FOURTH FIVE-YEAR REVIEW REPORT FOR
BEE CEE MANUFACTURING SUPERFUND SITE
DUNKLIN COUNTY, MISSOURI

Prepared by

U.S. Environmental Protection Agency
Region 7
Lenexa, Kansas

Urclaoiq

Mary P. Peterson, Director	Date

Superfund and Emergency Management Division


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Table of Contents

List of Abbreviations, Acronyms, and Definitions	iii

1.0 Introduction					4

Five-year Review Summary Form	5

2.0 Response Action Summary		5

2\1 Basis for Taking Action	5

2.2	Response Actions	!	6

2.2.1	Remedial Action Objectives	6

2.2.2	Remedy Components	6

2.3	Status of Implementation	7

2.4	Institutional Control Summary Table	7

2.5	Systems Operations/Operation & Maintenance	8

3.0 Progress Since Last Review	8

4.0 Five-year Review Process	10

4.1	Community Notification, Involvement, and Site Interviews	10

4.1.1	Community Notification, Involvement	10

4.1.2	Site Interviews	10

4.2	Data Review	10

4.3	Site Inspection	11

5.0 Technical Assessment		11

5.1	Question A: Is the remedy functioning as intended by the decision documents?	11

5.1.1	Remedial Action Performance	11

5.1.2	System Operations/O&M	11

5.1.3	Implementation of Institutional Controls and Other Measures		11

5.2	Question B: Are the exposure assumptions, toxicity data, cleanup levels, and remedial
action objectives (RAOs) used at the time of the remedy selection still valid?	12

5.2.1	Changes in Standards and To-Be-Considered Items	12

5.2.2	Changes in Toxicity and Other Contaminant Characteristics	12

5.2.3	Changes in Risk Assessment Methods	12

5.2.4	Changes in Exposure Pathways	13

5.3	Question C: Has any other information come to light that could call into question the
protectiveness of the remedy?	14

5.3.1	Natural Disaster Impacts				 14

5.3.2	Ecological Risks	14

6.0 Issues/Recommendations	15

6.1 Other Findings			15

7.0 Protectiveness Statement		16

8.0 Next Review	16

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Appendices

Appendix A - Reference List
Appendix B - Site Chronology
Appendix C - Physical Characteristics
Appendix D - Site Inspection Checklist
Appendix E - Photographs
Appendix F - Interview Record

Appendix G - Tables

Table 1-1 - Summary of Selected Site GW Sampling Data

Appendix H - Figures

Figure 1 - Location Map
Figure 2 - Well Locations

Appendix I - Site Sampling Reports Since Last Five-Year Review

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List of Abbreviations, Acronyms, and Definitions

ARARs

Applicable or Relevant and Appropriate Requirements

ATSDR

Agency for Toxic Substances and Disease Registry

CERCLA

Comprehensive Environmental Response, Compensation, and Liability Act

CFR

Code of Federal Regulations

COCs

Chemicals of Concern

COPCs

Chemicals of Concern

DGLS

Division of Geology and Land Survey (now Missouri Geological Survey)

EC

Environmental Covenant

EPA

U.S. Environmental Protection Agency

EP&R

EPA's Emergency Planning and Response Branch

ESD

Explanation of Significant Differences

FS

Feasibility Study

ft

feet

FIG

Further Investigation of Groundwater

FYR

Five-Year Review

IC

Institutional Contol

LTM

long-term monitoring

MCL

Maximum Contaminant Level

MDOH

Missouri Department of Health

MDHSS

Missouri Department of Health and Senior Services (formerly MDOH)

MDNR

Missouri Department of Natural Resources

mg/kg

milligrams per kilogram

mg/L

milligrams per liter

MNA

monitored natural attenuation

MW

Monitoring Well

NCP

National Contingency Plan

NPL

National Priorities List

O&M

operation and maintenance

OSC

On-Scene Coordinator

OSWER

Office of Solid Waste and Emergency Response

OU

operable unit

pH

A scale used to specify how acidic a water based solution is

POTW

Publicly Owned Treatment Works

PPb

parts per billion

PRGs

Preliminary Remediation Goals

PZ

piezometer

QAPP

Quality Assurance Project Plan

RAO

Remedial Action Objective

RI/FS

Remedial Investigation/Feasibility Study

ROD

Record of Decision

RSLs

Regional Screening Levels

SOW

Statement of Work

TAT

Technical Assistance Team

MDH

Missouri Department of Health

TEP

^ Toxicity Extraction Procedure

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1.0 Introduction

The purpose of a Five-Year Review, or FYR, is to evaluate the implementation and performance of a
remedy to determine if the remedy is and will continue to be protective of human health and the
environment. The methods, findings, and conclusions of these reviews are documented in five-year
review reports such as this one. In addition, five-year review reports identify issues found during the
review, if any, and document recommendations to address them.

The U.S. Environmental Protection Agency is preparing this five-year review pursuant to the
Comprehensive Environmental Response, Compensation, and Liability Act, or CERCLA, Section 121,
consistent with the National Oil and Hazardous Substances Pollution Contingency Plan, or NCP, 40
Code of Federal Regulations, or CFR, Section 300.430(f)(4)(ii)), and considering the EPA policy.

This is the fourth five-year review for the Bee Cee Manufacturing Superfund Site . The triggering action
for this statuatory review is the completion date of the previous five-year review, which was signed on
June 24, 2014. The five-year review has been prepared because hazardous substances, pollutants, or
contaminants remain at the site above levels that allow for unlimited use and unrestricted exposure, or
UU/UE.	\

The site consists of one operable unit, or OU1, that will be addressed in this FYR. OU1 addresses the
groundwater remedy, which consists of institutional controls, or ICs, and monitored natural attenuation,
or MNA.

Devin Pollock, the EPA Region 7 Remedial Project Manager, led the Bee Cee Manufacturing Superfund
Site FYR. Participants included Dan Nicoski, Hydrogeologist; Todd Phillips, Human Health Risk
Assessor; and Catherine Wooster-Brown, Ecological Risk Assessor; and Kyle Anderson, Missouri
Department of Natural Resources, or MDNR, Project Manager. The review began on June 22, 2018.

Site Background

The Bee Cee Manufacturing facility is located in the town of Maiden, Dunklin County, Missouri. The
site is located within the boundaries of Maiden Municipal Airport and Industrial Park, which was
formerly a U.S. military base.

The site covers approximately five acres and previously consisted of a metal plating facility and a
gravel-filled infiltration pit. The foundation of the manufacturing plant remains onsite. The gravel in the
pit has been removed, and the excavation was backfilled with clean soil. Appendix H, Figure 1 shows
the location of the site.

The land within one quarter-mile of the site is part of an industrial park. While most of it is vacant, some
areas are used for small industrial plants and warehouse space. The nearest home is just over one quarter
mile south of the site. Maiden's municipal water supply well No. 4 is located within one mile of the site,
but is cross-gradient from the site and is not threatened by releases at the site.

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Five-year Review Summary Form

2.0	Response Action Summary

2.1	Basis for Taking Action

The site was initially identified in July 13, 1981, when the MDNR's Southeast Regional office reported
chromium waste on the surface at the site during an investigation. Waste liquid from the process was
allowed to flow through a series of pipes directly onto the surface soil immediately north of the east end
of the facility. In a letter from the MDNR dated, July 27, 1981, Bee Cee Manufacturing was warned to
cease the discharge of untreated process water.

On July 1, 1992, the EPA approved an Action Memorandum For the Removal of Contaminated Surface
Soil at the Bee Cee site. The removal and site restoration was completed on August 20, 1992. Since the
removal was considered successful, soil was not considered as a medium of concern in the second risk
assessment. Only data collected during the 1993 Further Investigation of Groundwater, or FIG, were
used in order to identify potential health risks from exposure to groundwater.

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In summary, hexavalent chromium in shallow groundwater at the site presents an unacceptable risk for
non-carcinogenic effects. Calculations in the risk assessment show that the shallow groundwater at and
near the site presents an unacceptable carcinogenic risk due to its arsenic content. However,
concentrations of arsenic detected in groundwater from the site were lower than the concentration
detected in the background monitoring well. Therefore, remediation of arsenic is not appropriate for this
site. Zinc and trivalent chromium concentrations do not present unacceptable health risks according to
the calculations in the risk assessment. There is no health risk at the site from exposure to the soil
because the contaminated soil was removed from the site in July 1992.

2.2 Response Actions

A site chronology is presented in Appendix B.

The EPA approved an Action Memorandum For the Removal of Contaminated Surface Soil at the Bee
Cee site on July 1, 1992. The action level for the soil was set at 2,000 milligrams per kilogram, or
mg/kg, for total chromium and 180 mg/kg for hexavalent chromium. The scope of the removal included
contaminated soil and the portion of the Bee Cee Manufacturing building that contained five vats used
for metal plating processes.

On August 3, 1992, the EPA began the removal of the vats inside the building. Demolition of the
building began and was completed on August 5, 1992. Excavation and soil removal began on
August 12, 1992.

During the excavation of the soil, the EPA uncovered a 14 foot by 27 foot by 6 foot gravel pit in the
contaminated zone. The gravel appeared to have been used during Bee Cee's operation to facilitate
percolation of the wastewater discharge from the facility. The gravel was excavated and disposed of
along with the soil. A total of 356 tons of soil were removed.

2.2.1	Remedial Action Objectives

The primary chemical of concern at the site is hexavalent chromium. In consideration of this fact, the
following Remedial Action Objective, or RAO, was developed for the site and documented in the
September 1997 Record of Decision, or ROD, for the site:

• Prevent ingestion of water containing hexavalent chromium in excess of Maximum
Contaminant Levels or preliminary remediation goals, or MCLs or PRGs, respectivelyi

A 1992 memorandum from the Missouri Department of Health, or MDOH, provided PRGs for the Bee
Cee Manufacturing site. The PRG for hexavalent chromium in groundwater at this site is 18 micrograms
per liter, or |ig/L or 18 parts per billion, or ppb.

2.2.2	Remedy Components

The ROD, signed on September 30, 1997, described the selected remedy of MNA, groundwater
monitoring and ICs. ICs are in place to prevent future use of the groundwater in this part of the industrial
park and to warn potential purchasers of the contamination.

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2.3	Status of Implementation

Following the issuance of the ROD, the EPA approved the Remedial Design completed by the MDNR.
The EPA requested that the site owner, the city of Maiden, conduct the remedial work. The city
declined, citing a lack of financial means. Therefore, the site work was primarily federally funded, with
the MDNR performing the remedial work.

The state of Missouri Division of Geology and Land Survey, or DGLS, prepared the work plan and
specifications for the installation of five additional monitoring wells for the remedial action. The MDNR
and the EPA reviewed and approved these plans in 1993, prior to the award of a Cooperative
Agreement.

The five additional wells were installed in September 1-8, 1999. A Pre-Final Inspection was conducted
by theMDNR and the EPA on September 8, 1999. During the pre-final inspection, the MDNR and the
EPA determined that the construction activities of the remedial action performed by DGLS were in
accordance with the ROD, Statement of Work, or SOW, and Quality Assurance Project Plan, or QAPP,
for the site. The EPA signed a Preliminary closeout report prepared by the MDNR on
September 10, 1999, and construction of the remedy was considered complete.

In 2010, the EPA and the MDNR collected additional soil samples at the site to address one of the
recommendations from the second FYR to assess whether soil risk remained. This work was
documented in the "Addendum to the Bee Cee Manufacturing Site Second Five-Year Report," dated
May 2010. Surface and shallow subsurface soil was sampled in a grid pattern. The samples were
analyzed for hexavalent chromium, and those results were compared to human health risk criteria.
Several soil samples exceeded the human health risk level for residential use, but none of the samples
exceeded the human health risk level for industrial/commercial use. In August 2010, an Explanation of
Significant Differences, or ESD, was prepared that modified the remedy to include a land use control
preventing use of the site for residential, agricultural or child care purposes.

2.4	Institutional Control Summary Table

ICs have been in place through the use of the Missouri Registry, to prevent exposure to site
contaminants. The site was placed on the Registry on July 8, 1988. Because the source of the
contamination was deemed to have been removed, the only remaining exposure pathway is through
exposure to the contaminated groundwater. Therefore, the ICs in place ensure that no drinking water
wells are installed in the contaminated groundwater plume. In addition, the EPA worked with the city of
Maiden to place an Environmental Covenant, or EC, on the site in June 2009 to further ensure that
contaminated groundwater is not utilized for potable purposes. In August 2010, the EC was amended to
include the land use control established as the soil remedy in the ESD.

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Table 2-2; Summary of Planned and/or Implemented ICs

Media

ICs
Needed

ICs Called
for in the
Decision
Document

s

Impacted
Parcel(s)

IC
Objective

Title of IC
Instrument
Implemented and
Date (or planned)











Restrict the











installation of drinking
water wells within the











contamination plume











through the use of the

Groundwate
r

Yes

Yes

Approximate
ly four acres

Prevent access to
contaminated
groundwater

Missouri Registry.
Placed on Registry on
July 8, 1988

EC put in place by the
city of Maiden in June
2009 to further ensure
that contaminated
groundwater is not
utilized for potable
purposes











EC was modified in











August 2010, limiting

Soil

Yes

Yes

Approximate
ly 1/8 of an
acre

Limiting site use

the property to
industrial use and
prohibiting residential,

recreational,
agricultural, and child-
care uses.

2.5 Systems Operations/Operation & Maintenance

Tasks for managing the site include coordinating annual sampling of the monitoring wells, evaluating
data, assuring ICs remain in place and are complied with and consulting with the EPA regarding the site.
The Operation and Maintenance Plan, or O&M, was updated in September 2011. Appendix H, Figure 2
shows the location of the monitoring wells sampled annually. Groundwater is analyzed for hexavalent
and total chromium.

3.0 Progress Since Last Review

This section includes the protectiveness determinations, statements, and recommendations from the last
five-year review as well as the current status of those recommendations.

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Table 3-1: Protectiveness Determination/Statement from the 2014 FYR

OU 1

Protectiveness
Determination

Protectiveness Statement

1

Protective

The remedy at the Bee Cee Manufacturing Site currently
protects human health and the environment because the
groundwater plume is not migrating and institutional
controls are in place that prevent groundwater use and and
limit land use to industrial/commercial. In order to be
protective in the long-term, it is recommended that the
EPA conduct a screening level ecological risk assessment
to confirm the MDOH conclusions in the Remedial
Investigation/Feasibility Study, or RI/FS, and that the
MDNR conduct soil sampling in the vicinity of the former
manufacturing building.

Table 3

-2: Status of Recommendation from the 2014 FYR

OU
1

Issue

Recommendation

Current
Status

Current
Implementation
Status Description

Completio
n Date (if
applicable)

1

Sampling
conducted in
2010 to determine

risk from
contaminated on-

site soils was
incomplete due to
a lack of
historical
knowledge of the
former Bee Cee
Manufacturing
facility.

Complete sampling
of on-site soils and
reassess risk to
determine if soils
risk remains

Addressed
in Next
FYR

The MDNR and the
EPA will complete
sampling of on-site
soils in the area of the

former Bee Cee
Manufacturing facility
and reassess risk to
determine if
unacceptable soils risk
remains.

N/A

1

Data gaps exist in
the 1992
ecological risk
assessment

Collect surface
water, sediment and

soil samples and
conduct a screening-
level ecological risk
assessment

Addressed
in Next
FYR

The EPA will collect
surface water, sediment
and soil samples and
conduct a screening-
level ecological risk
assessment

N/A

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4.0Five-Year Review Process

4.1	Community Notification, Involvement, and Site Interviews

4.1.1	Community Notification, & Involvement

A public notice was made available by newspaper in the Delta Dunklin Democrat, September 2018,
stating that there was a FYR and inviting the public to submit any comments to the EPA. The notice
stated that results of the review and the report will be available via the EPA's internet-based repository.
The notice provided contact information for the EPA Remedial Project Manager and the following
website for additional information:

www.epa. gov/superfund/beeceemanufacturing

4.1.2	Site Interviews

During the FYR process, interviews were conducted to document any perceived problems or successes
with the remedy that has been implemented to date. Interviews were conducted with the following
people:

•	Kyle Anderson, MDNR

•	City of Maiden Airport Manager

•	Operations Manager, Weaver Popcorn (adjacent business owner to the Bee Cee Manufacturing
Superfund Site).

