce Bobbitt, MoDNR Unit Chief; and Evan Bryant, Environmental Program Specialist with
MDHSS. FAG Bearings, the site owner/operator, was notified of the initiation of the FYR. This review
began on May 1, 2023.

Site Background

The NCWS is in northern Newton County, Missouri. The site originates at the FAG Bearings facility,
which is located at 3900 South Rangeline Road in Joplin, Missouri. The approximate legal description
for the site includes the Sl/2 Section 19, Sections 30 and 31T27N, R32W. The geographic coordinates
to a central point on the FAG Bearings property are 37° 2' 46.108" north latitude and 94° 28' 5.016"
west longitude. The site extends southward through the neighborhoods of Silver Creek and Saginaw, to
the Thurman and Shoal Creek bottoms. The site includes the FAG Bearings property and all
groundwater, contaminated with trichloroethene (TCE) and its degradation products, extending south
from the FAG Bearings property to the Shoal Creek bottoms (See Appendix B, Site Boundary Map). The
total area impacted by the site encompasses approximately 2.5 square miles. Land use to the north of
the site is mainly businesses, including motels and restaurants. Land use to the south is primarily
residential with some scattered retail businesses. Future land use at and around the site is not
anticipated to change.

FAG Bearings has operated a ball bearing manufacturing plant at the site since approximately 1971. As
part of the manufacturing of balls for the bearings, FAG Bearings employed a TCE vapor degreasing
system to remove impurities. The degreasing system was operated from approximately 1972 to 1982,
when the balls were purchased from an outside supplier. In 1983, FAG Bearings decided to use the

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supply and return lines of the former TCE degreaser system as part of a wastewater system. During the
refitting of the piping, a clear liquid was observed spilling into a utility trench. It is suspected the fluid
was residual TCE from the former TCE degreaser system.

The site was initially discovered in April 1991 by the Missouri Department of Health, now called the
Missouri Department of Health and Senior Services (MDHSS), as part of another site investigation
which involved private well sampling. Residents in the neighborhoods of Silver Creek and Saginaw used
private domestic wells that utilized groundwater underlying the site. TCE and cis-l,2-dichloroethene
(cis-DCE) were detected in these wells at concentrations that exceeded the Maximum Contaminant
Levels (MCLs) established by the EPA.

FIVE-YEAR REVIEW SUMMARY FORM

Site Name: Newton County Wells

EPA ID:

MOD985798339

Region: 7

State: MO

City/County: Joplin/Jasper

NPL Status: Final

Multiple OUs?

No

Has the site achieved construction completion?

Yes

Lead agency: State

[If "Other Federal Agency", enter Agency name]:

Author name (Federal or State Project Manager): David Wennerstrom

Author affiliation: EPA Region 7

Review period: 4/4/2023 - 1/5/2024

Date of site inspection: 9/26/2023

Type of review: Policy

Review number: 3

Triggering action date: 4/4/2019

Due date (five years after triggering action date): 4/4/2024

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II. RESPONSE ACTION SUMMARY

Basis for Taking Action

TCE and its respective degradation products are the Contaminants of Concern (COCs) at the site. These
contaminants are classified as volatile organic compounds (VOCs).

•	VOCs - TCE; cis-DCE; trans-l,2-dichloroethene (trans-DCE); 1,2-dichloroethane; vinyl chloride
(VC).

Impacted media at the site include surface and subsurface soils at the facility, groundwater at the
facility which extends south through the neighborhoods of Silver Creek and Saginaw, and surface water
from seeps and springs. Exposure to COCs and associated risks were identified for the following media:

•	Soils - Unacceptable risks to human health due to potential direct exposure to contamination in
the shallow soils in the utility trench areas.

•	Groundwater - Unacceptable risks to human health due to the potential potable uses of the
contaminated groundwater, and potential ecological impacts resulting from uncontrolled
discharge from the Mississippian Aquifer to surface streams.

•	Surface water - Potential ecological effects associated with contaminated water discharged
through seeps and springs from the Mississippian Aquifer.

Response Actions

Response activities for the site include the following:

•	In the fall of 1991, well sampling indicated that homes located directly south of the FAG
Bearings property contained high concentrations of TCE. In response, bottled water was made
available to residents with contaminated wells as an interim action under an EPA initiated Time-
Critical Removal Action (TCRA) until connection to public water supply could be completed.

•	In January 1992, the residents of Silver Creek contracted with Missouri American Water
Company to provide a public water supply to the village.

•	In July 1992, the EPA included the residents of Saginaw in the bottled water TCRA.

•	In July 1993, the MoDNR secured funding to extend the public drinking water system to
residents in Saginaw.

•	In July 1994, public water systems were completed and included residents in the
neighborhoods of Silver Creek and Saginaw.

•	Between May 1995 and February 1996, Black and Veatch conducted a Phase I and Phase II
Remedial Investigation (Rl) for the MoDNR.

•	In December 1998, under an Abatement Order on Consent (AOC), the MoDNR agreed to allow
FAG Bearings to conduct a Rl of its property with MoDNR oversight, which identified the former
vapor degreaser pipeline utility trench as the TCE source area.

•	In July 2000, the EPA completed the National Priorities List (NPL) listing of the site.

•	In October 2000, the MoDNR and FAG Bearings entered into an AOC to conduct a Remedial
Investigation/Feasibility Study (RI/FS).

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•	In the spring of 2002, FAG Bearings initiated removal actions with the MoDNR oversight to
address the principal threat waste of TCE contaminated soils in the utility trench. In-situ
chemical oxidation (ISCO) was used to destroy the TCE contamination. Soil excavation was
conducted in other areas of the FAG Bearings property to remove impacted soils, which were
not a major contributor to the sources of aquifer contamination.

•	In June 2003, FAG Bearings completed removal actions at the site, including soil removal and
chemical oxidant injections in the source utility trench area.

•	The Record of Decision (ROD) for the site was finalized in September 2004.

Remedial Action Objectives

The Remedial Action Objectives of the ROD consist of:

1.	Maintain and enforce current conditions and existing regional regulatory controls that provide
protection from potential risk-producing exposure to the TCE and TCE degradation product
impacted portions of the Mississippian Aquifer.

2.	Reduce the concentration of TCE and TCE degradation products in the uppermost groundwater
of the NCWS to concentrations that are protective of the Mississippian Aquifer as a potable
water source with respect to TCE and TCE degradation products; and

3.	Return the Mississippian Aquifer water quality at the NCWS to potable conditions, with respect
to TCE and TCE degradation products.

Remedy Components Selected in the ROD

The major components of the selected remedy include the following:

•	Monitored natural attenuation (MNA) through hydrodynamic dispersion, a process of vertical
and horizontal movement of a contaminant through porous media due to dispersion and
diffusion forces, is the primary in-situ natural attenuation process throughout the Mississippian
Aquifer. This process will reduce the volume of COCs present in both the uppermost
groundwater and the Mississippian Aquifer at the site.

•	Institutional controls (ICs) will restrict groundwater usage and prevent migration of COCs from
the uppermost groundwater to the Mississippian Aquifer. ICs for the site include:

o Special Area 2 (now referred to as Area 11) Well Construction Rules.

o Monitoring usage of the public water supply system; and

o Enforcement of prohibition on using impacted wells with subsequent connection to the
public water supply system.

•	Biodegradation is occurring in the uppermost groundwater in the immediate area of the former
TCE pipeline trench.

•	Contingency to implement ISCO to treat areas of increased COC concentration on the bedrock
surface may be utilized.

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Cleanup Levels

The cleanup levels established in the ROD are presented below in Table 2-1. The groundwater
Remedial Action Objectives (RAOs) are defined by MCLs established by the EPA.

Table 2-1: MCLs of COCs in Groundwater

MCLs for COCs in Site Groundwater

Contaminant

MCL in parts per billion (ppb)

TCE

5

1,2-Dichloroethane

5

VC

2

Cis-1,2-DCE

70

Trans-1,2-DCE

100

Status of Implementation

The MoDNR and FAG Bearings signed a Consent Decree for the site in November 2006. The Remedial
Action Work Plan was approved by the MoDNR in July 2007. A groundwater monitoring system was
established to monitor water quality on the bedrock surface of the FAG Bearings property. Additional
wells were constructed within the neighborhoods of Silver Creek and Saginaw to monitor the quality of
the Mississippian Aquifer. The site achieved construction completion in April 2009. The site became
ready for reuse and redevelopment in March 2010.

IC Summary Table

Table 2-2: Summary of Planned and/or Implemented ICs

Media, engineered
controls, and areas
that do not
support UU/UE
based on current
conditions

ICs
Needed

ICs Called
for in the
Decision
Documents

Impacted
Parcel(s)

IC

Objective

Title of IC
Instrument
Implemented and
Date (or planned)

Groundwater

Yes

Yes

Silver
Creek and
Saginaw

Prohibit the
installation and use
of domestic
groundwater
supplies in impact
areas

10 CSR 23-3.090
Effective
7/27/1987
Amended
2/28/2019

ICs at the site are operating as originally planned in the ROD. The MoDNR enacted state regulation 10
CSR (Code of State Regulations) 23-3.090 as a regional Institutional Control in 1987, designating Special
Area 2 under Water Well Construction Code. This regulation restricts the installation of domestic wells

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into the contaminated portion of the Mississippian Aquifer and identifies minimum casing
requirements when drilling to the Ordovician Aquifer to prevent cross contamination between
contaminated portions of the Mississippian Aquifer and the deeper aquifers. On February 28, 2019,
revisions to 10 CSR 23-3.090 became effective. Special Area 2 is now designated as Area 11. These
changes restrict the installation of new shallow wells within impact areas. New shallow wells may be
drilled outside of an impact area, however, laboratory analysis of TCE and its degradation products are
required along with quantification of lead and cadmium. The revised rule also inhibits the mixing of the
upper and lower aquifers, therefore, sufficient casing must be installed into the deeper aquifer through
the Ozark Confining Unit. Anyone interested in installing or deepening a well in or around Area 11 is
highly encouraged to contact the Missouri Geological Survey for additional information at 800-361-
4827, as advance notice to the MoDNR is required prior to any major reconstruction of wells in Area

II.

Systems Operations/Operation & Maintenance

Operation & Maintenance (O&M) consists of inspection of the groundwater monitoring well network
during collection of samples. Groundwater monitoring occurs at the site to monitor MNA parameters
and COCs. All monitoring, data analysis and reporting expenses are funded by FAG Bearings.
Additionally, an O&M Plan for the two sub-slab depressurization systems (SSDSs) that are installed and
in operation at the FAG Bearings facility was developed in 2021. Construction of the two SSDSs
commenced in February 2019. An ISCO pilot study was commenced in fall 2023 and is expected to be
completed in spring 2024 near the former TCE pipeline trench, where increasing COC concentrations in
groundwater indicated potential continuing source contributions.

III.	PROGRESS SINCE THE LAST REVIEW

This section includes the protectiveness determinations and statements from the last FYR as well as
the recommendations from the last FYR and the status of those recommendations.

Table 3-1: Protectiveness Determinations/Statements from the 2019 FYR

ou#

Protectiveness
Determination

Protectiveness Statement







1

Short-term Protective

The remedy is currently protective of human health and the
environment because most of the contaminated soil at the site has
been addressed through excavation and ISCO injections. Residents
in areas of impacted groundwater have been offered connection to
public water supply and ICs in place restrict the installation of
domestic wells into the contaminated portions of the shallow
groundwater and the Mississippian Aquifer. To be protective long-
term, additional ISCO injections may be needed to ensure
protection of the aquifer.

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Table 3-2: Status of Recommendations from the 2019 FYR

ou#

Issue

Recommendations

Current
Status

Current Implementation
Status Description

Completion Date
(if applicable)

1

Remedy
Performance -
Potential for
rebounding in
the source area
may exist.

Continue monitoring
and evaluating TCE
trends. If increasing
trends continue or
increase, implement
the contingency plan
outlined in the ROD.

Ongoing

The groundwater monitoring
program for the third FYR
period was established in the
Second Amended Remedial
Action Work Plan submitted in
February 2020 and revised in
July 2020 on behalf of FAG
Bearings, LLC. TCE data were
presented in subsequent
annual reports (Ramboll, 2021,
2022). Four monitoring wells
south of the former TCE
transfer pipeline trench are
without trend or increasing.
Concentrations of cis-l,2-DCE
and vinyl chloride also are
increasing in some wells. An
ISCO pilot study was conducted
in this area in fall 2023 and
continuing through spring of
2024.

Groundwater sampling is
anticipated to continue during
the next reporting period.

Ongoing

1

Monitoring -
EPA's approach
for evaluating
the MNA has
been revised
since the original
evaluation at the
site.

Conduct an analytical
evaluation of MNA
parameters in the
trench area. If MNA
parameters do not
appear to be occuring
near the former
trench, and/or if a
significant decreasing
trend in TCE levels is
not observed in the
Mississippian Aquifer,
consider the
implementation of
ISCO injections.

Ongoing

The MNA program for the third
FYR period was established in
the Second Amended Remedial
Action Work Plan submitted in
February 2020 and revised in
July 2020 on behalf of FAG
Bearings, LLC. Evaluation was
provided in subsequent annual
reports (Ramboll, 2021, 2022).
An ISCO pilot study was
conducted in fall 2023 and
continuing through spring 2024
near the former TCE pipeline
trench, where increasing COC
concentrations in
groundwater indicated
potential continuing source
contributions.

Ongoing

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IV. FIVE-YEAR REVIEW PROCESS

Community Notification. Involvement & Site Interviews

A public notice was made available through the Joplin Globe as a display advertisement on June 24,
2023. The Joplin Globe is a local newspaper that serves the Joplin area. The public notice stated there
was a FYR and invited the public to submit any comments to the MoDNR and EPA. The results of the
review and the report will be made available at the site information repository located at the MoDNR,
Hazardous Waste Program, 1730 E. Elm Street, Jefferson City, Missouri, 65101. The report will also be
made available through the EPA's internet-based information repository which can be accessed by the
public through the following website:

https://www.epa.gov/superfund/search-superfund-five-year-reviews

During the FYR process, interviews were conducted to document any perceived problems or successes
with the remedy that has been implemented to date. On September 26, 2023, while at the site, Mr.
Bobbitt interviewed Mr. Doug Burge of Ramboll Environ, the environmental consulting firm working on
behalf of FAG Bearings. During the interview, Mr. Bobbitt and Mr. Burge discussed the remedy's
continuing performance at the site and how monitoring data continues to show most COC levels to be
diminishing and/or remaining stable and did not note any issues or concerns which may affect the
protectiveness of the remedy. Requests for interviews through an interview questionnaire form were
submitted to FAG Bearings as the property owner and the MoDNR. No public interviewees were
identified. Doug Burge of Ramboll Environ and Nicolas Graddy of MoDNR submitted responses. A copy
of the Interview Records is provided in Appendix C.

September 27-28, 2023, MoDNR representatives conducted door to door community interviews in the
neighborhoods of Silver Creek and Saginaw, which is located downgradient of the FAG Bearings facility.
Generally, the residents knew of the Superfund site. Furthermore, the MoDNR held a community
availability session on October 5, 2023, in Silver Creek neighborhood. A total of 16 community
members were in attendance. The goal of the availability session was to address any uncertainty or
questions that community members had with the site. Generally, the community members expressed
an interest in vapor intrusion sampling of their homes and wanted to know if there was a new
contaminant release or continued containment release from the FAG Bearings facility.

Data Review

The FYR evaluated available data to assess the effectiveness and progress of the MNA remedy in
achieving the RAOs outlined in the 2004 ROD and maintaining protectiveness. Sampling events
occurred in September 2020, May 2021, and May 2022. Because dry or low yield wells were often
encountered during the fall sampling events, the annual sampling events were moved from the fall to
the spring of each year. The associated annual reports (Ramboll, 2020, 2021, 2022) provided the
primary data reviewed.

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Sitewide Groundwater Sampling

A total of 28 wells are monitored at the site at a minimum of an annual basis and in some cases on a
semi-annual basis. Eighteen of these wells are completed in the uppermost groundwater region at the
site. The remaining 10 wells are completed in the deeper Mississippian Aquifer. Wells at the site are
sampled by new polyethylene bailers or by a site-dedicated pneumatic piston pump. In addition to the
well sampling, two surface water samples are collected. One surface sample is collected along the
eastern side of Saginaw Road, near the intersection of High Street, where it is supplied by Mississippian
Aquifer springs. The second surface sample is collected from Thurman Creek, downstream of the
Reddings Road Bridge, near the western bank in a portion of the stream channel which higher flow
occurs. The 2022 sampling event represents the 19th round of MNA sampling. Based upon regulator
comments to the RAWP and specifically issues with the fall sampling events encountering dry or low
yield wells, the annual sampling events were rescheduled from the fall, to now occur in the spring of
each year.

For uppermost groundwater:

•	Six monitoring wells are sampled adjacent to the former TCE transfer pipeline trench.
Concentrations in these wells are decreasing or without trend. No decreasing trend is noted in
the well with the highest TCE concentration (FAG-31, 726 |ag/L TCE in 2022).

•	Five monitoring wells are sampled south of the former TCE transfer pipeline trench. Except at
FAG-34 (decreasing, 582 |ag/L TCE in 2022), TCE concentrations are without trend or increasing
(31.7 to 537 |ag/L TCE in 2022). Concentrations of c/'s-1,2-DCE and vinyl chloride also are
increasing in some wells.

•	Four monitoring wells are sampled southwest of the facility buildings, near the southern facility
property line. While concentrations are generally decreasing in these wells, the well with the
highest concentration is without trend (FAG-50, 2,050 |ag/L TCE in 2022).

•	Of the two downgradient monitoring wells screened in uppermost groundwater, one well is
without trend (Rl-M Wl, 57.3 |ag/L TCE in 2022) and the other is non-detect (Rl-M W2, <1 |ag/L
TCE in 2022).

While concentrations of TCE and its degradation products are decreasing in some wells, other
monitoring wells show no decrease in elevated concentrations or increasing concentrations of TCE and
its degradation products. Except for the non-detect result, all TCE concentrations in uppermost
groundwater exceeded the vapor intrusion screening level for groundwater.

For the Mississippian Aquifer:

•	Five monitoring wells are sampled on the facility property. While TCE concentrations are
decreasing in at least one well near the southern property line (FAG-11, 2.3 |ag/L TCE in 2022), a
well directly south of the former TCE transfer pipeline trench shows recently increasing
concentrations of TCE and vinyl chloride at concentrations orders of magnitude above their
respective MCL (FAG-AW4, 1,160 |ag/L TCE and 28.5 |ag/L vinyl chloride in 2022).

•	Five monitoring wells are sampled downgradient of the facility property toward the
neighborhoods of Silver Creek and Saginaw. TCE concentrations in these wells range from 1.6
Hg/L to 64.2 |ag/L, with three of these wells continuing to exhibit TCE concentrations above the

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MCL.

Again, while concentrations of TCE and its degradation products are decreasing in some wells, other
monitoring wells show no decrease in elevated concentrations or increasing concentrations of TCE and
its degradation products. That the most elevated groundwater concentrations are just south of the
former TCE transfer pipeline trench suggests continued contributions from uppermost groundwater in
this source area.

MNA water quality parameters are collected for the uppermost and Mississippian aquifers. These
parameters include pH, temperature, specific conductivity, oxidation reduction potential and dissolved
oxygen. Data collected from the upper aquifer is supportive of ongoing natural attenuation processes,
primarily biodegradation adjacent to and south of the former TCE pipeline trench. The natural
attenuation process in the deeper Mississippian Aquifer appears to be from hydrodynamic dispersion.

The two surface water samples were collected a little over 1.5 miles south of the FAG Bearings facility.
TCE was the only VOC detected in the surface water samples. During the 2022 sampling event, TCE was
measured below the laboratory reporting limit (RL) for this compound (1.0 |ag/L) in RW-341A (0.60 J
l-ig/L) and SW-01 (0.92 J |ag/L), which is below levels of surface water quality concern and generally
consistent with recent measurements.

Residential Wells

In 2008, five residential wells were abandoned along a portion of Moorhead Drive, which is located
south-southwest of the site. These wells were identified as potential conduits to the Mississippian
Aquifer. The wells abandoned included residential wells RW-15 (3103 Moorhead), RW-16 (3207
Moorhead), RW-18 (3215 Moorhead), RW-19 (3219 Moorhead) and RW-20 (3223 Moorhead).

Five other residential wells were reviewed but ultimately were not selected to be abandoned. These
wells include: RW-14 (3101 Moorhead), RW-17 (3211 Moorhead), RW-24 (3016 Moorhead), RW-31
(3220 Moorhead) and RW-32 (3232 Moorhead). Owners of these five wells should be contacted
regularly to inquire upon their status and the potential for sampling and/or abandonment.

Vapor Intrusion

The first FYR report, dated April 2014, recommended further evaluation of the vapor intrusion
pathway. This recommendation was primarily because of revisions to procedures used to evaluate the
potential for vapor intrusion since completion of the 2004 baseline risk assessment for the NCWS that
included an assessment of the vapor intrusion pathway. In 2016 and 2017, a vapor intrusion pathway
evaluation was completed. Samples were collected at FAG Bearings property buildings and seven
residences near the facility's southern property boundary. Indoor air data collected indicated no
exposures to site related VOCs above established Removal Action levels to occupants of the residential
or FAG Bearings facility structures. Residential crawlspace data did not exceed established Removal
Action levels; however, sub-slab data collected beneath some FAG Bearings buildings indicated
exceedances of established RSLs for site related VOCs.

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Based on these findings and Agency recommendation, in February 2019, two sub-slab vapor mitigation
systems were installed in the facility's Building A and Service Building as a pre-emptive measure. An
O&M Plan was subsequently prepared for the two sub-slab depressurization systems.

Based on continued review of annual groundwater sampling data, an evaluation of whether impacted
uppermost groundwater presents a vapor intrusion concern for buildings near the facility's southern
boundary. This action is contained in as an Issue/Recommendation in Section VI below.

Site Inspection

A site inspection was conducted for the completion of this FYR. The purpose of the inspection was to
assess the protectiveness of the remedy.

The inspection of the site was conducted on September 26, 2023. In attendance were David
Wennerstrom and Jesse Kidwell of the EPA, Bryce Bobbitt and Nicolas Graddy from MoDNR, Doug
Burge and Edward Jones from Ramboll Environ and environmental consultant for FAG Bearings, and
Karen Bozeman of FAG Bearings. Site access required visitors to check-in at the facility security gate
where a visitor badge was issued. Ms. Bozman and Mr. Burge escorted the group throughout the
facility, including the FAG Bearings' buildings with SSDS. The tour concluded with inspection of several
monitoring well locations, as well as the new detention pond.

During the site inspection no specific issues were identified impacting current or future protectiveness
of the remedy.

V. TECHNICAL ASSESSMENT

QUESTION A: Is the remedy functioning as intended by the decision documents?

Question A Summary:

Institutional and engineering controls remain in place to address the first RAO. The remedy does not
appear to be meeting at least two of its RAOs. Concentrations of TCE and TCE degradation products in
the uppermost groundwater are not being significantly reduced and appear to be contributing to
increasing concentrations in the Mississippian Aquifer. Similarly, concentrations of TCE and TCE
degradation products in the Mississippian aquifer persist at concentrations significantly above the MCL
and are not being significantly reduced throughout the site. Concentrations in a well just south of the
former TCE transfer trench are increasing at already elevated TCE concentrations, such that MNA alone
is unlikely to return the Mississippian Aquifer water quality at site to potable conditions in a timely
manner. However, in general consistency with the contingency measure in the 2004 ROD, FAG
Bearings is currently conducting a pilot test for focused in-situ treatment of uppermost groundwater.

Because the RAOs reflect understanding of current risk at the time the 2004 ROD was written,
additional considerations are necessary to ensure the remedy remains protective. These include
reevaluation of pre-existing private well use and vapor intrusion potential and evaluating emerging
contaminants of concern.

11


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Remedial Action Performance

As discussed in the data review, although evidence of MNA is observed in uppermost groundwater at
the site, MNA appears insufficient to effectively reduce, within a reasonable amount of time,
concentrations of TCE and TCE degradation products in the uppermost groundwater of the NCWS to
concentrations that are protective of the Mississippian Aquifer as a potable water source with respect
to TCE and TCE degradation products.

Dispersion is the primary MNA mechanism in the Mississippian Aquifer and, based on the data review,
appears similarly insufficient to return the Mississippian Aquifer water quality at the site to potable
conditions with respect to TCE and TCE degradation products within a reasonable timeframe.

Per the 2004 ROD, if a significant decreasing trend in TCE levels is not observed in the Mississippian
Aquifer during the first five years of sampling, a contingency remedy to revert to ISCO may be
implemented. Based on the above observations and the contingency measure provided by the ROD,
FAG Bearings conducted a pilot test for focused in-situ treatment of uppermost groundwater within a
bedrock valley feature south of the pipeline trench and southwest of the facility buildings.

System Operations/O&M

During the FYR site inspection, the monitoring well network appeared reasonably well maintained,
although some flush-mount protective covers needed to be bolted down.

In 2019, FAG Bearings constructed two SSDSs for facility buildings. An O&M Plan for the SSDSs was
developed in 2021. The SSDSs were observed to be operational during the inspection.

Implementation of Institutional Controls and Other Measures

The facility engineering controls and regional ICs identified in the remedy remain intact. During the FYR
site inspection, the facility is surrounded by a well-maintained fence with a guard staffing the main
entrance.

Recently, the MoDNR updated the Missouri Water Well Construction Code, 10 CSR 23-3.090, and
Special Area 2 is now Area 11. Newton County, along with Jasper County, received this designation
restricting certain types of well construction because of contamination of portions of the "upper
aquifer" with lead, cadmium, TCE and TCE degradation products. The "upper aquifer," as defined in the
rules, "includes all formations constituting the Springfield Plateau Aquifer in the southwestern portions
of the State." Both the uppermost groundwater and the Mississippian Aquifer occur in those
designated formations. Therefore, the "upper aquifer" as defined in 10 CSR 23-3.100(5) includes both
the uppermost groundwater and the Mississippian aquifer as discussed herein.

The controls identified in the ROD do not protect against vapor intrusion. As noted above, in 2019, two
sub-slab vapor mitigation systems were installed in the facility's Building A and Service Building as a
pre-emptive measure. As an Issue and Recommendation in section VI of this report, additional vapor
intrusion sampling is recommended to revisit the potential for impact to residential buildings.

12


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QUESTION B: Are the exposure assumptions, toxicity data, cleanup levels and Remedial Action
Objectives fRAOs) used at the time of the remedy selection still valid?

Question B Summary:

Human Health Risk

The exposure assumptions, toxicity data and cleanup levels used at the time of remedy remain valid.
The groundwater cleanup levels are MCLs that have not changed since the implementation of the ROD
(see Table below).

In the previous FYR period, a vapor intrusion evaluation was conducted in which TCE and VC RMLs
were exceeded in sub-slab soil gas underneath the site facility. Vapor mitigation systems were installed
in two areas. In the offsite investigation, although COCs were detected in the indoor air and crawlspace
samples, there were no exceedances of Residential Vapor Intrusion Management Levels (Cancer Risk
lxlO"4 and HQ=1). After four quarters of consecutive air monitoring, it was concluded that continued
air monitoring at the site was not necessary. However, the uppermost groundwater plume persists and
is increasing in concentrations in some areas, and sub-slab vapors may accumulate over time. As such,
it is recommended that risk associated with potential residential vapor intrusion be re-evaluated.

The results in the 2022 Annual Remedial Action Report indicate COCs continue to be detected well
above groundwater cleanup levels. As indicated in the table below, the cleanup goals specified in the
ROD, although all values are MCLs, exceed the excess cumulative cancer risk range (lxlO 4 to lxlO 6)
specified by the NCP. For the remedy to remain protective of human health, ICs must continue to
restrict use of contaminated groundwater as a potable water source, engineering controls (onsite
vapor mitigations systems) must operate as intended, the potential residential vapor intrusion
pathway must be re-investigated and mitigated if necessary, and for residential non-potable usage,
COC concentration trends in the residential area Mississippian aquifer wells must not increase
significantly.

Groundwater Cleanup Levels

Contaminant

MCL in parts per
billion (ppb)

Cleanup Level
Carcinogenic
Risk*

TCE

5

l.OxlO"5

cis- 1,2-DCE

70

-

trans- 1,2-DCE

100

-

1,2-DCA

5

2.9xl0"5

VC

2

1.lxlO"4

Excess Cumulative
Carcinogenic Risk*

-

1.5xl0"4

* Carcinogenic Risk is calculated based on EPA November 2023 RSL Tables
Ecological Risk

13


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The only complete ecological exposure pathway is groundwater interaction with surface water in
spring water. TCE and its degradation products were found to be well below ecological screening levels
in both spring surface water samples (SW-01 and RW-341A). Therefore, the current remedy remains
protective of ecological risks.

Changes in Standards and TBCs

There have been no modifications to the MCLs since the ROD was issued. TBCs were not used in
selecting cleanup levels for the site. We are not aware of any newly promulgated standards that call
into question the protectiveness of the remedy.

Changes in Toxicity and Other Contaminant Characteristics

As discussed in the 2014 and 2019 FYRs, toxicity factors for several site contaminants, including TCE,
have changed since completion of the risk assessment in 2004. In November 2022, EPA implemented
new Inhalation Reference Concentrations (RfCs) for cis-l,2-DCE and trans-l,2-DCE. However, these
updates do not significantly alter the conclusions of the risk assessment, nor the protectiveness of the
remedy. The cleanup goals are MCLs which have not changed.

For vapor intrusion, at the most recent air monitoring event in the 2017 Second Quarter, it was
reported that there were no crawl space/indoor air screening levels available for cis-l,2-DCE and trans-
1,2-DCE. There are presently VISLs available for these COCs with the EPA RSL November 2023 update.
However, the data from the four quarters of offsite VI sampling were well below current EPA Region 7
VISLs for both isomers of DCE.

There are no other known changes to contaminant characteristics in this FYR period that impact the
protectiveness of the remedy.

Changes in Risk Assessment Methods

As discussed in the previous FYRs, there have been changes in the methodology used to assess
inhalation pathway exposure and risk since the completion of the baseline risk assessment and
addendum in 2004 and some minor updates to standard default exposure factors. These changes do
not significantly impact the conclusions of the risk assessment or the protectiveness of the remedy.

Changes in Exposure Pathways

Land use has not changed and there are no known changes in potential land use onsite.

Since the risk assessment and addendum in 2004, there have been updates in the evaluation of VI and
more conservative VISLs, as discussed in the 2014 and 2019 FYRs. These changes led to the
identification of subsurface vapor intrusion as a potential exposure pathway warranting further
evaluation. As discussed previously, vapor mitigation systems were voluntarily installed in the FAG
bearings buildings in response to these investigations. Although no COC concentration exceeded a level
of concern in offsite residences, the uppermost groundwater plume persists and is increasing in
concentrations in some areas, and sub-slab vapors may accumulate over time. COCs continue to be

14


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detected in both the Uppermost and Mississippian Aquifer well above cleanup levels, as documented
in the 2022 Annual Remedial Action Report, and groundwater VISLs.

The available data do not indicate any new contaminants. However, because of the site history as a ball
bearing manufacturing plant that had utilized a vapor degreasing system, the potential for associated
PFAS contamination is indicated (Gliige, J. et al, 2020; Gaines, 2022). Because of this and the potential
for the planned contingency measure (ISCO) to transform precursor PFAS into daughter PFAS with
established RSLs, sampling and analysis for PFAS is recommended.

There are no other known unanticipated byproducts of the remedy.

Expected Progress Towards Meeting RAOs

As noted above, contingency measures are needed to make effective progress toward the RAOs.
Additional actions are also necessary to ensure remedy protectiveness. These include revisiting pre-
existing private well use and vapor intrusion and evaluating emerging contaminants of concern.

QUESTION C: Has any other information come to light that could call into question the
protectiveness of the remedy?

No significant impacts from climate change are anticipated within the life of the remedy; however,
changes in groundwater level could alter the plume depth or ability of wells to produce water.

VI. ISSUES/RECOMMENDATIONS

Issues and Recommendations Identified in the Five-Year Review:

OU(s): 1

Issue Category: Remedy Performance

Issue: With MNA being insufficient in addressing contamination in the
upper aquifer, additional vapor intrusion sampling is recommended for
residential properties south of the FAG Bearings property. Re-evaluate
risk associated with potential residential vapor intrusion following the
completion of additional vapor intrusion sampling.

Recommendation: If additional vapor intrusion sampling activities
indicate a significant potential for vapor intrusion to the residences
identified, address elevated risk then step out vapor intrusion sampling
and/or collect additional lines of evidence to better assess current vapor
intrusion risks and sampling needs offsite, such as improved delineation
of the uppermost groundwater plume and soil gas sampling.

Affect Current
Protectiveness

Affect Future
Protectiveness

Party
Responsible

Oversight Party

Milestone Date

No

Yes

PRP

EPA/State

12/31/2025

15


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OTHER FINDINGS

In addition, the following recommendations were identified during the FYR and may improve
performance of the remedy, improve management of operations and maintenance or accelerate site
closeout, but do not affect current and/or future protectiveness:

•	In 2008, five residential wells were reviewed but not abandoned. These wells include: RW-14
(3101 Moorhead), RW-17 (3211 Moorhead), RW-24 (3016 Moorhead), RW-31 (3220 Moorhead)
and RW-32 (3232 Moorhead). Owners of these five wells should be contacted to inquire upon
their status. If possible, abandon these wells and/or sample them to improve understanding of
risk and impact.

•	Based on historical site activities and proposed treatment measures, groundwater sampling
should be conducted for PFAS.

VII. PROTECTIVENESS STATEMENT

Protectiveness Statement(s)

Operable Unit:

Protectiveness Determination:

Planned Addendum

OU1

Short-term Protective

Completion Date:





NA

Protectiveness Statement: The remedy at Newton County Wells is protective of human health
and the Environment in the short term. Most of the contaminated soil at the site has been
addressed through excavation and ISCO injections. ICs are in place to restrict the installation
of domestic wells into the contaminated portions of the shallow groundwater and the
Mississippian Aquifer. To be protective in the long-term, vapor intrusion sampling must be
conducted at the downgradient residential properties.

VIII. NEXT REVIEW

The next FYR for the Newton County Wells Superfund site is required five years from the completion
date of this review.

16


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APPENDIX A - REFERENCE LIST

Environ, 2004, Final Report of Remedial Investigation, Newton County Wells Site, Silver Creek and
Saginaw, Missouri. March.

Gaines, L.G.T., 2022, Historical and current usage of per- and polyfluoroalkyl substances (PFAS), A
literature review: American Journal of Industrial Medicine, May 25.
https://onlinelibrarv.wiley.com/doi/full/10.1002/aiim.23362

Gliige, J. et a I, 2020, An overview of the uses of per- and polyfluoroalkyl substances (PFAS):
Environmental Science, Processes & Impacts, 22:2345-2373, October 30.
https://pubs.rsc.org/en/content/articlelanding/2020/em/d0em00291g

Michigan Department of Environmental Quality, 2018, Recommended PFAS Screening & Evaluation
Procedure for Industrial Pretreatment Programs (IPPs). https://www.michigan.gov/-
/media/Project/Websites/egle/Documents/Programs/WRD/IPP/PFAS-Guidance-Screening-
Evaluation.pdf?rev=0504d567eebl4be5bdee513e8a51ffce

Missouri Department of Natural Resources, 2004, Record of Decision, Newton County Wells Site,
Jefferson City, Missouri. EPA/ROD/R07-04/655.

Missouri Department of Natural Resources, 2014, Five-Year Review Report for Newton County Wells
Superfund Site Newton County, Missouri.

Missouri Department of Natural Resources, 2019, Second Five-Year Review Report for Newton County
Wells Superfund Site Newton County, Missouri.

Ramboll Environ, 2017, Letter Re: Summary of Second Quarter 2017 Air Monitoring Event Newton
County Wells Site - Joplin, Missouri. July.

Ramboll US Consulting, Inc., 2021, Annual Report (Revision 1) Remedial Action - Newton County Wells
Site Silver Creek and Saginaw. December.

Ramboll US Consulting, Inc., 2022, Annual Report Remedial Action - Newton County Wells Site Silver
Creek and Saginaw. December.

U.S. Environmental Protection Agency, 1986, Guidelines for Ground-Water Classification under the EPA
Ground-water Protection Strategy. November.

U.S. Environmental Protection Agency, 1999, Use of Monitored Natural Attenuation at Superfund,
RCRA Corrective Action and Underground Storage Tank Sites: Office of Solid Waste and
Emergency Response, OSWER Directive 9200.4-17P, April 21.
https://www.epa.gov/sites/default/files/2014-02/documents/d9200.4-17.pdf


-------
U.S. Environmental Protection Agency, 2001, Comprehensive Five-Year Review Guidance: Office of Solid
Waste and Emergency Response (5204G), EPA 540-R-01-007, OSWER No. 9355.7-03B-P, June.
https://semspub.epa.gov/work/HQ/128607.pdf

U.S. Environmental Protection Agency, 2011, Recommended Evaluation of Institutional Controls,
Supplement to the Comprehensive Five-Year Review Guidance: Office of Solid Waste and
Emergency Response, OSWER Directive 9355.7-18, September 13.
https://semspub.epa.gov/work/HQ/175441.pdf

U.S. Environmental Protection Agency, 2012, Assessing Protectiveness at Sites for Vapor Intrusion,
Supplement to the Comprehensive Five-Year Review Guidance: Office of Solid Waste and
Emergency Response, OSWER Directive 9200.2-84, December 3.
https://semspub.epa.gov/work/HQ/176385.pdf

U.S. Environmental Protection Agency, 2013, Guidance for Evaluating Completion of Groundwater

Restoration Remedial Actions: Office of Solid Waste and Emergency Response, OSWER Directive
9355.0-129, November 25. https://semspub.epa.gov/work/HQ/175206.pdf

U.S. Environmental Protection Agency, 2014, Recommended Approach for Evaluating Completion of
Groundwater Restoration Remedial Actions at a Groundwater Monitoring Well: Office of Solid
Waste and Emergency Response, OSWER Directive 9283.1-44, August 11.
https://semspub.epa.gov/work/HQ/173689.pdf

U.S. Environmental Protection Agency, 2015, Groundwater Technical Considerations During the Five-
Year Review Process: Groundwater Forum Issue Paper, EPA-542-F-15-010, April.
https://www.epa.gov/sites/default/files/2015-06/documents/gwf fyr issue paper.pdf

U.S. Environmental Protection Agency, 2014, Human Health Evaluation Manual. Supplemental

Guidance: Update of Standard Default Exposure Factors. OSWER 9200.1-120. Office of Solid
Wast and Emergency Response, Washington, D. C.

U.S. Environmental Protection Agency, 2023, Regional Screening Levels, May.
https://www.epa.gov/risk/regional-screening-levels-rsls

U.S. Environmental Protection Agency, 2023, Regional Screening Levels (RSLs) - User's Guide.
www.epa.gov/risk/regional-screening-levels-rsls


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APPENDIX B - MAPS & FIGURES


-------
QONTOuft =KT«*MAL LiJ «Ct

vs	

SITE BOUMDAfty BASED ON
1 11 "''9 REMEDIAL 3NVESTIGATIOM

boi^mo:.

iJtS '--rvu-, ?.S M.-T--UM Sana Ji>v^k heat:. Kt»»o.n taipo^rMttnc i>_Ac:re*--u^«-
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ENVIRON

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I MTtf: X'JJ 1..-20LV

SITE LOCATION MAP

NEWTON COUNTY WELL SITE
VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE

1-1


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APPENDIX C - SITE INSPECTION


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v>EPA PUBLIC NOTICE

The U.S. Environmental Protection Agency (EPA) Region
7 has started the Third Five-Year Review for the Newton
County Wells Superfund Site. Five-Year Reviews are
required by the Comprehensive Environmental
Response, Compensation and Liability Act (CERCLA)
when hazardous substances remain on-site above levels
that permit unrestricted use and unlimited exposure.
Five-Year Reviews provide an opportunity to evaluate
the site remedy to determine whether it remains
protective of human health and the environment. This
Five-Year Review Report should be completed by May
2024.

Site project information is available to the public at web
repositories, including Five-Year Reviews (under Reports
and Documents). To view cleanup documents, please
visit EPA's Site Profile Page at:

www.epa.gov/superfund/newtoncountvwells (see Site
Documents & Data). If you do not have internet access,
you can view these documents online at this location:
Joplin Public Library, 1901 E 20th St., Joplin, MO 64804;
417-623-7953.

If you have questions about the site, please contact
Pamela Houston, EPA Community Involvement
Coordinator, at houston.pamelagepa.gov or 913-551-
7699.

Region 7

Iowa, Kansas,

Missouri, Nebraska
and Nine Tribal Nations

Third Five-Year Review Started
Newton County Wells Superfund Site
Joplin, Newton County, Missouri
June 2023

U.S. Environmental Protection Agency, Region 7
11201 Renner Boulevard, Lenexa, KS 66219
Toll-free: 1-800-223-0425


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INTERVIEW QUESTIONNAIRE

Site Name: Newton County Wells Superfund Site

EPA ID No.

Subject: Five-Year Review

Time:

Date:

Type:	Telephone

Location of Visit:

Visit

X Other

Incoming

Outgoing

Contact Made By

Name: David Wennerstrom

Title: Project Manager, Superfund Organization: US. EPA

Individual Contacted - Prepared by

Name: Douglas Burge

Title: Senior Manager

Organization: Ramboll

Telephone No.: 314-378-8065
E-mail Address: dbmge@ramboll.com

Street Address: 1807 Park 270 Drive, Suite 450
City, State, Zip Code: St Louis, MO 63146

Interview Questionnaire

1.	What is your overall impression of the project?

The project continues to move forward with implementing remedial actions to achieve the cleanup goals
prescribed by MDNR.

2.	Are you aware of any community concerns regarding the Site or its operation and administration?

MDNR reached out to me via e-mail in June 2023 regarding a question they received from a community member
regarding decreased flow the community member had noted in a small stream which flowed from the FAG facility
southern property boundary. I followed up with MDNR via e-mail and described that the water flow in this stream
was primarily from an NPDES permitted outfall of non-contact cooling water from the FAG facility and that recent
operational changes implemented to reduce and conserve water usage had eliminated the need for continued use
of this outfall.

3.	Are you aware of any events, incidents, or activities at the Site such as vandalism, trespassing, or emergency
response from local authorities?

In March 2023 the facility became aware of a leak in an underground pipeline used to transfer a petroleum
distillate product. An initial estimate of the volume of product which may have been released was 9,000 gallons.
Facility personnel immediately responded and reported the spill to MDNR and it was assigned Incident#
2303141705ZDH and to NRC and it was assigned report# 1362253. Subsequent investigation and remedial actions
were conducted by the facility with oversight provided by MDNR. It was determined that the release did not impact
surface water or depart the facility property.

4. Do you feel well informed about the Site's activities and progress?

Yes

5. Do you have any other comments, suggestions, or recommendations regarding this Site?

No


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INTERVIEW QUESTIONNAIRE

Site Name: Newton County Wells Superfund Site

EPA ID No.:

Subject: Five-Year Review

Time:

Date:

Type:	Telephone

Location of Visit:

Visit

X Other

Incoming

Outgoing

Contact Made By

Name: David Wennerstrom

Title: Project Manager, Superfund Organization: US. EPA

Individual Contacted - Prepared by

Name: Nicolas Graddy

Title: Remedial Project Manager

Organization: MoDNR

Telephone No.: (573)751-3026

E-mail Address: Nicolas.Graddy@dnr.mo.gov

Street Address: 1730 E Elm St.

City, State, Zip Code: Jefferson City. MO, 65101

Interview Questionnaire

1.	What is your overall impression of the project?

The project is progressing as intended by Schaeffler. Monitoring of groundwater wells continues. TCE levels and
associated daughter products are decreasing in many wells, but some wells remain stable to increasing. There are
also some wells that have significant decreases in TCE levels based on percentage, but the levels are still well over
the MCL. FAG Bearings/Schaeffler are currently completing a pilot study for further ISCO injections, in the hopes
that it will decrease TCE levels further at an accelerated rate. If the ISCO injections do not prove to significantly
lower the levels of TCE and its associated daughter products within a reasonable timeframe, then a new remedy
may need to be formed for the site.

Additionally, there needs to be another study for vapor intrusion sampling in residential homes that sit within the
TCE groundwater plume. There needs to be more data to confirm the results from the last study with vapor
intrusion in residential homes.

2.	Are you aware of any community concerns regarding the Site or its operation and administration?

Yes, the community is concerned with the amount of time it is taking for the remediation of the TCE plume.
Community members who still have wells would like to use their wells again for potable purposes. Also, the
community is concerned with possible Vapor Intrusion of TCE into their homes. The community would like to see
active VI sampling completed in the residential neighborhoods of Silver Creek and Saginaw. With the recent FYR
community interviews for the community involvement plan, many residents would like to be more informed on the
progress of the site.

3.	Are you aware of any events, incidents, or activities at the Site such as vandalism, trespassing, or emergency
response from local authorities?

No, I am unaware of any events, incidents, or activities related to the Site such as vandalism, trespassing, or
emergency response.

4.	Do you feel well informed about the Site's activities and progress?

Yes, I feel well informed about the Site's activities and progress.

5.	Do you have any other comments, suggestions, or recommendations regarding this Site?

I have no further comments at this time.


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L SITE INFORMATION

Site name: Newton County Wells

Date of inspection: September 26,2023

Location and Region: Joplin, MO / Region VII

EPA ID: MOD985798339

Agency, office, or company leading the five-year



Weather/temperature: Clear, Sunny, 70's

review: Missouri DNR





Remedy Includes: (Check all that apply)





~ Landfill cover/containment

X Monitored natural attenuation

IX] Access controls

~

Groundwater containment

X Institutional controls

~

Vertical barrier walls

~ Groundwater pump and treatment





~ Surface water collection and treatment





~ Other







Attachments: ~ Inspection team roster attached



~ Site map attached

II. INTERVIEWS (Check all that apply)

1. O&M site manager DougBurge



Senior Manager 09/26/2023

Name



Title Date

Interviewed X at site ~ at office ~ by phone

Phone no.

Problems, suggestions; ~ Report attached





In person interview conducted by MoDNR during Site Inspection. No issues were noted with Mr. Burge.

Discussed Fall 2023 ISCO event to be commenced in another month.

2. O&M staff

Name



Title Date

Interviewed ~ at site ~ at office ~ by phone

Phone no.

Problems, suggestions; ~ Report attached










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3. Local regulatory authorities and response agencies (i.e., State and Tribal offices, emergency response
office, police department, office of public health or environmental health, zoning office, recorder of
deeds, or other city and county offices, etc.) Fill in all that apply.

Agency	

Contact	 	 	 	

Name	Title	Date Phone no.

Problems; suggestions; ~ Report attached 	

Agency	

Contact	 	 	 	

Name	Title	Date Phone no.

Problems; suggestions; ~ Report attached 	

Agency	

Contact	 	 	 	

Name	Title	Date Phone no.

Problems; suggestions; ~ Report attached 	

Agency	

Contact	 	 	 	

Name	Title	Date Phone no.

Problems; suggestions; ~ Report attached 	

4. Other interviews (optional) ~ Report attached.


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m. ON-SITE DOCUMENTS & RECORDS VERIFIED (Check all that apply)

1. O&M Documents

~	O&M manual

~	As-built drawings

~	Maintenance logs
Remarks

~	Readily available

~	Readily available

~	Readily available

~	Up to date IX] N/A

~	Up to date IEI N/A

~	Up to date ~ N/A

2. Site-Specific Health and Safety Plan	~ Readily available ~ Up to date X N/A

X Contingency plan/emergency response plan ~ Readily available ~ Up to date ~ N/A
Remarks

O&M and OSHA Training Records

Remarks

Readily available

~ Up to date ~ N/A

Permits and Service Agreements

~	Air discharge permit

~	Effluent discharge

~	Waste disposal, POTW

~	Other permits	

Remarks

~	Readily available

~	Readily available

~	Readily available

~	Readily available

~	Up to date

~	Up to date

~	Up to date

~	Up to date

N/A
N/A
N/A
N/A

5. Gas Generation Records

Remarks

~ Readily available ~ Up to date

N/A

6. Settlement Monument Records

Remarks

~ Readily available ~ Up to date

N/A

7. Groundwater Monitoring Records

Remarks

~ Readily available ~ Up to date

N/A

Leachate Extraction Records

Remarks

~ Readily available ~ Up to date X N/A

9. Discharge Compliance Records

~	Air

~	Water (effluent)

Remarks

~	Readily available

~	Readily available

~	Up to date

~	Up to date

N/A
N/A

10. Daily Access/Security Logs

Remarks

~ Readily available ~ Up to date

N/A


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IV. O&M COSTS

1. O&M Organization

~	State in-house

~	PRP in-house

~	Federal Facility in-house

~	Other

2. O&M Cost Records

~	Readily available ~ Up to date

~	Funding mechanism/agreement in place

Original O&M cost estimate	~ Breakdown attached

Total annual cost by year for review period if available

From	To	~ Breakdown attached



Date



Date

Total cost



From



To





~ Breakdown attached



Date



Date

Total cost



From



To





~ Breakdown attached



Date



Date

Total cost



From



To





~ Breakdown attached



Date



Date

Total cost



From



To





~ Breakdown attached



Date



Date

Total cost



3. Unanticipated or Unusually High O&M Costs During Review Period

Describe costs and reasons:

None noted

V. ACCESS AND INSTITUTIONAL CONTROLS ~ Applicable ~ N/A

A. Fencing

1. Fencing damaged	~ Location shown on site map X Gates secured ~ N/A

Remarks

B. Other Access Restrictions

1. Signs and other security measures	~ Location shown on site map ~ N/A

Remarks: Security gate with manned guards at the entrance. Guards have authorized access log of
personnel

~	Contractor for State
X Contractor for PRP

~	Contractor for Federal Facility


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C. Institutional Controls (ICs)

1. Implementation and enforcement

Site conditions imply ICs not properly implemented	~ Yes ~ No ~ N/A

Site conditions imply ICs not being fully enforced	~ Yes ~ No ~ N/A

Type of monitoring (e.g., self-reporting, drive by) :Drive-by

Frequency: Annually

Responsible party/agency: MoDNR

Contact: Nicolas Graddy

Reporting is up-to-date

~ Yes

El No

~ N/A

Reports are verified by the lead agency

~ Yes

E No

~ N/A

Specific requirements in deed or decision documents have been met

IEI Yes

~ No

~ N/A

Violations have been reported

~ Yes

E No

~ N/A

Other problems or suggestions: ~ Report attached







2. Adequacy	X ICs are adequate ~ ICs are inadequate	~ N/A

Remarks

D. General

1. Vandalism/trespassing ~ Location shown on site map X No vandalism evident
Remarks

2. Land use changes on site E N/A

Remarks

3. Land use changes off site IEI N/A

Remarks

VI. GENERAL SITE CONDITIONS

A. Roads	X Applicable ~ N/A

1. Roads damaged	~ Location shown on site map ~ Roads adequate	X N/A

Remarks


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B. Other Site Conditions

Remarks

VH. LANDFILL COVERS ~ Applicable X N/A

A. Landfill Surface

1. Settlement (Low spots)

Areal extent	

Remarks

~ Location shown on site map ~ Settlement not evident
Depth	

2. Cracks

Lengths_
Remarks

~ Location shown on site map ~ Cracking not evident
Widths	 Depths	

Erosion

Areal extent_
Remarks

~ Location shown on site map
Depth	

~ Erosion not evident

Holes

Areal extent_
Remarks

~ Location shown on site map
Depth	

~ Holes not evident

5. Vegetative Cover	~ Grass	~ Cover properly established ~ No signs of stress

~ Trees/Shrubs (indicate size and locations on a diagram)

Remarks

6. Alternative Cover (armored rock, concrete, etc.) ~ N/A

Remarks

7. Bulges

Areal extent_
Remarks

~ Location shown on site map ~ Bulges not evident
Height	


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8.

Wet Areas/Water Damage

X Wet areas/water damage not evident



~ Wet areas

~ Location shown on site map Areal extent



~ Ponding

~ Location shown on site map Areal extent



~ Seeps

~ Location shown on site map Areal extent



~ Soft subgrade

~ Location shown on site map Areal extent



Remarks









9.

Slope Instability ~ Slides

~ Location shown on site map IX] No evidence of slope instability



Areal extent





Remarks









B.

Benches ~ Applicable

IX] N/A



(Horizontally constructed mounds of earth placed across a steep landfill side slope to interrupt the slope



in order to slow down the velocity of surface runoff and intercept and convey the runoff to a lined



channel.)



1.

Flows Bypass Bench

~ Location shown on site map ~ N/A or okay



Remarks









2.

Bench Breached

~ Location shown on site map ~ N/A or okay



Remarks









3.

Bench Overtopped

~ Location shown on site map ~ N/A or okay



Remarks









C.

Letdown Channels ~ Applicable

IEI N/A



(Channel lined with erosion control mats, riprap, grout bags, or gabions that descend down the steep side



slope of the cover and will allow the runoff water collected by the benches to move off of the landfill



cover without creating erosion gullies.)

1.

Settlement ~ Location shown on site map ~ No evidence of settlement



Areal extent

Depth



Remarks









2.

Material Degradation ~ Location shown on site map ~ No evidence of degradation



Material type

Areal extent



Remarks









3.

Erosion ~ Location shown on site map ~ No evidence of erosion



Areal extent

Depth



Remarks










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4.

Undercutting ~ Location shown on site
Areal extent Depth
Remarks

map ~ No evidence of undercutting









5.

Obstructions Type ~ No obstructions

~ Location shown on site map Areal extent

Size

Remarks











6.

Excessive Vegetative Growth Type

~	No evidence of excessive growth

~	Vegetation in channels does not obstruct flow

~	Location shown on site map Areal extent
Remarks











D.

Cover Penetrations ~ Applicable X N/A





1.

Gas Vents ~ Active ~ Passive

~	Properly secured/locked ~ Functioning ~ Routinely sampled

~	Evidence of leakage at penetration ~ Needs Maintenance
Remarks

~	Good condition

~	N/A









2.

Gas Monitoring Probes

~	Properly secured/locked ~ Functioning

~	Evidence of leakage at penetration
Remarks

~	Routinely sampled

~	Needs Maintenance

~	Good condition

~	N/A









3.

Monitoring Wells (within surface area of landfill)

~	Properly secured/locked ~ Functioning

~	Evidence of leakage at penetration
Remarks

~	Routinely sampled

~	Needs Maintenance

~	Good condition

~	N/A









4.

Leachate Extraction Wells

~	Properly secured/locked ~ Functioning

~	Evidence of leakage at penetration
Remarks

~	Routinely sampled

~	Needs Maintenance

~	Good condition

~	N/A









5.

Settlement Monuments ~ Located
Remarks

~ Routinely surveyed

~ N/A










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E.

Gas Collection and Treatment ~ Applicable

IX] N/A

1.

Gas Treatment Facilities

~	Flaring ~ Thermal destruction

~	Good condition ~ Needs Maintenance
Remarks

~ Collection for reuse







2.

Gas Collection Wells, Manifolds and Piping

~ Good condition ~ Needs Maintenance
Remarks









3.

Gas Monitoring Facilities (e.g., gas monitoring of adjacent homes or buildings)

~ Good condition ~ Needs Maintenance ~ N/A

Remarks







F.

Cover Drainage Layer ~ Applicable

IX] N/A

1.

Outlet Pipes Inspected ~ Functioning
Remarks

~ N/A







2.

Outlet Rock Inspected ~ Functioning
Remarks

~ N/A







G.

Detention/Sedimentation Ponds ~ Applicable

IX] N/A

1.

Siltation Areal extent Depth

~ N/A



~ Siltation not evident
Remarks









2.

Erosion Areal extent Depth



~ Erosion not evident
Remarks









3.

Outlet Works ~ Functioning ~ N/A
Remarks









4.

Dam ~ Functioning ~ N/A
Remarks










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H. Retaining Walls ~ Applicable IE N/A

1.

Deformations ~ Location shown on site map ~ Deformation not evident
Horizontal displacement Vertical displacement



Rotational displacement
Remarks









2.

Degradation ~ Location shown on site map
Remarks

~ Degradation not evident







I. Perimeter Ditches/Off-Site Discharge ~ Applicable

IEI N/A

1.

Siltation ~ Location shown on site map
Areal extent Depth
Remarks

~ Siltation not evident







2.

Vegetative Growth ~ Location shown on site map
~ Vegetation does not impede flow
Areal extent Type
Remarks

~ N/A







3.

Erosion ~ Location shown on site map

Areal extent Depth

Remarks

~ Erosion not evident







4.

Discharge Structure ~ Functioning ~ N/A
Remarks











VHI. VERTICAL BARRIER WALLS

~ Applicable X N/A

1.

Settlement ~ Location shown on site map

Areal extent Depth

Remarks

~ Settlement not evident







2.

Performance Monitoring





Type of monitoring ~ Performance not monitored
Frequency ~ Evidence of breaching
Head differential
Remarks








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IX. GROUNDWATER/SURFACE WATER REMEDIES ~ Applicable IE N/A

A.

Groundwater Extraction Wells, Pumps, and Pipelines ~ Applicable IE N/A

1.

Pumps, Wellhead Plumbing, and Electrical

~ Good condition ~ All required wells properly operating ~ Needs Maintenance ~ N/A
Remarks

2.

Extraction System Pipelines, Valves, Valve Boxes, and Other Appurtenances

~ Good condition ~ Needs Maintenance
Remarks

3.

Spare Parts and Equipment

~ Readily available ~ Good condition ~ Requires upgrade ~ Needs to be provided
Remarks

B. Surface Water Collection Structures, Pumps, and Pipelines ~ Applicable ~ N/A

1.

Collection Structures, Pumps, and Electrical

~ Good condition ~ Needs Maintenance
Remarks

2.

Surface Water Collection System Pipelines, Valves, Valve Boxes, and Other Appurtenances

~ Good condition ~ Needs Maintenance
Remarks

3.

Spare Parts and Equipment

~ Readily available ~ Good condition ~ Requires upgrade ~ Needs to be provided
Remarks


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C. Treatment System ~ Applicable X N/A

1. Treatment Train (Check components that apply)

~ Metals removal ~ Oil/water separation ~ Bioremediation

~ Air stripping ~ Carbon adsorbers



~ Filters



~ Additive (e.g., chelation agent, flocculent)

~ Others

~ Good condition ~ Needs Maintenance



~ Sampling ports properly marked and functional



~ Sampling/maintenance log displayed and up to date



~ Equipment properly identified



~ Quantity of groundwater treated annually



~ Quantity of surface water treated annually



Remarks





2. Electrical Enclosures and Panels (properly rated and functional)



~ N/A ~ Good condition ~ Needs Maintenance



Remarks





3. Tanks, Vaults, Storage Vessels



~ N/A ~ Good condition ~ Proper secondary containment

~ Needs Maintenance

Remarks





4. Discharge Structure and Appurtenances

~ N/A ~ Good condition ~ Needs Maintenance



Remarks





5. Treatment Building(s)



~ N/A ~ Good condition (esp. roof and doorways) ~ Needs repair

~ Chemicals and equipment properly stored



Remarks





6. Monitoring Wells (pump and treatment remedy)



~ Properly secured/locked ~ Functioning ~ Routinely sampled

~ Good condition

~ All required wells located ~ Needs Maintenance

~ N/A

Remarks





D. Monitoring Data

1. Monitoring Data



X Is routinely submitted on time X Is of acceptable quality



2. Monitoring data suggests:

~ Groundwater plume is effectively contained X Contaminant concentrations are declining


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E.

Monitored Natural Attenuation

1.

Monitoring Wells (natural attenuation remedy)

X Properly secured/locked X Functioning ~ Routinely sampled X Good condition
X All required wells located ~ Needs Maintenance ~ N/A
Remarks:

All wells sited, observed, and locked during inspection. No issues noted.

X. OTHER REMEDIES

If there are remedies applied at the site which are not covered above, attach an inspection sheet describing
the physical nature and condition of any facility associated with the remedy. An example would be soil
vapor extraction.

XL OVERALL OBSERVATIONS

A.

Implementation of the Remedy



Describe issues and observations relating to whether the remedy is effective and functioning as designed.
Begin with a brief statement of what the remedy is to accomplish (i.e., to contain contaminant plume,
minimize infiltration and gas emission, etc.).



Data shows that MNA continues to occur at the site

B.

Adequacy of O&M

Describe issues and observations related to the implementation and scope of O&M procedures. In
particular, discuss their relationship to the current and long-term protectiveness of the remedy.
N/A


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c.

Early Indicators of Potential Remedy Problems



Describe issues and observations such as unexpected changes in the cost or scope of O&M or a high



frequency of unscheduled repairs that suggest that the protectiveness of the remedy may be compromised



in the future.



No issues noted or identified

D.

Opportunities for Optimization



Describe possible opportunities for optimization in monitoring tasks or the operation of the remedy.



None noted during inspection


-------
Trip Report
Photo 1

Description:

Overhead View of Facility

Date:
Direction:

Photographer:

Previous Photo


-------
XM lit/ 1d1~S-

HaU, N^ioS	bfJ

,.4

—^AOjaJoZU^ Vr.^Ufir-	J5g^ ft-fitTe*

Trip Report
Photo 2

Description:

Five Year Review Inspection Sign-In Roster

Date: 9/26/23
Direction:

Photographer:

David Wennerstrom


-------
Trip Report
Photo 3

Description:

Active Plant Operations

Date: 9/26/23
Direction: North

Photographer:

David Wennerstrom


-------
Trip Report
Photo 4

Description:

Site Inspection Team

Date: 9/26/23
Direction: South

Photographer:

David Wennerstrom


-------
Trip Report
Photo 5

Description:

VMS Pipe with Protection

Date: 9/26/23
Direction: East

Photographer:

David Wennerstrom


-------
S^r™ -
1 £

r«/** _
I 4 ^

MHH

Trip Report
Photo 6

Description:

VMS Operational Confirmed - Negative Vacuum

Date: 9/26/23
Direction: North

Photographer:

David Wennerstrom


-------

-------
Trip Report
Photo 8

Description:

Flush Mount Monitoring Well Field - rear of facility

Date: 9/26/23
Direction: South

Photographer:

David Wennerstrom


-------
Trip Report
Photo 9

Description:

FAG 33-36 Monitoring Well Cluster

Date: 9/26/23
Direction: West

Photographer:

David Wennerstrom


-------
Trip Report
Photo 10

Description:

Detention Pond behind facility

Date: 9/26/23
Direction: South

Photographer:

David Wennerstrom


-------
Trip Report
Photo 11

Description:

FAG-S5 Monitoring Well Secured

Date: 9/26/23
Direction: South

Photographer:

David Wennerstrom


-------
File Name:

Photographer: David Wennerstrom
Type of Camera:

Digital Recording Media:

Original copy is stored in:

No changes were made in the original image files prior to storage on the hard drive.

Report Photo #

Photographer

Date

Approx. Time

Description

1

Wennerstrom

9/26/23

1116

Overhead View of Facility

2

Wennerstrom

9/26/23

1122

Five Year Review Inspection Sign-In Roster

3

Wennerstrom

9/26/23

1129

Active Plant Operations

4

Wennerstrom

9/26/23

1135

Site Inspection Team

5

Wennerstrom

9/26/23

1147

VMS Pipe with Protection

6

Wennerstrom

9/26/23

1152

VMS Operational Confirmed - Negative Vacuum

7

Wennerstrom

9/26/23

1157

VMS Roof Vent

8

Wennerstrom

9/26/23

1202

Flush Mount Monitoring Well Field - rear of facility

9

Wennerstrom

9/26/23

1215

FAG 33-36 Monitoring Well Cluster

10

Wennerstrom

9/26/23

1225

Detention Pond behind facility

11

Wennerstrom

9/26/23

1215

FAG-85 Monitoring Well Secured


-------
APPENDIX D - REPORTS


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IN-SITU CHEMICAL OXIDATION PILOT STUDY

Remedial Action - Newton County Wells Site
Silver Creek and Saginaw, Missouri

Prepared for

Missouri Department of Natural Resources

On behalf of

FAG Bearings, LLC
Joplin, Missouri

Prepared by

Ramboll US Consulting, Inc.

St. Louis, Missouri

Date

July 2023

Project Number

1690004605

122332^331


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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

Paae

1.	INTRODUCTION	1

1.1	Background	1

1.2	Site Setting Summary	4

1.2.1	Unconsolidated Overburden	4

1.2.2	Mississippian Aquifer	4

1.3	Site History and Current Status	5

1.3.1	Former Pipeline Trench Removal Action	5

1.3.2	Remedial Action Monitoring	6

1.3.3	Fate and Transport	6

1.4	Pilot Test Objectives	7

2.	PILOT TEST APPROACHES	9

2.1	Oxidant Selection	9

2.2	Reagent Delivery Approaches	9

2.3	ISCO Pilot Test Areas Selection	 10

2.3.1	Area A - Northeast to Southwest Trending Bedrock Depression	 10

2.3.2	Area B - North to South Trending Bedrock Depression	 10

2.3.3	Former TCE Pipeline Trench	 11

2.4	Monitoring Criteria	 11

3.	PILOT TEST IMPLEMENTATION PLAN	12

3.1	Permits and Authorizations	 12

3.2	Pilot Test New Injection and Monitoring Wells	 12

3.2.1	Area A	 12

3.2.2	Area B	 13

3.3	Implementation and Injection Plan	 13

3.3.1	Area A Injection Plan	 13

3.3.2	Area B Injection Plan	 14

3.3.3	Former TCE Pipeline Trench Injection Plan	 15

3.4	Waste Management	 16

3.5	Other Plans Related to Field Implementation	 16

3.6	Groundwater Parameter Monitoring	 16

3.7	Performance Monitoring Plan	 17

3.7.1	Baseline Groundwater Sampling Event	 17

3.7.2	Post Injection Groundwater Sampling	 17

4.	RECORD KEEPING AND REPORTING	18

4.1	Record Keeping	 18

4.2	Reporting	 18

5.	REFERENCES	19

July 2023	'


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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

¦LES

Table 1: Summary of Former TCE Pipeline Trench Perched Water Sampling Results (2022)

II RES
Figure 1: Site Location

Figure 2: Former TCE Pipeline Trench and Injection Wells

Figure 3: Uppermost Groundwater TCE Results Summary (1999 to 2022)

Figure 4: Spring Water and Mississippian Aquifer TCE Results Summary (1999 to 2022)

Figure 5: Top of Bedrock Contour Map

Figure 6: Locations of Proposed Pilot Test Areas

Figure 7: Proposed Pilot Test Area A

Figure 8: Proposed Pilot Test Area B

LIST OF APPENDICIES

Appendix A: Focused 2022 Trench Sampling Analytical Report

July 2023

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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

1, INTRODUCTION

This Pilot Study Work Plan describes the rationale and procedures for implementation of
focused in-situ chemical oxidation (ISCO) as part of the ongoing Remedial Action (RA) at
the Newton County Wells Site (NCWS or site) located in northern Newton County, Missouri.

The RA consists of those activities being undertaken by FAG Bearings LLC (FAG or FAG
Bearings) to implement the Record of Decision (ROD) executed on September 30, 2004,
related to the NCWS. The ROD constitutes the decision by the Missouri Department of
Natural Resources (MDNR) and USEPA Region VII on the RAs to be implemented at the
NCWS. The ROD is included as Attachment A to the Remedial Decision/Remedial Action
Consent Decree (RD/RA Consent Decree) between the State of Missouri (plaintiff) and FAG
Bearings, LLC (defendant) which became effective in January 2007.

As described in the 2022 RA Annual Report provided to MDNR and USEPA, FAG intends to
conduct a focused pilot study commencing in calendar year 2023 to provide additional
source control and enhancement of natural attenuation of impacted groundwater. The
extensive investigations of site conditions which have been completed combined with results
from ongoing routine monitoring of groundwater during the RA have been utilized in the
design of the pilot study.

1.1 BACKGROUND

The NCWS originates at the FAG facility located at 3900 South Rangeline Road in Joplin,
Missouri, and is defined as the FAG property and portions of the Villages of Silver Creek and
Saginaw, Missouri, where the compound trichloroethylene (TCE) and/or compounds
resulting from its natural degradation have come to be located (Figure 1). TCE and TCE
degradation products are driving environmental risk with respect to the NCWS.

In August 2000, USEPA formally placed NCWS on the National Priorities List (NPL) (EPA ID:
MOD985798339). Actions conducted with respect to the NCWS by FAG up to and including
the RA are summarized below.

Abatement Order on Consent (1998) and Removal Action

In November 1998, FAG entered into an Abatement Order on Consent (1998 AOC) with
MDNR that required FAG to conduct soil and groundwater investigation on its property and
focused groundwater and surface water sampling in the Villages of Silver Creek and
Saginaw.

The investigation determined that an accidental release from a former TCE transfer pipeline
in 1983 on the FAG property was the sole source of TCE and TCE degradation products on
the FAG property capable of producing groundwater impacts that were observed in the
Villages of Silver Creek and Saginaw. Unbeknownst to FAG, TCE had apparently not been
completely drained from the pipeline when it had been taken out of service and residual TCE
was released into the granular backfill of the pipeline trench when the pipeline was cut as

July 2023

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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

part of a construction project. Dissolved as well as dense non-aqueous phase liquid (DNAPL)
TCE was first identified in the pipeline trench in 2000.

FAG prepared an engineering evaluation/cost assessment (EE/CA) report which detailed the
findings of the 1998 AOC investigations and proposed non-time critical removal actions.
Between January 2002 and June 2003, multiple injections of chemical oxidant were
strategically implemented in the former pipeline trench to destroy TCE in the pipeline
trench. The location of the pipeline trench and associated injection wells utilized for ISCO
are provided on Figure 2. Concurrent with the ISCO treatment trench, focused removal of
impacted soil was also conducted beyond the limits of the former pipeline trench.

A report documenting activities completed to fulfill the requirements of the 1998 AOC,
including destruction of TCE in the pipeline trench and focused removal of soil, was
submitted to MDNR by FAG in December 2003.

Abatement Order on Consent (2000) and Remedial Investigation/Feasibility Study

In October 2000, FAG entered into an Abatement Order on Consent (2000 AOC) with MDNR
which required the performance of a Remedial Investigation/Feasibility Study (RI/FS) for the
NCWS.

In March 2004, FAG completed the RI/FS reports utilizing the comprehensive investigations
conducted to fulfill the both the 1998 and 2000 AOCs. This information provided the basis
for the development and evaluation of potential remedial response alternatives with respect
to the NCWS.

Record of Decision and RD/RA Consent Decree

In September 2004, MDNR and USEPA issued the final ROD which selected the following RA
objectives and remediation alternative for the NCWS.

RA Objectives

•	Maintain and enforce current conditions and existing regional regulatory controls that
provide protection from risk-producing exposure to the TCE and TCE degradation
product impacted portions of the Mississippian Aquifer;

•	Reduce the concentration of TCE and TCE degradation products in the uppermost
aquifer of the NCWS to concentrations that are protective of the Mississippian Aquifer
as a potable water source with respect to TCE and TCE degradation products; and

•	Return the Mississippian Aquifer water quality at the NCWS to potable conditions,
with respect to TCE and TCE degradation products.

Remediation Alternative

•	Monitored natural attenuation (MNA) to address the uppermost groundwater and the
Mississippian Aquifer.

July 2023

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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

•	Implementation/enforcement of existing regional institutional controls (ICs)
including:

-	Special Area 21 as provided in the Missouri Well Construction Rules;

-	Monitoring usage of public water supply systems; and

-	Enforcement of prohibition on usage of impacted wells for potable purposes
with subsequent connection to the public water supply system.

FAG is responsible for implementation of activities required for the MNA portion of the
chosen alternative for the NCWS while MDNR is responsible for the implementation/
enforcement of the existing regional institutional controls.

Subsequently, FAG entered into an RD/RA Consent Decree with MDNR with an effective date
of January 2007 to conduct an RA program to implement the ROD in accordance with the
requirements of the RD/RA Consent Decree. As noted by MDNR in the June 2005 Consent
Decree Statement of Work for the NCWS, "TCE and TCE degradation products present in the
soil and groundwater of the NCWS are a result of the cutting of and accidental release of
TCE from the former TCE transfer pipeline on the FAG Bearings property."

Implementation of RD/RA Consent Decree

Field activities required to implement the NCWS RA commenced in 2008 following submittal
of the Remedial Action Work Plan (RAWP) by FAG to MDNR and USEPA and subsequent
approval. Implementation of RA field activities and subsequent reporting remains ongoing
following the RAWP and subsequent amendments with inclusion of formal findings and
recommendations from MDNR and USEPA. A total of 17 RA groundwater/spring surface
water sampling events have been completed since implementation and through the most
recent event conducted in calendar year 2022.

The locations of all RA sampling points and tabulated summaries of TCE analytical results in
the uppermost groundwater and Mississippian Aquifer & spring surface water sampling
locations since the RA commenced are provided in Figures 3 and 4, respectively.

Detailed results presented in RA reports include calculated statistical temporal trends of
analytical results for TCE and TCE degradation products associated with each monitoring
location (if detected).

Criteria for effectiveness of MNA towards achieving the objective provided in the ROD and
Second Five Year Summary Report include:

•	ROD: "Should no significant decreasing trend in the levels of TCE be observed in the
Mississippian Aquifer during the first five years of sampling, over a consistent period
of time, a contingency to use ISCO to treat contamination in the uppermost
groundwater will be implemented."

1 Special Area 2 in the Missouri Well Construction Rules (Code) is now referred to as Area 11.

July 2023

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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

• Second Five Year Report: "If MNA parameters do not appear to be occurring near the
former trench and/or if a significant decreasing trend in TCE levels is not observed in
the Mississippian Aquifer consider the implementation of ISCO injections."

1.2 SITE SETTING SUMMARY

Following is a summary of the two water bearing units which are the focus of the NCWS RA
as specified in the ROD.

1.2.1	Unconsolidated Overburden

Unconsolidated overburden associated with NCWS is primarily a brownish red, silty-clay with
chert fragments and nodules suspended in the silty-clay matrix forming discrete,
discontinuous layers and lenses. The thickness of the unconsolidated overburden materials
in the northern portions of the site ranges from approximately 15 feet up to a maximum of
approximately 100 feet. This thickness is influenced by variations in the depth to the top of
bedrock as determined from multiple historic investigations conducted at the site (Figure 5).

Uppermost groundwater flows primarily through the granular basal overburden materials
and in some cases through interconnected transmissive zones in shallow bedrock at the
overburden/bedrock interface. The horizontal groundwater flow potential in the uppermost
groundwater bearing zone is primarily to the south, to the southwest and to the west from
the central portion of the FAG Bearings property. The actual flow direction in discrete areas
is controlled by the occurrence and distribution of the complex unconsolidated overburden
deposits as well as the relative presence/absence of a shallow transmissive zone at the
overburden/bedrock interface.

1.2.2	Mississippian Aquifer

The upper bedrock aquifer at the Site occurs within Mississippian aged limestone bedrock.
Secondary porosity and permeability resulting from fracturing, faulting and associated
solution weathering are a dominant control for the occurrence and yield of groundwater.
The Mississippian units consist of the relatively dense Warsaw formation which generally
provides minimal water yield to wells and is underlain by the Keokuk, Elsey and Reeds
Spring formations which have the potential to be more permeable and provide adequate
water yield to wells for domestic purposes. The basal Mississippian aged Pierson formation is
a dolomitic limestone which is less permeable and provides only limited potential water
yield.

Horizontal groundwater flow direction in the Mississippian Aquifer has been determined to
be generally from north to south across the Site through the more permeable water bearing
formations which are located between less permeable overlying and underlying bedrock
formations.

Fraction organic carbon measured in the bedrock units comprising the Mississippian Aquifer
are relatively low such that bedrock is unlikely to have a source of adsorbed organic

July 2023

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ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

contaminants that could influence groundwater long-term. However, solute migration
through fractures in bedrock may be influenced by matrix diffusion. Matrix diffusion refers
to a process in which solutes dissolved in groundwater diffuse both into and out of the rock
matrix. The potential for back diffusion from the rock matrix into open fractures could have
an effect on the longer-term remediation process.

1.3 SITE HISTORY AND CURRENT STATUS

As detailed in reports detailing the extensive investigations conducted of NCWS, a one-time
release was associated with reconstruction of a former subsurface TCE transfer pipeline on
the FAG Bearings property in 1983. This work was conducted by plumbing and excavation
contractors as part of a plan to potentially reuse sections of the pipeline as part of FAG's
wastewater treatment system. The pipeline was approximately 500 feet in length and
consisted of 2 inch diameter steel pipe. At the time the transfer pipeline was cut by the
contractors, TCE was no longer being used at the facility.

Unknown to FAG Bearings, TCE had not been completely drained from the pipeline when it
had been previously taken out of service and remnant TCE was accidentally released to the
excavation. This resulted in a finite volume of DNAPL accumulating in the granular backfill
materials of the shallow pipeline trench which had been constructed within the surrounding
dense native silty clay. DNAPL in the pipeline trench was first identified in 2000 as part of
the 1998 Removal Consent Order investigation and was determined to be limited to the
approximate center section of the trench.

1.3.1 Former Pipeline Trench Removal Action

As introduced in the background section, as part of enacting the 1998 AOC, a proactive and
significant remedial action was completed which focused on destruction of DNAPL and
dissolved phase TCE and TCE degradation products in the primary source of impact, the
granular backfill material of the shallow pipeline trench. This consisted of ISCO treatment of
the TCE DNAPL and associated dissolved phase impact in the former pipeline trench using
potassium permanganate as the oxidant. A total of approximately 30,000 gallons of
potassium permanganate solution was injected into the former TCE transfer pipeline trench
during multiple events. Injections were performed from January 2002 through June 2003
using constructed injection wells. An additional focused response action was conducted in
March 2003 consisting of excavation, offsite disposal and backfilling/grouting in specific
areas of identified vadose zone soil impact beyond the immediate area of the treated
pipeline trench.

Most of the volume of TCE released in the former transfer pipeline trench source was
determined to have been eliminated by ISCO at the conclusion of the removal actions which
included fully destroying DNAPL. Perched water in the treated pipeline trench source area
was most recently sampled in 2022 by collecting samples from five select injection wells
(IW-01, IW-04, IW-10, IW-16 and IW-20) installed within the trench (Figure 2). This
sampling event included the center section of the trench since this is the location where the
historic one-time release occurred and where the most significant impact had been

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identified. A summary of detected analytical parameters is provided in Table 1 and the
laboratory analytical report is included as Appendix A. As provided in the summary, the
injection well in the approximate center of the trench (IW-10) was the only well which
contained TCE at a relatively significant concentration [1,230 micrograms per liter (|jg/L)],
while injection wells located to the east and west had TCE measured significantly lower or
below laboratory reporting limits. These concentrations confirm that significant destruction
of TCE from the ISCO completed within the pipeline trench continues to be sustained and
that remnant measured concentrations are confined primarily within the general center
portion of the trench at concentrations well below those which could be indicative of any
potential DNAPL.

1.3.2	Remedial Action Monitoring

Implementation of the NCWS RA with respect to the RD/RA Consent Decree commenced in
2008 and remains ongoing. This was enacted following completion of activities related to the
1998 and 2000 AOCs.

A total of 17 RA groundwater and surface water sampling events have been completed and
the data sets acquired are detailed in routine RA reports provided to MDNR and USEPA.
These reports provide a detailed review of historic and recent RA results and also provide
calculated statistical temporal trends of analytical results for TCE and TCE degradation
products associated with each RA monitoring location (if detected). Summary tabulated
results of TCE measurements throughout the RA up to the most recent 2022 sampling event
are provided for the monitored uppermost groundwater and Mississippian Aquifer/spring
surface water locations are provided in Figures 3 and 4, respectively.

1.3.3	Fate and Transport

As detailed in the NCWS RI/FS and other documentation, dissolution of DNAPL that had
been present in the former TCE pipeline trench resulted in migration of limited quantities of
aqueous phase TCE through fractures in the unconsolidated overburden beneath the former
transfer pipeline trench. This resulted in an uppermost groundwater TCE plume residing
primarily on FAG Bearings property down-gradient of the trench which did also cross the
southern property boundary to a very limited and defined extent. The dissolved phase TCE
also migrated downward through the dense shallow bedrock and upon reaching the
Mississippian Aquifer it migrated horizontally in a generally southern direction. The following
two primary pathways of TCE groundwater migration on the FAG Bearings property beyond
the pipeline trench were identified.

North-South Trending Bedrock Depression

This bedrock feature is located below and south of the former TCE pipeline trench and
extends below surrounding top of rock elevation (Figure 5). Investigation and sampling of
soil and groundwater from unconsolidated deposits determined dissolved phase TCE had
migrated into this feature. Given the relatively strong downward component to the hydraulic
gradient between overburden and the Mississippian Aquifer at the site and the occurrence of

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TCE in groundwater in the Mississippian Aquifer proximate to this feature (e.g., FAG-AW-4),
it was evident dissolved phase TCE present in the uppermost groundwater migrated
downward and upon entering the Mississippian Aquifer has migrated horizontally following
the general southward flow direction.

TCE and TCE degradation products have been detected in uppermost groundwater wells
monitoring this feature including wells FAG-36 and FAG-85 completed in the deeper basal
portion of this feature. Calculated temporal trends for TCE and TCE degradation products in
specific uppermost wells monitoring this feature indicate generally stable or decreasing
trends for wells monitoring shallow and intermediate zones in this feature. Basal well FAG-
36 displays stable temporal trends over the short-term and increasing temporal trends over
the long-term, while basal well FAG-85 located down-gradient of FAG-36 displays relatively
stable temporal trends over both the short- and long-term.

Northeast-Southwest Trending Bedrock Depression

This bedrock feature is located southwest of the former TCE pipeline trench and becomes
more pronounced and extends below surrounding top of bedrock elevation approaching the
southern property boundary (Figure 5). Similar to the above-described north-south trending
feature, downward transport of dissolved phase TCE into this feature may be facilitated by
the relatively strong downward component to the hydraulic gradient between the uppermost
groundwater and the Mississippian Aquifer at the site. TCE migrating into this feature could
then migrate downward and upon entering the Mississippian Aquifer, the dissolved phase
TCE would migrate horizontally in a generally southward direction.

TCE and TCE degradation products have been detected in uppermost groundwater primarily
near the commencement of this feature (FAG-50) while monitoring wells completed in the
deeper portions of this feature contain low to trace concentrations of TCE. Calculated
temporal trends for TCE and TCE degradation products in uppermost wells monitoring this
feature indicate long-term stable or decreasing trends (if detected) while more recent term
trends indicate increasing temporal trends only near the commencement of this feature
(FAG-50).

1.4 PILOT TEST OBJECTIVES

As provided in the 2022 RA Report submitted to MDNR and USEPA, natural attenuation
continues to be effective with regard to the NCWS in that the majority of wells in both the
uppermost groundwater and Mississippian Aquifer have decreasing temporal trends
calculated for both long and short-term time frames. However, as also noted in the 2022 RA
Report, FAG Bearings recognized a subset of wells that display stable temporal trends while
also exceeding goal concentrations and a limited subset of wells that display increasing
temporal trends for specific compounds of concern. Based on these trends and the direction
provided by the NCWS ROD and subsequent discussion with MDNR and USEPA, FAG
Bearings committed to preparing a conceptual pilot test work plan towards conducting
focused in-situ treatment of uppermost groundwater. The objectives are to treat remnant
concentrations in the former pipeline trench source and to treat impact beyond the trench

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and expedite the natural attenuation process towards achieving the RA objectives as
provided in the NCWS ROD.

As previously described, ISCO conducted at the Site has been confirmed to be effective in
significantly destroying TCE mass which had accumulated in the former transfer pipeline
trench. Further, implementation of additional ISCO was retained in the NCWS ROD as a
potential contingency measure for the selected MNA remedy. Therefore, for the purposes of
this pilot test, ISCO will continue to be utilized for treatment of TCE and TCE degradation
products.

The pilot test will provide for the collection of data necessary to provide for expanded ISCO
in specific overburden zones outside of the former TCE pipeline transfer trench. This
implementation data will include reagent delivery methods, injection parameters (radius of
influence, pressures, rates and volumes and subsurface reactions) and the effects of ISCO
treatment on the impacted groundwater in the areas selected for treatment. Previous
reviews of tracer injections conducted during field activities associated with the RI indicated
an approximate 25 foot spacing of injection points could provide adequate and overlapping
radius of influence (ROI) coverage in the overburden. This work plan presents the pilot test
approaches, activities and a post-implementation sampling schedule to provide data to
evaluate these proposed activities and their effectiveness.

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2. PILOT TEST APPRO ACH ES

2.1	OXIDANT SELECTION

Permanganate has been previously utilized as an ISCO treatment amendment at NCWS and
has effectively destroyed TCE and TCE degradation products. For this pilot study, the
oxidant sodium permanganate (NaMnCk) has been identified for implementation. Sodium
permanganate is provided as a liquid solution which is easier to handle and mix in the field
versus potassium permanganate which is provided in a solid form. Mixing of the liquid
sodium permanganate will not create the risk of generating oxidant dust during
implementation and it also provides the option to be prepared at higher concentrations than
potassium permanganate. Furthermore, the amount of potassium permanganate which
would be utilized for this pilot test would likely trigger tracking and recording requirements
from the United States Department of Homeland Security (DHS), while there is not a similar
DHS requirement for sodium permanganate solution.

2.2	REAGENT DELIVERY APPROACHES

Reagent delivery for the pilot test will be within two general zones: one zone will consist of
a focused section of the shallow former TCE pipeline trench and the second zone will focus
on specified residual zones beyond the trench at depths greater than 20 feet below ground
surface (bgs). The oxidant reagent will be delivered in-situ into targeted zones through
injection. The primary methods for delivery of reagent in-situ is through the use of
temporary direct push injection (DPI) probes or constructed injection wells.

Based on the estimated depth interval of remnant impacts at NCWS, injections through
temporary direct push and constructed wells will be studied as part of the pilot test. Data
collected from the pilot tests will assist delivery method selection and design for subsequent
larger scale implementation. Following is a summary of each delivery approach.

Direct Push Delivery

Delivery of reagent using direct push drilling equipment and tooling can be conducted
relatively quickly with little or no surface disturbance remaining following completion. This
method provides greater flexibility in remedial design with lower capital cost as compared to
constructed injection points. However, DPI has certain limitations including the depths it can
effectively reach which can be influenced by several factors including the drilling rig utilized
and site-specific geology such as depth to competent bedrock, density of unconsolidated
lithologies, presence of large rocks or similar issues. Direct push delivery may require the
use of higher injection pressures in part because of the limited timeframes in which to
emplace the desired volume of reagent in an efficient manner.

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Injection Well Delivery

Delivery of reagent using constructed injection wells are typically required for injections in
deeper zones of unconsolidated units and situations where long-term injection points may
be necessary. Injection wells can become cost effective as compared to DPI when several
rounds of injection are anticipated. Injection wells can allow for lower injection rates and
pressures which can limit potential daylighting, provide for a longer timeframe to inject
reagent and prevent uncontrolled fracturing of the treatment zone. Wells can be constructed
in nested configurations within single borings to allow for multiple screened injection depth
intervals to be targeted.

Injection wells were successfully utilized at NCWS for the previous full scale ISCO treatment
of the former TCE pipeline trench. Select existing injection wells in the trench will be used
during the pilot test to provide tertiary treatment of remnant impact identified in the
general center section of the trench.

2.3 ISCO PILOT TEST AREAS SELECTION

Two areas outside of the former pipeline trench have been selected to evaluate delivery and
treatment of TCE and TCE degradation product impact based on historic and recent
groundwater data, temporal trend calculations, site determined fate and transport and
specific geologic settings and depths identified for treatment. The locations of these two
areas are provided on Figure 6 and described in the following sections.

2.3.1	Area A - Northeast to Southwest Trending Bedrock Depression

An area near uppermost groundwater monitoring well FAG-50 has been selected to conduct
DPIs to treat the relatively shallow overburden/bedrock interface at this location (Figure 7).
The existing monitoring well is screened from approximately 32-37 feet bgs and extends to
the approximate top of the overburden/bedrock interface. As previously described, this well
is situated at the commencement of the northeast to southwest trending bedrock depression
near the down-gradient property boundary which was identified in the NCWS RI as a
potential pathway of TCE impacted groundwater migration on the FAG Bearings property
outside the former pipeline trench.

A TCE concentration of 2,050 |jg/L was measured in FAG-50 during the most recent 2022
sampling event and temporal trends of TCE concentrations in this well have been
determined to be stable since RA monitoring commenced and increasing over the eight most
recent sampling events. Wells located further down-gradient in this bedrock depression
have much lower TCE concentrations as compared to FAG-50 and generally display
decreasing TCE temporal trends over both the long- and short-term (when detected).

2.3.2	Area B - North to South Trending Bedrock Depression

An area near an existing cluster of four uppermost groundwater monitoring wells (FAG-33
through FAG-36) has been selected to conduct a combination of DPIs and injection wells for

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treatment (Figure 8). This area is located down-gradient of the former TCE pipeline trench
and located within the north to south trending bedrock depression which was identified in
the NCWS RI as a potential pathway of TCE impacted groundwater migration on the FAG
Bearings property.

Within this bedrock feature, FAG-33 and FAG-34 represent shallower groundwater
conditions (screened intervals of 44-45 and 53-54 feet bgs, respectively), FAG-35
represents intermediate groundwater conditions (screen interval of 69-70 feet bgs) and
FAG-36 represents deep groundwater conditions (screen interval of 94-95 feet bgs). FAG-36
is set to the top of the overburden/bedrock interface and represents basal conditions in this
bedrock depression feature. FAG-85 additionally represents upper groundwater conditions in
the basal portion of this bedrock feature (total depth of 95 feet bgs) at a location down-
gradient of the four well cluster.

The most significant concentrations of TCE measured in this well cluster for the 2022 RA
monitoring event are associated with shallow well FAG-34 (582 |jg/L), intermediate well
FAG-35 (537 ug/L) and deep well FAG-36 (455 |jg/L). Of these wells, FAG-34 and FAG-35
have calculated decreasing or stable temporal trends over both the long- and short-term
while FAG-36 has a calculated increasing temporal trend over the long-term and a stable
temporal trend over the short-term. Further down-gradient deep well FAG-85 had a slightly
lower TCE concentration measured for the 2022 RA monitoring event (252 |jg/L) and its
calculated temporal trends remain stable over both the long- and short-term.

2.3.3 Former TCE Pipeline Trench

In addition to the two pilot test areas described above, a tertiary ISCO injection will be
completed within the approximate center portion of the former TCE pipeline trench to
further eliminate residual TCE and TCE degradation products measured primarily in existing
trench injection well IW-10 (2022 TCE concentration of 1,230 |jg/L). This injection event
will include IW-10 and two wells located immediately west (IW's 11 and 12) and two wells
located immediately east (IW's 8 and 9).

2.4 MONITORING CRITERIA

During field implementation, information to be gathered will include injection pressures,
volumes of reagent delivered, the ROI and other injection parameters. Groundwater in
monitoring wells and injection wells within Areas A and B (both new and existing wells) will
be sampled in advance of the pilot test injection event. Subsequent to the injection event
these wells will be monitored on a periodic basis for up to six months to provide data to
evaluate ISCO performance which will include analysis for concentrations of TCE and TCE
degradation products. In addition, IW-10 within the center portion of the former TCE
pipeline trench will be sampled from four to six months following tertiary treatment of the
trench to confirm continued diminished concentrations of TCE and TCE degradation
products. Limited purging of wells to be sampled for post-implementation monitoring
purposes will be utilized following methodology consistent with the RA (positive pressure
pumping methodology) to limit potential removal of any active remedial amendment.

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3. PILOT TEST IMPLEMENTATION PLAN

3.1	PERMITS AND AUTHORIZATIONS

Wells used for remediation of subsurface impact are considered Class V underground
injection control (UIC) wells. The state of Missouri has obtained primacy for its UIC program
from USEPA to include Class V wells. Consequently, all Class V injection wells must be
approved by MDNR with construction regulated by the Missouri Geological Survey.

Monitoring wells are subject to regulations and recordkeeping provided in the Missouri Well
Construction Code.

Construction of multiple injection wells within a single boring in order to capture different
depth intervals efficiently may require a variance from MDNR in advance of drilling due to
slightly restricted annular space. For the purpose of this work plan, it is assumed a variance
will be granted. However, alternate methods to install and construct injection wells can be
implemented if a variance is not granted such as individual borings specific to each injection
well rather than combining in a single boring.

In addition, to obtaining approval for the planned wells at the Site and prior to initiation of
invasive subsurface actions - the Missouri One-Call system will be notified to mark public
buried utilities in the areas of planned work. A private locating service will be contracted to
perform additional subsurface checks for buried utilities or other structures prior to the
commencement of invasive work.

3.2	PILOT TEST NEW INJECTION AND MONITORING WELLS

The following new injection wells (temporary or permanent) and monitoring wells are
planned for installation in each pilot test area.

3.2.1 Area A

In pilot test Area A, a new uppermost groundwater monitoring well will be installed slightly
down-gradient (south) of existing well FAG-50 to provide additional monitoring capability for
the pilot test in this area. The new well will be identified as FAG-50A and will be drilled to
the top of bedrock in order to intercept the overburden/bedrock interface similar to existing
well FAG-50. Based on nearby drilling logs, it is anticipated the new well will be drilled to a
total depth of no more than approximately 40 feet bgs. The new well will be completed
similar to other existing uppermost groundwater monitoring wells at the Site as a standard
2 inch diameter well with a 5 foot long screened section with an above grade protective
cover. Following construction, the monitoring will be developed with a submersible pump or
bailer assembly to remove fine material from the sand pack and well screen. Approximately
five measured casing volumes of water will be purged from the well for development.

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Subsequent to installation of FAG-50A, four temporary DPI points (DPA-1 to DPA-4) will be
drilled to intercept the overburden/bedrock interface and overlying upper groundwater zone
for emplacement of reagent. The approximate proposed locations for these DPI points and
new monitoring well are provided in Figure 7.

3.2.2 Area B

In pilot test Area B, a combination of shallow temporary DPI points and constructed
intermediate and deep injection wells will be installed within the general area of the existing
monitoring well cluster (FAG-33 through FAG-36). The existing wells will be used to provide
monitoring capability for the pilot test in this area.

Two shallow DPI points (DPB-1 and DPB-2) will be drilled to intercept the shallow
groundwater zone to include the depth interval monitored by FAG-34 (54-55 feet bgs). The
temporary injection points will focus on the depth interval of approximately 45-55 feet bgs.

Two nested injection wells (IWB-1 and IWB-2) will be constructed, which will consist of an
intermediate and deep screened interval in each. The intermediate wells (IWBI-1 and IWBI-
2) will be screened from approximately 65-75 feet bgs to include the depth interval
monitored by FAG-35 (69-70 feet bgs) and the deep wells (IWBD-1 and IWBD-2) will be
screened from approximately 85-95 feet bgs to include the depth interval monitored by
FAG-36 (94-95 feet bgs) as well to intersect the overburden/bedrock interface. The injection
wells will be constructed within 8-inch diameter borings and consist of 2-inch diameter PVC
with 10 foot screens and a hydrated bentonite seal installed between the screened intervals.
Following construction, the nested injection wells will be developed with a submersible pump
or bailer assembly to remove fine material from the sand pack and well screen.
Approximately five measured casing volumes of water will be purged from each well for
development.

The approximate proposed locations for these DPI and injection wells are provided in Figure
8.

3.3 IMPLEMENTATION AND INJECTION PLAN

Following is a summary of the injections to be completed for implementation of the pilot
test. For the purposes of this pilot test, it is assumed an approximate 3% NaMnCU solution
will be utilized for injection and treatment.

3.3.1 Area A Injection Plan

FAG-50 located within pilot test Area A is screened from 32-37 feet bgs within the area to
be subject to treatment and has a seasonal static water level which can range up to
approximately 30 feet bgs. The base of this well is completed at the overburden/bedrock
interface. Four temporary DPIs in Area A will be advanced to target the approximate depth
interval of 30-40 feet bgs with the primary focus to be on delivering treatment amendment
to the overburden/bedrock interface.

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Field injection procedures to be conducted in Area A include:

•	Advance DPI points DPA-1 and DPA-2 with 5 foot long screens to the overburden/
bedrock interface which is expected to be encountered at no more than
approximately 40 feet bgs;

•	Inject through DPA-1 and DPA-2 simultaneously;

•	Monitor FAG-50 and the new monitoring well FAG-50A throughout the injection
process to evaluate the radius of influence;

•	Record injection pressure, injection rate and injection volumes accepted at each
location;

•	Withdraw the DPI rods at both locations by 5 feet and repeat the injection and
monitoring process;

•	Based on preliminary observations from FAG-50 and FAG-50A determine the
approximate ROI resulting from injecting at DPA-1 and DPA-2;

•	Based on the approximate ROI determination and other field observations and
measurements, slightly adjust locations for DPA-3 and DPA-4 if determined to be
necessary;

•	Advance injection points DPA-3 and DPA-4 and repeat the process for injection as
described above; and

•	Each direct push boring will be grouted full length immediately following removal of
direct push tooling.

Based on a conservatively assumed ROI of 10-15 feet, the estimated total volume of
NaMn04 solution to be injected at Area A is approximately 3,000 gallons.

3.3.2 Area B Injection Plan

FAG-33 through FAG-36 are located within pilot test Area B and are screened at varying
depth intervals within the bedrock depression to be subject to this pilot test. The pilot test
designed for Area B will target the full depth of identified impacted groundwater to include
shallow, intermediate and deep injection intervals.

Field injection procedures to be conducted in Area B include:

•	Initial injections will be conducted simultaneously through the two deep injection
wells IWBD-1 and IWBD-2;

•	Deep well FAG-36 will be monitored throughout the injection process. The other
existing wells in this area will also be monitored for any potential influence from the
injections;

•	Record injection pressure, injection rate and injection volumes accepted at each
location;

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•	Following completion of the deep injections, the procedure will be repeated for the
intermediate screened injection wells IWBI-1 and IWBI-2. Intermediate well FAG-35
will be monitored throughout the injection process and existing wells in this area will
also be monitored for any potential influence from the injections;

•	Advance DPI points DPB-1 and DPB-2 with 5 foot long screens to a total depth of
approximately 55 feet bgs;

•	Inject through DPB-1 and DPB-2 simultaneously;

•	Monitor shallow wells FAG-33 and FAG-34 throughout the injection process. Also
monitor the other existing wells in this area for any potential influence from the
injections;

•	Record injection pressure, injection rate and injection volumes accepted at each
location;

•	Withdraw the DPI rods at both locations by five feet and repeat the injection and
monitoring process; and

•	Each direct push boring will be grouted full length immediately following removal of
direct push tooling.

Based on a conservatively assumed ROI of 10-15 feet, the estimated total volume of
NaMnC>4 solution to be injected in Area B is approximately 7,500 gallons.

3.3.3 Former TCE Pipeline Trench Injection Plan

In addition to the two pilot test areas, focused injections will be completed in the center
portion of the former TCE pipeline trench based on the results of sampling of perched water
collected in 2022 from specific injection wells. Five existing injection wells in the trench (IW-
08 through IW-12) will be utilized to complete tertiary treatment. The injection wells are 2
inches in diameter and and range to a depth of 8.5 to 10 feet bgs within this shallow trench
feature.

Injections will be conducted by simultaneously injecting into outermost wells IW-08 and IW-
12 and then stepping in towards the center of the trench and injecting simultaneously into
wells IW-09 and IW-11 before proceeding to center well IW-10 and injecting into it which
will be the primary focus of this treatment event. Multiple injections were previously
conducted in the trench during full-scale treatment of this source area and it was noted that
particularly during later injection events several wells appeared to have limited capacity to
accept injection volume. Reports describing the injections into the trench indicated this may
have been due in part to mineralization resulting from the early rounds of permanganate
injections. In order to maximize the volume of treatment amendment which may be injected
into these selected wells for this tertiary treatment event, it may be necessary to redevelop
the wells. Redevelopment would include surging and purging each well and noting recovery
rates and the turbidity of water produced during purging. Purging of the wells shortly before
injections would provide the added benefit of allowing additional volume to be injected by

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reducing the volume of perched water in this shallow feature that would need to be
displaced.

It is anticipated that up to approximately 50 gallons of NaMnCU solution will be injected into
each well identified above for a total of 250 gallons. Because of the shallow nature of the
trench, variable density and permeability of the backfill materials and potential historic
latent mineralization from historic injections, the tertiary injections will be conducted at slow
rates to limit potential for daylighting of reagent and to allow the maximum volume of
amendment to be emplaced into the section of trench identified for tertiary treatment.

3.4	WASTE MANAGEMENT

One advantage of in-situ treatment is the minimization of investigative derived waste (IDW)
generated from the remediation process.

For this pilot test, IDW to be generated will consist primarily of a limited amount of soil
cuttings from drilling of the new injection wells and water to be generated from
decontamination of drilling and injection equipment and development/sampling of wells.

The IDW soil will be containerized in labeled 55 gallon steel drums and staged in a central
location at the Site. At the conclusion of drilling activities, the containerized soil will be
sampled for characterization and waste disposal purposes. The IDW water will be
containerized in an onsite poly tank which is used for collection and short-term storage of
water generated from routine RA sampling activities or in labeled 55 gallon steel drums. The
water will be sampled for characterization purposes. If the water meets criteria established
in an existing agreement and procedures with the city of Joplin, the water will be discharged
to the Joplin sanitary sewer following receipt of permission from the city.

3.5	OTHER PLANS RELATED TO FIELD IMPLEMENTATION

The Site Health and Safety Plan (HASP) will be updated prior to the implementation of the
pilot testing and the Sampling and Analysis Plan (SAP) for NCWS will be updated to the
extent necessary to summarize actions not already described for the proposed pilot study.

3.6	GROUNDWATER PARAMETER MONITORING

Monitoring during pilot test field implementation will be conducted by the injection
subcontractor. The subcontractor will monitor injection points and nearby wells over the
course of the injections to gather information related to determining the efficiency and
influence of the injections. This will include collecting depth to water measurements and
collecting samples for visual indicators and colorimetric measurements as part of radius of
influence evaluation. Post-injection monitoring will be conducted by Ramboll.

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3.7 PERFORMANCE MONITORING PLAN

One round of baseline groundwater sampling and up to four rounds of post implementation
groundwater sampling events are proposed to evaluate the performance of ISCO injections
from pilot test Areas A and B. One post implementation sampling event of perched water
from select injection wells in the former TCE pipeline trench will be conducted after it is
determined the chemical oxidant has been largely exhausted.

3.7.1	Baseline Groundwater Sampling Event

Baseline groundwater samples will be collected from wells located in Areas A and B prior to
initiation of the pilot test injections. General baseline conditions in the trench have already
been adequately characterized from the recent sampling event summarized in this report.

In Area A, samples will be collected from two wells; FAG-50 and FAG-50A. In Area B,
samples will be collected from eight wells; FAG-33 through FAG-36, IWBI-1 and IWBI-2 and
IWBD-1 and IWBD-2. Samples will be collected following general procedures provided in the
SAP. All groundwater samples will be analyzed for TCL VOCs (EPA 8620B), manganese (EPA
6010C) and permanganate concentration (via colorimetric methods) and field measured
stabilization parameters to include dissolved oxygen (DO), oxidation-reduction potential
(ORP), pH and conductivity.

3.7.2	Post Injection Groundwater Sampling

Post injection groundwater sampling in Areas A and B will focus on the same wells as the
baseline groundwater sampling event. Three post injection groundwater sampling events
will be conducted at intervals of one, three and six months after the pilot test injections.
After six months, if it appears the emplaced permanganate has generally dissipated, the
pilot test will be considered complete. If it appears the emplaced permanganate remains
active at the six month sampling event, then additional sampling may be conducted at nine
or 12 months post-injection as considered necessary.

One post injection groundwater sampling of IW-10 will be conducted approximately six
months following the pilot test injection. If it appears the emplaced permanganate remains
active at the six month sampling event, then an additional sampling event may be
conducted at nine or 12 months post-injection as considered necessary.

All groundwater samples will be analyzed for TCL VOCs (EPA 8620B), manganese (EPA
6010C) and permanganate concentration (via colorimetric methods). Groundwater results
will be evaluated primarily for trends in any measured concentrations of TCE and TCE
degradation products and also with respect to laboratory and field measured indicator
parameters with regard to destruction of TCE and TCE degradation products.

July 2023

17

CEEEEfll


-------
ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

4. RECORD KEEPING AND REPORTIN<3

4.1	RECORD KEEPING

Ramboll will collect detailed notes for all field tasks including well installations, well
development, field injections and groundwater and perched water sampling.

•	General site conditions will be recorded for all field events.

•	Job safety meetings and briefings will be recorded for all field events.

•	During well installations, the soil cores from the boreholes will be logged to
understand the geological conditions in the vicinity of the injection/monitoring wells
and well construction logs will be completed.

•	During field injection, the subcontractor will provide all the monitoring and inventory
tracking information. Ramboll will also perform independent inventory tracking and
injection conditions recording for quality control.

•	During groundwater sampling, groundwater purging parameters from all wells will be
recorded and filed.

4.2	REPORTING

After obtaining required pilot test data, a summary report will be completed to describe the
testing program completed and the efficacy of the injections and treatment methodologies
that were implemented. Based on the results of the pilot test, additional focused pilot
testing and/or expansion of treatment zones relative to Areas A and B for larger scale
treatment may be proposed.

July 2023

18

CEEEEfll


-------
ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

5. REFERENCES

ENVIRON 2003, Report of Remedial Investigation, Newton County Wells Site, Joplin,

Missouri, ENVIRON International Corporation, St. Peters, Missouri, April 2003.

ENVIRON 2004, Feasibility Study, Newton County Wells Site, Village of Silver Creek and
Village of Saginaw, Newton County, Missouri, September 2004.

The Missouri Department of Natural Resources, 2004, Record of Decision, Newton County
Wells Site, Village of Silver Creek and Village of Saginaw, Newton County, Missouri,
September 2004.

Ramboll 2022, 2022 Annual Report, Remedial Action - Newton County Wells Site, Silver
Creek and Saginaw, Missouri, December 2022.

July 2023

19

CEEEEfll


-------
ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

TABLES

July 2023


-------
TABLE 1

SUMMARY OF FORMER TCE PIPELINE TRENCH PERCHED WATER SAMPLING
DETECTED VOLATILE ORGANIC COMPOUNDS AND LABORATORY MONITORED NATURAL ATTENUATION PARAMETERS

(MAY 2022)

Newton County Wells Site
Villages of Silver Creek and Saginaw, Missouri

Analyte

Units

Injection Wells

Minimum
Detection

Maximum
Detection

Total
Detections

Total
Samples

IW-01

IW-04

IW-10

IW-16

IW-20

Result

Result

Result

Result

Result

Volatile Organic Compounds

1,1-Dichloroethene

mq/l

<1.0

0.56 J

1.1

0.28 J

<1.0

0.28

1.1

3

5

cis-l,2-Dichloroethene

mq/l

1.0

28.6

223

547

<1.0

1.0

547

4

5

trans- 1,2-Dichloroethene

mq/l

<1.0

3.3

8.8

10.3

0.23 J

0.23

10.3

4

5

Trichloroethene

Mg/L

0.75 J

14.4

1,230

2.7

<1.0

0.75

1,230

4

5

Vinyl chloride

Mg/L

0.61 J

26.6

36.4

14.2

<1.0

0.61

36.4

4

5

Monitored Natural Attenuation Parameters (Laboratory)

Nitrate as N

mg/L

<0.10

<0.10

0.11

<0.10

<0.10

0.11

0.11

1

5

Sulfate

mg/L

7.0

14.8

4.2

0.80 J

24.1

0.80

24.1

5

5

Chloride

mg/L

5.3

28.2

17.9

22.0

61.6

5.3

61.6

5

5

Methane

ug/L

14.2

47.6

1,510

<10.0

299

14.2

1,510

4

5

Ethane

ug/L

<10.0

<10.0

7.1 J

<10.0

<10.0

7.1

7.1

1

5

Ethene

Mg/L

<10.0

<10.0

9.0 J

<10.0

<10.0

9.0

9.0

1

5

Iron

Mg/L

26,100

47,700

31,800

2,710

175,000

2,710

175,000

5

5

Notes:

pg/L:	Micrograms per liter

mg/L:	Milligrams per liter

<:	Not detected above the indicated concentration

J:	Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.


-------
ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

FIGURES

July 2023


-------
JOPLIN

Sunnyvale

ROBLIN ST

Gateway Drive

E36TH ST

MOORHEAD PR

KELLER OR

Silver Creek

[SILVER CREEK OR

E44TH ST

Village of \
Silver Creek

APRICOT Dl

WOODLAND OR

I^eawood

I AIL RIDGE DR

naw

REDDING

ARCH LN

Shoal Creek
Estates

Source: 2021 USGS 7.5 Minute Series Jopiin East, Missouri Topographic Quadrangle; Contour Interval 10 Feet.

I \ ~ l _ I ¦..S XV	\ Rnc /



(	^ SITE BOUNDARY BASED ON

1	~ REMEDIAL INVESTIGATION

FIGURE 01

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

SITE LOCATION MAP

KEY MAP

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

Map Scale: 1:24,000 | Map Center: 37"T59.0511",

-94°28'7.2214"


-------
BUILDING B * H

BUILDING C

BUILDING A

WAREHOUSE

|Aerial Imagery Source: Google Maps, dated 6/22/2022.