None of the interviewees noted any issues or concerns which may affect the protectiveness of the
remedy. Interviews are documented in Appendix D, Site Inspection Checklist and Appendix F,
Interview Record.

4.2	Data Review

Annual groundwater monitoring well sampling data was reviewed for the remedial action from sampling
events conducted since the last FYR. These events took place in March 2015, May 2016 and August
2017. Monitoring well-3, or MW-3, MW-4, MW-5, and MW-6 were sampled in each event, and the
2015 event also included wells MW-7 through MW-10. No detections of the COCs were found. MW-7
through MW-10 were abandoned in 2015 at the request of the city of Maiden to allow for development
within the Maiden Industrial Park. Given that none of these wells had detections of hexavalent
chromium above the PRG of 18 jag/1 over the past 14 years, the Hazardous Waste Program, Superfund
Section made arrangements for the wells to be abandoned. Sampling and inspection reports with photos
for these events are provided in Appendix I. Appendix H, Figure 2 shows the location of the
monitoring wells. Appendix G, Table 1-1 provides a summary of selected site sampling data since
sampling began. MW-1 is included in the table for historical reference even though it has not been
sampled since the 2nd FYR.

In summary, after reviewing the data from the wells that were sampled, since 2013, there have been no
exceedances of the hexavalent chromium PRG, and the contaminant trends in each well appear to be
stable or decreasing. One more groundwater sampling event will be completed and if the results are

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below the PRG of 18 (agL, then the site can be closed out as long as the Ecological Risk Assessment and
the results of additional soil sampling are not an issue.

4.3 Site Inspection

The inspection of the site was conducted on November 29, 2018. In attendance were Devin Pollock from
the EPA and Kyle Anderson from the MDNR. The purpose of the inspection was to assess the
protectiveness of the remedy.

The inspection team visited each of the Long Term Monitoring, or LTM, monitoring wells, which had
been last sampled in August 2017. All monitoring wells were located and found to be in good condition
and secured. A Site Inspection Checklist is contained in Appendix D, and photographs are presented in
Appendix E.

5.0	Technical Assessment

5.1	Question A: Is the remedy functioning as intended by the decision documents?

Question A Summary:

The groundwater remedy is functioning as intended by the ROD. Sampling activities related to natural
attenuation have been conducted in accordance with a site-specific O&M Plan. The results of this
sampling demonstrate that concentrations of hexavalent chromium remain below PRGs. An EC was put
in place by the city of Maiden in June 2009 to further ensure that contaminated groundwater is not
utilized for potable purposes. In August 2010, the EC was modified to limit the property use to industrial
use and prohibit residential, recreational, agricultural, and child-care uses.

5.1.1	Remedial Action Performance

Historically, hexavalent chromium and total chromium have mainly been detected in MW-3 (source area
well) and MW-5 (nearest downgradient well). Since the last FYR, total chromium has remained below
the groundwater MCL of 100 ppb in these wells and all wells sampled in the last five years. Also since
the last FYR, hexavalent chromium concentrations have been below the PRG of 18 (ig/L in these wells
and well MW-6, the fartherest downgradient well.

The generally declining contaminant levels and apparent stable groundwater plume indicate the remedy
is functioning as intended per the ROD.

5.1.2	System Operations/O&M

Operating procedures at the site are working in a mariner that will continue to maintain the effectiveness
of the remedy. No well integrity or maintenance issues were identified for the FYR period.

5.1.3	Implementation of Institutional Controls and Other Measures

ICs utilized to date have included the use of the Missouri Registry to prevent exposure to site
contaminants. An EC has also been utilized to address groundwater and land use restrictions at the site.

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5.2	Question B: Are the exposure assumptions, toxicity data, cleanup levels, and remedial
action objectives (RAOs) used at the time of the remedy selection still valid?

Question B Summary;

The exposure assumptions, toxicity data, cleanup levels, and RAOs used at the time of the remedy
selection are still valid. There have been no changes in the Applicable or Relevant and Appropriate
Requirements, or ARARs, for COCs. Changes in toxicity values do not affect risk estimates sufficiently
to bring the protectiveness of the remedy into question. Changes in risk assessment methods and
exposure pathways also do not bring the protectiveness of the remedy into question.

5.2.1	Changes in Standards and To-Be-Considered Items

New toxicity data became available in 2009 for hexavalent chromium, which led to a revision in
December 2009 to the Regional Screening Level, or RSL, for tap water. The RSL for hexavalent
chromium is currently 0.035 |_ig/L for tap water based on the November 2018 RSL tables.

In addition to changes in the EPA RSLs for hexavalent chromium in groundwater, changes were also
made to the EPA RSL for hexavalent chromium in soils. The site Removal Action utilized a hexavalent
chromium action level of 180 mg/kg. The current EPA residential RSL for hexavalent chromium is 0.30
mg/kg, while the industrial RSL is 6.3 mg/kg. After revisions of the RSLs, soil sampling at the site
identified soil contamination above RSLs, which led to the modification of the EC to prevent use of the
site for residential, agricultural or child care purposes.

There are acute and chronic hexavalent chromium ambient surface water criteria (U.S. EPA, 2009) and
updated ecological screening levels for metals (MacDonald et al., 2000) that were not used in the 1992
Final Risk Assessment or the 1997 ROD. Additional data collection of this media is recommended to
ensure sediment and surface water has not impacted ecological receptors.

5.2.2	Changes in Toxicity and Other Contaminant Characteristics

As identified and discussed above, several toxicity values have changed since the original risk
assessment was conducted and have resulted in substantially lower screening levels for soil and water.
As a result of these changes, the Second and Third FYRs recommended soil sampling at the site to
determine if soil risks are acceptable. Based upon those sampling results, the MDNR and the EPA
determined that a change to the ROD was necessary to implement an additional remedy for soil.
Additional sampling is still needed to characterize soils that exceed the soil PRG on the site (see Section

5.3	below).

We are not aware of any other changes to contaminant characteristic that could impact the
protectiveness of the remedy.

5.2.3	Changes in Risk Assessment Methods

The EPA has significantly revised its dermal risk assessment guidance since the completion of the
original risk assessment (U.S. EPA, 2004). A different approach is also used when estimating the health
risks from inhalation of volatile organic compounds during household use of contaminated groundwater
(i.e., bathing, showering, cooking, etc.) (U.S. EPA, 2009). In addition, several exposure assessment

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input parameters in the original risk assessment are different than values currently used, and the EPA
has also developed and implemented risk assessment guidance which evaluates the vapor intrusion
pathway.

As part of the Second FYR, a risk assessment report was completed that updated toxicity values and risk
assessment methods, where applicable. Based on the soil sampling results collected in March 2010, the
MDNR and the EPA determined that a change to the ROD was necessary to implement an additional
remedy for soil. An ESD for the Bee Cee Manufacturing Site was completed in July 2010 (U.S. EPA,
2010) to implement a significant change to the remedy for soil at the site. The proposed remedy change
for soil involved placing an IC in the form of an addendum to the existing EC for groundwater at the
site. This IC limits use of the site to industrial purposes and explicitly prohibits use of the site for
residential, agricultural or child care purposes. Sampling conducted in 2010 to determine risk from
contaminated on-site soils was incomplete due to a lack of historical knowledge of the former Bee Cee
Manufacturing facility foundation slab. Additional sampling of on-site soils near the former Bee Cee
slab is needed to reassess risk to determine if soils risk remains.

The 1992 Final Risk Assessment for the site concluded that because the site is located in an industrial
area, and the contamination is relatively localized, it did not appear to pose a threat to the environment.
It noted that there was chromium above Apparent Effects Threshold values in site soils. However, it also
noted that there was no evidence of exposure to sensitive species or native communities. This
assessment did not consider groundwater as a risk to the environment and did not evaluate surface water
as an ecological pathway. In 1992, the EPA published the Framework for Ecological Risk Assessment
as the first statement of principles for ecological risks. In 1997, the agency published the Guidelines for
Ecological Risk Assessment, which supersedes the 1992 guidance. However, the ecological risk
assessment performed for this site as part of the Final Risk Assessment did not follow any of the EPA
guidance. Therefore, Region 7 ecological risk assessors recommend that a screening level ecological
risk assessment be performed with updated surface water, sediment and soil samples (including both
total and hexavalent chromium) be collected at the Bee Cee Manufacturing Site.

Since the remedial action for the site only addressed groundwater, only a groundwater remedial action
objective was developed. This RAO for the site remains appropriate for groundwater, as site conditions
have not changed since implementation of the remedy.

5.2.4 Changes in Exposure Pathways

Land use has not changed at the site since the last FYR, and the EPA is not aware of any potential future
land use changes. The exposure assumptions used to determine risk included both current and potential
future exposures under a residential scenario. These assumptions were considered to be conservative and
reasonable in evaluating groundwater risk given the potential that the area could be converted to
residential use in the future.

There are no newly-identified contaminants or contaminant sources that would lead to a potential/actual
pathway not previously addressed by the remedy.

There are no unanticipated toxic byproducts or daughter products of the remedy which were not
evaluated at the time of remedy selection or addressed by the ROD.

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5.3 Question C: Has any other information come to light that could call into question the
protectiveness of the remedy?

On October 1, 2013, in response to an annual Registry Inspection Report submitted by the state Project
Manager to the Missouri Department of Health and Senior Services, or MDHSS, it was brought to the
attention of the MDNR that the physical location of the former Bee Cee Manufacturing Company
facility was not the building slab adjacent to the most contaminated site wells MW-3 and MW-5 as
believed, but rather the easternmost portion of the currently operating facility building directly to the
west. This assertion was verified using a survey map of the site contained in the FIG report and
comparing it to a present-day Google Earth map of the site. Based on this new piece of information, the
sampling grid for the site soil sampling conducted in 2010 was actually shifted approximately 125 feet
east of the believed location of the Bee Cee building slab. It is recommended that additional soil
sampling be conducted to assure that areas of the site to the west of the 2010 grid contain hexavalent
chromium levels below the human health risk level for industrial/commercial use of the site.

5.3.1	Natural Disaster Impacts

No natural disasters have occurred that could call the protectiveness of the remedy into question.

5.3.2	Ecological Risks

A screening level ecological risk assessment will be performed with updated surface water, sediment
and soil samples.

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6.0 Issues/Recommendations

Issucs/Rcconimcndntions

OU(s) without Issues/Recommendations Identified in the Five-Year Review:

None

Issues and Recommendations Identified in the Five-Year Review:

OU(s): 1

Issue Category: Monitoring

Issue: Soil sampling conducted in 2010 to determine risk from
contaminated on-site soils was incomplete due to a lack of historical
knowledge of the former Bee Cee Manufacturing facility.

Recommendation: Complete sampling of on-site soils in the area of the
former Bee Cee Manufacturing facility and reassess risk to determine if
unacceptable soil risk remains. Based on results, determine whether a
modification to the existing environmental covenant and/or ROD is
required.

Affect Current
Protectiveness

Affect Future
Protectiveness

Party
Responsible

Oversight
Party

Milestone Date

No

Yes

EPA/State

EPA

6/25/2021

Issues and Recommendations Identified in the Five-Year Review:

OU(s): 1

Issue Category: Monitoring

Issue: Data gaps exist in the 1992 ecological risk assessment

Recommendation: Collect surface water, sediment and soil samples and
conduct a screening-level ecological risk assessment

Affect Current
Protectiveness

Affect Future
Protectiveness

Party
Responsible

Oversight
Party

Milestone Date

No

Yes

EPA/State

EPA

6/25/2021

6.1 Other Findings

None

15


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BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

7.0 Protectiveness Statement

Operable Unit:
OU1

Protectiveness Determination:
Short-term Protective

Planned Addendum
Completion Date:

N/A

Protectiveness Statement: The remedy at the Bee Cee Manufacturing Site currently protects
human health and the environment because the groundwater contamination plume is not
migrating and institutional controls are in place that prevent groundwater use and limit land
use to industrial/commercial. In order to be protective in the long-term, it is recommended that
the EPA conduct a screening level ecological risk assessment to confirm the MDHSS'
conclusions in the RI/FS, and additional soil sampling be conducted in the vicinity of the
former manufacturing building.

8.0 Next Review

The next five-year review report for the Bee Cee Manufacturing Site is required five years from the
completion date of this review.

16


-------
APPENDIX A
REFERENCE LIST

j


-------
Agency for Toxic Substances and Disease Registry, 1995. Health Consultation, Bee Cee Manufacturing
Company, Maiden, Dunklin, County, Missouri.

MDH, 1992. Final Risk Assessment, Bee Cee Manufacturing Superfund Site, Dunklin County, MO.

Bureau of Environmental Epidemiology, Missouri Department of Health, Jefferson City, MO.

MDNR, 1993. Risk Assessment for Exposure to Contaminated Groundwater, Bee Cee Manufacturing
Site, Maiden, MO.

MDNR, 2009. Second Five Year Review Report for the Bee Cee Manufacturing Company Site. Maiden,
Dunklin County, Missouri.

I

MDNR, 2010. Addendum to the Bee Cee Manufacturing Site, Second Five-Year Review Report.

MDNR, 2010. Explanation of Significant Differences for the. Bee Cee Manufacturing Company
Superfund Site. Maiden, Dunklin County, Missouri. EPA ID No. MOD980860522.

MDNR, 2014. Second Five Year Review Report for the Bee Cee Manufacturing Company Site. Maiden,
Dunklin County, Missouri.

MDNR, 2015. Abbreviated Sampling Report, Bee Cee Manufacturing Site, Order Number 15031808,
Maiden, Dunklin County, MO.

MDNR, 2016. Abbreviated Sampling Report, Bee Cee Manufacturing Site, Order Number 160512009,
Maiden, Dunklin County, MO.

MDNR, 2017. Abbreviated Sampling Report, Bee Cee Manufacturing Site, Order Number 1708090005,
Maiden, Dunklin County, MO.

Sverdrup Environmental, 1993. Further Investigation of Groundwater Report at the Bee Cee
Manufacturing Superfund Site, Maiden, Missouri.

Sverdrup Environmental, 1994. Feasibility Study Report for the Bee Cee Manufacturing Superfund Site,
Maiden, Missouri.

U.S. EPA, 1997. Record of Decision, Bee Cee Manufacturing Superfund Site, Maiden, Missouri
September 1997.

U.S. EPA, 2001. Comprehensive Five-Year Review Guidance, Office of Emergency and Remedial
Response.

U.S. EPA, 2003. Region 5 RCRA Ecological Screening Levels.

http://epa.gov/region5/waste/carslpdfs/ecological-screening-levels-200308.pdf

U.S. EPA, 2004. Risk Assessment Guidance for Superfund Volume 1: Human Health Evaluation Manual
Remedial Response, Washington D.C. EPN540/R/99/005.

U.S. EPA, 2008. Ecological Soil Screening Levels for Chromium Interim Final. OSWER Directive
9285.7- 66. http://wvw.epa.gov/ecotox/ecossl/pdf/eco-ssl chromium.pdf


-------
U.S. EPA, 2009. Risk Assessment Guidance for Superfund: Volume I- Human Health Evaluation

Manual (Part F, Supplemental Guidance for Inhalation Risk Assessment). Office of Superfund
Remediation and Technology Innovation. USEPA-540-R-070-002.

U.S. EPA, 2009. Nationally Recommended Water Quality Criteria.

http://water.epa.gov/scitech/swguidance/standardslcriteria/current/

U.S. EPA, 2012. Assessing Protectiveness at Sites for Vapor Intrusion, Supplement to the
"Comprehensive Five-Year Review Guidance." OSWER Directive 9200.2-84.

U.S. EPA, 2018. Regional Screening Levels (RSL) Summary Table (TR=lE-06, HQ=1). November.
http://www.epa.gov/risk/regional-screening-levels-rsls


-------
APPENDIX B
SITE CHRONOLOGY


-------
BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

Site Chronology

Date

Event

07/1982

Site Discovery

6/10/1986

Final Listing on National Priorities List or NPL

7/08/1988

Bee Cee Manufacturing Site placed on MDNR's Registry

2/12/1992

Preliminary Removal Assessment

8/20/1992

Removal of Contaminated Surface Soil

12/21/1992

Human Health Risk Assessment completed

4/12-4/17/1993

Further Investigation of Groundwater was conducted

9/30/1997

Feasibility Study completed

9/30/1997

Record of Decision signed

3/5/1999

Remedial Design approved

8/31/1999

Cooperative Agreement signed

9/01-9/9/1999

Remedial Action completed

9/8/1999

Final Inspection conducted by the MDNR and the EPA

9/10/1999

Preliminary Close-out Report signed by the EPA

10/12/1999

First round of groundwater samples collected from all 10 wells

11/7/2000

Groundwater sampling conducted

11/15-11/16/2001

Groundwater sampling conducted

8/20-8/21/2003

Groundwater sampling conducted

9/30/2004

First FYR completed

4/25/2005

Groundwater sampling conducted

3/01/2006

Groundwater sampling conducted

7/02/2007

Groundwater sampling conducted

4/22/2008

Groundwater sampling conducted

4/6/2009

Groundwater sampling conducted

6/22/2009

Environmental Covenant placed

7/30/2009

Second FYR completed

3/23/2010

Groundwater sampling conducted

3/1/2011

Groundwater sampling conducted

3/7/2012

Groundwater sampling conducted

3/11/2013

Groundwater sampling conducted

3/10/2014

Groundwater sampling conducted

6/07/2010

Addendum to Second FYR

8/13/2010

Environmental Covenant amended

8/13/2010

Explanation of Significant Differences for soil remedy

9/30/2010

O&M Phase begins, State takes over Site

6/24/2015

Third FYR completed

3/17/2015

Groundwater sampling conducted

5/11/2016

Groundwater sampling conducted

8/1/2017

Groundwater sampling conducted


-------
APPENDIX C
PHYSICAL CHARACTERISTICS/
HISTORY OF CONTAMINATION


-------
BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

Physical Characteristics

The Bee Cee Manufacturing Site is located in the town of Maiden, Dunklin County, Missouri
(Figure 1). The site is located in the southeast Mississippi lowlands subdivision of the Gulf
Coastal Plain Province. Most of Dunklin County is a nearly level part of the current Mississippi
River Alluvial Plain. The town of Maiden consists of primarily residential and commercial/
industrial buildings with an approximate population of 4,277 (2010 Census data).

The contaminated soil, considered to be the source of the groundwater contamination, was
addressed in a 1992 removal.

The remedial action addresses the groundwater plume. The remedial investigation estimated the
groundwater plume to be 400 feet or ft. long by 400 ft. wide, with a maximum depth of 25 ft.
The plume was estimated to have traveled 438 ft. from the point of release. From the last five
rounds of annual sampling, the plume does not appear to have migrated past MW-6.

Land and Resource Use

\

The land within a quarter mile of the site is part of an industrial park. While most of it is vacant,
some areas are used for small industrial plants and warehouse space. The nearest home is just
over a quarter of a mile south of the site. Maiden's municipal water supply well No. 4 is located
within one mile of the site. Water from the site is not likely to impact this well since it is cross-
gradient from the site and is completed in an artesian aquifer approximately 800 feet below
ground surface.

History of Contamination

Bee Cee Manufacturing occupied the site from 1964 until early 1983 and produced aluminum
moldings for storm windows and doors. The window and door moldings were cleaned and
etched in preparation for application of a finishing coat of paint. A series of five open vats were
used to hold cleaning, etching and rinsing fluids that included chromic acid. The aluminum
moldings were dipped from one tank to another during the manufacturing process. The chemicals
in the various vats were identified under the trade names Alodine 4 780 and Ridoline 72.

Waste liquid from the process was allowed to flow through a series of pipes directly onto the
surface soil immediately north of the east end of the facility. Personnel from the Water Pollution
Control Unit of the MDNR's Southeast Regional Office reported chromium wastes on the surface
at the site during an investigation conducted July 13, 1981. In a letter from MDNR dated July 27,
1981, Bee Cee Manufacturing was warned to cease the discharge of untreated process water.

Bee Cee Manufacturing declared bankruptcy in 1983, and the site was taken over by Missouri
Aluminum Products Company. This company cut and assembled storm doors but did not include
chemical cleaning of aluminum in the process as did Bee Cee Manufacturing.

Falcon next occupied the site. Falcon only assembled aluminum door and window frames and
did not generate any hazardous wastes from their process. According to a bill of sale dated April
15, 1985, Falcon purchased certain assets from Missouri Aluminum Products Company. Falcon


-------
BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

did not purchase the vats. However, Falcon arranged to have the material that remained in the
tanks removed.

The contents of the five vats were sampled and analyzed by William A. Green and Associates of
Maiden, Missouri for pH, hexavalent chromium, total chromium, aluminum, nickel and lead to
determine compliance with discharge requirements to the local Publicly Owned Treatment
Works. According to a Falcon letter to MDNR dated December 20, 1985, the Maiden Board of
Public Works authorized discharging the contents of vats one, two, four and five, to the Public
Owned Treatment Works or POTW provided that the pH was adjusted to between 6 and 9 prior
to discharge.

The sludge in the four vats was removed. However, the vats were left in place. A
recommendation was made for the chromic acid solution in vat three, to be removed by a
hazardous waste disposal company. Falcon Door and Window requested authorization from
MDNR for removal of the waste material contained in the tank. According to a letter written by
WAGA to Falcon on March 20, 1986, Mid-America Transport Services, a licensed hazardous
waste transporter, removed and transported the chromic acid solution. According to the letter, the
tank walls were rinsed; however, a small amount of aluminum solution and less than one gallon
of rinse water remained on the tank bottom. The chromic acid solution was transported to Chem
Clear, Inc. in Chicago, Illinois, on March 20, 1986, as stated in a copy of the Uniform Hazardous
Waste Manifest.

During the time that the building was occupied by the various tenants, several sampling events
and evaluations of the groundwater (sampling nearby wells, not the site-specific wells installed
later), soil and "sludge" at the site were conducted. The MDNR Division of Environmental
Quality Laboratory Services Program collected samples from the following four sources: (1)
selected city wells, (2) liquid discharge from a pipe extending out of and onto the north side of
the building (from the area of the building that contained the chemical cleaning process vats), (3)
discolored soil north of the building, and (4) the five process vats. The Missouri Department of
Health also collected water samples at several nearby residential, irrigation and public water
supply wells from 1984 to 1991. Southeast Missouri State University conducted a test-pit survey
at the site in 1986.

A report prepared by MDNR on June 27, 1984, indicated that the sludge north of the building
was sampled and analyzed according to the Toxicity Extraction Procedure or TEP. The reported
chromium concentration was 2.5 milligrams per liter or mg/L. According to the report, the
regulatory TEP Limit for chromium was 5.0 mg/L. The discharge liquid from the building was
also analyzed and found to have a chromium concentration of 0.62 mg/L. Several wells located
near the site were also sampled; however, only three metals (aluminum, barium and lead) were
detected at concentrations, above their associated detection limit. Aluminum and chromium were
each detected at concentrations above detection levels at a residential well with concentrations at
1.0 and 0.032 mg/L, respectively. Samples taken from the two wells at the nearby golf course
had concentrations of barium above the detection level.


-------
BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

Seven City wells were monitored from March 1984 to September 1991 by MDOH. The
groundwater analytical data from samples taken from those wells indicated no concentrations of
chromium above the detection limit of 0'"005 mg/L.

The EPA's Emergency Planning and Response Branch or EP&R and Ecology and Environment's
Technical Assistance Team or TAT conducted a preliminary removal assessment on February
12, 1992. The Bee Cee Manufacturing building interior and exterior were inspected for future
removal procedures by representatives of EP&R, TAT, MDNR, a removal contractor and
Sverdrup Environmental Incorporated. The potential source area for chromium contamination
was the soil north of the east end of the metal treating facility where chemical-process liquids
were disposed. The soils in this area were sampled in April 1992 and were evaluated by the
collection of 40 soil samples. The EPA approved an Action Memorandum for the Removal of
Contaminated Surface Soil at the Bee Cee Manufacturing Site on July 1, 1992. The action level
for the soil was set at 2000 mg/kg for total chromium and 180 mg/kg for Hexavalent Chromium.
The scope of the removal included contaminated soil and the portion of the Bee cee
Manufacturing building that contained five vats used for metal plating processes.

On July 27, 1992, the EPA's On-Scene Coordinator and the site remediation contractor, Riedel
Environmental Services mobilized to the site. Removal of the contaminated soil, process tanks
and portions of the building was completed on August 20, 1992.

Beginning in late 1991, a RI of the site was condl :lcted. Parts of this investigation occurred
concurrently with the Removal Investigation and Removal Action. Later, a FIG was conducted.
Both investigations were conducted to better define the contamination of the site. TAT provided
assistance for the RI. Field activities for the RI were conducted from April 13 through 24, and
June 8 through 12, 1992. Field activities for the FIG were conducted from April 12 through April
17, 1993. Samples of groundwater, soil and air from the site were collected and analyzed. In
addition, sediment samples from the ditch north of the site were collected. The potential source
area for chromium contamination was found to be the soil north of the east end of the facility
where chemical-process liquids were disposed. A visibly stained surface area next to the building
that contained the process vats was considered the contamination zone.

Based on conclusions and recommendations contained in the RI, FIG and Risk Assessment, a
Feasibility Study or FS was ordered. The writing of the FS was completed in October 1994.
Information from the FS was used to select the most appropriate remedy for the remediation of
the contaminated groundwater at the Bee Cee Manufacturing Site. This selection was detailed ii)
the Proposed Plan, which was completed and released for public comment in April 1997. The
Record of Decision was signed on September 29, 1997.


-------
APPENDIX D
SITE INSPECTION CHECKLIST

i


-------
1. SHT. (NPUKMANON

Site ,awsi p.ae. C \»c / ¦<. -r « < ~i" '<> >«, »¦«<* >•~ .nvp>v-ii.a A^cue^j^v- >1 -:~ <>.•£

Location and Region.	 _ 		 __ CP4 ID: MOQ 9 g&g^

Agenc- ffic ot rf.rjjfun. UadiPj; trv five-year Weather/tenmeraUirc:

^ A V	Zfa^L ¦ H 2- °

Remedy Ipfiudrr tl k\ k j<< i\u \pp!y)

neat

~	Access controls

~	Groundwater pump and trcatm

v,u?\-kc «>,<,<.> < oihVt f iM.1 t>

~	Other

^Monitored natural attenuation
O li r(^ik1» ater containment
O V tv.ical barrier walls

ment

Attachments: O Inspection k- w i .<*(« a.u/u d

iltached

1. O&M site manager _ {< ^

II. IS IER\ >1* \\S iClveK «i( t^j:* vply)

! **• R{\ 4*>_-s» f H .&:*>) v-KK, 41 haV-

Name	rid,'

S-/fc-W

Date

Interviewed r D a! office u by phone Phone no, 5 """3 • " f< i i^lo
Probieins, suggestions: fi Report attack v1 _>•„*	%

2. O&M staff

phone Phone no,
ned

Tide

Date

D-l


-------
regulatory aurboritie* and response agencies (i.e., State and Tribal offices, emergency response
office, police department, office of public health or environmental health, zoning office, recorder of
deeds, or oiler city mud county offices, etc.) Fill in all that apply.

Agency

Contact

Avr/'.cf- *:.J	f+v-k

mmrnim A.	»

Name	Tak	Date PI

Problems; suggestions;&Reporr attached

r-- •* - ijl-M

Phone no.

.71

iVHlerw

Title

Date Phone no.

Agency

Contact 			

Name

Problems; suggestions; ~ Report attached

Title

Date fiwe 
-------
ill. OVSill KUdMKMSA Ki t OKDS VKHil fH> u'iku k cKi *

1,	O&M Drcumtiiiv

1, '(\tM ,\ m»\sv 1 ^,>>1 .in. > * 'r!	> da's' vi	.V •

'.1A*-build iu'iij. 1 luvuhU wsl.itMe	i > ip t>\ (lit.'	!'.N"'\ \

I >U«*tcranct VysA ^ • UvadiU a\4sl>t>k*	i i dac».	V. JN.V- .

Uencwits M i) V fts *\K ,f\t-/"? |'>jkl^..4:KAT_ -	>~v«V*s 3S-«H(«*¦? *••**t*-^-

/'!i.V{^ _><¦ hj, j H tJ-.. t~L>'#	t_

2,	Site-Spcrifle Health and Safer* !'U« C R-Mdilv .->>«! »bu>	' l*j> K-v*uic	f C'N A\
„k i i€\ ' 1j> umr^Hc it-poPi*'p'4.!i i' Rcad.h & ¦j-.'jbie	. Tp to \ijte	\ ; K 3. •"
Reru»*k« }t4s£ .! > pjVt. ©£ jf^.v /I ?jm L-

Permits H«;d Hcniu Agrmttmss

i Ad ihsc.wtgi i* mm	iK-v.eh iXdivMo

1 tilUC!« dlSCh.Mgv	''t\ll'V IXlnl'l!

t > Waste disposul IPO J A I	Rfjtuti} ,n.ul.'Mt u Up to ,

iTOu„ 		1 Ravxs available

Rerosrks

5, Gas Generation Records	~ Readily available O Up to dale

Remarks

^eftiernfiit	Record*	~"1 Re»JU\ avii'.aMt	H)p !¦> date (j. N «\

T ,,n»ui,»bte	' 5 >p to <1 iu>	V)

RiuUaik^

Diwlwrgt C cnipl/anco Records	., •

! 1 Ait	OReadily available ~ Up to date ' ""'N' \ xt

11U sic.- (effluent)	O Readily available ~ Up t ^ 0 Xx^ N' \ '

ki*tii4rks

10, Oat!> 4e«v« Staniri	" i^Mvhis .WA-bc*!? 1 U; >v j.tit	'^'-1*,^

Rcna-V N~s S	!> f!f 4 *? * .		, S

rWT rC	\l Akffo^% .W

v *i^w	_ * ¦-* il!i? h.^__ky 0>"V,y ct^*	.	______

D-3


-------
IV. O&M COSTS

<»&\t O'^-muvtion

x> •».. >n : •	r r-i -a n ft. v,k, >

i t^Pl' ,r->	f i , n!> k }>•>> »-s\»

i 1 • i A (,i< i ,«i.  n" >t * >> m V tv uil facility

O Other

Nt-Jto";:?;11 ^,,A,„ ^ji^. ¦¦

O Funding mechanism'agr cement in place

ku< >u, M v «s; ^tan- -# 5> oc-r* Iwf >' H^iiMown attached

Total annual cost by year for review period if available

From



To





~ Breakdown attached



Date



Dale

Total cost



From



To





O Breakdown attached



Date



Date

Total cost



From



To





0 Breakdown attached



Date





Total cost



From



To





~ Breakdown attached



Date



Date

Total cost



From



To





O Breakdown attached



Date



Dale

Total cost



3. Unanticipated or ll««s»al!y I*M OA U i «ts Dnring Review Period

Describe costs and reasons:

¥, \( Ci.Ss AN)* i , \ N .

D-4


-------
c.

Institutional Controls (ICs)



1.

< -vi ?' "*,<•. v.plemented Irr. 1 j
W ,i> td'ti. »<•. ,u\;t!v H <, (H f >»n> > su i\ ttiforced O Yes ONr {





T\po ,»rnhn is>> u>; '--f iilf-- Jrivel^ »>'£ j> ,

1 u\j,.cn."5 »v «i ?>T 'vfs/^.t s -1-" i
'l-.wpctteiHe ja«h^

M<> >u- ftsir

*\v



'JfiYcs DNo

ReriHN.-i v • r , ¦ . •-.. lead agency Vs V

1
1



Specific requirements in deed or decision documents have been met ,\t>* [ i M

Violations have been reported

Other problems or suggestions; O Report attached

W\' A

% N a.



















2.

Remarks

ON A













D.

General



1.

Viidaisni/treipissliif O Location shown on site map )L K\> veWi, evident
Remarks









JL.

1^^ nrf usc chior s < f i\

Remarks









3.

Land «\e changes off site ON/A









VI. GENERAL, SITE CONDITIONS

A. Roads "^Applicable ON/A

1.

ioi.fs d.t naged M , O Location shown fit? ,n.v < To

*t'it" f •-



D-5


-------
1. Other Site Conditions

Remarks Nl A

A. Landfill Siirfnc#

1.