FORMER TCE TRANSFER PIPELINE TRENCH
O INJECTION WELL

FORMER TCE PIPELINE TRENCH
AND INJECTION WELLS

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER AND
SAGINAW, MISSOURI

FIGURE 02

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY


-------


		

FAG-43 I

Date

Result ug/L |

10/5/1999

180

10/6/2002

110

10/21/2008

338

4/28/2009

275

10/15/2009

438

4/30/2010

330

10/19/2010

395

4/26/2011

313

10/26/2011

289

5/3/2012

1.0 U

10/10/2012

12.2

5/15/2013

1.0 U

10/19/2016

50.6

5/30/2017

1.0 U

10/11/2017

34.9

10/10/2018

1.0 U

9/16/2020

66.4

5/18/2021

1.0 U

5/17/2022

2.3

FAG-56

Date

Result ug/L

10/7/1999

30.0

4/5/2000

10.0

1/8/2002

6.0

5/8/2002

6.0

10/20/2008

8.3

4/28/2009

8.2

10/13/2009

8.2

4/28/2010

12.4

10/20/2010

6.5

4/27/2011

8.0

10/25/2011

8.9

5/1/2012

9.4

10/9/2012

8.6

5/14/2013

9.6

10/18/2016

15.1 J

5/27/2017

9.3

10/8/2017

9.5

10/9/2018

9.6

9/16/2020

5.9

5/18/2021

7.8

5/17/2022

8.9

I MM

v

ram

Result ug/L

FAG-31

Date

Result ug/L

10/6/1999

1,200

10/5/2002

920

10/23/2008

791

5/21/2009

861

10/15/2009

1,070

4/29/2010

719

10/21/2010

653

4/28/2011

698

10/27/2011

698

5/3/2012

698

10/11/2012

705

5/16/2013

724

10/20/2016

765

5/31/2017

719

10/12/2017

735

10/11/2018

934

9/17/2020

705

5/20/2021

733

5/19/2022

726

FAG-32

Date

Result ug/L

10/7/1999

60.0

1/11/2002

58.0

5/8/2002

90.0

10/4/2002

130

10/22/2008

1,730

5/20/2009

1,500

10/13/2009

1,670

4/29/2010

1,630

10/19/2010

1,590

4/28/2011

1,690

10/25/2011

1,620

5/1/2012

1,670

10/9/2012

1,770

5/16/2013

1,380

10/20/2016

1,570

6/1/2017

1,520

10/12/2017

1,780

10/10/2018

1,920

9/16/2020

1.0 U

5/19/2021

183

5/18/2022

49.5

FAG-74

Date

Result ug/L

4/3/2000

10,000

1/9/2002

10,000 E

5/8/2002

10,000 E

10/21/2008

2,720

5/21/2009

3,950

10/14/2009

2,760

4/28/2010

2,560

10/20/2010

1,070

4/28/2011

1,430

10/26/2011

893

5/1/2012

770

10/9/2012

575

5/16/2013

1,120

10/20/2016

200

5/26/2017

789

10/12/2017

101

10/10/2018

123

9/17/2020

37.5

5/21/2021

201

5/19/2022

4.0 J

;

m

f A,



Date

Result ug/L

10/7/1999

510 D

10/21/2008

202

4/28/2009

167

10/15/2009

119

4/29/2010

107

10/19/2010

146

4/26/2011

134

10/27/2011

135

5/3/2012

103

10/10/2012

130

5/14/2013

70.2

10/18/2016

50.6

5/27/2017

47.9

10/11/2017

53.5

10/9/2018

56.9

9/16/2020

39

5/18/2021

27.7

5/18/2022

21.1

	

_

OFAG-05

OUTER R°AD

..FAG-31 -v
FAG-32-0
FAG-22—C



FAG-73

Date

Result ug/L

4/5/2000

2,300

1/9/2002

11,000 E

5/8/2002

20,000 E

10/21/2008

1,130

5/21/2009

429

10/14/2009

358

4/28/2010

387

10/20/2010

514

4/28/2011

73

10/26/2011

82.3

5/1/2012

103

10/10/2012

163

5/16/2013

215

10/19/2016

249

5/31/2017

58.3

10/11/2017

171

10/10/2018

242

9/16/2020

132

5/19/2021

18.8

5/18/2022

22.8





JA-





•

FAG-35

Date

Result ug/L

10/6/1999

640

10/5/2002

620

10/23/2008

484

4/29/2009

510

10/15/2009

542

4/28/2010

602

10/20/2010

446

4/27/2011

583

10/27/2011

499

5/2/2012

436

10/11/2012

467

5/15/2013

429

10/19/2016

516

5/31/2017

432

10/11/2017

543

10/10/2018

597

9/16/2020

512

5/18/2021

488

5/18/2022

537

AG-43!

FAG-56Q

H9I

FAG-73
FAG-74

FAG-AW4 O 1	-1



qfag-1 1



¦¦

,iFAG-34i

nEBE!

¦^^JfFAG-33
FAG-50i

'.'¦i

|Oi

'7Lr*.-	-

nrn- -.	-*•- ~

» • *>•{<. <>U «*• fir *•;/

RI-MV

• i
><

RI-MW9 ORI-MW2

bmmI i m

m.

dated 3/20/2016.

RI-MW1

Date

Result ug/L

10/8/2002

0.53 J

10/22/2008

54.5

4/28/2009

51.4

10/15/2009

36.0 J

4/30/2010

53.2

10/19/2010

78.5

4/26/2011

80.7

10/28/2011

55.1

5/3/2012

41.2

10/10/2012

55.0

5/14/2013

85.1

10/18/2016

52.8

5/25/2017

96.4

10/8/2017

47.4

10/10/2018

99.7

9/15/2020

47.5

5/19/2021

68.3

5/17/2022

57.3







RI-MW2

Date

Result ug/L

10/8/2002

49.0

10/22/2008

1.0 U

4/27/2009

1.0 U

10/15/2009

1.0 U

4/29/2010

1.0 U

10/19/2010

1.0 U

4/26/2011

1.0 U

10/26/2011

1.0 U

5/3/2012

1.0 U

10/10/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 U

5/25/2017

1.0 U

10/8/2017

1.0 U

10/9/2018

1.0 u

9/15/2020

1.0 u

5/18/2021

1.0 u

5/17/2022

<1.0

mr-

FAG-47

Date

Result ug/L

10/5/1999

400

10/6/2002

270

10/21/2008

160

4/29/2009

66.5

10/13/2009

131

4/27/2010

119

10/20/2010

165

4/27/2011

140

10/27/2011

136

5/3/2012

116

10/9/2012

122

5/14/2013

93.4

10/18/2016

76.9

5/27/2017

69.2

10/8/2017

103

10/9/2018

63.3

9/15/2020

97.9

5/18/2021

55.4

5/18/2022

42.7

FAG-34

Date

Result ug/L

10/6/1999

1,200

10/7/2002

1,100

10/22/2008

882

4/29/2009

992

10/14/2009

804 J

4/27/2010

111

10/20/2010

712

4/27/2011

111

10/27/2011

761

5/2/2012

758

10/11/2012

820

5/15/2013

713

10/19/2016

574

5/25/2017

809

10/11/2017

644

10/10/2018

762

9/16/2020

500

5/19/2021

462

5/18/2022

582



FAG-36
FAG-35



».€







FAG-36

Date

Result ug/L

10/6/1999

750

10/7/2002

490

10/22/2008

565

5/20/2009

166

10/16/2009

366

4/28/2010

477

10/21/2010

286

4/27/2011

594

10/27/2011

524

5/3/2012

456

10/11/2012

508

5/15/2013

567

10/20/2016

566

5/31/2017

585

10/11/2017

676

10/10/2018

672

9/16/2020

531

5/19/2021

535

5/18/2022

455

FAG-856

¦ ¦. ¦ .. . . ¦

f 7
t|

¦¦¦

_,FAG-88^45FAG-^

-i i- !

Date

'U&It



*9i

Jkm>

	

Date



" — - —~

MRI-MW5M



RI-MW6

VER

DRIVE

f,;:J fl.lB •'

v	U~-*U



«* .»	• ¦

K Is?	"V

V* '	A-

/¦ •	-• •



— ¦ \r. .

10/6/1999
5/4/2000
10/7/2002
10/21/2008
5/20/2009
12/16/2009
4/28/2010
4/27/2011
10/25/2011
5/3/2012
10/10/2012
5/15/2013
10/20/2016
5/31/2017
10/8/2017
10/11/2017
9/15/2020
5/19/2021
5/19/2022

¦

Result ug/L

Date

Result ug/L

	

10/7/1999
4/4/2000
10/7/2002
10/23/2008
4/29/2009
10/13/2009
4/29/2010
10/20/2010
4/27/2011
10/26/2011
5/1/2012
10/10/2012
5/15/2013
10/19/2016
5/27/2017
10/8/2017
10/11/2018
9/15/2020
5/18/2021
5/17/2022

FAG-33

Date

Result ug/L

10/6/1999

7.0

10/4/2002

15.0

10/20/2008

19.5

4/28/2009

20.5

10/14/2009

20.2

4/27/2010

26.6

10/20/2010

26.1

4/27/2011

29.2

10/27/2011

20.2

5/2/2012

19.7

10/11/2012

17.3

5/14/2013

23.9

10/18/2016

28.1

5/27/2017

31.7

10/8/2017

31.0

10/9/2018

29.6

9/15/2020

28.3

5/18/2021

28.9

5/17/2022

31.7

10/6/2002
10/23/2008
5/20/2009
10/16/2009
4/30/2010
10/19/2010
4/27/2011
10/25/2011
5/2/2012
10/9/2012
5/15/2013
10/19/2016
5/31/2017
10/11/2017
10/11/2018
9/17/2020
5/21/2021
5/19/2022

Result ug/L

*- t./.



11

V j'i I

V ¦ fl
-

{



U • -



500

_J Feet



O	UPPERMOST GROUNDWATER MONITORING WELL

O	MISSISSIPPIAN AQUIFER WELL

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

D	= DILUTED

U	= NOT DETECTED

NS	= NOT SAMPLED; INSUFFICIENT WATER

UPPERMOST GROUNDWATER
ANALYTICAL RESULTS
TRICHLOROETHENE (TCE) 1999 TO 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 03

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EEEEfll


-------
PROJECT: 1690004605 DATED: 3/28/2023 DESIGNER: CKL/ELS

L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2023\04_Spr Wtr & Miss Aq Analytical Results-TCE.dwg

10/21/2008

4/29/2009

4/29/2009

10/15/2009

10/15/2009

4/29/2010

4/28/2010

10/21/2010

10/21/2010

4/28/2011

4/27/2011

10/27/2011

10/26/2011

5/3/2012

5/2/2012

10/11/2012

10/10/2012

5/16/2013

5/15/2013

10/20/2016

10/19/2016

5/31/2017

5/31/2017

10/12/2017

10/12/2017

10/11/2018

10/11/2018

9/17/2020

9/16/2020

5/19/2021

5/19/2021

5/18/2022

5/18/2022



Result ug/L

Result ug/L

10/16/2002

3/1/1999

10/21/2008

10/6/2002

4/28/2009

10/23/2008

10/14/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/27/2010

5/5/2011

10/19/2010

10/26/2011

5/5/2011

5/2/2012

10/26/2011

10/10/2012

5/3/2012

5/15/2013

10/10/2012

10/19/2016

5/14/2013

5/30/2017

10/19/2016

10/12/2017

5/30/2017

10/10/2018

10/11/2017

9/17/2020

10/10/2018

5/20/2021

9/16/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/16/2002

Result ug/L

10/20/2008

10/16/2002

4/28/2009

10/22/2008

10/13/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/28/2010

5/5/2011

10/20/2010

10/25/2011

4/26/2011

5/2/2012

10/26/2011

10/9/2012

5/2/2012

5/14/2013

10/10/2012

10/18/2016

5/14/2013

5/24/2017

10/18/2016

10/11/2017

5/25/2017

10/11/2018

10/8/2017

9/16/2020

10/10/2018

5/19/2021

9/18/2020

5/19/2022

RI-MW7

5/19/2021

5/18/2022

Result ug/L

10/15/2002

Result ug/L

10/21/2008

10/16/2002

4/28/2009

10/21/2008

10/13/2009

4/28/2009

4/27/2010

10/13/2009

10/20/2010

4/27/2010

4/26/2011

10/20/2010

10/25/2011

4/26/2011

5/1/2012

10/25/2011

10/9/2012

5/1/2012

5/15/2013

10/9/2012

10/19/2016

5/14/2013

5/30/2017

10/18/2016

10/11/2017

5/25/2017

10/9/2018

10/8/2017

9/16/2020

10/9/2018

5/18/2021

9/15/2020

5/17/2022

5/18/2021

5/17/2022

Result ug/L

10/15/2002

10/21/2008

Result ug/L

4/29/2009

6/7/1999

10/14/2009

1/1/2002

4/28/2010

3/1/2002

10/20/2010

Result ug/L

5/1/2002

4/27/2011

4/29/1993

7/1/2002

10/26/2011

6/1/1995

9/1/2002

5/2/2012

4/9/1999

11/1/2002

10/10/2012

10/23/2008

10/23/2008

5/15/2013

4/30/2009

4/30/2009

10/19/2016

10/16/2009

10/16/2009

5/30/2017

4/29/2010

4/29/2010

10/11/2017

10/20/2010

10/20/2010

10/9/2018

4/28/2011

4/28/2011

9/15/2020

10/25/2011

10/25/2011

5/18/2021

5/4/2012

5/4/2012

5/17/2022

10/10/2012

10/10/2012

5/15/2013

5/15/2013

10/20/2016

10/20/2016

5/31/2017

5/31/2017

10/11/2017

10/11/2017

10/11/2018

10/11/2018

9/17/2020

9/17/2020

5/20/2021

5/20/2021

5/19/2022

5/19/2022

RW-341A

|Aerial Imagery Source: Google Earth , dated 3/20/2016.

Date

10/14/2002
10/20/2008
4/27/2009
10/13/2009
j 4/26/2010

•	10/19/2010
4/26/2011

*	10/25/2011
! 5/1/2012

10/9/2012
5/14/2013
, 10/18/2016
j 5/25/2017
10/8/2017
10/9/2018
! 9/15/2020
5/18/2021
| 5/17/2022

Result ug/L

O	SURFACE WATER

O	UPPERMOST GROUNDWATER

O	MISSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EaSEsfll

SPRING WATER AND MISSISSIPPIAN
AQUIFER ANALYTICAL RESULTS
TRICHLOROETHENE (TCE) -1999 TO 2022

FIGURE 04

D = DILUTED
U = NOT DETECTED
NS = NOT SAMPLED; INSUFFICIENT WATER

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI


-------
TOP OF BEDROCK CONTOUR
(FEET ABOVE MEAN SEA LEVEL)

		I FORMER TRANSFER PIPELINE TRENCH

TOP OF BEDROCK CONTOUR MAP

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 05

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY


-------
[Aerial Imagery Source: Google Maps, dated 6/22/2022.

APPROXIMATE PILOT TEST INJECTION AREA
FORMER TCE TRANSFER PIPELINE TRENCH
O UPPERMOST GROUNDWATER
O MISSISSIPPI AQUIFER

LOCATIONS OF PROPOSED
PILOT TEST AREAS

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER AND
SAGINAW, MISSOURI

FIGURE 06

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY


-------
DRMO. ' cQDPA-2
O FAG-50

ij '

©FAG-50A

T'Q:°DPr

[Aerial Imagery Source: Google Maps, dated 9/26/2021

	TOP OF BEDROCK CONTOURS (FEET ABOVE MEAN SEA LEVEL)

O UPPERMOST GROUNDWATER MONITORING WELL

O APPROXIMATE LOCATIONS OF PROPOSED DIRECT PUSH
INJECTION LOCATION

0' APPROXIMATE LOCATION OF PROPOSED NEW MONITORING
WELL FAG-50A

PROPOSED PILOT TEST AREA A

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 07

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
r r-C1 \

\{0\

I Vtvi v

¦Aenaflmagery Source: Google Maps, dated 9/26/202O

—
/ ' /

w+t 'RT**-

•aWkSs' & HBBH
t, SH : * ,

¦ M I

L \

V

H J

i

.*



I

DF'B-1

„*

IWB-1

I \FAG-36 O ^ FAG-33

\ \tv \ \ v ¦ ° I

FAG-35 oOf^0",3^

DPB-2

INJECTION AREA DETAIL

	TOP OF BEDROCK CONTOURS (FEET ABOVE MEAN SEA LEVEL)

O UPPERMOST GROUNDWATER MONITORING WELL

O MISSISSIPPI AQUIFER WELL

O APPROXIMATE LOCATIONS OF PROPOSED DIRECT PUSH
INJECTION LOCATION

A INJECTION WELL

PROPOSED PILOT TEST AREA B

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 08

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
ISCO Pilot Study Work Plan - FAG Bearings
Remedial Action - NCWS
Silver Creek and Saginaw, Missouri

Focused 2022 Trench Sampling Analytical Report


-------
Face Analytical "

WHW.pceIabs.com

Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

June 06, 2022

Mr. Doug Burge
Ramboll

1807 Park 270 Drive
Suite 450

Saint Louis, MO 63146

RE: Project: NCWS(LISTA)

Pace Project No.: 60400847

Dear Mr. Burge:

Enclosed are the analytical results for sample(s) received by the laboratory on May 20, 2022. The results relate only to the
samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.

The test results provided in this final report were generated by each of the following laboratories within the Pace Network:

•	Pace Analytical Services - Indianapolis

•	Pace Analytical Services - Kansas City

If you have any questions concerning this report, please feel free to contact me.

Sincerely,

Jamie Church

jamie.church@pacelabs.com

314-838-7223

Project Manager

Enclosures

cc: Ian McQuaig, Ramboll US Consulting, Inc.



REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 1 of 31


-------
iceAnalytical

www.paceIibs.eom

CERTIFICATIONS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Pace Analytical Services Indianapolis

7726 Moller Road, Indianapolis, IN 46268
Illinois Accreditation #: 200074
Indiana Drinking Water Laboratory #: C-49-06
Kansas/TNI Certification #: E-10177
Kentucky UST Agency Interest #: 80226
Kentucky WW Laboratory ID #: 98019

Michigan Drinking Water Laboratory #9050
Ohio VAP Certified Laboratory #: CL0065
Oklahoma Laboratory #: 9204
Texas Certification #: T104704355
Wisconsin Laboratory #: 999788130
USDASoil Permit#: P330-19-00257

Pace Analytical Services Kansas

9608 Loiret Boulevard, Lenexa, KS 66219

Missouri Inorganic Drinking Water Certification #: 10090

Arkansas Drinking Water

Arkansas Certification #: 20-020-0

Arkansas Drinking Water

Illinois Certification #: 2000302021-3

Iowa Certification #: 118

Kansas/NELAP Certification #: E-10116

Louisiana Certification #: 03055

Nevada Certification #: KS000212020-2

Oklahoma Certification #: 9205/9935

Florida: Cert E871149 SEKS WET

Texas Certification #: T104704407-21-15

Utah Certification #: KS000212019-9

Illinois Certification #: 004592

Kansas Field Laboratory Accreditation: # E-92587

Missouri SEKS Micro Certification: 10070

Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 2 of 31


-------
Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

SAMPLE SUMMARY

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Lab ID	Sample ID	Matrix	Date Collected Date Received

60400847001

IW-16-W-17

Water

05/19/22

13:43

05/20/22 08:50

60400847002

IW-20-W-17

Water

05/19/22

14:10

05/20/22 08:50

60400847003

IW-04-W-17

Water

05/19/22

15:12

05/20/22 08:50

60400847004

IW-10-W-17

Water

05/19/22

14:36

05/20/22 08:50

60400847005

IW-01-W-17

Water

05/19/22

16:02

05/20/22 08:50

60400847006

TB-03-051922

Water

05/19/22

17:30

05/20/22 08:50

^Analytical

www.pacelibs.eom

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 3 of 31


-------
iceAnalytical

www.pacdiln.cani

Pace Analytical Services, LLC
9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

Project:

Pace Project No

NCWS (LIST A)
i.: 60400847

SAMPLE ANALYTE COUNT







Lab ID

Sample ID

Method

Analysts

Analytes
Reported

Laboratory

60400847001

IW-16-W-17

RSK175 Modified

DAP

3

PASI-I





EPA 6010

MA1

1

PASI-K





EPA 5030B/8260

CSC

69

PASI-K





EPA 300.0

CRN2

2

PASI-K





EPA 353.2

CRN2

1

PASI-K

60400847002

IW-20-W-17

RSK175 Modified

DAP

3

PASI-I





EPA 6010

MA1

1

PASI-K





EPA 5030B/8260

CSC

69

PASI-K





EPA 300.0

CRN2

2

PASI-K





EPA 353.2

CRN2

1

PASI-K

60400847003

IW-04-W-17

RSK175 Modified

DAP

3

PASI-I





EPA 6010

MA1

1

PASI-K





EPA 5030B/8260

CSC

69

PASI-K





EPA 300.0

CRN2

2

PASI-K





EPA 353.2

CRN2

1

PASI-K

60400847004

IW-10-W-17

RSK175 Modified

DAP

3

PASI-I





EPA 6010

MA1

1

PASI-K





EPA 5030B/8260

CSC

69

PASI-K





EPA 300.0

CRN2

2

PASI-K





EPA 353.2

CRN2

1

PASI-K

60400847005

IW-01-W-17

RSK175 Modified

DAP

3

PASI-I





EPA 6010

MA1

1

PASI-K





EPA 5030B/8260

CSC

69

PASI-K





EPA 300.0

CRN2

2

PASI-K





EPA 353.2

CRN2

1

PASI-K

60400847006

TB-03-051922

EPA 5030B/8260

CSC

69

PASI-K

PASI-I = Pace Analytical Services - Indianapolis
PASI-K = Pace Analytical Services - Kansas City

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 4 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-16-W-17

Lab ID:

60400847001 Collected:

05/19/22 13:43

Received: 05/20/22 08:50

Matrix: Water







Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/24/22 20:04

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/24/22 20:04

74-85-1

Methane

2080

ug/L

10.0

5.5

1



05/24/22 20:04

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

: EPA 3010









Pace Analytical Services - Kansas City













Iron

2710

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:51

7439-89-6

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City













Acetone

5.7J

ug/L

10.0

2.5

1



06/01/22 08

13

67-64-1

Benzene

0.40J

ug/L

1.0

0.14

1



06/01/22 08

13

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



06/01/22 08

13

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



06/01/22 08

13

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



06/01/22 08

13

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



06/01/22 08

13

75-25-2

Bromomethane

0.54J

ug/L

5.0

0.46

1



06/01/22 08

13

74-83-9 B

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



06/01/22 08

13

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



06/01/22 08

13

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



06/01/22 08

13

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 08

13

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



06/01/22 08

13

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



06/01/22 08

13

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



06/01/22 08

13

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



06/01/22 08

13

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



06/01/22 08

13

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



06/01/22 08

13

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



06/01/22 08

13

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



06/01/22 08

13

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



06/01/22 08

13

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



06/01/22 08

13

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



06/01/22 08

13

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



06/01/22 08

13

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



06/01/22 08

13

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 08

13

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 08

13

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



06/01/22 08

13

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



06/01/22 08

13

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



06/01/22 08

13

107-06-2

1,2-Dichloroethene (Total)

557

ug/L

20.0

4.4

20



06/01/22 21

08

540-59-0

1,1-Dichloroethene

0.28J

ug/L

1.0

0.22

1



06/01/22 08

13

75-35-4

cis-1,2-Dichloroethene

547

ug/L

20.0

2.6

20



06/01/22 21

08

156-59-2

trans-1,2-Dichloroethene

10.3

ug/L

1.0

0.10

1



06/01/22 08

13

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



06/01/22 08

13

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



06/01/22 08

13

142-28-9

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 5 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-16-W-17

Parameters

Lab ID: 60400847001 Collected: 05/19/22 13:43 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

06/01/22 08

13

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

06/01/22 08

13

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

06/01/22 08

13

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

06/01/22 08

13

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 08

13

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

06/01/22 08

13

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

06/01/22 08

13

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

06/01/22 08

13

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

06/01/22 08

13

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

06/01/22 08

13

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1

06/01/22 08

13

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1

06/01/22 08

13

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1

06/01/22 08

13

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 08

13

103-65-1

Styrene

ND

ug/L

1.0

0.12 1

06/01/22 08

13

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1

06/01/22 08

13

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1

06/01/22 08

13

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1

06/01/22 08

13

127-18-4

Toluene

0.26J

ug/L

1.0

0.25 1

06/01/22 08

13

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1

06/01/22 08

13

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1

06/01/22 08

13

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1

06/01/22 08

13

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1

06/01/22 08

13

79-00-5

Trichloroethene

2.7

ug/L

1.0

0.21 1

06/01/22 08

13

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1

06/01/22 08

13

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1

06/01/22 08

13

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1

06/01/22 08

13

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1

06/01/22 08

13

108-67-8

Vinyl chloride

14.2

ug/L

1.0

0.17 1

06/01/22 08

13

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1

06/01/22 08

13

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

100

%

80-120

1

06/01/22 08

13

460-00-4

Toluene-d8 (S)

99

%

80-120

1

06/01/22 08

13

2037-26-5

1,2-Dichlorobenzene-d4 (S)

101

%

80-120

1

06/01/22 08

13

2199-69-1

Preservation pH

1.0



0.10

1

06/01/22 08

13



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0











Pace Analytical Services -

Kansas City









Chloride

22.0

mg/L

10.0

5.3 10

05/27/22 17:00

16887-00-6

Sulfate

0.80J

mg/L

1.0

0.55 1

05/28/22 10:23

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

ND mg/L	0.10 0.079

05/21/22 10:28 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 6 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-20-W-17

Lab ID:

60400847002 Collected:

05/19/22 14:10

Received: 05/20/22 08:50 Matrix: Water









Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8 1



05/24/22 20:25

74-84-0



Ethene

ND

ug/L

10.0

7.1 1



05/24/22 20:25

74-85-1



Methane

299

ug/L

10.0

5.5 1



05/24/22 20:25

74-82-8



6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method: EPA 3010









Pace Analytical Services - Kansas City











Iron

175000

ug/L

50.0

5.6 1

05/23/22 13:10

05/25/22 12:53

7439-89-6



8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City











Acetone

3.4J

ug/L

10.0

2.5 1



06/01/22 07:58

67-64-1



Benzene

ND

ug/L

1.0

0.14 1



06/01/22 07:58

71-43-2



Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22 07:58

108-86-1



Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22 07:58

74-97-5



Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22 07:58

75-27-4



Bromoform

ND

ug/L

1.0

0.68 1



06/01/22 07:58

75-25-2



Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22 07:58

74-83-9



2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22 07:58

78-93-3



n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22 07:58

104-51-8



sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22 07:58

135-98-8



tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 07:58

98-06-6



Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22 07:58

75-15-0



Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22 07:58

56-23-5



Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22 07:58

108-90-7



Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22 07:58

75-00-3



Chloroform

ND

ug/L

1.0

0.22 1



06/01/22 07:58

67-66-3



Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22 07:58

74-87-3



2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22 07:58

95-49-8



4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22 07:58

106-43-4



1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22 07:58

96-12-8



Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22 07:58

124-48-1



1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22 07:58

106-93-4



Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22 07:58

74-95-3



1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22 07:58

95-50-1



1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07:58

541 -73-1



1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07:58

106-46-7



Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22 07:58

75-71-8



1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22 07:58

75-34-3



1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22 07:58

107-06-2



1,2-Dichloroethene (Total)

0.23J

ug/L

1.0

0.22 1



06/01/22 21:23

540-59-0



1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22 07:58

75-35-4



cis-1,2-Dichloroethene

0.23J

ug/L

1.0

0.13 1



06/01/22 21:23

156-59-2



trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22 21:23

156-60-5



1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22 07:58

78-87-5



1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22 07:58

142-28-9



REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 7 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-20-W-17

Lab ID:

60400847002

Collected:

05/19/22 14:10

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



06/01/22 07:58

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



06/01/22 07:58

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



06/01/22 07:58

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



06/01/22 07:58

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:58

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



06/01/22 07:58

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



06/01/22 07:58

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



06/01/22 07:58

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



06/01/22 07:58

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



06/01/22 07:58

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



06/01/22 07:58

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



06/01/22 07:58

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



06/01/22 07:58

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:58

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



06/01/22 07:58

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



06/01/22 07:58

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



06/01/22 07:58

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



06/01/22 07:58

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



06/01/22 07:58

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



06/01/22 07:58

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



06/01/22 07:58

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



06/01/22 07:58

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



06/01/22 07:58

79-00-5

Trichloroethene

ND

ug/L

1.0

0.21

1



06/01/22 21:23

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



06/01/22 07:58

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



06/01/22 07:58

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



06/01/22 07:58

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



06/01/22 07:58

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17

1



06/01/22 07:58

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



06/01/22 07:58

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

100

%

80-120



1



06/01/22 07:58

460-00-4

Toluene-d8 (S)

99

%

80-120



1



06/01/22 07:58

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

%

80-120



1



06/01/22 07:58

2199-69-1

Preservation pH

1.0



0.10



1



06/01/22 07:58



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

61.6

mg/L

10.0

5.3

10



05/27/22 17:28

16887-00-6

Sulfate

24.1

mg/L

10.0

5.5

10



05/27/22 17:28

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

ND

mg/L

0.10

0.079

1



05/21/22 10:30

14797-55-8

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 8 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-04-W-17

Lab ID:

60400847003 Collected:

05/19/22 15:12

Received: 05/20/22 08:50 Matrix: Water







Report









Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

RSK 175 Headspace

Analytical Method:

RSK 175 Modified











Pace Analytical Services - Indianapolis









Ethane

ND

ug/L

10.0

3.8 1



05/24/22 20:46

74-84-0

Ethene

ND

ug/L

10.0

7.1 1



05/24/22 20:46

74-85-1

Methane

47.6

ug/L

10.0

5.5 1



05/24/22 20:46

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method: EPA 3010







Pace Analytical Services - Kansas City









Iron

47700

ug/L

50.0

5.6 1

05/23/22 13:10

05/25/22 12:55

7439-89-6

8260 MSV

Analytical Method:

EPA 5030B/8260











Pace Analytical Services - Kansas City









Acetone

3.1J

ug/L

10.0

2.5 1



06/01/22 07:44

67-64-1

Benzene

0.35J

ug/L

1.0

0.14 1



06/01/22 07:44

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22 07:44

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22 07:44

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22 07:44

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22 07:44

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22 07:44

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22 07:44

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22 07:44

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22 07:44

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 07:44

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22 07:44

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22 07:44

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22 07:44

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22 07:44

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22 07:44

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22 07:44

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22 07:44

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22 07:44

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22 07:44

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22 07:44

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22 07:44

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22 07:44

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22 07:44

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07:44

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07:44

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22 07:44

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22 07:44

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22 07:44

107-06-2

1,2-Dichloroethene (Total)

32.0

ug/L

1.0

0.22 1



06/01/22 21:38

540-59-0

1,1-Dichloroethene

0.56J

ug/L

1.0

0.22 1



06/01/22 07:44

75-35-4

cis-1,2-Dichloroethene

28.6

ug/L

1.0

0.13 1



06/01/22 21:38

156-59-2

trans-1,2-Dichloroethene

3.3

ug/L

1.0

0.10 1



06/01/22 21:38

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22 07:44

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22 07:44

142-28-9

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 9 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-04-W-17

Lab ID:

60400847003

Collected:

05/19/22 15:12

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



06/01/22 07:44

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



06/01/22 07:44

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



06/01/22 07:44

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



06/01/22 07:44

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:44

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



06/01/22 07:44

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



06/01/22 07:44

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



06/01/22 07:44

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



06/01/22 07:44

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



06/01/22 07:44

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



06/01/22 07:44

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



06/01/22 07:44

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



06/01/22 07:44

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:44

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



06/01/22 07:44

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



06/01/22 07:44

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



06/01/22 07:44

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



06/01/22 07:44

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



06/01/22 07:44

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



06/01/22 07:44

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



06/01/22 07:44

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



06/01/22 07:44

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



06/01/22 07:44

79-00-5

Trichloroethene

14.4

ug/L

1.0

0.21

1



06/01/22 21:38

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



06/01/22 07:44

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



06/01/22 07:44

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



06/01/22 07:44

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



06/01/22 07:44

108-67-8

Vinyl chloride

26.6

ug/L

1.0

0.17

1



06/01/22 07:44

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



06/01/22 07:44

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

99

%

80-120



1



06/01/22 07:44

460-00-4

Toluene-d8 (S)

99

%

80-120



1



06/01/22 07:44

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

%

80-120



1



06/01/22 07:44

2199-69-1

Preservation pH

1.0



0.10



1



06/01/22 07:44



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

28.2

mg/L

10.0

5.3

10



05/28/22 10:37

16887-00-6 B

Sulfate

14.8

mg/L

10.0

5.5

10



05/28/22 10:37

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

ND

mg/L

0.10

0.079

1



05/21/22 10:34

14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 10 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-10-W-17

Lab ID: 60400847004 Collected: 05/19/22 14:36 Received: 05/20/22 08:50 Matrix: Water
Report

Parameters

Results

Units

Limit

VIDL

DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

7.1J

ug/L

10.0

3.8

1



05/24/22 21:08

74-84-0

Ethene

9.0J

ug/L

10.0

7.1

1



05/24/22 21:08

74-85-1

Methane

1510

ug/L

10.0

5.5

1



05/24/22 21:08

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method: EPA 3010







Pace Analytical Services - Kansas City











Iron

31800

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:57

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City











Acetone

3.1J

ug/L

10.0

2.5

1



06/01/22 07:29

67-64-1

Benzene

0.20J

ug/L

1.0

0.14

1



06/01/22 07:29

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



06/01/22 07:29

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



06/01/22 07:29

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



06/01/22 07:29

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



06/01/22 07:29

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



06/01/22 07:29

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



06/01/22 07:29

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



06/01/22 07:29

104-51-8

sec-Butylbenzene

0.20J

ug/L

1.0

0.11

1



06/01/22 07:29

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:29

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



06/01/22 07:29

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



06/01/22 07:29

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



06/01/22 07:29

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



06/01/22 07:29

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



06/01/22 07:29

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



06/01/22 07:29

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



06/01/22 07:29

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



06/01/22 07:29

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



06/01/22 07:29

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



06/01/22 07:29

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



06/01/22 07:29

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



06/01/22 07:29

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:29

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 07:29

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 07:29

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



06/01/22 07:29

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



06/01/22 07:29

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



06/01/22 07:29

107-06-2

1,2-Dichloroethene (Total)

232

ug/L

100

22.2

100



06/01/22 21:52

540-59-0

1,1-Dichloroethene

1.1

ug/L

1.0

0.22

1



06/01/22 07:29

75-35-4

cis-1,2-Dichloroethene

223

ug/L

100

12.9

100



06/01/22 21:52

156-59-2

trans-1,2-Dichloroethene

8.8

ug/L

1.0

0.10

1



06/01/22 07:29

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



06/01/22 07:29

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



06/01/22 07:29

142-28-9

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.	Page 11 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-10-W-17

Lab ID:

60400847004

Collected:

05/19/22 14:36

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



06/01/22 07:29

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



06/01/22 07:29

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



06/01/22 07:29

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



06/01/22 07:29

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:29

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



06/01/22 07:29

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



06/01/22 07:29

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



06/01/22 07:29

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



06/01/22 07:29

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



06/01/22 07:29

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



06/01/22 07:29

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



06/01/22 07:29

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



06/01/22 07:29

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 07:29

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



06/01/22 07:29

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



06/01/22 07:29

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



06/01/22 07:29

79-34-5

Tetrachloroethene

0.79J

ug/L

1.0

0.33

1



06/01/22 07:29

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



06/01/22 07:29

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



06/01/22 07:29

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



06/01/22 07:29

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



06/01/22 07:29

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



06/01/22 07:29

79-00-5

Trichloroethene

1230

ug/L

100

21.0

100



06/01/22 21:52

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



06/01/22 07:29

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



06/01/22 07:29

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



06/01/22 07:29

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



06/01/22 07:29

108-67-8

Vinyl chloride

36.4

ug/L

1.0

0.17

1



06/01/22 07:29

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



06/01/22 07:29

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

99

%

80-120



1



06/01/22 07:29

460-00-4

Toluene-d8 (S)

99

%

80-120



1



06/01/22 07:29

2037-26-5

1,2-Dichlorobenzene-d4 (S)

99

%

80-120



1



06/01/22 07:29

2199-69-1

Preservation pH

1.0



0.10



1



06/01/22 07:29



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

17.9

mg/L

1.0

0.53

1



05/28/22 10:51

16887-00-6

Sulfate

4.2

mg/L

1.0

0.55

1



05/28/22 10:51

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

0.11

mg/L

0.10

0.079

1



05/21/22 10:31

14797-55-8

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 12 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-01-W-17

Lab ID:

60400847005 Collected:

05/19/22 16:02

Received: 05/20/22 08:50

Matrix: Wate







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8 1



05/24/22 21:29

74-84-0

Ethene

ND

ug/L

10.0

7.1 1



05/24/22 21:29

74-85-1

Methane

14.2

ug/L

10.0

5.5 1



05/24/22 21:29

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method: EPA 3010









Pace Analytical Services - Kansas City











Iron

26100

ug/L

50.0

5.6 1

05/23/22 13:10

05/25/22 12:59

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City











Acetone

5.1J

ug/L

10.0

2.5 1



06/01/22 07

14

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22 07

14

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22 07

14

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22 07

14

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22 07

14

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22 07

14

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22 07

14

74-83-9

2-Butanone (MEK)

1.1J

ug/L

10.0

0.98 1



06/01/22 07

14

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22 07

14

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22 07

14

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 07

14

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22 07

14

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22 07

14

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22 07

14

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22 07

14

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22 07

14

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22 07

14

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22 07

14

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22 07

14

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22 07

14

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22 07

14

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22 07

14

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22 07

14

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22 07

14

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07

14

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 07

14

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22 07

14

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22 07

14

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22 07

14

107-06-2

1,2-Dichloroethene (Total)

1.0

ug/L

1.0

0.22 1



06/01/22 07

14

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22 07

14

75-35-4

cis-1,2-Dichloroethene

1.0

ug/L

1.0

0.13 1



06/01/22 07

14

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22 07

14

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22 07

14

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22 07

14

142-28-9

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 13 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: IW-01-W-17

Parameters

Lab ID: 60400847005 Collected: 05/19/22 16:02 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

06/01/22 07

14

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

06/01/22 07

14

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

06/01/22 07

14

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

06/01/22 07

14

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 07

14

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

06/01/22 07

14

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

06/01/22 07

14

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

06/01/22 07

14

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

06/01/22 07

14

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

06/01/22 07

14

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1

06/01/22 07

14

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1

06/01/22 07

14

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1

06/01/22 07

14

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 07

14

103-65-1

Styrene

ND

ug/L

1.0

0.12 1

06/01/22 07

14

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1

06/01/22 07

14

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1

06/01/22 07

14

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1

06/01/22 07

14

127-18-4

Toluene

ND

ug/L

1.0

0.25 1

06/01/22 07

14

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1

06/01/22 07

14

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1

06/01/22 07

14

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1

06/01/22 07

14

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1

06/01/22 07

14

79-00-5

Trichloroethene

0.75J

ug/L

1.0

0.21 1

06/01/22 07

14

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1

06/01/22 07

14

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1

06/01/22 07

14

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1

06/01/22 07

14

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1

06/01/22 07

14

108-67-8

Vinyl chloride

0.61J

ug/L

1.0

0.17 1

06/01/22 07

14

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1

06/01/22 07

14

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

100

%

80-120

1

06/01/22 07

14

460-00-4

Toluene-d8 (S)

99

%

80-120

1

06/01/22 07

14

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

%

80-120

1

06/01/22 07

14

2199-69-1

Preservation pH

1.0



0.10

1

06/01/22 07

14



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0











Pace Analytical Services -

Kansas City









Chloride

5.3

mg/L

1.0

0.53 1

05/28/22 11

19

16887-00-6

Sulfate

7.0

mg/L

1.0

0.55 1

05/28/22 11

19

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

ND mg/L	0.10 0.079

05/21/22 10:35 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 14 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: TB-03-051922

Lab ID:

60400847006

Collected:

05/19/22 17:30

Received: 05/20/22 08:50 Matrix: Water







Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City







Acetone

ND

ug/L

10.0

2.5 1

06/01/22 07:00

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

06/01/22 07:00

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

06/01/22 07:00

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

06/01/22 07:00

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

06/01/22 07:00

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

06/01/22 07:00

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

06/01/22 07:00

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

06/01/22 07:00

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

06/01/22 07:00

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

06/01/22 07:00

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 07:00

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

06/01/22 07:00

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

06/01/22 07:00

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

06/01/22 07:00

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

06/01/22 07:00

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

06/01/22 07:00

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

06/01/22 07:00

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

06/01/22 07:00

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

06/01/22 07:00

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

06/01/22 07:00

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

06/01/22 07:00

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

06/01/22 07:00

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

06/01/22 07:00

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

06/01/22 07:00

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

06/01/22 07:00

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

06/01/22 07:00

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

06/01/22 07:00

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

06/01/22 07:00

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

06/01/22 07:00

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1

06/01/22 07:00

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

06/01/22 07:00

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1

06/01/22 07:00

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

06/01/22 07:00

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

06/01/22 07:00

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

06/01/22 07:00

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

06/01/22 07:00

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

06/01/22 07:00

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

06/01/22 07:00

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

06/01/22 07:00

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

06/01/22 07:00

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

06/01/22 07:00

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

06/01/22 07:00

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

06/01/22 07:00

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

06/01/22 07:00

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

06/01/22 07:00

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 15 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400847

Sample: TB-03-051922

Lab ID:

60400847006

Collected:

05/19/22 17:30

Received:

05/20/22 08:50 Matrix: Water







Report









Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City









4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1



06/01/22 07:00

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



06/01/22 07:00

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



06/01/22 07:00

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 07:00

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



06/01/22 07:00

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22 07:00

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22 07:00

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22 07:00

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



06/01/22 07:00

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22 07:00

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22 07:00

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22 07:00

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22 07:00

79-00-5

Trichloroethene

ND

ug/L

1.0

0.21 1



06/01/22 07:00

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22 07:00

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22 07:00

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22 07:00

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22 07:00

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22 07:00

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22 07:00

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

99

%

80-120

1



06/01/22 07:00

460-00-4

Toluene-d8 (S)

99

%

80-120

1



06/01/22 07:00

2037-26-5

1,2-Dichlorobenzene-d4 (S)

103

%

80-120

1



06/01/22 07:00

2199-69-1

Preservation pH

1.0



0.10

1



06/01/22 07:00



Qual

Date: 06/06/2022 02:06 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 16 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:	677764	Analysis Method:	RSK175 Modified

QC Batch Method: RSK 175 Modified	Analysis Description: RSK 175 HEADSPACE

Laboratory:	Pace Analytical Services - Indianapolis

60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Associated Lab Samples:

METHOD BLANK: 3120790	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

Qualifiers

Ethane
Ethene
Methane

ug/L
ug/L
ug/L

ND
ND
ND

10.0
10.0
10.0

3.8
7.1
5.5

05/24/22 15:51
05/24/22 15:51
05/24/22 15:51

LABORATORY CONTROL SAMPLE: 3120791

Spike	LCS	LCS % Rec

Parameter Units Cone.	Result	% Rec Limits	Qualifiers

Ethane ug/L 1980	2060	104 77-136

Ethene ug/L 2250	2300	102 79-136

Methane ug/L 1980	1950	98 69-125

SAMPLE DUPLICATE: 3121431

50317161001	Dup	Max

Parameter

Units

Result

Result

RPD

RPD Qualifiers

Ethane

ug/L

ND

8.0J



20

Ethene

ug/L

ND

ND



20

Methane

ug/L

4050

3930

3

20

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

Date: 06/06/2022 02:06 PM	without the written consent of Pace Analytical Services, LLC.	Page 17 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:	788176	Analysis Method:	EPA 6010

QC Batch Method: EPA 3010	Analysis Description: 6010 MET

Laboratory:	Pace Analytical Services - Kansas City

60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Associated Lab Samples:

METHOD BLANK: 3141894	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

Qualifiers

Iron

ug/L

7.4J

50.0

5.6 05/25/22 12:27

LABORATORY CONTROL SAMPLE: 3141895

Spike	LCS	LCS	% Rec

Parameter	Units	Cone.	Result	% Rec	Limits	Qualifiers

Iron	ug/L	10000	9340	93	80-120

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3141896	3141897

MS	MSD

60400877003 Spike	Spike MS MSD MS MSD % Rec	Max

Parameter	Units Result Cone.	Cone.	Result Result % Rec % Rec Limits RPD RPD Qual

Iron	ug/L	9650 10000 10000 18200 17900	85	83 75-125 1 20

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 18 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:	789769	Analysis Method:	EPA 5030B/8260

QC Batch Method: EPA5030B/8260	Analysis Description: 8260 MSV Water 10 mL Purge

Laboratory:	Pace Analytical Services - Kansas City

60400847001, 60400847002, 60400847003, 60400847004, 60400847005, 60400847006

Associated Lab Samples:

METHOD BLANK: 3147760	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005, 60400847006

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

1,1,1,2-Tetrachloroethane

ug/L

ND

1.0

0.084

06/01/22 06:30

1,1,1-Trichloroethane

ug/L

ND

1.0

0.11

06/01/22 06:30

1,1,2,2-Tetrachloroethane

ug/L

ND

1.0

0.15

06/01/22 06:30

1,1,2-Trichloroethane

ug/L

ND

1.0

0.14

06/01/22 06:30

1,1-Dichloroethane

ug/L

ND

1.0

0.12

06/01/22 06:30

1,1-Dichloroethene

ug/L

ND

1.0

0.22

06/01/22 06:30

1,1-Dichloropropene

ug/L

ND

1.0

0.14

06/01/22 06:30

1,2,3-Trichlorobenzene

ug/L

ND

1.0

0.93

06/01/22 06:30

1,2,3-Trichloropropane

ug/L

ND

2.5

0.41

06/01/22 06:30

1,2,4-Trichlorobenzene

ug/L

ND

1.0

0.73

06/01/22 06:30

1,2,4-Trimethylbenzene

ug/L

ND

1.0

0.32

06/01/22 06:30

1,2-Dibromo-3-chloropropane

ug/L

ND

2.5

0.78

06/01/22 06:30

1,2-Dibromoethane (EDB)

ug/L

ND

1.0

0.20

06/01/22 06:30

1,2-Dichlorobenzene

ug/L

ND

1.0

0.12

06/01/22 06:30

1,2-Dichloroethane

ug/L

ND

1.0

0.21

06/01/22 06:30

1,2-Dichloroethene (Total)

ug/L

ND

1.0

0.22

06/01/22 06:30

1,2-Dichloropropane

ug/L

ND

1.0

0.14

06/01/22 06:30

1,3,5-Trimethylbenzene

ug/L

ND

1.0

0.090

06/01/22 06:30

1,3-Dichlorobenzene

ug/L

ND

1.0

0.13

06/01/22 06:30

1,3-Dichloropropane

ug/L

ND

1.0

0.10

06/01/22 06:30

1,4-Dichlorobenzene

ug/L

ND

1.0

0.13

06/01/22 06:30

2,2-Dichloropropane

ug/L

ND

1.0

0.16

06/01/22 06:30

2-Butanone (MEK)

ug/L

ND

10.0

0.98

06/01/22 06:30

2-Chlorotoluene

ug/L

ND

1.0

0.11

06/01/22 06:30

2-Hexanone

ug/L

ND

10.0

1.1

06/01/22 06:30

4-Chlorotoluene

ug/L

ND

1.0

0.15

06/01/22 06:30

4-Methyl-2-pentanone (MIBK)

ug/L

ND

10.0

0.74

06/01/22 06:30

Acetone

ug/L

ND

10.0

2.5

06/01/22 06:30

Benzene

ug/L

ND

1.0

0.14

06/01/22 06:30

Bromobenzene

ug/L

ND

1.0

0.088

06/01/22 06:30

Bromochloromethane

ug/L

ND

1.0

0.20

06/01/22 06:30

Bromodichloromethane

ug/L

ND

1.0

0.16

06/01/22 06:30

Bromoform

ug/L

ND

1.0

0.68

06/01/22 06:30

Bromomethane

ug/L

0.70J

5.0

0.46

06/01/22 06:30

Carbon disulfide

ug/L

ND

5.0

0.98

06/01/22 06:30

Carbon tetrachloride

ug/L

ND

1.0

0.17

06/01/22 06:30

Chlorobenzene

ug/L

ND

1.0

0.089

06/01/22 06:30

Chloroethane

ug/L

ND

1.0

0.37

06/01/22 06:30

Chloroform

ug/L

ND

1.0

0.22

06/01/22 06:30

Chloromethane

ug/L

0.34 J

1.0

0.28

06/01/22 06:30

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

Date: 06/06/2022 02:06 PM	without the written consent of Pace Analytical Services, LLC.	Page 19 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

METHOD BLANK: 3147760

Associated Lab Samples: 60400847001, 60400847002,

Matrix: Water

60400847003, 60400847004, 60400847005, 60400847006
Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

cis-1,2-Dichloroethene

ug/L

ND

1.0

0.13

06/01/22 06:30

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

06/01/22 06:30

Dibromochloromethane

ug/L

ND

1.0

0.30

06/01/22 06:30

Dibromomethane

ug/L

ND

1.0

0.11

06/01/22 06:30

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

06/01/22 06:30

Ethylbenzene

ug/L

ND

1.0

0.12

06/01/22 06:30

Hexachloro-1,3-butadiene

ug/L

ND

1.0

0.42

06/01/22 06:30

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

06/01/22 06:30

Methyl-tert-butyl ether

ug/L

ND

1.0

0.13

06/01/22 06:30

Methylene Chloride

ug/L

ND

1.0

0.39

06/01/22 06:30

n-Butylbenzene

ug/L

ND

1.0

0.15

06/01/22 06:30

n-Propylbenzene

ug/L

ND

1.0

0.12

06/01/22 06:30

Naphthalene

ug/L

ND

10.0

0.82

06/01/22 06:30

p-lsopropyltoluene

ug/L

ND

1.0

0.13

06/01/22 06:30

sec-Butylbenzene

ug/L

0.12J

1.0

0.11

06/01/22 06:30

Styrene

ug/L

ND

1.0

0.12

06/01/22 06:30

tert-Butylbenzene

ug/L

ND

1.0

0.12

06/01/22 06:30

Tetrachloroethene

ug/L

ND

1.0

0.33

06/01/22 06:30

Toluene

ug/L

ND

1.0

0.25

06/01/22 06:30

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

06/01/22 06:30

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

06/01/22 06:30

Trichloroethene

ug/L

ND

1.0

0.21

06/01/22 06:30

Trichlorofluoromethane

ug/L

ND

1.0

0.16

06/01/22 06:30

Vinyl chloride

ug/L

ND

1.0

0.17

06/01/22 06:30

Xylene (Total)

ug/L

ND

3.0

0.28

06/01/22 06:30

1,2-Dichlorobenzene-d4 (S)

%

101

80-120



06/01/22 06:30

4-Bromofluorobenzene (S)

%

100

80-120



06/01/22 06:30

Toluene-d8 (S)

%

99

80-120



06/01/22 06:30

Qualifiers

LABORATORY CONTROL SAMPLE: 3147761

Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,1,2-Tetrachloroethane

ug/L

20

20.7

104

80-120

1,1-Trichloroethane

ug/L

20

19.4

97

80-120

1,2,2-Tetrachloroethane

ug/L

20

18.4

92

75-125

1,2-Trichloroethane

ug/L

20

20.3

101

80-120

1-Dichloroethane

ug/L

20

19.5

98

75-125

1-Dichloroethene

ug/L

20

18.9

95

80-120

1-Dichloropropene

ug/L

20

19.6

98

80-125

2,3-Trichlorobenzene

ug/L

20

21.0

105

75-125

2,3-Trichloropropane

ug/L

20

19.6

98

80-125

2,4-Trichlorobenzene

ug/L

20

21.1

105

75-120

2,4-Trimethylbenzene

ug/L

20

20.2

101

80-125

2-Dibromo-3-chloropropane

ug/L

20

19.7

99

70-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 20 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

LABORATORY CONTROL SAMPLE: 3147761

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

1,2-Dibromoethane (EDB)

ug/L

20

20.0

100

80-120

1,2-Dichlorobenzene

ug/L

20

20.6

103

80-120

1,2-Dichloroethane

ug/L

20

20.1

101

75-120

1,2-Dichloroethene (Total)

ug/L

40

39.0

98

80-120

1,2-Dichloropropane

ug/L

20

19.6

98

80-125

1,3,5-Trimethylbenzene

ug/L

20

19.7

99

80-125

1,3-Dichlorobenzene

ug/L

20

20.6

103

80-120

1,3-Dichloropropane

ug/L

20

20.0

100

80-120

1,4-Dichlorobenzene

ug/L

20

20.1

101

80-120

2,2-Dichloropropane

ug/L

20

12.7

64

60-130

2-Butanone (MEK)

ug/L

100

83.9

84

40-150

2-Chlorotoluene

ug/L

20

20.0

100

80-120

2-Hexanone

ug/L

100

96.2

96

45-150

4-Chlorotoluene

ug/L

20

20.4

102

80-120

4-Methyl-2-pentanone (MIBK)

ug/L

100

99.4

99

65-140

Acetone

ug/L

100

76.1

76

20-175

Benzene

ug/L

20

20.3

102

80-120

Bromobenzene

ug/L

20

20.2

101

80-120

Bromochloromethane

ug/L

20

20.5

102

80-125

Bromodichloromethane

ug/L

20

19.9

99

80-125

Bromoform

ug/L

20

20.6

103

60-135

Bromomethane

ug/L

20

21.2

106

10-165

Carbon disulfide

ug/L

20

18.7

93

75-135

Carbon tetrachloride

ug/L

20

19.6

98

80-125

Chlorobenzene

ug/L

20

20.5

103

80-120

Chloroethane

ug/L

20

18.0

90

70-130

Chloroform

ug/L

20

19.5

98

80-120

Chloromethane

ug/L

20

17.6

88

35-155

cis-1,2-Dichloroethene

ug/L

20

19.6

98

80-120

cis-1,3-Dichloropropene

ug/L

20

18.8

94

80-125

Dibromochloromethane

ug/L

20

20.1

101

70-120

Dibromomethane

ug/L

20

19.5

98

80-120

Dichlorodifluoromethane

ug/L

20

17.0

85

50-150

Ethylbenzene

ug/L

20

20.3

102

80-120

Hexachloro-1,3-butadiene

ug/L

20

20.0

100

65-135

Isopropylbenzene (Cumene)

ug/L

20

20.6

103

80-125

Methyl-tert-butyl ether

ug/L

20

19.5

98

65-130

Methylene Chloride

ug/L

20

20.1

100

75-120

n-Butylbenzene

ug/L

20

19.0

95

80-125

n-Propylbenzene

ug/L

20

19.9

99

80-120

Naphthalene

ug/L

20

21.7

108

70-120

p-lsopropyltoluene

ug/L

20

20.0

100

80-135

sec-Butylbenzene

ug/L

20

20.1

100

80-120

Styrene

ug/L

20

20.8

104

80-120

tert-Butylbenzene

ug/L

20

20.6

103

80-120

Tetrachloroethene

ug/L

20

20.9

104

80-120

Toluene

ug/L

20

20.1

100

80-120

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 21 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

LABORATORY CONTROL SAMPLE: 3147761

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

trans-1,2-Dichloroethene

ug/L

20

19.5

97

80-120

trans-1,3-Dichloropropene

ug/L

20

18.8

94

75-120

Trichloroethene

ug/L

20

21.1

106

80-120

Trichlorofluoromethane

ug/L

20

18.9

94

80-130

Vinyl chloride

ug/L

20

18.3

92

65-130

Xylene (Total)

ug/L

60

60.6

101

80-120

1,2-Dichlorobenzene-d4 (S)

%





100

80-120

4-Bromofluorobenzene (S)

%





100

80-120

Toluene-d8 (S)

%





99

80-120

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 22 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:	790004	Analysis Method:	EPA 5030B/8260

QC Batch Method: EPA5030B/8260	Analysis Description: 8260 MSV Water 10 mL Purge

Laboratory:	Pace Analytical Services - Kansas City

60400847001, 60400847002, 60400847003, 60400847004

Associated Lab Samples:

METHOD BLANK: 3148556	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004

Blank	Reporting

Parameter

Units

Result

Limit

1,2-Dichloroethene (Total)

ug/L

ND

1.0

cis-1,2-Dichloroethene

ug/L

ND

1.0

trans-1,2-Dichloroethene

ug/L

ND

1.0

Trichloroethene

ug/L

ND

1.0

1,2-Dichlorobenzene-d4 (S)

%

101

80-120

4-Bromofluorobenzene (S)

%

100

80-120

Toluene-d8 (S)

%

100

80-120

MDL	Analyzed	Qualifiers

0.22 06/01/22 18:28
0.13 06/01/22 18:28
0.10 06/01/22 18:28
0.21 06/01/22 18:28
06/01/22 18:28
06/01/22 18:28
06/01/22 18:28

LABORATORY CONTROL SAMPLE: 3148557

Spike	LCS	LCS	% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,2-Dichloroethene (Total)

ug/L

40

37.8

94

80-120

cis-1,2-Dichloroethene

ug/L

20

19.2

96

80-120

trans-1,2-Dichloroethene

ug/L

20

18.6

93

80-120

Trichloroethene

ug/L

20

19.1

95

80-120

1,2-Dichlorobenzene-d4 (S)

%





100

80-120

4-Bromofluorobenzene (S)

%





101

80-120

Toluene-d8 (S)

%





100

80-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 23 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:	789130	Analysis Method:	EPA 300.0

QC Batch Method: EPA 300.0	Analysis Description: 300.0 IC Anions

Laboratory:	Pace Analytical Services - Kansas City

60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Associated Lab Samples:

METHOD BLANK: 3145234	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

Qualifiers

Chloride
Sulfate

mg/L
mg/L

0.53J
ND

1.0
1.0

0.53
0.55

05/27/22 11:54
05/27/22 11:54

METHOD BLANK: 3147238	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Blank	Reporting

Parameter	Units	Result	Limit	MDL	Analyzed	Qualifiers

Chloride	mg/L	0.53J	1.0	0.53 05/28/22 07:07

Sulfate	mg/L	ND	1.0	0.55 05/28/22 07:07

LABORATORY CONTROL SAMPLE: 3145235

Spike	LCS LCS % Rec

Parameter Units Cone.	Result % Rec Limits	Qualifiers

Chloride mg/L 5	4.6 92 90-110

Sulfate mg/L 5	5.2 104 90-110

LABORATORY CONTROL SAMPLE: 3147239

Spike	LCS LCS % Rec

Parameter Units Cone.	Result % Rec Limits	Qualifiers

Chloride mg/L 5	4.6 93 90-110

Sulfate mg/L 5	5.1 103 90-110

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3145236	3145237

MS	MSD

60401143001 Spike	Spike	MS MSD MS MSD % Rec	Max

Parameter Units Result Cone.	Cone.	Result Result % Rec % Rec Limits RPD RPD Qual

Chloride	mg/L	1010 1000 1000 2310 2510 130 150 80-120 8 15 M1

Sulfate	mg/L	2520 1000 1000 3810 4050 129 153 80-120 6 15 E,M1

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 24 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

MATRIX SPIKE SAMPLE:
Parameter

3145238

Units

60400847002
Result

Spike
Cone.

MS
Result

MS
% Rec

% Rec
Limits

Qualifiers

Chloride
Sulfate

mg/L
mg/L

61.6
24.1

50
50

109
69.4

94
91

80-120
80-120

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 25 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400847

QC Batch:
QC Batch Method

788091	Analysis Method:	EPA 353.2

EPA 353.2	Analysis Description: 353.2 Nitrate + Nitrite, Unpres.

Laboratory:	Pace Analytical Services - Kansas City

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

METHOD BLANK: 3141400	Matrix: Water

Associated Lab Samples: 60400847001, 60400847002, 60400847003, 60400847004, 60400847005

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

Qualifiers

Nitrogen, Nitrate

mg/L

ND

0.10

0.079

05/21/22 10:18





LABORATORY CONTROL SAMPLE:
Parameter

3141401
Units

Spike LCS
Cone. Result



LCS
% Rec

% Rec

Limits Qualifiers



Nitrogen, Nitrate

mg/L

1

0.99



99

70-130





MATRIX SPIKE SAMPLE:
Parameter

3141402
Units

60400810001
Result

Spike
Cone.



MS
Result

MS
% Rec

% Rec
Limits

Qualifiers

Nitrogen, Nitrate

mg/L

<0.079



1

0.97

97

70-130



MATRIX SPIKE SAMPLE:
Parameter

3141404
Units

60400847004
Result

Spike
Cone.



MS
Result

MS
% Rec

% Rec
Limits

Qualifiers

Nitrogen, Nitrate

mg/L

0.11



1

1.1

99

70-130



SAMPLE DUPLICATE: 3141403
Parameter

Units

60400810004
Result

Dup
Result



RPD

Max
RPD

Qualifiers



Nitrogen, Nitrate

mg/L

<0.079



ND



20





Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/06/2022 02:06 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 26 of 31


-------
\ce Analytical9

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALIFIERS

Project:

NCWS (LIST A)

Pace Project No.: 60400847
DEFINITIONS

DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.

ND - Not Detected at or above adjusted reporting limit.

TNTC - Too Numerous To Count

J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.

MDL-Adjusted Method Detection Limit.

PQL - Practical Quantitation Limit.

RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.

S - Surrogate

1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.

Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.

LCS(D) - Laboratory Control Sample (Duplicate)

MS(D) - Matrix Spike (Duplicate)

DUP - Sample Duplicate

RPD - Relative Percent Difference

NC - Not Calculable.

SG - Silica Gel - Clean-Up

U - Indicates the compound was analyzed for, but not detected.

N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.

Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as

"Total" may vary slightly from the sum of the reported component parameters.

Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.

TNI - The NELAC Institute.

ANALYTE QUALIFIERS

B	Analyte was detected in the associated method blank.

E	Analyte concentration exceeded the calibration range. The reported result is estimated.

M1	Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.

Date: 06/06/2022 02:06 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 27 of 31


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:

Pace Project No.

NCWS (LIST A)
60400847

Lab ID

Sample ID

QC Batch Method

QC Batch

Analytical

60400847001

IW-16-W-17

RSK175 Modified

677764



60400847002

IW-20-W-17

RSK175 Modified

677764



60400847003

IW-04-W-17

RSK175 Modified

677764



60400847004

IW-10-W-17

RSK175 Modified

677764



60400847005

IW-01-W-17

RSK175 Modified

677764



60400847001

IW-16-W-17

EPA 3010

788176

EPA 6010

60400847002

IW-20-W-17

EPA 3010

788176

EPA 6010

60400847003

IW-04-W-17

EPA 3010

788176

EPA 6010

60400847004

IW-10-W-17

EPA 3010

788176

EPA 6010

60400847005

IW-01-W-17

EPA 3010

788176

EPA 6010

60400847001

IW-16-W-17

EPA 5030B/8260

789769



60400847001

IW-16-W-17

EPA 5030B/8260

790004



60400847002

IW-20-W-17

EPA 5030B/8260

789769



60400847002

IW-20-W-17

EPA 5030B/8260

790004



60400847003

IW-04-W-17

EPA 5030B/8260

789769



60400847003

IW-04-W-17

EPA 5030B/8260

790004



60400847004

IW-10-W-17

EPA 5030B/8260

789769



60400847004

IW-10-W-17

EPA 5030B/8260

790004



60400847005

IW-01-W-17

EPA 5030B/8260

789769



60400847006

TB-03-051922

EPA 5030B/8260

789769



60400847001

IW-16-W-17

EPA 300.0

789130



60400847002

IW-20-W-17

EPA 300.0

789130



60400847003

IW-04-W-17

EPA 300.0

789130



60400847004

IW-10-W-17

EPA 300.0

789130



60400847005

IW-01-W-17

EPA 300.0

789130



60400847001

IW-16-W-17

EPA 353.2

788091



60400847002

IW-20-W-17

EPA 353.2

788091



60400847003

IW-04-W-17

EPA 353.2

788091



60400847004

IW-10-W-17

EPA 353.2

788091



60400847005

IW-01-W-17

EPA 353.2

788091



Analytical
Batch

788272
788272
788272
788272
788272

Date: 06/06/2022 02:06 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 28 of 31


-------
Wo# 6040084 7

DC#_Titfe: ENV-FRM-LENE-0009_Sample Cond

mil

Revision: 2

Effective Date: 01/12/2022

Issued By: Lenexa

Client Name: R^ *)" 'Cf\Yvf\

kH U

Tracking #: 11V)	QA ^ ^	Pace Shipping Label Used?- Yes No ~

Custody Seal on Cooler/Box Present: Yes No ~ /Seals int:!. Yes ~ No ~

Packing Material: Bubble Wrap \jf Bubble Bags B	Foam ~ None ~ Other

Thermometer Used: 1 & 1	Type of Ice:	Blue None

Cooler Temperature (°C): As-read

		I

Corr. Factor

0

•? 7
Corrected ~

Date and initials of person ' -¦
examining contents: /-		

Temperature should be above freezing to 6°C

Chain of Custody present:

B^es

~ No

~ n/a



Chain of Custody relinquished:

0Yes

~ No

~ n/a



Samples arrived within holding time:

S^Yes

~ No

~ n/a



Short Hold Time analyses (<72hr):

I^Yes

~ No

~ n/a

m

Rush Turn Around Time requested:

~Yes

Ono

~ n/a



Sufficient volume:

C^Yes

~ No

~ n/a



Correct containers used

IZfves

~ No

~ n/a

0t\IN Wt\*t± L Tlrif eitfvnkx foe

Pace containers used:

If^Yes

~ No

~ n/a

TKoj,

Containers intact:

S^Yes

~ No

~ n/a



Unpreserved 5035A / TX1005/1006 soils frozen in 48hrs?

~Yes

~ No

O^/A



Filtered volume received for dissolved tests?

~Yes

~ No

t^N/A



Sample labels match COC: Date / time / ID / analyses

I^Yes

~ No

~ N/A



Samples contain multiple phases? Matrix:

~Yes

b/no

~ n/a



Containers requiring pH preservation in compliance?

(HNOi, H?SO,i, HCI<2: NaOH>9 Sulfide. NaOH>10 Cyanide)
[Exceptions: VOA, Micro, O&G, KS TPH, OK-DROi LOT#:

ElYes

71 1*1

~ No
i

~ n/a

List sample IDs, volumes, lot #'s of preservative and the
date/time added.

Cyanide water sample checks:

Lead acetate strip turns dark? (Record only)

Potassium iodide test strip turns blue/purple? (Preserve)

~Yes
~Yes

~	no

~	No





Trip Blank present:

B^Yes

~ No

~ n/a



Headspace in VOA vials ( >6mm);

~ Yes

S^No

~ n/a



Samples from USDA Regulated Area: State:

~Yes

~ No

5^n/a



Additional labels attached to 5035A / TX1005 vials in the field?

~ Yes

Gj/o

~ n/a



Client Notification/ Resolution:
Person Contacted:

Comments/ Resolution:

Copy COC to Client?

~ate/Time:

Y / N

Field Data Required? Y / N

Project Manager Review:

Date:

Qualtrax Document ID: 30468

Page 1 of 1

Page 29 of 31


-------
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r I
csr^

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-t,

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01


-------
Remedial Action - Newton County Wells Site
Silver Creek and Saginaw, Missouri

Prepared for

Missouri Department of Natural Resources

On behalf of

FAG Bearings, LLC
Joplin, Missouri

Prepared by

Ramboll US Consulting, Inc.

St. Louis, Missouri

Date

December 2022

Project Number

1690004605


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Page

1	INTRODUCTION	1

2	BACKGROUND	2

3	2022 WELL INSPECTION AND MNA FIELD SAMPLING TASKS	6

3.1	Monitoring Well Inspection and Maintenance	6

3.2	Groundwater Sample Collection	6

3.2.1	Static Water Level and Total Well Depth Measurements	6

3.2.2	Monitoring Well Purging	7

3.2.2.1	Piston Pump	7

3.2.2.2	Bailer	8

3.2.3	Monitoring Well Sampling	9

3.3	Surface Water Sample Collection	 10

3.4	Analytical Methods	 11

3.5	Analytical and Field-Measured Results	 12

3.5.1	Uppermost Groundwater/Bedrock Interface Wells	 12

3.5.2	Mississippian Aquifer Wells	 14

3.5.3	Mississippian Aquifer Spring Surface Water Locations	 16

3.6	Data Quality Assessment	 17

3.6.1	Field Data	17

3.6.2	Laboratory Analytical Data	 17

4	DISCUSSION OF RESULTS	20

4.1	Groundwater Levels	20

4.1.1	Uppermost Groundwater	20

4.1.2	Mississippian Aquifer	20

4.2	COC Temporal Trend Analysis	21

4.2.1	Full MNA Data Set	22

4.2.2	Uppermost Groundwater/Bedrock Interface Wells	22

4.2.3	Mississippian Aquifer Wells	24

4.2.4	Mississippian Aquifer Spring Surface Water Locations	26

4.2.5	Recent MNA Data Set	27

4.2.6	Uppermost Groundwater/Bedrock Interface Wells	27

4.2.7	Mississippian Aquifer Wells	29

4.2.8	Mississippian Aquifer Spring Surface Water Locations	30

4.3	MNA Water Quality Indicator Analysis	31

4.3.1	Uppermost Groundwater Wells	32

4.3.2	Mississippian Aquifer Wells and Spring Surface Water	37

5	SUMMARY AND CONCLUSIONS	39

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Silver Creek and Saginaw, MO

l-ES

Table 3-1: Summary of Monitoring Well Static Water Level Measurements Collected (May
2022)

Table 3-2: Summary of Final Monitoring Well Groundwater and Spring Surface Water

Field Parameter Measurements (May 2022)

Table 3-3: Groundwater and Surface Sample Locations and List of Parameters to Support

Monitored Natural Attenuation for Remedial Action Activities
Table 3-4: Summary of Laboratory Monitored Natural Attenuation Parameters and
Detected Volatile Organic Compounds (May 2022)

URES

Figure 1-1: Site Location Map

Figure 3-1: Surface Water, Uppermost Groundwater and Mississippian Aquifer Well
Locations

Figure 3-2: Uppermost Groundwater Wells, Static Water Elevations (May 2022)

Figure 3-3: Mississippian Aquifer Wells, Static Water Elevations (May 2022)

Figure 4-1A: Uppermost Groundwater Analytical Results, Trichloroethene (2000 to 2022)
Figure 4-1B: Uppermost Groundwater Analytical Results, cis-l,2-Dichloroethene (2000 to
2022)

Figure 4-1C: Uppermost Groundwater Analytical Results, Vinyl Chloride (2000 to 2022)
Figure 4-2A: Spring Surface Water and Mississippian Aquifer Wells, Trichloroethene (2000
to 2022)

Figure 4-2B: Spring Surface Water and Mississippian Aquifer Wells Analytical Results, cis-

1,2-Dichloroethene (2000 to 2022)

Figure 4-2C: Spring Surface Water and Mississippian Aquifer Wells Analytical Results, Vinyl
Chloride Analytical Results (2000 to 2022)

CES

Appendix A
Appendix B
Appendix C
Appendix D:
Appendix E:

Well Inspection and Maintenance Logs (May 2022)

Field Instrument Calibration Logs (May 2022)

Groundwater and Surface Water Sampling Logs (May 2022)

Validated Analytical Laboratory Data Reports (May 2022)

Temporal Trend Analysis Data Input and Output

E-l Full MNA Data Set

E-2 Eight Most Recent Data Points

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RA - NCWS
Silver Creek and Saginaw, MO

This 2022 Annual Report summarizes and documents the activities conducted by FAG
Bearings, LLC (FAG Bearings) with regard to the Newton County Wells Site (NCWS) for
submittal to the Missouri Department of Natural Resources (MDNR).

The NCWS is located in northern Newton County in Joplin, Missouri and is defined as the
FAG Bearings property as well as portions of the aquifer beneath the Villages of Silver Creek
and Saginaw, in Newton County, Missouri, where trichloroethene (TCE) and/or compounds
from its ongoing degradation [primarily cis-l,2-dichloroethene (cis-l,2-DCE) and vinyl
chloride (VC)] have come to be located. These three parameters represent the primary
compounds of concern (COCs) with respect to the NCWS. As noted by the MDNR in the June
2005 Consent Decree Statement of Work for the NCWS; "TCE and TCE degradation products
present in the soil and groundwater of the NCWS are a result of the cutting of and
accidental release of TCE from the former TCE transfer pipeline on the FAG Bearings
property." The general boundary of the NCWS based on the results from the remedial
investigation are provided on Figure 1-1.

The activities described in this report were conducted during calendar year 2022 by Ramboll
US Consulting, Inc. (Ramboll) on behalf of FAG Bearings and consisted primarily of
completion of monitored natural attenuation (MNA) groundwater sampling of existing
permanent wells and surface spring water locations which are utilized to monitor ongoing
conditions with respect to the NCWS.

The MNA activities were conducted to satisfy the requirements for implementing the MDNR-
approved NCWS Remedial Action Work Plan (RAWP) dated June 2007 as revised by the
MDNR-approved NCWS First and Second Amended RAWPs dated December 2015 and July
2020, respectively.

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RA - NCWS
Silver Creek and Saginaw, MO

FAG Bearings entered into a Consent Decree with MDNR to implement the remedial action
(RA) for the NCWS. In advance of the RA Consent Decree, FAG Bearings conducted
significant investigation and thorough characterization of the NCWS which included
completion of an Engineering Evaluation/Cost Assessment (EE/CA) and Remedial
Investigation/Feasibility Study (RI/FS). Additionally, substantial source control measures
(focused soil removal and multiple rounds of in-situ chemical oxidation) were implemented
with respect to the TCE transfer pipeline trench in advance of the RA Consent Decree.

The EE/CA and RI were implemented following MDNR-approved work plans to include
completion of the following:

•	Advanced 396 continuously sampled soil borings representing over 10,000 feet of
overburden stratigraphy with collection of soil and groundwater samples.

•	Use of an on-site mobile laboratory for sample analysis to direct investigation and
delineation activities in real time, consisting of:

-	1,823 soil samples analyzed for target VOCs; and

-	263 groundwater samples analyzed for target VOCs.

•	Confirmation of mobile laboratory soil and groundwater results through fixed-base
laboratory analysis of 543 split samples.

•	Analysis of 252 permeability and passive soil gas samples.

•	Installation of 65 uppermost groundwater wells.

•	Hydraulic conductivity testing of approximately 30 uppermost groundwater wells

•	Tracer test studies in overburden groundwater using sodium bromide within the
area immediately down-gradient of the former TCE pipeline trench and within the
impacted area southwest of the former TCE pipeline trench.

•	Sampling of 24 residential wells on a every other month basis for a total of six
sampling events.

•	Five surface water and sediment samples.

•	Installation of three continuously cored angled bedrock borings which were
subsequently subject to geophysical analysis and in-situ interval hydraulic
conductivity testing.

•	Conversion of one angled boring into a Mississippian Aquifer monitoring well.

•	Installation of seven Mississippian Aquifer monitoring wells of which five were
installed in the Villages of Silver Creek and Saginaw to replace the need for
sampling residential wells and provide for subsequent abandonment of specific
residential wells.

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Silver Creek and Saginaw, MO

•	Pumping tests of the seven new Mississippian Aquifer monitoring wells.

•	Installation of one monitoring well into the deeper Cambro-Ordovician Aquifer.

The effective date of the RA Consent Decree was January 3, 2007. The NCWS Record of
Decision (ROD) provided remedial action objectives (RAOs) and the MDNR-chosen
remediation alternative with concurrence of the U.S. Environmental Protection Agency
(USEPA) consisting of:

Remedial Action Objectives

•	Maintain and enforce current conditions and existing regional regulatory controls that
provide protection from risk-producing exposure to the TCE and TCE degradation
product impacted portions of the Mississippian Aquifer;

•	Reduce the concentration of TCE and TCE degradation products in the uppermost
aquifer of the NCWS to concentrations that are protective of the Mississippian Aquifer
as a potable water source with respect to TCE and TCE degradation products; and

•	Return the Mississippian Aquifer water quality at the NCWS to potable conditions,
with respect to TCE and TCE degradation products.

Remediation Alternative

•	MNA to address the uppermost groundwater and the Mississippian Aquifer.

•	Implementation/enforcement of existing regional institutional controls (ICs)
including:

-	Area 11 (formerly Special Area 2) as provided in the Missouri Water Well
Construction Code - 10 CSR 23-3.090;

-	Monitoring usage of public water supply systems; and

-	Enforcement of prohibition on usage of impacted wells for potable purposes
with subsequent connection to the public water supply system.

FAG Bearings is responsible for implementation of activities required for the MNA portion of
the chosen alternative for the NCWS. As stated in the NCWS ROD, MDNR is responsible for
the implementation/enforcement of the existing regional ICs (including Area 11 specified
construction standards, state well plugging/abandonment rules and monitoring usage of the
public water supply systems) as required by the chosen alternative.

First Five Year Period

The RAWP dated June 2007 was submitted to MDNR and USEPA by Ramboll on behalf of
FAG Bearings to satisfy requirements under the governing Consent Decree and included
descriptions of RA activities to be conducted for the NCWS during the first five year period.

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Silver Creek and Saginaw, MO

At the conclusion of the first five year period, the First Five Year Summary Report dated
August 2013 was submitted to MDNR and USEPA by Ramboll on behalf of FAG Bearings.
This report presented a comprehensive analysis of the first five years of RA activities and
reporting which had been conducted toward implementation of the RAWP at the NCWS.

Activities completed during this time period included:

•	Abandonment of specifically identified NCWS investigative wells, northern
investigative wells and residential wells; and

•	Ten MNA sampling events, representing Rounds 1 through 10.

Following receipt of the First Five Year Summary Report, MDNR and USEPA completed the
First Five Year Review Report for the NCWS dated April 2014 which provided a deferred
protectiveness statement.

Second Five Year Period

The First Amended RAWP dated December 2015 was submitted to MDNR and USEPA by
Ramboll on behalf of FAG Bearings. The First Amended RAWP addressed issues and
recommendations provided in the First Five Year Review Report and provided a description
of RA activities to be conducted for the NCWS during the second five year period.

At the conclusion of the second five year period, the Second Five Year Summary Report
dated January 2019 was submitted to MDNR and USEPA by Ramboll on behalf of FAG
Bearings. This report presented a comprehensive analysis of the second five years of RA
activities and reporting which had been conducted towards implementation of the First
Amended RAWP at the NCWS.

Activities completed during this time period included:

•	Abandonment of specifically identified NCWS investigative wells and northern
investigative wells;

•	Four MNA sampling events, representing Rounds 11 through 14; and

•	Four quarterly vapor intrusion air monitoring events (representing specifically
identified and focused FAG Bearings facility and offsite down-gradient buildings).

Following receipt of the Second Five Year Summary Report, MDNR and USEPA completed
the Second Five Year Review Report for the NCWS dated April 2019 which provided a
protectiveness statement of short-term protective.

Third Five Year Period

The Second Amended RAWP for the NCWS dated July 2020 was submitted to MDNR and
USEPA by Ramboll on behalf of FAG Bearings and approved in a letter from MDNR dated
January 27, 2021.

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Activities completed during this time period thus far consist of:

•	Three MNA sampling events, representing Rounds 15 through 17; and

•	Submission of an updated Sampling and Analysis Plan (SAP) to MDNR and USEPA.

The following sections of this report describe the RA activities conducted in 2022 as part of
the implementation of the Second Amended RAWP at the NCWS through Round 17 of
groundwater monitoring.

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Silver Creek and Saginaw, MO

The annual groundwater monitoring event was conducted in May 2022 which represents
Round 17 of the MNA component of the NCWS RA. The monitoring network consists of 28
permanent monitoring wells shown on Figure 3-1 (18 screened in the uppermost
groundwater and 10 screened in the Mississippian Aquifer).

All activities associated with this sampling event were conducted following the general
procedures provided in the Second Amended RAWP and updated SAP for collection and
analysis of both groundwater and surface water samples. Ongoing annual MNA sampling is
planned to continue to be conducted during the first half of each calendar year as specified
in the Second RAWP.

Following is a summary of the inspection and field sampling of the monitoring well network
conducted for the 2022 RA sampling event.

3.1	MONITORING WELL INSPECTION AND MAINTENANCE

At the commencement of the sampling event, each permanent monitoring well was visually
inspected prior to sampling to confirm that the surface completions appeared to remain in
sound condition. In addition to visual inspection, the total depth of each well was measured
for comparison to the recorded constructed total depths to determine if any significant
changes had occurred due to silting or other anomalies.

Summary inspection and maintenance logs for this sampling event are provided in Appendix
A. No significant anomalies were observed in surface completions of the wells and no
significant variation of total measured depths versus recorded total depths were noted.
Consequently, no significant maintenance or corrective actions were necessary for any of
the wells during this sampling event.

3.2	GROUNDWATER SAMPLE COLLECTION

3.2.1 Static Water Level and Total Well Depth Measurements

Static groundwater levels and total well depths were measured, in each of the uppermost
groundwater and Mississippian Aquifer monitoring wells prior to the initiation of well purging
and sampling activities. Static water levels (SWLs) were measured in each of the 28
monitoring wells shown on Figure 3-1.

Monitoring wells were opened and (if necessary) allowed to equilibrate to atmospheric
conditions prior to the measurement of SWLs using an electronic water level meter. The
depth to SWL was measured in each well to the nearest 0.01 foot with respect to a
surveyed elevation point at the top of each well casing.

Measurements were conducted a consecutive order starting with wells that have had limited
or no historic impacts and finishing with wells with higher historic impacts to eliminate any

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potential cross-contamination between wells. The water level meter probe and portions of
the calibrated tape which were submerged were decontaminated prior to use and between
each well following the procedures described in the RAWPs and SAP.

Static water level measurements and calculated elevations from the May 2022 sampling
event are presented in Table 3-1. The uppermost groundwater and Mississippian Aquifer
calculated SWL elevations are also provided in feet above mean sea level (amsl) for each
well on Figures 3-2 and 3-3, respectively.

Total depth measurements were collected at each well immediately following collection of
SWLs using a weighted tape and recorded to the nearest 0.1 foot with respect to a surveyed
elevation point at the top of each well casing. Any portions of the weighted tape which were
submerged for collection of a measurement were decontaminated prior to use and between
each well following the procedures described in the RAWPs and SAP. The measured total
depths collected from each well during this sampling event and corresponding recorded total
constructed depths are presented on Table 3-1. As provided on the tabulated summary, no
significant differences in recent and recorded total depths were noted. Total depth
measurements will continue to be collected during each future MNA sampling event.

3.2.2 Monitoring Well Purging

Each monitoring well was purged prior to sample collection to remove standing water from
within the well casing in order to obtain a sample representative of the water-bearing zone
following the methodology provided in the RAWP and SAP.

Well purging and groundwater sample collection were performed using one of two methods;
1) a site-dedicated portable piston low-flow pump or 2) new single use polyethylene bailers.
For those monitoring wells in which adequate water was present and recharge has been
sufficient historically to maintain a continuous pumping rate, the piston pump was used to
purge and sample the wells. If adequate water was not available in a monitoring well and/or
recharge historically has not been adequate for use of the piston pump, then new bailers
using new bailing cord were used to purge and sample the well.

Field-measured stabilization parameters were measured during and at the conclusion of well
purging using YSI ProQuatro multi-parameter meters. The meters were calibrated on a daily
basis following the procedures provided in the equipment user manual. Completed summary
calibration logs for the two meters utilized for this sampling event are provided in Appendix
B.

The following sections describe the procedures used to purge wells with the site-dedicated
piston pump and new dedicated bailers.

3.2.2.1 Piston Pump

A total of thirteen wells were purged and sampled using the site-dedicated piston pump for
the 2022 MNA sampling event: Three wells screened in the uppermost groundwater (FAG-

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22, FAG-31 and FAG-36) and ten wells screened in the Mississippian Aquifer (FAG-AW4,
FAG-05, FAG-11, FAG-88, FAG-89, RI-MW5, RI-MW6, RI-MW7, RI-MW8 and RI-MW9).

For purging and sampling of each well, the piston pump intake was gently lowered into the
well with the pump intake placed approximately 5 feet above the bottom of the well. The
water level in each well was monitored during pumping and, if possible, the pumping rate
was adjusted such that the pumping rate did not exceed the well recharge rate (i.e., limited
draw down of water in the well). Measurements of depths to water at each well during
purging were similar to those collected historically in that most of the wells experienced
little or no draw down during purging and all of the wells maintained adequate recharge to
fully complete the purging process.

Field water quality parameters were measured continuously using a closed loop flow-
through cell until stabilization of all field parameters was achieved as provided in the RAWP
and SAP. Field measurements of pH, specific conductance (SC), temperature, oxidation
reduction potential (ORP) and dissolved oxygen (DO) were collected during the purging of
each well to ensure that subsequent groundwater samples were representative of conditions
in the monitored water bearing zone. However, activities associated with facility traffic at
well FAG-22 required the sampling crew to move and resulted in the samples from this well
being collected before one parameters (DO) had fully stabilized. Following collection of
laboratory samples , specific wells were analyzed in the field using a colorimeter for the
parameter ferrous iron as provided in the SAP.

Field sampling logs for each well from this sampling event are provided in Appendix C and a
summary of the final set of field measurements collected before sampling of each well is
provided in Table 3-2.

The piston pump and tubing were decontaminated prior to use and between use at each
monitoring well following the procedures described in the RAWP and SAP. As part of quality
assurance/quality control procedures, an equipment blank was collected from the piston
pump following decontamination and results are discussed in the data quality assessment
section.

3.2.2.2 Bailer

A total of 15 monitoring wells were purged and sampled using new dedicated disposable
bailers and bailing cord for the 2022 MNA sampling event, all screened in the uppermost
groundwater (FAG-32, FAG-33, FAG-34, FAG-35, FAG-43, FAG-46, FAG-47, FAG-50, FAG-
56, FAG-62, FAG-73, FAG-74, FAG-85, RI-MW1 and RI-MW2).

For purging and sampling of each well, the dedicated bailers were gently lowered into the
well and retrieved. As purging of wells progressed, representative grab samples were
collected on a periodic basis and field parameters (i.e., pH, SC, temperature, ORP and DO)
were measured.

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Wells were considered purged and ready for analytical sample collection after removal of a
minimum of three times the measured casing volume, the well bailed dry and/or the field
measured water quality parameters stabilized in accordance with the SAP. Following
stabilization, specific wells were analyzed in the field using a colorimeter for the parameter
ferrous iron.

Seven uppermost groundwater wells (FAG-32, FAG-33, FAG-34, FAG-50, FAG-56, FAG-73
and RI-MW1) purged dry (i.e., insufficient recharge in the well to allow continued bailing)
during this sampling event. This is similar to conditions noted during previous MNA sampling
events. In all cases, sample collection was conducted once a sufficient volume of water for
the required analyses recharged to the well.

Field sampling logs from this sampling event are provided in Appendix C and a summary of
the final set of field measurements before sampling of each well is provided in Table 3-2.

3.2.3 Monitoring Well Sampling

After each monitoring well was determined to have been adequately purged, groundwater
samples were collected for laboratory analysis. In the case of wells sampled using the piston
pump, the pumping rate was the same low flow rate as had been used to purge the wells.
In the case of wells sampled using bailers, a new double-check valve bailer dedicated to
each well was gently lowered into and retrieved from the water column similar to the well
purging technique and a bottom-emptying device was used to produce a controlled stream
of water from the bottom of the bailer.

Groundwater samples were obtained by directly filling laboratory provided sampling bottles
from the bailer or piston pump discharge. Sample bottles for organic parameters were filled
first followed by inorganic parameters. Samples for QA/QC purposes were collected by
alternately filling investigative and QA/QC sample bottles for each parameter.

A total of 28 investigative groundwater samples were collected. In addition, two field
duplicate samples and two matrix spike/matrix spike duplicate (MS/MSD) samples were
collected (one each from an upper groundwater well and one each from a Mississippian
Aquifer well). The field duplicates were "blind" samples in that they were provided with a
generic identification number and not labeled with the well number from which they were
collected. The field duplicates were collected from upper groundwater well FAG-35 (labeled
"FD-List A") and Mississippian Aquifer well FAG-05 (labeled "FD-List B"). The MS/MSD
samples were collected from upper groundwater well RI-MW2 and Mississippian Aquifer well
FAG-85. All samples were placed in insulated coolers with ice and shipped under chain of
custody control via overnight courier to Pace Analytical Services in Lenexa, Kansas, for
analysis. Laboratory-provided trip blank samples accompanied each shipment to the
laboratory.

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3.3 SURFACE WATER SAMPLE COLLECTION

Surface water samples were collected at two locations for this MNA sampling event [SW-01
and RW-341A (Figure 3-1)]. Each location represents spring water produced from the
Mississippian Aquifer.

Surface water sample SW-01 was collected from a small pond along the eastern side of
Saginaw Road near the intersection of High Street at a point where it is fed by Mississippian
Aquifer springs. This sample was collected from just in front of a culvert where water flows
under Saginaw Road and into a large pond. Surface water sample RW-341A was collected
from Thurman Creek downstream of the Reddings Road Bridge near the western bank in a
portion of the stream channel with higher flow conditions. Samples at each location were
collected by submerging new dedicated sample collection containers into the water and then
filling the laboratory provided sample containers (organic parameters were collected first
followed by inorganic parameters).

Field water quality parameters (i.e., pH, SC, ORP, DO and temperature) were measured at
the time each surface water sample was collected and no significant color/clarity nor odors
were noted during sample collection. Field sampling logs are provided in Appendix C and a
summary of field measurements are provided in Table 3-2.

All samples were placed in insulated coolers with ice and shipped under chain of custody
control via overnight courier to Pace Analytical Services in Lenexa, Kansas for analysis.

Precipitation

There was no precipitation on the day that surface water samples were collected (May 16).
Daily precipitation totals for the ten days preceding surface water sampling recorded at the
National Weather Service station at the Joplin Regional Airport (JLN) are summarized in the
following table.

JLN MAY 2022 DAILY PRECIPTIAON TOTALS (inches)

5/6

5/7

5/8

5/9

5/10

5/11

5/12

5/13

5/14

5/15

0.65

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.00

0.14

As noted on the table, the majority of the precipitation preceding the sampling event took
place on May 6 which was 10 days prior to sampling. Following that, the only additional
precipitation recorded was a minor amount on May 15 (the day prior to sampling) which
ended by 1,700 hours. The surface water samples were collected late afternoon on Monday,
May 16 in advance of precipitation predicted to occur during the remaining week.

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3.4 ANALYTICAL METHODS

Consistent with the rationale for analyses as documented in the ROD for NCWS as well as
the RAWPs and SAP, the dominant mechanisms for natural attenuation of TCE and
degradation products continue to be biodegradation in the upper groundwater and
hydrodynamic dispersion in the underlying Mississippian Aquifer.

Analytical methods were selected based on this rationale to monitor attenuation conditions
specific to the location of individual sampling points and are summarized on Table 3-3. For
identification and assessment purposes, wells have been grouped based on the geologic unit
they monitor and locations relative to the identified source of NCWS impact with the
potential to impact the Mississippian Aquifer - the former TCE transfer pipeline trench
located on the FAG Bearings property. Throughout the NCWS RA, wells have been grouped
as follows:

Uppermost Groundwater Wells

•	Northwest corner of FAG Bearings property (one well);

•	Southwest of FAG Bearings Service Building and southern FAG Bearings property line
(four wells);

•	Village of Silver Creek (two wells);

•	Adjacent to the former TCE pipeline transfer trench (six wells); and

•	South of the former TCE pipeline transfer trench (five wells).

Mississippian Aquifer Wells

•	On the FAG Bearings property (five wells); and

•	Villages of Silver Creek and Saginaw (five wells).

These groupings are provided on Table 3-3 as well as Figures 3-4A and 3-4B for uppermost
groundwater and Mississippian Aquifer wells, respectively.

Biodegradation Parameters

Samples were collected from the uppermost groundwater from 14 wells for this sampling
event (FAG-22, FAG-31, FAG-32, FAG-33, FAG-34, FAG-35, FAG-36, FAG-47, FAG-50, FAG-
56, FAG-62, FAG-73, FAG-74 and FAG-85) and analyzed for the following biodegradation
parameters in accordance with the indicated laboratory methods (i.e., List A):

•	Volatile organic compounds (VOCs): SW846 5030B/8260B;

•	Nitrate: EPA 353.2;

•	Sulfate: EPA 300.0;

•	Chloride: EPA 300.0;

•	Methane: RSK 175;

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•	Ethane: RSK 175;

•	Ethene: RSK 175; and

•	Total Iron: EPA 6010.

Hvdrodvnamic Dispersion Parameters

An additional 14 samples were collected for this sampling event from four wells screened
within the uppermost groundwater (FAG-43, FAG-46, RI-MW1 and RI-MW2) and all ten
wells screened within the Mississippian Aquifer (FAG-AW4, FAG-05, FAG-11, FAG-88, FAG-
89, RI-MW5, RI-MW6, RI-MW7, RI-MW8 and RI-MW9) and analyzed for the following
hydrodynamic dispersion parameters in accordance with the indicated laboratory methods
(i.e., List B):

. VOCs: SW846 5030B/8260B; and

•	Chloride: EPA 300.0.

The two spring surface water samples (SW-01 and RW-341A) were analyzed for the
following hydrodynamic dispersion parameters in accordance with the indicated laboratory
methods (i.e., List B):

. VOCs: SW846 5030B/8260B; and
• Chloride: EPA 300.0.

3.5 ANALYTICAL AND FIELD-MEASURED RESULTS

A summary of analytical results for samples collected from the uppermost groundwater,
Mississippian Aquifer and Mississippian Aquifer spring surface water sampling locations for
this sampling event (MNA Round 17) is presented in Table 3-4. The table includes data
qualifiers assigned by the laboratory or from subsequent third-party data validation. The
validated laboratory analytical data reports from this sampling event are provided in
Appendix D.

3.5.1 Uppermost Groundwater/Bedrock Interface Wells

A summary of the parameters detected in groundwater samples collected from the 18
monitoring wells screened within the uppermost groundwater is presented below.

VOC Analysis

Four VOCs were detected in more than one of the groundwater samples collected from the
uppermost wells, specifically: TCE and its degradation by-products cis-l,2-DCE, trans-1,2-
dichloroethene (trans-l,2-DCE) and VC. Although the parameter total dichloroethene is also
provided in the laboratory reports, it merely represents the sum of trans-l,2-DCE and cis-
1,2-DCE. The number of samples in which these four individual VOCs were detected and the
measured concentration ranges in micrograms per liter (|jg/L) are summarized in the
following table for this sampling event. The qualifier "J" indicates an estimated
concentration below the reporting limit but above the method detection limit.

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ANALYTE

NUMBER OF DETECTIONS

DETECTED CONCENTRATION RANGE

TCE

17 of 18 samples

2.3 to 2,050 pg/L

cis-l,2-DCE

17 of 18 samples

0.67 J to 367 pg/L

trans-l,2-DCE

9 of 18 samples

0.17 J to 6.5 pg/L

VC

7 of 18 samples

0.21 J to 53.8 pg/L

Eight of the samples from the uppermost groundwater required dilution by the laboratory
for VOC analysis, consequently the parameters provided in the above summary table had an
elevated detection limit for those wells. This consists of wells; FAG-34, FAG-35, FAG-36,
FAG-74 and FAG-85 (5x dilution), FAG-22 and FAG-31 (lOx dilution) and FAG-50 (25x
dilution). Although relatively lower concentration data may not be fully captured due to
laboratory dilution, those compounds measured at more significant levels are still being
identified and reported.

The majority of COC impact associated with uppermost groundwater wells is summarized in
the following table which provides the general location of each well by grouping and
measured concentrations of COCs during this sampling event.

WELL

TCE (pg/L)

CIS-1,2-DCE (pg/L)

VC (pg/L)

Adjacent to the Former TCE Transfer Pipeline Trench

FAG-22

379

206

30.8

FAG-31

726

210

<1.7

FAG-56

8.9

83.2

0.25 J

FAG-73

22.8

44.2

11.0

South of the Former TCE Transfer Pipeline Trench

FAG-34

582

221

2.9 J

FAG-35

537

111

0.95 J

FAG-36

455

168

<1.7

FAG-85

252

367

53.8

Southwest of Service Building and Southern FAG Bearings Property Line

FAG-50

2,050

157

<4.2

MNA Water Quality Indicator Parameters

The field measured parameters recorded at the conclusion of purging in uppermost
groundwater wells during the 2022 sampling event are provided on Table 3-2 with ranges of
each summarized as follows:

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•	pH ranged from 5.05 to 8.42 standard units (SU) (FAG-33 and FAG-32,
respectively);

•	SC ranged from 52.7 to 672 microsiemens per centimeter (pS/cm) (FAG-43 and
FAG-22, respectively);

•	ORP ranged from -115.9 to 309 millivolts (mV) (RI-MW2 and FAG-50, respectively);

•	DO ranged from 1.42 to 8.02 milligrams per liter (mg/L) (FAG-85 and FAG-31,
respectively);

•	Ferrous Iron ranged from non-detect (FAG-46, FAG-62, RI-MW1, FAG-56, FAG-34,
FAG-35 and FAG-36) to 3.75 mg/L (FAG-73); and

•	Temperature ranged from 15.2 to 21.4°C (FAG-50 and FAG-36, respectively).

The laboratory-measured concentrations from uppermost wells during the 2022 sampling
event are provided on Table 3-4. The number of samples with detected concentrations and
concentration ranges are summarized in the following table.

ANALYTE

NUMBER OF DETECTIONS

DETECTED CONCENTRATION RANGE

Nitrate as N

13 of 14 samples

0.08 J to 1.5 mg/L

Sulfate

14 of 14 samples

1.3 to 36.7 mg/L

Chloride

18 of 18 samples

1.6 to 26.1 mg/L

Methane

5 of 14 samples

7.8 J to 619 pg/L

Ethane

1 of 14 samples

14.1 pg/L

Ethene

1 of 14 samples

8.9 J pg/L

Iron

14 of 14 samples

23.5 J to 36,300 pg/L

3.5.2 Mississippian Aquifer Wells

A discussion of the parameters detected in groundwater samples collected from the ten
monitoring wells screened within the deeper Mississippian Aquifer is presented below.

VOC Analysis

Three VOCs (TCE, cis-l,2-DCE and VC) were detected in at least one of the groundwater
samples collected from the Mississippian Aquifer wells from the 2022 sampling event.
Concentration ranges and the number of samples in which these VOCs were detected are
summarized in the following table.

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ANALYTE

NUMBER OF DETECTIONS

DETECTED CONCENTRATION RANGE

TCE

10 of 10 samples

1.6 to 1,160 pg/L

cis-l,2-DCE

9 of 10 samples

0.28 J to 268 pg/L

VC

1 of 10 samples

28.5 pg/L

One well from the Mississippian Aquifer required dilution by the analytical laboratory for
VOC analysis (FAG-AW4 had a lOx dilution); however, this did not affect the number of
detections summarized in the above table since none of the compounds were non-detect
due to the elevated detection limits.

The following table summarizes COC concentrations measured in Mississippian Aquifer wells
from the 2022 sampling event with the general locations of each provided:

WELL

TCE(pg/L)

CIS-1,2-DCE (pg/L)

VC (pg/L)

South of the Former TCE Transfer Pipeline Trench

FAG-AW4

1,160

268

28.5

Northwest Corner of FAG Bearings Property

FAG-05

18.7

2.6

<0.17

FAG Bearings Southern Property Line

FAG-88

7.0

1.6

<0.17

FAG-89

8.6

1.3

<0.17

FAG-11

2.3

0.66 J

<0.17

Offsite Wells Nearest to FAG Bearings Property

RI-MW5

15.6

0.92 J

<0.17

RI-MW6

64.2

9.4

<0.17

RI-MW9

2.0

0.28 J

<0.17

Offsite Wells Furthest from FAG Bearings Property

RI-MW7

21.7

3.2

<0.17

RI-MW8

1.6

<0.13

<0.17

MNA Water Quality Indicator Parameters

The field measured parameters recorded at the conclusion of purging in Mississippian
Aquifer wells during the 2022 sampling event are provided on Table 3-2 with ranges of each
summarized as follows:

• pH ranged from 6.99 to 7.54 SU (FAG-05 and RI-MW6, respectively);

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•	SC ranged from 338.5 to 632 |jS/cm (RI-MW6 and FAG-11, respectively);

•	ORP ranged from 16.0 to 127.9 mV (FAG-11 and RI-MW6, respectively);

•	DO ranged from 2.97 to 6.31 mg/L (FAG-11 and RI-MW8, respectively); and

•	Temperature ranged from 15.0° to 17.4°C (FAG-11, FAG-88 and RI-MW5 (15°C) and
FAG-89, respectively).

The laboratory-measured MNA parameter chloride was collected from and detected in each
of the Mississippian Aquifer wells sampled. Results for each well are provided in Table 3-4
and concentrations ranged from 4.9 to 34.5 mg/L (FAG-89 and FAG-05, respectively).

3.5.3 Mississippian Aquifer Spring Surface Water Locations

A discussion of the parameters detected in the two surface water samples collected from
locations slightly over 1.5 miles south of the FAG Bearings property boundary and
precipitation at the time of and preceding the sampling event is presented below.

VOC Analysis

TCE was the only VOC detected in the surface water samples from the 2022 sampling event.
It was measured below the laboratory reporting limit (RL) for this compound (1.0 |jg/L) in
RW-341A (0.60 J |jg/L) and SW-01 (0.92 J |jg/L). This is generally consistent with recent
historic measurements in that TCE has occasionally been detected at very low
concentrations.

MNA Water Quality Indicator Parameters

The field measured parameters recorded at the two surface water locations for the 2022
sampling event are provided in Table 3-2 and summarized as follows:

•	pH was measured at 7.74 SU at SW-01 and 7.62 SU at RW-341A;

•	SC was measured at 364.2 |jS/cm at SW-01 and 357.6 |jS/cm at RW-341A;

•	ORP was measured at 73.0 mV at SW-01 and 82.4 mV at RW-341A;

•	DO was measured at 9.78 mg/L at SW-01 and 11.88 mg/L at RW-341A; and

•	Temperature was measured at 10.7°C at SW-01 and 12.4°C at RW-341A.

The laboratory-measured parameter chloride was collected from both sampling points and
measured at 7.5 and 7.6 mg/L in SW-01 and RW-341A, respectively.

Precipitation Summary

As described in Section 3.3, there was no precipitation the day spring surface water samples
were collected for this sampling event. This is similar to the previous 2021 sampling event
in that there was no precipitation on the day the spring surface water samples were
collected. During the ten days preceding these two sampling events, there was a total of
0.79 inches of precipitation in 2022 and 1.89 inches of precipitation in 2021.

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Analytical results for VOCs from surface water samples were very comparable between the
2022 and 2021 sampling event with only TCE detected at very low concentrations below its
MCL. TCE was measured in RW-341A at an estimated concentration of 0.6 |jg/L in 2022 and
at its reporting limit of 1.0 |jg/L in 2021. TCE was measured in SW-01 at an estimated
concentration of 0.92 |jg/L in 2022 and at 1.3 |jg/L in 2021. Although precipitation totals
prior to sampling in 2021 were over twice that in 2022, the measured concentrations of TCE
in 2021 were slightly higher than 2022. The differences in total precipitation preceding the
2022 and 2021 sampling events did not result in significant variations in the measured
concentrations of TCE.

3.6 DATA QUALITY ASSESSMENT

All field and analytical data were reviewed by Ramboll and independent third party
validation was conducted of the VOC laboratory data, as required by the SAP and Quality
Assurance Project Plan (QAPP). Review and validation findings are described below.

3.6.1	Field Data

Field data were collected and validated according to the RAWP and SAP. The field data and
documentation were evaluated against the following criteria, as appropriate:

•	Samples were collected at the specified locations identified in the RAWP and SAP;

•	Field instrumentation calibration and QA/QC checks on equipment occurred at the
intervals specified in the QAPP. Completed calibration logs from this sampling event
are provided in Appendix B; and

•	Sample documentation protocol and chain-of-custody protocols in the RAWP and SAP
were followed.

3.6.2	Laboratory Analytical Data

In accordance with the Amended RAWPs, all VOC analytical results and associated
laboratory data (SW846 5030B/8260B) received Stage 2A data validation by Environmental
Standards, Inc. (ESI), an independent data validation firm.

During the validation process, data qualifiers assigned by the analytical laboratory were
reviewed by ESI and additional data validation qualifiers were assigned to the results by
ESI, as necessary. These qualifiers indicate potential limitations on use of the data. In
addition, data qualifier codes and bias codes were added to the results to indicate the
reason(s) for qualification and the associated bias direction, if discernible. The laboratory
qualifiers and ESI quality assurance review and validation qualifiers are included with the
analytical reports package provided in Appendix D.

An equipment blank sample (EB-01) was collected following decontamination of the site
dedicated piston pump using laboratory supplied deionized water. The laboratory analytical
results did not indicate any cross-contamination of the sampling equipment tested.

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Laboratory-provided trip blank samples accompanied each shipment of samples to the
laboratory and analytical results did not indicate any cross-contamination of the samples.

The following sections provide a summary of the validation results.

General Usability Assessment

The data quality for VOCs was generally acceptable and the analytical data generated
continues to be adequate for determining NCWS conditions.

The overall quality of analytical data is inferred from the quantitative and qualitative data
quality indicators of reporting limits (RLs), accuracy, precision, completeness,
representativeness and comparability.

Validation of data are generally presented in two categories; reporting and procedural. No
reporting issues were noted by the QA review while a single procedural issue was noted.
The observed procedural issue was associated with preservation of the VOC sample for FAG-
34-W-17. The laboratory includes preservative in the VOC bottle ware such that when
sample is added the pH is reduced to below 2. However, the pH of this sample measured by
the laboratory upon receipt was noted to be 6. VOC samples with a pH greater than 2 are to
be analyzed within 7 days of collection but the laboratory did not analyze the sample within
this timeframe nor did they adjust the pH upon receipt and the validator identified
procedural discrepancy which could have biased the results low.

A general overall assessment of each of the data quality assurance objectives is provided in
the following:

•	RLs: During the sampling event, the minimum RLs required were attained on
undiluted samples. Elevated target analyte concentrations necessitated dilutions for
several samples. In such instances, the reviewer selected the result for each target
analyte, corresponding to the analysis run with the least dilution. All other analytes
were reported from the undiluted analysis. The laboratory reported results for VOCs
relative to RLs and method detection limits (MDLs). Results measured below the RL
but above the MDL were qualified by the laboratory as estimated values.

•	Accuracy: Accuracy is a measure of bias in a measurement system. The closer the
value of the measurement agrees with the true value, the more accurate the
measurement. This was expressed as the percent recovery of laboratory control
samples (LCSs), MS/MSDs and surrogates.

•	Surrogate spike recoveries, MSD and LCS results for COCs satisfied the applicable
evaluation criteria for accuracy.

•	Precision: Precision is a measure of repeatability. The MS/MSD results for VOCs and
the field duplicate relative percent difference (RPD) results satisfied applicable
precision criteria for COCs. As such, the overall level of precision demonstrated is
considered to be acceptable.

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•	Completeness: Completeness is a measure of the number of valid measurements
obtained in relation to the total number of measurements planned. Completeness is
expressed as the percentage of valid or usable measurements to planned
measurements. All data are considered usable as qualified. As such, the
completeness for the 2022 sampling event is 100%, which meets the QAPP-listed
completeness requirement of 90% or greater.

•	Representativeness: Representativeness is a qualitative parameter which expresses
the degree to which sample data accurately and precisely represents a characteristic
of a population, parameter variations at a sampling point or an environmental
condition. The agreement between the field duplicate results was used to assess
representativeness. The duplicate results from the 2022 sampling event indicate
general agreement and the samples collected are adequately representative of the
medium sampled.

•	Comparability: In essence, comparability was maintained by consistency in sampling
conditions, selection of sampling procedures, sample preservation methods (with the
exception of the previously noted preservation issue associated with the VOC sample
for FAG-34-W-17), analytical methods and data reporting units.

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This section provides a discussion of the static groundwater levels as well as the laboratory
analytical and field-measured results for samples collected from the two water bearing units
and down-gradient surface water locations. Data from the 2022 monitoring event, as well as
previously collected sample data from the RA have been used to evaluate COC
concentration trends and attenuation.

4.1 GROUNDWATER LEVELS

A summary of static water level measurements and calculated elevations from the 2022
sampling event are provided in Table 3-1. Following is a discussion of the results for the two
water-bearing units.

4.1.1	Uppermost Groundwater

SWLs ranged from approximately 2.21 feet below ground surface (bgs) in FAG-74 located
adjacent to the former TCE pipeline trench to 45.71 feet bgs in FAG-47 located on the FAG
Bearings property southwest of the Service Building. Groundwater elevations ranged from
approximately 997.80 feet amsl in RI-MW1 located on Moorehead Drive south of the FAG
Bearings property to 1,051.14 feet amsl in FAG-74 located adjacent to the former TCE
pipeline trench on the FAG Bearings property. Groundwater elevations calculated for
uppermost groundwater wells are provided on Figure 3-2.

These relative measurements are generally consistent with uppermost groundwater levels
from previous sampling events and are indicative of ongoing consistent groundwater flow
patterns with respect to the NCWS.

4.1.2	Mississippian Aquifer

SWLs on FAG Bearings property ranged from approximately 34.03 to 42.05 feet bgs (FAG-
05 and FAG-11, respectively). This does not include the SWL measured in angled well FAG-
AW4.1 SWLs south of the FAG Bearings property in the Villages of Silver Creek and Saginaw
ranged from approximately 2.76 to 83.76 feet bgs (RI-MW-8 and RI-MW-7, respectively).
Groundwater elevations ranged from 1,003.47 feet amsl in FAG-05 in the northwestern
portion of the FAG Bearings property to a low of approximately 935.89 feet amsl in RI-MW8
near the intersection of Saginaw Road and South Duquesne Road in the Village of Saginaw
at the southernmost boundary of the NCWS. Groundwater elevations calculated for
Mississippian Aquifer wells are provided on Figure 3-3.

These relative measurements are generally consistent with Mississippian Aquifer
groundwater levels from previous sampling events and are indicative of ongoing consistent
groundwater flow patterns with respect to the NCWS.

1 FAG-AW4 was drilled and constructed at an approximate 30 degree angle from vertical.

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4.2 COC TEMPORAL TREND ANALYSIS

Ramboll utilizes the Mann-Kendall non-parametric test (Gilbert 1987) to determine temporal
trends of the measured concentrations of COCs in the water samples collected. This test
evaluates whether values tend to increase or decrease over time through essentially a
monotonic trend regression analysis based on the idea that a lack of trend would fluctuate
randomly about a constant mean level with no apparent upward or downward pattern.

Because Mann-Kendall is a non-parametric test, it is not dependent upon the magnitude of
data, distribution of the data (does not have to have a normal distribution), missing data
from a particular sampling event nor spacing of monitoring events. Mann-Kendall assesses
whether a time-ordered data set exhibits an increasing or decreasing trend, at a
predetermined level of significance.

Ramboll had been utilizing the 3-tiered monitoring optimization (3TMO) software tool to
implement the Mann-Kendall tests and calculate temporal trends. However, the 3TMO tool is
not being updated to run on modern software and is no longer being supported. In order to
provide consistent trend analyses moving forward, Ramboll has transitioned to a Python
software tool to calculate temporal trends using the same Mann-Kendall non-parametric test
calculations which had been run by 3TMO. Datasets from previous reports were analyzed
through the new tool and validated that the trend results are the same as those returned by
3TMO.

The input dataset used for calculation consists of the tabulated concentrations of the COCs
(TCE, cis-l,2-DCE and VC) for each individual well in chronological order. Mann-Kendall
statistical analysis is then performed on each well using these concentrations via the python
tool, resulting in a temporal trend for each COC for each individual well. The temporal
trends for each constituent per well are tabulated and returned as an output file.

The applicable outcomes of the temporal trend analysis performed are as follows:

•	Increasing: Statistically significant increasing trend for concentrations (>95%
confidence);

•	Probably Increasing: Statistically significant increasing trend for concentrations (90-
95% confidence);

•	Stable: No statistically significant trend for concentrations along with low variability
for results (Coefficient of Variance <1);

•	No Trend: No statistically significant trend for concentrations along with high
variability for results (Coefficient of Variance >1);

•	Probably Decreasing: Statistically significant decreasing trend for concentrations (90-
95% confidence);

•	Decreasing: Statistically significant decreasing trend for concentrations (>95%
confidence);

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•	Not Detected (ND): Constituent has not been detected during the time period
analyzed; and

•	Less than the Practical Quantitation Limit (PQL): Concentration was detected in the
most recent sampling event below the PQL but above the calculated MDL, resulting in
an estimated concentration.

Following are summaries of the temporal trend analyses conducted for the two monitored
groundwater units. The temporal trend analyses are provided for two timeframes,
specifically:

•	The full MNA data set for each well which commences with the 2008 sampling event.
The input data set and output from this analysis are provided in Appendix E-l; and

•	Recent MNA data set for each well from the eight most recent sampling events. The
input data set and output from this analysis are provided in Appendix E-2.

The full MNA data set provides a summary of trends commencing shortly after
implementation of multiple full-scale in-situ chemical oxidation (ISCO) treatments of the
identified source of impact to the Mississippian Aquifer, the former TCE pipeline trench. The
smaller data set provides a review of results from a more recent time frame.

4.2.1	Full MNA Data Set

Analyses conducted of the full groundwater data set through the most recent 2022 sampling
event are detailed in the following sections for uppermost groundwater and Mississippian
Aquifer wells and surface spring water locations.