VII.

s o

Vcv< .n-K'C, %

is)

! alio > -'.H'1 on site map O Settlement not evident
Depth	_

ttion shown on site map O Cracking not evident
Widths 		 Depths

3. Erosion

Area! extent
Remarks

4, Holes
Ariv' i
Re

O Location shown on site map O Holes not evident
Depth	____	,	

5, \	t ' "	[i

11	lu-s t n.k », . „,Ki »\ ji jbs oi

rty established O No signs of stress

er (armored rock, concrete, etc.) O N/A

?, Bulges	>1 .i >n shown on site map I H^lges not evident

Area! extent 			_____

Remarks

D-6


-------
8.

Wet Areas/Winter Damage
~ Wet areas
'J Ponding
O Seeps
O Soft jubgrade
Remarks

~	Wet areas/wtler damage not evident

~	l ocation shown on site map Areal extent

n f on map a

x vV 1 map \vi!
i. i \ i>. • h,. < a on L¦* > \t< r sp' ihe „ 'ope
r \uri'kv .)»u! • ci > ;•< .i:\i ^«iu\ ihi* ru .< t,i

1.

Flows Bypass Bench
Remarks

O Location shown on site map O N./A or okay







2,

Bench Breached

Remarks

1 i >>. a, >i s •>:.<"«» on site map \ at okay







3.

ttench Ovi-t topped

Rt-n> r, L»

~ vi" f, : • vn on site map ON/A or okay







C.

KltfiwiiUuiiOrij ' >n ,¦« n

>Cn/a

4 1 * i ^ ^ uu H ^ ^ v,l< ^

L

Settlement

Areal extent

'o.i ^ho%vti, ,n site map O No evidence of settlement



Eema;l,f









2.

o! •V.<. Warttjn OLocr

Uv'u sKo'a r u,i map D No evidence of degradation













3.

Erosion
Areal extent

lion siunt u itn site map OKj, : „ cf erosion



Rcv»,i,ks



D-7


-------
4.

O Location shown on site map ~ Mo evidence of undercutting
Depth

5.

Obstructions pav CN, ,)*, ,> tactions
H1 ocation show-.. .i«. ¦ t- Area! extent

R-'msre

6,

\ i-tsxi» X % k,tk Type 	

wth

»l obstruct flow

Area! extern

D. Cover Pmrlr iimns . KM/A

1.

^ j* ^ A.cHv'*^ Passive

J »\oih - U ~ ¦ 0 I H5v\t.v,sr|» n Routinely sampled ~ Good condition

O Needs Maintenance

Remarks

2.

Gas Mouit.-vn; Firbts

~ Properly s stiaeiy sampled O Good condition
O Evidence« O Needs Maintenance O N/A
Remarks

3.

, v,-., c. ,\i,vl ra;»cu\io;> > .".h.iph ly sampled ~ Good condition
'1 " u'e<> ^ St\ . iNeeds Maintenance DN/A

4.

: kw \\ k n.T, uu.^4 ~ Routinely sampled ~ Good condition
I. .'vat.vt" < * "t.. ~ Needs Maintenance ON/A

5,

Settlement Monuments > . .rated ~ Routinely surveyed DN/A

Kfuudi,

D-l


-------
E.

• >i!ection and Treatment

¦•vp1 uihu' \

1.

iIay 11 »atment Facilities

arms* O Thermal destruction O Collection for reuse
condition^ Needs Maintenance







2.

Gas Coll.\ i; n W«|w M*)»iMk's asui
OGood ci«,ti!i,,s»si \'. eds Maintenance
Remarks







3.

Gas Monitoring Facilities (e.ggas raoru adjacent homes or buildings)

~ Good condition!) Needs Maintenance

Remarks









it Drainage Layer





Outlet Pipes Inspected

Remarks

O Functioning DM/A







2,

Outlet Rock Inspected

Remarks

O Functioning O N/A







C.

Dentition Sedimentation Ponds

0 App i .,1 Ic H N \

1.

SiltalioB Areal extent

u'r, ON/A



O Sillation not evident
Remarks









2.

Erosion Area' e\t^>

Deuth



O Erosion not evident
Remarks









3.

Outlet Works C
Remarks

~ N/A

1





4,

Dam E

Remarks

ON/A

D-9


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11. Retaining Walls

~ Applicable

1

1.

Deformations

O Location she

rmation not evident



Horizontal displacement > > .-,i ,<«' u->>s'! v>





Rotational displacement





Remarks













2.

Degradation

O Location shown on site map

O Degradation not evident



Remarks













I.

IVnnuncT Ditches/Off -5>m Pi5\ ,'nv<,e D APt>he -ole

C- \

I.

Siltation

on site map O Siltation not evident



Areal extent

Jflnt.il





Remarks











2,



uwth i ! » ,ao,s - 'h te map

. N





hs not impi >k> uCm\







Type		_	











3,

Erosion

O Lei, a' ..i» »Ntuon site map

O Erosion not evident



Arcal extent







Kx'UIlk,'













4.

Discharge Structure ~ Functioning ON/A





Remarks















VIII. VERWU Ka; u,m

> iot Biwiiiorei





Frequency	

i	.i tvidence of breaching



Head different

;





		 —













D-10


-------
			 IV GmW\m\.\Vai'Si:m-AiT u XTHRKIMUMIs ^Applicable ON A

A. GroiiaJ'vatrr I xrracn.jii Wells, I'timps. and Pipelines	i," AjpplicabL *5$ A/A

1. Pump*;, VWJIhuil Plumbing, nod I Ifrtriral

uooj co-KX-t.on, ' All enquire,! «;i!s I'lopf-K operating. ! Needs Maintenance O N/A.
Remark

2, (Atrai iion System Pipeline"., V hIh*?., VnWe Bmts, jet) Otltw Sppurhntatim

i i l»« vd conciitioiiO Needs -<> *,(ct
Remarks

3. Sparr fa< h and L'qmpraent

; RvJ,"*!^ a\,.liable ~ Good conditionD Requires upgrade ~ Needs to be provided

nemans

B. H'iSacr VMt*t Otllettf.w SUuetiii

1,	Ntmtrus, t'umpo »ihI I'h

i Oov,1 i »!.aiin>-\ '	fvtsSimc-ii^i'

liwnaiKS

2, Surface Water Collection System Pipeline v \ atves, Valve Boxes, and Other Appurtenances

O Good conditionD Needs Maintenance

Remarks

3. .Span" INr.'s jimI Equipment

i: Rciidilv iiva'iable ~ Good conditionD Requires upgrade ~ Needs to be provided
Rerv.'k:.

D-t:


-------
C. Trt

rmcnt System O Applicable ^NA



1,

\«etttiiMM 1 r.iin (Check components that apply)

vj Nirtat? rero.iv tl OOil/water separation ~ Bioremediation

> J A»i s<» ipjt.ui' O Carbon adsorbers

J Additi'«. u j , chciaiR.r'3®-i; ;}.v,i'ent)

'Joj I tv i, muu J >'ce i - M i^.u'ranc.
f. Sm.'uiiaa pior;rh n!«i< v, cow i^no'.orial
! S4iv.j.i 111tg,'ntrtin;enaf,c- hy ckapUve.1 u.:i' up 'o Jale

Qu0(1 Ci'S!«lu'.«),-K I NVod< Ma Uk'SUta C
Remnrks



3.

' K A ('1 !' °!<»idary containment ONeeds Maintenance



4

Discharge Structuie and Appwmiisiivs

t;N;A 1 "cridmo*r * Nrrai S^a^temncr

Remarks



5,

!'r ainitnf RMiullngis)

l5?s' ^ ' Ck.v;. wlnMiiusn ; vf and doot \\ay») U Xiiecis tupatr
Oiuntcals and -vu prwn p^x'.h su v.*

Remarks



6.

Monitoring B elH , pump urw iwmcu;

* 1 Prc^erh «YY>HedsK-krd ! u*\ < ly sampled O Gooc' .wiuilion
_i ,\lk uq'.rad vm It* hv.itcd Li NeetU Mdiute,ku>ce [ 1 S 'A

Remarks



D. Monitortitg Data

1,

?tl» • out:t>eH sutwi.'iea on t>riu ~ Is of acceptable quality



2.

Moanonuk dam Mip^esn

3 G;tvrivJ\vj»u t'iunw »s fftat.ieK cvn'o'Kv ^ .. e>>it nninant concentrations are declining



D-12


-------
I). Monitored Natural Attenuation

1, IVtouitpnm; \\elb u .tniu! altenuatso.; rwrcdO

Y* P»s Good condition

% All itVjU jit.: \\HI> letauv v \et(U Mi,-niinaisce	ON/A

Remarks

X OltlifRlFMHW.h 	

¦ appl ¦"! iS'.t' s.io w!sr» it,-- (\Hatnnc, attach aa s»Kjxvtu>tt M'^eet describing
'Bclccnaif i>h «\ins taod-u liKwa'o? witn th>* *emedy. An exAmpk would be soil

_	\i	'.WSKKVUIOVS

A, Iinpk-ini'itatH Ft-xteJj

Ost-. c\tv uvjt,, 4 no	p >» 'autiu , ^ is htuK ' !L»*	h « •: v,i< ' v ; •«, 4 designed

lky,U' v\'5h * (.» iff >v'a. >>t <> h.u 'tu «>• 'u?v s tc v.•>!• h 0 <0 >¦ s(ua>K Ctwta"ur.d,ii jlutne,
ui'iii Hi/c m'j, j-ttvui gas enn.wi i\, el > )	(

-T*U __Kefct"S*iy _C". -?Vi	cf Hvr>k 4rVn ^ >U"'	,^"t^h>uyft'o|v

C-V" *_ t"*l iM. 3	AkJ> J~	^ ^ 1'0 ^

~£v» jklAl-.t	M «!<¥•< s rt.1	tA»\O^iViJ+k* .\ S ti , fVr tt^y

>Q) otO&M _ _________ 		

last's vi>) ••%btnri u*\w : f ^ '¦ >, 'nolt ttio>> ,n J i U[ie cu v lvVJ	,es I;

J!••'« au >r re! .Hip >ta> >i a'.unt w»«i .ow Uv . p;js.N t>v,,u #s o* ibr *. vtetu

i*. i c v-y-jjl,"T «*>l*
N- v^k p> v x— *	^	_

D-13


-------
Describe issues and observations such as unexpected changes in the cost or scope of O&M or a high
frequency of unscheduled repairs, that suggest that the protectiveness of the remedy may be
compromised in the future.	If	.	,

3" >WV,: <\_V'* _	v- \y i iv^, r.*.!* A	f	J v

.•*>"£	s > AV--¦r4*r

.jx -rVvi	:S^

D. Opportunities for Optimization

Describe possible opportune!--; rcr optimization in monitoring tasks or the operation of t!

IUv i* v> .r (l ^	^; ;*>. n, ^ k.a	t

D-14


-------
APPENDIX E
SITE PHOTOGRAPHS


-------
Photo 1	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: West

Description: Looking West at MW-3 and MW-4

Photo 2	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: Northwest

Description: Looking Northwest at MW-3 and MW-4

l


-------
F

Photo 3	Date: November 29,2018

Location: Bee Cee Manufacturing Site	Direction: Northwest

Description: Looking Northwest MW-2



Photo 4	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: North

Description: Looking North MW-1

2


-------
Photo 5	Date: November 29,2018

Location: Bee Cee Manufacturing Site	Direction: North

Description: Looking North at MW-5 (Weaver popcorn facility)

Photo 6	Date: November 29,2018

Location: Bee Cee Manufacturing Site	Direction: North

Description: Looking North at MW-6 (Weaver Popcorn facility)

3


-------
Photo 7	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: West

Description: Looking west near the former Bee Cee Manufacturing Facility (soil removal area completed in 1992).
This is the area that needs additional soil sampling to determine if soils still remain a risk.

Photo 8	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: Northwest

Description: Looking Northwest near Bee Cee Manufacturing Facility

4


-------
Photo 9	Date: November 29,2018

Location: Bee Cee Manufacturing Site	Direction: Southeast

Description: Looking Southeast near the Weaver popcorn facility (this is the area where additional soil sampling
was completed in 2010).

Photo 10	Date: November 29, 2018

Location: Bee Cee Manufacturing Site	Direction: East

Description: Looking East near the Weaver popcorn property (this is the area where soil sampling was completed in
2010). MW-3 and MW-4 in the background.

5


-------
APPENDIX F
INTERVIEW RECORD


-------
mmurn, mssr-omb-p

Site Name: _£	I \ \ X < t -'fi Jl£.

Subject, f ; si £ >V^v- I » ¦ Q\V>

INTERVIEW UH ORD

EPA ID No-MCd S P fiJJ*.

T >«h*: f§ ', §0 «%y> { Date: a mfm

Type,	i ek'.phone KytOH»

s,> c*; -wK-s	t «w,i X fjwstvM t

<>h .-.Mil, /!).>	i	C'r

. Ate

ivV

Of I nmenntvm

A a\

.A10 £ 3 g 3 £

Dev.w fol!c.ft « V t jf A «iv4 k^la Afcl*rs»*»v> © -f

V»c-	v ; rV,	i iVv l"W ih"fi ;i"^JUs4v-Ut f'« vk

a V .<, \ V «?u I V»w? £**¥£.»	*"Y lit J

I* \,e	(,-r^cvt	AhJ, \S c>¦=• T X s o V \ W W «» J- o uVr^ii	fW,

v.^Wt U; w<» \> ft -^'^a <,-H	'* C..HciSt's

V«\ U	:t „^Wi	H + ^*v> WAN

f >AX r, C e'v- \ 4, u ^ +• \ t\ -. 1 V* A a£ Vv	Vlft- k«-£A. ^

i'u-t ¦.v\v-\\ i- w>*t ^ot -\ V , owM
-------
OSWEFt No. 9355.7-03B-P

iN!TKVii \V KK ORO

Site Name. c Cw M n * w\\K» f
Sub jet; \		

^ M'V ION- inof>	5

! *  Pg)|0,y. | t	g p A > ,s i>,^
«.vvl .-1-, Individual Cootai Hit

¦ iCHJ.	W U.A.VtV" forCcY?* Co,

• • neot 4

1 * . si »h» 2if |>

Nan

%iiress;

Vrh

Summary Of < ¦ rsation

P^v.v Col/.

v».	'¦-? v. «v»vc <•¦*• «>» •

W<+K ^	»>¦*> **/ V. .V-'W < — -*<*

Wt\\.5 v/OhXJl fcv	Wv <2. > y;i *• *«>, *v fk*rt *5. 'hi- jr>	~^a

j\ .-? vv.^' .1V	*- '}. vy* *'v» < -> V-'V Vs-SisV #'«

by AID^,

Page I of

(\,t»


-------
OSWLR No. 9355.7-C3B-P

INTF RVIFW RECORD

Site Name: Qua Ce6 Mtmul\

Subject:

EPA 10 No.-. /1o5 190M0S,
Time: |};Vo«* Date: 3,'i 111';

Type: 9 Telephone
Location of Visit;

Incoming 9 Outgoing

Contact Made By;

Name: [)»

.v^vt

be-k

vuuuiumayu;.

Title: RcmMi*. 1	Organization: B-fA

Individual Contacted:

Name. _kvfje.	tion: /lPfv£

Telephone No: j!"73--757- f«»o
Fax No:	.	,

E-Mail Address: Kfje. ^Vi|arso»i© Jjtt%v»i©,3DV

Street Address: 6d>T /"7 £~

City, State, Zip:	sok C-i 4vy /MO

Summary Of Conversation

P»geI of

I -
-------
fmmi	aoMssoaJMfi

To;	tthtM

Subject:	RE; Bee Cee Manufacturing nrR Questions

Dates	Wednesday, March 06, 2019 11:39:31 AM

Please see my responses below.

Thanks,

-Kyle

From; Pollock, Devin 

Sent; Wednesday, March 6, 2019 10:53 AM
To: Anderson, Kyle 

Subject: Bee Cee Manufacturing FYR Questions

Kyle,

I wanted to send you some questions as part of the FYR process for the Bee Cee Manufacturing Site.

Please see the questions below:

• What is your overall impression of the Site (any issues or concerns)?

Have there been routine communications or activities (site visits, inspections, reporting
activities, etc.) conducted by your office regarding the site? If so, please give purpose and
results.

The state continues tc * ' *		*site "*¦ *			 _x 		 1 unsis.

The slate remains in c	Jen

inspections at this site. Each year the state prepares an O&M inspection report and a
; ,, , 	 ,, :	tgto "	'¦ 	' : " ' say

•	Have there been any complaints, violations, or other incidents related to the site requiring a
response by your office? If so, please give details of the events and results of the responses.

None I

•	Have there been any significant changes in the O&M requirements, maintenance schedules,
or sampling routines since start-up or in the last five years? If so, do they affect the
protectiveness or effectiveness of the remedy? Please describe changes and impacts if


-------
applicable.

ior anything which would affect the

•	Have there been unexpected O&M difficulties or costs at the site since start-up or in the last
five years? if so, please give details.

None known.

•	Do you have any comments, suggestions, or recommendations regarding the site's
management or operation?

lion between the EPA and the state remains effective with the management

Thanks,

Devin Pollock
USEPA Region 7


-------
APPENDIX G
TABLES


-------
BEE CEE MANUFACTURING SUPERFUND SITE
FOURTH FIVE-YEAR REVIEW

Table 1-1: SUMMARY OF SELECTED SITE GMOUNDWATEH SAMPLING DATA



M.W-1

MW-3

MW-4

MW-5

MW-6



Ilex Cr
(p/1)

Total Cr
(p/1)

Hex Cr

{p/1)

Total Cr
(p/I)

Ilex Cr
(p/1)

Total Cr
(H/i)

Hex Cr
{p/1)

Total Cr

ftt/i)

HexCr

(p/I)

Total Cr
(p/1)

Ri 92



24.1

tfMMl

iMNi

NA

NA

liBHHil

¦MHn

NA

NA

FIG 93

--

40.7



¦ill

NA

NA

iililll8

jjliMil

NA

NA

AM 94

<10

<



73,

NA

NA

< 10

<25

NA

NA

am m

< 10

8*



NA

NA

< 10

5.95

NA

NA

AM %

ND

|~

MBm



NA

NA

ND

ND

NA

NA

AM 9?

ND

£





NA

NA

ND

ND

N A

NA

am m

ND

41

llMBi



NA

NA

1

7.47

NA

NA

AM '-w

ND

11



89.9

NA

NA

MM

_ „:IIL :	_

NA

NA

AM 00

ND



jflHMll

MMMlii

NA

NA

—

NA

NA

AM, 01

ND

ND



15.7

NA

NA 1 1 i : - 2

NA

NA

AM 03

ND

ND



42.4

NA

NA

30

.7

NA

NA

AM 04

ND

ND

liMfeil

41.2

NA

NA

10

15.1

NA

NA

AM 05

ND

ND

59

46.3

NA

	

NA 24

NA

NA

AM 06

ND

0.6

MillS

30

30,4

NA

NA

	 	

9.67

NA

NA

AM 07

ND

N

NA

NA

NA

NA

SMsngpMI

30

29.7

NA

NA

AM 08

ND

N

60

47.3

ND

0.25

13

11.7

ND

0.84

AM 09

ND

o.



37.7

ND

0.41

ND

11 s

ND

1.41

AM 10

NS

N

MiMBffll

26.2

ND

0.25

16

13.8

ND

1.33

AM 11

NS

N

I^Bii

43.2

ND

0.25

".13

9.1

2.83

2.5

AM 12

NS

N

Jft.te

43.2

ND

0.63

15.9

16.3

2.31

2,03

AM 13

NS

NS

41.5

39.5

ND

ND

4.98

4.55

ND

1.26

AM 14

NS

NS

15

12.7

ND

ND

12

10.5

ND

ND

AM 15

NS

NS

5,0

4.%

ND

ND

6.6

6.79

ND

2.89

AM 16

NS

NS

7.5

5.81

ND

ND

9.8

7.57

2.5

ND

AM 1?

NS

NS

16

13.7

ND

ND

10.0

9.45

ND

0.59

Rf = Remedial Investigation	Hex Cr = Hexavalent chromium

FIG = Further Investigation of GW Total Cr = "Total Chromium
AM = Annual Monitoring	ND =» Non Detect

Shaded = values are above site remediation goals	NA = Not Available


-------
APPENDIX H

FIGURES


-------
FIGURE 1


-------


Bee Cee Manufacturing

Dunklin County, Missouri

Figure I


-------
APPENDIX I
SITE SAMPLING REPORTS


-------
Abbreviated Sampling Report
Bee Cee Manufacturing Site
Order Number 150318008
Maiden, Dunklin County, MO

Site Information:

LDPR Code: FRBEC __ ESP Staff: jean Counihan,	

Job Code: NJOOBFEC		Ken Hannon			

Investigation Pate: 3'' 17/15			

Introduction:

Hazardous Waste Program (HWP) requested the Knvironmental Services Program (ESP)
personnel collect groundwater grab samples from eight monitoring wells at the Bee Cee
Manufacturing Site located in Maiden, Dunklin County, Missouri. Sampling was conducted as
part of an annual groundwater monitoring event. i'SP Environmental Specialists Sean Counihan
and Ken Hannon traveled to the site on March 17, 2015, to conduct sampling. H WP
Rnvironmenta! Specialist Hvan Kifer was also present during the sampling event.

Field Methods:

ESP personnel deployed clean V II). polyethylene tubing to within the screened interval of
each well. The tithing was attached to a peristaltic pump, which was used to evacuate each well
at a flow rate ot"approximately 200-501) ml/minute. Personnel placed the tubing down to the
bottom of the well and then pulled the tubing up two feet to ensure water was being drawn from
within each well's screened interval. Evacuated water was collected in a five-gallon bucket and
later poured out on the ground away from the wells.

Personnel determined water quality parameters every three minutes during well evacuation and
samples were collected once parameters stabilized (pH +/'- 0.2, turbidity 50 Nephelometric
Turbidity Units [NTUJ, and specific conductance and temperature within 10%). Sample
containers were then filled directly from the tubing. Specific conductance, temperature,
turbidity, and pH measurements were recorded at the time each sample was collected. Samples
were filtered and/or preserved in the field as appropriate for the anahtes of concern and placed
on ice in coolers. All samples were transported buck to the ESP laboratory in Jefferson City and
submitted for total and hexavalent chromium analyses.

Observations:

AH wells* protective casings and locks were intact upon arrival. The weather during sampling
was sunny and approximately 65 degrees Fahrenheit Winds were from the northeast at 15-25


-------
Bee Cec Manutaclming Site
Abbreviated Sampling Memo
March 17,2015
Page 2

miles per hour.

Well MW-3 did show a slight increase in turbidity from the previous sampling year, although
there had a been downward trend observed when compared to several other past sampling
events, 1 urbidity readings had decreased from 351 to 38 to ^.93 lo 1,8(1 NTUs respective!) when
compared lo the March 2011, 2012. 2013 and 2014 sampling events. The 4.51 NTH reading was
a slight increase in turbidity from the previous year. 1 he increase could be in pail to a large
amount of rainfall and snovvmclt thai had occurred in this area over the past few months. All the
wells sampled during this sampling event showed initial high turbid its' when purging procedures
were initiated. VIW-4 again contained a noticeably high amount of an orange slime (iron
bacteria.') in the purge water but cleared up after initial purging. Any discoloration or turbidity
noted during the other well s initial evacuation cleared up significantly by the time samples were
collected.

Refer to I able 1 for a description and location of each sample collected. Refer to Table 2 for
additional information recorded for each monitoring well.

Refer to the site map for the approximate locations of samples collected. Also attached are
analytical results of samples collected.


-------
Bee Cee Manufacturing Site
Abbreviated Sampling Memo
March P. 2015
Page 3

/vjH(LnvnM"f{
Kenneth Hannon
Environmental Specialist
Field Services Unit
Environmental Services Program

Eric

Sappington

Digitally signed by Eric Sappington
DN: cn=Erlc Sappington, o=DNR,
ou=Reld Services Unit,
email=eric.sappington@dni\mo.gov

, c-US

Date: 2015.05,04 13:54:5? -05 W

Eric Sappington
Unit Chief

Environmental Emergency Response/Field Services Unit
Environmental Services Program

c:

Evan Kifer. Environmental Specialist, HWP


-------
Table 1
Sample L isting
Bee Cee Manufacturing Site
Maiden. Dunklin County, Missouri
March 17.2015

Sample
Number

Date
Collected

Time
Collected

Sample Description



3-n 15

1430

Sample was clear and colorless. Purge water contained an oranae iinae that cleared prior to sarnplin°

15041 J 1

3 i 7,-15

! 44.-

_ °' MW Sample was clear and colorless. Purge water contained an orange tinge that cleared prior to sampling

150415

150416

3.17-15

1^03

Water_grab of MW-8. Sample was clear and colorless- Purge water contained an orange tintje that cleared prior to sampling

3''1715

1530

Water grab ot MW-/. Sample was clear and colorless. Purse water contained an orange tinge that cleared prior to sampling

150417

3/17,'15

1S50

WalcLSrab 01 MW-6. Sample was clear and colorless. Purge water contained an orange tin^c that cleared prior to sampling

151)418

3 ¦' 17*15

1620

	Watg,grab	SlMW-5. Sample was clear and colorless. Purse water contained an orange tint>c that cleared prior to sampling

150410

3 17/15

1610

Water grab of M\V -4. Sample had a slight orange tin«e and pursue contained a heavier orange tinge

15042(1

3/17 15

1648

W8'?!!™.!5 ofMW-3. Sample was clear and colorless. Purge water contained an orartae tinee that cleared nrior to sampling

150421

3/17 15

1648

Duplicate of 150420. ~ ' 				—-c_

Table 2
Monitoring Well Information
Bee Cee Manufacturing Site
Maiden, Dunklin County. Missouri
March 17, 2015

Well Identification

Diameter/Construction

Total Depth (ft)
From TOC

Depth to Water (ft )
From TOC

Water Column (ft)

Purge Rate (ml/min)

!U~t

2" I'Vf

iTiJi

1 9^90

9.08

450

\lW-4

r p\ c

51.40

9.90

• 1.50

450

IW-5

\

H

0.30

8.81

475

1W-6

p\ c

28.60

10,60

8.00

400

MW-7

2" P\ 0

29.15

10.50

8.65

400

MW-8

2" PVC

:.7S

10 80

17.91

400

IW-9

2" PVC

29.95

10.66

18.29

400

MW-IO

2" PVC

29.10

11.00

8.10

450


-------
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or-. SCttf"' e\V» »W rt t M«f i ;


-------
MISSOURI DEPARTMENT OF NATURAL RESOURCES
FIELD SHEET AND CHAIN-OF-CUSTODY RECORD

W"

Egg

Description of Delivery

~ Tape sesled and Initialed Total No. Of Containers: f
Q Shipped Carrier:

0 Hand Delivered By:

Collector's Name: „ iLn

Kenneth Harmon

(Pkose Print)

USE ONLY!



_____ Q
~

KCRO £
MoDOT f

115*0 [TsTrO n"5LRO 0~siS~O~WPP ~ MGS Q HWP 0 ESP

MDC n DHSS n other:

\So2>vSM

Location:

S\8>

Sample Number

Sample
Collected

Analyses Requested

Disinfect.
Type

Held Parameters
(include units)

Matrix
(theck onej

Container
Type

Preservative
Type

Number of

(Sample A|

Date;

3/17/2015

Total and Hexavaient Cr.

(ehnkcm)

0 None
Q Chlorine

~	UV

D Oione

~	Other:

D.O.





35DCM



1

flow



$( Water

,3SQJL»



1

PH

-i

~	Soil

~	Organic

~	Sludge
D Other:







For LabUsaOnfy

CfcyLfnf

Time-,

i^W

Temp.

-jLxltXiSS

—		 	—





Other:









Turbidity

f, B6 ffTU









)$(> H / V

(Sample B)

3/17/2015



13 None

O Chlorine

~	uv

D Oime

~	Other:

D.O.







Tiisr-

1

Flow



Q5 Water





1



C.HJT

n Sail







Lab Use Only

SttW^X)

Time:

f-l 17"

Temp.

/-A-rV IS-,9 *<•

n Sludge
D Other:



	—_



Other:









Turbidity

l) -J 6 VliA







>Co'i jr

{Sample C)

Date:

3/17/2015



0 "we

Q CNonne

0 uv
~ Ozone
PI Other;

D.O.



8 Water

2

1^1"

1

Flow



asocu

^4CT^

j—

pH



~ 5o«







For lob toe Only

Time:

/ <3 ST

Temp.

t6,H "C

~ ~[
til







Other:









Turbidity

5..61 A>7«



		__



Ztrj^

{Sample DJ

Out

3/17/2015

Total »nd Hexavaient Cr.

0 None

~	Chlorine

~	uv
D

O Ottei

D.O.



R Water

2SSCW

Tipwr-

—T—-

Flow





«L

i

PH

tend.



J Sot







for 1Mb Use Qnfy

Time:

1S30-

Temp.

i6,? **

3 Sludge







Other:



~ Other:







Turbidity

)P,(t tJTli









Relinquished By: J, > ,

		a£^32^o			

itecerved By:





3- If



T,me: li:5

S

Relinquished 8y:

deceived By;

Dale;

Time:

Relinquished By:

Received By:

Data:

Time:

MBMI EiwrtroMMflOl Stnlces Prognm

®18 mm Mth, Mfason C*y, MO 6S1M 873) S1MI1S

Page 1 of 2


-------
MISSOURI DEPARTMENT Of NATURAL RESOURCES
FIELD SHEET AND CHAIN-Of-CUSTOOY RECORD

Sample ft ldpr-.

FEBEC

|)ob Code:

NJOOBEEC

Sample Reference ID:

Facility ID;

Site/Study Name:

Bee tee Manufacturing

County:

Dunklin

iample Comment (where and how the sample was collected):

well faW-/0

B Grsb O Composite Q Modified Q Other:

SPS Coordinates
(UTM Zone 15
HAP83 Oniyl

"SampTe B [ujjT

X lasting

Y Northing

Accuracy

n
a

(cheek am]

S»E (meters)
PDOP

Sample Event Typaslcto:kme)

~	Bypws/SSO

Q Complaint

~	Emergency Response
Q Inspection

0 Investigation

~	Monitoring
Q Special Project

Sample Type; {cluck one}
H Mr	g——

Q Container Q Spill

~	QVQC O Wipes

0 Groundwater Q Storm Water
Q Organic Q Surtace Water
Q Sediment Q OKdwrge
Q Sludge

~	Prinking Water Supply

FEBEC

TtobtodtT

NJOOBEEC

Sample Reference ID:

Facility ID:

Sample Comment (where and how lie sample was collected):

u«?i( rw-i

Site/Study Name:

See tee Manufacturing

County:

Dunklin

0 Grab ~ Composite ~ Modified

D OOw:

SPS Coordinates

(UTM Zone 15
HAPaiOtiy)

~Sampi« C fiDPR:

X Easting

Y Worthing

Accuracy

E

(thttkemeJ

EPE (meters)
POOP

Sample Event Type:fetet*aflg)

~	Bvpks/sso

Q	complaint

O Emergency Response

0	Inspection

0	Investigation
Q Monitoring
0 Special Project

Sample Type: jcheck 
-------
MISSOURI DEPARTMENT OF NATURAL RESOURCES
FIELD SHEET AND CHAIN-OF-CUSTODY RECORD

HI

fffetseWnlf

SStote U kcro n~**o QoS5 TT&ro n swro IT

~ WoOQT ~ MOC ~ OHSS d Other:

»r% Mime:

Kenneth Harmon

fl Tape seated and mil
~ Shipped
0 H»nd Ocffwrtd

DesciTptiw^Del^rv*

T«tal No. Of Containers:

Carrier;
By:*

WPP

Simple Number

Sample
Collected

Analyses Requested

O MSS 0 HWP Q ESP

Disinfect.
Type

Field Parameters
(include units)

IAB USE ONtY!

Laboratory 10:

Matrix
(check ant)

Container

J2L

Preservative

36

Type

location:

Number of

Containers

IfOHIl

(Sample A)

Date:

3/17/2015

Total and Hexavalent Cr.

Forieb Use Only

(Sample B)

for Lab Use Only



Time:

I rs-0

Dale:

3/3,7/2015

Time;

16 ZD

Total and Hexawtont Cr,

(check oneI

0 None

~	Chlorine

~	w
O Ozone

~	Other:

0.0.

flow



Cond,

Temp.

Other:

Turbidity

B

Q Chlorine

~	W

~	Ozone
O	other:

D.O.

flow

EIL

Cond.

Temp.