4.2.2	Uppermost Groundwater/Bedrock Interface Wells

The outcomes of the temporal trend analysis for COCs from the full MNA data set of
uppermost groundwater wells, the relative locations of the wells (displayed on Figure 3-4A)
and the total number of samples included for the analysis are provided in the following
table:

SAMPLE

NUMBER

TEMPORAL TREND

LOCATION

OF
SAMPLES

TCE

CIS-1,2-DCE

vc

Northwest Corner of FAG Bearings Property

FAG-43

17

Decreasing

Decreasing

ND

Adjacent to Former TCE Transfer Pipeline Trench

FAG-22

17

Stable

Decreasing

Decreasing

FAG-31

17

Stable

Increasing

Stable

FAG-32

17

Stable

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SAMPLE

NUMBER

TEMPORAL TREND

LOCATION

OF
SAMPLES

TCE

CIS-1,2-DCE

VC

FAG-56

17

Stable

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Of the 11 wells located adjacent to or south of the former pipeline trench, two showed an
increasing trend for TCE (FAG-33 and FAG-36, both located south of the former pipeline
trench), three showed an increasing trend for cis-l,2-DCE (FAG-31, located adjacent to the
former pipeline trench and FAG-33 and FAG-36, located south of the former pipeline trench)
and one showed an increasing trend for VC (FAG-85, located south of the former pipeline
trench). FAG-50 (located southwest of the facility buildings) showed a probably increasing
trend for cis-l,2-DCE. These were the only wells and COCs in the uppermost groundwater
with increasing/probably increasing trends.

Measured Concentration Changes Over Time

In addition to considering statistical temporal trends of MNA sampling, the general change
in measured concentrations of TCE over time have also been reviewed. For this analysis, the
maximum historic concentrations of TCE (prior to 2008) were compared to concentrations
from the 2022 sampling event and the percentage change in the concentration was
calculated. The percentage change in the uppermost groundwater wells were calculated for
specific areas based on their relative locations with respect to the former trench and are
summarized as follows:

•	Wells located adjacent to former pipeline trench; 92% overall decrease in TCE;

•	Wells located south of the former pipeline trench; 50% overall decrease in TCE;

•	Wells located southwest of service building and near FAG Bearings southern property
line; 84% overall decrease in TCE; and

•	Wells located in the Village of Silver Creek; 17% overall increase in TCE.

Significant overall percentage decreases in measured concentrations of TCE in upper
groundwater has occurred since sampling commenced at the NCWS. Decreases have been
most significant for wells associated with measuring conditions relative to the former TCE
pipeline trench source which was subjected to significant remediation by ISCO.

FAG-32 (located adjacent to the former trench) was previously noted to have a significant
decrease in TCE between the 2018 and 2020 sampling events (1,920 and <1.0 ug/L,
respectively) and the 2021 and 2022 TCE levels remained at relatively low concentrations
(183 and 49.5 |jg/L, respectively). A specific reason for this recent decrease is not clear;
however, this well did have relatively low concentrations of TCE measured prior to 2008.
The ongoing level of TCE will continue to be tracked during future MNA sampling events.

4.2.3 Mississippian Aquifer Wells

The outcomes of the temporal trend analysis for COCs from the full MNA data set of
Mississippian Aquifer wells, the relative locations of the wells (displayed on Figure 3-4B) and
the total number of samples included in the analysis are provided in the following table:

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SAMPLE

NUMBER

TEMPORAL TREND

LOCATION

OF
SAMPLES

TCE

CIS-1,2-DCE

VC

FAG Bearings Property

FAG-AW4

17

Probably Increasing

Increasing

Increasing

FAG-05

17

Decreasing

Decreasing

ND

FAG-11

17

Decreasing

Decreasing

ND

FAG-88

17

Decreasing

Decreasing

ND

FAG-89

17

Stable

Stable

ND

South of FAG Bearings Property (Villages of Silver Creek and Saginaw)

RI-MW5

17

Stable

Stable

ND

RI-MW6

17

Stable

Stable

ND

RI-MW7

17

Increasing

Increasing

ND

RI-MW8

17

Decreasing

ND

ND

RI-MW9

17

Decreasing

Decreasing

ND

The majority of COCs detected have decreasing temporal trends since MNA sampling
commenced. A summary of the 30 potential outcomes of the temporal trend analysis (10
wells and three COCs) is as follows:

•	Ten non-detect outcomes (predominately VC) or 33% of potential outcomes.

•	Nine decreasing trend outcomes or 30% of potential outcomes (45% excluding non-
detect outcomes).

•	Six stable trend outcomes or 20% of potential outcomes (30% excluding non-detect
outcomes).

•	Five increasing or probably increasing trend outcomes or 17% of potential outcomes
(25% excluding non-detect outcomes. These consist of two for TCE, two for cis-1,2-
DCE and one for VC.

Of the five wells located on the FAG Bearings property, one well had a probably increasing
trend for TCE and increasing trends for cis-l,2-DCE and VC (FAG-AW4). Of the five wells
located south of the FAG Bearings property, only one had an increasing trend for TCE or cis-
1,2-DCE (RI-MW7) and all of the wells were non-detect for VC.

Measured Concentration Changes Over Time

In addition to considering statistical temporal trends of MNA sampling, the general change
in measured concentrations of TCE over time have also been reviewed. For this analysis, the
maximum historic concentrations of TCE (prior to 2008) were compared to concentrations

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from the 2022 sampling event and the percentage change in the concentration was
calculated. The percentage change in the Mississippian Aquifer wells were calculated for
specific areas based on their relative locations with respect to the FAG Bearings property
and are summarized as follows:

•	Wells located on the FAG Bearings Property; 10% overall decrease in TCE; and

•	Wells located off the FAG Bearings Property in the Villages of Silver Creek and
Saginaw; 59% overall decrease in TCE.

During this time period, an overall percentage decrease in measured concentrations of TCE
in Mississippian Aquifer wells has occurred since sampling commenced at the NCWS, with
the most significant decrease beyond the FAG property.

4.2.4 Mississippian Aquifer Spring Surface Water Locations

The outcomes of temporal trend analysis for COCs at the two surface water spring locations
utilizing the full MNA data set are provided in the following table:

SAMPLE

NUMBER

TEMPORAL TREND

LOCATION

OF
SAMPLES

TCE

CIS-1,2-DCE

VC

SW-01

17

Stable

ND

ND

RW-341A

17

Stable

ND

ND

Of the three COCs, two (cis-l,2-DCE and VC) remain non-detect in each surface water
spring location and the remaining COC (TCE) has a stable trend in each. The Mississippian
Aquifer serves as the primary source for perennial water flow for these surface water
sampling locations.

The only COC detected during the 2022 sampling event was TCE measured at estimated
concentrations of 0.92 J pg/L in SW-01 and 0.60 J pg/L in RW-341A. Both concentrations
fall below the laboratory reporting limit of 1 pg/L but above the calculated laboratory MDL of
0.21 pg/L and remain below the goal concentration for the Mississippian Aquifer of 5 pg/L.

Measured Concentration Changes Over Time

In addition to considering statistical temporal trends of MNA sampling, the general change
in measured concentration of TCE over time has also been reviewed. For this analysis the
maximum historic concentrations of TCE (prior to 2008) were compared to concentrations
from the 2022 sampling event and the percentage change in the concentration was
calculated. A 90% overall percentage decrease in TCE was calculated for the Mississippian
Aquifer sourced spring water locations.

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4.2.5	Recent MNA Data Set

Analyses conducted of relatively recent groundwater data, in this case consisting of the
eight most recent analytical results, up to and including the 2022 sampling event, are
detailed in the following sections for uppermost groundwater and Mississippian Aquifer wells
and surface spring water locations.

4.2.6	Uppermost Groundwater/Bedrock Interface Wells

The outcomes of the temporal trend analysis for COCs utilizing the eight most recent MNA
sampling results of uppermost groundwater wells, the relative locations of the wells
(displayed on Figure 3-4A) and the date range represented are provided in the following
table:

SAMPLE

DATE RANGE

TEMPORAL TREND

LOCATION

TCE

CIS-1,2-DCE

vc

Northwest Corner of FAG Bearings Property

FAG-43

5-13 to 5-22

No Trend

No Trend

ND

Adjacent to Former TCE Transfer Pipeline Trench

FAG-22

5-13 to 5-22

Decreasing

Decreasing

Stable

FAG-56

5-13 to 5-22

Probably Decreasing

Probably Decreasing


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SAMPLE

DATE RANGE

TEMPORAL TREND

LOCATION

TCE

CIS-1,2-DCE

VC

Village of Silver Creek

RI-MW1

5-13 to 5-22

Stable

Decreasing

ND

RI-MW2

5-13 to 5-22

ND

ND

ND

The majority of COCs detected utilizing the eight most recent data points for each well have
probably decreasing/decreasing temporal trends. A summary of the 54 potential outcomes
of the temporal trend analysis (18 wells and three COCs) is as follows:

•	Twelve non-detect outcomes (predominately VC) or 22% of the potential outcomes;

•	Three 
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•	Wells located adjacent to former pipeline trench; 76% overall decrease in TCE;

•	Wells located south of the former pipeline trench; 20% overall decrease in TCE;

•	Wells located southwest of service building and near FAG Bearings southern property
line; 25% overall increase in TCE (all of these wells decreased in relative
concentration except FAG-50 which had a relative increase); and

•	Wells located in the Village of Silver Creek; 37% overall decrease in TCE.

During this time period, overall percentage decreases in measured concentrations of TCE in
upper groundwater wells have occurred at the NCWS, with the exception of the wells
monitoring conditions southwest of the service building and near the FAG Bearings southern
property boundary.

4.2.7 Mississippian Aquifer Wells

The outcomes of the temporal trend analysis for COCs utilizing the eight most recent MNA
sampling results of Mississippian Aquifer wells, the relative locations of the wells (displayed
on Figure 3-4B) and the date range represented are provided in the following table:

SAMPLE

DATE RANGE

TEMPORAL TREND

LOCATION

TCE

CIS-1,2-DCE

vc

FAG Bearings Property

FAG-AW4

5-13 to 5-22

Stable

Stable

Increasing

FAG-05

5-13 to 5-22

Decreasing

Decreasing

ND

FAG-11

5-13 to 5-22

No Trend

Stable

ND

FAG-88

5-13 to 5-22

Stable

Decreasing

ND

FAG-89

5-13 to 5-22

Probably Decreasing

Stable

ND

South of FAG Bearings Proi

aerty (Villages of Silver Creek and Saginaw)

RI-MW5

5-13 to 5-22

Stable


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•	Ten non-detect outcomes (predominately VC) or 33% of potential outcomes.

•	One 
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SAMPLE

DATE RANGE

TEMPORAL TREND

LOCATION

TCE

CIS-1,2-DCE

VC

SW-01

5-13 to 5-22

Stable

ND

ND

RW-341A

5-13 to 5-22

Stable

ND

ND

TCE has a stable temporal trend at each surface water spring location during this timeframe
at concentrations that have been either non-detect or below the goal concentration for the
Mississippian Aquifer while cis-l,2-DCE and VC remain non-detect. The Mississippian Aquifer
serves as the primary source for perennial water flow for these surface water sampling
locations.

Measured Concentration Changes Over Time

In addition to considering statistical temporal trends of MNA sampling, the general change
in measured concentrations of TCE over time have also been reviewed. For this analysis, the
historic concentrations of TCE in the data set of each surface spring water location
representing the eighth most recent sampling event were to be compared to concentrations
from the 2022 sampling event and the percentage change calculated. However, the 2022
results for TCE at each location were both at estimated concentrations below the RL while
the historic data sets to be utilized for comparison were both below the RL with no
estimated concentration provided by the laboratory (as directed in the QAPP at that time).
Consequently, an accurate calculation of the percentage change over time could not be
completed because the data sets are not fully comparable. It should be noted that
concentrations at both locations remained either non-detect or below the goal concentration
of the Mississippian Aquifer throughout this timeframe.

4.3 MNA WATER QUALITY INDICATOR ANALYSIS

The dominant mechanism for natural attenuation of TCE is biodegradation in the uppermost
groundwater in the vicinity of the former TCE pipeline trench source is biodegradation. The
dominant mechanism for natural attenuation in uppermost groundwater relatively distant
from the former TCE pipeline trench source and in the deeper Mississippian Aquifer is
hydrodynamic dispersion.

Measurement of MNA water quality indicator parameters in uppermost groundwater wells in
the vicinity of the former TCE pipeline trench included certain biodegradation geochemical
indicator parameters while uppermost groundwater wells beyond the former pipeline trench.
Mississippian Aquifer wells and spring surface water were sampled for an abbreviated list of
geochemical parameters since hydrodynamic dispersion is the dominant natural attenuation
mechanism. Summaries of the MNA parameter results is provided in the following sections
based on the groundwater unit measured and the dominant natural attenuation process.

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4.3.1 Uppermost Groundwater Wells

The MNA sampling event conducted in 2022 included 14 uppermost groundwater wells that
were sampled for biodegradation parameters (consisting of six adjacent to the former
pipeline trench, five located south of the pipeline trench and three to the southwest of the
former pipeline trench) and four sampled relative to hydrodynamic dispersion parameters
(consisting of two wells located furthest west and two well located furthest south of the
former pipeline trench). These are specified in Table 3-3.

All of the wells had field-measured well stabilization parameters recorded and the
laboratory-measured parameter chloride collected while the wells most subject to
biodegradation were additionally sampled for the field-measured parameter ferrous iron and
the laboratory-measured parameters nitrate, sulfate, methane, ethane, ethene and iron.
Following is a summary review of the results of the field and laboratory-measured indicator
parameters based on the locations of the wells relative to the former TCE pipeline trench.

Adjacent to Former Pipeline Trench (Biodegradation')

The six uppermost groundwater wells located most immediately adjacent to the former TCE
pipeline trench and sampled in 2022 are FAG-22, FAG-31, FAG-32, FAG-56, FAG-73 and
FAG-74.

Field-Measured Parameters

•	pH was relatively neutral and ranged from 6.33 to 7.35 (FAG-56 and FAG-74,
respectively) with the exception of a slightly elevated pH (8.42) measured at FAG-
32. Neutral pH conditions are more conducive for biodegradation activities to take
place.

•	DO ranged from 2.29 to 8.02 mg/L (FAG-73 and FAG-31, respectively). Lower DO
measurement were associated with those wells in which a closed loop flow through
cell was utilized for field measurements as compared to those in which one was not
used due to the purging methodology. DO levels below approximately 0.5 mg/L are
more indicative of anaerobic conditions in which reductive dechlorination processes
occur.

•	ORP ranged from -38.1 to 153.8 mV (FAG-73 and FAG-56, respectively). Lower
levels of ORP (particularly negative values) are indicative of more active
biodegradation.

•	Ferrous Iron ranged from 0.0 to 3.75 mg/L (FAG-56 and FAG-73, respectively).
Levels above 1 mg/L are indicative of more active biodegradation processes.

Laboratory-Measured Parameters

•	Nitrate remained below 1 mg/L and ranged from <0.079 to 0.85 mg/L (FAG-73 and
FAG-31, respectively) with the exception of FAG-22 which was measured at 1.5
mg/L. It has been noted that FAG-22 typically has slightly higher nitrate

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measurements than the other wells in this grouping. Levels below 1 mg/L are
indicative of ongoing denitrification degradation.

•	Sulfate remained below 20 mg/L and ranged from 6.9 to 18.0 mg/L (FAG-74 and
FAG-22, respectively) with the exception of FAG-56 measured at 36.7 mg/L. It has
been noted that FAG-56 typically has slightly higher sulfate measurements than the
other wells in this grouping. Levels below 20 mg/L are indicative of biodegradation
reducing conditions.

•	Chloride was relatively elevated compared to an assumed background level of
approximately 2 mg/L and ranged from 4.5 to 26.1 mg/L (FAG-32 and FAG-56,
respectively) while FAG-74 was measured slightly lower at a concentration of 1.6
mg/L. Elevated concentrations of chloride are indicative of active biodegradation.

•	Methane remained below its RL of 10 |jg/L with the exception of FAG-22 and FAG-73
which were measured at 29.6 and 558 |jg/L, respectively. Elevated concentrations of
methane are indicative of active biodegradation. Methane concentrations above 500
|jg/L not only indicate very active biodegradation, but also the consequent
production and potential accumulation of the end stage degradation compound VC.
In recent MNA sampling events, FAG-73 has generally approached this level. During
this sampling event, FAG-73 had detectable concentrations of VC at a relatively low
concentration (11.0 |jg/L).

•	Ethane and Ethene remained below their RLs of 10 |jg/L in the wells sampled, with
the exception of FAG-73 which had a measured concentration of ethane (14.1 |jg/L).
These parameters are subject to very rapid biodegradation and their relative absence
as indicator compounds is not uncommon.

•	Iron was detected in each of the wells sampled with total concentrations ranging
from 124 to 36,300 |jg/L (FAG-22 and FAG-74, respectively).

Ferric iron serves as an electron acceptor which can be reduced to form ferrous iron. The
relative concentration of ferric iron can be determined by subtracting the measured level of
ferrous iron from the measured level of total iron. Positive levels of ferric iron are indicated
for three of the six wells in this grouping (FAG-56, FAG-73 and FAG-74).

South of Former Pipeline Trench (Biodegradation')

The five uppermost groundwater wells located south of the former pipeline trench and
sampled for biodegradation parameters in 2022 are FAG-33, FAG-34, FAG-35, FAG-36 and
FAG-85. These wells are located approximately 200 feet south of the former pipeline trench
to monitor uppermost groundwater primarily in a channelized bedrock depression.

Field-Measured Parameters

•	pH was relatively neutral and ranged from 6.68 to 7.19 (FAG-85 and FAG-35,
respectively). A slightly low pH (5.05) was measured in FAG-33 which generally has

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slightly lower pH measurements relative to this grouping of wells. Neutral pH is more
conducive for biodegradation activities to take place.

•	DO ranged from 1.42 to 3.04 mg/L (FAG-85 and FAG-33, respectively). These levels
are consistent compared to those measured during recent MNA sampling events,
with the exception of the 2021 MNA sampling event in which levels were slightly
elevated relative to other recent sampling events. Levels below approximately 0.5
mg/L are more indicative of anaerobic conditions in which reductive dechlorination
processes occur.

•	ORP was positive and ranged from 12 to 135.7 mV (FAG-34 and FAG-33,
respectively) with the exception of FAG-85 which was measured at -92.1 mV. Lower
levels of ORP (particularly negative values) are indicative of more active
biodegradation.

•	Ferrous Iron ranged from 0.00 to 2.4 mg/L (FAG-34, FAG-35 and FAG-36 and FAG-
85, respectively). Levels above 1 mg/L are indicative of more active biodegradation
processes.

Laboratory-Measured Parameters

•	Nitrate remained below 1 mg/L and ranged from 0.08 J to 0.19 mg/L (FAG-33 and
FAG-34, respectively) with the exception of FAG-35 which was measured at 1.4
mg/L. Levels below 1 mg/L are indicative of ongoing denitrification degradation.

•	Sulfate ranged from 1.3 to 15.3 mg/L (FAG-33 and FAG-35, respectively). Levels
below 20 mg/L are indicative of biodegradation reducing conditions.

•	Chloride was generally elevated as compared to an assumed background of
approximately 2 mg/L and ranged from 12.8 to 17.4 mg/L (FAG-85 and FAG-35,
respectively). Elevated concentrations of chloride are indicative of active
biodegradation.

•	Methane remained below its RL of 10 |jg/L in two wells (FAG-33 and FAG-34), with
exceedances at FAG-35 (25.2 |jg/L), FAG-36 (7.8 J |jg/L) and FAG-85 (619 |jg/L).
Elevated concentrations of methane are indicative of active biodegradation. Although
methane is often detected in FAG-85, the 2021 measured concentration (1,590 |jg/L)
was significantly elevated as compared to results from other recent MNA sampling
events. Concentrations in FAG-85 will be tracked in future sampling events to
determine ongoing levels. The end stage biodegradation compound VC was
measured at 53.8 |jg/L which is the highest level measured in this well since
monitoring commenced.

•	Ethane and Ethene remained below their RLs of 10 |jg/L in the wells sampled, with
the exception of an estimated concentration of ethene measured at FAG-85 (8.9 J
|jg/L). These parameters are subject to very rapid biodegradation and their relative
absence as indicator compounds is not uncommon.

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• Iron was detected in each of the wells sampled with total concentrations ranging
from 23.5 J to 9,650 |jg/L (FAG-35 and FAG-85, respectively).

Ferric iron serves as an electron acceptor which can be reduced to form ferrous iron. The
relative concentration of ferric iron can be determined by subtracting the measured level of
ferrous iron from the measured level of total iron. Positive levels of ferric iron are indicated
for all five wells in this grouping.

Southwest of Service Building (BiodearadatiorO

The three uppermost groundwater wells located southwest of the Service Building and
sampled for biodegradation parameters in 2022 are FAG-47, FAG-50 and FAG-62. These
wells are located from approximately 500 to 750 feet southwest of the former pipeline
trench (FAG-62 and FAG-47, respectively).

Field-Measured Parameters

•	pH was slightly below neutral and ranged from 5.32 to 6.58 (FAG-50 and FAG-62,
respectively). Neutral pH is more conducive for biodegradation activities to take
place.

•	DO ranged from 3.19 to 6.31 mg/L (FAG-47 and FAG-50, respectively). These levels
are consistent compared to those measured during recent MNA sampling events.
Levels below approximately 0.5 mg/L are more indicative of anaerobic conditions in
which reductive dechlorination processes occur.

•	ORP was positive and ranged from 22.3 to 309.2 mV (FAG-62 and FAG-50,
respectively). Lower levels of ORP (particularly negative values) are indicative of
more active biodegradation.

•	Ferrous Iron ranged from 0.0 to 0.5 mg/L (FAG-62 and FAG-47, respectively) and
are generally similar to those measured during recent MNA sampling events. Levels
above 1 mg/L are indicative of more active biodegradation processes.

Laboratory-Measured Parameters

•	Nitrate remained below 1 mg/L and ranged from 0.26 to 0.39 mg/L (FAG-62 and
FAG-50, respectively) with the exception of FAG-47 which was measured at 1.2
mg/L. Levels below 1 mg/L are indicative of ongoing denitrification degradation.

•	Sulfate ranged from 7.1 to 13.3 mg/L (FAG-47 and FAG-62, respectively). Levels
below 20 mg/L are indicative of biodegradation reducing conditions.

•	Chloride was generally elevated as compared to an assumed background of
approximately 2 mg/L and ranged from 9.8 to 16.6 mg/L (FAG-50 and FAG-62,
respectively). Elevated concentrations of chloride are indicative of active
biodegradation.

•	Methane remained below its RL of 10 |jg/L in each of the wells. Elevated
concentrations of methane are indicative of active biodegradation.

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•	Ethane and Ethene remained below their RLs of 10 |jg/L in the wells sampled. These
parameters are subject to very rapid biodegradation and their relative absence as
indicator compounds is not uncommon.

•	Iron was detected in each of the wells sampled with total concentrations ranging
from 243 to 23,800 |jg/L (FAG-47 and FAG-50, respectively).

Ferric iron serves as an electron acceptor which can be reduced to form ferrous iron. The
relative concentration of ferric iron can be determined by subtracting the measured level of
ferrous iron from the measured level of total iron. Positive levels of ferric iron are indicated
for two of the three wells in this grouping (FAG-56 and FAG-62).

Wells Sampled for Hvdrodvnamic Dispersion

The four remaining uppermost groundwater wells were sampled for hydrodynamic
dispersion parameters, specifically; FAG-43, FAG-46, RI-MW1 and RI-MW2. These wells are
located at a more significant distance from the former TCE pipeline trench source as
compared to the wells sampled for biodegradation parameters, consequently they are
scheduled to be sampled for hydrodynamic dispersion parameters. FAG-43 is located in the
northwest portion of the FAG Bearings property over 2,000 feet from the former TCE
pipeline trench, FAG-46 is located in the southwest portion of the FAG Bearings property
near the southern property boundary over 1,250 feet from the former TCE pipeline trench
and RI-MW1 and RI-MW2 are located south of FAG-46 beyond the FAG Bearings property
along Moorhead Drive over 1,250 feet from the former TCE pipeline trench.

Field-Measured Parameters

•	pH was generally neutral and ranged from 6.26 to 7.24 (FAG-46 and RI-MW1,
respectively) while the measured pH of FAG-43 (5.47) was lower than the other wells
in this grouping;

•	DO was consistently elevated and ranged from 3.06 to 4.18 mg/L (RI-MW2 and FAG-
43/FAG-46, respectively); and

•	ORP was slightly positive and ranged from 29.9 to 130.1 mV (RI-MW1 and FAG-46,
respectively) with the exception of FAG-43 (-115.9 mV) which was negative.

Laboratory-Measured Parameter

•	Chloride concentration was relatively elevated as compared to an assumed
background of 2.0 mg/L and ranged from 3.7 to 23.3 mg/L (FAG-43 and RI-MW2,
respectively).

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4.3.2 Mississippian Aquifer Wells and Spring Surface Water

The MNA sampling event conducted in 2022 included 10 Mississippian Aquifer wells and two
spring surface water samples sourced from the Mississippian Aquifer all of which were
sampled for hydrodynamic dispersion parameters. Five of the wells are located on the FAG
Bearings property and the remaining five wells and two surface spring water sampling
points are located south of the FAG Bearings property.

All of the wells had field-measured well stabilization parameters recorded and the
laboratory-measured parameter chloride collected. The spring surface water samples had
field-measured parameters recorded at the time of sample collection with the laboratory-
measured parameter chloride also collected. Following is a summary review of the results of
the field and laboratory-measured indicator parameter based on the locations and sources
of the samples.

Wells on FAG Bearings Property

The five Mississippian Aquifer wells located on the FAG Bearings property and sampled in
2022 are FAG-AW4, FAG-05, FAG-11, FAG-88 and FAG-89.

Field-Measured Parameters

•	pH was consistently neutral and ranged from 6.99 to 7.53 (FAG-05 and FAG-89,
respectively);

•	DO was relatively elevated and ranged from 2.97 to 5.6 mg/L (FAG-11 and FAG-89,
respectively); and

•	ORP remained positive and ranged from 16.0 to 115.3 mV (FAG-11 and FAG-05,
respectively).

Laboratory-Measured Parameter

• Chloride concentration ranged from 4.9 to 34.5 mg/L (FAG-89 and FAG-05,
respectively).

Wells South of FAG Bearings Property (Villages of Silver Creek and Saginaw!

The five Mississippian Aquifer wells located south of the FAG Bearings property sampled in
2022 are RI-MW5, RI-MW6, RI-MW7, RI-MW8 and RI-MW9.

Field-Measured Parameters

•	pH was consistently neutral and ranged from 7.05 to 7.54 (RI-MW8 and RI-MW6,
respectively);

•	DO was relatively elevated and ranged from 0.8 to 6.31 mg/L (RI-MW9 and RI-MW8,
respectively); and

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•	ORP ranged from -29.5 to 127.9 mV (RI-MW5 and RI-MW6, respectively).

Laboratory-Measured Parameter

•	Chloride concentrations ranged from 5.9 to 20.5 mg/L (RI-MW7 and RI-MW5,
respectively).

Surface Springs South of FAG Bearings Property

The two Mississippian Aquifer sourced surface spring water samples located off and to the

south of the FAG Bearings property sampled in 2022 are SW-01 and RW-341A.

Field-Measured Parameters

•	pH was relatively neutral in each (7.74 mg/L in SW-01 and 7.62 in RW-341A);

•	DO was highly elevated in each (9.78 mg/L in SW-01 and 11.88 mg/L in RW-341A)
and

•	ORP was positive in each (73.0 mV in SW-01 and 82.4 mg/V in RW-341A).

Laboratory-Measured Parameter

•	Chloride concentrations were nearly identical in each (7.5 mg/L in SW-01 and 7.6
mg/L in RW-341A).

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The conclusions and recommendations for this Annual Report presented below include
review and analysis of the results from 17 rounds of MNA sampling conducted with respect
to the NCWS RA through calendar year 2022.

Based on a review of results documented in this Annual Report, the ongoing sampling
continues to generate consistent and usable data necessary to evaluate the selected remedy
with the following conclusions and recommendations.

Upper Groundwater Wells

•	The primary natural attenuation process in the uppermost groundwater, particularly
in the area adjacent to and south of the former TCE transfer pipeline trench (the
identified sole source of NCWS impact) is biodegradation which continues to actively
reduce the mass of remnant impact.

•	A general comparison of TCE concentrations since sampling of upper groundwater
wells commenced with those from the most recent sampling indicate overall
decreases in TCE in wells located on the FAG Bearings property ranging from a 92%
decrease in wells adjacent to the former pipeline trench to a 50% decrease in wells
located south of the of the former pipeline trench.

•	A general comparison of the most recent eight MNA sampling events in wells located
on the FAG Bearings property indicates an overall decrease in TCE ranging from a
76% decrease in wells located adjacent to the former pipeline trench to a 20%
decrease in wells located south of the former pipeline trench. During this same time
frame, a 25% increase is indicated in wells located southwest of the FAG Service
Building.

•	Many of the MNA parameters are indicative of ongoing biodegradation conditions
which are further supported by the overall reductions in measured remnant impact
adjacent to and south of the former TCE pipeline trench.

•	Temporal trend analysis since MNA sampling commenced identified two specific
uppermost groundwater wells (out of 18 total) with statistically increasing TCE as
follows:

-	The six wells adjacent to the former pipeline trench had stable or decreasing
TCE trends with associated trends in TCE daughter products supportive of
ongoing biodegradation.

-	FAG-33 and FAG-36: Of the five wells monitoring conditions south of the
former pipeline trench location, two (FAG-33 and FAG-36) had calculated
statistically increasing TCE trends. Each well also had an increasing trend for
the TCE daughter product cis-l,2-DCE and not detected VC.

-	The remaining uppermost wells had stable or decreasing TCE trends except
one well in the Village of Silver Creek which was not detected (RI-MW2).

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Associated trends for the TCE daughter product cis-l,2-DCE in each well were
generally similar to those calculated for TCE and the compound VC was
primarily not detected above the PQL or decreasing.

•	Temporal trend analysis for the eight most recent MNA sampling events identified
one specific uppermost groundwater well (out of 18 total) with statistically increasing
TCE as follows:

-	The six wells adjacent to the former TCE pipeline trench had stable or
probably decreasing TCE trends with associated trends in the TCE daughter
product cis-l,2-DCE generally similar and VC generally similar or not
detected.

-	The five wells monitoring conditions south of the former pipeline trench
location had stable TCE trends. Two of these wells had calculated statistically
increasing or probably increasing trends for cis-l,2-DCE (FAG-33 and FAG-85,
respectively).

-	FAG-50 located southwest of the Service Building had a calculated statistically
increasing TCE trend. This well also had a statistically increasing trend for cis-
1,2-DCE and not detected VC.

-	The remaining uppermost wells had stable or decreasing TCE trends except
one well in the Village of Silver Creek which was not detected (RI-MW2) and
one well in the northwest area of FAG Bearings property which had no trend
(FAG-43). Associated trends for the TCE daughter product cis-l,2-DCE in
each well were generally similar to those calculated for TCE and the
compound VC was primarily not detected.

-	Upper groundwater wells providing data with respect to the side and down-
gradient periphery of this plume displayed either stable or decreasing
temporal trends indicative of a stable plume boundary.

Mississippian Aquifer Wells

•	The primary natural attenuation process in the Mississippian Aquifer continues to be
hydrodynamic dispersion which serves to diminish groundwater impact within this
unit.

•	A general comparison of TCE concentrations since sampling of Mississippian Aquifer
wells commenced with those from the most recent sampling event indicate overall
decreases in TCE in wells on FAG Bearings property (10% decrease) and wells south
of the FAG Bearings property (59% decrease).

•	A general comparison of the eight most recent sampling MNA sampling events
indicates an overall increase in TCE in wells on FAG Bearings property (20%
increase) and wells located south of the FAG Bearings property (51%).

December 2022

40

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Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

•	Temporal trend analysis since MNA sampling commenced identified one Mississippian
Aquifer well with a statistically increasing TCE concentration trend and one with a
statistically probably increasing concentration trend as follows:

-	Of the five wells monitoring conditions on the FAG Bearings property, one
(FAG-AW4) had a probably increasing trend for TCE. This well also had
increasing trends for cis-l,2-DCE and VC.

-	The remaining four wells on the FAG Bearings property had stable or
decreasing trends for TCE. The TCE daughter product cis-l,2-DCE had similar
trends in these wells and VC remained not detected.

-	Of the five wells monitoring conditions south of the FAG Bearings property,
one (RI-MW7) had an increasing trend for TCE. This well also had an
increasing trend for cis-l,2-DCE while VC was not detected.

-	The remaining four wells south of the FAG Bearings property had decreasing
or stable TCE trends as well as stable or decreasing trends for cis-l,2-DCE
(except for RI-MW8 which was not detected) while VC was not detected.

•	Temporal trend analysis over the eight most recent sampling events identified one
Mississippian Aquifer well (out of 10 total) with statistically increasing TCE
concentrations trends as follows:

-	Of the five wells monitoring conditions on the FAG Bearings Property, four
wells had either decreasing, probably decreasing or stable trends for TCE,
with FAG-11 having no trend for TCE. Trends were generally similar for cis-
1,2-DCE and not detected for VC, except for FAG-AW4 which had an
increasing VC trend.

-	Of the five wells monitoring conditions south of the FAG Bearings property in
the Villages of Silver Creek and Saginaw, one (RI-MW6) had an increasing
trend for TCE. This well also had an increasing trend for cis-l,2-DCE while VC
was not detected.

-	The remaining four wells south of the FAG Bearings property had stable or
decreasing trends for TCE while cis-l,2-DCE was not detected, stable or less
than the PQL and VC was not detected.

-	Mississippian Aquifer wells providing data with respect to the side and down-
gradient periphery of this plume displayed either stable or decreasing
temporal trends indicative of a stable plume boundary.

Mississippian Aquifer Spring Surface Water

•	The primary natural attenuation process in the two Mississippian Aquifer sourced
spring water locations continues to be hydrodynamic dispersion which serves to
diminish groundwater impact of the source for these spring water surface discharges.

December 2022

41

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Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

•	Of the two spring water sampling points, TCE concentrations in RW-341A have
always remained near or below the RL and below the goal concentration for the
source aquifer while SW-01 has remained near or below the RL and also below the
goal concentration for the source aquifer for two decades.

•	Temporal trend analysis since MNA sampling commenced and for the last eight
sampling events determined that TCE concentrations had a stable trend for both
locations while the daughter products cis-l,2-DCE and VC remained not detected.

•	The two surface water springs sampled (sourced from the Mississippian Aquifer) have
achieved the remediation goal objectives for COCs.

Remedial Actions

As provided in the NCWS ROD, the remedial alternative selected for the NCWS to achieve
remedial action objectives specified for the upper groundwater and Mississippian Aquifer are
MNA and implementation/enforcement of existing regional ICs. Implementation and
activities required for the MNA portion of the chosen alternative are the responsibility of FAG
Bearings.

The remedial action objectives specified for MNA are to:

•	Reduce the concentration of TCE and TCE degradation products in the uppermost
aquifer of the NCWS to concentrations that are protective of the Mississippian Aquifer
as a potable water source with respect to TCE and TCE degradation products; and

•	Return the Mississippian Aquifer water quality at the NCWS to potable conditions,
with respect to TCE and TCE degradation products.

Criteria for effectiveness of MNA towards achieving the objective provided in the ROD and
Second Five Year Summary Report include:

•	ROD: "Should no significant decreasing trend in the levels of TCE be observed in the
Mississippian Aquifer during the first five years of sampling, over a consistent period
of time, a contingency to use ISCO to treat contamination in the uppermost
groundwater will be implemented."

•	Second Five Year Report: "If MNA parameters do not appear to be occurring near the
former trench and/or if a significant decreasing trend in TCE levels is not observed in
the Mississippian Aquifer consider the implementation of ISCO injections."

MNA has been determined to continue to be effective with regard to the NCWS in that the
majority of wells in both the upper groundwater and Mississippian Aquifer show decreasing
trends since monitoring commenced. Decreasing/stable temporal trends of TCE are
associated with the majority of wells in both the upper groundwater and Mississippian
Aquifer since MNA sampling commenced and for the most recent eight sampling events.

December 2022

42

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Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Upper groundwater wells adjacent to the former TCE pipeline trench (the identified sole
source of impact associated with the NCWS) have either stable or decreasing statistical
trends since MNA sampling commenced and for the most recent eight sampling events with
overall total calculated percent decreases in TCE since sampling commenced and for the last
eight sampling events of 91% and 76%, respectively.

However, FAG Bearings recognizes a subset of wells detailed in this report that display
stable temporal trends for specific COCs which exceed goal concentrations as well as a
limited subset of wells that display increasing temporal trends for specific COCs. Based on
these observations and the direction provided by the ROD, FAG Bearings will prepare and
submit a conceptual pilot test work plan to MDNR and USEPA in preparation for conducting
focused in-situ treatment of the uppermost groundwater during calendar year 2023.

The plan will provide for additional in-situ focused source treatment of the former TCE
pipeline trench and will also include pilot scale in-situ treatment of upper groundwater to
confirm effective remediation and efficient treatment amendment delivery methodologies.
These proactive measures will build on previously implemented treatment and testing
conducted at the site including the significant ISCO treatment of the former TCE pipeline
trench as well as preliminary overburden groundwater tracer testing previously conducted at
two locations on FAG Bearings property; 1) within a bedrock valley feature located south of
the pipeline trench and 2) southwest of the FAG Bearings facility buildings. Based on the
results of the treatment and testing, potential modifications and/or upscaling of the
treatment within the upper groundwater may be implemented.

December 2022

43

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Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

December 2022


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TABLE 3-1

SUMMARY OF MONITORING WELL STATIC WATER LEVEL
MEASUREMENTS (May 2022)

Newton County Wells Site
Villages of Silver Creek and Saginaw, Missouri

Monitoring
Well
Number

Ground
Surface
Elevation
(feet amsl)

Top Of
Casing
Elevation
(feet amsl)

Static Water
Level Depth
(feet btoc)

Static Water
Level
Elevation
(feet amsl)

Static Water
Level Depth
(feet bgs)

Total Depth
(feet btoc)

Total Depth
(feet bgs)

Uppermost Groundwater/Bedrock Interface Well Locations

Northwest Corner of FAG Bearings Property

FAG-4 3

1,031.08

1,030.67

15.72

1,014.95

16.13

21.3

21.7

Southwest of Service Building and Southern FAG Bearings Property Line

FAG-46

1,049.28

1,051.51

47.99

1,003.52

45.76

57.6

55.4

FAG-47

1,045.24

1,047.54

48.01

999.53

45.71

54.4

52.1

FAG-50

1,042.12

1,044.36

34.56

1,009.80

32.32

39.9

37.7

FAG-62

1,047.74

1,047.41

25.20

1,022.21

25.53

30.0

30.3

Village of Silver Creek

RI-MW-1

1,042.19

1,041.64

43.84

997.80

44.39

63.3

63.9

RI-MW-2

1,036.48

1,036.06

32.45

1,003.61

32.87

99.8

100.2

Adjacent to the Former TCE Transfer Pipeline Trench

FAG-22

1,055.95

1,058.45

32.03

1,026.42

29.53

97.4

94.9

FAG-31

1,054.48

1,054.05

31.93

1,022.12

32.36

84.0

84.4

FAG-32

1,054.57

1,054.08

29.22

1,024.86

29.71

63.7

64.2

FAG-56

1,055.72

1,055.46

22.46

1,033.00

22.72

31.5

31.8

FAG-73

1,052.93

1,052.34

16.71

1,035.63

17.30

30.0

30.5

FAG-74

1,053.35

1,052.69

1.55

1,051.14

2.21

33.2

33.9

South of the Former TCE Transfer Pipeline Trench

FAG-33

1,049.63

1,051.81

28.64

1,023.17

26.46

47.5

45.3

FAG-34

1,049.52

1,051.82

28.85

1,022.97

26.55

56.5

54.2

FAG-35

1,049.63

1,051.99

29.92

1,022.07

27.56

71.7

69.4

FAG-36

1,049.84

1,052.05

31.26

1,020.79

29.05

97.6

95.3

FAG-8 5

1,046.81

1,046.28

26.44

1,019.84

26.97

94.4

94.9

Mississippian Aquifer Well Locations

FAG Bearings Property

FAG-AW4 1

1,051.97

1,055.62

55.88

999.74

52.24

161.5

157.9

FAG-05

1,037.50

1,037.20

33.73

1,003.47

34.03

194.8

195.1

FAG-11

1,045.26

1,047.00

43.79

1,003.21

42.05

194.0

192.2

FAG-88

1,038.59

1,038.59

39.90

998.69

39.90

170.00

170.00

FAG-89

1,036.35

1,038.26

36.71

1,001.55

34.80

175.0

173.1

Villages of Silver Creek and Saginaw

RI-MW-5

1,044.17

1,043.72

43.20

1,000.52

43.65

181.0

181.4

RI-MW-6

1,061.87

1,061.44

61.35

1,000.09

61.78

203.0

203.4

RI-MW-7

1,060.37

1,060.01

83.40

976.61

83.76

199.2

199.6

RI-MW-8

938.65

939.50

3.61

935.89

2.76

42.4

41.5

RI-MW-9

1,041.52

1,041.21

37.92

1,003.29

38.22

195.0

195.3

Notes:

1: FAG-AW4 was drilled and constructed at an angle of approximately 30 degrees from vertical

feet amsl:	Feet above mean sea level

feet bgs:	Feet below ground surface

feet btoc:	Feet below top of well casing

Page 1 of 1




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TABLE 3-2

SUMMARY OF FINAL MONITORING WELL GROUNDWATER AND SPRING SURFACE WATER FIELD PARAMETER MEASUREMENTS

(MAY 2022)

Newton County Wells Site
Villages of Silver Creek and Saginaw, Missouri

Monitoring
Well or Surface

Water
Identification

Wellhead
Condition

Well

Casing
Diameter
(inches)

Pump Type

Date
Purged

Date
Sampled

Static
Water
Level
(feet btoc)

Total Depth
of Well
Casing
(feet btoc)

Calculated Well
Volume Under
Static Conditions

Field Parameter Measurements

Time
Sampled

Actual Volume of
Water Purged

PH

(SU)

SC
(pS/cm)

ORP

(mV)

Temperature

DO
(mg/L)

Total
Ferrous

Iron
(mg/L)

Analytical
Parameter
List

Gallons

Liters

Gallons

Liters

(°C)

(°F)

Uppermost Groundwater

Northwest Corner of FAG Bearings Property

FAG-43

Good

2

Bailer

5/17/2022

5/17/2022

15.72

21.18

0.89

3.37

16:06

3.0

11.4

5.47

52.7

99.8

16.2

61.2

4.18

0.80

B

Southwest of Service Building and Southern FAG Bearings Property Line

FAG-46

Good

2

Bailer

5/18/2022

5/18/2022

47.99

57.61

1.57

5.94

9

45

5.0

18.9

6.26

365.2

130.1

15.4

59.7

4.18

0.00

B

FAG-47

Good

2

Bailer

5/18/2022

5/18/2022

48.01

54.38

1.04

3.93

8

45

7.0

26.5

6.08

348.5

166.8

15.3

59.5

3.19

0.50

A

FAG-50

Good

2

Bailer

5/19/2022

5/19/2022

34.56

39.9

0.87

3.29

8

46

1.5

5.7

5.32

199.7

309.20

15.20

59.4

6.31

0.40

A

FAG-62

Good

2

Bailer

5/17/2022

5/17/2022

25.20

29.58

0.71

2.70

15:15

4.0

15.1

6.58

484.10

22.30

16.90

62.4

3.34

0.00

A

Village of Silver Creek

RI-MW1

Good

2

Bailer

5/17/2022

5/17/2022

43.84

63.3

3.17

12.01

16:37

4.0

15.1

7.24

484

29.9

17.5

63.5

3.81

0.00

B

RI-MW2

Good

2

Bailer

5/17/2022

5/17/2022

32.45

99.8

10.98

41.55

12:52

12.0

45.4

6.88

471

-115.9

17.4

63.3

3.06

1.60

B

Adjacent to the Former TCE Transfer Pipeline Trench

FAG-22

Good

2

Piston Pump

5/19/2022

5/19/2022

32.32

97.38

10.60

40.14

11:20

15.0

56.8

7.09

672

82.6

15.3

59.5

3.26

0.10

A

FAG-31

Good

2

Piston Pump

5/19/2022

5/19/2022

29.70

83.88

8.83

33.43

9:25

7.0

26.5

7.22

481.6

101.9

15.5

59.9

8.02

0.19

A

FAG-32

Good

2

Bailer

5/18/2022

5/18/2022

29.22

63.41

5.57

21.09

16:40

8.5

32.2

8.42

209

-62.6

18.8

65.8

2.94

0.20

A

FAG-56

Good

2

Bailer

5/17/2022

5/17/2022

22.46

31.31

1.44

5.46

17:00

2.0

7.6

6.33

400.2

153.8

19.0

66.2

3.25

0.00

A

FAG-73

Good

2

Bailer

5/18/2022

5/18/2022

16.71

29.95

2.16

8.17

15:40

7.0

26.5

6.90

489.3

-38.1

18.6

65.5

2.29

3.75

A

FAG-74

Good

2

Bailer

5/19/2022

5/19/2022

1.55

32.27

5.01

18.95

16:58

8.0

30.3

7.35

200.1

-53.4

18.2

64.8

4.12

0.80

A

South of the Former TCE Transfer Pipeline Trench

FAG-33

Good

2

Bailer

5/17/2022

5/17/2022

28.64

47.35

3.05

11.54

17:20

5.0

18.9

5.05

132.5

135.7

16.5

61.7

3.04

0.02

A

FAG-34

Good

2

Bailer

5/18/2022

5/18/2022

28.85

56.47

4.50

17.04

14:25

15.0

56.8

6.75

380.1

12

16.2

61.2

1.77

0.00

A

FAG-35

Good

2

Bailer

5/18/2022

5/18/2022

29.92

71.74

6.82

25.80

11:45

20.0

75.7

7.19

541

42

16.5

61.7

1.82

0.00

A

FAG-36

Good

2

Piston Pump

5/18/2022

5/18/2022

22.62

97.55

12.21

46.23

15:15

11.0

41.6

6.72

400.3

90

21.4

70.5

2.04

0.00

A

FAG-85

Good

2

Bailer

5/19/2022

5/19/2022

26.44

92.72

10.80

40.89

10:17

11.0

41.6

6.68

493.1

-92.1

15.8

60.4

1.42

2.40

A



Minimum
Maximum

5.05
8.42

52.70
672

-115.9
309

15.2
21.4

59.4

70.5

1.42
8.02

0.00
3.75



Mississippian Aquifer Well Locations

FAG Bearings Property

FAG-AW4

Good

2

Piston Pump

5/18/2022

5/18/2022

55.88

161.5

17.22

65.18

17:00

15.0

56.8

7.13

612

97.8

16.1

61.0

4.12

nm

B

FAG-05

Good

2

Piston Pump

5/18/2022

5/18/2022

34.07

194.7

26.19

99.12

9:00

8.0

30.3

6.99

602.5

115.3

15.4

59.7

4.46

nm

B

FAG-11

Good

2

Piston Pump

5/18/2022

5/18/2022

44.04

194.0

24.44

92.51

11:05

13.0

49.2

7.10

632

16

15.0

59.0

2.97

nm

B

FAG-88

Good

4

Piston Pump

5/19/2022

5/19/2022

39.90

170.0

84.96

321.56

14:00

7.0

26.5

7.44

386.7

88.4

15.0

59.0

3.24

nm

B

FAG-89

Good

4

Piston Pump

5/19/2022

5/19/2022

37.25

175.0

89.95

340.46

15:10

5.0

18.9

7.53

421.8

42.8

17.4

63.3

5.6

nm

B

Villages of Silver Creek and Saginaw

RI-MW5

Good

4

Piston Pump

5/17/2022

5/17/2022

43.43

181.0

89.83

340.02

13:10

8.0

30.3

7.22

454.4

28.6

15.0

59.0

4.9

nm

B

RI-MW6

Good

4

Piston Pump

5/17/2022

5/17/2022

61.75

203.0

92.24

349.11

15:50

10.0

37.9

7.54

338.5

127.9

17.1

62.8

4.41

nm

B

RI-MW7

Good

4

Piston Pump

5/17/2022

5/17/2022

83.63

199.2

75.47

285.64

14:30

6.0

22.7

7.46

343.1

107

16.1

61.0

3.89

nm

B

RI-MW8

Good

4

Piston Pump

5/17/2022

5/17/2022

3.91

42.4

25.13

95.13

11:10

5.0

18.9

7.05

391.8

118.7

15.5

59.9

6.31

nm

B

RI-MW9

Good

4

Piston Pump

5/18/2022

5/18/2022

38.25

195.0

102.36

387.42

12:40

10.0

37.9

7.20

385.7

-29.5

15.2

59.4

0.8

nm

B



Minimum
Maximum

6.99
7.54

338.5
632

16.0
127.9

15.0
17.4

59.0
63.3

2.97
6.31

nm
nm



Mississippian Aquifer Spring Surface Water Sample Locations

Village of Saginaw

SW-01

na

na

na

na

5/19/2022

na

na

na

na

16:40

na

na

7.74

364.2

73.0

10.7

51.3

9.78

nm

B

RW-341A

na

na

na

na

5/19/2022

na

na

na

na

16:55

na

na

7.62

357.6

82.4

12.4

54.3

11.88

nm

B



Minimum
Maximum

7.62
7.74

357.6
364.2

73.0
82.4

10.7
12.4

51.3
54.3

9.78
11.88

nm
nm



Notes:

feet btoc
SC
ORP
DO
SI

(jS/cm

Page 1 of 1	EQSBsflS

Feet below top of well casing

F:

Degrees Fahrenheit

Specific conductivity

°C:

Degrees Celsius

Oxidation reduction potential

mV:

Millivolts

Dissolved oxygen

mg/L:

Milligrams per liter

Standard international units

nm:

Not measured

Microsiemens per centimeter

na:

Not applicable

Parameter A (biodegradation): Laboratory VOCs, Nitrate, Sulfate, Chloride, Methane, Ethane, Ethene
Parameter A (biodegradation): Field Oxidation Reduction Potential, Specific Conductance, Dissolved Oxygen, pH,

Temperature, Ferrous Iron
Parameter B (hydrodynamic dispersion): Laboratory VOCs, Chloride

Parameter B (hydrodynamic dispersion): Field Oxidation Reduction Potential, Specific Conductance,

Dissolved Oxygen, pH, and Temperature


-------
TABLE 3-3

GROUNDWATER AND SURFACE WATER SAMPLE LOCATIONS AND LIST OF PARAMETERS TO
SUPPORT MONITORED NATURAL ATTENUATION (MNA) FOR REMEDIAL ACTION ACTIVITIES

Newton County Wells Site
Villages of Silver Creek and Saginaw, Missouri

Sampling Location

Parameter List-A
(biodeqradation)

Parameter List-B
(hydrodynamic dispersion)

Uppermost Groundwater Well Locations

Northwest Corner of FAG Bearings Property

FAG-43



X

Southwest of Service Building and Southern FAG Bearings Property Line

FAG-46



X

FAG-47

X



FAG-50

X



FAG-62

X



Village of Silver Creek

RI-MW1



X

RI-MW2



X

Adjacent to the Former TCE Transfer Pipeline Trench

FAG-22

X



FAG-31

X



FAG-32

X



FAG-56

X



FAG-73

X



FAG-74

X



South of the Former TCE Transfer PipelineTrench

FAG-33

X



FAG-34

X



FAG-35

X



FAG-36

X



FAG-85

X



Mississippian Aquifer Wells

FAG Bearings Property

FAG-AW4



X

FAG-05



X

FAG-11



X

FAG-88



X

FAG-89



X

Villages of Silver Creek and Sac

|inaw

RI-MW5



X

RI-MW6



X

RI-MW7



X

RI-MW8



X

RI-MW9



X

Mississippian Aquifer Spring Surface Water Sample Locations

Village of Saginaw

SW-01



X

RW-341A



X

Notes:

Parameter List-A (biodegradation):

-	Laboratory; Volatile Organic Compounds, Nitrate, Sulfate, Chloride, Methane, Ethane, Ethene

-	Field; Oxidation Reduction Potential, Specific Conductance, Dissolved Oxygen, pH, Temperature and Ferrous Iron
Parameter List-B (hydrodynamic dispersion):

-	Laboratory; Volatile Organic Compounds and Chloride

-	Field; Oxidation Reduction Potential Specific Conductance, Dissolved Oxygen, pH and Temperature

Page 1 of 1




-------
TABLE 3-4

SUMMARY OF LABORATORY MONITORED NATURAL ATTENUATION PARAMETERS AND DETECTED VOLATILE ORGANIC COMPOUNDS

(MAY 2022)

Newton County Wells Site
Villages of Silver Creek and Saginaw, Missouri

Analyte

Units

Uppermost Groundwater Wells & Date Sampled

Minimum
Detection

Maximum
Detection

Total
Detections

Total
Investigative
Samples

FAG-22

FAG-31

FAG-32

FAG-33

FAG-34

FAG-35

FD-List A

FAG-36

FAG-43

FAG-46

FAG-47

FAG-50

FAG-56

FAG-62

FAG-73

FAG-74

FAG-85

RI-MW1

RI-MW2

5/19

5/19

5/18

5/17

5/18

5/18

5/18

5/18

5/17

5/18

5/18

5/19

5/17

5/17

5/18

5/19

5/19

5/17

5/17

Volatile Organic Compounds

1,1-Dichloroethene

|jg/L

2.4 J

<2.2

<0.22

<0.22

<1.1

<1.1

<1.1

<2.2

<0.22

<0.22

<0.12

<5.5

<0.22

<0.22

1.2

<1.1

43.1

<0.22

<0.22

1.2

43.1

3

18

1,2-Dichloroethene (Total)

|jg/L

211

215

12.5

4.7

226

115

108

174

0.67 J

1.7

3.2

157

84.3

9.6

46.8

<1.1

373

1.7

<0.22

0.67 J

373

16

18

cis-l,2-Dichloroethene

|jg/L

206

210

12.3

4.7

221

111

105

168

0.67 J

1.7

3.2

157

83.2

9.6

44.2

0.79 J

367

1.7

<0.13

0.67 J

367

17

18

trans-l,2-Dichloroethene

|jg/L

4.5 J

4.1 J

0.17 J

<0.10

4.9 J

3.3 J

3.2 J

6.5 J

<0.10

<0.10

<0.10

<2.6

1.1

<0.10

2.6

<0.51

5.1

<0.10

<0.10

0.17 J

6.5 J

9

18

Trichloroethene

|jg/L

379

726

49.5

31.7

582

537

520

455

2.3

21.1

42.7

2,050

8.9

16.3

22.8

4.0 J

252

57.3

<0.21

2.3

2,050

17

18

Vinyl chloride

|jg/L

30.8

<1.7

0.21 J

<0.17

2.9 J

0.95 J

<0.84

<1.7

<0.17

<0.17

<0.17

<4.2

0.25 J

<0.17

11.0

<0.84

53.8

<0.17

<0.17

0.21 J

53.8

7

18

Monitored Natural Attenuation Parameters (Laboratory)

Nitrate as N

mg/L

1.5

0.85

0.62

0.08 J

0.19

1.4

1.4

0.18

NA

NA

1.2

0.39

0.81

0.26

<0.079

0.40

0.17

NA

NA

0.08 J

1.5

13

14

Sulfate

mg/L

18.0

7.5

16.0

1.3

10.1

15.3

14.8

11.8

NA

NA

7.1

7.3

36.7

13.3

12.2

6.9

12.4

NA

NA

1.3

36.7

14

14

Chloride

mg/L

24.1

11.7

4.5

15.0

14.7

17.4

16.9

13.2

3.7

4.7

10.8

9.8

26.1

16.6

16.2

1.6

12.8

10.6

23.3

1.6

26.1

18

18

Methane

ug/L

29.6

<5.5

<5.5

<5.5

<5.5

25.2

24.6

7.8 J

NA

NA

<5.5

<5.5

<5.5

<5.5

558

<5.5

619

NA

NA

7.8 J

619

5

14

Ethane

ug/L

<3.8

<3.8

<3.8

<3.8

<3.8

<3.8

<3.8

<3.8

NA

NA

<3.8

<3.8

<3.8

<3.8

14.1

<3.8

<3.8

NA

NA

14.1

14.1

1

14

Ethene

mq/l

<7.1

<7.1

<7.1

<7.1

<7.1

<7.1

<7.1

<7.1

NA

NA

<7.1

<7.1

<7.1

<7.1

<7.1

<7.1

8.9 J

NA

NA

8.9 J

8.9

1

14

Iron

ug/L

124

188

1,380

611

921

23.5 J

42.9 J

3,250

NA

NA

243

23,800

531

3,670

4,010

36,300

9,650

NA

NA

23.5 J

36,300

14

14





Mississippian Aquifer Groundwater Wells & Date Sampled

Minimum
Detection

Maximum
Detection

Total
Detections

Total

Analyte

Units

FAG-05

FD-List B

FAG-11

FAG-88

FAG-89

FAG-AW4

RI-MW5

RI-MW6

RI-MW7

RI-MW8

RI-MW9

Investigative





5/18

5/18

5/18

5/19

5/19

5/18

5/17

5/17

5/17

5/17

5/18

Samples

Volatile Organic Compounds

1,2-Dichloroethene (Total)

mq/l

2.6

2.9

0.66 J

1.6

1.3

275

0.92 J

9.4

3.2

<0.22

0.28 J

0.28 J

275

9

10

cis-l,2-Dichloroethene

Mg/L

2.6

2.9

0.66 J

1.6

1.3

268

0.92 J

9.4

3.2

<0.13

0.28 J

0.28 J

268

9

10

Trichloroethene

Mg/L

18.7

18.0

2.3

7.0

8.6

1,160

15.6

64.2

21.7

1.6

2.0

1.6

1,160

10

10

Vinyl Chloride

Mg/L

<0.17

<0.17

<0.17

<0.17

<0.17

28.5

<0.17

<0.17

<0.17

<0.17

<0.17

28.5

28.5

1

10

Monitored Natural Attenuation Parameter (Laboratory)

Chloride

mg/L

34.5

34.0

32.6

6.2

4.9

16.2

20.5

9.2

5.9

9.0

13.6

4.9

34.5

10

10

Notes:

mg/L:	Milligrams per liter

jjg/L:	Micrograms per liter	|	1 = Parameter List A (biodegradation) Laboratory Parameters: VOCs, Nitrate, Sulfate, Chloride, Methane, Ethane, Ethene

NA:	Not analyzed

<:	Not detected above the indicated concentration	|	~| = Parameter List B (hydrodynamic dispersion) Laboratory Parameters: VOCs and Chloride

FD:	Field Duplicates - FD-List A = Duplicate of FAG-35 & FD-List B = Duplicate of FAG-05

J:	Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.





Spring Surface Water

Minimum
Detection

Maximum
Detection

Total
Detections

Total

Analyte

Units

RW-341A

SW-01

Investigative





5/19

5/19

Samples

Volatile Organic Compounds

Trichloroethene

Mg/L

o
o

0.92 J

0.60 J

0.92 J

2

2

Monitored Natural Attenuation Parameter (Laboratory)

Chloride

mg/L

7.6

7.5

7.5

7.6

2

2

Page 1 of 1

liFjlSimi


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

FIGURES

December 2022


-------
E32ND ST

JOPLIN

Sunnyvale

ROflUN ST

Gateway Drive

E36TH ST

MOORHBAD DR

KELLER DR
SILVER CREEK DR

Silver Creek

Village of
Silver Creek

APRICOT 01

WOODLAND DR

Leawood

'000- QUAIL RIDGE DR

REDO/NI

LN

Shoal Creek
Estates

Source: 2021 USGS 7.5 Minute Series Joplin East, Missouri Topographic Quadrangle; Contour Interval 10 Feet.

J \ ~ 1	! AW	\ Rue /



	. SITE BOUNDARY BASED ON

^	* REMEDIAL INVESTIGATION

FIGURE 1-1

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

SITE LOCATION MAP

KEY MAP

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

Map Scale: 1:24,000 | Map Center: 37"T59.0511",

-94°28'7.2214"


-------
MAMMONS BO U L

^ FAG"31?

FAG-32^

OUTER ROAD	FAG-22^.

FAG-56
FAG-AW4

u

. BeS

FAG-74
-FAG-73

FAG-OJO

P^FAG-85
-FAG-33B £<¦
lFAG-351'

FAG-43

FAG-11 O

^ MOORHEAD DR

O Ri-MW6Kf Zi

SILVER CREEK DRIVE

IVY LANE



<



r-.:

McCUTCHEON ST

SW-01

ARCH LANE

qmm

|Aerial Imagery Source: Google Earth™, dated 3/20/2016.

PROJECT: 1690004605 DATED: 9/15/2021 DESIGNER: CKL	L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2021\3-1_SW, UM GW& Miss Aq Locations.dwg

O SURFACE WATER
O UPPERMOST GROUNDWATER
O MiSSISSiPPIAN AQUIFER

SURFACE WATER, UPPERMOST GROUNDWATER
AND MISSISSIPPIAN AQUIFER WELL LOCATIONS

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 3-1

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
MAMMONS BO

FAG-32;
1024.86

fAG-3"t
1022.12

FAG-22-

1026.42

FAG-73
1035.63

FAG-74
1051.14

OUTER R°AD

FAG-56-

1033.00:

Z FAG^32l
1014.95

FAG-34

1022.97

gjij||||^PFAG-35—^
1022.07

FAG-62 O

1022.21 % FAG-33-
1023.17

1020.79

-FAG-85P.
1019.84

FAG-47 O

iFAG-5b

FAG-46 O

1003.52

1009.80

MOORHEAD DR

RI-MW1 .

997.80

SILVER CREEK DRIVE

|Aerial Imagery Source: Google Earth'M, dated 3/20/2016.

O UPPERMOST GROUNDWATER

997.80 WATER ELEVATION

(FEET ABOVE SEA LEVEL)

UPPERMOST GROUNDWATER WELLS
STATIC WATER ELEVATIONS MEASURED

ON MAY, 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 3-2

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EEEEfll


-------
PROJECT: 1690004605 DATED: 8/9/2022 DESIGNER: CKL

L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2022\3-3_Miss Aq, Static Water Elev (May 2022).dwg

FAG-AW4 O

999.74

J v

1003.21

RI-MW9
1003.29

MW5

« v I. "	f	* ^ " " — '

SILVER CREEK DRIVE

f' 7"

IVY LANE

OiRi-M'wH
I 976.61

wismas

McCUTCHEON ST

ARCH LANE

dated 3/20/2016.

33 nCT^SI

.1000.52 ~

FAG-05'O
1003.47

O MISSISSIPPIAN AQUIFER

935.89 WATER ELEVATION

(FEET ABOVE SEA LEVEL)

MISSISSIPPIAN AQUIFER WELLS
STATIC WATER ELEVATIONS
MEASURED ON MAY, 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 3-3

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

mm


-------
ttim

¦ -ji

1 •

MAMMONS BO

FAG-31

outer r°ad

FAG-74

FAG-43;

FAG-34

FAG-47 O

SET.	b jJfA&SoI

FAG-46 O	B	. R

' • - *:

MOORHEAD DR



SILVER CREEK DRIVE



|Aerial Imagery Source: Google Earth|M, dated 3/20/2016.

O	UPPERMOST GROUNDWATER

A	WELL LOCATED AT THE NORTHWEST CORNER OF THE FAG BEARINGS PROPERTY

B	WELLS LOCATED SOUTHWEST OF SERVICE BUILDING AND SOUTHERN FAG BEARINGS PROPERTY LINE

C	WELLS LOCATED IN THE VILLAGE OF SILVER CREEK

D	WELLS LOCATED ADJACENT TO THE FORMER TRICHLOROETHENE (TCE) TRANSFER PIPELINE TRENCH

E	WELLS LOCATED SOUTH OF THE FORMER TCE TRANSFER PIPELINE TRENCH

UPPERMOST GROUNDWATER WELLS
GENERAL GROUPINGS

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 3-4A

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
MAMMONS BO U L

OUTER R°AD

FAG-05'O

FAG-AW4 O

O FAG-11

o o

FAG-88 FAG-89

MOORHEAD OR

ORI-MW5

CREEK DRIVE

IVY LANE

0"rPmW73

McCUTCHEON ST

O RI-MWef

arch lane

lAerial Imagery Source: Google EarthrM, dated 3/20/2016.

PROJECT: 1690004605 DATED: 4/11/2022 DESIGNER: CKL	L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2022\3-4B_Miss Aq, Wells General Groupings.dwg

O MISSISSIPPIAN AQUIFER

A WELLS LOCATED ON THE FAG BEARINGS PROPERTY
B WELLS LOCATED IN THE VILLAGES OF SILVER CREEK AND SAGINAW

MISSISSIPPIAN AQUIFER WELLS
GENERAL GROUPINGS

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 3-4B

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
		

FAG-43 I

Date

Result ug/L |

10/5/1999

180

10/6/2002

110

10/21/2008

338

4/28/2009

275

10/15/2009

438

4/30/2010

330

10/19/2010

395

4/26/2011

313

10/26/2011

289

5/3/2012

1.0 U

10/10/2012

12.2

5/15/2013

1.0 U

10/19/2016

50.6

5/30/2017

1.0 U

10/11/2017

34.9

10/10/2018

1.0 U

9/16/2020

66.4

5/18/2021

1.0 U

5/17/2022

2.3

FAG-56

Date

Result ug/L

10/7/1999

30.0

4/5/2000

10.0

1/8/2002

6.0

5/8/2002

6.0

10/20/2008

8.3

4/28/2009

8.2

10/13/2009

8.2

4/28/2010

12.4

10/20/2010

6.5

4/27/2011

8.0

10/25/2011

8.9

5/1/2012

9.4

10/9/2012

8.6

5/14/2013

9.6

10/18/2016

15.1 J

5/27/2017

9.3

10/8/2017

9.5

10/9/2018

9.6

9/16/2020

5.9

5/18/2021

7.8

5/17/2022

8.9

I MM

v

ram

Result ug/L

mm

FAG-31

Date

Result ug/L

10/6/1999

1,200

10/5/2002

920

10/23/2008

791

5/21/2009

861

10/15/2009

1,070

4/29/2010

719

10/21/2010

653

4/28/2011

698

10/27/2011

698

5/3/2012

698

10/11/2012

705

5/16/2013

724

10/20/2016

765

5/31/2017

719

10/12/2017

735

10/11/2018

934

9/17/2020

705

5/20/2021

733

5/19/2022

726

FAG-32

Date

Result ug/L

10/7/1999

60.0

1/11/2002

58.0

5/8/2002

90.0

10/4/2002

130

10/22/2008

1,730

5/20/2009

1,500

10/13/2009

1,670

4/29/2010

1,630

10/19/2010

1,590

4/28/2011

1,690

10/25/2011

1,620

5/1/2012

1,670

10/9/2012

1,770

5/16/2013

1,380

10/20/2016

1,570

6/1/2017

1,520

10/12/2017

1,780

10/10/2018

1,920

9/16/2020

1.0 U

5/19/2021

183

5/18/2022

49.5

FAG-74

Date

Result ug/L

4/3/2000

10,000

1/9/2002

10,000 E

5/8/2002

10,000 E

10/21/2008

2,720

5/21/2009

3,950

10/14/2009

2,760

4/28/2010

2,560

10/20/2010

1,070

4/28/2011

1,430

10/26/2011

893

5/1/2012

770

10/9/2012

575

5/16/2013

1,120

10/20/2016

200

5/26/2017

789

10/12/2017

101

10/10/2018

123

9/17/2020

37.5

5/21/2021

201

5/19/2022

4.0 J

S5*

	

ram

OFAG-05

OUTER R°AD

..FAG-31
FAG-32-0
FAG-22—C



FAG-73

Date

Result ug/L

4/5/2000

2,300

1/9/2002

11,000 E

5/8/2002

20,000 E

10/21/2008

1,130

5/21/2009

429

10/14/2009

358

4/28/2010

387

10/20/2010

514

4/28/2011

73

10/26/2011

82.3

5/1/2012

103

10/10/2012

163

5/16/2013

215

10/19/2016

249

5/31/2017

58.3

10/11/2017

171

10/10/2018

242

9/16/2020

132

5/19/2021

18.8

5/18/2022

22.8





JA-



;

¥ A.



Date

Result ug/L

10/7/1999

510 D

10/21/2008

202

4/28/2009

167

10/15/2009

119

4/29/2010

107

10/19/2010

146

4/26/2011

134

10/27/2011

135

5/3/2012

103

10/10/2012

130

5/14/2013

70.2

10/18/2016

50.6

5/27/2017

47.9

10/11/2017

53.5

10/9/2018

56.9

9/16/2020

39

5/18/2021

27.7

5/18/2022

21.1

AG-43!

FAG-560
FAG-AW4 O

) FAG-73
FAG-74

Result ug/L

640
620
484
510
542
602
446
583

FAG-34

Date

Result ug/L

10/6/1999

1,200

10/7/2002

1,100

10/22/2008

882

4/29/2009

992

10/14/2009

804 J

4/27/2010

111

10/20/2010

712

4/27/2011

111

10/27/2011

761

5/2/2012

758

10/11/2012

820

5/15/2013

713

10/19/2016

574

5/25/2017

809

10/11/2017

644

10/10/2018

762

9/16/2020

500

5/19/2021

462

5/18/2022

582

Result ug/L

750
490
565

M

.



qfag-1 1





¦¦

FAG-47,0

¦H

' > i

FAG-620-I
.FAG-5OT

o

|FAG-34
llFAG-361

».€





v=

. -.V» -

'sEwm
¦ ¦¦ <•	'

'3^3--	-

rrT	- ~

¦RI-MW2I

¦RI-MW1I

» •- *	».' J

RI-MW9 ORI-MW2

— ' ~

«*

dated 3/20/2016.

RI-MW1

Date

Result ug/L

10/8/2002

0.53 J

10/22/2008

54.5

4/28/2009

51.4

10/15/2009

36.0 J

4/30/2010

53.2

10/19/2010

78.5

4/26/2011

80.7

10/28/2011

55.1

5/3/2012

41.2

10/10/2012

55.0

5/14/2013

85.1

10/18/2016

52.8

5/25/2017

96.4

10/8/2017

47.4

10/10/2018

99.7

9/15/2020

47.5

5/19/2021

68.3

5/17/2022

57.3







if.









—...

r?





RI-MW2



FAG-47

Date

Result ug/L

1

Date

Result ug/L

10/8/2002

49.0



10/5/1999

400

10/22/2008

1.0 U



10/6/2002

270

4/27/2009

1.0 U



10/21/2008

160

10/15/2009

1.0 U



4/29/2009

66.5

4/29/2010

1.0 U



10/13/2009

131

10/19/2010

1.0 U



4/27/2010

119

4/26/2011

1.0 U

ti

10/20/2010

165

10/26/2011

1.0 U



4/27/2011

140

5/3/2012

1.0 U



10/27/2011

136

10/10/2012

1.0 U

s

5/3/2012

116

5/14/2013

1.0 U

}

10/9/2012

122

10/18/2016

1.0 U

5/14/2013

93.4

5/25/2017

1.0 U

j, IV

10/18/2016

76.9

10/8/2017

1.0 U

m

5/27/2017

69.2

10/9/2018

1.0 u

10/8/2017

103

9/15/2020

1.0 u

¦4*

10/9/2018

63.3

5/18/2021

1.0 u

$

9/15/2020

97.9

5/17/2022

<1.0

5/18/2021

55.4





—
> ~

•

5/18/2022

42.7



fltlll





FAG-85



->r

M, ..

4 0v ' V

^,FAG-88^43FAG-ji

r~





*9i





> I ii • ¦ • .4
*



RI-MW6

VER

'V

r5





V •• «• ¦''



Date
10/6/1999
5/4/2000
10/7/2002
10/21/2008
5/20/2009
12/16/2009
4/28/2010
4/27/2011
10/25/2011
5/3/2012
10/10/2012
5/15/2013
10/20/2016
5/31/2017
10/8/2017
10/11/2017
9/15/2020
5/19/2021
5/19/2022



Result ug/L



Date

Result ug/L

10/7/1999

190

4/4/2000

1,500

10/7/2002

940

> 10/23/2008

413

| 4/29/2009

121

10/13/2009

126

4/29/2010

462

10/20/2010

294

4/27/2011

51.7

10/26/2011

185

5/1/2012

64.9

10/10/2012

103

i 5/15/2013

167

I 10/19/2016

33.6

4 5/27/2017

16.9

10/8/2017

NS

10/11/2018

NS

9/15/2020

NS

5/18/2021

23.9

5/17/2022

16.3

"

FAG-33

Date

Result ug/L

10/6/1999

7.0

10/4/2002

15.0

10/20/2008

19.5

4/28/2009

20.5

10/14/2009

20.2

4/27/2010

26.6

10/20/2010

26.1

4/27/2011

29.2

10/27/2011

20.2

5/2/2012

19.7

10/11/2012

17.3

5/14/2013

23.9

10/18/2016

28.1

5/27/2017

31.7

10/8/2017

31.0

10/9/2018

29.6

9/15/2020

28.3

5/18/2021

28.9

5/17/2022

31.7

¦



O	UPPERMOST GROUNDWATER

O	MiSSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

D	= DILUTED

U	= NOT DETECTED

NS	= NOT SAMPLED; INSUFFICIENT WATER

UPPERMOST GROUNDWATER
ANALYTICAL RESULTS
TRICHLOROETHENE (TCE) 1999 TO 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 4-1A

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY




-------
FAG-56

Date

Result ug/L

10/7/1999

23.0

4/5/2000

32.0

1/8/2002

20.0

5/8/2002

9.0

10/20/2008

72.8

4/28/2009

68.5

10/13/2009

83.8

4/28/2010

84.1

10/20/2010

101

4/27/2011

98.5

10/25/2011

124

5/1/2012

117

10/9/2012

114

5/14/2013

122

10/18/2016

105

5/27/2017

115

10/8/2017

120

10/9/2018

113

9/15/2020

72.2

5/18/2021

76.8

5/17/2022

83.2



I MM



W

Result ug/L

210 D
550
581
852
694
703
588
681
608
531
528
All
707
523
464
514

FAG-31

Date

Result ug/L

10/6/1999

64.0

10/5/2002

82.0

10/23/2008

116

5/21/2009

182

10/15/2009

184

4/29/2010

166

10/21/2010

170

4/28/2011

168

10/27/2011

168

5/3/2012

161

10/11/2012

201

5/16/2013

196

10/20/2016

305

5/31/2017

276

10/12/2017

247

10/11/2018

274

9/17/2020

244

5/20/2021

248

5/19/2022

210

FAG-32

Date

Result ug/L

10/7/1999

2.0

1/11/2002

4.0 J

5/8/2002

10=.0 U

10/4/2002

5.4

10/22/2008

363

5/20/2009

313

10/13/2009

375

4/29/2010

338

10/19/2010

347

4/28/2011

396

10/25/2011

406

5/1/2012

401

10/9/2012

487

5/16/2013

389

10/20/2016

481

5/31/2017

448

10/12/2017

448

10/10/2018

476

9/16/2020

1.0 U

5/19/2021

43.7

5/18/2022

12.3

FAG-74

Date

Result ug/L

4/3/2000

2,200

1/9/2002

2,800

5/8/2002

6,000 E

10/21/2008

2,540

5/21/2009

2,960

10/14/2009

2,410

4/28/2010

1,990

10/20/2010

1,210

4/28/2011

1,200

10/26/2011

1,140

5/1/2012

908

10/9/2012

875

5/16/2013

1,100

10/20/2016

321

5/26/2017

549

10/12/2017

254

10/10/2018

223

9/17/2020

113

5/21/2021

179

5/19/2022

0.79 J





	

OUTER R°AD

sFAG-31
FAG-32-\

3iFAG-43l

\

FAG-73

Date

Result ug/L

4/5/2000

5,800

1/9/2002

6,000

5/8/2002

6,000 E

10/21/2008

2,780

5/21/2009

951

10/14/2009

1,120

4/28/2010

1,390

10/20/2010

1,700

4/28/2011

143

10/26/2011

357

5/1/2012

396

10/10/2012

561

5/16/2013

425

10/19/2016

282

5/31/2017

96.6

10/11/2017

260

10/10/2018

305

9/16/2020

192

5/19/2021

45.8

5/18/2022

44.2







Date

Result ug/L |

10/7/1999

24.0

10/21/2008

128

4/28/2009

9.1

10/15/2009

9.1

4/29/2010

7.4

10/19/2010

9.8

4/26/2011

7.0

10/27/2011

6.6

5/3/2012

4.6

10/10/2012

5.1

5/14/2013

3.5

10/18/2016

2.8

5/27/2017

2.2

10/11/2017

4.7

10/9/2018

3.6

9/16/2020

5.3

5/18/2021

4.0

5/18/2022

1.7

I

V

A



*

it*

FAG-560
FAG-AW4 O

FAG-73
FAG-74



FAG-35

Date

Result ug/L

10/6/1999

67.0

10/5/2002

150

10/23/2008

126

4/29/2009

121

10/15/2009

122

4/28/2010

171

10/20/2010

134

4/27/2011

173

10/27/2011

147

5/2/2012

125

10/11/2012

134

5/15/2013

124

10/19/2016

126

5/31/2017

107

10/11/2017

123

10/10/2018

131

9/16/2020

110

5/18/2021

113

5/18/2022

111

-



1 *





v • .

»«





i* ¦ -Hf.ii*

: 4*.

OFAG-11

ill - ¦ i" ' it

V,

HH

FAG-62G-

I r|[FAG-5m

Sf47|0 O

¦FAG-35
P
FAG-33

FAG-34
FAG-36M



*^'V

n *



,w

> ¦



'

	

FAG-36

Date

Result ug/L

10/6/1999

64.0

10/7/2002

80.0

10/22/2008

104

5/20/2009

42.2

10/16/2009

80.8

4/28/2010

158

10/21/2010

182

4/27/2011

173

10/27/2011

192

5/3/2012

155

10/11/2012

183

5/15/2013

234

10/20/2016

235

5/31/2017

280

10/11/2017

197

10/10/2018

257

9/16/2020

229

5/19/2021

240

5/18/2022

168

•s&k ^

i

FAG-85

/ * 'Pi, *•'' i
..

t iL&irjkm





lAii I

*. I RI-MW1 ¦
-- *>

ORI-MW9 ORI-MW2

RI-MW2

Date

Result ug/L

10/8/2002

1.9

10/22/2008

1.0 U

4/27/2009

1.0 U

10/15/2009

1.0 U

4/29/2010

1.0 U

10/19/2010

1.0 U

4/26/2011

1.0 U

10/26/2011

1.0 U

5/3/2012

1.0 U

10/10/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 U

5/25/2017

1.0 U

10/8/2017

1.0 U

10/8/2017

1.0 U

9/15/2020

1.0 u

5/18/2021

1.0 u

| 5/17/2022

<1.0



&

L

• <

BbPjSUw® MaEJ

FAG-47

Date

Result ug/L

10/5/1999

25.0 U

10/6/2002

21.0

10/21/2008

14.3

4/29/2009

9.9

10/13/2009

12.5

4/27/2010

9.3

10/20/2010

11.9

4/27/2011

9.5

10/27/2011

CO
CO

5/3/2012

9.1

10/9/2012

9.7

5/14/2013

9.9

10/18/2016

10.6

5/27/2017

7.7

10/8/2017

11.3

10/8/2017

11.3

9/15/2020

7.9

5/18/2021

5.9

5/18/2022

3.2

'3;:: *"• ~

I

¦4 fB " *

¦¦T,jA
'•/ C»

' - • y

* .V. * ^ -

-• •- »y j .¦¦*

, I 1

asi- 1

¦ ' " 3*:.. f



(Jlllj 1

FAG-50

Date

Result ug/L

10/6/1999

500 U

5/4/2000

59.0

10/7/2002

10 J

10/21/2008

28.2

5/20/2009

54.8

10/16/2009

30.8

4/28/2010

32.8

4/27/2011

20 U

10/25/2011

20 U

5/3/2012

14.2

10/10/2012

20 U

5/15/2013

26.3

10/20/2016

91.5

5/31/2017

49.4

10/8/2017

NS

10/11/2018

NS

9/15/2020

NS

5/19/2021

62.4

5/19/2022

157

't i } m -



FAG-62

Date

Result ug/L

10/7/1999

180

4/4/2000

330

10/7/2002

150

10/23/2008

103

4/29/2009

26.9

10/13/2009

33.2

4/29/2010

129

10/20/2010

107

4/27/2011

15.3

10/26/2011

193

5/1/2012

61.6

10/10/2012

456

5/15/2013

277J

10/19/2016

13.1

5/27/2017

3.6

10/8/2017

NS

10/11/2018

NS

9/15/2020

NS

5/18/2021

13.8

5/17/2022

9.6

FAG-33

Date

Result ug/L

10/6/1999

1.0 U

10/4/2002

1.3

10/20/2008

2.6

4/28/2009

2.3

10/14/2009

3.0

4/27/2010

3.0

10/20/2010

2.8

4/27/2011

3.3

10/27/2011

2.7

5/2/2012

2.3

10/11/2012

2.3

5/14/2013

2.8

10/18/2016

3.5

5/27/2017

3.6

10/8/2017

3.3

10/9/2018

3.7

9/15/2020

3.8

5/18/2021

4.4

5/17/2022

4.7

1

^ fc'/l'

FAG-85

Date

Result ug/L

10/6/2002

130

10/23/2008

350

5/20/2009

71.1 J

10/16/2009

172

4/30/2010

105

10/19/2010

1.0 U

4/27/2011

231

10/25/2011

189 J

5/2/2012

182

10/9/2012

216

5/15/2013

200

10/19/2016

48.9

5/31/2017

170

10/11/2017

135

10/11/2018

221

9/17/2020

216

5/21/2021

204

5/19/2022

367







¦ 0

H L_

500
	I Feet

O	UPPERMOST GROUNDWATER

O	MiSSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

D	= DILUTED

U	= NOT DETECTED

NS	= NOT SAMPLED; INSUFFICIENT WATER

UPPERMOST GROUNDWATER
ANALYTICAL RESULTS
CIS-1.2-DICHLOROETHENE (DCE) 1999 TO 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 4-1B

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EEEEfll


-------
FAG-56

Date

Result ug/L

10/7/1999

1.0 U

4/5/2000

0.3 J

1/8/2002

1.0 U

5/8/2002

1.0 U

10/20/2008

1.0 U

4/28/2009

1.0 U

10/13/2009

1.0 U

4/28/2010

1.0 U

10/20/2010

1.0 U

4/27/2011

1.0 U

10/25/2011

1.0 U

5/1/2012

1.0 U

10/9/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 u

5/27/2017

1.0 u

10/8/2017

1.0 u

10/9/2018

1.0 u

9/16/2020

1.0 u

5/18/2021

1.0 u

5/17/2022

0.25 J





MW1- "30



I MM



W

Date

2/16/1999
10/4/2002
10/23/2008
5/21/2009
10/16/2009
4/29/2010
10/21/2010
4/28/2011
10/28/2011
5/3/2012
10/11/2012
5/16/2013
10/20/2016
5/31/2017
10/12/2017
10/11/2018
9/17/2020
5/20/2021
5/19/2022

Result ug/L

4.0 D

62.0

47.2
144
80.9
133
108
127

	101

117

80.7

60.8

93.1
63.1
73.6
110

25.0 U

18.3
30.8

Date

10/6/1999
10/5/2002
10/23/2008
5/21/2009
10/15/2009
4/29/2010
10/21/2010
4/28/2011
10/27/2011
5/3/2012
10/11/2012
5/16/2013
10/20/2016
5/31/2017
10/12/2017
10/11/2018
9/17/2020
5/20/2021
5/19/2022

Result ug/L

50.0 U
50.0 U
10.0 U
1.0 U
1.0 U
10.0 U
10.0 U
10.0 U
1.0 U
1.0 U
1.0 U
1.0 U

10.0 u
10.0 u
10.0 u
10.0 u
10.0 u
10.0 u

<10.0

FAG-32

Date

Result ug/L

10/7/1999

2.0 U

1/11/2002

1.0 U

5/8/2002

1.0 U

10/4/2002

1.0 U

10/22/2008

1.0 U

5/20/2009

1.0 U

10/13/2009

1.0 U

4/29/2010

25.0 U

10/19/2010

20.0 U

4/28/2011

20.0 U

10/25/2011

1.0 U

5/1/2012

20.0 U

10/9/2012

20.0 U

5/16/2013

20.0 U

10/20/2016

20.0 U

6/1/2017

20.0 U

10/12/2017

20.0 U

10/10/2018

20.0 U

9/16/2020

1.0 U

5/19/2021

1.0 U

5/18/2022

0.21 J



i , ' ,

FAG-74

Date

Result ug/L

4/3/2000

93.0 J

1/9/2002

120 J

10/21/2008

188

5/21/2009

213

10/14/2009

222

4/28/2010

181

10/20/2010

134

4/28/2011

161

10/26/2011

151

5/1/2012

146

10/9/2012

148

5/16/2013

149

10/20/2016

75

5/26/2017

75.2

10/12/2017

44.0

10/10/2018

31.1

9/17/2020

11.3

5/21/2021

18.9

5/19/2022

<5.0

* w

't

J

Date

Result ug/L I

10/7/1999

10 U

10/21/2008

10 U

4/28/2009

1.0 U

10/15/2009

1.0 U

4/29/2010

1.0 U

10/19/2010

1.0 u

4/26/2011

1.0 u

10/27/2011

1.0 u

5/3/2012

1.0 u

10/10/2012

1.0 u

5/14/2013

1.0 u

10/18/2016

1.0 u

5/27/2017

1.0 u

10/11/2017

1.0 u

10/9/2018

1.0 u

9/16/2020

1.0 u

5/18/2021

1.0 u

5/18/2022

<1.0

/
/



!

/



OUTER R°AD

=CfcAG-43J

V «

..ssr?®5

FAG-31 —
FAG-32—
FAG-22—

¦SKi.\j
FAG-560
FAG-AW4i O



FAG-73

Date

Result ug/L

4/5/2000

780

1/9/2002

93.0 J

5/8/2002

120 J

10/21/2008

965

5/21/2009

778

10/14/2009

896

4/28/2010

1060

10/20/2010

488

4/28/2011

152

10/26/2011

616

5/1/2012

471

10/10/2012

415

5/16/2013

510

10/19/2016

212

5/31/2017

177

10/11/2017

140

10/10/2018

212

9/16/2020

33

5/19/2021

4.2

5/18/2022

11.0



ippfT '



4
JK'i*





"P..U



FAG-73
FAG-74



FAG-11

o

		

01 iV.

r E _

4 A

dated 3/20/2016.

RI-MW2

Date

Result ug/L

10/8/2002

1.0 U

10/22/2008

1.0 U

4/27/2009

1.0 U

10/15/2009

1.0 U

4/29/2010

1.0 U

10/19/2010

1.0 U

4/26/2011

1.0 U

10/26/2011

1.0 U

5/3/2012

1.0 U

10/10/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 U

5/25/2017

1.0 U

10/8/2017

1.0 U

10/9/2018

1.0 u

9/15/2020

1.0 u

5/18/2021

1.0 u

| 5/17/2022

<1.0

t. m

h

v k

»'?, i:/JV'5

IRVMiiVm Mffi

FAG-47

Date

Result ug/L

10/5/1999

25.0 U

10/6/2002

10.0 U

10/21/2008

1.0 U

4/29/2009

1.0 U

10/13/2009

1.0 U

4/27/2010

1.0 U

10/20/2010

1.0 U

4/27/2011

1.0 U

10/27/2011

1.0 U

5/3/2012

1.0 U

10/9/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 U

5/27/2017

1.0 u

10/8/2017

1.0 u

10/9/2018

1.0 u

9/15/2020

1.0 u

5/18/2021

1.0 u

5/18/2022

<1.0

41' ¥1

Date

10/6/1999

10/5/2002

10/23/2008

4/29/2009

10/15/2009

4/28/2010

10/20/2010

4/27/2011

10/27/2011

5/2/2012

10/11/2012

5/15/2013

10/19/2016

5/31/2017

10/11/2017

10/10/2018

9/16/2020

5/18/2021

5/18/2022
	

Result ug/L

25.0 U
25.0 U
_J.O U
10.0 U
_J.O U
1.0 U
10.0 U
10.0 U
10.0 U
1.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
5.0 U
_5.0 U
5.0 U
0.95 J

C



-



Date

10/6/1999
10/7/2002
10/22/2008
4/29/2009
10/14/2009
4/27/2010
10/20/2010
4/27/2011
10/27/2011
5/2/2012
10/11/2012
5/15/2013
10/19/2016
5/25/2017
10/11/2017
10/10/2018
9/16/2020
5/19/2021
5/18/2022

Result ug/L

v *

FAG-36

Date

Result ug/L

10/6/1999

50.0 U

10/7/2002

25.0 U

10/22/2008

13.6

5/20/2009

6.9 J

10/16/2009

12.2 J

4/28/2010

14.9

10/21/2010

15.0

4/27/2011

11.6 J

10/27/2011

10.0 U

5/3/2012

12.2

10/11/2012

6.2

5/15/2013

6.7

10/20/2016

10.6

5/31/2017

5.9

10/11/2017

6.8

10/10/2018

6.5

9/16/2020

5.0 U

5/19/2021

10.0 U

5/18/2022

<10.0



-?:x

FAG-50

Date

Result ug/L

10/6/1999

500 U

5/4/2000

5.0 U

10/7/2002

25.0 U

10/21/2008

1.0 U

5/20/2009

1.0 U

12/16/2009

1.0 U

4/28/2010

1.0 U

4/27/2011

20.0 U

10/25/2011

20.0 U

5/3/2012

1.0 U

10/10/2012

20.0 U

5/15/2013

20.0 U

10/20/2016

20.0 U

5/31/2017

20.0 U

10/8/2017

NS

10/11/2017

NS

9/15/2020

NS

5/19/2021

20.0 U

5/19/2022

<25.0

i ¦¦

i

H
"

, '4



FAG-62

Date

Result ug/L

10/7/1999

37.0

4/4/2000

50.0 U

10/7/2002

25.0 U

10/23/2008

1.0 U

4/29/2009

2.0 U

10/13/2009

1.0 U

4/29/2010

1.0 U

10/20/2010

2.0 U

4/27/2011

1.0 U

10/26/2011

1.0 U

5/1/2012

1.0 U

10/10/2012

2.0 U

5/15/2013

5.0 U

10/19/2016

1.0 U

5/27/2017

1.0 U

10/8/2017

NS

10/11/2018

NS

9/15/2020

NS

5/18/2021

1.0 U

5/17/2022

<1.0

-



•S&K ^

FAG-33

Date

Result ug/L

10/6/1999

1.0 U

10/4/2002

1.0 U

10/20/2008

1.0 U

4/28/2009

1.0 U

10/14/2009

1.0 U

4/27/2010

1.0 U

10/20/2010

1.0 U

4/27/2011

1.0 U

10/27/2011

1.0 U

5/2/2012

1.0 U

10/11/2012

1.0 U

5/14/2013

1.0 U

10/18/2016

1.0 U

5/27/2017

1.0 U

10/8/2017

1.0 u

10/9/2018

1.0 u

9/15/2020

1.0 u

5/18/2021

1.0 u

5/17/2022

<1.0

1

FAG-85

Date

Result ug/L

10/6/2002

25.0 U

10/23/2008

5.0 U

5/20/2009

10.0 U

10/16/2009

5.0 U

4/30/2010

1.0 U

10/19/2010

1.0 U

4/27/2011

3.3

10/25/2011

20.0 U

5/2/2012

20.0 U

10/9/2012

5.0 U

5/15/2013

5.0 U

10/19/2016

5.0 U

5/31/2017

2.0 U

10/11/2017

10.0 U

10/11/2018

2.5

9/17/2020

10.0 U

5/21/2021

37.2

5/19/2022

53.8

'





¦ 0

H L_

500
	I Feet

O	UPPERMOST GROUNDWATER

O	MiSSISSiPPIAN AQUIFER

J	= ESTIMATED CONCENTRATION

U	= NOT DETECTED

NS	= NOT SAMPLED; INSUFFICIENT WATER

UPPERMOST GROUNDWATER
ANALYTICAL RESULTS
VINYL CHLORIDE (VC) 1999 TO 2021

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 4-1C

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EEEEfll


-------
MAMMONS BO U Lv

Result ug/L

Result ug/L

2/23/1999

10/16/2002

10/5/2002

10/23/2008

10/21/2008

4/29/2009

4/29/2009

10/15/2009

10/15/2009

4/29/2010

4/28/2010

10/21/2010

10/21/2010

4/28/2011

A D 1 FAG-22—^
FAG-56—
FAG-AW4—

5&fag-620^

FAG-33—f
• ¦ UFAG-47 Q O ¦
O!',	FAG-50 FA|

4/27/2011

10/27/2011

10/26/2011

5/3/2012

5/2/2012

10/11/2012

10/10/2012

5/16/2013

5/15/2013

10/20/2016

10/19/2016

5/31/2017

5/31/2017

10/12/2017

10/12/2017

10/11/2018

10/11/2018

9/17/2020

9/16/2020

5/19/2021

5/19/2021

5/18/2022

5/18/2022

Result ug/L

Result ug/L

10/16/2002

3/1/1999

10/21/2008

10/6/2002

4/28/2009



10/23/2008

10/14/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/27/2010

5/5/2011

10/19/2010

10/26/2011

5/5/2011

5/2/2012

10/26/2011

10/10/2012

5/3/2012

5/15/2013

10/10/2012

10/19/2016

5/14/2013

5/30/2017

10/19/2016

10/12/2017

5/30/2017

10/10/2018

10/11/2017

9/17/2020

10/10/2018

5/20/2021

9/16/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/16/2002

Result ug/L

10/20/2008

10/16/2002

4/28/2009

10/22/2008

10/13/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/28/2010

5/5/2011

10/20/2010

10/25/2011

4/26/2011

5/2/2012

10/26/2011

10/9/2012

5/2/2012

5/14/2013

10/10/2012

10/18/2016

5/14/2013

5/24/2017

10/18/2016

10/11/2017

5/25/2017

10/11/2018

10/8/2017

9/16/2020

10/10/2018

5/19/2021

9/18/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/15/2002

Result ug/L

10/21/2008

10/16/2002

4/28/2009

10/21/2008

10/13/2009

4/28/2009

4/27/2010

10/13/2009

10/20/2010

4/27/2010

4/26/2011



10/20/2010

10/25/2011

4/26/2011

5/1/2012

10/25/2011

10/9/2012

5/1/2012

5/15/2013

Result ug/L

10/9/2012

10/19/2016

5/14/2013

10/14/2002

5/30/2017

10/18/2016

10/20/2008

10/11/2017

5/25/2017

4/27/2009

10/9/2018

10/8/2017

10/13/2009

9/16/2020

10/9/2018

4/26/2010

5/18/2021

9/15/2020

10/19/2010

5/17/2022

5/18/2021

4/26/2011

5/17/2022

10/25/2011

Result ug/L

5/1/2012

10/9/2012

10/15/2002

5/14/2013

10/21/2008

Result ug/L

10/18/2016

4/29/2009

5/25/2017

6/7/1999

10/14/2009

10/8/2017

1/1/2002

4/28/2010

10/9/2018

3/1/2002

10/20/2010

Result ug/L

9/15/2020

5/1/2002

4/27/2011

4/29/1993

5/18/2021

7/1/2002

10/26/2011

6/1/1995

5/17/2022

9/1/2002

5/2/2012

4/9/1999

11/1/2002

10/10/2012

10/23/2008

10/23/2008

5/15/2013

4/30/2009

4/30/2009

10/19/2016

10/16/2009

10/16/2009

5/30/2017

4/29/2010

4/29/2010

10/11/2017

10/20/2010

10/20/2010

10/9/2018

4/28/2011

4/28/2011

9/15/2020

10/25/2011

10/25/2011

5/18/2021

5/4/2012

5/4/2012

5/17/2022

10/10/2012

10/10/2012

5/15/2013

5/15/2013

10/20/2016

10/20/2016

5/31/2017

5/31/2017

10/11/2017

10/11/2017

10/11/2018

10/11/2018

9/17/2020

9/17/2020

5/20/2021

5/20/2021

5/19/2022

5/19/2022

Hi mhsHME

[Aerial Imagery Source: Google Earth , dated 3/20/2016.

RW-341A

PROJECT: 1690004605 DATED: 8/9/2022 DESIGNER: CKL	L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2022\4-2A_SprWtr& Miss Aq Analytical Results-TCE.dwg

O	SURFACE WATER

O	UPPERMOST GROUNDWATER

O	MISSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

EaSEsfll

SPRING WATER AND MISSISSIPPIAN
AQUIFER ANALYTICAL RESULTS
TRICHLOROETHENE (TCE) -1999 TO 2022

FIGURE 4-2A

D = DILUTED
U = NOT DETECTED
NS = NOT SAMPLED; INSUFFICIENT WATER

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI


-------
MAMMONS BO U

r." efBj I v-/-®

Result ug/L

Result ug/L

2/23/1999

10/16/2002

10/5/2002

10/23/2008

10/21/2008

4/29/2009

4/29/2009

10/15/2009

10/15/2009

4/29/2010

4/28/2010

10/21/2010

10/21/2010

4/28/2011

0	FAG-22—

F AG-56—
• FAG-AW4-—(j	—

b h

FAG-50 FAG-88 FAG-89

4/27/2011

10/27/2011

10/26/2011

5/3/2012

5/2/2012

10/11/2012

10/10/2012

5/16/2013

5/15/2013

10/20/2016

10/19/2016

5/31/2017

5/31/2017

10/12/2017

10/11/2018

10/11/2018

9/16/2020

9/17/2020

9/16/2020

5/19/2021

5/19/2021

5/18/2022

5/18/2022

Result ug/L

Result ug/L

* 10/16/2002

3/1/1999

10/21/2008

10/6/2002

4/28/2009

10/23/2008

10/14/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/27/2010

5/5/2011

10/19/2010

10/26/2011

5/5/2011

5/2/2012

10/26/2011

10/10/2012

5/3/2012

5/15/2013

10/10/2012

10/19/2016

5/14/2013

5/30/2017

10/19/2016

10/12/2017

5/30/2017

10/10/2018

10/11/2017

9/17/2020

10/10/2018

5/20/2021

9/16/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/16/2002

Result ug/L

10/20/2008

10/16/2002

4/28/2009

10/22/2008

10/13/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/28/2010

5/5/2011

10/20/2010

10/25/2011

4/26/2011

5/2/2012

10/26/2011

10/9/2012

5/2/2012

5/14/2013

10/10/2012

10/18/2016

5/14/2013

5/24/2017

10/18/2016

10/11/2017

5/25/2017

10/11/2018

10/8/2017

9/16/2020

10/10/2018

5/19/2021

9/18/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/15/2002

Result ug/L

10/21/2008

10/16/2002

4/28/2009

10/21/2008

10/13/2009

4/28/2009

4/27/2010

10/13/2009

10/20/2010

4/27/2010

4/26/2011

10/20/2010

10/25/2011

4/26/2011

5/1/2012

10/25/2011

10/9/2012

5/1/2012

5/15/2013

Result ug/L

10/9/2012

10/19/2016



5/14/2013

10/14/2002

5/30/2017

10/18/2016

10/20/2008

10/11/2017

5/25/2017

4/27/2009

10/9/2018

10/8/2017

10/13/2009

9/16/2020

10/9/2018

4/26/2010

5/18/2021

9/15/2020

10/19/2010

5/17/2022

5/18/2021

4/26/2011

5/17/2022

10/25/2011

Result ug/L

5/1/2012

10/9/2012

10/15/2002

5/14/2013

10/21/2008

Result ug/L

10/18/2016

4/29/2009

5/25/2017

6/7/1999

10/14/2009

10/8/2017

1/1/2002

4/28/2010

10/9/2018

3/1/2002

10/20/2010



9/15/2020

5/1/2002

4/27/2011

5/18/2021

7/1/2002

10/26/2011

Result ug/L

5/17/2022

9/1/2002

5/2/2012

4/9/1999

11/1/2002

10/10/2012

10/23/2008

10/23/2008

5/15/2013

4/30/2009

4/30/2009

10/19/2016

10/16/2009

10/16/2009

5/30/2017

4/29/2010

4/29/2010

10/11/2017

10/20/2010

10/20/2010

10/9/2018

4/28/2011

4/28/2011

9/15/2020

10/25/2011

10/25/2011

5/18/2021

5/4/2012

5/4/2012

5/17/2022

10/10/2012

10/10/2012

5/15/2013

5/15/2013

10/20/2016

10/20/2016

5/31/2017

5/31/2017

10/11/2017

10/11/2017

10/11/2018

10/11/2018

9/17/2020

9/17/2020

5/20/2021

5/20/2021

5/19/2022

5/19/2022

O RW-341A

|Aerial Imagery Source: Google EarthrM, dated 3/20/2016.

PROJECT: 1690004605 DATED: 12/6/2022 DESIGNER: CKL	L:\Loop Project Files\_CAD\1690004605_FAG Bearings\_2022\4-2B_Spr Wtr & Miss Aq Analytical Results-DCE.d

O	SURFACE WATER

O	UPPERMOST GROUNDWATER

O	MiSSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

D	= DILUTED

U	= NOT DETECTED

NA	= NOT ANALYZED

SPRING WATER AND MISSISSIPPIAN AQUIFER

ANALYTICAL RESULTS
CIS-1.2-DICHLOROETHENE (DCE) -1999 TO 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 4-2B

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

LiZfli


-------
MAMMONS BO U Lv

Result ug/L

Result ug/L

2/23/1999

10/16/2002

10/5/2002

10/23/2008

10/21/2008

4/29/2009

4/29/2009

10/15/2009

10/15/2009

4/29/2010

4/28/2010

10/21/2010

10/21/2010

4/28/2011

A D	. .. FAG-22-v^n

FAG-56—--i"
FAG-AW4—C

Kfag-62Q\' /

FAG-33^
FAG-47 O O u
O FAG-46 FAG-50 FAG

4/27/2011

10/27/2011

10/26/2011

5/3/2012

5/2/2012

10/11/2012

10/10/2012

5/16/2013

5/15/2013

10/20/2016

10/19/2016

5/31/2017

5/31/2017

10/12/2017

10/12/2017

10/11/2018

10/11/2018

9/17/2020

9/16/2020

5/19/2021

5/19/2021

5/18/2022

5/18/2022

Result ug/L

Result ug/L

10/16/2002

3/1/1999

10/21/2008

10/6/2002

4/28/2009

10/23/2008

10/14/2009

cp. y

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/27/2010

5/5/2011

10/19/2010

10/26/2011

5/5/2011

5/2/2012

10/26/2011

10/10/2012

5/3/2012

5/15/2013

10/10/2012

10/19/2016

5/14/2013

5/30/2017

10/19/2016

10/12/2017

5/30/2017

10/10/2018

10/11/2017

9/17/2020

10/10/2018

5/20/2021

9/16/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/16/2002

Result ug/L

10/20/2008

10/16/2002

4/28/2009

10/22/2008

10/13/2009

4/29/2009

4/27/2010

10/14/2009

10/19/2010

4/28/2010

5/5/2011

10/20/2010

10/25/2011

4/26/2011

5/2/2012

10/26/2011

10/9/2012

5/2/2012

5/14/2013

10/10/2012

10/18/2016

5/14/2013

5/24/2017

10/18/2016

10/11/2017

5/25/2017

10/11/2018

10/8/2017

9/16/2020

10/10/2018

5/19/2021

9/18/2020

5/19/2022

5/19/2021

5/18/2022

Result ug/L

10/15/2002

Result ug/L

10/21/2008

10/16/2002

4/28/2009

10/21/2008

10/13/2009

4/28/2009

4/27/2010

10/13/2009

10/20/2010

4/27/2010

4/26/2011

10/20/2010

10/25/2011

4/26/2011

5/1/2012

10/25/2011

10/9/2012

5/1/2012

5/15/2013

Result ug/L

10/9/2012

10/19/2016

5/14/2013

10/14/2002

5/30/2017

10/18/2016

10/20/2008

10/11/2017

5/25/2017

4/27/2009

10/9/2018

10/8/2017

10/13/2009

9/16/2020

10/9/2018

4/26/2010

5/18/2021

9/15/2020

10/19/2010

5/17/2022

5/18/2021

4/26/2011

5/17/2022

10/25/2011

Result ug/L

5/1/2012

10/9/2012

10/15/2002

5/14/2013

10/21/2008

10/18/2016

4/29/2009

5/25/2017

10/14/2009

10/8/2017

4/28/2010

10/9/2018

10/20/2010

9/15/2020

4/27/2011

5/18/2021

10/26/2011

Result ug/L

Result ug/L

5/17/2022

5/2/2012

4/9/1999

6/7/1999

10/10/2012

10/23/2008

10/23/2008

5/15/2013

4/30/2009

4/30/2009

10/19/2016

10/16/2009

10/16/2009

5/30/2017

4/29/2010

4/29/2010

10/11/2017

10/20/2010

10/20/2010

10/9/2017

4/28/2011

4/28/2011

9/15/2020

10/25/2011

10/25/2011

5/18/2021

5/4/2012

5/4/2012

5/172022

10/10/2012

10/10/2012

5/15/2013

5/15/2013

10/20/2016

10/20/2016

5/31/2017

5/31/2017

10/11/2017

10/11/2017

10/11/2018

10/11/2018

9/17/2020

9/17/2020

5/20/2021

5/20/2021

5/19/2022

5/19/2022



|Aerial Imagery Source: Google EarthrM, dated 3/20/2016.

PROJECT: 1690004605 DATED: 12/6/2022 DESIGNER: CKL	L:\Loop Project Files\_CAD\1690004605,FAG Bearings\_2022\4-2C_Spr Wtr & Miss Aq Analytical Results-VC.d

O	SURFACE WATER

O	UPPERMOST GROUNDWATER

O	MiSSISSiPPIAN AQUIFER

E	= EXCEEDS CALIBRATION RANGE

J	= ESTIMATED CONCENTRATION

D	= DILUTED

U	= NOT DETECTED

NA	= NOT ANALYZED

SPRING WATER AND MISSISSIPPIAN
AQUIFER ANALYTICAL RESULTS
VINYL CHLORIDE (VC) -1999 TO 2022

NEWTON COUNTY WELLS SITE

VILLAGES OF SILVER CREEK AND
SAGINAW, MISSOURI

FIGURE 4-2C

RAMBOLL US CONSULTING, INC.

A RAMBOLL COMPANY

LiZfli


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Well Inspection and Maintenance Logs (May 2022)

December 2022


-------
monitoring well inspection record

NEWTON COUNTY WELLS SITE
VILLAGES OF SILVER CREEK AND SAGINAW, MISSOURI

Sample Event:	Awt/A-*- ffUtS

Date;	/ 0k					

Personnel and afmialitm: \M t CC, Sje.. J"? (g£ 4-^

Well

inspected

(Yes/No)

FAG-47

V

	 f\

FAG-SO

Y

/\Jo

FAG-62

V

/l/c*

RI-MW-l

V

AJm

RI-MW-2

y

/iJo

FAG-22

Y

*4* XT"

FAG-56

Y

/U

FAG-31

Y

AJp

FAE-32

Y

AJs

FAG-74

Y

A>o

FAC-73

Y



FAG-33

Y



FAG-34

Y

/t4

FAG-35

V

	AJo

FAG'36

y

Mp

FAG-85

w

•

AJo

FAG-AW4

r

/A

	/V; D	

FAG-OS

Y

A/„

FAG-11

Y

AJo

FAC-88

Y

Ma

FAG-89

V

//o

RI-MW-9

y

M

RI-MW-5

Y


-------
MONITORING WELL MAINTENANCE RECORD
NEWTON COUNTY WELLS SITE
VILLAGES OF SILVER CREEK AND SAGINAW, MISSOURI

Sample Event: _	Auai/Av fcu>3

Date:

Personnel:	c.cnftirA.b 'SM+uitY, XZbllm

Well

Describe maintance required, time-frame maintenance will be conducted within, maintenance
conducted, or reason well could not be inspected, (attach additional sheets if necessary)



f"A	bolhr,	irvvx. eci.1^

N-/


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Field Instrument Calibration Logs (May 2022)

December 2022


-------
FieW	Calibration Checklist

Date: -5/H 	

Calibrated by:	C/j

3-Point pH calibration (should take at least 4.5 minutes):

1

2

3

4

5

6

7

8

9

10

11

Lot#

OkhfrH Exp:J t	3

Pour pH 7.0 standard into the calibration cup and immerse pH sensor.

Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH. Note below.

Discard used calibration standard, and rinse calibration cup and probes with Dl water.

Pour pH 4.0 standard into the calibration cup and immerse pH sensor. Lot	Exp:_J.

Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH. Note standard below.

Discard used calibration standard, and nnse calibration cup and probes with Dl water.



Pour pH 10.0 standard into the calibration cup and immerse pH sensor. Lot ft i
Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH. Note below

C£>HnX Exp:

12 Discard used calibration standard, and rinse calibration cup and probes with Dl water.

Dissolved Oxygen (% DO) calibration (should tete af teas* 10 minutes)

r	_11 iFliyoi Hint..

1.

2.

3.

4.

5.

6.

7.

+ 10tnin



Ensure unit has been on for at least 10 minutes.

Fnfer the local barometric pressure.

{Note: to convert from inches (common on a weather app or forecast) to mmHg, multiply by 25 4, then

to correct to Joplin's altitude, subtract 27.07 mmHg.) _ --jv?

•?<>'oi in x25.4 = o^mmHq -27.07 = -bJ-H JO mmHg

Place ~3mm of Dl water in the bottom of the calibration cup.
i inhtiv screw on the calibration cup (only 1 or 2 threads!)

iSZin minutes for the air in the cup to become water-saturated and temp to stabilize.

'caHbrate after 30 seconds of no significant change in DO. Note below.

Discard used Dl water, and rinse calibration cup and probes with Dl water.

YSI - Serial Numberf^C^^

1	Specific Conductance. ^ .tfb 4^

2	ORP; KS-8

3	pH: point ,:?¦*«



point 2
point 3

\QO0

YSI - Serial Numbenf^^	^

1. Specific Conductance: 7-t
2 ORP:

3- pH:

Point 1:3. 6^1
Point 2: b -^3
Point 3: 10.3(3

Scjr-\

itu	' f

(0|.3'/°

Do ¦ I05: 7-7,


-------
'eld Equ^Le^ Calibration Checklist	x

Date

Calibrated by: C | AA
Turn on YSI.

Specific Conductance calibration (should take af least 1.5 minutes): Lot U: 0bSMS'X
our conductivity standard into calibration cup and immerse sensor.

Aiiow 1 rn/nuts for temperature stabilization.

Press calibrate" after 30 seconds of no significant change in specific conductance. Note below

FiiCf-arH		, . , .		 3	.	...

2.

3.

4.

'—	vw	u) ny aiyiintudfu viianyc in ajjcuiii-«

Discard used calibration standard, and rinse calibration cup and probes with Di water

6f	Exo: &ofJ- ^

Lot#:

ORP calibration (should take af least 1.5 minutes): 		.	

1.	Pour ORP (Zobeli) standard into calibration cup and immerse sensor.

2.	Allow 1 minute for temperature stabilization.

3.	Press "calibrate" after 30 seconds of no significant change in ORP. Note below.

4.	Discard used calibration standard, and rinse calibration cup and probes with DI water

3-Point pH calibration (should take af least 4.5 minutes):	A, y.,

1. Pour pH 7.0 standard into the calibration cup and immerse pH sensor Lot # Uj£_E5z—-3^XP-
Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH. Note below.

Discard used calibration standard, and rinse calibration cup and probes with DI water

¦ \\IpAx

2.

3.

4.

5.

6.

7.

8.

9.

10.

11.

12.

Lot#

Pour pH 4,0 standard into the calibration cup and immerse pH sensor.

Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH Note standard below.
Discard used calibration standard, and rinse calibration cup and probes with DI water

DQ£(38 Exp:Jl/%/±3-

Pour pH 10.0 standard into the calibration cup and immerse pH sensor. Lot #

Allow 1 minute for temperature stabilization.

Press "calibrate" after 30 seconds of no significant change in pH Note below
Discard used calibration standard, and rinse calibration cup and probes with DI water.

L)GH3ci 3.Exp: ^

Dissolved Oxygen (% DO) calibration (should take af least 10 minutes).

1 Ensure unit has been on for at least 10 minutes: Initial time: _0±t0
Enter the local barometric pressure.

+ 10min

2.

3.

4.

5.

6.

7.

e local uaronieuiu yieoouic.

(Note: to convert from inches (common on a weather app or forecast) to mmHg, multiply by 25 4, then
to correct to Joplin's altitude subtract 27.07 mmHg.)	~v

"?tin y	mmHg - 27.07 =		mmHcj

Place ~3rnmof"Diwater in the bottom of the calibration cup.
i inhtiv crrew on the calibration cup (only 1 or 2 threads!)

Smrninutes for the air in the cup to become water-saturated and temp to stabilize.

P ess !caS after 30 seconds of no significant change in DO. Note beiow.

Discard used DI water, and rinse calibration cup and probes with DI water.

YSI - Serial Number:£/t?3)~£>

1 Specific Conductance. I-*n

2. ORP: 3"3 ^

3 PH'Point 1: 3-^
point2:
point 3:

\>D-,

YSI - Serial Number:	S

1.	Specific Conductance:

2.	ORP:

3.	pH:

Point 1:3. 85"

Point 2:fj. c, ^

Point 3: q g

Di: 
-------
Reid Equipment ra. ^

ntCa")bration Checklist

Date:

Calibrated by; £c» [M

Tum on YSI.

1.	Cfllbratl0n (should take at least 1.5 minutes): Lot #: OtP W 5 S Exp:	_

2-	?andafd int0 ««bration cup and immerse sensor	

3. FW - , 5 • temPerature stabilization

4 Disrarrfnco^ft8 ,f8r 30 seconds of no significant change in specific conductance. Note below.

^''bration standard, and rinse calibration cup and probes with Dl water.

*a'tea'feasf1.5 minutes): Lotfr H f, M < F,n	.

? aii« .* - ^ ^ standard into calibration cup and immerse sensor.

*• £,iow I min"te for temperature stabilization.

. Press calibrate" after 30 seconds of no significant change in ORP. Note below,
iscard used calibration standard, and rinse calibration cup and probes with Dl water.

3-Point pH calibration (should take at least 4.5 minutes):	. ,	,, /-to fs \

1.	Pour pH 7,0 standard into the calibration cup and immerse pH sensor. Lot U f) d H Exp:	' I ^ ^

2.	Allow 1 minute for temperature stabilization.

3.	Press "calibrate" after 30 seconds of no significant change in pH. Note below.

4.	Discard used calibration standard, and rinse calibration cup and probes with Dl water.

5.	Pour pH 4 0 standard into the calibration cup and immerse pH sensor. Lot #	& Exp: 11

6.	Allow 1 minute for temperature stabilization.

7.	Press "calibrate" after 30 seconds of no significant change in pH. Note standard below.

8.	Discard used calibration standard, and rinse calibration cup and probes with Dl water.

9.	Pour pH 10.0 standard into the calibration cup and immerse pH sensor. Lot #QGH^^ Exp:

10.	Allow 1 minute for temperature stabilization.

11.	Press "calibrate" after 30 seconds of no significant change in pH. Note below

12.	Discard used calibration standard, and rinse calibration cup and probes with Dl water.

Dissolved Oxygen (% DO) calibration (should take at least 10 minutes):

1 Ensure unit has been on for at least 10 minutes; Initial time: O too + 10min =__6JMO

2.	Enter the local barometric pressure.

(Note: to convert from inches (common on a weather app or forecast) to mmHg, multiply by 25.4, then
to correct to Joplin's altitude subtract 27.07 mmHg.)

30 .oH in. x 25.4 = l-C.^.ofU mmHg - 27.07 = J •*?*•/fa mmHg

3.	Place -3mm of Di water in the bottom of the calibration cup.

4	Lightiy screw on the calibration cup (only 1 or 2 threads!)

5	Allow 10 minutes for the air in the cup to become water-saturated and temp to stabilize.

6	Press "calibrate" after 30 seconds of no significant change in DO. Note below.

7	Discard used Di water, and rinse calibration cup and probes with Dl water.

YSI - Serial Number:c

1 Specific Conductance:	%

2.

3. pH-"

DD

q,o3

| %

Point 1
Point 2
point 3

YSI - Serial Number: Ft40 I >65

1

2.

3.	pH:



. Specific Conductance: 1,17 ^7

Point 1: 3.^9
Point2:

Point 3: iCkq3

00: lol.


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Groundwater and Surface Water Sampling Logs
(May 2022)

December 2022


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

- Temp °C

Spec Cond (uS/cm)

DO fmg/L}

pH

ORP(mV)

Flow (mL/min)

Notes

«ftO

34-.0U

/a.?

6«A.3



b

1.20. a*

M60



96 6

Vi.o-9-

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uoa



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tin









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19. 







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SAMPLE COLLECTION DATA

[Date «T/igZ^

[Time: *00

Sample Numbers
Note any QA/QC Samples:

#of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

5

*/£»n«l. VaA

m



f

3^f> mL, pl<*ff#Uy



a/, I trifles

















1

Hach Ampule

None

Ferrous Iron

A/KU

OBSERVATIONS/COMMENTS:

collco+ List & Fi'ala tMp-

WEATHER:

WF, £V\&w«r
-------
•GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

IpE

Temp C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)





3M





_H£2i2_

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341-

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SAMPLE COLLECTION DATA



jSampie Number PHh-n-w-rr

JNote any QA/Q.C samples:

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(me/L)



HOmL t/fWl

¦Hr,f

vn(j$

i

"LfiOmL pfalk fs

rrv> /

mininrtrs

















i

Hach Ampuie

None

Ferrous iron

Max.

WEATHER-

Ti°t\ sunny.


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605



it of Containers

3,

Size/Type

Horn I

Preservative

40nou VOf\

Wd

Analytical Parameter(s)

-L.

OBSERVATIONS/COMMENTS:

DO ^o^\V\'ZJ2/. N&zcLtcl "to (Y)0Ve^ van odr (HO
Site ernpl otjec +c obfzw/h to pAx)pcuA^Q^
	p/\et-z^-	

mu y^m u

	Hach Ampule	

flflVlA

"W

	J^Ar^ t

./v< TV\Y (A Sa;,



None

njJ/vL/r^;

Result
(mg/L)

Ferrous Iron

WEATHER:

OJO

%& \ A . U U0 F.


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Purge Time (24 hour)



Depth to Water (feet)

751 '	

Temp UC

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP (mV)

Fiow (mL/min)

¦ut (fi

33-

1EE



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£j±D_

2d

fl

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^23

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Si

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12ZLJ2-

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^4,

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aa

SU£L

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5*y>

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IS/, 9

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SAMPLE COLLECTION DATA

[Sample Number: FAA-- ^1— \a/~ I ~7

e:

iNote any QA/Q.C samples:

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
~ (mg/L)

•3

*n «o/. \,nn

W4

\/DA

*

qn»,i. vqA-



MPh ,1

i

ij^o ya l. pi a c+t o

l\XnA£> ^ y



(

1

1>=0 pld&hCs

Hach Artfpule

rums, <&a
-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

SAMPLE COLLECTION DATA

mmmm-fiTTi

¦Time:

Tfefe-

{Sample Number:

INote any QA/QC samples:



# of Containers

Size/Type

Preservative

Analytical Parameter(s)





1 Ml© ^

\/qA- 1

Hc.y

veCs



4

1 MO , iA... 1 1

si -

~/C/k





i

S~\t 7'



/? 5

Result

s

/wt

MIUO"?



(mg/L)

1

Hach Ampule

None

Ferrous Iron

o.^"D

OBSERVATIONS/COMMENTS:

of 85











weather § 3 °p

P^f-L[ J

P-

•—0
>

o

' j l/J< A d

ss£




-------
e §

- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

|PROJECT NAME: Newton County Wells Site

WELL PURGE DATA

Date/Time 15^ 1

Well Construction

*z,* we, stvjbuj?



Total Volume Purged (gallons)

5 AM

Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)



|Static Water Level



Well Measurement Technique

?

r**

1

|Total Depth



Well Purge Equipment



jScreen Length (feet)



Other (list here) \tlWt 1

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feejf

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min) /

Notes

1*3.0

/

\v/. 15

w%.a

5«





/



\t>m

/

Ho.**

WO. 9

JS.S4

%AZ

ZfZXa

/





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tm-iL







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SAMPLE COLLECTION D

IT A















Late

iTime: " J

[Sample Number:



Note any QA/QC samples

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)



3









¦b









4







Result

!







(me/L)

1

Hach Ampule

None

Ferrous iron

©»02

OBSERVATIONS/COMMENTS:





WEATHER:


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

¦PROJECT NUMBER: 1690004605

(PROJECT NAME: Newton County Wells Site

¦_	

jDate/Time	| g/\%! H

LOCATION NUMBER:

! 1

Weil Construction

Sampler



Total Volume Purged (gallons)

Well Measurements (feet below top of casing)

54.H*

Pump is set at (feet below top of casing)

Static Water Level

Well Measurement Technique

Total Depth

Well Purge Equipment

Screen Length (feet)

FIELD PARAMETERS

Other (list here)

I Weil tfV ( 5-

Depth to water (feet)

Temp C

1-3.M

Spec Cond (uS/cm)

DO (mg/L)

. XIM

ORP (mV)

T

Flow (njL/min)

a

i2fU



&

iPr

*ȣ/ V ar\

£

y





SAMPLE COLLECTION DATA



(Sample Number:

Note any QA/QC samples:



# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

i


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

SAMPLE COLLECTION DATA

|Date W14L4. 1

Sample Number:







|Time:	 w



Note any QA/O.C samples: J? •" Crt5"T" A w

<>5V



#of Containers

Size/Type

Preservative

Analytical Parameter(s)



t

Hti snL vA«. f i

Htl

l/ec





Mr» /hL

/-l

A1



1

t .





Result



A* 1/

ItTi t, «-C I ^

f j

(mg/L)

1

Hach Ampule*

None

Ferrous Iron

O

OBSERVATIONS/COMMENTS:

WEATHER: ft i

or

F,










-------
. GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP(mV)

Fiow (mL/min)

Notes







3*1 U. to

S.2.S

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12.1. *5

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————













































~	

















——

SAMPLE COLLECTION DATA

fc;

02. 3-

Sample Number:

Note any QA/QC samples:

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

%

WftmL



V&Cc,

•3

ttftrv.u VtPr

yiXVv-o

MCf

I

7-0

OBSERVATIONS/COMMENTS:

WEATHER:

SD'fj f*rH\j cioway.


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

|PROJECT NAME: Newton County Wells Site

LOCATION NUMBER:

WELL PURGE DATA





Well Construction



Sampier I Y-t/ye-

Total Volume Purged (gallons)



Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)



Static Water Level



Well Measurement Technique



Total Depth

±\. %

Well Purge Equipment



Screen Length (feet)



Other (list here) ftsOVC*- , A\XfiA * VJ6&VC 1

FIELD PARAMETERS

,gu6gc Tmi_e ^4 IiuotT

"Depth to Water (feejft

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min) /

Notes

* o

/

tt.'A



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1

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)











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/ /











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i ^











/



SAMPLE COLLECTION DATA

(Date:



Sample Number: — M'i" U





Fime:



zzj

Note any QA/QC samples:——





ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)



<2,



MCt.





l

rtJl ftoi&L.















Result









(mg/L)

i

Hach Ampule

None

Ferrous Iron

®-?T

OBSERVATIONS/COMMENTS:

Y\o










-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Depth to Water (feet)

Temp °C

lb. 1

Spec Cond (uS/cm)

"S5F

£

DO (mg/L)

SSI

pH

52E
EI

ORP (mV)



~SL

Flow (mL/min)

o

32:

1£5

3-

SEE

¦

3:

s

1 3 B-3

Ik



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UfT- A



s.o

LI

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ion

SAMPLE COLLECTION DATA



jSampie Number:

|Note any QA/QC samples:	L»t£*T A

001 m

ANALYSES

# of Containers

Size/Type

f # Preservative

Analytical Parameter(s)

Result
(me/L)

s



K&-\



1

a!n /»V i- *£*S/vv,





















1

Hach Ampule

None

Ferrous Iron

o-o

OBSERVATIONS/COMMENTS:

^ f* ^ j>ew+^-i cU-» dy U/ i^eJ iS/**p


-------
¦ GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

¦PROJECT NAME: Newton County Wells Site

WELL PURGE DATA



Well Construction

'-=•< '' PuC Sfic-k. v3^>

Isampler | ~StC-S (

Total Volume Purged (gallons)

-=h

|Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

Ay/A-

|Static Water Level



Well Measurement Technique



|Total Depth



Well Purge Equipment

i / -*—

|Screen Length (feet)



|0ther (list here) ^ \*l\/ 2*1. a«kA I

FIELD PARAMETERS

Purge Time (24 hour)

15

#of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/U

?

Hn V<9A



I/O c € f


-------
• GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

PROJECT NUMBER: 1690004605

PROJECT NAME: Newton County Weils Site

WELL PURGE DATA

LOCATION NUMBER:

fhcn-eo

Date/Time



Well Construction



Sampler



Total Volume Purged (gallons)

Well Measurements (feet below top of casing)

Stati^A/ater Level	'

Pump is set at {feet below top of casing)



Well MeasurementTechnique

Total Depth

iBL

Well Purge Equipment



Screen Length (feet)

FIELD PARAMETERS

Other (list here) ftoiVCl AlvV Vt

¦Purge Time (24 hour)-



•Depth to Water (feet)

2

Temp C

Spec Cond (uS/cm)

DO (mg/L)

9--QU

<*-t>

pH

ORP(mV)

Fiow (mL/min)



\M.1-

77U\



£

A±iJs_

2.Jzls.

_SS£L







-f

SAMPLE COLLECTION DATA

Sample Number:

t>fc4Vf

Note any QA/QC samples:

ANALYSES

#of Containers

Size/Type

Preservative

Analytical Parameter(s)













-3-









\







Result

i







(mg/L)

i

Hach Ampule

None

Ferrous iron

SM

OBSERVATIONS/COMMENTS:

rvocd&~(

WEATHER:	\JVJ


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

|PROJECT NAME: Newton County Wells Site

WELL PURGE DATA

(LOCATION NUMBER:

st-

Date/Time

ti\o

Well Construction

Z"

Sampler



Total Voiume Purged (gallons)



Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

Static Water Level

Well Measurement Technique

Total Depth

_H^4.

Well Purge Equipment

Other (list here) fe&S.\£jf, fteu&s&C- VAWC



Screen Length (feet)

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feei

Temp °C

TTT

Spec Cond (uS/cm)

iO	

DO (mg/L)

PH

ORP (mV)

Flow (mL/min)

z

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1



w.i

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n- D



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2.







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SAMPLE COLLECTION DATA



¦Time: I^tCD

INote any QA/QC samples:

ANALYSES

#of Containers

Size/Type

Preservative

Analytical Parameter(s)



1









3









1







Result

t







(mg/L)

1

Hach Ampule

None

Ferrous Iron

©.CO

OBSERVATIONS/COMMENTS:



WEATHER:


-------
6

V

- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

(PROJECT NUMBER: 1690004605

|PROJECT NAME: Newton County Wells Site

LOCATION NUMBER:

WELL PURGE DATA

Date/Time 14H1"

Well Construction

±« Alt 4^5*.

Sampler

Total Volume Purged (gallons)



Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

		

{Static Water Level



Well Measurement Technique

®		

(Total Depth



Well Purge Equipment



jScreen Length (feet)



Other (list here) gCM.Vg,V , d vtClUC I

FIELD PARAMETERS

.... .

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP(mV)

Flow (mL/min) /

Notes



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SAMPLE COLLECTION DATA

Time: lyi/

Sample Number: fA6m-U»£. -\»-X?r
Note any QA/QC samples: •

ANALYSES

ttof Containers

Size/Type

Preservative

Analytical Parameter(s)













5









i







Result

f







(mg/L)

1

Hach Ampuie

None

Ferrous Iron



OBSERVATIONS/COMMENTS:

HwdW b \A0\ Ofc.5 VWAQXi

WEATHER, -q ^	^	j £	.


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

¦PROJECT NAME: Newton County Weils Site

LOCATION NUMBER:

WELL PURGE DATA





Well Construction



Sampler | J (C ~ f/V\

Total Volume Purged (gallons)



Well Measurements (feet beiow top of casing)

Pump is set at (feet below top of casing)

A>U*

|static Water Level



Well Measurement Technique

/*/v.

|Total Depth



Well Purge Equipment



jScreen Length (feet)



Other (list here) | O-t \\ ^1 ^ 1 S I

FIELD PARAMETERS



Depth t(

Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP (mV)

Flow (

nL/min)

Notes

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-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

¦PROJECT NUMBER: 1690004605

FIELD PARAMETERS

ll6Lii7~

"Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)

Notes



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SAMPLE COLLECTION DATA

[Time: 1 te *7 Pi

[Sample Number:

Note any QA/QC samples:

ft of Containers

Size/Type

Preservative

Analytical Parameter(s)



s









4









1







Result









(mg/L)

1

Hach Ampule

None

Ferrous Iron

o.p

OBSERVATIONS/COMMENTS.^ \^V^\>A5L3 Y«, (X£» (XVcVVWX^/


-------
¦ GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

FIELD PARAMETERS

Rjiyo-UmiU^a liuuiT"

—I^&JL	

Depth to Water (feet)

^ Temp°C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)

^ Notes

Jo

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SAMPLE COLLECTION DATA

¦Date: ^
fTime:



[Sample Number:

mm







Note any QA/QC samples: K\(

#of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

































1

Hach Ampule

None

Ferrous Iron

"2.H



WfcAIHbR>

\ Vno 0A3 v

Lr


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

Temp C

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP (mV)

Flow (mL/min)

j5Hi

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SAMPLE COLLECTION DATA

|P31
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siMV

Sample Number:

Note any QA/QC samples:

# of Containers

Size/Type

HO V.QA

in

Analytical Parameter(s)

"W



U4Vr I.

t/yi,..

UqaT

, AJqup.

id



Acu^i



Besult
(mg/L)

X

Hach Ampule

SM_

OBSERVATIONS/COMMENTS:


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

¦PROJECT NUMBER: 1690004605

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

Temp C

EE

Spec Cond (uS/cm)

-^7U~7

DO (mg/L)

PH

ORP (mV)

Flow (mL/min)

^r

n

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mt:
TO

377 Kn ¦ \



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i f rrs

TTTlC

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5

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SAMPLE COLLECTION DATA



Sample Number:



Note any QA/Q.C samples:

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)



mi \!GA



VUA







Uti-

5

•?,'S"Q rr>\r\&A-,r-.

M IVi" v

T\cO> yv,









i

Hach Ampule

None

Ferrous Iron

Jib.

WEATHER:

"16° v- >


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

|PRQJECT NAME: Newton County Wells Site

WELL PURGE DATA

{LOCATION NUMBER:	.

Date/Time

Sampler

ET/El





Well Construction

Total Volume Purged (gallons)

Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

J4ZHS

Static Water Level

Total Depth

firri

5^

Weil Measurement Technique

Well Purge Equipment

p/s-fon pump

Screen Length (feet)

FIELD PARAMETERS

10.4

Other (list here)

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)

Notes

1 to O *-->

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SAMPLE COLLECTION DATA

[Date:	i

Sample Number: FACa-ftWM-

it-gd

Note any QA/QC samples:

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(he/L)

:^5

HOmL V n A

-tfrw

\/OCs



to m \ M Oft

n oao

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1

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None

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jam.

"SwnoTmeasured.Tap® does n*f- •*¦+ irrto we/l	p/'sfojo pump

WEATHER:

W", sunny


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

IPROJECT NAME: Newton County Wells Site

(LOCATION NUMBER:



WELL PURGE DATA

Date/Time - 1/Z* \'&2j>

Well Construction

i»« Aft ,l^k 	—

Sampler

Total Volume Purged (gallons)



Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)



Istatic Water Level



Well Measurement Technique

_	

|Total Depth



Well Purge Equipment



|Screen Length (feet)



Other (list here) feJU-eiT/ 1

FIEL^ PARAMETERS

(^ttfge-l iiny hour)

MX

Depth to Water (feet)^

7 T V
Temp C

Spec Cond (uS/cm)'

DO (mg/L) pH ORP (mV)

Flow (mL/min) j

Notes

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SAMPLE COLLECTION DATA

I.MMi

ISample Number: ^1/



|Time: \V ^



{Note any QA/QC samples: *¦ ¦



	1

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)



-b

HO ssl, v/0~J\

V\Ci~





%











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Result









(mg/L)

1

Hach Ampule

None

Ferrous Iron

QCtt

OBSERVATIONS/COMMENTS:

Y\C>

weather.


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

[PROJECT NAME: Newton County Wells Site

LOCATION NUMBER:



Date/Time

Sampler

SZS

Well Construction

Total Volume Purged (gallons)







Well Measurements (feet below top of casing)

t2..U

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SAMPLE COLLECTION DATA

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

3k1

16r^y/OPi

no-



t *C5»

*V*Srtl
-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

|PROJECT NAME: Newton County Wells Site

rrfowF

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

an

ORP(mV)

Flow (mL/min)

Notes

ItOS

WS.4B

1 8.ft

361.

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H.
-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

IPROJECT NAME: Newton County Wells Site

WELL PURGE DATA

I LOCATION NUMBER:

&l-MW U>

Date/Time





Well Construction

Sampler

CJtt, /fN\

Total Volume Purged (gallons)

Well Measurements (feet below top of casing)

Tj? I ' 5

Pump is set at (feet below top of casing)

HI

Static Water Level

Total Depth

£o3

Well Measurement Technique

Well Purge Equipment

pixiTsvr fii/1-frvp

Screen Length (feet)

FiELD PARAMETERS

2-0

Other (list here)

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)

Notes

1505

_1£J



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te



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TT ^v	

		











































SAMPLE COLLECTION DATA

|Date^^_

|Time: [

fsi1/27s

Sample Number:



660

Note any QA/QC samples:

ANALYSES

#of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)



qftfrrt- /OA .

Hti

vnrx

T

•2Gr> rv\L hiasnc

V\bYVL^

IMCLt^

















1

Hach Ampule

None

Ferrous Iron

run

OBSERVATIONS/COMMENTS:

WEATHER:

Q,b f i Cuirvrvv^. ^ ^


-------
• GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

¦LOCATION NUMBER:

|PROJECT NAME: Newton County Wells Site

WELL PURGE DATA

^muarja

12,'2- (Wc;

Well Construction

H'l PVO -£tliX. In

Sampler | M

Total Volume Purged (gallons)

LP

Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

191

|Static Water Level

?3. (e5

Well Measurement Technique

Pi STDvA puvymti

|Totai Depth

/

23.

ZO.q







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SAMPLE COLLECTION D

VTA















[Date:	/ ^ .

Sample Number:

PI-A/viO- 1 - t-o ' l^T

Note any QA/QC samples:

ANALYSES

#of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)



MOroL V/OA



1/0 OS .

i

rr\ U p 1 a vH r .»

in 0

OnltrfcLe^

















1

Hach Ampule

None

Ferrous Iron

n m

OBSERVATIONS/COMMENTS:




-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

[PROJECT NUMBER: 1690004605	|LOCATION NUMBER:

[PROJECT NAME: Newton County Wells Site	fZI-MW&

iDate C//?/g.2.	1 Sample Number: gt - MIAI g-W-/T-

fTime:	I I i Q	|Note any QA/Q.C samples:		

ANALYSES

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)

-5

40*nL- voft

frbl

VOC/s

i

ifonu [ladies

rurr-es

Chloride^

















1

Hach Ampule

None

Ferrous Iron

AM	

OBSERVATIONS/COMMENTS:

WEATHER:

0 londy. Uo'F,


-------
y Di&tlA&S iS&Vtt, wj OWiVJLH fWlt ?} g^tL^r. -ORC/.

- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

IPROJECT NAME: Newton County Welis Site

WELL PURGE DATA

lUf/TCT

Sampler

2^L.

i^Ar./o^

iilSL

Well Construction

Total Volume Purged (gallons)

*+!' yvc, -Fiu^T

_Z

Well Measurements (feet below top of casing)

38.2S

Pump is set at (feet below top of casing)

HI

Static Water Level

Total Depth

125_

Well Measurement Technique

Well Purge Equipment

pi.entry j9Uyy]f

Screen Length (feet)

FIELD PARAMETERS

2-0

Other (list here)

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP (mV)

Flow (mL/min)

Notes

iM-O

*R. ^

rta.H

362.©

«f.BS



7.^1 .-T-

t+rsn



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M.*9

l+n1-. 4







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ChCcJL- 'tfJrtiv\ i.ei



3
-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

[PROJECT NAME: Newton County Wells Site

WELL PURGE DATA

Date/Time A /)£?!/? .7^

Well Construction

	



Total Volume Purged (gallons)

	

Well Measurements (feet below to

3 of casingf

Pump is set at (feet below top of casing)

	

Static Water Level

•

Well MeasurementTechnique

		

Screen Length (feet)

		

Other (list here)



FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

PH

ORP(mV)

Flow (mL/min)

Notes





[ft. 1

31^. q_

°l .-7«

inn

7^.ft

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SAMPLE COLLECTION DATA

Pate: .K / 1 S
|Time:



f \ io 'vlfsN

|Sample Number:

Note any QA/QC sampte:

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)



*rU wU_ \Jdl^,

WIM

\/0 k

I

¦?£Ci m>L pla^+iY.

f\\d.\/V fl,

~f Iv-iCVft

















1

Hach Ampule

None

Ferrous Iron

wM

OBSERVATIONS/COMMENTS:

WEATHER:

%Qj\r,


-------
- GROUNDWATER & SPRING SURFACE WATER SAMPLING LOG

IPROJECT NUMBER: 1690004605

(PROJECT NAME: Newton County Wells Site

WELL PURGE DATA

Date/Time F?l\Oi [?~ 1 laH-K

Well Construction

c		



Total Volume Purged (gallons)

..	

Well Measurements (feet below top of casing)

Pump is set at (feet below top of casing)

_

|Static Water Levef

		*

Weil Measurement Technique

-—

|Total Depth



Well Purge Equipment

—

|Screen Length (feet)



Other (list here) 1

FIELD PARAMETERS

Purge Time (24 hour)

Depth to Water (feet)

Temp °C

Spec Cond (uS/cm)

DO (mg/L)

pH

ORP (mV)

Flow (mL/min)

Notes

llosn

—	

17.*



l i

7, (pi



	

















































































































































































































































































SAMPLE COLLECTION DATA

k?m ?<7<

# of Containers

Size/Type

Preservative

Analytical Parameter(s)

Result
(mg/L)



i>f, |.« v/QA.

Mr I'J

\//>A

i

9 r>Q ^ r.

"|v lrvy\ i,





\













1

Hach Ampule

None

Ferrous Iron

klM

WEATHER:	.1	*

^ cJ~j \ )	cWu-Ay


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Validated Analytical Laboratory Data Reports (May 2022)

December 2022


-------
Setting the Standards for Innovative Environmental Solutions

July 22, 2022

Mr. Doug Burge, R.G., P.G.

Senior Manager
RamboII

1807 Park 270 Drive, Suite 450
Saint Louis, MO 63146

Dear Mr. Burge:

Enclosed is the quality assurance review of the analytical data for 44 aqueous samples
(including quality control samples) collected on May 17, 18, and 19, 2022, at the Fischers
Aktien-Gesellschaft Bearings Corporation Newton County Wells Site. Based on this quality
assurance review, several results were qualified as estimated due to holding-time exceedance,
a high laboratory control sample recovery, low matrix spike/matrix spike duplicate recoveries,
and quantitation between the sample-specific method detection limit and reporting limit.

If you have any questions or comments, please do not hesitate to call.

Sincerely,	Sincerely,

7F). SmmAm

C, luv iA&dcal



0

Erin E. Rodgers

Principal Chemist

Caroline M. Rowshan

Senior Quality Assurance Chemist/

Project Manager

CMR/EER:ks

Enc.

Copy to: Caroline Chavers - RamboII
Ian McQuaig - RamboII

1140 Valley Forge Road P.O.BoxSlO Valley Forge, PA 19482 Teii810.935.557? Fax: 610,935.5583 Web: www.envstd.com


-------
Setting the Standards for Innovative Environmental Solutions

QUALITY ASSURANCE REVIEW
OF THE AQUEOUS SAMPLES COLLECTED AT THE
FISCHERS AKTIEN-GESELLSCHAFT BEARINGS CORPORATION
NEWTON COUNTY WELLS SITE
ON MAY 17, 18, AND 19, 2022

July 22, 2022

Prepared for:

RAMBOLL

1807 Park 270 Drive, Suite 320
Saint Louis, MO 63146

Prepared by:

ENVIRONMENTAL STANDARDS, INC.

1140 Valley Forge Road
P.O. Box 810
Valley Forge, PA 19482-0810

© 2022 Environmental Standards, Inc. - All Rights Reserved

1140 Valley Forge Road P.O.Box810 Valley Forge,PA 19482 610.935.5S77 I >610.935,5583 VU. www.envstd.com


-------
TABLE OF CONTENTS

Introduction

Section 1 Quality Assurance Review

A.	Organic Data

B.	Conclusions

Section 2 Analytical Results

A.	Pace Project Number 60400603

B.	Pace Project Number 60400849

C.	Pace Project Number 60400877

Section 3 Organic Data Support Documentation

A.	Pace Project Number 60400603

B.	Pace Project Number 60400849

C.	Pace Project Number 60400877

Section 4 Project Chain-of-Custody Records

Section 5 Project Correspondence


-------
Introduction

This quality assurance (QA) review is based upon an examination of data generated from the
analyses of the 44 groundwater samples (including quality control [QC] samples) that were
collected on May 17, 18, and 19, 2022, by Ramboll in association with the Fischers
Aktien-Gesellschaft (FAG) Bearings Corporation Newton County Wells Site. The analytical data
for the aqueous samples in Pace Analytical Services, LLC (Pace) Project Numbers 60400603,
60400849, and 60400877 underwent Stage 2A validation (batch QC summary form review only)
as indicated on Table 1.

This Limited review has been performed with guidance from the "National Functional Guidelines
for Organic Data Review" (US EPA, October 1999). This document was used to aid the data
reviewer in the interpretation of the QC analysis results and in the overall evaluation of the
sample data deliverables.

The reported analytical results are presented in Section 2. Data were examined to determine
the usability of the analytical results and the compliance relative to the requirements specified in
the published analytical method and Appendix A Addendum to September 2001 Remedial
Investigation Sampling and Analysis Plan and June 2007 Remedial Action Work Plan
(December 2015).

Data not qualified in this report should be considered valid based on the QC criteria that have
been reviewed. Details of this QA review are presented in Section 1 of this report. This report
was prepared to provide a review of the laboratory analyses and reported analytical results.
QA reviews of laboratory-generated data routinely identify various problems associated with
analytical measurements, even from the most experienced and capable laboratories.


-------
TABLE 1

SAMPLES INCLUDED IN THIS QUALITY ASSURANCE REVIEW

Ramboll Environ
Sample Identification

Laboratory

Sample
Identification

Pace
Project
Number

Matrix

Date
Sample
Collected

Parameter
Examined

RI-MW8-W-17

60400603001

60400603

Aq

5/17/22

V

RI-MW2-W-17

60400603002

60400603

Aq

5/17/22

V

RI-MW2-W-17MS
(Matrix Spike)

3144001

60400603

Aq

5/17/22

V

RI-MW2-W-17MSD
(Matrix Spike Duplicate)

3144002

60400603

Aq

5/17/22

V

RI-MW5-W-17

60400603003

60400603

Aq

5/17/22

V

RI-MW7-W-17

60400603004

60400603

Aq

5/17/22

V

RI-MW6-W-17

60400603005

60400603

Aq

5/17/22

V

FAG-62-W-17

60400603006

60400603

Aq

5/17/22

V

FAG-43-W-17

60400603007

60400603

Aq

5/17/22

V

RI-MW1 -W-17

60400603008

60400603

Aq

5/17/22

V

FAG-56-W-17

60400603009

60400603

Aq

5/17/22

V

FAG-33-W-17

60400603010

60400603

Aq

5/17/22

V

TB-01-051722
(Trip Blank)

60400603011

60400603

Aq

5/17/22

V

FAG-47-W-17

60400849001

60400849

Aq

5/18/22

V

FAG-46-W-17

60400849002

60400849

Aq

5/18/22

V

FAG-05-W-17

60400849003

60400849

Aq

5/18/22

V

FD-LIST B-05182022
(Field Duplicate of FAG-05-W-17)

60400849004

60400849

Aq

5/18/22

V

FAG-11-W-17

60400849005

60400849

Aq

5/18/22

V

FAG-35-W-17

60400849006

60400849

Aq

5/18/22

V

FD-LIST A-05182022
(Field Duplicate of FAG-35-W-17)

60400849007

60400849

Aq

5/18/22

V

R1-MW9-W-17

60400849008

60400849

Aq

5/18/22

V

FAG-34-W-17

60400849009

60400849

Aq

5/18/22

V

FAG-36-W-17

60400849010

60400849

Aq

5/18/22

V

FAG-73-W-17

60400849011

60400849

Aq

5/18/22

V

FAG-32-W-17

60400849012

60400849

Aq

5/18/22

V

FAG-AW4-W-17

60400849013

60400849

Aq

5/18/22

V


-------
TABLE 1 (Cont.)



Laboratory

Pace



Date



Ramboll Environ

Sample

Project



Sample

Parameter

Sample Identification

Identification

Number

Matrix

Collected

Examined

FAG-AW4-W-17MS

3144758

60400849

Aq

5/18/22

V

(Matrix Spike)







FAG-AW4-W-17MSD

3144759

60400849

Aq

5/18/22

V

(Matrix Spike Duplicate)









TB-01-051822

60400849014

60400849

Aq

5/18/22

V

(Trip Blank)









TB-02-051822

60400849015

60400849

Aq

5/18/22

V

(Trip Blank)









FAG-50-W-17

60400877001

60400877

Aq

5/19/22

V

FAG-31-W-17

60400877002

60400877

Aq

5/19/22

V

FAG-85-W-17

60400877003

60400877

Aq

5/19/22

V

FAG-85-W-17MS

3147266

60400877

Aq

5/19/22

V

(Matrix Spike)









FAG-85-W-17MSD

3147267

60400877

Aq

5/19/22

V

(Matrix Spike Duplicate)









FAG-22-W-17

60400877004

60400877

Aq

5/19/22

V

FAG-88-W-17

60400877005

60400877

Aq

5/19/22

V

FAG-89-W-17

60400877006

60400877

Aq

5/19/22

V

SW-01-W-17

60400877007

60400877

Aq

5/19/22

V

RW-341A-W-17

60400877008

60400877

Aq

5/19/22

V

FAG-74-W-17

60400877009

60400877

Aq

5/19/22

V

EB-01

60400877010

60400877

Aq

5/19/22

V

(Equipment Blank)









TB-01-05192022

60400877011

60400877

Aq

5/19/22

V

(Trip Blank)









TB-02-05192022

60400877012

60400877

Aq

5/19/22

V

(Trip Blank)









NOTE:

V - Volatile Organic Compounds by SW-846 Method 8260. (44 analyses)


-------
Section 1 Quality Assurance Review

A. Organic Data

The organic analyses of 44 aqueous samples (including QC samples) were performed by Pace
in Lenexa, Kansas. All samples were analyzed for volatile organic compounds (VOCs) by
SW-846 Method 8260 and were validated as indicated on Table 1. Reduced data package
deliverables, which allowed for a Limited, third-party validation, were provided.

The findings offered in this report are based on a review of the holding times, condition of
samples upon laboratory receipt, laboratory and field blank results, field duplicate precision,
laboratory control sample (LCS) recoveries, matrix spike/matrix spike duplicate (MS/MSD)
recoveries and precision, and surrogate recoveries.

Issues are typically presented in two categories - reporting issues and procedural issues.
Reporting issues are data deliverable issues that can easily be corrected and that may or may
not impact the usability of the reported results. Procedural issues are issues that cannot be
corrected and address method compliance issues; these issues may or may not impact the
usability of the reported results. No reporting issues were identified in this QA review, and one
procedural issue was identified in this QA review. The data reviewer has included copies of QC
forms and other documentation needed to support any changes made to the data package in
the Organic Data Support Documentation (Section 3) of this report.

Reporting Issues

No reporting issues were observed for this QA review.

Procedural Issue

In Pace Project Number 60400849, sample FAG-34-W-17 was unpreserved (pH > 2)
and was analyzed beyond the 7-day holding-time requirement from sample collection to
analysis as specified in SW-846 Chapter 4. Qualification of data due to this issue is
addressed in the subsequent Organic Data Qualifiers section (see Project
Correspondence [Section 5]).

Comments

1.	For Pace Project Number 60400603, the Chain-of-Custody (COC) Record sample
RI-MW-6-W-17 was logged in by the laboratory with the sample identification (ID)
RI-MW6-W-17. Based upon previous sampling rounds, RI-MW6-W-17 is the correct
sample ID. Environmental Standards has utilized RI-MW6-W-17 as the sample ID in this
report.

2.	The laboratory did not sign and date the "Accepted By" field on the second page of the
COC Record.


-------
Page 2

3. The following field duplicate pairs were submitted and analyzed for VOCs with these

data sets. Acceptable precision and sample representativeness (i.e., the relative percent
difference between results was < 20% when both results were > 5* the reporting limit
[RL], or the difference between the results was < the RL when at least one result was
< 5* the RL) were demonstrated between the reported results in the duplicate samples.
Complete comparisons of the field duplicate positive results are included in Section 3.

Pace Project Number	Parent Sample	Field Duplicate Sample

60400849	FAG-05-W-17	FD-LIST B-05182022

60400849	FAG-35-W-17	FD-LIST A-05192022

4. The laboratory analyzed the samples on the table below at initial dilutions for the

analyses indicated. The method detection limits (MDLs) and RLs for all target analytes
were raised based on the dilution performed, and the "not-detected" results were
reported at elevated detection limits.

Pace Project Number
60400849

60400849
60400877
60400877
60400877

Sample(s)

FAG-35-W-17,

FD-LIST A-05182022, and
FAG-34-W-17
FAG-36-W-17 and FAG-AW4-W-17

FAG-50-W-17

FAG-31-W-17 and FAG-22-W-17

FAG-85-W-17 and FAG-74-W-17

Dilution Factor
5-fold

10-fold
25-fold
10-fold
5-fold

5. The samples in the data packages provided for review were collectively analyzed for
VOCs, gases (specifically ethane, ethene, and methane), total iron, and anions
(specifically, chloride, sulfate, and nitrate). Per Ramboll's previous request, data
validation was performed on the VOC data only.

With regard to data usability, the principal areas of concern are holding-time exceedance, a high
LCS recovery, low MS/MSD recoveries, and quantitation between the sample-specific MDL and
RL. Based on a review of the data provided, the following organic data qualifiers are offered.
The following organic data usability issues represent an interpretation of the QC results
obtained for the project samples. Accordingly, the following data usability issues should not
necessarily be construed as an indication of laboratory performance.

\\esi-file-6\working\ramboll environ\2022 newton county wells dv\018045\final\ramboll environ_fag_ annual 2022 gw report_final.docx


-------
Page 3

Organic Data Qualifiers

The MDLs and RLs for benzene; bromobenzene; n-butylbenzene; sec-butylbenzene;
te/f-butylbenzene; chlorobenzene; 2-chlorotoluene; 4-chlorotoluene;

1,2-dichlorobenzene; 1,3-dichlorobenzene; 1,4-dichlorobenzene; ethylbenzene;
isopropylbenzene (cumene); p-isopropyltoluene; naphthalene; n-propylbenzene; toluene;
1,2,3-trichlorobenzene; 1,2,4-trichlorobenzene; 1,2,4-trimethylbenzene;
1,3,5-trimethylbenzene; and xylene (total) in Pace Project Number 60400849 sample
FAG-34-W-17 may be higher than reported, and the "not-detected" results have been
flagged "UJ" on the Analytical Results forms. The sample was analyzed beyond the 7-
day holding-time requirement for sample collection to analysis for unpreserved VOC
samples (see Procedural Issue).

The positive results reported for methylene chloride in Pace Project Number 60400877
samples FAG-50-W-17 and FAG-31-W-17 should be considered estimated and have
been flagged "J" on the Analytical Results forms. A high LCS recovery (> the laboratory
lower acceptance limit) was observed for this compound in the associated LCS analysis.

The M DLs and RLs for 1,1,1,2-tetrachloroethane; 1,1,1 -trichloroethane;
1,1,2,2-tetrachloroethane; 1,1,2-trichloroethane; 1,2,3-trichlorobenzene;
1,2-dibromo-3-chloropropane; 1,2-dibromoethane (EDB); 1,2-dichlorobenzene;
1,2-dichloropropane; 1,3-dichlorobenzene; 1,3-dichloropropane; 4-chlorotoluene;
bromobenzene; bromochloromethane; bromodichloromethane; carbon tetrachloride;
chlorobenzene; chloroform; dibromochloromethane; dibromomethane; and methylene
chloride in Pace Project Number 60400603 sample RI-MW2-W-17 may be higher than
reported, and the "not-detected" results have been flagged "UJ" on the Analytical Results
forms. Low recoveries (< the laboratory lower acceptance limit) were observed for these
compounds in the associated MS/MSD analyses.

The MDL and RL for 1,2-dibromo-3-chloropropane in Pace Project Number 60400849
sample FAG-AW4-W-17 may be higher than reported, and the "not-detected" result has
been flagged "UJ" on the Analytical Results form. A low recovery (< the laboratory lower
acceptance limit) was observed for this compound in the associated MS analysis.

All results reported at concentrations less than the sample-specific RL (adjusted for
dilution factors and sample volume) and above the MDL should be considered estimated
and have been flagged "J" on the Analytical Results forms.

\\esi-file-6\working\ramboll environ\2022 newton county wells dv\018045\final\ramboll environ_fag_ annual 2022 gw report_final.docx


-------
Page 4

B. Conclusions

This QA review has identified several aspects of the data that required qualification. The
analytical data should be considered acceptable for use unless otherwise indicated in the QA
review. In order to use any of the data, the data user should understand the qualifications and
limitations specified in this QA review. The Analytical Results are presented in Section 2. The
Organic Data Support Documentation is presented in Section 3. The Project Chain-of-Custody
Records are presented in Section 4, and Project Correspondence is provided in Section 5.

Report Prepared by,	Report Reviewed by,

Kelsey M. Heck
Quality Assurance Chemist

Caroline M. Rowshan
Senior Quality Assurance Chen

Project Manager

Report Reviewed and Approved by,

Erin E. Rodgers
Principal Chemist

ENVIRONMENTAL STANDARDS, INC.
1140 Valley Forge Road
P.O. Box 810

Valley Forge, PA 19482-0810
(610) 935-5577

Date: 7/22/22

\\esi-file-6\working\ramboll environ\2022 newton county wells dv\018045\finai\ramboii environ_fag_ annual 2022 gw report_final.docx


-------
ORGANIC DATA QUALIFIERS

U This compound was not detected at or above the associated reporting limit.

U* This compound should be considered "not-detected" because it was detected in an
associated blank at a similar level.

J Quantitation is approximate due to limitations identified during the quality assurance
review (data validation).

UR Unusable practical quantitation limit; compound may or may not be present in this
sample.

R Unusable positive result; compound may or may not be present in this sample.

UJ This compound was not detected, but the practical quantitation limit is probably higher
due to a low bias identified during the quality assurance review.

N This result should be considered a tentative qualitative identification.


-------
SECTION 2
ANALYTICAL RESULTS


-------
A. PACE PROJECT NUMBER 60400603


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW8-W-17 + .

Lab ID:

60400603001

Collected:

05/17/22 11:10

Received:

05/18/22 08:50 Matrix: Water

~





Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City









Acetone

W ND

ug/L

10.0

2.5 1



05/25/22

16:31

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



05/25/22

16:31

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



05/25/22

16:31

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



05/25/22

16:31

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



05/25/22

16:31

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



05/25/22

16:31

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



05/25/22

16:31

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



05/25/22

16:31

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



05/25/22

16:31

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



05/25/22

16:31

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

16:31

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



05/25/22

16:31

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



05/25/22

16:31

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



05/25/22

16:31

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



05/25/22

16:31

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



05/25/22

16:31

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



05/25/22

16:31

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



05/25/22

16:31

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



05/25/22

16:31

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



05/25/22

16:31

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



05/25/22

16:31

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



05/25/22

16:31

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



05/25/22

16:31

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



05/25/22

16:31

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/25/22

16:31

541 -73-1

1,4-Dichlorobenzene

0.14J

ug/L

1.0

0.13 1



05/25/22

16:31

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



05/25/22

16:31

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



05/25/22

16:31

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



05/25/22

16:31

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



05/25/22

16:31

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



05/25/22

16:31

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



05/25/22

16:31

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



05/25/22

16:31

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



05/25/22

16:31

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



05/25/22

16:31

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



05/25/22

16:31

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



05/25/22

16:31

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



05/25/22

16:31

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



05/25/22

16:31

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

16:31

100-41-4

Hexachloro-1,3-butadiene

0.48J

ug/L

1.0

0.42 1



05/25/22

16:31

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



05/25/22

16:31

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



05/25/22

16:31

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



05/25/22

16:31

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



05/25/22

16:31

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 5 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW8-W-17 +

Lab ID:

60400603001

Collected:

05/17/22 11:10

Received:

05/18/22 08:50 Matrix: Water



~





Report













Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

Kansas City













4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1



05/25/22

16:31

108-10-1



Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



05/25/22

16:31

1634-04-4



Naphthalene

0.87J

ug/L

10.0

0.82 1



05/25/22

16:31

91-20-3



n-Propylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

16:31

103-65-1



Styrene

ND

ug/L

1.0

0.12 1



05/25/22

16:31

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



05/25/22

16:31

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



05/25/22

16:31

79-34-5



Tetrachloroethene

ND

ug/L

1.0

0.33 1



05/25/22

16:31

127-18-4



Toluene

ND

ug/L

1.0

0.25 1



05/25/22

16:31

108-88-3



1,2,3-Trichlorobenzene

1.4

ug/L

1.0

0.93 1



05/25/22

16:31

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



05/25/22

16:31

120-82-1



1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



05/25/22

16:31

71-55-6



1,1,2-Trichloroethane

0.28J

ug/L

1.0

0.14 1



05/25/22

16:31

79-00-5



Trichloroethene

1.6

ug/L

1.0

0.21 1



05/25/22

16:31

79-01-6



Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



05/25/22

16:31

75-69-4



1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



05/25/22

16:31

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



05/25/22

16:31

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



05/25/22

16:31

108-67-8



Vinyl chloride

ND

ug/L

1.0

0.17 1



05/25/22

16:31

75-01-4



Xylene (Total)

ND

ug/L

3.0

0.28 1



05/25/22

16:31

1330-20-7



Surrogates

4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichlorobenzene-d4 (S)
Preservation pH

300.0 IC Anions 28 Days

Chloride

102
101
99
1.0.

%
%
%

80-120
80-120
80-120
0.10

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

9.0 mg/L	1.0

05/25/22 16:31
05/25/22 16:31
05/25/22 16:31
05/25/22 16:31

460-00-4

2037-26-5

2199-69-1

0.53

05/27/22 11:54 16887-00-6

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 6 of 44


-------
\ce Analytical9

www.pacdiln.cani

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW2-W-17	-''Lab ID: 60400603002 Collected: 05/17/22 12:52 Received: 05/18/22 08:50 Matrix: Water

Parameters

Results

Units





Report
Limit

MDL DF

Prepared

Analyzed

CAS No.

C

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services

Kansas City











Acetone

^ ND

ug/L





10.0

2.5 1



05/25/22

16:47

67-64-1



Benzene

ND

ug/L





1.0

0.14 1



05/25/22

16:47

71-43-2



Bromobenzene

ND

ug/L

UJ

1.0

0.088 1



05/25/22

16:47

108-86-1

M1

Bromochloromethane

ND

ug/L





1.0

0.20 1



05/25/22

16:47

74-97-5

M1

Bromodichloromethane

ND

ug/L



f

1.0

0.16 1



05/25/22

16:47

75-27-4

M1

Bromoform

ND

ug/L





1.0

0.68 1



05/25/22

16:47

75-25-2



Bromomethane

ND

ug/L





5.0

0.46 1



05/25/22

16:47

74-83-9



2-Butanone (MEK)

ND

ug/L





10.0

0.98 1



05/25/22

16:47

78-93-3



n-Butylbenzene

ND

ug/L





1.0

0.15 1



05/25/22

16:47

104-51-8



sec-Butylbenzene

ND

ug/L





1.0

0.11 1



05/25/22

16:47

135-98-8



tert-Butylbenzene

ND

ug/L





1.0

0.12 1



05/25/22

16:47

98-06-6



Carbon disulfide

ND

ug/L





5.0

0.98 1



05/25/22

16:47

75-15-0



Carbon tetrachloride

ND

ug/L

UJ

1.0

0.17 1



05/25/22

16:47

56-23-5

M1

Chlorobenzene

ND

ug/L

UJ

1.0

0.089 1



05/25/22

16:47

108-90-7

M1

Chloroethane

0.75J

ug/L





1.0

0.37 1



05/25/22

16:47

75-00-3



Chloroform

ND

ug/L

UJ

1.0

0.22 1



05/25/22

16:47

67-66-3

M1

Chloromethane

ND

ug/L





1.0

0.28 1



05/25/22

16:47

74-87-3



2-Chlorotoluene

ND

ug/L





1.0

0.11 1



05/25/22

16:47

95-49-8



4-Chlorotoluene

ND

ug/L

UJ

1.0

0.15 1



05/25/22

16:47

106-43-4

M1

1,2-Dibromo-3-chloropropane

ND

ug/L





2.5

0.78 1



05/25/22

16:47

96-12-8

M1

Dibromochloromethane

ND

ug/L





1.0

0.30 1



05/25/22

16:47

124-48-1

M1

1,2-Dibromoethane (EDB)

ND

ug/L





1.0

0.20 1



05/25/22

16:47

106-93-4

M1

Dibromomethane

ND

ug/L





1.0

0.11 1



05/25/22

16:47

74-95-3

M1

1,2-Dichlorobenzene

ND

ug/L





1.0

0.12 1



05/25/22

16:47

95-50-1

M1

1,3-Dichlorobenzene

ND

ug/L

\

(

1.0

0.13 1



05/25/22

16:47

541 -73-1

M1

1,4-Dichlorobenzene

ND

ug/L





1.0

0.13 1



05/25/22

16:47

106-46-7



Dichlorodifluoromethane

ND

ug/L





1.0

0.20 1



05/25/22

16:47

75-71-8



1,1-Dichloroethane

ND

ug/L





1.0

0.12 1



05/25/22

16:47

75-34-3



1,2-Dichloroethane

ND

ug/L





1.0

0.21 1



05/25/22

16:47

107-06-2



1,2-Dichloroethene (Total)

ND

ug/L





1.0

0.22 1



05/25/22

16:47

540-59-0



1,1-Dichloroethene

ND

ug/L





1.0

0.22 1



05/25/22

16:47

75-35-4



cis-1,2-Dichloroethene

ND

ug/L





1.0

0.13 1



05/25/22

16:47

156-59-2



trans-1,2-Dichloroethene

ND

ug/L





1.0

0.10 1



05/25/22

16:47

156-60-5



1,2-Dichloropropane

ND

ug/L

UJ

1.0

0.14 1



05/25/22

16:47

78-87-5

M1

1,3-Dichloropropane

ND

ug/L

UJ

1.0

0.10 1



05/25/22

16:47

142-28-9

M1

2,2-Dichloropropane

ND

ug/L





1.0

0.16 1



05/25/22

16:47

594-20-7



1,1-Dichloropropene

ND

ug/L





1.0

0.14 1



05/25/22

16:47

563-58-6



cis-1,3-Dichloropropene

ND

ug/L





1.0

0.078 1



05/25/22

16:47

10061 -01 -5



trans-1,3-Dichloropropene

ND

ug/L





1.0

0.18 1



05/25/22

16:47

10061 -02-6



Ethylbenzene

ND

ug/L





1.0

0.12 1



05/25/22

16:47

100-41-4



Hexachloro-1,3-butadiene

ND

ug/L





1.0

0.42 1



05/25/22

16:47

87-68-3



2-Hexanone

ND

ug/L





10.0

1.1 1



05/25/22

16:47

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L





1.0

0.097 1



05/25/22

16:47

98-82-8



p-lsopropyltoluene

ND

ug/L





1.0

0.13 1



05/25/22

16:47

99-87-6



Methylene Chloride

ND

ug/L

UJ

1.0

0.39 1



05/25/22

16:47

75-09-2

M1

ANALYTICAL RESULTS

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 7 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW2-W-17

Parameters

Lab ID: 60400603002 Collected: 05/17/22 12:52 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)

ND

ug/L



10.0

0.74 1

05/25/22

16:47

108-10-1



Methyl-tert-butyl ether

ND

ug/L



1.0

0.13 1

05/25/22

16:47

1634-04-4



Naphthalene

ND

ug/L



10.0

0.82 1

05/25/22

16:47

91-20-3



n-Propylbenzene

ND

ug/L



1.0

0.12 1

05/25/22

16:47

103-65-1



Styrene

ND

ug/L



1.0

0.12 1

05/25/22

16:47

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

UJ

1.0

0.084 1

05/25/22

16:47

630-20-6

M1

1,1,2,2-Tetrachloroethane

ND

ug/L

UJ

1.0

0.15 1

05/25/22

16:47

79-34-5

M1

Tetrachloroethene

ND

ug/L



1.0

0.33 1

05/25/22

16:47

127-18-4



Toluene

ND

ug/L



1.0

0.25 1

05/25/22

16:47

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

UJ

1.0

0.93 1

05/25/22

16:47

87-61-6

M1

1,2,4-Trichlorobenzene

ND

ug/L



1.0

0.73 1

05/25/22

16:47

120-82-1



1,1,1-Trichloroethane

ND

ug/L

UJ

1.0

0.11 1

05/25/22

16:47

71-55-6

M1

1,1,2-Trichloroethane

ND

ug/L

UJ

1.0

0.14 1

05/25/22

16:47

79-00-5

M1

Trichloroethene

ND

ug/L



1.0

0.21 1

05/25/22

16:47

79-01-6



Trichlorofluoromethane

ND

ug/L



1.0

0.16 1

05/25/22

16:47

75-69-4



1,2,3-Trichloropropane

ND

ug/L



2.5

0.41 1

05/25/22

16:47

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L



1.0

0.32 1

05/25/22

16:47

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L



1.0

0.090 1

05/25/22

16:47

108-67-8



Vinyl chloride

ND

ug/L



1.0

0.17 1

05/25/22

16:47

75-01-4



Xylene (Total)

ND

ug/L



3.0

0.28 1

05/25/22

16:47

1330-20-7



Surrogates



















4-Bromofluorobenzene (S)

100

%



80-120

1

05/25/22

16:47

460-00-4



Toluene-d8 (S)

98

%



80-120

1

05/25/22

16:47

2037-26-5



1,2-Dichlorobenzene-d4 (S)

99

%



80-120

1

05/25/22

16:47

2199-69-1



Preservation pH

1.0

—



0.10

1

05/25/22

16:47





300.0 IC Anions 28 Days

Analytical Method:

EPA 300.0













Pace Analytical Services -

Kansas City











Chloride

23.3

mg/L



20.0

10.5 20

05/26/22

16:24

16887-00-6

M1

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 8 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW5-W-17 +

^ Lab ID:

60400603003

Collected:

05/17/22 13:10

Received:

05/18/22 08:50 Matrix: Water

~





Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City





*





Acetone

^ ND

ug/L

10.0

2.5 1



05/25/22

17:35

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



05/25/22

17:35

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



05/25/22

17:35

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



05/25/22

17:35

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



05/25/22

17:35

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



05/25/22

17:35

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



05/25/22

17:35

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



05/25/22

17:35

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



05/25/22

17:35

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



05/25/22

17:35

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

17:35

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



05/25/22

17:35

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



05/25/22

17:35

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



05/25/22

17:35

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



05/25/22

17:35

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



05/25/22

17:35

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



05/25/22

17:35

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



05/25/22

17:35

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



05/25/22

17:35

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



05/25/22

17:35

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



05/25/22

17:35

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



05/25/22

17:35

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



05/25/22

17:35

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



05/25/22

17:35

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/25/22

17:35

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/25/22

17:35

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



05/25/22

17:35

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



05/25/22

17:35

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



05/25/22

17:35

107-06-2

1,2-Dichloroethene (Total)

0.92J

ug/L

1.0

0.22 1



05/25/22

17:35

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



05/25/22

17:35

75-35-4

cis-1,2-Dichloroethene

0.92J

ug/L

1.0

0.13 1



05/25/22

17:35

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



05/25/22

17:35

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



05/25/22

17:35

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



05/25/22

17:35

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



05/25/22

17:35

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



05/25/22

17:35

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



05/25/22

17:35

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



05/25/22

17:35

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

17:35

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



05/25/22

17:35

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



05/25/22

17:35

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



05/25/22

17:35

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



05/25/22

17:35

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



05/25/22

17:35

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 9 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW5-W-17 +

Lab ID:

60400603003

Collected:

05/17/22 13:10

Received:

05/18/22 08:50 Matrix: Water



~





Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





y





4-Methyl-2-pentanone (MIBK)

sf* ND

ug/L

10.0

0.74 1



05/25/22 17:35

108-10-1



Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



05/25/22 17:35

1634-04-4



Naphthalene

ND

ug/L

10.0

0.82 1



05/25/22 17:35

91-20-3



n-Propylbenzene

ND

ug/L

1.0

0.12 1



05/25/22 17:35

103-65-1



Styrene

ND

ug/L

1.0

0.12 1



05/25/22 17:35

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



05/25/22 17:35

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



05/25/22 17:35

79-34-5



Tetrachloroethene

ND

ug/L

1.0

0.33 1



05/25/22 17:35

127-18-4



Toluene

ND

ug/L

1.0

0.25 1



05/25/22 17:35

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



05/25/22 17:35

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



05/25/22 17:35

120-82-1



1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



05/25/22 17:35

71-55-6



1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



05/25/22 17:35

79-00-5



Trichloroethene

15.6

ug/L

1.0

0.21 1



05/25/22 17:35

79-01-6



Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



05/25/22 17:35

75-69-4



1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



05/25/22 17:35

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



05/25/22 17:35

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



05/25/22 17:35

108-67-8



Vinyl chloride

ND

ug/L

1.0

0.17 1



05/25/22 17:35

75-01-4



Xylene (Total)

ND

ug/L

3.0

0.28 1



05/25/22 17:35

1330-20-7



Surrogates

4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichlorobenzene-d4 (S)
Preservation pH

300.0 IC Anions 28 Days

Chloride

102
99
98
1.0

%
%
%

80-120
80-120
80-120
0.10

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

20.5 mg/L	20.0

05/25/22 17:35
05/25/22 17:35
05/25/22 17:35
05/25/22 17:35

460-00-4

2037-26-5

2199-69-1

10.5 20

05/26/22 17:19 16887-00-6

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 10 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW7-W-17 +

Lab ID:

60400603004

Collected:

05/17/22 14:30

Received: 05/18/22 08:50 Matrix: Water

~





Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City







Acetone

ND

ug/L

10.0

2.5 1

05/25/22 17:51

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/25/22 17:51

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/25/22 17:51

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/25/22 17:51

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/25/22 17:51

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/25/22 17:51

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/25/22 17:51

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/25/22 17:51

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/25/22 17:51

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/25/22 17:51

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 17:51

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/25/22 17:51

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/25/22 17:51

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/25/22 17:51

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/25/22 17:51

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/25/22 17:51

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/25/22 17:51

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/25/22 17:51

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/25/22 17:51

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/25/22 17:51

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/25/22 17:51

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/25/22 17:51

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/25/22 17:51

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/25/22 17:51

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 17:51

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 17:51

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/25/22 17:51

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/25/22 17:51

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/25/22 17:51

107-06-2

1,2-Dichloroethene (Total)

3.2

ug/L

1.0

0.22 1

05/25/22 17:51

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/25/22 17:51

75-35-4

cis-1,2-Dichloroethene

3.2

ug/L

1.0

0.13 1

05/25/22 17:51

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/25/22 17:51

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/25/22 17:51

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/25/22 17:51

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/25/22 17:51

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/25/22 17:51

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/25/22 17:51

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/25/22 17:51

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 17:51

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/25/22 17:51

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/25/22 17:51

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/25/22 17:51

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/25/22 17:51

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/25/22 17:51

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 11 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW7-W-17

Parameters

Lab ID: 60400603004 Collected: 05/17/22 14:30 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

05/25/22 17:51

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/25/22 17:51

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/25/22 17:51

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/25/22 17:51

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/25/22 17:51

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/25/22 17:51

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/25/22 17:51

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/25/22 17:51

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/25/22 17:51

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/25/22 17:51

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/25/22 17:51

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/25/22 17:51

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/25/22 17:51

79-00-5

Trichloroethene



21.7

ug/L

1.0

0.21 1

05/25/22 17:51

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/25/22 17:51

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/25/22 17:51

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/25/22 17:51

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/25/22 17:51

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/25/22 17:51

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/25/22 17:51

1330-20-7

Surrogates















4-Bromofluorobenzene (S)



102

%

80-120

1

05/25/22 17:51

460-00-4

Toluene-d8 (S)



100

%

80-120

1

05/25/22 17:51

2037-26-5

1,2-Dichlorobenzene-d4 (S)



99 z'

%

80-120

1

05/25/22 17:51

2199-69-1

Preservation pH



1.0



0.10

1

05/25/22 17:51



300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

5.9 mg/L	1.0

0.53

05/27/22 12:21 16887-00-6 M1

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

Date: 06/02/2022 03:03 PM	without the written consent of Pace Analytical Services, LLC.	Page 12 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW6-W-17 +

^ Lab ID:

60400603005

Collected:

05/17/22 15:50

Received:

05/18/22 08:50

Matrix: Water

~





Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





/





Acetone

if ND

ug/L

10.0

2.5 1



05/25/22 18

:07

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



05/25/22 18

:07

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



05/25/22 18

:07

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



05/25/22 18

:07

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



05/25/22 18

:07

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



05/25/22 18

:07

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



05/25/22 18

:07

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



05/25/22 18

:07

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



05/25/22 18

:07

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



05/25/22 18

:07

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



05/25/22 18

:07

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



05/25/22 18

:07

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



05/25/22 18

:07

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



05/25/22 18

:07

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



05/25/22 18

:07

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



05/25/22 18

:07

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



05/25/22 18

:07

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



05/25/22 18

:07

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



05/25/22 18

:07

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



05/25/22 18

:07

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



05/25/22 18

:07

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



05/25/22 18

:07

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



05/25/22 18

:07

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



05/25/22 18

:07

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/25/22 18

:07

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/25/22 18

:07

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



05/25/22 18

:07

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



05/25/22 18

:07

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



05/25/22 18

:07

107-06-2

1,2-Dichloroethene (Total)

9.4

ug/L

1.0

0.22 1



05/25/22 18

:07

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



05/25/22 18

:07

75-35-4

cis-1,2-Dichloroethene

9.4

ug/L

1.0

0.13 1



05/25/22 18

:07

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



05/25/22 18

:07

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



05/25/22 18

:07

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



05/25/22 18

:07

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



05/25/22 18

:07

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



05/25/22 18

:07

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



05/25/22 18

:07

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



05/25/22 18

:07

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



05/25/22 18

:07

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



05/25/22 18

:07

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



05/25/22 18

:07

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



05/25/22 18

:07

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



05/25/22 18

:07

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



05/25/22 18

:07

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 13 of 44


-------
Pace Analytical Services, LLC

ice Analytical'

www.pacdiln.cani	(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW6-W-17 ^	Lab ID: 60400603005 Collected: 05/17/22 15:50 Received: 05/18/22 08:50 Matrix: Water

Report

Parameters	Results	Units	Limit MDL DF Prepared	Analyzed CAS No. Qual

8260 MSV	Analytical Method: EPA5030B/8260

Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

05/25/22 18:07

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/25/22 18:07

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/25/22 18:07

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/25/22 18:07

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/25/22 18:07

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/25/22 18:07

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/25/22 18:07

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/25/22 18:07

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/25/22 18:07

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/25/22 18:07

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/25/22 18:07

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/25/22 18:07

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/25/22 18:07

79-00-5

Trichloroethene



64.2

ug/L

1.0

0.21 1

05/25/22 18:07

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/25/22 18:07

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/25/22 18:07

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/25/22 18:07

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/25/22 18:07

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/25/22 18:07

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/25/22 18:07

1330-20-7

Surrogates















4-Bromofluorobenzene (S)



101

%

80-120

1

05/25/22 18:07

460-00-4

Toluene-d8 (S)



101

%

80-120

1

05/25/22 18:07

2037-26-5

1,2-Dichlorobenzene-d4 (S)



97 '

%

80-120

1

05/25/22 18:07

2199-69-1

Preservation pH



1.0 -



0.10

1

05/25/22 18:07



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0









Pace Analytical Services -

Kansas City







Chloride



9.2

mg/L

1.0

0.53 1

05/27/22 13:31

16887-00-

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 14 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-62-W-17

Parameters

Lab ID: 60400603006 Collected: 05/17/22 15:15 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Ethane
Ethene
Methane

6010 MET ICP

Iron

8260 MSV

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

ND
ND
ND

ug/L
ug/L
ug/L

10.0
10.0
10.0

3.8
7.1
5.5

05/20/22 14:07
05/20/22 14:07
05/20/22 14:07

74-84-0
74-85-1
74-82-8

Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Kansas City

3670 ug/L	50.0	5.6 1 05/19/22 13:25 05/20/22 20:56 7439-89-6

Analytical Method: EPA5030B/8260

Acetone

^ ND

ug/L

10.0

2.5 1

05/25/22 18:23

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/25/22 18:23

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/25/22 18:23

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:23

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/25/22 18:23

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/25/22 18:23

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/25/22 18:23

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/25/22 18:23

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/25/22 18:23

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/25/22 18:23

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:23

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/25/22 18:23

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/25/22 18:23

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/25/22 18:23

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/25/22 18:23

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/25/22 18:23

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/25/22 18:23

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/25/22 18:23

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/25/22 18:23

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/25/22 18:23

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/25/22 18:23

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/25/22 18:23

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/25/22 18:23

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:23

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:23

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:23

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:23

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/25/22 18:23

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/25/22 18:23

107-06-2

1,2-Dichloroethene (Total)

9.6

ug/L

1.0

0.22 1

05/25/22 18:23

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/25/22 18:23

75-35-4

cis-1,2-Dichloroethene

9.6

ug/L

1.0

0.13 1

05/25/22 18:23

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/25/22 18:23

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/25/22 18:23

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/25/22 18:23

142-28-9

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 15 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-62-W-17

Parameters

Lab ID: 60400603006 Collected: 05/17/22 15:15 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

2,2-Dichloropropane

^ ND

ug/L

1.0

0.16 1

05/25/22 18:23

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/25/22 18:23

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/25/22 18:23

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/25/22 18:23

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:23

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/25/22 18:23

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/25/22 18:23

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/25/22 18:23

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/25/22 18:23

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/25/22 18:23

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1

05/25/22 18:23

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1

05/25/22 18:23

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1

05/25/22 18:23

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:23

103-65-1

Styrene

ND

ug/L

1.0

0.12 1

05/25/22 18:23

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1

05/25/22 18:23

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1

05/25/22 18:23

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1

05/25/22 18:23

127-18-4

Toluene

ND

ug/L

1.0

0.25 1

05/25/22 18:23

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1

05/25/22 18:23

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1

05/25/22 18:23

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1

05/25/22 18:23

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1

05/25/22 18:23

79-00-5

Trichloroethene

16.3

ug/L

1.0

0.21 1

05/25/22 18:23

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1

05/25/22 18:23

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1

05/25/22 18:23

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1

05/25/22 18:23

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1

05/25/22 18:23

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1

05/25/22 18:23

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1

05/25/22 18:23

1330-20-7

Surrogates













4-Bromofluorobenzene (S)

sf" 102

%

80-120

1

05/25/22 18:23

460-00-4

Toluene-d8 (S)

101

/ %

80-120

1

05/25/22 18:23

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

%

80-120

1

05/25/22 18:23

2199-69-1

Preservation pH

1.0



0.10

1

05/25/22 18:23



300.0 IC Anions 28 Days

Analytical Method:

EPA 300.0









Pace Analytical Services - Kansas City







Chloride

16.6

mg/L

1.0

0.53 1

05/27/22 13:44

16887-00-6

Sulfate

13.3

mg/L

1.0

0.55 1

05/27/22 13:44

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method:

EPA 353.2









Pace Analytical Services - Kansas City







Nitrogen, Nitrate

0.26

mg/L

0.10

0.079 1

05/19/22 10:22

14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 16 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-43-W-17 +

"" Lab ID:

60400603007

Collected:

05/17/22 16:06

Received: 05/18/22 08:50 Matrix: Water

~





Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City







Acetone

~ ND

ug/L

10.0

2.5 1

05/25/22 18:39

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/25/22 18:39

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/25/22 18:39

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:39

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/25/22 18:39

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/25/22 18:39

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/25/22 18:39

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/25/22 18:39

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/25/22 18:39

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/25/22 18:39

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:39

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/25/22 18:39

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/25/22 18:39

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/25/22 18:39

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/25/22 18:39

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/25/22 18:39

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/25/22 18:39

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/25/22 18:39

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/25/22 18:39

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/25/22 18:39

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/25/22 18:39

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/25/22 18:39

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/25/22 18:39

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:39

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:39

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:39

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:39

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/25/22 18:39

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/25/22 18:39

107-06-2

1,2-Dichloroethene (Total)

0.67J

ug/L

1.0

0.22 1

05/25/22 18:39

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/25/22 18:39

75-35-4

cis-1,2-Dichloroethene

0.67J

ug/L

1.0

0.13 1

05/25/22 18:39

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/25/22 18:39

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/25/22 18:39

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/25/22 18:39

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/25/22 18:39

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/25/22 18:39

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/25/22 18:39

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/25/22 18:39

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:39

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/25/22 18:39

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/25/22 18:39

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/25/22 18:39

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/25/22 18:39

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/25/22 18:39

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 17 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-43-W-17 +

Lab ID:

60400603007

Collected:

05/17/22 16:06

Received:

05/18/22 08:50 Matrix: Water

~





Report









Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City





y



4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1



05/25/22 18:39

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



05/25/22 18:39

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



05/25/22 18:39

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



05/25/22 18:39

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



05/25/22 18:39

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



05/25/22 18:39

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



05/25/22 18:39

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



05/25/22 18:39

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



05/25/22 18:39

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



05/25/22 18:39

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



05/25/22 18:39

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



05/25/22 18:39

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



05/25/22 18:39

79-00-5

Trichloroethene

2.3

ug/L

1.0

0.21 1



05/25/22 18:39

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



05/25/22 18:39

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



05/25/22 18:39

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



05/25/22 18:39

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



05/25/22 18:39

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



05/25/22 18:39

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



05/25/22 18:39

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

103

%

80-120

1



05/25/22 18:39

460-00-4

Toluene-d8 (S)

100

%

80-120

1



05/25/22 18:39

2037-26-5

1,2-Dichlorobenzene-d4 (S)

98

^ %

80-120

1



05/25/22 18:39

2199-69-1

Preservation pH

1.0

—

0.10

1



05/25/22 18:39



Qual

300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

3.7

mg/L

1.0

0.53

05/27/22 13:58 16887-00-6

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 18 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW1-W-17 +

Lab ID:

60400603008

Collected:

05/17/22 16:37

Received: 05/18/22 08:50 Matrix: Water

~





Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City







Acetone

^ ND

ug/L

10.0

2.5 1

05/25/22 18:55

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/25/22 18:55

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/25/22 18:55

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:55

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/25/22 18:55

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/25/22 18:55

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/25/22 18:55

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/25/22 18:55

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/25/22 18:55

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/25/22 18:55

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:55

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/25/22 18:55

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/25/22 18:55

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/25/22 18:55

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/25/22 18:55

75-00-3

Chloroform

0.27J

ug/L

1.0

0.22 1

05/25/22 18:55

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/25/22 18:55

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/25/22 18:55

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/25/22 18:55

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/25/22 18:55

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/25/22 18:55

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/25/22 18:55

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/25/22 18:55

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:55

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:55

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/25/22 18:55

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/25/22 18:55

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/25/22 18:55

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/25/22 18:55

107-06-2

1,2-Dichloroethene (Total)

1.7

ug/L

1.0

0.22 1

05/25/22 18:55

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/25/22 18:55

75-35-4

cis-1,2-Dichloroethene

1.7

ug/L

1.0

0.13 1

05/25/22 18:55

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/25/22 18:55

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/25/22 18:55

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/25/22 18:55

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/25/22 18:55

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/25/22 18:55

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/25/22 18:55

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/25/22 18:55

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 18:55

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/25/22 18:55

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/25/22 18:55

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/25/22 18:55

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/25/22 18:55

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/25/22 18:55

75-09-2

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 19 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: RI-MW1-W-17 +

Lab ID:

60400603008

Collected:

05/17/22 16:37

Received:

05/18/22 08:50

Matrix: Water

~







Report











Parameters

Results



Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





/





4-Methyl-2-pentanone (MIBK)

~ ND



ug/L

10.0

0.74 1



05/25/22 18

:55

108-10-1

Methyl-tert-butyl ether

ND



ug/L

1.0

0.13 1



05/25/22 18

:55

1634-04-4

Naphthalene

ND



ug/L

10.0

0.82 1



05/25/22 18

:55

91-20-3

n-Propylbenzene

ND



ug/L

1.0

0.12 1



05/25/22 18

:55

103-65-1

Styrene

ND



ug/L

1.0

0.12 1



05/25/22 18

:55

100-42-5

1,1,1,2-Tetrachloroethane

ND



ug/L

1.0

0.084 1



05/25/22 18

:55

630-20-6

1,1,2,2-Tetrachloroethane

ND



ug/L

1.0

0.15 1



05/25/22 18

:55

79-34-5

Tetrachloroethene

ND



ug/L

1.0

0.33 1



05/25/22 18

:55

127-18-4

Toluene

ND



ug/L

1.0

0.25 1



05/25/22 18

:55

108-88-3

1,2,3-Trichlorobenzene

ND



ug/L

1.0

0.93 1



05/25/22 18

:55

87-61-6

1,2,4-Trichlorobenzene

ND



ug/L

1.0

0.73 1



05/25/22 18

:55

120-82-1

1,1,1-Trichloroethane

ND



ug/L

1.0

0.11 1



05/25/22 18

:55

71-55-6

1,1,2-Trichloroethane

ND



ug/L

1.0

0.14 1



05/25/22 18

:55

79-00-5

Trichloroethene

57.3



ug/L

1.0

0.21 1



05/25/22 18

:55

79-01-6

Trichlorofluoromethane

ND



ug/L

1.0

0.16 1



05/25/22 18

:55

75-69-4

1,2,3-Trichloropropane

ND



ug/L

2.5

0.41 1



05/25/22 18

:55

96-18-4

1,2,4-Trimethylbenzene

ND



ug/L

1.0

0.32 1



05/25/22 18

:55

95-63-6

1,3,5-Trimethylbenzene

ND



ug/L

1.0

0.090 1



05/25/22 18

:55

108-67-8

Vinyl chloride

ND



ug/L

1.0

0.17 1



05/25/22 18

:55

75-01-4

Xylene (Total)

ND



ug/L

3.0

0.28 1



05/25/22 18

:55

1330-20-7

Surrogates



















4-Bromofluorobenzene (S)

103



%

80-120

1



05/25/22 18

:55

460-00-4

Toluene-d8 (S)

99



%

80-120

1



05/25/22 18

:55

2037-26-5

1,2-Dichlorobenzene-d4 (S)

98



%

80-120

1



05/25/22 18

:55

2199-69-1

Preservation pH

1.0

y



0.10

1



05/25/22 18

:55



Qual

300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

10.6 mg/L	1.0

0.53

05/27/22 14:12 16887-00-6

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 20 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-56-W-17 +

Lab ID:

60400603009 Collected:

05/17/22 17:00

Received: 05/18/22 08:50

Matrix: Wate

~





Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/20/22 14:28

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/20/22 14:28

74-85-1

Methane

ND

ug/L

10.0

5.5

1



05/20/22 14:28

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010









Pace Analytical Services - Kansas City













Iron

531

ug/L

50.0

5.6

1

05/19/22 13:25

05/20/22 20:58

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City







/





Acetone

ND

ug/L

10.0

2.5

1



05/25/22 19

11

67-64-1

Benzene

ND

ug/L

1.0

0.14

1



05/25/22 19

11

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



05/25/22 19

11

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



05/25/22 19

11

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



05/25/22 19

11

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



05/25/22 19

11

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



05/25/22 19

11

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



05/25/22 19

11

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



05/25/22 19

11

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



05/25/22 19

11

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



05/25/22 19

11

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



05/25/22 19

11

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



05/25/22 19

11

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



05/25/22 19

11

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



05/25/22 19

11

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



05/25/22 19

11

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



05/25/22 19

11

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



05/25/22 19

11

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



05/25/22 19

11

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



05/25/22 19

11

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



05/25/22 19

11

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



05/25/22 19

11

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



05/25/22 19

11

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



05/25/22 19

11

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/25/22 19

11

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/25/22 19

11

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



05/25/22 19

11

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



05/25/22 19

11

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



05/25/22 19

11

107-06-2

1,2-Dichloroethene (Total)

84.3

ug/L

1.0

0.22

1



05/25/22 19

11

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22

1



05/25/22 19

11

75-35-4

cis-1,2-Dichloroethene

83.2

ug/L

1.0

0.13

1



05/25/22 19

11

156-59-2

trans-1,2-Dichloroethene

1.1

ug/L

1.0

0.10

1



05/25/22 19

11

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



05/25/22 19

11

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



05/25/22 19

11

142-28-9

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 21 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-56-W-17

Parameters

Lab ID: 60400603009 Collected: 05/17/22 17:00 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method:

EPA 5030B/8260











Pace Analytical Services - Kansas City



/





2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/25/22 19

11

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/25/22 19

11

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/25/22 19

11

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/25/22 19

11

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 19

11

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/25/22 19

11

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/25/22 19

11

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/25/22 19

11

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/25/22 19

11

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/25/22 19

11

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1

05/25/22 19

11

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1

05/25/22 19

11

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1

05/25/22 19

11

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1

05/25/22 19

11

103-65-1

Styrene

ND

ug/L

1.0

0.12 1

05/25/22 19

11

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1

05/25/22 19

11

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1

05/25/22 19

11

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1

05/25/22 19

11

127-18-4

Toluene

ND

ug/L

1.0

0.25 1

05/25/22 19

11

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1

05/25/22 19

11

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1

05/25/22 19

11

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1

05/25/22 19

11

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1

05/25/22 19

11

79-00-5

Trichloroethene

8.9

ug/L

1.0

0.21 1

05/25/22 19

11

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1

05/25/22 19

11

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1

05/25/22 19

11

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1

05/25/22 19

11

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1

05/25/22 19

11

108-67-8

Vinyl chloride

0.25J

ug/L

1.0

0.17 1

05/25/22 19

11

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1

05/25/22 19

11

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

98

%

80-120

1

05/25/22 19

11

460-00-4

Toluene-d8 (S)

100

%

80-120

1

05/25/22 19

11

2037-26-5

1,2-Dichlorobenzene-d4 (S)

98

/ %

80-120

1

05/25/22 19

11

2199-69-1

Preservation pH

1.0

~

0.10

1

05/25/22 19

11



300.0 IC Anions 28 Days

Analytical Method:

EPA 300.0











Pace Analytical Services - Kansas City









Chloride

26.1

mg/L

20.0

10.5 20

05/27/22 00:42

16887-00-6

Qual

Sulfate

353.2 Nitrogen, N02/N03 unpres

36.7

mg/L

20.0

11.0 20

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.81 mg/L	0.10 0.079 1

05/27/22 00:42 14808-79-8

05/19/22 10:25 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 22 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-33-W-17

Parameters

__ Lab ID: 60400603010 Collected: 05/17/22 17:20 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Ethane
Ethene
Methane

6010 MET ICP

Iron

8260 MSV

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

ND
ND
ND

ug/L
ug/L
ug/L

10.0
10.0
10.0

3.8
7.1
5.5

05/20/22 15:10
05/20/22 15:10
05/20/22 15:10

74-84-0
74-85-1
74-82-8

Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Kansas City

611 ug/L	50.0	5.6 1 05/19/22 13:25 05/20/22 21:04 7439-89-6

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

Acetone

^ ND

ug/L

10.0

2.5

Benzene

ND

ug/L

1.0

0.14

Bromobenzene

ND

ug/L

1.0

0.088

Bromochloromethane

ND

ug/L

1.0

0.20

Bromodichloromethane

ND

ug/L

1.0

0.16

Bromoform

ND

ug/L

1.0

0.68

Bromomethane

ND

ug/L

5.0

0.46

2-Butanone (MEK)

ND

ug/L

10.0

0.98

n-Butylbenzene

ND

ug/L

1.0

0.15

sec-Butylbenzene

ND

ug/L

1.0

0.11

tert-Butylbenzene

ND

ug/L

1.0

0.12

Carbon disulfide

ND

ug/L

5.0

0.98

Carbon tetrachloride

ND

ug/L

1.0

0.17

Chlorobenzene

ND

ug/L

1.0

0.089

Chloroethane

ND

ug/L

1.0

0.37

Chloroform

ND

ug/L

1.0

0.22

Chloromethane

ND

ug/L

1.0

0.28

2-Chlorotoluene

ND

ug/L

1.0

0.11

4-Chlorotoluene

ND

ug/L

1.0

0.15

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

Dibromochloromethane

ND

ug/L

1.0

0.30

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

Dibromomethane

ND

ug/L

1.0

0.11

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1,2-Dichloroethene (Total)

4.7

ug/L

1.0

0.22

1,1-Dichloroethene

ND

ug/L

1.0

0.22

cis-1,2-Dichloroethene

4.7

ug/L

1.0

0.13

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1,3-Dichloropropane

ND

ug/L

1.0

0.10

05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27
05/25/22 19:27

67-64-1
71-43-2
108-86-1

74-97-5

75-27-4
75-25-2

74-83-9
78-93-3

104-51-8
135-98-8
98-06-6

75-15-0
56-23-5

108-90-7
75-00-3
67-66-3
74-87-3

95-49-8

106-43-4

96-12-8

124-48-1
106-93-4

74-95-3
95-50-1
541 -73-1

106-46-7

75-71-8
75-34-3

107-06-2
540-59-0
75-35-4

156-59-2
156-60-5
78-87-5
142-28-9

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 23 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: FAG-33-W-17 +

Lab ID:

60400603010

Collected:

05/17/22 17:20

Received:

05/18/22 08:50 Matrix: Water

~





Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



05/25/22 19:27

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



05/25/22 19:27

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



05/25/22 19:27

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



05/25/22 19:27

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



05/25/22 19:27

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



05/25/22 19:27

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



05/25/22 19:27

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



05/25/22 19:27

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



05/25/22 19:27

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



05/25/22 19:27

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



05/25/22 19:27

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



05/25/22 19:27

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



05/25/22 19:27

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



05/25/22 19:27

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



05/25/22 19:27

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



05/25/22 19:27

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



05/25/22 19:27

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



05/25/22 19:27

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



05/25/22 19:27

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



05/25/22 19:27

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



05/25/22 19:27

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



05/25/22 19:27

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



05/25/22 19:27

79-00-5

Trichloroethene

31.7

ug/L

1.0

0.21

1



05/25/22 19:27

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



05/25/22 19:27

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



05/25/22 19:27

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



05/25/22 19:27

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



05/25/22 19:27

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17

1



05/25/22 19:27

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



05/25/22 19:27

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

101

%

80-120



1



05/25/22 19:27

460-00-4

Toluene-d8 (S)

100

%

80-120



1



05/25/22 19:27

2037-26-5

1,2-Dichlorobenzene-d4 (S)

102^

%

80-120



1



05/25/22 19:27

2199-69-1

Preservation pH

1.0^"



0.10



1



05/25/22 19:27



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

15.0

mg/L

1.0

0.53

1



05/27/22 14:26

16887-00-6

Sulfate

1.3

mg/L

1.0

0.55

1



05/27/22 14:26

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

0.080J

mg/L

0.10

0.079

1



05/19/22 10:26

14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 24 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: TB-01-051722

Parameters



Lab ID: 60400603011 Collected: 05/17/22 18:00 Received: 05/18/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF Prepared

Analyzed CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260

all ND; no qual.

Acetone



ND

ug/L

10.0

2.5 1

05/25/22 19:43

67-64-1

Benzene



ND

ug/L

1.0

0.14 1

05/25/22 19:43

71-43-2

Bromobenzene



ND

ug/L

1.0

0.088 1

05/25/22 19:43

108-86-1

Bromochloromethane



ND

ug/L

1.0

0.20 1

05/25/22 19:43

74-97-5

Bromodichloromethane



ND

ug/L

1.0

0.16 1

05/25/22 19:43

75-27-4

Bromoform



ND

ug/L

1.0

0.68 1

05/25/22 19:43

75-25-2

Bromomethane



ND

ug/L

5.0

0.46 1

05/25/22 19:43

74-83-9

2-Butanone (MEK)



ND

ug/L

10.0

0.98 1

05/25/22 19:43

78-93-3

n-Butylbenzene



ND

ug/L

1.0

0.15 1

05/25/22 19:43

104-51-8

sec-Butylbenzene



ND

ug/L

1.0

0.11 1

05/25/22 19:43

135-98-8

tert-Butylbenzene



ND

ug/L

1.0

0.12 1

05/25/22 19:43

98-06-6

Carbon disulfide



ND

ug/L

5.0

0.98 1

05/25/22 19:43

75-15-0

Carbon tetrachloride



ND

ug/L

1.0

0.17 1

05/25/22 19:43

56-23-5

Chlorobenzene



ND

ug/L

1.0

0.089 1

05/25/22 19:43

108-90-7

Chloroethane



ND

ug/L

1.0

0.37 1

05/25/22 19:43

75-00-3

Chloroform



ND

ug/L

1.0

0.22 1

05/25/22 19:43

67-66-3

Chloromethane



ND

ug/L

1.0

0.28 1

05/25/22 19:43

74-87-3

2-Chlorotoluene



ND

ug/L

1.0

0.11 1

05/25/22 19:43

95-49-8

4-Chlorotoluene



ND

ug/L

1.0

0.15 1

05/25/22 19:43

106-43-4

1,2-Dibromo-3-chloropropane



ND

ug/L

2.5

0.78 1

05/25/22 19:43

96-12-8

Dibromochloromethane



ND

ug/L

1.0

0.30 1

05/25/22 19:43

124-48-1

1,2-Dibromoethane (EDB)



ND

ug/L

1.0

0.20 1

05/25/22 19:43

106-93-4

Dibromomethane



ND

ug/L

1.0

0.11 1

05/25/22 19:43

74-95-3

1,2-Dichlorobenzene



ND

ug/L

1.0

0.12 1

05/25/22 19:43

95-50-1

1,3-Dichlorobenzene



ND

ug/L

1.0

0.13 1

05/25/22 19:43

541 -73-1

1,4-Dichlorobenzene



ND

ug/L

1.0

0.13 1

05/25/22 19:43

106-46-7

Dichlorodifluoromethane



ND

ug/L

1.0

0.20 1

05/25/22 19:43

75-71-8

1,1-Dichloroethane



ND

ug/L

1.0

0.12 1

05/25/22 19:43

75-34-3

1,2-Dichloroethane



ND

ug/L

1.0

0.21 1

05/25/22 19:43

107-06-2

1,2-Dichloroethene (Total)



ND

ug/L

1.0

0.22 1

05/25/22 19:43

540-59-0

1,1-Dichloroethene



ND

ug/L

1.0

0.22 1

05/25/22 19:43

75-35-4

cis-1,2-Dichloroethene



ND

ug/L

1.0

0.13 1

05/25/22 19:43

156-59-2

trans-1,2-Dichloroethene



ND

ug/L

1.0

0.10 1

05/25/22 19:43

156-60-5

1,2-Dichloropropane



ND

ug/L

1.0

0.14 1

05/25/22 19:43

78-87-5

1,3-Dichloropropane



ND

ug/L

1.0

0.10 1

05/25/22 19:43

142-28-9

2,2-Dichloropropane



ND

ug/L

1.0

0.16 1

05/25/22 19:43

594-20-7

1,1-Dichloropropene



ND

ug/L

1.0

0.14 1

05/25/22 19:43

563-58-6

cis-1,3-Dichloropropene



ND

ug/L

1.0

0.078 1

05/25/22 19:43

10061 -01 -5

trans-1,3-Dichloropropene



ND

ug/L

1.0

0.18 1

05/25/22 19:43

10061 -02-6

Ethylbenzene



ND

ug/L

1.0

0.12 1

05/25/22 19:43

100-41-4

Hexachloro-1,3-butadiene



ND

ug/L

1.0

0.42 1

05/25/22 19:43

87-68-3

2-Hexanone



ND

ug/L

10.0

1.1 1

05/25/22 19:43

591 -78-6

Isopropylbenzene (Cumene)



ND

ug/L

1.0

0.097 1

05/25/22 19:43

98-82-8

p-lsopropyltoluene



ND

ug/L

1.0

0.13 1

05/25/22 19:43

99-87-6

Methylene Chloride



ND

ug/L

1.0

0.39 1

05/25/22 19:43

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 25 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Sample: TB-01-051722 +

Lab ID:

60400603011

Collected:

05/17/22 18:00

Received:

05/18/22 08:50 Matrix: Water



~





Report













Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

Kansas City





/







4-Methyl-2-pentanone (MIBK)

^ ND

ug/L

10.0

0.74 1



05/25/22

19:43

108-10-1



Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



05/25/22

19:43

1634-04-4



Naphthalene

ND

ug/L

10.0

0.82 1



05/25/22

19:43

91-20-3



n-Propylbenzene

ND

ug/L

1.0

0.12 1



05/25/22

19:43

103-65-1



Styrene

ND

ug/L

1.0

0.12 1



05/25/22

19:43

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



05/25/22

19:43

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



05/25/22

19:43

79-34-5



Tetrachloroethene

ND

ug/L

1.0

0.33 1



05/25/22

19:43

127-18-4



Toluene

ND

ug/L

1.0

0.25 1



05/25/22

19:43

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



05/25/22

19:43

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



05/25/22

19:43

120-82-1



1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



05/25/22

19:43

71-55-6



1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



05/25/22

19:43

79-00-5



Trichloroethene

ND

ug/L

1.0

0.21 1



05/25/22

19:43

79-01-6



Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



05/25/22

19:43

75-69-4



1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



05/25/22

19:43

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



05/25/22

19:43

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



05/25/22

19:43

108-67-8



Vinyl chloride

ND

ug/L

1.0

0.17 1



05/25/22

19:43

75-01-4



Xylene (Total)

ND

ug/L

3.0

0.28 1



05/25/22

19:43

1330-20-7



Surrogates

4-Bromofluorobenzene (S)
Toluene-d8 (S)
1,2-Dichlorobenzene-d4 (S)
Preservation pH

104
101
101 ¦
1.0 ¦

%
%
%

80-120
80-120
80-120
0.10

05/25/22 19:43
05/25/22 19:43
05/25/22 19:43
05/25/22 19:43

460-00-4

2037-26-5

2199-69-1

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 26 of 44


-------
B. PACE PROJECT NUMBER 60400849


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-47-W-17

-x Lab ID:

60400849001 Collected:

05/18/22 08:45

Received: 05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8

1



05/23/22 17:52

74-84-0 L1

Ethene

ND

ug/L

10.0

7.1

1



05/23/22 17:52

74-85-1 L1

Methane

ND

ug/L

10.0

5.5

1



05/23/22 17:52

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010







Pace Analytical Services - Kansas City











Iron

243

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:31

7439-89-6

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City







* '



Acetone

ND

ug/L

10.0

2.5

1



05/27/22 02:55

67-64-1

Benzene

ND

ug/L

1.0

0.14

1



05/27/22 02:55

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



05/27/22 02:55

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



05/27/22 02:55

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



05/27/22 02:55

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



05/27/22 02:55

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



05/27/22 02:55

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



05/27/22 02:55

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



05/27/22 02:55

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



05/27/22 02:55

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 02:55

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



05/27/22 02:55

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



05/27/22 02:55

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



05/27/22 02:55

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



05/27/22 02:55

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



05/27/22 02:55

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



05/27/22 02:55

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



05/27/22 02:55

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



05/27/22 02:55

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



05/27/22 02:55

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



05/27/22 02:55

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



05/27/22 02:55

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



05/27/22 02:55

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



05/27/22 02:55

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/27/22 02:55

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/27/22 02:55

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



05/27/22 02:55

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



05/27/22 02:55

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



05/27/22 02:55

107-06-2

1,2-Dichloroethene (Total)

3.2

ug/L

1.0

0.22

1



05/27/22 02:55

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22

1



05/27/22 02:55

75-35-4

cis-1,2-Dichloroethene

3.2

ug/L

1.0

0.13

1



05/27/22 02:55

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10

1



05/27/22 02:55

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



05/27/22 02:55

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



05/27/22 02:55

142-28-9

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 6 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-47-W-17

Lab ID:

60400849001

Collected:

05/18/22 08:45

Received:

05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City







r



2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



05/27/22 02:55

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



05/27/22 02:55

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



05/27/22 02:55

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



05/27/22 02:55

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 02:55

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



05/27/22 02:55

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



05/27/22 02:55

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



05/27/22 02:55

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



05/27/22 02:55

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



05/27/22 02:55

75-09-2 L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



05/27/22 02:55

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



05/27/22 02:55

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



05/27/22 02:55

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 02:55

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



05/27/22 02:55

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



05/27/22 02:55

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



05/27/22 02:55

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



05/27/22 02:55

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



05/27/22 02:55

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



05/27/22 02:55

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



05/27/22 02:55

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



05/27/22 02:55

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



05/27/22 02:55

79-00-5

Trichloroethene

42.7

ug/L

1.0

0.21

1



05/27/22 02:55

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



05/27/22 02:55

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



05/27/22 02:55

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



05/27/22 02:55

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



05/27/22 02:55

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17

1



05/27/22 02:55

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



05/27/22 02:55

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

%

CD

%

80-120



1



05/27/22 02:55

460-00-4

Toluene-d8 (S)

100

%

80-120



1



05/27/22 02:55

2037-26-5

1,2-Dichlorobenzene-d4 (S)

98

J %

80-120



1



05/27/22 02:55

2199-69-1

Preservation pH

1.0

/

0.10



1



05/27/22 02:55



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

10.8

mg/L

1.0

0.53

1



05/27/22 11:27

16887-00-6

Sulfate

7.1

mg/L

1.0

0.55

1



05/27/22 11:27

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2











Nitrogen, Nitrate

Pace Analytical Services - Kansas City
1.2 mg/L	0.10

0.079

05/23/22 10:43 14797-55-8 H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 7 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-46-W-17 +

	Lab ID:

60400849002

Collected:

05/18/22 09:45

Received: 05/19/22 08:50 Matrix: Water

~





Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260



/





Pace Analytical Services

Kansas City



1



Acetone

^ ND

ug/L

10.0

2.5 1

05/27/22 03:08

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/27/22 03:08

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 03:08

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 03:08

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 03:08

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 03:08

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 03:08

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 03:08

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 03:08

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 03:08

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 03:08

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 03:08

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 03:08

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 03:08

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 03:08

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 03:08

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 03:08

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 03:08

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 03:08

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 03:08

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 03:08

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 03:08

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 03:08

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 03:08

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 03:08

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 03:08

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 03:08

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 03:08

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 03:08

107-06-2

1,2-Dichloroethene (Total)

1.7

ug/L

1.0

0.22 1

05/27/22 03:08

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 03:08

75-35-4

cis-1,2-Dichloroethene

1.7

ug/L

1.0

0.13 1

05/27/22 03:08

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 03:08

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 03:08

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 03:08

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 03:08

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 03:08

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 03:08

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 03:08

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 03:08

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/27/22 03:08

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/27/22 03:08

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/27/22 03:08

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/27/22 03:08

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/27/22 03:08

75-09-2 L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 8 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-46-W-17

Parameters

Lab ID: 60400849002 Collected: 05/18/22 09:45 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA5030B/8260

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

05/27/22 03:08

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/27/22 03:08

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/27/22 03:08

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 03:08

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/27/22 03:08

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/27/22 03:08

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/27/22 03:08

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/27/22 03:08

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/27/22 03:08

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/27/22 03:08

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/27/22 03:08

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/27/22 03:08

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/27/22 03:08

79-00-5

Trichloroethene



21.1

ug/L

1.0

0.21 1

05/27/22 03:08

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/27/22 03:08

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/27/22 03:08

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/27/22 03:08

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/27/22 03:08

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/27/22 03:08

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/27/22 03:08

1330-20-7

Surrogates















4-Bromofluorobenzene (S)



97

%

80-120

1

05/27/22 03:08

460-00-4

Toluene-d8 (S)



100

%

80-120

1

05/27/22 03:08

2037-26-5

1,2-Dichlorobenzene-d4 (S)



101 -

%

80-120

1

05/27/22 03:08

2199-69-1

Preservation pH



1.0



0.10

1

05/27/22 03:08



Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

4.7 mg/L	1.0

0.53

05/27/22 11:40 16887-00-6 B

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 9 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

"7"

Sample: FAG-05-W-17

Parameters

Lab ID: 60400849003 Collected: 05/18/22 09:00 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

Ethane

ND

ug/L

10.0

CO
00

05/24/22 18:19

74-84-0

Ethene

ND

ug/L

10.0

7.1 1

05/24/22 18:19

74-85-1

Methane

ND

ug/L

10.0

LO
LO

05/24/22 18:19

74-82-8

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services -

Kansas City



V



Acetone

ND

ug/L

10.0

2.5 1

05/27/22 02:27

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/27/22 02:27

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 02:27

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 02:27

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 02:27

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 02:27

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 02:27

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 02:27

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 02:27

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 02:27

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 02:27

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 02:27

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 02:27

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 02:27

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 02:27

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 02:27

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 02:27

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 02:27

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 02:27

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 02:27

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 02:27

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 02:27

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 02:27

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 02:27

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02:27

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02:27

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 02:27

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 02:27

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 02:27

107-06-2

1,2-Dichloroethene (Total)

2.6

ug/L

1.0

0.22 1

05/27/22 02:27

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 02:27

75-35-4

cis-1,2-Dichloroethene

2.6

ug/L

1.0

0.13 1

05/27/22 02:27

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 02:27

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 02:27

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 02:27

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 02:27

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 02:27

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 02:27

10061 -01 -

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 02:27

10061 -02-

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 10 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-05-W-17 ^

Parameters

Lab ID: 60400849003 Collected: 05/18/22 09:00 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260

Ethylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:27

100-41-4

Hexachloro-1,3-butadiene



ND

ug/L

1.0

0.42 1

05/27/22 02:27

87-68-3

2-Hexanone



ND

ug/L

10.0

1.1 1

05/27/22 02:27

591 -78-6

Isopropylbenzene (Cumene)



ND

ug/L

1.0

0.097 1

05/27/22 02:27

98-82-8

p-lsopropyltoluene



ND

ug/L

1.0

0.13 1

05/27/22 02:27

99-87-6

Methylene Chloride



ND

ug/L

1.0

0.39 1

05/27/22 02:27

75-09-2

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

05/27/22 02:27

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/27/22 02:27

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/27/22 02:27

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:27

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/27/22 02:27

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/27/22 02:27

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/27/22 02:27

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/27/22 02:27

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/27/22 02:27

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/27/22 02:27

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/27/22 02:27

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/27/22 02:27

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/27/22 02:27

79-00-5

Trichloroethene



18.7

ug/L

1.0

0.21 1

05/27/22 02:27

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/27/22 02:27

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/27/22 02:27

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/27/22 02:27

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/27/22 02:27

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/27/22 02:27

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/27/22 02:27

1330-20-7

Surrogates















4-Bromofluorobenzene (S)



96

%

80-120

1

05/27/22 02:27

460-00-4

Toluene-d8 (S)



99

/ %

80-120

1

05/27/22 02:27

2037-26-5

1,2-Dichlorobenzene-d4 (S)



102

80-120

1

05/27/22 02:27

2199-69-1

Preservation pH



1.0



0.10

1

05/27/22 02:27



300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

34.5 mg/L	10.0

11.2 mg/L	10.0

5.3
5.5

10
10

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

1.1 mg/L	0.10 0.079

L1

05/26/22 21:54 16887-00-6
05/26/22 21:54 14808-79-8

05/23/22 10:45 14797-55-8 H1

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 11 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FD-LIST B-05182022

Parameters

Lab ID: 60400849004 Collected: 05/18/22 09:00 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF Prepared

Analyzed CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260

Acetone

/

ND

ug/L

10.0

2.5 1

05/27/22 02:41

67-64-1

Benzene



ND

ug/L

1.0

0.14 1

05/27/22 02:41

71-43-2

Bromobenzene



ND

ug/L

1.0

0.088 1

05/27/22 02:41

108-86-1

Bromochloromethane



ND

ug/L

1.0

0.20 1

05/27/22 02:41

74-97-5

Bromodichloromethane



ND

ug/L

1.0

0.16 1

05/27/22 02:41

75-27-4

Bromoform



ND

ug/L

1.0

0.68 1

05/27/22 02:41

75-25-2

Bromomethane



ND

ug/L

5.0

0.46 1

05/27/22 02:41

74-83-9

2-Butanone (MEK)



ND

ug/L

10.0

0.98 1

05/27/22 02:41

78-93-3

n-Butylbenzene



ND

ug/L

1.0

0.15 1

05/27/22 02:41

104-51-8

sec-Butylbenzene



ND

ug/L

1.0

0.11 1

05/27/22 02:41

135-98-8

tert-Butylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:41

98-06-6

Carbon disulfide



ND

ug/L

5.0

0.98 1

05/27/22 02:41

75-15-0

Carbon tetrachloride



ND

ug/L

1.0

0.17 1

05/27/22 02:41

56-23-5

Chlorobenzene



ND

ug/L

1.0

0.089 1

05/27/22 02:41

108-90-7

Chloroethane



ND

ug/L

1.0

0.37 1

05/27/22 02:41

75-00-3

Chloroform



ND

ug/L

1.0

0.22 1

05/27/22 02:41

67-66-3

Chloromethane



ND

ug/L

1.0

0.28 1

05/27/22 02:41

74-87-3

2-Chlorotoluene



ND

ug/L

1.0

0.11 1

05/27/22 02:41

95-49-8

4-Chlorotoluene



ND

ug/L

1.0

0.15 1

05/27/22 02:41

106-43-4

1,2-Dibromo-3-chloropropane



ND

ug/L

2.5

0.78 1

05/27/22 02:41

96-12-8

Dibromochloromethane



ND

ug/L

1.0

0.30 1

05/27/22 02:41

124-48-1

1,2-Dibromoethane (EDB)



ND

ug/L

1.0

0.20 1

05/27/22 02:41

106-93-4

Dibromomethane



ND

ug/L

1.0

0.11 1

05/27/22 02:41

74-95-3

1,2-Dichlorobenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:41

95-50-1

1,3-Dichlorobenzene



ND

ug/L

1.0

0.13 1

05/27/22 02:41

541 -73-1

1,4-Dichlorobenzene



ND

ug/L

1.0

0.13 1

05/27/22 02:41

106-46-7

Dichlorodifluoromethane



ND

ug/L

1.0

0.20 1

05/27/22 02:41

75-71-8

1,1-Dichloroethane



ND

ug/L

1.0

0.12 1

05/27/22 02:41

75-34-3

1,2-Dichloroethane



ND

ug/L

1.0

0.21 1

05/27/22 02:41

107-06-2

1,2-Dichloroethene (Total)



2.9

ug/L

1.0

0.22 1

05/27/22 02:41

540-59-0

1,1-Dichloroethene



ND

ug/L

1.0

0.22 1

05/27/22 02:41

75-35-4

cis-1,2-Dichloroethene



2.9

ug/L

1.0

0.13 1

05/27/22 02:41

156-59-2

trans-1,2-Dichloroethene



ND

ug/L

1.0

0.10 1

05/27/22 02:41

156-60-5

1,2-Dichloropropane



ND

ug/L

1.0

0.14 1

05/27/22 02:41

78-87-5

1,3-Dichloropropane



ND

ug/L

1.0

0.10 1

05/27/22 02:41

142-28-9

2,2-Dichloropropane



ND

ug/L

1.0

0.16 1

05/27/22 02:41

594-20-7

1,1-Dichloropropene



ND

ug/L

1.0

0.14 1

05/27/22 02:41

563-58-6

cis-1,3-Dichloropropene



ND

ug/L

1.0

0.078 1

05/27/22 02:41

10061 -01 -5

trans-1,3-Dichloropropene



ND

ug/L

1.0

0.18 1

05/27/22 02:41

10061 -02-6

Ethylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:41

100-41-4

Hexachloro-1,3-butadiene



ND

ug/L

1.0

0.42 1

05/27/22 02:41

87-68-3

2-Hexanone



ND

ug/L

10.0

1.1 1

05/27/22 02:41

591 -78-6

Isopropylbenzene (Cumene)



ND

ug/L

1.0

0.097 1

05/27/22 02:41

98-82-8

p-lsopropyltoluene



ND

ug/L

1.0

0.13 1

05/27/22 02:41

99-87-6

Methylene Chloride



ND

ug/L

1.0

0.39 1

05/27/22 02:41

75-09-2

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 12 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FD-LIST B-05182022

Lab ID: 60400849004 Collected: 05/18/22 09:00 Received: 05/19/22 08:50 Matrix: Water

V

Parameters

Results

Units

Report
Limit

MDL DF

Prepared

Analyzed

CAS No

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

- Kansas City





/



4-Methyl-2-pentanone (MIBK)

/

ND

ug/L

10.0

0.74 1



05/27/22 02:41

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1



05/27/22 02:41

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1



05/27/22 02:41

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1



05/27/22 02:41

103-65-1

Styrene



ND

ug/L

1.0

0.12 1



05/27/22 02:41

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1



05/27/22 02:41

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1



05/27/22 02:41

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1



05/27/22 02:41

127-18-4

Toluene



ND

ug/L

1.0

0.25 1



05/27/22 02:41

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1



05/27/22 02:41

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1



05/27/22 02:41

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1



05/27/22 02:41

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1



05/27/22 02:41

79-00-5

Trichloroethene



18.0

ug/L

1.0

0.21 1



05/27/22 02:41

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1



05/27/22 02:41

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1



05/27/22 02:41

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1



05/27/22 02:41

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1



05/27/22 02:41

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1



05/27/22 02:41

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1



05/27/22 02:41

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)



101

%

80-120

1



05/27/22 02:41

460-00-4

Toluene-d8 (S)



102

%

80-120

1



05/27/22 02:41

2037-26-5

1,2-Dichlorobenzene-d4 (S)



100

' %

80-120

1



05/27/22 02:41

2199-69-1

Preservation pH



1.0

S

0.10

1



05/27/22 02:41



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0











Pace Analytical Services

- Kansas City









Chloride



34.0

mg/L

10.0

5.3 10



05/26/22 22:22

16887-00-

Qual

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

Date: 06/03/2022 02:36 PM	without the written consent of Pace Analytical Services, LLC.	Page 13 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-11-W-17 ^

Lab ID:

60400849005

Collected:

05/18/22 11:05

Received: 05/19/22 08:50 Matrix: Water







Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City



~



Acetone

W 6.1J

ug/L

10.0

2.5 1

05/27/22 02:00

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/27/22 02:00

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 02:00

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 02:00

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 02:00

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 02:00

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 02:00

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 02:00

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 02:00

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 02:00

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 02:00

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 02:00

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 02:00

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 02:00

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 02:00

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 02:00

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 02:00

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 02:00

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 02:00

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 02:00

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 02:00

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 02:00

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 02:00

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 02:00

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02:00

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02:00

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 02:00

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 02:00

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 02:00

107-06-2

1,2-Dichloroethene (Total)

0.66J

ug/L

1.0

0.22 1

05/27/22 02:00

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 02:00

75-35-4

cis-1,2-Dichloroethene

0.66J

ug/L

1.0

0.13 1

05/27/22 02:00

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 02:00

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 02:00

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 02:00

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 02:00

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 02:00

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 02:00

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 02:00

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 02:00

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/27/22 02:00

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/27/22 02:00

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/27/22 02:00

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/27/22 02:00

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/27/22 02:00

75-09-2 L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 14 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-11-W-17

Parameters

Lab ID: 60400849005 Collected: 05/18/22 11:05 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)

~

ND

ug/L

10.0

0.74 1

05/27/22 02:00

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/27/22 02:00

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/27/22 02:00

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 02:00

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/27/22 02:00

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/27/22 02:00

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/27/22 02:00

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/27/22 02:00

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/27/22 02:00

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/27/22 02:00

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/27/22 02:00

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/27/22 02:00

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/27/22 02:00

79-00-5

Trichloroethene



2.3

ug/L

1.0

0.21 1

05/27/22 02:00

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/27/22 02:00

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/27/22 02:00

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/27/22 02:00

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/27/22 02:00

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/27/22 02:00

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/27/22 02:00

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

/

96

%

80-120

1

05/27/22 02:00

460-00-4

Toluene-d8 (S)



100

%

80-120

1

05/27/22 02:00

2037-26-5

1,2-Dichlorobenzene-d4 (S)



102

%

80-120

1

05/27/22 02:00

2199-69-1

Preservation pH



1.0

f

0.10

1

05/27/22 02:00



300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

32.6 mg/L	10.0

5.3 10

05/26/22 22:50 16887-00-6 B

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,

Date: 06/03/2022 02:36 PM	without the written consent of Pace Analytical Services, LLC.	Page 15 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-35-W-17 +

Lab ID:

60400849006 Collected:

05/18/22 11:45

Received: 05/19/22 08:50 Matrix: Water



~W





Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/23/22 18:13

74-84-0

L1

Ethene

ND

ug/L

10.0

7.1

1



05/23/22 18:13

74-85-1

L1

Methane

25.2

ug/L

10.0

5.5

1



05/23/22 18:13

74-82-8



6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010









Pace Analytical Services - Kansas City













Iron

23.5J

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:33

7439-89-6

B

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City







y





Acetone

ND

ug/L

50.0

12.7

5



05/27/22 03:35

67-64-1



Benzene

ND

ug/L

5.0

0.68

5



05/27/22 03:35

71-43-2



Bromobenzene

ND

ug/L

5.0

0.44

5



05/27/22 03:35

108-86-1



Bromochloromethane

ND

ug/L

5.0

1.0

5



05/27/22 03:35

74-97-5



Bromodichloromethane

ND

ug/L

5.0

0.78

5



05/27/22 03:35

75-27-4



Bromoform

ND

ug/L

5.0

3.4

5



05/27/22 03:35

75-25-2



Bromomethane

ND

ug/L

25.0

2.3

5



05/27/22 03:35

74-83-9



2-Butanone (MEK)