Other:

Turbidity

AjfiJL



JSJLf£_

TT

A Water

~	Soil
O Organic

~	Sludge

~	Other:

JBESg.

jstsmit

I

3L

10 7tt

f.'ik.





H	Water

5	SoM

3]	Organic

3]	Sludge

~	Other:

?.3<5 biV*

HC

\ZOH ic\

Cample C)

3/17/2015

fitrlab Use Only Time:



\iL) o

0	None
Q Chlorine

~	W

~	Ozone
dj	Other:

D.O.

flow

PH

Cond.

Temp.

Other:

TurbWfty

7.33

2z±LJA1l.



Water
~ St*.

1]	Organic
D Sludge

2]	Other:

am

J3SB

m

P5T





iCOHZO

(Sample Of

Date:

3/17/2015

Total and Hexavalent Cr.

for tub Use Only

Time:

i

Rtlr»n«ishtd By:

Refinqufchsc By:

Jljja&Zl&ZL.

ReSnqushed By.

0	None
PI Chlorine

~	W

O	Ozone

~	Other:

D.O.

Flow

eh__

Cond.

Jt-Sl

/ S"fe.3

Temp.

Other:

c/.t v(.

g Water
Sod
3 Organic

~	Sludge

~	«her:





—

Turbidity

, ST/ mtt

Received I

s	—

Date:

Received By:

Date:

3-W-1S

jpci«d

By:

Date:

Time;

1!:S5T

Time:

Time:

MDNR Ewlroommul Sswlces Program

2710 Wwt Mn, Jefew City»MO SS109 (573) 57&-3J1S

fi§S i Of 2


-------
MISSOURI DEPARTMENT Of NATURAL RESOURCES
HELD SHEET AND CHAIN-OF-CUSTODY RECORD

"SampleA [ldprT

FE8EC

Facility ID:

Sample Comment (where and how the sample was collected):

ytfl

Job Cod*:

NJOOBEfC

Slte/Stiidy

Sample Comment (where and how the sample was collected);

w-tii

Bee Cee Manufacturing
"W~Srab~TJ~Composlte ~""hiod/id	~55*r~

County;

DunkBn

Sample fmmt fmmstctmk onei

~	B««VS5D

~	Complaint
Q	Emergency Response
Q	IrapeCHon
0	investigation
O	Monitoring

~	Speonpn^tet

Sample Type: (check am}

~	a* 0*15

Q Container Q Spill

~	QiVQt ~ Wipes

0 Groundwater Q Storm Water
0 Organic Q
O Sediment Q Discharge
D Sludge

j Water Supply

GPS Coordinates
(UTM Zone 15
NAD83 Only)

X Easting

Y Worthing

Accuracy

((heck one}

~	EPE(metws)

~	PDOP

Q	Complaint

0	Emergency Response

0	Inspection

0	Investigation

O	Monitoring

0	Special Project

O	Container	Q	Spill

~	QWQC	O	Wipes

~	Groundwater	Q	Storm Water
0	Organic	Q	Surface Water

~	Sediment	0	Discharge
0	Sludge

~	Drinking Water Supply

Facility ID;

Site/Study Name:

Sample Comment {where and how the sample was collected):

Bee Cee Manufacturing

Dunklin

T3~5* ~ Composite ~ ModifW	{"J Other:

We 1/ PHV-

Sample Event Typa;fcheck rntj

~	BfpasslSSO
O	Complaint
PI	Emergency Response

~	Inspection
0	Investigation
O	Mentoring

S«mpl« Type: {check me)

ITa* 0	m"

~	Container Q	Spill

~	QA/QC O	wipes

0 Groundwater O	Storm Water

l~1 Organic 0	Surface Water

~	Sediment Q	Discharge
0 Sludge

Sample Comment (where and how the sample was collected):

wpD my-J

	0 Grab TT"5n'iF«5e Q	0 Ottxw;

{UTM Zone 15
NA083 On)y)

Remarta:

X Easting

¥ Worthing

Accuracy

(check am)

n~T5if(S»Ssr
~ POOP

~	Bypass/So

Q	Complaint

~	Emergency Response

~	Inspection
0	Investigation
0	Monitoring
O	Special Project

Air	~	Soil

Container	0	Spill

QA/QC	~	Wipes

Groundwater	0	Storm Water

Organic	Q	Surface Water

Sediment	Q	Discharge
Sludge

Drinking Water Syppty

X8°c

MDNR eovironmemai Services Program

2710 West Main. Jefferson City, MO 651<» (5731526-3315

Page 2 of 2


-------
MISSOURI DEPARTMENT Of NATURAL RESOURCES [f •
FIELD SHEET AND CHA1N-OF-CUSTODY RECORD

~	Taps sealed and initialed Total No. Of Containers; fs

~	Shipped Carrier:

0 Hand Delivered Sy:

Loiiector'sfcame: „ u „ 			

Kenneth Harmon

(Please Print)



W

Laboratory ID:

Location:

Affiliation: U

KCKO £
HoOOT f

] HERO ~ alio ~ SLRO ~ SWRO ~ WPP Q M6S Q HWP 0 ESP
HOC ~ OHS5 ~ Offier:



Sample Number

Sample
Collected

Analyses Requested

Disinfect.
Type

field Parameters

(include units)

Matrix

icMdt ant;

Container

Type

Preservative

Type

Number of

i& 1IU

(Sample A)

3/17/2015



(check arte)
13 None

O Chlorine

~	uv

~	Ozone

~	Other:

D.O.