ND

ug/L

50.0

4.9

5



05/27/22 03:35

78-93-3



n-Butylbenzene

ND

ug/L

5.0

0.76

5



05/27/22 03:35

104-51-8



sec-Butylbenzene

ND

ug/L

5.0

0.55

5



05/27/22 03:35

135-98-8



tert-Butylbenzene

ND

ug/L

5.0

0.60

5



05/27/22 03:35

98-06-6



Carbon disulfide

ND

ug/L

25.0

4.9

5



05/27/22 03:35

75-15-0



Carbon tetrachloride

ND

ug/L

5.0

0.86

5



05/27/22 03:35

56-23-5



Chlorobenzene

ND

ug/L

5.0

0.44

5



05/27/22 03:35

108-90-7



Chloroethane

ND

ug/L

5.0

1.9

5



05/27/22 03:35

75-00-3



Chloroform

ND

ug/L

5.0

1.1

5



05/27/22 03:35

67-66-3



Chloromethane

ND

ug/L

5.0

1.4

5



05/27/22 03:35

74-87-3



2-Chlorotoluene

ND

ug/L

5.0

0.54

5



05/27/22 03:35

95-49-8



4-Chlorotoluene

ND

ug/L

5.0

0.74

5



05/27/22 03:35

106-43-4



1,2-Dibromo-3-chloropropane

ND

ug/L

12.5

3.9

5



05/27/22 03:35

96-12-8



Dibromochloromethane

ND

ug/L

5.0

1.5

5



05/27/22 03:35

124-48-1



1,2-Dibromoethane (EDB)

ND

ug/L

5.0

0.98

5



05/27/22 03:35

106-93-4



Dibromomethane

ND

ug/L

5.0

0.54

5



05/27/22 03:35

74-95-3



1,2-Dichlorobenzene

ND

ug/L

5.0

0.62

5



05/27/22 03:35

95-50-1



1,3-Dichlorobenzene

ND

ug/L

5.0

0.66

5



05/27/22 03:35

541 -73-1



1,4-Dichlorobenzene

ND

ug/L

5.0

0.66

5



05/27/22 03:35

106-46-7



Dichlorodifluoromethane

ND

ug/L

5.0

1.0

5



05/27/22 03:35

75-71-8



1,1-Dichloroethane

ND

ug/L

5.0

0.61

5



05/27/22 03:35

75-34-3



1,2-Dichloroethane

ND

ug/L

5.0

1.1

5



05/27/22 03:35

107-06-2



1,2-Dichloroethene (Total)

115

ug/L

5.0

1.1

5



05/27/22 03:35

540-59-0



1,1-Dichloroethene

ND

ug/L

5.0

1.1

5



05/27/22 03:35

75-35-4



cis-1,2-Dichloroethene

111

ug/L

5.0

0.64

5



05/27/22 03:35

156-59-2



trans-1,2-Dichloroethene

3.3J

ug/L

5.0

0.51

5



05/27/22 03:35

156-60-5



1,2-Dichloropropane

ND

ug/L

5.0

0.70

5



05/27/22 03:35

78-87-5



1,3-Dichloropropane

ND

ug/L

5.0

0.52

5



05/27/22 03:35

142-28-9



REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 16 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-35-W-17 ^

Lab ID:

60400849006

Collected:

05/18/22 11:45

Received:

05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City







~



2,2-Dichloropropane

ND

ug/L

5.0

0.81

5



05/27/22 03:35

594-20-7

1,1-Dichloropropene

ND

ug/L

5.0

0.68

5



05/27/22 03:35

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

5.0

0.39

5



05/27/22 03:35

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

5.0

0.91

5



05/27/22 03:35

10061 -02-6

Ethylbenzene

ND

ug/L

5.0

0.60

5



05/27/22 03:35

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

5.0

2.1

5



05/27/22 03:35

87-68-3

2-Hexanone

ND

ug/L

50.0

5.5

5



05/27/22 03:35

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

5.0

0.48

5



05/27/22 03:35

98-82-8

p-lsopropyltoluene

ND

ug/L

5.0

0.64

5



05/27/22 03:35

99-87-6

Methylene Chloride

ND

ug/L

5.0

2.0

5



05/27/22 03:35

75-09-2 L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

50.0

3.7

5



05/27/22 03:35

108-10-1

Methyl-tert-butyl ether

ND

ug/L

5.0

0.64

5



05/27/22 03:35

1634-04-4

Naphthalene

ND

ug/L

50.0

4.1

5



05/27/22 03:35

91-20-3

n-Propylbenzene

ND

ug/L

5.0

0.60

5



05/27/22 03:35

103-65-1

Styrene

ND

ug/L

5.0

0.62

5



05/27/22 03:35

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

5.0

0.42

5



05/27/22 03:35

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

5.0

0.77

5



05/27/22 03:35

79-34-5

Tetrachloroethene

ND

ug/L

5.0

1.6

5



05/27/22 03:35

127-18-4

Toluene

ND

ug/L

5.0

1.3

5



05/27/22 03:35

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

5.0

4.6

5



05/27/22 03:35

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

5.0

3.7

5



05/27/22 03:35

120-82-1

1,1,1-Trichloroethane

ND

ug/L

5.0

0.54

5



05/27/22 03:35

71-55-6

1,1,2-Trichloroethane

ND

ug/L

5.0

0.71

5



05/27/22 03:35

79-00-5

Trichloroethene

537

ug/L

5.0

1.0

5



05/27/22 03:35

79-01-6

Trichlorofluoromethane

ND

ug/L

5.0

0.82

5



05/27/22 03:35

75-69-4

1,2,3-Trichloropropane

ND

ug/L

12.5

2.0

5



05/27/22 03:35

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

5.0

1.6

5



05/27/22 03:35

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

5.0

0.45

5



05/27/22 03:35

108-67-8

Vinyl chloride

0.95J

ug/L

5.0

0.84

5



05/27/22 03:35

75-01-4

Xylene (Total)

ND

ug/L

15.0

1.4

5



05/27/22 03:35

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

97

%

80-120



5



05/27/22 03:35

460-00-4

Toluene-d8 (S)

102

%

80-120



5



05/27/22 03:35

2037-26-5

1,2-Dichlorobenzene-d4 (S)

102

' %

80-120



5



05/27/22 03:35

2199-69-1

Preservation pH

1.0

t

0.10



5



05/27/22 03:35



300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

17.4 mg/L	10.0

15.3 mg/L	10.0

5.3
5.5

10
10

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

1.4 mg/L	0.10 0.079

05/26/22 23:17 16887-00-6
05/26/22 23:17 14808-79-8

05/23/22 10:46 14797-55-8 H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 17 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849 y

Sample: FD-LIST A-05182022

Lab ID:

60400849007 Collected:

05/18/22 11:45

Received: 05/19/22 08:50 Matrix: Water



/





Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/23/22 18:34

74-84-0

L1

Ethene

ND

ug/L

10.0

7.1

1



05/23/22 18:34

74-85-1

L1

Methane

24.6

ug/L

10.0

5.5

1



05/23/22 18:34

74-82-8



6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010









Pace Analytical Services - Kansas City













Iron

42.9J

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:35

7439-89-6

B

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City







/





Acetone

S ND

ug/L

50.0

12.7

5



05/27/22 03:49

67-64-1



Benzene

ND

ug/L

5.0

0.68

5



05/27/22 03:49

71-43-2



Bromobenzene

ND

ug/L

5.0

0.44

5



05/27/22 03:49

108-86-1



Bromochloromethane

ND

ug/L

5.0

1.0

5



05/27/22 03:49

74-97-5



Bromodichloromethane

ND

ug/L

5.0

0.78

5



05/27/22 03:49

75-27-4



Bromoform

ND

ug/L

5.0

3.4

5



05/27/22 03:49

75-25-2



Bromomethane

ND

ug/L

25.0

2.3

5



05/27/22 03:49

74-83-9



2-Butanone (MEK)

ND

ug/L

50.0

4.9

5



05/27/22 03:49

78-93-3



n-Butylbenzene

ND

ug/L

5.0

0.76

5



05/27/22 03:49

104-51-8



sec-Butylbenzene

ND

ug/L

5.0

0.55

5



05/27/22 03:49

135-98-8



tert-Butylbenzene

ND

ug/L

5.0

0.60

5



05/27/22 03:49

98-06-6



Carbon disulfide

ND

ug/L

25.0

4.9

5



05/27/22 03:49

75-15-0



Carbon tetrachloride

ND

ug/L

5.0

0.86

5



05/27/22 03:49

56-23-5



Chlorobenzene

ND

ug/L

5.0

0.44

5



05/27/22 03:49

108-90-7



Chloroethane

ND

ug/L

5.0

1.9

5



05/27/22 03:49

75-00-3



Chloroform

ND

ug/L

5.0

1.1

5



05/27/22 03:49

67-66-3



Chloromethane

ND

ug/L

5.0

1.4

5



05/27/22 03:49

74-87-3



2-Chlorotoluene

ND

ug/L

5.0

0.54

5



05/27/22 03:49

95-49-8



4-Chlorotoluene

ND

ug/L

5.0

0.74

5



05/27/22 03:49

106-43-4



1,2-Dibromo-3-chloropropane

ND

ug/L

12.5

3.9

5



05/27/22 03:49

96-12-8



Dibromochloromethane

ND

ug/L

5.0

1.5

5



05/27/22 03:49

124-48-1



1,2-Dibromoethane (EDB)

ND

ug/L

5.0

0.98

5



05/27/22 03:49

106-93-4



Dibromomethane

ND

ug/L

5.0

0.54

5



05/27/22 03:49

74-95-3



1,2-Dichlorobenzene

ND

ug/L

5.0

0.62

5



05/27/22 03:49

95-50-1



1,3-Dichlorobenzene

ND

ug/L

5.0

0.66

5



05/27/22 03:49

541 -73-1



1,4-Dichlorobenzene

ND

ug/L

5.0

0.66

5



05/27/22 03:49

106-46-7



Dichlorodifluoromethane

ND

ug/L

5.0

1.0

5



05/27/22 03:49

75-71-8



1,1-Dichloroethane

ND

ug/L

5.0

0.61

5



05/27/22 03:49

75-34-3



1,2-Dichloroethane

ND

ug/L

5.0

1.1

5



05/27/22 03:49

107-06-2



1,2-Dichloroethene (Total)

108

ug/L

5.0

1.1

5



05/27/22 03:49

540-59-0



1,1-Dichloroethene

ND

ug/L

5.0

1.1

5



05/27/22 03:49

75-35-4



cis-1,2-Dichloroethene

105

ug/L

5.0

0.64

5



05/27/22 03:49

156-59-2



trans-1,2-Dichloroethene

3.2J

ug/L

5.0

0.51

5



05/27/22 03:49

156-60-5



1,2-Dichloropropane

ND

ug/L

5.0

0.70

5



05/27/22 03:49

78-87-5



1,3-Dichloropropane

ND

ug/L

5.0

0.52

5



05/27/22 03:49

142-28-9



REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 18 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FD-LIST A-05182022



Lab ID:

60400849007

Collected:

05/18/22 11:45

Received:

05/19/22 08:50 Matrix: Water











Report













Parameters



Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV



Analytical Method: EPA5030B/8260

















Pace Analytical Services

- Kansas City







/





2,2-Dichloropropane



if ND

ug/L

5.0

0.81

5



05/27/22 03:49

594-20-7



1,1-Dichloropropene



ND

ug/L

5.0

0.68

5



05/27/22 03:49

563-58-6



cis-1,3-Dichloropropene



ND

ug/L

5.0

0.39

5



05/27/22 03:49

10061 -01 -5



trans-1,3-Dichloropropene



ND

ug/L

5.0

0.91

5



05/27/22 03:49

10061 -02-6



Ethylbenzene



ND

ug/L

5.0

0.60

5



05/27/22 03:49

100-41-4



Hexachloro-1,3-butadiene



ND

ug/L

5.0

2.1

5



05/27/22 03:49

87-68-3



2-Hexanone



ND

ug/L

50.0

5.5

5



05/27/22 03:49

591 -78-6



Isopropylbenzene (Cumene)



ND

ug/L

5.0

0.48

5



05/27/22 03:49

98-82-8



p-lsopropyltoluene



ND

ug/L

5.0

0.64

5



05/27/22 03:49

99-87-6



Methylene Chloride



ND

ug/L

5.0

2.0

5



05/27/22 03:49

75-09-2

L1

4-Methyl-2-pentanone (MIBK)



ND

ug/L

50.0

3.7

5



05/27/22 03:49

108-10-1



Methyl-tert-butyl ether



ND

ug/L

5.0

0.64

5



05/27/22 03:49

1634-04-4



Naphthalene



ND

ug/L

50.0

4.1

5



05/27/22 03:49

91-20-3



n-Propylbenzene



ND

ug/L

5.0

0.60

5



05/27/22 03:49

103-65-1



Styrene



ND

ug/L

5.0

0.62

5



05/27/22 03:49

100-42-5



1,1,1,2-Tetrachloroethane



ND

ug/L

5.0

0.42

5



05/27/22 03:49

630-20-6



1,1,2,2-Tetrachloroethane



ND

ug/L

5.0

0.77

5



05/27/22 03:49

79-34-5



Tetrachloroethene



ND

ug/L

5.0

1.6

5



05/27/22 03:49

127-18-4



Toluene



ND

ug/L

5.0

1.3

5



05/27/22 03:49

108-88-3



1,2,3-Trichlorobenzene



ND

ug/L

5.0

4.6

5



05/27/22 03:49

87-61-6



1,2,4-Trichlorobenzene



ND

ug/L

5.0

3.7

5



05/27/22 03:49

120-82-1



1,1,1-Trichloroethane



ND

ug/L

5.0

0.54

5



05/27/22 03:49

71-55-6



1,1,2-Trichloroethane



ND

ug/L

5.0

0.71

5



05/27/22 03:49

79-00-5



Trichloroethene



520

ug/L

5.0

1.0

5



05/27/22 03:49

79-01-6



Trichlorofluoromethane



ND

ug/L

5.0

0.82

5



05/27/22 03:49

75-69-4



1,2,3-Trichloropropane



ND

ug/L

12.5

2.0

5



05/27/22 03:49

96-18-4



1,2,4-Trimethylbenzene



ND

ug/L

5.0

1.6

5



05/27/22 03:49

95-63-6



1,3,5-Trimethylbenzene



ND

ug/L

5.0

0.45

5



05/27/22 03:49

108-67-8



Vinyl chloride



ND

ug/L

5.0

0.84

5



05/27/22 03:49

75-01-4



Xylene (Total)



ND

ug/L

15.0

1.4

5



05/27/22 03:49

1330-20-7



Surrogates





















4-Bromofluorobenzene (S)



97

%

80-120



5



05/27/22 03:49

460-00-4



Toluene-d8 (S)



100

. %

80-120



5



05/27/22 03:49

2037-26-5



1,2-Dichlorobenzene-d4 (S)



100

[ %

80-120



5



05/27/22 03:49

2199-69-1



Preservation pH



1.0



0.10



5



05/27/22 03:49





300.0 IC Anions 28 Days



Analytical Method: EPA 300.0

















Pace Analytical Services

- Kansas City













Chloride



16.9

mg/L

10.0

5.3

10



05/26/22 23:45

16887-00-6

B

Sulfate



14.8

mg/L

10.0

5.5

10



05/26/22 23:45

14808-79-8



353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2

















Pace Analytical Services

- Kansas City













Nitrogen, Nitrate



1.4

mg/L

0.10

0.079

1



05/23/22 10:49

14797-55-8

H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 19 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: R1-MW9-W-17 ^

Lab ID:

60400849008

Collected:

05/18/22 12:40

Received: 05/19/22 08:50

Matrix: Water







Report









Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City









Acetone

if ND

ug/L

10.0

2.5 1

05/27/22 02

14

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/27/22 02

14

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 02

14

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 02

14

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 02

14

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 02

14

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 02

14

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 02

14

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 02

14

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 02

14

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 02

14

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 02

14

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 02

14

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 02

14

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 02

14

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 02

14

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 02

14

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 02

14

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 02

14

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 02

14

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 02

14

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 02

14

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 02

14

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 02

14

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02

14

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 02

14

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 02

14

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 02

14

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 02

14

107-06-2

1,2-Dichloroethene (Total)

0.28J

ug/L

1.0

0.22 1

05/27/22 02

14

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 02

14

75-35-4

cis-1,2-Dichloroethene

0.28J

ug/L

1.0

0.13 1

05/27/22 02

14

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 02

14

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 02

14

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 02

14

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 02

14

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 02

14

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 02

14

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 02

14

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 02

14

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/27/22 02

14

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/27/22 02

14

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/27/22 02

14

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/27/22 02

14

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/27/22 02

14

75-09-2 L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 20 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: R1-MW9-W-17 ^

Lab ID:

60400849008

Collected:

05/18/22 12:40

Received:

05/19/22 08:50

Matrix: Water









Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City





V





4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1



05/27/22 02

14

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1



05/27/22 02

14

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1



05/27/22 02

14

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1



05/27/22 02

14

103-65-1

Styrene



ND

ug/L

1.0

0.12 1



05/27/22 02

14

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1



05/27/22 02

14

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1



05/27/22 02

14

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1



05/27/22 02

14

127-18-4

Toluene



ND

ug/L

1.0

0.25 1



05/27/22 02

14

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1



05/27/22 02

14

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1



05/27/22 02

14

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1



05/27/22 02

14

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1



05/27/22 02

14

79-00-5

Trichloroethene



2.0

ug/L

1.0

0.21 1



05/27/22 02

14

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1



05/27/22 02

14

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1



05/27/22 02

14

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1



05/27/22 02

14

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1



05/27/22 02

14

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1



05/27/22 02

14

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1



05/27/22 02

14

1330-20-7

Surrogates



















4-Bromofluorobenzene (S)

/

97

%

80-120

1



05/27/22 02

14

460-00-4

Toluene-d8 (S)



101

%

80-120

1



05/27/22 02

14

2037-26-5

1,2-Dichlorobenzene-d4 (S)



106

/ %

80-120

1



05/27/22 02

14

2199-69-1

Preservation pH



1.0



0.10

1



05/27/22 02

14



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride



13.6

mg/L

10.0

5.3 10



05/27/22 00:41

16887-00-

Qual

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 21 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-34-W-17

Parameters

Lab ID: 60400849009 Collected: 05/18/22 14:25 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Ethane
Ethene
Methane

6010 MET ICP

Iron

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

ND
ND
ND

ug/L
ug/L
ug/L

10.0
10.0
10.0

3.8
7.1
5.5

05/23/22 18:56
05/23/22 18:56
05/23/22 18:56

74-84-0
74-85-1
74-82-8

Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Kansas City

921 ug/L	50.0	5.6 1

05/23/22 13:10 05/25/22 12:37 7439-89-6

8260 MSV

Analytical Method:

EPA 5030B/8260











Pace Analytical Services -

Kansas City





tr



Acetone

ND

ug/L



50.0

12.7

5

05/27/22 04:03

67-64-1

Benzene

ND

ug/L

UJ

5.0

0.68

5

05/27/22 04:03

71-43-2

Bromobenzene

ND

ug/L

UJ

5.0

0.44

5

05/27/22 04:03

108-86-1

Bromochloromethane

ND

ug/L



5.0

1.0

5

05/27/22 04:03

74-97-5

Bromodichloromethane

ND

ug/L



5.0

0.78

5

05/27/22 04:03

75-27-4

Bromoform

ND

ug/L



5.0

3.4

5

05/27/22 04:03

75-25-2

Bromomethane

ND

ug/L



25.0

2.3

5

05/27/22 04:03

74-83-9

2-Butanone (MEK)

ND

ug/L



50.0

4.9

5

05/27/22 04:03

78-93-3

n-Butylbenzene

ND

ug/L

UJ

5.0

0.76

5

05/27/22 04:03

104-51-8

sec-Butylbenzene

ND

ug/L

I

5.0

0.55

5

05/27/22 04:03

135-98-8

tert-Butylbenzene

ND

ug/L

V

5.0

0.60

5

05/27/22 04:03

98-06-6

Carbon disulfide

ND

ug/L



25.0

4.9

5

05/27/22 04:03

75-15-0

Carbon tetrachloride

ND

ug/L



5.0

0.86

5

05/27/22 04:03

56-23-5

Chlorobenzene

ND

ug/L

UJ

5.0

0.44

5

05/27/22 04:03

108-90-7

Chloroethane

ND

ug/L



5.0

1.9

5

05/27/22 04:03

75-00-3

Chloroform

ND

ug/L



5.0

1.1

5

05/27/22 04:03

67-66-3

Chloromethane

ND

ug/L



5.0

1.4

5

05/27/22 04:03

74-87-3

2-Chlorotoluene

ND

ug/L

UJ

5.0

0.54

5

05/27/22 04:03

95-49-8

4-Chlorotoluene

ND

ug/L

UJ

5.0

0.74

5

05/27/22 04:03

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L



12.5

3.9

5

05/27/22 04:03

96-12-8

Dibromochloromethane

ND

ug/L



5.0

1.5

5

05/27/22 04:03

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L



5.0

0.98

5

05/27/22 04:03

106-93-4

Dibromomethane

ND

ug/L



5.0

0.54

5

05/27/22 04:03

74-95-3

1,2-Dichlorobenzene

ND

ug/L

UJ

5.0

0.62

5

05/27/22 04:03

95-50-1

1,3-Dichlorobenzene

ND

ug/L

I

5.0

0.66

5

05/27/22 04:03

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

y

5.0

0.66

5

05/27/22 04:03

106-46-7

Dichlorodifluoromethane

ND

ug/L



5.0

1.0

5

05/27/22 04:03

75-71-8

1,1-Dichloroethane

ND

ug/L



5.0

0.61

5

05/27/22 04:03

75-34-3

1,2-Dichloroethane

ND

ug/L



5.0

1.1

5

05/27/22 04:03

107-06-2

1,2-Dichloroethene (Total)

226

ug/L



5.0

1.1

5

05/27/22 04:03

540-59-0

1,1-Dichloroethene

ND

ug/L



5.0

1.1

5

05/27/22 04:03

75-35-4

cis-1,2-Dichloroethene

221

ug/L



5.0

0.64

5

05/27/22 04:03

156-59-2

trans-1,2-Dichloroethene

4.9J

ug/L



5.0

0.51

5

05/27/22 04:03

156-60-5

1,2-Dichloropropane

ND

ug/L



5.0

0.70

5

05/27/22 04:03

78-87-5

1,3-Dichloropropane

ND

ug/L



5.0

0.52

5

05/27/22 04:03

142-28-9

L1
L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 22 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-34-W-17

Lab ID: 60400849009

Collected:

05/18/22 14:25

Received:

05/19/22 08:50 Matrix: Water









Report











Parameters

Results

Units



Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services

Kansas City











2,2-Dichloropropane

^ ND

ug/L



5.0

0.81

5



05/27/22 04:03

594-20-7

1,1-Dichloropropene

ND

ug/L



5.0

0.68

5



05/27/22 04:03

563-58-6

cis-1,3-Dichloropropene

ND

ug/L



5.0

0.39

5



05/27/22 04:03

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L



5.0

0.91

5



05/27/22 04:03

10061 -02-6

Ethylbenzene

ND

ug/L

UJ

5.0

0.60

5



05/27/22 04:03

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L



5.0

2.1

5



05/27/22 04:03

87-68-3

2-Hexanone

ND

ug/L



50.0

5.5

5



05/27/22 04:03

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

UJ

5.0

0.48

5



05/27/22 04:03

98-82-8

p-lsopropyltoluene

ND

ug/L

UJ

5.0

0.64

5



05/27/22 04:03

99-87-6

Methylene Chloride

ND

ug/L



5.0

2.0

5



05/27/22 04:03

75-09-2 L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L



50.0

3.7

5



05/27/22 04:03

108-10-1

Methyl-tert-butyl ether

ND

ug/L



5.0

0.64

5



05/27/22 04:03

1634-04-4

Naphthalene

ND

ug/L

UJ

50.0

4.1

5



05/27/22 04:03

91-20-3

n-Propylbenzene

ND

ug/L

UJ

5.0

0.60

5



05/27/22 04:03

103-65-1

Styrene

ND

ug/L



5.0

0.62

5



05/27/22 04:03

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L



5.0

0.42

5



05/27/22 04:03

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L



5.0

0.77

5



05/27/22 04:03

79-34-5

Tetrachloroethene

ND

ug/L



5.0

1.6

5



05/27/22 04:03

127-18-4

Toluene

ND

ug/L

UJ

5.0

1.3

5



05/27/22 04:03

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

I

5.0

4.6

5



05/27/22 04:03

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

y

5.0

3.7

5



05/27/22 04:03

120-82-1

1,1,1-Trichloroethane

ND

ug/L



5.0

0.54

5



05/27/22 04:03

71-55-6

1,1,2-Trichloroethane

ND

ug/L



5.0

0.71

5



05/27/22 04:03

79-00-5

Trichloroethene

582

ug/L



5.0

1.0

5



05/27/22 04:03

79-01-6

Trichlorofluoromethane

ND

ug/L



5.0

0.82

5



05/27/22 04:03

75-69-4

1,2,3-Trichloropropane

ND

ug/L



12.5

2.0

5



05/27/22 04:03

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

UJ

5.0

1.6

5



05/27/22 04:03

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

UJ

5.0

0.45

5



05/27/22 04:03

108-67-8

Vinyl chloride

2.9J

ug/L



5.0

0.84

5



05/27/22 04:03

75-01-4

Xylene (Total)

ND

ug/L

UJ

15.0

1.4

5



05/27/22 04:03

1330-20-7

Surrogates



















4-Bromofluorobenzene (S)

102

%



80-120



5



05/27/22 04:03

460-00-4

Toluene-d8 (S)

102

%



80-120



5



05/27/22 04:03

2037-26-5

1,2-Dichlorobenzene-d4 (S)

103 / %



80-120



5



05/27/22 04:03

2199-69-1

Preservation pH

6.0





0.10



5



05/27/22 04:03



300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

14.7 mg/L	10.0

10.1 mg/L	10.0

5.3
5.5

10
10

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.19 mg/L	0.10 0.079

05/27/22 01:08 16887-00-6
05/27/22 01:08 14808-79-8

05/23/22 10:50 14797-55-8 H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 23 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-36-W-17

Lab ID: 60400849010 Collected: 05/18/22 15:15 Received: 05/19/22 08:50 Matrix: Water
Report

Parameters

Results

Units

Limit

VIDL

DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8

1



05/23/22 19:17

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/23/22 19:17

74-85-1

Methane

7.8J

ug/L

10.0

5.5

1



05/23/22 19:17

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

: EPA 3010







Pace Analytical Services - Kansas City











Iron

3250

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:39

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City







~



Acetone

W ND

ug/L

100

25.4

10



05/27/22 04:30

67-64-1

Benzene

ND

ug/L

10.0

1.4

10



05/27/22 04:30

71-43-2

Bromobenzene

ND

ug/L

10.0

0.88

10



05/27/22 04:30

108-86-1

Bromochloromethane

ND

ug/L

10.0

2.0

10



05/27/22 04:30

74-97-5

Bromodichloromethane

ND

ug/L

10.0

1.6

10



05/27/22 04:30

75-27-4

Bromoform

ND

ug/L

10.0

6.8

10



05/27/22 04:30

75-25-2

Bromomethane

ND

ug/L

50.0

4.6

10



05/27/22 04:30

74-83-9

2-Butanone (MEK)

ND

ug/L

100

9.8

10



05/27/22 04:30

78-93-3

n-Butylbenzene

ND

ug/L

10.0

1.5

10



05/27/22 04:30

104-51-8

sec-Butylbenzene

ND

ug/L

10.0

1.1

10



05/27/22 04:30

135-98-8

tert-Butylbenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:30

98-06-6

Carbon disulfide

ND

ug/L

50.0

9.8

10



05/27/22 04:30

75-15-0

Carbon tetrachloride

ND

ug/L

10.0

1.7

10



05/27/22 04:30

56-23-5

Chlorobenzene

ND

ug/L

10.0

0.89

10



05/27/22 04:30

108-90-7

Chloroethane

ND

ug/L

10.0

3.7

10



05/27/22 04:30

75-00-3

Chloroform

ND

ug/L

10.0

2.2

10



05/27/22 04:30

67-66-3

Chloromethane

ND

ug/L

10.0

2.8

10



05/27/22 04:30

74-87-3

2-Chlorotoluene

ND

ug/L

10.0

1.1

10



05/27/22 04:30

95-49-8

4-Chlorotoluene

ND

ug/L

10.0

1.5

10



05/27/22 04:30

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

25.0

7.8

10



05/27/22 04:30

96-12-8

Dibromochloromethane

ND

ug/L

10.0

3.0

10



05/27/22 04:30

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

10.0

2.0

10



05/27/22 04:30

106-93-4

Dibromomethane

ND

ug/L

10.0

1.1

10



05/27/22 04:30

74-95-3

1,2-Dichlorobenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:30

95-50-1

1,3-Dichlorobenzene

ND

ug/L

10.0

1.3

10



05/27/22 04:30

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

10.0

1.3

10



05/27/22 04:30

106-46-7

Dichlorodifluoromethane

ND

ug/L

10.0

2.0

10



05/27/22 04:30

75-71-8

1,1-Dichloroethane

ND

ug/L

10.0

1.2

10



05/27/22 04:30

75-34-3

1,2-Dichloroethane

ND

ug/L

10.0

2.1

10



05/27/22 04:30

107-06-2

1,2-Dichloroethene (Total)

174

ug/L

10.0

2.2

10



05/27/22 04:30

540-59-0

1,1-Dichloroethene

ND

ug/L

10.0

2.2

10



05/27/22 04:30

75-35-4

cis-1,2-Dichloroethene

168

ug/L

10.0

1.3

10



05/27/22 04:30

156-59-2

trans-1,2-Dichloroethene

6.5J

ug/L

10.0

1.0

10



05/27/22 04:30

156-60-5

1,2-Dichloropropane

ND

ug/L

10.0

1.4

10



05/27/22 04:30

78-87-5

1,3-Dichloropropane

ND

ug/L

10.0

1.0

10



05/27/22 04:30

142-28-9

Qual

L1
L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 24 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-36-W-17 ^

Lab ID

60400849010

Collected:

05/18/22 15:15

Received:

05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

^ ND

ug/L

10.0

1.6

10



05/27/22 04:30

594-20-7

1,1-Dichloropropene

ND

ug/L

10.0

1.4

10



05/27/22 04:30

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

10.0

0.78

10



05/27/22 04:30

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

10.0

1.8

10



05/27/22 04:30

10061 -02-6

Ethylbenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:30

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

10.0

4.2

10



05/27/22 04:30

87-68-3

2-Hexanone

ND

ug/L

100

11.0

10



05/27/22 04:30

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

10.0

0.97

10



05/27/22 04:30

98-82-8

p-lsopropyltoluene

ND

ug/L

10.0

1.3

10



05/27/22 04:30

99-87-6

Methylene Chloride

ND

ug/L

10.0

3.9

10



05/27/22 04:30

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

100

7.4

10



05/27/22 04:30

108-10-1

Methyl-tert-butyl ether

ND

ug/L

10.0

1.3

10



05/27/22 04:30

1634-04-4

Naphthalene

ND

ug/L

100

8.2

10



05/27/22 04:30

91-20-3

n-Propylbenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:30

103-65-1

Styrene

ND

ug/L

10.0

1.2

10



05/27/22 04:30

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

10.0

0.84

10



05/27/22 04:30

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

10.0

1.5

10



05/27/22 04:30

79-34-5

Tetrachloroethene

ND

ug/L

10.0

3.3

10



05/27/22 04:30

127-18-4

Toluene

ND

ug/L

10.0

2.5

10



05/27/22 04:30

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

10.0

9.3

10



05/27/22 04:30

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

10.0

7.3

10



05/27/22 04:30

120-82-1

1,1,1-Trichloroethane

ND

ug/L

10.0

1.1

10



05/27/22 04:30

71-55-6

1,1,2-Trichloroethane

ND

ug/L

10.0

1.4

10



05/27/22 04:30

79-00-5

Trichloroethene

455

ug/L

10.0

2.1

10



05/27/22 04:30

79-01-6

Trichlorofluoromethane

ND

ug/L

10.0

1.6

10



05/27/22 04:30

75-69-4

1,2,3-Trichloropropane

ND

ug/L

25.0

4.1

10



05/27/22 04:30

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

10.0

3.2

10



05/27/22 04:30

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

10.0

0.90

10



05/27/22 04:30

108-67-8

Vinyl chloride

ND

ug/L

10.0

1.7

10



05/27/22 04:30

75-01-4

Xylene (Total)

ND

ug/L

30.0

2.8

10



05/27/22 04:30

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

94

%

80-120



10



05/27/22 04:30

460-00-4

Toluene-d8 (S)

99

/ %

80-120



10



05/27/22 04:30

2037-26-5

1,2-Dichlorobenzene-d4 (S)

99

' %

80-120



10



05/27/22 04:30

2199-69-1

Preservation pH

1.0

"""

0.10



10



05/27/22 04:30



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

13.2

mg/L

10.0

5.3

10



05/26/22 17:47

16887-00-6

Sulfate

11.8

mg/L

10.0

5.5

10



05/26/22 17:47

14808-79-8

Qual

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.18 mg/L	0.10 0.079

L1

05/23/22 10:51 14797-55-8 H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 25 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

^L.

Sample: FAG-73-W-17 ^

Lab ID: 60400849011 Collected: 05/18/22 15:40 Received: 05/19/22 08:50 Matrix: Water
Report

Parameters

Results

Units

Limit

VIDL

DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

14.1

ug/L

10.0

3.8

1



05/24/22 19:01

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/24/22 19:01

74-85-1

Methane

558

ug/L

10.0

5.5

1



05/24/22 19:01

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010







Pace Analytical Services - Kansas City











Iron

4010

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22 12:41

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City







~



Acetone

ND

ug/L

10.0

2.5

1



05/27/22 03:22

67-64-1

Benzene

ND

ug/L

1.0

0.14

1



05/27/22 03:22

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



05/27/22 03:22

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



05/27/22 03:22

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



05/27/22 03:22

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



05/27/22 03:22

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



05/27/22 03:22

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



05/27/22 03:22

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



05/27/22 03:22

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



05/27/22 03:22

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 03:22

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



05/27/22 03:22

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



05/27/22 03:22

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



05/27/22 03:22

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



05/27/22 03:22

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



05/27/22 03:22

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



05/27/22 03:22

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



05/27/22 03:22

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



05/27/22 03:22

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



05/27/22 03:22

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



05/27/22 03:22

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



05/27/22 03:22

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



05/27/22 03:22

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



05/27/22 03:22

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/27/22 03:22

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



05/27/22 03:22

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



05/27/22 03:22

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



05/27/22 03:22

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



05/27/22 03:22

107-06-2

1,2-Dichloroethene (Total)

46.8

ug/L

1.0

0.22

1



05/27/22 03:22

540-59-0

1,1-Dichloroethene

1.2

ug/L

1.0

0.22

1



05/27/22 03:22

75-35-4

cis-1,2-Dichloroethene

44.2

ug/L

1.0

0.13

1



05/27/22 03:22

156-59-2

trans-1,2-Dichloroethene

2.6

ug/L

1.0

0.10

1



05/27/22 03:22

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



05/27/22 03:22

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



05/27/22 03:22

142-28-9

Qual

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 26 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-73-W-17 ^

Lab ID: 60400849011

Collected:

05/18/22 15:40

Received:

05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City











2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



05/27/22 03:22

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



05/27/22 03:22

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



05/27/22 03:22

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



05/27/22 03:22

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 03:22

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



05/27/22 03:22

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



05/27/22 03:22

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



05/27/22 03:22

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



05/27/22 03:22

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



05/27/22 03:22

75-09-2 L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



05/27/22 03:22

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



05/27/22 03:22

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



05/27/22 03:22

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



05/27/22 03:22

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



05/27/22 03:22

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



05/27/22 03:22

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



05/27/22 03:22

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



05/27/22 03:22

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



05/27/22 03:22

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



05/27/22 03:22

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



05/27/22 03:22

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



05/27/22 03:22

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



05/27/22 03:22

79-00-5

Trichloroethene

22.8

ug/L

1.0

0.21

1



05/27/22 03:22

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



05/27/22 03:22

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



05/27/22 03:22

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



05/27/22 03:22

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



05/27/22 03:22

108-67-8

Vinyl chloride

11.0

ug/L

1.0

0.17

1



05/27/22 03:22

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



05/27/22 03:22

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

98

%

80-120



1



05/27/22 03:22

460-00-4

Toluene-d8 (S)

101

%

80-120



1



05/27/22 03:22

2037-26-5

1,2-Dichlorobenzene-d4 (S)

101 '

%

80-120



1



05/27/22 03:22

2199-69-1

Preservation pH

1.0 ^



0.10



1



05/27/22 03:22



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

16.2

mg/L

10.0

5.3

10



05/26/22 18:14

16887-00-6

Sulfate

12.2

mg/L

10.0

5.5

10



05/26/22 18:14

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

ND mg/L	0.10 0.079 1

05/23/22 10:52 14797-55-8 H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 27 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-32-W-17

Lab ID:

60400849012 Collected:

05/18/22 16:50

Received: 05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8 1



05/24/22

19:22

74-84-0

Ethene

ND

ug/L

10.0

7.1 1



05/24/22

19:22

74-85-1

Methane

ND

ug/L

10.0

5.5 1



05/24/22

19:22

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method: EPA 3010









Pace Analytical Services - Kansas City











Iron

1380

ug/L

50.0

5.6 1

05/23/22 13:10

05/25/22

12:43

7439-89-6

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City





+





Acetone

W ND

ug/L

10.0

2.5 1



05/31/22

15:09

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



05/31/22

15:09

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



05/31/22

15:09

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



05/31/22

15:09

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



05/31/22

15:09

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



05/31/22

15:09

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



05/31/22

15:09

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



05/31/22

15:09

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



05/31/22

15:09

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



05/31/22

15:09

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



05/31/22

15:09

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



05/31/22

15:09

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



05/31/22

15:09

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



05/31/22

15:09

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



05/31/22

15:09

75-00-3 L1

Chloroform

ND

ug/L

1.0

0.22 1



05/31/22

15:09

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



05/31/22

15:09

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



05/31/22

15:09

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



05/31/22

15:09

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



05/31/22

15:09

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



05/31/22

15:09

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



05/31/22

15:09

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



05/31/22

15:09

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



05/31/22

15:09

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/31/22

15:09

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



05/31/22

15:09

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



05/31/22

15:09

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



05/31/22

15:09

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



05/31/22

15:09

107-06-2

1,2-Dichloroethene (Total)

12.5

ug/L

1.0

0.22 1



05/31/22

15:09

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



05/31/22

15:09

75-35-4

cis-1,2-Dichloroethene

12.3

ug/L

1.0

0.13 1



05/31/22

15:09

156-59-2

trans-1,2-Dichloroethene

0.17J

ug/L

1.0

0.10 1



05/31/22

15:09

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



05/31/22

15:09

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



05/31/22

15:09

142-28-9

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 28 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-32-W-17

Lab ID:

60400849012

Collected:

05/18/22 16:50

Received:

05/19/22 08:50 Matrix: Water









Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

- Kansas City













2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



05/31/22 15:09

594-20-7



1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



05/31/22 15:09

563-58-6



cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



05/31/22 15:09

10061 -01 -5



trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



05/31/22 15:09

10061 -02-6



Ethylbenzene

ND

ug/L

1.0

0.12

1



05/31/22 15:09

100-41-4



Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



05/31/22 15:09

87-68-3



2-Hexanone

ND

ug/L

10.0

1.1

1



05/31/22 15:09

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



05/31/22 15:09

98-82-8



p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



05/31/22 15:09

99-87-6



Methylene Chloride

ND

ug/L

1.0

0.39

1



05/31/22 15:09

75-09-2

L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



05/31/22 15:09

108-10-1



Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



05/31/22 15:09

1634-04-4



Naphthalene

ND

ug/L

10.0

0.82

1



05/31/22 15:09

91-20-3



n-Propylbenzene

ND

ug/L

1.0

0.12

1



05/31/22 15:09

103-65-1



Styrene

ND

ug/L

1.0

0.12

1



05/31/22 15:09

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



05/31/22 15:09

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



05/31/22 15:09

79-34-5



Tetrachloroethene

ND

ug/L

1.0

0.33

1



05/31/22 15:09

127-18-4



Toluene

ND

ug/L

1.0

0.25

1



05/31/22 15:09

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



05/31/22 15:09

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



05/31/22 15:09

120-82-1



1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



05/31/22 15:09

71-55-6



1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



05/31/22 15:09

79-00-5



Trichloroethene

49.5

ug/L

1.0

0.21

1



05/31/22 15:09

79-01-6



Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



05/31/22 15:09

75-69-4



1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



05/31/22 15:09

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



05/31/22 15:09

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



05/31/22 15:09

108-67-8



Vinyl chloride

0.21J

ug/L

1.0

0.17

1



05/31/22 15:09

75-01-4



Xylene (Total)

ND

ug/L

3.0

0.28

1



05/31/22 15:09

1330-20-7



Surrogates



















4-Bromofluorobenzene (S)

V 104

%

80-120



1



05/31/22 15:09

460-00-4



Toluene-d8 (S)

w 96

%

80-120



1



05/31/22 15:09

2037-26-5



1,2-Dichlorobenzene-d4 (S)

100

%

80-120



1



05/31/22 15:09

2199-69-1



Preservation pH

1.0



0.10



1



05/31/22 15:09





300.0 IC Anions 28 Days

Analytical Method: EPA 300.0















Pace Analytical Services

- Kansas City













Chloride

4.5

mg/L

1.0

0.53

1



05/27/22 12:08

16887-00-6



Sulfate

16.0

mg/L

1.0

0.55

1



05/27/22 12:08

14808-79-8



353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2















Pace Analytical Services

- Kansas City













Nitrogen, Nitrate

0.62

mg/L

0.10

0.079

1



05/23/22 10:53

14797-55-8

H1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 29 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-AW4-W-17 ^

Lab ID:

60400849013

Collected:

05/18/22 17:00

Received:

05/19/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

RSK 175 Headspace

Analytical Method: RSK 175 Modified













Pace Analytical Services

- Indianapolis











Ethane

ND

ug/L

10.0

3.8

1



05/24/22 19:43

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/24/22 19:43

74-85-1

Methane

52.8

ug/L

10.0

5.5

1



05/24/22 19:43

74-82-8

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City







/



Acetone

ND

ug/L

100

25.4

10



05/27/22 04:43

67-64-1

Benzene

ND

ug/L

10.0

1.4

10



05/27/22 04:43

71-43-2

Bromobenzene

ND

ug/L

10.0

0.88

10



05/27/22 04:43

108-86-1

Bromochloromethane

ND

ug/L

10.0

2.0

10



05/27/22 04:43

74-97-5

Bromodichloromethane

ND

ug/L

10.0

1.6

10



05/27/22 04:43

75-27-4

Bromoform

ND

ug/L

10.0

6.8

10



05/27/22 04:43

75-25-2

Bromomethane

ND

ug/L

50.0

4.6

10



05/27/22 04:43

74-83-9

2-Butanone (MEK)

ND

ug/L

100

9.8

10



05/27/22 04:43

78-93-3

n-Butylbenzene

ND

ug/L

10.0

1.5

10



05/27/22 04:43

104-51-8

sec-Butylbenzene

ND

ug/L

10.0

1.1

10



05/27/22 04:43

135-98-8

tert-Butylbenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:43

98-06-6

Carbon disulfide

ND

ug/L

50.0

9.8

10



05/27/22 04:43

75-15-0

Carbon tetrachloride

ND

ug/L

10.0

1.7

10



05/27/22 04:43

56-23-5

Chlorobenzene

ND

ug/L

10.0

0.89

10



05/27/22 04:43

108-90-7

Chloroethane

ND

ug/L

10.0

3.7

10



05/27/22 04:43

75-00-3

Chloroform

ND

ug/L

10.0

2.2

10



05/27/22 04:43

67-66-3

Chloromethane

ND

ug/L

10.0

2.8

10



05/27/22 04:43

74-87-3

2-Chlorotoluene

ND

ug/L

10.0

1.1

10



05/27/22 04:43

95-49-8

4-Chlorotoluene

ND

ug/L

10.0

1.5

10



05/27/22 04:43

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L UJ

25.0

7.8

10



05/27/22 04:43

96-12-8

Dibromochloromethane

ND

ug/L

10.0

3.0

10



05/27/22 04:43

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

10.0

2.0

10



05/27/22 04:43

106-93-4

Dibromomethane

ND

ug/L

10.0

1.1

10



05/27/22 04:43

74-95-3

1,2-Dichlorobenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:43

95-50-1

1,3-Dichlorobenzene

ND

ug/L

10.0

1.3

10



05/27/22 04:43

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

10.0

1.3

10



05/27/22 04:43

106-46-7

Dichlorodifluoromethane

ND

ug/L

10.0

2.0

10



05/27/22 04:43

75-71-8

1,1-Dichloroethane

ND

ug/L

10.0

1.2

10



05/27/22 04:43

75-34-3

1,2-Dichloroethane

ND

ug/L

10.0

2.1

10



05/27/22 04:43

107-06-2

1,2-Dichloroethene (Total)

275

ug/L

10.0

2.2

10



05/27/22 04:43

540-59-0

1,1-Dichloroethene

ND

ug/L

10.0

2.2

10



05/27/22 04:43

75-35-4

cis-1,2-Dichloroethene

268

ug/L

10.0

1.3

10



05/27/22 04:43

156-59-2

trans-1,2-Dichloroethene

7.6J

ug/L

10.0

1.0

10



05/27/22 04:43

156-60-5

1,2-Dichloropropane

ND

ug/L

10.0

1.4

10



05/27/22 04:43

78-87-5

1,3-Dichloropropane

ND

ug/L

10.0

1.0

10



05/27/22 04:43

142-28-9

2,2-Dichloropropane

ND

ug/L

10.0

1.6

10



05/27/22 04:43

594-20-7

1,1-Dichloropropene

ND

ug/L

10.0

1.4

10



05/27/22 04:43

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

10.0

0.78

10



05/27/22 04:43

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

10.0

1.8

10



05/27/22 04:43

10061 -02-6

Qual

M1.R1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 30 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: FAG-AW4-W-17

Lab ID:

60400849013

Collected:

05/18/22 17:00

Received:

05/19/22 08:50 Matrix: Water









Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

Kansas City







V





Ethylbenzene

^ ND

ug/L

10.0

1.2

10



05/27/22 04:43

100-41-4



Hexachloro-1,3-butadiene

ND

ug/L

10.0

4.2

10



05/27/22 04:43

87-68-3



2-Hexanone

ND

ug/L

100

11.0

10



05/27/22 04:43

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L

10.0

0.97

10



05/27/22 04:43

98-82-8



p-lsopropyltoluene

ND

ug/L

10.0

1.3

10



05/27/22 04:43

99-87-6



Methylene Chloride

ND

ug/L

10.0

3.9

10



05/27/22 04:43

75-09-2

L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

100

7.4

10



05/27/22 04:43

108-10-1



Methyl-tert-butyl ether

ND

ug/L

10.0

1.3

10



05/27/22 04:43

1634-04-4



Naphthalene

ND

ug/L

100

8.2

10



05/27/22 04:43

91-20-3



n-Propylbenzene

ND

ug/L

10.0

1.2

10



05/27/22 04:43

103-65-1



Styrene

ND

ug/L

10.0

1.2

10



05/27/22 04:43

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

10.0

0.84

10



05/27/22 04:43

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

10.0

1.5

10



05/27/22 04:43

79-34-5



Tetrachloroethene

ND

ug/L

10.0

3.3

10



05/27/22 04:43

127-18-4



Toluene

ND

ug/L

10.0

2.5

10



05/27/22 04:43

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

10.0

9.3

10



05/27/22 04:43

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

10.0

7.3

10



05/27/22 04:43

120-82-1



1,1,1-Trichloroethane

ND

ug/L

10.0

1.1

10



05/27/22 04:43

71-55-6



1,1,2-Trichloroethane

ND

ug/L

10.0

1.4

10



05/27/22 04:43

79-00-5



Trichloroethene

1160

ug/L

10.0

2.1

10



05/27/22 04:43

79-01-6

M1

Trichlorofluoromethane

ND

ug/L

10.0

1.6

10



05/27/22 04:43

75-69-4



1,2,3-Trichloropropane

ND

ug/L

25.0

4.1

10



05/27/22 04:43

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

10.0

3.2

10



05/27/22 04:43

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

10.0

0.90

10



05/27/22 04:43

108-67-8



Vinyl chloride

28.5

ug/L

10.0

1.7

10



05/27/22 04:43

75-01-4



Xylene (Total)

ND

ug/L

30.0

2.8

10



05/27/22 04:43

1330-20-7



Surrogates



















4-Bromofluorobenzene (S)

94

%

80-120



10



05/27/22 04:43

460-00-4



Toluene-d8 (S)

100

%

80-120



10



05/27/22 04:43

2037-26-5



1,2-Dichlorobenzene-d4 (S)

102

% •

80-120



10



05/27/22 04:43

2199-69-1



Preservation pH

1.0



0.10



10



05/27/22 04:43





300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

16.2 mg/L	10.0

18.1 mg/L	10.0

5.3
5.5

10
10

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

1.3 mg/L	0.10 0.079

05/26/22 19:37 16887-00-6
05/26/22 19:37 14808-79-8

05/23/22 10:53 14797-55-8 H1

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 31 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849 j

Sample: TB-01-051822 ^

Lab ID:

60400849014

Collected:

05/18/22 17:43

Received: 05/19/22 08:50 Matrix: Water







Report







Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260









Pace Analytical Services

Kansas City



+



Acetone

ND

ug/L

10.0

2.5 1

05/27/22 00:52

67-64-1

Benzene

~ nd

ug/L

1.0

0.14 1

05/27/22 00:52

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 00:52

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 00:52

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 00:52

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 00:52

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 00:52

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 00:52

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 00:52

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 00:52

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 00:52

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 00:52

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 00:52

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 00:52

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 00:52

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 00:52

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 00:52

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 00:52

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 00:52

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 00:52

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 00:52

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 00:52

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 00:52

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 00:52

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 00:52

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 00:52

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 00:52

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 00:52

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 00:52

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1

05/27/22 00:52

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 00:52

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1

05/27/22 00:52

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 00:52

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 00:52

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 00:52

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 00:52

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 00:52

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 00:52

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 00:52

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 00:52

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/27/22 00:52

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/27/22 00:52

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/27/22 00:52

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/27/22 00:52

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/27/22 00:52

75-09-2 L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 32 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: TB-01-051822

Parameters

Lab ID: 60400849014 Collected: 05/18/22 17:43 Received: 05/19/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

05/27/22 00:52

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

05/27/22 00:52

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

05/27/22 00:52

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

05/27/22 00:52

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

05/27/22 00:52

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

05/27/22 00:52

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

05/27/22 00:52

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

05/27/22 00:52

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

05/27/22 00:52

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

05/27/22 00:52

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

05/27/22 00:52

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

05/27/22 00:52

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

05/27/22 00:52

79-00-5

Trichloroethene



ND

ug/L

1.0

0.21 1

05/27/22 00:52

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

05/27/22 00:52

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

05/27/22 00:52

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

05/27/22 00:52

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

05/27/22 00:52

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

05/27/22 00:52

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

05/27/22 00:52

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

*

98

%

80-120

1

05/27/22 00:52

460-00-4

Toluene-d8 (S)



100

%

80-120

1

05/27/22 00:52

2037-26-5

1,2-Dichlorobenzene-d4 (S)



102

%

80-120

1

05/27/22 00:52

2199-69-1

Preservation pH



1.0 ^



0.10

1

05/27/22 00:52



Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 33 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: TB-02-051822 ^

Lab ID:

60400849015

Collected:

05/18/22 17:49

Received: 05/19/22 08:50

Matrix: Water







Report









Parameters

Results

Units

Limit

MDL DF

Prepared Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City



/





Acetone

W ND

ug/L

10.0

2.5 1

05/27/22 01

05

67-64-1

Benzene

ND

ug/L

1.0

0.14 1

05/27/22 01

05

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1

05/27/22 01

05

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1

05/27/22 01

05

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1

05/27/22 01

05

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1

05/27/22 01

05

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1

05/27/22 01

05

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1

05/27/22 01

05

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1

05/27/22 01

05

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1

05/27/22 01

05

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 01

05

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1

05/27/22 01

05

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1

05/27/22 01

05

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1

05/27/22 01

05

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1

05/27/22 01

05

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1

05/27/22 01

05

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1

05/27/22 01

05

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1

05/27/22 01

05

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1

05/27/22 01

05

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1

05/27/22 01

05

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1

05/27/22 01

05

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1

05/27/22 01

05

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1

05/27/22 01

05

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1

05/27/22 01

05

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 01

05

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1

05/27/22 01

05

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1

05/27/22 01

05

75-71-8

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1

05/27/22 01

05

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1

05/27/22 01

05

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1

05/27/22 01

05

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1

05/27/22 01

05

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1

05/27/22 01

05

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1

05/27/22 01

05

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1

05/27/22 01

05

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1

05/27/22 01

05

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1

05/27/22 01

05

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1

05/27/22 01

05

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1

05/27/22 01

05

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1

05/27/22 01

05

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1

05/27/22 01

05

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1

05/27/22 01

05

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1

05/27/22 01

05

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1

05/27/22 01

05

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1

05/27/22 01

05

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1

05/27/22 01

05

75-09-2 L1

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 34 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Sample: TB-02-051822 ^

Lab ID:

60400849015

Collected:

05/18/22 17:49

Received:

05/19/22 08:50

Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





~





4-Methyl-2-pentanone (MIBK)

i/* ND

ug/L

10.0

0.74 1



05/27/22 01

05

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



05/27/22 01

05

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



05/27/22 01

05

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



05/27/22 01

05

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



05/27/22 01

05

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



05/27/22 01

05

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



05/27/22 01

05

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



05/27/22 01

05

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



05/27/22 01

05

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



05/27/22 01

05

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



05/27/22 01

05

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



05/27/22 01

05

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



05/27/22 01

05

79-00-5

Trichloroethene

ND

ug/L

1.0

0.21 1



05/27/22 01

05

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



05/27/22 01

05

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



05/27/22 01

05

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



05/27/22 01

05

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



05/27/22 01

05

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



05/27/22 01

05

75-01-4

Xylene (Total)

ND

/ug/L

3.0

0.28 1



05/27/22 01

05

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

96

%

80-120

1



05/27/22 01

05

460-00-4

Toluene-d8 (S)

99

/ %

80-120

1



05/27/22 01

05

2037-26-5

1,2-Dichlorobenzene-d4 (S)

104

' %

80-120

1



05/27/22 01

05

2199-69-1

Preservation pH

1.0

/

0.10

1



05/27/22 01

05



Qual

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 35 of 61


-------
C. PACE PROJECT NUMBER 60400877


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-50-W-17

Parameters

Lab ID: 60400877001 Collected: 05/19/22 08:46 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method: RSK 175 Modified



Pace Analytical Services - Indianapolis









Ethane

ND

ug/L

10.0

3.8

1

05/25/22 01:46

74-84-0

Ethene

ND

ug/L

10.0

7.1

1

05/25/22 01:46

74-85-1

Methane

ND

ug/L

10.0

5.5

1

05/25/22 01:46

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Methoc

: EPA 3010







Pace Analytical Services - Kansas City









Iron

23800

ug/L

150

16.9

3 05/23/22 13:10

05/25/22 13:21

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260











Pace Analytical Services - Kansas City





¦ ^



Acetone

ND

ug/L

250

63.5

25

05/31/22 17:40

67-64-1

Benzene

ND

ug/L

25.0

3.4

25

05/31/22 17:40

71-43-2

Bromobenzene

ND

ug/L

25.0

2.2

25

05/31/22 17:40

108-86-1

Bromochloromethane

ND

ug/L

25.0

5.0

25

05/31/22 17:40

74-97-5

Bromodichloromethane

ND

ug/L

25.0

3.9

25

05/31/22 17:40

75-27-4

Bromoform

ND

ug/L

25.0

16.9

25

05/31/22 17:40

75-25-2

Bromomethane

ND

ug/L

125

11.5

25

05/31/22 17:40

74-83-9

2-Butanone (MEK)

ND

ug/L

250

24.4

25

05/31/22 17:40

78-93-3

n-Butylbenzene

ND

ug/L

25.0

3.8

25

05/31/22 17:40

104-51-8

sec-Butylbenzene

ND

ug/L

25.0

2.8

25

05/31/22 17:40

135-98-8

tert-Butylbenzene

ND

ug/L

25.0

3.0

25

05/31/22 17:40

98-06-6

Carbon disulfide

ND

ug/L

125

24.4

25

05/31/22 17:40

75-15-0

Carbon tetrachloride

ND

ug/L

25.0

4.3

25

05/31/22 17:40

56-23-5

Chlorobenzene

ND

ug/L

25.0

2.2

25

05/31/22 17:40

108-90-7

Chloroethane

ND

ug/L

25.0

9.4

25

05/31/22 17:40

75-00-3

Chloroform

ND

ug/L

25.0

5.5

25

05/31/22 17:40

67-66-3

Chloromethane

ND

ug/L

25.0

7.1

25

05/31/22 17:40

74-87-3

2-Chlorotoluene

ND

ug/L

25.0

2.7

25

05/31/22 17:40

95-49-8

4-Chlorotoluene

ND

ug/L

25.0

3.7

25

05/31/22 17:40

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

62.5

19.5

25

05/31/22 17:40

96-12-8

Dibromochloromethane

ND

ug/L

25.0

7.6

25

05/31/22 17:40

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

25.0

4.9

25

05/31/22 17:40

106-93-4

Dibromomethane

ND

ug/L

25.0

2.7

25

05/31/22 17:40

74-95-3

1,2-Dichlorobenzene

ND

ug/L

25.0

3.1

25

05/31/22 17:40

95-50-1

1,3-Dichlorobenzene

ND

ug/L

25.0

3.3

25

05/31/22 17:40

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

25.0

3.3

25

05/31/22 17:40

106-46-7

Dichlorodifluoromethane

ND

ug/L

25.0

5.0

25

05/31/22 17:40

75-71-8

1,1-Dichloroethane

ND

ug/L

25.0

3.0

25

05/31/22 17:40

75-34-3

1,2-Dichloroethane

ND

ug/L

25.0

5.3

25

05/31/22 17:40

107-06-2

1,2-Dichloroethene (Total)

157

ug/L

25.0

5.6

25

05/31/22 17:40

540-59-0

1,1-Dichloroethene

ND

ug/L

25.0

5.5

25

05/31/22 17:40

75-35-4

cis-1,2-Dichloroethene

157

ug/L

25.0

3.2

25

05/31/22 17:40

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

25.0

2.6

25

05/31/22 17:40

156-60-5

1,2-Dichloropropane

ND

ug/L

25.0

3.5

25

05/31/22 17:40

78-87-5

1,3-Dichloropropane

ND

ug/L

25.0

2.6

25

05/31/22 17:40

142-28-9

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 6 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-50-W-17

Lab ID:

60400877001

Collected:

05/19/22 08:46

Received:

05/20/22 08:50 Matrix: Water







Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

Kansas City







/





2,2-Dichloropropane

^ ND

ug/L

25.0

4.0

25



05/31/22

17:40

594-20-7

1,1-Dichloropropene

ND

ug/L

25.0

3.4

25



05/31/22

17:40

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

25.0

1.9

25



05/31/22

17:40

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

25.0

4.6

25



05/31/22

17:40

10061 -02-6

Ethylbenzene

ND

ug/L

25.0

3.0

25



05/31/22

17:40

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

25.0

10.4

25



05/31/22

17:40

87-68-3

2-Hexanone

ND

ug/L

250

27.5

25



05/31/22

17:40

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

25.0

2.4

25



05/31/22

17:40

98-82-8

p-lsopropyltoluene

ND

ug/L

25.0

3.2

25



05/31/22

17:40

99-87-6

Methylene Chloride

23.1J

J ug/L

25.0

9.8

25



05/31/22

17:40

75-09-2 L1

4-Methyl-2-pentanone (MIBK)

ND

ug/L

250

18.4

25



05/31/22

17:40

108-10-1

Methyl-tert-butyl ether

ND

ug/L

25.0

3.2

25



05/31/22

17:40

1634-04-4

Naphthalene

ND

ug/L

250

20.6

25



05/31/22

17:40

91-20-3

n-Propylbenzene

ND

ug/L

25.0

3.0

25



05/31/22

17:40

103-65-1

Styrene

ND

ug/L

25.0

3.1

25



05/31/22

17:40

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

25.0

2.1

25



05/31/22

17:40

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

25.0

3.8

25



05/31/22

17:40

79-34-5

Tetrachloroethene

ND

ug/L

25.0

8.2

25



05/31/22

17:40

127-18-4

Toluene

ND

ug/L

25.0

6.3

25



05/31/22

17:40

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

25.0

23.2

25



05/31/22

17:40

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

25.0

18.3

25



05/31/22

17:40

120-82-1

1,1,1-Trichloroethane

ND

ug/L

25.0

2.7

25



05/31/22

17:40

71-55-6

1,1,2-Trichloroethane

5.4J

ug/L

25.0

3.6

25



05/31/22

17:40

79-00-5

Trichloroethene

2050

ug/L

25.0

5.2

25



05/31/22

17:40

79-01-6

Trichlorofluoromethane

ND

ug/L

25.0

4.1

25



05/31/22

17:40

75-69-4

1,2,3-Trichloropropane

ND

ug/L

62.5

10.2

25



05/31/22

17:40

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

25.0

8.1

25



05/31/22

17:40

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

25.0

2.2

25



05/31/22

17:40

108-67-8

Vinyl chloride

ND

ug/L

25.0

4.2

25



05/31/22

17:40

75-01-4

Xylene (Total)

ND

ug/L

75.0

7.0

25



05/31/22

17:40

1330-20-7

Surrogates



















4-Bromofluorobenzene (S)

97

%

80-120



25



05/31/22

17:40

460-00-4

Toluene-d8 (S)

100

%

80-120



25



05/31/22

17:40

2037-26-5

1,2-Dichlorobenzene-d4 (S)

101

%

80-120



25



05/31/22

17:40

2199-69-1

Preservation pH

1.0

•

0.10



25



05/31/22

17:40



300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

9.8 mg/L	1.0

7.3 mg/L	1.0

0.53
0.55

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.39 mg/L	0.10 0.079

05/27/22 17:26 16887-00-6
05/27/22 17:26 14808-79-8

05/20/22 17:01 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 7 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-31-W-17

Parameters

Lab ID: 60400877002 Collected: 05/19/22 09:25 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Ethane
Ethene
Methane

6010 MET ICP

Iron

8260 MSV

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

ND
ND
ND

ug/L
ug/L
ug/L

10.0
10.0
10.0

3.8
7.1
5.5

05/25/22 02:07
05/25/22 02:07
05/25/22 02:07

74-84-0
74-85-1
74-82-8

Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Kansas City

188 ug/L	50.0	5.6 1

Analytical Method: EPA5030B/8260

05/23/22 13:10 05/25/22 13:03 7439-89-6



Pace Analytical Services -

Kansas City









Acetone

ND

ug/L

100

25.4

10

05/31/22 17:53

67-64-1

Benzene

ND

ug/L

10.0

1.4

10

05/31/22 17:53

71-43-2

Bromobenzene

ND

ug/L

10.0

0.88

10

05/31/22 17:53

108-86-1

Bromochloromethane

ND

ug/L

10.0

2.0

10

05/31/22 17:53

74-97-5

Bromodichloromethane

ND

ug/L

10.0

1.6

10

05/31/22 17:53

75-27-4

Bromoform

ND

ug/L

10.0

6.8

10

05/31/22 17:53

75-25-2

Bromomethane

ND

ug/L

50.0

4.6

10

05/31/22 17:53

74-83-9

2-Butanone (MEK)

ND

ug/L

100

9.8

10

05/31/22 17:53

78-93-3

n-Butylbenzene

ND

ug/L

10.0

1.5

10

05/31/22 17:53

104-51-8

sec-Butylbenzene

ND

ug/L

10.0

1.1

10

05/31/22 17:53

135-98-8

tert-Butylbenzene

ND

ug/L

10.0

1.2

10

05/31/22 17:53

98-06-6

Carbon disulfide

ND

ug/L

50.0

9.8

10

05/31/22 17:53

75-15-0

Carbon tetrachloride

ND

ug/L

10.0

1.7

10

05/31/22 17:53

56-23-5

Chlorobenzene

ND

ug/L

10.0

0.89

10

05/31/22 17:53

108-90-7

Chloroethane

ND

ug/L

10.0

3.7

10

05/31/22 17:53

75-00-3

Chloroform

ND

ug/L

10.0

2.2

10

05/31/22 17:53

67-66-3

Chloromethane

ND

ug/L

10.0

2.8

10

05/31/22 17:53

74-87-3

2-Chlorotoluene

ND

ug/L

10.0

1.1

10

05/31/22 17:53

95-49-8

4-Chlorotoluene

ND

ug/L

10.0

1.5

10

05/31/22 17:53

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

25.0

7.8

10

05/31/22 17:53

96-12-8

Dibromochloromethane

ND

ug/L

10.0

3.0

10

05/31/22 17:53

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

10.0

2.0

10

05/31/22 17:53

106-93-4

Dibromomethane

ND

ug/L

10.0

1.1

10

05/31/22 17:53

74-95-3

1,2-Dichlorobenzene

ND

ug/L

10.0

1.2

10

05/31/22 17:53

95-50-1

1,3-Dichlorobenzene

ND

ug/L

10.0

1.3

10

05/31/22 17:53

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

10.0

1.3

10

05/31/22 17:53

106-46-7

Dichlorodifluoromethane

ND

ug/L

10.0

2.0

10

05/31/22 17:53

75-71-8

1,1-Dichloroethane

ND

ug/L

10.0

1.2

10

05/31/22 17:53

75-34-3

1,2-Dichloroethane

ND

ug/L

10.0

2.1

10

05/31/22 17:53

107-06-2

1,2-Dichloroethene (Total)

215

ug/L

10.0

2.2

10

05/31/22 17:53

540-59-0

1,1-Dichloroethene

ND

ug/L

10.0

2.2

10

05/31/22 17:53

75-35-4

cis-1,2-Dichloroethene

210

ug/L

10.0

1.3

10

05/31/22 17:53

156-59-2

trans-1,2-Dichloroethene

4.1J

ug/L

10.0

1.0

10

05/31/22 17:53

156-60-5

1,2-Dichloropropane

ND

ug/L

10.0

1.4

10

05/31/22 17:53

78-87-5

1,3-Dichloropropane

ND

ug/L

10.0

1.0

10

05/31/22 17:53

142-28-9

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 8 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-31-W-17

Lab ID: 60400877002

Collected:

05/19/22 09:25

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City







~



2,2-Dichloropropane

if ND

ug/L

10.0

1.6

10



05/31/22 17:53

594-20-7

1,1-Dichloropropene

ND

ug/L

10.0

1.4

10



05/31/22 17:53

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

10.0

0.78

10



05/31/22 17:53

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

10.0

1.8

10



05/31/22 17:53

10061 -02-6

Ethylbenzene

ND

ug/L

10.0

1.2

10



05/31/22 17:53

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

10.0

4.2

10



05/31/22 17:53

87-68-3

2-Hexanone

ND

ug/L

100

11.0

10



05/31/22 17:53

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

10.0

0.97

10



05/31/22 17:53

98-82-8

p-lsopropyltoluene

ND

ug/L

10.0

1.3

10



05/31/22 17:53

99-87-6

Methylene Chloride

12.9

J ug/L

10.0

3.9

10



05/31/22 17:53

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

100

7.4

10



05/31/22 17:53

108-10-1

Methyl-tert-butyl ether

ND

ug/L

10.0

1.3

10



05/31/22 17:53

1634-04-4

Naphthalene

ND

ug/L

100

8.2

10



05/31/22 17:53

91-20-3

n-Propylbenzene

ND

ug/L

10.0

1.2

10



05/31/22 17:53

103-65-1

Styrene

ND

ug/L

10.0

1.2

10



05/31/22 17:53

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

10.0

0.84

10



05/31/22 17:53

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

10.0

1.5

10



05/31/22 17:53

79-34-5

Tetrachloroethene

ND

ug/L

10.0

3.3

10



05/31/22 17:53

127-18-4

Toluene

ND

ug/L

10.0

2.5

10



05/31/22 17:53

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

10.0

9.3

10



05/31/22 17:53

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

10.0

7.3

10



05/31/22 17:53

120-82-1

1,1,1-Trichloroethane

ND

ug/L

10.0

1.1

10



05/31/22 17:53

71-55-6

1,1,2-Trichloroethane

ND

ug/L

10.0

1.4

10



05/31/22 17:53

79-00-5

Trichloroethene

726

ug/L

10.0

2.1

10



05/31/22 17:53

79-01-6

Trichlorofluoromethane

ND

ug/L

10.0

1.6

10



05/31/22 17:53

75-69-4

1,2,3-Trichloropropane

ND

ug/L

25.0

4.1

10



05/31/22 17:53

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

10.0

3.2

10



05/31/22 17:53

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

10.0

0.90

10



05/31/22 17:53

108-67-8

Vinyl chloride

ND

ug/L

10.0

1.7

10



05/31/22 17:53

75-01-4

Xylene (Total)

ND

ug/L

30.0

2.8

10



05/31/22 17:53

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

^ 96

%

80-120



10



05/31/22 17:53

460-00-4

Toluene-d8 (S)

100

%

80-120



10



05/31/22 17:53

2037-26-5

1,2-Dichlorobenzene-d4 (S)

102

/ %

80-120



10



05/31/22 17:53

2199-69-1

Preservation pH

1.0



0.10



10



05/31/22 17:53



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

11.7

mg/L

1.0

0.53

1



05/27/22 17:40

16887-00-6

Sulfate

7.5

mg/L

1.0

0.55

1



05/27/22 17:40

14808-79-8

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

0.85

mg/L

0.10

0.079

1



05/20/22 17:02

14797-55-8

Qual

C9.L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 9 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877



Sample: FAG-85-W-17

Parameters

Lab ID: 60400877003 Collected: 05/19/22 10:17 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

Ethane

ND

ug/L

10.0

3.8

1

05/25/22

14:32

74-84-0

Ethene

8.9J

ug/L

10.0

7.1

1

05/25/22

14:32

74-85-1

Methane

619

ug/L

10.0

5.5

1

05/25/22

14:32

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010









Pace Analytical Services - Kansas City











Iron

9650

ug/L

50.0

5.6

1 05/23/22 13:10

05/25/22

13:05

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City





/





Acetone

ND

ug/L

50.0

12.7

5

06/01/22

15:47

67-64-1

Benzene

ND

ug/L

5.0

0.68

5

06/01/22

15:47

71-43-2

Bromobenzene

ND

ug/L

5.0

0.44

5

06/01/22

15:47

108-86-1

Bromochloromethane

ND

ug/L

5.0

1.0

5

06/01/22

15:47

74-97-5

Bromodichloromethane

ND

ug/L

5.0

0.78

5

06/01/22

15:47

75-27-4

Bromoform

ND

ug/L

5.0

3.4

5

06/01/22

15:47

75-25-2

Bromomethane

ND

ug/L

25.0

2.3

5

06/01/22

15:47

74-83-9

2-Butanone (MEK)

ND

ug/L

50.0

4.9

5

06/01/22

15:47

78-93-3

n-Butylbenzene

ND

ug/L

5.0

0.76

5

06/01/22

15:47

104-51-8

sec-Butylbenzene

ND

ug/L

5.0

0.55

5

06/01/22

15:47

135-98-8

tert-Butylbenzene

ND

ug/L

5.0

0.60

5

06/01/22

15:47

98-06-6

Carbon disulfide

ND

ug/L

25.0

4.9

5

06/01/22

15:47

75-15-0

Carbon tetrachloride

ND

ug/L

5.0

0.86

5

06/01/22

15:47

56-23-5

Chlorobenzene

ND

ug/L

5.0

0.44

5

06/01/22

15:47

108-90-7

Chloroethane

ND

ug/L

5.0

1.9

5

06/01/22

15:47

75-00-3

Chloroform

ND

ug/L

5.0

1.1

5

06/01/22

15:47

67-66-3

Chloromethane

ND

ug/L

5.0

1.4

5

06/01/22

15:47

74-87-3

2-Chlorotoluene

ND

ug/L

5.0

0.54

5

06/01/22

15:47

95-49-8

4-Chlorotoluene

ND

ug/L

5.0

0.74

5

06/01/22

15:47

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

12.5

3.9

5

06/01/22

15:47

96-12-8

Dibromochloromethane

ND

ug/L

5.0

1.5

5

06/01/22

15:47

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

5.0

0.98

5

06/01/22

15:47

106-93-4

Dibromomethane

ND

ug/L

5.0

0.54

5

06/01/22

15:47

74-95-3

1,2-Dichlorobenzene

ND

ug/L

5.0

0.62

5

06/01/22

15:47

95-50-1

1,3-Dichlorobenzene

ND

ug/L

5.0

0.66

5

06/01/22

15:47

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

5.0

0.66

5

06/01/22

15:47

106-46-7

Dichlorodifluoromethane

ND

ug/L

5.0

1.0

5

06/01/22

15:47

75-71-8

1,1-Dichloroethane

ND

ug/L

5.0

0.61

5

06/01/22

15:47

75-34-3

1,2-Dichloroethane

ND

ug/L

5.0

1.1

5

06/01/22

15:47

107-06-2

1,2-Dichloroethene (Total)

373

ug/L

5.0

1.1

5

06/01/22

15:47

540-59-0

1,1-Dichloroethene

43.1

ug/L

5.0

1.1

5

06/01/22

15:47

75-35-4

cis-1,2-Dichloroethene

367

ug/L

5.0

0.64

5

06/01/22

15:47

156-59-2

trans-1,2-Dichloroethene

5.1

ug/L

5.0

0.51

5

06/01/22

15:47

156-60-5

1,2-Dichloropropane

ND

ug/L

5.0

0.70

5

06/01/22

15:47

78-87-5

1,3-Dichloropropane

ND

ug/L

5.0

0.52

5

06/01/22

15:47

142-28-9

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 10 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-85-W-17

Lab ID:

60400877003

Collected:

05/19/22 10:17

Received:

05/20/22 08:50 Matrix: Water



T





Report















Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260

















Pace Analytical Services

Kansas City















2,2-Dichloropropane

V ND

ug/L

5.0

0.81

5



06/01/22

15:47

594-20-7



1,1-Dichloropropene

ND

ug/L

5.0

0.68

5



06/01/22

15:47

563-58-6



cis-1,3-Dichloropropene

ND

ug/L

5.0

0.39

5



06/01/22

15:47

10061 -01 -5



trans-1,3-Dichloropropene

ND

ug/L

5.0

0.91

5



06/01/22

15:47

10061 -02-6



Ethylbenzene

ND

ug/L

5.0

0.60

5



06/01/22

15:47

100-41-4



Hexachloro-1,3-butadiene

ND

ug/L

5.0

2.1

5



06/01/22

15:47

87-68-3



2-Hexanone

ND

ug/L

50.0

5.5

5



06/01/22

15:47

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L

5.0

0.48

5



06/01/22

15:47

98-82-8



p-lsopropyltoluene

ND

ug/L

5.0

0.64

5



06/01/22

15:47

99-87-6



Methylene Chloride

ND

ug/L

5.0

2.0

5



06/01/22

15:47

75-09-2



4-Methyl-2-pentanone (MIBK)

ND

ug/L

50.0

3.7

5



06/01/22

15:47

108-10-1



Methyl-tert-butyl ether

ND

ug/L

5.0

0.64

5



06/01/22

15:47

1634-04-4



Naphthalene

ND

ug/L

50.0

4.1

5



06/01/22

15:47

91-20-3



n-Propylbenzene

ND

ug/L

5.0

0.60

5



06/01/22

15:47

103-65-1



Styrene

ND

ug/L

5.0

0.62

5



06/01/22

15:47

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

5.0

0.42

5



06/01/22

15:47

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

5.0

0.77

5



06/01/22

15:47

79-34-5



Tetrachloroethene

ND

ug/L

5.0

1.6

5



06/01/22

15:47

127-18-4



Toluene

ND

ug/L

5.0

1.3

5



06/01/22

15:47

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

5.0

4.6

5



06/01/22

15:47

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

5.0

3.7

5



06/01/22

15:47

120-82-1



1,1,1-Trichloroethane

ND

ug/L

5.0

0.54

5



06/01/22

15:47

71-55-6



1,1,2-Trichloroethane

ND

ug/L

5.0

0.71

5



06/01/22

15:47

79-00-5



Trichloroethene

252

ug/L

5.0

1.0

5



06/01/22

15:47

79-01-6



Trichlorofluoromethane

ND

ug/L

5.0

0.82

5



06/01/22

15:47

75-69-4



1,2,3-Trichloropropane

ND

ug/L

12.5

2.0

5



06/01/22

15:47

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

5.0

1.6

5



06/01/22

15:47

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

5.0

0.45

5



06/01/22

15:47

108-67-8



Vinyl chloride

53.8

ug/L

5.0

0.84

5



06/01/22

15:47

75-01-4



Xylene (Total)

ND

ug/L

15.0

1.4

5



06/01/22

15:47

1330-20-7



Surrogates





















4-Bromofluorobenzene (S)

105

%

80-120



5



06/01/22

15:47

460-00-4



Toluene-d8 (S)

97

%

80-120



5



06/01/22

15:47

2037-26-5



1,2-Dichlorobenzene-d4 (S)

101 y

%

80-120



5



06/01/22

15:47

2199-69-1



Preservation pH

1.0 -



0.10



5



06/01/22

15:47





300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

12.8 mg/L	1.0 0.53

12.4 mg/L	1.0 0.55

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.17 mg/L	0.10 0.079

05/27/22 18:07 16887-00-6
05/27/22 18:07 14808-79-8

05/20/22 17:03 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 11 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-22-W-17

Parameters

Lab ID: 60400877004 Collected: 05/19/22 11:20 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

RSK 175 Headspace

Ethane
Ethene
Methane

6010 MET ICP

Iron

8260 MSV

Analytical Method: RSK 175 Modified
Pace Analytical Services - Indianapolis

ND
ND
29.6

ug/L
ug/L
ug/L

10.0
10.0
10.0

3.8
7.1
5.5

05/25/22 15:14
05/25/22 15:14
05/25/22 15:14

74-84-0
74-85-1
74-82-8

Analytical Method: EPA 6010 Preparation Method: EPA 3010
Pace Analytical Services - Kansas City

124 ug/L	50.0	5.6 1

Analytical Method: EPA5030B/8260

05/23/22 13:10 05/25/22 13:15 7439-89-6

.#•

Pace Analytical Services -

Kansas City





/



w

Acetone

41.7J

ug/L

100

25.4

10

06/01/22 15:33

67-64-1

Benzene

ND

ug/L

10.0

1.4

10

06/01/22 15:33

71-43-2

Bromobenzene

ND

ug/L

10.0

0.88

10

06/01/22 15:33

108-86-1

Bromochloromethane

ND

ug/L

10.0

2.0

10

06/01/22 15:33

74-97-5

Bromodichloromethane

ND

ug/L

10.0

1.6

10

06/01/22 15:33

75-27-4

Bromoform

ND

ug/L

10.0

6.8

10

06/01/22 15:33

75-25-2

Bromomethane

ND

ug/L

50.0

4.6

10

06/01/22 15:33

74-83-9

2-Butanone (MEK)

ND

ug/L

100

9.8

10

06/01/22 15:33

78-93-3

n-Butylbenzene

ND

ug/L

10.0

1.5

10

06/01/22 15:33

104-51-8

sec-Butylbenzene

ND

ug/L

10.0

1.1

10

06/01/22 15:33

135-98-8

tert-Butylbenzene

ND

ug/L

10.0

1.2

10

06/01/22 15:33

98-06-6

Carbon disulfide

ND

ug/L

50.0

9.8

10

06/01/22 15:33

75-15-0

Carbon tetrachloride

ND

ug/L

10.0

1.7

10

06/01/22 15:33

56-23-5

Chlorobenzene

ND

ug/L

10.0

0.89

10

06/01/22 15:33

108-90-7

Chloroethane

ND

ug/L

10.0

3.7

10

06/01/22 15:33

75-00-3

Chloroform

2.3J

ug/L

10.0

2.2

10

06/01/22 15:33

67-66-3

Chloromethane

ND

ug/L

10.0

2.8

10

06/01/22 15:33

74-87-3

2-Chlorotoluene

ND

ug/L

10.0

1.1

10

06/01/22 15:33

95-49-8

4-Chlorotoluene

ND

ug/L

10.0

1.5

10

06/01/22 15:33

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

25.0

7.8

10

06/01/22 15:33

96-12-8

Dibromochloromethane

ND

ug/L

10.0

3.0

10

06/01/22 15:33

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

10.0

2.0

10

06/01/22 15:33

106-93-4

Dibromomethane

ND

ug/L

10.0

1.1

10

06/01/22 15:33

74-95-3

1,2-Dichlorobenzene

ND

ug/L

10.0

1.2

10

06/01/22 15:33

95-50-1

1,3-Dichlorobenzene

ND

ug/L

10.0

1.3

10

06/01/22 15:33

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

10.0

1.3

10

06/01/22 15:33

106-46-7

Dichlorodifluoromethane

ND

ug/L

10.0

2.0

10

06/01/22 15:33

75-71-8

1,1-Dichloroethane

ND

ug/L

10.0

1.2

10

06/01/22 15:33

75-34-3

1,2-Dichloroethane

ND

ug/L

10.0

2.1

10

06/01/22 15:33

107-06-2

1,2-Dichloroethene (Total)

211

ug/L

10.0

2.2

10

06/01/22 15:33

540-59-0

1,1-Dichloroethene

2.4J

ug/L

10.0

2.2

10

06/01/22 15:33

75-35-4

cis-1,2-Dichloroethene

206

ug/L

10.0

1.3

10

06/01/22 15:33

156-59-2

trans-1,2-Dichloroethene

4.5J

ug/L

10.0

1.0

10

06/01/22 15:33

156-60-5

1,2-Dichloropropane

ND

ug/L

10.0

1.4

10

06/01/22 15:33

78-87-5

1,3-Dichloropropane

ND

ug/L

10.0

1.0

10

06/01/22 15:33

142-28-9

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 12 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-22-W-17

Lab ID:

60400877004

Collected:

05/19/22 11:20

Received:

05/20/22 08:50 Matrix: Water

T





Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City







/



2,2-Dichloropropane

~ ND

ug/L

10.0

1.6

10



06/01/22 15:33

594-20-7

1,1-Dichloropropene

ND

ug/L

10.0

1.4

10



06/01/22 15:33

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

10.0

0.78

10



06/01/22 15:33

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

10.0

1.8

10



06/01/22 15:33

10061 -02-6

Ethylbenzene

ND

ug/L

10.0

1.2

10



06/01/22 15:33

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

10.0

4.2

10



06/01/22 15:33

87-68-3

2-Hexanone

ND

ug/L

100

11.0

10



06/01/22 15:33

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

10.0

0.97

10



06/01/22 15:33

98-82-8

p-lsopropyltoluene

ND

ug/L

10.0

1.3

10



06/01/22 15:33

99-87-6

Methylene Chloride

ND

ug/L

10.0

3.9

10



06/01/22 15:33

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

100

7.4

10



06/01/22 15:33

108-10-1

Methyl-tert-butyl ether

ND

ug/L

10.0

1.3

10



06/01/22 15:33

1634-04-4

Naphthalene

ND

ug/L

100

8.2

10



06/01/22 15:33

91-20-3

n-Propylbenzene

ND

ug/L

10.0

1.2

10



06/01/22 15:33

103-65-1

Styrene

ND

ug/L

10.0

1.2

10



06/01/22 15:33

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

10.0

0.84

10



06/01/22 15:33

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

10.0

1.5

10



06/01/22 15:33

79-34-5

Tetrachloroethene

ND

ug/L

10.0

3.3

10



06/01/22 15:33

127-18-4

Toluene

ND

ug/L

10.0

2.5

10



06/01/22 15:33

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

10.0

9.3

10



06/01/22 15:33

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

10.0

7.3

10



06/01/22 15:33

120-82-1

1,1,1-Trichloroethane

ND

ug/L

10.0

1.1

10



06/01/22 15:33

71-55-6

1,1,2-Trichloroethane

ND

ug/L

10.0

1.4

10



06/01/22 15:33

79-00-5

Trichloroethene

379

ug/L

10.0

2.1

10



06/01/22 15:33

79-01-6

Trichlorofluoromethane

ND

ug/L

10.0

1.6

10



06/01/22 15:33

75-69-4

1,2,3-Trichloropropane

ND

ug/L

25.0

4.1

10



06/01/22 15:33

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

10.0

3.2

10



06/01/22 15:33

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

10.0

0.90

10



06/01/22 15:33

108-67-8

Vinyl chloride

30.8

ug/L

10.0

1.7

10



06/01/22 15:33

75-01-4

Xylene (Total)

ND

ug/L

30.0

2.8

10



06/01/22 15:33

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

103

%

80-120



10



06/01/22 15:33

460-00-4

Toluene-d8 (S)

98

%

80-120



10



06/01/22 15:33

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100'

%

80-120



10



06/01/22 15:33

2199-69-1

Preservation pH

1.0 ^

0.10



10



06/01/22 15:33



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

24.1

mg/L

2.0

1.1

2



05/28/22 12:26

16887-00-6

Sulfate

18.0

mg/L

1.0

0.55

1



05/27/22 19:31

14808-79-8

Qual

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

1.5 mg/L	0.10 0.079

05/20/22 17:05 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 13 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877



Sample: FAG-88-W-17 y.

Lab ID:

60400877005 Collected:

05/19/22 14:00

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified













Pace Analytical Services - Indianapolis











Ethane

ND

ug/L

10.0

3.8

1



05/25/22 15:36

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/25/22 15:36

74-85-1

Methane

ND

ug/L

10.0

5.5

1



05/25/22 15:36

74-82-8

8260 MSV

Analytical Method:

EPA 5030B/8260













Pace Analytical Services - Kansas City







/



Acetone

S ND

ug/L

10.0

2.5

1



06/01/22 14:39

67-64-1

Benzene

ND

ug/L

1.0

0.14

1



06/01/22 14:39

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



06/01/22 14:39

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



06/01/22 14:39

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



06/01/22 14:39

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



06/01/22 14:39

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



06/01/22 14:39

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



06/01/22 14:39

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



06/01/22 14:39

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



06/01/22 14:39

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 14:39

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



06/01/22 14:39

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



06/01/22 14:39

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



06/01/22 14:39

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



06/01/22 14:39

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



06/01/22 14:39

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



06/01/22 14:39

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



06/01/22 14:39

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



06/01/22 14:39

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



06/01/22 14:39

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



06/01/22 14:39

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



06/01/22 14:39

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



06/01/22 14:39

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



06/01/22 14:39

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 14:39

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22 14:39

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



06/01/22 14:39

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



06/01/22 14:39

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



06/01/22 14:39

107-06-2

1,2-Dichloroethene (Total)

1.6

ug/L

1.0

0.22

1



06/01/22 14:39

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22

1



06/01/22 14:39

75-35-4

cis-1,2-Dichloroethene

1.6

ug/L

1.0

0.13

1



06/01/22 14:39

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10

1



06/01/22 14:39

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



06/01/22 14:39

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



06/01/22 14:39

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



06/01/22 14:39

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



06/01/22 14:39

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



06/01/22 14:39

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



06/01/22 14:39

10061 -02-6

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 14 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-88-W-17 ^

Lab ID:

60400877005

Collected:

05/19/22 14:00

Received:

05/20/22 08:50 Matrix: Water



~





Report













Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260















Pace Analytical Services

Kansas City





/







Ethylbenzene

^ nd

ug/L

1.0

0.12 1



06/01/22

14:39

100-41-4



Hexachloro-1,3-butadiene

w ND

ug/L

1.0

0.42 1



06/01/22

14:39

87-68-3



2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22

14:39

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22

14:39

98-82-8



p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22

14:39

99-87-6



Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22

14:39

75-09-2



4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1



06/01/22

14:39

108-10-1



Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



06/01/22

14:39

1634-04-4



Naphthalene

ND

ug/L

10.0

0.82 1



06/01/22

14:39

91-20-3



n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

14:39

103-65-1



Styrene

ND

ug/L

1.0

0.12 1



06/01/22

14:39

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22

14:39

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22

14:39

79-34-5



Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22

14:39

127-18-4



Toluene

ND

ug/L

1.0

0.25 1



06/01/22

14:39

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22

14:39

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22

14:39

120-82-1



1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22

14:39

71-55-6



1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22

14:39

79-00-5



Trichloroethene

7.0

ug/L

1.0

0.21 1



06/01/22

14:39

79-01-6



Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22

14:39

75-69-4



1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22

14:39

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22

14:39

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22

14:39

108-67-8



Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22

14:39

75-01-4



Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22

14:39

1330-20-7



Surrogates



















4-Bromofluorobenzene (S)

106

%

80-120

1



06/01/22

14:39

460-00-4



Toluene-d8 (S)

99

%

80-120

1



06/01/22

14:39

2037-26-5



1,2-Dichlorobenzene-d4 (S)

102

%

80-120

1



06/01/22

14:39

2199-69-1



Preservation pH

1.0



0.10

1



06/01/22

14:39





300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

6.2 mg/L	1.0 0.53

10.1 mg/L	1.0 0.55

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.73 mg/L	0.10 0.079 1

05/27/22 19:44 16887-00-6
05/27/22 19:44 14808-79-8

05/21/22 10:29 14797-55-8

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 15 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877



Sample: FAG-89-W-17

Lab ID:

60400877006 Collected:

05/19/22 15:10

Received:

05/20/22 08:50 Matrix: Water







Report













Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No. Qual

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/25/22

15:57

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/25/22

15:57

74-85-1

Methane

ND

ug/L

10.0

5.5

1



05/25/22

15:57

74-82-8

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City







~





Acetone

ND

ug/L

10.0

2.5

1



06/01/22

14:52

67-64-1

Benzene

ND

ug/L

1.0

0.14

1



06/01/22

14:52

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088

1



06/01/22

14:52

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20

1



06/01/22

14:52

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16

1



06/01/22

14:52

75-27-4

Bromoform

ND

ug/L

1.0

0.68

1



06/01/22

14:52

75-25-2

Bromomethane

ND

ug/L

5.0

0.46

1



06/01/22

14:52

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98

1



06/01/22

14:52

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15

1



06/01/22

14:52

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11

1



06/01/22

14:52

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12

1



06/01/22

14:52

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98

1



06/01/22

14:52

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17

1



06/01/22

14:52

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089

1



06/01/22

14:52

108-90-7

Chloroethane

ND

ug/L

1.0

0.37

1



06/01/22

14:52

75-00-3

Chloroform

ND

ug/L

1.0

0.22

1



06/01/22

14:52

67-66-3

Chloromethane

ND

ug/L

1.0

0.28

1



06/01/22

14:52

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11

1



06/01/22

14:52

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15

1



06/01/22

14:52

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78

1



06/01/22

14:52

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30

1



06/01/22

14:52

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20

1



06/01/22

14:52

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11

1



06/01/22

14:52

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12

1



06/01/22

14:52

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22

14:52

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13

1



06/01/22

14:52

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20

1



06/01/22

14:52

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12

1



06/01/22

14:52

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21

1



06/01/22

14:52

107-06-2

1,2-Dichloroethene (Total)

1.3

ug/L

1.0

0.22

1



06/01/22

14:52

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22

1



06/01/22

14:52

75-35-4

cis-1,2-Dichloroethene

1.3

ug/L

1.0

0.13

1



06/01/22

14:52

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10

1



06/01/22

14:52

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14

1



06/01/22

14:52

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10

1



06/01/22

14:52

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16

1



06/01/22

14:52

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14

1



06/01/22

14:52

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078

1



06/01/22

14:52

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18

1



06/01/22

14:52

10061 -02-6

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 16 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-89-W-17

Lab ID:

60400877006

Collected:

05/19/22 15:10

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

- Kansas City







~



Ethylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 14:52

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42

1



06/01/22 14:52

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1

1



06/01/22 14:52

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097

1



06/01/22 14:52

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13

1



06/01/22 14:52

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39

1



06/01/22 14:52

75-09-2

4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74

1



06/01/22 14:52

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13

1



06/01/22 14:52

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82

1



06/01/22 14:52

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12

1



06/01/22 14:52

103-65-1

Styrene

ND

ug/L

1.0

0.12

1



06/01/22 14:52

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084

1



06/01/22 14:52

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15

1



06/01/22 14:52

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33

1



06/01/22 14:52

127-18-4

Toluene

ND

ug/L

1.0

0.25

1



06/01/22 14:52

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93

1



06/01/22 14:52

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73

1



06/01/22 14:52

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11

1



06/01/22 14:52

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14

1



06/01/22 14:52

79-00-5

Trichloroethene

8.6

ug/L

1.0

0.21

1



06/01/22 14:52

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16

1



06/01/22 14:52

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41

1



06/01/22 14:52

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32

1



06/01/22 14:52

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090

1



06/01/22 14:52

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17

1



06/01/22 14:52

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28

1



06/01/22 14:52

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

~ 108

%

80-120



1



06/01/22 14:52

460-00-4

Toluene-d8 (S)

98

%

80-120



1



06/01/22 14:52

2037-26-5

1,2-Dichlorobenzene-d4 (S)

102 '

%

80-120



1



06/01/22 14:52

2199-69-1

Preservation pH

1.0 ^

~

0.10



1



06/01/22 14:52



300.0 IC Anions 28 Days

Analytical Method: EPA 300.0













Pace Analytical Services

- Kansas City











Chloride

4.9

mg/L

1.0

0.53

1



05/27/22 19:58

16887-00-

Sulfate

9.9

mg/L

1.0

0.55

1



05/27/22 19:58

14808-79-

353.2 Nitrogen, N02/N03 unpres

Analytical Method: EPA 353.2













Pace Analytical Services

- Kansas City











Nitrogen, Nitrate

1.2

mg/L

0.10

0.079

1



05/21/22 10:33

14797-55-

Qual

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 17 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: SW-01-W-17

Lab ID:

60400877007

Collected:

05/19/22 16:40

Received:

05/20/22 08:50

Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





/





Acetone

S ND

ug/L

10.0

2.5 1



06/01/22 14

11

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22 14

11

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22 14

11

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22 14

11

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22 14

11

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22 14

11

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22 14

11

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22 14

11

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22 14

11

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22 14

11

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 14

11

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22 14

11

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22 14

11

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22 14

11

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22 14

11

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22 14

11

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22 14

11

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22 14

11

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22 14

11

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22 14

11

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22 14

11

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22 14

11

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22 14

11

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22 14

11

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 14

11

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 14

11

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22 14

11

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22 14

11

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22 14

11

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



06/01/22 14

11

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22 14

11

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



06/01/22 14

11

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22 14

11

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22 14

11

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22 14

11

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



06/01/22 14

11

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



06/01/22 14

11

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



06/01/22 14

11

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



06/01/22 14

11

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 14

11

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



06/01/22 14

11

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22 14

11

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22 14

11

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22 14

11

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22 14

11

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 18 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: SW-01-W-17 ^

Lab ID:

60400877007

Collected:

05/19/22 16:40

Received:

05/20/22 08:50

Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





/





4-Methyl-2-pentanone (MIBK)

y nd

ug/L

10.0

0.74 1



06/01/22 14

11

108-10-1

Methyl-tert-butyl ether

~ nd

ug/L

1.0

0.13 1



06/01/22 14

11

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



06/01/22 14

11

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 14

11

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



06/01/22 14

11

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22 14

11

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22 14

11

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22 14

11

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



06/01/22 14

11

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22 14

11

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22 14

11

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22 14

11

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22 14

11

79-00-5

Trichloroethene

0.92J

ug/L

1.0

0.21 1



06/01/22 14

11

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22 14

11

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22 14

11

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22 14

11

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22 14

11

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22 14

11

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22 14

11

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

if 100

%

80-120

1



06/01/22 14

11

460-00-4

Toluene-d8 (S)

100

%

80-120

1



06/01/22 14

11

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100 ,

%

80-120

1



06/01/22 14

11

2199-69-1

Preservation pH

1.0 y



0.10

1



06/01/22 14

11



Qual

300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

7.5

mg/L

1.0

0.53

05/27/22 20:12 16887-00-6

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 19 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

r.

Sample: RW-341A-W-17 ^

Lab ID:

60400877008

Collected:

05/19/22 16:55

Received:

05/20/22 08:50 Matrix: Water

~





Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





'





Acetone

y ND

ug/L

10.0

2.5 1



06/01/22

14:25

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22

14:25

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22

14:25

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22

14:25

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22

14:25

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22

14:25

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22

14:25

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22

14:25

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22

14:25

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22

14:25

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

14:25

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22

14:25

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22

14:25

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22

14:25

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22

14:25

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22

14:25

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22

14:25

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22

14:25

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22

14:25

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22

14:25

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22

14:25

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22

14:25

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22

14:25

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22

14:25

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

14:25

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

14:25

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22

14:25

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22

14:25

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22

14:25

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



06/01/22

14:25

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22

14:25

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



06/01/22

14:25

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22

14:25

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22

14:25

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22

14:25

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



06/01/22

14:25

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



06/01/22

14:25

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



06/01/22

14:25

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



06/01/22

14:25

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

14:25

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



06/01/22

14:25

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22

14:25

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22

14:25

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22

14:25

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22

14:25

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 20 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: RW-341A-W-17

Lab ID:

60400877008

Collected:

05/19/22 16:55

Received:

05/20/22 08:50 Matrix: Water

w





Report









Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260











Pace Analytical Services

Kansas City





V



4-Methyl-2-pentanone (MIBK)

~ ND

ug/L

10.0

0.74 1



06/01/22 14:25

108-10-1

Methyl-tert-butyl ether

NT ND

ug/L

1.0

0.13 1



06/01/22 14:25

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



06/01/22 14:25

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 14:25

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



06/01/22 14:25

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22 14:25

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22 14:25

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22 14:25

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



06/01/22 14:25

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22 14:25

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22 14:25

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22 14:25

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22 14:25

79-00-5

Trichloroethene

0.60J

ug/L

1.0

0.21 1



06/01/22 14:25

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22 14:25

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22 14:25

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22 14:25

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22 14:25

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22 14:25

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22 14:25

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

_/• 101

%

80-120

1



06/01/22 14:25

460-00-4

Toluene-d8 (S)

98

%

80-120

1



06/01/22 14:25

2037-26-5

1,2-Dichlorobenzene-d4 (S)

99

f %

80-120

1



06/01/22 14:25

2199-69-1

Preservation pH

1.0

-S

0.10

1



06/01/22 14:25



Qual

300.0 IC Anions 28 Days

Chloride

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

7.6

mg/L

1.0

0.53

05/27/22 20:26 16887-00-6

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 21 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-74-W-17

Lab ID: 60400877009 Collected: 05/19/22 16:58 Received: 05/20/22 08:50 Matrix: Water
Report

Parameters

Results

Units

Limit

VIDL

DF

Prepared

Analyzed

CAS N

RSK 175 Headspace

Analytical Method:

RSK 175 Modified















Pace Analytical Services - Indianapolis













Ethane

ND

ug/L

10.0

3.8

1



05/25/22

16:18

74-84-0

Ethene

ND

ug/L

10.0

7.1

1



05/25/22

16:18

74-85-1

Methane

ND

ug/L

10.0

5.5

1



05/25/22

16:18

74-82-8

6010 MET ICP

Analytical Method:

EPA 6010 Preparation Method

EPA 3010









Pace Analytical Services - Kansas City













Iron

36300

ug/L

50.0

5.6

1

05/23/22 13:10

05/25/22

13:17

7439-89-

8260 MSV

Analytical Method:

EPA 5030B/8260















Pace Analytical Services - Kansas City













Acetone

y ND

ug/L

50.0

12.7

5



06/01/22

15:06

67-64-1

Benzene

ND

ug/L

5.0

0.68

5



06/01/22

15:06

71-43-2

Bromobenzene

ND

ug/L

5.0

0.44

5



06/01/22

15:06

108-86-1

Bromochloromethane

ND

ug/L

5.0

1.0

5



06/01/22

15:06

74-97-5

Bromodichloromethane

ND

ug/L

5.0

0.78

5



06/01/22

15:06

75-27-4

Bromoform

ND

ug/L

5.0

3.4

5



06/01/22

15:06

75-25-2

Bromomethane

ND

ug/L

25.0

2.3

5



06/01/22

15:06

74-83-9

2-Butanone (MEK)

ND

ug/L

50.0

4.9

5



06/01/22

15:06

78-93-3

n-Butylbenzene

ND

ug/L

5.0

0.76

5



06/01/22

15:06

104-51-8

sec-Butylbenzene

ND

ug/L

5.0

0.55

5



06/01/22

15:06

135-98-8

tert-Butylbenzene

ND

ug/L

5.0

0.60

5



06/01/22

15:06

98-06-6

Carbon disulfide

ND

ug/L

25.0

4.9

5



06/01/22

15:06

75-15-0

Carbon tetrachloride

ND

ug/L

5.0

0.86

5



06/01/22

15:06

56-23-5

Chlorobenzene

ND

ug/L

5.0

0.44

5



06/01/22

15:06

108-90-7

Chloroethane

ND

ug/L

5.0

1.9

5



06/01/22

15:06

75-00-3

Chloroform

ND

ug/L

5.0

1.1

5



06/01/22

15:06

67-66-3

Chloromethane

ND

ug/L

5.0

1.4

5



06/01/22

15:06

74-87-3

2-Chlorotoluene

ND

ug/L

5.0

0.54

5



06/01/22

15:06

95-49-8

4-Chlorotoluene

ND

ug/L

5.0

0.74

5



06/01/22

15:06

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

12.5

3.9

5



06/01/22

15:06

96-12-8

Dibromochloromethane

ND

ug/L

5.0

1.5

5



06/01/22

15:06

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

5.0

0.98

5



06/01/22

15:06

106-93-4

Dibromomethane

ND

ug/L

5.0

0.54

5



06/01/22

15:06

74-95-3

1,2-Dichlorobenzene

ND

ug/L

5.0

0.62

5



06/01/22

15:06

95-50-1

1,3-Dichlorobenzene

ND

ug/L

5.0

0.66

5



06/01/22

15:06

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

5.0

0.66

5



06/01/22

15:06

106-46-7

Dichlorodifluoromethane

ND

ug/L

5.0

1.0

5



06/01/22

15:06

75-71-8

1,1-Dichloroethane

ND

ug/L

5.0

0.61

5



06/01/22

15:06

75-34-3

1,2-Dichloroethane

ND

ug/L

5.0

1.1

5



06/01/22

15:06

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

5.0

1.1

5



06/01/22

15:06

540-59-0

1,1-Dichloroethene

ND

ug/L

5.0

1.1

5



06/01/22

15:06

75-35-4

cis-1,2-Dichloroethene

0.79J

ug/L

5.0

0.64

5



06/01/22

15:06

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

5.0

0.51

5



06/01/22

15:06

156-60-5

1,2-Dichloropropane

ND

ug/L

5.0

0.70

5



06/01/22

15:06

78-87-5

1,3-Dichloropropane

ND

ug/L

5.0

0.52

5



06/01/22

15:06

142-28-9

Qual

L1

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 22 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: FAG-74-W-17

Lab ID:

60400877009

Collected:

05/19/22 16:58

Received:

05/20/22 08:50 Matrix: Water









Report















Parameters

Results

Units

Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260

















Pace Analytical Services

Kansas City







y







2,2-Dichloropropane

y- ND

ug/L

5.0

0.81

5



06/01/22

15:06

594-20-7



1,1-Dichloropropene

ND

ug/L

5.0

0.68

5



06/01/22

15:06

563-58-6



cis-1,3-Dichloropropene

ND

ug/L

5.0

0.39

5



06/01/22

15:06

10061 -01 -5



trans-1,3-Dichloropropene

ND

ug/L

5.0

0.91

5



06/01/22

15:06

10061 -02-6



Ethylbenzene

ND

ug/L

5.0

0.60

5



06/01/22

15:06

100-41-4



Hexachloro-1,3-butadiene

ND

ug/L

5.0

2.1

5



06/01/22

15:06

87-68-3



2-Hexanone

ND

ug/L

50.0

5.5

5



06/01/22

15:06

591 -78-6



Isopropylbenzene (Cumene)

ND

ug/L

5.0

0.48

5



06/01/22

15:06

98-82-8



p-lsopropyltoluene

ND

ug/L

5.0

0.64

5



06/01/22

15:06

99-87-6



Methylene Chloride

5.3

ug/L

5.0

2.0

5



06/01/22

15:06

75-09-2

C9

4-Methyl-2-pentanone (MIBK)

ND

ug/L

50.0

3.7

5



06/01/22

15:06

108-10-1



Methyl-tert-butyl ether

ND

ug/L

5.0

0.64

5



06/01/22

15:06

1634-04-4



Naphthalene

ND

ug/L

50.0

4.1

5



06/01/22

15:06

91-20-3



n-Propylbenzene

ND

ug/L

5.0

0.60

5



06/01/22

15:06

103-65-1



Styrene

ND

ug/L

5.0

0.62

5



06/01/22

15:06

100-42-5



1,1,1,2-Tetrachloroethane

ND

ug/L

5.0

0.42

5



06/01/22

15:06

630-20-6



1,1,2,2-Tetrachloroethane

ND

ug/L

5.0

0.77

5



06/01/22

15:06

79-34-5



Tetrachloroethene

ND

ug/L

5.0

1.6

5



06/01/22

15:06

127-18-4



Toluene

ND

ug/L

5.0

1.3

5



06/01/22

15:06

108-88-3



1,2,3-Trichlorobenzene

ND

ug/L

5.0

4.6

5



06/01/22

15:06

87-61-6



1,2,4-Trichlorobenzene

ND

ug/L

5.0

3.7

5



06/01/22

15:06

120-82-1



1,1,1-Trichloroethane

ND

ug/L

5.0

0.54

5



06/01/22

15:06

71-55-6



1,1,2-Trichloroethane

ND

ug/L

5.0

0.71

5



06/01/22

15:06

79-00-5



Trichloroethene

4.0J

ug/L

5.0

1.0

5



06/01/22

15:06

79-01-6



Trichlorofluoromethane

ND

ug/L

5.0

0.82

5



06/01/22

15:06

75-69-4



1,2,3-Trichloropropane

ND

ug/L

12.5

2.0

5



06/01/22

15:06

96-18-4



1,2,4-Trimethylbenzene

ND

ug/L

5.0

1.6

5



06/01/22

15:06

95-63-6



1,3,5-Trimethylbenzene

ND

ug/L

5.0

0.45

5



06/01/22

15:06

108-67-8



Vinyl chloride

ND

ug/L

5.0

0.84

5



06/01/22

15:06

75-01-4



Xylene (Total)

ND

ug/L

15.0

1.4

5



06/01/22

15:06

1330-20-7



Surrogates





















4-Bromofluorobenzene (S)

100

%

80-120



5



06/01/22

15:06

460-00-4

F1

Toluene-d8 (S)

97

%

80-120



5



06/01/22

15:06

2037-26-5



1,2-Dichlorobenzene-d4 (S)

102"^

%

80-120



5



06/01/22

15:06

2199-69-1



Preservation pH

1.0

/¦

0.10



5



06/01/22

15:06





300.0 IC Anions 28 Days

Chloride
Sulfate

353.2 Nitrogen, N02/N03 unpres

Nitrogen, Nitrate

Analytical Method: EPA 300.0
Pace Analytical Services - Kansas City

1.6 mg/L	1.0 0.53

6.9 mg/L	1.0 0.55

Analytical Method: EPA 353.2
Pace Analytical Services - Kansas City

0.40 mg/L	0.10 0.079

05/27/22 20:40 16887-00-6
05/27/22 20:40 14808-79-8

05/21/22 10:36 14797-55-8

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 23 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: EB-01 ^

Lab ID:

60400877010

Collected:

05/19/22 17:00

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





V





Acetone

ND

ug/L

10.0

2.5 1



06/01/22

13:58

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22

13:58

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22

13:58

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22

13:58

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22

13:58

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22

13:58

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22

13:58

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22

13:58

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22

13:58

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22

13:58

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

13:58

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22

13:58

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22

13:58

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22

13:58

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22

13:58

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22

13:58

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22

13:58

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22

13:58

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22

13:58

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22

13:58

96-12-8

Dibromochloromethane

0.52J

ug/L

1.0

0.30 1



06/01/22

13:58

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22

13:58

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22

13:58

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22

13:58

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

13:58

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

13:58

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22

13:58

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22

13:58

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22

13:58

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



06/01/22

13:58

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22

13:58

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



06/01/22

13:58

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22

13:58

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22

13:58

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22

13:58

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



06/01/22

13:58

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



06/01/22

13:58

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



06/01/22

13:58

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



06/01/22

13:58

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

13:58

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



06/01/22

13:58

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22

13:58

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22

13:58

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22

13:58

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22

13:58

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 24 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: EB-01

Lab ID:

60400877010

Collected:

05/19/22 17:00

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No.

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City











4-Methyl-2-pentanone (MIBK)

S ND

ug/L

10.0

0.74 1



06/01/22

13:58

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



06/01/22

13:58

1634-04-4

Naphthalene

ND

ug/L

10.0

0.82 1



06/01/22

13:58

91-20-3

n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

13:58

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



06/01/22

13:58

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22

13:58

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22

13:58

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22

13:58

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



06/01/22

13:58

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22

13:58

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22

13:58

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22

13:58

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22

13:58

79-00-5

Trichloroethene

ND

ug/L

1.0

0.21 1



06/01/22

13:58

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22

13:58

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22

13:58

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22

13:58

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22

13:58

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22

13:58

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22

13:58

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

107

%

80-120

1



06/01/22

13:58

460-00-4

Toluene-d8 (S)

97

%

80-120

1



06/01/22

13:58

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

_ %

80-120

1



06/01/22

13:58

2199-69-1

Preservation pH

1.0



0.10

1



06/01/22

13:58



Qual

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 25 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: TB-01-05192022

Lab ID:

60400877011

Collected:

05/19/22 17:30

Received:

05/20/22 08:50

Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





/





Acetone

^ ND

ug/L

10.0

2.5 1



06/01/22 11

54

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22 11

54

71-43-2

Bromobenzene

0.14J

ug/L

1.0

0.088 1



06/01/22 11

54

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22 11

54

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22 11

54

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22 11

54

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22 11

54

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22 11

54

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22 11

54

104-51-8 B

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22 11

54

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 11

54

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22 11

54

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22 11

54

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22 11

54

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22 11

54

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22 11

54

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22 11

54

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22 11

54

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22 11

54

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22 11

54

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22 11

54

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22 11

54

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22 11

54

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22 11

54

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 11

54

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22 11

54

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22 11

54

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22 11

54

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22 11

54

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



06/01/22 11

54

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22 11

54

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



06/01/22 11

54

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22 11

54

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22 11

54

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22 11

54

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



06/01/22 11

54

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



06/01/22 11

54

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



06/01/22 11

54

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



06/01/22 11

54

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 11

54

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



06/01/22 11

54

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22 11

54

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22 11

54

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22 11

54

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22 11

54

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 26 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: TB-01-05192022 ^

Lab ID:

60400877011

Collected:

05/19/22 17:30

Received:

05/20/22 08:50

Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City





~





4-Methyl-2-pentanone (MIBK)

ND

ug/L

10.0

0.74 1



06/01/22 11

54

108-10-1

Methyl-tert-butyl ether

ND

ug/L

1.0

0.13 1



06/01/22 11

54

1634-04-4

Naphthalene

0.91J

ug/L

10.0

0.82 1



06/01/22 11

54

91-20-3 B

n-Propylbenzene

ND

ug/L

1.0

0.12 1



06/01/22 11

54

103-65-1

Styrene

ND

ug/L

1.0

0.12 1



06/01/22 11

54

100-42-5

1,1,1,2-Tetrachloroethane

ND

ug/L

1.0

0.084 1



06/01/22 11

54

630-20-6

1,1,2,2-Tetrachloroethane

ND

ug/L

1.0

0.15 1



06/01/22 11

54

79-34-5

Tetrachloroethene

ND

ug/L

1.0

0.33 1



06/01/22 11

54

127-18-4

Toluene

ND

ug/L

1.0

0.25 1



06/01/22 11

54

108-88-3

1,2,3-Trichlorobenzene

ND

ug/L

1.0

0.93 1



06/01/22 11

54

87-61-6

1,2,4-Trichlorobenzene

ND

ug/L

1.0

0.73 1



06/01/22 11

54

120-82-1

1,1,1-Trichloroethane

ND

ug/L

1.0

0.11 1



06/01/22 11

54

71-55-6

1,1,2-Trichloroethane

ND

ug/L

1.0

0.14 1



06/01/22 11

54

79-00-5

Trichloroethene

ND

ug/L

1.0

0.21 1



06/01/22 11

54

79-01-6

Trichlorofluoromethane

ND

ug/L

1.0

0.16 1



06/01/22 11

54

75-69-4

1,2,3-Trichloropropane

ND

ug/L

2.5

0.41 1



06/01/22 11

54

96-18-4

1,2,4-Trimethylbenzene

ND

ug/L

1.0

0.32 1



06/01/22 11

54

95-63-6

1,3,5-Trimethylbenzene

ND

ug/L

1.0

0.090 1



06/01/22 11

54

108-67-8

Vinyl chloride

ND

ug/L

1.0

0.17 1



06/01/22 11

54

75-01-4

Xylene (Total)

ND

ug/L

3.0

0.28 1



06/01/22 11

54

1330-20-7

Surrogates

















4-Bromofluorobenzene (S)

^ 98

%

80-120

1



06/01/22 11

54

460-00-4

Toluene-d8 (S)

98



80-120

1



06/01/22 11

54

2037-26-5

1,2-Dichlorobenzene-d4 (S)

100

^ %

80-120

1



06/01/22 11

54

2199-69-1

Preservation pH

1.0



0.10

1



06/01/22 11

54



Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 27 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: TB-02-05192022

Lab ID:

60400877012

Collected:

05/19/22 17:30

Received:

05/20/22 08:50 Matrix: Water







Report











Parameters

Results

Units

Limit

MDL DF

Prepared

Analyzed

CAS No. Qual

8260 MSV

Analytical Method: EPA5030B/8260













Pace Analytical Services

Kansas City









Acetone

^ ND

ug/L

10.0

2.5 1



06/01/22

12:08

67-64-1

Benzene

ND

ug/L

1.0

0.14 1



06/01/22

12:08

71-43-2

Bromobenzene

ND

ug/L

1.0

0.088 1



06/01/22

12:08

108-86-1

Bromochloromethane

ND

ug/L

1.0

0.20 1



06/01/22

12:08

74-97-5

Bromodichloromethane

ND

ug/L

1.0

0.16 1



06/01/22

12:08

75-27-4

Bromoform

ND

ug/L

1.0

0.68 1



06/01/22

12:08

75-25-2

Bromomethane

ND

ug/L

5.0

0.46 1



06/01/22

12:08

74-83-9

2-Butanone (MEK)

ND

ug/L

10.0

0.98 1



06/01/22

12:08

78-93-3

n-Butylbenzene

ND

ug/L

1.0

0.15 1



06/01/22

12:08

104-51-8

sec-Butylbenzene

ND

ug/L

1.0

0.11 1



06/01/22

12:08

135-98-8

tert-Butylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

12:08

98-06-6

Carbon disulfide

ND

ug/L

5.0

0.98 1



06/01/22

12:08

75-15-0

Carbon tetrachloride

ND

ug/L

1.0

0.17 1



06/01/22

12:08

56-23-5

Chlorobenzene

ND

ug/L

1.0

0.089 1



06/01/22

12:08

108-90-7

Chloroethane

ND

ug/L

1.0

0.37 1



06/01/22

12:08

75-00-3

Chloroform

ND

ug/L

1.0

0.22 1



06/01/22

12:08

67-66-3

Chloromethane

ND

ug/L

1.0

0.28 1



06/01/22

12:08

74-87-3

2-Chlorotoluene

ND

ug/L

1.0

0.11 1



06/01/22

12:08

95-49-8

4-Chlorotoluene

ND

ug/L

1.0

0.15 1



06/01/22

12:08

106-43-4

1,2-Dibromo-3-chloropropane

ND

ug/L

2.5

0.78 1



06/01/22

12:08

96-12-8

Dibromochloromethane

ND

ug/L

1.0

0.30 1



06/01/22

12:08

124-48-1

1,2-Dibromoethane (EDB)

ND

ug/L

1.0

0.20 1



06/01/22

12:08

106-93-4

Dibromomethane

ND

ug/L

1.0

0.11 1



06/01/22

12:08

74-95-3

1,2-Dichlorobenzene

ND

ug/L

1.0

0.12 1



06/01/22

12:08

95-50-1

1,3-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

12:08

541 -73-1

1,4-Dichlorobenzene

ND

ug/L

1.0

0.13 1



06/01/22

12:08

106-46-7

Dichlorodifluoromethane

ND

ug/L

1.0

0.20 1



06/01/22

12:08

75-71-8 L1

1,1-Dichloroethane

ND

ug/L

1.0

0.12 1



06/01/22

12:08

75-34-3

1,2-Dichloroethane

ND

ug/L

1.0

0.21 1



06/01/22

12:08

107-06-2

1,2-Dichloroethene (Total)

ND

ug/L

1.0

0.22 1



06/01/22

12:08

540-59-0

1,1-Dichloroethene

ND

ug/L

1.0

0.22 1



06/01/22

12:08

75-35-4

cis-1,2-Dichloroethene

ND

ug/L

1.0

0.13 1



06/01/22

12:08

156-59-2

trans-1,2-Dichloroethene

ND

ug/L

1.0

0.10 1



06/01/22

12:08

156-60-5

1,2-Dichloropropane

ND

ug/L

1.0

0.14 1



06/01/22

12:08

78-87-5

1,3-Dichloropropane

ND

ug/L

1.0

0.10 1



06/01/22

12:08

142-28-9

2,2-Dichloropropane

ND

ug/L

1.0

0.16 1



06/01/22

12:08

594-20-7

1,1-Dichloropropene

ND

ug/L

1.0

0.14 1



06/01/22

12:08

563-58-6

cis-1,3-Dichloropropene

ND

ug/L

1.0

0.078 1



06/01/22

12:08

10061 -01 -5

trans-1,3-Dichloropropene

ND

ug/L

1.0

0.18 1



06/01/22

12:08

10061 -02-6

Ethylbenzene

ND

ug/L

1.0

0.12 1



06/01/22

12:08

100-41-4

Hexachloro-1,3-butadiene

ND

ug/L

1.0

0.42 1



06/01/22

12:08

87-68-3

2-Hexanone

ND

ug/L

10.0

1.1 1



06/01/22

12:08

591 -78-6

Isopropylbenzene (Cumene)

ND

ug/L

1.0

0.097 1



06/01/22

12:08

98-82-8

p-lsopropyltoluene

ND

ug/L

1.0

0.13 1



06/01/22

12:08

99-87-6

Methylene Chloride

ND

ug/L

1.0

0.39 1



06/01/22

12:08

75-09-2

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 28 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

ANALYTICAL RESULTS

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Sample: TB-02-05192022

Parameters

Lab ID: 60400877012 Collected: 05/19/22 17:30 Received: 05/20/22 08:50 Matrix: Water

Results

Units

Report
Limit

MDL

DF

Prepared

Analyzed

CAS No.

Qual

8260 MSV

Analytical Method: EPA5030B/8260
Pace Analytical Services - Kansas City

4-Methyl-2-pentanone (MIBK)



ND

ug/L

10.0

0.74 1

06/01/22 12:08

108-10-1

Methyl-tert-butyl ether



ND

ug/L

1.0

0.13 1

06/01/22 12:08

1634-04-4

Naphthalene



ND

ug/L

10.0

0.82 1

06/01/22 12:08

91-20-3

n-Propylbenzene



ND

ug/L

1.0

0.12 1

06/01/22 12:08

103-65-1

Styrene



ND

ug/L

1.0

0.12 1

06/01/22 12:08

100-42-5

1,1,1,2-Tetrachloroethane



ND

ug/L

1.0

0.084 1

06/01/22 12:08

630-20-6

1,1,2,2-Tetrachloroethane



ND

ug/L

1.0

0.15 1

06/01/22 12:08

79-34-5

Tetrachloroethene



ND

ug/L

1.0

0.33 1

06/01/22 12:08

127-18-4

Toluene



ND

ug/L

1.0

0.25 1

06/01/22 12:08

108-88-3

1,2,3-Trichlorobenzene



ND

ug/L

1.0

0.93 1

06/01/22 12:08

87-61-6

1,2,4-Trichlorobenzene



ND

ug/L

1.0

0.73 1

06/01/22 12:08

120-82-1

1,1,1-Trichloroethane



ND

ug/L

1.0

0.11 1

06/01/22 12:08

71-55-6

1,1,2-Trichloroethane



ND

ug/L

1.0

0.14 1

06/01/22 12:08

79-00-5

Trichloroethene



ND

ug/L

1.0

0.21 1

06/01/22 12:08

79-01-6

Trichlorofluoromethane



ND

ug/L

1.0

0.16 1

06/01/22 12:08

75-69-4

1,2,3-Trichloropropane



ND

ug/L

2.5

0.41 1

06/01/22 12:08

96-18-4

1,2,4-Trimethylbenzene



ND

ug/L

1.0

0.32 1

06/01/22 12:08

95-63-6

1,3,5-Trimethylbenzene



ND

ug/L

1.0

0.090 1

06/01/22 12:08

108-67-8

Vinyl chloride



ND

ug/L

1.0

0.17 1

06/01/22 12:08

75-01-4

Xylene (Total)



ND

ug/L

3.0

0.28 1

06/01/22 12:08

1330-20-7

Surrogates















4-Bromofluorobenzene (S)

y

105

%

80-120

1

06/01/22 12:08

460-00-4

Toluene-d8 (S)



97

%

80-120

1

06/01/22 12:08

2037-26-5

1,2-Dichlorobenzene-d4 (S)



104

%

80-120

1

06/01/22 12:08

2199-69-1

Preservation pH



1.0

y

0.10

1

06/01/22 12:08



Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 29 of 52


-------
SECTION 3

ORGANIC DATA SUPPORT DOCUMENTATION


-------
A. PACE PROJECT NUMBER 60400603


-------
ORGANIC ANALYSIS SUPPORT DOCUMENTATION

Client Name

Ramboll

EnvStd Project Manager:

CMR

Site/Project Name

2022 Newton County Wells Site

Reviewed by:

KMH

Job Number/Task/Subtask

018045

Approved by:

CMR

Laboratory/Location

Pace Kansas

Completion Date:

7/9/22

SDG

60400603

Validation Level:

2

Sample Collection Dates

5/17/22

The following table indicates criteria that
were examined, the identified problems,
and support documentation attachments.

t 73

-------
BLANK ANALYSIS RESULTS FOR ORGANIC PARAMETERS

Fraction

(1)

Matrix
(Aq„ S)

Blank
Type
(2)

Blank Sample Number

Contaminant

Concentration
(mg/Kg-Soil,
ug/L, Aq)

Qualification limit

5x

10x

V

Aq

MB

3143999

None present



0

0

V

Aq

TB

TB-01-051722

None present



0

0













0

0













0

0













0

0













0

0













0

0













0

0













0

0













0

0













0

0













0

0













0

0

1	- V = Volatile; S = Semivolatile; P = Pesticide/PCB; O = Other: 	

2	- MB = Method Blank; TB = Trip Blank; EB = Equipment Blank; FB = Field Blank; IB = Instrument Blank; SB = Storage Blank
Notes:


-------
Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

SAMPLE SUMMARY

Project:	NCWS(LISTA)

Pace Project No.: 60400603

Lab ID

Sample ID

Matrix

Date Collected ^

Date Received

60400603001

RI-MW8-W-17 ^

Water

05/17/22

11:10

05/18/22 08:50

60400603002

RI-MW2-W-17

Water

05/17/22

12:52

05/18/22 08:50

60400603003

RI-MW5-W-17

Water

05/17/22

13:10

05/18/22 08:50

60400603004

RI-MW7-W-17

Water

05/17/22

14:30

05/18/22 08:50

60400603005

RI-MW6-W-17 RI-IVIW-6-W-17

Water

05/17/22

15:50

05/18/22 08:50

60400603006

FAG-62-W-17

Water

05/17/22

15:15

05/18/22 08:50

60400603007

FAG-43-W-17 ^

Water

05/17/22

16:06

05/18/22 08:50

60400603008

RI-MW1-W-17^

Water

05/17/22

16:37

05/18/22 08:50

60400603009

FAG-56-W-17^

Water

05/17/22

17:00

05/18/22 08:50

60400603010

FAG-33-W-17^

Water

05/17/22

17:20

05/18/22 08:50

60400603011

TB-01-051722^

Water

05/17/22

18:00

05/18/22 08:50

^Analytical

www.pacelibs.eom

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 3 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400603

QC Batch:
QC Batch Method:

788798

EPA 5030B/8260

Associated Lab Samples:

60400603001, 60400603002,
60400603008, 60400603009,

Analysis Method:	EPA 5030B/8260

Analysis Description: 8260 MSV Water 10 mL Purge
Laboratory:	Pace Analytical Services - Kansas City

60400603003, 60400603004, 60400603005, 60400603006, 60400603007,
60400603010, 60400603011

METHOD BLANK: 3143999
Associated Lab Samples:

60400603001, 60400603002,
60400603008, 60400603009,

Matrix: Water

60400603003, 60400603004,
60400603010, 60400603011
Blank	Reporting

all ND; no qual.

60400603005, 60400603006, 60400603007,

Parameter

Units

Result

Limit

MDL

Analyzed

1,1,1,2-Tetrachloroethane

ug/L

ND

1.0

0.084

05/25/22 15:53

1,1,1-Trichloroethane

ug/L

ND

1.0

0.11

05/25/22 15:53

1,1,2,2-Tetrachloroethane

ug/L

ND

1.0

0.15

05/25/22 15:53

1,1,2-Trichloroethane

ug/L

ND

1.0

0.14

05/25/22 15:53

1,1-Dichloroethane

ug/L

ND

1.0

0.12

05/25/22 15:53

1,1-Dichloroethene

ug/L

ND

1.0

0.22

05/25/22 15:53

1,1-Dichloropropene

ug/L

ND

1.0

0.14

05/25/22 15:53

1,2,3-Trichlorobenzene

ug/L

ND

1.0

0.93

05/25/22 15:53

1,2,3-Trichloropropane

ug/L

ND

2.5

0.41

05/25/22 15:53

1,2,4-Trichlorobenzene

ug/L

ND

1.0

0.73

05/25/22 15:53

1,2,4-Trimethylbenzene

ug/L

ND

1.0

0.32

05/25/22 15:53

1,2-Dibromo-3-chloropropane

ug/L

ND

2.5

0.78

05/25/22 15:53

1,2-Dibromoethane (EDB)

ug/L

ND

1.0

0.20

05/25/22 15:53

1,2-Dichlorobenzene

ug/L

ND

1.0

0.12

05/25/22 15:53

1,2-Dichloroethane

ug/L

ND

1.0

0.21

05/25/22 15:53

1,2-Dichloroethene (Total)

ug/L

ND

1.0

0.22

05/25/22 15:53

1,2-Dichloropropane

ug/L

ND

1.0

0.14

05/25/22 15:53

1,3,5-Trimethylbenzene

ug/L

ND

1.0

0.090

05/25/22 15:53

1,3-Dichlorobenzene

ug/L

ND

1.0

0.13

05/25/22 15:53

1,3-Dichloropropane

ug/L

ND

1.0

0.10

05/25/22 15:53

1,4-Dichlorobenzene

ug/L

ND

1.0

0.13

05/25/22 15:53

2,2-Dichloropropane

ug/L

ND

1.0

0.16

05/25/22 15:53

2-Butanone (MEK)

ug/L

ND

10.0

0.98

05/25/22 15:53

2-Chlorotoluene

ug/L

ND

1.0

0.11

05/25/22 15:53

2-Hexanone

ug/L

ND

10.0

1.1

05/25/22 15:53

4-Chlorotoluene

ug/L

ND

1.0

0.15

05/25/22 15:53

4-Methyl-2-pentanone (MIBK)

ug/L

ND

10.0

0.74

05/25/22 15:53

Acetone

ug/L

ND

10.0

2.5

05/25/22 15:53

Benzene

ug/L

ND

1.0

0.14

05/25/22 15:53

Bromobenzene

ug/L

ND

1.0

0.088

05/25/22 15:53

Bromochloromethane

ug/L

ND

1.0

0.20

05/25/22 15:53

Bromodichloromethane

ug/L

ND

1.0

0.16

05/25/22 15:53

Bromoform

ug/L

ND

1.0

0.68

05/25/22 15:53

Bromomethane

ug/L

ND

5.0

0.46

05/25/22 15:53

Carbon disulfide

ug/L

ND

5.0

0.98

05/25/22 15:53

Carbon tetrachloride

ug/L

ND

1.0

0.17

05/25/22 15:53

Chlorobenzene

ug/L

ND

1.0

0.089

05/25/22 15:53

Chloroethane

ug/L

ND

1.0

0.37

05/25/22 15:53

Chloroform

ug/L

ND X

1.0

0.22

05/25/22 15:53

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 29 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400603

METHOD BLANK: 3143999

Matrix: Water

Associated Lab Samples:

60400603001, 60400603002, 60400603003, 60400603004, 60400603005, 60400603006, 60400603007,
60400603008, 60400603009, 60400603010, 60400603011

Blank	Reporting

Parameter

Units

Result

Limit

MDL

Analyzed

Chloromethane

ug/L

ND

1.0

0.28

05/25/22 15:53

cis-1,2-Dichloroethene

ug/L

ND

1.0

0.13

05/25/22 15:53

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

05/25/22 15:53

Dibromochloromethane

ug/L

ND

1.0

0.30

05/25/22 15:53

Dibromomethane

ug/L

ND

1.0

0.11

05/25/22 15:53

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

05/25/22 15:53

Ethylbenzene

ug/L

ND

1.0

0.12

05/25/22 15:53

Hexachloro-1,3-butadiene

ug/L

ND

1.0

0.42

05/25/22 15:53

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

05/25/22 15:53

Methyl-tert-butyl ether

ug/L

ND

1.0

0.13

05/25/22 15:53

Methylene Chloride

ug/L

ND

1.0

0.39

05/25/22 15:53

n-Butylbenzene

ug/L

ND

1.0

0.15

05/25/22 15:53

n-Propylbenzene

ug/L

ND

1.0

0.12

05/25/22 15:53

Naphthalene

ug/L

ND

10.0

0.82

05/25/22 15:53

p-lsopropyltoluene

ug/L

ND

1.0

0.13

05/25/22 15:53

sec-Butylbenzene

ug/L

ND

1.0

0.11

05/25/22 15:53

Styrene

ug/L

ND

1.0

0.12

05/25/22 15:53

tert-Butylbenzene

ug/L

ND

1.0

0.12

05/25/22 15:53

Tetrachloroethene

ug/L

ND

1.0

0.33

05/25/22 15:53

Toluene

ug/L

ND

1.0

0.25

05/25/22 15:53

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

05/25/22 15:53

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

05/25/22 15:53

Trichloroethene

ug/L

ND

1.0

0.21

05/25/22 15:53

Trichlorofluoromethane

ug/L

ND

1.0

0.16

05/25/22 15:53

Vinyl chloride

ug/L

ND

1.0

0.17

05/25/22 15:53

Xylene (Total)

ug/L

ND

3.0

0.28

05/25/22 15:53

1,2-Dichlorobenzene-d4 (S)

%

S

CD

00

80-120



05/25/22 15:53

4-Bromofluorobenzene (S)

%

100

80-120



05/25/22 15:53

Toluene-d8 (S)

%

98

80-120



05/25/22 15:53

Qualifiers

LABORATORY CONTROL SAMPLE: 3144000

Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,1,2-Tetrachloroethane

ug/L

20

18.6

93

80-120

1,1-Trichloroethane

ug/L

20

18.5

92

80-120

1,2,2-Tetrachloroethane

ug/L

20

19.0

95

75-125

1,2-Trichloroethane

ug/L

20

19.3

96

80-120

1-Dichloroethane

ug/L

20

19.2

96

75-125

1-Dichloroethene

ug/L

20

19.8

99

80-120

1-Dichloropropene

ug/L

20

18.5

93

80-125

2,3-Trichlorobenzene

ug/L

20

17.0

85^

75-125

2,3-Trichloropropane

ug/L

20

20.0

~ 100

80-125

2,4-Trichlorobenzene

ug/L

20

16.9

85 .

, 75-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 30 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400603

LABORATORY CONTROL SAMPLE:

3144000













Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,2,4-Trimethylbenzene

ug/L

20

18.2

91

80-125

1,2-Dibromo-3-chloropropane

ug/L

20

18.4

92

70-120

1,2-Dibromoethane (EDB)

ug/L

20

18.5

93

80-120

1,2-Dichlorobenzene

ug/L

20

18.3

92

80-120

1,2-Dichloroethane

ug/L

20

18.9

95

75-120

1,2-Dichloroethene (Total)

ug/L

40

37.4

94

80-120

1,2-Dichloropropane

ug/L

20

18.6

93

80-125

1,3,5-Trimethylbenzene

ug/L

20

17.8

89

80-125

1,3-Dichlorobenzene

ug/L

20

17.9

89

80-120

1,3-Dichloropropane

ug/L

20

19.8

99

80-120

1,4-Dichlorobenzene

ug/L

20

17.5

87

80-120

2,2-Dichloropropane

ug/L

20

18.3

91

60-130

2-Butanone (MEK)

ug/L

100

114

114

40-150

2-Chlorotoluene

ug/L

20

18.3

92

80-120

2-Hexanone

ug/L

100

115

115^

45-150

4-Chlorotoluene

ug/L

20

17.6

88

80-120

4-Methyl-2-pentanone (MIBK)

ug/L

100

109

109

65-140

Acetone

ug/L

100

133

133

20-175

Benzene

ug/L

20

18.5

93

80-120

Bromobenzene

ug/L

20

17.6

88

80-120

Bromochloromethane

ug/L

20

19.3

96

80-125

Bromodichloromethane

ug/L

20

19.4

97

80-125

Bromoform

ug/L

20

20.0

100

60-135

Bromomethane

ug/L

20

20.9

105

10-165

Carbon disulfide

ug/L

20

19.0

95

75-135

Carbon tetrachloride

ug/L

20

18.0

90

80-125

Chlorobenzene

ug/L

20

18.9

94^

80-120

Chloroethane

ug/L

20

20.5

102

70-130

Chloroform

ug/L

20

18.4

92

80-120

Chloromethane

ug/L

20

19.6

98

35-155

cis-1,2-Dichloroethene

ug/L

20

18.7

93

80-120

cis-1,3-Dichloropropene

ug/L

20

18.9

95

80-125

Dibromochloromethane

ug/L

20

19.5

98

70-120

Dibromomethane

ug/L

20

19.3

96

80-120

Dichlorodifluoromethane

ug/L

20

19.2

96

50-150

Ethylbenzene

ug/L

20

18.0

90

80-120

Hexachloro-1,3-butadiene

ug/L

20

16.3

82

65-135

Isopropylbenzene (Cumene)

ug/L

20

18.3

91

80-125

Methyl-tert-butyl ether

ug/L

20

20.1

101

65-130

Methylene Chloride

ug/L

20

18.1

91

75-120

n-Butylbenzene

ug/L

20

16.6

83

80-125

n-Propylbenzene

ug/L

20

17.6

88

80-120

Naphthalene

ug/L

20

19.1

96

70-120

p-lsopropyltoluene

ug/L

20

17.2

86

80-135

sec-Butylbenzene

ug/L

20

17.5

88

80-120

Styrene

ug/L

20

19.7

98

80-120

tert-Butylbenzene

ug/L

20

17.2

\

CD

CO

80-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 31 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400603

LABORATORY CONTROL SAMPLE: 3144000

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

Tetrachloroethene

ug/L

20

18.6

93

80-120

Toluene

ug/L

20

18.4

92

80-120

trans-1,2-Dichloroethene

ug/L

20

18.8

94

80-120

trans-1,3-Dichloropropene

ug/L

20

18.9

95

75-120

Trichloroethene

ug/L

20

19.5

97

80-120

Trichlorofluoromethane

ug/L

20

17.6

88

80-130

Vinyl chloride

ug/L

20

17.8

89

65-130

Xylene (Total)

ug/L

60

53.6

89

80-120

1,2-Dichlorobenzene-d4 (S)

%





99

80-120

4-Bromofluorobenzene (S)

%





98

80-120

Toluene-d8 (S)

%





99 /

80-120

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3144001	3144002

^ MS MSD

\ 60400603002 Spike Spike MS MSD MS MSD ^ % Rec ^ Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec

% Rec

Limits

RPD

RPD Qual

1,1,1,2-Tetrachloroethane

ug/L

ND

20

20

12.3

13.0

61

65

70-125

6

15 M1 UJ

1,1,1-Trichloroethane

ug/L

ND

20

20

13.3

13.9

67

70

75-130

4

15 M1 UJ

1,1,2,2-Tetrachloroethane —

ug/L

ND

20

20

12.1

13.4

60

67

65-130

11

15 M1 UJ

1,1,2-Trichloroethane ^

ug/L

ND

20

20

12.1

13.3

60

67

70-120

10

20 M1 UJ

1,1-Dichloroethane

ug/L

ND

20

20

13.1

14.0

66

70

61-130

6

15

1,1-Dichloroethene

ug/L

ND

20

20

13.7

15.0

69

75

60-135

9

25

1,1-Dichloropropene

ug/L

ND

20

20

13.4

13.9

67

70

55-145

4

20

1,2,3-Trichlorobenzene ^

ug/L

ND

20

20

9.9

10.9

49

54

55-120

9

25 M1 UJ

1,2,3-Trichloropropane

ug/L

ND

20

20

12.2

13.5

61

67

60-135

10

20

1,2,4-Trichlorobenzene

ug/L

ND

20

20

10.5

11.4

51

56

50-125

9

25

1,2,4-Trimethylbenzene

ug/L

ND

20

20

12.5

13.2

63

66

60-135

5

20

1,2-Dibromo-3-

ug/L

ND

20

20

10.4

12.6

52

63

55-125

19

25 M1 UJ

chloropropane





















1,2-Dibromoethane (EDB) -

ug/L

ND

20

20

11.7

12.8

58

64

65-125

9

20 M1 UJ

1,2-Dichlorobenzene r

ug/L

ND

20

20

12.5

12.9

62

65

65-120

3

20 M1 UJ

1,2-Dichloroethane

ug/L

ND

20

20

12.7

13.8

64

69

30-160

8

25

1,2-Dichloroethene (Total)

ug/L

ND

40

40

27.0

28.3

68

71

65-125

4

20

1,2-Dichloropropane —

ug/L

ND

20

20

12.8

13.1

64

65

65-130

2

20 M1 UJ

1,3,5-Trimethylbenzene

ug/L

ND

20

20

12.7

13.1

63

65

60-135

3

20

1,3-Dichlorobenzene

ug/L

ND

20

20

12.4

13.0

62

65

65-120

5

20 M1 UJ

1,3-Dichloropropane -

ug/L

ND

20

20

12.4

13.2

62

66

70-120

6

20 M1 UJ

1,4-Dichlorobenzene

ug/L

ND

20

20

12.0

12.8

60

64

60-125

7

20

2,2-Dichloropropane

ug/L

ND

20

20

14.6

15.5

73

78

40-130

6

30

2-Butanone (MEK)

ug/L

ND

100

100

42.2

46.0

42

46

30-130

9

25

2-Chlorotoluene

ug/L

ND

20

20

13.0

13.4

65

67

65-125

3

20

2-Hexanone

ug/L

ND

100

100

42.7

46.3

43

46

40-135

8

20

4-Chlorotoluene

ug/L

ND

20

20

12.4

13.0

62

65

65-125

5

20 M1 UJ

4-Methyl-2-pentanone

ug/L

ND

100

100

62.1

68.0

62

68

60-135

9

20

(MIBK)





















Acetone

ug/L

ND

100

100

29.3

31.4

29

31

10-150

7

25

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 32 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400603

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3144001



3144002



















MS

MSD



















60400603002

Spike

Spike

MS

MSD

MS^

MSD ^

% Rec



Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec

% Rec

Limits

RPD

RPD Qual

Benzene

ug/L

ND

20

20

13.3

14.0

66

70

20-155

5

25

Bromobenzene

ug/L

ND

20

20

12.5

13.1

62

66

65-120

5

15 M1 UJ

Bromochloromethane

ug/L

ND

20

20

12.7

13.7

63

69

65-125

8

20 M1 UJ

Bromodichloromethane ""

ug/L

ND

20

20

13.0

13.8

65

69

70-130

6

15 M1 UJ

Bromoform

ug/L

ND

20

20

12.8

13.4

64

67

50-125

5

20

Bromomethane

ug/L

ND

20

20

13.7

14.6

69

73

10-155

6

45

Carbon disulfide

ug/L

ND

20

20

13.7

14.3

69

72

55-140

4

25

Carbon tetrachloride --

ug/L

ND

20

20

13.5

14.0

68

70

70-140

3

20 M1 UJ

Chlorobenzene

ug/L

ND

20

20

12.5

13.5

63

67

65-130

7

20 M1 UJ

Chloroethane

ug/L

" 0.75J

20

20

16.3

18.7

78

90

20-180

14

20

Chloroform -

ug/L

ND

20

20

12.8

13.7

64

68

70-125

6

20 M1 UJ

Chloromethane

ug/L

ND

20

20

14.2

15.0

71

75

20-160

6

30

cis-1,2-Dichloroethene

ug/L

ND

20

20

13.1

13.6

65

68

55-130

4

20

cis-1,3-Dichloropropene

ug/L

ND

20

20

12.2

13.2

61

66

60-125

8

20

Dibromochloromethane "*

ug/L

ND

20

20

12.5

13.3

62

67

65-120

7

20 M1 UJ

Dibromomethane

ug/L

ND

20

20

11.7

13.6

58

68

65-125

15

20 M1 UJ

Dichlorodifluoromethane

ug/L

ND

20

20

12.8

13.5

64

67

10-175

5

25

Ethylbenzene

ug/L

ND

20

20

12.4

13.3

62

67

20-160

7

25

Hexachloro-1,3-butadiene

ug/L

ND

20

20

10.6

11.9

53

59

40-130

11

30

Isopropylbenzene

ug/L

ND

20

20

13.0

13.6

65

68

65-140

4

20

(Cumene)





















Methyl-tert-butyl ether

ug/L

ND

20

20

12.2

13.4

61

67

25-160

9

30

Methylene Chloride -

ug/L

ND

20

20

11.8

12.9

59

64

60-125

9

25 M1 UJ

n-Butylbenzene

ug/L

ND

20

20

11.7

12.4

58

62

50-140

6

25

n-Propylbenzene

ug/L

ND

20

20

13.0

13.4

65

67

60-130

3

20

Naphthalene

ug/L

ND

20

20

11.2

11.7

56

58

30-150

4

25

p-lsopropyltoluene

ug/L

ND

20

20

11.9

12.8

60

64

50-150

7

20

sec-Butylbenzene

ug/L

ND

20

20

12.7

13.0

64

65

60-140

2

20

Styrene

ug/L

ND

20

20

13.0

13.9

65

70

40-145

7

30

tert-Butylbenzene

ug/L

ND

20

20

12.3

13.0

62

65

60-130

5

20

Tetrachloroethene

ug/L

ND

20

20

12.9

13.8

65

69

55-135

7

25

Toluene

ug/L

ND

20

20

12.7

13.5

64

67

25-150

6

25

trans-1,2-Dichloroethene

ug/L

ND

20

20

14.0

14.7

70

73

60-130

5

20

trans-1,3-Dichloropropene

ug/L

ND

20

20

12.2

12.9

61

65

60-120

5

15

Trichloroethene

ug/L

ND

20

20

13.4

13.9

67

70

50-145

4

20

Trichlorofluoromethane

ug/L

ND

20

20

12.5

13.4

62

67

50-155

8

20

Vinyl chloride

ug/L

ND

20

20

13.6

14.0

68

70

40-155

3

25

Xylene (Total)

ug/L

ND

60

60

36.8

38.8

61

65

15-160

5

30

1,2-Dichlorobenzene-d4 (S)

%











97

98

80-120

/



4-Bromofluorobenzene (S)

%











101

101

80-120





Toluene-d8 (S)

%











99

99

80-120





/

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/02/2022 03:03 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 33 of 44


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:

Pace Project No.

NCWS (LIST A)
60400603

Lab ID

Sample ID

QC Batch Method

QC Batch

60400603006

FAG-62-W-17

RSK175 Modified

677369

60400603009

FAG-56-W-17

RSK175 Modified

677369

60400603010

FAG-33-W-17

RSK175 Modified

677369

60400603006

FAG-62-W-17

EPA 3010

787705

60400603009

FAG-56-W-17

EPA 3010

787705

60400603010

FAG-33-W-17

EPA 3010

787705

60400603001

RI-MW8-W-17

EPA 5030B/8260

788798 ^

60400603002

RI-MW2-W-17

EPA 5030B/8260

788798

60400603003

RI-MW5-W-17

EPA 5030B/8260

788798

60400603004

RI-MW7-W-17

EPA 5030B/8260

788798

60400603005

RI-MW6-W-17

EPA 5030 B/8260

788798

60400603006

FAG-62-W-17

EPA 5030B/8260

788798

60400603007

FAG-43-W-17

EPA 5030 B/8260

788798

60400603008

RI-MW1-W-17

EPA 5030B/8260

788798

60400603009

FAG-56-W-17

EPA 5030 B/8260

788798

60400603010

FAG-33-W-17

EPA 5030 B/8260

788798

60400603011

TB-01-051722

EPA 5030 B/8260

788798

60400603001

RI-MW8-W-17

EPA 300.0

788864

60400603002

RI-MW2-W-17

EPA 300.0

788864

60400603003

RI-MW5-W-17

EPA 300.0

788864

60400603004

RI-MW7-W-17

EPA 300.0

788858

60400603005

RI-MW6-W-17

EPA 300.0

788858

60400603006

FAG-62-W-17

EPA 300.0

788858

60400603007

FAG-43-W-17

EPA 300.0

788858

60400603008

RI-MW1-W-17

EPA 300.0

788858

60400603009

FAG-56-W-17

EPA 300.0

788858

60400603010

FAG-33-W-17

EPA 300.0

788858

60400603006

FAG-62-W-17

EPA 353.2

787649

60400603009

FAG-56-W-17

EPA 353.2

787649

60400603010

FAG-33-W-17

EPA 353.2

787649

Analytical Method

Analytical
Batch

EPA 6010
EPA 6010
EPA 6010

787785
787785
787785

Date: 06/02/2022 03:03 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 40 of 44


-------
B. PACE PROJECT NUMBER 60400849


-------
ORGANIC ANALYSIS SUPPORT DOCUMENTATION

Client Name
Site/Project Name
Job Number/Task/Subtask
Laboratory/Location
SDG

Sample Collection Dates

Ramboll

2022 Newton County Wells Site

018045

Pace Kansas

60400849

EnvStd Project Manager:
Reviewed by:
Approved by:
Completion Date:
Validation Level:

5/18/22

CMR

KMH

CMR

7/10/22

The following table indicates criteria that
were examined, the identified problems,
and support documentation attachments.

t 73

-------
BLANK ANALYSIS RESULTS FOR ORGANIC PARAMETERS

Fraction

(1)

Matrix
(Aq„ S)

Blank
Type
(2)

Blank Sample Number

Contaminant

Concentration
(mg/Kg-Soil,
ug/L, Aq)

Qualification limit

5x

10x

V

Aq

MB

3144380

1,2,3-Trichloro benzene

1.5

7.5

15

V

Aq

MB

3144380

Hexachloro-1,3-butadiene

0.48

2.4

4.8

V

Aq

MB

3144380

Methylene Chloride

0.59

2.95

5.9

V

Aq

MB

3144380

Naphthalene

0.88

4.4

8.8

V

Aq

MB

3147245

1,2,3-Trichloro benzene

1.1

5.5

11

V

Aq

MB

3147245

1,2,4-Trichloro benzene

0.91

4.55

9.1

V

Aq

MB

3147245

cis-1,2-Dichloroethene

0.19

0.95

1.9

V

Aq

MB

3147245

Naphthalene

1.5

7.5

15

V

Aq

TB

TB-01-051822

None present



0

0

V

Aq

TB

TB-02-051822

None present



0

0













0

0













0

0













0

0

1	- V = Volatile; S = Semivolatile; P = Pesticide/PCB; O = Other: 	

2	- MB = Method Blank; TB = Trip Blank; EB = Equipment Blank; FB = Field Blank; IB = Instrument Blank; SB = Storage Blank
Notes: All MB contaminant analytes were not detected or > 5x in the assoc samples. Qualification not warranted.	


-------
DVF_DUP
Page 1 of 1

ENVIRONMENTAL STANDARDS, INC.
EVALUATION OF DUPLICATE RESULTS

Effective Date: 11/23/2015
Revision: 0

Matrix: ® Aqueous O Non-aq.
Reporting Level: ®mdl Oql
Units: |jg/L

PRECISION OBJECTIVES:

If Both Results > 5 x Their QL, RPD <: 20

If Either Result < 5 x Its QL, Dif. <: 1 x Highest QL

Sample ID:

FAG-35-W-17

Duplicate Sample ID:

FD-LISTA-05182022

Analyte

Sample
Concentration

Qual

QL

MDL

Duplicate
Concentration

Qual

QL

MDL

Difference

RPD

Flag

cis-1,2-Dichloroethene

111



5

0.64

105



5

0.64

NA

6%



trans-1,2-Dichloroethene

3.3



5

0.51

3.2



5

0.51

NA

NA



Trichloroethene

537



5

1

520



5

1

NA

3%



Vinyl chloride

0.95



5

0.84

0.84

U

5

0.84

NA

NA



1,2-Dichloroethene (Total)

115



5

1.1

108



5

1.1

NA

6%











































































































































































































































































































































































































































































































































































































































































































































































NOTES:





Qual:

Qualifier(s) based on evaluation(s) other than Total/vs. Dissolved comparison, if applicable (J, U, U* or B)



RPD:

Relative Percent Difference



QL:

Quantitation Limit



MDL:

Method Detection Limit



RL:

Reporting Limit. RL = QL for QL reporting and MDL for MDL reporting



J:

The analyte concentration should be considered estimated



U:

The analyte was not detected in the sample at or above the RL indicated. The RL will be used for comparison purposes.



UJ:

The analyte was not detected in the sample at or above the Reporting Limit Indicated. The RL is approximate.



R:

The analyte was analyzed for and detected, but sample results are unreliable. The presence or absence of the analyte cannot be

verified.

UR:

The analyte was analyzed for and not detected, but the determination that the analyte was not present in the sample is unreliable.

The presence or



absence of the analyte cannot be verified.



U*

The result was blank qualified. The RL will be used for comparison purposes.



NA:

The MDL (for QL reporting), RPD or Difference is not applicable



Comments:

\\esi-file-6\Working\Ramboll Environ\2022 Newton County Wells DV\018045\DRAFT\Support Docs\60400849\DVF_DUP_60400849_LIST_A


-------
DVF_DUP
Page 1 of 1

ENVIRONMENTAL STANDARDS, INC.
EVALUATION OF DUPLICATE RESULTS

Effective Date: 11/23/2015
Revision: 0

Matrix: ® Aqueous O Non-aq.
Reporting Level: ®mdl Gql
Units: |jg/L

PRECISION OBJECTIVES:

If Both Results > 5 x Their QL, RPD <: 20

If Either Result < 5 x Its QL, Dif. <: 1 x Highest QL

Sample ID:

FAG-05-W-17

Duplicate Sample ID:

FD-LIST B-05182022

Analyte

Sample
Concentration

Qual

QL

MDL

Duplicate
Concentration

Qual

QL

MDL

Difference

RPD

Flag

1,2-Dichloroethene (Total)

2.6



1

0.22

2.9



1

0.22

0.3

NA



cis-1,2-Dichloroethene

2.6



1

0.13

2.9



1

0.13

0.3

NA



Trichloroethene

18.7



1

0.21

18



1

0.21

NA

4%



























































































































































































































































































































































































































































































































































































































































































































































































































NOTES:





Qual:

Qualifier(s) based on evaluation(s) other than Total/vs. Dissolved comparison, if applicable (J, U, U* or B)



RPD:

Relative Percent Difference



QL:

Quantitation Limit



MDL:

Method Detection Limit



RL:

Reporting Limit. RL = QL for QL reporting and MDL for MDL reporting



J:

The analyte concentration should be considered estimated



U:

The analyte was not detected in the sample at or above the RL indicated. The RL will be used for comparison purposes.



UJ:

The analyte was not detected in the sample at or above the Reporting Limit Indicated. The RL is approximate.



R:

The analyte was analyzed for and detected, but sample results are unreliable. The presence or absence of the analyte cannot be

verified.

UR:

The analyte was analyzed for and not detected, but the determination that the analyte was not present in the sample is unreliable.

The presence or



absence of the analyte cannot be verified.



U*

The result was blank qualified. The RL will be used for comparison purposes.



NA:

The MDL (for QL reporting), RPD or Difference is not applicable



Comments:

\\esi-file-6\Working\Ramboll Environ\2022 Newton County Wells DV\018045\DRAFT\Support Docs\60400849\DVF_DUP_60400849_LIST_B


-------
Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

SAMPLE SUMMARY

Project:	NCWS (LIST B)

Pace Project No.: 60400849

Lab ID

Sample ID



Matrix

Date Collected

Date Received

60400849001

FAG-47-W-17 V**



Water

05/18/22

08:45

05/19/22 08:50

60400849002

FAG-46-W-17



Water

05/18/22

09:45

05/19/22 08:50

60400849003

FAG-05-W-17 ^



Water

05/18/22

09:00

05/19/22 08:50

60400849004

FD-LIST B-05182022

Water

05/18/22

09:00

05/19/22 08:50

60400849005

FAG-11-W-17 ^



Water

05/18/22

11:05

05/19/22 08:50

60400849006

FAG-35-W-17 ^



Water

05/18/22

11:45

05/19/22 08:50

60400849007

FD-LIST A-05182022



Water

05/18/22

11:45

05/19/22 08:50

60400849008

R1-MW9-W-17 y



Water

05/18/22

12:40

05/19/22 08:50

60400849009

FAG-34-W-17 ^



Water

05/18/22

14:25

05/19/22 08:50

60400849010

FAG-36-W-17 if



Water

05/18/22

15:15

05/19/22 08:50

60400849011

FAG-73-W-17 S



Water

05/18/22

15:40

05/19/22 08:50

60400849012

FAG-32-W-17 ^



Water

05/18/22

16:50

05/19/22 08:50

60400849013

FAG-AW4-W-17



Water

05/18/22

17:00

05/19/22 08:50

60400849014

TB-01-051822



Water

05/18/22

17:43

05/19/22 08:50

60400849015

TB-02-051822 ^



Water

05/18/22

17:49

05/19/22 08:50

^Analytical

www.pacelibs.eom

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 3 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

QC Batch:	788926	Analysis Method:	EPA 5030B/8260

QC Batch Method: EPA5030B/8260 ^	Analysis Description: 8260 MSV Water 10 mL Purge

Laboratory:	Pace Analytical Services - Kansas City

60400849001, 60400849002, 60400849003, 60400849004, 60400849005, 60400849006, 60400849007,
60400849008, 60400849009, 60400849010, 60400849011, 60400849013, 60400849014, 60400849015

Associated Lab Samples:

METHOD BLANK: 3144380
Associated Lab Samples:

Matrix: Water

60400849001, 60400849002, 60400849003, 60400849004,
60400849008, 60400849009, 60400849010, 60400849011,

60400849005, 60400849006, 60400849007, ^
60400849013, 60400849014, 60400849015

Qualifiers

Parameter

Units

Result



i ill ly

Limit

MDL

Analyzed

1,1,1,2-Tetrachloroethane

ug/L



ND

1.0

0.084

05/27/22 00:38

1,1,1-Trichloroethane

ug/L



ND

1.0

0.11

05/27/22 00:38

1,1,2,2-Tetrachloroethane

ug/L



ND

1.0

0.15

05/27/22 00:38

1,1,2-Trichloroethane

ug/L



ND

1.0

0.14

05/27/22 00:38

1,1-Dichloroethane

ug/L



ND

1.0

0.12

05/27/22 00:38

1,1-Dichloroethene

ug/L



ND

1.0

0.22

05/27/22 00:38

1,1-Dichloropropene

ug/L

all samples ND-
no qual

ND

1.0

0.14

05/27/22 00:38

1,2,3-Trichlorobenzene

ug/L

1.5

1.0

0.93

05/27/22 00:38

1,2,3-Trichloropropane

ug/L

ND

2.5

0.41

05/27/22 00:38

1,2,4-Trichlorobenzene

ug/L



ND

1.0

0.73

05/27/22 00:38

1,2,4-Trimethylbenzene

ug/L



ND

1.0

0.32

05/27/22 00:38

1,2-Dibromo-3-chloropropane

ug/L



ND

2.5

0.78

05/27/22 00:38

1,2-Dibromoethane (EDB)

ug/L



ND

1.0

0.20

05/27/22 00:38

1,2-Dichlorobenzene

ug/L



ND

1.0

0.12

05/27/22 00:38

1,2-Dichloroethane

ug/L



ND

1.0

0.21

05/27/22 00:38

1,2-Dichloroethene (Total)

ug/L



ND

1.0

0.22

05/27/22 00:38

1,2-Dichloropropane

ug/L



ND

1.0

0.14

05/27/22 00:38

1,3,5-Trimethylbenzene

ug/L



ND

1.0

0.090

05/27/22 00:38

1,3-Dichlorobenzene

ug/L



ND

1.0

0.13

05/27/22 00:38

1,3-Dichloropropane

ug/L



ND

1.0

0.10

05/27/22 00:38

1,4-Dichlorobenzene

ug/L



ND

1.0

0.13

05/27/22 00:38

2,2-Dichloropropane

ug/L



ND

1.0

0.16

05/27/22 00:38

2-Butanone (MEK)

ug/L



ND

10.0

0.98

05/27/22 00:38

2-Chlorotoluene

ug/L



ND

1.0

0.11

05/27/22 00:38

2-Hexanone

ug/L



ND

10.0

1.1

05/27/22 00:38

4-Chlorotoluene

ug/L



ND

1.0

0.15

05/27/22 00:38

4-Methyl-2-pentanone (MIBK)

ug/L



ND

10.0

0.74

05/27/22 00:38

Acetone

ug/L



ND

10.0

2.5

05/27/22 00:38

Benzene

ug/L



ND

1.0

0.14

05/27/22 00:38

Bromobenzene

ug/L



ND

1.0

0.088

05/27/22 00:38

Bromochloromethane

ug/L



ND

1.0

0.20

05/27/22 00:38

Bromodichloromethane

ug/L



ND

1.0

0.16

05/27/22 00:38

Bromoform

ug/L



ND

1.0

0.68

05/27/22 00:38

Bromomethane

ug/L



ND

5.0

0.46

05/27/22 00:38

Carbon disulfide

ug/L



ND

5.0

0.98

05/27/22 00:38

Carbon tetrachloride

ug/L



ND

1.0

0.17

05/27/22 00:38

Chlorobenzene

ug/L



ND

1.0

0.089

05/27/22 00:38

Chloroethane

ug/L



ND

10

0.37

05/27/22 00:38

Chloroform

ug/L



ND

/ 1.0

0.22

05/27/22 00:38

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 39 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

METHOD BLANK: 3144380

Matrix: Water

Associated Lab Samples:

60400849001, 60400849002, 60400849003, 60400849004, 60400849005, 60400849006, 60400849007,
60400849008, 60400849009, 60400849010, 60400849011, 60400849013, 60400849014, 60400849015





Blank
Result

Reporting





Parameter

Units

Limit

MDL

Analyzed

Chloromethane

ug/L

ND

1.0

0.28

05/27/22 00:38

cis-1,2-Dichloroethene

ug/L

ND

1.0

0.13

05/27/22 00:38

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

05/27/22 00:38

Dibromochloromethane

ug/L

ND

1.0

0.30

05/27/22 00:38

Dibromomethane

ug/L

ND

1.0

0.11

05/27/22 00:38

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

05/27/22 00:38

Ethylbenzene

ug/L

ND

1.0

0.12

05/27/22 00:38

Hexachloro-1,3-butadiene

ug/L

1 0.48J

1.0

0.42

05/27/22 00:38

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

05/27/22 00:38

Methyl-tert-butyl ether

ug/L

ND

1 0.59J

1.0

0.13

05/27/22 00:38

Methylene Chloride

ug/L

1.0

0.39

05/27/22 00:38

n-Butylbenzene

ug/L

ND

1.0

0.15

05/27/22 00:38

n-Propylbenzene

ug/L

ND

1.0

0.12

05/27/22 00:38

Naphthalene

ug/L

1 0.88J

10.0

0.82

05/27/22 00:38

p-lsopropyltoluene

ug/L

ND

1.0

0.13

05/27/22 00:38

sec-Butylbenzene

ug/L

ND

1.0

0.11

05/27/22 00:38

Styrene

ug/L

ND

1.0

0.12

05/27/22 00:38

tert-Butylbenzene

ug/L

ND

1.0

0.12

05/27/22 00:38

Tetrachloroethene

ug/L

ND

1.0

0.33

05/27/22 00:38

Toluene

ug/L

ND

1.0

0.25

05/27/22 00:38

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

05/27/22 00:38

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

05/27/22 00:38

Trichloroethene

ug/L

ND

1.0

0.21

05/27/22 00:38

Trichlorofluoromethane

ug/L

ND

1.0

0.16

05/27/22 00:38

Vinyl chloride

ug/L

ND

	^ 1.0

0.17

05/27/22 00:38

Xylene (Total)

ug/L

ND

3.0

0.28

05/27/22 00:38

1,2-Dichlorobenzene-d4 (S)

%

103

80-120



05/27/22 00:38

4-Bromofluorobenzene (S)

%

94

80-120



05/27/22 00:38

Toluene-d8 (S)

%

101

80-120



05/27/22 00:38

Qualifiers

1 : all samples ND-
no qual

LABORATORY CONTROL SAMPLE: 3144381

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

1,1,1,2-Tetrachloroethane

ug/L

20

19.0

95

80-120

1,1,1-Trichloroethane

ug/L

20

17.9

90

80-120

1,1,2,2-Tetrachloroethane

ug/L

20

19.5

98

75-125

1,1,2-Trichloroethane

ug/L

20

19.5

98

80-120

1,1-Dichloroethane

ug/L

20

20.0

100

75-125

1,1-Dichloroethene

ug/L

20

20.0

100

80-120

1,1-Dichloropropene

ug/L

20

19.3

96

80-125

1,2,3-Trichlorobenzene

ug/L

20

15.4

77

75-125

1,2,3-Trichloropropane

ug/L

20

17.8

89

80-125

1,2,4-Trichlorobenzene

ug/L

20

18.0

90

75-120

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 40 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

LABORATORY CONTROL SAMPLE: 3144381





Spike

LCS

LCS
% Rec

% Rec

Parameter

Units

Cone.

Result

Limits

1,2,4-Trimethylbenzene

ug/L

20

18.4

92

80-125

1,2-Dibromo-3-chloropropane

ug/L

20

17.0

85

70-120

1,2-Dibromoethane (EDB)

ug/L

20

20.0

100

80-120

1,2-Dichlorobenzene

ug/L

20

18.8

94

80-120

1,2-Dichloroethane

ug/L

20

18.8

94

75-120

1,2-Dichloroethene (Total)

ug/L

40

35.0

87

80-120

1,2-Dichloropropane

ug/L

20

19.8

99

80-125

1,3,5-Trimethylbenzene

ug/L

20

18.2

91

80-125

1,3-Dichlorobenzene

ug/L

20

19.0

95

80-120

1,3-Dichloropropane

ug/L

20

21.2

106

80-120

1,4-Dichlorobenzene

ug/L

20

18.5

92

80-120

2,2-Dichloropropane

ug/L

20

15.3

76

60-130

2-Butanone (MEK)

ug/L

100

72.5

72

40-150

2-Chlorotoluene

ug/L

20

18.1

90

80-120

2-Hexanone

ug/L

100

69.5

70

45-150

4-Chlorotoluene

ug/L

20

18.6

93

80-120

4-Methyl-2-pentanone (MIBK)

ug/L

100

88.1

88

65-140

Acetone

ug/L

100

72.7

73

20-175

Benzene

ug/L

20

19.5

98

80-120

Bromobenzene

ug/L

20

18.6

93

80-120

Bromochloromethane

ug/L

20

17.1

85

80-125

Bromodichloromethane

ug/L

20

18.4

92

80-125

Bromoform

ug/L

20

15.7

78

60-135

Bromomethane

ug/L

20

16.8

84

10-165

Carbon disulfide

ug/L

20

19.6

98

75-135

Carbon tetrachloride

ug/L

20

16.5

83

80-125

Chlorobenzene

ug/L

20

20.0

100

80-120

Chloroethane

ug/L

20

19.5

98

70-130

Chloroform

ug/L

20

16.5

82

80-120

Chloromethane

ug/L

20

20.5

103

35-155

cis-1,2-Dichloroethene

ug/L

20

17.7

89

80-120

cis-1,3-Dichloropropene

ug/L

20

18.0

90

80-125

Dibromochloromethane

ug/L

20

16.9

85

70-120

Dibromomethane

ug/L

20

19.7

98

80-120

Dichlorodifluoromethane

ug/L

20

20.8

104

50-150

Ethylbenzene

ug/L

20

19.7

98

80-120

Hexachloro-1,3-butadiene

ug/L

20

15.4

77

65-135

Isopropylbenzene (Cumene)

ug/L

20

20.7

103

80-125

Methyl-tert-butyl ether

ug/L

20

19.6

98

65-130

Methylene Chloride

ug/L

20

28.6

143

75-120

n-Butylbenzene

ug/L

20

18.1

90

80-125

n-Propylbenzene

ug/L

20

19.3

96

80-120

Naphthalene

ug/L

20

17.1

85

70-120

p-lsopropyltoluene

ug/L

20

18.9

95

80-135

sec-Butylbenzene

ug/L

20

19.2

96

80-120

Styrene

ug/L

20

19.8

99

80-120

tert-Butylbenzene

ug/L

20

19.1

95

80-120

Qualifiers



L1 all samples ND - no qual

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 41 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

LABORATORY CONTROL SAMPLE: 3144381





Spike

LCS

LCS
% Rec W

% Rec

Parameter

Units

Cone.

Result

Limits

Tetrachloroethene

ug/L

20

19.2

96

80-120

Toluene

ug/L

20

19.0

95

80-120

trans-1,2-Dichloroethene

ug/L

20

17.3

86

80-120

trans-1,3-Dichloropropene

ug/L

20

17.8

89

75-120

Trichloroethene

ug/L

20

19.2

96

80-120

Trichlorofluoromethane

ug/L

20

20.5

103 ^

80-130

Vinyl chloride

ug/L

20

20.6

103

65-130

Xylene (Total)

ug/L

60

59.3

99

80-120

1,2-Dichlorobenzene-d4 (S)

%





100

80-120

4-Bromofluorobenzene (S)

%





95 .
102 '

80-120

Toluene-d8 (S)

%





80-120

Qualifiers

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3144758^



3144759





















MS

MSD





















60400849013

Spike

Spike

MS

MSD

MS^ MSDfT

% Rec


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3144758



3144759



















MS

MSD



















60400849013

Spike

Spike

MS

MSD

MS ^ MSDnf*

% Rec



Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec % Rec

Limits

RPD

RPD Qual

Benzene

ug/L

ND

200

200

207

203

104

101

20-155

2

25

Bromobenzene

ug/L

ND

200

200

191

190

95

95

65-120

0

15

Bromochloromethane

ug/L

ND

200

200

178

194

89

97

65-125

8

20

Bromodichloromethane

ug/L

ND

200

200

181

199

91

99

70-130

9

15

Bromoform

ug/L

ND

200

200

139

145

69

72^50-125

4^20

Bromomethane

ug/L

ND

200

200

181

196

91

98

10-155

8

45

Carbon disulfide

ug/L

ND

200

200

204

212

102

106

55-140

4

25

Carbon tetrachloride

ug/L

ND

200

200

172

175

86

88

70-140

2

20

Chlorobenzene

ug/L

ND

200

200

202

208

101

104

65-130

3

20

Chloroethane

ug/L

ND

200

200

207

203

103

102

20-180

2

20

Chloroform

ug/L

ND

200

200

164

182

82

91

70-125

10

20

Chloromethane

ug/L

ND

200

200

219

226

110

113

20-160

3

30

cis-1,2-Dichloroethene

ug/L

--~~268

200

200

458

497

95

1151/55-130

8,

~ 20

cis-1,3-Dichloropropene

ug/L

ND

200

200

183

188

92

94

60-125

2

20

Dibromochloromethane

ug/L

ND

200

200

148

167

74

83

65-120

12

20

Dibromomethane

ug/L

ND

200

200

188

225

94

113

65-125

18

20

Dichlorodifluoromethane

ug/L

ND

200

200

197

188

99

94

10-175

5

25

Ethylbenzene

ug/L

ND

200

200

209

201

105

100

20-160

4

25

Hexachloro-1,3-butadiene

ug/L

ND

200

200

164

171

82

85

40-130

4

30

Isopropylbenzene

ug/L

ND

200

200

217

219

108

110

65-140

1

20

(Cumene)





















Methyl-tert-butyl ether

ug/L

ND

200

200

195

210

97

105

25-160

8

30

Methylene Chloride

ug/L

ND

200

200

218

225

109

113

60-125

3

25

n-Butylbenzene

ug/L

ND

200

200

184

198

92

99

50-140

7

25

n-Propylbenzene

ug/L

ND

200

200

202

198

101

99

60-130

2

20

Naphthalene

ug/L

ND

200

200

166

213

83

106

30-150

25

25

p-lsopropyltoluene

ug/L

ND

200

200

195

200

97

100

50-150

3

20

sec-Butylbenzene

ug/L

ND

200

200

195

202

97

101

60-140

4

20

Styrene

ug/L

ND

200

200

201

204

100

102

40-145

2

30

tert-Butylbenzene

ug/L

ND

200

200

198

196

99

98

60-130

1

20

Tetrachloroethene

ug/L

ND

200

200

192

200

96

100^55-135

4,

#25

Toluene

ug/L

ND

200

200

195

201

98

101

25-150

3

25

trans-1,2-Dichloroethene

ug/L

7.6J

200

200

183

192

88

92

60-130

5

20

trans-1,3-Dichloropropene

ug/L

ND

200

200

173

186

87

93

60-120

8

15

Trichloroethene

ug/L

1160

200

200

1480

1470

162

156

50-145

1

20 M1

Trichlorofluoromethane

ug/L

ND

200

200

203

214

102

107

50-155

5

20

Vinyl chloride

ug/L

28.5

200

200

247

235

109

103

40-155

5

25

Xylene (Total)

ug/L

ND

600

600

613

631

102

105

15-160

3

30

1,2-Dichlorobenzene-d4 (S)

%











104

101

80-120





4-Bromofluorobenzene (S)

%











100

95

80-120





Toluene-d8 (S)

%











102

103

80-120





Preservation pH



1.0





1.0

1.0







0



2: SR > 4x SA; no eval

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 43 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:

Pace Project No.

NCWS (LIST B)
60400849

QC Batch:
QC Batch Method:

789629

EPA 5030B/8260

Associated Lab Samples: 60400849012

Analysis Method:
Analysis Description:
Laboratory:

EPA 5030B/8260

8260 MSV Water 10 mL Purge

Pace Analytical Services - Kansas City

METHOD BLANK: 3147245
Associated Lab Samples: 60400849012

Matrix: Water

Parameter

Units

Blank «
Result

Reporting
Limit

MDL

Analyzed



1,1,1,2-Tetrachloroethane

ug/L

ND

1.0

0.084

05/31/22 14

13

1,1,1-Trichloroethane

ug/L

ND

1.0

0.11

05/31/22 14

13

1,1,2,2-Tetrachloroethane

ug/L

ND

1.0

0.15

05/31/22 14

13

1,1,2-Trichloroethane

ug/L

ND

1.0

0.14

05/31/22 14

13

1,1-Dichloroethane

ug/L

ND

1.0

0.12

05/31/22 14

13

1,1-Dichloroethene

ug/L

ND

1.0

0.22

05/31/22 14

13

1,1-Dichloropropene

ug/L

ND

1.0

0.14

05/31/22 14

13

1,2,3-Trichlorobenzene

ug/L

1.1

1.0

0.93

05/31/22 14

13

1,2,3-Trichloropropane

ug/L

ND

2.5

0.41

05/31/22 14

13

1,2,4-Trichlorobenzene

ug/L

0.91 J

1.0

0.73

05/31/22 14

13

1,2,4-Trimethylbenzene

ug/L

ND

1.0

0.32

05/31/22 14

13

1,2-Dibromo-3-chloropropane

ug/L

ND

2.5

0.78

05/31/22 14

13

1,2-Dibromoethane (EDB)

ug/L

ND

1.0

0.20

05/31/22 14

13

1,2-Dichlorobenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

1,2-Dichloroethane

ug/L

ND

1.0

0.21

05/31/22 14

13

1,2-Dichloroethene (Total)

ug/L

ND

1.0

0.22

05/31/22 14

13

1,2-Dichloropropane

ug/L

ND

1.0

0.14

05/31/22 14

13

1,3,5-Trimethylbenzene

ug/L

ND

1.0

0.090

05/31/22 14

13

1,3-Dichlorobenzene

ug/L

ND

1.0

0.13

05/31/22 14

13

1,3-Dichloropropane

ug/L

ND

1.0

0.10

05/31/22 14

13

1,4-Dichlorobenzene

ug/L

ND

1.0

0.13

05/31/22 14

13

2,2-Dichloropropane

ug/L

ND

1.0

0.16

05/31/22 14

13

2-Butanone (MEK)

ug/L

ND

10.0

0.98

05/31/22 14

13

2-Chlorotoluene

ug/L

ND

1.0

0.11

05/31/22 14

13

2-Hexanone

ug/L

ND

10.0

1.1

05/31/22 14

13

4-Chlorotoluene

ug/L

ND

1.0

0.15

05/31/22 14

13

4-Methyl-2-pentanone (MIBK)

ug/L

ND

10.0

0.74

05/31/22 14

13

Acetone

ug/L

ND

10.0

2.5

05/31/22 14

13

Benzene

ug/L

ND

1.0

0.14

05/31/22 14

13

Bromobenzene

ug/L

ND

1.0

0.088

05/31/22 14

13

Bromochloromethane

ug/L

ND

1.0

0.20

05/31/22 14

13

Bromodichloromethane

ug/L

ND

1.0

0.16

05/31/22 14

13

Bromoform

ug/L

ND

1.0

0.68

05/31/22 14

13

Bromomethane

ug/L

ND

5.0

0.46

05/31/22 14

13

Carbon disulfide

ug/L

ND

5.0

0.98

05/31/22 14

13

Carbon tetrachloride

ug/L

ND

1.0

0.17

05/31/22 14

13

Chlorobenzene

ug/L

ND

1.0

0.089

05/31/22 14

13

Chloroethane

ug/L

ND

1.0

0.37

05/31/22 14

13

Chloroform

ug/L

ND

1.0

0.22

05/31/22 14

13

Chloromethane

ug/L

ND

1.0

0.28

05/31/22 14

13

Qualifiers

sample ND - no qual
sample ND - no qual

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 44 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:

Pace Project No.

NCWS (LIST B)
60400849

METHOD BLANK: 3147245
Associated Lab Samples: 60400849012

Matrix: Water

Blank

Reporting

Parameter

Units

Result

Limit

MDL

Analyzed



cis-1,2-Dichloroethene

ug/L

0.19J

1.0

0.13

05/31/22 14

13

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

05/31/22 14

13

Dibromochloromethane

ug/L

ND

1.0

0.30

05/31/22 14

13

Dibromomethane

ug/L

ND

1.0

0.11

05/31/22 14

13

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

05/31/22 14

13

Ethylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Hexachloro-1,3-butadiene

ug/L

ND

1.0

0.42

05/31/22 14

13

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

05/31/22 14

13

Methyl-tert-butyl ether

ug/L

ND

1.0

0.13

05/31/22 14

13

Methylene Chloride

ug/L

ND

1.0

0.39

05/31/22 14

13

n-Butylbenzene

ug/L

ND

1.0

0.15

05/31/22 14

13

n-Propylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Naphthalene

ug/L

1.5J

10.0

0.82

05/31/22 14

13

p-lsopropyltoluene

ug/L

ND

1.0

0.13

05/31/22 14

13

sec-Butylbenzene

ug/L

ND

1.0

0.11

05/31/22 14

13

Styrene

ug/L

ND

1.0

0.12

05/31/22 14

13

tert-Butylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Tetrachloroethene

ug/L

ND

1.0

0.33

05/31/22 14

13

Toluene

ug/L

ND

1.0

0.25

05/31/22 14

13

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

05/31/22 14

13

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

05/31/22 14

13

Trichloroethene

ug/L

ND

1.0

0.21

05/31/22 14

13

Trichlorofluoromethane

ug/L

ND

1.0

0.16

05/31/22 14

13

Vinyl chloride

ug/L

ND

1.0

0.17

05/31/22 14

13

Xylene (Total)

ug/L

ND

3.0

0.28

05/31/22 14

13

1,2-Dichlorobenzene-d4 (S)

%

100

80-120



05/31/22 14

13

4-Bromofluorobenzene (S)

%

99

80-120



05/31/22 14

13

Toluene-d8 (S)

%

96

80-120



05/31/22 14

13

Qualifiers

5x - no qual

sample ND - no qual

ABORATORY CONTROL SAMPLE:

3147246













Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

,1,1,2-Tetrachloroethane

ug/L

20

19.0

95^

80-120

,1,1-Trichloroethane

ug/L

20

19.0

95

80-120

,1,2,2-Tetrachloroethane

ug/L

20

18.6

93

75-125

,1,2-Trichloroethane

ug/L

20

18.2

91

80-120

,1-Dichloroethane

ug/L

20

19.6

98

75-125

,1-Dichloroethene

ug/L

20

22.8

114

80-120

,1-Dichloropropene

ug/L

20

18.8

94^

80-125

,2,3-Trichlorobenzene

ug/L

20

17.6

88

75-125

,2,3-Trichloropropane

ug/L

20

18.7

94

80-125

,2,4-Trichlorobenzene

ug/L

20

19.4

97

75-120

,2,4-Trimethylbenzene

ug/L

20

18.9

94

80-125

,2-Dibromo-3-chloropropane

ug/L

20

14.1

71 V

70-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 45 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

LABORATORY CONTROL SAMPLE: 3147246





Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,2-Dibromoethane (EDB)

ug/L

20

18.8

94

80-120

1,2-Dichlorobenzene

ug/L

20

19.5

97

80-120

1,2-Dichloroethane

ug/L

20

16.0

80

75-120

1,2-Dichloroethene (Total)

ug/L

40

41.4

103

80-120

1,2-Dichloropropane

ug/L

20

17.9

89

80-125

1,3,5-Trimethylbenzene

ug/L

20

18.6

93

80-125

1,3-Dichlorobenzene

ug/L

20

19.8

99

80-120

1,3-Dichloropropane

ug/L

20

17.9

90

80-120

1,4-Dichlorobenzene

ug/L

20

19.3

96

80-120

2,2-Dichloropropane

ug/L

20

18.9

94

60-130

2-Butanone (MEK)

ug/L

100

48.4

48

40-150

2-Chlorotoluene

ug/L

20

18.6

93

80-120

2-Hexanone

ug/L

100

48.0

^ 48

45-150

4-Chlorotoluene

ug/L

20

19.1

96

80-120

4-Methyl-2-pentanone (MIBK)

ug/L

100

64.6

65

65-140

Acetone

ug/L

100

77.1

77

20-175

Benzene

ug/L

20

19.2

96

80-120

Bromobenzene

ug/L

20

19.5

97

80-120

Bromochloromethane

ug/L

20

19.3

96

80-125

Bromodichloromethane

ug/L

20

18.6

93

80-125

Bromoform

ug/L

20

16.3

81

60-135

Bromomethane

ug/L

20

15.7

78

10-165

Carbon disulfide

ug/L

20

24.3

121

75-135

Carbon tetrachloride

ug/L

20

18.9

95

80-125

Chlorobenzene

ug/L

20

20.0

100

80-120

Chloroethane

ug/L

20

26.8

134

70-130

Chloroform

ug/L

20

16.4

82

80-120

Chloromethane

ug/L

20

21.8

109

35-155

cis-1,2-Dichloroethene

ug/L

20

19.3

96

80-120

cis-1,3-Dichloropropene

ug/L

20

19.6

98

80-125

Dibromochloromethane

ug/L

20

15.4

77

70-120

Dibromomethane

ug/L

20

18.5

92

80-120

Dichlorodifluoromethane

ug/L

20

23.4

117

50-150

Ethylbenzene

ug/L

20

19.9

100

80-120

Hexachloro-1,3-butadiene

ug/L

20

19.7

99

65-135

Isopropylbenzene (Cumene)

ug/L

20

21.3

107

80-125

Methyl-tert-butyl ether

ug/L

20

22.4

112

65-130

Methylene Chloride

ug/L

20

46.3

232 , >

75-120

n-Butylbenzene

ug/L

20

18.4

92

80-125

n-Propylbenzene

ug/L

20

20.2

101

80-120

Naphthalene

ug/L

20

16.9

84

70-120

p-lsopropyltoluene

ug/L

20

19.0

95

80-135

sec-Butylbenzene

ug/L

20

19.8

99

80-120

Styrene

ug/L

20

21.0

105

80-120

tert-Butylbenzene

ug/L

20

19.4

97

80-120

Tetrachloroethene

ug/L

20

22.3

111

80-120

Toluene

ug/L

20

17.9

89^.—

' 80-120

Qualifiers

L1 all samples ND - no qual

L1

all samples ND - no qual



Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 46 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:

Pace Project No.

NCWS (LIST B)
60400849

LABORATORY CONTROL SAMPLE: 3147246

Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

trans-1,2-Dichloroethene

ug/L

20

22.1

111

80-120

trans-1,3-Dichloropropene

ug/L

20

16.9

85

75-120

Trichloroethene

ug/L

20

19.2

96

80-120

Trichlorofluoromethane

ug/L

20

24.5

122

80-130

Vinyl chloride

ug/L

20

24.1

121

65-130

Xylene (Total)

ug/L

60

61.4

102

80-120

1,2-Dichlorobenzene-d4 (S)

%





101

80-120

4-Bromofluorobenzene (S)

%





94

80-120

Toluene-d8 (S)

%





93

80-120

Qualifiers

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147247	3147248

MS MSD

nonSDG no eval	60401278038 Spike Spike MS MSD MS ,,, MSD^ % Rec " Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec % Rec

Limits

RPD

RPD

C

1,1,1,2-Tetrachloroethane

ug/L

ND

100

100

97.6

107

98

107

70-125

9

15



1,1,1-Trichloroethane

ug/L

ND

100

100

77.7

92.4

78

92

75-130

17

15

R1

1,1,2,2-Tetrachloroethane

ug/L

ND

100

100

123

139

123

139

65-130

12

15

M1

1,1,2-Trichloroethane

ug/L

ND

100

100

117

126

117

126

70-120

8

20

M1

1,1-Dichloroethane

ug/L

ND

100

100

71.4

75.4

71

75

61-130

5

15



1,1-Dichloroethene

ug/L

ND

100

100

77.8

81.4

78

81

60-135

5

25



1,1-Dichloropropene

ug/L

ND

100

100

84.8

88.1

85

88

55-145

4

20



1,2,3-Trichlorobenzene

ug/L

ND

100

100

86.3

102

86

102

55-120

17

25



1,2,3-Trichloropropane

ug/L

ND

100

100

127

144

127

144

. fc0-135

12^20

M1

1,2,4-Trichlorobenzene

ug/L

ND

100

100

79.6

93.5

80

93

50-125

16

25



1,2,4-Trimethylbenzene

ug/L

ND

100

100

72.8

77.9

73

78

60-135

7

20



1,2-Dibromo-3-

ug/L

ND

100

100

115

126

115

126

55-125

9

25

M1

chloropropane























1,2-Dibromoethane (EDB)

ug/L

ND

100

100

120

139

120

139

65-125

15

20

M1

1,2-Dichlorobenzene

ug/L

ND

100

100

86.7

96.5

87

96

65-120

11

20



1,2-Dichloroethane

ug/L

ND

100

100

100

106

100

106

30-160

5

25



1,2-Dichloroethene (Total)

ug/L

ND

200

200

165

172

82

86

65-125

4

20



1,2-Dichloropropane

ug/L

ND

100

100

99.7

101

100

101

65-130

2

20



1,3,5-Trimethylbenzene

ug/L

ND

100

100

69.9

74.5

70

75

60-135

6

20



1,3-Dichlorobenzene

ug/L

ND

100

100

79.4

87.6

79

88

65-120

10

20



1,3-Dichloropropane

ug/L

ND

100

100

114

123

114

123

70-120

8

20

M1

1,4-Dichlorobenzene

ug/L

ND

100

100

81.3

88.4

81

88

60-125

8

20



2,2-Dichloropropane

ug/L

ND

100

100

61.9

65.5

62

65

40-130

6

30



2-Butanone (MEK)

ug/L

ND

500

500

217

284

37

51

30-130

27

25

R1

2-Chlorotoluene

ug/L

ND

100

100

74.6

78.0

75

78

65-125

4

20



2-Hexanone

ug/L

ND

500

500

332

396

66

79^40-135

18^20



4-Chlorotoluene

ug/L

ND

100

100

77.6

84.0

78

84

65-125

8

20



4-Methyl-2-pentanone

ug/L

ND

500

500

594

642

119

128

60-135

8

20



(MIBK)























Acetone

ug/L

ND

500

500

117

164

21

31

10-150

34

25

R1

Benzene

ug/L

ND

100

100

99.2

97.9

99

98

20-155

1

25



Bromobenzene

ug/L

ND

100

100

92.5

101

93

101

65-120

8

15



Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 47 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS (LIST B)

Pace Project No.: 60400849

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147247



3147248



















MS

MSD



















60401278038

Spike

Spike

MS

MSD

MS MSD rf% Rec



Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec % Rec

Limits

RPD

RPD Qual

Bromochloromethane

ug/L

ND

100

100

95.6

120

96

120

65-125

22

20 R1

Bromodichloromethane

ug/L

ND

100

100

103

110

103

110

70-130

7

15

Bromoform

ug/L

ND

100

100

104

120

104

120

50-125

15

20

Bromomethane

ug/L

ND

100

100

58.8

63.3

59

63

10-155

7

45

Carbon disulfide

ug/L

ND

100

100

72.1

74.1

72

74

55-140

3

25

Carbon tetrachloride

ug/L

ND

100

100

84.7

90.5

85 ^

91 70-140

7 f>^0

Chlorobenzene

ug/L

ND

100

100

99.9

104

96

100

65-130

4

20

Chloroethane

ug/L

ND

100

100

89.3

81.8

89

82

20-180

9

20

Chloroform

ug/L

ND

100

100

74.2

89.8

73

88

70-125

19

20

Chloromethane

ug/L

ND

100

100

66.5

65.5

67

65

20-160

2

30

cis-1,2-Dichloroethene

ug/L

ND

100

100

86.2

88.4

86

88

55-130

2

20

cis-1,3-Dichloropropene

ug/L

ND

100

100

104

108

104

108

60-125

4

20

Dibromochloromethane

ug/L

ND

100

100

97.4

102

97

102

65-120

5

20

Dibromomethane

ug/L

ND

100

100

119

120

119

120

65-125

1

20

Dichlorodifluoromethane

ug/L

ND

100

100

80.3

80.2

80

80

10-175

0

25

Ethylbenzene

ug/L

ND

100

100

85.3

92.5

85

92

20-160

8

25

Hexachloro-1,3-butadiene

ug/L

ND

100

100

88.8

98.4

89

98

40-130

10

30

Isopropylbenzene

ug/L

ND

100

100

84.3

89.1

84

89

65-140

6

20

(Cumene)





















Methyl-tert-butyl ether

ug/L

ND

100

100

117

126

117

126

25-160

8

30

Methylene Chloride

ug/L

7.5

100

100

109

107

102

100 60-125

2 25

n-Butylbenzene

ug/L

ND

100

100

64.5

69.6

65

70

50-140

8

25

n-Propylbenzene

ug/L

ND

100

100

72.8

76.8

73

77

60-130

5

20

Naphthalene

ug/L

ND

100

100

106

131

106

131

30-150

21

25

p-lsopropyltoluene

ug/L

ND

100

100

69.6

71.9

70

72

50-150

3

20

sec-Butylbenzene

ug/L

ND

100

100

70.0

72.3

70

72

60-140

3

20

Styrene

ug/L

ND

100

100

95.5

101

95

101

40-145

5

30

tert-Butylbenzene

ug/L

ND

100

100

69.5

74.7

70

75

60-130

7

20

Tetrachloroethene

ug/L

ND

100

100

95.4

98.1

95

98

55-135

3

25

Toluene

ug/L

ND

100

100

88.5

92.0

89

92

25-150

4

25

trans-1,2-Dichloroethene

ug/L

ND

100

100

78.5

83.8

79

84

60-130

6

20

trans-1,3-Dichloropropene

ug/L

ND

100

100

102

111

102

111

60-120

9

15

Trichloroethene

ug/L

ND

100

100

106

92.7

106

93

50-145

14

20

Trichlorofluoromethane

ug/L

ND

100

100

75.7

80.7

76

81

50-155

6

20

Vinyl chloride

ug/L

ND

100

100

77.5

78.9

78

79

40-155

2

25

Xylene (Total)

ug/L

ND

300

300

272

282

91

94

15-160

4

30

1,2-Dichlorobenzene-d4 (S)

%











105

106

80-120





4-Bromofluorobenzene (S)

%











96

96

80-120





Toluene-d8 (S)

%











96

96

80-120





Preservation pH



1.0





1.0

1.0







0



Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 48 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:

Pace Project No.

NCWS (LIST B)
60400849

Lab ID

Sample ID

QC Batch Method

QC Batch

Analytical

60400849001

FAG-47-W-17

RSK175 Modified

677762



60400849003

FAG-05-W-17

RSK175 Modified

677764



60400849006

FAG-35-W-17

RSK175 Modified

677762



60400849007

FD-LIST A-05182022

RSK175 Modified

677762



60400849009

FAG-34-W-17

RSK175 Modified

677762



60400849010

FAG-36-W-17

RSK175 Modified

677762



60400849011

FAG-73-W-17

RSK175 Modified

677764



60400849012

FAG-32-W-17

RSK175 Modified

677764



60400849013

FAG-AW4-W-17

RSK175 Modified

677764



60400849001

FAG-47-W-17

EPA 3010

788176

EPA 6010

60400849006

FAG-35-W-17

EPA 3010

788176

EPA 6010

60400849007

FD-LIST A-05182022

EPA 3010

788176

EPA 6010

60400849009

FAG-34-W-17

EPA 3010

788176

EPA 6010

60400849010

FAG-36-W-17

EPA 3010

788176

EPA 6010

60400849011

FAG-73-W-17

EPA 3010

788176

EPA 6010

60400849012

FAG-32-W-17

EPA 3010

788176

EPA 6010

60400849001

^ FAG-47-W-17

EPA 5030B/8260

788926



60400849002

FAG-46-W-17

EPA 5030B/8260

788926



60400849003

FAG-05-W-17

EPA 5030B/8260

788926 '



60400849004

FD-LIST B-05182022

EPA 5030B/8260

788926



60400849005

FAG-11-W-17

EPA 5030B/8260

788926



60400849006

FAG-35-W-17

EPA 5030B/8260

788926



60400849007

FD-LIST A-05182022

EPA 5030B/8260

788926



60400849008

R1-MW9-W-17

EPA 5030 B/8260

788926



60400849009

FAG-34-W-17

EPA 5030 B/8260

788926



60400849010

FAG-36-W-17

EPA 5030B/8260

788926



60400849011

FAG-73-W-17

EPA 5030 B/8260

788926



60400849012

^ FAG-32-W-17

EPA 5030 B/8260

789629



60400849013

y- FAG-AW4-W-17

EPA 5030B/8260

788926

/

60400849014

TB-01-051822

EPA 5030 B/8260

788926



60400849015

TB-02-051822

EPA 5030B/8260

788926



60400849001

FAG-47-W-17

EPA 300.0

788861



60400849002

FAG-46-W-17

EPA 300.0

788861



60400849003

FAG-05-W-17

EPA 300.0

788861



60400849004

FD-LIST B-05182022

EPA 300.0

788861



60400849005

FAG-11-W-17

EPA 300.0

788861



60400849006

FAG-35-W-17

EPA 300.0

788861



60400849007

FD-LIST A-05182022

EPA 300.0

788861



60400849008

R1-MW9-W-17

EPA 300.0

788861



60400849009

FAG-34-W-17

EPA 300.0

788861



60400849010

FAG-36-W-17

EPA 300.0

788864



60400849011

FAG-73-W-17

EPA 300.0

788864



60400849012

FAG-32-W-17

EPA 300.0

788864



60400849013

FAG-AW4-W-17

EPA 300.0

788864



Analytical
Batch

788272
788272
788272
788272
788272
788272
788272

REPORT OF LABORATORY ANALYSIS

Date: 06/03/2022 02:36 PM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 55 of 61


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:

Pace Project No.

NCWS (LIST B)
60400849

Lab ID

Sample ID

QC Batch Method

QC Batch

60400849001

FAG-47-W-17

EPA 353.2

788141

60400849003

FAG-05-W-17

EPA 353.2

788141

60400849006

FAG-35-W-17

EPA 353.2

788141

60400849007

FD-LIST A-05182022

EPA 353.2

788141

60400849009

FAG-34-W-17

EPA 353.2

788141

60400849010

FAG-36-W-17

EPA 353.2

788141

60400849011

FAG-73-W-17

EPA 353.2

788141

60400849012

FAG-32-W-17

EPA 353.2

788141

60400849013

FAG-AW4-W-17

EPA 353.2

788141

Analytical Method

Analytical
Batch

Date: 06/03/2022 02:36 PM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 56 of 61


-------
%ce Analytical*

www.p&G&t&bs com

60MSV8 INSTRUMENT SEQUENCE LOG
Analysis Method: o, 2 to

Instrument Batch:

Date
VOC ICAL

C>!S I 1 (.!*'¦>¦

i»GRO

File

001

002

Sample No.

Position
Verified

Batch

Dilution

_e.H

IS

ss

Comments







- - -

„ -







— — - 7 . -





003

004













. ¦

f—

-

. - _







005















006



—

—











-

007





/ X





-



008

009

	_A_-









r_

- -

—

- •

—





1
1





ft.

010

011











1









1







012

013













- „

§







7n //



—-







014

-









—

1

1







015

-



——









016



	

--







i

-





017

018

	_ ..













-

—-



	

	



019

020

021

022

023

- - 	 —:	

1



$L~



	

—

- -

—

—

	







-- 		 - - - -



1



















__











__ ___			 _

024

025

- - 	

	









	



1







028
027

*r	







_±_



-



•



028

J32JL

030

031

032

i





'





	

	











- —

	

	__

- —

		



		 -





—





_		

033

034

t , if r 1 . >. , «¦ ' />'

!	







-

______





1



"""" '

ji-

035

	 	

036







___

—

1



037

038

039









lt.







!

,

. ^	

J







j

i

1

1

1





ft.

_040

041

042







it

	 f



	 .





_



.

~*



c.













It.

#043
044_
.045

046

							

		





i





IL. ti1 Ji-ji Clfi







1
!

V"



ft





-





:..t. ;¦ I !

1/



L

*04

048

il A



,,	j,	—	

r

--









It /». tletJ











(L-

1

I j







L	 "	"¦ 	

,j-e/vfiStandarcl ID No.i ; \

\llSflV3

t: —

*'r fit>ft Q Batch

ICAL/CCAi-j
LCS/MS/L1"'

GRO CCAL
GRt 1 SSV

12-hr Tune Start pi :oe\
Stop n ¦?>

JJJJtLlX-

Page 144 of 150


-------
Paco Analytical

/Jif t ^Co- r?

60MSV8 INSTRUMENT SEQUENCE LOG

Instrument Batch:

Analysis Method

Dat- IJLl
VOC1CAL;

Ot" <' 1

H,!7 *

' j-i' bGR0

File

001

002

003

004

005

006

007

008

009

010

011

012

013

014

015

016

017

018

019

020

021

022

023

024.

025

026

027

028

029

030

031

032

033

034

035

036

037

038

Sample No.

Position

Verified

¦>/



Batch

Dilution

.PtL

i i

IS

ss

v-^

039

040

041
> 042
043

.MfL





Comments

,leA



9Ml»

044

045

"-046

047

04'8

41

Jo£x_



o os, 9 o f 3
m7	7a i >4 <4 ?Tin

^Standard 10 N&"





s X

/tx

ICAL/CCAL
LCS/MS/2"
' GRO CCAL
~ GROSSV'

id-/



Unpreserved - HI >7 days 
-------
C. PACE PROJECT NUMBER 60400877


-------
ORGANIC ANALYSIS SUPPORT DOCUMENTATION

Client Name

Ramboll

EnvStd Project Manager:

CMR

Site/Project Name

2022 Newton County Wells Site

Reviewed by:

KMH

Job Number/Task/Subtask

018045

Approved by:

CMR

Laboratory/Location

Pace Kansas

Completion Date:

7/9/22

SDG

60400877

Validation Level:

2

Sample Collection Dates

5/19/21

The following table indicates criteria that
were examined, the identified problems,
and support documentation attachments.

t 73

-------
BLANK ANALYSIS RESULTS FOR ORGANIC PARAMETERS

Fraction

(1)

Matrix
(Aq„ S)

Blank
Type
(2)

Blank Sample Number

Contaminant

Concentration
(mg/Kg-Soil,
ug/L, Aq)

Qualification limit

5x

10x

V

Aq

MB

3147245

1,2,4-T rich lorobenzene

0.91

4.55

9.1

V

Aq

MB

3147245

cis-1,2-Dichloroethene

0.19

0.95

1.9

V

Aq

MB

3147245

Naphthalene

1.5

7.5

15

V

Aq

MB

3147264

1,2,3-Trich lorobenzene

1.1

5.5

11

V

Aq

MB

3147264

n-Butylbenzene

0.19

0.95

1.9

V

Aq

MB

3147264

Naphthalene

1

5

10

V

Aq

EB

EB-01

Dibromochloromethane

0.52

2.6

5.2

V

Aq

TB

TB-01-05192022

Bromobenzene

0.14

0.7

1.4









Naphthalene

0.91

4.55

9.1

V

Aq

TB

TB-02-05192022

None present



0

0













0

0













0

0













0

0

1	- V = Volatile; S = Semivolatile; P = Pesticide/PCB; O = Other: 	

2	- MB = Method Blank; TB = Trip Blank; EB = Equipment Blank; FB = Field Blank; IB = Instrument Blank; SB = Storage Blank
Notes: All MB contaminant analytes were not detected or > 5x in any of the samples. Qualification not warranted.	


-------
Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

SAMPLE SUMMARY

Project:	NCWS(LISTA)

Pace Project No.: 60400877

Lab ID

Sample ID

Matrix

Date Collected

Date Received

60400877001

FAG-50-W-17^

Water

05/19/22 08:46

05/20/22 08:50

60400877002

FAG-31-W-17

Water

05/19/22 09:25

05/20/22 08:50

60400877003

FAG-85-W-17 xf

Water

05/19/22 10:17

05/20/22 08:50

60400877004

FAG-22-W-17 ^

Water

05/19/22 11:20

05/20/22 08:50

60400877005

FAG-88-W-17 sf

Water

05/19/22 14:00

05/20/22 08:50

60400877006

FAG-89-W-17 ^

Water

05/19/22 15:10

05/20/22 08:50

60400877007

SW-01-W-17 ^

Water

05/19/22 16:40

05/20/22 08:50

60400877008

RW-341A-W-17

Water

05/19/22 16:55

05/20/22 08:50

60400877009

FAG-74-W-17 if

Water

05/19/22 16:58

05/20/22 08:50

60400877010

EB-01

Water

05/19/22 17:00

05/20/22 08:50

60400877011

TB-01-05192022

Water

05/19/22 17:30

05/20/22 08:50

60400877012

TB-02-05192022 ^

Water

05/19/22 17:30

05/20/22 08:50

^Analytical

www.pacelibs.eom

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 3 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

QC Batch:
QC Batch Method:

789629 ^
EPA 5030B/8260

Analysis Method:
Analysis Description:
Laboratory:

EPA 5030B/8260

8260 MSV Water 10 mL Purge

Pace Analytical Services - Kansas City

Associated Lab Samples: 60400877001, 60400877002

METHOD BLANK: 3147245

Associated Lab Samples: 60400877001, 60400877002

Matrix: Water

Blank

Reporting

Parameter

Units

Result

Limit

MDL

Analyzed



1,1,1,2-Tetrachloroethane

ug/L

ND

1.0

0.084

05/31/22 14

13

1,1,1-Trichloroethane

ug/L

ND

1.0

0.11

05/31/22 14

13

1,1,2,2-Tetrachloroethane

ug/L

ND

1.0

0.15

05/31/22 14

13

1,1,2-Trichloroethane

ug/L

ND

1.0

0.14

05/31/22 14

13

1,1-Dichloroethane

ug/L

ND

1.0

0.12

05/31/22 14

13

1,1-Dichloroethene

ug/L

ND

1.0

0.22

05/31/22 14

13

1,1-Dichloropropene

ug/L

ND

1.0

0.14

05/31/22 14

13

1,2,3-Trichlorobenzene

ug/L

1.1

1.0

0.93

05/31/22 14

13

1,2,3-Trichloropropane

ug/L

ND

2.5

0.41

05/31/22 14

13

1,2,4-Trichlorobenzene

ug/L

0.91 J

1.0

0.73

05/31/22 14

13

1,2,4-Trimethylbenzene

ug/L

ND

1.0

0.32

05/31/22 14

13

1,2-Dibromo-3-chloropropane

ug/L

ND

2.5

0.78

05/31/22 14

13

1,2-Dibromoethane (EDB)

ug/L

ND

1.0

0.20

05/31/22 14

13

1,2-Dichlorobenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

1,2-Dichloroethane

ug/L

ND

1.0

0.21

05/31/22 14

13

1,2-Dichloroethene (Total)

ug/L

ND

1.0

0.22

05/31/22 14

13

1,2-Dichloropropane

ug/L

ND

1.0

0.14

05/31/22 14

13

1,3,5-Trimethylbenzene

ug/L

ND

1.0

0.090

05/31/22 14

13

1,3-Dichlorobenzene

ug/L

ND

1.0

0.13

05/31/22 14

13

1,3-Dichloropropane

ug/L

ND

1.0

0.10

05/31/22 14

13

1,4-Dichlorobenzene

ug/L

ND

1.0

0.13

05/31/22 14

13

2,2-Dichloropropane

ug/L

ND

1.0

0.16

05/31/22 14

13

2-Butanone (MEK)

ug/L

ND

10.0

0.98

05/31/22 14

13

2-Chlorotoluene

ug/L

ND

1.0

0.11

05/31/22 14

13

2-Hexanone

ug/L

ND

10.0

1.1

05/31/22 14

13

4-Chlorotoluene

ug/L

ND

1.0

0.15

05/31/22 14

13

4-Methyl-2-pentanone (MIBK)

ug/L

ND

10.0

0.74

05/31/22 14

13

Acetone

ug/L

ND

10.0

2.5

05/31/22 14

13

Benzene

ug/L

ND

1.0

0.14

05/31/22 14

13

Bromobenzene

ug/L

ND

1.0

0.088

05/31/22 14

13

Bromochloromethane

ug/L

ND

1.0

0.20

05/31/22 14

13

Bromodichloromethane

ug/L

ND

1.0

0.16

05/31/22 14

13

Bromoform

ug/L

ND

1.0

0.68

05/31/22 14

13

Bromomethane

ug/L

ND

5.0

0.46

05/31/22 14

13

Carbon disulfide

ug/L

ND

5.0

0.98

05/31/22 14

13

Carbon tetrachloride

ug/L

ND

1.0

0.17

05/31/22 14

13

Chlorobenzene

ug/L

ND

1.0

0.089

05/31/22 14

13

Chloroethane

ug/L

ND

1.0

0.37

05/31/22 14

13

Chloroform

ug/L

ND

1.0

0.22

05/31/22 14

13

Chloromethane

ug/L

ND

1.0

0.28

05/31/22 14

13

Qualifiers

all samples ND - no qual

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 33 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

METHOD BLANK: 3147245

Associated Lab Samples: 60400877001, 60400877002

Matrix: Water

Blank

^ Reporting

Parameter

Units

Result ^

Limit

MDL

Analyzed



cis-1,2-Dichloroethene

ug/L

0.19J

1.0

0.13

05/31/22 14

13

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

05/31/22 14

13

Dibromochloromethane

ug/L

ND

1.0

0.30

05/31/22 14

13

Dibromomethane

ug/L

ND

1.0

0.11

05/31/22 14

13

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

05/31/22 14

13

Ethylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Hexachloro-1,3-butadiene

ug/L

ND

1.0

0.42

05/31/22 14

13

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

05/31/22 14

13

Methyl-tert-butyl ether

ug/L

ND

1.0

0.13

05/31/22 14

13

Methylene Chloride

ug/L

ND

1.0

0.39

05/31/22 14

13

n-Butylbenzene

ug/L

ND

1.0

0.15

05/31/22 14

13

n-Propylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Naphthalene

ug/L

1.5J

10.0

0.82

05/31/22 14

13

p-lsopropyltoluene

ug/L

ND

1.0

0.13

05/31/22 14

13

sec-Butylbenzene

ug/L

ND

1.0

0.11

05/31/22 14

13

Styrene

ug/L

ND

1.0

0.12

05/31/22 14

13

tert-Butylbenzene

ug/L

ND

1.0

0.12

05/31/22 14

13

Tetrachloroethene

ug/L

ND

1.0

0.33

05/31/22 14

13

Toluene

ug/L

ND

1.0

0.25

05/31/22 14

13

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

05/31/22 14

13

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

05/31/22 14

13

Trichloroethene

ug/L

ND

1.0

0.21

05/31/22 14

13

Trichlorofluoromethane

ug/L

ND

1.0

0.16

05/31/22 14

13

Vinyl chloride

ug/L

ND

10

0.17

05/31/22 14

13

Xylene (Total)

ug/L

ND

3.0

0.28

05/31/22 14

13

1,2-Dichlorobenzene-d4 (S)

%

100

80-120



05/31/22 14

13

4-Bromofluorobenzene (S)

%

99

80-120



05/31/22 14

13

Toluene-d8 (S)

%

96

80-120



05/31/22 14

13

Qualifiers

all samples >5x - no qual

all samples ND- no qual

LABORATORY CONTROL SAMPLE: 3147246





Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits

1,1,1,2-Tetrachloroethane

ug/L

20

19.0

95

80-120

1,1,1-Trichloroethane

ug/L

20

19.0

95

80-120

1,1,2,2-Tetrachloroethane

ug/L

20

18.6

93

75-125

1,1,2-Trichloroethane

ug/L

20

18.2

91

80-120

1,1-Dichloroethane

ug/L

20

19.6

98

75-125

1,1-Dichloroethene

ug/L

20

22.8

114

80-120

1,1-Dichloropropene

ug/L

20

18.8

94

80-125

1,2,3-Trichlorobenzene

ug/L

20

17.6

88

75-125

1,2,3-Trichloropropane

ug/L

20

18.7

94

80-125

1,2,4-Trichlorobenzene

ug/L

20

19.4

97

75-120

1,2,4-Trimethylbenzene

ug/L

20

18.9

94

80-125

1,2-Dibromo-3-chloropropane

ug/L

20

14.1

71

70-120

Qualifiers

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 34 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

LABORATORY CONTROL SAMPLE:

3147246 y-













Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec

Limits Qualifiers

1,2-Dibromoethane (EDB)

ug/L

20

18.8

94

80-120

1,2-Dichlorobenzene

ug/L

20

19.5

97

80-120

1,2-Dichloroethane

ug/L

20

16.0

80

75-120

1,2-Dichloroethene (Total)

ug/L

40

41.4

103

80-120

1,2-Dichloropropane

ug/L

20

17.9

89

80-125

1,3,5-Trimethylbenzene

ug/L

20

18.6

93

80-125

1,3-Dichlorobenzene

ug/L

20

19.8

99

80-120

1,3-Dichloropropane

ug/L

20

17.9

90

80-120

1,4-Dichlorobenzene

ug/L

20

19.3

96

80-120

2,2-Dichloropropane

ug/L

20

18.9

94

60-130

2-Butanone (MEK)

ug/L

100

48.4

48

40-150

2-Chlorotoluene

ug/L

20

18.6

93

80-120

2-Hexanone

ug/L

100

48.0

48

45-150

4-Chlorotoluene

ug/L

20

19.1

96 ^

80-120

4-Methyl-2-pentanone (MIBK)

ug/L

100

64.6

65

65-140

Acetone

ug/L

100

77.1

77

20-175

Benzene

ug/L

20

19.2

96

80-120

Bromobenzene

ug/L

20

19.5

97

80-120

Bromochloromethane

ug/L

20

19.3

96

80-125

Bromodichloromethane

ug/L

20

18.6

93

80-125

Bromoform

ug/L

20

16.3

81

60-135

Bromomethane

ug/L

20

15.7

78

10-165

Carbon disulfide

ug/L

20

24.3

121

75-135

Carbon tetrachloride

ug/L

20

18.9

95 
-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

LABORATORY CONTROL SAMPLE: 3147246

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

trans-1,2-Dichloroethene

ug/L

20

22.1

111

80-120

trans-1,3-Dichloropropene

ug/L

20

16.9

85™#*

75-120

Trichloroethene

ug/L

20

19.2

96

80-120

Trichlorofluoromethane

ug/L

20

24.5

122

80-130

Vinyl chloride

ug/L

20

24.1

121

65-130

Xylene (Total)

ug/L

60

61.4

102

80-120

1,2-Dichlorobenzene-d4 (S)

%





101

80-120

4-Bromofluorobenzene (S)

%





94 /

93 f

80-120

Toluene-d8 (S)

%





80-120

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147247	3147248

non SDG

no eval ,,
Parameter Units

60401278038
Result

MS
Spike
Cone.

MSD
Spike
Cone.

MS
Result

MSD
Result

MS
% Rec

MSD
% Rec

% Rec
Limits

RPD

Max
RPD

C

1,1,1,2-Tetrachloroethane

ug/L

ND

100

100

97.6

107

98

107

70-125

9

15



1,1,1-Trichloroethane

ug/L

ND

100

100

77.7

92.4

78

92

75-130

17

15

R1

1,1,2,2-Tetrachloroethane

ug/L

ND

100

100

123

139

123

139

65-130

12

15

M1

1,1,2-Trichloroethane

ug/L

ND

100

100

117

126

117

126

70-120

8

20

M1

1,1-Dichloroethane

ug/L

ND

100

100

71.4

75.4

71

75

61-130

5

15



1,1-Dichloroethene

ug/L

ND

100

100

77.8

81.4

78

81

60-135

5

25



1,1-Dichloropropene

ug/L

ND

100

100

84.8

88.1

85

88

55-145

4

20



1,2,3-Trichlorobenzene

ug/L

ND

100

100

86.3

102

86

102

55-120

17

25



1,2,3-Trichloropropane

ug/L

ND

100

100

127

144

127

144

60-135

12

20

M1

1,2,4-Trichlorobenzene

ug/L

ND

100

100

79.6

93.5

80

93

50-125

16

25



1,2,4-Trimethylbenzene

ug/L

ND

100

100

72.8

77.9

73

78

60-135

7

20



1,2-Dibromo-3-

ug/L

ND

100

100

115

126

115

126

55-125

9

25

M1

chloropropane























1,2-Dibromoethane (EDB)

ug/L

ND

100

100

120

139

120

139

65-125

15

20

M1

1,2-Dichlorobenzene

ug/L

ND

100

100

86.7

96.5

87

96

65-120

11

20



1,2-Dichloroethane

ug/L

ND

100

100

100

106

100

106

30-160

5

25



1,2-Dichloroethene (Total)

ug/L

ND

200

200

165

172

82

86

65-125

4

20



1,2-Dichloropropane

ug/L

ND

100

100

99.7

101

100

101

65-130

2

20



1,3,5-Trimethylbenzene

ug/L

ND

100

100

69.9

74.5

70

75

60-135

6

20



1,3-Dichlorobenzene

ug/L

ND

100

100

79.4

87.6

79

88

65-120

10

20



1,3-Dichloropropane

ug/L

ND

100

100

114

123

114

123

70-120

8

20

M1

1,4-Dichlorobenzene

ug/L

ND

100

100

81.3

88.4

81

88

60-125

8

20



2,2-Dichloropropane

ug/L

ND

100

100

61.9

65.5

62

65

40-130

6

30



2-Butanone (MEK)

ug/L

ND

500

500

217

284

37

51

30-130

27

25

R1

2-Chlorotoluene

ug/L

ND

100

100

74.6

78.0

75

78

65-125

4

20



2-Hexanone

ug/L

ND

500

500

332

396

66

79

40-135

18

20



4-Chlorotoluene

ug/L

ND

100

100

77.6

84.0

78

84

65-125

8

20



4-Methyl-2-pentanone

ug/L

ND

500

500

594

642

119

128

60-135

8

20



(MIBK)























Acetone

ug/L

ND

500

500

117

164

21

31

10-150

34

25

R1

Benzene

ug/L

ND

100

100

99.2

97.9

99

98

20-155

1

25



Bromobenzene

ug/L

ND

100

100

92.5

101

93

101

65-120

8

15



Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 36 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147247

3147248

non SDG
Parameter

Units

60401278038
Result

MS
Spike
Cone.

MSD
Spike
Cone.

MS
Result

MSD
Result

MS
% Rec

MSD
% Rec

% Rec
Limits

RPD

Max

RPD C

Bromochloromethane

ug/L

ND

100

100

95.6

120

96

120

65-125

22

20 R1

Bromodichloromethane

ug/L

ND

100

100

103

110

103

110

70-130

7

15

Bromoform

ug/L

ND

100

100

104

120

104

120

50-125

15

20

Bromomethane

ug/L

ND

100

100

58.8

63.3

59

63

10-155

7

45

Carbon disulfide

ug/L

ND

100

100

72.1

74.1

72

74

55-140

3

25

Carbon tetrachloride

ug/L

ND

100

100

84.7

90.5

85

91

70-140

7

20

Chlorobenzene

ug/L

ND

100

100

99.9

104

96

100

65-130

4

20

Chloroethane

ug/L

ND

100

100

89.3

81.8

89

82

20-180

9

20

Chloroform

ug/L

ND

100

100

74.2

89.8

73

88

70-125

19

20

Chloromethane

ug/L

ND

100

100

66.5

65.5

67

65

20-160

2

30

cis-1,2-Dichloroethene

ug/L

ND

100

100

86.2

88.4

86

88

55-130

2

20

cis-1,3-Dichloropropene

ug/L

ND

100

100

104

108

104

108

60-125

4

20

Dibromochloromethane

ug/L

ND

100

100

97.4

102

97

102

65-120

5

20

Dibromomethane

ug/L

ND

100

100

119

120

119

120

65-125

1

20

Dichlorodifluoromethane

ug/L

ND

100

100

80.3

80.2

80

80

10-175

0

25

Ethylbenzene

ug/L

ND

100

100

85.3

92.5

85

92

20-160

8

25

Hexachloro-1,3-butadiene

ug/L

ND

100

100

88.8

98.4

89

98

40-130

10

30

Isopropylbenzene

ug/L

ND

100

100

84.3

89.1

84

89

65-140

6

20

(Cumene)





















Methyl-tert-butyl ether

ug/L

ND

100

100

117

126

117

126

25-160

8

30

Methylene Chloride

ug/L

7.5

100

100

109

107

102

100

60-125

2

25

n-Butylbenzene

ug/L

ND

100

100

64.5

69.6

65

70

50-140

8

25

n-Propylbenzene

ug/L

ND

100

100

72.8

76.8

73

77

60-130

5

20

Naphthalene

ug/L

ND

100

100

106

131

106

131

30-150

21

25

p-lsopropyltoluene

ug/L

ND

100

100

69.6

71.9

70

72

50-150

3

20

sec-Butylbenzene

ug/L

ND

100

100

70.0

72.3

70

72

60-140

3

20

Styrene

ug/L

ND

100

100

95.5

101

95

101

40-145

5

30

tert-Butylbenzene

ug/L

ND

100

100

69.5

74.7

70

75

60-130

7

20

Tetrachloroethene

ug/L

ND

100

100

95.4

98.1

95

98

55-135

3

25

Toluene

ug/L

ND

100

100

88.5

92.0

89

92

25-150

4

25

trans-1,2-Dichloroethene

ug/L

ND

100

100

78.5

83.8

79

84

60-130

6

20

trans-1,3-Dichloropropene

ug/L

ND

100

100

102

111

102

111

60-120

9

15

Trichloroethene

ug/L

ND

100

100

106

92.7

106

93

50-145

14

20

Trichlorofluoromethane

ug/L

ND

100

100

75.7

80.7

76

81

50-155

6

20

Vinyl chloride

ug/L

ND

100

100

77.5

78.9

78

79

40-155

2

25

Xylene (Total)

ug/L

ND

300

300

272

282

91

94

15-160

4

30

1,2-Dichlorobenzene-d4 (S)

%











105

106

80-120





4-Bromofluorobenzene (S)

%











96

96

80-120





Toluene-d8 (S)

%











96

96

80-120





Preservation pH



1.0





1.0

1.0







0



Qual

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 37 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877 ^

QC Batch:
QC Batch Method:

789635

EPA 5030B/8260

Associated Lab Samples:

60400877003, 60400877004,
60400877010, 60400877011,

Analysis Method:

Analysis Description:
Laboratory:

60400877005, 60400877006,
60400877012

EPA 5030B/8260

8260 MSV Water 10 mL Purge

Pace Analytical Services - Kansas City

60400877007, 60400877008, 60400877009,

METHOD BLANK: 3147264
Associated Lab Samples:

60400877003, 60400877004,
60400877010, 60400877011,

Matrix: Water

60400877005, 60400877006,
60400877012

60400877007, 60400877008, 60400877009,

Parameter

Units

Blank
Result

~

Reporting
Limit

MDL

Analyzed



1,1,1,2-Tetrachloroethane

ug/L



ND

1.0

0.084

06/01/22

11

40

1,1,1-Trichloroethane

ug/L



ND

1.0

0.11

06/01/22

11

40

1,1,2,2-Tetrachloroethane

ug/L



ND

1.0

0.15

06/01/22

11

40

1,1,2-Trichloroethane

ug/L



ND

1.0

0.14

06/01/22

11

40

1,1-Dichloroethane

ug/L



ND

1.0

0.12

06/01/22

11

40

1,1-Dichloroethene

ug/L



ND

1.0

0.22

06/01/22

11

40

1,1-Dichloropropene

ug/L



ND

1.0

0.14

06/01/22

11

40

1,2,3-Trichlorobenzene

ug/L



1.1

1.0

0.93

06/01/22

11

40

1,2,3-Trichloropropane

ug/L



ND

2.5

0.41

06/01/22

11

40

1,2,4-Trichlorobenzene

ug/L



ND

1.0

0.73

06/01/22

11

40

1,2,4-Trimethylbenzene

ug/L



ND

1.0

0.32

06/01/22

11

40

1,2-Dibromo-3-chloropropane

ug/L



ND

2.5

0.78

06/01/22

11

40

1,2-Dibromoethane (EDB)

ug/L



ND

1.0

0.20

06/01/22

11

40

1,2-Dichlorobenzene

ug/L



ND

1.0

0.12

06/01/22

11

40

1,2-Dichloroethane

ug/L



ND

1.0

0.21

06/01/22

11

40

1,2-Dichloroethene (Total)

ug/L



ND

1.0

0.22

06/01/22

11

40

1,2-Dichloropropane

ug/L



ND

1.0

0.14

06/01/22

11

40

1,3,5-Trimethylbenzene

ug/L



ND

1.0

0.090

06/01/22

11

40

1,3-Dichlorobenzene

ug/L



ND

1.0

0.13

06/01/22

11

40

1,3-Dichloropropane

ug/L



ND

1.0

0.10

06/01/22

11

40

1,4-Dichlorobenzene

ug/L



ND

1.0

0.13

06/01/22

11

40

2,2-Dichloropropane

ug/L



ND

1.0

0.16

06/01/22

11

40

2-Butanone (MEK)

ug/L



ND

10.0

0.98

06/01/22

11

40

2-Chlorotoluene

ug/L



ND

1.0

0.11

06/01/22

11

40

2-Hexanone

ug/L



ND

10.0

1.1

06/01/22

11

40

4-Chlorotoluene

ug/L



ND

1.0

0.15

06/01/22

11

40

4-Methyl-2-pentanone (MIBK)

ug/L



ND

10.0

0.74

06/01/22

11

40

Acetone

ug/L



ND

10.0

2.5

06/01/22

11

40

Benzene

ug/L



ND

1.0

0.14

06/01/22

11

40

Bromobenzene

ug/L



ND

1.0

0.088

06/01/22

11

40

Bromochloromethane

ug/L



ND

1.0

0.20

06/01/22

11

40

Bromodichloromethane

ug/L



ND

1.0

0.16

06/01/22

11

40

Bromoform

ug/L



ND

1.0

0.68

06/01/22

11

40

Bromomethane

ug/L



ND

5.0

0.46

06/01/22

11

40

Carbon disulfide

ug/L



ND

5.0

0.98

06/01/22

11

40

Carbon tetrachloride

ug/L



ND

1.0

0.17

06/01/22

11

40

Chlorobenzene

ug/L



ND

1.0

0.089

06/01/22

11

40

Chloroethane

ug/L



ND

1.0

0.37

06/01/22

11

40

Chloroform

ug/L



ND

1.0

0.22

06/01/22

11

40

Qualifiers

all samples ND - no qual

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 38 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

METHOD BLANK: 3147264

Matrix: Water

Associated Lab Samples:

60400877003, 60400877004, 60400877005, 60400877006, 60400877007, 60400877008, 60400877009,
60400877010, 60400877011, 60400877012

Blank	Reporting

Parameter

Units

Result if

Limit

MDL

Analyzed



Chloromethane

ug/L

ND

1.0

0.28

06/01/22 11

40

cis-1,2-Dichloroethene

ug/L

ND

1.0

0.13

06/01/22 11

40

cis-1,3-Dichloropropene

ug/L

ND

1.0

0.078

06/01/22 11

40

Dibromochloromethane

ug/L

ND

1.0

0.30

06/01/22 11

40

Dibromomethane

ug/L

ND

1.0

0.11

06/01/22 11

40

Dichlorodifluoromethane

ug/L

ND

1.0

0.20

06/01/22 11

40

Ethylbenzene

ug/L

ND

1.0

0.12

06/01/22 11

40

Hexachloro-1,3-butadiene

ug/L

ND

1.0

0.42

06/01/22 11

40

Isopropylbenzene (Cumene)

ug/L

ND

1.0

0.097

06/01/22 11

40

Methyl-tert-butyl ether

ug/L

ND

1.0

0.13

06/01/22 11

40

Methylene Chloride

ug/L

ND

1.0

0.39

06/01/22 11

40

n-Butylbenzene

ug/L

0.19J

1.0

0.15

06/01/22 11

40

n-Propylbenzene

ug/L

ND

1.0

0.12

06/01/22 11

40

Naphthalene

ug/L

1.0J

10.0

0.82

06/01/22 11

40

p-lsopropyltoluene

ug/L

ND

1.0

0.13

06/01/22 11

40

sec-Butylbenzene

ug/L

ND

1.0

0.11

06/01/22 11

40

Styrene

ug/L

ND

1.0

0.12

06/01/22 11

40

tert-Butylbenzene

ug/L

ND

1.0

0.12

06/01/22 11

40

Tetrachloroethene

ug/L

ND

1.0

0.33

06/01/22 11

40

Toluene

ug/L

ND

1.0

0.25

06/01/22 11

40

trans-1,2-Dichloroethene

ug/L

ND

1.0

0.10

06/01/22 11

40

trans-1,3-Dichloropropene

ug/L

ND

1.0

0.18

06/01/22 11

40

Trichloroethene

ug/L

ND

1.0

0.21

06/01/22 11

40

Trichlorofluoromethane

ug/L

ND

1.0

0.16

06/01/22 11

40

Vinyl chloride

ug/L

ND

1.0

0.17

06/01/22 11

40

Xylene (Total)

ug/L

ND

3.0

0.28

06/01/22 11

40

1,2-Dichlorobenzene-d4 (S)

%

99

80-120



06/01/22 11

40

4-Bromofluorobenzene (S)

%

102

80-120



06/01/22 11

40

Toluene-d8 (S)

%

98

- 80-120



06/01/22 11

40

Qualifiers

ill samples ND - no qual
I samples ND; no qual

LABORATORY CONTROL SAMPLE: 3147265

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

1,1,2-Tetrachloroethane

ug/L

20

18.2

91

80-120

1,1-Trichloroethane

ug/L

20

19.2

96

80-120

1,2,2-Tetrachloroethane

ug/L

20

18.7

94

75-125

1,2-Trichloroethane

ug/L

20

18.3

91

80-120

1-Dichloroethane

ug/L

20

17.9

89

75-125

1-Dichloroethene

ug/L

20

18.4

92

80-120

1-Dichloropropene

ug/L

20

19.8

99

80-125

2,3-Trichlorobenzene

ug/L

20

19.0

95

75-125

2,3-Trichloropropane

ug/L

20

18.7

94

80-125

2,4-Trichlorobenzene

ug/L

20

18.8

9V

75-120

Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 39 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

LABORATORY CONTROL SAMPLE:

3147265













Spike

LCS

LCS

% Rec

Parameter

Units

Cone.