"OTT

-gKBl-

1

Flow



Sfi Water

"Sep

"Tt

1

PH



I 1 *

Illl
~~~~







Cond









For lot Use Only

kj4U%)

Time:

Temp,









Other:









Turbidity,











p__

Date:



» 1 S &
~ ~~~~

D.O.



lalll
~ ~~~~







flow









19}

pH

Cond.

		







for ukUmOatf

Time:

Temp.









Other:









Turbidity









(Sample 0

Date:

,

~ ~~~~

0.0.



~ water







Flow













1 Soil







fertfli Oft Oalf

Dmc:

Temp.



D Sludge

~ Ottw;







Other:









Turbidity











(Sample D)

Dale:



~ ~~~~

D.O.



~	Water

~	M







Fit









P» .......









Cond.



~	Organic

~	Sludge







fot lob Use Onty

rime:

Temp.









Other:



~ Other:







Turbidity





















Refinquisbed 8y: j, , ,

—_——.— ' 	UJ&nstt53ri.„			



D,„

-15

Ti-

__J

Relinquished By:

Received By:

5# fee:

Time: —1

Relinquished By:

Received By:

Date

Tim«: ——————-4

MD1* t**tr»nm«nui Sefvtccj Program

mo West M»i», Jellamn Qtf, MO 8$»S fSBf S2I-33IS

Pip I of 2


-------
MISSOURI DEPARTMENT OF NATURAL RESOURCES
FIELD SHEET AND CHAIN-Of-CUSTODY RECORD

Sample A Iidpr:

FE8EC

Job Code:

NJOOBtEC.

[SampteRefefence 10:

Facility 10;

Site/Study Name;

See tee Manufacturing

County:

Sample Comment (where and how the sample was collected):

GPS Coordinates
{UTM Zone IS
MAD83 Only)

0 Grab Q Composite ~ M^ified

Dunklin

D other:

Sample Event Type:fcto*enef

Sample B

X Easting

Y Worthing

Accuracy

fdxdtamj

PDOP

U	Bypass/SSO

n	Complaint

O	Emergency Response

0	Inspection

|3	Investigation

Q	Monitoring

O	Special Project

kmt}

O	^	~	Sol!

1H	Container	Q	Spill

~	QA/QC	~	Wipes
0	Groundwater	Q	Storm

~	Organic	Q	Surface Water
Q	Sediment	tH	Discharge
D	Sludae

f"~]	DtirrMng Water Supply

IDPR:

JofcCeie;

Sample Reference ID:

Facility ID;

Sft#/5t«§? name

County;

Sample Event TypeifciwrftoneJ

Sample Comment (where and how the saraph was collected);

~ Grab ~ composite ~ Modified Q Other

SPS l
(UTM lotto 15
NAP83 Onty)

"Sampie"

X easting

Y NortWng

Accuracy

(check am}
Q EPE (meters)

~	Bypass/SSO

Q	Complaint

Q	Emergency Response

Q	inspection

0	Investtoation

Q	Monitoring

0	Special Project

Sample Type: (check ami

~	A»	~ Soil

0 Container Q Spill

~	QA/QC ~ Wipes

0 Groundwater Q Storm Water
0 Organic Q Surface Water
Q Sediment Q Discharge
O Sludge

n MnMng Water Stipply

LDPR:

[JotTcodc

"pimpSteferencelD:

Facility IB:

Site/Study Name:

Sample Comment (where and how the ample was collected):

County:

"~""Grab ~ Composes !_J

~ Otter:

GPS Coordinates
(UTM Zone IS
MAD83 0»lyJ

Sample D

X Easting

Y Northing

Accuracy

(check me)

~ EPE (meters)
HI POOP

Sample Event Typesfrfieet sue)

FT" B/pasySSO

~	Complaint

Q	Emergency Response

Q	Inspection

0	Investigation

Q	Monitoring

Q	Specisi Project

Sample Type; (check one)

~	A*	~	Soil
Q	Container	Q	Spill

~	QA/QC	~	Wipes
[3	Groundwater Q	Stonm
Q	Organic

~	Sediment	0	Discharge
O	Sludge

~	Prinking Water Supply

LDPR:

Job Coit:

Sample Reference ID;

Facility ID;

Site/Study Name:

County.

Sample Comment {where and how tha sample was eoltecte#

~ Grab O Composite ~ Modified ~ Other:

SPS Coordinates
{UTM Zone 15
MA083 Onty)

Remarks:

X lasting

Y Northing

Accuracy

(dwdtom)

~ W (meter*)"

am

Sample Event Type;fo>fdi our;

Q	Bypass/SSO

Q	Complaint

Q	Emergency Response
Q Inspection
0 Investigation

O	Monitoring

Q	Special Project

Sample Type: (thetkom)

~	**	"" ~	So#

Q	Container	Q	Spill

o	QA/QC	~	wpes

(3	Groundwater Q	Storm Water

0	Organic	Q	Surface Water

~	Sediment	~	Discharge
0	Sludge

~	OrioMng

<3-S°C-

MDNR Environmental Services Program

2710 West Main, Jefferson City, MO 65109 <573} 526-331S

Cage Jef2


-------
Or «&¦

STATE OF MISSOURI

DEPARTMENT OF NATURAL RESOURCES.

PO Box 176 Jefferson City MO 05102-0176

Environmental Services Program
RESULTS OF SAMPLE ANALYSES
LOPR/Job Cods;	Program, Contact:

FEBEC/NJOOBEEC	HWP Evan Kifer

Evan Kifer

Hazardous Waste Program

Q-







Order ID:
150318008

Report Date;
5/1/2015

Sample: AC44779	Customer#: 150413

¦ ¦lllllll	Site; Bee Gee Manufacturing	County: Dunklin

Collect Data: 3/17/2015 2 20:00 PM	Collector; KENNETH HANNON	Affiliation: ESP

Comments: Grab: Well WW-10

Project; NJ00BEEC

Test

6020 Metals-Total Recoverable
Dissolved Hexavaient Chromium

Field pH

Field Specific Conductivity
Field Temperature
field Turbidity

Sample: AC44780

Parametar/Method

Chromium/SW 848 8020
Dissolved Hexavaient
Chromium/SW 848 7196A
Field pH/EPA 150 1
Field Specific Conductivity/SM 2510
Field Temperature/EPA 170.1
Field Turbidity/EPA 180.1

Result

Units

Qualifiers)

1.45

pg/L

08

<0.002

mg/L

ND

6.58

pH Units



141.1 uS/cm





16.3 C





1,80

MTU



Customer#: 150414

Collect Date: 3/17/2015 2:45:00 PM

Bee Cee Manufacturing

Collector: KENNETH HANNON

County: Dunklin
Affiliation: ESP

Comments: Grab; Well MW-9

Project: NJ00BEEC

Test

Parameter/Method

Result

Units

6020 Metals-Total Recoverable

Chromium/SW 848 6020

3.15

pg/L

Dissolved Hexavaient Chromium

Dissolved Hexavaient

<0.002

mg/L



Chromium/SW 846 7196A



Field pH

Field pH/EPA 150.1

6.45

pH Units

Field Specific Conductivity

Field Specific Conductivity/SM 2510 85.3 uS/cm

Field Temperature

Field Temperature/EPA 170.1

15.9 C



Field Turbidity

Field Turbidity/EPA 180.1

4 76

NTU

Qualifier^

ND

Ocder ID: 150318008 {1/3)

Page 1 of 3


-------
Sample: AC44781	Customer i: 150415

llllllllllllllll	S,tK Bee Gee Manufacturing	County: Dunklin

Colled Date: 3/17/2015 3:05:00 Ptrt	Colteetor: KENNETH HANNON	Affiliation: ESP

Comments; Grab; Well MW-8

Project: M

test 	

6020 Metals-Total Recoverable
Dissolved Hexavalent Chromium

Field pH

Field Specific Conductivity

Field Temperature

Field Turbidity		

Paramstar/Method

.Result

2.60

<0.002

Units

J2uaflflsr{s)

Chromium/SW 846 6020

Dissolved Hexavalent
Chromlum/SW 848 7198A
Field pH/EPA 150.1	6.43

Field Specific Conductivity/SM 2510 105.4 uS/Offl
Field Temperature/EPA 170,1 18.4 C

Field Turbidity/EPA 180.1

3.82

pg/L
mg/L

pH Units

NTU

ND

Sample: AC44782

|

Collect Date: 3/17/2015 3:30:00 PM

Collector: KENNETH HANNON

Comments: Grab, Well MW-7

Customer#: 150416

County: Dunklin
Affiliation: ESP

Project: NJ00BEEC

iTest

Parameter/Method

Result

6020 Metals-Total Recoverable
Dissolved Hexavalent Chromium

Field pH

Field Specific Conductivity

Field Temperature

Field Turbidity 	

Chromium/SW 848 8020	3.41

Dissolved Hexavalent	0.0028 - ¦¦
Chromium/SW 848 719SA

Field pH/EPA 150.1	8.5?

Field Specific Conductivity/SM 2510 179.2 uS/cm

Field Temperature/EPA 170.1	16 7 C

Field Turbidity/EPA 180.1	10.8

Unite

Mg/L
mg/L

pH Units

NTU

Qualifl»r(s)

Sample: AC44783

lllllllllllllll	Site: Bee Cee Manufacturing

Collect Date: 3/17/2015 3:50:00 PM	Collector: KENNETH HANNON

Customer#: 150417

County: Dunklin
Affiliation: ESP

Comments: Grab; Well MW-8

Project: NJOOBEEC

Tost

6020 Metals-Total Recoverable
Dissolved Hexavalent Chromium

Field pH

Field Specific Conductivity

Field Temperature

Field Turbidity	

Parameter/Method	Result

Chromium/SW 846 8020	2.89

Dissolved Hexavalent	<0.002
Chromium/SW 846 7196A

Field pH/EPA 150.1	8.48
Field Specific Conduct! vity/SM 2510 227 uS/cm

Field Temperature/EPA 170.1	15.8 C

Field Turbidity/EPA 180,1	9.10

Units

«/L

mg/L

pB Units

NTU

Qualifiers) _
ND '

Sample: AC44784

Collect Date: 3/17/2015 4:20:00 PM

Site: Bee Cee Manufacturing

Collector: KENNETH HANNON

Customer#: 150418

County: Dunklin

Affiliation: ESP

Comments: Grab; Well MW-8

Project: NJ00E

Test	 	_		

020 Metals-Total Recoverable
Dissolved Hexavalent Chromium

Field pH

Field Specific Conductivity

ield Temperature
Field Turbidity

Parameter/Method 			Result

Chromium/SW 848 6020	8.79

Dissolved Hexavalent	0.0066
Chromium/SW 846 7198A

Field pH/EPA 150.1	5.92

Field Specific Conductivity/SM 2510	135.5 uS/cm

Field Temperature/EPA 170.1	14.3 C

Field Turbidity/EPA 180.1	7.36

Units

Mg/L
mg/L

pH Units
NTU

Qualifier^)

Order ID: 150318006 (2/3)

Page 2 of 3


-------
Sample; AC44785



Customer#: 150419

¦llllllll

Site: Bee Cee Manufacturing



County: Dunklin

Collect Data: 3/17/2015 4:40:00 PM Collector: KENNETH HANNON



Affiliation: ESP



Comments: Grab, Well MW-4









Project: NJOOBEEC

Test

Parameter/Method Result

Units

Qualifier^)

6020 Metals-Total Recoverable

Chromium/SW 848 8020 --0 50

|jg/L

ND, 08

Dissolved Hexavalertt Chromium

Dissolved Hexavalent <0 002

mg/L

ND



Chromium/SW 848 7198A :



Field pH

Field pH/EPA 150 1 7 33

pH Units



Field Specific Conductivity

Field Specific Conductrvity/SM 2510 281 uS/cm





Field Temperature

Field Temperature/EPA 170.1 18.0 C





Field Turbidity

Field Turbidity/EPA 180.1 87.9

NTU



Sample: AC44788



Customer #:

150420

iiirim miii ii

Sit#: Bee Cee Manufacturing



County: Dunklin

Collect Date: 3/17/2015 4,48-00 PM Collector: KENNETH HANNON



Affiliation: ESP



Comments: Grab; Well MW-3









Project: NJOOBEEC

Test

Parameter/Method Result .

Units

QunUfietfs)

6020 Metals-Total Recoverable

Chromium/SW 846 6020 4.98

pg/L



Dissolved Hexavalent Chromium

Dissolved Hexavalertt 0.0050

mg/L





Chromium/SW 848 7196A



Field pH

Field pH/EPA 150.1 4.92

pH Units



Field Specific Conductivity

Field Specific Conductivity/SM 2510 158.3 uS/cm





Field Temperature

Field Temperature/EPA 170.1 9.8 C





Field Turbidity

Field Turbidity/EPA 180.1 4.51

NTU



Sample; AC44787



Customer #:

150421

IlflMHIIIIHlfllHIIHHflU

Site: Bee Cee Manufacturing



County: Dunklin

Collect Date: 3/17/2015 12:00:00 AM Collector: KENNETH HANNON



Affiliation: ESP



Comments: Grab: Blind Duplicate









Project: NJOOBEEC

Test

Parameter/Method Result

Units

Quaiifter(s)

B020 Metals-Total Recoverable

Chromium/SW 848 8020 4 97

pg/l



Dissolved Hexavatent Chromium

Dissolved Hexavalent 0.0050

mg/L





Chromium/SW 848 7196A



The analysis of this sample was performed In accordance with procedures approved or recognized by the U. S Environmental Protection Agency,

Data Qualifcrfs)

05 Estimated value, detected below PQt 08 Anaiyte present in blank at > % reported value
3JM- NO	 Not detected at reported value 	

Chris Boldt, Laboratory Manager
Environmental Services Program
Division of Environmental Quality



Order ID; 150318008 {313)

Page 3 of 3


-------
Abbreviated Sampling Report
Bee Cee .Manufacturing Site
Maiden, Dunklin County, MO

Site Information:

LDPR Code: FEBEC	_ - ESP Staff: Sean Comiihan 	„

Job Code: NJCWBEEC		KenJtija$«L__^

Investigation Date: 5/11/16		

Introduction:

Hazardous Waste Program fKWP> requested the Fnvironmeutai Services Progt am (FKP^
personnel collect groundwater grab sampler ftom lout momtormg wells at ihe Bee Cee

Manufacturing Site located in Maiden. Dunklm Gnmn, Missouri Sampling w as conducted a>
part of an annual groundwater monitoring event, HSP Hwsromnental Specialists Scan Counihtm
and Ken Hannon trase'ed to the site on May \ I, „!o!6„ to conduct samphm;. 11 \V P
Environmental Specialists Fvan Kafer and Kvlc Anderson were aiso present during the sampling
e\ cut along with Andtew Cneseke from I'SUPA

Field Methods:

FSP personnel deployed clean V! D. polyethylene tubing to within the screened interval of each
well. The tubing was attached to a peristal he pump, which was used to e\ aenate each well at a
How rate of approximately 200-500 mfnunute Pei sonnel placed the Hibing down to the bottom
of the well and then pa'led the ashing up two feet to ensure water was being diawn ftom within
each well's screened interval. Fvaeaatod water was collected in a live-gallon bueket and Utter
poured out on the ground awu> irom the wells.

Personnel determined water quaht> parameters every dime minutes during wdl evacuation and

samples were collected once parameters .stabilized tpf i - - 0 2. turbidity 50 Nephelometric
Turbidity Units [Nil1], and specific conductance and temperature within 10%f Sample
eonfatrteis were then filled directly from the tubing. Specific conductance, temperature,
turbidity, and pH measurements were recorded at the time each sample was collected. Samples
were filtered ami-or preserved in the field as appropriate for the analyses of concern and placed
on ice tn eoolers All samples wete transported back to the FSP lahorators in Jefferson City and
submitted for total md hexa\ akmt chromium aiMi)Stts,

Observations:

All wells' protective casings and lucks were intact upon arrival The weather dun up, sampling
was sunny and approximate!) 84 degrees Fahrenheit Winds w ere from the southwest at 15-25


-------
Bse I'ee Manulactunng ^tU1
Yt.bie, uted Sampling Mvnx

M.u 11, 23m

miles per hour.

MW-4 again conx.vmd a n>ituv,xl.>i\ high amount of an omngu sume (u*or. bacteria?) in the purge

water tut cleared up aftet initial purging. \m ii!M.ok".tt;on 01 turbidity noted during the other
well's miu.il ev> ila time samples were collected.

Refer to Table 1 foe a dcaci »piu>ii and locution of each sample collected. Refer to Table 2 for
additional information rcceided lor each monitoring well. Also attached are the chain of custody
and malyticJ icsuiih of sample^ collected.

By Eric Suppington at 2 59 pm, Mug 09, 2018

trie Nappingkm
i nil Chief

I nvitvmmemal L ires gene . Rc^poi^e Hdd Services Unit
F.iiuionmonta! Services Program

HoyrvnSf{

Kenneth Harmon

Environmental Specialist
Field Services Unit
Environmental Services Program

APPROVED

c: L'van Kifei, 1'iivuunmental Spcuahsu HWP

K\le Anderson, Fnvsroamenud Spcciad.st. IIWP


-------
Fable 1
Sample t is! my
Bv-e C'ec Vfamilacfutmg Sitv-
Maiden, Dunklin Counts Missouri
May N. Tmo

Sample

Dale



Number

(ollecfecl

1

16?"6^

•>< I 1 ! 0



i (%J !;<,{i

> i 1 Hi



So_*

¦'•')! -Ifc !

1 ''2 ToS

^ II 16 |

!f076»s



Time

Sample Description

Wnfc-j-jj' 'J' ot MVV -o _ Sample \\j*s cleji .mci utlotk « P v\]rp:tn|>
¦ \Vatv-i guh a!	Sample \»e« cleat ami toleiless s\nee w;stei u.nlanud ,ui «>»angf tmgv- that Je<»»e() jn wt to sampling

W.itCi i)l MW-i Sample had a flight <'r.titjy tinge and pisfve tonuuneti a Ueavifi orange tinee

W.ite uab <>f MNV-j ^Sampk u„>\ eleai ami ei'lni less, foige vm!ci vonuii'itvl.» milk) tinge that (ic,»sctljpiit>r to sampling _

n*i>V(]KUuntv Nh^uuri
via\ ii _i < (>•»

Well Id

«	i i nidi lk\ub i ft * I

>ie;>nihaSu»r> J	l omu'C'^'I ! , ' . 1

f	I !>' !» « < «	[

I to '.Citet ! it!
From TOC

MW

hl'A-'-
MW ^
MW-6

1 ,-v <>

s 1.42
19,91
28

, .
-------
Collector's Name;

Buuti

!m&$e rnntj

m

MISSOURI DEPARTMENT OF NATURAL liSOURCES
FIELD SHEET AND CHAIN-OF-CUSTODY RECORD

Q Tape stated and
~ *

ri	w

n	osjm

, )	othvt

Sit

How

Cond.
Temp

Otnet



cf*1" '•«

k/ . £•_

Wsler

~

[J Cigar*
P lyt'w
O Ottwrt

A" Til

/, *7

ifisa-jfefe.
ias^Lfen

21:

Dair.

I f 2 7 i- " j s , ,

(5#mpte Cj

Cr.

For Lab Use Only

fkrsa'®



i

•>

o.e

p i	Mo lt>

[" |	riiiiTif%'

n	*

~	0"««e

D	oiw.

Fk'W, 1

£*?'/
^ZZZZl5II£__

(Hbw I 		

TiXktv * J.V,-

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[>< Wjtv<

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Organv.
(_ ] Sudije
[] "*«•'

Sad, JUU.
Sam'

L

CK>_

Becoivfid By

Received By;

6tL

D"* 51 til to

Time,

: 11 4c

Date.

TifTI0X

¦Reilmuishetl By:

Rtctiwi By:

Date;

vdkr Emrt!oiw»iitt3l SemeesP«iram

2730 W*5t M»k	«y, MO 65109 e?IJSt6-S31S

I>a|el8f2


-------
Facility ID:

MISSOURI DEPARTMENT OF NATURAL RESOURCES
FIELD SHEET AND CHAIN-QF-CUSTODY RECORD

Sample A

LOPR:

FEBEC

lob Code:

NJOOBEEC

Site/Study Name:

Sample Comment fwhera and ho* the sample was collected):

r*\ yJ • i Cs+v 17 fo

Bee Gee Manufacturing
13 Srat* Q Composite Q Modified Q other:

Sample Reference 10:

County:

Dun kin

GPS Coordinates
(UTM Zone IS
NAD83 Only

a

Y Northing

Accuracy

(cheek uoel
[J EPE (meters)

D poop

Igmpie Stent Typeiiaerit one}

n	Complaint

Q	Emergency Response

G	tepection

0	Investigation

O	Monitoring

0	SectBi Project

Sample B [iopr:

FIB6C

&MWpleTfpg {check got)
n f*r	~ Soi

Q Container Q Spill

~	sWQC fj Wipes

[3 Groundwater Q Storm Water
Q Organic [~] Surface Wat<

~	Sediment Q Discharge