Result

% Rec if

Limits

1,2,4-Trimethylbenzene

ug/L

20

18.4

92

80-125

1,2-Dibromo-3-chloropropane

ug/L

20

18.4

92

70-120

1,2-Dibromoethane (EDB)

ug/L

20

17.5

87

80-120

1,2-Dichlorobenzene

ug/L

20

19.6

98

80-120

1,2-Dichloroethane

ug/L

20

17.8

89

75-120

1,2-Dichloroethene (Total)

ug/L

40

35.3

88

80-120

1,2-Dichloropropane

ug/L

20

19.3

96

80-125

1,3,5-Trimethylbenzene

ug/L

20

18.8

94

80-125

1,3-Dichlorobenzene

ug/L

20

19.6

98

80-120

1,3-Dichloropropane

ug/L

20

18.4

92 
-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

LABORATORY CONTROL SAMPLE: 3147265

Parameter

Units

Spike
Cone.

LCS
Result

LCS
% Rec

% Rec
Limits

Qualifiers

Tetrachloroethene

ug/L

20

18.0

90

80-120

Toluene

ug/L

20

18.6

93

80-120

trans-1,2-Dichloroethene

ug/L

20

18.2

91

80-120

trans-1,3-Dichloropropene

ug/L

20

18.8

94

75-120

Trichloroethene

ug/L

20

18.4

92

80-120

Trichlorofluoromethane

ug/L

20

19.1

96

80-130

Vinyl chloride

ug/L

20

21.7

108

65-130

Xylene (Total)

ug/L

60

55.3

92

80-120

1,2-Dichlorobenzene-d4 (S)

%





100

80-120

4-Bromofluorobenzene (S)

%





98

80-120

Toluene-d8 (S)

%





97

80-120



MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147266

z-' MS
60400877003 Spike
Parameter Units Result Cone.

MSD
Spike
Cone.

3147267

MS
Result

MSD
Result

MS MSD 
-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA

Project:	NCWS(LISTA)

Pace Project No.: 60400877

MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3147266



3147267



















MS

MSD



















60400877003

Spike

Spike

MS

MSD

MS vf MSD^

% Rec

~

Max

Parameter

Units

Result

Cone.

Cone.

Result

Result

% Rec % Rec

Limits

RPD

RPD Qual

Benzene

ug/L

ND

100

100

99.6

102

100

102

20-155

2

25

Bromobenzene

ug/L

ND

100

100

92.6

96.5

93

97

65-120

4

15

Bromochloromethane

ug/L

ND

100

100

91.6

97.5

92

97

65-125

6

20

Bromodichloromethane

ug/L

ND

100

100

96.0

101

96

101

70-130

5

15

Bromoform

ug/L

ND

100

100

80.6

85.9

81

86

50-125

6

20

Bromomethane

ug/L

ND

100

100

107

111

107

111

10-155

3

45

Carbon disulfide

ug/L

ND

100

100

100

106

100

106

55-140

5

25

Carbon tetrachloride

ug/L

ND

100

100

104

107

104

107

70-140

3

20

Chlorobenzene

ug/L

ND

100

100

92.5

97.2

93

97

65-130

5

20

Chloroethane

ug/L

ND

100

100

116

122

116

122

20-180

5

20

Chloroform

ug/L

ND

100

100

91.3

96.6

91

96^*70-125

6 20

Chloromethane

ug/L

ND

100

100

125

130

125

130

20-160

4

30

cis-1,2-Dichloroethene

ug/L

367

100

100

462

470

94

102

55-130

2

20

cis-1,3-Dichloropropene

ug/L

ND

100

100

95.6

97.6

96

98

60-125

2

20

Dibromochloromethane

ug/L

ND

100

100

82.2

86.8

82

87

65-120

5

20

Dibromomethane

ug/L

ND

100

100

93.3

98.8

93

99

65-125

6

20

Dichlorodifluoromethane

ug/L

ND

100

100

169

173

169

173

10-175

2

25

Ethylbenzene

ug/L

ND

100

100

94.8

97.5

95

97

20-160

3

25

Hexachloro-1,3-butadiene

ug/L

ND

100

100

83.5

91.0

84

91

40-130

9

30

Isopropylbenzene

ug/L

ND

100

100

100

101

100

101

65-140

0

20

(Cumene)











94^









Methyl-tert-butyl ether

ug/L

ND

100

100

93.9

103

103^25-160

9^T30

Methylene Chloride

ug/L

ND

100

100

105

108

103

107

60-125

3

25

n-Butylbenzene

ug/L

ND

100

100

88.0

92.9

88

93

50-140

6

25

n-Propylbenzene

ug/L

ND

100

100

94.6

96.7

95

97

60-130

2

20

Naphthalene

ug/L

ND

100

100

80.8

94.3

81

94

30-150

15

25

p-lsopropyltoluene

ug/L

ND

100

100

90.2

97.4

90

97

50-150

8

20

sec-Butylbenzene

ug/L

ND

100

100

92.1

96.7

92

97

60-140

5

20

Styrene

ug/L

ND

100

100

94.6

96.1

95

96

40-145

2

30

tert-Butylbenzene

ug/L

ND

100

100

94.1

99.3

94

99

60-130

5

20

Tetrachloroethene

ug/L

ND

100

100

92.6

95.0

93

95

55-135

3

25

Toluene

ug/L

ND

100

100

97.0

99.1

97

99

25-150

2

25

trans-1,2-Dichloroethene

ug/L

5.1

100

100

97.2

102

92

97

60-130

5

20

trans-1,3-Dichloropropene

ug/L

ND

100

100

92.0

98.0

92

98

60-120

6

15

Trichloroethene

ug/L

252

100

100

361

362

109

110

50-145

0

20

Trichlorofluoromethane

ug/L

ND

100

100

97.7

99.0

98

99

50-155

1

20

Vinyl chloride

ug/L

53.8

100

100

165

170

111

117

40-155

3

25

Xylene (Total)

ug/L

ND

300

300

283

290

94

97 w15-160

2 30

1,2-Dichlorobenzene-d4 (S)

%











101

100

80-120





4-Bromofluorobenzene (S)

%











102

103

80-120





Toluene-d8 (S)

%











97

CD

80-120





Preservation pH



1.0





1.0

1.0

s



0



Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.

REPORT OF LABORATORY ANALYSIS

Date: 06/04/2022 07:54 AM

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 42 of 52


-------
iceAnalytical

www.paceIibs.eom

Pace Analytical Services, LLC

9608 Loiret Blvd.
Lenexa, KS 66219
(913)599-5665

QUALITY CONTROL DATA CROSS REFERENCE TABLE

Project:

Pace Project No.

NCWS (LIST A)
60400877

Lab ID

Sample ID

QC Batch Method

QC Batch

Analytical

60400877001

FAG-50-W-17

RSK175 Modified

678072



60400877002

FAG-31-W-17

RSK175 Modified

678072



60400877003

FAG-85-W-17

RSK175 Modified

678305



60400877004

FAG-22-W-17

RSK175 Modified

678305



60400877005

FAG-88-W-17

RSK175 Modified

678305



60400877006

FAG-89-W-17

RSK175 Modified

678305



60400877009

FAG-74-W-17

RSK175 Modified

678305



60400877001

FAG-50-W-17

EPA 3010

788176

EPA 6010

60400877002

FAG-31-W-17

EPA 3010

788176

EPA 6010

60400877003

FAG-85-W-17

EPA 3010

788176

EPA 6010

60400877004

FAG-22-W-17

EPA 3010

788176

EPA 6010

60400877009

FAG-74-W-17

EPA 3010

788176

EPA 6010

60400877001

FAG-50-W-17

EPA 5030B/8260

789629 ^



60400877002

FAG-31-W-17

EPA 5030B/8260

789629



60400877003

FAG-85-W-17

EPA 5030B/8260

789635



60400877004

FAG-22-W-17

EPA 5030B/8260

789635



60400877005

FAG-88-W-17

EPA 5030B/8260

789635



60400877006

FAG-89-W-17

EPA 5030B/8260

789635



60400877007

SW-01-W-17

EPA 5030B/8260

789635



60400877008

RW-341A-W-17

EPA 5030B/8260

789635



60400877009

FAG-74-W-17

EPA 5030B/8260

789635



60400877010

EB-01

EPA 5030B/8260

789635



60400877011

TB-01-05192022

EPA 5030B/8260

789635



60400877012

TB-02-05192022

EPA 5030B/8260

789635



60400877001

FAG-50-W-17

EPA 300.0

789132



60400877002

FAG-31-W-17

EPA 300.0

789132



60400877003

FAG-85-W-17

EPA 300.0

789132



60400877004

FAG-22-W-17

EPA 300.0

789132



60400877005

FAG-88-W-17

EPA 300.0

789132



60400877006

FAG-89-W-17

EPA 300.0

789132



60400877007

SW-01-W-17

EPA 300.0

789132



60400877008

RW-341A-W-17

EPA 300.0

789132



60400877009

FAG-74-W-17

EPA 300.0

789132



60400877001

FAG-50-W-17

EPA 353.2

788080



60400877002

FAG-31-W-17

EPA 353.2

788080



60400877003

FAG-85-W-17

EPA 353.2

788080



60400877004

FAG-22-W-17

EPA 353.2

788080



60400877005

FAG-88-W-17

EPA 353.2

788091



60400877006

FAG-89-W-17

EPA 353.2

788091



60400877009

FAG-74-W-17

EPA 353.2

788091



Analytical
Batch

788272
788272
788272
788272
788272

Date: 06/04/2022 07:54 AM

REPORT OF LABORATORY ANALYSIS

This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.

Page 48 of 52


-------
SECTION 4
PROJECT CHAIN-OF-CUSTODY RECORDS


-------
race Analytical

CHAIN-OF-CUSTODYI Analytical Request Document

The Chain-of-Custody is a LEGAL DOCUMENT. Ail relevant fields must be completed accurately.

Section A

Required Client Information:

Section B

Required Project Information:

Section C

invoice Information:

Page:

X

Company: Ramboll Environ

Report To: Doug Burge

Attention:



Address: 1807 Park 270 Drive, Ste 450

Copy To: llJlluj MR*

Company Name:

REGULATORY AGENCY

St. Louis, MO 63146



Address:

NPDES r GROU^? WATER f DRINKING WATER

Email To

Phone:

Request

dburae@rambolI.CQm

Purchase Order No

Project Name: NCWS (List A)

Project Number: 1937680A

Pace Quote
Reference:

pace Project Jamie Church

Manager:

Pace Profile #: 1320

1 ~ UST 1"" RCRA

P OTHFR

314-513-1973 Fax: 314-513-1951
id Due Date/TAT:

Site Location
STATE:

MO





Requested Analysis Filtered (Y/N)



%
m

in

t

Section D Valid Matrix Codes
Required Client Information MATRIX CODE
DRINKING WATER DW
WATER WT
WASTE WATER WW
PRODUCT P
SOIL/SOLID SL
OIL OL

SAMPLE ID ™ apP

(A-Z, 0-9 /,-) OTHER OT
Sample IDs MUST BE UNIQUE ^)SSUE ts

Vv

MATRIX CODE (see valid codes to left)

6T

2
O
o

If

o

03
<
SX

0

S

as
a.

LU

~_

<
m

COLLECTED

SAMPLE TEMP AT COLLECTION

# OF CONTAINERS

Preservatives

52
>

























T" «PT

COMPOSITE
END/GRAB

| Unpreserved |

d

w

I

o
z

X

o

X

X

o

CO

z

o

0?

eg
CD

Z

o
c
CD

a

CD

0
£

o

ilAnalysis Test4

*

8
;>

0

0
CD

z

0
ZJ

CO

Chloride

Methane/Ethane/Ethene

Total Iron













Z

>

0)
c:
¦c
o

JZ

O
76

a
¦a

'to
CD

Cd

QofoOQO)

Pace Project No./ Lab I.D.

DATE

TIME

*

DATE

TIME

1

£1~mw8- to - IT-

WT

G





#vj?.

lllo



1







X











X





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2

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%

















ADDITIONAL COMMENTS

RELINQUISHED BY I AFFILIATION

DATE

TIME/*"

ACCEPTj^JD BY / AFFILIATION

DATE

TIME

SAMPLE CONDITIONS



1











If

T V X







	-"V,

—// 	¦



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ge 42 of 44

SAMPLER NAME AND SIGNATURE

c

a.

£
CD

1—

Received on ;
Ice (Y/N)

Custody Sealea
Cooler (Y/N)

Samples Intact
(Y/N)

PRINT Name of SAMPLER: | /XlQtUAl t, ^

y			

SIGNATURE of SAMPLER:



•Important Note; By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1 5% per month for any invoices not paid within 30 days

F-ALL-Q-020rev. 08,12-0ct-2007


-------


'ceAnatytical

CHAIN-OF-CUSTODY /Analytical Request Document

The Chain-of-Custody is a LEGAL DOCUMENT All relevant fields must be completed accurately

Section A

Required Client h

rnmria

Section B

Required Project Information:

R

1807 Park 270 Drive, Ste 450

St. Louis, MO 63146

Phone: 314-513-1973

Fax: 314-513-1951

Requested Due Date/TAT:

Section C

rtion:

Rodo* Tc Doug Burge

Copy To:



NrV 'S IW

Project Number: "j 937680A

Page:

Facr O-o'e
Reference:

Jamie Church

1320

¦2. "Q

REGULATORY AGENCY

NPDES

LIST

GROUND WATER
PCRA

DRINKING WATER
OTHER 	

Site Location
STATE:

MO

-!

6

7

8

?_

10

11

12

, D

J Client Information

SAMPLE ID

(A-Z 0-9/,-)
p'e IDs MUST BE UNIQUE

soil/sol

OIL

WiPE

AIR

OTHER
TISSUE

atrsx Codes

ESSE

WATSF? DW
WT

'ATE.R WW
P

LID	SL

T8 ^ oi ~ oS~'VaA

ADDITIONAL COMMENTS

COLLECTED

OMPOSiTE
START

G ;

G I

A

w

If m

RELINQUISHED BY I AFFILIATION

Preservatives

°Ji

x x
—!—

TIME



Requested Analysis Fiitered (Y/N)



ACCEPTED BY / AFFILIATION

QctfOOtoG]

-

Pace Project No./ Lab I.D.

SAMPLE CONDITIONS

CQ
fl>

Aif	KtQ^tb





iJimx

Qli

2

; v r





SAMPLER NAME AND SIGNATURE

PRINT Name of SAMPLER:

SIGNATURE of SAMPLER

Mc (vj 
-------
UO#:60400603

{&i,

ce

l.AHf 'M .(£(> u

DC#_Titl@: ENV-FRM-LENE-0009_Sample C

60400603

Revision: 2

Client Name: Wl | jg.n yjfor)

Effective Date: 01/12/2022 Issued By: Lenexa

Courier:

FedEx tsl UPS ~ VIA ~	Clay ~ PEX ~ ECI ~ Pace ~ Xroads ~ Client ~ Other ~

Tracking #: 2.732- Of, I WTV	Pace Shipping Label UsedJ	Yes [/ No ~

Custody Sea! on Cooler'Box Present: ^Y'es S>	No ~ Seals intact: Yes 0	No ~

Packing Material: _J3uhbie Wrap .(/ Bubble Bags i/	Foam ~	None ~

Thermometer Used: ^ V"1 \	Type of Ice: Blue None	/

Cooler Temperature (°C): As-read S S	Corr. Factor—^ Corrected	2^--b ^

Temperature shciuki be above freezing to 6"C

Other



Chain of Custody present:

ddCes DNo

~ n/a

~

Chain of Custody relinquished:

0Yes DNo

~ n/a



Samples arrived within holding time:

S^es ONo

~ n/a



Short Hold Time analyses (<72hr):

^Yes ONo

~ n/a

/VDX

Rush Turn Around Time requested:

~Yes

~ n/a



Sufficient volume:

s Dno

~ n/a



Correct containers used:

E^Yes DNo

~ n/a



Pace containers used:

Q^es UHo

~ n/a



Containers intact:

O^Yes DNo

~ n/a



Undeserved 5038A / TX1005/1006 soils frozen in 48hrs?

~Yes DNo

~/a



Filtered volume received for dissolved tests?

~Yes DNo

B^n/a



Sample labels match COC: Date / time / ID / analyses

fl^Yes DNo

~ n/a



Samples contain multiple phases? Matrix: WT

~Yes

No

~ n/a



Containers requiring pH preservation in compliance? ^
(HNO3, H2SOj, HCK2; NaOH>9 Sulfide, NaOH>10 Cyanide)
(Exceptions: VOA, Micro, O&G, KS TPH, OK-DRO) LOT#:

s/ves Dfio

~ n/a

List sample IDs, volumes, lot #'s of preservative and the
date/time added.

Cyanide water sample checks:

Lead acetate strip turns dark? (Record only)

Potassium iodide test strip turns blue/purple? (Preserve)

~ Yes DNo
~Yes DNo





Trip Blank present:

G^es DNo

~ n/a

/

Headspace in VOA vials ( >6mm):

~ Yes s/io

~ n/a



Samples from USDA Regulated Area: State:

~Yes ~



SIn/a



Additional labels attached to 5035A / TX1005 vials in the field?

~ Yes Q

w Dn/a



Client Notification/ Resolution

Person Contacted: _____
Comments/ Resolution:

Project Manager Review: 			Date:

Qualtrax Document ID: 30468	Page 1 of 1

Copy COC to Client? Y / N Field Data Required? Y / N
Date/Time: 			

Page 41 of 44


-------
DC#_Title: ENV-FRM-LENE-00Q1_Sample Container Count
Revision: 3 | Effective Date: 12/22/2021 | Issued by: Lenexa

Client: &»v/w h? \ p p, ref,		 _ 	Profile #_ U %o

^ Arcwj (.Lftr A)	 N..R1 - t'7 M yp\t> KH8-1 gf;v

		"		, Hor &

coc

Line Item



VG9H

DG9H

DG9Q

VG9U

DG9U

DG9M

DG9B

...

BG1U

AG1H

AG1U

AG2U

AG3S

AG4U

AG5U

JGFU

jWGKU

WGDU

3
a.

CD

BP2U

BP3U

z
K.

CO

BP3N

£
CQ

8

CL

CO

BP3C

N

to
El
CO

Z)
D

a.

§

ZPLC

S

s





1



*







































































































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3



U2U





































%

























	







































1-























5

I







































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*>





































a.



.1



















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*





































a.



%



















10



*





*































1



a



















11

V

2-

Th1

fl'm

•Mr{

































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.:¦











































i



















Container Codes

Glass

Plastic



Misc.

DG9B

40mL bisulfate clear vial

WGKU 	

8oz clear soil iar

BP1C

1L NAOH plastic

I

Wipe/Swab

DG9H

40mL HCI amber voa vial

WGFU	

4oz clear soil jar

BP1N

1L HN03 plastic



120mL Coliform Na Thiosulfate

DG9M

40mL MeOH clear vial

WG2U

2oz clear soil iar

BP1S

1LH2S04 plastic

ZPLC

Ziploc Bag

DG9Q

40mL TSP amber vial

JGFU

4oz unpreserved amber wide

BP1U

1L unpreserved plastic

AF

Air Filter

DG9S

40mL H2S04 amber vial

AGOU

100mL unores amber qlass

BP1Z

1L NaOH, Zn Acetate

C

Air Cassettes

DG9T

40mL Na Thio amber vial

AG1H

1L HCI amber qlass

BP2C

500mL NAOH plastic

R

Terracore Kit

DG9U

40mL amber unpreserved

AG1S

1L H2S04 amber glass

BP2N

500mL HN03 plastic

U

Summa Can

VG9H

40mL HCI clear vial

AG1T

1L Na Thiosulfate clear/amber qlass

BP2S

500mL H2S04 plastic





VG9T

40mL Na Thio. clear vial

AG1U

1 liter unpres amber glass

BP2U

SOOmL unpreserved plastic





VG9U

40mL unpreserved clear vial

AG2N

500mL HN03 amber qlass

BP2Z

500mL NaOH, Zn Acetate

Matrix

BG1S

1 liter H2S04 clear glass

AG2S

500mL H2S04 amber glass

BP3C

250mL NaOH plastic

BG1U

1 liter unpres glass

AG3S

250mL H2S04 amber glass

BP3F

250mL HN03 plastic - field filtered

WT

Water

BG3H

250ml HCI Clear qlass

AG2U

500mL unpres amber glass

BP3N

250mL HN03 plastic

SL

Solid

BG3U

250mL Unpres Clear qlass

AG3U

250mL unpres amber qlass

BP3U

250mL unpreserved plastic

NAL

Non-aqueous Liquid

WGDU

16oz clear soil iar

AG4U

125mL unpres amber glass

BP3S

250mL H2S04 plastic

OL

OIL



AG5U

100mL unpres amber qlass

BP3Z

250mL NaOH, Zn Acetate

WP

Wipe









BP4U

125mL unpreserved plastic

DW

Drinking Water









BP4N

125mL HN03 plastic













BP4S

125mL H2S04 plastic













WPDU

16oz unoresserved plstic





Work Order Number:



Qualtrax Document ID: 30422

Pace Analytical Services, LLC

Page 1 of 1


-------
^	CHAIN-OF-CUSTODY / Analytical Request Document

£

aC6 Analytical	The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.

Section A	Section B	Section C

Required Client information:	Required Project Information:	Invoice Information:

Company: Ramboll Environ

Report To: Doug Burge

Attention:



Address: 1807 Park 270 Drive, Ste 453



Company Name:

REGULATORY AGENCY

St. Louis, MO 63146



Address:

r NPDES i" GROUND WATER T DRINKING WATER

Email To

dburae@ramboll.com

Purchase Order No..:

Pace Quote
Reference:

! UST i " RCRA

\ ~ HTHFR





Phone: 314-513-1973 Fax: 314-513-1951

Requested Due Date/TAT:

Project Name: NCWS (List B)
Project Number 1937680A

Pace Project Jamie Church

Manager:

Pace Profile#: ^320

Sits Location
STATE:

MO





Requested Analysis Filtered (Y/N)



ITEM #

Section D Vsiid Matrix Codes
Required Client Information MATRIX CODE
DRNKING WATER DW
WATER WT
WASTE WATER WW
PRODUCT P
SOIL/SOLID SL
OIL OL

SAMPLE ID ™=E £

(A-Z, 0-9 /,-) OT-IER OT
Sample IDs MUST BE UNIQUE TISSUE ts

MATRIX CODE (see valid codes to left)

SAMPLE TYPE (G-GRAB C=COMP)

COLLECTED

SAMPLE TEMP AT COLLECTION

# OF CONTAINERS

Preservatives

z
>

























COMPOSITE
START

COMPOSITE
END/GRAB

| Unpreserved |



o
z

X

o

X

I

o

CO
-Z.

o

CO
CO

z

o
c

CO

s

03

5

0
£
O

t Analysis Test!

VOCs ^ s.

Chloride ^ \

Sulfate

(Nitrate

Methane/Ethane/Ethene

i
>2













z

£
QJ
c;

o
jz
O
__

3

73
'tn






/









X

X

























S

FaG-34- 



V

V









X

V

y

X

y

¥

















10

fA O " 3 (o ~ U* ~ f

WT

G









ts-'T



s

y



*"

X









V

X

X

X

y

¥¦

















11



WT

G









iwo



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y



r

y









y

>

r

y

*

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12

f4G'3* -

WT

G





%

*

ftS"o



"5

/*



y

•f









Vr

X

y

Y

*

*

















ADDITIONAL COMMENTS

RELINQUISHED BY I AFFILIATION

DATE

TIME

ACCEPTED BY / AFFILIATION

DATE

TIME

SAMPLE CONDITIONS









K jMt. of*

ipk?



-n J

i

W W 4/











-1I f/















/









I ,





















(Q

-------
Face Analytical

CHA1N-0F-CUST0DY / Analytical Request Document

The Chain-of-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.

Section A

Required Client information:

Section B

Required Project Information:

Section C

invoice information:

Company:

Ramboll Environ

Report To: Doug Burge

Page:

2. • A

Address:

1807 Park 270 Drive, Ste 450

c.„»	^

Company Name:

REGULATORY AGENCY

St. Louis, MO 63146

Address:

dbyrqe@ramboll.com

£"ce Quote
Reference:

NPDES
UST

GROUND WATER

RCRA

DRSNKING WATER
OTHER 	

Phone: 314-513-1973

Fax: 314-513-1951

Project Name: NCWS (List B)

Pace Project Jamie Church
Manager

Requested Due Date/TAT:

Project Number 193768QA

Pace Profile#: 1320

Site Location
STATE:

S

p

Section D

juired Client Information

SAMPLE ID

(A-Z, 0-9 /,-)

Sample IDs MUST BE UNIQUE tissue

Valid Matrix Codes

MATRIX

CODE

DRINKING WAT

DW

WATER

WT

WASTE WATE

WW

PRODUCT

p

SOIL/SOLID

SI...

Oil

OL

WIPE

WP

AIR

AR

OTHER

OT

TISSUE

TS

COLLECTED

COMPOSITE
START

COMPOSITE
END/GRAB



V>

Preservatives

Requested Analysis Filtered (Y/N)

I



2.

•ft

0®

A0 „

w

Pace Project HoJ Lab I.D.

FAG - A

WT



TB-al- r>*T

T&-02.-OG182.2~

WT

9

10

11

12

ADDITIONAL COMMENTS

RELINQUISHED BY / AFFILIATION

f Ate. (^~/v t'cy

tM



j~

a"

mi

DATE



ACCEPTED BY / AFFILIATION
		" ---

TIME

/ SAMPLE CONDITIONS

U9<*o

2J



y-

jL

L

O
O)

SAMPLER NAME AND SIGNATURE

PRINT Name of SAMPLER:

SIGNATURE of SAMPLER:

J A

DATE Signed
(MM/DDfYY):



"Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late oargf" of 1 5r,. pe-t month for any invoices not paid within 30 days

F-ALL-Q-02Qrev.08, 12-0ct-2007


-------
DG#_Title: ENV-FRM-LENE-0009_Sample Con S040064S

UO#: 60400849

!iillllil!l!lllllll!l

Revision: 2



Effective Date: 01/12/2022

issued By: Lenexa

Client Name:

Courier: FedEx jzf UPS ~ VIA ~ Clay ~ PEX ~ ECI ~ Pace ~ Xroads ~ Client ~ Other ~
Tracking#: 2.123 0V& 71 Bt	Pace Shipping Label Used? Yes^f No ~

'Custody Seal on Cooler/Box Present: Yesjzf'' No ~ Seals intact: Yesjzf'

Packing Material:
Thermometer Used:

Cooler Temperature (°C): As-read

No ~

Bubble Wrap ~ Bubble Bags	Foam ~

~T^q1	Type of Ice: yt/ej) Blue None

1L Corr. Factor ~\ 0 Corrected

No ~

None ~

W

Other

rflfLC

Onto and initials of person W /
Examining contents: L3~s/<~0(Zl

Chain of Custody present:

JZlYes

~ No

~ n/a



Chain of Custody relinquished:

jzfyes

~ No

~ n/a



Samples arrived within holding time:

^Yes

~ No

~ n/a



Short Hold Time analyses (<72hr):

~ Yes

_^No

~ n/a



Rush Turn Around Time requested:

~ Yes

^No

~ n/a



Sufficient volume:

^lYes

~ No

~ n/a



Correct containers used:

JZlYes

~ No

~ n/a



Pace containers used:

y^Yes

~ No

~ n/a



Containers intact: LS £lU>hX



JZTno

~n/a

I OectX'

Unpreserved 5035A / TX1005/1006 soils frozen in 48hrs?

~ Yes

~ No

^N/A



Filtered volume received for dissolved tests?

~Yes

~ No

^N/A



Sample labels match COC: Date / time / ID / analyses

J^Yes

~ No

~ n/a



Samples contain multiple phases? Matrix:K/f"

~Yes

j^No

~ n/a



Containers requiring pH preservation in compliance?
(HN03l H2S04, HCI<2; NaOH>9 Sulfide, NaOH>10 Cyanide)
(Exceptions: VOA, Micro, O&G. KS TPH. OK-DRO) LOT#:

jZ&es QNo

~ n/a

List sample IDs, volumes, lot #'s of preservative and the
date/time added.

Cyanide water sample checks:

Lead acetate strip turns dark? (Record only)

Potassium iodide test strip turns blue/purple? (Preserve)

~Yes
~Yes

~	No

~	No





Trip Blank present:

^Yes

~ No

~ n/a



Headspace in VOA vials ( >6mm):

~Yes

{^No

~ n/a



Samples from USDA Requlated Area: State:/! $

~Yes

^No

~ n/a



Additional labels attached to 5035A/ TX1005 vials in the field?

~ Yes

~ No

JZIn/A



Client Notification/ Resolution:
Person Contacted: _____
Comments/ Resolution:

Copy COC to Client?
Date/Time:

Y / N

Field Data Required?

Y / N

Project Manager Review:

Date:

Qualtrax Document ID: 30468

Page 1 of 1

Page 57 of 61


-------
DC#Jitle: ENV-FRM-LENE-0Q01_Sample Container Count
Revision: 3 | Effective Date: 12/22/2021 | Issued by: Lenexa

Client

Site:

Profile #

: Mews a;s+e)	_______ Notes		

ccc

Lmse Item

Matrix

I
O

CD
>

DG9H

DG9Q

VG9U

DG9U

DG9M

DG9B

BG1U

AG'IH

AG1U

AG2U

AG3S

AG4U

z>

to
O
<

JGFU

WGKU

WGDU



A

BP3U

8P1N

z

s?

CO

£
m

BP3S

BP3C

Ql

CO

z>
£
5

ZPLC

JZ

a





1

VTT







3































{



I



















2

urr







































i























3

wr

3





3































I

























UfT

3





































i























5

vrr

3





































I























6

sJT

f





3































f



1



















7

WT

3





3































I



I





















wr

3





































I























@

wr

3





1































I



1





















v/T

3





?































I



\



















11

uT

3





?































V



I



















'

wT

3





J































L



I



















Godts 	 	 	-	

Giass

Plastic



Misc.

DG9B

40mL bisulfate clear vial

WGKU

8oz clear soil jar

BP1C

1LNAOH plastic

I

Wipe/Swab

DG9H

40mL MCI amber voa vial

VvGfU ~

4oz clear soil jar

BP1N

1L HN03 plastic

SP5T

120ml Coiiform Na Thiosulfate

DG9M

40mL MeOH clear vial

WG2U

2oz clear soil iar

BP1S

1L H2S04 plastic

ZPLC

Ziploc Baq

DG9Q

40mL TSP amber via!

JGFU

4oz unpreserved amber wide

BP1U

1L unpreserved plastic

AF

Air Filter

DG9S

40mL H2S04 amber vial

AG0U

100mL unores amber qlass

BP1Z

1L NaOH, Zn Acetate

C

Air Cassettes

DG9T

40mL Na Thio amber vial

AG1H

1L HCI amber glass

BP2C

500mL NAOH plastic

R

Terracore Kit

DG9U

40mL amber unpreserved

AG1S

1L H2S04 amber glass

BP2N

500mL HN03 plastic

U

Summa Can

VG9H

40mL HCI clear vial

AG1T

1L Na Thiosulfate clear/amber glass

BP2S

500mL H2S04 plastic





VG9T

40mL Na Thio. clear vial

AG1U

1 liter unpres amber glass

BP2U

500mL unpreserved plastic





VG9U

40mL unpreserved clear vial

AG2N

500mL HN03 amber glass

BP2Z

500mL NaOH. Zn Acetate



Matrix

BG1S

1 liter H2S04 clear glass

AG2S

500mL H2S04 amber glass

BP3C

250mL NaOH plastic





BG1U

1 liter unpres glass

AG3S

250mL H2S04 amber qlass

BP3F

250mL HN03 plastic - field filtered

WT

Water

BG3H

250mL HCL Clear glass

AG2U

500mL unpres amber qlass

BP3N

250mL HN03 plastic

SL

SgM

BG3U

250mL Unpres Clear glass

AG3U

250mL unpres amber glass

BP3U

250mL unpreserved plastic

NAL

Non-aqueous Liquid

wr;ni i

Ifiny rfpar soil iar

AG4U

125mL unores amber qlass

BP3S

250m L H2S04 plastic

OL

Oil-



AG5U

100mL unpres amber qlass

BP3Z

BDjI! 1

250mL NaOH, Zn Acetate

WP

DW

Wipe

Drinkina Water

Work Order Number:

BP4N

125mL HN03 plastic

BP4S
WPDU

|125mL H2S04 plastic

i 16oz unpresserved plslic

o
O)

Quaitrax Document ID: 30422

Pace Analytical Services, LLC

Page 1 of 1


-------
DC#_Title: ENV-FRM-LENE-0001..Sample Container Count
Revision: 3 | Effective Date: 12/22/2021 | Issued by: Lenexa

Client:

				 Profile# ttla

Site: Mews lusi-S)	

Notes

coc

Line Item

1

ra

2

H60A

DG9H

%
CD
D

3
o>
0
>

DG9U

DG9M

DG9B

BG1U

AG1H

AG1U

IAG2U

AG3S

D

O
<

AG5U

IJGFU

WGKU

IWGDU

IBP1U

BP2U

IBP3U

z

CL
EG

5

0L

QQ

£
m

IBP3S



2

CD

3

£

§

ZPLC

Other





1

wT

3





3































i























•

wr

1

4rk

> M

























































3

wr

1

Jw

» hi*































































1



























































5

































































6

































































7

































































8

































































9

































































10

































































11

































































12

































































Container Codes

Glass

Plastic

Misc.

DG9B

40mL Disulfate clear vial

WGKU

8oz clear soil iar

BP1C

1L NAOH plastic

I

Wipe/Swab

DG9H

40mL HCl amber voa viai

WGFU

4oz clear soil iar

BP1N

1L HN03 plastic

SP5T

120mL Coliform Na Thiosulfate

DG9M

40mL MeOH clear vial

WG2U

2oz clear soil iar

BP1S

1LH2S04 plastic

ZPLC

Ziploc Bag

DG9Q

40mL TSP amber vial

JGFU

4oz unpreserved amber wide

BP1U

1L unpreserved plastic

AF

Air Filter

DG9S

40mL H2S04 amber vial

AG0U

10OmL unores amber class

BP1Z

1L NaOH. Zn Acetate

C

Air Cassettes

DG9T

40mL Na Thio amber vial

AG1H

1L HCl amber glass

BP2C

500mL NAOH plastic

R

Terra core Kit

DG9U

40mL amber unoreserved

AG1S

1L H2S04 amber glass

BP2N

500mL HN03 plastic

U

Summa Can

VG9H

40mL HCl clear vial

AG1T

1L Na Thiosulfate clear/amber qlass

BP2S

500m L H2S04 plastic





VG9T

40mL Na Thio. clear vial

AG1U

1 liter unpres amber glass

BP2U

500m L unpreserved plastic





VG9U

40mL unoreserved clear vial

AG2N

500mL HN03 amber glass

BP2Z

500mL NaOH. Zn Acetate

Matrix

BG1S

1 liter H2S04 clear glass

AG2S

5O0mL H2S04 amber glass

BP3C

250mL NaOH plastic

BG1U

1 liter unpres glass

AG3S

250mL H2S04 amber glass

BP3F

250mL HN03 plastic - field filtered

WT

Water

BG3H

250mL HCL Clear a lass

AG2U

500mL unpres amber glass

BP3N

250mL HN03 plastic

SL

Solid

BG3U

250mL Unores Clear glass

AG3U

250mL unores amber a lass

BP3U

250mL unpreserved plastic

NAL

Non-aqueous Liquid

WGDU

16oz clear soil jar

AG4U

125mL unores amber glass

BP3S

250m L H2S04 plastic

OL

OIL



AG5U

100mL unpres amber glass

BP3Z

250mL NaOH. Zn Acetate

WP

Wipe









BP4U

125mL unpreserved plastic

DW

Drinking Water









BP4N

125mL HN03 plastic













BP4S

125mL H2S04 plastic













WPDU

16oz unpresserved plstic





Work Order Number:

fl>
O)

o
O)

Qualtrax Document ID: 30422

Pace Analytical Services, LLC

Page 1 of 1


-------
Pace Analytical

CHAIN-OF-CUSTODY / Analytical Request Document

The Chain-of-Custody is a LEGAL DOCUMENT AH relevant fields must be completed accurately,.

Section A
Required Client information:

Section B
Required Project Information:

Section C

Invoice Information:

Page:



Of -O



L



Company: Ramboll Environ

Report To: Doug Burge

Attention:



			a	-M,			

Address: 1807 Park 270 Drive, Sta 450



",rTo' *****•*»- /rM

Company Name:

REGULATORY AGENCY

St. Louis, MO 63146



	



r NPDES T" GROUNDWATER r DRINKING WATER
r IIRT i" RCRA r OTHFR

Email To: dburqe(5>ramboll.com



chase Order No:



Phone: 314-513-1973 Fax:314-513-1951
Requested Due Date/TAT: ^

ject Name: NCWS (List A)
ject Number 1937680A

Pace hrojeci jamie Church

Pace Profile#: 1320

Site Location
STATE:

MO

11111111111111



Requested Analysis Filtered (Y/N)



ITEM#

Section D Valid Matrix Codes
Required Client Information MATRIX CODE
DRINKING WATER DW
WATER WT
WASTEWATER WW
PRODUCT P
SOIL/SOLID SL
OIL OL

SAMPLE ID »PE ^

(A-Z, 0-91 ,-) OTHER OT
Sample IDs MUST BE UNIQUE ts

MATRIX CODE (see valid codes to feft)

SAMPLE TYPE (G-GRA8 C=COMP)

COLLECTED

SAMPLE TEMP AT COLLECTION

# OF CONTAINERS

Preservatives

z

























COMPOSITE
START

FJaD-C? \b

T3
£
3
£
a.
c
D

0
to,

1

o
z

X

0

1

o

05

z

o

CO

6N

co

Z

o
c
cc
£

0
£
o

f Analysis Test J

/

€0

8
>

»

<~*»

"ro

iz



WT

G









io 1 "3-



8

>e



*

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x

X

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pag ^<5~U-n - Ai5D

WT

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lo iq.



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FAG -"3-^- -{"!•

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r

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WT

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Mm





<





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8

PAG-m

WT

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iffiD





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SkJ -01 - Wt - 11

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G









lb HO



H

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X









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10

- am i a ~ isJ ~ \%



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11



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*¦

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?

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>

















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tR-ci4.

WT

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\s













V









K



























ADDITIONAL COMMENTS

RELINQUISHED BY / AFFILIATION

DATE

TIME

ACCEPTED BY/AFFILIATION

DATE

TIME

SAMPLE CONDITIONS



f/W-> fi«"c



I6H





Ql'hl



^7-

N0 y y





































TJ

















CQ

cn
o
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cn
ho

SAMPLER NAME AND SIGNATURE

o

c
CL

E
©
H

: T5 —

c i ^

o CO #£. -S

-n 2 O c c ^
® ^ - « 2

,> "w >» £j7 ®

? S O O

ffi ^ 7S O C

q: 3 o «

o w

PRINT Name of SAMPLER: (j%^. M C'sk^-'X

SIGNATURE of SAMPLER: ^ •

os/h

'Important Note: By signing this torn you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1 5% per month for any invoices not paid within 30 <

F-ALL-Q-D20rev 08, 12-Oct-20G7


-------
-•®C7

- race Analytical

GHAIN-OF-CUSTODY /Analytical Request Document

The Chain-of-Custody is a LEGAL DOCUMENT All relevant fields must be completed accurately.

Section A

Required Client information:

Section B

Section C
Invoice information:

Page:

x - a,

Company: Ramboll Environ

£7

>ort To: Doug Burge

Attention:





Address: 1807 Park 270 Drive, Ste 450

»to: Uhj (9

Company Name:

REGULATORY AGENCY

St Louis, MO 63146





—	



P NPDES T GROUNDWATER T DRINKING WATER

Email To

dburae® ram boll.com

Purchase Order No.:





T UST 1 ' RCRA T OTHER











Phone: 314-513-1973 |Fax: 314-513-1951

Project Name: NCWS (List A)

Pace Profile#

Jamie Church

Site Location
STATE:

MO

¦¦¦

Requested Due Date/TAT: ^ \ ^

Project Number: 1937680A

1320



Requested Analysis Filtered (Y/N)



ITEM#

Section D Valid Matrix Codes
Required Client Information MATRIX CODE
DRiNKINQ WATER DW

WATER WT
WASTE WATER WW
PRODUCT P
SOIL/SOLID SL
Oil OL

SAMPLE ID ™PE

(A-Z, 0-91 ,-) OTHER OT
Sample IDs MUST BE UNIQUE tissue ts

o

TJ
O

To

>

©

LU
Q

8
><

£

1

o_

6

o

El

o

m
<

CD
ll

C5

LU
CL

h-

HI
Q.

s

<
W

COLLECTED

SAMPLE TEMP AT COLLECTION

# OF CONTAINERS

Preservatives

z

>

























COMPOSITE
START

COMPOSITE
END/GRAB

| Unpreserved |

d

X

o
z

X

I !0H I

X

0

1

i

| Methanol |

o>

(Analysis Test J.

VOCs

0
"TO

Sulfate

Chloride

Methane/Ethane/Ethene

Total Iron |













Residual Chlorine (Y/N)

Pace Project No./ Lab I.D.

DATE

TIME

DATE

TIME

1



WT

G











9s







<











X



























2

t«-oa -oifca-sis

WT

G





4*

(too



a







X





































3



WT

G

























































4



WT

G

























































5



WT

G

























































6



WT

G

























































7



WT

G

























































S



WT

G

























































9



WT

G

























































10



WT

G

























































11



WT

G

























































12



WT

G

























































ADDITIONAL COMMENTS

RELINQUISHED BY I AFFILIATION

DATE

TIME

ACCEPTED BY / AFFILIATION

DATE

TIME

SAMPLE CONDITIONS



Hie <-

fS3\



) J idju.

Q)iyO

} 9

/ ¦». lL>>



f

v

j



i



































TJ





















ige 51 of 52

SAMPLER NAME AND SIGNATURE

Temp in °C

Received on
Ice (¥/N)

Cooler (Y/N)

5

c —

CL

£

03

PRINT Name of SAMPLER: , C **C't 6

SIGNATURE of SAMPLER: .* .£?



'Important Note: By signing this form you are accepting Pace's NET 30 day payment terms and agreeing to late charges of 1 5% per month for any invoices not paid within 30

F-ALL.-Q-020rev.08,12-Oct-2O07


-------
DC#_Title: ENV-FRM-LENE-0009_Samplr 604008?

no# 60400877



Revision: 2

Effective Date: 01/12/2022

Issued By: Lenexa

Client Name:

Courier: FedEx s/ UPS ~ VIA ~ Clay ~ PEX ~ ECI ~ Pace ~ Xroads ~ Client ~ Other ~
Tracking #: 2,7 » t(,¦}.">. 0X	Pace Shipping Label Used? Yest/ No ~

Custody Seal on Cooler/Box Present: .Xes\zf No ~ Seals intact: Yesl^ No ~

Packing Material: Bubble Wrap W Bubble Bags {$)	Foam ~ None ~ Other [p/'Z,

Thermometer Used: Tl'0 I

Type of Ice: tfteQ Blue None

Cooler Temperature (°C): As-read	Corr. Factor—^	Corrected 1 \~L

/

pate and initials of person
Examining contents:".' /'

Chain of Custody present;



~ No

~ n/a



Chain of Custody relinquished'

f^Yes

~ No

~ n/a



Samples arrived within holding time:

Sfvas

~ No

~ n/a



Short Hold Time analyses («72lu):

®(Yes

~ No

~ n/a

afoy

Rush Turn Around Time requested:

~ Yes

H^o

~ n/a



Sufficient volume;

vO^es

~ No

~ n/a



Correct containers used;

Q^es

~ No

~ n/a



Pace containers used:

QVes

~ No

~ n/a



Containers intact:

\3ybs

~ No

~ n/a



Unpreserved 5035A / TX1005/1006 soils frozen in 48hrs?

~Yes

~ No

S^N/A



Filtered volume received for dissolved tests?

~ Yes

~ No

S^n/a



Sample labels match COC: Date / time / ID / analyses

Q^es

~ No

~n/a



Samples contain multiple phases? Matrix: \rSC

~Yes

[Mo

~ n/a



Containers requiring pH preservation in compliance?

(HMO,, H2S04, HCK2; NaOH>9 Sulfide, NaOH>10 Cyanide)

E^Yes

~ No

~ n/a

List sample IDs, volumes, lot #'s of preservative and the
date/time added.

(Exaenlions: VOA, Micro, O&G, KS TPH, OK-DHOS LOT#-

A l'"\







Cyanide water sample checks:









Lead acetate strip turns dark? (Record only)

~Yes

~ No





Potassium iodide test strip turns blue/purple? (Preserve)

~Yes

~ No





Trip Blank present;

KJ^es

~ No

~ n/a



Headspace in VOA vials ( >6mm);

~Yes

SJfho

~ n/a



Samples from USDA Requlaled Area: State;

~Yes

~ No

hWa



Additional labels attached to 5035A / TX1005 vials in the field?

~Yes

S^No

~ n/a



Person Contacted:
Communis/ Resolution:

Copy COC to Client?

Date/Time:

Y / N

Field Data Required? Y / N

Project Manager Review:

Date:

Qualtrax Document ID: 30468

Page 1 of 1

Page 49 of 52


-------
DC#_Title: ENV-FRM-LENE-0001__Sample Container Count
Revision: 3 | Effective Date: | Issued by: Lenexa

dient: Rov/*\ \>Q 1 I t ft \/l	^	Profile# ^10

Slte: h/V^ ^	A )

COC
Line Item

Matrix

£
5

DG9H

DG9Q
VG9U

=5

Ui

o

Q

DG9M

m

CD
O

BG1U

AG1H

IAG1U

IAG2U

IAG3S

AG4U

Z>
to

0

<

JGFU

D

i

WGDU
BP1U

8P2U

BP3U

BP1N

BP3N

BP3F

BP3S

BP3C
BP3Z

O
Q

CL
£

ZPLC

Other





1

sHT

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i y





























1



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j











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>



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t

























7

II





























































£

I

'3



































X























g

;





3



































a



















10



3



























































11

i



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PkM*X

, -j-

-01



















































, 2



X-

mi

? b .

¦re ¦

02 1

















































Container Codes

Glass

Plastic

Misc.

DG9B

40mL bisulfate clear vial

WGKU

Soz clear soil jar

BP1C

1L NAOH plastic

i

Wipe/Swab

DG9H

40mL HCI amber voa vial

WGFU

4oz clear soil iar

BP1N

1L HN03 plastic

SP5T

120mL Coliform Na Thiosulfate

DG9M

40mL MeOH clear vial

WG2U

2oz clear soil jar

BP1S

1L H2S04 plastic

ZPLC

Ziploc Baa

DG9Q

40mL TSP amber vial

JGFU

4oz unpreserved amber wide

BP1U

1L unpreserved plastic

AF

Air Filter

DG9S

40mL H2S04 amber vial

AG0U

100mL unores amber glass

BP1Z

1L NaOH. Zn Acetate

C

Air Cassettes

DG9T

40mL Na Th o amber vial

AG1H

1L HCI amber alass

BP2C

500mL NAOH plastic

R

Terracore Kit

DG9U

40mL amber unpreserved

AG1S

1L H2S04 amber glass

BP2N

500mL HN03 plastic

U

Summa Can

VG9H

40mL HCI clear vial

AG1T

1L Na Thiosulfate clear/amber glass

BP2S

500mL H2S04 plastic





VG9T

40mL Na Th o. clear vial

AG1U

1 liter unpres amber glass

BP2U

500mL unpreserved plastic





VG9U

40mL unpreserved clear vial

AG2N

500mL HN03 amber alass

BP2Z

5G0mL NaOH. Zn Acetate

Matrix

BG1S

1 liter H2S04 clear glass

AG2S

500mL H2S04 amber class

BP3C

250mL NaOH plastic

BG1U

1 liter unpres glass

AG3S

250mL H2S04 amber glass

BP3F

250mL HN03 Dlastic - field filtered

WT

Water

BG3H

250mL HCL Clear glass

AG2U

500mL unpres amber glass



250mL HN03 plastic

SL

Solid

BG3U

250mL Unprss Clear qlass

AG3U

250mL unpres amber glass

BP3U

250mL unpreserved plastic

NAL

Non-aqueous Liquid

WGDU

16oz clear soil iar

AG4U

125mL unpres amber glass

BP3S

250mL H2S04 plastic

OL

OIL



AG5U

100mL unpres amber glass

BP3Z

250mL NaOH, Zn Acetate

WP

Wipe









BP4U

125mL unpreserved plastic

DW

Drinking Water









BP4N

125mL HN03 plastic













BP4S

125mL H2S04 plastic













WPDU

16oz unpresserved plstic



Work Order Number:



Qualtrax Document ID: 30422

Pace Analytical Services, LLC

Page 1 of 1


-------
SECTION 5
PROJECT CORRESPONDENCE


-------
From:

To:

Cc:

Subject:

Date:

Attachments:

Jamie Church
Douglas M. Burae

Caroline Rowshan: Ian McOuaia: Caroline Chavers: Erin Rodaers

RE: NCWS 2022 GW

Tuesday, July 19, 2022 11:24:49 AM

imaae003.pna

RL 60MSV8 052622.pdf

This sender is trusted.

Attached is the runlog from 05/26/22. That batch/sample is on the 2nd page of the pdf. I highlighted
the sample and the pH.

All Rush requests must be pre-approved by the laboratory. Please contact me before submitting
a Rush project.

Jamie Church

Project Management Lead | St. Louis Service Center Manager
O: 314.838.7223 | M: 314.413.6227 | nacelahs.com

PROCESS PAYMENTS ONLINE - Online Bill Pav

From: Douglas M. Burge 

Sent: Tuesday, July 19, 2022 9:51 AM

To: Jamie Church 

Cc: Caroline Rowshan ; Ian McQuaig ;
Caroline Chavers ; Erin Rodgers 

Subject: RE: NCWS 2022 GW

CAUTION: This email originated from outside Pace Analytical. Do not click links or open
attachments unless you recognize the sender and know the content is safe.

Thank you Jamie,

Can you provide a copy of the logbook page with pH entries so that our validators can confirm there
was no transcription error?

Doug

Doug M. Burge, RG, PG

Senior Manager
D +1 314 5902963
M +1 314 3788065


-------
From: Jamie Church 

Sent: Tuesday, July 19, 2022 8:07 AM

To: Douglas M. Burge 

Cc: Caroline Rowshan : Ian McQuaig :

Caroline Chavers : Erin Rodgers 

Subject: RE: NCWS 2022 GW

Doug, the lab has informed me that the sample has already been disposed of so we cannot verify the
sample pH.

All Rush requests must be pre-approved by the laboratory. Please contact me before submitting
a Rush project.

Jamie Church

Project Management Lead | St. Louis Service Center Manager
O: 314.838.7223 | M: 314.413.6227 | nacelahs.com

PROCESS PAYMENTS ONLINE - Online Bill Pav

From: Douglas M. Burge 

Sent: Monday, July 11, 2022 10:30 AM

To: Jamie Church 

Cc: Caroline Rowshan : Ian McQuaig <1 MCQUAlG@ramboll.com>:
Caroline Chavers : Erin Rodgers 

Subject: FW: NCWS 2022 GW

CAUTION: This email originated from outside Pace Analytical. Do not click links or open
attachments unless you recognize the sender and know the content is safe.

Hi Jamie,

Please review and respond to the data inquiry described below from Environmental Standards with
regard to the attached analytical sample for the Newton County Wells Site.

Thank you, Doug

Doug M. Burge, RG, PG

Senior Manager
D +1 314 5902963
M +1 314 3788065

From: Caroline Rowshan 
Sent: Monday, July 11, 2022 10:01 AM


-------
To: Douglas M. Burge 

Cc: Ian McQuaig <1MCGUA1G(5)ramboll.com>: Caroline Chavers : Erin
Rodgers 

Subject: RE: NCWS 2022 GW

Hi Doug:

We have a data inquiry to send to the laboratory. Please see below and attached.

SDG 60400849

1. For sample FAG-34-W-17 (Lab ID 60400849009), the lab has reported a pH of 6 (see attached
Form 1). Please ask the lab to confirm that this pH was correctly reported as all other samples
report a pH < 2. Qualification may be needed if this sample was not properly preserved for VOCs.

Thanks,

Caroline Rowshan
Environmental Standards, Inc.

610.935.5577x415

From: Douglas M. Burge 

Sent: Tuesday, June 21, 2022 11:35 AM
To: Erin Rodgers 

Cc: Caroline Rowshan : Ian McQuaig <1 MCQUAlG@ramboll.com>:
Caroline Chavers 

Subject: NCWS 2022 GW

Hello Erin,

Attached are the groundwater analytical reports for the Newton County Wells Site project from the
2022 annual monitoring event. As previously discussed, we will need the VOC data validated as
conducted for previous analytical. EPA asked that we include the MDL moving forward, so that is
included in the reports this year.

Thanks, Doug

Doug M. Burge, RG, PG

Senior Manager
D + 314.590.2963
M + 314.378.8065
dburae@ramboll.com

Ramboll

1807 Park 270 Drive, Suite 450
St. Louis, MO 63146
www.ramboll.com


-------
NOTICE— The contents of this email and any attachments may contain confidential,
privileged, and/or legally protected information and are for the sole use of the addressee (s).
Any review or distribution by others is strictly prohibited. If you are not the intended recipient,
please contact the sender immediately and delete any copies.

^ Please consider the environment before printing this email

NOTICE— The contents of this email and any attachments may contain confidential,
privileged, and/or legally protected information and are for the sole use of the addressee (s).
Any review or distribution by others is strictly prohibited. If you are not the intended recipient,
please contact the sender immediately and delete any copies.

^ Please consider the environment before printing this email


-------
%ce Analytical*

www.p&G&t&bs com

60MSV8 INSTRUMENT SEQUENCE LOG
Analysis Method: o, 2 to

Instrument Batch:

Date
VOC ICAL

C>!S I 1 (.!*'¦>¦

i»GRO

File

001

002

Sample No.

Position
Verified

Batch

Dilution

_e.H

IS

ss

Comments







- - -

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003

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12-hr Tune Start pi :oe\
Stop n ¦?>

JJJJtLlX-

Page 144 of 150


-------
Paco Analytical

/Jif t ^Co- r?

60MSV8 INSTRUMENT SEQUENCE LOG

Instrument Batch:

Analysis Method

Dat- IJLl
VOC1CAL;

Ot" <' 1

H,!7 *

' j-i' bGR0

File

001

002

003

004

005

006

007

008

009

010

011

012

013

014

015

016

017

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019

020

021

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024.

025

026

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Sample No.

Position

Verified

¦>/



Batch

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.PtL

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043

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90





o o 	9o/3

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/ A/£,77

Page 146 of 150


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Temporal Trend Analysis Data Input and Output

December 2022


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Full MNA Data Set

December 2022


-------
MANN KENDALL ANALYSIS OUTPUT

Location

Samples

Min Date

Max Date

cis-l,2-Dichloroethene

Trichloroethene

Vinyl chloride

FAG-05

17

2008-10-2100:00:00

2022-05-18 00:00:00

Decreasing (p=0.002)

Decreasing (p=0.001)

All ND

FAG-11

17

2008-10-23 00:00:00

2022-05-18 00:00:00

Decreasing (p=<0.001)

Decreasing (p=<0.001)

All ND

FAG-22

17

2008-10-23 00:00:00

2022-05-19 00:00:00

Decreasing (p=<0.001)

Stable (p=0.435, cv=0.381)

Decreasing (p=0.008)

FAG-31

17

2008-10-23 00:00:00

2022-05-19 00:00:00

Increasing (p=0.004)

Stable (p=0.370, cv=0.133)

Stable (p=0.181, cv=0.711)

FAG-32

17

2008-10-22 00:00:00

2022-05-18 00:00:00

Stable (p=0.282, cv=0.461)

Stable (p=0.108, cv=0.446)


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-05

10/21/2008

cis-1,2-Dichloroethene

16.7

ug/L



FAG-05

4/29/2009

cis-1,2-Dichloroethene

14.7

ug/L



FAG-05

10/15/2009

cis-1,2-Dichloroethene

17.3

ug/L



FAG-05

4/28/2010

cis-1,2-Dichloroethene

10.7

ug/L



FAG-05

10/21/2010

cis-1,2-Dichloroethene

21.8

ug/L



FAG-05

4/27/2011

cis-1,2-Dichloroethene

8.6

ug/L



FAG-05

10/26/2011

cis-1,2-Dichloroethene

17.4

ug/L



FAG-05

5/2/2012

cis-1,2-Dichloroethene

8.1

ug/L



FAG-05

10/10/2012

cis-1,2-Dichloroethene

14

ug/L



FAG-05

5/15/2013

cis-1,2-Dichloroethene

6.1

ug/L



FAG-05

10/21/2008

Tr

chloroethene

94.2

ug/L



FAG-05

4/29/2009

Tr

chloroethene

88.1

ug/L



FAG-05

10/15/2009

Tr

chloroethene

63.6

ug/L

J

FAG-05

4/28/2010

Tr

chloroethene

64.4

ug/L



FAG-05

10/21/2010

Tr

chloroethene

87.5

ug/L



FAG-05

4/27/2011

Tr

chloroethene

47.8

ug/L



FAG-05

10/26/2011

Tr

chloroethene

77.6

ug/L



FAG-05

5/2/2012

Tr

chloroethene

44

ug/L



FAG-05

10/10/2012

Tr

chloroethene

62

ug/L



FAG-05

5/15/2013

Tr

chloroethene

35.9

ug/L



FAG-05

10/21/2008

Vinyl chloride

1

ug/L

U

FAG-05

4/29/2009

Vinyl chloride

1

ug/L

U

FAG-05

10/15/2009

Vinyl chloride

1

ug/L

u

FAG-05

4/28/2010

Vinyl chloride

1

ug/L

u

FAG-05

10/21/2010

Vinyl chloride

1

ug/L

u

FAG-05

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-05

10/26/2011

Vinyl chloride

1

ug/L

u

FAG-05

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-05

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-05

5/15/2013

Vinyl chloride

1

ug/L

u

FAG-11

10/23/2008

cis-1,2-Dichloroethene

2.7

ug/L



FAG-11

4/29/2009

cis-1,2-Dichloroethene

2.2

ug/L



FAG-11

10/14/2009

cis-1,2-Dichloroethene

2.5

ug/L



FAG-11

4/27/2010

cis-1,2-Dichloroethene

1.7

ug/L



FAG-11

10/19/2010

cis-1,2-Dichloroethene

2.5

ug/L



FAG-11

5/5/2011

cis-1,2-Dichloroethene

2.2

ug/L



FAG-11

10/26/2011

cis-1,2-Dichloroethene

2.9

ug/L



FAG-11

5/3/2012

cis-1,2-Dichloroethene

2.2

ug/L



FAG-11

10/10/2012

cis-1,2-Dichloroethene

2

ug/L



FAG-11

5/14/2013

cis-1,2-Dichloroethene

1.5

ug/L



FAG-11

10/23/2008

Tr

chloroethene

18.4

ug/L



FAG-11

4/29/2009

Tr

chloroethene

11.4

ug/L



FAG-11

10/14/2009

Tr

chloroethene

15.8

ug/L



FAG-11

4/27/2010

Tr

chloroethene

10.6

ug/L



FAG-11

10/19/2010

Tr

chloroethene

15.2

ug/L



FAG-11

5/5/2011

Tr

chloroethene

13.7

ug/L



FAG-11

10/26/2011

Tr

chloroethene

15.1

ug/L



FAG-11

5/3/2012

Tr

chloroethene

13.5

ug/L



FAG-11

10/10/2012

Tr

chloroethene

10.8

ug/L



FAG-11

5/14/2013

Tr

chloroethene

8

ug/L



FAG-11

10/23/2008

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-11

4/29/2009

FAG-11

10/14/2009

FAG-11

4/27/2010

FAG-11

10/19/2010

FAG-11

5/5/2011

FAG-11

10/26/2011

FAG-11

5/3/2012

FAG-11

10/10/2012

FAG-11

5/14/2013

FAG-22

10/23/2008

FAG-22

5/21/2009

FAG-22

10/16/2009

FAG-22

4/29/2010

FAG-22

10/21/2010

FAG-22

4/28/2011

FAG-22

10/28/2011

FAG-22

5/3/2012

FAG-22

10/11/2012

FAG-22

5/16/2013

FAG-22

10/23/2008

FAG-22

5/21/2009

FAG-22

10/16/2009

FAG-22

4/29/2010

FAG-22

10/21/2010

FAG-22

4/28/2011

FAG-22

10/28/2011

FAG-22

5/3/2012

FAG-22

10/11/2012

FAG-22

5/16/2013

FAG-22

10/23/2008

FAG-22

5/21/2009

FAG-22

10/16/2009

FAG-22

4/29/2010

FAG-22

10/21/2010

FAG-22

4/28/2011

FAG-22

10/28/2011

FAG-22

5/3/2012

FAG-22

10/11/2012

FAG-22

5/16/2013

FAG-31

10/23/2008

FAG-31

5/21/2009

FAG-31

10/15/2009

FAG-31

4/29/2010

FAG-31

10/21/2010

FAG-31

4/28/2011

FAG-31

10/27/2011

FAG-31

5/3/2012

FAG-31

10/11/2012

FAG-31

5/16/2013

FAG-31

10/23/2008

FAG-31

5/21/2009

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

581

ug/L



852

ug/L



694

ug/L



703

ug/L



588

ug/L



681

ug/L



608

ug/L



531

ug/L



528

ug/L



477

ug/L



1120

ug/L



1230

ug/L



1110

ug/L



932

ug/L



788

ug/L



1280

ug/L



1410

ug/L



1300

ug/L



1660

ug/L



1510

ug/L



47.2

ug/L



144

ug/L



80.9

ug/L



133

ug/L



108

ug/L



127

ug/L



101

ug/L



117

ug/L



80.7

ug/L



60.8

ug/L



116

ug/L



182

ug/L



184

ug/L



166

ug/L



170

ug/L



168

ug/L



168

ug/L



161

ug/L



201

ug/L



196

ug/L



791

ug/L



861

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

FAG-31

10/15/2009

Trichloroethene

1070

ug/L



FAG-31

4/29/2010

Trichloroethene

719

ug/L



FAG-31

10/21/2010

Trichloroethene

653

ug/L



FAG-31

4/28/2011

Trichloroethene

698

ug/L



FAG-31

10/27/2011

Trichloroethene

698

ug/L



FAG-31

5/3/2012

Trichloroethene

698

ug/L



FAG-31

10/11/2012

Trichloroethene

705

ug/L



FAG-31

5/16/2013

Trichloroethene

724

ug/L



FAG-31

10/23/2008

Vinyl chloride

10

ug/L



FAG-31

5/21/2009

Vinyl chloride

1

ug/L

U

FAG-31

10/15/2009

Vinyl chloride

1

ug/L

u

FAG-31

4/29/2010

Vinyl chloride

10

ug/L

u

FAG-31

10/21/2010

Vinyl chloride

10

ug/L

u

FAG-31

4/28/2011

Vinyl chloride

10

ug/L

u

FAG-31

10/27/2011

Vinyl chloride

1

ug/L

u

FAG-31

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-31

10/11/2012

Vinyl chloride

1

ug/L

u

FAG-31

5/16/2013

Vinyl chloride

1

ug/L

u

FAG-32

10/22/2008

cis-1,2-Dichloroethene

363

ug/L



FAG-32

5/20/2009

cis-1,2-Dichloroethene

313

ug/L



FAG-32

10/13/2009

cis-1,2-Dichloroethene

375

ug/L



FAG-32

4/29/2010

cis-1,2-Dichloroethene

338

ug/L



FAG-32

10/19/2010

cis-1,2-Dichloroethene

347

ug/L



FAG-32

4/28/2011

cis-1,2-Dichloroethene

396

ug/L



FAG-32

10/25/2011

cis-1,2-Dichloroethene

406

ug/L



FAG-32

5/1/2012

cis-1,2-Dichloroethene

401

ug/L



FAG-32

10/9/2012

cis-1,2-Dichloroethene

487

ug/L



FAG-32

5/16/2013

cis-1,2-Dichloroethene

389

ug/L



FAG-32

10/22/2008

Trichloroethene

1730

ug/L



FAG-32

5/20/2009

Trichloroethene

1500

ug/L



FAG-32

10/13/2009

Trichloroethene

1670

ug/L



FAG-32

4/29/2010

Trichloroethene

1630

ug/L



FAG-32

10/19/2010

Trichloroethene

1590

ug/L



FAG-32

4/28/2011

Trichloroethene

1690

ug/L



FAG-32

10/25/2011

Trichloroethene

1620

ug/L



FAG-32

5/1/2012

Trichloroethene

1670

ug/L



FAG-32

10/9/2012

Trichloroethene

1770

ug/L



FAG-32

5/16/2013

Trichloroethene

1380

ug/L



FAG-32

10/22/2008

Vinyl chloride

1

ug/L

u

FAG-32

5/20/2009

Vinyl chloride

1

ug/L

u

FAG-32

10/13/2009

Vinyl chloride

1

ug/L

u

FAG-32

4/29/2010

Vinyl chloride

1

ug/L

u

FAG-32

10/19/2010

Vinyl chloride

25

ug/L

u

FAG-32

4/28/2011

Vinyl chloride

20

ug/L

u

FAG-32

10/25/2011

Vinyl chloride

20

ug/L

u

FAG-32

5/1/2012

Vinyl chloride

1

ug/L

u

FAG-32

10/9/2012

Vinyl chloride

20

ug/L

u

FAG-32

5/16/2013

Vinyl chloride

20

ug/L

u

FAG-33

10/20/2008

cis-1,2-Dichloroethene

2.6

ug/L



FAG-33

4/28/2009

cis-1,2-Dichloroethene

2.3

ug/L



FAG-33

10/14/2009

cis-1,2-Dichloroethene

3

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-33

4/27/2010

cis-1,2-Dichloroethene

3

ug/L



FAG-33

10/20/2010

cis-1,2-Dichloroethene

2.8

ug/L



FAG-33

4/27/2011

cis-1,2-Dichloroethene

3.3

ug/L



FAG-33

10/27/2011

cis-1,2-Dichloroethene

2.7

ug/L



FAG-33

5/2/2012

cis-1,2-Dichloroethene

2.3

ug/L



FAG-33

10/11/2012

cis-1,2-Dichloroethene

2.3

ug/L



FAG-33

5/14/2013

cis-1,2-Dichloroethene

2.8

ug/L



FAG-33

10/20/2008

Tr

chloroethene

19.5

ug/L



FAG-33

4/28/2009

Tr

chloroethene

20.5

ug/L



FAG-33

10/14/2009

Tr

chloroethene

20.2

ug/L



FAG-33

4/27/2010

Tr

chloroethene

26.6

ug/L



FAG-33

10/20/2010

Tr

chloroethene

26.1

ug/L



FAG-33

4/27/2011

Tr

chloroethene

29.2

ug/L



FAG-33

10/27/2011

Tr

chloroethene

20.2

ug/L



FAG-33

5/2/2012

Tr

chloroethene

19.7

ug/L



FAG-33

10/11/2012

Tr

chloroethene

17.3

ug/L



FAG-33

5/14/2013

Tr

chloroethene

23.9

ug/L



FAG-33

10/20/2008

Vinyl chloride

1

ug/L

U

FAG-33

4/28/2009

Vinyl chloride

1

ug/L

U

FAG-33

10/14/2009

Vinyl chloride

1

ug/L

u

FAG-33

4/27/2010

Vinyl chloride

1

ug/L

u

FAG-33

10/20/2010

Vinyl chloride

1

ug/L

u

FAG-33

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-33

10/27/2011

Vinyl chloride

1

ug/L

u

FAG-33

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-33

10/11/2012

Vinyl chloride

1

ug/L

u

FAG-33

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-34

10/22/2008

cis-1,2-Dichloroethene

442

ug/L



FAG-34

4/29/2009

cis-1,2-Dichloroethene

403

ug/L



FAG-34

10/14/2009

cis-1,2-Dichloroethene

384

ug/L



FAG-34

4/27/2010

cis-1,2-Dichloroethene

399

ug/L



FAG-34

10/20/2010

cis-1,2-Dichloroethene

421

ug/L



FAG-34

4/27/2011

cis-1,2-Dichloroethene

380

ug/L



FAG-34

10/27/2011

cis-1,2-Dichloroethene

345

ug/L



FAG-34

5/2/2012

cis-1,2-Dichloroethene

341

ug/L



FAG-34

10/11/2012

cis-1,2-Dichloroethene

358

ug/L



FAG-34

5/15/2013

cis-1,2-Dichloroethene

337

ug/L



FAG-34

10/22/2008

Tr

chloroethene

882

ug/L



FAG-34

4/29/2009

Tr

chloroethene

992

ug/L



FAG-34

10/14/2009

Tr

chloroethene

804

ug/L

J

FAG-34

4/27/2010

Tr

chloroethene

777

ug/L



FAG-34

10/20/2010

Tr

chloroethene

712

ug/L



FAG-34

4/27/2011

Tr

chloroethene

777

ug/L



FAG-34

10/27/2011

Tr

chloroethene

761

ug/L



FAG-34

5/2/2012

Tr

chloroethene

758

ug/L



FAG-34

10/11/2012

Tr

chloroethene

820

ug/L



FAG-34

5/15/2013

Tr

chloroethene

713

ug/L



FAG-34

10/22/2008

Vinyl chloride

13.6

ug/L



FAG-34

4/29/2009

Vinyl chloride

6.9

ug/L

J

FAG-34

10/14/2009

Vinyl chloride

12.2

ug/L

J

FAG-34

4/27/2010

Vinyl chloride

14.9

ug/L




-------
MANN KENDALL INPUT

Well ID	Sample Date	Sample	Value

FAG-34	10/20/2010	Vinyl chloride	15

FAG-34	4/27/2011	Vinyl chloride	11.6

FAG-34	10/27/2011	Vinyl chloride	10

FAG-34	5/2/2012	Vinyl chloride	12.2

FAG-34	10/11/2012	Vinyl chloride	6.2

FAG-34	5/15/2013	Vinyl chloride	6.7

FAG-35	10/23/2008	cis-1,2-Dichloroethene	126

FAG-35	4/29/2009	cis-1,2-Dichloroethene	121

FAG-35	10/15/2009	cis-1,2-Dichloroethene	122

FAG-35	4/28/2010	cis-1,2-Dichloroethene	171

FAG-35	10/20/2010	cis-1,2-Dichloroethene	134

FAG-35	4/27/2011	cis-1,2-Dichloroethene	173

FAG-35	10/27/2011	cis-1,2-Dichloroethene	147

FAG-35	5/2/2012	cis-1,2-Dichloroethene	125

FAG-35	10/11/2012	cis-1,2-Dichloroethene	134

FAG-35	5/15/2013	cis-1,2-Dichloroethene	124

FAG-35	10/23/2008	Trichloroethene	484

FAG-35	4/29/2009	Trichloroethene	510

FAG-35	10/15/2009	Trichloroethene	542

FAG-35	4/28/2010	Trichloroethene	602

FAG-35	10/20/2010	Trichloroethene	446

FAG-35	4/27/2011	Trichloroethene	583

FAG-35	10/27/2011	Trichloroethene	499

FAG-35	5/2/2012	Trichloroethene	436

FAG-35	10/11/2012	Trichloroethene	467

FAG-35	5/15/2013	Trichloroethene	429

FAG-35	10/23/2008	Vinyl chloride	1

FAG-35	4/29/2009	Vinyl chloride	10

FAG-35	10/15/2009	Vinyl chloride	1

FAG-35	4/28/2010	Vinyl chloride	1

FAG-35	10/20/2010	Vinyl chloride	10

FAG-35	4/27/2011	Vinyl chloride	10

FAG-35	10/27/2011	Vinyl chloride	10

FAG-35	5/2/2012	Vinyl chloride	1

FAG-35	10/11/2012	Vinyl chloride	5

FAG-35	5/15/2013	Vinyl chloride	5

FAG-36	10/22/2008	cis-1,2-Dichloroethene	104

FAG-36	5/20/2009	cis-1,2-Dichloroethene	42.2

FAG-36	10/16/2009	cis-1,2-Dichloroethene	80.8

FAG-36	4/28/2010	cis-1,2-Dichloroethene	158

FAG-36	10/21/2010	cis-1,2-Dichloroethene	182

FAG-36	4/27/2011	cis-1,2-Dichloroethene	173

FAG-36	10/27/2011	cis-1,2-Dichloroethene	192

FAG-36	5/3/2012	cis-1,2-Dichloroethene	155

FAG-36	10/11/2012	cis-1,2-Dichloroethene	183

FAG-36	5/15/2013	cis-1,2-Dichloroethene	234

FAG-36	10/22/2008	Trichloroethene	565

FAG-36	5/20/2009	Trichloroethene	166

FAG-36	10/16/2009	Trichloroethene	366

FAG-36	4/28/2010	Trichloroethene	477

FAG-36	10/21/2010	Trichloroethene	286

Units Qualifier

ug/L
ug/L J
ug/L U
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L
ug/L


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-36

4/27/2011

Trichloroethene

594

ug/L



FAG-36

10/27/2011

Trichloroethene

524

ug/L



FAG-36

5/3/2012

Trichloroethene

456

ug/L



FAG-36

10/11/2012

Trichloroethene

508

ug/L



FAG-36

5/15/2013

Trichloroethene

567

ug/L



FAG-36

10/22/2008

Vinyl chloride

5

ug/L

U

FAG-36

5/20/2009

Vinyl chloride

1

ug/L

U

FAG-36

10/16/2009

Vinyl chloride

5

ug/L

u

FAG-36

4/28/2010

Vinyl chloride

10

ug/L

u

FAG-36

10/21/2010

Vinyl chloride

2

ug/L

u

FAG-36

4/27/2011

Vinyl chloride

10

ug/L

u

FAG-36

10/27/2011

Vinyl chloride

10

ug/L

u

FAG-36

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-36

10/11/2012

Vinyl chloride

10

ug/L

u

FAG-36

5/15/2013

Vinyl chloride

10

ug/L

u

FAG-43

10/21/2008

cis-1,2-Dichloroethene

106

ug/L



FAG-43

4/28/2009

cis-1,2-Dichloroethene

87.1

ug/L



FAG-43

10/15/2009

cis-1,2-Dichloroethene

110

ug/L



FAG-43

4/30/2010

cis-1,2-Dichloroethene

105

ug/L



FAG-43

10/19/2010

cis-1,2-Dichloroethene

106

ug/L



FAG-43

4/26/2011

cis-1,2-Dichloroethene

82.1

ug/L



FAG-43

10/26/2011

cis-1,2-Dichloroethene

91.8

ug/L



FAG-43

5/3/2012

cis-1,2-Dichloroethene

1

ug/L

u

FAG-43

10/10/2012

cis-1,2-Dichloroethene

3.2

ug/L



FAG-43

5/15/2013

cis-1,2-Dichloroethene

1

ug/L

u

FAG-43

10/21/2008

Tr

chloroethene

338

ug/L



FAG-43

4/28/2009

Tr

chloroethene

275

ug/L



FAG-43

10/15/2009

Tr

chloroethene

438

ug/L



FAG-43

4/30/2010

Tr

chloroethene

330

ug/L



FAG-43

10/19/2010

Tr

chloroethene

395

ug/L



FAG-43

4/26/2011

Tr

chloroethene

313

ug/L



FAG-43

10/26/2011

Tr

chloroethene

289

ug/L



FAG-43

5/3/2012

Tr

chloroethene

1

ug/L

u

FAG-43

10/10/2012

Tr

chloroethene

12.2

ug/L



FAG-43

5/15/2013

Tr

chloroethene

1

ug/L

u

FAG-43

10/21/2008

Vinyl chloride

1

ug/L

u

FAG-43

4/28/2009

Vinyl chloride

1

ug/L

u

FAG-43

10/15/2009

Vinyl chloride

1

ug/L

u

FAG-43

4/30/2010

Vinyl chloride

1

ug/L

u

FAG-43

10/19/2010

Vinyl chloride

5

ug/L

u

FAG-43

4/26/2011

Vinyl chloride

5

ug/L

u

FAG-43

10/26/2011

Vinyl chloride

5

ug/L

u

FAG-43

5/3/2012

Vinyl chloride

5

ug/L

u

FAG-43

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-43

5/15/2013

Vinyl chloride

1

ug/L

u

FAG-46

10/21/2008

cis-1,2-Dichloroethene

12.8

ug/L



FAG-46

4/28/2009

cis-1,2-Dichloroethene

9.1

ug/L



FAG-46

10/15/2009

cis-1,2-Dichloroethene

9.1

ug/L



FAG-46

4/29/2010

cis-1,2-Dichloroethene

7.4

ug/L



FAG-46

10/19/2010

cis-1,2-Dichloroethene

9.8

ug/L



FAG-46

4/26/2011

cis-1,2-Dichloroethene

7

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-46

10/27/2011

cis-1,2-Dichloroethene

6.9

ug/L



FAG-46

5/3/2012

cis-1,2-Dichloroethene

4.6

ug/L



FAG-46

10/10/2012

cis-1,2-Dichloroethene

5.1

ug/L



FAG-46

5/14/2013

cis-1,2-Dichloroethene

3.5

ug/L



FAG-46

10/21/2008

Tr

chloroethene

202

ug/L



FAG-46

4/28/2009

Tr

chloroethene

167

ug/L



FAG-46

10/15/2009

Tr

chloroethene

119

ug/L



FAG-46

4/29/2010

Tr

chloroethene

107

ug/L



FAG-46

10/19/2010

Tr

chloroethene

146

ug/L



FAG-46

4/26/2011

Tr

chloroethene

134

ug/L



FAG-46

10/27/2011

Tr

chloroethene

135

ug/L



FAG-46

5/3/2012

Tr

chloroethene

103

ug/L



FAG-46

10/10/2012

Tr

chloroethene

130

ug/L



FAG-46

5/14/2013

Tr

chloroethene

70.2

ug/L



FAG-46

10/21/2008

Vinyl chloride

1

ug/L

U

FAG-46

4/28/2009

Vinyl chloride

1

ug/L

U

FAG-46

10/15/2009

Vinyl chloride

1

ug/L

u

FAG-46

4/29/2010

Vinyl chloride

1

ug/L

u

FAG-46

10/19/2010

Vinyl chloride

1

ug/L

u

FAG-46

4/26/2011

Vinyl chloride

1

ug/L

u

FAG-46

10/27/2011

Vinyl chloride

1

ug/L

u

FAG-46

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-46

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-46

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-47

10/21/2008

cis-1,2-Dichloroethene

14.3

ug/L



FAG-47

4/29/2009

cis-1,2-Dichloroethene

9.9

ug/L



FAG-47

10/13/2009

cis-1,2-Dichloroethene

12.5

ug/L



FAG-47

4/27/2010

cis-1,2-Dichloroethene

9.3

ug/L



FAG-47

10/20/2010

cis-1,2-Dichloroethene

11.9

ug/L



FAG-47

4/27/2011

cis-1,2-Dichloroethene

9.5

ug/L



FAG-47

10/27/2011

cis-1,2-Dichloroethene

8.8

ug/L



FAG-47

5/3/2012

cis-1,2-Dichloroethene

9.1

ug/L



FAG-47

10/9/2012

cis-1,2-Dichloroethene

9.7

ug/L



FAG-47

5/14/2013

cis-1,2-Dichloroethene

9.9

ug/L



FAG-47

10/21/2008

Tr

chloroethene

160

ug/L



FAG-47

4/29/2009

Tr

chloroethene

66.5

ug/L



FAG-47

10/13/2009

Tr

chloroethene

131

ug/L



FAG-47

4/27/2010

Tr

chloroethene

119

ug/L



FAG-47

10/20/2010

Tr

chloroethene

165

ug/L



FAG-47

4/27/2011

Tr

chloroethene

140

ug/L



FAG-47

10/27/2011

Tr

chloroethene

136

ug/L



FAG-47

5/3/2012

Tr

chloroethene

116

ug/L



FAG-47

10/9/2012

Tr

chloroethene

122

ug/L



FAG-47

5/14/2013

Tr

chloroethene

93.4

ug/L



FAG-47

10/21/2008

Vinyl chloride

1

ug/L

u

FAG-47

4/29/2009

Vinyl chloride

1

ug/L

u

FAG-47

10/13/2009

Vinyl chloride

1

ug/L

u

FAG-47

4/27/2010

Vinyl chloride

1

ug/L

u

FAG-47

10/20/2010

Vinyl chloride

1

ug/L

u

FAG-47

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-47

10/27/2011

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-47

5/3/2012

FAG-47

10/9/2012

FAG-47

5/14/2013

FAG-50

10/21/2008

FAG-50

5/20/2009

FAG-50

12/16/2009

FAG-50

4/28/2010

FAG-50

4/27/2011

FAG-50

10/25/2011

FAG-50

5/3/2012

FAG-50

10/10/2012

FAG-50

5/15/2013

FAG-50

10/21/2008

FAG-50

5/20/2009

FAG-50

12/16/2009

FAG-50

4/28/2010

FAG-50

4/27/2011

FAG-50

10/25/2011

FAG-50

5/3/2012

FAG-50

10/10/2012

FAG-50

5/15/2013

FAG-50

10/21/2008

FAG-50

5/20/2009

FAG-50

12/16/2009

FAG-50

4/28/2010

FAG-50

4/27/2011

FAG-50

10/25/2011

FAG-50

5/3/2012

FAG-50

10/10/2012

FAG-50

5/15/2013

FAG-56

10/20/2008

FAG-56

4/28/2009

FAG-56

10/13/2009

FAG-56

4/28/2010

FAG-56

10/20/2010

FAG-56

4/27/2011

FAG-56

10/25/2011

FAG-56

5/1/2012

FAG-56

10/9/2012

FAG-56

5/14/2013

FAG-56

10/20/2008

FAG-56

4/28/2009

FAG-56

10/13/2009

FAG-56

4/28/2010

FAG-56

10/20/2010

FAG-56

4/27/2011

FAG-56

10/25/2011

FAG-56

5/1/2012

FAG-56

10/9/2012

FAG-56

5/14/2013

FAG-56

10/20/2008

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

28.2

ug/L



54.8

ug/L



30.8

ug/L



32.8

ug/L



20

ug/L

u

20

ug/L

u

14.2

ug/L



20

ug/L

u

26.3

ug/L



4130

ug/L



7030

ug/L



3220

ug/L



3590

ug/L



1040

ug/L



1350

ug/L



957

ug/L



1290

ug/L



2160

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

20

ug/L

u

20

ug/L

u

1

ug/L

u

20

ug/L

u

20

ug/L

u

72.8

ug/L



68.5

ug/L



83.8

ug/L



84.1

ug/L



101

ug/L



98.5

ug/L



124

ug/L



117

ug/L



114

ug/L



122

ug/L



8.3

ug/L



8.2

ug/L



8.2

ug/L



12.4

ug/L



6.5

ug/L



8

ug/L



8.9

ug/L



9.4

ug/L



8.6

ug/L



9.6

ug/L



1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-56

4/28/2009

FAG-56

10/13/2009

FAG-56

4/28/2010

FAG-56

10/20/2010

FAG-56

4/27/2011

FAG-56

10/25/2011

FAG-56

5/1/2012

FAG-56

10/9/2012

FAG-56

5/14/2013

FAG-62

10/23/2008

FAG-62

4/29/2009

FAG-62

10/13/2009

FAG-62

4/29/2010

FAG-62

10/20/2010

FAG-62

4/27/2011

FAG-62

10/26/2011

FAG-62

5/1/2012

FAG-62

10/10/2012

FAG-62

5/15/2013

FAG-62

10/23/2008

FAG-62

4/29/2009

FAG-62

10/13/2009

FAG-62

4/29/2010

FAG-62

10/20/2010

FAG-62

4/27/2011

FAG-62

10/26/2011

FAG-62

5/1/2012

FAG-62

10/10/2012

FAG-62

5/15/2013

FAG-62

10/23/2008

FAG-62

4/29/2009

FAG-62

10/13/2009

FAG-62

4/29/2010

FAG-62

10/20/2010

FAG-62

4/27/2011

FAG-62

10/26/2011

FAG-62

5/1/2012

FAG-62

10/10/2012

FAG-62

5/15/2013

FAG-73

10/21/2008

FAG-73

5/21/2009

FAG-73

10/14/2009

FAG-73

4/28/2010

FAG-73

10/20/2010

FAG-73

4/28/2011

FAG-73

10/26/2011

FAG-73

5/1/2012

FAG-73

10/10/2012

FAG-73

5/16/2013

FAG-73

10/21/2008

FAG-73

5/21/2009

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

103

ug/L



26.9

ug/L



33.2

ug/L



129

ug/L



107

ug/L



15.3

ug/L



193

ug/L



61.6

ug/L



456

ug/L



277

ug/L

j

413

ug/L



121

ug/L



126

ug/L



462

ug/L



294

ug/L



51.7

ug/L



185

ug/L



64.9

ug/L



103

ug/L



167

ug/L



1

ug/L

u

2

ug/L

u

1

ug/L

u

1

ug/L

u

2

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

2

ug/L

u

5

ug/L

u

2780

ug/L



951

ug/L



1120

ug/L



1390

ug/L



1700

ug/L



143

ug/L



357

ug/L



396

ug/L



561

ug/L



425

ug/L



1130

ug/L



429

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-73

10/14/2009

FAG-73

4/28/2010

FAG-73

10/20/2010

FAG-73

4/28/2011

FAG-73

10/26/2011

FAG-73

5/1/2012

FAG-73

10/10/2012

FAG-73

5/16/2013

FAG-73

10/21/2008

FAG-73

5/21/2009

FAG-73

10/14/2009

FAG-73

4/28/2010

FAG-73

10/20/2010

FAG-73

4/28/2011

FAG-73

10/26/2011

FAG-73

5/1/2012

FAG-73

10/10/2012

FAG-73

5/16/2013

FAG-74

10/21/2008

FAG-74

5/21/2009

FAG-74

10/14/2009

FAG-74

4/28/2010

FAG-74

10/20/2010

FAG-74

4/28/2011

FAG-74

10/26/2011

FAG-74

5/1/2012

FAG-74

10/9/2012

FAG-74

5/16/2013

FAG-74

10/21/2008

FAG-74

5/21/2009

FAG-74

10/14/2009

FAG-74

4/28/2010

FAG-74

10/20/2010

FAG-74

4/28/2011

FAG-74

10/26/2011

FAG-74

5/1/2012

FAG-74

10/9/2012

FAG-74

5/16/2013

FAG-74

10/21/2008

FAG-74

5/21/2009

FAG-74

10/14/2009

FAG-74

4/28/2010

FAG-74

10/20/2010

FAG-74

4/28/2011

FAG-74

10/26/2011

FAG-74

5/1/2012

FAG-74

10/9/2012

FAG-74

5/16/2013

FAG-85

10/23/2008

FAG-85

5/20/2009

FAG-85

10/16/2009

Sample

Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene

Value

Units Qualifier

358

ug/L

387

ug/L

514

ug/L

73

ug/L

82.3

ug/L

103

ug/L

163

ug/L

215

ug/L

965

ug/L

778

ug/L

896

ug/L

1060

ug/L

488

ug/L

152

ug/L

616

ug/L

471

ug/L

415

ug/L

510

ug/L

2540

ug/L

2960

ug/L

2410

ug/L

1990

ug/L

1210

ug/L

1200

ug/L

1140

ug/L

908

ug/L

875

ug/L

1100

ug/L

2720

ug/L

3950

ug/L

2760

ug/L

2560

ug/L

1070

ug/L

1430

ug/L

893

ug/L

770

ug/L

575

ug/L

1120

ug/L

188

ug/L

213

ug/L

222

ug/L

181

ug/L

134

ug/L

161

ug/L

151

ug/L

146

ug/L

148

ug/L

149

ug/L

350

ug/L

71.1

ug/L J

172

ug/L


-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-85

4/30/2010

FAG-85

10/19/2010

FAG-85

4/27/2011

FAG-85

10/25/2011

FAG-85

5/2/2012

FAG-85

10/9/2012

FAG-85

5/15/2013

FAG-85

10/23/2008

FAG-85

5/20/2009

FAG-85

10/16/2009

FAG-85

4/30/2010

FAG-85

10/19/2010

FAG-85

4/27/2011

FAG-85

10/25/2011

FAG-85

5/2/2012

FAG-85

10/9/2012

FAG-85

5/15/2013

FAG-85

10/23/2008

FAG-85

5/20/2009

FAG-85

10/16/2009

FAG-85

4/30/2010

FAG-85

10/19/2010

FAG-85

4/27/2011

FAG-85

10/25/2011

FAG-85

5/2/2012

FAG-85

10/9/2012

FAG-85

5/15/2013

FAG-88

10/20/2008

FAG-88

4/28/2009

FAG-88

10/13/2009

FAG-88

4/27/2010

FAG-88

10/19/2010

FAG-88

5/5/2011

FAG-88

10/25/2011

FAG-88

5/2/2012

FAG-88

10/9/2012

FAG-88

5/14/2013

FAG-88

10/20/2008

FAG-88

4/28/2009

FAG-88

10/13/2009

FAG-88

4/27/2010

FAG-88

10/19/2010

FAG-88

5/5/2011

FAG-88

10/25/2011

FAG-88

5/2/2012

FAG-88

10/9/2012

FAG-88

5/14/2013

FAG-88

10/20/2008

FAG-88

4/28/2009

FAG-88

10/13/2009

FAG-88

4/27/2010

Sample

cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride

Value Units Qualifier

105

ug/L



1

ug/L

U

231

ug/L



189

ug/L

J

182

ug/L



216

ug/L



200

ug/L



244

ug/L



161

ug/L

J

580

ug/L



177

ug/L



6.4

ug/L



692

ug/L



650

ug/L

J

637

ug/L



671

ug/L



596

ug/L



5

ug/L

U

10

ug/L

u

5

ug/L

u

1

ug/L

u

1

ug/L

u

3.3

ug/L



20

ug/L

u

20

ug/L

u

5

ug/L

u

5

ug/L

u

4.1

ug/L



3.8

ug/L



4.1

ug/L



4.3

ug/L



4.1

ug/L



3.4

ug/L



3.2

ug/L



2.5

ug/L



2.4

ug/L



2.5

ug/L



11.3

ug/L



11.9

ug/L



11.7

ug/L



12.6

ug/L



13

ug/L



10.8

ug/L



9.3

ug/L



8.5

ug/L



7.3

ug/L



6.4

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-88

10/19/2010

FAG-88

5/5/2011

FAG-88

10/25/2011

FAG-88

5/2/2012

FAG-88

10/9/2012

FAG-88

5/14/2013

FAG-89

10/21/2008

FAG-89

4/28/2009

FAG-89

10/14/2009

FAG-89

4/27/2010

FAG-89

10/19/2010

FAG-89

5/5/2011

FAG-89

10/26/2011

FAG-89

5/2/2012

FAG-89

10/10/2012

FAG-89

5/15/2013

FAG-89

10/21/2008

FAG-89

4/28/2009

FAG-89

10/14/2009

FAG-89

4/27/2010

FAG-89

10/19/2010

FAG-89

5/5/2011

FAG-89

10/26/2011

FAG-89

5/2/2012

FAG-89

10/10/2012

FAG-89

5/15/2013

FAG-89

10/21/2008

FAG-89

4/28/2009

FAG-89

10/14/2009

FAG-89

4/27/2010

FAG-89

10/19/2010

FAG-89

5/5/2011

FAG-89

10/26/2011

FAG-89

5/2/2012

FAG-89

10/10/2012

FAG-89

5/15/2013

FAG-AW4

10/23/2008

FAG-AW4

4/29/2009

FAG-AW4

10/15/2009

FAG-AW4

4/29/2010

FAG-AW4

10/21/2010

FAG-AW4

4/28/2011

FAG-AW4

10/27/2011

FAG-AW4

5/3/2012

FAG-AW4

10/11/2012

FAG-AW4

5/16/2013

FAG-AW4

10/23/2008

FAG-AW4

4/29/2009

FAG-AW4

10/15/2009

FAG-AW4

4/29/2010

FAG-AW4

10/21/2010

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1.9

ug/L



1.3

ug/L



1.5

ug/L



1.3

ug/L



1.4

ug/L



1.7

ug/L



2.4

ug/L



1.5

ug/L



3.1

ug/L



3.4

ug/L



17.7

ug/L



12.2

ug/L



12

ug/L



7.9

ug/L



11.4

ug/L



11.8

ug/L



16.6

ug/L



13.2

ug/L



33.4

ug/L



37.7

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

188

ug/L



186

ug/L



177

ug/L



191

ug/L



213

ug/L



200

ug/L



200

ug/L



194

ug/L



218

ug/L



225

ug/L



983

ug/L



1050

ug/L



1300

ug/L

J

898

ug/L



946

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

FAG-AW4

4/28/2011

FAG-AW4

10/27/2011

FAG-AW4

5/3/2012

FAG-AW4

10/11/2012

FAG-AW4

5/16/2013

FAG-AW4

10/23/2008

FAG-AW4

4/29/2009

FAG-AW4

10/15/2009

FAG-AW4

4/29/2010

FAG-AW4

10/21/2010

FAG-AW4

4/28/2011

FAG-AW4

10/27/2011

FAG-AW4

5/3/2012

FAG-AW4

10/11/2012

FAG-AW4

5/16/2013

RI-MW1

10/22/2008

RI-MW1

4/28/2009

RI-MW1

10/15/2009

RI-MW1

4/30/2010

RI-MW1

10/19/2010

RI-MW1

4/26/2011

RI-MW1

10/28/2011

RI-MW1

5/3/2012

RI-MW1

10/10/2012

RI-MW1

5/14/2013

RI-MW1

10/22/2008

RI-MW1

4/28/2009

RI-MW1

10/15/2009

RI-MW1

4/30/2010

RI-MW1

10/19/2010

RI-MW1

4/26/2011

RI-MW1

10/28/2011

RI-MW1

5/3/2012

RI-MW1

10/10/2012

RI-MW1

5/14/2013

RI-MW1

10/22/2008

RI-MW1

4/28/2009

RI-MW1

10/15/2009

RI-MW1

4/30/2010

RI-MW1

10/19/2010

RI-MW1

4/26/2011

RI-MW1

10/28/2011

RI-MW1

5/3/2012

RI-MW1

10/10/2012

RI-MW1

5/14/2013

RI-MW2

10/22/2008

RI-MW2

4/27/2009

RI-MW2

10/15/2009

RI-MW2

4/29/2010

RI-MW2

10/19/2010

RI-MW2

4/26/2011

Sample	Value

Trichloroethene	940

Trichloroethene	957

Trichloroethene	874

Trichloroethene	873

Trichloroethene	912

Vinyl chloride	10

Vinyl chloride	1

Vinyl chloride	1

Vinyl chloride	10

Vinyl chloride	10

Vinyl chloride	10

Vinyl chloride	11.5

Vinyl chloride	10

Vinyl chloride	10

Vinyl chloride	10.9

cis-1,2-Dichloroethene	5

cis-1,2-Dichloroethene	2.9

cis-1,2-Dichloroethene	2.6

cis-1,2-Dichloroethene	2.4

cis-1,2-Dichloroethene	2.8

cis-1,2-Dichloroethene	2.6

cis-1,2-Dichloroethene	2.5

cis-1,2-Dichloroethene	1.6

cis-1,2-Dichloroethene	2.6

cis-1,2-Dichloroethene	3.6

Trichloroethene	54.5

Trichloroethene	51.4

Trichloroethene	36

Trichloroethene	53.2

Trichloroethene	78.5

Trichloroethene	80.7

Trichloroethene	55.1

Trichloroethene	41.2

Trichloroethene	55

Trichloroethene	85.1

Vinyl chloride	5

Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene

Units

Q

ug/L



ug/L



ug/L



ug/L



ug/L



ug/L

U

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L



ug/L

u

ug/L

u

ug/L



ug/L

u

ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L

J

ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L



ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

RI-MW2

10/26/2011

RI-MW2

5/3/2012

RI-MW2

10/10/2012

RI-MW2

5/14/2013

RI-MW2

10/22/2008

RI-MW2

4/27/2009

RI-MW2

10/15/2009

RI-MW2

4/29/2010

RI-MW2

10/19/2010

RI-MW2

4/26/2011

RI-MW2

10/26/2011

RI-MW2

5/3/2012

RI-MW2

10/10/2012

RI-MW2

5/14/2013

RI-MW2

10/22/2008

RI-MW2

4/27/2009

RI-MW2

10/15/2009

RI-MW2

4/29/2010

RI-MW2

10/19/2010

RI-MW2

4/26/2011

RI-MW2

10/26/2011

RI-MW2

5/3/2012

RI-MW2

10/10/2012

RI-MW2

5/14/2013

RI-MW5

10/21/2008

RI-MW5

4/28/2009

RI-MW5

10/13/2009

RI-MW5

4/27/2010

RI-MW5

10/20/2010

RI-MW5

4/26/2011

RI-MW5

10/25/2011

RI-MW5

5/1/2012

RI-MW5

10/9/2012

RI-MW5

5/14/2013

RI-MW5

10/21/2008

RI-MW5

4/28/2009

RI-MW5

10/13/2009

RI-MW5

4/27/2010

RI-MW5

10/20/2010

RI-MW5

4/26/2011

RI-MW5

10/25/2011

RI-MW5

5/1/2012

RI-MW5

10/9/2012

RI-MW5

5/14/2013

RI-MW5

10/21/2008

RI-MW5

4/28/2009

RI-MW5

10/13/2009

RI-MW5

4/27/2010

RI-MW5

10/20/2010

RI-MW5

4/26/2011

RI-MW5

10/25/2011

Sample

cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1.4

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

12.7

ug/L



19.4

ug/L

J

12.7

ug/L



25.8

ug/L



13.6

ug/L



4.3

ug/L



8.5

ug/L



7.4

ug/L



5.9

ug/L



4.8

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

RI-MW5

5/1/2012

RI-MW5

10/9/2012

RI-MW5

5/14/2013

RI-MW6

10/21/2008

RI-MW6

4/29/2009

RI-MW6

10/14/2009

RI-MW6

4/28/2010

RI-MW6

10/20/2010

RI-MW6

4/27/2011

RI-MW6

10/26/2011

RI-MW6

5/2/2012

RI-MW6

10/10/2012

RI-MW6

5/15/2013

RI-MW6

10/21/2008

RI-MW6

4/29/2009

RI-MW6

10/14/2009

RI-MW6

4/28/2010

RI-MW6

10/20/2010

RI-MW6

4/27/2011

RI-MW6

10/26/2011

RI-MW6

5/2/2012

RI-MW6

10/10/2012

RI-MW6

5/15/2013

RI-MW6

10/21/2008

RI-MW6

4/29/2009

RI-MW6

10/14/2009

RI-MW6

4/28/2010

RI-MW6

10/20/2010

RI-MW6

4/27/2011

RI-MW6

10/26/2011

RI-MW6

5/2/2012

RI-MW6

10/10/2012

RI-MW6

5/15/2013

RI-MW7

10/21/2008

RI-MW7

4/28/2009

RI-MW7

10/13/2009

RI-MW7

4/27/2010

RI-MW7

10/20/2010

RI-MW7

4/26/2011

RI-MW7

10/25/2011

RI-MW7

5/1/2012

RI-MW7

10/9/2012

RI-MW7

5/15/2013

RI-MW7

10/21/2008

RI-MW7

4/28/2009

RI-MW7

10/13/2009

RI-MW7

4/27/2010

RI-MW7

10/20/2010

RI-MW7

4/26/2011

RI-MW7

10/25/2011

RI-MW7

5/1/2012

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

5.6

ug/L



6.4

ug/L



6.1

ug/L



9.2

ug/L



7.1

ug/L



7.6

ug/L



6.3

ug/L



5.4

ug/L



5.2

ug/L



3.6

ug/L



39.8

ug/L



47.2

ug/L



40

ug/L



72.2

ug/L



48.8

ug/L



48.6

ug/L



38.4

ug/L



33.6

ug/L



29.5

ug/L



17.9

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L



1.2

ug/L



1.8

ug/L



2

ug/L



2.2

ug/L



2.8

ug/L



2.8

ug/L



2.7

ug/L



4

ug/L



3.5

ug/L



11.4

ug/L



14.3

ug/L



18.9

ug/L



20

ug/L



20.3

ug/L



26.7

ug/L



23.7

ug/L



28.4

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

RI-MW7

10/9/2012

RI-MW7

5/15/2013

RI-MW7

10/21/2008

RI-MW7

4/28/2009

RI-MW7

10/13/2009

RI-MW7

4/27/2010

RI-MW7

10/20/2010

RI-MW7

4/26/2011

RI-MW7

10/25/2011

RI-MW7

5/1/2012

RI-MW7

10/9/2012

RI-MW7

5/15/2013

RI-MW8

10/20/2008

RI-MW8

4/27/2009

RI-MW8

10/13/2009

RI-MW8

4/26/2010

RI-MW8

10/19/2010

RI-MW8

4/26/2011

RI-MW8

10/25/2011

RI-MW8

5/1/2012

RI-MW8

10/9/2012

RI-MW8

5/14/2013

RI-MW8

10/20/2008

RI-MW8

4/27/2009

RI-MW8

10/13/2009

RI-MW8

4/26/2010

RI-MW8

10/19/2010

RI-MW8

4/26/2011

RI-MW8

10/25/2011

RI-MW8

5/1/2012

RI-MW8

10/9/2012

RI-MW8

5/14/2013

RI-MW8

10/20/2008

RI-MW8

4/27/2009

RI-MW8

10/13/2009

RI-MW8

4/26/2010

RI-MW8

10/19/2010

RI-MW8

4/26/2011

RI-MW8

10/25/2011

RI-MW8

5/1/2012

RI-MW8

10/9/2012

RI-MW8

5/14/2013

RI-MW9

10/22/2008

RI-MW9

4/29/2009

RI-MW9

10/14/2009

RI-MW9

4/28/2010

RI-MW9

10/20/2010

RI-MW9

4/26/2011

RI-MW9

10/26/2011

RI-MW9

5/2/2012

RI-MW9

10/10/2012

Sample

Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene

Value Units Qualifier

31.9

ug/L



33.4

ug/L



1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

4.1

ug/L



4.5

ug/L

J

4.8

ug/L



5.9

ug/L



4.4

ug/L



4.3

ug/L



3.1

ug/L



3.7

ug/L



3.9

ug/L



3.7

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

2.4

ug/L



2.7

ug/L



2.5

ug/L



3

ug/L



2

ug/L



1.6

ug/L



1.4

ug/L



1

ug/L

u

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

RI-MW9

5/14/2013

RI-MW9

10/22/2008

RI-MW9

4/29/2009

RI-MW9

10/14/2009

RI-MW9

4/28/2010

RI-MW9

10/20/2010

RI-MW9

4/26/2011

RI-MW9

10/26/2011

RI-MW9

5/2/2012

RI-MW9

10/10/2012

RI-MW9

5/14/2013

RI-MW9

10/22/2008

RI-MW9

4/29/2009

RI-MW9

10/14/2009

RI-MW9

4/28/2010

RI-MW9

10/20/2010

RI-MW9

4/26/2011

RI-MW9

10/26/2011

RI-MW9

5/2/2012

RI-MW9

10/10/2012

RI-MW9

5/14/2013

RW-341A

10/23/2008

RW-341A

4/30/2009

RW-341 A

10/16/2009

RW-341 A

4/29/2010

RW-341 A

10/20/2010

RW-341 A

4/28/2011

RW-341 A

10/25/2011

RW-341 A

5/4/2012

RW-341 A

10/10/2012

RW-341 A

5/15/2013

RW-341 A

10/23/2008

RW-341 A

4/30/2009

RW-341 A

10/16/2009

RW-341 A

4/29/2010

RW-341 A

10/20/2010

RW-341 A

4/28/2011

RW-341 A

10/25/2011

RW-341 A

5/4/2012

RW-341 A

10/10/2012

RW-341 A

5/15/2013

RW-341 A

10/23/2008

RW-341 A

4/30/2009

RW-341 A

10/16/2009

RW-341 A

4/29/2010

RW-341 A

10/20/2010

RW-341 A

4/28/2011

RW-341 A

10/25/2011

RW-341 A

5/4/2012

RW-341 A

10/10/2012

RW-341 A

5/15/2013

Sample

cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride

Value Units Qualifier

1

ug/L

U

46.4

ug/L



54.2

ug/L



44.9

ug/L



53

ug/L



34.4

ug/L



27.7

ug/L



22.1

ug/L



14.2

ug/L



10.3

ug/L



9.6

ug/L



1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1.9

ug/L



1

ug/L

u

1

ug/L

u

2.1

ug/L



1.1

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L



1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

SW-01

FAG-05

FAG-11

FAG-22

FAG-31

FAG-32

FAG-33

FAG-34

FAG-35

FAG-36

FAG-43

FAG-46

FAG-47

FAG-50

FAG-56

FAG-62

FAG-73

FAG-74

FAG-85

FAG-88

FAG-89

FAG-AW4

Sample Date

10/23/2008
4/30/2009
10/16/2009
4/29/2010
10/20/2010
4/28/2011
10/25/2011
5/4/2012
10/10/2012
5/15/2013
10/23/2008
4/30/2009
10/16/2009
4/29/2010
10/20/2010
4/28/2011
10/25/2011
5/4/2012
10/10/2012
5/15/2013
10/23/2008
4/30/2009
10/16/2009
4/29/2010
10/20/2010
4/28/2011
10/25/2011
5/4/2012
10/10/2012
5/15/2013
10/19/2016
10/19/2016
10/20/2016
10/20/2016
10/20/2016
10/18/2016
10/19/2016
10/19/2016
10/20/2016
10/19/2016
10/18/2016
10/18/2016
10/20/2016
10/18/2016
10/19/2016
10/19/2016
10/20/2016
10/19/2016
10/18/2016
10/19/2016
10/20/2016

Sample

cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene

Value Units Qualifier

ug/l
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/

.6 ug/

.1 ug/

.1 ug/
ug/
ug/

.6 ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/

7.2 ug/

¦9 ug/

707 ug/

305 ug/

481 ug/

3.5 ug/

326 ug/

126 ug/

235 ug/

9.9 ug/

2.8 ug/

10.6 ug/

91.5 ug/

105 ug/

13.1 ug/

282 ug/

321 ug/

48.9 ug/

2.2	ug/

2.3	ug/

270 ug/


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

RI-MW1

10/18/2016

cis-1,2-Dichloroethene

2.2

ug/L



RI-MW2

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

10/19/2016

cis-1,2-Dichloroethene

6.4

ug/L



RI-MW7

10/19/2016

cis-1,2-Dichloroethene

3.3

ug/L



RI-MW8

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RW-341A

10/20/2016

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/20/2016

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

10/19/2016

Tr

chloroethene

75.6

ug/L



FAG-11

10/19/2016

Tr

chloroethene

9.6

ug/L



FAG-22

10/20/2016

Tr

chloroethene

1340

ug/L



FAG-31

10/20/2016

Tr

chloroethene

765

ug/L



FAG-32

10/20/2016

Tr

chloroethene

1570

ug/L



FAG-33

10/18/2016

Tr

chloroethene

28.1

ug/L



FAG-34

10/19/2016

Tr

chloroethene

574

ug/L



FAG-35

10/19/2016

Tr

chloroethene

516

ug/L



FAG-36

10/20/2016

Tr

chloroethene

566

ug/L



FAG-43

10/19/2016

Tr

chloroethene

50.6

ug/L



FAG-46

10/18/2016

Tr

chloroethene

50.6

ug/L



FAG-47

10/18/2016

Tr

chloroethene

76.9

ug/L



FAG-50

10/20/2016

Tr

chloroethene

2610

ug/L



FAG-56

10/18/2016

Tr

chloroethene

15.1

ug/L

J

FAG-62

10/19/2016

Tr

chloroethene

33.6

ug/L



FAG-73

10/19/2016

Tr

chloroethene

249

ug/L



FAG-74

10/20/2016

Tr

chloroethene

200

ug/L



FAG-85

10/19/2016

Tr

chloroethene

146

ug/L



FAG-88

10/18/2016

Tr

chloroethene

7.1

ug/L



FAG-89

10/19/2016

Tr

chloroethene

20.8

ug/L



FAG-AW4

10/20/2016

Tr

chloroethene

1150

ug/L

J

RI-MW1

10/18/2016

Tr

chloroethene

52.8

ug/L



RI-MW2

10/18/2016

Tr

chloroethene

1

ug/L

u

RI-MW5

10/18/2016

Tr

chloroethene

18.3

ug/L



RI-MW6

10/19/2016

Tr

chloroethene

38.1

ug/L



RI-MW7

10/19/2016

Tr

chloroethene

25.5

ug/L



RI-MW8

10/18/2016

Tr

chloroethene

3.1

ug/L



RI-MW9

10/18/2016

Tr

chloroethene

9.5

ug/L



RW-341 A

10/20/2016

Tr

chloroethene

1

ug/L

u

SW-01

10/20/2016

Tr

chloroethene

1

ug/L

u

FAG-05

10/19/2016

Vinyl chloride

1

ug/L

u

FAG-11

10/19/2016

Vinyl chloride

1

ug/L

u

FAG-22

10/20/2016

Vinyl chloride

93.1

ug/L



FAG-31

10/20/2016

Vinyl chloride

10

ug/L

u

FAG-32

10/20/2016

Vinyl chloride

20

ug/L

u

FAG-33

10/18/2016

Vinyl chloride

1

ug/L

u

FAG-34

10/19/2016

Vinyl chloride

10.6

ug/L



FAG-35

10/19/2016

Vinyl chloride

5

ug/L

u

FAG-36

10/20/2016

Vinyl chloride

20

ug/L

u

FAG-43

10/19/2016

Vinyl chloride

1

ug/L

u

FAG-46

10/18/2016

Vinyl chloride

1

ug/L

u

FAG-47

10/18/2016

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-50

10/20/2016

Viny

chloride

20

ug/L

U

FAG-56

10/18/2016

Viny

chloride

1

ug/L

U

FAG-62

10/19/2016

Viny

chloride

1

ug/L

u

FAG-73

10/19/2016

Viny

chloride

212

ug/L



FAG-74

10/20/2016

Viny

chloride

75

ug/L



FAG-85

10/19/2016

Viny

chloride

5

ug/L

u

FAG-88

10/18/2016

Viny

chloride

1

ug/L

u

FAG-89

10/19/2016

Viny

chloride

1

ug/L

u

FAG-AW4

10/20/2016

Viny

chloride

16.2

ug/L



RI-MW1

10/18/2016

Viny

chloride

1

ug/L

u

RI-MW2

10/18/2016

Viny

chloride

1

ug/L

u

RI-MW5

10/18/2016

Viny

chloride

1

ug/L

u

RI-MW6

10/19/2016

Viny

chloride

1

ug/L

u

RI-MW7

10/19/2016

Viny

chloride

1

ug/L

u

RI-MW8

10/18/2016

Viny

chloride

1

ug/L

u

RI-MW9

10/18/2016

Viny

chloride

1

ug/L

u

RW-341A

10/20/2016

Viny

chloride

1

ug/L

u

SW-01

10/20/2016

Viny

chloride

1

ug/L

u

FAG-05

5/31/2017

cis-1

,2-Dichloroethene

6.2

ug/L



FAG-11

5/30/2017

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-22

5/31/2017

cis-1

,2-Dichloroethene

523

ug/L



FAG-31

5/31/2017

cis-1

,2-Dichloroethene

276

ug/L



FAG-32

5/31/2017

cis-1

,2-Dichloroethene

448

ug/L



FAG-33

5/27/2017

cis-1

,2-Dichloroethene

3.6

ug/L



FAG-34

5/26/2017

cis-1

,2-Dichloroethene

330

ug/L



FAG-35

5/31/2017

cis-1

,2-Dichloroethene

107

ug/L



FAG-36

5/31/2017

cis-1

,2-Dichloroethene

280

ug/L



FAG-43

5/31/2017

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-46

5/27/2017

cis-1

,2-Dichloroethene

2.2

ug/L



FAG-47

5/27/2017

cis-1

,2-Dichloroethene

7.7

ug/L



FAG-50

5/31/2017

cis-1

,2-Dichloroethene

49.4

ug/L



FAG-56

5/27/2017

cis-1

,2-Dichloroethene

115

ug/L



FAG-62

5/27/2017

cis-1

,2-Dichloroethene

3.6

ug/L



FAG-73

5/31/2017

cis-1

,2-Dichloroethene

96.6

ug/L



FAG-74

5/26/2017

cis-1

,2-Dichloroethene

549

ug/L



FAG-85

5/31/2017

cis-1

,2-Dichloroethene

170

ug/L



FAG-88

5/24/2017

cis-1

,2-Dichloroethene

2

ug/L



FAG-89

5/30/2017

cis-1

,2-Dichloroethene

2

ug/L



FAG-AW4

5/31/2017

cis-1

,2-Dichloroethene

302

ug/L



RI-MW1

5/25/2017

cis-1

,2-Dichloroethene

3

ug/L



RI-MW2

5/25/2017

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW5

5/25/2017

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW6

5/30/2017

cis-1

,2-Dichloroethene

4.2

ug/L



RI-MW7

5/30/2017

cis-1

,2-Dichloroethene

3.3

ug/L



RI-MW8

5/25/2017

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW9

5/25/2017

cis-1

,2-Dichloroethene

1

ug/L

u

RW-341 A

5/31/2017

cis-1

,2-Dichloroethene

1

ug/L

u

SW-01

5/31/2017

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-05

5/31/2017

Trichloroethene

32.8

ug/L



FAG-11

5/30/2017

Trichloroethene

1.9

ug/L



FAG-22

5/31/2017

Trichloroethene

1860

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-31

5/31/2017

Tr

chloroethene

719

ug/L



FAG-32

5/31/2017

Tr

chloroethene

1520

ug/L



FAG-33

5/27/2017

Tr

chloroethene

31.7

ug/L



FAG-34

5/26/2017

Tr

chloroethene

809

ug/L



FAG-35

5/31/2017

Tr

chloroethene

432

ug/L



FAG-36

5/31/2017

Tr

chloroethene

585

ug/L



FAG-43

5/31/2017

Tr

chloroethene

1

ug/L

U

FAG-46

5/27/2017

Tr

chloroethene

47.9

ug/L



FAG-47

5/27/2017

Tr

chloroethene

69.2

ug/L



FAG-50

5/31/2017

Tr

chloroethene

2610

ug/L



FAG-56

5/27/2017

Tr

chloroethene

9.3

ug/L



FAG-62

5/27/2017

Tr

chloroethene

33.6

ug/L



FAG-73

5/31/2017

Tr

chloroethene

58.3

ug/L



FAG-74

5/26/2017

Tr

chloroethene

789

ug/L



FAG-85

5/31/2017

Tr

chloroethene

527

ug/L



FAG-88

5/24/2017

Tr

chloroethene

6.8

ug/L



FAG-89

5/30/2017

Tr

chloroethene

18.8

ug/L



FAG-AW4

5/31/2017

Tr

chloroethene

1070

ug/L



RI-MW1

5/25/2017

Tr

chloroethene

96.4

ug/L



RI-MW2

5/25/2017

Tr

chloroethene

1

ug/L

U

RI-MW5

5/25/2017

Tr

chloroethene

12.7

ug/L



RI-MW6

5/30/2017

Tr

chloroethene

22.2

ug/L



RI-MW7

5/30/2017

Tr

chloroethene

25.8

ug/L



RI-MW8

5/25/2017

Tr

chloroethene

3.4

ug/L



RI-MW9

5/25/2017

Tr

chloroethene

6.4

ug/L



RW-341A

5/31/2017

Tr

chloroethene

1

ug/L

u

SW-01

5/31/2017

Tr

chloroethene

1

ug/L

u

FAG-05

5/31/2017

Vinyl

chlor

de

1

ug/L

u

FAG-11

5/30/2017

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/31/2017

Vinyl

chlor

de

63.1

ug/L



FAG-31

5/31/2017

Vinyl

chlor

de

10

ug/L

u

FAG-32

5/31/2017

Vinyl

chlor

de

20

ug/L

u

FAG-33

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-34

5/26/2017

Vinyl

chlor

de

5.9

ug/L



FAG-35

5/31/2017

Vinyl

chlor

de

5

ug/L

u

FAG-36

5/31/2017

Vinyl

chlor

de

10

ug/L

u

FAG-43

5/31/2017

Vinyl

chlor

de

1

ug/L

u

FAG-46

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/31/2017

Vinyl

chlor

de

20

ug/L

u

FAG-56

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-62

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/31/2017

Vinyl

chlor

de

177

ug/L



FAG-74

5/26/2017

Vinyl

chlor

de

75.2

ug/L



FAG-85

5/31/2017

Vinyl

chlor

de

2

ug/L

u

FAG-88

5/24/2017

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/30/2017

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

5/31/2017

Vinyl

chlor

de

18.7

ug/L



RI-MW1

5/25/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/25/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/25/2017

Vinyl

chlor

de

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

RI-MW6

5/30/2017

RI-MW7

5/30/2017

RI-MW8

5/25/2017

RI-MW9

5/25/2017

RW-341A

5/31/2017

SW-01

5/31/2017

FAG-05

10/12/2017

FAG-11

10/11/2017

FAG-22

10/12/2017

FAG-31

10/12/2017

FAG-32

10/12/2017

FAG-33

10/8/2017

FAG-34

10/11/2017

FAG-35

10/11/2017

FAG-36

10/11/2017

FAG-43

10/11/2017

FAG-46

10/11/2017

FAG-47

10/8/2017

FAG-56

10/10/2017

FAG-73

10/11/2017

FAG-74

10/12/2017

FAG-85

10/11/2017

FAG-88

10/11/2017

FAG-89

10/12/2017

FAG-AW4

10/12/2017

RI-MW1

10/8/2017

RI-MW2

10/8/2017

RI-MW5

10/8/2017

RI-MW6

10/11/2017

RI-MW7

10/11/2017

RI-MW8

10/8/2017

RI-MW9

10/8/2017

RW-341 A

10/11/2017

SW-01

10/11/2017

FAG-05

10/12/2017

FAG-11

10/11/2017

FAG-22

10/12/2017

FAG-31

10/12/2017

FAG-32

10/12/2017

FAG-33

10/8/2017

FAG-34

10/11/2017

FAG-35

10/11/2017

FAG-36

10/11/2017

FAG-43

10/11/2017

FAG-46

10/11/2017

FAG-47

10/8/2017

FAG-56

10/10/2017

FAG-73

10/11/2017

FAG-74

10/12/2017

FAG-85

10/11/2017

FAG-88

10/11/2017

Sample

Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
Vinyl chloride
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene
Trichloroethene

Value Units Qualifier

1

ug/L

U

1

ug/L

U

1

ug/L

u

1

ug/L

u

1

ug/L

u

1

ug/L

u

14.5

ug/L



1

ug/L

u

464

ug/L



247

ug/L



448

ug/L



3.3

ug/L



324

ug/L



123

ug/L



197

ug/L



11.7

ug/L



4.7

ug/L



11.3

ug/L



120

ug/L



260

ug/L



254

ug/L



135

ug/L



1.8

ug/L



2.4

ug/L



299

ug/L



2.6

ug/L



1

ug/L

u

1

ug/L

u

5.6

ug/L



4.4

ug/L



1

ug/L

u

1.4

ug/L



1

ug/L

u

1

ug/L

u

69.6

ug/L



1

ug/L

u

1280

ug/L



735

ug/L



1780

ug/L



31

ug/L



644

ug/L



543

ug/L



676

ug/L



34.9

ug/L



53.5

ug/L



103

ug/L



9.5

ug/L



171

ug/L



101

ug/L



442

ug/L



5.9

ug/L




-------
MANN KENDALL INPUT

Well ID

FAG-89

FAG-AW4

RI-MW1

RI-MW2

RI-MW5

RI-MW6

RI-MW7

RI-MW8

RI-MW9

RW-341A

SW-01

FAG-05

FAG-11

FAG-22

FAG-31

FAG-32

FAG-33

FAG-34

FAG-35

FAG-36

FAG-43

FAG-46

FAG-47

FAG-56

FAG-73

FAG-74

FAG-85

FAG-88

FAG-89

FAG-AW4

RI-MW1

RI-MW2

RI-MW5

RI-MW6

RI-MW7

RI-MW8

RI-MW9

RW-341 A

SW-01

FAG-05

FAG-11

FAG-22

FAG-31

FAG-32

FAG-33

FAG-34

FAG-35

FAG-36

FAG-43

FAG-46

FAG-47

Sample Date

10/12/2017

10/12/2017

10/8/2017

10/8/2017

10/8/2017

10/11/2017

10/11/2017

10/8/2017

10/8/2017

10/11/2017

10/11/2017

10/12/2017

10/11/2017

10/12/2017

10/12/2017

10/12/2017

10/8/2017

10/11/2017

10/11/2017

10/11/2017

10/11/2017

10/11/2017

10/8/2017

10/10/2017

10/11/2017

10/12/2017

10/11/2017

10/11/2017

10/12/2017

10/12/2017

10/8/2017

10/8/2017

10/8/2017

10/11/2017

10/11/2017

10/8/2017

10/8/2017

10/11/2017

10/11/2017

10/11/2018

10/10/2018

10/11/2018

10/11/2018

10/10/2018

10/9/2018

10/10/2018

10/10/2018

10/10/2018

10/10/2018

10/9/2018

10/9/2018

Sample

chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene
chloroethene

Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny
Viny

chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor
chlor

de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de
de

Value

20.9
1120

47.4
1

17.5
30.9
32
3.1
4.5

.3

73.6
0
20

cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene
cis-1,2-Dichloroethene

.8
0

40
44
0

9.9

2.8

514
274
476
3.7
320
131
257
1

3.6
8.6

Units Qualifier

ug/L
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/
ug/


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

FAG-56

10/9/2018

cis-1,2-Dichloroethene

113

ug/L



FAG-73

10/10/2018

cis-1,2-Dichloroethene

305

ug/L



FAG-74

10/10/2018

cis-1,2-Dichloroethene

223

ug/L



FAG-85

10/11/2018

cis-1,2-Dichloroethene

221

ug/L



FAG-88

10/11/2018

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

10/10/2018

cis-1,2-Dichloroethene

5.7

ug/L



FAG-AW4

10/11/2018

cis-1,2-Dichloroethene

311

ug/L



RI-MW1

10/10/2018

cis-1,2-Dichloroethene

2.8

ug/L



RI-MW2

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

10/9/2018

cis-1,2-Dichloroethene

4

ug/L



RI-MW7

10/9/2018

cis-1,2-Dichloroethene

4.1

ug/L



RI-MW8

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/10/2018

cis-1,2-Dichloroethene

1

ug/L



RW-341A

10/11/2018

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/11/2018

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

10/11/2018

Tr

chloroethene

67.9

ug/L



FAG-11

10/10/2018

Tr

chloroethene

1

ug/L

u

FAG-22

10/11/2018

Tr

chloroethene

1680

ug/L



FAG-31

10/11/2018

Tr

chloroethene

934

ug/L



FAG-32

10/10/2018

Tr

chloroethene

1920

ug/L



FAG-33

10/9/2018

Tr

chloroethene

29.6

ug/L



FAG-34

10/10/2018

Tr

chloroethene

762

ug/L



FAG-35

10/10/2018

Tr

chloroethene

597

ug/L



FAG-36

10/10/2018

Tr

chloroethene

672

ug/L



FAG-43

10/10/2018

Tr

chloroethene

1

ug/L

u

FAG-46

10/9/2018

Tr

chloroethene

56.9

ug/L



FAG-47

10/9/2018

Tr

chloroethene

63.3

ug/L



FAG-56

10/9/2018

Tr

chloroethene

9.6

ug/L



FAG-73

10/10/2018

Tr

chloroethene

242

ug/L



FAG-74

10/10/2018

Tr

chloroethene

123

ug/L



FAG-85

10/11/2018

Tr

chloroethene

794

ug/L



FAG-88

10/11/2018

Tr

chloroethene

5.7

ug/L



FAG-89

10/10/2018

Tr

chloroethene

63.6

ug/L



FAG-AW4

10/11/2018

Tr

chloroethene

1250

ug/L



RI-MW1

10/10/2018

Tr

chloroethene

99.7

ug/L



RI-MW2

10/9/2018

Tr

chloroethene

1

ug/L

u

RI-MW5

10/9/2018

Tr

chloroethene

13.5

ug/L



RI-MW6

10/9/2018

Tr

chloroethene

21.7

ug/L



RI-MW7

10/9/2018

Tr

chloroethene

33.1

ug/L



RI-MW8

10/9/2018

Tr

chloroethene

3.1

ug/L



RI-MW9

10/10/2018

Tr

chloroethene

4.5

ug/L



RW-341 A

10/11/2018

Tr

chloroethene

1

ug/L

u

SW-01

10/11/2018

Tr

chloroethene

1.5

ug/L



FAG-05

10/11/2018

Vinyl chloride

1

ug/L

u

FAG-11

10/10/2018

Vinyl chloride

1

ug/L

u

FAG-22

10/11/2018

Vinyl chloride

110

ug/L



FAG-31

10/11/2018

Vinyl chloride

10

ug/L

u

FAG-32

10/10/2018

Vinyl chloride

20

ug/L

u

FAG-33

10/9/2018

Vinyl chloride

1

ug/L

u

FAG-34

10/10/2018

Vinyl chloride

6.5

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-35

10/10/2018

Viny

chlor

de

5

ug/L

U

FAG-36

10/10/2018

Viny

chlor

de

10

ug/L

U

FAG-43

10/10/2018

Viny

chlor

de

1

ug/L

u

FAG-46

10/9/2018

Viny

chlor

de

1

ug/L

u

FAG-47

10/9/2018

Viny

chlor

de

1

ug/L

u

FAG-56

10/9/2018

Viny

chlor

de

1

ug/L

u

FAG-73

10/10/2018

Viny

chlor

de

212

ug/L



FAG-74

10/10/2018

Viny

chlor

de

31.1

ug/L



FAG-85

10/11/2018

Viny

chlor

de

2.5

ug/L



FAG-88

10/11/2018

Viny

chlor

de

1

ug/L

u

FAG-89

10/10/2018

Viny

chlor

de

1

ug/L

u

FAG-AW4

10/11/2018

Viny

chlor

de

35.2

ug/L



RI-MW1

10/10/2018

Viny

chlor

de

1

ug/L

u

RI-MW2

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW5

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW6

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW7

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW8

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW9

10/10/2018

Viny

chlor

de

1

ug/L

u

RW-341A

10/11/2018

Viny

chlor

de

1

ug/L

u

SW-01

10/11/2018

Viny

chlor

de

1

ug/L

u

FAG-05

9/16/2020

cis-1

,2-Dichloroethene

5.5

ug/L



FAG-11

9/16/2020

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-22

9/17/2020

cis-1

,2-Dichloroethene

189

ug/L



FAG-31

9/17/2020

cis-1

,2-Dichloroethene

244

ug/L



FAG-32

9/16/2020

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-33

9/15/2020

cis-1

,2-Dichloroethene

3.8

ug/L



FAG-34

9/16/2020

cis-1

,2-Dichloroethene

249

ug/L



FAG-35

9/16/2020

cis-1

,2-Dichloroethene

110

ug/L



FAG-36

9/16/2020

cis-1

,2-Dichloroethene

229

ug/L



FAG-43

9/16/2020

cis-1

,2-Dichloroethene

23.2

ug/L



FAG-46

9/16/2020

cis-1

,2-Dichloroethene

5.3

ug/L



FAG-47

9/15/2020

cis-1

,2-Dichloroethene

7.9

ug/L



FAG-56

9/15/2020

cis-1

,2-Dichloroethene

72.2

ug/L



FAG-73

9/16/2020

cis-1

,2-Dichloroethene

192

ug/L



FAG-74

9/17/2020

cis-1

,2-Dichloroethene

113

ug/L



FAG-85

9/17/2020

cis-1

,2-Dichloroethene

216

ug/L



FAG-88

9/16/2020

cis-1

,2-Dichloroethene

2.1

ug/L



FAG-89

9/17/2020

cis-1

,2-Dichloroethene

1.2

ug/L



FAG-AW4

9/17/2020

cis-1

,2-Dichloroethene

241

ug/L



RI-MW1

9/15/2020

cis-1

,2-Dichloroethene

1.3

ug/L



RI-MW2

9/15/2020

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW5

9/15/2020

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW6

9/15/2020

cis-1

,2-Dichloroethene

7.9

ug/L



RI-MW7

9/15/2020

cis-1

,2-Dichloroethene

1.6

ug/L



RI-MW8

9/15/2020

cis-1

,2-Dichloroethene

1

ug/L

u

RI-MW9

9/16/2020

cis-1

,2-Dichloroethene

1

ug/L

u

RW-341 A

9/17/2020

cis-1

,2-Dichloroethene

1

ug/L

u

SW-01

9/17/2020

cis-1

,2-Dichloroethene

1

ug/L

u

FAG-05

9/16/2020

Trichloroethene

31.7

ug/L



FAG-11

9/16/2020

Trichloroethene

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-22

9/17/2020

Tr

chloroethene

420

ug/L



FAG-31

9/17/2020

Tr

chloroethene

705

ug/L



FAG-32

9/16/2020

Tr

chloroethene

1

ug/L

U

FAG-33

9/15/2020

Tr

chloroethene

28.3

ug/L



FAG-34

9/16/2020

Tr

chloroethene

500

ug/L



FAG-35

9/16/2020

Tr

chloroethene

512

ug/L



FAG-36

9/16/2020

Tr

chloroethene

531

ug/L



FAG-43

9/16/2020

Tr

chloroethene

66.4

ug/L



FAG-46

9/16/2020

Tr

chloroethene

39

ug/L



FAG-47

9/15/2020

Tr

chloroethene

97.9

ug/L



FAG-56

9/15/2020

Tr

chloroethene

5.9

ug/L



FAG-73

9/16/2020

Tr

chloroethene

132

ug/L



FAG-74

9/17/2020

Tr

chloroethene

37.5

ug/L



FAG-85

9/17/2020

Tr

chloroethene

345

ug/L



FAG-88

9/16/2020

Tr

chloroethene

7.8

ug/L



FAG-89

9/17/2020

Tr

chloroethene

7

ug/L



FAG-AW4

9/17/2020

Tr

chloroethene

966

ug/L



RI-MW1

9/15/2020

Tr

chloroethene

47.5

ug/L



RI-MW2

9/15/2020

Tr

chloroethene

1

ug/L

U

RI-MW5

9/15/2020

Tr

chloroethene

14.5

ug/L



RI-MW6

9/15/2020

Tr

chloroethene

40.2

ug/L



RI-MW7

9/15/2020

Tr

chloroethene

11.1

ug/L



RI-MW8

9/15/2020

Tr

chloroethene

1.7

ug/L



RI-MW9

9/16/2020

Tr

chloroethene

4.4

ug/L



RW-341A

9/17/2020

Tr

chloroethene

1

ug/L

u

SW-01

9/17/2020

Tr

chloroethene

1.2

ug/L



FAG-05

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-11

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-22

9/17/2020

Vinyl

chlor

de

25

ug/L

u

FAG-31

9/17/2020

Vinyl

chlor

de

10

ug/L

u

FAG-32

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-33

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-34

9/16/2020

Vinyl

chlor

de



ug/L

u

FAG-35

9/16/2020

Vinyl

chlor

de



ug/L

u

FAG-36

9/16/2020

Vinyl

chlor

de

10

ug/L

u

FAG-43

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-46

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-47

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-56

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-73

9/16/2020

Vinyl

chlor

de

33

ug/L



FAG-74

9/17/2020

Vinyl

chlor

de

11.3

ug/L



FAG-85

9/17/2020

Vinyl

chlor

de

10

ug/L

u

FAG-88

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-89

9/17/2020

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

9/17/2020

Vinyl

chlor

de

23.2

ug/L



RI-MW1

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW2

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW5

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW6

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW7

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW8

9/15/2020

Vinyl

chlor

de

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

RI-MW9

9/16/2020

Vinyl chloride

1

ug/L

U

RW-341A

9/17/2020

Vinyl chloride

1

ug/L

U

SW-01

9/17/2020

Vinyl chloride

1

ug/L

u

FAG-05

5/19/2021

cis-1,2-Dichloroethene

3.1

ug/L



FAG-11

5/19/2021

cis-1,2-Dichloroethene

1

ug/L

u

FAG-22

5/20/2021

cis-1,2-Dichloroethene

165

ug/L



FAG-31

5/20/2021

cis-1,2-Dichloroethene

248

ug/L



FAG-32

5/19/2021

cis-1,2-Dichloroethene

43.7

ug/L



FAG-33

5/18/2021

cis-1,2-Dichloroethene

4.4

ug/L



FAG-34

5/19/2021

cis-1,2-Dichloroethene

238

ug/L



FAG-35

5/18/2021

cis-1,2-Dichloroethene

113

ug/L



FAG-36

5/19/2021

cis-1,2-Dichloroethene

240

ug/L



FAG-43

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

FAG-46

5/18/2021

cis-1,2-Dichloroethene

4

ug/L



FAG-47

5/18/2021

cis-1,2-Dichloroethene

5.9

ug/L



FAG-50

5/19/2021

cis-1,2-Dichloroethene

62.4

ug/L



FAG-56

5/18/2021

cis-1,2-Dichloroethene

76.8

ug/L



FAG-62

5/18/2021

cis-1,2-Dichloroethene

13.8

ug/L



FAG-73

5/19/2021

cis-1,2-Dichloroethene

45.8

ug/L



FAG-74

5/21/2021

cis-1,2-Dichloroethene

179

ug/L



FAG-85

5/21/2021

cis-1,2-Dichloroethene

204

ug/L



FAG-88

5/19/2021

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

5/20/2021

cis-1,2-Dichloroethene

1.3

ug/L



FAG-AW4

5/19/2021

cis-1,2-Dichloroethene

292

ug/L



RI-MW1

5/19/2021

cis-1,2-Dichloroethene

2

ug/L



RI-MW2

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

5/18/2021

cis-1,2-Dichloroethene

8.2

ug/L



RI-MW7

5/18/2021

cis-1,2-Dichloroethene

2.9

ug/L



RI-MW8

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

5/19/2021

cis-1,2-Dichloroethene

1

ug/L

u

RW-341 A

5/20/2021

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/20/2021

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

5/19/2021

Tr

chloroethene

23.9

ug/L



FAG-11

5/19/2021

Tr

chloroethene

1

ug/L

u

FAG-22

5/20/2021

Tr

chloroethene

344

ug/L



FAG-31

5/20/2021

Tr

chloroethene

733

ug/L



FAG-32

5/19/2021

Tr

chloroethene

183

ug/L



FAG-33

5/18/2021

Tr

chloroethene

28.9

ug/L



FAG-34

5/19/2021

Tr

chloroethene

462

ug/L



FAG-35

5/18/2021

Tr

chloroethene

488

ug/L



FAG-36

5/19/2021

Tr

chloroethene

535

ug/L



FAG-43

5/18/2021

Tr

chloroethene

1

ug/L

u

FAG-46

5/18/2021

Tr

chloroethene

27.7

ug/L



FAG-47

5/18/2021

Tr

chloroethene

55.4

ug/L



FAG-50

5/19/2021

Tr

chloroethene

3220

ug/L



FAG-56

5/18/2021

Tr

chloroethene

7.8

ug/L



FAG-62

5/18/2021

Tr

chloroethene

23.9

ug/L



FAG-73

5/19/2021

Tr

chloroethene

18.8

ug/L



FAG-74

5/21/2021

Tr

chloroethene

201

ug/L



FAG-85

5/21/2021

Tr

chloroethene

610

ug/L




-------
MANN KENDALL

INPUT

Well ID

Sample Date

Sample



Value Units

Q

FAG-88

5/19/2021

Tr

chloroethene

6.5

ug/L



FAG-89

5/20/2021

Tr

chloroethene

10.3

ug/L



FAG-AW4

5/19/2021

Tr

chloroethene

1150

ug/L



RI-MW1

5/19/2021

Tr

chloroethene

68.3

ug/L



RI-MW2

5/18/2021

Tr

chloroethene

1

ug/L

U

RI-MW5

5/18/2021

Tr

chloroethene

1

ug/L

U

RI-MW6

5/18/2021

Tr

chloroethene

45.4

ug/L



RI-MW7

5/18/2021

Tr

chloroethene

19.5

ug/L



RI-MW8

5/18/2021

Tr

chloroethene

2.1

ug/L



RI-MW9

5/19/2021

Tr

chloroethene

6.9

ug/L



RW-341A

5/20/2021

Tr

chloroethene

1

ug/L



SW-01

5/20/2021

Tr

chloroethene

1.3

ug/L



FAG-05

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-11

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/20/2021

Vinyl

chlor

de

18.3

ug/L



FAG-31

5/20/2021

Vinyl

chlor

de

10

ug/L

u

FAG-32

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-33

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-34

5/19/2021

Vinyl

chlor

de



ug/L

u

FAG-35

5/18/2021

Vinyl

chlor

de



ug/L

u

FAG-36

5/19/2021

Vinyl

chlor

de

10

ug/L

u

FAG-43

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-46

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/19/2021

Vinyl

chlor

de

20

ug/L

u

FAG-56

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-62

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/19/2021

Vinyl

chlor

de

4.2

ug/L



FAG-74

5/21/2021

Vinyl

chlor

de

18.9

ug/L



FAG-85

5/21/2021

Vinyl

chlor

de

37.2

ug/L



FAG-88

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/20/2021

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

5/19/2021

Vinyl

chlor

de

24.2

ug/L



RI-MW1

5/19/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW6

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW7

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW8

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW9

5/19/2021

Vinyl

chlor

de

1

ug/L

u

RW-341 A

5/20/2021

Vinyl

chlor

de

1

ug/L

u

SW-01

5/20/2021

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/19/2022 Tr

chloroethene

379 ug/L



FAG-31

5/19/2022 Tr

chloroethene

726 ug/L



FAG-33

5/17/2022 Tr

chloroethene

31.7 ug/L



FAG-43

5/17/2022 Tr

chloroethene

2.3 ug/L



FAG-50

5/19/2022 Tr

chloroethene

2050 ug/L



FAG-56

5/17/2022 Tr

chloroethene

8.9 ug/L



FAG-62

5/17/2022 Tr

chloroethene

16.3 ug/L



FAG-74

5/19/2022 Tr

chloroethene



4 ug/L

J

FAG-85

5/19/2022 Tr

chloroethene

252 ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-88

5/19/2022

Tr

chloroethene

7

ug/L



FAG-89

5/19/2022

Tr

chloroethene

8.6

ug/L



RI-MW1

5/17/2022

Tr

chloroethene

57.3

ug/L



RI-MW2

5/17/2022

Tr

chloroethene

1

ug/L

U

RI-MW5

5/17/2022

Tr

chloroethene

15.6

ug/L



RI-MW6

5/17/2022

Tr

chloroethene

64.2

ug/L



RI-MW7

5/17/2022

Tr

chloroethene

21.7

ug/L



RI-MW8

5/17/2022

Tr

chloroethene

1.6

ug/L



RW-341A

5/19/2022

Tr

chloroethene

0.6

ug/L

J

SW-01

5/19/2022

Tr

chloroethene

0.92

ug/L

J

FAG-05

5/18/2022

Tr

chloroethene

18.7

ug/L



FAG-11

5/18/2022

Tr

chloroethene

2.3

ug/L



FAG-32

5/18/2022

Tr

chloroethene

49.5

ug/L



FAG-34

5/18/2022

Tr

chloroethene

582

ug/L



FAG-35

5/18/2022

Tr

chloroethene

537

ug/L



FAG-36

5/18/2022

Tr

chloroethene

455

ug/L



FAG-46

5/18/2022

Tr

chloroethene

21.1

ug/L



FAG-47

5/18/2022

Tr

chloroethene

42.7

ug/L



FAG-73

5/18/2022

Tr

chloroethene

22.8

ug/L



FAG-AW4

5/18/2022

Tr

chloroethene

1160

ug/L



RI-MW9

5/18/2022

Tr

chloroethene

2

ug/L



FAG-22

5/19/2022

Vinyl

chlor

de

30.8

ug/L



FAG-31

5/19/2022

Vinyl

chlor

de

10

ug/L

U

FAG-33

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-43

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/19/2022

Vinyl

chlor

de

25

ug/L

u

FAG-56

5/17/2022

Vinyl

chlor

de

0.25

ug/L

J

FAG-62

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-74

5/19/2022

Vinyl

chlor

de

5

ug/L

u

FAG-85

5/19/2022

Vinyl

chlor

de

53.8

ug/L



FAG-88

5/19/2022

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/19/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW1

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW6

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW7

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW8

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RW-341 A

5/19/2022

Vinyl

chlor

de

1

ug/L

u

SW-01

5/19/2022

Vinyl

chlor

de

1

ug/L

u

FAG-05

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-11

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-32

5/18/2022

Vinyl

chlor

de

0.21

ug/L

J

FAG-34

5/18/2022

Vinyl

chlor

de

2.9

ug/L

J

FAG-35

5/18/2022

Vinyl

chlor

de

0.95

ug/L

J

FAG-36

5/18/2022

Vinyl

chlor

de

10

ug/L

u

FAG-46

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/18/2022

Vinyl

chlor

de

11

ug/L



FAG-AW4

5/18/2022

Vinyl

chlor

de

28.5

ug/L



RI-MW9

5/18/2022

Vinyl

chlor

de

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-22

5/19/2022

cis-1,2-Dichloroethene

206

ug/L



FAG-31

5/19/2022

cis-1,2-Dichloroethene

210

ug/L



FAG-33

5/17/2022

cis-1,2-Dichloroethene

4.7

ug/L



FAG-43

5/17/2022

cis-1,2-Dichloroethene

0.67

ug/L

J

FAG-50

5/19/2022

cis-1,2-Dichloroethene

157

ug/L



FAG-56

5/17/2022

cis-1,2-Dichloroethene

83.2

ug/L



FAG-62

5/17/2022

cis-1,2-Dichloroethene

9.6

ug/L



FAG-74

5/19/2022

cis-1,2-Dichloroethene

0.79

ug/L

J

FAG-85

5/19/2022

cis-1,2-Dichloroethene

367

ug/L



FAG-88

5/19/2022

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

5/19/2022

cis-1,2-Dichloroethene

1.3

ug/L



RI-MW1

5/17/2022

cis-1,2-Dichloroethene

1.7

ug/L



RI-MW2

5/17/2022

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

5/17/2022

cis-1,2-Dichloroethene

0.92

ug/L

J

RI-MW6

5/17/2022

cis-1,2-Dichloroethene

9.4

ug/L



RI-MW7

5/17/2022

cis-1,2-Dichloroethene

3.2

ug/L



RI-MW8

5/17/2022

cis-1,2-Dichloroethene

1

ug/L

U

RW-341A

5/19/2022

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/19/2022

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

5/18/2022

cis-1,2-Dichloroethene

2.6

ug/L



FAG-11

5/18/2022

cis-1,2-Dichloroethene

0.66

ug/L

J

FAG-32

5/18/2022

cis-1,2-Dichloroethene

12.3

ug/L



FAG-34

5/18/2022

cis-1,2-Dichloroethene

221

ug/L



FAG-35

5/18/2022

cis-1,2-Dichloroethene

111

ug/L



FAG-36

5/18/2022

cis-1,2-Dichloroethene

168

ug/L



FAG-46

5/18/2022

cis-1,2-Dichloroethene

1.7

ug/L



FAG-47

5/18/2022

cis-1,2-Dichloroethene

3.2

ug/L



FAG-73

5/18/2022

cis-1,2-Dichloroethene

44.2

ug/L



FAG-AW4

5/18/2022

cis-1,2-Dichloroethene

268

ug/L



RI-MW9

5/18/2022

cis-1,2-Dichloroethene

0.28

ug/L

J


-------
Prepared for FAG Bearings LLC

2022 Annual Report
RA - NCWS
Silver Creek and Saginaw, MO

Eight Most Recent Data Points

December 2022


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

FAG-05

4/27/2011

cis-1,2-Dichloroethene

8.6

ug/L

FAG-05

10/26/2011

cis-1,2-Dichloroethene

17.4

ug/L

FAG-05

5/2/2012

cis-1,2-Dichloroethene

8.1

ug/L

FAG-05

10/10/2012

cis-1,2-Dichloroethene

14

ug/L

FAG-05

5/15/2013

cis-1,2-Dichloroethene

6.1

ug/L

FAG-05

4/27/2011

Trichloroethene

47.8

ug/L

FAG-05

10/26/2011

Trichloroethene

77.6

ug/L

FAG-05

5/2/2012

Trichloroethene

44

ug/L

FAG-05

10/10/2012

Trichloroethene

62

ug/L

FAG-05

5/15/2013

Trichloroethene

35.9

ug/L

FAG-05

4/27/2011

Vinyl chloride

1

ug/L

FAG-05

10/26/2011

Vinyl chloride

1

ug/L

FAG-05

5/2/2012

Vinyl chloride

1

ug/L

FAG-05

10/10/2012

Vinyl chloride

1

ug/L

FAG-05

5/15/2013

Vinyl chloride

1

ug/L

FAG-11

5/5/2011

cis-1,2-Dichloroethene

2.2

ug/L

FAG-11

10/26/2011

cis-1,2-Dichloroethene

2.9

ug/L

FAG-11

5/3/2012

cis-1,2-Dichloroethene

2.2

ug/L

FAG-11

10/10/2012

cis-1,2-Dichloroethene

2

ug/L

FAG-11

5/14/2013

cis-1,2-Dichloroethene

1.5

ug/L

FAG-11

5/5/2011

Trichloroethene

13.7

ug/L

FAG-11

10/26/2011

Trichloroethene

15.1

ug/L

FAG-11

5/3/2012

Trichloroethene

13.5

ug/L

FAG-11

10/10/2012

Trichloroethene

10.8

ug/L

FAG-11

5/14/2013

Trichloroethene

8

ug/L

FAG-11

5/5/2011

Vinyl chloride

1

ug/L

FAG-11

10/26/2011

Vinyl chloride

1

ug/L

FAG-11

5/3/2012

Vinyl chloride

1

ug/L

FAG-11

10/10/2012

Vinyl chloride

1

ug/L

FAG-11

5/14/2013

Vinyl chloride

1

ug/L

FAG-22

4/28/2011

cis-1,2-Dichloroethene

681

ug/L

FAG-22

10/28/2011

cis-1,2-Dichloroethene

608

ug/L

FAG-22

5/3/2012

cis-1,2-Dichloroethene

531

ug/L

FAG-22

10/11/2012

cis-1,2-Dichloroethene

528

ug/L

FAG-22

5/16/2013

cis-1,2-Dichloroethene

477

ug/L

FAG-22

4/28/2011

Trichloroethene

1280

ug/L

FAG-22

10/28/2011

Trichloroethene

1410

ug/L

FAG-22

5/3/2012

Trichloroethene

1300

ug/L

FAG-22

10/11/2012

Trichloroethene

1660

ug/L

FAG-22

5/16/2013

Trichloroethene

1510

ug/L

FAG-22

4/28/2011

Vinyl chloride

127

ug/L

FAG-22

10/28/2011

Vinyl chloride

101

ug/L

FAG-22

5/3/2012

Vinyl chloride

117

ug/L

FAG-22

10/11/2012

Vinyl chloride

80.7

ug/L

FAG-22

5/16/2013

Vinyl chloride

60.8

ug/L

FAG-31

4/28/2011

cis-1,2-Dichloroethene

168

ug/L

FAG-31

10/27/2011

cis-1,2-Dichloroethene

168

ug/L

FAG-31

5/3/2012

cis-1,2-Dichloroethene

161

ug/L

FAG-31

10/11/2012

cis-1,2-Dichloroethene

201

ug/L

FAG-31

5/16/2013

cis-1,2-Dichloroethene

196

ug/L

FAG-31

4/28/2011

Trichloroethene

698

ug/L

FAG-31

10/27/2011

Trichloroethene

698

ug/L

Qualifier

U
U

u
u
u

u
u
u
u
u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-31

5/3/2012

Trichloroethene

698

ug/L



FAG-31

10/11/2012

Trichloroethene

705

ug/L



FAG-31

5/16/2013

Trichloroethene

724

ug/L



FAG-31

4/28/2011

Vinyl chloride

10

ug/L

U

FAG-31

10/27/2011

Vinyl chloride

1

ug/L

U

FAG-31

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-31

10/11/2012

Vinyl chloride

1

ug/L

u

FAG-31

5/16/2013

Vinyl chloride

1

ug/L

u

FAG-32

4/28/2011

cis-1,2-Dichloroethene

396

ug/L



FAG-32

10/25/2011

cis-1,2-Dichloroethene

406

ug/L



FAG-32

5/1/2012

cis-1,2-Dichloroethene

401

ug/L



FAG-32

10/9/2012

cis-1,2-Dichloroethene

487

ug/L



FAG-32

5/16/2013

cis-1,2-Dichloroethene

389

ug/L



FAG-32

4/28/2011

Trichloroethene

1690

ug/L



FAG-32

10/25/2011

Trichloroethene

1620

ug/L



FAG-32

5/1/2012

Trichloroethene

1670

ug/L



FAG-32

10/9/2012

Trichloroethene

1770

ug/L



FAG-32

5/16/2013

Trichloroethene

1380

ug/L



FAG-32

4/28/2011

Vinyl chloride

20

ug/L

u

FAG-32

10/25/2011

Vinyl chloride

20

ug/L

u

FAG-32

5/1/2012

Vinyl chloride

1

ug/L

u

FAG-32

10/9/2012

Vinyl chloride

20

ug/L

u

FAG-32

5/16/2013

Vinyl chloride

20

ug/L

u

FAG-33

4/27/2011

cis-1,2-Dichloroethene

3.3

ug/L



FAG-33

10/27/2011

cis-1,2-Dichloroethene

2.7

ug/L



FAG-33

5/2/2012

cis-1,2-Dichloroethene

2.3

ug/L



FAG-33

10/11/2012

cis-1,2-Dichloroethene

2.3

ug/L



FAG-33

5/14/2013

cis-1,2-Dichloroethene

2.8

ug/L



FAG-33

4/27/2011

Trichloroethene

29.2

ug/L



FAG-33

10/27/2011

Trichloroethene

20.2

ug/L



FAG-33

5/2/2012

Trichloroethene

19.7

ug/L



FAG-33

10/11/2012

Trichloroethene

17.3

ug/L



FAG-33

5/14/2013

Trichloroethene

23.9

ug/L



FAG-33

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-33

10/27/2011

Vinyl chloride

1

ug/L

u

FAG-33

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-33

10/11/2012

Vinyl chloride

1

ug/L

u

FAG-33

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-34

4/27/2011

cis-1,2-Dichloroethene

380

ug/L



FAG-34

10/27/2011

cis-1,2-Dichloroethene

345

ug/L



FAG-34

5/2/2012

cis-1,2-Dichloroethene

341

ug/L



FAG-34

10/11/2012

cis-1,2-Dichloroethene

358

ug/L



FAG-34

5/15/2013

cis-1,2-Dichloroethene

337

ug/L



FAG-34

4/27/2011

Trichloroethene

777

ug/L



FAG-34

10/27/2011

Trichloroethene

761

ug/L



FAG-34

5/2/2012

Trichloroethene

758

ug/L



FAG-34

10/11/2012

Trichloroethene

820

ug/L



FAG-34

5/15/2013

Trichloroethene

713

ug/L



FAG-34

4/27/2011

Vinyl chloride

11.6

ug/L

J

FAG-34

10/27/2011

Vinyl chloride

10

ug/L

u

FAG-34

5/2/2012

Vinyl chloride

12.2

ug/L



FAG-34

10/11/2012

Vinyl chloride

6.2

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-34

5/15/2013

Vinyl chloride

6.7

ug/L



FAG-35

4/27/2011

cis-1,2-Dichloroethene

173

ug/L



FAG-35

10/27/2011

cis-1,2-Dichloroethene

147

ug/L



FAG-35

5/2/2012

cis-1,2-Dichloroethene

125

ug/L



FAG-35

10/11/2012

cis-1,2-Dichloroethene

134

ug/L



FAG-35

5/15/2013

cis-1,2-Dichloroethene

124

ug/L



FAG-35

4/27/2011

Trichloroethene

583

ug/L



FAG-35

10/27/2011

Trichloroethene

499

ug/L



FAG-35

5/2/2012

Trichloroethene

436

ug/L



FAG-35

10/11/2012

Trichloroethene

467

ug/L



FAG-35

5/15/2013

Trichloroethene

429

ug/L



FAG-35

4/27/2011

Vinyl chloride

10

ug/L

U

FAG-35

10/27/2011

Vinyl chloride

10

ug/L

U

FAG-35

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-35

10/11/2012

Vinyl chloride

5

ug/L

u

FAG-35

5/15/2013

Vinyl chloride

5

ug/L

u

FAG-36

4/27/2011

cis-1,2-Dichloroethene

173

ug/L



FAG-36

10/27/2011

cis-1,2-Dichloroethene

192

ug/L



FAG-36

5/3/2012

cis-1,2-Dichloroethene

155

ug/L



FAG-36

10/11/2012

cis-1,2-Dichloroethene

183

ug/L



FAG-36

5/15/2013

cis-1,2-Dichloroethene

234

ug/L



FAG-36

4/27/2011

Trichloroethene

594

ug/L



FAG-36

10/27/2011

Trichloroethene

524

ug/L



FAG-36

5/3/2012

Trichloroethene

456

ug/L



FAG-36

10/11/2012

Trichloroethene

508

ug/L



FAG-36

5/15/2013

Trichloroethene

567

ug/L



FAG-36

4/27/2011

Vinyl chloride

10

ug/L

u

FAG-36

10/27/2011

Vinyl chloride

10

ug/L

u

FAG-36

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-36

10/11/2012

Vinyl chloride

10

ug/L

u

FAG-36

5/15/2013

Vinyl chloride

10

ug/L

u

FAG-43

4/26/2011

cis-1,2-Dichloroethene

82.1

ug/L



FAG-43

10/26/2011

cis-1,2-Dichloroethene

91.8

ug/L



FAG-43

5/3/2012

cis-1,2-Dichloroethene

1

ug/L

u

FAG-43

10/10/2012

cis-1,2-Dichloroethene

3.2

ug/L



FAG-43

5/15/2013

cis-1,2-Dichloroethene

1

ug/L

u

FAG-43

4/26/2011

Trichloroethene

313

ug/L



FAG-43

10/26/2011

Trichloroethene

289

ug/L



FAG-43

5/3/2012

Trichloroethene

1

ug/L

u

FAG-43

10/10/2012

Trichloroethene

12.2

ug/L



FAG-43

5/15/2013

Trichloroethene

1

ug/L

u

FAG-43

4/26/2011

Vinyl chloride

5

ug/L

u

FAG-43

10/26/2011

Vinyl chloride

5

ug/L

u

FAG-43

5/3/2012

Vinyl chloride

5

ug/L

u

FAG-43

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-43

5/15/2013

Vinyl chloride

1

ug/L

u

FAG-46

4/26/2011

cis-1,2-Dichloroethene

7

ug/L



FAG-46

10/27/2011

cis-1,2-Dichloroethene

6.9

ug/L



FAG-46

5/3/2012

cis-1,2-Dichloroethene

4.6

ug/L



FAG-46

10/10/2012

cis-1,2-Dichloroethene

5.1

ug/L



FAG-46

5/14/2013

cis-1,2-Dichloroethene

3.5

ug/L



FAG-46

4/26/2011

Trichloroethene

134

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-46

10/27/2011

Trichloroethene

135

ug/L



FAG-46

5/3/2012

Trichloroethene

103

ug/L



FAG-46

10/10/2012

Trichloroethene

130

ug/L



FAG-46

5/14/2013

Trichloroethene

70.2

ug/L



FAG-46

4/26/2011

Vinyl chloride

1

ug/L

U

FAG-46

10/27/2011

Vinyl chloride

1

ug/L

U

FAG-46

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-46

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-46

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-47

4/27/2011

cis-1,2-Dichloroethene

9.5

ug/L



FAG-47

10/27/2011

cis-1,2-Dichloroethene

8.8

ug/L



FAG-47

5/3/2012

cis-1,2-Dichloroethene

9.1

ug/L



FAG-47

10/9/2012

cis-1,2-Dichloroethene

9.7

ug/L



FAG-47

5/14/2013

cis-1,2-Dichloroethene

9.9

ug/L



FAG-47

4/27/2011

Trichloroethene

140

ug/L



FAG-47

10/27/2011

Trichloroethene

136

ug/L



FAG-47

5/3/2012

Trichloroethene

116

ug/L



FAG-47

10/9/2012

Trichloroethene

122

ug/L



FAG-47

5/14/2013

Trichloroethene

93.4

ug/L



FAG-47

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-47

10/27/2011

Vinyl chloride

1

ug/L

u

FAG-47

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-47

10/9/2012

Vinyl chloride

1

ug/L

u

FAG-47

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-50

4/27/2011

cis-1,2-Dichloroethene

20

ug/L

u

FAG-50

10/25/2011

cis-1,2-Dichloroethene

20

ug/L

u

FAG-50

5/3/2012

cis-1,2-Dichloroethene

14.2

ug/L



FAG-50

10/10/2012

cis-1,2-Dichloroethene

20

ug/L

u

FAG-50

5/15/2013

cis-1,2-Dichloroethene

26.3

ug/L



FAG-50

4/27/2011

Trichloroethene

1040

ug/L



FAG-50

10/25/2011

Trichloroethene

1350

ug/L



FAG-50

5/3/2012

Trichloroethene

957

ug/L



FAG-50

10/10/2012

Trichloroethene

1290

ug/L



FAG-50

5/15/2013

Trichloroethene

2160

ug/L



FAG-50

4/27/2011

Vinyl chloride

20

ug/L

u

FAG-50

10/25/2011

Vinyl chloride

20

ug/L

u

FAG-50

5/3/2012

Vinyl chloride

1

ug/L

u

FAG-50

10/10/2012

Vinyl chloride

20

ug/L

u

FAG-50

5/15/2013

Vinyl chloride

20

ug/L

u

FAG-56

4/27/2011

cis-1,2-Dichloroethene

98.5

ug/L



FAG-56

10/25/2011

cis-1,2-Dichloroethene

124

ug/L



FAG-56

5/1/2012

cis-1,2-Dichloroethene

117

ug/L



FAG-56

10/9/2012

cis-1,2-Dichloroethene

114

ug/L



FAG-56

5/14/2013

cis-1,2-Dichloroethene

122

ug/L



FAG-56

4/27/2011

Trichloroethene

8

ug/L



FAG-56

10/25/2011

Trichloroethene

8.9

ug/L



FAG-56

5/1/2012

Trichloroethene

9.4

ug/L



FAG-56

10/9/2012

Trichloroethene

8.6

ug/L



FAG-56

5/14/2013

Trichloroethene

9.6

ug/L



FAG-56

4/27/2011

Vinyl chloride

1

ug/L

u

FAG-56

10/25/2011

Vinyl chloride

1

ug/L

u

FAG-56

5/1/2012

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

FAG-56

10/9/2012

Vinyl chloride

1

ug/L

FAG-56

5/14/2013

Vinyl chloride

1

ug/L

FAG-62

4/27/2011

cis-1,2-Dichloroethene

15.3

ug/L

FAG-62

10/26/2011

cis-1,2-Dichloroethene

193

ug/L

FAG-62

5/1/2012

cis-1,2-Dichloroethene

61.6

ug/L

FAG-62

10/10/2012

cis-1,2-Dichloroethene

456

ug/L

FAG-62

5/15/2013

cis-1,2-Dichloroethene

277

ug/L

FAG-62

4/27/2011

Trichloroethene

51.7

ug/L

FAG-62

10/26/2011

Trichloroethene

185

ug/L

FAG-62

5/1/2012

Trichloroethene

64.9

ug/L

FAG-62

10/10/2012

Trichloroethene

103

ug/L

FAG-62

5/15/2013

Trichloroethene

167

ug/L

FAG-62

4/27/2011

Vinyl chloride

1

ug/L

FAG-62

10/26/2011

Vinyl chloride

1

ug/L

FAG-62

5/1/2012

Vinyl chloride

1

ug/L

FAG-62

10/10/2012

Vinyl chloride

2

ug/L

FAG-62

5/15/2013

Vinyl chloride

5

ug/L

FAG-73

4/28/2011

cis-1,2-Dichloroethene

143

ug/L

FAG-73

10/26/2011

cis-1,2-Dichloroethene

357

ug/L

FAG-73

5/1/2012

cis-1,2-Dichloroethene

396

ug/L

FAG-73

10/10/2012

cis-1,2-Dichloroethene

561

ug/L

FAG-73

5/16/2013

cis-1,2-Dichloroethene

425

ug/L

FAG-73

4/28/2011

Trichloroethene

73

ug/L

FAG-73

10/26/2011

Trichloroethene

82.3

ug/L

FAG-73

5/1/2012

Trichloroethene

103

ug/L

FAG-73

10/10/2012

Trichloroethene

163

ug/L

FAG-73

5/16/2013

Trichloroethene

215

ug/L

FAG-73

4/28/2011

Vinyl chloride

152

ug/L

FAG-73

10/26/2011

Vinyl chloride

616

ug/L

FAG-73

5/1/2012

Vinyl chloride

471

ug/L

FAG-73

10/10/2012

Vinyl chloride

415

ug/L

FAG-73

5/16/2013

Vinyl chloride

510

ug/L

FAG-74

4/28/2011

cis-1,2-Dichloroethene

1200

ug/L

FAG-74

10/26/2011

cis-1,2-Dichloroethene

1140

ug/L

FAG-74

5/1/2012

cis-1,2-Dichloroethene

908

ug/L

FAG-74

10/9/2012

cis-1,2-Dichloroethene

875

ug/L

FAG-74

5/16/2013

cis-1,2-Dichloroethene

1100

ug/L

FAG-74

4/28/2011

Trichloroethene

1430

ug/L

FAG-74

10/26/2011

Trichloroethene

893

ug/L

FAG-74

5/1/2012

Trichloroethene

770

ug/L

FAG-74

10/9/2012

Trichloroethene

575

ug/L

FAG-74

5/16/2013

Trichloroethene

1120

ug/L

FAG-74

4/28/2011

Vinyl chloride

161

ug/L

FAG-74

10/26/2011

Vinyl chloride

151

ug/L

FAG-74

5/1/2012

Vinyl chloride

146

ug/L

FAG-74

10/9/2012

Vinyl chloride

148

ug/L

FAG-74

5/16/2013

Vinyl chloride

149

ug/L

FAG-85

4/27/2011

cis-1,2-Dichloroethene

231

ug/L

FAG-85

10/25/2011

cis-1,2-Dichloroethene

189

ug/L

FAG-85

5/2/2012

cis-1,2-Dichloroethene

182

ug/L

FAG-85

10/9/2012

cis-1,2-Dichloroethene

216

ug/L

FAG-85

5/15/2013

cis-1,2-Dichloroethene

200

ug/L

Qualifier

U
U

u
u
u
u
u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-85

4/27/2011

Trichloroethene

692

ug/L



FAG-85

10/25/2011

Trichloroethene

650

ug/L

J

FAG-85

5/2/2012

Trichloroethene

637

ug/L



FAG-85

10/9/2012

Trichloroethene

671

ug/L



FAG-85

5/15/2013

Trichloroethene

596

ug/L



FAG-85

4/27/2011

Vinyl chloride

3.3

ug/L



FAG-85

10/25/2011

Vinyl chloride

20

ug/L

U

FAG-85

5/2/2012

Vinyl chloride

20

ug/L

U

FAG-85

10/9/2012

Vinyl chloride

5

ug/L

u

FAG-85

5/15/2013

Vinyl chloride

5

ug/L

u

FAG-88

5/5/2011

cis-1,2-Dichloroethene

3.4

ug/L



FAG-88

10/25/2011

cis-1,2-Dichloroethene

3.2

ug/L



FAG-88

5/2/2012

cis-1,2-Dichloroethene

2.5

ug/L



FAG-88

10/9/2012

cis-1,2-Dichloroethene

2.4

ug/L



FAG-88

5/14/2013

cis-1,2-Dichloroethene

2.5

ug/L



FAG-88

5/5/2011

Trichloroethene

10.8

ug/L



FAG-88

10/25/2011

Trichloroethene

9.3

ug/L



FAG-88

5/2/2012

Trichloroethene

8.5

ug/L



FAG-88

10/9/2012

Trichloroethene

7.3

ug/L



FAG-88

5/14/2013

Trichloroethene

6.4

ug/L



FAG-88

5/5/2011

Vinyl chloride

1

ug/L

u

FAG-88

10/25/2011

Vinyl chloride

1

ug/L

u

FAG-88

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-88

10/9/2012

Vinyl chloride

1

ug/L

u

FAG-88

5/14/2013

Vinyl chloride

1

ug/L

u

FAG-89

5/5/2011

cis-1,2-Dichloroethene

1.7

ug/L



FAG-89

10/26/2011

cis-1,2-Dichloroethene

2.4

ug/L



FAG-89

5/2/2012

cis-1,2-Dichloroethene

1.5

ug/L



FAG-89

10/10/2012

cis-1,2-Dichloroethene

3.1

ug/L



FAG-89

5/15/2013

cis-1,2-Dichloroethene

3.4

ug/L



FAG-89

5/5/2011

Trichloroethene

11.8

ug/L



FAG-89

10/26/2011

Trichloroethene

16.6

ug/L



FAG-89

5/2/2012

Trichloroethene

13.2

ug/L



FAG-89

10/10/2012

Trichloroethene

33.4

ug/L



FAG-89

5/15/2013

Trichloroethene

37.7

ug/L



FAG-89

5/5/2011

Vinyl chloride

1

ug/L

u

FAG-89

10/26/2011

Vinyl chloride

1

ug/L

u

FAG-89

5/2/2012

Vinyl chloride

1

ug/L

u

FAG-89

10/10/2012

Vinyl chloride

1

ug/L

u

FAG-89

5/15/2013

Vinyl chloride

1

ug/L

u

FAG-AW4

4/28/2011

cis-1,2-Dichloroethene

200

ug/L



FAG-AW4

10/27/2011

cis-1,2-Dichloroethene

200

ug/L



FAG-AW4

5/3/2012

cis-1,2-Dichloroethene

194

ug/L



FAG-AW4

10/11/2012

cis-1,2-Dichloroethene

218

ug/L



FAG-AW4

5/16/2013

cis-1,2-Dichloroethene

225

ug/L



FAG-AW4

4/28/2011

Trichloroethene

940

ug/L



FAG-AW4

10/27/2011

Trichloroethene

957

ug/L



FAG-AW4

5/3/2012

Trichloroethene

874

ug/L



FAG-AW4

10/11/2012

Trichloroethene

873

ug/L



FAG-AW4

5/16/2013

Trichloroethene

912

ug/L



FAG-AW4

4/28/2011

Vinyl chloride

10

ug/L

u

FAG-AW4

10/27/2011

Vinyl chloride

11.5

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-AW4

5/3/2012

Vinyl chloride

10

ug/L

U

FAG-AW4

10/11/2012

Vinyl chloride

10

ug/L

U

FAG-AW4

5/16/2013

Vinyl chloride

10.9

ug/L



RI-MW1

4/26/2011

cis-1,2-Dichloroethene

2.6

ug/L



RI-MW1

10/28/2011

cis-1,2-Dichloroethene

2.5

ug/L



RI-MW1

5/3/2012

cis-1,2-Dichloroethene

1.6

ug/L



RI-MW1

10/10/2012

cis-1,2-Dichloroethene

2.6

ug/L



RI-MW1

5/14/2013

cis-1,2-Dichloroethene

3.6

ug/L



RI-MW1

4/26/2011

Trichloroethene

80.7

ug/L



RI-MW1

10/28/2011

Trichloroethene

55.1

ug/L



RI-MW1

5/3/2012

Trichloroethene

41.2

ug/L



RI-MW1

10/10/2012

Trichloroethene

55

ug/L



RI-MW1

5/14/2013

Trichloroethene

85.1

ug/L



RI-MW1

4/26/2011

Vinyl chloride

1

ug/L

u

RI-MW1

10/28/2011

Vinyl chloride

1

ug/L

u

RI-MW1

5/3/2012

Vinyl chloride

1

ug/L

u

RI-MW1

10/10/2012

Vinyl chloride

1

ug/L

u

RI-MW1

5/14/2013

Vinyl chloride

1

ug/L

u

RI-MW2

4/26/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW2

10/26/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW2

5/3/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW2

10/10/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW2

5/14/2013

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW2

4/26/2011

Trichloroethene

1

ug/L

u

RI-MW2

10/26/2011

Trichloroethene

1

ug/L

u

RI-MW2

5/3/2012

Trichloroethene

1

ug/L

u

RI-MW2

10/10/2012

Trichloroethene

1

ug/L

u

RI-MW2

5/14/2013

Trichloroethene

1

ug/L

u

RI-MW2

4/26/2011

Vinyl chloride

1

ug/L

u

RI-MW2

10/26/2011

Vinyl chloride

1

ug/L

u

RI-MW2

5/3/2012

Vinyl chloride

1

ug/L

u

RI-MW2

10/10/2012

Vinyl chloride

1

ug/L

u

RI-MW2

5/14/2013

Vinyl chloride

1

ug/L

u

RI-MW5

4/26/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

10/25/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

5/1/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

10/9/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

5/14/2013

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

4/26/2011

Trichloroethene

4.3

ug/L



RI-MW5

10/25/2011

Trichloroethene

8.5

ug/L



RI-MW5

5/1/2012

Trichloroethene

7.4

ug/L



RI-MW5

10/9/2012

Trichloroethene

5.9

ug/L



RI-MW5

5/14/2013

Trichloroethene

4.8

ug/L



RI-MW5

4/26/2011

Vinyl chloride

1

ug/L

u

RI-MW5

10/25/2011

Vinyl chloride

1

ug/L

u

RI-MW5

5/1/2012

Vinyl chloride

1

ug/L

u

RI-MW5

10/9/2012

Vinyl chloride

1

ug/L

u

RI-MW5

5/14/2013

Vinyl chloride

1

ug/L

u

RI-MW6

4/27/2011

cis-1,2-Dichloroethene

7.6

ug/L



RI-MW6

10/26/2011

cis-1,2-Dichloroethene

6.3

ug/L



RI-MW6

5/2/2012

cis-1,2-Dichloroethene

5.4

ug/L



RI-MW6

10/10/2012

cis-1,2-Dichloroethene

5.2

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

RI-MW6

5/15/2013

cis-1,2-Dichloroethene

3.6

ug/L



RI-MW6

4/27/2011

Trichloroethene

48.6

ug/L



RI-MW6

10/26/2011

Trichloroethene

38.4

ug/L



RI-MW6

5/2/2012

Trichloroethene

33.6

ug/L



RI-MW6

10/10/2012

Trichloroethene

29.5

ug/L



RI-MW6

5/15/2013

Trichloroethene

17.9

ug/L



RI-MW6

4/27/2011

Vinyl chloride

1

ug/L

U

RI-MW6

10/26/2011

Vinyl chloride

1

ug/L

U

RI-MW6

5/2/2012

Vinyl chloride

1

ug/L

u

RI-MW6

10/10/2012

Vinyl chloride

1

ug/L

u

RI-MW6

5/15/2013

Vinyl chloride

1

ug/L

u

RI-MW7

4/26/2011

cis-1,2-Dichloroethene

2.8

ug/L



RI-MW7

10/25/2011

cis-1,2-Dichloroethene

2.8

ug/L



RI-MW7

5/1/2012

cis-1,2-Dichloroethene

2.7

ug/L



RI-MW7

10/9/2012

cis-1,2-Dichloroethene

4

ug/L



RI-MW7

5/15/2013

cis-1,2-Dichloroethene

3.5

ug/L



RI-MW7

4/26/2011

Trichloroethene

26.7

ug/L



RI-MW7

10/25/2011

Trichloroethene

23.7

ug/L



RI-MW7

5/1/2012

Trichloroethene

28.4

ug/L



RI-MW7

10/9/2012

Trichloroethene

31.9

ug/L



RI-MW7

5/15/2013

Trichloroethene

33.4

ug/L



RI-MW7

4/26/2011

Vinyl chloride

1

ug/L

u

RI-MW7

10/25/2011

Vinyl chloride

1

ug/L

u

RI-MW7

5/1/2012

Vinyl chloride

1

ug/L

u

RI-MW7

10/9/2012

Vinyl chloride

1

ug/L

u

RI-MW7

5/15/2013

Vinyl chloride

1

ug/L

u

RI-MW8

4/26/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW8

10/25/2011

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW8

5/1/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW8

10/9/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW8

5/14/2013

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW8

4/26/2011

Trichloroethene

4.3

ug/L



RI-MW8

10/25/2011

Trichloroethene

3.1

ug/L



RI-MW8

5/1/2012

Trichloroethene

3.7

ug/L



RI-MW8

10/9/2012

Trichloroethene

3.9

ug/L



RI-MW8

5/14/2013

Trichloroethene

3.7

ug/L



RI-MW8

4/26/2011

Vinyl chloride

1

ug/L

u

RI-MW8

10/25/2011

Vinyl chloride

1

ug/L

u

RI-MW8

5/1/2012

Vinyl chloride

1

ug/L

u

RI-MW8

10/9/2012

Vinyl chloride

1

ug/L

u

RI-MW8

5/14/2013

Vinyl chloride

1

ug/L

u

RI-MW9

4/26/2011

cis-1,2-Dichloroethene

1.6

ug/L



RI-MW9

10/26/2011

cis-1,2-Dichloroethene

1.4

ug/L



RI-MW9

5/2/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/10/2012

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

5/14/2013

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

4/26/2011

Trichloroethene

27.7

ug/L



RI-MW9

10/26/2011

Trichloroethene

22.1

ug/L



RI-MW9

5/2/2012

Trichloroethene

14.2

ug/L



RI-MW9

10/10/2012

Trichloroethene

10.3

ug/L



RI-MW9

5/14/2013

Trichloroethene

9.6

ug/L



RI-MW9

4/26/2011

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

RI-MW9

10/26/2011

Vinyl chloride

1

ug/L

U

RI-MW9

5/2/2012

Vinyl chloride

1

ug/L

U

RI-MW9

10/10/2012

Vinyl chloride

1

ug/L

u

RI-MW9

5/14/2013

Vinyl chloride

1

ug/L

u

RW-341A

4/28/2011

cis-1,2-Dichloroethene

1

ug/L

u

RW-341A

10/25/2011

cis-1,2-Dichloroethene

1

ug/L

u

RW-341 A

5/4/2012

cis-1,2-Dichloroethene

1

ug/L

u

RW-341 A

10/10/2012

cis-1,2-Dichloroethene

1

ug/L

u

RW-341 A

5/15/2013

cis-1,2-Dichloroethene

1

ug/L

u

RW-341 A

4/28/2011

Trichloroethene

1

ug/L

u

RW-341 A

10/25/2011

Trichloroethene

1

ug/L

u

RW-341 A

5/4/2012

Trichloroethene

1

ug/L



RW-341 A

10/10/2012

Trichloroethene

1

ug/L

u

RW-341 A

5/15/2013

Trichloroethene

1

ug/L

u

RW-341 A

4/28/2011

Vinyl chloride

1

ug/L

u

RW-341 A

10/25/2011

Vinyl chloride

1

ug/L

u

RW-341 A

5/4/2012

Vinyl chloride

1

ug/L

u

RW-341 A

10/10/2012

Vinyl chloride

1

ug/L

u

RW-341 A

5/15/2013

Vinyl chloride

1

ug/L

u

SW-01

4/28/2011

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/25/2011

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/4/2012

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/10/2012

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/15/2013

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

4/28/2011

Trichloroethene

1.1

ug/L



SW-01

10/25/2011

Trichloroethene

1

ug/L

u

SW-01

5/4/2012

Trichloroethene

1

ug/L

u

SW-01

10/10/2012

Trichloroethene

1.6

ug/L



SW-01

5/15/2013

Trichloroethene

1

ug/L

u

SW-01

4/28/2011

Vinyl chloride

1

ug/L

u

SW-01

10/25/2011

Vinyl chloride

1

ug/L

u

SW-01

5/4/2012

Vinyl chloride

1

ug/L

u

SW-01

10/10/2012

Vinyl chloride

1

ug/L

u

SW-01

5/15/2013

Vinyl chloride

1

ug/L

u

FAG-05

10/19/2016

cis-1,2-Dichloroethene

17.2

ug/L



FAG-11

10/19/2016

cis-1,2-Dichloroethene

1.9

ug/L



FAG-22

10/20/2016

cis-1,2-Dichloroethene

707

ug/L



FAG-31

10/20/2016

cis-1,2-Dichloroethene

305

ug/L



FAG-32

10/20/2016

cis-1,2-Dichloroethene

481

ug/L



FAG-33

10/18/2016

cis-1,2-Dichloroethene

3.5

ug/L



FAG-34

10/19/2016

cis-1,2-Dichloroethene

326

ug/L



FAG-35

10/19/2016

cis-1,2-Dichloroethene

126

ug/L



FAG-36

10/20/2016

cis-1,2-Dichloroethene

235

ug/L



FAG-43

10/19/2016

cis-1,2-Dichloroethene

9.9

ug/L



FAG-46

10/18/2016

cis-1,2-Dichloroethene

2.8

ug/L



FAG-47

10/18/2016

cis-1,2-Dichloroethene

10.6

ug/L



FAG-50

10/20/2016

cis-1,2-Dichloroethene

91.5

ug/L



FAG-56

10/18/2016

cis-1,2-Dichloroethene

105

ug/L



FAG-62

10/19/2016

cis-1,2-Dichloroethene

13.1

ug/L



FAG-73

10/19/2016

cis-1,2-Dichloroethene

282

ug/L



FAG-74

10/20/2016

cis-1,2-Dichloroethene

321

ug/L



FAG-85

10/19/2016

cis-1,2-Dichloroethene

48.9

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

FAG-88

10/18/2016

cis-1,2-Dichloroethene

2.2

ug/L



FAG-89

10/19/2016

cis-1,2-Dichloroethene

2.3

ug/L



FAG-AW4

10/20/2016

cis-1,2-Dichloroethene

270

ug/L



RI-MW1

10/18/2016

cis-1,2-Dichloroethene

2.2

ug/L



RI-MW2

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

10/19/2016

cis-1,2-Dichloroethene

6.4

ug/L



RI-MW7

10/19/2016

cis-1,2-Dichloroethene

3.3

ug/L



RI-MW8

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/18/2016

cis-1,2-Dichloroethene

1

ug/L

u

RW-341A

10/20/2016

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/20/2016

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

10/19/2016

Tr

chloroethene

75.6

ug/L



FAG-11

10/19/2016

Tr

chloroethene

9.6

ug/L



FAG-22

10/20/2016

Tr

chloroethene

1340

ug/L



FAG-31

10/20/2016

Tr

chloroethene

765

ug/L



FAG-32

10/20/2016

Tr

chloroethene

1570

ug/L



FAG-33

10/18/2016

Tr

chloroethene

28.1

ug/L



FAG-34

10/19/2016

Tr

chloroethene

574

ug/L



FAG-35

10/19/2016

Tr

chloroethene

516

ug/L



FAG-36

10/20/2016

Tr

chloroethene

566

ug/L



FAG-43

10/19/2016

Tr

chloroethene

50.6

ug/L



FAG-46

10/18/2016

Tr

chloroethene

50.6

ug/L



FAG-47

10/18/2016

Tr

chloroethene

76.9

ug/L



FAG-50

10/20/2016

Tr

chloroethene

2610

ug/L



FAG-56

10/18/2016

Tr

chloroethene

15.1

ug/L

J

FAG-62

10/19/2016

Tr

chloroethene

33.6

ug/L



FAG-73

10/19/2016

Tr

chloroethene

249

ug/L



FAG-74

10/20/2016

Tr

chloroethene

200

ug/L



FAG-85

10/19/2016

Tr

chloroethene

146

ug/L



FAG-88

10/18/2016

Tr

chloroethene

7.1

ug/L



FAG-89

10/19/2016

Tr

chloroethene

20.8

ug/L



FAG-AW4

10/20/2016

Tr

chloroethene

1150

ug/L

J

RI-MW1

10/18/2016

Tr

chloroethene

52.8

ug/L



RI-MW2

10/18/2016

Tr

chloroethene

1

ug/L

u

RI-MW5

10/18/2016

Tr

chloroethene

18.3

ug/L



RI-MW6

10/19/2016

Tr

chloroethene

38.1

ug/L



RI-MW7

10/19/2016

Tr

chloroethene

25.5

ug/L



RI-MW8

10/18/2016

Tr

chloroethene

3.1

ug/L



RI-MW9

10/18/2016

Tr

chloroethene

9.5

ug/L



RW-341 A

10/20/2016

Tr

chloroethene

1

ug/L

u

SW-01

10/20/2016

Tr

chloroethene

1

ug/L

u

FAG-05

10/19/2016

Vinyl chloride

1

ug/L

u

FAG-11

10/19/2016

Vinyl chloride

1

ug/L

u

FAG-22

10/20/2016

Vinyl chloride

93.1

ug/L



FAG-31

10/20/2016

Vinyl chloride

10

ug/L

u

FAG-32

10/20/2016

Vinyl chloride

20

ug/L

u

FAG-33

10/18/2016

Vinyl chloride

1

ug/L

u

FAG-34

10/19/2016

Vinyl chloride

10.6

ug/L



FAG-35

10/19/2016

Vinyl chloride

5

ug/L

u

FAG-36

10/20/2016

Vinyl chloride

20

ug/L

u

FAG-43

10/19/2016

Vinyl chloride

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-46

10/18/2016

Viny

chlor

de

1

ug/L

U

FAG-47

10/18/2016

Viny

chlor

de

1

ug/L

U

FAG-50

10/20/2016

Viny

chlor

de

20

ug/L

u

FAG-56

10/18/2016

Viny

chlor

de

1

ug/L

u

FAG-62

10/19/2016

Viny

chlor

de

1

ug/L

u

FAG-73

10/19/2016

Viny

chlor

de

212

ug/L



FAG-74

10/20/2016

Viny

chlor

de

75

ug/L



FAG-85

10/19/2016

Viny

chlor

de

5

ug/L

u

FAG-88

10/18/2016

Viny

chlor

de

1

ug/L

u

FAG-89

10/19/2016

Viny

chlor

de

1

ug/L

u

FAG-AW4

10/20/2016

Viny

chlor

de

16.2

ug/L



RI-MW1

10/18/2016

Viny

chlor

de

1

ug/L

u

RI-MW2

10/18/2016

Viny

chlor

de

1

ug/L

u

RI-MW5

10/18/2016

Viny

chlor

de

1

ug/L

u

RI-MW6

10/19/2016

Viny

chlor

de

1

ug/L

u

RI-MW7

10/19/2016

Viny

chlor

de

1

ug/L

u

RI-MW8

10/18/2016

Viny

chlor

de

1

ug/L

u

RI-MW9

10/18/2016

Viny

chlor

de

1

ug/L

u

RW-341A

10/20/2016

Viny

chlor

de

1

ug/L

u

SW-01

10/20/2016

Viny

chlor

de

1

ug/L

u

FAG-05

5/31/2017

cis-1

2-Dichloroethene

6.2

ug/L



FAG-11

5/30/2017

cis-1

2-Dichloroethene

1

ug/L

u

FAG-22

5/31/2017

cis-1

2-Dichloroethene

523

ug/L



FAG-31

5/31/2017

cis-1

2-Dichloroethene

276

ug/L



FAG-32

5/31/2017

cis-1

2-Dichloroethene

448

ug/L



FAG-33

5/27/2017

cis-1

2-Dichloroethene

3.6

ug/L



FAG-34

5/26/2017

cis-1

2-Dichloroethene

330

ug/L



FAG-35

5/31/2017

cis-1

2-Dichloroethene

107

ug/L



FAG-36

5/31/2017

cis-1

2-Dichloroethene

280

ug/L



FAG-43

5/31/2017

cis-1

2-Dichloroethene

1

ug/L

u

FAG-46

5/27/2017

cis-1

2-Dichloroethene

2.2

ug/L



FAG-47

5/27/2017

cis-1

2-Dichloroethene

7.7

ug/L



FAG-50

5/31/2017

cis-1

2-Dichloroethene

49.4

ug/L



FAG-56

5/27/2017

cis-1

2-Dichloroethene

115

ug/L



FAG-62

5/27/2017

cis-1

2-Dichloroethene

3.6

ug/L



FAG-73

5/31/2017

cis-1

2-Dichloroethene

96.6

ug/L



FAG-74

5/26/2017

cis-1

2-Dichloroethene

549

ug/L



FAG-85

5/31/2017

cis-1

2-Dichloroethene

170

ug/L



FAG-88

5/24/2017

cis-1

2-Dichloroethene

2

ug/L



FAG-89

5/30/2017

cis-1

2-Dichloroethene

2

ug/L



FAG-AW4

5/31/2017

cis-1

2-Dichloroethene

302

ug/L



RI-MW1

5/25/2017

cis-1

2-Dichloroethene

3

ug/L



RI-MW2

5/25/2017

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW5

5/25/2017

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW6

5/30/2017

cis-1

2-Dichloroethene

4.2

ug/L



RI-MW7

5/30/2017

cis-1

2-Dichloroethene

3.3

ug/L



RI-MW8

5/25/2017

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW9

5/25/2017

cis-1

2-Dichloroethene

1

ug/L

u

RW-341 A

5/31/2017

cis-1

2-Dichloroethene

1

ug/L

u

SW-01

5/31/2017

cis-1

2-Dichloroethene

1

ug/L

u

FAG-05

5/31/2017

Trichloroethene

32.8

ug/L



FAG-11

5/30/2017

Trichloroethene

1.9

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-22

5/31/2017

Tr

chloroethene

1860

ug/L



FAG-31

5/31/2017

Tr

chloroethene

719

ug/L



FAG-32

5/31/2017

Tr

chloroethene

1520

ug/L



FAG-33

5/27/2017

Tr

chloroethene

31.7

ug/L



FAG-34

5/26/2017

Tr

chloroethene

809

ug/L



FAG-35

5/31/2017

Tr

chloroethene

432

ug/L



FAG-36

5/31/2017

Tr

chloroethene

585

ug/L



FAG-43

5/31/2017

Tr

chloroethene

1

ug/L

U

FAG-46

5/27/2017

Tr

chloroethene

47.9

ug/L



FAG-47

5/27/2017

Tr

chloroethene

69.2

ug/L



FAG-50

5/31/2017

Tr

chloroethene

2610

ug/L



FAG-56

5/27/2017

Tr

chloroethene

9.3

ug/L



FAG-62

5/27/2017

Tr

chloroethene

33.6

ug/L



FAG-73

5/31/2017

Tr

chloroethene

58.3

ug/L



FAG-74

5/26/2017

Tr

chloroethene

789

ug/L



FAG-85

5/31/2017

Tr

chloroethene

527

ug/L



FAG-88

5/24/2017

Tr

chloroethene

6.8

ug/L



FAG-89

5/30/2017

Tr

chloroethene

18.8

ug/L



FAG-AW4

5/31/2017

Tr

chloroethene

1070

ug/L



RI-MW1

5/25/2017

Tr

chloroethene

96.4

ug/L



RI-MW2

5/25/2017

Tr

chloroethene

1

ug/L

U

RI-MW5

5/25/2017

Tr

chloroethene

12.7

ug/L



RI-MW6

5/30/2017

Tr

chloroethene

22.2

ug/L



RI-MW7

5/30/2017

Tr

chloroethene

25.8

ug/L



RI-MW8

5/25/2017

Tr

chloroethene

3.4

ug/L



RI-MW9

5/25/2017

Tr

chloroethene

6.4

ug/L



RW-341A

5/31/2017

Tr

chloroethene

1

ug/L

u

SW-01

5/31/2017

Tr

chloroethene

1

ug/L

u

FAG-05

5/31/2017

Vinyl

chlor

de

1

ug/L

u

FAG-11

5/30/2017

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/31/2017

Vinyl

chlor

de

63.1

ug/L



FAG-31

5/31/2017

Vinyl

chlor

de

10

ug/L

u

FAG-32

5/31/2017

Vinyl

chlor

de

20

ug/L

u

FAG-33

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-34

5/26/2017

Vinyl

chlor

de

5.9

ug/L



FAG-35

5/31/2017

Vinyl

chlor

de

5

ug/L

u

FAG-36

5/31/2017

Vinyl

chlor

de

10

ug/L

u

FAG-43

5/31/2017

Vinyl

chlor

de

1

ug/L

u

FAG-46

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/31/2017

Vinyl

chlor

de

20

ug/L

u

FAG-56

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-62

5/27/2017

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/31/2017

Vinyl

chlor

de

177

ug/L



FAG-74

5/26/2017

Vinyl

chlor

de

75.2

ug/L



FAG-85

5/31/2017

Vinyl

chlor

de

2

ug/L

u

FAG-88

5/24/2017

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/30/2017

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

5/31/2017

Vinyl

chlor

de

18.7

ug/L



RI-MW1

5/25/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/25/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/25/2017

Vinyl

chlor

de

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

RI-MW6

5/30/2017

Vinyl chloride

1

ug/L

U

RI-MW7

5/30/2017

Vinyl chloride

1

ug/L

U

RI-MW8

5/25/2017

Vinyl chloride

1

ug/L

u

RI-MW9

5/25/2017

Vinyl chloride

1

ug/L

u

RW-341A

5/31/2017

Vinyl chloride

1

ug/L

u

SW-01

5/31/2017

Vinyl chloride

1

ug/L

u

FAG-05

10/12/2017

cis-1,2-Dichloroethene

14.5

ug/L



FAG-11

10/11/2017

cis-1,2-Dichloroethene

1

ug/L

u

FAG-22

10/12/2017

cis-1,2-Dichloroethene

464

ug/L



FAG-31

10/12/2017

cis-1,2-Dichloroethene

247

ug/L



FAG-32

10/12/2017

cis-1,2-Dichloroethene

448

ug/L



FAG-33

10/8/2017

cis-1,2-Dichloroethene

3.3

ug/L



FAG-34

10/11/2017

cis-1,2-Dichloroethene

324

ug/L



FAG-35

10/11/2017

cis-1,2-Dichloroethene

123

ug/L



FAG-36

10/11/2017

cis-1,2-Dichloroethene

197

ug/L



FAG-43

10/11/2017

cis-1,2-Dichloroethene

11.7

ug/L



FAG-46

10/11/2017

cis-1,2-Dichloroethene

4.7

ug/L



FAG-47

10/8/2017

cis-1,2-Dichloroethene

11.3

ug/L



FAG-56

10/10/2017

cis-1,2-Dichloroethene

120

ug/L



FAG-73

10/11/2017

cis-1,2-Dichloroethene

260

ug/L



FAG-74

10/12/2017

cis-1,2-Dichloroethene

254

ug/L



FAG-85

10/11/2017

cis-1,2-Dichloroethene

135

ug/L



FAG-88

10/11/2017

cis-1,2-Dichloroethene

1.8

ug/L



FAG-89

10/12/2017

cis-1,2-Dichloroethene

2.4

ug/L



FAG-AW4

10/12/2017

cis-1,2-Dichloroethene

299

ug/L



RI-MW1

10/8/2017

cis-1,2-Dichloroethene

2.6

ug/L



RI-MW2

10/8/2017

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW5

10/8/2017

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

10/11/2017

cis-1,2-Dichloroethene

5.6

ug/L



RI-MW7

10/11/2017

cis-1,2-Dichloroethene

4.4

ug/L



RI-MW8

10/8/2017

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/8/2017

cis-1,2-Dichloroethene

1.4

ug/L



RW-341 A

10/11/2017

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/11/2017

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

10/12/2017

Tr

chloroethene

69.6

ug/L



FAG-11

10/11/2017

Tr

chloroethene

1

ug/L

u

FAG-22

10/12/2017

Tr

chloroethene

1280

ug/L



FAG-31

10/12/2017

Tr

chloroethene

735

ug/L



FAG-32

10/12/2017

Tr

chloroethene

1780

ug/L



FAG-33

10/8/2017

Tr

chloroethene

31

ug/L



FAG-34

10/11/2017

Tr

chloroethene

644

ug/L



FAG-35

10/11/2017

Tr

chloroethene

543

ug/L



FAG-36

10/11/2017

Tr

chloroethene

676

ug/L



FAG-43

10/11/2017

Tr

chloroethene

34.9

ug/L



FAG-46

10/11/2017

Tr

chloroethene

53.5

ug/L



FAG-47

10/8/2017

Tr

chloroethene

103

ug/L



FAG-56

10/10/2017

Tr

chloroethene

9.5

ug/L



FAG-73

10/11/2017

Tr

chloroethene

171

ug/L



FAG-74

10/12/2017

Tr

chloroethene

101

ug/L



FAG-85

10/11/2017

Tr

chloroethene

442

ug/L



FAG-88

10/11/2017

Tr

chloroethene

5.9

ug/L



FAG-89

10/12/2017

Tr

chloroethene

20.9

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-AW4

10/12/2017

Tr

chloroethene

1120

ug/L



RI-MW1

10/8/2017

Tr

chloroethene

47.4

ug/L



RI-MW2

10/8/2017

Tr

chloroethene

1

ug/L

U

RI-MW5

10/8/2017

Tr

chloroethene

17.5

ug/L



RI-MW6

10/11/2017

Tr

chloroethene

30.9

ug/L



RI-MW7

10/11/2017

Tr

chloroethene

32

ug/L



RI-MW8

10/8/2017

Tr

chloroethene

3.1

ug/L



RI-MW9

10/8/2017

Tr

chloroethene

4.5

ug/L



RW-341A

10/11/2017

Tr

chloroethene

1

ug/L



SW-01

10/11/2017

Tr

chloroethene

1.3

ug/L



FAG-05

10/12/2017

Vinyl

chlor

de

1

ug/L

U

FAG-11

10/11/2017

Vinyl

chlor

de

1

ug/L

u

FAG-22

10/12/2017

Vinyl

chlor

de

73.6

ug/L



FAG-31

10/12/2017

Vinyl

chlor

de

10

ug/L

u

FAG-32

10/12/2017

Vinyl

chlor

de

20

ug/L

u

FAG-33

10/8/2017

Vinyl

chlor

de

1

ug/L

u

FAG-34

10/11/2017

Vinyl

chlor

de

6.8

ug/L



FAG-35

10/11/2017

Vinyl

chlor

de



ug/L

u

FAG-36

10/11/2017

Vinyl

chlor

de

10

ug/L

u

FAG-43

10/11/2017

Vinyl

chlor

de

1

ug/L

u

FAG-46

10/11/2017

Vinyl

chlor

de

1

ug/L

u

FAG-47

10/8/2017

Vinyl

chlor

de

1

ug/L

u

FAG-56

10/10/2017

Vinyl

chlor

de

1

ug/L

u

FAG-73

10/11/2017

Vinyl

chlor

de

140

ug/L



FAG-74

10/12/2017

Vinyl

chlor

de

44

ug/L



FAG-85

10/11/2017

Vinyl

chlor

de

10

ug/L

u

FAG-88

10/11/2017

Vinyl

chlor

de

1

ug/L

u

FAG-89

10/12/2017

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

10/12/2017

Vinyl

chlor

de

19.9

ug/L



RI-MW1

10/8/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW2

10/8/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW5

10/8/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW6

10/11/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW7

10/11/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW8

10/8/2017

Vinyl

chlor

de

1

ug/L

u

RI-MW9

10/8/2017

Vinyl

chlor

de

1

ug/L

u

RW-341 A

10/11/2017

Vinyl

chlor

de

1

ug/L

u

SW-01

10/11/2017

Vinyl

chlor

de

1

ug/L

u

FAG-05

10/11/2018

cis-1,2-Dichloroethene

12.8

ug/L



FAG-11

10/10/2018

cis-1,2-Dichloroethene

1

ug/L

u

FAG-22

10/11/2018

cis-1,2-Dichloroethene

514

ug/L



FAG-31

10/11/2018

cis-1,2-Dichloroethene

274

ug/L



FAG-32

10/10/2018

cis-1,2-Dichloroethene

476

ug/L



FAG-33

10/9/2018

cis-1,2-Dichloroethene

3.7

ug/L



FAG-34

10/10/2018

cis-1,2-Dichloroethene

320

ug/L



FAG-35

10/10/2018

cis-1,2-Dichloroethene

131

ug/L



FAG-36

10/10/2018

cis-1,2-Dichloroethene

257

ug/L



FAG-43

10/10/2018

cis-1,2-Dichloroethene

1

ug/L

u

FAG-46

10/9/2018

cis-1,2-Dichloroethene

3.6

ug/L



FAG-47

10/9/2018

cis-1,2-Dichloroethene

8.6

ug/L



FAG-56

10/9/2018

cis-1,2-Dichloroethene

113

ug/L



FAG-73

10/10/2018

cis-1,2-Dichloroethene

305

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

FAG-74

10/10/2018

cis-1,2-Dichloroethene

223

ug/L



FAG-85

10/11/2018

cis-1,2-Dichloroethene

221

ug/L



FAG-88

10/11/2018

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

10/10/2018

cis-1,2-Dichloroethene

5.7

ug/L



FAG-AW4

10/11/2018

cis-1,2-Dichloroethene

311

ug/L



RI-MW1

10/10/2018

cis-1,2-Dichloroethene

2.8

ug/L



RI-MW2

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

10/9/2018

cis-1,2-Dichloroethene

4

ug/L



RI-MW7

10/9/2018

cis-1,2-Dichloroethene

4.1

ug/L



RI-MW8

10/9/2018

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

10/10/2018

cis-1,2-Dichloroethene

1

ug/L



RW-341A

10/11/2018

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

10/11/2018

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

10/11/2018

Tr

chloroethene

67.9

ug/L



FAG-11

10/10/2018

Tr

chloroethene

1

ug/L

u

FAG-22

10/11/2018

Tr

chloroethene

1680

ug/L



FAG-31

10/11/2018

Tr

chloroethene

934

ug/L



FAG-32

10/10/2018

Tr

chloroethene

1920

ug/L



FAG-33

10/9/2018

Tr

chloroethene

29.6

ug/L



FAG-34

10/10/2018

Tr

chloroethene

762

ug/L



FAG-35

10/10/2018

Tr

chloroethene

597

ug/L



FAG-36

10/10/2018

Tr

chloroethene

672

ug/L



FAG-43

10/10/2018

Tr

chloroethene

1

ug/L

u

FAG-46

10/9/2018

Tr

chloroethene

56.9

ug/L



FAG-47

10/9/2018

Tr

chloroethene

63.3

ug/L



FAG-56

10/9/2018

Tr

chloroethene

9.6

ug/L



FAG-73

10/10/2018

Tr

chloroethene

242

ug/L



FAG-74

10/10/2018

Tr

chloroethene

123

ug/L



FAG-85

10/11/2018

Tr

chloroethene

794

ug/L



FAG-88

10/11/2018

Tr

chloroethene

5.7

ug/L



FAG-89

10/10/2018

Tr

chloroethene

63.6

ug/L



FAG-AW4

10/11/2018

Tr

chloroethene

1250

ug/L



RI-MW1

10/10/2018

Tr

chloroethene

99.7

ug/L



RI-MW2

10/9/2018

Tr

chloroethene

1

ug/L

u

RI-MW5

10/9/2018

Tr

chloroethene

13.5

ug/L



RI-MW6

10/9/2018

Tr

chloroethene

21.7

ug/L



RI-MW7

10/9/2018

Tr

chloroethene

33.1

ug/L



RI-MW8

10/9/2018

Tr

chloroethene

3.1

ug/L



RI-MW9

10/10/2018

Tr

chloroethene

4.5

ug/L



RW-341 A

10/11/2018

Tr

chloroethene

1

ug/L

u

SW-01

10/11/2018

Tr

chloroethene

1.5

ug/L



FAG-05

10/11/2018

Vinyl chloride

1

ug/L

u

FAG-11

10/10/2018

Vinyl chloride

1

ug/L

u

FAG-22

10/11/2018

Vinyl chloride

110

ug/L



FAG-31

10/11/2018

Vinyl chloride

10

ug/L

u

FAG-32

10/10/2018

Vinyl chloride

20

ug/L

u

FAG-33

10/9/2018

Vinyl chloride

1

ug/L

u

FAG-34

10/10/2018

Vinyl chloride

6.5

ug/L



FAG-35

10/10/2018

Vinyl chloride

5

ug/L

u

FAG-36

10/10/2018

Vinyl chloride

10

ug/L

u

FAG-43

10/10/2018

Vinyl chloride

1

ug/L

u

Qualifier


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-46

10/9/2018

Viny

chlor

de

1

ug/L

U

FAG-47

10/9/2018

Viny

chlor

de

1

ug/L

U

FAG-56

10/9/2018

Viny

chlor

de

1

ug/L

u

FAG-73

10/10/2018

Viny

chlor

de

212

ug/L



FAG-74

10/10/2018

Viny

chlor

de

31.1

ug/L



FAG-85

10/11/2018

Viny

chlor

de

2.5

ug/L



FAG-88

10/11/2018

Viny

chlor

de

1

ug/L

u

FAG-89

10/10/2018

Viny

chlor

de

1

ug/L

u

FAG-AW4

10/11/2018

Viny

chlor

de

35.2

ug/L



RI-MW1

10/10/2018

Viny

chlor

de

1

ug/L

u

RI-MW2

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW5

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW6

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW7

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW8

10/9/2018

Viny

chlor

de

1

ug/L

u

RI-MW9

10/10/2018

Viny

chlor

de

1

ug/L

u

RW-341A

10/11/2018

Viny

chlor

de

1

ug/L

u

SW-01

10/11/2018

Viny

chlor

de

1

ug/L

u

FAG-05

9/16/2020

cis-1

2-Dichloroethene

5.5

ug/L



FAG-11

9/16/2020

cis-1

2-Dichloroethene

1

ug/L

u

FAG-22

9/17/2020

cis-1

2-Dichloroethene

189

ug/L



FAG-31

9/17/2020

cis-1

2-Dichloroethene

244

ug/L



FAG-32

9/16/2020

cis-1

2-Dichloroethene

1

ug/L

u

FAG-33

9/15/2020

cis-1

2-Dichloroethene

3.8

ug/L



FAG-34

9/16/2020

cis-1

2-Dichloroethene

249

ug/L



FAG-35

9/16/2020

cis-1

2-Dichloroethene

110

ug/L



FAG-36

9/16/2020

cis-1

2-Dichloroethene

229

ug/L



FAG-43

9/16/2020

cis-1

2-Dichloroethene

23.2

ug/L



FAG-46

9/16/2020

cis-1

2-Dichloroethene

5.3

ug/L



FAG-47

9/15/2020

cis-1

2-Dichloroethene

7.9

ug/L



FAG-56

9/15/2020

cis-1

2-Dichloroethene

72.2

ug/L



FAG-73

9/16/2020

cis-1

2-Dichloroethene

192

ug/L



FAG-74

9/17/2020

cis-1

2-Dichloroethene

113

ug/L



FAG-85

9/17/2020

cis-1

2-Dichloroethene

216

ug/L



FAG-88

9/16/2020

cis-1

2-Dichloroethene

2.1

ug/L



FAG-89

9/17/2020

cis-1

2-Dichloroethene

1.2

ug/L



FAG-AW4

9/17/2020

cis-1

2-Dichloroethene

241

ug/L



RI-MW1

9/15/2020

cis-1

2-Dichloroethene

1.3

ug/L



RI-MW2

9/15/2020

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW5

9/15/2020

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW6

9/15/2020

cis-1

2-Dichloroethene

7.9

ug/L



RI-MW7

9/15/2020

cis-1

2-Dichloroethene

1.6

ug/L



RI-MW8

9/15/2020

cis-1

2-Dichloroethene

1

ug/L

u

RI-MW9

9/16/2020

cis-1

2-Dichloroethene

1

ug/L

u

RW-341 A

9/17/2020

cis-1

2-Dichloroethene

1

ug/L

u

SW-01

9/17/2020

cis-1

2-Dichloroethene

1

ug/L

u

FAG-05

9/16/2020

Trichloroethene

31.7

ug/L



FAG-11

9/16/2020

Trichloroethene

1

ug/L

u

FAG-22

9/17/2020

Trichloroethene

420

ug/L



FAG-31

9/17/2020

Trichloroethene

705

ug/L



FAG-32

9/16/2020

Trichloroethene

1

ug/L

u

FAG-33

9/15/2020

Trichloroethene

28.3

ug/L




-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Qualifier

FAG-34

9/16/2020

Tr

chloroethene

500

ug/L



FAG-35

9/16/2020

Tr

chloroethene

512

ug/L



FAG-36

9/16/2020

Tr

chloroethene

531

ug/L



FAG-43

9/16/2020

Tr

chloroethene

66.4

ug/L



FAG-46

9/16/2020

Tr

chloroethene

39

ug/L



FAG-47

9/15/2020

Tr

chloroethene

97.9

ug/L



FAG-56

9/15/2020

Tr

chloroethene

5.9

ug/L



FAG-73

9/16/2020

Tr

chloroethene

132

ug/L



FAG-74

9/17/2020

Tr

chloroethene

37.5

ug/L



FAG-85

9/17/2020

Tr

chloroethene

345

ug/L



FAG-88

9/16/2020

Tr

chloroethene

7.8

ug/L



FAG-89

9/17/2020

Tr

chloroethene

7

ug/L



FAG-AW4

9/17/2020

Tr

chloroethene

966

ug/L



RI-MW1

9/15/2020

Tr

chloroethene

47.5

ug/L



RI-MW2

9/15/2020

Tr

chloroethene

1

ug/L

U

RI-MW5

9/15/2020

Tr

chloroethene

14.5

ug/L



RI-MW6

9/15/2020

Tr

chloroethene

40.2

ug/L



RI-MW7

9/15/2020

Tr

chloroethene

11.1

ug/L



RI-MW8

9/15/2020

Tr

chloroethene

1.7

ug/L



RI-MW9

9/16/2020

Tr

chloroethene

4.4

ug/L



RW-341A

9/17/2020

Tr

chloroethene

1

ug/L

U

SW-01

9/17/2020

Tr

chloroethene

1.2

ug/L



FAG-05

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-11

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-22

9/17/2020

Vinyl

chlor

de

25

ug/L

u

FAG-31

9/17/2020

Vinyl

chlor

de

10

ug/L

u

FAG-32

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-33

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-34

9/16/2020

Vinyl

chlor

de



ug/L

u

FAG-35

9/16/2020

Vinyl

chlor

de



ug/L

u

FAG-36

9/16/2020

Vinyl

chlor

de

10

ug/L

u

FAG-43

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-46

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-47

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-56

9/15/2020

Vinyl

chlor

de

1

ug/L

u

FAG-73

9/16/2020

Vinyl

chlor

de

33

ug/L



FAG-74

9/17/2020

Vinyl

chlor

de

11.3

ug/L



FAG-85

9/17/2020

Vinyl

chlor

de

10

ug/L

u

FAG-88

9/16/2020

Vinyl

chlor

de

1

ug/L

u

FAG-89

9/17/2020

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

9/17/2020

Vinyl

chlor

de

23.2

ug/L



RI-MW1

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW2

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW5

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW6

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW7

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW8

9/15/2020

Vinyl

chlor

de

1

ug/L

u

RI-MW9

9/16/2020

Vinyl

chlor

de

1

ug/L

u

RW-341 A

9/17/2020

Vinyl

chlor

de

1

ug/L

u

SW-01

9/17/2020

Vinyl

chlor

de

1

ug/L

u

FAG-05

5/19/2021 cis-1,2-Dichloroethene

3.1

ug/L



FAG-11

5/19/2021 cis-1,2-Dichloroethene

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Qualifier

FAG-22

5/20/2021

cis-1,2-Dichloroethene

165

ug/L



FAG-31

5/20/2021

cis-1,2-Dichloroethene

248

ug/L



FAG-32

5/19/2021

cis-1,2-Dichloroethene

43.7

ug/L



FAG-33

5/18/2021

cis-1,2-Dichloroethene

4.4

ug/L



FAG-34

5/19/2021

cis-1,2-Dichloroethene

238

ug/L



FAG-35

5/18/2021

cis-1,2-Dichloroethene

113

ug/L



FAG-36

5/19/2021

cis-1,2-Dichloroethene

240

ug/L



FAG-43

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

U

FAG-46

5/18/2021

cis-1,2-Dichloroethene

4

ug/L



FAG-47

5/18/2021

cis-1,2-Dichloroethene

5.9

ug/L



FAG-50

5/19/2021

cis-1,2-Dichloroethene

62.4

ug/L



FAG-56

5/18/2021

cis-1,2-Dichloroethene

76.8

ug/L



FAG-62

5/18/2021

cis-1,2-Dichloroethene

13.8

ug/L



FAG-73

5/19/2021

cis-1,2-Dichloroethene

45.8

ug/L



FAG-74

5/21/2021

cis-1,2-Dichloroethene

179

ug/L



FAG-85

5/21/2021

cis-1,2-Dichloroethene

204

ug/L



FAG-88

5/19/2021

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

5/20/2021

cis-1,2-Dichloroethene

1.3

ug/L



FAG-AW4

5/19/2021

cis-1,2-Dichloroethene

292

ug/L



RI-MW1

5/19/2021

cis-1,2-Dichloroethene

2

ug/L



RI-MW2

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW6

5/18/2021

cis-1,2-Dichloroethene

8.2

ug/L



RI-MW7

5/18/2021

cis-1,2-Dichloroethene

2.9

ug/L



RI-MW8

5/18/2021

cis-1,2-Dichloroethene

1

ug/L

u

RI-MW9

5/19/2021

cis-1,2-Dichloroethene

1

ug/L

u

RW-341A

5/20/2021

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/20/2021

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

5/19/2021

Tr

chloroethene

23.9

ug/L



FAG-11

5/19/2021

Tr

chloroethene

1

ug/L

u

FAG-22

5/20/2021

Tr

chloroethene

344

ug/L



FAG-31

5/20/2021

Tr

chloroethene

733

ug/L



FAG-32

5/19/2021

Tr

chloroethene

183

ug/L



FAG-33

5/18/2021

Tr

chloroethene

28.9

ug/L



FAG-34

5/19/2021

Tr

chloroethene

462

ug/L



FAG-35

5/18/2021

Tr

chloroethene

488

ug/L



FAG-36

5/19/2021

Tr

chloroethene

535

ug/L



FAG-43

5/18/2021

Tr

chloroethene

1

ug/L

u

FAG-46

5/18/2021

Tr

chloroethene

27.7

ug/L



FAG-47

5/18/2021

Tr

chloroethene

55.4

ug/L



FAG-50

5/19/2021

Tr

chloroethene

3220

ug/L



FAG-56

5/18/2021

Tr

chloroethene

7.8

ug/L



FAG-62

5/18/2021

Tr

chloroethene

23.9

ug/L



FAG-73

5/19/2021

Tr

chloroethene

18.8

ug/L



FAG-74

5/21/2021

Tr

chloroethene

201

ug/L



FAG-85

5/21/2021

Tr

chloroethene

610

ug/L



FAG-88

5/19/2021

Tr

chloroethene

6.5

ug/L



FAG-89

5/20/2021

Tr

chloroethene

10.3

ug/L



FAG-AW4

5/19/2021

Tr

chloroethene

1150

ug/L



RI-MW1

5/19/2021

Tr

chloroethene

68.3

ug/L



RI-MW2

5/18/2021

Tr

chloroethene

1

ug/L

u

RI-MW5

5/18/2021

Tr

chloroethene

1

ug/L

u


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value Units

Q

RI-MW6

5/18/2021

Trichloroethene

45.4

ug/L



RI-MW7

5/18/2021

Trichloroethene

19.5

ug/L



RI-MW8

5/18/2021

Trichloroethene

2.1

ug/L



RI-MW9

5/19/2021

Trichloroethene

6.9

ug/L



RW-341A

5/20/2021

Trichloroethene

1

ug/L



SW-01

5/20/2021

Trichloroethene

1.3

ug/L



FAG-05

5/19/2021

Vinyl

chlor

de

1

ug/L

U

FAG-11

5/19/2021

Vinyl

chlor

de

1

ug/L

U

FAG-22

5/20/2021

Vinyl

chlor

de

18.3

ug/L



FAG-31

5/20/2021

Vinyl

chlor

de

10

ug/L

u

FAG-32

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-33

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-34

5/19/2021

Vinyl

chlor

de



ug/L

u

FAG-35

5/18/2021

Vinyl

chlor

de



ug/L

u

FAG-36

5/19/2021

Vinyl

chlor

de

10

ug/L

u

FAG-43

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-46

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/19/2021

Vinyl

chlor

de

20

ug/L

u

FAG-56

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-62

5/18/2021

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/19/2021

Vinyl

chlor

de

4.2

ug/L



FAG-74

5/21/2021

Vinyl

chlor

de

18.9

ug/L



FAG-85

5/21/2021

Vinyl

chlor

de

37.2

ug/L



FAG-88

5/19/2021

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/20/2021

Vinyl

chlor

de

1

ug/L

u

FAG-AW4

5/19/2021

Vinyl

chlor

de

24.2

ug/L



RI-MW1

5/19/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW6

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW7

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW8

5/18/2021

Vinyl

chlor

de

1

ug/L

u

RI-MW9

5/19/2021

Vinyl

chlor

de

1

ug/L

u

RW-341 A

5/20/2021

Vinyl

chlor

de

1

ug/L

u

SW-01

5/20/2021

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/19/2022

Tr

chloroethene



379 ug/L



FAG-31

5/19/2022

Tr

chloroethene



726 ug/L



FAG-33

5/17/2022

Tr

chloroethene



31.7 ug/L



FAG-43

5/17/2022

Tr

chloroethene



2.3 ug/L



FAG-50

5/19/2022

Tr

chloroethene



2050 ug/L



FAG-56

5/17/2022

Tr

chloroethene



8.9 ug/L



FAG-62

5/17/2022

Tr

chloroethene



16.3 ug/L



FAG-74

5/19/2022

Tr

chloroethene



4 ug/L

J

FAG-85

5/19/2022

Tr

chloroethene



252 ug/L



FAG-88

5/19/2022

Tr

chloroethene



7 ug/L



FAG-89

5/19/2022

Tr

chloroethene



8.6 ug/L



RI-MW1

5/17/2022

Tr

chloroethene



57.3 ug/L



RI-MW2

5/17/2022

Tr

chloroethene



1 ug/L

u

RI-MW5

5/17/2022

Tr

chloroethene



15.6 ug/L



RI-MW6

5/17/2022

Tr

chloroethene



64.2 ug/L



RI-MW7

5/17/2022

Tr

chloroethene



21.7 ug/L



Qualifier


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample



Value

Units

Q

RI-MW8

5/17/2022

Tr

chloroethene

1.6

ug/L



RW-341A

5/19/2022

Tr

chloroethene

0.6

ug/L

J

SW-01

5/19/2022

Tr

chloroethene

0.92

ug/L

J

FAG-05

5/18/2022

Tr

chloroethene

18.7

ug/L



FAG-11

5/18/2022

Tr

chloroethene

2.3

ug/L



FAG-32

5/18/2022

Tr

chloroethene

49.5

ug/L



FAG-34

5/18/2022

Tr

chloroethene

582

ug/L



FAG-35

5/18/2022

Tr

chloroethene

537

ug/L



FAG-36

5/18/2022

Tr

chloroethene

455

ug/L



FAG-46

5/18/2022

Tr

chloroethene

21.1

ug/L



FAG-47

5/18/2022

Tr

chloroethene

42.7

ug/L



FAG-73

5/18/2022

Tr

chloroethene

22.8

ug/L



FAG-AW4

5/18/2022

Tr

chloroethene

1160

ug/L



RI-MW9

5/18/2022

Tr

chloroethene

2

ug/L



FAG-22

5/19/2022

Vinyl

chlor

de

30.8

ug/L



FAG-31

5/19/2022

Vinyl

chlor

de

10

ug/L

U

FAG-33

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-43

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-50

5/19/2022

Vinyl

chlor

de

25

ug/L

u

FAG-56

5/17/2022

Vinyl

chlor

de

0.25

ug/L

J

FAG-62

5/17/2022

Vinyl

chlor

de

1

ug/L

u

FAG-74

5/19/2022

Vinyl

chlor

de

5

ug/L

u

FAG-85

5/19/2022

Vinyl

chlor

de

53.8

ug/L



FAG-88

5/19/2022

Vinyl

chlor

de

1

ug/L

u

FAG-89

5/19/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW1

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW2

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW5

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW6

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MVW

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RI-MW8

5/17/2022

Vinyl

chlor

de

1

ug/L

u

RW-341 A

5/19/2022

Vinyl

chlor

de

1

ug/L

u

SW-01

5/19/2022

Vinyl

chlor

de

1

ug/L

u

FAG-05

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-11

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-32

5/18/2022

Vinyl

chlor

de

0.21

ug/L

J

FAG-34

5/18/2022

Vinyl

chlor

de

2.9

ug/L

J

FAG-35

5/18/2022

Vinyl

chlor

de

0.95

ug/L

J

FAG-36

5/18/2022

Vinyl

chlor

de

10

ug/L

u

FAG-46

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-47

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-73

5/18/2022

Vinyl

chlor

de

11

ug/L



FAG-AW4

5/18/2022

Vinyl

chlor

de

28.5

ug/L



RI-MW9

5/18/2022

Vinyl

chlor

de

1

ug/L

u

FAG-22

5/19/2022

cis-1,2-Dichloroethene

206

ug/L



FAG-31

5/19/2022

cis-1,2-Dichloroethene

210

ug/L



FAG-33

5/17/2022

cis-1,2-Dichloroethene

4.7

ug/L



FAG-43

5/17/2022

cis-1,2-Dichloroethene

0.67

ug/L

J

FAG-50

5/19/2022

cis-1,2-Dichloroethene

157

ug/L



FAG-56

5/17/2022

cis-1,2-Dichloroethene

83.2

ug/L



FAG-62

5/17/2022

cis-1,2-Dichloroethene

9.6

ug/L



FAG-74

5/19/2022

cis-1,2-Dichloroethene

0.79

ug/L

J

Qualifier


-------
MANN KENDALL INPUT

Well ID

Sample Date

Sample

Value

Units

Q

FAG-85

5/19/2022

cis-1,2-Dichloroethene

367

ug/L



FAG-88

5/19/2022

cis-1,2-Dichloroethene

1.6

ug/L



FAG-89

5/19/2022

cis-1,2-Dichloroethene

1.3

ug/L



RI-MW1

5/17/2022

cis-1,2-Dichloroethene

1.7

ug/L



RI-MW2

5/17/2022

cis-1,2-Dichloroethene

1

ug/L

U

RI-MW5

5/17/2022

cis-1,2-Dichloroethene

0.92

ug/L

J

RI-MW6

5/17/2022

cis-1,2-Dichloroethene

9.4

ug/L



RI-MW7

5/17/2022

cis-1,2-Dichloroethene

3.2

ug/L



RI-MW8

5/17/2022

cis-1,2-Dichloroethene

1

ug/L

u

RW-341A

5/19/2022

cis-1,2-Dichloroethene

1

ug/L

u

SW-01

5/19/2022

cis-1,2-Dichloroethene

1

ug/L

u

FAG-05

5/18/2022

cis-1,2-Dichloroethene

2.6

ug/L



FAG-11

5/18/2022

cis-1,2-Dichloroethene

0.66

ug/L

J

FAG-32

5/18/2022

cis-1,2-Dichloroethene

12.3

ug/L



FAG-34

5/18/2022

cis-1,2-Dichloroethene

221

ug/L



FAG-35

5/18/2022

cis-1,2-Dichloroethene

111

ug/L



FAG-36

5/18/2022

cis-1,2-Dichloroethene

168

ug/L



FAG-46

5/18/2022

cis-1,2-Dichloroethene

1.7

ug/L



FAG-47

5/18/2022

cis-1,2-Dichloroethene

3.2

ug/L



FAG-73

5/18/2022

cis-1,2-Dichloroethene

44.2

ug/L



FAG-AW4

5/18/2022

cis-1,2-Dichloroethene

268

ug/L



RI-MW9

5/18/2022

cis-1,2-Dichloroethene

0.28

ug/L

J


-------
MANN KENDALL ANALYSIS OUTPUT (Last 8 Sampling Events)

Location

Samples

Min Date

Max Date

Trichloroethene

cis-l,2-Dichloroethene

Vinyl chloride

FAG-05

8

2013-05-15 00:00:00

2022-05-18 00:00:00

Decreasing

Decreasing

All ND

FAG-11

8

2013-05-14 00:00:00

2022-05-18 00:00:00

No Trend

Stable

All ND

FAG-22

8

2013-05-16 00:00:00

2022-05-19 00:00:00

Decreasing

Decreasing

Stable

FAG-31

8

2013-05-16 00:00:00

2022-05-19 00:00:00

Stable

Stable

All ND

FAG-32

8

2013-05-16 00:00:00

2022-05-18 00:00:00

Stable

Stable


-------