Q Sludge

D_Mgn8Wat»Stippty

lob Code:

NJOOBEEC

Site/Study Name:

Bee Cec Manufacturing

* Comment {where and how the sample was colectei):

Sample Reference 10;

County:

Dunklin

Grab

Campsite

Modified

Other:

Facility ID: '

Site/Study Nam,: geg Cee Manufectufing

Duni;;n

Sample Event lype-.fchnk <*»>

Sample Typa: (chtdoml

Q Bypass/SSO
Q Complaint
0 Emergence ttespr csi
Q Inspection
0 Investigation 1
D Monitorinq

~	«r ~ Soil

~	OffeMS' Q Spill

~	QWQC [1 Wloes

Q Groundwater Q storm Warn
Q Organic [_] $jrfae« Vteitei
Q SeiOrtifitl jj] Oschargs

~	Sludge

£T

Sample Comment {where and how the sample was collected); Q Grab ( i fompovti' U Modlfed [j oilier:

fh U -pH , T^~®~ f&"£-*}

SPS Coordinates
{UTM Zone IS
NAD83 Only)

X Eartteg

[ ¥ Northing

Accuracy (dmkont)







0 Fit- Cncte >)
~ WOP

O Special Project

Sample C

BPS Coordinates



Y Northing



lelmskmm^

¦UTM Zone 15







H" tPe{m««rs)

PAD83 On!y)

===s===^^

L==^^



~ 9DOP

Sample Event Typeifcteckontj

TTCSSss*

~	CorrpiaSnt

~	Emergency Tesjw pedai Pisjject

Sample Type: (check me)

Q Container [] Spill

~	WQC ~ Wipes

0 Groundwater Q Storm Water

~	[_J surface Wate'

[J Sct'imeiii £ J Disctogp
Q Sludge

Onok'rtq Wite Supply

LDPR:

FEBEC

[job Cotte:

rMce 10,

Sample D

IDPR:

FEBEC

Facility ID:

S»a/Study Name:

jlob Cote;

NJOOBEEC

Sample Comment {where and how the sample was coltectiij:

. I D ** *W7ur',.

BeeCse Manufacturing

__	pi Com()osjti, f] Mofsr^g

County:

iSample Reference !D:

Dunklin



6 PS Coordinates
(UTM Zone 15
NAD83 Only}

X Easting

Y Northing

Accuracy

{chic* tmej

0*~^*{m5Brer*

~ POOP

Sample Event Tvpt: {check ant}

IIW^mQ

~	Complaint

Q	Emergency Response

O	Inspection

(3	Investigation

~	Monitoring

~	Special Project

Saw pie Type: jehtdtom)

~	«r	13 Sal

~	Container Q Spill

~	QA/QC ~ Wipes

0 Groundwater Q Storm Water
D Organic Q Surface

~	Sediment (3 JSfscharje
f) "jiLdgp

Water Su;

MONR Pnrfl r>m* nr^l Swrvfres Pros-ram

?710W»<;1 Main t»ffn/tnn Cl*v MO fiMOT WIS)	q

D*»*m •» «-r


-------
r



MISSOURI DEPARTMENT OF NATURAL RESOURCES
FIELD SHEET AMD CHA1N-OF-CUSTODY RECORD

Description of Delivery
[I Tape sealed and initialed	Total No. Of Containers:

f~] Shipped	Carrier:		

0 Hand Delivered	By;	



Cclector's Name:
f«ea« Print)

Kenneth Hannon

Affiliation: D WRO	Q"SSo

[~1 MoDOT ~ MDC

Sample Mumber

i» '*! (*'

(Sample A|

for tab Use Only

Sample
Collected

DaW

5/11/2016

lime:

,D»te:

(Sawpfe i)

for Lab Use Only

TJ fcvTO"

[1 DHSS

i.P0"
~ Other:

"~ SWRO n WPP ~ MGS O HWT R f-SP

Analyses Requested

Total and Bexavaleot Cr.

Disinfect.



Type



'rhecknae)

D.O.

PI None

Mow

{_"] Chfenne

..

n »•

Corwl.

LJ 0!hpf*

Othet_._

Field Parameters
imiyJe u/iitsi

zjz:

•+- ¦

_ 4——

i

V

-4	

=t

¦+—¦

——

	L	

	

LftB USE ONLY I

Laboratory ID:

\6Q5QOO^

Matrix

(fftftA .vw:

#5	Water
~

["I	Orginit

~	SwU*

! "J	Ctbe-

5coma „c*f\

D Water

r	^

lJ	5>«j»nit

y

\"J	OtJwi

Container
Type

Preservative
Type

T

locaticn.

1>1A~

Number of
Containers

¦	I	

"p

—J—

_J_

+
_4~

i=
+1

I Date

|j«iph; C)

tor Lab i

Ontftir

{Sample P|

far Isb Us* Only

Relinquished By;

Relinquished By



Reilnoulshec) By;



D.O.

L3

riow

fl {"»¦<•«!

P'

~ IW

tend

L~l UWHJ



n

Ol'.e,

——

f~1 Water
Sol

Otqaita
I I Sludge

' ] vther

~

n

T~

L I	Now

I]	th'ttrtw

~	uv

1 1	0»!«

LJ

P.O.

Flow

pH

Cond

Temp,

_j_

4_

—,i

• -4-

OPw

lj	xv3w<
Li

fl	^nfcie

~	Other:

±

deceived By;



?eeelved 3y:

?ecel«d 9y;

Date:

Tiw

4 o

Tinw

Time;

mows Eiwlronrneitai Sfretces Program

2710 West Main,	Dry. MO 65300 (573) 526431S

Pigtlttfl


-------
MISSOURI DEPARTMENT Of NATURAL RESOURCES
FIELD SHEET AND CHAIN-OF-CU5TQDY RECORD .

Sample A

FEBEC

Code;

NJOOBEEC

Sample Reference ID;

Facility ID;

SPS Coordinates
(UTM Zoae 15
WAP83 Only)

Stte/Stuif Name:

Bee tee Manufacturing

County:

Sample Comment (where and how the sample wss collected):

l3> 1/ *>d tA*f>L .

0 Stib fl Oxvpottr ~ Modifwd"

Dunklin
rl otv •

X Easting

YNortMpg

Accuracy

(check one}

LJ £l'£ {meters)
fl POOP

Sample Event Type:(check me)

~	8yp«VS5Q

{_)	CMiiipiafnt

Q	fcmenjency Raspefce

Q	Inspection

0	Investigation

t~l	Mcwtloi'ftg

0	SfifiMt Project

Sample Type: (check a*;

Air

Container
OVQC

O son
~

~

spill

Wipes

Groundwater ~ Stotm Water
Organic ~ Surface Water
Sfdiment [fj Disdta»ge
Sludge
Printing Water Supply

Sampei pint;

Job Code:

Sample Reference ID:

FadRty IB;

Site/Study Name:

Sample Comment (where and how the sample wa» colectpdh

~ 6H»H ~ Composite ~

Other!

GPS Coordinates
(UTM Zone IS
WADM Onl#		

Sample C

X Easting

y Worth Inf

Accuracy

(check om)
0 frPf (rr«s^)

k

POOP

jjarnple Event Ifpeiftfewtonej

Sypaa/SSO

Q	Complaint

O	Emergency Response

Q	Inspection

Q	InvestSgitlon

O	Monitoring

O	SpetMl P(&|«*

Sample Ty pe: letiesk em}

[Tis—~

[_] Coinstner f~l Sp-li

~	QVQC Q Wipes

[J	Groundwattt Q Storm Water

O	Organic (

~	Mdtmert Q DiscfM">'

~	Sludge

~	DrinMng Water Supply

IDPR;

lob Coda:

[sanipie Rfteren

Facility ID:

Site/Study Name:

Sample Comment {where and how the simple was collected);

Li Ottwr;

SPS Coordinates
{UTM Zone 15
HA083 Only)

X tasting"

V Northing

Accuracy

(Atckam)

Q tP£ (meters)
~ POOP

Sample Event Typeset coe/

~	B^pass/SSD
O	Compirtnt

O	Emergency Response

~	Inspection

~	investigation
Q	MonAwing

~	Special Project

Sample Type: (check one)

~	Air	Q	Sol!

~	Container	~	Sp«i

~	WQC	~	Mpas

jH]	Groundwater	Q	Storm Water

Q	Organic

~	Sediment	["J	Discharge

~	Staff®

~	DfinMnfl Water Supply

Sample D u>ph:

Job Coda:

"jsample

Reference 10:

facility ID:

Site/Study Name:

Sample Comment (where and how th« sample was collected):

County:

n »»t>	rrMoSsr™



Other:

GPS Coordinates
{UTM Zone IS
NAD83 Only)

Remarks:

X Easting

¥ Worthing

Accuracy

Icheck me)
ETepe 'm etas)

Sample Event Iype;/ci>ectoMj

~	ayp«vsso

Q	Complaint

~	Emergency Response

~	Inspection
Q	Investigation
Q	Monitoring

Special Project

Sample Type: ftfretk em!

~	**	~	Soli

~	Container	f]	SpAi

mm	D	Mpes

Groundwater	Q	Storm Water

Q Ongante	Q	Surfaa Water

fl Swimrnt	["|	Dtalwoe

n siudee

B

5-z-o

MDNR Environmental Sarvfces Projrwn

*710 W«t Main tafftwmn Cllv MO (TClf*) HIV

*1 -\t "1


-------


Missouri Department of Natural

Environmental Services Progiam

PO Box 178 Jetfetson Citv MO 05102-0176

RESULTS OF SAMPLE ANALYSES

LDPR/Job Code;
FEBEC/NJOOBEEC

Program, Conuct.
HWP Evan Kifer

Evan Kifer

Hazardous Waste Program

ces

Order ID
150512000

Report Date:
6/28/2016

II

Sample: AC73276

llllllll	Site: Bee Gee Manufacturing

Collect Date: 5/11/2016 2:35:00 PM	Collector: KENNETH HANNON

Comments: Grab, MW-06. ID# 162765

Customer #: 162765

County: Dunktm
Affiliation: ESP

Project: NJ00E

Test

6020 Metais-Totai Recoverable

Dissolved Hexavaient Chromium

Field pH

Field Specie Conductivity

Field Temperature
field Turtidity

Sample: AC73277

lllillilllllll Slte: BeeCeefcfe

Collect Date: 511112018 3:00 00 PM	Collecto

Parameter/Method	Result

Chrcmium/SW 846 6020	<0 80

Dissolved Hexavaient	0 0025

Chrommm/SW 846 71$6A

Field pH/EPA !50 1	6 34
Field Specific Conductiviiy/SM 2510 266 u$/cro

Field 'I empefaiye/l-'PA 70 1	20 0 C

Kieid 'Uiffai(My.TPA	v _

Units

U§fl
mg/L

pH Units

MTU

Qualifter(s)

NO. 06

05

HANNON

Comment*. Grab. MW-05, ID# 162756

Customer f: 162/66

County: Dunklin
Affiliation: ESP

Project: NJ00BPEC

[Test

BlkV VMais let< > Kr crxerable

rtpxtiaier,; v momiurn

If iWd pri

)f ip>d Jpeafic Co iductivity
field Temperature
,F «eid <

Parameter/Method
Chromsuni/SW 846 6020
Dissolved Hexavaient
Chronwm/SW 646 7196A
Field pH/EFA 150 1
Field Specific Conduct v.ty
Field Temperature/E^A 1?,
field Tuibidity/EPA 18«i *

Result

7,5?

0 0098

6 46

2510 108 9 uSIcm
tS 2 C
1.1

Units

Mi/i
mg/l

pH Units

MTU

Qualifierts)

06

Order ID: 180812009 (1/2)

Page 1 of 2


-------
Customer #; 16278?

Site: E

>0 PM

Dunklin

Affiliat

Pararnoter/Mothod

/cm

pH Units

Project:

QuaUfter(s)

NO, 06

m

ltd i ufbidity	__

S i»'v>rh> 4C""32,?^

1

Collect Data:

Site; Bee Gee Manufacturing

1 55 00 PM	Collector;	¦ >'

Affiliat

Dunklin

Project: NJOOBEEC

iissolvecl Hexavatent Chromti
¦i eld pH

ietcl Specific Conductivity
>ield Temperature

"	^€7,1180

p.t II-k it n

alltct Date:

6 18

12510 150 2 uS/cm
18 6 C

<1

Site: Bee Gee Mam

I	Collector:

pH Unite

Metals-1 otal Recoverable crtromium/bw two ou/u
>ived Hexavatent Chromium Dissolved Hexavalent

Chromium/SW 848 7196

Result
5 92
0 0075

ncl Duplicate

Units

Ijgit

mg/L

impie was perioirm

-1 £35

i t>ii > ¦"! • i > s appio,

Affilia

Dunklm

P

Project: N

Qualifier(3)

06

PQI

015 Estimated value QC data eulsnle linns

Curl Luecktnhoff,

-,i »• -j	-> i • . f." -

t • < < 1>, !•' in'» i '	
-------
r i"

L< , h

(' ¦¦

P.'

:	yV;

r

7,

r;...:

„	_

; v1 ; .

i.,.

i-.

•• ; C
<

¦



?"> i \ r u < *	• , *-v

~i1 7" : ' ¦ : ~

Ub

.->7,.* -l u r: '
, r

¦¦



r' t.-0 ---r ¦


-------



-------
Abbreviated Sampling Report
Bee Cee Manufacturing Site
Maiden. Dunklin ( ounty, MO

Site Information:

1 I >i,R Code: 1 fOFC _ ESP Staff: Ken Harmon

Job (We: MWih'.		

Investigation Oau? S_S '7 .					

Introduction:

Hazardous Waste Piogram (HWT) requested the rnvinur.tu'jita! Services Program (IrSP)
peisonnci collect groutidwa.ei grab samples iVora font momtonng wc'K at the Bee fee
Manufacturing Site located in Maiden, Dunkim ( os.mt>„ Missouri Sampling w,>s conducted as
part oi an annuai ground u atei momtoting event I*V»P F nuronmentat Specialist ken Harmon
trav clcd to the site on August 8. ,'!!)! 7, to conduct :,t>rop!nu;. HWP Lnuromntntal Specialist
Kvle Anderson was also present dining die Mamphtig euait.

Field Methods:

KSP personnel deployed clean V i P polvetnvlcnc uibiot> to vuihin the screened inki val of

each well The tubing \\ as attached to a penraalne pump, which \vf>s used to evacuate each well
at a flow rate ot'appfoxnnatei) 2u()->it«a to!'minute Personnel placed the tubing clown to the
bottom of the well ami then polled the tubing up two feet to or,sure water was being dtawn from
within each well's scjeened mtet\al i\uuuted watct nas co".ected m a five-gallon backet and
latet poured out on the ground aw a v. ftom lie >udi;

Personnel determine*! wMu	parameters cwtv three minutes during well evacuation and

samples v\ ere collected once parameters stahih.'ed (pH 40.2, tarhidi»y - 50 Nephelometric
1 urbidit) Units j N'tland spec*tic conductance and h-niperature u ithm ! tSample
toiuainerh weie then tilled directh from the "atlwtg, Specific conductance, temperature,
turbidity, and pi I measurements weie tecoidcd at die time each sample aa% collected Samples
were filtered arid or preserved in the fit Id as appropriate tor the analytic of concent and placed
on ice in coolers, All samples were transposed hack to the SfSP laboratory in Jefferson City and.
submitted for total arid he\a\alent chromium juahses,

Observations:

All wells' protective casings aad 'uek.s were intact upon atmai The weather during sampling
was hunttv and approximately 84 dc^'txs Fahrenheit Winds nere hom the northwest at 8-3 2

miles per how.


-------
No wells contained any significant amount of turbidity. All well samples collected were
considered clear, colorless and odorless.

Refer to I able i tor a tleseuHton and :oeation o! each wimple collected Retei u< Table 2 for
iuhlitional nitonrutjon recorded for cuds nioim\>nn;.: we!!. \Im> attached ate the chain of custody
and analytical results of samples collected

hue Sappmgkni
' >rn Chief

F:t\ iioatneiual Rirtetgeney Response/Field Services Unit
PnvmMimental Services Program

Kyle Anderson, Environmental Specialist, BWP

Kenneth liaaiuui

Fin jfonmeffliii Specialist
Field Set \ ices Us til
l;nvmmmenM( Kervk-es Program

:APPROVED


-------
I JlM<1 I

Sample I

Bee (Vc Manof.Rliinn^ >ire
Maiden. Dunklin (\mm\, Missouri
Aus'u^t X. ?OI v

[i Kamplr

aai,

Time

i iSiiiisbf

k otii-'CU'd



TT^'.'Tt"

I/I/I?



1 ?' - :"s ^

SSI'

i ^4(1

vt;} i y

	8/1/17

1611

"•vYi-i;

"f/g/1?

1628



S -•? 1

if.'S

 \il MH
U ll.'t •)! h\\\ -4

tas clear and colorless.
v..;t^plc was clear and colorless.

°.impts' was clear and colorless.
W.tk't it' M\\ ^ S.sm^l!.jv\as cUm; ,uui;oVlos

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m

llltflftt RESOURCES
CUSTOOV RECORD

StertSTSS1"'

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ll »'«<«*

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Analyse* R«quested

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Missouri Department of Natural Resources

Environmental Services Program

PO Box 176 Jefferson City MO 65102-0176

RESULTS OF SAMPLE ANALYSES

LDPR/Job Code:	Program, Contact

FEBEC/NJOOBEEC	HWP t- van Kiten

Order ID:
170809005

Report Date;
9/1/2017

Evan Kifer

Hazardous Waste Program

Sample; AD05722
Collect Date; 8/8/201? 3,2' :00

Test

6020 Metals-Total RecovwaHt
Dissolved Hexavalerit Chromium

Field pH

f«eW Specific Conductivity
Fieh! Tempetaturs
Field Turbidity		

Customer f; 173? 17

Site; Bee Cee Manufacturing	County. Dunklin

ffd	Collector; KEN HANNON	Affiliation- FSP'ECR

Comments: Gut) WW 0r>. ID* 1732 !?

Project- NJ00BEEC

Pa'ameter-Metftod _	Result

Ch'omiiiftvSVV 846 6021,	0,59

Dissolved Hexavalent	<0.00?
Chromium,fSW 846 ?196A

Field pH€ PA 150 I	G t»9
field Specific Conductivity,'SM i'510 444 0 u$/crn

Fiolu Temperature,'EP4 1	1 ,i0 i' C

Ftekl turblilitv/EPA 180 1	1,0

U	iifier(s)__

j-ci-'t	Cft

mg/l	ND

pH i, IpitS

N1U

Sample: AD05723

ill!

Customer#;

Site, flee Cee Manufacturing
Collect Date; 8/8/2017 3;46;Q0 PM	Collector; KEN hAMNON

/,C 1B

Count

Affiliation; l">

lim

Comments, MVY-05, 'Off i7*V IP

Project; NJ00BEEC

Test

60i>0 Wetais-Tolal Recoverable!
Dissolved H«xava!ent Chromium

field ph

Field Specific Conductivity
Field Temperature
Field Turbidity

Param«rter/M»thod_	Result

Ch urn U!»i 'SW 84c 6020	9 45

HPxaWent	0 0^0
CrfamHi'ivSW b46 719»-V\

field pM.1-"p'\ 1*>0 t	n -V

Field Sptvi'ic ConciuctMfv SM	'0 19b C uSH.m

Field te^iper.ituie.FPA 110	> ?3 0 €

field Turbiclity/Ef-A 1Sf t	*-t

QualMerjsj

Order ID: 170809005 (1/2)

Paget of2


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Sample: AD05724

Collect Dale: 8/8/2017 4:11:00 PM

Comments: Grab; MW-04, ID# 173219.

Project: NJOQBEEC

Test _

6020 Metjiis? Tut.f ^ ovevn"
Dissolved Hewweri

Field siH

Fiold Specific Cmt'ii I.viiy

Field Temperature

Field 1 urfaidity _ 		

Result

Pararneter'MetSioa _ __

Cr.ro«n,*.'-i/^l\ two 00 ,Y	vt)

r.iMtoU^d Hfx.H.'iuri	>vf!
i h; omt *m 8'/v 7

field pH/EPA 150.1	7.76

1 n-> mv<, *1," * "su t v tySM	-M6 h . S en

Field Temperature/EPA 170.1	18.8 C

Htiii "'iitVit/'H'A UH' i	„

Units

Qualiiertsl

ND
ND

pH Units

NTU

Sample: AD05T25

Hlltili 1111 illl 1

iiiiw hm ,»s «iii: n:s
Collect Dale" «/8/;l0 i ? 4,28:00 PM

Site: Bee Cee Manufacturing

Collector; KEN HAtMWON

Customer #: 173220

County: Dunklin

Affiliation- tSFMLER

Test

PaiamehniWi'thad

Comments; Grab: MW-03, ID# 173220,
Result	Units

Project: NJ00I

Qualifier^)

8020 Metals-Total Recoverable	Clromfu«-i'GvV »niv'{3

Dissolved Haxavaient Chromium	Dissolved Hexavalenf

Chromium/SW 848 7196A

Field pH	> i S,i j-li j PA '• V :

Field Specific Conductivity	« i? r>M * *£

Field Turbidity	!-»jd 'tulnv1«;v:	1

pH Units

NTU

Sample: AD05726

1111(11111111

Site: Bee Cee Manufacturing

Collect Date: 8/8/2017 12:00:00 AM

Collector: KEI

Customer # 17322?

County: Dunklin

Affiliation: ESP/EER

C -ab:BIir»cl Duplicate.

Profect: NJOOBEECj

Test

6020 Metals ~ ^:al Rt»cou-r >h t*
Dissolved Hoxavaein Cbwtttr"

ParamoteuMetiiod
Ok-mijrn SVV 546 K' .T
Di&seketl

iJhrcm'uns.Sl'v' ' 19I5A

Resu.t
14 5
0 011'

Units

T.„,

malt

Qualifier^)

•	«!;>«• iVWv'.ort t\ii

M,'< VVi tp'1 .iM.'po-teii ,jn t-

he arj'js>> j! ttvs s	ochn t* >< ,< t> w'ts jus < - - * t'd o* uvr y '¦•zitf i\ ;}"«*¦ v S f'l i»vs

Kevin Thoenert,

Laboratory Manager
Environmental Services Program
Division of Environmental Quality

Order ID; 170809005 (2/2)

Page 2 of 2


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